Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
DRC-2012-001194 - 0901a068802b2d2d
DRC.2012-00119A DENISO MINES Denison Mines (USA) Corp 1050 17th Street Suite 950 Denver CO 80265 USA Tel 303 628 7798 Fax 303 3894125 www denisonmines com February 28 2012 VIA FEDERAL EXPRESS Mr Rusty Lundberg Co Executive Secretary Utah Department of Environmental Quality 195 North 1950 West Salt Lake City UT 84114 4820 DearMr Lundberg Re State of Utah Radioactive Material License No UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July 1,2011 through December 31,2011 As required by Utah Administrative Code R 313 24 4 (incorporating by reference 10 CFR 40 65 (subpartl)) and License Condition 11 3A of Stale of Utah Radioactive Matenals License No UTl900479 enclosed is the Semi Annual Affluent Momtonng Report for the White Mesa Mill for the penod July 1 2011 through December 31, 2011 Dunng the period Denison did not collect a running surface water sample from Westwater Canyon for all of the required analytes Ihis is noted in Section 6 0 of this report pursuant to Utah Administrative Code R314 14 15(c) (in) An altemative sample was collected for all analytes as discussed m that Section Corrective actions to prevent recurrence are also reported m Section 6 0 If you have any questions regardmg this report please contact the undersigned at (303) 389 4132 Yours very truly DENISON MINES (USA) CORP Jo Ann Tischler Director Compliance and Permitting cc RonF Hochstein Harold R Roberts David C Frydenlund David E Turk Katherine Wemel February 28, 2012 VIA FEDERAL EXPRESS Mr. Rusty Lundberg Co-Executive Secretary Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84114-4820 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July 1,2011 through December 31, 2011 Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303 628·7798 Fax: 303 3894125 www.denisonmines.com As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpartl», and License Condition 11.3A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period July 1,2011 through December 31,2011. During the period, Denison did not collect a "running" surface water sample from Westwater Canyon for all of the required analytes. This is noted in Section 6.0 of this report, pursuant to Utah Administrative Code R314-14-15( c) (iii). An alternative sample was collected for all analytes as discussed in that Section. Corrective actions to prevent recurrence are also reported in Section 6.0. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly, ~~ DENISON MINES (USA) CORP. Jo Ann Tischler Director, Compliance and Permitting CC Ron F. Hochstein Harold R. Roberts David C. Frydenlund David E. Turk Katherine Weinel White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (July through December, 2011) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 February 28, 2012 Table of Contents 1.0 IN"TRODUCTION .................................................................................................. 1 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLIN"G ..................................... 2 2.1 Program Overview ............................................................................................... 2 2.2 Sampling Protocol and Analytical Results ........................................................... 2 2.3 General Observations ............. ~ ............................................................................. 3 2.4 Site Specific Sampling Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ............................................................ .' ........................ 8 5.0 STACK SAMPLIN"G ............................................................................................... 9 6.0 SURFACE WATER MONITORIN"G .................................................................... 11 7.0 SOIL SAMPLIN"G ................................................................................................. 12 8.0 METEOROLOGICAL MONITORIN"G ................................................................. 12 9.0 SIGNATURE ......................................................................................................... 13 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-210 Concentration Example Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits) Table 6 Environmental OSL Dosimeter Measurements (Gamma) Table 7 Stack Sampling Requirements Table 8 Stack Effluent Concentrations and Release Rates INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tab 1 BHV-l Air Sampling Graphs and Data Table Tab 2 BHV -2 Air Sampling Graphs and Data Table Tab 3 BHV -3 Air Sampling Graphs and Data Table Tab 4 BHV -4 Air Sampling Graphs and Data Table Tab 5 BHV -5 Air Sampling Graphs and Data Table Tab 6 BHV -6 Air Sampling Graphs and Data Table C Air Particulate Loading Graphs and QAlQC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Graphs, Data Table, Laboratory Results and QAlQC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QAlQC 11 WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER, 2011 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5 (east), and BHV-4 (south). BHV-1 serves as a surrogate for the nearest resident (BHV -1 is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV-3), which was monitored for airborne particulate up until November, 1995, at which time background was established, but is no longer monitored for air particulate; and • A station specifically requested by the White Mesa Ute Community south of the Mill Site (BVH-6); a) External (direct) gamma radiation measured at air monitoring stations BHV -1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6; b) Vegetation at three site periphery locations, for uptake of radiation; c) Stack release rates from the Mill's air emissions sources; d) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; e) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; 1 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\Jul_to_Dec_201 LSAER_text.docx t) Groundwater (up and down gradient) of the Mill facility; andl g) Seeps and springs in the vicinity of the Mill.l This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV-l, BHV-2, BHV-4, and BHV-5) are requIred by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV -3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring data base had been compiled at BHV -3 to establish a representative airborne radionuclide background for the Mill. It should be noted, however, that while air sampling was discontinued at this location, gamma measurements and soil sampling continue to be collected at BHV-3. In addition to the environmental air sampling locations described above, an additional station (BHV -6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb- 210 activity. Fugitive dust standards for the facility are limited by the Mill's State of Utah Air Approval Order, which sets a 20% visual opacity standard. The specific 1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 N:\Required Reports\Semi Annual Effluent Reports\20ll July to Dec\JuCto_Dec_20l CSAER_text.docx locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled High Volume Air Monitoring Stations included as Attachment A. Station BHV- 3, which is no longer sampled for air particulate is located approximately 3.5 miles west of the Mill facility and is not indicated on that Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this July through December, 2011 reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QAlQC information) reported by the laboratory for the July through December 2011 time period are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and composited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station for the second half of 2011 and the underlying data are included as Attachment D. It should be noted that for graphical illustration purposes, values reported at zero, values reported at less than the prescribed detection limit « 1 x 10-16 uCi/ml) and missing values were plotted as 1 x 10-16 uCi/ml concentrations. Where other "less than" values were indicated (i.e., where detection limits for the data varied from 1 x 10-16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-210 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay 3 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\JuLto_Dec_2011_SAER_text.docx products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 below, demonstrating elevated Pb-210 activity where no uranium milling operations are located nearby. Pb-210 activity concentrations can be expected to be even higher for locations in the western U.S. where uranium ore bodies are commonly located. In April 1977, prior to Mill construction and Mill operations, air particulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/ml (13.0E-3 pCi/m3)2 Table 1-NCRP Report 94-Global Pb-210 Concentration Example . State Pb-210 Concentration uBqlM3 . uCilml , California 600 1.6E-14 illinois 1500 4.1E-14 Ohio 300 8.1E-15 Massachusetts 700 1.9E-14 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data supports the conclusion that airborne particulate is well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower Limits of Detection consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract analytical laboratory for this reporting period. In fact, the data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has ever exceeded the ECL at the Mill. With regard to that particular single measurement, 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30,1978, Section 2.9.1.1 4 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\JuLto_Dec_201 LSAER_text.docx while it is important to consider and evaluate an individual measurement exceeding the ECL, for public dose estimation purposes, it is the average annual concentration that is of primary significance. In that instance, the average annual concentration of Th-230 for BHV -5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALARA goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 3rd and 4th Quarters 2011 Monitoring 3rd Qtr. 4th Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (EeL) ECL (uCi/ml) BHVI 2.92E-16 6.73E-16 9.00E-14 5.36E-OI BHV2 l.17E-16 3.65E-16 9.00E-14 2.68E-OI BHV4 l.32E-15 I.04E-15 9.00E-14 1.3IE+OO BHV5 3.IIE-15 4.44E-15 9.00E-14 4.I9E+OO BHV6 2.05E-15 -3.I4E-15 9.00E-14 2.88E+OO Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 3rd and 4th Quarters 2011 Monitoring 3rd Qtr. 4th Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/nU) Limit (ECL) . ECL (uCi/ml) BHVI l.17E-16 l.19E-16 2.00E-14 5.90E-OI BHV2 3.04E-17 2.72E-17 2.00E-14 1.44E-OI BHV4 7.89E-16 3.25E-16 2.00E-14 2.79E+OO BHV5 l.14E-15 2.I4E-15 2.00E-14 8.20E+OO BHV6 6.I2E-16 l.09E-15 2.00E-14 4.26E+OO 5 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\JuLto_Dec_201 LSAER_text.docx Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 3rd and 4th Quarters 2011 Monitoring 3rd Qtr. . 4th Qtr. Effluent Average Station Result Result . Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVI 6.76E-17 8.58E-17 9.00E-13 8.52E-03 BHV2 2.81E-17 4.54E-17 9.00E-13 4.08E-03 BHV4 1.28E-16 2.28E-16 9.00E-13 1.98E-02 BHV5 5.75E-16 1.53E-15 9.00E-13 1. 17E-Ol BHV6 1.88E-16 7.65E-16 9.00E-13 5.29E-02 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 3rd and 4th Quarters 2011 Monitoring 3rd Qtr. 4th Qtr. Effluent Average Station Result Result .. Concentration Percent (uCi/ml) (uCi/ml) Limit· (ECL) ECL (uCi/ml) BHVI 1.14E-14 1.73E-14 6.00E-13 2.39E+00 BHV2 1.03E-14 1.58E-14 6.00E-13 2. 18E+00 BHV4 1.18E-14 1.14E-14 6.00E-13 1.93E+00 BHV5 1.41E-14 2.05E-14 6.00E-13 2.88E+00 BHV6 9.93E-15 1.89E-14 6.00E-13 2.40E+00 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the revised 10 CFR Part 20 standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was discontinued in 1995. Instead, Denison demonstrates compliance with these limits and the requirements of R313-15-301 by calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division of Radiation Control ("DRC") on July 28,2008. This calculation is performed by use of the Mll..DOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The anal ysis under both the MILDOS and Mll..DOS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the concentrations of radioactive dust and radon at individual receptor locations around the Mill. 6 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\1uLto_Dec_201 CSAER_text.docx The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 1 00 mrem regulatory limit in R313-15-301 (1)( a) for all pathways, including air particulate and radon, and well below the AhARA goal of 10 mremlyr for air emissions excluding radon as set out in R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U30 8 and 1.5% V 205) and Arizona Strip ore (0.637% U30 8). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -1 at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the 3rd and 4th quarters of 2011 utilizing passive integrating devices, optically stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-l, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). Measurements obtained from location BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented at Attachment E to this report. 7 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\Jul_to_Dec_201 LSAER_text.docx Table 6-Environmental Optically Stimulated Luminescence Dosimeter ~easurements(;amma) Monitoring 3rd Qtr 4th Qtr 3rd Qtr 4th Qtr Cumulative Station Res:ult Result Result Less .. Result Less Semi- (mrem) (mrem) Background Background Annual (mrem) (mrem) Estimate * (mrem) BHVI 39.6 31.5 7.7 4.1 11.8 BHV2 33.7 25.9 1.8 -1.5 1.8 BHV3 31.9 27.4 0 0 0 BHV4 33.9 27.7 2 0.3 2.3 BHV5 40.6 29.9 8.7 2.5 11.2 BHV6 34.7 29.9 2.8 2.5 5.3 *Negative values treated as zero for cumulative dose The results for this period indicate that above background measurements for stations BVH-1, BVH-2, BVH-4, BVH-5 and BHV-6 are within regulatory limits. BHV-1 is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV-l. The annual individual member of the public limit is 100 mrem/yr for combined internal and external exposure. 4.0 VE(;ETATION SA~PLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. The U.S. Nuclear Regulatory Commission ("NRC") Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. During the 2011 grazing season, three sets of samples have been collected, on June 23, 2011, July 27, 2011, and November 23, 2011. At the conclusion of the third quarter of 2011, three sets of samples have been collected consistent with Regulatory Guide 4.14. The data from the June 2011 sampling is included in the January to June 2011 Semi-Annual Effluent Report ("SAER") which was submitted to the DRC on August 31, 2011. Data from the July and November sampling events are included in this report. Section 4.2 of the Mill's Environmental Protection Manual states that vegetation samples are to be collected during the early spring, late spring and fall (i.e., the growing seasons). During the January to June 2011 period, the early spring samples were inadvertently omitted. The late spring sample was collected just past the end of spring (on June 23, 2011). An additional summer sample was collected on July 27, 2011 in place of the omitted early spring sample. As a result, as discussed above, three samples have been collected by the end of the 2011 grazing season meeting the requirements of NRC Regulatory Guide 4.14. 8 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\1uLto_Dec_201 LSAER_text.docx Graphical log-scale presentation of the vegetation sampling results, together with the analytical results reported by the Mill's contract laboratory (including QAlQC information) for this sampling period, are included at Attachment F of this report. The 2011 data results are within the variation of previous sampling episodes. 5.0 STACK SAMPLING Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: DUSA-1, 2/07 (the "Environmental Protection Manual") gas stack samples are collected at the Mill in accordance with the calendar year schedule shown below: Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging Baghouse) Yellowcake Dryer (Yellowcake Baghouse) Quarterly None If operating, U -nat If operating, U-nat Semi -annuall y If operating, U-nat, If operating, U-nat, If operating, U-nat, Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-210 The yellowcake dryer and yellowcake baghouse did not operate during the 3rd quarter of 2011 due to a maintenance shutdown of the facility, and therefore, no gas stack samples were collected during the 3rd quarter of 2011. The yellowcake dryer, yellowcake baghouse, and grizzly operated during the 4th quarter of 2011. The analytical results of stack sampling conducted for the 1 st and 2nd Quarter of 2011 and for the 4th Quarter of 2011, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate (uCi/sec) for U-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The actual analytical results reported by the laboratory for the 4th quarter of 2011 are provided in Attachment G to this report. It is also . important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL's for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi-annual reporting purposes. 9 N:\Required Reports\Serni Annual Effluent Reports\2011 July to Dec\Jul_to_Dec_201 LSAER_text.docx North YC Dryer, Run 1 North YC Dryer, Run 2 Yellowcake Baghouse North YC Dryer, Run 1 North YC Dryer, Run 2 Yellowcake Baghouse Grizzly Baghouse Table 8-Stack Effluent Concentrations and Release Rates V-Nat. Th-230 Th-230 Ra-226 Ra-226 V-Nat u/Ci/Cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec Pb-210 uCi/cc Pb-210 uCi/sec ~' • ,' ••• iJ'J ~. ,:~;, ;'li:~ :.~ '", , t _ i,\;1., \!Ivl \~~. . f/;' :c" -'ic'~l '. ~~: '", . ~ " ,~. -('" .<1 ",,~rt l)." " ;'1"" S.02E-09 3. 17E-03 Not Not Not Not Not Not Required Required Required Required Required Required 3.67E-09 1.93E-03 Not Not Not Not Not Not Required Required Required Required Required Required 2.90E-09 2.92E-03 Required Required Required Not Not Not Not Required Required Required Not . Not 1.76E-08 9.21E-03 1.76E-12 9.2SE-07 4.20E-14 2.20E-08 7.S2E-12 3.94E-06 1.S4E-08 7.S6E-03 2.12E-12 1.04E-06 4.79E-14 2.3SE-08 7.94E-12 3.90E-06 8.S8E-09 8.22E-03 1.97E-ll 1. 89E-OS 1.96E-13 1.88E-07 8.32E-13 7.97E-07 9.71E-12 S.96E-06 1.09E-13 6.67E-08 .," ".1< Not Not Not Required Required Required . " Not Required . . ,. ~'i', Ii 3rd Qtr, 2011 North YC Dryer, Run 1 North YC Dryer, Run 2 Yellowcake Baghouse .: .:: ' "\~, !o', '" ,. ~"4th Qtr, 2011 . '. North YC Dryer, Run 1 North YC Dryer, Run 2 Yellowcake Baghouse Grizzly Baghouse No samples were collected as the facility was not operating due to a maintenance shutdown. Not Required Not Required Not Required '"" Not Not Not Not Not Required Required Required Not Not Not Required Required Required Not Not Not Required Required Required Required Not · Required Required Not Required Not ./ Not Required · Required ;; i·, ".'F I , '/,,':, ~. 6.02E-12 3.S2E-06 2.96E-13 1.74E-07 7.4SE-14 4.36E-08 3.91E-12 2.29E-06 8.29E-09 4.74E-03 7.76E-13 4.43E-07 S.S3E-14 3.16E-08 S.00E-12 2.8SE-06 1.08E-09 1.17E-03 4.0SE-13 4.38E-07 3.99E-14 4.31E-08 6.73E-12 3.81E-06 1.47E-13 Not Not Required Required 8.33E-08 10 1.98E-13 Not Required 2. 14E-07 Not Required N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\JuLto_Dec201 LSAER_text.docx 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Cottonwood Creek is an intermittent ephemeral drainage located southwest and down- gradient of the Mill complex. Westwater Canyon is a drainage located west of the Mill facility, which is rarely flowing. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample in the event that surface water is not available for sampling. Westwater Canyon surface water was not sampled in the 1st or 2nd quarter 2011 because no water was present during that reporting period. A surface water sample was collected from Westwater Canyon during the 3rd quarter 2011; however, the sample was not analyzed for all of the constituents required under the License, part 11.2 B. The 3rd quarter 2011 sample was only analyzed for total dissolved solids ("TDS") and total suspended solids ("TSS"). The inadvertent omission was noted in the 4th quarter 2011, and repeated attempts were made to collect the sample prior to the end of the quarter. No surface water was present for sampling, and there was no opportunity for hand tool development of the site for the collection of pooled surface water due to seasonal conditions. The License, part 11.2 B, states that "A sediment sample shall not be taken in place of a water sample unless a water sample was not available." Surface water was present during the reporting period, and as such the collection of a sediment sample in lieu of surface water was not allowable per the License requirement in Part 11.2 B. During the latter part of the 4th quarter 2011, snow/frozen precipitation was present on the surface of the locations routinely sampled. Because the snow would become "running" surface water upon thawing, the snow/frozen precipitation overlaying the sample sites was substituted for the surface water sample for Westwater Canyon. The sample was collected, allowed to melt and submitted for analysis of all of the required constituents. The data from the analysis of that sample is included in Attachment H. Denison has noted the failure to collect a "running" surface water sample from Westwater Canyon for all of the constituents listed in the License, part 11.2 B. An investigation into the root cause of the failure and the corrective actions taken to prevent recurrence was completed by the Mill's QA Manager. The cause of this inadvertent omission was due to Mill Personnel changes and confusion related to implementation of the Standard Operating Procedure ("SOP") for surface water sampling. To address prevention of recurrence, Denison has noted that the Mill Personnel changes are complete and the responsible Mill Personnel have been apprised and alerted to the previous omission. Additionally, Mill Personnel responsible for the surface water sampling have been retrained on the SOP and have been requested to read the SOP prior to each planned sampling event. The Mill's Environmental Protection Manual, requires that Cottonwood Creek be sampled for TDS and total suspended solids TSS quarterly, and the License, Part 11.2 B requires that Cottonwood Creek be sampled for dissolved and suspended radionuclides 11 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\Jul_to_Dec_201 LSAER_text.docx including Gross Alpha, Unat, Ra-226, Th-230 semi-annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS and TSS during the 3rd quarter. Surface water was not collected from Cottonwood Creek during the 4th quarter of 2011 because there was no surface water present during the quarter. The field data sheets for the surface water sampling events, along with graphs showing historic results are included as Attachment H. The results of this sampling indicate that surface water results remain low and within the range of typical background. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6) once per year during August or as soon as possible thereafter, but no later than September 30 of each year. In accordance with the Mill's Environmental Protection Manual, surface soils were collected in August 2011. All soil samples were analyzed, on a dry basis, for Ra-226 and U-nat. Annual soil samples were collected at the six air monitoring stations. The results of these samplings indicate that soils at the air monitoring stations remain low and within the range of typical background. A graphical presentation of historical results for soils at the air monitoring stations, together with analytical sample results for the August 2011 sampling are provided in Attachment I. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of July through December, 2011. This information is retained at the Mill site for agency review. 12 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\JuLto_Dec_201 LSAER_text.docx 9.0 SIGNATURE This Report was prepared by Denison Mines (USA) Corp. on February 28, 2012. Denison Mines (USA) Corp. David C. Frydenlund Vice President, Regulatory Affairs and Counsel 13 N:\Required Reports\Semi Annual Effluent Reports\2011 July to Dec\.Jul_to_Dec201 LSAER_text.docx ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS w:\USI\\tJIal'I\M!I\::!.~\.~..IaIn:aIJM,P.!anMllCPlan 3.z.rlna!\r IC 2.3<t J4101t2Plt ~"tIUtli¢bilalar '1 ~ ~.-J .". ) ( : .... ~ ., ...... I I , ~A ... ,' ,I) :. , ,l~'; ,--.J ~"~ 1""> V BHV-2 o ;0 N , I l /.l "'1 ~ J I I.' / / , I • ,<ft / , I #.., \' LL I "'., 1" I-f~ I - 4' : .. ' ~ I I I ~ 1# \\ '. I) /~; I II II j l I .~~ ',,: *,,,\ / 2000 o 2000 \ I SCALE IN FrrT / \ ~., !,I ~'T ::! i r i ' ' _, ! j "Ci , ( \ , ( ,~ -.. '; , '# ~I r#,! " \ \' -(-' * :: / '\ \. ! I " ... .,. I ) ... \ r--" "\ ..... ""-H. I / ~ .. " ,,--C~~-;~ : -- \ Il ~t / '" ~e'i>~ .. / '~ ;,/- / ) t.......-• ,,,,_11 : , ... 0& .~ "./ \ , I \ / J I \ , I ( r' ; ; t 2 \ 5 ; i , " z ,/ \ I I ) "----'\ \ \ \ I "\, ',,,,, , I <" ,II' I .. ... I ... "'" i..>.~ I_ .. ?-~I# ..... ,~ I --\. --I .. \. I , .. \ l .. \ ~/ \ ,~"""',,-: vi ~~ '--; (~ _n_1I Property Boundary Reservation Boundary Canyon Rim o BHV-5 BHV-6 ~ 40 .. ~ ..... j : .. , .". " I ... .. ' , ~ luI oc: > \ ")~ ... I ... ... I ... o Air Monitor Stations "-~ I ... ... I ~ \ ... ... I -1 I! j\\: .. ' .. --~. ... 1 \'-:. -. \. i.\\t #., " 'II.. \~ I ~ J .. -', ~ f _ \.~J\\ At\~ '1 .'" ~ c. ~ J ! I '-i -~ ! ..L.. --.., ~I"'~ II "~ ",""" ~ Denison Mines (USA) Corp. Projee.t WHITE MESA MILL REVISIONS laIe: lIT [late Figure 2.3-1 ..J #7"", , 4l\ .,. ~ .. ," ~ ...... ., WI "-" ... ".. \ .". .c I <10; , ... ' Jo. I }l 1" ## o""ISQJ}i~ Mlllats ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV-l AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB I ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = ' 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.3SE-1S S.OOE-12 1.2SE-12 7.82E-16 8.00E-14 2.00E-14 1.06E-1S 2.00E-12 S.OOE-13 2.S7E-14 4.00E-12 1.00E-12 12/14/1981 1.S6E-1S S.00E-12 1.2SE-12 1.49E-1S 8.00E-14 2.00E-14 1.93E-1S 2.00E-12 S.OOE-13 2.64E-14 4.00E-12 1.00E-12 3/29/1982 2.16E-1S S.00E-12 1.2SE-12 2.93E-1S 8.00E-14 2.00E-14 1.16E-1S 2.00E-12 S.OOE-13 2.09E-14 4.00E-12 1.00E-12 6/30/1982 4.69E-1S S.00E-12 1.2SE-12 3.46E-1S 8.00E-14 2.00E-14 2.38E-1S 2.00E-12 S.OOE-13 2.14E-14 4.00E-12 1.00E-12 9/27/1982 4.4SE-1S S.00E-12 1.2SE-12 3.29E-1S 8.00E-14 2.00E-14 3.23E-1S 2.00E-12 S.OOE-13 1.99E-14 4.00E-12 1.00E-12 1/3/1983 4.39E-1S S.00E-12 1.2SE-12 S.91E-16 8.00E-14 2.00E-14 9.14E-16 2.00E-12 S.OOE-13 4.87E-14 4.00E-12 1.00E-12 4/4/1983 7.SlE-16 S.00E-12 1.2SE-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 S.OOE-13 1.88E-14 4.00E-12 1.00E-12 6/30/1983 2.68E-16 S.00E-12 1.2SE-12 6.92E-16 8.00E-14 2.00E-14 7.92E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 1.00E-12 10/3/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/3/1984 2.87E-1S S.00E-12 1.2SE-12 1.14E-16 8.00E-14 2.00E-14 1.79E-16 2.00E-12 S.OOE-13 1.06E-14 4.00E-12 1.00E-12 4/2/1984 1.S9E-1S S.00E-12 1.2SE-12 3.40E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.34E-14 4.00E-12 1.00E-12 7/2/1984 3.10E-1S S.00E-12 1.2SE-12 1.00E-1S 8.00E-14 2.00E-14 2.09E-1S 2.00E-12 S.OOE-13 1.88E-14 4.00E-12 1.00E-12 10/1/1984 6.42E-16 S.00E-12 1.2SE-12 1.39E-16 8.00E-14 2.00E-14 1.94E-16 2.00E-12 S.OOE-13 1.8SE-14 4.00E-12 1.00E-12 1/2/1985 S.06E-16 S.00E-12 1.2SE-12 4.S6E-16 8.00E-14 2.00E-14 3.49E-16 2.00E-12 S.OOE-13 3.03E-14 4.00E-12 1.00E-12 4/1/1985 O.OOE+OO S.OOE-12 1.2SE-12 1.23E-1S 8.00E-14 2.00E-14 4.88E-16 2.00E-12 S.OOE-13 8.06E-1S 4.00E-12 1.00E-12 7/1/1985 7.17E-16 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 1.0SE-1S 2.00E-12 S.OOE-13 2.1SE-14 4.00E-12 1.00E-12 9/30/1985 6.13E-16 S.00E-12 1.2SE-12 1.18E-16 8.00E-14 2.00E-14 3.7lE-16 2.00E-12 S.OOE-13 3.64E-1S 4.00E-12 1.00E-12 1/2/1986 3.42E-1S S.00E-12 1.2SE-12 4.74E-16 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/1/1986 3.98E-1S S.00E-12 1.2SE-12 9.74E-16 8.00E-14 2.00E-14 1.S0E-1S 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 1.00E-12 6/30/1986 S.SlE-17 S.00E-12 1.2SE-12 3.S2E-16 8.00E-14 2.00E-14 1.37E-1S 2.00E-12 S.OOE-13 1.23E-14 4.00E-12 1.00E-12 10/27/1986 1.99E-1S S.OOE-12 1.2SE-12 3.06E-16 8.00E-14 2.00E-14 1.2SE-1S 2.00E-12 S.OOE-13 1.08E-14 4.00E-12 1.00E-12 12/15/1986 1.67E-1S S.00E-12 1.2SE-12 l.16E-16 8.00E-14 2.00E-14 S.98E-16 2.00E-12 S.OOE-13 l.37E-14 4.00E-12 l.OOE-12 3/16/1987 2.33E-1S S.00E-12 l.2SE-12 4.30E-16 8.00E-14 2.00E-14 l.92E-16 2.00E-12 S.OOE-13 S.S9E-14 4.00E-12 l.OOE-12 5/11/1987 2.36E-1S S.00E-12 1.2SE-12 7.69E-16 8.00E-14 2.00E-14 8.76E-16 2.00E-12 S.OOE-13 l.4SE-14 4.00E-12 l.OOE-12 9/9/1987 2.27E-1S S.00E-12 l.2SE-12 2.44E-1S 8.00E-14 2.00E-14 8.S1E-16 2.00E-12 S.OOE-13 3.14E-14 4.00E-12 1.00E-12 11/2/1987 2.7SE-1S S.00E-12 1.2SE-12 2.46E-1S 8.00E-14 2.00E-14 l.34E-1S 2.00E-12 S.OOE-13 2.79E-14 4.00E-12 1.00E-12 2/16/1988 1.07E-1S S.00E-12 l.2SE-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 2.00E-12 S.OOE-13 4.0lE-14 4.00E-12 1.00E-12 5/18/1988 l.98E-1S S.00E-12 l.2SE-12 1.2SE-1S 8.00E-14 2.00E-14 6.40E-16 2.00E-12 S.OOE-13 l.07E-14 4.00E-12 l.OOE-12 8/15/1988 2.06E-1S S.00E-12 1.2SE-12 3.41E-1S 8.00E-14 2.00E-14 S.08E-16 2.00E-12 S.OOE-13 l.62E-14 4.00E-12 l.OOE-12 11/14/1988 3.94E-1S S.00E-12 l.2SE-12 2.12E-1S 8.00E-14 2.00E-14 l.01E-1S 2.00E-12 S.OOE-13 2.47E-14 4.00E-12 l.OOE-12 2/13/1989 l.99E-1S S.00E-12 1.2SE-12 S.73E-16 8.00E-14 2.00E-14 S.99E-16 2.00E-12 S.OOE-13 3.23E-14 4.00E-12 l.OOE-12 5/15/1989 l.70E-1S S.00E-12 l.2SE-12 6.32E-16 8.00E-14 2.00E-14 S.86E-16 2.00E-12 S.OOE-13 6.16E-IS 4.00E-12 l.OOE-12 8/14/1989 2.3lE-1S S.00E-12 l.2SE-12 2.31E-16 o 8.00E-14 2.00E-14 1.77E-16 2.00E-12 S.OOE-13 7.6SE-1S 4.00E-12 1.00E-12 11/13/1989 4.72E-1S S.00E-12 1.2SE-12 l.71E-1S 8.00E-14 2.00E-14 l.S2E-1S 2.00E-12 S.OOE-13 1.89E-14 4.00E-12 1.00E-12 2/12/1990 3.44E-16 S.00E-12 l.2SE-12 8.39E-16 8.00E-14 2.00E-14 8.31E-16 2.00E-12 S.OOE-13 2.S7E-14 4.00E-12 l.OOE-12 5/14/1990 3.03E-1S S.00E-12 l.2SE-12 l.47E-1S 8.00E-14 2.00E-14 l.04E-1S 2.00E-12 S.OOE-13 l.79E-14 4.00E-12 l.OOE-12 8/13/1990 1.64E-1S S.00E-12 l.2SE-12 l.49E-IS 8.00E-14 2.00E-14 3.34E-16 2.00E-12 S.OOE-13 8.27E-1S 4.00E-12 l.OOE-12 11/12/1990 1.48E-1S S.00E-12 l.2SE-12 7.S0E-16 8.00E-14 2.00E-14 S.80E-16 2.00E-12 S.OOE-13 2.16E-14 4.00E-12 l.00E-12 2/11/1991 l.90E-16 S.00E-12 l.2SE-12 3.48E-17 8.00E-14 2.00E-14 7.91E-17 2.00E-12 S.OOE-13 3.79E-14 4.00E-12 1.00E-12 5/13/1991 3.42E-16 S.00E-12 1.2SE-12 1.34E-1S 8.00E-14 2.00E-14 7.39E-16 2.00E-12 S.OOE-13 l.46E-14 4.00E-12 1.00E-12 8/12/1991 2.77E-16 S.00E-12 l.2SE-12 4.17E-17 8.00E-14 2.00E-14 l.4SE-16 2.00E-12 S.OOE-13 l.80E-14 4.00E-12 1.00E-12 11/11/1991 6.6SE-17 S.00E-12 1.2SE-12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 S.OOE-13 1.06E-14 4.00E-12 l.OOE-12 2/10/1992 1.94E-16 S.00E-12 l.2SE-12 4.28E-17 8.00E-14 2.00E-14 4.08E-17 2.00E-12 S.OOE-13 3.S1E-14 4.00E-12 l.OOE-12 5/11/1992 2.S4E-16 S.00E-12 l.2SE-12 6.49E-16 8.00E-14 2.00E-14 6.86E-17 2.00E-12 S.OOE-13 1.38E-14 4.00E-12 l.OOE-12 8/10/1992 l.73E-16 S.00E-12 l.2SE-12 l.SSE-16 8.00E-14 2.00E-14 l.20E-16 2.00E-12 S.OOE-13 l.S3E-14 4.00E-12 l.OOE-12 11/9/1992 l.S6E-16 S.00E-12 l.2SE-12 3.19E-17 8.00E-14 2.00E-14 4.90E-18 2.00E-12 S.OOE-13 l.86E-14 4.00E-12 1.00E-12 2/9/1993 2.10E-16 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 3.89E-17 2.00E-12 S.OOE-13 2.S2E-14 4.00E-12 l.OOE-12 5/10/1993 l.00E-16 s.00E-12 1.2sE-12 4.11E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 S.OOE-13 l.26E-14 4.00E-12 l.OOE-12 8/10/1993 2.30E-16 s .00E-12 1.2SE-12 6.00E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 S.OOE-13 1.60E-14 4.00E-12 l.OOE-12 11/8/1993 S.00E-12 l.2sE-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 l.s7E-14 4.00E-12 l.OOE-12 2/7/1994 1.82E-16 S.00E-12 l.2sE-12 S.00E-18 8.00E-14 2.00E-14 4.30E-17 2.00E-12 S.OOE-13 2.S9E-14 4.00E-12 l.00E-12 5/9/1994 3.60E-16 s.00E-12 l.2SE-12 2.70E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 s.OOE-13 l.60E-14 4.00E-12 1.00E-12 8/9/1994 4.04E-16 S.00E-12 l.2SE-12 2.70E-16 8.00E-14 2.00E-14 2.94E-16 2.00E-12 s.OOE-13 2.00E-1S 4.00E-12 1.00E-12 11/7/1994 9.18E-17 S.00E-12 l.2SE-12 3.60E-16 8.00E-14 2.00E-14 2.9lE-16 2.00E-12 S.OOE-13 2.00E-1S 4.00E-12 l.OOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARA Goal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 L77E-16 9.00E-14 2.2sE-14 9.70E-17 2.00E-14 s.00E-1s 9.70E-17 9.00E-13 2.2sE-13 8.60E-1s 6.00E-13 LsOE-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 s.36E-16 2.00E-14 s.00E-1s L60E-1s 9.00E-13 2.2sE-13 3.84E-1s 6.00E-13 LsOE-13 8/9/1995 2.70E-16 9.00E-14 2.2sE-14 L60E-16 2.00E-14 s.00E-1s 2.76E-16 9.00E-13 2.2sE-13 3.76E-1s 6.00E-13 1.s0E-13 11/11/199S 4.80E-1s 9.00E-14 2.2sE-14 6.41E-16 2.00E-14 s.00E-1s 8.93E-16 9.00E-13 2.2sE-13 s.20E~ls 6.00E-13 LsOE-13 2/5/1996 S.34E-1S 9.00E-14 2.2sE-14 2.30E-1s 2.00E-14 s.00E-1s l.30E-1S 9.00E-13 2.2sE-13 4.20E-1s 6.00E-13 LsOE-13 5/6/1996 s.llE-16 9.00E-14 2.2sE-14 3.06E-16 2.00E-14 S.00E-1s L40E-16 9.00E-13 2.2sE-13 7.03E-1s 6.00E-13 LsOE-13 8/5/1996 s.99E-16 9.00E-14 2.2sE-14 LsSE-1S 2.00E-14 S.00E-1s 2.03E-16 9.00E-13 2.2sE-13 s.94E-1s 6.00E-13 LsOE-13 11/6/1996 3.38E-16 9.00E-14 2.2sE-14 S.4sE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 L22E-14 6.00E-13 LsOE-13 2/6/1997 LOOE-16 9.00E-14 2.2sE-14 L2sE-16 2.00E-14 s.00E-1s L28E-16 9.00E-13 2.2sE-13 s.68E-1s 6.00E-13 LsOE-13 5/5/1997 L09E-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 4.39E-1s 6.00E-13 LsOE-13 8/11/1997 2.88E-16 9.00E-14 2.2sE-14 3.83E-16 2.00E-14 s.00E-1s L82E-16 9.00E-13 2.2sE-13 s.29E-1s 6.00E-13 LsOE-13 1/5/1998 3.24E-16 9.00E-14 2.2SE-14 3.47E-16 2.00E-14 s.00E-1s L19E-16 9.00E-13 2.2sE-13 4.73E-1s 6.00E-13 LsOE-13 4/28/1998 4.7sE-16 9.00E-14 2.2sE-14 6.73E-16 2.00E-14 s.00E-1s s.69E-16 9.00E-13 2.2sE-13 s.94E-1s 6.00E-13 LsOE-13 7/31/1998 8.84E-16 9.00E-14 2.2sE-14 L93E-1s 2.00E-14 s.00E-1s 1.43E-1s 9.00E-13 2.2sE-13 s.22E-1s 6.00E-13 1.s0E-13 9/28/1998 2.8lE-16 9.00E-14 2.2sE-14 2.89E-16 2.00E-14 s.00E-1s L80E-16 9.00E-13 2.2sE-13 4.64E-1s 6.00E-13 1.s0E-13 12/28/1998 8.08E-16 9.00E-14 2.2sE-14 4.93E-16 2.00E-14 s.00E-1s s.OlE-16 9.00E-13 2.2sE-13 1.06E-14 6.00E-13 LsOE-13 3/29/1999 2.06E-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 s.00E-1S L42E-16 9.00E-13 2.2sE-13 6.69E-1s 6.00E-13 LsOE-13 7/3/1999 s.31E-16 9.00E-14 2.2sE-14 2.47E-16 2.00E-14 s.00E-1s 2.23E-16 9.00E-13 2.2sE-13 6.44E-1s 6.00E-13 LsOE-13 9/27/1999 8.98E-16 9.00E-14 2.2sE-14 3.90E-16 2.00E-14 s.00E-1s 2.96E-16 9.00E-13 2.2sE-13 7.29E-1s 6.00E-13 LsOE-13 12/28/1999 1.48E-1s 9.00E-14 2.2sE-14 6.00E-16 2.00E-14 s.00E-1s s.s7E-16 9.00E-13 2.2sE-13 6.19E-1s 6.00E-13 LsOE-13 3/27/2000 LOOE-16 9.00E-14 2.2SE-14 L06E-16 2.00E-14 S.00E-1s LOOE-16 9.00E-13 2.2SE-13 6.23E-1s 6.00E-13 1.s0E-13 6/26/2000 3.47E-16 9.00E-14 2.2SE-14 3.46E-16 2.00E-14 s.00E-1s 3.62E-16 9.00E-13 2.2sE-13 4.s0E-1s 6.00E-13 1.s0E-13 9/26/2000 2.slE-16 9.00E-14 2.2sE-14 1.78E-16 2.00E-14 s.00E-1s 3.2sE-16 9.00E-13 2.2sE-13 8.ssE-1s 6.00E-13 LsOE-13 12/26/2000 LOOE-16 9.00E-14 2.2sE-14 L42E-16 2.00E-14 s.00E-1s L31E-16 9.00E-13 2.2sE-13 7.77E-1s 6.00E-13 LsOE-13 3/26/2001 3.10E-16 9.00E-14 2.2sE-14 LOOE-1s 2.00E-14 s.09E-1s LOOE-1s 9.00E-13 2.2sE-13 7.19E-1s 6.00E-13 LsOE-13 7/29/2001 Ls2E-16 9.00E-14 2.2sE-14 L44E-16 2.00E-14 s.00E-1s L77E-16 9.00E-13 2.2sE-13 7.21E-1s 6.00E-13 LsOE-13 9/24/2001 L03E-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 8.09E-1s 6.00E-13 LsOE-13 , 12/31/2001 LOOE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 l.39E-1S 6.00E-13 LSOE-13 4/1/2002 2.0sE-16 9.00E-14 2.2sE-14 2.44E-16 2.00E-14 s.00E-1S 2.29E-16 9.00E-13 2.2sE-13 8.1sEc1s 6.00E-13 LsOE-13 7/1/2002 3.ssE-16 9.00E-14 2.2sE-14 4.8sE-16 2.00E-14 s.00E-1s L06E-16 9.00E-13 2.2sE-13 7.6sE-1s 6.00E-13 LSOE-13 9/30/2002 L17E-16 9.00E-14 2.2sE-14 L61E-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 3.68E-1s 6.00E-13 l.SOE-13 12/30/2002 LOOE-16 9.00E-14 2.2SE-14 L03E-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 9.46E-1S 6.00E-13 LsOE-13 3/31/2003 L20E-16 9.00E-14 2.2sE-14 L12E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.68E-1s 6.00E-13 LsOE-13 6/30/2003 2.18E-16 9.00E-14 2.2sE-14 3.40E-16 2.00E-14 S.00E-1s L67E-16 9.00E-13 2.2sE-13 s.96E-1s 6.00E-13 1.s0E-13 9/29/2003 LOOE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 S.00E-1s LOOE-16 9.00E-13 2.2sE-13 7.28E-1s 6.00E-13 LsOE-13 12/29/2003 LOOE-16 9.00E-14 2.2sE-14 2.s4E-16 2.00E-14 S.00E-1s 3.3sE-16 9.00E-13 2.2sE-13 6.2sE-1s 6.00E-13 LsOE-13 3/29/2004 LOOE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1S LOOE-16 9.00E-13 2.2sE-13 1.s4E-14 6.00E-13 LsOE-13 6/27/2004 1.00E-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1S LOOE-16 9.00E-13 2.2sE-13 3.04E-1s 6.00E-13 LsOE-13 9/27/2004 LOOE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 LOsE-14 6.00E-13 LsOE-13 12/27/2004 LOOE-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 LS9E-14 6.00E-13 LsOE-13 3/28/2005 LOOE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 7.42E-1s 6.00E-13 LsOE-13 6/29/2005 LOOE-16 9.00E-14 2.2sE-14 L30E-16 2.00E-14 s.00E-1s L20E-16 9.00E-13 2.2SE-13 7.94E-1s 6.00E-13 1.s0E-13 9/26/2005 LOOE-16 9.00E-14 2.2sE-14 2.s6E-16 2.00E-14 s.00E-1s 2.42E-16 9.00E-13 2.2sE-13 L22E-14 6.00E-13 1.s0E-13 1/3/2006 2.13E-16 9.00E-14 2.2sE-14 1.04E-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 3.73E-14 6.00E-13 LsOE-13 4/3/2006 1.62E-16 9.00E-14 2.2sE-14 L86E-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 8.36E-1s 6.00E-13 LsOE-13 7/3/2006 L86E-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 9.77E-1s 6.00E-13 LsOE-13 10/2/2006 LOOE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 L30E-14 6.00E-13 1.S0E-13 1/1/2007 LOOE-16 9.00E-14 2.2sE-14 L47E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 L17E-14 6.00E-13 LsOE-13 4/2/2007 2.23E-16 9.00E-14 2.2sE-14 L63E-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 L6sE-14 6.00E-13 LsOE-13 7/2/2007 3.3sE-16 9.00E-14 2.2sE-14 l.34E-16 2.00E-14 s.00E-1s L36E-16 9.00E-13 2.2sE-13 L78E-14 6.00E-13 LsOE-13 9/30/2007 L1sE-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 7.68E-1s 6.00E-13 1.S0E-13 12/31/2007 LOOE-16 9.00E-14 2.2sE-14 L93E-16 2.00E-14 s .00E-1s LOOE-16 9.00E-13 2.2sE-13 L3lE-14 6.00E-13 1.s0E-13 3/31/2008 L14E-16 9.00E-14 2.2sE-14 L13E-16 2.00E-14 s .00E-1s LOOE-16 9.00E-13 2.2sE-13 6.44E-1s 6.00E-13 LsOE-13 6/30/2008 7.09E-16 9.00E-14 2.2sE-14 3.83E-16 2.00E-14 s.00E-1s 2.27E-16 9.00E-13 2.2sE-13 6.s2E-1s 6.00E-13 LsOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-1T Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = SE-13 uCi/ml BHV-1PB ALARA Goal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal = 2.2SE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/200S 7.69E-16 9.00E-14 2.2SE-14 2.94E-16 2.00E-14 S.00E-1S 1.90E-16 9.00E-13 2.2SE-13 7.64E-1S 6.00E-13 l.S0E-13 ! 12/31/200S 1.21E-1S 9.00E-14 2.2SE-14 4.76E-16 2.00E-14 S.00E-1S 3.34E-16 9.00E-13 2.2SE-13 1.16E-14 6.00E-13 1.S0E-13 3/15/2009 2.14E-1S 9.00E-14 2.2SE-14 1.02E-1S 2.00E-14 S.00E-1S 1.00E-1S 9.00E-13 2.2SE-13 4.44E-1S 6.00E-13 ' 1.S0E-13 6/15/2009 S.97E-17 9.00E-14 2.2SE-14 2.3SE-16 2.00E-14 S.00E-1S 2.1SE-16 9.00E-13 2.2SE-13 S.13E-1S 6.00E-13 l.S0E-13 9/15/2009 9.SSE-16 9.00E-14 2.2SE-14 1.71E-16 2.00E-14 S.00E-1S 9.S7E-17 9.00E-13 2.2SE-13 9.47E-1S 6.00E-13 l.S0E-13 12/15/2009 1.24E-1S 9.00E-14 2.2SE-14 9.2SE-17 2.00E-14 S.00E-1S S.60E-17 9.00E-13 2.2SE-13 S.9SE-1S 6.00E-13 1.S0E-13 3/31/2010 1.97E-1S 9.00E-14 2.2SE-14 2.1SE-16 2.00E-14 S.00E-1S 3.27E-16 9.00E-13 2.2SE-13 1.00E-14 6.00E-13 l.S0E-13 6/30/2010 l.SSE-1S 9.00E-14 2.2SE-14 4.71E-16 2.00E-14 S.00E-1S 7.70E-16 9.00E-13 2.2SE-13 4.07E-1S 6.00E-13 1.S0E-13 9/30/2010 S.42E-16 9.00E-14 2.2SE-14 2.S0E-16 2.00E-14 S.00E-1S 1.31E-16 9.00E-13 2.2SE-13 6.S0E-1S 6.00E-13 l.S0E-13 12/31/2010 1.27E-1S 9.00E-14 2.2SE-14 2.32E-16 2.00E-14 S.00E-1S 2.30E-16 9.00E-13 2.2SE-13 1.27E-14 6.00E-13 1.S0E-13 4/4/2011 9.0lE-16 9.00E-14 2.2SE-14 1.90E-16 2.00E-14 S.00E-1S 3.64E-16 9.00E-13 2.2SE-13 1.09E-14 6.00E-13 l.S0E-13 7/4/2011 1.S9E-1S 9.00E-14 2.2SE-14 S.31E-16 2.00E-14 S.00E-1S 4.99E-16 9.00E-13 2.2SE-13 S.3SE-1S 6.00E-13 1.S0E-13 10/3/2011 2.92E-16 9.00E-14 2.2SE-14 1.17E-16 2.00E-14 S.00E-1S 6.76E-17 9.00E-13 2.2SE-13 1. 14E-14 6.00E-13 1.S0E-13 1/3/2012 6.73E-16 9.00E-14 2.2SE-14 1.19E-16 2.00E-14 S.00E-1S S.SSE-17 9.00E-13 2.2SE-13 1.73E-14 6.00E-13 1.S0E-13 -E ::::: (.) :::l -f/) c: o .~ co '-... c: CI) u c: o (.) CI) -c u :::l c: o -c co a: ,.... :> ~ m C\J or-uJ 0 ~ Cf) or-uJ 0 ~ I~ I- ~ • «: i~ ~~ ---.... ~ -.c:: • ~ [!. I~ 1«: ~ I· f:::::: ~ tc: ~ N ;:::: 1< t-- ~ fi. ~ 0, ~ • ~ .. -;;;;;;; --;J .. ~ ~ ~ t I· ~' ~ ~ ~ ~F::: ; ~ . ...q or- uJ 0 ~ -:::.~ X ~ 14lIl 1llli i:~ ~ .!--~ .:: ~ ~ .... ... :.-.... :::::::.111 :.~ ~ • IJtV ::... ~-~ ~~ I ~~~ ~ ...... ~ .:. ~ ~ ~-des o~-des 60-deS BO-deS La-deS 90-des so-des --~~~ ,~ ..-.' .« ~ '~~ ... :-~ . ... -~. ..-:-< --~-.... ::.6 ~ 4"::::: va-des 0 so-des or- C\J -b Go-des co Q) .....J ~o-des t ;::. ,~ • . OO-deS <.0 C\J ~ .. ~ ~~ ~ .... -~ 66-deS C\J E ~~ .~ ~ .. -::? ... ~» ::! ~ +c:::: ~ ~~ B6-deS ::J ~ co L6-deS a: t 96-deS !]~ ... --. . ~ ~~t ::::::= ~ .111"" :::::: ~~tl" ~ r-. • ~ la~ ~ ~ :...4 ~ ~ ~ ~~~ ~ .... S6-deS 0 Cf) C\J v6-deS E ::J ·c S6-deS 0 ..c r- G6-deS + ~6-des ct1 ~ ..cf":; _P::ot ~ 06-deS ::J ~ .... iP'f' r--. ~ ~ t~ ~~ ~ '"--A. ,.~ z 6B-deS E ::J BB-deS 'c ~ ::::s. .... 1 -.::: » ..... ~I-" 4~'~ ~ LB-deS :::> t 9B-deS ~ -v ...... t;::---r---... ~ ~h.. SB-des --vB-des .... ~ ..-...... ! .... SB-des tA ~ .--.-GB-deS ~ ~ ~ ~B-des L.{) <.0 r---co or-or-or-or- uJ uJ uJ uJ 0 0 0 0 ~ ~ ~ ~ (ereos DOl ) 1.00E-11 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml 1.00E-12 I I 1.00E-13 I r Q) (ij o BHV-1 Uranium-Natural Concentrations (uCi/ml) ~.OOE-14 r~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ~ M.A" ~ X tt ~nn_ln_n1_LL___LLn~ .. "..,ft_...L_L.1J\ ___ n __ n_n___________ __--'_nL_ • ~ _nJr ~ __ ~ LI ___ IL M'{ _LLtL6. ., .... , 7'\/\r ,I \ • 1'1 • ~~ V \ I \.... ~ • 1l • V~ Jt. •• I \ 1 \ T ".ll \I~ 1\ 1\. • __ J .. 1.00E-16 L ~ ·V ~ • W u -~ ~ \I v\ ....... [jJ U ~ 1.00E-17 T"" C\J (1) .q-L{) (0 ........ co 0) a T"" C\J (1) .q-L{) (0 ........ co 0) a T"" C\J (1) .q-L{) (0 ........ co 0) a co co co co co co co co co 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) a a a a a a a a a a T"" T"" 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. I 6. 6. 6. 6. 6. 6. a.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) tn c: o "+=i CO '-... c: Q) o c: o o o ('I) C'\I I E :l "~ o J: I- T""" ::> ::I: m --,........ Cf) .q- 'T'-'T'- uJ uJ 0 0 ~ ~ I .. ~ ~F::: ~ ~ ~ ~f::': r.. p ~ !---I--~ "''''''1 ... ~ ~ -R 1+= ~ : ~ 1+= E;: I· F::: [;:1 -"'F-. r+-~ -~ ~ I+F:::: ~ ~ I~~ ~~ ~~ ~ ~t;: .. ~ ~ .... .... ~ -~ -~ ""~ f- i::ood • c::::::::. ~~ ~ .... kill leI--~ ~ ~r c:::::- I .... .... iA ... ~I-" .,.. E =-+ ~. -~ I.~ --~ ~ ~ --tool--f-4t-I-~ ~lJ ..- r-"l-t--r-+ .. r-I--~I-r-6. H·. r. I-r--. !). !.4~ .... ~ ~ I~ i------~ ........ L{) <.0 'T'-'T'-uJ uJ 0 0 0 ~ (ere~s 001) ~ ~-des o~-des 60-deS so-des La-des 90-deS so-des va-des 80-deS Go-des ~o-des OO-deS 66-deS S6-deS L6-deS 96-deS S6-deS v6-deS I~~N~ 86-deS ..... 1-4 G6-deS i-" .. i-~ ... ~6-des 06-deS 6S-deS SS-deS LS-deS 9S-deS SS-deS vS-deS 8s-des GS-deS ~s-des I'--co 'T'-'T'- uJ uJ 0 0 ~ ~ 1.00E-11 1.00E-12 1.00E-13 ---l.OOE-14 Q) (ij () CJ) C') o .....J -r.OOE-15 1.00E-16 1.00E-17 1.00E-18 -- Effluent Concentration limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/mi • ~\ .. 'lV\ ~ ..... ~ .... ~ . \' ""-"I" r1&. ~ ~ ." \ • T \ I II ~ " . ., \ \ 6 \ I V ~ \I \ . ... ... • \It • ... .J \r l' • LL or-C\I ('I) .q-L() co I"--CX) 0) 0 or-C\I CX) CX) CX) CX) CX) CX) CX) CX) CX) 0) 0) 0) a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) .. ('I) 0) a. Q) CJ) BHV-1 Radium-226 Concentrations (uCi/ml) \ " , t ~ 1 ..... I' .. \I J[ I' \ \ \ 1f ...... V 1\ ..li .. \ • 6' 6\ ", T\ • A I V \ 6' \ I \ \ . 1\ • .J l f \. J ~ ~P¥ ~ ~ \JLJV. ~A ...... J \ ...... &~AAj v \ 1)1 <iii .q-L() co I"--CX) 0) 0 or-C\I ('I) .q-L() co I"--CX) 0) 0 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 or-0r-a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) E ...... (3 ::l -t/) c o ";:: as ~ ... c CI) (,) c o o o T-N I "'C as CI) ...J :-. - C\I Ct) ,..... ,..... ,..... uJ uJ uJ 0 0 0 ~ ~ ~ ~ ~ ~-des t. ... ~ o ~-des ~ ~ • "4, 60-deS so-des ~ ~ LO-deS 90-deS "F:: I--- ~ so-des «; f-I-::...1 Po-des .-::::::: ~. ~~. so-des ~o-des -... -f--b6 ~o-des ...... '-f' • t ~~: ~-• , ~~ ~ I~ I-~ ~t OO-deS 66-deS S6-deS L6-deS 96-deS S6-deS w~ P6-deS 1-= [!. I ~ ~ • :::::--~ tc:: r::; ;:::: «: ~ S6-deS ~6-des ~6-des 06-deS 6S-deS ~ • ~ ~~ -~ ~ ~ t:::. ss-des LS-deS l"iCP;;;;;; ~ 9S-deS t.. ... c:::= ~ ~ J I. k ~ ~:::: ~~ ~~ I ss-des Ps-des ss-des ~s-des ~s-des -.;;t L{) co f"-.. ,..... ,..... ,..... ,..... uJ uJ uJ uJ 0 ~ 0 0 0 0 ~ ~ (el1305601) TAB 2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE ~ Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal= 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal = 2.2SE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARAGOAl = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 L39E-1S S.OOE-12 1.2SE-12 3.69E-16 8.00E-14 2.00E-14 S.92E-16 2.00E-12 S.OOE-13 L67E-14 4.00E-12 LOOE-12 12/14/1981 4.62E-16 S.00E-12 L2SE-12 8.03E-16 8.00E-14 2.00E-14 3.62E-16 2.00E-12 S.OOE-13 L33E-14 4.00E-12 LOOE-12 3/29/1982 7.07E-16 S.00E-12 L2SE-12 1.10E-1S 8.00E-14 2.00E-14 7.27E-16 2.00E-12 S.OOE-13 1.S2E-14 4.00E-12 1.00E-12 6/30/1982 8.84E-16 S.00E-12 l.2SE-12 7.73E-16 8.00E-14 2.00E-14 4.78E-16 2.00E-12 S.OOE-13 1.98E-14 4.00E-12 1.00E-12 9/27/1982 l.23E-1S S.00E-12 1.2SE-12 3.60E-16 8.00E-14 2.00E-14 8.73E-16 2.00E-12 S.OOE-13 2.3SE-14 4.00E-12 1.00E-12 1/3/1983 2.64E-1S S.00E-12 1.2SE-12 2.SSE-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 S.OOE-13 2.8SE-14 4.00E-12 1.00E-12 4/4/1983 2.14E-16 S.00E-12 1.2SE-12 1.02E-16 8.00E-14 2.00E-14 l.S7E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 6/30/1983 2.8SE-16 S.00E-12 1.2SE-12 2.06E-16 8.00E-14 2.00E-14 2.24E-16 2.00E-12 S.OOE-13 1.79E-14 4.00E-12 1.00E-12 10/3/1983 2.70E-16 S.00E-12 1.2SE-12 3.36E-16 8.00E-14 2.00E-14 4.37E-16 2.00E-12 S.OOE-13 L78E-14 4.00E-12 1.00E-12 1/3/1984 2.78E-1S S.00E-12 l.2SE-12 1.20E-16 8.00E-14 2.00E-14 6.64E-17 2.00E-12 S.OOE-13 9.14E-1S 4.00E-12 LOOE-12 '4/2/1984 4.28E-16 S.00E-12 1.2SE-12 1.7SE-16 8.00E-14 2.00E-14 4.S7E-17 2.00E-12 S.OOE-13 3.SSE-14 4.00E-12 1.00E-12 7/2/1984 2.78E-1S S.00E-12 1'.2SE-12 8.12E-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 S.OOE-13 1.68E-14 4.00E-12 1.00E-12 10/1/1984 2.69E-16 S.00E-12 1.2SE-12 2.66E-17 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 1.77E-14 4.00E-12 1.00E-12 1/2/1985 2.1SE-16 S.00E-12 1.2SE-12 7.SSE-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 3.19E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 S.00E-12 1.2SE-12 1.67E-16 8.00E-14 2.00E-14 6.7SE-17 2.00E-12 S.OOE-13 7.S6E-1S 4.00E-12 1.00E-12 7/1/1985 3.70E-17 S.00E-12 1.2SE-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 S.OOE-13 1.31E-14 4.00E-12 1.00E-12 9/30/1985 9.32E-17 S.00E-12 1.2SE-12 2.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.64E-1S 4.00E-12 1.00E-12 1/2/1986 1.00E-16 S.00E-12 1.2SE-12 2.16E-16 8.00E-14 2.00E-14 2.1SE-17 2.00E-12 S.OOE-13 3.04E-16 4.00E-12 1.00E-12 4/1/1986 1.31E-1S S.00E-12 1.2SE-12 l.SOE-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 2.90E-1S 4.00E-12 1.00E-12 6/30/1986 2.23E-16 S.00E-12 1.2SE-12 1.32E-16 8.00E-14 2.00E-14 7.09E-17 2.00E-12 S.OOE-13 2.S3E-14 4.00E-12 1.00E-12 10/27/1986 6.41E-16 S.00E-12 1.2SE-12 L74E-16 8.00E-14 2.00E-14 3.67E-16 2.00E-12 S.OOE-13 1.04E-14 4.00E-12 1.00E-12 12/15/1986 3.S6E-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.0SE-16 2.00E-12 S.OOE-13 7.81E-1S 4.00E-12 1.00E-12 3/16/1987 S.31E-16 S.00E-12 1.2SE-12 1.30E-16 8.00E-14 2.00E-14 7.74E-17 2.00E-12 S.OOE-13 3.80E-14 4.00E-12 1.00E-12 5/11/1987 4.06E-16 S.00E-12 1.2SE-12 6.63E-17 8.00E-14 2.00E-14 1.34E-16 2.00E-12 S.OOE-13 1.10E-14 4.00E-12 1.00E-12 9/9/1987 2.74E-16 S.OOE-12 L2SE-12 2.38E-16 8.00E-14 2.00E-14 1.38E-16 2.00E-12 S.OOE-13 1.04E-14 4.00E-12 1.00E-12 11/2/1987 3.73E-16 S.00E-12 1.2SE-12 3.11E-16 8.00E-14 2.00E-14 1.83E-16 2.00E-12 S.OOE-13 1.17E-14 4.00E-12 1.00E-12 2/16/1988 2.78E-1S S.00E-12 1.2SE-12 2.31E-17 8.00E-14 2.00E-14 1.20E-16 2.00E-12 S.OOE-13 3.SSE-14 4.00E-12 1.00E-12 5/18/1988 4.63E-16 S.00E-12 1.2SE-12 1.49E-16 8.00E-14 2.00E-14 2.30E-16 2.00E-12 S.OOE-13 L18E-14 4.00E-12 1.00E-12 8/15/1988 8.06E-16 S.00E-12 1.2SE-12 8.69E-16 8.00E-14 2.00E-14 1.80E-16 2.00E-12 S.OOE-13 1.42E-14 4.00E-12 1.00E-12 11/14/1988 4.34E-16 S.00E-12 l.2SE-12 6.76E-16 8.00E-14 2.00E-14 LS7E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 LOOE-12 2/13/1989 S.80E-16 S.00E-12 L2SE-12 2.8SE-16 8.00E-14 2.00E-14 1.SSE-16 2.00E-12 S.OOE-13 2.80E-14 4.00E-12 LOOE-12 5/15/1989 S.06E-16 S.00E-12 1.2SE-12 2.28E-16 8.00E-14 2.00E-14 L63E-16 2.00E-12 S.OOE-13 6.0SE-1S 4.00E-12 LOOE-12 8/14/1989 4.71E-16 S.00E-12 L2SE-12 9.60E-16 8.00E-14 2.00E-14 l.26E-1S 2.00E-12 S.OOE-13 6.6SE-1S 4.00E-12 LOOE-12 11/13/1989 L14E-1S S.00E-12 L2SE-12 4.08E-16 8.00E-14 2.00E-14 4.18E-16 2.00E-12 S.OOE-13 LS9E-14 4.00E-12 LOOE-12 2/12/1990 L09E-1S S.00E-12 L2SE-12 3.2SE-16 8.00E-14 2.00E-14 3.74E-16 2.00E-12 S.OOE-13 L98E-14 4.00E-12 1.00E-12 5/14/1990 9.32E-16 S.00E-12 1.2SE-12 S.27E-16 8.00E-14 2.00E-14 3.97E-16 2.00E-12 S.OOE-13 L69E-14 4.00E-12 LOOE-12 8/13/1990 L66E-16 S.00E-12 1.2SE-12 S.49E-16 8.00E-14 2.00E-14 4.7SE-17 2.00E-12 S.OOE-13 L27E-1S 4.00E-12 LOOE-12 11/12/1990 6.0SE-16 S.00E-12 1.2SE-12 2.64E-16 8.00E-14 2.00E-14 1.93E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 LOOE-12 2/11/1991 8.72E-17 S.00E-12 L2SE-12 7.00E-18 8.00E-14 2.00E-14 3.33E-17 2.00E-12 S.OOE-13 3.49E-14 4.00E-12 LOOE-12 5/13/1991 L16E-16 S.00E-12 L2SE-12 3.86E-16 8.00E-14 2.00E-14 2.80E-16 2.00E-12 S.OOE-13 LSOE-14 4.00E-12 LOOE-12 8/12/1991 9.02E-17 S.00E-12 L2SE-12 8.82E-17 8.00E-14 2.00E-14 7.6SE-17 2.00E-12 S.OOE-13 LS8E-14 4.00E-12 1.00E-12 11/11/1991 4.81E-17 S.00E-12 1.2SE-12 3.82E-17 8.00E-14 2.00E-14 2.S4E-17 2.00E-12 S.OOE-13 1.4SE-14 4.00E-12 1.00E-12 2/10/1992 1.S4E-16 S.00E-12 1.2SE-12 6.82E-17 8.00E-14 2.00E-14 1.40E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 1.00E-12 5/11/1992 2.38E-16 S.00E-12 L2SE-12 7.63E-17 8.00E-14 2.00E-14 3.07E-17 2.00E-12 S.OOE-13 L27E-14 4.00E-12 LOOE-12 8/10/1992 L01E-16 S.00E-12 L2SE-12 7.07E-17 8.00E-14 2.00E-14 2.80E-17 2.00E-12 S.OOE-13 L41E-14 4.00E-12 LOOE-12 11/9/1992 S.20E-17 S.00E-12 L2SE-12 3.6SE-17 8.00E-14 2.00E-14 L78E-17 2.00E-12 S.OOE-13 L71E-14 4.00E-12 1.00E-12 2/9/1993 2.39E-16 S.00E-12 L2SE-12 2.97E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 LOOE-12 5/10/1993 LOOE-16 S.00E-12 1.2SE-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 S.OOE-13 L34E-14 4.00E-12 LOOE-12 8/10/1993 L90E-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 L80E-14 4.00E-12 LOOE-12 11/8/1993 LOOE-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 1.49E-14 4.00E-12 1.00E-12 2/7/1994 2.23E-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 1.84E-16 2.00E-12 S.OOE-13 2.19E-14 4.00E-12 LOOE-12 5/9/1994 2.16E-16 S.00E-12 1.2SE-12 7.20E-17 8.00E-14 2.00E-14 9.89E-17 2.00E-12 S.OOE-13 L37E-14 4.00E-12 LOOE-12 8/9/1994 9.29E-17 S.00E-12 L2SE-12 2.96E-16 8.00E-14 2.00E-14 3.04E-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 11/7/1994 9.21E-17 S.00E-12 L2SE-12 2.3SE-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARA Goal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.18E-16 9.00E-14 2.2sE-14 9.70E-17 2.00E-14 s.00E-1s 9.70E-17 9.00E-13 2.2sE-13 7.42E-1s 6.00E-13 l.SOE-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 1.20E-16 2.00E-14 s.00E-1s 3.s0E-16 9.00E-13 2.2sE-13 3.90E-1s 6.00E-13 1.s0E-13 8/9/1995 8.90E-17 9.00E-14 2.2sE-14 9.67E-17 2.00E-14 s.00E-1s 1.3sE-16 9.00E-13 2.2sE-13 2.38E-16 6.00E-13 1.s0E-13 11/11/1995 2.83E-1s 9.00E-14 2.2sE-14 4.09E-16 2.00E-14 s.00E-1s s.23E-16 9.00E-13 2.2sE-13 6.77E-1s 6.00E-13 1.s0E-13 2/5/1996 1. 7sE-1s 9.00E-14 2.2sE-14 8.66E-16 2.00E-14 s.00E-1s 4.86E-16 9.00E-13 2.2sE-13 3.s0E-1s 6.00E-13 1.s0E-13 5/6/1996 1.40E-16 9.00E-14 2.2sE-14 1.1sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.8sE-1s 6.00E-13 1.s0E-13 8/5/1996 1.43E-16 9.00E-14 2.2sE-14 2.78E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 s.83E-1s 6.00E-13 1.s0E-13 11/6/1996 1.4sE-16 9.00E-14 2.2sE-14 1.s7E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.19E-14 6.00E-13 1.s0E-13 2/6/1997 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 s.84E-16 6.00E-13 1.s0E-13 5/5/1997 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 3.89E-1s 6.00E-13 1.s0E-13 8/11/1997 1.00E-16 9.00E-14 2.2sE-14 1.09E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 s.69E-1s 6.00E-13 1.s0E-13 1/5/1998 2.ssE-16 9.00E-14 2.2sE-14 1.07E-16 2.00E-14 s.00E-1s s.00E-17 9.00E-13 2.2sE-13 s.l1E-1s 6.00E-13 1.s0E-13 4/28/1998 1.20E-16 9.00E-14 2.2sE-14 1.71E-16 2.00E-14 s.00E-1s 1.28E-16 9.00E-13 2.2sE-13 6.40E-1s 6.00E-13 1.s0E-13 7/31/1998 1.47E-16 9.00E-14 2.2sE-14 4.24E-16 2.00E-14 s.00E-1S 3.39E-16 9.00E-13 2.2sE-13 4.80E-1s 6.00E-13 1.s0E-13 9/28/1998 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.26E-1s 6.00E-13 1.s0E-13 12/28/1998 2.s4E-16 9.00E-14 2.2sE-14 2.1sE-16 2.00E-14 s.00E-1s l.38E-16 9.00E-13 2.2sE-13 6.88E-1s 6.00E-13 1.s0E-13 3/29/1999 1.07E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.61E-1s 6.00E-13 1.s0E-13 7/3/1999 2.46E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.9sE-1s 6.00E-13 1.s0E-13 9/27/1999 2.81E-16 9.00E-14 2.2sE-14 1.41E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.3sE-1s 6.00E-13 1.s0E-13 12/28/1999 s.20E-16 9.00E-14 2.2sE-14 2.60E-16 2.00E-14 s.00E-1s 2.01E-16 9.00E-13 2.2sE-13 7.00E-1s 6.00E-13 1.s0E-13 3/27/2000 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.12E-1s 6.00E-13 1.s0E-13 6/26/2000 1.10E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.16E-16 9.00E-13 2.2sE-13 s.07E-1s 6.00E-13 1.s0E-13 9/26/2000 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 s.31E-1s 6.00E-13 1.s0E-13 12/26/2000 1.26E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.4sE-1s 6.00E-13 1.s0E-13 3/26/2001 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.9sE-1s 6.00E-13 1.s0E-13 7/2/2001 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.s6E-1s 6.00E-13 1.s0E-13 9/24/2001 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.16E-1s 6.00E-13 1.s0E-13 12/31/2001 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 2.20E-1s 6.00E-13 1.s0E-13 4/1/2002 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.9sE-1s 6.00E-13 1.s0E-13 7/1/2002 1.2sE-16 9.00E-14 2.2sE-14 1.43E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 8.2sE-1s 6.00E-13 1.s0E-13 9/30/2002 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 3.69E-1s 6.00E-13 1.s0E-13 12/30/2002 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.91E-1s 6.00E-13 1.s0E-13 3/31/2003 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.16E-1s 6.00E-13 1.s0E-13 6/30/2003 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 s.27E-1s 6.00E-13 1.s0E-13 9/29/2003 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.23E-1s 6.00E-13 1.s0E-13 12/29/2003 1.00E-16 9.00E-14 2.2sE-1~ 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.80E-1s 6.00E-13 1.s0E-13 3/29/2004 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 2.04E-14 6.00E-13 1.s0E-13 6/27/2004 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 3.09E-1s 6.00E-13 1.s0E-13 9/27/2004 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.73E-14 6.00E-13 1.s0E-13 12/27/2004 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.30E-14 6.00E-13 1.s0E-13 3/28/2005 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 8.88E-1s 6.00E-13 1.s0E-13 6/29/2005 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 8.8sE-1s 6.00E-13 1.s0E-13 9/26/2005 1.00E-16 9.00E-14 2.2sE-14 1.99E-16 2.00E-14 s.00E-1s 1.44E-16 9.00E-13 2.2sE-13 3.81E-14 6.00E-13 1.s0E-13 1/3/2006 1.29E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 4.08E-16 9.00E-13 2.2sE-13 6.s8E-14 6.00E-13 1.s0E-13 4/3/2006 1.02E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.08E-14 6.00E-13 1.s0E-13 7/3/2006 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 1.s0E-13 10/2/2006 1.30E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.68E-14 6.00E-13 1.s0E-13 1/1/2007 1.24E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.38E-14 6.00E-13 1.s0E-13 4/2/2007 1.40E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.63E-14 6.00E-13 1.s0E-13 7/2/2007 1.04E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.36E-14 6.00E-13 1.s0E-13 9/30/2007 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 8.24E-1s 6.00E-13 1.s0E-13 12/31/2007 1.91E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.18E-14 6.00E-13 1.s0E-13 3/30/2008 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.49E-1s 6.00E-13 1.s0E-13 6/30/2008 1.29E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.82E-1s 6.00E-13 1.s0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 2.73E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 8.30E-1S 6.00E-13 l.SOE-13 12/31/2008 S.71E-16 9.00E-14 2.2SE-14 l.61E-16 2.00E-14 S.00E-1S l.2SE-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 l.SOE-13 3/15/2009 3.96E-16 9.00E-14 2.2SE-14 1.38E-16 2.00E-14 S.00E-1S l.07E-16 9.00E-13 2.2SE-13 4.81E-1S 6.00E-13 l.SOE-13 6/15/2009 1.24E-17 9.00E-14 2.2SE-14 4.64E-17 2.00E-14 S.00E-1S S.l1E-17 9.00E-13 2.2SE-13 4.S8E-1S 6.00E-13 l.SOE-13 9/15/2009 2.43E-16 9.00E-14 2.2SE-14 S.28E-17 2.00E-14 S.00E-1S 4.84E-17 9.00E-13 2.2SE-13 1.19E-14 6.00E-13 1.S0E-13 12/15/2009 S.72E-16 9.00E-14 2.2SE-14 2.94E-17 2.00E-14 S.00E-1S 2.S7E-17 9.00E-13 2.2SE-13 6.70E-1S 6.00E-13 1.S0E-13 3/31/2010 SA7E-16 9.00E-14 2.2SE-14 l.42E-17 2.00E-14 S.00E-1S 4.66E-17 9.00E-13 2.2SE-13 8.24E-1S 6.00E-13 l.SOE-13 6/30/2010 3.S8E-16 9.00E-14 2.2SE-14 6.64E-17 2.00E-14 S.00E-1S 9.90E-17 9.00E-13 2.2SE-13 2.01E-1S 6.00E-13 l.SOE-13 9/30/2010 2.91E-16 9.00E-14 2.2SE-14 4.48E-17 2.00E-14 S.00E-1S S.72E-17 9.00E-13 2.2SE-13 1.08E-1S 6.00E-13 1.S0E-13 12/31/2010 S.73E-16 9.00E-14 2.2SE-14 7.24E-17 2.00E-14 S.00E-1S 6.76E-17 9.00E-13 2.2SE-13 l.3SE-14 6.00E-13 1.S0E-13 4/4/2011 3.79E-16 9.00E-14 2.2SE-14 4.01E-17 2.00E-14 S.00E-1S 9.11E-17 9.00E-13 2.2SE-13 l.06E-14 6.00E-13 l.SOE-13 7/4/2011 3.07E-16 9.00E-14 2.2SE-14 8.S4E-17 2.00E-14 S.00E-1S 9.21E-17 9.00E-13 2.2SE-13 7.21E-1S 6.00E-13 l.SOE-13 10/3/2011 1.17E-16 9.00E-14 2.2SE-14 3.04E-17 2.00E-14 S.00E-1S 2.81E-17 9.00E-13 2.2SE-13 l.03E-14 6.00E-13 l.SOE-13 1/3/2012 3.6SE-16 9.00E-14 2.2SE-14 2.72E-17 2.00E-14 S.00E-1S 4.S4E-17 9.00E-13 2.2SE-13 l.S8E-14 6.00E-13 l.SOE-13 ~ ~ r--~ "-::::'11 ~ ~ ~~ I--::0 tc~ ~~ ~ ~ ~. • ,~ ::::+ ~ .. += r--~ I ..... ,;a~ -~ .... ~~ tc~ ~ ~~. r-+- ~ ~ .-04 ~ ~-des o~-des 60-des 80-deS La-des 90-deS ~, ....., ... ~~ -..., ~ --so-des ~ va-des ~ ~" ~-. ~~ ~ ~ -I--;::.t -~ --~ ~ ~ ;~~ .-;.) ~ .. oc::::: .... ~ ~ ~ ~ ~-. , .. ~ • .J ~ l +::: ~ ~~ ......... ..... :tj ... ~~ ~ ~~ ~i"'P ':Ii;;.. ........ r. ~ ;a • ~ ~ ~ I. f::::: .. eo. ~= ~ h ~ r. • ~ ~ ~ ~ I. r=:: 1 ~ ~ P. I· :::::::: =-.. ~C ! J :::~ .~ ~ ~ -. ~ ,,- I" ::::::: b ~- ~ 14~ ~ ... ~ • -• l--A ..... -':;;;:::i;: ~ 0 80-deS ,.... C\I -6 em-des ctI Q) .....J ~o-des t aD-des <.0 C\I 66-deS C\I E 86-deS :::J :0 ctI L6-deS a: t 96-deS S6-deS 0 ('f) C\I v6-deS E .~ 86-deS 0 .s::::. r- e6-deS t ~6-des ro '- 06-deS :::J "E z 68-deS E .~ 88-deS c ctI '- L8-deS ::::> t 98-deS T ..... " .-::: S8-deS ~ c::::: ~ .. .... • :::::::: ~ • F "=:II! L ~ ~ -..... -... ~ ,- ~ • .:,;;1 • . .. v8-deS 88-deS e8-deS ~8-des C\I ('f) ""'" L() <.0 ,...... 00 ,.... ,.... ,.... ,.... ,.... ,.... ,.... Lit Lit Lit Lit Lit Lit Lit 0 ~ 0 0 0 0 0 0 ~ ~ ~ ~ ~ ~ (elBos 501) 1.00E-11 1.00E-12 1.00E-13 Q) ro (,) ~ .OOE-14 0) o .....J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml t 1 t J ~ .. 1" -/\ ... \I 1\6 II \"."",.1 • l1li 1\/1... ..... II '/. " I r -. , • \/ ~ t .. \ • \* f~ 'W\ * " ... v .... ~ ~ C\I ('t) ~ L!) (0 '" CD 0) 0 ~ C\I ('t) ~ CD CD CD CD CD CD CD CD CD 0) 0) 0) 0) 0) 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) BHV-2 Uranium-Natural Concentrations (uCi/ml) ~ '. .... ... --... n 1\ 1\ /\.. J I I ~ ~~ ~ t' 1 ~ .... ,/ ~WV l.A~~ ~ ¥ L!) (0 '" CD 0) 0 ~ C\I ('t) ~ L!) (0 '" CD 0) 0 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) (j) tn c: o "~ cu :... ... c: (1) () c: o (J o ('I) N I E :::s ";: o .c l- N :> l: m C\I T'""" T'""" W W 0 0 ~ ~ ~~ 1--~ 4 Ct) .;:t L.{) T'""" T'""" T'""" W W W 0 0 0 ~ o 0 ~ere~s oOlf ~~r ~ ~-des ~~~ ~~ o~-des ,..~ ~p. I ~ • 60-deS BO-deS LO-deS ~ ~ 90-deS ~ ~< so-des va-des so-des ~ ~o-des ~o-des oo-des I~ ~ ~ 66-deS .::;: .. -=: r--~ ~ ~ t::::::.. B6-deS L6-de S 96-deS r-.~~ r-~ ~ ~ ..... S6-deS v6-deS ~ ~ S6-deS r-.N~ ... ~ ~6-des --~~ 11..= ~6-des ,~~ .... .-~~ -I-~ ... ~ 1--....... 06-deS 6B-deS BB-deS == ... ~ ~ j 1-1-t:::= ~ LB-deS 9B-deS SB-des vB-des l-I--~ 14 ~ ~ ~~. ~ SB-des ~B-des r-. ~B-des {O "-<X> T'""" T'""" T'""" W W W 0 0 0 ~ ~ ~ 1.00E-1 1 1.00E-12 1.00E-13 Q) (ij (,) Ul.OOE-14 0) o 2- 1.00E-1S 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml BHV-2 Radium-226 Concentrations (uCi/ml) Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml t " , , \I .. \ • .A. • \ 1\ , .., tJ '1 JI • ~ T \ J 1.t1V~ '\1 \I • T"'" ~ ~ ~ ~ ~ ~ 00 m 00 00 00 00 00 00 00 00 00 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) (J) (J) (J) (J) (J) (J) (J) (J) (J) \ • \ , .. 1'T ... . \ l' 1\ 1\1 f\ jJ~J ¥ t 1\ I .. \ 1\1 ~ ~ \ .... ~ 4t "I ¥ • o T"'" m m 6. 6. Q) Q) (J) (J) ~ (t) ~ m m m 6. 6. 6. Q) Q) Q) (J) (J) (J) ~ m I Q. Q) (J) ~ m 6. Q) (J) 4 ~ ... + lit A...... III ~ m '"' 6. Q) (J) 00 m 6. Q) (J) m m 6. Q) (J) o o 6. Q) (J) T"'" o 6. Q) (J) ~ o 6. Q) (J) ~ o 6. Q) (J) ~ o 6. Q) (J) .. 11 1\ i\ ~ o 6. Q) (J) ~ o 6. Q) (J) ~ o 6. Q) (J) A .... ..... .. '''''If " 00 o 6. Q) (J) \I • m o 6. Q) (J) o T"'" 6. Q) (J) , HI V .. T"'" T"'" 6. Q) (J) tn c: o ; as '-... c: CI) u c: o (.) o ~ N I "C as CI) ...J N :> ::I: III 'r" uJ 0 ~ -,... C\J Ct) 'r" 'r" I uJ w 0 0 ~ ~ ~ ~ ~-des t. ~ ... ~ ~ • ~- o~-des 60-deS 80-des ~ ~ LO-deS 90-deS ~F:: ............... -... so-des ~ --b,jj vO-deS .-=:: ~. 80-deS :=~ Go-des ---~ ~o-des ;. OO-deS 66-deS • t~ ~ +: .- ~ 86-deS L6-deS 96-deS ~ ..I .~~~ S6-deS t-~~ ....... v6-deS ~ 1« ~ I ~ ~ I. f:::::: ~ ~ ~ ;::: 1«: ~ 86-deS G6-deS ~6-des 06-deS 68-deS 4 fi. ~~ t: ~ ~ ~ 00::::;:: 88-deS L8-deS -, 98-deS • ... ~ ~ ~ t • :::::: ---. ~::: .-J~ l S8-des v8-des 88-des G8-deS ~8-des ~ LO <0 I'-- 'r" 'r" 'r" 'r" uJ uJ uJ uJ 0 0 0 0 ~ ~ 0 ~ (el1305001) TAB 3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE Date IEffluent Concentration limit = 9E-14 uCi/ml BHV-3U Effluent Concentration limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit :: 9E~13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB j~lARA Goal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml AlARA Goal = 2.2SE-:L3 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Conc EFC EFCA 9/28/1981 :L.74E-IS S.00E-12 L2SE-12 9.02E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-:l2 S.OOE-13 I.S4E-J.4 4.00E-12 LOOE-12 12/14/1981 1.59E-IS S.OOE-12 L2SE-12 S.03E-16 8.00E-14 2.00E-14 l.30E-16 2.00E-:L2 S.OOE-13 2.2SE-J.4 4.00E-12 LOOE-12 3/29/1982 3.76E-16 S.00E-12 L2SE-12 S.2SE-16 8.00E-14 2.00E-14 4.08E-16 2.00E-:L2 S.OOE-13 1.96E-J.4 4.00E-12 1.00E-12 6/30/1982 :l.83E-16 S.00E-12 1.2SE-12 2.16E-16 8.00E-14 2.00E-14 L41E-IS 2.00E-:L2 S.OOE-13 2.40E-14 4.00E-12 1.00E-12 9/27/1982 S.9SE-16 S.OOE-12 L2SE-12 L44E-IS 8.00E-14 2.00E-14 S.36E-16 2.00E-12 S.OOE-13 1.43E-J.4 4.00E-12 LOOE-12 1/3/1983 2.0SE-16 S.00E-12 L2SE-12 1.23E-16 8.00E-14 2.00E-14 l.10E-16 2.00E-:L2 S.OOE-13 3.01E-14 4.00E-12 LOOE-12 4/4/1983 :l.00E-16 S.00E-12 L2SE-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 S.OOE-13 L39E-14 4.00E-12 LOOE-12 6/30/1983 :l.06E-16 S.00E-12 L2SE-12 9.S9E-17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 S.OOE-13 1.70E-14 4.00E-12 LOOE-12 10/3/1983 :l.91E-16 S.00E-12 1.2SE-12 3.0SE-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 S.OOE-13 1.76E-14 4.00E-12 LOOE-12 1/3/1984 :l.0IE-16 S.00E-12 L2SE-12 9.S1E-17 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 9.17E-1S 4.00E-12 LOOE-12 4/2/1984 8.22E-16 S.00E-12 L2SE-12 7.S2E-16 8.00E-14 2.00E-14 S.20E-17 2.00E-12 S.00E-13 3.47E-14 4.00E-12 1.00E-12 7/2/1984 S.29E-16 S.OOE-12 L2SE-12 6.18E-16 8.00E-14 2.00E-14 L40E-16 2.00E-12 S.OOE-13 L32E-14 4.00E-12 LOOE-12 10/1/1984 :L.74E-16 S.00E-12 1.2SE-12 7.lOE-17 8.00E-14 2.00E-14 LOOE-16 2.00E-1.2 S.OOE-13 1.08E-14 4.00E-12 LOOE-12 1/2/1985 :l.OOE-17 S.OOE-12 L2SE-12 7.10E-17 8.00E-14 2.00E-14 7.80E-17 2.00E-12 S.OOE-13 2.73E-14 4.00E-12 LOOE-12 4/1/1985 :L.00E-16 S.00E-12 L2SE-12 2.76E-16 8.00E-14 2.00E-14 4.10E-17 ~:2 S.OOE-13 1.12E-l4 4.00E-12 LOOE-12 7/1/1985 :L.04E-16 S.00E-12 L2SE-12 1.00E-16 8.00E-14 2.00E-14 LOOE-16 2.00E-J.2 S.OOE-13 L64E-l4 4.00E-12 LOOE-12 9/30/1985 :L.00E-16 S.00E-12 L2SE-12 LOOE-IS 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 L73E-14 4.00E-12 LOOE-12 1/2/1986 1.03E-IS S.00E-12 1.2SE-12 3.17E-16 8.00E-14 2.00E-14 1.2SE-16 2.00E-12 S.OOE-13 L21E-17 4.00E-:L2 LOOE-12 4/1/1986 8.04E-16 S.00E-12 L2SE-12 L93E-17 8.00E-14 2.00E-14 I.S4E-16 2.00E-12 S.OOE-13 L69E-l4 4.00E-12 1.00E-12 6/30/1986 4.29E-16 S.00E-12 L2SE-12 L77E-16 8.00E-14 2.00E-14 2.83E-16 2.00E-J.2 S.OOE-13 L97E-14 4.00E-12 LOOE-12 10/27/1986 6.4SE-16 S.00E-12 1.2SE-12 9.89E-17 8.00E-14 2.00E-14 4.16E-IS 2.00E-12 S.OOE-13 1.64E-14 4.00E-:l2 LOOE-12 12/15/1986 1.31E-16 S.00E-12 L2SE-12 O.OOE+OO 8.00E-14 2.00E-14 4.16E-17 2.00E-12 S.OOE-13 4.60E-IS 4.00E-:L2 LOOE-12 3/16/1987 2.0lE-16 S.00E-12 L2SE-12 1.20E-16 8.00E-14 2.00E-14 S.73E-17 2.00E-12 S.OOE-13 L60E-l4 4.00E-12 1.00E-12 5/11/1987 2.16E-16 S.00E-12 1.2SE-12 L96E-16 8.00E-14 2.00E-14 7.38E-17 2.00E-12 S.OOE-13 I.S9E-14 4.00E-12 1.00E-12 9/9/1987 2.4lE-16 S.OOE-12 1.2SE-12 2.18E-16 8.00E-14 2.00E-14 3.S2E-17 2.00E-12 S.OOE-13 L46E-14 4.00E-12 LOOE-12 11/2/1987 2.44E-16 S.00E-12 L2SE-12 2.32E-16 8.00E-14 2.00E-14 2.37E-17 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 2/16/1988 B.08E-16 S.OOE-12 L2SE-12 2.SSE-16 8.00E-14 2.00E-14 3.42E-16 2.00E-J.2 S.OOE-13 S.61E-14 4.00E-12 LOOE-12 5/18/1988 1.14E-16 S.OOE-12 L2SE-12 4.14E-17 8.00E-14 2.00E-14 LOOE-16 2.00E-J.2 S.OOE-13 L20E-14 4.00E-12 LOOE-12 8/15/1988 2.08E-16 S.00E-12 L2SE-12 3.06E-16 8.00E-14 2.00E-14 3.6SE-17 2.00E-12 S.OOE-13 1.36E-14 4.00E-12 LOOE-12 11/14/1988 4.21E-16 S.00E-12 1.2SE-12 2.93E-16 8.00E-14 2.00E-14 L09E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 LOOE-12 2/13/1989 4.4SE-16 S.00E-12 L2SE-12 4.78E-17 8.00E-14 2.00E-14 2.47E-17 2.00E-12 S.OOE-13 3.34E-14 4.00E-12 LOOE-12 5/15/1989 l.OSE-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 2.4SE-17 2.00E-J.2 S.OOE-13 6.S6E-1S 4.00E-12 LOOE-12 8/14/1989 1..31E-16 S.OOE-12 l.2SE-12 S.8SE-17 8.00E-14 2.00E-14 3.97E-17 2.00E-12 S.OOE-13 6.7SE-IS 4.00E-12 l.00E-12 11/13/1989 1.67E-16 S.00E-12 1.2SE-12 3.87E-17 8.00E-14 2.00E-14 8.03E-17 2.00E-12 S.OOE-13 l.69E-14 4.00E-12 l.OOE-12 2/12/1990 4.43E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 3.S0E-17 2.00E-12 S.OOE-13 2.37E-14 4.00E-12 l.OOE-12 5/14/1990 3.84E-16 S.00E-12 1.2SE-12 2.S4E-16 8.00E-14 2.00E-14 l.02E-16 2.00E-12 S.OOE-13 l.68E-14 4.00E-12 LOOE-12 8/13/1990 7.27E-17 S.00E-12 1.2SE-12 2.87E-16 8.00E-14 2.00E-14 l.21E-17 2.00E-12 S.OOE-13 7.86E-IS 4.00E-12 l.00E-12 11/12/1990 1..84E-16 S.00E-12 l.2SE-12 l.34E-16 8.00E-14 2.00E-14 8.S3E-17 2.00E-12 S.OOE-13 2.01E-14 4.00E-12 LOOE-12 2/11/1991 4.66E-17 S.00E-12 L2SE-12 8.48E-16 8.00E-14 2.00E-14 L94E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 LOOE-12 5/13/1991 S.OSE-17 S.00E-12 L2SE-12 7.40E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 LSOE-14 4.00E-12 LOOE-12 8/12/1991 7.14E-17 S.00E-12 L2SE-12 6.22E-17 8.00E-14 2.00E-14 7.9SE-17 2.00E-12 S.OOE-13 L77E-14 4.00E-12 LOOE-12 11/11/1991 1.41E-17 S.00E-12 L2SE-12 2.19E-18 8.00E-14 2.00E-14 2.7SE-17 2.00E-12 S.OOE-13 L18E-14 4.00E-12 LOOE-12 2/10/1992 8.12E-17 S.OOE-12 1.2SE-12 2.3SE-17 8.00E-14 2.00E-14 2.76E-18 2.00E-12 S.OOE-13 3.S7E-14 4.00E-12 LOOE-12 5/11/1992 9.18E-17 S.00E-12 L2SE-12 S.80E-17 8.00E-14 2.00E-14 3.36E-17 2.00E-12 S.OOE-13 L28E-14 4.00E-12 1.00E-12 8/10/1992 l.00E-18 S.00E-12 L2SE-12 4.19E-17 8.00E-14 2.00E-14 2.00E-18 2.00E-12 S.OOE-13 LS9E-14 4.00E-12 LOOE-12 11/9/1992 4.00E-17 S.00E-12 L2SE-12 2.68E-17 8.00E-14 2.00E-14 L07E-17 2.00E-12 S.OOE-13 L8lE-14 4.00E-12 LOOE-12 2/9/1993 7.94E-17 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 L09E-16 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 LOOE-12 5/10/1993 l.60E-17 S.00E-12 L2SE-12 S.07E-17 8.00E-14 2.00E-14 7.64E-17 2.00E-12 S.OOE-13 l.26E-14 4.00E-12 LOOE-12 8/10/1993 c..OOE-17 S.00E-12 L2SE-12 6.00E-18 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 LSOE-14 4.00E-12 LOOE-12 11/8/1993 l.00E-16 S.00E-12 1.2SE-12 l.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 , S.OOE-13 2.lOE-14 4.00E-12 LOOE-12 2/7/1994 l.6lE-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 S.OOE-13 2.23E-14 4.00E-12 LOOE-12 5/9/1994 2.77E-16 S.00E-12 1.2SE-12 2.80E-17 8.00E-14 2.00E-14 8.37E-18 2.00E-12 S.OOE-13 L40E-14 4.00E-12 LOOE-12 8/9/1994 7.39E-17 S.00E-12 1.2SE-12 LOOE-16 8.00E-14 2.00E-14 l.14E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 1.00E-12 11/7/1994 9.OSE-17 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 1.00E-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = SE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 7.99E-17 9.00E-14 2.2SE-14 9.60E-17 2.00E-14 s.OOE-ls 9.60E-17 9.00E-13 2.2sE-13 9.0sE-ls 6.00E-13 l.s0E-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 9.80E-17 2.00E-14 s.OOE-ls 8.60E-17 9.00E-13 2.2sE-13 2.88E-ls 6.00E-13 1.s0E-13 8/9/1995 7.30E-17 9.00E-14 2.2sE-14 9.20E-17 2.00E-14 s.OOE-ls 4.40E-17 9.00E-13 2.2SE-13 1.96E-ls 6.00E-13 1.s0E-13 11/11/1995 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-IS 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.S0E-13 2/5/1996 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 S.OOE-IS 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 5/6/1996 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.S3E-14 6.00E-13 1.S0E-13 8/5/1996 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 s.OOE-IS 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 11/6/1996 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 2/6/1997 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 5/5/1997 1.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.S3E-14 6.00E-13 1.S0E-13 8/11/1997 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2SE-13 1.31E-14 6.00E-13 1.s0E-13 1/5/1998 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 S.OOE-ls 6.S8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 I.S0E-13 4/28/1998 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 1.s0E-13 7/31/1998 1.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.OOE-IS 1.82E-16 9.00E-13 2.2sE-13 1.S3E-14 6.00E-13 1.S0E-13 9/28/1998 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.S0E-13 12/28/1998 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-IS 6.S8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 1.S0E-13 3/29/1999 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-IS 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.s0E-13 7/3/1999 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 S.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 1.S0E-13 9/27/1999 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 S.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 12/28/1999 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-IS 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 3/28/2000 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 I.S0E-13 6/26/2000 1.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.S3E-14 6.00E-13 1.s0E-13 9/26/2000 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3~99E-16 9.00E-13 2.2SE-13 1.31E-14 6.00E-13 1.s0E-13 12/26/2000 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 1.S0E-13 3/26/2001 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 7/2/2001 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 1.s0E-13 9/24/2001 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.S0E-13 12/31/2001 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.S8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.S0E-13 4/1/2002 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 S.OOE-IS 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 7/1/2002 1.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.S3E-14 6.00E-13 1.s0E-13 9/30/2002 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 12/30/2002 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 S.00E-1s 6.S8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 3/31/2003 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-IS 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 1.s0E-13 6/30/2003 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2SE-13 l.s3E-14 6.00E-13 l.s0E-13 9/29/2003 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00Ec13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 12/29/2003 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 3/29/2004 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 6/27/2004 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2SE-13 l.s3E-14 6.00E-13 1.S0E-13 9/27/2004 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 12/27/2004 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 s.OOE-IS 6.sSE-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 3/28/2005 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 6/29/2005 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 1.s0E-13 9/26/2005 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 S.00E-1s 3.99E-16 9.00E-13 2.2SE-13 1.31E-14 6.00E-13 1.S0E-13 1/3/2006 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6;00E-13 1.s0E-13 4/3/2006 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 7/3/2006 1.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1s 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 l .s0E-13 10/2/2006 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 1/1/2006 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-lS 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 l .s0E-13 4/2/2007 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 7/2/2007 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 1.s0E-13 9/30/2007 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 12/31/2007 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 3/31/2008 3.41E-16 9.00E-14' 2.2sE-14 2.26E-16 2.00E-14 s.OOE-IS 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 6/30/2008 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.S3E-14 6.00E-13 l.s0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARA Goal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 L31E-14 6.00E-13 LSOE-13 12/31/2008 3.16E-16 9.00E-14 2.2SE-14 L31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 L91E-14 6.00E-13 LSOE-13 3/1S/2009 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14-S.00E-1S L18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 LSOE-13 6/1S/2009 L31E-16 9.00E-14 2.2SE-14 l.39E-16 2.00E-14 S.00E-1S L82E-16 9.00E-13 2.2SE-13 LS3E-14 6.00E-13 1.S0E-13 9/1S/2009 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 L31E-14 6.00E-13 LSOE-13 12/1S/2009 3.16E-16 9.00E-14 2.2SE-14 L31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 L91E-14 6.00E-13 LSOE-13 3/31/2010 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S L18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 LSOE-13 6/30/2010 L31E-16 9.00E-14 2.2SE-14 L39E-16 2.00E-14 S.00E-1S L82E-16 9.00E-13 2.2SE-13 LS3E-14 6.00E-13 LSOE-13 9/30/2010 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 L31E-14 6.00E-13 1.S0E-13 12/31/2010 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 LSOE-13 4/4/2011 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S L18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 LSOE-13 7/4/2011 1.31E-16 9.00E-14 2.2SE-14 L39E-16 2.00E-14 S.00E-1S L82E-16 9.00E-13 2.2SE-13 LS3E-14 6.00E-13 LSOE-13 10/3/2011 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 L31E-14 6.00E-13 LSOE-13 1/3/2012 3.16E-16 9.00E-14 2.2SE-14 L31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 L91E-14 6.00E-13 1.S0E-13 --'------ -E :::: U ::l --tJ) t: o :;:; co 10.. ... t: CI) (.) t: o U CI) :2 (.) ::l t: o "C co a: ('t) > :x:: m .1== C\I ('I) T""" T""" uJ uJ 0 0 q q T""" ~ ~ ~ -=:: ~ -=:: -=:: -=:: -=:: -=:: -=:: ~ -=:: -:::: tc:; ~ 1 ~ ~ F:: ~ F; « I. ~ r-..... ~ 1+ ::::::: ~ K ~ • ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ .... :-i-- ~ ,- ~ ~ ~ > ~ t ~ 1- ~ T ~ ~ ~ ~ :::::. ~ ..... """ T""" uJ 0 q .... NllEiiii; ~ l1 ..... NllIIii:ii;; ~ 11--' _1Iii::: ~ l' ..... ---,. NllIiiii; ~ 1'--' _E::: ~ ~~ ~ "'" ~ 11 -. _II:: .... ~ 1'-' _EO::: l,-' ~ _E:: ... ~ I'" -Iiiiiji ~ 1'-' _.::: -~ ,-. _s;;: ---, .. ~ ,. "II!!:::: -~ ,-. ~J ~ -. ,. ~ ::::::;;.- ~ I' -. _IllS::: ~ ~-des o ~-des 60-deS 80-deS LO-deS 90-deS 90-deS Po-des 0 80-deS T""" C\I -6 Go-des co Q) .....J ~o-des t OO-deS <.0 C\I 66-deS C\I E 86-deS ::J :a co L6-deS a: t 96-deS .. ,~ F-::;t-• P ~ ;...~. -:::;;;z ~ 96-deS 0 ('I) C\I P6-deS E ::J "C ... ~ 86-deS 0 ..c I- A"" -I-A. G6-deS t ~. ...--~6-des (ij ~ -~ '"" .t ~ ~ ~. I-~l ~, t:t 1; ~ !;; • ::=. 06-deS ::J m z 68-deS E ::J 88-deS "c ~ -~ " .... .... + --.. ~ c;~ .... ~ :::::> L8-des t 98-des ... ~- 98-deS ~ ::::.... .,.", ~ '::::~ I ~~ !!£:::aiII ~ II1II +c: I f:~ P8-deS 88-deS G8-deS ;--~~ -::::::.. --' ~8-des L.{) <.0 r--.. 00 T""" T""" T""" T""" uJ uJ uJ uJ 0 q 0 0 0 q q q (elBos 001) 1.00E-11 1.00E-12 1.00E-13 ---l.OOE-14 Q) (ij () if) 0) o --.J '1'.OOE-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml -. ~ .... , ]II" A , / " l.J\ I , • I ..... ..... \ ..... .J.. \ , , f \ I~ l... TV \ , ~ 1.. \ 1 \ 'J ... ~~ .J. J{ 'i V \~ .... ~ \ \ ~ T""" C\J ('I) "'¢ L() <.0 ,...... co (j) 0 T""" co co co co co co co co co (j) (j) 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) if) (J) if) if) if) if) if) if) (J) if) if) BHV-3 Uranium-Natural Concentrations (uCi/ml) .......... ~ ............................ ~ ........................... 1f /\T \T \T \T \T \T \T \T \T \T \T \T \T \T \T \T /\ I ~ ~ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ~ ~ ¥ ¥ V ¥ ¥ I , tl • C\J ('I) "'¢ L() <.0 ,...... co (j) 0 T""" C\J ('I) "'¢ L() <.0 ,...... co (j) 0 (j) (j) (j) (j) (j) (j) (j) (j) 0 0 0 0 0 0 0 0 0 0 T""" T""" 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (J) if) if) if) if) if) if) (J) (J) if) (J) if) if) (J) (J) if) if) if) if) if) rn t: o "+=i CO Jo.. .... t: CI) (,) t: o o o M N I E :::l "i: o .c: I- M :> ::I: m \ C\J T""" T""" ill ill 0 0 ~ ~ "" --~ 4 6oc: Ct) -q-L() T""" T""" T""" ill ill ill 0 0 0 ~ o 0 ~eIB~S DOlf .f::::: ! .p. .F:p:. .p. .F::p. .~ .f:::::p. .~p:. ~p. ._p. .~~ .t;:=. .:::::::t::::. .~ .:::::::p. .~p. .~ .:::::::~ .~::::. .5: .:::::::~ .~~ I.:> r-p. I.~p:. .~ ~ ~-des o ~-des 60-deS so-des LO-deS 90-deS so-des vO-deS 80-des Go-des ~o-des OO-deS 66-deS S6-deS L6-deS 96-deS S6-deS ~ ~ r-F='~ ~ v6-deS 86-deS ~ ~~. G6-deS r-r-..... ~6-des -r--p. ~ ~ r-p~ ~ ~ ~t: ~ ~~ 06-deS 6S-deS ss-des , r- ~ ~ LS-deS 9S-deS oc: ~ ss-des vs-des --~K ~ ---.... 8S-deS ... :::04 ,.::: Gs-deS ~ ~s-des <.0 f'-.. co T""" T""" T""" ill ill ill 0 0 0 ~ ~ ~ ~F--. ~ ~ ~-des ~F=-. ~ o~-des ::- E --.... (3 ::l - -I ~~ r::::: ~ ~::::.. ~ ~ ~ ~ iO::::: .,.., ~ ~ 60-deS BO-deS La-des 90-deS tn C 0 "';; CO J... ... C C1) () c 0 0 CD C\I \. C\I I E ::l ~::::.. ~ ~:::::. ~ ~~ ~ ~::::. ~ ~::::., ~ ~:::::: ~ ~::::., ~ so-des va-des 80-deS ~o-des ~o-des oo-des 66-deS " CO a: C"') :> J: m -.-=-~ I ~~ r:::: --~ ~r--... ~ III B6-deS L6-deS 96-deS S6-deS "",,-""~~ ..1 ~ v6-deS "R ~ 86-deS • t:=!!:0.0.1 ~6-des ~ 1-'-..-~6-des 1-'-..-4 ~ ~ 06-deS ~ ~. r..~ l • 1-'- ~. I.c:::::: ~ 6B-deS BB-deS 1'. ;:19' LB-deS ~ ~ ~ 9B-deS SB-deS ~ vB-des ~ ~ "---8B-deS ....... +== • "'''4 ~-:::. ..... ~B-des ~B-des T""" C\I Ct) ..q L{) CO l"-co T""" T""" T""" T""" T""" T""" T""" T""" uJ uJ uJ uJ uJ uJ uJ uJ 0 0 0 0 0 0 0 q q q o 0 q q ~ele::>s BOlf 0 q E ....... (3 :::J -In r:::: o .~ ca ~ ... r:::: CD o r:::: o (.) o ,.... N I -C ca CD ...J ('I) ::> J: m T""" uJ 0 ~ -- ,:::: C\J C') T""" T""" uJ uJ 0 0 ~ ~ ~ L:ji ~ ~ ~ -::: ~ .:::; ~ -::: ~ .:::; ~ .:::; ~ -::: ~ .:::; ~ .:::; ~ -::: ~ tr::: ~ tr::: > t( t> -::: ~ ~ .... 1-- 1 ~ ~ -::: ~ +::::::: ~ ~::::; > « ~ !.~ ~ -... 1-~ ,. ( '"' ~ to:::: 5. .:::::::-~ 0=:::: ;: ~ ~ ~ • .... ~ T""" uJ 0 0 (eIB~S 001) ~ L{) <.0 T""" T""" uJ uJ 0 0 ~ ~ ... T I'-- T""" uJ 0 ~ ~ ~-des o~-des 60-deS 80-deS La-des 90-deS so-des 170-deS 80-deS co-des ~o-des OO-deS 66-deS 86-deS L6-deS 96-deS S6-deS 176-deS 86-deS c6-deS ~6-des 06-deS 68-deS 88-deS L8-deS 98-deS S8-deS 178-deS 88-deS c8-deS ~8-des TAB 4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 S.20E-IS S.OOE-12 l.2SE-12 2.93E-IS 8.00E-14 2.00E-14 2.74E-IS 2.00E-12 S.OOE-13 l.84E-14 4.00E-12 1.00E-12 12/14/1981 4.S3E-IS S.OOE-12 l.2SE-12 l.78E-IS 8.00E-14 2.00E-14 2.29E-IS 2.00E-12 S.OOE-13 2.S4E-14 4.00E-12 l.OOE-12 3/29/1982 l.06E-IS S.00E-12 l.2SE-12 l.42E-14 8.00E-14 2.00E-14 l.07E-IS 2.00E-12 S.OOE-13 2.31E-14 4.00E-12 l.OOE-12 6/30/1982 6.03E-IS S.00E-12 l.2SE-12 l.S7E-14 8.00E-14 2.00E-14 2.62E-IS 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 l.OOE-12 9/27/1982 l.26E-14 S.OOE-12 l.2SE-12 7.S8E-16 8.00E-14 2.00E-14 S.3SE-IS 2.00E-12 S.OOE-13 2.68E-14 4.00E-12 l.OOE-12 1/3/1983 4.33E-IS S.00E-12 l.2SE-12 6.S2E-16 8100E-14 2.00E-14 6.04E-16 2.00E-12 S.OOE-13 2.S7E-14 4.00E-12 l.OOE-12 4/4/1983 l.2SE-IS S.00E-12 l.2SE-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 l.OOE-12 6/30/1983 3.73E-16 S.OOE-12 l.2SE-12 9.43E-16 8.00E-14 2.00E-14 4.13E-16 2.00E-12 S.OOE-13 1.20E-14 4.00E-12 l.OOE-12 10/3/1983 2.S4E-16 S.00E-12 l.2SE-12 l.SIE-16 8.00E-14 2.00E-14 2.6SE-16 2.00E-12 S.OOE-13 2.S0E-14 4.00E-12 l.OOE-12 1/3/1984 2.76E-IS S.00E-12 l.2SE-12 l.60E-16 8.00E-14 2.00E-14 l.OSE-16 2.00E-12 S.OOE-13 l.S9E-16 4.00E-12 l.00E-12 4/2/1984 4.27E-16 S.00E-12 l.2SE-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 2.00E-12 S.OOE-13 3.67E-14 4.00E-12 l.OOE-12 7/2/1984 2.S7E-IS S.00E-12 l.2SE-12 l.36E-16 8.00E-14 2.00E-14-l.l1E-16 2.00E-12 S.OOE-13 l.S8E-14 4.00E-12 l.OOE-12 10/1/1984 4.18E-16 S.00E-12 l.2SE-12 3.S4E-16 8.00E-14 2.00E-14 l.10E-17 2.00E-12 S.OOE-13 9.83E-IS 4.00E-12 l.OOE-12 1/2/1985 S.30E-17 S.00E-12 l.2SE-12 3.SSE-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 2.S7E-14 4.00E-12 1.00E-12 4/1/1985 l.00E-16 S.00E-12 l.2SE-12 6.00E-16 8.00E-14 2.00E-14 4.3SE-17 2.00E-12 S.OOE-13 S.02E-IS 4.00E-12 l.OOE-12 7/1/1985 9.36E-16 S.00E-12 l.2SE-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 2.00E-12 S.OOE-13 7.48E-IS 4.00E-12 l.OOE-12 9/30/1985 l.46E-IS S.00E-12 l.2SE-12 7.69E-16 8.00E-14 2.00E-14 S.38E-16 2.00E-12 S.OOE-13 7.86E-IS 4.00E-12 l.OOE-12 1/2/1986 8.40E-IS S.OOE-12 l.2SE-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 1.00E-12 4/1/1986 S.79E-IS S.00E-12 l.2SE-12 S.80E-16 8.00E-14 2.00E-14 l.34E-IS 2.00E-12 S.OOE-13 l.33E-14 4.00E-12 l.OOE-12 6/30/1986 S.19E-IS S.00E-12 l.2SE-12 7.83E-16 8.00E-14 2.00E-14 2.20E-IS 2.00E-12 S.OOE-13 7.14E-16 4.00E-12 1.00E-12 10/27/1986 4.60E-IS S.00E-12 l.2SE-12 4.67E-16 8.00E-14 2.00E-14 2.37E-IS 2.00E-12 S.OOE-13 l.13E-14 4.00E-12 l.OOE-12 12/15/1986 2.7SE-IS S.00E-12 l.2SE-12 S.90E-16 8.00E-14 2.00E-14 9.39E-16 2.00E-12 S.OOE-13 l.20E-14 4.00E-12 l.OOE-12 3/16/1987 4.64E-IS S.00E-12 l.2SE-12 l.18E-IS 8.00E-14 2.00E-14 4.97E-16 2.00E-12 S.OOE-13 S.89E-14 4.00E-12 l.OOE-12 5/11/1987 4.3SE-1S S.00E-12 l.2SE-12 l.23E-14 8.00E-14 2.00E-14 l.13E-1S 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 l.00E-12 9/9/1987 6.39E-IS S.00E-12 l.2SE-12 l.SOE-14 8.00E-14 2.00E-14 2.26E-1S 2.00E-12 S.OOE-13 l.S7E-14 4.00E-12 l.OOE-12 11/2/1987 6.72E-IS S.00E-12 l.2SE-12 4.S3E-16 8.00E-14 2.00E-14 2.20E-1S 2.00E-12 S.OOE-13 2.SSE-14 4.00E-12 l.OOE-12 2/16/1988 l.91E-IS S.00E-12 l.2SE-12 l.3SE-14 8.00E-14 2.00E-14 4.42E-16 2.00E-12 S.OOE-13 4.44E-14 4.00E-12 l.OOE-12 5/18/1988 l.78E-14 S.00E-12 l.2SE-12 4.39E-14 8.00E-14 2.00E-14 4.92E-16 2.00E-12 S.OOE-13 l.38E-14 4.00E-12 l.OOE-12 8/15/1988 7.S6E-IS S.00E-12 l.2SE-12 3.31E-14 8.00E-14 2.00E-14 l.SIE-1S 2.00E-12 S.OOE-13 l.97E-14 4.00E-12 l.OOE-12 11/14/1988 1.47E-14 S.00E-12 l.2SE-12 l.S6E-1S 8.00E-14 2.00E-14 2.S7E-1S 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 1.00E-12 2/13/1989 2.47E-1S S.00E-12 l.2SE-12 3.14E-1S 8.00E-14 2.00E-14 6.94E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.00E-12 5/15/1989 2.S0E-16 S.00E-12 l.2SE-12 7.68E-IS 8.00E-14 2.00E-14 9.03E-16 2.00E-12 S.OOE-13 8.0SE-IS 4.00E-12 l.00E-12 8/14/1989 6.S0E-IS S.00E-12 1.2SE-12 4.72E-1S 8.00E-14 2.00E-14 2.3SE-IS 2.00E-12 S.OOE-13 9.9SE-1S 4.00E-12 l.OOE-12 11/13/1989 9.63E-IS S.00E-12 1.2SE-12 4.0SE-1S 8.00E-14 2.00E-14 4.03E-IS 2.00E-12 S.OOE-13 l.99E-14 4.00E-12 l.OOE-12 2/12/1990 8.92E-1S S.00E-12 l.2SE-12 3.S6E-IS 8.00E-14 2.00E-14 2.89E-1S 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 l.OOE-12 5/14/1990 8.90E-IS S.00E-12 l.2SE-12 3.S8E-IS 8.00E-14 2.00E-14 2.33E-1S 2.00E-12 S.OOE-13 2.09E-14 4.00E-12 l.OOE-12 8/13/1990 1.92E-IS S.00E-12 l.2SE-12 l.87E-IS 8.00E-14 2.00E-14 S.06E-16 2.00E-12 S.OOE-13 8.86E-IS 4.00E-12 l.OOE-12 11/12/1990 2.91E-1S S.00E-12 l.2SE-12 2.2SE-17 8.00E-14 2.00E-14 l.08E-1S 2.00E-12 S.OOE-13 2.19E-14 4.00E-12 l.OOE-12 2/11/1991 l.67E-16 S.00E-12 l.2SE-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 S.OOE-13 4.19E-14 4.00E-12 1.00E-12 5/13/1991 l.87E-16 S.00E-12 l.2SE-12 2.61E-IS 8.00E-14 2.00E-14 3.S4E-16 2.00E-12 S.OOE-13 l.40E-14 4.00E-12 l.OOE-12 8/12/1991 4.8SE-16 S.00E-12 l.2SE-12 4.38E-16 8.00E-14 2.00E-14 l.27E-16 2.00E-12 S.OOE-13 2.20E-14 4.00E-12 1.00E-12 11/11/1991 l.77E-16 S.00E-12 l.2SE-12 1.46E-16 8.00E-14 2.00E-14 3.76E-17 2.00E-12 S.OOE-13 1.1SE-14 4.00E-12 l.OOE-12 2/10/1992 l.83E-16 S.00E-12 l.2SE-12 l.9SE-IS 8.00E-14 2.00E-14 l.33E-16 2.00E-12 S.OOE-13 3.3SE-14 4.00E-12 l.OOE-12 5/11/1992 4.40E-16 S.00E-12 l.2SE-12 2.S6E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.00E-12 8/10/1992 9.09E-17 S.00E-12 l.2SE-12 1.1SE-16 8.00E-14 2.00E-14 4.S0E-17 2.00E-12 S.OOE-13 1.S7E-14 4.00E-12 l.00E-12 11/9/1992 2.07E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 3.62E-17 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 1.00E-12 2/9/1993 l.73E-16 S.00E-12 l.2SE-12 2.76E-17 8.00E-14 2.00E-14 2.89E-17 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 5/10/1993 2.70E-17 S.00E-12 1.2SE-12 2.S0E-17 8.00E-14 2.00E-14 8.74E-17 2.00E-12 S.OOE-13 l.2SE-14 4.00E-12 l.OOE-12 8/10/1993 9.00E-17 S.OOE-12 1.2SE-12 l.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 I .S0E-14 4.00E-12 l.OOE-12 11/8/1993 l.00E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 6.00E-17 2.00E-12 S.OOE-13 l.7SE-14 4.00E-12 1.00E-12 2/7/1994 l.10E-16 S.00E-12 l.2SE-12 3.38E-16 8.00E-14 2.00E-14 2.21E-16 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 5/9/1994 3.80E-16 S.00E-12 l.2SE-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 S.OOE-13 l.73E-14 4.00E-12 l.OOE-12 8/9/1994 3.8SE-16 S.00E-12 l.2SE-12 3.S3E-16 8.00E-14 2.00E-14 l.00E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 l.OOE-12 11/7/1994 6.21E-17 S.00E-12 l.2SE-12 9.70E-17 8.00E-14 2.00E-14 l.96E-16 2.00E-12 S.OOE-13 l.OOE-16 4.00E-12 l.OOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 3.70E-16 9.00E-14 2.2SE-14 9.80E-17 2.00E-14 S.00E-1S 9.70E-17 9.00E-13 2.2SE-13 8.84E-1S 6.00E-13 1.S0E-13 5/9/1995 9.40E-17 9.00E-14 2.2SE-14 2.86E-16 2.00E-14 S.00E-1S L90E-16 9.00E-13 2.2SE-13 2.90E-1S 6.00E-13 1.S0E-13 8/9/1995 L4SE-16 9.00E-14 2.2SE-14 2.3lE-1S 2.00E-14 S.00E-1S 7.lDE-17 9.00E-13 2.2SE-13 2.70E-1S 6.00E-13 1.S0E-13 11/11/1995 L43E-14 9.00E-14 2.2SE-14 S.70E-1S 2.00E-14 S.00E-1S 2.61E-1S 9.00E-13 2.2SE-13 S.60E-1S 6.00E-13 LSOE-13 2/5/1996 1.19E-14 9.00E-14 2.2SE-14 3.80E-16 2.00E-14 S.00E-1S 6.10E-1S 9.00E-13 2.2SE-13 6.48E-1S 6.00E-13 LSOE-13 5/6/1996 4.SSE-16 9.00E-14 2.2SE-14 3.S7E-1S 2.00E-14 S.00E-1S 2.84E-16 9.00E-13 2.2SE-13 7.68E-1S 6.00E-13 LSOE-13 8/5/1996 7.78E-16 9.00E-14 2.2SE-14 3.S1E-1S 2.00E-14 S.00E-1S L69E-16 9.00E-13 2.2SE-13 4.90E-1S 6.00E-13 LSOE-13 11/6/1996 L36E-1S 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S 4.2lE-16 9.00E-13 2.2SE-13 1.10E-14 6.00E-13 LSOE-13 2/6/1997 LOOE-16 9.00E-14 2.2SE-14 1.40E-16 2.00E-14 S.00E-1S L03E-16 9.00E-13 2.2SE-13 6.76E-1S 6.00E-13 LSOE-13 5/5/1997 LOOE-16 9.00E-14 2.2SE-14 4.00E-16 2.00E-14 S.00E-1S 2.24E-16 9.00E-13 2.2SE-13 4.SSE-1S 6.00E-13 LSOE-13 8/11/1997 4.74E-16 9.00E-14 2.2SE-14 9.07E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 S.SSE-1S 6.00E-13 LSOE-13 1/5/1998 8.31E-16 9.00E-14 2.2SE-14 4.82E-16 2.00E-14 S.00E-1S L77E-16 9.00E-13 2.2SE-13 S.28E-1S 6.00E-13 LSOE-13 4/28/1998 3.32E-16 9.00E-14 2.2SE-14 4.43E-1S 2.00E-14 S.00E-1S l.21E-16 9.00E-13 2.2SE-13 7.43E-1S 6.00E-13 1.S0E-13 7/31/1998 4.60E-16 9.00E-14 2.2SE-14 9.02E-16 2.00E-14 S.00E-1S 3.S4E-16 9.00E-13 2.2SE-13 6.9lE-1S 6.00E-13 LSOE-13 9/28/1998 4.08E-16 9.00E-14 2.2SE-14 4.93E-16 2.00E-14 S.00E-1S 2.S3E-16 9.00E-13 2.2SE-13 4.S2E-1S 6.00E-13 LSOE-13 12/28/1998 7.72E-16 9.00E-14 2.2SE-14 3.7SE-16 2.00E-14 S.00E-1S 3.43E-16 9.00E-13 2.2SE-13 6.73E-1S 6.00E-13 LSOE-13 3/29/1999 S.l1E-16 9.00E-14 2.2SE-14 4.70E-16 2.00E-14 S.00E-1S 3.70E-16 9.00E-13 2.2SE-13 8.96E-1S 6.00E-13 1.S0E-13 7/3/1999 S.90E-16 9.00E-14 2.2SE-14 9.89E-16 2.00E-14 S.00E-1S l.28E-16 9.00E-13 2.2SE-13 6.40E-1S 6.00E-13 1.S0E-13 9/27/1999 L70E-1S 9.00E-14 2.2SE-14 7.S0E-16 2.00E-14 S.00E-1S 4.61E-16 9.00E-13 2.2SE-13 7.86E-1S 6.00E-13 LSOE-13 12/28/1999 L03E-1S 9.00E-14 2.2SE-14 7.S0E-16 2.00E-14 S.00E-1S 2.43E-16 9.00E-13 2.2SE-13 6.42E-1S 6.00E-13 LSOE-13 3/27/2000 LOOE-16 9.00E-14 2.2SE-14 2.13E-16 2.00E-14 S.00E-1S 2.20E-16 9.00E-13 2.2SE-13 S.61E-1S 6.00E-13 LSOE-13 6/26/2000 L7SE-16 9.00E-14 2.2SE-14 3.08E-16 2.00E-14 S.00E-1S L11E-16 9.00E-13 2.2SE-13 3.92E-1S 6.00E-13 LSOE-13 9/26/2000 3.6SE-16 9.00E-14 2.2SE-14 2.01E-16 2.00E-14 S.00E-1S 2.24E-16 9.00E-13 2.2SE-13 7.79E-1S 6.00E-13 LSOE-13 12/26/2000 2.27E-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S 4.3SE-16 9.00E-13 2.2SE-13 8.4SE-1S 6.00E-13 LSOE-13 3/26/2001 L4SE-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.37E-1S 6.00E-13 1.S0E-13 7/2/2001 LOOE-16 9.00E-14 2.2SE-14 LOSE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.99E-1S 6.00E-13 1.S0E-13 9/24/2001 L9lE-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S 2.01E-16 9.00E-13 2.2SE-13 8.04E-1S 6.00E-13 LSOE-13 12/31/2001 1.38E-16 9.00E-14 2.2SE-14 2.0SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 L83E-1S 6.00E-13 LSOE-13 4/1/2002 2.20E-16 9.00E-14 2.2SE-14 3.38E-16 2.00E-14 S.00E-1S L26E-16 9.00E-13 2.2SE-13 7.48E-1S 6.00E-13 LSOE-13 7/1/2002 L97E-16 9.00E-14 2.2SE-14 4.10E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 7.40E-1S 6.00E-13 LSOE-13 9/30/2002 2.30E-16 9.00E-14 2.2SE-14 2.42E-16 2.00E-14 S.00E-1S LS6E-16 9.00E-13 2.2SE-13 4.21E-1S 6.00E-13 1.S0E-13 12/30/2002 LOOE-16 9.00E-14 2.2SE-14 L92E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 9.42E-1S 6.00E-13 1.S0E-13 3/31/2003 2.S0E-16 9.00E-14 2.2SE-14 L69E-16 2.00E-14 S.00E-1S L29E-16 9.00E-13 2.2SE-13 4.SSE-1S 6.00E-13 1.S0E-13 6/30/2003 LOOE-16 9.00E-14 2.2SE-14 2.87E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 4.20E-1S 6.00E-13 LSOE-13 9/29/2003 LOOE-16 9.00E-14 2.2SE-14 8.S3E-16 2.00E-14 S.00E-1S 3.32E-16 9.00E-13 2.2SE-13 8.69E-1S 6.00E-13 LSOE-13 12/29/2003 1.02E-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S L49E-1S 9.00E-13 2.2SE-13 9.4SE-1S 6.00E-13 LSOE-13 3/29/2004 LOOE-16 9.00E-14 2.2SE-14 L26E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 2.00E-1S 6.00E-13 LSOE-13 6/27/2004 LOOE-16 9.00E-14 2.2SE-14 2.S3E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 3.23E-1S 6.00E-13 LSOE-13 9/27/2004 LOOE-16 9.00E-14 2.2SE-14 L1SE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 9.68E-1S 6.00E-13 LSOE-13 12/27/2004 LOOE-16 9.00E-14 2.2SE-14 2.30E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 1.37E-14 6.00E-13 LSOE-13 3/28/2005 LOOE-16 9.00E-14 2.2SE-14 2.66E-16 2.00E-14 S.00E-1S 3.1SE-16 9.00E-13 2.2SE-13 9.22E-1S 6.00E-13 1.S0E-13 6/29/2005 L47E-16 9.00E-14 2.2SE-14 L4SE-1S 2.00E-14 S.00E-1S 1.42E-16 9.00E-13 2.2SE-13 9.34E-1S 6.00E-13 1.S0E-13 9/26/2005 2.0lE-16 9.00E-14 2.2SE-14 2.06E-16 2.00E-14 S.00E-1S 4.80E-16 9.00E-13 2.2SE-13 2.12E-14 6.00E-13 1.S0E-13 1/3/2006 4.S4E-16 9.00E-14 2.2SE-14 L24E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 3.60E-14 6.00E-13 LSOE-13 4/3/2006 L99E-16 9.00E-14 2.2SE-14 L32E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 8.36E-1S 6.00E-13 LSOE-13 7/3/2006 2.76E-16 9.00E-14 2.2SE-14 2.63E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L03E-14 6.00E-13 LSOE-13 10/2/2006 4.97E-16 9.00E-14 2.2SE-14 2.37E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L60E-14 6.00E-13 1.S0E-13 1/1/2007 6.46E-16 9.00E-14 2.2SE-14 2.81E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 2.10E-14 6.00E-13 LSOE-13 4/2/2007 7.08E-16 9.00E-14 2.2SE-14 3.20E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 LS4E-14 6.00E-13 LSOE-13 7/2/2007 9.4lE-16 9.00E-14 2.2SE-14 L46E-16 2.00E-14 S.00E-1S L99E-16 9.00E-13 2.2SE-13 2.S6E-14 6.00E-13 LSOE-13 9/30/2007 3.30E-16 9.00E-14 2.2SE-14 S.SOE-16 2.00E-14 S.00E-15 LOOE-16 9.00E-13 2.2SE-13 7.S7E-1S 6.00E-13 1.S0E-13 12/31/2007 L42 E-1S 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 9.93E-1S 6.00E-13 1.S0E-13 3/31/2008 L2SE-16 9.00E-14 2.2SE-14 7.72E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 4.09E-1S 6.00E-13 LSOE-13 6/30/2008 L28E-1S 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S 3.61E-16 9.00E-13 2.2SE-13 L18E-14 6.00E-13 LSOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/200S 2.72E-1S 9.00E-14 2.2SE-14 L27E-1S 2.00E-14 S.00E-1S 7.66E-16 9.00E-13 2.2SE-13 L10E-14 6.00E-13 LSOE-13 12/31/200S 2.SSE-1S 9.00E-14 2.2SE-14 1.10E-1S 2.00E-14 S.00E-1S 6.S6E-16 9.00E-13 2.2SE-13 l.3SE-14 6.00E-13 LSOE-13 3/15/2009 LS6E-1S 9.00E-14 2.2SE-14 4.S7E-16 2.00E-14 S.00E-1S 2.99E-16 9.00E-13 2.2SE-13 4.97E-1S 6.00E-13 LSOE-13 6/15/2009 S.67E-17 9.00E-14 2.2SE-14 2.17E-16 2.00E-14 S.00E-1S LS1E-16 9.00E-13 2.2SE-13 4.47E-1S 6.00E-13 LSOE-13 9/15/2009 4.0SE-1S 9.00E-14 2.2SE-14 L4SE-1S 2.00E-14 S.00E-1S 2.S2E-16 9.00E-13 2.2SE-13 L24E-14 6.00E-13 1.S0E-13 12/15/2009 6.S0E-1S 9.00E-14 2.2SE-14 3.4SE-16 2.00E-14 S.00E-1S l.33E-16 9.00E-13 2.2SE-13 7.60E-1S 6.00E-13 LSOE-13 3/31/2010 6.0lE-1S 9.00E-14 2.2SE-14 l.26E-16 2.00E-14 S.00E-1S l.34E-16 9.00E-13 2.2SE-13 L19E-14 6.00E-13 LSOE-13 6/30/2010 2.33E-1S 9.00E-14 2.2SE-14 7.29E-16 2.00E-14 S.00E-1S 2.66E-16 9.00E-13 2.2SE-13 3.27E-1S 6.00E-13 1.S0E-13 9/30/2010 4.77E-1S 9.00E-14 2.2SE-14 1.S0E-1S 2.00E-14 S.00E-1S S.23E-16 9.00E-13 2.2SE-13 S.l1E-1S 6.00E-13 LSOE-13 12/31/2010 3.93E-1S 9.00E-14 2.2SE-14 3.90E-16 2.00E-14 S.00E-1S 2.S6E-16 9.00E-13 2.2SE-13 L13E-14 6.00E-13 LSOE-13 4/4/2011 L29E-1S 9.00E-14 2.2SE-14 L40E-16 2.00E-14 S.00E-1S LSSE-16 9.00E-13 2.2SE-13 L1lE-14 6.00E-13 1.S0E-13 7/4/2011 3.30E-1S 9.00E-14 2.2SE-14 S.44E-16 2.00E-14 S.00E-1S 4.1SE-16 9.00E-13 2.2SE-13 S.26E-1S 6.00E-13 LSOE-13 10/3/2011 L32E-1S 9.00E-14 2.2SE-14 7.S9E-16 2.00E-14 S.00E-1S L2SE-16 9.00E-13 2.2SE-13 L1SE-14 6.00E-13 LSOE-13 1/3/2012 L04E-1S 9.00E-14 2.2SE-14 3.2SE-16 2.00E-14 S.00E-1S 2.2SE-16 9.00E-13 2.2SE-13 1.14E-14 6.00E-13 LSOE-13 E ....... (3 ::J -tn C o .';:; ~ '-... c CI) o c o o CI) "'C U ::J c .2 "'C ~ a: III::t :> ::::J: m C\J Ct) ..,-..,- uJ uJ 0 0 ~ ~ ..,- ~ : .... .... ~ ~ ~ .-::: ~ • ~ r:; --r-- ~ • .... ~ ~ f:: ~ ~ f; :!. I· f::::: 5: • I ~c:: ~ ::::== ~ ~ .... ~ .-- ~ 411~ ~ ........ .... -. ... ... ~ ,,1= -~ ""' ~ .... ~K I~ ~ ... i,..oo-" ... ;::::. ~ ~ ~ ... "'" ..,- uJ 0 ~ ~ ~ f-'" -... ~ • F::: "'-' 1.41.::: ~ ,,~ 10-~ .... ~ ~ -~ ~ 6.. .,.:::;;;; I--~ ~ ~-des o~-des :::: tr-. i-J .. r.;; -r-._ -~~ ~ ~~ , -..x 60-deS so-des -::~ ..... ..... ~~ • ~ ~ ~- ~==-~ r::!Ie..... ... .....~ La-deS 90-deS so-des • t::>4 1""1" t::::::..~ I ~ t--...... va-deS 0 ~~ -.....:; ..: ~ -6j! ~ ~:04 ~ ~ -r-:::::. • ~~ ~ ~ ~ ~ • Ii: ~ ~ r-. ;:::.. I;;. ~ .~ ~ ,.-... It ~ !~ --~ ~r.... ::::r-, :!... ~~ -~ '~ ... >o~ .. ~ ~. ~ ~ ~ Io-~ • IX to-..... L.... ---;:. so-des ..,- C\J -6 Go-des ell Q) .....J ~o-des t OO-deS co C\J 66-deS C\J E S6-deS :::J is ell L6-deS II: t 96-deS .... 1-,. ... ~ --= S6-deS 0 Ct) C\J v6-deS E :::J ·c ~ S6-deS 0 .r:. r- ~~ ~~. ..... G6-deS t = ~ r-~ 1=0. .... 111-.... ... ~ I'-i!:!"" ~6-des (ij ~ ,.::::;: • Jt. ~ :.. ........ .... 06-deS :::J Cti z 6S-deS E .... :::J r+- ..... ~ .... h,i ... ~ ~~~ ~it' ... ss-des ·c ell ~ LS-deS :::> t 9S-deS r--r--i......& I .. k--~J ss-des I'-~~ ~ -". .... vs-des ... '-""-~ ..... ss-des ~~ I---..... ~ 10-'" Ie Gs-des ~ " ~ ... ~s-des L!) co f'-. co ..,-..,-..,-..,- uJ uJ uJ uJ 0 ~ 0 0 0 ~ ~ ~ ..,- (ereos 001) 1.00E-11 1.00E-12 1.00E-13 Q) (ij () Cf.I .OOE-14 0> o d 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.25E-14 uCi/ml Pre 1994 MPC Limit = 5E-12uCi/ml Pre 1994 ALARA Goal = 1.25E-12 uCi/ml BHV-4 Uranium-Natural Concentrations (uCi/ml) t t~ ~~ ..... \ \0. _ ~ T ... j' \ I"f. .. , . ~-\ \ ~ ,\ I \I \ \I~. \ \ I· ~ ~ 1)1 1'\ ,\ /\ j \ f ~. 1r ~ t ~ V~ 1/ J\ I~ ~ l. T.. T"II.. 1PT \ ~ 1\ 1\ n , I ~ 1t 1\ J • ~ ~ /\/ .... 1'/\ 1 I~ ... t J'f ~ .. \(t j V J II V' ~V\ IT. II , . , " \I • or-C\J Ct) .;:t LO <0 ,...... co 0') 0 or-C\J Ct) .;:t LO <0 ,...... co 0') 0 or-C\J Ct) .;:t LO <0 ,...... co 0') 0 co co co co co co co co co 0') 0') 0') 0') 0') 0') 0') 0') 0') 0') 0 0 0 0 0 0 0 0 0 0 or-0r-a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) E ...... (3 ::::J -tn C o "';:; CO J.. ... C CJ) o c o o o ('t) N I E ::::J "~ o J: I- ~ ::> J: OJ .~ C\J (1) T""" T""" T""" uJ uJ uJ 0 0 0 ~ ~ ~ T""" ~ ~ ~ ...... ~ IZ:~ I-f... -~ """"'"" I'-~ l ...- -""4 ~ ....... -..... ~'"' ~ -. ~ ~ v· ...r L() T""" T""" uJ uJ 0 0 0 ~ (ele~s 601) ... -..... ,,-I-r--P+ .... ~~ ~ ~-des o~-des -f+ ~ :::::-. .1-F=-' 60-deS so-des =-=-'I C ~ i ~ -4 LO-deS 90-des so-des -r-~ 1+= ~ Fro-r--. ~ , I ~~ ~ ~ ~ ~ ~ ~ 1-- vO-deS 80-deS Go-des ~o-des OO-deS 66-deS :--.... ... ..... ~ S6-deS i-'::=-r t-~~ r-~ L6-deS 96-deS S6-deS ..-~ : . .-~ i4l-1.2 .--A -~ , .... v6-deS 86-deS G6-deS ~ 14---~ ~6-des '"' 06-deS 6S-deS ss-des I .... LS-deS ~~ 9S-deS • 6::::1-~ ss-des I· =:::::: p. • ~ -r""'" :-- vs-des 8S-deS Gs-des ~s-des CD ,...... T""" T""" uJ uJ 0 0 ~ ~ .... ~ i~~ :::: ~ 41' f-i-. 1-", ~ t:l ~I""" ~~ P. "-~ -~ ~ ~ ~ ~-des o ~-des 60-deS so-des LO-deS ~ ~ ~ 90-deS ~ '-f::: -~ -~ ~ c::::: ~ ~ so-des vo-des ~ ..-= ~-3 ~ so-des Go-des ~o-des ~ .c::: ~ ::>t !. .,:::::: :::::+ ! ......- ~ ~ • I~~ :::: p. ..... oo-des 66-deS S6-deS L6-deS 96-deS f..,.. ..... ~ ""I--~ ~ I.~ r--~ S6-deS v6-deS S6-deS :*~ G6-deS ,.--... f-f:o. .~ -+-~6-des ~ ~ 06-deS ,. -~K ... --6S-deS +:: ::;:: ~ ~-~ ~ ss-des LS-deS 1 --......... -~ ~ c:::_ ~ - 9S-deS ss-des -,.4i; vs-des =;;,.. -... :::;::.:::1411 ~(" ss-des 40::: :::;: - ~ ~ Gs-des ~s-des C\I Cf) ~ L() <0 I'--a::> T-" T-" T-" T-" T-" T-" T-" T-" W W W uJ uJ uJ uJ uJ 0 0 0 0 0 0 0 C! C! C! o 0 C! C! ~ereos oOlf 0 C! -:§ o :J -tn s:: o ;; as J... ... s:: Cl) (J s:: o o o T"'" C\I I "C as Cl) ...J ~ ::::-J: m ~ """ C\I ('f) T""" T""" T""" uJ uJ uJ 0 0 0 q q q I: : ~~ • -I-~ ~ ~, ~ ~~ ~ I ~ ,. ~ ~ ~I--N r--- ~ .. -~~:::o - :~ :::.4 -I--t::::.. .::;.. ::. ~~ 4 ~~ ~r.. t:, """ ~ < ~ ~ ~ C!. • =::::: • g: I ~IC: ::; ~ ~ ~ ~ .--- ~ 141::: -r+-Dt l-4I ...... ~K ~ ~~~ .~ ...... ...- .... p. ) I... ~ T""" uJ 0 0 (elBos 001) ~ ~-des o~-des 60-deS 80-deS LO-deS 90-deS so-des Po-des 80-deS Go-des ~o-des OO-deS 66-deS 86-deS L6-deS 96-deS S6-deS P6-deS 86-deS G6-deS ~6-des 06-deS 68-deS 88-deS L8-deS 98-deS S8-deS P8-deS ~ .... 88-deS G8-des ~8-des L{) <0 I"-- T""" T""" T""" uJ uJ I W 0 0 0 q q q TAB 5 BHV-5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.44E-1S S.00E-12 1.2SE-12 1.S3E-1S 8.00E-14 2.00E-14 7.S4E-16 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 1.00E-12 12/14/1981 4.84E-1S S.00E-12 1.2SE-12 2.78E-1S 8.00E-14 2.00E-14 1.84E-1S 2.00E-12 S.OOE-13 1.S3E-14 4.00E-12 1.00E-12 3/29/1982 1.04E-1S S.00E-12 1.2SE-12 2.62E-1S 8.00E-14 2.00E-14 1.11E-1S 2.00E-12 S.OOE-13 2.98E-14 4.00E-12 1.00E-12 6/30/1982 3.61E-1S S.00E-12 1.2SE-12 7.61E-1S 8.00E-14 2.00E-14 1.39E-1S 2.00E-12 S.OOE-13 1.80E-1S 4.00E-12 1.00E-12 9/27/1982 1.71E-14 S.00E-12 1.2SE-12 9.46E-1S 8.00E-14 2.00E-14 3.80E-1S 2.00E-12 S.OOE-13 2.3SE-14 4.00E-12 1.00E-12 1/3/1983 1.90E-14 S.00E-12 1.2SE-12 S.77E-1S 8.00E-14 2.00E-14 9.34E-17 2.00E-12 S.OOE-13 4.32E-14 4.00E-12 1.00E-12 4/4/1983 S.00E-12 1.2SE-12 2.33E-1S 8.00E-14 2.00E-14 S.93E-16 2.00E-12 S.OOE-13 3.01E-14 4.00E-12 1.00E-12 6/30/1983 7.62E-16 S.00E-12 1.2SE-12 3.2SE-1S 8.00E~14 2.00E-14 6.28E-1S 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 1.00E-12 10/3/1983 4.86E-16 S.00E-12 l.2SE-12 1.10E-1S 8.00E-14 2.00E-14 3.63E-16 2.00E-12 S.OOE-13 2.08E-14 4.00E-12 1.00E-12 1/3/1984 6.96E-1S S.00E-12 1.2SE-12 9.69E-16 8.00E-14 2.00E-14 9.60E-16 2.00E-12 S.OOE-13 1.83E-14 4.00E-12 1.00E-12 4/2/1984 1.64E-1S S.00E-12 1.2SE-12 1.34E-1S 8.00E-14 2.00E-14 3.88E-1S 2.00E-12 S.OOE-13 4.67E-14 4.00E-12 1.00E-12 7/2/1984 1.12E-1S S.00E-12 1.2SE-12 1.92E-1S 8.00E-14 2.00E-14 3.3lE-1S 2.00E-12 S.OOE-13 2.2lE-14 4.00E-12 1.00E-12 10/1/1984 l.1lE-1S S.00E-12 1.2SE-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 2.00E-12 S.OOE-13 1.S7E-14 4.00E-12 1.00E-12 1/2/1985 7.32E-16 S.00E-12 1.2SE-12 6.7lE-16 8.00E-14 2.00E-14 4.94E-16 2.00E-12 S.OOE-13 2.42E-14 4.00E-12 1.00E-12 4/1/1985 2.36E-16 S.00E-12 1.2SE-12 S.43E-16 8.00E-14 2.00E-14 2.71E-16 2.00E-12 S.OOE-13 1.2SE-14 4.00E-12 1.00E-12 7/1/1985 7.S8E-16 S.00E-12 1.2SE-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 S.OOE-13 2.1SE-14 4.00E-12 1.00E-12 9/30/1985 7.47E-1S S.00E-12 1.2SE-12 1.16E-1S 8.00E-14 2.00E-14 2.19E-1S 2.00E-12 S.OOE-13 9.20E-1S 4.00E-12 1.00E-12 1/2/1986 1.7SE-14 S.00E-12 1.2SE-12 7.24E-1S 8.00E-14 2.00E-14 3.83E-1S 2.00E-12 S.OOE-13 1.13E-16 4.00E-12 1.00E-12 4/1/1986 2.99E-14 S.00E-12 1.2SE-12 7.64E-1S 8.00E-14 2.00E-14 1.S1E-14 2.00E-12 S.OOE-13 2.22E-14 4.00E-12 1.00E-12 6/30/1986 2.23E-14 S.00E-12 l.2SE-12 S.19E-1S 8.00E-14 2.00E-14 1.0SE-14 2.00E-12 S.OOE-13 2.16E-14 4.00E-12 1.00E-12 10/27/1986 2.33E-14 S.00E-12 1.2SE-12 7.78E-1S 8.00E-14 2.00E-14 1.60E-14 2.00E-12 S.OOE-13 2.02E-14 4.00E-12 1.00E-12 12/15/1986 3.40E-14 S.00E-12 1.2SE-12 S.3SE-1S 8.00E-14 2.00E-14 1.47E-14 2.00E-12 S.OOE-13 2.82E-14 4.00E-12 1.00E-12 3/16/1987 2.06E-14 S.00E-12 1.2SE-12 4.S0E-1S 8.00E-14 2.00E-14 6.74E-1S 2.00E-12 S.OOE-13 7.29E-14 4.00E-12 1.00E-12 5/11/1987 2.S0E-14 S.00E-12 l.2SE-12 8.S4E-1S 8.00E-14 2.00E-14 8.1SE-1S 2.00E-12 S.OOE-13 3.28E-14 4.00E-12 1.00E-12 9/9/1987 2.6SE-14 S.00E-12 1.2SE-12 6.62E-1S 8.00E-14 2.00E-14 9.34E-1S 2.00E-12 S.OOE-13 2.77E-14 4.00E-12 1.00E-12 11/2/1987 1.80E-14 S.00E-12 1.2SE-12 7.09E-1S 8.00E-14 2.00E-14 7.20E-1S 2.00E-12 S.OOE-13 1.77E-14 4.00E-12 1.00E-12 2/16/1988 1.01E-14 S.00E-12 1.2SE-12 2.98E-1S 8.00E-14 2.00E-14 3.93E-1S 2.00E-12 S.OOE-13 3.36E-14 4.00E-12 1.00E-12 5/18/1988 1.78E-14 S.00E-12 1.2SE-12 8.14E-1S 8.00E-14 2.00E-14 7.43E-1S 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 1.00E-12 8/15/1988 1.79E-14 S.00E-12 1.2SE-12 1.49E-14 8.00E-14 2.00E-14 S.34E-1S 2.00E-12 S.OOE-13 2.4SE-14 4.00E-12 1.00E-12 11/14/1988 4.46E-14 S.00E-12 1.2SE-12 1.39E-14 8.00E-14 2.00E-14 1.17E-14 2.00E-12 S.OOE-13 3.43E-14 4.00E-12 1.00E-12 2/13/1989 1.67E-14 S.00E-12 1.2SE-12 S.S4E-1S 8.00E-14 2.00E-14 7.20E-1S 2.00E-12 S.OOE-13 S.02E-14 4.00E-12 1.00E-12 5/15/1989 2.03E-14 S.00E-12 1.2SE-12 7.0SE-1S 8.00E-14 2.00E-14 9.S6E-16 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.00E-12 8/14/1989 2.81E-1S S.00E-12 1.2SE-12 3.78E-1S 8.00E-14 2.00E-14 9.26E-1S 2.00E-12 S.OOE-13 1.S0E-14 4.00E-12 1.00E-12 11/13/1989 S.38E-14 S.00E-12 1.2SE-12 8.0lE-1S 8.00E-14 2.00E-14 1.81E-14 2.00E-12 S.OOE-13 4.09E-14 4.00E-12 1.00E-12 2/12/1990 4.48E-14 S.00E-12 1.2SE-12 1.48E-14 8.00E-14 2.00E-14 1.28E-14 2.00E-12 S.OOE-13 3.88E-14 4.00E-12 1.00E-12 5/14/1990 2.18E-14 S.00E-12 1.2SE-12 1.70E-14 8.00E-14 2.00E-14 1.S9E-14 2.00E-12 S.OOE-13 3.49E-14 4.00E-12 1.00E-12 8/13/1990 9.S3E-1S S.00E-12 1.2SE-12 1.70E-14 8.00E-14 2.00E-14 3.27E-1S 2.00E-12 S.OOE-13 1.27E-14 4.00E-12 1.00E-12 11/12/1990 1.11E-14 S.00E-12 1.2SE-12 S.27E-1S 8.00E-14 2.00E-14 S.38E-1S 2.00E-12 S.OOE-13 1.S6E-14 4.00E-12 1.00E-12 2/11/1991 6.3SE-16 S.00E-12 l.2SE-12 3.13E-16 8.00E-14 2.00E-14 2.3lE-16 2.00E-12 S.OOE-13 3.89E-14 4.00E-12 1.00E-12 5/13/1991 1.22E-1S S.00E-12 1.2SE-12 6.14E-1S 8.00E-14 2.00E-14 4.41E-1S 2.00E-12 S.OOE-13 2.S0E-14 4.00E-12 1.00E-12 8/12/1991 7.84E-16 S.00E-12 1.2SE-12 1.43E-1S 8.00E-14 2.00E-14 4.47E-16 2.00E-12 S.OOE-13 1.84E-14 4.00E-12 1.00E-12 11/11/1991 S.37E-16 S.00E-12 1.2SE-12 4.20E-16 8.00E-14 2.00E-14 1.37E-16 2.00E-12 S.OOE-13 1.27E-14 4.00E-12 1.00E-12 2/10/1992 3.S4E-16 S.00E-12 1.2SE-12 1.18E-16 8.00E-14 2.00E-14 4.08E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 1.00E-12 5/11/1992 4.71E-16 S.00E-12 1.2SE-12 9.S8E-16 8.00E-14 2.00E-14 8.3lE-17 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.00E-12 8/10/1992 S.32E-1S S.00E-12 1.2SE-12 3.36E-16 8.00E-14 2.00E-14 1.6SE-16 2.00E-12 S.OOE-13 1.S9E-14 4.00E-12 1.00E-12 11/9/1992 3.66E-16 S.00E-12 1.2SE-12 2.2SE-16 8.00E-14 2.00E-14 1.08E-16 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 1.00E-12 2/9/1993 2.0SE-16 S.00E-12 1.2SE-12 9.14E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 1.00E-12 5/10/1993 4.80E-16 S.00E-12 1.2SE-12 8.2SE-16 8.00E-14 2.00E-14 1.26E-1S 2.00E-12 S.OOE-13 1.83E-14 4.00E-12 1.00E-12 8/10/1993 8.30E-16 S.00E-12 1.2SE-12 1.90E-16 8.00E-14 2.00E-14 2.10E-16 2.00E-12 S.OOE-13 1.70E-14 4.00E-12 1.00E-12 11/8/1993 2.70E-16 S.00E-12 1.2SE-12 8.00E-17 8.00E-14 2.00E-14 7.00E-17 2.00E-12 S.OOE-13 2.34E-14 4.00E-12 1.00E-12 2/7/1994 3.18E-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 S.18E-16 2.00E-12 S.OOE-13 3.64E-14 4.00E-12 1.00E-12 5/9/1994 1.80E-1S S.00E-12 1.2SE-12 9.78E-16 8.00E-14 2.00E-14 1.10E-1S 2.00E-12 S.OOE-13 8.30E-1S 4.00E-12 1.00E-12 8/9/1994 2.67E-1S S.00E-12 1.2SE-12 1.11E-1S 8.00E-14 2.00E-14 4.9SE-16 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.21E-17 S.00E-12 1.2SE-12 1.S9E-1S 8.00E-14 2.00E-14 1.66E-1S 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 _._- Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARA Goal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARA Goal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Cone EFC EFCA 2/7/1995 l.slE-1s 9.00E-14 2.2sE-14 9.s0E-16 2.00E-14 s.00E-1s 9.70E-17 9.00E-13 2.2sE-13 9.3sE-1s 6.00E-13 l.sOE-13 5/9/1995 2.2lE-16 9.00E-14 2.2sE-14 8.s6E-16 2.00E-14 S.00E-1s 3.06E-1s 9.00E-13 2.2SE-13 4.34E-1s 6.00E-13 l.sOE-13 8/9/1995 l.66E-16 9.00E-14 2.2sE-14 1.67E-1s 2.00E-14 s.00E-1s 3.90E-1s 9.00E-13 2.2SE-13 s.60E-1s 6.00E-13 l.sOE-13 11/11/1995 2.04E-14 9.00E-14 2.2sE-14 6.70E-1s 2.00E-14 s.00E-1s 7.6sE-1s 9.00E-13 2.2sE-13 4.47E-1s 6.00E-13 l.sOE-13 2/5/1996 4.s0E-14 9.00E-14 2.2sE-14 3.s8E-14 2.00E-14 s.00E-1s 2.39E-14 9.00E-13 2.2sE-13 7.30E-1S 6.00E-13 l.sOE-13 5/6/1996 l. 76E-1s 9.00E-14 2.2sE-14 3.s7E-1s 2.00E-14 s.00E-1s 9.SsE-16 9.00E-13 2.2sE-13 7.s4E-1s 6.00E-13 l.SOE-13 8/5/1996 2.37E-1s 9.00E-14 2.2sE-14 8.18E-1s 2.00E-14 s.00E-1s 7.46E-16 9.00E-13 2.2sE-13 s.7sE-1s 6.00E-13 l.sOE-13 11/6/1996 3.s3E-1s 9.00E-14 2.2sE-14 s.31E-1s 2.00E-14 s.00E-1s 9.39E-16 9.00E-13 2.2sE-13 l.2lE-14 6.00E-13 1.s0E-13 2/6/1997 1.84E-16 9.00E-14 2.2sE-14 2.01E-16 2.00E-14 s.00E-1s 1.87E-16 9.00E-13 2.2sE-13 6.14E-1s 6.00E-13 1.s0E-13 5/5/1997 s.7sE-16 9.00E-14 2.2sE-14 7.24E-16 2.00E-14 s.00E-1s 6.07E-16 9.00E-13 2.2sE-13 4.7SE-1s 6.00E-13 1.S0E-13 8/11/1997 l.21E-1s 9.00E-14 2.2sE-14 7.39E-16 2.00E-14 s.00E-1s s.OsE-16 9.00E-13 2.2SE-13 4.92E-1s 6.00E-13 l.sOE-13 1/5/1998 9.89E-16 9.00E-14 2.2sE-14 l.92E-1S 2.00E-14 s.00E-1S 6.2lE-16 9.00E-13 2.2sE-13 4.68E-1s 6.00E-13 l.sOE-13 4/28/1998 2.84E-1s 9.00E-14 2.2sE-14 2.38E-1s 2.00E-14 s.00E-1s l.72E-1s 9.00E-13 2.2sE-13 7.3sE-1S 6.00E-13 l.sOE-13 7/31/1998 7.49E-16 9.00E-14 2.2sE-14 l.49E-1s 2.00E-14 s.00E-1s 8.34E-16 9.00E-13 2.2sE-13 7.01E-1s 6.00E-13 l.sOE-13 9/28/1998 1.07E-1s 9.00E-14 2.2sE-14 9.20E-16 2.00E-14 s.00E-1s 6.32E-16 9.00E-13 2.2sE-13 3.9SE-1s 6.00E-13 1.s0E-13 12/28/1998 8.slE-1s 9.00E-14 2.2sE-14 4.s8E-1s 2.00E-14 S.00E-1s 4.s8E-1s 9.00E-13 2.2sE-13 l.43E-14 6.00E-13 l.sOE-13 3/29/1999 3.7sE-1s 9.00E-14 2.2sE-14 2.4sE-1s 2.00E-14 s.00E-1s 2.39E-1s 9.00E-13 2.2sE-13 8.46E-1s 6.00E-13 l.sOE-13 7/3/1999 l.s3E-1S 9.00E-14 2.2sE-14 8.6sE-16 2.00E-14 s.00E-1S 6.s2E-16 9.00E-13 2.2SE-13 7.20E-1s 6.00E-13 l.sOE-13 9/27/1999 S.83E-1s 9.00E-14 2.2sE-14 3.S2E-1s 2.00E-14 s.00E-1s 2.ssE-1s 9.00E-13 2.2sE-13 8.22E-1s 6.00E-13 l.sOE-13 12/28/1999 9.48E-1s 9.00E-14 2.2SE-14 6.20E-1s 2.00E-14 s.00E-1s 3.96E-1s 9.00E-13 2.2sE-13 7.s6E-1s 6.00E-13 1.S0E-13 3/27/2000 2.06E-1s 9.00E-14 2.2sE-14 l.27E-1s 2.00E-14 S.00E-1s l.09E-1s 9.00E-13 2.2sE-13 7.72E-1s 6.00E-13 1.s0E-13 6/26/2000 l.sOE-1s 9.00E-14 2.2sE-14 1.24E-1S 2.00E-14 s.00E-1S l.OlE-1s 9.00E-13 2.2SE-13 4.36E-1s 6.00E-13 l.sOE-13 9/26/2000 l.04E-1s 9.00E-14 2.2sE-14 s.4sE-16 2.00E-14 s.00E-1s 6.0lE-16 9.00E-13 2.2sE-13 7.67E-1s 6.00E-13 l.sOE-13 12/26/2000 1.48E-1s 9.00E-14 2.2SE-14 7.s6E-16 2.00E-14 s.00E-1s 6.84E-16 9.00E-13 2.2sE-13 7.00E-1S 6.00E-13 l.sOE-13 3/26/2001 4.27E-16 9.00E-14 2.2sE-14 2.19E-16 2.00E-14 s.00E-1s 1.89E-16 9.00E-13 2.2sE-13 6.13E-1s 6.00E-13 1.s0E-13 7/2/2001 4.s2E-16 9.00E-14 2.2sE-14 4.02E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 7.48E-1s 6.00E-13 1.s0E-13 9/24/2001 4.6sE-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 s.00E-1s 2.02E-16 9.00E-13 2.2sE-13 6.98E-1s 6.00E-13 1.s0E-13 12/31/2001 7.40E-16 9.00E-14 2.2sE-14 3.s1E-16 2.00E-14 s.00E-1s 3.64E-16 9.00E-13 2.2sE-13 4.72E-1s 6.00E-13 l.sOE-13 4/1/2002 l.26E-1s 9.00E-14 2.2sE-14 7.s3E-16 2.00E-14 s.00E-1s 7.19E-16 9.00E-13 2.2sE-13 9.6sE-1s 6.00E-13 l.sOE-13 7/1/2002 l.02E-1s 9.00E-14 2.2sE-14 l.03E-1S 2.00E-14 s.00E-1S 3.39E-16 9.00E-13 2.2sE-13 7.20E-1s 6.00E-13 l.sOE-13 9/30/2002 S.82E-16 9.00E-14 2.2SE-14 9.28E-16 2.00E-14 s.00E-1s 3.14E-16 9.00E-13 2.2sE-13 4.48E-1s 6.00E-13 l.sOE-13 12/30/2002 l.00E-16 9.00E-14 2.2SE-14 7.67E-16 2.00E-14 s.00E-1s 3.48E-16 9.00E-13 2.2sE-13 9.s6E-1S 6.00E-13 1.S0E-13 3/31/2003 1.13E-1s 9.00E-14 2.2sE-14 7.4lE-16 2.00E-14 s.00E-1s 4.41E-16 9.00E-13 2.2sE-13 6.68E-1s 6.00E-13 1.s0E-13 6/30/2003 4.3sE-16 9.00E-14 2.2sE-14 s.08E-16 2.00E-14 S.00E-1s 2.s1E-16 9.00E-13 2.2sE-13 l.34E-1s 6.00E-13 1.s0E-13 9/29/2003 l.slE-16 9.00E-14 2.2sE-14 l.02E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 7.28E-1s 6.00E-13 l.sOE-13 12/29/2003 l.s2E-16 9.00E-14 2.2sE-14 l.S4E-16 2.00E-14 s.00E-1S l.slE-16 9.00E-13 2.2SE-13 7.02E-1s 6.00E-13 l.sOE-13 3/29/2004 1.00E-16 9.00E-14 2.2sE-14 l.12E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 8.82E-1s 6.00E-13 l.sOE-13 6/27/2004 1.18E-16 9.00E-14 2.2sE-14 3.1lE-16 2.00E-14 s.00E-1s l.2sE-16 9.00E-13 2.2sE-13 2.47E-1s 6.00E-13 l.sOE-13 9/27/2004 l.16E-16 9.00E-14 2.2sE-14 l.72E-16 2.00E-14 s.00E-1s l.18E-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 1.s0E-13 12/27/2004 l.14E-16 9.00E-14 2.2sE-14 l.06E-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2sE-13 l.s9E-14 6.00E-13 l.sOE-13 3/28/2005 l.00E-16 9.00E-14 2.2sE-14 2.04E-16 2.00E-14 s.00E-1s l.83E-16 9.00E-13 2.2sE-13 8.s7E-1s 6.00E-13 l.sOE-13 6/29/2005 l.83E-16 9.00E-14 2.2sE-14 3.81E-16 2.00E-14 s.00E-1s 3.09E-16 9.00E-13 2.2sE-13 l.06E-14 6.00E-13 l.sOE-13 9/26/2005 2.87E-16 9.00E-14 2.2sE-14 8.21E-16 2.00E-14 s.00E-1s 3.71E-14 9.00E-13 2.2sE-13 6.28E-14 6.00E-13 l.sOE-13 1/3/2006 8.74E-16 9.00E-14 2.2sE-14 3.79E-16 2.00E-14 s.00E-1s l.31E-16 9.00E-13 2.2sE-13 4.32E-14 6.00E-13 l.sOE-13 4/3/2006 s.22E-16 9.00E-14 2.2sE-14 6.66E-16 2.00E-14 s.00E-1s l.l1E-16 9.00E-13 2.2sE-13 9.34E-1s 6.00E-13 1.s0E-13 7/3/2006 3.08E-16 9.00E-14 2.2sE-14 l.10E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 l.2SE-14 6.00E-13 l.sOE-13 10/2/2006 9.14E-16 9.00E-14 2.2sE-14 4.9sE-16 2.00E-14 s.00E-1s l.86E-16 9.00E-13 2.2sE-13 l.67E-14 6.00E-13 l.sOE-13 1/1/2007 9.49E-16 9.00E-14 2.2sE-14 6.81E-16 2.00E-14 s.00E-1S 2.02E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.sOE-13 4/2/2007 l.08E-1s 9.00E-14 2.2sE-14 8.22E-16 2.00E-14 s.00E-1s 2.26E-16 9.00E-13 2.2sE-13 1.64E-14 6.00E-13 l.sOE-13 7/2/2007 l.s4E-1s 9.00E-14 2.2sE-14 8.16E-16 2.00E-14 S.00E-1s 4.76E-16 9.00E-13 2.2SE-13 2.12E-14 6.00E-13 l.sOE-13 9/30/2007 4.90E-16 9.00E-14 2.2sE-14 2.37E-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2sE-13 6.6sE-1s 6.00E-13 l.sOE-13 12/31/2007 l.46E-1s 9.00E-14 2.2sE-14 s.67E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 l.02E-14 6.00E-13 l.sOE-13 3/31/2008 3.16E-16 9.00E-14 2.2sE-14 6.17E-16 2.00E-14 s.00E-1s 3.71E-16 9.00E-13 2.2sE-13 4.82E-1s 6.00E-13 l.sOE-13 6/30/2008 3.13E-1s 9.00E-14 2.2SE-14 l.sSE-1s 2.00E-14 s.00E-1s 9.27E-16 9.00E-13 2.2sE-13 7.40E-1s 6.00E-13 l.sOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/200S 7.0SE-1s 9.00E-14 2.2sE-14 3.41E-ls 2.00E-14 s.OOE-ls 2.s2E-ls 9.00E-13 2.2sE-13 .1.1sE-14 6.00E-13 l.s0E-13 12/31/200S 7.22E-ls 9.00E-14 2.2sE-14 2.S2E-ls 2.00E-14 s.OOE-ls 3.03E-1s 9.00E-13 2.2sE-13 l.s9E-14 6.00E-13 l.s0E-13 3/15/2009 4.13E-ls 9.00E-14 2.2sE-14 1.39E-1s 2.00E-14 s.OOE-ls 1.41E~ls 9.00E-13 2.2sE-13 4.66E-ls 6.00E-13 l.s0E-13 6/15/2009 2.31E-16 9.00E-14 2.2sE-14 7.79E-16 2.00E-14 s.OOE-ls 6.37E-16 9.00E-13 2.2sE-13 4.18E-ls 6.00E-13 l.s0E-13 9/15/2009 3.10E-ls 9.00E-14 2.2sE-14 9.20E-16 2.00E-14 s.OOE-ls 6.36E-16 9.00E-13 2.2sE-13 1.21E-14 6.00E-13 1.s0E-13 12/15/2009 s.77E-ls 9.00E-14 2.2sE-14 3.13E-16 2.00E-14 s.OOE-ls 1.92E-16 9.00E-13 2.2sE-13 2.48E-iS 6.00E-13 l.s0E-13 3/31/2010 4.78E-ls 9.00E-14 2.2sE-14 3.73E-16 2.00E-14 s.OOE-ls 4.19E-16 9.00E-13 2.2sE-13 1.30E-14 6.00E-13 1.s0E-13 6/30/2010 4.3sE-1s 9.00E-14 2.2sE-14 7.S4E-16 2.00E-14 s.OOE-ls 1.0sE-ls 9.00E-13 2.2sE-13 4.40E-1s 6.00E-13 1.s0E-13 9/30/2010 3.s7E-ls 9.00E-14 2.2sE-14 1.14E-ls 2.00E-14 s.OOE-ls 7.97E-16 9.00E-13 2.2sE-13 3.7SE-ls 6.00E-13 1.s0E-13 12/31/2010 8.s2E-ls 9.00E-14 2.2sE-14 l.4sE-ls 2.00E-14 s.OOE-ls 1.29E-ls 9.00E-13 2.2sE-13 1.33E-14 6.00E-13 1.s0E-13 4/4/2011 3.20E-ls 9.00E-14 2.2sE-14 8.89E-16 2.00E-14 s.OOE-ls 1.10E-ls 9.00E-13 2.2sE-13 1.48E-14 6.00E-13 l.s0E-13 7/4/2011 6.98E-ls 9.00E-14 2.2sE-14 2.03E-ls 2.00E-14 s.OOE-ls 2.s2E-ls 9.00E-13 2.2sE-13 1.08E-14 6.00E-13 l.s0E-13 10/3/2011 3.l1E-ls 9.00E-14 2.2sE-14 1.14E-ls 2.00E-14 s.00E-1s s.7sE-16 9.00E-13 2.2sE-13 1.41E-14 6.00E-13 l.s0E-13 1/3/2012 4.44E-ls 9.00E-14 2.2sE-14 2.14E-1s 2.00E-14 s.OOE-ls l.s3E-ls 9.00E-13 2.2sE-13 2.0sE-14 6.00E-13 l.s0E-13 -:§ o ::s -tn t: o '; ctS '-~ t: CI) U t: o o CI) :2 u ::s t: .2 "C ctS a: Lt') :> ::I: m C\J ,...- uJ 0 ~ ('t) ,...- uJ 0 ~ ..... ~ I-" I~ ~ I. ~ ~ .. ~ ~ ~~ f* I. ... .. .. :::::: . ~ ~ .... .. «:; ~ .~ ...;...;: -. ~ +: ~ I-- ~ F; ~ ::::::::: p K -~~ -.... ~---IP ..... ~.,. -~ Lt; ~ ~ ~~ --.:..:: • :s. • ,. ..... -• ~ t --.... "'" ~ ""'" ,...- I w 0 ~ "F: ~~ r ... ~ ~ ::~ ~ ;. :::a"" ~~ ~ .. r-~ ~ T ~ ~-des o~-des 60-deS ~~ ~ ~ 80-deS t...~. .-=: ~-~ a ~ --.. ~~ ~r-. ... ...",. ~ 11l1li ... LO-deS 90-des -~ ~ """"lII -:::= .. ~k ~ ~ ~ , -,..:::. ~ _;J ~~~ Ie ... ...... ...... !-=:: ~ ~~ ~ ~ "':::. A 5. so-des vo-des 0 so-des ,...- C\J -6 Go-des co Q) .....J ~o-des + OO-deS <0 C\J -~ 66-deS C\J E ... ,;;~ ... ...,~ ~ :~~ f~ ~~ ......... ~ 86-deS :::J :.c co L6-deS a: + 96-deS 1'1 ~~ ~ .....ii~ i-o ~ S6-deS 0 ('t) C\J v6-deS E :::J """4 --~ ....... I....--" , ~ T ".:::: S6-deS 0 ..c ..... ......;;;:!II -~ ~ ~ ~ ~ r-::0.1 ...... "'!II - ~ G6-deS + ~6-des ~ ~ 06-deS :::J Cti z 68-deS E :::J • III 88-deS c ~ ...1=1 ~~ .~ :J4 L8-deS ::J + 98-deS ~ .. .... S8-deS -=iIIC~ ... rZ! ~ v8-deS ~ I .... S8-deS ,..1"---..... G8-deS -. :::::. -.: ... ---~8-des L{) <0 f'-.. ex:> ,...-,...-,...-,...- uJ I uJ uJ w 0 0 0 0 ~ ~ ~ ~ (el13os BOl) :=- ~ (.) ::s -tn c: o ",4:: CO lI.. ... c: CI) (J c: o (.) (ij lI.. ::s ... CO Z I E ::s c: CO lI.. :l Lt) :> :I: m C\J Ct) ~ ~ ~ uJ uJ uJ 0 0 0 C! C! C! ~ I'" ~ ~ t ::a4 ~I--I--i-I--I-f; ~~ ....... 100- .... -..... ....... ~ ~ .. J. --~ ;- .... ....... ---~ ~ ~ '- I.~!... .... I"'~ .... .... :....... ~ • .... .. -I---~ ~ ~ ~ .F: ~ r-!> ~ I. ~ t+--- i.--~ L ~ -~ ~~ -. 'o::::t L!J ~ ~ uJ uJ 0 0 0 C! (elBos 001) ~ ~-des o ~-des .... 60-des so-des ;;;::r" ::~~ LO-deS 1-1'-~~~ ~ 90-deS I-1-1""--~ D I--f41---I-- so-des vO-deS so-des fo""~ Go-des :~ ~o-des OO-deS 66-deS S6-deS ~r-r-I:::::..i.. L6-deS 96-deS .... ..... S6-deS v6-deS f-~~ 1-1'-0 ~t-p..~ J... S6-deS G6-deS i-"~ ~~ ~6-des ~ 06-deS 6S-deS ss-des LS-deS 9s-des ss-des ~ ~~ po. vs-des r-P ss-des Gs-des ~s-des <0 I'- ~ ~ uJ uJ 0 0 C! C! In C o +=i CO Jo.. ... C (1) U C o (.) o ('I) C\I I E ::::s .~ o .t: ~ Lt) ::> ::I: m C\I (1) or-or-or- uJ uJ uJ 0 0 0 q q q ~~ ~ ~t: -+"'" ......-.. ~ -¥ .... ~ - .1:::: ~ ::::::== ~ ::+=== ............. 1& 1-1-I--r+-.. ~ ~ I""'""""" .....- C ...... ;::,. ~ t:. .. -. ~ ::::d ~~~ ~~ 1---r--. ~ ~S; l---4 ~ .. ~ 1--t.. ~ ~ L!) or-or- uJ uJ 0 0 0 q (elBos 601) ~ ~-des o~-des ...... ~ ... -60-deS 80-des .-~~ La-des :::::.. 90-deS f'p~ I'-r-. ~~ p ~~ ~ -,,0'- so-des va-des 80-deS Go-des ....... ~~ ~ ~~ ... -~ ~o-des OO-deS 66-deS 86-deS L6-deS 1'-1-1-1::::..0 96-deS S6-deS v6-deS -~ 86-deS -~ ~ ~ G6-deS ..... -4"""" I-~ ~6-des 06-deS 68-deS 88-deS L8-deS 98-deS ~~' ~I'-I-~ S8-deS v8-deS 88-deS G8-deS ~8-des <0 """ or-or- uJ uJ 0 0 q q 1.00E-1 1 1.00E-12 1.00E-13 Q) ~ u CJ:I.OOE-14 0> o d 1.00E-1S 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml -------------------- ~ • M ... "'I T\.I \ 1_ .. 1 II /I ~ 1 'h 'I' 'F II I I ' J 7'J J I I ... il .... I V It"Ir I • • \/ \ • ~ \ t~ '1 • , Jl ..... .,-C\J ('I) """ L!) <D f'-.. co 0) 0 .,-C\J co co co co co co co co co 0) 0) 0) 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) \ • \ \ ~ .~ 6. .I. T 'F l. \ ('I) """ 0) 0) 6. 6. Q) Q) CI) CI) BHV-5 Radium-226 Concentrations (uCi/ml) • .~ I I .J. ip .... ~ 1\ 1J .... .~ f\ 1\ f ~ \ L / \ .~' j n.,.;" .... 1\ I .. , IT I \ • 1 J ,. I , ~ .... \ /1 ? \ r V \ 1 ~ I ~ I V • V \!vJ J 1 ... L!) <D f'-.. co 0) 0 .,-C\J ('I) """ L!) <D f'-.. co 0) 0 .,- 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 .,-.,- 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) 1.00E-1 1 1.00E-12 1.00E-13 Q) co C,.) ClLOOE-14 0> o d 1.00E-1S 1.00E-16 1.00E-17 ~ ~ T""" co 6. Q) CJ) Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml " .... • 1P " J{ .... .... I)" 1\ J ... *\ r .. ~ T . " + ",. ~ 41 J "'..1),11 \, \, ~ 1\ J\ ~, ... ¥V' "Y • .. ~~ .... ~ ~ ~ C\J ('f) ""'" L{) <0 f'-.. co 0) 0 T""" C\J ('f) co co co co co co co co 0) 0) 0) 0) 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) BHV-5 Lead-210 Concentrations (uCi/ml) I I I r'-. ~ \ .. t ~ " ... ~ \l!' .... " i t .~ 1\ r -" .... r""f'I \ ~""I( 1,('. "Y ,. r , , ,. .... "" .... J \I \I .... V \I , \I \ , •• ..... II • ... , \ .. ~ ~ "Y \I U • • • l ""'" L{) <0 f'-.. co 0) 0 T""" C\J ('f) ""'" L{) <0 f'-.. co 0) 0 T""" 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 T""" T""" 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) TAB 6 BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 12/14/1981 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 3/29/1982 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 J 6/30/1982 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 9/27/1982 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/3/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/4/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 6/30/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/3/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/3/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/2/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 7/2/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/1/1984 S.00E-12 l.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/2/198S S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 I 4/1/198S S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 7/1/198S S.OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 9/30/198S S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/2/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/1/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 6/30/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/27/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 12/1S/1986 S.00E-12 l.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 3/16/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/11/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 9/9/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/2/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/16/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/18/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/lS/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/14/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/13/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/lS/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/14/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/13/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/12/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/14/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/13/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/12/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/11/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/13/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/12/1991 S.00E-12 l.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/11/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/10/1992 S.OOE-12 l.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/11/1992 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-1~ 8/10/1992 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/9/1992 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/9/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/10/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/10/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/8/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/7/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 S/9/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/9/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/7/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 Date Effluent Concentration limit = 9E-14 uCi/ml BHV-6U Effluent Concentration limit = 2E-14 uCi/ml BHV-6T Effluent Concentration limit = 9E-13 uCi/ml BHV-6R Effluent Concentration limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC limit = SE-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 5/9/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 8/9/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 11/11/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 2/5/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 5/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 8/5/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 11/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 2/6/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 5/5/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 8/11/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.S0E-13 1/5/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 4/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 7/31/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 9/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 12/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 3/29/1999 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.S0E-13 7/3/1999 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.S0E-13 9/27/1999 3.03E-1S 9.00E-14 2.2SE-14 1.37E-1S 2.00E-14 S.00E-1S 8.72E-16 9.00E-13 2.2SE-13 7.SSE-1S 6.00E-13 l.S0E-13 12/28/1999 S.01E-1S 9.00E-14 2.2SE-14 2.89E-1S 2.00E-14 S.00E-1S 1.31E-1S 9.00E-13 2.2SE-13 8.10E-1S 6.00E-13 l.S0E-13 3/30/2000 7.46E-16 9.00E-14 2.2SE-14 S.2SE-16 2.00E-14 S.00E-1S 3.00E-16 9.00E-13 2.2SE-13 7.83E-1S 6.00E-13 l.S0E-13 6/26/2000 S.40E-16 9.00E-14 2.2SE-14 3.S3E-16 2.00E-14 S.00E-1S 6.11E-16 9.00E-13 2.2SE-13 4.83E-1S 6.00E-13 l.S0E-13 9/25/2000 3.7SE-16 9.00E-14 2.2SE-14 2.23E-16 2.00E-14 S.00E-1S 1.91E-16 9.00E-13 2.2SE-13 6.41E-1S 6.00E-13 l.S0E-13 12/26/2000 S.21E-16 9.00E-14 2.2SE-14 3.39E-16 2.00E-14 S.00E-1S 3.28E-17 9.00E-13 2.2SE-13 8.S7E-1S 6.00E-13 1.S0E-13 3/26/2001 1.42E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.1SE-1S 6.00E-13 1.S0E-13 7/2/2001 1.81E-16 9.00E-14 2.2SE-14 1.66E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 l.S0E-13 9/24/2001 3.08E-16 9.00E-14 2.2SE-14 1.01E-16 2.00E-14 S.00E-1S 1.77E-16 9.00E-13 2.2SE-13 8.S9E-1S 6.00E-13 1.S0E-13 12/31/2001 3.31E-16 9.00E-14 2.2SE-14 1.2SE-16 2.00E-14 S.00E-1S 1.09E-16 9.00E-13 2.2SE-13 3.14E-1S 6.00E-13 l.S0E-13 4/1/2002 4.77E-16 9.00E-14 2.2SE-14 2.94E-16 2.00E-14 S.00E-1S 1.96E-16 9.00E-13 2.2SE-13 8.61E-1S 6.00E-13 l.S0E-13 7/1/2002 3.68E-16 9.00E-14 2.2SE-14 4.41E-16 2.00E-14 S.00E-1S 1.76E-16 9.00E-13 2.2SE-13 8.20E-1S 6.00E-13 l.S0E-13 9/30/2002 3.67E-16 9.00E-14 2.2SE-14 S.60E-16 2.00E-14 S.00E-1S 1.80E-16 9.00E-13 2.2SE-13 S.SSE-1S 6.00E-13 l.S0E-13 12/30/2002 1.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 1.67E-16 9.00E-13 2.2SE-13 1.3SE-14 6.00E-13 l.S0E-13 3/31/2003 1.98E-16 9.00E-14 2.2SE-14 1.68E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.77E-1S 6.00E-13 l.S0E-13 6/30/2003 1.18E-16 9.00E-14 2.2SE-14 1.1SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.92E-1S 6.00E-13 l.S0E-13 9/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.30E-1S 6.00E-13 l.S0E-13 12/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.36E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.66E-1S 6.00E-13 l.S0E-13 3/29/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.17E-1S 6.00E-13 l.S0E-13 6/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.SSE-1S 6.00E-13 l.S0E-13 9/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.38E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.22E-14 6.00E-13 l.S0E-13 12/27/2004 1.0SE-16 9.00E-14 2.2SE-14 1.72E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 l.S2E-14 6.00E-13 l.S0E-13 3/28/2005 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.34E-1S 6.00E-13 1.S0E-13 6/29/2005 1.28E-16 9.00E-14 2.2SE-14 1.01E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.8SE-1S 6.00E-13 l.S0E-13 9/26/2005 1.98E-16 9.00E-14 2.2SE-14 S.98E-16 2.00E-14 S.00E-1S 3.SSE-16 9.00E-13 2.2SE-13 1.71E-14 6.00E-13 l.S0E-13 1/3/2006 7.67E-16 9.00E-14 2.2SE-14 2.88E-16 2.00E-14 S.00E-1S 3.60E-1S 9.00E-13 2.2SE-13 4.8SE-14 6.00E-13 l.S0E-13 4/3/2006 2.92E-16 9.00E-14 2.2SE-14 2.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.11E-14 6.00E-13 l.S0E-13 7/3/2006 3.2SE-16 9.00E-14 2.2SE-14 2.36E-16 2.00E-14 S.00E-1S 1.08E-16 9.00E-13 2.2SE-13 1.10E-14 6.00E-13 l.S0E-13 10/2/2006 S.03E-16 9.00E-14 2.2SE-14 1.49E-16 2.00E-14 S.00E-1S 1.19E-16 9.00E-13 2.2SE-13 2.13E-1S 6.00E-13 1.S0E-13 1/1/2007 8.31E-16 9.00E-14 2.2SE-14 2.49E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.70E-14 6.00E-13 l.S0E-13 4/2/2007 S.36E-16 9.00E-14 2.2SE-14 3.1SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.43E-14 6.00E-13 1.S0E-13 7/2/2007 1.08E-1.S 9.00E-14 2.2SE-14 2.18E-16 2.00E-14 S.00E-1S l.S4E-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 l.S0E-13 9/30/2007 3.92E-16 9.00E-14 2.2SE-14 1.02E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.38E-1S 6.00E-13 l.S0E-13 12/31/2007 2.92E-1S 9.00E-14 2.2SE-14 l.SSE-1S 2.00E-14 S.00E-1S 3.16E-16 9.00E-13 2.2SE-13 9.19E-1S 6.00E-13 l.S0E-13 3/31/2008 4.34E-16 9.00E-14 2.2SE-14 3.SlE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.99E-1S 6.00E-13 l.S0E-13 6/3102008 1.88E-1S 9.00E-14 2.2SE-14 9.00E-16 2.00E-14 S.00E-1S 4.04E-16 9.00E-13 2.2SE-13 7.41E-1S 6.00E-13 1.S0E-13 Date Effluent Concentration limit = 9E-14 uCi/ml BHV-6U Effluent Concentration limit = 2E-14 uCi/ml BHV-6T Effluent Concentration limit = 9E-13 uCi/ml BHV-6R Effluent Concentration limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/200B 4.B2E-1S 9.00E-14 2.2SE-14 2.10E-1S 2.00E-14 S.00E-1S L27E-1S 9.00E-13 2.2SE-13 LOOE-14 6.00E-13 LSOE-13 12/31/200B 4.BOE-1S 9.00E-14 2.2SE-14 L70E-1S 2.00E-14 S.00E-1S 1.2SE-1S 9.00E-13 2.2SE-13 1.49E-14 6.00E-13 LSOE-13 3/15/2009 2.77E-1S 9.00E-14 2.2SE-14 L01E-1S 2.00E-14 S.00E-1S 7.B2E-16 9.00E-13 2.2SE-13 6.46E-1S 6.00E-13 LSOE-13 6/15/2009 L41E-16 9.00E-14 2.2SE-14 2.67E-16 2.00E-14 S.00E-1S LBlE-16 9.00E-13 2.2SE-13 S.76E-1S 6.00E-13 LSOE-13 9/15/2009 4.B7E-1S 9.00E-14 2.2SE-14 4.32E-16 2.00E-14 S.00E-1S 2.23E-16 9.00E-13 2.2SE-13 B.9BE-1S 6.00E-13 1.S0E-13 12/15/2009 9.24E-1S 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S L1SE-16 9.00E-13 2.2SE-13 6.44E-1S 6.00E-13 LSOE-13 3/31/2010 9.63E-1S 9.00E-14 2.2SE-14 LB2E-16 2.00E-14 S.00E-1S 2.06E-16 9.00E-13 2.2SE-13 L37E-14 6.00E-13 LSOE-13 6/30/2010 3.62E-1S 9.00E-14 2.2SE-14 3.94E-16 2.00E-14 S.00E-1S 4.B9E-16 9.00E-13 2.2SE-13 4.30E-1S 6.00E-13 LSOE-13 9/30/2010 S.42E-1S 9.00E-14 2.2SE-14 LOBE-IS 2.00E-14 S.00E-1S S.6BE-16 9.00E-13 2.2SE-13 3.9BE-1S 6.00E-13 1.S0E-13 12/31/2010 1.24E-14 9.00E-14 2.2SE-14 L21E-1S 2.00E-14 S.00E-1S LOOE-1S 9.00E-13 2.2SE-13 1.S3E-14 6.00E-13 LSOE-13 4/4/2011 2.70E-1S 9.00E-14 2.2SE-14 4.62E-16 2.00E-14 S.00E-1S 6.S1E-16 9.00E-13 2.2SE-13 L29E-14 6.00E-13 LSOE-13 7/4/2011 3.0lE-1S 9.00E-14 2.2SE-14 7.07E-16 2.00E-14 S.00E-1S S.7SE-16 9.00E-13 2.2SE-13 7.97E-1S 6.00E-13 1.S0E-13 10/3/2011 2.0SE-1S 9.00E-14 2.2SE-14 6.12E-16 2.00E-14 S.00E-1S LBBE-16 9.00E-13 2.2SE-13 9.93E-1S 6.00E-13 LSOE-13 1/3/2012 3.14E-1S 9.00E-14 2.2SE-14 1.09E-1S 2.00E-14 S.00E-1S 7.6SE-16 9.00E-13 2.2SE-13 1.B9E-14 6.00E-13 LSOE-13 fn c: o ",t:: «S '-... c: G) CJ c: o (.) G) :2 CJ :::l c: o "C «S a: CD :> J: m ""F ~ X ..... .-=:l «::; ~~ ~ -1 r-~ .. +== ~>-~ ~. ~ ~ ~ ~ ~~ ~:-.. ~ 4 --.; iIIIo... )~ ~ • - t-!"" ~~ j.o"" ~ ~. ~. t--~P4 ~ ~). .... N ~-~ ~~ • c:;::.. :::~ ~1111.... L1 ~ 4'-~ "0-I... ~41 ~ ~ ;:;; :810 ~ ~ "'14 ~ ... ~ ~~ ~1 .~ ., l~ «: ~ ~-ce:=- ". ~~ b ~ ~ ....~ <0 ,- uJ ~~ I'--,- I W ~ ~Oc/8/0 ~ BOOc/08/6 900c/9c/6 o ,-" C\I -b cOOc/08/6 ~ ....J + <0 C\I 666~/Lc/6C';J E :::J iJ CO a: 966 ~/9/B + o Ct') C\I E :::J 866~/O~/B~ r- + ~ 066~/8~/B~ z E :::J ·c ~ :::> LB6~/6/6 + 17B6 ~/~/O ~ ~B6 ~/Bc/6 1.00E-1 1 1.00E-12 1.00E-13 CD (ij u Cf.I.OOE-14 0> o d 1.00E-1S 1.00E-16 1.00E-17 or-ex:> 0) or-co ~ Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml ~ ex:> 0) or--0r-o I'--ex:> 0) or--~ o 0) 0) or- cY5 or-co C') 0) 0) 0r-o ~ BHV-6 Uranium-Natural Concentrations (uCi/ml) co 0) 0) or--~ ]I ~ ~ 0) 0) 0) or-~ ~ 0) ... Vl ~ ., ~., \ r 'J! \ .... 'A o o 2J £2 0) ~ I \ I 1 ~ T • .tI. • 1 r t6 1 .... J o o ~ ~ 0) 1 • ... o o ~ o £2 0) ~ ~ t I \ ,. \I • \ ....... ~ ~ 0r-o ~ 1.00E-11 1.00E-12 1.00E-13 Q) (ij (,) Cf.1.00E-14 0> o .....J '-'" 1.00E-1S 1.00E-16 1.00E-17 T""" CX) 0) T""" -CX) ~ 0) Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = 8E-14uCi/ml ""'" I'-0 CX) CX) 0) 0) 0) 0) T""" T""" T""" - - - T""" 0) ('f) --T""" 0 0) -CX) ('f) 0) Q') T""" 25 T""" co , , BHV-6 Thorium-230 Concentrations (uCi/ml) CD 0) 0) T""" -~ ~ J\ .... ,. ... "\ .\ 1\ •• ~ . \ .. V\ T \ ~f~ W VAl 'r'¥ ~ 0) 0) 0) T""" r:::: ~ C\J o o ~ f2 0) o o ~ ~ Q') .. ~ /\ .It • \I • o o ~ f2 Q') I v--, • .J.. • ,/\ T ... I • T""" o ~ o 1.00E-11 1.00E-12 1.00E-13 Q) ro () Cf.I .OOE-14 0> o 2- 1.00E-15 1.00E-16 1.00E-17 T"" co Q) T"" -co ~ Q) Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml ~ f"-.. co co Q) Q) T"" T"" - - T"" Q) - - 0 Q) o Q) Q) T"" ?> T"" co ('f) Q) Q) T"" 25 T"" co \ • \ , BHV-6 Radium-226 Concentrations (uCi/ml) (0 Q) Q) T"" -~ ~ Q) Q) Q) T"" r:::: ~ Q) 11" 1\ II \ "'" t '....N\ " , o o ~ ~ ~ I J o o ~ aJ ~ ~ .J.. • T 1\ L.JJ~ o o ~ ~ .... ~ .... T \ , I \I \.1 V ." • T"" o ~ 25 1.00E-11 1.00E-12 1.00E-13 Q) ca <..> Cf.I.OOE-14 0> o d 1.00E-1S 1.00E-16 1.00E-17 or-co 0') or--co ~ 0') Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml ~ I"--co co 0') 0') or-or---0r-O') - -o 0') 0 0') 0') or--(t) 0r--co (t) 0') 0') 25 or--co I I I BHV-6 Lead-210 Concentrations (uCi/ml) <.0 0') 0') or--~ 0') 0') 0') or--I"--~ v .... "I 1\ I ~ A1 \ •• "Y \. \I ~ C\J o o ~ o ~ 0') U • o o ~ ~ 0') .... ~ M ..... J.. o o ~ ~ .... t. ~ I ..... "Y 0r-o ~ ~ o ATTACHMENT C AIR PARTICULATE LABORATORY RESULTS AND QAlQC www.energylab.com Analytical ExcsllsncB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 'Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 ANALYTICAL SUMMARY REPORT December 26,2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11100215 Project Name: 3rd Quarter Air 2011 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 10/5/2011 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C11100215-001 BHV-1 10/03/11 00:00 10/05/11 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C11100215-002 BHV-2 10/03/11 00:00 10/05/11 Filter Sam e As Above C11100215-003 BHV-4 10/03/11 00:00 10/05/11 Filter Same As Above C11100215-004 BHV-5 10/03/11 00:00 10/05/11 Filter Same As Above C11100215-005 BHV-6 10/03/11 00:00 10/05/11 Filter Same As Above C11100215-006 Blank 10/03/11 00:00 10/05/11 Filter Same As Above The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: Digitally signed by Steve Carlston Date: 2011.12.26 15:21 :41 -07:00 Page 1 of 23 www.energylab.com Analytical besl/snell Sines 1952 Ifelena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette Wy 866-686-7175 • Ra id City, SD 888-672-1225 III Colle e Station, IX 888-&90-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Report Date: 12/26/11 Sample Delivery Group: C11100215 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 23 -~] www.energylab.com ~Helena.MT877-472-0711 .BillingS.MT 800-735-4489 • Casper, WY 888-235-0515 Ana/ytical Excel/enceSi~ . Gillette, WY 866-686-7175 • Rapid ~ity, SD 888-672-1225 • College Station, TX 888-690-2218 mGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 26, 2011 PROJECT: 3rd Quarter Air 2011 SAMPLEID: BHV-1 Quarter/Date Sampled Concentration Air Volume Radionuclide ,..CilmL CI1040259-001 natU 9.01E-16 First Quarter 2011 230Th 1.90E-16 Air Volume in mLs 226Ra 3.64E-16 1.35E+ll 210Pb 1.09E-14 Quarter/Date Sampled Concentration Air Volume Radionuclide ,..CilmL CI1070215-001 natu 1.59E-15 Second Quarter 2011 230Th 5.3lE-16 Air Volume in mLs 226Ra 4.99E-16 1.38E+ll 210Pb 8.38E-15 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL CI1100215-001 natu 2.92E-16 Third Quarter 2011 230Th 1.17E-16 Air Volume in mLs 226Ra 6.76E-17 1.24E+ll 210Pb 1.14E-14 +LLD's are from Reg. Guide 4.14 Counting Precision ,..CilmL N/A 2E-17 2E-17 lE-16 Counting Precision ,..CilmL N/A 5E-17 2E-17 2E-16 Counting Precision ,..CilmL N/A 2E-17 lE-17 lE-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC,..CilmL N/A 3E-18 2E-18 8E-17 MDC,..CilmL N/A 4E-18 3E-18 lE-16 MDC,..CilmL N/A 9E-18 6E-18 SE-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL /JCilmL Concentration lE-16 9E-14 1.00E+OO lE-16 3E-14 6.32E-Ol lE-16 9E-13 4.04E-02 2E-15 6E-13 1. 82E+OO L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 l.77E+OO lE-16 3E-14 1. 77E+OO lE-16 9E-13 5.54E-02 2E-15 6E-13 1.40E+OO L.L.D.+ Effluent Cone. * % Effluent ,..CilmL /JCilmL Concentration lE-16 9E-14 3.2SE-Ol lE-16 3E-14 3.89E-Ol lE-16 9E-13 7.SlE-03 2E-15 6E-13 1.9lE+OO Page 3 of 23 EI\ERGY LABORATORIES www.energylab.com Analytical ExcsllsncB Sines 7!152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY .8&&-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Air 2011 C11100215-001 Client Sample ID BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0537 36.3 1420 14 6.7 8.4 1.3 0.7 15 2.7 1.1 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pCilFilter pCi/Filter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pC ilFi Iter Qualifiers RL 0.0003 0.2 Report Date: 12/26/11 Collection Date: 10/03/11 DateReceived: 10/05/11 Matrix: Filter MCL! QCL Method Analysis Date 1 By SW6020 10/11/11 12:281 sml SW6020 10/11/1112:28/sml E909.0 11/04/11 12:271 eli-cs E909.0 11/04/11 12:27 1 eli-cs E909.0 11104/11 12:271 eli-cs E903.0 10/19/1113:16/js E903.0 10/19/11 13:161 js E903.0 10/19/1113:16/js E908.0 11/10/1113:50/dmf E908.0 11/10/11 13:501 dmf E908.0 11/10/11 13:501 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 23 EI\ERGY LABORATORIES www.energylab.com Analytical Excellence Since 1952 r Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 26, 2011 PROJECT: 3rd Quarter Air 2011 SAMPLE ID: BHV-2 QuarterlDate Sampled Radionuclide Concentration Air Volume ,..CilmL C11040259-002 natU 3.79E-16 First Quarter 2011 230Th 4.01E-17 Air Volume in mLs 226Ra 9.11E-17 1.31E+ll 210Pb 1.06E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL C11070215-002 natu 3.07E-16 Second Quarter 2011 230Th 8.54E-17 Air Volume in mLs 226Ra 9.2lE-17 1.38E+11 210Pb 7.21E-15 Counting Precision ,..CilmL N/A 6E-18 8E-18 lE-16 Counting Precision ,..CilmL N/A 1E-17 9E-18 1E-16 QuarterlDate Sampled Concentration Counting Air Volume Radionuclide ,..CilmL C11100215-002 natU 1.17E-16 Third Quarter 2011 230Th 3.04E-17 Air Volume in mLs 226Ra 2.8lE-17 1.24E+ll 210Pb 1.03E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21 0 Precision ,..CilmL N/A 7E-18 7E-18 lE-16 MDC,..CilmL N/A 2E-18 2E-18 8E-17 MDC,..CilmL N/A 3E-18 3E-18 9E-17 MDC,..CilmL N/A 4E-18 6E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 4.2lE-01 1E-16 3E-14 1. 34E-01 1E-16 9E-13 1.01E-02 2E-15 6E-13 1.76E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 3.4lE-01 lE-16 3E-14 2.85E-01 lE-16 9E-13 1.02E-02 2E-15 6E-13 1.20E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration IE-16 9E-14 1.30E-Ol 1E-16 3E-14 1.0 lE-O 1 lE-16 9E-13 3.12E-03 2E-15 6E-13 1.72E+OO Page 5 of 23 EN:RGY LABORATORIES ..,~ Analytical Exes/Jsnca Sines 1!152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 866-686-7175 It Rapid City, SD 888-672-1225 • Col/ege Station, IX 888-690-2218 -M ' www..nergyl'b.com f ,"· -------------------=--------------------------------------------------------- LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Lab ID: C11100215-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES . TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0214 14.5 12S0 13 6.S 3.5 0.9 0.7 3.S 0.S9 0.50 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pCilFilter pCi/Filter pCilFilter pCilFilter pC i/Fi Iter pCilFilter pCilFilter pC ilFi Iter Qualifiers Rl 0.0003 0.2 Report Date: 12/26/11 Collection Date: 10/03/11 DateReceived: 10/05/11 Matrix: Filter MCU QCl Method Analysis Date / By SW6020 10/11/11 12:301 sml SW6020 10/11/11 12:301 sml E909.0 11/04/11 14:421 eli-cs E909.0 11/04/11 14:421 eli-cs E909.0 11/04/11 14:42 1 eli-cs E903.0 10/19/1113:16/js E903.0 10/19/1113:16/js E903.0 10/19/11 13:161 js E90S.0 11/10/11 13:501 dmf E90S.0 11/10/1113:50/dmf E90S.0 11/10/1113:50/dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of23 EN:RGY LABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 26, 2011 PROJECT: 3rd Quarter Air 2011 SAMPLE ID: BHV-4 Quarter/Date Sampled Concentration Air Volume Radionuclide ,..CilmL CI1040259-003 Datu 1.29E-15 First Quarter 2011 230Th 1.40E-16 Air Volume in mLs 226Ra 1.58E-16 1.25E+ll 210Pb 1.11E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL CI1070215-003 Datu 3.30E-15 Second Quarter 2011 230Th 5.44E-16 Air Volume in mLs 226Ra 4.18E-16 1. 17E+11 210Pb 8.26E-15 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL Cl1100215-003 Datu 1.32E-15 Third Quarter 2011 230Th 7.89E-16 Air Volume in mLs 226Ra 1.28E-16 1.38E+11 210Pb 1.18E-14 +LLD's are from Reg. Guide 4.14 Counting Precision ,..CilmL N/A 2E-17 lE-17 lE-16 Counting Precision ,..CilmL N/A 5E-17 2E-17 2E-16 Counting Precision ,..CilmL N/A 8E-17 lE-17 lE-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC,..CilmL N/A 3E-18 3E-18 8E-17 MDC,..CilmL N/A 6E-18 4E-18 lE-16 MDC,..CilmL N/A 8E-18 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 1.44E+00 lE-16 3E-14 4.66E-Ol lE-16 9E-13 1.75E-02 2E-15 6E-13 1.86E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.66E+00 lE-16 3E-14 1.8lE+00 lE-16 9E-13 4.65E-02 2E-15 6E-13 1.38E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 1. 46E+00 lE-16 3E-14 2.63E+00 lE-16 9E-13 1.43E-02 2E-15 6E-13 1.96E+00 Page 7 of 23. EN:RGY l.ABORATORIES www.energylab.com Analytical ExcsllBIICfI Sil1cs 1952 Helena, MT 877-472-0711 11 Billings, MT 800-735-4489 III Casper, WY 888-235-0515 Giliette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Lab 10: C11100215-003 Client Sample 10 BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOe Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.269 1S2 1620 15 6.S 17.7 1.S 0.7 109 11 1.1 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pCilFilter pCi/Filter pCilFilter pC i/Fi Iter pCilFilter pC ilFi Iter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 12/26/11 Collection Date: 10/03/11 DateReceived: 10/05/11 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 10/11/11 12:321 sml SW6020 10/11/11 12:321 sml E909.0 11/04/11 21 :27 1 eli-cs E909.0 11/04/11 21 :27 1 eli-cs E909.0 11/04/11 21 :27 1 eli-cs E903.0 10/19/1113:16/js E903.0 10/19/11 13:16 1 js E903.0 10/19/11 13:161 js E90S.0 11/10/1113:50/dmf E90S.0 11/10/11 13:501 dmf E90S.0 11/10/11 13:501 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. .Page 8 of 23 EN:RGY LABORATORIES ,; "' www.energylab.com ( Analytical Excellence Since 1952 J Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 26, 2011 PROJECT: 3rd Quarter Air 2011 SAMPLE ID: BHV-S QuarterlDate Sampled Radionuclide Concentration Air Volume ,..CilmL CI1040259-004 natu 3.20E-15 First Quarter 2011 230Th 8.89E-16 Air Volume in mLs 226Ra l.10E-15 1.32E+ll 210Pb 1.48E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL CI1070215-004 natU 6.98E-15 Second Quarter 2011 230Th 2.03E-15 Air Volume in mLs 226Ra 2.52E-15 1.38E+ll 210Pb 1.08E-14 Counting Precision ,..CilmL N/A 8E-17 3E-17 2E-16 Counting Precision ,..CilmL N/A 2E-16 5E-17 2E-16 QuarterlDate Sampled Concentration Counting Air Volume Radionuclide ,..CilmL C 111 00215-004 natU 3.1lE-15 Third Quarter 2011 230Th l.14E-15 Air Volume in mLs 226Ra 5.75E-16 1.35E+ll 210Pb 1.4lE-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O Precision ,..CilmL N/A lE-16 3E-17 lE-16 MDC,..CilmL N/A 3E-18 2E-18 7E-17 MDC,..CilmL N/A 6E-18 3E-18 8E-17 MDC,..CilmL N/A 2E-17 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.56E+00 lE-16 3E-14 2.96E+00 lE-16 9E-13 1.22E-01 2E-15 6E-13 2.46E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 7.75E+00 lE-16 3E-14 6.76E+00 lE-16 9E-13 2.80E-Ol 2E-15 6E-13 1.8lE+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.46E+00 lE-16 3E-14 3.80E+00 lE-16 9E-13 6.38E-02 2E-15 6E-13 2.36E+00 Page 9 of 23 ~-----------------------------------------------------www.energylab.com ( Analytical ExcsllsncB Sines 1952 J .. Helena, MT 877-472-0711 • Billings, !'AT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Air 2011 C11100215-004 Client Sample 10 BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.620 420 1910 16 6.7 77.5 3.6 0.7 154 18 3.2 MOC -Minimum detectable concentration Units mgtfilter pC ilFi Iter pCilFilter pCilFilter pC i/Fi Iter pC ilFi Iter pCilFilter pC ilFi Iter pC ilFi Iter pCilFilter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 12/26/11 Collection Date: 10/03/11 DateReceived: 10/05/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 10/11/11 12:331 sml SW6020 10/11/11 12:331 sml E909.0 11/04/11 23:41 1 eli-cs E909.0 11/04/11 23:41 1 eli-cs E909.0 11104/11 23:41 1 eli-cs E903.0 10/19/11 13:161 js E903.0 10/19/1113:16/js E903.0 10/19/11 13:161 js E908.0 11/10/11 13:501 dmf E908.0 11/10/1113:50/dmf E908.0 11110/11 13:501 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Pag~ 10 of 23 EN:RGY LABORATORIES ~._.-;-l1N www.energylab.comHelena.MT877-472-0711 ·Biliings.MT 800-735-4489 • Casper, WY 888-235-0515 .. -~ Analytical Exceflence Since 1952 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 ~~============~~~----~----------~--~--.----------~--~-------- mGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 26, 2011 PROJECT: 3rd Quarter Air 2011 SAMPLE ID: BHV-6 QuarterlDate Sampled Radionuclide Concentration Air Volume ,..CilmL C11040259-005 natu 2.70E-15 First Quarter 2011 230Th 4.62E-16 Air Volume in mLs 226Ra 6.51E-16 1.32E+ll 2IOPb 1.29E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL C11070215-005 natu 3.0lE-15 Second Quarter 2011 230Th 7.07E-16 Air Volume in mLs 226Ra 5.75E-16 1.38E+ll 2IOPb 7.97E-15 Counting Precision ,..CilmL N/A 4E-17 2E-17 1E-16 Counting Precision ,..CilmL N/A 7E-17 2E-17 lE-16 QuarterlDate Sampled Concentration Counting Air Volume Radionuclide ,..CilmL Cll100215-005 natu 2.05E-15 Third Quarter 2011 230Th 6.12E-16 Air Volume in mLs 226Ra 1.88E-16 1.35E+ll 2IOPb 9.93E-15 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O Precision ,..CilmL N/A 8E-17 2E-17 lE-16 MDC,..CilmL N/A 3E-18 2E-18 7E-17 MDC,..CilmL N/A 5E-18 3E-18 9E-17 MDC,..CilmL N/A 1E-17 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.00E+00 lE-16 3E-14 1. 54E+00 lE-16 9E-13 7.24E-02 2E-15 6E-13 2. 14E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 3.35E+00 1E-16 3E-14 2.36E+00 1E-16 9E-13 6.39E-02 2E-15 6E-13 1.33E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 2.28E+00 1E-16 3E-14 2.04E+00 1E-16 9E-13 2.09E-02 2E-15 6E-13 1.65E+00 Page 11 of 23 www.energylab.com . : ... . Helena, MT 877-472-0711 • Billings, I'dT 800-735-4489 -Casper, WY 888-235-0515 EN:RGY L.A60RATORIES Analytical ExcsllBflCIl Sines 1!152 r ----. . ; -. Gillette, wv86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Lab ID: C11100215-005 Client Sample ID BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.409 277 1340 14 6.S 25.4 2.1 0.7 83 10 1.5 MOC -Minimum detectable concentration Units mg/filter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter Qualifiers Rl 0.0003 0.2 Report Date: 12/26/11 Collection Date: 10/03/11 DateReceived: 10/05/11 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 10/11/11 12:391 sml SW6020 10/11/11 12:391 sml E909.0 11/05/11 01 :56 1 eli-cs E909.0 11/05/11 01 :561 eli-cs E909.0 11/05/11 01 :56 1 eli-cs E903.0 10/19/1113:16/js E903.0 10/19/11 13:161 js E903.0 10/19/11 13:161 js E90S.0 11/10/11 13:501 dmf E90S.0 11/10/11 13:501 dmf E90S.0 11/10/11 13:501 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 23 ------~lN www.energylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 t~ Analytical Excellence Since 1952 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 EN:RGY LABORATORIES ====~~==========~~------~--------~--~----------~--~------- IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 26, 2011 PROJECT: 3rd Quarter Air 2011 SAMPLE ID: Blank Quarter/Date Sampled Radionuclide Concentration Air Volume pCilmL C11040259-006 natu 1.22E-17 First Quarter 2011 230Th 5.84E-19 Air Volume in mLs 226Ra 5.16E-18 1.36E+11 210Pb -4.5lE-17 Counting Precision pCilmL N/A 2E-18 2E-18 4E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. Quarter/Date Sampled Concentration Counting Air Volume Radionuclide pCilmL Precision pCilmL C11070215-006 natu l.05E-17 N/A Second Quarter 2011 230Th 6.69E-18 2E-18 Air Volume in mLs 226Ra -4.89E-20 2E-18 1.36E+11 210Pb -8.89E-18 5E-17 Note: ThiS sample uses 136,000,000 L of air volume for comparison purposes. Quarter/Date Sampled Concentration Counting Radionuclide Precision Air Volume pCilmL pCilmL C11100215-006 natu 2.42E-17 N/A Third Quarter 2011 230Th 5.37E-18 3E-18 Air Volume in mLs 226Ra 7.16E-18 4E-18 1.36E+11 210Pb l.44E-17 3E-17 Note: ThiS sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCpCilmL N/A 3E-18 3E-18 7E-17 MDCpCilmL N/A 2E-18 3E-18 9E-17 MDCpCilmL N/A 3E-18 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 1.35E-02 lE-16 3E-14 l.95E-03 lE-16 9E-13 5.73E-04 2E-15 6E-13 -7.5lE-03 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration 1E-16 9E-14 1.17E-02 lE-16 3E-14 2.23E-02 1E-16 9E-13 -5.43E-06 2E-15 6E-13 -1.48E-03 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration 1E-16 9E-14 2.68E-02 1E-16 3E-14 1.79E-02 1E-16 9E-13 7.96E-04 2E-15 6E-13 2.40E-03 Page 13 of 23 EN:RGY LABORATORIES www.energylab.com AflBlytical ExesllBflCII SiRes 1!152 r - .. Helena, MT 877-472-0711 • Billings, MY 800-735-4489 • Casper, WY 888-235-0515 . Gillette, WY 866-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Air 2011 C11100215-006 Client Sample 10 Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0049 3.3 2.0 4.1 6.S 1 0.6 0.7 0.73 0.39 O.4S MOC -Minimum detectable concentration Units mg/filter pCVFilter pCVFilter pCVFilter pC i/Fi Iter pC VFi Iter pCVFilter pCVFilter pCVFilter pCVFilter pC VFi Iter Report Date: 12/26/11 Collection Date: 10/03/11 DateReceived: 10/05/11 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date 1 By 0.0003 SW6020 10/11/11 12:401 sml 0.2 SW6020 10/11/11 12:401 sml U E909.0 11/05/11 04:11 1 eJi-cs E909.0 11/05/11 04:11 1 eli-cs E909.0 11/05/11 04:11 1 eli-cs E903.0 10/19/1113:16/js E903.0 10/19/1113:16/js E903.0 10/19/1113:16/js E90S.0 11/10/11 13:501 dmf E90S.0 11/10/11 13:501 dmf E90S.0 11/10/11 13:501 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 14 of 23 EI'ERGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 .-Casper, WY 888-235-0515 Gillette, WY .866-686-7175 • Rapid City, sa 888-672-1225 • College Station, IX 888-&90-2218 LABORATORIES Analytical fxcsllsncs Sines 1852 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Analyte Count Result Units Method: E903.0 Sample 10: C11100215-004AMS Radium 226 Sample 10: C11100215-004AMSO Radium 226 Sample 10: LCS-31467 Radium 226 Sample 10: MB-31467 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike 135 pCi/Filter Sample Matrix Spike Duplicate 135 pCilFilter Laboratory Control Sample 10.2 pCilFilter Method Blank -0.2 pCilFilter 0.1 pCilFilter 0.3 pCi/Filter Report Date: 12/26/11 Work Order: C11100215 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_111 013A 97 70 130 Run: BERTHOLD 770-2_111013A 97 70 130 0.1 Run: BERTHOLD 770-2_111 013A 87 70 130 Run: BERTHOLD 770-2_111 013A NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: R152310 10/19/11 13:16 10/19/11 13:16 20.4 10/19/11 14:53 10/19/11 14:53 U Page 15 of 23 EN:RGY LABORATORIES Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Helena, MT 877-472-0711 • Billings, MT 800-735-448S -Casper, WY 888-235-0515 Gillette, WY 866-686,.7175 ,. Rapid City, SD 888-672-1225 " College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 12/26/11 Work Order: C11100215 Analyte Count Result Units RL O/oREC Low Limit High Limit RPO RPOLimit Qual Method: E908.0 Sample 10: LCS-31467 Thorium 230 Sample 10: M 8-31467 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Sample 10: C11100389-002FMS Thorium 230 Sample 10: C11100389-002FMSO Thorium 230 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Laboratory Control Sample 9.68 pCi/Filter Method Blank 0.1 pCilFilter 0.09 pCi/Filter 0.1 pCi/Filter Sample Matrix Spike 9.5 pCi/L Sample Matrix Spike Duplicate 10 pCi/L Run: ALPHANAL YST _111107 A 98 70 130 Run: ALPHANAL YST _111107 A Run: ALPHANAL YST _111107 A 97 70 130 Run: ALPHANALYST _111107A 103 70 130 7.7 ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: R153165 11/10/11 13:50 11/10/1113:50 U 11/10/1113:50 11/10/1113:50 31.7 Page 16 of 23 -----~-===== ----~------------.--------------------------------------EN:RGY www.energylab.com Helena, MT 877-472-0711 111 Billings, MT 800-735-4489 111 Gasper, WY 888-235-0515 Gilleti:e, WY866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-&90-2218 LASORATORIES Analytical Excsl18llCB Sines 1952 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 Analyte Count Result Units Method: E909.0 Sample 10: C111 00215-002AM SO Sample Matrix Spike Duplicate Lead 210 2900 pCilFilter Sample 10: C11100215-002AMS Sample Matrix Spike Lead 210 3030 pCilFilter Sample 10: LCS-15018 Laboratory Control Sample Lead 210 518 pCi/Filter Sample 10: MB-15018 3 Method Blank Lead 210 -0.1 pCi/Filter Lead 210 precision (±) 4 pCi/Filter Lead 210 MDC 7 pCi/Filter Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC 96 103 92 Report Date: 12/26/11 Work Order: C11100215 Low Limit High Limit RPO RPOLimit Qual Batch: T _15018 Run: SUB-T42787 11/04/1119:12 70 130 4.1 12.4 Run: SUB-T42787 11/04/11 16:57 70 130 Run: SUB-T42787 11/04/11 10:13 70 130 Run: SUB-T42787 11/04/11 07:58 U ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 17 of 23 EN:RGY LABORATORIES www.energylab.com ~--Helena.MT877-472-0111 .Billin~~ MT 800-735-4489 11 Casper, 'NY 888-235-0515 AnalyticalExcsllsncsSincs 19S2 .. J; .•.. .. Gillette, WY 866-686-7175 . Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 Client: Denison Mines USA Corp Project: 3rd Quarter Air 2011 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 12/26/11 Work Order: C11100215 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW6020 Batch: 31467 Sample 10: MB-31467 Method Blank Run: ICPMS4-C_111010A 10/10/11 15:43 Uranium 3E-05 mglfilter Sample 10: LCS2-31467 Laboratory Control Sample Run: ICPMS4-C_111 01 OA 10/10/11 15:44 Uranium 0.116 mglfilter 0.00030 115 85 115 Sample 10: C111 0021S-006AM S Sample Matrix Spike Run: ICPMS4-C_111010A 10/10/11 16:34 Uranium 0.0543 mglfilter 0.00030 100 75 125 Sample 10: C111 0021S-006AM SO Sample Matrix Spike Duplicate Run: ICPMS4-C_111 01 OA 10/10/11 16:35 Uranium 0.0533 mglfilter 0.00030 98 75 125 1.9 20 Method: SW6020 Sample 10: ICV Uranium 2 Initial Calibration Verification Standard Analytical Run: ICPMS4-C_111 011 A 10/11/1112:00 0.0482 mg/L Uranium, Activity 32.7 pC ilL Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.00030 0.20 96 90 90 110 110 NO -Not detected at the reporting limit. Page 18 of23 EN:RGY LABORATORIES www.energylab.com Analytical ExCSUIHlCS Sincs '952 I ) Helena, MT 877-472-0711 .. Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 .. Rapid City, SD 888-672-1225 .. College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C11100215 Login completed by: Kristy Gisse Reviewed by: BL2000\kschroeder Reviewed Date: 10/6/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes [{1 Yes 0 Yes 0 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 'C NA Yes 0 Yes 0 Date Received: 10/5/2011 No 0 No 0 No 0 No 0 No 0 NoO No 0 No 0 No 0 No 0 No 0 No 0 Received by: ca Carrier UPS-NDA name: Not Present 0 Not Present [{1 Not Present [{1 No VOA vials submitted [{1 Not Applicable [{1 Page 19 of 23 -u Ol co ('I) N o '0 ...., N eN 1·~g({"7 '.fMI'MM' Chain of Custody and Analytical Request Record PLEASE PRINT (Provide as much informationa~p_Q~sible.) Page~Of~ co~~e: ~ , )'AfJi,oAi (f}1A£C Project N~rrye, ~WS, per.mit, Etc. _ I Sample Origin I' 3M eJAA-d.Jr.d Ill'" ::!'tJJ/ State: I/ti EPA/State Compliance: Yes 1J No D Email: Report ~ ~~resse,~ g-O'j . fdhnd,d?, 1A.1 ~LfSJ1 Contact ~e: -" 11 ~PhonetFax: _t1J/AY1_J{J~ IBS h1X'/Z~/ Sampler: (Please Print) k1rl ~,d Invoice AdCfreSs: • ~ (' <;L1tM'L Invoice CTnfact &f1tione: -I ~~-- Purchase Order: QuotMSottle Order: Special RePort/Formats: Dow D EO OlE OT(Electronic Data) $: c ..... ~oc:n~ ~m:201"" ._> -Q) ~(I)~ ~~ LilllW.i\11 W®U® OO~®(!D[§@L1[g[Q) • c gl R w I Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page uP:;: AJDA= Cooler ID(s): ~X o POTWMlWTP Format: ___ _ o State: o LEVEL IV ---- 83:~ ~ C) 'O«~I~I~ 0.(1) 0 .... >-=>1= CI F-> (I) , ~ .... QjjB c:::'£ ::lw .... --> zc..<I~El E ~I ~ o Other: ----D NELAC ~SAM-PLE-ID-ENT-IFICA-TIO-N~~--~~~~·~ lName, Location, Interval, etc.) ~ ~ J ~ ~R#t/-I Io/~I \ 115-A 1~lt I AI)( 2lllil,2 1-'j-'"I \ I 1 I(IAI~IX ~IN / ~ 1 ( 1 I 1 I 1)( I ~ I X IX. 1fJ1t£-b 1 J 1 I , II ~ 1;( l'x I ~ fjjy~ ~ 1 tI 1 I \ ( I ~ I~ I )< I X ~K __ r'~%3"11 \ 1/5-1} LXJxlx IX 7' \ I ~ I' 8 9 10 I.. Custody "C Comments: 0 C .:: e I U co l-E « :l W ~ I 5 w co en "C c co Ci5 I H Receive<:! by (print): OatefTime: ",,,,,;p;JJifo C L"""'o On Ice: Y~ Custody Seal r On Bottle On Cooler N Intact Y N Signature Y N Match , ~ ~~ ~ II c.. , I J {)t)~/5 1<::::::1 ~ ~ I~ I~ CO) I~ ~ Signafure: Record Received by (print): OatefTime: Signature: MUSTbe~--------------------------------~~~~~ __ ~~~ ______ -.~~ ____ ~ Signed Sample Disposal: Return to Client: Lab Disposal: 9) ;r In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information. downloadable fee schedule, forms, and links. WRGY LABORATORIES February 14, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 www.energylab.com Analytical fxul18llcII Sines 1952 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO' 888-672-1225 • College Station, TX 888-690-2218 ANALYTICAL SUMMARY REPORT Workorder No.: C12010190 Project Name: 4th Quarter Air 2011 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 1/6/2012 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C12010190-001 BHV-1 01/03/12 00:00 01/06/12 Filter C12010190-002 BHV-2 01/03/1200:0001/06/12 Filter C12010190-003 BHV-4 01/03/1200:0001/06/12 Filter C12010190-004 BHV-5 01/03/1200:0001/06/12 Filter C12010190-005 BHV-6 01/03/1200:00 01/06/12 Filter C12010190-006 Blank 01/03/1200:0001/06/12 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic Same As Above Same As Above Sam e As Above Same As Above Same As Above The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: a/'" T'{;6~~~ Interim Branch Manager Digitally signed by Steve Carlston Date: 2012.02.14 18: 12:32 -07:00 Page 1 of 22 www.energylab.com Analytiul Excs/lenclI SiRCS 7152 Helena, MT B77~472-0711 . Billings, MT 800~735~4489 . Casper, WY 8S8-235~0515 Gillette Wy 866-686-7175 • Ra id Ci ,SD 888-672-1225 (I Colle e Station, IX 888-690-221S CLIENT: Denison Mines USA Corp Project: 4th Quarter Air 2011 Report Date: 02/14/12 Sample Delivery Group: C12010190 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1115 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 14,2012 PROJECT: 4th Quarter Air 2011 SAMPLEID: BHV-1 Quarter/Date Sampled Concentration Air Volume Radionuclide ,..CilmL C11040259-001 natU 9.0lE-16 First Quarter 2011 230Th 1.90E-16 Air Volume in mLs 226Ra 3.64E-16 1.35E+ll 210Pb 1.09E-14 Quarter/Date Sampled Concentration Air Volume Radionuclide ,..CilmL CI1070215-001 natU 1.59E-15 Second Quarter 2011 230Th 5.3lE-16 Air Volume in mLs 226Ra 4.99E-16 1.38E+ll 210Pb 8.38E-15 Quarter/Date Sampled Concentration Air Volume Radionuclide ,..CilmL CI1100215-001 natU 2.92E-16 Third Quarter 2011 230Th 1.17E-16 Air Volume in mLs 226Ra 6.76E-17 1.24E+ll 210Pb 1.14E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL C 120 1 0 190-00 1 natU 6.73E-16 Fourth Quarter 2011 230Th 1.19E-16 Air Volume in mLs 226Ra 8.58E-17 1.38E+ll 210Pb 1.73E-14 +LLD's are from Reg. Guide 4.14 Counting Precision ,..CilmL N/A 2E-17 2E-17 lE-16 Counting Precision ,..CilmL N/A 5E-17 2E-17 2E-16 Counting Precision ,..CilmL N/A 2E-17 lE-17 IE-16 Counting Precision ,..CilmL N/A 2E-17 8E-18 lE-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC,..CilmL N/A 3E-18 2E-18 8E-17 MDC,..CilmL N/A 4E-18 3E-18 lE-16 MDC,..CilmL N/A 9E-18 6E-18 5E-17 MDC,..CilmL N/A 8E-18 3E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 1.00E+00 lE-16 3E-14 6.32E-01 1E-16 9E-13 4.04E-02 2E-15 6E-13 1.82E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 l.77E+OO lE-16 3E-14 l.77E+OO lE-16 9E-13 5.54E-02 2E-15 6E-13 1.40E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.25E-Ol IE-16 3E-14 3.89E-Ol 1E-16 9E-13 7.5lE-03 2E-15 6E-13 1.9IE+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 7.48E-Ol lE-16 3E-14 3.96E-01 lE-16 9E-13 9.54E-03 2E-15 6E-13 2.88E+00 Page 3 of 22 -----llfl EN:RGY LABORATORIES www.energylab.com Analytical Exes/fBl/cll Sil1Clll952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Lab 10: C12010190-001 Client Sample 10 BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.137 92.9 23S0 19 6.3 11.S 1.2 0.4 16 3.0 1.1 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 02/14/12 Collection Date: 01/03/12 DateReceived: 01/06/12 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 01/13/1217:051 sml SW6020 01/13/1217:051 sml E909.0 02/03/1220:541 eli-cs E909.0 02/03/1220:541 eli-cs E909.0 02/03/1220:541 eli-cs E903.0 01/20/1213:251 trs E903.0 01/20/1213:251 trs E903.0 01/20/1213:251 trs E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf E908.0 01/17/12 09:091 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 14,2012 PROJECT: 4th Quarter Air 2011 SAMPLE ID: BHV-2 Quarter/Date Sampled Concentration Air Volume Radionuclide J,lCilmL C11040259-002 natu 3.79E-16 First Quarter 2011 230Th 4.01E-17 Air Volume in mLs 226Ra 9.11E-17 l.3lE+ll 2\OPb l.06E-14 Quarter/Date Sampled Concentration Air Volume Radionuclide J,lCilmL C11070215-002 natu 3.07E-16 Second Quarter 2011 230Th 8.54E-17 Air Volume in mLs 226Ra 9.2lE-17 1.38E+ll 2\OPb 7.2lE-15 Quarter/Date Sampled Concentration Air Volume Radionuclide J,lCilmL C 111 00215-002 natu l.17E-16 Third Quarter 2011 230Th 3.04E-17 Air Volume in mLs 226Ra 2.8lE-17 1.24E+l1 2\OPb l.03E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume J,lCilmL C 120 1 0190-002 natu 3.65E-16 Fourth Quarter 2011 230Th 2.72E-17 Air Volume in mLs 226Ra 4.54E-17 1.38E+l1 2\OPb l.58E-14 +LLD's are from Reg. Guide 4.14 Counting Precision J,lCilmL N/A 6E-18 8E-18 lE-16 Counting Precision J,lCilmL N/A lE-17 9E-18 lE-16 Counting Precision J,lCilmL N/A 7E-18 7E-18 lE-16 Counting Precision J,lCilmL N/A 7E-18 6E-18 lE-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJ,lCilmL N/A 2E-18 2E-18 8E-17 MDCJ,lCilmL N/A 3E-18 3E-18 9E-17 MDCJ,lCilmL N/A 4E-18 6E-18 5E-17 MDCJ,lCilmL N/A 4E-18 3E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent J,lCilmL J,lCilmL Concentration lE-16 9E-14 4.2lE-01 lE-16 3E-14 l.34E-01 lE~16 9E-13 l.01E-02 2E-15 6E-13 1.76E+00 L.L.D.+ Effluent Cone. * % Effluent J,lCilmL J,lCilmL Concentration lE-16 9E-14 3.41E-Ol lE-16 3E-14 2.85E-Ol lE-16 9E-13 l.02E-02 2E-15 6E-13 1.20E+00 L.L.D.+ Effluent Cone. * % Effluent J,lCilmL J,lCilmL Concentration lE-16 9E-14 1.30E-Ol lE-16 3E-14 l.OlE-01 lE-16 9E-13 3. 12E-03 2E-15 6E-13 l.72E+OO L.L.D.+ Effluent Cone. * % Effluent J,lCilmL J,lCilmL Concentration lE-16 9E-14 4.06E-Ol lE-16 3E-14 9.06E-02 1E-16 9E-13 5.04E-03 2E-15 6E-13 2.63E+00 Page 5 of 22 www.energylab.com Analytical ExeslfsncB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Gasper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 LablD: C12010190-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES . TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0743 50.3 2170 1S 6.4 6.3 0.9 0.4 3.7 0.91 0.54 MDC -Minimum detectable concentration Units mglfilter pCVFilter pCVFilter pCVFilter pCi/Filter pCVFilter pCVFilter pCVFilter pCVFilter pC VFi Iter pCVFilter Qualifiers Rl 0.0003 0.2 Report Date: 02/14/12 Collection Date: 01/03/12 DateReceived: 01/06/12 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 01/13/1217:0S/sml SW6020 01/13/1217:0S/sml E909.0 02/03/12 22:59 1 eli-cs E909.0 02/03/1222:591 eli-cs E909.0 02103/12 22:591 eli-cs E903.0 01/20/12 13:251 trs E903.0 01/20/12 13:251 trs E903.0 01/20/12 13:251 trs E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 14,2012 PROJECT: 4th Quarter Air 2011 SAMPLE ID: BHV-4 QuarterlDate Sampled Concentration Radionuclide Air Volume ,..CilmL C11040259-003 nalU 1.29E-15 First Quarter 2011 230Th 1.40E-16 Air Volume in mLs 226Ra 1.58E-16 1.25E+11 2!OPb 1.11E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume ,..CilmL Cll070215-003 nalU 3.30E-15 Second Quarter 2011 230Th 5.44E-16 Air Volume in mLs 226Ra 4.18E-16 1. 17E+ 11 2!OPb 8.26E-15 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL CI1100215-003 nalU 1.32E-15 Third Quarter 2011 230Th 7.89E-16 Air Volume in mLs 226Ra 1.28E-16 1.38E+11 2!OPb 1.18E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume ,..CilmL C12010190-003 nalU 1.04E-15 Fourth Quarter 2011 230Th 3.25E-16 Air Volume in mLs 226Ra 2.28E-16 1.38E+ll 2!OPb 1.14E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O Counting Precision MDC,..CifmL ,..CilmL N/A N/A 2E-17 3E-18 lE-17 3E-18 lE-16 8E-17 Counting Precision MDC,..CifmL ,..CilmL N/A N/A 5E-17 6E-18 2E-17 4E-18 2E-16 lE-16 Counting Precision MDC,..CifmL ,..CilmL N/A N/A 8E-17 8E-18 lE-17 5E-18 1E-16 5E-17 Counting Precision MDC,..CifmL ,..CilmL N/A N/A 4E-17 7E-18 lE-17 3E-18 lE-16 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 1.44E+00 lE-16 3E-14 4.66E-01 lE-16 9E-13 1.75E-02 2E-15 6E-13 1. 86E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.66E+00 lE-16 3E-14 1.8lE+00 lE-16 9E-13 4.65E-02 2E-15 6E-13 1.38E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CifmL ,..CilmL Concentration 1E-16 9E-14 1.46E+00 lE-16 3E-14 2.63E+OO 1E-16 9E-13 1.43E-02 2E-15 6E-13 1.96E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 1.16E+OO lE-16 3E-14 1.08E+00 1E-16 9E-13 2.54E-02 2E-15 6E-13 1. 89E+00 Page 7 of 22 WRGY LABORATORIES :~ www.energylab.com Analytical best/BIles Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 -Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Lab ID: C12010190-003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.212 144 1570 15 6.4 31.5 1.9 0.4 45 5.5 0.96 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pCilFilter pC i/Fi Iter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 02/14/12 Collection Date: 01/03/12 DateReceived: 01/06/12 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 01/13/12 17:101 sml SW6020 01/13/1217:10/sml E909.0 02/04/1201 :041 eli-cs E909.0 02/04/1201 :04 1 eli-cs E909.0 02104/12 01 :041 eli-cs E903.0 01/20/1215:0S/trs E903.0 01/20/12 15:0S 1 trs E903.0 01/20/12 15:0S 1 trs E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 mGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 14,2012 PROJECT: 4th Quarter Air 2011 SAMPLE ID: BHV-5 QuarterlDate Sampled Concentration Air Volume Radionuclide pCilmL CII040259-004 natU 3.20E-15 First Quarter 2011 230Th 8.89E-16 Air Volume in mLs 226Ra 1.10E-15 1.32E+ll 210Pb 1.48E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide pCilmL CI1070215-004 natu 6.98E-15 Second Quarter 2011 230Th 2.03E-15 Air Volume in mLs 226Ra 2.52E-15 1.38E+ll 210Pb 1.08E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide pCilmL C 11100215-004 natu 3.11E-15 Third Quarter 2011 230Th 1.14E-15 Air Volume in mLs 226Ra 5.75E-16 1.35E+ll 210Pb 1.41E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume pCilmL C12010190-004 natu 4.44E-15 Fourth Quarter 2011 230Th 2.14E-15 Air Volume in mLs 226Ra 1.53E-15 1.30E+ll 210Pb 2.05E-14 +LLD's are from Reg. Guide 4.14 Counting Precision pCilmL N/A 8E-17 3E-17 2E-16 Counting Precision pCilmL N/A 2E-16 5E-17 2E-16 Counting Precision pCilmL N/A lE-16 3E-17 lE-16 Counting Precision pCilmL N/A 2E-16 3E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCpCilmL N/A 3E-18 2E-18 7E-17 MDCpCilmL N/A 6E-18 3E-18 8E-17 MDCpCilmL N/A 2E-17 5E-18 5E-17 MDCpCilmL N/A 2E-17 3E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 3.56E+00 lE-16 3E-14 2.96E+00 lE-16 9E-13 1.22E-Ol 2E-15 6E-13 2.46E+00 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 7.75E+00 lE-16 3E-14 6.76E+00 lE-16 9E-13 2.80E-Ol 2E-15 6E-13 1.8lE+00 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 3.46E+00 lE-16 3E-14 3.80E+00 lE-16 9E-13 6.38E-02 2E-15 6E-13 2.36E+00 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 4.94E+00 lE-16 3E-14 7. 12E+00 lE-16 9E-13 1.70E-Ol 2E-15 6E-13 3.42E+00 Page 9 of 22 ----E RGY LABORATORIES rE~ .~ wwwl'nergylab.com f ~.~ ArI8lytical ExesllsnCfJ Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Gasper, WY 888j 235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Lab 10: C12010190-004 Client Sample 10 BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.853 578 2670 20 6.4 199 4.5 0.4 278 27 3.1 MDC -Minimum detectable concentration Units mg/filter pCVFilter pCVFilter pCVFilter pCi/Filter pCVFilter pCi/Filter pC VFi Iter pCVFilter pCVFilter pCVFilter Report Date: 02/14/12 Collection Date: 01/03/12 DateReceived: 01/06/12 Matrix: Filter MCU Qualifiers Rl QCl Method Analysis Date / By D D 0.001 SW6020 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. ND -Not detected at the reporting limit. D -Rl increased due to sample matrix. 02/13/12 19:29/ sml 02113/1219:291 sml 02/04/1203:091 eli-cs 02/04/1203:091 eli-cs 02/04/1203:091 eli-cs 01/20/1215:081 trs 01/20/1215:081 trs 01/20/1215:08/trs 01/17/1209:091 dmf 01/17/1209:09/ dmf 01/17/1209:091 dmf Page 10 of 22 www.energylab.com Ana/ftical ExceUence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 14,2012 PROJECT: 4th Quarter Air 2011 SAMPLE ID: BHV-6 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL C11040259-005 natu 2.70E-15 First Quarter 2011 230Th 4.62E-16 Air Volume in mLs 226Ra 6.5lE-16 1.32E+ll 210Pb 1.29E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL C11070215-005 natu 3.01E-15 Second Quarter 2011 230Th 7.07E-16 Air Volume in mLs 226Ra 5.75E-16 1.38E+ll 210Pb 7.97E-15 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL C11100215-005 natu 2.05E-15 Third Quarter 2011 230Th 6.12E-16 Air Volume in mLs 226Ra 1.88E-16 1.35E+ll 210Pb 9.93E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume ,..CilmL C12010190-005 natu 3.14E-15 Fourth Quarter 2011 230Th 1.09E-15 Air Volume in mLs 226Ra 7.65E-16 1.38E+ll 210Pb 1.89E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Counting Precision MDC,..CilmL ,..CilmL N/A N/A 4E-17 3E-18 2E-17 2E-18 lE-16 7E-17 Counting Precision MDC,..CilmL ,..CilmL N/A N/A 7E-17 5E-18 2E-17 3E-18 1E-16 9E-17 Counting Precision MDC,..CilmL ,..CilmL N/A N/A 8E-17 lE-17 2E-17 5E-18 1E-16 5E-17 Counting Precision MDC,..CilmL ,..CilmL N/A N/A lE-16 9E-18 2E-17 3E-18 1E-16 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.00E+00 1E-16 3E-14 1.54E+00 lE-16 9E-13 7.24E-02 2E-15 6E-13 2. 14E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 3.35E+00 lE-16 3E-14 2.36E+00 lE-16 9E-13 6.39E-02 2E-15 6E-13 1.33E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 2.28E+OO lE-16 3E-14 2.04E+OO lE-16 9E-13 2.09E-02 2E-15 6E-13 1.65E+OO L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration lE-16 9E-14 3.49E+OO lE-16 3E-14 3.64E+OO 1E-16 9E-13 8.50E-02 2E-15 6E-13 3.14E+OO Page 11 of 22 ======----------~~ www.energylab.com . ~~ Analytical ExClJlIsncfI SinClJ 7952 EN:RGY L.ABORATORIES Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Lab ID: C12010190-005 Client Sample ID BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.639 433 2600 20 6.4 105 3.4 0.4 151 15 1.3 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pCilFilter pCilFilter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 02/14/12 Collection Date: 01/03/12 DateReceived: 01/06/12 Matrix: Filter MeL! Qel Method Analysis Date 1 By SW6020 01/13/1217:14/sml SW6020 01/13/1217:141 sml E909.0 02/04/1205:141 eli-cs E909.0 02/04/1205:141 eli-cs E909.0 02/04/12 05:141 eli-cs E903.0 01/20/12 15:0S 1 trs E903.0 01/20/12 15:0S 1 trs E903.0 01/20/1215:0S/trs E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:091 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 14,2012 PROJECT: 4th Quarter Air 2011 SAMPLE ID: Blank QuarterlDate Sampled RadionucIide Concentration Air Volume J.1CilmL CI10402S9-006 natU 1.22E-17 First Quarter 2011 230Th S.84E-19 Air Volume in mLs 226Ra S.16E-18 1.36E+ll 210Pb -4.5lE-17 Counting Precision J.1CilmL N/A 2E-18 2E-18 4E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume J.1CilmL J.1CilmL CI107021S-006 natU l.OSE-17 N/A Second Quarter 2011 230Th 6.69E-18 2E-18 Air Volume in mLs 226Ra -4. 89E-20 2E-18 1.36E+ 11 210Pb -8.89E-18 SE-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. QuarterlDate Sampled Concentration Counting Air Volume RadionucIide J.1CilmL Precision J.1CilmL CI110021S-006 natu 2.42E-17 N/A Third Quarter 2011 230Th S.37E-18 3E-18 Air Volume in mLs 226Ra 7.16E-18 4E-18 1.36E+ 11 210Pb 1.44E-17 3E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. QuarterlDate Sampled Concentration Counting RadionucIide Precision Air Volume J.1CilmL J.1CilmL C12010190-006 natU 8.36E-18 N/A Fourth Quarter 2011 230Th 4.70E-18 2E-18 Air Volume in mLs 226Ra 4.73E-18 2E-18 1.36E+ 11 210Pb 2.41E-17 3E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJ.1CilmL N/A 3E-18 3E-18 7E-17 MDCJ.1CilmL N/A 2E-18 3E-18 9E-17 MDCJ.1CilmL N/A 3E-18 SE-18 SE-17 MDCJ.1CilmL N/A 2E-18 3E-18 SE-17 L.L.D.+ Effluent Cone. * % Effluent J.1CilmL J.1CilmL Concentration lE-16 9E-14 1.3SE-02 lE-16 3E-14 l.9SE-03 lE-16 9E-13 S.73E-04 2E-IS 6E-13 -7.SIE-03 L.L.D.+ Effluent Cone. * % Effluent J.1CilmL J.1CilmL Concentration lE-16 9E-14 1.17E-02 lE-16 3E-14 2.23E-02 lE-16 9E-13 -S.43E-06 2E-IS 6E-13 -1.48E-03 L.L.D.+ Effluent Cone. * % Effluent J.1CilmL J.1CilmL Concentration lE-16 9E-14 2.68E-02 lE-16 3E-14 1.79E-02 lE-16 9E-13 7.96E-04 2E-IS 6E-13 2.40E-03 L.L.D.+ Effluent Cone. * % Effluent J.1CilmL J.1CilmL Concentration lE-16 9E-14 9.28E-03 lE-16 3E-14 I.S7E-02 lE-16 9E-13 S.26E-04 2E-IS 6E-13 4.02E-03 Page 13 of 22 E RGY LABORATORIES www.energylab.com Arlalytical ExesllBIICIl Sines 7852 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 4th Quarter Air 2011 C12010190-006 Client Sample ID Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0017 1.1 3.3 4.3 7.1 0.6 0.3 0.4 0.64 0.2S 0.27 MOC -Minimum detectable concentration Units mg/filter pC VFi Iter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter Report Date: 02/14/12 Collection Date: 01/03/12 DateReceived: 01/06/12 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date 1 By 0.0003 SW6020 01/13/1217:151 sml 0.2 SW6020 01/13/1217:151 sml U E909.0 02/04/1207:191 eli-cs E909.0 02/04/12 07:191 eJi-cs E909.0 02/04/1207:191 eli-cs E903.0 01/20/12 15:0S 1 trs E903.0 01/20/1215:0S/trs E903.0 01/20/12 15:0S 1 trs E90S.0 01/17/1209:091 dmf E90S.0 01/17/1209:09/dmf E90S.0 01/17/12 09:091 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 14 of 22 www.energylab.com Analytical E.xcsIIBflcfI Sines 1952 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Analyte Count Method: E903.0 Result Units Sample 10: C12010200-001AMS Sample Matrix Spike Radium 226 3S.7 pCi/Filter Sample 10: C12010200-001AMSO Sample Matrix Spike Duplicate Radium 226 39.9 pCi/Filter Sample 10: LCS-32412 Laboratory Control Sample Radium 226 13.3 pCi/Filter Sample 10: M 8-32412 3 Method Blank Radium 226 -O.OS pCi/Filter Radium 226 precision (±) 0.1 pCilFilter Radium 226 MDC 0.3 pCilFilter Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 02/14/12 Work Order: C12010190 RL %REC Low Limit High Limit RPD RPOLimit Qual Batch: R155577 Run: BERTHOLD 770-1_120112B 01/20/12 11 :53 97 70 130 Run: BERTHOLD 770-1 120112B 01/20/12 11 :53 - 102 70 130 3.2 25 Run: BERTHOLD 770-1 120112B 01/20/12 13:25 - 112 70 130 Run: BERTHOLD 770-1 120112B 01/20/1213:25 - U NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 15 of 22 ,EN:RGY LABORATORIES www.energylab.com Analytical Exes/fence Sincs 7952 Helena, MT 817 -472-0111 • Billings, MT 800-735-4489 -Casper, WY 888-235-0515 Gillette, WY 86&-686-1175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Analyte Count Result Units Method: E908.0 Sample 10: C12010190-004AOUP Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Sample 10: C12010190-006AMS Thorium 230 Sample 10: LCS-32413 Thorium 230 Sample 10: MB-32413 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Sample Duplicate 284 pCi/Filter 26.7 pCilFilter 1.71 pCi/Filter Sample Matrix Spike 75.3 pCilFilter Laboratory Control Sample 10.9 pCi/Filter Method Blank 0.07 pCi/Filter 0.08 pCi/Filter 0.1 pCi/Filter Report Date: 02/14/12 Work Order: C12010190 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: ALPHANAL YST _120112A 2.3 Run: ALPHANAL YST _120112A 117 70 130 Run: ALPHANAL YST _120112A 111 70 130 Run: ALPHANAL YST _120112A ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 32413 01/17/1209:09 29 01/17/1209:09 01/17/1209:09 01/17/1209:09 U Page 16 of 22 www.energylab.com Analytical ExcsllsncB Sincs 1952 Helena, MT 877-472-0711 11 Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Air 2011 Analyte Count Result Units Method: E909.0 Sample 10: MB-15541 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-15541 Lead 210 Sample 10: C12010190-006AMS Lead 210 Sample 10: C12010190-006AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 3 Method Blank 0.7 pCi/Filter 4 pCi/Filter 6 pCi/Filter Laboratory Control Sample 541 pCilFilter Sample Matrix Spike 1640 pCi/Filter Sample Matrix Spike Duplicate 1660 pCi/Filter MDC -Minimum detectable concentration Report Date: 02/14/12 Work Order: C12010190 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: SUB-T43898 Run: SUB-T43898 97 70 130 Run: SUB-T43898 99 70 130 Run: SUB-T43898 98 70 130 ND -Not detected at the reporting limit. 0.7 Batch: T _15541 02/03/12 16:44 U 02/03/12 18:49 02/04/12 09:24 02/04/12 11 :29 13.5 U -Not detected at minimum detectable concentration Page 17 of 22 EI\ERGY www:energylab.com Helena, MT B77 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 " College Station, TX 888-690-2218 LABORATORIE':S Analytical Exes/fence Sines 1952 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 02/14/12 Project: 4th Quarter Air 2011 Work Order: C12010190 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: SW6020 SamplelD: ICV Uranium Method: SW6020 SamplelD: MB-32413 Uranium SamplelD: LCS2-32413 Uranium SamplelD: C1201 0190-001 ADI L Uranium SamplelD: C1201 0190-006AM S Uranium SamplelD: C1201 0190-006AM SD Uranium Method: SW6020 SamplelD: MB-32413 Uranium SamplelD: LCS2-32413 Uranium SamplelD: C12010190-004AMS Uranium SamplelD: C1201 0190-004AM SD Uranium Method: SW6020 SamplelD: ICV 2 Uranium Uranium, Activity Method: SW6020 SamplelD: MB-32413 Uranium Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. Analytical Run: ICPMS2-C_120113A Initial Calibration Verification Standard 01/13/1215:21 0.0508 mglL 0.00030 102 90 110 Batch: 32413 Method Blank Run: ICPMS2-C_120113A 01/13/1216:52 ND mg/filter 6E-05 Laboratory Control Sample Run: ICPMS2-C_120113A 01/13/1216:54 0.102 mg/filter 0.00030 102 85 115 Serial Dilution Run: ICPMS2-C_ 120113A 01/13/1217:06 0.133 mg/filter 0.0014 2.8 20 Sample Matrix Spike Run: ICPMS2-C_120113A 01/13/1217:17 0.0542 mg/filter 0.00030 105 75 125 Sample Matrix Spike Duplicate Run: ICPMS2-C_120113A 01/13/1217:19 0.0540 mg/filter 0.00030 105 75 125 0.3 20 Batch: 32413 Method Blank Run: ICPMS2-C_120116A 01/16/1216:03 ND mg/filter 6E-05 Laboratory Control Sample Run: ICPMS2-C_120116A 01/16/1216:05 0.110 mg/filter 0.00030 110 85 115 Sample Matrix Spike Run: ICPMS2-C_ 120116A 01/16/1216:12 0.713 mg/filter 0.00030 75 125 A Sample Matrix Spike Duplicate Run: ICPMS2-C_120116A 01/16/1216:14 0.714 mg/filter 0.00030 75 125 0.1 20 A Analytical Run: ICPMS2-C_120213B Initial Calibration Verification Standard 02/13/12 17:34 0.0510 mglL 34.5 pCi/L Method Blank ND mg/filter 0.00030 102 90 110 0.20 102 90 110 Batch: 32413 Run: ICPMS2-C_120213B 02/13/12 19:27 6E-05 A -The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. MDC -Minimum detectable concentration Page 18 of 22 EN:RGY LABORATORIES www.energyJab.com Analytical ExcsHsncB Siflt:8 7852 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C12010190 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 1/9/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes D Yes D Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' N/A "c Yes D Yes D Date Received: 1/6/2012 Received by: kg Carrier 2Day name: No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present 0' Not Present 0' No VOA vials submitted 0' Not Applicable 0' Page 19 of 22 I ""U Ol co '. CD I\.) o o -I\.) I\.) Chain of Custody and Analytical Request Record Page --I-of --L-1999;~.y .. ,:-r.'rZIl.»llSW PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: P£A:\oSQoA.. ,;V\'i ,A...e....s yt''-D l.) c..r -te.-;-A~r ~OQ... State: UI Yes La'" No 0 Report Mail Address: P ... 0 .. [SO)' 160'l Contact Name: Phone/Fax: Email: Sampler: (Please Print) g \ ~d-. ~ V'-t\ VI. fL.j~' \ &t-rf\0-P~l./V'-u-~3S~67g· ?-?-~\ 6. c---r"", fI"... P~L~ Invoice Address: -.... Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: ~tN~~ SA,~e.- Special ReporUFormats: ~[b W®D@ OO~@QD~Lf(g[Q) ... Contact ELI prior to 5hipped by: d. /l. 3: RUSH sample submittal u.fS, ?fI . 'J Cl Q) ~O{/)..c. for charges and Cooler 10(s): (/ ~[[);g 01 :v 0 fi R scheduling -See ._> 0 :>oro w C Instruction Page !loX DDW D EDD/EDT{Electronic Data) aCl)CI)ctl s c: en (/) I 0s= ~ 0) "0 Receipt Temp o POlWMlWTP () c Comments: Format: u <t:~1.2,~ ::J U ~tj4-o State: D LEVEL IV '0 ,,-COI-2 $ ~ « e °C ., <1> c ·-f-ro ... ~ro.2 0 ~ c o Other: o NELAC ~~Icri I + ~ :s On Ice: y® d -r-:J <1>.= 115 3: ~ d N 5 z a.. <t:1 ar Cl W 'E Custody Seal ~~ ~ >1 \ I W ro On Bottle , U) "0 CI) ~ d c:: On Cooler ~ ...0 m cl U5 H Intact Y N SAMPLE IDENTIFICATION Collection Collection , c.. MATRIX ..... Signature (Name, Location, Interval, etc,) Date Time Match Y N 1 ~ }3 or A -X EHV~ 1 ~.. \<~ .. r~ X )<. X !~ 2 EH.V _ ?---. ( X X ~ i. I~ 3 [SHLI-Y I 'J X ~ X i\Q) ( Innn 4g~tI-S ) ( X )( x. X I~ I~ 5BWv-1, \~ X )( X X I"=' ~ 6 131o..l'~ ~ ·3-1~ l:3-A )( x· X X ~ 7 ~ ~ 8 ~ 0 9 ~ I!cJ /)/ tJ/ftf 10 t:::::! ' Custody Relinquished by (prip~ DatelTime: 1000 ~: ti Received by (print): DatelTime: Signature: h-A .. ~ l·t..I;1..0~ ~4-. ~ Record Relinquished by (print): DatefTime: Signature: Received by (print): Dalemme: Signature: MUST be Signed I'(ecelveo Dy L8Doratory: Uateillme: 1",30 I< :;ilgnature: Sample Disposal: Return to Client: Lab Disposal: f ·'-J~ r;·.) C-. 5~ L In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility, All sub-contract data will be clearly notated on your analytical report. I Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links, ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA a a a !=> f-> 0 0 0 f-> 0 a a f-> a a a f-> a a a f-> a a a a 1/5/2009 2/5/2009 3/5/2009 4/5/2009 . 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 » + 10/5/2009 -. ""'" OJ 11/5/2009 '" I ,... OJ < 12/5/2009 ~ ,... -. + 1/5/2010 0 ::l 2/5/2010 "'tJ OJ I 3/5/2010 OJ < ""'" N 4/5/2010 ,... -. n + 5/5/2010 c: OJ OJ 6/5/2010 ,... I tD < .J::,. 7/5/2010 r-0 + 8/5/2010 OJ 9/5/2010 a.. OJ I ::l < 10/5/2010 C7Q Ln ........ 11/5/2010 + 3 12/5/2010 C7Q OJ ............... I 1/5/2011 3 < m w 2/5/2011 -...... 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 0 0 0 0 0 .... i-> 0 0 .... 0 .... 0 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 O:J 11/5/2009 :I: 12/5/2009 < I 1/5/2010 ~ ""C 2/5/2010 OJ ~ 3/5/2010 r+ -. n 4/5/2010 C t · 5/5/2010 OJ r+ tD tp 6/5/2010 :::r: r-< ~ 7/5/2010 0 OJ 8/5/2010 c.. 9/5/2010 ::s (JQ 10/5/2010 ......... 3 11/5/2010 (JQ , 12/5/2010 3 1/5/2011 w ~ 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 0 0 ~ 0 0 I-> 0 I-> 0 I-> I-> 0 0 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 O:J 11/5/2009 ::J: 12/5/2009 < I 1/5/2010 N 2/5/2010 • -0 OJ ~ 3/5/2010 r+ --n 4/5/2010 c: + 5/5/2010 OJ r+ tD OJ 6/5/2010 :c r-< N 7/5/2010 0 OJ 8/5/2010 a.. --::J 9/5/2010 C7Q 10/5/2010 ........ 3 11/5/2010 C7Q .............. 12/5/2010 3 1/5/2011 · w ~ 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 0 ~ ~ ~ ...... a 0 0 ...... a 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 0 1/5/2009 I II I ~I • ~- 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 g:J 11/5/2009 :::I: 12/5/2009 < I 1/5/2010 ~ -a 2/5/2010 Q,J "'"'I 3/5/2010 r+ -. n 4/5/2010 c: + 5/5/2010 Q,J r+ tD OJ 6/5/2010 :r: r-< 0 l:. 7/5/2010 Q,J 8/5/2010 c.. 9/5/2010 ::::s (JQ 10/5/2010 ......... 3 11/5/2010 (JQ .............. 12/5/2010 3 1/5/2011 w ......... 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 0 0 0 0 I-' 0 ..... 0 0 I-' 0 I-' 0 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 o:J 11/5/2009 ::I: 12/5/2009 < I 1/5/2010 U1 "'tJ 2/5/2010 OJ .., 3/5/2010 ,... -. n 4/5/2010 c: + 5/5/2010 OJ ,... (1) OJ 6/5/2010 :::c r-< Ln 7/5/2010 0 OJ 8/5/2010 c.. 9/5/2010 :l C1Q 10/5/2010 ........ 3 11/5/2010 C1Q ............... 12/5/2010 3 1/5/2011 w .........- 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 I !=' ~ 0 a 0 a ~ 0 a ~ 0 0 0 0 0 0 0 ~ 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 C:J 11/5/2009 :J: < I 12/5/2009 0'\ 1/5/2010 . '"tJ OJ 2/5/2010 -, r+ -. 3/5/2010 n 4/5/2010 c:: OJ + r+ 5/5/2010 tD r-OJ 6/5/2010 I 0 < 7/5/2010 OJ ~ 8/5/2010 a.. ::J 9/5/2010 (1Q .--... 10/5/2010 3 (1Q 11/5/2010 " 12/5/2010 3 UJ ........ 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 -L S / 2011 Period: July 5,2011 through October 4,2011 (3rd Quarter 2011) \ Page 1 " BHV -1 on stream % 92.2% BHV·1 Total Volume: 4.39E+06 Week Fitter Start Stop Stop Start Total Total Loading, Per Cent .. -. _ .. -.. . . .~-.-..... --...... ,_, .0. "... .. __ ._ .0. 0_0. 1 8153852 5-Jul-11 II-Jul-ll 4.6794 4.5063 0.1731 31034.0 30890.6 8605.8 8.894.653 0.0195 99.6% 36.5 2 8400966 ll-Jul-ll I8-Jul-11 4.4959 4.3055 0.1904 31207.4 31034.0 10404.0 10,900,514 0.0175 103.2% 37.0 3 8400961 18-Jul-II 2S-Jul-Il 4.5538 4.3244 0.2294 31373.0 31207.4 9936.6 lO.41O,808 0.0220 98.6% 37.0 4 840095S 25-Jul-ll I-Aug-ll 4.4097 4.2790 0.1307 31542.8 31373.0 10188.6 10,674.834 0.0122 101.1% 37.0 5 8400946 OI-Aug-I I 8-Aug-11 4.4659 4.3444 0.1215 31709.8 31542.8 10020.6 10.498,816 0.0116 99.4% 37.0 6 8400940 08-Aug-ll IS-Aug-II 4.3654 4.3360 0.0294 31709.8 31709.8 0.0 ° #DIV/O! 0.0% 37.0 7 8400937 IS-Aug-ll 22-Aug-ll 4.4979 4.3478 0.1501 31878.4 31709.8 10112,4 10,566,362 0.0142 100.3% 36.9 8 8400931 22-Aug-11 29-Aug-1I 4.4373 4.2973 0.1400 32042.3 31878.4 9838.2 10,279,853 0.0136 97.6% 36.9 9 8400925 29-Aug-ll 5-Sep-ll 4.4788 4.2852 0.1936 32236.0 32042.3 11623.2 12,144,985 0.0159 115.3% 36.9 10 8153846 05-Sep-11 12-Sep-1I 4.6240 4.5267 0.0973 32376.3 32236.0 8414.4 8,720.656 O.oI 12 83.5% 36.6 tl 8153840 12-Sep-1 I 19-5ep-1 I 4.5965 4.5156 0.0809 32544.6 32376.3 10096.2 10,406,489 O.OO7S 100.2% 36.4 12 8153834 J9-Sep-11 26-Sep-ll 4.6278 4.5226 0.1052 32712.7 32544.6 10086.6 10,396,594 0.0101 100.1% 36.4 13 8153832 26-Sep-11 3-0Cl-II 4.7467 4.5187 0.2280 32881.5 32712.7 10132.8 10,444,214 0.0218 100.5% 36.4 Totals 90 2160.0 4.5368538 4.3939385 0.1438 119459.4 124,338,777 #DN/O! 92.3% 36.8 BHV-2 on stream % 92.1% BHV·2 Total Volume: 4.39E+06 Week Filter Start Stop Stop Start Total Total Loading, Per Cent .. . -_ ............. _.--.-._--,_,-.. _ .. . .... -..... -........... _ ........ "'" . ... ..,. ... -.. ........ _ ... . .... 1 6153853 05-Jul-11 11-Jul-11 4.7483 4.4924 0.2559 41222.6 41079.3 8599.2 8,887.831 0.0288 99.5% 36.5 2 8400965 11-Jul-l1 18-Jul-l1 4.5384 4.2573 0.2811 41396.5 41222.6 10434.6 10,932,574 0.0257 103.5% 37.0 3 8400960 l8-Jul-ll 25-Jul-l1 4.5968 4.3252 0.2716 41559.2 41396.5 9759.6 10,225,361 0.0266 96.6% 37.0 4 8400954 2S-Jul-11 01-Aug-11 4.5453 4.3242 0.2211 41729.0 41559.2 lO1S6.2 10,672,319 0.0207 101.1% 37.0 5 8400947 01-Aug-l1 08-Aug-11 4.5823 4.3354 0.2469 41895.7 41729.0 10002.0 10,479,329 0.0236 99.2% 37.0 6 8400941 OB-Aug-11 15-Aug-11 4.3456 4.2976 0.0482 41895.7 41895.7 0.0 0 #DIV/O! 0.0% 37.0 7 8400936 15-Aug·l1 22-Aug.l1 4.6578 4.3547 0.3031 42064.8 41895.7 10146.0 10,601,471 0.0286 100.7% 36.9 8 8400930 22-Aug-11 29-Aug-11 4.5733 4.3424 0.2309 42228.8 42064.8 9839.4 10,281,107 0.0225 97.6% 36.9 9 8400924 29-Aug-11 05-Sep-11 4.5928 4.3154 0.2774 42422.0 42228.8 11596.2 12,116.773 0.0229 115.0% 36.9 10 8153847 05-Sep·11 12-Sep-11 4.6916 4.5335 0.1581 42562.4 42422.0 8420.4 8,726,B74 0.0181 83.5% 36.6 11 8153841 12-Sep-11 19-5ep-11 4.6409 4.5223 0.1186 42731 .0 42562.4 10117.2 10,428,134 0.0114 100.4% 36.4 12 8153835 19-5ep-11 26-Sep-11 4.7054 4.5154 0.1900 42899.1 42731.0 100&7.2 10,397,212 0.0183 100.1% 36.4 13 8153829 26-Sep-11 03-0ct-11 4.9104 4.4960 0.4124 43069.0 42899.1 lO195.8 10,509,150 0.0392 101.1% 36.4 "----L.. Totals 90 2160.0 4.62532 4.39337 0.2319 119383.8 124.258,135 #DIV/O! 92.2% 36.8 BHV-4 on stream % 102.3% BHV·4 Total Volume: 4.88E+06 Week Filter Start Stop Stop Start Total Total Loading, Per Cent ,._-.. __ . _.--_.-.---,_ ..... .._. ..... -....... -. .... --.... -~-"';:r"'-_., _ .. __ ... __ a .r. 1 8153854 05-Jul-ll 11-Jul-11 4.6472 4.5055 0.1417 16384.0 16240.0 8641.8 8,931,861 0.0159 100.0% 36.5 2 8400967 11-Jul-11 18-Jul-l1 4.5727 4.3148 0.2579 16557.0 16384.0 10381.2 10,876,626 0.0237 103.0% 37.0 3 8400959 18-Jul-11 25-Jul-11 4.5700 4.2940 0.2760 16723.3 16557.0 9979.8 10,456,069 0.0264 99.0% 37.0 (C ; 4 8400953 25-Jul-11 01-Aug-11 4.5186 4.3420 0.1766 16891.5 16723.3 10087.8 10,569,223 0.0167 100.1% 37.0 ) 5 8400946 01-Aug-11 Oa-Aug-l1 4.4619 4.3162 0.1457 17058.9 16891.5 10047.6 10,527,105 0.0138 99.7% 37.0 I ) 6 8400942 08-Aug-11 1S-Aug-11 4.4722 4.2986 0.1736 17228.1 17058.9 10149.6 10,633.973 0.0163 100.7% 37.0 7 8400935 15-Aug-11 22-Aug-11 4.5385 4.3011 0.2374 17396.9 17228.1 10131.6 10,586,424 0.0224 100.5% 36.9 ~ 8 8400929 22-Aug-11 29-Aug-11 4.5447 4.3161 0.2266 17561.1 17396.9 9848.4 10.290,511 0.0222 97.7% 36.9 ~ 9 8400923 29-Aug-11 OS-Sep-l1 4.6235 4.3312 0.2923 17752.7 17561.1 11494.8 12,010,821 0.0243 114.0% 36.9 10 6153848 05-Sep-11 12-Sep-11 4.6041 4.5311 0.2923 17893.8 17752.7 11494.8 11,913,172 0.0245 B4.0% 36.6 11 8153842 12-Sep-11 19-5ep-11 4.6296 4.5279 0.1017 18063.2 17693.8 10165.8 10,478,228 0.0097 100.9% 36.4 12 8153836 19-5ep·l1 26-Sep-11 4.5900 4.5186 0.0714 18230.3 18063.2 10029.6 10,337,842 0.0069 99.5% 36.4 13 8153830 26-Sep-11 03-0ct-11 4.7816 4.4999 0.2817 18400.1 18230.3 10183.8 10,496,781 0.0268 101.0% 36.4 ~ .......... Totals 90 2160.0 4.58112 4.39208 0.2059 132636.6 138,1 08,636 . ~92 100.0% 36.8 _ ••• _~. ") I t: "'U Q) <C CD '" '" o -.. '. '" c.v Week 1 2 3 4 5 6 7 8 9 10 11 12 13 BHV-5 on stream % Filter Start ... -~ .. --. -...... ~ .... 8153855 05-Jul-11 8400963 l1-Jul-11 8400958 18-Jul-11 8400952 25·Jul·11 8400949 01-Aug-l1 8400943 08-Aug-11 8400934 1S-Aug-l1 8400928 22-Aug-l1 8400922 29-Aug-11 8153849 OS-Sep-11 8153843 12-Sep-11 8153837 19-5ep-11 8153828 26-Sep-11 Totals 90 100.0% Slop _.-_._--._.- lhJul-11 4.7259 4.5153 1B-Jul-,1 4.5716 4.3260 25-Jul-11 4.5658 4.2922 01-Aug-11 4.4680 4.3069 OS-Aug-11 4.5812 4.3054 15-Aug-ll 4.7850 4.3422 22-Aug-11 4.5244 4.3163 29-Aug-11 4.4615 4.2720 05-Sep-11 4.5432 4.2940 12-Sep-11 4.5810 4.5074 19-5ep-11 4.6313 4.5239 26-Sep-11 4.6688 4.5186 03-0ct-11 4.7747 4.4990 2160.0 4.60634 4.38609 ,. "'/)/I~/~ BHV-5 Total Volume: 4.76E+06 .... Stop Start Total Total Loading, Per Cent .. -.. .......... . .... -~ --.. -_ ......... . ... -.-....... ~. --- - 0.2106 40509.8 40365.4 8667.0 8,957,907 0.0235 100.3% 36.S 0.2456 40682.9 40509.8 10385.4 10,881.026 0.0226 103.0% 37.0 0,2736 40848,7 40682.9 9948.0 10,422.752 0.0263 98.7% 37.0 0,1611 41017.6 40848.7 10134.0 10,617,628 0,0152 100.5% 37.0 0.2758 41184.8 41017.6 10029.0 10,507,617 0.0262 99.5% 37.0 0.4428 41354,0 41184.8 1Ol57.4 10,642,145 0.0416 100.8% 37.0 0.2081 41522,5 41354.0 IOlOS.8 10,559,466 0.0197 100.3% 36.9 0.1895 41686.6 41522.5 9844.8 10,286,749 0.0184 97.7% 36.9 0.2492 41878.7 41686.6 11527.& 12,045,302 0.0207 114.4% 36.9 0.0736 42019.7 41878.7 8459.4 8,767,293 0,0084 83.9% 36.6 0.1074 42188.6 42019.7 10137.6 10,449,161 0.0103 100.6% 36.4 0.1502 42356.2 42188.6 10055.4 10.364,435 0.Q145 99.8% 36.4 0.2757 42524.3 42356.2 10084.8 10,394,738 0.0265 100.0% 36.4 0,2202 7797800 129536.4 134,896,221 0.0211 100.0% 36.8 -.,., IJ Q) co (I) I\) (.V o -+0 I\) (.V Period: July 5, 2011 through October 4,2011 (3rd Quarter 2011) BHV·6 on stream % Week Filter Start ----_ .. - 1 8153856 05-Jul-11 2 8400968 11-Jul-11 3 8400957 18-Jul-11 4 8400951 2S-Jul-11 5 8400950 01-Aug-11 6 8400944 OS-Aug-11 7 8400933 1S-Aug-11 8 8400927 22-Aug-11 9 8400921 29-Aug-11 10 8153850 OS-Sep-11 11 8153844 12-Sep-l1 12 8153838 19-5ep-11 13 8153827 26-Sep-l1 Totals 90 ALL BHV on stream % Week :# Blanks Start Date 1 8400864 05-Jul-11 2 8400962 11-Jul-11 3 8400956 18-Jul-l1 4 8400945 25-Jul-l1 5 8400939 01-Aug-11 6 8400938 OS-Aug-l1 7 8400932 15-Aug-l1 8 8400926 22-Aug-l1 9 8153845 29-Aug-11 10 8153839 OS-Sep-11 11 8153833 12-Sep-11 12 8153831 19-5ep-11 13 8400920 26-Sep-11 Totals 90 100.0% Stop -_.- 11-Jul-l1 18-Jul-11 25-Jul-11 01-Aug-11 08-Aug-11 15-Aug-11 22-Aug-11 29-Aug-11 OS-Sep-11 12-Sep-11 19-5ep-l1 26-Sep-11 03-0ct-11 2160.0 97.3% Stop Date l1-Jul-11 lS-Jul-l1 25-Jul-11 01-Aug-l1 08-Aug-l1 is-Aug-l1 22-Aug-11 29-Aug-11 05-Sep-l1 12-Sep-l1 19-5ep-11 26-Sap-11 03-0ct-11 2160.0 ~ .. -~- 4.6547 4.4815 4.5276 4.4446 4.5403 4.6706 4.5118 4.4753 4.5365 4.5737 4.5992 4.6215 4.6239 4.55855 Net 4.3147 4.2825 4.3071 4.2782 4.3354 4.3002 4.3372 4.3430 4.5279 4.4949 4.5131 4.5199 4.3281 4.3756 L lI/tJp')/1\ Stop --.-. -..... -..... - 4.4800 0.1747 6289.9 4.2960 0.1855 6463.2 4.3183 0.2093 6629.2 4.3480 0.0966 6797.9 4.3371 0.2032 6964.6 4.3500 0.3206 7134.4 4.3449 0.1669 7303.0 4.3303 0.1450 7467.1 4.3158 0.2207 7658.6 4.5205 0.0532 7800.2 4.5335 0.0657 7969.2 4.5299 0.0916 8136.6 4.4817 0.1422 8306.5 4.39892 0.1596 " Page 2 BHV-6 Total Volume: 4.77E+06 Start Total Total Loading, Per Cent . --.-~ -... --_. __ .-·-:'iiiil:.:'·-.0 • ____ 0 •• -_ . 6145.6 8658.6 8,949,225 0.0195 100.2% 36.5 6289.9 10398.0 10,894,227 0.0170 103.2% 37.0 6463.2 9960.6 10,435,953 0.0201 98.8% 37.0 6629.2 lOt 17.2 10,600,027 0.0091 100.4% 37.0 6797.9 10006.2 10,483,729 0.0194 99.3% 37.0 6964.9 10165.2 10,650,317 0.0301 100.8% 37.0 7134.4 10116.0 10,570,124 0.0158 100.4% 36.9 7303.0 9846.0 10,288,003 0.0141 97.7% 36.9 7467.1 11491.2 12,007,059 0.0184 114.0% 36.9 7658.6 8495.4 8,804,604 0.0060 84.3% 36.6 7800.2 10143.0 10,454,727 0.0063 100.6% 36.4 7969.2 10045.2 10,353,921 0.0088 99.7% 36.4 8136.6 10192.8 10,506.058 0.0135 101.1% 36.4 129635.4 134,997,975 0.0152 100.0% 36.8 Per~od: October 4,2011 through January 3, 2012(4th Quarter 2011) BHV-1 on stream % Week Filter # N be um r ) 8400919 2 8400914 3 8400907 4 8400902 5 8153818 6 8J53812 7 8153808 8 8400000 9 8399996 10 8399987 II 8399981 12 8399975 13 8399972 Totals Start D ate 3-Oct-l ) IO-Oct-ll 17-Oct-11 24-Oct-ll 31-Oct-Il 07-Nov-ll 14-Nov-ll 21-Nov-1l 28-Nov-l1 05-Dec,11 12-Dec-11 19-Dec·ll 26-Dec-ll 91 BHV-2 on stream % Week Filter # N be um r 1 8400918 2 8400913 3 8400906 4 8153826 5 8153819 6 8153811 7 8153807 8 8399999 9 8399995 10 8399988 11 8399982 12 8399976 13 8399971 Totals Start o t ae 03-0ct-11 10-0ct-11 17-0ct-11 24-0ct-11 31-Oct-11 07-Nov-11 14-Nov-11 21-Nov-11 28-Nov-11 05-0ec-11 12-0ec-11 19-Dec-11 26·J)ec..11 91 BHV-4 on stream % Week Filter Start # Number Date 1 8400917 03-0ct-11 2 8400912 10-0ct-11 3 8400905 17-0ct-11 4 6153825 24..Qct-11 5 8153820 31-0ct-11 6 8153813 07-Nov-11 7 8153806 14-Nov.11 8 8153801 21-Nov-11 9 6399994 28-Nov-11 10 8399989 05-0ec-11 11 8399983 12-0ec-11 12 8399977 19-0eo-11 13 8399970 26-0ec·11 Totals 91 BHV-5 on stream % Week Filter Start # Number Date 1 8400916 03-0ct-11 2 8400911 10-0ct-11 3 8400904 17-Oct-11 4 8153822 24-0ct-11 5 8153821 31-0ctM11 6 8153814 07-Nov-11 7 8153805 14-Nov-11 8 8153802 21-Nov-11 9 8399993 28-Nov-11 10 8399990 05-Dec-11 11 8399964 12-Dec-11 12 8399978 19-Dec-11 13 8399969 26-Dec-11 Totals 91 101.1% Stop D ate 10-Oct-11 17-Oct-II 24-Oct-11 31-Oct-1I 7-Nov-11 14-Nov-1l 21-Nov-11 28-Nov-11 5-Dec-1I 12-Dec-1I 19-Dec-JI 26-Dec-ll 2-Jan-12 2184.0 101.0% Stop o t aa 10-0ct-11 17-0ct-11 24-0ct-11 31-0ct-11 07-Nov-11 14-Nov-11 21-Nov-11 28-Nov-11 OS-Dec-11 12-Dec-11 19-0ec-11 2f3..0ec,11 02-Jan-12 2184.0 101.1% Stop Date 10-0ct-11 17-0ct-11 24-0ct-11 31-0ct-11 07-Nov-11 14-Nov·11 21-Nov-11 2a-Nov-11 05-0ec-11 12-Dec-11 19-Dec-11 26-Dec-11 02·Jan-12 2184.0 95.3% Stop Date 10-0ct-11 17-0ct-11 24-Oct-11 31-0ct-11 07-Nov-11 14-Nov-11 21-Nov-11 28-Nov-11 05-0ec-11 12-Dec-11 i9-0ec-11 26-Dec-11 02-Jan·12 2184.0 Gross Tare 4.3979 4.3018 4.3968 4.3124 4.3968 4.3077 4.3733 4.2903 4.6628 4.5218 4.5861 4.5140 4.7043 4.4968 4.3742 4.2779 4.4230 4.2821 4.3366 4.2520 4.3131 4.2586 4.2825 4.2133 4.3368 4.1882 4.429554 4.324377 G ross T are 4.3668 4.2658 4.4879 4.3289 4.4722 4.2722 4.6490 4.5209 4.7318 4.5223 4.6009 4.4923 4.7929 4.4868 4.4462 4.2773 4.4759 4.2612 4.3605 4.2063 4.3115 4.2299 4.3340 4.2075 4.5165 4.2269 4.503546 4.33064 Gross Tare 4.4057 4.3138 4.3414 4.2696 4.2640 4.2543 4.6155 4.5140 4.6900 4.5026 4.5935 4.5261 4.6668 4.5180 4.5319 4.5037 4.4182 4.2745 4.3287 4.2661 4.2647 4.2287 4.2525 4.2330 4.2993 4.2214 4.436323 4.35583 Gross Tare 4.4202 4.3019 4.4155 4.3018 4.5655 4.2983 4.6407 4.5314 4.7200 4.5043 4.5962 4.4994 4.5566 4.5067 4.8837 4.4949 4.4614 4.2868 4.3630 4.2750 4.3351 4.2709 4.3193 4.2404 4.3562 4.1838 4.493338 4.3612 Net 0.0961 0.0844 0.0891 0.0830 0.1410 0.0721 0.2075 0.0963 0.1409 0.0846 0.0545 0.0692 0.1486 0.1052 N et 0.1010 0.1590 0.2000 0.1261 0.2095 0.1086 0.3061 0.1689 0.2147 0.1542 0.0616 0.1265 0.2896 0.1729 Net 0.0919 0.0718 0.0097 0,1015 0.1874 0.0674 0.1488 0.0282 0.1437 0.0626 0.0360 0.0195 0.0779 0.0805 Net 0.1183 0.1137 0.2672 0.1093 0.2157 0.0968 0.0499 0.1688 0.1746 0.0880 0.0642 0.0789 0.1724 0.1321 Stop Time 33051.3 33216.4 33388.9 33553.4 33721.1 33894.5 34059.5 34225.2 34394.5 34561.4 34729.0 34924.7 35089.2 Stop T' Ime 43237.7 43402.7 43575.0 43739.5 43907.6 44080.5 44245.9 44411.7 44581.7 44747.3 44915.5 45111.1 45275.8 Stop Time 16570.6 18733.7 18907.4 19072.0 19240.1 19412.8 19517.1 19742.8 19911.8 20078.0 20246.9 20442.3 20607.8 Stop Time 42692.6 42855.6 43029.1 43193.8 43360.7 43533.9 43598.3 43762.2 43919.7 44085.4 44254.2 44449.6 44615.0 BHV-1 Start T' Ime 32881.5 33051.3 33216.4 33388.9 33553.4 337211 33894.5 34059.5 34225.2 34394.5 34561.4 34729.0 34924.7 BHV-2 Start T Ime 43069.0 43237.7 43402.7 43575.0 43739.5 43907.6 44080.5 44245.9 44411.7 44581.7 44747.3 44915.5 45111.1 BHV-4 Start Time 18400.1 18570.6 18733.7 18907.4 19072.0 19240.1 19412.8 19577.1 19742.8 19911.8 20078.0 20246.9 20442.3 SHV-5 Start Time 42524.3 42692.6 42855.6 43029.1 43193.8 43360.7 43533.9 43598.3 43762.2 43919.7 44085.4 44254.2 44459.6 Total T' Ime 10186.2 9903.0 10350.6 9874.2 10057.8 10404.6 9898.8 9946.2 10153.2 10018.2 10055.4 11739.0 9874.8 132462 Total T Ime 10121.4 9901.2 10332.6 9871.2 10087.2 10375.8 9924.0 9944.4 10200.6 9939.6 10087.8 11739.0 9882.0 132406.8 Total Time 10234.2 9781.2 1042S.0 9873.6 10087.8 10359.6 9851.4 9945.6 10141.2 9972.6 10132.2 11720.4 9931.8 132462.6 Total Time 10096.8 9783.6 10409.4 9881.4 10015.2 10390.2 3864.6 9832.8 9452.4 9936.6 10132.& 11719.2 9324.0 124839 Total Volume: 4.87E+06 Total L' Iters 10,528,099 10,375,604 10,844,565 10,345,430 10,537,792 10,901.142 10,343,174 1O,392.70t 10,608,994 10,382,828 10.364,435 12.099,777 10,178,285 137,902,826 Loading, . Per Cent mgtm3 o S n tream 0.0091 101.1% 0.0081 98.2% 0.0082 102.7% 0.0080 98.0% 0.0134 99.8% 0.0066 103.2% 0.0201 98.2% 0.0093 98.7% 0.0133 100.7% 0.0081 99.4% 0.0053 99.8% 0.0057 116.5% 0.0146 98.0% 0.0100 101.1% Total Volume: 4.87E+06 Total l't I ers 10,461,124 10,373,718 10,825,706 10,342,287 10,568,595 10,870,968 10,369,505 10,390,821 10,656,522 10,301,368 10,397,831 12,099,777 10,185,706 137,845,926 Loading, Per Cent t 3 0 S mQlm n tream 0.0097 100.4% 0.0153 98.2% 0.0185 102.5% 0.0124 97.9% 0.0198 100.1% 0.0100 102.9% 0.0295 98.5% 0.0163 98.7% 0.0201 101.2% 0.0150 98.6% 0.0078 100.1% 0.0105 116.5% 0.0284 98.0"/0 0.0164 101.0% Total Volume: 4.87E+06 Total Loading, Per Cent liters mg/m3 On Stream 10,577,710 0.0087 101.5% 10,247,992 0.0070 97.0% 10,922,516 0.0009 103.4% 10,344,801 0.0098 98.0% 10,569,223 0.0177 100,1% 10,853,995 0.0062 102.8% 10,299,915 0.0144 97.8% 10,392,074 0.0027 98.7% 10,596,455 0.0136 100.6% 10,335,569 0.0061 98.9% 10.443,595 0.0034 100.5% 12,080,606 0.0016 116.3% 10,237,036 0.0076 98.5% 137,901,487 0.0077 101.1% Total Volume: 4.59E+06 Total Loading, Per Cent liters mg/m3 On Stream 10,435,698 0.0113 100.2% 10,250,506 0.0111 97.1% 10,906,171 0.0245 103.3% 10,352,973 0.0106 98.0% 10,493,159 0.0206 99.4% 10,886,055 0.0089 103.1% 4,038,088 0.0124 38.3% 10,274,211 0.0164 97.5% 9,876,734 0.0177 93.8% 10.298,258 0.0085 98.6% 10,444,214 0.0061 100.5% 12,079,369 0.0065 116.3% 9,610,557 0.0179 92.5% 129,945,993 0.0133 95.3% Page 21 of 22 Page 1 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.S 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36,9 36.6 36.4 36.4 36.4 36.8 SCFM 365 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 r Period: October 4, 2011 through January 3, 2012(4th Quarter 2011) BHV-S on stream % Week Filter Start # Number Date 1 8400915 03-0ct-11 2 8400910 10-0ct-11 3 8400903 17-0ct-11 4 8153823 24-Oct-11 5. 8153824 31-Qct-11 6 8153815 07-Nov-11 7 8153804 14-Nov-11 8 8153803 21-Nov-11 9 8399992 28-Nov-11 10 8399991 05-Dec-11 11 8399985 12-Dec-11 12 8399979 19-Dec-11 13 8399968 26-Dec-11 Totals 91 ALL BHV on stream % Week # Blanks Start Date 1 8400909 03-0ct-11 2 8400908 10-0ct·11 3 • 8400901 17-0ct-11 4 8153817 24-0ct-11 5 8153810 31-0ct-11 6 8153809 07-Nov-11 7 8399998 14-Nov-11 8 8399997 21-Nov-11 9 8399986 28-Nov-11 10 8399960 05-Dec-11 11 8399974 12-0ec-11 12 8399973 19-0ec-11 13 8399967 26-0ec-11 Totals 91 101.1% Stop Date 10-0ct-11 17-Oct-11 24-Oct-11 31-0ct-11 07-Nov-11 14-Nov-11 21-Nov-11 28·Nov-11 0S-Dec-11 12-Dec-11 19-Dec-11 26-Dec-11 02-Jan-12 2184.0 99.9% Stop Date 10-0ct-11 17-0ct-11 24-0ct-11 31-0ct-11 07-Nov-11 14-Nov-11 21-Nov-11 2a-Nov-11 05-Dec-11 12-Dec-11 19-0ec-11 26-Dec-11 02-Jan-12 2184.0 Gross 4.3667 4.4066 4.4964 4.6121 4.6741 4.6067 4.7366 4.6175 4.4384 4.2873 4.2972 4.2583 4.4350 4.479454 Net 4.3066 4.2458 4.3051 4.5142 4.5085 4.5233 4.2337 4.2868 4.2352 4.2539 4.2349 4.1980 4.2439 4.3146 Stop Tare Net Time 4.2595 0.1072 8477.0 4.2966 0.1100 8640.2 4.3246 0.1718 8813.3 4.5094 0.1027 8977.9 4.4973 0.1768 9146.1 4.5205 0.0862 9319.1 4.5000 0.2366 9483.4 4.4884 0.1291 9649.1 4.2718 0.1666 9818.2 4.2610 0.0263 9984.1 4.2375 0.0597 10152.9 4.1875 0.0708 10348.2 4.2469 0.1881 10513.7 4.35392 0.1255 Page 2 BHV-6 Total Volume: 4.87E+06 Start Total Total Loading, Per Cent Time Time Liters mglm3 On Stream SCFM 8306.5 10228.8 10,572,129 0.0101 101.5% 365 6477.0 9790.8 10,258,050 0.0107 97.1% 37.0 8640.2 10388.4 10,884,169 0.0158 103.1% 37.0 8813.3 9877.2 10,348,573 0.0099 98.0% 37.0 8977.9 10092.0 10,573,624 0.0167 100.1% 37.0 9146.1 10378.2 10,873,482 0.0079 103.0% 37.0 9319.1 9855.0 10,297,407 0.0230 97.8% 36.9 9483.4 9947.4 10,393,955 0.0124 98.7% 36.9 9649.1 10143.0 10,598,336 0.0157 100.6% 36.9 9818.2 9951.6 10,313,804 0.0025 98.7% 36.6 9984.1 10131.6 10,442,977 0.0057 100.5% 36.4 10152.9 11719.8 12,079,987 0.0059 116.3% 36.4 10346.2 9928.8 10,233,944 0.0184 98.5% 36.4 132432.6 137,870,438 0.0119 101.1% 36.8 Page 22 of 22 ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA I White Mesa Mill Ambient Gamma Levels Over-Time] 50.00 ~------------------------------------------------------------------------------------------------------------------------------~ 45.00 I ..t. 40.00 I II .... 35.00 I II ..t. I I ... I I ... 30.00 l0-a> t 25.00 ro ::J 0--E a> C( 20.00 .. E 15.00 10.00 I II • • II 5.00 I ~l V -.n1lrlT-""'" I I ..,.... I \: Pi ,-w. T1:::.-I \ W _ '" I " ,1:, \ • I .... II S. \' " 30-Sep_81 05-JUI_83 04-Apr_85 03-Feb_8? 11-0ct_88 16-JUI_90 10-Apr_92 13-Jan_94 16-0ct_95 8-JUI_9? 13-Apr_99 20-Feb_01 15-0ct_02 9-JUI-04 10-Apr_06 31-DeC_O? 2-0ct_09 VvH"r~ ME:SA MIL.L. Background (BHV-3) subtracted from BHV-1 , BHV-2, BHV-4, BHV-5, and BHV--6 ~BHV-1 ~BHV-2 -'-BHV-3 _BHV-4 _BHV-5 ....... BHV-6 [Willt!MesaMillUArnbient Gamma Levels Over Time BHV-11 50.00 ~------------------------------------~-------------------------------------------------------------------------------, 45.00 +1--------------------------------------------------------------------------------------------------------------------------~ 40.00 +1--------------------------------------------------------------------------------------------------------------------------~ 35.00 +1--------------------------------------------------------------------------------------------------------------------------~ 30.00 lo... Q) ........ lo... CU 25.00 :::J rr ......... E Q) a> 20.00 E 15.00 10.00 I I' 5.00 I • II I I .,. , I 1J: \' 'I 30-Sep_81 03-0Ct_83 07_0ct_85 09-0Ct_87 30-0Ct_89 30-Sep_91 8-0Ct_93 16-0ct_95 10_AI 12-0 t 24-0 t Ivoll_97 c -99 c -01 3-0ct-03 17_0ct_ 05 30-0ct_07 2-0ct-09 Background (BHV-3) Subtracted from BHV-1 .-------------- _e_BHV-1 ! White Mesa Mill Ambient Gamma Levels Over Time BHV-2! 50.00 ~------------------------------------------------------------------------------------------------------------~ 45.00 +1----------------------------------------------------------------------------------------------------------------------1 40.00 +1--------------------------------------------------------------------------------------------------------------, 35.00 +1--------------------------------------------------------------------------------------------------------------------------, 30.00 ~ Q) t:: ctS :::J 0-25.00 '-E Q) a: E·· 20.00 15.00 +1------------------------------------------------------------------------------------------------------------------; 10.00 1 • 5.00 1 IT I' J'. • Dr 1'f 0.00 ...... ,-,..' ~~., .~.,., I ••• ,1F •• ii "" ,..II~ii ... ~;:w:;:; ... III. ~., ~w."".,.,,, 30~Sep~81 03~Oct~83 0?~Oct~85 09~Oct~8? 30~Oct~89 30~Sep~91 8~Oct~93 16~O 10~AI 12~o t 24~O t 3~Oct ct~95 Ivoll~9? c ~99 c ~01 ~03 30 2~Oct 0 D/~€CI /:) A 17_0C1_05 -0C/-07 -9 . "lD/A.nON Background (BHV-3) Subtracted from BHV-2 ____ BHV-2 I White Mesa Mill Ambient Gamma Levels Over Time BHV-31 50.00 ~--------------------------------------------------------------------------------------------------------------------------------------------~ 45.00 I • 40.00 I II • 35.00 I II • I I _ I I • 30.00 ..... Q) t: ~ ::J" -B" 25.00 E Q) a: E 20.00 15.00 10.00 5.00 +I--------------------------------------------------------------------------------------------~--------------------------------------1 0.00 +'~i~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 30-Sep_81 03-0Ct_83 07_0Ct_85 09-0Ct_87 30-0ct 30-Se 8-0co 9 -89 P-91 ,-3 Background (BHV-3) DIR~cr RADIA, liON 24-0ct_01 3-0ct_03 30-0ct_07 2-0ct_09 16-0ct_95 10-Nov_97 12-0ct_99 17_0ct_05 -'-BHV-3 I White Mesa Mill Ambient Gamma Levels Over Time BHV-41 50.00 ~--------------------------------------------------------------------------------------------------------------------------------~ 45.00 +I ----------------------------------------------------------------------------------~---------------------------------------------1 40.00 +1---------------------------------------------------------------------------------------------------------------------------------1 35.00 30.00 ..... Q.) t 25.00 CO ~ J! E Q.) c:: 20.00 E 15.00 10.00 5.00 1 • I ... \ 1f • , I , I 0.00 ~,~ -; , , , , ~, , , , , ¥ ' • ' .-"I ... ~ ~ .... i ' ~ ;-; ~.~ _ ' • ¥ ~ , • ' , .. ' ... i ¥ ~ W=' ~ , ,-='j-I.' .... ' ¥ • 30~Sep~81 03~Oct~83 07~Oct~85 09~Oct~87 30~Oct~89 30~Sep~91 8'Oct~93 16~Oct~95 10~Nov~97 12~Oct~99 24~Oct~01 3~Oct~03 17~Oct~05 30·0ct~07 2~Oct~09 DIR£CI RADIA, liON Background (BHV-3) Subtracted from BHV-4 r ------.-------'BHV-4 ~ Q) +-' ~ al :::s 0--.... E Q) a: E I White Mesa Mill Ambient Gamma Levels Over Time BHV-sl 50.00 ~----------------------------------------------------------------------------------------------------------~ 45.00 l,--------------------------------------------l 40.00 +1--------------------------------------------------------------------------------------------------------------------~ 35.00 +1 ----------------------------------------------------------------------------------------------------------------~ 30.00 25.00 20.00 15.00 +I----------------~------------------------------------------------------------------------------------------~ 10.00 I • 5.00 I I I ,. ... ,~. Fb~ ' .... na "... J I 1 , I :.L: II ,., II I I 0.00 ,..., M , , •• , , ••• , , • , • , , • , , • , , • , , _ , .-..r , A , 30~Sep~81 03~OCt~83 07~OCt~85 09~OCt~87 30~Oct~89 30~Sep~91 8~OCt~93 16~Oct~95 10~Nov~97 12~Oct~99 24~Oct~Ol 3~Oct~03 17~Oct~05 30~OCt~07 2~Oct~09 DIR£cr ~D IArlON Background (BHV-3) Subtracted from BHV-5 ____ BHV-5 I White Mesa Mill Ambient Gamma Levels Over Time BHV-61 50.00 45.00 40.00 35.00 30.00 Q; t ct:S 25.00 :::J 0--E -0) a: 20.00 E 15.00 10.00 5.00 0.00 ~ _.r ------- 30-Sep_81 03-0ct_83 O?-Oct_85 09-0ct_8? 30-0ct_89 30-Sep_91 8-0ct_93 16-0ct_95 10-Nov_9? 12-0ct_99 24-0ct_01 3-0ct_03 1?_Oct_05 30-0ct_O? 2-0ct-09 DIR~CI RAD/4 /JON Background (BHV-3) Subtracted from BHV-6 ---+-BHV-6 White Mesa Mill Third Quarter 2011 Environmental Spherical Gamma Monitor Results Mean Badge Number Location Control Administration Vault 1 V205 Control Room 2 BHV-6 3 Ore Stor. -Molycorp Area 4 Vanadium Precip.Area 5 Yellocake Drying Area 6 Leach 7 SAG Mill Control Room 8 Yellowcake Precip. 9 Central Control Room 10 Trommel Screen (ore pad) 11 North East Comer Ore Pad 12 Met. Lab 13 Filter Press Room 14 BHV-1 15 BHV-2 16 BHV-3 17 BHV-4 18 BHV-5 19 SAG Mill 20 Tails 21 CCD 22 North SX 23 Administration Building 24 Admin Parking Lot 25 Yellowcake Packaging 26 Yellowcake Storage 27 Bucking Room 28 Mill Lunch Room 29 South SX 30 Mtce. Super. 's Office 31 Ore Feed Grizzly 32 Scalehouse 33 Sample Plant (OBS) 34 Front Gate 45 AF -Barrel Dump Station 46 AF Circuit -South 47 AF Circuit -North 51 North Control # 1 52 North Control # 2 53 Vault 54 CaF2 Barrel Dump Station Date Issued 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 Date Returned 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 Total Days Badge at WMM 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 Ambient Dose Equivalent 38.5 58.9 34.7 827.7 195 247.2 353.2 184.7 114.8 358.8 260 81.7 178.8 39.6 33.7 31.9 33.9 40.6 424.6 89.4 122.6 84.4 42.6 109.8 1983.8 415.5 126.5 72 170.7 58.4 416 240 352.7 242.4 270.1 78.8 164.3 41.3 ,38.6 39.7 43.2 mRem/ hour mRem/Day 0.02 0.401 0.03 0.614 0.02 0.361 0.36 8.622 0.00 0.000 0.08 2.031 0.11 2.575 0.15 3.679 0.08 1.924 0.05 1.196 0.16 3.738 0.11 2.708 0.04 0.851 0.08 1.863 0.02 0.413 0.01 0.351 0.01 0.332 0.01 0.353 0.02 0.423 0.18 4.423 0.04 0.931 0.05 1.277 0.04 0.879 0.02 0.444 0.05 1.144 0.86 20.665 0.18 4.328 0.05 1.318 0.03 0.750 0.07 1.778 0.03 0.608 0.18 4.333 0.10 2.500 0.15 3.674 0.11 2.525 0.12 2.814 0.03 0.821 0.07 1.711 0.02 0.430 0.02 0.402 0.02 0.414 0.02 0.450 mReml Week 2.81 4.29 2.53 60.35 0.00 14.22 18.03 25.75 13.47 8.37 26.16 18.96 5.96 13.04 2.89 2.46 2.33 2.47 2.96 30.96 6.52 8.94 6.15 3.11 8.01 144.65 30.30 9.22 5.25 12.45 4.26 30.33 17.50 25.72 17.68 19.69 5.75 11.98 3.01 2.81 2.89 3.15 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 54 White Mesa Mill Fourth Quarter 2011 Environmental Spherical Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Corner Ore Pad Met. Lab Filter Press Room BHV-l BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control # 2 Vault CaF2 Barrel Dump Station Date Issued 10110/2011 10/10/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10/10/2011 10/10/2011 10110/2011 10/10/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10/10/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10110/2011 10/10/2011 10/10/2011 10110/2011 10/10/2011 10/10/2011 10110/2011 10110/2011 10110/2011 Date Returned 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12130/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12130/2011 Total Days Badge at WMM 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 . 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 81 Mean Ambient Dose Equivalent 34.5 48.7 29.9 1273.2 84.7 205.3 218 325.1 138.8 75.7 142.8 146.7 57 115 31.5 25.9 27.4 27.7 29.9 495.5 42.1 74.4 60.6 36.8 81.7 1052.4 292.9 101.9 54.1 130.7 44.4 333.5 182.1 261.4 175.1 206.3 62.4 123 31.7 27.7 26.1 435.7 mReml hour 0.02 0.03 0.02 0.65 0.04 0.11 0.11 0.17 0.07 0.04 0.07 0.08 0.03 0.06 0.02 0.01 0.01 0.01 0.02 0.25 0.02 0.04 0.03 0.02 0.04 0.54 0.15 0.05 0.03 0.07 0.02 0.17 0.09 0.13 0.09 0.11 0.03 0.06 0.02 0.01 0.01 0.22 mRem/Day 0.426 0.601 0.369 15.719 1.046 2.535 2.691 4.014 1.714 0.935 1.763 1.811 0.704 1.420 0.389 0.320 0.338 0.342 0.369 6.117 0.520 0.919 0.748 0.454 1.009 12.993 3.616 1.258 0.668 1.614 0.548 4.117 2.248 3.227 2.162 2.547 0.770 1.519 0.391 0.342 0.322 5.379 mReml Week 2.98 4.21 2.58 110.03 7.32 17.74 18.84 28.10 12.00 6.54 12.34 12.68 4.93 9.94 2.72 2.24 2.37 2.39 2.58 42.82 3.64 6.43 5.24 3.18 7.06 90.95 25.31 8.81 4.68 11.30 3.84 28.82 15.74 22.59 15.13 17.83 5.39 10.63 2.74 2.39 2.26 37.65 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAlQC (Log Scale) <=> <=> <=> <=> <=> <=> <=> 0 0 0 0 0 0 0 m m m m m m m 6 6 6 6 6 6 6 ex> '" 0> c..n +:>. w I\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 i ~~ :c S» I 8/27/1989 ~ I ~~ I\) I\) 0) 8/27/1990 ~ ~ 0 0 8/27/1991 ~ Jr-~ :::s 0 (I) 8/27/1992 ~ -, ~ ~ :::s ,.. ""t 8/27/1993 S» ,.. O· t 8/27/1994 :::s 0 z 8/27/1995 :::s m < 8/27/1996 (I) (Q T (I) ,.. 8/27/1997 S» ,.. z O· ~ 8/27/1998 :::s -8/27/1999 s:::: t 0 :::::: 8/27/2000 '" C/) (Q ~ -8/27/2001 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 (Log Scale) (:) (:) (:) (:) (:) (:) (:) 0 0 0 0 0 0 0 m m m m m m m " 6 6 6 6 6 6 6 ex> -....,J Q) (J1 .J::>. (..:) I\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 i --------'i" "'C C" 8/27/1989 ~ .... ~ I I\) ..... 0 8/27/1990 ~ IE ~ 1 0 0 8/27/1991 ~ I" ::::J (") (1) 8/27/1992 ~ ..... 1_ r-~ ::::J .... "'" 8/27/1993 Q) .... o· t 8/27/1994 ::::J tn z 8/27/1995 ::::J m < 8/27/1996 (1) (Q T (1) .... 8/27/1997 Q) .... z o· :2: 8/27/1998 ::::J -8/27/1999 i J I" ~ c: f 0 , 8/27/2000 " (j) (Q :2: -8/27/2001 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 (Log Scale) ..... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m 6 6 6 6 6 6 6 ex> ---J (j) (J1 ~ c..u I\.) 01-Jan-81 01-Jan-82 ~ Ir fl I :e :I: 01-Jan-83 ~ I =i m 01 -Jan-84 s:: m 01-Jan-85 ~ ~I en » 01-Jan-86 s:: 01-Jan-87 -t ~ r-r- 01-Jan-88 -t ~ 1 --PI Z 0 01 -Jan-89 -t I----....~ :IJ -I 01-Jan-90 -t 1 ~ :I: m 01-Jan-91 » en -I 01-Jan-92 0 t ." 01 -Jan-93 s:: JJ 01-Jan-94 r- ~ -r-N f,:IJ I\) 01-Jan-95 0> _.0) ....... I T "I\) 01 -Jan-96 (QI\) -0') 'lJ 01-Jan-97 0) 0-::J N Co ...... 0 01 -Jan-98 ""CJ tT 01-Jan-99 -t ~ I I\) ...... 01-Jan-OO -t ..-=:: 0 0 01-Jan-01 -t V .....-0 ::J (") 01-Jan-02 -t ~~ (1) ::J ,.. 01-Jan-03 -t ~ .r-"""t 0) ,.. 01 -Jan-04 ~ ~ o· ::J tn 01-Jan-05 ::J 01-Jan-06 -t --~I < (1) (Q 01 -Jan-07 -t ---I --- (1) ,.. 0) 01 -Jan-08 -t ...... 1 .........-,.. o· ::J 01 -Jan-09 01-Jan-10 01 -Jan-11 (Log Scale) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m 6 6 6 6 6 6 6 co '-I (J) 01 ~ W I\) 01-Jan-81 :e 01-Jan-82 l J.../'~ ~I ::J: =i 01-Jan-83 l ...... ~ 1 m s: 01-Jan-84 l ......... ~ m en 01-Jan-S51 » s: 01 -Jan-86 • • 01 -Jan-87 Z 01-Jan-88 l ~ I ~ 0 :0 01-Jan-89 l I~~ -4 ::J: 01 -Jan-90 l /.........,. :e m 01 -Jan-91 l ~r----....~ en -4 01-Jan-92 0 t ." 01-Jan-93 s: JJ • Sl> 01-Jan-94 c-. r:., I\) 0:0 0> 01-Jan-95 _.S» "-. T "I\) 01 -Jan-96 CCI\) -0) ""0 S» 0" 01-Jan-97 ::s r:., ...... Q. 0 ""C 01-Jan-98 C'" • 01-Jan-99 l ~1 7 I\) ~ 0 01-Jan-OO -j --0 0 01-Jan-01 l _I .-==::: ::::::a::: • ::s (") 01-Jan-02 l ",""a..,.L (I) ::s ... .., 01-Jan-03 l • ..... 1·-" S» ... 01-Jan-04 ~ 51::: I o· • ::s tn 01-Jan-05 ::s 01-Jan-06 l -"\:sl < -(I) CC 01-Jan-07 l ~ ~ (I) ... S» ... 01-Jan-08 I I ~I o· ::s 01-Jan-09 01 -Jan-10 01-Jan-11 • • !; I • ,---_. (Log Scale) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m m m 6 6 6 6 6 6 6 6 + 0 ()) -....,J 0'> CJ1 ~ VJ I\) --'" 0 01-Jan-81 ::E 01-Jan-82 l IL'" I ~ ::t: =i 01-Jan-83 l -.......... -r---.-m s: 01-Jan-84 l ~I ~ m en 01-Jan-S5 1 ~ l> s: 01 -Jan-86 .... .... 01-Jan-87 en 01-Jan-88 l I ... 1 , 0 C 01-Jan-89 l '\.. 1-~ -I ::t: 01-Jan-90 l / 1 .,. ::E m en 01-Jan-91 -I 0 01-Jan-92 t " 01-Jan-93 s: :D .... Sl) -C"" r\, 01-Jan-94 I\) OJ] 0> _.0) 01-Jan-95 ....... T "I\) (QI\) 01-Jan-96 -0) "'U 0) 0-01-Jan-97 :::s ~ c. 0 "tJ 01 -Jan-98 C'" • 01-Jan-99 ~ Ikdf I I\) ...... 0 01-Jan-OO 0 0 01-Jan-01 l -I' III :::s (") CD 01-Jan-02 l ~~ :::s ... ~ 01-Jan-03 l .:l :lilt 1 ~ 0) ... o· 01 -Jan-041 :::s en 01-Jan-05 :::s < 01-Jan-06 CD (Q 01-Jan-07 l ~I II CD ... 0) ... 01-Jan-08 I 1 o· :::s 01 -Jan-09 01-Jan-10 01-Jan-11 WHITE MESA MILL FORAGE RADIONUCLIDE DATA TABLE USED FOR MAKING GRAPHS SAMPLEDQTR SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd'8S 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0ct-8S 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 lO-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 lO-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S ll-Apr-9S 2nd'9S 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 lS-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 2nd '00 22-Juf,l-00 . NE 3.90E-04 L40E-04 L31E-04 L60E-04 2.67E-06 9.36E-OS L12E-04 L09E-04 3.47E-04 S.61E-04 LOSE-03 8.20E-OS L1SE-04 S.72E-04 S.01E-04 8.70E-04 S.90E-04 L60E-04 2.lOE-04 4.S0E-04 3.20E-OS S.60E-04 1.50E-04 6.00E-04 2.60E-04 L80E-04 L60E-04 L20E-04 9.10E-OS 4.S0E-04 3.60E-OS LOOE-OS 7.90E-OS 3.70E-OS 3.00E-OS 6.60E-OS L80E-04 L71E-OS 2.40E-04 6.70E-OS LSOE-OS S.50E-OS S.20E-OS 3.00E-OS Ll0E-OS LlOE-OS 8.00E-06 9.lOE-OS L80E-OS S.70E-OS 2.00E-04 6.03E-OS 2.30E-OS LSOE-04 L20E-06 Ra-226 Pb-210 NW SW NE NW SW 2.73E-03 9.50E-04 LlOE-03 7.10E-03 LSOE-04 2.00E-04 3.00E-OS 6.80E-04 8.30E-04 LSOE-04 L04E-04 L37E-OS 4.90E-04 6.40E-04 3.80E-04 2.00E-OS 3.40E-04 8.00E-04 2.20E-04 3.68E-03 2.36E-06 L7SE-OS L08E-04 8.00E-OS 7.92E-04 8.58E-OS 7.13E-04 4.97E-04 3.53E-04 2.51E-03 L19E-04 S.39E-OS L84E-04 1.58E-04 6.88E-04 9.78E-OS 6.40E-OS 7.80E-04 2.16E-03 L20E-03 2.08E-04 8.27E-OS 3.7SE-03 L60E-03 L80E-03 6.0SE-04 2.72E-04 7.82E-03 2.58E-03 4.70E-03 Ll0E-04 4.73E-04 3.22E-03 8.63E-04 7.07E-04 6.10E-OS 6.60E-OS 7.70E-04 4.90E-04 L07E-04 2.83E-04 S.10E-04 3.80E-04 LSOE-03 8.86E-04 LS7E-04 2.49E-03 4.40E-03 4.14E-03 6.66E-04 3.78E-04 1.57E-03 4.78E-03 L6SE-02 S.20E-04 2.60E-04 6.80E-04 L70E-03 L70E-03 4.10E-04 4.lOE-04 LSOE-03 L60E-03 2.20E-03 L60E-04 2.90E-04 9.50E-04 S.SOE-04 7.50E-04 3.60E-04 L80E-04 L70E-03 L80E-03 2.40E-03 2.60E-04 2.30E-04 L40E-03 L90E-03 2.90E-03 3.10E-OS LSOE-04 1.50E-04 L60E-04 4.30E-03 6.20E-04 3.lOE-04 LlOE-03 L70E-03 4.20E-03 3.40E-04 L30E-04 2.30E-04 7.40E-04 1.50E-03 S.10E-04 4.30E-04 2.04E-03 LOOE-03 3.50E-03 3.60E-04 2.S0E-04 3.30E-04 4.80E-04 2.39E-03 L70E-04 LlOE-04 3.20E-04 3.20E-04 6.60E-04 8.80E-OS 6.lOE-OS 3.30E-04 2.90E-04 6.10E-04 3.00E-04 3.40E-OS 3.00E-04 4.lOE-04 2.20E-04 3.10E-04 8.00E-OS L90E-04 4.70E-04 L20E-04 S.00E-04 6.S0E-OS L09E-03 LSOE-03 9.10E-04 2.00E-OS L60E-OS LSOE-04 9.60E-OS 3.20E-04 6.50E-06 L90E-OS 7.50E-OS L20E-04 2.20E-04 L20E-04 L60E-OS 7.10E-04 L21E-03 7.60E-04 L80E-OS 2.60E-OS 2.80E-04 2.lOE-04 3.40E-04 S.20E-OS 3.00E-OS 4.30E-OS L70E-OS S.10E-OS 3.lOE-OS S.30E-04 7.lOE-04 4.20E-04 L20E-04 2.00E-OS 4.40E-04 9.80E-04 3.90E-04 3.73E-OS L7SE-OS 3.00E-OS 7.80E-OS L30E-04 2.40E-04 LOOE-04 L70E-04 2.60E-04 2.60E-04 8.40E-OS L70E-OS L40E-04 L20E-04 L60E-04 L90E-OS 6.40E-06 S.10E-OS 4.50E-OS 4.40E-OS L20E-04 2.30E-OS 6.70E-OS LOOE-OS 6.60E-OS 8.30E-OS 4.20E-OS 3.20E-OS 6.80E-OS LOOE-04 3.60E-OS 2.10E-OS 1.40E-04 8.50E-OS L90E-04 3.30E-OS S.50E-06 4.lOE-OS 4.40E-OS 3.30E-OS S.40E-06 S.30E-06 2.10E-OS 3.20E-OS L90E-OS 8.90E-06 2.50E-OS L40E-04 3.40E-04 L30E-04 9.20E-OS 7.90E-OS 4.S0E-04 4.60E-04 3.90E-04 6.50E-08 3.60E-07 4.00E-OS 3.20E-07 L70E-07 4.20E-OS 4.30E-OS 8.70E-OS L70E-04 2.50E-04 6.20E-OS 2.40E-OS 3.00E-04 L40E-04 L70E-04 S.4SE-OS 2.23E-OS L40E-04 9.20E-OS 2.30E-04 LlOE-04 LSOE-04 2.10E-OS 2.80E-OS L70E-OS 3.70E-OS LOOE-04 L60E-04 2.70E-04 LlOE-04 2.90.E-OS · L30E-06 L60E-04 2.80E-04 2.00E-04 WHITE MESA MILL FORAGE RADIONUCLIDE DATA TABLE USED FOR MAKING GRAPHS SAMPLED QTR SAMPLED DATE 4th '00 21-Dec-00 1st '01 30-Apr-01 2nd '01 14-Jun-01 4th '01 17-Dec-01 1st '02 07-May-02 2nd '02 07-Jul-02 4th '02 lS-Dec-02 1st '03 21-Mar-03 2nd '03 10-Jun-03 4th '03 20-Nov-03 1st '04 OB-Apr-04 2nd '04 12-Jun-04 4th '04 30-Nov-04 1st 'OS 21-Apr-OS 2nd 'OS 13-Jun-OS 4th 'OS lO-Nov-OS 1st '06 03-Apr-06 2nd '06 16-Jun-06 4th '06 2B-Nov-06 1st '07 30-Mar-07 2nd '07 1-Jun-07 4th '07 23-Nov-07 1st 'OB 22-Apr-OB 2nd 'OB 1B-Jun-OB 4th 'OB 12-Dec-OB 1st '09 2B-Apr-09 2nd '09 17-Jun-09 4th '09 1B-Dec-09 1st'lO 13-May-10 2nd '10 1B-Jun-10 4TH '10 20-Dec-lO 2nd '11 23-Jun-ll 3rd ' 11 27-Jul-ll 4th '11 23-Nov-ll Ra-226 NE NW 1.60E-06 2.30E-06 1.00E-06 2.lOE-OS 2.30E-06 1.30E-06 9.lOE-06 3.70E-OS 3.30E-OS 4.90E-OS S.SSE-OS B.BBE-OS 7.7SE-OS 1.S0E-04 9.lOE-06 S.OOE-OS 2.50E-OS S.60E-OS S.70E-OS 3.20E-04 9.3BE-OS 6.29E-OS S.63E-OS 6.51E-OS B.41E-OS 7.50E-OS S.60E-OS 4.90E-OS 9.lOE-06 2.30E-OS 6.00E-OS 7.40E-OS B.OOE-OS 1.00E-04 4.lOE-OS 9.S0E-OS 1.17E-04 4.30E-OS 9.70E-OS S.10E-OS 1.30E-OS 7.30E-OS 7.00E-OS 6.6E-06 3.6E-06 2.BE-06 3.2E-OS 3.2E-06 1.S0E-04 7.3E-OS S.9E-04 S.3E-OS 1.9E-OS 1.6E-06 1.70E-04 S.5E-OS 2.2E-04 1.9E-04 6.5E-OS 2.3E-OS 2.3E-OS B.6E-06 2.4E-07 2.lE-07 4.9E-06 4.2E-06 7.2E-06 7.7E-06 Pb-210 SW NE NW SW 1.20E-06 S.10E-OS 3.30E-04 1.20E-04 1.BOE-06 1.20E-06 7.60E-07 B.30E-07 2.60E-06 3.BOE-06 1.BOE-06 1.10E-06 2.63E-06 3.57E-OS 6.72E-OS 9.40E-OS 3.50E-OS 4.S0E-OS 1.2BE-04 1.36E-04 4.02E-OS S.31E-OS B.33E-OS 7.04E-OS B.lOE-OS 1.29E-04 3.16E-04 2.B7E-04 3.70E-OS 1.13E-OS 4.20E-06 2.69E-OS 1.30E-OS 3.26E-06 1.BBE-04 1.00E-07 1.60E-04 4.0SE-OS 4.B9E-04 1.42E-04 1.40E-04 S.BBE-OS 1.94E-OS 6.lOE-06 6.S1E-OS 6.42E-OS 1.B7E-OS S.27E-OS B.40E-OS 2.4BE-04 4.4SE-04 3.39E-04 1.70E-OS S.BOE-OS 1.27E-04 4.50E-OS 1.S0E-OS 1.lOE-OS 4.70E-OS 7.00E-OS 3.BOE-OS 1.70E-06 2.40E-06 1.20E-06 1.00E-04 3.40E-04 6.54E-04 3.30E-04 3.40E-OS 1.16E-04 4.4BE-04 1.37E-04 7.31E-OS 3.2BE-04 3.2SE-04 2.9BE-04 3.00E-OS 3.40E-04 2.64E-04 3.20E-04 1.10E-04 1.20E-04 S.30E-04 3.20E-04 S.60E-OS S.00E-04 7.00E-04 6.40E-04 3.20E-OS 2.3E-04 4.40E-04 2.30E-04 1.20E-OS 6.9E-OS 1.40E-04 S.OOE-OS 9.20E-OS 3.60E-04 4.40E-04 9.6E-07 2.60E-OS 3.4E-04 1.90E-04 3.70E-OS 2.40E-OS 3.6E-OS 4.30E-OS 3.50E-OS 3.1E-OS 4.BOE-04 3.0E-04 2.lE-04 2.00E-OS 1.9E-04 S.10E-04 S.60E-OS 1.10E-OS 1.4E-04 B.30E-OS 7.BOE-OS 6.70E-06 1.0E-OS 1.10E-07 B.00E-07 1.7E-07 2.9E-06 2.2E-06 2.5E-06 1.6E-OS 9.5E-OS 2.3E-04 9.SE-OS 7.BE-07 7.2E-07 S.BE-07 S.9E-07 l'IWW.energylab.com r----· Hele;;'-MT 877-'472-"0711 .Billings~T 800-735=4489 • C;;e~ 888-235-0515' AnalyticalfxcstlsncB Sincsl952 J 'Gillette, WY 866-686-1175 (,I Rapid City, SD 888-672-1225 t. College Station, IX 888-690-2218 September 13, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11 071 050 ANAL VTICAL SUMMARY REPORT Project Name: 2nd Vegetation Sample 2011 Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 7/28/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 071 050-001 North West 07/27/11 9:50 07/28/11 Vegetation Digestion, Radiochemistry Lead 210 Radium 226 C11 071 050-002 North East 07/27/11 8:45 07/28/11 Vegetation Same As Above C11 071 050-003 South West 07/27/11 8:00 07/28/11 Vegetation Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the ONOC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as received basis unless otherwise indicated. Samples corrected for dry weight indicate units that have -dry appended. If you have any questions regarding these test results, please call. Report Approved By: cS¥~D tJ~'Y Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.09.13 15:54:50 -06:00 Page 1 of 9 ,_ .•. _ .. __ .. _----'---_. -. ------------------ www.energylab.com Analytical Exestlence Since '952 Helena, MT 877 -472 .. 0711 U Billings, MT 800-735-4489 11 Casper, WY 888-235-0515 Gillette, WY 866-686-7175 " Rapid City, SD 888-672-1225 • College Station, lX888-690-2213 CLIENT: Denison Mines USA Corp Project: 2nd Vegetation Sample 2011 Report Date: 09/13/11 Sample Delivery Group: C11 071 050 CASE NARRATIVE BRANCH LABORATORY SUBCONTRACT ANALYSIS Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4°C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of ,exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All sarryples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of9 I'IWW.energylab.com Analytical Excellsnce Sincs 1.952 [ -------_._._--_._------ Helena, MT 877-472-0711 • Billings, MT 800-135-4489 1) Casper, WY 888-235-0515 Gillette, WY 866-686-7175 Iff Rapid City, SD 888-672-1225 a College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 2nd Vegetation Sample 2011 C11 071 050-001 Client Sample 10: North West Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 2.3E-04 2.5E-06 2.3E-06 235 2.5 2.3 4.2E-06 5.4E-07 2.7E-07 4.2 0.54 0.27 MOC -Minimum detectable concentration Units uCilkg uCilkg uCi/kg pCi/kg pCilkg pCilkg uCi/kg uCi/kg uCilkg pCilkg pCilkg pCi/kg Qualifier Rl Report Date: 09/13/11 Collection Date: 07/27/11 09:50 DateReceived: 07/28/11 Matrix: Vegetation MCL! QCl Method Analysis Date 1 By E909.0 08/29/1 1 02:51 / eli-cs E909.0 08/29/11 02:51 1 eli-cs E909.0 08129/11 02:51 1 eli-cs E909.0 08129/11 02:51 1 eli-cs E909.0 08/29/11 02:51 1 eli-cs E909.0 08/29/11 02:51 1 eli-cs E903.0 08124/11 12:23 1 trs E903.0 08124/11 12:231 trs E903.0 08/24/11 12 :23 1 trs E903.0 08/24/1 1 12 :23 1 trs E903.0 08/24/11 12:231 trs E903.0 08124/11 12:231 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of9 www.energylab.com Analytical Excsllsnc8 Sincs 1952 J-_. __ . __ .. --. -----.. --------~ Helena, MT 877-472-071 1 II Billings, MT 800'-735-4489 ~ Casper, WY 888-235-0515 Gillette, WY 866-69S-7175 g Rapid City, SD 888-672-1225 Ii College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 2nd Vegetation Sample 2011 C11 071 050-002 Client Sample 10: North East Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 9.5E-05 2.1 E-06 2.5E~06 95.5 2.1 2.5 4.9E-06 6.3E-07 3.2E-07 4.9 0.63 0.32 Units uCilkg uCi/kg uCilkg pCi/kg pCi/kg pCi/kg uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg MOC -Minimum detectable concentration Qualifier RL Report Date: 09/13/11 Collection Date: 07/27/11 08:45 DateReceived: 07/28/11 Matrix: Vegetation MCL! QCL Method Analysis Date 1 By E909.0 08/29/11 18:21 1 eli-cs E909.0 08129/1 1 18:21 1 eli-cs E909.0 08/29/11 18:21 1 eli-cs E909.0 08129/11 18:21 1 eli-cs E909.0 08129/11 18:21 1 eli-cs E909.0 08129/11 18:21 1 eli-cs E903.0 08124/11 12:231 trs E903.0 08124/11 12:231 trs E903.0 08124/11 12:231 trs E903.0 08124/11 12:231 trs E903.0 08124/11 12:231 trs E903.0 08124/11 12:231 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of9 WNW.energylab.com Analytical Excsl/snce Sines '952 f _ .. _" __ T.-_._. __ ..... ____ ... _________ -..-. ___ • __ _ '~, Helena, Ml 871-472-0711 fl Billings, Ml 800-735-4489 I) Casper, WY 888-235-0515 , Gillette, WY 866-686-1175 • Rapid City, SD 888-672-1225 It College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 2nd Vegetation Sample 2011 C11 071 050-003 Client Sample ID: South West Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 9.5E-05 1.6E-06 1.7E-06 95.2 1.6 1.7 1.6E-05 1.0E-06 2.6E-07 16.0 1.0 0.26 Units uCi/kg uCilkg uCi/kg pCi/kg pCilkg pCi/kg uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCilkg MOC -Minimum detectable concentration Qualifier Rl Report Date: 09/13/11 Collection Date: 07/27/11 08:00 DateReceived: 07/28/11 Matrix: Vegetation MCL! aCl Method Analysis Date 1 By E909.0 08130/11 09:51 1 eli-cs E909.0 08/30/11 09:51 1 eli-cs E909.0 08130/11 09:51 1 eli-cs E909.0 08130/11 09:51 1 eli-cs E909.0 08/30/11 09:51 1 eli-cs E909.0 08130/11 09:51 1 eli-cs E903.0 08124/11 12:231 trs E903.0 08124/11 12:23 1 trs E903.0 08124/11 12:231 trs E903.0 08124/11 12:231 trs E903.0 08124/11 12:23 1 trs E903.0 08/24/11 12:23 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of9 www.energylab.com Analytical Excsllence Sincs 1952 Helena, MT 877·472-[}711 81 Billings, MT 800-735-4489 {I Casper, WY 888-235-0515 Gillette, Wy 866-686-7175 • Rapid City, SO 888-672-1225 II College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Vegetation Sample 2011 Analyte Method: E903.0 Sample 10: LCS-30749 Radium 226 Sample 10: MB-30749 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C11080290-001AMS Radium 226 Count Result Units 3 Laboratory Control Sample 1.5E-05 uCilkg Method Blank 6E-07 uCilkg 3E-07 uCi/kg 4E-07 uCilkg Sample Matrix Spike 850 pCi/g-dry Report Date: 09/13/11 Work Order: C11 071 050 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-1_110817B 130 70 130 Run: BERTHOLD 770-1 110817B Run: BERTHOLD 770-1_110817B 1390 70 130 Batch: R149852 08/24/11 12:23 08/24/11 12:23 08/24/11 12:23 S -Sample activity for this radionuclide is much larger than the spike activity added. Therefore the matrix spike recovery could not be calculated. The LCS is acceptable; this batch is approved. Sample 10: C11080290-003AOUP 3 Sample Duplicate Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 220 pCi/g-dry 1.3 pCi/g-dry 0.034 pCi/g-dry Run: BERTHOLD 770-C110817B 3.8 ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 08/24/11 13:56 11.2 Page 6 of 9 I'IWW.energylab.com Analytical ExesllSflCB Sines '952 f -------~--..... ..-..-.--,.---.----. . ... Helena, MT 877-472-0711 e Billings, MT 800-735-4489 11 Casper, WY 888-235-0515 . Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 e College station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Vegetation Sample 2011 Analyte Count Result Units Method: E909.0 Sample 10 : C11071050-003AMSO Lead 210 Sample 10 : C1 1071050-003AMS Lead 210 Sample 10: LCS-14666 Lead 210 Sample 10 : MB-14666 Lead 210 Lead 210 precision (±) Lead 210 MDC Lead 210 precision (±) altu Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike Duplicate 0.00026 uCilkg Sample Matrix Spike 0.00026 uCilkg Laboratory Control Sample 0.00062 uCilkg 4 Method Blank 3E-06 uCilkg 4E-06 uCi/kg 6E-06 uCilkg 4 pCilkg MDC -Minimum detectable concentration RL Report Date: 09/13/11 Work Order: C11 071 050 %REC Low Limit High Limit RPO RPOLimit Qual Batch: T _14666 Run: SUB-T41959 08/31/11 17:51 89 70 130 0.9 11.7 Run: SUB-T41959 08/31/11 02:21 90 70 130 Run: SUB-T41959 08/28/11 11 :21 100 70 130 Run: SUB-T41959 08/27/11 20:51 U NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 7 of9 www.energylab.com Analytical Exesllence Sincs 1952 r --· ----.----------,-------.-.-- . Helena, MT 877-472-0711 It Billings, MT 800-735-4489 It Casper, WY 888-235-0515 _" Gillette, WY 866-686-7175 " Rapid City, SO 888-672-1225 u College Statinn, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C1 1071050 Login completed by: Corinne Wagner Reviewed by: BL2000\alynch Reviewed Date: 8/1/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' N/Ne Yes 0 Yes 0 Date Received: 7/28/2011 Received by: kg No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 NoD No 0 Carrier Next Day Air name: Not Present D Not Present D Not Present 0' No VOA vials submitted 0' Not Applicable 0' Page 8 of 9 "1J 0) <D CD CD 0 -.. CD lugr,eay Chain of Custody and Analytical Request Record Page_J_of~ .'«·';1#"-#114., Compa~me: d-)eA1; ~{J~ m ,;""e-,l Report Mail Add~~S(s c-vy.. 8-{/1 fDa~I;"C,t1Tk"'{rlJ Invoice Address: ~ $c.~ Special Report/Formats: DDW D POTWIVVWTP o State: D Other:---- o EDD/EDT(Electronic Data) Format: ___ _ o LEVEL IV D NELAC PLEASE PRINT (PrQ"ide as much information as possible.) Project Name, PWSr perm.it, Etc. . I Sample Origin ;2Y'A \ I~(I LhJ"1;~ S(JJ~L~l1 State: LA T EPA/State Compliance: Yes 0 No 0 Contact Name: I PhonefFai: Email: )2tJ\-< g/~-L ,'It!' Z'ZZ/ Sampler: (Please Prjnt) ~~f,Jt4~i~ Invoice tontact & Phone: Purchase Order: Quote/Bottle OrdeJJ .~~ Shipped by: 5: CI ~ ~o tJ)jg ~1D~OII... '-> 0 >,.$ ~(/)en C'Q ~ o ~~::> u:S;:'o C'Q 0) ...... oCt: enl.Q .5 o ....... Ollt§ &G[l&{1 W@D@ OO~@l1D~~1]) • ~I R Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page ~5~~ 09rI0(8): m &"* § '':: .c :>">1= a EF-> C'Q I ;:,~:31D $: z o. ........ I~Cl § >1 en c w ::r: 0 « I-~ W w CIJ f'J ....... ~ c "0 C ~ I U eo c S ~ I 5 co "0 C eo ... ~ Comments: Receipt Temp UIA-9 C On Ice: y () Custody Seal On Bottle Y N On Cooler Intact SAMPLE IDENTIFICATION ColI~tion 1 MATRIX Time 001 H ~: Signature (bN Match ~~""' ~ Xix XI~ xix 5 -6 -7 -8 -9 -10 Record Relinquish1 by (print): DatelTime: F Re~y (pnnr-i _.--. ----Oate7Time: J/>t3 'C:::::;A'" (..,.A.J~ TJltr-l/i ~ &nature: Received by (print): Date/Time: Received by (print): Oate/Time: I~ I~ ~ ~ I~ I~ ~ ~/l\ (6)ut01I asD ~ Igs to) rcfo1 I~ I~ Signafure: Signature: ~ustOdY MUST be KGC'IIVed by LabOratory: Signed Samj)I~Disposal: Return to Client: Lab Disposal: Uatetllme: ,.~,> .. ·l{ q to ~jgj,(;:r ~ K1tt.5it.{ ~: ~ r v In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested, This serves as notice of this possibility, All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.eneraylab.com for additional information, downloadable fee schedule. forms, and links. -------(jirl'" www.energylab.comHelena.MY877-472-071t -Biliings.MT 800-735-4489 -Casper, WY 888-235-0515 . .:-~ Anslytica/ ExcsllsnclJ Sines 1952~iUette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, 1)( 888-690-221 a ====~----------------~------~~~----------~~~------------~--~--------- EN:RGY I..ASORATORIES ANAL VTICAL SUMMARY REPORT February 09,2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11110979 Project Name: Late Fall Vegetation Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 11/29/2011 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C11110979-001 North East 11/23/11 9:00 11/29/11 Vegetation Digestion, Radiochemistry Lead 210 Radium 226 C11110979-002 North West 11/23/11 10:00 11/29/11 Vegetation Same As Above C11110979-003 South West 11/23/11 11 :00 11/29/11 Vegetation Same As Above The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: cS¥~D tJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.02.09 13:35:19 -07:00 Page 1 of 9 www.energyJab.com Analytical ExcsllBflCB SinCll '952 Helena, MT 877-472-0711 • Billings, MT 801l-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 CLIENT: Denison Mines USA Corp Project: Late Fall Vegetation Report Date: 02/09/12 Sample Delivery Group: C11110979 CASE NARRATIVE BRANCH LABORATORY SUBCONTRACT ANALYSIS Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 9 www.energylab.com Analytical ExcsllsncB Sines 1952 r -----,,' Helena, MT 877-472-0711 • Billings, MT 801J-735-4489 . Casper, WY 888-235-0515 ,_ ..~illette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 EN:RGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Late Fall Vegetation C11110979-001 Client Sample ID: North East Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 8.8E-08 4.3E-07 7.2E-07 0.088 0.43 0.72 7.2E-06 7.5E-07 2.9E-07 7.2 0.75 0.29 MOC -Minimum detectable concentration Units uCi/kg uCi/kg uCilkg pCi/kg pCi/kg pCi/kg uCi/kg uCi/kg uCilkg pCilkg pCi/kg pCilkg Report Date: 02/09/12 Collection Date: 11/23/11 09:00 DateReceived: 11/29/11 Matrix: Vegetation MCL! Qualifier Rl QCl Method Analysis Date 1 By U E909.0 01129/12 12:581 eli-cs E909.0 01129/12 12:581 eli-cs E909.0 01/29/12 12:581 eli-cs U E909.0 01/29/1212:581 eli-cs E909.0 01/29/1212:581 eli-cs E909.0 01/29/12 12 :58 1 eli-cs E903.0 12128/11 15:451 trs E903.0 12128/11 15:451 trs E903.0 12/28/11 15:451 trs E903.0 12/28/11 15:451 trs E903.0 12128/11 15 :45 1 trs E903.0 12/28/11 15:451 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 3 of 9 . E~RGY LABORATORIES www.energy.ab.com 1; Analytical Excsllsnc8 Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .~illette, WY 866-686-7175 • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp Late Fall Vegetation Lab lD: C 1111 0979-002 Client Sample ID: North West Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -1.1E-06 3.4E-07 5.8E-07 -1.1 0.34 0.58 7.7E-06 6.8E-07 2.3E-07 7.7 0.68 0.23 MOC -Minimum detectable concentration Units uCi/kg uCilkg uCi/kg pCi/kg pCi/kg pCi/kg uCilkg uCilkg uCilkg pCi/kg pCi/kg pCi/kg Report Date: 02/09/12 Collection Date: 11/23/11 10:00 DateReceived: 11/29/11 Matrix: Vegetation MCL! Qualifier RL QCL Method Analysis Date I By U E909.0 01/30/1201 :03 1 eli-cs E909.0 01/30/1201 :03 1 eli-cs E909.0 01/30/1201 :03 1 eli-cs U E909.0 01/30/1201 :03 1 eli-cs E909.0 01/30/1201 :03 1 eli-cs E909.0 01/30/12 01 :03 1 eli-cs E903.0 12/28/11 15:45 1 trs E903.0 12/28/11 15:451 trs E903.0 12/28/11 15:45 1 trs E903.0 12128/11 15:451 trs E903.0 12128/11 15:451 trs E903.0 12128/11 15:451 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration . Page 4 of9 EI\ERGY LABORATORIES www.energylab.com Analytical Excsllence Sincs 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp Late Fall Vegetation LablD: C 1111 0979-003 Client Sample ID: South West Analyses RADIONUCLIDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MOC Lead 210 altu Lead 210 precision (±) altu Lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: RL -Analyte reporting limit. QCl -Quality control limit. Result -5.0E-07 3.5E-07 5.9E-07 -0.50 0.35 0.59 7.8E-07 2.5E-07 2.3E-07 0.78 0.25 0.23 MOC - Minimum detectable concentration Units uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg uCilkg uCilkg uCi/kg pCi/kg pCi/kg pCilkg Report Date: 02/09/12 Collection Date: 11/23/11 11 :00 DateReceived: 11/29/11 Matrix: Vegetation MCL! Qualifier Rl QCl Method Analysis Date 1 By U E909.0 01/30/1213:081 eli-cs E909.0 01/30/12 13 :08 1 eli-cs E909.0 01/30/1213:081 eli-cs U E909.0 01/30/12 13:081 eli-cs E909.0 01/30/1213:081 eli-cs E909.0 01/30/1213:081 eli-cs E903.0 12/28/11 15:45 1 trs E903.0 12/28/11 15 :45 1 trs E903.0 12128/11 15:451 trs E903.0 12128/11 15:451 trs E903.0 12128/11 15:451 trs E903.0 12/28/11 15 :45 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 5 of 9 EI\ERGY LABORATORIES www.energylab.com Analytical ExcsllsncB Sim:. 1952 Helena, MT 877-472-071 1 " Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 866-6B6-7175 • Rapid City, SD 888-672-1225 .. College Station, IX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Late Fall Vegetation Analyte Count Result Units Method: E903.0 Sample 10: C1111 0943-006AMS Radium 226 Sample 10: C1 1110943-006AMSO Radium 226 Sample 10: LCS-32126 Radium 226 Sample 10: MB-32126 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike 2.0 pCi/g-dry Sample Matrix Spike Duplicate 2.1 pCi/g-dry Laboratory Control Sample 0.29 pCi/g-dry 3 Method Blank 1.0E-05 pCi/g-dry 0.0001 pCi/g-dry 0.0002 pCi/g-dry MDC -Minimum detectable concentration Report Date: 02/09/12 Work Order: C11110979 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: RA226-5754 Run: BERTHOLD 770-2_111216A 12/28/11 14:13 85 70 130 Run: BERTHOLD 770-2 111216A 12/28/11 14:13 - 91 70 130 3.7 21.5 Run: BERTHOLD 770-2 111216A 12/28/11 14:13 - 96 70 130 Run: BERTHOLD 770-2 111216A 12/28/11 15:45 - U ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 6of9 EN:RGY LABORATO RI ES www.energylab.com J'; Analytical Excel/snell Sincg 1952 Helena, MT B77 -472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Late Fall Vegetation Analyte Count Result Units Method: E909.0 Sample 10: MB-15391 Lead 210 Lead 210 precision (±) Lead 210 MDC Lead 210 precision (±) altu Sample 10: LCS-15391 Lead 210 Sample 10: C11110979-003AMS Lead 210 Sample 10: C11110979~003AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 4 Method Blank 1 E-06 2E-06 3E-06 2 uCi/kg uCilkg uCilkg pCi/kg Laboratory Control Sample 0.00062 uCilkg Sample Matrix Spike 0.00039 uCilkg Sample Matrix Spike Duplicate 0.00038 uCi/kg MDC -Minimum detectable concentration Report Date: 02/09/12 Work Order: C11110979 RL %REC Low Limit High Limit Run: SUB-T43503 Run: SUB-T43503 111 70 130 Run: SUB-T43503 114 70 130 Run: SUB-T43503 114 70 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual 0.7 Batch: T _15391 R 01/28/12 12:48 U 01/29/12 00:53 01/31/1201 :13 01/31/1213:18 11.4 U -Not detected at minimum detectable concentration Page 7of9 'ENZRGY LABORATORIES ml'" www.ene.rgylab.com ~Helena.MT877-472-0711 .Billings.MT 800-735-4489 · Casper, WY 888-235-0515 • "Ii] AnalyticaIExcsllsnceSincs1952 j~, _, ~iIIette, WY 866-686-7175 . Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp Login completed by: Edith McPike Reviewed by: BL2000\cwagner Reviewed Date: 12/1/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody s'igned when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes D Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' N/A''C Yes D Yes D 111111111111111111111111111111111111111111111111111111I C11110979 Date Received: 11/29/2011 Received by: kg No D No D No D No D No D No D No D No D No D No D No D No D Carrier NDA name: Not Present D Not Present D Not Present 0' No VOA vials submitted 0' Not Applicable 0' Page 8 of9 tugr{ey Chain of Custody and Analytical Request Record PLEASE PRINT (Provide a~much information as possible.) Page_J _of~ ,.t~t.j;&tI.#tl4' Company Name: De4\~~on M~ne~ Project Name, PWS, Permit, Etc., I Sample Origin Lo..-fe ':0..1\ V~~~+cJ,o" State: (AT EPA/State Compliance: Yes ~ No 0 Contact Name: Phone/Fax: Email: Sampler: (Please Print) Report Mail Address: 1'0 130)( gOG{ 131M~ ;,,_~ ~-r ~L.\o II R ~ PlA.lt~er \..i3S bIg ;l;2;J.. \ ~l1,,~r HblltJ#-~ Invoice Address: Invoice Contact & Phone: ~M(. Special Report/Formats: Dow D POTWIWWTP o State: ----o Other: ---- D EDD/EOT(Electronic Data) Format: ___ _ D LEVEL IV D NELAC . r' II t' '"' ec Ion I UATRIX I lime I ... ,..,.. uate 1 No4 ~~+ I tl/~/lI Ioq 11l~/JI I DO I \ .. V I l Y II 11Q)0 11-v' )0 II-V 2 NOM-h vVes£t l,tI.lY II Il()~ I • 3 S{)~ \/Jes:r I H/~'lIl' IIIC 4 5 6 7 8 9 10 Custody Record MUST be Signed Sample Disposal: Lab Disposal: .$&(tnc , Received by (print): Received by (print): I Received by Laboratory: Purchase Order: Quote/Bottle Order: t=' o ~ w ....... I "0 o § <t e I-ro I-E <{ .= w 'E W ro en -g ro Ci5 .. R u 5 H Datelfime: DatefTime: DatelTlme: 1J-J~'~ II Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page Comments: Shipped by: ({P> )I.JJ JI Cooler lo(s): L //(111 (~) Receipt Temp !VIA °C On Ice: Y @) Custody Seal ~"ff\' On Bottle On Cooler Y N Intact Y N Signature Match ~ I~ ~ I~ I~ ~ ~ I~.~ I~ CO) I~) Y N 1~/IIQJffl Signafure: 1' .. ~.5 Signature: V Sigr:pture: fir.') G,: 55e In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information. downloadable fee schedule. forms, and links. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: FOURTH QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORATION NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER HAGHOUSE GRIZZLY BAGHOUSE / BLANDING, UTAH November 21-22, 2011 by: TETCO 391 E~lst 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines Corporation 6425 S Hwy 91 Blanding, Utah 84511 Date of Report: January 31, 2012 CERTIFICATION OF REPORT INTEGRITY Technical En1issions Testing Company (TETCO) certifies that this report represents the truth as 'Nell as can be derived by the methods employed. Every ef.fort was made to obtain accurate and representative data and to con1ply vvith procedures set forth in the Federal Register. Dean Kitchen Date: _____ -L-h_·....".-Z'----j/'--'k=--___ _ 7 Paul R Kitchen () Reviewer: ~ZKa r \...-- Date: 2 ;;, 20 (2 __ ii TABLE OF CONTENTS Introduction Test Purpose ......................................................................................................................... 1 Test Location and Type of Process ...................................................................................... 1 Test Dates ............................................................................................................................. 1 Pollutants Tested and Methods Applied .............................................................................. 1 Test Participants ................................................................................................................... 2 Deviations FrOln EPA Methods .......................................................................................... .2 Quality Assurance ................................................................................................................ 2 SUlnmary of Results Elnission Results .................................................................................................................. 3 Process Data ......................................................................................................................... 3 Description of Collected Samples ........................................................................................ 3 Discussion of Errors or Inegularities .................................................................................. .4 Percent Isokinetics ............................................................................................................... 4 Source Operation Process Control Devices Operation ..................................................................................... 5 Process Representativeness .................................................................................................. 5 Sampling and Analysis Procedures Sal11pling Port Locatioll ....................................................................................................... 6 Samplillg Point Location ...................................................................................................... 6 Sampling Train Description ................................................................................................. 7 Sanlpling and Analytical Procedures ................................................................................... 7 Quality ASSllfal1Ce ................................................................................................................ 7 Appendices A: C0111plete Results and Sal11ple Calculations B: Raw Field Data C: Laboratory Data al1d Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Conespondence iii LIST OF TABLES Table I Measured Radionuclide Emissions ...................................................................................... 3 II Percellt Isokinetics ............................................................................................................... 4 III San1pling Point Location ...................................................................................................... 6 IV COlnplete Results, N011h Yellow Cake Scrubber .............................................. Appendix A V COlnplete Results, Yellow Cake Dryer Baghouse ............................................. Appenclix A VI Complete Results, Grizzly Baghouse ................................................................. Appendix A LIST OF FIGURES Figure 1 Facility Schenlatic Representation North Yellow Cake Scrubber ..................... Appendix 0 2 Facility Schenlatic Representation Yellow Cake Dryer Baghouse .................... Appendix D 3 Facility Schelnatic Representation Grizzly Baghouse ....................................... Appendix D 4 Schenlatic of Method 5/114 Sampling Train ..................................................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide en1issions frOln the North Yellow Cake Scrubber, Yellow Cake Dryer Baghouse~ and Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat and Th-230 on the Grizzly Baghouse and U-Nat, Th-230~ Ra-226, and Pb-210 on the North Yellow Cake Scrubber and Yellow Cake Dryer Baghouse. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 111iles south of Blanding, Utah. Uranil1l11 ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Yellow Cake Dryer Baghouse. The Packaging enclosure also discharges into the Yellow Cake Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the tinle of the test. The South YeHow Cake Dryer is currently not operational. The Grizzly Baghouse serves as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 though 3 in Appendix D. Test Dates One run was completed on the Grizzly Baghouse November 22, 2011 . One test nm was cOlnpleted on the NYC Dryer Scrubber November 21, 2011 and one run on the 22nd• One fun was completed on the Yello\v Cake Dryer Baghouse Novenlber 21 ,2011. Pollutants Tested and Methods Applied The tests were a determination of radionuc1ide elnissions in accordance with EPA Method 51114. Test run filters and front wash residues were sent to Test Alnerica located in Richland~ Washington for radionuclide analysis. Test Participants Test Facility Ryan Palmer David Turk State Agency None TETCO Pau] Kitchen Mike McNamara Deviations From EPA Methods None QuaJity Assurance Scott Christensen Joseph Kitchen Kawai McNatnara Testing procedures and san1ple recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbookfbr Air Pollution Meas'uremenl Systems. 2 SUMMARY OF RESULTS Elnission Results Table r presents the findings of the test in Curies per dry standard cubic foot. Tables IV -VI1 in Appendix A have 1110re detailed test information. Table I. Measured Radionuclide Emissions Run # 2 AVE N orth Yellow Cake Scrubber pCi/dscf pCi/hr 311.5 2.325E+07 234.8 1.705E+07 273.1 2.0t5E+07 Process Data Yellow Cake Dryer Baghouse Grizzly Baghouse pCi/dscf pCi/hr pCildscf pCi/hr 30.6 4.216E+06 0.192 1.381 E+04 The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p) were recorded and are found 011 the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test filters for the North Yellow Cake Scrubber were heavily covered with a off white colored particulate. The front washes were clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. The test filters for the Grizzly Baghouse were had no visible particulate. The front wash was clear in appearance. 3 Discussion of Errors or lrregularities None Percent Isokinetic Sampling Each of the tests was isokinetic within the ± 10% of 100% criterion specified in the Federal Register. lsokinetic values for each test run are presented in Table II. Table II. Percent Isol{inetic Sam lin North YeHow Yellow Cake Grizzly Run # Cake Scrubber Dryer Baghouse Baghouse 100 98 101 2 99 4 SOlJRCE OPERATION Process Contro] Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse ~p readings vv'ere recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated nonnally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside dimneter of the Notih Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter san1ple port are located 6.3 diameters (9.5 feet) downstreanl frOll1 the last disturbance and 6.3 diameters (9.5 feet) upstreanl from the next disturbance. Figure 1 in Appendix 0 is a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The t\VO, four-inch dian1eter sample ports are located 28.38 dianleters (454 inches) downstream fron1 the last disturbance and 3.56 dian1eters (57 inches) upstream from the next disturbance. The sanlple port locations are depicted in Figure 2 in Appendix D. The inside diatl1eter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch dianleter san1ple ports located 2.56 diatneters ( 48 inches) do\vnstream from the last disturbance and 1.31 diameters (24.5 inches) upstream frOlTI the next disturbance. The sanlple port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each smnpling point fron1 the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by n1easuring the distance from the inside wall. Table III. Sam Point Location Sanlple Point 1 2 3 4 5 6 7 8 9 10 11 1.2 NYC Scrubber 0.58 1.89 3.49 5.81 12.] 9 14.51 ce (inches) from Insi D 6 0.70 2.34 4.74 11.26 13.66 15.30 0.502 1.26 2.21 3.32 4.69 6.68 12.08 14.06 15.43 16.54 17.48 18.25 use Sampling Train Description To deternline the actual emission rates for this stack; 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sanlpling trains were made of inert Inaterials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-5/114 are constructed to nleet the specifications outlined in the CFR. The tenlperature sensors are K -type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sanlpling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sa111p1ing and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equiplnent set-up, sanlpling procedures, salnple recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook/or Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and San1ple Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Con1plete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Table VI Con1plete Results, Grizzly Baghouse Nomenclature Sample Equations A NYC Scrubber TABLE IV COMPLETE RESULTS DENISON MINES CORPORATION\ BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol Description Dimensions Run #1 Run #2 Date 11/2 1/20 11 11/22/20 I I Filter # 5836 5843 Begin Time Test Began 9:13 7:11 End Time Test Ended 17:38 15:21 Pbm Meter Barometric Pressure In, I-Ig, Abs 24.40 24.60 flH Orifice Pressure Drop In.I-lzO 1.061 0.982 Y Meter Calibration Y Factor dimensionless 1.001 1.001 Vm Volume Gas Samplcd--Meter Conditions cf 333.787 319.268 Tm Avg Meter Temperature of 83.3 82.1 "flP Sq Root Velocity Head Root In. Hi) 0.2728 0.2623 Wtwc Weight Water Collected Grams 820.9 75 1.0 T\ Duration of Test Minutes 480 480 Cp Pilot Tube Coefficient Dinlensionless 0.84 0.84 On Nozzle Diameter Inches 0.3800 0.3800 CO2 Volume % Carbon Dioxide Percent 3.20 3.00 O2 Volume % Oxygen Percent 17.40 16.60 N2 &CO Volume % Nitrogen and Carbon Monoxide Percent 79.40 80.40 Vmstd Volume Gas Sampled (Standard) dscf 265.652 256.680 Vw Volum(~ Water Vapor scf 38.705 35.410 B w s (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.127 0.121 Bws (saturated) Fraction f-lP in Stac.k Gas (Saturated) Fraction 0.138 0.l32 Bws Fraction H20 in Stack Gas * Fraction 0.l27 0.121 Xd Fraction of Dry Gas Fraction 0.873 0.879 Md Molecular WI. Dry Gas Ib/lbmol 29.21 29.14 Ms Molecular Wt. Stack (Jas Ib/lbmol 27.78 27.79 %1 Percent lsokinetic Percent 99.8 99.1 AVe Ts A vg Stack Temperature "F 119.0 117.8 118.4 As Stack Cross Sectional Area Sq, FI. 1.767 1.767 PG Slack Static Pressure In. H2O -0.] 10 -0. J]O Pbp Sample Port Barometric Pressure Ill, Hg, Abs 24.33 24.53 Ps Stack Pressnre In, Hg. Abs 24.322 24.522 Os Stac.k Gas Volumetric Flow Rate (Std) dscHn J .24E+03 1.2I E+03 1.23E+03 Oa Stack Gas Volumetric Flow Rate (Actual) dill 1.92E+03 1.84E+03 1.88£+03 Vs Velocity of Stack Gas fpm 1.09E+03 1.04£+03 1.06E+03 Curies Radiolluclides per sample pCi 82741.6 60270.8 Crad Concentration of Radiol1l1clides pCiidsef 31 ) .466 234.809 273.138 ERrad Emission R.ate of Radiolluclides pO/hI' 2.325E+07 1.705E+07 2.015E+07 * Jfthe measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value wi ll be used in all calculations (40 erR 60, Method 4, Section 12.1.7), Symbol Date Filter # Begin End Pblll ~H Y Ym Tll1 ~",p Wtwc Tt Cp On CO2 O2 N2 &CO Vmstd Vw Bws Xd Md Ms %1 Ts As PG Pbp Ps Qs Qa Vs Curies Crad ERrad TABLE V COMPLETE RESULTS, PM DENISON MINES CORPORATION YELLOW CAKE DRYER BAGHOUS£ DescriEtion Dimensions Date Time Test Began Time Test Ende·d Meter Barometric Pressure In. Hg. Abs Orifice Pressllre Drop In. Hi) Meter Calibration Y Factor dimensionless Volume Gas Sampled--Meter Conditions cf Avg Meter Temperature of Sq Rool Velocity Head Root In. H2O Weight Water Collect.ed Grams Duration t)[Test Minutc5 Pilot Tube Coefficient Dimensionless Nozzle Diameter Inches Vohune % Carbon Dioxide Percent Volume % Oxygen Percent Volume % Nitrogen and Carbon Monoxide Percent Volume Gas Sampled (Standard) dscf Volume Water Vapor scf Fraction H20 in Stack Gas Fraction fraction of Dry Gas Fraction Molecular WI. Dry Gas Ib/lbmol Molecular Wt. Stack Gas Ib/lblllol Percent Isokinetic Percent Avg Stack Temperature <IF Stack Cross Sectional Area Sq. Ft. Stack Slatic Pressure 111. H20 Sample 1"011 Barometric Pressure /11. Hg. Abs St<lck Pressure In. J-lg. Abs Stack Gas Volumetric Flow Rate (Std) dscfm Stack Gas Volumetric Flow Rate (Actual) din Velocity ofS{ack Gas ipm RadionncJides per sample pei Concentration ofRadiolluclides pei/dsef Emission Rate ofRadiolluclides pCilhr Dryer Baghollse Run #1 11/21/2011 5838 10:30 12:32 24.40 1.516 1.003 97.600 69.7 0.5546 18.2 120 0.84 0.2755 0.00 20.90 79.10 79.940 0.858 0.011 0.989 28.84 28.72 97.9 85.6 1.396 ~0.18 24.33 24.317 2.29£+03 2.95£+03 2.1 IE+03 2448.0 30.6230 4.216E+06 Symbol Date Filter # Begin End Pbm i1H Y Vm Till .j~P Wtwc Tt Cp On CO2 O2 N2 &CO Vmstd Vw Bws Xd Md Ms %1 Ts As Pc; Pbp Ps Os Oa Vs Curies Crad ERrad TABLE VI COMPLETE RESULTS, PM DENISON MINES CORPORATION GRIZZLY BAG HOUSE Description Dimensions Date Time Tcst Began Time Test Ended Meter Barometric Pressure In. Hg. Abs Orifice Pressure Drop In. H2O Meter Calibration Y Factor dimensionless Volume Gas Sampled--Meter Conditions cf Avg Meter Temperature of Sq Root Velocity Head Root In. H/) Weight Water Collected Grams Duration ofTesl Minutes Pitot Tube Coefticient Dimensionless Nozzle Diameter Inches Volume % Carbon Dioxide Percent Volume % Oxygen Percent Valn.me % Nitrogen and Carbon Monoxide Percent Volume Gas Sampled (Standard) dscf Volume Waler Vapor scf Fraction H20 in Stack Gas Fraction Fraction of Dry Gas Fraction Molecular Wt. Dry Gas lb/lbrnol Molecular WI. Stack Gas Ib/lbmol Percent Isokillcl'ic Percent Avg Stack Temperatnre OF Stack Cross Sectional Area Sq. Ft. Stack Static Pressure In. H20 Sample Port Baromeiric Pressure In. /-lg. Abs Stack Pressure In. Hg. Abs Stack Gas Voilimetric Flow Rate (Std) dscl1n Stack Gas Volumetric Flow Rate (Actual) cfm Velocity of Stack Gas fplll RadiOl1l1clides per sample pCi Concentration of Radionuc1ides pCi/dscr Emission Rate of Radionllclides pCi/hl' Grizzly Run #1 1\/22/201\ 5841 8:11 20:01 24.55 0.783 1.003 292.611 76.6 0.2038 28.7 480 0.84 0.3798 0.00 20.90 79.10 237.519 1.353 0.006 0.994 28.84 28.77 100.8 59.6 1.917 -0.03 24.52 24.518 1.20E+03 1.44E+03 7.54E+02 45.7 0.1924 1.38\ E+04 %1 = percent isokinetic, percent As = stack cross-sectional area" (fe) AS~P = see "I/i1P M5 Nomenclature Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas CB = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cr = concentration of particulate matter, front half (gr/dscf, I b/d scf, etc.) Cmetal = concentration of metals (ppm, )lg/ft3, etc.) atomic symbol replaces I1metal" CO2 = percent carbon dioxide in the stack gas Cp == pitot tube coefficient (0.84) Cx (avg) = species symbol replaces x . Cx (corr) == actual gas concentration corrected to required percent O2 i1H = orifice pressure drop (inches H20) i1H@ == orifice pressure (inches H20) ~P = stack flow pressure differential (inches H20) Ds = diameter of the stack (feet) On = nozzle diameter (inches) EA == percent excess air ERB == emission rate of back half particulate (Ib/hr) ERF == emission rate of front half particulate (Ib/hr) ERmmBtll == emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = mUltiplier of test point i1P to determine test point ~H L = length of rectangular stack (inches) mBtll == thousand Btu Md = molecular weight of stack gas, dry basis (lb/lb-mol) Mp == mass ofparticulate on filter (mg) MFP == mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp == mass of particulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmol) N2 == percent nitrogen in the stack gas O2 = percent oxygen in the stack gas "I/~P = average of the square roots of ilP (may also be referred to as AS~P) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) P G = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) e = time of test (minutes) Qa = stack gas volumetric flow rate (actrn) Qs = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetrie flow (ft3/rnin, wscfm) Ts == stack temperature (F) Tstd = absolute temperature at standard conditions (528°R) Tt = see 8 Um = mean molecular speed (cm/s) Vm = sample volume (fe) at meter conditions Vmstd = volume standard (dscf)) sample volume adjusted to 68°F and 29.92 inches Hg. MS Nomenclature Vs = velocity of stack gas (fpm) V we = volume water vapor (set) at 68()F and 29.92 inches Hg. W == Width of rectangular stack (inches) Wtwc = weight of the condensed water collected (grams) Xd == fraction of dry gas Y == meter calibration V-factor (dimensionless) Method 5 %1 = Vmstd· (Ts + 460)· 10391 (8 eVs • Ps e Xd e 0/) As = (OS2 I 4) • 1t Bws:::: Vw I (Vmstd +Vw) CB = MB e 0.01543/Vmstel Cr = Mfp • 0.01543 1 Vmstd Cx (corr) = Cx (avg) • (20.9 -desired 0/002) I (20.9 -actual 0/002) Deq = 2 • L • W I (L + W) Dn des :::: ~ {0.0269 • (Pbm + 0.0735) I [(T m + 460) e Cp • Xd • ~[(Ts + 460) • Ms) 1 (1\ • t1P)]} EA :::: (%02 -0.5 (YOCO) / [0.264 %N2 -(%02 -0.5 %CO)] ERB = Cn • Qs • 0.00857 ERF :::: Cf • Qs • 0.00857 ERmmBtu::: ERx 1 (mmBtu 1 hr) K-fact:::: 846.72 e Dn4. ,1H(a}· Cp 2 e X/· Md· ps • (Tm + 460) 1 [Ms· (Ts + 460) e (Pbm + ~H 113.6)J Mel = CO2 • 0.44 + O2 • 0.32 + N2 ·0.28 Ms = (Md • Xd) + (18 • Bws) Ps= Pbp +(Pc;/13.6) Qa = Vs· As Qs:::: Qa· Xd • Ps • Tstd 1 [(Ts + 460) • Pstd] Qw = Qs I Xd Vmstd = Vm e Y • Tstd • (Pbm + t1H 113.6) 1 [Pstd • (Tm + 460)] Vs =: 85.49· 60· Cp· -it1P· ~ [(Ts + 460) I (Ps • Ms)] Vwc =Wtwc • 0.04715 Xd = 1 -Bws APPENDIX B N orth Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Field Data Sheet Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Data Grizzly Baghouse Preliluinary Velocity Traverse and Smnpling Point Location Data Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Denison Mines Stack Identification North Yellow Cake Scrubber Date ;11"11 ;1 /, 2-011 I Barometric Pressure Pbm ;1. '1.. ' tLtJ inHg Pbp 0,,'2 .. 33 in Hg N BO Static Pressure (P G) ~-'I/ in H20 Estimated Moisture (Bws) a % Sample Height from Ground '70 feet A Comments: Stack Diu 18 Reference. 0 Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last dIsturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F 1 3.2 0.58 0.58 2 10.5 1.89 1.89 lI"'/.~ rl .6Lf 3 19.4 3.49 3.49 1I'l". 4 32.3 5.81 5.81 ,O{,.s 5 67.7 12.19 12.19 11f> 6 80.6 14.51 14.51 10& 7 89.5 16.11 16.11 8 96.8 17.42 17.42 110 )18 10 Averages: Ts L. Flow ---- ~P -v~p ------- KEY=> TETCO li:i Field Data Sheet Filter Sl}JL Sample Box~ Plant: Denison Mines Location: North Yellowcake Dryer Scrubber Date: No";:2. f 'lOl f Operator: Pa. v f K-K, f.ch e A Traverse Time DGM 6P 6H (inH,O) Vacuum Temperatures (1') Point Clock Min (9) IIlJ) (IIlH1O} Desired Actual \II1Het) Stack (T,) Probe Probe Out Filter Effluent B 1 '1~ l3 0 1(p.02~ "O(p I ~l-,g~ Z.O ItS-,)1 v ;;":fo 55 1 15 '1S. I 'ltv • Ole .gz-·8'--,·0 liB .:2&5 21-1 SLf 2 30 S<f ._~ <t z,. ,b!.oZ-,FS ~K '-/,0 II(P ?-10 2(P'V ~0 2 45 &3 . &.(1-.0&2 .g~ .~6 r·O 1ft-2!p3 z..S(.~ 5<1' 3 60 1-3.D3 1 ,,00 .{<> .83 5 ,0 /2-Z-)...ee.S" )...~~ ~3 3 75 ~2. > "702-.00 ·83 ·8?:> s~o /2,7-J,cpB z..S7-SS' 4 90 ql. 513 orZ-I. Or.:? '·()O {".[J ill I,;2.qR k;24 Cj $'"3 4 105 161. ns-,oi2-l.o2.-/.02.-IT'o 113 ).~} ~4.D 53 5 120 {(2-Of" .07 i'~f-/.2 f-C). V {f"1 ~o ,).'18 5"s 5 135 l (;'~. 4 ~ z.. ,10 1/·<-/7.-i-t..f Z-l ti,o II (P 2(c1B ';)(Ph 5"b 6 150 { !J5". I.{ J(P .O~b Lz.-z, 1,2-Z-flO IIJ£:t ;;.={,;;.. k?2latJ )8 6 165 f~f#. 85'<P ,°9 1,2-7-f, 2-1-{2...C> IlL ?-5 V )..&7:;; &3 7 180 !S8.3('-/ .01 /. '2..7-J .z:j. I ~ /3.0 Uq ;;...~r 12 ::r; {.$2.,.; 7 195 /(;9 ,r38 .c(i I~ZT f"lr-I'I.{) (t9 )..L{l{ ~(.,T (~o 8 210 fft ~O4 ·085" /-~o (~ 20 /5·0 I{e, ;JJ1.0 2 7 z" ~2- 8 225 lca.~ 1-5cr ,("8~ J,/~ {. (8 1f.f.O It'1 :2.'-f:) ZqS ~I Y ;,',/3 240 203. Z-t 1- Total ..J ___ _ Average ,j DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check to.,/~tr llt ,O 0,00 \ ~.ot-\. \\~ ~ Gkt\N\.'dw\' Q1 t~~ aJf f~ ~ e.- DGM Temp ,(Tm) Out In &r &1 (qZ-(,S" &5' 1'2....- ~::r ;.-::;- /09 ?-'7 ?l gf 72-152.-r'!> (~_U 7-s [gS 1-~ 8'9 rh '11 +-2 10 1-'1 0 r eo <r3 >!f 9C; g3 fh -- Vac ("Hg) ;2 \,0 Page --.f_ of_~ Run #-L. r BQ N A Stack Diameter 18" __ Port Reference _0.0" Ports are Ports are ~ Upstream from next disturbance 9.5' Downstream from last disturbance Assumed Moisture Probe 2..'TCr 4-13 % Cp ~ Nozzle Calibration l,pD .:sgo -'!>8c) ~ >~ AvgDn <)~ inches Gas Bag lie. -.3 Console ---=S,--_ Y·Factor /.r)O( 6H@ I J-Ieft; in H20 Barometric Pressures Pbm ?--t...{-(t_'V __ in fig Pbp 2.. 4-~~ in Hg Pc; -.I( in H20 Leak Check Pre Post ft'/mm f)..eO z... ~z...-. vue In Hg lP:O n_;Q P,tot Rate C-co V 00 In H:O ,.f7' ,?-5 2,)'" . ~ Water Collected Time Sampled Review K '" @Tm K = @Tm Rate (fe/min) o ,OOL, g min ~~ Field Data Sheet Plant: Denison Mines Date: p~ V 2.,.( ~ 1,0 f! Traverse Time Pomt Clock Mio(9) 1 12 !~1 240 1 255 2 270 2 285 3 300 3 315 4 330 4 345 5 360 5 375 6 * 390 6 405 7 420 7 435 8 450 DGM (111 2-o4·I13 Z-tZ-.t.f2rt:; 7-20 . 'l3<Z 'Z..tq~5w' .l3~.~t?1 J. ,-q... '2-1-'i 2..5(0.0'<3 Jl(P&.811 )..:'t8.0 'f:t.; 2~ ~L&'8(P ~e)~. ~}t:t 3t<.{. l<-l o 3 2-5"'. '-(( 0 "33t, f"1-'1 ') t{g. u5i' 8 465 1'\G10~ o'rf3 Ul! 38 480 'A;rl. q~Z--- L.\p L.\H (mH2O) (.nH,O) Desired Actual ,O!{S' .&:-,&3 I{)Lf~ ,(#3 .&$ .05 ,1-1 .7-/ -O~ .it -:;'1 ,OS .1f -rl IO~ .1-1 ."f f ~o~ /., 3 J./3 f08s I! 2.-\ I. ?.,\ ~O'l5 1(3~ i ·3'{ ,oct5' \ .34 1,34 ~. oq 1,,2-1-I,L1 101 I· ~t-1·1,7 .o7~ 1,3Lf j .3e.t .0'13 ;.30 1<30 (01 }.1-f4 / .. 2..& .09 ,.:z{g {,1.(P Vacuum (inHg) ;>,(') 3 .0 '-t.o £./.0 5.0 5.0 ~.o '7~O 10.0 /3·0 "io l{.() ~.o lo ~·o fO·D TETCO Filter ___ Sample Box~ ~fSgl..f'l-- Location: North Yellowcake Dryer Scrubber Operator: Pa.o/ 1:-K. k~ e(\. Temperatures ("I') Stack (Is) Probe Probe Out Filter Effluent 118 ;;z.SC{ 2-33 ~'f tZ.;l,/ Z--SC? 2S~ lftO 12--z, )-&. r '~f ~2- ( z..1 J-~ ( t?-(;{(,:) 4(3 1)../ Z-.>-CZ Z5<j 52- I ;).lj .A.'-i) ~o ~L-I I .;&..{ ,-3e 62-Car 5'0 J;t.'O 2,53 ~&t+ 50 ncr ~'-/Z, d-(.e'-f S-1 I ~C> l).ut,! :2-t2... 5'-/ 12.3 ;)7-0 ;2l(S s-? f '&v 2-5g ~s,Q, 52- I{~ ;<'-!<-( .:Au 2... 54 IlCf .25D ;).&(p 51-/[1 ;;..9{) 40 S'Z- n9 "'2.-5'5 d....~1 5"2- Total Average ;1.>'.~t/-J ~.1z..~ -I. ~?,Z~/ '1:>"7/15 1.o(P{/ .~ t t(tO/ Additional (Extra) Leak Check Information DGM before Leak Check Vac (UHg) Rate (fe/min) DGM After Leak Check 30L ~~q "'LA> ,0 o·I!JO~ ~t)2. tt l \ . ,. -¥ G~ Ii ~ L<;''. :::.P> ~ DGM Temp (T.,) Out In 83> 8kL 8'1 <to ~s q-z-, f?5' 92- 8:r 9tf 8::t-1'-{ g>g 1(0 f?7 78 ~1 ICO 8-? 100 8'2:-<8+ ~{ I I 80 c;.l_ 80 13 11 7'2:- tf:i '!'2- 5,2-4 83.3/ Vac ("Hg) J..~,o Page ~_ot~ Run #_1_ t sO N A Stack Diameter 18" __ Port Reference _0.0"_ Ports are Ports are ~ Upstream from next disturbance 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe z-=tCr Cp 0 .84 Nozzle Calibration :",>go -')&'O ~ ~ Avg Dn -~ 81) inches Gas Bag l+-C -3 Console_5' __ _ Y-Factor I, r::> C; ( ~H@ ~ inH20 Barometric Pressures Pbm .f..q.4 0 in Hg Pbl> .A. 4{ • -; 3 in Hg Pa ,....1 I in HzO Leak Check Pre post ft3/mln ____ _ vac In Hg ____ _ Pltot Rate ____ _ 10H,O ____ _ Water Collected 800 ~9 g IimeSamp\ed U 30 min Review K= K= PL~ @Im @Im Rate (fe/min) i I 0,001.0 i , I 1ft..( Field Data Sheet Plant: Denison Mines Date: NQv '2-"t-t lOt! Traverse Time Point Clock Min (6) , 1 :r:r i 0 ) 8 1 15 2 30 2 45 3 60 3 75 4 90 4 105 5 120 5 135 6 150 6 165 7 180 7 195 8 210 8 225 Jf WlI 240 DGM (f1'1 '3 '13. 1.1--"Z-. ~~C 5:;:r 387 /18'1 3'7$i .38~ '-'10f4, .>tB l{ILf. &0 t,... l.-{?.?..., glO '-13 £.1-1 r 4l.(o.r 'r(tl HYr-' ~tt1 4~.5-. L( tZ-- 1..£&3> t:>73 Llr-L.OYz-- u$l{) . uti I , • c LI fe . 9 t11 C-fCfl ,~Y3 501-t &~ LlP LlH (on H,O) 'HlH~OI Desired Actual .-o$' ,&6 ·~8 .05 ,~e · tP 6 <OS"" .. ('8 ~&B ~04:r rG,L-( ./#4 ,(}{t;' ,(, ( • Cp( -048 .(p:;-,(;S ,0)' .~g · t; f3 ,ass ,,1-~ ·15' d)~O t ~'-o) , 5l-5;~ tOz.-{ 5-"-...... 155' ,tiLl&; .&3 ·(c,5 .05 -&8 .&B . (9:; .&6 ·&8 ,c!)<) ,&8 -(p CO ,e£<;" . rftJ . rlp ,00 .lf3 .g3 Total v ___ _ Average V - ---------------------. -- ------ DGM before Leak Check Vac (tlHg) 6 v 1-. tli1 H.o TETCO Filter 5'Btr~ Sample Box_~ __ Location: NOlth Yellowcake Dryer Scrubber .0 ,'D V f t Operator: r o~v l r-1,,\ ~ r-c.",1... e:'Y). VaCllum Temperatures ('h (1I1r-i.gi Stack (TJ Probe Probe Out Filter Effluent ~.o 0 9 )"7,;=r l~{5' .t.I"L 3·0 /]..0 2.52-:?-53 '-/,/ 3.0 !I ? ;;'3'( J...&~ L/'"/ .3.0 ! z.o ).(40 ;2,.(gS' 4~ ;,. () 1.:1-f :z..s-s> ~q 4'-/ ['-I. [) /2--/ -'-'-/'-1 ?G. Z. tr1- 5.0 I~f ~~e ,).(p2. 48 /§-o ( z,2--<J.ff(P ;;ty;(c S"'I (..0 /2..3 ;yt.{) 7-(Jt.9 S-c;- &.0 /W .).41 '2(,8 S3 1,0 118 ;t.qz.-~8 So f/J) I z. I ~\.(y )..(pf> s-r ~.o f ~O ;ti--{3 ~tp.y !i2- 1.0 tZ--O ;utS-'--70 ~~ If) ·0 !t' A~4 ~B fFS- /1.0 /1-{ HP, /-1'0 Sf£; Rate (ft3/min) DGM After Leak Check 0·00\ 50T· ~Lt<6 * L. t.-.«. ~ ~ hrt-1'yS o~rn~ 120M" c0.e~-e y J 'i Page _I_Of L Run I! ~ OGM Temp crill) r BO N Out In 51 C;. A ~O &3 Stack Diameter 18" __ Port Reference _0.0"_ fur 70 Ports are ~ Upstream from next disturbance fJS-7 ~ Ports are 9.5' Downstream from last disturbance &7 r ::;5: Assumed Moisture 4-13 % (;7 i-?-Probe 2-7-(r Cp 0.84 ;;f @) Nozzle Calibration 1-2..-~2. .3!O . 3f?D 3<fD -3Jio t ! qz.... A vg Dn ,~g () inches r-z-~L Gas Bag /I( .... ? rs 8'3 Console ,5- 1S' g'1 Y-Factor ;. eN) l 1-3 81' L'.H@ /. 4g~ in H20 ?5 ?S' Barometric Pressures IS-9ro Pbm .:z~,(P{) in Hg .-,g 81 Pbr ).'-1 '.("3 in Hg Pc; -"1 1 in H20 Leak Check Pre Post ft'/mlll 0.002-O-t9cJ '2 vnc In Hg 2 {.O lZ-_D PilOt Rate b .e>'"D Q-~2f.) In H~O .2..5 ,2-(" Water Collected g Time Sampled mm Review K= @Tr.1 K = @TIII Vac ("Hg) Rate (fe/min) U.O 0.00"1 JJ~_I _ Field Data Sheet TETCO Filter ___ Sample Box~:.. __ ___ ~~_I __ .. __ Plant: Denison Mines Location: North Yellowcake Dryer Scrubber Date: Nov 2..2:.--/ ~(\ Operator: \>(("'v\ l<-l<" f-cl,e..r"'\ Traverse Time DGM ~p L\H (In HzO) Vacuum Temperatures ('1') Pomt Clock Min (e) (fi3, itnH~O} Desired Actual tin Hg) Stack (TJ Probe Probe Out Filter Eft1uent IT 1 11'.1.,-' 240 SoJ.8Lf£ .01'8 f.o~ f~08 <-1<0 /:J..t( J...rf .).4i.j 5J 1 255 51 €. '-leer ,f}i r.1i I. If 4.Ai {).:~ ::J-~7-~Lic, 51 2 270 5'-'t-Z3t.o .09 f ·z--S' ( .Z-~ S.'O 1'2-1 L~ ?~Z, 5 1 2 285 540 .500 ,ois {. f~ I.;g ~-o (2.2-ZS'1 ~ss-51 3 IZr 300 55t..'5 Lj ! .087--L 1(..( I·f Lf :t,'O f A'!; ~Ct3 2-50 51.., 3 315 5' &-2. • !I 14 ,f}gl.-ldir I,ll.{ r·o I z.-z-).&2-250 S-I 4 330 513. f&& .. ()g~ I. f8 {·/8 &.0 I z. z--t51 ;;"<-(1 5 ' 4 345 5'"8'-f.oQ3 ,o~5: I·' ?? /. Ii? 7.0 /''2..5 25"fo :J..47-j-.3 5 13 360 ~'iS: 049 ,0'1 If 2-5 /. z t:;; /O.C {'?"(p :J.SO ;;.qf 5'L 5 375 UOb.t.iG to 1 /. z.-';-Lzs it.D r 2-2-, 1-38 )..L;S' S"2 6 390 (n::;-. $)~ tf .o~:;-1. ~l{ '·3~ 12.'0 1(8 :;Lu,/ d.-<..(f~ 53 6 405 (P 30.0'13 -01S-f. Sf{ 1.31..{ (2·0 01 ;;lCtt! -'-Lt9 sS- 7 f '-! ~ i 420 ~"[Z· UC[ _ 1(55 t v'f1 /J{7 [2.:0 1(/> 4n.5 ~S3 :;-&:> 7 ') 435 {,~q. &l'O 'Ib~ [-'19 /(<(9 12-0 /03 25S' 256 S-s- 8 450 Wt-, /2-1 JJfs /,&3 (.('3 12-.0 12---"26D vS "7~ ,~ 8 465 &86. 1t5 Jib l.(g 3 /.if3 lZ.O 31-2.-58 1-03 58. l5'.tl 480 ~Y3. ,(;1 Total 31~1';u.8v'i v 8:01'10 -~ 3L£i \ Average \i -1.(,2-3 ./ G ·~fl.J "1tl 111-.6/ .. -_. DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check 4.'" / l,' ") I ~ DGM Temp (Tm) Out rn Po gS- Sf '4" .• ~ 8 / 13 r't 1z., f:g ~l 1-'9 rz. 80 73 81 9s' 81 '1s 83 '18 ~fj /6() .85 I f) 0 f18 10'7 'tv 10,/ C;Z-I~ '1(( lo~ 5ZS(o 8'L·' / Vac ("Hg) -- Page~of "Z.. Rlm#~ r N B Q A Port Reference -0.0" Stack Diameter 18" __ Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture Probe Z=rCr 4-13 % Cp 0.84 Nozzle Calibration ·)g'O ·;8D . S ~O . sgo Avg Do' 380 inches Gas Bag H-( ,... 3 Console <) Y-Factor I.CO ( c.H@ {.,L{8 ~ in H20 Barometric Pressures Pbm 2J-I_lc~ in Hg Pb ~ l.[ ·53 in Hg p - p(~({ in H20 Leak Check Pre Post fit/mIll O·w t vac III Hg G ( .0 PItO[ Race InH,-O (9 .. 00 -7, S/ ~ (Z,D D·oO 1'" IZ~ Water Collected lS(~ 0 g Time Sampled 4 ~ mi n Rate (fe/min) . f9'K ReVIew f--; K= K= @Tm ('0TI11 Yellow Cake Dryer Baghouse Prelim 6 pts blank Facility Denison Mines Stack Identification North Yel low Cake Dryer Baghouse Date II/ '1.\ { if i Barometric Pressure B Pbm 2i§,4¥v in Hg Pbp 2. (.1. 33 in Hg -0 N Static Pressure (PG) -, Ie in H2O A Estimated Moisture (Bw.,) .,~ I,S% Sample Height from Ground fee t Comments: Stack Dla 16 Reference 0 Potts are 57" Upstream from next dIsturbance Ports are 468" Downstream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F 1 4.4 0.70 0.70 2 14.6 2.34 2.34 71 ,l.( 3 29.6 4.74 4.74 4 7004 11.26 11.26 gZ.')3 5 85.4 13.66 13.66 6 95.6 15.30 15.30 (fl... ,,1.1 Averages: Ts LFlow ----AP __ _ -.j~p ---- KEY=> ~_J~ Field Data Sheet Plant: Denison Mines Date: l \ { 1..-t I ii TETCO FilterS'S 3 ~_ Sample Box D Location: North Yellowcake Dryer Baghouse Operator: v'A~ -vii 5:; :t/ CV1A, t;A \" CA", Traverse Time DGM t.P L\H (,nH,O) VaCUUln Temperatures. l"F! Pmnt Clock Min (9) IflJ, (mH;O) Desired A 1 1~··30 0 f.,ilCf.p~ ,2., L1.3 2 leo ~!(."zgl 15 \ t.)t.. 3 to (. Z-<-(,") '-, ,,?>'3 LI..'Z.. 4 30 ~:;2.. 7(0 ~ 3'1..-\ .-)1 5 4fD '··.p.oz..{ ,yt.. 1,11 6 So \-i~. 11< ')(. t,'z... £> 1 n-, ':>'t-bO ~ (1, tz.O .'tg ~l 300 2 ('t) I;. (,(.Z70 .z..'1 I' ~ 'J 3 So (,.1-:>, lt D -1..' i ,~~ 4 '10 (, Bo. gSo -:0/ L ~L 5 to<) (.. 89.. qz..-) .')t.t \. ~! 6 il O '<f(2), '"1 {) ·7..9 t • '-t;;, 11'.31. .. i '2-0 7o~, 11<1 , Total if I/f ~-7.~OO "';"'{;J) J Average ,1 ..; \'i )l\.~ Comments Time Bag house L\P Time ~t) ~ 31" l.9 II'S ~ iD~H. 1,0 1\ '.5t:? h~t1r 2,) \ t ',1.(" ---- Actual (IH.Hg) 1.1.3 Z. Lf 2.-z.. I. (.t,. ~I it'5( Lf' 1,5'1" 4 l,(z.. 4 (~ 3~ ~ ll'i:!> ~ t,<-\3 ~ L 'B 1.-t.\ II~I S td:> 5 1€,lCfov \,)\56 Baghouse L\P '"Lo )\{ 1'1 -- Stack (T,) Probe ~.,-z... l70 83 210 8) 27( ~~ l.1e... Bj -L(,,~ e ·) LbO ~~ Zl{ Bio tc.,cr g-:r 2. <"f e'f-2.(.. 0 8'e 210 8H ZIt..- toz--::r-v ~{,(, Probe Out Filter Effiuent ~8-) lfJ( 5'1 1.70 2,70 SI ty{ V;'Z.. Sl Z"3t3 2~O 53 ~bO 2,(.-;) 54 2".'10 2.4)' (''l 2'15 :!:!;z.{O 55 z. 'i '{ 2.5<t $'-1 l So 2(,,3 51{ (.10 2.G:.) Sy 2. 50 ('Io~ 55 'L s·" 1-<"1 3:;- 9 f>~,J(~s DGM Temp (T "') Out In 5, 57 '='0 tD:J '(1,3 to <::, )-7~ (,1 I~ "8 (~ ~~ -71 1.06' I~ (.,4' \ 1-) tt'O l~ !t 7't 1"L 1'1 tCOi)v ('" 9,,10 Page --l--of __ I_ Run #_\_ i B AO N Stack Diameter J 6" Port Reference _0.0"_ Ports are Ports are ~ Upstream from next disturbance 468" Downstream from last disturbance Assumed Moisture % ---- Probe 1<9 -G Cp~ Nozzle Calibration >l.2/~ \,2.70' 1.:2..7 {., !?.71 ---//.--- Avg Dn ~. t. 1., 0 Inches Gas Bag Ambient Air Console __ <-1 ....... __ Y-factor l . 003 6.H@ ~q~H20 Barometric Pressures Pbm Z <.{ . 40 in Hg Pbp Z t4 _ '3> 3-in Hg Pc; -. iL-mH20 Leak Check Pre ft'/mm OoOI! 'lac m Hg t.1. P,tot Rate 0.0 In H,O 5"·0 Water Collected Time Sampled Review Post 0 ·003 ~ 0·0 4'0' !~(1- ~O ~#t K = K ~ @Tm (irT.n - g min Grizzly Baghouse Prelim] 2 pts blank Facility Denison Mines Stack Identification Grizzl~ Baghouse Date 1/-22. -I ( - r Barometric P.'essure Pbm :2:1. ,s-5"-in Hg Pbp ~(./ .!>-z in Hg N AO B Static Pressure (Po) -'03 in H2O Estimated Moisture (BwJ I % Sample Height from Ground 30 feet Comments: Stack Dla 18.75 Reference 3.0 Must use 36" probe or longer to keep box outside handrail Ports are 24.5" Upstream from next disturbance Ports are 48" Downstream fTom last dIsturbance Traverse Percent Distance From: POI'ts Point Diameter ID Reference A B C D E F I 2.1 0.50 3.50 2 6.7 1.26 4.26 }'t? u~ ,$'1 ,0'1 3 11.8 2.21 5.21 4 17.7 3.32 6.32 51-,04 IP'6 .., tOL.{~ 5 25.0 4.69 7.69 6 35.6 6.68 9.68 5"1 ('8 :3 .ott5 (>4 7 64.4 12.08 15.08 8 75.0 14.06 17.06 ~()i.(~ (.t~ IOl{'3 9 82.3 15.43 18.43 10 88.2 16.54 19.54 )5' 1"1 11-0 .{9 '()I..( I I 93.2 17.48 20.48 12 97.9 18.25 21.25 Averages: Ts L Flow ---- ~P ~f!.P -------- KEY=> pq __ Field Data Sheet i3 p. Plant Denison Mines Date: 1I ( l'l.l tj Traverse Time PolO! Clock Min (e) 1 ~'. t\ 0 2 20 3 40 4 n;.S'!'" G,O 5 ~o 6 too 7 t·t o 8 !'-iv 9 I C,Q 10 i '0D 11 ZoO 12 _1. 7,0 1 t~:.o! Z'iO 2 1,(,0 3 z.8u 4 300 5 3Z~ 6 JM\) 7 3(0.0 8 3So 9 Yoo 10 4t~ 11 yti° 12 't!,u 2.o:0 { L.f 9O Total Average Comments ll'. \"; ,rv ~ f'" j( '7 ~ \,\. 'Z~,,~ ""), L \'~' ~ .. ~...... ~,<:, .J (l..:> \t.J'-J-..?J ~\~..JV ~ t; f ~ \2~~7 Q)" '-{ TETCO Filter 5@ (_ Sample Box~ __ Location: Grizzly Baghouse Operator: M. f-1 ;'0\ !?.,IN\,J2.,,CV- DGM ~p ~H (lnH,O) Vacuum Temperatures (F} ,Il"j (JIIH,O) DeSIred Actual \,"Hg) Stack (T.) 707.'-1 )3 .(4) ,Sf d~h t.. 41 7u ,,01'{) i0c.{'Z-'80 l~t) z.. 5 3 l ~ L Cftf) ,o"1} I ~1. d~'t. 2-5<-[ .., '-t<-t, ~"1l e1"i) j eO IS( t 55 .., 5' '1.000 ,oY«{ d3 -z, , ~1--z.. (P 6 -zt-9, c.{{ { 'o"l~ leO ,So 2:. !DB tSf,17...0 .0'11-,is a1 6 Z-"t8 7.1 ~<..{, ( ,-,0 .04.7... i/~ t'10 l... lo'i e~,'1 7) ~rI;1 t1J ~ ( 6'f 1.-(g~ 8< '1 -o'"t () ,0'-\ l 1"1<0 17~ 1-fA) n .,A! .0<..[( 1(<0 t c & t, 6'( ~llJ "'v ~ e~~, \10 '0'-\\ 1"''' n (' z.., ~) fh;·/qo , .. ~C1 • fo <% lb~ 2,-~O gG(, I" q)--H')~' 'b~ ,'-8 t ("0 8'1 L. Stf( .he nt .I { t 5q 't~'t. '-l~f .61..1( ,,"1 11 '1 \ 5·~ '90 1. S~\{ .ct.f'$" ,e{ I <b~ 2..-$8 ttl) . ,,1.-) .0<"\-)" ,fO r ,'6S-z.. 5r '11..l .1 '6u 'oYZ-.~o , ~C> 1. s~ q 3<1. 5'lD ' o<.{'Z-t 'do ISo Z. [;5 ~5 i ."\"({ , o<-l.l 11 'a (,B 1-55 q(.,!.{. V~) .o~~ .1'2.. .,7.-2-53 ct15. 'Sl.{o • o-i () \'1r.. (i (, '1.-51...- (HS"l,Q3D .<1'10 (7~ ,1(.:, 1. 51.- 10 00 . o~t{ 1.'1 '2.. .~(l v:_ {\" t(lH~" I S t {~j iLl)o/ >j ,1..0')'0 Drt9~ B{j-Y St.,..jr 00\10.(\ ~'1LtO 00,1i\.t" lot . () t. up -~ \,1:, S\O f-,.Q.,;;>("'" J ...... , lSZ.-( S<q ·5 8 ?06"l \S \ (oJ'''' \' '\> f' It."..e \,,\q; '" ~ IQ~ \ .n\) Probe ProbeOllt Filter 2'10 2 73 Z'13 " "30 1.-)0 2.1{) z-r0 l<;l Z-<f"t (. 'ft{ Z~'1' "~I 22,.( l H. ZJC,.:, l.'f"f-2.. 1b '-'t ~ "l,10 2.<i'l V-19 l. <·tt Z50 2;0 l4i (.)(., 'Z j 'Z... 2~7 2(.(1 Z4'"i 'l.k) Z {\ l)1 1.."<1 l <t<1 LY"t L.~Cf 2..3:> 2.3.5 tILl) 2..2-1 lz.q t.<.ft) 'l.}l 2>7 2.')~ Z3 7" 2:'35' "-4, 2.)(" z.~ ~ 2--(0 138 2.)B 21 0 ·'2.-<'{3 "Z..l{3 "t10 l ~) ~r ) 17.:J u,:, 2 ~) !1 ~ 1..54. Z)'/.f -z.'1 ~ 'Z.:~Pi l39 t(z., t "$> z,~j' Effluent (.,-{ ljCf 50 Sl S O 51 5"2.- 5 'Z- 5 'l. 51.- 52- Sz:.. 57- I..jq 4q '19 '-l'l '19 Li 9 =>0 5l '-R '-1<3 li'e Pagel __ .of_t_ Run #_t_ DGM Temp (Tm) r ~08 N Out [n 5'5 5s 60 ce Stack Diameter 18.75" Port Reference ~ (Pi 10 1 3 (C B( 8e 8)' 1'8 7r 1:<-/ 7J r-3 "1 2.. T I., {Z- 1-.1 11 f9 Ie 78 l'{ "II{ rtf 7fp 7g !B) 8'1 8r;, 'to 9? ___ 7-tf ,S 7)' 11 7~ f\.> '/ 7'1 BJ 8-z., 8~ B~ (13 53 Ports are Ports are 3& ICo .01' !~. S{5 ~ Upstream from next dIsturbance 48" Downstream from last disturbance Assumed Moisture ____ 0,'0 Probe ~ Cp 0.84 Nozzle Calibration ~~ oio .3 80 Avg Dil • 379' ~ inches Gas Bag Ambient Air Console ......:;:U+1 __ _ Y-Factor i ,.a~3 .1H@ 11-f"1l in HzO Barometric Pressures , lo\ r.--" Pbm (,. .) j mHg Pbp _2 lhS~ in Hg Pc; -,a3 in HzO Leak Check Pre Post fr'/nlln 0, 002.-0 .003 "3c inHg~ l Q ,Qo P,lot Rale O,e c.O (nH:O '1? 11 ... 1 Water Collected 2(3 ~ i-(I '" Time Sampled L{ ~(j min Review ~- K= K= @TIT' @TI1l North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSA T) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Alllbient) Grizzly Baghouse Sample Recovery Gas Analysis Data (Alubient) Chain of Custody Lab Analysis APPENDIXC c North Yellow Cake Dryer Scrubber METHODS Facility: Denison Mine Stack Identification: NYC Scrubber ------------------------------------ IMPINGERS 5~~<e 5g~} 5 l5'1 Z, lMflNGERS IMPINGERS Final (g) Initial (g) Net (g) Final (g) Initial (g) Net (g) [MPINGERS Fina] (g) Initial (g) Net (g) Run: ---:..--Sample Box: C ,--- implnger NUDlber -#m I ~ 1 ~ 1 5 6 Initial Volume of liquid (H20) in impingers, (ml) drop out 1 100 1 100 1 SIlica Gel 1 ~~,o ~q2., t-ft €3. 3 Ct'11. q 5 '1'1.& It} ,~5.l-/ .5"0&"i 57{)."" ':2.,.1-~tft!).o 540.' m·B V It..&? :L1~1.-O 5<-[-1 i-·1 ,·1 " ~.(p Total (g) fjZrO.'j 1/ =========== Run: 1-Sample Box: ---- lmpinger Number 1 =-= =*= I 3 1 4 I ~ Initial Volume of liquid (H20) In impingers, (ml) drop out I 100 I 100 I Silica Gel Total (g) Run: ----Sample Box: ---- lmpinger Number .4.13 1.4-15 6 Initial Volume of liquid (H20) in impingers, (m!) drop out 1 100 I 100 I Silica Gel ------~-------+------_r------~-----~------- -------4-------+------~------~------4_-- =====±================================ Total (g) =========== Run: ----Sample Box: __ _ ImplDger Number 2-.1.1--14-1 5 6 Initial Volume of liquid (H20) in impingers, (ml) drop out I 100 I 100 1 SiliiEJ ------~-------+------~------1-------+-------- ------~------_+----~~------1-------+------- ============================================= Total (g) ========= Plant ])eA,-'IPf1-n.., Location Analytical M ethod ____ {9_I'S--=--a...._f _____ _ Aycl'age Net Net Actual Net Net Date II -"'l.{ .... /1 Gas Reading Volume Test No. t Gas Bag No. fr("',3 CO2 3(z... 3· z.,.. ~.?-~< z~ '3,,2-1" 'Z-:L. "2-Ambient Temp (tJ<) Operator IKe<. 2.0."ftl 20·(p 2.0,& If· I.( I?~ Avc,'nge ActUlll Net Actual Net Net Date [1-2,2--1f Gas Reading Reading Volume Test No. t, Gas Bag No. 1fC-Z, 3,,0 S .. O ~~O =$,0 S .. c.:> "$.0 3.c Ambient Temp t, . .s-' Operator eJX. (Net is Actual O2 Reading Minus Actual L9·(p )e.,. G? /9'.(0 14·(, /9. (p 'U~~ 14,-te, CO2 Reading). N2 (Net is 100 Minus Actual U2 Keadll1g). II----.----II----,------III--~--.__~-__li Average Date -----Test No. -----Gas Bag No. ____ _ Ambient Temp ___ ~_ Operator ----- Gas Actual Reading Net Actual Reading t02 was determined lIsing a gas analyzer CO is not measured, as it has the same molecular weight as N2 Net Nel Volume Yellow Cake Dryer Baghouse NYC Baghouse M5 Facility: Denison Mines Date: nl2\/lI Stack Identification: rJ 'I c... \3 S~ " () J Se.-,,' IMPINGERS Final (g) Initial (g) Net (g) Run: ----Sample Box: P ---- Implnger Number I 3 I 4 I 5 6 .......... Initial Volume of liquid (H20) in impingers, (mt) 100 100 I I Silica Gel I "98.0 ~LO\~ SCfcLL.-<fl2ler 1,{,",} {"o~ ·a Sq{)I~ gq~,> -r'J.3 V~((" ~,tc, IB·L<j Total (g) i 8,2 . j fRK. ~============== -.. -~---.----.-._---_. __ .. _-_._._-----.---.----.----.-----.. ---------------.-.-~----.-.----_. __ ._. __ ._._. __ ....... _----------------- IMPINGERS Run: ----Sample Box: ----- 1 2 Impinger NUlnber I-Lilli Initial Volume of liquid (H20) in impingers, (mt) 100 100 I I Silica Gel I Final (g) ___ --1 ___ --1 ___ --+ ___ --+ ___ --+ ____ _ Initial (g) -------I-------I-----~--------+------+--------Net (g) ============================================= IMPINGERS Run: ----Sample Box: ---- Impinger ~ umber 1 -l..1.L1...L15 6 -Initial Volume ofliquid (H20) in impingers, (ml) [00 100 I I Silica Gel I Final (g) ------~------~------~------~------~--------Initial (g) ------~~----~~----~------~------~--------Net (g) ============================================= Total (g) ============== IMeINGERS Run: ------Sample Box: ---- Implnger Number ..L ~ I .J. I .!, I 5 6 Initial Volume of liquid (H20) in impingers, (ml) 100 I 00 I I Silica Gel I Final (g)-----ll----~----~--------t-----t---- Initial (g) ____ --1,.--____ --1 ____ --1 ___ --1 ____ --+ ____ _ Net (g) ============================================= Total (g) ================ Grizzly Baghouse rvlethod 5 Faci I it) : ___ O.:.....;:e..:...;.A...:..::.-: S_o_{\_--!-M....;:. \.!...;I Y\....:..e..~> _______ _ Date: l II tv l( Stack I dentification: __ -..:2b:...:.t....1;...::L=..:?..=-:!~'lI-t ___ ~ ________ _ IMPINGERS Filter Number: s;e~L IMPINGERS Filter Number: IMPINGERS Filter Number: Run: -----\ Sample Box: ~ __ 2 lmpinger N1.unber ~ I 4 I 5 ~ InItial V(!/ume ofhqUid d-J:O) In Itnpinger::.. (ml) I ()O 100 1 I \dk(l {"I I Final (gl " ': 0 Initial (~) 'GtS.o ~~~-~~~-~----+-~~~4_----~------- Net (gl .... 3~.O Total (~l Run: -----Sample Box: ___ _ Implnger NUluber 3 I 4 I 5 6 Inlttal VoIUrllt' of liquid (\-120) 1I1llnpmgcb. (ml) Final (gl -------~----+------+------4_------~------ Initial (g) -------+-----+------~-----_r------~------Net (g) ==========================~====~======= Total (g) ======== Run: ----Sample Box: ---- Implnger Number ....L -1--13 1J...li 6 Initial Volume of liquid (H20) in impingers_ (ml) 100 100 I I "ilicl ~ic;1 I Final (gl --------r------+-------+-------4-------~------- Initial (g) --------r-----+------+------4-------~-------Net (g) ==========================~====~======= Total (g) ======== Chain of Custody Record Tt.l-4124 (1007' Client Tetco -.....• --~.,-.~.--... "., ........... -.. -.... -................. -Address 391 East 620 South City I State l'zlp Corle American Fork Ut 84003. Profect Name and Location ISta.teJ Denison Mine 20114th Qt.Jart.:er ContJaotlPurchtuJe OrdGrIQvote No. -.--... -... ~-.....•.. -.... ,,, .. ~-,-~~-... , Sample J. D. No. and DescriptIOn Date (Containers far each sampltP may be combined on one lme) 5841 R1 Grizzly filter and beaker 11/22/11 5836 R1 NYC filters{5837,5842) and beaker 11/21/11 5843 R2 NYC filters(5844) and beaker 11/22/11 5838 Baghouse Filter and beaker 11/21/11 -.~--.----.... ._ ..... _ •• ~ ....... _ •••• H •••••• _ •• ~." ........... ______ • __ •••• " ••• __ Possible Hazard Identification o Non-Hazsro o Flammable o SKin Irril8nt o PoisonS Tum Around Time Required Temperature on Receipt __ _ TestAmerica Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMEN1AL TESTING P(()/set Msnafler Date Chail.7 01 Cus/t:Jdv Number Dean Kitchen 11/28/2011 i6iepho(18 NUmber (:Area Code)IFax Number LebNumber _J~Q~~_':l9Z -9,lQ6 Page of .. -.~ •.. ,- Site Contact Lab Contact Anafysis (Attach list rt Scott Christensen,Ryall Palmer more space Is needed) Cartie",Waybifl MHllber Spec/allnstructlons/ Containers & Q Conditions of Receipt Matrix PreS8fYstives 0 ~ 1"1 .. m N & L ... i ~ ~. ~ «'l' -b I ~ i ~~ ~ is 1\1 III· nme '8 2 a: S .b <C ;4 __ c-f--. 8:30 X ! X X i ...... ~ ..... ~' .. H. -~ ...... ~ ........... ~ ...... -.. 8:00 X X X X X 8:00 X X X X X 9:30 X 1 x. .X X X I ... -.•.... ....... -.-... ,~.".-, ....... J __ _ .0- i I ~ I I I .......... ... -,", . _" ....... I I ! i .. --.----.. _,-I Semple DispoSBI (A fee may be as.sesseo if s8!tl(Jfes 8rt: rei8med o Unknown 0 Return To Client o Disposal By Lab o Archive For ___ Months longer th.m 1 month) • aCRcq,jiremsnts (Specify) o 24~.c~r~ ,::9 48 Hours ~R: ~ys o 14 Days 0 21 Days 0 othera.SD.er method Oats L J i ""'" . I" """";..,.; By ,-, Tan. t, Relfnatlsh;d By b "' ~ .. -.... !.&~ 7.£--.. ?~~!. T1~'-:-~ O_O_+r 2:;-.-;;R::-ooe-.-cIvedc:-;-;By::------------------"-='-.----l...;;;-~--- 3. RGiinquished By Comments When Complete Email to:DeanorPaultetco@tetco-ut.com b!f:fTR IBUTJON: WHITe· Refurrred to C!ief/{ wilh Report; CANARY-Stays with fheSair.ple; -PINK -Ff$ld Copy soc No. Order No. 44230 Analytical Data Package Prepared For DellisOll Mines (USA) Cor p. 2011 4th Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 23 Pages Report No.: 50369 Results in this report relate only to the sampJe(s) analyzed. Client Sample ID (List Order) Lot-Sa No. WorkO.·dcr Report DB ID 5836 R1 NYC J1 L020485-2 MPEV81AD 9MPEV810 FIL TERS(5837 ,5842) 5836 R1 NYC J 1 L020485-2 MPEV81AC 9MPEV810 FILTERS(5837,5842) 5836 R1 NYC J 1 L020485-2 MPEV82AA 9MPEV820 FIL TERS(5837 ,5842) 5836 R1 NYC J 1 L020485·2 MPEV82AE 9MPEV820 FILTERS( 5837 ,5842) 5838 BAGHOUSE FILTER J1 L020485-4 MPEWA1AD 9MPEWA10 AND BEAKE 5838 BAGHOUSE FILTER J 1 L020485-4 MPEWA1AC 9MPEWA10 AND BEAKE 5838 BAGHOUSE FILTER J1 L020485-4 MPEWA1AA 9MPEWA10 AND BEAKE 5838 BAGHOUSE FILTER J1 L020485·4 MPEWA1AE 9MPEWA10 AND BEAKE 5841 R1 GRIZZLY FILTER J1 L020485·1 MPEV71AA 9MPEV710 AND BEA 5841 R1 GRIZZLY FILTER J1 L020485·1 MPEV71AE 9MPEV710 AND BEA 5843 R2 NYC J 1 L020485·3 NIPEV91AD 9MPEV910 FIL TERS(5844) AND 5843 R2 NYC J 1 L020485·3 MPEV91AC 9MPEV910 FILTERS(5844) AND 5843 R2 NYC J1 L020485·3 MPEV92AA 9MPEV920 FIL TERS(5844) AND 5843 R2 NYC J1 L020485·3 MPEV92AE 9MPEV920 FIL TERS(5844) AND ---_._----_._-------_. TestAmerica rptSTLRchTitle v3.73 TestAmerica Laboratories, Inc. Batch No. 1340141 1340142 1340143 1355141 1340141 1340142 1340143 1340144 1342159 1342160 1340141 1340142 1340143 1355141 Certificate of Analysis January 30, 2012 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDG Number I. Introduction December ),2011 Denison Mine 2011 4th Quarter Four (4) Stack Filter Samples 44230 CASE NARRATIVE On December 1,2011, four stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J 1 L020485. 11. Sample Receipt The samples were received in good eondition and no anomalies were noted during check~in. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical unceliainties. The analysis requested was: TestAmerica Laboratories, fnc. Alpha Spectt·oscopy Thorium-228, -230, ~232 by method RL-ALP-OO t Uranium-234, -235, -238 by method RL-ALP-004 Gamma Spectroscopy Pb-210 by method RL-GA-OO I Alpha Scintillation Radium-226 by method RL-RA-OO 1 2 Denison Mines (USA) Corp January 30, 2012 lV. Quality Control The analytical result tor each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. V. Comments Alpba Spectroscopy Thorium-228,230,232 Samples 5836 Rl NYC and 5843 R2 NYC were put through the separates process a second time when U- 234 appeared in the Th-229 region of interest. The achieved MDA of the samples exceeds the detection limit due to insufficient sample volume. However, in most cases, the activity of the samples exceeds the MDA and detection limit. The data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Uranium-234, 235, 238 Samples 5836 Rl NYC and 5843 R2 NYC initially failed due to smeared spectra. The re-analysis is within acceptance criteria. The achieved MDA ofthe batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA (mel detection limit for three of the fOLlr samples. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Gamma Spectroscopy Pb-210 The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. The LCS recovery yield is just above acceptance limits. A recount did not improve the recovery. There is no sample volume remaining for re-analysis. Data is repOlted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Alpba Scintillation Radium-226 The Ba-133 tracer yield of sample 5836 R 1 NYC is below acceptance criteria due to slLspected matrix interferences. The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. Sample activity exceeds MDA and detection limit for all of the samples. Data is accepted. Except as noted, the LCS, batch blank and sample results are within acceptance limits. J certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan (~'-g(f\O~ 2012.01.31 10:37:00 -08'00' Erika Jordan Customer Service Manager TestAmerica Laboratories. Inc 3 Drinking Water Method Cross References DRINKING WATER ASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) TestAmerica Richland's SOP N EPA 901.1 Cs-134, 1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297~ 1994 Edition". The approach, "Law of Propagation of Errors", involves the identi fication of all variables in an analyticalmcthod which are used to derive a result. These variables arc related to the 3nalyticall'csult (R) by some functional relationship, R = constants * t~xs,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncettainties (ul) arc then combined using a statistical model that provides the most probable overall uncertainty val UC. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncettainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum~of .. the .. squares of the individualunceriainties. The uncertainty associated with the derived result is the combined uncertainty (ue) multiplied by the coverag(~ 1~lCt()r (1,2, or 3). When three or more sample replicates are lIsed to derive the analytical result. the type A uncertainty is the standard deviation of the mean value (Sl?n), where S is the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation ofthe general "Law of Propagation of Errors" equations and specific example are available on -.----------------- TestAmerica rl)tGell~ralllJfo v3.72 TestAmerica Laboratories, Inc. 4 o. Hatch Bias COCNo Count ErrOl' (#s) Total Uncert (#s) Uc_ Combined Uncertainty. (#s), Coverage Factor CRDL (RL) Lot-Sample No MDClMDA Primal), Detectol' Ratio U-234/1.1-238 RstfMDC RstlT ot U cet1 RCIlO.-t DB No RER SDG Sum Rpt Alpba Spec Rst(s) Work Order The QC preparation batch number that relates laboratory sampJes to QC samples that were prepared and analyzed together. Detined by the equation (Result/Expected)-J as clclined by ANSI N 13.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Scintillation Counting (LSe) the batch blank count is the background. All known uncertainties associated wilh the preparation and analysis of the sample are propagated to give a measure of tile uncertainty associated with the result, lie the combined uncertainty. The unceltainty is absolute and in the same units as the result. TI1C coverage factor defines the width of the confidence interval, 1,2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmcrica ·'default" nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency. Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=( 1.645 * Sqrt(2*(BkgmdCnt/BkgrndCntMin)/SCntMin)) * (Col1vFctl(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the Ll MS soltware to track samples received on the same day 10r a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield. and Volume with a Type I and II error probability of appro xi mal ely 5%. MDe = (4.65 * Sqrt((BkgrndCntIBkgrndCntMin)/SCntMin) + 2.7I1SCntMin) * (Cot1vFct/(Eff * Yld * Abn * Vol) * lngrFct). For LSC methods the batch blank is lIsed as a measure of the background variability. "n1e instmmenl identifier associated with the analysis of the sample aliquot. TI1e U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321 Cis 1.038. Ratio of the Result to the MDe. A value greater than I may indicate activity above background at a high level or confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor 01'2 a value greater tJlan I may indicate activity above background at approximately the 95%) level ofconfidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in conceIt with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Worl< Order Number. The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2+ TPUd2)] as defined by ICPT l30A where S is the original sample result, D is the result ofthe duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total unccliainty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by 'festAmerica upon sample receipt. The sum of the report.ed alpha spec results tor tests derived from the same sample excluding duplicate result where the results are in the same units. The L1MS software assign tcst specific identifier. i I I I I I I I I I I l Yield The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. I _________ -::.==--==-:-=-==---==:.--=-=-==-~__=====__== _ _:__===__=_= _ _==__=_--;;;:::=___==_=_=-_=_:;:_==_=__~==__=_=== _ _=__-=-..::==.:=-_c=:::_=~:._=.::;_==__=.:._==" .. =;""_;:"_=I. __ T estAmerica I'ptGcnerallnfo v3,72 TestAmerica Laboratories, Inc. 5 Sample Results Summary Date: 31-Jan-12 TestAmerica Ordered by Method, Batch No., Client Sample 10. Report No. : 50369 SDG No: 44230 Client Id Tracer Batch Work Order Parameter Result +-Uncertainty ( 2s) Qual Units Yield MOL CRDL RER2 1340143 RICHRC5011 5836 R1 NYC FIL TERS(5837,5842) MPEV82AA TH-228 1.44E-08 +-1.3E-08 U UCI/SA 50% 1.63E-08 3.00E-15 TH-230 2.20E-06 +-3.9E-07 Uel/SA 50% 1.55E-08 3.00E-15 TH-232 1.43E-08 +-1.4E-08 U UCI/SA 50% 1.88E-08 3.00E-15 5838 BAG HOUSE FIL TER AND BEAKE MPEWA1AA TH-228 5.47E-09 +-7.2E-09 U UCI/SA 102% 1.17E-08 3.00E-15 TH-230 9.04E-07 +-1.6E-07 UCI/SA 102% 9.29E-09 3.00E-15 TH-232 7.57E-09 +-7.6E-09 U UCI/SA 102% 9.29E-09 3.00E-15 5843 R2 NYC FIL TERS(5844) AND MPEV92AA TH-228 2.61E-08 +-2.2E-08 U UCI/SA 57% 3.67E-08 3.00E-15 TH-230 5.58E-06 +-9.3E-07 Uel/SA 57% 2.54E-08 3.00E-15 TH-232 3.04E-08 +-1.8E-08 UCI/SA 57% 1.58E-08 3.00E-15 1342159 RICHRC5011 5841 R1 GRIZZLY FIL TER AND BEA MPEV71AA TH-228 2.12E-08 +-1.4E-08 UCI/SA 88% 1.52E-08 3.00E-15 TH-230 9.51 E-07 +-1.7E-07 UCI/SA 88% 1.17E-08 3.00E-15 TH-232 1.58E-08 +-1.1 E-08 UCI/SA 88% 1.17E-08 3.00E-15 1340144 FFSR 5838 BAG HOUSE FILTER AND BEAKE MPEWA1AE U-234 1.20E-03 +-2.6E-04 UCI/SA 89% 3.22E-05 9.00E-15 U-235 4.71 E-05 +-3.6E-05 UCI/SA 89% 3.22E-05 9.00E-15 U-238 1.20E-03 +-2.6E-04 UCI/SA 89% 3.22E-05 9.00E-15 1342160 FFSR 5841 R1 GRIZZLY FILTER AND BEA MPEV71AE U-234 4.64E-06 +-1.7E-05 U UCI/SA 88% 4.53E-05 9.00E-15 U-235 2.09E-05 +-2.4E-05 U UCI/SA 88% 3.28E-05 9.00E-15 U-238 1.97E-05 +-2.4E-05 U UCI/SA 88% 3.66E-05 9.00E-15 1355141 FFSR 5836 R1 NYC FILTERS(5837,5842) MPEV82AE U-234 4.12E-02 +-9.1 E-03 UCI/SA 91% 1.29E-03 9.00E-15 U-235 1.81 E-03 +-1.4E-03 UCI/SA 91% 1.04E-03 9.00E-15 U-238 3.97E-02 +-8.9E-03 UCI/SA 91% 1.04E-03 9.00E-15 5843 R2 NYC FIL TERS(5844) AND MPEV92AE U-234 3.03E-02 +-7.8E-03 UCI/SA 94% 1.55E-03 9.00E-15 U-235 9.29E-04 +-1.1E-03 U Uel/SA 94% 1.25E-03 9.00E-15 T estAmerica RER2 -Replicate Error Ratio = (S-D)/lsqrt(sq(TPUs)+sq(TPlJd»)/ liS defined by ICPT BOA. rptSTLRchSaSum U Qual -Analyzed for but not detected above limiting criteria. Limit (~riteria is less than the Mdc/Mda/Mdl, Tot.al lllltcrt, CRD!', RDL or mary2 V5.2.18.2 not identified by gamma scan software. A2002 TestAme.rica Laboratories, Inc. 6 Report No. : 50369 Client Id Batch Work Order Parameter 1355141 FFSR 5843 R2 NYC FIL TERS(5844) AND MPEV92AE U-238 1340141 RICHRC5011 5836 R1 NYC FIL TERS(5837,5842) MPEV81AD Pb-210 5838 BAGHOUSE FILTER AND BEAKE MPEWA1AD Pb-210 5843 R2 NYC FIL TERS(5844) AND MPEV91AD Pb-210 1340142 RL-RA-001 5836 R1 NYC FILTERS(5837,5842) MPEV8iAC RA-226 5838 BAGHOUSE FILTER AND BEAKE MPEWA1AC RA-226 5843 R2 NYC FIL TERS(5844) AND MPEV91AC RA-226 No. of Results: 30 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample 10. Result +. Uncertainty (2s) Qual Units 2.90E-02 +-7.SE-03 UCI/SA 2.94E-05 +-S.OE-06 UCIISA 4.47E-07 +-3.6E-07 u UCI/SA 3.63E-OS +-6.3E-06 UCI/SA 5.60E-07 +-2.6E-07 9.02E-08 +-3.SE-08 4.02E-07 +-1.5E-07 Date: 31-Jan-12 SDG No: 44230 Tracer Yield 94% 72% 66% 48% 11% 95% 22% MOL CROl RER2 1.SSE-03 9.00E-iS 5.20E-07 6.00E-i4 5.91 E-07 6.00E-14 8.66E-07 6.00E-14 3.0SE-07 9.00E-14 4.22E-08 9.00E-14 1.54E-07 9.00E-14 T estAmerica rptSTLRchSa$um mary2 VS.2.18.2 A2002 RERl -Replicate Errol' Ratio = (S-D)/lsql't(sq(Tf'tJs)+sq(TPLJd»)1 as defined by ICPT BOA. lJ Qual -Analyzed for but not detected llbove limiting niter'in. Limit criteria is less than the MdrlMdaJMdl, Total (JJlced, eRD!., RilL or not identified by g:lmma SCan software. TestAmerica Laboratories, Inc. 7 QC Results Summary Date: 31 ~Jan-12 TestAmerica Ordered by Method, Batch No, QC Type,. Report No.: 50369 SDG No.: 44230 Batch Tracer LCS Work Order Parameter Result +-Uncertainty ( 25) Qual Units Yield Recovery Bias MOL RICHRC5011 1340143 BLANK ac, MPG251AA TH-22B -1.66E-OB +-2.3E-08 U UCI/SA 30% 7.05E-08 TH-230 3.24E-07 +-9.BE-OB UCI/SA 30% 4.92E-08 TH-232 1.50E-08 +-2.0E-OB U UCI/SA 30% 3.22E-08 1340143 LCS, MPG251AC TH-230 2.22E-06 +-3.7E-07 UCI/SA 95% 97% 0.0 1.34E-08 RICHRC5011 1342159 BLANK QC, MPJ091AA TH-228 2.70E-09 +-5.6E-09 U UCIISA 94% 1.1 7E-08 TH-230 4.94E-09 +-6.9E-09 U UCI/SA 94% 1.25E-08 TH-232 2.33E-09 +-4.3E-09 U UCI/SA 94% 8.21 E-09 1342159 LCS, MPJ091AC TH-230 1.78E-06 +-3.0E-07 UCI/SA 79% 99% 0.0 1.98E-08 FFSR 1340144 BLANK QC, MPG261AA U-234 2.24E-08 +-2.3E-08 U UCI/SA 99% 2.68E-08 U-235 O.OOE+OO +-1.1 E-08 U UCI/SA 99% 2.68E-08 U-238 8.97E-09 +-1.6E-08 U UCIISA 99 % 3.17E-08 1340144 LCS, MPG261AC U-234 8.22E-07 +-2.1 E-07 UCI/SA 71 % 83% -0.2 3.87E-08 U-238 1.10E-06 +-2.6E-07 UCI/SA 71 % 106% 0.1 4.56E-08 FFSR 1342160 BLANK QC, MPJ1A1AA U-234 -1 .24E-09 +-1.3E-08 U UCI/SA 102% 2.98E-08 U-235 3.73E-09 +-1.3E-08 U UCI/SA 102% 3.51E-08 U-238 3.73E-09 +-1.3E-08 U UCIISA 102% 3.51 E-08 1342160 LCS, MPJ1A1AC U-234 8.76E-07 +-2.2E-07 UCIISA 73% 93% -0.1 3.68E-08 U-238 1.18E-06 +-2.7E-07 UCI/SA 73% 119% 0.2 3.68E-08 FFSR 1355141 BLANK ac, MPVEH1AA U-234 1.16E-08 +-2.0E-08 U UCI/SA 95% 3.70E-08 U-235 -5.54E-10 +-1.4E-08 U UCIJSA 95% 2.79E-08 U-238 2.08E-08 +-2.4E-08 U UCIISA 95% 2.79E-08 1355141 LCS, MPVEH1AC U-234 1.00E-06 +-2.3E-07 UCI/SA 96% 102% 0.0 2.88E-08 U-238 1.00E-06 +-2.3E-07 UCI/SA 96% 97% 0.0 3.27E-08 RICHRC5011 1340141 BLANK ac, MPG211AA Pb-210 1.39E-07 +-3.3E-07 U UCI/SA 66% 5.71E-07 1340141 LCS , TestAmeriea Bias -(ResuJtJExp('{'tcd)-t as defined by ANSI N13.30. rptSTLRchQcSum lJ Qual-Analyzed for but not detected abow limiting (~riteria. Limit critl'I'ia is less than the MddMdalMdl, Total lJnccrt, CIU)L, HDt or mary V5.2.18.2 not iMntificd by gamm~\ scan softwat'c. A2002 TestAmerica Laboratories, Inc. 8 Report No. : 50369 Batch Work Order Parameter MPG212AC Pb-210 RL-RA-001 1340142 BLANK ac, MPG241 AA RA-226 1340142 LCS, MPG241AC RA-226 No. of Results: 27 QC Results Summary TestAmerica Ordered by Method, Batch No, QC Type,. Result +-Uncertainty ( 2s) Qual Units 1.59E-05 +-2.SE-06 UCIISA 1.23E-08 +-1. 9E-OS U 1.11 E-05 +-2.6E-06 T estAmerica Bias -(l{('sult/Expected).1 liS detlned by ANSI N 13.30. Date: 31-Jan-12 SDG No.: 44230 Tracer LCS Yield Recovery Bias MOL 52% 176% 0.8 7.63E-07 100% 3.05E-08 84% 112% 0.1 3.65E-08 rptSTLRchQcSum LJ Qual· Analyzed for but not ddeeted above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total l inred, CRDL, RDL or mary VS.2.18.2 not identified by gamma scall software. A2002 'festAmerica Laboratories, Inc. 9 FORM I Date: 31-Jan-12 SAMPLE RESULTS Lab Name: TestAmerica SDG: 44230 Collection Date: 11/21 /2011 8:00:00 AM Lot-Sample No.: J1L020485-2 Report No.: 50369 Received Date: 12/1/2011 11 :00:00 AM Client Sample 10: 5836 R1 NYC FILTERS(5837,5842) COC No.: Matrix: AIR FILTER 2011 4th Quarter Ordered b~ Client Sample 10, Batch No. Result Count · Total MOL, Rpt Unit, Yield RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstlTotUcert Prep Date Size Size Detector Batch: 1340141 RICHRC5011 Work Order: MPEV81AD Report DB 10: 9MPEV810 Pb-210 2.94E-05 B.3E-07 5.0E-06 5.20E-07 UCIISA 72% (56.6) 1/12/1202:39 p 1.0 0.98021 GPC31D 2.53E-07 6.00E-14 (11.7) Sample Sample Batch: 1340142 RL-RA-001 Work Order: MPEV81 AC Report DB 10: 9MPEV810 RA-226 5.60E-07 2.2E-07 2.6E-07 3.05E-07 11% (1.8) 1/11/1205:22 p 1.0 0.9802 ASC9MA 1.43E-07 9.00E-14 (4.3) 9 9 Batch: 1340143 RICHRC5011 Work Order: MPEV82AA Report DB 10: 9MPEV820 TH-228 1.44E-08 U 1.3E-OB 1.3E-08 1.63E-OB UC/ISA 50% 0.88 1/10/12 02:50 p 1.0 0.98021 AlP27 4.24E-09 3.00E-i5 (2.2) Sample Sample TH-230 2.20E-06 1.6E-07 3.9E-07 i.55E-OB UCI/SA 50% (141.8) 1/10/12 02:50 p 1.0 0.98021 ALP27 4.04E-09 3.00E-15 (11.2) Sample Sample TH-232 1.43E-08 U i.4E-08 1.4E-08 1.B8E-08 UCI/SA 50% 0.76 1/10/1202:50 p 1.0 0.98021 ALP27 5.71 E-09 3.00E-15 (2,) Sample Sample Batch: 1355141 FFSR Work Order: MPEV82AE Report DB 10: 9MPEV820 U-234 4.12E-02 6.5E-03 9.1 E-03 1.29E-03 UCI/SA 91 % (32.) 12/28/11 04:59 p 1.0 0.00002 AlP211 2.94E-04 9.00E-i5 (9.) Sample Sample U-235 1.B1E-03 1.4E-03 1.4E-03 1.04E-03 UCI/SA 91 % (1.7) 12/28/11 04:59 p 1.0 0.00002 ALP211 1.70E-04 9.00E-i5 (2.6) Sample Sample U-238 3.97E-02 6.4E-03 8.9E-03 1.04E-03 UCI/SA 91 % (38.2) 12/28/11 04:59 p 1.0 0.00002 ALP211 1.70E-04 9.00E-15 (8.9) Sample Sample ----.-.•. ---------Ratio U·234/238 = 1.0 TestAmerica MDCIMDA,Lc. Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency. Yield, and Volume. rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdclMda/Mdf, Total Uncert, CROL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 Lab Name: TestAmerica Lot-Sample No.: J1 L020485-2 FORM I SAMPLE RESULTS SOG: 44230 Report No. : 50369 Client Sample 10: 5836 R1 NYC FIL TERS(5837,5842) 2011 4th Quarter COC No.: Result Count Total MOL, Rpt Unit, Yield RstlMDL, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL} RstiTotUcert No. of Results: 8 Comments: Date: 31-Jan-12 Collection Date: 11/21/2011 8:00:00 AM Received Date: 12/1/2011 11 :00:00 AM Matrix: Analysis; Prep Date AIR FILTER Ordered by Client Sample ID, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MOCIMOA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.1S.2 A2002 FORM I Date: 31-Jan-12 SAMPLE RESULTS Lab Name: TestAmerica SDG: 44230 Collection Date: 11/21/2011 9:30:00 AM Lot-Sample No.: J1L020485-4 Report No.: 50369 Received Date: 12/1/201111 :00:00AM Client Sample 10: 5838 BAGHOUSE FILTER AND BEAK COC No.: Matrix: AIR FILTER 2011 4th Quarter Ordered b~ Client Sample 10, Batch No. Result Count Total MOL, Rpt Unit, Yield RstiMOL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDl(Rl) RstiTotUcert Prep Date Size Size Detector Batch: 1340141 RICHRC5011 Work Order: MPEWA 1AD Report DB ID: 9MPEWA10 Pb-210 4.47E-07 U 3.5E-07 3.6E-07 5.91 E-07 UCI/SA 66% 0.76 1/12/1202:39 p 1.0 0.98996 GPC32B 2.88E-07 6.00E-14 (2.5) Sample Sample Batch: 1340142 RL-RA-001 Work Order: MPEWA1AC Report DB 10: 9MPEWA10 RA-226 9.02E-08 3.0E-08 3.5E-OB 4.22E-08 95% (2.1) 1/11/1205:21 p 1.0 0.99 ASCDUE 1.99E-08 9.00E-14 (5.1) 9 9 Batch: 1340143 RICHRC5011 Work Order: MPEWA1AA Report DB ID: 9MPEWA10 TH-228 5.47E-09 U 7.1E-09 7.2E-09 1.17E-OB UCI/SA 102% 0.47 12/30/11 07:55 p 1.0 0.98996 ALP27 3.56E-09 3.00E-15 (1.5) Sample Sample TH-230 9.04E-07 7.7E-OB 1.6E-07 9.29E-09 UCI/SA 102% (97. 3) 12/30/1107:55 p 1.0 0.98996 ALP27 2.42E-09 3.00E-15 (11.1) Sample Sample TH-232 7.57E-09 U 7.5E-09 7.6E-09 9.29E-09 UCIISA 102% 0.81 12/30/11 07:55 p 1.0 0.98996 ALP27 2.42E-09 3.00E-15 (2.) Sample Sample Batch: 1340144 FFSR Work Order: MPEWA1AE Report DB 10: 9MPEWA 10 U-234 1.20E-03 1.BE-04 2.6E-04 3.22E-05 UCI/SA 89% (37.2) 12/16/11 06:00 p 1.0 0.00102 ALP10 7.01 E-06 9.00E-15 (9.2) Sample Sample U-235 4.71E-05 3.6E-05 3.6E-05 3.22E-05 UCIISA 89% (1.5) 12/16/11 06:00 p 1.0 0.00102 ALP10 7.01 E-06 9.00E-15 (2.6) Sample Sample U-238 1.20E-03 1.8E-04 2.6E-04 3.22E-05 UCI/SA 89% (37.3) 12/16/11 06:00 p 1.0 0.00102 ALPi0 7.01E-06 9.00E-15 (9.2) Sample Sample -------- RaUo U-2341238 = 1.0 TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTlRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Tota! Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 TestAmenca LaboratOrIes. lne. 12 Lab Name: TestAmerica Lot-Sample No.: J1l020485-4 FORM I SAMPLE RESULTS SDG: 44230 Client Sample 10: 5838 BAGHOUSE FILTER AND BEAK 2011 4th Quarter Report No. : 50369 COC No.: Result Count Total MOL, Rpt Unit, Yield RstlMDL, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDl(RL) RstlTotUcert No. of Results: 8 Comments: Date: 31-Jan-12 Collection Date: 11/21/2011 9:30:00 AM Received Date: 12/1/2011 11 :00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample 10, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 FORM I Date: 31-Jan-12 SAMPLE RESULTS lab Name: TestAmerica SDG: 44230 Collection Date: 11/22/2011 8:30:00 AM Lot-Sample No.: J1 L020485-1 Report No.: 50369 Received Date: 12/1/2011 11 :00:00 AM Client Sample 10: 5841 R1 GRIZZLY FILTER AND BEA COC No.: Matrix: AIR FILTER 2011 4th Quarter Ordered b~ Client Sample 10, Batch No. Result Count Total MOL, Rpt Unit, Yield RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstiTotUcert Prep Date Size Size Detector Batch: 1342159 RICHRC5011 Work Order: MPEV71AA Report DB ID: 9MPEV710 TH-228 2.12E-08 1.3E-08 1.4E-OS 1.S2E-08 UCI/SA 88% (1.4) 12/24/11 01 : 12 a 1.0 0.98988 ALP113 S.37E-09 3.00E-1S (3.1) Sample Sample TH-230 9.51E-07 7.SE-08 i .7E-07 1.17E-08 UCI/SA SS% (81.7) 12/24111 01:12 a 1.0 0.98988 ALP113 3.6SE-09 3.00E-1S (11.2) Sample Sample TH-232 1.5SE-08 1.1 E-OS 1.1 E-08 1.17E-OS UCI/SA 88% (1.4) 12/24/1101:12 a 1.0 0.98988 ALP113 3.68E-09 3.00E-1S (2.9) Sample Sample Batch: 1342160 FFSR Work Order: MPEV71AE Report DB 10: 9MPEV710 U-234 4.64E-06 U i.7E-05 1.7E-OS 4.S3E-05 UCI/SA 8S% 0.1 12127/11 12:02 p 1.0 0.0011 ALPS 1.48E-05 9.00E-iS 0.53 Sample Sample U-235 2.09E-05 U 2.3E-OS 2.4E-OS 3.2SE-05 UCIISA 88% 0.64 12/27/1 1 12:02 p 1.0 0.0011 ALPS 8.S3E-06 9.00E-iS (1.8) Sample Sample U-238 1.97E-05 U 2.4E-OS 2.4E-OS 3.66E-OS UCIISA 88% 0.54 12/27(11 12:02 p 1,0 0.0011 ALP5 1.0SE-OS 9.00E-15 (1.7) Sample Sample Ratio U·2341238 = 0.2 No. of Results: 6 Comments: TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limtting criteria. Limit criteria is less than the MdclMda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 J4 FORM I Date: 31-Jan-12 SAMPLE RESULTS Lab Name: TestAmerica SOG; 44230 Collection Date: 11/22/2011 8:00:00 AM lot-Sample No.: J1l020485-3 Report No. : 50369 Received Date: 12/1/2011 11:00:00 AM Client Sample 10: 5843 R2 NYC FIL TERS(5844) AND COC No.: Matrix: AIR FILTER 2011 4th Quarter Ordered b~ Client Samele ID, Batch No. Result Count Tota' MDL, Rpt Unit, Yield RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstlTotUcert Prep Date Size Size Detector Batch: 1340141 RICHRC5011 Work Order: MPEV91AD Report DB ID: 9MPEV910 Pb-21 0 3.63E-05 1.2E-06 6.3E-06 8.66E-07 UCI/SA 48% (42.) 1/12/12 02:39 p 1.0 0.98994 GPC32A 4.22E-07 6.00E-14 (11.5) Sample Sample Batch: 1340142 RL-RA-001 Work Order: MPEV91AC Report DB ID: 9MPEV910 RA-226 4.02E-07 1.1 E-07 1.5E-07 1.S4E-07 22% (2.6) 1/11/12 05:23 p 1.0 0.9899 ASCASA 7.23E-08 9.00E-14 (5.3) 9 9 Batch: 1340143 RICHRC5011 Work Order: MPEV92AA Report DB 10: 9MPEV920 TH-228 2.61E-08 U 2.2E-08 2.2E-08 3.67E-08 UCI/SA 57% 0.71 1/10/1202:51 p 1.0 0.98994 ALP28 1.51 E-08 3.00E-15 (2.3) Sample Sample TH-230 5.58E-06 2.3E-07 9.3E-07 2.54E-08 UCI/SA 57% (219.9) 1/10/1202:51 p 1.0 0.98994 ALP28 9.57E-09 3.00E-15 (11.9) Sample Sample TH-232 3.04E-08 1.7E-08 1.8E-08 i.58E-08 UCI/SA 57% (1.9) 1/10/1202:51 p 1.0 0.98994 ALP28 4.79E-09 3.00E-15 (3.4) Sample Sample Batch: 1355141 FFSR Work Order: MPEV92AE Report DB ID: 9MPEV920 U-234 3.03E-02 6.1 E-03 7.8E-03 i.55E-03 UCIISA 94% (19.6) 12/28/11 05:00 p 1.0 0.00002 ALP212 3.53E-04 9.00E-15 (7.8) Sample Sample U-235 9.29E-04 U 1.1 E-03 1.1 E-03 1.2SE-03 UCI/SA 94% 0.75 12/28/11 05:00 p 1.0 0.00002 ALP212 2.04E-04 9.00E-15 (1.7) Sample Sample U-238 2.90E-02 6.0E-03 7.5E-03 i.55E-03 UCI/SA 94% (18.8) 12/28/11 05:00 p 1.0 0.00002 ALP212 3.53E-04 9.00E-15 (7.7) Sample Sample _._. __ ~ __ M ____ Ratio U-2341238 = 1.0 TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSampte U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/MdJ, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 Lab Name: TestAmerica Lot-Sample No.: J1 L020485-3 FORM I SAMPLE RESULTS SOG: 44230 Client Sample 10; 5843 R2 NYC Fil TERS(5844) AND 2011 4th Quarter Report No. ; 50369 COC No.: Result Count Total MOL, Rpt Unit, Yield RstlMDL, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstlTotUcert No. of Results: 8 Comments: Date: 31-Jan-12 Collection Date: 11/22/2011 8:00:00 AM Received Date: 12/1/2011 11:00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample ID, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/MdalMdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.18.2 A2002 FORM II Date: 31-Jan-12 BLANK RESUl TS Lab Name: T estAmerica SOG: 44230 Matrix: AIR Report No. : 50369 Count Total MOL, Rpt Unit, RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDl Yield RstlTotUcert Prep Date Size Size Detector Batch: 1340141 RICHRC5011 Work Order: MPG211AA Report DB 10: MPG211 AB Pb-21 0 1.39E-07 U 3.3E-07 3.3E-07 5.71 E-07 UCI/SA 66% 0.24 1/12/1202:39 p 220.59 220.59 GPC32C 2.78E-07 6.00E-14 0.85 Sample Sample Batch: 1340142 RL-RA-001 Work Order: MPG241AA Report DB 10: MPG241AB RA-226 1.23E-OB U 1.BE-OB 1.9E-OB 3.05E-OB 100% 0.4 1/11/1205:21 p 220.59 ASCESD 1.43E-OB 9.00E-14 (1.3) 9 Batch: 1340144 FFSR Work Order: MPG261AA Report DB 10: MPG261AB U-234 2.24E-OB U 2.3E-OB 2.3E-08 2.6BE-08 UCI/SA 99% 0.84 12/16/11 06:01 p 1.0 1.0 ALP11 5.83E-09 9.00E-1S (2.) Sample Sample U-235 O.OOE+OO U O.OE+OO 1.1 E-08 2.68E-08 UCI/SA 99% O. 12116/11 06:01 p 1.0 1.0 ALP11 5.83E-09 9.00E-iS O. Sample Sample U-238 B.97E-09 U 1.6E-08 1.6E-08 3.17E-08 UCI/SA 99% 0.28 12/16/1106:01 p 1.0 1.0 ALP11 8.24E-09 9.00E-15 (1,1) Sample Sample Ratio U-2341238 = 2.5 ----- Batch: 1342160 FFSR Work Order: MPJ1A1AA Report DB 10: MPJ1A1AB U-234 -1.24E-09 U 1.3E-08 1.3E-08 2.98E-08 UCI/SA 102% -0.04 12/27/1112:03p 0.25 0.25 ALP7 6.47E-09 9.00E-i5 -0.2 Sample Sample U-235 3.73E-09 U 1.3E-08 1.3E-08 3.51 E-08 UCI/SA 102% 0.11 12/271'11 12:03 p 0.25 0.25 ALP7 9.1SE-09 9.00E-iS 0.58 Sample Sample U-238 3.73E-09 U 1.3E-08 1.3E-08 3.51 E-08 UCI/SA 102% 0.11 12/27/11 12:03 p 0.25 0.25 ALP? 9.15E-09 9.00E-15 0.58 Sample Sample Ratio U-2341238 = -0.3 ------------------.-.--~--------.---,--.---Batch: 1355141 FFSR Work Order: MPVEH1AA Report DB 10: MPVEH1AB TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBlank lJ Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdcfMda/!\'ldl, Totallincert, CRDL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 TesrAmerlca Laboratones .. Inc. 17 FORM II Date: 31-Jan-12 BLANK RESUL TS Lab Name: TestAmerica SDG: 44230 Matrix: AIR Report No. : 50369 Count Total MOL, Rpt Unit, RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error (2 s) Uncert( 2 s) Lc CROL Yield RstlTotUcert Prep Date Size Size Detector U-234 1.16E-OB U 2.0E-OB 2.0E-OB 3.70E-OB UCI/SA 95% 0.31 12/28/11 05:00 p 0.99 0.99 ALP213 9.12E-09 9.00E-1S (1.2) Sample Sample U-235 -S.S4E-10 U 1.4E-08 1.4E-08 2.79E-08 UCI/SA 9S% -0.02 12/2B/11 OS:OO p 0.99 0.99 ALP213 4.56E-09 9.00E-15 -O.OB Sample Sample U-238 2.0BE-08 U 2.4E-08 2.4E-08 2.79E-08 UCI/SA 95% 0.75 12/28/11 05:00 p 0.99 0.99 ALP213 4.56E-09 9.00E-15 (1.7) Sample Sample Ratio U-2341238 = 0.6 Batch: 1340143 RICHRC5011 Work Order: MPG251AA Report DB 10: MPG251AB TH-228 -i.66E-08 U 2.3E-08 2.3E-08 7.05E-08 UCI/SA 30% -0.23 12/30/11 07:55 p 220.59 220.59 ALP28 2.87E-OB 3.00E-15 -( 1.4) Sample Sample TH-230 3.24E-07 B.OE-OS 9.8E-OS 4.92E-OB UCI/SA 30% (6.6) 12/30/11 07:55 p 220.59 220.59 ALP2B 1.B2E-08 3.00E-i5 (6.6) Sample Sample TH-232 1.50E-08 U 1.9E-OB 2.0E-OB 3.22E-08 UCI/SA 30% 0.47 12130/11 07:55 p 220.59 220.59 ALP2B 9.75E-09 3.00E-15 (1.S) Sample Sample Batch: 1342159 RICHRC5011 Work Order: MPJ091AA Report DB 10: MPJ091AB TH-228 2.70E-09 U 5.6E-09 5.6E-09 1.17E-OS UCI/SA 94% 0.23 12/24/1101:1 2a 199.46 199.46 ALP116 3.S2E-09 3.00E.;.15 0.96 Sample Sample TH-230 4.94E-09 U 6.9E-09 6.9E-09 1.25E-08 UCIISA 94% 0.4 12/24/1101:12 a 199.46 199.46 ALP116 4.2SE-09 3.00E-15 (1.4) Sample Sample TH-232 2.33E-09 U 4.3E-09 4.3E-09 B.21 E-09 UCf/SA 94% 0.2S 12/24/11 01 :12 a 199.46 199.46 ALP116 2.14E-09 3.00E-15 (1.1) Sample Sample .'---'-~--~--------'---.-------'----------'-----.---------_._--------_._--.- No. of Results: 17 Comments: TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBlank lJ Qual -Analyzed for but not detected above limiting criteria. Limit criteria is Jess than the Mdc/Mda/Mdl. Total Vncert, CRDL. RDL or not identified by gamma scan software. V5.2.18.2 A2002 TcstAmeflca Labomtones, Inc. lab Name: TestAmerica Matrix: AIR Count Parameter Result Qual Error (2s) Batch: 1340141 RICHRC5011 Pb-210 1.59E-05 8.1E-07 Batch: 1340142 RL-RA-001 RA-226 1.11 E-05 2.0E-07 -- Batch: 1340144 FFSR U-234 8.22E-07 1.6E-07 U-238 1.10E-06 1.9E-07 Batch: 1342160 FFSR U-234 8.76E-07 1.6E-07 U-238 1.18E-06 1.9E-07 Batch: 1355141 FFSR U-234 1.00E-06 1.7E-07 U-238 1.00E-06 1.7E-07 --------_._---- Batch: 1340143 RICHRC5011 FORM II Les RESULTS Total Report Expected Uncert( 2 s) MDL Unit Yield Expected Ullcert Work Order: MPG212AC Report DB ID: MPGZ12CS 2.8E-06 7.63E-07 UCI/SA 52% 9.02E-06 1.51 E-07 Ree Limits: 75 125 Work Order: MPG241 AC Report DB ID: MPG241CS 2.6E-06 3.65E-08 84% 9.93E-06 1.01 E-07 Ree Limits: 75 125 Work Order: MPG261AC Report DB ID: MPG261 CS 2.1E-07 3.87E-08 UCI/SA 71% 9.93E-07 3.08E-08 Ree Limits: 75 125 2.6E-07 4.56E-08 UCI/SA 71% 1.04E-06 3.22E-08 Rec Limits: 75 125 Date: 31-Jan-12 SDG: 44230 Report No. : 50369 Recovery, Analysis, Aliquot Primary Bias Prep Date Size Detector 176% 1/17/1211:01 a 220.35 GPC32B 0.8 Sample 112% 1/11/1205:21 p 220.35 ASCHMA 0.1 9 83% 12/16/1106:01 p 1.0 ALP12 -0.2 Sample 106% 12/16/11 06:01 p 1.0 ALP12 0.1 Sample -----_. -------.- Work Order: MPJ1A1AC Report DB 10: MPJ1A1CS 2.2E-07 3.68E-08 UCI/SA 73% 9.44E-07 2.93E-08 93% 12/27/1112:03p 0,26 ALP8 Ree Limits: 75 125 -0.1 Sample 2.7E-07 3.68E-08 UCi/SA 73% 9.89E-07 3,07E-08 119% 12/27/11 12:03 p 0.26 ALP8 Rec Limits: 75 125 0.2 Sample .-----------_._- Work Order: MPVEH1AC Report DB 10: MPVEH1 CS 2.3E-07 2.88E-08 UCI/SA 96% 9.84E-07 3.05E-08 102% 12/28/11 05:01 p 1.01 ALP215 Rec Limits: 75 125 0.0 Sample 2.3E-07 3.27E-08 UCI/SA 96% 1.03E-06 3.20E-08 97% 12128/11 05:01 p 1.01 ALP215 Rec Limits: 75 125 0.0 Sample ---------.---------.---------~------------------------.. -~-----------.-.. --------.-.----... ----------- Work Order: MPG251AC Report OB 10: MPG251CS TestAmerica Bias -(Result/Expectedj-l as defined by ANSI N13.30. rptSTLRchLcs VS.2.18.2 A2002 19 lab Name: TestAmerica Matrix: AIR Count Parameter Result Qual Error ( 2 s) TH-230 2.22E-06 1.3E-07 Batch: 1342159 RICHRC5011 TH-230 i.78E-06 1,1 E-07 No. of Results: 10 Comments: Total Uncert( 2 s) 3.7E-07 MOL FORM II Les RESULTS Report Unit Yield 1.34E-08 UCI/SA 95% Ree limits: Expected Expected Uncert 2.29E-06 4.66E-08 75 125 Work Order: MPJ091AC Report DB 10: MPJ091CS 3.0E-07 i.98E-08 UCI/SA 79% i.80E-06 1.88E-08 Ree Limits: 75 125 TestAmerica Bias -(ResuIt/Expected)-l as defined by ANSI N13.30. rptSTLRchLcs V5.2.18.2 A2002 TestAmenca Laboratones. Inc. 20 SDG: 44230 Report No.: 50369 Recovery, Analysis, Bias Prep Date 97% 12/30/11 07:56 p 0.0 99% 12/24/11 01 : 12 a 0.0 Date: 31-Jan-12 Aliquot Primary Size Detector 220.35 ALP113 Sample 201.6 ALP118 Sample ~ >-::; r; rs i'-> , 1» CT' 0' f! Q 0" Y' ?) tv :~ ~ .. ; ~ -; ~ f: .'-' ~:, : ·«~~:'.;:I' ~:'~.~~:-! Chain of Custody Record Temperature on Receipt ___ ,_ Drjnkfng Water? Yes 0 No 0 TAL-4124 (IO07} Cll8m Prolect Manager Tetco , Dean Kitchen Address' -.-.-------.... -.--.--.-.--.. -l@lI3poon9 Numwr (Area Cods)/Fax Number ,391 East 620 South _.,,_,,_ ~._~O1.-49.-2:9.l0.6. City .. hate I ZIo Code Sife Contact , American ForkUt.. , 840.03 SwttChri.ten ... n,Ryanl'aimer Lal>Contacr Proiect Name and LOC<ltiorT 'Stare) CcIrlier/Wsybill Number Denison Mine 20114th Quarter TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 'Date ! f 11 !?8/2011 it. Commct/Purchliise Order/Quote No. Ma.trix Containers & Preserva5ves _._-.--.-..... _----.J Sample I.D_ No. and Description (Contamers fer each samp!o may /:)a cDmbined on on& line) 5841 Rl Grizzly filter and beaker 5836 Rl NYC filters(S837,S842) and beaker 5,843 R2N~C filters(58«.)_an? beaker 5838 Saghouse Filter and beaker ------. __ .,. Date Time 11/22/11 ,I 8:30 \. 11/21/11 . Ii 8:0.0 11/22/11 I' 8:00 11/21/11 . Ii 9:30 ~ 1 & I ~ I l ~ I tL~ X r-' ---'1-I 1 !X! i I !,X t I I fx ; [ I T I ,+-I I i i§1~i§ ~ ~~ Xl X X: .. ~! LX .. x. LxI x' X X x ' x. x' ... x· I I I I I I I I I I I CI"l8io of CLlSli:JeN Number Page of Special tnstnJctJonS/ Conditions of Receipt ~DG#L/'I2s0 {of-::#. J ! L()WY?S j I rT-1 ---~r____ ,---------, , I i I Iii 11111 H--H+UI---+--+-+11------+-----r ITrTT--1 I II I I I I I I ! ! I I LI I L ilL_I II II I i 1-1 rr-IIIIII I L.I,-------,---,-I 1--,---,-1 I ~II __ Possible Hazard Idsntificalic{1 ! Semple Dispc,58.1 I I I I I o Non-Hazard 0 Flammable 0 Skin. Irritwlt 0 Poison S 0 Unknown 10 Be1t.tm To Client Turn Around Time Rsqufred o 24 HoofS 0, 48 Hours ...... P 7 Days 0 14 Days 0 21 Days 0 ()ther as.oer method ..... ~ o Dlsposa( By LaD o Archive Fat ___ Monlhs (A fel: may be asse$3f)d if sernpfes f1.re rcteined longer than 1 month) 1. R.8EfiQtlisJlfJdBYi . ') [D2le/, ,Time .Dats . • Time / / ~ v./ / : /1 '0 . I '/' I II//," . .l---~ r '--7 __ ~ .. U2$"--?'!.!!J rV -<-) '", -j vU 2. ReJinq(jjshsd By ~ . I Dale I Time ,'Dats I 'f1me I 3. RelinqtJd1ed By I [)as I Time -i3. Rsceived~ I Date. I Time G<>mmellts When Complete Email to:DeanorPaultetco@tetco-ut.com DISTRIBUTION: WHITE: -Re!urned to erien! "lilh Repor/; CAlVARY -Stays wili1 fhe S2mpfe; FINK -Fl<;lcI Copy TestAmerica ......... ~~,.j~ 1'HE lEAD(;R IN I;NVl!WNMr.:mAL T!;HTIHG Sample Check-in List Date/Time ReCe1Ved:_'\.1l \ \ II 00 Container GM Screen Result: (Airlock) (,> 0 ,'.-"( Initia1skY~ Sample GM Screen Result (Sample Receiving) ~~7 ~=-)nitialsfC/~l DEN Client: __ .. _ .. _ .. ________ _ SDG#: 'l LI2 :J __ Q __ NA [] SAF#:._. _____ . ___ . ____ .~~~. __ .. ____ . ___ "_NAqf_ LotNumber: ___ 'S) l 0' 2(; <-( ? 5"' Chain of Custody # -_-.6J-1A ________ . _____ .. _______ . ___________________ _ Shipping Container ID: {~~ . NA [ ] Air Bill NLlmber: _________ . Samples received inside shipping container/cooler/box yes:rt-] Continue with 1 through 4. Initial appropriate response. No [ ] Go to 5, add conmlcnt. to #16. Yes [ No [ No Custody Seal ~ Yes [ No [ No Custody Seal 1)1:::::] 1. Custody Seals on shipping container intact? 2. Custody Seals dated and signed? 3. Cooler temperature: __ oC NADGJ· 4. Venniculite/packing materials is Wet [ Dry I: Item 5 through 16 for samples, Initial appropriate response. 5. 6. 7. 8. 9. 10. 11. 12, Chain of Custody record present? Ye~/] No[ Number of samples received (Each sample may contain multiple bottles): ___ 4 _________ _ Containers received: Lf X b&f\<e.f 'i X ?iti" k, S h ------_ .. _------------- Sample holding times exceeded? Samples have: _._~tape __ custody seals Matrix: A (FLT, Wipe, Solid, Soil) ~S (Air, Niosh 7400) ~les: are in good condition __ are broken __ Other ____ _ NA[ Yes [ hazard labels ~_ appropriate sample labels __ I (Water) . __ T (Biological, Ni-63) __ are leaking ___ have air bubbles (Only for samples requiring no head space) Samp,le. pH ~pp:-opriate for analysis requested . , -: es [ ] No [ ] NA~. , . (If aCldJtlCatlOn IS necessary, then docume t sample ID, lnltlal pH, amount of RNO) added anclp.1::I. after addItIOn on table overleaf) RPL ID # of preservative used: (\ . 13. Were any anomalies identified in sample receipt? Yes [ ] No & 14. Description of anomalies (include sample numbers): N~_~-__ ~_--_------- LS-023, Rev. 15,07/11 See over for additional information. 'restAmerica Laboratories, Inc. 22 TestAmerica JilLUai 7-.. ''!tft1! TH(' LJ:;AI)£R IN ENVIHONMENTAL TESrtNO 15. Sample Location, Sample Collector Listed on COe? * *For documentation only. No corrective action needed. 16. Additional Information: Yes~ No[ ------------------------.--------------------------A-~-[ J Client/Courier denied temperature check. fl-vrl)Client/Courier unpack cooler. Sample Custodian: ~__ ~ __ Date: 12 ~ J.-U----------/' Client Informed on, ____ _ by __________ __ Person contacted _______ _ N.No action necessary; process as is J..,. Pr~icct Manager .. ~ CJ.~---~,----Date ,t ?£!LI Ll1-----___________ _ SA1V1PLE ID Initial pH Acid Amt FinaIpE SAMPLEID Initial pH Acid Amt Final pH I" ~ I\r ~ ~ 'V~ ~ 1\/ Ww '\?(~ 'f4 "\'J \f~ ~ i" ,~ ---~ ,. ~ --/ 1\( 't-"'< l~\ \f ~~ ~ ~ ~ I\~ ~ \ \~ , :I ---\~ \~:> \~ ~ ~ 1"-::.. -- ------\ :;:J' K \ /' \/ ,,\ ~, \~ V y/; .. -~ /./ X 'V \ \ -- \ \ I~ \ LS-023, Rev. 15,07/11 See over for additional information. TestAmerica Laboratories, Inc, 23 APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Grizzly Baghouse Figure 3. Facility Schematic Representation Production and Control Equipnlent Data North Yello\v Cake (Scrubber F]ow Rates) Yellow Cake Dryer Baghouse (4.5 banels filled during test) Grizzly (tph of 11laterial and belt speed) o Facility: D ------~~~~~~--~~~~--.~------------------- Stackfdentification: North Yellovv Cake Scrubber e @ lllSOll Illes 1+-0~1 t , , a t y o a: Distance upstream from next disturbance, feet ~: Distance downstream from last disturbance~ feet y: Distance of Sample Level to Ground, feet 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, of 9 "'" .J -------------------- 9 ~., .J 6 ,-' .) ------------------ 1811 ------------------ 8-15%) 100-120 ------------------ Estimated Velocity, fpm 1,100 Control Unit Type: Scrubber Number of Ports 'I ~ Process Type: Yellow Cake Processing ~ L..-..--~ Figure 1. Facility Schematic Representation iii s Facility: D nlson t ex ! y 'f --------~~~--~~--~--~-------------------------------- Stack Identification: Yellow Cal<.e Bagll0'use 1+-0~1 : , ~ ex: Distance upstream from next disturbance, inches 57" ------------------- ~: Distance downstream from last disturbance, inches 454!1 y: Distance of Sample Level to Ground, feet 65' 0: Stack Inside Diameter, inches i61l ------------------- Estimated Moisture, percent O-~%) Estimated Temperature, of 125 ------------------- Estimated Velocity, fpm 1 AOO Control Unit Type: Baghouse Number ofPOlts 0(: Figure 2. Facility Sc ''') L Process Type: Yelio\Y Cake Proct'5sing FaCilily:Deni son IVlln e s t a ~ y Stack Identification: Grizzly Baghouse 1+-0-+1 13 a: Distance upstream fi'om next disturbance, inches 24.5" ------------------- 13: Distance downstream from last disturbance, inches 48ff '! ,>. _ 0 y: Distance of Sample Level to Ground, feet ____________ _ 18.75" 0: Stack Inside Diameter, inches ________ _ Estimated Moisture, percent 1 ~'O i~.mhient Estimated Temperature, of ------------------- Estimated Velocity, fpm 775 Number of Ports 2 Process Type: Control Unit Type: ""-""'---------11 Ore Unloading and Conveying Baghouse Figure 3. Facility Schematic Representation Denison Mine Process Data Source: North Yellow Cake Date: ttJel/ 21, 2011 Scrubber Flow GPM Time #1 #2 ~P 1//L 5, Iff 7JYf ~~E) 0; ~ bit 5d 18 4.,;q,~ 1;'1- IO~/:r 5 ~ 2,;"1..-IO.oLf 3 .1·~ 10 -J-{l 5,~1 9, ~tt 3~8 1/:18 '5 ¥l-n q,1't< ~~,~ I J : '..j to 5-, { 7 ~. ~f 3. ? 12:/((; ~ .. Z-2-/0.0 7 3.B /.l.:4!;" 5 .l-5' to.Of--3t(pQ 13~ 19 5/2.-"2-IO,Oz..-3'1'6 t"~;·s ( s ... " ~ z Z / () -00 ~ ·'-:>1- vLf ~ IS" f) .].-~ °1,18 :s -1-0 1tP.45" 5: oS-91&6 ~:tl lS:IS $,It.a ~~q{ 3.&9 16-:t.{8 G. "ll-/0. eo 'S.;t 2:- )(P : Lb 5 I IS 1. qt-~.&( ftl:4'( 5 ;l,.O <i.'1f ~.11- I~/S~" 5,/9 9.cty 3·fl t f; 'i& $ ,l9 '1 I Q &--) ,&5' Denison Mines Process Data Source: North Yellow Cake Date: Alev Z 2.., Loll Scrubber Flow GPM Time #1 #2 ~p 1-:/'( 5.1((2. '1~85-5 .. :;~l..- }643 ;) ./'1 ttv'l{ 3~Col- t?~11 5.12--CZ /:It, 3.~8 8: LIt.( '5 ~o8 CZ·&6 3 .. 13 9: /'-/ 5.0:;-'1. ~B "3>. &8 '7~'1y 5.o~ 9/&t1 3·1~ I 0 ; 13 5.1L cit t5' "3 . f(..; 10 : ~'3 ~.o~ ~t:rl 3,&;4 It.' 2~1 5~ to C'L fLf ~3 . u; (Q 11',6:; 5~ /~~ '1.r't ~31 fO 1'Z~Z.<! ~ lILt '1,"1'1 s. &;L{ t L: $',3 L/. €b' <1,33 3~~S- t '3 ! 2".'1 £../,57 q,e~ ~. ~'f f3 ~St..f '1ICfo a .. flo 3,10 I Lf. b 2J1 '-/ ,qt.f 1~ 41 ... 3.~~ Iq :5'1 ~ ,'13 1t~8 t{,OQ Denison Mines Process Data Source: Grizzly Baghouse Date: ll! L7-/tl Time Ton/Integrator tph fpm /' 1_\J~e{ Sf lo'l~3 ~;y) q'.IO ~ l 10 ) '10 101 /'1.., "7 ~ 1.1392.0 <-\ r '!Q<t~3 -" ?~l3'l~O 9u \3: l ) to~,3 t31~ '{ ( 1 t ~ ~ ~o 96 f ""(,, ~J ,'-\: if ?# t J ~ sf ~D taql~ 1<1'. l.\ 6' ll~ of) ~f l v~ ("3 Is: (J L l ~ ot..., ,(' ll) 109 , ( ,s: L.\ ( L/ "./ "l.\ t'))) SO \ oq(~ t~: ! )'~ ""2 .. 14 oq 0 3D lO~l'- l~:t{$" l..lLi\IO LfD l o'f I ~ tl : ,{ L-\ L\ \ Yo ~O loql t l'\~l(\ /"" L.J'i \L ) 50 10 't IL.. 1~: ,{ 1(1419) roO I Vert L- lB:ys 'll (~ 1.1.0 80 JoeL) /' t ~. ~' l I ") L(LtL<1f 1J I ocr ( l l q :t.f) Ll'il/) 3D It)C(I) APPENDIXE Calibration of the console dry gas 11leter(s), pitot tubes, nozzles dimneters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas rv1eter Calibration Data Fornls Type S Pitot Tube Inspection Data Smnple Box Temperature Sensor Calibration E Temperature Sensor t ~probe Type S Pitot Tube Temperature Nozzle t-WT~ sensor~ GoOSeneCk! . .~ ~i~ / Probe ----,. / Type S Pitot Tube ~ Temperature Sensor Glass Filter Holder Heated Area ImpingerTrain qJtional. May 8eRep/aced B! An Equivalent Condenser I Temperature Sensor ,-------------- tmpingers Stack Wall Manometer Dry Gas . \.. Meter ) Figure 4 Schematic of Method 51114 Salnpling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three entlcal onflces to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 9 ill!WdlIa__ ---..'."f!! _ . :~"~.,.-~, - I & .,"" ~?O~ 3) Run at tested vacuum (from Onfice Calibration Report). for a penod of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and Information In the GREEN cells. YELLOW cells are calculated. METER SERIAL #:!-I ---'''-'-..:..:.;;;....--\ CRITICAL ORIFICE SET SERIAL #: L' ___ ----' EQUIPMENT ID #: o G G K' I TESTED FACTOR VACUUM RUN;-] (AVG) I (in Hg) 0.8137 13 2 0.8137 13 0.8137 13 0.5317 13 0.5317 13 0.5317 13 0.3307 13 2 0.3307 13 0.3.307 13 949.50'1 954.735 960.015 966.9.02 972.1.24 977.544 983.4501) 988.857 994.191 USING THE CRITICAL ORIFJCES AS CALIBRATION STANDARDS' 954.735 9S0.015 965.317 972.124 .977.544 982 .• 827 988.857 994.191 999.697 5.234 5.280 5.302 5.222 5.420 5.283 5.407 5.334 5.506 72 68 72 73 '---_7_2_ 76 72 1:\2 72 86 72 88 72 88 7~ 89 72 92 73 66 613 76 68 7U ,---SO --'!~--70 86 72 76 88 76 80 _9~ ~-83 89 83 87 92 87 89 I 93 90 92 I INITIAL FINAL AVG(Pba,) 25.26 25.25 ELAPSED TIME (MIN) e 68.75 !1.00 4.4450 71.75 5.00 445.88 74.00 5.00 4.4585 79.00 7.50 1.12 4.3.318 82.50 1.75 1.12 44671 85.25 1.50 1.12 4.3322 86.75 12.25 0.42 4.4127 89.25 12.00 0.42 4.3333 91.75 12.25 0.42 4.4528 2011 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECAlIBRA TED 1 4.4552 L.QQ1 4.4552 0.999 4.4552 0 .• 999 AVG= 1.QQQ. -0.32 4.3668 1.008 4..5123 M1Q. 4.3668 1:QQ! AVG= 1.009 0.52 4.4361 1Jl.Q§. 4_3456 1.003 4.4361 0.996 AVG= 1.001 -0.20 1.564 1.556 1M2 1.542 1.532 1:.lli 1.470 1.464 1.457 The follOWing equations are used to calculate Ine standara volumes of air passed througl1 the DGM V", (SId) and the cntlcal onflce, V" (SId) and the DGM calibration factor Y These eauallons are automatically calculatea In the spreadSheet abol/e. AVERAGE DRY GAS METER CALIBRA nON FACTOR, Y;:: I 1.00f] (1) (2) (3) I'm",.,o . .: K., ",r'm* Pbar .... It:J.H I 13b) Tm Vcr ,,,I Fba,." ~ =-K'* 7ramb = Net volume of gas sample passed through DGM corrected to standard conditions K, '" 1764 °Riln rig IEngllsh) 03858 °K/fTlm Hg (Metnc) T", '" Absolute DGM avg temperature lOR· EngltstJ oK · Metnc) ;:: Volume of gas sample passed through the cntical onflce corrected to standard condillons Tan'" = .Aosolute afY1blent temperature (OR -Enghsn of< • Metnc) K = Average K' factor from Critical Onflce Callbrallofl I-er ,',' r= I-m .. ,,, = DGM calibration factor AVERAGE LlH@=\ 1.517 2 L\HIl!l = (0.75 e) LlH (VOl(std)) Vcr(std) v'" Temperature Sensors Reference In Out OF 33 67 201 OF 34 67 203 OF 34 67 202 PRE Console #4 Calibration 2011 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 'itt ~ §Hi1~--'-' 'tis MM·; __ " ,/-- 1) Select three critical onflces to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Onfice Calibration Report). for a penod of lime necessary to achieve a minimum lotal volume of 5 cubiC feet. 4) Record data and information In the r;;0" '."" cells, YELLOW cells are calculated. o G G RUN' I 2 2 3 K' FACTOR (AVG) 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 O.3l07 0.3307 0.3307 METER SERIAL #:1-1 ---C;':":';":;"-i CRITICAL ORIF!CE SET SERIAL #:L..' ___ -' TESTED VACUUM (inHg) 12 12 12 13 13 ~1_3_ 13 13 13 155.004 161.521 168.043 136.700 142.672 148.297 116.20 125.809 131.075 1&1.521 168.04;1 174.568 142.6n 148.297 153.926 125.809 131.075 13G.357 6.517 6.522 6.525 5.972 5.625 5.6.29 9.609 5.266 5.282 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 74 82 74 83 74 ,-------83 74 81 74 80 74 81 74 76 74 78 74 80 83 89 8'3 93 83 96 eo 84 81 86 82 ~ 78 77 SO 80 81 81 I 2011 Pre-Calibration INITIAL FINAL AVG (Pb.,) ~.10--1 25.10 IF Y VARIATION EXCEEDS 2.00%. ORIFICE SHOULD BE RECALIBRA TEO ELAPSED 1 DGM 1 TIME~MINII I 1 AVG 93 86.75 Ei.OQ 2.55 ~ 5.3045 9.:.m • 96 88.75 6.00 2 .• 55 5.3046 5.3045 1.000 99 90.25 (too 2.55 5 •. 2926 5.3045 1.W. -- AVG= 1.000 -0.09 86 82.76 8.50 1.11 4.8905 4 .• 9104 1.004 88 83.T5 8.00 1.11 4.5978 4,6215 1.005 "--~ 85.00 8.00 1.11 ~ 4.6215 1.007 AVG= 1.00S 0.47 80 77.75 Llli! 7.9047 0.997 81 79.75 4.3273 4.3117 0.996 84 81.50 4.3264 4.3117 0.997 AVG;: 0.997 ..(l.38 The follOWIng equanons are used to calculate the standard volumes of air passed through the DGM. V", (sid) and the crrtlCai oflf,ce V" (sid) and Ihe DGM calibration facto! Y These equations are automatically calculated ,n the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 1-1.001-, (1) (2) (3) ,'m".," = f.:.' T·m*!'bar.H8.H 13 0) Tm :: Net volume of gas sample passed through DGM. corrected to standard conditions K, ;: 1764 °Rlm /-ig <English, 03858 °Klf11m Hg (MelnC) Vel' '1,1 Pbal'~~ ""* JT;;l1b r'CI "W }'=--r"11I .. "1 Ton;: Absolute DGM avg temperature (OR -English ",< -MetriC) = Volume of gas sample passed through the Critical Orifice corrected to standard conditions T.mb" Aosolute ambient temperature \ OR _ Erglisl'1 "" -Metnc) K';: Average K' factor from Cntlcal Onflce Calibration = DGM calibratIOn factor AVERAGE c,.H@ =1 1.485 t.H@ = (0.75 S )2 tlH (Vm{std)) Vcr{std) V", Temperature Sensors Reference In Out OF OF OF 32 32 32 72 73 73 203 201 202 1.498 1.493 1.489 1.532 1..ill. 1.526 1.437 1.432 1.428 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical onflces to calibrate the dry gas meter which bracket the expected operating range 2) Record barometric pressure before and after calibration procedure 155 il!tltM/L-1!t!Ii!!!iiWF F""" ~ t~ ~ _!!r;;t~'-"., f 3) Run at tested vacuum (from Onflce Calibration Report). for a penod of time necessary to achieve a minimum total volume of 5 cubiC feet Facility Denison Mines 4) Record data and information m the GREEN cells. YELLOW cells are calculated K' TESTED FACTOR I VACUUM RUN# (AVG) (inHg) G: 0.5317 15 0.5317 15 0.5317 15 G: o.s~08 1.2 0.6808 12 0.6808 12 G: 0.3307 20 0.3307 20 0.3307 20 METER SERIAL #:c=J CRITICAL ORIFICE SET SERIAL #:~ 32.475 37.710 ~ - 49.677 55.475 61.298 I 14.152 I 19.693 I 24.736 37.710 42.940 48.174 55.475 61.298 67.113 19.693 24.736 29.785 5.235 5.230 5.234 5.798 5.823 5.815 5.541 5.043 5.049 USING THE CRITICAL ORIFICES AS CALI BRA nON STANDARDS: 64 64 S4 64 6'4 64 64 64 64 70 71 75 78 71 71 78 80 71 73 80 80 72 72 80 81 72 73 81 82 73 73 82 82 62 66 69 71 66 68 71 71 68 69 71 72 INITIAL DGM AVG 73.5 75 76 76.25 77.00 77.50 67.00 69.00 70.00 FINAL 25.65 ELAPSED TIME (MIN) e 7.50 7.pO 7.50 6.50 6.50 6.50 12.75 11.50 11.50 AVG (Pbo,) 25.65 t.l0 1.10 1.10 1.95 1.9.5 1.95 0.45 0.45 0.45 IF Y VARIATION EXCEEDS 2.00%. ORIFICE SHOULD BE RECALIBRATED 1 4.456 4.47 1.003 4.44 4.47 1.007 4.435 4.47 1.008 AVG= 1.006 0.56 4.9223 ~ 1:Qlli! 4.9366 4,960 1.005 4.9253 4.960 1.007 AVG= 1.006 0.63 4.7663 4.7260 0.992 4.3215 4.2627 0.986 4.3185 4.2627 0.987 AVG= 0.988 -1.19 The fOllOWing equations are used to calculate the standard volumes of air passed througtl the DGM V", (std) and the cntlcal onflce Vel (std) and tne DGM calibration factor. Y Tnese equations are automatically calculated In the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 11 .000 I (1) (2) (3) Vm = K, * Vm * P bar ..,. (!~J! II 3 6) Tm Vcr,.w , Pbar >l' e K'* JTamb = Net volume of gas sample passed through DGM corrected to standard conditions K. = 17 64 °R"n Hg (ECigllsh) 03858 °K/mm Hg {Metnc) T", ;: Absolute DGM avg 1emperature (OR -English oK· Metnc) = Volume of gas sample passed through the cntlcal onfice corrected to standard condllions T3mb = Absolute amolent temperature (oR· English OK -Metnc) K' = Average K' factor from Cntlcal Onflce Calioratlon Vcr"" y = -. = DGM calibration factor lIn,,,,,, AVERAGE~H@ =11.552] ~H@ = ( 0.75 e)2 ~H (Vm(std>\ Vc,(std) Vm ) 1.483 1.479 1.476 1.60 1.60 1.60 1.58 1.58 1.58 postcalibratlon 2011 #4 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ ,mttM&iMMlti1JM.WOW -_."., . "." . Ii) .tf, 4I¥E,d-- 1) Select three critical onflces to calibrate the dry gas meter wrllch bracket the expected operating range 2) Record barometric pressure before and after calibration procedure 3) Run at tested vacuum (from Orifice Calibration Report), for a penod of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and Information In the GREEN cells. YELLOW cells are calculated. METER SERIAL #:r--'-'---'---,! CRITICAL ORIFICE SET SERIAL #: 14535 EQUIPMENT ID #: K' TESTED ...------r----II FACTOR I VACUUM RUN# I (AVG) 0' 0: 0.33.07 0.3307 0.3307 0.5317 0.5311 0.5317 (inHg) 20 20 20 15 15 15 751.770 151.178 757,178 762.410 762.410 769.494 775.15Q 780.393 780.393 785.654 785.654 790.924 5.408 5.232 7.084 5.243 5.261 5.270 68 66 68 71 68 74 6.8 79 68 80 68 81 -- 71 66 74 71 n 76 80 85 81 89 82 90 71 76 81 89 90 90 D:~ I .0 .0 .0 I I I I I I USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: , Facility INITIAL FINAL AVG (Pba,) 25.65 25.65 ELAPSED TIME (MIN) e 68.5 12.50 73 12.00 77 ~ 83.25 7.50 1.10 85.00 7.50 1.10 85.75 7.50 1.10 0.00 §§ 0.00 0.00 Denison Mines 4.6380 4.4491 5.9791 4.3831 4.3840 4.3855 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 4.6157 ~ 4.4311 0.996 6.0005 1.004 AVG= 0.998 -0.86 4.4527 1.016 4.4527 1.016 4.4527 1.015 AVG= 1.016 0.86 AVG= The follOWing equations are used to calculate tne standard volumes of air passed through the OGM. V." (std) and the cntlcal Orifice V'" (std). and the OGM calibration factor Y These equations are automaticallY calculateo If' tne spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 11.007] (1) (2) (3) (1m .. ", = K, * Vm* Pbar+{t1H 1136) 7111 Vcr '1'/ Pbar "'~ K'* JTamb '" Net volume of gas sample passed through DGM corrected to standard conditions K, = 1764 °R/ln Hg (English) 03858 °Klmrn Hg (MetriC) T", = Absolute DGM avg temperature (OR -English OK -MetriC) = Volume of gas sample passed through the Critical onflce. corrected to standard conditions Tomb = AbSOlute ambient temperature (OR -Engllsn ~K -Metnc) K' = Average K' iactor from Cntlcal Onflce Calibration Vcr "J. r t.m "<1 = DGM calibration factor AVERAGE l1H@ =11.434 I l1H@= ( 0.75 e)2 ~H fY-m(std») Vc,(std) \ Vm 1.415 1.403 1.393 1.47 1.46 1.46 POST Console #5 Calibration 2010 Type S Pitot Tube Inspection Data Datt;!· <~t-I ff Pitot Tube Id..:ntification: ___ ...:........ _______ _ Dt PA"'.4SC';> in. ~P!.:...R "' __ ' _(,.!....I.....;:r;;:..--D~' ___ in. [\1 < 5° f'>l"" _____ _ ~Z--~.I~ I .......... t __ .n .--- Z :5.0.125 in, Z= I~ C) 1~~. in. C?~~:~:~+_ .. _.w W So O.oJ125 in. W=-_ . c)O'c_in, The pitot tube meets the specifications for a calibration f<lctor ofO.84'? Prahl'! Slack Temperature Sensor Calibrati~n· = Reference: Temperature Source (Medium) Continuitv tIeat Check 248 AIR ICE WATER BOIL WATER SILICONE OIL Tem erature Reft~rcn(e Sensor ("F) ("F) C> \ I '1.---in. '~71 (L": in, ;>,l' in, ye-.S Type S Pitot Tube Inspection Data Date: --------Pitot Tube Identification: "1,. "l. -6( --~~---------------- D\ Technician:_v_<_.--=~,---~-=-:..-.c:-=-'.:..:::::...::....:; ____ . ___ _ ,., ... Fj-· -'l-- A .-~ j PA r ~" in. PA = 1-1 t{ ~ in. 1'8 = ~ (d ~ in al < 10Q Ctj= Ct2 < 10° a2= Z::; 0.125 in, W ::;0.03125 in. W= ,d03 in, W > 3 inches W = __ -3..=. ___ in. Z > 3/4 Inch Z = __ "--___ 111 y", _-""S.e.._l_I_(....c....I_'l1 The Pltot tube meets the specifications for a caltbratlon factor of 0.84" "1 cmperature Sensor CalibratIOn Reference r'{~i~~;~~ Temperature Temperature Temperature Source Reference Sensor Difference (Mcdlluu) CF) ("F) (F) AIR IV ~"1 ( Probe Continuity .......-r ~_S_ Heat Check 248 -.:::::jJ \.( (/~ Z. {S.-C) AIR .. "10 Q(f) '1 r ICE \VATER ~~ ~ 3,,'? () Slack BOfL WATER -e. D S t11>e;--n SILICONE OIL = Ot Type S Pitot Tube Inspection Data Pitot Tube {dentificath>n: ~S ~ ~,-C>t Technician: Ko" r,,)9. ~ wt ~ f{'~~ ~=j:: Dt= ,s I S"- in. I p ... "" ({ S-<i( in. Pa ~ . 4c;~~ in. ((.\ < 100 at"" (',(2 < 10" Ct!'" c.. 131 < 5° Z~O.l25in . z=_,ooL in. . ~-. _~:=:=+~ .. _.w w:;; 0.03125 in. ,oJ /' W:= _----'_-'k2t.L-_ in. W> 3 inches G' W= in --Y'---- Z> 3/4 inch z= __ .....:-. ___ in. y:o __ 0_J ..:...%-.-;&t,-, _ in. The pitot tube m,\ets the specifications fo, a cnlibration factor of 0.84') y Stack Temperatur~ Sensor Calibration Reference: Tem eraturc Temperalure Diflerence (F) :~J---+----i~ . \ o BOIL WATER SfLlCONE OIL TETCO Sample Box Temperature Sensor Calibration Date ########tI CalIbrator. Mike McNamara ------------------------------------------- Unit I I) A B c D E F Thermocouple Location Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impingcr Out Oven Probe Out Impinger Out Impinger Out G Impinger Out H Impinger Out I Impinger Out J Temperature Source Reference Omega CL3512A Temp. OitT. or Result (!>F). P/F APPENDIX F The testing followed the sanle procedures as outlined in previous protocols and tests at this facility. ATTACHMENT H SURFACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-06 1.00E-07 1.00E-08 -CI) (ij (,) cn1.00E-09 C) o ...J - 1.00E-10 1.00E-11 1.00E-12 ~<o ~"OJ ~~ •• • . ~ i ----~ .. ~ ~"OJ ~1' Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) • • .. ... -.. -- 2>~ ~"Oj ~~ • -• • ..... -..., . • • ... .-.. ..... -"" OjOjfl:> ~~ ~ro ... i . ... .... • •• ~ • -- 2><0 ~"Oj ~,,~ "tV - • .. • • • .... • T ... .. T . ----------------------- ~ "OjOJ ,,~ ~ -------- ~" ~ ~~ro .. ~~ ~~ro • U-Nat. _ Th-230 A Ra-226 ------ ~c:o ~ ~ ,,~ ~~Oj ~ro ~rv • ... --• --- 1.00E-05 1.00E-06 1.00E-07 -Q) (ij (.) (1)1 .OOE-08 C) o ..J - 1.00E-09 1.00E-10 1.00E-11 • OJ'bf),, ~-,..;;, ~ • .. ~ Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) A • • • • • a •• • •••••• • • •• •••• •••• ••••• • ~ -::..,...03 ~~ ----_. --_ .. _- C?>C?>f)" ~-,..;;, ,...rV" -~-~~ - 9)'b ~,...Oj ~ro -_. • U-Nat. -Th-230 A Ra-226 ~'>::> ~ ~ ,..." ~C?> ~ ~,...03 0.1 0.01 0.001 0.0001 0.00001 -Q) ~.000001 (J) ~0000001 - 1 E-08 1 E-09 1 E-10 1 E-11 1 E-12 1 E-13 ~~OJ ~~~ ~OJ ~ ~~ ~<:S Westwater Creek Dissolved Radionuclide Concentrations (uCi/ml) ------------------ -- ,,~ ~ ~f\.t')) ,,~ <.j.rV~ ,,~ ~ ~~<:S ,,~ ~ \~qj ~~ ,,~ ~ rV~ • U-Nat. -Th-230 A Ra-226 ,,~ ~~~ ,,~ ~ ~~ ~ "Y ,," ~ ~ ~t')) ~~f\. ~~~ 0.1 0.01 0.001 0.0001 0.00001 -(1) ~.000001 (J) ®000001 ..J -1 E-08 1 E-09 1 E..,10 1 E-11 1 E-12 1 E-13 'f:>OJ ~~ ~OJ ~~b( ~~ Westwater Creek Suspended Radionuclide Concentrations (uCi/ml) 'I\~(;::) ~'1"l1) • ~(;::) ~~ ~~(;::) cS-~~ ~~(;::) :\~q) ~~ ~~~ rV'1"co • U-Nat -Th 230 A Ra-226 I ~~~ rd-co '::;..~~ ~~ - ~~~ ~ ~l1) :\~'1" ~~ (~) White Mesa Mill -Standard Operating Procedures Book # 11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-I Page 5 ofS Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA Mll..L LOCATION (Circle one):Cottonwood cree~er canyonyther (describe) ___ _ DATE: q/ 15 /~O I r pH BUFFER 7.0 _7-'--0 ___ _ BY: -J.:""e.r Uol/;1't (Sampler's initials) pH BUFFER 4.0 _L_l_, 0 ___ _ SPECIFIC CONDUCTIVITY -.&.q~q-!..1~ ______ u=M.:.:::H:.=..;O=s STEAM DEPTH: 3 i I --~--------------- pHofWATER ___ 7~<S~' ____________ ~ TEMP qD L- , l COND Umhos 1507.3 COND flmhos g 05 i.J pH Units 7 SS pH units /. by Temp °c }O · b'= COND flmhos go 5 . ~ COND flmhos ~05 .j pH units 7· bO pH units -1. £.:) Temp °C I D . b!:, Temp °c 10. f:.7 Comments: Epr-.5c...M.priv\.6 f'-VedAf.. p!)"cc",rlP..\= e..rS (educe 'tu...\"'-A 6...f\.A-SCt:-W\f le...s w~rt.. c-O\L::."L~ecl 0...+ 0&20. L e-ft >~ t:'-o..-r og;Zt), } '" 0 ' White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 o Date: 2/07 Revision: DUSA-I Page 5 ofS Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one~wood cr-;i) Westwater Canyon Other (describe) ___ _ DATE: q.l J 5,12D\\ pH BUFFER 7.0 _7J....Jt:-........ ()'---__ BY: 6c-r1""~ A-P~Lt\A.~ II::>(J (Sampler's initials) pH BUFFER 4.0 _y~{)~ __ _ SPECIFIC CONDUCTIVITY __ ql...-q...!-9-i--___ ~bl=::.M=H~O=s STEAM DEPTH: --PI Q""--\_':.~I-'-'l ....... \-' ___ _ pHofWATER ___ =Z~.~_5~ __________ _ COND umhos ;2. 3D .. 0 pH Units 7". 7 Y TempOC 12. 59 COND flmhos :2 2 {, n Y pH units 7£ 7' q TempOC '2 .... 60 Comments: TEMP q 0 t- • 1 COND Ilmhos :2"] 0 -' 7 pH units 7., &> I TempQC 12,59 COND flmhos 2. '$/ .. 5 pH units 7_ 21 Temp °C j :2 .-60 A .... r~vkA 0>0--),,' tk 0:.1:: 0 r 30. (~tj..,cr-;.A) 'rc....lI\.t'\, e.c :t 12.)lv,t6. P0:\ tA/\.e..J f~e..-SC'-A+ ~(Ar $c.....M.fL~~ c..V~At 9 6:. re.-Mt<le..r-::J l.JytL +p=K..e...A.. C<..V\.A .$4-V"\-p \(..$ W~\'--= ?-Q Lt f:-.~ td a tog> yo. L t,...(: +-S l t e.. CA.t bg 4.5 ... C-, 6 v J.. y s tl-~ e....> c... ~ t e.-VV\..f u-£?. + v r e.. LJC,-S q 0 C-.. White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2. J o Date: 2/07 Revision: DUSA-l Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one)&Ottonwood Cre~ Westwater Canyon Other (describe) ___ _ pH BUFFER 7.0 2 0 BY: 6ec..t-r---~v'\.... eAL~.A.e..r (Sampler' s initials) pH BUFFER 4.0 Lj" 0 SPECIFIC CONDUCTIVITY __ q...;..........:q~q..!--_____ u=M=H:.::..;O=s STEAM DEPTH: pH of WATER __________ _ TEMP ____________ _ • > COND ;:::.;"mh=o::::;..::s~ ___ _ COND~~mh~o~s~ ______ __ pH Units ______ _ pH units ______ _ Temp °c ______ _ Temp °C ______ _ COND~~mh==os~ ______ __ COND~=mh=o~s~ ______ __ pH units ______ _ pH units ______ _ Temp °c ______ _ TempoC __________ _ Comments: vA cr', vc:.-c! C2A (~t"C.... a...t (2iDo~ {?~rr-i"/\-:3 e:.yt\.~ P{-(..SeJLi.-c k 1 G C-\L... t......->tA.? eft-.I'-t, 6 V'-e..-p ~o +-CJ v./ ~ tC-..-lL-e-~ « L\""e.e.JL, k&"'(J\ CA.-.s~d ~UAt of: Svt-pw\ byt v'\Q L-J&--t-c.r +c;> SlA..M f 1 e..( White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-I Page 5 ofS Attachment A FIELD WATER ANALYSIS SURFACE WATER WI-IITE MESA MILL LOCATION (Circle one ):Cottonwood Creek~water Can0?V Other (describe ) ___ _ DATE: 12/2-3/2011 pH BUFFER 7.0 :2 a BY: 6a. CI'-l' 6 e I vV&- (Sampler's initials) pH BUFFER 4.0 l-l ~ C) SPECIFIC CONDUCTIVITY __ q,--Cf~'_q....&....--___ --,u~M-,=H=-O:.=s STEAM DEPTH: . pHofWATER ____________________ __ TEMP • ! COND z:::umh=o:=..:s~ ___ ~ CONDf.lmhos pH Units _____ _ pH units Temp °c ______ _ TempoC COND J.lmbo.:.:s~ ___ _ CONDJ.tmhos pH units ________ _ pH units Temp °C ______ _ TempoC Comments: A L i""'~ ve-tA. (2 A-5 ~ t L a..:r 0 75 t2 . by--il-~.A.-j g..yAv\' \2vyS ev"-t-9c.r ~e.At1 k.)tA-S h. kA.tA-.$~l\ f4-l-c:..-bw of >AC) l..s); bv t 0-{2 \....V(>\, t e:-r ±-o S t\..M fie-. -r vv c) fke to5 w e.r t!--i-~ t=-erA.. .. -r~~b ~o.5 White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manualt Section 2.1 Date: 2/07 Revision: DUSA-I i Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA Mn..L LOCATION (Circle one):Cottonwood Creek QYestwater C~Other (describe) ___ _ DATE: I ;;l .. 2-cr .. )..0 II pH BUFFER 7.0 =z 0 BY: ~C-lt; II'\. eo l Mer (Sampler's initials) pH BUFFER 4.0 _L,~l~." ~Q"----__ SPECIFIC CONDUCTIVITY ___ q:........q~q~ ___ ~u~MH~O~s STEAM DEPTH: ~--,()~_\l _____ _ pH of WATER _7~_7..!..-.-.3~ ___ _ TEMP ---.;.2~O~r-.::O=-~ -Y..J..- • I ----------------------------------------------------------- COND J!mhos I 2 .. q COND~=mili=o~s~ ______ __ pH Units __ ~ ___ _ pH units _______ _ Temp °c _______ _ COND Il=mh=os:::..-___ _ COND ~=mh=o.;;.;:s~ ___ _ pH units ______ _ pH units _______ _ Temp °c ________ _ Temp °C ______ _ Comments: alVC"'Ir:; G 1:1. Tn (,h+tX~D. fA.. ,o./CA".·bt.1 StAMPk, r JbCH/('..l,A ,$¥\ot-> £ro~ +"'-e.. Wc.-5 ·t-v./(l..-t",r ?i~t.. hd 11\. +0 L le...~A S &~lltJ.I\... bv(,....\::..(....-\-t. To f~A.Ol e.~v~k .sf"v()~ to t?;l\t-L--t.-bvcJt~t..s :c Wo...\~c..cA. 5b Y~reAs uf +--""-t..-('.,r~c..-~ wv....(...'!-+~t.->!I\.OI.-V" ~A. f\.-O+ 0Ae.-l-\--c.A.. wt...e,A,. t-k/L.. bvc..-t..c:..+s Wt:..re.. ~(.1\\ r t-oedC: ... ~ke..N bc...",~ .\-o t""-~ tlJ..V'A.:I/v~ J'+r{)\..t~~A ~u: lot~ ~ (.L..~ \I!...\-i-""-c..~ S~+ (}t/e-t'""I"\.,~.5.""t~ I'h.e.... ';2-;70-\1 -'A..N\.p\ .. '\.~ e,..vc!,/\,,+ t-oot:--Plc.-..c-~ CA-t-lL.i3 .. r () L l' • l, ..;...> • \ . \ e.1""'"V\..\tt t,.....,+ OY'\.e-.se...+-0-.,-y'o..r~!.r V..5 lA/(,t...> h'r-\VCAl l:J,A.. .$,+(.. Q4...+-C>7()o . .5I1'\.-OW l-~v... V'V'\.c:...t ·t-~ Ov .;..>" , ~4"". ,iA-L.re... t.Vc.J rov~J...... \1 3 Gc..-\ \0 AS 0 of l.o./"'--i e.r-\,1\.. l-\.....e.-bv,Jv'--:ts. v 5c..A 0.... p~r-D~ +c.. \ 1<-f(.!..v\f "f) 9n~(..t--rh..e. t..V'~-+e.r-~ R-e...>erV'Ql-.:t\v'e..5 \.t/(/t'e, ()..J..J.e.A .1 -.s"'.Mftt..J lA/e4'c:... fl~cc.l.;A... +-k~ ~"'iJ..~e.. - () EN:RGY www.energylab.com Mafyt!caIEXc8/hffl1:, SI1N:i11952 a~, ME B1il .. 4jr:Z"n'll' " ,j • 'Billings, Mr'SOO· 735 .. 4489 • Casper,WY 888 .. 235-0515 , $11888~6t2;'1225 • ' , TX 888-6QO-2218 L.ABORATORIES September 26,2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11090773 ANAL VTICAL SUMMARY REPORT Project Name: 3rd Quarter Surface Water Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 9/21/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11090773-001 Cottonwood 09/15/11 8:40 09/21/11 Aqueous Solids, Total Suspended C11090773-002 Westwater 09/15/11 8:20 09/21/11 Aqueous Same As Above C11090773-003 Temp Blank 09/15/11 0 :00 09/21/11 Aqueous Temperature The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as received basis unless otherwise indicated. If you have any questions regarding these test results, please call. Report Approved By: c5¥~D tJ~~ Reporting Supervisor Digitally signed by ";; Stephanie Waldrop Date: 2011.09.2623:21 :11 -06:00 Page 1 of 8 www.energylab.com Analytical fxcsllSIICI Sim:s 1952 .' --. . . .H_e~f1a,MfJll .. 47-2.;0111 • Billings, rKr BOO~ 135 .. 4489 • Casper, WY 888 .. 235-0515 . Gillette;'wY86&~;686.7175 ·.Ra id Ci ,·SD.88B-672-1225· College Station, IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Surface Water Report Date: 09/26/11 Sample Delivery Group: C11090773 CASE NARRATIVE LABORATORY COMMENTS TDS analysis inadvertently missed at login and was past hold time when noticed. Client notified of error on 9/23/11 and will submit new samples. Energy Laboratories apologizes for any inconvenience this may have caused. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 8 EN:RGY LA BORATORIES www.energylab.com Alialytital ExC81lsnl:tI Sincs '952 •. '., • Helena;' MT 817~41-2 .. 0711 -8Wings, MT 800-735-4489 • Casper, WY 888-235-D515 ".~_.~m!it;Wfii6~:.8~2711~ ·R~Jiid City,SD .888:-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Surface Water C11090773-001 Client Sample ID: Cottonwood Analyses PHYSICAL PROPERTIES Solids, Total Suspended TSS @ 105 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 8860 mg/l D -Rl increased due to sample matrix. Report Date: 09/26/11 Collection Date: 09/15/11 08:40 DateReceived: 09/21/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method AnalYSis Date / By D 100 A2540 D 09/21/11 09:58/ wc MCl -Maximum contaminant level. ND -Not detected at the reporting limit. . Page 3 of 8 EN:RGY LABORATORIES www.energylab.com AIlalyticalExcillllHlcB Sines 1952 ,<:, '. ::O,~leM;Mf'~17~4t2-1i711 • Billings,MrBOO~735 .. 44~9 • Casper,WY 888-23~-0515 WJIpif¢~:~1i:~·Q$6~711~ • Rapid City, SO 80':-672-1225 • ColiegeStation, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Surface Water C11090773-002 Client Sample 10: Westwater Analyses PHYSICAL PROPERTIES Solids, Total Suspended TSS @ 105 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 748 mg/l D -Rl increased due to sample matrix. Report Date: 09/26/11 Collection Date: 09/15/11 08:20 DateReceived: 09/21/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By D 20 A2540 D 09/21/11 10:26/ wc MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 8 EN:RGY LABORATORIES www.energylab.com AnB/ytical ExcBIlsnt:, Sincs .1952 " ....... >~~~~".~JJU,en-472-D711 -Sillings, Mt 800-735-4489 • Casper, WY 888-235-0515 TI.~~~/W:j(6.~,'Bl':7H~~ Rapip City, SOB88~6t2-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Surface Water C11090773-003 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.2 Qualifier Rl Report Date: 09/26/11 Collection Date: 09/15/11 DateReceived: 09/21/11 Matrix: Aqueous MCL! QCl Method Analysis Date / By E170.1 09/21/11 09:251 kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 5 of 8 E~RGY LABORATORIES www.energylab.com An_I ExcsllBf1C1 Sines 1952 " ,~> .: .. ~H~ieit~,J,rr: a7l-4t27D7-1 t • Billings, MT BOO-735-4489 • Casper, WY 888-235-0515 "~~I~ija.~.~Yi6f'8~"71t~ • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Surface Water Analyte Count Result Units Method: A2540 D Sample ID: MBLK1_ Solids, Total Suspended TSS @ 105 C Method Blank ND mg/L Sample ID: LCS1_ Laboratory Control Sample Solids, Total Suspended TSS @ 105 C 191 mg/L Sample ID: C11090773-001ADUP Sample Duplicate Solids, Total Suspended TSS @ 105 C 9140 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 09/26/11 Work Order: C11090773 RL %REC Low Limit High Limit Run: BAL-1_11 0921 A 2 Run: BAL-1_110921A 6.0 95 60 110 Run:BAL-1110921A 120 ND -Not detected at the reporting limit. RPD RPDLimit Qual 3.1 Batch: R150891 09/21/1 1 09:56 09/21/11 09:57 09/21/11 10:06 5 Page 6 of 8 . EI\ERGY LABORATORIES .~1~ www.energylab.com. t~ Anatytieal ExcslllHWfJ SltlCB 1952 ".:: ~. '~H~f~o,~;,'Mt8n -412-,0711 •. Biliings,MT 800-735-4489 • Casper, VIY 888-235-0515 i~.v ~!~~~i ~l6,Q~JB6-717~. RapidCitY, SO 88B.;&72-1225 • College Station, IX 888-6~O-2218 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C11090773 Login completed by: Debra Williams Reviewed by: BL2000\kschroeder Reviewed Date: 9/26/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 2.2'C On Ice Yes 0 Yes 0' Date Received: 9/21/2011 Received by: dw Carrier NDA name: No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0' No VOA vials submitted 0' Not Applicable 0 Page 7 of 8 EI\ERGY aD" Chain of Custody and Analytical Request Record page __ ( ofL Company Name: ~ ~ M, ".--. /eNJ ~~ (I ( IN€:S_ Report M~iI AddrjSs: ~ t1 /J' ,0 '~~X-()() 7 ,'t/"nitl1ti IAI K'IS II Invoice Adares~ 0~~ Special ReporUFormats: Dow o EDO/EDT(Electronic Data) o POTWNVWTP Format: ____ _ o State: D LEVEL IV o Other: ----o NELAC ---- SAMPLE IDENTIFICATION (~ame, Location, Interval, etc.) TILwcnJ 2 /,Jj &..Th i"A kg 3Tp~eIG~ 4 I-----V 5 6 7 8 9 10 Collection Date Collection Time 1JS·JL __ I~qO l~llS:l( lL2~o Lh PLEASE PRINT (Provide as much information aS~Qssible.] proid a2j PWS, Permit, .. E. te., Sample 0 .. r .... i.9in c '5 lAM.-riA SiL~ ltJ£k Slate: _fA. r EPA/State Compliance: Yes ~ No 0 jz:e:JlkcL Phon;~ ezZ/ Email Sampler: (Please Print) rZa" IikL Invoi~ Contact & Phone: I Purchase Order: Quite/Bottle Order: ~~ ~ o ..... Vlo Q) lo. VJ..t:: ~co~OI Qj ._> 0 >. ...... B",..oo ~ ~ C""w VJ > 0>= ~ C1l u>oo c _<001·-32 o >-all c '-<J.).£!:l c: . .::: ~~I~o Er-> ~ t ::sQ).~a3~ zCi.<Claro ~ >1 en MATRIX /::~ l-vJ ~&~ W®D@ OOrn@C!D~1f'rn[Q) Cl ~ W ~ I ........ () -g « ::s .... ~ ~ ~ I- ~ I I I I I I I~ j Received by (print): • Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page R u Comments: 5 H J(JJo 1t:1 J /hIf,g: Jib Ivl -r; M~ Shl1J'S-IV~ Cooler 10(s): C-{i~ Re:;::I 0c On Ice: f]2N Custody Seal On Bottla ~ N On Cooler N Intact N Signature ~ N Match U ~ I~ ~ I I'"=' ~ [l!I£. CO) ~ I~ (6i 1ll0Ct07Z; I~' r' Datemme: Signature: ~ Custody ~ FI~c()rcl ~~~~~~~~~~~~~~~~~~~L---~~~~~-------------+rR~e~ce~iv~e7d~by~(~p7.rin~t)~:----------~D~a~te~mr.l=m~e:~---------------'S~ig=n=at~u=re~:--------------~ a MUSTb~r--4~------------------------____ ~~~~==~~~~~ ________ ~~ ______ ~ co Signecl Return to Client: Lab Disposal: r In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted t er certified laboratories in order to complete the analysis requested, This serves as notice of this possibility. All sub-contract data will be rly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ---00' """.nergylab.tllm : ~~ Analytical Excellence Sines '952 EN:RGY LABORATORIES r Helena, MT 877-472-0711 .. Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 ANALYTICAL SUMMARY REPORT February 02,2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12010049 Project Name: 4th Quarter Surface Water Semi-Annual 2011 Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 1/4/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12010049-001 Westwater 12/29/11 14:30 01/04/12 Aqueous C12010049-002 Temp Blank 12/29/11 0:00 01/04/12 Aqueous Sample Filtering Uranium, Dissolved Uranium, Suspended Digestion, Total Metals Gross Alpha minus Rn222 and Uranium Radium 226, Dissolved Radium 226, Suspended Thorium, Isotopic Thorium, Suspended Isotopic Solids, Total Dissolved Solids, Total Suspended Temperature The analyses presented in this report were performed at Energy Laborafories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: c3¥~ D uJCA1~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.02.02 12:04:48 -07:00 Page 1 of 12 ~.---------'-----.. ---.-------- www.energylab.com Analytical Exesllenes Sines '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 ., Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Ra id Ci ,SD 888-672-1225 • Colle e Station, IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 4th Quarter Surface Water Semi-Annual 2011 Report Date: 02/02/12 Sample Delivery Group: C12010049 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EN:RGY LABORATORIES www.energylab.com Analytical Excsllence Sines '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 -Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-672-1225 • College Station, rx888-690-22t8 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: LablD: 4th Quarter Surface Water Semi-Annual 2011 C 120 10049-001 Client Sample ID: Westwater Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Solids, Total Suspended TSS @ 105 C METALS -DISSOLVED Uranium METALS-SUSPENDED Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC RADIONUCLIDES -SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 16 mg/L ND mg/L ND mg/L 0.0014 mg/L 0.1 pCi/L 0.2 pCi/L 0.4 pCi/L -0.006 pCi/L 0.09 pC ilL 0.17 pCi/L 0.09 pC ilL 0.1 pCi/L 0.2 pC ilL 0.30 pCi/L 0.15 pC ilL 0.17 pCi/L 0.7 pC ilL 0.4 pC ilL 0.4 pCi/L MDC -Minimum detectable concentration Report Date: 02/02/12 Collection Date: 12/29/11 14:30 DateReceived: 01/04/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By 10 A2540 C 01/04/12 13:151 wc 4 A2540 D 01/05/1209:12/1r 0.0003 E200.8 01/05/1220:271 sml 0.0003 E200.8 01/13/1216:091 sml U E900.1 01/31/1214:571 plj E900.1 01/31/1214:571 plj E900.1 01/31/1214:571 plj U E903.0 01/23/1214:41 /Ibb E903.0 01/23/1214:41 Ilbb E903.0 01/23/1214:41 Ilbb U E908.0 01/12/1209:231 dmf E908.0 01/12/1209:231 dmf E908.0 01/12/1209:231 dmf E903.0 01/19/1200:551 trs E903.0 01/19/12 00:55 I trs E903.0 01119/12 00:551 trs E908.0 01/17/1208:471 dmf E908.0 01/17/1208:471 dmf E908.0 01/17/1208:471 dmf MCL -Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 3 of 12 EI\.ERGY LABORATORIES www.energylab.com f Analytical ExcsllBnCB Sincs '952 Helena, MT 877-472-0711 tI Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 4th Quarter Surface Water Semi-Annual 2011 C 1201 0049-002 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.6 Qualifier Rl Report Date: 02/02/12 Collection Date: 12/29/11 DateReceived: 01/04/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By E170.1 01/04/1209:201 kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 12 -'-'--r;m' E~RGY· LABORATORIES www.energylab.com Analytical ExesllsnclI Sincs 19S2 r Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp ' Project: 4th Quarter Surface Water Semi-Annual 2011 Analyte Count Result Method: A2540 C Sample 10: MBLK1_120104 Solids, Total Dissolved TDS @ 180 C Method Blank ND Units mg/L Sample 10: LCS1_120104 Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1650 mg/L Sample 10: C12010056-001AMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 2550 mg/L Sample 10: C11120864-002AOUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 679 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 02/02/12 Work Order: C12010049 RL %REC Low Limit High Limit Run: BAL-1_120104A 10 Run: BAL-C120104A 10 99 90 110 Run: BAL-1 120104A 10 101 90 110 Run: BAL-1 120104A 10 ND -Not detected at the reporting limit. RPO RPOLimit Qual Batch: 120104_1_SLDS-TDS-W 01/04/1213:14 01/04/1213:14 01/04/1213:15 01/04/1216:09 0.8 5 Page 5 of 12 www.energylab.com Analytical Exes/Jence Si11I:e 7952 r----_.-Helena, MT 877-472-0111 " Billings, MT 800-735-4489 " Gasper, WY 888-235-0515 Gillette, WY 86&-&86-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Surface Water Semi-Annual 2011 Analyte Count Result Method: A2540 D Sample ID: MBLK1_120105 Solids, Total Suspended TSS @ 105 C Method Blank ND Units mg/L Sample ID: LCS1_120105 Laboratory Control Sample Solids, Total Suspended TSS @ 105 C 189 mg/L Sample ID: C12010045-004BDUP Sample Duplicate Solids, Total Suspended TSS @ 105 C 136 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 02/02/12 Work Order: C12010049 RL %REC Low Limit High Limit Run: BAL-1_120105A 4.0 Run: BAL-1_120105A 6.0 95 60 110 Run: BAL-1 120105A 12 ND -Not detected at the reporting limit. RPD RPDLimit Qual Batch: 1201 05_1_SLDS-TDS-W 01/05/1209:09 3.0 01/05/1209:09 01/05/12 09:11 5 Page 6 of 12 I l I I ---.. ----tei· W\WI,energyl.~"m r-----Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-051 5 ""'~ Ana/yticBIExcsIJ8IIc,Sincs 7952 ) Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 EI'\E'RGY LABORATORIES ==~----------------~--------~------------~--~------------~----~-------- QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Surface Water Semi-Annual 2011 Report Date: 02/02/12 Work Order: C12010049 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.8 Sample 10: ICV Uranium Method: E200.8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: C12010073-001AMS Uranium Sample 10: C12010073-001AMSO Uranium Method: E200.8 Sample 10: ICV Uranium Method: E200.8 Sample 10: MB-32412 Uranium Sample 10: LCS2-32412 Uranium Sample 10: C12010200-007AMS Uranium Sample 10: C12010200-007AMSO Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0478 mg/L 0.00030 96 Method Blank NO mg/L 0.00030 Laboratory Fortified Blank 0.0493 mg/L 0.00030 90 Sample Matrix Spike 0.0497 mg/L 0.0010 99 Sample Matrix Spike Duplicate 0.0507 mg/L 0.0010 101 Initial Calibration Verification Standard 0.0508 mg/L 0.00030 102 Method Blank NO mg/L 0.00030 Laboratory Control Sample 0.104 mg/L 0.00030 104 Sample Matrix Spike 0.0528 pCilFilter 0.00030 106 Sample Matrix Spike Duplicate 0.0571 pCi/Filter 0.00030 114 Analytical Run: ICPMS2-C_120105B 01/05/1218:32 90 110 Run: ICPMS2-C_1201 05B Run: ICPMS2-C_120105B 85 115 Run: ICPMS2-C 120105B - 70 130 Run: ICPMS2-C_120105B 70 130 1.9 Batch: R155074 01/05/12 18:41 01/05/12 18:45 01/05/1220:34 01/05/1220:36 20 Analytical Run: ICPMS2-C_120113A 01/13/1215:21 90 110 Run: ICPMS2-C_120113A Run: ICPMS2-C_120113A 85 115 Run: ICPMS2-C_120113A 70 130 Run: ICPMS2-C_120113A 70 130 7.8 Batch: 32412 01/13/12 16:04 01/13/1216:06 01/13/1216:47 01/13/1216:49 20 NO -Not detected at the reporting limit. Page 7 of 12 ------==== :.~J'" www.energylab.comHeleM.MT877-472-0711 ·Billings.MT 800-735-4489 • Gasper, WY 888-235-0515 .... ~~ Analytical Excel/snell Since 1952 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-&90-2218 EI\ERGY LABORATORIES ~~~~~--~~--------------------~---------- QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Surface Water Semi-Annual 2011 Report Date: 02/02/12 Work Order: C12010049 Analyte Count Result Units Method: E900.1 Sample 10: MB-GA-0500 Gross Alpha minus Rn & U 3 Method Blank Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Sample 10: LCS-GA-0500 Gross Alpha minus Rn & U 0.116 pC ilL 0.239 0.379 pCi/L pC ilL Laboratory Control Sample 27.4 pC ilL RL %REC Low Limit High Limit Run: G542M_120123A Run: G542M_120123A 131 70 130 -LCS response is outside of the acceptance range for this analysis. Since the MS, MS, and MSD are acceptable the batch is approved. Sample 10: C12010151-001GMS Sample Matrix Spike Run: G542M_120123A Gross Alpha minus Rn & U 44.2 pCilL 104 70 130 Sample 10: C12010151-001GMSO Sample Matrix Spike Duplicate Run: G542M_120123A Gross Alpha minus Rn & U 43.8 pCilL 104 70 130 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of adviso.ry limits. U -Not detected at minimum detectable concentration RPO RPOLimit Qual Batch: GA-0500 01/31/1214:57 U 01/31/12 14:57 S 01/31/1216:50 01/31/1216:50 0.9 22.8 Page 8 of 12 E~RGY LABORATORIES www.energylab.com Analytical Exes/lenc. SirJcg '952 r Helena, MT 877-472-0711 • Billings, MT 800-735-4489 11 Casper, WY 888-235-0515 Gillette, WY 866-686-7175 . Rapid City, SO 888-672-1225 It College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Surface Water Semi-Annual 2011 Analyte Count Result Units Method: E903.0 Sample 10: C11120834-004AMS Radium 226 Sample 10: C11120834-004AMSO Radium 226 Sample 10: LCS-32369 Radium 226 Sample Matrix Spike 5.13E-07 pCi/Filter Sample Matrix Spike Duplicate 5.11 E-07 pCi/Filter Laboratory Control Sample 13.0 pCi/Filter Sample 10: MB-32369 Radium 226 3 Method Blank Radium 226 precision (±) Radium 226 MDC Method: E903.0 Sample 10: MB-RA226-5791 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-RA226-5791 Radium 226 Sample 10: C12010392-0020MS Radium 226 Sample 10: C12010392-0020MSO Radium 226 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration -0.0594 pCi/Filter 0.150 pCi/Filter 0.299 pCi/Filter Method Blank -0.11 pC ilL 0.075 pC ilL 0.19 pC ilL Laboratory Control Sample 5.8 pCi/L Sample Matrix Spike 14 pC ilL Sample Matrix Spike Duplicate 15 pC ilL Report Date: 02/02/12 Work Order: C12010049 RL %REC Low Limit High Limit RPO RPOLimit Qual 116 116 110 94 116 119 Batch: R155484 Run: BERTHOLD 770-1_120112A 01/18/1223:14 70 130 Run: BERTHOLD 770-1 120112A 01/18/1223:14 70 130 0.3 25.3 Run: BERTHOLD 770-1 120112A 01/19/12 00:55 70 130 Run: BERTHOLD 770-1 120112A 01/19/12 00:55 U Batch: RA226-5791 Run: BERTHOLD 770-2_120117A01/23/12 14:41 U Run: BERTHOLD 770-2_120117A 01/23/12 14:41 80 120 Run:BERTHOLD770~ 120117A 01/23/1214:41 - 70 130 Run: BERTHOLD 770-2 120117A 01/23/1214:41 - 70 130 1.5 27.2 ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 9 of 12 .---------' ---, ,----,-----,-------www.energylab.com ( Analytical Excsllenctl Since 1952 J Helena, MT 871-472-0711 • Billings, MT 800-735-4489 " Gasper, WY 888-235-0515 Gillette, WY 866-686-7175 ... Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Surface Water Semi-Annual 2011 Analyte Count Result Units Method: E908.0 Sample 10: LCS-RA-TH-ISO-1S46 Thorium 230 Sample 10: C11120731-0010MS Thorium 230 Sample 10: C11120731-0010MSO Thorium 230 Laboratory Control Sample 6.12 pCi/L Sample Matrix Spike 11 pCi/L Sample Matrix Spike Duplicate 9.4 pC ilL Sample 10: MB-RA-TH-ISO-1S46 3 Method Blank Thorium 230 -0.0231 pCi/L Thorium 230 precision (±) Thorium 230 MDC Method: E908.0 Sample 10: C12010049-0010MS Thorium 230 Sample 10: C12010049-0010MSO Thorium 230 Sample 10: LCS-32412 Thorium 230 Sample 10: MB-32412 Thorium 230 Thorium 230 precision (±) ThoriUm 230 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration 0.0675 pCi/L 0.214 pCi/L Sample Matrix Spike 34 pCilL Sample Matrix Spike Duplicate 40 pCi/L Laboratory Control Sample 11.3 pCi/Filter Method Blank 0.157 pCilFilter 0.127 pCi/Filter 0.198 pCi/Filter Report Date: 02/02/12 Work Order: C12010049 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: RA-TH-ISO-1546 Run: ALPHANALYST_12011 OA 108 70 130 Run: ALPHANAL YST _12011 OA 100 70 130 Run: ALPHANALYST_12011 OA 85 70 130 17 Run: ALPHANALYST_12011 OA Run: EGG-ORTEC_120112A 104 70 130 Run: EGG-ORTEC_120112A 121 70 130 15 Run: EGG-ORTEC_120112A 115 70 130 Run: EGG-ORTEC_120112A NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration 01/12/1209:23 01/12/1209:23 01/12/1209:24 39.4 01/12/12 09:24 U Batch: 32412 01/17/1208:47 01/17/12 08:47 44.5 01/16/1215:52 01/16/1215:52 U Page 10 of 12 E,~RGY LABORATORIES www.energyJab.com f Analytical ExcsIIBflCB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 1111111111111111111111111111111111111111111111111111111 C12010049 Login completed by: Kristy Gisse Reviewed by: BL2000\kschroeder Reviewed Date: 1/4/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0' Yes 0' Yes D Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 2.6'C On Ice Yes D Yes 0' Date Received: 1/4/2012 Received by: kg No D No D No D No D No D No D No D No D No D No D No D No D Carrier UPS-NDA name: Not Present D Not Present D Not Present 0' No VOA vials submitted 0' Not Applicable D Sample filtered, and preserved as necessary for dissolved and suspended analysis. Page 11 of 12 ""U ru (C ,CD I--lo. I~ --... --lo. I\.) fll7Brl~ Mt4!!M,nm . . ---_ ....... , ... _,... __ . ..,. ....... __ ....... _ •••• -."'.,.,.. •• ,.. .... ~v __ ...... _., Company Name: Project Name, PWS, Permit, Etc. .$iU"'\.; AM.c.I' ..... ~O,' Sample Origin EPNState Compliance: D&tItw'1.:6.A .AI\._~IA.4!. . <-'-(ttA-o JJ c..r +' e,r S ur' ~1J...t,.~ (,)~+U'" State: V T' Yes ~ No 0 Report Mail Address: p. O. gox 8"Q Contact Name: Phone/Fax: Email: Sampler: (Please Print) I3I~ol'~ vT g4.fSll 6-.r'" "'-p~\~ "",~S "67r .. ~ ~~l 6. __ ~t'--;~ P .... \~ Invoice Address: -Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: .stA.~t!->dtr~ Special Report/Formats: ~11 W@D@ 1M@:@on~~[Q) .-Contact ELI prior to Shipped by: 3: Lf. f5,./Y' f) .4 0 "-RUSH sample submittal ~OCl)~ 11 ,~ for charges and Cooler ID{s): 2:!m;gOI (u ~ ~~ ~ 0 ~ R scheduUng -See L l f'11 f ._> 0 >-16 o OW D EDD/EDT(Electronic Data) ~CI)~~S ~ ~ W I nstruction Page 03:= ~ 0> ~ ..: ~ :c "C Re~tT2: 0C D POlWIWWTP Format: u 001:: 4 <..) c: Comments: '0 «CI)I'-I:s2 '" ~ :::J U D State: D LEVEL IV •. Q)~.5 ~ ~ « E? L.. Q)_ "---1 I-ro ~~rgo c: D Other: 0 NELAC ~ ....... :; On Ice: (v)N E~ ('G I ...... « ::l Q).!::: Q:) 3: ..., l-S zo..«l~o () ~V'I ~ .. ,'j .~ W -0 Custody Seal Y([) L.. ~ >1 -1 W co On Bottle \1'1 -1 "'1i C/) "'0 ~N C/} ~ ~ .c: On Cooler l-l-~ ....... ..... ~ H Intact d)N ~ i" ~ CI) SAMPLE IDENTIFICATION Collection Collection MATRIX ~ l ) ~ Signature CDN (Name, Location, Interval, etc.) Date Time '\I ~ ~ Match 1 LJ "-5 r l..J ~--tt..-r 12. .. ~q, " I~>O 1-tJ i-)C ;< 1.< J< ~ ~ 2 TCrY\{J I3I~v'/< i~ 3 <Q) Rnn 4 ~ 5 lo...;;::'l ~ 6 ~. 7 ~ClgO loof1 8 ~ j 9 I~ 1 10 1r::Jl Custody Relinquished by (print): DateJTima: Signature: p~ Received by (print): Datamme: Signature: (,...,..~~ P ... I.AA~'-,. 3--::l()I~ /, ..... -... Record Relinquished by (print): Datemme: Signature: Received by (print): DatelTime: Signature: MUST be Signed KGCelvea Dy L.8DOrawry: uateJ lime: cl~pG ;<;gnatz: Sample Disposal: Return to Client: Lab Disposal: /·'1·1, r/J .' .) 5< In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub·contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC 0 I\) ~ 0 c.n c.n I\) c.n w c..n Jul-98 Oct-98 Jan-99 Apr-99 Jul-99 Oct-99 Jan-OO Apr-OO Jul-OO Oct-OO Jan-01 Apr-01 Jul-01 Oct-01 Jan-02 Apr-02 :c t Jul-02 m c. OJ Oct-02 c: I Jan-03 3 "f= I Apr-03 I\) ...... I\) Jul-03 0) + Oct-03 0 Jan-04 0 OJ :::J I Apr-04 0 < CD r\:, Jul-04 :::J .... Oct-04 .., m + Jan-OS ~ Apr-OS 0 :::J OJ Jul-OS tJ) I < Oct-OS :::J W Jan-06 en t Apr-06 2. Jul-06 ...-. "'C OJ I Oct-06 0 < Jan-07 ;S ~ -Apr-07 + Jul-07 Oct-07 OJ Jan-08 I < Apr-08 0, Jul-08 + Oct-08 Jan-09 OJ Apr-09 I "f= Jul-09 0) Oct-09 Jan-10 Apr-10 Jul-10 Oct-10 Jan-11 Apr-11 Jul-11 t OJ I ~ ...... + OJ I < r\:> + OJ I < W t OJ I < ~ + OJ I < ell + OJ I < m Jul-9S Oct-9S Jan-99 Apr-99 Jul-99 Oct-99 Jan-OO Apr-OO Jul-OO Oct-OO Jan-01 Apr-01 Jul-01 Oct-01 Jan-02 Apr-02 Jul-02 Oct-02 Jan-03 Apr-03 Jul-03 Oct-03 Jan-04 Apr-04 Jul-04 Oct-04 Jan-05 Apr-05 Jul-05 Oct-05 Jan-06 Apr-06 Jul-06 Oct-06 Jan-07 Apr-07 Jul-07 Oct-07 Jan-OS Apr-OS Jul-OS Oct-OS Jan-09 Apr-09 Jul-09 Oct-09 Jan-10 Apr-10 Jul-10 Oct-10 Jan-11 Apr-11 Jul-11 o o c.n c.n I\) I\) (J'1 c.v c.v (J'1 ~ ~ (J'1 c: ""'Ii Q) ::::J s:: 3 I Z Q) =-+ o o ::::J (') CD ::::J ... ""'Ii Q) ... o· ::::J (J) ::::J CJ) o -"'C o ~ - BHV-1 Date Ra-V-Nat 226 9/7/80 0.650 0.420 9/8/81 0.400 1.800 12/3/81 0.790 0.770 6/30/82 0.423 0.384 5/5/83 0.471 0.410 6/4/84 0.713 0.866 10/12/8 2.960 0.886 4 8/28/85 1.630 0.800 8/1/86 0.369 0.654 8/17/87 0.600 0.800 8/28/88 1.500 1.600 8/25/88 1.200 1.600 8/1/90 2.900 5.800 8/5/91 3.900 8.800 8/13/92 1.200 2.200 8/13/93 2.000 1.700 8/3/94 1.000 1.600 8/28/95 2.810 4.700 8/13/96 1.700 2.150 8/1/97 0.540 0.310 7/1/98 1.600 3.050 8/24/99 2.270 1.740 12/1/00 1.510 1.210 8/23/01 1.000 1.000 8/1/02 1.300 1.350 8/5/03 0.800 0.990 8/9/04 0.600 0.610 8/3/05 0.900 0.960 8/7/06 0.700 0.760 8/8/07 1.100 2.370 8/20/08 0.900 1.230 8/10/09 0.800 0.880 8/2/10 1.3 1.09 8/23/11 0.9 1.32 *Data not avatlable. WHITE MESA MILL Soil Sampling Results (VALUES) x 10-3 uCi/kg BHV-2 BHV-3 BHV-4 Ra-V-Nat Ra-V-Nat Ra-V-Nat 226 226 226 0.340 0.420 0.420 0.420 0.410 12.194 0.300 · 0.600 0.300 0.600 0.200 3.000 0.440 0.560 0.890 0.420 0.750 0.630 0.412 0.180 0.265 0.207 0.478 0.260 0.569 0.550 0.461 0.340 0.643 0.340 0.618 0.683 0.489 0.471 0.124 0.324 2.330 0.069 2.880 0.721 3.490 0.804 2.190 0.424 2.270 0.424 4.330 0.294 0.466 0.866 0.382 0.694 0.396 0.826 1.500 0.900 0.800 0.600 1.200 0.700 1.300 0.700 0.600 0.900 1.000 1.300 1.100 3.000 0.800 1.000 1.100 1.400 1.000 1.400 0.800 1.400 1.800 1.300 1.700 2.600 2.600 5.700 1.800 2.600 0.900 1.400 0.800 1.200 0.900 0.900 1.400 1.700 1.100 1.900 0.800 1.600 0.700 0.800 0.700 0.900 0.700 1.100 0.680 0.200 0.880 0.650 0.580 0.240 0.600 0.460 0.300 0.210 0.500 0.520 0.560 0.160 0.410 0.270 0.410 0.260 0.700 0.580 0.500 0.450 1.000 1.190 0.780 0.840 0.530 0.420 0.840 0.770 0.810 0.530 * * 0.830 1.220 0.600 0.300 0.400 0.300 0.900 1.000 0.900 0.524 0.500 0.297 1.200 1.490 0.600 0.790 0.500 0.330 0.600 0.4300 0.400 0.250 0.400 0.220 0.600 0.5100 0.700 0.340 0.600 0.270 0.600 0.3800 0.440 0.250 0.410 0.250 0.520 0.480 0.700 0.530 0.200 0.550 0.500 0.740 0.300 0.430 0.600 0.980 0.500 0.790 0.700 0.540 0.700 1.080 0.800 0.610 1.0 1.49 0.8 0.62 1.3 1.69 0.4 0.32 0.4 0.4 0.5 0.58 BHV-5 BHV-6 Ra-V-Nat Ra-V-Nat 226 226 0.230 14.89 1 -- 0.300 0.600 -- 0.550 0.420 -- 0.449 0.216 -- 0.147 0.140 -- 0.132 0.310 -- 2.550 0.817 -- 1.280 0.577 -- 0.728 0.836 -- 1.500 1.300 -- 3.800 5.000 -- 2.900 5.700 -- 3.700 3.200 -- 2.500 4.400 -- 1.100 1.800 -- 4.800 3.500 -- 3.000 3.800 -- 2.800 1.600 -- 1.900 2.010 -- 1.700 1.500 -- 3.000 2.760 -- 3.270 3.150 -- : 2.810 3.250 -- 1.200 1.100 -- 2.400 2.810 60.00 0.550 0.280 0.420 0.600 0.530 1.000 1.400 0.900 1.400 0.700 0.410 1.000 1.200 1.400 1.300 0.780 0.650 1.100 1.450 0.800 0.930 0.800 1.330 0.500 0.670 2.600 2.980 0.500 0.810 1.7 1.69 0.8 0.87 1.0 1.48 0.6 0.86 EN:RGY LABORATORIES www.energylab.com lnsIytiCal Ei'cs/lsnci Sines 1952 <'<'":HeIe'l~Jdf~'il~4t~:D!1 t .BUHngsfM.l"80~-7~5w4489 • Casper,WY 888 .. 235-8515 ~tte,·WY.I,j~,(86::Y;t15 .R,@Pi~,Gi~i .SO.8e8-'t2-12~5 . Colleg~Stat~on, IX 888-690-2218 ANAL VTICAL SUMMARY REPORT October 13, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11 081 063 Project Name: Annual Soils 2011 Energy Laboratories, Inc. Casper WY received the following 7 samples for Denison Mines USA Corp on 8/26/2011 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test . C11 081 063-001 BHV-1 08/23/11 8:33 08/26/11 Soil Uranium, Total Digestion For RadioChemistry Radium 226 C 11 081 063-002 BHV-2 08/23/11 8:45 08/26/11 Soil Same As Above C11 081 063-003 Black Mesa 08/23/11 9:03 08/26/11 Soil Same As Above C 11 081 063-004 BHV-4 08/23/11 9:40 08/26/11 Soil Same As Above C 11081063-005 BHV-5 08/23/11 9:55 08/26/11 Soil Same As Above C11 081 063-006 BHV-6 08/23/11 9:50 08/26/11 Soil Same As Above C11 081063-007 Westwater 08/23/11 9:29 08/26/11 Soil Same As Above The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analyt}cal Report, the QNQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as received basis unless otherwise indicated. If you have any questions regarding these test results, please call. Report Approved By: c5¥~D uJal~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.10.13 10:59:56 -06:00 Page 1 of 13 wWw.~nergylab.c~m mtytiCal bt:sllsncBS;iJcs 1952 CLIENT: Denison Mines USA Corp Project: Annual Soils 2011 Report Date: 10/13/11 Sample Delivery Group: C11 081 063 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 13 EI\ERGY LABORATORIES www.eliergylab.com hllytical ExcsllBnc; SineS '.952 ;,:<' . }f.ele.na, Mr::8i1~4j~~1i711 .·BUling~;.Mr800-135w4489 • Casper, WY 888 .. 235-0515 J~i!;&j~~\~'.8·6-1jl~~R,~·Piq,¢ity, SD.8QB:-672-1225 . C~lIege,Station, 'rX888-690:-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp Annual Soils 2011 Lab 10: C11 081 063-001 Client Sample 10: BHV-1 Analyses METALS -TOTAL Uranium RADIONUCLIDES .. TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.32 0.9 0.06 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier Rl 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 08:33 DateReceived: 08/26/11 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/06/11 16:361 sml E903.0 09/21/11 17:131 js E903.0 09121/11 17:131 js E903.0 09121/11 17:131 js MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 13 EN:RGY LABORATORIES www.energylab.com Ans/ytiliaiExcBIlsnUSincs 1952 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Annual Soils 2011 Lab ID: C11 081 063-002 Client Sample ID: BHV-2 Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.32 0.4 0.04 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier Rl 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 08:45 DateReceived: 08/26/11 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/06/11 16:421 sml E903.0 09/21/11 17:13/ js E903.0 09121/11 17:131 js E903.0 09121/11 17:131 js MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 13 EN:RGY LABORATORIES wWw.energylab.cf)n1 Anafytical uesllBnc; Sioo,,952 ". , HJ;lel1;a~'Ml)t7"412-:P711 . Billings, ~ 800·735-44~9 • Casper, WY 888-235-0515 " Gii~)'e, wy ~8U:J86-jj 1~ • RapId Gity, SD 888-672-1225 • CQllege,Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp Annual Soils 2011 Lab 10: C11 081 063-003 Client Sample 10: Black Mesa Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.40 0.4 0.05 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier Rl 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 09:03 DateReceived: 08/26/11 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/06/11 16:451 sml E903.0 09121/11 17:131 js E903.0 09121/11 17:131 js E903.0 09121/11 17:131 js MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 13 Ef\ERGY L.ABORATORIES wWw.energylati.com MaIytitBIExcsnsnc; Sines 1952 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Annual Soils 2011 Lab 10: C11 081 063-004 Client Sample 10: BHV-4 Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.58 0.5 0.05 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier Rl 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 09:40 DateReceived: 08/26/11 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/06/11 16:48 1 sml E903.0 09121/11 17:131 js E903.0 09121/11 17:131 js E903.0 09/21/1117:13/js MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 13 EN:RGY LI\BORATORI ES www.~nergylab.coin AnBlytiCalEXUllBi1c1l Sine.,952 ~£~lt1·1~4.1:~~07.11·.·B:lrIi~ngs,MT8.00.735~44~9 • Casper,Vf{ 8~8-235·~5l5 ,<~~o{t'~~tjl1 ~·~~.~PiPJ!ityi~·~~8Q~~'7)~.12~5 . College,St~tipn, lX 88.-690-221 e LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Annual Soils 2011 Lab ID: C11 081 063-005 Client Sample ID: BHV-5 Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Rapium 226 precision (±) Radium 226 MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 1.48 1.0 0.07 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier RL 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 09:55 DateReceived: 08/26/11 Matrix: Soil MCL! QCL Method Analysis Date / By SW6020 09/06/11 16:51 1 sml E903.0 09/21/11 17:131 js E903.0 09/21/1117:13/js E903.0 09/21/11 17:13/ js MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 13 EI\ERGY LABORATORIES wwW:energylab.~om M8lyticaiEXc;liBfIcS SinCs 1952 .' ,·~!!lel~~cr,:~~!1'lt4t2~O'l11 . 'Bliling~, Mr 800~735w44B9 • Casper,\vy 88~ .. 2.35·0~1' ;.ID')@';llg~li?~~ ·R~piqGity,S~,888:-672~1225 . CollegeStat!on, IX 88.-690-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp Annual Soils 2011 Lab ID: C11 081 063-006 Client Sample ID: BHV-6 Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.86 0.6 0.05 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier Rl 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 09:50 DateReceived: 08/26/11 Matrix: Soil MCL! QCl Method Analysis Date / By SW6020 09/06/11 16:541 sml E903.0 09/21/11 17:131 js E903.0 09/21/1117:13/js E903.0 09/21/11 17:131 js MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 13 EN:RGY, LABORATORIES www.energylab.com AnalytiCal ExC8llsiicil Sii1CBIS52 1 .• 'BUlings,Ml B~O-7.35-44$9 • Casper, wy 888-235·0~15 qi~iSD~8JB~&t2~12~5 .C~llege stat~on, T)( 888-6'0-:2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp Annual Soils 2011 Lab 10: C11 081063-007 Client Sample 10: Westwater Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.12 0.1 0.03 0.02 MOC -Minimum detectable concentration Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g-dry Qualifier Rl 0.02 Report Date: 10/13/11 Collection Date: 08/23/11 09:29 DateReceived: 08/26/11 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/06/11 16:581 sml E903.0 09121/11 17:131 js E903.0 09/21/1117:13/js E903.0 09121/11 17:131 js MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 13 EN:RGY ,... LABORATORIES wWw.energylab.com M6.1 ExulltHicB Sliles 1.952 .. ",·:~i{~]~lJ,a-,.:~·'li~41;2~O'{ll ..• BiUing~~ Mf~iio-735';44.9 . Casper,W'f 888.-235-0515 iIJ~tfe; \w"Pl,;~8@·;1f1l. R~piq mty, so~ 888-&72.; 1225 • College Station, 1X' 888-6,0-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Annual Soils 2011 Analyte Count Result Units Method: E903.0 Sample 10: C11081063-007AMS Radium 226 Sample 10: C11081063-007AMSO Radium 226 Sample 10: LCS-31023 Radium 226 Sample 10: MB-31023 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike 1.6 pCi/g-dry Sample Matrix Spike Duplicate 1 .6 pCi/g-dry Laboratory Control Sample 0.29 pCi/g-dry 3 Method Blank -0.00015 pCi/g-dry 0.00014 pCi/g-dry 0.00032 pCi/g-dry MDC -Minimum detectable concentration Report Date: 10/13/11 Work Order: C11 081 063 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: 31023 Run: BERTHOLD 770-1_110914A 09/21/11 17:13 100 70 130 Run: BERTHOLD 770-1 110914A 09/21/11 17:13 100 70 130 1.9 25 Run: BERTHOLD 770-1 110914A 09/21/11 21 :35 97 70 130 Run: BERTHOLD 770-1 110914A 09/21/11 21 :35 U ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 10 of 13 EI\ERGY LABORATORIES m .energylati.com AnI_I ExCIIllsnc. SiiJCB .7852 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Annual Soils 2011 Analyte Count Result Units Method: SW6020 Sample 10: MB-31023 Uranium Sample 10: LCS2-31023 Uranium Sample 10: C11081071-006AMS4 Uranium Sample 10: C11081071-006AMSO Uranium Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Method Blank NO mg/kg-dry Laboratory Control Sample 1.71 mg/kg-dry Sample Matrix Spike 57 mg/kg Sample Matrix Spike Duplicate 47 mg/kg Report Date: 10/13/11 Work Order: C11 081 063 RL %REC Low Limit High Limit Run: ICPMS4-C_11 0906A 0.020 Run: ICPMS4-C_110906A 0.015 86 75 125 Run: ICPMS4-C_ 110906A 0.50 75 125 Run: ICPMS4-C_11 0906A 0.50 75 125 RPO RPOLimit Qual 18 Batch: 31023 09/06/11 16:15 09/06/11 16:18 09/06/11 20:29 A 09/06/11 20:32 20 A A -The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. MDC -Minimum detectable concentration Page 11 of 13 EN:RGY LABORATORIES ~1" wwW.energylab.com ~ Analjtieal ExciIUsm:, SinU 1952 :' ~·'H~le~~5IfB77}41.2;blll . Billings, MT 800-735-4489 · Casper. WY 888-235-0515 iif~1tefvki4:s'~~686~:~n~~· R.apidJitY •. sp.88B-.72.;1225 • Col/ege Sfat!on, ix 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C11 081 063 Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 8/29/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? A" samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 23.6'C Yes 0 Yes 0 Date Received: 8/26/2011 Received by: kg No 0 NoO No 0 No 0 No 0 NoO No 0 No 0 No 0 NoO No 0 No 0 Carrier Next Day Air name: Not Present 0 Not Present 0 Not Present 0' No VOA vials submitted 0' Not Applicable 0' Page 12 of 13 -0 III (Q (l) ~ w o ....., ~ w ''1~'/{''Y Chain of Custody and Analytical Request Record Page ---1-of -L •• ,..",zla»J •• PLEASE PRINT (Provide as much information as possible.) c~;me Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: r \ ,~ '\ s..tj Y'\ (\/\ \,,-lA !LAJ~oJ S" )'1.5 State: U..,-Yes D No 0 RepOrtMail Addr(S: , 0'1 Contact Name: Phone/Fax: Email: Sampler: (Please Print) e·O . tA¥ ~ aatl ~/YVtf!:t£ ~fd"W!~ 11,t.JiV/ ,'!?h rvl /J1t: fA -r X if S '/ / fL; 7-<;5 22/_1 Invoice Address:-~ InvoicEi Contact & Phone: Purchase Order: QuotelBottle order: --1 ... -')~vvvl_ ~~ -- Special Report/Formats: ~&[b W@D@ OOrn:@(ill~~@ • Contact ELI prior to Shipped by: ~ Ltr5,A/ tJA 0 Q; RUSH sample submittal ~o u).&:. ~ for charges and Cooler ID(s): ~1D;gOI Q; C R scheduling -See GI:~~) ._> 0 >.15 W t:. Instruction Page DDW o E DD/EDT(Electronic Data) J9(1)(I}t03: c: u, ~ J: -0 D POTWIWWTP Format: 03:'6 to C) () c: Comments: Receipt Temp ~<(I}I.Q~ :::J U 23. ~ D State: D LEVEL IV o ... ml c: « e °c G) CD c:'-I-eo ] a.rol~ Ci c: o Other: D NELAC t-~ On Ice: vf) E~ro ' « :::J :::J CD-: 13) 3: ~ ~ l-S zQ..~larc W "E Custody Seal ~ ~ >1 ~ W ('0 On Bottle Y ~ (J) "C 00 c: On Cooler ~ 19 ~ I en H Intact CV N SAMPLE IDENTIFICATION Collection Collection MATRIX ~ Signature (9 (Name, Location, Interval, etc.) Date Time Match 1 RUII -J I~J23J7A11 Ot,)5 1-.5 'f X ~ 2 J~J.kJ -2 , ; fJxLfS' /-S X I~ \( 3;J51tvJ( M~A ()q(JJ /-5 X x. ~ Innn 4i3JH -Lf (}1'10 I -S ,. ~ I~ ~ 5Mv~~ ItJ15.~ . J -S 1-"'j. .;:;:::J ~ 6~HV,. it? , 11J1s-D 1-S X 'f. ~~ 7!tJLsr~ F<!Z3JOII (jq11 I-~ )( X ~'jJ~lD~ 8 / I ~. 9 , 10 ~ ...., Custody R~::YfI/MeL Dag7JS/3J// ~re: Received by (print): Oatemme: Signature: Ii5/) Record R9linqui,hed by (print): Dat~mme:' U Signature: ' Received by (print): Datemme: Signature: MUST be Signed I~vea Dy LaQOrawry: l!atelilme: ;:iJgnature: Sample Disposal: Return to Client: Lab Disposal: ~ .1....; t6._~_// 9."~ In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links.