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HomeMy WebLinkAboutDRC-2011-007271 - 0901a06880267271n n n U u 4 DENISO MINES Denison Mines (USA) Corp. 105017th Street, Suite 950 Denver, CO 80265 USA Tel: 303 628-7798 Fax: 303 389-4125 www.clenisdnmines.com August 31, 2011 VIA FEDERAL EXPRESS Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West RO. Box 144820 Salt Lake City, UT 84114-4820 Dear Mr. Lundberg: / Re: State of Utah Radioactive Material Lta White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period January 1, 2011 through June 30,2011 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart!)), and License Condition 11.3 A of State of Utah Radioactive Materials License No. UT 1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period January 1, 2011 through June 30, 201L If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly, DENISON MINES (USA) CORP. Jo Ann Tischler Director, Compliance and Permitting cc Ron F. Hoehstein Harold R, Roberts David C. Frydenlund David E.Turk Katherine Weinel Central Files August 31, 2011 VIA FEDERAL EXPRESS Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period January 1,2011 through June 30, 2011 Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303628-7798 Fax: 303389-4125 www.denisonmines.com As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart1)), and License Condition 11.3 A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period January 1, 2011 through June 30, 2011. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly, ~~ DENISON MINES (USA) CORP. Jo Ann Tischler Director, Compliance and Permitting CC Ron F. Hochstein Harold R. Roberts David C. Frydenlund David E. Turk Katherine Weinel Central Files White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (January through June, 2011) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 August 31, 2011 Table of Contents 1.0 INTRODUCTION .................................................................................................. 1 2.0 ENVIRONMENT AL AIR PARTICULATE SAMPLING ..................................... 2 2.1 Program Overview ............................................................................................... 2 2.2 Sampling Protocol and Analytical Results ........................................................... 2 2.3 General Observations ........................................................................................... 3 2.4 Site Specific Sampling Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ..................................................................................... 8 5.0 STACK SAMPLING ............................................................................................... 9 6.0 SURFACE WATER MONITORING .................................................................... 11 7.0 SOIL SAMPLING ................................................................................................. 11 8.0 METEOROLOGICAL MONITORING ................................................................ 11 9.0 SIGNATURE ......................................................................................................... 12 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-21O Concentration Example Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-21O (Comparison to Limits) Table 6 Environmental OSL Dosimeter Measurements (Gamma) Table 7 Stack Sampling Requirements Table 8 Stack Effluent Concentrations and Release Rates INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tabl BHV-l Air Sampling Graphs and Data Table Tab 2 BHV -2 Air Sampling Graphs and Data Table Tab 3 BHV-3 Air Sampling Graphs and Data Table Tab 4 BHV -4 Air Sampling Graphs and Data Table Tab 5 BHV-5 Air Sampling Graphs and Data Table Tab 6 BHV -6 Air Sampling Graphs and Data Table C Air Particulate Loading Graphs and QAJQC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Graphs. Data Table, Laboratory Results and QAJQC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QAJQC ii WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER, 2010 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-l and BHV-2 (north), BHV-5 (east), and BHV-4 (south). BHV-l serves as a surrogate for the nearest resident (BHV-l is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV-3), which was monitored for airborne particulate up until November, 1995, at which time background was established, but is no longer monitored for air particulate; and • A station specifically requested by the White Mesa Ute Community south ofthe Mill Site (BVH-6); a) External (direct) gamma radiation measured at air monitoring stations BHV-l, BHV -2, BHV -3, BHV -4, BHV -5 and BHV -6; b) Vegetation at three site periphery locations, for uptake of radiation; c) Stack release rates from the Mill's air emissions sources; d) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; e) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; 1 N :\Required Reports\Semi Annual Effluent Reports\20 11 Jan to June\Jan_to_Jun_20 II_Semi_annual_EffluenCReport_Main_text.docx f) Groundwater (up and down gradient) of the Mill facility; and l g) Seeps and springs in the vicinity of the Mill. I This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV-l, BHV-2, BHV -4, and BHV -5) are required by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring data base had been compiled at BHV -3 to establish a representative airborne radionuc1ide background for the Mill. It should be noted, however, that while air sampling was discontinued at this location, gamma measurements and soil sampling continue to be collected at BHV-3. In addition to the environmental air sampling locations described above, an additional station (BHV-6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb- 210 activity. Fugitive dust standards for the facility are limited by the Mill's State of I Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 N:\Required Reports\Semi Annual Effluent Reports\20ll Jan to JuneVan_to_Jul1_2011_Semi_annual_EftluenCReport_Mail1_text.doex Utah Air Approval Order, which sets a 20% visual opacity standard. The specific locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled High Volume Air Monitoring Stations included as Attachment A. Station BHV- 3, which is no longer sampled for air particulate is located approximately 3.5 miles west of the Mill facility and is not indicated on that Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this January through June, 2011 reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QAJQC information) reported by the laboratory are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and composited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station for the second half of 2010 and the underlying data are included as Attachment D. It should be noted that for graphical illustration purposes, values reported at zero, values reported at less than the prescribed detection limit « 1 X 10-16 uCi/ml) and missing values were plotted as 1 x 10-16 uCi/ml concentrations. Where other "less than" values were indicated (i.e., where detection limits for the data varied from 1 x 10-16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-21O concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay 3 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to June\J an_to_Jun_20 II_Semi_annuaLEffluenCReport_Main_text.docx products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Ph-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-21O is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 below, demonstrating elevated Pb-21O activity where no uranium milling operations are located nearby. Pb-210 activity concentrations can be expected to he even higher for locations in the western U.S. where uranium ore bodies are commonly located. In April 1977, prior to Mill construction and Mill operations, air particulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/ml (13.0E-3 pCi/m3)2 Table 1-NCRP Report 94-Global Pb-210 Concentration Example State Ph·210 Concentration uBqlMJ uCilrnl California 600 1.6E-14 lllinois 1500 4.lE-14 Ohio 300 8.lE-iS Massachusetts 700 1.9E-I4 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data supports the conclusion that airborne particulate is well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). It should also be noted that the analytical laboratory maintained Lower Limits of Detection consistent with NRC Regulatory Guide 4.14 for this reporting period. In fact, the data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utahfor Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30,1978, Section 2.9.1.1 4 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to JuneVan_to_Jun_2011_Semi_annuaLEffluencReport_Main_text.doex ever exceeded the ECL at the Mill. With regard to that particular single measurement, while it is important to consider and evaluate an individual measurement exceeding the ECL, for public dose estimation purposes it is the average annual concentration that is of primary significance. In that instance, the average annual concentration of Th-230 for BHV-5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALAR A goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVI 9.01E-16 1.59E-15 9.00E-14 1.38E+OO BHV2 3.79E-16 3.07E-16 9.00E-14 3.81E-Ol BHV4 1.29E-15 3.30E-15 9.00E-14 2.55E+OO BHV5 3.20E-15 6.98E-15 9.00E-14 5.66E+OO BHV6 2.70E-15 3.01E-15 9.00E-14 3. 17E+OO Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Station Result Result (uCi/ml) (uCi/ml) BHVI 1.90E-16 5.31E-16 BHV2 4.01E-17 8.54E-17 BHV4 1.40E-16 5.44E-16 BHV5 8.89E-16 2.03E-15 BHV6 4.62E-16 7.07E-16 5 N :\Required Reports\Semi Annual Effluent Reports\20 II Jan to June\Jan_to_Jun_20 Il_SemLannual_EffluenCReport_Main_text.docx Effluent Average Concentration Percent Limit (ECL) ECL (uCi/ml) 2.00E-14 1.80E+OO 2.00E-14 3.14E-Ol 2.00E-14 1.7lE+OO 2.00E-14 7.30E+OO 2.00E-14 2.92E+OO Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVI 3.64E-I6 4.99E-16 9.00E-13 4.79E-02 BHV2 9. llE-17 9.21E-17 9.00E-13 l.02E-02 BHV4 1.58E-16 4.18E-16 9.00E-13 3.20E-02 BHV5 1.1OE-I5 2.52E-15 9.00E-13 2.0IE-Ol BHV6 6.51E-16 5.75E-16 9.00E-13 6.8IE-02 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVI 1.09E-I4 8.38E-15 6.00E-13 1.61E+OO BHV2 1.06E-14 7.21E-I5 6.00E-13 1.48E+OO BHV4 1. llE-14 8.26E-15 6.00E-13 1.6IE+OO BHV5 1.48E-I4 1.08E-14 6.00E-13 2. 13E+OO BHV6 1.29E-14 7.97E-15 6.00E-13 1.74E+OO 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the new 10 CFR Part 20 standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was discontinued in 1995. Instead, Denison demonstrates compliance with these limits and the requirements of R313-15-301 by calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division on July 28, 2008. This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the 6 N:\Required Reports\Semi Annual Effluent Reports\20ll Jan to June\Jan_to_Jufl_2011_SemLannual_EffluenCReport_Main_text.docx concentrations of radioactive dust and radon at individual receptor locations around the Mill. The MILDOS and MILD OS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 100 mrem regulatory limit in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well below the ALARA goal of 10 mrernJyr for air emissions excluding radon as set out in R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U30 8 and 1.5% VzOs) and Arizona Strip ore (0.637% U308). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -1 at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the 1st and 2nd quarters of 2011 utilizing passive integrating devices, optically stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-l, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). Measurements obtained from location BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented at Attachment E to this report. 7 N :\Required Reports\Semi Annual Effluent Reports\20 II Jan to June\Jan_to_Jun_ZOII_Semi_annual_Eftluent_ReporcMain_text.docx Table 6-Environmental Optically Stimulated Luminescence Dosimeter ~easurements (iamma) Monitoring 1st Qtr 2nd Qtr 1st Qtr 2nd Qtr Cumulative Station Result Result Result Less Result Less Semi- (mrem) (mrem) Background Background Annual (mrem) (mrem) Estimate* (mrem) BHVI 41.7 26 7.7 3.6 11.3 BHV2 34.3 24.2 0.3 1.8 2.1 BHV3 34 22.4 0 0 0 BHV4 38.2 21.5 4.2 -0.9 4.2 BHV5 42.2 25.6 8.2 3.2 11.4 BHV6 32.7 24.8 -1.3 2.4 2.4 *Negative values treated as zero for cumulative dose The results for this period indicate that above background measurements for stations BVH-1, BVH-2, BVH-4, BVH-5 and BHV-6 are within regulatory limits. BHV-1 is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV -1. The annual individual member of the public limit is 100 rnrem/yr for combined internal and external exposure. 4.0 VE(iETATION SAMPLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. The U.S. Nuclear Regulatory Commission ("NRC") Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. During the 2011 grazing season, two sets of samples have been collected to date, on June 23, 2011 and in July 2011. A third set of samples is planned for the fall season. At the conclusion of the third quarter of 2011, three sets will have been collected consistent with Regulatory Guide 4.14. The data from the June 2011 sampling is included in the current January to June 2011 Semi-Annual Effluent Report ("SAER"). Data from the July and fall sampling will be included in the July to December 2011 SAER. Section 4.2 of the Mill's Environmental Protection Manual states that vegetation samples are to be collected during the early spring, late spring and fall (i.e., the growing seasons). During the January to June 2011 period, the early spring samples were inadvertently omitted. The late spring sample was collected just past the end of spring (on June 23, 2011). An additional summer sample was collected in July 2011 in place of the omitted early spring sample. As a result, as discussed above, three samples will have been collected by the end of the 2011 grazing season meeting the requirements of NRC Regulatory Guide 4.14. 8 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to JuneVan_to_Jun_20 II_Semi_annuaLEftluent_Report_Main_text.docx Graphical log-scale presentation of the vegetation sampling results for this reporting period, together with the analytical results reported by the Mill's contract laboratory (including QAlQC information) are included at Attachment F of this report. The 2nd quarter data results are within the variation of previous sampling episodes. 5.0 STACK SAMPLING Vnder Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: DVSA-1, 2/07 (the "Environmental Protection Manual") gas stack samples are collected at the Mill in accordance with the calendar year schedule shown below: Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging Baghouse) Yellowcake Dryer (Yellowcake Baghouse) Quarterly None If operating, V-nat If operating, V-nat Semi-annually If operating, V-nat, If operating, V-nat, If operating, V-nat, Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-21 0 The yellowcake dryer and yellowcake baghouse operated during the 1st quarter of 2011. The yellowcake dryer, yellowcake baghouse, and grizzly operated during the 2nd quarter of2011. The analytical results of stack sampling conducted for the 1st and 2nd Quarter of 2011, as well as for the 3rd and 4th Quarters of 2010, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate (uCi/sec) for V-Nat, Th-230, Ra-226 and Pb-21O at each of the stacks sampled. The actual analytical results reported by the laboratory for the 1st and 2nd quarters of 2011 are provided in Attachment G to this report. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL' s for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi-annual reporting purposes. 9 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to June\.Jan_to_Jun_2011_SemLannuaLEffluenCReport_Main_text.docx Table 8-Stack Effiuent Concentrations and Release Rates U-Nat V-Nat. Th-230 Th-230 Ra-226 Ra-226 Pb-2IO Pb-2l0 u/Ci/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCilcc uCi/sec 3"1 Qtr, 2010 North YC Dryer, Run Not Not Not Not Not Not 1 6.97E-09 4.2IE-03 Required Re_quired Re'luired Required Required Required North YC Dryer, Run Not Not Not Not Not Not 2 9.02E-09 5.32E-03 Required Re_quired Required Required Required Required Yellowcake Not Not Not Not Not Not Baghouse 1.37E-09 4.57E-05 Required Required Required Required Required Required 4,n Qtr, 2010 North YC Dryer, Run 1 1.44E-08 7.33E-03 2.IOE-II 1.07E-05 3.32E-12 l.69E-06 8.89E-14 4.53E-08 North YC Dryer, Run 2 1.25E-08 6.5IE-03 7.97E-12 4.14E-06 2.73E-I2 1.42E-06 2.18E-13 1.13E-07 Yellowcake Baghouse 1.05E-09 9.19E-04 5.50E-12 4.80E-06 2.87E-13 2.51E-07 4.23E-14 3.69E-08 1 ~l Qtr, 2011 North YC Dryer, Run Not Not Not Not Not Not 1 5.02E-09 3.17E-03 Required Required Required Required Required Required North YC Dryer, Run Not Not Not Not Not Not 2 3.67E-09 1.93E-03 Required Required Required Required Required Required Yellowcake Not Not Not Not Not Not Baghouse 2.90E-09 2.92E-03 Required Required Required Required Required Required 2nd Qtr, 2011 North YC Dryer, Run 1 1.76E-08 9.2IE-03 l.76E-12 9.25E-07 4.20E-I4 2.20E-08 7.52E-12 3.94E-06 North YC Dryer, Run 2 1.54E-08 7.56E-03 2.12E-12 1.04E-06 4.79E-14 2.35E-08 7.94E-12 3.90E-06 Yellowcake Baghouse 8.S8E-09 8.22E-03 1.97E-li 1. 89E-OS 1.96E-13 1.88E-07 8.32E-13 7.97E-07 Grizzly Not Not Not Not Baghouse 9.71E-12 5.96E-06 1.09E-13 6.67E-08 Required Required Required Required 10 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to J une\J an_to_J un_20 11_Semi_annual_EffluenCReport_Main_texLdocx 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample in the event that surface water is not available for sampling. Westwater Canyon surface water was not sampled in the first or second quarter 2011 because no water was present during this reporting period. Attempts to collect a surface water sample from Westwater Canyon will continue through the next reporting period. If no surface water is available, a sediment sample will be collected as required. The Mill's Environmental Protection Manual, requires that Cottonwood Creek be sampled for total dissolved solids (TDS) and total suspended solids (TSS) quarterly and dissolved and suspended radionuclides including Gross Alpha, Unat, Ra-226, Th-230 semi-annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS and TSS during both the 1 st and 2nd quarter and for the dissolved and suspended radionuclides noted above during the 2nd quarter. Cottonwood Creek is an intermittent ephemeral drainage located southwest and down- gradient of the Mill complex. Westwater Canyon is a drainage located west of the Mill facility, which is rarely flowing. The field data sheets for the surface water sampling attempts, along with graphs showing historic results are included as Attachment H. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6) once per year during August or as soon as possible thereafter, but no later than September 30 of each year. In accordance with the Mill's Environmental Protection Manual, surface soils will be collected during the third quarter 2011 and will be discussed in the July through December 2011 report. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of January through June, 2011. This information is retained at the Mill site for agency review. 11 N:\Required Reports\Semi Annual Effluent Reports\201 I Jan to J une\Jan_to_Jun_20 I LSemi_annual_Effl uenCReport_Main_text.docx 9.0 SIGNATURE This RepOit was prepared by Denison Mines (USA) Corp. on August 3 1, 20 11. Denison Mines (USA) Corp. By: Davi . Fry olund Vice Presiden • Regulatory Affairs and Counsel N:\Rcql,lired Rcpons\Semi Annual Emucnl Rcpons\2011 Jan 10 June\IruuoJuvOl l_SeIllLannuDLErnuen[_Rcpott~ain_tcxl.doc); ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS W:lUSAlUlilhWiI\C\'Igs\.qr.lamaticn Plar"'flecPlan 32·rlllllllr<l",e 2.3-1 Air MonItoIinq.dwQ Fiqur& 2.30, 14101f.1011 ~r r ~ ~... \"'.:i"· l I ~. o BHV-2 N ~I ~ ... ' ~ ,... ... VI ~,. ,~ ( " 1 *I; ,-...I •• ~ ... I .... ... -,"-, ~ ... -,/ ..... , .t J ' . ..' 0# Ie-, ---, .... f i i --, \ .. , , \" I / , , -- , I + , / , I ~ . ) 2000 ~ 0 2000 I ~W SCAl.£ IN FEET '. I \ \. ""' ",,, \ , / .. 1 i I ',,~ , ~/'I ~v ~/1 , \ I I 1--, , ., .. , ... .., ' ~ ... = , ... ... • ~ -.-'. ::~." I , I" 1IIt. ... #, > " ~, \ -. (' .I~ I' ~ : / ... , " , -) v-i:' I '-I -: ... ,...-' , __ ,''''A' " ~ ... " ,,---c,.eev. ,oJ ,,..,--, ~ ... L !fElL NO. 1 J L:! ~ ~ '\ .. 'l ' '" 1J\'Il. , "'-, ~e"~ ,/ , /-1 " " ) '-........-, , .... -'1...,'"...,:,. ... .. , .. I ,/ r---\ , , I \ I I I \ I ( .,..J , () \ ~ <> • % \ &. ~ z /~ I , , / I ------" \ " "~oC. "\ -- ~ ttl' I .. .. ~...I --..-.. .. 'Ar,_ I I'~ --" .. ,r-I ~ I .. \ "-I ~.j ~'I ,,'" , l , ,/' , , \ , ---'---, '---, , , ( ... -., , .. .. I .. f ~, , .......... ~ r,.~ o 8HV-~ o BHV-5 o BHV-6 ,.. .... :t. ... 4 J : -:. ... ' ... 1 , , ... ... ... tU' .. ,. \ ~~ .. I .. .. I .. ~ ... .. I ... .. I ,. \ --I ( ,/ # I ' ~1 ~ I! ~"\ B! .. t .. ,~ \'-' i .,~ . . .. \~< -• ~ .. . -" " ... \-. ..L. _~ ,~ '" ! ,,~ ~,.! ! -., \-l. ... \..... ~ ':: I, ~ \ ". c. I ~ .,' "- I, '--, I., tl ,'" ~.~ '] , .. ~, .. ... ~\\\ ~ ; i;, ~~ L - # \\ ~ -~\:..... I 0 ;).1 .. 191 " ... ... - " ... ,t " #, I;. -" .. ~~ t, ... ~ I" .. #, .. * ... ~ ..... " ... .., -J .,'" !q. ,~ ~ l' u~ I ( .. ~ ~ ... ... LL ri ~ " I-~,,~, ~" ."fL. u ... ,-' t{ _11-11- Property Boundary Reservation Boundary Canyon Rim o Air Monitor Stations Project REVISIONS Dace Denison Mines (USA) Corp. WHITE MESA MILL County: SAN JUAN j Slafe: UT Figure 2.3-1 High Volume Air Monitoring Stations O'NISOJ)~J MI .... ~ _ 1II1'II 2.3-1_.0'" monitorinl.cfwg ,,,,rIMBj: B. loi&mld1baotat ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV-l AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml IIHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-1T Effluent Concentration Umit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB I ALARAGoal= 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE·13 uCi/ml ALARAGoal = l.SE-13 uCi/ml I Pre 1994 MPC Limit = SE-12 uCi/ml pre 1994 MPC Limit = 8E-14 uCi/ml Pr~ 1994 MPC LimIt = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml I Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-lZ uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.35E-15 5.00E-12 1.25E-12 7.82£-16 8.00E-14 2.00£-14 1.06E-15 2.00£-12 5.00E-13 2.57E-14 4.00£-12 1.00E-12 12/14/1981 1.56E-15 5.00E-U 1.25E-12 1.49E-15 8.00E-14 2.00E-14 1.93E-15 2.00E-12 5_00E-13 2.64E-14 4.00E-U 1.00E-12 3/29/1982 2.16E-15 5.00E-12 1.25E-12 2.93E-15 8.00E-14 2.00E-14 1.16E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 1.00E-12 6/30/1982 4.69E-15 5.00E-12 1.25E-12 3.46E-15 8.00E-14 2.00E-14 2.38E-15 2.00E-12 5.00E-13 2.14E-14 4.00E-12 1.00E-12 9/27/1982 4.45E-15 5.00E-12 1.25E-12 3.29E-15 8.00E-14 2.00E-14 3.23HS 2.00E-12 5.00E-13 1.99E-14 4.00E-12 1.00E-12 1/3/1983 4.39E-15 5.00E-12 1.25E-12 5.91E-16 8.00E-14 2.00E-14 9.14E-16 2.00E-12 5.00E-13 4.87E-14 4.00E-12 1.00E-12 4/4/1983 7.51E-16 5.00E-12 1.25E-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 5.00E-13 1.88E-14 4.00E-12 1.00E-12 6/30/1983 2.68E-16 5.00E-12 1.25E-12 6.92E-16 8.00E-14 2.00E-14 7.92E-16 2.00E-12 5.00E-13 2.00E-14 4.00E-U 1.00E-12 10/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E·12 5.00E-13 4.00E-12 1.00E-12 1/3/1984 2.87E-15 5.00E-12 1.25E-12 1.14E-16 8.00E-14 2.00E-14 1.79E-16 2.00E-12 5.00E-13 1.06E-14 4_00E-12 1.00E-12 4/2/1984 1.59E-15 5.00E-12 1.25E-12 3.40E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 3.34E-14 4_00E-12 1.00E-12 7/2/1984 3.10E-15 5.00E-12 1.25E-12 1.00E-15 8.00E-14 2.00E-14 2.09E-15 2.00E-12 5.00E-13 1.88E-14 4.00E-12 1.00E-12 10/1/1984 6.42E-16 5.00E-12 1.25E-12 1.39E-16 8.00E-14 2.00E-14 1.94E-16 2.00E-12 5.00E-13 1.85E-14 4.00E-12 1.00E-12 1/2/1985 5.06E-16 5.00E-12 1.25E-12 4.56E-16 8.00E-14 2.00E-14 3.49E-16 2.00E·12 5.00E-13 3.03E-14 4.00E-12 1.00E-12 4/1/1985 O.OOE+OO 5.00E-U 1.25E-12 1.23E-15 8.00E-14 2.00E-14 4.88E-16 2.00E-12 5.00E-13 8.06E-15 4.00E-12 1.00E-12 7/1/1985 7.17E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 1.05E-15 2.00E-12 5.00E-13 2.15E-14 4.00E-12 1.00E-12 9/30/1985 6.13E-16 5.00E-12 1.25E-12 1.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 3.64E-15 4.00E-12 1.00E-U 1/2/1986 3.42E-15 5.00E-12 1.25E-12 4.74E-16 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 4/1/1986 .3.98E-15 5.00E-12 1.25E-12 9.74E-16 8.00E-14 2.00E-14 1.50E-15 2.00E-12 5.00E-13 1.41E-14 4.00E-12 1.00E-12 6/30/1986 5.51E-17 5.00E-12 1.25E-12 3.52E-16 8.00E-14 2.00E-14 1.37E-15 2.00E-12 5.00E-13 1.23E-14 4.00E-12 1.00E-12 10/27/1986 1.99E-15 5.00E-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 1.25E-15 2.00E-12 5.00E-13 1.08E-14 4.00E-U 1.00E-12 12/15/1986 1.67E-15 5.00E-U 1.25E-12 1.16E-16 8.00E-14 2.00E-14 5.98E-16 2.00E-12 5.00E-13 1.37E-14 4.00E-U 1.00E-12 3/16/1987 2.33E-15 5.00E-12 1.25E-12 4.30E-16 8.00E-14 2.00E-14 1.92E-16 2.00E-12 5.00E-13 5.59E-14 4.00E-U 1.00E-12 5/11/1987 2.36E-15 5.00E-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 8.76E-16 2.00E-12 5.00E-13 1.45E-14 4.00E-12 1.00E-U 9/9/1987 2.27E-15 5.00E-U 1.25E-12 2.44E-15 8.00E-14 2.00E-14 8.51E-16 2.00E-12 5.00E-13 3.14E-14 4.00E-U 1.00E-U 11/2/1987 2.75E-15 5.00E-12 1.25E-12 2.46E-15 8.00E-14 2.00E-14 1.34E-15 2.00E-12 5.00E-13 2.79E-14 4.00E-U 1.00E-12 2/16/1988 1.07E-15 5.00E-12 1.25E-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 2.00E-12 5.00E-13 4.01E-14 4.00E-12 1.00E-12 5/18/1988 1.98E-15 5.00E-12 1.25E-12 1.25E-15 8.00E-14 2.00E-14 6.40E-16 2.00E-12 5.00E-13 1.07E-14 4.00E-12 1.00E-12 8/15/1988 2.06E-15 5.00E-12 1.25E-12 3.41E-15 8.00E-14 2.00E-14 5.08E-16 2.00E-12 5.00E-13 1.62E-14 4.00E-12 1.00E-12 11/14/1988 3.94E-15 .5.00E-12 1.25E-12 2.12E-15 8.00E-14 2.00E-14 1.01E-15 2.00E-12 5.00E-13 2.47E-14 4.00E-12 1.00E-12 2/13/1989 1.99E-15 5.00E-12 1.25E-12 5.73E-16 8.00E-14 2.00E-14 5_99E-16 2.00E-12 5.00E-13 3.23E-14 4.00E-12 1.00E-12 5/15/1989 1.70E-15 5.00E-12 1.25E-12 6.32E-16 8.00E-14 2.00E-14 5.86E-16 2.00E-12 5.00E-13 6.16E-15 4.00E-12 1.00E-12 8/14/1989 2.31E-15 5.00E·12 1.25E-12 2.31E-16 8.00E-14 2.00E-14 1.77E-16 2.00E-12 5.00E-13 7.65E-15 4.00E-12 1.00E-U 11/13/1989 4.72E-15 5.00E-12 1.25E-12 1.71E-15 8.00E-14 2.00E-14 1.52E-15 2.00E-12 5.00E-13 1.89E-14 4.00E-12 1.00E-12 2/12/1990 3.44E-16 5.00E-12 1.25E-12 8.39E-16 8.00E-14 2.00E-14 8.31E-16 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 5/14/1990 3.03E-15 5.00E-12 1.25E-12 1.47E-15 8.00E-14 2.00E-14 1.04E-15 2.00E-12 5.00E-13 1.79E-14 4.00E-12 1.00E-12 8/13/1990 1.64E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 3.34E-16 2.00E-12 5.00E-13 8.27E-15 4.00E-12 1.00E-U 11/12/1990 1.48E-15 5.00E-12 1.25E-12 7.50E-16 8.00E-14 2.00E-14 5.80E-16 2.00E-12 5.00E-13 2.16E-14 4.00E-12 1.00E-12 2/11/1991 1.90E-16 5.00E-12 1.25E-12 3.48E-17 8.00E-14 2.00E-14 7.91E-17 2.00E-12 5.00E-13 3.79E-14 4.00E-12 1.00E-12 5/13/1991 3.42E-16 5.00E-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 7.39E-16 2.00E-12 5.00E-13 1.46E-14 4.00E·12 1.00E-12 8/12/1991 2.77E-16 5.00E-U 1.25E-12 4.17E-17 8.00E-14 2.00E-14 1.45E-16 2.00E-12 5.00E-13 1.80E-14 4.00E-U 1.00E-12 U/U/1991 6.65E-17 5.00E-U 1.25E-12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 1.06E-14 4.00E-12 1.00E-U 2/10/1992 1.94E-16 5.00E-12 1.25E-U 4.28E-17 8.00E-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.51E-14 4.00E-12 1.00E-12 5/11/1992 2.54E-16 5.00E·U 1.25E-12 6.49E-16 8.00E-14 2.00E-14 6.86E-17 2.00E-12 5.00E-13 1.38E-14 4.00E-12 1.00E-12 8/10/1992 1.73E-16 5.00E-12 1.25E-12 1.55E-16 8.00E-14 2.00E-14 1.20E-16 2.00E-12 5.00E-13 1.53E-14 4.00E-U 1.00E-12 11/9/1992 1.56E-16 6.00E-12 1.25E-12 3.19E-17 8.00E-14 2.00E-14 4.90E-18 2.00E-12 5.00E-13 1.86E-14 4.00E-12 1.00E-12 2/9/1993 2.10E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 3.89E-17 2.00E-12 5.00E-13 2.52E-14 4.00E-12 1.00E-12 6/10/1993 1.00E-16 5.00E-U 1.25E-12 4.11E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 5.00E-13 1.26E-14 4.00E-U 1.00E-12 8/10/1993 .2.30E-16 5.00E-12 1.25E-12 6.00E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 5.00E-13 1.60E-14 4.00E-U 1.00E-12 11/8/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 1_57E-14 4.00E-12 1.00E-12 2/7/1994 1.82E-16 5.00E-12 1.25E-12 5.00E-18 8.00E-14 2.00E-14 4.30E-17 2.00E-12 5.00E·13 2.59E-14 4.00E-12 1.00E-12 5/9/1994 3.60E-16 5.00E-U 1.25E-12 2.70E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 5.00E-13 1.60E-14 4.00E-12 1.00E-12 8/9/1994 4.04E-16 5.00E-12 1.25E-12 2.70E-16 8.00E-14 2.00E-14 2.94E-16 2.00E-12 5.00E-13 2.00E-15 4.00E-12 1.00E-U 11/7/1994 9.18E-17 5.00E-12 1.25E-U 3.60E-16 8.00E-14 2.00E-14 2.91E-16 2.00E-12 5.00E-13 2.00E-15 4.00E-U 1.00E-U Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARAGoal-2.25E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC Lim)t = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.77E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 S.00E-15 9.70E-17 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 5.36E-16 2.00E-14 $.00E-15 1.60E-15 9.00E-13 2.25E-13 3.84E-15 6.00E-13 1.50E-13 8/9/1995 2.70E-16 9.00E-14 2.25E-14 1.60E-16 2.00E-14 5.00E-15 2.76E-16 9.00E-13 2.25E-13 3.76E-15 6.00E-13 1.50E-13 11/11/1995 4.80E-15 9.00E-14 2.25E-14 6.41E-16 2.00E-14 5.00E-15 8.93E-16 9.00E-13 2.25E-13 5.20E-15 6.00E·13 1.50E·13 2/5/1996 5.34E-15 9.00E-14 2.25E-14 2.30E·15 2.00E-14 5.00E-15 1.30E·15 9.00E-13 2.25E-13 4.20E-15 6.00E-13 1.50E·13 5/6/1996 5.11E-16 9_00E·14 2.25E-14 3.06E-16 2.00E-14 5.00E-15 1.40E-16 9.00E-13 2.25E·13 7.03E-15 6.00E·13 1_50E-13 8/5/1996 5.99E·16 9.00E·14 2.25E-14 1.55E·15 2.00E-14 5.00E-15 2.03E-16 9.00E·13 2.25E-13 5.94E-15 6.00E-13 1.50E-13 11/6/1996 3.38E-16 9.00E·14 2.25E-14 5.45E·16 2.00E·14 5.00E·15 1.00E-16 9.00E·13 2.25E·13 1.22E·14 6.00E·13 1.50E-13 2/6/1997 1.00E-16 9.00E·14 2.25E-14 1.25E-16 2.00E-14 5.00E-15 1.28E-16 9.00E·13 2.25E-13 5.68E-15 6.00E·13 1.50E·13 5/5/1997 1.09E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E·13 2.25E·13 4.39E-15 6.00E·13 1.50E-13 8/11/1997 2.88E·16 9.00E-14 2.25E-14 3,83E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E·13 5.29E-15 6.00E-13 1.50E-13 1/5/1998 3.24E-16 9.00E-14 2.25E-14 3.47E-16 2.00E-14 5.00E-15 1.19E-16 9.00E-13 2.25E·13 4.73E-15 6.00E·13 1.50E·13 4/28/1998 4.75E-16 9.00E·14 2.25E-14 6.73E-16 2.00E-14 5.00E-15 5.69E-16 9.00E-13 2.25E-13 5.94E-15 6.00E·13 1.50E-13 7/31/1998 8.84E-16 9.00E-14 2.25E-14 1.93E-15 2.00E-14 5.00E·15 1.43E-15 9.00E-13 2.25E-13 5.22E-15 6.00E·13 1_50E-13 9/28/1998 :Z.81E-16 9.00E·14 2.25E-14 2.89E-16 2.00E-14 5.00E·15 1.80E-16 9.00E-13 2.25E-13 4.64E-15 6.00E·13 1.50E·13 12/28/1998 8.08E-16 9.00E·14 2.25E-14 4.93E-16 2.00E-14 5.00E·15 5.01E-16 9.00E-13 2.25E-13 1.06E-14 6.00E·13 1.50E-13 3/29/1999 2.06E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5.00E-15 1.42E-16 9.00E·13 2.25E-13 6.69E·15 6_00E·13 1.50E-13 7/3/1999 5.31E-16 9.00E·14 2.25E-14 2.47E-16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13 9/27/1999 8.98E-16 9.00E-14 2.25E-14 3.90E-16 2.00E-14 5.00E-15 2.96E-16 .9.00E-13 2.25E-13 7.29E-15 6.00E-13 1.50E-13 12/28/1999 1.48E-15 9.00E-14 2.25E-14 6.00E·16 2.00E-14 5.00E-15 S.57E-16 9.00E·13 2.25E-13 6.19E·15 6.00E-13 1.50E·13 3/27/2000 1.00E·16 9.00E·14 2.25E-14 1.06E·16 2.00E-14 5.00E-15 1.00E-16 9.00E·13 2.25E-13 6.23E-15 6_00E·13 1_50E-13 6/26/2000 3.47E-16 9.00E-14 2.25E-14 3.46E-16 2.00E-14 5.00E-15 3.62E-16 9.00E·13 2.25E·13 4.50E-15 6.00E-13 1.50E-13 9/26/2000 2.51E-16 9.00E·14 2.25E·14 1.78E-16 2_00E-14 5.00E-15 3.25E-16 9.00E-13 2.25E-13 8.55E-15 6.00E-13 1.50E-13 12/26/2000 1.00E-16 9.00E-14 2.25E-14 1.42E-16 .2.00E-14 5.00E-15 i.31E-16 9.00E-13 2.25E-13 7.77E-15 6.00E·13 1.50E-13 3/26/2001 3.10E·16 9.00E-14 2.25E-14 1.00E-15 2.00E-14 5.00E-15 1.00E-15 9.00E-13 2.25E·13 7.19E·15 6.00E·13 1.50E-13 7/29/2001 1.52E·16 9.00E-14 2.25E-14 1.44E-16 2.00E-14 5.00E-15 1.77E-16 9.00E·13 2.25E-13 7.21E-15 6.00E-13 1.50E-13 9/24/2001 1.03E-16 9.00E-14 2.25E-14 1_00E-16 2_00E·14 5.00E·15 1.00E-16 9.00E-13 2_25E-13 8.09E-15 6.00E·13 1.50E-13 12/31/2001 1.00E-16 9.00E·14 2.25E-14 1.00E·16 2.00E-14 5.00E-15 1.00E-16 9.00E·13 2.25E·13 1.39E·15 6.00E·13 1.50E·13 4/1/2002 2.05E-16 .9.00E-14 2.25E-14 2.44E-16 2.00E-14 5.00E·15 2.29E-16 9.00E-13 2.25E-13 8.15E-15 6.00E-13 1.50E-13 7/1/2002 3_55E-16 9.00E-14 2.25E-14 4.85E-16 2.00E-14 5.00E-15 1.06E-16 9.00E-13 2.25E-13 7.65E-15 6.00E-13 1.50E-13 9/30/2002 1.17E-16 9.00E-14 2.25E-14 1.61E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.68E-15 6.00E-13 1.50E-13 12/30/2002 1.00E-16 9.00E-14 2.25E-14 1.03E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.46E-15 6.00E-13 1.50E-13 3/31/2003 1.20E-16 9.00E-14 2.25E-14 1.12E-16 2_00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13 6/30/2003 2.18E-16 9.00E-14 2.25E-14 3.40E-16 2_00E-14 5.00E-15 1.67E-16 9.00E-13 2.25E-13 5.96E-15 6.00E-13 1.50E-13 9/29/2003 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13 12/29/2003 LOOE-16 9.00E-14 2.25E-14 2.54E-16 2.00E-14 5.00E-15 3.35E-16 9.00E-13 2.25E-13 6.25E-15 6.00E-13 1.50E-13 3/29/2004 1.00E-16 9.00E-14 ·2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 6/27/2004 LOOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-l6 9.00E-13 2.25E-13 3.04E-15 6.00E-13 1.50E-13 9/27/2004 LOOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.05E-14 6.00E-13 1.50E-13 12/27/2004 1.00E-16 9_00E-14 2_25E-14 1.00E-16 2_00£-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.59E-14 6_00E-13 1.50E-13 3/28/2005 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.42E-15 6.00E-13 1.50E-13 6/29/2005 1.00E-16 9.00E-14 2_25E-14 1.30E-16 2.00E-14 5.00E-15 1.20E-16 9.00E-13 2.25E-13 7.94E-15 6.00E-13 1.50E-13 9/26/2005 1.00E-16 9.00E-14 2.25E-14 2.56E-16 2.00E-14 5.00E-15 2.42E-16 9.00E-13 2.25E-13 1.22E-14 6.00E-13 1.50E-13 1/3/2006 2.13E-16 9.00E-14 2.25E-14 1.04E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.73E-14 6.00E-13 1.50E-13 4/3/2006 1.62E-16 9.00E-14 2.25E-14 1.86E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.36E-15 6.00E-13 1.50E-13 7/3/2006 1.86E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.77E-15 6.00E-13 1.50E-13 10/2/2006 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25£-13 1.30E-14 6.00E-13 1_50E-13 1/1/2007 1.00E-16 9.00E-14 2.25E-14 1.47E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.17E-14 6.00E-13 1.50E-13 4/2/2007 2.23E-16 9.00E-14 2.25E-14 1.63E-16 2_00E-14 S.00E-15 1.00E-16 9.00E-13 2.25E-13 1.65E-14 6.00E-13 1.50E-13 7/2/2007 3.35E-16 9.00E-14 2.25E-14 1.34E-16 2.00E-14 5.00E-15 1.36E-16 9.00E-13 2.25E-13 1.78E-14 6.00E-13 1.50E-13 9/30/2007 1.15E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.68E-15 6.00E-13 1.50E-13 12/31/2007 1.00E-16 9.00E-14 2.25E-14 1.93E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 3/31/2008 1.14E-16 9.00E-14 2.25E-14 1.13E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13 6/30/2008 7.09E-16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 5.00E-15 2.27E-16 9.00E-13 2.25E-13 6.52E-15 6.00E-13 ... 1.50E-13 Date Effluent Concentration limit = 9E-14 uCi/ml BHV-1U Effluent Concentration limit -2E-14 uCi/ml BHV-1T effluent Concentration limit = 9E-13 uCi/ml BHV-1R Effluent Concentration limit = 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.25E-14 uCi/ml ALARAGoal = 5E-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal-1.5E-13 uCi/ml Pre 1994 MPC limit = 5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 7.69E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 5.00E-15 1.90E-16 9.00E-13 2.25E-13 7.64E-15 6.00E-13 1.50E-13 12/31/200S 1.21E-15 9.00E-14 2.25E-14 4.76E-16 2.00E-14 S.00E-15 3.34E-16 9.00E-13 2.25E-13 1.16[-14 6.00E-13 1.50E-13 3/15/2009 2.14E-15 9.00E-14 2.2SE-14 1.02E-1S 2.00E-14 S.00E-15 1.00E-15 9.00E-13 2.2SE-13 4.44E-15 6.00E-13 1.50E-13 6/15/2009 5.97E-17 9.00E-14 2.25E-14 2.35E-16 2.00E-14 S.00E-15 2.1SE-16 9.00E-13 2.2SE-13 5.13E-15 6.00E-13 1.50E-13 9/15/2009 9.55E-16 9.00E-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 9.87E-17 9.00E-13 2.25E-13 9.47E-15 6.00E-13 1.50E-13 12/15/2009 1.24E-15 9.00E-14 2.25E-14 9.25E·17 2.00E·14 5.00E-15 5.60E-17 9.00E-13 2.25E-13 5.95E-1S 6.00E-13 1.50E-13 3/31/2010 1.97E-15 9.00E-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 3.27E-16 9.00E-13 2.25E-13 1.00E-14 6.00E-13 1.50E-13 6/3012010 1.5SE-15 9.00E-14 2.25E-14 4.71E-16 2.00E-14 5.00E-15 7.70E-16 9.00E-13 2.25E-13 4.07E-15 6.00E-13 1.50E-13 9/30/2010 8.42E-16 9.00E-14 2.25E-14 2.S0E-16 2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 6.80E-15 6.00E-13 1.50E-13 12/31/2010 1.27E-15 9.00E-14 2.25E-14 2.32E-16 2.00E-14 S.00E-15 2.30E-16 9.00E-13 2.25E-13 1.27E-14 6.00E-13 1.50E-13 4/4/2011 9.01E-16 9.00E-14 2.25E-14 1.90E-16 2.00E-14 5.00E-15 3.64E-16 9.00E-13 2.25E-13 1.09E-14 6.00E-13 1.50E-13 7/4/201 ~ ~.:!.5 ~14 2.25E-14 5.31E-16 2.00E-14 S.00E-15 4.99E-16 9.00E-13 2.25E-13 8.3SE-15 6.00E-13 1.50E-13 ---- III C o ~ ... c CD (.) C o o CD 'C (.) ::::J C o 'C CO a: ,.... :> J: m C\I C') .-.- I I W W 0 0 C! q .-.- J. • ~ ~ 1'-:::: -.. ~ ..c:: ~ • ~ .:: ~ ~ ::::::: ~ Ir:: ::; ;:::: «:: .....-. ~ F-. ~ II;:; ~ ~ :=::.. -, ~ ~ t I. k:" ---4 ~. "'f:::: ~ .~ v .-I W 0 q -,..;~ ~ .:: ~ :. ~ t..- o~-das so-das • -.. ~ ..... M~ so-das ~ ..... ~ ~ -.; LO-daS 90-daS go-das vo-das .... ... ::;.. 80-daS 0 .-• ~ :::0. ..... -.. ~ ~ ~ ~ ... ........ ""~,~ ~ ~ ~ ~ ~ ~ ~ 6oc::: ~~ C\I Go-das I "0 CIS Q) ~o-das -.J + oo-daS ss-das co C\I C\I I ss-das E ::J '6 LS-daS CIS a:: 9s-das + IU '! t --" 9S-daS 0 C') C\I --~ ~1Ir" vs-das I E ::J • • ~ ~ ~ .. ~. "4 8S-daS "C a ..t: I- GS-daS + ~s-das (ij At-:: .. ~ OS-das "-::J ro ~ r.... ~ ~ ~. ::>I 1 r-:- bt ~ """" • ss-das z E ss-das "~ c:: CIS "- LS-das ::J + 9S-das r. -"'r:-r----. ~ gS-daS vs-das ~ ...... ..... • -8S-das iJ :;, Gs-das -~ """ ~s-das LO co t--co .-.-.-.- I I I I W W W W 0 0 0 0 q q q q .-.-.-.- (ale~s 501) 1.00E-11 1.00E-12 1.00E-13 m (ij u (f)1.00E-14 01 o ....J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml BHV-1 Uranium-Natural Concentrations (uCi/ml) Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCilml ...... t ~ I¥ ,.... co 6. (1) (f) \11 • C\J C') co co I I c.. c.. (l) (1) (f) (f) ¥ "<t co 6. (1) (f) .,. LO co I c.. (l) (f) 1\ ~ J..\.. PI 'l ~ CD co 6. (1) (f) r-.... co 6. (1) (f) co co I c.. (l) (f) 0> co I c.. (1) (f) T\ ., o 0> 6. (1) (f) • .,. V"t .A ..... I I~· ,.... 0> I c.. (l) (f) C\J 0> 6. (1) (f) C') 0> 6. (l) (f) W "<t 0> I c.. (1) (f) LO 0> 6. (1) (f) \ Y +_ .Al~ \ T V CD 0> I c.. (l) (f) r-.... 0> I c.. (1) (f) V I "1£ co 0> 6. (l) (f) ~ 0> 0> I c.. (l) (f) • t I~ l\ l' • VV o o I c.. (1) (f) ,.... o I c.. (1) (f) J\ C\J o I c.. (l) (f) , C') o I c.. (l) (f) "<t o I c.. (1) (f) _. .... J j~ ~ , LO o I c.. (l) (f) CD o I c.. (1) (f) r-.... o I c.. (l) (f) , co o I c.. (l) (f) ""') , 0> o I c.. (l) (f) o ,.... I c.. (1) (f) 1.00E-12 1.00E-13 1.00E-14 w Cii u U)1.00E-1S OJ o ~ 1.00E-16 1.00E-17 1.00E-18 T""" ex> , 0. Q) U) Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = SE-14uCi/ml .... T \ \ C\l ex> , 0. Q) U) • ~ f). t j J \ t . .,. • • , .... ~ I I 1 J , J ~ C') ex> , 0. Q) UJ , """ LO ex> ex> , , 0. 0. Q) Q) U) U) co ex> , 0. Q) U) t--ex> 6.. Q) U) ex> ex> , 0. Q) U) ~ \ ~ 0) ex> , 0. Q) U) o 0) , 0. Q) U) T""" 0) , 0. Q) UJ ~ • C\l 0) , 0. Q) U) .<Ii. , C') 0) , 0. Q) U) 1 It ~\ """ 0) 6.. Q) U) BHV-1 Thorium-230 Concentrations (uCi/ml) i n ~ " , \I • LO 0) , 0. Q) U) , r+ co 0) ~ 6.. Q) U) 1 t--0) 6.. Q) U) ~ J[ V\ T ex> 0) 6.. Q) U) ~ 0) 0) 6.. Q) U) • , I • 1\ \ + I\t t ~~ \,j \1V~ )'AM o o 6.. Q) U) T""" o , 0. Q) U) ~ , 0. Q) U) C') o , 0. Q) U) """ o , 0. Q) U) LO o 6.. Q) U) co o 6.. Q) U) t--o 6.. Q) U) T "II" N . 1\ I , .... ~ J. ~J ex> o 6.. Q) U) V 0) o 6.. Q) U) o 6.. Q) U) ... 1.00E-11 1.00E-12 1.00E-13 .--1.00E-14 <Ll «i u Cf) 0> o ...J -1.00E-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml • f"\ IN\ 't t ~ ... ..... co , a. <Ll Cf) & , I • C\I (Y) co co , , a. a. <Ll <Ll Cf) Cf) • • V "<t LO co co co co , , , a. a. a. <Ll <Ll <Ll Cf) Cf) Cf) ~ r--. co , a. <Ll Cf) co co , a. <Ll Cf) ~ 'II 0) co , a. <Ll Cf) • a 0) , a. <Ll Cf) lr • ..... 0) C. <Ll Cf) i C\I 0) C. <Ll Cf) (Y) 0) , a. <Ll Cf) \ , '- T"\ "<t 0) , \ a. <Ll Cf) BHV-1 Radium-226 Concentrations (uCi/ml) • LO 0) , jI a. <Ll Cf) , " .J V \ .-~ V co 0) C. <Ll Cf) r--. 0) C. <Ll Cf) co 0) C. <Ll Cf) 0) 0) , a. <Ll Cf) .. • J \ \ . 1\ ~ ¥ V\"'}J~ a a , a. <Ll Cf) ..... a , a. <Ll Cf) C\I a C. <Ll Cf) (Y) a C. <Ll Cf) "<t a , a. <Ll Cf) * j\ LO a , a. <Ll Cf) co a , a. <Ll Cf) • .1. Jt j" \ r--. a C. <Ll Cf) co a C. <Ll Cf) 0) a , a. <Ll Cf) " • ¥' a ..... , a. <Ll Cf) l' III C o ~ -c CD (,) C o CJ o ,.... ~ 'tJ CO CD ...J ,.... :> J: m ..... I UJ 0 q I"'" C\J C") ,-,- I I UJ UJ 0 0 q q J. 1:0 • ~ « ~ ""'r:: ~ 1«; -9c:: ~ 1==. ~ ~ , ~ ~ • ~ t ~ ~ ~ ~ 1.:::::- ~f:; ~ p I.: h I ~ r-.. ~ ~ ~ b. -, .... ~ r I. k:" ~ -~ .. ;;;,. r; '>t ..... W 0 q (eleos 601) - -. U') CD ..... ,- I I UJ UJ 0 0 q q ..... - . ,..... ,.... I UJ 0 q ,.... o~-des 60-deS so-des La-des 90-deS so-des "!la-deS £o-deS Go-des ~o-des OO-deS 66-deS ss-des LS-deS 9s-des ss-daS "!ls-des £S-daS GS-deS ~6-das os-des 6S-deS ss-des Ls-das 9S-deS ss-das "!ls-des £s-das Gs-deS ~s-das TAB 2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ZT Effluent Concentration Limit = 9E-13 uCi/ml lIHV-ZR Effluent Concentration Limit = 6E-13 uCi/ml BHV-ZPB ALARAGoal= 2.ZSE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= ;Z.ZSE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = 5E-UuCi/ml Pre 1994 MPC Limit -8E-14 uCi/ml Pre 1994 MPC Limit = ZE-UuCi/ml Pre 1994 MPC Limit = 4E-1Z uCi/ml Pre 1994 ALARA GOAL = 1.ZSE-1Z uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-UuCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.39E-1S S.OOE-12 l.2SE-12 3.69E-16 8.00E-14 2.00E-14 5.92E-16 2.00E-12 5.00E-13 1.67E-14 4.00E-12 1.00E-12 12/14/1981 4_62E-16 5.00E-12 1.2SE-12 8.03E-16 8.00E-14 2.00E-14 3.62E-16 .2.00E-12 S.OOE-13 l.33E-14 4.00E-12 1.00E-12 3/29/1982 7.07E-16 S.OOE-12 1.2SE-12 l.lOE-1S 8.00E-14 2.00E-14 7.27E-16 2.00E-12 5.00E-13 1.S2E-14 4.00E-12 1.00E-12 6/30/1982 8.84E-16 S.OOE-12 1.2SE-12 7.73E-16 8.00E-14 2.00E-14 4.78E-16 2.00E-12 5.00E-13 1.98E-14 4.00E-12 1.00E-12 9/27/1982 1.23E-1s 5.00E-12 1.2sE-12 3.60E-16 8.00E-14 2.00E-14 8.73E-16 2.00E-12 5.00E-13 2.3sE-14 4.00E-12 1.00E-12 1/3/1983 2.64E-1s 5.00E-12 1.2SE-12 2.SSE-16 8.00E-14 ~.00E-14 1.98E-16 2.00E-12 S.OOE-13 2.8SE-14 4.00E-12 1.00E-12 4/4/1983 :2.14E-16 5.00E-12 1.2SE-12 1.02E-16 8.00E-14 2.00E-14 1.S7E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 I 6/30/1983 2·85E-16 5.00E-12 1.25E-12 2.06E-16 8.00E-14 2.00E-14 2.24E-16 2.00E-12 s.OOE-13 1.79E-14 4.00E-12 1.00E-12 10/3/1983 2.70E-16 5.00E-12 1.2SE-12 3.36E-16 8.00E-14 2.00E-14 4.37E-16 2.00E-12 5.00E-13 1.78E-14 4.00E-12 1.00E-12 1/3/1984 2.78E-1s 5.00E-12 1.25E-12 1.20E-16 8.00E-14 2.00E-14 6.64E-17 2.00E-12 s.OOE-13 9.14E-15 4.00E-12 1.00E-12 4/2/1984 4.28E-16 5.00E-12 1.25E-12 1.7sE-16 8.00E-14 2.00E-14 4.57E-17 2.00E·12 s.OOE-13 3.55E-14 4.00E-12 1.00E-12 7/2/1984 2.78E-15 s.00E-12 1.25E-12 8.12E-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 5.00E-13 1.68E-14 4.00E-12 1.00E-12 10/1/1984 2.69E-16 s.OOE-12 1.2SE-12 2.66E-17 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 s.OOE-13 1.77E-14 4.00E-12 1.00E-12 1/2/1985 2.15E-16 5.00E-12 1.25E-12 7.55E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 5.00E-13 3.19E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 5.00E-12 1.25E-12 1.67E-16 8.00E-14 2.00E-14 6.75E-17 2.00E-12 5.00E-13 7.56E-15 4.00E-12 1.00E-12 7/1/1985 3.70E-17 S.OOE-12 1.2sE-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 S.OOE-13 1.31E-14 4.00E-12 1.00E-12 9/30/1985 9.32E-17 5.00E-12 1.25E-12 2.18E-16 B.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.64E-15 4.00E-12 1.00E-12 1/2/1986 1.00E-16 5.00E-12 1.25E-12 2.16E-16 8.00E-14 2.00E-14 2.1SE-17 2.00E-12 5.00E-13 3.04E-16 4.00E-12 1.00E-12 4/1/1986 1.31E-15 5.00E-12 1.2sE-12 1.50E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 2.90E-15 4.00E-12 1.00E-12 6/30/1986 2.23E-16 5.00E-12 1.2SE-12 1.32E-16 8.00E-14 2.00E-14 7.09E-17 2.00E-12 S.OOE-13 2.s3E-14 4.00E-12 1.00E-12 10/27/1986 6A1E-16 5.00E-12 1.2SE-12 1.74E-16 8.00E-14 2.00E-14 3.67E-16 2.00E-12 s.OOE-13 1.04E-14 4.00E-12 1.00E-12 12/15/1986 3.56E-16 s.OOE-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.05E-16 2.00E-12 s.OOE-13 '7.81E-1s 4.00E-12 1.00E-12 3/16/1987 5.31E-16 s.00E-12 1.25E-12 l.30E-16 8.00E-14 2.00E-14 7.74E-17 2.00E-12 s.OOE-13 3.80E-14 4.00E-12 1.00E-12 S/11/1987 4.06E-16 s.OOE-12 1.25E-12 6.63E-17 8.00E-14 2.00E-14 1.34E-16 2.00E-12 5.0DE-13 1.10E-14 4.00E-12 1.0DE-12 9/9/1987 2.74E-16 S.OOE-12 1.2sE-12 2.38E-16 8.00E-14 2.00E-14 1.38E-16 2.00E-12 s.OOE-13 1.04E-14 4.0DE-12 1.00E-12 11/2/1987 3.73E-16 S.OOE-12 l.25E-12 3.11E-16 8.00E-14 2.00E-14 1.83E-16 2.00E-12 S.OOE-13 1.17E-14 4.00E-12 1.00E-12 2/16/1988 2.78E-1S 5.0DE-12 1.2sE-12 2.31E-17 8.00E-14 2.00E-14 1.20E-16 2.00E-12 S.OOE-13 3.SSE-14 4.00E-12 1.00E-12 5/18/1988 4.63E-16 S.DDE-12 1.25E-12 1.49E-16 8.00E-14 2.00E-14 2.3DE-16 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 1.0DE-12 8/15/1988 8.06E-16 5.00E-12 1.2sE-12 8.69E-16 8.00E-14 2.0DE-14 1.8DE-16 2.00E-12 5.0DE-13 1.42E-14 4.00E-12 1.00E-12 11/14/1988 4.34E-16 S.ODE-12 1.25E-12 6.76E-16 8.00E-14 2.DOE-14 1.57E-16 2.0DE-12 S.DOE-13 2.2SE-14 4.00E-12 1.00E-12 2/13/1989 5.80E-16 s.OOE-12 1.25E-12 2.8SE-16 8.00E-14 2.DOE-14 1.55E-16 2.00E-12 S.DOE-13 2.8DE-14 4.00E-12 1.00E-12 5/15/1989 s.06E-16 5.0DE-12 1.2SE-12 2.28E-16 8.DDE-14 2.00E-14 1.63E-16 2.00E-12 5.00E-13 6.0SE-15 4.00E-12 1.00E-12 8/14/1989 4.71E-16 5.00E-12 1.2SE-12 9.60E-16 8.00E-14 2.00E-14 1.26E-1S 2.00E-12 S.OOE-13 6.65E-1s 4.00E-12 1.00E-12 11/13/1989 1.l4E-1S S.OOE-12 1.2SE-12 4.08E-16 8.00E-14 2.00E-14 4.18E-16 2.00E-12 s.OOE-13 1.59E-14 4.00E-12 1.00E-12 2/12/1990 1.09E-1S s.OOE-12 1.2SE-12 3.2SE-16 8.00E-14 2.00E-14 3.74E-16 2.00E-12 S.OOE-13 1.98E-14 4.00E-12 1.00E-12 5/14/1990 9.32E-16 S.OOE·12 1.2SE-12 S.27E-16 8.00E-14 2.00E-14 3.97E-16 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 1.00E-12 8/13/1990 1.66E·16 s.00E-12 1.2SE-12 S.49E-16 8.00E-14 2.00E-14 4.7sE-17 2.00E-12 S.OOE-13 1.27E-15 4.00E-12 1.00E-12 11/12/1990 6.0SE-16 s.00E-12 1.2SE-12 2.64E-16 8.00E-14 2.00E-14 1.93E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 1.00E-12 2/11/1991 8.nE-17 5.00E-12 1.25E-12 7.00E-18 8.00E-14 2.00E-14 3.33E-17 2.00E-12 5.00E-13 3.49E-14 4.00E-12 1.00E-12 5/13/1991 1.16E-16 S.OOE-12 1.25E-12 3.86E-16 8.00E-14 2.00E-14 2.80E-16 2.00E-12 5.00E-13 1.50E-14 4.00E-12 1.00E-12 8/12/1991 9.02E-17 S.OOE-12 1.25E-12 8.82E-17 8.00E-14 2.00E-14 7.6SE-17 2.00E-12 S.OOE-13 l.S8E-14 4.00E-12 1.00E-12 11/11/1991 4.81E-17 S.OOE-12 1.25E-12 3.82E-17 8.00E-14 2.00E-14 2.S4E-17 2.00E-12 S.OOE-13 1.4SE-14 4.00E-12 1.00E-12 2/10/1992 1.S4E-16 S.00E-12 1.2SE-12 6.82E-17 S.00E-14 2.00E-14 1.40E-17 2.00E-12 S.OOE-13 3A1E-14 4.00E-12 1.00E-12 5/11/1992 2.38E-16 S.00E-12 1.2SE-12 7.63E-17 8.00E-14 2.00E-14 3.07E-17 2.00E-12 S.OOE-13 1.27E-14 4.00E-12 1.00E-12 8/10/1992 1.01E-16 S.00E-12 1.2SE-12 7.07E-17 8.00E-14 2.00E-14 2.80E-17 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 1.00E-12 11/9/1992 S.20E-17 S.00E-12 1.2SE-12 3.6SE-17 8.00E-14 2.00E-14 l.7SE-17 2.00E-12 S.OOE-13 1.71E-14 4.00E-12 1.00E-12 2/9/1993 2.39E-16 s.00E-12 1.2SE-12 2.97E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 1.00E-12 5/10/1993 1.00E-16 s.OOE-12 1.2SE-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 5.00£-13 1.34E-14 4.00E-12 1.00E-12 8/10/1993 1.90E-16 s.OOE-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.80E-14 4.00E-12 1.00E-12 11/8/1993 1.00E-16 S.00E-12 1.25£-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.49E-14 4.00E-12 1.00E-12 2/7/1994 2.23E-16 S.OOE-12 1.2SE-12 1.00£-16 8.00E-14 2.00E-14 1.84£-16 2.00£-12 6.00£-13 2.19E-14 4.00E-12 1.00E-12 5/9/1994 2.i6E-16 5.00E-12 1.2SE-12 7.20E-17 8.00E-14 2.00E-14 9.89E-17 2.00E-12 5.00E-13 1.37E-14 4.00E-12 1.00E-12 8/9/1994 9.29E-17 S.OOE-12 1.2SE-12 2.96E-16 8.00E-14 2.00E-14 3.04E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.21E-17 5.00E-12 1.2SE-12 2.3SE-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit = ZE-14 uCi/ml BHV-ZT Effluent Concentration Limit = 9E-13 uCi/ml BHV-ZR Effluent Concentration Limit = 6E-13 uCi/ml BHV-ZPB I ALARAGoal = Z.Z5E-14 uCi/ml ALARAGoal = .SE-13 uCi/ml ALARAGoal = Z.ZSE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml I Pre 1994 MPC Limit = SE-lZ uCi/ml Pre 1994, MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = ZE-1Z uCi/ml Pre 1994 MPC limit" 4E-1Z uCi/ml Pre 1994 ALARA GOAL -1.ZSE-1Z uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-lZ uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.18E-16 9_00E-14 2.2SE-14 9.70E-17 2.00E-14 S.00E-15 9.70E-17 9.00E-13 2.2SE-13 7.42E-1S 6_00E-13 l.SOE-13 5/9/1995 9.40E-17 9.00E-14 2.2SE-14 1.20E-16 2.00E-14 S.00E-1S 3.S0E-16 9.00E-13 2.2SE-13 3.90E-1S 6.00E-13 1.S0E-13 8/9/1995 8.90E-17 9.00E-14 2.2SE-14 9.67E-17 2.00E-14 S.00E-1S l.3SE-16 9.00E-13 2.2SE-13 2.38E-16 6.00E-13 l.SOE-13 11/11/1995 2.83E-1S 9.00E-14 2.2SE-14 4.09E-16 2.00E-14 S.00E-1S S.23E-16 9.00E-13 2.2SE-13 6.77E-1S 6.00E-13 l.SOE-13 2/5/1996 1.7SE-1S 9.00E-14 2.2SE-14 8.66E-16 2.00E-14 S.00E-1S 4.86E-16 9.00E-13 2.2SE-13 a.SOE-1S 6.00E-13 l.SOE-13 5/6/1996 1.40E-16 9.00E-14 .2.2SE-14 1.1SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.8SE-1S 6.00E-13 l.SOE-13 8/5/1996 1A3E-16 9.00E-14 2.2SE-14 2.78E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.83E-1S 6.00E-13 l.S0E-13 11/6/1996 lASE-16 9.00E-14 2.2SE-14 l.S7E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.19E-14 6.00E-13 l.S0E-13 2/6/1997 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 5.84E-16 6.00E-13 l.S0E-13 5/5/1997 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.89E-1S 6.00E-13 l.S0E-13 8/11/1997 1.00E-16 9.00E-14 2.2SE-14 1.09E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 5.69E-1S 6.00E-13 l.S0E-13 1/5/1998 2.5SE-16 9.00E-14 2.2SE-14 1.07E-16 2.00E-14 S.00E-1S S.00E-17 9.00E-13 2.2SE-13 5_11E-1S 6.00E-13 l.SOE-13 4/28/1998 1.20E-16 9.00E-14 2.2SE-14 1.71E-16 2,00E-14 S.00E-1S 1.28E-16 9.00E-13 .2.2SE-13 6AOE-1S 6.00E-13 l.S0E-13 7/31/1998 1.47E-16 9.00E-14 2.2SE-14 4.24E-16 2.00E-14 S.00E-1S 3.39E-16 9.00E-13 2.2SE-13 4.80E-1S 6_00E-13 l.S0E-13 9/28/1998 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E·13 .2.2SE-13 4.26E-1S 6.00E-13 l.SOE-13 12/28/1998 2.S4E-16 9.00E·14 2.2SE-14 2.1SE-16 2.00E-14 S.00E-1S 1.38E-16 9.00E-13 2.2SE-13 G.88E-1S 6.00E-13 l.S0E-13 3/29/1999 1.07E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 .2.2SE-13 7.61E-1S 6.00E-13 l.SOE-13 7/3/1999 2.46E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 l.S0E-13 9/27/1999 2.81E-16 9.00E-14 2.2SE-14 1.41E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2_2SE-13 7.3SE-1S 6.00E-13 l.SOE-13 12/2S/1999 S.20E-16 9.00E-14 2.2SE-14 2.60E-16 2.00E-14 S.00E-1S 2.01E-16 9.00E-13 2.2SE-13 7.00E-1S 6.00E-13 1.S0E-13 3/27/2000 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2_2SE-13 7.12E-1S 6.00E-13 l.S0E-13 6/26/2000 1.1OE-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.16E-16 9.00E-13 2.2SE-13 S.07E-1S 6.00E-13 l,sOE-13 9/26/2000 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.31E-1S 6.00E-13 l.S0E-13 12/26/2000 1.26E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.4SE-1S 6.00E-13 l.S0E-13 3/26/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 1.50E-13 7/2/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.S6E-1S 6.00E-13 1.S0E-13 9/24/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 .5.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.16E-1S 6.00E-13 1.S0E-13 12/31/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 2.20E-1S 6.00E-13 1.S0E-13 4/1/2002 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.9SE-1S 6.00E-13 1.S0E-13 7/1/2002 1.2SE-16 9.00E-14 2.2SE-14 1.43E-16 2.00E-14 5.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.2SE-1S 6.00E-13 1.S0E-13 9/30/2002 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.69E-1S 6.00E-13 1.S0E-13 12/30/2002 1.00E-16 9_00E-14 2.2SE-14 1.00E-16 2.00E-14 5.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.91E-1S 6.00E-13 1.S0E-13 3/31/2003 1.00E-16 9_00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.16E-1S 6.00E-13 1.50E-13 6/30/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9_00E-13 2.2SE-13 S.27E-1S 6.00E-13 1.50E-13 9/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 5.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.23E-1S 6.00E-13 l.SOE-13 12/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.S0E-1S 6.00E-13 1.50E-13 3/29/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 5_00E-1S 1.00E-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 l.S0E-13 6/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.09E-1S 6.00E-13 l.S0E-13 9/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 5.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.73E-14 6.00E-13 1.S0E-13 12/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.30E-14 6_00E-13 1.S0E-13 3/2S/200S 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S_00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.S8E-1S 6.00E-13 1.S0E-13 6/29/2005 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.SSE-1S 6_00E-13 1.S0E-13 9/26/200S 1.00E-16 9.00E-14 2.2SE-14 1.99E-16 2.00E-14 S.00E-1S 1.44E-16 9.00E-13 2.2SE-13 3.S1E-14 6.00E-13 l.S0E-13 1/3/2006 1.29E-16 9.00E-14 2.2SE-14 .1.00E-16 2.00E-14 S.00E-1S 4.0SE-16 9.00E-13 2.2SE-13 6.SSE-14 6.00E-13 l.SOE-13 4/3/2006 1.02E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.0SE-14 6.00E-13 l.S0E-13 7/3/2006 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 10/2/2006 1.30E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.6SE-14 6.00E-13 l.S0E-13 1/1/2007 1.24E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.3SE-14 6.00E-13 l.SOE-13 4/2/2007 1.40E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.63E-14 6.00E-13 l.SOE-13 7/2/2007 1.04E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.36E-14 6.00E-13 l.S0E-13 9/30/2007 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.24E-1S 6.00E-13 l.SOE-13 12/31/2007 1.91E-16 9.00E-14 .2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.18E-14 6.00E-13 1.SOE-13 3/30/2008 1.00E-16 9.00E-14 .2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.49E-1S 6.00E-13 l.S0E-13 6/30/200S .1.29E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S :1.00E-16 9.00E-13 2.2SE-13 4.82E-1S 6.00E-13 1.S0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration limit = 9E-13 uCi/ml BHV-2R Effluent Concentration limit = 6E-13 uCi/ml BHV-2PB ALARAGoal= 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCiJml ALARAGoal= 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-UuCi/ml Pte 1'394 MPC Limit " 8E-14 uCi/ml Pre 1994 MPC Limit-2E-12 uCi/ml Pre 1994 MPC Limit = 4E-UuCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 9/30/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 12/31/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 5.00E-15 1.07E-16 9.00E-13 2.25E-13 4.81E-15 6.00E-13 1.50E-13 6/15/2009 1.24E-17 9.00E-14 2.25E-14 4.64E-17 2.00E-14 5.00E-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 6.00E-13 1.50E-13 9/15/2009 2.43E-16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 5.00E-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 12/15/2009 .5.72E-16 9.00E-14 2.25E-14 2.94E-17 2.00E-14 5.00E-15 2.57E-17 9.00E-13 2.25E-13 6.70E-15 6.00E-13 1.50E-13 3/31/2010 5.47E-16 9.00E-14 2.25E-14 1.42E-17 2.00E-14 5.00E-15 4.66E-17 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 6/30/2010 3.58E-16 9.00E-14 2.25E-14 6.64E-17 2.00E-14 5.00E-15 9.90E-17 9.00E-13 2.25E-13 2.01E-15 6.00E-13 1.50E-13 9/30/2010 2.91E-16 9.00E-14 2.25E-14 4.48E-17 2.00E-14 5.00E-15 5.72E-17 9.00E-13 2.25E-13 1.08E-15 6.00E-13 1.50E-13 12/31/2010 5.73E-16 9.00E-14 2.25E-14 7.24E-17 2.00E-14 5.00E-15 6.76E-17 9.00E-13 2.25E-13 1.35E-14 6.00E-13 1.50E-13 4/4/2011 3.79E-16 9.00E-14 2.25E-14 4.01E-17 2.00E-14 5.00E-15 9.11E-17 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 7/4/2011 3.07E-16 9.00E-14 2.25E-14 8.54E-17 2.00E-14 5.00E-15 9_21E-17 9.00E-13 2.25E-13 7.21E-15 6.00E-13 1.50E-13 I/) c:: o i lo., ... c:: Q) CJ c:: o u Q) "C -CJ ::J c:: o :.a «S II: N :> ::I: [Q C\I .-I w a ~ ... I. • • • ~ I.. (V') .- I w a ~ ~ • i L -=:::::::: • • ? ~ i =::::: -:::: ~ ~ ~ F=.. i) I .... ,.........A -!':::::: , b::::: ~ r ~ "<t .- I w a ~ ,~ ::> ~ .,. • o~-das :ooe ~~ t 'Y 60-daS I). ~ ~ - so-das LO-daS 90-daS -4 OC:r--, ~ go-das vo-das 80-daS a .-C\I I ,. ~ GO-daS -0 t1l Q) r-t=oI - ~ ... b: I)' .. ~ ~" 1'-: ~ • Itc== ~ ~o-das -l + OO-daS CD 66-deS C\I C\I I S6-deS E ::J '0 L6-deS t1l a: 96-deS + ,.... ~L'!" .. ~ "« =-. 96-deS a (V') C\I v6-deS I E ::J 4:? 86-deS ".: 0 £ .. ..;;>I ~-• • ~ ~r: ~ ..... I- G6-deS + ~6-des (ij 06-des .... ::J -J ,. ~ ~ ~'-' - t1l 6S-deS z E ::J ss-des c t1l 1 -::. ~~ ~ - ..... LS-deS ::J + 9s-des 9S-deS -vs-das .......... • "'I: L 8s-das ,..... r--... ~ .-.. -• • Gs-des ~s-des LO CD I'-<X) .-.-. W W . w W a a a a ~ ~ ~ ~ .-.- (el8os 6Ol) 1.00E-11 1.00E-12 1.00E-13 Q) (ij u U)1.00E-14 Cl o ....J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCilml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml ~ ~ , .. I. 'In.. 1/. ,,. Jr ~ Ii • \I .... \ • 1* f\ rw\. ,.... co 6.. Q) U) ~ I a. Q) U) C') co I a. Q) U) v co 6.. Q) U) .. li) co I a. Q) U) <D co 6.. Q) U) r--. co I a. Q) U) co co 6.. Q) U) 0> co 6.. Q) U) o 0> I a. Q) U) ,.... 0> 6.. Q) U) C\J 0> 6.. Q) U) C') 0> 6.. Q) U) v 0> 6.. Q) U) BHV-2 Uranium-Natural Concentrations (uCilml) It.. '~ li) 0> 6.. Q) U) I ~ t' "\ JWV <D 0> 6.. Q) U) r--. 0> 6.. Q) U) co 0> I a. Q) U) 0> 0> 6.. Q) U) l6A o o 6.. Q) U) ,.... o I a. Q) U) .A. C\J o 6.. Q) U) , C') o 6.. Q) U) v o I a. Q) U) ~ li) o 6.. Q) U) <D o I a. Q) U) r--. o I a. Q) U) co o 6.. Q) U) I , \ '"' ~ T 0> o 6.. Q) U) o ,.... I a. Q) U) - en c o ",e::o cu ... -c CI) () c o o o M ~ E ::::s "i: o .c l- N :::- J: III .-.- uJ o q C\I .-I UJ 0 q ... - 4 C') -.;t L{) .-,.... .- I I I UJ UJ UJ 0 0 0 q q q ,.... telEOS cOlf ... k «: ~ F;: ~~ ~ ~ ~ to::: ~ --. ~ ~ - j.- ""1;11 !--~ ~ r-; ~ ~ ~ ~ t-~ 14 ~ t> ~~ CD ,.... I UJ 0 q .- ..... po. , • r--.- I UJ 0 q .- - - - - - - CO .-I UJ 0 q o~-des 60-deS BO-deS La-des 90-deS go-des '\i'O-deS 80-deS Go-des ~o-des OO-deS 66-deS B6-deS L6-deS 96-deS 96-deS '\i'6-deS 86-des G6-deS ~6-des 06-deS 6B-des BB-des LB-deS 9B-deS SB-des '\i'B-deS 8B-daS GB-deS ~B-das ."",,-..... .. ,-C\l C") ~ LO ,-,-,-,- W I W I I w w W a a a a a ~ ~ ~ ~ ~ ,-(alB:>§" DOl) ~ ...... ~;.,... ........ < ~ ~ I·F -... .::::::: :::>+ -~~ ~ ~ ~.--- ~ ~. • ~ IP' F - ..- l- : ...... ~ ~ ~I-' CD W a ~ ,- ~ ... • i:04 -~r ~ .. • • ~ - I"- W a ~ ,- o~-das 60-das 80-daS LO-daS go-das so-das vo-das 80-das co-das W-daS oo-das 66-daS 86-das L6-daS 96-daS S6-daS v6-daS 86-daS c6-daS ~6-das 06-daS 68-daS B8-das La-daS 98-daS sa-das v8-daS 88-daS ca-das ~a-das -E =:::: o ::l -In C o :; ... ... c Q) u c o o o ""'" C}I "C ca Q) ..J N :> ::I: ED ,..-,..- W a ~ ...- C'J (t) ,..-...- I I W W a a ~ ~ J. J:> • r- « ~ ""F-j-.. 1«::;; -.-::: IJ ~ ~ ~ , , r-• ~ t tc: ~ ~ .~ • ~ tc::::; p It( It-- I ~r.. ~ ~~ b. ~ rs ~ , 14F::: ~ "f:: ~~ ~. ~ V ,..- I W a ~ (alBos DOl) - .... LO ...-I W a ~ ...- co ...-I W a ~ - t--,..- I W a ~ o~-das 60-daS so-das LO-daS 90-daS go-das vO-daS 80-daS GO-daS ~o-das OO-daS 66-das S6-daS L6-daS 96-das 96-daS v6-daS 86-daS G6-daS ~6-das 06-daS 6S-daS ss-das LS-daS 9S-daS gs-das vs-das 8S-daS Gs-daS ~s-das TAB 3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB I ALARAGoal= 2.25E-14 uCi/ml ALARAGoal= 5E-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml I Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.74£-15 5.00E·12 1.25E-12 9.02E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 5.00E-13 1.54E-14 4.00E-12 1.00E-12 12/14/1981 1.59E-15 5.00E-12 1.25E-12 5.03E-16 8.00E-14 2.00E-14 1.30E-16 2.00E-12 5.00E-13 2.25E-14 4.00E-12 1.00E-12 3/29/1982 3.76E-16 5.00E-12 1.25E-12 5.25E-16 8.00E-14 2.00E-14 4.08E-16 .2.00E-12 5.00E·13 1.96E-14 4.00E-12 1.00E-12 6/30/1982 ,3.83E-16 5.00E-12 1.25E-12 2.16E-16 8.00E-14 2.00E-14 1.41E-15 2.00E-12 s.ooe.-n 2.40E-14 4.00E-12 1.00E-12 9/27/1982 5.95E-16 5.00E-12 1.25E-12 1.44E-15 8.00E-14 2.00E-14 5.36E-16 2.00E-12 5.00E-13 1.43E-14 4.00E-12 1.00E-12 1/3/1983 2.05E-16 5.00E-12 1.25E-12 1.23E-16 8.00E-14 2.00E-14 1.10E-16 2.00E-12 5.00E-13 3.01E-14 4.00E-12 1.00E-12 4/4/1983 1.00E-16 5.00E-12 1.25E-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 5.00E-13 1.39E-14 4.00E-12 1.00E-12 6/30/1983 3.06E-16 5.00E-12 1.25E-12 9,59E-17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 5.00E-13 1.70E-14 4.00E-12 1.00E-12 10/3/1983 1.91E-16 5.00E-12 1.25E-12 3.05E-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 5.00E-13 1.76E-14 4.00E-12 1.00E-12 1/3/1984 3.01E-16 5.00E-12 1.25E-12 9.51E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 9.17E-15 4.00E-12 1.00E-12 4/2/1984 8.22E-16 5.00E-12 1.25E-12 7.52E-16 8.00E-14 2.00E-14 5.20E-17 2.00E-12 5.00E-13 3.47E-14 4.00E-12 1.00E-12 7/2/1984 5.29E-16 5.00E-12 1.25E-12 6.18E-16 8.00E-14 2.00E-14 1.40E-16 2.00E-12 5.00E-13 1.32E·14 4.00E-12 1.00E-12 10/1/1984 1.74E-16 5.00E-12 1.25E-12 7.10E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.08E-14 4.00E-12 1.00E-12 1/2/1985 1.00E-17 5.00E-12 1.25E-12 7.10E-17 8.00E-14 2.00E-14 7.80E-17 2.00E-12 5.00E-13 2.73E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 5.00E-12 1.25E-12 2.76E-16 8.00E-14 2.00E-14 4.10E-17 2.00E-12 5.00E-13 1.12E-14 4.00E-12 1.00E·12 7/1/1985 1.04E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.64E-14 4.00E-12 1.00E·12 9/30/1985 1.00E-16 5.00E-12 1.25E-12 LODE-IS 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.73E-14 4.00E-12 1.00E-12 1/2/1986 1.03E-15 5.00E-12 1.25E-12 3.17E-16 8.00E-14 2.00E-14 1.25E-16 2.00E-12 5.00E-13 1.21E-17 4.00E-12 1.00E-12 4/1/1986 8.04E-16 5.00E-12 1.25E-12 1.93E-17 8.00E-14 2.00E-14 1.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-12 1.00E-12 6/30/1986 4.29E·16 5.00E-12 1.25E-12 1.77E-16 8.00E-14 2.00E-14 2.83E-16 2.00E-12 5.00E-13 1.97E·14 4.00E-12 1.00E-12 10/27/1986 6.45E-16 5.00E-12 1.25E-12 9.89E-17 8.00E-14 2.00E-14 4.16E-15 2.00E-12 5.00E-13 1.64E-14 4.00E-12 1.00E-12 12/15/1986 1.31E-16 5.00E-12 1.25E-12 O.OOE+OO 8.00E-14 2.00E-14 4.16E-17 2.00E-12 5.00E-13 4.60E-15 4.00E-12 1.00E-12 3/16/1987 2.01E-16 5.00E-12 1.25E-12 1.20E-16 8.00E-14 2.00E-14 5.73E-17 2.00E-12 5.00E-13 1.60E-14 4.00E-12 1.00E-12 5/11/1987 2.16E-16 5.00E-12 1.25E-12 1.96E-16 8.00E-14 2.00E-14 7.38E-17 2.00E-12 5.00E-13 1.59E-14 4.00E-12 1.00E-12 9/9/1987 2.41E-16 5.00E-12 1.25E-12 2.18E-16 8.00E-14 2.00E-14 3.52E-17 2.00E-12 5.00E-13 1.46E-14 4.00E-12 1.00E-12 11/2/1987 2.44E-16 5.00E-12 1.25E-12 2.32E-16 8.00E-14 2.00E-14 2.37E-17 2.00E-12 5.00E-13 2.48E-14 4.00E-12 1.00E-12 2/16/1988 8.08E-16 5.00E-12 1.25E-12 2.55E-16 8.00E-14 2.00E-14 3.42E-16 2.00E-12 5.00E-13 5.61E-14 4.00E-12 1.00E-12 5/18/1988 1.14E-16 5.00E-12 1.25E-12 4.14E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 1.00E-12 8/15/1988 2.08E-16 5.00E-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 3.65E-17 2.00E-12 5.00E-13 1.36E-14 4.00E-12 1.00E-12 U/14/1988 4.21E-16 5.00E-12 1.25E-12 2.93E-16 8.00E-14 2.00E-14 1.09E-16 2.00E-12 5.00E-13 2.48E-14 4.00E-12 1.00E-12 2/13/1989 4.45E-16 5.00E-12 1.25E-12 4.78E-17 8.00E-14 2.00E-14 2.47E-17 2.00E-12 5.00E-13 3.34E-14 4.00E-12 1.00E-12 5/15/1989 1.05E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 2.45E-17 2.00E·12 5.00E-13 6.56E-15 4.00E-12 1.00E-12 8/14/1989 1.31E-16 5.00E-12 1.25E-12 5.85E-17 8.00E-14 2.00E-14 3.97E-17 2.00E-12 5.00E-13 6.75E-15 4.00E-12 1.00E-12 11/13/1989 1.67E-16 5.00E-12 1.25E-12 3.87E-17 8.00E-14 2.00E-14 8.03E-17 2.00E-12 5.00E-13 1.69E-14 4.00E-12 1.00E-12 2/12/1990 4.43E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 3.50E-17 2.00E-12 5.00E-13 2.37E-14 4.00E-12 1.00E-12 5/14/1990 3.84E-16 5.00E-12 1.25E-12 2.54E-16 8.00E-14 2.00E-14 1.02E-16 2.00E-12 5.00E-13 1.68E-14 4.00E-12 1.00E-12 8/13/1990 7.27E-17 5.00E-12 1.25E-12 2.87E-16 8.00E-14 2.00E-14 1.21E-17 2.00E-12 5.00E-13 7.86E-15 4.00E-12 1.00E-12 11/12/1990 1.84E-16 5.00E-12 1.25E-12 1.34E-16 8.00E-14 2.00E-14 8.53E-17 2.00E-12 5.00E-13 2.01E-14 4.00E-12 1.00E-12 2/11/1991 4.66E-17 5.00E-12 1.25E-12 8.48E-16 8.00E-14 2.00E-14 1.94E-17 2.00E-12 5.00E-13 3.69E-14 4.00E-12 1.00E-12 5/13/1991 5.05E-17 5.00E-12 1.25E-12 7.40E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 5.00E-13 1.50E-14 4.00E-12 1.00E-12 8/12/1991 7.14E-17 5.00E-12 1.25E-12 6.22E-17 I!.DOE-14 2.00E-14 7.95E-17 2.00E-12 5.00E·13 1.77E-14 4.00E·12 1.00E-12 11/11/1991 1.41E-17 5.00E-12 1.25E-12 2.19E-18 8.00E-14 2.00E-14 2.75E-17 2.00E-12 5.00E-13 1.18E-14 4.00E-12 1.00E-12 2/10/1992 8.12E-17 5.00E-12 1.25E-12 2.35E-17 8.00E-14 2.00E-14 2.76E-18 2.00E-12 5.00E-13 3.57E-14 4.00E-12 1.00E-12 5/11/1992 9.18E-17 .5.00E-12 1.25E-12 5.80E-17 8.00E-14 2.00E-14 3.36E-17 2.00E-12 5.00E-13 1.28E-14 4.00E-12 1.00E-12 8/10/1992 2.00E-18 5.00E-12 1.25E-12 4.19E-17 8.00E-14 2.00E-14 2.00E-18 2.00E-12 5.00E-13 1.59E-14 4.00E-12 1.00E-12 11/9/1992 4.00E-17 5.00E-12 1.25E-12 2.68E-17 8.00E-14 2.00E-14 1.07E-17 2.00E-12 5.00E-13 1.81E-14 4.00E-12 1.00E-12 2/9/l993 7.94E-17 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.09E-16 2.00E-12 5.00E-13 2.69E-14 4.00E-12 1.00E-12 5/10/1993 1.60E-17 5.00E-12 1.25E-12 5.07E-17 8.00E-14 l.00E-14 7.64E-17 2.00E-12 5.00E-13 1.26E-14 4.00E-12 1.00E-12 8/10/1993 6.00E-17 5.00E-12 1.25E-12 6.00E-18 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.50E-14 4.00E-12 1.00E-12 11f8{1993 1.00E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 2.10E-14 4.00E-12 1.00E-12 2/7/l994 1.61E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 5.00E-13 2.23E-14 4.00E-12 1.00E-12 5/9/1994 2.77E-16 5.00E-12 1.25E-12 2.80E-17 8.00E-14 2.00E-14 8.37E-18 2.00E-12 5.00E-13 1.40E-14 4.00E-12 1.00E-12 8/9/l994 7.39E-17 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.14E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.05E-17 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E·12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 - Date Effluent Concentration Limit -9E-14 uCi/mJ BHV-3U Effluent Concentration Limit = 2E-14 uCi/mJ BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.25E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml ALARAGoal = 2.25E-13 uCi/mJ ALARAGoal= 1.5E-13 uCi/mJ Pre 1994 MPC Limit ~ 5E-12 uCi/mJ Pre 1994 MPC Limit = 8E-14 uCi/mJ Pte 1994 MPC Limit = 2E-12 uCi/mJ Pre 1994 MPC Limit = 4E-12 uCi/mJ Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/mJ Pre 1994 ALARA GOAL = lE-12 uCi/mJ Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 2/7/1995 7.99E-17 9.00E-14 2.25E-14 9.60E-17 2.00E-14 5.00E-15 9.60E-17 9.00E-13 2.25E-13 9.05E-15 6.00E-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 9.S0E-17 2.00E-14 5.00E-15 8.60E-17 9.00E-13 2.25E-13 2.S8E-15 6.00E-13 1.50E-13 8/9/1995 7.30E-17 9.00E-14 2.25E-14 9.20E-17 2.00E-14 5.00E-15 4.40E-17 9.00E-13 2.25E-13 1.96E-15 6.00E-13 1.50E-13 11/11/1995 3.16E-16 9.00E-14 .2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.5SE-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 2/5/1996 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.1SE-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 S/6/1996 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/5/1996 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 11/6/1996 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E·14 5.00E·15 6.5SE·17 9.00E·13 2.25E·13 1.91E-14 6.00E-13 1.50E-13 2/6/1997 3.41E·16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.1SE-16 9.00E-13 2'25E-13 2.69E-14 6.00E-13 1.50E-13 $/5/1997 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/11/1997 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E·14 6.00E-13 1.50E-13 1/5/1998 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/28/1998 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E·13 7/31/1998 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E·14 6.00E-13 1.50E-13 9/28/1998 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E·13 1.31E-14 6.00E-13 1.50E·13 12/28/1998 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E·14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 8/29/1999 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5,00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/1999 1.31E-16 9.00E-14 '2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.S2E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/27/1999 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/28/1999 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E·13 1.91E-14 6.00E-13 1.50E-13 3/28/2000 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/26/2000 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/26/2000 3.00E-16 '.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/26/2000 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/26/2001 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2001 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/24/2001 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2001 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E·15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/1/2002 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/1/2002 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2002 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/30/2002 3.16E-16 9.00E-14 '2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.5SE-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2003 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 ;Z.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2003 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/29/2003 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/29/2003 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 '1.91E-14 6.00E-13 1.50E-13 3/29/2004 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/27/2004 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/27/2004 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/27/2004 3.16E-16 9.00E-14 2.25E-14 1.31E-16 ,2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/28/2005 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/29/2005 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/26/2005 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 1/3/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.5SE-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/3/2006 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.ISE-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/2006 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 10/2/2006 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 1/1/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/2/2007 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2007 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2007 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2007 3.16E-16 .9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2008 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2008 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 .9.00E-13 .2.25E-13 1.53E-14 6.00E-13 1.50E-13 - Date Effluent Concentration limit = 9E-14 uCi/ml BHV-3U Effluent Concentration limit = 2E-14 uCi/ml BHV-3T Effluent Concentration limit = 9E-13 uCi/ml BHV-3R Effluent Concentration limit -6E-13 uCi/ml BHV-3PB ALARAGoal-2.25E-14 uCi/ml ALARAGoal = 5E-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC limit = 5E-12 uCi/ml Pre 1994 IYIPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC Umit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2008 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/15/-2009 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/15/2009 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/15/2009 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/15/2009 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.00E-1S 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2010 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2010 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2010 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2010 3.16E-16 9.00E,14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/4/2011 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.ooE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/4/2011 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.ooE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 -- -:§ o ::s -In c: o :; '--c: CD (,) c: o o CD "C -(,) ::s c: o "C cu a: C") > :::J: ED C\I uJ 0 ~ ~F C') T"" I LlJ 0 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ L7 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ t> ~ ~ ~ 1 ~ ~ ~ ~f::: ~ .. :::::; r;:: ~ ~ I" ~ ~ i-r+-It. 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"""(ereos BOlr 1,1- I,t::r::. 1t.r:=+ I,t::~ :~~r::. ~ r::. ,-...... ::::+ ,-...... ::::+ ,-...... ::::+ 1'-~ r::. 11~ ~ r::. I'~ ~ ~ 11~ ~ r::. I'~ I~t: ~ I ~ ,..... :::+ ,~ ..... :::+ 1:: - ~ ;:: tc::::: ~I -~ ""N t::". , ....... ~ - ~ ....... ~ ~ ;:::-~ ~ to ,.... I w 0 C! .. ~ ,.. I"- W 0 C! - co W 0 C! o~-des 60-deS so-des La-des go-des 90-deS va-des 80-deS em-des w-des oo-des 66-deS 86-deS L6-deS 96-deS 96-deS v6-deS 86-deS G6-deS ~6-des 06-deS 6S-deS 8S-deS LS-deS 9S-deS 9S-deS vs-des 88-deS Gs-deS ~s-des -E -(3 ::::J -en c o ".j:i C'tI ~ -c CD (,) C o () o ('I) C\I I E ::::J "i: o .s:. I- ('I) :> ~ ca C\J ,..- I W W 0 0 ~ ~ .. ~ C") ~ U') ,..- W W I W 0 0 0 ~ ~ ~ (eIEOS 60lf 14 P. ~I=::: ~ 14 14~ ~ '.1=::: ~ • I·F: t;. ,.~ ~ 4 '.F: ~ ,.k ~k ~ ~ • ~F:: ~ • I.~ ~ I.k ~ I.k • ~ '.~ ~ 1.1:::: ~ • I.f::: ~ • ~ ~ t--. t.. 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It ~~ ~ Ii'" I I"-..- I UJ 0 q ..- . ro W 0 q o~-des 60-deS so-des LO-deS 90-deS 90-deS vO-deS 80-deS Go-des ~o-des OO-deS 66-deS S6-deS L6-deS 96-deS 96-deS v6-deS 86-deS G6-deS ~6-des 06-deS 6S-deS ss-des LS-deS 9s-des 9s-des vs-des 8S-deS GS-deS ~s-des 1.00E-11 1.00E-12 1.00E-13 Q) Cii o (j)1 .00E-14 OJ o ....J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1E-12 uCi/ml /I • I 41 ~ Y ~f\. 1\ X t t_ ~ 1\ It Jt ... .... ~~ v.'l~ .-C\J C") "<:t co co co co I I I I Q. Q. Q. Q. 0> 0> 0> 0> (j) (j) (j) (j) LO co , Q. <D (j) ~'~V co co 6.. <D (j) , f'-. co 6.. <D (j) co co 6.. <D (j) "r ~~V') . 0) co 6.. <D (j) . o 0) 6.. 0> (j) .- O'l , Q. <D (j) C\J 0) I Q. 0> (j) . C") 0) 6.. <D (j) "<:t 0) 6.. 0> (j) BHV-3 Lead-210 Concentrations (uCi/ml) 1< }t. ~. J5.. }t. Jf.. Jf.. }t. ~ ~ Jt It. ~ ~ ~ ~ \l LO 0) 6.. <D (j) VVVVVVVVVV~'VV'VVl co 0) 6.. 0> (j) f'-. 0) , Q. <D (j) co 0) 6.. <D (j) 0) 0) 6.. 0> (j) o o , Q. 0> (j) .-o 6.. 0> (j) , C\J o , Q. 0> (j) C") o 6.. <D (j) "<:t o 6.. 0> (j) LO o I Q. 0> (j) co o , Q. 0> (j) f'-. o I Q. <D (j) co o 6.. <D (j) 0) o , Q. <D (j) o .- 6.. <D (j) TAB 4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal= 2_25E-14 uCi/ml ALARA Goal = .5E-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = .1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC LImit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA i 9/28/1981 5.20E-15 5.00E-12 "1.25E-12 2.93E-15 8.00E-14 2.00E-14 2.74E-15 2.00E-12 5.00E-13 1.84E-14 4.00E-12 1.00E-12 I 12/14/1981 4.53E-15 5.00E-12 1.25E-12 1.78E-15 8.00E-14 2.00E-14 2.29E-15 2.00E-12 5.00E-13 2.54E-14 4.00E-12 1.00E-12 i 3/29/1982 1.06E-15 5.00E-12 1.25E-12 1.42E-14 8.00E-14 2.00E-14 1.07E-15 2.00E-12 5.00E-13 2.31E-14 4.00E-12 1.00E-12 I 6/30/1982 6.03E-15 5.00E-12 1.25E-12 1.57E-14 8_00E-14 2.00E-14 2.62E-15 2.00E-12 ,5.00E-13 2.25E-14 4_00E-12 1.00E-12 I 9/27/1982 1.26E-14 5.00E-12 1.25E-12 7.58E-16 8.00E-14 2.00E-14 5.35E-15 2.00E-12 5.00E-13 2.68E-14 4_00E-12 1.00E-12 1/3/1983 4.33E-15 5.00E-12 1.25E-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 4/4/1983 1.25E-15 5.00E·12 1.25E-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2.00E-12 5.00E-13 2.00E-14 4.00E-12 1.00E-12 6/30/1983 3.73E-16 5.00E-12 1.25E-12 9.43E-16 8.00E-14 2.00E-14 4_13E-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 1.00E-12 10/3/1983 2.54E-16 ~.00E-12 1.25E-12 1.51E-16 8.00E-14 2.00E-14 2.65E-16 2.00E-12 5.00E-13 2.50E-14 4.00E-12 1.00E-12 1/3/1984 2.76E-15 5.00E-12 1.25E-12 1.60E-16 8.00E-14 2.00E-14 1.05E-16 2.00E-12 5.00E-13 1.59E-16 4.00E-12 1.00E-12 4/2/1984 4.27E-16 5.00E-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 2.00E-12 5.00E-13 3.67E-14 4.00E-12 1.00E-12 7/2/1984 2_57E-15 5.00E-12 1.25E-12 1.36E-16 8.00E-14 2.00E-14 1.11E-16 2.00E-12 5.00E-13 1.58E-14 4.00E-12 1.00E-12 10/1/1984 4.18E-16 5.00E-12 1.25E-12 3.54E-16 8.00E-14 2.00E-14 1.10E-17 2.00E-12 5.00E-13 9.83E-15 11.00E-12 1.00E-12 1/2/1985 5.30E-17 5.00E-12 1.25E-12 3.55E-17 8.00E-14 2.00E-14 7_00E-18 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 5.00E-12 1.25E-12 6.00E-16 8.00E-14 2.00E-14 4.35E-17 2.00E-12 .5.00E-13 5.02E-15 4.00E-12 1.00E-12 7/1/1985 9.36E-16 5.00E-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 2.00E-12 5.00E-13 7.48E-15 4.00E-12 1.00E-12 9/30/1985 1.46E-15 5.00E-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 5.38E-16 2.00E-12 5.00E-13 7.86E-15 4.00E-12 1.00E-12 1/2/1986 8.40E-15 5.00E-12 1.25E-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 2.00E-12 5.00E-13 2.12E-14 4.00E-12 1.00E-12 4/1/1986 5.79E-15 5.00E-12 1.25E-12 5.80E-16 8.00E-14 2.00E-14 1.34E-15 2.00E-12 5.00E-13 1.33E-14 4.00E-12 1.00E-12 6/30/1986 5.19E-15 5.00E-12 1.25E-12 7.83E-16 8.00E-14 2.00E-14 2.20E-15 2.00E-12 5.00E-13 7.14E-16 4.00E-12 1.00E-12 10/27/1986 4.60E-15 5.00E-12 1.25E-12 4.67E-16 8.00E·14 2.00E-14 2.37E-15 2.00E-12 5.00E-13 1.13E-14 4.00E-12 1.00E·12 12/15/1986 2.75E-15 5.00E-12 1.25E-12 5.90E-16 8.00E-14 2.00E-14 9.39E-16 2.00E·12 5.00E-13 1.20E·14 4.00E-12 1.00E-12 3/16/1987 4.64E-15 5.00E-12 1.25E-12 1.18E-15 8.00E-14 2.00E-14 4.97E-16 2.00E-12 5.00E-13 5.89E-14 4.00E-12 1.00E-12 5/11/1987 4.35E-15 5.00E-12 1.25E-12 1.23E·14 8.00E-14 2.00E-14 1.13E-15 2.00E-12 5.00E-13 2.21E-14 4.00E-12 1.00E-12 9/9/1987 6.39E-15 5.00E-12 1.25E-12 1.50E-14 8.00E-14 2.00E-14 2.26E-15 2.00E-12 5.00E-13 1.57E-14 4.00E-12 1.00E-12 11/2/1987 6.72E-15 5.00E-12 1.25E-12 4.53E-16 8.00E-14 .2.00E-14 2.20E-15 2.00E-12 5.00E-13 2.55E-14 4.00E-12 1.00E-12 2/16/1988 1.91E-15 5.00E-12 1.25E-12 1.35E-14 8.00E-14 2.00E-14 4.42E-16 2.00E-12 5.00E-13 4.44E-14 4.00E-12 1.00E-12 5/18/1988 1.78E-14 5.00E-12 1.25E-12 4.39E-14 8.00E-14 .2.00E-14 4.92E-16 2.00E-12 5.00E-13 1.38E-14 4.00E-12 1.00E-12 8/15/1988 7.56E-15 5.00E·12 1.25E-12 3.31E-14 8.00E-14 2.00E-14 1.51E-15 2.00E-12 5.00E-13 1.97E-14 4.00E-12 1.00E-12 11/14/1988 1.47E-14 5.00E-12 1.25E-12 1.56E-15 8.00E-14 2.00E-14 2.57E-15 2.00E-12 5_00E·13 2.12E-14 4.00E-12 1.00E-12 2/13/1989 2.47E-15 5.00E-12 1.25E-12 3.14E-15 8.00E-14 2.00E-14 6.94E-16 2.00E-12 5.00E-13 2.12E-14 4.00E-12 1.00E-12 5/15/1989 2.50E-16 5.00E-12 1.25E-12 7.68E-15 8.00E-14 2.00E-14 9.03E-16 2.00E-12 5.00E-13 8.05E-15 4.00E-12 1.00E-12 8/14/1989 6.50E-15 5.00E-12 1.25E-12 4.72E·15 8.00E-14 2.00E-14 2.35E-15 2.00E-12 5.00E-13 9.95E-15 4.00E-12 1.00E-12 11/13/1989 9.63E-15 5.00E-12 1.25E-12 4.05E-15 8.00E-14 2.00E-14 4.03E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 1.00E-12 2/12/1990 8.92E-15 5.00E-12 1.25E-12 3.56E-15 8.00E-14 2.00E-14 2.89E-15 2.00E-12 5.00E-13 2.69E-14 4.00E-12 1.00E-12 5/14/1990 8.90E-15 5.00E-12 1.25E-12 3.58E-15 8.00E-14 2.00E-14 2.33E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 1.00E-12 8/13/1990 1.92E-15 5.00E-12 1.25E-12 1.87E-15 8.00E-14 2.00E-14 5.06E-16 2.00E-12 5.00E-13 8.86E-15 4.00E-12 1.00E-12 11/12/1990 2.91E-15 5.00E-12 1.25E-12 2.25E-17 8.00E-14 2.00E-14 1.08E-15 2.00E-12 5.00E-13 2.19E-14 4.00E-12 1,00E-12 2/11/1991 1.67E-16 5.00E-12 1.25E-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 5.00E-13 4.19E-14 4.00E-12 1.00E-12 5/13/1991 1.87E-16 5.00E-12 1.25E-12 2.61E-15 8.00E-14 2.00E-14 3.54E-16 2.00E-12 5.00E-13 1.40E-14 4.00E-12 1.00E-12 8/12(1991 4.85E-16 5.00E-12 1.25E-12 4.38E-16 8.00E-14 2.00E-14 1.27E-16 2.00E-12 5.00E-13 2.20E-14 4_00E-12 1.00E-12 11/11/1991 1.77E-16 5.00E-12 1.25E-12 1.46E-16 8.00E-14 2.00E-14 3.76E-17 2.00E-12 5.00E-13 1.15E-14 4.00E-12 1.00E-12 2/10/1992 1.83E-16 5.00E-12 1.25E-12 1.95E-15 8.00E-14 2.00E-14 1.33E-16 2.00E-12 5.00E-13 3.35E-14 4.00E-12 1.00E-12 5/11/1992 4.40E-16 5.00E-12 1.25E-12 2.56E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 5.00E-13 1.41E-14 4.00E-12 1.00E-12 8/10/1992 9.09E-17 5.00E-12 1.25E-12 1.15E-16 8.00E-14 2.00E-14 4.50E-17 2.00E-12 5.00E-13 1.57E-14 4.00E-12 1.00E-12 11/9/1992 2.07E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 3.62E-17 2.00E-12 5.00E-13 2.24E-14 4.00E-12 1.00E-12 2/9/1993 1.73E-16 5.00E-12 1.25E-12 1.76E-17 8.00E-14 2.00E-14 2.89E-17 2.00E-12 5.00E-13 :3.08E-14 4.00E-12 1.00E-12 5/10/1993 2.70E-17 5.00E-12 1.25E-12 2.50E-17 8.00E-14 2.00E-14 8.74E-17 2.00E-12 5.00E-13 '1.25E-14 4.00E-12 1.00E-12 8/10/1993 9.00E-17 5.00E-12 1.25E-12 1.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 1.50E-14 4.00E-12 1.00E-12 11/8/1993 1.00E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 6.00E-17 2.00E-12 5.00E-13 1.75E-14 4.00E-12 1.00E-12 1/7j1994 1.10E-16 5.00E-12 1.25E-12 3.38E-16 8.00E-14 2.00E-14 2.21E-16 2.00E-12 5.00E-13 3.08E-14 4.00E-12 1.00E-12 5/9/1994 3.80E-16 5.00E-12 1.25E-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 .5.00E-13 1.73E-14 4.00E-12 1.00E-12 8/9/1994 3.85E-16 5.00E-12 1.25E-12 3.53E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 6.21E-17 5.00E-12 1.25E-12 9.70E-17 8.00E-14 2.00E-14 1.96E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 --- Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal= Z.ZSE-l4 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= Z.2SE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit = SE-lZ uCi/ml Pre 1994 MPC limit,. SE-14 uCi/ml Pre 1994 MPC limit = ZE-12 uCi/ml Pre 1994 MPC Limit = 4E-lZ uCi/ml Pre 1994 ALARA GOAL = l.ZSE-l2 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/199S 3.70E-16 9.00E-14 2.2sE-14 9.80E-17 2.00E-14 s.OOE-ls 9.70E-17 9.00E-13 2.2sE-13 8.84E-1s 6.00E-13 1.s0E-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 2.86E-16 2.00E-14 s.00E-1s 1.90E-16 9.00E-13 2.2sE-13 2.90E-ls 6.00E-13 1.50E-13 8/9/1995 l.4sE-16 9.00E-14 2.2sE-14 2.31E-1s 2.00E-14 s.00E-1S 7.10E-17 9.00E-13 2.2sE-13 2.70E-1s 6.00E-13 l.sOE-13 11/11/1995 1.43E-14 9.00E-14 2.2sE-14 S.70E-1s 2.00E-14 s.00E-1S 2.61E-ls 9.00E-13 2.2sE-13 s.60E-1s 6.00E-13 1.50E-13 2/5/1996 1.19E-14 9.00E-14 2.2sE-14 3.80E-16 l.00E-14 s.00E-1S 6.10E-ls 9.00E-13 2.2sE-13 6.4SE-1s 6.00E-13 l.sOE-13 5/6/1996 4.ssE-16 9.00E-14 2.2sE-14 3.s7E-1s 2.00E-14 s.00E-1s 2.84E-16 9.00E-13 2.2sE-13 7.68E-1s 6.00E-13 l.sOE-13 8/5/1996 7.78E-16 9.00E-14 2.2SE-14 3.s1E-1s 2.00E-14 s.00E-1s 1.69E-16 9.00E-13 2.2sE-13 4.90E-1s 6.00E-13 1.s0E-13 11/6/1996 1.36E-1s 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 s.00E-1s 4.21E-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 l.sOE-13 2/6/1997 1.00E-16 9.00E-14 2.2sE-14 1.40E-16 2.00E-14 s.00E-1S 1.03E-16 9.00E-13 2.2sE-13 6.76E-ls 6.00E-13 1.s0E-13 5/5/1997 1.00E-16 9.00E-14 2.2sE-14 4.00E-16 2.00E-14 s.00E-1s 2.24E-16 9.00E-13 2.2sE-13 4.sSE-ls 6.00E-13 1.s0E-13 8/11/1997 4.74E-16 9.00E-14 2.2sE-14 9.07E-16 l.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 s.ssE-ls 6.00E-13 1.S0E-13 1/5/1998 8.31E-16 9.00E-14 2.2sE-14 4.82E-16 2.00E-14 s.OOE-ls 1.77E-16 9.00E-13 2.2sE-13 s.28E-ls 6.00E-13 l.sOE-13 4/28/1998 3.32E-16 9.00E-14 2.2sE-14 4.43E-1S 2.00E-14 s.00E-1S 1.21E-16 9.00E-13 2.2sE-13 7.43E-1S 5.00E-13 l.SOE-13 7/31/1998 4.60E-16 9.00E-14 2.2sE-14 9.02E-16 2.00E-14 s.00E-1S 3.S4E-16 9.00E-13 2.2SE-13 6.91E-1S 6.00E-13 l.SOE-13 9/28/1998 4.08E-16 9.00E-14 2.2SE-14 4.93E-16 l.00E-14 s.00E-1S 2.53E-16 9.00E-13 2.2sE-13 4.52E-1s 6.00E-13 l.S0E-13 12/28/1998 7.nE-16 9.00E-14 2.2sE-14 3.7sE-16 l.00E-14 s.OOE-ls 3.43E-16 9.00E-13 2.2sE-13 6.73E-1S 6.00E-13 l.s0E-13 3/29/1999 s.l1E-16 9.00E-14 2.2sE-14 4.70E-16 2.00E-14 s.00E-1s 3.70E-16 9.00E-13 2.2SE-13 B.96E-1S 6.00E-13 1.50E-13 7/3/1999 S.90E-16 9.00E-14 2.2sE-14 9.89E-16 2.00E-14 s.00E-1S 1.28E-16 9.00E-13 2.2sE-13 5·40E-IS 6.00E-13 1.50E-13 9/27/1999 1.70E-1S 9.00E-14 2.2sE-14 7.s0E-16 2.00E-14 s.00E-1s 4.61E-16 9.00E-13 2.2sE-13 7.86E-ls 6.00E-13 l.SOE-13 12/28/1999 1.03E-15 9.00E-14 2.2sE-14 7.s0E-16 2.00E-14 s.00E-1S 2.43E-16 9.00E-13 2.2sE-13 G.42E-ls 6.00E-13 1.50E-13 3/27/2000 1.00E-16 9.00E-14 2.2sE-14 2.13E-16 2.00E-14 s.00E-1s 2.20E-16 9.00E-13 2.2sE-13 s.61E-1s 6.00E-13 1.50E-13 I 6/26/2000 1.7sE-16 9.00E-14 2.2sE-14 3.08E-16 2.00E-14 s.00E-1s 1.11E-16 9.00E-13 2.2sE-13 B.92E-1s 6.00E-13 l.s0E-13 I 9/26/2000 3.6sE-16 9.00E-14 2.2sE-14 .2.01E-16 2.00E-14 s.00E-1s 2.24E-16 9.00E-13 2.2sE-13 7.79E-15 6.00E-13 1.s0E-13 I 12/26/2000 2.27E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 4.3sE-16 9.00E-13 ~.25E-13 8.4sE-ls 6.00E-13 l.sOE-13 3/26/2001 1.4sE-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.37E-15 6.00E-13 l.sOE-13 7/2/2001 1.00E-16 9.00E-14 2.2sE-14 1.0sE-16 2.00E-14 S.OOE-ls 1.00E-16 9.00E-13 2.2sE-13 6.99E-1s 6.00E-13 ·l.sOE-13 9/24/2001 1.91E-16 9.00E-14 .2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 2.01E-16 9.00E-13 2.2sE-13 8.04E-1s 6.00E-13 1.sOE-13 12/31/2001 l.38E-16 9.00E-14 2.2sE-14 2.0sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.83E-ls 6.00E-13 1.50E-13 4/1/2002 2.20E-16 9.00E-14 1.2sE-14 3.38E-16 2.00E-14 s.00E-1s 1.26E-16 9.00E-13 2.2sE-13 7.48E-1s 6.00E-13 1.s0E-13 7/1/2002 l.97E-16 9.00E-14 2.2sE-14 4.10E-16 2.00E-14 s.OOE-ls 1.00E-16 9.00E-13 z'2sE-13 7.40E-1s 6.00E-13 1.50E-13 9/30/2002 2.30E-16 9.00E-14 2.2sE-14 2.42E-16 2.00E-14 s.00E-1s 1.S6E-16 9.00E-13 ~.2SE-13 4.21E-1s 6.00E-13 1.s0E-13 '12/30/2002 1.00E-16 9.00E-14 2.2sE-14 1.92E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.42E-ls 6.00E-13 l.S0E-13 3/31/2003 2.s0E-16 9.00E-14 2.2sE-14 1.69E-16 2.00E-14 s.00E-1s l.29E-16 9.00E-13 2.2sE-13 4.ssE-IS 6.00E-13 1.S0E-13 6/30/2003 1.00E-16 9.00E-14 2.2sE-14 2.87E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2SE-13 4.20E-1s 6.00E-13 1.s0E-13 9/29/2003 1.00E-16 9.00E-14 2.2sE-14 8.s3E-16 2.00E-14 S.00E-1s 3.32E-16 9.00E-13 2.2SE-13 8.69E-1s 6.00E-13 l.sOE-13 12/29/2003 1.02E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 S.00E-1s 1.49E-1S 9.00E-13 2.2SE-13 9.4SE-IS 6.00E-13 1.s0E-13 3/29/2004 t.00E-16 9.00E-14 2.2sE-14 1.26E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 2.00E-1s 6.00E-13 1.s0E-13 6/27/2004 l.00E-16 9.00E-14 2.2SE-14 2.53E-16 2.00E-14 S.OOE-IS 1.00E-16 9.00E-13 2.2SE-13 3.23E-15 6.00E-13 1.S0E-13 9/27/2004 1.00E-16 9.00E-14 2.2sE-14 1.1SE-16 2.00E-14 s.OOE-ls l.00E-16 9.00E-13 2.2SE-13 9.68E-1S 6.00E-13 1.S0E-13 12/27/2004 1.00E-16 9.00E-14 2.2SE-14 2.30E-16 2.00E-14 S.OOE-IS 1.00E-16 9.00E-13 2.2SE-13 l.37E-14 6.00E-13 l.S0E-13 3/28/2005 i.00E-16 9.00E-14 2.2SE-14 2.66E-16 2.00E-14 S.00E-1S 3.1sE-16 9.00E-13 2.2SE-13 9.22E-IS 6.00E-13 l.SOE-13 6/29/2005 1.47E-16 9.00E-14 2.2sE-14 1.4sE-ls 2.00E-14 S.00E-1s 1.42E-16 9.00E-13 2.2sE-13 9.34E-1s 6.00E-13 l.sOE-13 9/26/2005 2.0lE-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 S.OOE-Is 4.80E-16 9.00E-13 2.2sE-13 2.12E-14 6.00E-13 1.sOE-13 1/3/2006 4.54E-16 9.00E-14 2.2sE-14 1.24E-16 2.00E-14 s.OOE-ls l.00E-16 9.00E-13 2.2sE-13 3.60E-14 6.00E-13 1.s0E-13 4/3/2006 l.99E-16 9.00E-14 2.2sE-14 1.32E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2SE-13 8.36E-ls 6.00E-13 l.s0E-13 7/3/2006 2.76E-16 9.00E-14 2.2sE-14 2.63E-16 2.00E-14 S.OOE-ls l.00E-16 9.00E-13 2.2sE-13 1.03E-14 6.00E-13 1.s0E-13 10/2/2006 4.97E-16 9.00E-14 2.2sE-14 2.37E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.60E-14 6.00E·13 1.50E-13 1/1/2007 6A6E-16 9.00E-14 2.2sE-14 2.8lE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2SE-13 2.l0E-14 6.00E-13 1.50E-13 4/2/2007 7.08E-16 9.00E-14 2.2SE-14 3.20E-16 2.00E-14 S.OOE-lS 1.00E-16 9.00E-13 2.2SE-13 l.S4E-14 6.00E-13 1.50E-13 7/2/2007 9.4lE-16 9.00E-14 2.2SE-14 1.46E-16 l.00E-14 S.00E-1S 1.99E-16 9.00E-13 2.2SE·13 2.S6E-14 6.00E-13 l.SOE-13 9/30/2007 3.30E-16 9.00E-14 2.2SE-14 S.SOE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.57E-1S 6.00E-13 1.S0E-13 12/31/2007 1.42 E-1S 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.OOE-lS 1.00E-16 9.00E-13 2.2SE-13 9.93E-1S 6.00E-13 1.S0E-13 3/31/2008 1.2sE-16 9.00E-14 2.2SE-14 'l.nE-16 2.00E-14 S.OOE-lS 1.00E-16 9.00E-13 2.2SE-13 4.09E-ls 6.00E-13 1.S0E-13 6/30/2008 l.28E-1S 9.00E-14 2.2SE-14 1.00E-16 l.00E-14 s.00E-1s 3.61E-16 9.00E-13 2.2SE-13 1.18E-14 6.00E-13 1.SOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2£-14 uCi/ml BHV-4T Effluent Concentration limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal= 2.25E-14 uCi/ml ALARA Goal = 5£-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Umit = 2E-12 uCi/ml Pre 1994 MPC Limit -4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 12/31/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/15/2009 1.56E-15 9.00E-14 2.25E-14 4.57E-16 2.00E-14 5.00E-15 2.99E-16 9.00E-13 2.25E-13 4.97E-15 6.00E-13 1.50E-13 6/15/2009 5.67E-17 9.00E-14 2.25E-14 2.17E-16 2.00E-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13 9/15/2009 4.05E-15 9.00E-14 2.25E-14 1.45E-15 2.00E-14 5.00E-15 2.52E-16 9.00E-13 2.25E-13 1.24E-14 6.00E-13 1.50E-13 12/15/2009 6.50E-15 9.00E-14 2.25E-14 3.48E-16 2.00E-14 5.00E-15 1.33E-16 9.00E-13 2.25E-13 7.60E-15 6.00E-13 1.50E-13 3/31/2010 6.01E-15 9.00E-14 2.25E-14 1.26E-16 2.00E-14 5.00E-15 1.34E-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 6/30/2010 2.33E-15 9.00E-14 2.25E-14 7.29E-16 2.00E-14 5.00E-15 2.66E-16 9.00E-13 2.25E-13 3.27E-15 6.00E-13 1.50E-13 9/30/2010 4.77E-15 9.00E-14 2.25E-14 1.80E-15 2.00E-14 5.00E-15 8.23E-16 9.00E-13 2.25E-13 5.11E-15 6.00E-13 1.50E-13 12/31/2010 3.93E-15 9.00E-14 2.25E-14 3.90E-16 2.00E-14 1i.00E-15 2.56E-16 9.00E-13 2.25E-13 1.13E-14 6.00E-13 1.50E-13 4/4/2011 1.29E-15 9.00E-14 2.25E-14 1.40E-16 2.00E-14 5.00E-15 1.58E-16 9.00E-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 7/4/2011 3.30E-15 9.00E-14 2.25E-14 5.44E-16 2.00E-14 5.00E-15 4.18E-16 9.00E-13 2.25E-13 8.26E-15 6.00E-13 1.50E-13 -------- -E :'::::: o ~ -en c o '-; """ -c CD Co) C o o CD "C Co) :::J C o "C ca II: o::t :> ::I: m N C') T""" ..... , , w w 0 0 ~ ~ : .. ~ .. .-.: ~ 4 ~""-4 ---«:: • jP < ~ --:; ;. • <: ~ 40::::: ::::. ..... -~ ...- ~ ..... ~ I-'" I.~ I"'F: ~ -..-;;: ...... 4K 1"-C> ... >+ ) ~ ~ '<t T""" , w 0 ~ ..... -:::::=+ ::=-iii:: :--61;;0 --o~-das "r;; ::.f , ~ 60-daS <II.. .... -so-das 4 § --. N ......... ~::::; ~ ~ LO-daS 90-daS 90-daS ~ ~ .. ~ ~ vo-das ~ ..::: :::>I .~ ~ .... 1::=>. -.~ ~ ~ 'h .-"'l! --- 80-daS 0 ~ N co-das , ~ co Q) W-daS -l + oo-das ~ . .,... .. -~ • .~ :! ;:It ~ f-,., <D 66-daS N ~ S6-daS E :::::l '6 L6-daS co a: • -~ -96-das + ...... J .-.. 96-daS 0 C') N -v6-daS , E 1ti E: :::::l ~ 86-daS .;:: 0 .!: ~~ i'. f- c6-daS + • ---~6-das .. ~ .-(ij "" 06-daS '-:::::l -~': co 6S-daS z E :::::l ""'+-ss-das 'c co iii .. r--. ~ .. ~ '- LS-daS ~ + 9S-daS -;;;>' 9S-daS vs-das 8s-das .. cs-daS ., ~s-das lO <D I"-<Xl T""" T""" T""" T""" , , , , w UJ w w 0 0 0 0 ~ ~ ~ ~ T""" ..... ..... (al8os 001) 1.00E-11 1.00E-12 1.00E-13 Q) (ij (.) C/)1.00E-14 C> o ....J - 1.00E-1S 1.00E-16 1.00E-17 •• ..... co I a. Q) C/) Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCilml --- t ~~ • ,.- • \} 1 ... 'It. ~ T .. 1\ 11 1\/ ~ .. - , C\I C') ..;t co co co I I I a. a. a. Q) Q) Q) C/) C/) C/) , LO co 6.. Q) C/) (0 t--co co 6.. 6.. Q) Q) C/) C/) co co I a. Q) C/) (J) co I a. Q) C/) o (J) I a. Q) C/) ..... (J) 6.. Q) C/) .... \r C\I (J) 6.. <Il C/) - v • T I J. C') (J) 6.. Q) C/) ..;t (J) 6.. Q) C/) 1\ BHV-4 Uranium-Natural Concentrations (uCi/ml) ~ v LO (J) I a. Q) C/) , (0 (J) 6.. Q) C/) T \~ t--(J) 6.. Q) CJ) • co (J) 6.. <Il C/) - ~ 1t r. ... t II 'V'.~ \ (J) 0 (J) 0 I I a. a. Q) Q) C/) CJ) ..... o I a. Q) C/) C\I o 6.. Q) C/) C') o 6.. Q) C/) ..;t o 6.. Q) C/) • T 1\ I JV I' LO o 6.. Q) C/) (0 o 6.. Q) C/) • t--o I a. Q) C/) ~ ~ ~ co o I a. Q) C/) (J) o 6.. Q) C/) ~ 'I: , \1 o ..... 6.. Q) C/) V - II) c o '';:; as "--c Q) () c o (J o ('t) ~ E ~ 'i: o .c I- "I::t > ::I: m ..... J.J o o ..... I~~ C\I ('I) ..... ..... I I W W 0 0 ~ ~ ..... ~ - II: ;;;.,---,... ... "'-- r- iii ~~ .... '"" ..... ...:: ..... 19' '<t LO ..... J.J J.J 0 0 C! ~ (alBos 001) ..... ... 1.-~ o~-das 1.1-~ It+--I>' 60-daS 80-das ...... I ~:.-~ ~ ~ LO-daS 90-daS so-das I~ ~ f-jI....., ~ ~~ ~ ~ vo-das 80-daS Go-daS w-das .J~ ~ oo-das 66-daS ~~ 86-daS h~ t--k L6-das 96-daS S6-das --~~ - 14Ir-. ~ v6-daS 86-daS ., L--4 G6-daS t..i-~ ,... ~6-das 06-das 68-das 88-daS L8-daS • 98-daS J,:; ~ S8-daS ~ f=:: t;:. • ~ j..... I- v8-daS 88-daS G8-daS ~8-das <D r-... ..... ..... I I W W 0 0 ~ C! ..... 1.00E-11 1.00E-12 1.00E-13 _1.00E-14 Q) Iii u en Ol o -l -1.00E-1S 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml I r.t .... ~ ..... V. t \, f \ I \ ""\ I \L 9 ~ • 1\ f1 ~ .+ .... ~ r-co I a. Q) en C\I co 6.. Q) en . C') co I a. Q) en '<:t co 6.. Q) en \l) co I a. Q) en co co 6.. Q) en r--co I a. Q) en co co I a. Q) en en co I a. Q) en , o en I a. Q) en r-en 6.. Q) en C\I en I ~ a. Q) en BHV-4 Radium-226 Concentrations (uCi/ml) \ 1. 1. • 4\ I \fV\ C') en 6.. Q) en '<:t en 6.. Q) en \l) en I a. Q) en /I 1t~ " /I " \ . /. \ '+.. ·v.VJ co en 6.. Q) en r--en 6.. Q) en co en 6.. Q) en ~ V en en I a. Q) en o o I a. Q) en 1 I ifuAAl r-o I a. Q) en C\I o I a. Q) en C') o 6.. Q) en .... 11 1\/\ l' \ '<:t o I a. Q) en \l) o I a. Q) en co o 6.. Q) en 1\..1 r--o I a. Q) en Y I ,~ '~I co o 6.. Q) en ¥~ ~ en o I a. Q) en o r- 6.. Q) en 1.00E-11 1.00E-12 1.00E-13 Q) nl u (/J 1.00E-14 Cl o .-.J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALAR A Goal = 1 E-12 uCilml • /\ ... 1\ • ~i 1\ t ... .t \.-.AJ\.I\~ 1\ ,.... co I C. Q) (/J C\I co 6.. Q) (/J V I~J' {) ~ ~ 'J{ \ J \/ ¥~... V C') "<t L{) co co co I I I C. C. C. Q) Q) Q) (/J (/J (/J , CD co I C. Q) (/J r-... co 6.. Q) (/J , co 0) co co I I C. C. Q) Q) (/J (/J o 0) 6.. Q) (/J ,.... 0) 6.. Q) (/J C\I 0) I C. Q) (/J C') 0) 6.. Q) (/J "<t 0) I C. Q) (/J BHV-4 Lead-210 Concentrations (uCi/ml) • I ..... 1I ..... L{) 0) I C. Q) (/J CD 0) 6.. Q) (/J r-... 0) I C. Q) (/J • co 0) I C. Q) (/J 0) 0) 6.. Q) (/J .... o o I C. Q) (/J -- I V • ,.... o 6.. Q) (/J ~- C\I o 6.. Q) (/J C') o 6.. Q) (/J 'II ~ 1\1 ~ JI "<t o 6.. Q) (/J LO o I C. Q) (/J ... ~ r CD o 6.. Q) (/J r-... o 6.. Q) (/J • tt ... ... co o I C. Q) (/J .. , 0) o 6.. Q) (/J ~ o ,.... 6.. Q) (/J TAB 5 BHV -5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit-SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC LImit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.44E-1S 5.00E-12 1.25E-l2 ·1.53E-15 8.00E-14 2.00E-14 7.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-l2 1.00E-l2 l2/14/1981 4.84E-15 5.00E-12 1.25E-l2 2.78E-15 8.00E-14 2.00E-14 1.84E-15 2.00E-12 5.00E-13 :1.53E-14 4.00E-12 1.00E-l2 3/29/1982 1.04E-15 5.00E-12 1.25E-l2 2.62E-15 8.00E-14 2.00E-14 1.11E-15 2.00E-l2 5.00E-13 2.98E-14 4.00E-l2 1.00E-l2 6/30/1982 3.61E-15 5.00E-12 1.25E-12 'l.61E-15 8.00E-14 2.00E-14 1.39E-15 2.00E-12 5.00E-13 1.80E-15 4.00E-l2 1.00E-12 9/27/1982 1.71E-14 5.00E-12 1.25E-12 9.46E-15 8.00E·14 2.00E-14 3.80E-15 2.00E-12 5.00E-13 2.35E-14 4.00E-12 1.00E-12 1/3/1983 1.90E-14 5.00E-12 1.25E-12 5.77E-15 8.00E-14 2.00E-14 9.34E-17 2.00E-12 5.00E-13 4.32E-14 4.00E-12 .1.00E-l2 4/4/1983 5.00E-12 1.25E-12 2.33E-15 8.00E-14 2.00E-14 5.93E-16 2.00E-12 5.00E-13 3.01E-14 4.00E-12 1.00E-l2 6/30/1983 7.62E-16 5.00E-12 1.25E-12 3.25E-15 8.00E-14 2.00E-14 6.28E-15 2.00E-12 5.00E-13 2.69E-14 4.00E-12 1.00E-l2 10/3/1983 4.86E-16 S.00E-12 1.25E-12 1.lOE-15 8.00E-14 2.00E-14 3.63E-16 2.00E-l2 5.00E-13 2.08E-14 4.00E-12 1.00E-l2 1/3/1984 6.96E-15 5.00E-12 1.25E-12 9.69E-16 8.00E-14 2.00E-14 9.60E-16 2.00E-12 5.00E-13 1.83E-14 4.00E-12 1.00E-l2 4/2/1984 1.64E-15 5.00E-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 3.88E-15 2.00E-l2 5.00E-13 4.67E-14 4.00E-12 1.00E-12 7/2/1984 1.12E-15 5.00E-12 1.25E-12 1.92E-15 8.00E-14 2.00E-14 3.31E-15 2.00E-12 5.00E-13 .2.21E-14 4.00E-12 1.00E-12 10/1/1984 1.11E-15 5.00E-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 2.00E-12 5.00E-13 1.57E-14 4.00E-12 1.00E-12 1/2/1985 7.32E·16 5.00E-12 1.25E-12 6.71E·16 8.00E-14 2.00E-14 4.94E-16 2.00E-12 5.00E-13 2.42E-14 4.00E-12 1.00E-12 4/1/1985 2.36E-16 5.00E-12 '1.25E-l2 5.43E-16 8.00E-14 2.00E-14 2.71E-16 2.00E-12 5.00E-13 1.25E-14 4.00E-12 1.00E-12 7/1/1985 7.58E-16 5.00E-12 1.25E-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 5.00E-13 2.15E-14 4.00E-12 1.00E-l2 9/30/1985 7.47E-15 5.00E-12 1.25E-12 1.16E-15 8.00E-14 2.00E-14 2.19E-15 2.00E-12 5.00E-13 9.20E-15 4.00E-12 1.00E-l2 1/2/1986 1.75E-14 5.00E-l2 1.25E-12 7.24E-15 8.00E-14 2.00E-14 :3.83E-15 2.00E-12 5.00E-13 1.13E-16 4.00E-12 1.00E-12 4/1/1986 2.99E-14 5.00E-12 1.25E-12 7.64E-15 8.00E-14 2.00E-14 1.51E-14 2.00E-l2 5.00E-13 2.22E-14 4.00E-12 1.00E-12 6/30/1986 2.23E-14 5.00E-l2 1.25E-12 5.19E-15 8.00E-14 2.00E-14 1.05E-14 2.00E-12 5.00E-13 2.16E-14 4.00E-12 1.00E-l2 10/27/1986 2.33E-14 5.00E-12 1.25E-12 7.78E-15 8.00E-14 2.00E-14 1.60E-14 .2.00E-l2 5.00E-13 2.02E-14 4.00E-12 1.00E-12 .12/15/1986 3.40E-14 5.00E-12 1.25E-12 5.35E-15 8.00E-14 2.00E-14 1.47E-14 2.00E-12 5.00E-13 2.82E-14 4.00E-12 1.00E-12 3/16/1987 2.06E-14 5.00E-12 1.25E-12 4.50E-15 8.00E-14 2.00E-14 6.74E-15 2.00E-12 5.00E-13 7.29E-14 4.00E-12 1.00E-12 5/11/1987 2.50E-14 5.00E-12 1.25E-12 8.54E-15 8.00E-14 2.00E-14 8.15E-15 2.00E-12 5.00E-13 3.28E-14 4.00E-12 1.00E-12 9/9/1987 2.65E-14 5.00E-12 1.25E-12 6.62E-15 8.00E-14 2.00E-14 9.34E-15 2.00E-12 5.00E-13 2.77E-14 4.00E-12 1.00E-12 11/2/1987 1.80E-14 5.00E-12 1.25E-12 7.09E-15 8.00E-14 2.00E-14 7.20E-15 2.00E-12 5.00E-13 1.77E-14 4.00E-12 1.00E-l2 2/16/1988 1.01E-14 5.00E-12 1.25E-12 2.98E-15 8.00E-14 2.00E-14 3.93E-15 2.00E-12 5.00E-13 3.36E-14 4.00E-12 1.00E-l2 5/18/1988 1.78E-14 5.00E-12 1.25E-12 8.14E-15 8.00E-14 2.00E-14 7.43E-15 2.00E-12 5.00E-13 2.l2E-14 4.00E-12 1.00E-l2 8/15/1988 1.79E-14 5.00E-12 1.25E-12 1.49E-14 8.00E-14 2.00E-14 5.34E-15 2.00E-12 5.00E-13 2.45E-14 4_00E-12 1.00E-l2 11/14/1988 4.46E-14 5.00E-l2 1.25E-l2 1.39E-14 8.00E-14 2.00E-14 1.17E-14 2.00E-12 5.00E-13 3.43E-14 4.00E-12 1.00E-12 2/13/1989 1.67E-14 5.00E-12 1.25E-12 5.54E-15 8.00E-14 2.00E-14 7.20E-15 2.00E-12 5.00E-13 5.02E-14 4.00E-12 1.00E-l2 5/15/1989 2.03E-14 5.00E-12 1.25E-12 7.05E-15 8.00E-14 .2.00E-14 9.56E-16 2.00E-12 5.00E-13 1.43E-14 4.00E-12 1.00E-12 8/14/1989 2.81E-15 5.00E-12 1.25E-12 3.78E-15 8.00E-14 2.00E-14 9.26E-15 2.00E-12 5.00E-13 1.50E-14 4.00E-l2 1.00E-12 11/13/1989 5.38E-14 5.00E-12 1.25E-12 8.01E-15 8.00E-14 2.00E-14 1.81E-14 2.00E-l2 5.00E-13 4.09E-14 4.00E-12 1.00E-l2 2/12/1990 4.48E-14 5.00E-12 1.25E-12 1.48E-14 8.00E-14 2.00E-14 1.28E-14 2.00E-12 5.00E-13 3.88E-14 4.00E-l2 1.00E-l2 5/14/1990 2.18E·14 5.00E-12 1.25E-l2 1.70E-14 8.00E-14 2.00E-14 1.59E-14 2.00E-l2 5.00E-13 3.49E-14 4.00E-l2 1.00E-l2 8/13/1990 9_53E-15 5.00E-12 1.25E-l2 1.70E-14 8.00E-14 2.00E-14 3.27E-15 2.00E-12 5.00E-13 1.27E-14 4.00E-l2 1.00E-12 11/12/1990 1.11E-14 5.00E-12 1.25E-12 5.27E-15 8.00E-14 2.00E-14 5.38E-15 2.00E-12 5.00E-13 1.56E-14 4.00E-12 1.00E-l2 2/11/1991 6.35E-16 5.00E-l2 1.25E-l2 3.13E-16 8.00E-14 2.00E-14 2.31E-16 2.00E-12 5.00E-13 3.89E-14 4.00E-12 1.00E-l2 5/13/1991 1.22E-15 5.00E-l2 1.25E-l2 6.14E-15 8.00E-14 2.00E-14 4.41E-15 2.00E-12 5.00E-13 2.50E-14 4.00E-12 1.00E-12 8/12/1991 7.84E-16 5.00E-12 1.25E-12 1.43E-15 8.00E-14 2.00E-14 4.47E-16 2.00E-12 5.00E-13 1.84E-14 4.00E-12 1.00E-l2 11/11/1991 5.37E-16 5.00E-12 1.25E-12 4.20E-16 8.00E-14 2.00E-14 1.37E-16 2.00E-l2 5.00E-13 1.27E-14 4.00E-12 1.00E-12 2/10/1992 3.54E-16 5.00E-12 1.25E-12 1.18E-16 8.00E-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.69E-14 4.00E-12 1.00E-l2 5/11/1992 4.71E-16 5.00E-12 1.25E-12 9.58E-16 8.00E-14 2.00E-14 8.31E-17 2.00E-12 5.00E-13 1.43E-14 4.00E-l2 1.00E-12 8/10/1992 5.32E-15 5.00E-12 1.25E-l2 3.36E-16 8.00E-14 2.00E-14 1.65E-16 2.00E-12 5.00E-13 1.59E-14 4.00E-12 1.00E-12 11/9/1992 3.66E-16 5.00E-12 1.25E-l2 2.25E-16 8.00E-14 2.00E-14 1.08E-16 2.00E-12 5.00E-13 2.24E-14 4.00E-12 1.00E-l2 2/9/1993 2.05E-16 5.00E-12 1.25E-12 9.14E-17 /!.00E-14 2.00E-14 6.31E-17 2.00E-12 5.00E-13 3.41E-14 4.00E-12 1.00E-l2 5/10/1993 4.80E-16 5.00E-l2 1.25E-12 8.25E-16 8.00E-14 2.00E-14 1.26E-15 2.00E-l2 5.00E-13 1.83E-14 4.00E-12 1.00E-12 8/10/1993 8.30E-16 5.00E-12 1.25E-12 1.90E-16 8.00E-14 2.00E-14 2.10E-16 2.00E-l2 S.OOE-13 1.70E-14 4.00E-12 1.00E-l2 11/8/1993 2.70E-16 5.00E-12 1.25E-l2 8.00E-17 8.00E-14 2.00E-14 7_00E-17 2.00E-12 5.00E-13 :;1.34E-14 4.00E-12 1.00E-12 2/7/1994 3.18E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 5.18E-16 2.00E-12 5.00E-13 .3.64E-14 4.00E-12 1.00E-12 5/9/1994 1.80E-15 5.00E-12 1.25E-12 9.78E-16 8.00E-14 2.00E-14 1.10E-15 2.00E-12 .5.00E-13 8.30E-15 4.00E-12 1.00E-12 8/9/1994 2.67E-15 5.00E-12 1.25E-12 1.11E-15 8.00E-14 2.00E-14 4.95E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.21E-17 5.00E-12 1.25E-12 1.59E-15 8.00E-14 2.00E-14 1.66E-15 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1.00E-l2 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-5U Effluent Concentration Limit = 2E-14 uCi/ml BHV-5T Effluent Concentration Limit = 9E-13 uCi/ml BHV-5R Effluent Concentration Limit = 6E-13 uCi/ml BHV-5PB ALARAGoal = 2.25E-14 uCi/ml ALARAGoal= 5E-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.51E-15 9.00E-14 2.25E-14 9.50E-16 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 9.35E-15 6.00E-13 1.50E-13 5/9/1995 2.21E-16 9.00E-14 2.25E-14 8.56E-16 2.00E-14 5.00E-15 3.06E-15 9.00E-13 2.25E-13 4.34E-15 6.00E-13 1.50E-13 8/9/1995 1.66E-16 9.00E-14 2.25E-14 1.67E-15 2.00E-14 5.00E-15 3.90E-15 9.00E-13 2.25E-13 5.60E-15 6.00E-13 1.50E-13 11/11/1995 2.04E-14 9.00E-14 2.25E-14 6.70E-15 2.00E-14 5.00E-15 7.65E-15 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13 2/5/1996 4.50E-14 9.00E-14 2.25E-14 3.58E-14 2.00E-14 5.00E-15 2.39E-14 9.00E-13 .2.25E-13 7.30E-15 6.00E-13 1.50E-13 5/6/1996 1.76E-15 9.00E-14 .2.25E-14 3.57E-15 2.00E-14 5.00E-15 9.55E-16 9.00E-13 2.25E-13 7.54E-15 6.00E-13 1.50E-13 8/5/1996 2.37E-15 9.00E-14 2.25E-14 8.18E-15 2.00E-14 5.00E-15 7.46E-16 9.00E-13 2.25E-13 5.75E-15 6.00E-13 1.50E-13 11/6/1996 3.53E-15 9.00E-14 2.25E-14 5.31E-15 2.00E-14 5.00E-15 9.39E-16 9.00E-13 ~.25E-13 1.21E·14 6.00E-13 1.50E-13 2/6/1997 1.84E-16 9.00E-14 2.25E-14 2.01E-16 2.00E-14 5.00E-15 1.87E-16 9.00E-13 2.25E-13 6.14E-15 6.00E-13 1.50E-13 5/5/1997 5.75E-16 ,9.00E-14 2.25E-14 7.24E-16 2.00E-14 5.00E-15 6.07E-16 9.00E-13 2.25E-13 4.75E-15 6.00E-13 1.50E-13 8/11/1997 1.21E-15 9.00E-14 2.25E-14 7.39E-16 2.00E-14 5.00E-15 5.05E-16 9.00E-13 2.25E-13 4.92E-15 6.00E-13 1.50E-13 1/5/1998 9.89E-16 9.00E-14 2.25E-14 1.92E-15 2.00E-14 5.00E-15 6.21E-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13 4/28/1998 2.84E-15 9.00E-14 2.25E-14 2.38E-15 2.00E-14 5.00E-15 1.72E-15 9.00E-13 2.25E-13 7.35E-15 6.00E-13 1.50E-13 7/31/1998 7.49E-16 9.00E-14 2.25E-14 1.49E-15 2.00E-14 5.00E-15 8.34E-16 9.00E-13 2.25E-13 7.01E-15 6.00E-13 1.50E-13 9/28/1998 1.07E-15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 5.00E-15 6.32E-16 9.00E-13 2.25E·13 3.95E·15 6.00E-13 1.50E-13 12/28/1998 8.51E-15 9.00E-14 2.25E-14 4.58E-15 2.00E-14 5.00E-15 4.58E-15 9.00E-13 2.25E-13 1.43E-14 6.00E-13 1.50E-13 3/29/1999 3.75E-15 9.00E-14 2.25E-14 2.45E-15 2.00E-14 5.00E-15 2.39E-15 9.00E-13 2.25E-13 8.46E·15 6.00E-13 1.50E-13 7/3/1999 1.53E-15 9.00E-14 2.25E-14 8.65E-16 2.00E-14 5.00E-15 6.52E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13 9/27/1999 5.83E-15 9.00E-14 2.25E-14 3.52E-15 2.00E-14 5.00E-15 2.55E-15 9.00E-13 2.25E-13 8.22E-15 6.00E-13 1.50E-13 12/28/1999 9.48E-15 9.00E-14 2.25E-14 6.20E-15 2.00E-14 5.00E-15 3.96E-15 9.00E-13 2.25E-13 7.56E-15 6.00E-13 1.50E-13 3/27/2000 2.06E-15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 5.00E-15 1.09E-15 9.00E-13 2.25E-13 7.72E-15 6.00E-13 1.50E-13 6/26/2000 1.50E-15 9.00E-14 2.25E-14 1.24E-15 2.00E-14 5.00E-15 1.01E-15 9.00E-13 2.25E-13 4.36E-15 6.00E-13 1.50E-13 9/26/2000 1.04E-15 9.00E-14 2.25E-14 5.45E-16 2.00E-14 5.00E-15 6,01E-16 9.00E-13 2.25E-13 7.67E-15 6.00E-13 1.50E-13 12/26/2000 1.48E-15 9.00E-14 2.25E-14 7.56E-16 2.00E-14 5.00E-15 6.84E-16 9.00E-13 2.25E-13 7.00E-15 6.00E-13 1.50E-13 3/26/2001 4.27E-16 9.00E-14 2.25E-14 2.19E-16 2.00E-14 5.00E-15 1.89E-16 9.00E-13 2.25E-13 6.13E-15 6.00E-13 1.50E-13 7/2/2001 4.52E-16 9.00E-14 2.25E-14 4.02E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13 9/24/2001 4.65E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5.00E-15 2.02E-16 9.00E-13 2.25E-13 6.98E-15 6.00E-13 1.50E-13 12/31/2001 7.40E-16 9.00E-14 2.25E-14 3.51E-16 2.00E-14 5.00E-15 3.64E-16 9.00E-13 2.25E-13 4.72E-15 6.00E-13 1.50E-13 4/1/2002 1.26E-15 9.00E-14 2.25E·14 7.53E-16 2.00E-14 5.00E-15 7.19E-16 9.00E-13 2.25E-13 9.65E-15 6.00E-13 1.50E-13 7/1/2002 1.02E-15 9.00E-14 2.25E-14 '1.03E-15 2.00E-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13 9/30/2002 5.82E-16 9.00E-14 2.25E-14 9.28E-16 2.00E-14 5.00E-15 3.14E-16 9.00E-13 2.25E-13 4.48E-15 6.00E-13 1.50E-13 12/30/2002 1.00E-16 9.00E-14 2.25E-14 7.67E-16 2.00E-14 5.00E-15 3.48E-16 9.00E-13 2.25E-13 9.56E-15 6.00E-13 1.50E-13 3/31/2003 1.13E-15 9.00E-14 2.25E-14 7.41E-16 2.00E-14 5.00E-15 4.41E-16 9.00E-13 2.25E-13 6.68E-15 6.00E-13 1.50E-13 ! 6/30/2003 4.35E-16 9.00E-14 2.25E-14 5.08E-16 2.00E-14 5.00E-15 2.51E-16 9.00E-13 2.25E-13 1.34E-15 6.00E-13 1.50E-13 9/29/2003 1.51E-16 9.00E-14 2.25E-14 1.02E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13 12/29/2003 1.52E-16 9.00E-14 2.25E·14 1.54E-16 2.00E-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 7.02E-15 6.00E-13 1.50E-13 3/29/2004 1.00E-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.82E-15 6.00E-13 1.50E-13 6/27/2004 1.18E-16 9.00E-14 2.25E-14 3.11E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.47E-15 6.00E-13 1.50E-13 9/27/2004 1.16E-16 9.00E-14 2.25E-14 1.72E-16 2.00E-14 5.00E-15 1.18E-16 9.00E·13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 12/27/2004 1.14E-16 9.00E-14 2.25E-14 1.06E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13 3/28/2005 1.00E-16 9.00E-14 2.25E-14 2.04E-16 2.00E-14 5.00E-15 1.83E-16 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13 6/29/2005 1.83E-16 9.00E-14 2.25E-14 3.81E-16 2.00E-14 5.00E-15 3.09E-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 9/26/2005 2.87E-16 9.00E-14 2.25E-14 8.21E-16 2.00E-14 5.00E-15 3.71E-14 9.00E-13 2.25E-13 6.28E-14 6.00E-13 l ,50E-13 1/3/2006 8.74E-16 9.00E-14 2.25E-14 3.79E-16 2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 4.32E-14 6.00E-13 1.50E-13 4/3/2006 5.22E-16 9.00E·14 2.25E-14 6.66E-16 2.00E-14 5.00E-15 1.11E-16 9,00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13 7/3/2006 3.08E-16 9.00E-14 2.25E-14 1.10E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.25E-14 6.00E-13 1.50E-13 10/2/2006 9.14E-16 9.00E-14 2.25E-14 4.95E-16 2.00E-14 5.00E-15 1.86E-16 9.00E-13 2.25E-13 1.67E-14 6.00E-13 1.50E-13 1/1/2007 9.49E-16 9.00E-14 2.25E-14 6.81E-16 2.00E-14 5.00E-15 2.02E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 4/2/2007 1.08E-15 9.00E-14 2.25E-14 8.22E-16 2.00E-14 5.00E-15 2.26E-16 9.00E-13 2.25E-13 1.64E-14 6.00E-13 1.50E-13 7/2/2007 1.54E-15 9.00E-14 2.25E-14 8.16E-16 2.00E-14 5.00E-15 4.76E-16 9.00E-13 2.25E-13 2.12E-14 6.00E-13 1.50E-13 9/30/2007 4.90E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.65E-15 6.00E-13 1.50E-13 12/31/2007 1.46E-15 9.00E-14 2.25E-14 5.67E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.02E-14 6.00E-13 1.50E-13 3/31/2008 3.16E-16 9.00E-14 2.25E-14 6.17E-16 2.00E-14 5.00E-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 6.00E-13 1.50E-13 6/30/2008 3.13E-15 9.00E-14 2.25E-14 1.55E-15 2.00E-14 5.00E-15 9.27E-16 9.00E-13 2.25E-13 7.40E-15 6.00E-13 1.50E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal= 2.2SE-14 uCi/ml ALARAGoal= 5E-13 uCi/ml ALARA Goal = 2.2SE-13 uCi/ml ALARAGoal= l.SE-13 uCi/ml Pre 1994 MPC Umlt = SE-12 uCi/ml Pre 1994 MPC Li mit = 8E-14 uCi/ml Pt'e 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL-SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.2SE-14 2.00E-14 S.ooE-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 12/31/2008 9.00E-14 2.25E-l4 l.00E-l4 5.00E-15 9.00E-13 2.25E·13 6.00E-13 1.50E·13 3/15/2009 4.13E-15 9.00E·14 2.25E-l4 1.39E-15 2.00E·14 S.00E-15 1.41E·15 9.00E-13 2.25E·13 4.66E-15 6.00E-13 1.50E-13 6/15/2009 2.31E-16 9.00E·14 2.25E-14 7.79E-16 2.00E-14 S.00E-15 6.37E-16 9.00E-13 2.2SE·13 4.18E-15 6.00E-13 1.50E·13 9/15/2009 3.10E-15 9.00E-14 2.25E·14 9.20E·16 2.00E·14 S.00E-15 6.36E-16 9.00E-13 2.25E-13 1.21E-14 6.00E·13 1.50E-13 12/15/2009 5.77E·15 9.00E-14 2.25E-14 3.13E-16 2.00E-14 S.00E·15 1.92E-16 9.00E-13 2.2SE-13 2.48E-15 6.00E-13 1.50E-13 3/31/2010 4.78E-1S 9.00E-14 2.2SE-14 3.73E·16 2.00E-14 S.00E·1S 4.19E·16 9.00E-13 2.2SE-13 1.30E·14 6.00E-13 l.S0E·13 6/30/2010 4.3SE·l5 9.00E-14 2.25E·14 7.84E-16 2.00E·14 S.00E-1S 1.05E-1S 9.00E-13 2.2SE-13 4.40E-15 6.00E·13 1.50E-13 9/30/2010 3.57E-1S 9.00E-14 2.2SE·14 1.14E-15 2.00E·14 S.00E-15 7.97E-16 9.00E-13 2.2SE-13 3.78E·lS 6.00E·13 1.S0E·13 12/31/2010 8.S2E-1S 9.00E-14 2.2SE-14 1.4SE-15 2.00E·14 S.00E-15 1.29E-1S 9.00E-13 2.2SE·13 1.33E-14 6.00E·13 1.50E-13 4/4/2011 3.20E-1S 9.00E-14 2.2SE-14 8.89E-16 2.00E·14 S.00E-15 1.10E-1S 9.00E-13 2.2SE-13 1.48E·14 6.00E-13 1.50E-13 7/4/2011 6.98E-1S 9.00E-14 2.25E·14 2.03E-lS 2.00E-14 S.00E·1S 2.52E-1S 9.00E-l3 2.2SE-13 1.08E·l4 6.00E-13 1.50E-13 -----_ .. ---- -E :'::::: (.) ::l -II) c o '; a.. -C C1) (J c o (.) C1) "C (J ::l C o "C ca a: II) :> J: m (\J Co') ,.-,.- 0 0 W W a 0 ~ ~ .. ~ .=:; .. ~~ ~ lie ~ I. L.. ~ ~ ~ .. I,-- I~~ ~ t-... ~ ~ .. • ~ .:::;;; • 1 ~ ? • Iioi1III: ~ ~ .. l!"' ~.;::. ;~ ~ g: ~ l ~ ~ ,.- 0 W a ~ ~ -, i ll" N~ ~ jj o~-das 60-daS ... ..... 80-daS • --~ I-N ' ... - LO-daS 90-daS .~ r-~ ~ """"'-.. ~k ~ =-- go-das vo-das 80-daS a 'r"" (\J 0 ~ J. F' • 1--., ~~ t:::::. V 14 A - GO-daS "t:I (1j Q) W-daS --l + OO-daS co 66-daS (\J (\J 0 • ~ ~ .......... 86-das E :l '5 L6-daS (1j a: 96-daS + ~" ~ ::.;"" !.... ~ 96-daS a Co') (\J v6-daS 0 E :l _. 86-daS ";:: 0 .!: f- I:.:A' ~ ,. ~ -f-+""" G6-daS + ~6-das (ij 06-das ... :l 1U 6B-daS z E :l 88-daS "c (1j ~~. 14~ ~ ... L8-daS ~ + 98-daS gB-das W" ~ v8-daS 8B-daS I-... G8-das ~B-das L{) <D ,.... co ,.-,.-,.- 0 w 0 I W W w a 0 a a ~ ~ ~ ~ 'r"" ,.- (aIB:lS !50l) 1.00E-11 1.00E-12 1.00E-13 Q) n1 u CJ)1.00E-14 0> o ....J - 1.00E-1S 1.00E-16 1.00E-17 ~ .... co 6.. Q) CJ) Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml r ~ \. , C\J C') '<:t co co co 6.. 6.. 6.. Q) Q) Q) CJ) CJ) CJ) • • 1\ "..~ I _\ r LO co , 0. Q) CJ) co co , 0. Q) CJ) V¥1 I"-co 6.. Q) CJ) co co 6.. Q) CJ) I • \ ~ Q) co 6.. Q) CJ) ~ o Q) 6.. Q) CJ) l~ • .... 0> 6.. Q) CJ) I v. • C\J Q) , 0. Q) CJ) C') Q) , 0. Q) CJ) ~ r '<:t 0> 6.. Q) CJ) BHV-5 Uranium-Natural Concentrations (uCi/ml) ~ LO 0> 6.. Q) CJ) i 1* , co Q) 6.. Q) CJ) 'K .J I"-Q) , 0. Q) CJ) co 0> , 0. Q) CJ) \ .,. \, 1 ~~ Q) 0 Q) 0 6.. 6.. Q) Q) CJ) CJ) .... o 6.. Q) CJ) "-. . • \ 1 }l \ T ~ C\J o , 0. Q) CJ) , C') o , 0. Q) CJ) '<:t o , 0. Q) CJ) , LO o 6.. Q) CJ) co o 6.. Q) CJ) ~~ I"-o 6.. Q) CJ) co o , 0. Q) CJ) ~ -\. ,L •• 0> o , 0. Q) CJ) o .... 6.. Q) CJ) - en c o i ... -c CI) Co) c o (,) o C") ~ E ::l 'i: o .c l- Ll) :> ::I: m .-w o o (\J C".l .-.-, , w w 0 0 C! C! ~~ I. oa. '-- C ~ t:. ~~ ~~ r-tt. "<t .-, w 0 C! (alBos DOl) -;; ~ .... +- I--i.A. • 1--... h • ~ ~ f... ~ ~ t:::.. J :;:::::; -:;¥ ~ I--b- ~ ~ -....... . i.<I - [5 ~ It) T""" , w 0 C! T""" P ~ ....- ~ . (!) .-, w 0 C! .- - - - - - - - - - - "-T""" , w 0 C! .- o~-das 60-das BO-daS Lo-das 90-daS 90-daS vO-daS 80-das Go-das ~o-das OO-daS 66-daS B6-daS L6-daS 96-daS 96-das v6-daS 86-das G6-das ~6-das 06-daS 6B-daS BB-daS LB-daS 9B-daS 9B-daS vB-daS 8B-daS GB-daS ~B-das til C o ',t:j m 10... -C C\) U C o (.) CD C\I C\I • E j 'C m a: I.t) :> ::I: a:a W a C! T""" ~ ... 1- C\.I C') T""" T""" I I W W a a C! C! T""" I· ~:;:- ill .... ... ~ IlIoI ~ • 1::.. '~ ~r--.. ~ f".. v T""" I W a C! (alBos 001) ~ ~ ... W -- ..:::::::: ... • - R L!) T""" I W a C! HI'--b. .. ..... F='"'4 ~ ...... ~ ~ ~ 14~ It-~ P - . .."" -- ~ ~ -+- ~ I"li !. CD T""" I W a C! T""" - - " T""" I W a C! T""" o~-des 60-das 80-daS LO-deS 90-das so-des vO-deS 80-deS Go-des ~o-des OO-deS 66-deS 86-deS L6-deS 96-deS S6-deS v6-deS 86-daS G6-deS ~6-das 06-deS 68-des 88-deS L8-deS 98-das S8-das v8-daS 88-daS G8-daS ~8-des 1.00E-11 1.00E-12 1.00E-13 <D (ij o cl.l1.00E-14 0) o ....J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml • y /I" ..... /\.. 1\ J.. • • \ r... 1\ T • ,. ~ • "'-I ••• J "".I'JI \ I \ 1 ~ 1\ J\ • .. -.., V'i • .. ~~ .... ..... C\J C') '"<t LO <0 I'-00 (J) a ..... C\J C') 00 00 00 00 00 00 00 00 00 (J) (J) (J) (J) 0 6.. 6.. 6.. 6.. 0 0 6.. 0 0 6.. 6.. 6.. 0.. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J '"<t (J) 6.. Q) C/J BHV-5 Lead-210 Concentrations (uCi/ml) • ~ ~~ lJV ..... t t ~ •• ...... 11 & ... . .... -. • \I .. tI • • LO <0 I'-00 (J) a ..... C\J C') '"<t LO <0 I'-00 (J) a (J) (J) (J) (J) (J) a a a a a a a a a a 6.. 6.. 0 6.. 0 6.. 6.. 6.. 6.. 6.. 0 6.. 6.. 0 0 6.. a. a. 0.. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J C/J TAB 6 BHV -6 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit -9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal= 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = .\lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 12/14/1981 5.00E-12 .1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 3/29/1982 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 ;1..00E-12 6/30/1982 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 9/27/1982 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 I 1/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 I 4/4/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 6/30/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 10/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 I 1/3/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 4/2/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 7/2/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 10/1/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 1/2/1985 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 4/1/1985 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E·12 7/1/1985 5.00E·12 1.25E·12 8.00E-14 2.00E-14 2.00E·12 S.OOE·13 4.00E-12 1.00E-12 9/30/1985 5.00E·12 1.25E·12 8.00E-14 2.00E-14 2.00E·12 5.00E·13 4.00E-12 1.00E-12 1/2/1986 5.00E-12 1.25E-12 8.00E-14 2.00E·14 2.00E·12 5.00E-13 4.00E-12 1.00E·12 4/1/1986 5.00E·12 1.25E-12 8.00E-14 2.00E-14 <.OOE-12 5.00E-13 4.00E-12 1.00E·12 6/30/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 10/27/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1..00E-12 12/15/1986 .5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 3/16/1987 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 5/11/1987 5.00E·12 1.25H2 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E·12 1.00E-12 9/9/1987 5.00E-12 1.25E-12 8.00E·14 2.00E·14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/2/1987 5.00E·12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E·12 1.00E-12 2/16/1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 5/18/1988 5.00E-12 1.25E-12 8.00E-14 2.00E·14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/15/1988 5.00E-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/14/1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 2/13/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E·13 4.00E-12 1.00E-12 5/15/1989 5.00E·12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/14/1989 5.00E-12 1.25E·12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/13/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1,00E-12 2/12/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 5/14/1990 5.00E-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/13/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/12/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 2/11/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 1.00E-12 5/13/1991 5.00E-12 1.25E-12 8.00E·14 .2.00E·14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/12/1991 5.00E·12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/11/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E·12 1.00E-12 2/10/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4,00E-12 1,00E-12 5/11/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/10/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4_00E-12 1.00E·12 11/9/1992 5.00E-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 5.00E-13 4.00E·12 1.00E-12 2/9/1993 5.00E-12 1.25E-12 8.00E-14 2.00E·14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 5/10/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 1.00E-12 8/10/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/8/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E·13 4.00E·12 1.00E-12 2/7/1994 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 1.00E-12 5/9/1994 5.00E·12 .1.25E·12 8.00E-14 2.00E·14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/9/1994 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/7/1994 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = SE-13 uCi/ml "HV-6R Effluent Concentration Limit = 6E-13 uCi/ml "HV-6PB ALARAGoal= 2.2SE-14 uCilml ALARA Goal = SE-13 uCi/ml ALARAGoal= 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = 6E-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA '2/7/1995 9_00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 5/9/1995 9.00E-14 2.2sE-14 2.00E-14 s.00E-1s .9.00E-13 2.2SE-13 6_00E-13 LSOE-13 8/9/1995 9.00E-14 2.2sE-14 2.00E-14 5.00E-1S B.OOE-13 2.2sE-13 6.00E-13 LSOE-13 11/11/1995 9.00E·14 2.2sE·14 2.00E-14 S.00E-1s .9.00E-13 2.2SE-13 6.00E-13 LSOE-13 2/5/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 5/6/1996 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 LSOE-13 8/5/1996 9.00E-14 2.2SE-14 2.00E-14 .5.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.50E-13 11/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 2/6/1997 9.00E-14 2.2SE-14 2.00E-14 5.00E-1S 9.00E-13 2.2sE-13 6.00E-13 1.50E-13 5/5/1997 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 LsOE-13 8/11/1997 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 1.s0E-13 1/5/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-15 9.00E-13 2.2sE-13 6.00E-13 1.S0E-13 4/28/1998 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 1.s0E-13 7/31/1998 9.00E-14 2.2sE-14 2.00E-14 S.00E-1S 9.00E-13 2.2sE-13 6.00E-13 1.s0E-13 9/28/1998 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 1.s0E-13 12/28/1998 9.00E-14 2.2sE-14 2.00E-14 5.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.s0E-13 3129/1999 9.00E-14 2.2sE-14 2.00E-14 S.OOE-ls 9.00E-13 2.2sE-13 6_00E-13 1.S0E-13 7/3/1999 9.00E-14 2.2sE·14 2.00E-14 S.00E-1s 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 9/27/1999 3.03E-1s 9.00E-14 2.2sE-14 1.37E-1S 2.00E-14 S.00E-1S 8.72E-16 9.00E-13 2.2SE-13 7.SSE-1S 6.00E-13 1.S0E-13 12/28/1999 S.01E-1S 9.00E-14 2.2SE-14 2.89E-1S 2.00E-14 S.00E-1S 1.31E-1S 9.00E-13 2.2SE-13 8.lDE-lS 6.00E-13 1.S0E-13 3/30/2000 7.46E-16 9.00E-14 2.2SE-14 S.2SE-16 2.00E-14 S.00E-1S 3.00E-16 9.00E-13 2.2SE-13 7.83E-1S 6.00E-13 l.S0E-13 6/26/2000 S.40E-16 9.00E-14 2.2SE-14 3.S3E-16 2.00E-14 S.00E-1S 6.11E-16 9.00E-13 2.2SE-13 4.83E-1S 6.00E-13 1.S0E-13 9/25/2000 3.7SE-16 9.00E-14 2.2SE-14 2.23E-16 2.00E-14 S.00E-1S L91E-16 9.00E-13 2.2SE-13 6.41E-1S 6.00E-13 1.S0E-13 12/26/2000 S.21E-16 9.00E-14 2.2SE-14 3.39E-16 2.00E-14 S.00E-1S 3.28E-17 9.00E-13 2.2SE-13 8.S7E-1S 6.00E-13 1.S0E-13 3/26/2001 1.42E-16 9.00E-14 2.2SE-14 .l.00E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2SE-13 6.1SE-1S 6.00E-13 1.50E-13 7/2/2001 1.SlE-16 9.00E-14 2.2SE-14 1.66E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 6.9sE-1S 6.00E-13 1.S0E-13 9/24/2001 3.0SE-16 9.00E-14 2.2sE-14 1.01E-16 2.00E-14 S.00E-1S 1.77E-16 9.00E-13 2.2sE-13 S.59E-1s 6.00E-13 l.SOE-13 12/31/2001 3.31E-16 9.00E-14 2.2SE-14 1.2SE-16 2.00E-14 S.00E-1S 1.09E-16 9.00E-13 2.2sE-13 3.14E-1s 6.00E-13 l.SOE-13 I 4/1/2002 4.77E-16 9.00E-14 2.2SE-14 1.94E-16 2.00E-14 S.00E-1S 1.96E-16 9.00E-13 2.2sE-13 B.61E-1S 6.00E-13 l.SOE-13 7/1/2002 3.6SE-16 9.00E-14 2.2SE-14 4.41E-16 2.00E-14 S.00E-1S 1.76E-16 9.00E·13 2.2sE-13 iI.20E-lS 6.00E-13 1.S0E-13 9/30/2002 3.67E-16 .9.00E-14 2.2SE-14 5.60E-16 2.00E-14 S.00E-1S L80E-16 9.00E-13 2.2SE-13 S.SSE-1S 6.00E-13 l.SOE-13 12/30/2002 1.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1s l.67E-16 900E-13 2.2SE-13 l.3SE-14 6.00E-13 l.SOE-13 3/31/2003 1.98E-16 9.00E-14 2.2sE·14 L68E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2sE-13 l.77E-ls 6.00E-13 l.sOE-13 6/30/2003 1.lSE-16 9.00E-14 2.2SE-14 1.1sE-16 2.00E-14 s.OOE-ls 1.00E-16 9.00E-13 2.2sE-13 5.92E-ls 6.00E-13 l.sOE-13 9/29/2003 LOOE-16 9.00E-14 2.2sE-14 l.00E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.25E-13 8.30E-1s 6.00E-13 LsOE-13 '12/29/2003 1.00E-16 9.00E-14 2.2sE-14 1.36E-16 2.00E-14 s.OOE-lS l.00E-16 9.00E-13 2.2sE-13 6.66E-1s 6.00E-13 l.sOE-13 3/29/2004 1.00E-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.OOE-ls l.00E-16 9.00E-13 2.2sE-13 B.17E-1s 6.00E-13 LSOE-13 6/27/2004 l.00E-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2sE·13 3.SsE-lS 6.00E-13 LSOE-13 9/27/2004 ·l.00E-16 9.00E-14 2.2SE-14 1.3SE-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2SE-13 L22E-14 6.00E-13 LSOE-13 12/27/2004 l.OSE-16 9.00E-14 2.2sE-14 L72E-16 2.00E-14 s.OOE-lS l.00E-16 9.00E·13 2.2sE·13 Ls2E-14 6.00E-13 LSOE-13 3/2S/200S l.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 s.OOE-lS 1.00E-16 9.00E-13 2.2SE-13 9.34E-1s 6,00E-13 1.S0E·13 6}29/200s 1.2BE-16 9.00E-14 2.2sE-14 1.01E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 9.SsE-ls 6.00E-13 LsOE-13 9/26/2005 l.9SE-16 9.00E-14 2.2sE-14 S.9SE-16 2.00E-14 S.00E-1S 3.5SE-16 9.00E-13 2.2SE-13 1.71E-14 6.00E-13 1.s0E-13 1/3/2006 7.67E-16 9.00E-14 2.2sE-14 2.SSE-16 2.00E-14 G.00E-1S 3.60E-1s 9.00E-13 2.2sE-13 4.8SE-14 6.00E-13 1.S0E-13 4/3/2006 2.92E-16 9.00E-14 2.2sE-14 2.00E-16 2.00E-14 5.00E-1S 1.00E-16 9.00E-13 2.2sE-13 1.11E-14 6.00E-13 1.s0E-13 7/3/2006 3.2SE-16 9.00E-14 2.2sE-14 2.36E-16 2.00E-14 S.00E-1s 1.0SE-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 1.S0E-13 lD/2/2006 S.03E-16 9.00E-14 2.2sE-14 1.49E-16 2.00E-14 S.00E-1s 1.19E-16 9.00E-13 2.2SE-13 2.13E-1S 6.00E-13 1.S0E-13 1/1/2007 S.31E-16 9.00E-14 2.2sE-14 2.49E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E·13 2.2SE-13 1.70E-14 6.00E-13 1.S0E-13 4/2/2007 S.36E-16 9.00E-14 2.2SE-14 3.1SE-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2SE-13 1.43E-14 6.00E-13 1.S0E-13 7/2/2007 1.08E-1S 9.00E-14 2.2sE-14 2.1SE-16 2.00E-14 S.00E-1s 1.s4E-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 1.s0E-13 9/30/2007 3.92E-16 9.00E-14 2.2SE-14 1.02E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.3SE-ls 6.00E-13 1.50E-13 12/31/2007 2.92E-1S 9.00E-14 2.2SE-14 1.SSE-1S 2.00E-14 S.00E-1s 3.16E-16 9.00E-13 2.2SE-13 9.19E-1s 6.00E-13 l.S0E-13 3/31/200S 4.34E-16 9.00E-14 2.2sE-14 3.S1E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2sE-13 s.99E-1S 6.00E-13 1.s0E-13 6/310200S 1.SSE-IS 9.00E-14 2.2sE-14 9.00E-16 2.00E-14 S.OOE-IS 4.04E-16 9.00E-13 2.2sE-13 7.41E-ls 6.00E-13 1.s0E-13 - Date Effluent Concentration limit = 9E-14 uCi/ml BHV-6U Effluent Concentration limit = ZE-14 uCi/ml BHV-6T Effluent Concentration limit = 9E-13 uCi/ml BHV-6R Effluent Concentration limit = 6E-13 uCi/ml BHV-6PB ALARAGoal= Z.ZSE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= Z.ZSE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit" SE-lZ uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml pre 1994 MPC limit = 2E-IZ uCi/ml Pre 1994 MPC Limit = 4E-IZ uCi/ml Pre 1994 ALARA GOAL = l.ZSE-lZ uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-IZ uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 l.sOE-13 12/31/200S 9.00E-14 2.2sE-14 2.00E-14 S.00E-1s 9.00E-13 2.2sE-13 6.00E-13 l.sOE-13 3/15/2009 2.77E-1s 9.00E-14 2.2sE-14 1.01E-1s 2.00E-14 5.00E-1s 7.S2E-16 9.00E-13 2.2sE-13 6.46E-1s 6.00E-13 l.s0E-13 6/1S/2009 1.41E-16 9.00E-14 2.2SE-14 2.67E-16 2.00E-14 S.00E-1S l.SIE-16 9.00E-13 2.2SE-13 S.76E-1S 6.00E-13 1.S0E-13 9/1S/2009 4.S7E-IS 9.00E-14 2.2SE-14 4.32E-16 2.00E-14 5.00E-1S 2.BE-16 9.00E-13 2.2SE-13 8.98E-IS 6.00E-13 1.S0E-13 12/1S/2009 9.24E-1S 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.OOE-IS 1.1SE-16 9.00E-13 2.2SE-13 6.44E-1S 6.00E-13 1.S0E-13 3/31/2010 9.63E-1S 9.00E-14 2.2SE-14 l.S2E-16 2.00E-14 S.00E-1s 2.06E-16 9.00E-13 2.2SE-13 1.37E-14 6.00E-13 l.SOE-13 6/30/2010 3.62E-1S 9.00E-14 2.2SE-14 3.94E-16 2.00E-14 S.OOE-IS 4.S9E-16 9.00E-13 2.2SE-13 4.30E-1S 6.00E-13 1.50E-13 9/30/2010 s.42E-1S 9.00E-14 2.2SE-14 1.0SE-1S 2.00E-14 S.00E-1S S.6SE-16 9.00E-13 2.2SE-13 3.9SE-1S 6.00E-13 1.S0E-13 12/31/2010 l.24E-14 9.00E-14 2.2SE-14 1.21E-1S 2.00E-14 S.00E-1S 1.00E-1S 9.00E-13 2.2SE-13 1.S3E-14 6.00E-13 1.S0E-13 4/4/2011 2.70E-1S 9.00E-14 2.2sE-14 4.62E-16 2.00E-14 S.00E-1S 6.S1E-16 9.00E-13 2.2SE-13 1.29E-14 6.00E-13 1.S0E-13 7/4/2011 3.01E-1S 9.00E-14 2.2SE-14 7.07E-16 2.00E-14 S.00E-1S S.7SE-16 9.00E-13 2.2SE-13 7.97E-1S 6.00E-13 1.S0E-13 I/J s:::: o ; ca '--s:::: (1) u s:::: o o (1) "C U j s:::: .9 "C ca a:: CO :> ::I: m ==- C\J .-w .- K .-:= ~ ....l ....... ~ .-::: ~ .- I W I ~ S1~ ~ •• • =-4 ~ ~ ...... t.{) .-w .- ~. ~ ... Ci ~ "- ..::: ~ ~ 4 ~ ~ ~~"4! .~ ~~ ~ ~ ~ ~ '~ J ~ ~ ~ ~ CD .-w - - - - - -- GO 800e/08/6 SOOe/ge/6 a .-C\J eOOe/08/~ Q) --l + CD 666 ~/ LG/ERj E :J '0 ca a:: 966~/S/8 + a (t) C\J E :J 866~/O~/8~ l- t Cii 066~/8~/8~ z E :J C ~ L86~/6/6 + 1786 ~/~/O ~ ~86 ~/8e/6 1.00E-11 1.00E-12 1.00E-13 W n1 u Ul1.00E-14 OJ o d 1.00E-15 1.00E-16 1.00E-17 ..-<X) 0) ..---<X) ~ O'l Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.25E-14 uCi/ml Pre 1994 MPC Limit = 5E-12uCi/ml Pre 1994 ALARA Goal = 1.25E-12 uCi/ml """ I'-0 <X) <X) 0) 0) 0) O'l ..-..-..-------..-O'l CI') ----..-0 O'l --<X) CI') 0) O'l ..-0 ,.... --<X) BHV-6 Uranium-Natural Concentrations (uCi/ml) f ..I.. • .. T • 'J\ ~ r • ~~ y r \ 1 '9' V' ~ .~ i I . . co 0) C\J Ll) <X) 0) 0) 0 0 0 O'l O'l 0 0 0 ..-..-~ ~ ~ --t::: Ll) 0 0 --~ CI') ~ ~ <X) --O'l 0) O'l en c: o '';; f! -c: (1) (J c: o (.,) o M ('II I E ::::I 'i: o .c I- (0 ::> J: In ,.-.-w o o .- C\J C') .-.-I I UJ UJ 0 0 ~ ~ , , I'C !-. I.-- """ L() .-.-I W UJ 0 0 ~ ~ (alEos 501) .- It · ~ ~ It I. ~ 800e/08/6 ~ft - ~~ i::::="" P. ~~ 900e/ge/6 I~ ~~ ~ I-r-., ~ ~ I· t;; ~ eOOe/08/6 666~/LG/6 966 ~/9/8 866 ~/O ~/8 · 066 ~/8 ~/8 L86 ~/6/6 -· -v86 ~/~/O~ - ~86 ~/8e/6 <D t--,.-.- I I W UJ 0 0 ~ ~ ,.... 1.00E-11 1.00E-12 1.00E-13 Q) (ii u UJ1.00E-14 OJ o ~ 1.00E-1S 1.00E-16 1.00E-17 T""" co ()) T""" ...... co ~ ()) Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml , "<t ""-0 co co ()) ()) ()) ()) T""" T""" T""" ...... ...... ...... T""" ()) C') ...... ...... T""" 0 ()) ...... co \ , , , , , , C') ()) ()) T""" ...... 0 T""" ...... co BHV-6 Radium-226 Concentrations (uCi/ml) ~ II \ , , , <D ()) ()) ()) ()) ()) T""" T""" ...... ...... LO ""-...... C\l co ...... ()) N\ C\l 0 0 ~ 0 C') ...... ()) j LO o o ~ ~ .. T A ~,JJV , , co o o ~ o ~ ()) T I 1*_1 ." 1.00E-11 1.00E-12 1.00E-13 Q) (ij u oo1.00E-14 0> o ....J - 1.00E-15 1.00E-16 1.00E-17 - ,-co 0) ,--.... co ~ 0) Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCilml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1E-12 uCi/ml , " ..;t I"-co co 0) 0) ,-,--.... -.... ,-0) -.... -.... 0 0) 0 0) 0) ,--.... (Y) ,--.... co (Y) 0) 0) ,--.... 0 ,--.... co BHV-6 Lead-210 Concentrations (uCi/ml) <D 0) 0) ,--.... ~ co 0) 0) 0) ,- r:::: ~ ..... \, J. 1t , C\J o o ~ ~ 0) /' I AJ • LO o o ~ ~ ~ M o o ~ ~ t ~ .... I , " ATTACHMENT C AIR PARTICULATE LABORATORY RESULTS AND QAlQC EN:RGY www.energylab.COm Helens.MT877-472-o711 ·Billings.MT 800-735-4489 • Caspar, WY 888-235-0515 ~ ~ExuI/H&.smc. 1952 Gillette, WY 8&6-686-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-221 B •• '\: ~ .) i i ·"1 (,.): ., --------------~------~~~~~~~~~--~~~--~---------- May 29, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11040259 ANALYTICAL SUMMARY REPORT Project Name: 1 st Quarter BHV Air 2011 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 4/7/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test Cl1040259-001 BHV-l 04/04/11 00:00 04/07/11 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic Cll040259-002 BHV-2 04/04/11 00 :00 04/07/11 Filter Same As Above Cl1040259-003 BHV-4 04/04/11 00 :00 04/07/11 Filter Same As Above C 11040259-004 BHV-5 04/04/11 00:00 04/07/11 Filter Same As Above Cll040259-005 BHV-6 04/04/11 00 :00 04/07/11 Filter Same As Above Cl1040259-006 Blank 04/04/11 00:00 04/07/11 Filter Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAIQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: . /' • c?j/ "L~-__ .-(;{:(71':.::>. ( 't vV' ~ • Interi m Branch Manager Digitally signed by Steve Carlston Date: 2011.05.29 17:45:42 -06:00 Page 1 of 22 WWI'/.energylab.com AnI/ytIc.I &c.u.nt;. SIncI 1m Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-88&-7175 • Rapid City, SO 888-&72-1225 • College Station, IX 888-&90-221 B CLIENT: Denison Mines USA Corp Project: 1 st Quarter BHV Air 2011 Report Date: OS/29/11 Sample Delivery Group: Cll040259 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL{S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochem ical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreCiates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 EN:RGY l.;\L ..... :·r·,~~1 ,-:-: L~ www.energylab.com ~~Slnc. '151 Helena, MT 1111-472-0711 • Billings, MT 8011-135-4489 • Ca!per, WY 888-235-0515 Gillette, WY 8&&-686-7175 • Rapid City, SD 888-&72-1225 • College Stetion, TX 888-690-2218 mGH VOLUME AIR SAMPLING REPORT CLmNT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: lst Quarter BHV Air 2011 SAMPLE ID: BHV-l QuarterlDate Sampled Radionuclide Concentration Air Volume IlCilmL C 11040259-00 I nillU 9.0IE-16 First Quarter 20 II 230Th 1.90E-16 Air Volume in mLs 226Ra 3.64E-16 1.35E+II 2JOPb 1.09E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Counting Precision MDCIlCilmL IlCilmL N/A N/A 2E-17 3E-18 2E-17 2E-18 IE-16 8E-17 L.L.D.+ Effluent Conc.* % Effluent IlCilmL IlCilmL Concentration IE-16 9E-14 1.00E+00 IE-16 3E-14 6.32E-OI IE-16 9E-13 4.04E-02 2E-15 6E-13 1.82E+00 Page 3 of 22 EI\ERGY L/',-~8r L I C .,It-.- www.energylab.com AnIIyII~1 uClIiMwI SlRu 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-186-7175 • Rapid City, SO 888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter BHV Air 2011 C11040259-001 Client Sample 10 BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIOES -TOTAL lead 210 lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.179 121 1470 19 11 49.1 2.0 0.3 26 2.6 0.35 MDC -Minimum detectable concentration Units mglfiner pCilFilter pCi/Filter pCilFilter pCilFilter pCi/Filter pCilFilter pC ilFi Iter pCilFilter pC ilFi Iter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: OS/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 04/13/11 18:40 1 sml SW6020 04/13111 18:401 sml E909.0 05117/11 05:591 eli-cs E909.0 05117/11 05:591 eli-cs E909.0 05/17/11 05:591 eli-cs E903.0 04125/11 23:45 1 Irs E903.0 04/25/11 23:45 1 trs E903.0 04/25111 23:45 1 trs E908.0 05/02111 13:56 1 dmf E908.0 05/02111 13:56 1 dmf E90B.0 05/02111 13:56 1 dmf MCl -Maximum conta'Tlinant level. ND -Not detected at the reporting limit. Page 4 of 22 EI\ERGY :_i\l~r)I'(."-1 C;i I ·_~.:j www.energylab.com ~/buillnuShJu 1152 Helena, MT 811·472·0711 • Biflings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 86&·686· 7175 • Rapid City, SD 888·612·1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-2 QuarterlDate Sampled Radionuelide Concentration Air Volume IlCilmL CI1040259-002 nalU 3.79E-16 First Quarter 2011 23°Th 4.01E-17 Air Volume in mLs 226Ra 9.11E-17 1.31E+Il 210Pb 1.06E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-23D Week for Radium-226 Day for Lead-21D Counting Precision MDCIlCilmL IlCilmL N/A N/A 6E-18 2E-18 8E-18 2E-18 lE-16 8E-17 L.L.D.+ Effluent Cone. * % Effluent IlCilmL IlCilmL Concentration IE-16 9E-14 4.21E-Ol lE-16 3E-14 l.34E-01 lE-16 9E-13 I.OIE-02 2E-15 6E-13 1.76E+00 Page 5 of 22 EN:RGY '--,\ p~ _ J ,\ ~ ',) ." I" ~ m;J" www.energylab.com AIg/ylfc.IEx~.Si_ 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-612-1225 • CoUege Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1 st Quarter BHV Air 2011 C11040259-002 Client Sample 10 BHV-2 Analyses TRACE METALS Uranium Uranium. Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Ana/yte reporting limit. QCl -Quality control limit. Result 0.0735 49.8 1390 17 9.9 12.0 1.0 0.3 5.3 0.83 0.29 MOC -Minimum detectable concentration Units mg/filter pCVFilter pCVFilter pCilFilter pCilFilter pCVFilter pCVFilter pCilFilter pCVFilter pCVFilter pCVFilter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCL! QCL Method Analysis Date 1 By SW6020 04/13/11 18:451 sml SW6020 04/13/11 18:451 sml E909.0 05/17/11 12:361 eli-cs E909.0 05/17/11 12:361 eli-cs E909.0 05/17/11 12:36 1 eli-cs E903.0 04/25/11 23:45 1 trs E903.0 04/25/11 23:451 trs E903.0 04/25/11 23:451 trs E908.0 05/02111 13:561 dmf E908.0 05/02111 13:561 dmf E908.0 05/02111 13:561 dmf MCl -Maximum contcrninant level. NO -Not detected at the reporting limit. Page 6 of 22 EN:RGY L;,[J:">i /' 1", ,:-,IL !"~ , .. WI'IW.energylab.com AIII/rlial buliltlu ShICII!152 Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, S[) 888-672-1225 • College Station, 1X 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-4 Counting QuarterlDate Sampled Concentration Air Volume RadionucIide JlCilmL Precision CII0402S9-003 "'''V 1.29E-IS First Quarter 20 II 230Th 1.40E-16 Air Volume in mLs 226Ra l.S8E-16 1.2SE+ll 210Pb 1.11E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O JlCilmL N/A 2E-17 lE-17 lE-16 MDCJlCilmL N/A 3E-18 3E-18 8E-17 L.L.D.+ Effluent Conc.* % Effluent JlCilmL ,..CilmL Concentration IE-16 9E-14 1.44E+00 IE-16 3E-14 4.66E-Ol IE-16 9E-13 1.75E-02 2E-IS 6E-13 1.86E+00 Page 7 of 22 EN:RGY ,\~c)r ,-1' ... ·,\'_·: www.energylab.com ~/Ex""I/IC' SIne. 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Slation, lX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter BHV Air 2011 C11040259-003 Client Sample 10 BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIOES -TOTAL Lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOe Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Report Definitions: Rl -Anaiyte reporting limit. QCl -Quality control limit. Result 0.239 162 1400 17 9.9 19.7 1.4 0.4 18 2.0 0.35 MOe -Minimum detectable concentration Units mgtfilter pCi/Filter pCVFilter pCi/Filter pC i/Fi Iter pCVFilter pCVFilter pC VFi Iter pCVFilter pCi/Filter pCVFilter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 OateReceived: 04/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 04/13/11 18:491 sml SW6020 04113/11 18:49 1 sml E909.0 05/17/11 14:47 I eli-cs E909.0 05117/11 14:47 I eli-cs E909.0 05117/11 14:47 I eli-cs E903.0 04/25/11 23 :45 I trs E903.0 04/25/11 23:45 1 trs E903.0 04/25/11 23:45 1 trs E908.0 05/02111 13:56 1 dmf E908.0 05102111 13:561 dmf E908.0 05/02111 13 :56 I dmf Mel -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 22 EI\ERGY II' .j: r, I'·'-Ir...:'- www.energylab.com AMflbl ExuH_ Shtu "52 Helena,MT 811-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLEID: BHV-S Quarter/Date Sampled Radionuclide Concentration Air Volume IlCilmL C11040259-004 naLU 3.20E-15 First Quarter 20 I I 23DTh 8.89E-16 Air Volume in mLs 226Ra 1.l0E-15 l.32E+ll 210Pb 1.48E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B - Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Counting Precision MDCIlCilmL IlCilmL N/A N/A 8E-17 3E-18 3E-17 2E-18 2E-16 7E-17 L.L.D.+ Effluent Cone. * % Effluent IlCilmL IlCilmL Concentration IE-16 9E-14 3.56E+00 IE-16 3E-14 2.96E+00 IE-16 9E-13 1.22E-01 2E-15 6E-13 2.46E+00 Page 9 of 22 EN:RGY 1_/\ -~:::)I ','.1 (,' , .... ~::... www.energylab.com AM/yIJciJI ExulllllC' SIne. IIJ1 Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-0515 GII/ette, WY 8&&-&86-7175 • Rapid City, SD 888-672-1225 • Col/ege station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter BHV Air 2011 C11040259-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.624 423 1950 20 9.9 145 3.6 0.3 117 10 0.38 MOC -Minimum detectable concentration Units mglfi~er pC i/Fi Iter pCVFi/ter pCilFi/ter pCilFilter pCilFi/ter pCilFilter pCilFilter pCilFi/ter pCilFilter pCi/Fi/ter Qualifiers Rl 0.0003 0.2 Report Date: OS/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 04/13/11 19:091 sml SW6020 04113/11 19 :09 1 sml E909.0 05/17/11 16:591 eli-cs E909.0 05/17/11 16:59/ eli-cs E909.0 05/17/11 16:591 eli-cs E903.0 04/25/11 23:451 trs E903.0 04/25/11 23:45 1 trs E903.0 04/25/11 23 :45 1 trs E908.0 05/02111 13 :56 1 dmf E908.0 05/02111 13:561 dmf E908.0 05102111 13 :56 1 dmf MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 10 of 22 EN:RGY 1.:\£·"";1:";.' r'-,: -!1l:G m;J'. www.energylab.com AM/JIim £Xu'llne. ShrcI "52 Helena, MT 811·472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SO 888·672-1225 • College Station, TX 888-690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-6 QuarterlDate Sampled Radionuclide Concentration Air Volume ~CilmL CII040259-005 natU 2.70E-15 First Quarter 20 II 23D.yh 4.62E-16 Air Volume in mLs 226Ra 6.5IE-16 l.32E+Il 210Pb 1.29E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concenlration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O Counting Precision MDC~CilmL ~CilmL N/A N/A 4E-17 3E-18 2E-17 2E-18 lE-16 7E-17 L.L.D.+ Effluent Cone." % Effluent ~CilmL ~CilmL Concentration IE-16 9E-14 3.00E+00 IE-I 6 3E-14 1.54E+OO IE-16 9E-13 7.24E-02 2E-15 6E-13 2.14E+00 Page 11 of 22 EN:RGY ... i\~:')[U.I( '1-;'':; www.energylab.com AM/ytIt:II Ex~.u.nc. SiRClIW Halena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 . Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter BHV Air 2011 Cll040259-005 Client Sample 10 BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL Lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.527 356 1700 19 9.B B6.0 2.B 0.3 61 5.B 0.37 MOC -Minimum detectable concentration Units mglfilter pCVFilter pCVFilter pCilFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: OS/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 04/13/11 19:131 sml SW6020 04/13/11 19:131 sml E909.0 05/17/11 19:11 1 eli-cs E909.0 05/1711119:11/eli-cs E909.0 05/17/11 19:11 1 elks E903.0 04/25/11 23:45 1 trs E903.0 04/25/11 23:451 trs E903.0 04/25/11 23:451 trs E90B.0 05/02111 13 :56 1 dmf E90B.0 05/02111 13:56 1 dmf E90B.0 05/02111 13 :56 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 EN:RGY L~\·.~ :)n .. , I ' ;: 9. :L ~: www.energylab.com A~/Ex""_SlI1U "52 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: Blank QuarterlDate Sampled RadionucUde Concentration Air Volume "CilmL CII040259-006 n31U 1.22E-17 First Quarter 20 II 23~h 5.84E-19 Air Volume in mLs 226Ra 5.16E-18 1.36E+ll 210Pb -4.5IE-17 Counting Precision "CilmL N/A 2E-18 2E-18 4E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC"CilmL N/A 3E-18 3E-18 7E-17 L.L.D! Effluent Cone. >I< % Effluent "CilmL "CilmL Concentration lE-16 9E-14 l.35E-02 lE-16 3E-14 1.95E-03 IE-16 9E-13 5.73E-04 2E-15 6E-13 -7.5 I E-03 Page 13 of 22 EN:RGY /\'-::"':"jl ,,~r()~' l-:~ WNW.energylab.com Alu/ylic61 Ex",,-, smc. 1m Helona, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspor, WY 888-235-0515 GiJlette, WY 866-686-7175 • Rapid City, SD 888-612-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter BHV Air 2011 C 11040259-006 Client Sample 10 Blank Analyses TRACE METALS Uranium Uranium, Activity RADIO NUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0024 1.7 -6 5.8 9.9 0.7 0.3 0.3 0.08 0.30 0.37 MOC -Minimum detectable concentration Units mglfiHer pCi/Filter pCilFilter pCilFilter pCi/Filter pCilFilter pCi/Filter pCilFilter pC ilFi Iter pC ilFi Iter pCi/Filter Report Date: 05/29/11 Collection Date: 04104/11 OateReceived: 04/07/11 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date / By U u 0.0003 SW6020 0.2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. NO -Not detected at the reporting limit. 04/13/11 19:17/ sml 04/13/1119:17/ sml 05/17/11 21 :23/ eli-cs 05/17111 21 :23 / eli-cs 05/17/11 21 :23 / eli-cs 04/25/11 23 :45 / trs 04/25/11 23:45 / trs 04/25/11 23:45 / trs 05/02111 13:56/ dmf 05/02111 13:56 / dmf 05/02111 13:56 / dmf U -Not detected at minimum detectable concentration Page 14 of 22 EI\ERGY _,-,' ... ,-)I i,~ I (:: 'iL ', www.energylab.com AM/yllm Ezullll/lll. SIIIC. lW Helena, NT 877-472-0711 • Billings, MT 800-735-4489 • Casper, W'f 888-235-0515 Gillette, W'f 8&&-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 sl Quarter BHV Air 2011 Analyte Count Result Units Method: E903.0 Sample 10: LCS-29538 Radium 226 Sample 10: MB-29538 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: Cl1040296-001HMS Radium 226 Sample 10: C11040296-001HMSO Radium 226 Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 12.2 pCi/Filter 3 Method Blank 0.03 pCi/Filter 0.1 pCi/Filter 0.2 pCi/Filter Sample Matrix Spike 10 pCi/L Sample Matrix Spike Duplicate 9.2 pCi/L MDC -Minimum detectable concentration Report Date: OS/29/11 Work Order: C11040259 RL %REC Low LImit High Limit RPO RPOLimit Qual Run: TENNELEC-3_110419A 101 70 130 Run: TENNELEC-3_110419A Run: TENNELEC-3_110419A 101 70 130 Run: TENNELEC-3_110419A 93 70 130 8.7 NO -Not detected at the reporting limi!. U -Not detected at minimum detectable concentration Batch: R145159 04/25/11 23:45 04/25/11 23:44 U 04/26111 01 :24 04/26/11 01 :24 24.1 Page 15 of 22 EN:RGY _" -',)1 -'"It" l www.energylab.com AIuIytfa/ £1"1/_, S/nu lISt Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter BHV Air 2011 Analyte Count Result Units Method: E908.0 Sample 10: LCS-29538 Thorium 230 Sample 10: MB-29538 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Sample 10: C11040257-001AMS Thorium 230 Sample 10: C11040257-001AMSO Thorium 230 Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 10.9 pCi/Filter 3 Method Blank ·0.08 pCi/Filter 0.07 pCi/Filter 0.1 pCi/Filter Sample Matrix Spike 56.4 pCi/Filter Sample Matrix Spike Duplicate 57.7 pCi/Filter MDC -Minimum detectable concentration Report Date: OS/29/11 Work Order: C11040259 RL %REC Low Limit High Limit Run: EGG·ORTEC_11 0428B 111 70 130 Run: EGG-ORTEC_11 0428B Run: EGG-ORTEC_11 0428B 109 70 130 Run: EGG-ORTEC_11 0428B RPO RPOLlmit Qual Batch: R145606 05/02111 13:56 05/02111 13:56 U 05/02111 13:56 112 70 130 2.4 05/02111 13 :56 31 .B ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 16 of 22 EI\ERGY I.,\-~C)j ,t\l f __ 'I Z-<~ www.energylab.com AMJytI~1 rxCllmIl&. SIne. 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-&8&-7175 • Rapid CI1y, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter BHV Air 2011 Analyte Count Result Units Method: E909.0 Sample 10: C11040259-001AMSO Lead 210 Sample 10: C11040259-001AMS Lead 210 Sample Matrix Spike Duplicate 2250 pCi/Filter Sample Matrix Spike 2160 pCi/Filter RL %REC 73 65 Report Date: OS/29/11 Work Order: Cl1040259 Low Limit High Limit RPO RPOLimit Qual Batch: T _13784 Run: SUB-T40416 05/17/11 10:24 70 130 4.4 13.6 Run: SUB-T40416 05/17/11 08:11 70 130 S -Spike response is outside of the acceptance range for this analysis. Since the LCS and the RPD for the MS MSD pair are acceptable, the response is considered to be matrix related. The batch is approved. Sample 10: LCS-137B4 Lead 210 Sample 10: MB-13784 Lead 210 Lead 210 precision (±) Lead 210 MDC Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 279 pCi/Fliter 3 Method Blank -4 pCi/Filter 6 pCi/Fliter 10 pCi/Filter MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration 80 Run: SUB-T40416 70 Run: SUB-T40416 130 ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 05/17/11 03:47 05/17/11 01 :35 U Page 17 of 22 EN:RGY ~.I\-~Uh · ... '('; ',-. ~ www.energylab.com wlfllal fxullHel SIRu 1152 Helena, MT877-472-0711 • Billings, MT 800-135-4489 • Gasper, WY 888-235-0515 GilieHe, WY 866-886-7175 • Rapid City, SD 888-672-1225 • College station, TIC 888-690-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: OS/29/11 Project: 1 st Quarter BHV Air 2011 Work Order: C11040259 Analyte Count Result Units RL %REC Low Limit High Limit APO APOLlmlt Cual Method: SW6020 Batch: 29538 Sample 10: MB-29538 Method Blank Run: ICPMS4-C _11 0413A 04/13/11 18:28 Uranium 4E-05 mglfilter Sample 10: LCS2-29538 Laboratory Control Sample Run: ICPMS4-C_110413A 04/13/11 18:32 Uranium 0_107 mglfilter 0.00030 107 85 115 Sample 10: C11040259-006AMS Sample Matrix Spike Run: ICPMS4-C_110413A 04/13/11 19:21 Uranium 0.0588 mglfilter 0.00030 113 75 125 Sample 10: C11040259-006AMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_110413A 04/13/11 19:26 Uranium 0.0585 mglfilter 0.00030 112 75 125 0.4 20 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 18 of 22 EI\ERGY LAClOr"l\l Or(IL~ tFl~ www.energylab.com f ~ ~IExcsIIem:fSl_lm Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 886-686-7175 • Rapid City, SD 888-612-1225 • College Station, 1)( 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 11111111 ~IIIIIII~~ I~~ 111111111 mlli~ IIIII~ C11040259 Login completed by: Halley Ackerman Reviewed by: BL2000\kschroeder Reviewed Date: 4/14/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received wilhin holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0" Yes 0 Yes 0 Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" NA"C Yes 0 Yes 0 Date Received: 417/2011 Received by: ha Carrier 2Day name: No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 NoD No 0 No 0 No 0 Not Present 0 Not Present 0" Not Present 0" No VOA vials submitted 0" Not Applicable 0" Page 19 of 22 'U til co CD N o o -N N '«'rt~7 Chain of Custody and Analytical Request Record PLEASE PRINT (Provide as much information as possible.) A@eJ;ltl·U"'" Company Name: ~. . ~ !-2r"b~oJ tYl1N2~ Project Name, PWS, Permit, Etc, I Sample Origin / S-' QIA;z..n t! State: v..r Report Mail Addressi:? n-() t..~X 6-G7 'J5 (a nAlYl ~ /A '/ k'-lS'"11 Contact Name: Phone/Fax: Email: ~~ ~IWl6IL 61%-2tZI Invoice Address: / Invoice' Contact & Phone: Purchase Order: -St",",,-c ~~ page~ofL EPA/State Compliance: • Yes ~ No D Sampler: (Please Print) -ChArI' U~I Quote/Bottle 6r~ Special Report/Formats: &GMill, W©O@ ~@:®(!!J~@:@ ~ ... 1 Contact ELI prior to Shipped by: RUSH sample submittal 1.1)'PI Dow D EOO/EOT(Electronic Data) o POTWNVWTP Format: ____ _ D State: ___ _ n Other: ___ _ D LEVEL IV n NELAC o ~ ~O(/}~ ~co;gOI di '19> 0 »-c(/)~ ~ ~ 8~=a ~ en o~~I~I~ Io...(])~c·­ill CUll 0 o~ ~~I~ . 5 <1.>.= ii) ~ z"'C. «I C) 0 ~ ~1 (/) ~~J ~. ~-S-A-M-P-L-E-I-DE-N-T-IF-IC-A-T-IO-N--,----.----r---~ . ~ (Name. Location, Interval, etc.) ~ 1BJtv _1 I \/~ 11>--4 1)(1 ~I X I X 215 JhJ -2. , /I I I I I I X I Xl)( I 'x 3JS.}t1/ ~ II I l I ' I , X I X I X ~y 4 tIN ~ ~ I ) I I . I I I X h< I X I X 51JH~ ~ I _J I I I I Ix Ix lx li 6 :Kla r\ ~ I'PeuwllJ_ ' It) -A I i lLl x l X 7 9 10 Custody Sign!!lUre: Rece" R~o~ ~- o ~ W C I "0 () c « e ~ (II ~ E .-r' .::1 ..... r- W "0 W ro (f) -g .!!l (/) R I for charges and scheduling -See Instruction Page U I Comments: 5 H 1sJ~ Receipt Temp V\)i~ On Ice: Custody Seal On Bottle On Cooier Intact Signature Match I~ I~ I{Q) IlruL ~ I'=' i~ ~ ~ I~ ~ °C vQt, Y N o N (3N (9N ~b40~ It:::::!. MUSTber---------------------------------~~~~~--~~--------~~ __ ----~ s. y a raory: Igned Sample Disposal: Return to Client: . Lab Disposal: .•. --., ~ In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. www.energylab.com AMIytIt2I r-JlHc. S/I/U 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-612-1225 • College StatiDn, TX 888-&80-2218 ANALYTICAL SUMMARY REPORT August 07, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: Cll070215 Project Name: 2nd Quarter BHV Air 2011 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 7/7/2011 for analysis. Sample 10 Client Sample ID Collect Date Receive Date Matrix Test Cll070215-001 BHV-l 07/04/11 00:00 07/07/11 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic Cll070215-002 BHV-2 07/04/11 00:00 07/07/11 Filter Same As Above Cll070215-003 BHV-4 07/04/11 00:00 07/07/11 Filter Same As Above Cll070215-004 BHV-5 07/04/11 00:00 07/07/11 Filter Same As Above Cll070215-005 BHV-6 07/04/11 00 :00 07/07/11 Filter Same As Above Cll070215-006 Blank 07/04/11 00:00 07/07/11 Filter Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAIQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as rece ived basis unless otherwise indicated. Samples corrected for dry weight indicate units that have -dry appended. If you have any questions regarding these test results, please call. / /'" Report Approved By: ... l-{~(;7b n~ ,'/. Interim Branch Manager Digitally signed by Steve Carlston Date: 2011 .08.07 13:58:26 -06:00 Page 1 of 22 www.energylab.com AMJtIkMEIdn&.S/IJu 1m Helena, MT 811-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&·&8&-7175 • Ra id C ,SD 888-&72-1225 • Colle e Station, TX 888-&80-221 B CLIENT: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Report Date: 08/07/11 Sample Delivery Group: C11070215 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun . GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTI FICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysiS data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 EN:RGY • /',U:"')I/~\I L f.?1l '.J www.energylab.com AM/JfIaI~SbIcIII5Z Halena, MT 877-472-0711 • Bil/ings, MT 108-735-4489 • Casper, 'NY 181-235-0515 Gillatto, WY 168-888-7175 • Rapid City, SD 118-&72-1225 • Collage Station, IX 188-&90-2211 HIGH VOLUME AIR SAMPLING REPORT CLmNT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-l Quarter/Date Sampled Radionuclide Concentration Air Volume JlCilmL CII040259-001 naLU 9.0IE-16 First Quarter 2011 230Th 1.90E-16 Air Volume in mLs 226Ra 3.64E-16 1.35E+ll 210Pb 1.09E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume JlCilmL Cl [070215-001 nalU 1.59E-15 Second Quarter 20 II 230Th 5.31E-16 Air Volume in mLs 226Ra 4.99E-16 1.38E+II 210Pb 8.38E-15 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 2E-17 2E-17 IE-16 Counting Precision JlCilmL N/A 5E-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJlCilmL N/A 3E-18 2E-18 8E-17 MDCJlCilmL N/A 4E-18 3E-18 lE-16 L.L.D.+ Eftluent Cone. * % Eftluent JlCilmL JlCiImL Concentration lE-16 9E-14 1.00E+00 IE-16 3E-14 6.32E-OI IE-16 9E-13 4.04E-02 2E-15 6E-13 1.82E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 I.77E+oo lE-16 3E-14 I.77E+OO lE-16 9E-13 5.54E-02 2E-15 6E-13 1.40E+00 Page 3 of 22 EN:RGY ~ /\1:::!01'/" ( .... '41:... ~ WYtW.energylab.com .. /Ttkllb~.~ 1m Helena, MT 817-412-11711 • Billings, MT BGO-735-4489 • Casper, WY 881-235-1515 Gillette, WY 888-188-7175 • Rapid City, SD 188-172-1225 • College Station, IX 188-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11070215-001 Client Sample ID BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. Result 0.323 219 1150 23 14 6B.B 2.B 0.4 73 7.2 0.60 MOC -Minimum detectable concentration Units mglfilter pCilFilter pCi/Filter pCilFiiter pCilFilter pC ilFi iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 07/13/11 15:221 sml SW6020 07/13/11 15:22/ sml E909.0 07/2B/11 16:541 eli-cs E909.0 07/2B/11 16:541 eli·cs E909.0 07/2B/11 16:541 eli·cs E903.0 07/20/11 21 :551 trs E903.0 07/20/11 21 :55 / trs E903.0 07/20/11 21 :55 1 trs E90B.0 07/26/11 15:461 dm! E90B.0 07/26/1115:461 dm! E90B.0 07/26/11 15:461 dm! MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 22 EN:RGY l J\! lor,./\I '~.UJE ~ www.nrgylab.com AIIIITtfaI ~ SIIru 'lIZ Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 868-186-1175 • Rapid City, SD 888-672-1225 • College Station, TX 888-S90-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-2 Quarter/Date Sampled Radionuclide Concentration Air Volume IlCilmL C II 040259-002 nalU 3.79E-16 First Quarter 20 II 230Th 4.0IE-17 Air Volume in rnLs 226Ra 9.l1E-17 1.3IE+II 2IOPb 1.06E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume IlCilmL CII0702lS-002 nalU 3.07E-16 Second Quarter 20 II 230Th 8.S4E-17 Air Volume in rnLs 226Ra 9.21E-17 1.38E+ll 210Pb 7.2IE-lS +lLD's are from Reg. Guide 4.14 Counting Precision IlCilmL N/A 6E-18 8E-18 IE-16 Counting Precision IlCilmL N/A 1E-17 9E-18 lE-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCIlCilmL N/A 2E-18 2E-18 8E-17 MDCIlCilmL N/A 3E-18 3E-18 9E-17 LL.D.+ Effluent Cone. * % Effluent IlCilmL IlCiImL Concentration IE-16 9E-14 4.2IE-OI IE-16 3E-14 1.34E-OI IE-16 9E-13 1.0 I E-02 2E-IS 6E-13 l.76E+OO L.L.D.+ Effluent Conc.* % Effluent IlCiImL IlCilmL Concentration lE-16 9E-14 3.4lE-OI lE-16 3E-14 2.8SE-OI 1E-16 9E-13 1.02E-02 2E-IS 6E-13 1.20E+00 Page 5 of 22 EN:RGY , 1\':'1 ..... )1 11\1 Clll·_· ... www.energylab.com AM/yIkM w.u.-SbIU 1m Helena, MTB17-472-D711 • BIllings, MT 800-735-4489 · Casper, WY 881-235-0515 Gillette, WY 816-186-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-&80-221 a LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11070215-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIO NUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0625 42.3 994 19 12 12.7 1.3 0.4 12 1.7 0.46 MOC -Minimum detectable concentration Units mg/fi~er pCI/Filter pCi/Filter pCilFilter pCilFilter pCilFilter pCi/Filter pC ilFi Iter pCilFilter pC ilFi Iter pCI/Filter Qualifiers Rl 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 07/13/11 15:39 / sml SW6020 07/13/1115:391 sml E909.0 07128/11 20:121 eli-cs E909.0 07/28/11 20:12/ eli-cs E909.0 07/28111 20:12/ eli-cs E903.0 07/20/11 21 :55 / trs E903.0 07/20/11 21 :55 !trs E903.0 07/20/11 21 :55 !trs E908.0 07/26/11 15:46/ dmf E908.0 07/26/11 15:46 / dmf E908.0 07/26/11 15:46 / dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 22 EN:RGY I I\tJU',:", !...I./IL ~~ www.energylab.com AMI1tIa/~Shru '152 Halena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-888-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 mGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLEID: BHV-4 QuarterlDate Sampled Radionuclide Concentration Air Volume pCilmL CII040259-003 natu 1.29E-15 First Quarter 20 II 23~h 1.40E-16 Air Volume in mLs 226Ra 1.58E-16 l.25E+11 210Pb l.lIE-14 QuarterlDate Sampled Concentration Radionuclide Air Volume ",CilmL CII07021S-003 nalU 3.30E-IS Second Quarter 2011 230Th S.44E-16 Air Volume in mLs 226Ra 4.18E-16 1.17E+l l 210Pb 8.26E-15 +LLD's are from Reg. Guide 4.14 Counting Precision ",Ci/mL N/A 2E-17 lE-17 lE-16 Counting Precision ",CilmL N/A SE-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCpCilmL N/A 3E-18 3E-18 8E-17 MDC",CilmL N/A 6E-18 4E-18 lE-16 L.L.D.+ Effluent Cone. * % Effluent pCilmL ",CilmL Concentration lE-16 9E-14 1.44E+00 lE-16 3E-14 4.66E-OI lE-16 9E-13 1.75E-02 2E-15 6E-13 l.86E+00 L.L.D.+ Effluent Cone. * % Effluent ",Ci/mL ",CilmL Concentration lE-16 9E-14 3.66E+00 lE-16 3E-14 1.81E+00 lE-16 9E-13 4.6SE-02 2E-15 6E-13 1.38E+00 Page 7 of 22 EI\ERGY :\I:i(.)HAj C jIlL:"'" www.energylab.com AIJMtIIM ~ SIircI 1m Helena, MT871-472-11711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 88&-188-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11070215-003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 Lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. Result 0.571 386 967 19 12 49.0 2.5 0.4 64 6.1 0.73 MOC -Minimum detectable concentration Units mglfiHer pCVFilter pCVFilter pCVFilter pCilFilter pCI/Filter pC ilFi Iter pCVFilter pCilFilter pC ilFi Iter pCilFilter Qualifiers RL 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCL Method Analysis Date 1 By SW6020 07/13111 15:43/ sml SW6020 07/13/11 15:43 /sml E909.0 07/28/11 21: 18 / eli-cs E909.0 07/28/11 21 :18 / eli-cs E909.0 07/28111 21 :18 / eJi-cs E903.0 07/20/11 21 :5511rs E903.0 07/20/11 21 :5511rs E903.0 07/20/11 21 :5511rs E908.0 07/26/11 15:461 dmf E908.0 07/26/11 15:46 / dmf E908.0 07/26111 15:46/ dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 22 E"fRGY , )\' ~:::JH.·\I CHI! :..... www.energylab.com ANJrtIaI~SInu 'lSI Helena, MT 877-412-0711 • BIllings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&8&-7115 • Rapid City, SD 888-172-1225 • Collage Station, TX 888-680-2218 ffiGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV·S Quarter/Date Sampled Radionuclide Concentration Air Volume JlCi!mL C 11 040259-004 nalU 3.20E-15 First Quarter 20 II 230Th 8.89E-16 Air Volume in mLs 226Ra 1.l0E-15 1.32E+ll 2IOPb 1.4SE-14 Quarter/Date Sampled Concentration Radionuclide Air Volume JlCilrnL Cll070215-004 nalU 6.9SE-15 Second Quarter 2011 2JOTh 2.03E-lS Air Volume in mLs 226Ra 2.S2E-IS l.38E+ll 2IOPb 1.0SE-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A SE-17 3E-17 2E-l6 Counting Precision JlCilrnL N/A 2E-16 5E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJlCilmL N/A 3E-18 2E-IS 7E-17 MDCJlCilrnL N/A 6E-lS 3E-IS 8E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilrnL JlCilmL Concentration IE·l6 9E-14 3.56E+00 IE·16 3E-14 2.96E+00 IE·l6 9E-13 1.22E-01 2E·l5 6E-13 2.46E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration IE·16 9E-14 7.7SE+00 IE·16 3E-14 6.76E+00 IE·16 9E-13 2.80E·OI 2E·15 6E-13 l.SIE+OO Page 9 of 22 EI\ERGY ,\t 1 ... )1 I/'. I r -'1~ll -:... www.energylab.com AuI!IkM~SIItu 1151 Halans. MT877·472-0711 • Billings. MT 800·735·4489 . Casper. WY 888·235·D515 Gilletta. WY 888·186·7175 • Rapid City, SD 888·672·1225 • Collage Station, TX 888·690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper. WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11070215-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES • TOTAL lead 210 lead 210 precision (±) lead210MDC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.42 962 1490 23 12 347 6.6 0.4 280 25 O.BB MDC -Minimum detectable concentration Units mgifiHer pCilFilter pCilFilter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCVFilter pCVFilter pC ilFi Iter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 07/13/11 16:031 sml SW6020 07/13111 16:031 sml E909.0 07/28/11 22:241 eli-cs E909.0 07/28/11 22:241 eli-cs E909.0 07128111 22:24/ eli-cs E903.0 07/20/11 21 :55 / trs E903.0 07/20/11 21 :55 1 trs E903.0 07/20/11 21 :55 1 trs E90B.0 07/26/11 15:461 dmf E90B.0 07/26/11 15:461 dmf E908.0 07126/11 15:46/ dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 22 EN:RGY • /\' ) .• .)1.':1.1 :...·~r .... 1l :.... www.energylab.com AHIJfIaI bc.lIetIu SIne. '151 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 888-188-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-610-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-6 QuarterlDate Sampled Concentration Air Volume Radionuclide "CilmL CII040259-00S nalU 2.70E-15 firsl Quarter 20 II 2l0Th 4.62E-16 Air Volume in mL~ 226Ra 6.5IE-16 l.32E+II 2lUPb 1.29E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide "CilmL Cl1070215-005 na,V 3.01E-15 Second Quarter 2011 2l0Th 7.07E-16 Air Volume in mLs 226Ra 5.75E-16 l.38E+II 2!OPb 7.97E-15 +LLD's are from Reg. Guide 4.14 Counting Precision "CilmL N/A 4E-17 2E-17 IE-16 Counting Precision "CilmL N/A 7E-17 2E-17 lE-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Vranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC"CilmL N/A 3E-18 2E-18 7E-17 MDC"CilmL N/A 5E-18 3E-18 9E-17 L.L.D.+ Effluent Conc.* % Effluent "CilmL "CilmL Concentration lE-16 9E-14 3.00E+OO lE-16 3E-14 1.54E+00 IE-16 9E-13 7.24E-02 2E-15 6E-13 2.14E+OO L.L.D.+ Effluent Conc.* % Effluent "Ci!mL "CilmL Concentration lE-16 9E-14 3.35E+OO lE-16 3E-14 2.36E+OO IE-16 9E-13 6.39E-02 2E-15 6E-13 l.33E+OO Page 11 of 22 EI\ERGY _.\l::!OII,~,1 C I ~k J www.energylab.com Au/yIfu/ buIIfIlcf SIRu 1151 Helena, MT877-47Z-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-8515 Gillette, WY 88&-886-7115 • Rapid City, so a88-&72-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Den ison Mines USA Corp 2nd Quarter BHV Air 2011 C11070215-005 Client Sample 10 BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIOES -TOTAL lead 210 lead 210 precision (±l lead 210 MOC Radium 226 Radium 226 precision (±l Radium 226 MOC Thorium 230 Thorium 230 precision (±l Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.613 415 1100 20 12 79.2 3.1 0.4 97 9.3 0.75 MOC -Minimum detectable concentration Units mg/fiker pCVFilter pCVFilter pCVFilter pCVFilter pCVFilter pCi/Fllter pCVFilter pCi/Filter pCVFilter pCVFilter Qualifiers Rl 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07104/11 DateReceived: 07107/11 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 07/13111 16:071 sml SW6020 07/13/11 16:071 sml E909.0 07/28/11 23:301 eli-cs E909.0 07/28/11 23:30 1 eli-cs E909.0 07/28/11 23:301 eli-cs E903.0 07/20/11 21 :551 trs E903.0 07120/11 21 :551 trs E903.0 07/20/11 21 :551 trs E908.0 07126/11 15:46 1 dmf E908.0 07/26/11 15:46 1 dmf E908.0 07/26/11 15:461 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 EN:RGY L I\UC)l~./dUI<ll ~ www.energylab.com AaIytIaI ExWiltlclSInu '152 Helena, MT 877-472-0711 • Billings, MT 80'-735-4489 • Casper, WY 888-235-0515 Gillette, WY 811-186-7175 • Rapid City, SO 888-&12-1225 • College Station, 1X 888-610-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: Blank QuarterIDate Sampled Radionuclide Concentration Air Volume IICilmL CII040259-006 naLU 1.22E-17 FIrst Quarter 20 II 230Th S.84E-19 Air Volume in mLs 226Ra S.16E-18 1.36E+I I 110Pb -4.SIE-17 Counting Precision IICi/mL N/A 2E-18 2E-18 4E-17 Note: ThIS snmple uses J36,000,OOO L of aIr volume for comparison purpose.~. Counting QuarterIDate Sampled Concentration Radionuclide Precision Air Volume IICi/mL IICi/mL C1107021S-006 natu 1.0SE-I7 N/A Second Quarter 20 II 23~h 6.69E-18 2E-18 Air Volume in mLs 226Ra -4.89E-20 2E-18 l.36E+II 210Pb -8.89E-18 SE-17 Note: This sample uses 136,000,000 L of aIr volume for comparIson purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCIiCi/mL N/A 3E-18 3E-18 7E-17 MDCIiCi/mL N/A 2E-18 3E-18 9E-17 L.L.D.+ Effluent Cone. * % Effluent IICi/mL IICi/mL Concentration 1E-16 9E-14 1.3SE-02 IE-16 3E-14 1.9SE-03 IE-16 9E-13 S.73E-04 2E-IS 6E-13 -7.SIE-03 L.L.D.+ Effluent Cone. * % Effluent "Ci/mL "CiImL Concentration IE-16 9E-14 1.l7E-02 IE-16 3E-14 2.23E-02 lE-16 9E-13 -S.43E-06 2E-IS 6E-13 -1.48E-03 Page 13 of 22 EN:RGY r.l':lUhi\1 O t1'lL ~ www.energylab.com AM/yIII:M~SItIM 1m Halena, MT817·472-0711 • Billings, MT BOO·735·4489 · Casper, WY 888-235·0515 Gillatta, WY 88&·188·7175 . Rapid City, SD 888·872·1225 . College Station,IX 888-890-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11070215-006 Client Sample ID Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES • TOTAL lead 210 lead 210 precision (±l lead 210 MOC Radium 226 Radium 226 precision (±l Radium 226 MOC Thorium 230 Thorium 230 precision (±l Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0021 1.4 -1 7.1 12 -0.007 0.3 0.5 0.91 0.34 0.34 MOC -Minimum detectable concentration Units mg/fi~er pCi/Filter pCilFilter pCi/Filter pCi/Filter pCi/Filter pCilFilter pCi/Filter pCi/Filter pCi/Filter pCilFilter Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date 1 By 0.0003 SW6020 07/13/1116:12/sml 0.2 SW6020 07/13/1116:12/sml U E909.0 07/29/11 00:371 eli-cs E909.0 07129/11 00:371 eli-cs E909.0 07129/11 00:371 eli-cs U E903.0 07120/11 21 :55 1 trs E903.0 07/20/11 21 :55 1 trs E903.0 07120/11 21 :55 1 trs E90B.0 07/26/11 15:461 dmf E90B.0 07/26/11 15:461 dmf E90B.0 07/26/11 15:46 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 14 of 22 EI\ERGY .' A t .)1 j~~1 t.HI ' .. www.energylab.com Anl/flkll ExufIItlc.smu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-188-7175 • Rapid City, SD 888-812-1225 • College Station, 1X 888-&90-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: E903.0 Sample 10: MB-30350 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS·30350 Radium 226 Sample 10: C11061115·001HMS Radium 226 Sample 10: C11061115·001HMSO Radium 226 Qualifiers: RL -Analyte reporting limit. 3 Method Blank -0.1 pCi/Filter 0.1 pCi/Filter 0.3 pCi/Filter Laboratory Control Sample 23.8 pCi/Filter Sample Matrix Spike 24 pCi/L Sample Matrix Spike Duplicate 24 pCi/L MDC -Minimum detectable concentration Report Date: 08/07/11 Work Order: C11070215 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_11 0715A Run: BERTHOLD 770-2_11 0715A 101 70 130 Run: BERTHOLD 770-2_110715A 99 70 130 Run: BERTHOLD 770-2_11 0715A 103 70 130 1.4 ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: R148357 07/20/11 17:30 U 07/20/11 17:30 07/20/11 17:30 07/20/11 17:30 21.5 Page 15 of 22 EN:RGY www.energylab.com Helena, Mr 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-888-7175 • Rapid City, so 888-672-1225 • College Station, IX 888-690-2218 1\' :~)I .. \ I OH'!: !.... AlulyliIl6/ EJuU-. SI.Iu 1m QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: E908.0 Sample 10: C11070215-002AMS Thorium 230 Sample 10: C11070215-002AMSO Thorium 230 Sample 10: LCS-30397 Thorium 230 Sample 10: MB-30397 Thorium 230 Thorium 230 precision {±} Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike 108 pCi/Filter Sample Matrix Spike Duplicate 110 pCi/Filter Laboratory Control Sample 10.9 pCi/Filter Method Blank 0.2 pCi/Filter 0.1 pCi/Filter 0.1 pCi/Filter Report Date: 08/07/11 Work Order: C11070215 RL %REC Low Limit High Limit Run: EGG-ORTEC_11 0722A 101 70 130 Run: EGG-ORTEC_11 0722A 103 70 130 Run: EGG-ORTEC_110722A 110 70 130 Run: EGG-ORTEC_11 0722A ND -Not detected at the reporting limit. RPO RPOLimit Qual 1.4 Batch: 30397 07/26/11 15:46 07/26/11 15:46 29.5 07/26/11 15:46 07/26/11 15:46 Page 16 of 22 EN:RGY I\f \")1 U\.I (.'Ht'_ ~ rar www.energylab.com AMIfIIaI~SIRu llU Helena, MT 877·472-0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 8&&·&8&·7175 • Rapid City, SD 888·&72·1225 • Collaga Slation, 1X 888-&90-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: E909.0 Sample 10: C11 070215·001 AMSO Sample Matrix Spike Duplicate Lead 210 2450 pCi/Filter Sample 10: C11 070215·001 AMS Sample Matrix Spike Lead 210 2340 pCi/Filter Sample 10: LCS·14463 Laboratory Control Sample Lead 210 337 pCi/Filter Sample 10: MB·14463 3 Method Blank Lead 210 0.5 pCi/Filter Lead 210 precision (±) 7 pCi/Filter Lead 210 MDC 10 pCi/Filter Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC 121 117 95 Report Date: 08/07/11 Work Order: C11070215 Low Limit High Limit RPO RPOLimit Qual Batch: T _14463 Run: SUB-T41490 07/28/11 19:06 70 130 4.8 14.5 Run: SUB-T41490 07/28/11 18:00 70 130 Run: SUB-T41490 07/28/11 15:48 70 130 Run: SUB-T41490 07/28/11 14:42 U ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 17 of 22 EN:RGY /\ ~ ! ()J j. ~, C 'I « It' www.energylab.com AMIyfJm ~ SiIIa 1m Helena, MT 877-472-11711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-188-7175 • Rapid City, SD 188-872-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: SW6020 Sample 10: MB-30397 Method Blank Uranium 0.0001 mg/filter Sample 10: LCS2-30397 Laboratory Control Sample Uranium 0.109 mg/filter Sample 10: Cll070228-003AMS Sample Matrix Spike Uranium 9.48E-09 mg/filter Sample 10: Cll070228-G03AMSO Sample Matrix Spike Duplicate Uranium 9.43E-09 mg/filter Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 08/07/11 Work Order: C11070215 RL %REC Low Limit High Limit Run: ICPMS4-C_l10713A Run: ICPMS4-C~11 0713A 0.00030 109 85 115 Run: ICPMS4-C_11 0713A 0.00030 117 75 125 Run: ICPMS4-C_11 0713A 0.00030 116 75 125 ND -Not detected aI the reporting limit. RPO RPOLimit Qual Batch: 30397 07/13/1115:10 07/13/11 15:14 07/13/1116:32 07/13/11 16:36 20 Page 18 of 22 EN:RGY l /\. ,f .1-<.-, I f I II' "j www.energyiab.comHelena.MT877-472-0711 .Billlngs.MT 800-735-4489 • Casper, WY 888-235-0515 A4IIy/k:II rrcllh"".s.c. 1m Gillatta, WY 818-688-7175 • Rapid City, SD 888-872-1225 • Collega Station, TX 888-690-2218 Workorder Receipt Checklist IIIIIIIIIIIIIIIIIIIIIII~IIIIIIIIIIIIIUI~IIIIIIIIII Denison Mines USA Corp C11070215 Login completed by: Debra Williams Reviewed by: BL2000\kschroeder Reviewed Date: 7/7/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custocy agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0" Yes D Yes D Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" 'C NA Yes D Yes D Date Received: 7/7/2011 Received by: ckw No D No D No D No D No D No D No D No D No D No D No D No D Carrier 2nd Day Air name: Not Present D Not Present 0" Not Present 0" No VOA vials submitted 0" Not Applicable 0" Page 19 of 22 "U OJ (C CD N o o -N N 1#IN{r,y .'.,li.Uditt' Chain of Custody and Analytical Request Record Page _\ _ of _, _ PLEASE PRINT (Provide as much information as possible.) Project Name, PWS, Permit, Etc. I Sample Origin :;2. n d.. ~OJ"'-\er .;1..011 State: \AT Company Name: De.niso() M~t1~ EPA/State Compliance: Yes 0' No 0 Contact Name: Phone/Fax: Email: Sampler: (Please Print) Report Mail Address: PO B 0)(' B ICAf\a~~ v.."T ~09 8Y;)1 'R~o..r"\ ?~,~V" 43S ~ 78 ~ \ ~,..cr +JoH/dt4L '..J Invoice Address: SbV"1c:.. Special Report/Formats: Invoice Contact & Phone: .s~tyI<. ~ o ~ ~O U)~ ~(Il~OI :u {iillfI&[1" W@D@ rn1rn®lliJ~§[ID 0 UJ Purchase Order: Quote/Bottle Order: .. ~ I R t:.. Contact Ell prior to RUSH sample submittal for charges and scheduling -See Instruction Page t\P0:~ Cooler ID(s): ~ DDW o EDD/EDT(Electronic Data) o POTWfWWTP Format: ___ _ o State: ___ _ D LEVEL IV 'i§>~ i'C'rn cU)<i5 on $: 0:>= ~ CD u:>°o"" "0 « ~Iiiil ~ QjQ)"".-~ c.:m 0 Ci E~I16 ' RTIf7J-0C I '0 U C ~ e I U co Comments: On Ice: va Custody Seal ® On Bottle On Cooler Intact V N Signature y N Match :i~~I~~ ~ 0 ~~ 0 E >1 (Il- U'j <. <i r< r--S~AM~P~L~E~ID~E=N~T=IF-IC-A-T-IO-N---'-------'------~------~ ~ ~ ~ (Name, Location, Interval, etc.) MATRIX :::5 l-0' Cl- o Other: ----o NELAC t-E « :::J f-I S UJ 'E UJ co (J) '0 "" co Ci5 I H B~\J-I I~ \ i \3-A t'1.ir iJ{I'i I I I I I I I I I~ I: ~:~~~ I / I \ I I I { I i I ~ III I I i I I I I I ~ I 4 f>H" -5 I I I I I I I '...t.1 '" i Y.. I t...1 I I I I I I I I~ 5 \\\l\) -b I J I l'f i y: 1 1 1 ~ I I I I I I I I I I~ : BIMk 1~/~%1hr=' 113-A I j 11 1 ~ Ipi I I I I I I I I II 8 I~ D. 10 9 ~ II 6/01-JS- Custody Received by (prfrl:J: Data1Tim&: Signature: R ecord f-:!!'''''''''~~!'''7~P-'t'-----=''--~~~--LI-=>'''''-''''';::'--''''''~~'-L.-=--~wr.:..'''''I----1 Received by (print): DatelTime: Signature: MUST be r----------------------------------1h~~~~~~~--~::ft~~·e~'ffi~~~·~~----~~~~~~~~~u~~~:------------_1 Signed Sample Disposal: Return to Client: Lab Disposal; ,_I J 4 1.:,/) In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to ~certifled laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sUb-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA nol/S/9 nol/s/s nOl/S/t; nOl/S/E nOl/S/l nOl/S/T. oWl/sIlL oWl/sIn -OWl/S/OT. M \0 I E OWl/S/6 > :::c ........ co QO oWl/sIs T E -OWl/S/L LI') QO :> c: OWl/S/9 :::c .-co "'C + nJ oWl/sIs 0 ...... oWl/sIt; <:t I GJ > :::c .... OWl/S/E co nJ + -:::s OWl/S/l u .-N .... oWl/sIT. I '-> nJ :::c co 0.. 600l/S/1L + c: 600l/s/n 0 .-.-t .... 600l/S/0T. I nJ > :::c .... co V) 600l/S/6 + '-.-<C 600l/S/S 600l/S/L 600l/S/9 600l/S/S 600l/S/t; 600l/S/E 600l/S/l 600l/S/T. 0 0 0 0 .-t 0 0 0 .-t 0 0 0 .-t 0 0 0 .-t 0 0 0 .-i c:i c:i c:i c:i a a ~ ...... 0 0 ...... 0 a ...... a a ...... a a a a a a a 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 ~ IA-.:; D::J J: 10/5/2009 ., I ~~ < I 11/5/2009 1 17 ~ "'C 12/5/2009 1 I~ Q) ~ _. 1/5/2010 1 ~I~ n c: -2/5/2010 ] + Q) ~ c;I 3/5/2010 to I r-< 0 I 4/5/2010 ...... Q) 5/5/2010 1 --~ a.. ::::s 6/5/2010 -I ~ OQ -7/5/2010 -I r 3 OQ 8/5/2010 -I ~-........ 3 9/5/2010 1 I K: w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 0 0 !=l ~ 0 0 ~ 0 0 ~ 0 0 ~ 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 ~ F OJ :J: 10/5/2009 -I ~ < I 11/5/2009 -I 1 -N _=.I "'C 12/5/2009 -I 1 _____ OJ "'" r"t' -. 1/5/2010 -I 1-"" n r:: - + 2/5/20lD 1 ~ OJ r"t' OJ 3/5/2010 -r=: tD I r-< I 4/5/2010 0 N ~ OJ 5/5/2010 1 -~ Q. j 6/5/2010 1 ............... ---OQ -7/5/2010 1 -=:. 3 OQ 8/5/2010 1 ~-, 3 9/5/2010 -I .-w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 0 0 0 P I-' a a a I-' a 0 0 I-' 0 0 0 I-' 0 0 0 I-' 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 ~ I S o:J J: 10/5/2009 l .r---< I 11/5/2009 -I I ~ ~ "'C 12/5/2009 i k: -OJ ~ _. 1/5/2010 i ' r----.. n t: - 2/5/2010 1 + ~ OJ "' OJ 3/5/2010 tD :::r: r-< 0 .{:. 4/5/2010 OJ 5/5/2010 i -.~ a.. ::::J 6/5/2010 i ~ OQ -7/5/2010 i ~ 3 OQ 8/5/2010 i ~ ........ 3 9/5/2010 -l ~ w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 I ~ 4/5/2011 -I 5/5/2011 i I \-~ 6/5/2011 i 0 0 !=' ...... (:) (:) ...... (:) 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 ~ I ~ Cl ::I: 10/5/2009 -1 ~-< I U1 11/5/2009 -1 ..--a 12/5/2009 -! 1 ...6 OJ '""I ,... -. 1/5/2010 -I I ~ n C + 2/5/2010 ] OJ ,... III 3/5/2010 tD ::r: r-< 0 I 4/5/2010 U"I OJ 5/5/2010 -I -_--:::t. c. -. ::::J 6/5/2010 -1 ~ OQ -7/5/2010 -I r---3 OQ 8/5/2010 -1 ~ ........ 3 9/5/2010 -l ~ w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 0 0 !=> I-' 0 0 I-' 0 0 I-' 0 0 I-' 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 ~ 1,3 03 :J: 10/5/2009 -1 I ~ < I 11/5/2009 -I 17 en "'C 12/5/2009 -1 L~ C» ~ _. 1/5/2010 -1 I '~ n C - + 2/5/2010 ] C» .... OJ 3/5/2010 tD :r: r-< I 4/5/2010 0 0"1 C» 5/5/2010 -1 .. ~ a.. -. ::l 6/5/2010 l ~ OQ -7/5/2010 l ~" 3 OQ 8/5/2010 -1 ~ ......... 3 9/5/2010 -l ,~ w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 Period: January 4, 2011 through AprilS, 2011 (1st Quarter 2010) Page 1 BHV-1 on stream % 98.9% BHV-1 Total Volume: 4.76E+06 Week Filter Start Stop Stop Start Tolal Total Loading, Per Cent It Number Date Date Gross Tare Net 11me Time Time Liters mg/m3 On Stream SCFM I 8400769 3-J.n-11 10-Jan-11 4.3737 4.2875 0.0862 26673.8 26524.4 8962.8 9.263.636 0.0093 88.9% 36.5 2 8153706 1O-Jon-11 17-Jan-I I 4.5015 4.4591 0.0424 26838.4 26673.8 9876.6 10,347,944 0.0041 98.0% 37.0 3 8153701 17-Jan-11 24-Jan-ll 4_5169 4.4726 0.0443 27006.1 26838.4 10062.6 10.542.821 0.0042 99.8% 37.0 4 8400764 24-Jan-11 31-J.n-11 4.3489 4.2843 0.0646 27172.9 27006.1 10006.2 10,483.729 0.0062 99.3% 37.0 5 8400757 31-Jan-11 7-Feb-11 4.3670 4.2963 0.0707 27345.7 27172.9 10365.0 10,859,652 0.0065 102.8% 37.0 6 8400751 07-Feb-11 14-Feb-11 4.3523 4.2764 0.0759 27513.3 27345.7 10059.6 10.539.678 0.0072 99.8% 37.0 7 8400745 14-Feb-11 22-F<1r1 I 4.5413 4.3123 0.2290 27677.7 27513.3 9863.4 10,306,184 0.0222 85.6% 36.9 8 8400739 22-Feb-1 I 28-Feb-11 4.4408 4.3215 0.1193 27845.4 27677.7 10062.6 10,514.327 0.0113 116.5% 36.9 9 8400733 28-Feb-1 I 7-Mar-11 4.4423 4.3350 0.1073 28015.6 27845.4 10210.2 10.668.553 0.0101 101.3% 36.9 10 8400727 07-Mar-11 14-Mar-11 4.5000 4.4026 0.0974 28180.0 28015.6 9867.6 10.226.747 0.0095 97.9% 36.6 II 8153893 14-M.r-11 21-M.r-11 4.8345 4.5073 0.3272 28345.6 28180.0 9933.6 10.238.892 0.0320 98.5% 36.4 12 8153889 21-M.r-11 28-Mar-11 4.8549 4.5269 0.3280 28514.6 28345.6 10137.0 10,448.543 0.0314 100.6% 36.4 13 8153882 28-Mar-1I 4-Apr-1\ 4.7049 4.5399 0.1650 28683.6 28514.6 10144.2 10.455.964 0.0158 100.6% 36.4 Totals 91 2184.0 4.5214615 4.3862846 0.1352 129551.4 134,896,670 0.0131 99.2% 36.8 BHV-2 on stream % 96.1% BHV-2 Total Volume: 4.63E+06 Week Filter Start Slop Stop Start Total Total Loading, Per Cent # Number Date Date Gross Tare Net TTme Time Time Liters mg/m3 On Stream SCFM 1 8400768 03-Jan-ll 10-Jan-l1 4.3712 4.2694 0.1018 36802.9 36712.9 5402.4 5.583.731 0.0182 53.6% 36.5 2 8153707 10-Jan-l1 17-Jan-l1 4.5262 4.4670 0.0592 37029.8 36862.9 10011.6 10.489.387 0.0056 99.3% 37.0 3 8153702 17-Jan-l1 24-Jan-ll 4.5282 4.4970 0.0312 37195.4 37029.8 9936.6 10,410.808 0.0030 98.6% 37.0 4 8400763 24-Jan-l1 31-Jan-ll 4.4544 4.3125 0.1419 37362.7 37195.4 10042.8 10,522,076 0.0135 99.6% 37.0 5 8400756 31-Jan-ll 07-Felrll 4.4422 4.3025 0.1397 37534.8 37362.7 10324.8 10,817.534 0.0129 102.4% 37.0 6 8400750 07-Feb-l1 14-Feb-ll 4.5059 4.3179 0.1880 37702.0 37534.8 10033.2 10,512,018 0.0179 99.5% 37.0 7 8400744 14-Feb-ll 22-Felrll 4.6270 4.3174 0.3096 37866.8 37702.0 9888.0 10.331,889 0.0300 85.8% 36.9 8 8400738 22-Feb-l1 28-Feb-ll 4.4864 4.3244 I 0.1 620 38034.2 37866.8 10039.8 10,490,503 0.0154 116.2% 36.9 9 8400732 28-Feb-l1 07-Mar-ll 4.5879 4.3425 0.2454 38204.8 38034.2 10238.4 10,698,019 0.0229 101.6% 36.9 10 8400726 07-Mar-ll 14-Mar-ll 4_5913 4.3908 0.2005 38368.8 38204.8 9840.0 10,198,143 0.0197 97.6% 36.6 11 8153895 14-Mar-l1 21-Mar-l1 4.9000 4.5298 0.3702 38534.8 38368.8 9957.0 10,263,011 0.0361 98.8% 36.4 12 8153890 21-Mar-l1 28-Mar-ll 49993 4.4944 0.5049 38703.6 38534.8 10132.8 10,444.214 0.0483 100.5% 36.4 13 8153883 28-Mar-l1 04-Apr-l1 4.8264 4.5088 0.3176 38872.7 38703.6 10144.2 10,455.964 0.0304 100.6% 36.4 Totals 91 2184.0 4.60357 4.39034 , 0.2132 125991.6 131.217,295 0.0211 96.5% 36.8 BHV-4 on stream % 91.8% BHV-4 Total Volume: 4.42E+06 Week Filter Start Stop Stop Start Total Total Loading, Per Cent # Number Date Date Gross Tare Net TTme Time Time Liters mg/m3 On Stream SCFM 1 8400767 03-Jan-ll 10-Jan-ll 4.3533 4.2769 I 0.0764 12474.7 12359.4 6917.4 7,149,582 0.0107 68.6% 36.5 2 8153708 la-Jan-l1 17-Jan-ll 4.4982 4.4817 0.0165 12568.6 12474.7 5634.0 5,902.873 0.0028 55_9% 37.0 3 8153703 17-Jan-l1 24-Jan-ll 4.5059 4.4946 0.0113 12688.3 12568.6 7179.0 7.521,606 0.0015 71 .2% 37.0 4 8400762 24-Jen-l1 31-Jan-l1 4.3469 4.2909 0.0560 12856.8 12688.3 10109.4 10,591.854 0.0053 100.3% 37.0 5 8400755 31-Jan-l1 07-Feb-l1 4.3436 4.2679 0.0756 13027.7 12856.8 10254.0 10,743,355 0.0070 101.7% 37.0 6 8400749 07-Feb-l1 14-Feb-ll 4.3748 4.3028 0.0720 13196.3 13027.7 10119.0 10,601.912 0.0068 100.4% 37.0 7 8400743 14-Feb-ll 22-Felrl1 4.5247 4.3257 0.1990 13361.0 13196.3 9882.6 10,326.246 0.0193 85.8% 36.9 8 8400737 22-Feb-l1 28-Feb-ll 4.3452 4.2963 0.0489 13528.6 13361_0 10057.2 10,508.684 0.0047 t16.4% 36.9 9 8400731 28-Feb-l1 07-Mar-l1 4.4019 4.3119 0.0900 13699.3 13526.6 10240.2 10,699.900 0.0084 101.6% 36.9 10 8400725 07-Mar-ll 14-Mar-ll 4.5626 4.4265 0.1361 13863.1 13699.3 9824.4 10.1 e1 ,975 0.0134 97.5% 36.6 11 8153896 14-Mar-l1 21-Mar-l1 4.8648 4.5081 0.3567 14029.0 13863.1 9956.4 10,262.392 0.0348 98.8% 36.4 12 8153891 21-Mar-l1 28-Mar-l1 49032 4.5259 0.3773 14197.0 14029.0 10080.0 10.389.791 0.0363 100.0% 36.4 13 8153884 28-Mar-ll 04-Apr-ll 4.6763 4.5130 0.1633 14364.9 14197.0 10074.0 10.383.607 0.0157 99.9% J6.4 Totals 91 2184.0 4.51548 4.36632 0.1292 120327.6 125.263.778 0.0128 92.2% 36.8 BHV-5 on stream % 96.7% BHV-S Total Volume: 4.66E+06 Week Filter Start Stop Stop Start Total Total Loading, Per Cent # Number Date Dale Gross Tare Net Time Time Time Liters mg/m3 On Stream SCFM 1 8400766 03-Jan-ll 10-Jan-ll 4.4122 4.3042 0.1060 36193.2 36045.4 8868.6 9,166.274 0.0118 88.0% 36.5 2 8153709 10-Jan-ll 17-Jan-l1 4.5390 4.4721 0.0669 36328.5 36193.2 B116.2 8,503.532 0.0079 80.5% 37.0 3 8153899 17-Jan-l1 24-Jan-l1 4.6295 4.5336 0.0959 36482.6 36328.5 9246.0 9.687.250 0.0099 91 .7% 37_0 4 8400761 24-Jan-l1 31-Jan-l1 4.3723 4.2642 0.10Bl 36650.9 36482.6 10101.6 10.583.682 0.0102 100.2% 37.0 5 8400754 31-Jan-l1 07-Feb-l1 4.4108 4.2917 0.1191 36822.0 36650.9 10267.8 10,757,814 0.0111 101.9% 37.0 6 8400748 07-Feb-l1 14-Feb-ll 4.4055 4.2802 0.1253 369905 36822.5 10080.0 10.561,051 0.0119 100.0% 37.0 7 8400742 14-Feb-l1 22-Feb-l1 4.6182 4.3224 0.2958 37154.7 36990.5 9855.6 10,298.034 0.0287 85.6% 36.9 6 8400736 22-Feb-l1 28-Feb-ll 4.4709 4.3308 I 0.1401 37322.3 37154.7 10054.8 10,506.177 0.0133 116.4% 36.9 9 8400730 28-Feb-ll 07-Mar-ll 4.4675 4.3450 0.1 225 37492.8 37322.3 10228.8 10,687.988 0.0115 1015% 36.9 10 8400724 07-Mar-l1 14-Mar-l1 4.5828 4.4312 0.1516 37657.2 37492.8 9867.6 10,226.747 0.0148 97.9% 36.6 11 8153897 14-Mar-ll 21-Mar-l1 4.8945 4.5262 I 0.3683 37822.7 37657.0 9939.0 10,244,458 0.0360 98.6% 36.4 12 8153892 21-Mar-l1 28-Mar-l1 4.9667 4.5254 0.4413 37990.7 37822.7 10081.2 10.391.028 0.0425 100.0% 36.4 13 8153885 28-Mar-ll 04-Apr-l1 4.7820 4.5161 0.2659 38158_1 37990.7 10045.8 10.354.540 0.0257 99.7% 36.4 Totals 91 2184.0 4.58092 4.39562 0.1653 126753 131 ,968,574 0.0181 97.1% 36.8 Page 21 of 22 Period: January 4,2011 through AprilS, 2011 (1st Quarter 2010) BHV-6 on stream % Week Filter Start # Number Date 1 8400765 03-Jan-l1 2 6153710 10-Jan-l1 3 8153704 17-Jan-ll 4 6400760 24-Jan-ll 5 8400753 31-Jan-ll 6 8400747 07-Feb-l1 7 8400741 14-Fab-ll 8 8400735 22-Feb-l1 9 8400729 28-Feb-l1 10 8400723 07-Mar-l1 11 8153698 14-Mar-l1 12 8153688 21-Mar-ll 13 8153886 28-Mar-l1 Totals 91 ALL BHVon stream % Week /I Blanks Start Date 1 8153705 03-Jan-11 2 6153900 10-Jan-l1 3 8400759 17·Jan-l1 4 8400758 24-Jan-ll 5 8400752 31-Jan-l1 6 8400746 07-Feb-ll 7 8400740 14-Feb-l1 8 8400734 22-Feb-l1 9 8400728 28-Feb-ll 10 8153894 07-Mar-l1 11 8153887 14-Mar-ll 12 8153881 21-Mar-l1 13 8153875 28-Mar-ll Totals 91 96.7% Stop Date 10-Jan-ll 17-Jan-l1 24-Jan-l1 31-Jan-l1 07-Feb-ll 14-Feb-ll 22-Feb-ll 28-Feb-l1 07-Mar-ll 14-Mar-l1 21-Mar-ll 28-Mar-l1 04-Apr-l1 2184.0 96,1% Stop Dale 10-Jan-l1 17-Jan-ll 24-Jan-ll 31-Jan-ll 07-Feb-l1 14-Feb-ll 22-Feb-l1 28-Feb-l1 07·Mar-l1 14-Mar-ll 21-Mar-l1 28-Mar-ll 04-Apr-l1 2184.0 Gross 4.3800 4.4979 4.5260 4.3556 4.4589 4.4284 4.5313 4.4723 4.5319 4.5567 4.9076 4.9254 4.8300 4.56954 Net 4.4671 4.4608 4.2868 4.2449 4.3191 4.3180 4.3201 4.3008 4.3325 4.5203 4.4993 4.5035 4,5082 4.3940 Stop Tare Nat Time 4.2809 0.0991 1973.2 4.4556 0.0423 2108.6 4.4790 0.0490 2263.2 4.3033 0.0523 2431.3 4.3259 0.1330 2602.4 4.3027 0.1257 2770.9 4,2819 0.2494 2935.3 4.3251 0.1472 3102.9 4.3962 0.1357 3273.5 4.4225 0.1342 3437.6 4_5278 0.3798 3603.2 4.5292 0.3962 3771.3 4.5168 0.3132 3938.2 4.39592 0.1736 Page 2 BHV·6 Total Volume: 4.66E+06 Start Total Total Loading, Per Cent Time Time Liters mg/m3 On Stream SCFM 1825.3 8872.8 9,170,615 0.0108 88.0% 36.5 1973.2 8122.2 8,509,819 0.0050 60.6% 37.0 2106.6 9280.8 9,723,711 0.0050 92.1% 31.0 2263.2 10084.2 10,565,452 0.0050 100_0% 37,0 2431 .3 10263.6 10,753,413 0.0124 101.8% 37.0 2602.4 10108.8 10,591,226 0.0119 100.3% 37.0 2770.9 9867.6 10,310,573 0.0242 65.7% 36.9 2935.3 10056.0 10,507,430 0.0140 116.4% 36.9 3102.9 10235.4 10,694,884 0.0127 101.5% 36.9 3273.5 9848.4 10,206,648 0.0131 97.7% 36.6 3437.6 9936.0 10,241,365 0.0371 98.6% 36.4 3603.2 10080.6 10,390,409 0.0361 100.0% 36.4 3771.3 lOOL7.6 10.325,473 0.0303 99.4% 36.4 126774 131,991,218 0.0169 97.1% 36.8 Page 22 of 22 Period: April 5, 2011 through JulV 5, 2011 (2nd Quarter 2011) Page 1 SHV·1 on stream % 101.0% BHV-1 Total Volume: 4.67E+06 Week Filter Start Stop Stop Start Total Total loading, Per Cent It Nl.lmber Date Da te Gross Tare Net Time Time TIme Uters malm3 Qn Stream S CFM I 8153816 4-Apr·11 II-Apr-II 5.0637 4.4850 0.5787 28850.1 28683.6 9988.S 10.324.073 0.0561 99.1% 36.5 2 8153870 II-Apr-ll IS-Apr-II 4.7359 4.5115 0.2244 29018.4 28850.1 10096.2 10.578.024 0.0212 100.2% 37.0 3 3400721 18-Apr-1I 25-Apr-11 4.6449 4.4479 0.1970 29186.1 29018.4 10063_2 10.543.450 0.0187 99.8% 37.0 4 8400715 25-Apr-1 I 2-May-Ll 4.5507 4.4261 0.1246 29355.1 29186.1 10137.6 10,621.400 0.0117 100.6% 37.0 5 3400709 02-May-ll 9·May-ll 4.6184 4_3763 0.2421 29522.1 29355.1 10024.2 10.502,588 0.0231 99.4% 37.0 6 8400702 09-May-11 16-May·JI 4.5690 4.3920 0.1770 29688.9 29522.1 10006.8 10,484,358 0.0169 99.3% 37.0 7 8400997 16oMay-Ll 23-May-11 4.5190 4.3382 0.1808 29857.8 29688.9 10133.4 10,588,305 0.0171 100.5% 36.9 8 8400991 23-May-Ll 3O-M'ay-11 5.0540 4.3246 0.7294 30049.7 29857.8 11514.6 12,031,509 0.0606 114.2% 369 9 8400985 3()'May-ll 6-Jun-11 4.5512 4.3015 0.2437 30194.9 30049.7 8714.4 9.105.604 0.0268 86.5% 369 10 8153864 06-Jun-Il 13-Jun-11 4.8220 4.5244 0.2976 30J61.7 ]0194.9 10002.6 10.366,661 0.0287 99.2% 36.6 II 81.53858 13-Jun-11 20-Jun-11 4.6910 4.5195 0.1715 30529.7 30361.7 10080.0 10.389,79l 0.0165 100.0% 36.4 12 8400977 2().Jun-11 27-Jun-1 I 4.4738 4.3369 0.1369 30697.1 30529.7 10049.4 10.358,251 0.0132 99.7% 36.4 13 8400971 27-Jun-ll 4-Jul-1 I 4.6759 4.2996 0.3763 30890.6 30697.1 11604.6 11.961 .247 00315 115.1% 36.4 Tolals 91 2184.0 4.6899615 4.4068846 0.2831 132415.8 137.855.261 0.0263 101.0% 36.8 BHV-2 on stream % 101.0% BHV-2 Total Volume: 4.87E+06 Week Finer Start Stop Stop Start Total Total loading. Per Cent /I Number Dale Date Gross Tare Net Time Time TIme Utero mClt'm3 On Stream SCFM 1 8153677 04-Apr-11 II-Apr-l1 5.2444 4.5076 0.7366 39039.4 36672.7 10002.6 10.336.336 0.0712 99.2% 36.5 2 8153871 11-Apr-11 IS-Apr-11 4.6957 4.5359 0.3598 39207.5 39039.4 10087.2 10,568,595 0.0340 100.1% 37.0 3 8400720 16-Apr-11 25-Apr-l 1 4.7165 4.4149 0.3016 39374.8 39207.5 10035.6 10,514,532 0.0267 99.6% 37.0 4 8400714 25-Apr-11 02-May-lt 4.5849 4.4433 0.1416 39544.3 39374.9 10165.2 10,650,317 0.0133 100.8% 37.0 5 8400708 02-May-11 09-May-11 4.7269 4.4315 0.2954 39710.7 39544.3 9982.2 10,456.584 0.0262 99.0% 37.0 6 6400703 09-Mey-ll 16-May-11 4.6369 4.3848 0.2541 39676.1 39710.7 10047.0 10,526,476 0.0241 99.7% 37.0 7 8400996 16-May-11 23-May-l1 4.5604 4.3334 0.2270 40046.4 39878.1 10098.6 10,551,943 0.0215 100.2% 36.9 9 8400990 23-May-l1 30-May-11 5.1102 4.3271 0.7831 40238.3 40046.4 11512.2 t2.029.002 0.0651 114.2% 36.9 9 8400984 30-May-l1 06-Jun-11 4.6406 4.3157 0.3249 40363.0 40238.3 8680.2 9,069,669 0.0356 86.1% 36.9 10 8153665 06-Jun-11 13-Jun-11 4.9004 4.5266 0.3738 40550.9 40383.0 10076.4 10,443,147 0.0356 100.0% 36.6 11 6153659 13-Jl.ln-l1 2D-Jun-l1 4.7116 4.4687 0.2229 40716.3 40550.9 10042.2 10,350,629 0.0215 99.6% 36.4 12 8400976 20-Jun-11 27-Jun-11 4.6200 4.3166 0.3020 40665.6 40716.3 100~1.2 10,360,100 0.0292 99.7% 36.4 13 8400973 27-Jun·l1 04-Jul-l1 4.6613 4.3177 0.5436 41079.3 40665.6 \1610.0 11 ,966,613 0.0454 115.2% 36.4 Totals 91 2164.0 4.78557 4.41123 0.3743 132390.6 137,828,549 0.0349 101.0% 36.8 BHV-4 on stream % 65.9% BHV-4 Total Volume: 4.14E+OS Week Filter Start Stop Slop Start Total Total loading, Per Cent • Number Date Dete Gross Tare Net TIme TIme TIme UtelB mo/m3 On Stream SCFM 1 8153878 04-Apr-ll l1-Apr-11 4.9000 4.5215 0.3765 14530.6 14364.9 9952.8 10.266,865 0.0368 96.7% 365 2 9153672 l1-Apr-l1 18-Apr-l1 4.5120 4.5036 0.0084 14538.9 t4530.8 487.2 510,451 0.0165 4.8% 37.0 3 8400719 1B-Apr-l1 25-A~r-l1 4.6179 4.3733 0.2446 14703.8 1453B.9 9896.4 10,366,669 0.0236 96.2",(, 37.0 4 8400713 25-Apr-11 02-May-l1 4.6332 4.4070 0.2262 14874.3 14703.8 10229.4 10,717,561 0.0211 101.5% 37.0 5 8400707 02-May-11 09-May-11 4.4075 4.4192 -0.0117 15041.0 14674.3 10002.6 10,479,957 -0.0011 99.2% 37.0 6 8400704 09-May-11 16-May-11 4.5817 4.3967 0.1850 15207.9 15041.0 10012.2 10.490,016 0.0176 99.3% 37.0 7 8400995 16-May-l1 23-May-11 4.4659 42669 0.1990 15376.8 15207.9 10134.6 10,589,559 0.0186 100.5% 36.9 6 8400969 23-May-l1 30-May-l1 5.0688 4.3346 0.7542 15568.7 15316.8 11515.8 12,032,763 0.0627 114.2",(, 36.9 9 8400963 SO-May-11 06·Jun-11 4.6341 4.3246 0.3095 15713.4 15568.7 8679.6 9,069,242 0.0341 66.1% 36.9 10 6153B66 OS-Jun-11 13-Jun-11 4.7811 4.4954 0.2657 15679.9 15713.4 9987.6 10,351,115 0.0276 99.1% 36.6 11 B153860 13-Jun-11 20·Jun-tt 4.4954 4.5011 -0.0057 15879.9 15679.9 0.6 618 -9.2167 0.0% 36.4 12 8400975 2D-Jun-11 27-Jun-11 4.3639 4.2779 0.0860 16047.5 15679.9 10058.4 10.367.527 0.00B3 99.6% 36.4 13 8400969 27-Jun-11 04-Jul-11 4.7065 4.2765 0.4300 16240.0 16047.5 11546.4 11 ,901.256 0.0361 114.5% 36.4 Totals 91 2184.0 4.62985 4.39219 0.2377 112503.6 117.165,641 -0.6657 85.9% 36.8 BHV-5 on stream % 101.1% BHV-5 Total Volume: 4.B7E+06 Week Filler Start Stop Stop Slart Total Total loading, Per Cent • Number Date Dale Gross Tare Net Time TIme TIme Utero malm3 On Stream SCFM 1 B153679 04-Apr-11 l1-Apr-11 5.2932 4.5170 0.7762 36325.1 36158.1 10020.6 10,356,941 0.0749 99.4% 36.5 2 8153B73 11-Apr-11 18-Apr-l1 4.B720 4.5025 0.3695 38494.1 38325.1 10136.4 10,820,143 0.0348 100.8% 37.0 3 6400718 18-Apr-11 25-Apr-11 4.7131 4.4456 0.2675 38660.5 38494.1 9985.8 10,462,356 0.0256 99.1% 37.0 4 8400712 25-Apr.11 02-May-11 4.6483 4.4225 0.2256 38630.9 38660.0 10251.0 10,740.212 0.0210 101.7% 37.0 5 8400706 02-May-l1 09-May-l1 4.9720 4.3985 0.5735 38998.2 38830.9 10038.6 10,517,676 0.0645 99.6% 37.0 6 8401000 09-May-11 16-May-11 4.6046 4.3493 0.2553 39164.6 38998.2 9988.2 10,464,970 0.0244 99.1% 37.0 7 8400994 16-May-l1 23-May-11 4.5646 4.3331 0.2316 39333.4 39164.8 10124.4 10,578,901 0.0219 100.4% 36.9 8 8400988 23-May-11 SO-May-11 5.3001 4.2786 1.0215 39525.3 39333.4 1I517.0 12,034,017 0.0849 114.3% 36.9 9 8400962 3G-May-l1 06-Jun-l1 4.6633 4.3127 0.3506 39670.0 39525.3 8682.6 9,072,376 0.0386 96.1% 36.9 10 8153867 06-Jun-l1 13-Jun·l1 4.8722 4.5326 0.3396 39636.6 39670.0 9993.6 10,357,333 0.0328 99.1% 36.6 11 B153661 13-Jun.l1 20-Jun·11 4.6331 4.5085 0.3246 40005.6 39836.6 10143.0 10,454,727 0.0310 100.8% 36.4 12 6400979 2O-Jun-l1 27-Jun-11 4.4222 4.3139 0.1063 40172.7 40005.6 10020.6 10,32B,565 0.0105 99.4% 36.4 13 8400974 27-Jun-l1 04-Jul-l1 4.7935 4.3273 0_4682 40365.4 40172.7 11562.6 11,917.956 0.0391 114.7% 36.4 Totals 91 2184.0 4.61171 4.40324 0.4085 7797800 132464.4 137,906,073 O.03BO 101.1% 36.8 ""Pa eZlOTL. 9 Period: April 5, 2011 through July 5, 2011 (2nd Quarter 2011) SHV-6 011 stream % Week Fitter Start f Number Date 1 8153880 04-Apr-ll 2 8153874 II-Apr-II 3 8400717 18-Apr-ll 4 8400711 25-Apr-11 5 8400705 02-May-11 6 8400999 09-May-l1 7 8400993 16-May-l1 8 84009B7 23-May-l1 9 8400981 30-May-ll 10 8153868 OS-Jun-l1 11 8153B62 13-Jun-ll 12 8400980 20-Jun-l1 13 8400972 27-Jun-l1 Tolals 91 ALL BHV on stream % Week # Blanks Start Date 1 8153869 Q4-Apr-l1 2 8400722 l1-Apr-l1 3 8400716 1 a-Apr-l1 4 8400710 25-Apr-ll 5 8400701 02-May-11 6 8400998 09-May-l1 7 8400992 16-May-l1 8 8400986 23-May-l1 9 8153863 30-May-l1 10 8153857 06-Jun-11 11 8400918 13-Jun-11 12 8400970 20-Jun-l1 13 8153851 27-Jun-l1 Toteis 91 101.1% Stop Date l'-Apr·l1 18-Apr-l1 25-Apr-ll 02-May-ll 09-May-l1 16-May-ll 23-May-l1 30-May-l1 06-Jun-l1 13-Jun-11 20-Jun-ll 27-Jun-l1 04-Jul-il 2184.0 98.0% Slop Date l1-Apr-li 18-Apr-l1 25-Apr-l1 02-May-l1 09-MaV-11 16-May-l1 23-May-l1 3D-May.l1 06-Jun-11 13-Jun-11 20-Jun-l1 27-Jun-l1 04-Jul-11 2184.0 Gross 5.0261 4.8707 4.6669 4.6318 4.6670 4.4B94 4.4807 4.9981 4.5186 4.7920 4.6950 4.4575 4.6210 4.68575 Nel 4.4960 4.4061 4.4186 4.4222 4.4305 4.3180 4.2806 4.3208 4.5047 4.5049 4.3069 4.3220 4.6145 4.4038 Slop Tare Nel TIme 4.4999 0.5262 4105.4 4.5197 0.3510 4274.6 4.4378 0.2291 4441.4 4.4340 0.t978 4611.5 4.3952 0.2718 4778.2 4.3058 0.1836 4945.2 4.3315 0.1492 5114.0 4.3260 0.6721 5305.9 4_2751 0.2435 5450.3 4.5267 0.2653 5617.0 4.5055 0.1896 5785.7 4.3188 0.1387 5953.2 4.2719 0.3491 6145.6 4.39599 0.2898 Page 2 BHV·6 Total Volume: 4.87E+OB Start Total Total Loading, Per Cent Time Time Ulers mglm3 On Stream SCFM 3938.2 10033.2 10,369,964 0.0507 99.5% 36.5 4105.4 10150.2 10,634,601 0.0330 100.7% 370 4274.6 10008.6 10.486,244 0.0218 99.3% 370 4441.4 10205.4 10,692,436 0.0165 101.2% 370 4611.5 10001.4 10,478,700 0.0259 99.2% )70 4778.2 10020.6 10,498,816 0.0175 99.4% 37.0 4945.2 10126.2 10,580,182 0.0141 100.5% 36.9 5114.0 11517.6 12,034,644 0.0558 114.3% 36.9 5305.9 8662.8 9,051,687 0.0269 85.9% ]6.9 5450.3 9999.6 10,363,551 0.0256 99.2% 36.6 5617.0 10120.8 10,431,845 0.0162 100.4% 364 5786.7 10055.4 10,364,435 0.0134 99.8% 36.4 5953.2 11542.8 11.897.548 0.0293 114.5% 36.4 132444.6 137,665,253 0.0270 101 .1% 36.8 Page 22 of 22 ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA 50.00 45.00 40.00 35.00 30.00 ... Q) t:: 25.cta :::J ~ E Q) 20.~ 15.00 10.00 5.00 0.00 I I I White Mesa Mill Ambient Gamma Levels Over Time I t1 · J ~ ~ ~ ~ ~I~" ~j ~r • }f \ tt ~ ~ r. £v ~~ A rv ~ ~ V ~'J .11 ~J\ n / ~ 'i 'J to ~ V j Y. ~ Jj • ~IJ ~ - ~ !~L -ft n ~ "f ,R I ... " !III • \ -~ ~~* I -:.a R ~ ~ ;~ i"lm J"i n"irJ "l~~ OJ . ~ ,\j .. ~ ~ ___ .. 1'~!;.. _ ~ ~~ III ~ !:!!-.~ ~ m 30-SeP-81 05.JUI_B3 D4-A,pr-B5 03-Feb-Bl 11-oC1-BB 16-JUI_90 10-A,pr_92 13-Jan_94 16-0Ct_95 B-JUI-9l 13-A,pr_99 20-Feb-O 1 15-octo02 9-JUlo04 10_,/1_ 31-De 2-0ctoO "'~ro06 coOl 9 WHir£: M£:SA, MILL Background (BHV-3) subtracted from BHV-l, BHV-2, BHV-4, BHV-5, and BHV--6 __ BHV-1 ___ BHV-2 ......... BHV·3 --BHV-4 __ BHV-S -BHV-6 [White Mesa Mill Ambient Gamma Levels Over Time BHV-1 [ 50.00 ~------------------------------------------------------------------------------=====-------------------------------------- 45.00 ~I----------------------------------------------------------------------------------------------------------------- 40.00 +1--------------------------------------------------------------------------------------------------------------------~ 35.00 i----------------------------------------------------------------------------------------------------------------1 30.00 ~ Q) t ca 25.00 ::J 0-........ E Q) a: 20.00 E 15.00 10.00 i 1 1-1 ---------------------------------------t 5.00 1 • " _ I 1 • I . '~I 0.00 I ~ ~. i .. , ,:-:,. ~ "-W ...-:,:-: hlllllllilC """"'U.r,-I" W W· .. tIlAunAulI.r"". ,.,.~., .. :-:", i ' i .' ... 1 30-Sep_81 03-0ct_83 O?-Oct_85 09-0ct_8? 30-0ct_89 30-Sep_91 8-0ct_93 16-0ct_95 10-Nov_9? 12-0ct_99 24-0ct_01 3_0ct_03 1?-Oct_05 30-0ct_O? 2-0ct_09 Background (BHV-3) Subtracted from BHV-1 -'-SHV-1 , White Mesa Mill Ambient Gamma Levels Over Time BHV-21 50.00 45.00 40.00 35.00 30.00 ..... Q) t::: 25.00 CU ~ a---E Q) 20.00 a: E 15.00 10.00 ~ • 5.00 I n IH-I-.. .. J!r-I 0.00 ~s ~o ~Ot ~Ot ~Ot ~s ~ct ~Oct ~. ~O ~-o ~ct ~O ~-o ~ct ep-81 ct-83 c -85 c -87 c -89 ep-91 -93 -95 'vo"'-97 ct-99 ct-01 -03 ct-os ct-07 -09 Background (BHV-3) Subtracted from BHV-2 ,--------+-BHV-2 -- I White Mesa Mill Ambient Gamma Levels Over Time -BHV-3j 50.00 45.00 40.00 35.00 30.00 .... Q) 't 25.00 ctl :::::l ~ E Q) a: 20.00 E --ff ~, -~r w ~ • _ ~ It ~ l ~ ~I 4 __ !~! A n' ~ ~ V .~~ 1f\J \lf~ !. II ~ ~,~. • ~ . ~ -., ~, 15.00 10.00 5.00 0.00 ,., ., F , • ••••••• •• •• • • •••• ,. 30-Sep-81 03-0Ct_B3 07-0ct_BS 09-0ct_B7 30-0ct_B9 30-Sep_91 B-Oct_93 16-0ct_9S 10-Nov_97 12-0ct_99 24-0ct_01 3-0ct-03 17_0ct-os 3D-Oct_07 2-0ct_09 Background (BHV-3) __ BHV-3 [ White Mesa Mill Ambient Gamma Levels Over Time BHV-41 50.00 45.00 +1----------------------------------------------------------------------------------------------------- 40.00 l~---------------------------------------~ 35.00 1,---------------------------------------1 30.00 >-Q) t::: 25.00 ctS :J 0---E Q) a: 20.00 E 15.00 10.00' II 5.00' • I "-H"I' • ,,1-1------------------------\ 0.00 tIA·, ".",~. ,-,<" '" fl., i", iii .,41" ¥~ ! 'j"-,,~;-; ilJl!",,·.ii'., ¥. " ... iii ti'''-:=;'''-:;VW·.,:'j,'\Ii!iI' ~"'M 30-S 03-0 07-0 09-0 30-0 30-S B-Oct ep-B1 ct-B3 ct-Bs ct-B7 ct-B9 ep-91 -93 16-Oct 10-"0 12-0ct 24-0ct 3-0ct 0 17-0ct 3D-Oct 2-0Ct 0 -95 'y, 11-97 -99 -01 -3 '-Os '-07 - 9 Background (BHV-3) Subtracted from BHV-4 -_ .. _----- _BHV-4 I White Mesa Mill Ambient Gamma Levels Over Time BHv-51 50.00 45.00 40.00 35.00 30.00 ..... Q) t 25.00 ro ::J 0--E Q) C( 20.00 E 15.00 10.00 5.00 0.00 30-Sep_81 03-0Cl_83 O?-OCl_85 09_0Cl_8? 30-0Cl_89 30-Sep_91 8-0Cl_93 16-0Cl_95 10-Nov_9? 12-0Cl_99 24-0Cl_01 3-0Cl-03 1?_OC1_05 30-0Cf_O? 2-0C1_09 Background (BHV-3) Subtracted from BHV-5 --+-BHv-s-1 I White Mesa Mill Ainbient Gamma Levels Over Time SHv-sl 50.00 45.00 40.00 35.00 I 30.00 Qj 25.00 1:: ro :::l , I 0-I E 20.00 Q) a: E 15.00 10.00 5 . .00 0.00 ~ A~ .. .. .. ~ . .. , .. , .. " ~ .. .. "'------- ~ ~O ~o ~-M-~ ~ ~-mo. ~ ~-~ ~ ~ ~ ~ ~ ~~7M~ ~~ ~~~~~, ~ ~~7~ Background (BHV-3) Subtracted from BHV-6 r --SI1V·6 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 White Mesa Mill First Quarter 2011 Environmental Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Corner Ore Pad Met. Lab Filter Press Room BHV-l BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control # 2 Vault Mean Total Days Ambient Date Date Badge at Dose mReml Issued Returned WMM Equivalent hour 11712011 4/28/2011 11712011 4128/2011 11712011 412812011 1171201 1 4/28/20 I I 117/2011 4/28/2011 11712011 4/28/20 I I 117/2011 4128/2011 11712011 4/28120 I 1 11712011 4/28/2011 11712011 4/28/2011 11712011 4128/2011 11712011 412812011 11712011 4/2812011 11712011 4/28/2011 11712011 4/28/2011 11712011 4/28/2011 11712011 4/2812011 11712011 4128120 II 11712011 4/2812011 11712011 412812011 11712011 4128/2011 11712011 412812011 11712011 4128/2011 11712011 4/2812011 11712011 4128/2011 11712011 412812011 11712011 412812011 11712011 412812011 11712011 4/28/2011 117 120 I 1 4/28/20 11 11712011 4/28/2011 11712011 4/28/2011 11712011 4128120 II 11712011 412812011 11712011 4/2812011 11712011 4/28/2011 11712011 4/28/2011 11712011 4128/2011 11712011 4/28/2011 11712011 4/28/2011 11712011 4128/2011 III 111 III 111 III III 111 I 11 111 111 111 111 III III 111 III III 111 III 111 III III 111 111 111 III 111 III 111 111 111 111 111 111 111 111 111 III 111 111 111 38.9 59.8 32.7 961 119 165.4 297.8 357.7 125.4 98.8 337.3 215 85.4 214.6 41.7 34.3 34 38.2 42.2 471.1 144.6 89.1 102.8 49.9 106 871.4 421.9 112.8 65 .7 180.1 60.4 447.1 233.4 370.9 232.8 284 142.9 172 40.6 37.9 39 0.01 0.02 0.01 0.36 0.04 0.06 0.11 0.13 0.05 0.04 0.13 0.08 0.03 0.08 0.02 0.01 0.01 0.01 0.02 0.18 0.05 0.03 0.04 0.02 0.04 0.33 0.16 0.04 0.02 0.07 0.02 0.17 0.09 0.14 0.09 0.11 0.05 0.06 0.02 0.01 0.01 mReml Day 0.350 0.539 0.295 8.658 1.072 1.490 2.683 3.223 1.130 0.890 3.039 1.937 0.769 1.933 0.376 0.309 0.306 0.344 0.380 4.244 1.303 0.803 0.926 0.450 0.955 7.850 3.801 1.016 0.592 1.623 0.544 4.028 2.103 3.341 2.097 2.559 1.287 1.550 0.366 0.341 0.351 mReml Week 2.45 3.77 2.06 60.60 7.50 10.43 18.78 22.56 7.91 6.23 21.27 13.56 5.39 13.53 2.63 2.16 2.14 2.41 2.66 29.71 9.12 5.62 6.48 3.15 6.68 54.95 26.61 7.11 4.14 11.36 3.81 28.20 14.72 23.39 14.68 17.91 9.01 10.85 2.56 2.39 2.46 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 * Lost Badge White Mesa Mill Second Quarter 2011 Environmental Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Corner Ore Pad Met. Lab Filter Press Room BHV-l BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control # 2 Date Issued 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 Date Returned 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 Total Days Badge at WMM 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 Ambient Dose Equivalen t 27.7 34.9 24.8 487.9 71.5 162.2 220.9 73.7 60.6 225.9 49 143.3 26 24.2 22.4 21.5 25.6 282.1 90.9 55.7 65.2 27.8 66.6 623.7 220.1 75.2 44.7 104.3 38.3 284.5 152.4 244.1 246.4 126 33.4 56.1 25.1 21.3 mReml hour 0.02 0.02 0.01 0.29 0.04 0.10 0.00 0.13 0.04 0.04 0.14 0.00 0.03 0.09 0.02 0.01 0.01 0.01 0.02 0.17 0.05 0.03 0.04 0.02 0.04 0.38 0.13 0.05 0.03 0.06 0.02 0.17 0.09 0.15 0.15 0.08 0.02 0.03 0.02 0.01 mRem/Day 0.401 0.506 0.359 7.071 1.036 2.351 0.000 3.201 1.068 0.878 3.274 0.000 0.710 2.077 0.377 0.351 0.325 0.312 0.371 4.088 1.317 0.807 0.945 0.403 0.965 9.039 3.190 1.090 0.648 1.512 0.555 4.123 2.209 3.538 3.571 1.826 0.484 0.813 0.364 0.309 mReml Week 2.81 3.54 2.52 49.50 7.25 16.46 0.00* 22.41 7.48 6.15 22.92 0.00* 4.97 14.54 2.64 2.46 2.27 2.18 2.60 28.62 9.22 5.65 6.61 2.82 6.76 63.27 22.33 7.63 4.53 10.58 3.89 28.86 15.46 24.76 25.00 12.78 3.39 5.69 2.55 2.16 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QNQC (Log Scale) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I 6 I I 0 0 0 0 0 0 (Xl -....J OJ (J1 """ VJ I\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 ~ 8/27/1987 - 8/27/1988 -I ~ 1 JJ Q) I 8/27/1989 -I I -~ N N Q) 8/27/1990 -I ~ 0 0 8/27/1991 ~ II~ ~ n CD 8/27/1992 -I -1 " ~ ~ -~ Q) 8127/1993 j -O· f 8/27/1994 ~ en z ~ m 8/27/1995 < CD 8/27/1996 CC T CD -8/27/1997 Q) -z O· ::'E 8/27/1998 ~ -s:::: t 8/27/1999 0 :::::.: en 8/27/2000 -" ::'E CC - 8/27/2001 8/27/2002 8/27/2003 8/27/2004 - 8/27/2005 8/27/2006 - 8/27/2007 8/27/2008 8/27/2009 8/27/2010 (Log Scale) -" a a a a a a a 0 0 0 0 0 0 0 m m m m m m m I I I I I 6 I 0 0 0 0 0 0 co -..J 0) 01 .j::. c.v f\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 ~ I........:: I .n.~ 1 " C" I 8/27/1989 j I -~ I N ...... 0 8/27/1990 -0 0 8/27/1991 ~ " =:::L. ::::J (') CD 8/27/1992 -I ..... 1_ r ~ ::::J -~ m 812711993 1 5 '~ -o· f ::::J 8/27/1994 en z 3' m 8/27/1995 < CD T 8/27/1996 Ul CD -8/27/1997 m -z o· :E 8/27/1998 ::::J -t: f 8/27/1999 -0 :::::: (f) 8/27/2000 '" ::E Ul - 8/27/2001 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 (Log Scale) ...... <::> <::> 0 0 <::> <::> <::> 0 0 0 <::> <::> 0 0 m m I I 0 0 w I\) m m m I I I 0 0 0 0) (}1 .j:>. m m I I 0 0 (Xl -....J 01-Jan-81 L 01-Jan-82 -:e :::I 01-Jan-83 -~ m 01-Jan-84 S m CJ) » 01-Jan-85 - 01-Jan-86 -s r-01-Jan-87 r- Z 0 01-Jan-88 :xJ -I 01-Jan-89 :::I 01-Jan-9O m » CJ) -I 01-Jan-91 0 "T1 S r- -r-~:xJ _.£1) -I "N (ON -0) £I) 01-Jan-92 tl 01-Jan-93 ~I 01-Jan-94 -I'V I'V fl 01-Jan-95 - 01-Jan-96 -u ::::J C. 9"1 01-Jan-97 I'V ~ ""C C' 0 . 01-Jan-98 I N ...a. 01-Jan-99 0 01-Jan-OO (') 0 ::::J n 01-Jan-01 C'D ::::J -01-Jan-02 .., £I) -O· 01-Jan-03 ::::J en 01-Jan-04 01-Jan-05 ::::J < C'D (0 01-Jan-06 C'D -£I) 01-Jan-07 -O· ::::J 01-Jan-08 01-Jan-09 01-Jan-10 01-Jan-11 (Log Scale) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m I I 0 0 OJ -....I m m I I 0 0 c.u I\) m m m 6 I I 0 0 0) 01 .J:>. 01-Jan-81 =E 01-Jan-82 ::I: =i 01-Jan-83 m s: 01-Jan-84 -m en 01-Jan-85 » s: 01-Jan-86 I I 01-Jan-87 Z 01-Jan-88 0 :::c 01-Jan-89 -4 ::I: 01-Jan-90 =E m en 01-Jan-91 -4 0 r 01-Jan-92 :1)1 01-Jan-93 "T1 s: I P> ~I 01-Jan-94 01-Jan-95 TI 01-Jan-96 ""0 C" ~I 01-Jan-97 . 01-Jan-98 "C I O:::C _.£1) -. ~I\) CCI\) -0) £I) :::l a. "'C C" • I\) 01-Jan-99 ...... 0 01-Jan-OO 0 0 01-Jan-01 :::l (") tD 01-Jan-02 :::l -""'I £I) 01-Jan-03 -O· 01-Jan-04 :::l en 01-Jan-05 :::l < 01-Jan-06 tD CC tD 01-Jan-07 -£I) -01-Jan-08 O· :::l 01-Jan-09 01-Jan-10 - 01-Jan-11 t JJ ~ I\J OJ T ""C 0-r\, -o o o m I o (Xl 01-Jan-81 01-Jan-82 01-Jan-83 - 01-Jan-84 01-Jan-85 01-Jan-86 - 01-Jan-87 01-Jan-88 01-Jan-89 01-Jan-90 01-Jan-91 - 01-Jan-92 01-Jan-93 - 01-Jan-94 01-Jan-95 01-Jan-96 - 01-Jan-97 01-Jan-98 01 -Jan-99 01-Jan-OO 01-Jan-01 01-Jan-02 01-Jan-03 01-Jan-04 01-Jan-05 01-Jan-06 - 01-Jan-07 01-Jan-08 - 01-Jan-09 01-Jan-10 01-Jan-11 o o m I o --...J (Log Scale) a a a 0 0 0 m m m 6 6 I 0 en 01 .j:>. a 0 m I 0 W ~ o o m I o I\) o o m I o o o m + o o ::e :J: =t m s:: m en » s:: -• • I en o c: -4 :J: ::e m ~ o ." s:: -• c' Oll _.0) -I ~N CCN -0) 0) :::l Q. "0 C" I N ...... o o o :::l (') CD :::l -Sil -o· :::l en :i' < CD CC CD -0) -o· :::l WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED OTR. SAMPLED DATE 3rd'81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd'82 01-Jul-82 4th 'B2 30-Nov-S2 2nd'B3 13-Apr-S3 3rd '83 0l-Jul-S3 4th '83 30-Jan-84 2nd '84 2S-Jun-S4 4th '84 14-Nov-84 2nd 'ss 27-Mar-8S 3rd 'BS lS-Jul-SS 4th'SS 09-0ct-SS 2nd 'S6 24-Mar-S6 3rd '86 10-Jul-S6 4th '86 lS-0ec-S6 2nd'S7 20-Apr-S7 3rd'S7 OS-Jun-S7 4th'S7 22-0ec-S7 2nd'SS 19-Apr-SS 3rd'SS 28-Jul-SS 2nd'S9 07-Apr-S9 3rd'89 06-Jun-S9 4th '89 07-Nov-S9 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd'90 17-0ct-90 1st '91 lD-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd'93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd'94 2S-Nov-94 1st '9S ll-Apr-9S 2nd '95 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96· 31-Jul-96 3rd'96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '9S 23-Mar-98 2nd '9S 16-Jun-98 4th '98 OS-Nov-9S 2nd '99 lS-Apr-99 3rd'99 07-Jul-99 4th '99 02-0ec-99 2nd '00 21-Apr-00 2nd '00 22-Jun-00 Ra-ZZ6 VALUE (uCi/Kg) 3.90E-04 1.40E-04 1.31E-04 l.60E-04 2.67E-06 9.36E-OS 1.12E-04 l.09E-04 3A7E-04 S.61E-04 1.0SE-03 8.20E-OS 1.1SE-04 S.72E-04 S.OlE-04 B.70E-04 S.90E-04 l.60E-04 2.10E-04 4.S0E-04 3.20E-OS S.60E-04 l.S0E-04 6.00E-04 2.60E-04 1.BOE-04 1.60E-04 1.20E-04 9.10E-OS 4.S0E-04 3.60E-OS l.OOE-OS 7.90E-OS 3.70E-OS 3.00E-OS 6.60E-OS 1.S0E-04 l.71E-OS 2AOE-04 6.70E-OS 1.50E-OS S.SOE-OS S.20E-OS 3.00E-OS 1.10E-OS 1.lDE-OS S.OOE-06 <9.lDE-OS 1.80E-OS S.70E-OS 2.00E-04 6.03E-OS 2.30E-OS l.S0E-04 l.20E-06 Ra-ZZ6 LLD Pb-Zl0 Pb-Zl0 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-OS) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (l.OE-06) 1.0E-OS S.OE-08 l.lDE-03 1.0E-04 1.0E-06 1.0E-OS S.OE-08 6.80E-04 8.0E-OS 1.0E-06 1.3E-OS l.OE-06 4.90E-04 7.0E-OS 8.0E-OS l.OE-OS S.OE-08 8.00E-04 1.7E-04 l.OE-07 l.lE-06 l.OE-06 1.0SE-04 9.0E-06 1.OE-OS 6.2E-06 8.0E-09 4.97E-04 9.3E-OS 1.0E-04 1.2E-OS 6.0E-06 l.S4E-04 l.2E-OS 1.0E-06 8.0E-06 4.0E-06 7.S0E-04 6.2E-OS 6.0E-OS l.2E-OS 2.0E-09 3.7SE-03 l.6E-04 4.0E-OS 2.0E-04 2.0E-07 7.B2E-03 3.3E-04 7.0E-08 3.0E-OS 2.0E-06 3.22E-03 1AE-04 2.0E-OS 7.0E-06 3.0E-06 7.70E-04 1.3E-04 2.0E-04 l.OE-OS 3.0E-06 S.10E-04 3.0E-OS 2.OE-OS 2.1E-OS 4.0E-06 2A9E-03 l.OE-04 1.DE-OS 1.3E-OS 3.0E-06 1.S7E-03 l.7E-03 2.0E-04 S.OE-OS 3.0E-06 6.80E-04 3.0E-OS 3.0E-06 7.0E-OS S.OE-OS 1.SOE-03 l.OE-04 1.0E-06 3.0E-OS S.OE-08 9.S0E-04 4.0E-OS 1.OE-06 4.0E-OS S.OE-OS 1.70E-03 1.0E-04 1.OE-06 7.0E-OS S.OE-OS 1.40E-03 1.0E·04 1.0E-06 2.2E-OS S.OE-08 1.S0E-04 4AE-04 1.0E-06 4.0E-OS *** 1.10E-03 1.0E-01 ••• 2.0E-OS ••• 2.30E-04 2.0E-OS ••• S.OE-OS 7.0E-06 2.04E-03 7.0E-OS 1.4E-OS 3.0E-OS 4.0E-06 3.30E-04 2.0E-OS 2.2E-OS 2.0E-OS S.OE-OS 3.20E-04 2.0E-OS l.OE-06 2.0E-OS S.OE-OS 3.30E-04 2.0E-OS 1.0E-06 2.0E-OS S.OE-06 3.00E-04 2.0E-OS 1.0E-06 1.6E-OS 2.0E-07 1.90E-04 2.0E-OS 2.0E-07 4.0E-OS S.OE-OS 1.09E-03 S.OE-OS 1.0E-06 1.OE-OS 2.0E-06 l.S0E-04 2.0E-OS 1.0E-OS 7.0E-06 2.0E-07 7.50E-OS 2.0E-OS 1.0E-06 3.SE-OS 3.0E-06 7.10E-04 7.0E-OS 2.0E-OS 2.2E-OS 3.0E-06 2.S0E-04 3.0E-OS 2.OE-OS 1.SE-OS 3.0E-06 4.30E-OS 3.5E-OS 2.0E-OS 2.7E-OS 3.0E-06 S.30E-04 6.0E-OS 2.0E-OS 4.0E-OS 3.0E-OS 4AOE-04 6.0E-OS 2.0E-04 1.2E-06 9.0E-OS 3.00E-OS 6.1E-06 4.SE-06 l.SE-OS 1.7E-07 1.70E-04 l.lE-OS S.3E-07 SAE-06 l.6E-07 1.40E-04 1.3E-OS 7.9E-07 l.SE-06 l.SE-07 S.lDE-OS 4.SE-06 7.6E-07 S.OE-06 1.8E-07 6.70E-OS 1.0E-OS S.SE-07 2.SE-06 l.SE-07 3.20E-OS 4.5E-06 1.SE-07 2.SE-06 1.SE-07 lAOE-04 7.1E-06 9.3E-07 4.7E-07 1.2E-07 4.10E-OS 3.6E-06 6.1E-07 4.3E-07 1.3E-07 2.10E-OS 7.3E-07 6.7E-07 1.2E-06 S.6E-07 1.40E-04 4.6E-06 l.lE-07 9.1E-OS 9.1E-OS <4.S0E-04 4.SE-04 4.5E-04 1.2E-06 6.3E-OS 4.00E-OS 1.8E-06 3.2E-07 1.0E-06 8.2E-OS S.70E-OS S.OE-06 4.1E-07 3.0E-OG l.2E-07 3.00E-04 l.OE-OS G.OE-OS l.4E-06 S.3E-08 lAOE-04 4.7E-OG 4.2E-07 1.0E-06 2.3E-07 2.10E-OS l.OE-OG 1.1E-06 3.0E-06 l.2E-07 1.60E-04 S.OE-06 S.9E-07 1.0E-07 2.SE-07 1.60E-04 1.DE-OS lAE-06 4th '00 21-0ec-00 1.60E-06 l.1E-06 3.7E-07 S.10E-OS S.OE-06 1.9E-06 1st '01 30-Apr-01 1.00E-06 1.0E-07 2.4E-07 <1.2E-06 1.0E-07 2.4E-07 2nd '01 14-Jun-01 2.30E-06 2.0E-07 9.9E-OB 3.BOE-06 2.0E-07 S.OE-07 4th '01 17-0ec-01 9.10E-06 2.4E-06 1.2E-07 3.57E-OS 3.0E-06 6.0E-07 1st '02 07-May-02 3.30E-OS l.BE-06 7.6E-07 4.50E-OS 2.6E-06 1.OE-OS 2nd '02 07-Jul-02 S.5SE-OS 2.BE-06 7.6E-07 S.31E-OS 3.9E-06 1.0E-OS 4th '02 lS-0ec-02 7.7SE-OS 3.6E-06 7.6E-07 l.29E-04 6.2E-06 1.0E-OS 1st '03 21-Mar-03 9.10E-06 l.3E-06 3.6E-07 1. 13 E-OS 1.6E-06 3.4E-06 2nd '03 1O-Jun-03 2.S0E-OS l.3E-06 3.6E-07 3.26E-06 2.0E-06 7.4E-OB 4th '03 20-Nov-03 S.70E-OS 3.5E-06 l.SE-07 4.0SE-OS S.BE-06 B.3E-07 1st '04 OB-Apr-04 9.3BE-OS 3.7E-06 1.lE-07 S.BBE-OS 3.0E-06 S.SE-07 2nd '04 12-Jun-04 S.63E-OS 3.4E-06 1.BE-07 6.42E-OS S.9E-06 9.0E-07 4th '04 30-Nov-04 B.41E-OS S.SOE-06 2.00E-OB 2.4BE-04 1.40E-OS 3.00E-07 1st '05 21-Apr-OS S.60E-OS 3.00E-06 1.40E-07 S.BOE-OS 4.00E-06 6.90E-07 2nd '05 13-Jun-OS 9.10E-06 1.S0E-06 1.BOE-07 1.10E-OS 1.20E-OS 9.00E-07 4th '05 10-Nov-OS 6.00E-OS 3.00E-06 1.10E-1O 1.70E-06 6.40E-07 S.SOE-lO 1st '06 03-Apr-06 B.OOE-OS S.00E-06 S.OOE-OB 3.40E-04 1.20E-OS 1.00E-06 2nd '06 16-Jun-06 4.10E-OS 3.lOE-06 S.OOE-OB 1.16E-04 6.10E-06 1.00E-06 4th '06 2B-Nov-06 1.17E-04 4.60E-06 1.90E-07 3.2BE-04 9.50E-06 9.50E-07 1st '07 30-Mar-07 9.70E-OS 4.40E-06 1.90E-07 3.40E-04 B.70E-06 B.4-07 2nd '07 1-Jun-07 l.30E-OS 1.60E-06 1.90E-07 1.20E-04 6.60E-06 9.70E-07 4th '07 23-Nov-07 7.00E-OS B.20E-06 2.00E-07 S.00E-04 2.00E-OS 1.20E-06 1st 'OB 22-Apr-OB 3.6E-06 3.00E-06 S.20E-07 2.3E-04 1.40E-OS 1.00E-06 2nd'OB 1B-Jun-OB 3.2E-OS 3.20E-06 1.BOE-06 6.9E-OS 3.S0E-OS S.SOE-OS 4th 'OB 12-0ec-OB 1st '09 2B-Apr-09 S.9E-04 l.3SE-OS 1.S0E-06 3.4E-04 l.30E-OS 1.S0E-06 2nd '09 17-Jun-09 1.9E-OS 1.4SE-06 4.90E-07 3.6E-OS 1.10E-OS 1.BOE-OS 4th '09 1B-Oec-09 1.7E-04 S.90E-06 4.BE-04 l.20E-OS 1st '10 13-May-10 2.2E-04 7.20E-06 1.10E-06 1.9E-04 1.90E-OS 2.90E-OS 2nd '10 1B-Jun-10 6.SE-OS 3.40E-06 7.60E-07 1.4E-04 1.90E-OS 2.90E-OS 4th '10 20-0ec-10 2.3E-OS 1.70E-06 S.20E-07 1.0E-OS 1.S0E-06 2.30E-06 2nd '11 23-Jun-11 2.4E-07 1.4E-07 1.BE-07 <2.9E-06 1.7E-06 2.9E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd'81 27-Aug-81 4th '81 20-0ct-81 2nd '82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd '87 20-Apr-87 3rd '87 05-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 lD-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '95 ll-Apr-95 2nd '95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd'97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 2.73E-03 2.00E-04 1.04E-04 2.00E-05 2.36E-06 8.58E-05 1.19E-04 9.78E-OS 2.08E-04 6.05E-04 1.lDE-04 6.lDE-05 1.07E-04 8.86E-04 6.66E-04 5.20E-04 4.10E-04 1.60E-04 3.60E-04 2.60E-04 3.10E-05 6.20E-04 3.40E-04 5.10E-04 3.60E-04 1.70E-04 8.80E-05 3.00E-04 3.lDE-04 5.00E-04 2.00E-05 6.50E-06 1.20E-04 1.80E-05 5.20E-05 5.lDE-05 1.20E-04 3.73E-05 2.40E-04 8.40E-05 1.90E-05 1.20E-04 8.30E-05 3.60E-05 3.30E-05 5.40E-06 8.90E-06 <9.20E-05 < 6.50E-08 4.20E-05 6.20E-05 5.45E-05 1.10E-04 3.70E-05 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCI/Kg) uCi/Kg (I.OE-06) 5.0E-05 5.0E-08 7.10E-03 3.0E-04 1.0E-06 1.0E-05 5.0E-08 8.30E-04 5.0E-05 1.0E-06 9.0E-06 7.0E-06 6.40E-04 5.0E-05 4.0E-05 1.0E-05 5.0E-08 2.20E-04 9.0E-05 1.0E-07 9.5E-07 1.0E-06 8.00E-05 1.0E-05 1.0E-05 1.4E-05 2.0E-08 3.53E-04 1.9E-05 1.0E-05 1.lE-05 5.0E-06 1.58E-04 1.3E-05 1.0E-05 7.0E-06 2.0E-06 2.16E-03 3.4E-04 3.0E-04 1.0E-05 3.0E-09 1.60E-03 7.0E-05 3.0E-08 1.6E-04 2.0E-07 2.58E-03 1.1E-04 3.0E-08 8.0E-06 3.0E-06 8.63E-04 4.2E-05 3.0E-05 6.0E-06 2.0E-06 5.40E-04 5.0E-05 5.0E-05 6.0E-06 2.0E-06 3.80E-04 3.0E-05 2.0E-05 1.8E-05 2.0E-06 4.40E-03 1.9E-04 3.0E-05 1.8E-05 3.0E-06 4.78E-03 2.1E-04 6.0E-05 1.0E-04 3.0E-06 1.70E-03 1.0E-04 6.0E-05 1.0E-04 5.0E-08 1.60E-03 1.0E-04 1.0E-06 3.0E-05 5.0E-08 5.50E-04 4.0E-05 1.0E-06 5.0E-05 5.0E-08 1.80E-03 1.0E-04 1.0E-06 5.0E-05 5.0E-08 1.90E-03 1.0E-04 1.0E-06 1.9E-05 5.0E-08 1.60E-04 4.0E-05 1.0E-06 5.0E-05 *** 1.70E-03 1.0E-04 *** 3.0E-05 *** 7.40E-04 3.0E-05 *** 6.0E-05 7.0E-06 1.00E-03 7.0E-05 1.4E-05 3.0E-05 4.0E-06 4.80E-04 2.0E-05 2.2E-05 2.0E-05 5.0E-08 3.20E-04 2.0E-05 1.0E-06 1.6E-05 5.0E-08 2.90E-04 2.0E-05 1.0E-06 3.0E-05 5.0E-06 4.10E-04 2.OE-05 1.0E-06 3.0E-05 2.0E-07 4.70E-04 2.0E-05 2.OE-07 4.0E-05 5.0E-08 1.50E-03 1.0E-04 1.0E-06 8.0E-06 2.0E-06 9.60E-05 1.4E-05 1.0E-05 6.0E-06 2.0E-06 1.20E-04 2.0E-05 1.0E-06 4.0E-05 3.0E-06 1.21E-03 8.0E-05 2.0E-05 1.7E-05 3.0E-06 2.lDE-04 3.0E-05 2.0E-05 1.9E-05 3.0E-06 1.70E-05 3.6E-05 2.0E-05 2.3E-05 3.0E-06 7.lDE-04 6.0E-05 2.0E-05 1.0E-05 3.0E-05 9.80E-04 1.6E-04 2.0E-04 1.6E-06 8.4E-08 7.80E-05 7.1E-06 4.2E-07 1.5E-05 1.7E-07 2.60E-04 1.3E-05 8.3E-07 6.1E-06 1.5E-07 1.20E-04 1.1E-05 7.5E-05 1.5E-06 1.4E-07 4.50E-05 4.3E-06 7.2E-07 6.8E-06 1.4E-07 1.00E-05 5.8E-06 7.1E-07 3.3E-06 1.9E-07 6.80E-05 6.3E-06 1.8E-07 2.5E-06 1.6E-07 8.50E-05 5.6E-06 8.4E-07 2.3E-06 1.7E-07 4.40E-05 4.8E-06 8.4E-07 3.5E-07 1.6E-07 3.20E-05 9.0E-07 7.8E-07 7.2E-07 5.4E-07 3.40E-04 6.7E-06 1.lE-07 9.2E-05 9.2E-05 <4.60E-04 4.6E-04 4.6E-04 6.5E-08 6.5E-08 <3.20E-07 3.2E-07 3.2E-07 1.0E-06 1.1E-07 1.70E-04 1.0E-05 5.5E-07 1.0E-06 1.0E-07 1.40E-04 7.0E-06 1.0E-07 1.4E-06 8.3E-08 9.20E-05 4.0E-06 4.2E-07 3.0E-06 2.2E-07 2.80E-05 1.0E-06 1.1E-06 1.0E-06 2.4E-07 2.70E-04 1.0E-05 1.2E-06 2nd '00 22-Jun-00 2.90E-Os 1.0E-06 3.3E-07 2.BOE-04 2.0E-Os 1.7E-06 4th '00 21-0ec-00 2.30E-06 1,4E-06 3.7E-07 3.30E-04 s.OE-Os 1.9E-06 1st '01 30-Apr-01 2.10E-Os 1.0E-06 1.sE-07 <7.6E-07 N/A 7.6E-07 2nd '01 14-Jun-01 l.30E-06 4.0E-OB 1.2E-07 1.BOE-06 3.0E-OB s.9E-07 4th '01 17-0ec-01 3.70E-Os 7.67E-07 B.30E-OB 6.72E-Os 2.62E-06 6.00E-07 1st '02 07-May-02 4.90E-Os 2,40E-06 7.60E-07 1.2BE-04 s.61E-06 1.00E-Os 2nd '02 07-Jul-02 B.BBE-Os 4.32E-06 7.60E-07 B.33E-OS 4.32E-06 1.00E-Os 4th '02 ls-0ec-02 1.s0E-04 6.2E-06 7.60E-07 3.16E-04 1.07E-Os 1.0E-Os 1st '03 21-Mar-03 s.OOE-OS 3,4E-06 2.71E-06 <4.2e-6 4.20E-06 2nd '03 1O-Jun-03 s.60E-Os 2.0E-06 4.lOE-07 1.BBE-04 S.14E-06 B.2E-OB 4th '03 20-Nov-03 3.20E-04 B.2E-06 1.70E-07 4.B9E-04 1.2SE-Os B.3E-07 1st '04 OB-Apr-04 6.29E-Os 4.1E-06 2.00E-07 1.94E-Os 4.00E-06 1.0E-06 2nd '04 12-Jun-04 6.s1E-Os 3,4E-06 1.30E-07 1.B7E-Os 3.90E-06 6.SE-07 4th '04 30-Nov-04 7.s0E-Os 4.6E-06 2.0E-OB 4,4sE-04 1.40E-Os 3.0E-07 1st '05 21-Apr-OS 4.90E-Os 2.70E-06 1.30E-07 1.27E-04 4.BOE-06 6.50E-07 2nd '05 13-Jun-Os 2.30E-Os 2.10E-06 1.50E-07 4.70E-Os S.10E-06 7.60E-07 4th '05 10-Nov-OS 7,40E-Os 3.50E-06 1.20E-10 2,40E-06 B.10E-OB S.BOE-10 1st '06 03-Apr-06 1.00E-04 6.00E-06 S.OOE-OB 6.s4E-04 1.s0E-Os l.00E-06 2nd '06 16-Jun-06 9.s0E-Os s.90E-06 S.OOE-OB 4,4BE-04 1,40E-OS l.00E-06 4th '06 2B-Nov-06 B.13E-Os 4.10E-06 2.20E-07 3.2sE-04 1.12E-06 l.OOE-Os 1st '07 30-Mar-07 4.30E-Os 2.60E-06 l.70E-07 2.64E-04 7.20E-06 B.60E-07 2nd '07 1-Jun-07 s.10E-Os 3.20E-06 2.30E-07 s.30E-04 1,40E-06 1.20E-06 4th '07 23-Nov-07 7.30E-Os 6.6E-06 S.OE-OB 7.00E-04 2.20E-Os 1.10E-06 1st 'OB 22-Apr-OB 2.BE-06 2.BE-06 7.20E-07 4,40E-04 2.0E-OS 1.0E-06 2nd 'OB IB-Jun-OB 3.2E-06 3.3E-06 1.BOE-06 1.40E-04 3.3E-OS s.sE-Os 4th 'OB 12-0ec-OB 7.3E-Os 3.2E-06 7.40E-07 4,40E-04 2.5E-OS 3.2E-Os 1st '09 2B-Apr-09 s.3E-Os 3.6E-06 1.10E-06 1.90E-04 l.sE-OS 2.2E-Os 2nd '09 17-Jun-09 2.3E-Os 1.6E-Os S.2E-07 4.30E-Os 1.00E-Os 1.7E-Os 4th '09 IB-Oec-09 S.sOE-Os 3.s0E-06 3.0E-04 1.10E-OS 1st '10 13-May-lO 1.9E-04 6.10E-06 9,40E-07 s.lE-04 2.40E-Os 3.lOE-Os 2nd '10 IB-Jun-lO 2.3E-Os 2.00E-06 7.70E-07 B.3E-Os 1.BOE-Os 2.90E-Os 4TH '10 20-0ec-lO B.6E-06 9.lOE-07 3.90E-07 l.lE-07 6.BOE-07 1.10E-06 2nd '11 23-Jun-11 2.1E-07 1.20E-07 1.40E-07 <2.2E-06 1.30E-06 2.20E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 15-Apr-82 3rd '82 01-Jul-82 4th 'B2 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-B4 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd '86 1O-Jul-86 4th '86 18-Dec-86 2nd '87 20-Apr-87 3rd '87 05-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd'88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th 'B9 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 1O·Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 1O-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '95 ll-Apr-95 2nd '95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96· 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-5ep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 9.50E-04 3.00E-05 1.37E-05 3.40E-04 1.75E-05 7.13E-04 5.39E-05 6.40E-05 8.27E-05 2.72E-04 4.73E-04 6.60E·05 2.83E·04 1.57E-04 3.7BE-04 2.60E-04 4.lOE-04 2.90E-04 1.80E-04 2.30E·04 1.50E-04 3.10E-04 1.30E-04 4.30E-04 2.50E-04 1.10E-04 6.10E-05 3.40E·05 8.00E·05 6.50E-05 1.60E-05 1.90E-05 1.60E-05 2.60E-05 3.00E·05 3.10E·05 2.00E-05 1.75E·05 1.00E·04 1.70E-05 6.40E-06 2.30E-05 4.20E·05 2.10E·05 5.50E-06 5.30E·06 2.50E-05 <7.90E-05 3.60E·07 4.30E-05 2.40E-05 2.23E-05 1.50E-04 1.00E-04 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06) 2.0E-05 5.0E-08 1.50E-04 1.0E-05 1.0E-06 3.0E-06 5.0E-OB 1.50E-04 2.0E-05 1.0E-06 3.0E-06 3.0E-06 3.80E-04 4.0E-05 4.0E-05 2.0E-05 5.0E-OB 3.68E-03 2.7E-04 1.0E-07 3.0E-06 2.0E-06 7.92E-04 4.0E-06 2.0E-05 7.3E-05 9.0E·OB 2.51E-03 3.0E-04 3.0E·04 4.5E-06 2.0E-06 6.88E-04 4.3E-05 4.0E-05 7.0E-06 4.0E-06 1.20E-03 1.0E-04 4.0E-05 6.3E-06 3.0E-09 1.80E-03 1.0E-04 9.0E-08 1.5E-04 2.0E-07 4.70E-03 7.2E-04 3.0E-07 1.6E-07 3.0E-06 7.07E-04 3.6E-05 3.0E-05 7.0E-06 4.0E-06 4.90E-04 3.0E-05 3.0E-05 2.0E-05 7.0E-06 1.50E-03 1.0E-04 7.0E-05 1.0E-05 4.0E-06 4.14E-03 1.8E-04 3.0E-05 1.0E-05 2.0E-06 1.65E-02 7.0E-04 1.0E-04 2.0E-05 2.0E-06 1.70E·03 1.0E-04 1.0E·04 7.0E-05 5.0E-08 2.20E-03 1.0E-04 1.0E-06 4.0E-05 5.0E-08 7.50E-04 5.0E-05 1.0E-06 3.0E-05 5.0E-08 2.40E-03 1.0E-04 1.0E-06 5.0E-05 5.0E-08 2.90E-03 1.0E-04 1.0E-06 3.0E-05 5.0E-08 4.30E-03 2.0E-04 1.0E-06 4.0E-05 ... 4.20E-03 1.0E-04 ••• 2.0E-05 ••• 1.50E-03 1.0E-04 ••• 5.0E-05 1.4E-05 3.50E-03 1.4E-04 2.7E-05 3.0E-05 5.0E-06 2.39E-03 5.0E-05 2.5E-05 2.0E-05 5.0E-08 6.60E-04 3.0E-05 1.0E-06 1.4E-05 5.0E-08 6.lOE-04 3.0E·05 1.0E-06 1.1E-05 5.0E-06 2.20E-04 1.0E-05 1.0E-06 6.0E-06 2.0E-07 1.20E-04 1.0E-05 2.0E-07 1.4E-05 5.0E-08 9.10E-04 5.0E-05 1.0E-06 7.0E-06 2.0E-06 3.20E-04 2.0E-05 1.0E-05 1.0E-05 2.0E-07 2.20E-04 2.0E-05 1.0E-06 1.8E-05 3.0E-06 7.60E-04 6.0E-05 2.0E-05 2.0E-05 3.0E-06 3.40E-04 3.0E-05 2.0E-05 1.4E-05 3.0E-06 O.OOE+OO 3.OE-05 2.0E-05 1.6E-05 3.0E-06 4.20E-04 6.0E-05 2.0E-05 5.0E-06 3.0E-05 3.90E-04 8.0E-05 2.0E-04 1.7E-06 7.6E-08 1.30E-04 7.8E-06 3.8E-07 9.0E-06 1.5E-07 2.60E-04 1.2E-05 7.4E-07 1.5E-06 1.6E-07 1.60E-04 loSE-OS 8.1E-07 6.0E-07 1.4E-07 4.40E-05 4.2E-06 7.0E-07 2.2E-06 1.7E-07 6.60E-05 9.6E-06 8.3E-07 2.2E-06 1.7E-07 1.00E-04 6.7E-06 1.8E-07 2.0E-06 1.6E-07 1.90E-04 7.3E-06 8.2E-07 4.2E-07 1.4E-07 3.30E-05 3.9E-06 7.0E-07 3.2E-07 1.3E-07 1.90E-05 6.9E-07 6.3E-07 9.5E-07 5.9E-07 1.30E-04 4.7E-06 1.2E-07 7.9E-05 7.9E-05 <3.90E-04 3.9E-04 3.9E-04 1.4E-07 3.3E-08 <1.7E-07 1.7E-07 1.7E-07 1.0E-06 7.6E-08 2.50E-04 1.0E-05 3.8E-07 1.0E-06 1.2E-07 1.70E-04 B.OE-06 6.2E-07 8.6E-07 1.2E-07 2.30E-04 7.0E-06 5.9E-07 3.0E-06 2.0E-07 1.70E-05 1.0E-06 1.0E-06 2.0E-06 1.2E-07 1.10E-04 7.0E-06 6.1E-07 2nd '00 22-Jun-00 1.30E-06 1.0E-07 2.4E-07 2.00E-04 LOE-OS 1.2E-06 4th '00 21-0ec-OO 1.20E-06 9.0E-07 2.4E-07 L20E-04 3.0E-OS 1.2E-06 1st '01 30-Apr-01 LBOE-06 1.0E-07 L7E-07 <B.3E-07 N/A B.3E-07 2nd '01 14-Jun-01 2.60E-06 2.0E-07 9.9E-OB 1.10E-06 2.0E-OB S.OE-07 4th '01 17-0ec-01 2.63E-06 4.6E-OS 1.2E-07 9.40E-OS 3.7E-06 6.0E-07 1st '02 07-May-02 3.S0E-OS 2.2E-06 7.6E-07 1.36E-04 S.6E-06 1.0E-OS 2nd '02 07-Jul-02 4.02E-OS 2.3E-06 7.6E-07 7.04E-OS 4.1E-06 1.0E-OS 4th '02 lS-0ec-02 B.10E-OS 3.9E-06 7.6E-07 2.B7E-04 B.5E-06 1.0E-OS 1st '03 21-Mar-03 3.70E-OS 2.6E-06 2.4E-06 2.69E-OS 2.0E-06 3.7E-06 2nd '03 10-Jun-03 1.30E-OS 1.0E-06 S.2E-07 <LOOE-07 1.0E-07 4th '03 20-Nov-03 L60E-04 1.3E-OS 1.2E-07 L42E-04 6.4E-06 S.9E-07 1st '04 OB-Apr-04 1.40E-04 7.7E-06 l.1E-07 6.10E-06 2.7E-06 S.SE-07 2nd '04 12-Jun-04 6.S1E-OS 3.2E-06 l.SE-07 S.27E-OS 4.9E-06 7.6E-07 4th '04 30-Nov-04 B.40E-OS S.7E-06 3.0E-OB 3.39E-04 1.6E-OS 3.0E-07 1st '05 21-Apr-OS l.70E-OS 1.6E-06 1.3E-07 4.50E-OS 3.SE-06 6.5E-07 2nd '05 13-Jun-OS 1.S0E-OS 1.6E-06 1.4E-07 7.00E-OS S.lE-06 6.9E-07 4th '05 10-Nov-OS 3.BOE-OS 2.1E-06 B.6E-10 L20E-06 4.BE-OB 4.3E-10 1st '06 03-Apr-06 1.00E-04 6.0E-06 S.OE-OB 3.30E-04 l.lE-OS LOE-06 2nd '06 16-Jun-06 3.40E-OS 2.SE-06 S.OE-OB 1.37E-04 6.0E-06 LOE-06 4th '06 2B-Nov-06 7.31E-OS 3.20E-06 1.60E-07 2.9BE-04 B.SOE-06 B.20E-07 1st '07 30-Mar-07 3.00E-OS 2.20E-06 1.70E-07 3.20E-04 7.90E-06 B.40E-07 2nd '07 1-Jun-07 1.10E-04 4.60E-06 2.3-07 3.20E-04 1.10E-OS 1.10E-06 4th '07 23-Nov-07 S.60E-OS S.20E-06 S.OOE-OB 6.40E-04 L90E-OS LOOE-06 1st 'OB 22-Apr-OB 3.20E-OS 2.30E-06 7.20E-07 2.30E-04 LSOE-OS 1.00E-06 2nd 'OB 1B-Jun-OB 1.2SE-OS 2.20E-06 l.BOE-06 S.OOE-OS 3.00E-OS 4.BOE-03 4th 'OB 12-0ec-OB 1st '09 28-Apr-09 2.60E-OS 2.90E-06 1.40E-06 3.70E-OS LSOE-06 2.50E-OS 2nd '09 17-Jun-09 2.40E-OS 1.40E-06 3.90E-07 3.50E-OS 7.90E-06 1.30E-OS 4th '09 1B-Oec-09 3.1E-OS 2.30E-06 2.1E-04 B.40E-06 1st'lD 13-May-lD 2.0E-OS 2.10E-06 9.40E-07 S.6E-OS l.SOE-OS 2.40E-OS 2nd '10 1B-Jun-10 1.lE-OS 1.30E-06 6.60E-07 7.8E-OS 1.60E-OS 2.50E-OS 4th '10 20-0ec-lD 6.7E-06 9.lDE-07 4.BOE-07 B.OE-07 7.90E-07 1.30E-06 2nd '11 23-Jun-11 <1.7E-07 6.9E-OB 1.7E-07 <2.SE-06 1.SE-06 2.SE-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected dunng this penod EN:RGY ,':.')I~hlC'H:_ J www.energylab.com ARI1fIaI~~ Igsz Halena, MT 877"72-0711 • Billings, MT 800-735-4489 • Casper, W'l881-235-0515 Gillette, W'I 81&-68&-7175 • Rapid City, so 888-172-1225 • Col/ege Station, IX 888-690-2218 August 02, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11 061 059 ANAL VTICAL SUMMARY REPORT Project Name: Late Spring Vegetation Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 6/24/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 061 059-001 North East 06/23/11 9:00 06/24/11 Vegetation Digestion, Radiochemistry Lead 210 Rad ium 226 C11 061 059-002 North West 06/23/11 9:45 06/24/11 Vegetation Same As Above C 11 061 059-003 South West 06/23/11 10:15 06/24/11 Vegetation Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing . All samples are reported on an as received basis unless otherwise indicated. Samples corrected for dry weight indicate units that have -dry appended. If you have any questions regarding these test results, please call. Report Approved By: c3¥~ £) tJtJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.08.02 15:46:38 -06:00 Page 1 of 9 EN:RGY ~ 1"'.'I\,)lf'\IUI.;!.':.... ~ www.energylab.com AM/yfh:6I~SIIru 1m Helana, lIlT 871-472-0711 • Billings, lIlT 800·735·4489 • Casper, W'f 8.8-235-0515 Gillette, WY 88&·&86·7175 • Ra Id City, so 888·&72·1225 . College Station, TX 888·&80·2218 CLIENT: Denison Mines USA Corp Project: Late Spring Vegetation Report Date: 08/02/11 Sample Delivery Group: C11 061059 CASE NARRATIVE BRANCH LABORATORY SUBCONTRACT ANALYSIS Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 9 EN:RGY •• ' l·t.· .. JC1-':" ._ www.energy1ab.com AM/tfII:«~SIIa ,m Helena, tIT 877-472-0711 • Billings, PM BGO·735·4489 • Casper, WY 888·235·0515 Gillette, WY 886·888·7175 . Rapid City, SO 188·672·1225 . CollegeSlalion, IX 188-610·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Late Spring Vegetation C11 061 059-001 Client Sample 10: North East Analyses RAOIONUCLlDES· TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC aJtu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -3.0E-08 1.7E-06 2.9E-06 -0.030 1.7 2.9 2.4E-07 1.4E-07 1.8E-07 0.24 0.14 0.18 Units uCi/kg uCilkg uCilkg pCi/kg pCi/kg pCi/kg uCi/kg uCi/kg uCi/kg pCilkg pCi/kg pCi/kg MDC -Minimum detectable concentration Report Date: 08/02/11 Collection Date: 06/23/11 09:00 OateReceived: 06/24/11 Matrix: Vegetation MCU Qualifier RL QCL Method Analysis Date 1 By U E909.0 07128/11 08:01 1 eli-cs E909.0 07/28/11 08:01 1 eJi-cs E909.0 07/28/11 08:01 1 eJi-cs U E909.0 07128/11 08:01 1 eJi-cs E909.0 07128/11 08:01 1 eJi-cs E909.0 07128/11 08:01 1 eli-cs E903.0 07120/11 23:321trs E903.0 07120/11 23:321 trs E903.0 07120/11 23 :32 1 trs E903.0 07/20/11 23:321 trs E903.0 07120/11 23:321 trs E903.0 07120/11 23:321 trs MCl -Maximum contaminant level. ND -Not detected at the reporting Jimit. U -Not detected at minimum detectable concentration Page 3 of 9 EN:RGY "\IJ')I~r\I ' I~t ~, www.energylab.com AM/ftIcII Elu/Iftu SIRe, 1151 Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515 Gillette, WY 8&6-186-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp Late Spring Vegetation C11 061 059-002 Client Sample ID: North West Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±l lead 210 MOC lead 210 altu lead 210 precision (±l altu lead 210 MOC altu Radium 226 Radium 226 precision (±l Radium 226 MOC Radium 226 altu Radium 226 altu precision (±l Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -3.3E-07 1.SE-06 2.2E-06 -0.S3 1.3 2.2 2.1 E-07 1.2E-07 1.4E-07 0.21 0.12 0.14 Units uCi/kg uCi/kg uCilkg pCi/kg pCi/kg pCilkg uCi/kg uCilkg uCi/kg pCi/kg pCi/kg pCi/kg MOC -Minimum detectable concentration Report Date: 08/02/11 Collection Date: 06/23/11 09:45 DateReceived: 06/24/11 Matrix: Vegetation MCL! Qualifier Rl QCl Method Analysis Date 1 By U E909.0 07128/11 11 :01 1 eli-cs E909.0 07128/11 11 :01 1 eli-cs E909.0 07/28/11 11 :01 1 eli-cs U E909.0 07128/11 11 :01 1 eli-cs E909.0 07128/11 11 :01 1 eli-cs E909.0 07/28/11 11 :01 1 eli-cs E90S.0 07/20/11 23:321 trs E903.0 07/20111 23 :32 1 trs E903.0 07120/11 23 :321 trs E903.0 07120111 23 :3211r5 E903.0 07120/11 23 :32/1rs E90S.0 07/20/11 23:32/1rs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 4 of 9 EN:RGY ;~ •• \..) t.,' i, I t:;f -.'1' "... WWN.energylab.com ~1~SiIIc.II5t Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 818-235-0515 Gillette, WY 866-888-7175 • Rapid City, so 888-&72-1225 • College Station, IX 118-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Late Spring Vegetation C11 061 059-003 Client Sample ID: South West Analyses RADIONUCLIDES -TOTAL Lead 210 Lead 210 precision (±l Lead 210 MOC Lead 210 altu lead 210 precision (±l altu Lead 210 MOC altu Radium 226 Radium 226 precision (±l Radium 226 MOC Radium 226 altu Radium 226 altu precision (±l Radium 226 altu MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -7.3E-07 1.5E-06 2.5E-06 -0.73 1.5 2.5 -8.9E-08 6.9E-08 1.7E-07 -0.089 0.069 0.17 Units uCi/kg uCilkg uCi/kg pCi/kg pCi/kg pCilkg uCilkg uCi/kg uCi/kg pCi/kg pCilkg pCi/kg MOC -Minimum detectable concentration Report Date: 08/02/11 Collection Date: 06/23/11 10:15 DateReceived: 06/24/11 Matrix: Vegetation MCll Qualifier Rl QCl Method Analysis Date 1 By U E909.0 07128/11 12:01 1 elks E909.0 07/28/11 12:01 1 elks E909.0 07128/11 12:01 1 elks U E909.0 07128/11 12:01 1 eli-cs E909.0 07128/11 12:01 1 eli-cs E909.0 07/28/11 12:01 1 eli-cs U E903.0 07/20/11 23:321 trs E903.0 07120/11 23:321 trs E903.0 07120/11 23:321 trs U E903.0 07120/11 23:321 trs E903.0 07/20/11 23:321 trs E903.0 07120/11 23:321 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 5 of 9 EI\ERGY ,'" ':"1.1 .. 1 ,_ 1,11\ • www.8ntrgyiab.com ~EIuIIMa~ /IIIZ Helena, MT 877-472-D711 • Billings, MT 800-735-4489 • Casper, WY 8118-235-0515 Gillette, WY 886-888-7175 • Rapid City, SD 888-&72-1225 • College Station, 1J( 888-680-2218 Client: Denison Mines USA Corp Project: Late Spring Vegetation QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 08/02/11 Work Order: C11 061 059 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E903.0 Sample 10: MB-30410 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-30410 Radium 226 Sample 10: C11061059-002AMS Radium 226 Sample 10: C11061059-002AMSO Radium 226 Qualifiers: RL -Analyte reporting limit. 3 MOC -Minimum detectable concentration Method Blank 2E-07 uCi/kg 2E-07 uCi/kg 3E-07 uCilkg Laboratory Control Sample 3.0E-OS uCi/kg Sample Matrix Spike 2.SE-OS uCi/kg Sample Matrix Spike Duplicate 2.6E-OS uCi/kg Run: BERTHOLD 770-1 _11 071SA Run: BERTHOLD 770-1_11 071SA 116 70 130 Run: BERTHOLD 770-1 _11071SA 109 70 130 Run: BERTHOLD 770-1 _11071SA 111 70 130 3.3 ND -Not detected at the reporting limit. Batch: 30410 07/20/11 23:32 U 07/20/11 23:32 07/20/11 23:32 07/20/11 23:32 20.7 U -Not detected at minimum detectable concentration Page 6 of 9 EN:RGY / ( )1." I, ll .. 11 • www.energytab.com AMIItIaI~ .. 1m Helena, MT 177-472-0711 • Billings, MT 801-135-4489 • Casper, WY 888-235-0515 Gillette, WY 88&-88&-7175 • Rapid City, SD 888-&72-1225 • College Station, lX 888-680-2218 Client: Denison Mines USA Corp Project: Late Spring Vegetation oAtoe Summary Report Prepared by Casper, WY Branch Report Date: 08/02/11 Work Order: C11 061 059 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E909.0 Sample 10: C11061059-001AMSO Lead 210 Sample 10: C11061059-001AMS Lead 210 Sample 10: LCS-14459 Lead 210 Sample 10: MB-14459 Lead 210 Lead 210 precision (±) Lead 210 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike Duplicate 0.00023 uCi/kg Sample Matrix Spike 0.00020 uCi/kg Laboratory Control Sample 0.00030 uCi/kg Method Blank 2E-06 uCi/kg 7E-06 uCi/kg 1E-05 uCi/kg Batch: T_14459 Run: SUB-T41494 07/28/11 10:01 95 70 130 10 18.3 Run: SUB-T41494 07/28/11 09:01 83 70 130 Run: SUB-T41494 07/28/11 07:01 81 70 130 Run: SUB-T41494 07/28/11 06:01 U ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 7 of 9 EN:RGY ,,.. 1(11.,-,,',1' • www.energylab.com AMIfIieM~SitIc, 1m Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-1515 Gil/alte, WY 888-886-7171 • Rapid City, SO 888-&72-1225 • Collage Stalion, lX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp IIIIIII ~IIIIIIIIIIIIIIIII~IIIIIIIIIIII!IIIIIIII~ C11061059 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 6/28/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chai n of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Received 2 samples on 6-27-11. Yes 0" Yes 0" Yes 0 Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" "C NA Yes 0 Yes 0 Date Received: 6/24/2011 Received by: dw Carrier NDA name: No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0" No VOA vials submitted 0" Not Applicable 0" Page 8 of 9 Chain of Custody and Analytical Request Record Page -.L of 1-__ lY;{ff'lY •• meJ.-I1.mrilZW PLEASE PRINT jProvide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: De,J/soJ 1Yl,~ 1~ '\/)A'.:..e. It~ IU~~ State: /A.1 Yes ~ No 0 Report Mail ~d~res~~ ~O '1 COnli?Name: ~I / Phonel~x: Email : Sampler: ~Iease Print) P}3;;/JL~dfVtC. !AI .S<4 ~-// 1!v4r-~/lf-VI/ #J'Ft"1if 2'ZeL tb~W/~ d;wv~ InVOice Address: / Invoice Contact & Phone: Purchase Order: QuotelBottle Order: ,.-SL~:C; il AE .- Special ReporVFormats: ?: ~r!:, \?@D@ ~~®I]J~@:[Q) .. Contact ELI prior to . linL'I~ fIJi "'" a .... RUSH sample submittal .-1. f'.~ IIA1 ~ 0 "':S ~ for charges and Cooler lOis): ~ CD ~ ~]j 0 ~ R scheduling -See C I--t-' O 0 J9>U) «)~ w c. Instruction Page (~ OW EOD/EDT(Electronic Data) c:o~]! ~:> I '0 R I T >--«) 01 c: ecepl 11 o POTWIWWTP Format: ~«~1~1~ ~ is U Comm~nts: I iV'\ 0 o State: 0 LEVEL IV ~ t* s;§ I-~ re~~ ot(....,..... ~-c o Other: 0 NELAC ~~r~. " ~ 5 .'1 \\.~ On Ice: Y N :3 0):.:( ID ~ ~ '7\ ~ 5 /'~ .,. zc. l:ira .1'': ~ W 'E " ?--7-~ q t) Custody Seal ';:1 E >1 ~ ~ UJ <Il OnBoltle \!y ~ (/J -g On Cooler Y N .1 . til I--S-A-M-P-LE-'D-E-N-T-IF-/C-A-T-I-O-N--'--C-o-I'ec-tio-n-r-C-O-II-ec-tl-'o-n-l--M-A-T-R-'X---''''R ~ U5 H :::~ture V») N (Name, Location, Interval, etc.) Date Time ~ Match I Y N l/11ve;r#h< 1 r tlz,;/t#! t1to() / --J/ IX X ~ 2 M rt-'/t.. /.I\J e,j -} r;;t} leI/I / of '1~'-} -1/ X X ~ 3 Y;~/)J4--r ?/Z)JZ//1 Jt1J ~ / -tI ;t ~ ~ 4 I' .II 5 ~ J 6 ~ I 7 ~ 8 ~ 0) 9 ~ / 10 ~'llrJ~/6 57 Custody R~~dby (prir]) I OaleJT1"",: lOt) . li~/ Receivedhy(prln1]' Date!Time: signature: R ~"'-~h=-r t;/ZJ2!/J? y ~ M ~~~ r~e Relinqui~hed by win!) OateJ1i,ne' D ">'9'~'u,u. ReceIVe:! by Iprlnt); OatelTima. Signature: • ~~vea py yal!'! "ro: I r..... ~Ignalure: Signed Sample Disposal: Relurn to Client: Lab Disposal: (U 1) () fh-v 1A-1.. '"'L-t/ -}Lf)' In certain circumstances. samples submitted to Enemv Laboratories. Inc. mav be subconlrac~d \, othe~ertified laboratories in order to complete the analvsis reauested. Visit Ollr w<>h site at www.aner~lV)ab.C<Qffi for additional information, downloadable fee schedule, forms. ana links. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: FIRST QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORATION NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH February 15-16, 2011 by: TETCO 391 East 620 South American Fork, UT 84003 Phone. (801) 492-9106 Fax (801) 492-9107 fax Denison Mine.s Corporation 6425 SHwy91 Blanding, Utah 84511 Date of Report: May 31 2011 CERTlf71CATlON OF REPORT [NTEGRITY Technical Emission Testing "ornpany (T TC ) ccrtitie that thi report represents the truth as well a. CEln be d rived by the methods empLoyed. Every etforl WElS mad 1 obtain accurate and rcpr senlalive data and to comply with proccdur s • et forth in til Federal Register. Mike McNamara Revicwer: __ ----'1tJ"-"-'''--_k:t-' __________ _ Date: _______ S'_I_"!>_'_I _II _______ _ Dean A Kitchen Dat : _______ F_-.... )::...J.{_--_'-1/'---__ _ ii TABLE OF CONTENTS Introduction Test Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Test Location and Type of Process .......................................... 1 Test Dates ............................................................. 1 Pollutants Tested and Methods Applied ...................................... 1 Test Participants ......................................................... 2 Deviations From EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Summary of Results Emission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 3 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sampling and Analysis Procedures Sampling Port Location ................................................... 6 Sampling Point Location .................................................. 6 Sampling Train Description ................................................ 6 Sampling and Analytical Procedures ......................................... 7 Quality Assurance ....................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measured Radionuclide Emissions .......................................... 3 II Percent Isokinetics ....................................................... 4 III Sampling Point Location .................................................. 6 IV Complete Results, North Yellow Cake Scrubber ...................... Appendix A V Complete Results, Yellow Cake Dryer Baghouse ...................... Appendix A LIST OF FIGURES Figure 1 Facility Schematic Repre entation North Yellow Cake Scrubber .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D 3 Schematic of Method 5/114 Sampling Train .......................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the North Yellow Cake Scrubber and the Yellow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat only. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 and 2 in Appendix D. Test Dates One test run was completed on the NYC Dryer February 15,2011 and one run on February 16th• One run was completed on the Dryer Baghouse February 15,2011. Pollutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. 1 Test Participants Test Facility State Agency TETCO Ryan Palmer None Doug Olsen Kawai McNamara Deviations -From EPA Methods None Quality Assurance Mike McNamara Testing procedure and sample recovery techniques were according to those outlined in tile Federal Register and the Quality it surance Handbookfor Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VI in Appendix A have more detailed information. Table I. Mea ured Ra ionuclide Emissions North Yellow Cake Scrubber Yellow Cake Dryer Run # Baghouse Process Data 1 2 AVE pCi/dscf 1 A19E+02 1.042E+02 1.230E+02 pCi/hr 1.l43E +07 6.9S1E+06 9.190E+06 pCi/dscf pCilhr 8.224E+Ol 1.OSOE+07 8.224E+Ol 1.050E+07 The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test filters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. Discussion of Errors or Irreeularities None 3 Percent Isokinetic Sampling Each of the te sts were isokinetic within the ± 1 0% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Q uality. Division of Air Quality specilication of isokinetic sampl ing point by point. Isokinetic va lues for each test run are presented in Table II. Table II P, rccn. Isokinc.ic Sam lin. Run # 2 North Yellow Cake Scrubber 96 99 4 Yellow Cake Dryer Baghouse 98 SOURCE OPERATION Process Control Devices Operation All process control devices were operated nonnally. Recorded scrubber water flow, pressure and baghouse ilp readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Sampline Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure 1 in Appendix D is a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Samplin2 Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Sample Point 0.70 2 1.89 2.34 3 3.49 4.74 4 5.81 11.26 5 12.19 13.66 6 14.51 15.30 7 Samplin2 Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. 6 The tack analyzer used to conduct Method 1-5/114 are con tructed to meet the pecification outlined in the CFR. The temp rature sensors are K-type thermocouple. Heater vacuum and pitot line connections have been designed to be interchangeable with all unit used by the tester. A 316 tainJes teel probe liner wa used for the tests. Figure 4 in Appendix E i a ketch of the Methods 5/1] 4 ampLing train. Sample boxes were prepared for te ling by following the prescribed procedures outlined in Methods 5/114. Sampline and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment et-up, sampling procedures ample recovery and equip eot calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality A ·surance Handbook/or Air Pollution Mea urement System. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C; Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Re sults F: Re lated Correspondence 8 APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Nomenclature Sample Equations A TABLE IV NYC Scrubber COMPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol DescriEtion Dimensions Run #1 Run #2 Date 2/15/11 2/16/11 Filter # 5714 5617 Begin Time Test Began 8:06 7:40 End Time Test Ended 16:17 15:55 Pbm Meter Barometric Pressure In. Hg. Abs 24.50 24.35 l1H Orifice Pressure Drop In. H20 1.288 0.934 Y Meter Calibration Y Factor dimensionless 0.993 0.993 Vm Volume Gas Sampled-Meter Conditions cf 355.420 307.159 Tm Avg Meter Temperature "F 97.1 95.4 -Vl1P Sq Root Velocity Head Root In. H2O 0.2694 0.2224 WIWc Weight Water Collected Grams 855.7 572.3 Tt Duration of Test Minutes 480 480 Cp Pitot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.3805 0.3805 CO2 Volume % Carbon Dioxide Percent 3.00 3.00 O2 Volumc % Oxygen Percent 17.00 16.90 N2 &CO Volume % Nitrogen and Carbon Monoxide Percent 80.00 80.10 Vm.td Volume Gas Sampled (Standard) dscf 274.962 236.648 Vw Volwne Water Vapor scf 40.346 26.984 Bws (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.128 0.102 Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.060 0.055 Bws Fraction H20 in Stack Gas * Fraction 0.060 0.055 ~ Fraction of o I)' Gas Fraction 0.940 0.945 Md Molecular Wt. DI)' Gas lb/lbmol 29.16 29.1 6 Ms Molecular WI. Stack Gas lb/lbmol 28.49 28.54 %1 Percent Isokinetic Percent 95.5 99.2 AVG Ts Avg Stack Temperature 'F 90.9 88.1 89.5 As Stack Cross Sectional Area Sq. FI. 1.767 1.767 PG Stack Static Pressure In. H20 -0.050 -0.050 Pbp Sample Port Barometric Pressure In. Hg. Abs 24.43 24.28 Ps Stack Pressure In. Hg. Abs 24.426 24.276 Qs Stack Gas Volumetric Flow Rate (Std) dscfin l.34E+03 1.1lE+03 1.23E+03 Q. Stack Gas Volumetric Flow Rate (Actual) cfin 1.82E+03 l.51E+03 1.67E+03 Vs Velocity of Stack Gas tpm 1.03E+03 8.52E+02 9.43E+02 Curies Radionuclides per sample pCi 39021.0 24649.0 Crad Concentration of Radionuclides pCi/dscf 141.914 104.159 123.037 ERrad Emission Rate of Radionuclides pCiIbr 1.143E+07 6.95IE+06 9.190E+06 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CPR 60, Method 4, Section 12.1.7). Oryer BaghoUSll TABLE V COMPLETE RESULTS, PM DENISON MINES CORPORATION YELLOW CAKE DRYER BAGHOUSE Symbol DescriEtion Dimensions Run #1 Date Date 2/15/11 Filter # 5715 Begin Time Test Degnn 9:23 End Time Test Ended 11:25 Pbm Meter D!U'Ometric Pressure llL Hg. Abs 25.50 MI Orilice Pressure Drop In. H,O 1.303 Y Meter Calibnllion Y factor dimensionless 1.001 Vm Volume Ons Snmplcd-Mctcr C<;mditions cf 91.348 Tm Avg MeIer Tempenllurc "F 97.5 ...jill' Sq Root Veloeil)' Hcnd Root In. H10 0.5056 Wtwc Weight Water Collected GrnlllS 18.2 Tt Dumlion of Test Minutes 120 Cp PiiOI Tube Coefficient Dimen iOllless 0.84 Do Novle Diameter Inohes 0.2758 CO2 Volume % Cnrbon Dioxide Pc=nt 0.00 O2 Volume % Oxygen Pcrecnl 20.90 N2 &CO Volume % Nltrogl:n and Cnrbon Monoxide· Percent 79.10 Vm.td Volume Gns Srunplcd (Stnndnrd) dsof 74.085 Vw Volume Wntc.r Vnpor scr 0.858 Bw. Fruction H,O in Stock Ons Fl'Ilctioll 0.01l JC.i Fmclioll of Dry G.s Fmetion 0.989 Md Molecular WI. Dry OOS Ibllbmol 28 .84 M. M.olcculllr WL SlIlck Ons Ibl1bmol 28.71 %1 Percent Isokinclic Poreent 97.6 Ts Avg SUlek TcmpcrntufC) OF 89.8 As Stack Cro~s Sectional Area Sq. FL 1.396 Pa S!8ck Stntie Pressure In. H,O -0.18 Pbp Sample Pan' B~romQlrie Pressure In. Jig. Abs 25.43 p. SUlek Pressure In. Hg. Ails 25.417 Q. Slock Gns Volumelric Flow Rale (SId) <lscfm 2.13E+03 Q. Stnck Gas Volumetric Flow RaIC (Actual) crm 2.64E+03 V. Velocity ofStnck CDS rplll 1.89E+03 Curies Rndionuclldes pcr snmptc pCl 6093.0 Crad Conccntl'lltlon orRodianuclides pClldscf 82.2433 ERrad Emission ROlc of Radio"uelidcs pCilhr J.050£+07 %1 = percent isokinetic, percent As = stack cross-sectional area (ft3) AS~ = see ..Jf.P M5 Nomenclature Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas CB = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cf = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) Crnet•l = concentration of metals (ppm, Ilg/fe, etc.) atomic symbol replaces "metal" CO2 = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) C x (avg) = species symbol replaces x . Cx (corr) = actual gas concentration corrected to required percent O 2 f.H = orifice pressure drop (inches H 20) f.H@ = orifice pressure (inches H20) f.P = stack flow pressure differential (inches H20) Ds = diameter ofthe stack (feet) Dn = nozzle diameter (inches) EA = percent excess air ERB = emission rate of back half particulate (lb/hr) ERF = emission rate of front half particulate (lblhr) ERrnrnBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point f.P to determine test point f.H L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lb/lb-mol) MF = mass of particulate on filter (mg) MFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmol) N2 = percent nitrogen in the stack gas O2 = percent oxygen in the stack gas ..Jf.P = average of the square roots of f.P (may also be referred to as ASf.P) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) PG = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) 8 = time of test (minutes) Qa = stack gas volumetric flow rate (acfm) Qs = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (fe/min, wscfm) Ts = stack temperature (OF) Tstd = absolute temperature at standard conditions (528°R) Tt = see 8 M5 Nomenclature Um = mean molecular speed (cmls) Vm = sample volume (nl) at meter conditions Vll\td == volume standard (dscf), sample volume adjusted to 68~ and 29.92 inches Hg. VI = velocity o f stack gas (fpm) V we == volume water vapor (scI) at 68'-'F and 29.92 inchcs Hg. W = Width ofrcct3ngular slack (inches) Wt..... = weight oCthe condensed water collected (grams) Xd = fraction of dry gas Y = meter calibration Y -factor (dimensionless) Method 5 %1 = Vllls.d • (T, + 460)' 1039 1 (9 • V, • P, • Xd • 0/) A,= (Ds2 /4)' 'It B,,"S = V wI (Vmild +V w) Cn = Me ' 0.01 543 1 VmSld Cr = Mfp ' 0.01543 1 Vm,;ld Cx (COlT) = CX{avg)' (20.9· desired %0 2) I (20.9· actual %0 2) D .. = 2 ' L' W /(L+W) D.", = '{0.0269 • (Ph. + 0.0735) / [(T. + 460) • C, • Xd • '[(T. + 460) • M.) / (I', • "I')]} EA = (%02 -0.5 %CO) 1 [0.264 %N2 -(%02 -0.5 %CO)] ERB = CD • Q •• 0.00857 ER, = C,' Q, • 0.00857 ER"""UIIl = ERx 1 (m mBtu 1 hr) K-fact = 846.72 • Dn4 • 6.H@ • C/ • X/ • Md • P, • (T", + 460) 1 [M$ • (T$ + 460) • (Pb", + 6 1-1 1 13.6)] Md = CO2' 0.44 + O2 • 0.32 + N2 '0.28 M, = (Md' Xd)+(18 ' B.J Ps =Pbp +(Po /13 .6) Q.=V,·As Q,= Qa · Xd' Ps ' T,'d l [(Ts + 460) • Plld] Qw= Q,I Xd Vm~ld = Vm • Y • TSld • (Pb", + 6.H I [3.6) I [PS1d • (Till + 460)] v, = 85.49 ' 60· Cp ' '''I'' oJ [(T, + 460) / (1',' M,)] Vwc = Wfwc ' 0.047 15 Xd=l -Bw. APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Denison Mines Stack ldentification North Yellow Cake Scrubber Date r Bll rometric Pressu re Pbm in Hg Pbp in Hg N "0 Static Pressure (P G) in H2O Estimated Moisture (8ws) % Sample Height from Ground feet A Comments: Slack Dia. 18 Reference: 0 Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbonce Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F I 3.2 0.58 0.58 2 10.5 1.89 1.89 3 19.4 3.49 3.49 4 32.3 5.81 5.81 5 67.7 12.19 12.19 6 80.6 14.51 14.51 7 89.5 16.11 16.11 8 96.8 17.42 17.42 Averages: Ts LFlow ---- l\P ___ _ ..J!lP ---- KEY=> ~IT_s __ ~l\_p __ L_F_IO_w~1 -.5 __ Field Data Sheet Plant: Deniso~nes Date. l.~l t! \ \ " Tru,\Jcrsc Time POint Clock Min (0) {+-1 y: It .0 0 1 15 2 30 2 45 3 60 3 75 4 90 4 105 -5 120 6~~ 5 135 6 150 6 165 7 180 7 195 8 210 8 225 ( IZ.:\)~ 240 Totai Average DGM IlP Filter ~1-/~TETCO s~TI Sample BOx __ ~ __ Location: North Yellowcake Dryer Scrubber Operator. 9/\ \ IlH ~"H,ol II vacuum" Te~peratllres ;"J.' DGM T~mp (T~) \"~ (III ~l:O} Des i red I Actual ,',II" II Stack (T,) I Probe I p,,*,,, OU[ I Filter I Effluent II Out I In 'II) q ·~~~L._1,) L·-:r~J rv Il &f () ! 'l,Z.~1 t,ZY! z. t~! ':1'1 II~~ $'D"t·~f" J~GOlroollo611 -z..-Il ¥~ 17..t.11 -r.-5D1 t If11 y~ JL3:¥1 "('1 i 15"'. ~D,\ '-- ..J Additional (Extra) Leak Check Information j (>tl 1'\\"tt-"'\ (; ,:\v r-\ ~~>~"""'\ DGM before Leak Check V "to. C>O~ Vac ("Hg) Rate (fe/min) DGM After Leak Check Vac ("Hg) (,10 . .-z..,(o~ page _LoC~ Run#l i "0 N A Stack Diameter 18" __ Pon Reference _0.0" Pons arc 9.5' Upstream from next disturbance Pons are 9.5' Downstream from last disturbance Assumed Moisture 4-13 % 1-~ Probe z... . -CJl~ Nozzle Calibration "'7 f" I c I ~ 5$~ ~ 30" l<ak Check' f!g ftJlmln (). 0 b ":t v!!c in Hg 2.' 0 .0 ¥" P"o[R". () .()~ In HoO • z.S" Post .1 a ·CD1 ~ 0 .0 ."Z...S Water Collected g Rate (fe/min) Time Sampled A mm Review K= K= I @Tn • @Tm ~ (" 11't· 'f ,0 T 15' f __ L Field Data Sheet TETCO (. Filter ~ Sample Box ___ _ Plant DeniSO) Minep Date Z. I ~ I t I Location: North ~lowcak~ Dryer Scrubber Operator ~ POint DGM Trsvers= 6P I Vacuum If-----r--....:..::..::r-:.:..:::...:.:..:..;,.T-'---.---i~..::...::"'-'-'T"'~"'-- ~ ~-M~ ~ ,~-_1 30_2 ~S----1. vtr_3 rS-__ 3 .50 __ 4 o{~ __ 4 (J~ 5 ~.;(,)II·D~I j.<)~! \ ·-;~1·'1f-g·-1l.,5(, 1J.~4_~y~rs-+I[3jJ. q~ I ~llJ ·41-z..t ~ I, D~ II· a~ M y]! ){17-~!tS£ I Zs'11 ~1-t53JL531 _ i6 I ~I "=\ t~ . (olvll . O~ z..,1~ 1 _~I '111_l'iUUJ,,!'1 J ~~¥I i5~ IfA () JI~!r -~ 1 -i~(( ,/ Ls·r·o~~J ·-.srll-r.:JL . ..::liLLt.'fC1 'lOs"! 'tss-I ~-z.-1r!1(,Tto> 1&1t.~l~Q'f5rl·3bJ ·,·;DII-?JI ,,~:::L~Wl Z,1.{)f'l.-Yt.i5> I~I //\ '5 -w.LofrTIl ·os~[Dt.1 r·()CII-~[3j;JJ./>'1I1"..t«1 z~t.j S-31l ,,\(,1 '/oj 10 __ 5 J~ _6 '-lr-__ 6 r'l:fl~l.o5";-Il.L.dtll·o'Z(l[ 5 11 Af LE'lolzQ'1I", ~11 S"~ll ~" I f) 'C- 1-q~ . I ~..:111 · ol9S"' III· w i t· vc' II in II q \ 1l63-r 1.S"'1.1 ly" I 6"(..ll cO\~l~l '}~·,.!Ovll ·obl1I1·1:iLl~Jl1iJl q\ I 't5'\ I U~i'i<t 15'>11 ,,11 /~"J 60 7 ~~-Z.-~Lr&QII~J /. i t JI_~l:LLl t:-\_?L~S1 'Z:.53 L 6'YJ~T / (j ~ f~ __ 7 <6 1(0. ~(;£--Fo~f I· ~~LL· ~'1I[-uJ[Zf"TIi{;fl1,,~~1 ~5"il [poIL1QC/ lOT '3 D _8 ! Q~O> JI-ll('S'lLWJl -Z:DII Ch II q 1-l'biPY I t.ClZ;1 1.$11&..6 III () \ I 101 '""~ 8 ,,~·.1.Atl~ITJ-\ I \. \llL~l gji]~ C91 I z.GIP I ~~ \ I 19 1/ ir/O"Zf tiD ~SD-tfID rV1..~l{ I 1", (,(0 q Total 2:>;r.,-\UV ~~~<t ...{ (:z.? Z j01 4ft-. -z, 1ft1 \.t--~~ 9c.~ t1 i--A~'erage 'i Additional (Extra) Leak Check Infonnation DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak ,Check Vac ("Hg) G t () . v~y ~ .,.0 _ r"\"' Page.Cof C Run#J i sQ N A Port Reference 0.0"_ Ports are 9.5' Upstream from next disturbance Ports arc 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe Z -:f-b Cp 0.B4 Nozzle Calibration f . '3 ~O . 3}-o . 3H ,3 Y AvgD". ~~cSi~ --- Gas Bag C -('Sb Console (p Y-Factor -" "t '3 ~H@ , . ~ :>inh-r,o Barometric Pressures Pb z., "'. ~D in Ho Pb"' ~ "I , ,,( :s-in H: "--~--- PL -= . o· 5 in H20 L""kChcck Pre aMi ft'/nun C>~bV -005" vacill Ifg 1.'t-~ PI tot R3te 0·0 ~. 0 InH,O . "L$" . '1,.5 WatcrCol!ected e~S . 1-g Time Sampled ~ min Review (;t' K-@Tm K= @Tm Rate (ft3/min) ~ __ Field Data Sheet Plant: Deniso!,! Mines Date: ?.. \ \'" l L I Tr:l.Ver31:! Time DGM ~p ~H (',H,O) POi nt Clock Min (9) (fT)) lIIlH)O) Desired Actual 1 :)-: LtD 0 ~.5 I .\o\ -dt6 ·1 3 '1') 1 15 " S-~. -:\ 10 'O'f;, _~t) .~V 2 30 C;S-~&'.~2, 1 ·o'f,) .~~ . ~3> 2 45 bTt-. Y!;' .0'1:3 ·~U -~() 3 60 .<6 (gfo . ~ 3S" 'D~ U ·1-'-1 .i-'-\ 3 75 )('fL{. '1 ¥Y' -01, . % {) ·Yo 4 90 '1 D?·~ '}\ -b'1~ ·~o '50 4 105 9/1k6~ · 0 '1 -1 .. ~~ ,y,") 5 120 "'Il-t:'J cS 'Oyt .~"\ -yc, S 135 '1 ;, 1. "flO ·0'1S' .$-~ .y~ 6 150 VJ"'O·lJLt~ · OS) I '11"1 i .0./ 6 165 C;6'O.;t.jD ~D~ )'00 \ ... ,,) 7 180 CfIlO'71 "\ -O5"} I '60 }·OO 7 195 4+D.t-t\ ,057 I· c> {) I· P L? 8 210 q~O :L~ · I1ti5' ! 'o"f !.ovj 8 225 q'1-O . '5' ~ "1 --051-J'b r-\'0 t- II: 'iO 240 / 0" D . G"c.1! , j{{ '1 . 'Zr-'lb Vacuum (inN:!) -v ?/ 1/ -1/ "V -V ~. ~ \..I, l7 CJ 5' I.,? (., ill -r Filter 5'tXf TETCO r&tCl' SampleBOx~ Location: NortlfYellowcake Dryer Scrubber Operator: \ Pv \ ----, Temperatures (~) Stack (T,) Probe ProbcOut Filter ~5' 1, ~6 t"J1-l.. .. yv ~~ £.,. '-{ '1 'Z.4.( '2.-» ~~ -v'1:'> 1."'11 t. to( I ~-:r-Z~ -z..'{ '1 'ZHI ~X z, "\ I 1.5'1 Zll'1 _1l~ 1..?9 t. ,5-~5) aj £,1.'1 lSO ZI-l{ 9f~ 1" 'l--"" Z4~ 1-"<S' _~ l 1.:;C 2'-11-Z'-t) ~ 'f' .~ 7.e:;; Z~y .C6 ") tV)" ~5\ 2-...(.5 ~l 1/5r '7 '-I. '1 v-{~ ~(j ~lJ:7 1SO. ~\.{y 1(~ '2--~3 'ZS''-( 'Z-{ ~ i-~ 7~? ls;v l;·rt ~"\ tql-\ ~~() 1..<.{ "'I Eft1uent '1)' yt 4<6 5t:J t)D Gt S-'t... .:;-, 5', 5'1 53> s--\ ~1/ 5-3 SO ~C> ---------'------- Total I L{ ~, 1--''1D oJ -- Average -J Additional (Extra) Leak Check Information DGM before leak Check Vac ("Hg) Rate (ft3/min) DGM After Leak Check !60D.C:>c...( I Co\. 005- DGM T cmp (T m) Out In ['1 _~ "t--,- ~ -11 } '1/ _<ir0 --W t:;i~ 1f~ ~r ~S-CjD ~r ~I "0-'1 ,)1- f?Jo '1S' ql ~& ql '1~ '1) '1~ q.<-j ,., q~ 10/ 1<1 10 1 ~1 (oj Vac ("Hg) v Page _I _of _ ~ Run;l,g i sQ N A Stack Diameter 18". _ Port Reference _0,0" Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe 2 1--G Cp 0.84 Nozzle Calibration ·3~O .3~C> .3.f-( 3s-f Avg Dn -'.t " .=,-inchcs " .e-Gas Bag /-:::--0 J Console (p V·Factor j "13 6H@ { ~ 53: in H20 Barometric Prcssures Pb",Z c..j. '3~ _inHg Pb 2 "'I · 2 l' in Hg ·TI'-7~ ":~ ____ inHl0 '" Look (,h",,'<' ell) Il'/min 0·0 o~ v>r ,n H3--..bj Pilo, Rat. <,. 0 1,",0 ~ Post o -OOL( '2T O. D .'tS Water Coilected g Rata (ft3/min) Time Sampled /\ min Review K= K= I7J @Tm @T", --c;:-Field Data Sheet TETCO Filter Sf. I r Sample BQx ____ _ Plant: Denison ,Min s Dale' z., , ,l. 1/ Location: North ~lJowcakt Dryer Scrubber Operator' 12:1 I Traverse Time DGM I'>P .6H (111 H~OJ Va~uunt Temperatures 'OF: POint Clock Min (8) (1,.1.1 tloH,OI Desired Actuiil (JIlHz) Stack (T,) Probe ProbcOut Filter Effluent '-f <> 1 Jl·.r~ 240 ". SO\ fl·c>:> -~ct A "'I 1.,-t:<'f -2,10 ru-0 tZ~ 5"'1 ,~ 1 255 ((.7.-1S-'O~ . q",( A i "7/' s<1--' t-1-1 L'7~ "2-;5'" s r 2 270 2.D .") ~ "f ,0"-\ q .'tu ·QO z.,. '~(p "l~S 1.) . .f&t t.'13 5"? .z, :S-2 285 'O·~b~ Oc.(~ -<?to -qO ~ ~(o 't.=t O 'l~-z.-~\~ 5'1 3 300 L{o·orl .b5D -~~ . '1 ~ ~ C6-' I--ZtiO 1.,W 1-)(P 5'S ). -3 315 L{Q·12S :~5'V .'15' '''5" 3 ~ 25'~ 23~ 2"31 S-t{ > 5>'1 ;f,bS-'I'd ·c;.o ,&'to ? 7f I-* ~3+ '2'3;;-3S-• 4 330 .0 [> 4 345 {lJq .1 ... '-I". ,o? .'1 }-.c;"1 "'"3 ~(Q ~ .. {; 2;7 t~\ 5'h D 5 360 ¥ .O~15 05''1 1.(») I ·b ~ ~ t.?c:" nc.> 1.-~ 1.-11 5'; s 5 375 «~ o ~'1 ,O{)) J ./ L{ '·tt-! ~ ~'1 14$ 1,4 'Z. ~3 ~"Z- n 6 390 '1' .11r\ ·05« /. (0 )·1 t} 'c; tjD '2. (P(" ~v... Z't\ .;--S . ~ 6 405 II D '1,..~-z, ·O~ ,.OS l· (» 5-VJO Z '-t<J 1M,t? 1."5) ~'-f >u 7 420 1 2 O.Y~\ d7S'5 /-ot; t '0<;-0 Gj'l/ '2. '-1.5 Z-3ft.; Z. 'l S'-f .. 7 435 I~·if~? -0'50 ,'\r-.e; c.,-L;, q'V ~ l{t.--1.-1f" lsi L,-<-/ b 1-- " 8 450 [.J.D ,loU -o4.¥ -"tl ,0\ f.o ~> "2'1~ 'Z:{i "l-'"tZ 5'"> .s-a 465 jtfq. l~~ -O(..lY ,~ ( A I (p '11..-t5(P l...W 1.~ l 5) IS·~ 480 I G''i. JTU l5"r_~(, '; ~ , !'"/'1.2.crD --._---- Total ")01-, \5'1 ,I 1-.l \ ~~ -·Z'1·'6<1 2.'?Jt 0 .,/ Average oJ ' ~ '0t;1 ' q 'r"! co~· \ Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate (fe'mln) DGM After Leak Check t Db \ _ ooC; , DGM Temp (T m) Out In eq'i q-z. ~s--(o f 11-It:; ~ .!1'tf tD ~ '1'1 /05 to (oJ::; fO't.-led J bZ 10"1 10> 10 -:t /01.. to '~ 101. 101- lot !o¥ /0 '?> lor 10<-J 0<; tbj laY 1D~ 105£ ?,fD}- 0-., ~-. L( Vac ("Hg) Page Z--_of z.. Run # _ 2.. i '0 N A Stack Diameter 18" __ Port Reference _0.0"_ Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-13 % 21-b Probe Cp~ Nozzle Calibration ", 3 ~D .3~C> .:s~r .3 fl Avg D, • ~ 110S;;:;ches Gas Bag j::: -O-.S- Console V Y'Factor~3 I'>H@ (. (;5' 1m HP B3romelr~ Pressures l'b", Y . ~.,) _ in Hg Pb 'l,...~r-, H r ~l-_Jn g p;V ~_inH20 , Leak Chock: Pre Post L I fi'/mm 0.00 t Q. (.jO '1 vac in Hg '2 / -L.5.. Pi tot Rate Q.'O C·G InH,O . Z;;= " <-,:j--- Water Collected "'-'7-? 3 :;1, ~ v g Time Sampled '7/-80 min Review pc; J K= @T", K= @Tm Rate (ft3/min) Yellow Cake Dryer Baghouse Prelim G pts blank Facility Denison Mines Stack Identification North Yellow Cake Dryer Baghollse Date r Barometric Pressure B PbOi ill Hg Pbl' inl-lg N 0 Static Pressure (Pc;) in HtO A Estimated Moisture (BwJ I % Sample Height from Ground feet Comments: Stac.k Din 16 Referen~e: 0 Ports arc 57" Upstrc.am rrom next disturhanc.e Ports .1re 468" Downstn~wn from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F I 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11.26 :) 85.4 13.66 13.66 6 95.6 15.30 15.30 Averages: Ts ___ _ L Plow ----L\P ___ _ ,JL\P ---- KEY => ____ Field Data Sheet B A Plant: Dellis(lII Mines Dale: "2. f ')'/1 \ Traverse Time Point Clnck Min (6) =±j 't: 'Z.3 0 to ----.U '2:0 4 )0 5 c.j~ 6 So 1 IO:1.{ ~O 2 70 3 ~o 4 ~o 5 100 6 ~ :v \I:z..i 11.'C -I _ TOlal • ~ ....... !) ..... . C'OIT1II'l:1ll~ Time q '''-' . '-) <i'·~6. K>~6' )0 \ 'Llo TETCO Fdter_ S 11 S Sampte Box---.!2.. _ DGM aP tt.H (~HzO) Y:lcuUn\ if .. ') (in. liP ' Desired Actual (m II~' 11111.001-. z.z.. l.( L I.t 'Z-:> l%"i..\.t{t) 11.::> I,n \ .11 "3- l~o,<{~ ''Z.3 l..t) l.t") 3 l'l·S'" I tCf l . 't-r "Ii) 'i 2ot."l'10 <ill \. fs' l'J)" ~ l..l'~. 1'(0 ,~\ 1·51 1,;1 'i 2.t.L 11>3 • '2.\ 1·01 L.el 3 ,t<i_~CiO '1.0 t.oL l. tlt. I.{ Z'}b. 01(' '(0 l.o;:,'t, I.~t.. It 2. 't3. 0 is' 1'7.." l."n 1.'i1 'i 'l.Sl 110 .}u ~,'f'-l.)l.. t.{ Z{'1.J~) .. ~o t· {z. t, )l. "\ 2{'7.350 -----~ <it. )~B .J G,. o{,~~./ lS.&3/ I • 51)!)~ L. )o~ Baghouse tiP Time 8aghouse Ll.P 1.., \ ,0 '. 'i-(' 3·9 1'~ \~~o~ ~\ , ~. \ 1.~ Location: North Yellowcake Dryer 8aghousc Operator M. 1"'\ s,-.L~ u.- Temperatures (~11 Stack (T,) Probe Probe OUi Filter Emuent S5 '2.(.,~ l.~ 27<;) "''1 Bl l.V{ 2'1k? l~~ Sb B8 (7'0 1.~(o ZIo7 57 ~{>; Z-7C 2.'t.3 lb.} 57 ~O 1.~1' 2<t't 1..10» 58 ~t ZZ1 £.I{L 2ro{ !-( 'if "Z. ~1.. l.'-I1. (b'2.. <"1 9'0 1.(1 ~ '2.f2 5<1 '11 2:)1 'Z..'.q 2.1"'1 S~ 'i\ "2:31.. l"}e U8 (00 1~ N:> 1.~{ ",-t "0 CD 2.4l 2"£0 2bD (.0 ----- lol€ .. / ~cr. 6 -~ . " EJ50.r!'-'> DGM T.",p (Too' Out In '7 11 €?. -ec..{ ~J 9l Cfa 70 qlf I~<> ~t. IO~ Cf(" 101 '1, loe \00 Ito 100 Ito 100 ut Loi hi --- 2. 3t.ll/ 'il.( Page _ ~ of. _l_ Run #_!_ B t AO N Stack Diameter 16" Port Reference _00"_ Ports are S7" Upstream from nexl disturbance Ports are 468" Downstream from last disturbance Assumed Moisture % Prube I ~-~ Cp~ Nozzle Calibration .,.1 .2.7'" .z.1'(., '1..1~ Avg Do • ~'{8 inches Oas \3ag Ambient Air Console --.2. Y-faclor j. -'0 l <lH~ l. ~ 6e. in H,O Barometric Pressures Pbm -Z -, _;) .1 _ ill Hg Pb" '2.-l."f~ il1Hg p'J -.Ie inH,O Leak Check Pre Post n"lmin 0 .,00] O-OO'Z.. .... a::ulHg L\)60 Pitor ~aft: O· '0 ~IH,o q·O 1=D 0-0 ~ '" !~I{.,... Water Collected ________ _ : 7 t:) Time Sampled _____ _ Review K= K-- ~ @T" «iIT ...-' '" g mIn North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custod y Lab Analy i APPENDIXC c North Yellow Cake Dryer Scrubber METHOD 5 Date: Facility: Denison Mine Stack Identification: NYC Scrubber ---------- ~--~~~------------------------ ~. ----IMPINGERS IMPINGERS 5l [l- IMPINGERS Final (g) Initial (g) Net (s) Run: I - drop out , 7f)J'1 Lf13.o ~1'2..\l Run: drop out , Final (s) gt () . 0 Initial (g) I..ll1. (c, Net (g) 3~ 'l.. • Run: 1 - drop out . l Sample Box: C- Impinger Number 2 I J I 4 I 5 6 Inilial Volume of liquid (l-hO) in impingers, (ml) I 100 I 100 I , , I • Sf> <f. ?, 15q·~ "21.'\ ~l"'l.( 5l~.':3 {..I(fl.( l'oo0. ~ ("f)411 z.C06,o 1,1.3 1(1.1 \0.0 Total (s) ======= Sample Box: lmpingcr Numbel' 2 -I ..J.. I 4 I .2.. Initial Volume ofliquid (1110) in illlpingers, (ml) I 100 I 100 I Total (g) ~======== Sample Box: lmpinger Number -*-I 3 I 4 I 5 Initial VoluIne ofliquid (HID) in impingcrs. (ml) I 100 I 100 I Silica Gel • 85'1. ~ <. ~c.,Co I ~3'o 6 Silica Gel 6 Silica Gel Final (g)-----1------+-----I----f----.-l----- Initial (g) ------+-----+---~-----_r----+_----Net (g) ============~====~================== Total (g) ======= -_._-------------------... _-------IMPINGERS Run: Sample Box: Impmger Number .,L ..L I 3 I 4 I i 6 Initinl Volume of liquid (liIO) in impingcrs, (ml) drop out I 100 I 100 I SilicaUcI , Final (g)------I------I-----If-----+----+---- Initial (g) -----+-----~--~r_----r---+_---- Net (g) ============~====~====~====~~==== Total (g) ====== 7../IS/1l Plant._t""V_·~_Yl_1_·7<--C>_(/\ _________ _ ",u\IC c:)Cr-,"--Location __ l_Vl .!....I_~ _________ _ Analytical Method __ ~-=---________ _ Do" 1i;I Tesl No. Gns Bag No, ,-0 Ambient Temp ,t Opemtor -'/;-di-'-9<:.t--- Date 1)/~ )11 Test No. 7..- Gas Bag No. ~-D2' Ambient Temp ~~ Operator Gas COl O2 (Net is Actual O2 Reading Minus Actual CO2 Reading), Nl (Net is lOa Minus Actual O2 Reading). Gas CO2 I Actual Ntt Reolding ~·o ?,o 'l,{).b 11t.o [i~WJ .. Actual Re~ding ~,() ~. c) RUN 2 3 Average t\ctual Net Aetu.1 Net Net R(.din~ R~ailing Volumc 5·0 5.0 .? Q ~() ~.O "('c>6 ( 'f.cj ?rJ·(l fl·C) , t·o ~I ;~.;.Iil '.:V.i~~:Jit I~~:\.x;.~th (*,~lfNr~l~ Average Net Ac.fual Net Net Rellding Volume 3·0 ~·o .s·c ::; ·6 3-d 1'1 'i ) £:;. J I (P't u''/ RUN 11----r------11f------..;2r----11f-,----......:3i----l1 A\'erage Date -----Test No. ____ _ Gas Bag No. ____ _ Ambient Tcmp ____ _ Opcrator ____ _ Gas 0 1 (Net is Actual O2 Reading Minus Actual CO2 Reading). Nl (Net is 100 Minus Actual O2 Reading). Actual R •• ding r-;et Actual Net Reading t 01 was dctcmlined using a gas analyzer CO is not measllred, as it has the same molecular weight as N1 Actu.l Ne' Rtadiug Nct Volume Yellow Cake Dryer Baghouse NYC Baghouse M5 Facility: Denison Mines Date: L(l'; Ilr Stack Identification: ~N.;...Y;...C;;..:::B.;:;JagO!::h.:..::o..::.us:..:e:...-. ___________ _ JMP[NGERS IMPrNGERS IMPINGERS Final (g) lnitial (g) Net (g) Run : Sample Box: j) Impinge .. Number 2 I 2... I 4 I 5 Initial Vllium • of liquid (H20) in ill1pillg~rs. (ml) 100 100 I I SilicaGd I I I . . , ~ ~cr~.'1 (,Cf8 I'L-~ I ~I. 1 Pll "" 110., (0 "0.4 (, OG-(. I q, t;'~. (" ~ 13.'Z-l,~ S', (, IB·o IO,rL n (. Total (g) l) ======= Run: Sample Box: 2 Impmger Number I 3 I -1-I 5 6 Inilial VoIUlIl\! ofliCJlIId (H20) in impingers, (ml) 100 100 I I Silica Gel I Final (g) ------I---~-----+---_4_---__I_---- Initial (g) ___ ---1 ___ --I-___ _I_----I-----I----- Net (g)===::::::::!===::::!:===d===::::::!::===::::::!::==== Total (g)======== Run: Sample Box: tmpingel' Number 2 wi. I 4 I 5 6 Inilial Volume of liquid (H20) in impill!!,crs, (mf) 100 100 I I $i]icaGel I Final (g) ------Ir---~---_I_---_4_----+----- Initial (g) ____ I-__ ---1 ___ ~------+-----1--_-- Net (g) ======6=====~==========~====~~==== Total (g) ======= IMPINGERS Run : Sample Box: ..L 2 tminger Number I 3 I 4 I 5 6 Inilial Volume of liquid (11)0) in impingers, (ml) 100 100 I I Silica Gel I Final (g)---.-----1f------I-----4----I----_4_---- Initial (g) ----ii-----l----I-----+----+---- Net (g) ======~====d=====~====~====~~==== Total (g) ======= Chain of Custody Record TAI.. .... '~.(I(l(17) CJtfJnl Tetco Address 391 East 620 South Cfl)l American FDrk I~~e IZ;:~~3 ProleCl Name and /..(r.ation ISla.&» Denison Mine 20111st Quarter c.:onwcllPutt:lIll,*, OtrJE(/QlJoIC No. ---. Sample I.D. No. and DescriptIOn Dale (CQ(1~alr1ef5 (or eaen sampiB may b~ comblfleti on one 1m) R! Baghouse filter 15715) and beaker 2/15/2011 R1 NYC filters 15714,5716) and beaker 2/15/2011 R2 NVC filters (5717,5718) and beaker 2/16/2011 . . . -- . .. -.. -..... --- Temperature on Rcr...elpt __ _ TestAmerica Drinking water? YesO NoD THE LEADER IN ENVIRONMENTAL TESTING Prol"ll~qe-Dale Cbofll (tf CWlliJdv l\Iumbe; Dean Kitchen 2/18/2011 ,ol6Phallo Numbs( tA(sa Ca::e)fFax Nurrt;cr W Numbltr 801-492-9106 Page of ._--Site Contact LabCWllacr Af'.81Y6is (Artat:h lisl if Scott ctnisten$en,Ryan Palmer more space Is nesded) C1mierJWilybi!1 NlJmber SpeclallnstructJonsl I Containers & Conditions of Receipt Matrix '" Pre9ervstives c ... ... I ;; '" ... N 'l' N .,; I s ~l I ~ § § ~~ '" F ,;, .. Time 1 l ~ ::> ~ !l . ~ ~ ~:;: . f-i -.. I 10:00 X X I I -l-I 1 8:00 X X 8:00 X I X I I l I ! . , I I . 1 . , '--I-I 1 I I 1 ! I , j , I , I I I I ! I I .. _ . . -J POSSible HlIZUid fdcoffficalion .J ~mp.! Dispa..~ (A fee may lie OS8el!lJed if fIafrIPIefJ ere retllined o Non·Hazard o FlrlmmBb,'tl o SKin 'rrilMl o PoisonS [lUIJka.;>wJL DBmumIa CfJent o Di$p068IByLab o ArchiIIB Por . __ Mo.'1Ihs IoogBr thiiIt 1 mcmh) nlln Around Tlma R6tiuJred ac P.(J4uircnrtHiis (Spedfy) o 24HcufS o 14Vays o 21 0ays C orMr as Der.meth.od 1. R9OtJ11IlJd By ODto ITIl7li1 A .,.. "". ___ J._...J ....... <1<. nI" ... ', ....... "'Y I ~~.. I ~~~~~~--------------------------------~~~------~------~~~~~.--------2. Reflr.ovtSlted 8'/ I 3, FieaeMrrJ By ____ I ();up 17Tme Ccmm9fJ1$ When CDmplete Email to: Dean Dr Paul tetcD@tetco-ut.cDm DiStRIBUTION: WHITE -P.a~vmlJd /r; Ciienl ",ilt. qepr::l; CAi\!ARY -5:3)'$ ",'/:" It", s;;;r.;:JIi: piNK. P.okl Cq>y SDGNo. Order No. 42802 TestAmerica rptSTLRchTitle v3.73 TestAmerica Laboratories, Inc. Analytical Data Package Prepared For Denison Mines (USA) Corp. Denison Mine 20111st Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 14 Pages Report No.: 46110 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID R1 BAGHOUSE FIL TER J1 B240526-1 METXG1AA 9METXG10 (5715) & BE R1 NYC FILTERS J1 B240526-2 METXV1AA 9METXV10 (5714,5716) & B R2 NYC FILTERS J1 B240526-3 METX21AA 9METX210 (5717,5718) & B Batch No. 1055400 1055400 1055400 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Certificate of Analysis March 31,2011 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction Februaty 22, 2011 Denison Mine 2011 1 st Quarter Three (3) Stack Filter Samples 42802 CASE NARRATIVE On February 22, 2011, three stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J1B240526. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ill. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: Alpha Spectroscopy Uranium-234, -235, -238 by method RL-ALP-004 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. TestAmerica Laboratories, Inc. 2 Denison Mine (USA) Corp March 3 I 20 II V. Comments Alpha Spectroscopy Uranium-234, 235.238 The LC recovery yield exceeds acceptance criteria. The LC was recounted and is now within acceptance limits. The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The ample activity exceeds the MDA and detection limit for the ample and the batch blank activity is below the ample and the LCS. Data i ac epted. Except a noted tbe LCS batch blank sample and sample duplicate results are within acceptance limits. 1 certify that this Certificate of Analysis is ill compliance with the SOW and/or NELAC both technically and forcomplelene , for other lhan the conditions detailed above. The LaboratolY Manager or a de ignee, as verified by the following signature ha authorized relea e of the data contained in thi hard copy data package. Reviewed and approved: Erika Jordan Customer Service Manager Te tAmerica Laboratories, Inc. 3 Drinking Water Method Cross References r DRINKING WATER ASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) TestAmerica Richland's SOP N o. EPA 901.1 Cs-134,1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 i Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (uJ are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (ue) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S17n), where S is the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation ofthe general "Law of Propagation of Errors" equations and specific example are available on request. TestAmerica rptGeneralInfo v3.72 TestAmerica Laboratories, Inc. 4 Action Lev Batch Bias COCNo Count Error (#s) Total Uncert (#s) lie _ Combined Uncertainty. (#s), Coverage Factor CRDL (RL) Lc Lot-Sample No MDqMDA Primary Detector Ratio U-234/u-238 Rst/MDC Rst/TotUcert Report DB No RER SDG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmerica Report Definitions An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by the equation (ResultlExpected)-1 as defined by ANSI NI3.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, Ue the combined uncertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width of the confidence interval, 1,2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default" nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 * Sqrt(2*(BkgmdCntlBkgmdCntMin)/SCntMin» * (ConvFct/(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume with a Type I and II error probability of approximately 5%. MDC = (4.65 * Sqrt«BkgmdCntlBkgmdCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFctl(Eff * Yld * Abn * Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/u-238 ratio for natural uranium in NIST SRM 4321C is 1.038. Ratio of the Result to the MDC. A value greater than I may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than I may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order Number. The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results are in the same units. The LIMS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. rptGeneralInfo v3.72 TestAmerica Laboratories, Inc. 5 Report No. : 46110 Client Id Batch Work Order Parameter 1055400 FFSR R1 BAGHOUSE FILTER (5715) & BE METXG1AA U-234 U-235 U-238 R1 NYC FILTERS (5714,5716) & B METXV1AA U-234 U-235 U-238 R2 NYC FILTERS (5717,5718) & B METX21AA U-234 U-235 U-238 No. of Results: 9 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample ID. Result +-Uncertainty (25) Qual Units 2.87E-03 +-5.3E-04 UCIISA 1.23E-04 +-6.2E-05 UCI/SA 3.10E-03 +-5.7E-04 UCI/SA 1.90E-02 +-3.0E-03 UCI/SA 6.21E-04 +-1.5E-04 UCI/SA 1.94E-02 +-3.1E-03 UCI/SA 1.23E-02 +-2.0E-03 UCI/SA 3.49E-04 +-1.1E-04 UCI/SA 1.20E-02 +-2.0E-03 UCI/SA Date: 31-Mar-11 SDG No: 42802 Tracer MOC or Yield MOA CROL RER2 94% 3.90E-05 9.00E-15 94% 3.15E-05 9.00E-15 94% 3.15E-05 9.00E-15 95% 3.35E-05 9.00E-15 95% 2.70E-05 9.00E-15 95% 4.40E-05 9.00E-15 100% 2.95E-05 9.00E-15 100% 2.38E-05 9.00E-15 100% 2.95E-05 9.00E-15 TestAmerica RER2 -Replicate Error Ratio = (S-D)/lsqrt(sq(TPUs)+sq(TPUd»] as defined by lePT BOA. rptSTLRchSaSum mary2 V5.2.12 A2002 TestAmerica Laboratories, Inc. 6 Report No. : 46110 Batch Work Order Parameter FFSR 1055400 BLANK ac, MEVA41AA U-234 U-235 U-238 1055400 LCS, MEVA42AC U-234 U-238 No. of Results: 5 QC Results Summary TestAmerica Ordered by Method, Batch No, QC Type,. Result +-Uncertainty ( 2s) Qual Units 7.2BE-09 +-1.5E-OB U UCI/SA -5.B3E-10 +-1.5E-OB U UCI/SA -S.83E-10 +-1.5E-08 U UCI/SA 1.11 E-06 +-2.6E-07 UCI/SA 1.24E-06 +-2.8E-07 UCIISA TestAmerica Bias -(Result/Expected)-l as defined by ANSI N13.30. Date: 31-Mar-11 SOG No.: 42802 Tracer LCS Yield Recovery Bias MDCIMDA 93% 2.93E-OB 93% 2.93E-OB 93% 2.93E-08 72% 113% 0.1 3.B3E-08 72% 121% 0.2 4.52E-08 rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uocert, CRDL, RDL or mary V5.2.12 not identified by gamma scan software. A2002 TestAmerica Laboratories, Inc. 7 Lab Name: TestAmerica Lot-Sample No.: J1 B240526-1 FORM I SAMPLE RESULTS SDG: 42802 Report No.: 46110 Client Sample ID: R1 BAGHOUSE FILTER (5715) & BE Denison Mine 2011 1 st Quarter COC No.: Parameter Batch: 1055400 U-234 U-235 U-238 No. of Results: 3 Result Count Qual Error ( 2 s) FFSR 2.87E-03 2.8E-04 1.23E-04 5.9E-OS 3.10E-03 2.9E-04 Comments: Total MDClMDA, Rpt Unit, Yield RstlMDC, Uncert{ 2 s) Action Lev Lc CRDL{RL) RstITotUcert Work Order: METXG1AA Report DB 10: 9METXG10 S.3E-04 3.90E-OS UCI/SA 94% (73.5) 1.02E-OS 9.00E-15 (10.8) 6.2E-OS 3.1SE-05 UCI/SA 94% (3.9) 6.42E-06 9.00E-15 (4.) 5.7E-04 3.15E-05 UCIISA 94% (98.4) 6.42E-06 9.00E-15 (10.9) Ratio U-2341238 = 0.9 Date: 31-Mar-11 Collection Date: 2/15/2011 10:00:00 AM Received Date: 2/22/2011 10:00:00 AM Matrix: OTHER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 3/30/11 04:48 a 3/30/11 04:48 a 3/30/11 04:48 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00101 Sample 0.00101 Sample 0.00101 Sample Primary Detector ALP213 ALP213 ALP213 TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdclMda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.12 A2002 TestAmerica Laboratories, Inc. 8 Lab Name: TestAmerica Lot-Sample No.: J1B240526-2 FORM I SAMPLE RESULTS SDG: 42802 Client Sample 10: R1 NYC FILTERS (5714,5716) & B Denison Mine 2011 1 st Quarter Report No.: 46110 cac No.: Parameter Batch: 1055400 U-234 U-235 U-238 No. of Results: 3 Result Count Qual Error ( 2 s) FFSR 1.90E-02 6.4E-04 6.21E-04 1.2E-04 1.94E-02 6.5E-04 Comments: Total MDCIMDA, Rpt Unit, Yield RstlMDC, Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert Work Order: METXV1AA Report DB ID: 9METXV10 3.0E-03 3.35E-05 UCI/SA 95% (566.3) 9.42E-06 9.00E-15 (12.6) 1.5E-04 2.70E-05 UCI/SA 95% (23.) 6.17E-06 9.00E-15 (8.2) 3.1 E-03 4.40E-05 UCI/SA 95% (440.1) 1.47E-05 9.00E-15 (12.6) Ratio U-234/238 = 1.0 Date: 31-Mar-11 Collection Date: 2/15/2011 8:00:00 AM Received Date: 2/22/2011 10:00:00 AM Matrix: OTHER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 3/30/11 04:48 a 3/30/11 04:48 a 3/30/11 04:48 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00115 Sample 0.00115 Sample 0.00115 Sample Primary Detector ALP214 ALP214 ALP214 TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.12 A2002 TestAmerica Laboratories, Inc. 9 Lab Name: TestAmerica Lot-Sample No.: J1B240526-3 FORM I SAMPLE RESULTS SDG: 42802 Client Sample ID: R2 NYC FILTERS (5717,5718) & B Denison Mine 2011 1st Quarter Report No.: 46110 COC No.: Parameter Batch: 1055400 U-234 U-235 U-238 No. of Results: 3 Result Count Qual Error ( 2 s) FFSR 1.23E-02 5.4E-04 3.49E-04 9.1 E-05 1.20E-02 5.3E-04 Comments: Total MDCIMDA, Rpt Unit, Yield RstlMDC, Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert Work Order: METX21AA Report DB ID: 9METX210 2.0E-03 2.95E-05 UCI/SA 100% (415.7) 6.74E-06 9.00E-15 (12.3) 1.1 E-04 2.38E-05 UCI/SA 100% (14.7) 3.89E-06 9.00E-15 (6.6) 2.0E-03 2.95E-05 UCI/SA 100% (407.7) 6.74E-06 9.00E-15 (12.3) Ratio U-2341238 = 1.0 Date: 31-Mar-11 Collection Date: 2/16/2011 8:00:00 AM Received Date: 2/22/2011 10:00:00 AM Matrix: OTHER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 3/30/11 04:48 a 3/30/11 04:48 a 3/30/11 04:48 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00116 Sample 0.00116 Sample 0.00116 Sample Primary Detector ALP215 ALP215 ALP215 TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdclMda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.12 A2002 TestAmerica Laboratories, Inc. 10 Lab Name: TestAmerica Matrix: OTHER Count Parameter Result Qual Error ( 2 s) Batch: 1055400 FFSR U-234 7.2BE-09 U 1.5E-OB U-235 -5.B3E-10 U 1.5E-OB U-238 -5.B3E-10 U 1.5E-OB No. of Results: 3 Comments: Total Uncert( 2 s) FORM II BLANK RESULTS MDCIMDA, Rpt Unit, Lc CRDL Yield RstlMDC, RstITotUcert Work Order: MEVA41AA Report DB ID: MEVA41AB 1.5E-OB 2.93E-OB UCI/SA 93% 0.25 4.79E-09 9.00E-15 0.99 1.5E-OB 2.93E-OB UCI/SA 93% -0.02 4.79E-09 9.00E-15 -0.08 1.5E-OB 2.93E-08 UCI/SA 93% -0.02 4.79E-09 9.00E-15 -0.08 SDG: 42802 Report No.: 46110 Analysis, Total Sa Prep Date Size 3/30/11 04:48 a 1.0 Sample 3/30/11 04:4B a 1.0 Sample 3/30/11 04:48 a 1.0 Sample Ratio U-234/238 = -12.5 MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Date: 31-Mar-11 Aliquot Primary Size Detector 1.0 ALP216 Sample 1.0 ALP216 Sample 1.0 ALP216 Sample TestAmerica rptSTLRchBlank VS.2.12 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 11 Lab Name: TestAmerica Matrix: OTHER Count Parameter Result Qual Error ( 2 s) Batch: 1055400 U-234 U-238 No. of Results: 2 FFSR 1.11 E-06 1.9E-07 1.24E-06 2.0E-07 Comments: FORM II LeS RESULTS Total Report SDG: 42802 Report No.: 46110 Expected Recovery, Uncert( 2 s) MDCIMDA Unit Yield Expected Uncert Bias Analysis, Prep Date Work Order: MEVA42AC Report DB 10: MEVA42CS 2.6E-07 3.B3E-OB UCIISA 72% 9.B4E-07 3.05E-OB 113% 3/31/11 04:13 a Rec Limits: 75 125 0.1 2.BE-07 4.52E-OB UCI/SA 72% 1.03E-06 3.20E-OB 121 % 3/31/11 04:13 a Rec Limits: 75 125 0.2 TestAmerica Bias -(ResultlExpected)-l as defined by ANSI N13.30. rptSTLRchLcs VS.2.12 A2002 TestAmerica Laboratories, Inc. 12 Date: 31-Mar-11 Aliquot Size 1.0 Sample 1.0 Sample Primary Detector ALP12 ALP12 -3 (1) en f. £r t""'1 ~ o ~ ::l. (1) .Y' 5" :-> -w Chain of Custody Record 0, ....... , .. , .... , Temperature on Receipt __ _ Drinking Water? Yes 0 No 0 TestAmerica 1111111111111111111111111111111 J1B240526 THE LEADER IN ENVIRONMENTAL TESTING Cllenr Tetco I r:~.~a~~;hen I f;~18/2011 iLCuWddiUi Mdless[ I ,'eJephoneN!J~r{Area.CodB)/FaxNumoor . UlbNumber 391 East 620 South _ ' 801-492-9l06 i Page of _ Cily l . 111 Slate 1,.,2li;>~ _ Site Conracc Lab COI1tacr Analysis (Attach Jist if Amencan Fork I LUL I~ 84003 S"'ttChrist.n'en,R .... P.lm.r , ;':()(ffl spac9lsn9ed9d) Proi~ Nmnc eM Lw;alion (SIa1e) Cam"eQl~ybll1 Number ~I~ Denison Mine 2011 1st Quarter _ I II, Special lnstructiom C<JnuncflPutctuwe 0rriarIQu0t9 No. . Containers & ei Conifltions of Rece~ Ma/fIX Preservatives I _ :il ~ r:: I· . 1 "'... "l: ,~ r;<. r;< ~ ~r=: Sample I.D. No. and DBsClfption Date Time 2· _ !! g 8 _ 0 \5 :::. ~ ;. ~ •• (comaJneJ'S for each samp19 may ba combinsd 011 ana lhe) i ~ ~ ~ ~ I ! ~ ~ ~ ~ l~ I. ; _ .. -I [I! "I ~rA 1(''''; -:3:::7<"" --:/r.~ Rl Baghouse filter (5715) and beaker . P1S/2o.ll ; .... 10.;0.0. .. ' X ! X --l .L1f/( 10 71J'i\.. \. J \ /' J.J I .... ~ ,(S9'l 50'/: I Rl NYC filt~rs (5714.5716) and beaker ! . 2/15/20.11 'l ~:Do. J xl I ~ II J )~ ~rrlX \[7' (r;, ~ .i;/f; [R2 NYC filters (5717.5718) and beaker I 2/16/20.11 : 8:OOl Xl I j x: -I . A~ 1~f1 .)(V ..... [7 L. .... ~j)ttt7. -.. ~ .2., I 1:!r==J ! j c.. L -~I I I ! I I 1 I L ..... -_ ·C~I I I I f I , II. . ~ l l I I I I I Possible H8ZDId /rJstlIifiCstion ISamp!~ ~ fA fee maybe assessed if samples are millintJd o Non·Htrzarr:! 0 FlllI1Imabl" 0 Skin Irri/IJIII 0 Poison S 0 Unknovl(1 0 Relum To ClIent 0 Disposal By Lab 0 Archiva For ___ /lfoTllhs l«Igor thm 1 mJn/h) Thm Around Time RsquJred Q~-F!Oqulrom6nl:l (SpecfJY) o 24Hours o 14 Days 0 210ays 7ime ~ .::i:L /O/l??"L, 3. R<1!r1qulshedBy CommB()Is When Complete Email to;DeanorPaultetco@tetco-ut.com DISTRIBUTION; WHIrE· Rerurned 10 Cfielfl wiUr Report; CANARY-Stays witll tIlE Sample; -FINK -Aela Copy TestAmenca 1!1t1J12'@.1fI.#' &m®'¥g*,~~Q -riE Li:.ADER !N ~NY'ROI"-l"-"ENTAL Ti:.S7ING Sample Check-in List D8efTnn' """,iv,d, -2 · 22-.;2:1 ~ 30h'?( GM So,",n R,,,"t (om) _---',~.Z?~_ (~) · yr-Initials(t]) Client: =v -f2r"\...J ~DG ~: .L/JZ8oz !\A [] SA.F ;';': ________ !\A [ j -\I,;O::-K Order ~I!wbe~ v-~6ZVO S 26=~6 ::'f C).lS~;)c:,::,:: __________ _ Shipp~g Container ill: --6 . .o.ir Bill ;';' ---------------->6j heD 1 dJrougD. S for Ship?iDg cam2.iner only. bitiai 1'.ppropriae :espozse. 1. 2. ~. 4. Custody Sec.ls cllited and signed? Ch2.in of Cuswdy resod present~ Cooler tempe:ramTe: ____ K.~ Yes-1)l No [ Yes1)] ~o [ ~"'o CU5lOdy Se2.i l 5.Ve::nicu1l1e'packmg m2.len2.l.5 is 2':A [ hem 6 ;:h;ough 10 for samples. Ini1ial 2.ppropr-ia.te response. 6. 7. 8. 9. 10. 1l. 12. Number of samples in shipping container (Each sample ID2.y contain multiple bottles): Sample holding times exceeded? ~pleshe.ve: ~tape __ custody seals NA[ ] Yes [ hazard labels .L§ppropnate sample labels 3 CO 2 C6dfri~tJ1/J ] NO.VCj jYL{ ~¥f~. 111111111/ 111111111111111111111 J1i3240526 S~les: (fjifl L A. ) ~ are in good condition 'I.. 'fVt() __ are leaking __ are broken. ~ __ have air bubbles (Only for samples requiring no head space) Sample pH appropriate for analysis requested Yes [ ] No [ J N/A rAl (Note discrepancies in #13) (If acidification necessary, then document sample ill, initial pH, ~~t ofHN03 added and pH after addition) RPL ill "# of preservative used : _______________________________ _ Sample Location, Sample Collector Listed? * *For documentation only. No conective action needed. ~No[J Were any anomalies identified in sample receipt? Yes [ ] N~ 13. Description of anomalies (include sample numbers): NA [ ], _____________________ _ ~ee other side for additional comments ,~~ sample Custodia~~~" Date: 2·22~6~ Client Infonned on. _________ by __________ Pe.rson contacted. __________ _ [~NO action necessary; process as is Project Manager 2~'9., q lTtd4~ Date,--=~:.....-_tz.,_=__L....!...(~( .'-1 _____ _ TestAmerica h~bQM:o¥re'S·, irtc.1 0/1 0 14 APP ENDrx D North Yellow Cake Scrubber Figure I. Facility Schematic Representati on Yellow Cake Dryer 8aghouse Figure 2. Facility Schematic Representation Process Data (Retained by Denison Mines) D Fadhty Denison Mines t a t y Stack Identification: North Yellow Cake Scrubber 1+-0-+1 , , ~ a: Distance upstream from next disturbance, feet ---- ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet ___ -:... 0: Stack Inside Diameter, incbes ____ _ Estimated Moisture, percent Estimated Temperature, of ----- Estimated Velocity, fpm ~, ~ ---~----- Control Unit Type: Scrubber Number of Ports Figure 1. Facility Schematic Representation Process Type: Yellow Cake Processing Focility Denison Mines t a t y Stack Identification: Baghouse 1+-0~1 , , 13 a: Distance upstream from next disturbance, inches 13: Distance downstream from last disturbance, inches y: Distance of Sample Level to Ground, feet 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, "F Estimated Velocity, tpm Control Unit Type: Baghouse Number of Ports 57" 454" 65' 16" 0-2% 125 1,400 2 Figure 2. Facility Schematic Representation Process Type: Yellow Cake Processing Denison Mine Process Data J I Source: NOlih Yellow Cake Date: Z-/U")~/i( Scrubber Flow GPM Time #1 #2 L\P ~< DD CJ~ \ L\. I ~ r ::}-- C() , 'S () ~,~ i '-\. \ .~ I '~ c1 00 ~·I.I \~. { -S,ld "} , 3 i) q .! \>, ~ ;.(., I j) -D D C, ,\ \~, L. ~, 's (c). ~() 01.t-\ ~. &, ).~ ,,: 6(;> q,c I ') -1-~.0 I ( -~ /) "t ' ... 1 /),y '7' t, ''f'r)O I 1/ ' (,\. sr 1'3'1 ~.~ (z. ! ~D t1·s tY,c) 1·& r ) ~ U lJ C!,)' (4· \ '-:1 ~ :)' \ 7" ~I.) c,. ~ ~ ~1 f ,'''-~.G, tL.{voD q,? I~' u S· (p (f.-(. ~D ~'i ("3 '} ~.~ \ >.' v D o '~ , ? 131~ '?, S,-- ( ~ : "?o 0 ·'z..... I)' 1" ),{" I{;'. (,JD 11'. \ t~· ~ '~,~ 1(': -Sl,) °1·( (<:;.) s· ~ Denison Mines Process Data ) Ji'.~ .·~1 ---r.: I ( Source: North Yellow Cake Date: Z (~ , Scrubber Flow GPM Time #1 #2 ~p J:~ () q.) l~· Y ~. "?:> ~>:, () () ~'1 ( <;, 1-)·3 r: ?V OJ. [.,1 I)' & ).) '1~oi> ~·1 l~'"Z. ; . .> t:1: 70 '1 .7 (~.q '3. z. rv ~o 0 C;1, S \~.c) 7 'Z: 10:") [) c1 (, i Yt0 )·1 II :0 D ~'1-..j " ~ ~.) \ ( '.3 0 "-1.~ lU, "3 5·, IZ:o() q.Co t t-~ 'f ~ • ..-z, l'l~ }O ct· S L L.( , 0 $' '7 t -S: D Q tf·5 lY,O ~'3 I"'?: 3[.) OJ. !t I J t \ > r '2-- (1;1.)0 &1.Y; It-{ . ( ~. -z. 1'-1',30 CJ.& \ ,( . \ ~.z.. I )' DO c,.S-l L~ I \ ~. I I ( j D 0'C, \. l..\ r-Z-~. \ !G ~ 00 £1.1-lL(·~ 1·Z r& : -,() APPENDIX E Cali bration of the console dry gas meter(s). pilOllUbcs, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in Ihe Quality Assurance Handbook. The appropriate calibration data are presented in the fo llowing pages. The nozzle calibrations are recorded on the first page of th e field dala sheets. Figure 3 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pilot Tube Inspection Data Sampl e Box Temperature Sensor Ca libration E Temperature Sensor , ~probe Type S Pitot Tube Temperature Temperature Sensor I mpinger Train Optional, May 8e Replaced 6J An Ec.uivalent Contlenser I Temperature Sensor Nozzle I-W Tra::.ed sensor~ Gooseneck I 1-------------- Impingers ~ ~ / Pn:be ------""'\ / Type S Pitot Tube ~ Stack Wall Glass Filter Holder Hea.ted Area Manometer Temperature Water Sensors Orifice Empty Silica Gel By-pass Valve Main Valve Air-Tight Pump Figure 3 Schematic of Method 5/114 Sampling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ !!GZ &I -'WJIi*1!i, ~~ 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells. YELLOW ceUs are calculated. METER SERIAL #: I--=.:==---t CRITICAL ORJFICE SET SERIAL #:1 1453S EQUIPMENT 10 #: K' I TESTED .-------.----11 FACTOR I VACUUM G G G RUN# 1 (AVG) 2 3 2 3 2 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 (In Hg) 12 12 12 13 13 13 13 13 13 155.004 161.521 168.043 136.700 142.672 148.297 116.20 125.809 131.075 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 161.521 168.043 174.568 142.612_ 148.297 153.926 125.809 131.075 136.357 6.517 6.522 6.525 5.972 5.625 5.629 11.609 5.266 5.282 74 82 74 83 74 83 74 81 74 80 74 81 74 76 74 78 74 80 83 89 83 93 83 96 80 84 81 86 82 88 78 77 80 80 81 81 2011 Pre-Calibration FINAL AVG(P,.) 25.10 25.10 IF Y VARJATION EXCEEDS 2.00%. ORIFICE SHOULD BE RECALIBRATED ELAPSED I 1 D:l AVG I TIMEa(MIN) 93 96 99 86.75 6.00 ~ ~ 5.3045 ~ 1.498 88.75 6.00 2.55 5.3046 5.3045 !J!l!l!. !.m 90.25 6.00 2.55 5.2928 5.3045 1.002 1.489 AVG= !J!l!l!. -lI.09 86 82.75 8.50 1.11 ~ 4.9104 1.004 1.532 88 83.75 8.00 1.11 4.5978 4.6215 1.005 1.529 89 85.00 8.00 1.11 4.5905 4.6215 1,!!l!I 1.526 AVG= ~ l!& 80 81 84 77.75 22.00 § ~ 7.9047 0.997 !,ill 79.75 12.00 0.40 4.3273 guz ~ 1.432 81.50 12.00 0.40 4.3264 guz 0.997 !,ill AVG= ~ -lI.38 The following equations are used to calculate the standard volumes of air passed through the DGM. Vm (std). and the critical orifice. Va (std). and the DGM calibration factor. Y. These equations are automatically calculated In the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR. Y = I 1.001 (1) (2) (3) Vm(.,dl = K , * Vm. Pbar + (I!.H /13.6) Tm Pbar *6 Vcr!."d ) = K'* ~Tamb = Net volume of gas sample passed through DGM. corrected to standard conditions K, = 17.64 OR/in. Hg (English). 0.3858 "KImm Hg (Metric) T m = Absolute DGM avg. lemperalure (OR· English. OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T ..... = Absolute ambient temperalure ('R -English, 'K -Metric) Vcr(SId) y = -- K' = Average K' factor from Critical Orifice Calibration = DGM calibration factor Vm(std) AVERAGE AH@ =1 1.485 2 AH@= (0.759) AH (Vm(std») Vc.(std) Vm Temperature Sensors Reference tn Out OF 32 72 203 OF 32 73 201 OF 32 73 202 Pre 2011 5 console METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. t:s-,., ..... , ~. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN celis, YELLOW cells are calculated. METER SERIAL #:~ CRITICAL ORIFICE SET SERIAL II: ~ EQUIPMENT ID #: K' TESTED .----.---11 FACTOR IVACUUM G G G RUN# I (AVG) 2 3 2 3 2 3 0.8137 0.8137 0.8137 0.5317 0.5311 0.5317 0.3301 0.3307 0.3307 (In Hg) 13 13 13 - 12 12 12 12 12 12 443.725 449.104 454.492 460.802 466.60 ~2 477.70 482.955 488.227 USING THE CRITICAl ORIFICES AS CAliBRATION STANDARDS: 449.104 454.492 459.885 466.60 471.872 477.157 482.955 488.227 493.613 5.379 5.388 5.393 5.198 5.212 5.285 5.255 5.272 5.386 71 73 71 79 71 82 72 78 12 80 72 81 72 78 72 79 ~ 82 79 73 82 73 85 73 80 75 81 75 81 75 79 76 82 77 82 78 FINAL 25.20 ELAPSED ::l TIME (MIN) AVG e 73 73 14 74.5 § 76.75 5.00 78.5 5.00 75 75 ~ 77.00 § 17.15 7.50 78.25 7.50 77 n.50 12..00 78 79.00 12.00 80 80.50 12.25 AVG(P ... ) 25.20 § 4.5153 3.00 4.5039 3.00 ~ 1.20 ~ 1.20 ~ 1.20 4.3826 § ~ 0.43 4.3559 0.43 4.4378 2011 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ! ~ 0.986 ~ 0.988 ~ 0.990 AVG= l!J!M :!b§1 ~ ~ ~ ~ ~ 0.994 AVG= ~ l!J.l! 4.3370 ~ ~ 0.996 ~ 0.998 AVG= ~ ~ The folawing equations are used to calculate the standard voumes of air passed through the DGM, V m (std), and the critical orfice, V" (std), and the DGM ca6bration factor, Y. These equations are automatical~ calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I -0:9931 (1) (2) (3) Vm(.«d) = K, *Vm * Pbar+ (Mf /13.6) Tm Pbar *0 Vcr(."d) = K'· .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17.64 "RIin. Hg (English), 0.3858 "KImm Hg (Metric) T m = Absolute DGM avg. temperature (OR -English. OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T ..... = Absolute ambient temperature (OR -English. OK -Metric) K' = Average K' factor from Critical Orifice Calibration VCl(std) y= --= DGM calibration factor Vml,"/) AVERAGE AH@=I 1_657 AH~= ( 0.75 9 )2 AH (y"m(std)) V.,(std) \ V," Temperature Sensors Reference In Out OF 33 68 202 OF 33 67 202 OF 34 67 202 PRE Console #6 Calibration 2011 1.I!!!! ~ 1.775 1.662 !.!Ell 1M!! 1.534 1.530 1.526 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate Ihe dry gas meter which bracket the expected operating range 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of lime necessary to achieve a minimum lotal volume of 5 cubic feel. Facility Denison NYC Baghouse 4) Record dala and informalion in the GREEN cells. YELLOW cells are calculated. CRITICAL ORIFICE SET SERIAL #,,'--___ ..J K' I TESTED ...-----,..----ll FACTOR VACUUM RUN# I IAVGI (in Hg) G: 0.5317 15 0.5317 15 0.5317 15 269.70 l!74.838 274.838 280.035 2BO.035 285.285 D:~§ D:~§ USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 5.138 5.197 5.250 .0 .0 .0 .0 .0 .0 FINAL AVG(P",,) 25.45 25.45 EQUIPMENT 10 #: ELAPSED I ;;J AVG I TlME~MINI r:;J 72 Sol 59 Sol 64 57.75 7.75 1.20 72 59 64 64 73 65 7.75 1.20 72 64 69 73 78 71 7.75 1.20 I I II n :: §§ I I! III :: §§ IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 I 4.4733 ~ l,Q11 4,4621 4.5481 ~ 4.4566 4.5481 1J!ll AVG= 1...Q1! 0.00 AVG= AVG= The following equations are used to calculale Ihe standora V{Jlumes of air passed through the DGM. V, (sid). and Ihe critical orif~e. V" (sid) and the DGM calibration factor. Y. These equations are automalically calculated in lhe spreedsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = r 1.019 I (1) (2) (31 Vm,,,,, = K,. Vm* Pbar + (!1H 1\3.6) Tm Pbar * e . -K'* JiC'(JI:i) -•• ./Tamb = Net volume of gas sample passed through DGM. corrected to standard ccndrtions K, = 1764 OR/in Hg (English). 0.3858 'Klmm Hg (Metric) T m = Absolute DGM avg temperature (OR -Engli'h. 'K -Metric) = Volume of gas sample passed through the critical orifice. ccrrected to standard ccnditions TBm~ = Absolutg ambient temperature (lR -English, elK· Metric) K';;; A~erage K' factor fram Critical Orifice Calibratior VC';Jld) y = -"-= DGM calibralion factor Vm(J;dl AVERAGE AH®:[ 1 ~84 1 AHilIl = (0.756)2 AH /'!.mlstd)) Ve,(std) \ Vm b; .1,IQ§ ~ 1.664 POST Console #5 Calibration 2010 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES !is ",#,1_._ "'i.. ';;1'-;;" _~'V~ ~~. .-. 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. f' .. 3) Run at tested vacuum (from Orifice Calibration Report), for a period oftime necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated METER SERIAL II: 1--='-'-'-'------1 CRITICAL ORIFICE SET SERIAL II: I 14535 K' TESTED I FACTOR I VACUUM (AVG) (in Hg) G: 0_5311 15 0.15311 15 0.5317 15 161.753 186.171 166.717 171.871 111.871 177.041) D:~~ D:~~ USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 5.024 5.10 5.163 .0 .0 .0 .0 .0 .0 EQUIPMENT ID II: 57 42 41 55 63 61 41 56 63 75 61 56 64 75 81 1--1 1 1 I 1 1 1 I 1 1 1 INITIAL DGM AVG 51.15 60.25 69 0.00 0.00 0.00 0.00 0.00 0.00 FINAL 25.45 ELAPSED TIME (MIN) 6 1-50 1.50 7.50 § § AVG(P",) 25.45 1.20 1.20 1.20 § § Denison NYC Scrubber 4.4253 4.4188 !Jill IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 4.4222 ~ 4.4222 1.Q!!1 4.4222 1.005 AVG" 1J!Q! !!J!Q AVG= AVG" The following equations are used 10 calculate the standard volumes of air passed through the DGM, Vm (st~), and Ills critical orifice. V" (stO), and the DGM calibration factor. Y. These equations are automatically calculated in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.002 1 (1) (2) (3) Vm("d) = K, * Vlrl * Pbar + (tlH 113.6) Tm Pbar * e r _ K'* Y'cr(srdl -.JTamb " Net volume of gas sample passed through DGM, corrected to standard conditions K, : 17.64 'R!!n. Hg (English), 03658 'Klmm Hg (Metric) T ~: Absolute DGM avg. temperature ('R -English, OK -MetriC) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T,m' = Absolu1e ambiant temperature ("R -English, 'K -Metric) K': Average K' factor from Critical Orifice Calibration Vcr:Hd) y = -' = DGM calibration factor Vm(Jtd' AVERAGE llH@ =/ 1.S'!!:l 2 ~H@ = (0.75 e) llH (Vm(std,) V,,(std) V,. Temperature Sensors Reference In Out OF 33 67 121 OF 34 66 120 OF 34 65 120 Post test Console #6 1.110 1.682 1,lli Date: \'(-'1-/0 ~ 8:: I PA , t PB y _~;:~:~t.·.-.w -~ ., .•. :~ .,-.. rv ...... .,., .. ....,.1 1J1=l($" £ p, .... JI'v'_ ~ "·+:11 ! " r ... ~,..'i .. ' Type S Pitot Tube Inspection Data Pi tot Tube Id~ntiftcation: __ d1----=_-....:f:....-t'-=----______ _ Technician: k'. "It c,< N g tAA£-cr-.... Dt= . ~-)5-in Is P A = Pa ? _-'y_e.=,'-S"'--___ _ PA = .4S-0 m. Is 1.05' D, ~ D, ~ 1.50' D, ? __ Y.......=-c....-'--"'5"'--___ _ PB = • l( r:,-() In. «,<10· «1== a, < 10· a,= '1... p, < 5· 13, = __ ..:-__ _ Z 5. 0.125 in 2= • 0 l"~, l . in W 5. a 03125 in W= . QO'2._in. - W > 3 inches W= C& \ 11 '" in, Z > 3/4 inch Z= -'L .S< in, y ~ 3 inches y = --1 >Lc.:L 111. The pilot tube meets the specifications for a calibration factor oro 84? Temperature Sensor Calibration Reference '. Temperature Temperature Tcmp~ra!lIre Source Reference Sensor Difference (Medium) ("F) ("F) (DF) AIR 10 ~1 0 C') Probe Continuity .--7 \loU, ~ Heat Check 248 --? V-e.<':> ~(_V ,) AIR to ,6 () ICE WATER -Stf> }:.O r Stack Ball. WATER l..e:> t.( 1-h·l,. I SILICONE OIL Dal¢: DI y A pI A Type S Pitat Tube Inspection Data Pitot Tube Identification: _'1..--=._"'"'_-__ 6( ______ _ Technician: K. ~\..c.J-Q.c.~ Dt=. 3. 7 ~ .:...!P A:l-=_·_L-:..:.-/--'l../"-""S'---_11l -'PB"-= __ ,_f.[L...-jlJ'--z"--__ in CLI<IO· CL, < 10' PI < 5° p, < 5° Z" 0.125 in CL, = __ 7.-:-__ _ u, = ___ 1'---__ Z = _ • 0 (} z.. _ in. W= • C) ()J in. w = __ -3-= ___ in Z = __ ..l....-___ in. _-:--____ y 2: 3 inches Y = --..;S=-_l_I_y-'----_ in The pitot lube meets the speCifications for a calibration factor oro 84" Temperature Sensor Calibration Reference' Temperatllre Temperature Tcmperalur.: Source Reference Sensor Difference (Medium) (,,1') ("F) (01') AIR tV ~cr ( Probe Continuity -7' 'fe, S H~al Check 248 -9 \.( e,.-':;:, 2..&-0 AIR cO ()(o ~ I ICE WATER ":> -~ 3,"? f) Slack BOIL WATER cDS (JlJc; ~ SILICONE OIL TETCO Sample Box Temperature Sensor Calibration Date: 12/29/1 0 Calibrator: Mike MeN amara Reference: Omega CL35l2A Thermocouple Temperature Temperature Temp. Diff. Unit ID Location Source Reference Sensor or Result (Medium) (oF) (oF) (oF), P/F Oven Water 34 34 0 Water 203 203 0 A Probe Out Water 34 33 1 Water 203 204 -1 Water 34 36 -2 Impinger Out Water 203 203 0 Oven Water 32 34 -2 Water 203 204 -1 B Probe Out Water 32 33 -1 Water 202 204 -2 Impinger Out Water 31 31 0 Water 203 205 -2 Oven Water 34 36 -2 Water 204 205 -1 C Probe Out Water 34 36 -2 Water 203 205 -2 Impinger Out Water 34 36 -2 Water 203 201 2 Oven Water 33 33 0 Water 203 203 0 D Probe Out Water 33 33 0 Water 202 203 -1 Impinger Out Water 33 33 0 Water 203 201 2 Oven Water 33 34 -1 Water 203 203 0 E Probe Out Water 33 34 -1 Water 203 204 -1 Impinger Out Water 33 33 0 Water 203 204 -1 Oven Water 33 33 0 Water 203 202 1 F Probe Out Water 33 33 0 Water 203 201 2 Impinger Out Water 33 34 -1 Water 203 201 2 II Impinger Out G water~ 33 34 -1 Water 203 202 1 II Impinger Out H Water 33 35 -2 Water 203 202 1 Impinger Out I Water 33 33 0 II Water 203 204 -1 Impinger Out J Water 33 33 0 Water 203 204 -1 APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. Prepared for: SECOND QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORATION NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE GRIZZLY BAGHOUSE BLANDING, UTAH May 24-27 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines CorporatiQn 6425 S Rwy91 Blanding, Utah 84511 Date of Report: July 18, 2011 CERTIFI ATlO OF REP RT LNT 'GR ITY Technical "missions Testing Company (TET 0) certiHe that this report represents the lruUl (, well as an be derived by the methods empl,oye I. ~' er effort was l11ad ~ to obtain accurate and representative data and to campI with procdun::s set forth in lh Federal Regi Icr. ~1I1 Kitch 11 Revi w r: ____ ---<:::~:::.....::.~..o.:::..;"'--_/«__K~:.L_:.--'__--___ _ /)alc: _____ ---L-l_-.L-I.L..Y_~_-_1_1 ____ _ ~ Jo eph Kitchen R view "J """"""', ~ ........ D~lte: ..\e ~-1]5 ~ \\ ii TABLE OF CONTENTS Introduction Test Purpose ............................................................ 1 Test Location and Type of Process .......................................... 1 Test Dates ............................................................. 1 Pollutants Tested and Methods Applied ...................................... 1 Test Participants ......................................................... 2 Deviations From EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Summary of Results Emission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 4 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sampling and Analysis Procedures Sampling Port Location ................................................... 6 Sampling Point Location .................................................. 6 Sampling Train Description ................................................ 7 Sampling and Analytical Procedures ......................................... 7 Quality Assurance ....................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measw'ed Radionuclide Emissions .......................................... 3 II Percent Isokinetics ....................................................... 4 III Sampling Point Location .................................................. 6 IV Complete Results, North Yellow Cake Scrubber ...................... Appendix A V Complete Results, Yellow Cake Dryer Baghouse ...................... Appendix A VI Complete Results, Grizzly Bagbouse ............................... Appendix A LIST OF FIGURES Figure 1 Facility Schematic Representation North Yellow Cake Scrubber .......... Appendix D 2 Facitity Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D 3 Facility Schematic Representation Grizzly Baghouse ................... Appendix D 4 Schematic of Method 5/114 Sampling Train .......................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radio nuclide emissions from the North Yellow Cake Scrubber, Yellow Cake Dryer Baghouse, and Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat and Th-230 on the Grizzly Baghouse and U-Nat, Th-230, Ra-226, and Pb-21O on the North Yellow Cake Scrubber and Yellow Cake Dryer Baghouse. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 though 3 in Appendix D. Test Dates One run was completed on the Grizzly Baghouse May 24,2011. One test run was completed on the NYC Dryer May 25 2011 and one run on the 26 th. One run was completed on the Dryer Baghouse May 27,2011. Pollutants Tested and Methods Applied The tests were a determination of radio nuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. 1 Test Participants Test Facility State Agency TETCO Ryan Palmer None Paul Kitchen Mike McNamara Deviations From EPA Methods None Quality Assurance Joseph Kitchen Testing procedures and sample reoovery technique were according to tho e outlined in the Federal Register and the Quality Assurance I-landbookJor Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the fmdings of the test in Curies per dry standard cubic foot. Tables IV-VII in Appendix A have more detailed information. Table 1. Measured Radionuclide Emissions North Yellow Cake Yellow Cake Dryer Grizzly Baghouse Run # Scrubber Baghouse pCildscf pCiIhr pCildscf pCilhr pCi/dscf pCi/hr I 498.4 3.3 I OE+07 243.5 2.969E+07 0.277 2.158E+04 2 436.7 2.738E+07 AVE 467.5 3.024E+07 243.5 2.969E+07 0.277 2.158E+04 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (l\p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (l\p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test filters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. The test filters for the Grizzly Baghouse were had no visible particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities 3 None Percent Isokinetic SampJing Each of the tests were isokinetic within the ±10% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokineric sampling point by point. Isokinetic values for each test run are presented in Table II. Table n. Percent sokinetic Sam lin North Yellow Yellow Cake Run # Cake Scrubber Dryer Baghouse Grizzly Baghouse 1 2 99 100 99 100 r.~.,.-.. -" --~ ---. -I' . --. . : • I -I • ( " ", I : _.:1 _ ..1 ___ ~ -:.-= ~ __ ! ___ -: .. 4 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow , pressure and baghouse p readings were recorded and are found on the test run sheet or in Appendix D. Process Representativenes~ The facility was operated normally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure 1 in Appendix D is a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. The inside diameter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch diameter sample ports located 2.56 diameters (48 inches) downstream from the last disturbance and 1.31 diameters (24.5 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Sample Point 2 3 4 5 6 7 8 9 10 11 12 NYC 0.58 1.89 3.49 5.81 12.19 14.51 Distance (inches) from Inside Wall 6 0.70 2.34 4.74 11.26 13.66 15.30 0.50 1.26 2.21 3.32 4.69 6.68 12.08 14.06 15.43 16.54 17.48 18.25 Sampling Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment set-up, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook/or Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer 8aghouse Table VI Complete Results, Grizzly 8 aghouse Nomenclature Sample Equations A TABLE IV NYC Scrubber COMPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol DescriEtion Dimensions Run #1 Run #2 Date 5/25/11 5/26/11 Filter # 5786 5770 Begin Time Test Began 8:15 8:08 End Time Test Ended 16:27 20:27 Pbm Meter Barometric Pressure In. Hg. Abs 24.50 24.35 t.H Orifice Pressure Drop In. H2O 0.820 0.770 Y Meter Calibration Y Factor dimensionless 1.001 1.001 Vm Volume Gas Sampled--Meter Conditions ef 301.880 288.884 Tm Avg Meter Temperature OF 100.6 101.4 Vt.p Sq Root Velocity Head Root In. H2O 0.2375 0.2255 Wtwc Weight Water Collected Grams 719.0 737.2 Tt Duration of Test Minutes 480 480 Cp Pitot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.3795 0.3795 CO2 Volume % Carbon Dioxide Percent 2.80 3.80 O2 Volwne % Oxygen Percent 16.40 16.60 N2 &CO Volume % Nitrogen and Carbon Monoxide Percent 80.80 79.60 Vmstd Volume Gas Sampled (Standard) dscf 233.627 221.853 Vw Volume Water Vapor scf 33.901 34.759 Bws (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.127 0.135 Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.114 0.114 Bws Fraction H20 in Stack Gas * Fraction 0.114 0.114 Xd fraction of Dry Gas Fraction 0.886 0.886 Md Molecular Wt. Dry Gas lbllbmol 29.10 29.27 Ms Molecular WI. Stack Gas lbllbmol 27.84 27.98 %1 Percent Isokinetic Percent 98.9 99.5 AVG Ts Avg Stack Temperature Of 112.4 112.3 112.4 As Stack Cross Sectional Area Sq. ft. 1.767 1.767 PG Stack Static Pressure In. H2O -0.065 -0.065 Pbp Sample Port Barometric Pressure In. Hg. Abs 24.43 24.28 Ps Stack Pressure In. Hg. Abs 24.425 24.275 Qs Stack Gas Volumetric Flow Rate (Std) dscfin 1.11E+03 1.04E+03 1.08E+03 Q. Stack Gas Volumetric Flow Rate (Actual) cfin 1.66E+03 1.58E+03 1.62E+03 Vs Velocity of Stack Gas fj>m 9.39E+02 8.92E+02 9.15E+02 Curies Radionuelides per sample pCi 116431.6 96883.3 Crad Concentration of Radionuelides pCi/dsef 498.366 436.700 467.533 ERrad Emission Rate of Radio nuclides pCiIhr 3.31OE+07 2.738E+07 3.024E+07 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1.7). Symbol Date Filter # Begin End Pbrn H Y Vm Tm ..J6P WL,,,,, T, p On O2 O2 2&CO Vrn&td Vw Bws Xd Md M, %1 T. As Po Pbl' p. Q. Qa V. Curies rad ERrad DescriEtion Date Time Test Began Time Test Ended Meler Barometric PreS>lIre Orifice Pres<ur. Drop Meter Calibrnti()fI Y Faillor Volume Gas Sumplcd-Metcr Conditions A"g Meter TOIl1I,crntur • II Root Velocity I'lcad Weight Walet Collecled Dutnl[on orTcsl PilOI Tub<: Coefficient oule Dinrneter Volume % CorOOn Dioxide Volume % OXYIlcn TABLE V COMPIJETE RESULT ,PM DENI ON MINE CORPORI\TION Y ·LLOW CAKE DRY R BAm'IOU E Dimensions Run #1 5/27/11 5769 7:17 9:20 In. Hg. Abs 24.35 tn. H,O I.3l2 dimcllsionlcs. 1.004 or 88.585 "F 84.3 Root In. 1'1,0 0.5033 Grorns 26.3 1"f1nUlti 120 Dimensionless 0.84 Inches 0.2740 I'en:clll 0.00 Percenl 20.90 Vohm •• % Nilmgcn nnd Carbon MOllo"ide Percenl 79.10 VohuilC OIlS mnplcd ( I."dard) mer 70.493 Volume W"ter Vapor 5Cr 1.240 Freclion H,O II l'lCk Oas Frnction 0.017 Frnc1ion of Dry G.s Fraction 0.983 Moleeolnr WL Dry Ow; IbIlbmol 28.84 Moleculor WL Slack Gas Ibllbrnol 28.65 Pcreenl L okinelic Percenl 98.6 AvgSlnck Tempem!orc OF 105.4 SI.ck Cross Sectional ArIln Sq, Fl. 1.396 SI"c~ SIUlic Pr"55ure In. H2O -0.18 S""'plo 1'01'1 IlHmmelric I'",ssu.ro In. Hg. Alls 24.28 tack Pressure In.. !-IS. Ah< 24.267 rock Gns Volumetric Plow Rate (SId) ds.fin 2.03 '+03 Stack On. Volumclric Flow Rute (A.,ual) cfiu 2.73 +03 Velocity orSlne Gas rpm 1.96 '+03 Rndionuclides p"r 5111111'10 pCi 17164.8 Conccnrratlon orRndionuclides pCildscf 243.4970 Emission Rfllc of R .dlonuelides pCi/hr 2.969E+07 Dryer Bughouse ymbal Date Filter # Begin End Pbn, H Y Vm Tn, ..Jt.P Wt.,.'C T, p Dn CO2 O2 N2 &eO VmSld Vw Bw. Xd Md M5 %1 T! A. Po Pbp P, Q~ Qa V. uries Crud ERrad Description Date Ime TeSI Begsn Time TeS! Ended MOlor aftro""'ri~ Prc.sj;ure Ori fie. Pressuno Drop Meter CoJibmlion Y !'aClor Volume O~S ""'pled-Me,er Conditions AvS MClcrTempcmrurc S" Ro~t Velocity Hcnd Woisln Wmcr CoU.ct~<l DUll\liOIl ofTc:;, "ilo, Tube CocOicicm Noz:de Oiwl1elcr Volwne % Corbo ... Dio~idc Volume % O~y&.n Volume % Nitroge" Dnd CaJbon MonoKidc Volume Ow; Sampled (Sw.durd) Volulll. W.,cr Vnpor Froclion H]O in Slack 0 •• l'raclioll of OJ)' Ons Molec,,"'r W1. Dry Oos Molc~ulnr WI. Stnc~ Oa. Pereell! lookinetic Ai'll Slack TcmpcmuJlC lock Cross Scclionnl Area I.ck Siotic PresSI"" Snmp'c Poll Boro"""ri" Pressure tock Ptossure mek GlIS Vollln .. tric Flow R.,e (Sid) SlaCK Oos Volum\!tric Mow Rnle (/\C1ulll) VelocjlY of Slack OM Rtldlonllclidc.s p<tr SIImpl. ConcCfltrtlijOIl of Rnd iOlluel ides 'mission Rnto of Rndionuolidts TABLE VI COMPLETE RE$UL TS PM D • NI 0 MINE CORPORATION GRlZZL Y BAGIIOUSE Dimensions In. Hs. Abs In. 1-1,0 dimensionless of "F Roolln.lI,o 0","", Minutes DiJnensiOJllcss Inches Percenl Pctce,,, Percelll dscf sef fra.,IolI Fmelioll Ibllbmol IbIIbll10l rcrccnL OF Sq. FL In_II,O In. HII. Abs In. HS-Abs d>!cfin cfm [pm pCl pCildsof pCiIbr Run #1 5/2411 1 5785 7:53 15:58 24.20 0.863 1.001 310.106 88.7 0.2257 50.7 480 0.84 0.3700 0.00 20.90 79.10 242.234 2.391 0.0 10 0.990 28.84 28.73 99.9 71.1 1.917 -0.03 24.17 24.168 1.30E+03 1.63 +03 8.5J E+02 67.2 0.2774 2. I 58E+04 Gnzzly %1 = percent isokinetic, percent As = stack cross-sectional area (fe) ASL'lP = see ..JL'lP M5 Nomenclature Btu = unit heat value (British thennal unit) Bws = fraction of water in stack gas CB = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cf = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) Cmetal = concentration of metals (ppm, ~g/ft3, etc.) atomic symbol replaces "metal" CO2 = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) C -species symbol replaces x . x (avg)- Cx (eorr) = actual gas concentration corrected to required percent O2 L'lH = orifice pressure drop (inches H20) L'lH@ = orifice pressure (inches H20) L'lP = stack flow pressure differential (inches H20) Ds = diameter of the stack (feet) Dn = nozzle diameter (inches) EA = percent excess air ERB = emission rate of back half particulate (lblhr) ERF = emission rate offront half particulate (lblhr) ERmmBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point L'lP to detennine test point L'lH L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lb/lb-mol) MF = mass of particulate on filter (mg) MFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmol) N2 = percent nitrogen in the stack gas O2 = percent oxygen in the stack gas ..JL'lP = average of the square roots of L'lP (may also be referred to as ASL'lP) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) P G = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) 8 = time of test (minutes) Qa = stack gas volumetric flow rate (acfm) Qs = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (fe Imin, wscfm) Ts = stack temperature CF) Tstd = absolute temperature at standard conditions (528°R) Tt = see 8 M5 Nomenclature lim = mean molecular speed (em/s) Vm = sample volume (nJ) at meter conditions VmJ1d "" volume standard (dser), sample volume adjusted to 68~ and 29.92 inches Hg. Vs = velocity of stack gas (rpm) v we "" volume water vapor (scf) at 68°p and 29.92 inches Hg. W = Width of rectangular stack (inches) WL..e = weight of the condensed water collected (grams) Xci = fraction of dry gas Y = meter calibration V-factor (dimensionless) Method 5 %1 = VI1lsId ' (T, +460)' 1039 1 (0 ' V,' p.' Xd' Dn2) A,=(Ds'/4)on 8",. = V.., 1 (Vmsld +V..,) Co = Mil' 0.01543 1 Vms1d C(= Mrp ' 0.01543 1 Vm,rd Cx (eon-) = Cx (lYe) • (20.9· desired %0:0 f (20.9 • actual %0 2) D.,=2oLoW /(L +W) D, .... = "{0.0269 0 (Pb. + 0.0735) I {(T m + 460) 0 C, 0 X, 0 "[(T, + 460) 0 MJ I (I', 0 LIP)]) EA = (%02 -0.5 %CO) 1 [0.264 %N2 • (%02 • 0.5 %CO)] ERa = Cn • QI • 0.00857 ERr = Cr ' Os " 0.00857 ER",mBru = ERx I (mmBtu I hr) K·fact = 846.72 • Dn4 • L\H@" C/ • X/ " Md " I' •• (Trn + 460) 1 [Ms -(T, + 460) • (Pbm + L\H 1 13.6)1 M d = CO2 " 0.44 + O2 • 0.32 + Nz "0.28 Ms= (Md " XJ +(18 " B"",) P, = Pbl' + (Po 1 13.6) Q.=Vs·A, Q,= Qa" Xd " Ps " TsLd 1 [(Ts +460) " P.uJ OW =Os/Xd Vms1d = Vm " Y • T,rd • (Pbm + L\H 1 13.6) 1 Wild " (T m + 460)1 V, = 85.49 0 60 0 Cp 0 "LIP 0 oJ [(T, + 460) I (I', 0 M,)] Vwe= Wlwc " 0.04715 Xd =I -Bws APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Field Data Sheet Yellow Cake Dryer Baghollse Prelimina'ry Velocity Traverse and Sampling Point Location Data Field Field Data Grizzly Bagbouse Preliminary Velocity Traverse and Sampling Point Location Data Field Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Denison Mines Stack Identification North Yellow Cake Scrubber Date f!rl4-,,,:z~ UJ' I i Barometric Pressure Pbrn .l<J.'~ inHg Pbp .;J."/. «.3. in Hg N "0 Static Pressure (Po) -;O~s. in H2O Estimated Moisture (Bws) % Sample Height from Ground to feet A Comments: Stack Dia. IS Reference: a Ports arc 9.5' Upstream Ii-om next disturbance Ports are 9.5' DO"'1strcam from last disturb~nce Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F 1 3.2 0.58 0.5& lit 2 10.5 1.89 1.89 .01./1 3 19.4 3.49 3.49 III ,oS~ 4 32.3 5.&1 5.81 III ,0&2.- 5 67.7 12.19 12.19 lIb I ~(p ,0 6 80.6 14.51 14.51 110 , o~'f 7 89.5 16.11 16.11 I/O ,0(,,0 8 96.8 17.42 17.42 \ Averages: Ts LFlow ---- ~p ..j~P -------- KEY => ... IT_S __ --'-il_P_L_F_IO_w.,j1 11'-/ _ Fteld D3ta Sheet Plant Denison Mines Date mq,y 25. 20/1 ; Tril'~·cr:;c Time DGM ~p Point Clock Min (Ill la: I':C.CJ ~ 1 O~:I)" 0 {"OLO~~ .o"l B 1 15 ~ I 0, '4rL 10)'3 2 30 {.! 1 .. t'1,-\ • ())"3 2 45 40'S, I,:> • 1;))'2.- 3 60 "37.0(.1.-'05"1 3 75 Co ~(., • ')'2..:$' ,-,:)}) 4 90 Co. '6' 0 ,u.t;J 10Sb 4 105 (.:.,,'1,l3,{ '010 5 120 (" "1-). IO~ • o,""i 5 135 '<as. H.Z. IO("jO 6 150 "''f5 . ~'i~ ,01.'3 6 165 1 oS", 3 S"'/ .t1(. ( 7 180 1 \.5 .ll1-loJb 7 195 '1 l."\, \.(..l , ·~Sb 8 210 ,3 't, I-s'L • !>~(. 8 225 "1 '1":S,o,!-i ,,,6{ n\d 240 =If!> .(fS T \JfI\. "'~). 0'0"1 Ilo reo rill~r 515'\ Sample Box _ b J\H ~Ir, -1;:'1) V3cuum DC:Slnd Actuoi 'PllI!!! . (.6 ,~0 2- .1) ,-7'{ 1- ,1) tl') 3 tl~ ,13 (.{ ." ", '-i , 7 CO tf~ 5 loaO ,eD 5 1,00 /,00 ! • 'f'L 1'11..-7 ·9 -{' ''1{ e ''1.1 .q\ 10 ,10'0 ,g~ 10 .~\ .'a ( l\ ,~~ .<at U .~l ,o( t'2- .q,l:l ,'So l3 ---~--- ./ I.otation North Yellowcake Dryer Scruhh~r Operator M. "" ~rJ" .. vVwSo--. Temperatures \ h SracklTJ Probe Prot>.: Out FJiter Emuent ilL Z. 7)" lIt 27\ ("'4 113 '"2.1! l7'S'" i"1)" ~c.j ii3 ZiB Li? -Zl,y c.,C,( W2.. Z'"~ 2.,\ l,\ ~O ue.. 2'1'1 2.n_ 21'L. 56 II~ 2~~ 7.\.~ lG.c::' 5Cf 11<1 l'-lIQ 'Z.b) l.~)-'-0 11'\ Z.{L Zb""t 7.fo( 59 11-6 Z.fo 'lbl 1.(. I (01 uflt Z/~ 7..70 L7D b'1.- \\1' "2.,(, z,( Z,r-"i ltJ 2"1"L-2.1") 213 55 \10.{ 2" 1 .::1,-\ "l/4 5(" /' 210 z.1'i 1."1"t 59 In ~I) '2..70 1. 7'{ '2.(Lt (..l It) 25if 'Z"1"l 'll'1 (,'Z... TOlal r-\5 1.'1sot ... ~·'3l.~o 13.!{O/ j(3'1{'/ .A.\er8ge I 'J" 0 So ~ .1 j cp_ ,8'1 (,l 1If. 3 Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check Pag.< _I of l. Run " L DGM TOlnplT.! i B 0 N Out In (,,3 (,3 A b® It Port Rt:f~rer1ce 00" . Stack Diameter _13" __ l l{ CS t Ports are Po EB_ Ports (lr~ 6'1 '11... '0'1 ~S '1/ )oC) C:f~ (03- '1) lo~ 1 l 100 '11 110 100 110 I ()o hu \eo 1\0 \00 loq '1'1 100 --- lQ'11 / Cf3·7 ~ Upstream from next disturbance 9.5' Downstre,m from last disturbance Assumed MOIsture 4-13 % Probe )1-4-Cp~ Noale CalIb ration ~ ·;80 :;14 .~8D Avg D, -"'.719., inches Gas 83g ~ -OS- c.,n,010_ .... 5'--_ Y.f'actor~ "H@ ~ inH,O Barometnt Pressures Pb",j l'i.SO In H~ Pb,_q.4.43 ____ m Hg p,; -. OMS' in H:O LC<Jk Chc;!clo. .Er£. f~)/1II1n D.OOv ,.,<in H,; Zo.S' PiuIR", 0.00 ,,, 11,0 • ZIj ~. O.OOL 5,0 Cl!...QQ 1-r;' Watcr Collected S Time S""pled m,n Rc\'i~w K~ K~ '~{ZTnl til. i"'l1 Vac ("Hg) Rate (ftJ/m~ L \ '-\ Field Data Sheet Plant: Denison Mines Date: S l 'l,. 5} II Travene Time DGM 6P 6H i"H,G) Vacwm Point Clock Min (9) ,IlJ ~ {I"K;Ol Desired Actual ~I<lllg) A.. , 1 12'.1.1 240 15~. Sol ,o'i1. ,~I ·'l "L 1 255 Ib z.. 0'1) .0';[ ,1'-1 IlL( :s 2 270 110. (,{'\. ,O)'L ,') II)" > 2 285 17'1.'50 .tlO~ 1,'"1 .1'-1 '{ 3 300 18~ ,qc;(p .e,)! 113 113 5 3 315 "lP,S10 .oSI (1 ) 11 -( 5 4 330 ~O(.. g l~ ,0$'1 1"'1 111 G, 4 345 I BI(q.OL~ '0"" .qL , 't'L "1 5 360 8~·'1t..1 .0(,) .,~ .'1''-5 5 375 €3(". o'H lOb)' ,qt;. ,q" Cj 6 390 ca"(g. 'Bj .o{,o .'fo ."10 10 6 405 i~S-b, t'il • 0(.., .t\[ ,<\( l~ 7 420 16Cc,G,· or..~ ,~-s ,b ·8'"\ . €i\'{ 10 7 435 875,/01 .o{!., ,St{ , ~34 Il 8 450 ig25. 3l:.e . oj'£, .BC{ lSI{ l [ 8 465 ~'15, 013 I 6~C. ,S~ ,SI.{ \'L \1:" li 480 yo"t ,(03\ -lSI .ow l~d:fO 150,10.,0 ..j 1,6003 ,3;l 00 Total 3et 88011" /' --. /. Average ..j.,2~l) / 2(g,2..)O Additional (Extra) Leak Check Infonnation • 91..0) -/ THeo Filter 51'0(; Sample Box_~ Location: North Yellowcake Dryer Scrubber Operator: M. M ~M.Q...J:o:.-- Stack (1',) II Lf II" II)" tiLl 1I3 10 8 llJ Il, llO Ibl, !Ot 10 5 105" \ (J :) 1 a...( 10D l~") LU2 )5q~ 111.. 'i Temperatures ""') Prob~ Prnb.:Oul Filla Effluent ~3\ "l>1 '2.n b$ zro 'Z.5"'t lS,-\ G.( ,-~r Z,,; l.(.~ 5'1 1,",0 ZG.l{ 'U"\ f&,'G. Z)) Z"i l.C,if bo Z.1[ 7TL 'lTL G:.l 21') 1.7) 2-1) (...2 2(,,'6 l13 ~13 (..3 1 '\~ 270 l70 G:.3 lb<{ en. ZTL ,l. IC.~ l"'1\ ll\ (.,~ ~('f 2"1t Z'I G.t.t 'ZZ.~ 'Z.b'Z-l.l.L. Col (.~) ~"''6 1..'-'0 fa! Z.~) tt"-2..1 \. G,'L. l.c.,l 1..'10 lr'O ~'{ DGM before Leak Chack Vac ("Hg) Rate (fe/min) DGM Atter Leak Check DGM Tcn.p (T .. J Out In q~ 'iq 97 \<25 qcr 10"1 q9 lo~ Ci8 101 ~'i lOS LoL-11 0 Ib"Z-I\l 10L-113 I Q c.. 11 2- lof 11'-1 ~o8 (II {0'1 115 III llO UL J<..O liz... I~V c.. 'f:)9 fDa'" ,/ Vac ("Hg) Page ~ of -z. _ Run # I i sQ N A Stack Diameter _18" __ Port Reference _0,0"_ Ports arc Ports are ~ Upstr""m from ne>.! disturbance 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe ilJz Cp 0.84 N07--zle Calibration .319 .3~O ,:51'1. ,~:c~ AvgD, .11'\)' i:;:-- Gas Bag E.-Or Console--=5~ __ y -Factor ~. JO l 6Hl!I ~ '-l~I;..,"H,O Barometnc Pressures Pb", L L4, )'0 in Hg Pb 1. I.l· 4"} in JIg p ;- PG -• 0 (. ) in H20 Leak Ch«k Pre ft:"min 9. oef vacinHg 2..0.5 fes 0002- 5.v Pioo,R.,. 0.0 ~ InH,O C. as o.tf Water Collected ,ICC, 0 g Time Sampled 4 f)'O min Review' AIw;.. K= K= @T", @T~ Rate (tt3/min) , I I ---L-'-':':1_ Field Data Sheet Plan!. Denison Mines Date: \I\o\C<.v ~ t 2.c t, I Tmverllc "fIlTH! DUM "p ~H ...... .Qj VaCllUm Point Clock Min (8) dl\ IUIIII~). Desired & ) 1 g;Ofi 0 'rOS.l-I..( f ,0'10 .~r 1 15 '1t 2.. Cft.{o ,O~() .S? 2 30 ~lO. {'&'l ,ol.("Z-.~O 2 45 . /f.z.s, 5E~ .o<l.S' • (,<{ 3 60 <t3b .8<-tf .OLfr) .£.,(g 3 75 f1"<{~. :).I..!~ ,aut;; .fH~ 4 90 9:53. ~1-.oSS" ,~D 4 105 Q"1.li3 .o~-• €f> 5 120 'i'11. crl-~ ,0S8 ,8'1 5 135 erg L Llgc=t 058 .3<1 6 150 '1ctl O~~ CSt-·tH. 6 165 JOOD.Sl'l,. .O{gO , Eff 7 180 {OIO. ;S-O .o~ .18 7 ¥ 195 tD ,'t.!J 30 .06'8 '81 8 210 \02-9.09'\. • s:)t III 8 225 ' 038. t%.. . o 'f) ''') 240 l o<{ ~ .G.eS Total 14l, Jbl) ~.51tS !,:\verage oj .;z.,1,..%/ Additional (Extra) Leak Check Information Actual 'II'H!:'I ,S"4-Z.O .Sf 2,.0 .. ~o 3.0 • (,Cf '(.0 I {p(p 5.0 . (,'S' 5.0 .go 1--0 -8'0 'i.o -fe{ 8.0 • Sf{ ~~ ,fit IO.i> .8'€ 12..0 ·rB (2..0 ,81 11.0 loon \1.0 d.[ \2..0 jl,l('() ·1;s ./ 5710 TETCO 0 Filtcr_ Sample Flox I..) LocatIOn: North YellolVcakt: Dryer Scrubber Operator' .~ ( ~. !<t I,;" N7 Temperatures (I, Stack (TJ Probe Pr.)b<.' Out Fdter Eft1uent 1J1-23. '" l.3~ 2,~ ~ (",3 /1'?J :l.~ J.45" J.1.{l{ 1D.o 1/3 Z fa t Jv2 ;l(p2-&1I {(3 2-S0 ;?SB I ~ (.,0 /tv ~-c; '2SO 2$"'0 ( .. Z- II.$' :Z3~ zs-h ZS' (0'1 (I~ J.~f,; 2Sz... 2-52-&~ {I(P ).(pC( ?4fj Zf./P. &/ IN ;;H~'t ~C{r if.. 4. 0 (..2- I {'f ?-&Z-Ub 12<'> ~2 /13 ~&Co ~SB ~ (P3 III ;)[,,9 2.50 ~Sl !..c:- NO z.~o 2.>2:-z-sz-CP'2.. ~Cf 2S'f 2.,5) 25S" Utl.- lo~ 211 Z'io 'Z.'ia (pf,p 101 l'Z..t6 Z<.\) l'-\) &>J, ,-n{ / (0·9,; DGM before Leak Cheek VOle ("Hg) Rate (fe/min) DGM After Leak Cheek DGM rernp <T ~l Out In ('1 t..b 7f-f ~3 :n-83 ~3 '0 ~(s, ?S- <[0 100 'Tz /e;'Z- ~'t tOY 9':) /(){;;> 'ic" {tJf.... ?8 ~ /7 tiD tao /£1 10 0 ill 'it 'It..[ q, t o~ 3000'/ q~,8 Vae ("Hg) rage _ / "f_~ Run" -L i -0 N A Stack Diameter 18" Port Reference _00" Ports are 9.5' Upstream from next disturbance Ports are 9,5' Downstream from last disturbance Assumed Moisture 4-13 % Probe 1-'fCr Cp~ Nozzle Calibration .:ll.L . :lilo ~ .j~O Avg DII ~ '''¥is-inch~s Gas Bag f-o~ Console~ Y-Fact(lr / .O() , :\H@ r. 'I S'<Q in H,O Barometric Pressures Pbm _.2.~ ___ 10 Hg Pb" 2 '-/. l-f{ in Hg P;; -: O(,~ In H"O L~k nl~d.. rre n\:'min ()~OOy V['" 'r. Hg ZO.-; ~ 0.0 02.. 5.0 PI!ot R'lic Q. CD o. O() lnH:O ~ ~ Woller Collected g Rate (ft3/min) Tunc Sampled min Re\'ll':\\ K ~~Tm K-1ft: I-t t ){ ~ kvt J~fI II ~ 'lL! tl r't H'? S ~ ... ~ deW l\ R€.STA.tl (.Me \''5:£0 ~ \ t lL.l Field Oata Sheet Plant: Denison Mines Date (1.\ t..-I,. "L(, I lOll Tr.a .... ersc Time DGM ~p 6.H (" ><,0) POint Clock Min (6) (r.» (inH:.O; Desired Actual 1 I",:-q 240 5l. l'-\'l ' oS" .1S 1.f5 1 255 v;O.;"~c.( 'O~-~ ·S>3 .83 2 270 (per ,7~" .0ss ·~3 ·83 2 285 ~.z.€<1 '''55 .~~ .9'3> 3 300 g8.8z..~ -oC[1-·12-~rL 3 315 41.1'10 .O~r ,8-r ·'8t 4 330 lOt, ,('1't. .0Sl ,B'! .e'l 4 345 !'" .QZ2 ,O~) .N ~gc.r 5 360 /)..19. ,{1~ .Ol{~ . &'1 ,(/t 5 375 (,S.D1''-' • r 1.-l1.g~ lun 6 390 ("F€ .2..'tt ,o<l.S" .{,~ ,(..9 6 405 {Sr. 018 ,()t.{5' .r., 'i '(''1 7 420 lcP&.1-40 .oW .~( .(, ( 7 435 l/),Q4<" ,o'1t .,,~ <(:'3 8 450 { ~z..J-'?'i ·0(..[1 ·~3 ." !, 8 465 {'to.V; rS-,ollO . (, I , It;( 2o',t..1-480 Iq~ &t1... Total L ~~ .t~g~ I V ~. v~'t5 l1..~ " Va.:uum ,tllHRJ 3-1) <.f.r;) ~.D <t.O 'f.0 5D 5.0 S.O ¥..O q,D 1--0 1,0 '1-.0 1 ,0 7'0 r·l> THeo Filter 5111 SampleHox~I3 __ Location' North Yellowcake Dryer Scrubber OpemlOr: I'\~ 1.1-£ Mu-!~CI'--. Temperatures ~"fl Stack tT.) Probe Probe Out Filter Effluent If '1 ';l'-{p.; .2+0 ;}.(0-9 Vi> 1 1I3 2~B ~G..<t .;}.(p'f CoC'a 113 ~'-{1-P40 ~2-(;5 1(1( 2S1 ~~9 .2..G.fs ros- / IS-?,yD l-S'3 ;) '10 ,,~ lIS-).t..{o ~t.t/ :2U:O ~'/ /flo .;).tJ?. ;l(..'-{ -"48 (9.'-( /l~ ~'3 1~f."B ~3 !P3 /1 'I .;t.3(o ().so ')...I..{() {qJ ( ("2.-z-So 2.f.,C( 2.5'( ("'0 1t3 )..~'-! ~4R 2?>r 1;0 1,'Z...-153 i;!(...1 ;2'-lT ~ (13 ~f.,2... 2"7-0 2S~ ~( (1'2.. z5Q "L60 z,(..o (..l.. /11..-l1.{q 8~B J.~Go ~3 IfL/ 21'1 Uz. ;l.Sz.. (;3 18, [1' Average V (t.'l5{ / ,:rl-o / t ~2.>/ Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate (fefmin) DGM After Leak Check DGM l'm>p (T .. I Out In f'1 1?9 10 ( (0(0 105 il3 10& Ijb lO7-118- /6::; If t t(/f I'~ jO&;, fI£ lo(p j Ii- /0,<; itS' lOS-,u lOS 11(p lo,{ II£( /0') LI"Z..- lol... It./ lol.-II I )!i.1(.; 10(.'; / Vac ("Hg) Page "L of '-Run # 1---, ---- i BQ N A Stack Diameter 18" Port Reference _0,0" Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture Probe 2., ~ Nozzle Calibration 4·13 % Cp~ ,;'"19. ,,3180 l37<1 ,3Bo Avg Dn ,~1'i)' inches Gas Bag t...o) Console--,5=-__ Y-Factor~ ,~H@ \"'<-I~I:> ,"HoO Barometric Pressures. Pbm 1.4,~ )' inHg Pb. 'l.'{''l..-~ in Hg Pu -,'-i' inH:O Leok Ch.,~ Pre Eru! fi'ljmLn O ,OO~ f}.Wf V3C in Hg W.e t-eA) Pltot R3.te 0 ,00 ...JL9b InHzO 11..5' ,l.S Water Collected ::;-31-, -z... Time Sampled Review Rate (ft3/min) ~~D PRK. K ~ K= @Tm @T~ g min Yellow Cake Dryer Baghouse Prelim G pts blank '" Facility Denison Mines Stack Identitication North Yellow Cake Dryer Bilghouse Date S i"ll./II i Barometric l'ressure B Pblll 1..4.'\) in Hg Pb" l. .... ~~ in \-Ig N 0 Static Pressure (PG) ~in Hl) -.If, A Estimated Moisture (8w,) I n(~) Sample Height from Ground feet CommelJts: Slaek Din 16 Reference: 0 Ports are 57" LJpstremn Irom next disturbance f'orts are 468" Downstream frolll last disturbanee fjlflo Traverse Percent Distance From: Ports Point Diameter ID Reference A B C-&. D E F 1 4.4 0.70 0.70 2 14.6 2.34 2.34 " nO .1 'l • £II 3 29.6 4.74 4.74 4 70.4 11 .26 11 .26 "n .,,1 III ,1.1 5 85.4 13.66 \3.66 5' Ill.. (; 95.6 15.30 15.30 ,ii' .'11 Averages: Ts \1\ LFlow 6P ,"t.l\, "3 ~6P ITs KEY => L flOW! 6P • o'\;\ }l'j 5~ '~n \i) ~ Field Data Sheet TETCO (- Filter 57"~ Sample Box -Page ( of _( Run# L Plant: Denison Mines Dale: ~ ( 'L' ( U Tnl.vcrsc Tinle POint Cloc~ Min (e) 1 ~ 0 2 to 3 1.0 4 30 5 4.0 6 So 1 8!2D 100 2 10 3 80 4 '10 5 iffo 6 ilO -.5:'Z.o !tD I DGM (tl') 39.n'i 1b. ZCoz. S''>.,l(O O~.'i9\ (,~ LoO -1I-L. c.crs 8L1.,0 8'f.5~'2. q(", .,,, lo<{.5Se 112.. '\0'\ 11.O·I2.l 11.'.,,'1 i'lP ~H lioH~O) Ya'CIHlm ~'" 11,0, Desired Actual {in11t'l) .1.\ L·~L I.~, 1..- l"t\ 1..o"T I'~' 3 ~ l..l ""'t>'1. ,.lDl 3 l'2..g I,~f tillS" 'i 1'l..'i \ ,"{o il<./.r; i1 I~'" \. )4, 1.'3"\ '\ ,'2.'{ t. 'l.1{ I.-t"l to( i 1.(0 11")( 1.3{ _'1 1'1.(.-la, ll~"5' "I ~'t.q l·fo l,{O '{ (1.7 l.<'/O i,I.(O '-! l't~ I,q'( I. Ii"> 'i ~ Tot,,1 BB~ 5SS.,; (,.0'10 l \15 -lL{o"'" A\I,,:.mg,c ~ .50'?>:) L. ~ 12- Comments. Time I Baghouse aP Time I 3aghouse aP 1 :1.l 4.' 1 \(0 f-L ~ t:1.., ~ j l., S··~41 411.- Location: North Yellowcake Dryer l3aghouse Operator: M .I~ ~N ",.."",c,...( tr- Temperalures \~I) Stack (T,) Probe ProbcOul Filkr Emuent 10 \ 'Z7~ 21'0 Zeo b1 ! C"L-1.12. 1..10 1.1'0 ~" Ic~ ,,1r 11{ '2..1-{ S(" lOt{ 77'-Z70 1.70 51 loti 110 Z,{' t../? see lo~ 1.":; t'1f Z1)-5t1 lo~ 7..1'5 t 1 C!I 2.10 1.:>0 lO(" 2.10 1.1') 21'S 55 10 1 H} 1., I 2. il 51 ! &1 "t.t..<.t oz.tll 2(:.1 ~l 10'1 "If:,) 2(0 250 5~ 110 Zf'l Z;rl 2.n .59 I I i'Z .. laS ,.... ~5-,ll I DGM ·tc",pIT~) B i t AO N Out In lL ..,\ 13 1> Slack Diameter _16" Porl Reference _0.0"_ l~ Bo !~1 ~ Bf fi Co ~8 '10 91 ~" '-' 8z.. &b B7 S ~ e~ "10 1ft.. ~3 'IS' Ports are Porl, ore 2022.. '04.,,( ./ 57" lJ p;tream Cram next disturbance 468" Downstream from last dISturbance Assumed Moisture o· --..:..--" Probe 18 c.:, Cp 0.84 Nozzle CalIbration .21) .17:} 1'2.7'; .t.,tt Avg Dn • t 7"io inch~s Gas Bag Ambient Air Console .3 Y~Factor~ i'lH@ It ,,~, on H20 Baromenic Pressures Pb", '2.'1 , :3 5 in Hg Pbr '2 ... 1£ in Hg P . _. I e in H.O ~'. ~ l.oelk Ch,,,k-Pre fr"mln 0. 00 4: va:: 111 HE_1..Q.& !'ill.! D·OO"l---e.o Pilot R.'e 0 . 0 C.O tnH,O q.O ~ Water Collected ). Ii 3 !l TImc~m~~ ~n Re\'i:.:.w K~ K- @Tn~ @(f .. 8 5",-ne-~S Grizzly Baghouse Prelim 12 pts blank Facility Denison Mines Stack Identificalion Grizzly Baghouse Date /"Vlt.l'A1 ;U/ 10 {I i Barometric Pressure Pbm d-J1 .2.-0 in JIg Pbp ;;; l./. I t-in Ilg N Ao e Static Pressure (P (;) -.03 inHp Estimated Moisture (BwJ I o/., Sample Height from Ground SO feet Comments: Stack Dia. 18.75 Rdc,cnce: 3.0 Must use 36" Erobe or IOll!;ler to keeE box outside handrail Pools are 24.5" Upstream from next disturbollCl' ['orts arc 48 " Downstream from 1",[ disturbance Traverse l)ercent Distance From: Ports Point Diameter ID Reference A B C D E F I 2.1 0.50 3.50 2 6.7 1.26 4.26 cr/ _ ,()4~ 3 11.8 2.21 5.21 4 17.7 3.32 6.32 :~I,t Ol/ 8 5 25.0 4.69 7.69 6 35.6 6.68 j,,'1 ,. 9.68 ,O~ 7 64.4 12.08 15.08 8 75.0 14.06 17.06 ,,"I . ID~.r 9 82.3 15.43 18.43 10 88.2 16.54 19.54 vq , f)S2-- II 93.2 17.48 20.48 12 97.9 18.25 21.25 Averages: T s ___ _ LFlow l1P ___ _ '1'£'11' ___ _ KEY=> R'L __ Fiold DJt. She"t Plont D~Itl~OIl Mllt~s Date .Yi 0"f <24 j 1£> {/ T~:I ...... 't:4; Tlln~ [)GM .~P ~H LnH:O'. P(tJnl Clock Min (0) .h _1I.v, D~sired ActlLal b 1 1-:S3 0 Jq l. \?;P;, ,oSO ·ili.--,8~ 2 Z"o 303.5).'1 .O'{~ '1-~ , 1"<j 3 40 3($'". gOr .048 .&0 ·80 4 &;0 ~z.~. 2..(0 I o~""D ,at{ ·8« 5 go 3'1D.813 ,osO ·8't .&'f 6 10-0 3'33 . .55'8 .0S~ • a'''1 , 8"'1 7 /'Vv !>GC9./..2..eo 'OS~ ·87 · €'t 8 ~'-iO ,14. t..?CcLf (055 .q 2-qz... 9 1",0 '<t3.~~ ,O~O . !?.,;-·~S 10 [go I.j06'·~.a ·05"3 • 'to '7D 11 we '-1('t.).'-f.O 0)0 ·8~ 85 12 "l-"lO 143z.. j{P2-.fJso ,g S"" .8S- A 1 11:55 )..:.(f) 1445. II <{ .04) ,:;-7-,"if 2 'J.WJ 4::'-'1-. '3~9 .o<t~ .n .&'L 3 :L~b '-('to. () L(2, .O<{g .~l. .g2.. 4 ~OO '-Igz.. r5'& .oS8 I '?Cf .99 5 ~W l.{'90. S<t{p .os~f' .'i'-( · 'it{ 6 "3'-10 Z; If>. e>q~ OS-)' . 9'lf '7'1 7 l/iQ 52.3. ~tl ,05'3 ,'10 · '1-0 8 7:J<3'O S 3(0.801 .O'{f( .8'-.82..- 9 !.too 5 qq. so5' ,O~~ • g 't. .~2.... 10 l.fli) 5c"l.. (2..1 ,b~, .q'/) ,qo 11 lj'1D 575. 'Z..o~ .053 .~ ·qo 12 4/iO 58R L{81o ,(9) .'8'S-,b'S' IS: SJi Vjg7) 1&0 l. ;)...q L{ Totai ::'10. /vlo/-. ~.qlj0 2-0.,..( TEfCO Fil1er~t8J_n SampkBox ,: Location: Grial)' !3aghouse Oporator: POll! K.. KLtde-n V;;'(;!,lUtTJ T em pcTJ.tures \ I I -II" Stack (T.) Probe Prob.:OUl Filter t{·o ('5 .).<-11-d(,(o "):'to ~.D (p~ 'J...{.,O ;':;:0 253 «.0 I,a":f ~I.p~ ").~ 2 !{O <t.o (;g J.. 'i Z--).(Pf MIl '-f.b 4-0 )...4/P ~9 ).'{8 4.0 ~~ ).un IV t15o;;; 260 <f.b 13 ;;. t{O ;l..5lj l2~s £t·O :rtf Z~ 2.&b R--3" L/.V ?'L ~40 )1I5 l-30 Lf.o :;{p Z-S-(a .2.'-( f.2 'to <.(.0 '1-5 2,.) '-I ;t<,ts b2~2. I.f.V f:S 2'iz... 2.-53 2.30 3.0 :n 2:;-1 2S'{ ~3D '-I·V :t'i 260 2-5fg ~!.( 4.0 ~t-2(-11 'z<-t't 2.2.'1 4.D t( .;J-q. f ~Cj J.t.I6P l(.o i-or ~r ~S-f2.38 lj.o 1-3 2..32-J.'-tH ;2.30 ,(.0 ..10 7?JZ-:?.1L Zl6 '(.0 t.e~ l'-lO ~!..f~ -Z~I Lf.() &1 ?..SD 2.--50 &'33 tiD c.,~ '?-~3 J..&3 '2«0 'i.D 1'1 J~'1 25''6 ;}"35 l{.D 1''1--'L$~ ~'0 0~cr l1-0~ Average ..j .2.1..5'1/ .~u~/ ---±l:lJ r~mr;lr:llt~ DG~'I Temp (1 ",) EflllLent OUI In So &1-&~ 4~ ::;2-i? 50 17-8S' 53 1-1 '&¥ ~o ! {? I ~9 5"1-gz. 91 Sf ~3 'Z3 57 fS-~Cf. 5'8 g& 7.b &,0 ~t '7b f_'O 71 '00 f.so q, /t)f) &.3 ~8 cr3 Sl.... Ft 't'l 5'0 72-?8 50 CZ I ~8 ~ ~ ~ 9(0 5.3 ~f! 91e; 53 ~:r 9( S?> 9.0 r1-53 Rr 9< 53 ~S-qz, 53 88 CZS' ~~ ~ro 9<1 1../2 <)f? 'il~.t/ Pa~,,_\ __ or __ L_ Run" __ L i AO B N Stack Diameter 18. 75" Porl RI,;It:.n.:nc~ ~ Ports art: 24.5" Upsuc:am from OC.xt di~turbaOl.:~ Ports ~re 48" Downstream from la5t disturbance.! Assumed MOisture Probe S~ __ ..:... __ ~O Cp~ Nozzk Calibration ~ ~ .~1\) .'3:;-0 Avg D, .')100 inches Gas Bag Ambient Air Consok_""Sc-_ Y-Fa"lor~ :c\H@ /. 'tg&, ill H,o Baromt!tric Pn.::::sur.:s Pb", _;;1:1. '2..:0 Pbo ~'{.!1- p,,_...:'"'.03_ L"k Ch", Pre ft'Jr.1in 0.003 vac '" 1-1" 2.1. 0 PliO I R,,, D .00 Ir.H,O ,z...;' in Kg in Hg inH;O ~ I2..:QQl L.O 0·00 JS. WalerColkcled 5'0.7-g Time Sampled 480 min Review f'KK K ·- K~ /~r::'L @(rm North Yellow Cake Scrubber Sample Recovery Gas Analysis Dala (ORSAT) Yellow Cake Dryer Baghousc Sample Recovery Gas Analysis Data (Ambient) Grizzly Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain or Custody Lab Analysis APPENDlXC c North Yellow Cake Dryer Scrubber METHOD 5 Date: . -Facility: Denison Mine -------- Stack Identification: NYC s,C V'J 4~c..(L --=-:---::-----------------._ .... _._-- IMPINGERS TMPINGERS IMPINGERS IMPINGERS Run: C~ot:r' Sample Box: J3/ j lmpinger Numbel' I 3 I 4 I 2.. (j -Initial Volume of liquid (H10) in impingers. (ml) drop out I 100 ! 100 I Silica Gel I , . Total (g) -'1 , q . 0 ----_._----_._-------- Run: L-Sample Box: Ij I J Impinger Number 2 1 ..L 1 -L1...i.. Initial Volume of liquid (H20) in impingers, (ml) drop out I 100 I 100 I Silica Gel I Final (g) --'-.;;.:;.;---'--+...J....I..~~-t-i-~5.:..;:S~. ()~. -+"'-'-'''-=;....--t=---''''-t---:..~'-=~ Initial (g) ~n. I ~-=-~~-~-r----;=~~-~~~--r-~~- Net (g) :~!>~, ~ ====================================~== Total (g) -/3 ~r. L =========== ----- Run: Sample Box: lll1pingel" Number 1 ~ I ~ I .i. I 5 6 Initial Volume of \Iq.uid (H!O) in impingors, (ml) drop out I 100 I 100 I Silica Gel , Final (g)----t-----+-----f----+----of----- Initial (g)----+-----+-----f----+----t---- Net (g) =====~============================= Total (g) ========= Run: Sample Box: Impinger Number .l-I -1-\ .!. I 5 6 Initial Volume of liquid (H,O) in llIlpingcrs, (ml) drop out I 100 I 100 I SilicaGcl I Final (g) -----r----+----i-----\-----r------ Initial (g) -------+-------r-----;-------+------~-----Net (g) ====================~===================== Total (g) ====== ~ \ '-.. -,. II .,.-/ ... .' j--; b' "'i/ Plant ·D.e / 1 11i.L<.L..l..--I-\"~t.!£..:' Analytical Method ORSAT Date sfaS/1! Test No. _-'-__ _ Gas Bag No. t5. -05" "'> ./ A III h ienl Tem P ---""r:..<!/c_'So<..-__ Operator f)KK. Date 51 z ft, It I Test No. "2- Gas Bag No. -r-"',.---"o-?-;-- Ambient Temp 1 B Operator M 5 M Date -----Test No. ____ _ Gas Bag No. -----Ambient Temp ____ _ Operator ----- Ga.~ COl O2 (Net is Actual O2 Reading Minus Actual CO2 Reading). Nz (Net is 100 Minus Actual O2 Reading). Gas COl O2 (Net is Actual O2 Reading Minus Actual CO2 Reading). Nl (Net is 100 Minus Actual O2 Reading). Ga.~ CO2 O2 (Net is Actual O2 Reading Minus Actual C01 Reading). N2 (Net is 100 Minus !Actual O2 Reading). I Aclual R.ading llCO 1( .... 2.· !~~ .{j • ~:. i¥1 t~~lwj 1;7' " I Actual R •• diug ~.fb '20' "t "'" ;&'1, .... ::4 1'·~~rI . , .. -." I Arlual Reading Ill.; RUN 2 ",.t Actual Net Re.ading Z, e 2.8 2.S 1<0.1.\ ['tIL IlDA et>, {? f~a 80·8 RUN 2 "'el Actual Net Reading ~·6 :).8 3.8 l(o·{g 1.0.'\ l~'(. 1'1·10 I\~!l~~, ~,: :.\('~~l," , . ,ll. b RUN 2 Nel AClual "et R •• ding r~. ,~~, ('0 is !lot measured. as it has the same molecular weIght as N2 3 Averagl' Aclu,,1 Net Nel Readin~ VolUUle z.e 2.(3 2,B Iq.L.. 1101~ (~ ,Ll I~~·~};i"w'· .~ ... ~". . I ~~~ 8o,e Bo.8 3 Average Actual Nel Net Reading Volume 3.8 3·B 3.9 20,'-\ \ b . "-\ lo,~ W:~t:{ ~" .~~~ -,q.0 79. h 3 Average Actuall [\el Net Reading Vulume ,.~~I!i~ ~7:~~~~ Yellow Cake Dryer Baghouse Dryer Baghouse Facility: Denison Mines Date: S /:J.=f /1/ Slack Identitication: Yellow Cake Dryer Baghouse IMPJNGERS Filter Number: 1j't~?q IMPINGERS Filter Number: IMPJNGERS Filter Number: Final (g) Initial (g) Net (g) Run: I Sample Box: \? Impinger Number I =-2 I ,J. I wi-I 5 .ll. Inilial Vol lime orli'qllid (HlO) In ilJ1pinl!~r~. (Illil 100 100 I I SG I , : , , , . t-O C/. 0 b3i./ .h &1'-/ .S-Q43.z,. 1 ul, l. ClBvb G (') v I 'lZ~)\ '1 ..... 3,(0 (,.0 /' </ 1-l.§' Total (g) Z <e. 3 ============== Run: Sample Box: llllpingcr Number ..L1.l.1..1.1.2-. Initial Volume ofliqllid (HP) in ililpingcrs. (ml) 100 100 I I SG I Final (g) -----If------I----4-----+-----+---- lnitial (g) ____ I-__ --II-__ ----1 ___ -1 ___ -1 ___ _ Nel (g) ======~====~====~===========6===== Tol,L! (g) ====== Run: Sample Box: ImpingeI' Number ..L. .l. I 3 I -i-I 5 Initial Vol lime ofiiquid (HP) in illlpingers. (ml) 100 100 I I SG I Final (g) -----I---~I-----II-------I-------I------ lllitial (g) -----I-----~I-----I--------I---------I-----Net (g) ======~====~====~====d======b===== Total (g) ====== Grizzly Baghouse NYC BaghuuS"e M5 Facility: Denison Mines Date: ---------- Stack Identification: ~~=4-!~?..!::Z;::..~~).:fY ____________ _ -. GER' f; '/ J,c.(>,"- S7'iSr; IMPINGERS IMPINGERS Final (g) Initial (g) Net (g) Run: ( Sample Box: E IEF ..L Impmge.' Number .L I..:LI ...L ..§.. Inilial Volume of liquid (H,O) ill iml)illllers (ml) 100 I 100 I -I Silica Gel I I I , I • , . /'~f,S 110 tl.C/ (" I '-I.ftp Iq 90 .(o 7 o?O I{£ tf/t'. I ~tJCf. I 9J.fo, q -2./.$ 1';-,0 ~" 'Ie;, ~ Total (g)===-6=D==, r~=== Run : Sample Box: impmger Number 1 --!-I ~ I -1-I 5 Inilinl Volume ofli(lUill (H20) ill impingcrs, (Ill!) 100 100 I I Silica Gel I Final (g)-----I------il-----II------I-----I---- Initial (g) ___ --!I--__ --I ___ --+ ___ --+ ___ --+ ___ _ Net (g) =======6======b======b======~===~======= Total (g) ======= Run: Sample Box: Impinge.' Numbel' J.. I 3 I ...L I .£ 6 Initial Vulume ofllquid (Ii OJ in impingcrs, (JIll) 100 100 I I Silica Gel I Final (g)----I------If---~---_I---_I---­ Initial (g)----I------If------I---_I---_I---- Net (g) ==================~===========k===== IMPINGERS Run: Sample Box: IIllI,ingcl' Number 1 -..L 1.L1 4 Ii Initial Volume ofliquitl (11,0) in imllingcrs, (m!l 100 100 I I Silica Gel I Final (g)----I-----II----_I---_I------J.---- Initial (g) ----f------j:---_I----I----I----- Net (g) ==================~====~=====k===== Total (g) ====== Chain of Custody Record TAL4124 (1007) Temperature on Receipt __ _ Drinking Water? Yes 0 No 0 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ellem Proiect Meno.<1l!Jr Oaoc Cf/l;in of Cusfady Number Tetco Dean Kitchen 5/31/2011 Address --', i8/Sphone Number !Area Cooo}fFitX Mvnbcr /.JJb Numbe- 391 East 620 South 801-492-9106 Page of Cit}. ISlaw 1 I/O CcWe --'Site Coo;"Cl 'Lab Cor.taCl Analysis (Attach lisl if American Fork Ut 1,84003 S' ... Ch'i"..,.n.R""'P.imor morsspac9i6needed) Proiccs NlJme er.tJ LOIllIdM {Sl!1!!1 C;mi~'Wi!yb{!J NlKJlber Denison Mine 2011 2nd Quarter Spec/a/Instructions! (,'ontmctlpvrcna,g; OI't1l;tfGuolo Na, . COrltainer.; 8 c Conditions of Receipt Matrix Preservatives ~,:;: ;e ;;: --. ,-, I .. N '" 't> (contamers~~,::a: ~~~;~-':,,~~~:::::::'on Ol!a lm) Date ,77me ~ j ~ ~ ! ~ ~ 2 i ~~ ~ ~ : ,; 5785 Rl Grizzly filter and beaker 5/24/11 i 8:00 X X "" i l , • __ ---l-' --11--1--1-- 5784,5786 Rl NYC filters and beaker 5/25/11 1 8:00 X 1 'f..." 11\ 'f.. i 5770,5771 R2 NYC filters and beaker 5/26/11 8:00 X I ~ ~ X, X I 5769 Baghouse Filter and beaker 5/27/11 8:00 X I I X, ~ r... A I --I I --I _, I . I I : I I I ! I I -_. I '~'+-~-+-4-~~~-r-+-+-+-+-1-1~~~r--------------- Possible HszarrJ 1d!xlIIfiCIJdOfl IS!l,71PIt! ~sal {A fee l7l6y be es5~d if ssmp/es ale rtt~inEd o N",,-Hazard 0 Flammoo,'e 0 SiM '''*'''1 0 Pair"" fJ 0 (JfIknoo.m 0 R"rum To Clittnl 0 Dispo6Bl By Lab 0 Archive For ___ hfDnlhs !ong9( than 1 mcnrt» ilnfl Arcur.d Tit119 Fisqulra" ac Rc(/wcmer.ts (Specify) o 24 Houts 0 4C Hou", 0 7 Days 0 74 Days 0 27 Days C 0fTt1X' as oer methDd :.!:7r.J .. -Io.. ? -" "'"'-.... l (J~ 1.Rt1t:!llv1J!Jay Time 2. 2_R2ce/~ay 2. R~tiirJliJd8y Comments When Complete Email to:DeanorPaui tetco@tetco·ut.com iiiSTRTsuTi()N; wrilTE -Rillufffec/ f':I criltil ....!iI't P..potl' CANAi'lY -$:<lys with 11'", SampllI; FIt« -('"41'" Qr.py SDGNo. 43264 TestAmerlca Order No. rptSTLRchTitle v3.73 TestAmerica Laboratories, Inc. Analytical Data Package Prepared For Denison Mines (USA) Corp. Denison Mine 20112nd Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 19 Pages Report No.: 47442 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID Batch No. ------------.--- --------- 5769 BAGHOUSE FILTER J1 F080456-4 MJ3XW1AA 9MJ3XW10 1161154 & BEAKER 5769 BAGHOUSE FILTER J1F080456-4 MJ3XW1AE 9MJ3XW10 1161156 & BEAKER 5769 BAGHOUSE FILTER J1 F080456-4 & BEAKER 5769 BAGHOUSE FILTER J1 F080456-4 & BEAKER 5770, 5771 R2 NYC FILTERS & BE 5770, 5771 R2 NYC FILTERS & BE 5770, 5771 R2 NYC FILTERS & BE 5770, 5771 R2 NYC FILTERS & BE 5784, 5786 R1 NYC FILTERS & BE 5784, 5786 R1 NYC FILTERS & BE 5784, 5786 R1 NYC FILTERS & BE 5784, 5786 R1 NYC FILTERS & BE J1 F080456-3 J1 F080456-3 J1 F080456-3 J1 F080456-3 J1 F080456-2 J1 F080456-2 J1 F080456-2 J1 F080456-2 5785 R1 GRIZZLY FILTER J1 F080456-1 & BEAKE 5785 R1 GRIZZLY FILTER J1 F080456-1 & BEAKE MJ3XW1AC 9MJ3XW10 1161158 MJ3XW1AD 9MJ3XW10 1161160 MJ3XQ1AA 9MJ3XQ10 1161154 MJ3XQ1AE 9MJ3XQ10 1161156 MJ3XQ1AC 9MJ3XQ10 1161158 MJ3XQ1AD 9MJ3XQ10 1161160 MJ3XM1AA 9MJ3XM10 1161154 MJ3XM1AE 9MJ3XM10 1161156 MJ3XM1AC 9MJ3XM10 1161158 MJ3XM1AD 9MJ3XM10 1161160 MJ3XF1AA 9MJ3XF10 1161154 MJ3XF1AC 9MJ3XF10 1161156 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Certificate of Analysis July 15,2011 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction June 3, 2011 Denison Mine 2011 1st Quarter Four (4) Stack Filter Samples 43264 CASE NARRATIVE On June 3, 2011, four stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J1F080456. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: TestAmerica Laboratories, Inc. Alpha Spectroscopy Thorium-228, -230, -232 by method RL-ALP-001 Uranium-234, -235, -238 by method RL-ALP-004 Gamma Spectroscopy Pb-21O by method RL-GA-001 Alpha Scintillation Radium-226 by method RL-RA-001 2 Denison Mines (USA) Corp July 15,2011 IV. Quality Control The analytical result for each analysis perfonned includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. V. Comments Alpha Spectroscopy Thorium-228, 230, 232 The achieved MDA of the samples exceeds the detection limit. However, in most cases, the activity of the samples exceeds the MDA and detection limit. The data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Uranium-234, 235, 238 The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA and detection limit for three of the four samples. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Gamma Spectroscopy Pb-210 The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. The LCS recovery yield is just above acceptance limits. There is no sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Alpha Scintillation Radium-226 The achieved MDA exceeds the detection limit due to sample volume available for analysis. Sample activity exceeds MDA and detection limit for all of the samples. Data is accepted. Except as noted, the LCS, batch blank and sample results are within acceptance limits. I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan Customer Service Manager TestAmerica Laboratories, Inc. 3 Drinking Water Method Cross References DRINKING WATERASTM METHOD CROSS REFERENCES Referenced Method I sotope(s) TestAmerica Richland's SOP N EPA 901.1 Cs-134,1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 Results in this report relate only to the sample{s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (Ui) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (Sf? n), where S is the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation of the general "Law of Propagation of Errors" equations and specific example are available on request. TestAmerica rptGeneralInfo v3.72 TestAmerica Laboratories, Inc. 4 o. Action Lev Batch Bias COCNo Count Error (#s) Total Vocert (#s) u<_ Combilled Ullcertaillty. (#s), Coverage Factor CRDL(RL) Lc Lot-Sample No MDCJMDA Primary Detector Ratio V-234/V-238 RstlMDC RstlTotUcert Report DB No RER SDG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmerica Re ort Definitions An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by the equation (Result/Expected)-l as defined by ANSI NI3.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, Uc the combined ullcertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width of the confidence interval, I, 2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default" nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 * Sqrt(2*(BkgmdCntlBkgmdCntMin)/SCntMin» * (ConvFctl(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume with a Type I and II error probability of approximately 5%. MDC = (4.65 * Sqrt«BkgmdCnt/BkgmdCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn * Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/u-238 ratio for natural uranium in NIST SRM 432lC is 1.038. Ratio of the Result to the MDC. A value greater than I may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than 1 may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order Number. The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2+ TPUd2)] as defined by ICPT BOA where S is the original sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results are in the same units. The L1MS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. rptGenerallnro v3.72 TestAmerica Laboratories, Inc. 5 Sample Results Summary Date: 1S-Jul-11 TestAmerica Ordered by Method, Batch No., Client Sample ID. Report No. : 47442 SDG No: 43264 Client Id Tracer MOC or Batch Work Order Parameter Result +-Uncertainty ( 25) Qual Units Yield MOA CROL RER2 1161154 RICHRC5011 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AA TH-22B 1.6BE-07 +-4.9E-OB UCI/SA 10B% 1.B4E-OB TH-230 3.B7E-05 +-6.0E-06 UCI/SA 10B% 1.7BE-OB 3.00E-15 TH-232 4.02E-07 +-B.BE-OB UCI/SA 10B% 1.78E-08 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AA TH-228 6.59E-08 +-3.SE-08 UCI/SA 69% 2.8SE-08 TH-230 1.31 E-05 +-2.1 E-06 UCI/SA 69% 2.76E-OB 3.00E-1S TH-232 1.35E-07 +-S.OE-08 UCI/SA 69% 2.76E-08 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AA TH-228 4.14E-08 +-2.8E-08 UCI/SA 68% 2.77E-08 TH-230 1.15E-05 +-1.9E-06 UCI/SA 68% 2.68E-08 3.00E-15 TH-232 1.46E-07 +-5.3E-08 UCI/SA 68% 2.6BE-OB 5785 R1 GRIZZLY FILTER & BEAKE MJ3XF1AA TH-228 3.06E-09 +-2.2E-08 U UCI/SA 64% 4.31E-08 TH-230 6.8SE-07 +-1.4E-07 UCI/SA 64% 3.18E-08 3.00E-15 TH-232 5.61 E-OB +-2.8E-08 UCI/SA 64% 2.17E-08 1161156 FFSR 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AE U-234 8.56E-03 +-2.0E-03 UCI/SA 91% 3.73E-05 9.00E-15 U-235 2.44E-04 +-9.7E-05 UCI/SA 91% 3.16E-05 9.00E-15 U-238 8.32E-03 +-1.9E-03 UCI/SA 91% 4.S3E-05 9.00E-15 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AE U-234 4.75E-02 +-1.0E-02 UCIISA 83% 1.40E-04 9.00E-15 U-235 2.42E-03 +-7.1 E-04 UCI/SA 83% 9.99E-05 9.00E-15 U-238 4.69E-02 +-9.9E-03 UCI/SA 83% 1.45E-04 9.00E-15 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AE U-234 5.65E-02 +-1.3E-02 UCI/SA 76% 2.21E-04 9.00E-15 U-23S 3.37E-03 +-9.7E-04 UCI/SA 76% 1.46E-04 9.00E-15 U-238 5.65E-02 +-1.3E-02 UCI/SA 76% 2.44E-04 9.00E-15 5785 R1 GRIZZLY FILTER & BEAKE MJ3XF1AC U-234 3.32E-OS +-3.8E-OS U UCI/SA 107% 6.71E-05 9.00E-15 U-235 1.41 E-05 +-2.7E-05 U UCI/SA 107% S.72E-05 9.00E-15 U-23B 1.92E-05 +-3.6E-OS U UCI/SA 107% 7.68E-05 9.00E-15 1161160 RICHRC5011 TestAmerica RER2 -Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))l as dermed by ICPT BOA. rptSTLRchSaSum U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/MdalMdl, Total Uncert, CRDL, RDL or mary2 V5.2.15 not identified by gamma scan software. A2002 TestAmerica Laboratories, Inc. 6 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample ID. Report No. : 47442 Client Id Tracer Batch Work Order Parameter Result +-Uncertainty ( 2s) Qual Units Yield 1161160 RICHRC5011 5769 BAGHOUSE FILTER & BEAKER MJ3XW1AD Pb-210 1.66E-06 +-4.8E-07 UCI/SA 69% 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AD Pb-210 4.99E-OS +-B.4E-06 UCI/SA 79% 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AD Pb-210 4.9BE-OS +-B.4E-06 UCI/SA B3% 1161158 RL-RA-001 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AC RA-226 3.91E-07 +-B.9E-OB 100% 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AC RA-226 3.01E-07 +-7.9E-OB 77% 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AC RA-226 2.78E-07 +-7.2E-08 69% No. of Results: 30 TestAmerica rptSTLRchSaSum mary2 V5.2.15 A2002 RER2 -Replicate Error Ratio = (S-D)/(sqrt(sq(TPUs)+sq(TPUd»( as defmed by ICPT BOA. TestAmerica Laboratories, Inc. 7 Date: 15-Jul-11 SDG No: 43264 MDCor MDA CRDL RER2 5.89E-07 6.00E-14 S.15E-07 6.00E-14 4.S9E-07 6.00E-14 2.70E-OB 9.00E-14 6.78E-08 9.00E-14 4.7BE-08 9.00E-14 QC Results Summary Date: 15-Jul-11 TestAmerica Ordered by Method, Batch No, QC Type,. Report No. : 47442 SDG No.: 43264 Batch Tracer LCS Work Order Parameter Result +-Uncertainty ( 2s) Qual Units Yield Recovery Bias MDClMDA RICHRC5011 1161154 BLANK aG, MJ56F1AA TH-228 7.05E-09 +-1.2E-08 U UCI/SA 86% 2.18E-08 TH-230 6.58E-08 +-2.8E-08 UCI/SA 86% 2.11 E-08 TH-232 2.72E-08 +-1.7E-08 UCI/SA 86% 1.67E-08 1161154 LGS, MJ56F1AC TH-230 1.97E-06 +-3AE-07 J UCI/SA 60% 86% -0.1 2.66E-08 FFSR 1161156 BLANK aG, MJ56H1AA U-234 O.OOE+OO +-5.0E-08 U UCI/SA 93% 1.17E-07 U-235 -4.87E-09 +-5.0E-08 U UCI/SA 93% 1.17E-07 U-238 9.73E-08 +-9.9E-08 U UCI/SA 93% 1.17E-07 1161156 LGS, MJ56H1AC U-234 3.37E-06 +-7.9E-07 UCI/SA 89% 93% -0.1 1.21 E-07 U-238 3.88E-06 +-8.7E-07 UCI/SA 89% 102% 0.0 1.21 E-07 RICHRC5011 1161160 BLANK aG, MJ56M1AA Pb-210 3.04E-07 +-3.2E-07 U UCI/SA 76% 5A8E-07 1161160 LGS, MJ56M2AC Pb-210 1.15E-05 +-2.0E-06 UCI/SA 79% 127% 0.3 4.63E-07 RL-RA-001 1161158 BLANK aG, MJ56J1AA RA-226 1.32E-08 +-2.8E-08 U 83% 4.74E-08 1161158 LGS, MJ56J1AC RA-226 9.07E-06 +-2.1E-06 J 100% 91% -0.1 4.18E-08 No. of Results: 13 Bias -(ResultlExpected)-l as defined by ANSI N13.30. TestAmerica rptSTLRchQcSum mary V5.2.15 A2002 J Qual-No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 8 FORM I Date: 15-J ul-11 SAMPLE RESUL TS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/27/2011 8:00:00 AM Lot-Sample No.: J1 F080456-4 Report No.: 47442 Received Date: 6/3/2011 11 :00:00 AM Client Sample 10: 5769 BAGHOUSE FILTER & BEAKER COC No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered b~ Client Sample 10, Batch No. Result Count Total MDCIMDA, Rpt Unit, Yield RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert Prep Date Size Size Detector Batch: 1161154 RtCHRC5011 Work Order: MJ3XW1AA Report DB ID: 9MJ3XW10 TH-228 1.68E-07 4.2E-OB 4.9E-OB 1.B4E-OB UCI/SA 10B% (9.1) 6/27/11 10:47 p 1.0 0.99001 ALP175 5.B2E-09 (6.8) Sample Sample TH-230 3.B7E-OS 6.1 E-07 6.0E-06 1.7BE-OB UCI/SA 10B% (2169.7) 6/27/11 10:47 p 1.0 0.99001 ALP175 5.64E-09 3.00E-15 (12.8) Sample Sample TH-232 4.02E-07 6.3E-OB B.BE-OB 1.7BE-OB UCI/SA 10B% (22.6) 6/27/11 10:47 p 1.0 0.99001 ALP175 5.64E-09 (9.1) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XW1AE Report DB ID: 9MJ3XW10 U-234 8.S6E-03 4.BE-04 2.0E-03 3.73E-05 UCI/SA 91% (229.6) 6/16/11 06:37 p 1.0 0.00103 ALP7 9.71 E-06 9.00E-15 (8.8) Sample Sample U-235 2.44E-04 8.0E-05 9.7E-05 3.16E-05 UCI/SA 91% (7.7) 6/16/11 06:37 p 1.0 0.00103 ALP7 6.B7E-06 9.00E-15 (5.) Sample Sample U-238 8.32E-03 4.7E-04 1.9E-03 4.53E-05 UCI/SA 91% (183.4) 6/16/11 06:37 p 1.0 0.00103 ALP7 1.37E-05 9.00E-15 (8.8) Sample Sample Ratio U-234/238 = 1.0 Batch: 1161158 RL-RA-001 Work Order: MJ3XW1AC Report DB ID: 9MJ3XW10 RA-226 3.91 E-07 4.0E-OB B.9E-OB 2.70E-08 100% (14.5) 7/7/11 05:32 p 1.0 0.99 ASCJMB 1.23E-OB 9.00E-14 (8.8) Sample Sample Batch: 1161160 RICHRC5011 Work Order: MJ3XW1AD Report DB 10: 9MJ3XW10 Pb-21 0 1.66E-06 3.9E-07 4.BE-07 5.B9E-07 UCI/SA 69% (2.8) 7/7/11 06:3B a 1.0 0.99001 GPC31D 2.B7E-07 6.00E-14 (6.9) Sample Sample TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/MdalMdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 9 Lab Name: TestAmerica Lot-Sample No.: J1 F080456-4 FORM I SAMPLE RESULTS Client Sample ID: 5769 BAGHOUSE FILTER & BEAKER Denison Mine 2011 2nd Quarter SDG: 43264 Report No.: 47442 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield RstIMDC, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert No. of Results: 8 Comments: Date: 15-J ul-11 Collection Date: 5/27/2011 8:00:00 AM Received Date: 6/3/2011 11 :00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample 10. Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit. RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 10 FORM I Date: 15-J ul-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/26/2011 8:00:00 AM Lot-Sample No.: J1F080456-3 Report No.: 47442 Received Date: 6/3/2011 11 :00:00 AM Client Sample ID: 5770, 5771 R2 NYC FILTERS & BE cac No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered bl Client Sample ID. Batch No. Result Count Total MDClMDA, Rpt Unit, Yield RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XQ1AA Report DB ID: 9MJ3XQ10 TH-228 6.59E-OB 3.3E-OB 3.5E-OB 2.B5E-OB UCI/SA 69% (2.3) 6/27/1110:47p 1.0 0.98995 ALP174 9.02E-09 (3.8) Sample Sample TH-230 1.31E-05 4.4E-07 2.1 E-06 2.76E-OB UCI/SA 69% (472.4) 6/27/1110:47 P 1.0 0.98995 ALP174 B.73E-09 3.00E-15 (12.4) Sample Sample TH-232 1.35E-07 4.6E-08 5.0E-OB 2.76E-08 UCI/SA 69% (4.9) 6/27/11 10:47 p 1.0 0.98995 ALP174 8.73E-09 (5.4) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XQ1AE Report DB ID: 9MJ3XQ10 U-234 4.75E-02 2.2E-03 1.0E-02 1.40E-04 UCI/SA 83% (338.8) 6/16/11 05:21 p 1.0 0.00101 ALP5 3.40E-05 9.00E-15 (9.5) Sample Sample U-235 2.42E-03 5.1 E-04 7.1 E-04 9.99E-05 UCI/SA B3% (24.3) 6/16/11 05:21 p 1.0 0.00101 ALP5 1.39E-05 9.00E-15 (6.8) Sample Sample U-238 4.69E-02 2.2E-03 9.9E-03 1.45E-04 UCI/SA B3% (322.7) 6/16/11 05:21 p 1.0 0.00101 ALP5 3.67E-05 9.00E-15 (9.5) Sample Sample Ratio U-234/238 = 1.0 Batch: 1161158 RL-RA-001 Work Order: MJ3XQ1AC Report DB ID: 9MJ3XQ10 RA-226 3.01E-07 5.4E-08 7.9E-OB 6.7BE-OB 77% (4.4) 7/7/11 05:31 p 1.0 0.99 ASC2HA 3.24E-08 9.00E-14 (7.6) Sample Sample Batch: 1161160 RICHRC5011 Work Order: MJ3XQ1AD Report DB ID: 9MJ3XQ10 Pb-21 0 4.99E-05 1.0E-06 B.4E-06 5.15E-07 UCI/SA 79% (96.9) 7/7/11 06:38 a 1.0 0.98995 GPC31C 2.51 E-07 6.00E-14 (11.9) Sample Sample TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 11 Lab Name: TestAmerica Lot-Sample No.: J1 F080456-3 FORM I SAMPLE RESULTS Client Sample 10: 5770,5771 R2 NYC FILTERS & BE Denison Mine 2011 2nd Quarter SDG: 43264 Report No.: 47442 cac No.: Result Count Total MDCIMDA, Rpt Unit, Yield RstlMDC, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert No. of Results: 8 Comments: Date: 15-Jul-11 Collection Date: 5/26/2011 8:00:00 AM Received Date: 6/3/2011 11 :00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample ID, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 12 FORM I Date: 15-Jul-11 SAMPLE RESUL TS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/25/2011 8:00:00 AM Lot-Sample No.: J1 F080456-2 Report No.: 47442 Received Date: 6/3/2011 11 :00:00 AM Client Sample 10: 5784, 5786 R1 NYC FILTERS & BE cac No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered by Client Sample 10, Batch No. Result Count Total MDClMDA, Rpt Unit, Yield RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XM1AA Report DB ID: 9MJ3XM10 TH-228 4.14E-OB 2.7E-OB 2.BE-OB 2.77E-OB UCI/SA 6B% (1.5) 6/27/11 10:47 p 1.0 0.99003 ALP173 B.76E-09 (3.) Sample Sample TH-230 1.1SE-OS 4.1 E-07 1.9E-06 2.6BE-OB UCI/SA 6B% (42B.3) 6/27/11 10:47 p 1.0 0.99003 ALP173 B.4BE-09 3.00E-15 (12.4) Sample Sample TH-232 1.46E-07 4.7E-OB 5.3E-OB 2.6BE-OB UCI/SA 6B% (5.4) 6/27/11 10:47 P 1.0 0.99003 ALP173 B.4BE-09 (5.6) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XM1AE Report DB ID: 9MJ3XM10 U-234 S.6SE-02 2.6E-03 1.3E-02 2.21 E-04 UCI/SA 76% (256.3) 6/16/11 05:21 p 1.0 0.00104 ALP4 6.91E-05 9.00E-15 (9.) Sample Sample U-235 3.37E-03 6.4E-04 9.7E-04 1.46E-04 UCI/SA 76% (23.1) 6/16/11 05:21 p 1.0 0.00104 ALP4 3.17E-05 9.00E-15 (6.9) Sample Sample U-238 S.6SE-02 2.6E-03 1.3E-02 2.44E-04 UCI/SA 76% (231.B) 6/16/11 05:21 p 1.0 0.00104 ALP4 B.OBE-05 9.00E-15 (9.) Sample Sample Ratio U-2341238 = 1.0 Batch: 1161158 RL-RA-001 Work Order: MJ3XM1AC Report DB ID: 9MJ3XM10 RA-226 2.7BE-07 4.6E-OB 7.2E-OB 4.7BE-OB 69% (5. B) 7/7/11 05:34 p 1.0 0.99 ASC1MB 2.22E-OB 9.00E-14 (7. B) Sample Sample Batch: 1161160 RICHRC5011 Work Order: MJ3XM1AD Report DB ID: 9MJ3XM10 Pb-21 0 4.98E-OS 1.0E-06 B.4E-06 4.59E-07 UCI/SA B3% (10B.6) 7/7/11 06:3B a 1.0 0.99003 GPC31B 2.23E-07 6.00E-14 (11.9) Sample Sample TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 13 Lab Name: TestAmerica Lot-Sample No.: J1 F080456-2 FORM I SAMPLE RESULTS Client Sample 10: 5784, 5786 R1 NYC FILTERS & BE Denison Mine 2011 2nd Quarter SDG: 43264 Report No. : 47442 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield RstlMDC, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstlTotUcert No. of Results: 8 Comments: Date: 15-Jul-11 Collection Date: 5/25/2011 8:00:00 AM Received Date: 6/3/2011 11 :00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample ID. Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been aSSigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/MdalMdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 14 FORM I Date: 15-Jul-11 SAMPLE RESUL TS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/24/2011 8:00:00 AM Lot-Sample No.: J1 F080456-1 Report No.: 47442 Received Date: 6/3/2011 11 :00:00 AM Client Sample ID: 5785 R1 GRIZZLY FILTER & BEAKE cac No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered bl Client Sample 10, Batch No. Result Count Total MDCIMDA, Rpt Unit, Yield RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XF1AA Report DB 10: 9MJ3XF10 TH-228 3.06E-09 U 2.2E-OB 2.2E-OB 4.31 E-OB UCI/SA 64% 0.07 6/27/11 10:47 p 1.0 0.98932 ALP171 1.74E-OB 0.28 Sample Sample TH-230 6.SSE-07 9.1 E-OB 1.4E-07 3.1BE-OB UCIISA 64% (21.6) 6/27/11 10:47 P 1.0 0.98932 ALP171 1.19E-OB 3.00E-15 (9.8) Sample Sample TH-232 S.61E-OS 2.7E-OB 2.BE-OB 2.17E-OB UCIISA 64% (2.6) 6/27/11 10:47 p 1.0 0.98932 ALP171 6.B7E-09 (4.) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XF1AC Report DB ID: 9MJ3XF10 U-234 3.32E-OS U 3.7E-05 3.BE-05 6.71 E-05 UCIISA 107% 0.5 6/16/11 06:36 p 1.0 0.00095 ALP3 2.49E-05 9.00E-15 (1.8) Sample Sample U-235 1.41 E-OS U 2.7E-05 2.7E-05 5.72E-05 UCIISA 107% 0.25 6/16/11 06:36 p 1.0 0.00095 ALP3 2.00E-05 9.00E-15 (1.) Sample Sample U-238 1.92E-OS U 3.6E-05 3.6E-05 7.6BE-05 UCIISA 107% 0.25 6/16/11 06:36 p 1.0 0.00095 ALP3 2.97E-05 9.00E-i5 (1.1) Sample Sample Ratio U-2341238 = 1.7 No. of Results: 6 Comments: TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, ROL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 15 FORM II Date: 15-Jul-11 BLANK RESUL TS Lab Name: TestAmerica SDG: 43264 Matrix: AIR Report No.: 47442 Count Total MDCIMDA, Rpt Unit, RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield RstITotUcert Prep Date Size Size Detector Batch: 1161160 RICHRC5011 Work Order: MJ56M1AA Report DB 10: MJ56M1AB Pb-21 0 3.04E-07 U 3.2E-07 3.2E-07 5ABE-07 UCI/SA 76% 0.56 7/7/11 06:3B a 1.0 1.0 GPC32A 2.67E-07 6.00E-14 (1 .9) Sample Sample --------Batch: 1161158 RL-RA-001 Work Order: MJ56J1AA Report DB 10: MJ56J1AB RA-226 1.32E-OB U 2.BE-OB 2.BE-OB 4.74E-OB B3% 0.2B 7/7/11 05:31 p 1.0 1.0 ASCKMF 2.23E-OB 9.00E-14 0.94 Sample Sample Batch: 1161156 FFSR Work Order: MJ56H1AA Report DB 10: MJ56H1AB U-234 O.OOE+OO U O.OE+OO 5.0E-OB 1.17E-07 UCI/SA 93% O. 6/16/11 06:3B p 1.0 0.25 ALP9 2.53E-08 9.00E-15 O. Sample Sample U-235 -4.B7E-09 U 5.0E-OB 5.0E-OB 1.17E-07 UCI/SA 93% -0.04 6/16/11 06:3B p 1.0 0.25 ALP9 2.53E-OB 9.00E-15 -0.2 Sample Sample U-238 9.73E-OB U 9.BE-OB 9.9E-OB 1.17E-07 UCI/SA 93% 0.B4 6/16/11 06:38 p 1.0 0.25 ALP9 2.53E-OB 9.00E-15 (2 .) Sample Sample Batch: 1161154 RICHRC5011 Work Order: MJ56F1AA Report DB 10: MJ56F1AB TH-228 7.05E-09 U 1.2E-OB 1.2E-08 2.1BE-OB UCI/SA 86% 0.32 6/27/1110:47p 1.0 1.0 ALP176 7.73E-09 (1 .1 ) Sample Sample TH-230 6.5BE-OB 2.6E-OB 2.8E-OB 2.11 E-OB UCI/SA 86% (3.1 ) 6/27/11 10:47 p 1.0 1.0 ALP176 7 A 7E-09 3.00E-15 (4.7) Sample Sample TH-232 2.72E-OB 1.7E-OB 1.7E-OB 1.67E-OB UCI/SA B6% (1 .6) 6/27/11 10:47 p 1.0 1.0 ALP176 5.2BE-09 (3.1 ) Sample Sample No. of Results: 8 Comments: TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBlank V5.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/MdI, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 16 Lab Name: TestAmerica Matrix: AIR Count Parameter Result Qual Error ( 2 s) Batch: 1161160 RICHRC5011 Pb-21 0 1.15E-05 5.4E-07 Batch: 1161158 RL-RA-001 RA-226 9.07E-06 1.7E-07 Batch: 1161156 FFSR U-234 3.37E-06 5.BE-07 U-238 3.8BE-06 6.3E-07 Batch: 1161154 RICHRC5011 TH-230 1.97E-06 1.5E-07 No. of Results: 5 Comments: FORM II LCS RESULTS Total Report Expected Uncert(2 s) MDC(MDA Unit Yield Expected Uncert Work Order: MJ56M2AC Report DB 10: MJ56M2CS 2.0E-06 4.63E-07 UCI/SA 79% 9.07E-06 1.52E-07 Rec Limits: 20 115 Work Order: MJ56J1AC Report DB 10: MJ56J1CS 2.1 E-06 4.1BE-OB 100% 9.95E-06 1.01 E-07 Rec Limits: 70 130 Work Order: MJ56H1AC Report DB 10: MJ56H1CS 7.9E-07 1.21 E-07 UCI/SA 89% 3.64E-06 1.13E-07 Rec Limits: 70 130 B.7E-07 1.21 E-07 UCI/SA B9% 3.B1 E-06 1.1BE-07 Rec Limits: 70 130 Work Order: MJ56F1AC Report DB 10: MJ56F1CS 3.4E-07 2.66E-OB UCI/SA 60% 2.2BE-06 4.63E-OB Rec Limits: 70 130 TestAmerica rptSTLRchLcs V5.2.15 A2002 Bias -(ResultlExpected)-1 as defined by ANSI N13.30. TestAmerica Laboratories, Inc. 17 Date: 15-Jul-11 SDG: 43264 Report No.: 47442 Recovery, Analysis, Aliquot Primary Bias Prep Date Size Detector 127% 7/B/11 07:51 a 1.0 GPC31B 0.3 Sample 91% 717/11 05:32 p 1.0 ASCPMD -0.1 Sample 93% 6/16/11 06:38 p 0.27 ALP10 -0.1 Sample 102% 6/16/11 06:38 p 0.27 ALP10 0.0 Sample B6% 6/27/11 10:47 p 1.0 ALP177 -0.1 Sample -l et ~ 3 et ::!. (") PO j r l r::r o a o ::l. et S" :::l r> 00 w • :. ~ ~=-~ .' ... -. .~ ...... Chain of Custody Record TAL-4124(1otm TemDeratlire on Receipt __ _ TestAmerica Drin.'<ing Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING GReBr ?ro{!;Ci Men.11..Q:eT Dl1:& Ch6in af Cus!cd\' I)[urrbe!. Tetco Dean Kitchen . 5/31/2011 I I Address -,oi6Qhon9 Numt>er ,Area CoCG)J.=a~ Num':xu LIlb Numb£:!' 391 East 620 South 1801-4$2-9106 .. ~ Page of CiIJl • . -,stare IZID Cope _ Site eor;r= ~ Lab ConIac:! AP.aJysis (Al1aCh lisJ if Amerrcan Fork .Ut L 84003 ~ SoottCh,"t.nsen,Ry<I"Palme, ~~SPaC$lsneeded) P(oi~ct N&71e /!I1d ~on fS/zfu1 CarTier,Wayblll Number I I Denison Mine 2011 2nd Quarter ._. _ .~ I ~pecj<:, lnstf'.1ction~/ Ccnrm~PurcllosC Or.iaJtQuo:c No. , . i.iontamers if i 0 1 Lonamons ot ReceIpt MEl.flX Preservatfv'es ~ _ 0 I ~ ;j ---" " '<' I ~ ~ "! -0 Sample !.D. No. and DesCription Date ! Time ~. _ e @ 8 _ ~ ~~ ::. 1-, ~ ~ (conralnelS for each sampl9 may tis combined on ong (ffIfI) j ~ ~ ~ ~ ~ ~ ~ i! '" tli<: 5785 R1 Grizzly filter and beaker -. S/24/11 ..f 8:00 . X I I X 'fel , ! /VlJ3 >( f 5784,5786 R1 NYCfilters;nd beaker . ~ y~5/i.1 _ c ·t~~~ ., X: i 'N 1. I ~'X 1--I I L"VlI:\XAIl 5770, 5771. ~2 NYC filters and b!aker. _ j 5/26/11 &:00 X I 1 'l\ f.: X ,x ! /\~ Q 5769 Sagh~-u5e Filter and beaker -5i27/11 ~ r 8:00 -. X! I I J\ ~"1:J 'A,: I I ! /1/1 J ,;Z"x \IV -I .j ; I I I' r 'I .... ["-t-[! I 1 I ! (~~! Gr1JL;~' 1111111111111111111111111111111 +-+-f----1ii--l--i-i---l-+-+--+-I-+--+-+------ LOt di-'j-IPOroL1~ J1 F080456 , ! lQ ..':()f1{1'! '=tllolJl 1 I bM~J)FAJ I I I I I poiSolilii Fiez:ord IderJilitiation o Non-H3zarrJ 0 Flammable 0 Skin Irriltmt I SSm,P:e O/SposeJ o Polson 9 . 0 Unknown ! 0 Retum To Client fA fee may be assessed if ssmpleillue retllined o Disposal By Lab 0 Archive Far ___ Marrlhs longer thm 1 month) 111m AtrJvnd 'me Rsquired ac D~ulremM/s(Siiei;7Yj o 24 Hours 0 48 Hours 0 7 Days 0 14 Oays 0 21 Days I T""e /I cr0 2. (umt 3. RiJiirquisheiJ8j ~mm""lS When Complete Email to:DeanorPaultetco@tetco-ut.com 5!~TRIBUTJON: WHITE ~ Re!urned t:> C!1tffl1 Iv'.fh P.e;»rt c::MV;RY -S;aofl ,·:tll 1IIe SJJJr~ PINK ~ AiildCapy TestAmerica £.l:iirt8i-iWi;~"""~ 7HE L:ADER IN C:1'.NIR.ONM~NTAl T'CSTING Sample Check-in List Date/TUne Received: b 13j It ~,IL.=.()-""""o--GM Screen Result (out) --!....:/,U--,bl----(in)-~--'r"'.,.---InitialsffL Client; [)c"'iSoV1 SDG #: Lj :S./&L\ NA [] SAl' ~:, ___ . _____ ~A [J V..-ork Order Number: ..) I FC>6Ql..lG7R Chain of Custody "# ______________ _ Sbippi.r'.g Container ID',, ____________ ~.;, th-il' Bill i= ____________ . ____ --'~A t*_l l:em 1 through 5 for sbipping ::omaine:-only. :t:,i~i2.! appro;l1i2.te response, CUSlOCY Se,js on shipping coutziner :ma:.t? Yes [ }\'o [ ~ ~o Custody Seal ~ CuslOdy Seals G.arcd and sign"d? Yes [ No l ] ~o Custody sea~ Chzin of CuslOdy record present? _ Yes ~o [ ] Coole: teillperarure: ____ ">\A [~~-5 \'e;-:niculne'packiJ!g mate:-;c.!s is ~A [ -,j,,'et [ J Dry f+-i.--- 1. 3, 4. Item 6 Through 10 for samples, biTiz.l appropriaTe response. 6. ~umber of samples in shipping container (Each sample rmy comain multiple bottles): Y-fi) I beCLkf4..fkj I b (lt6 7. Sample holding times exceeded? NA [ ] Yes [ ] No [/-j-f..--' 8. 9, Samples have: tape == custody seals ~ e'-in good condition are broken ~h~ardlabe~ ~appIOpriate sample labels __ are leaking __ have air bubbles (Only for samples requiring no head space) 10. Sample pH appropriate for analysis requested Yes [ ] No [ ] N/A}J r l [,Note discrepancies in #13) (If acidification necessary, then document sample ID, initial pH, ~'~fHN03 added and pH after addition) RPL ID # of preservative used :. ______________________________ _ 11. ,Sample Location, Sample Collector Listed? * *For documentation only, No corrective action needed. 12, Were any anomalies identified in sample receipt? Yes [ ] No ~.~V-' 13. Description of anomalies (include sample numbers): NA [ ], _____________________ _ ~ ( See other side for ad,~itional comment~ sample Custodian~ ~ __ / L1~~ Date:+:A.-SLHI--I6[l:-l--[ ___ _ Cllent Informed on by Person contacted. _________ _ [~ No act] on necessarYi process as is Project Manager 2< &£.. 0 kJr;tok: Date._~~!q~/!:.....!.II ____ _ LS-023, Rev. 12, 10/10 TestAmerica Laboratories, Inc. 19 APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Grizzly Baghouse Figure 3. Facility Schematic Representation Production and Control Equipment Data NOIth Yellow Cake (Scrubber Flow Rate(s) Yellow Cake Dryer Baghouse (8 baITels filled during test) Grizzly (tpb of material and belt speed) D F.oility. Denison Mines t a 1 y Stack Identification: North Yellow Cake Scrubber 1+-0 .... 1 , , ~ a: Distance upstream from next disturbance, feet ---- ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet ____ _ Estimated Moisture, percent Estimated Temperature, "F ____ _ Estimated Velocity, [pm Control Unit Type: Scrubber Number of Ports Figure 1. Facility Schematic Representation Process Type: Yellow Cake Processing Facility: Denison Mines t ex y Stack Identification: Yellow Cake Dryer Baghouse ex: Distance upstream from next disturbance, inches 5~ ----- 13: Distance downstream from last disturbance, inches 45 y: Distance of Sample Level to Ground, feet 6: 0: Stack Inside Diameter, inches H Estimated Moisture, percent O-~ 1~ Estimated Temperature, of ----- Estimated Velocity, fPm ___ ..... 1 ,"-4 Control Unit Type: Baghouse Number of Ports 2 Figure 2. Facility Schematic Representati, Facility. Denison Mines t ex ! y Stack Identification: Grizzly Baghouse ex: Distance upstream from next disturbance, inches 24. ----- ~: Distance downstream from last disturbance, inches 4~ 2: y: Distance of Sample Level to Ground, feet ____ _ 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, of Estimated Velocity, fpm Control Unit Type: Baghouse Number of Ports 18.' ---- 1 ~ Amt ----- 7~ ----- 2 Figure 3. Facility Schematic Representatil Denison Mine Process Data Source: North Yellow Cake Date: SI2)/!~ Scrubber Flow GPM Time #1 #2 ~P 8: l S" 4,Q IL,o 1rO \3: L\) q,'O ,t,'T '3,0 '1:LC ~,6 10, :;r-:",-0 <:\")0 1, ") 111 L-3,0 lo:'2...u c 11\:} \Lo J,O 10',)'0 9, E \'2., D J,0 \ \',1.0 \0,0 \L,D 3,0 \ l', :)0 10, l n_,L ~,O t)..', 3-D 10 ' \ \21L 31 0 1~(oO 9,1 \(,1 S,O \3:30 to'l 1'2, L J,o L,-\', 00 10, \ 17.., [...-S,O Jt.U JD 9." Il,o ),0 If: 00 cr I\?) \ t, 9 ),0 \).'30 '\,'] IL,I 3 d ii;,~ \ (g: or> 913 \ 1,1..-"3,0 Denison Mines Process Data Source: North Yellow Cake Date: JIVI c;. '1 ;;L~ / Z 0 / I Scrubber Flow GPM Time #1 #2 t,p g ~o)' /6. ! '2,Z-L. '1 S:3S /& ,0 12. ( LJ=r- '--) 'v <' ", , 'O,D I ~. f l I '-r ';:3 ) '1, (p l !.) Z·1 /1' . ()~' .J, l' ( • -(7 ! I . 7-l·i J()!~·s ~,9 t 7_. / "2, '"Jr //.'0S" q.7-I/, 7-Z,9 .5 ~\V t-O OUc\ (\ I .~ I or t6,--l \ 0 ('), rs,O ~) 10'\ ~.-J I 5 . ->, r:; • --1 -,>--" o --1 Of 10, ~3 5,{ I c/' :)0 '1,3 //,(J "l, (.1 It:o() ~(.? /5,0 3.0 11 :30 1, I J~. z.. Z·cr /&: ~o 1..7-(1;, 1) 5.0 I 8 ~ ~t) 9·fR /'Z-.-z. 7·cr )9.' Ob ~.~ /'3.2.-"3.0 Iq ~30 q.[ /;.-0 2-. '1 'Lo',oo 'f.~ I~ ,-z, ~_o 10 ',~t q.J l ~, ( L~'t Denison Mines Process Data Source: Grizzly BaQhouse Date: mt:kt ~f./ 201/ Time ro V1 .> TPII r: PYVl. :t;so lrg99S-t~S 101·3 9;2-3 It9ot.(S" /30 /69'b 8:~O 191090 /35"' /ocr.&? ("1: lO 11-9/4-S 3>30 /6?~ <:'1' -0 o ,) (:rcf ?pO 115--/ oC;, t- 1(J~J('lo t :;-:12 L/O I (),~~ /07 l /0 :60 /19 2-'6 D [/,;-lo,(,S-' II : 2-0 (7c; 3l~-/00 1073 II . so 1}9 Yf5 &D ) 69. (p 12', ?.,[J I Fll/Z s /20 /0;: .:;,-- I'l-:SV (11 cl1-0 1-/,0 c, I /0 (, . 13 ~ 20 (+'7 SOD 1S /00.(,(( I:~ '.SD frY S'-S-O ;1-./0 / () ? ~-- I ~ '.2.:0 17?59'o 5-.s~ 10°((0 It.t :50 (J-CJ (/.1&5 (/.I () 10 (1-(0 IS-·,7.-D I1-Cft1 1S go /()'i 1 IS-:SD {1-'1930 I 40 / (Y-f, f APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 51114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-te t Dry Gas Meter Calibration Data Fonus Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E Temperature Sensor + ~ Probe ~ Type S Pitot Tube Temperature Temperature Sensor lC11Jinger Train Qltional. May Be Replaced Bi !vi Equivalent Condenser I Temperature Sensor Nozzle t-B:tTrcred sensor~ Gooseneck I 1--- - -~pj;:;'g;~ - - -- ~ Ga;s.jirej / Atile ---,. / Type S Pitot Tube ~ Stack Wall Glass Filter Holder Manometer Temperature Water Sensors Orifice Dry Gas Meter Empty Silica Gel Air-Tight Pump Figure 4 Schematic of Method 5/114 Sampling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ ~ 9 -.... °"*1 -1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN celis, YELLOW celis are calculated. METER SERIAL w:11522588 I CRITICAL ORIFICE SET SERIAL #: 14535 EQUIPMENT 10 #: K' ( TESTED .-------,---~I FACTOR I VACUUM G G G RUN# I (AVGl 0.8137 2 0.8137 3 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 (In Hgl 13 13 13 13 13 13 13 13 13 896.006 901.301 906.609 912.40 917.596 922.809 928.304 933.524 938.841 USING THE CRITICAl ORIFICES AS CALIBRATION STANDARDS: 901.301 906.609 911.936 917.596 922.809 928.018 933.524 938.841 944.055 __ 5.295 5.308 5.327 5.196 5.213 5.209 5.220 5.317 5.214 74 74 74 76 74 79 74 79 74 80 74 82 74 82 14 81 74 83 76 70 79 70 SO 72 80 75 82 74 83 77 83 78 83 79 84 80 Facility New Calibration 2011 FINAL AVG (P .. ,) 25.30 25.3 IF Y VARIATION EXCEEDS 2.000/. ORIFICE SHOULD BE RECALIBRATED ELAPSED I 1 D:l AVG ITIM~MINll B 70 72 73 72.5 § § 4.4778 ~ ~ 74.25 .5.00 2.90 !llil ~ ~ 76.00 5.00 2.90 ~ ~ ~ 82 77 78 AVG: 0.996 ~ 79.00 § 1.20 4.3198 4.3672 !,ill 78.25 7.50 1.20 ~ 4.3672 ~ 80.00 7.50 1,20 ~ ~ !!lli! AVG: 1.009 0.48 79 80 80 80.50 12.00 § 4.3182 ~ ~ 80.75 12.25 0.44 ~ ~ 1.009 81.75 12,00 0.44 4.3032 ~ 1.010 AVG = 12!!l! !ill The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical orifice, V,,(std), and the DGM calibration factor, Y. These equations ace automatically calculated in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.004 1 (1) (2) (3) Vm(."d) = K, • Vm' Pbar+(tJ.fIl 13.6) Tnr Pbar * El Vcr(.,oj) = K' • .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17.64 'R/in. Hg (English), 0.3858 'K1mm Hg (Metric) Tm = Absolute DGM avg. temperature (OR -English, OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb = Absolute ambient temperature (OR -English, OK -Metric) K' = Average K' factor from Critical Orifice Calibration Vcr{Jlld) y = -= DGM calibration factor Vm(s/d) Pre Calibration 2008 AVERAGE AH@=I 1.649 AH@ = (0.759)2 AH (Vm(std)\ Vc,(std) Vm J T em perature Sensors Reference In Out OF 34 67 202 OF 34 67 202 OF 35 67 204 !ill 1.Zll ~ !:!M ~ l:.§g ~ 1.560 1.557 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 1iS----.. 421 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL II:~ CRITICAL ORIFICE SET SERIAL 11;~ EQUIPMENT 10 II: K' TESTED I FACTOR I VACUUM I RUN # (AVG) (I" HgI o o G 2 2 3 2 3 0.8137 12 0.8137 12 0.8137 12 0.5317 13 0.5317 13 0.5317 13 0.3307 13 0.3307 13 0.3307 ~ 155.004 161.521 168.043 136.700 142.672 148.297 116.20 125.809 131.075 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 161.521 168.043 174.568 142.672 148.297 153.926 125.809 131.075 136.357 6.517 6.522 6.525 5.972 5.625 5.629 9.609 5.266 5.282 74 82 74 83 74 83 74 81 74 80 74 81 74 76 74 78 74 80 83 89 93 83 93 96 83 96 99 80 84 86 81 86 88 82 88 89 78 77 80 80 80 81 81 81 84 FINAL AVG(P ... ,) 25.10 25.10 1 I ELAPSED DGM ITIME~MIN) AVG 86.75 6.00 § 88.75 6.00 2.55 90.25 6.00 2.55 82.75 § 1.11 83.75 8.00 1.11 85.00 8.00 1.11 77.75 22.00 ~ 79.75 12.00 0.40 81.50 12.00 0.40 ~ 5.3046 5.2926 ~ ~ 4.5905 7.9255 ~ ~ 2011 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ! ~ g"m ~ 1.000 ~ 1.002 AVG= ~ -0.09 ~ 1.004 !&ill ~ ~ 1.l!l!I AVG= ~ 0.47 7.9047 g"m 4.3117 0.996 4.3117 !!J!l!l AVG= g"m :Y!! ~ ~ 1.489 1.532 1.ill 1.526 !,ill, 1.432 1.428 The following equations are used to calculate the slandard volumes of air passed through the DGM, V m (sid), and the critical orifICe, Va (std), and the DGM calibration factor, Y These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1,001 (1) (2) (3) Vm("'d) = K) • Vm * Pba,.+ (DoH 113.6) Till Pbar * e Vcr .. "d) = K' • .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17.64 °Rl1n. Hg (English). 0.3858 °Klmm Hg (Metric) T m = Absolute DGM avg. temperature (OR -English, OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T ~b = Absolute ambient temperature (OR -English, OK -Metric) K' = Average K' factor from Critical Orifice Calibration VCY(.YIJ) y= --= DGM calibration factor Vm(SIJ) AVERAGE AIi@=(-1.4as:] AH@= (0.759)2 Ali (Vm(std)) V,,(std) Vm Temperature Sensors Reference In Out OF 32 72 203 OF 32 73 201 OF 32 73 202 Pre 2011 5 console METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meier which bracket the expected operating range. E YffiMf'iiW.iWF ---~~~ .. ~ .;:1I!f!--~-' i)1~~ ~.'-'" I· 2) Record barometric pressure belore end after calibration procedure. 3) Run at tesled vacuum (from Orilice Calibration Report), for a period 01 time necessary to achieve a minimum lotal volume of 5 cubic feet 4) Record data and informalion In the GREEN cells, YELLOW cells are calculaled METER SERIAL #:t-===--<j OATE~~ METER PART /I:~ CRITICAL ORIFICE SET SERIAL #,1 1453S EQUIPMENT 10 #: K' TESTED FACTOR I VACUUM RUN # (AVG) (InHa) 0.5:117 13 0.5317 13 0.5317 11 53.103 6.2.664 62.554 71.213 71.213 78.444 9.551 8.559 7.231 69 67 69 72 69 75 72 7Z 75 75 7& 80 78 8D 81 G' D:rn§ D:rn§ .0 .0 .0 .0 .0 .0 1-'-1 I I I I I II II USING THE CRITICAL ORIFICES AS CALIBRAnON STANDARDS: f FaCility FINAL 25.20 ELAPSED 0:l TIME (MIN) AVG e 71.5Q 14.00 7S.5D 12.50 79.00 10.50 0.00 § 0.00 0.00 0.00 § 0.00 0.00 AVG(P""J 25.20 1.10 1.10 1.10 § § DENNISON MINES 8.0184 71319 '.&eS2 IF Y VARIATION EXCEEDS 2.0~, ORIFICE SHOULD BE RECALIBRATED 1 B.1581 1.017 7.2841 1m 6,1187 1J!ll AVG= 1m M!! AVG3 AVG= The !ollc'tloing aQuations are liSa,j to calculate the standard volumes of air passed thiDUgt; u';~ DGM. V If: (stdl. and the critical QlifiCe, V:3 (51d), and the DGM calibration faclDr. Y These equations are automatically calcula1ad in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y =1 1.020 (1) (2) (3) Vm'."d.' = K, .Vm* Pbar+(!1H 1J3.6) Tm Pbar .0 VC'\.1 .... ' ::::; K''''' .JTamb = Net volume of gas sample passed It1rough DGM, corrected to standard conditions K, = 17 64 'R~n Hg (English), 0 3B5S 'Klmm Hg (MetriC) T m ;;; Absolule DGM avg temperature (OR -English, OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T~rb= Absolute ambient temperature l=R -Engllsh,;1K -MetriC) K' = Average K' ~actor from CritIcal OrifICe Caflbration V'C'(JI'" y----= DGM calibration fector -VmiJl.I: Pre Calibration 2008 AVERAGE ~He =1 1.519 2 ~Hd!! = (0.75 e) AH (Vmlstd») V"lsld) Vm !,H9. 1£!l. ~ METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 CUbic feet. 4) Record data and information in the GREEN cells. YELLOW cells are calculated. METER SERJAL 1t:c=J CRJTICAl ORIFiCE SeT SeRIALI!-;~ EQUIPMENT 10 II: K' TESTED .-----.----11 FACTOR I VACUUM RUN II 1 (AVGI (in Hg) 0.4238 12 205.301 210.825 5.525 10 67 70 70 75 0.4238 12 210.825 217.220 6.394 70 70 73 75 78 0.4238 12 217.220 222.801 5.581 70 73 75 78 81 G' D:rnEB D:rn EB .0 .0 .0 .0 .0 .0 I III D I I II II USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: Facility FINAL 25.30 1 1 ELAPSED DGM I TIMe~MtN) AVG 70.50 10.00 74.00 11.50 76.75 10.00 0.00 § 0.00 0.00 0.00 § 0.00 0.00 Denison Mines AVG(P ... ) 25.30 0.67 4.6598 0.67 5.3573 0.67 4.6522 § § IF V VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 4.6588 1.000 5.3576 hQQll 4.6588 JJ!ll AVG~ 1M!! 0.00 AVG~ AVG~ 1.464 1.455 M£ The follow!!1g €Qu8!ions aI'S m:ed to calculate the standard volumes of ai:' pa5Sed !hrcugh the DGM, Vm (s~), and thE crif.cal orifice, V, (std) and the DGM carob,ation factor, Y. These equations are automatically calculated in the spreadsheel above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 11.000 I (1) (2) (3) Vcr("J, = K'* Pbar * El .JTamb VCI;,:;li y= - Vm,Jt.:l, = Net volume of gas sample passed through DGM, corrected to standard conditions K, ~ 17 64 'R/in Hg (English). 0 3858 'Klmm Hg (MetriC) T m ~ Absolute DGM avg temperature ('R • English, "K. Metne) ~ Volume of gas sample passed through the critical orifice, correcled to standard conditions T~mb ~ Abso,ute ambient temperature (OR -Ell9llsh. =K -Metric) K'::: Average K' factor from Cri!ical Orifice Calibration = DGM calibra~on factor AVERAGE t.H~ =11.4561 2 AH@ ~ (0.75 a) t.H (Vm(std)) V,,(std) Vm POST Console #5 Calibration 2010 Type S Pitot Tube Inspection Data Dat~' I 7. " "I -I () Pi tat Tube ldentitication' __ or---.:_-....:(---.:g-'~ ______ _ DI t ~ I PA A ! , II A. PEl I Dt= ' ~-'S-10, PA "" . l-i S' 0 ilL [s P A = Pa ? Ye 5 --~~~--------Is 1.05· D, ~ D, ~ \.50· D, ? __ V.J.....,.;.c:...-=-5 ....... _____ _ Po = .L(CO in Ct,<to' 0.,= (.(,< 10' Ct.2= '1... lr----...........,~BA ' ~ I [-~ 1'1 < 5' III < 5' '---!... 132 Z"O,125 in. Z= I f~l C· ~~.. in --- W" 0,03125 in W= _' • OO'2~in, W> 3 inches W= Z > 3/4 inch Z= I , I --' •• ,. ""I~r-;: _____ Y::::I inches ! The pilot tube m~ets the specifications for a calibration factor 0[0 &41 Temperature Sensor Callbratl<l1l Reference Temperature Temrx:rature Source Ref~rence Sensor (M~dium) ("F) (OF) AIR 10 ""10 Probe Continuity . ,......---..------..--1----'7 Heat Check 248 -'F Y-e.& AIR 10 ,0 IC£WATER ~r6 :~() Stack BOIL WATER WL( 1-h ~ SILICONE OIL C,. \ 17 . in -7/ V in. in Temperamre Difference (of) b ~~::2 '1~.V 1') h I I Type S Pitot Tube Inspection Data Date: _\.:.--1_p_'_--,(--,0 __ Pi tot Tube Identification' _"1---=:._""'_-_6( ______ _ OF . S 7 ~ in. --,P A:-=_' _4--'--t...-'-I ..... ~~_in. ~PB!!....= __ • --Ltr......;qJ-LZ __ 1n Is P A = Pn ? r -c. ? Is 1.05' D, :S D, :S 1.50' D, ? ==~V=-e..-:===<s======== 0., '= __ £:--:-__ _ ":=-_....:.'--- ~I < 5" PI = __ --'-__ _ ~,< s" P, =_---'0""--__ Z"O 125 in Z =_ .00 z.. _in. I i W" 0 03125 in. W > 3 inches Z> 3/4 inch W= W= Z= -.-~-, . ..r=:,.: ____ Y~3 inches ~_~~'w ! The pilot tuue meels the specifications for a calibration factor of 0.84" Temperature Sensor Calibration Reference' Temperature Temperature , Source Reference Sensor (Medium) C'F) ("F) AIR IV ~cr Probe Continuity ---7' Heat Check 248 -9 '-( e."b AIR ,0 ~(o "t ICE WATER "::.~ 3,"? Stack BOlL WATER cDS 7.J?;cr: SILICONE Oil . (JO...5 in, .:s in. in. Tcml'crnturc Dinerence con ( y(/ S "2.. &-() I /") f) Date: \ '" -1;) .-\0 Dt t :: :11"""- Y"""L========="""C::-_j z ..... s'., ,-c::t::> Type S Pitot Tube Inspection Data Pitot Tube Jdcntification._L:t:.;~l.l_-~V(:...!..._-.-::~=-___ _ Technician I.{ • IV\. v1\.£c...h(1Q'("-'3, r .~7S HI. Is P A = P B ? -'1¥L-t:,./:J,£._9:;,-=--___ _ -,I' AO-=----4-' _Y.L.f.(.J-51N..-__ in Is 1.05' 0, :5: D,:5: 1.50' 0, ? \ I -<c~ ~4JI[-=.!~-=--- eL, < 10' a, < I D· i3, <5' ZoO 0125 in W $003125 in W> 3 inches Z > 3/4 inch !x, = __ 1.-""""--__ _ a, =----.3~-- fl, = __ -"0'--__ p, =-_&=--- r-.-Z = • () '") S in W= Of" in ~ I W= 11 " in Z= 1 '1-, in I ""-_-",,I...Il;.IJU-.... ~ ... -4==1,; _____ y ~ J inches y= 3 f-t_ 111. The pilot tube m~ets the specifications for a calihration factor ofO.84~ Temperature Sellsor Calibration Reference' TelTlperature ,. ~mpc:r.ll\lr<: Temperature Source Ref~rencc Sensor Difference (MedIum) (uF) ("F) (OF) AiR (() 7f (A~ b Probe Continuity -. .......--'-r.e--~ Heat Check 248 -7 y~ 7.C;D AIR ICn CW' lo~ 0 ICE WATER S 1_ l?L U Stack BOIL WATER 17o f...-1 Z. OCJ/ () SILICONE OIL TETCO Sample Box Temperature Sensor Calibration Date: 12/29/1 0 Calibrator: Mike McNamara Reference: Ome~a CL3512A Thermocouple Temperature Temperature Temp. Diff. Unit ID Location Source Reference Sensor or Result (Medium) (oF) (oF) ("F), PIF Oven Water 34 34 0 Water 203 203 0 A Water 34 33 1 Probe Out Water 203 204 -1 Water 34 36 -2 Impinger Out Water 203 203 0 Oven Water 32 34 -2 Water 203 204 -1 B Water 32 33 -I Probe Out Water 202 204 -2 Water 31 31 0 Impinger Out Water 203 205 -2 Water 34 36 -2 Oven Water 204 205 -1 C Water 34 36 -2 Probe Out Water 203 205 -2 Water 34 36 -2 [mpinger Out Water 203 201 2 Oven Water 33 33 0 Water 203 203 0 D Water 33 33 0 Probe Out Water 202 203 -1 Water 33 33 0 Impinger Out Water 203 201 2 Oven Water 33 34 -1 Water 203 203 0 E Water 33 34 -1 Probe Out Water 203 204 -1 Impinger Out Water 33 33 0 Water 203 204 -1 Oven Water 33 33 0 Water 203 202 1 F Water 33 33 0 Probe Out Water 203 201 2 Water 33 34 -1 Impinger Out Water 203 201 2 I Impinger Out G Water 33 34 -1 Water 203 202 1 I Impinger Out H Water 33 35 -2 Water 203 202 1 I Impinger Out I Water 33 33 0 Water 203 204 -1 I Impinger Out J Water 33 33 0 Water 203 204 -1 APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. ATTACHMENT H SURFACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-05 1.00E-06 1.00E-07 -CII Cii ~.OOE-08 •• en o ....I - 1.00E-09 1.00E-10 1.00E-11 OJ'Of), ~" ~ • • • • --- • • ._---- Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) & • • • ... • • • • ":. .. - --- • • - • - ... .. -*-++-•• • . . ------... . ........ .....-. ~ ~~Oj ~~ OJOJf), ~" ~~'" p;,'O ~~Oj ~ro • U-Nat. _ Th-230 A Ra-226 t;)~ ~ ~ <, 'i::J~OJ ~r,; <,}" & .. • -- 1.00E-06 1.00E-07 1.00E-08 -.!! as u cn1 .00E-09 Cl o ..J - 1.00E-10 1.00E-11 1.00E-12 fb<O "Q) ~~ . ...., • = -•• • si-~"Q) ~f1,~ Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) • -• • • ~ • '" • ~ ... ~ . ...., •• ...., • ~ --= • ----• .. .. • .---. • • • . -------. .. . . .. -------••• ~ - , ~~ ~~ ~<o ~co !:.)" ~ !:.)!O !:.)O; Q) "Q) ~"Q) ~"Q) ~ ~ ~ ~ ~" ~ ~rv (I.~ r}rv ~'V ~,,~ ~"t;;:j rJ n}rv ~rv cb''V n} "rv " • U-Nat. .Th-230 • Ra-226 I EN:RGY ,\ l ~.J I . \ I \... I ~,. ,,-. www.energylab.com AMIyI/I:IIEBIf.Ww .. ,m Halene, MT 877--472-0711 • Billings, MT 801-735-4489 . Caspar, WY 888-235-0515 Gillatta, WY 11&-&88-7175 • Rapid City, SD 188-172-1225 • College Station, IX 881-&99-2218 March 25, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11030344 ANAL VTICAL SUMMARY REPORT Project Name: 1 st Quarter Surface Water 2011 Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 3/11/2011 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C11030344-001 Cottonwood 03/09/11 11 :05 03/11/11 Aqueous Solids, Total Dissolved Solids, Total Suspended C11030344-002 Temp Blank 03/09/11 0 :00 03/11 /11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: cS¥~J) tJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011 .03.25 10:04:52 -06:00 Page 1 of 8 WYtW.energylab.com AMIytItM EmIINI:I SIIIu 1m Helena, NT 877·472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235-0515 Gillette WY 868·186· 7175 • Ra Id CI so 188·872·1225 • Colla e Stalion IX 881-890·2218 CLIENT: Denison Mines USA Corp Project: 1 st Quarter Surface Water 2011 Report Date: 03/25/11 Sample Delivery Group: C11030344 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 8 EN:RGY i\''; )1 </\ I ( ! 'I .: www.energylab.com AIIIIytIaI b,,'" SItIc. IW Halena, 1fT 877-47NI711 • Billings, MT BOI-735-4489 • Caspar, WY 888-235-8515 Gilletta, WY 888-188-71 75 • Rapid City, SO 888-&12-1225 • Collage Station, IX 881-180-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab 10: 1 st Quarter Surface Water 2011 C11030344-001 Client Sample 10: Cottonwood Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Solids, Total Suspended TSS @ 105 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 425 7 Units mgll mg/l Qualifiers Rl 10 4 Report Date: 03/25/11 Collection Date: 03/09/11 11 :05 DateReceived: 03/11/11 Matrix: Aqueous MCU QCl Method Analysis Date I By A2540 C 03/11/1115:45/1r A2540 D 03/11/1116:40/1mc MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 3 of 8 EN:RGY .\, ()I ~.\ltjl.I.·~ www.energylab.com ~/ wfl.rccl SItru ,m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-D515 Gillette, WY 88&-18&-7175 · Rapid Ciiy, SD 188-&72-1225 · Coli ega Station, TX888-69D-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1 st Quarter Surface Water 2011 C11030344-002 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.0 Qualifiers Rl Report Date: 03/25/11 Collection Date: 03/09/11 DateReceived: 03/11/11 Matrix: Aqueous MCL! QCl Method Analysis Date / By E170.1 03/11/11 09:00/ kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 8 EN:RGY ") II ud ~)f.I ' '_ www.energylab.com AIuIfIIt:M~SIIrcI' 1m Helena, MT 817-472-0711 -Billings, MT 800-735-4481 -Casper, WY 888-235-1515 Gillette, WY 88&·&88-7175 -Rapid City, SD 888-&72-1225 -College Station, 1)( 888-810-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter Surface Water 2011 Analyte Count Result Units Method: A2540 C Sample 10: MBLK1_110311 Solids, Total Dissolved TDS @ 180 C Method Blank ND mg/L Sample 10: LCSC110311 Laboratory Control Sample Solids, Total Dissolved TDS@ 180 C 984 mg/L Sample 10: C11030313-002AMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 2590 mg/L Sample 10: C11030344-001AOUP Sample Duplicate Solids, Total Dissolved TDS@ 180 C 410 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 03/25/11 Work Order: C11030344 RL %REC Low Limit High Limit Run: BAL-1_110311A 4 Run: BAL-1 _110311A 10 98 90 110 Run: BAL-1 _110311A 10 102 90 110 Run: BAL-1 _110311A 10 ND -Not detected at the reporting limit. RPO RPOLimit Qual Batch: 110311_CSLDS-TDS-W 03/11/11 15:40 03/11/11 15:40 03/11/11 15 :44 03/11/11 15:46 3.4 10 Page 5 of 8 EN:RGY , .. ~>(H~J\l tlll:' ~. www.energylab.com AM/yf/M EluI1Mn'-' '151 Helena, MT 877·472-0711 • Billings, MT 800·735·4488 • Casper, WY 888-235-1515 Gillette, WY 885·188·7175 • Rapid City, SO 188·672·1225 • College Station, 1X 881480-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter Surface Water 2011 Analyte Count Result Units Method: A2540 D Sample 10: MBLK1_ Solids, Total Suspended TSS @ 105 C Method Blank ND mg/L Sample ID: LCS1_ Laboratory Control Sample Solids, Total Suspended TSS @ 105 C 150 mg/L Sample ID: C11030372·003ADUP Sample Duplicate Solids, Total Suspended TSS @ 105 C ND mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 03/25/11 Work Order: C 11030344 RL %REC Low Limit High Limit Run: BAL-1 _110311B 6 Run: BAL-C 110311B 12 75 60 110 Run: BAL-C 110311B 4.0 ND -Not detected at the reporting limit. RPD RPDLimit Qual Batch: R143577 03/11/11 16 :40 03/11/11 16:40 03/11/11 16:42 10 Page 6 of 8 www.energyleb.com Atu/fIIaI £Ja/Iaw S/IJa IW Helana, MT 877~72-0711 • Billings, MT 801-735-44811 • Casper, WV 888-235-0515 Gillatta, W'( 18&-&88-7175 • Rapid City, so 111-172-1225 • College Station, TX 881-&10-2218 Workorder Receipt Checklist Denison Mines USA Corp II"IIIIIIIII~ 11II 11111 I~I~I C11030344 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 3/15/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper containerlbottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.0'C On Ice Yes D Yes 0 Date Received: 3/11/2011 Received by: ha Carrier name: FedEx No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0 No VOA vials submitted 0 Not Applicable D Page 7 of 8 "'U til (C CD co o -co tafl(97 Chain of Custody and Analytical Request Record Page_l _of~ PLEASE PRINT (Provide as much information as possible.) Company Name: M; (\e.~ Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: D~n·;.s Dtl lSI Q\AC).rt~ (' S;:,..MCl.l:.e We...+e,r State: l(/ Yes g'" No 0 I Report Mail Address: PO ~O"l< ~Ot{ Contact Name: Phone/Fax: Email: Sampler: (Please Print) I <O\M~·'('\C\ LX\" ~!..\~i\ R~/).{\ rl>o..\N)ef L\3..'S (" 7g ~\ i\jO\tl Po-.lttlGJ I Invoice Address:-.....l Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: , ~N'"I\e ~(f\t. Special Report/Formats: ~ ~W®O® ~@{lD~m@ .. Contact ELI prior to I~;(J~ LY-e ~ RUSH sample submittal ~OCll~ ~ for charges and Cooler Il(s}: ~Cl~C5J Q) 0 R scheduling -See ~ o DW D EDD/EDT(Electronic Data) 1§> a5 iO <6 W t:. Instruction Page cCl)'Us l:l ~ I "0 o POlW f\NWTP Fonmat: 83:'5 gj g () c Comments: ReceiptTemp :l U .... < COliIlt:><: <t: e "0 °c o State: 0 LEVEL IV o ~ c: "-<rim c:".:;: I--III is a.ml,Bo c D Other: D NELAC I--.... On Ice: <!)N E~m ' <t: :l :l..92~I~~ l-S zo.. 0>0 ~ W "E Custody Seal E >1 ~ W III On Bottle Y N ~ rn "0 ffi: c: OnCocler 'r-\-~ H Intact CI) SAMPLE IDENTIFICATION Collection Collection MATRIX Signature Q)N (Name, Location, Interval, etc.) Date Time Match 1 ~ o-tto(ju.JOO~ "!.-q-l.DI\ \ lOt... \ -w '/. 'i ~ 2 ..... ~ ~ - 3 _L~~_'h\C\. ~'C g nnn 4 ~. 5 ~ ~ 6 ~ 7 ~ 8 ~ 9 , ~ 10 ':! Y/&Jtf.3 y~ Custody 1~":~S;;bY~\ :1&.u ~_~~;;\ I \O~(;) ::Jl!tllII: ... naJJJ~k J Received by (PIlot) DaleJTln\e: Slgn~ture; Record ReiMuished by (prinl~ d DaleITIme: Sognature: .....J Received by (print): DatelTl!11e; Signature; MUST be Signed Ke ... ,vO(J "Y u DOralOry: 3~\~\ \ -~ rt~~~ Sample Disposal: Return to Client: Lab Disposal: -r-'0 In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated 00 your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule. forms, and links. EN:RGY .~\ \)lj~\I CI..t ~~ www.energylab.com AMIybI EmIINa $flu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatte, WY 8&B·B8B· 7175 • Rapid City, SD 888-&12-1225 • College station, IX 888-690-2218 ANALYTICAL SUMMARY REPORT June 23, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11050696 Quote ID: C1640 -POC Wells Project Name: Semi-Annual Surface Water 2011 Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 5/20/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11050696-001 Cottonwood Creek 05/18/11 8 :30 05/20/11 Aqueous Metals by ICP/ICPMS, Dissolved Sample Filtering Uranium, Suspended Digestion, Total Metals Gross Alpha minus Rn222 and Uranium Radium 226, Dissolved Radium 226, Suspended Thorium, Isotopic Thorium, Suspended Isotopic Solids, Total Dissolved Solids, Total Suspended C11050696-002 Temp Blank 05/18/11 0 :00 05/20/11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~cD WtJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.06.23 14:38:43 ·06:00 Page 1 of 12 www.energy1ab.com AM/yIIoI~SI.u '1151 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-D515 Gillette, WY 8&&-188-7175 • Ra id City, SO 888-&72-1225 • College Siafion. TX 888-690-2218 CLIENT: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Report Date: 06/23/11 Sample Delivery Group: C11050696 CASE NARRATIVE TH230 ANALYSIS USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency prior to using these results for compliance purposes. RA226 ANALYSIS USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency prior to using these results for compliance purposes. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-! -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EI\ERGY /\ I )' 1/, I ~~: ~' • www.energylab.com ~1m.u.-SIRu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-18&-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Lab 10: C11050696-001 Client Sample 10: Cottonwood Creek Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Solids, Total Suspended TSS @ 105 C METALS -DISSOLVED Uranium METALS-SUSPENDED Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC RADIONUCLIDES -SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC -See Case Narrative regarding Ra226 analysis. -See Case Narrative regarding Th230 analysis. Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 463 mg/L ND mg/L 10.2 ug/L ND ug/L 0.2 pC ilL 0.2 pC ilL 0.3 pCilL 0.06 pCi/L 0.13 pCilL 0.21 pCi/L 0.07 pC ilL 0.1 pC ilL 0.2 pCi/L -0.2 pCi/L 0.18 pCi/L 0.45 pC ilL 0.2 pCilL 0.2 pCi/L 0.3 pCilL MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Report Date: 06/23/11 Collection Date: 05/18/11 08 :30 DateReceived: 05/20/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By D U U U U U 10 A2540 C 6 A2540 D 0.3 E200.8 0.30 E200.8 E900.1 E900.1 E900.1 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. 05/20/11 14 :19/1mc 05/20/11 15 :00 lime 06/22/11 13 :021 sml 05/31 /1118:21/sml 06/16/11 11 : 13 1 ep 06/16/11 11 :131 ep 06/16/11 11 :13 1 ep 05131/11 12:051 trs 05/31/11 12:051 trs 05131/11 12:051 trs 06114/11 08:49 1 dm! 06/14/11 08:491 dmf 06114/11 08:49 1 dm! 05131/11 17:25 1 trs 05131/11 17:25 1 trs 05/31/11 17:25 /trs 06/09/11 11 :02 1 dm! 06109/11 11 :02 1 dm! 06/09/11 11 :02 1 dm! Page 3 of 12 ---~ EN:RGY .' /\t-I °llJd CHI .~ www.enefgylab.com AM/ytJaI rn.u-. SiIu 1111 Halena, fIT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-188-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-610-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Semi-Annual Surface Water 2011 C11050696-002 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 4.0 Qualifier RL Report Date: 06/23/11 Collection Date: 05/18/11 DateRecelved: OS/20/11 Matrix: Aqueous MCU QCL Method Analysis Date 1 By E170.1 05/20/11 08:501 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 12 EN:RGY i'.tJ(]f:/.ICHlt .~ www.energylab.com AMITIIa/ EluIIMI" $1_ '1$2 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218 OA/oe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Count Result Units Method: A2540 C Sample 10: MBLK1_ Method Blank Solids, Total Dissolved TDS @ 180 C ND mg/L Sample 10: LCS1_ Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1010 mg/L Sample 10: C11050660-002AOUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 1750 mg/L Sample 10: C11050712-001BMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 2430 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 4 10 10 10 Report Date: 06/23/11 Work Order: C11050696 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R146206 Run: BAL-1_11 0520B OS/20/11 14:14 Run: BAL-1_11 0520B OS/20/11 14:14 101 90 110 Run: BAL-1 _110520B OS/20/1114:12 0.1 10 Run: BAL-C 110520B OS/20/11 14:22 100 90 110 ND -Not detected at the reporting limit. Page 5 of 12 EN:RGY "\~'01 /J'''C;''''l ·. www.energylab.com ~ ExuIIMu SIIIu llf1 Helena, MT 877-472-0711 • Billings, MT 800-735-44" • Casper, WY 888-235-0515 Gillotte, WY 8&6-&8&-7175 • Rapid CHy, SO 818-872-1225 • Cot/ege Station, lX 888-680-2218 OA/oe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Report Date: Work Order: ------------------------- Analyte Count Result Units RL %REC Low Limit High Limit RPO Method: A2540 0 Sample 10: MBLKC Method Blank Run: BAL-C110S20A Solids, Total Suspended TSS @ 105 C ND mg/L 2 Sample 10: LCS1_ Laboratory Control Sample Run: BAL-1_110S20A Solids, Total Suspended TSS @ 10S C 144 mg/L 12 72 60 110 Sample 10: C11050687-001AOUP Sample Duplicate Run: BAL-1 _110S20A Solids, Total Suspended TSS @ 105 C 184 mg/L 24 0.0 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration 06/23/11 C11050696 RPOLimit Qual Batch: R146133 OS/20/11 14:S9 OS/20/11 14:S9 OS/20/11 1S:00 10 Page 6 of 12 EN:RGY I\fjOI~,\f vlll~ '-> www.energylab.com IMJttIaI buIIMU SIIIa 1m Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 816-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-680-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Count Result Units Method: E200.8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: C11050696-001BMS4 Uranium Sample 10: C11050696-001BMSO Uranium Method: E200.8 Sample 10: MB-29928 Uranium Sample 10: LCS2-29928 Uranium Sample 10: C11050675-001HMS Uranium Sample 10: C11050675-001HMSO Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank 5E-05 mg/L Laboratory Fortified Blank 0.0524 mg/L Sample Matrix Spike 0.0636 mg/L Sample Matrix Spike Duplicate 0.0701 mg/L Method Blank ND mg/L Laboratory Control Sample 0.102 mg/L Sample Matrix Spike 0.00500 mg/L Sample Matrix Spike Duplicate 0.00514 mg/L Report Date: 06/23/11 Work Order: C11050696 RL %REC Low Limit High Limit Run: ICPMS2-C_11 0622A 1E-05 Run: ICPMS2-C_11 0622A 0.00030 105 85 115 Run: ICPMS2-C_11 0622A 0.00030 107 70 130 Run: ICPMS2-C_11 0622A 0.00030 120 70 130 Run: ICPMS4-C_11 0531 A 7E-05 Run: ICPMS4-C_11 0531 A 0.00030 102 85 115 Run: ICPMS4-C_11 0531 A 0.00030 105 70 130 Run: ICPMS4-C_11 0531 A 0.00030 109 70 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual 9.7 2.9 Batch: R147252 06/22/11 11 :41 06/22/11 11 :44 06/22/11 13 :05 06/22/11 13:07 20 Batch: 29928 05/31/11 18:16 05/31/11 18:18 05/31/11 18:29 05/31/11 18:30 20 Page 7 of 12 EN:RGY ,\ I. ::'))11\ I (")1 ~Il '. www.energytab.com AM/fIIaI ~StlIu II1S2 Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 811-235-0515 Gillette, WY 11&-188-7175 • RapId City, SO 888-872-1225 • College Station, lX 881-&10-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Report Date: 06/23/11 Work Order: C11050696 ------------------- Analyte Method: E900.1 Sample 10: MB-GA-0440 Gross Alpha minus Rn & U Count Result 3 Method Blank 0.1 Gross Alpha minus Rn & U Precision (±) 0.5 Gross Alpha minus Rn & U MDC 0.8 Units pCi/L pCi/L pCi/L Sample 10: LCS-GA-0440 Gross Alpha minus Rn & U Laboratory Control Sample Sample 10: C11050582-010CMS Gross Alpha minus Rn & U Sample 10: C11 050582-01 OCMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC - Minimum detectable concentration 22.6 pC ilL Sample Matrix Spike 44.8 pCi/L Sample Matrix Spike Duplicate 44.3 pCi/L RL %REC Low Limit High Limit Run: G542M_110613A Run: G542M_110613A 106 70 130 Run: G542M_110613A 95 70 130 Run: G542M_110613A 94 70 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 1.1 Batch: GA-0440 06/15/11 16:01 U 06115/11 16:01 06116/1111 :13 06116/1111:13 26 U -Not detected at minimum detectable concentration Page 8 of 12 EN:RGY ,'\ t ~ \ ~ I I'; '-, www.energylab.com AIIIIftIm IxuIIInu SIl1C11IW Helena, MT 877-.472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 886-686-1175 • Rapid City, SD 888-672-1225 • Col/ege Station, TX 888-690-2218 OA/oe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Report Date: 06/23/11 Work Order: C11050696 ------------------------------- Analyte Count Result Units Method: E903.0 Sample 10: C110S0640-o03EMS Radium 226 Sample 10: C110S0640-003EMSO Radium 226 Sample 10: MB-RA226-S37S Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-RA226-S37S Radium 226 3 Sample Matrix Spike 13 pCi/L Sample Matrix Spike Duplicate 13 pCi/L Method Blank -0.04 pCi/L 0.1 pCi/L 0.2 pCi/L Laboratory Control Sample 7.5 pCi/L RL %REC Low Limit High Limit RPO RPOLlmlt Qual Run: BERTHOLD 770·1 _110520A 103 70 130 Run: BERTHOLD 770-1 _11 0520A 100 m 1~ 3.1 Run: BERTHOLD 770-1 _110520A Run: BERTHOLD 770-1 _11 0520A 119 85 115 Batch: RA226-5375 05/31/11 10:32 05/31/11 10:32 24.6 05/31/11 12:05 U 05/31 /11 12:05 S • lCS response is outside of the acceptance range for this analysis. Since the MB, MS, and MSD are acceptable the batch is approved. Method: E903.0 Sample 10: C110S067S-001HOUP Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C110S0696-0010MS Radium 226 Sample 10: LCS-29928 Radium 226 Sample 10: MB-29928 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Sample Duplicate -0.041 pCi/L 0.047 pCi/L 0.11 pCilL Sample Matrix Spike 20 pC ilL Laboratory Control Sample 12 pCi/L Method Blank ·0.1 pC ilL 0.1 pCIIL 0.3 pCi/L U -Not detected at minimum detectable concentralion 98 Run: BERTHOLD 770-2_11 0525A 150 Run: BERTHOLD 770·2_11 0525A 70 130 Run: BERTHOLD 770-2_11 0525A 102 85 115 Run: BERTHOLD 770-2_110525A NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Batch: RA226-5384 05/31/11 17:25 379.3 U 05/31/11 17:25 05/31/11 17:25 05/31/11 17:25 U Page 9 of 12 EN:RGY , l ., [ ~, I ~ ., J www.energylab.com ~I fulllllJl!' SIJIu 1152 Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&86-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Count Result Units Method: E908.0 Sample 10: C11050675-002HMS Thorium 230 Sample 10: C11050675-002HMSO Thorium 230 Sample 10: LCS-29928 Thorium 230 Sample 10: MB-29928 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Method: E90S.0 Sample 10: LCS-RA-TH-ISO-1403 Thorium 230 Sample 10: C11060153-0120MS Thorium 230 Sample 10: C11060153·0120MSO Thorium 230 Sample 10: MB·RA·TH·ISO·1403 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Sample Matrix Spike 7.9 pCi/L Sample Matrix Spike Duplicate 8.5 pCilL Laboratory Control Sample 8.5 pCi/L Method Blank 0.04 pCi/L 0.1 pCi/L 0.3 pCi/L Laboratory Control Sample 6.0 pCi/L Sample Matrix Spike 12 pCi/L Sample Matrix Spike Duplicate 15 pCilL Method Blank -0.02 pCi/L 0.09 pCilL 0.2 pCi/L Report Date: 06/23/11 Work Order: C11050696 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: 29928 Run: EGG-ORTEC_110607A 06/09/11 11 :02 91 70 130 Run: EGG-ORTEC_110607A 100 70 130 7.9 06/09/11 11 :02 37.7 Run: EGG-ORTEC_110607A 87 70 130 Run: EGG-ORTEC_110607A Run: EGG-ORTEC_110610A 102 70 130 Run: EGG-ORTEC_11 061 OA 94 70 130 Run: EGG-ORTEC_11 061 OA 06109/11 11 :02 06/09/11 11 :02 U Batch: RA-TH-ISO-1403 06/14/11 08:49 06/14/11 13:20 115 70 130 19 06/14/11 13:20 38.9 Run: EGG-ORTEC_110610A ND -Not detected at the reporting limit. 06/14/11 13:20 U U -Not detected at minimum detectable concentration Page 10 of 12 EI\ERGY '\I,e I "I. I.' " www.energytab.com AalytJQI~$Itru 1151 Helene, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-05\5 Gillette, WY 866-&86-1175 • Rapid City, SO 888·672·1225 . Collage Slation, TX 888·690·2218 Workorder Receipt Checklist Denison Mines USA Corp IIIIIIII ~111~lllIlllllllllillllllll~III~1I11I1 ~II C11050696 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 5/20/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper containerlbottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0' Yes 0' Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 4.0'C On Ice Yes 0 Yes 0' Date Received: 5/20/2011 Received by: em Carrier FedEx name: No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0' No VOA vials submitted 0' Not Applicable 0 Sample split, filtered, and preserved as necessary for dissolved and suspended analysis. Page 11 of 12 IgEIr(eV Chain of Custody and Analytical Request Record Page _,_ of _,_ MtdihA'I!kll4' Company Name: DdI;SOfl M ;n~ Report Mail Address: fO fIO)C goCf Blcwl~n..1 UT BLi511 Invoice Address: ~ct.fW)(.. Special Report/Formats: Dow o EDD/EOT(Electronic Data) o POTWNVWTP o State: ___ _ o Other: Format:~ __ _ o LEVEL IV o NELAC SAMPLE IDENTIFICATION Collection Collection (Name, Location, Interval, etc.) Date Time 1 L~++orWlOOL c.,.u.K I 'SlJU II I 0S30 2~j)fi#4- 3 I' 4 -5 - 6 -7 -8 -9 - PLEASE PRINT (Provide as much information as possible.) Project Name, PWS, Permit, Etc. I Sample Origin EPNState Compliance: Se.m; Af1t)~' 5u.r+",Cc. LJtA,,+et'" ~Oll Contact Name: Phone/Fax: R ~ 0.." f' ,,) mer y35 '78 ~a~1 Invoice Contact & Phone: ~".,~ $: o -~o ",jg :gal~OI ~ 'j§>~ ~iil c (J) Ci5 '" :s: o::>=~ Cl u::> 0 0 c '0 « ~liXil :i2 ~ 2tS c=.§ ~~I~C? :l 0).= a; 3: zc..«Ig>o ~ >1 (J) MATRIX l-W ~LN1S7@D@ ~rn@QD[3@'U'[§[Q) ~\l'I l-~ Cl w I 0 « I-~ W w (/J State: w Yes [2( No 0 Email: Sampler: (Please Print) ...,.. ~lJe'" HolI: ~ '1 Purchase Order: Quote/Bottle Order: .. ~ R "0 C e I U ro c 5 ~ I S ro "0 C ~I H Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page (/je¢/ Comments: Re ,;;emp °c On Ice: 1"iTN Custody Seal • .......,. OnBott:e o.tu On Coole, Intact y Signature • N Match ~ ~ ~ ~ '= ~ ~ (6) u=::. ~ ~ 1~/hs'~t 'U I 10 I~ tll <C Custody (I) ..... N Record 0 DateITime Signatu,o: ReCeIved by (print); Sig118tu,e: *:i~,;;ytnll;! ... ~/I;;; 1030 :"\IIIlUIf '1!';''L DaIeffime: Reh~qulshed by (pml): 'J Daiemme: -U ---Signalure: "" ~OGelved by (prlrot): -MUST be ..... N Si!]ned reCeIved bezw~ Dale! 15"'~ -Srg03lUre' I Sample Disposal: Return to Client: Lab DISPOSal:~ ~ 8J;:u In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule. forms, and links. ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QNQC Soil samples are collected during the third quarter. This Attachment has been deliberately left blank.