DRC-2009-006027 - 0901a0688014768d

State of Utah
JONM. HUNTSMAN, JK.
Govenioi-
GARY HF.RBERT
Lieiiienom Governor
Department of
Environmental Quality
Anunda Smith
Al tiiii^ L.xcrniivi' Director
DIVI.SION OF RADIATION CONTROL
Dane L FincTfruck
Director
btc- POT -a)u^o.n
MEMORANDUM
TO: Loren Morton, Section Manager
KROM: Dean Henderson, HydTogeologist
DATE: November 3, 2009
/fi?/^ ,/ v^i
///>f
SUBJECT: Data Evaluation for the Split Sampling of Well MW-32 in December 2008.
Groundwater Inspection Module at the Denison Mines (USA) Corp.
White Mesa Mill facilily near Blanding, Utah
On December 9, 2008 a field inspection and split sampling was conducted at Denison Mines
(USA) Coip. (hereafter "DUSA") White Mesa Mill facility near Blanding, Utah. On January 12,
2009 the field inspection and split sampling event were summarized in a Division of Radiation
Control (hereafter "DRC") staff memorandum (hereafter "DRC 2009"). However, as addressed in
DRC 2009 the split sampling results for MW-32 had not been received from Lionville Laboratory
therefore, the data evaluation of the split sample results would be performed at a later date. The
sample results were received by DRC from Lionville Laboratory on March 30, 2009. This is a
data evaluation of the split sample results for well MW-32 for the December 9, 2009 accelerated
sampling event.
DRC DATA EVLAUATION
The data evaluation will follow the DRC Data Evaluation requirements in the Utah Department of
Environmental Quality Division of Radiation Control Guidance for Groundwater Split Sampiing
CoUection at Uranium Mill Operations (hereafter "Guidance'').
Data Validation
Verify That Analvsis Was Conducted Within Metiiod Holding Times
The required analytical method for cadmium, iron, manganese, and nickel in Table 1 in section
8.2 of the While Mesa Uranium Mill Ground Water Monitoring Quality Assurance Plan (hereafter
"QAP") is E200.8. However, in Table A6-C of AttachmenI D of the State of Ulah Contract
168 North l'J50 West • Salt Uke Citv. UT
Mailing Addre.is. P.O.Box 144850 • .Sail Like Cily, UT 84114-4850
Telephone iXOI l 536-4250 • Fax ^8nl) 5.13-40'J7 -TDD («01) 536 4414
ttinied on 100^: recycled p;ipcr
(Contract # 086096) Ihert^afier "Contraci"] with Eberline Services states that the analytical
method for cadmium, iron, manganese, and nickel concentrations in water will be SW 6010B.
According to Table 2-35 in chapter 2 of the EPA publication SW 846, entitled Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods (hereafter "EPA SW 846"), SW 60I0B is an
acceptable analytical method to analyze for concentrations for the four metals, listed above, in
water. As documented in the Table 1 below, the SW 601 OB method analysis was conducted
wiihin 6 month holding time as required in Table 2-36 of chapter 2 of EPA SW 846.
Table 1
Sample Holding Times
Parameter
Cadmium,
iron.
Manganese,
and Nickel
''Well Sample Date
MW-32
12/09/08
MW-99
J 2/09/08
^Date Sample
Analyzed
MW-32
02/25/09
MW-99
02/25/09
"^"•'Required
SW 6010 B
Method
Holding
Time for
Listed
Parameters
6 months
Was Sample
Analyzed With in
the Required
Holding Time
MW-32
yes
MW-99
yes
1. See pages I o\'l and 2 of 2 nf ttie Inorganic Analysis Dala P.nckage ofthe Lionville Laboratory Analyses Data
Package (see Attachment 1).
2. Sec copy ofthe Custody TrnnsTer Record/Lab Work Request in the Lionville Laboratory Analyses Datn Package
(sec Attachment 1).
3. .See Table 2-3-'^ and Table 2-36 in chapter 2 of the EPA SW 846.
4. See Table A6-C of Attachmem D of the State Contract.
Verify That Appropriate Anaivtical methods were used
The Guidance states "//i the case of analytical methods, the DRC will use the same methods found
in the facility's approved QAP to lhe extent practicable.'' The DRC contracted laboralory,
Lionville Laboratory, uses method SW 6010B to analyze for concentrations of cadmium, iron,
manganese, and nickel in water. Although this method is not the same method used by DUSA
(E200.8), as stated above, method SW 6010B is an acceptable analytical method to analyze for
concentrations of cadmium, iron, manganese, and nickel in water. Therefore, method SW 6010B
was a practicable method to analyze for the 4 lisied metals above. According to pages 1 of 2 and
2 of 2 of the Inorganic Analysis Data Package of the Lionville Laboratory Analyses Data Package
(see Aitachmeni I) cadmium, iron, manganese, and nickel were analyzed using method SW 6010
B.
Verify That Detection Limits Were Appropriate
As stated above, method SW 6010B is an acceptable analytical meihod lo analyze for
concentrations of cadmium, iron, inanganese, and nickel in water. The detection limit for these
four metals musl be at or below the ground water compliance limit (hereafter "GWCL") for each
metal found in Table 2 in Part C. I of the Stale of Utah Division of Water Qualily Department of
Environmental Quality Utah Waler Qualily Board Ground Water Discharge Permit. UGW370004,
for Denison Mines (USA) Corp. (hereafter "Permit"). Table 2 below compares lhe GWCL for
cadmium, iron, manganese, and nickel in Table 2 in Part C. I of the Permii wilh the detection limil
for method SW 6010B used by Lionville Laboratory. Based on this comparison in appears that
the detection limits were appropriate.
Table 2
Detection Limits
Parameter
Cadmium
Iron
Manganese
Nickel
'GWCL for
Class HI
Water
2.5
5,500
400
50
'SW6010B
Method
Detection
Limit
0.5
50
1
4
Detection
Limits Were
Appropriate
Yes
Yes
Yes
yes
L See page I of I Method Detection and Reporting Limils oflhe Inorganic Analysis Data
Package ofthe Lionville Laboratory Analyses Data Package (see Attachment I).
2. See Tabic 2 in Part C. 1 of the Permit
Verifying That Laboratory Control Samples (e.g., blind duplicates, field blanks, etc.) Were
Within Limits Specified In the QAP
Section 4.3.3 of the DUSA QAP, requires:
"4.3.3 Field Duplicates
One DupUcale set of samples submitted with each Batch (defined in Section 4.3.4) ofsainples
(OTG, Field and Laboratory Qtiality Assurance/Quality Control, 7.8), taken from one of fhe
wells being sampled and will he submiited to the Analytical Laboratory and analyzed for all
contaminants listed in Table 2 ofthe GWDP (EPA SW-846. Chapter /. .Section 3.4.1)."
Section 4.3.4 of the DUSA QAP, requires:
"4.3.4 Definition of "Batch"
For the purposes ofthis Plan, a Batch is defined as 20 or fewer samples (FA SW-846, Chapter
1, Section 5.0, page 23). "
DRC collected a duplicate sample for MW-32 and identified it as MW-99. This duplicate sample
was the only laboratory control sample the DRC submitted to the Laboratory for analysis, and was
sufficient to meet the DUSA QAP requiremenis listed above.
The Table 3 below compares the sample results for MW-32 with its duplicate sample results for
MW-99 using the relative percent difference (hereafter "RPD") equation found in the Guidance.
EPA guidelines which have been established for evaluating duplicate samples being analyzed by
the same laboratory have sel a criterion of 20% RPD (or less) as acceptable. Based on comparing
the sample result for MW-32 and MW-99, the RPD for each parameter is less than 20% and
therefore the analytical dala for these two samples arc acceptable.
Table 3
Comparing DRC Samples
Parameter
Cadmium
Iron
Manganese
Nickel
Concentration (pg/L)
MW-32
(DRC)
3.26
8330
5340
61.4
MW-99
(DRC Duplicntcof
MW32)
3.52
8490
5480
62.3
RPD%
7.7
1.9
2.6
1.5
Comments
Based on the Lionville Laboralory informalion provided above it is determined that the analytical
data for DRC water samples collect from well MW-32 and the duplicate sample for MW-32,
MW-99, qualifies to be compared against DUSA water sample from well MW-32.
DRC ys. DUSA Data Comparison-Non Radiological Parameters
Comparability of the DUSA and DRC laboratory results for non-radiologies was determined using
the RPD equation found in the Guidance. EPA guidelines which have been established for
evaluating contract laboratories have set a criterion of 20% RPD (or less) as acceptable. However,
the 20% RPD criterion was established for duplicate samples being analyzed by the same
laboratory. There are many more variables when analysis by 2 different laboratories is involved,
and consequently, the variability belween the two samples will be greater. Unfortunately, RPD
criteria are not available for this scenario. Precedent established by another Division in DEQ
allows a 30% RPD when comparing split sampling data between two separate laboratories. Using
this as a basis for the uranium mill split samples, an RPD of 30% or less will be acceptable and no
further evalualion will be required. When the RPD is greater than 30%, corrective action will be
required. The Table 4 below shows the RPD results for cadmium, iron, manganese, and nickel
between DRC MW-32 and DUSA MW-32. Il appears that all the RPD vaiues are below 30% and
are therefore considered comparable. Therefore, jt appears that the analytical results for the DRC
water sample from well MW-32 and the DUSA water sample from well MW-32 are
representative of the cadmium, iron, manganese, and nickel concentrations in the water from well
MW-32.
Table 4
RPD Results
Parameter
Cadmium
Iron
Manganese
Nickel
'GWCL
(Mg/L)
2.5
5,500
400
50
Concentration (pg/L)
MW-32
(DRC)
3.26
8330
5340
61.4
'MW-32
(DUSA)
2.61
9020
5590
59
RPD%
22.1
8.0
4.6
4.0
I <j WV. L ^ urounuwaicr yu:iiiiy t, ompjiance Limits luuiid in I anie l oi mc uuiA rcrmii
2. A copy of lhe iahocilory anal>liL-al report for Ul.'S.A sumple MW 32 can he seen in Ailachmenr 2, andcin also be found
lhe White Mcsd L'raniiim Mill Groundwater Monitoring Report 4* Ouarter (October through Decembet 2008).
SUMMARY
Based on the dala provided above, the results for both groundwater samples from DUSA MW-32
and from DRC MW-32 are comparable. No corrective action was needed under the Guidance.
In addition, concenirations of cadmium, iron, manganese, and nickel in the groundwater samples
for DUSA MW-32 and for DRC MW-32 exceeded GWCL set in Table 2 of Ihe DUSA Peimil.
Thus the reason for required accelerated monitoring as required in Part I.G. I of the Permit.
References
Denison Mines (USA) Corp., March 16, 2009, Revision 4, White Mesa Uranium Mill Ground
Water Monitoring Quality Assurance Plan
Denison Mines (USA) Corp., February 2009. White Mesa Uranium Mill Groundwater Monitoring
Report 4"' Quarter (October through December 2008)
Division of Radiation Control, August 7. 2007, Utah Departmeni of Environmental Quality
Division of Radiation Control Guidance for Groundwater Split Sampling Collection at Uranium
Mill Operations.
Division of Radiation Control, January 12, 2009, Memorandum, Subject: Field Inspection and
split sampling results for Groundwater Monitoring Groundwaier Inspection Module 61 at the
Denison Mines (USA) Corp. (DUSA) White Mesa Mill facilily near Blanding, Utah.
Division of Radiation Control, March 23, 2009, Memorandum, Subject: Review of the 3^
Quarter, 2008 (dated November 28, 2008) and 4'^ Quarter, 2008 (February 25, 2009), Routine
Groundwater Monitoring Reports, Groundwater Discharge Permit (Permit) UG370004, Denison
Mines (USA) Coip. (DUSA), White Mesa Mill, Blanding, Utah.
EPA, December 1996, Revision 6, EPA publication SW 846, entitled Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods.
Lionville Laboratory, March 26, 2009. Analyses Data Package
Slate of Utah, Department of Environmentai Quality, Division of Radiation Control, September
17, 2007, State of Utah Contraci, Contract # 086096
State of Utah Division of Water Qualily Departmeni of Environmental Quality Utah Water
Quality Board Salt Lake City, Ulah 84114-4870, March 17, 2008, Ground Water Discharge
Permii, UGW370004, for Denison Mines (USA) Corp.
^ ^
AUachment 1
Laboratory Analytical Report for DRC Samples M\V-32 and MW-99
ANALVSES DATA PACKAGE COVER PAGE
6010B
Laboratory: Lionville Laboralory
Client: Eberline Utah
SDG:
Projeci: Utah DRC
Client Sample Id:
MW-J2
MW-99
Lab Sample Id:
0812092-01
0812092-02
I certify that this data package is in compliance with the terms and conditions ofthe contract both technically and for completeness, for
other than the conditions detailed above. Release ofthe data contained in this hardcopy data package and in computeFreadable data
submined on diskette has been autorized by tlie Laboratory Manager or the Managers designee, as verified by the following signatures
Signature:
Date:
Iv^JL-Naine: -^g] t-n> t^ n i t ts
3>jSLU>lo'i Title: L-^^c/Y^crJi^^ m>L^^i-5^
• -5 ^•>
B8636S831
Page 1 of 1
TABLE OF CONTENTS
METALS Page
Cover Page 001
Table of Contents 002
Chain of Custody 003
Case Narrative 006
Inorganic Analysis Data Package 011
Raw Data 026
A. Metals by TCP 027
B. Mercur>' n/a
Digestion Log 106
002
ks/tc-tcmplaic
CUain ot custody
.i i
^ r
k
«:
s •9 «j
^
1<> te
1 k~
I
^9
i 1 Q.
9
o
D m
-(
^ n
3
5
3
JP.
5"
u
a
3 •
B Q.
D
a
o
H
•
>•
^>
=i
3?^
. .^"'
!!_< N
^--.
^ f=,^
^1
V
^
\
*i Si'
1^
-^^^5
^-
!&^ ^
o.
v^
l;
X
X
H
^
^
><
\
X
X
^t.
5?
o
I?
iff r
•7
'V^^AW
id
*0
0\
^-1
^1
8 III ri
1$
••. I
i^
s
*A •\
'^:i S ^i^^
^^>
i ^
^
3
?<-
:^-^^
b^
o r
tn Z 0>
it
D
i
VOA
BNA
Pest/
PCE
Harb
O-
S?^i-
¥
'^is
o o
3
r m
H
m
(0 z >
m
>
m
CA
3X.
O
O
c
o 0)
z -fc
3
IS-
<:> fi)
I
(D
c
(D
(A
-a u
CD
as
CO
O
r
Lioaville Laboratory Incorporattd
S.AMPLE RECEIPT CHECKLIST (SRC)
CLIENT. •' ^ -
Pmjcct/SA5/S0W/RtIcasc #:
LvLI Batch #: d^lXi 09^ Sample Custodian
••^.//. -JS^^C^
WOTE: EXPLAIN ALL DISCREPANCIES T
1. Samples Hand De'ivsrtd or Shjppedj)
2. Custody ScaJs on cooltrs or shipping
tontaintr? ir.lact, signed Sc dated?
3. Ouisidc of coohrs or shi ppin g^ conuin ers ziz
free from daniage?.;
4. /Jl cxDCcted paperwork rtcelvtd {coc &
othtr client specific infonnatioD'} scaled in
plactic bag and easily accessible?
5. Samples received cooled or ambient?
How was the temperature taken?
Is the Temp. Crittria met for these samples?
(Hg in soils @4°C)
6. Custody seals on sample contzinen iniart,
signed and dated?
7. COC (Client & LvLI) signed & dated?
S. Sample containers arc intact?
9. All samples on COC received?
All samples received on COC?
10. Ail sample label informalion matches COC?
11. Samples properly preserved? (If #5 is no,
then this is no.)
11. Samples received v/ithin hold times?
Short holds taken to wet lab?
tarVOA^rOC, TOX free of headspace?
1 i. QC rJckcrs placed on bottles designated
by client?
)5. Shipment meets LvLI Sample .Axccptance
Policy? (Identify all bottles that do not meet
the policy, which is on the reverse ofthis page.]
16. Project Manager contacted concerning any
discrepancies?
Person Ccirtaotcd ^j • S7?jJ€
Carrier Ui^S (^ct,l^/uJi AWdi# ^i:U^^d ^-^^-^
DYes
R^t
^^ Ycs
Temp
a^es
^'
• Yci
D No d-HlirS^als
DKo Ccmme.nLs:
"C Cooler #
^0Tcnip. BXank • D Other (Specify):
DMo
DNo n No Seals;:.
c/fes
aya
a Yci
a^ci
a Yes
[>?«
• Yes
DNo
ONo
DNo
QND
• No
DNo
DNo
DNo
DND
DNo
O-WM.
ayi/.'K
pi^
DNo DNM.
p^^= /.^-/f-rj^_
BS^S^SS
Case
Narrative
\
\
\
A
264 Weisn Pool Road
L:^tC:;. h'entiiyij'di-iij 1ij341
Fax {6101 280-3041
Case Narrative
Client: EBERLINE-UTAH
LVL#: 0812092
METALS
W.O.#: 11343-001-9999-00
DateReceived: 12-18-08
The following is a suinmary of the QC results accompanying the sample results. Lionville
Laboratory (LvL) certifies that all test results meet the requirements of NELAC except as noted
below.
1. Tliis narrative covers the analyses of 2 waler samples.
2. The sample was prepared and analyzed in accordance with SW-846 protocol and reported
with CLP deliverable. The samples were not preconcentrated at digestion as per 200.7
method.
3. All analyses were performed within the reqiiired holding times.
4. Please refer to the Sample Receipt Check List for sample discrepancies in LvLl's sample
acceptance policy.
5. All Initial and Continuing Calibration Verifications (ICV/CCVs) were within control Umits.
6. All Initial and Continuing Calibration Blanks (ICB/CCBs) were within method criteria.
7. All preparation/method blanks were within method criteria.
8. All ICP Interference Check Standards were within control limits.
9. All laboratory control samples (LCS) were witiiin the 85-115% control limits.
10. The serial dilution percent differences were within SW-846 control limits.
11 The matrix spike (MS) recovery for 1 analyte was outside the 70-130% control limits.
12. For anal>-tes where the MS is out of control, a post-digestion MS (PDS) is performed. A
serial dilution is performed for Mercury. A PDS was prepared at meaningful concentration
levels.
13. The duplicate analysis was within the 20% Relative Percent Difference (RPD) control
limits.
r •5liaic'jneials-.packaces'cbCTlme_u(nh\ml2 ~ 0 92 . dOC
The resuks presented in this repon relate only to lhe aiidl^iiea! testing and cnndilions ofthe samples nl receipt and during; storatie All pages of thi:> ii^port are intcjjial pans ofthe analytical
14. LvL is NELAP accredited by the State of Pennsylvania. For a complete hsting of
accrediting authorities and the corresponding analytes/mcthods, please contact your Pioject
Manager.
'aniei
.awiratory Manager
Lionville Laboratory
Date
alm/ml2-092
BSsggessB
METALS METHOD GLOSSARY
The following methods are used as reference for the digestion and analysis of samples contained within this
Leachina Procedure: 1310 131] 1312 Olher:
CLP Metals Digestion and Analysis Methods: _ILM03.0 __ILM04.0
Metah Digestion Methods: ^3005A _30JOA _3015 __3020A _3050B _3051 _200.7 _SS17
Other:
MetaJs Analysis Methods
Aluminum
Antimony
Arsenic
Barium
Beryllium
Bismuth
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Lithium
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Rare Earths
Selenium
Silicon
Silica
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Uranium
Vanadium
Zinc
Zirconium
Other:
S\V846
_6010B
601 OB 7041 >
601 OB 7060A'
6010B
_6010B
_6010B'
^OlOB
TeOJOB 7131A'
6010B
6010B 7191*
601 OB
_6010B 7211^
TeOlOB
6010B 7421 *
6010B 7430-
601 OB \
7601 OB \
7470A^ 7471A^
__6fll OB
J^OIOB
6010B 7610 *
_6010B'
601 OB 7740 =
_6010B'
6010B
60I0B 7761'
601 OB 7770-
601 OB
_6010B __7841^
601 OB
6010B
601 OB >
601 OB
601 OB
601 OB '
EPA STD MID
200.7
200.7 204.2
200.7 206.2 3113B
200.7
200.7
200.7 •
200.7
200,7 213.2
200.7
200.7 218.2
200.7
200.7 220.2
200.7
200.7 239.2 3113B
200.7
200.7
200.7
245.1' 245.5'
200.7
200.7
200.7 258.1 *
200.7 •
200.7 270J SnSB
200.7
200.7
200.7 272.2
200.7 273.r
200.7
200.7 279.2 200.9
_^200.7
200.7
200,7 '
200.7
200.7
200.7 '
Method:
F.PA
OSWR
1620
1620
_1620
1620
1620
__1620
1620
USAIHAMA
—99
_99
99
99
99
99
99
99
__99
SS17
99
99
99
99
99
99
99
_99
99
__99
99
_?9
99
99
99
99
99
_99
__99
99
99
99
99
99
_99
L-W14133/M-«3uQI
mBBBB^
264 Welsh Pod Roue.
cxtc-'P., Pennvyivar.u^ ''3341
Phone (610) ZBG-30C0
Fax [phone]
Inorganics Notes and Definitions
U
J
H
E
N
D
Dry
Wet
RPD
Indicates that the parameter was not detected at or above the reported limit.
Estimated concentration, concentration between the MDL and the MRL.
Holding time exceeded
Data associated with failed ICP serial dilution results
Spiked sample recovery not within control limits
Results reported from a dilution; related reporting limits are elevated due to
the presence of an interference or a high Target value
Replicate analysis not within control limits
Sample results reported on a dry weight basts
Sample results reported on a wet weight (as received) basis
Relative Percent Difference
r.';;roupd.Ma^0C'?jiiorL;anjcjicies_(lcfiniliDns_0j0.^L'9.c]oiesiDcfinniiiiisdn-
5^36eeiQ
Inorganic Analysis Data Package
VLI
8^^sn
INORGANIC ANALVSIS DATA SHEET
6010B MW-32
Laborator>'
Client
Matrix
Sampled
Solids
Batch
Lionville Laborator>'
Eberline Utah
Water
12/09/08 11:00
Laboratoi^ ID: 0812092-01
SDG:
Project: Utah DRC
File ID: ICPO225A-0I8
0.00
L902152 Sequence:
Prepared: 02/23/09 09:07 Analyzed: 02/25/09 12:08
Preparation: SW 300.^A Initial/Final: 50mL/50mL
9030034 Calibration: UNASSIGNED Instrument Thermo iTEVA
CAS NO.
7440-43-9
7439-89-6
7439-96-5
7440-02-0
Analyte
Cadmium
Iron
Manganese
Nickel
Concentration
3.26
8330
5340
61.4
Dilution
Factor
1
1
I
I
Q Method
60 JOB
601 OB
601 OB
601 OB
Page I of2
atKw^oii:.
INORGANIC ANALYSIS DATA SHEET
6010B MW-99
Laboratory
Client
Matrix
Sampled
Solids
Batch
Lionville Laboratory
Eberline Utah
Water
] 2/09/08 10:00
0.00
L902152
SDG:
Project: Utah DRC
Laborator>'ID: 0812092-02 File ID
Prepared: 02/23/09 09:07 Analyzed
Preparation: SW 3005A InitiaLfinai
Sequence: 9030034 Calibration: UNASSIGNED
1CP0225A-Q24
02/25/09 12:55
5QniL/50mL
Instrument: Thenno ITEVA
CAS NO.
7440-43-9
7439-89-6
7439-96-5
7440-02-0
Analyte
Cadmium
Iron
Manganese
Nickel
Concentration
(ug/L)
3.52
8490
5480
62.3
Dilution
Factor
1
1
1
1
Q Method
601 OB
601 OB
601 OB
601 OB
1
Page 2 of2
898668813
INITIAL AND CONTINUING CALIBRATION CHECK
601 OB
Laboratory: Lionville Laboratory SDG:
Client: Eberline Utah Projeci: Utah DRC
Instrument ID: Thermo ITEVA Calibration: UNASSIGNED
Control Limt: +/- 10.00% Sequence: 9030034
Lab Sample ID
9030034-lCVl
9030034-CCVl
9030034-CCV2
9030034-CCV3
9030034-CCV4
Analyte
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Cadmium •
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
True
375.00
3750.0
3750.0
375.00
500.00
5000.0
5000.0
500.00
500.00
5000.0
5000.0
500.00
500.00
5000.0
5000.0
500.00
500.00
5000.0
5000.0
500.00
Found
374
3810
3790
376
500
5080
5020
503
499
5050
5080
504
506
4990
5090
506
501
4960
5130
506
%R
100
IOI
101
100
100
102
100
101
100
101
102
IOI
101
100
102
101
IOO
99
103
101
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l..
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Method
601 OB
601 OB
601 OB
601 OB
601 OB
601 OB
601 OB
60108
601 OB
601 OB
601 OB
601 OB
601 OB
60108
601 OB
601 OB
601 OB
601 OB
6010B
60108
* Values outside of QC limits
Page I of 1
6898^814
Laboratory: Lionville Laboratory
Client: Eberline Utah
Instrument ID: Thermo iTEVA
Sequence: 9030034
CRDL STANDARD
6010B
SDG:
Project: Utah DRC
Calibration: UNASSIGNED
Lab Sample ID
9030034-CRLl
9030034-CRL2
Analyte
Cadmium
Cadmium
Iron
Iron
Manganese
Manganese
Nickel
Nickel
Cadmium
Cadmium
Iron
Iron
Manganese
Manganese
Nickel
Nickel
True
20.000
20.000
200.00
200.00
200.00
200.00
20.000
20.000
20.000
20.000
200.00
200.00
200.00
200.00
20.000
20.000
Found
20.4
20.4
207
207
205
205
20.7
20.7
20.5
20.5
199
199
206
206
20.8
20.8
%R
102
102
104
104
103
103
103
103
102
102
99
99
103
103
104
104
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
QC Limts
50-150
50- 150
50- 150
50-150
50-150
50-150
50- 150
50- 150
50-150
50- 150
50-150
50-150
50-150
50-150
50-150
50-150
* Values outside of QC limits
Page 1 of
8868^915
BLANKS
6010B
Laboratory: Lionville Laboratorv
Client: Ebedine Utah
Instrument ID: Thermo iTEVA
Sequence: 9030034
SDG:
Project: Utah DRC
Calibration: UNASSIGNED
Lab Sample ID
9030034-ICBI
9030034-CCBl
L902152-BLK1
9030034-CCB2
9030034-CCB3
9030034-CCB4
Analyte
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Cadmium
Iron
Manganese
Nickel
Found
0.05
2.71
0.86
0.06
0.12
12.2
1.06
0.25
-0.03
18.2
0.82
4.03
0.06
1.10
0.76
0.05
0.11
1.82
0.73
0.15
0.05
5.75
2.42
0.12
MRL
3.00
500
5.00
20.0
3.00
500
5.00
20.0
3.00
500
5.00
20.0
3.00
500
5.00
20.0
3.00
500
5.00
20.0
3.00
500
5.00
20.0
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug'L
UgA.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
C
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Method
601 OB
601 OB
601 OB
601 OB
6010B
601 OB
601 OB
6010B
6010B
60108
601 OB
601 OB
60I0B
601 OB
601 OB
601 OB
601 OB
601 OB
601 OB
60108
601 OB
601 OB
601 OB
60108
* Result above Reponing Limit
Page 1 of 1
9633^16
ICP INTERFERENCE CHECK SAMPLE
601 OB
Laboratory: Lionville Laboratorv
Client: Eberline Utah
Instrument ID: Thenno iTEVA
Sequence: 9030034
SDG:
Project: Utah DRC
Calibration: UNASSIGNED
Lab Sample ID
9030034-IFAl
9030034-1 FBI
Analyte
Cadmium
Cadmium
Iron
Iron
Manganese
Manganese
Nickel
Nickel
Cadmium
Cadmium
Iron
Iron
Manganese
Manganese
Nickel
Nickel
True
0.0000
0.0000
200000
200000
0.0000
0.0000
0.0000
0.0000
1000.0
1000.0
40000
40000
500.00
500.00
1000.0
1000.0
Found
0.13
0.13
199,100.00
199,100.00
-2.29
-2.29
-6.88
-6.88
1,008.00
1.008.00
40,070.00
40,070.00
497.50
497.50
967.60
967.60
%R
100
IOO
101
101
100
100
100
100
97
97
Unils
ug'L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/'L
ug/L
ug/L
ug/L
ug/L
ug'L
ug/L
ug/L
u&'L
ug/L
* Values outside of QC limits
Page 1 of 1
6G8866617
MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY
60I0B MW-J2
Laboratory:
Clienl:
Matrix:
Batch:
Preparation:
Lionville Laboratoi-v
Eberline Utah
Water
L902152
SW 3005A
SDG:
Proiect: Utali DRC
Laboratorv' ID: L902I52-MS2
Initial/Final; 50niL/50mL
Source Sample Name: MW-32
COMPOUND
Cadmium
Iron
Manganese
Nickel
SPIKE
ADDED
(ug/L)
50.000
1000.0
500.00
500.00
SAMPLE
CONCENTRATION
(Ug-L)
3.26
8330
5340
61.4
MS
CONCENTRATION
(ug/L)
53.5
9530
6010
544
MS
REC. t!
101
119
134
97
QC
LIMITS
REC.
j?. 7-5-4^
^ 75 135
\k 75 125
'Z^::^5 135
^ Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
V
Page 1 of 1
8^^8919
POST DIGEST SPIKE SAMPLE RECOVERY
6010B
MW-32
Laboratory: Lionville Laboratory
Clienl: Eberline Utah
Matrix: Water
Batch: L902152
Preparation: SW 3005A
Source Sample Name: MW-32
SDG:
Project: Utah DRC
Laboratory ID: L902152-PS2
Lab Source ID: 0812092-01
Initial/Final: 5QmL/50mL
% Solids:
Analyte
Cadmium
Iron
Manganese
Nickel
Control
Limit
%R
0-200
0-200
0-200
0-200
Spike Sample
Result (SSR)
(ug/L)
109
10300
7350
161
Sample
Resuh (SR)
(ug/L)
3.26
8330
5340
61.4
Spike
Added (SA)
(ug/L)
2000.0
%R
IOI
* Values outside of QC limils
Page 1 of 1
96^66613
DUPLICATES
6010B
MW-32
Laborator>'
Client
Matrix
Batch
Preparation
Lionville Labornton,'
Eberline Utah
Water
L902152
SW J005A
Source Sample Natne: MW-32
SDG
Project
Laborator)' 1D
Lab Source ID
InitiaLFinal
% Solids
Utah DRC
L902152-DUP2
0812092-01
50mL.'50mL
ANALYTE
Cadmium
Iron
Manganese
Nickel
CONTROL
LIMIT
20
20
20
20
SAMPLE
CONCENTR.\TION
(ug/L)
3.26
8330
5340
61.4
C DUPLICATE
CONCENTRATION
(ug/L)
3.38
8440
5380
62.2
C RPD
%
4
1
0.7
1
Q
METHOD
601 OB
601 OB
fiOlOB
60] ou
* Values outside of QC limits
'' Values Less Than Reporting Limit
Page 1 of 1
LCS / LCS DUPLICATE RECOVERY
6010B
Laboratory:
Client:
Matrix:
Batch:
Preparation:
Lionville Laboratorv
Eberline Utah
Water
L902152
SW 3005A
SDG:
Project: Ulah DRC
Laborator)' ID: L902152-BS1
InitiaL'Final: 50mL/50mL
COMPOLFND
Cadmium
Iron
Manganese
Nickel
SPIKE
ADDED
(ug/'L)
250.00
5000.0
750.00
2000.0
LCS
CONCENTRATION
(ug.'L)
245
4950
758
1990
LCS
%
REC. ^
98
99
IOI
100
QC
LIMITS
REC.
* .«e—t^
J 80 120
^ .80 UQ
ft Column to be used to llai? recoverv- and RPD values with an asterisk
* Values outside of QC limits loon D-C uvivtk
Page 1 of 1
ee^s
SERIAL DILUTION
60108
MW-32
Laboralory: Lionville Laboratorv
Clienl: Eberline Utah
Matrix: Water
Sequence: 9030034
Preparation: L9Q21 52
Source Sample Name: MW-J2
SDG:
Project: Utah DRC
Laboratorv' ID: 90J0034-SRD2
Lab Source ID: 0812092-01
Initial/Final: 50. 50
% Solids:
* Values outside of QC limits
Analyte
Cadmium
Iron
Manganese
Nickel
Initial Sample
Result (I)
3.26
8330
5340
61.4
C
Serial
Dilution
Result (S)
3.77
8680
5620
66.1
C
%
Difference
Q
14 % r'
4
5
7
Method
601 OB
601 OB
601 OB
601 OB
QC Limits
°/b
Difference
10
10
10
!0
^
*
LH
Page 2 of 3
METHOD DETECTION AND REPORTING LIMITS
601 OB
Laboratory: Lionville Laboratory
Client: Eberline Utah
Matrix: Water
SDG:
Project: Utah DRC
Instrument: Thermo iTEVA
Analyte
Cadmium
Iron
Manganese
Nickel
MDL
0.500
50
1
4
MRL
3
500
5
20
Units
ug/L
ug/L
ug/L
ug/L
Page 1 of I
S6^S9623
PREPARATION BATCH SUMMARY
60108
Laboratory: Lionville Laboratorv
Client: Eberline Utah
Batch: L902152 Batch Matrix: Water
SDG:
Project:
Preparation:
Utah DRC
SW 3005A
SAMPLE NAME
MW-32
MW-99
Blank
LCS
MW-32
MW-32
MW-32
LAB SAMPLE ID
0812092-01
0812092-02
L902152-BLK1
L902152-BS1
L902152-DUP2
L902152-MS2
L902152-PS2
LAB FILE ID
ICP0225A-018
ICP0225A-024
ICP0225A-012
ICP0225A-032
ICP0225A-020
ICP0225A-021
1CP0225A-036
DATE PREPARED
02/23./09 09:07
02/23/09 09:07
02/23/09 09:07
02.23/09 09:07
02/23/09 09:07
02/23/09 09:07
02.'23/09 09:07
OBSERVATIONS
unpreseved, pres. on 2 '20/09
unpreseved, pres. on 2/20/09
Page 1 of
898998824
ANALYSIS BATCH (SEQUENCE) SUMMARY
6010B
Laboratory:
Client:
Sequence:
Matrix:
Lionville Laboratory
Eberline Utah
9030034
Water
SDG:
Project:
Inslrument:
Calibration:
Utah DRC
Thermo ITEVA
UNASSIGNED
Sample Name
Cal Standard
Cal Standard
Cal Standard
Initial Cal Check
Initial Cal Blank
MRL Check
Interference Check A
Interference Check B
Calibration Check
Calibration Blank
Blank
Serial Dilution
MW-32
MW-32
MW-32
MW-32
Calibration Check
Calibration Blank
MW-99
Serial Dilution
LCS
Calibration Check
Calibration Blank
MW-32
MRL Check
Calibration Check
Calibration Blank
Lab Sample ID
9030034-CALl
9030034-CAL2
9030034-CAL3
9030034-ICVl
9030034-ICBI
9030034-CRLl
9030034-IFAl
9030034-lFBI
9030034-CCVl
9030034-CCBl
L902I52-BLK1
9030034-SRX)l
0812092-01
9030034-SRD2
L902152-DUP2
L902152-MS2
9030034-CCV2
9030034-CCB2
0812092-02
9030034-SRD3
L902152-BS1
9030034-CCV3
9030034-CCB3
L902152-PS2
9030034-CRL2
9030034-CCV4
9030034-CCB4
Lab File ID
1CP0225A-001
ICP0225A-002
ICP0225A-003
1CP0225A-005
1CPO225A-006
ICP0225A-007
ICP0225A-008
ICP0225A-009
ICP0225A-0I0
1CP0225A-011
1CP0225A-012
1CP0225A-014
ICP0225A-018
1CP0225A-019
1CP0225A-020
ICP0225A-02I
1CP0225A-022
ICP0225A-023
ICP0225A-024
ICP0225A-026
ICP0225A-032
ICP0225A-034
ICP0225A-035
ICP0225A-036
ICP0225A-038
ICP0225A-039
ICP0225A-040
Analysis Dale/Time
02/25/09 10:01
02/25/09 10:08
02/25/09 10:15
02/25/09 10:30
02/25/09 10:38
02/25/09 10:45
02/25/09 10:52
02/25/09 10:59
02/25/09 11:07
02.'25/09 11:14
02/25/09 11:21
02/25/09 11:37
02/25./09 12:08
02/25/09 12:16
02/25/09 12:23
02./25/09 12:31
02/25/09 12:40
02/25/09 12:48
02/25/09 12:55
02/25/09 13:10
02/25/09 13:57
02/25.'O9 14:13
02/25/09 14:22
02/25/09 14:29
02/25/09 14:44
02/25/09 14:51
02/25/09 14:59
Page 1 of
S66^^Z5
Raw Data
vLI
yiiaiwiiigtMioiitmiaKC.
889^9829
Metals By ICP
VL/,
BS&BBBSZ
f tiowviiictiUOMrORirihC
t
Sample Name: SEQ-CAL1 Acquired: 2/25/2009 10:01:52 Type: Cal
Method: METHOD DVP{v114) Mode: IR Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom 1D3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
J Ag3280
Cls/S
.0000
.000
329.7
.0000
.0000
.0000
Be3t30-2
Cts/S
-.0008
.0002
21.53
-.0010
-.0007
-.0008
All 670
Cts/S
.0001
.0000
16.32
.0001
.0001
.0001
Bi2230
Cls/S
-.0002
.0001
31.57
-.0002
-.0001
-.0002
v/
A]3g61
OS'S
-.0007
.0004
62.60
-.0011
-.0006
-.0003
J
Ca317g Cts/S
.0067
.0001
1.690
.0068
.0067
.0066
J As1890
Cts/S
-.0001
.0000
1.813
-.0001
-.0001
-.0001
Ca3933
Cts/S
.0168
.0004
2.130
.0165
.0168
.0172
B 2089
Cts/S
.0002
.0000
2.802
.0002
.0002
.0002
Cd2283
Cta/S
.0004
.0000
1.941
.0004
.0003
.0004
y
Ba4554 Ba4554-2
Cts/S
.0013
.0001
7.400
.0013
.0012
.0013
s/
Co2286 Cts/S
-.0002
.0000
9.409
-.0002
-.0002
-.0002
Cts/S
.0042
.0001
3.488
.0044
.0041
.0042
Cr2677^
Cts/S
.0001
.0000
23.90
.0001
.0001
.0001
Be2348 Be234&-2
Cts/S
.0000
.000
37.81
.0000
.0000
.0000
Cu2178
Cts/S
.0000
.000
82.77
.0000
-.ooot .0000
Cts/S
.0001
.0001
66.44
.0002
.0000
.0002
Cu2199
Cts^S
.0000
.0001
113.2
.0000
.0001
.0001
Be3130
Cts/S
-.0013
.0000
1.883
-.0012
-.0013
-.0013
Cu3273
Cts/S
-.0011
.0002
18.15
-.0012
-.0013
-.0009
2/25/2009 13:52:10
2
Sampte Name; SEQ-CAL1 Acquired; 2/25/2009 10.-0l;52 Type; OsA
Method: METHOD DVP(v114) Mode: IR Corr. Factor: 1.000000
User: admin Custom IDt: Custom ID2: Custom (D3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
EJem
Units
Avg
Stddev
%RSD
#1
#2
#3
->
Fe2599^
Cts/S
.0000
.000
219.0
.0000
OOOO
-.0002
* Ni2316^
Cts/S
-.0003
.0000
15.23
-.0002
-.0003
-.0002
Fe2714
Cis/S
.0000
.000
39.76
.0000
-.0001
.OOOO
P 1774
Cls/S
.0001
.0000
8.059
.0001
.0001
.0001
y K 7664^
Cts/S
.0025
. .0009
35.40
.0031
.0015
Li6707
Cts/S
.0017
.0004
23.06
.0021
.0015
.0028 .0014 ,
Pb2203 Sb2068
Cts/S
-.0002
.0001
31.09
-.0002
-.0002
-.0003
v3
Cts/S
.0000
.000
92.63
.0000
.0000
-.0001
^
•^^
J Mg2790
Ct^S
-.0001
.0001
101.6
-.0001
.0000
-.0001
Sel960
Cts/S
.0000
.000
62.65
.0000
-.0001
.0000
1
-^
g^
Mg2652
Cts/S
-.0003
.0002
63.06
-.0004
-.0005
-.0001
SJ2124
Cts/S
.0005
.0000
3.646
.0005
.0005
.0005
'^^
Mn2576
Cta/S
.0000
.000
120.3
-.0001
.0000
-.0001
Si2124-2
Cts/S
.0001
.0000
16.90
.0001
.0000
.0001
1^^ O-^^^."-"^
-^^
^
Mn2576-2
Cts/S
-.0001
.0001
114.7
-.0002
.0000
-.0002
Sn1899
Cts/S
.0000
.000
203.6
.0000
.0000
.0000
Mo2020
Cls/S
.0000
.0000
269.4
.0000
.0000
.0000
Sr2165
Cts/S
-.0003
.0000
11.44
-.0002
-.0003
-.0003
c \/ Na5895 ^
Cts/S
-.0033
.0001
3.808
-.0033
-.0034
-.0031
Sr4215
Cts/S
-.0007
.0001
20.63
-.0007
-.0005
^ -.0008
-3-C?or2-5Tt
i T^
-0-2.
Sample Name: SEOCALI Acquired: 2/25/2009 10:01:52 Type: Cal
Method: METHOD DVP(v114) Mode: IR Con". Factor: 1.000000
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Custom IDI:
Th2837
Cts/S
.0001
.0000
35.44
.0001
.0001
.0002
Zr339l
Cls/S
.0002
.0000
A.672
.0002
.0002
.0002
Ti3349
Cts/S
.0001
.0000
28.39
.0001
.0001
.0001
Zr3391-2
Cts/S
.0002
.0000
20.92
.0003
.0002
.0002
Custom ID2:
Ti334&-2
Cls/S
.0003
.0001
41.54
.0004
.0002
.0003
Custom IDS:
y
TI1908 U 2635
Cts/S Cls/S
-.0001 -.0001
.0000 .0000
33.69 14.91
-.0001 -.0001
.0000 -.0001
-.0001 -.0001
U 3854
ClS/S
.0005
.0000
9.327
.0004
.0005
.0005
U 4090
Cts/S
.0000
.000
472.9
.0000
.0000
oooo
y
V 2924 Zn2138
Cts/S Cts/S
.0002 .0008
.0000 .0000
32.73 2.007
.0001 .0008
.0001 .0008
.0002 .0009
v/
Zn213e-2
Cls/S
.0001
.0000
13.01
.0001
.0001
.0000
2/25/2009 13:52:10
4
Sample Name: SEOCALI Acquired: 2/25/2009 10:01:52 Type: Cal
Method: METHOD DVP(v114) Mode: IR Con". Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment:
Int. Std. Y_2243 y_3600 Y_3710
Units Cls/S Cls/S Cts/S
Avg 25018. 172510. 17613.
Stddev 158. 1652. 63.
%RSD .63029 .95752 .35689
#1 25199 174020. 17544
#2 24909. 172770. 17667.
#3 24947. 170750. 17627.
RRS9g88e5
Sample Name: SEQ-C<AL2 Acquired. 2/25/2009 10:08:46 Type: Cal
Method: METHOD 0VP(v114) Mode: IR Corr. Faclor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Ag3280
Cls/S
.0831
.0007
.8030
.0832
.0824
.0337
812230
Cts/S
.0329
.0001
.3502
.0328
.0331
.0329
All 670
Cts/S
.8360
.0033
.3986
.8325
.8391
.8365
Ca3933
Cts/S
U.44
.01
.1064
11.46
11.44
11.44
AS1890
Cts/S
.0256
.aaoz
.6941
.0256
.0260
.0259
Cd2288
Cls/S
.5170
.0020
.3917
.5150
.5191
.5169
B 2089
Cts/S
.1096
.0005
.4595
.1091
.1101
.1095
Co22a6
Cts/S
.3272
.0015
.4510
.325S
.3287
.3273
Ba4554
Cls/S
2.802
.030
1.076
2.828
2.769
2.810
Cr2677
Cls/S
.0773
.0007
.9231
.0732
.0770
.0784
Ba4554-2
Cts/S
1.003
.005
.4950
1.005
1.008
.9979
Cu2178
Cls/S
.0257
.0002
.6318
.0255
.0259
.0257
Be2348
Cts/S
.4017
.0037
.9191
.4022
.3978
.4052
Cu2199
Cts/S
.0460
.0002
.3289
.0459
.0461
.0459
Be234S-2
Cts/S
.2868
.0007
.2377
.2874
.2861
.2868
Cu3273
Cls/S
.0Z9Q
.0003
.8885
.0297
.0302
.0299
Be3130
Cts/S
2.311
.035
1.494
2.331
2.272
2.332
Fe2714
Os/S
.0390
.0003
.8754
.0391
.0386
.0393
Ba3130-2
Cts/S
1.157
.001
.0433
1.157
1.157
1.158
Li6707
Cts/S
T.S96
.003
.1812
1.896
1.900
1.893
2/25/2009 13:52:10
2
Sample Name: SEQ-CAL2 Acquired; 2/25/2009 tO;08;46 Type; Cal
Method: METHOD DVP(v114) Mode: IR Con". Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Mg2852
Cls/S
.5417
.0029
.5416
.5402
.5451
.5398
Sr4215
Cts/S
1.240
.005
.3935
1.243
1.242
1.234
Mo2020
Cts/S
.1313
.0007
.5674
.1305
.1320
.1313
Ti3349
Cts/S
.2386
.0021
.8748
.2390
.2366
.2408
Ni2316
Cts/S
.1876
.0008
.4298
.1869
.1885
.1875
Ti3349-2
Cts/S
.1033
.0002
.2095
.1036
.1032
.1033
Pb2203
Cts/S
.0508
.0002
.3289
.0507
.0510
.0507
Til 908
Ota's
.0216
.0001
.5376
.0214
.0217
.0216
Sb2068
Cts/S
.0267
.0001
.5274
.0266
.0269
.0268
Zn2138
Cts/S
.5035
- .0021
.4200
.5014
.5056
.5035
Sel960
Cts/S
.0147
.0001
.8440
.0145
.0148
.0147
Zn2138-2
Cts/S
.0533
.0002
.3993
.0531
.0534
.0535
Si2124
Cts/S
.0295
.0001
.3769
.0294
.0296
.0296
Si2124-2
Cts/S
.0026
.0000
.4702
.0026
.0026
.0026
Sn1899
Cts/S
.0746
.0004
.4894
.0743
.0750
.0745
Sr2165
Cts/S
.1849
.0006
.3186
.1844
.1856
.1349
SS^S5S38
Sample Name: SEQ-CAL2 Acquired: 2/25/2009 10:08:46 Type: Cal
Method: METHOD DVP{v114) Mode: IR Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std. Y_224S Y_3600 Y_3710
Units Cts/S Cts/S Cts/S
Avg 24857. 170220. 17753.
Stddev 58. 1575. 63.
%RSD .23509 .92499 .35589
#1 24897. 169640. 17819.
#2 24790. 172000. 17693.
#3 24883. 169020. 17747.
83^38931
Sample Name: SEQ-CAL3 Acquired; 2/2E*/2009 10:15:46 Type: Cal
Meihod: METHOD DVP(v1l4) Mode: IR Con. Factor; 1.000000
User admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Inl. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
A1S961
Cts/S
2.027
.005
.2389
2.024
2.025
2.033
Y 3600
Cts/S
165140.
873.
.52879
164710.
164570.
166150.
Ca3179
Cls/S
2.313
.004
.1562
2.316
2.309
2.314
Y 3710
Cts/S
17806.
48.
.27097
17843.
17823.
17752.
Fe2599
Cis/S
1.461
.002
.1270
• 1.462
1,459
1.461
K 7664
Cts/S
1.191
.002
.1778
1.193
1.189
1.191
Mg2790
Cls/S
.2274
.0006
.2534
.2281
.2271
.2271
Mn2576
Cls/S
3.592
.030
.8379
3.592
3.622
3.561
Mn2576-2
Cls/S
1.677
.002
.1040
1.678
1.678
1.675
Na5895
Cts/S
2.253
.001
.0298
2.253
2.252
2.253
V 2924
Cts/S
.6465
.0029
.4562
.6498
.6441
.6457
88^^932
Sample Name: SEQ-CAL4 Acquired: 2/25/2009 10:22:53 Type: Cal
Method: METHOD DVP(v114) Mode; IR Cor. Factor: 1.000000
User; admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
n2 #3
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
P 1774
Cls/S
.0490
.0002
.4184
.0490
.0492
.0488
Y 2243
Cts/S
25655.
39.
.15034
25691.
25614.
25660.
Th2837
Cts/S
.0376
.0002
.5902
.0378
.0374
0378
Y 3600
Cts/S
175460.
478.
.27240
175100.
176000.
175270.
U 2635
Cls/S
.0033
.0000
.6316
.0033
.0033
.0033
Y 3710
Cts/S
18569.
139.
.74677
1B500.
18478.
18728.
U 3854
Cls/S
.0104
.0001
.9028
.0104
.0103
.0105
U 4090
Cts/S
.0108
.0001
.5588
.0109
.0108
.0108
Zr3391
Cls/S
.4912
.0024
.4846
.4929
.4885
.4921
ZrS391-2
Cts/S
.2114
.0010
.4515
.2119
.2121
.2103
89^35933
Sample Name: 1CV1 Acquired; 2/25/2009 10;30;37 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Corr. Fartor: 1.000000
User; admin Custom IDI; Custom ID2: Custom IDS:
Comment;
ustom
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Ag3280
ppb
363.4
1.9
.5252
365.4
361.7
362.9
Chk Pass
Be31S0-2
ppb
374.7
1.3
.3422
373.4
376.0
S74.7
Chk Pass
All 670
ppb
F4183.
11.
.2746
4188.
4191.
4170.
Chk Fail
3750.
10.00%
Bi22S0
ppb
381.6
2,2
.5654
383,3
382,2
379,2
Chk Pass
AI3961
ppb
37S4.
16.
.4272
3736.
3768.
3756.
Chk Pass
Ca3179
ppb
1517.
2.
.1246
J517.
1515.
1519.
Chk Pass
AS1890
ppb
370.3
1.4
.3732
370.1
371.8
369.1
Chk Pass
Ca3933
ppb
1511.
2.
.1412
1510.
1513.
1509.
Chk Pass
B_2089
ppb
370.1
1.2
.3249
371.3
370.0
S68.9
Chk Pass
Cd2288
ppb
374.4
1.0
.2790
375.6
374.2
373.6
Chk Pass
Ba4554
ppb
392.7
2.5
.6360
395.1
390.2
392.8
Chk Pass
Co2286
ppb
375.0
.9
.2330
375.9
375.0
374.2
Chk Pass
B34554-2
ppb
377.9
.9
.2403
377.2
378.9
377.6
Chk Pass
Cr2677
ppb
377.3
3.3
.8668
330.8
374.3
376.7
Chk Pass
Be2348
ppb
370.0
2.8
.7452
372.7
367.2
370.1
Chk Pass
Cu2178
ppb
378.4
.1
.0343
378.5
378.3
378.5
Chk Pass
Be2348-2
ppb
373.1
.9
.2451
374.0
373.1
372.1
Chk Pass
Cu2199
ppb
376.9
.7
.1875
376.3
377.7
376.7
Chk Pass
Be3130
ppb
377.4
S.2
.8437
S80.7
374.4
377.1
Chk Pass
Cu3273
ppb
378.0
5.8
1.53S
383.1
371.7
379.1
Chk Pass
2/25/2009 13:52:11
2
Sample Name: tCVl Acquired: 2/25/2009 10:30:37 Type: QC
Meihod: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User; admin Custom IDI: Custom ID2: Custom 1D3;
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#S
Check?
Value
Range
Fe2599
ppb
3806.
12.
.3116
3796.
3819.
3804.
Chk Pass
Ni2316
ppb
376.5
.6
.1704
377.1
376.7
S75.8
Chk Pass
Fe2714
ppb
3781.
40.
1.060
3821.
3741.
3782.
Chk Pass
P_1774
ppb
783.6
2.6
.3359
785.1
785.0
780.5
Chk Pass
K_7664
ppb
3725.
19.
.5174
3740,
3731.
3703.
Chk Pass
Pb2203
379.7
1.0
.2714
380.7
379.7
378.6
Chk Pass
Li6707
ppb
3054.
2.
.0546
3055.
3055.
3052.
Chk Pass
Sb2063
ppb
375.9
.7
.1966
376.4
376.4
375.1
Chk Pass
Mg2790
ppb
3072.
20.
.6653
3068.
3095.
3054.
Chk Pass
Sel960
ppb
367.7
.4
,1105
368.2
367.4
367.6
Chk Pass
Mg2852
ppb
3048.
12.
.4089
3034.
3052.
3058.
Chk Pass
Si2124
ppb
397.2
1.2
.2934
397.9
397.8
395.8
Chk Pass
Mn2576
ppb
3853.
23.
.5887
3871.
3828.
3862.
Chk Pass
Si2124-2
ppb
400.6
4.0
1.001
396.2
401.6
404.0
Chk Pass
Mn2576-2
ppb
3791.
10.
.2637
3791.
3801.
3781.
Chk Pass
Sn1899
ppb
372.8
.9
.2530
373.2
373.4
371.7
Chk Pass
Mo2020
ppb
371.6
1.4
.3739
372.3
372.5
370.0
Chk Pass
Sr2165
ppb
373.4
1.2
.3345
374.8
372.6
372.7
Chk Pass
Na5895
ppb
3788.
20.
.5325
3809.
3785.
3769.
Chk Pass
Sr4215
ppb
377.9
1.0
.2723
378.2
373.7
376.7
Chk Pass
9^898934
Sample Name: ICVl Acquired: 2/25/2009 10:30:37 Type: QC
Mathod: METHOD DVP(v114) Mode: CONC Con. Faclor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2837
ppb
754.7
7.5
.9924
763.0
748.4
752.7
Chk Pass
2r3391
ppb
761.8
4.3
.5689
765.5
757.0
762.8
Chk Pass
Ti3349
ppb
369.2
2.3
.6304
371.2
366.7
369.8
Chk Pass
Zr3391-2
ppb
767.3
7.1
.9239
766.0
774.9
760.9
Chk Pass
TiSS49-2
ppb
370.1
3.6
.9814
374.3
368.4
367.6
Chk Pass
Til 908
ppb
371.8
2.6
.7030
372.7
373.9
368.9
Chk Pass
U_2635
ppb
968.4
15.0
1.550
976.9
977.2
951.0
Chk Pass
U_3854
ppb
F 845.8
45
.5339
849.4
840.8
847.3
Chk Fail
1000.
-10.00%
U_4090
ppb
1060.
17.
1.622
1080.
1050.
1051.
Chk Pass
V_2924
ppb
3709.
20.
.5467
3728.
3688.
3711.
Chk Pass
Zn2138
ppb
375.2
.7
.1943
376.0
375.0
374.6
Chk Pass
Zn2138-2
ppb
372.4
1.4
.3687
371.0
372.5
373.7
Chk Pass
2/25/200913:52:11
4
Sample Name: ICVl Acquired: 2/25/2009 10:30:37 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con". Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Coniment:
Int. Std.
Unils
Avg
Stddev
%RSD
Y 2243
Cts/S
25331.
94.
.37052
Y 3600
Cls/S
173130.
640.
.36971
Y 3710
as/s 18632.
27.
.14518
#1
#2
#3
25227. 172820. 18663.
25356. 173860 18617
25409. 172700. 18615.
Sample Name: CCB Acquired: 2/25/2009 10:33:06 Type: QC
Method: METHOD DVP{v114) Mode; CONC Con-. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment: J
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Ag32eO
ppb
.7556
.5223
69.13
1.051
1.063
.1525
Chk Pass
Ee3130-2
ppb
.0310
,0320
103.2
.0614
.0341
-.0024
Chk Pass
Alt 670
ppb
3.016
1.215
40.27
4.319
2.814
1.915
Chk Pass
Bi2230
ppb
-2.240
1.888
84.27
-1.270
-4.416
-1.035
Chk Pass
AJ3961
ppb
-2.621
8.511
324.7
-8.063
-6.983
7.186
Chk Pass
Ca3179
ppb
-1.975
3.908
197.8
-6.409
-.4869
.9696
Chk Pass
As 1890
ppb
.5077
.4140
81-53
.7787
.0312
.7132
Chk Pass
Ca3933
ppb
-.0232
.2957
1275.
-.0807
-.2859
.2970
Chk Pass
B_2089
ppb
-.1481
.3500
236.4
-.0002
-.5477
-1038
Chk Pass
Cd2288
ppb
.0531
.0759
143.0
.1335
-.0173
.0431
Chk Pass
Ba4554
ppb
.0248
.0304
122.8
.0088
.0057
-0599
Chk Pass
Co2286
ppb
.0932
.0344
36.92
.1319
-0662
.0814
Chk Pass
Ba4554-2
ppb
-7249
.3487
48.10
-.3269
-.9764
--3713
Chk Pa££
Cr2677
ppb
-.0830
.3364
405.2
-.2926
.3050
-.2615
Chk Pass
6e2348
ppb
.0915
.0193
21.07
.0705
.0954
.1085
Chk Pass
Cu2178
ppb
-.4578
1.543
337.0
-1.342
1.324
-1.355
Chk Pass
Be2348-2
ppb
-.0634
.1675
264.1
.1019
-.2330
-.0591
Chk Pass
Cu2l99
ppb
.9368
.4032
43-04
.4830
1.254
1.073
Chk Pass
Be3130
ppb
.0854
.0191
22.37
-0714
.0776
.1072
Chk Pass
Cu327S
ppb
4.855
6.124
126.1
-1.703
10.43
5.342
Chk Pass
2/25/2009 13:52:11
2
Sample Name; CCB Acquired: 2/25/2009 10:38:06 Type:.QC
Method: METHOD DVP(v114) Mode: CONC Corr. Faclor; 1.000000
User: admin Custom IDI: Custom ID2: Custom 1D3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1 n
#3
Check ?
High Limit
Low Limit
Fe2599
ppb
2.713
1.071
39.46
1.904
2.308
3.927
Chk Pass
Ni2316
ppb
.0574
.2303
401.1
.2824
-.1778
.0676
Chk Pass
Fe2714
ppb
-5.469
5.946
108.7
-6.743
1.010
-10.68
Chk Pass
P_1774
ppb
-.1086
-7879
725.6
-.7553
.7689
-.3394
Chk Pass
K_7664
ppb
-1.318
51.53
3911.
-37.42
-24.22
57.69
Chk Pass
Pb220S
ppb
.7966 .
1.121
140.7
.7690
1.931
-.3102
Chk Pass
Li6707
ppb
F 2.827
.753
26.62
2.967
3.500
2.014
Chk Fail
2.000
-2.000
Sb2068
ppb
.7778
.2169
27.89
.5275
.9102
.8958
Chk Pass
Mg2790
ppb
-1.798
8.607
478.8
7.736
-4.135
-8.994
Chk Pass
Sel960
ppb
-.1595
1.428
895.8
-1.774
.9386
.3573
Chk Pass
Mg2852
ppb
3.548
1.353
38.13
4.620
3.996
2.028
C)ik Pass
Si2124
ppb
.0929
.9287
999.9
1.113
-.6926
-.1467
Chk Pass
Mn2576
ppb
.8864
.2580
29.11
.6924
.7875
1.179
Chk Pass
Si2124-2
ppb
1.312
2.574
196.1
2696
-1.657
2.899
Chk Pass
Mn2576-2
ppb
.8600
.2523
29.39
1.048
.9589
.5727
Chk Pass
Sn1899
ppb
.2873
.0663
23.07
.3401
.2129
.3089
Chk Pass
Mo2020
ppb
-.1436
.0505
35.19
-.1164
-.1124
-.2019
Chk Pass
Sr2165
ppb
.3443
.1425
41.39
.3041
.5025
.2261
Chk Pass
Na5895
ppb
12-73
15.59
122.5
26.40
16-05
-4.256
Chk Pass
Sr4215
ppb
-.0679
.1023
176.6
-.1691
.0322
-.0369
Chk Pass
9988^935
Sampie Name: CCB Acquired: 2/25/2009 10:38:06 Type: QC
Method: METHOD DVP{vl 14) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS"
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Chock?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Th2337
ppb
-1.077
.546
50.63
-.5477
-1.638
-t.046
Chk Pass
Zr3391
ppb
.1773
.2162
122.0
.1749
-.0378
.3947
Chk Pass
TiS349
ppb
.0041
.1012
2483.
-.0196
-.0832
.1150
Chk Pass
Zr3391-2
ppb
3.166
1.828
57.73
1.098
4.567
3.834
Chk Pass
Ti 3349-2
ppb
.2025
.7785
384.5
.3219
.9144
-.6288
Chk Pass
TI1908
ppb
.7261
.6118
84.25
1.063
.0200
1.096
Chk Pass
U_26S5
ppb
.2429
5.485
2258.
3.155
-6.084
3.658
Chk Pass
U_3854
ppb
-21.67
20.29
93.65
-42.70
-2.208
-20.10
Chk Pass
U_4090
ppb
17.83
4.07
22.82
15.04
22.49
15.94
Chk Pass
V 2924
ppb
.3082
.4535
147.1
-2116
.5137
.6226
Chk Pass
Zn2138
ppb
-.3889
.0647
16.63
-.4632
-.3583
-.3448
Chk Pass
Zn2138-2
ppb
.0295
.2690
912.5
.3296
-.0513
-.1899
Chk Pass
2'25/2009 13:52:11
4
Sample Name; CCB /Acquired; 2/25/2009 10:38:06 Type: QC
Method; METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom 1D2: Custom IDS:
Comment;
(nt. Sto.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Qs/S
25208.
39.
.35210
25281.
25109.
25233.
Y 3600
Cts/S
174700.
1S91.
1.0822
172520.
17S60O.
175970.
Y 3710
Cts/S
19002.
437.
2.3010
18896.
19482.
18627.
89^38837
Sample Name: CRI Acquired: 2/25/2009 10:45.08 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Corr. Factor: 1 OOOOOO
User: admin Custom IDI: Custom ID2; Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
Ag3280
ppb
20.02
.06
.2946
All 670
ppb
246.3
1.8
.7408
AI3961
ppb
216.4
2.2
1.017
Asl890
ppb
22,05
,75
3.412
B_2089
ppb
20.12
.40
1.993
Ba4554
ppb
21.90
.04
.2001
Ba4554-2
ppb
19-80
.72
3.650
Be2348
ppb
19.33
.03
.1575
Be2348-2
ppb
19.60
.25
1.282
Be3130
ppb
19.55
.09
.4566
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
20.08
20.01
19.97
248.4
245,7
244.9
215.9
214.5
218.S
22.62
2234
21.20
20.48
19.69
20.18
21.88
21.86
21.95
20.58
19.66
19.16
19.30
19.36
19.34
19.32
19.81
19.65
19.46
19.55
19.64
Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass
Be3130-2
ppb
20.05
.20
.9772
Bi22S0
ppb
19.41
1.25
6.467
Ca3179
ppb
75.05
4.20
5.600
CaS9S3
ppb
80.64
.16
.1974
Cd228a
ppb
20.41
.02
.1149
Co2286
ppb
20.65
.12
.5825
Cr2677
ppb
20.14
.35
1.718
Cu2178
ppb
20.35
1.06
5.221
Cu2199
ppb
21.04
.44
2.074
Cu3273
ppb
25.61
1.38
5.377
#1
#2
#3
Check?
Value
Range
20.08
19.84
20.23
19.87
17.99
20.36
79.53
71.20
74.42
80.62
80.49
80.80
20.44
20.40
20.39
20.55
20.62
20.73
20.35
20.33
19.74
19.18
21.25
20.62
20.66
20.97
21.51
25.63
26.98
24.23
Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass 'Chk Pass Chk Pass
2/25/2009 13:52:11
2
Sample Name: CRI Acquired; 2/25/2009 10:45:08 Type: QC
Method; METHOD DVP(v114) Mode; CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
Value
Range
Fe2599
ppb
207.0
.7
.3399
207.2
207.7
206.3
Chk Pass
Ni2316
ppb
20.68
.20
.9528
20.88
20.49
20.67
Chk Pass
Fe27l4
ppb
204-3
3.7
1.815
203.4
208.4
201.1
Chk Pass
P 1774
ppb
147.1
1.6
1-057
148.9
146.3
146.0
Chk Pass
K^7664
ppb
233.5
18.4
7.857
248.0
212.9
239-6
Chk Pass
Pb2203
ppb
20.94
1.12
5.334
22-19
20.04
20.60
Chk Pass
LJ6707
ppb
169.4
1.5
.3937
167.8
170.9
169.5
Chk Pass
Sb2068
ppb
21.34
.46
2.158
21.80
21.33
20.88
Chk Pass
Mg2790
ppb
165.8
21.2
12.78
147.3
161-3
188.9
Chk Pass
Sel960
ppb
22.01
1.37
6.206
21.68
20.85
23.52
Chk Pass
Mg2S52
ppb
169.8
1.2
.7315
1712
169.0
169.1
Chk Pass
312124
ppb
130.1
2.0
1.557
129.6
128.4
132.3
Chk Pass
Mn2576
ppb
207.3
.4
.1972
206.9
207.5
207.7
Chk Pass
Si2124-2
ppb
11S.2
13.0
10.97
1322
106.6
115-7
Chk Pass
Mn2576-2
ppb
205.1
1.3
.6288
205.7
203.7
206.1
Chk Pass
Snl899
ppb
20-41
-07
.3283
20.43
20.35
20.39
Chk Pass
Mo2020
ppb
20.26
.11
.5228
20-16
20-37
20.24
Chk Pass
Sf2165
ppb
20.57
.17
.8327
20.51
20.43
20.76
Chk Pass
Na5895
ppb
227.4
12.3
5.416
234.7
213.2
234.2
Chk Pass
Sr4215
ppb
20.41
.02
.1155
20.41
20-38
20.43
Chk Pass
Sample Name: CRI Acquired: 2/25/2009 10:45:08 Type: QC
Method; METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2837
ppb
143.6
1.2
-8691
1422
144.2
144.4
Chk Pass
Zr3391
ppb
145.1
.4
.2902
144.7
145.2
145.5
Chk Pass
TiS349
ppb
19.93
.09
.4478
19.35
19.93
20.02
Chk Pass
2r3391-2
ppb
146.8
1.6
1.108
144.9
147.6
147.9
Chk Pass
TI3349-2
ppb
21.03
1.31
6.245
22.23
19.63
21.23
Chk Pass
TII 908
ppb
20.56
.70
3.421
21.19
19.80
20.69
Chk Pass
U_2635
ppb
198.7
5.7
2.S7S
204.4
198.7
193.0
None
U_S854
ppb
167-4
18.5
11.07
188.6
153.8
159.9
None
U_4090
Ppb
196.8
8.1
4.118
198-0
204.2
183.2
None
V_2924
ppb
195.6
.8
.4120
195.3
195.1
196.6
Chk Pass
Zn2138
ppb
19.92
.09
.4651
19.81
19.96
19.98
Chk Pass
Zn2138-2
ppb
19.50
.27
1.397
19.73
19.57
19.20
Chk Pass
2/25/200913:5211
4
Sample Name: CRI Acquired: 2/25/2009 10:45:03 Type: QC
Method: METHOD DVP{v114) Mode; CONC Con. Factor 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Inl. Sid.
Units
Avg
Stddev
%RSD
Y 2243
Cls/S
24989.
22.
.08670
Y 3600
Cla/S
173520.
75.
.04301
Y 3710
Cts/S
18809.
58.
.31029
#1
#2
#3
25010. 173550. 18808.
24967. 173570. 18869.
24991. 173430. 18752.
Sample Name: ISAl Acquired: 2/25/2009 10:52:02 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Corr. Factor 1.000000
User: admin Custom ID1; Custom lD2i Custom IDS:
Comment: V
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
AgS280
ppb
.0041
.4392
106S0.
.4726
-.3984
-.0617
All 670
ppb
30730.
164.
.5340
S0830.
30810.
30540.
AI3961
ppb
521900.
1796,
.3442
522300.
523400.
519900.
AS1890
ppb
-5.946
1.673
28.14
-4.056
-6.543
-7.240
B_2089
ppb
2.079
.312
15.03
1.725
2317
2.193
Ba4554
ppb
.0443
.0135
30.47
.0429
.0584
.0315
Ba4554-2
ppb
-.6916
.2239
32.37
-.5659
-.5589
-.9501
Be2348
ppb
-1.318
.103
7.853
-1.272
-1.246
-1.436
Be2348-2
ppb
-.9922
.3687
37.16
-1.199
-.5666
-1211
BeSISO
ppb
-.3338
-0132
3.961
-.3419
-.3410
-.3186
Check ?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Chech?
Value
Range
None
Be3130-2
ppb
-.1810
.1281
70.79
-.3007
-.0459
-.1963
None
None Chk Pass
Bi22S0
ppb
-39.60
2.15
5.421
-38.36
-38.36
-42.08
Ca3179
ppb
486100.
3648.
.7505
483400.
4S4700.
490300.
None Chk Pass
None
Ca393S
None None None None None None
ppb
None
Cd2288
ppb
.1306
.0914
69.98
.0683
.2356
.0880
Co2286
ppb
-.8526
.0322
3.776
-.8403
-.3891
-.8283
Cr2677
ppb
2.936
.225
7.645
2715
3.164
2.929
Cu2178
ppb
1.223
2.427
198.5
2388
-1.567
2.848
Cu2199
ppb
-7.976
.858
10.75
-7.926
-8.858
-7.145
Cu3273
ppb
16.94
3.77
22.28
13.63
21.05
16.14
None None None None None None
2/25/2009 13:52:11
2
Sample Name: ISAl Acquired: 2/25/2009 10:52:02 Type: QC
Meihod: METHOD DVP(vl 14) Mode: CONC Con. Faclor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS;
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Fe2599
ppb
199100.
474.
.2381
198800-
199700.
198900.
Chk Pass
Ni23l6
ppb
-6-876
.131
1.900
-6.853
-6.758
-7.017
None
Fe2714
ppb
196700.
750.
.3831
195400.
196500-
195100.
None
P_1774
ppb
9.411
1.631
17.33
10.34
7.528
10.37
None
K_7664
ppb
-54.83
31.05
56.63
-72.94
-72.56
-18.98
None
Pb220S
ppb
1.263
3.610
285.8
3.954
2.675
-2.840
None
U6707
ppb
14.68
.96
6.571
15.65
13.73
14.66
None
Sb2068
ppb
3.372
3.094
91.74
6.078
-.0007
4.040
None
Mg2790
ppb
499200.
937.
.1877
498800.
500300.
498600.
Chk Pass
Sel960
ppb
6.482
2.323
35.84
7.096
3.913
8.436
None
Mg2852
ppb
432300.
2119.
.4902
429800.
433400.
433600.
None
Si2124
ppb
-9.464
1.170
12.36
-9.580
-10.57
-8.241
None
Mn2576
ppb
-3.024
.135
4.462
-3.086
-3.116
-2.869
None
Si2124-2
ppb
14.16
7.28
51.44
22.39
11-50
8.574
None
Mn2576-2
ppb
-2287
.381
16.65
-2.669
-2.283
-1.907
None
Snl899
ppb
-.9312
.2999
32.21
-.6930
-1.268
-.8325
None
Mo2020
ppb
-.4495
.4249
94.54
-.7382
-.6486
.0385
None
Sr2165
ppb
-13.52
.47
3.481
-12.99
-13.90
-13.67
None
Na5895
ppb
52-62
5.57
10.59
50.32
58.97
48.57
None
Sr4215
ppb
.3688
.1081
29.32
.4912
.2863
.3288
None
9^99^46
Sample Name: ISAl Acquired: 2/25/2009 10:52:02 Type: QC
Method; METHOD DVPfvl 14) Mode: CONC Com. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Bern
Units
Avg
Slddev
%RSD
«1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
«3
Th2837
ppb
-1.681
3.182
189.3
1.382
-1.454
-4.970
Ti3349
ppb
1.804
.118
6.523
1.834
1.903
1.674
Ti3349-2
ppb
6.838
1.416
20.70
6.857
8.244
5.412
711908
ppb
-.7125
1.385
194.4
-.6329
-2.136
.6312
U_2635
ppb
-87.78
19.97
22.75
-85.83
-108.7
-68.86
U_3854
ppb
-260.9
7-3
2.798
-269.4
-256.3
-257.1
U_4090
ppb
-13.83
5.53
40.03
-19.58
-8.539
-13.36
V_2924
ppb
-6.185
.132
2126
-6.336
-6.130
-6.091
Zn2138
ppb
3.717
.149
4.010
3.872
3.707
3.574
Zn2138-2
ppb
-.4944
.4531
91.65
-.9975
-.3667
-.1188
None None
Zr3391
ppb
1-575
.352
22.34
1.245
1.534
1.945
Zr3391-2
ppb
3.257
.527
16.18
3.732
2.690
3.349
None None None None None None None None
Check?
Value
Range
None None
2/25/2009 13:52:11
4
Sample Name: ISA1 Acquired: 2/25/2009 10:52:02 Type: QC
MeUiod: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
Cts/S
23252.
62.
.26506
Y 3600
Cts/S
155620.
188.
.12089
Y 3710
Cts/S
18509.
43.
.23091
#1
#2
#3
23224. 155470. 13550.
23209. 155550. 18465.
23323. 155830. 18512.
89998^^1
Sample Name; ISBl Acquired: 2/25/2009 10:59:13 Type: QC
Meihod: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment: /
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Ag32ao
ppb
1033.
4.
.4320
1037.
1028.
1034.
Chk Pass
Be3130-2
ppb
506.9
16.3
3.220
488.1
516.2
516.5
Chk Pass
All 670
ppb
30560.
45.
.1474
30530.
30610.
30540.
None
8i2230
ppb
996.3
62
.6174
993.9
991.7
1003.
Chk Pass
At3961
ppb
101600.
3264.
3212
97330.
103300.
103600.
Chk Pass
Ca3179
ppb
98250.
3026.
3.080
94760.
100100.
99950.
Chk Pass
As 1890
ppb
993.6
5.0
.5014
993.9
988.5
998.5
Chk Pass
Ca3933
ppb
86920.
911.
1.048
86090.
87890.
86770.
None
B_20fi9
ppb
989.3
5.7
.5779
985.6
986.4
995.9
Chk Pass
Cd2283
ppb
1008.
5.
.4724
1005-
1005.
1013.
Chk Pass
Ba4554
ppb
523.6
2.3
.4331
525.6
521.1
524.0
Chk Pass
Co22S6
ppb
485.9
23
.4771
4S4.3
484.4
488.6
Chk Pass
B34554-2
ppb
510.3
15.9
3.120
491.9
519.7
519.3
Chk Pass
Cr2677
ppb
500.9
3.2
.6353
50S.5
497.3
501.7
Chk Pass
Be234d
ppb
516.5
28
-5443
518.6
513.3
517.7
Chk Pass
Cu2178
ppb
490.7
4.8
.9816
488.9
487.0
496-1
Chk Pass
Be2348-2
ppb
506.6
15.7
3.096
488.5
516.6
514.6
Chk Pass
Cu2199
ppb
485.3
22
.4490
483.7
484.4
487.8
Chk Pass
Be3130
ppb
522.9
3.1
.5993
525.0
519.3
524.3
Chk Pass
Cu3273
ppb
478.0
18.7
3.907
456.4
489.0
438.6
Chk Pass
2/25/200913:52:11
2
Sample Name: ISBI Acquired: 2/25/2009 10:59:13 Type: QC
Method: METHOD DVP{v114) Mode: CONC Con". Factor: 1.000000
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check ?
Value
Range
Fe2599
ppb
40070.
1279.
3.193
38590.
40810.
40800-
Chk Pass
Ni2316
ppb
967-6
5.0
.5193
965.7
963.9
973.3
Chk Pass
Fe2714
ppb
39990.
156.
.3888
40030.
39810.
40070.
None
P_1774
ppb
1057.
S.
.2816
1054.
1057.
1060.
Chk Pass
K_7664
ppb
5043.
102
2016
4934.
5135-
5058.
Chk Pass
Pb220S
ppb
965.5
5.3
.5530
965.4
960.3
970-9
Chk Pass
Li6707
ppb
2047.
56.
2736
1982.
2076.
2082.
Chk Pass
Sb2068
ppb
1012-
2.
.1967
1010.
1011.
1014.
Chk Pass
Mg2790
ppb
98540-
3003.
3.048
95070.
100400.
100200.
Chk Pass
Sel960
ppb
9S9.0
5.9
.5942
983.8
987.7
995.4
Chk Pass
Mg2852
ppb
98430.
3050.
3.099
94910.
100100.
100200.
Chk Pass
Si2124
ppb
1023.
6.
.5469
1021.
1019.
1030.
Chk Pass
Mn2576
ppb
506.5
2.4
.4673
508.7
504.0
506.8
Chk Pass
Si2124-2
ppb
1014
21.
2080
990.1
1030.
1022.
Chk Pass
Mn2576-2
ppb
497.5
14.9
S.005
480.2
506.3
505.9
Chk Pass
Sn1899
ppb
985.7
4.2
.4303
983.1
983.4
990.6
Chk Pass
Mo2020
ppb
1009.
5.
.5031
1005.
10O7.
1015.
Chk Pass
Sr2165
ppb
958.8
4.6
.4817
957.1
955.2
964.0
Chk Pass
Na5895
ppb
1034.
24.
2.307
1007.
1049.
1047.
Chk Pass
Sr4215
ppb
998.4
29.7
2.975
964.2
1014.
1017.
Chk Pass
88^S88it2
Sample Name: ISBI Acquired; 2/25/2009 10:59:13 Type: QC
Method: METHOD DVP(vll4) Mode; CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2837
ppb
1018.
4.
-3927
1023.
1015.
1016.
Chk Pass
ZrSSgi
ppb
1045.
4.
.3908
1049.
1041.
1044.
Chk Pass
Ti3349
ppb
1017.
4.
.4207
1021.
1013.
1019.
Chk P3SS
Zr339l-2
ppb
1020.
35.
3.448
979.7
1039.
1042.
Chk Pass
TiS349-2
ppb
998-2
32.7
3.272
9612
1023-
1010.
Chk Pass
Til 908
ppb
956.7
6.6
.6901
954.9
951.2
964.0
Chk Pass
U_2635
ppb
825.1
10.0
1.213
836.6
818.S
820.5
Chk Pass
U_3854
ppb
896.0
45.7
5.097
948.7
369.9
869.4
Chk Pass
U^4090
ppb
1031.
17.
1-614
1029.
1015.
1048.
Chk Pass
V_2g24
ppb
504.3
1.8
.3665
506-1
502.4
504.3
Chk Pass
Zn2138
ppb
1008.
5.
-5184
1005.
1004.
1014.
Chk Pass
Zn2138-2
ppb
977.3
20.1
2.060
954.2
991.6
985.9
Chk Pass
2/25/2009 13:52:11
4
Sample Name; ISBI Acquired: 2/25/2009 10:59:13 Type: QC
Method: METHOD DVP(v114) Mode; CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std.
Unils
Avg
Stddev
%RSD
#1
#2
#3
Y_2243
Os/S
24461.
51.
.20695
Y_3600
Cts/S
167180.
1090.
.65211
Y_3710
Cls/S
18980.
369.
1.9455
24511. 166940. 19406.
24463. 168380- 18745.
24410. 1662-10. 18790.
88^83643
Sample Name: CCV Acquired: 2/25/2009 11:07:22 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor; 1.000000
User: admin Custom IDI: Custom tD2: Custom IDS:
Comment: y
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Ag3280
ppb
487.9
2.9
.5960
485.9
4912
486.4
Chk Pass
Be3130-2
ppb
503-0
1-3
.2560
504.4
502.8
501.9
Chk Pass
AJ1670
ppb
5384.
20.
.3774
5407.
5373.
5368.
Chk Pass
BI2230
ppb
506.1
1.9
.3314
507.6
506.8
503.9
Chk Pass
AI3961
ppb
5044-
21.
.4091
5067.
5032.
5032.
Chk Pass
Ca3179
ppb
2052.
9.
.4520
2063.
2048.
2046.
Chk Pass
AS1890
ppb
498.4
3.0
.6060
501.0
499.3
495.1
Chk Pass
CaS933
ppb
2077.
3.
.1507
2080.
2078.
2074.
Chk Pass
B_2039
ppb
498.7
1.5
.2910
498.7
4972
500.1
Chk Pass
CC12288
ppb
499.8
.7
.1433
500.3
499.0
500.1
Chk Pass
Ba4554
ppb
527.1
3.1
.5799
524.6
530.5
526.1
Chk Pass
Co7?86
ppb
500.2
.7
.1421
500.7
499.4
500.5
Chk Pass
Ba4554-2
ppb
507.1
1.8
.3629
508.7
507.6
505.1
Chk Pass
Cr2677
ppb
500.4
2.5
.4918
498.0
502.9
500.3
Chk Pass
Be2S48
ppb
495.2
2.8
.5626
493.0
498.3
494-3
Chk Pass
Cu2178
ppb
508.7
.3
.0564
508.7
509.0
508-4
Chk Pass
Be2348-2
ppb
496.9
1.0
.1995
497.8
497.2
495.8
Chk Pass
Cu2199
ppb
501.5
.8
.1523
502.3
501.4
500.8
Chk Pass
Be3130
ppb
501.1
3.0
.6074
498.8
504.6
500.1
Chk Pass
Cu3273
ppb
501.2
5.4
1.069
504.1
504.4
495.0
Chk Pass
2/25/200913:5212
2
Sample Name: CCV Acquired: 2/25/2009 11:07:22 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Fe2599
ppb
5081.
11.
.2072
5090.
5069.
5084.
Chk Pass
Nt2S16
ppb
502-6
.6
.1224
502.2
502.2
503.3
Chk Pass
Fe27l4
ppb
5033.
31.
.6217
5002.
5064.
5034.
Chk Pass
P_1774
ppb
1060.
2.
.2229
1062.
1058.
1059.
Chk Pass
K_7654
ppb
5081.
20.
.3912
5084.
5050.
5099.
Chk Pass
Pb2203
ppb
502.2
.2
-0440
502.5
502.1
502.0
Chk Pass
Li6707
ppb
4095.
9.
.2084
4103.
4096.
4086.
Chk Pass
Sb2068
ppb
509.0
25
.4893
511.9
507.4
507.8
Chk Pass
Mg2790
ppb
4110.
33.
.8093
4148.
4096.
4086.
Chk Pass
Sel960
ppb
497.0
1.4
.2878
495.9
498.6
496.5
Chk Pass
Mg2852
ppb
4105.
8.
.2063
4113.
4096.
4104.
Chk Pass
St2124
ppb
537.0
1.4
2524
535.9
536.6
538.5
Chk Pass
Mn2576
ppb
5077.
31.
.6157
5048.
5110.
5073.
Chk Pass
Si2124-2
ppb
536-4
4.0
.7387
535.7
532.8
540.7
Chk Pass
Mn2576-2
ppb
5021.
15.
.2976
5033.
5016.
5010.
Chk Pass
Sn1899
ppb
495.2
1.3
.3570
497.0
493.5
494.9
Chk Pass
MO2020
ppb
500.7
.6
.1116
501.3
500.2
500.6
Chk Pass
Sr2165
ppb
494.3
.6
.1287
494.4
493.7
494.9
Chk Pass
Na5895
ppb
5041.
4.
.0703
5046.
5039.
5040.
Chk Pass
Sr4215
ppb
506.2
2.4
.4718
608.3
506.8
503.6
Chk Pass
8989998dd
Sample Name: CCV Acquired: 2/25/2009 11:07:22 Type: QC
Meihod: METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2837
ppb
1010.
7.
.7250
1005.
1018.
1006.
Chk Pass
ZrS391
ppb
1045.
7.
.6306
1040.
1053.
1041.
Chk Pass
Ti3349
ppb
498.6
3.1
.6120
497.5
502.3
496.7
Chk Pass
ZrSS91-2
ppb
1036.
3.
.3223
1033.
1039.
1032.
Chk Pass
Ti3349-2
ppb
494.2
3.3
.6717
497.8
493.6
491.2
Chk Pass
Til 908
ppb
496.2
.3
.0509
495.9
496.2
496.4
Chk Pass
U_2635
ppb
1956.
21.
1-095
1938.
1980.
1951.
Chk Pass
U_3854
ppb
1829.
23.
1.268
1812.
1820.
1856.
Chk Pass
U„4090
ppb
2085.
2.
.1164
2086.
2083.
2087.
Chk Pass
V_2924
ppb
4958.
32.
.6468
4937.
4995.
4942.
Chk Pass
Zn2138
ppb
504-1
.2
.0345
504.1
503.9
504.2
Chk Pass
Zn2l3&-2
ppb
491.3
3.9
.7858
494.7
487.1
492.1
Chk Pass
2/25/200913:52:12
4
Sample Name: CCV Acquired: 2/25/2009 11:07:22 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Corr. Factor: 1 OOOOOO
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
Cts/S
25263.
7.
.02724
Y 3600
Cts/S
175160.
S32.
-47502
Y 3710
Cls/S
19264.
124.
.64392
#1
#2
#3
25271. 17570Q. 19135.
25257. 17^200. 19382
25262. 175580. 19276.
5^5^d5
Sample Name: CCB Acquired: 2/25/2009 11 ;14;53 Type: QC
Method: METHOD DVP{vi 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom tD2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umil
Lew Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
/\g3280
ppb
.3608
.1617
44.81
.4436
.1745
.4642
Chk Pass
Be3130-2
ppb
-.0299
.0801
267.4
.0575
-.0475
-.0998
Chk Pass
AH 670
ppb
13.35
7.24
5421
20.93
12.63
6.505
Chk Pass
Bi2230
ppb
-2.103
.185
8-773
-1.890
-2.193
-2.224
Chk Pass
AI3961
ppb
28.60
11.15
38.98
33.54
15.83
36.42
Chk Pass
Ca3179
ppb
29-00
3.71
12.78
31,95
30.19
24.84
Chk Pass
Asl890
ppb
1.468
.326
22.22
1.256
1.306
1-844
Chk Pass
Ca3933
ppb
29.24
5.69
19.45
35.30
28.41
24.01
Chk Pass
B_2039
ppb
.2002
.3368
168.2
.5155
.2398
-.1546
Chk Pass
Cd2288
ppb
.1161
.0469
40.40
.1005
.1688
.0790
Chk Pass
Ba4554
ppb
.0410
,0395
96.20
.0689
.0583
-.0041
Chk Pass
C02286
ppb
.0921
.0926
100.5
.0363
.0410
.1989
Chk Pass
Ba4554-2
ppb
-.5743
.0142
2.475
-.5794
-.5852
-.5532
Chk Pass
Cr2677
ppb
-.2194
.1330
60.63
-.3731
-.1424
-.1428
Chk Pass
Be2348
ppb
.1344
.0632
47.04
.1681
.1736
.0615
Chk Pass
Cu2178
ppb
-1261
1.785
1416.
2.015
-1.533
-.1036
Chk Pass
Be2348-2
ppb
-.0833
.2772
332.6
.0245
.1237
-.3982
Chk Pass
Cu2199
ppb
.1952
.8334
426.9
-.7534
.8095
.5296
Chk Pass
Be3130
ppb
.1564
.0082
5.241
.1656
.1499
.1537
Chk Pass
CuS273
ppb
2.709
2.632
97.13
-.3237
4.064
4.388
Chk Pass
2/25/200913:52:12
2
Sample Name: CCB Acquired: 2/25/2009 11:14:5S Type: QC
Meihod: METHOD DVP(vl14) Mode: CONC Corr. Factor; 1.000000
User: admin Custom IDI; Custom ID2: Custom ID3:
Comment;
Elem
Units
Avg
Stddev
?i.RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSO
#1
#2
#3
Check?
High Limit
Low Limil
Fe2599
ppb
12.16
2.82
23.19
15.27
11.46
9.756
Chk Pass
Ni23l6
ppb
.2501
.0583
23.29
.2496
.1921
.3036
Chk Pass
Fe2714
14.04
211
15.01
14.30
11.82
16.01
Chk Pass
P_1774
ppb
.2212
-6245
282.4
-.8924
.3428
-.1139
Chk Pass
K_7664
ppb
-35.25
17.10
48.52
-26.52
-24.27
-54.95
Chk Pass
Pb220S
ppb
-.4803
.4923
1025
-.9301
.0457
-.5565
Chk Pass
Li6707
ppb
.0688
.8955
1302.
-.2645
-.6123
1.083
Chk Pass
Sb2068
ppb
-.1903
.6971
366.3
.6075
-.4964
-,6820
ChK Pass
Mg2790
ppb
26.82
24.06
89.69
53.85
7.776
18.83
Chk Pass
Se1960
ppb
2.637
1.069
40.52
1.604
2.570
3.738
Chk Pass
Mg2852
ppb
32.90
4.50
13.68
37.72
3216
28.82
Chk Pass
312124
ppb
.3479
1.553
446.6
-J.442
1.134
1.351
Chk Pass
Mn2576
ppb
.8451
-1186
14.04
.8774
.9442
.7137
Chk Pass
Si2124-2
ppb
4.536
3214
70.85
1-157
4.897
7.554
Chk Pass
Mn2576-2
ppb
1.056
.212
20.06
1.301
.9476
.9211
Chk Pass
Sn1899
ppb
.2531
.2732
107.9
-3591
.4574
-.0572
Chk Pass
Mo2020
ppb
.1483
.0889
59.95
.2366
.0588
.1494
Chk Pass
Sf2165
ppb
.4111
.1633
39.71
.5943
.3578
.2812
Chk Pass
Na5895
ppb
27.58
11.94
43.30
38.63
2921
14.91
ChK Pass
Sr4215
ppb
.2367
.1701
71.85
.2919
.0459
.3723
Chk Pass
98^98949
Sampte Name; CCB Aoquirad: 2/25/2009 11 ;14;53 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User; admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th2837
ppb
.5457
.6618
121.3
1.262
.4182
-.0431
Chk Pass
ZrSS91
ppb
.1155
.1128
97.69
-.0061
.1357
.2168
Chk Pass
Ti3349
ppb
.0356
.1158
325.1
-.0746
.1563
.0252
Chk Pass
Zr3391-2
ppb
.4309
.9528
221.1
-.6650
1.063
-8947
Chk Pass
Ti3349-2
ppb
-1.660
.646
38.94
-1.087
-1.532
-2.360
Chk Pass
TI1908
ppb
1.427
1.323
93-10
1.894
-.0721
2.458
Chk Pass
U„26S5
ppb
16.49
12.00
72.75
9.643
30.35
9.488
Chk Pass
U_3854
ppb
-19.87
2121
106.3
-21.08
1.919
^0.46
Chk Pass
U„4090
ppb
7.217
18.86
261.3
-1041
4.962
27-10
Chk Pass
V^2924
ppb
.3091
.5214
168.7
.6202
.5998
-.2929
Chk Pass
Zn2138
ppb
-.4412
-0553
12.54
-.3307
-.4536
-.4393
Chk Pass
Zn2138-2
ppb
-.3560
.3591
100.9
-.7699
-.1279
-.1701
Chk Pass
2/25/2009 13:52:12
4
Sample Name: CCB /Acquired; 2/25/2009 11:14:53 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment:
Int. Std.
Unils
Avg
Stddev
%RSD
#1
#2
03
Y 2243
Cts/S
25081.
49.
.19546
2509S.
25119.
25025.
Y 3600
Cts/S
174540.
372.
21328
174820.
174120.
174680.
Y 3710
Cts/S
19315.
38.
.45749
19365.
19213.
19366.
8969^94?
Sample Name: L902152-BLK1
Method: METHOD DVP(v114)
User: admin Custom IDI;
Comment:
Acquired; 2/25/2009 11:21:54 Type: Unk
Mode: CONC Con. Faclor: 1.000000
Custom ID2: Custom ID3: y
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Ag3280
ppb
.3081
.2744
89.05
.0119
.3587
.5537
Chk Pass
BeS130-2
ppb
.0945
.2422
256,3
. .3738
-.0579
-.0324
Chk Pass
All 670
ppb
16.50
3.02
18.31
19.73
16.03
13.74
Chk Pass
Bi2230
ppb
-1.339
.692
51.67
-.9899
-2136
-.8914
Chk Pass
A)3961
ppb
33.58
2.32
6.902
31.53
36.10
33.13
Chk Pass
Ca3179
ppb
49.13
11.14
22.67
5741
53.52
36.47
Chk Pass
Asia90
ppb
1.069
.896
83.87
.5570
.5454
2.104
Chk Pass
Ca3933
ppb
50.69
7.06
13.93
58.04
50.09
43.95
Chk Pass
B_2089
ppb
.3511
.4189
119.3
-.0720
.3596
.7657
Chk Pass
Cd2288
ppb
-.0302
.0756
2500
-.0088
.0323
-.1142
Chk Pass
Ba4554
ppb
.0000
-016
5380000.
-.0167
.0140
.0027
Chk Pass
Co2286
ppb
.2078
.2232
107.4
.0403
.4612
.1219
Chk Pass
Ba4554-2
ppb
-.8403
.1813
21.57
-.8766
-1.001
-.6436
Chk Pass
Cr2677
ppb
.8125
.1764
21.71
1.015
.7333
.6897
Chk Pass
Be2348
ppb
.0607
.0074
12.27
.0659
.0522
.0640
Chk Pass
Cu2173
ppb
-2144
.7242
337.8
-.6230
.6218
-.6419
Chk Pass
Be2348-2
ppb
-.0617
.0911
147.6
.0314
-.1506
-.0660
Chk Pass
Cu2ig9
ppb
.1962
.9395
478.8
.4353
-.8397
.9931
Chk Pass
BeS130
ppb
.0973
.0112
11.54
.1030
.1045
.0343
Chk Pass
CuS273
ppb
6.50S
4.683
72.01
11.63
5.420
2.457
Chk Pass
2/25/200913:52:12
2
Sample Name: L902152-BLKl
Method: METHOD DVP(v114)
User: admin Custom IDl:
Comment:
Acquired: 2/25/2009 11:21:54 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
«1
*2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
18.22
1.41
7.714
19.84
17.36
17.46
Chk Pass
Ni2316
ppb
4.026
.142
3.533
3.898
4.180
4.001
Chk Pass
Fe2714
ppb
15.27
4.53
29.68
15.60
10.58
19.63
Chk Pass
P_1774
ppb
.3612
.1959
54.23
.5428
.1536
.3874
Chk Pass
K_7664
ppb
8.441
93.99
1114.
116.5
-36.39
-54.74
Chk Pass
Pb2203
ppb
.3086
.8264
267.8
-.6285
.9331
.6214
Chk Pass
Li6707
ppb
.3698
2.475
669.2
1.484
-2.466
2.091
Chk Pass
Sb2068
ppb
.9256
.6094
65.84
1.624
.6532
.4999
Chk Pass
Mg2790
ppb
15.69
13.82
88.11
3.283
7.148
31.64
Chk Pass
Sel960
ppb
1.248
.797
63.86
.7883
2163
.7873
Chk Pass
Mg2852
ppb
33.65
8.36
24.85
42.66
32.12
26.15
Chk Pass
Si2124
ppb
14.14
.26
1.814
14.41
13.91
14.09
Chk Pass
Mn2576
ppb
-4501
.0595
13.22
.5073
.4545
.3885
Chk Pass
Si2124-2
ppb
9.986
10.53
105.4
16.73
15.37
-2.145
Chk Pass
Mn2576-2
ppb
.8157
.5626
68.97
.7423
1.411
.2934
Chk Pass
Snl899
ppb
1.054
.162
15.34
.8677
1.142
1.153
Chk Pass
Mo2020
ppb
.8743
.1330
1521
.7638
.8371
1.022
Chk Pass
.Sr2l65
ppb
.1672
.0344
50.49
.0698
.2186
2133
Chk Pass
Na5895
ppb
4.360
18.01
4132
22.71
3.670
-13.30
Chk Pass
Sr4215
ppb
.3504
.0643
13.35
.3838
.2763
.3912
Chk Pass
99899^48
Sample Name: L902152-BLK1
Method: METHOD DVP(vll4)
User: admin Custom IDI:
Cornmeni:
Acquired: 2/25/2009 11:21 ;54 Type: Unk
Mode: CONC Conr. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th2837
ppb
.1369
1.105
806.9
-.4084
-.5893
1.409
Chk Pass
Zr3391
ppb
.1310
.1152
87,92
.1703
.2214
-0013
Chk Pass
TiSS49
ppb
.2042
.0274
13.42
.2234
.1728
.2164
Chk Pass
Zr3391-2
ppb
1.911
.494
25.87
2.209
2.132
1.340
Chk Pass
Ti3349-2
ppb
-1.312
.661
50.41
-.9070
-2.074
-.9531
Chk Pass
TII 908
ppb
.8320
.4750
57.09
1.300
.3507
.8449
Chk Pass
U_2635
ppb
32.86
18.84
57.33
52-39
14.79
3141
Chk Pass
U,3854
ppb
-47.72
11.29
23.65
-60.76
-41.30
-41.12
Chk Pass
U^4090
ppb
21-27
13.78
64.80
10.21
16.89
36.71
Chk Pass
V_2924
ppb
-.1664
.1185
71.22
-.2742
-.1854
-.0395
Chk Pass
Zn2138
ppb
1.522
.104
6.822
1.508
1.632
1.426
Chk Pass
Zn2138-2
ppb
1.995
.260
13.05
2.296
1.839
1.851
Chk Pass
2/25/2009 13:52:12
4
Sample Name; L902152-BLK1
Meihod: METHOD DVP(v114)
User: admin Custom (Dl:
Comment:
Acquired: 2/25/2009 11:21:54 Type: Unk
Mode; CONC Corr. Factor: 1.000000
Custom ID2; Custom IDS:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y^2243
Cts/S
25263.
21.
.08217
Y_3600
Cts/S
177350.
1220.
.68769
Y„3710
Cls/S
19848.
45.
.22604
25280. 175940. 19S03.
25270. 178100. 19S93.
25240. J78000. 19349.
9993^^5
Sample Name: 0902040-01
Method: METHOD DVP(v114)
User- admin Custom IDI:
Comment:
Aociuired: 2/25/2009 11 ;29:33 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS;
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
»2
#3
Check 7
High Limit
Low Limil
Ag32S0
ppb
.3181
.8207
258.0
.7053
.8736
-.6246
Chk Pass
Ba3130-2
ppb
.1507
.1902
1262
.3088
.2036
-.0603
Chk Pass
All 670
ppb
3030.
18.
.5793
3049.
3023.
3016.
Chk Pass
Bi22S0
ppb
-.8213
2.826
344.1
2.113
-1.051
-3.526
Chk Pass
AI39ei
ppb
2847.
5.
.1858
2842.
2852.
2347.
Chk Pass
Ca3179
ppb
58830.
74.
.1264
58910-
5SS00.
58780.
Chk Pass
As1890
ppb
5.428
.898
16.54
4.627
5.259
6.399
Chk Pass
Ca3933
ppb
F 54460.
570.
1.047
54050-
55110.
54220.
Chk Fail
10000.
-10000.
B_2089
ppb
46.17
.32
.6843
46.27
46.43
45-82
Chk Pass
Cd2288
ppb
.3317
.0563
16.67
.2368
-3935
-3148
Chk Pass
6a4554
ppb
115.9
.5
.4596
116.5
115.9
115.4
Chk Pass
Co2286
ppb
1.678
.027
1.585
1.651
1.680
1.704
Chk Pass
Ba4554-2
ppb
113.1
.4
.3577
113.6
113.1
1127
Chk Pass
Cr2677
ppb
8.414
.318
3-780
8.666
8.056
8.519
Chk Pass
Be234S
ppb
.1713
.0310
18.08
.1698
.1411
.2029
Chk Pass
Cu2178
ppb
10-60
49
4.637
10.13
10.55
11.11
Chk Pass
Be234fi-2
ppb
.0004
.0863
22710.
.0709
-.0959
.0262
Chk Pass
Cu2199
ppb
10.07
.61
6.089
10.65
9.423
10.14
Chk Pass
Be3130
ppb
.1852
.0209
11.29
.1704
.1762
.2091
Chk Pass
Cu3273
ppb
15.25
3.61
23.70
11.09
17.09
17.58
Chk Pass
2/25.^00913:52:12
2
Sample Name: 0902040-01
Method: METHOD DVP{v114)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 11:29:33 Type: Unk
Mode: CONC Con. Factor 1.000000
Custom ID2: Custom IDS;
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
3040.
3.
.0915
3037.
3041.
3042.
Chk Pass
Ni2316
ppb
8.757
-116
1.321
8.776
8.633
8.862
Chk Pass
Fe2714
ppb
2991.
22.
.7372
3015.
2934.
2973.
Chk Pass
P_1774
ppb
281.7
1.1
.3743
232.9
281.1
281.2
Chk Pass
K 7664
ppb
3621.
87.
2.395
3566.
3721.
3577.
Chk Pass
Pb2203
ppb
5.810
.757
13.03
5.539
5.188
6.653
Chk Pass
Li6707
ppb
9.646
.872
9.041
8.947
10.62
9.369
Chk Pass
Sb2068
ppb
2-841
1.483
52.20
3.237
4.048
1.186
Chk Pass
Mg2790
ppb
16880.
30.
.1750
16920.
16870.
16860-
Chk Pass
Sel960
ppb
3.408
1.308
38.37
1.991
4.569
3.663
Chk Pass
Mo2352
ppb
F 17160.
24-
.1418
17170.
17190.
17140.
Chk Fail
10000.
-10000.
Si2l24
ppb
8458.
16.
.1945
8475.
8455.
3443.
Chk Pass
Mn2576
ppb
178-8
1.1
.6330
179.8
178.9
177.6
Chk Pass
Si2124-2
ppb
7924.
34.
.4329
7958.
7923.
7890.
Chk Pass
Mn2576-2
ppb
178,6
1.1
.6116
178.4
179.7
177-5
Chk Pass
Sniagg
ppb
1.611
.230
14.25
1.840
1.381
1.613
Chk Pass
Mo2020
ppb
4.276
.135
3.145
4.171
4.428
4.229
Chk Pass
Sr2l65
ppb
453.8
1.2
.2749
455-2
453.3
452.9
Chk Pass
Na5895
ppb
181300.
340-
.1876
181700.
181300.
181000.
Chk Pass
Sr4215
ppb
474.3
.5
.1053
474.8
474.2
473.8
Chk Pass
bi2t;^wS5a
Sample Name: 0902040-01 Acquired: 2/25/2009 11:29:33 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1 .QQQOOO
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Th2837
ppb
-.9378
1.005
107.2
-1.225
-1.768
.1800
Chk Pass
Zr3S91
ppb
2.567
.219
8.520
2.418
2.464
2.818
Chk Pass
Ti3S49
ppb
75.64
.24
.3133
75.59
75.90
75.43
Chk Pass
2rS391-2
ppb
3.857
3.174
82,30
3.004
7.370
1.196
Chk Pass
Ti3S49-2
ppb
74.01
.83
1.119
73.25
73.88
74.89
Chk Pass
Til 908
ppb
.9958
1.851
185.9
-.5509
3.047
.4915
Chk Pass
U_2635
ppb
-4.240
14.61
344.7
-15.35
-9-042
12.17
Chk Pass
U_3354
ppb
-24.66
8.36
33.88
-30.33
-15.06
-28-58
Chk Pass
U_4090
ppb
20.40
13.66
66.95
6.769
34.08
20.35
Chk Pass
V_2924
ppb
13.04
.57
4.391
12.94
13.66
12.52
Chk Pass
Zn2138
ppb
99.84
.32
.3189
1002
99.81
99.54
Chk Pass
Zn213a-2
ppb
94.75
.76
.8013
95.28
93.88
95.09
Chk Pass
2/25/200913:52:12
4
Sample Name: 0902040-01 Acquired: 2/25/2009 11:29:33 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
24027.
61.
.25511
Y 3600
Cls/S
165500.
487.
.29410
Y 3710
Cls/S
19507.
52.
.26503
23956. 164930. 19487.
24062. 165940. 19566.
24062. 165600. 19469.
88^98951
c^^
Sample Name: 0902040-SR[^ Acquired: 2/25/2009 11:37:15 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1 OOOOOO
User: admin Custom IDl: Custom ID2: Custom ID3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
high Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#S
Check?
High Limit
Low Limit
Ag3280
ppb
-.3221
.6040
187.5
-.5354
-.7906
.3596
Chk Pass
Be3130-2
ppb
.1064
.0351
79-94
.0758
.0409
.2025
Chk Pass
All 670
ppb
665.4
84
1263
659.9
675.0
661.1
Chk Pass
Bi2230
ppb
-1.900
1.081
56.89
-3.013
-.8542
-1.833
Chk Pass
AI3961
ppb
591.2
33.0
5.587
570.6
573.7
629.3
Chk Pass
CaS179
ppb
11970.
214.
1.787
11860.
11830.
12210.
Chk Pass
Asl890
ppb
1.982
1.466
73.97
2.745
.2917
2.909
Chk Pass
Ca39S3
ppb
F11800.
169.
1.433
11990.
11680.
11730.
Chk Fail
10000.
-10000.
B_2089
ppb
9.324
.010
.1107
9.327
9.332
9.312
Chk Pass
Cd228S
ppb
-.0553
-1142
206.8
.0555
-.0486
-.1727
Chk Pass
Ba4554
ppb
23.90
.23
.9653
24.07
23.99
23.64
Chk Pass
C02286
ppb
.4120
-0888
21.56
.4989
.3214
.4157
Chk Pass
Ba4554-2
ppb
22.35
.61
2.719
22.50
21.63
22.87
Chk Pass
Cr2677
ppb
1.493
.159
10.65
1.316
1.624
1.539
Chk Pass
Be2S48
ppb
.0082
.0100
121.9
.0132
-.0033
.0146
Chk Pass
Cu2178
ppb
1.256
.765
60.90
.5248
2.051
1.193
Chk Pass
Be2348-2
ppb
-.0877
.2244
255.8
-.1030
-.3040
.1439
Chk Pass
Cu2199
ppb
2.911
1.716
53.92
2.855
4.654
1.225
Chk Pass
BeS130
ppb
.0839
.0247
29.47
.0572
.0885
.1059
Chk Pass
CuS273
ppb
9.323
3.906
41.89
13.68
6.135
8.154
Chk Pass
2/25/2009 13:52:12
2
Sample Name: 0902040-SRD1
Method: METHOD DVP(vl14)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 11:37:15 Type: Unk
Mode: CONC Con. Factor; 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
625.1
13.4
2.149
615.9
618.8
640.5
Chk Pass
Ni2S16
ppb
1-952
.223
11.42
1.698
2.039
2.118
Chk Pass
F62714
ppb
605.9
17.1
2.815
615.4
616.1
586.2
Chk Pass
P_1774
ppb
55.45
1.06
1.905
56.05
54.23
56.07
Chk Pass
K_7664
ppb
724.3
73.3
10.12
663.8
703.3
805.9
Chk Pass
Pb2203
ppb
1.391
.231
20.19
1.566
1.541
1.067
Chk Psss
Li6707
ppb
2.879
1.634
56.75
3.439
4.158
1.038
Chk Pass
Sb2068
ppb
.3522
.9434
267.9
-.2247
-.1596
1.441
Chk Pass
Mg2790
ppb
3474.
30.
2.305
3459.
3403.
3561.
Chk Pass
Sel960
ppb
-.9488
1.171
123.4
-1.806
-1.426
.3350
Chk Pass
Mg2852
ppb
3531-
72.
2-051
3491.
348 7.
3615.
Chk Pass
312124
ppb
1714.
19.
1.101
1702.
1736.
1704.
Chk Pass
Mn2576
ppb
36.27
.42
1.167
36.47
36.55
35.78
Chk Pass
Si2124-2
ppb
1603.
4.
.2367
1607.
1604.
1599.
Chk Pass
Mn2576-2
ppb
36.74
.83
2.250
35.95
36.66
37.60
Chk Pass
Sn1899
ppb
.3090
.0940
30-42
.3431
.3812
.2027
Chk Pass
Mo2020
ppb
-8635
.1270
14.71
.7603
1.005
.8249
Chk Pass
Sr2l65
ppb
94.27
1.16
1.230
93.66
95.61
93.55
Chk Pass
Na5S95
ppb
37360.
70S.
1.883
37050.
36850.
38160.
Chk Pass
Sr4215
ppb
97.11
1.85
1.901
96.47
95.67
99.19
Chk Pass
69^8895^
a^*5^f^
N^ Ol
Sample Name: 0902O4O-SRD>^ Acquired: 2/25/2009 11:37:15 Type: Unk
Method: METHOD DVP(vll4) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
»2
#3
Check?
High Limit
Low Limit
Th28S7
ppb
-.5759
.8968
155.7
-1.187
.4536
-.9944
Chk Pass
Zr339l
ppb
-6397
.0347
5.430
.6197
.6196
.6798
Chk Pass
Ti3349
ppb
15.52
.06
.4149
15.58
15.45
15.51
Chk Pass
Zr3391-2
ppb
.6663
.6023
90.39
.9465
1.077
-.0250
Chk Pass
Ti3349-2
ppb
14.56
1.89
12.98
15.87
12.39
15.41
Chk Pass
TII 903
ppb
1.076
.812
75.48
1.560
.1384
1.529
Chk Pass
U_2635
ppb
31.75
14.39
45.34
27.10
20.25
47.39
Chk Pass
U_3854
ppb
-43.39
42.89
98.85
-84.99
.6908
-45.88
Chk Pass
U_4090
ppb
15.93
3.92
24.59
20.22
15.02
12.54
Chk Pass
V_2924
ppb
2.404
.383
15.43
2.899
2.411
2143
Chk Pass
Zn2138
ppb
20 03
.24
1.209
19.96
20.30
19.83
Chk Pass
Zn2138-2
ppb
19.87
.35
1.775
20.07
19.47
20.09
Chk Pass
2/25/200913:52:12
4
Sampte Name: 0902040-SRD1
Method: METHOD DVP{vl 14)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 11:37:15 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
Int. Std-
Units
Avg
Stddev
%RSD
#1
#2
#3
Y_2243
Cts/S
24548.
140.
.57148
24659.
24390.
24595.
Y 3600
Cts/S
172330.
1885.
1.0937
172120.
170570.
174320.
Y 3710
Cts/S
19518.
251.
1.2844
19601.
19717.
19237.
e%8g8e53
Sample Name
«^)?^^
^ ^V'^^3 ^ ^'^
: 0902040-DUIJ3^ Acquired: 2/25/2009 11:45:00
Meihod: METHOD DVP(v114) Mode: CONC
User admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Custom IDI:
AgS230
ppb
-.0336
.2912
865.5
-.3651
.0831
.1810
Chk Pass
BeS1S0-2
ppb
.0708
.0992
140.1
.1811
-.0111
.0423
Chk Pass
All 670
ppb
3039.
4.
.1377
3044.
3037.
3037.
Chk Pass
Bi2230
ppb
-3.085
1.445
46.33
-2.749
-1.839
^.669
Chk Pass
Custom ID2:
AI3961
ppb
2884.
7-
.2581
2893.
2880.
2880.
Chk Pass
Ca3179
ppb
59250.
442.
.7457
59030.
58970.
59760.
Chk Pass
Corr. Factor
Type:1
: 1.000000
Custom IDS:
As1890
ppb
4.588
.558
12.17
4.405
5215
4.145
Chk Pass
Ca39SS
ppb
F 54710.
260.
.4748
54460.
54700.
54980.
Chk Fail
10000.
-10000.
B_2089
ppb
45.85
.22
.4773
46.07
45.86
45.63
Chk Pass
Cd2288
ppb
.2539
.0255
10-05
.2454
.2826
.2338
Chk Pass
Jnk
Ba4554
ppb
115-5
.8
.7350
116.4
114.3
1152
Chk Pass
Co2286
ppb
1.759
.125
7.108
1.644
1.740
1.892
Chk Pass
Ba4554-2
ppb
115.0
12
1.040
114.1
114.5
116.4
Chk Pass
Cr2677
ppb
8.332
.118
1.422
8.205
8.440
8.351
Chk Pass
Be2348
ppb
.1235
.0285
23.12
.0942
.1249
.1512
Chk Pass
Cu2178
ppb
9.816
.356
3.629
9.430
9.383
10.13
Chk Pass
Be2348-2
ppb
-.0820
.3578
436.6
.0851
-.4928
.1618
Chk Pass
Cu2199
ppb
12.27
1.41
11.46
13.10
10.65
13.07
Chk Pass
BeSISO
ppb
.1782
.0167
9.356
.1937
.1605
.1305
Chk Pass
Cu3273
ppb
12.97
7.66
59.06
12.24
20.97
5.701
Chk Pass
2/25/2009 13:52:13
2
Sample Name: 0902040-DUP1 Acquired: 2/25/2009 11:45:00
Method: METHOD DVP(v114) Mode: CONC
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Custom IDI: <
Fe2599
ppb
3083.
35.
1.147
3070.
3056.
3123.
Chk Pass
Ni2316
ppb
8.903
.147
1.648
8.811
9.072
8.825
Chk Pass
Fe2714
ppb
2989.
IS.
.4444
3004.
2981.
2982.
Chk Pass
P_1774
ppb
281.9
1.4
.4837
283.5
281.3
281.0
Chk Pass
Custom ID2:
K_7664
ppb
3646.
83.
2.268
3662.
3556.
3719.
Chk Pass
Pb220S
ppb
5.412
.433
8.003
5.722
5.593
4917
Chk Pass
Corr. Factor
Type:l
:1.000000
Custom IDS:
Li6707
ppb
9.933
1.969
19.83
11.99
8.069
9.735
Chk Pass
Sb2068
ppb
3.356
.865
25.78
4.263
2.540
3.266
Chk Pass
Mg2790
ppb
17040.
126.
.7375
17000.
16940.
17180.
Chk Pass
Sel960
ppb
1.606
2.047
127.5
3.110
2.433
-.7256
Chk Pass
Jnk
Mg2852
ppb
F 17200.
94.
.5471
17140.
17150.
17310.
Chk Fail
10000.
-10000.
St2124
ppb
7861.
63.
.8043
7793.
7B60.
7924.
Chk Pass
Mn2576
ppb
177-7
1.6
.8899
179.5
176.7
176.9
Chk Pass
Si2124-2
ppb
7207.
33.
.4539
7172
7210.
7233.
Chk Pass
Mn2576-2
ppb
181.4
1.2
.6486
181.0
180.4
182.7
Chk Pass
Sn1399
ppb
1-408
.342
24.31
1.563
1.646
1.016
Chk Pass
Mo2020
ppb
4.066
.111
2.736
3.963
4.052
4.184
Chk Pass
Sr2165
ppb
454.9
1.7
.3639
456.8
454.2
453.7
Chk Pass
Na5395
ppb
183900.
1519-
.8258
183000.
183100.
185700.
Chk Pass
Sr4215
ppb
479.1
4.5
.9303
477.0
476.0
484.2
Chk Pass
8^^6sa
Sample Name: 0&02040-DUP>'
Meihod: METHOD DVP(vll4)
User: admin Custom ID1:
Comment:
Acquired: 2/25/2009 11 ;45;00 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom IDS;
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th23S7
ppb
.4140
.1833
44.27
.6071
.3925
.2424
Chk Pass
Zr3391
ppb
2.680
.297
11.09
2.709
2370
2963
Chk Pass
Ti3349
ppb
75.96
.71
.9313
76.74
75.37
75.77
Chk Pass
Zr3391-2
ppb
2.568
.733
28.54
1.805
3.267
2.631
Chk Pass
Ti3349-2.
ppb
76.77
.62
.3045
76.89
76.10
77.31
Chk Pass
TII 908
ppb
.3913
1.256
321.0
-.3796
-2873
1.841
Chk Pass
U_2635
ppb
6.588
10.11
1534
17.40
-2.624
4.934
Chk Pass
U_3854
ppb
-28.67
20.91
72.96
-7.312
-29.57
-49-11
Chk Pass
U_4090
ppb
16.71
20.19
120.8
6.940
3.262
39.92
Chk Pass
V_2924
ppb
13.08
.28
2.179
13.32
12.76
13.14
Chk Pass
Zn2133
ppb
101.2
.1
.0759
101-3
101.1
1012
Chk Pass
Zn2138-2
ppb
96.31
.39
.4025
95.89
96.39
96.66
Chk Pass
2/25/200913:5213
4
Sample Name: Q902040-DUP1
Method: METHOD DVP(vll4)
User: admin Custom IDl:
Comment:
/Acquired: 2/25/2009 11:45:00 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
InL Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
23917.
25.
.10402
Y 3600
Cts/S
166470.
618.
.37135
Y 3710
Cls/S
19401.
43.
.22008
23889. 165760. 19446.
23936. 166800. 10361.
23925. 166860. 19395.
969998^5
Sample Name; 0902040-MS^
Method: METHOD DVP(v114)
User; admin Custom IDI:
Comment:
Acquired: 2/25/2009 11:52:44 Type: Unk
Mode: CONC Corr. Factor: 1,000000
Custom ID2; Custom IDS:
2/25/2009 13:52:13
1
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Umit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Umit
AgS280\/
ppb
50.55
1.00
1.972
49.41
50.99
51.25
All 670
ppb
5543.
17.
.3100
5525.
5559.
5545.
Chk Pass Chk Pass
Be3130-2y
ppb
50.82
.45
.8789
51.22
50.90
50.34
Bi223Q
ppb
-3.148
.723
22.97
-2,421
-3.157
-3.867
Chk Pass Chk Pass
AI3961^
ppb
5536.
15.
.2639
5525.
5530.
5553.
Chk Pass 1
Ca3179^
ppb
83660-
391.
.4672
84090.
83570.
833S0.
Chk Pass
AS1890 ^
ppb
2030.
7.
.3602
2021.
2034.
2034.
3hk Pass
Ca3933
ppb
F 75450.
744-
.9861
76300.
74950.
75090.
Chk Fail
1OOOO,
-10000.
^ B_2039
ppb
1048.
3.
.3186
1044.
1050.
1049.
Chk Pass
Ba4554
ppb
2101.
16.
.7427
2118.
2087.
2099.
Chk Pass
Cd228S^ Co2286
ppb
50.06
21
.4227
50.06
49.85
50.27
Chk Pass
ppb
486.3
1.9
.3818
484.3
487.9
48^.8
Chk Pass
Ba4554-2 V
ppb
2140.
3.
.1488
2141.
2143.
2137.
Be2348
ppb
51.27
.23
.4495
51.23
51.06
51.52
Chk Pass Chk Pass
si Cr2677^
ppb
20S.2
1.1
.5211
205.3
204.1
206.3
Be2348-2
ppb
49.93
.43
.8619
50.40
49.56
49.32
Chk Pass
Cu2178^ Cu2199
ppb
257.2
3.2
1.258
253.3
259.8
253.6
Chk Pass Chk Pass
ppb
2523
1.3
.4971
250.9
252.7
253.4
Chk Pass
BeSlSO
ppb
50.97
.21
.4085
51.01
50.75
51.16
Chk Pass
Cu3273
ppb
261.0
4.5
1.732
266.1
259.8
257.3
Chk Pass
2^25/2009 13:52:13
2
Sampte Name: 0902040-MS1 Acquired: 2/25/2009 11:52:44 Type; Unk
Method: METHOD DVP(vl 14) Mode; CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Etem
Units
.^vg
Stddev
%RSD
#1 n
#3
Check?
High Limit
Low Limit
Fe2599 \f
ppb
4148.
9.
.2202
4154.
4151.
4137.
Fe2714
ppb
4069.
32.
.7878
4049.
4051.
4106.
Chk Pass Chk Pass
Ni2316'^
ppb
493-1
1-8
.3612
•491.1
494.6
493.7
P 1774
ppb
284.6
1.1
.4007
283.3
284.8
285.6
Chk Pass Chk Pass
K 7664 >y
ppb
28650.
144.
.5030
28820.
28580.
28560.
U6707
ppb
1023.
5.
.4438
1028.
1020.
1020.
Mg2790V
ppb
41190.
144.
.3503
41350.
41130.
41080-
Chk Pass Chk Pass Chk Pass
J
Pb2203^
ppb
477.1
2.4
.5092 474.6
479.5
477.2
Sb206fi ^
ppb
488.8
2.8
.5649
485.7
489.7
490.9
Chk Pass Chk Pass
Set960
ppb
1994.
6.
.3194
19S9.
2001.
1994.
Chk Pass
Mg2852
ppb
F41560.
169.
.4076
41660.
41650.
41360.
Chk Fail
10000.
-10000.
Si2124
ppb
9830-
35.
.3565
9739.
9850.
9849.
Chk Pass
Mn2576
ppb
677.6
1.8
.2607
678.3
675.6
679.0
Chk Pass
Si2124-2
ppb
9227.
46.
-4963
9231.
9179.
9271.
Chk Pass
Mn2576-2^ Mo2020
ppb ppb
670.2 1017.
2.4 4.
.3615 .3611
673.0 1013.
669.0 1019.
eeS.7 1020-
Chk Pass Chk Pass
Snl899 Sf216S
ppb ppb
960.9 1410.
28 5.
.2944 .3397
958.0 1405.
96S.7 1413.
961.0 1412.
Chk Pass Chk Pass
1
Na5895
ppb
20S500.
317.
.1522
208900.
208400.
208300.
Chk Pass
Sf4215
ppb
1499.
3.
.1749
1501.
1500.
1496.
Chk Pass
x/
8668993^
Sampie Name: 0902040-MS>'
Method: METHOD DVP(v114)
User: admin Custom IDI:
Acquired: 2/25/2009 11:52:44 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2; Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
low Limit
Th28S7
ppb
-.1510
2.485
1645.
.7191
1.782
-2.954
Chk Pass
Zr3391
ppb
2.990
.097
3.248
2881
3.021
3.068
Chk Pass
TiSS49
ppb
1085.
4.
.3564
1036.
1081.
1088.
Chk Pass
Zr3391-2
ppb
3.485
1.479
42.44
4.075
4.579
1.802
Chk Pass
Ti3349-2
ppb
1071-
9.
.8822
108O.
1062
1072.
Chk Pass
T(190a'^
ppb
1845.
9.
.4617
1836.
1853.
1847.
U_2635
ppb
-530.0
10.6
2.003
-530.7
-519.0
-540.2
Chk Pass Chk Pass
U_3854
ppb
-37-35
19.22
51.44
-23.46
-59.28
-29.32
Chk Pass
U_4090
ppb
27.50
16.71
60.76
8,643
33.40
40.47
Chk Pass
V_2924^
ppb
510.7
14
.2647
509.9
509.9
512.2
Zn21S8
ppb
605.9
2.1
.3391
603.5
607.3
606.8
Chk Pass Chk Pass
Zn2138-2
ppb
571.7
.8
-1463
572.5
570,9
571.7
Chk Pass
v/
2/25/200913:52:13
4
Sampte Name: 0902040-MSl Acquired: 2/25/2009 11:52:44 Type: Unk
Meihod: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User; admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std.
Unils
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
23702.
23.
.09836
Y 3600
Cls/S
163490.
678.
.41485
Y 3710
Cts/S
19513.
16.
.08303
23728. 162990 19495.
23682. 164260. 19525.
23697. 163220. 19519.
S89389K7
2/25/2009 13:52:13
1
Sampte Name: 0902040-02 Acquired: 2/25/2009 12:00:23 Type: Unk
Method: METHOD DVP(v114) Mode; CONC Con. Factor: 1.000000
User; admin Custom IDi: Custom tD2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Etem
Units
Avg
Stddev
%RSD
#1
#2
ff3
Check ?
High Limil
Low Umil
Ag3280
ppb
.2851
.5187
182.0
.1319
.8631
-.1398
Chk Pass
BeS130-2
ppb
.3188
.1149
36.05
.3447
4185
.1931
Chk Pass
All 670
ppb
7025.
13.
.1867
7040.
7019.
7016.
Chk Pass
Bi2230
ppb
-3.022
.847
28.02
-2.652
-2.423
-3.991
Chk Pass
AI3961
ppb
7225.
119.
1.652
7173-
7141.
7362.
Chk Pass
Ca3179
ppb
64580.
938.
1-452
64110.
63970.
65660.
Chk Pass
Asl890
ppb
6.356
.678
10.67
6.139
7.116
5.813
Chk Pass
Ca3933
ppb
F 58990,
246.
.4165
59180.
58710.
59090.
Chk Fail
10000.
-10000.
B_20S9
ppb
50.76
.52
1.024
51.36
50.42
50.50
Chk Pass
Cd2288
ppb
.5329
.1075
20.13
.6464
.5198
.4325
Chk Pass
Ba4554
ppb
183.9
.3
.1496
183.7
183.9
184.3
Chk Pass
Co2286
ppb
S.752
.203
5.421
3.837
3.850
3.518
Chk Pass
Ba4554-2
ppb
182.6
2.9
1.598
181.3
180.6
136.0
Chk Pass
Cr2677
ppb
14.30
.31
2.193
14.66
14.08
1417
Chk Pass
Be2348
ppb
.2575
.0483
18.75
.2774
.2927
.2025
Chk Pass
Cu2178
ppb
14.37
1-60
11.10
14.66
12.65
15.80
Chk Pass
Be2S48-2
ppb
-.1716
.1589
92,59
-.0005
-.3145
-.1998
Chk Pass
Cu2199
ppb
15.93
.13
.8293
16.07
15.92
15-80
Chk Pass
BeSlSO
ppb
-3288
.0133
4.058
.3133
.3334
.3393
Chk Pass
CuS27S
ppb
21.39
9.52
44.52
10.51
28.23
25.43
Chk Pass
Sample Name: 0902040-02 Acquired: 2/25/2009 12:00:23 Type; Unk
Method: METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom ID 1: Custom ID2: Custom IDS:
Comment:
2/25/2009 13:52:13
2
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
7677.
105.
1.369
7635.
7599.
7797.
Chk Pass
Ni2316
ppb
13.96
.33
2.351
13.80
14.33
13.73
Chk Pass
Fe2714
ppb
7512.
20.
.2607
7506.
7497.
7534.
Chk Pass
P_1774
ppb
501.4
.8
.1525
501.8
500.5
501.9
Chk Pass
K_7664
ppb
4829.
142.
2.941
4742.
4752.
4993.
Chk Pass
Pb2203
ppb
7.85S
.610
7.769
7.218
8.435
7.906
Chk Pass
Li6707
ppb
12.92
-84
6.538
12.85
13.79
12.11
Chk Pass
Sb2068
ppb
5.447
1.084
19.90
4.660
4.997
6.683
Chk Pass
Mg2790
ppb
19250.
334.
1.736
19120.
18990.
19620.
Chk Pass
Sel960
ppb
3.892
2.882
74.06
6.263
.6358
4.721
Chk Pass
Mg2852
ppb
F 19520.
279.
1.428
19390.
19330.
19840.
Chk Fail
10000.
-10000.
Si2124
ppb
16120.
52.
.3249
16120.
16060.
16170.
Chk Pass
Mn2576
ppb
319.2
1.5
.4543
318.3
318.5
320.9
Chk Pass
Si2124-2
ppb
15220.
146.
.9620
15330.
15110.
15160.
Chk Pass
Mn2576-2
ppb
318.2
3.3
1.188
317-1
315.1
322.4
Chk Pass
Sn1899
ppb
1.281
.365
28.48
1.665
1.238
.9395
Chk Pass
Mo2020
ppb
5.515
.109
1.972
5.425
5.636
5.484
Chk Pass
Sr2165
ppb
533.0
.8
.1564
533.8
532.8
532-2
Chk Pass
Na5895
ppb
208700.
2599.
1.245
207400.
207100.
211700.
Chk Pass
Sr4215
ppb
565.7
8.7
1.538
560.8
560.4
575.7
Chk Pass
Sample Name: 0902040-02 Acquired: 2/25/2009 12:00:23 Type: Unk
Method: METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2; Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th28S7
ppb
2.723
2.306
84.65
3.397
4.617
.1561
Chk Pass
Zr3391
ppb
5.357
.307
5.734
5.293
5.087
5.691
Chk Pass
Ti3349
ppb
227.2
1.3
.5922
227.1
226.0
228.6
Chk Pass
Zr3391-2
ppb
5.237
.987
18-84
6,270
4304
5.138
Chk Pass
Ti3349-2
ppb
227.4
2.7
1.192
228.4
224.3
229.4
Chk Pass
TII 908
ppb
1.465
1.544
105.4
2-463
-.3137
2.246
Chk Pass
U_2635
ppb
-9.689
4.851
50.07
-5.436
-8.656
-14.97
Chk Pass
U_3854
ppb
-79-36
26.91
33.91
-106.3
-79.30
-52.48
Chk Pass
U_4090
ppb
10.74
15.91
148.1
11.51
26.25
-5.541
Chk Pass
V_2924
ppb
23.90
.21
.8980
23.65
24.03
24.01
Chk Pass
Zn2138
ppb
140.2
.2
.1250
140.0
140.2
140.3
Chk Pass
Zn2138-2
ppb
133.1
.5
.3399
133.7
132.8
132.7
Chk Pass
2/25/200913:52:13
4
Sample Name: 0902040-02 Acquired: 2/25/2009 12:00:23 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: l.OOOOOO
User; admin Custom IDl: Custom ID2: Custom IDS;
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
24152
12-
.05109
2414 :i.
24146.
24166.
Y 3600
Qs/S
165880-
628.
.37367
166590
165390.
165670.
Y 3710
as/s 19522
63.
.32418
10481.
19594.
19489.
9889^^5
2/25/2009 13:52:13
1
Sample Name: 0812092-01 Acquired; 2/25/2009 12:08:03 Type: Unk
Method: METHOD DVP{v114) Mode: CONC Corr. Factor; 1.000000
User: admin Custom IDI: Custom ID2: Custom IDSj
Comment:
ol,T=€.,r^v\,T4; <Tf\y^
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limil
Low Limit
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Ag3280
ppb
-.6194
.2245
36.25
-.3685
-.6882
-.8015
Be3130
ppb
-.1427
.0157
11.02
-.1294
-.1386
-.1601
All 670
ppb
57.21
.32
.5590
56.85
57.34
57.45
AI3961
ppb
91.11
9.14
10.03
98.23
9429
80.80
/\s1890
ppb
2.922
1.275
43.65
1-608
3.002
4.155
6^2089
ppb
172.6
.8
.4694
171.9
173.5
172.5
Ba4554
ppb
11.51
.42
3.671
11.30
11.24
12.00
Ba4554-2
ppb
10.45
.35
3.362
10.05
10.71
10.58
Be2348
ppb
.3563
-0280
7.870
.3247
-3782
.3661
BeS 130-2
ppb
-.0644
.1425
221-2
-.0272
-.2218
.0558
Bi22S0
ppb
-.7662
2.214
289.0
-2.188
-1.895
1.785
Ctik Pass Chk Pass Chk Pass
Ca3179
ppb
F 507900.
15640.
3.079
489900.
• 515200.
518600.
Chk Fail
500000.
-500000.
Ca3933
ppb
Cd2288
ppb
3.257
.090
2.778
3.178
3.237
3.356
y Co2286
ppb
49.54
.28
.5729
49.23
49.62
49.78
Cr2677
ppb
.3083
.4616
149.7
-.1925
.4007
.7167
Be2S48-2
ppb
.2206
.1263
57.25
.3339
.2434
.0845
Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass
Cu2178
ppb
2.329
2796
120.0
-.8486
3.424
4.412
Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass
2/25/200913:52:13
2
Sampte Name: 0812092-01
Method: METHOD DVP(v114)
User: admin Custom IDI;
Comment:
Acquired: 2/25/2009 12:08:03 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Cu2199
ppb
5.152
2-135
41-44
7.608
3.742
4.106
Chk Pass
Mn2576-2^
ppb
5340.
63.
1.176
5289.
5320.
5410.
Chk Pass
Cu3273
ppb
26.72
8.14
30.46
19.85
35.71
24.60
Chk Pass
Mo2020
ppb
11.26
.24
2.109
11.26
11.03
11.51
Chk Pass
Fe2599^/
ppb
8334.
105.
1.258
8255.
8295.
8453.
Chk Pass
Na5895
ppb
241800.
2805.
1.160
239100.
241700.
244700.
Chk Pass
Fe2714
ppb
8512.
305.
3.583
8359.
8314.
8863.
Chk Pass
Ni2316
ppb
61.39
.44
.7129
60.83
61.64
61.63
Chk Pass
K^7664
ppb
14230.
144
1.013
14090.
14230.
14380.
Chk Pass
P_1774
ppb
2.673
.444
16-60
2510
3.175
2.333
Chk Pass
116707
ppb
368.5
8.8
2.399
362.1
364.8
378.6
Chk Pass
Pb2203
ppb
-4.883
.851
17.43
-3.924
-5.174
-5.550
Chk Pass
Mg2790
ppb
227700.
3038.
1.334
225200.
226900.
231100.
Chk Pass
Sb2068
ppb
.9164
2.172
237.0
S.16S
-1.172
.7579
Chk Pass
Mg2852
ppb
F 213100.
7520.
3-529
217000.
204400.
217900.
Chk Fail
10OOO.
-10000.
Sel960
ppb
-1.223
1.981
161.9
-.4151
.2258
-3.481
Chk Pass
Mn2576
ppb
S557.
170.
3.061
5474.
5444.
5753.
Chk Pass
Si2124
ppb
5644.
31.
.5470
5609.
5668.
5656.
Chk Pass
Sample Name: 0812092-01 Acquired; 2'25'200g 12:08:03 Type: Unk
Meihod: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
»2
#3
Check?
High Limit
Low Limit
Si2124-2
ppb
5239.
53.
1.005
5208.
5210.
5300.
Chk Pass
U_S854
ppb
-65.77
11.13
16.99
-7410
-70.14
-53.07
Chk Pass
Sn1899
ppb
.4553
-2491
54-72
.2068
.7051
.4539
Chk Pass
U_4090
ppb
16-82
16.89
100.5
-2.671
27.32
25.81
Chk Pass
Sr2165
ppb
11590.
73.
.6316
11510.
11650.
11600.
Chk Pass
V_2924
ppb
18.42
99
6.035
16.03
15.68
17.54
Chk Pass
Sr4215
ppb
12510.
92.
.7322
12450.
12460.
12610.
Chk Pass
Zn2138
ppb
145-9
.9
.5891
145.0
146.7
146.0
Chk Pass
Th2837
ppb
.4255
1.264
296.9
.8070
-.9348
1.454
Chk Pass
Zn2138-2
ppb
133.9
1.4
1.020
132.5
134.0
135.2
Chk Pass
TiS349
ppb
1-796
.049
2.705
1.852
1.762
1.775
Chk Pass
Zr3391
ppb
-.3677
.1843
50.13
-.5279
-.1662
-.4091
Chk Pass
TiS349-2
ppb
4.362
2.110
48.37
6.734
2.694
3.657
Chk Pass
Zr3S91-2
ppb
,9113
,6132
67.29
1.585
.7638
.3854
Chk Pass
Til 908
ppb
-2.<tt4
.968
32.93
-2.346
-2.405
-4.051
Chk Pass
U_2635
ppb
a4.5i
20.01
23.67
99.03
92.32
61.69
Chk Pass
2/25/200913:52:13
4
Sampte Name: 0812092-01 Acquired: 2/25/2009 12:08:03 Type: Unk
Method: METHOD DVP(v114) Mode; CONC Corr. Factor: 1 .OOOOOO
User: admin Custom IDl: Custom ID2; Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cls/S
22339.
88.
.39186
22437.
22361
22318.
Y 3600
Cts/S
153410.
4265.
2.7801
155070.
156590.
148560.
Y 3710
as/s 19265.
191.
.99180
19421.
19324.
19052.
SBS^^St
2/25/200913:52:13
1
Sample Name: 0812092-SRD2 Acquired: 2/25/2009 12:16:10 Type: Unk
Method; METHOD DVP(vl 14) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umil
Low Limit
AgS280
ppb
-.1309
.1152
37.97
-.0329
-.2578
-.1022
Chk Pass
BeS130-2
ppb
.0224
.1044
465.1
.0157
-.0784
.1301
Chk Pass
/yi670
ppb
14.24
-51
3.560
14.63
13.67
14.43
Chk Pass
Bi2230
ppb
-1.239
.350
28.23
-.9978
-1.079
-1.640
Chk Pass
AI3961
ppb
19.78
8.00
40.44
21.63
26.69
11.02
Chk Pass
Ca3179
.ppb
106200.
99.
.0932
106200.
106000.
106200.
Chk Pass
As1890
ppb
2181
1.278
58.62
3.039
.7114
2.791
Chk Pass
Ca39S3
ppb
F 92780.
129.
.1384
92640.
92890.
92820.
Chk Fail
10000.
-10000.
B_2089
ppb
36.29
.54
1.482
35.74
36.32
36.81
Chk Pass
Ba4554
ppb
2.334
.031
1.S22
2.364
2.336
2.303
Chk Pass
/
Cd2288 Co2286
ppb ppb
.7532 10.56
.0193 .14
2.564 1.361
.7702
.7322
.7572
Chk Pass
10.52
10.45
10.72
Chk Pass
Ba4554-2
ppb
2.043
.534
26.13
2.563
1.501
2.061
Chk Pass
Cr2677
ppb
.0681
.1050
154-3
.0000
.0152
.1890
Chk Pass
Be2348
ppb
.0935
.0284
30.35
.0622
.1175
.1009
Chk Pass
Cu2173
ppb
1.249
1.939
155.3
3.350
.8682
-.4716
Chk Pass
Be2348-2
ppb
.0329
.3652
1110.
-.2193
-.1336
.4517
Chk Pass
Cu2199
ppb
1.218
.114
9.333
1.192
1.120
1.342
Chk Pass
Be3130
ppb
.0286
.0223
77.70
.0325
.0047
.0437
Chk Pass
Cu3273
ppb
8.768
9.381
107.0
14.06
14.31
-2.063
Chk Pass
2/25/2009 13:52:14
2
Sampte Name: Oai2092-SRD2
Method: METHOD DVP(v114)
User: admin Custom ID 1:
Comment:
Acquired: 2/25/2009 12:16:10 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2; Custom ID3:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Fe2599^
ppb
17S7.
4.
.2462
1740.
1738-
1732
Fe2714
ppb
1722
14.
.8189
1727-
1733.
1706.
Chk Pass Chk Pass
Ni2316V
ppb
13.22
.14
1.060
13.13
13.38
13.14
P 1774
ppb
1.785
.672
37.65
2.227
2116
1.012
Chk Pass Chk Pass
K_7664
ppb
2879.
31.
1.079
2893.
2901.
2844.
Chk Pass
Pb2203
ppb
-.5178
.6609
127.6
.1121
-1.206
-.4597
Chk Pass
116707
ppb
74.18
1.59
2.141
75.95
73.70
72.89
Chk Pass
Sb2068
ppb
.7474
.2535
33.92
.5558
1.035
.6516
Chk Pass
Mg2790
ppb
47520.
147.
.3086
47550.
47360.
47650.
Chk Pass
Sel960
ppb
-.2893
3.446
1191.
-t213
2.250
1.094
Chk Pass
Mg2852
ppb
F 47200.
130.
.2754
47260.
47050.
47290.
Chk Fail
10000.
-1 OOOO.
312124
ppb
1142.
13.
1.112
1137.
1132.
1156.
Chk Pass
Mn2576
ppb
1133.
9.
.8174
1142.
1132
1124.
Chk Pass
Si2124-2
ppb
1054.
18.
1.722
1061.
loss.
1068-
Chk Pass
Mn2576-2 Mo2020
ppb
1123.
1.
.1228
1124.
1122.
1122.
Chk Pass
Sn1899
ppb
.1618
.3138
193.9
-.1659
.4595
.1918
Chk Pass
ppb
2.338
.114
4.856
2.209
2.425
2.380
Chk Pass
Sr2165
ppb
2442.
31.
1.256
2426.
2423.
2478.
Chk Pass
Na5895
ppb
49540.
92.
.1850
49590.
49430.
49590.
Chk Pass
Sr4215
ppb
2525.
4.
.1701
2530.
2522.
2525.
Chk Pass
SCOw
Sampte Name: 0812092-SRD2 Acquired; 2'25/2009 12:16:10 Type; Unk
Method: METHOD DVP(v114) Mode: CONC Con. Faaor: 1.000000
User admin Custom IDl: Custom 1D2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
Check ?
High Limit
Low Limil
Elem
Units
Avg
Stddev
%RSD
#1
rf2
#3
Check?
High Limit
Low Limil
Th2337
ppb
.8889
3.062
344.5
.5731
4.097
-2.003
Chk Pass
2rS391
ppb
-.1738
-1752
100.8
-.2771
-2727
.0285
Chk Pass
Ti3349
ppb
4-124
.083
2.133
4.217
4.113
4.042
Chk Pass
ZrS391-2
ppb
1.679
.613
36.52
1.127
1.571
2.338
Chk Pass
Ti3349-2
ppb
3-845
1.206
31.35
4.732
4.331
2.473
Chk Pass
Til 908
ppb
-.5265
.9682
133.9
.1031
-.0411
-1.641
Chk Pass
U_2635
ppb
41.93
9.54
22.75
31.11
45.55
49.13
Chk Pass
U_3854
ppb
-23.63
7.14
30-20
-20.64
-13.48
-31.78
Chk Pass
U_4090
ppb
16.50
8.72
52.81
23.29
6.673
19.56
Chk Pass
V_2924
ppb
11.74
.32
2.736
1203
U.80
11.39
Chk Pass
2n21S8
ppb
29.94
.36
1.199
29.71
29.75
30.35
Chk Pass
Zn2138-2
ppb
28.25
-62
2.191
28.95
28.02
27.78
Chk Pass
2/25/2009 13:52 14
4
Sample Name: 0812092-SRD2
Method: METHOD DVP(v114)
User: admin Custom IDl:
Comment:
/Quired: 2/25/2009 12:16:10 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom IDS:
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
Cts/S
23405.
147.
.62996
Y 3600
Cts/S
164710.
1161.
.70513
Y 3710
Cts/S
18771.
101.
.53650
#1
#2
#3
23510. 163410. 13727.
23469. 165080. 18886.
23237. 165640. 18699.
8998^893
2/25/200913:5214
1
Sample Name: 0ai2092-DUP;
Method: METHOD DVP(vii4)
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1 n
#3
Check ?
High Limil
Low Limit
Custom IDI:
Ag3280
ppb
-.4146
.4918
118.6
-.5413
-.3303
.1283
Chk Pass
Be3130
ppb
-.1425
-0297
20.83
-.1753
-.1346
--117S
Chk Pass
> Acquired; 2/25/2009 12:23:54 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2:
All 670
ppb
61.30
1.25
2.039
60.10
6260
61.20
Chk Pass
BeS 130-2
ppb
-.1587
.1153
72.67
-.2851
-.0591
-.1320
Chk P3S5
AI3961
ppb
89.78
16-85
18.77
75.10
1082
86.07
Chk Pass
Bi2230
ppb
-.9919
1.976
199.3
-.5506
-3.152
.7266
Chk Pass
Custom IDS:
As1890
ppb
.6564
1.089
166.0
.3333
1.871
-.2350
Chk Pass
Ca3179
ppb
F 512400.
11530.
2.250
525300.
508500.
503300-
Chk Fail
500000.
-500000.
B_2089
ppb
173.7
2.4
1.410
171.9
176.5
172.7
Chk Pass
CaS933
ppb
'•
Chk Pass
Ba4554
ppb
11.23
.09
.8039
11.18
11.17
11.33
Chk Pass
Cd2283
ppb
3.379
.125
3.709
3.410
3.436
3.242
Chk Pass
Ba4554-2
ppb
10.81
.18
1.660
10.87
10.61
10.96
Chk Pass
Co2286
ppb
49.84
.71
1.431
49.22
50.62
49.68
Chk Pass
Be2348
ppb
.3470
.0079
2.267
.3558
.3444
.3408
Chk Pass
Cr2677
ppb
.5643
.4769
84.51
.9509
.7106
.0314
Chk Pass
Be2348-2
ppb
.1355
.0675
49.84
.0583
.1834
.1643
Chk Pass
Cu2l78
ppb
.6317
1.344
212.7
1.449
-.9191
1.366
Chk Pass
2/25/2009 13:52:14
2
Sample Name: 08l2092-t3UP2
Method; METHOD DVP(vl14)
User: admin
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Custom IDl:
Cu2199
ppb
4.884
1.356
27.77
4.493
6.392
3.766
Chk Pass
Mn2576-2
PPb
6375.
11.
.2053
5374
5365.
538?.
Chk Pass
1 AT/iuired: 2/25/2009 12:23:54 Type: Unk
Mode: CONC Corr
Custom ID2:
Cu3273
ppb
2820
8.45
29.96
35.60
19.00
30.01
Chk Pyss
Mo2020
ppb
11.16
.08
.7301
11.08
11.16
1124
Chk Pass
v/
Fe2599
ppb
8441.
11.
.1344
8434.
8436.
3454.
Chk Pass
Na5895
ppb
243700-
361.
.3532
243000.
243400.
244600.
Chk Pass
.Factor: 1.000000
Custom IDS
Fe2714
ppb
8434.
72.
.3563
8386.
8398.
8517.
Chk Pass
Ni2316^
ppb
62.19
1.00
1.611
61.45
63.33
61.79
Chk Pass
K^7664
ppb
14460.
52.
.3573
14520.
14420.
14440.
Chk Pass
PJ774
ppb
• 2732
.705
25.80
2.975
3.283
1.937
Chk Pass
Li6707
ppb
371.7
29
.7913
368.4
374.2
3725
Chk Pass
Pb2203
ppb
-4.737
.141
2.976
-4.744
^.874
-4.593
Chk Pass
Mg2790
ppb
231600.
442.
.1910
231300.
231400.
232100.
Chk Pass
Sb2068
ppb
-1.145
1.256
109.7
-2.264
.2132
-1.334
Chk Pass
Mg2852
ppb
F 277400.
1101.
.4949
223700.
222200.
221500.
Chk Fail
10000.
-10000.
Sel960
ppb
-2.409
2.116
87.35
-4.814
-1.580
-.8328
Chk Pass
Mn2576
ppb
5497.
30.
.5440
5531.
5485.
5475.
Chk Pass
Si2124
ppb
5667.
75.
1.327
5603.
5750.
5648.
Chk Pass
9^S9889ii
iy^5/:iiuuy is:a.^:i4
3
Sample Name: 0812092-DUP2 Acquired: 2/25/2009 12:23:54 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor; 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limit
Si2124-2
ppb
5204.
36.
.6854
5163.
5221.
5227.
Chk Pass
U_3854
ppb
-48.25
19.71
40.85
-55.25
-63.51
-26.00
Chk Pass
Sn1899
ppb
.7652
.2664
34.82
.9507
.4599
.8849
Chk Pass
U_4090
ppb
-9.880
26.97
273.0
-7.943
-37.77
16.07
Chk Pass
Sr2165
ppb
11740.
160.
1.362
11600.
11910.
11700.
Chk Pass
V_2924
ppb
17.16
.47
2.735
17.23
16.66
17.59
Chk Pass
Sr4215
ppb
12490.
24.
.1921
12470.
12490.
12520.
Chk Pass
Zn21S8
ppb
154.3
2.4
1.556
152.3
157.0
153.6
Chk Pass
Th2837
ppb
-.4457
1.581
354.7
-1.390
1.380
-1.327
Chk Pass
Zn2138-2
ppb
140.8
1.2
.8419
139.9
140.4
142.1
• Chk Pass
Ti3349
ppb
2.426
.406
16-72
2.891
2.237
2.149
Chk Pass
Zr3391
ppb
-.2105
.1297
61.64
-.1376
-.3501
-.0937
Chk Pass
Ti 3349-2
ppb
6-974
3.154
45.22
6.487
4.093
10.34
Chk Pass
Zr3391-2
ppb
3.298
2.495
75.65
.4203
4.615
4.858
Chk Pass
TII 908
ppb
-2.395
1.304
54.42
-3.524
-.9686
-2.693
Chk Pass
U_2635
ppb
77.93
13.71
17.60
89.35
62.72
81.72
Chk Pass
2/25/2009 13:52:14
4
Sampte Name: 0812092-DUP2
Method: METHOD DVP(v114)
User: admin Custom IDl:
Comment:
Acquired: 2/25/2009 12:23:54 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom ID3:
Int. Sid.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y^2243
Cls/S
21793.
228-
1.0447
22023.
21567
21788.
Y 3600
Cts/S
150430.
680.
.45173
150990.
150750.
149710.
Y 3710
Cta/S
18092
122.
.67669
18196.
18123.
17957.
89^^99
Sample Name: 0S12092-MS2
Method: METHOD DVP(v114)
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#2
#3
Check?
High Limit
Low Limit
Custom IDl:
AgS280
ppb
50.73
.82
1.611
51.07
49.80
51.32
Chk Pass
Be3130
ppb
50.62
.72
1.416
50.84
49.82
51.20
Chk Pass
Acquired : 2/25/2009 1231:59 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2:
All 670
ppb
2165-
7.
.3243
2173.
2161.
2162
Chk Pass
BeS 130-2
ppb
49-65
.28
.5580
49.68
49.36
49.91
Chk Pass
AI3961
ppb
2131.
8.
.3643
2139.
2131.
2124,
Chk Pass
Bi2230
ppb
-4.937
.636
12.89
-5.174
-4216
-5.420
Chk Pass
Custom IDS:
AS1890
ppb
2091.
4,
.1905
2096.
2088.
2090.
Chk Pass
Ca3179
ppb
F 538700.
6768.
1.256
533400.
546400.
536400.
Chk Fail
500000.
-500000.
B_2089
ppb
1167.
2.
.1734
1170.
1166.
1167.
Chk Pass
Ca3933
ppb
" —
Chk Pass
Ba4554
ppb
1988.
15.
.7561
1996.
1970.
1997.
Chk Pass
y/
Cd2233
ppb
53.52
.13
.2406
53.64
53.38
53.54
Chk Pass
Ba4554-2
ppb
2053.
2.
.0973
2051.
2053.
2055.
Chk Pass
Co2286
ppb
529.5
1,3
.2463
530.9
528.3
529.4
Chk Pass
Be2348
ppb
52.34
.68
1.303
52.66
51.56
5281
Chk Pass
Cr2677
ppb
198.0
3.0
1.53S
198.3
1949
200.9
Chk Pass
862348-2
ppb
51.49
21
.4056
51.63
51.60
51.25
Chk Pass
Cu2178
ppb
2452
1.9
.7670
243,3
247.1
245.1
Chk Pass
2/25/2009 14:07:35
2
Sampte Name: 0812092-MS2
Method: METHOD DVP(vll4)
User; admin Custom IDI:
Comment:
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#S
Check ?
High Limil
Low Umit
Cu2199
ppb
249.2
12
.4941
249.3
250.4
248.0
Chk Pass
Mn2576-2^
ppb
6008.
14.
.2259
5993.
6020.
6010.
Chk Pass
Acquired: 2/25/2009 12:31:59 Type: Unk
Mode' CONC Con. Factor: 1.000000
Custom ID2: Custom ID3:
Cu3273
ppb
272.2
2.1
.7858
274.7
271.0
271.1
Chk Pass
Mo2020
ppb
1041.
2.
.2380
1043.
1038.
1041.
Chk Pass
Fe2599
ppb
9527-
20.
.2142
9514.
9517.
9551.
Chk Pass
Na5895
ppb
274500-
503.
.1831
274400.
275400.
274700.
Chk Pass
Fe2714
ppb
9408.
128.
1.361
9459.
9263.
9503.
Chk Pass
Ni2316
ppb
544.0
1.1
2102
545.3
543.1
543.7
Chk Pass
K_7664
ppb
40590.
93.
.2301
40620.
40430.
40650.
Chk Pass
P_1774
ppb
2.746
.199
7.243
2.859
2.863
2.516
Chk Pass
U6707
ppb
1434.
4.
.3013
1430.
1438.
1435.
Chk Pass
Pb2203
ppb
459.6
.5
.1109
460.1
459.0
459.6
Chk Pass
Mg2790
ppb
261500.
371.
.1417
261200.
261400.
261900.
Chk Pass
Sb2068
ppb
488.9
3.6
.7326
4872
493.0
486.5
Chk Pass
Mg2852
ppb
F 245800.
868.
.3531
246700.
245000.
245500.
Chk Fail
10000.
-10000.
Sel960
ppb
2059.
3.
.3897
2067.
2059.
2051.
Chk Pass
Mn2576
ppb
6073.
76.
1.243
eo99.
5988.
6132
Chk Pass
312124
ppb
6644.
14.
.2048
6659.
6635.
6637.
Chk Pass
uSB^G^cuu
Sample Name: 0812092-MS2
Method: METHOD DVP(v114)
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
«1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limit
Custom IDI:
Si2124-2
ppb
6182.
41,
.6551
6144.
6224.
6178.
Chk Pass
U_3854
ppb
-54.00
24.17
44.75
-68.90
-66.98
-26.12
Chk Pass
Acquired: 2/25/2009 12:31:59 Type: Unk
Mode: CONC Corr. Factor. 1.000000
Custom ID2:
Sn1899
ppb
952.1
1.7
.1814
954.0
951.4
950.8
Chk Pass
U_4090
ppb
26.82
13.33
49.71
12.19
30.00
38.27
Chk Pass
Sr2165
ppb
12750-
32.
.2530
12790.
12720.
12750.
Chk Pass
V_2924
ppb
518.8
3.0
1.546
521.9
509.6
524.7
Chk Pass
Custom IDS:
Sr4215
ppb
13760.
19.
.1404
13740.
13780.
13760.
Chk Pass
Zn2138
ppb
661.3
1.3
2725
663.1
659.6
661.1
Chk Pass
Th2837
ppb
1.579
2.366
149.3
4.2B5
.5571
-.1040
Chk Pass
2n2138-2
ppb
610.1
2.0
.3277
609.3
608.3
612.3
Chk Pass
TiSS49
ppb
1018.
13.
1.315
1025.
1003.
1027.
Chk Pass
Zr3391
ppb
-.6902
.0983
14-24
-.6793
-.5975
--7933
Chk Pass
Ti3349-2
ppb
1013.
6.
.5450
101Q.
1010.
1020.
Chk Pass
Zr33gi-2
ppb
2.995
1.098
36.66
1,779
3.295
3.912
Chk Pass
TI1908
ppb
1770.
5.
.2563
1775.
1768.
1766.
Chk Pass
U_2635
ppb
-447.9
53.7
11.98
^57.6
-390.1
-496.1
Chk Pass
2/25/2009 14:07:36
4
Sample Name: 0812092-MS2
Method: METHOD DVP(vll4)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 12:31:59 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom fD2: Custom (D3:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
21051.
61.
.29023
20987
21108.
21058.
Y 3600
Cts/S
145020.
1407.
.96984
144860.
146510.
143710.
Y 3710
Cts/S
17366.
63.
.36348
17430.
17304.
17364.
Sample Name: CCV2 Acquired: 2/25/2009 12:40:37 Type: QC
Meihod: METHOD DVP(v114) Mode: CONC Con. Faclor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment: sy
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Unhs
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Ag3280
ppb
486.9
3.5
.7247
486.8
490.4
483.4
Chk Pass
Be3130-2
ppb
503.2
.6
.1190
503.4
503.6
502.5
Chk Pass
All 670
ppb
5426.
27-
.4936
5457.
5412.
5409-
Chk Pass
Bi2230
ppb
500.8
4.3
.8487
504.8
496.3
501.4
Chk Pass
A13961
ppb
5118.
33.
.7454
5147.
5075.
5133.
Chk Pass
CaS179
ppb
2069.
28.
1.357
2052.
2054.
2102.
Chk Pass
As1S90
ppb
496.0
25
.4973
497.3
493.2
497.6
Chk Pass
Ca3933
ppb
2100.
' 1.177
2078.
2095.
2127.
Chk Pass
B^2039
ppb
496.1
2.2
.4511
493.7
495-0
494.6
Chk Pass
Cd2288
ppb
499-4
2.3
.4675
502.1
497.9
498.3
Chk Pass
Ba4554
ppb
524.0
4.0
.7710
523.4
523.3
520.3
Chk Pass
002286
ppb
499-3
2.6
.5152
502.2
497.5
493.1
Chk Pass
Ba4554-2
ppb
509.8
1.0
.1916
509.6
509-0
510.9
Chk Pass
Cr2677
ppb
499-4
4.1
.8262
499.6
503-5
4952
Chk Pass
Be2S48
ppb
492.6
3-6
.7241
492.3
496.3
4892
Chk Pass
Cu2178
ppb
509-3
2-6
.5046
512.0
506.8
509-2
Chk Pass
Be2343-2
ppb
504.5
1.6
.3205
505.6
502.6
505.3
Chk Pass
CU2199
ppb
501-1
2.8
.5497
503.8
493.3
501-4
Chk Pass
BeSlSO
ppb
500.4
3.8
.7515
499.7
504.4
497.0
Chk Pass
Cu3273
ppb
494.8
6.6
1.340
488.3
494.6
501.5
Chk Pass
2/25/200913:52:14
2
Sample Name: CCV2 Acquired: 2/25/2009 12:40:37 Type: QC
Method: METHOD DVP(vl14) Mode: CONC Con. Faclor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#3
Check?
Value
Range
Fe2599
ppb
5048-
10.
.1956
5059.
5043.
5042.
Chk Pass
Nt2316
ppb
50S.7
2.3
.4562
506.0
501.4
503.6
Chk Pass
Fe2714
ppb
5009.
40.
-8079
4996.
5054.
4977.
Chk Pass
PJ774
ppb
1049.
6.
.6063
1056.
1046-
1045.
Chk Pass
K_7664
ppb
5157.
110.
2134
5253.
5180.
5037.
Chk Pass
Pb2203
ppb
499.3
.6
.1182
499.9
499.2
498.8
Chk Pass
U6707
ppb
4201.
10.
.2400
4206.
4207.
4189.
Chk Pass
Sb2068
ppb
502.3
1.8
.3629
504.4
501.2
501.4
Chk Pass
Mg2790
ppb
4134.
36.
.8676
4094.
4143.
4164.
Chk Pass
Sel960
ppb
497.7
3.4
.6832
501.3
494.5
497.3
Chk Pass
Mg2852
ppb
4096.
6.
.1436
4090.
4095.
4102.
Chk Pass
Si2124
ppb
547.1
1.4
.2495
548.6
546.7
546.0
Chk Pass
Mn2576
ppb
5125.
39.
.7604
5118.
5166.
5089.
Chk Pass
Si2124-2
ppb
535.2
18.1
3.378
514.4
546.9
544.4
Chk Pass
Mn2576-2
ppb
5084.
21.
.4058
5076.
5069.
5108.
Chk Pass
Snl899
ppb
494.1
2.3
.4597
496.7
4926
492.9
Chk Pass
Mo2020
ppb
503.2
2.0
.4064
505.4
501.3
502.9
Chk Pass
Sr2165
ppb
496.7
25
.5104
499-6
495.2
495.3
Chk Pass
Na5895
ppb
5348.
29.
.5370
5318.
5350.
5376.
Chk Pass
Sr4215
ppb
510.6
1.8
.3499
509.2
510.1
512.6
Chk Pass
2/25/2009 13:5214
3
Sample Name: CCV2 Acquired; 2/25/2009 12;40:37 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom ID1: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
itfl n
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2837
ppb
1005.
7.
.7176
1004.
1012.
997.9
Chk Pass
Zr3391
ppb
1041.
8.
.7327
1039.
1049.
1034.
Chk Pass
TiS349
ppb
498.7
4.1
.8216
493.S
5029
494.7
Chk Pass
Zr3391-2
ppb
1039.
2.
.2221
1037.
1038.
1042.
Chk Pass
Ti3349-2
ppb
497-7
1.5
. .2946
499.0
498.2
496.1
Chk Pass
Tti 908
ppb
497.8
.1
.0181
497.7
497.9
497.9
Chk Pass
U^2635
ppb
1932.
12.
.6015
1934.
1943.
1920.
Chk Pass
U_S854
ppb
1832.
30.
1.617
1819.
1866.
1312.
Chk Pass
U_4090
ppb
2062-
29.
1.395
2076.
2081.
2029.
Chk Pass
V_2924
ppb
4955.
40.
.8030
4949.
4998.
4919.
Chk Pass
Zn2138
ppb
504.4
22
-4367
507.0
502.8
503.5
Chk Pass
Zn2138-2
ppb
486.8
.8
.1698
487.5
485.9
487.0
Chk Pass
2/25/2009 13:52:14
4
Sampte Name: CCW Acquired: 2/25/2009 12:40:37 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Corr. Factor; 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment;
Int. Std.
Unils
Avg
Slddev
%RSD
#1
#2
#3
Y 2243
Cts/S
23484.
74.
.31356
Y 3600
Cts/S
161940.
655.
.40478
Y 3710
Cts/S
17530.
79.
.45211
2339S. 1C1650. 17509.
23520. 161470. 17613.
23533. 162680. 17463.
Socccccco
Sampte Name: CCB2 Acquired; 2/25/2009 12:48:05 Type: QC
Method: METHOD DVP(v114) Mode; CONC Con. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment: ./
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limil
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Ag3280
ppb
-.2304
.3004
130.4
-.4324
-.3735
.1148
Chk Pass
BeSlSO-2
ppb
-.1185
.0729
61.56
-.1951
-.1106
-.0498
Chk Pass
/Ml 670
ppb
.8913
.1188
13.33
.9358
.9814
.7566
Chk Pass
Bi2230
ppb
-2.236
2.021
90.38
-1.795
-.4724
-4.442
Chk Pass
AIS961
ppb
8.412
3480
41.37
10.68
4.405
10.15
Chk Pass
Ca3179
ppb
17.94
13.62
75.94
4.025
18.55
31.25
Chk Pass
Asl890
ppb
1.299
.425
32.70
1.720
1.306
.8703
Chk Pass
CaS933
ppb
24.66
15.13
61.35
10.87
22.26
40.34
Chk Pass
B_2089
ppb
.5892
.0684
11.61
.6643
.5730
.5304
Chk Pass
Cd2288
ppb
.0589
.0525
89.27
.0296
.1195
.0275
Chk Pass
Ba4554
ppb
.2598
.0811
31.22
.3213
.2902
.1679
Chk Pass
Co2286
ppb
,2568
.2407
93.75
.3945
.3970
-.0212
Chk Pass
Ba4554-2
ppb
.1791
.4970
277.5
.4859
-.3943
.4456
Chk Pass
Cr2677
ppb
-.0468
.2732
584.1
2142
-.3308
-.0238
Chk Pass
Be2348
ppb
.1233
.0394
31.94
.1682
.0949
-1067
Chk Pass
Cu2178
ppb
-.3625
.4273
117.9
-.2402
-.0096
-.8376
Chk Pass
Be2348-2
ppb
-.0265
.7183
2711.
-.4755
.8020
-.4060
Chk Pass
Cu2199
ppb
-7551
.8719
115.5
1.255
1.262
-.2517
Chk Pass
BeSlSO
ppb
.1153
.0060
5.195
.1222
.1113
.1124
Chk Pass
CuS273
ppb
3.161
3.300
104.4
1.381
6.968
1.133
Chk Pass
High Limit
Low Limit
2/25/2009 13:52:14
2
Sample Name: CCB2 Acquired: 2/25/2009 12:48:05 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Umit
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
1.101
4.208
382.3
.1093
5.716
-2.523
Chk Pass
Ni2316
ppb
.0498
.3570
716.7
.3623
.1264
-.3393
Chk Pass
Fe27l4
ppb
-6.251
4.574
73.18
-9-998
-7.602
-1.153
Chk Pass
P_1774
ppb
.6728
.8255
122.7
.2462
1.624
.1479
Chk Pass
K_7664
ppb
49.11
12.00
24.44
36.11
59.77
51.47
Chk Pass
Pb2203
ppb
.3327
.1463
44.12
.2675
-5008
.2298
Chk Pass
Li6707
ppb
F 4.523
1.529
33.80
6.175
3.157
4.237
Chk Fait
2.000
-2.000
Sb2063
ppb
-.1752
1.208
689.6
.8244
-1.518
.1680
Chk Pass
Mg2790
ppb
18.66
14.31
76.69
31.82
20.73
3.427
Chk Pass
Sel960
ppb
.8715
2840
325.8
4.088
-.1866
-1.287
Chk Pass
Mg2852
ppb
12.25
6-91
56.40
5.622
11.71
19.41
Chk Pass
312124
ppb
6.982
.527
7.550
7.179
7.381
6.384
Chk Pass
Mn2576
ppb
1.605
.292
18.17
1.846
1.639
1.281
Chk Pass
Si2124-2
ppb
-.9436
22.58
2393.
-4.002
23.01
-21.84
Chk Pass
Mn2576-2
ppb
.7575
.7750
102.3
-.1026
1.401
.9737
Chk Pass
Sn1899
ppb
.0539
.2185
405.8
.2905
.0113
-.1403
Chk Pass
Mo2020
ppb
.1588
.2206
138.9
.3108
.2598
-.0942
Chk Pass
Sr2165
ppb
F 1.158
29.70
1.152
1.505
.8172
Chk Fail
1.000
-1.000
Na5895
ppb
F 125.2
9.9
7.926
125.9
134.7
114.9
Chk Fail
100.0
-100.0
Sr4215
ppb
-5925
.2236
37.73
.3631
.6047
.8098
Chk Pass
8^398879
2/25/200913:5214
3
Sampte Name: CCB2 Acquired: 2/25/2009 12:43:05 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom ID3:
Comment:
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limil
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Umit
Low Umil
Th2337
ppb
.0897
1.261
1406-
-.9042
-.3345
1.508
Chk Pass
Zr3391
ppb
-1156
• .1754
151.7
.1989
.2338
-.0859
Chk Pass
Ti3349
ppb
.0763
.1067
139.9
.0586
-.0205
.1907
Chk Pass
Zr3391-2
ppb
.5471
1.785
326.2
2.605
-.3809
-.5325
Chk Pass
TiS349-2
ppb
-.2797
1.525
545.1
.3718
.8109
-2.022
Chk Pass
Til 908
ppb
.7739
1.534
198.2
2.096
1.134
-.9077
Chk Pass
U_2635
ppb
1250
7-65
61.20
20.53
11.66
5.303
Chk Pass
U_3854
ppb
-18-95
10.03
52.94
-28.08
-8.210
-20.56
Chk Pass
U_4090
ppb
19.07
15.74
82-55
35.19
18.31
3.725
Chk Pass
V_2924
ppb
-6034
.2533
42.06
.3893
-8837
.5371
Chk Pass
Zn21S8
ppb
-.2651
.0628
23.69
-2145
-.3354
-.2455
Chk Pass
Zn2138-2
ppb
-4172
.7768
1862
-8102
-9190
-.4775
Chk Pass
2/25/200913:5214
4
Sample Name: CCB2 Acquired: 2/25/2009 12:48:05 Type: QC
Method: METHOD DVP{v1l4) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
23407.
22.
.09189
Y 3600
Cts/S
164110.
743.
.45291
Y 3710
Cts/S
17534.
12
.07109
23404. 16492G. 17547,
233S6. 163470. 17522.
23429. 163930. 17531
99698^71
2/25/2009 13:52:14
1
Sample Name: 0812092-02 Acquired: 2/25/2009 12:55:05 Type: Unk
Method; METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment:
Etem
Units
Avg
Stddev
%RSO
#1
#2
#3
Check?
High Limit
Lov^r Limit
Elem
Units
Avg
Stddev
%RSD
#1
U3
Check ?
High Limit
Low Limit
AgS280
ppb
-.5632
.2020
35.86
-.5810
-.7557
-.3529
Chk Pass
BeS130
ppb
-.1136
.0316
27.82
-.0771
-.1308
-.1328
Chk Pass
AM 670
ppb
66.91
1.36
2.033
65.89
68.45
66-38
Chk Pass
Be3130-2
ppb
-.0353
.1776
503.3
-.1345
.1698
-.1412
Chk Pass
AI3961
ppb
88.12
15.20
17.25
70.37
99.59
93.90
Chk Pass
612230
ppb
-1.537
1.131
76.81
-1.878
-2-510
-.2237
Chk Pass
As1890
ppb
2.292
2.451
107.0
3.043
-.4470
4279
Chk Pass
Ca3179
ppb
F 518000-
2300.
.4440
519500.
515300.
519100.
Chk Fail
500000.
-500000.
B„2089
ppb
173.7
.3
.1878
173.7
173.3
174.0
Chk Pass
Ca3933
ppb
"
Chk Pass
Ba4554
ppb
11.43
.11
.9819
11.39
11.35
11.56
Chk Pass
Ba4554-2
ppb
11.53
.26
2-214
11.25
11-74
11.61
Chk Pass
Cd2288^ Co2286
ppb ppb
3.524 49-99
.135 .10
3.830 .2002
3-680
3.451
3.441
Chk Pass
50.08
49.88
50.01
Chk Pass
Be234S
ppb
.3991
.0266
6.659
.4052
.3700
.4221
Chk Pass
Cr2677
ppb
.7204
.2472
34.32
.8001
.9179
.4431
Chk Pass
Be2348-2
ppb
.0440
2882
654.3
.2874
-.2742
.1190
Chk Pass
Cu2178
ppb
2-244
.184
8.207
2.413
2.261
2051
Chk Pass
2/25/200913:5215
2
Sample Name: 0812092-02 Acquired: 2/25/2009 12:55:05 Type: Unk
Method: METHOD DVP{v114) Mode: CONC Corr. Factor: 1.000000
User; admin Custom IDl; Custom ID2: Custom IDS:
Comment:
y Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Cu2199
ppb
5.680
.904
15.92
5.929
4677
6.434
Chk Pass
Mn2576-2
ppb
5483.
12.
2158
5495.
5472.
5482.
Chk Pass
Cu3273
ppb
22.99
6.46
28-10
16.67
22.71
29.58
Chk Pass
Mo2020
ppb
11.29
.14
1211
11.38
11.13
11.35
Chk Pass
Fe2599
ppb
8487.
10.
.1173
8476.
8488.
3496.
Chk Pass
Na5395
ppb
243400.
503.
.2024
248900.
247900.
248200.
Chk Pass
Fe2714
ppb
8551.
96.
1.121
8510.
84S3.
8661.
K_7664
ppb
14550-
58.
.4005
14600.
14530.
14490.
Chk Pass Chk Pass
Ni2316^
ppb
62.26
.52
.8298
62.80
6221
61.77
P_1774
ppb
2.912
.684
23.50
3.246
3.366
2125
Chk Pass Chk Pass
Li6707
ppb
377.8
.8
.2071
377.5
378.7
377.2
Chk Pass
Pb2203
ppb
-5.523
.688
12.46
-6.309
-5.228
-5.031
Chk Pass
Mg2790
ppb
235300.
299.
.1270
235500.
235000.
235400.
Chk Pass
Sb2068
ppb
-.4706
.7919
163.3
.3994
-.6618
-1.149
Chk Pass
Mg2852
ppb
F 223700,
2894.
1.294
226000.
224500.
220500.
Chk Fail
10000.
-10000.
Sel960
ppb
-3.975
1.781
44.80
-5.306
-1.952
-4.668
Chk Pass
Mn2576
ppb
5649.
53.
.9399
5612.
5626.
5710.
Chk Pass
Si2l24
ppb
5631.
18.
.3175
5649.
5631.
5613.
Chk Pass
889999972
Sample Name: 0812092-02 Acquired: 2/25/2009 12:55:05 Type: Unk
Method; METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDl; Custom ID2: Custom ID3:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Etem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Si2124-2
ppb
5210.
24.
.4560
5214.
5134.
5231.
Chk Pass
U_3854
ppb
-2.822
18.63
660.0
-24.15
5.444
10.24
Chk Pass
Sn1899
ppb
1.281
.106
8.278
1.360
1.322
1.160
Chk Pass
U_4090
ppb
5.817
31.20
536.4
-23.03
1.549
38.93
Chk Pass
Sr2165
ppb
11790.
15.
.1285
11800.
11770.
11780.
Chk Pass
V_2924
ppb
19.73
.93
4.715
18.78
19.76
20.64
Chk Pass
Sr4215
ppb
12610.
23-
.1815
12620-
12580.
12620.
Chk Pass
Zn2138
ppb
149.5
.3
.1753
149.8
149.5
149.2
Chk Pass
Th2337
ppb
2.972
4.010
134.9
7.135
2.645
-.8645
Chk Pass
Zn2138-2
ppb
137-2
12
.8588
138.3
136.0
137.3
Chk Pass
Ti3349
ppb
2.793
.010
.3463
2.738
2.787
2.804
Chk Pass
Zr3391
ppb
-.3191
-1964
61.55
-.5123
-.3254
-.1196
Chk Pass
TiS349-2
ppb
8.201
1.956
23.35
7.683
10.36
6.556
Chk Pass
Zr3391-2
ppb
.7578
2.927
386.3
-.9191
-.9451
4.137
Chk Pass
TII 908
ppb
-1.521
1,266
83.23
-1.272
-.3979
-2.393
Chk Pass
U_2635
ppb
41.27
17.94
43.46
59.50
23.64
40.68
Chk Pass
225/2009 13:52:15
4
Sample Name: 0312092-02
Method: METHOD DVP(vll4)
User: admin Custom IDI:
Comment:
Acquired; 2/25/2009 12:55:05 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
20695.
17.
.03283
20713.
20695.
20678.
Y 3600
Cts/S
142640.
1578.
1.1064
143660.
143440.
140820.
Y 3710
Cts/S
17133.
59,
.34574
17119.
17199.
17083.
39^9^73
225/200913:52:15
1
Sampte Name: 0812080-03 i Acquired: 2/25/2009 13:03:10
Method: METHOD DVP(v114) Mode: CONC
User:admin Custom IDI: Custom ID2:
Comment:
Elem
Unils
Avg
Slddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Ag3280
ppb
.8362
.4266
51.02
.5223
.6637
1.322
Chk Pass
BeS130-2
ppb
.3023
.2250
74.43
.2433
.5509
.1126
Chk Pass
AJ1670
ppb
126.1
.9
.7133
127.1
125.6
125.5
Chk Pass
Bi22S0
ppb
.7707
1.372
178.0
1.733
1.380
-.8006
Chk Pass
/y3961
ppb
128.6
8.7
6.787
125.5
121.9
138.5
Chk Pass
CaS179
ppb
33000.
35.
.1066
32970.
32990.
33040.
Chk Pass
Type: Unk
Corr. Factor: 1.000000
Custom IDS:
Asl890
ppb
1.1Q1
-180
16-37
1.304
1.037
.9614
Chk Pass
Ca39S3
ppb
F32040.
103.
.3206
32160.
31970-
31990.
Chk Fail
10000.
-10000.
B_2089
ppb
8-291
.486
5.864
8-B48
8.074
7.951
Chk Pass
Cd2288
ppb
1.497
.052
3.504
1-555
1.482
1.453
Chk Pass
V^ crn>^
Ba4554
ppb
268.4
1.3
.4676
269.8
2682
267.3
Chk Pass
Co2286
ppb
1.293
.281
21.76
1-494
.9712
1.413
Chk Pass
Ba4554-2
ppb
265.4
.2
.0780
265.6
265.4
265.2
Chk Pass
Cr2677
ppb
1.623
.245
15.10
1.824
1.350
1.694
Chk Pass
Be234S
ppb
.2913
.0267
9.172
.3200
.2672
.2868
Chk Pass
Cu2178
ppb
2.328
.905
33.37
3.371
1.852
1.760
Chk Pass
Be2S48-2
ppb
.1763
.2237
126.9
.0652
.0300
.4339
Chk Pass
Cu2199
ppb
3.788
.020
.5199
3.770
3.809
3,784
Chk Pass
BeSlSO
ppb
.3317
.0090
2.705
.3215
.3383
.3354
Chk Pass
Cu3273
ppb
11.91
5.02
42.15
9.768
17.65
8.320
Chk Pass
2/25/2009 13:5215
2
Sample Name: 0812080-03 Acquired: 2/25/2009 13:03:10 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS;
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Fe2599
ppb
15.73
2.47
15.70
14.33
14.28
18.58
Chk Pass
Ni2316
ppb
34-25
.13
.3855
34.40
34.22
34.14
Chk Pass
Fe2714
ppb
11.17
6.81
60.93
18.60
5.239
9.671
Chk Pass
P_1774
ppb
1.540
1.057
68.63
2.663
.5724
1.380
Chk Pass
K_7664
ppb
2263.
60.
2.633
2194.
2300.
2295.
Chk Pass C
Pb2203"^
ppb
-2.506
1.659
66.20
-1.508
-4.422
-1.590
U6707
ppb
13.72
.78
5.704
12.93
14.50
13.72
ihkPass
Sb2068
ppb
-1.217
.437
35.90
-1.716
-.9038
-1.031
Chk Pass Chk Pass
Mg2790
ppb
13230.
50.
.3793
13170.
13270.
13230.
Chk Pass
Sel960
ppb
1.159
2.117
182.7
2.871
-1.208
1.813
Chk Pass
Mg2852
ppb
F 13050.
43.
.3263
13060.
13010.
13090.
Chk Fail
10000.
-10000.
312124
ppb
3035.
9.
.2992
3030.
3030.
3045.
Chk Pass
Mn2576
ppb
261.1
1-9
.7093
263.1
260.8
259.4
Chk Pass
Si2124-2
ppb
2833.
22.
.7653
2321.
2858.
2819.
Chk Pass
Mn2576-2
ppb
258.6
1.8
.6966
257.6
260.7
257.7
Chk Pass
Sn1899
ppb
.4863
.0442
9.096
.5210
.5013
.4365
Chk Pass
Mo2020
ppb
.9392
.1750
18.63
.7463
1.088
.9837
Chk Pass
Sf2165
ppb
94.09
.26
.2712
94.37
94.05
93.86
Chk Pass
Na5395
ppb
179100-
276.
.1539
178800.
179300.
179300.
Chk Pass
Sr4215
ppb
99.12
.29
.2961
99.14
98.82
99.40
Chk Pass
899^K7£l
2/25/200913:52:15
3
Sample Name: 0812030-03 Acquired: 2/25/2009 13:03:10 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom 1D2: Custom IDS:
Comment:
Elem
Unils
Avg
Slddev
%RSD
m
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limil
Low Limit
Th2837
ppb
1.568
.841
53.62
2.294
-6469
1.763
Chk Pass
ZrSS91
ppb
-.0651
.3174
437.9
-.4232
.1593
.0732
Chk Pass
Ti3349
ppb
3.236
.139
4.302
3.078
3.341
3-289
Chk Pass
Zr339l-2
ppb
1367
.572
41.81
.8499
1-980
1-270
Chk Pass
Ti3349-2
ppb
2.018
1.870
92.67
4.064
.3952
1.596
Chk Pass
Til 908
ppb
-.4065
1.341
330.0
-.1399
.7816
-1.861
Chk Pass
U_2635
ppb
-67.62
12.87
19.03
-53.69
-79.06
-70.11
Chk Pass
U_3854
ppb
36.02
14.59
40.50
19.18
44.08
44.79
Chk Pass
U_4090
ppb
13.36
12.53
93.80
7.837
27.71
4.540
Chk Pass
V_2924
ppb
4.279
.095
2.224
4.378
4.270
4.189
Chk Pass
Zn2138
ppb
76.92
21
.2777
76.84
76.76
77.16
Chk Pass
Zn2138-2
ppb
71.98
.17
.2427
71-84
7218
71.92
Chk Pass
2/25/2009 13:52:15
4
Sampte Name: 0812080-03 Acquired; 2/25/2009 13:03:10 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Corr. Faaor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
21695.
27.
.12407
Y_3600
Cts/S
149150.
635-
.42582
Y 3710
Cts/S
16592
32.
,19496
21702. 148450. 16629.
21G65. 149630. 16573.
21718. 149310. 16574.
39^5^75
^
Sample Name: 0812OB0-SRD>'
Method: METHOD DVP{v114)
User: admin Custom IDl:
Comment:
o^^\vA^''
Acquired: 2/25/2009 13:10:56 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Ag3280
ppb
-.0294
.5178
1760.
-.2598
-.3921
.5636
Chk Pass
Be3130-2
ppb
-.0536
.1300
242.4
.0424
-.0017
-.2016
Chk Pass
All 670
ppb
26.68
.23
.8717
26.74
26-42
26.87
Chk Pass
Bi22S0
ppb
-2.005
.923
46.04
-1.924
-2.967
-1.126
Chk Pass
AI3961
ppb
20.35
1226
60.25
11.84
34.40
14.80
Chk Pass
Ca3179
ppb
6616.
40.
.6039
6582.
6660.
6607.
Chk Pass
As 1890
ppb
.8161
-9661
118.4
-.2686
1.584
1.132
Chk Pass
CaS93S
ppb
6614
108.
1.636
6493.
6648-
6701.
Chk Pass
B_2039
ppb
1.B73
.172
9211
1.723
2.061
1.834
Chk Pass
Cd2288
ppb
.3974
-0482
12.13
.4346
.3429
.4148
Chk Pass
Ba4554
ppb
55.73
.14
.2566
55.36
55.77
55.58
Chk Pass
Co2236
ppb
.2518
.1338
55.11
.4027
.2228
.1298
Chk Pass
Ba4554-2
ppb
53.01
.36
.6786
53.01
53-36
52.64
Chk Pass
Cr2677
ppb
.3296
.2472
75.01
.1842
.6151
-1896
Chk Pass
Be2S48
ppb
.0897
.0168
18.68
.0794
.0807
.1091
Chk Pass
Cu2l73
ppb
.8074
1.307
161.8
-.3733
.5842
2.211
Chk Pass
Be2348-2
ppb
-.2322
.1277
55.00
-.1918
-.3753
-.1296
Chk Pass
Cu2199
ppb
.3347
1.830
546.7
-.8459
-.5928
2.443
Chk Pass
B©3130
ppb
.1293
.0089
6.920
.1353
.1336
.1190
Chk Pass
CuS273
ppb
.6101
11.07
1814.
-7.663
-3.689
13.18
Chk Pass
2/25/2009 13:52:15
2
Sample Name: 0812080-SRDl Acquired: 2/25/2009 13:10:56
Method: METHOD DVP(vl 14) Mode: CONC
User: edmtn
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Umit
Custom IDl:
F62599
ppb
4.458
4.234
94.98
3.874
.5460
8.954
Chk Pass
Ni2316
ppb
7.124
.372
5219
7.295
6.697
7.379
Chk Pass
Fe2714
ppb
11.79
4.14
35.12
8.916
9.920
16.54
Chk Pass
P_1774
ppb
.6672
.0562
3-430
.6025
.6944
.7046
Chk Pass
Custom ID2;
K_7664
ppb
416.6
52.5
12.60
466.6
421.1
361.9
Chk Pass
Con. Factor
Type: I
: 1.000000
Custom IDS:
U6707
ppb
2.319
1.343
79.48
.3482
2.609
4.000
Chk Pass
Pb2203 Sb2Q68
ppb ppb
-.8942 -1-583
.5397 1.577
60.36 99.62
-.9290
-.3380
-1.416
Chk Pass
-3.379
-.4217
-.9492
Chk Pass
Mg2790
ppb
2659.
46.
1.736
2620.
2710.
2648.
Chk Pass
Sel960
ppb
-.2907
-9180
315.8
-.4633
.7032
-1.107
Chk Pass
Jnk
Mg2352
ppb
2648.
23.
.3741
2628.
2673.
2642.
Chk Pass
Si2124
ppb
619.1
.4
.0568
6192
619.4
618.7
Chk Pass
Mn2576
ppb
53.00
.24
.4502
53.28
52.87
52.86
Chk Pass
Si2124-2
ppb
583.5
6.4
1.104
576-7
589.5
584.2
Chk Pass
Mn2576-2
ppb
52.20
.15
.2900
52.33
52.03
52-23
Chk Pass
SnlS99
ppb
.3597
.2367
65.81
.4200
.0986
.5603
Chk Pass
Mo2020
ppb
.2092
.1399
66.87
.2883
.2911
.0477
Chk Pass
Sr2165
ppb
20.03
.21
1.026
20.15
20.15
19.79
Chk Pass
Na5895
ppb
36270.
197.
.5425
36190.
36500.
36130.
Chk Pass
Sr4215
ppb
19.52
.36
1.845
19.92
19.43
19.21
Chk Pass
899399979
AA'
Sampte Name: 0812030-SRl3^ Acquired: 2/25/2009 13:10:56 Type: Unk
Method; METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
3
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th2837
ppb
.3678
2.6SS
715.8
-.0850
3.198
-2-010
Chk Pass
ZrSS91
ppb
-.0782
.1190
1522
-.1213
-.1697
.0564
Chk Pass
Ti3349
ppb
.8395
.0676
8.049
.7614
.3738
-8782
Chk Pass
Zr3391-2
ppb
.8378
1.149
137.1
-.2774
.7732
2.018
Chk Pass
Ti3349-2
ppb
.7524
1.259
167.4
2135
.4492
-.3275
Chk Pass
TI1908
ppb
.6458
1.610
249.2
-1.095
2.081
.9512
Chk Pass
U_2635
ppb
1.518
19.02
1253.
-10.99
-7.860
23.40
Chk Pass
U_3854
ppb
-15.14
1.17
7.737
-16.32
-15,12
-13.98
Chk Pass
U_4090
ppb
21.43
9.53
44.47
2240
11.46
30.44
Chk Pass
V_2924
ppb
.7302
.7549
103.4
1.499
-.0099
.7016
Chk Pass
Zn21S8
ppb
15.65
-08
.5092
15,57
15.73
15.65
Chk Pass
Zn21S8-2
ppb
15.04
.26
1.706
15.16
14.75
15.22
Chk Pass
2/25/2009 13:52:15
4
Sampte Name: 0812080-SRDl
Method: METHOD DVP(vl14)
User: admin Custom IDI:
Comment;
Acquired: 2/25/2009 13:10:56 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
Inl. Std.
Units
Avg
Slddev
%RSD
#1
#2
#3
Y 2243
Cts/S
22200.
3.
.01320
Y 3600
Cls/S
156370.
1055.
.67470
Y 3710
Cls/S
17064.
25.
.14928
22201. 156640. 17087.
22197. 155210. 17068.
22202. 157270. 17036.
98^99877
Sample Name: 0812080-DUP1
Method: METHOD DVP(v114)
User: admin Custom IDl:
Comment:
Acquired: 2/25/2009 13:18:40 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Lew Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Ag3280
ppb
.4051
.5508
136,0
-.1791
,9148
.4797
Chk Pass
BeS130-2
ppb
-1770
•2118
119.7
.1424
-4039
-.0154
Chk Pass
All 670
ppb
120.9
1.7
1.432
1202
119.5
1228
Chk Pass
Bi22SQ
ppb
-2-371
.537
22.64
-1.761
-2-770
-2-582
Chk Pass
AI3961
ppb
112.9
14.8
13.07
110.1
99-75
128.9
Chk Pass
Ca3179
ppb
32400,
229.
-7067
32290,
32240,
32660,
Chk Pass
Asl890
ppb
1-759
.945
53.70
2631
1.891
,7554
Chk Pass
Ca3933
ppb
F 31610.
306.
.9675
31960.
31490.
31390.
Chk Fai!
10000,
-10000.
B_2039
ppb
7.713
.163
2.106
7.555
7.330
7.705
Chk Pass
Cd2288
ppb
1,490
.041
2.776
1.535
1,453
1,482
Chk Pass
Ba4554
ppb
260.5
9.6
3.685
265.1
267.1
249.5
Chk Pass
Co22&6
ppb
1.202
.220
18.30
1.031
1.068
1.455
Chk Pass
Ba4554-2
ppb
262.3
2.6
-9803
260.8
260.7
265.2
Chk Pass
Cr2677
ppb
1.523
.387
25.42
1,564
1.888
1.117
Chk Pass
Be2348
ppb
.2067
-0265
12-83
.2058
.2336
.1306
Chk Pass
Cu217a
ppb
3.822
.523
13.69
4.184
3.222
4.059
Chk Pass
Be2348-2
ppb
.0691
.1459
211.1
.2321
-.0496
.0249
Chk Pass
Cu2199
ppb
4-676
1.761
37.66
5.271
6-062
2.694
Chk Pass
BeSlSO
ppb
.3071
.0070
2.268
.3127
.3092
.2993
Chk Pass
Cu3273
ppb
19.15
8.76
45.74
16.22
28.99
12.23
Chk Pass
2/25/200913:52:15
2
Sample Name: 03120aO-DUP1
Method: METHOD DVP{v114)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 13:18:40 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS;
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limil
Fe2599
ppb
13.46
1-53
11-40
14.68
13.97
11.74
Chk Pass
Ni2316
ppb
33.68
.43
1.422
33.17
33.78
34.11
Chk Pass
Fe2714
ppb
8.682
10.35
119.2
2.206
3.222
20.62
Chk Pass
P_1774
ppb
5.040
.378
7.492
4.815
5.476
4.829
Chk Pass
K_7664
ppb
2148.
18.
.8590
2133.
2141
2168.
Chk Pass
i
U6707
ppb
9.745
1.488
15.27
11.43
9211
8.598
Chk Pass
r
V
Pb2203 Sb206a
ppb ppb
-1.564 .0998
1.062 1.980
67.87 1934.
-.3359
-2.446
-1.860
Chk Pass
-1.089
2-336
-.9970
Chk Pass
Mg2790
ppb
12930.
109.
.8434
12920.
12330.
TS040.
Chk Pass
Sel960
ppb
2.793
3.056
109.4
3.714
-.6173
5.282
Chk Pass
Mg2852
ppb
F12860.
100-
.7760
12800.
12810.
12980.
Chk Fail
10000.
-10000.
Si2124
ppb
3003.
34.
1.116
2986.
2981.
3042.
Chk Pass
Mn2576
ppb
249-0
9-0
3.626
2532
255.1
238-6
Chk Pass
Si2124-2
ppb
2808.
13.
.4469
2822.
2799.
2802.
Chk Pass
Mn2576-2
ppb
254-5
3-6
1,410
253.0
251.8
258-5
Chk Pass
Sn1899
ppb
1-564
.111
7.105
1.693
1.496
1.504
Chk Pass
Mo2020
ppb
.8066
.1633
20.24
.6243
.8561
.9394
Chk Pass
Sr2165
ppb
91.30
.93
1.014
91.12
90-47
92.30
Chk Pass
Na5895
ppb
177600.
1638.
.9226
177400.
176000.
179300.
Chk Pass
Sr4215
ppb
96.30
1.16
1.204
95.62
95.63
97.64
Chk Pass
99^SaS79
Sampte Name: 0812080-DUP1
Method: METHOD DVP(v114)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2Q09 13:18:40 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th28S7
ppb
.0573
.3532
616.4
.2336
-.3496
.2380
Chk Pass
2rS391
ppb
-.0036
.1352
3796.
-.1456
.0113
.1235
Chk Pass
TiSS49
ppb
2.978
210
7.053
3.214
2.905
2.814
Chk Pass
Zr3S91-2
ppb
-.5256
1.750
333-0
-2.399
-.2445
1.067
Chk Pass
Ti 3349-2
ppb
1.649
1.693
102.7
2.263
-.2661
2.949
Chk Pass
TII 908
ppb
-.4057
.5482
135.1
-.3352
-.9856
.1039
Chk Pass
U_2635
ppb
-70-73
18-79
26.57
-55.40
-91.70
-65.10
Chk Pass
U_3854
ppb
1401
6.30
43.53
21.62
8-506
11.90
Chk Pass
U_4090
ppb
15-69
9.74
62.08
24.07
5.003
13.00
Chk Pass
V_2924
ppb
4.388
.281
6.393
4.193
4.709
4.261
Chk Pass
Zn2138
ppb
75.88
91
1.201
75.42
75.30
76.94
Chk Pass
Zn2138-2
ppb
71.40
.43
.5981
71.77
70.93
71.49
Chk Pass
2/25/200913:5215
4
Sampte Name: 0812080-DUPl Acquired: 2/25/2009 13:18:40 Type: Unk
Method: METHOD bVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2; Custom ID3:
Comment:
Inl. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
21647.
128.
.59345
Y 3600
Cts/S
154000.
6215.
4.0368
Y 3710
Cts/S
17000.
48.
.28257
21671. 151070. 17022.
21761. 149800. 17033.
21508. 161140. 16945
888^B87S
Sample Name: 0812080-MS1
Method: METHOD DVP(v114)
User: admin Custom IDI:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Eiem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limil
Ag3280
ppb
52-04
-51
.9880
52,29
52.37
51-45
Acquired: 2/25/2009 13:26:25 Type; Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom IDS;
All 670
ppb
2267.
2.
.0785
2265.
2269.
2266.
Chk Pass Chk Pass
BeS 130-2
ppb
51-75
.13
.2542
51.87
51.61
51.77
8(2230
ppb
-3.962
1-497
37.77
-3.358
-5.667
-2.862
Chk Pass Chk Pass
AI3961
ppb
2156.
29.
1.331
2123.
2157.
2185.
Chk Pass
Ca3179
ppb
57840.
148.
.2556
58000-
57780.
57720.
Chk Pass
A51890
ppb
2024.
1.
.0686
2024.
2022-
2025.
Chk Pass
Ca3933
ppb
F 54370.
192
.3523
54290.
54590.
54240.
Chk Fail
10000.
-10000.
B_2089
ppb
1024.
2.
.2172
1022
1026.
1025.
Chk Pass
Cd2288
ppb
51.26
.38
.7392
50.84
51.38
51.56
Chk Pass
Ba4554
ppb
2302.
59.
2.583
2294.
2364-
2246.
Chk Pass
Co2286
ppb
490.4
.3
.1555
489.7
490.3
4912
Chk Pass
Ba4554-2
ppb
2302-
6-
.2471
2308.
2298.
2300.
Chk Pass
Cr2677
ppb
199.7
4.0
2.015
197.0
204.3
197.7
Chk Pass
Be2S48
ppb
51.25
.80
1.553
50.87
5217
50.72
Chk Pass
Cu2178
ppb 255.2
3.1
1.225
2574
256.5
251.6
Chk Pass
Be2348-2
ppb
51.40
.37
.7209
51.82
51.13
51.24
Chk Pass
Cu2199
ppb
246.9
.8
.3182
246.0
247.5
247.3
Chk Pass
BeSlSO
ppb
51.29
.39
1.738
50.84
52.32
50.71
Chk Pass
Cu3273
ppb
252.8
4.6
1.826
258.1
250.2
250.0
Chk Pass
2/25/2009 13:52:15
2
Sampte Name: 0312080-MS1
Method: METHOD DVP(v114)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 13:26:25 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2: Custom ID3:
Elem
Units
Avg
Stddev
%RSD
#1
02
J*S
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Fe2599
ppb
1021.
9.
.8377
1022
1012.
1029.
Chk Pass
Ni2316
ppb
527.5
.8
.1462
526.7
528.3
527.6
Chk Pass
Fe2714
ppb
1002.
13.
1.331
992.6
1017.
995.9
Chk Pass
P_1774
ppb
2.794
.127
4.526
2.940
2.713
2.730
Chk Pass
K_7664
ppb
27660.
146.
.5272
27830.
27580.
27570.
Chk Pass C
Pb2203
ppb
478.3
.2
-0410
478.5
478.5
478.1
U6707
ppb
1064,
1.
.1027
1064.
1062.
1064.
:;hk Pass
Sb2068
ppb
486.8
.3
.0557
486.6
486.7
487.1
Chk Pass Chk Pass
Mg2790
ppb
37880.
105.
.2771
37890.
37980.
37770.
Chk Pass
Sel960
ppb
2019.
6.
.2823
2018.
2025.
2014.
Chk Pass
Mg2852
ppb
F 37610.
103.
.2747
37700.
37640.
37500-
Chk Fail
10000.
-10000.
Si2124
ppb
4128.
7.
.1740
4121.
4135.
4128.
Chk Pass
Mn2576
ppb
768.6
13.4
1.738
759.0
783.9
763.0
Chk Pass
Si2124-2
ppb
3880.
22.
.5708
3861.
3904.
3875.
Chk Pass
Mn2576-2
ppb
761.1
4.5
.5919
765.9
757.0
760.5
Chk Pass
Sn1899
ppb
965.0
2.4
.2537
9622
966.1
966.7
Chk Pass
Mo2020
ppb
1037.
2.
.1973
1035.
1039.
1036.
Chk Pass
Sr2165
ppb
1060.
2.
.1925
1058.
1062
1061-
Chk Pass
Na5895
ppb
206100.
413.
.2005
206500.
206000.
205700.
Chk Pass
Sr4215
ppb
1127.
2.
2147
1129.
1125.
1126.
Chk Pass
39^9^88
ii/Z3;^UU3 ij.:}^. 1^
Sample Name: 0812080-MSl
Method: METHOD DVP(v114)
User: admin Custom IDI:
Comment;
Acquired: 2/25/2009 13:26:25 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom (D2 Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Th28S7
ppb
-.3956
.3898
98.54
-.6944
-.5373
.0454
Chk Pass
Zr339l
ppb
-.3693
.1506
40.30
-.2123
-.3827
-.5127
Chk Pass
TiS349
ppb
1034.
17.
1 614
1023.
1053.
1026.
Chk Pass
Zr3391-2
ppb
1.407
1.914
136.0
-.5926
1.593
3.221
Chk Pass
Ti3349-2
ppb
1023.
3.
.3265
1025.
1019.
1025.
Chk Pass
Til 908
ppb
1907.
5.
-2520
1903.
1912.
1906.
Chk Pass
U_2635
ppb
-585.4
16.7
2-858
-594.7
-595.4
-566.1
Chk Pass
U_3854
ppb
-23-64
21.27
89.94
-34.80
-37.01
.8790
Chk Pass
U_4090
ppb
42.61
11.24
26.38
45.04
52.44
30.36
Chk Pass
V_2924
ppb
513.2
8.6
1.674
508.4
523.2
508.2
Chk Pass
Zn2138
ppb
590.9
1.0
.1612
589.3
591.6
591-2
Chk Pass
Zn2138-2
ppb
554,7
2.0
.3536
552.5
556.2
5554
Chk Pass
2/25/200913:52:15
4
Sampte Name: 0312080-MS1
Method; METHOD DVP{v114)
User: admin Custom IDl:
Comment:
Acquired: 2/25/2009 13:26:25 Type: Unk
Mode: CONC Corr. Factor: 1.000000
Custom ID2; Custom IDS:
Int. Std.
Unils
Avg
Slddev
%RSD
#1
#2
#3
Y 2243
CtaS
21392.
48.
.22652
21412.
21357.
21427.
Y 3600
Cts/S
149330-
1313.
1.2138
150270.
147240.
150480.
Y 3710
Cts/S
17196.
38.
21854
17188.
17164.
17237.
88^3^91
Sampte Name; 0812080-^01 Acquired: 2/25/2009 13:34:05 Type: Unk
Method: METHOD DVP(v114) Mode; CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Ag32S0
ppb
-.0434
.3636
837.1
.3679
-.3221
-.1762
Chk Pass
Be31S0.2
ppb
.1370
.0633
46.20
.0749
.2014
.1348
Chk Pass
Ail 670
ppb
152.7
.1
.0538
152.7
152.7
152.6
Chk Pass
Bi2230
ppb
.1539
.8190
5322
.9350
.2252
-.6985
Chk Pass
AI3961
ppb
149.6
16-3
10.36
142.4
1382
1682
Chk Pass
CaS179
ppb
29980.
31.
.1019
30010.
29960.
29960.
Chk Pass
As1890
ppb
2.645
.992
37.49
1.522
3.011
3.401
Chk Pass
CaS933
ppb
F 29520.
53.
.1795
29570.
29510.
29470.
Chk Fail
10000.
-10000.
B_2089
ppb
10.40
.54
5-175
9.820
10.88
10.51
Chk Pass
Cd2288
ppb
.9997
-0299
2.990
.9770
.9886
1.034
Chk Pass
Ba4554
ppb
303.5
1.9
.6155
301.3
304.6
304.5
Chk Pass
Co2286
ppb
41.92
.25
.5926
41.64
42.01
4211
Chk Pass
Ba4554-2
ppb
302.5
.2
.0734
302.5
3022
302.6
Chk Pass
Cr2677
ppb
-8460
2214
26.17
1.062
.8562
.6197
Chk Pass
Be2348
ppb
.1426
.0239
16.77
.1478
-1165
-1635
Chk Pass
Cu2178
ppb
.9259
.7343
79.30
.6387
.3787
1.760
Chk Pass
Be2348-2
ppb
.0142
.4167
2938.
-.3962
.4369
.0018
Chk Pass
Cu2199
ppb
3.178
1.099
34.57
1.984
4.147
3.403
Chk Pass
BeSlSO
ppb
JJ327
.0133
5.705
2189
.2454
.2339
Chk Pass
Cu3273
ppb
7.265
4.801
66.08
3-171
1255
6.075
Chk Pass
2/25/200913:52:16
2
Sampte Name: 0812080-001 Acquired: 2/25/2009 13:34:05 Type: Unk
Method: METHOD DVP(vll4) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limit
Etem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limil
Fe2599
ppb
841.1
2.6
-3060
343.0
8421
838.2
Chk Pass
Ni2316
ppb
35.69
.38
1.057
35.69
36.07
35.31
Chk Pass
Fe2714
ppb
B41.7
12.4
t-4 70
323.8
853.5
842.9
Chk Pass
P_1774
ppb
6.107
1.461
23.93
5.004
7.765
5.553
Chk Pass
K_7664
ppb
1705.
74.
4.S41
1623.
1767.
1725.
Chk Pass
Li6707
ppb
10.34
.69
6.625
9.612
10.97
10.44
Chk Pass
V
Pb2203 Sb2068
ppb ppb
-.9768 -.5899
.5289 1.157
54.14 196.1
-.4617
-1.519
-.9503
Chk Pass
.3539
-1.881
-.2431
Chk Pass
Mg2790
ppb
12940.
22.
.1728
12930.
12960.
12920.
Chk Pass
Sel960
ppb
1.619
.465
28.74
1.895
1.032
1.331
Chk Pass
Mg2852
ppb
F 12890.
34.
.2637
12910
12350.
12890.
Chk Fail
10000.
-10000.
Si2124
ppb
2986-
5.
.1744
2988.
2989.
2980.
Chk Pass
Mn2576
ppb
1771.
10.
.5753
1759.
1779.
1775.
Chk Pass
Si2124-2
ppb
2759.
14.
.4967
2774.
2753.
2749.
Chk Pass
Mn2576-2
ppb
1737.
9.
.5208
1731.
1748.
1733.
Chk Pass
Sn1899
ppb
1.084
.336
31.03
.7320
1.117
1.402
Chk Pass
MO2020
ppb
.8871
.0732
8.249
.8183
.8790
.9640
Chk Pass
Sr2165
ppb
122.9
.1
.0930
123.0
1228
123.0
Chk Pass
Na5895
ppb
308400.
1100.
.3567
308300.
309500.
307300.
Chk Pass
Sr4215
ppb
130.5
-8
.6509
130.6
131.3
129.6
Chk Pass
RP?^99998g
Cll.U'V '^\^\^\ 3
Sampte Name; 0812080-^01 Acquired: 2/25/2009 13:34:05 Type: Unk
Meihod: METHOD DVP(v114) IWode: CONC Com Faaor: 1.000(X}0
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th2837
ppb
.0365
2-241
6136-
2.490
-.4776
-1.902
Chk Pass
Zr3391
ppb
.2976
.3321
111.6
-.0582
.5995
.3515
Chk Pass
Ti3349
ppb
3.250
.043
1-313
3.220
3.299
3.231
Chk Pass
Zr3391-2
ppb
1.106
3.127
282.7
4.450
.6131
-1.745
Chk Pass
Ti3349-2
ppb
2.632
1.011
38-41
3.135
1.468
3.292
Chk Pass
Til 908
ppb
.1960
.5556
283.5
.3555
-.4220
.6544
Chk Pass
U_2635
ppb
-32.81
19.90
60.67
^5.71
-42.83
-9.887
Chk Pass
U_3854
ppb
-15.95
10.67
66.37
-3.982
-24.46
-19.43
Chk Pass
U_4090
ppb
6.904
15.14
2192
7.045
-8.302
21.97
Chk Pass
V„2924
ppb
4.657
1.022
21.94
3.872
5.812
4.287
Chk Pass
Zn2138
ppb
42.63
.07
.1655
42.55
42.65
42.68
Chk Pass
Zn2138-2
ppb
39.64
.39
.9935
39.72
39.22
39.99
Chk Pass
2/25/200913:52:16
4
Sampte Name: 0812030-001 Acquired: 2/25/2009 13:34:05 Type: Unk
Method: METHOD DVP(v114) Mode; CONC Con. Factor; 1.000000
User: admin . Custom IDl: Custom ID2: Custom ID3:
Comment:
Int. Sid-
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cls/S
21552.
30.
.13700
21585.
21544.
21528.
Y 3600
Cts/S
148960.
786.
.52795
149210.
143070.
149580.
Y 3710
Cls/S
17439.
81.
.46207
17431.
17363.
17523.
88^9993
Sampte Name: 0812080-02
Method: METHOD DVP(v114)
User: admin Custom IDI:
Comment:
Aoquired: 225/2009 13:41:43 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom IDS:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Umit
Etem
Units
Avg
Stddev
%RSO
#1
#2
#S
Check?
High Limit
Low Limit
Ag3280
ppb
-.5473
.4022
73.50
-.1764
-.9743
-.4906
Chk Pass
Be3130-2
ppb
-.0192
.0908
472.4
.0240
-.1235
.0419
Chk Pass
An670
ppb
59-52
.42
.7045
59.97
59-43
59.15
Chk Pass
812230
ppb
-1.559
1.794
115.0
.3389
-1-790
-3.227
Chk Pass
A(S961
ppb
50. fe
2.05
4.084
5245
49.52
48.51
Chk Pass
Ca3179
ppb
21670.
31.
.1446
21700.
21670.
21640.
Chk Pass
AS1890
ppb
2.126
.369
17.36
1.783
2.517
2.079
Chk PasF.
Ca3933
ppb
F 21810.
189.
.8667
22010.
21640.
21790.
Chk Fail
10000.
-10000.
B_2089
ppb
18.13
.32
1.782
18.01
17.89
18.50
Chk Pass
Cd2233
ppb
.4608
.0402
8.715
.4462
.4300
.5062
Chk Pass
Ba4554
ppb
85.49
.70
.8172
36.27
85.27
84.92
Chk Pass
Co2286
ppb
19.71
.07
.3433
19.72
19.77
19.64
Chk Pass
Ba4554-2
ppb
83.63
.19
.2290
83.86
83.53
83.52
Chk Pass
Cr2677
ppb
2.151
.165
7.678
2.328
2.000
2126
Chk Pass
Be2348
ppb
-1881
.0494
26-25
.1711
.2437
.1495
Chk Pass
Cu2l78
ppb
-5277
-4963
94.04
.4458
.0775
1.060
Chk Pass
Be2348-2
ppb
-.3668
.1057
28.83
-.3156
-4884
-.2964
Chk Pass
Cu2199
ppb
1.917
1.396
72.81
2.323
3.065
.3632
Chk Pass
BeSlSO
ppb
.1718
.0281
16.36
.1394
.1863
.1898
Chk Pass
Cu3273
ppb
8.182
2.100
25.67
7.112
10.60
6.8S2
Chk Pass
2/25/2009 13:5216
2
Sambte Name; 0812080-02 Acquired: 2/25/2009 13:41:48 Type: Unk
Method; METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User; admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Umit
Fe2599
ppb
122.5
22
1.800
121.7
125.0
120.8
Chk Pass
Ni2316
ppb
23.13
.53
2.311
23.53
22.53
23.34
Chk Pass
Fe2714
ppb
124.6
.9
.6905
125.3
124.8
123.6
Chk Pass
P_1774
ppb
6.6G4
.466
6,972
7-160
6,228
6,664
Chk Pass
K_7664
ppb
1592-
34.
2.159
1570.
1631.
1574-
Chk Pass
Pb220S^
ppb
-.5790
1.893
327.8
.9606
-2.700
.0021
Chk Pass
U6707
ppb
16.72
.50
3.012
16.92
16.14
17.08
Chk Pass
Sb2a68
ppb
-.5782
1.068
1S4.3
.3186
-1.760
-.2928
Chk Pass
Mg2790
ppb
12050.
49.
-4031
12100.
12020.
12020.
Chk Pass
Sel960
ppb
-2.523
.83?
33,15
-1.997
-3.483
-2.085
Chk Pass
Mg2852
ppb
F12040.
26.
2143
12040-
12060.
12010.
Chk Fail
10000.
-10000.
Si2124
ppb
3036.
5.
.1690
3041.
3031.
3038.
Chk Pass
Mn2576
ppb
3243.
22.
.6766
3268-
3237.
3226.
Chk Pass
Si2124-2
ppb
2791-
50.
1.777
2740.
2793.
2839.
Chk Pass
Mn2576-2
ppb
3187.
6.
.1768
3193.
3182.
3186.
Chk Pass
Sn1899
ppb
1.398
.152
10.89
1.231
1.436
1.528
Chk Pass
Mo2020
ppb
1.249
.115
9.190
1217
1.376
1.153
Chk Pass
Sr2165
ppb
76.72
.20
.2595
76.50
76.76
76.89
Chk Pass
Na5895
ppb
191700.
696.
.3631
192200.
191900.
190900.
Chk Pass
Sr4215
ppb
81.22
.16
.2014
81.15
81.40
81.09
Chk Pass
BaSBR^^^fQ^
Sample Name: 0812080-02 Acquired: 2/25/2009 13:41:48 Type: Unk
Method. METHOD DVP(vl 14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDt; Custom ID2: Custom IDS:
Comment;
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umil
Low Limit
Th2837
ppb
-3879
.9911
255.5
,9230
.9965
-.7558
Chk Pass
Zr3391
ppb
.0349
.0431
123.4
-.0144
.0541
.0652
Chk Pass
TiSS49
ppb
2.566
.063
2.470
2.590
2.615
2.495
Chk Pass
Zr3391-2
ppb
.1258
2.306
1833.
2.555
-.1461
-2.032
Chk Pass
Ti3349-2
ppb
1.200
.915
76.27
.2672
2.097
1.237
Chk Pass
Til 908
ppb
.4946
1.015
205.2
1.229
-.6638
.9184
Chk Pass
U_2635
ppb
50.93
1216
23.87
38.60
62.91
51.27
Chk Pass
U_3854
ppb
-.4158
11.35
2730.
12.24
-3.769
-9.714
Chk Pass
U_4090
ppb
16.49
7.76
47.06
21.31
20.09
7.587
Chk Pass
V_2924
ppb
4.131
.934
22.61
4.435
3.071
4.836
Chk Pass
2n2138
ppb
23.19
.04
.1663
23.23
23.18
23.15
Chk Pass
Zn21S8-2
ppb
21.59
.12
.5727
21.70
21.46
21.63
Chk Pass
2/25/200913:52:16
4
Sample Name: 0812080-02 Acquired: 2/25/2009 13:41:48 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom 1D3:
Comment:
Int. Std.
Units
Avg
Slddev
%RSD
#1
#2
#3
Y_2243
Cls/S
21880.
2.
.00949
Y_3600
Cts/S
153320.
1211.
.73999
Y_S710
Cts/S
17763.
29.
.16424
21880. 151960. 17775.
2188.3. 153720. 17736.
21879. 154290. 17793.
S9ffi6tSS5
Sample Name: 0812080-04 Acquired: 2/25/2009 13:49:33 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User; admin Custom IDI: Custom ID2; Custom IDS:
Comment
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limil
Ag3280
ppb
1.021
-166
16.27
.8446
1.044
1.174
/yi670
ppb
122.1
1.5
1.202
1212
1212
123.8
Chk Pass Chk Pass
BeS 130-2
ppb
.1681
.1974
117.4
.3907
.0996
.0141
Bi2230
ppb
-1.531
.946
61.80
-1219
-2.594
-.7802
Chk Pass Chk Pass
AI3961
ppb
120.0
9-3
7.786
111.1
129.7
119.3
Chk Pass
CaS179
ppb
31840
48.
.1520
S1390.
31790.
31830.
Chk Pass
Asl890
ppb
1.718
.792
46.10
.8040
2.203
2.147
Chk Pass
Ca3933
ppb
F 31080.
227.
.7316
31320.
30870.
31040.
Chk Fail
10000.
-10000.
B_2089
ppb
7.742
.239
3.086
8.017
7.587
7.621
Chk Pass
Cd2288
ppb
1.516
.041
2.694
1.477
1.512
1.558
Chk Pass
Ba4554
ppb
. 270-6
2.4
.8957
273.1
270.5
268.3
Chk Pass
Co2286
ppb
1.663
.104
6.263
1.732
1.543
1.71S
Chk Pass
Ba4554-2
ppb
260.4
.9
.3294
261.4
260.1
259.8
Chk Pass
Cr2677
ppb
1.438
.071
4.967
1.403
1.520
1.387
Chk Pass
Be2348
ppb
.2157
.0341
15.81
.2524
.2099
.1849
Chk Pass
Cu2178
ppb
2.749
.217
7.900
2.864
2.885
2.499
Chk Pass
Be2348-2
ppb
.1566
.3250
207.5
.0880
.5105
-.1286
Chk Pass
Cu2199
ppb
3.008
.187
6.204
2.957
3215
2.853
Chk Pass
BeSlSO
ppb
.3461
-0337
9.735
.3709
.3078
.3596
Chk Pass
CU3273
ppb
8.493
5.244
61.75
2.580
10.32
12.58
Chk Pass
2/25/2009 14:38:21
2
Sampie Name: 0812080-W ^ Acquired; 2/25/2009 13:49:33
Method: METHOD DVP(vl14) Mode: CONC
User: admin
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limil
CiJ,stnmlDl:
Fe2599
ppb
18.17
2.40
13.22
15.93
20.71
17.88
Chk Pass
Ni2316
ppb
34.36
.26
.7531
34.65
34.17
34.26
Chk Pass
Fe2714
ppb
21.26
7.77
36.57
30.17
15.87
17.73
Chk Pass
P_1774
ppb
1.959
.562
28.71
1.395
1.962
2.520
Chk Pass
Custom ID2:
K_7664
ppb
2087.
51.
2.462
2064.
2052.
2146.
Chk Pass
Type: Unk
Con. Factor: 1.000000
Custom 1D3:
U6707
ppb
9.308
.633
6.798
8.760
IOOO
9.163
Chk Pass
Pb2203^ Sb2068
ppb ppb
-1.273 .2217
.567 .5760
44.59 259.8
-.6965
-1.831
-1.290
Chk Pass
-.2978
.1217
.8411
Chk Pass
Mg2790
ppb
12690.
23.
.1776
12710.
12690.
12670.
Chk Pass
Sel960
ppb
-0073
2-745
37820.
-.3141
-2.562
2.898
Chk Pass
Mg2852
ppb
F12740.
14.
.1104
12750.
12720.
12740.
Chk Fail
10000.
-10000.
Si2124
ppb
3036.
10.
.3172
3030.
3031.
3047.
Chk Pass
Mn2576
ppb
255.8
2.2
.8599
258.1
255-4
253.8
Chk Pass
Si2124-2
ppb
2760.
17.
.6221
2774.
2741.
2764.
Chk Pass
Mn2576-2
ppb
250.6
1.6
.6301
252.4
250.2
249.3
Chk Pass
Sn1899
ppb
.5899
.3285
55.69
.3527
.9648
.4521
Chk Pass
Mo2020
ppb
.9377
.1385
14.77
1.047
.9839
.7820
Chk Pass
Sr2165
ppb
90.61
.24
.2623
90.44
90.51
90.88
Chk Pass
Na5895
ppb
175300.
757.
.4373
176100.
175100.
174600.
Chk Pass
Sr4215
ppb
94.17
.39
.4136
94.53
94.23
93.76
Chk Pass
9^^9889
<JA.^'^UU^
Sampte Name: 0812080-04
Method; METHOD DVP(v114)
User; admin Custom IDI:
Comment:
Acquired: 2/25/2009 13:49:33 Type: Unk
Mode: CONC Con. Factor: 1 OOOOOO
Custom ID2: Custom IDS:
Etem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
»2
#3
Check?
High Umil
Low Umit
Th2837
ppb
-.5971
3.655
612.1
-.6242
3.072
-4.239
Chk Pass
ZrS391
ppb
-0904
.3310
3662
.0495
-.2182
.4399
Cfik Pass
Ti3349
ppb
3.001
.245
8.161
3.266
2.955
2783
Chk Pass
Zf3391-2
ppb
.2032
1.460
718.6
-.8141
-.4525
1.876
Chk Pass
TiSS49-2
ppb
1.178
1.857
157.6
1.809
2.638
-.9123
Chk Pass
Til 908
ppb
2594
.4715
181 7
.6439
-.2666
.4009
Chk Pass
U_2635
ppb
-40.41
8.23
20.48
-30.90
-45.96
^4.36
Chk Pass
U_3854
ppb
3.257
11.43
351.0
2.645
-7.856
14.98
Chk Pass
U_4090
ppb
20 57
12.65
61.49
6.518
24.13
31.05
Chk Pass
V_2924
ppb
3.842
235
8.124
3.739
4.111
3-675
Chk Pass
Zn21Sa
ppb
78.36
.20
.2555
7821
78.28
78.59
Chk Pass
2n21S8-2
ppb
71.20
.24
.3316
71.44
70.97
71.20
Chk Pass
2/25/2009 14:38:21
4
Sample Name: 0812080-04 Acquired: 2/25/2009 13:49:33 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Corr. Faclor: 1.000000
User:admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std.
Unils
Avg
Slddev
%RSD
#1
#2
#3
Y_224S
CtaS
21744.
4.
.01653
21746.
21747.
21740.
Y 3600
Cts/S
152000-
1532
1.0406
150680.
151570.
153760.
Y 3710
Cls/S
17904.
50-
.27826
17868.
17883.
17961.
888889887
Sample Name : L902152-BS1 Acquired: 2/25/2009 13:57:18
Method: METHOD DVP(v114) Mode: CONC
User; admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limit
Elem
Uriits
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Umit
Custom IDt: (
AgS230
ppb
510.7
1.0
.1934
511.4
5112
509.6
Chk Pass
Be31S0-2
ppb
255.6
.4
.1515
256.0
2554
255.3
Chk Pass
All 670
ppb
5189.
26.
.4964
5180.
5218.
5168.
Chk Pass
Bi2230
ppb
-12.51
.69
5-545
-12.73
-11.73
-13.06
Chk Pass
Custom (D2:
AIS961
ppb
5081.
15.
.3000
5064.
5092.
5088.
Chk Pass
Ca3179
ppb
24580.
13.
.0521
24590.
24600.
24570.
Chk Pass
Type: Unk
Con. Factor; 1.000000
Custom IDS:
As1890
ppb
9845.
41.
.4166
9821.
9892.
9821.
Chk Pass
Ca3933
ppb
F 24580.
380.
1.545
24170.
24670.
24910.
Chk Fail
10000.
-10000.
y
B^2039
ppb
5046.
20.
.3907
5027.
5067.
5043.
Chk Pass
Cd2288
ppb
2450
.5
.2075
244.5
245.5
245.1
Chk Pass
Ba4554
ppb
5063.
15.
.3057
5056.
5081.
5053.
Chk Pass
Co2286
ppb
2469.
9.
.3506
2462.
2479.
2465.
Chk Pass
Ba4554-2
ppb
5134.
10.
.1950
5128.
5146.
5130.
Chk Pass
Cr2677
ppb
487.0
2.9
.5891
4901
486.3
484.5
Chk Pass
Be2S48
ppb
249.6
.6
.2585
249.8
250.1
248.9
Chk Pass
Cu2178
ppb
1267.
8.
.6046
1262
1276.
1264.
Chk Pass
Be2343-2
ppb
254.8
1.0
.3799
254.1
255.9
254.4
Chk Pass
Cu2199
ppb
1206.
4.
.3593
1202
1211.
1205.
Chk Pass
BeSlSO
ppb
250.7
.6
.2354
251.3
250.7
250.2
Chk Pass
Cu327S
ppb
1217.
6.
.4876
1223.
1218.
1211.
Chk Pass
2/25/2009 14:42:06
2
Sample Name: L902152-BS1
Method: METHOD DVP(v114)
User: admin Custom IDI:
Comment;
Acquired: 2/25/2009 13:57:18 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom 1D2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limil
Elem
Units
Avg
Stddev
%RSD
*1
#2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
4946.
5.
.1110
4948.
4950.
4940.
Chk Pass
Ni2316
ppb
1994.
8.
.3815
1988.
2003.
1992.
Chk Pass
Fe2714
ppb
4837.
14.
.2874
4853.
4826.
4833.
Chk Pass
P_1774
ppb
1.040
.995
95.72
1.876
-.0609
1.304
Chk Pass
K_7664
ppb
24920.
98.
.3921
24970.
24930.
24800.
Chk Pass
Pb2203
ppb
2402.
12.
.4983
2393.
2416.
2396.
Chk Pass
Li6707
ppb
5281.
14.
.2556
5276.
5296.
5270.
Chk Pass
Sb2068
ppb
2982.
11.
.3641
2971.
2992.
2984.
Chk Pass
Mg2790
ppb
24650.
87.
.3532
24610.
24750.
24580.
Chk Pass
Sel960
ppb
9941.
46.
.4644
9898.
9990.
9935.
Chk Pass
Mg2852
ppb
F24510.
61.
.2478
24500.
24570.
24450.
Chk Fail
10000.
-10000
Si2124
ppb
4893.
25.
.5198
4868.
4919.
4890.
Chk Pass
Mn2576
ppb
760.3
2.1
.2761
760.7
762.2
758.0
Chk Pass
Si2124-2
ppb
4595.
25.
.5502
4607.
4566.
4612.
Chk Pass
Mn2576-2
ppb
757.9
12
.1548
757.1
759.2
757.3
Chk Pass
Sn1899
ppb
4822.
18.
.3672
4810.
4843.
4814.
Chk Pass
Mo2020
ppb
5153.
24.
.4688
5132.
5179.
5149.
Chk Pass
Sr2165
ppb
4864.
19.
.3979
4851.
4886.
4855.
Chk Pass
Na5895
ppb
25930-
24.
.0943
25900.
25940.
25940.
Chk Pass
Sr4215
ppb
5151.
9.
.1776
5141.
5159.
5152.
Chk Pass
nqtmnncnff
Sample Name; L902152-BS1 Acquired: 2/25/2009 13:57:18 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS;
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th2837
ppb
-3.295
.662
20.10
-3.754
-3.594
-2.536
Chk Pass
Zr339l
ppb
-1.240
.135
10.87
-1.294
-1.087
-1.340
Chk Pass
Ti3349
ppb
5208.
7.
.1428
5207.
5216.
5201.
Chk Pass
Zr3391-2
ppb
.7891
1.013
128.4
1.913
-.0536
.5075
Chk Pass
Ti3349-2
ppb
5161.
3.
.0603
5160.
5165.
5159.
Chk Pass
TII 908
ppb
9911
49.
-4965
9876.
9967.
9889.
Chk Pass
U_2635
ppb
-1388.
15.
1.073
-1396.
-1397.
-1371.
Chk Pass
U_3854
ppb
-59.62
13.06
21.91
-45.79
-71.76
-61.30
Chk Pass
U 4090
ppb
137.2
3.7
2.704
139-8
138.9
133.0
Chk Pass
V_2924
ppb
2476.
5.
.2059
2476.
2481.
2470.
Chk Pass
Zn2138
ppb
1018.
4.
.3618
1015.
1022.
1016.
Chk Pass
Zn21S8-2
ppb
948.9
4.9
.5157
951.7
943.3
951.8
Chk Pass
2/25/2009 14:42:06
4
Sample Name: L902152-BS1 Acquired: 2/25/2009 13:57:18 Type: Unk
Meihod: METHOD DVP(vl 14) Mode: CONC Corr. Facton 1.000000
User: admin Custom iDl; Custom ID2: Custom ID3:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
Cts/S
22496.
47.
21027
Y 3600
Cts/S
159510.
571.
.35309
Y 3710
Cts/S
18206.
79.
.43367
#1
#2
#3
22525. 158880. 18129.
22442. 159660. 13287.
22523. 159990. 18203
99^98989
Sampte Name: 0902040-Psi
Meihod: METHOD DVP(v114)
»'^'^^^\^'\
Acquired: 2/25/2009 14:04:56 Type; Unk
Mode: CONC Corr. Factor: 1.000000 Pr^' ^OOO ^?^
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Custom IDl:
Ag3280
ppb
99.38
3.35
3.369
101.9
100.7
95.58
Chk Pass
Be3l30-2
ppb
105.4
.4
.3754
105.7
105.4
104.9
Chk Pass
All 670
ppb
4843.
13.
.2608
4834.
4857.
4837-
Chk Pass
Bi2230
ppb
99.64
212
2.126
98.55
102.1
98.30
Chk Pass
Custom ID2:
•\
"^
AIS96r
ppb
4847.
32.
.6600
4869.
4362.
4811.
Chk Pass
Ca3179
ppb
58160.
53.
.0919
58210.
58150.
58100
Chk Pass
Custom IDS; ^
Asl890
ppb
109.5
1.5
1.402
110.9
109.8
107.8
Chk Pass
Ca39S3
ppb
F 55170.
372.
.6741
54740.
55320.
55440.
Chk Fail
10000.
-10000.
B^2089
ppb
151-7
.4
.2630
151.5
1522
151.4
Chk Pass
Cd22e8
ppb
103.0
.3
.2788
1027
1032
103.1
Chk Pass
Ba4554
ppb
213.2
7.4
3.460
219.4
215.1
205.0
Chk Pass
Co2286
ppb
101.8
.2
.2100
101.7
102.0
101.6
Chk Pass
Ba4554-2
ppb
215.6
.4
.1900
216.1
215.4
215.4
Chk Pass
Cr2677
ppb
103-9
3-4
3.305
106.8
104.7
100.1
Chk Pass
Be2348
ppb
99.95
3.65
3.650
103.Q
100.9
95.93
Chk Pass
Cu2178
ppb
116-1
.9
.7606
115-4
116.0
117.1
Chk Pass
Be2S48-2
ppb
103.1
1.0
.9567
1042
102.8
1023
Chk Pass
Cu2199
ppb
113.1
.7
.6084
113.4
112.3
113.6
Chk Pass
Be3130
ppb
101.4
3.6
3.560
1045
1023
97.44
Chk Pass
Cu3273
ppb
116.5
3.4
2.899
114.3
1204
114.8
Chk Pass
2/25/2009 14:38:30
2
Sample Name; 0902040-PSS
Meihod: METHOD DVP(v114)
User: admin Custom IDI:
Comment:
Acquired: 2/25/2009 14:04:56 Type: Unk
Mode: CONC Corr. Factor; 1.000000
Custom ID2: Custom IDS:
Elem
Units
Avg
Stddev
%RSD
#1
#2
rfS
Check ?
High Limit
Low Limit
Elem
Units
Avg
Slddev
%RSD
#1
#3
Check?
High Limil
Low Limit
Fe2599
ppb
4892.
21.
,4341
4915.
4890.
4873.
Chk Pass
Ni2316
ppb
109.3
.5
.4789
108.9
109.9
1092
Chk Pass
Fe2714
ppb
4640.
174
3.744
4774.
4704.
4444.
Chk Pass
P_1774
ppb
272.5
1.3
.4845
271.1
273.8
272.5
Chk Pass
K_7664
ppb
5590.
120
2.141
5542.
5502.
5726.
Chk Pass
Pb2203
ppb
102.0
.1
.0611
101.9
102.0
102.0
Chk Pass
Li6707
ppb
1666.
3.
.1535
1663.
1667.
1667.
Chk Pass
Sb2068
ppb
106.4
.5
-4343
106.5
105.9
106.7
Chk Pass
Mg2790
ppb
18170.
102.
.5639
18200.
13250.
18050.
Chk Pass
Sel960
ppb
107.8
-1
.0900
107.7
107-9
107.9
Chk Pass
Mg2852
ppb
F 18100.
70
.3890
18180.
13060.
18060.
Chk Fail
10000.
-10000.
Si2l24
ppb
8733.
34.
.3904
8696.
3763.
8741.
Chk Pass
Mn2576
ppb
173.5
6.0
3.482
178.6
175.2
166.8
Chk Pass
Si2124-2
ppb
7951.
42.
.5332
7968.
7983.
7903.
Chk Pass
Mn2576-2
ppb
179.4
1.3
.7415
180.5
179.8
177.9
Chk Pass
Sn1899
ppb
98.54
.50
.5109
98.40
99.10
98.12
Chk Pass
Mo2020
ppb
110.2
.0
.0325
110.3
110.3
1102
Chk Pass
Sr2165
ppb
543-0
1.7
.3121
541.0
544.1
543.8
Chk Pass
Na5895
ppb
187700.
558.
.2973
133200.
187800.
187100.
Chk Pass
Sr4215
ppb
577.2
1.8
.3148
579.2
576.9
575.6
ChK Pass
6989^959
Sample Name: 0902040-PSi
Method: METHOD DVP(vl14)
User: admin Custom IDI;
Comment:
Acquired: 2/25/2009 14:04:56 Type: Unk
Mode: CONC Con. Factor; 1.000000
Custom ID2: Custom IDS:
Elem
Unils
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Umit
Low Limit
Th2837
ppb
-1.701
.979
57.58
-.8317
-2.761
-1.503
Chk Pass
Zr3391
ppb
2.700
.432
15.99
2.915
2.933
2.203
Chk Pass
TiSS49
ppb
175.7
6.6
3.757
181.3
177.2
168.4
Chk Pass
Zr3391-2
ppb
2.672
1.251
46.83
1.229
3.462
3.325
Chk Pass
Ti3349-2
ppb
182.0
2.7
1.510
178.3
183.4
183.8
Chk Pass
TII 908
ppb
98.94
-46
.4627
99.05
99.33
98.43
Chk Pass
U_26S5
ppb
-21.68
13.12
60.49
-15.40
-36.76
-12.89
Chk Pass
U_3854
ppb
-15.18
19.05
125.5
-.8784
-36.81
-7.358
Chk Pass
U_4090
ppb
47.20
16.93
35.96
35.34
39.62
66.65
Chk Pass
V_2924
ppb
13.45
1.00
7.405
13.91
14.13
12.30
Chk Pass
Zn2138
ppb
205.1
.7
.3230
204.5
205.8
2052
Chk Pass
Zn2138-2
ppb
188.6
.9
.4526
138.5
189.6
187.9
Chk Pass
2/25/2009 14:33:30
4
Sample Name: 0902040-PS3
Method: METHOD DVP(v114)
User: admin Custom IDl:
Comment:
/Quired: 2/25/2009 14:04:56 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2: Custom IDS:
Int. Std.
Units
Avg
Stddev
%RSD
#1
n2
#3
Y 2243
Qs/S
22022.
33.
.15124
Y 3600
Cta/S
160470.
5287.
3.2945
Y 3710
as/s
18475.
79.
.42664
22043. 156560. 18484.
21984. 158370. 18392.
22040. 166490. 18549.
898959951
Sample Name: CCV3 Acquired: 2/25/2009 14:13:52 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment: y
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Ag3280
ppb
484.8
1.4
.2896
4349
483.3
486.1
Chk Pass
Be3l3Q-2
ppb
509.0
1.4
.2698
507-5
509.9
509.7
Chk Pass
All 670
ppb
5185.
27.
.5179
5163.
5177.
5215.
Chk Pass
Bi2230
ppb
515-3
42
.8140
512.1
513.9
520.1
Chk Pass
A13961
ppb
5082.
28.
.5481
5063.
5114.
5069.
Chk Pass
Ca3179
ppb
1969.
7.
.3788
1960
1973.
1972.
Chk Pass
As1890
ppb
492.6
4.2
.8426
488.6
492.3
496.9
Chk Pass
CaS9S3
ppb
2050.
3.
.1439
2047.
2053.
2049.
Chk Pass
B_2089
ppb
510.4
3.4
.6618
507.5
509.6
514.1
Chk Pass
Cd2288
ppb
505.5
32
.6273
503.1
504.3
509.1
Chk Pass
Ba4554
ppb
531-3
2.1
.3886
531.1
529.3
533.4
Chk Pass
Co2286
ppb
501.9
3.0
.5927
499.7
500.7
505.3
Chk Pass
Ba4554-2
ppb
509.5
23
.4503
509.8
511.7
507.1
Chk Pass
Cr2677
ppb
481.4
1.1
.2260
481.4
480.4
482.5
Chk Pass
Be2348
ppb
481-9
1.8
.3690
482.2
480.0
483.5
Chk Pass
Cu2178
ppb
528.1
4.2
.7866
524.3
527.4
532.6
Chk Pass
Be2S48-2
ppb
503.6
2.1
.4178
501.3
504.1
505.5
Chk Pass
Cu2199
ppb
5103
3.0
.5875
508.9
508.2
513.7
Chk Pass
BeS130
ppb
490.1
1.9
.3806
491.2
488.0
491.1
Chk Pass
Cu3273
ppb
505.2
72
1.431
496.9
510.2
508-5
Chk Pass
2/25/2009 14:38:36
2
Sampte Name: CCVS Acquired: 2/25/2009 14:13:52 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
VaJue
Range
Fe2599
ppb
4994.
15.
.2916
4938.
5010.
4983.
Chk Pass
Ni2S16
ppb
505.5
3.4
-6685
502.7
504.6
509.3
Chk Pass
Fa2714
ppb
4830.
26.
.5303
4834.
4802-
4853.
Chk Pass
P_1774
ppb
104O.
7.
.6305
1034.
1038.
1047.
Chk Pass
K_7664
ppb
5049.
38.
.7444
5083.
5009.
5055.
Chk Pass
Pb2203
ppb
492.1
32
.6507
490.0
490.6
495.8
Chk Pass
Li6707
ppb
4320.
11.
.2649
4313.
4333.
4314
Chk Pass
Sb2068
ppb
513.5
4.4
.8665
509.9
512.0
5184
Chk Pass
Mg2790
ppb
4002.
32.
.7944
3972.
4035.
3998.
Chk Pass
Sel960
ppb
491.8
6.3
1.280
488.8
487.6
499.0
Chk Pass
Mg2852
ppb
3977.
25.
.6181
3986.
3996.
3949.
Chk Pass
Mn2576
ppb
4965.
53.
1.076
5014.
4908.
4973.
Chk Pass
Si2124 Si2124-2
ppb ppb
F 556.4 532.6
3.0 8.3
.534^*^ 1.553
554.4
555.0
559.8
Chk Fail
500.0
10.00%
539.3
523.4
535.1
Chk Pass
Mn2576-2
ppb
5086.
16.
.3207
5067.
5094.
5097.
Chk Pass
Sn1899
ppb
435.4
3.5
.7147
482.9
484.0
489.4
Chk Pass
Mo2020 ,
ppb
512.8
3.6
.7011
509.9
511.7
516.3
Chk Pass
Sr2165
ppb
489.9
3.5
.7201
436.9
489.0
49S.3
Chk Pass
/^Na5895
ppb
5345.
38.
.7117
5342.
5384.
5308.
Chk Pass
Sr4215
ppb
511.5
1.3
.2567
510.7
513.0
510.7
Chk Pass
9^^3S^.
Sample Name: CCVS Acquired: 2/25/2009 14:13:52 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con'. Factor: 1.000000
User; admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
Ml
#3
Check?
Value
Range
Etem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2837
ppb
995.1
5.6
.5613
998.9
933.7
997.8
Chk Pass
Zr339l
ppb
1042
3.
.3315
1042
1038.
1045.
Chk Pass
T73349
ppb
499.3
2.5
.4960
500.7
4964
500.7
Chk Pass
Zr3S91-2
ppb
1046.
4.
.3749
1043.
1050.
1043.
Chk Pass
Ti3349-2
ppb
506.7
1.5
.3001
505.6
503.4
506.1
Chk Pass
TII 908
ppb
501.1
5.6
1.124
496.2
499.8
507.2
Chk Pass
U_2635
ppb
1982.
20.
.9976
1961.
2001.
1982.
Chk Pass
U_3S54
ppb
1841.
15.
.8260
1829.
1858.
1837.
Chk Pass
U,4090
ppb
2117.
28.
1.339
2128.
2034.
2138.
Chk Pass
V_2924
ppb
4905.
20.
.4083
4912
4883-
4921.
Chk Pass
Zn213S
ppb
509.3
32
.6358
506.6
508.3
512.9
Chk Pass
Zn2138-2
ppb
473.8
.7
.1549
473.0
474.0
474.5
ChK Pass
2/25/2009 14:38:36
4
Sampte Name: CCVS Acquired; 2/25/2009 14:13:52 Type: QC
Method: METHOD DVP{v114) Mode; CONC Corr. Factor: 1.000000
User: admin Custom tD1: Custom ID2: Custom IDS:
Comment;
InL Std.
Units
Avg
Slddev
%RSD
Y 2243
as/s 22571.
69.
.30560
Y 3600
Cts/S
163690.
956.
.58386
Y 3710
Cts/S
13645.
33.
.17759
#1
#2
#3
22627. 162870. 18668.
22591. 164740. 13607.
22494. 163450. 18659
896399853^
Sample Name: CCB3 /Vcquired: 2/25/2009 14:22:00 Type; QC
Method: METHOD DVP(v114) Mode: CONC Cor. Faclor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS: ,
Comment: v/
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Ag3280
ppb
.3625
.2335
78.20
.6607
.3302
.0965
Chk Pass
Be3130-2
ppb
-0658
.0352
53.40
.0436
.1064
.0475
Chk Pass
All 670
ppb
1.364
.238
17.45
1.108
1.406
1.578
Chk Pass
Bi2230
ppb
-1.717
1.433
83.47
-.6254
-1.136
-3.340
Chk Pass
AI3961
ppb
^.070
3.622
8900
-7.700
-.4564
-4.052
Chk Pass
Ca3179
ppb
27.66
1.33
6-611
27.12
26.16
29.70
Chk Pass
As1890
ppb
1.511
1.082
71.57
.4868
2.643
1.405
Chk Pass
Ca3933
ppb
32.54
.19
.5877
32.43
32.39
32.75
Chk Pass
B_2039
ppb
1.013
.388
38.30
.6264
1.403
1.011
Chk Pass
Cd2288
ppb
.1056
.0603
57.14
.0417
.1135
.1615
Chk Pass
Ba4554
ppb
.1845
.0873
47.35
.2739
-1800
.0994
Chk Pass
Co2286
ppb
.2575
.0571
22.16
.3218
.2127
.2381
Chk Pass
Ba4554-2
ppb
-.8589
.3023
35.20
-.5246
-.9390
-1.113
Chk Pass
Cr2677
ppb
-.2630
.1624
61.75
-.1683
-.4505
-.1701
Chk Pass
Be2343
ppb
.0619
.0332
53.54
.0420
-1002
.0435
Chk Pass
Cu217a
ppb
-1-066
2.005
188.0
-3.092
.9185
-1-026
Chk Pass
Be2348-2
ppb
-.4099
-3166
77-2S
-.0527
-.5214
-.6553
Chk Pass
Cu2199
ppb
1.066
.706
66.20
1.649
.2814
1.267
Chk Pass
BeS130
ppb
.2431
.0283
11.65
.2733
.2387
.2171
Chk Pass
CuS273
ppb
4.589
5218
113-7
10.09
-.2877
3.964
Chk Pass
2/25/2009 14:39:29
2
Sample Name: CCB3 Acquired: 2/25/2009 14:22:00 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con". Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom 1D3:
Comment;
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Fe2599
ppb
1.823
1.808
99.22
3.910
.7214
.8367
Chk Pass
Ni2316
ppb
.1515
.1035
68.33
.2554
.0485
.1505
Chk Pass
Fe2714
ppb
-2.505
5.526
220.6
.7909
.5794
-8.334
Chk Pass
P_1774
ppb
2.023
.526
26.00
1.449
2.139
2.481
Chk Pass
K_7664
ppb
-28.43
35.42
124.6
-32.68
-61.53
8.932
Chk Pass
Pb2203
ppb
-.2465
.2291
92.94
-.0721
-.5060
-.1614
Chk Pass
Li6707
ppb
-.8200
2171
264.8
1.632
-1.595
-2.497
Chk Pass
Sb2068
ppb
-8052
.7693
95.54
.4470
1.688
.2804
Chk Pass
Mg2790
ppb
3.230
19.29
597.2
-10.48
-5.118
25.28
Chk Pass
Sel960
ppb
.8121
1.521
1872
1.851
--9S31
1-518
Chk Pass
Mg2352
ppb
2.937
.710
24.16
3.160
2142
3.508
Chk Pass
Si2124
ppb
3.915
.566
14.45
3.467
4.551
3.728
Chk Pass
Mn2576
ppb
1.036
.330
31.82
1.371
1.028
.7112
Chk Pass
Si2124-2
ppb
.1975
4.328
2192.
-.7826
-3.556
4.931
Chk Pass
Mn2576-2
ppb
.7274
.2716
37.34
.4951
.6610
1.026
Chk Pass
Sn1899
ppb
.4311
.3055
70.86
.7434
.1329
4171
Chk Pass
Mo2020
ppb
.0787
.0445
56.55
.1062
.1027
.0274
Chk Pass
Sr2165
ppb
.4549
.1687
37.09
.3377
.6463
.3301
Chk Pass
Na5895
ppb
F 105.9
3.1
2.957
108.4
106.8
102.4
Chk Fail
100.0
-100.0
Sr4215
ppb
-.0749
.2599
347.2
.0332
.0671
-.3749
Chk Pass
99998^94
Sampte Name: CCB3 Acquired: 2'25/2009 14:22:00 Type: QC
Method: METHOD DVP(vl14) Mode: CONC Corr. Factor: 1.000000
User admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Umil
Low Limit
Etem.
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Umil
Low Limil
Th2837
ppb
-.2360
.9177
388.8
-1.257
.0301
.5192
Chk Pass
Zr3391
ppb
-.0027
.0351
1281.
.0018
-.0399
.0298
Chk Pass
TiSS49
ppb
.1076
.0784
72.81
.0321
.1022
.1886
Chk Pass
Zr3S91-2
ppb
1.603
1.330
82.96
2.891
.2345
1.684
Chk Pass
Ti3349-2
ppb
-1.247
.539
43.24
-.8374
-1.858
-1.045
Chk Pass
TII 908
ppb
.8389
.5520
65.80
.9216
.2502
1.345
Chk Pass
U_2635
ppb
17.14
18.61
108.6
33.26
-3-225
21.39
Chk Pass
U_S354
ppb
-48.08
19.74
41.04
-57.88
-25.37
-61.00
Chk Pass
U_4090
ppb
15.88
3.37
21.19
12.50
19.23
15.90
Chk Pass
V_2924
ppb
.5716
.3313
57.95
.2790
.5046
.9313
Chk Pass
Zn21S8
ppb
.2081
-0056
2.706
2134
2088
2022
Chk Pass
Zn21S8-2
ppb
.1296
.6572
507.2
-.1796
.8844
-.3160
Chk Pass
2/25/200914:39:29
4
Sample Name: CCBS Acquired: 2/25/2009 14:22:00 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Faclor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
Cts/S
22304.
42.
.19020
Y 3600
Cts/S
163310.
1020.
.62450
Y 3710
Cts/S
18765.
22-
.11963
#1
#2
#3
22351. 164190. 18766.
22295. 163550. 18743.
22268. 162190. 18788.
^9899595
Sample Name: 0812092-PS2
Method: METI-
User: admin
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#3
Check?
High Limit
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High LlmK
Low Limit
10DDVP(vll4)
Custom IDl:
Ag3280
ppb
104.8
1.3
1.277
106.3
103.9
1042
Chk Pass
BeSlSO
ppb
103.7
12
1.186
105.0
102.7
103.3
Chk Pass
Acquired: : 2/25/2009 14:29:04 Type: Unk
Mode: CONC Con. Facton 1.000000 ,^ — ir.-.^ opV* c.,«,nm im- ^VI -^ 2-, OOO ?V t>
All 670
ppb
2076.
14.
.6659
2061-
2089.
2078.
Chk Pass
Be3130-2
ppb
104.7
.5
.4952
105.2
104.6
1042
Chk Pass
AI3961
ppb
2117.
22.
1.034
2136.
2093.
2122.
Chk Pass
Bi2230
ppb
104.9
.4
.4017
104.4
104.9
105.3
Chk Pass
AS1890
ppb
108.1
1.0
.9233
109.3
107.3
107.8
Chk Pass
Ca3179
ppb
F 508700.
7333.
1.541
516600
508500.
500900.
Chk Fail
500000.
-500000.
'
B_2089
ppb
279-0
1.8
.6312
277.6
281.0
273.6
Chk Pass
Ca393S
ppb
t. *****
Chk Pass
Ba4554
ppb
114.3
1.4
1.198
115.8
1132
113.8
Chk Pass
Cd2288
ppb
108.9
.6
.5528
103.3
109.5
108.3
Chk Pass
Ba4554-2
ppb
113.8
.4
.3502
1143
113.5
113.7
Chk Pass
C02286
ppb
147.7
.9
.6010
146.8
148.6
147.7
Chk Pass
Be2S48
ppb
105.2
12
1.181
106.6
104.3
104.6
Chk Pass
Cr2677
ppb
98.26
.92
-9361
99.27
97.47
98.04
Chk Pass
—^—
Be2S4S-2
ppb
106.5
.4
.3723
106.8
106.1
106.6
Chk Pass
Cu2178
ppb
107.5
1.6
1.482
1062
107.0
109.3
Chk Pass
2/25/2009 14:39:42
2
Sample Name: 0812092-PS2
Meihod: METHOD DVP(vl 14)
User: admin
Comment;
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Umit
Custom IDl
Cu2l99
ppb
110.5
1.7
1.545
109.0
112.S
110.1
Chk Pass
^^ Mn2576-2
ppb
7353.
37.
.4999
7396.
7331.
7333.
Chk Pass
Acquired: 2/25/2009 14:29:04 Type: Unk
Mode: CONC Con. Factor: 1.000000
Custom ID2:
Cu3273
ppb
136.5
4.2
3.043
132.0
140.2
1372
Chk Pass
^
Mo2020
ppb
119.2
.9
.7439
118.3
120.1
119.3
Chk Pass
Fe259g
ppb
10300.
70.
.6806
10370.
10280.
10230.
Chk Pass
Na5895
ppb
250400.
1596.
.6373
252200.
249300.
249700.
Chk Pass
Custom IDS;
Fe2714
ppb
9927.
126.
1.272
10070.
9857.
9851.
Chk Pass
Ni2316
ppb
160.9
1.0
.6045
1602
162.0
1606
Chk Pass
K_7664
ppb
16630.
95.
.5734
16710.
16660.
16530.
Chk Pass
P_1774
ppb
4.742
-321
6-769
4.402
5.041
4.782
Chk Pass
Li6707
ppb
2146.
17.
.7729
2165.
2139.
2134.
Chk Pass
Pb2203
ppb
89.91
.27
.3035
90.15
39.61
89.96
Chk Pass
Mg2790
ppb
231600.
1039.
.4486
232800.
231000.
230900.
Chk Pass
Sb2068
ppb
107.6
1.1
1.028
108.8
106.6
107.4
Chk Pass
Mg2852
ppb
F 221800.
1237.
.5578
222400.
222600.
220400.
Chk Fail
10000.
-10000.
Sel960
ppb
103.9
2.0
1.929
104.8
1052
101.6
Chk Pass
Mn2576
ppb
7309.
76.
1.036
7362.
7223.
7S43.
Chk Pass
312124
ppb
5859.
29.
.4875
5832.
5889.
5857.
Chk Pass
^88^996
Sample Name: 0812092-PS2 Acquired; 2/25/2009 14:29:04 Type; Unk
Method: METHOD DVP{v114) Mode: CONC Con. Factor; 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS;
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Si2124-2
ppb
5243.
19.
.3590
5221.
5251.
5256.
Chk Pass
U_3854
ppb
-63.68
25.10
39.42
-43.29
-61.71
-56.04
Chk Pass
Snl899
ppb
95.06
.61
.6399
94.54
95.73
94.91
Chk Pass
U_4090
ppb
52.86
6.32
11.96
55.05
57.79
45.73
Chk Pass
Sr2165
ppb
11590.
54-
.4656
11540
11650.
11590.
Chk Pass
V_2924
ppb
18.65
.27
1.427
18.37
18-67
18.90
Chk Pass
Sr4215
ppb
12630.
84.
.6624
12720.
12570.
12590.
Chk Pass
Zn2138
ppb
255.0
1.6
.6318
253.5
256.7
254-8
Chk Pass
Th2837
ppb
-.4623
.3817
82.55
-.6436
-.7196
-.0238
Chk Pass
Zn2138-2
ppb
227.4
.8
.3520
228.3
226.8
227.1
Chk Pass
TiSS49
ppb
108.1
1.3
1.210
109-6
107.1
107-5
Chk Pass
ZrSS91
ppb
-.1866
.0827
44.32
-.2034
.-.2595
-.0968
Chk Pass
Ti3349-2
ppb
112.1
1.0
.8768
113.0
1122
111.1
Chk Pass
Zr3391-2
ppb
1.858
1.001
53.87
.7235
2616
2.235
Chk Pass
TI1908
ppb
88.42
1.42
1.611
37.39
90.04
87.32
Chk Pass
U_2635
ppb
50.46
8.13
16.10
41.99
58.19
51.21
Chk Pass
2/25/2009 14:39:42
4
Sampte Name: 0812092-PS2
Method: METHOD DVP(vll4)
User: admin Custom IDl:
Comment;
Acquired: 2/25/2009 14:29:04 Type: Unk
Mode; CONC Con-. Factor: 1.000000
Custom ID2; Custom IDS:
Int. Std.
Unils
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
19775.
143.
.72525
19935.
19731.
19653.
Y 3600
Cls/S
143340.
883.
.61596
142420.
144180.
143430
Y 3710
Cts/S
17705.
35.
.19534
17670.
17706.
1773?.
sotiatsooQ.'y
Sampte Name: BLK Acquired: 2/25/2009 14:37:03 Type: Unk
Method: METHOD DVP(vl14) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment: ^/^
Elem
Unils
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Etem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limil
Ag3280
ppb
-.2967
.2214
74.62
-.3829
-.0452
-.4620
Chk Pass
BeS 130-2
ppb
.0494
.1276
258.5
.0209
-.0616
.1837
Chk Pass
A(1670
ppb
1.333
214
16.02
1.575
1.253
1.171
Chk Pass
Bi2230
ppb
-3.126
1.873
59.93
-2.697
-5.176
-1.504
Chk Pass
AI3961
ppb
-8.919
8.196
91,89
-a.736
-1721
-.8162
Chk Pass
CaS179
ppb
47.16
22.92
48.60
23.33
49.10
69.04
Chk Pass
As 1890
ppb
2.088
.992
47.49
3214
1.342
1.709
Chk Pass
Ca3933
ppb
58.11
18.55
31.92
37.56
63.14
73,62
Chk Pass
B 2089
ppb
.2564
.2558
99.80
-.0306
.3388
.4608
Chk Pass
012288
ppb
-0587
.0356
145.8
-.0229
-0513
.1478
Chk Pass
Ba4554
ppb
.0119
.0360
302.0
.0305
.0343
. -.0296
Chk Pass
Co2286
ppb
.0879
,1507
171.4
-.0313
.1377
.2074
Chk Pass
Ba4554-2
ppb
.0133
.3131
2345.
-.1737
-.1611
.3743
Chk Pass
Cr2677
ppb
-.3948
.5236
132.6
-.0209
-.9932
-.1703
Chk Pass
Be2348
ppb
.0174
.0476
273.6
.0615
-.0331
.0238
Chk Pass
Cu2178
ppb
.4583
.6565
143.3
1.196
-.0629
.2422
Chk Pass
Be2348-2
ppb
-.2429
.2852
117.4
-.1790
.0049
-.5547
Chk Pass
Cu2199
ppb
.7709
1.241
161.0
1.343
1.623
-.6534
Chk Pass
BeSlSO
ppb
.1976
.0353
17.85
.2270
.1585
.2073
Chk Pass
Cu327S
ppb
5.483
3.760
68.59
8.413
1.242
6.793
Chk Pass
2/25/2009 15:03:36
2
Sampte Name: BLK Acquired: 2/25/2009 14:37:03 Type: Unk
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
»3
Check?
High Limit
Low Limil
Fe2599
ppb
2.626
4.884
. 186.0
3.703
-2.707
6.381
Chk Pass
Ni2S16
ppb
.3015
.2126
70.52
.2596
.1129
.5318
Chk Pass
Fe2714
ppb
6.245
3.617
57.91
6.343
2581
9.812
Chk Pass
P_1774
ppb
.5026
.6763
134.6
1.281
.0574
.1696
Chk Pass
K_7664
ppb
26.74
58.09
217-3
-39.26
70.13
49.33
Chk Pass
Pb2203
ppb
1.237
.752
60.82
2001
1213
.4971
Chk Pass
U6707
ppb
-1.408
3.532
250.8
-1.009
-5.123
1.907
Chk Pass
Sb2068
ppb
.8681
.9947
114.6
2017
.3149
.2730
Chk Pass
Mg2790
ppb
34.85
19.83
56.90
13.51
5271
38.32
Chk Pass
Sel960
ppb
1.075
.852
79.25
1.493
1.636
.0947
Chk Pass
Mg2352
ppb
25.77
8.17
31.70
17.30
26.40
33.61
Chk Pass
Si2124
ppb
3.763
.299
7.940
3.652
4.101
3.536
Chk Pass
Mn2576
ppb
1.137
.481
4231
1.637
1.095
-6781
Chk Pass
Si2124-2
ppb
3.830
5-814
151.8
10.50
1.185
-1906
Chk Pass
Mn2576-2
ppb
1.197
.390
32.60
1.490
.7538
1.347
Chk Pass
Snl899
ppb
.5523
.0372
6.729
.5158
.5901
.5510
Chk Pass
Mo2020
ppb
-.0412
.0846
205.3
.0520
-.0625
-.1131
Chk Pass
Sr2165
ppb
.9642
.3396
35.22
.5726
1.178
1.142
Chk Pass
Na5895
ppb
170.6
1.6
.9646
172.4
1692
170.1
Chk Pass
Sr4215
ppb
1.714
.395
23.07
1-SOl
1.753
2.083
Chk Pass
68^9^
Sampte Name: BLK Acquired: 2/25/2009 14:37:03 Type: Unk
Method: METHOD DVP(vll4) Mode: CONC Con. Factor; 1.000000
User: admin Custom IDI: Custom 1D2: Custom ID3:
Comment:
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Th2337
ppb
-.0064
.4400
6397.
-.3515
-.1568
.4891
Chk Pass
Zr3391
ppb
-.1015
2111
207.9
-.0685
.0911
-.3271
Chk Pass
Ti3349
ppb
.0873
.0538
61.63
.0747
.0409
.1463
Chk Pass
ZrS391-2
ppb
1.915
.401
20.93
2.181
2.111
1.454
Chk Pass
Ti3S49-2
ppb
-.1512
-5430
359-0
-.0520
--7370
.3353
Chk Pass
Til 908
ppb
.1512
.9205
608.8
.5910
-.9067
.7694
Chk Pass
U_26S5
ppb
9.909
10.80
109.0
-2.265
18.34
13.66
Chk Pass
U_3854
ppb
-56.72
34.32
60.51
-87.70
-19.82
-62.63
Chk Pass
U_4090
ppb
27.60
8.08
29.27
29.46
34.60
18.76
Chk Pass
V_2924
ppb
-.2135
.1804
34.53
-.0974
-.4213
-.1216
Chk Pass
Zn2l38
ppb
--5820
.0939
16.14
-.6122
-.6571
-.4766
Chk Pass
Zn2138-2
ppb
-.8953
.8614
96.22
-1.434
.0982
-1.350
Chk Pass
2/25/200915:03:36
4
Sample Name: BLK Acquired; 2/25/2009 14:37:03 Type: Unk
Method: METHOD DVP{v114) Mode; CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment;
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
as/s 21307.
22.
.10259
Y 3600
Cts/S
157270.
1331.
.34642
Y 3710
Cts/S
17614.
28.
.15868
#1
#2
#3
21318. 156830. 17644.
21321. 156220. 17589.
21282. 158770. 17609.
9988^995
Sampla Name: CRI Acquired: 2/25/2009 14;44;49 Type; QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDl: Custom 1D2: Custom IDS; .
Comment: -\/
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Ag3280
ppb
19.38
.48
2.498
18.82
19.69
1962
Chk Pass
BeS 130-2
ppb
20.41
.65
3.193
19.66
20.77
20.81
Chk Pass
All 670
ppb
231.0
1.1
.4870
2314
229.7
231-8
Chk Pass
512230
ppb
17-58
1.00
5.679
18.73
16.96
17.05
Chk Pass
A13961
ppb
207.4
17.0
8.211
200.3
226.8
195.1
Chk Pass
CaS179
ppb
70.69
2.55
3.609
67.75
72.05
72.27
Chk Pass
Asl890
ppb
20.64
1.41
6.833
19.03
21.22
21.67
Chk Pass
CaS933
ppb
84 92
1.24
1.461
84.20
84.21
36.35
Chk Pass
B_2089
ppb
20.74
.17
.8153
20.58
20.72
20.92
Chk Pass
Cd2283
ppb
2047
.12
.6099
20.44
20.36
20.61
Chk Pass
Ba4554
ppb
21.44
.20
.9302
21.54
21-21
21.57
Chk Pass
002286
ppb
20.39
.11
.5289
20.29
20.39
20.50
Chk Pass
Ba4554-2
ppb
19.88
.79
3.954
19.05
20.61
19.99
Chk Pass
Cr2677
ppb
18.41
.20
1.034
18.61
18.21
18.41
Chk Pass
Be2348
ppb
18.29
.25
1.374
18.33
18.03
18.53
Chk Pass
Cu2178
ppb
21.39
.84
3.910
21.41
22.21
20.54
Chk Pass
Be2348-2
ppb
19.86
.21
1.040
19.73
19.75
20.10
Chk Pass
Cu2199
ppb
22.18
.96
4-336
22.00
23.22
21.32
Chk Pass
BeSlSO
ppb
18.58
.25
1.333
18.68
18.30
18.76
Chk Pass
CuS273
ppb
F 31.35
4.40
14.04
32.15
35.29
26.60
Chk Fail
20.00
50.00%
2/25/2009 15:03;57
2
Sampte Name: CRI Acquired; 2/25/2009 14;44:49 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User; admin Custom IDl; Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
#2
*3
Check?
Value
Range
Fe2599
ppb
198.8
4.3
2.163
194.3
199.1
202.9
Chk Pass
Ni2316
ppb
2OS0
.09
-4110
20.89
20.30
20.71
Chk Pass
Fe2714
ppb
184-1
5.1
2.796
183.1
179.5
189.7
Chk Pass
P_.1774
ppb
1409
.9
.6053
141.9
140.5
140.3
Chk Pass
K_7664
ppb
1549
17.9
11.59
151.1
1744
139.2
Chk Pass
Pb2203
ppb
21.31
1.14
5.353
21.36
22.43
20.15
Chk Pass
U6707
ppb
176.1
3.7
2.101
172.0
1772
179.1
Chk Pass
Sb2068
ppb
21.13
.98
4.622
21.07
2214
20.19
Chk Pass
Mg2790
ppb
156-9
132
11.60
153.5
176.6
1407
Chk Pass
Sel960
ppb
23.13
1.13
4.901
22.17
22.84
24.33
Chk Pass
Mg2S52
ppb
162.3
3.3
2.057
158.8
162.8
165.4
Chk Pass
Si2124
ppb
139.6
1.5
1.088
139.1
13S.3
141.3
Chk Pass
Mn2576
ppb
203.7
2.3
1.365
205.2
200.5
205.3
Chk Pass
Si2124-2
ppb
115.3
3.0
2.627
117.9
116.1
112.0
Chk Pass
Mn2576-2
ppb
205.9
4.9
2.398
200.2
208.5
209,0
Chk Pass
Sn1899
ppb
19.34
.15
.7532
19.99
19.69
19.34
Chk Pass
Mo2020
ppb
20.91
-04
.1887
20.96
20.90
20.88
Chk Pass
Sr2l65
ppb
20.36
.15
.7553
20.30
20.53
20.24
Chk Pass
NQ5895
ppb
F 315.8
23.0
7.269
313.3
339.7
293.9
Chk Fail
200.0
50.00°!!
Sr4215
ppb
20.32
.33
1.626
20.15
20.12
20.70
Chk Pass
K^83t^
2/25/2009 15:03:57
3
Sample Name: CRI Acquired: 2/25/2009 14:44:49 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
J»3
Check?
Value
Range
Elem
Units
Avg
Stddev
%RSD
#1
ft2
Check?
Value
Range
Th2837
ppb
133.9
1.8
1.363
135.1
131.8
134.8
Chk Pass
Zr3391
ppb
145.5
1.7
1.193
1462
143.5
146.7
Chk Pass
TiS349
ppb
19.90
.31
1.577
2026
19-71
19.72
Chk pass
Zr339l-2
ppb
148.4
1.9
1.263
146.3
ld9.9
149.0
Chk pass
Ti 3349-2
ppb
20.11
.48
2,391
20.30
19.57
20.47
Chk Pass
Til 903
ppb
21.73
1.12
5.163
20-50
22-02
22.68
Chk Pass
U_2635
ppb
222-7
16.4
7.381
215.7
210.9
241.5
None
U_3854
ppb
111.6
132
11.85
1262
100.6
107.8
None
U_4090
ppb
192.8
4.9
2.561
193-6
197.3
187.5
None
V_2924
ppb
190.7
2.7
1.432
1920
187.5
192.5
Chk Pass
Zn2138
ppb
20.02
.10
.4944
19.90
20.06
20.09
Chk Pass
Zn2138-2
ppb
19.17
.14
.7173
19.26
19.23
19.01
Chk Pass
2/25/2009 15:03:57
4
Sample Name: CRI Acquired: 2/25/2009 14:44:49 Type: QC
Method; METHOD DVP(v114) Mode: CONC Corr. Factor; 1.000000
User: admin Custom IDI: Custom 1D2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cts/S
21342.
42.
.19578
21365.
21368.
21294.
Y 3600
Cts/S
159^60.
1020.
.63554
158660.
160700.
159P40.
Y 3710
Cts/S
17835.
155.
.86941
18003.
17804.
17697.
9888^191
\
(^iW ^\c^W\
:-LJt M-KJU^ I xJ.\J^..\J I
Sample Name: CCV "^ Acquired: 2/25/2009 14:51:46 Type: QC
Method: METHOD DVP(vl 14) Mode: CONC Con. Faclor: 1.000000 *
User: admin Custom IDl: Custom ID2: Custom IDS: .^
Comment:
Elem
Units
Avg
Stddev
%BSO
#1
#2 .
#3
Check?
Value
Range
Elem
Units
Ave
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
AgS280
ppb
487.0
5.6
1.154
484.2
483.4
493.5
Chk Pass
BeS 130-2
ppb
508.2
.7
.1347
503.8
508.3
507.5
Chk Pass
AH 670
ppb
5129.
6.
.1116
5123.
5135.
5129.
Chk Pass
Bi2230
ppb
507.3
1.9
.3678
503.5
508.2
505.2
Chk Pass
At3961
ppb
5125.
14.
.2649
5128.
5137.
5110.
Chk Pass
Ca3179
ppb
1967.
12
.6319
1958.
1981.
1962.
Chk Pass
As 1890
ppb
487.0
12
.2545
486.6
486.1
488.4
Chk Pass
CaS933
ppb
2058.
6.
.2909
2052.
2064.
2059.
Chk Pass
B_2089
ppb
505.6
.5
.0979
505.8
505.0
505.9
Chk Pass
Cd2288
ppb
501.3
.5
.0935
501-5
500.7
501.5
Chk Pass
Ba4554
ppb
538.2
5.8
1.077
534.8
534-9
544.9
Chk Pass
Co2236
ppb
497.5
.8
.1594
497.1
497.0
498.4
Chk Pass
Ba4554-2
ppb
507.9
1.7
.3443
509.6
507.8
506.1
Chk Pass
Cr2677
ppb
481.6
6.7
1.184
478.8
477.7
488.1
Chk Pass
Be2348
ppb
478.8
5.6
1.180
475.9
475.1
435.3
Chk Pass
Cu2178
ppb
530-3
.5
.0354
530.4
529.9
530.8
Chk Pass
Be2348-2
ppb
509.3
1.7
.3256
510.8
509.7
507.5
Chk Pass
Cu2199
ppb
507.5
.9
.1772
506-4
507.8
508.1
Chk Pass
BeSlSO
ppb
484-8
5.2
1.073
481.8
481.8
490.3
Chk Pass
CuS27S
ppb
503.7
1.7
.3416
504.8
504.6
501.7
Chk Pass
2/25/200915:04:51
2
Sample Name: CCV Acquired: 2/25/2009 14:51:46 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check ?
Value
Range
Etem
Units
Avg
Stddev
%PSD
#1
#2
#3
Check?
Value
Range
Fe2599
ppb
4966.
19.
.3780
4976.
4951.
4940.
Chk Pass
Ni2S16
ppb
506.2
2.3
.4606
504.2
505.8
508.8
Chk Pass
F62714
ppb
4833.
49.
1.017
4791.
4820.
4887.
Chk Pass
P_1774
ppb
1016.
1.
.0572
1015.
1016.
1016.
Chk Pass
K_7664
ppb
4922.
57.
1.161
4857.
4949.
4961.
Chk Pass
Pb2203
ppb
489.6
2.0
.4169
490.9
487.3
490.7
Chk Pass
Li6707
ppb
4386.
14
.3243
4391.
4396.
4369.
Chk Pass
Sb2063
ppb
508.3
1.1
.2242
5072
50S.2
509.5
Chk Pass
Mg2790
ppb
3972-
23.
.5722
3965.
3953-
3997.
Chk Pass
Se1960
ppb
495-3
3-7
.7413
491.6
495.3
499.0
Chk Pass
MQ2852
ppb
3969.
13.
-3240
3978.
3975.
3954.
Chk Pass
3(2124
ppb
F 558.7
2.9
.520^.,
559."8
555.4
560.9
Chk Fail
500.0
10.00%
Mn2576
ppb
5069.
47.
.9349
5075.
5019.
5113.
Chk Pass
Si2124-2
ppb
521.4
11.3
fe- 2.161
534.3
51S.6
5162
Chk Pass
Mn2576-2
ppb
5128.
6.
-1164
5135.
5124.
5126.
Chk Pass
Sn1399
ppb
477.3
.5
.1064
476.9
477.2
477.9
Chk Pass
Mo2020
ppb
514-4
1.3
.2538
513.2
5142
515.8
Chk Pass
Sr2165
ppb
483.1
.1
.0253
483.0
433.1
483.2
Chk Pass
Na5895
ppb
5363.
8-
.1444
5357.
5372.
5360.
Chk Pass
Sr4215
ppb
512.7
14
.2753
513.6
513.3
511.1
Chk Pass
99^192
H
^LV\ ^Vil 0'
Sample Name: CCV H Acquired: 2/25/2009 14:51:46 Type: QC
Meihod: METHOD DVP(vl 14) Mode: CONC Con. Factor: 1 OOOOOO
User: admin Custom IDI; Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check ?
Value
Range
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
Value
Range
Th2B37
ppb
981.6
7.6
.7732
973.1
976.5
990.3
Chk Pass
ZrSS91
ppb
1061-
11.
1.057
1055.
1055.
1074.
Chk Pass
TiS349
ppb
503.7
5.6
1.112
500.2
500.8
5102
Chk Pass
Zr3S91.2
ppb
1053-
1.
.1028
1054.
1053.
1052.
Chk Pass
Ti3349-2
ppb
508.6
2.1
.4132
506.6
. 510.8
508.5
Chk Pass
TI1908
ppb
503.2
3-4
.6695
500.8
501.7
507.0
Chk Pass
U^2635
ppb
1996.
9.
.4360
1990.
1992.
2006.
Chk Pass
U_3854
ppb
1923.
38.
1.965
1892.
1912
1965.
Chk Pass
U_4090
ppb
2152
32.
1.473
2146.
2124
2137.
Chk Pass
V_2924
ppb
4913.
55.
1.110
4881.
4883.
4976.
Chk Pass
Zn2138
ppb
508.8
12
.2370
507.9
503.2
510.1
Chk Pass
Zn2133-2
ppb
476.1
.9
.1833
475-1
476.1
476.9
Chk Pass
2/25/2009 15:04:51
4
Sample Name: CCV Acquired: 2/25/2009 14:51:46 Type: QC
Method: METHOD DVP(v114) Mode: CONC Con. Factor: 1.000000
User: admin Custom IDl; Custom iD2: Custom IDS:
Comment:
Int. Std.
Units
Avg
Stddev
%RSD
Y 2243
Cts/S
21680.
5.
.02098
Y 3600
Cts/S
156730.
1866.
1-1908
Y 3710
Cts/S
17912.
71.
.39712
#1
#2
#3
21676. 157660. 17865.
21678. 157950. 17877
21685. 154!i30. 179^4.
^^v
ffilv\ '\ W^
Sampte Name: CCB^ /Acquired: 2/25/2009 14:59:18 Type: QC
Method; METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000 /
User; admin
Comment:
Custom IDI: Custom ID2: Custom IDS:
1
Elem
Units
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Units
Avg
Stddev
%RSQ
#1
#2
#3
Check ?
High Limit
Lew Limit
Ag3280
ppb
-.0894
.1159
129.7
.0042
-2191
-.0534
Be3130-2
ppb
.2432
.2055
84.52
.4795
.1440
.1061
A11670
ppb
2.601
.204
7-837
2767
2.663
2.374
A13961
ppb
9.311
11.65
1252
3.082
21.53
-1.680
As1390
ppb
2.546
.750
29.43
2.007
2.230
3.402
B_2089
ppb
.4977
.1845
37.06
.6886
.4841
.3205
Ba4554
ppb
.0516
.0203
39.40
.0378
.0749
.0420
Ba4554-2
ppb
-.0767
.3369
504.7
.3586
-.2072
-.3315
Be2S48 Be234S-2
ppb ppb
.0787 -.0927
.0221 .2747
28.13 2962
.0780
.1011
.0569
-.1682
-.3217
2118
Bi22S0
ppb
-3.031
1.283
42.33
-3.396
-4.091
.1.605
Ca3179
ppb
-7.223
2.977
41.22
-10.62
-5.987
-5.063
CaS9SS
ppb
8-992
.655
7.287
9.733
8.757
8-487
Cd2288
ppb
.0519
.1090
210.0
.1293
-.0727
-0991
Co2286
ppb
.1311
.1463
111.6
.1505
-.0239
.2667
Cr2677
ppb
-.1792
.2680
149.6
-.2056
.1011
-.4329
Cu2178
ppb
-.1683
.9663
574.2
-.4179
-.9854
.8984
Cu2199
ppb
.5467
.6676
1221
1.106
-.1925
.7270
Be3130
Ppb
.2918
.0028
.9683
.2950
.2902
.2900
Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass
Cu3273
ppb
5.975
11-47
192.0
17.97
4.856
-4.899
Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass Chk Pass
2/25/200915:07:02
2
Sample Name: CCB Acquired: 2/25/2009 14:59:18 Type: QC
Method: METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDl: Custom ID2: Custom IDS:
Comment:
Elem
Units
Avg
Slddev
%RSD
#1
#2
#3
Check?
High Limit
Low Limit
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check ?
High Limit
Low Limit
Fe2599
ppb
5.752
2.559
44.50
6.791
2.836
7.628
Chk Pass
Ni2316
ppb
.1155
.2361
204.3
-.1534
.2117
.2834
Chk Pass
Fe2714
ppb
-1.008
6.539
648.7
3.469
2.020
-8.513
Chk pass
P_1774
ppb
-.7032
.0862
12.26
-.7931
-.6212
-.6952
Chk Pass
K_7664
ppb
-128-8
15.9
12.31
-1432
-111.3
-131.3
Chk Pass
Pb220S
ppb
-.0282
.0999
353.6
-.0397
.0769
-.1219
Chk Pass
Li6707
ppb
F2148
1.539
71.64
3.873
.9139
1.658
Chk Fail
2.000
-2.000
Sb2068
ppb
1.159
1.703
146.9
3.119
.0345
.3248
Chk Pass
Mg2790
ppb
15.95
2.97
18.60
15.29
19.19
13.37
Chk Pass
Sel960
ppb
1.992
1.148
57-60
.6754
2.524
2.1)1
Chk Pass
Mg2852
ppb
9.151
.266
2.903
9.030
8.967
9.456
Chk Pass
Si2124
ppb
4-119
.301
7.320
4.390
3.795
4172
Chk Pass
Mn2576
ppb
1.301
.105
3.063
1.253
1.421
1.225
Chk Pass
Si2124-2
ppb
-2.035
9.546
469.0
-12.84
5.2S7
1-502
Chk Pass
Mn2576.2
ppb
F 2.423
.149
6.157
2.253
2.481
2534
Chk Fail
2.000
-2.000
Snia99
ppb
-7662
.1020
13,31
.6497
.8393
.8096
Chk Pass
Mo2020
ppb
.1052
.0903
85.82
.2036
.0652
.0413
Chk Pass
Sr2165
ppb
.2787
.1843
66.13
.0801
.3117
.4443
Chk Pass
Na5895
ppb
F 114.2
16.4
14.35
117.1
96.57
129.0
Chk Fail
100.0
-100.0
Sr4215
ppb
.2190
.0585
26.73
.1758
.1956
.2856
Chk Pass
9§^Sui.wQ
•\ Sampte Name: CCB " Acquired: 2/25/2009 14:59:18 Type: QC
Method; METHOD DVP(v114) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2: Custom ID3:
Comment:
2/25/200915:07:02
3
Elem
Unils
Avg
Stddev
%RSD
#1
#2
#3
Check?
High Limil
Low Limit
Elem
Units
Avg
Stddev
%RSD
#1
ft2
#3
Check?
High Umil
Low Limit
Th23S7
ppb
-1.002
1.673
167.0
.9165
-1.759
-2.162
Chk Pass
Zr3391
ppb
.1027
.3659
356.2
-.2066
.0082
.5066
Chk Pass
Ti3349
ppb
-.1342
.1006
74.94
-.1642
-.0221
-2165
Chk Pass
Zr3391-2
ppb
1.660
.837
50.42
2.338
1.917
.7247
Chk Pass
Ti3349-2
ppb
-1.583
.809
51.12
-1.988
-2.111
-.6515
Chk Pass
TII 908
ppb
1.067
.099
9.316
1.179
1.031
.9903
Chk Pass
UJ635
ppb
30.60
21.25
69.44
42.85
42.89
6.062
Chk Pass
U_SS54
ppb
-58.01
6.78
11.69
-58.72
-64.42
-50.91
Chk Pass
U_4090
ppb
9.794
4.657
47.55
6.005
14.99
8.382
Chk Pass
V_2924
ppb
1.533
.382
24.92
1.199
1.950
1.449
Chk Pass
Zn21S8
ppb
-.4339
.0345
7.956
-.3948
-.4600
-.4470
Chk Pass
Zn2138-2
ppb
.0903
.2960
327.8
-.2456
.3132
.2033
Chk Pass
2/25/2009 15:07:02
4
Sample Name: CCB Acquired: 2/25/2009 14:59:18 Type: QC
Method; METHOD DVP(vl14) Mode: CONC Corr. Factor: 1.000000
User: admin Custom IDI: Custom ID2; Custom ID3:
Comment:
Int. Std.
Unils
Avg
Stddev
%RSD
#1
#2
#3
Y 2243
Cls/S
21644.
54.
.24902
21704.
21623.
21600.
Y 3600
Cts/S
157980.
391.
.24762
158140.
158270.
157540.
Y 3710
Cts/S
18198.
55.
.30079
1S165.
18169.
13261.
3893^185
D\oestion Log
gg^esi^
.1 I
Lionville Laboratory Incorporated
Digestion Batch i¥: L-^^^jy/S/"
Dat&Time Initiated: A/:^5/gj /tOnJ
DataTimc Completed: \^zJzvd^ U') O
Ana]yst(s): t^f^
Mabix: Soil ^^^M
Instr. Type: insir. type: AA riyr /
Parameters: (fjSh&jO > H^L /^^f^SD^ Pk'^
tS3>/ Undieestcd i ' (circieone) figaste©/ undigested I ' (
^^^»- m ;^,
Balance Cal Verify Y (N^
)lGESTIOf
Method: SW
(circle)
Logbook
1 RECORD
*:'T'?7
-.=£OP: L-SPI-3020 Rev. 00
%m^
3010A
3015
3020A
7060A (As/Sc)
7760A (Ag)
3050B
3051
DW
MCAWW
SM
200-7(1994)
200.9
3113B
200.7(1982)
200 (AA)
206.2 (.As/Se)
3030C OfC)
CLP ILMO3.0 Other
Hot Plate Temp:
t
^6'
coc Batch iLoiiV,
OSl^^CD/
4lH-
£^3 fTiP^ /ois
6M
mi^o9t'c\ ClP.
fH^
OT/
O^O-^O^O-OI
OiR-
O}'?
0^
L.9t 7.1^-^1 ^ fci
--
-"^
*§ Spike
|o^Vol(s)
(mL)
o.sA
CS J.
O.SIJL
(!,'5AA
\KM W-
-^ \
Initial
Wt/Vol
(g/mL)
7t»4
^^-
^ JlJ t4^
—•
.. fn /J./'^^^^-°--'^ VvUm^i^^'^^i Final
Vol
(mL)
^Aul
_ -
ri^
pH
<2
cL
,^
.
Type: '
To/So/
TC
r^
. —
—^
1
' t<lb-\i
Texture
/(i,rt-
«-^
_,_— •
nj
Color/Appearance
cXii^/ccL^^^^j^
A— ^/fUflOVS A^UM^
-
LMAAJ Lff'^-^^J-^^'^
1
_,^-^-—"
"^
Artifact
/
^^.-^^
Turb
Spiking IDs:
MS?*: gl,lfD-04^CV
LCS#:
Reagent IDs:
HNO3
HCL
H2O2
1:1 HNO3
1:1 HCL
IS. li
FileID#; ^^^^C^ ^A<?'V^*-s
LIMS Transfer: Y N ' 'T/^^P '
Lta Review By/Date: j
-5K ioi
L-SP1-3020-A-0601 Page#: 065
Lionville Laboratory
Incorporated
Analyst: ^^9
ICP RUN LOG
Metals Analysis by ICP
Logbook*: S^*^
- OP/Rev. # ME-ICP
Instnjment ID: J^^P^^QQ
Peak Profile: f^i&aACV\
Spectral Shift Units: -— Time: ^'^ S^
Data Pile
3Ddrfe22Sft
XCP022S&
"^^-^
Digest
Batch
L5o2_^S^
U3o2-M>7_
L^t^z-WTs,
ue>t3-2_\<D<i
"^^^^
Client Batcti
Numtwr
^"^
h<i\% CiST-
a<l>2.oio
0<i\2-\^0
©SN^*^^
O^fllA-?)
a<il2_6-73
^
^r\cyt^
7=[yi^-<^
SPLS
Bi)
07-
02.
Mathod
File
:v^ir^
1^'
01
o3frO >^,<.\>:>
oifvc p-:^
3)fl-C
^
""
'^^^S>h
^^
File Trans,
to LIMS
y-^
^^^^
Repro-
Rle
(Y/N)
CommBnis
CHJ
CN3
^\
Standard
ICAL
ICV/CCV
ME-lCP/O-0602
ID
5\2^o3Vo^ oz
—02^
Prep Date
W]og
Exp Oate
Reviewed by/Date.
Page# 077 B
-^Y\ ^i^ iO'
(pi'.n-* .\^ M'F-OTO;'.! j.ouo 'i-.v,
8^^8168
>
hti
^ t^ ^l Ir^
-J J J Ei«i
ifi^ IP 0
i 1 ) ^
^ fB
l\i^ ca
Cl-
-1^
V
,^
^ i
S
o
CD
CC
o
B
B n P CT
^
r-T-
1
•a
3'
O
£.
5*'
pa
o"
o o p
cr
o
3
r
p
3
o
B r
o "-b
F
o.
W3
r M
m
9
S 3
n
S
«:
a
1 B
3
0
0
I
Wi
\
\
.^ i
fJ \ 1 —
—
X
>
1
( 3
—
so
h o 3
3
o
B
n
8
<
o o*
p
4i.
3
, .
o o
N.
Lfl to
O t-ft
3 P
r- t-
o o p p o o ffi ffi o 2
" O
U
tZl
i
T
0
^
0
DA
7
1
0
T
0
• —
_
3
•—•
o 3 rr
^
^ o 3
i^ K)
O tJ%
B B
r- r O O
o o 3 S
ffi ffi
o 2 " o
O
L O
>
0
1
(A
T
0
ffN
p.
o o
3
Ut Nl
O f~n
B 3
r r
8 R 3 3 o o
ffi ffi o 2
~ o
o
e
<
_
0^
n \ * <
o
0
1 0
4
LP
KJ S3 IO
3 3 3 r 1- r-
K»
O
O
3
•-* Ltn
P b
P^ ^ s O 9 3 O
ffi 5
Q o
0
hi
9 fV^
' o
4
0\
0
1 1
0 0
0
0
1
0
5^
I—l
3
r
^
3
_^
3
t-
^ •
o o
3
<-rt to
o o« 3 3
r t-o o
o o P 3 o o
ffi ffi o 2 • - o
\ r
^
0
J
ft
0
^X.
^
^— ^ -1 — 3 3 3
1
, •
o o
3
r
<-rt S)
O Ul
3 3
r r
S S 3 3 O O
ffi ffi
o 2 ^ o laj
-<7
3
0
IP
cn
CD s a. n
a.
2
IP
3
o •1
P3
•-».
e
O T)
^.^
C^ O 3
« c E
i 3 Ei
•== "=^ »,i
3. £L £• 3'
'3 n
«Q A
r* "1
> 9 ' »
» 2 3
f» C: 9 5 '^
9
>
o
B.
o
O
J
O
o
r
a*
o
o
a n o
o
to
2:
o
5^2:
a e.
O w
o ^
o s^
o* OQ O* o o pr
I
ti-<
to
p-o
^
0 3 S-
n
fO
s
p
•1
c* a. o
B
;; •o to "1
2 o '0 r o
CTQ
o
OQ cr o o
^
H
QB^IK
End of Package
VLI
888^8X18
-2.
Laboratory A.a.V..caWcpon for DUSA.
ENERGr MM.MII«>fll«
ENERCYLABORATORIES, INC. • 2393SaltCrwkHighway(82601) • P.O. Box3258 • Casper, WYd2602
TdlFme888.235.0515 • 307.Z35.0515 • Fax [phone] • casper&energylab.com' www.e/^ergylab.com
LABORATORY ANALYTICAL REPORT
Client: Denison Mines (USA) Corp
Project: December Groundwater
tjblD: C08120444-003
Client Sample ID: MW32
ReportDate: 01/05/09
Collection Date: 12/09/08 10:50
DateReceived: 12/11/08
Matrix: Aqueous
Amryses RMult Unit! Qualtflen RL
MCU
QCL Mathod Analysis Oate / By
METALS - DISSOLVED
Cadmium
Iron
Manganese
Nickel
RADIONUCUDES. DISSOLVED
G(OSS Alptia minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
2.61 ugA.
9020 ugA.
5540 ug/L
59 ug/L
S.S pCi/L
0.8 pCi/L
0.4 pCl/L
0.50
30
10
20
E200.e
E200.7
E200.7
E200.8
E900.1
E900.1
E900.1
12/15/08 21:56/ts
12/3CM)8 16:58/cp
12/30/08 16:58/cp
12/15/08 21:56/1*
12/22/08 18:48/cgr
12/22/08 18:48/cgr
12/22/08 18:48/cgr
Raport
Dalinftfona:
RL - Analyts reporting limit
QCL - Quality control limit
MOC - Minimum detBCtabte concsntratian
MCL - Maximum contaminant level.
ND - Not detected at the reporting limit.