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DRC-2012-002112 - 0901a06880318da8
State of Utah GARYR HERBERT Governor GREG BELL Lieutenant Governor department of Environmental Quality Amanda Smith Executive Director DIVISION OF RADL\TION CONTROL Rusty Lundberg Director C-201^n)02112 October 22, 2012 Jo Ann S Tischler, Director, Compliance Energy Fuels Resources (USA) Inc 225 Union Boulevard, Suite 600 Lakewood, CO 80228 Subject Radioactive Matenal License No UTl900479 2012 Radiation Protection Inspection, Module RADMOD-SSS-01 Dear Ms Tischler This letter refers to the inspection conducted at the Energy Fuels Resources (USA) facility m Blandmg, UT on September 19 and 20, 2012 by a representative of the Division of Radiation Control (DRC), Utah Department of Environmental Quality The cooperation and hospitality afforded the DRC inspector by the personnel at the Blandmg uranium mill dunng the inspection are appreciated The inspection was an examination of your facilities as they relate to compliance with the Utah Radiation Control Rules and the conditions of the Radioactive Matenals License Number UT 1900479 The inspection consisted of personnel interviews, document reviews and direct observations by the inspector The activities and practices reviewed dunng the inspection with respect to radiological surveys, shipping conveyance and contamer releases, shipping papers, and radioactive calibration sources were found to be in compliance with relevant requirements, however, there are several recommendations that may strengthen the mill operations The recommendations are included m the enclosed Inspection Report If you have any question, please contact Boyd Imai at (801) 536-4250 Sincerely, Rusty Lundberg, Director RL/BMI bl Enclosure cc/enc David Turk, Energy Fuels Resources (USA), Blandmg, UT Shiya Wang, CDPHE, Denver, CO 195 North 1950 West • Salt Lake City, UT Mailing Address P O Box 144850 • Salt Lake City, UT 84114-4850 Telephone (801) 536-4250 • Fax (801) 533^097 'TDD (801) 536-4414 www deq Utah gov Pnnted on 100% recycled paper INSPECTION REPORT Inspection Module RADMOD-SSS-01 Surveys/Shipping Papers/Sources Radioactive Matenal License No UT 1900479 Inspection Location Energy Fuels Resources (USA), Blandmg, UT Inspection Date(s) September 19,2012 through September 20, 2012 Inspector Boyd Imai, Utah Division of Radiation Control (DRC) Accompanied By Shiya Wang, Colorado Department of Public Health and Environment (CDPHE) Personnel Contacted Daniel HiUsten, Tanner Holladay, Ronnie Nieves, Justin Perkins, Chance Singer, Terry Slade, David Turk Inspection Summarv The inspection was opened on September 19, 2012 v^ith a meeting among D HiUsten, R Nieves, D Turk, S Wang and the inspector. (S. Wang had requested to accompany and observe a DRC compliance inspection ) Inspection Objectives were stated which included. 1 Observe release surveys and preparation of product containers, equipment, conveyances (general releases and DOT compliance) 2 Assess completion of shipping papers and supporting documentation 3 Inventory Sources 4 Review release and facility surveys 5 Time permitting, look at a penmeter air sampling station Areas inspected included. • Ore Truck Releases • Product Drum Preparation • Product Drum Shipping Papers • Contamer Releases • Source Inventory • Penmeter Air Sampling Stations (informational only) The inspector held a closeout meeting on September 20, 2012 with D Hillsten, R Nieves, T Slade, and D Turk of Energy Fuels Resources and S Wang of the State of Colorado to review the inspection activities, observations, and conclusions Findings No citable violations or deficiencies were observed dunng the inspection Two minor items were addressed dunng the inspection 1) an operational procedure needs Page 1 of 6 F \wp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc updating and 2) a release survey form needs to be modified to document a 1-meter exposure rate reading on product drums. Inspection Items Ore Truck Releases Releasing empty ore trucks from the facility is a vexing regulatory problem. Compliance with the regulations is dependent upon the approach the facility chooses to take Procedures indicate that end dump trailers are released either for restncted or unrestncted use Two empty ore trucks were observed exiting the facility The extenors of the conveyances were decontaminated and radiological surveys were taken of the extenors Surveys of the intenors were not observed The conveyances were marked with the wordings "For Radioactive Matenal (Use) Only" and "Radioactive LSA" suggesting that the vehicles were being released under the provisions of 49 CFR 173 443(d) However, no shipping papers or documents were sent with the dnvers that would indicate that the vehicles were transporting a Class 7 radioactive matenal It was not clear whether the vehicles were released under restncted or unrestncted conditions If unrestncted, the trailers should not be marked "Radioactive LSA " Procedure titled End Dump Trailer Acceptance, Handling & Release, No. PBL-9 needs review and updating, e g references to UN2910 with respect to "EMPTY" packages needs to be changed to UN2908 and attached regulations are outdated For restncted release, the Licensee must comply with all applicable requirements and not just selectively choose provisions that provide relief from certain restnctions, e g applying conditions found m 49 CFR 173.443(d) does not absolve the shipper from compliance with all other hazardous matenal shipping requirements such as shipping papers, markings, labels, etc If the Licensee makes the determination that the released conveyance is not a Class 7 radioactive matenal transfer then 49 CFR 173 443(d) provisions cannot be applied and other release cntena must be applied, i e more restnctive contamination release levels Product Drum Preparation The product, UaOg "yellow cake" is packed in 55-gallon metal drums Drums used are certified Type A containers suitable for the shipment of Low Specific Activity (LSA-1) radioactive matenals A radiological survey was performed on each drum A contact dose rate survey and a contamination survey were performed on each drum The contamination survey was done with a direct frisk on each drum and a sample per load of drums had smear samples taken and analyzed for venfication purposes, all documented on the "Drum Contamination Survey" form Radioactive Yellow-H labels were not yet applied to the drums since it was only a partial load of drums that were being prepared at the time ofthe inspection. Labels and markings were to be applied later m the preparation process Deficiencies It was noted that a 1-meter dose rate was not measured dunng the drum preparation process This measurement is necessary m determining which type of radioactive matenal label is Page 2 of 6 F \vvp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc appropnate, i e Radioactive White-I, Radioactive Yellow-E, or Radioactive Yellow-in as per 49 CFR 172 403(b) and (c) and 173 403, Transport Index Dunng the closeout meeting the Licensee indicated that the measurement is taken before the drums are loaded onto the transport vehicle Product Drum Shipping Papers From the previous inspection deficiencies were noted in the shipping paper information A sample of the shipping papers of recent shipments was examined for completeness It was venfied that the deficiencies identified in the pnor inspection were corrected The Licensee uses a Straight Bill of Lading as the shipping papers and m those reviewed no discrepancies were identified However, there was a document associated with the Straight Bill of Lading that did not precisely conespond with the information provided on the shipping paper Specifically, the document titled "Shipping Paper" did not identify the category of label applied to each package in the shipment as required in 49 CFR 172 203(d)(4) and it did not identify the chemical form as specified m 49 CFR 172 203(d)(2) Further, the proper shipping name did not include the "(LSA-1)" designation Apparently, this information is maintained on a spreadsheet for mtemal purposes and is not utilized as the shipping paper prescnbed in 49 CFR 172 200 through 204 The dnver of the transport vehicle is provided with a "Dnver Routing Instruction" and "Camers' Instructions." Deficiencies The instructions provided to the dnvers should include the information specified in 49 CFR 173 403 Exclusive Use and required by 173 427(a)(6)(iv) Container Releases Three intermodal containers GFLU001035, GFLUOOl 180, and GFLUOOl 1801 were qualified for unrestncted release Release surveys of these containers are documented on "Energy Fuels Resources (USA) Inc , Equipment Survey for Unrestncted Release" forms No containers were bemg released as "EMPTY" UN2908 dunng the inspection Deficiencies None Source Inventory The Source Inventory list was checked against the sources in storage The Licensee indicated that only two of the sources on the list are used to check detection instruments, the remainder are not utilized for any purposes The Licensee provided documentation for source leak testing performed by Ronan Engineenng Co Deficiencies The Source Inventory list did not identify four check sources m storage* Bi-210 (0 053 |LICI), Page 3 of 6 F \wp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Cl-36 (0 0182 nCi), Pm-147 (0 096 jiCi), and C-14 (0 165 \iCi) And there was one missmg Th- 230 source no 5995-09 (on the list but not m storage) None of these sources are used Perimeter Air Sampling Stations As a courtesy, the Licensee escorted the inspector and S Wang to an air sampling site to see how a station is configured and assembled Samples are collected for particulate monitonng, radon monitonng, and gamma dose at each of five sampling locations ; Closeout Meeting The inspector held a closeout meeting with D Hillsten, R Nieves, T Slade, and D Turk of Energy Fuels Resources (USA) and S Wang of CDPHE on September 20,2012 The observations descnbed above were summanzed dunng the meeting Recommendations to the Licensee Operating Procedures It IS strongly recommended that operating procedures No PBL-2, Intermodal Container Acceptance, Handling & Release and No PBL-9, End Dump Trailer Acceptance, Handling & Release be reviewed and updated There have been changes to the U S Department of Transportation (DOT) hazardous matenal transportation regulations since the procedures were first implemented and those changes need to be reflected in the procedures, including the attached DOT excerpts Of particular importance, in this regard, is the change to the contamination limits table found m 49 CFR 173 443 (Table 11 m the old regulations. Table 9 m the current regulations) Outwardly it appears that the limits were increased by a factor of 10 However, this is not the case Essentially, the limits are the same but a distinction is made between smearable/wipeable contamination (Table 11) and total removable contamination (Table 9) In Table 11a wiping efficiency (0.10) is factored in the table values, whereas, the shipper must adjust the survey results to convert smearable/wipeable contamination to total removable contamination before companng numbers with the Table 9 limits The shipper may use actual wipe efficiency or may use an assumed efficiency of 0 10 It IS a suggested that the procedural requirements for releasing conveyances and packagmgs as "EMPTY" be revised to conespond with the requirements specified in 49 CFR 173 428 including contamination and dose rate limits The UN number for empty packagmgs changed from UN 2910 to UN 2908 Although not prohibited, the notice "This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive matenal, excepted package-empty packaging, UN 2908" is no longer required to accompany the shipment (formerly specified in 49 CFR 173 422, last appeanng in the 2003 edition) Although this notice is cunently applied to the outgoing empty containers and contains the four digit UN identification number for empty packagmgs, for bulk containers there is a size requirement for the UN 2908 marking (49 CFR 172 302 and 173 332) which the number on the notice does not conform As was discussed in the closeout meeting, caution is encouraged when releasing end dump trucks and other conveyances that transported the uranium ores, especially with "restncted" releases Page 4 of 6 F \wp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Release cntena may depend upon the classification of the ore when it amved at the Licensee's facility A DOT regulated Class 7 radioactive matenal shipment upon amval may dictate what levels of radiological contamination and exposure rates are permissible for release. The Licensee may have a number of options but must apply all the cntena that correspond to the option selected For example, a shipper may apply the provisions found in 49 CFR 173 443(d) but cannot ignore the other radioactive matenal. Class 7 requirements found m 49 CFR Subchapter C Unfortunately, when the DOT changed the defimtion of "radioactive matenal" from a concentration of 2000 pCi/g of any radionuclide to radionuclide specific concentrations and consignment activity limits conesponding changes were not made to accommodate special provisions such as 49 CFR 173 443(d). Shippers are left to figure it out for themselves Full compliance is a difficult task that takes carefbl assessment and scrutiny The Licensee indicated that the "lawyers" might need to get involved in this matter The Licensee should use the term "exclusive use" cautiously The t6rm has several meamngs and could impact compliance issues if not used in the proper context, especially if it is in reference to the provisions m 49 CFR 173 443(d). It is recommended that, because the regulations have changed since the procedures were first implemented, a careful review of the current regulations be performed and that the procedures be revised to capture all applicable options that the Licensee may choose to take m releasing conveyances It should be kept m mind that when doing the review there are multiple options for a "restncted release" each with separate and distinct radiological release and hazardous matenal shipping cntena Shipping Papers It appears that the shipping paper deficiencies identified in the previous inspection have been corrected As stated above, the Licensee's "Shipping Paper" information did not accurately reflect the information provided on the Bill of Lading. Fortunately, the official document, the Bill of Lading, contained the necessary information. But to avoid compliance problems the documents should contam the same information It is recommended that all documents associated with a shipment of the product matenal be consistent with one another. Additionally, 49 CFR 173.427(a)(6)(iv) states "Specific instructions for maintenance of exclusive use shipment controls shall be provided by the offeror to the earner Such instructions must be included with the shipping paper mformation" The Licensee does provide the earner with "Dnver Routing Instruction" and "Camers' Instructions", however, it is recommended that the information specified in 49 CFR 173 403, Exclusive Use be included m those dnver's instructions That being "The consignor and the earner must ensure that any loading or unloading is performed by personnel having radiological training and resources appropnate for safe handling ofthe consignment. The consignor must provide to the initial earner specific wntten instructions for maintenance of exclusive use shipment controls, including the vehicle survey requirement of §173 443(c) as apphcable, and include these instructions with the shipping paper information provided to the earner by the consignor " Page 5 of 6 s F \wp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Radiological Surveys When Class 7 radioactive matenals are shipped and the packages require Class 7 labels, the highest exposure rate measurement taken one meter from the surface of each package is required to determme which Radioactive Labels (White-I, Yellow-II or Yellow-IE) are to be applied The Licensee mdicated that the measurements are taken but the results were not documented The Licensee indicated that a line item could be added to the survey form indicatmg the measured 1-meter exposure rate It is recommended that this addition to the form be made and that the survey readings be documented there It is recogmzed that staffing is a challenge for the Licensee with respect to Radiation Techmcians The health physics management is encouraged to be vigilant in recruiting quality techmcians, m providing trainmg (initial, on-the-job, and continual), in mentonng, and in taking every opportumty to remforce radiological release limits and survey techmques The bnef observations of the staff conducting radiological surveys indicated that the radiation techmcians performed the basic radiological survey functions adequately and mamtamed the necessary documentation Routme facility contamination surveys are performed weekly It is recommended that this practice continue Source Inventory Because only two ofthe sources on the inventory list are actually used for checking survey instruments it is recommended that all extraneous sources be examined for then exempt status and eliminated from the source inventory and disposed m an appropnate manner Portable gauge sources are regulated imder a separate license and should continue to be controlled accordingly. The management of portable gauges will be evaluated when the Licensee is inspected for compliance with the conditions of the portable gauge license. Recommendations for the Next Inspection • Assess revisions to the operating procedures • Venfy the container survey form includes 1 -meter exposure rate measurements • Evaluate consistency in the product shipment file • Evaluate dnver instructions for exclusive use controls Recommendation to the DRC Director Although there were areas where process improvements could be made, nothing observed dunng the inspection appeared to directly violate license or regulatory requirements It is therefore recommended that no enforcement action be taken at this time Prepared By BoydM Imai (dy^l^U^ October 19,2012 Page 6 of 6 F \wpMnspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Inspection Keport ana Inspection Moilule MDMoa-sssoi Checklist INSPECTION REPORT Inspection Module. RADMOD-SSS-01 • Surveys/Shipping Papers/Sources Radioactive Matenal License No UT 1900479 Inspection Location: Energy Fuels Resources (USA), Blandmg, UT Inspection Date(s) September 19,2012 through September 20,2012 Inspector Boyd Imai, Utah Division of Radiation Control (DRC) Accompamed By Shiya Wang, Colorado Department of Public Health and Environment (CDPHE) Personnel Contacted: Daniel Hillsten, Tanner Holladay, Ronme Nieves, Justin Perkins, Chance Singer, Terry Slade, David Turk Inspection Summarv The inspection was opened on September 19,2012 with a meeting among D Hillsten, R Nieves, D Turk, S Wang and the inspector (S Wang had requested to accompany and observe a DRC compliance inspection ) Inspection Objectives were stated which included 1 Observe release surveys and preparation of product containers, equipment, conveyances (general releases and DOT compliance) 2. Assess completion of shipping papers and supporting documentation 3 Inventory Sources 4 Review release and facility surveys 5 Time permitting, look at a penmeter air sampling station Areas inspected included • Ore Truck Releases • Product Drum Preparation • Product Drum Shipping Papers • Container Releases • Source Inventory • Penmeter Air Sampling Stations (informational only) The inspector held a closeout meeting on September 20, 2012 with D Hillsten, R Nieves, T Slade, and D Turk of Energy Fuels Resources and S Wang ofthe State of Colorado to review the inspection activities, observations, and conclusions Findings No citable violations or deficiencies were observed dunng the inspection Two minor items were addressed dunng the inspection 1) an operational procedure needs Page 1 of 6 F \v^Mnspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc updating and 2) a release survey form needs to be modified to document a 1-meter exposure rate reading on product drums Inspection Items Ore Truck Releases Releasing empty ore tmcks from the facility is a vexing regulatory problem Compliance with the regulations is dependent upon the approach the facility chooses to take Procedures indicate that end dump trailers are released either for restncted or imrestncted use Two empty ore trucks were observed exiting the facility. The extenors of the conveyances were decontaminated and radiological surveys were taken of the extenors. Surveys of the intenors were not observed The conveyances were marked with the wordings "For Radioactive Matenal (Use) Only" and "Radioactive LSA" suggesting that the vehicles were being released under the provisions of 49 CFR 173 443(d) However, no shipping papers or documents were sent with the dnvers that would indicate that the vehicles were transporting a Class 7 radioactive matenal It was not clear whether the vehicles were released under restncted or unrestncted conditions If unrestncted, the trailers should not be marked "Radioactive LSA " Procedure titled End Dump Trailer Acceptance, Handling & Release, No PBL-9 needs review and updating, e g references to UN2910 with respect to "EMPTY" packages needs to be changed to UN2908 and attached regulations are outdated For restncted release, the Licensee must comply with all applicable requirements and not just selectively choose provisions that provide relief from certain restnctions, e g applying conditions found in 49 CFR 173.443(d) does not absolve the shipper from compliance with all other hazardous matenal shipping requirements such as shipping papers, markings, labels, etc. If the Licensee makes the determination that the released conveyance is not a Class 7 radioactive matenal transfer then 49 CFR 173 443(d) provisions cannot be applied and other release cntena must be applied, i e. more restnctive contamination release levels. Product Drum Preparation The product, UsOg "yellow cake" is packed m 55-gallon metal drums Drums used are certified Type A containers suitable for the shipment of Low Specific Activity (LSA-1) radioactive matenals A radiological survey was performed on each drum A contact dose rate survey and a contamination survey were performed on each drum The contamination survey was done with-a direct fiisk on each drum and a sample per load of drums had smear samples taken and analyzed for venfication purposes, all documented on the "Drum Contamination Survey" form Radioactive Yellow-H labels were not yet applied to the drums since it was only a partial load of drums that were being prepared at the time of the inspection Labels and markings were to be applied later m the preparation process Deficiencies It was noted that a 1-meter dose rate was not measured dunng the drum preparation process This measurement is necessary m determining which type of radioactive matenal label is Page 2 of 6 F \wp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc appropnate, i e Radioactive White-I, Radioactive Yellow-H, or Radioactive Yellow-IH as per 49 CFR 172 403(b) and (c) and 173 403, Transport Index Dunng the closeout meeting the Licensee indicated that the measurement is taken before the drums are loaded onto the transport vehicle Product Drum Shipping Papers From the previous inspection deficiencies were noted in the shipping paper information A sample of the shipping papers of recent shipments was examined for completeness It was venfied that the deficiencies identified m the pnor inspection were corrected The Licensee uses a Straight Bill of Lading as the shipping papers and m those reviewed no discrepancies were identified However, there was a document associated with the Straight Bill of Lading that did not precisely conespond with the information provided on the shipping paper Specifically, the document titled "Shipping Paper" did not identify the category of label applied to each package in the shipment as required in 49 CFR 172 203(d)(4) and it did not identify the chemical form as specified in 49 CFR 172 203(d)(2). Further, the proper shipping name did not include the "(LSA-1)" designation Apparently, this information is maintained on a spreadsheet for intemal purposes and is not utilized as the shipping paper prescnbed in 49 CFR 172 200 through 204 The dnver of the transport vehicle is provided with a "Dnver Routing Instruction" and "Camers' Instructions " Deficiencies The instructions provided to the dnvers should include the information specified in 49 CFR 173 403 Exclusive Use and required by 173 427(a)(6)(iv). Container Releases Three intermodal containers GFLU001035, GFLUOOl 180, and GFLUOOl 1801 were qualified for unrestncted release Release surveys of these containers are documented on "Energy Fuels Resources (USA) Inc , Equipment Survey for Unrestncted Release" forms No containers were being released as "EMPTY" UN2908 dunng the inspection Deficiencies None Source Inventory The Source Inventory list was checked against the sources in storage The Licensee indicated that only two of the sources on the list are used to check detection instruments, the remainder are not utilized for any purposes The Licensee provided documentation for source leak testing performed by Ronan Engineenng Co. Deficiencies The Source Inventory list did not identify four check sources in storage Bi-210 (0 053 |iCi), Page 3 of 6 ' F \wp\Inspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Cl-36 (0 0182 ^Ci), Pm-147 (0 096 ^iCi) , and C-14 (0 165 ^iCi) And there was one missing Th- 230 source no 5995-09 (on the list but not m storage) None of these sources are used Perimeter Air Sampling Stations As a courtesy, the Licensee escorted the inspector and S Wang to an air sampling site to see how a station is configured and assembled Samples are collected for particulate monitonng, radon momtonng, and gamma dose at each of five sampling locations Closeout Meeting The inspector held a closeout meeting with D Hillsten, R Nieves, T Slade, and D Turk of Energy Fuels Resources (USA) and S. Wang of CDPHE on September 20,2012 The observations descnbed above were summarized dunng the meeting Recommendations to the Licensee Operating Procedures It IS strongly recommended that operating procedures No PBL-2, Intermodal Container Acceptance, Handling & Release and No. PBL-9, End Dump Trailer Acceptance, Handling & Release be reviewed and updated There have been changes to the U S Department of Transportation (DOT) hazardous matenal transportation regulations since the procedures were first implemented and those changes need to be reflected m the procedures, including the attached DOT excerpts \ Of particular importance, in this regard, is the change to the contamination limits table found in 49 CFR 173 443 (Table 11 m the old regulations. Table 9 in the cunent regulations) Outwardly it appears that the limits were increased by a factor of 10 However, this is not the case Essentially, the limits are the same but a distinction is made between smearable/wipeable contamination (Table 11) and total removable contamination (Table 9) In Table 11a wiping efficiency (0 10) is factored in the table values, whereas, the shipper must adjust the survey results to convert smearable/wipeable contamination to total removable contamination before companng numbers with the Table 9 limits The shipper may use actual wipe efficiency or may use an assumed efficiency of 0 10 It IS a suggested that the procedural requirements for releasing conveyances and packagmgs as "EMPTY" be revised to conespond with the requirements specified in 49 CFR 173 428 including contamination and dose rate limits The UN number for empty packagmgs changed from UN 2910 to UN 2908 Although not prohibited, the notice "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive matenal, excepted package-empty packaging, UN 2908" is no longer required to accompany the shipment (formerly specified m 49 CFR 173 422, last appeanng in the 2003 edition) Although this notice is cunently applied to the outgoing empty containers and contains the four digit UN identification number for empty packagmgs, for bulk containers there is a size requirement for the UN 2908 marking (49 CFR 172 302 and 173 332) which the number on the notice does not conform As was discussed m the closeout meeting, caution is encouraged when releasing end dump trucks and other conveyances that transported the uramum ores, especially with "restncted" releases. Page 4 of 6 F \v\T)Mnspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Release cntena may depend upon the classification of the ore when it amved at the Licensee's facility A DOT regulated Class 7 radioactive matenal shipment upon amval may dictate what levels of radiological contamination and exposure rates are permissible for release The Licensee may have a number of options but must apply all the cntena that conespond to the option selected. For example, a shipper may apply the provisions found in 49 CFR 173 443(d) but cannot ignore the other radioactive matenal. Class 7 requirements found m 49 CFR Subchapter C. Unfortunately, when the DOT changed the defimtion of "radioactive matenal" from a concentration of2000 pCi/g of any radionuclide to radionuclide specific concentrations and consignment activity limits conesponding changes were not made to accommodate special provisions such as 49 CFR 173 443(d) Shippers are left to figure it out for themselves Full compliance is a difficult task that takes careful assessment and scrutiny. The Licensee indicated that the "lawyers" might need to get involved in this matter. The Licensee should use the term "exclusive use" cautiously The term has several meamngs and could impact compliance issues if not used in the proper context, especially if it is in reference to the provisions m 49 CFR 173 443(d) It is recommended that, because the regulations have changed since the procedures were first implemented, a careful review of the cunent regulations be performed and that the procedures be revised to capture all applicable options that the Licensee may choose to take in releasing conveyances It should be kept in mind that when doing the review there are multiple options for a "restncted release" each with separate and distinct radiological release and hazardous matenal shipping cntena Shipping Papers It appears that the shipping paper deficiencies identified m the previous inspection have been conected As stated above, the Licensee's "Shipping Paper" information did not accurately reflect the information provided on the Bill of Lading Fortunately, the official document, the Bill of Lading, contained the necessary information But to avoid compliance problems the documents should contain the same information It is recommended that all documents associated with a shipment of the product matenal be consistent with one another Additionally, 49 CFR 173 427(a)(6)(iv) states. "Specific instructions for maintenance of exclusive use shipment controls shall be provided by the offeror to the earner Such instructions must be included with the shipping paper information" The Licensee does provide the camer with "Dnver Routing Instruction" and "Camers' Instructions"; however, it is recommended that the information specified in 49 CFR 173 403, Exclusive Use be included in those dnver's instructions That being. "The consignor and the camer must ensure that any loading or unloading is performed by personnel having radiological training and resources appropnate for safe handling ofthe consignment The consignor must provide to the initial camer specific wntten instructions for maintenance of exclusive use shipment controls, including the vehicle survey requirement of §173 443(c) as applicable, and include these instructions with the shipping paper information provided to the camer by the consignor " ' Page 5 of 6 F \wpMnspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc Radiological Surveys When Class 7 radioactive matenals are shipped and the packages require Class 7 labels, the highest exposure rate measurement taken one meter from the surface of each package is required to determine which Radioactive Labels (White-I, Yellow-H or Yellow-IH) are to be applied The Licensee indicated that the measurements are taken but the results were not documented The Licensee indicated that a line item could be added to the survey form indicating the measured 1-meter exposure rate It is recommended that this addition to the form be made and that the survey readings be documented there It IS recognized that staffing is a challenge for the Licensee with respect to Radiation Techmcians The healjh physics management is encouraged to be vigilant in recruiting quality techmcians, in providing training (initial, on-the-job, and continual), in mentonng, and m taking every opportunity to reinforce radiological release limits and survey techniques The bnef observations of the staff conducting radiological surveys indicated that the radiation techmcians performed the basic radiological survey functions adequately and maintained the necessary documentation Routine facility contamination surveys are performed weekly It is recommended that this practice continue Source Inventory Because only two of the sources on the inventory list are actually used for checking survey instruments it is recommended that all extraneous sources be examined for their exempt status and eliminated from the source inventory and disposed in an appropnate manner Portable gauge sources are regulated under a separate license and should continue to be controlled accordingly The management of portable gauges will be evaluated when the Licensee IS inspected for compliance with the conditions of the portable gauge license Recommendations for the Next Inspection • Assess revisions to the operating procedures • Venfy the container survey form includes 1-meter exposure rate measurements • Evaluate consistency in the product shipment file • Evaluate dnver instructions for exclusive use controls Recommendation to the DRC Director Although there were areas where process improvements could be made, nothing observed dunng the inspection appeared to directly violate license or regulatory requirements It is therefore recommended that no enforcement action be taken at this time Prepared By BoydM Imai October 19,2012 Page 6 of 6 F \wpMnspections\Energy Fuel, Blandmg, UTMnspectionReportRevO doc UTAH DIVISION OF RADIATION CONTROL RADIATION PROTECTION INSPECTION MODULE RADMOD-SSS-01 SURVEYS/SHIPPING PAPERS/SOURCES DENISON MINES - WHITE MESA URANIUM MILL RADIOACTIVE MATERIAL LICENSE UTl900479 References Radioactive Matenal License UTl900479, License Renewal Application dated February 28, 2007, Radiation Protection Manual, Section 5,10CFR20, NRC Regulatory Guide 8 30, NRC Regulatory Guide 8.31, Utah Admimstrative Code R313-15 DATE ?//?//2^ OPENING MEETING MEETING MEMBERS ,,:;.^Tei^)K0i^ ^EmailAdcffim r-.''^ Bi^ra,w ^t}c\^ U \rad\COMMON\Uranium millsM le(2)UTl 900479 EnergyFuels Resources (Denison Mines) - White Mesa UMillMIP Inspection modules\2012Mnspection ModulesMiADMOD-SSS-02 rev 1 doc JV^^\>t<-nr- DISCUSSION 4p {e<2i-g XS^ <ft>^ Cu^V's^vcijM. (Qj^ysjuc^rwsg ^^•^ysg/y-v^ ^tAea-^g SAjov-v>gA4 3'^ ^ SITE STAFF COMMENTS ^ JrLjk^ /^f^.,^ U \rad\COMMON\Uranium millsM le(2)UTl900479 EnergyFuels Resources (Denison Mines) - White Mesa UMill\HP Inspection modules\2012Mnspection ModulesMlADMOD-SSS-02 rev 1 doc DATE ^/^// CLOSEOUT MEETING MEETDSTG MEMBERS NAME COMPANY CONTACT ESfFORMATION r I U \rad\COMMON\Uranium millsM le(2)UT1900479 EnergyFuels Resources (Denison Mines) - White Mesa UMillNHP Inspection modules\2012Mnspection Modules\RADMOD-SSS-02 rev 1 doc RELEASE SURVEYS for Product Drums, Intermodals and Ore Trucks Radiation Protection Manual Section 2 6 Equipment Release Surveys and 2 7 Product Shipment Surveys (Appendix E 2007 license renewal) 1. Observe the RSO or designee perform a release survey on the filled product drums Descnbe what they did Comments- 2. Observe the RSO or designee perform an unrestricted release survey on the Intermodals. Descnbe what they did Comments* . -L ^ \ r d T\ M Bo \ 3 Observe the RSO or designee perform a DOT Empty release survey on the Intermodals Descnbe what they did Comments. r 4 Observe the RSO or designee perform a release survey on an Ore Truck Descnbe what they did Comments i>'t " (^-s^J^v^cJ^^'^ I^^VY^-Z^VS- U-S^ <3>uJ-t^ ' ':CV--a<--oi_ S^-^^-r 5. Perform an independent Survey on each ofthe above items and descnbe how you did your survey and document the results Comments. (Product Drums) Comments (Unrestncted Intermodal) S<-CA-VAgv^3 U \rad\COMMON\Uranium millsM le(2)UTl900479 EnergyFuels Resources (Denison Mines) - White Mesa UMill\HP Inspection modules\2012Mnspection Modules\RADMOD-SSS-02 rev I doc Comments. (DOT Empty Intermodal) Comments: (Ore Truck) ^ . r 6. Was a survey (dose rate measurement) taken of the transport vehicle mtenor surfaces'^ Comments: ^ 7. How did the RSO or designee document their surveys'^ Comments* 8. Review the release surveys for the past year. Comments* Q^-^i^ju^y-JiJi ^£^v^ (fr^ /to^ ca^^-t-%>utAour3' -ft^'^^A'^ ^jj^g^^v^s- V^e-a,A-v^ SHIPPING PAPERS. LABELING AND PACKAGING "T^^/LJ S^fg.Ae_ DO"r3 9. Observe an Ore Tmck(s) Descnbe how they are labeled/placard. (49 CFR 172) Comments r-*:^^^^ ,V-ir- ^ ^ U \rad\COMMON\Uranium millsM le(2)UTl 900479 EnergyFuels Resources (Denison Miries) - White Mesa UMillMlP Inspection modules\2012Mnspection ModulesM^DMOD-SSS-02 rev 1 doc 10 Observe Yellowcake drums how are they labeled (49 CFR 172) Comments ^ ^uQ^ s-A^.^i/rKiLA^ Kjcj^ -a^u-g^iis- UU iue.J. 11. Observe Yellowcake shipment truck how is it placard. (49 CFR 172) Comments. C ' f) - 2^ice_ Date on shippmg paper Descnption (UN#, Proper shipping name, hazard class) Physical and/or Chemical form Radionuclide Activity Class Emergency phone # Exclusive shipment (Y/N) V Certified Comments: ^^r-<g|^c<.A.>v^ x^t^^^/^u^^o^aJ-^ /ry Y9 Cfp~ 2LO<:> Date on shippmg paper Descnption (UN#, Proper shipping name, hazard class) Physical and/or Chemical form U \rad\COMMON\Uranium millsM le(2)UTl 900479 EnergyFuels Resources (Denison Mines) - White Mesa UMillMIP Inspection modules\2012\Inspection ModulesMlADMOD-SSS-02 rev 1 doc Radionuclide Activity Class Emergency phone # Exclusive shipment (Y/N) Certified Comments* SOURCE CHECKS. INVENTORY AND SECURITY Radiation Protection Manual Section 3.0 Equipment/Calibration (Appendix E 2007 hcense renewal) 14 Observe the RSO or designee perform an Instrument Source Check Descnbe what they did Comments. 15. How do they document their source Inventory Comments. \ \AJLj::4..a;^| <^-AJOv/rc^ n"(^-z-:s>e> <j^Sf^6'09 4oo O^'/H 16. Where are the sources kept*^ Comments V 17. Any new source received*? Comments lO U \rad\COMMON\Uranium millsM le(2)UTl900479 EnergyFuels Resources (Denison Mines) - White Mesa UMill\HP Inspection modules\2012Mnspection ModulesMlADMOD-SSS-02 rev 1 doc Dnno f. r.f\t\ 18 Any source disposed of? Comments /J6 19. Were leak tests performed on the sources? Comments: /, g^3^(CA^ Sf>yCM^ C^^-g^CKT^ C2_7-^(l^Kr Release Limits Alpha (Umestncted and Product) Beta-Gamma (Unrestncted Only) Ore Trucks (Sole Use Transport) 49CFR173.443(d) Average Maximum Removable Average Maximum Intemal Surfaces Extemal Surfaces: 5,000 dpm//: 15,000 dpi 1,000 dpi 0.2 mr/hr 1.0 mr/hr or 15,000 dpm/cm^ 10 mR/hr 7 contact 2 mR/hr 7 at 1 meter 22,000 dpm/lOOcm^ a Removable 0 dpm/cm^ 49CFR173.443(d)(1) states* ^4 .sMrvey of the interior surfaces ofthe empty vehicle shows that the radiation dose rate at any pomt does not exceed 0.1 mSv per hour (10 mrem per hour) at the surface or 0 02 mSv per hour (2mrem per hour) at 1 m (3 feet) from the surface U \rad\COMMON\Uranium millsM le(2)UTl900479 EnergyFuels Resources (Denison Mines) - White Mesa UMillXHP Inspection modules\2012Mnspection Modules\RADMOD-SSS-02 rev 1 doc Interview with the Radiation Safety Tech.(s) 1 Name: ^ ft^rfc-iiA^ 2. Job Title* K-j MisAc ^ 3. How long have you been a Radiation Safety Tech? ^ u/i^^_ 4. How were/are you trained to be a Radiation Safety Tech? OJT 5. How long did your traimng lasf? ^ ^o^)b^ 6 Descnbe how you would survey product drums before they leave the restncted area? 7 What are the release limits for productdrums? /^t^e^ Ju^t^Z/ttjis^^^ ^ cJ^z/v^ 8 Descnbe how you would survey an Ore Truck out of the restncted area"? I^V*^ ^Tr^^ii. ^ />r .e-a.e,C^^^cgX (^fvc-^oC^ v^Nj^JiL^ l:'qtbJi=^ 9. What are the release limits for the Ore Truck? ^ /^>A|a-g "Z f JO^^^AP- —Agx-^^ » 10 Descnbe how you would perform an uamstficted release survey on an Intermodal Container*? 11. What are the release limits for an unrestncted release? ^ f<^^^^^M. 3 <s>^<:^ (5<5-<^o 12. Have them demonstrate how to^ou^^check an mstrume^ 13 How often are instruments source checked? 14 Where are the procedures kept that tell you how to perform a survey or source check an mstrumenf? K'^t^-W.oC^ ?T-A^-Ui>l^ \M.2Av^-^t — (l^P/^^ 15 Have you read those procedures'? V-e^ 16. If you have a question about your lop, how would you get it answered*? 9^^^^ A-^ R P K ^ Comments* \ - U \rad\COMMON\Uranium millsM le(2)UTI 900479 EnergyFuels Resources (Denison Mines) - White Mesa UMill\HP Inspection modules\20I2\Inspection Modules\RADMOD-SSS-02 rev 1 doc ProHnct Shipping Papers Page 1 of 1 STRAIGHT BILL OF LADING ORIGINAL-NOT NEGOTl^U RSB Logistics RSBI Shipper No Cam^ No, Date 9/10/2012 Be of Camef) (SCAQ on coStictim iMHvenreliipRieats, me letcefis G(X> nnist ^?pearii^^ othoTOiIss pnwkieCI ui^tem439. 1 From- ShfbDer ENERGY FUELS RESOURCES USA INC. To. Consianee CAMECO CORPORATION Street 6425 SOUTH HWY 191 Street HIGHWAY 10 Qtv BLAMDING State UT ZioCode B4S11 Citv BUND RIVER state ON. CANADA Zip Code 99352 24 hr Ernergency Contact tfiJ No CHEMtREC 1-8D0w|24-93eft Route NOTIFY UPON ARRIVAL DIANE FOtCO @705/356-1498 EXT 3285 Vehicle Number No ofunits& container ^pe HM Basic Description Proper St^ifwig Name, Hazani Oass. iCai >ti{iuat>on Number (UN WAj.fmidngGroup, pgr 172101,172^02,172203 Totaf Quantity OVeight, Votutne. Gedfons, ete) Weight (Sufatectto Coiiuvbun) fUCfE Charges (For CanTer XX na UN2»12, RAOIOACTiVE IMTERIAt, LOW Sf»EClFie ACnvlTY (L8A-1). iWZ^ CUSS 7 QROSS 42995 LBS 19516 K6S UftANIUM ORE CONCENTRATE AS URANIUM OXIPE U-308 PHYSICAL FORM: SOUD CHEMiCALFQRM: OXB»E ACtlVrrY: 46bq {.19 Cl) PER DRUM iJBgLS AH>UEd: RADldACtfve YELL^r TRANSPORT fNPEX; 0.4 PER^RUM PLACA3WS.1tM10ACTIVE mis VEHICLE IS ASStGMED FOR EXCHJSJVE USE OF ENERGY FUELS RESOURCESt USA INC. UNDER PROVISIOHS OF 49 CFR OO NOT LOAD OTHER FREIGHT IHTHiS VEHICLE. TRANSFER EN ROUTEtt^ BI^AK SEAL TRUCK SEAL NUM&ER: PLACARDS TENDERED- YES: X NOO Npt©-(^)\Wl?I9t^eraleISdepefldflraonra6Je shipper;arfrequkedtQSatespecHlc^flyon a*4l)ng 9m s3E4«d or iia(:lsied of fts |M|ieily a hereby ispeciflcaBy alBiEd iqr Sie il^^ 1 hflreby dedare Sist 4ie contenis of IM^ . eapdprnemmftiByuirf^aaicptclydes^^ dxne fay tie ]Xtiper dt^fbig nanta and are cMEcned, packaged, moiked, avil 1siMled/4ibcndL Old aS lespetit* appfteeUe Hi^tenraQpiu? andijatfonaf govefumeirial laspdationa. ON BEHALF OF SUFFER COO AtntS COS) Fge. couECTi e {2)VmOT'aieSp^EcsiU»lsi«{inn@anG^ped^«1mVESoncaihe«t^^ BsbH^f <r oecterg s yisKm, to ccntei^lbbffiy Et)tf to lk?d^ pioyCEtons. S89 NKR. Ksm 172. ^CamafiSesmfilitv^^eelalciaiSt^KittsmvsSiitS^ b» so marked and ps«9csged seta ensure eaDitrsnspartaStin. See Section 2(e} of ten 36o Bni'of Isttig. Fre^ and S(Btefl)snt5 ol Chais» and SecS^ iBnns and ecndUcns fcrs fistof sud> arddoa. 1 hflreby dedare Sist 4ie contenis of IM^ . eapdprnemmftiByuirf^aaicptclydes^^ dxne fay tie ]Xtiper dt^fbig nanta and are cMEcned, packaged, moiked, avil 1siMled/4ibcndL Old aS lespetit* appfteeUe Hi^tenraQpiu? andijatfonaf govefumeirial laspdationa. ON BEHALF OF SUFFER sl0n thalofiaittiB ckflunni^ Tb^frtBttJB#nrfw^fitdrfiiwjirfff^>WiyflflBt^M(fMwl]wp'wt<rf TOTAL CHARGES « FREIGHT CHARGED acotudMnbiatd b tniKibB {2)VmOT'aieSp^EcsiU»lsi«{inn@anG^ped^«1mVESoncaihe«t^^ BsbH^f <r oecterg s yisKm, to ccntei^lbbffiy Et)tf to lk?d^ pioyCEtons. S89 NKR. Ksm 172. ^CamafiSesmfilitv^^eelalciaiSt^KittsmvsSiitS^ b» so marked and ps«9csged seta ensure eaDitrsnspartaStin. See Section 2(e} of ten 36o Bni'of Isttig. Fre^ and S(Btefl)snt5 ol Chais» and SecS^ iBnns and ecndUcns fcrs fistof sud> arddoa. TOTAL CHARGES « FREIGHT CHARGED acotudMnbiatd b tniKibB REMITCOD TO /UIIDRESS RBCBVEO miieAloimdas^SceSamaadisiBanfSieamfheiaSBillv^ exceptasnoWCconlxnlssidcanBtaafcnnlcnbafpsdiagesu^^ and dastMdasln<8iaM abawwWch said canier^iiard im^inub>,t<hM«iM>Mi<iiH>wrJiiiiti>.ih«rr^^ Itisiiuti^^.^n»dastoead)tanferirf«Hdr.aoy(A«ailp^^ propel^ lhataigytaaice to liapartannadlagacindaf doll tojut^^ St^iperhMel^cariahbBkdlwteteBsrwftaaflwtaftiateiinsaBduiiiUt^ stilipeFandaceapaBd for Mmsa); and lis assigns. SHIPPER. ENERGY FUELS RESOURCES USA INC CARRipRr^ LOGISTICS, INC, TRANSPORT #0612-730 PER]^^{$~^^(9f DATE rAiT-io-t2. DATE r WorkCentre 7346 Transmi ss i on Re port G3 I D 435 678 2224 Date/Time 09/14/2012 05 58AM Page 1 (Last Page) Local Name Denison Mines Logo White Mesa Mill BlancJing Ut Document has been sent Document Size 8 5X11"SEP Energy Fuels Resources (USA) Inc. 642JS HigtR«ayl91 POBox809 Bland]iig,UT84Sll Tel 435 678 2221 FAX. 435.678 2224 Facsimile Transmittal Pu Compiw C,^ nomber ) r^cS" rZZ% Fnm. Ti^lT^I, PaKalofi Z- ^^<:.•(• Cu$(.a,.-5 Weft Total Pages Scanned 2 Total Pages Sent No Doc Remote Station Start Time Duration Pages Contents 1725 7053561223 5 56AM Note RE Resend MB PG Pol I ing RB SA Send Again EN Send to MaiIbox Relay Broadcast Engaged BC Broadcas t RS Re I ay Send AS Auto Send MP MuIti Polling BF Box Fax Forward TM Terminated RV CP Remote Service CompIe ted Fuels Resources (USA) Inc, 6425 S Highway 191, PO Box 809 Blandmg, UT 84511 Tel 435-678-2221 FAX 435-678-2224 Facsimile Transmittal To: -TN. ^ . Date. Fax Company: C^^^^^r^ number: From: "l^cju^^lTU 1/ Page 1 of: Re: ?,0L Lv- B^^^ U4 U us DEPARTMENT OF COMMERCE-EcwmMsarulSlaisticsAfcninis!^ CENSUS BUREAU - BUREAU OF EXPORT ADMIMlSTRATlON FORM7525"V(7-I8>2003) SHiPPER*S KCPOBT DECLARATION QMB NO 0307^152 ta. U S PFUNdPJM. PARTY IN (H7ERES7 (U^rKCoi^ name snd akbsss) ENERGY FUELS RESOURCES USA INC 6425 SOUTH HWY 191 BUNDING, UT b. USPPI'S BN ORS) OR iO MO 84-1372857 ZIP CODE 84511 C PARTIES TO TRAMSACTKHii @R^led 4a.(A.T|MATEGON8)aNEE «kmplete name and adifressi CAMECO CORPORATION, ONE ELDORADO ROAD BLIND RIVER, ONTARIO. CANADA IfcfNTERMECaATECONSfeNEE (Comply name ml adtkess} Sa. FORWARDING AGENT (Cmjplete name tmd atkfrgis) RSB LOGISTIC SERVICES. INC 2425 SOUTH 4TH STREET PADUCAH,Ky 42003 ll. FORWARDING AGE^f^S EiN (IRS) NO 54-1243432 ZOATE(»=eXK)RTAT!ON 10 SEPTEMBER 2012 3. TRANSPORTATON REFERENCE WO 0612-730 0. POINT (STAH) OF ORIGIN FTZNO UT 7. COUNTRy OF ULTIMATE OESmKfm CANADA B.LOADING PIER (Vasselonly} B^vEnmt^TmmmmiitfSm^ TRUCK f*. CPSmm lOBfTIFtCATtON CODE RSBI iS. SHIPMENT REFERENCE NO 0612-730 10. E}ff>QRnNQ CARRIER RSB LOGISTIC 11. PORT (^EXPORT a^ULTSTE MARIE tBi^rrRY NUMBER 17, HAZARDOUS MATERIALS Wives DNO ia. IN BONO CODE ift, ROUTED EXPORT ITWJSACnON •YTO 12. PORT OFmOADtNG (Vissseiandaira^ 13. C0NTAlNEffi2El><V«s$e/«>$^ •Y«8 DNO 20. SCHEDULE B DESCRIPTION OF COMMODmES (tJsetxjkmsZZ^) DIP orM (21) SCHSHJLEBNUKffiER (WANTTTV-SCtOlA£BlMlT($) SKIPPiNQ WEIGHT ttStan VffMPROOUCTMftKfV VEHICLETITIE NUMBER VALUE (U.8do«af£, 2844102010 URANIUM ORE CONCENTRATE 43 DRUMS LOT 88 17932 KGS 19516 KGS $2,045,833 00 27. UCENSE NOAIOEKSE EXCEPTK»4 SVMBOiAUTHORiZA'nON XSOU8798 39, Duly (smtbetteffleei or«iQ)loy0e KATHRYN WALTERS 28. ECCN {Wlm require^ 90M fceiMythataiiaailemeft&roaaeattii and vmeistsnd <tw instiuctons lh» mtppM'* EXpMt deeUiral sala, may oe impaaed fat maieng fstae souse fi^SAlO] , actask>!WuSitigaguiito(e}^conMaitd I customs putpo8e$ MomtatmcorOatwaJm^mebuoemtlcottectaniiViailitaverexl afon erf (hia ifocuimitf. 9^ forth in^ N$«f*«eCw«y nu Owi Of ftmKfutoit ^atemsnts herein, MM to pfovida Ifte reqw anexpoAaiioflOSUSC Seei.3as;22U9C sea407 lausc Sec CUSTOWERACCREP 10 SEPTEMBER 2012 Tele{rfiatta Na dlmSata Ama Code) 270-444-6004 ««n«M«M- aqDpeftBgiMtOdClaia^CeranytucMSsaf dMunM«« HtotM^ iiMaM «>iett W Jrsm put«» «^ the Setntaiy detntes 9t>i $uch «iaiRpew wsuU be cot^^ i)tfen« ^tmt (TH* 19. Ctiapter 9. SMMn 301 (d!>. ifttl^ OSce at Eiqport EiAi<a)inent Setrice M, AUTHEHTfCATKW ^Mto »HJ{/;/KO E-fnail address pa<Jucah@rsbloglsttc com TM$ fomt fsvsf be ptstfed by private parties prcnildedl it conlotms to the official foim Far sale by the StqperintendEnt erf Dooimeite, ^emtn«nt P^StS^a^ce Wfe£tegt(« QC20402,a(iaics3!Cuaem-s0i£tftetBl{e<3QTS.Th«^e«%sftW^to1«ftitifteS^^ Etedinattet^ is ^t^klble from d» U.S, Coisus Bufeau, Washing OC 20233 I ftevi^nu^ Canada Customs and Excise ^AN/y^A CUSTOMS INVOICE 1 Ofl 1. Vendor (Name and Addiess) ENERGY FUELS RESOURCES USA INC. 6«S SOUTH HWr IBI BRANDING. W 84511 2. Date of Oirect Shipment to Canada SEPTQHBQ21D,2012 3. Other References (Include Purchaser's Order Na) LOT da 4. Cims^tiBs tNatnB.and Addrssi^ CAMECO CORPORATION ONE ELDORADO ROAD BLIND RtVER, ON, CANADA 5 Purcfiaa«fs Name and Address oiherthan Coiafi^iefe^ 4. Cims^tiBs tNatnB.and Addrssi^ CAMECO CORPORATION ONE ELDORADO ROAD BLIND RtVER, ON, CANADA & ^ouittry of Tf aishqsnent NONE 4. Cims^tiBs tNatnB.and Addrssi^ CAMECO CORPORATION ONE ELDORADO ROAD BLIND RtVER, ON, CANADA 7 Cdiffllryiif Orl^of Coj»ds U.SA T.ltansportaBon GtveModetrndnaceiiiDirei^SiilPBienttoCanaite I^LOGlSTiClNC. ROAD TRANSPORT CROSSING AT SAULTSfE.MAl%IE»MI a CondHions of Sale and Terns of Payment (ije.Sai«^Con^ini»nt3hipiii«nt.tjeasea Ooods^etc) FOR PROCESSING AND RETURN T.ltansportaBon GtveModetrndnaceiiiDirei^SiilPBienttoCanaite I^LOGlSTiClNC. ROAD TRANSPORT CROSSING AT SAULTSfE.MAl%IE»MI 10 Currency of SutUuiri»ut USD 11.Ng<rf 4i 12.gtW6»H;att<w<rfCwampdMg9tWnd<fyaclca9B^Msilw Descffptlon and CluHBCteitetles,Grade, 4luOTtit^ DRUMS URANIUM ORE CONCaiTRATi NET WEIGIfT CONCENTRATE: 39533 L^ 17932 KGS Cameco is importer of Reoortland e taking care of all Charges witti regards to Customs aaarance Near North is the broker on behalf of Cameco. PatriGlcPlourtle Near Nof^ Custonv Brewers Inc 1855JLasaHefilvd Sudbury, ON, P3A 2A3, Canada rm 1-705-560-24G0 Fax# 1-705-560-6928 Emaifc. patrtckp@neamorthaistoms com 19. Quantify (StatoUnit) 39533 LBS Setting Prtee 14. Price UnH $51.75A3 19w Totaf $24I45,B33.^< 10 if4ny«f fields 1t» 17 are kieluded on on ^tteehed commercial Inveloe, cheek box D CommencNi Invoice No. , 10 Total Vlfef^ Net 39533 LBS Qrass 42995 LBS 17 Invoice Total $?^5,833,^Q 19 Bqiotttf*ifr Niank^^^ Ad«fi«&s ^ other UuA Vehdv) SAMEAS^SNDOR 20 Originator (H»ne and Adifiess)^ David Turk 21 DepaftmenttaRtdingOfapplteabto) 22.lffteMs23to2SaronotappBcafiifa,<Aw;kgasbox 23 irincbufedlhfield 17 Indicflte amount (I) TramportaUon daarqes, expBtisBs, and insurance from the place ^ dir^aJiqunent to Canada incwred afler ^portidfon Itito Canat^ $ Qi^EjqpigyitpacMRS 24w tf not Ineftided on field 17 indicafB amowt: OfTraasportBiton tiierges, expenses and {nsursice ty the place of direct shipment taCanada (d) Amounts for commisskHe other than faiq^ng commfsslofls fH0Ejq}ortPa<3dtt<f 25. <3ieck ^ appflcahfe} 0) Royalty payments or subsequent proceeds are panf or payalile Iqr 0»f»ncliaser (G) Tbe laifchaser has^ suy^iied goodsisr services for use In the |vo(faictfon of these goods www.rsbloglsticcom RSB LOGISTIC INC Phone 306-242-8300 219 Cardinal Crescent TolI-Fr«e 800-667-3934 Saskatoon, SK S7L7K8 Fax 306-242-2311 Canada September 05,2012 Robert Caldwell, Chief Fuel Cycle Security and Transportation Branch U.S Nuclear Regulatory Commission Office of Nuclear Security and Incident Response Division of Security Policy RSB Reference No.. 0612-730F ADVANCE NOTIFICATION OF EXPORT SHIPMENT In accordance with the requirements for implementation of the Convention on the Physical Protection of Nuclear Material, we are submitting the following 1) Shipper. Receiver and Carner Energy Fuels Resouces (USA) Inc 435-678-2221 Formerly Denison Mines Corporation 6425 South Highway 191 White Mesa Mill Blanding, UT Cameco Corporation 705-356-1496 Highway 17 West Blind River, ON, Canada POR 1B0 RSB LOGISTIC INC. 306-242-8300 219 Cardinal Cr Saskatoon, SK S7L 7K8 2) Physical Descnption This shipment will consist of 43 Drums of Uranium Ore Concentrate (U-30B) in 1 x 53' trailer The total weight of the shipment is 17,932 kg of U-308 Lot 88 SASKATOON, SK PADUCAH, KY Robert Caldwell September 05, 2012 Page 2 3) Transportation and Route Schedule The surface transportation from Blanding, UTto Blind River, ON will be the responsibility of RSB LOGISTIC INC. Export from the United States will occur at Sault Ste Marie, ON on or about September 14,2012. Shipment Routing Departs Blanding, UT September 10,2012 Arrives Sault Ste Mane, ON September 14,2012 Arrives Blind River, ON September 15, 2012 4) Export License: NRC License No XSOU8798 This shipment will be protected dunng transport in accordance with Annex 1 to the Convention on Physical Protection of Nuclear Materials Sincerely, Helge Struthers Int'i Transportation Specialist RSB LOGISTIC SERVICES INC SASECATOON, SK PADUCAH, KY \ ss LOGISTIC www.rsbIogistic.com RSB LOGISTIC INC 219 Cardmal Crescent Saskatoon, SK S7L 7K8 Canada Phone Toll-Free Fax 306-242-8300 800-667-3934 306-242-2311 ATTACHMENT 1 RE Energy Fuels Resources (USA) Inc - Lot # 88 Certification of Export Filing: THESE COMMODITIES, TECHNOLOGY OR SOFTWARE WERE EXPORTED FROM THE UNITED STATES IN ACCORDANCE WITH THE EXPORT ADMINISTRATION REGULATIONS DIVERSION CONTRARY TO U S. LAW PROHIBrrED. NO SED REQUIRED-AES-132637752-RFI162362. AES-ITN-X20120906034794 SASKATOON, SK PADUCAH, KY Denison Mines (USA) Corp. White Mesa Mill Notice of Product Shipment Date lO-Sep-12 Product: Lot No.: 88 Trans. No. 638 Customer P.O. or Order Number: U3O8 VA" AMV' Other X Gross Weight Tare Weight Net Weight NetMafl Weight (lb) ' Weight as U3O8 (lb ) Weight as U-Nat (lb ) " Net Mat'l Weight (kg) [ Weight as UjOg (kg) Weight as U-Nat (kg) N/A Destination: Cameco Corporation 328 Eldorado Road Blind River, ON POR IBO Canada 77,860 34,380 43,480 40,844 0 39,533 0 33,524 0 18,526 0 17,932 0 15,206 0 Shipper Energy Fuels Resources via RSB Logistics Shipment No YC-88 Shippers Paper Shipper Energy Fuels Resources HOLDINGS CORP 6426 SOUTH HIGHWAY 191. P O BOX 809 BLANDING. UT 84512 CONSIGNEE Cameco Corporation 328 Eldorado Road Blind River, ON POR 1 BO Canada DELIVERING CARRIER DATE CONTRACT NO LOT NO 9/10/2012 97-538 YC-88 RSB Logistics TRACTOR NO TRAILER NO SEAL NO 53809 253128 7804 Seal# 007804 PARTIAL LOT COMPLETE LOT GROSS WEIGHT (lbs / kg) XXX 77,860 35,317 Matenal Shipping Description EXPULSIVE USE SHIPMENT Radioactive Matenal, low specific activity Activity 8 GBq - Transport Index 0 4 Class7UN2912 43 Drums of Natural Uranium (U-Nat) Solid Form Received in good condition, except as noted Emergency Contact Phone Number: Chemtrec 1-800-424-9300 Account # 223794 Signature of Driver Received By This IS to certif ly that the above named materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation Date Signature urces^€ Energy Fuels Resourcesflepresentative Date Denison iVitnes Corp 6425 S Highway 191, PO Box 809 Blandmg, UT 84511 USA Tel 435S78-2221 Fax 435 678-2224 wvm denisonmlnes com SHIPMENT SURVEY CONTRACT NO TRACTOR NO LOT NO TRUCK CARRIER TRAILER NO ili. MODEL NO SERIAL NO CALIBRATION EFFICIENCY FACTOR MDA ALPHA SURVEY INSTRUMENTS TOTAL MODEL NO SERIAL NO CALIBRATION EFFICIENCY FACTOR ALLOWABLE LIMITS (FIXED) 5,000 PPM AVG 15.000 PPM MAX (REMOVABLE) 1,000 PPM REMOVABLE 10 feu l-L^ ikl 1 0 SURFACE AREA OF PROBE 100 cm^ X EFFICIENCY OF INSTRUMENT (%) = FACTOR 100 (EFFICIENCY/1 OOcm^) Factor X counts/minute = Pisintegrations/minute/IOOcm' INSTRUMENT NO SERIAL NO CALIBRATION TRAILER SURFACE SIX FEET DISTANCE DRIVERS SEAT SLEEPER 3 GAMMA SURVEY (49 CFR 173 441 (b) (1)) MEASURED IN MILLIREMS/ HOUR 9 - Xtj\/^-;z7 (MR/HR) 200 MR/HR ALLOWABLE 10 MR/HR ALLOWABLE 2 MR/HR ALLOWABLE 2 MR/HR ALLOWABLE ALL DRUMS WERE INSPECTED PRIOR TO LOADING ALL DRUMS WERE TIGHTLY SEALED NONE LEAKED AND THERE WAS NO LOOSE MATERIAL IN THE VEHICLE INSPECTOR SIGNATURE DATE ^-l£?-(Z^ lype Of Shipment Vg^uQU fxi^tcg^ Lot# ^2 Drum # Total Alpha dpm/100 cm^ Top Sides Removable Alpha dpm/100 cm^ Top Sides p/Y Average mrem/hr 1 2 t^X.CL. M 1 2 VLV (. 3 be 4 4 5 i-B ^ to (. 6 ^gl/^ 7 8 //'^ 9 10 11 12 13 14 \ / \ \ / 15 16 17 18 19 20 1 21 22 23 24 •\ N / 25 '3 If total Alpha is greater than or equal to 1,000 dpm/100 cm^ a removable smear is required Alpha Meter Model # SN# Removable Alpha Cai Date \') Model # SN# Beta/Gamma Meter 1_ Model # SN# Check Date )? pg^l Cal Date 10 Th 230 @ 33.000 dpm dpm Average ^ ooo Efficiency \gr \ Bkg ^0 Check Date i/} Aoci \^ Th 230 @ 33,000 dpm Efficiency XS- ^^^o Bkg iiA\ . Cal Date IMJV^LT 1^^ Check Date 7 T)eC. Cs137 SN#2 Reading 1. M.r| wt^ Bkg c) c H Mr| tV\i^ Drum 27 28 29 30 31 32 33 dprn/100 cm^ Top Sides ^^^^ RemovaPe Alpha dpm/100 cm^ "op Sides Pages |3/Y i/era mrem/hr 3Z 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 Comnnents: DOE/NRG FORM 741 (6-2011) Previous editions are obsolete MANDATORY DATA COLLECTION AUTHORIZED BY 10 CFR 30 40 60 70 72 74 75 150 Public Laws 83-703 93-438 95-91 US DEPARTMENT OF ENERGY AND US NUCLEAR REGULATORY COMMISSION NUCLEAR iVIATERIAL TRANSACTION REPORT APPROVED BY OMB NO 3150-0003 EXPIRES 05/31/2014 Estimated burdenper response to comply with this mandatory collecbon request 1 hour and 15 minutes This information IS required for IAEA accounting reports that show changes in inventory of nuclear matenals Send comments regarding burden estimate to the Information Services Branch (T-5 F53), U S Nuclear Regulatory Commission Washington DC 20555-0001, or by internet e-mail to infocollects resource@nrc gov, and to the Desk Officer Office of Information and Regulatory Affairs NEOB-10202 (3150-0003), Office of Management and Budget Washington, DC 20503 If a means used to impose an information collection does not display a currently valid OMB control number fhe NRC may not conduct or sponsor and a person ts not required to respond to, the mformation collection 1 SHippEirsRis 2 RECEIVER SRIS 3 TRANSACnON NO 4 CORRECTION NO 5 PROCeSSINO CODE « ACTION CODE 7 DOCUMENTATION (Only If documm* ii dntllM SECRET) XRA RDLA 00638 I SHIPPER A L SHIPPER A PAGES COPY COPIES SERIES Energy Fuels Resources (USA) Inc 6425 South Hwy 191 Blanding, Utah 84511 cATTEHTioM David Turlc d TELEPHONE (435)678-2221 10 NO OF DATA UNES 01 Cameco Corporation Eldorado Road Blind River, Ontario, Canada 12jt SHIPPED FOR ACCOUNT OF c ATTENTION- d TELEPHONE 11 NATURE OF TRANSACTION 13J SHIPPED TO ACCOUMf OF 14 TRANSFER AUTHORITY-CONTRACT NM DRAFT OR ORDER NUMBER 15 EXPORT OR IMPORT TRANSFERS UCENSE NO XSOU8798 NO DISTRIBUTION OF COPIES XRA NMMSS RDLA 16 MATERIAL TYPE ANO DESCRIPTION 43 Drums of Natural Uranium (Split US and Canadian Obligated matenal) 01 32 193 OBLIGATED ISOTOPE WEIGHT For Enriched Uranhan Orly 22. ACTION OATE 09 10 2012 23a MISCELLANEOUS b CONCISE NOTE ATTACHED • REPORTABLE? | | YES ^ NO b SMPPEirS CORRECTION d RECEIVER-S MEASUREMENT : RECEIVERS CORRECTION 24 TOTAL GROSS WEIGHT 19,516 25 TOTAL VOLUME (Wkste Tmatm Only) BACK REFERENCE NUMBER TYPE OF INV CHANGE MATE RIAL TYPE COMP/ FACIUTY CODE KEY MEAS POINT OMP METHOD GROSS WEIGHT ELEMENT UUITOF ERROR ISOTOPE UMIT OF ERROR 01 YC Lot 88 43 N 032 15,206 26s SHIPPERS DATA S/GNATURE OF AUTHORIZED OFFICIAL AND DATE SIGNED 4» 4^ 4» 27s RECEIVER'S DATA SIGNATURE OF AUTHORIZED OFFICIAL AND OATE SIGNED WARNING FALSE STATEMENTS IN THIS CERTIFICATE MAY BE SUBJECT TO CIVIL AND/OR CRIMINAL PENALTIES NRC REGULATIONS REQUIRE THAT SUBMISSIONS TO THE NRC BE COMPLETE AND ACCURATE IN ALL MATERIAL RESPECTS 18 U S C SECTION 1001 MAKES IT A CRIMINAL OFFENSE TO MAKE A WILLFULLY FALSE STATEMENT OR REPRESENTATION TO ANY DEPARTMENT OR AGENCY OF THE UNITED STATES AS TO ANY MATTER WITHIN ITS JURISDICTION DOE/NRC FORM 741 (6-2011) OOE/NRC FORM 741 (6-2011) Previous editions are obsolete MANDATORY DATA COLLECTION AUTHORIZED BY 10 CFR 30 40 50 70 72 74 75 150 Public Laws 83-703 93-438 95-91 US DEPARTMENT OF ENERGY ANO U S NUCLEAR REGULATORY COMMISSION NUCLEAR MATERIAL TRANSACTION REPORT APPROVED BY OMB NO 3150-0003 EXPIRES 05/31/2014 Estimated burden per response to comply with this mandatory collecbon request 1 hour and 15 minutes This information IS required for IAEA accounting reports that show changes in inventory of nuclear matenals Send comments regardinq burden estimate to the Infonnation Services Branch (T-5 F53), U S Nuclear Regulatoiy Commission, Washington, DC 20555-0001, or by internet e-mail to infocollects resource@nrc gov, and to the Desk (jfficer Office of Information and Regulatory Affairs, NEOB-10202, (3150-0003), OfRce of Management and Budget Washington, DC 20503 If a means used to impose an informabon collection does not display a currently valid OMB control number, the NRC may not conduct or sponsor, and a person is not required to respond to, the information collecbon 1 SHIPPER'S RIS 2 RECEIVER'S RIS 9 TRANSACTKIN NO 4 CORRECTION NO 5 PROCESSING CODE 6 ACTION CODE 7 DOCUMENTATION (Only »dacunKnll.diwnW SECRET) XRA XRA 638 iM PASES COPY COPIES SERIES »a NAME ANO ADDRESS Energy Fuels Resources (USA) Inc 6425 South Hwy 191 Blandmg, Utah 84511 0 ATTENTION David Turk d TELEPHONE (435) 678-2221 10 NO OF DATA UNES 01 12a SHIPPED FOR ACCOUNT OF c ATTENTION d TELEPHONE 11 NATURE OF TRANSACTION 13J SHIPPED TO ACCOUNT OF 14 TRANSFER AUTHORITY CONTRACT NM DRAFT OR ORDER NUMBER 15 EXPORTORIMPORTTRANSFERS UCENSE NO Gen Lie XRA NMMSS DISTRIBUTION OF COPIES 16 MATERIAL TYPE AND DESCRIPTION 43 Drums of Natural Uranium (U S matenal) ELEMENT WEIGHT OBLIGATED ISOTOPE WEIGHT For Eitficbed Uianiun Only 22. ACTION OATE 23a MISCELLANEOUS b CONCISE NOTE ATTACHED • UK REPORTABLE? | [ YES | NO b SHIPPERS CORRECTION 09 04 2012 d RECEIVERS MEASUREMENT • RECEIVERS CORRECTION 24. TOTAL GROSS WEIGHT 19,516 25 TOTAL VOLUME OMstt Tnm/an Only) BACK REFERENCE NUMBER TYPE OF INV CHANGE MATE RIAL TYPE COMP/ FACILITY CODE KEY MEAS POINT OMP METHOD GROSS WEIGHT ELEMENT UMrroF ERROR ISOTOPE UMrroF ERROR 26s SHIPPER'S DATA SIGNATURE OF AUTHORIZED OFFICIAL ANO DATE SIGNED 4^ 4» 4^ 27s RECEIVER'S DATA SIGNATURE OF AUTHORIZED OFFICIAL AND DATE SIGNED 01 34 YC Lot 43 N 32 15,013 WARNING FALSE STATEMENTS IN THIS CERTIFICATE MAY BE SUBJECT TO CIVIL AND/OR CRIMINAL PENALTIES NRC REGULATIONS REQUIRE THAT SUBMISSIONS TO THE NRC BE COMPLETE AND ACCURATE IN ALL MATERIAL RESPECTS 18 U S C SECTION 1001 MAKES IT A CRIMINAL OFFENSE TO MAKE A WILLFULLY FALSE STATEMENT OR REPRESENTATION TO ANY DEPARTMENT OR AGENCY OF THE UNITED STATES AS TO ANY MATTER WITHIN ITS JURISDICTION DOE/NRC FORM 741 (6-2011) WorkCentre 7346 Transm i ss o n Re port G3 I D 435 678 2224. Date/T i nn« 09/10/2012 06 57AM Page 1 (Last Page) Local Name Denison Mines Logo White Mesa Mi I I Blanding Ut Document has been sent Document Size 8 5X11"SEF Total Pages Scanned 2 Total Pages Sent No Doc Remote Station Start Time Duration Pages Con tents 1307 3019031998 Note RE Resend MB PG Po I I I ng RB SA Send Again EN Send to Ma i I box Relay Broadcast Engaged BC Broadcast RS Re I ay Send AS Auto Send MP MuIti Polling BF Box Fax Forward TM Terminated RV CP Remote Service CompI e t ed Enm'Qu Fuels Rsources IU5R) Inc. mmmm 6425 S Highway 191 PO Box809 Blanding, Ut 84511 USA YC Lot 88 Tel 435-678-2221 Fax 435-678-2224 www energyfuels com 96 79 % U3O8 Est grade Forgin Oper Production 82 08 %U Gross Gross Net lbs Net Kg Net lbs Net Kg Obligated U Initial Dates Tare lbs Tare Kg lbs Kg Net lbs Net Kg U3O8 U3O8 U U Kg by Drum OK 28-Aug 1 50 23 1,000 454 950 431 920 417 780 354 CK 2 50 23 1,000 454 950 431 920 417 780 354 OK 3 50 23 1,000 454 950 431 920 417 780 354 CK 4 50 23 1,000 454 950 431 920 417 780 354 JB 5 50 23 1,000 454 950 431 920 417 780 354 JB 6 50 23 1.000 454 950 431 920 417 780 354 JB 7 50 23 1,000 454 950 431 920 417 780 354 JB 8 50 23 1,000 454 950 431 920 417 780 354 JB 9 50 23 1,000 454 950 431 920 417 780 354 CK 29-Aug 10 50 23 1,000 454 950 431 920 417 780 354 CK 11 50 23 1,000 454 950 431 920 417 780 354 CK 12 50 23 1,000 454 950 431 920 417 780 354 JB 13 50 23 999 453 949 430 919 416 779 353 JB 14 50 23 1,000 454 950 431 920 417 780 354 JB 15 50 23 1,000 454 950 431 920 417 780 354 JS 30-Aug 16 50 23 1,000 454 950 431 920 417 780 354 JS 17 50 23 1,000 454 950 431 920 417 780 354 JS 18 50 23 999 453 949 430 919 416 779 353 JS 19 50 23 1,000 454 950 431 920 417 780 354 JS 20 50 23 999 453 949 430 919 416 779 353 JS 21 50 23 1,001 454 951 431 920 417 781 354 JS 22 50 23 997 452 947 429 917 415 777 352 JS 23 50 23 1,001 454 951 431 920 417 781 354 CK 24 50 23 1,000 454 950 431 920 417 780 354 CK 25 50 23 1,000 454 950 431 920 417 780 354 CK 26 50 23 1,000 454 950 431 920 417 780 354 CK 27 50 23 1,000 454 950 431 920 417 780 354 CK 28 50 23 1,000 454 950 431 920 417 780 354 CK 29 50 23 1,000 454 950 431 920 417 780 354 CK 30 50 23 1,000 454 950 431 920 417 780 354 JB 3-Sep 31 50 23 1,000 454 950 431 920 417 780 354 193 JB 32 50 23 1,000 454 950 431 920 417 780 354 JB 33 50 23 1,000 454 950 431 920 417 780 354 JB 34 50 23 1,000 454 950 431 920 417 780 354 JB 35 50 23 1,000 454 950 431 920 417 780 354 PK 36 50 23 1,000 454 950 431 920 417 780 354 PK 37 50 23 1,000 454 950 431 920 417 780 354 PK 38 51 23 1,000 454 949 431 919 417 779 354 PK 39 50 23 1,000 454 950 431 920 417 780 354 PK 40 50 23 1,000 454 950 431 920 417 780 354 J B 4-Sep 41 50 23 1,000 454 950 431 920 417 780 354 J B 42 50 23 999 453 949 430 919 416 779 353 JB 43 50 23 1,000 454 950 431 920 417 780 354 Total tare lbs 2,151 Total tare Kg 989 Total gross lbs 42,995 Total gross Kg 19,516 Total Net lbs 40,844 Total Net Kg 18,526 Total lbs U3O8 39,533 Total Kg UaOg 17,932 Total lbs U 33,524 Total Kg U 15,206 Total Obligated 193 Calcined 0 Reaen 193 KF 0 White Mesa Mill Date 07/11 Revision DUSA-2 Transportation Accident Response Plan Page 41 of 44 Figure 4.2 ACCIDENT REPORT 10 Date Time 2 0 Person Calling Capacity From Telephone No Who Else Notified 3 0 Accident Location 4 0 Description of the Accident Persons Injured Name(s) Treatment Accident Description 5.0 Was Any Company Material Spilled from the Vehicle(s)'^ 6 0 What Action Has Been Taken to Contain the Matenal'? 7 0 Please report this information to one of the following Monday - Friday 8*00 a m to 4 30 p m MST Harold R Roberts, Executive Vice President - Operations Denver, Colorado Telephone No. 303-628-7798 day time, work days Night and weekend contact Telephone No (303) 756-9050, Cell Phone (303) 902-2870 Dan Hillsten, Mill Manager, White Mesa Mill, Blanding, Utah Telephone No. 435-678-2221 day time, work days Night and weekend contact Telephone No (435) 979-3041 41 Energy Fuels Resources (USA) Inc. Material Safety Data Sheet Energy Fuels Resources (USA) Inc requests that users of this EFR product study this data sheet to become aware of the product's hazards, and promote safe handling of the product by making this information availble to Its employees, agents and contractors If the matenal is resold. Energy Fuels Resources (USA) Inc requests that the purchaser be furnished a copy of this data sheet and advised to provide the information herein to its ^ employees, agents and contractors Section I Product Indentification Product Name Yellowcake Creation Date December 6,1993 Revision Date April 20, 2008 CAS Numbers 1344-59-8, 13721-34-1, 1314-64-3, 1309-37-1,7778-18-9, 12136-45-7,7757-82-6, 1314-62-1,7631-86-9, 1344-28-1 Chemical/AUoy Name Uramum Uranyl Oxides, Uranium Octaoxide Formula/Composition UjOg (65-95%), Na2U207 (2-21%, UO2SO4 (2-14%), Fe203 (0-2%), CaS04 (0-4%), K2O (6-2 5%), Na2S04 (0-10%), V2O5 (0-1 5%), S1O2 (0-1%), AI2O3 (0-4%) Synonyms UsOg, Uranium Concentrates Formula/Composition UjOg (65-95%), Na2U207 (2-21%, UO2SO4 (2-14%), Fe203 (0-2%), CaS04 (0-4%), K2O (6-2 5%), Na2S04 (0-10%), V2O5 (0-1 5%), S1O2 (0-1%), AI2O3 (0-4%) Transportation Placard Required - UN2912, Radioactive Class 7 Formula/Composition UjOg (65-95%), Na2U207 (2-21%, UO2SO4 (2-14%), Fe203 (0-2%), CaS04 (0-4%), K2O (6-2 5%), Na2S04 (0-10%), V2O5 (0-1 5%), S1O2 (0-1%), AI2O3 (0-4%) Section n Phvsical Data Size 0 25 inch (0 64 cm) Solubility m Water (g/100 cc) UO2SO4 soluble, CaS04 0 21, Na2S04 4 8, V2O5 0 8, K2O V Sol, U3O8, Na2U207, Fe203, S1O2, AI2O3 insoluble Specific Gravity (H2O = 1) 8 3 Melting Point T ("C) U3O8 2372 (1300) decomp, Fe203 2849 (1565), CaS04 2642 (1450), K2O 662 (350) decomp, Na2S04 1623 (884), V2O5 1274 (690), S1O2 2930 (1610), AI2O3 3762 (2072), Na2U207, UO2SO4 not available Odor None Melting Point T ("C) U3O8 2372 (1300) decomp, Fe203 2849 (1565), CaS04 2642 (1450), K2O 662 (350) decomp, Na2S04 1623 (884), V2O5 1274 (690), S1O2 2930 (1610), AI2O3 3762 (2072), Na2U207, UO2SO4 not available Appearance Yellow to olive-green powder Melting Point T ("C) U3O8 2372 (1300) decomp, Fe203 2849 (1565), CaS04 2642 (1450), K2O 662 (350) decomp, Na2S04 1623 (884), V2O5 1274 (690), S1O2 2930 (1610), AI2O3 3762 (2072), Na2U207, UO2SO4 not available Bulk Density 80-190 lbs/ft' (1 3-3 0 g/cm") Melting Point T ("C) U3O8 2372 (1300) decomp, Fe203 2849 (1565), CaS04 2642 (1450), K2O 662 (350) decomp, Na2S04 1623 (884), V2O5 1274 (690), S1O2 2930 (1610), AI2O3 3762 (2072), Na2U207, UO2SO4 not available Molecular Weight UjOg 842, Na2U207 634, UO2SO4 336, Fe203 160, CaS04 136, K2O 94, Na2S04 142, V2O5182, S1O2 60, AI2O3 102 Melting Point T ("C) U3O8 2372 (1300) decomp, Fe203 2849 (1565), CaS04 2642 (1450), K2O 662 (350) decomp, Na2S04 1623 (884), V2O5 1274 (690), S1O2 2930 (1610), AI2O3 3762 (2072), Na2U207, UO2SO4 not available Molecular Weight UjOg 842, Na2U207 634, UO2SO4 336, Fe203 160, CaS04 136, K2O 94, Na2S04 142, V2O5182, S1O2 60, AI2O3 102 Boiling Pomt S1O2 4046 (2230), AI2O3 5396 (2980), Others not available Vapor Pressure Essentially ml Percent Volatile Not applicable Evaporation Rate Not applicable Section III Hazardous Ingredients Material or Component (CAS #) Weight % TLV Uranium-Uranyl Oxides, U3O8, (1344-59-8) (65-95) 0 2 mg/m^ - TWA8 (1)(3) (Insoluble Compound) (As U) Sodium Diuranate, Na2U207 (13721-34-1) (2-21) 0 6mg/m^-STEL(l)(3) Uranyl Sulfate, UO2SO4 (1314-64-3) (2-14) 0 05 mg/m^ - TWA8 (1) 0 2 mg/m^ - TWA8 (3) 0 6mg/m^-STEL(3) Iron Oxide, Fe203 (1309-37-1) (0-2) 10 mgW, fume (1) 5 mg Fe/m^ fume (3) Calcium Sulfate, CaS04 (7778-18-9) (0-4) 10 mgW - TWA8 (total)(3) 15 mg/m^ - TWA8 (total)(3) 5 mgW - TWA8 (respirable)(l) Potassium Oxide, K2O (12136-45-7) (0-2) No PELS listed (1)(2)(3)(4)(5) Sodium Sulfate, Na2S04 (7757-82-6) (0-5) No PELs listed (1)(2)(3)(4)(5) Energy Fuels Resources (USA) Inc. Inhalation Remove victim to fresh au: Give oxygen if breathing is difficult Call a physician promptly If breathing has stopped, perform artificial respirations Eyes Flush eyes promptly with large quantities of water for at least fifteen minutes If irritation is present, see a physician promptly NOTE TO PHYSICIAN Treat poisoning with intravenous bicarbonate to facilitate lenal excietion Piompt administi ation of EDTA enhances removal of uranium (*)Failure to follow the precautionary measures recommended in Sections V, VI, VII, VIII and IX may result in overexposure Section V Fire and Explosion Data Combustibility Essentially non-combustible Flammable Limits Not applicable Flash Pomt (Test method) Not applicable Autoignition Temperature Not applicable Explosion Tendency None Extinguishing Media No fire hazard Special Fu-e-Fightmg Procedures Avoid procedures which may create dust When fighting a fire involving this material, wear full protective equipment including positive-pressure breathing apparatus Mimimze spread of water-borne solids Unusual Fire and Explosive Hazard None Section VI Reactivity Data Stability Stable in air and water Soluble in HNO3 with formation of uranyl nitrate Soluble in HF/H2SO4 Decomposes m UO2 at 2372°F (1300°C) Conditions to Avoid None Hazardous Decomposition Products None See "Stability" for possible reaction products Materials to Avoid None Section VII Spill. Leak, and Disposal Information Steps to be taken if Material is Spilled or Released Restrict persons not involved with cleanup from the area of the spill until cleanup is completed Use HEPA dust collection or temporary cover, if available, to control the level of airborne dust Use shovel, vacuum, or mechanical means to collect spilled material Avoid maneuvering with compressed air or any other method which generates dust Cleanup personnel should wear skin and eye protection and avoid the inhalation of dust by the use of appropriate respiratory protection Radioactive materials license condition must also be followed Neutralizing Agents None Waste Disposal Method Steps to be taken if material is spilled or released This material contains ingredients which are included m 40 CFR 302, Table 302 4, "List of Hazardous Substances and Reportable Quantities" This material is a "low specific activity" radioactive regulated material and must be disposed of in accordance with Nuclear Regulatory Commission, state and local regulations Section VIII Special Protection Information Ventilation Provide sufficient mechanical HEPA dust collection, combined with administrative controls, if applicable and needed to keep exposures below the permissible exposure limit Eye Protection Dust resistant safety glasses should be woin Facilities to flush the eyes with water should be readily available • Energy Fuels Resources (USA) Inc. FOR INDUSTRLM. USE ONLY Precautions for handling and storage "Materizil should be stored in tightly closed containers and kept dry Eating or smoking should not be permitted in areas where dust is present Avoid contamination of clothing with this material and wash hands thoroughly with soap or mild detergent and water before eating, smoking, or using toilet facilities Other Precautions Carcinogen Listings National Toxicology Program Annual Report (NTP) Not Listed International Agency for Research on Cancer (lARC) Not Listed OSHA 29 CFR Part 1910, Subpart 2 Not Listed Energy Fuels Resources (USA) Inc behoves that the data herein are current as of the effective date of this data sheet and that the opinions herein are those of quahfied experts Since the product and the information herein will be used outside the control of Energy Fuels Resources (USA) Inc , it is the user's responsibility to estabhsh conditions for safe use of the product The data herein relate only to the product of Energy Fuels Resources (USA) Inc and may not be applicable for products of other manufacturers WorkCentre 7346 Transmission Report 435 678 2224 Date/Time 09/10/2012 08 ISAM Page 1 (Last Page) Local Name Denison Mines Logo White Mesa Mi I I Blanding Ut Document has been sent Document Size 8 5X11"SEF ^RSB LOGISTIC wwwJtUogbticcoiii RSBLOdSnCINC. 219 Ctiduul Oesxnl Sukato<iii,5K STL 7m Pbone. 30S-^42-8300 Toll Ftea 80(l«S7-3934 Pm 306-242-2311 ATTACHMENTl RE Energy Fuels Resources (USA) Inc.-Lot #88 Certfficataa o/S:qmt PiEng THESE COMMODinES 'reCHNOLOOY OR SOFIWARE WERE EXPORTED FROM THB UNTIEI) STATES IN ACCORDANCE WTFH THE EXPORT ADMINISTRAITON REGULATIONS DIVERSION CONTRARY TO US LAWPROHEBrrED NOSED REQtJIRED-AES-132637752-RFn62362. AES UN X20120906034794 SASKAIOCHSK Total Pages Scanned 6 Total Pages Sent 6 No Doc Remote Station Start Time Duration Pages Co n t e n t s 1 1319 705 2S2-1153 9-1O 8 15AM Note RE Resend PG Pol I ing SA Send Ag; MB Send to Ma i I box RB Relay Broadcast EN Engaged BC Broadcast RS Re I ay Send AS Auto Send MP Mu I t I Po Ming BF Box Fax Forward TM Terminated RV CP Remote Servici Comp I e t ed I 1 f r I 0» • • M 11 I' M'' !! 11 < i' • i ' ^ iii,i.n ,1' r 1 " >• > b i HI X) 'I r^- I j I i.j' .f > i ill,! ''"i I ' i I.! -'f '111,-' n.' » t'^ J I ftjt I ;j r?'> ill , =f i I ir\,'v A } ! I !! . .'.".I .fs J i. M. -I .; <^\^'.(\f\ ! j. M I fH' f ni 5 I* J i .J/,''f»J ; I')/'! Ki^i !'/"'! I'l/i 'Ml,' n/;; s f i f'^' "i I,' U3 © \ CL OJ D-OJ I- (3 a PQ a: UD cs OD OJ OJ I (S I CL LU CO 0/7SB LOGISTIC Driver Routing Instruction Product Class: Radioactive Material. Low Specific Activity. (LSA) n.o.s. 7 i/?vr# 2912 Shipper Denison Mhies, Blandmir. UT Consignee- Cameco Blind River. ON Freight Bill^: K036315 Trip #: 54947 Have you hauled this product before? O Yes O No (If NO, call Safety Director immediately @ 306-242-8300) SPECIAL INSTRUCTIONS: 1. Acknowledge receipt of 6 instruction sheets by initialing and faxing back to (306) 65) -0600. 2. No riders/passengers allowed during this trip. 3. Entire driver routing instruction package to be rehu-ned to RSB with trip paperwork. 4 Two load bars required. 5 Tractor Backup Alarm required. 6. Drivers MUST call ahead to Boarder Crossing @ 906-632-8822 ext. 272, advising of Radioactive load 7. Escorts required for International / Mackinac Bridge see Page 4 for instructions. Please acknowledge that each of the following duties are completed by checking the appropriate circle ACKNOW INITIALS ''Safety Above Air Please Remember. When roads are poor, get off the road Do not take any chances with this load' Ai The Shipper's: Enroute O Confirm Product Description matches B/L O B/L is complete & in compliance O Placards on trailer before loading O Spare placards received from shipper O Spill Kit Complete O MSDS sheets received from shipper O Load is blocked and braced O Trailer is sealed {Dnver mttst not break seal) Seal Is trailer sealed with bolt seal? O Tire checks (2 hours/100 miles) O Placard check (2 hours) O Stop at all railroad crossings O Authorization required to unhook from trailer O If disabled contact Saskatoon O Do not travel if chains are required Lock & Security Procetiures Maintain awareness ofthe following O Check trailer seal for tampermg O Trailer must be seated upon deliveiy O Secure tractor, shut off engine O Do not leave keys inside tractor O Keep unit visible when unattended Q Check 5**' wheel and other equipment O Mamtam regular contact via satellite or cellular O Yes O No Bid Customs Break Seal? O Yes O No (If YES, call Dispatch immediately) Customs Broker: Near North Border Crossing: Sault Ste Marie. ON New seal U 53809 Unit Signature Fonn #036 Updated March 2012 Page 1 Date Guide 162 Btonduig UT - Blind River ON 0RSB LOGIsfk Driver Routing Instrucmn Product Radioactive Material, Low Specific Actmtv (LSA), n.o.s. Class. JL C/Ar# 2972 Shipper: Denison Mines. Blandmg. UT Consignee' Cameco Blind River. ON In an Emergency, contact 911 or local authorities, then notify RSB (306) 242-$300. The following route must be followed. Any deviations must be reported to RSB immediately to ensure regulatory and customer compliance. St/Prv Route Interchange Leg Total UT North US-191 + US-191 Ramp 105 9 105,9 UT Right Ramp Ramp 1-70 0.3 106 2 UT East 1-70 (to UT/CO State Line) 49.1 155 3 CO East 1-70 + 1-70 Exit 87 86.5 241.8 CO Keep right Exit 87 + Exit 87 US-6 0,4 242 2 CO East US-6 + US-6 CO-13 35 245 7 CO North CO-13 (to CO/WY State Line) 127.9 373.6 WY North WY-789 Creston Junction, WY 53.2 426.8 WY North WY-789 + WY-789 Ramp 01 426 9 WY Right Ramp Ramp 1-80 a2 427,1 WY East 1-80 (to WY/NE State Line) 214.6 641.7 NE East 1-80 ^ 1-80 Ramp 102 743.7 NE Keep left Ramp Ramp 1-80 1.1 744.8 NE East 1-80 +1-80 Exit 446 341.3 10861 NE Keep right Exit 446 + Exit 4461-680 0.6 1086J NE North 1-680 (to NE/IA State Line) 12.9 1099.6 IA East 1-680 - Merman Bridge Rd + 1-680 Exit 38 3.1 1102.7 lA Keep right Exit 36 + Exit 381-29 03 1103 IA North i-29 + 1-29 Exit 71 9.4 1112.4 IA Keep right Exit 71 + Exit 711-680 0.4 1112.8 IA East 1-680 +1-680 Exit 29A 15 9 1128.7 IA Straight Exlt29A + Exit 29A1-80 0.7 1129.4 IA East 1-80 +1-80 Exit 137B 109.6 1239 IA Keep left Exit 1378 + Exit 137B 1-35 06 1239.6 IA North 1-35 (to lA/MN State Line) 131.2 1370.8 MN North 1-35 +1-35 Exit 13A 12.9 1383.7 MN Keep right Exit 13A + Exitl3A 1-90 05 1384.2 MN East 1-90 (to MN/WI State Line) 115.1 1499.3 Wl East 1-90 +1-90 Exit 45 44 9 1544.2 Wl Keep left Exit 45 + Exit 451-94 0.6 1544.8 Wl West 1-94 +1-94 Exit 143 3 1547.8 Wl Keep right Exit 143 + Exit 143 WI-21 0.3 1548.1 Wl East WI-21 Tomah, Wl 08 1548.9 Wl East WI-21 Necedah, Wi 23.8 1572,7 Wl East WI-21 + WI-21 Ramp 76 8 1649.5 Wl Left Ramp Ramp US-41 0.2 1649.7 Wl North US-41 (to WI/MI State Line) 101.8 1751.5 Ml North US-41 Daggett, Mi 25 7 1777.2 Ml North US-41 US-41 53 2 1830.4 Page 2 Guide 162 Uodat^d March 2013 Page 2 Blandinc U f-Blind River ON 90/20"d \ZL3 0iS DUSI 301 esa 90:8T 3T0S-A0-d @RSB LOGISTH^ Driver Routing Instr^on Product Radioactive Material. Low Specific Acttvitv (LSA). n,os. Class. J_ IW# 2912 Shipper- Denison Mines. Blandmg. UT Consignee- Cameco Blind River, ON St/Prv Route Interchange Leg Total Mi East US-2 + US-2 MI-117 77 3 1907,7 Ml North Mi-117 + MI-117 MI-28 14.5 1922.2 Ml East MI-28 Newberry, Ml 8.1 1930.3 Ml East MI-28 + MI-28 Ramp 48.5 1978 8 Ml Left Ramp Ramp 1-75 0.4 1979.2 Ml North 1-75 +1-75 1-75 8.3 1987.5 Ml North International Brg -1-75 (to US/CA Country Line) 1.1 1988 6 ON North ON-17 B + ON-17 B ON-17 B 1.1 1989.7 ON East ON-17 B + ON-17 B ON-17 3.6 1993.3 ON East ON-17 + ON-17 Local 83.1 2076.4 ON Left Eldorado RO Blind River, ON 0.2 2076.6 Fonn #036 Updated-March 2012 90/£0'd lZi,S PPP 0iS Page 3 01ISIson asd Guide 162 Blandmg UT - Bluid River ON i0 8T 2T02-i0-d3S Bridge Crossing Procedures INTERNATIONAL BRIDGE - Escorts required for loads of Class I, loads in excess of 12' wide and loads in excess of 144,000 lbs. - Escorts are no charge - Toll for 5 axle unit is $20.00 U.S. or $21.15 CDM - To arrange for escort, if required: -Northbound - call 906-635-5255, ext 0 -Southbound - call 705-942-4345, ext 0 MACKINAC BRIDGE (IF REQUIRED) - Escorts required for ALL Hazmat (Placarded) loads, - Escorts are no charge. - Travel in right lane - min. 500 ft spacing - Use 4-way flashers - Maximum speed is 20 mph - ToUis$4.50U,S./axle. - To arrange for escort, if required. o Northbound - Use phone at South end of bridge to call Bridge Authority (exit 339) o Southboimd - Stop at toll booth. - Bridge Authority can be contacted at 906-643-7600. Please contact the Saskatoon Safety Department if you have any questions. 90/p0'd TEl.9 PPP 0iLZ 0I1SI901 aSd <L0:8T ZT0Z-LQ-d35 CARRIER'S INSTRUCTIONS YOUR CARGO IS CALCINED PRODUCT THIS MATERIAL: 1) Is NOT explosive. 2) Can be approached without danger. The amount of radiation is insignificant. 3) WiU not bum. 4) Should not be swallowed or put m mouth. 5) Should not be inhaled. IN THE EVENT OF ACCIDENT, AS SOON AS POSSIBLE: ~ 1) Take prefiminary precautions (below). DispUy these instructions as necessary to local authorities on fhe scene to obtain their hdp. 2) Evaluate tiie situation, and record all pertinent infonnation. 3) CaD collect (or have local auffaorities call for you); Cameco (705)3S6'14$6 Cameco Security . BLIND RIVER, ONTARIO If possible, have emi autiiority participate in caU. 4) Make no other statements or phone calls exc^t on.in5tnicttons 'firom Cameco or RSB Logistic, Inc. PRELIMINARY PRBCAimONS - A. .CONTAINERS ARE NOT LEAKING, and are not seriously.damaged. Containers may or may not have been thrown from truck. Truck may or may not have been damaged^ 1) Caution people not to tamper with the containers. Use dvil authorities to help you if necessaiy. 2) It is not necessaiy to have a specific distance between people and the container or the truck, but for ease of controllixig the situation, ask people to stay bade 10 - 15 feet 3) If closed containers are l^ng on the right of way, obtain assistance from whatever dvil authority is available to move containers to the side ofthe right of way. 4) Ensure local audiorides that there is no danger in handHng closed containers. B. CONTAINERS ARE LEAKING OR DAMAGED TOO SERIOUSLY TO BE MOVED. Truck may or may not have been damaged. 1) Caution people to stay away from the material. Keep them at a distance of at least 25 feet up wind. Extreme distance is notiiecessary. Assure local authorities that there is no danger from radiation but that people avoid inhaling any dust from the material. 2) This vehicle contains a box or dnim of emergency equipment such as plastic sheeting, stakes, nails, respirators, etc. this material should be used to perform the foUowing steps: a) Avoid trackage of material. Keep material from running into streets, gutters, sewers, etc. Prevent the material from being scattered by the wind. b) ' Avoid inhaling dust from the material. When covering the material, use a respirator C. FIRE INVOLVING THE TRUCX OR IN IMMEBJATE VICINITY OF TRUCHEC. 1) Isolate the truck from people and property if possible. Use civil authorities for help. 2) . Obtain fire fighting help from local groups. . . 3) Keep fire away, from calcined product containers if po^iHe.' 4) Use precautions to avoid inhaling smoke from any fire involviiig your cargo because of possibility of airborne particles , " " "90/S0-d TZLS PPP QLZ OliSIQOn aSd <L0:8T ZTQZ-L0-d3S Radioactivo iyl(p:erial$ (Low to ModeraiHf Level Radiation) POTENTIAL HAZARDS Health • Radietion presents minimal risk to transpoit workers, emergency response personnel and the public during transportation »iccidcnt9. Packaging durability increases as potential Aazardf of radioacuve conient increases. • Undamagpd packages are safe. ConteniS of damaged packages may cause higher external radiation exposure, or both external and internal radiation exposure if contents are released. • Low radiation hazard when material is inside container If matenal is released from pacicage or bulk contamer, hazffsd will vary hem low to moderate • Level of hazard will dqsend on the ^^pe and amount of ladioactivity, the kind of matenal it is m, and/or die sur&ces it is on. • Some material may be released &om packages dunng accidents of moderate severity but risks to people are not gceaL • Released radioactive materials or contambated objects usually will be visible if packaging fails • Some exclusive use shipments of bulk and i>adcaged materials will not have "RADIOACTTVB" labels Placards, markings and shipping papers provide identificatian. • Some packages may have a "RADIOACTIVE" label and a second hazard labeL The second hazard is usually greater than the radiation hazard; so follow this GUIDE as well as ^e response GUIDE for the second hazard class label. • Some radioactive materials cannot be detected by commonly available mstruments • Runoif irom control of cargo fire may cause low-level pollution. Rrc» or • Some of these matenals may bum, but most do not ignite readily. Explosion ^ Uranium and Thorium metal cuttings may ignite spontaneously if exposed to air (see GUIDE 136), • Nitrates are oxidizers and may ignite odier combustibles (see GUIDE 141), PUBLIC SAFETY 4 CALL Emarganey Response Telephone Number on Shj^ping Paper first If Shippiog Paper not available or no answer, refer to appropriate telepboDO number listed at the ead of this section. • Priorities for reseue^ Ufe^aving, flrst aid, fire control and other hazards are higher than the priority for measuring radiation levels. • Radiation Authority must be notified of accident condiuons. Radiation Audiority is usually responsible for decisions about radiological consequences and closure of emergencies. • As an immediate precautionary measure, isolate spill or leak area for at least 25 meters (75 feet) in all directions, u Stay upwind. D Keep unauthonzed personnel away. • Detain or isolate uninjured persons or equipment suspected to be contaminated,- delay dccontanunadon and cleanup until instructions are received from Radiation Authority. Pfolectlve • Positive pressure self-contained breathing apparatus (SCBA) and structural firefighters' protective clothing will Clothing provide adequate protection Evacuation Large Spill • Consider initial downwind evacuation for at least 100 meters (330 feet) Fire • When a lei:ge quantity of this material is involved in a major fire, consider an initial evacuation distance of 300 meters (IOOO feet) k all dnecLions ErvJERGENCY RESPONSE Fire • Presence of radioactive material will not influence the fire control processes and should not influence selection of techmques. • Move containers from fire area if you can do it without risk. • Do not move damaged packages; move undamaged packages out of fire zone Small fire • Dry chemical, CQ-, water spray or regular foam. Large Fire • Water spray, fog (flooding amounts # Dike fire-control water for later disposal. Spill or • Do not couch damaged packages or spilled matenal l^ak ^ Cover liquid spill with sand, earth or other non-combustible absoibent material 4 Dike to collect large liquid spills. • Cover powder spill with plastic sheet or taip to minimize spreading. Fiist Aid • Medical problems take priority over radiological concems, • Use first aid treatment according to the nature ofthe mjury • Do not dela^ care and transport of a seriously mjuied person. • Give artificial respimtioo if victim is not breathing • Administer oxygen if breathing is difficult. • In case of contact with substance, wipe from skin immediately; flush skin or eyes with running water for at least 20 mmutes • Injured persons contaminated by contact with released matenal are not a serious hazard to health care personnel, equipment or facilities. • Ensure that medical personnel are aware of the material(s) involved and take precautions to protect themselves and prevent spread of contamination © Danatec Educational Services Ltd. 90/90 "d IZiLS PPP QIZ Excerpts from the 2004Eme/genqy Response Guidebook page 667 DUSI son aSd Z.0 ST ZT0Z-L^-63S Date 5-Sep-12 YC lot 88 WWIVl Cameco Cameco Cameco, Element: Analysis % Penalty Spec. % Surcharge U3O8 96 79 0 00 8 0 74 1 00 4 00 0 As 0 03 0 05 0 15 0 Zr 0 00 0 10 0 50 0 Na + K 0 62 1 00 2 00 0 0 00 0 00 0 00 V 0 01 0 10 0 50 0 Mo 0 08 0 10 0 30 0 Fe 0 02 1 00 2 00 0 YC lot 88 Converter Surcharge $ cost $0,007 lbs Uadsl Cameco 0 00 0 0000 Total lbs Total Ka Gross 40,844 18,527 U3O8 39,209 17,796 U 33,255 15,086 Totals 0.00 Sign Off Dan Hiilsten Craig Barlow UnrestrlctenRelease Documentation 3 O ENERGY FUELS RESOURCES (USA) INC. DECONTAMINATION FINAL RELEASE I have venfied that tractor NA and/or container Tractor Number 11 [ has been checked for any contammation and has been Container Number authorized for final release. — Radiation Technician 9 J | 5 / / RadiationUeparttnent Title Date R \radiation\Forms\decon doc o o ENERGY FUELS RESOURCES (USA) INC. DECONTAMINATION FINAL RELEASE I have verified that tractor NA and/or container , Tractor Number G^Fh ') ODIO'^.S has been checked for any contamination and has been Container Number authorized for final release. iAAJiX\\ Y^>-A.^\>.Z-.^ Radiation Technician 9 - / S ~ / Radiation Department Title Date R \radiation\Fonns\decon doc 1 Date ^rVZzyh Container ID Cj-^^\0CyOl^ Inside Locations rgy Fuels Resources (USA) Inc. quipment Survey for Unrestricted Release Surveyed By %) :>7'>K p.fK.' k Outside Locations Front 19 L Side 13 14 23^^ 15 16 RSide 7 8 22—^ 9 10 11 1 2 3 4 5 6 20 Tailgate Location # Total Alpha dpm/IOOcm' Removable Alpha dpm/IOOcm* Beta Gamma 1 t 0.1 2 3 I3S"C> 4 7Ao 5 6 7 8 9 I3S-0 10 00 11 12 13 14 15 135-T) 16 17 18 'N 19 Total Atpha Instrument SN Cal Date :N5IOE 1.10 dpm/iOOcm' Location 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 Rails Total Removable Alpha Alpha Beta # dpnt/iOOcm* dpm/IOOcm* Gamma ^o> 1 to 1 to I il// m \ k ^^ w % Y ho ol Truck and Tire Survey 1 0 0 2 3 00 004 5 00 OOe Total Alpha/ Beta-Gamma •ocatlon 1 cpm It Truck Ext Function Check (5x1 mm) Til 230 @ 33000 dpm Bkg Average _ %.0 Dpm Average _ */ i^?^ Efficiency 12 HO^ EfTFactor 9i Q MDA Removable alpha • 1000 dpm/IOOcm^ ^ed alpha - 5000 dpm/1 OOcm^ average 15000 dpm/IOOcm^ maximum Instrument Data Removable Alpha Model SN lH(»7gl Cal Date L <^u«^.lf: Function Check(5x1 mm) Alpha Bkg Ave I 1 Alpha eff ^J^^fj^ Alpha Factor 1^ TRAILER TIRES 7 00 0 08 9 00 OO10 11 00 OO12 Total Alpha/ Beta-Gamma Location cpm Total Beta/Gamma Model # SN Cal Date Source Reading Bkg 10 11 cs {"^1 ~ Chassis Ext ^ OMTfltr O'o3 3! Comments > Beta - Gamma - 0 2 mr/hr @ 1cm average 1 0 mr/hr @ 1cm maximum o o o ENERGY FUELS RESOURCES (USA) INC. DECONTAMINATION FINAL RELEASE I have verified that tractor NA and/or container Tractor Number OO [I ^0 has been checked for any contamination and has been Container Number authorized for final release Radiation Technician Radiation Department Title Date R \radiation\Forms\decon doc 1 Equ Date 3L11IV^ Container ID <9 1 \ ^ Q Location i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 Total Alpha Inside Locations irgy Fuels Resources (USA) Inc. quipment Survey for Unrestricted Release Surveyed By TusV>v. "^^VCiKla. Outside Locations Front 19 L Side 13 14 7 8 1 2 2a ^ 15 16 22 9 10 3 4 RSide 11 5 6 20 Tailgate Total Alpha dpm/IOOcm* Removable Alpha dpm/IOOcm* Beta Gamma r f ^ 1 w. / /k-\ / ^ f CS'? 28 fcoTtor^ dpm/1 OOcm* Location i 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 Rails 27 ^ Oft Front 37 29 27 ^ Oft 34 -—-36 7 31 25 V 7 31 Total Alpha dpm/IOOcm* 24 Removable Alpha dpm/IOOcm* Beta Gamma 1 J A / / \ \ to 1 1 1 1 f % 1 \ 1 Truck and Tire Survey >UTSIO£ LXO 1 0 0 2 3 00 004 5 00 OOe Total Alpha/ Beta-Gamma •ocatton i cpm Tmck Ext 3z: Instrument Data TRAILER TIRES 7 00 OOe 9 00 O0io 11 00 O0i2 Total Alpha/ Beta-Gamma Location cpm Instrument SN Cal Date Function Check (5x1 mm) Th 230 @ 33000 dpm Bkg Average ^.Q Dpm Average__tj^kg^_ Effiaency 1'^")% Eff Factor MDA lil Removable alpha -1000 dpm/IOOcm' p alpha - 5000 dpm/IOOcm'average ^ ' 15000 dpm/1 OOcm' maximum Beta - Gamma - 0 2 mr/hr @ 1cm average 10 mr/hr @ 1cm maximum /Removable Alpha Model SN Cal Date Function Check(5x Alpha Bkg Ave Alpha eff /\lpha Factor 1 mm) Total Beta/Gamma Model* SN Cal Date Source Reading Bkg Y12 Cs Ml Chassis Ext 10 Mi Comments Weekly facility Snivoys White Mesa Mill Weekly Alpha Survey Date: 9-/^-/^ Technician: f^eafl Z^fA^ Alpha Survey Instruments Fixed IVIodel#: 3 Serial #. ]?S5gl Calibration: 11 Efficiency: 1^.^% Factor* 7.^ Background: 3^ MDA: jg| Removable Model #: 55^^ Serial #: 1153^ Calibration: lOfkl^J^ Efficiency: Factor- 3.9 Background: Z^-? MDA: 73. gy Notes: All fixed readings are in dpm/100 cm T or t = Total or Fixed Alpha Reading in dpm/100 cm^ R or r = Removable Alpha Reading per swipe or filter (approximately 100 cm^) RSO Reviewed: RSO Comments: 44 Maintenance and Warehouse Areas ^\etjr ^ oof /^/3-* Foreman'j Office deik Elect Foreman's Warehous e Office Instrument Warehouse supply Office pe/k Maintenance Operatian Foreman s Office Operation Foreman s tjffice •plow fl oo»* Survey-Alpha Date 'i-IA-ia 3 Inst Cal Date _A7^ SN /J?5S'7 Tech All units m dpm/100 cm Change/Lunch Room IVIen's Locl<er Room Women's Locl<er Room Sliower f^or^< ro«*^ Laundry Room Table -floor Survey-Alpha Date ^'19-^13^ Inst Table 4 Cal Date /7/?Mg All units in dpm/100 cm^ iikJU T^^lo Luncli Room Table Scalehouse Restroom pi cor Table Survey-Alpha Date ?'/3 Inst 3 Cal Datt Tech All units m dpm/100 cm Central Control Room Table Table Survey-Alpha Date 9-/3'/<2 Inst 3 Cal Date /7/?y /3 Tech Mi All units in dpm/100 cm Table X'^)^ b EMPLOYEE SPOT ALPHA CONTAMINATION SURVEY DATE 1 NAME BOOTS CLOTHES HANDS COMMENTS 9'/3'/a J Tfre.f P««-l2y m T \ j covc^r^lf^ Alplia Instrument Information instrument iViodei 3 Instrument SN 1^3(^1 Th23o Source SN S^i'O^ DPM 39006 CPIVi Efficiency Efficiency Factor 7.4 ReleasePneeauns No PBL-2 Rev No • R-3 Date July 25,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title Intermodal Container Acceptance, Handling & Release Page 1 of7 LO Purpose The follovvdng procedure applies to acceptance, handling, and release of intermodal containers from International Uranium (USA) Corporation (lUSA) White Mesa Mill (Mill). lUSA receives matenal for processing, in either bulk or non-bulk packagmg This procedure addresses one form of bulk packaging - intermodal containers (IMCs) This procedure may be amended, subject to approval by lUSA's Safety and Enviromnental Review Panel (SERP), from time to time as appropriate to address the individual requirements of specific feed materials, or projects 2.0 Ore Receiving 1. Check truck scale for zero balance at the beginmng of each shift 2. Inbound IMCs will be dropped off m a designated staging area near the Scale House outside the Restncted Area 3 Inspect the inbound IMC for the items hsted on the Intermodal Container Inspection Form (copy attached) Notify Mill management of any discrepancies as soon as practicable The Intermodal Container Inspection Forms will be turned in to tiie Mill office on a daily basis 4 Inspect all copies of the Bill of Lading (BOL) to ensure that the shipment is destined for the White Mesa Mill and that all shippmg documentation is in order (see Section 8 2) If any discrepancies are noted notify the Mill management immediately. Do not dump the container until all paperwork discrepancies are corrected. 5 Assign next available shipment number and White Mesa Mill load number to the inbound IMC Record the White Mesa Mill load number, mboimd date and both tiie truck and IMC numbers on the Scale house Weight Ticket (SWT). 6 A White Mesa tmck will be used to retneve the loaded IMCs stored m the staging area, outside the Restricted Area, and transport them into the Restricted Area The Mill truck will be visually inspected and scanned prior to leavmg the Restricted Area to pick up a loaded IMC 3.0 Ore Dumping i 1 Prior to the dumping of the IMC the tarp and tarp support structures, if applicable, are inspected for damage and then removed 2 Connect the Bartlett tipper to the loaded IMC chassis and transport across the truck scales. P \Adrmn\Master SOPs\Book lO^PBL Sops\PBL-2 IMC SOP Rev3 (08 07 02) doc No PBL-2 Rev No. R-3 Date July 25,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title Intermodal Contamer Acceptance, Handling & Release Page 2 of7 3 Enter tiie loaded weight of tiie IMC on tiie IMC SWT. 4 After weighing the IMC, proceed to the tarping and untarping station. Inspect the tarp then roll the tarp forward. Report the conditions of the tarp and bows ofthe IMC to the Scalehouse via radio. Then proceed to the designated ore storage area and dump the material. 5 After dumping the material, retum the IMC back to the taipmg station and replace the tarp and the bows, unless the IMC is being decontaminated for unrestncted release. 6 After the IMC has been retarped, transport the empty IMC back across the scales for an empty weight 7 Record the empty weight on the appropnate IMC SWT 8 At the end of each day, tum in outbound SWT to Mill Records Manager. 9 , The Mill Records Manager will fill out a Daily Materials Receipts form to obtain the net weight of the material in each IMC 10. After weighing the IMC, the Bartlett tipper will deposit the IMC in a designated area, within the Restncted Area, for decontaimnation. 11 Use a front-end loader or similar equipment to push material into the designated ore lot pile 12 Once an ore lot pile is complete, label the pile with the appropriate • ore lot number 4.0 Decontamination and Release of IMCs All IMCs, chassis and tires will be decontaminated after dumping prior to leaving the White Mesa Mill Generators or transporters will notify lUSA whether a specific IMC and chassis is to be released for restricted or unrestricted use Any IMCs that are to be released for restricted use will be decontaminated 'according to the requirements contained in U.S Department of Transportation (DOT) Part 49 CFR 173 441 and 173 443 (a copy of which is attached) Any IMCs that are to be released for unrestricted use will be decontammated according to the requirements found m Table 1 of the Nuclear Regulatory Commission's (NRC's) Policy and Gmdance Directive FC-85-23, "Guidelines for Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use or Termination of Licenses for Byproduct, Source, or Special Nuclear Material" issued May 1987 (a copy is attached)". IMCs requiring repair will be decontaminated for unrestncted release, to facilitate repairs by the transporter at the P \Admin\Master SOPs\Book 10_PBL Sops\PBL-2 IMC SOP Rev3 (08 07 02) doc No PBL-2 Rev No.. R-3 Date. July 25,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title. Intermodal Container Acceptance, Handling & Release Page 3 of 7 transporter's own site IMCs may be repaired without undergoing full decontamination if repaired within the Restricted Area of the Mill 5.0 Decontamination and Release of IMCs for Restricted Use 1. A White Mesa Mill truck mil pick up the empty IMC, from the staging area within the Restricted Area, and transport it to the decontamination pad. 2 Decontammate the exterior of each IMC, chassis and tires thoroughly, using a high-pressure water wash Put the chassis into the extended position to improve access to the rear chassis tires. 3 After the IMC is decontaminated, use the White Mesa Mill truck or other designated on-site equivalent equipment to move the IMC along the decontamination route. The decontamination route is a graveled roadway specifically designed for decontaminated equipment to exit the restricted area Do not leave the decontamination route. If it becomes necessary due to environmental conditions or residual mud in the tires etc., proceed along the decontamination route to the secondary wash station. Wash any visual residual mud off of the tires, chassis or exterior surface of the container. 4 Proceed along the decontamination route to the tertiary decontamination and final scanmng area. 5 Contact a Radiation Technician to perform a radiological contamination survey of the IMC If the Radiation Techmcian indicates select areas on the IMC that require further decontamination, decontammate those areas as necessary. 6 The Radiation Technician or RSO will scan the IMC, chassis, tires and White Mesa Mill track in various locations as shown on the IMC Container Survey for Restricted Release (attached) and document the scan readings on the Container Survey for Restncted Release. The contamination survey will be performed using appropnate radiological instrumentation for total activity in accordance with DOT transportation regulations The release standards to be met for restricted release are contained in U.S. Department of Transportation (DOT) Part 49 CFR 173 441 and 173.443 (a copy of which is attached) 7 If the IMC, chassis or tires do not meet the radiological release survey requirements or shows visually observable contaminaton, the IMC will either be returned to the secondary decontamination pad for further decontamination or will be washed again at the tertiary decontamination area 8 The Radiation Techmcian or RSO will fill out the IMC survey for Restncted Release form (copy attached) to document that the IMC has been authorized for release for restncted use. These forms are filed in the Radiation Department The P \Admin\Master SOPs\Book 10_PBL Sops\PBL-2 IMC SOP Rev 3 (08 07 02) doc No PBL-2 Rev No.. R-3 Date July 25,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title Intermodal Contamer Acceptance, Handling & Release Page 4 of7 Radiation Techmcian or RSO will place a white sticker on the IMC that says, "EMPTY" and "This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive material, excepted package - empty package, 9 After an IMC has been released, the IMC will be delivered by a White Mesa Mill truck to the designated staging area for empty IMCs, outside the Restricted Area After staging a loaded IMC in the designated area, the incoming driver will pick up an empty IMC at the designated area Prior to leaving the staging area the chiver will perform a visual inspection of the IMC, chassis and tires Leaving his tmck outside of the Restncted Area, the driver will retum to the Scale House to pick-up the documentation for the empty IMC and sign the Intermodal Container Inspection Form 10 A Radiation Techmcian, or the RSO, will scan the designated decontamination route and staging area(s) on a quarterly basis. The survey readings will be recorded and kept on file in the Radiation Department 6.0 Decontamination and Release of IMCs for Unrestricted Use 1 A White Mesa Mill tmck will pick up the empty IMC, from the staging area within the Restricted Area, and transport it to the decontaminaton pad. 2 Open the tailgate and decontaminate each IMC usmg a high-pressure water wash Make sure to thoroughly wash the inside and outside of each IMC, the chassis and tures 3. After the IMC is decontaminated, use the White Mesa Mill truck or other designated on-site equivalent equipment to move tiie IMC along the decontamination route. The decontamination route is a graveled roadway specifically designed for decontaminated equipment to exit the restricted area Do not leave the decontamination route If it becomes necessary due to envuronmental conditions or residual mud m the thes etc, proceed along the decontammation route to the secondary wash station Wash any visual residual mud off of the tires, chassis or exterior surface of the contamer. Otherwise, proceed along the decontamination route to the tertiary decontamination and final scanning area 4 Contact a member of the Radiation Department staff to conduct the appropriate radiological survey of the IMC, chassis, tures and White Mesa Mill tmck, as delineated in Section 2 6 of the White Mesa Mill Radiation Protection Manual The release standards to be met for unrestricted release are contained in Table 1 of the Nuclear Regulatory Commission's (NRC's) Policy and (juidance Directive FC-85-23, "Guidelines for Decontamination of Facilities and Eqmpment Prior to P \Admin\Master SOPsVBook 10_PBL Sops\PBL-2 IMC SOP Rev3 (08 07 02) doc ( No PBL-2 Rev No. R-3 Date: July 25,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title Intermodal Container Acceptance, Handling & Release Page 5 of 7 Release for Unrestricted Use or Termination of Licenses for Byproduct, Source, or Special Nuclear Material" issued May 1987 (Copy attached). 5 The Radiation Technician will perform a radiological contamination survey of the IMC If the Radiation Technician indicates select areas on the IMC that require further decontamination, decontaminate those areas as necessary. 6. If the IMC, chassis or tires do not meet the radiological release survey requirements and/or has visually observable contamination, the IMC will either be returned to the secondary decontamination pad for further decontamination or will be washed again at the tertiary decontamination area. 7 If the IMC, chassis and tires meet the radiological release survey and visual inspection requirements, the Radiation Technician will place a red sticker on the / IMC tiiat says, "THIS CONTAINER HAS BEEN FULLY DECONTAMINATED AND SURVEYED FOR "UNRESTRICTED USE" BY: (FILL IN NAME OF RADIATION TECHNICIAN)" The RSO or Radiation Technician that perfonned the release survey will then sign the red sticker and date h In addition, the RSO or Radiation Techmcian will fill out a Decontamination Final Release Form (a copy of which is attached) to document that the IMC has been cleared for unrestricted release. The form includes a schematic diagram of the IMC with points to be scaimed and locations on the schematic to fill in survey values for each IMC. The Decontamination Release Form will be turned in to the Mill Administration Office daily for filing and distnbution 8 After an IMC has been released, the IMC will be delivered by the White Mesa Mill truck to the designated staging area for empty IMCs, outside the Restricted Area After staging a loaded IMC in the designated area, the incoming dnver will pick up an empty IMC at the designated area Prior to leaving the staging area, the driver will do a visual mspection of the IMC, chassis and tires Leaving his tmck outside of the Restricted Area, the driver will retum to the Scale House to pick-up the documentation for the empty IMC and sign the Intemiodal Container Inspection Form 7.0 Hazard Identification and Safety 7 1 Required Persormel Protective Equipment (PPE) In all areas of the Mill covered by this procedure, hard hats, safety glasses and steel-toed shoes are reqmred as a minimum. These must be worn in all areas of the Mill witii the exception of the Administration Building P \Admin\Master SOPsNBook 10_PBL Sops\PBL-2 IMC SOP Rev3 (08 07 02) doc No PBL-2 Rev No.. R-3 Date July 25,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title Intermodal Container Acceptance, Handling & Release Page 6 of7 7 2 Industrial Hazards and Safety 1 Use caution when chassis are backing onto the Ore Pad 2. Ensure that all persormel within 50 feet of the area where the IMC is hooked up to the Bartlett tipper are aware that dumping is about to commence. 3. Bartiett tipper operators must use caution during the dumping process. Move at least 25 feet away from the rear of the IMC during the imUal dumping operation. 4 Do not place any part of your body inside the IMC when the chassis is being tipped and the tailgate is open. The IMC could be lowered or accidentally fall at any time, which would cause the tailgate to close rapidly and result in injury. Only work under the tailgate after it has been properly blocked open. 5 Be aware of high-pressure wash water. 6 When the crane is in operation, make sure all persormel, except the persons in charge of the tag lines, are 50 feet away from the IMC bemg moved The persons m charge of the tag lines should never be underneath the IMC that is being moved 7. Be aware of slippery conditions on the ore pad during periods of inclement weather 8 Be aware of the potential for ice bmld-up on and around the decontamination pad during penods of cold weather. 9. Use caution when entering or exiting eqmpment Be sure to use the ladders and hand rails Do not jump off of the equipment. 10 Always use a ladder when entering and/or exiting the interior of an IMC 8.0 Paperwork Tracking 1 Each IMC will have a umque sequential project number assigned to it at the generating facility This number will be entered onto the Bill of Lading (BOL) and attached to the IMC prior to shipment from the generation site 2 Upon arrival at the White Mesa Mill, the tmck driver will tum m all of his/her paperwork to the Scale House operator who will verify tiiat the BOL number, IMC number and project number assigned to.the shipment match on all copies of the BOL The Scale House operator will also verify that tiie actual IMC number matches tiie BOL IMC Number If there are any discrepancies in any of the numbers notify Mill management immediately. Only origmal paperwork will P \Admin\Master SOPs\Book 10_PBL Sops\PBL-2 IMC SOP Rev3 (08 07 02) doc r INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title Intermodal Contamer Acceptance, Handling & Release No. PBL-2 Rev No R-3 Date July 25,2002 Page 7 of7 be accepted. If the original paperwork does not come vsdth the IMC, notify Mill management immediately. The Scale House operator will sign the BOL, acknowledging receipt of the material at the Mill, if all of the paperwork is m order Depending on contractual and/or sampling requirements, final acceptance or rejection of certain altemate feed materials may be contingent on analytical results. Each IMC will be transported across the scale at the Mill pnor to and after being unloaded The appropnate information will be entered into the project database All copies of the SWTs and BOLs will be forwarded to the Mill Records Manager on a daily basis or other frequency specified by Mill Management, from time to time The Mill Records Manager will compile and reconcile the BOL's and SWTs for distribution. The accounting department will forward a summary of all receipts to the International Uranium corporate office and the generator of the matenal at least twice monthly, or at other frequencies as determmed for the specific project P \Admin\Master SOPs\Book lO^PBL Sops\PBL-2 IMC SOP Rev3 (08 07 02) doc INTERNATIONAL URANIUM WHITE MESA MILL INTERMODAL CONTAINER INSPECTION FORM Number Container Number Chassis Number 1 Correct Paperwork 2 Decontaminated 3 Tarps 4 Tarp Tie Downs 5 Tarp Support Bows 6 Bow Attachment Brackets 7 Lifting Lugs 8 Structural Damage 9 Latch Mechanisms 10 Tires 11 Mudflaps Additional Comments Date lUC Driver&Trk Num. incoming Outgoing INTERNATIONAL URANIUM (USA) CORPORATION DECONTAMINATION FINAL RELEASE I have venfied that tractor NA and/or container Tractor Number has been checked for any contammation and has been Contamer Number authorized for final release Radiation Technician Radiation Department Title Date C \windows\TEMP\decon SOP doc International Uranium (USA) Corporation Intermodal Container Survey for Restricted Release Oate Container ID Ashland or Linde Surveyed By Outside Locations Lccatlon# 24 25 26 27 28 29 30 31 32 33 34 35 36 37 Rails Instrument Data Total Alpha/ Beta/Gamma Model # SN Cal Date Source Efficiency Total Alpha/ Beta-Gamma cpm lUSA Truck and Tire Survey 0 0 0 0 00 00 00 Tota! Alpha/ Beta-Gamma ^9caHpn| cpm 1 2 3 4 5 6 Truck Ext IMC CHASSIS TIRES 00 00 00 00 00 00 Total Alpha/ Beta-Gamma Location # cpm 7 8 9 10 11 12 Chassis Ext ASH2(b) Date: Location # 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 international Uranium (USA) Corporation Intermodal Container Survey for Unrestricted Release Container ID Inside Locations Ashland or Linde Front 19 L Side 13 14 V 23 15 16 RSide 17 18 7 8 22 9 10 21 11 12 1 2 3 4 5 6 20 Tailgate Total Alpha dpm/IOOcm* Removable Alpha dpm/IOOcm* Surveyed By. Outside Locations dpm/1 OOcm* Location # 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 Rails Total Removable Alpha Alpha dpm/IOOcm* dpm/IOOcm* f «ny location exceeds 1000 dpm/100 cm2 total alpha a swear/wipe survey for removable alphe must be performed }wever additional removabia apB» swipes although not required may be performed Instrument Data Total Alpha Instrument ESP-1 / AC-3 SN 02299 / 1 02286 / 2 Cal Date I ' Function Check (5x1 mm) r/> 230 ©30300 dpm Bkg Average Dpm Average Removable Alpha Model SN Cal Date Function Check(5x1 min) Alpha Bkg Ave Alpha eff* Alpha Factor Total Beta/Oamma Model # SN Cal Date Source Efflclency lUSA Truck and Tire Survey 1 0 02 3 00 004 5 00 OOe Total Alpha/ Beta-Gamma -pcatloin ( cpm 1 Truck Ext IMC CHASSIS TIRES 7 00 O08 9 00 O0io 11 00 O0i2 Total Alpha/ Beta-Gamma Location I cpm 10 11 12 Chassis Ext ASH2(a) UocummtKetnevai nnp.//inveDgBieaccessgpogov/cgfouv^. wiiii^c-^y«er/\n.i'^i/j«dcv^iiun-^itti tra-ic [Code of Federal Regulations] [Title 49, Volume 2, Parts 100 to 185] [Revised as of October 1, 1999] From the U.S. Goverimient Printing Office via GPO Access [CISE: 49CEm73.441] ^ ^ ^ [Page 582-583] TITLE 49~TRANSPORTATION CHAPTER I—RESEARCH AND SPECIAL PROGRAMS ADMINISTRATION, DEPARTMENT OF TRANSPORTATION ^ PART 173—SHIPPERS—GENERAL REQUIREMENTS FOR SHIPMENTS AND PACKAGINGS—Table of Cont Subpart I—Class 7 (Radioactive] Materials Sec. 173.441 Radiation level limitations. (a) Except as provided in paragraph (b) of this section, each package of Class 7 (radioactive) materials offered for transportation must be designed and prepared for shipmerit, so that under conditions normally incident to transportation, the radiation level does not exceed 2 mSv/hour (200 mrem/hour) at any point on the external surface of the package, and the transport index does not exceed 10. [[Page 583]] (b) A package which exceeds the radiation level limits specified in ^ paragraph (a) of this section must be'transported by exclusive use shipment, and the radiation levels for such shipment may not exceed the following during transportation: (1) 2 mSv/h (200 mrem/h} on the external surface of the package unless the following conditions are met, in which case the limit is 10 mSv/h (1000 mrem/h): (1) The shipment is made in a closed transport vehicle; (ii) The package is secured within the vehicle so that its position remains fixed during transportation; and (iii) There are no loading or unloading operations between the beginning and end of the transportation; (2) 2 mSv/h (200 mrem/h) at any point on the outer surfaces of the - vehicle, including the top and underside of the vehicle; or m the case of a flat-bed style vehicle, at any point on the vertical planes projected from the outer edges of the vehicle, on the upper surface of the load or enclosure if used, and on the lower extemal surface of the vehicle; (3) 0.1 mSv/h (10 mrem/h) at any point 2 meters (6.6 feet) from the outer lateral surfaces of the vehicle (excluding the top and underside of the vehicle); or in the case of a flat-bed style vehicle, at any point 2 meters (6.6 feet) from the vertical planes projected by the outer edges of the vehicle (excluding the top and underside of the , vehicle); and (4) 0.02 mSv/h (2mrem/h) in any normally occupied space, except that this provision does not apply to carriers if they operate under the provisions of a State or federally regulated radiation protection ^ program and if personnel under their control who are in such an occupied space wear radiation dosimetry devices. (c) For shipments made under the provisions of paragraph (b) of this section, the offeror shall provide specific written instructions for maintenance of the exclusive use shipment controls to the carrier. The ' instructions must be included with the shipping paper infonnation. The instructions must be sufficient so that, when followed, they will cause the carrier to avoid actions that will unnecessarily delay delivery or unnecessarily result in increased radiation levels or radiation exposures to transport workers or members of the general public. WAIS Document Retneval httpy/frwebgate access gpo gov/cgi-bin/a. imrLE«49&PAR'I^173&SECTION«441&TYPE«^ (d) Packages exceeding the radiation level or transport index prescribed in paragraph (a) of this section may not be transported by aircraft. [Amdt. 173-244, 60 FR 50307, Sept. 28, 1995, as amended at 63 FR 48568, ' Sept. 10, 1998] WAIS Dooument Retneval http //fnvebgate access gpo.gov/cgt-bin/g. i?TITLE'=49&PART°173&SECTZON'>443&TYPE-lH [Code of Federal Regulations] [Title 49, Volume 2, Parts 100 to 185] [Revised as of October 1, 1999] From the U.S. Government Printing Office via GPO Access [CITE: 49CFR173.443] [Page 583-584] TITLE 49—TRANSPORTATION CHAPTER I—RESEARCH AND SPECIAL PROGRAMS ADMINISTRATION, DEPARTMENT OF TRANSPORTATION PART 173—SHIPPERS—GENERAL REQUIREMENTS FOR SHIPMENTS AND PACKAGINGS—Table of Cont Subpart I—Class 7 (Radioactive) Materials Sec. 173.443 Contamination control. (a) The level of non-fixed (removable) radioactive contamination on the external surfaces of each package offered for transport must be kept as low as reasonably achievable. The level of non-fixed radioactive contamination may not exceed the limits set forth in table 11 and must be determined by either: (1) Wiping an area of 300 square centimeters of the surface concerned with an absorbent material, using moderate pressure, and measuring the activity on the wiping material. Sufficient measurements must be taken in the most appropriate locations to yield a representative assessment of the non-fixed contamination levels. The amount of radioactivity measured on any single wiping material, when averaged over the surface wiped, may not exceed the limits set forth in table 11 at any time during transport; or (2) Using other methods of assessment of equal or greater efficiency, in which case the efficiency of the method used must be taken into account and [[Page 584]] the non-fixed contamination on the external surfaces of the package may not exceed ten times the limits set forth in table 11, as follows: Table 11—Non-Fixed External Radioactive Contaraination-Wipe Limits Maximum permissible limits Contaminant Bq/cm<SUP>2</SUP> uCi/cm<SUP>2</SUP> Beta and gamma emitters and low toxicity 0.4 10<SUP>-5</SUP> 22 alpha emitters All other alpha emitting radionuclides.. 0.04 10<SUP>-6</SUP> 2.2 (b) Except as provided in paragraph (d) of this section, in the case of packages transported as exclusive use shipments by rail or public highway only, the removable (non-fixed) radioactive contamination on any package at any time during transport may not exceed ten times the levels prescribed in paragraph (a) of this section. The levels at the beginning of transport may not exceed the levels prescribed in paragraph (a) of this section. (c) Except as provided in paragraph (d) of this section, each transport vehicle used for transporting Class 7 (radioactive) materials as an exclusive use shipment that utilizes the provisions of paragraph (b) of this section must be surveyed with appropriate radiation detection instruments after each use. A vehicle may not be returned to service until the radiation dose rate at each accessible surface is iVAIS Document Retrieval httpy/rrwebgatcaccess gpo.gov/cgi-bin/g. .nBn.E-49&PART"I73&SECTION'M43&TVPE-TE: 0.005 roSv per hour (0.5 mrem per hour) or less, and there is no significant removable (non-fixed) radioactive surface contamination as specified in paragraph (a) of this section. (d) Paragraphs (b) and (c) of this section do not apply to any i closed transport vehicle used solely for the transportation by highway or rail of Class 7 (radioactive) material packages with contamination levels that do not exceed 10 times the levels prescribed in paragraph (a) of this section if— (1) A survey of the interior surfaces of the empty vehicle shows that the radiation dose rate at any point does not exceed 0.1 mSv per hour (10 mrem per hour) at the surface or 0.02 mSv per hour (2 mrem per hour) at 1 meter (3.3 feet) from the surface; (2) Each vehicle is stenciled with the words ^^For Radioactive Materials Use Only" in letters at least 76 millimeters (3 inches) high in a conspicuous place on both sides of the exterior of the vehicle; and (3) Each vehicle is kept closed except for loading or unloading. [Amdt. 173-244, 60 FR 50307, Sept. 28, 1995, as amended by Amdt. 173- 244, 61 FR 20753, May 8, 1996] 06/14/2000 II-nAI GIIIOFL'NES FOR DECOKWINATrPN OF FACILITIES ANO EQUlPHm PRIOR TO RELEA:E FOR UNRESTRICTED USF CP TERMINATION OF LICENSES FOR BYPRODUCT, SOURCF, OR SPECIAL NUCLEAR MATERIAL c^j, U.S. Nuclear Regulatory Conwlssion Division of Fuel Cycle, Medical, Academic, and Conwerclal Use Safety ' Wasfilngton, DC 20555 May 1987 t J ' Thp instructions in this cu'de, in conjunction wUh Tjble I, specfv t^p rad^nnuclides and radiation exposure rotp Hmits which should be 'i^ed In dPcontaF'*ndtion and survey of sfr'aces or prenises and pcuipment pnor to abandonment or release Vr unrestr'.rted use. The limits m TeMe 1 do not apply to premises, equipment, or scrap containing induced radioactivity for which the radiological considerations pertinent to their use may be different. The release of such facilities or items from regulatory ccntrol is cmsidered on a case-by-case. 1. 4. The licensee shi»ll malte a reasonable effort to eliminate resic^ual contamination. Radioactivity on pqulpnent or surfaces shall not be covered by paint, plating, or other covering material unless tontamination levels, as determined by a survey and documented, are below the limits specified in Table 1 prior to the application of the covering. A reasonable effort must be made to minimize the contamination prior to use of any covering, ^ The radioactivity on the interior surfaces of pipes, drain lines, or ductwork shall be determined hy making measurements at all traps, and other appropriate access points, provided that contamination at these locations Is likely to be representative of contamination on the inteno 0^ the pipes, drain lines, or ductwork. Surfaces nf premises, eou or scrap which are likely to be contaminated but are of such size. 1. construction, or location as to make the surface inaccessible for purposes of measurement shall be presumed to be contaminated in excess of the limits Upon request, the Conmlsslon may authorize a licensee to relinquish possession or control of premises, equipment, or scrap having surfaces contaminated with materials in excess of the limits specified. This may include, but would not be limited to, special circumstances such as razinq of buildings, transfer to premises tn another organization cnntinuing work with radioactive materials, or conversation of facilities to a long-term storage nr standby status. Such requests must: a. Provide detailed, specific information describing the premises, equipment or scrap, radioactive contaminants, and the nature, extent, and degree of residual surface contamination. b. Provide a detailed health and safety analysis which reflects that the residual amounts of materials on surface areas, toqether with other considerations such as prospective use of the premises, eoulpnent, or scrap, are unlikely to result In an unreasonable risk to the health and safety of the public. 5. Pnor to release of premises ^or unrcftricted use, the licensne shall make a comprehensive radiatmr survey which establisbes that rortamination " within the limits specified m Table 1. A copv the survey reoort shall he fHec* Kith the nivt<;ion Fuel Cycle, Medical, Academic, and Conrerclal l.'se Safety. U. S. NurVar Regulatorv Commission, Washinaton, OC 20555. and also the Administrator of the NRC Recional Office having jwrisdiction. The report- should be filed at least 30 days prior to the planned date of abandonment. The survey report shall: a. Ic'cntify the premises. b. Show that reasonable effort has been made to eliminate residual contamination. c. Describe the scope of the survey and general procedures followed. d. State the findlnas of the survey in units specified in the instruction. Followlpo review of the report, the *IK will consider visiting the facilities to confirm the survey. TABIC I ACaPTABLE SURrACE CONTAHIHATIOII LtVELS NUCllOCS* AVERAGE^ C f MAXtNUnt» <l f REMOVABLE** « f U-nat. U-23S. U-236. and associated decay products Transuranics. Ra-226. Ra^ZZS. Th.230. Th.226. Pa-231. Ac.22;. M25. 1-129 Th.nat, Th-232, Sr-90. Ra*223« R)-224. U-232. 1-126. 1-131. 1-133 Ceta-^an:^ cnitlers (nuclides wUh decay rodes other than alphj emission or spontaneous fission) except Sr-90 and others noted above. • 5.000 dpm tt/tOO cn^ 100 dp^/100 (M? 1000 dp«/100 an2 5000 dpn BT/100 cm^ 15.000 dp« o/lOO on^ 300 dpa/100 Ca2 3000 dpq/100 cn2 15.000 dpn BT/100 at? 1.000 dps o/lOO CB^ 20 dpn/lOO c«2 200 dpo/lOO cn^ 1000 dpm BY/1 00 cm^ •Where surface contamination by both alpha- and beta-gaona-cnltting nuclides exists, the limits established for >inK. .-^ tl,^ nuclides Should apply independently. eswonshed for alpha, and beta-gamna-eniltlng *»As used in this table. dp« (disintegrations per minute) means the rate of emission by radioactive material as Ai^tmt^eut u ... counts per minute observed by an appropriate detector for background, efficiency, and geometric factori associated^ilh tS instJ^nLuon c.'loasurenents of average contaminant should not be averaged over more than 1 square meter. For obiects of «...-r>^. , . should be derived for each such object. ^ [ surface area, the average ^The maxifflun contamination level applies to an area of not more than 100 cm^. «Thc amount of removable radioactive material per 100 cm^ of surface area should be detenalned by wiplnq that ar»a with A^y, tt\*m^ AhsoruMt raper. applying moderate pressure, and assessing the anount of radioactive material on the wipe with an aoDro»pl*Ii 1^^*™°! r kn^.n efficiency. When removable contamination on objects of less surface area Is detemfoed. the pertinent levJlJ ShoSldh! ** proportionally and the entire surface should be wiped. *^ * reduced 'the average and maxirauo radiation levels associated with surface contamtnation resulting from beta-gamna emitters should not •^r- A 0.2 mrad/hr at 1 cm and 1.0 mrad/hr at 1 cm. respectively, measured through not more than 7 minigrams per square centimeter of total absorber. ' • ' INTERNATIONAL URANIUM (USA) CORPORATION DECONTAMINATION FINAL RELEASE I have venfied that tractor NA and/or container Tractor Number , has been checked for any contamination and has been Contamer Number authonzed for final release Radiation Technician Radiaton Department Title Date C \windows\TEMP\decon SOP doc No PBL-9 Rev No R-0 Date Oct 4,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title End Dump Trailer Acceptance, Handling & Release Page 1 of 6 1.0 Purpose The following procedure applies to acceptance, handhng, and release of end dump trailers at the White Mesa Mill (the "Mill") International Uranium (USA) Corporation ("lUSA") receives material for processing, in either bulk or non-bulk packagmg. This procedure addresses one form of bulk packaging - end dump trailers. This procedure may be amended, subject to approval by lUSA's Safety and Environmental Review Panel (SERP), firom time to time as appropnate to address the individual requirements of specific feed materials, or projects. 2.0 Ore Receiving 1. Check truck scale for zero balance at the begiiming of each shift. 2 Wlien each truck driver enters the Restricted Area for the first time, the Scale house operator wall provide hazard training for the driver. The driver will be provided with the Safety Trainmg Form (copy attached) All drivers will be required to read the Safety Trammg Form and sign and date the Safety Training Form indicating that they understand and agree to follow lUSA's safety rules and procedures while on company property The Scale house operator will sign the Safety Training Form as the instructor for lUSA. Completed Safety Training Forms will be turned m to the Safety Department for fiiture reference 3 Inspect all copies of the Bill of Lading (BOL) to ensure that the shipment is destined for the Mill and that all shipping documentation is in order (see Section 8.2) If any discrepancies are noted notify the Mill management immediately. Do not empty the end dump trailer until all paperwork discrepancies are corrected. 4 Assign next available shipment number and Mill load number to the inbound shipment Record the Mill load number, inbound date and both the truck and end dump trailer numbers on the Scale house Weight Ticket (SWT) 5. Enter the loaded weight of the end dump truck and trailer on the SWT. 3.0 Ore Unloading 1 After weighing the truck and trailer, direct the driver to the specified ore storage pad area where the matenal will be unloaded. Pnor to unloading the tarp is inspected for damage and then removed, if necessary The driver is then directed to unload the material, ensuring all persormel are clear of the trailer and the immediate area. 2 After unloading the material replace the tarp, unless the trailer is being decontaminated for unrestncted release P \Admin\Master SOPs\Book 10_PBL Sops\PBL-9\PBL-9 End Dump SOP Rev 0 (10 04 02) doc No PBL-9 Rev No R-0 Date Oct 4,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title End Dump Trailer Acceptance, Handling & Release Page 2 of 6 3. After the tarp has been replaced on the trailer, direct the dnver back to the scales for an empty weight 4 Record the empty weight on the appropriate SWT 5 Use a front-end loader or similar equipment to push matenal into the designated ore lot pile. 4.0 Decontamination and Release of End Dump Trailers and Trucks All end dump trailers and trucks will be decontaminated after unloading prior to leaving the Mill Generators or transporters will notify lUSA whether a specific trailer is to be released for restncted or unrestricted use. Any trailers that are to be released for restricted use will be decontaminated according to the requirements contained in U S Department of Transportation (DOT) Part 49 CFR 173 441(b) and 173 443 (copies attached). Any trailers that are to be released for unrestricted use will be decontaminated according to the requirements found in Table 1 of the Nuclear Regulatory Commission's (NRC's) Pohcy and Guidance Directive FC-85-23, "Guidelines for Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use or Termination of Licenses for Byproduct, Source, or Special Nuclear Material" issued May 1987 (copy attached) Trailers requiring repair wdll be decontaminated for unrestricted release, to facilitate repairs by the transporter at the transporter's own site Trailers may be repaired without undergoing full decontamination if repaired within the Restricted Area of the Mill. 5.0 Decontamination and Release of Equipment for Restricted Use 1 After the tarp has been replaced on the trailer and the empty weight obtained, the dnver will be directed to the decontamination pad. 2 Decontaminate the exterior of each trailer, truck and tires thoroughly, using a high-pressure water wash. 3 After the truck and trailer are decontaminated, the driver will be directed to the gate, along the decontamination route The decontamination route is a graveled roadway specifically designed for decontaminated equipment to exit the Restricted Area If it becomes necessary due to environmental conditions or residual mud m the tires etc., direct the driver to proceed along the decontammation route to the secondary wash station. Wash any visual residual mud off ofthe tkes, or extenor surface of the truck and trailer. Otherwise, direct the driver to proceed along the decontamination route to the tertiary decontamination and final scanning area P \Admin\Master SOPs\Book 10_PBL Sops\PBL-9\PBL-9 End Dump SOP Rev 0 (10 04 02) doc No PBL-9 Rev No R-0 Date Oct 4,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title End Dump Trailer Acceptance, Handling & Release Page 3 of6 6.0 1 Contact a Radiation Technician to perform a radiological contamination survey for restricted release of the truck and trailer If the Radiation Technician indicates areas on the truck or trailer that require fiirthei decontamination, decontaminate those areas as necessary ^ The Radiation Technician or RSO will scan the trailer, truck, and tires m various locations as shown on the Eqmpment Survey for Restricted Release (copy attached) and document the scan readings on the Equipment Survey for Restricted Release. The contamination survey will be perfomied using appropriate radiological instrumentation for total activity in accordance with DOT transportation regulations. The release standards to be met for restricted release are contained m U S Department of Transportation (DOT) Part 49 CFR 173 441(b) and 173 443 (copies attached). If the trailer, truck or tires do not meet the radiological release survey requirements or shows visually observable contamination, the truck and trailer will either be returned to the secondary decontamination pad for fiirther decontamination or will be washed again at the tertiary decontamination area The Radiation Technician or RSO will fill out the Equipment Survey for Restricted Release form (copy attached) to document that the truck and trailer has been authonzed for release for restricted use. These forms are filed in the Radiation Department. The Radiation Techmcian or RSO will place a white sticker on the trailer that says, "EMPTY" and "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive material, excepted package - empty package, UN2910" After a truck and trailer have been released, the driver will perform a visual inspection of the truck, trailer and tires Leaving his truck outside of the Restricted Area, the driver will retum to the Scale House to pick up the documentation for the empty trailer Decontamination and Release of Equipment for Unrestricted Use After the empty weight of the trailer has been obtained, the driver will be directed to the decontamination pad. The tarp will not be replaced on the trailer or, if necessary, the tarp shall be removed. Open the trailer tailgate, elevate the trailer ensunng that there are no overhead hazards and decontaminate the trailer using a high-pressure water wash Make sure to thoroughly wash the inside and outside of the trailer. The tmck and tires shall also be washed. P \Admin\Master SOPs\Book 10_PBL Sops\PBL-9\PBL-9 End Dump SOP Rev 0 (10 04 02) doc No PBL-9 Rev. No. R-0 Date Oct 4,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title' End Dump Trailer Acceptance, Handlmg & Release Page 4 of 6 After the truck and trailer are decontaminated, the driver is directed to follow the decontamination route The decontamination route is a graveled roadway specifically designed for decontaminated equipment to exit the Restncted Area If It becomes necessary due to environmental conditions or residual mud in the tires etc, the driver is instructed to proceed along the decontamination route to the secondary wash station Wash any visual residual mud off of the tires, or exterior surface of the container Otherwise, the dnver is instructed to proceed along the decontammation loute to the tertiary decontamination and final scanning area. Contact a member of the Radiation Department staff to conduct the appropnate radiological survey for unrestricted release of the tmck, trailer and tires The release standards to be met for unrestricted release are contained in Table 1 ofthe Nuclear Regulatory Commission's (NRC's) Policy and Guidance Directive FC- 85-23, "Guidelines for Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use or Termination of Licenses for Byproduct, Source, or Special Nuclear Material" issued May 1987 (copy attached). The RSO will prepare a memorandum detailing the applicable standard on Table 1 for each project The RSO will also provide die training of the Radiation Technicians required The Radiation Technician will perform a radiological contammation survey of the truck and trailer. If the Radiation Technician indicates areas that require fiirther decontamination, decontammate those areas as necessary If the tmck, trailer and tires meet the radiological release survey and visual inspection requirements, the Radiation Technician will place a red sticker on the trailer that says, "THIS CONTAINER HAS BEEN FULLY DECONTAMINATED AND SURVEYED FOR "UNRESTRICTED USE" BY- (FILL IN NAME OF RADIATION TECHNICIAN)" The RSO or Radiation Technician that performed the release survey will then sign the red sticker and date It. In addition, the RSO or Radiation Techmcian will fill out a Decontamination Final Release Form (copy attached) to document that the tmck and trailer have been cleared for unrestricted release. The Decontamination Release Form will be turned in to the Mill Admimstration Office daily for filmg and distribution After a tmck and trailer have been released, the driver will do a visual inspection of the tmck and trailer. Leaving his truck outside of the Restricted Area, the driver will retum to the Scale House to pick up the documentation for the empty trailer P \Admin\Master SOPs\Book 10_PBL Sops\PBL-9\PBL-9 End Dump SOP Rev 0 (10 04 02) doc No PBL-9 Rev No R-0 Date: Oct 4,2002 INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title End Dump Trailer Acceptance, Handling & Release Page 5 of 6 7.0 Hazard Identification and Safety 7 1 Required Personal Protective Equipment (P?E) In all areas of the Mill covered by this procedure, hard hats, safety glasses and steel-toed shoes are required at a minimum. These must be worn in all areas of the Mill with the exception of the Administration Building 7.2 Industrial Hazards and Safety 1 Use caution when the trailers are backing onto the Ore Pad 2 Ensure that all persormel within 50 feet of the area where the end dump trailer are aware that unloading is about to commence. Move at least 25 feet away from the rear of the tiailer during the initial unloading operation 3 Dnvers must use caution dunng the imloading process and be aware of any overhead hazards ^ 4 Do not place any part of your body mside the trailer when the trailer is being tipped and the tailgate is open Only work around the tailgate after it has been properly blocked open 5 Be aware of high-pressure wash water 6. Be aware of slippery conditions on the ore pad during periods of inclement weather \ 1 Be aware of the potential for ice build-up on and around the decontamination pad - during periods of cold weather. 8 Use caution when entering or exiting equipment Be sure to use the ladders and hand rails Do not jump off of the equipment. 9 Always use a ladder when entenng and/or exiting the interior of an end dump trailer. 8.0 Paperwork Tracking 1. Each trailer will have a umque sequential project number assigned to it at the generating facility This number will be entered onto the Bill of Lading (BOL) and attached to the trailer prior to shipment from the generation site P \Admin\Master SOPs\Book 10__PBL Sops\PBL-9\PBL-9 End Dump SOP Rev 0 (10 04 02) doc INTERNATIONAL URANIUM (USA) CORPORATION STANDARD OPERATING PROCEDURES Title End Dump Trailer Acceptance, Handling & Release No PBL-9 Rev. No R-0 Date Oct 4,2002 Page 6 of 6 Upon amval at the Mill, the tmck driver wall turn in all of his/her paperwork to the Scale House operator who will verify that the BOL number, trailer number and project number assigned to the shipment match on all copies of the BOL, The Scale House operator wall also verify that the actual trailer number matches the BOL Trailer Number If there are any discrepancies in any of the numbers notify Mill management immediately. Only original paperwork will be accepted If the original paperwork does not come with the trailer, notify Mill management immediately. The Scale House operator will sign the BOL, acknowledging receipt of tiie matenal at the Mill, if all of the paperwork is in order Depending on contractual and/or sampling requirements, final acceptance or rejection of certain altemate feed maten^s may be contingent on analytical results Each trailer wall be transported across the scale at the Mill prior to and after bemg unloaded The appropriate information will be entered into the project database All copies of the SWTs and BOLs will be forwarded to the Mill Records Manager on a daily basis or other frequency specified by Mill Management, from time to time The Mill Records Manager will compile and reconcile tiie BOL's and SWTs for distribution P \Admin\Master SOPs\Book 10_PBL Sops\PBL-9\PBL-9 End Dump SOP Rev 0 (10 04 02) doc SAFETY TRAINING FOR ALTERNATE FEED DELIVERY PERSONNEL Welcome to International Uranium (USA) Corporation's, White Mesa Mill In order to assure your safety while on our property, we would like to acquaint you with the safety mles and procedures, which you wall be required to follow while on our property. 1.0 General Safety 1 Approved hard hats and safety glasses are reqmred at all times except when inside the cab of your truck 2 This is a smoke free facility No smoking is allowed on the property Eating anything, drinking, chewing candy, gum or tobacco is also not allowed in .the Mill restricted area due to radiation hazards 3 All mobile equipment will not exceed a speed limit of 5 miles per hour 4 Be aware of the possibility of a tmck turning over while dumping Ensure that the tmck IS on level ground and biakes are set prior to dumping 5 Check for potential overhead hazards pnor to dumping 6 If matenal is hung up in the trailer bed, it is not permissible to work in the bed while it is m the dump position If it is necessary to get m the bed of the trailer to free a hang up, the bed must be lowered 7 Be aware of slippery conditions on the ore pad during penods of inclement weather 8 Be aware of the potential for ice build-up on and around the decontamination pad during periods of cold weather 9 Use caution when entering or exiting equipment * 2.0 Radiation Safety 1 All drivers are required to scan for alpha radiation prior to leaving the Mill restncted area 2. All eqmpment, i e trucks and trailers, will be scaimed for radiation prior to leaving the Mill's restricted area Driver (Pnnted) - Scale House Operator Driver (Signature) Date P \Admin\Master SOPs\Book 10_PBL Sops\PBL-9\PBL-9 End Dump SOP Att A (10 04 02) doc , WAi!> Liocument Hemevai nnp.//irweogateaccess.gpogov/cgi*oin/g..winuc-nyoemivi-^i/JACACUinjiH-mlo&i irc- [Code of Federal Regulations] (Title 49, Volume 2, Parts 100 to 185] [Revised as of October 1, 1999] From the U.S. Goverrunent Printing Office via GPO Access [CITE: 49CFR173.441] [Page 582-583] TITLE 49—TRANSPORTATION { ' CHAPTER I—RESEARCH AND SPECIAL PROGRAMS ADMINISTRATION, DEPARTMENT OF i TRANSPORTATION, ^ PART 173—SHIPPERS—GENERAL REQUIREMENTS POR SHIPMENTS AND PACKAGINGS—Table of Cont Subpart I—Class 7 (Radioactive) Materials Sec. 173.441 Radiation level limitations. \ (a) Except as provided in paragraph (b) of this section, each package of Class. 7 (radioactive) materials offered for transportation must be designed and prepared for shipment, so that under conditions normally incident to transportation, the radiation level does not exceed 2 mSv/hour (200 mrem/hour) at any point on the external surface of the package, and the tralnsport index does not exceed 10. [[Page 583]] (b) A package which exceeds the radiation level limits specified in paragraph (a) of this section must be transported by exclusive use shipment, and the radiation levels for such shipment may not exceed the following during transportation: (1) 2 roSv/h (200 mrem/h) on the external ,surface of the package unless the following conditions are met, in which case the limit is 10 mSv/h (1000 mrem/h):' ' (1) The shipment is made in a closed transport vehicle; (ii) The package is secured within the vehicle so that its position remains fixed-during transportation; and \ (iii) There are no loading or unloading operations between the beginning and end of the transportation; (2) 2 mSv/h (200 mrem/h) at any point on the outer surfaces of the vehicle, including the top and underside of the vehicle; or in the case of a flat-ted style vehicle, at any point on the vertical planes projected from the outer edges of the vehicle, on the upper surface of the load or enclosure if used, and on the lower external surface of the vehicle; ^ (3) 0.1 mSv/h (10 rarem/h) at any point 2 meters (6.6 feet) from the outer lateral surfaces of the vehicle (excluding.the top and underside of the vehicle); or in the case of a flat-bed style vehicle, at any point 2 meters (6.6 feet) from the vertical planes projected by the outer edges of the vehicle (excluding the top and underside of the vehicle); and (4) 0.02 mSv/h (2mrem/h) in any normally occupied space, except that this provision does not apply to carriers if they operate under the provision^ of a State or federally regulated radiation protection program and if personnel under their control who are in such an occupied space wear radiation dosimetry devices. (c) For shipments made under the provisions of^ paragraph (b) of this section, the offeror shall provide specific written instructions for maintenance of the exclusive use shipment controls to the carrier. The instructions must be included with the shipping paper information. The instructions must be sufficient so that, when followed, they, will cause the carrier to avoid actions that will unnecessarily delay delivery or unnecessarily result in increased radiation levels or radiation exposures to transport workers or members of the general public. WAIS Document Retrieval ^ httpi/Zfrwebgatcaccess gpo gov/cgi.bm/g...irnTLE"49&PART»173&SECTION»441&TYPE=TI (d) Packages exceeding the radiation level or transport index ' prescribed in paragraph (a) of this section may not be transported by aircraft. (Amdt. 173-244, 60 FR 50307, Sept. 28, 1995, as amended at 63 FR 48568, Sept. 10, 1998] WAIS Document Retneval http//frwebgare.access gpo.gov/cgl-bm/g t?TlTLE"^9&PART^173&SECTION«»«443&TYPE'»Tl [Code of Federal Regulations] [Title 49, Volume 2, Parts 100 to 185] [Revised as of October 1, 1999] Prom the U.S. Government Printing Office via GPO Access [CITE: 49CFR173.443] [Page 583-584] TITLE 49—TRANSPORTATION CHAPTER I—RESEARCH AND SPECIAL PROGRAMS ADMINISTRATION, DEPARTMENT OP TRANSPORTATION PART 173—SHIPPERS—GENERAL REQUIREMENTS FOR SHIPMENTS AND PACKAGINGS—Table of Cont Subpart I—Class 7 (Radioactive) Materials Sec. 173.443 Contamination control. (a) The level of non-fixed (removable) radioactive contamination on the external surfaces of each package offered for transport must be kept as low as reasonably achievable. The level of non-fixed radioactive contamination may not exceed the limits set forth m table 11 and must be determined by either: (1) Wiping an area of 300 square centimeters of the surface concerned with an absorbent material, using moderate pressure, and measuring the activity on the wiping material. Sufficient measurements must be taken in the most appropriate locations to yield a representative assessment of the non-fixed contamination levels. The amount of radioactivity measured on any single wiping material, when averaged over the surface wiped, may not exceed the limits set forth in table 11 at any time during transport; or (2) Using other methods of assessment of equal or greater efficiency, m which case the efficiency of thfe method used must be taken into account and [[Page 584]] the non-fixed contamination on the external surfaces of the package may not exceed ten times the limits set forth in table 11, as follows: Table 11—Non-Fixed External Radioactive Contamination-Wipe Limits Maximum permissible limits Contaminant Bq/cm<SUP>2</SUP> uCi/cm<SUP>2</SUP> Beta and gamma emitters and low toxicity 0.4 10<SUP>-5</SUP> 22 alpha emitters All other alpha emitting radionuclides.. 0.04 10<SUp>-6</SUP> 2.2 (b) Except as provided m paragraph (d) of this section, in the case of packages transported as exclusive use shipments by rail or public highway only, the removable (non-fixed) radioactive contamination on any package at any time during transport may not exceed ten times the levels prescribed in paragraph (a) of this section. The levels at the beginning of transport may not exceed the levels prescribed in paragraph (a) of this section. (c) Except as provided in paragraph (d) of this section, each transport vehicle used for transporting Class 7 (radioactive) materials as an exclusive use shipment that utili2es the provisions of paragraph (b) of this section must be surveyed with appropriate radiation detection instruments after each use. A vehicle may not be returned to service until the radiation dose rate at each accessible surface is WAIS Document Retrieval http'/Zfrwebgate access gpo.gov/cgi-bm/g i7nTLE"M9&PART"173&SECnON"443&TYPE'=Tl 0.005 mSv per hour (0.5 mrem per hour) or less, and there is no significant removable (non-fixed) radioactive surface contamination as specified in paragraph (a) of this section. (d) Paragraphs (b) and (c) of this section do not apply to any closed transport vehicle used solely for the transportation by highway or rail of Class 7 (radioactive) material packages with contamination levels that do not exceed 10 times the levels prescribed in paragraph (a) of this section if— (1) A survey of the interior surfaces of the empty vehicle shows that the radiation dose rate at any point does not exceed 0.1 mSv per hour (10 mrem per hour) at the surface or 0.02 mSv per hour (2 mrem per hour) at 1 meter (3.3 feet) from the surface; (2) Each vehicle is stenciled with the words '*For Radioactive Materials Use Only*' in letters at least 76 millimeters (3 inches) high in a conspicuous place on both sides of the exterior of the vehicle; and (3) Each vehicle is kept closed except for loading or unloading. [Amdt. 173-244, 60 FR 50307, Sept. 28, 1995, as amended by Amdt. 173- 244, 61 FR 20753, May 8, 1996] GUIDELINES FOR DECONTAMINATION OF FAdLITIBS AND EQUIPMENT PRIOR TO RELEASE FOR UNRESTRICrTED USB OR TERMINATION OF UCENSES FOR BYPRODUCT, SOURCE, OR SPECIAL NUCLEAR MATERIAL U.S. Nuclear Regulatory Commission Division of Fuel Cycle, Medical, Academic, and Commercial Use Safety Washington, DC 20555 April 1993 The instructions in this guide, in conjunction with Table 1, spedfy the radionuclides and radiation exposure rate limits which sboidd be used in decontamination and survey of surfeces or premises and equipmrat prior to abandonment or release for uniestiicted use. The limits in Tfblt 1 do not apply to premises, equipment, or scrap containing induced radioactivity for which the radiological considerations pertinent to their use may be different. The release of such facilities or items from regulatory control is considered on a cas&-by-case basis. 1. The licensee shall make a reasonable effort to eliminate residual contamination. 2. Radioactivity on equipment or surfaces shall not be coveted by paint, plating, or otiier covering material unless contamination levels, as determined by a survey and documented, aie bdow the limits specified in Table 1 prior to the application of die covering. A reasonable effort must be made to minimize the contamination prior to use of any covering. 3. The radioactivity on die interior sur£u;es of pipes, dram lines, or ductwork shall be determined by making measurements at all tn^s, and other appropriate access points, provided that contamination at these locations is likely to be rqnesentative of contamination on the interior of die pipes, drain lines, or ductwork. Surfeces of premises, equipment, or scrap which are likely to be contaminated but are of such size, constmction, or location as to make the surfiEice inaccessible for purposes of measurement shall be presumed to be contaminated in excess of die limits. 4. Upon request, Uie Commission may autiioiize a licensee to relinquish possession or control of premises, equipment, or scrap having surfaces contaminated with materials in excess of the limits specified. This may include, but would not be limited to, special circumstances such as razmg of buildmgs, transfer of premises to another oxganization continuing work with radioactive materials, or conversion of facilities to a long-term storage or standby status. Such requests must: a. Provide detailed, specific information describing the premises, equipment or scrap, radioactive contaminants, and the nature, extent and degree of residual'sur&ce contamination. b. Provide a detailed health and safety analysis which reflects that the residual amoimts of materials on surface areas, together with other considerations such as prospective use of the premises, equipment, or scrap, are unlikely to result in an unreasonable risk to the healtii and safety of the public. 5. Prior to release of premises for unrestricted use, the licoisee shall make a comprehensive radiation survey which establishes that contamination is witiiin die limits specified in Table 1. A copy of die survey report shall be filed witii tiie Division of Fuel Cycle Safety and Safeguards, U.S. Nuclear Regulatory Commission, Washington, D.C. 20555, and also the Administrator of the NRC Regional Office haviog jurisdiction, llie reports should be filed at least 30 days prior to Uie planned date of abandonment. The survey report shall: a. Identify the premises. b. Show Uiat reasonable effort has be^ made to eliminate residual contamuiation. c. Describe Uie scope of the survey and general procedures followed. d. State Uie findings of the survey in units specified in the instmctions. Following review of tiie report, the NRC will consider visiting Uie facilities to confirm the survey. •to TABLE 1 ACCEPTABLE SURFACE CONTAMINATION LEVELS NUCUDES* AVERAGE?" MAXIMUM^*' REMOVABLE^*' U-nat, U-235, U-238, and associated decay products Transuranics, Ra-226, Ra-228, Th-230, ni-228, Pa-231, Ac-227, M25,1-129 Hi-nat, Th-232, Sr-90, Ra-223, Ra-224. U-232,1-126,1-131, 1-133 Beta-gamma enutters (nuclides with decay modes other than alpha enn^on or spontaneous fission) ejicept Sr-90 and ofbisrs noted above 5,000 dpm a/lOO cm' 100 dpna/100 cm* 1,000 dpm/100 can* 5,000 dpm /?yi00 cn^ 15,0CK) dpm ce/lOO cn^ 300 dpm/lOO cm* 3,000 dpm/lOO cn^ 15,000 dpm fiyflOO cm* 1,000 dpm a/100 cm* 20 dpm/lOO cm* 200 dpm/lOO cm* 1,000 dpm J87/IOO cnr* Where suiface contamination by both alalia- and beta-ganmia-emitting nnchdes exists, the limits established for alpha- and beta-gamna-emitting nuclides ^ould i^l^ ind^pendenUy. As used in diis table, d^ (disint^rations per nnnute) means the rate of emission by radioactive material as determined by correcting the counts per minute observed by an appropriate detector for background, efficiency, and geometric factors assodated \^th fhe instrummtation. Measurements of average contaminant should not be averaged over more than 1 square meto* For objects of less surface area, flie average should be derived finr eadi such object. The maximum contandnation level i^lies to an area of not more than 100 cm*. The amount of xemovable radioactive matensi per 100 cm* of surfece area should be determined by wiping that area with dry filter or soft absorbent papNt applying moderate pressure, and assessing the amount of radioactive material on the vnpt with an appropriate instrnmoit of known effvAeocy. When removable contamination on objects of less surfoce area is determmed, the pertinent levels should be reduced proportionally and fbe> oatibre surface should be wiped. The avoage and maximum radiation levels associated with surfiice contammation resnltmg from beta-gamma emitters should not exceed 0 2 mrad/hr at 1 cm and 1 0 mrad/hr at 1 cm, respectively, measured tfarongfa not more than 7 milligrams per square cratimeter of total absorber. IBiBI International Uranium (USA) Corporation Equipment Survey for Restricted Release Date Contamer ID: Surveyed By Outside Locations Location # 24 25 26 27 28 29 30 31 32 33 34 35 36 37 Ralls instrument Data Total Alpha/ Beta/Oantma Model # SN Cal Date Source Efficiency Total Alpha/ Beta-Oamma cpm Truck and Tire Survey 0 0 00 00 00 00 Total Alpha/ Bata-Camma Location # cpm 1 2 3 4 5 6 Truclc Ext TRAILER TIRES 7 9 11 00 00 00 00 00 00 Total Alpha/ Beta-Oamma Location # cpm 10 12 7 8 9 10 11 12 Chassis Ext PBL-9 (10 04 02) END DUMP(b) xls International Uranium (USA) Corporation Equipment Survey for Unrestricted Release Date Container ID. Inside Locations Locatioii # 1 2 3 4 5 6 7 B 9 10 11 12 13 14 15 16 17 18 19 Front 19 L Side 13 14 23 15 16 R Side 17 18 7 8 22 9 10 21 11 12 1 2 3 4 5 6 20 Tailgate Total Alpha dpm/IOOcm' Removable Alpha dpm/IOOcm* Surveyed By Outside Locations dpm/IOOcm* Location # 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 Rails Total Alpha dpm/1 OOcm* Removable Alpha dpm/IOOcm* iny locelion exceeds 1000 dpm/100 cm2 total elpto, a swearAvipe survey (or removabte elptia must be perfonned /ever, eddUonat removable apths t\Nfpes aKIwuglt not required may be performed Instrument Data Total Alpha Instrument E5P-1 / AC-3 SN 02299 / 1 02286 / 2 Cal Date Function Check(5x1 mm) Th 230 @ 30300 dpm BKg Average Dpm Average Removaltle Alpha Model SN Cal Date Function Check (5x1 mm) Alpha Bkg Ave Alpha eff Alpha Faclor Tota/ Beta/Qamma Model it SN [ Cal Date Source Efficiency Truck and Tire Survey 1 0 02 3 00 004 5 00 OOe Total Alpha/ Beta-Gamma •ocatlon cpm Truck Ext TRAILER TIRES 7 GO OOs 9 00 O0io 11 00 O0i2 Total Alpha/ Beta-Gamma Locatipn cpm 10 11 12 Chassis Ext PBL-9 (10 04 02) END DUMP(a) xls (• # INTERNATIONAL URANIUM (USA) CORPORATION DECONTAMINATION FINAL RELEASE I have verified that tractor NA and/or container Tractor Number has been checked for any contamination and has been Contamer Number authonzed for final release Radiation Technician Radiaton Department Title Date C \wmdows\TEMP\decon SOP doc Type A Packaging Cenillcatlon SKOLNIK xhibit 11 2A - Type A Test Report Revision 03 Revision Date 17 July 2009 TESTING PERFORMED BY SKOLNIK INDUSTRIES. INC CQ5506 TESTING LAB - AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 10-090 TYPE A TEST REPORT DRAWING NUMBER CQ5506 Rev /\2 MATERIAL Carbon Steel UN RATING SOLIDS 1A2/X435/S UN RATING LIQUIDS 1/\2/Y1 5/150 DRUM TYPE Open Head THICKNESS 0 0433"-0 0480" (18 GA) RING 12 GA (RBH2212) CAPACITY 55 Gallon NUT/BOLT TYPE 5/8"-11 UNCx4" INSIDE DIAMETER 22 5" GASKET "D" - EPDM (GE5500) OVERALL HEIGHT 34 75" CLOSING INSTRUCTIONS PQ 080 Rev C ROLLING HOOPS 3 FITTINGS 2" & 3/4" Rieke CHIME TYPE Round Chime NUCLEAR VENT None SEAM CONSTRUCTION Lap Weld TESTING IS PERFORMED USING SURROGATE CONTENTS SOLIDS (SMALL PARTICLE SIZE) Sodium Bicarbonate. Sand, Flour, Fluorescein Dye SOLIDS (HEAVY BULKY MATERIAL) Lead Blocks. Steel Plate, Inner Steel Drum GROSS MASS OF TESTED DRUM 960 lbs EACH DRUM SHALL BE INSPECTED FOR CONFORMANCE TO 49CFR § 173 462 AND SOP 11 2 SECTION 4 0 DOES EACH DRUM CONFORM TO THE REQUIRED PRE-TESTING INSPECTION'? Yes This report ensures that Skolnik Industries, Inc has successfully performed the Type A Packaging Tests as descnbed in 49 CFR § 173 465 using sunrogate contents and that all requirements of 49 CFR § 173 462 were met pnor to testing This packaging is capable of withstanding, without aipture or leakage, the vibration standard in 49 CFR § 178 608 (49 CFR § 173 410(f)) This packaging has been tested according to 49 CFR § 178 605 to support compliance with 49 CFR § 173 412(f), results are listed within this report Skolnik Industnes, Inc does not, and cannot, certify this packaging as a DOT 7A Type A Package, it is the responsibility of the packager / shipper to certify that the package meets all of the applicable requirements Customer must be aware of subsequent Type A requirements including, but not limited to the following 49 CFR §172 310 Class 7 (radioactive) matenals 49 CFR §178 2 Applicability and responsibility 49 CFR §178 350 Specification 7A, general packaging, Type A Additional information on this subject can be found within DOT clanfication letter Ref No 05-0074 and DOE Office of Transportation Regulatory and Legislative Development Highlights Issue Number EM/OT-001 dated November 2005 PERFORMED BY APPROVED BY STGNATURE Moises Basilio/Quality Assurance Tech PRINTED NAME / TITLE Matt Dick/Manager of Quality Assurance PRINTED NAME / TITLE SKolnik Industnes Inc 4900 S Kilboum Avenue Chicago, IL 60632-4593 USA 773 735 0700 Page 1 of 8 SKOLNIK Oruma of Stcd xhibit 11 2A - Type A Test Report Revision 03 Revision Date 17 July 2009 PART NUMBER CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES, INC TESTING LAB - AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT ID NUMBER 10-090 TYPE A PACKAGING TESTS 49CFR § 173.465 DATE 7/7/2010 TIME 7 45 AM TEST SEQUENCE # 1 SPRAY DURATION 1 Hour SOAK DURATION 2 Hours RESULT No Loss of Contents s BC Q TEST RESULT PHOTOGRAPHS I- ^ LZ IO o. Ui (09 ec €C UJ u. Drum #1 was closed to a torque of 60 ft-lbs and a nng gap of 0 426 inches Contents of Drunns #1 and #2 used for testing Heavy Bulky Matenal Lead Blocks, Steel Plate, Compacted Inner Drum Contents of Drums #1 and #2 used for testing Small Particle Size Sodium Bicarbonate, Sand Flour, Fluorescein Dye Drum #1 was sprayed with water for one hour to simulate exposure to rainfall at a rate of at least 2" per hour Drum #1 was allowed to set for a penod of 2 hours so that the water has soaked into the maximum extent No loss of contents was observed due to the water spray test of49CFR§ 173 465(b) Skolnik Industries Inc 4900 S Kilboum Avenue Chicago IL 60832-4593 USA 773 735 0700 Page 2 of 8 SKOLNIK Drums of Steel Exhibit 11 2A - Type A Test Report Revision 03 Revision Date 17 July 2009 mMmmmm^m CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES, INC TESTING LAB-AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT 10-090 TEST SEQUENCE # RESULT CQ5506 is not capable of preventing loss of content dunng 49CFR 173 465(c)(2) and (c)(1) MAXIMUM TOP CRUSH PATTERN MAXIMUM BOTTOM CRUSH PATTERN CQ5506 IS not capable of preventing loss of content dunng the senes of testing as discnbed in 49CFR 173 465(c)(2) and 49CFR 173 465(c)(1) This test was perfomed on 7/7/2010 resulting in loss of contents Additional information is available upon request Skolnik Industnes, Inc 4900 8 Kilboum Avenue Chicago, IL 60632-4593 USA 773 735 0700 Page 3 of 8 SKOLNIK Drums of Scool hibit 11.2A - Type A Test Report Revision 03 Revision Date 17 July 2009 PART NUMBER CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES, INC TESTING LAB - AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT ID NUMBER 10-090 TYPE A PACKAGING TESTS 49CFR § 173.465 DATE 7/7/2010 TIME 11 10 AM TEST SEQUENCE # 3 DROP HEIGHT 4 feet RESULT No Loss of Contents RU I M # : M/0<IMUM TOP CRUSH PATTERN 16 00" x 5 50" MAXIMUM BOTTOM ' CRUSH PATTERN N/A O TEST RESULT PHOTOGRAPHS (0 u 0. "* " (09 UJ UJ £ ^ o Drum #1 was dropped from a height of 4 feet onto Drum #1 was dropped to cause the maximum amount of the drum/nng/bolt assembly damage to the safety features being tested ' * \ — • • Visible damage was observed due to the 4 foot drop No loss of content was observed due to this senes of onto the assembly of Drum #1, crush pattem of tests that were performed on Drum #1 16 00" X 5 50" Skolnik Industries Inc 4900 S Kilboum Avenue Chicago, IL 60632-4593 USA 773 735 0700 Page 4 of 8 SKOLNIK Drums of Stoo4 xhibit 11.2A - Type A Test Report Revision 03 Revision Date 17 July 2009 PART NUMBER CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES, INC / TESTING LAB - AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT ID NUMBER 10-090 TYPE A PACKAGING TESTS 49CFR § 173.465 DATE 7/7/2010 TIME 12 45 PM TEST SEQUENCE # 1 CM SPRAY DURATION 1 hour SOAK DURATION 2 hours RU M RESULT No Loss of Content O TEST RESULT PHOTOGRAPHS a. ^ (0 (09 CC €C 1$ Drum #2 was closed to a torque of 60 ft-lbs and a Drum #2 was allowed to set for a penod of 2 hours so nng gap of 0 451 inches Drum #2 was sprayed with that the water has soaked into the maximum extent No water for one hour to simulate exposure to rainfall at loss of contents was observed due to the water spray test a rate of at least 2" per hour of 49CFR § 173 465(b) Skolnik Industnes inc 4900 S Kilboum Avenue Chicago, IL 60632-4593 USA 773 735 0700 Page 5 of 8 SKOLNIK Drums of Seed Exhibit 11 2A - Type A Test Report Revision 03 Revision Date 17 July 2009 PART NUMBER CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES, INC TESTING LAB - AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT ID NUMBER 10-090 TYPE A PACKAGING TESTS 49CFR § 173.465 CN s O DATE 7/8/2010 COMPRESSIVE LOAD CALCULATION 5 X GROSS MASS = TIME 4796 lbs 6 30 AM TEST SEQUENCE # 13(kPa)x TT(0 D /2)'^2 = 933 lbs USE THE GREATER OF THE CALCULATED LOADS TEST DURATION 24 hours with a load of at least 4796 lbs OD = OUTSIDE DIAMETER RESULT No Loss of Contents TEST RESULT PHOTOGRAPHS m IO IU <s S *ot < u. H- O CO 0> A compressive load of at least 4796 lbs was applied The overall height of Drum #2 pnor to performing the uniformly to two opposite sides of Drum #2 for at stack test was 34 75" least 24 hours The overall height of Drum #2 after the 24 hour No loss of content occunred dunng the stack test The penod of the stack test was 34 75", no defomriation O D was approximated at 25" for the compressive load of Drum #2 occurred calculation Skolnik Industries Inc 4900 S Niboum Avenue Chicago IL 60632-4593 USA 773 735 0700 Page 6 of 8 SKOLNIK Oroms of Stcol Exhibit 11.2A - Type A Test Report Revision 03 Revision Date 17 July 2009 PART NUMBER CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES, INC TESTING LAB - AKA "SDCC 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT ID NUMBER 10-090 TYPE A PACKAGING TESTS 49CFR § 173.465 s CC a DATE 7/7/2010 PENETRATION BAR DIAMETER 1 252" VERIFICATION TIME 11 00 AM TEST SEQUENCE # 2_ MASS 16 53 lbs 49CFR § 173 465(e)(1) 1 25(in) 49CFR § 173 465(e)(1) 13 2(lbs) DROP HEIGHT 3 3 feet from the lowest point of the penetration bar to the point of impact RESULT No Loss of Contents TEST RESULT PHOTOGRAPHS ill z o p cc li. o P Drum #1 was placed onto a ndged, flat, honzontal surface The penetration bar was dropped from a height of 3 3 feet This drop was performed at two locations on Drum #1 Drop 1 on the cover created a dent that was 1 750" in diameter and 0 324" deep Drum #1 was then placed onto its side for drop 2 that was performed on the body of the drum The penetration bar was dropped from a height of 3 3 feet This drop created a dent that was 4 25" in diameter and 0 142" deep No loss of content occurred due to this series of tests Skolnik industnes Inc 4900 S Kiiboum Avenue Chicago IL 60632-4593 USA 773 735 0700 Page 7 of 8 SKOLNIK Drums of Stoo) Exhibit 11 2A - Type A Test Report Revision 03 Revision Oate 17 July 2009 PART NUMBER CQ5506 TESTING PERFORMED BY SKOLNIK INDUSTRIES. INC TESTING LAB - AKA "SDCC" 4900 S Kilboum Avenue Chicago, Illinois 60632 TYPE A TEST REPORT ID NUMBER 10-090 TYPE A PACKAGING TESTS 49CFR § 173.465 IO I CO « S 3 tc o DATE 6/28/2010 TIME 10 00 AM TEST SEQUENCE # TEST PRESSURE 150 kPa DURATION 5 minutes once the test pressure is achieved RESULT No Loss of Contents TEST RESULT PHOTOGRAPHS Drums #3, #4. and #5 were closed to a torque of 60 No loss of contents was observed dunng this sequence ft-lbs and a nng gap of 0 230", 0 309", and 0 330" of testing Hydrostatic testing was performed in accordance With 49CFR 178 605 to support compliance with 49CFR 173 412(f) The drums were filled with water to a test pressure of 150 kPa for a duration of 5 minutes DESCRIPTION ID/SERIAL NUMBER DUE DATE 1- 6" Caliper 6398978 May-2011 Ui IU 1- K alf Z Pressure Gauge DPG-1 May-2011 ^ 111 OS Torque Wrench 33498 May-2011 ME A S U R EQ U I Torque Wrench 990 May-2011 ME A S U R EQ U I Measunng Tape 12 ft N/A Scale 140154 May-2011 Skolnik Industries Inc 4900 S Kilboum Avenue Chicago IL 60632-4593 USA 773 735 0700 Page 8 of 8 other Supporting Pocnmontatlon Page 1 of 2 Boyd Imai - Fwd: ChangelBf Titles and Contact Infor Ation for Energy Fuels Resources (USA) Inc. From: Ryan Johnson To: Imai, Boyd Date: 9/17/2012 9:55 AM Subject: Fwd: Changes of Titles and Contact Information for Energy Fuels Resources (USA) Inc. Ryan Johnson, P.G. Environmental Scientist/Health Physicist Utah Division of Radiation Control . »> Phillip Goble 8/15/2012 12:48 PM »> Thought you'd be interested. >» David Frydenlund <DFrydenlund@energyfuels.com> 8/15/2012 12:32 PM »> Phil, Further to our call yesterday morning, this is to confirm that Denison Mines (USA) Corp changed its name to Energy Fuels Resources (USA) Inc effective July 25,2012 The name has changed, but the entity remains the same Also, some changes have been made in the titles of certain personnel The following table sets out the current titles and contact information forthe key personnel that DRC corresponds with on a regular basis regarding White Mesa Mill matters Name Current Title Comments Email Address Direct Telephone Number Stephen P Antony President and Chief Executive Officer santonv(5)ener6vfuels com (303) 974-2142 Harold R Roberts Executive Vice President and Chief Operating Officer hroberts@energvfuels com (303) 389-4160 David C Frydenlund Senior Vice President, Regulatory Affairs and General Counsel dfrvdenlund(5)energvfuels com (303) 389-4130 Jo Anns Tischler Director, Compliance itischlerpenerevfuels com (303) 389-4132 KathermeA Weinel Quality Assurance Manager (No Change to Title) kweinel@ener6vfuels com (303) 389-4134 Daniel L Hillsten Mill Manager (No Change to Titie) dhillsten^energvfuels com (435) 678-4105 David E Turk Manager, Environmental, Health and Safety dturk@energvfuels com (435) 678-4113 Ronnie B Nieves Mill Radiation Safety Officer rnieves@energvfuels com (435) 678-4114 Jaime J Massey Environmental Compliance Assistant (No Change to Title) imassev@energvfuels com (303) 389- 4167 file://C:\Documents and Settings\Blmai\Local Settings\Temp\XPGrp... 9/17/2012 Page 2 of 2 Effective August 20, 2012, Energy Fuels Resources (USA) Inc will be moving its offices to the following address Energy Fuels Resources (USA) Inc 225 Union Blvd , Suite 600 Lakewood, CO 80228 The mam phone number will continue to be (303) 628-7798 The fax number will continue to be (303) 389-4125 Please let me know if you have any questions, or require any further information Dave David Frydenlund Vice President, Regulatory Affairs, Counsel and Corp Secretary Energy Fuels Resources (USA) Inc. t 303-389-4130 |f 303-389-4125 1050 17th Street, Suite 950 Denver, CO, US, 80265 http //www energyfuels com This e-mail is intended for the exclusive use the of person(s) mentioned as the recipient(s) This message and any attached files with it are confidential and may contain privileged or propnetary information If you are not the intended rec!pient(s) please delete this message and notify the sender You may not use, distribute print or copy this message if you are not the intended recipient(s) file://C:\Documents and Settings\Blmai\Local Settings\temp\XPGrp... 9/17/2012 "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908" "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " 'This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " 'This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908 " 'This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908" "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908" "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908 " 'This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified m 49 CFR 173 428 for radioactive matenals excepted package-empty package, UN2908" 'This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908 " "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908" "This package conforms to the conditions and limitations specified in 49 CFR 173 428 for radioactive materials excepted package-empty package, UN2908"