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HomeMy WebLinkAboutDRC-2011-007451_9 - 0901a0688027e867APPENDIX A SEMI-ANNUAL EFFLUENT REPORT (JANUARY THROUGH JUNE, 2011) FOR THE WHITE MESA MILL PREPARED BY DENISON MINES (USA) CORP. INDEPENDENCE PLAZA 1050 17TH STREET, SUITE 950 DENVER, CO 80265    OENISOt!l MINES August 31, 2011 VIA FEDERAL EXPRESS Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period January 1, 2011 through June 30, 2011 Denison Mines {USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel : 303 628-7798 Fax: 303 389-4125 www.denisonmines.com As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart1)), and License Condition 11.3 A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period January 1, 2011 through June 30, 2011. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly, ~~ DENISON MINES (USA) CoRP. JoAnn Tischler Director, Compliance and Permitting CC Ron F. Hochstein Harold R. Roberts David C. Frydenlund David E. Turk Katherine Weinel Central Files White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (January through June, 2011) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 August 31, 2011 Table of Contents 1.0 INTRODUCTION .................................................................................................. 1 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING ..................................... 2 2.1 Program Overview ............................................................................................... 2 2.2 Sampling Protocol and Analytical Results ........................................................... 2 2.3 General Observations ............................................................................................ 3 2.4 Site Specific Sampling Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ..................................................................................... 8 5.0 STACK SAMPLING ............................................................................................... 9 6.0 SURFACE WATER MONITORING .................................................................... 11 7.0 SOIL SAMPLING ................................................................................................. 11 8.0 METEOROLOGICAL MONITORING ................................................................ 11 9.0 SIGNATURE ......................................................................................................... 12 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-210 Concentration Example Table 2 Air Monitoring Station Results U-N at (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits) Table 6 Environmental OSL Dosimeter Measurements (Gamma) Table 7 Stack Sampling Requirements Table 8 Stack Effluent Concentrations and Release Rates 1 INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tabl BHV-1 Air Sampling Graphs and Data Table Tab 2 BHV -2 Air Sampling Graphs and Data Table Tab 3 BHV-3 Air Sampling Graphs and Data Table Tab 4 BHV-4 Air Sampling Graphs and Data Table Tab 5 BHV -5 Air Sampling Graphs and Data Table Tab 6 BHV -6 Air Sampling Graphs and Data Table C Air Particulate Loading Graphs and QA/QC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Grapbs, Data Table, Laboratory Results and QA/QC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QA/QC ii WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER, 2010 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5 (east), and BHV-4 (south). BHV-1 serves as a surrogate for the nearest resident (BHV-1 is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV-3), which was monitored for airborne particulate up until November, 1995, at which time background was established, but is no longer monitored for air particulate; and • A station specifically requested by the White Mesa Ute Community south of the Mill Site (BVH-6); a) External (direct) gamma radiation measured at air monitoring stations BHV -1, BHV -2, BHV -3, BHV -4, BHV -5 and BHV -6; b) Vegetation at three site periphery locations, for uptake of radiation; c) Stack release rates from the Mill's air emissions sources; d) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; e) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; 1 N :\Required Reports\Semi Annual Effluent Reports\20 11 Jan to June\Jan_to_Jun_20 ll_Semi_annual_Effluent_Report_Main_text.docx f) Groundwater (up and down gradient) of the Mill facility; and 1 g) Seeps and springs in the vicinity of the Mill. 1 This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV-1, BHV-2, BHV -4, and BHV -5) are required by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV-1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring data base had been compiled at BHV -3 to establish a representative airborne radionuclide background for the Mill. It should be noted, however, that while air sampling was discontinued at this location, gamma measurements and soil sampling continue to be collected at BHV-3. In addition to the environmental air sampling locations described above, an additional station (BHV-6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb- 210 activity. Fugitive dust standards for the facility are limited by the Mill's State of 1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to JuneVan_to_Jun_20Il_Semi_annual_Effluent_Report_Main_text.docx Utah Air Approval Order, which sets a 20% visual opacity standard. The specific locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled High Volume Air Monitoring Stations included as Attachment A. Station BHV- 3, which is no longer sampled for air particulate is located approximately 3.5 miles west of the Mill facility and is not indicated on that Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this January through June, 2011 reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QA/QC information) reported by the laboratory are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and composited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station for the second half of 2010 and the underlying data are included as Attachment D. It should be noted that for graphical illustration purposes, values reported at zero, values reported at less than the prescribed detection limit ( < 1 x 10-16 uCi/rnl) and missing values were plotted as 1 x 10-16 uCi/rnl concentrations. Where other "less than" values were indicated (i.e., where detection limits for the data varied from 1 X w-16 uCi/rnl), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-210 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay 3 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to June \.I an_to_Jun_20 ll_Semi_annual_Eftluent_Report_Main_text.docx products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 below, demonstrating elevated Pb-210 activity where no uranium milling operations are located nearby. Pb-210 activity concentrations can be expected to be even higher for locations in the western U.S. where uranium ore bodies are commonly located. In April 1977, prior to Mill construction and Mill operations, air particulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/ml (13.0E-3 pCi/m3)2 Table 1-NCRP Report 94-Global Pb-210 Concentration Example State Pb-210 Concentration uBq/MJ uCi/ml California 600 1.6E-14 lllinois 1500 4.1E-14 Ohio 300 8.1E-15 Massachusetts 700 1.9E-14 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data supports the conclusion that airborne particulate is well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). It should also be noted that the analytical laboratory maintained Lower Limits of Detection consistent with NRC Regulatory Guide 4.14 for this reporting period. In fact, the data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1 4 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to JuneVan_to_Jun_20 ll_Semi_annuai_Effluent_Report_Main_text.docx ever exceeded the ECL at the Mill. With regard to that particular single measurement, while it is important to consider and evaluate an individual measurement exceeding the ECL, for public dose estimation purposes it is the average annual concentration that is of primary significance. In that instance, the average annual concentration of Th-230 for BHV-5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALARA goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVl 9.01E-16 1.59E-15 9.00E-14 1.38E+00 BHV2 3.79E-16 3.07E-16 9.00E-14 3.81E-01 BHV4 1.29E-15 3.30E-15 9.00E-14 2.55E+00 BHV5 3.20E-15 6.98E-15 9.00E-14 5.66E+00 BHV6 2.70E-15 3.01E-15 9.00E-14 3.17E+00 Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Station Result Result (uCi/ml) (uCi/ml) BHVl 1.90E-16 5.31E-16 BHV2 4.01E-17 8.54E-17 BHV4 1.40E-16 5.44E-16 BHV5 8.89E-16 2.03E-15 BHV6 4.62E-16 7.07E-16 5 N :\Required Reports\Semi Annual Effluent Reports\20 11 Jan to JuneVan_to_Jun_20 ll_Semi_annual_Effluent_Report_Main_text.docx Effluent Average Concentration Percent Limit (ECL) ECL (uCi/ml) 2.00E-14 1.80E+00 2.00E-14 3.14E-Ol 2.00E-14 1.7lE+00 2.00E-14 7.30E+00 2.00E-14 2.92E+00 Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVI 3.64E-16 4.99E-16 9.00E-13 4.79E-02 BHV2 9.11E-17 9.21E-17 9.00E-13 1.02E-02 BHV4 1.58E-16 4.18E-16 9.00E-13 3.20E-02 BHV5 l.lOE-15 2.52E-15 9.00E-13 2.01E-Ol BHV6 6.51E-16 5.75E-16 9.00E-13 6.81E-02 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 1st and 2nd Quarters 2011 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHVI 1.09E-14 8.38E-15 6.00E-13 1.61E+00 BHV2 1.06E-14 7.21E-15 6.00E-13 1.48E+00 BHV4 l.llE-14 8.26E-15 6.00E-13 1.61E+00 BHV5 1.48E-14 1.08E-14 6.00E-13 2.13E+00 BHV6 1.29E-14 7.97E-15 6.00E-13 1.74E+00 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the new 10 CFR Part 20 standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was discontinued in 1995. Instead, Denison demonstrates compliance with these limits and the requirements of R313-15-301 by calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division on July 28, 2008. This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the 6 N:\Required Reports\Serni Annual Effluent Reports\2011 Jan to J une\Jan_to_J un_20 ll_Semi_annual_Effluent_Report_Main_text.docx concentrations of radioactive dust and radon at individual receptor locations around the Mill. The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 100 mrem regulatory limit in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well below the ALARA goal of 10 mrernlyr for air emissions excluding radon as set out in R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U30 8 and 1.5% V20 5) and Arizona Strip ore (0.637% 0 30 8). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -1 at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the 1st and 2nd quarters of 2011 utilizing passive integrating devices, optically stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-1, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). Measurements obtained from location BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented at Attachment E to this report. 7 N :\Required Reports\Semi Annual Effluent Reports\20 II Jan to June\Jan_to_Jun_20II_Semi_annual_Effluent_Report_Main_text.docx Table 6-Environmental Optically Stimulated Luminescence Dosimeter ~easurements (<iamma) Monitoring 1st Qtr 2nd Qtr 1st Qtr 2nd Qtr Cumulative Station Result Result Result Less Result Less Semi- (mrem) (mrem) Background Background Annual (mrem) (mrem) Estimate* (mrem) BHVl 41.7 26 7.7 3.6 11.3 BHV2 34.3 24.2 0.3 1.8 2.1 BHV3 34 22.4 0 0 0 BHV4 38.2 21.5 4.2 -0.9 4.2 BHV5 42.2 25.6 8.2 3.2 11.4 BHV6 32.7 24.8 -1.3 2.4 2.4 *Negative values treated as zero for cumulative dose The results for this period indicate that above background measurements for stations BVH-1, BVH-2, BVH-4, BVH-5 and BHV-6 are within regulatory limits. BHV-1 is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV-1. The annual individual member of the public limit is 100 mrem/yr for combined internal and extemal exposure. 4.0 VE<iETATION SAMPLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. The U.S. Nuclear Regulatory Commission ("NRC") Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. During the 20 11 grazing season, two sets of samples have been collected to date, on June 23, 2011 and in July 2011. A third set of samples is planned for the fall season. At the conclusion of the third quarter of 2011, three sets will have been collected consistent with Regulatory Guide 4.14. The data from the June 2011 sampling is included in the current January to June 2011 Semi-Annual Effluent Report ("SAER"). Data from the July and fall sampling will be included in the July to December 2011 SAER. Section 4.2 of the Mill's Environmental Protection Manual states that vegetation samples are to be collected during the early spring, late spring and fall (i.e., the growing seasons). During the January to June 2011 period, the early spring samples were inadvertently omitted. The late spring sample was collected just past the end of spring (on June 23, 2011). An additional summer sample was collected in July 2011 in place of the omitted early spring sample. As a result, as discussed above, three samples will have been collected by the end of the 2011 grazing season meeting the requirements of NRC Regulatory Guide 4.14. 8 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to JuneVan_to_Jun_20 II_Semi_annual_Effluent_Report_Main_text.docx Graphical log-scale presentation of the vegetation sampling results for this reporting period, together with the analytical results reported by the Mill's contract laboratory (including QA/QC information) are included at Attachment F of this report. The 2nd quarter data results are within the variation of previous sampling episodes. 5.0 STACK SAMPLING Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: DUSA-1 , 2/07 (the "Environmental Protection Manual") gas stack samples are collected at the Mill in accordance with the calendar year schedule shown below: Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging Baghouse) Yellowcake Dryer (Yellowcake Baghouse) Quarterly None If operating, U-nat If operating, U-nat Semi-annually If operating, U-nat, If operating, U-nat, If operating, U-nat, Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-210 The yellowcake dryer and yellowcake baghouse operated during the 1st quarter of 2011. The yellowcake dryer, yellowcake baghouse, and grizzly operated during the 2nd quarter of 2011. The analytical results of stack sampling conducted for the 1st and 2nd Quarter of 2011, as well as for the 3rd and 4th Quarters of 2010, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate (uCi/sec) for U-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The actual analytical results reported by the laboratory for the 1st and 2nd quarters of 2011 are provided in Attachment G to this report. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL's for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi-annual reporting purposes. 9 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to June\Jan_to_Jun_20li_Semi_annuai_Effluent_Report_Main_text.docx Table 8-Stack Effluent Concentrations and Release Rates U-Nat U-Nat. Th-230 Th-230 Ra-226 Ra-226 Pb-210 Pb-210 u/Ci/cc uCi/sec uCi/cc uCiJsec uCi/cc uCi/sec uCilcc uCi/sec 3m Qtr, 2010 North YC Dryer, Run Not Not Not Not Not Not 1 6.97E-09 4.21E-03 Required Required Required Required Required Required North YC Dryer, Run Not Not Not Not Not Not 2 9.02E-09 5.32E-03 Required Required Required Required Required Required Yellowcake Not Not Not Not Not Not Baghouse 1.37E-09 4.57E-05 Required Required Required Required Required Required 4'h Qtr, 2010 North YC Dryer, Run 1 1.44E-08 7.33E-03 2.10E-ll l.07E-05 3.32E-12 1.69E-06 8.89E-14 4.53E-08 North YC Dryer, Run 2 l.25E-08 6.51E-03 7.97E-12 4.14E-06 2.73E-12 1.42E-06 2.18E-13 1.13E-07 Yellowcake Baghouse l.OSE-09 9.19E-04 5.50E-12 4.80E-06 2.87E-13 2.51E-07 4.23E-14 3.69E-08 (H Qtr, 2011 North YC Dryer, Run Not Not Not Not Not Not I 5.02E-09 3.17E-03 Required Required Required Required Required Required North YC Dryer, Run Not Not Not Not Not Not 2 3.67E-09 l .93E-03 Required Required Required Required Required Required Yellowcake Not Not Not Not Not Not Baghouse 2.90E-09 2.92E-03 Required Required Required Required Required Required 2nd Qtr, 2011 North YC Dryer, Run I 1.76E-08 9.2IE-03 1.76E-l2 9.25E-07 4.20E-14 2.20E-08 7.52E-12 3.94E-06 North YC Dryer, Run 2 1.54E-08 7.56E-03 2.12E-l2 1.04E-06 4.79E-14 2.35E-08 7.94E-l2 3.90E-06 Yellowcake Baghouse 8.58E-09 8.22E-03 1.97E-ll 1.89E-05 1.96E-13 1.88E-07 8.32E-13 7.97E-07 Grizzly Not Not Not Not Baghouse 9.7IE-12 5.96E-06 1.09E-13 6.67E-08 Required Required Required Re_q_uired 10 N:\Required Reports\Semi Annual Effluent Reports\2011 Jan to 1 une\J an_to_J un_20 ll_Semi_annual_Effluent_Report_Main_text.docx 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample in the event that surface water is not available for sampling. Westwater Canyon surface water was not sampled in the first or second quarter 2011 because no water was present during this reporting period. Attempts to collect a surface water sample from Westwater Canyon will continue through the next reporting period. If no surface water is available, a sediment sample will be collected as required. The Mill's Environmental Protection Manual, requires that Cottonwood Creek be sampled for total dissolved solids (TDS) and total suspended solids (TSS) quarterly and dissolved and suspended radionuclides including Gross Alpha, Unat, Ra-226, Th-230 semi-annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS and TSS during both the 1st and 2nd quarter and for the dissolved and suspended radionuclides noted above during the 2nd quarter. Cottonwood Creek is an intermittent ephemeral drainage located southwest and down- gradient of the Mill complex. Westwater Canyon is a drainage located west of the Mill facility, which is rarely flowing. The field data sheets for the surface water sampling attempts, along with graphs showing historic results are included as Attachment H. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6) once per year during August or as soon as possible thereafter, but no later than September 30 of each year. In accordance with the Mill's Environmental Protection Manual, surface soils will be collected during the third quarter 2011 and will be discussed in the July through December 2011 report. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of January through June, 2011. This information is retained at the Mill site for agency review. 11 N:\Required Reports\Semi Annual Effluent Reports\201 I Jan to J une\Jan_to_Jun_20 li_Semi_annual_Effl uent_Report_Main_text.docx 9.0 SIGNATURE Tbis Report was prepared by Denison Mines (USA) Corp. on August 3 1, 2011. Denison Mines (USA) Corp. By: Davi . Fry nlund Vice President, Regulatory Affairs and Counsel N:\Requircd Reports\Semi Annunl Effiuent Rcports\2011 Jan to June\Jan_to_Jun_20 II_Scmi_annuni_Eftluem_Rcport_Main_textdocx ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS ' .... I ' . -.. I ~ ... .. ' ... \ \ I I I \ . ( ~ ' "--... I ' I \ .. -' -,., ~, ....... c~:::_..-, ' ... • .. -I ( t''' ... -I .. .. I .. .. .. ' w , .. , ~1\.;' I ,-..J I ~ ..... __ ..-, , , / , .... .. I --' . ~ ' I \\ ,, ~ \ \ .. -I ... - t I ) r---' I I ----' -- I I I , , I ' ,) t ' / ~ f # -\ ., # '·· ;' ... .. I ~ .. 0 BHV-~ ... ... .. ~ .___ __ '\ \. - { ' \ \ ' I ( , \ I l \ / \ -I .. .. I , .. -.. I Property Boundary Reservation Boundary Canyon Rim .. ,. \ ") ..... ... ... I ~ i ... 0 Air Monitor Stations 0 BHV-5 c BHV-6 I ... ~ I ,. ... \ ... ... I 0 N ~ I --/ I 2000 0 2000 \ SCALE IN FEET I 0 ( I .... ... J .... I Denison Mines (USA) Corp. Project REVISIONS Date Bv 11109 dis 1113111 BM 112.7/11 eM WHITE MESA MILL Figure 2.3-1 High Volume Air Monitoring Stations ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV-1 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml SHV-1U Ufluent Concentration Limit= 2E-14 uCi/ml BHV-1T Effluent Concentration Limit= 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB AlARAGoal= 2.25E-14 uCi/ml AlARAGoal = SE-13 uCi/ml AlARAGoal = 2.25E·13 uCi/ml AlARAGoal-l.SE-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml pre 1994 MPC Limit = BE-14 uCi/ml Pte 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Umlt = 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL= 5E-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.35E-15 5.00£-12 1.25£-12 7.82E-16 8.00E-14 2.00£-14 1.06£-15 2.00E-12 5.00E-13 2.57£-14 4.00E·12 l.OOE-12 12/14/1981 1.56£-15 5.00E-12 1.25E-12 1.49£-15 8.00E-14 l.OOE-14 1.93£-15 2.00£·12 5.00£-13 2.64E-14 4.00E-12 l.OOE-12 3/29/1982 2.16E-15 5.00£-12 1.25£-12 2.93E·15 8.00£-14 2.00£-14 1.16£-15 2.00£·12 S.OOE-13 2.09E-14 4.00£-12 1.00E-12 6/30/1982 4.69£-15 5.00£-12 1.25£-12 3.46£-15 8.00£-14 .l.OOE-14 2.38£-15 2.00£-12 5.00£-13 2.14£-14 4.00£-12 1.00£-12 9/27/1982 4.45£-15 5.00£-12 1.25£-12 3.29E-15 8.00£-14 l.OOE-14 3.23£-15 2.00E-12 5.00E-13 1.99£-14 4.00£-12 1.00£-12 1/3/1983 4.39£-15 5.00£-12 1.25£-12 5.91£-16 8.00£-14 2.00£-14 9.14£-16 2.00£-12 5.00£-13 4.87£-14 4.00£-12 1.00£-12 4/4/1983 7.51£-16 5.00£-12 1.25£-12 2.13£·16 8.00£-14 2.00E·14 3.20£-16 2.00E-12 5.00£-13 1.88E-14 4.00£-12 1.00£-12 6/30/1983 2.68£-16 5.00£-12 1.25£-12 6.92£-16 8.00£-14 2.00£-14 7.92£-16 2.00£-12 5.00£-13 2.00£-14 4.00£-12 1.00£-12 10/3/1983 5.00£-12 1.25£-12 8.00£-14 2.00£-14 O.OOE+OO 2.00£·12 5.00£-13 4.00£-12 1.00£-12 1/3/1984 2.87£-15 5.00£-12 1.25£-12 1.14£-16 8.00£-14 2.00£-14 1.79£-16 2.00£-12 5.00£-13 1.06£-14 4.00£-12 1.00£-12 4/2/1984 1.59£-15 5,00£-12 1.25E-12 3.40£-16 8.00£-14 2.00£-14 3.71£-16 2.00£-12 5.00£-13 3.34£-14 4.00£-12 1.00£-12 7/2/1984 3.10£-15 5.00£-12 1.25£-12 l.OOE-15 8.00£-14 2.00£-14 2.09£-15 2.00£-12 5.00£-13 1.88£-14 4.00£-12 1.00E-12 10/1/1984 6.42E-16 5.00£-12 1.25£-12 1.39£-16 8.00£-14 2.00£-14 1.94£-16 2.00£-12 S.OOE-13 1.85£-14 4.00£-12 1.00£-12 1/2/1985 5.06E-16 5.00£-12 1.25£-12 4.56£-16 8.00£-14 2.00E-14 3.49£-16 2.00E·12 5.00£-13 .3.03E-14 4.00£-12 l .OOE-12 4/1/1985 O.OOE+OO 5.00£-12 1.25£-12 1.23£-15 8.00£-14 2.00£-14 4.88£-16 2.00£-12 5.00£-13 8.06£-15 4.00£-12 l.OOE-12 7/1/1985 7.17£-16 S.OOE-12 1.25£-12 8.00£-14 2.00£-14 1.05£-15 2.00£-12 5.00£-13 2.15E-14 4.00£-12 l.OOE-12 9/30/1985 6.13£-16 5.00E·12 1.25£-12 1.18£·16 B.OOE-14 2.00£-14 3.71£-16 2.00£-12 5.00£-13 3.64£-15 4.00£-12 l.OOE-12 1/2/1986 3.42£-15 S.OOE-12 1.25£-12 4.74£-16 8.00£-14 2.00£-14 2.00£-12 S.OOE-13 4.00£-12 l.OOE-12 4/1/1986 3.98£-15 5.00£-12 1.25£-12 9.74£-16 8.00£-14 2.00£-14 1.50£-15 2.00£-12 5.00£-13 1.41£-14 4.00£-12 l.OOE-12 6/30/1986 5.51£-17 S.OOE-12 1.25£-12 3.52£-16 8.00£-14 2.00£·14 1.37£-15 2.00£-12 5.00£-13 1.23£-14 4.00E-12 1.00£-12 10/27/1986 1.99£-15 5.00£-12 1.25£-12 3.06£-16 8.00£-14 2.00£-14 1.25£-15 2.00£·12 5.00£-13 1.08£-14 4.00£-12 1.00£-12 12/15/1986 1.67£-15 5.00£-12 1.25£-12 1.16£-16 8.00£-14 2.00£-14 5.98£-16 2.00£-12 5.00£-13 1.37£-14 4.00£-12 1.00£-12 3/16/1987 2.33£-15 5.00£-12 1.25£-12 4.30£·16 8.00£-14 2.00£-14 1.92£-16 2.00£-12 5.00£·13 5.59£-14 4.00£-12 1.00£-12 5/11/1987 2.36£-15 5.00£-12 1.25£-12 7.69£-16 8.00£-14 2.00£·14 8.76£-16 2.00£-12 5.00£-13 1.45E-14 4.00£-12 1.00£-12 9/9/1987 2.27£-15 5.00£-12 1.25E-12 2.44£-15 8.00£-14 2.00£-14 8.51E-16 2.00£·12 5.00E-13 3.14£-14 4.00£-12 l.OOE-12 11/2/1987 2.75£-15 5.00£-12 1.25£-12 2.46£-15 8.00£-14 2.00£-14 1.34£-15 2.00E-12 5.00£-13 2.79£-14 4.00£-12 1.00£-12 2/16/1988 1.07E-15 5.00£-12 1.25£-12 1.47£·16 8.00£-14 2.00£-14 4.44E-16 2.00E·12 5.00£-13 4.01E-14 4.00£-12 1.00E-12 5/18/1988 1.98£-15 5.00£-12 1.25£-12 1.25£-15 8.00E-14 2.00£-14 6.40£-16 2.00£-12 5.00£-13 1.07£-14 4.00E-12 1.00£-12 8/15/1988 2.06£-15 5.00£-12 1.25£-12 3.41£-15 S.OOE-14 2.00£-14 5.08£-16 2.00£-12 S.OOE-13 1.62£-14 4.00£-12 1.00£-12 11/14/1988 3.94£-15 5.00£-12 1.25£-12 2.12£·15 8.00£-14 2.00£-14 1.01£-15 2.00£-12 5.00£-13 2.47£-14 4.00£-12 l.OOE-12 2/13/1989 1.99£-15 S.OOE-12 1.25£-12 5.73£-16 8.00£-14 2.00£-14 5.99£-16 2.00£·12 S.OOE-13 3.23£-14 4.00£-12 1.00E-12 5/15/1989 1.70£-15 5.00£-12 1.25£-12 6.32£-16 S.OOE-14 2.00£-14 5.86£-16 2.00£-12 5.00£-13 6.16£-15 4.00£-12 l.OOE-12 8/14/1989 2.31E-15 S.OOE-12 1.25£-12 2.31E·16 8.00£-14 2.00E·14 1.77£-16 2.00£·12 S.OOE-13 7.65E-15 4.00£-12 l.OOE-12 11/13/1989 4.72£-15 S.OOE-12 1.25£-12 1.71E-15 8.00£-14 2.00E-14 1.52£-15 2.00£-12 5.00£-13 1.89£-14 4.00£-12 1.00£-12 2/12/1990 3.44£-16 S.OOE-12 1.25£-12 8.39£-16 8.00£-14 2.00£-14 8.31£-16 2.00£-12 5.00£-13 2.57E-14 4.00£-12 1.00£-12 5/14/1990 3.03£-15 5.00£-12 1.25£-12 1.47£-15 8.00£-14 2.00£-14 1.04£-15 2.00£-12 5.00£-13 1.79£-14 4.00£-12 1.00£-12 8/13/1990 1.64£-15 5.00£-12 1.25£-12 1.49£-15 8.00£-14 2.00£-14 3.34£-16 2.00£-12 5.00£-13 8.27£-15 4.00£-12 l.OOE-12 11/12/1990 1.48£-15 5.00£-12 1.25£-12 7.SOE-16 8.00£-14 2.00£-14 5.80£-16 2.00£-12 5.00£-13 2.16£-14 4.00£-12 1.00£-12 2/11/1991 1.90£-16 5.00£-12 1.25£-12 3.48£-17 8.00£-14 2.00£-14 7.91£-17 2.00£·12 5.00£-13 3.79£-14 4.00E-12 1.00£-12 5/13/1991 3.42£-16 5.00£-12 1.25E-12 1.34E-15 8.00E-14 2.00£·14 7.39E-16 2.00£-12 5.00£-13 1.46E-14 4.00£-12 l.OOE-12 8/12/1991 2.77£-16 5.00£-12 1.25£-12 4.17E-17 8.00£-14 2.00£-14 1.45£-16 2.00£·12 5.00£-13 1.80£-14 4.00£-12 1.00£-12 U /U/1991 6.65£-17 5.00£-12 1.25£-12 9.13£-17 8.00£-14 2.00£-14 2.77£-17 2.00£-12 5.00£-13 1.06£-14 4.00£-12 1.00£-12 2/10/1992 1.94£-16 5.00£-12 1.25£-12 4.28£-17 8.00£-14 2.00£-14 4.08£-17 2.00£·12 5.00£-13 S.S1E-14 4.00£-12 l .OOE-12 5/11/1992 2.54£-16 5.00£-12 1.25£-12 6.49£-16 8.00£-14 2.00£-14 6.86£-17 2.00£-12 5.00£-13 1.38£-14 4.00£-12 1.00£-12 8/10/1992 1.73£-16 S.OOE-12 1.25£-12 1.55£-16 8.00E-14 2.00£-14 1.20£-16 2.00£·12 5.00£-13 1.53£-14 4.00£-12 l.OOE-12 11/9/1992 1.56£-16 S.OOE-12 1.25£-12 3.19£-17 8.00£-14 2.00£-14 4.90£-18 2.00£-12 S.OOE-13 1.86£-14 4.00£-12 l.OOE-12 2/9/1993 2.10E-16 S.OOE-12 1.25£-12 S.OOE-14 2.00£-14 3.89E-17 2.00£-12 5.00E-13 2.52£-14 4.00£-12 l.OOE-12 5/10/1993 l.OOE-16 5.00£-12 1.25£-12 4.11£-17 B.OOE-14 2.00£-14 6.43£-17 2.00£-12 5.00£-13 1.26£-14 4.00£-12 l.OOE-12 8/10/1993 2.30£-16 5.00E-12 1.25E-12 6.00£-17 8.00£-14 2.00£-14 6.43£-17 2.00£-12 5.00£-13 1,60E-14 4.00£-12 l.OOE-12 11/8/1993 5.00£-12 1.25£-12 8.00£-14 2.00£-14 O.OOE+OO 2.00£-12 S.OOE-13 1.57£-14 4.00£-12 1.00£-12 2/7/1994 1.82E-16 S.OOE-12 1.25£-12 5.00£-18 B.OOE-14 2.00£-14 4.30£-17 2.00£-12 5.00£-13 2.59£-14 4.00£-12 l.OOE-12 5/9/1994 3.60£-16 5.00£-12 1.25£-12 2.70£·16 8.00£-14 2.00£·14 2.87£-16 2.00£·12 5.00£-13 1.60£-14 4.00£-12 l.OOE-12 8/9/1994 4.04£-16 5.00£-12 1.25£-12 2.70£-16 8.00£-14 2.00£-14 2.94£-16 2.00£-12 5.00£-13 2.00£-15 4.00£-12 1.00£-12 11/7/1994 9.18£-17 5.00E-12 1.25£-12 3.60£-16 8.00£-14 2.00E·14 2.91E-16 2.00£-12 5.00£-13 2.00£-15 4.00£-12 l.OOE-12 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-1U Effluent Concentration Limit= 2E-14 uCi/ml BHV-lT effluent Concentration limit= 9E-13 uCi/ml BHV-lR Effluent Concentration limit= 6E-13 uCi/ml BHV-lPB ALARAGoal= 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC limit : SE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 M PC Limit = 4E-12 uCi/ml Pre 1994 A LARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.77E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 S.OOE-15 9.70E-17 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.SOE-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 5.36E-16 2.00E-14 .S.OOE-15 1.60E-15 9.00E-13 2.25E-13 3.84E-15 6.00E-13 1.SOE-13 8/9/1995 l.70E-16 9.00E-14 2.25E-14 1.60E-16 2.00E-14 S.OOE-15 2.76E-16 9.00E-13 2.25E-13 3.76E-15 6.00E-13 1.50E-13 11/11/1995 4.80E-15 9.00E-14 2.25E-14 6.41E-16 2.00E-14 S.OOE-15 8.93E-16 9.00E-13 2.25E-13 5.20E-15 6.00E-13 1.50E-13 2/5/1996 5.34E-15 9.00E-14 2.25E-14 2.30E-15 2.00E-14 S.OOE-15 1.30E-15 9.00E-13 2.25E·13 4.20E-15 6.00E-13 1.50E-13 5/6/1996 5.11E-16 9.00E-14 2.25E-14 3.06E-16 2.00E-14 S.OOE-15 1.40E-16 9.00E-13 2.25E-13 7.03E-15 6.00E-13 1.50E-13 8/5/1996 S.99E-16 9.00E-14 2.25E-14 1.55E-15 2.00E-14 S.OOE-15 2.03E-16 9.00E-13 2.25E-13 5.94E-15 6.00E-13 1.50E-13 11/6/1996 3.38E-16 9.00E-14 2.25E-14 5.45E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.22E-14 6.00E-13 1.50E-13 2/6/1997 l.OOE-16 9.00E-14 2.25E-14 1.25E-16 2.00E-14 S.OOE-15 L28E-16 9.00E-13 2.25E-13 5.68E-15 6.00E-13 1.50E-13 5/5/1997 L09E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 4.39E-15 6.00E-13 1.50E-13 8/11/1997 2.88E-16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 5.29E-15 6.00E-13 1.50E-13 1/5/1998 3.24E-16 9.00E-14 2.25E-14 3.47E-16 2.00E-14 S.OOE-15 1.19E-16 9.00E-13 2.25E-13 4.73E-15 6.00E-13 1.50E-13 4/28/1998 4.75E-16 9.00E-14 2.25E-14 6.73E-16 2.00E-14 5.00E-15 5.69E-16 9.00E-13 2.25E·13 5.94E-15 6.00E-13 1.50E-13 7/31/1998 8.84E-16 9.00E-14 2.25E-14 1.93E-15 2.00E-14 5.00E-15 1.43E-15 9.00E-13 2.25E·13 5.22E-15 6.00E-13 1.50E-13 9/28/1998 2.81E-16 9.00E-14 2.25E-14 2.89E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-l3 4.64E-15 6.00E-13 1.50E-13 12/28/1998 8.08E-16 9.00E-14 2.25E-14 4.93E-16 2.00E-14 5.00E-15 5.01E-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 3/29/1999 2.06E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5.00E-15 1.42E-16 9.00E-13 2.25E-13 6.69E-15 6.00E-13 1.50E-13 7/3/1999 5.31E-16 9.00E-14 2.25E-14 2.47E-16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13 9/27/1999 8.98E-16 9.00E-14 2.25E-14 3.90E-16 2.00E-14 5.00E-15 2.96E-16 9.00E-13 2.25E-13 7.29E-15 6.00E-13 1.50E-13 12/28/1999 1.48E-15 9.00E-14 2.25E-14 6.00E·16 2.00E-14 5.00E-15 5.57E-16 9.00E-13 2.25E-13 6.19E-15 6.00E-13 l.SOE-13 3/27/2000 l.OOE-16 9.00E-14 2.2SE-14 1.06E-16 2.00E-14 5.00E-15 l.OOE-16 .9.00E-13 2.25E-13 6.23E-15 6.00E-13 1.50E-13 6/26/2000 3.47E-16 9.00E-14 2.25E-14 3.46E-16 2.00E-14 5.00E-15 .3.62E-16 9.00E-13 2.25E-13 4.50E-15 6.00E-13 L50E-13 9/26/2000 2.51E-16 9.00E-14 2.25E-14 1.78E-16 2.00E-14 5.00E-15 3.25E-16 9.00E-13 2.25E-13 8.55E-15 6.00E-13 1.50E-13 12/26/2000 l.OOE-16 9.00E-14 2.25E-14 1.42E-16 2.00E-14 S.OOE-15 1.31E-16 9.00E-13 2.25E·13 7.77E-15 6.00E-13 1.50E-13 3/26/2001 3.10E-16 9.00E-14 2.25E-14 1.00E-15 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 7.19E-15 6.00E-13 1.50E-13 7/29/2001 1.52E-16 S.OOE-14 2.25E-14 1.44E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 7.21E-15 6.00E-13 1.50E-13 9/24/2001 1.03E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 LOOE-16 9.00E-13 2.25E·13 8.09E-15 6.00E-13 1.50E-13 12/31/2001 l.OOE-16 9.00E-14 2.25E·14 1.00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 l.25E-l3 1.39E-15 6.00E-13 1.50E-13 4/l/2002 2.05E-16 9.00E-14 2.25E-14 2.44E-16 2.00E-14 5.00E-l5 2.29E-16 9.00E-13 2.25E-13 8.15E-15 6.00E-13 1.50E-13 7/l/2002 3.55E-16 9.00E-l4 2.25E-14 4.85E-l6 2.00E-14 5.00E-15 1.06E-16 9.00E-13 2.25E-13 7.65E-15 6.00E-13 1.50E-13 9/30/2002 1.17E-16 9.00E-14 2.25E-14 1.61E-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.68E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 1.03E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.46E-15 6.00E·13 1.50E-13 3/31/2003 1.20E-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 5.00E·15 1.00E-16 9.00E-13 .2.25E-13 4.68E-15 6.00E-13 1.50E-13 6/30/2003 2.18E·16 9.00E·14 2.25E-14 3.40E·16 2.00E·14 S.OOE-15 1.67E-16 9.00E·13 2.25E-13 5.96E·15 6.00E-13 1.50E·13 9/29/2003 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E·14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.28E-15 6.00E·13 1.50E·13 12/29/2003 l.OOE-16 9.00E-14 2.25E-14 2.54E-16 2.00E-14 S.OOE-15 3.35E-16 9.00E-13 2.25E-13 6.25E-15 6.00E-13 1.50E-13 3/29/2004 t.OOE-16 9.00E-14 2.25E·14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 S.OOE-13 2.25E-13 1.54E-14 6.00E·l3 1.50E-13 6/27/2004 l.OOE-16 9.00E-14 2.25E·14 1.00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.04E-15 6.00E-13 1.50E-13 9/27/2004 l.OOE-16 9.00E·14 2.25E-14 1.00E-16 2.00E-14 5.00E·15 l.OOE-16 9.00E-13 2.25E·13 1.05E-14 6.00E-13 l.SOE-13 12/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13 3/28/2005 l.OOE-16 9.00E-14 2.25E·14 l.OOE-16 2.00E·14 5.00E-15 l.OOE-16 9.00E-13 2.25E·13 7.42E-15 6.00E-13 l.SOE-13 6/29/2005 1.00E·16 9.00E-14 2.25E-14 1.30E-16 Z.OOE-14 5.00E-15 1.20E-16 9.00E·13 l.25E·13 7.94E-15 6.00E·13 1.50E-13 9/26/2005 l.OOE-16 9.00E-14 2.25E-14 2.56E-16 2.00E-14 S.OOE-15 2.42E-16 9.00E-13 2.25E·13 1.22E-14 6.00E-13 1.50E-13 1/3/2006 2.13E-16 9.00E-14 2.25E·14 1.04E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.73E·14 6.00E-13 1.50E-13 4/3/2006 1.62E-16 9.00E-14 2.25E-14 1.86E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.2SE·13 8.36E-15 6.00E-13 1.50E-13 7/3/2006 1.86E-16 9.00E-14 2,25E-14 1.00E-16 2.00E·14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.77E-15 6.00E·13 l.SOE-13 10/2/2006 l.OOE·16 9.00E-14 2.25E-14 1.00E·16 2,00E·14 5.00E-15 l.OOE-16 9.00E·13 2.25E-13 1,30E-14 6.00E·13 1.50E·13 1/1/2007 l.OOE·16 9.00E-14 2.25E-14 1.47E-16 2.00E·14 5.00E-15 l.OOE-16 9.00E-13 2.25E·13 1.17E-14 6.00E·13 1.50E-13 4/2/2007 2.23E-16 9.00E·14 2.25E-14 1.63E-16 2.00E·14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.65E·14 6.00E-13 1.50E-13 7/2/2007 D5E-16 9.00E-14 2.25E-14 1.34E-16 2.00E-14 5.00E-15 1.36E-16 9.00E-13 2.25E·13 1.78E-14 6.00E·13 1.50E-13 9/30/2007 1.15E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.68E-15 6.00E·13 1.50E-13 12/31/2007 l.OOE-16 9.00E-14 2.25E-14 1.93E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 3/31/2008 1.14E-16 9.00E-14 2.25E-14 1.13E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13 6/30/2008 7.09E·16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 S.OOE-15 2.27E-16 9.00E-13 2.25E-13 6.52E-15 6.00E·13 1.50E-13 Date Effluent Concentration limit= 9E-14 uCi/ml BHV-1U Effluent Concentration limit= ZE-14 uCi/ml BHV-1T Effluent Concentration limit= 9E-13 uCi/ml BHV-1R Effluent Concentration limit= GE-13 uCi/ml BHV-1PB AlARAGoal= 2.Z5E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml AlARAGoal= 1.5E-13 uCi/ml pre 1994 MPC limit= SE-12 uCi/ml Pre 1994 MPC limit -BE-14 uCi/ml Pre 1994 MPC limit= 2E-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 7.69E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 S.OOE-15 1.90E-16 9.00E-13 2.25E-13 7.64E-15 6.00E-13 1.50E-13 12/31/2008 1.21E-15 9.00E-14 2.25E-14 4.76E-16 2.00E-14 S.OOE-15 3.34E·16 9.00E-13 2.25E-13 1.16E-14 6.00E-13 1.50E-13 3/15/2009 2.14E-15 9.00E-14 2.25E-14 1.02E-15 2.00E-14 S.OOE-15 1.00E-15 9.00E-13 2.25E-13 4.44E-15 6.00E-13 1.50E-13 6/15/2009 5.97E-17 9.00E-14 2.25E-14 2.35E-16 ~.OOE-14 S.OOE-15 2.18E-16 9.00E-13 2.25E-13 5.13E-15 6.00E-13 1.50E-13 9/15/2009 9.55E-16 9.00E-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 9.87E-17 9.00E-13 2.25E-13 9.47E-15 6.00E-13 l.SOE-13 12/15/2009 1.24E-15 9.00E-14 2.25E-14 9.25E-17 2.00E-14 5.00E-15 5.60E-17 9.00E-13 2.25E-13 5.95E-15 6.00E-13 l.SOE-13 3/31/2010 1.97E-15 9.00E-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 3.27E-16 9.00E-13 2.25E-13 l.OOE-14 6.00E-13 1.50E-13 6130/2010 1.58E-15 9.00E-14 2.25E-14 4.71E-16 2.00E-14 5.00E-15 7.70E-16 9.00E-13 2.25E-13 4.07E-15 6.00E-13 1.50E-13 9/30/2010 8.42E-16 9.00E-14 2.25E-14 2.80E-16 2.00E-14 5.00E-15 l.31E-16 9.00E-13 2.25E-13 6.80E-15 6.00E-13 1.50E-13 12/31/2010 1.27E-15 9.00E-14 2.25E-14 2.32E-16 2.00E-14 S.OOE-15 2.30E-16 9.00E-13 2.25E-13 1.27E-14 6.00E-13 1.50E-13 4/4/2011 9.01E-16 9.00E-14 2.25E-14 1.90E-16 2.00E-14 5.00E-15 3.64E-16 9.00E-13 2.25E-13 1.09E-14 6.00E-13 1.50E-13 7/4/2011 1.59E-15 9.00E-14 2.25E-14 5.31E-16 2.00E-14 S.OOE-15 4.99E-16 9.00E-13 2.25E-13 8.38E-15 6.00E-13 1.50E-13 "' c 0 ~ ... c Cl) (.) c 0 0 Cl) 'C (.) ::::J c 0 'C co a: ,.... :> J: m C\1 C') .-.- I I w w 0 0 <:::! C! .-.- ~ ~ ~ • r- «: ~ ... :::::.: --.. ~ .c::: ~ =-• - • 4 ~ • • .. , .::: ~ ~ . ..-~ "'=::; - ~ ~ ~ .... I ~ ..... ~ ~ ~ t... b. ) ~ ~ -.::::::: ~ ,4 ~ ~ ~:::: _...:~ ;· iiJ '<:t .-I w 0 <:::! ,...__ ~~ ~ ::::::.. ..,.. o~-das 6o-das -.. ~ !..-" ... ~ so-das ~ 1•-.... ~ 4 ec -....: La-das go-das go-d as vo-das -·-~ £o-das 0 .- ~ ..>Ill ... '-.. ~ //~ !'f . C\1 I Go-d as "0 CIS Q) ~a-d as _J + oo-das .......... It;~ ~ 66-das co C\1 C\1 I 86-das E ::J '6 ~ 7 L6-das CIS a: :.'! ... ~ 96-das + ~ -::::0 96-das 0 C') C\1 --..-;::. r-v6-das I E ::J • • ~ ~ ~ • £6-das ·;:: 0 ..t: I- G6-das + ~6-das (ij At-:; .. ~ 06-das ..... ::J ro ~ ~ ~ ~ ~ ..... 6s-das z E sa-d as -~ c:: CIS ..... :::.1 ll -;:,. ~. La-das ::::> + gs-das ~--r-+ • ga-d as vs-das ~ ...... ~ .... £s-das r:.. Gs-das -~ ...;, ~a-des LO co ,..... co .-.-.-.- I I I I w w w w 0 0 0 0 <:::! <:::! C! <:::! .-.-.-.- (are~s 6o1) 1.00E-11 1.00E-12 1.00E-13 Q) (ij u W1.00E-14 01 0 :::::!.. 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml BHV-1 Uranium-Natural Concentrations (uCi/ml) Pre 1994 MPC Limit= 5E-12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml ._.. I I _J. \I\ ¥ ..... co 6. (I) (f) • C\J (I) co co 6. 6. (!) (I) (f) (f) ¥ oo;t co 6. (I) (f) ., LO co I I 0.. (!) (f) 7'1 II -.4{ 1\../; 1¥ - (0 co 6. (I) (f) 'I ... " co 6. (I) (f) co co I 0.. (!) (f) 0'> co I 0.. (I) (f) 1'1 I~ 0 0'> 6. (I) (f) • ~ v, .A ... + I r~· ..... 0'> I 0.. (!) (f) ~ 6. (I) (f) (I) 0'> 6. (!) (f) ~ oo;t 0'> I 0.. (I) (f) LO 0'> 6. (I) (f) J Y II I • ~ \ T J (0 0'> I 0.. (I) (f) r-.... 0'> I 0.. (I) (f) I ....ll co 0'> 6. (!) (f) 0'> 0'> I 0.. (I) (f) 1t ... • ~1\ 1 _VV 0 0 6. (I) (f) ..... 0 I 0.. (I) (f) • J\ C\J 0 I 0.. (!) (f) 0 (I) 0 I 0.. (I) (f) oo;t 0 I 0.. (I) (f) 4 ... J J'5J ..... LO 0 I 0.. (!) (f) (0 0 6. (I) (f) r-.... 0 I 0.. (!) (f) ' co 0 I 0.. (!) (f) ""') 0'> 0 6. (!) (f) 0 ..... I 0.. (I) (f) 1.00E-12 1.00E-13 1.00E-14 w Cii (.) UJ1.00E-15 Cl 0 ~ 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit= 2E-14 uCi/ml ALARA Goal= 5E-13 uCi/ml Pre 1994 MPC Limit= 8E-14uCi/ml .... • T \ 11 n •. f \ t I t ' ~" T"" ro ' 0. Q) U) C\1 ro I 0. Q) U) ~ • .,. ... .. , ... I i/ I 1 j l J ¥ C') ro I 0. Q) UJ ' ""' LO ro ro 6.. c. Q) Q) U) U) co ro I 0. Q) U) t--oo 6.. Q) U) ro ro I 0. Q) U) \i I 0) ro I 0. Q) U) 0 0) I 0. Q) U) T"" 0) I 0. Q) UJ ~ ~ C\1 0) I 0. Q) U) ~ C') 0) I 0. Q) U) l T ~T ""' 0) 6.. Q) U) BHV-1 Thorium-230 Concentrations (uCi/ml) • n X fiT Tr ' LO 0) I 0. Q) U) T ,...- T ([ co 0) 6.. Q) U) t--O) 6.. Q) U) ~ 1r IT\T u ro 0) 6.. Q) U) 0) 0) 6.. Q) U) • I I • 1\ \ + /\t ~~ \1 'JV~ ' 0 0 6.. Q) U) T"" 0 I 0. Q) U) ~ I 0. Q) U) C') 0 I 0. Q) U) ""' 0 I 0. Q) U) ., 7V t I""' )~~ LO 0 6.. Q) U) co 0 6.. Q) U) t--o 6.. Q) U) ro 0 6.. Q) U) 'II" 1\ I • J. '' v 0) 0 6.. Q) U) 0 6.. Q) U) • 1.00E-11 1.00E-12 1.00E-13 ,..._1.00E-14 Cll (ij u Cf) 0> 0 ....J -1.00E-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit= 9E-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml Pre 1994 MPC Limit= 2E-12uCi/ml Pre 1994 ALARA Goal = SE-13 uCi/ml • .. , N\ ...... ~ k • T'"" c:o I a. Cll Cf) .1. ' I • ' ' C\1 (Y) c:o c:o I I a. a. Cll Cll Cf) Cf) • .. • v ~ ~ <II • ... ' '<;)" LO CO ,...._ c:o C> 0 T'"" C\1 (Y) c:o c:o c:o c:o c:o c:o C> C> C> C> 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. 6.. Cll Cll Cll Cll Cll Cll Cll Cll Cll Cll Cf) Cf) Cf) Cf) Cf) Cf) Cf) Cf) Cf) Cf) \ ' ~ r1 """ C> I ~ a. Cll Cf) BHV-1 Radium-226 Concentrations (uCi/ml) ~ v .... ' LO C> I a. Cll Cf) 1 'I' ..L ..... v \. ~ "¥ ' co C> 6.. Cll Cf) ' ,...._ C> 6.. Cll Cf) c:o C> 6.. Cll Cf) C> C> I a. Cll Cf) -• I \ \ . 1\ v ~ '\1\.. }J~ 0 0 I a. Cll Cf) T'"" 0 I a. Cll Cf) C\1 0 6.. Cll Cf) (Y) 0 6.. Cll Cf) """ 0 I a. Cll Cf) .. .J\ LO 0 I a. Cll Cf) ' co 0 I a. Cll Cf) . • •1 • .A j""' \ ,...._ 0 6.. Cll Cf) c:o 0 6.. Cll Cf) C> 0 I a. Cll Cf) • • ¥ 0 T'"" I a. Cll Cf) , 1.00E-11 1.00E-12 1.00E-13 Q) «i u U)1.00E-1 4 Cl 0 ~ 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 6E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCi/ml Pre 1994 ALARA Goal= 1E-12 uCilml 11" 1\ . .... .. II .. 7r 9 ~ \ l\ 1\ r· ,_ It l\ 1\ .~ _! .,.... co 6. Q) U) C\J co I c.. Q) U) '" 1- (Y) co 6. Q) U) • '"<!" 1.0 co co I I c.. c.. Q) Q) U) U) ...)¥ . <D co I c.. Q) U) . 1"-co 6. Q) U) '1 T'f ~VV'~ co 0> co co I I c.. c.. Q) Q) U) U) 0 0> I c.. Q) U) .,.... 0> 6. Q) U) C\J 0> I c.. Q) U) (Y) 0> 6. Q) U) 1 '"<!" 0> 6. Q) U) BHV-1 Lead-21 0 Concentrations (uCi/ml) F'lll. ..... 1.0 0> 6. Q) U) t <D 0> I c.. Q) U) .. . .... .. 1"-0> I c.. Q) U) co 0> 6. Q) U) 0> 0> I c.. Q) U) • 0 0 6. Q) U) ~ .,.... 0 I c.. Q) U) II • • C\J 0 6. Q) U) ' (Y) 0 I c.. Q) U) 1 f1 ~ ~ J J '"<!" 0 6. Q) U) 1.0 0 I c.. Q) U) #1 ~ . <D 0 I c.. Q) U) 1"-0 I c.. Q) U) co 0 I c.. Q) U) • 0> 0 I c.. Q) U) -- ,._ 11. 0 .,.... I c.. Q) U) TAB2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit-ZE-14 uCi/ml BHV-2T Effluent Concentration Limit = 9£-13 uCi/ml BHV-2R Effluent Concentration Limit -6£-13 uCi/ml BHV-2PB ALARAGoal-2.25£-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.25£-13 uCi/ml ALARAGoal-1.5£-13 uCi/ml Pre 1994 MPC Limit= 5E-UuCi/ml Pre 1994 MPC Limit-BE-14 uCi/ml Pre 1994 MPC Limit= ZE-UuCi/ml Pre 1994 MPC Limit= 4£-12 uCi/ml Pre 1994 ALARA GOAL -1.25£-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= 1£-UuCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.39£-15 5.00£-12 1.25£-12 3.69£-16 8.00£-14 2.00£-14 5.92£-16 2.00£-12 5.00£-13 1.67£-14 4.00£-12 1.00£-12 12/14/1981 4.62£-16 S.OOE-12 1.25£-12 8.03£-16 8.00£-14 2.00£-14 3.62£-16 2.00E-12 5.00£-13 1.33£-14 4.00£-12 l.OOE-12 3/29/1982 7.07£-16 5.00£-12 1.25£-12 1.10£-15 8.00£-14 2.00E-14 7.27£-16 Z.OOE-12 5.00£-13 1.52£-14 4.00£-12 1.00£-12 6/30/1982 8.84E-16 S.OOE-12 1.25E-12 7.73£-16 8.00£-14 2.00£-14 4.78£-16 2.00£-12 5.00£-13 1.98£-14 4.00£-12 l.OOE-12 9/27/1982 1.23£-15 5.00£-12 1.25£-12 3.60£-16 8.00£-14 2.00£-14 8.73£-16 2.00£-12 5.00£-13 2.35£-14 4.00£-12 l.OOE-12 1/3/1983 2.64£-15 5.00£-12 1.25£-12 2.55£-16 8.00£-14 ~.OOE-14 1.98£-16 2.00£-12 5.00£-13 2.85£-14 4.00£-12 l.OOE-12 4/4/1983 2.14£-16 5.00£-12 1.25£-12 1.02£-16 8.00£-14 2.00£-14 1.57£-16 2.00£-12 5.00£-13 2.48£-14 4.00£-12 1.00£-12 6/30/1983 2.85£-16 5.00£-12 1.25£-12 2.06£-16 8.00£-14 l.OOE-14 2.24£-16 2.00£-12 5.00£-13 1.79£-14 4.00£-12 1.00£-12 10/3/1983 2.70£-16 5.00£-12 1.25£-12 3.36£-16 8.00£-14 l.OOE-14 4.37£-16 2.00£-12 5.00£-13 1.78£-14 4.00£-12 1.00£-12 1/3}1984 2.78£-15 5.00£-12 1.25£-12 1.20£-16 8.00£-14 2.00£-14 6.64£-17 2.00£-12 5.00£-13 9.14£-15 4.00£-12 1.00£-12 4/2/1984 4.28£-16 5.00£-12 1.25£-12 1.75£-16 8.00E-14 2.00£-14 4.57£-17 2.00£-12 5.00£-13 3.55£·14 4.00£-12 1.00£-12 7/2/1984 2.78£-15 5.00£-12 1.25£-12 8.12£-16 8.00£-14 2.00£-14 1.98£-16 2.00£-12 5.00£-13 1.68£-14 4.00£-12 1.00£-12 10/1/1984 2.69£-16 5.00£-12 1.25£-12 2.66£-17 8.00£-14 2.00£-14 0.00£+00 2.00£-12 5.00£-13 1.77£-14 4.00£-12 1.00£-12 1/2/1985 2.15£-16 5.00£-12 1.25£-12 7.55£-16 8.00E-14 2.00£-14 2.87£-16 2.00£-12 5.00£-13 3.19E-14 4.00£-12 1.00£-12 4/1/1985 1.00£-16 5.00£-12 1.25E-12 1.67£-16 8.00E-14 2.00£-14 6.75£-17 2.00£-12 5.00E-13 7.56£-15 4.00£-12 1.00E-12 7/1/1985 3.70E-17 5.00£-12 1.25£-12 9.00£-16 8.00E-14 2.00£-14 4.90£-17 2.00£-12 5.00£-13 1.31E-14 4.00£-12 1.00E-12 9/30/1985 9.32£·17 5.00£-12 1.25£-12 2.18£-16 S.OOE-14 2.00£-14 3.71£-16 2.00£-12 5.00£-13 3.64£-15 4.00£-12 1.00£-12 1/2/1986 1.00£-16 5.00£-12 1.25£-12 2.16£-16 8.00£-14 2.00£-14 2.15£-17 2.00£-12 5.00£-13 3.04£-16 4.00£-12 1.00£-12 4/1/1986 1.31£-15 5.00£-12 1.25£-12 1.50£-16 8.00£-14 2.00£-14 3.71£-16 2.00£-12 5.00£-13 2.90£-15 4.00£-12 1.00£-12 6/30/1986 2.23£-16 5.00£-12 1.25£-12 1.32£-16 8.00£-14 2.00£-14 7.09£-17 2.00£-12 5.00£-13 2.53£-14 4.00£-12 1.00£-12 10/27/1986 6.41£-16 5.00£-12 1.25£-12 1.74£-16 8.00£-14 2.00£-14 3.67£-16 2.00£-12 5.00£-13 1.04£-14 4.00£-12 1.00£-12 12/15/1986 3.56£-16 5.00£-12 1.25£-12 1.00£-16 8.00£-14 2.00£-14 1.05£-16 2.00£-12 5.00£-13 '7.81£-15 4.00£-12 l.OOE-12 3/16/1987 5.31£-16 5.00£-12 1.25£-12 1.30£-16 8.00£-14 2.00£-14 7.74£-17 2.00£-12 5.00£-13 3.80£-14 4.00£-12 l.OOE-12 5/11/1987 4.06£-16 5.00£-12 1.25E-12 6.63£-17 8.00E-14 2.00£-14 1.34E-16 2.00£-12 5.00£-13 1.10E-14 4.00£-12 l.OOE-12 9/9/1987 2.74£-16 5.00£-12 1.25£-12 2.38£-16 8.00£-14 2.00£-14 1.38£-16 2.00£-12 5.00£-13 1.04£-14 4.00£-12 1.00£-12 11/2/1987 3.73£-16 S.OOE-12 1.25E-12 3.11£-16 8.00E-14 2.00£-14 1.83£-16 2.00£-12 5.00£-13 1.17£-14 4.00£-12 l.OOE-12 2/16/1988 2.78£-15 5.00£-12 1.25£-12 2.31£-17 8.00£-14 2.00£-14 1.20£-16 2.00£-12 S.OOE-13 3.55£-14 4.00£-12 1.00£-12 5/18/1988 4.63£-16 S.OOE-12 1.25£-12 1.49£-16 8.00£-14 2.00£-14 2.30£-16 2.00£-12 5.00£-13 1.18£-14 4.00£-12 l.OOE-12 8/15/1988 8.06£-16 S.OOE-12 1.25£-12 8.69£-16 8.00£-14 2.00£-14 1.80£-16 2.00£-12 5.00£-13 1.42£-14 4.00£-12 l.OOE-12 11/14/1988 4.34£-16 5.00£-12 1.25£-12 6.76£-16 8.00£-14 2.00£-14 1.57£-16 2.00£-12 5.00£-13 2.25£-14 4.00£-12 1.00£-12 2/13/1989 5.80£-16 5.00£-12 1.25£-12 2.85£-16 8.00£-14 2.00£-14 1.55£-16 2.00£-12 5.00£-13 2.80£-14 4.00£-12 1.00£-12 5/15/1989 5.06£-16 5.00£-12 1.25£-12 2.28£-16 8.00£-14 2.00£-14 1.63£-16 2.00£-12 5.00£-13 6.05£-15 4.00£-12 1.00£-12 8/14/1989 4.71£-16 5.00£-12 1.25£-12 9.60£-16 8.00£-14 2.00£-14 1.26£-15 2.00£-12 5.00£-13 6.65£-15 4.00£-12 1.00£-12 11/13/1989 1.14£-15 5.00£-12 1.25£-12 4.08£-16 8.00£-14 2.00£-14 4.18£-16 2.00£-12 S.OOE-13 1.59£-14 4.00£-12 1.00£-12 2/12/1990 1.09£-15 5.00£-12 1.25£-12 3.25£-16 8.00£-14 2.00£-14 3.74£-16 2.00£-12 5.00£-13 1.98£-14 4.00£-12 1.00£-12 5/14/1990 9.32£-16 5.00£-12 1.25£-12 5.27£-16 8.00£-14 2.00£-14 3.97£-16 2.00£-12 5.00£-13 1.69£-14 4.00£-12 1.00£-12 8/13/1990 1.66£-16 5.00£-12 1.25£-12 5.49£-16 8.00£·14 2.00£-14 4.75£-17 2.00£-12 5.00£-13 1.27£-15 4.00£-12 1.00£·12 11/12/1990 6.05£-16 5.00£-12 1.25£-12 2.64£-16 8.00£-14 2.00£-14 1.93£-16 2.00£-12 5.00£-13 2.25£-14 4.00£-12 1.00£-12 2/11/1991 8.72£-17 5.00£-12 1.25£-12 7.00£-18 8.00£-14 2.00£-14 3.33£-17 2.00£-12 5.00£-13 3.49£-14 4.00£-12 1.00£-12 5/13/1991 1.16£-16 5.00£-12 1.25£-12 3.86£-16 8.00£-14 2.00£-14 2.80£-16 2.00£-12 5.00£-13 1.50£·14 4.00£-12 1.00£-12 8/12/1991 9.02£-17 5.00£-12 1.25£-12 8.82E-17 I!.OOE-14 2.00£-14 7.65£-17 2.00E-12 5.00£-13 1.58£·14 4.00£-12 l.OOE-12 11/11/1991 4.81£-17 5.00£-12 1.25E-12 3.82E-17 8.00£-14 2.00£-14 2.54£-17 2.00£-12 5.00£-13 1.45£-14 4.00£-12 1.00£-12 2/10/1992 1.54E-16 5.00£-12 1.25£-12 6.82£-17 S.OOE-14 2.00£-14 1.40£-17 2.00E-12 5.00£-13 3.41£-14 4.00£-12 1.00£-12 5/11/1992 2.38£-16 5.00£-12 1.25E-12 7.63£-17 S.OOE-14 2.00£-14 3.07£-17 2.00£-12 5.00£-13 1.27£-14 4.00£-12 1.00£-12 8/10/1992 1.01£-16 5.00£-12 1.25£-12 7.07£-17 8.00£-14 2.00£-14 2.80£-17 2.00£-12 5.00£-13 1.41£-14 4.00£-12 1.00£-12 11/9/1992 5.20£-17 5.00£-12 1.25£-12 3.65£-17 8.00£-14 2.00£-14 1.78£-17 2.00£-12 5.00£-13 1.71£-14 4.00£-12 l.OOE-12 2/9/1993 2.39£-16 5.00£-12 1.25£-12 2.97£-17 8.00£-14 2.00£-14 6.31£-17 2.00£-12 5.00£-13 3.41£·14 4.00£-12 l.OOE-12 5/10/1993 1.00£-16 5,00£-12 1.25£-12 7.11£-17 8.00£-14 2.00£-14 3.19£-17 2.00£-12 S.OOE-13 1.34£-14 4.00E-12 1.00£-12 8/10/1993 1.90£-16 5.00£-12 1.25£-12 1.00£-16 8.00£-14 2.00£-14 l.OOE-16 2.00£-12 5.00£-13 l.SOE-14 4.00£-12 l.OOE-12 11/8/1993 1.00E-16 5.00£-12 1.25E-12 l.OOE-16 8.00£-14 2.00£-14 LOOE-16 2.00£-12 S.OOE-13 1.49£-14 4.00£-12 l.OOE-12 2/7/1994 2.23£-16 5.00£-12 1.25£-12 1.00£-16 8.00£-14 2.00£-14 1.84£-16 2.00E-12 5.00£-13 2.19E-14 4.00E-12 l.OOE-12 5/9/1994 2.16E-16 S.OOE-12 1.25£-12 7.20£-17 8.00£-14 2.00E-14 9.89£-17 Z.OOE-12 5.00£-13 1.37£-14 4.00£-12 1.00£-12 8/9/1994 9.29£-17 5.00£-12 1.25£-12 2.96£-16 8.00£-14 2.00£-14 3.04£-16 2.00£-12 5.00£-13 l.OOE-16 4.00£-12 1.00£·12 11/7/1994 9.21£-17 5.00£-12 1.25£-12 2.35£-16 8.00£-14 2.00£-14 l.OOE-16 2.00£-12 5.00£-13 1.00£-16 4.00£-12 1.00£-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit= 9E-13 uCi/ml BHV-2R Effluent Concentration Limit= 6E-13 uCi/ml BHV-2PB AIARAGoal = 2.25E-14 uCi/ml AIARAGoal = SE-13 uCi/ml AIARAGoal = 2.25E-13 uCi/ml AIARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994· MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 AIARA GOAL -1.25E-12 uCi/ml Pre 1994 AIARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone ~FC EFCA 2/7/1995 1.18E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 ;1.25E-13 7.42E-15 G.OOE-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 1.20E-16 2.00E-14 5.00E-15 3.50E-16 9.00E-13 2.25E-13 3.90E-15 6.00E-13 1,50E-13 8/9/1995 8.90E-17 9.00E-14 2.25E-14 9.67E-17 2.00E-14 5.00E-15 1.35E-16 9.00E-13 2.25E-13 2.38E-16 6.00E-13 1.50E-13 11/11/1995 2.83E-15 9.00E-14 2.25E-14 4.09E-16 2.00E-14 5.00E-15 5.23E-16 9.00E-13 2.25E-13 6.77E-15 6.00E-13 1.50E-13 2/5/1996 1.75E-15 9.00E-14 2.25E-14 8.66E-16 2.00E-14 5.00E-15 4.86E-16 9.00E-13 2.25E-13 3.50E-15 6.00E-13 1.50E-13 5/6/1996 1.40E-16 9.00E-14 L25E-14 1.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.85E-15 6.00E-13 1.50E-13 8/5/1996 1.43E-16 9.00E-14 2.25E-14 2.78E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.83E-15 6.00E-13 1.50E-13 11/6/1996 1.45E-16 9.00E-14 2.25E-14 1.57E-16 2.00E-14 5.00E-15 l.OOE-16 g.OOE-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 2/6/1997 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 l.25E-13 5.84E-16 6.00E-13 1.50E-13 5/5/1997 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.89E-15 6.00E-13 1.50E-13 8/11/1997 l.OOE-16 9.00E-14 2.25E-14 1.09E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.69E-15 6.00E-13 1.50E-13 1/5/1998 2.55E-16 9.00E-14 2.25E-14 1.07E-16 2.00E-14 5.00E-15 S.OOE-17 9.00E-13 2.25E-13 S.llE-15 6.00E-13 l.SOE-13 4/28/1998 1.20E-16 9.00E-14 2.25E-14 1.71E-16 l.OOE-14 5.00E-15 1.28E-16 9.00E-13 ,2.25E-13 6.40E-15 6.00E-13 1.50E-13 7/31/1998 1.47E-16 9.00E-14 2.25E-14 4.24E-16 Z.OOE-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 4.80E-15 6.00E-13 l.SOE-13 9/28/1998 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 L25E-13 4.26E-15 6.00E-13 1.50E-13 12/28/1998 2.54E-16 9.00E-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 1.38E-16 9.00E-13 2.25E-13 6.88E-15 6,00E-13 1.50E-13 3/29/1999 1.07E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 L25E-13 7.61E-15 6.00E-13 1.50E-13 7/3/1999 2.46E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E·15 6.00E-13 1.50E-13 9/27/1999 2.81E-16 9.00E-14 2.25E-14 1.41E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.35E-15 6.00E-13 1.50E-13 12/28/1999 5.20E-16 9.00E-14 2.25E-14 2.60E-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 2.25E-13 7.00E-15 6.00E-13 1.50E-13 3/27/2000 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.12E-15 6.00E-13 1.50E-13 6/26/2000 l.lOE-16 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 S.OOE-15 1.16E-16 9.00E-13 2.25E-13 5.07E-15 6.00E-13 1.50E-13 9/26/2000 .l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 5.31E-15 6.00E-13 1.50E-13 12/26/2000 1.26E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.45E-15 6.00E-13 1.50E-13 3/26/2001 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE·15 1.00E-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 7/2/2001 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 6.56E-15 6.00E-13 1.50E-13 9/24/2001 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 6.16E·15 6.00E-13 1.50E-13 12/31/2001 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.20E-15 6.00E-13 1.50E-13 4/1/2002 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2,25E-13 9.95E-15 6.00E-13 1.50E-13 7/1/2002 1.25E-16 9.00E-14 2.25E-14 1.43E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 8.25E-15 6.00E-13 1.50E-13 9/30/2002 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 3.69E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 6.91E-15 6.00E-13 1.50E-13 3/31/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13 6/30/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 5.27E-15 6.00E-13 1.50E-13 9/29/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.23E-15 6.00E·13 1.50E-13 12/29/2003 1,00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 7.80E-15 6.00E-13 1.50E-13 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 6/27/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 3.09E-15 6.00E-13 1.50E-13 9/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.73E-14 6.00E-13 1.50E-13 12/27/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 3/28/2005 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 8.88E-15 6.00E-13 1.50E-13 6/29/2005 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 8.85E-15 6.00E-13 1.50E-13 9/26/2005 1.00E-16 9.00E-14 2.25E-14 1.99E-16 Z.OOE-14 5.00E-15 1.44E-16 9.00E-13 2.25E-13 3.81E-14 6.00E-13 1.50E-13 1/3/2006 1.29E-16 9.00E-14 2.25E-14 ,l.OOE-16 2.00E-14 5.00E-15 4.08E-16 9.00E-13 2.25E-13 6.58E-14 6.00E-13 1.50E-13 4/3/2006 1.02E-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.08E-14 6.00E-13 1.50E-13 7/3/2006 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.00E-13 1.50E-13 10/2/2006 1.30E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.68E-14 6.00E-13 1.50E-13 1/1/2007 1.24E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.38E-14 6.00E-13 1.50E-13 4/2/2007 1.40E-16 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.63E-14 6.00E-13 1.50E-13 7/2/2007 1.04E-16 9,00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.36E-14 6.00E-13 1.50E-13 9/30/2007 1.00E-16 g.OOE-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 12/31/2007 1.91E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13 3/30/2008 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.49E-15 6.00E-13 1.50E-13 6/30/2008 .1.29E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l .OOE-16 9.00E-13 2.25E-13 4.82E-15 6.00E-13 1.50E-13 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit= ZE-14 uCi/ml BHV-2T Effluent Concentration Limit= 9E-13 uCi/ml BHV-ZR Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal= Z.ZSE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal = Z.ZSE-13 uCi/ml ALARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-UuCi/ml Pre 1994 MPC Limit = SE-14 uCi/ml Pre 1994 MPC Limit= ZE-12 uCi/ml Pre 1994 MPC Limit -4E-12 uCi/ml Pre 1994 ALARA GOAL= l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL= 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 l .50E-13 12/31/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 5.00E-15 1.07E-16 9.00E-13 2.25E-13 4.81E-15 G.OOE-13 1.50E-13 6/15/2009 1.24E-17 9.00E-14 2.25E-14 4.64E-17 2.00E-14 5.00E-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 G.OOE-13 1.50E-13 9/15/2009 2.43E-16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 S.OOE-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 G.OOE-13 1.50E-13 12/15/2009 .5.72E-16 9.00E-14 2.25E-14 2.94E-17 2.00E-14 5.00E-15 2.57E-17 9.00E-13 2.25E-13 6.70E-15 G.OOE-13 1.50E-13 3/31/2010 5.47E-16 9.00E-14 2.25E-14 1.42E-17 2.00E-14 S.OOE-15 4.66E-17 9.00E-13 2.25E-13 8.24E-15 G.OOE-13 1.50E-13 6/30/2010 3.58E-16 9.00E-14 2.25E-14 6.64E-17 2.00E-14 S.OOE-15 9.90E-17 9.00E-13 2.25E-13 2.01E-15 G.OOE-13 1.50E-13 9/30/2010 2.91E-16 9.00E-14 2.25E-14 4.48E-17 2.00E-14 5.00E-15 5.72E-17 9.00E-13 2.25E-13 1.08E-15 G.OOE-13 1.50E-13 12/31/2010 5.73E-16 9.00E-14 2.25E-14 7.24E-17 2.00E-14 5.00E-15 6.76E-17 9.00E-13 2.25E-13 1.35E-14 6.00E-13 1.50E-13 4/4/2011 3.79E-16 9.00E-14 2.25E-14 4.01E-17 2.00E-14 S.OOE-15 9.11E-17 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 7/4/2011 3.07E-16 9.00E-14 2.25E-14 8.54E-17 2.00E-14 S.OOE-15 9-21E-17 9.00E-13 2.25E-13 7.21E-15 6.00E-13 l.SOE-13 In c:: 0 --; lo. ... c:: Q) CJ c:: 0 0 Q) :2 -CJ ::J c:: 0 :.a «S a: C\1 ::> :I: al C\1 (Y) ,..-,..- I I w w 0 0 ~ ~ ,..- ........ • •:::::: •::::::: •::::: ~ I+ ::::::: ..... '4 0:::::: .. - \ 2 • , ~ i .... L -=:::::;:::: ::.• t-1-- .. h ... t:::• ?: ~ 1 c t::!. 0 l,....-A .-:: ~ r ~ '<t ...- I w 0 ~ ,~ ::> ....,.;:::;;::ooo ~;:· • r--"""'" .. ~ .... , o~-das eo-das ...- ~ ~ so-das La-das go-d as oc:....._, ~ so-das -vo-das E:o-das 0 ...-C\1 I ~ co-das -o (13 Q) b<l .; 4 ~a-d as __J + oo-das r-.~ ~ -~ ee-das co C\1 C\1 I se-das E ::J i5 .-:: N tc:: ~ Le-das (13 a: ee-das + .... .~ ~..: :Jill se-das 0 (Y) C\1 ve-das I E ~::?. ::J E:e-das ·;:: 0 .c. .. .:::::::: s ~r: • -~ ~ ... f- ce-das + ~e-das (ij ~~ ~ .. -- J - ~r. 1-~ ~ - oe-das .... ::J -ro es-das z E ::J ss-das c ctl -:::. ,.~~ ~ ..... ..... La-das :::::> + gg-das ss-das -vs-das ~ I" "' §r """' ~ f. - E:s-das cs-das ~s-das 1.() co 1'-CX) ...-...-...-w w w I w 0 0 0 0 ~ ~ ~ ~ ..-,..- (a1eos DOl) 1.00E-11 1.00E-12 1.00E-13 Q) (ij (.) U'Jl.OOE-14 Cl 0 _J - 1.00E-15 1.00E-16 1.00E-17 • ,.... co a. Cl> U) Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E-12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml ~ I .. '\.flo. ..... 11• '' lr ~ • • v ~ t .. \ • I* f~ rw\ .. ~ I c. Cl> U) C') co ' c. Cl> U) '<t co a. Cl> U) ' ll) co ' c. Cl> U) <D co a. Cl> U) r--. co ' c. Cl> U) co co ' c. Cl> U) 0> co a. Cl> U) 0 0> ' c. Cl> U) ... ,.... 0> a. Cl> U) C\J 0> a. Cl> U) C') 0> a. Cl> U) '<t 0> a. Cl> U) BHV-2 Uranium-Natural Concentrations (uCi/ml) it. 11 ll) 0> a. Cl> U) I ~ t, "\JWY. <D 0> a. Cl> U) ' r--. 0> a. Cl> U) co 0> ' c. Cl> U) 0> (J) a. Cl> U) l.A 0 0 a. Cl> U) ,.... 0 ' c. Cl> U) A C\1 0 a. Cl> U) ' C') 0 a. Cl> U) '<t 0 ' c. Cl> U) ~ ll) 0 a. Cl> U) <D 0 I c. Cl> U) r--. 0 ' c. Cl> U) co 0 a. Cl> U) \ /~"""\, ~ ~ 0> 0 a. Cl> U) 0 ,.... ' c. Cl> U) - en c 0 "+0 cu .... -c Cl) () c 0 0 0 C") ~ E ::::s "i: 0 .c 1- C\1 :> :I: Ill T'""" T'""" uJ 0 0 C\1 C") T'""" T'""" I I UJ UJ 0 0 q q -- 4 "<t 1.() T'""" T'""" I I UJ UJ 0 0 q q (aiE:lS 6o1) .... k ~ !« k ~~ t-~ ~ ~ b.. t-~ ~ ~ - ~ t- ~r fi ~ J t== ~ I•~ ~ 14-~ p:. <D T'""" I UJ 0 q !-' ..... ~ ~~ 1'- T'""" I UJ 0 q T'""" - - CX) T'""" I UJ 0 q o~-das so-das so-das La-das go-das so-das vo-das £o-das cm-das ~o-das oo-das 66-das 95-das L6-das 95-das ss-das 175-das £6-das c6-das ~6-das os-das se-das es-das La-das gg-das ss-das vs-das £s-das cs-das ~s-das :::- .§ 0 ::s -rn t: 0 .. ca II.. -t: C1) (,) t: 0 (.) CD C\1 C\1 I E ::s =s ca " C\1 :> :I: a::l ,.,.. ,..-C\l ,..-w I UJ 0 0 ~ ~ io-loo .. C") "':t 1.0 ,..-,..-,..-w I I UJ UJ 0 0 0 ~ ~ ~ ,..- (a1eos f3ol) ~ ........ ~~--k ~ ~ I"!'== r-... .... P+ !. 6:::--"'== ~ ~ ~ • ~ ...... ~F t-- ..... I--.._ r=::r-. ~ ~ ~ CD w 0 ~ ,..- t::~ :.4 ;;; ~ ~ t:=+ ,.....i+- - - I'- w 0 ~ ,..- o~-das 6o-das so-das Lo-das go-d as so-das vo-das E:o-das cm-das w-das oo-das 66-das 86-das L6-das 96-das S6-das v6-das 86-das G6-das ~6-das 05-das 68-das ss-das La-das gg-das ss-das vs-das E:s-das Gs-das ~s-das -E :::::: 0 :I -"' c 0 ; .... ... c G) u c 0 0 0 ,.... C}l "C ca G) ..J N :> ::I: Ill ,...-,...-w 0 ~ ...- C'J (t) ,...-...- I I w w 0 0 ~ ~ J. 1:> • r- « ~ ""r-)-.. I«:; -..-::: ~ ~ '- ~ ~ , • r-• tl4 t tc: ~ ~ ·~ •c:::::::: ~ tc:::; p I t~: ,.._ I ~r-. ~ ~~ b. ~ rs ~ ' I•F::: ~ .. F: ~~ ~· ~ v ,...- I w 0 ~ (a1eos ool) - ..... 1.0 ...-I w 0 ~ ...- co ...-I w 0 ~ - t--,...- I w 0 ~ o~-das 6o-das so-das Lo-das go-das go-d as vo-das 8o-das co-das ~o-das oo-das 66-das 86-das L6-das 95-das 96-das v6-das 86-das c6-das ~6-das 06-das 6s-das ss-das Ls-das gs-das gs-das vs-das 8s-das cs-das ~s-das TAB3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit= ZE-14 uCi/ml BHV-3T Effluent Concentration Limit= 9E-13 uCi/ml BHV-3R Effluent Concentration Limit= 6E-13 uCi/ml BHV-3PB AlARAGoal = 2.25E-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.25E-l3 uCi/ml AlARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC Limit= ZE-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-1Z uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.74E-15 S.OOE-12 l.25E-12 9.02E-16 8.00E·14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 1.54E-14 4.00E-12 l.OOE-12 12/14/1981 1.59E-15 5.00E-12 l.25E-12 5.03E-16 8.00E-14 2.00E-14 1.30E-16 2.00E-12 S.OOE-13 2.25E-14 4.00E-12 l.OOE-12 3/29/1982 3.76E-16 S.OOE-12 l.2SE-12 5.2SE-16 8.00E-14 2.00E-14 4.08E-16 l .OOE-12 S.OOE-13 1.96E-14 4.00E-l2 l.OOE-12 6/30/1982 3.83E-16 5.00E-12 1.25E-12 2.16E-16 8.00E·l4 l.OOE-14 1.41E-15 2.00E-12 S.OOE.·l3 2.40E-14 4.00E-12 l.OOE-12 9/27/1982 5.95E-16 5.00E-12 1.25E-12 1.44E-15 8.00E-14 2.00E-14 5.36E-16 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.00E-12 1/3/1983 2.05E-16 5.00E-12 l.25E-12 1.23E-16 8.00E-14 2.00E-14 1.10E·16 2.00E-12 5.00E-13 3.01E-14 4.00E-12 l.OOE-12 4/4/1983 l.OOE-16 5.00E-12 1.25E-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 5.00E-13 1.39E-14 4.00E-12 1.00E-12 6/30/1983 3.06E-16 5.00E-12 1.25E-12 9.59E·17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 5.00E-13 1.70E·14 4.00E-12 l.OOE-12 10/3/1983 1.91E-16 5.00E-12 l.25E-12 3.05E-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 S.OOE-13 1.76E-14 4.00E-12 1.00E-12 1/3/1984 3.01E-16 5.00E-12 1.25E-12 9.51E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 9.17E-15 4.00E-12 l.OOE-12 4/2/1984 8.22E-16 S.OOE-12 1.25E-12 7.52E-16 8.00E-14 2.00E-14 5.20E-17 2.00E-12 S.OOE-13 3.47E-14 4.00E-12 1.00E-12 7/2/1984 5.29E-16 5.00E-12 1.25E-12 6.18E-16 8.00E-14 2.00E-14 l.40E-16 2.00E-12 S.OOE-13 1.32E·14 4.00E-12 1.00E-12 10/1/1984 l.74E-16 5.00E-12 1.25E-12 7.10E-17 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.08£-14 4.00£-12 l.OOE-12 1/2/1985 1.00E-17 5.00£-12 1.25E-12 7.10E-17 S.OOE-14 2.00E-14 7.80E-17 2.00E-12 S.OOE-13 2.73E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 5.00E-12 1.25E-12 2.76E-16 8.00E-14 2.00E-14 4.10E-17 2.00E-12 S.OOE-13 1.12E-14 4.00E-12 l.OOE-12 7/1/1985 1.04E-16 5.00E-12 L25E-12 1.00E-16 8.00E-14 2.00E-14 l.OOE-16 l.OOE-12 5.00E-13 1.64E-14 4.00E-12 l.OOE-12 9/30/1985 l.OOE-16 .5.00E-12 1.25E-12 1.00E-15 S.OOE-14 2.00E-14 1.00E-16 2.00E-12 5.00E·13 1.73E-14 4.00E-12 l.OOE-12 1/2/1986 1.03E-15 'S.OOE-12 1.25E-12 3.17E-16 8.00E-14 2.00E-14 1.25E-16 2.00E-12 5.00E-13 1.21E-17 4.00E-12 l.OOE-12 4/1/1986 8.04E-16 S.OOE-12 1.25E-12 1.93E-17 8.00E-14 2.00E-14 1.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-12 l.OOE-12 6/30/1986 4.29E·16 S.OOE-12 1.25E-12 1.77E-16 8.00E-14 2.00E-14 2.83E-16 2.00E-12 S.OOE-13 1.97E·14 4.00E-12 l.OOE-12 10/27/1986 6.45E-16 S.OOE-12 1.2SE-12 9.89E-17 8.00E-14 2.00E-14 4.16E-15 2.00E-12 5.00E-13 1.64E-14 4.00E-12 1.00E-12 12/15/1986 1.31E-16 5.00E-l2 1.25E-12 O.OOE+OO 8.00E-14 2.00E-14 4.16E-17 2.00E-12 5.00E-13 4.60E-15 4.00E-12 1.00E-12 3/16/1987 2.01E-16 5.00E-12 1.25E-12 l.20E-16 8.00E-14 2.00E-14 5,73E-17 2.00E-12 5.00E-13 1.60E-14 4.00E-12 1.00E-12 5/11/1987 2,16E-16 5.00E-12 1.25E-12 1.96E-16 8.00E-14 2.00E-14 7.38E-17 2.00E-12 5.00E-13 1.59E-14 4.00E-12 l.OOE-12 9/9/1987 2.41E-16 5.00E-12 1.25E-12 2.18E-16 B.OOE-14 2.00E-14 3.52E-17 l.OOE-12 5.00E-13 1.46E-14 4.00E-12 1.00E-12 11/2/1987 2.44E-16 5.00E-12 1.25E-12 2.32E-16 S.OOE-14 2.00E-14 2.37E-17 2.00E-12 5.00E-13 2.48E-14 4.00E-12 l.OOE-12 2/16/1988 8.08E-16 5.00E-12 1.25E-12 2.55E-16 8.00E-14 2.00E-14 3.42E-16 2.00E-12 5.00E-13 5.61E-14 4.00E-12 l.OOE-12 S/18/1988 1.14E-16 S.OOE-12 1.2SE-12 4.14E-17 8.00E-14 2.00E-14 1.00E-16 2.00£-12 5.00E-13 1.20E-14 4.00E-12 l.OOE-12 8/15/1988 2.08E-16 5.00E-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 3.65E-17 2.00E-12 5.00E-13 1.36E-14 4.00E-12 l.OOE-12 11/14/1988 4.21E-16 5.00E-12 1.25E-12 2.93E-16 8.00E-14 2.00E-14 l.09E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 l.OOE-12 2/13/1989 4.45E-16 S.OOE-12 1.25E-12 4.78E-17 8.00E-14 2.00E-14 2.47E-17 2.00E-12 .S.OOE-13 3.34E-14 4.00E-12 l.OOE-12 S/15/1989 l.OSE-16 S.OOE-12 1.2SE-12 l.OOE-16 8.00E-14 2.00E-14 2.45E-17 2.00E-12 5.00E-13 6.56E-15 4.00E-12 1.00E-12 8/14/1989 1.31E-16 S.OOE-12 1.2SE-12 5.85E-17 8.00£-14 2.00E-14 3.97E-17 2.00E-12 5.00E-13 6.75E-15 4.00E-12 l.OOE-12 11/13/1989 1.67E-16 5.00E-12 1.25E-12 3.87E-17 8.00E-14 2.00E-14 8.03E-17 2.00E-12 5.00E-13 1.69E-14 4.00E-12 l.OOE-12 2/12/1990 4.43E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 3.50E-17 2.00E-12 5.00E-13 2.37E-14 4.00E-12 1.00E-12 5/14/1990 3.84E-16 5.00E-12 l.2SE-12 2.54E-16 8.00E-14 2.00E-14 1,02E-16 2.00E-12 5.00E-13 1.68E-14 4.00E-12 l.OOE-12 8/13/1990 7.27E-17 5.00E-12 1.25E-12 2.87E-16 8.00E-14 2.00E-14 l.21E-17 2.00E-12 5.00E-13 7.86E-15 4.00E-12 l.OOE-12 11/12/1990 1.84E-16 S.OOE-12 l.25E-12 1.34E-16 8.00E-14 2.00E-14 8.53E-17 2.00E-12 S.OOE-13 2.01E-14 4.00E-12 1.00E-12 2/11/1991 4.66E-17 S.OOE-12 1.25E-12 8.48E-16 S.OOE-14 2.00E-14 1.94E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 1.00E-12 5/13/1991 5.05E·17 5.00E-12 1.25E-12 7.40E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 1.50E-14 4.00E-12 1.00E-12 8/12/1991 7.14E-17 5.00£-12 1.2SE-12 6.22E-17 g.OOE-14 2.00E-14 7.95E-17 2.00E-12 5.00E-13 1.77E-14 4.00E-12 LOOE-12 11/11/1991 1.41E-17 S.OOE-12 l.25E-12 2.19E-18 S.OOE-14 2.00E-14 2.7SE-17 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 l.OOE-12 2/10/1992 8.12E-17 5.00E-12 1.25E-12 2.3SE-17 S.OOE-14 2.00E-14 2.76E-18 2.00E-12 5.00E-13 3.57E-14 4,00E-12 l.OOE-12 5/11/1992 9.18E-17 S.OOE-12 l.25E-12 S.SOE-17 S.OOE-14 2.00E-14 3.36E-17 l.OOE-12 S.OOE-13 l.28E-14 4.00E-12 l.OOE-12 8/10/1992 2.00E-18 S.OOE-12 1.2SE-12 4.19E-17 B.OOE-14 2.00E-14 2.00E-18 l.OOE-12 S.OOE-13 1.59E-14 4.00E-12 l.OOE-12 11/9/1992 4.00E-17 5.00E-12 1.25E-12 2.68E-17 8.00E-14 2.00E-14 l.07E-17 2.00E-12 S.OOE-13 1.81E-14 4.00E-12 1.00E-12 2/9/1993 7.94E-17 5.00E-12 1.25E-12 1.00E-16 S.OOE-14 l.OOE-14 1,09E-16 2.00E-12 5.00E-13 2.69E·14 4.00E-12 1.00E-12 5/10/1993 1.60E-17 S.OOE-12 1.2SE-12 5.07E-17 8.00E-14 2.00E-14 7.64E-17 2.00E-12 5.00E-13 1.26E-14 4.00E-12 1.00E-12 8/10/1993 6.00E-17 5.00E-12 1.25E-12 6.00E-18 S.OOE-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12 11/8/1993 l.OOE-16 S.OOE-12 l.25E-12 1.00E-16 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 S.OOE-13 2.10E-14 4.00E-12 1.00E-12 2/7/1994 1.61E-16 S.OOE-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 5.00E-13 2.23E-14 4.00E-12 1.00E-12 5/9/1994 2..77E-16 S.OOE-12 1.25E-12 2.80E-17 8.00E-14 2.00E-14 8.37E-18 2.00E-12 5.00E-13 1.40E-14 4.00E-12 1.00E-12 8/9/1994 7.39E-17 S.OOE-12 l.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.14E-16 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 l.OOE-12 11/7/1994 9.05E-17 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 Date Effluent Concentration limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = ZE-14 uCi/ml BHV-3T Effluent Concentration limit= 9E-13 uCi/ml BHV-3R Effluent Concentration limit= 6E-13 uCi/ml BHV-3PB AIARAGoal-2.2SE-14 uCi/ml ALARA Goal-SE-13 uCi/ml AlARAGoal-Z.ZSE-13 uCi/ml AlARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC limit = SE-12 uCi/ml Pre 1994 MPC limit= BE-14 uCi/ml Pre 1994 MPC limit= ZE-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= l.ZSE-12 uCi/ml Pre 1994 A lARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 7.99E-17 9.00E-14 2.25E-14 9.60E-17 2.00E-14 5.00E-15 9.60E-17 9.00E-13 2.25E-13 9.05E-15 6.00E-13 1.SOE-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 9.80E-17 l.OOE-14 5.00E-15 8.60E-17 ,9.00E-13 2.25E-13 2.88E-15 6.00E-13 1.50E-13 8/9/1995 7.30E-17 9.00E-14 2.25E-14 9.20E-17 l.OOE-14 5.00E-15 4.40E-17 9.00E-13 2.25E-13 1.96E-15 6.00E-13 1.50E-13 11/11/1995 3.16E-16 !l.OOE-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 l.25E-13 1.91E-14 6.00E-13 1.50E-13 2/5/1996 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 S/6/1996 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/5/1996 3.00E-16 9.00E-14 2.25E-14 3.43E-16 Z.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 11/6/1996 3.16E-16 9.00E-14 l.l5E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 l.25E-13 1.91E-14 6.00E-13 1.50E-13 2/6/1997 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 l..18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 5/5/1997 1.31E-16 9.00E-14 2.25E-14 1.39E-16 Z.OOE-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/11/1997 3.00E-16 9.00E-14 2.25E-14 3.43E-16 Z.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E·l4 6.00E-13 1.50E-13 1/5/1998 3.16E-16 9.00E-14 2.25E-l4 1.31E-16 Z.OOE-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91£-14 6.00E-13 l.SOE-13 4/28/1998 3.41E-16 9.00E-14 l.25E-14 2.26E-16 l.OOE-14 S.OOE-15 1.18E-16 9.00E-13 z.25E-13 2.69E-14 6.00E-13 l.SOE-13 7/31/1998 l.31E-l6 9.00E-14 2.25E-14 1.39E-16 l.OOE-14 5.00E-15 1.82E-16 S.OOE-13 2.25E-13 1.53E·14 6.00E-13 1.50E-13 9/28/1998 3.00E-16 9.00E-14 l.25E-14 3.43E-16 Z.OOE-14 5.00E-15 3.99E-16 9.00E-13 l.25E-13 1.31E-14 6.00E-13 1.50E-13 12/28/1998 3.16E-16 9.00E-14 2.25E-14 1.31E-16 l.OOE-14 5.00E-15 6.58E-17 9.00E-13 2.l5E-13 1.91E-14 6.00E-13 1.50E-13 3/29/1999 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 '2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/1999 1.31E-16 9.00E-14 2.25E-14 1.39E-16 l.OOE-14 5.00E-15 1.82E-16 9.00E-13 l .l5E-13 1.53E-14 6.00E-13 1.50E-13 9/27/1999 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/28/1999 3.16E-16 9.00E-14 2.25E-14 1.31E-16 l.OOE-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 l.91E-14 6.00E-13 1.50E-13 3/28/2000 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/26/2000 1.31E-16 9.00E-14 l .25E-14 1.39E-16 l.OOE-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/26/2000 3.00E-16 g.OOE-14 2.25E-14 3.43E-16 l.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.SOE-13 12/26/2000 3.16E-16 9.00E-14 2,25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/26/2001 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2001 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/24/2001 3.00E-16 9.00E-14 2.25E-14 3.43E-16 l.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 '1.31E-14 6.00E-13 1.50E-13 12/31/2001 3.16E-16 9.00E-14 2.25E-14 1.31E-16 l.OOE-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/1/2002 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/1/2002 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2002 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/30/2002 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2003 3.41E-16 9.00E-14 2.25E-14 l.l6E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2003 1.31E-16 9.00E-14 2,25E-14 1.39E-16 2.00E-14 5.00E-15 l.82E-16 9.00E-13 2,25E-13 1.53E-14 6.00E-13 l.SOE-13 9/29/2003 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.50E-13 12/29/2003 3.16E-16 9.00E-14 2.25E-14 l.31E-16 l.OOE-14 5.00E-15 6.58E-17 9.00E-l3 2.25E-13 l.91E-14 6.00E-l3 l.50E-13 3/29/2004 3.41E-16 9.00E-14 2.25E-14 2.l6E-16 l.OOE-14 5.00E-15 l.l8E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/27/2004 l.31E-16 9.00E-14 2.25E-14 1.39E-16 l.OOE-14 5.00E-15 1.82E-16 9.00E-13 2.25E-l3 1.53E-14 6.00E-13 l.SOE-13 9/27/2004 3.00E-16 9.00E-14 2.25E-14 3.43E-16 l.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-l3 1.50E-13 12/27/2004 3.16E-16 9.00E-14 2.25E-14 1.31E-16 l .OOE-14 5.00E-15 6.58E-17 9.00E-13 2,25E-13 l.91E-14 6.00E-13 L50E-13 3/28/2005 3.41E-16 9.00E-14 l.25E-14 2.26E-16 2.00E-14 5,00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 l.50E-13 6/29/2005 1.31E-16 9.00E-14 2.25E-14 1.39E-16 l .OOE-14 5.00E-15 l.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 l.50E-13 9/26/2005 3.00E-16 9.00E-14 .2.25E-14 3.43E-16 l.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.50E-13 1/3/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 S.OOE-13 2.25E-13 l.91E-14 6.00E-13 1.50E-13 4/3/2006 3.41E-16 9.00E-14 .2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/2006 1.31E-16 9.00E-14 2.25E-14 l.39E-16 2.00E-14 5.00E-15 l.82E-16 S.OOE-13 2.25E-13 1.53E-14 6.00E-13 l .50E-13 10/2/2006 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 1/1/2006 3.16E-16 9.00E-14 .2.25E-14 l.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 l.91E-14 6.00E-13 1.50E-13 4/2/2007 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2007 1.31E-16 9.00E-14 2.25E-14 1.39E-16 l.OOE-14 5.00E-15 l.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-l3 1.50E-l3 9/30/2007 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 S.OOE-13 2.25E-l3 l.31E-14 6.00E-l3 1.50E-13 12/31/2007 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6S8E-17 9.00E-13 2.25E-l3 l.91E-14 6.00E-13 1.50E-13 3/31/2008 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 l.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 l.SOE-13 6/30/2008 1,31E-16 9.00E-14 2.25E-14 l.39E-16 l.OOE-14 5.00E-15 1.82E-16 .9.00E-13 2.25E-13 l.53E-14 6.00E-13 l.SOE-13 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-3U Effluent Concentration limit = 2E-14 uCi/ml BHV-3T Effluent Concentration limit= 9E-13 uCi/ml BHV-3R Effluent Concentration limit= 6E-13 uCi/ml BHV-3PB ALARAGoal= 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC limit= SE-12 uCi/ml Pre 1994 MPC limit= SE-14 uCi/ml Pre 1994 MPC limit= 2E-12 uCi/ml Pre 1994 MPC Umit = 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 3.00E-16 9.00E-14 2.25E-14 3.43E-16 Z.OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2008 3.16E-16 9.00E-14 2.25E-14 1.31E-16 Z.OOE-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/15/2009 3.41E-16 9.00E-14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 l.lSE-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/15/2009 l.31E-16 9.00E-14 2.25E-14 1.39E-16 Z.OOE-14 5.00E-15 l.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/15/2009 3.00E-16 9.00E-14 2.25E-14 3.43E-16 Z.OOE-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/15/2009 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2010 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2010 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 l.50E-13 9/30/2010 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 l.31E-14 6.00E-13 1.50E-13 12/31/2010 3.16E-16 9.00E,14 2.25E-14 '1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 l.50E-13 4/4/2011 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l .OOE-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/4/2011 1.31E-16 9.00E-14 l.25E-14 1.39E-16 l.OOE-14 5.00E-15 l.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 -:§ 0 :::J -In c 0 :; "--c Cl> CJ c 0 0 Cl> 'tJ (j :::J c 0 'tJ cu a: ('I) :> :::J: al ' C\1 uJ 0 ~ C') .-I LlJ 0 ~ ~~ ~~ ~~ ~~ ~~ ~~ ~~ ~~ ~~ ~~ ~~ ~ ~~ ~l ... ~t> ~~ 1 ...... ~ tc:: ~ .:::;;; ~ .. ::::: r;:: I• ~ I" r-... t:::!. F=r--r+-11- ~ ~ ~ I• b:- ~ ~ I ~ p.. • r-.... "'d" uJ 0 ~ -,, .... ~ ,, ., ~ 11 , ~ .. 110;; ~ ,, ., .. 110;; -~~ ~ ~ ,,, .. .::: 11., ~ .. .::: 11•., ~ .. 110;; 11., ~ .. 110;; ~ 1., .. .:: 11 ... ~ .. .::: , ... ~ .. .:: , ... ~ I, ... ~ ~r;;;;. , ... .... 1 ... ~ ~ -.ol ~ - ..... l•r----...; t--1'1 ~N .:;;;;;; . !-"-~ ~ ~ ~ ... I ~ ~II: _.;:;:r: ..-=:: P"' I.T" -~ ._. I() (!) .-.- uJ I LlJ 0 0 ~ ~ .-.- (areos Bo1) I . o~-das -ao-das eo-das -La-das go-das -go-d as -vo-das £o-des 0 .- C\1 co-das I "0 ro Cl) ~o-des _J + oo-das aa-das (!) C\1 C\1 I ea-das E -~ "0 La-das ro a: ga-das + ,. ga-das 0 C') C\1 -va-das I E ::J -·c £a-des 0 ..c 1-. ca-das + -~a-des ~ (ij ~ R~ ~ oa-das .... ::J "'iii ae-das z E ::J !. ee-das ·c: ro .... ~i+ r-Le-das => + ge-das ge-das ' -ve-das 8e-das ce-das I ~e-das ,...... ro .-.-I I LlJ LlJ 0 0 ~ ~ .- -E :'::::: (.) ::::s -U) 1: 0 ·.; m "--1: C1) (.) 1: 0 (.) «i "-::::s -m z I E ::::s 1: m "-:::l (W') ::> :::r: al ,.... C\J ,.... uJ uJ 0 0 ~ ~ r C') '<t l[) ,.... ,.... uJ I uJ w 0 0 0 ~ ~ ~ ,....(areos Bolr 1'- ""'-::::.. ~-~~ ::::.. 1- ""'-::::.. 1- ""'-::::.. -~~- ,~::::.. ~~·:::. ~""'-~-:::. ~ ""'-.:::::. - :~t:~ ~~~ ~~~~ ~~~ ~-\ ..... ~-::::.. ~ ~t:·:=.. ~· ~ ~-~ \ .... ::::.. t:: - t<::: ;:: ~ r-~ ~N b::.. ~ ~ ~ ~ __ ...... ~~ ~ .... ~ ~ ~ co ,.... I w 0 ~ ,.... -.... .. I ,.,;;;; ,.. ,..... uJ 0 ~ - - . - - . - . . . - co uJ 0 ~ o~-das eo-des so-das Lo-des go-des go-des va-des £o-des co-das ~o-des oo-das 6e-das 95-das Le-das 95-das 95-das ve-das 8e-das ce-des ~6-das 05-das 59-das sa-des La-das gg-das gg-das va-des 8a-das ca-des ~g-das -E -0 ::::J -(/) c 0 +=i C'tl ... -c G) (.) c 0 (.) 0 (") C\1 I E ::::J "i: 0 .s:. 1- C") > :I: ca ,.... I w 0 ~ .... C\J (I') w w 0 0 ~ ~ 4 1•1=:: 4 1•1=:: I•~ 4 :•F:: I•~ 4 I•F:: 4 I•F:: 4 !4 !:::: 4 ~!:::: 4 •=:::: .I~ • ,40::::: 4 :·I~ ·~ • •< • - ~ ~ I' ~ ""= ~ """ l.() ,.... w I w 0 0 ~ ~ (aiB:lS 60lJ ~ ~ ~ ~ t;. p. ~ ~ ~ ~ S! s: ~ ~ ~ s: ~ ;::.• ~ .... ~ r--. • ~ ~ r=::: ~I .... c.o w 0 ~ . I'-,.... I w 0 ~ ,.... . - - - - - - - . - - . . - co w 0 ~ o~-das 6o-das so-das Lo-das go-d as so-das vo-das 8o-das co-das ~o-das oo-das 55-das 86-das L6-das 95-das 95-das 175-das 86-das c6-das ~5-das 05-das 6s-das gg-das Ls-das gg-das ss-das vs-das 8s-das cs-das ~g-das -:§ 0 ::::s -Ill s::::: 0 :;:::; ca '--s::::: Q) () s::::: 0 0 CD N N I E ::::s "C ca a: ('t) > ::I: al ,.,.. C\J ..... w ' w 0 0 q q io-io' +<= . (") ""'" I!) ..... w ' w w 0 0 0 q q q (a1eas DOlJ ~ ~~-~ ~r-~ ~~-~ r-b. ~~ ~ :-~ :-r--.. '"'~'-r--.. :-r--.. ~:-r--.. "'r-r--.. "'~'-..,. ::::: ..... ~:::::: -..... "'~'-..... ... •c:::::::; ~ """' __.. !"-" ~ ~ ~ ~ H :-.... ~ (!) w 0 q I ..,......;;; ~ ~tl It fi?"' I'-..... ' w 0 q - - - - - - co w 0 q o~-das 6o-das so-das Lo-des go-des go-des vo-das so-das Go-des ~o-des oo-das 66-das 86-das L6·das 95-das 95-das v6·das £6-das G6·das ~5-das 05-das 6s-das ss-das Ls-das gg-das gg-das vs-das ss-das Gs-das ~s-das 1.00E-11 1.00E-12 1.00E-13 Q) Cii 0 cm.OOE-14 Ol 0 _J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 6E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCilml Pre 1994 ALARA Goal= 1E-12 uCi/ml /I • • ~ y 1 ~/\ 1\ 7r t _t_ ~ 1\ L\ Jt .,. ~T~~ ~'I r'1·,.. v ''' ~~v, ' . ' . ~ N ~ ~ ~ m ~ ro m o ~ ro ro ro ro ro ro ro ro ro m m ~ ~ ~ n ~ ~ n ~ n n ~ ID ID ID ill ill ill ill ID ID ID ill w w w w w w w w w w w N m I Q_ ID w . ~ ~ m m 6.. 6. m m w w BHV-3 Lead-21 0 Concentrations (uCi/ml) .1.. Jt. ~ }(.. JJ }(.. }(.. Jt. ~ ~ )! 1t. ~ ~ ~ ~ vvvvvvvvvvvvvvv II "\J ~ m 6.. m w m m 6.. ID w ~ m ' Q_ m w ro m 6.. m w m m 6.. m w 0 0 6.. m w ~ 0 6.. m w ' N 0 I Q_ m w ~ 0 6.. ID w ~ 0 6.. ID w ~ 0 ' Q_ ID w m 0 6.. m w ~ 0 ' Q_ m w ro 0 6.. ID w m 0 6.. m w 0 ~ 6.. ID w TAB4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-4U Effluent Concentration Limit= ZE-14 uCi/ml BHV-4T Effluent Concentration Limit= 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal= 2.2SE-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = .l.SE-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit= 2E-l2 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 5.20E-15 5.00E-12 .1.25E-12 2.93E-15 S.OOE-14 2.00E-14 2.74E-15 2.00E-12 5.00E-13 1.84E-14 4.00E-12 l .OOE-12 12/14/1981 4.53E-15 5.00E-12 1.25E-12 1.78E-15 S.OOE-14 2.00E-14 2.29E-15 2.00E-12 S.OOE-13 2.54E-14 4.00E-12 l.OOE-12 3/29/1982 1.06E-15 5.00E-12 1.25E-12 1.42E-14 S.OOE-14 2.00E-14 1.07E-15 2.00E-12 S.OOE-13 2.31E-14 4.00E-12 1.00E-12 6/30/1982 6.03E-15 S.OOE-12 1.25E-12 1.57E-14 S.OOE-14 2.00E-14 2.62E-15 2.00E-12 S.OOE-13 2.25E-14 4.00E-12 l.OOE-12 9/27/1982 1.26E-14 S.OOE-12 1.25E-12 7.58E-16 8.00E-14 2.00E-14 5.35E-15 2.00E-12 S.OOE-13 2.68E-14 4.00E-12 1.00E-12 1/3/1983 4.33E-15 S.OOE-12 1.25E-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 l.OOE-12 4/4/1983 1.25E-15 S.OOE-12 1.25E-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 1.00E-12 6/30/1983 3.73E-16 S.OOE-12 1.25E-12 9.43E-16 S.OOE-14 2.00E-14 4.13E-16 z.OOE-12 S.OOE-13 1.20E-14 4.00E-12 l.OOE-12 10/3/1983 2.54E-16 s.OOE-12 1.25E-12 1.51E-16 S.OOE-14 2.00E-14 2.65E-16 2.00E-12 ,S.OOE-13 2.50E-14 4.00E-12 l.OOE-12 1/3/1984 2.76E-15 S.OOE-12 1.25E-12 1.60E-16 S.OOE-14 2.00E-14 1.05E-16 2.00E-12 ,S.OOE-13 1.59E-16 4.00E-12 l .OOE-12 4/2/1984 4.27E-16 S.OOE-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 l.OOE-12 S.OOE-13 3.67E-14 4.00E-12 l.OOE-12 7/2/1984 2.57E-15 S.OOE-12 1.25E-12 1.36E-16 8.00E-14 2.00E-14 1.11E-16 2.00E-12 S.OOE-13 1.58E-14 4.00E-12 LOOE-12 10/1/1984 4.18E-16 S.OOE-12 1.25E-12 3.54E-16 8.00E-14 2.00E-14 l.lOE-17 .2.00E-12 5.00E-13 9.83E-15 /I.OOE-12 l.OOE-12 1/2/1985 5.30E-17 S.OOE-12 1.25E-12 3.55E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 5.00E-13 2.57E-14 4.00E-12 l.OOE-12 4/1/1985 l.OOE-16 S.OOE-12 1.25E-12 6.00E-16 8.00E-14 2.00E-14 4.35E-17 l.OOE-12 S.OOE-13 5.02E-15 4.00E-12 l.OOE-12 7/1/1985 9.36E-16 S.OOE-12 1.2SE-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 .l.OOE-12 S.OOE-13 7.48E-15 4.00E-12 l.OOE-12 9/30/1985 1.46E-15 S.OOE-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 5.38E-16 l.OOE-12 S.OOE-13 7.86E-15 4.00E-12 l.OOE-12 1/2/1986 8.40E-15 S.OOE-12 L25E-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 Z.OOE-12 5.00E-13 2.12E-14 4.00E-12 l.OOE-12 4/1/1986 5.79E-15 5.00E-12 L25E-12 5.80E-16 S.OOE-14 2.00E-14 1.34E-15 2.00E-12 5.00E-13 1.33E-14 4.00E-12 l.OOE-12 6/30/1986 5.19E-15 5.00E-12 1.25E-12 7.83E-16 8.00E-14 2.00E-14 2.20E-15 l.OOE-12 5.00E-13 7.14E-16 4.00E-12 l.OOE-12 10/27/1986 4.60E-15 5.00E-12 1.25E-12 4.67E-16 S.OOE-14 2.00E-14 2.37E-15 2.00E-12 5.00E-13 1.13E-14 4.00E-12 l.OOE-12 12/15/1986 2.75E-15 5.00E-12 1.25E-12 5.90E-16 8.00E-14 2.00E-14 9.39E-16 l.OOE-12 5.00E-13 1.20E-14 II.OOE-12 l.OOE-12 3/16/1987 4.64E-15 5.00E-12 1.25E-12 L18E-15 S.OOE-14 2.00E-14 4.97E-16 2.00E-12 5.00E-13 5.89E-14 4.00E-12 l.OOE-12 5/11/1987 4.35E-15 5.00E-12 1.25E-12 1.23E-14 S.OOE-14 2.00E-14 1.13E-15 l.OOE-12 5.00E-13 2.21E-14 4.00E-12 l.OOE-12 9/9/1987 6.39E-15 S.OOE-12 1.25E-12 1.50E-14 8.00E-14 2.00E-14 2.26E-15 2.00E-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12 11/2/1987 6.72E-15 5.00E-12 1.25E-12 4.53E-16 8.00E-14 2.00E-14 2.20E-15 l.OOE-12 5.00E-13 2.55E-14 4.00E-12 l.OOE-12 2/16/1988 1.91E-15 5.00E-12 1.25E-12 1.35E-14 8.00E-14 .l.OOE-14 4.42E-16 2.00E-12 5.00E-13 4.44E-14 4.00E-12 1.00E-12 5/18/1988 1.78E-14 5.00E-12 1.25E-12 4.39E-14 8.00E-14 l.OOE-14 4.92E-16 l.OOE-12 5.00E-13 1.38E-14 4.00E-12 1.00E-12 8/15/1988 7.56E-15 5.00E-12 1.25E-12 3.31E-14 8.00E-14 l.OOE-14 1.51E-15 l.OOE-12 5.00E-13 1.97E-14 4.00E-12 1.00E-12 11/14/1988 1.47E-14 5.00E-12 1.25E-12 1.56E-15 8.00E-14 2.00E-14 2.57E-15 2.00E-12 5.00E-13 2.12E-14 4.00E-12 1.00E-12 2/13/1989 2.47E-15 5.00E-12 1.25E-12 3.14E-15 8.00E-14 l.OOE-14 6.94E-16 2.00E-12 5.00E-13 2.12E-14 4.00E-12 1.00E-12 5/15/1989 2.50E-16 5.00E-12 1.25E-12 7.68E-15 8.00E-14 2.00E-14 9.03E-16 2.00E-12 5.00E-13 8.05E-15 4.00E-12 l.OOE-12 8/14/1989 6.50E-15 5.00E-12 1.25E-12 4.72E-15 8.00E-14 2.00E-14 2.35E-15 2.00E-12 5.00E-13 9.95E-15 4.00E-12 1.00E-12 11/13/1989 9.63E-15 5.00E-12 1.25E-12 4.05E-15 8.00E-14 2.00E-14 4.03E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 l.OOE-12 2/12/1990 8.92E-15 5.00E-12 1.25E-12 3.56E-15 8.00E-14 2.00E-14 2.89E-15 2.00E-12 5.00E-13 2.69E-14 4.00E-12 l.OOE-12 5/14/1990 8.90E-15 5.00E-12 1.25E-12 3.58E-15 8.00E-14 2.00E-14 2.33E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 l.OOE-12 8/13/1990 1.92E-15 5.00E-12 1.25E-12 1.87E-15 8.00E-14 2.00E-14 5.06E-16 2.00E-12 5.00E-13 8.86E-15 4.00E-12 l.OOE-12 11/12/1990 2.91E-15 5.00E-12 1.25E-12 2.25E-17 8.00E-14 2.00E-14 1.08E-15 2.00E-12 5.00E-13 2.19E-14 4.00E-12 1.00E-12 2/11/1991 1.67E-16 5.00E-12 1.25E-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 5.00E-13 4.19E-14 4.00E-12 1.00E-12 5/13/1991 1.87E-16 5.00E-12 1.25E-12 2.61E-15 S.OOE-14 2.00E-14 3.54E-16 2.00E-12 5.00E-13 1.40E-14 4.00E-12 l.OOE-12 8/12/1991 4.85E-16 5.00E-12 1.25E-12 4.38E-16 S.OOE-14 2.00E-14 1.27E-16 2.00E-12 5.00E-13 2.20E-14 4.00E-12 1.00E-12 11/11/1991 1.77E-16 5.00E-12 1.25E-12 1.46E-16 S.OOE-14 2.00E-14 3.76E-17 2.00E-12 5.00E-13 1.15E-14 4.00E-12 1.00E-12 2/10/1992 1.83E-16 S.OOE-12 1.25E-12 '1.95E-15 S.OOE-14 2.00E-14 1.33E-16 2.00E-12 S.OOE-13 3.35E-14 4.00E-12 1.00E-12 5/11/1992 4.40E-16 5,00E-12 1.25E-12 2.56E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12 8/10/1992 9.09E-17 5.00E-12 1.25E-12 1.15E-16 8.00E-14 2.00E-14 4.SOE-17 2.00E-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12 11/9/1992 2.07E-16 5.00E-12 1.25E-12 1.00E-16 S.OOE-14 2.00E-14 3.62E-17 2.00E-12 5.00E-13 2.24E-14 4.00E-12 l.OOE-12 2/9/1993 1.73E-16 5.00E-12 1.25E-12 2.76E-17 S.OOE-14 2.00E-14 2.89E-17 2.00E-12 5.00E-13 .3.08E-14 4.00E-12 l.OOE-12 5/10/1993 2.70E-17 5.00E-12 1.25E-12 2.50E-17 S.OOE-14 2.00E-14 8.74E-17 2.00E-12 5.00E-13 l.25E-14 4.00E-12 l.OOE-12 8/10/1993 9.00E-17 S.OOE-12 1.25E-12 1.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 l.SOE-14 4.00E-12 l.OOE-12 11/8/1993 1.00E-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 G.OOE-17 2.00E-12 S.OOE-13 1.75E-14 4.00E-12 l.OOE-12 2/7/1994 l.lOE-16 S.OOE-12 1.2SE-12 3.38E-16 S.OOE-14 2.00E-14 2.21E-16 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 S/9/1994 3.80E-16 S.OOE-12 1,25E-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 S.OOE-13 1.73E-14 4.00E-12 l.OOE-12 8/9/1994 3.85E-16 5.00E-12 1.2SE-12 3.53E-16 S.OOE-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 l.OOE-16 4.00E-12 l.OOE-12 11/7/1994 6.21E-17 5.00E-12 l.25E-12 9.70E-17 S.OOE-14 2.00E-14 l.96E-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-4U Effluent Concentration Limit= 2E-14 uCi/ml BHV-4T Effluent Concentration Limit= 9E-13 uCi/ml BHV-4R Effluent Concentration Limit= 6E-13 uCi/ml BHV-4PB ALARAGoal= Z.ZSE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= Z.ZSE-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC limit: SE-14 uCi/ml Pre 1994 MPC Limit = ZE-12 uCi/ml Pre 1994 MPC Limit: 4E-1Z uCi/ml Pre 1994 ALARA GOAL= 1.ZSE-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 3.70E-16 9.00E-14 2.25E-14 9.80E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 8.84E-15 6.00E-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 2.86E-16 2.00E-14 5.00E-15 1.90E-16 9.00E-13 2.25E-13 2.90E-15 6.00E-13 1.50E-13 8/9/1995 1.45E-16 9.00E-14 2.25E-14 2.31E-15 2.00E-14 5.00E-15 7.10E-17 9.00E-13 2.25E-13 2.70E-15 6.00E-13 1.50E-13 11/11/1995 1.43E-14 9.00E-14 2.25E-14 5.70E-15 2.00E-14 5.00E-15 2.61E-15 9.00E-13 2.25E-13 5.60E-15 6.00E-13 1.50E-13 2/5/1996 1.19E-14 9.00E-14 2.25E-14 3.80E-16 Z.OOE-14 5.00E-15 6.10E-15 9.00E-13 2.25E-13 6.48E-15 6.00E-13 1.50E-13 5/6/1996 4.55E-16 9.00E-14 2.25E-14 3.57E-15 2.00E-14 5.00E-15 2.84E-16 9.00E-13 2.25E-13 7.68E-15 6.00E-13 1.50E-13 8/5/1996 7.78E-16 9.00E-14 2.25E-14 3.51E-15 .2.00E-14 5.00E-15 1.69E-16 9.00E-13 2.25E-13 4.90E-15 6.00E-13 1.50E-13 11/6/1996 1.36E-15 9.00E-14 2.25E-14 l .OOE-16 2.00E-14 5.00E-15 4.21E-16 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 2/6/1997 1.00E-16 9.00E-14 2.25E-14 1.40E-16 l.OOE-14 5.00E-15 1.03E-16 9.00E-13 2.25E-13 6.76E-15 6.00E-13 1.50E-13 5/5/1997 1.00E-16 9.00E-14 2.25E-14 4.00E-16 2.00E-14 5.00E-15 2.24E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 1.50E-13 8/11/1997 4.74E-16 9.00E-14 2.25E-14 9.07E-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.55E-15 6.00E-13 1.50E-13 1/5/1998 8.31E-16 9.00E-14 2.25E-14 4.82E-16 l.OOE-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 5.28E-15 6.00E-13 1.50E-13 4/28/1998 3.32E-16 9.00E-14 2.25E-14 4.43E-15 z.OOE-14 5.00E-15 1.21E-16 9.00E-13 2.25E-13 7.43E-15 6.00E-13 1.50E-13 7/31/1998 4.60E-16 9.00E-14 2.25E-14 9.02E-16 2.00E-14 5.00E-15 3.54E-16 9.00E-13 2.25E-13 6.91E-15 6.00E-13 1.50E-13 9/28/1998 4.08E-16 9.00E-14 2.25E-14 4.93E-16 l.OOE-14 5.00E-15 2.53E-16 9.00E-13 2.25E-13 4.52E-15 6.00E-13 1.50E-13 12/28/1998 7.72E-16 9.00E-14 2.25E-14 3.75E-16 Z.OOE-14 5.00E-15 3.43E-16 9.00E-13 2.25E-13 6.73E-15 6.00E-13 l .50E-13 3/29/1999 5.11E-16 9.00E-14 2.25E-14 4.70E-16 2.00E-14 5.00E-15 3.70E-16 9.00E-13 2.25E-13 8.96E-15 6.00E-13 l.SOE-13 7/3/1999 5.90E-16 9.00E-14 2.25E-14 9.89E-16 Z.OOE-14 5.00E-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E-13 1.50E-13 9/27/1999 1.70E-15 9.00E-14 2.25E-14 7.50E-16 2.00E-14 5.00E-15 4.61E-16 9.00E-13 2.25E-13 7.86E-15 6.00E-13 1.50E-13 12/28/1999 1.03E-15 9.00E-14 2.25E-14 7.50E-16 Z.OOE-14 5.00E-15 2.43E-16 9.00E-13 2.25E-13 6.42E-15 6.00E-13 1.50E-13 3/27/2000 l.OOE-16 9.00E-14 .2.25E-14 2.13E-16 Z.OOE-14 5.00E-15 2.20E-16 9.00E-13 2.25E-13 S.61E-15 6.00E-13 l.SOE-13 6/26/2000 1.75E-16 9.00E-14 2.25E-14 3.08E-16 Z.OOE-14 5.00E-15 1.11E-16 9.00E-13 2.25E-13 3.92E-15 6.00E-13 1.50E-13 9/26/2000 3.65E-16 9.00E-14 2.25E-14 2.01E-16 Z.OOE-14 5.00E-15 2.24E-16 9.00E-13 2.25E-13 7.79E-15 6.00E-13 1.50E-13 12/26/2000 2.27E-16 9.00E-14 2.25E-14 1.00E-16 Z.OOE-14 5.00E-15 4.35E-16 9.00E-13 ~.25E-13 8.4SE-15 6.00E-13 1.50E-13 3/26/2001 1.45E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.37E-15 6.00E-13 1.50E-13 7/2/2001 1.00E-16 9.00E-14 2.25E-14 1.05E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.99E-15 6.00E-13 1.50E·13 9/24/2001 1.91E-16 9.00E-14 .2.25E-14 l.OOE-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 .2.25E-13 8.04E-15 6.00E-13 1.50E-13 12/31/2001 1.38E-16 9.00E-14 2.25E-14 2.05E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.83E-15 6.00E-13 1.50E-13 4/1/2002 2.20E-16 9.00E-14 1.25E-14 3.38E-16 2.00E-14 5.00E-15 1.26E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13 7/1/2002 1.97E-16 9.00E-14 2.25E-14 4.10E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 .2.25E-13 7.40E-15 6.00E-13 1.50E-13 9/30/2002 2.30E-16 9.00E-14 2.25E-14 2.42E-16 2.00E-14 5.00E-15 1.56E-16 9.00E-13 z.25E-13 4.21E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 1.92E-16 2.00E-14 5.00E-15 t.OOE-16 g.OOE-13 2.25E-13 9.42E-15 6.00E-13 1.50E-13 '3/31/2003 2.50E-16 S.OOE-14 2.25E-14 1.69E-16 2.00E-14 5.00E-15 1.29E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 1.50E-13 6/30/2003 l.OOE-16 9.00E-14 2.25E-14 2.87E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.20E-15 6.00E-13 1.50E-13 9/29/2003 1.00E-16 9.00E-14 2.25E-14 8.53E-16 2.00E-14 S.OOE-15 3.32E-16 9.00E-13 2.25E-13 8.69E-15 6.00E-13 1.50E-13 12/29/2003 1.02E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 1.49E-15 9.00E-13 2.25E-13 9.45E-15 6.00E-13 1.50E-13 3/29/2004 .l.OOE-16 9.00E-14 2.25E-14 1.26E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 2.00E-15 6.00E-13 1.50E-13 6/27/2004 l.OOE-16 9.00E-14 2.25E-14 2.53E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 3.23E-15 6.00E-13 1.50E-13 9/27/2004 1.00E-16 9.00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.68E-15 6.00E-13 1.50E-13 12/27/2004 l.OOE-16 9.00E-14 2.25E-14 2.30E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13 3/28/2005 'l.OOE-16 9.00E-14 2.25E-14 2.66E-16 2.00E-14 S.OOE-15 3.15E-16 9.00E-13 2.25E-13 9.22E-15 6.00E-13 1.50E-13 6/29/2005 1.47E-16 9.00E-14 2.25E-14 1.45E-15 2.00E-14 S.OOE-15 1.42E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13 9/26/2005 2.01E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 S.OOE-15 4.80E-16 9.00E-13 2.25E-13 2.12E-14 G.OOE-13 1.50E-13 1/3/2006 4.54E-16 9.00E-14 2.25E-14 1.24E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.60E-14 6.00E-13 1.50E-13 4/3/2006 1.99E-16 9.00E-14 2.25E-14 1.32E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.36E-15 6.00E-13 1.50E-13 7/3/2006 2.76E-16 9.00E-14 2.25E-14 2.63E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 10/2/2006 4.97E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13 1/1/2007 6.46E-16 9.00E-14 2.25E-14 2.81E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 2,10E-14 6.00E-13 1.50E-13 4/2/2007 7.08E-16 9.00E-14 2.25E-14 3.20E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 7/2/2007 9.41E-16 9.00E-14 2.25E-14 1.46E-16 Z.OOE-14 S.OOE-15 1.99E-16 9.00E-13 2.25E·13 2.56E-14 6.00E-13 1.50E-13 9/30/2007 3.30E-16 9.00E-14 2.25E-14 5.50E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.57E-15 6.00E-13 1.50E-13 12/31/2007 1.42 E-15 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 9.93E-15 6.00E-13 1.50E-13 3/31/2008 1.25E-16 9.00E-14 2.25E-14 '7,72E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 4.09E-15 6.00E-13 1.50E-13 6/30/2008 1.28E-15 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 3.61E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-4U Effluent Concentration Limit= ZE-14 uCi/ml BHV-4T Effluent Concentration limit= 9E-13 uCi/ml BHV-4R Effluent Concentration Limit= 6E-13 uCi/ml BHV-4PB AlARAGoal= 2.25E-14 uCi/ml AlARAGoal= SE-13 uCi/ml AlARAGoal= 2.25E-13 uCi/ml AlARAGoal = l.SE-13 uCi/ml Pre 1994 MPC limit= SE-12 uCi/ml Pre 1994 MPC Limit-BE-14 uCi/ml Pre 1994 MPC limit: ZE-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 AlARA GOAL= l.ZSE-12 uCi/ml Pre 1994 AlARA GOAL = SE-13 uCi/ml Pre 1994 AlARA GOAL= 1E-l2 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 12/31/2008 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/15/2009 1.56E-15 9.00E-14 2.25E-14 4.57E-16 2.00E-14 S.OOE-15 2.99E-16 9.00E-13 2.25E-13 4.97E-15 6.00E-13 1.50E-13 6/15/2009 5.67E-17 9.00E-14 2.25E-14 2.17E-16 2.00E-14 S.OOE-15 1.51E-16 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13 9/15/2009 4.05E-15 9.00E-14 2.25E-14 1.45E-15 2.00E-14 S.OOE-15 2.52E-16 9.00E-13 2.25E-13 1.24E-14 6.00E-13 1.50E-13 12/15/2009 6.50E-15 9.00E-14 2.25E-14 3.48E-16 2.00E-14 5.00E-15 1.33E-16 9.00E-13 2.25E-13 7.60E-15 6.00E-13 1.50E-13 3/31/2010 6.01E-15 9.00E-14 2.25E-14 1.26E-16 2.00E-14 S.OOE-15 1.34E-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 6/30/2010 2.33E-15 9.00E-14 2.25E-14 7.29E-16 2.00E-14 S.OOE-15 2.66E-16 9.00E-13 2.25E-13 3.27E-15 6.00E-13 1.50E-13 9/30/2010 4.77E-15 9.00E-14 2.25E-14 1.80E-15 2.00E-14 S.OOE-15 8.23E-16 9.00E-13 2.25E-13 5.11E-15 6.00E-13 1.50E-13 12/31/2010 3.93E-15 9.00E-14 2.25E-14 3.90E-16 2.00E-14 S.OOE-15 2.56E-16 9.00E-13 2.25E-13 1.13E-14 6.00E-13 l .SOE-13 4/4/2011 1.29E-15 9.00E-14 2.25E-14 1.40E-16 2.00E-14 S.OOE-15 1.58E-16 9.00E-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 7/4/2011 3.30E-15 9.00E-14 2.25E-14 5.44E-16 2.00E-14 5.00E-15 4.18E-16 9.00E-13 2.25E-13 8.26E-15 6.00E-13 1.50E-13 -E :::::: 0 ~ -en c 0 ·; "--c Q) (,) c 0 0 Q) "C (,) ~ c 0 "C ca a: o::t > :I: m N C') .-.-I I w w 0 0 ~ ~ : • ~ .. 1.-.: ~ 4 ~N --«:: • Jr ~ K ~ ~ ~ ~ • ~ ~ ;: 4C::: ..... ~ ~ ...... ~,_. I•...,. !llt.....r-- ~"' ..... .... "\.. "1. •C:::::.. .. ~ -... > ~ ~ "'55: ~ .-I w 0 ~ .- -t:::=+ ~ ~-.g ~~ :::.:.. .. r-"'-o~-das ~ !.-·~ ~ .... 6o-das .... ...._ -so-das --• ~ ~r--. ~ ·~ La-das go-das go-das =-.. "'i: ..... "'4:::::,. ~ ..:::::: vo-das "I ........ ::;., .. ~ >4 ~~ 1-1-i:::>!. ,..:;;; 1.-"1' -p~ ~ -~ .. ~ I-p-. ~ :It !<: ~ ~~ -~ 8o-das 0 .-N co-das I "'C ro Q) w-das ...J + oo-das <0 66-das N ~ 96-das E :::l '5 L6·das ro a: 96-das + ~ 96-das 0 C') v6-das ~ E -:::l 1---86-das ·;:: 0 ..c ~~ =-· ff 1- c6-das + ...... ~ ~6-das ,jii :::::!!;;. ""' 06-das ~ :::l -.J J. V"' ro 69-das z E :::l ...._ ee-das ·c: ro ~ ... r--. ~ .. • .... La-das :::> + gg-das H--r-.... .::::::0 gg-das ve-das 89-das ce-das ~ '~""' ~g-das ll) <0 1'-<0 .-..-.-.- I I w I w w w 0 0 0 0 ~ ~ ~ ~ .-.-,..- (a1eos 6o1) 1.00E-11 1.00E-12 1.00E-13 Q) co 0 U)1.00E-14 0> 0 ....J - 1.00E-15 1.00E-16 1.00E-17 ~ \ .... CX) I a. Q) U) Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E-12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml t ~ • \ v • 1)1 f ~ ~ I \ I ~ .. C\1 C') """ II) (0 1'-CX) C) 0 .... CX) CX) CX) CX) CX) CX) CX) CX) C) C) I I I 6.. 6.. 6.. I I I 6.. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) U) U) U) U) U) U) U) U) U) U) l"l ... v"1 .1 v • C\1 C') """ C) C) C) 6.. 6.. 6.. Q) Q) Q) U) U) U) BHV-4 Uranium-Natural Concentrations (uCi/ml) ~ 1'1.. \/1 ' \ ~ ~ ~ ~ ~ 9" Will. • T • 1r H 1 • I'• ... t 1\J' J 1 II VI ·v\ I ~ II) (0 1'-CX) C) 0 .... C\1 C') """ II) (0 1'-CX) C) 0 C) C) C) C) C) 0 0 0 0 0 0 0 0 0 0 .... I 6.. 6.. 6.. I 6.. I 6.. 6.. 6.. 6.. 6.. I I 6.. 6.. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) U) U) U) U) U) U) U) U) U) U) U) U) U) U) U) U) - rn c 0 ·.;:; ca """ -c G) () c 0 (.) 0 C") ~ E :::s 'i: 0 .c 1- "'::t > :I: m ..... Li..J 0 0 ~~~ C\1 ('I) ..... ..... I I w w 0 0 ~ ~ ..... ~ - - lr ;;;.,-..... -,.... ... ;;;;;..__ r- ~ ~~ .... '""' ..... ....:::: _.;19' """ 10 ..... Li..J Li..J 0 0 <=! ~ (aiBOS DOl) ..... I-f-~ .... ~ o~-das !.I-~ it+--!="' 6o-das so-das ...... I ~:.-~ ~ ~ La-das go-d as so-das I~ ~ ~-~ ~ Itt~ ~ ~ vo-das E:o-das GO-das w-das .J~ ~ oo-das 66-das ~~ 86-das h ... t--r.... L6-das 96-das 96-das ---. ~~ -l•r-~ v6-das 86-das 7 L- _. G6-das ... ~ -~6-das 06-das 6s-das sa-d as La-das It ga-d as J,:; ~ sa-d as ~ f:::::::: t;:. • ~ 1-1-- vs-das E:s-das Gs-das ~s-das <D "' ..... ..... I I w w 0 0 ~ <=! ..... 1.00E-11 1.00E-12 1.00E-13 .--...1 .OOE-14 Q) «i t) (/) Ol 0 .....J -1.00E-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit= 9E-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml Pre 1994 MPC Limit= 2E-12uCi/ml Pre 1994 ALARA Goal= 5E-13 uCi/ml I 1\. ~1 ..... t + ... v. 1\1 f\ I \ ..-co I a. Q) (/) " ~ ~ ' C\j (") co co 6. 6. Q) Q) (/) (/) ~ '<:t co 6.. Q) (/) \l + 1.{) co I a. Q) (/) co co 6.. Q) (/) !0 6.. Q) (/) rr co co I a. Q) (/) en co I a. Q) (/) • 0 en I a. Q) (/) ,. 1\ Jl tt .... ..-en I a. Q) (/) ..., C\j 0> I .... a. Q) (/) BHV-4 Radium-226 Concentrations (uCi/ml) \ ' ' • 4\ I W\i (") en 6.. Q) (/) '<:t en 6.. Q) (/) 1.{) en I a. Q) (/) II ."" 1\ '' • ,. \ , ... ·v.~ ~ v. co en 6.. Q) (/) r-.... en I a. Q) (/) co en 6.. Q) (/) en en I a. Q) (/) 0 0 I a. Q) (/) 1 •II I 1\1\ iA.NJ J¥\ ..-0 I a. Q) (/) C\j 0 I a. Q) (/) (") '<:t 0 0 6. 6.. Q) Q) (/) (/) 1.{) 0 6.. Q) (/) co 0 6.. Q) (/) • I Al r-.... 0 I a. Q) (/) co 0 6.. Q) (/) \1t ,~, ¥~ ~ en 0 I a. Q) (/) 0 ..- 6.. Q) (/) 1.00E-11 1.00E-12 1.00E-13 Q) (ii u oo 1.00E-14 Cl 0 __J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 6E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCi/ml Pre 1994 ALAR A Goal = 1 E-12 uCi/ml • /' .. 1\ • ..... .... 1,..........1 1\ 1 .. •t \.-A~\./\4\ 1\ ,.... co I c. Q) (/) C\1 co 6.. Q) (/) " ' C') co I c. Q) (/) v /'J~lf\ I \1 ¥~ 'vi V ~ "<:t L() co co 6.. 6. Q) Q) (/) (f) CD co I c. Q) (/) ,...._ co 6.. Q) (/) co 0) co co I I c. c. Q) Q) (/) (/) I 0 0) 6.. Q) (/) ,.... 0) 6.. Q) (/) C\1 0) I c. Q) (/) C') 0) 6.. Q) (/) "<:t 0) I c. Q) (/) BHV-4 Lead-21 0 Concentrations (uCi/ml) \ I ~ L() 0) I c. Q) (/) • ..., . CD 0) 6.. Q) (/) ,...._ 0) I c. Q) (/) • co 0) 6.. Q) (/) 0) 0) 6.. Q) (/) v ..... 0 0 I c. Q) (/) v • ,.... 0 6.. Q) (/) ... -. C\1 0 6.. Q) (/) C') 0 6.. Q) (f) w ~\ AI I ~ IJ ' "<:t 0 6.. Q) (/) L() 0 I c. Q) (/) .. ~ j'¥ CD 0 6.. Q) (f) ,...._ 0 6.. Q) (/) • JL co 0 I c. Q) (f) tf ... ... 0) 0 6.. Q) (/) r ~ 0 ,.... 6.. Q) (f) TABS BHV -5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit= 9E-13 uCi/ml BHV-SR Effluent Concentration Limit= 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit-SE-12 uCi/ml Pre 1994 MPC Limit = SE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.44E-15 5.00E-12 1.25E-12 l.S3E-15 8.00E-14 2.00E-14 7.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-12 1.00E-12 12/14/1981 4.84E-15 5.00E-12 1.25E-12 2.78E-15 8.00E-14 2.00E-14 1.84E-15 2.00E-12 5.00E-13 :L53E-14 4.00E-12 l.OOE-12 3/29/1982 1.04E-15 5.00E-12 1.25E-12 2.62E-15 8.00E-14 2.00E-14 1.11E-15 2.00E-12 5.00E-13 2.98E-14 4.00E-12 l.OOE-12 6/30/1982 3.61E-15 5.00E-12 1.25E-12 7.61E-15 S.OOE-14 2.00E-14 1.39E-15 2.00E-12 5.00E-13 1.80E-15 4.00E-12 l.OOE-12 9/27/1982 1.71E-14 5.00E-12 1.25E-12 9.46E-15 8.00E·14 2.00E-14 3.80E-15 2.00E-12 S.OOE-13 2.35E-14 4.00E-12 1.00E-12 1/3/1983 1.90E-14 5.00E-12 1.25E-12 5.77E-15 8.00E-14 2.00E-14 9.34E-17 2.00E-12 5.00E-13 4.32E-14 4.00E-12 .l.OOE-12 4/4/1983 5.00E-12 1.25E-12 2.33E-15 8.00E-14 2.00E-14 5.93E-16 2.00E-12 S.OOE-13 3.01E-14 4.00E-12 l.OOE-12 6/30/1983 7.62E-16 S.OOE-12 1.25E-12 3.25E-15 8.00E-14 2.00E-14 6.28E-15 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 l.OOE-12 10/3/1983 4.86E-16 S.OOE-12 1.25E-12 1.10E-15 8.00E-14 2.00E-14 3.63E-16 2.00E-12 5.00E-13 2.08E-14 4.00E-12 l.OOE-12 1/3/1984 6.96E-15 S.OOE-12 1.25E-12 9.69E-16 8.00E-14 2.00E-14 9.60E-16 2.00E-12 S.OOE-13 1.83E-14 4.00E-12 l.OOE-12 4/2/1984 1.64E-15 5.00E-12 1.25E-12 L34E-15 8.00E-14 2.00E-14 3.88E-15 2.00E-12 S.OOE-13 4.67E-14 4.00E-12 l.OOE-12 7/2/1984 1.12E-15 S.OOE-12 1.25E-12 1.92E-15 8.00E-14 2.00E-14 3.31E-15 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 l.OOE-12 10/1/1984 1.11E-15 S.OOE-12 1.25E-12 3.13E-16 B.OOE-14 2.00E-14 4.21E-16 2.00E-12 S.OOE-13 1.57E-14 4.00E-12 l.OOE-12 1/2/1985 7.32E-16 S.OOE-12 1.25E-12 6.71E-16 8.00E-14 2.00E-14 4.94E-16 l.OOE-12 S.OOE-13 2.42E-14 4.00E-12 l.OOE-12 4/1/1985 2.36E-16 5.00E-12 1.25E-12 S.43E-16 8.00E-14 2.00E-14 2.71E-16 2.00E-12 5.00E-13 1.25E-14 4.00E-12 l.OOE-12 7/1/1985 7.58E-16 S.OOE-12 '1.25E-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 S.OOE-13 2.15E-14 4.00E-12 l.OOE-12 9/30/1985 7.47E-15 6.00E-12 1.25E-12 1.16E-15 8.00E-14 2.00E-14 2.19E-15 2.00E-12 5.00E-13 9.20E-15 4.00E-12 LOOE-12 1/2/1986 1.75E-14 S.OOE-12 1.25E-12 7.24E-15 8.00E-14 2.00E-14 3.83E-15 z.OOE-12 S.OOE-13 1.13E-16 4.00E-12 1.00E-12 4/1/1986 2.99E-14 S.OOE-12 1.25E-12 7.64E-15 8.00E-14 2.00E-14 1.51E-14 2.00E-12 S.OOE-13 2.22E-14 4.00E-12 l.OOE-12 6/30/1986 2.23E-14 S.OOE-12 1.25E-12 5.19E-15 8.00E-14 2.00E-14 1.05E-14 2.00E-12 S.OOE-13 2.16E-14 4.00E-12 l.OOE-12 10/27/1986 2.33E-14 S.OOE-12 1.25E-12 7.78E-15 8.00E-14 2.00E-14 1.60E-14 .2.00E-12 S.OOE-13 2.02E-14 4.00E-12 l.OOE-12 12/15/1986 3.40E-14 S.OOE-12 1.25E-12 5.35E-15 8.00E-14 2.00E-14 1.47E-14 2.00E-12 5.00E-13 2.82E-14 4.00E-12 l.OOE-12 3/16/1987 2.06E-14 S.OOE-12 1.25E-12 4.50E-15 8.00E-14 2.00E-14 6.74E-15 2.00E-12 5.00E-13 7.29E-14 4.00E-12 l.OOE-12 5/11/1987 l.50E-14 5.00E-12 1.25E-12 8.54E-15 8.00E-14 l.OOE-14 8.15E-15 2.00E-12 S.OOE-13 3.28E-14 4.00E-12 l.OOE-12 9/9/1987 2.65E-14 S.OOE-12 1.25E-12 6.62E-15 8.00E-14 2.00E-14 9.34E-15 2.00E-12 5.00E-13 2.77E-14 4.00E-12 l.OOE-12 11/2/1987 .1.80E-14 S.OOE-12 1.25E-12 7.09E-15 8.00E-14 2.00E-14 7.20E-15 2.00E-12 5.00E-13 1,77E-14 4.00E-12 l.OOE-12 2/16/1988 1.01E-14 S.OOE-12 1.25E-12 2.98E-15 8.00E-14 2.00E-14 3.93E-15 2.00E-12 S.OOE-13 3.36E·14 4.00E-12 l.OOE-12 5/18/1988 1.78E-14 S.OOE-12 1.25E-12 8.14E-15 8.00E-14 2.00E-14 7.43E-15 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 8/15/1988 1.79E-14 S.OOE-12 1.25E-12 1.49E-14 8.00E-14 2.00E-14 5.34E-15 2.00E-12 S.OOE-13 2.45E-14 4.00E-12 l.OOE-12 11/14/1988 4.46E-14 S.OOE-12 1.25E-12 1.39E-14 8.00E-14 2.00E-14 1.17E-14 2.00E-12 S.OOE-13 3.43E-14 4.00E-12 1.00E-12 2/13/1989 1.67E-14 S.OOE-12 1.25E-12 5.54E-15 8.00E-14 2.00E-14 7.20E-15 2.00E-12 S.OOE-13 5.02E-14 4.00E-12 1.00E-12 5/15/1989 2.03E-14 S.OOE-12 1.25E-12 7.05E-15 8.00E-14 .2.00E-14 9.56E-16 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.00E-12 8/14/1989 2.81E-15 5.00E-12 1.25E-12 3.78E-15 8.00E-14 2.00E-14 9.26E-15 2.00E-12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12 11/13/1989 5.38E-14 5.00E-12 1.25E-12 8.01E-15 8.00E-14 2.00E-14 1.81E-14 2.00E-12 5.00E-13 4.09E-14 4.00E-12 l.OOE-12 2/12/1990 4.48E-14 S.OOE-12 1.25E-12 1.48E-14 8.00E-14 2.00E-14 1.28E-14 2.00E-12 5.00E-13 3.88E-14 4.00E-12 l.OOE-12 5/14/1990 2.18E-14 5.00E-12 1.25E-12 1.70E-14 8.00E-14 Z.OOE-14 1.59E-14 2.00E-12 5.00E-13 3.49E-14 4.00E-12 l.OOE-12 8/13/1990 9.53E-15 5.00E-12 1.25E-12 1.70E-14 8.00E-14 Z.OOE-14 3.27E-15 2.00E-12 5.00E-13 1.27E-14 4.00E-12 l.OOE-12 11/12/1990 1.11E-14 5.00E-12 1.25E-12 5.27E-15 8.00E-14 2.00E-14 5.38E-15 2.00E-12 5.00E-13 1.56E-14 4.00E-12 l.OOE-12 2/11/1991 6.35E-16 5.00E-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 2.31E-16 2.00E-12 5.00E-13 3.89E-14 4.00E-12 1.00E-12 5/13/1991 1.22E-15 5.00E-12 1.25E-12 6.14E-15 8.00E-14 Z.OOE-14 4.41E-15 2.00E-12 S.OOE-13 2.SOE-14 4.00E-12 1.00E-12 8/12/1991 7.84E-16 5.00E-12 1.25E-12 1.43E-15 8.00E-14 Z.OOE-14 4.47E-16 2.00E-12 5.00E-13 1.84E-14 4.00E-12 1.00E-12 11/11/1991 5.37E-16 5.00E-12 1.25E-12 4.20E-16 8.00E-14 2.00E-14 1.37E-16 2.00E-12 5.00E-13 1.27E-14 4.00E-12 1.00E-12 2/10/1992 3.54E-16 S.OOE-12 1.25E-12 1.18E-16 S.OOE-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.69E-14 4.00E-12 l.OOE-12 5/11/1992 4.71E-16 S.OOE-12 1.25E-12 9.S8E-16 S.OOE-14 2.00E-14 8.31E-17 2.00E-12 5.00E-13 1.43E-14 4.00E-12 l.OOE-12 8/10/1992 5.32E-15 5.00E-12 1.25E-12 3.36E-16 S.OOE-14 2.00E-14 1.65E-16 2.00E-12 5.00E-13 1.59E-14 4.00E-12 l.OOE-12 11/9/1992 3.66E-16 S.OOE-12 1.25E-12 2.25E-16 S.OOE-14 2.00E-14 1.08E-16 2.00E-12 5.00E-13 2.24E-14 4.00E-12 l.OOE-12 2/9/1993 2.05E-16 5.00E-12 1.25E-12 9.14E-17 j!.OOE-14 2.00E-14 6.31E-17 2.00E-12 5.00E-13 3.41E-14 4.00E-12 l.OOE-12 5/10/1993 4.80E-16 5.00E-12 l .25E-12 8.25E-16 8.00E-14 2.00E-14 1.26E-15 2.00E-12 S.OOE-13 1.83E-14 4.00E-12 l.OOE-12 8/10/1993 8.30E-16 5.00E-12 1.25E-12 1.90E-16 S.OOE-14 2.00E-14 2.10E-16 2.00E-12 S.OOE-13 1.70E-14 4.00E-12 l.OOE-12 11/8/1993 2.70E-16 S.OOE-12 1.25E-12 8.00E-17 S.OOE-14 2.00E-14 7.00E-17 l.OOE-12 S.OOE-13 2.34E-14 4.00E-12 l.OOE-12 2/7/1994 3.18E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 5.18E-16 2.00E-12 S.OOE-13 3.64E-14 4.00E-12 l.OOE-12 5/9/1994 1.80E-15 S.OOE-12 1.25E-12 9.78E-16 B.OOE-14 2.00E-14 1.10E-15 l.OOE-12 S.OOE-13 8.30E-15 4.00E-12 l.OOE-12 8/9/1994 2.67E-15 S.OOE-12 1,25E-12 1.11E-15 8.00E-14 2.00E-14 4.95E-16 l.OOE-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.21E-17 S.OOE-12 1.25E-12 1.59E-15 8.00E-14 2.00E-14 '1.66E-15 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 l.OOE-12 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit= 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.25E-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit = SE-14 uCi/ml Pre 1994 MPC Limit= ZE-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.51E-15 9.00E-14 2.25E-14 9.50E-16 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 9.35E-15 G.OOE-13 l.SOE-13 5/9/1995 2.21E-16 9.00E-14 2.25E-14 8.56E-16 l.OOE-14 5.00E-15 3.06E-15 9.00E-13 2.25E-13 4.34E-15 6.00E-13 l.SOE-13 8/9/1995 1.66E-16 9.00E-14 2.25E-14 1.67E-15 2.00E-14 5.00E-15 3.90E-15 9.00E-13 2.25E-13 5.60E-15 G.OOE-13 1.50E-13 11/11/1995 2.04E-14 9.00E-14 2.25E-14 6.70E-15 l.OOE-14 5.00E-15 7.65E-15 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13 2/5/1996 4.50E-14 9.00E-14 2.25E-14 3.58E-14 l.OOE-14 5.00E-15 2.39E-14 9.00E-13 2.25E-13 7.30E-15 6.00E-13 1.50E-13 5/6/1996 1.76E-15 9.00E-14 2.25E-14 3.57E-15 l.OOE-14 5.00E-15 9.55E-16 9.00E-13 2.25E-13 7.54E-15 6.00E-13 1.50E-13 8/5/1996 2.37E-15 9.00E-14 2.25E-14 8.18E-15 l.OOE-14 5.00E-15 7.46E-16 9.00E-13 2.25E-13 5.75E-15 6.00E-13 1.50E-13 11/6/1996 3.53E-15 9.00E-14 2.25E-14 5.31E-15 l.OOE-14 5.00E-15 9.39E-16 9.00E-13 ~-25E-13 1.21E-14 6.00E-13 1.50E-13 2/6/1997 1.84E-16 9.00E-14 2.25E-14 2.01E-16 l.OOE-14 5.00E-15 1.87E-16 !l.OOE-13 2.25E-13 6.14E-15 6.00E-13 1.50E-13 5/5/1997 5.75E-16 9.00E-14 2.25E-14 7.24E-16 l.OOE-14 5.00E-15 6.07E-16 9.00E-13 2.25E-13 4.75E-15 6.00E-13 1.50E-13 8/11/1997 1.21E-15 9.00E-14 2.25E-14 7.39E-16 2.00E-14 5.00E-15 5.05E-16 9.00E-13 2.25E-13 4.92E-15 6.00E-13 1.50E-13 1/5/1998 9.89E-16 9.00E-14 2.25E-14 1.92E-15 2.00E-14 S.OOE-15 6.21E-16 9.00£-13 l.25E-13 4.68E-15 6.00E-13 1.50E-13 4/28/1998 2.84E-15 9.00E-14 2.25E-14 2.38E-15 2.00E-14 5.00E-15 '1.72E-15 9.00E-13 2.25E-13 7.35E-15 6.00E-13 1.50E-13 7/31/1998 7.49E-16 9.00E-14 2.25E-14 1.49E-15 2.00E-14 S.OOE-15 8.34E-16 9.00E-13 2.25E-13 7.01E-15 6.00E-13 1.50E-13 9/28/1998 1.07E-15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 S.OOE-15 6.32E-16 9.00E-13 2.25E-13 3.95E-15 6,00E-13 1.50E-13 12/28/1998 8.51E-15 9.00E-14 2.25E-14 4.58E-15 2.00E-14 S.OOE-15 4.58E-15 9.00E-13 2.25E-13 1.43E-14 6.00E-13 1.50E-13 3/29/1999 3.75E-15 9.00E-14 2.25E-14 2.45E-15 2.00E-14 5.00E-15 2.39E-15 9.00E-13 2.25E-13 8.46E-15 6.00E-13 1.50E-13 7/3/1999 1.53E-15 9.00E-14 2.25E-14 8.65E-16 2,00E-14 S.OOE-15 6.52E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.SOE-13 9/27/1999 5.83E-15 9.00E-14 2.25E-14 3.52E-15 2.00E-14 5.00£-15 2.55E-15 9.00E-13 2.25E-13 8.22E-15 6.00E-13 1.50E-13 12/28/1999 9.48E-15 9.00E-14 2.25E-14 6.20E-15 2.00E-14 S.OOE-15 3.96E-15 9.00E-13 2.25E-13 7.56E-15 6.00E-13 1.50E-13 3/27/2000 2.06E-15 9.00E-14 2.25E-14 1.27E-15 l.OOE-14 S.OOE-15 1.09E-15 9.00E-13 2.25E-13 7.72E-15 6.00E-13 1.50£-13 6/26/2000 1.50E-15 9.00E-14 2.25£-14 1.24E-15 2.00E-14 5.00E-15 1.01E-15 9.00E-13 2.25E-13 4.36E-15 6.00E-13 1.50E-13 9/26/2000 1.04E-15 9.00E-14 2.25E-14 5.45E-16 2.00E-14 5.00E-15 6,01E-16 9.00E-13 2.25E-13 7.67E-15 6.00E-13 1.50E-13 12/26/2000 1.48E-15 9.00E-14 2.25E-14 7.56E-16 2.00E-14 S.OOE-15 6.84E-16 9.00E-13 2.25E-13 7.00E-15 6.00E-13 1.50E-13 3/26/2001 4.27E-16 9.00E-14 2.25E-14 2.19E-16 2.00E-14 5.00£-15 1.89E-16 9.00E-13 2.25E-13 6.13E-15 6.00E-13 1.50E-13 7/2/2001 4.52E-16 9.00E-14 2.25E-14 4.02E-16 l.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13 9/24/2001 4.65E-16 9.00E-14 2.25E-14 2.06E-16 l.OOE-14 5.00E-15 2.02E-16 9.00E-13 2.25E-13 6.98£-15 6.00E-13 1.50E-13 12/31/2001 7.40E-16 9.00E-14 2.25E-14 3.51E-16 l.OOE-14 5.00E-15 3.64E-16 9.00E-13 2.25E-13 4.72E-15 6.00E-13 1.50E-13 4/1/2002 1.26E-15 9.00E-14 2.25E-14 7.53E-16 l.OOE-14 5.00E-15 7.19E-16 9.00E-13 2.25E-13 9.65E-15 G.OOE-13 1.50E-13 7/1/2002 1.02E-15 9.00E-14 2.25E-14 '1.03E-15 2.00E-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 l.SOE-13 9/30/2002 5.82E-16 9.00E-14 2.25E-14 9.28E-16 2.00E-14 5.00E-15 3.14E-16 9.00E-13 2.25E-13 4.48E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 7.67E-16 2.00E-14 5.00E-15 3.48E-16 9.00E-13 2.25E-13 9.56E-15 6.00E-13 1.50E-13 3/31/2003 1.13E-15 9.00E-14 2.25E-14 7.41E-16 2.00E-14 5.00E-15 4.41£-16 9.00E-13 2.25E-13 6.68E-15 6.00E-13 1.50E-13 6/30/2003 4.35E-16 9.00E-14 2.25E-14 5.08E-16 2.00E-14 5.00E-15 2.51E-16 9.00E-13 2.25E-13 1.34E-15 6.00E-13 1.50E-13 9/29/2003 1.51E-16 9.00E-14 2.25E-14 1.02E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13 12/29/2003 1.52E-16 9.00E-14 2.25E-14 1.54E-16 l.OOE-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 7.02E-15 6.00E-13 1.50E-13 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.12E-16 l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.82E-15 6.00E-13 1.50E-13 6/27/2004 1.18E-16 9.00E-14 2.25E-14 3.11E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.47E-15 6.00E-13 1.50E-13 9/27/2004 1.16E-16 9.00E-14 2.25E-14 1.72E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 12/27/2004 1.14E-16 9.00E-14 2.25E-14 1.06E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13 3/28/2005 l.OOE-16 9.00E-14 2.25E-14 2.04E-16 2.00E-14 5.00E-15 1.83E-16 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13 6/29/2005 1.83E-16 9.00E-14 2.25E-14 3.81E-16 2.00E-14 S.OOE-15 3.09E-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 9/26/2005 2.87E-16 9.00E-14 2.25E-14 8.21E-16 2.00E-14 S.OOE-15 3.71E-14 9.00E-13 2.25E-13 6.28E-14 6.00E-13 1.50E-13 1/3/2006 8.74E-16 9.00E-14 2.25E-14 3.79E-16 2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25£-13 4.32E-14 6.00E-13 1.50E-13 4/3/2006 5.22E-16 9.00£-14 2.25E-14 6.66E-16 2.00E-14 5.00E-15 1.11E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13 7/3/2006 3.08E-16 9,00E-14 2.25E-14 1.10E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.25E-14 6.00E-13 1.50E-13 10/2/2006 9.14E-16 9.00E-14 2.25E-14 4.95E-16 2.00E-14 S.OOE-15 1.86E-16 9.00E-13 2.25E-13 1.67E-14 6.00E-13 1.50E-13 1/1/2007 9.49E-16 9.00E-14 2.25E-14 6.81E-16 2.00E-14 5.00E-15 2.02E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 4/2/2007 l.OBE-15 9.00E-14 2.25E-14 8.22E-16 2.00E-14 5.00E-15 2.26E-16 9.00E-13 2.25E-13 1.64E-14 6.00E-13 1.50E-13 7/2/2007 l.S4E-15 9.00E-14 2.25E-14 8.16E-16 2.00E-14 5.00E-15 4.76E-16 9.00E-13 2.25E-13 2.12E-14 6.00E-13 1.50E-13 9/30/2007 4.90E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.65E-15 6.00E-13 1.50E-13 12/31/2007 1.46E-15 9.00E-14 2.25E-14 5.67E-16 l.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.02£-14 G.OOE-13 1.50E-13 3/31/2008 3.16E-16 9.00E-14 2.25E-14 6.17E-16 l.OOE-14 5.00E-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 G.OOE-13 1.50E-13 6/30/2008 3.13E-15 9.00E-14 r25E-14 1.55E-15 l.OOE-14 5.00E-15 9.27E-16 9.00E-13 2.25E-13 7.40E-15 6.00E-13 l.SOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-5U Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit= 9E-13 uCi/ml BHV-5R Effluent Concentration Limit= 6E-13 uCi/ml BHV-5PB ALARAGoal= 2.25E-14 uCi/ml ALARAGoal-5E-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARAGoal= 1.5E-13 uCi/ml Pre 1994 MPC limit= 5E-12 uCi/ml Pre 1994 MPC limit= SE-14 uCi/ml Pt'e 1994 MPC limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= 5E-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-l3 1.50E-l3 12/31/2008 9.00E-14 2.25E-14 l.OOE-14 5.00E·15 9.00E-13 2.25E·13 6.00E-13 1.50£-13 3/15/2009 4.13E-15 9.00E-14 2.25E-14 1.39E-15 2.00E·14 5.00E-15 1.41E-15 9.00E-13 2.25E-13 4.66£-15 6.00E-13 1.50E-13 6/15/2009 2.31£-16 9.00E·14 2.25£-14 7.79E-16 l.OOE-14 5.00E-15 6.37£-16 9.00E-13 2.25E-13 4.18E-15 6.00£-13 1.50E·13 9/15/2009 3.10E-15 9.00£-14 2.25E-14 9.20£-16 2.00£-14 5.00£-15 6.36E-16 9.00£-13 2.25£-13 1.21E-14 6.00£-13 1.50E-13 12/15/2009 5.77E-15 9.00E-14 2.25£-14 3.13E-16 2.00E-14 5.00£-15 1.92E-16 9.00E-13 2.25E-13 2.48E-15 6.00£-13 1.50E-13 3/31/2010 4.78E-15 9.00E-14 2.25E-14 3.73E-16 2.00E-14 5.00£-15 4.19£-16 9.00E-13 2.25E·13 1.30E-14 6.00E-13 1.50E·13 6/30/2010 4.35E-15 9.00E-14 2.25E-14 7.84E-16 2.00£-14 5.00E-15 1.05E-15 9.00E-13 2.25E-13 4.40E-15 6.00E-13 1.50£-13 9/30/2010 3.57£-15 9.00E-14 2.25£·14 1.14E-15 2.00£-14 5.00E-15 7.97E-16 9.00E-13 2.25E-13 3.78E-15 6.00£-13 1.50£-13 12/31/2010 8.52£-15 9.00£-14 2.25£-14 1.45E-15 2.00£-14 S.OOE-15 1.29£-15 9.00£-13 2.25£-13 1.33£-14 6.00£-13 1.50£-13 4/4/2011 3.20£-15 9.00£-14 2.25£-14 8.89£-16 2.00£-14 5.00E-15 1.10£-15 9.00£-13 2.25£-13 1.48£-14 6.00£-13 1.50£-13 7/4/2011 6.98£-15 9.00£-14 2.25£-14 2.03£-15 l.OOE-14 5.00E-15 2.52£-15 9.00£-13 2.25E-13 1.08£-14 6.00£-13 l.SOE-13 -E :::::: 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C1) "C (J ::::J c 0 "C m a: ll) :> :I: m C\J (") ,.-T""" I I w w 0 0 ~ ~ ~ .. • ~ ~ Ill ·~ • ~~ , I•~ t!. ~r-p ~~ ~ ~,. ~ ..J ~ !4!1t I-. ~ 14 ~ ..,;::;::. 1.4 ~ I""' f ~ 1'1 -~ .. ~ I• lt-1::: lA t--~ ~ I•F:: ~ .... ~ ~ oo::t T""" I w 0 ~ ~~ ... R 14,. +-~~ b ij - o~-das so-das ~ .. ..._ so-das ~ Lo-das ~ r-"'-4] ~ -go-d as ~ ~ le.. go-d as """"' ~ t:::~ ~:.:::: vo-das E:o-das 0 T""" C\J It 14 ~ «. •• t-...... ~"" ? ~ .. ~ - ~~ p.- GO-d as -6 ro Q) w-das _J t oo-das co ss-das C\J C\J I ss-das E :I '6 .. ~ ~ fT~ ..... Ls-das ro a: gs-das t ,.,.. ,.._ .... gs-das 0 (") C\J vs-das I E :I -· E:s-das ·c: 0 ..c. I-...... ~ ::.-+"" F-1 G6·das t ~6-das (ij t:.llo os-das .... :I -ro sa-d as z E :I ss-das ·c: ro 1::1~ ft .... La-das :::> t gs-das gg-das vs-das JJ' ~ ~ E:a-das GS-das ~a-das L{) <D ,.... CX) T""" T""" T""" I uJ I I w w w 0 0 0 0 ~ ~ ~ ~ ,.-,.- (a1e::>s Dol) 1.00E-11 1.00E-12 1.00E-13 Q) ~ () CJ)1.00E-14 0> 0 .....1 - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E·12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml • \ M\t1 \ ~ r ' v¥ \ /1 1 ..... CXl 6.. Q) (/) ~ \. . C\J C') "<:!" CXl CXl CXl 6.. 6.. 6.. Q) Q) Q) (/) (/) (/) \. ~ U') CXl ' a. Q) (/) <D CXl ' a. Q) (/) t--eo 6.. Q) (/) CXl CXl 6.. Q) (/) 0) CXl 6.. Q) (/) 0 0) 6.. Q) (/) • • ..... 0) 6.. Q) (/) T '-I \41 ' C\J 0) ' v.. • C') 0) a. 6.. Q) (/) Q) (/) ~ f ' "<:!" 0) 6.. Q) (/) BHV-5 Uranium-Natural Concentrations (uCi/ml) • U') 0) 6.. Q) (/) i I* • CD 0) 6.. Q) (/) X ..1 1'--0) ' a. Q) (/) CXl 0) ' a. Q) (/) ~ \ l ~ ~ 0) 0 0) 0 6.. 6.. Q) Q) (/) (/) - ..... 0 6.. Q) (/) ~ C\J 0 ' a. Q) (/) • • \ 1 \ , ~ ' C') 0 ' a. Q) (/) "<:!" 0 ' a. Q) (/) ' U') 0 6.. Q) (/) f ll <D 0 -~~ 1'--0 6.. 6.. Q) (/) Q) (/) CXl 0 I a. Q) (/) 0) 0 I a. Q) (/) _, •JL 0 ..... 6.. Q) (/) -:§ 0 ::::J -"' c 0 i ... -c Cl) (,) c 0 0 0 ('I) ~ E ::::J 'i: 0 .c I- Ll) :> ::I: al .,..... w 0 0 <'J ('I") ..-..-I I w w 0 0 C! C! I.a. "~ • ~ 1-- c ~· t::. l::o ~ ~~ f-It. ""' ..-I UJ 0 C! (a1eos DOl) ;; o~-das ~ 6o-das ... .._ eo-das H .. La-das 1-go-d as • ... t-. ~ ~~ ~ go-d as vo-das E:o-das ~ co-das ~~ i-P:.. _t' ~a-d as oo-das ~ 66-das [K' 95-das ~ L6-das 95-das .._ 95-das ~~ v6-das .....-86-das ~lA ~ c6-das ..... ~ ;;::oo-. ...... ~6-das 06-das 6e-das ee-das Le-das gg-das gg-das K ve-das ~ E:e-das ce-das ...... ~g-das I{) (.0 ,...._ .,..... ..-.,..... I I I w w w 0 C! 0 0 C! C! ..-..-.,..... "' c 0 ... m II, -c Cl) u c 0 (.) CD N N I E j "C m a: l.l) ::> :I: al w 0 C! ,.- ,..... 1"'-..1- (\,1 (") ,.-,.- I I w w 0 0 C! C! ,.- ... ~ ...... lab::: f.+ ~ ~ • ~ I$ ~!'--.. ~ ~F v ,.- I w 0 C! (are~s oo1) ~ ~ ... -4 l--- I+< 4 t-- R I!) ,.- I w 0 C! ~ ..... ba. .. I-t-- ~ ~ ....... ~ f+-~ l•l ............ p ~ b!. ~ ~ I ~ f.-+- ~ ~ c.o ,.- I w 0 C! ,.- - - 1'--,.- I w 0 C! ,.- o~-das ao-das so-das La-das go-d as so-das vo-das 8o-das c::o-das ~o-des oo-das aa-das sa-des La-das ga-das sa-des va-des 8a-das c::a-das ~a-das oa-das as-das ss-das Ls-das gs-das ss-das vs-das 8s-das c::s-das ~s-das 1.00E-11 1.00E-12 1.00E-13 Q) (ij (.) en1 .00E-14 0) 0 ....J - 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 6E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCi/ml Pre 1994 ALARA Goal= 1 E-12 uCi/ml • y If /\.. 1\ /.11. •• , -. 1\ T • 11' .~ f ~~· t ... w..I "'<I~ I \ I~ 1\ 4\. ~ .• '¥'¥' • .. ~ ~ .... ..-C\J C') "<t LO co ""'" co (J) 0 ..-C\J C') co co co co co co co co co (J) (J) (J) (J) 6.. 6.. 6.. 6.. 6.. ' ' 6.. ' ' 6.. 6.. ' a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en I "<t (J) 6.. Q) en BHV-5 Lead-21 0 Concentrations (uCi/ml) • • ~ ~ I# it~ , .. ....... v & ~ . ~ _ .. ... • LO co ""'" co (J) 0 ..-C\J C') "<!" LO co ""'" co (J) 0 (J) (J) (J) (J) (J) 0 0 0 0 0 0 0 0 0 0 6.. 6.. ' 6.. ' 6.. 6.. 6.. 6.. 6.. 6.. ' 6.. ' ' 6.. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en (/) (/) (/) (/) en en en (/) (/) (/) (/) en TAB6 BHV -6 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit-9E-14 uCi/ml BHV-6U Effluent Concentration Limit= 2E-14 uCi/ml BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml BHV·6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal= 2.25E-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= SE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= !E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 12/14/1981 S.OOE-12 .l.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 3/29/1982 S.OOE-12 l .25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l .OOE-12 6/30/1982 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l .OOE-12 9/27/1982 S.OOE-12 l.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 1/3/1983 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 4/4/1983 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 6/30/1983 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 10/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 1/3/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 4/2/1984 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 7/2/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/1/1984 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 1/2/1985 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/1/1985 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4 .. 00E-12 1.00E-12 7/1/1985 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 9/30/1985 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 1/2/1986 .S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 4/1/1986 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 i!.OOE-12 5.00E-13 4.00E-12 l.OOE-12 6/30/1986 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 l.OOE-12 S.OOE-13 4.00E-12 l.OOE-12 10/27/1986 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 12/15/1986 .S.OOE-12 1.25E-12 8.00E-14 2.00E-14 l.OOE-12 S.OOE-13 4.00E-12 l.OOE-12 3/16/1987 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 5/11/1987 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 9/9/1987 S.OOE-12 1.25E·12 8.00E·14 2.00E·14 2.00E-12 S.OOE-13 4.00E·12 l.OOE-12 11/2/1987 5.00E·12 1.25E-12 8.00E-14 2.00E-14 l.OOE-12 S.OOE-13 4.00E·12 l.OOE-12 2/16/1988 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 5/18/1988 S.OOE-12 1.25E-12 8.00E-14 2.00E·14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 8/15/1988 S.OOE-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 11/14/1988 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 2/13/1989 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E·13 4.00E-12 l.OOE-12 5/15/1989 5.00E·12 1.25E-12 8.00E-14 .Z.OOE-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 8/14/1989 5.00E-12 1.25E·12 8.00E-14 .Z.OOE-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 11/13/1989 5.00E-12 1,25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 2/12/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 5/14/1990 S.OOE-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/13/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 11/12j1990 5.00E-12 1.25E-12 8.00E-14 l.OOE-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 2/11/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 1.00E-12 5/13/1991 S.OOE-12 1.25E-12 8.00E·14 2.00E·14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/12/1991 5.00E·12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/11/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E·12 l.OOE-12 2/10/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 5/11/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 8/10/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 l.OOE·12 11/9/1992 5.00E-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 5.00E-13 4.00E·12 1.00E-12 2/9/1993 5.00E-12 1.25E-12 B.OOE-14 2.00E·14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/10/1993 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2,00E-12 5.00E-13 4.00E-12 1.00E-12 8j10)1993 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/8/1993 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 2/7/1994 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 5/9/1994 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 8/9/1994 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l .OOE-12 11/7/1994 5.00E-12 1.25E-12 8,00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 LOOE-12 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-6U Effluent Concentration Limit= ZE-14 uCi/ml BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml "HV-6R Effluent Concentration Limit = 6E-13 uCi/ml "HV-6PB ALARAGoal= 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = .SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uC!/ml Pre 19.94 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 9.00E-14 2.25E-14 2.00E-14 5.00E-15 S.OOE-13 2.25E-13 6.00E-13 1.50E-13 5/9/1995 9.00E-14 2.25E-14 2.00E-14 5.00E-15 .9.00E-13 2.25E-13 6.00E-13 1.50E-13 8/9/1995 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 11/11/1995 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 2/5/1996 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 5/6/1996 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 8/5/1996 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 11/6/1996 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 2/6/1997 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 5/5/1997 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 8/11/1997 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 1/5/1998 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 4/28/1998 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 7/31/1998 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 9/28/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 12/28/1998 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/29/1999 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 7/3/1999 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 9/27/1999 3.03E-15 9.00E-14 2.25E-14 1.37E-15 2.00E-14 S.OOE-15 8.72E-16 9.00E-13 2.25E-13 7.55E-15 6.00E-13 1.50E-13 12/28/1999 5.01E-15 9.00E-14 2.25E-14 2.89E-15 2.00E-14 5.00E-15 1.31E-15 9.00E-13 2.25E-13 8.10E-15 6.00E-13 1.50E-13 3/30/2000 7.46E-16 9.00E-14 2.25E-14 5.25E-16 2.00E-14 S.OOE-15 3.00E-16 9.00E-13 2.25E-13 7.83E-15 6.00E-13 1.50E-13 6/26/2000 5.40E-16 9.00E-14 2.25E-14 3.53E-16 2.00E-14 S.OOE-15 6.11E-16 9.00E-13 2.25E-13 4.83E-15 6.00E-13 1.50E-13 9/25/2000 3.75E-16 9.00E-14 2.25E-14 2.23E-16 2.00E-14 5.00E-15 1.91E-16 9.00E-13 2.25E-13 6.41E-15 6.00E-13 1.50E-13 12/26/2000 5.21E-16 9.00E-14 2.25E-14 3.39E-16 2.00E-14 5.00E-15 3.28E-17 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13 3/26/2001 1.42E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.15E-15 6.00E-13 1.50E-13 7/2/2001 1.81E-16 9.00E-14 2.25E-14 1.66E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 9/24/2001 3.08E-16 9.00E-14 2.25E-14 1.01E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 8.59E-15 6.00E-13 1.50E-13 12/31/2001 3.31E-16 9.00E-14 2.25E-14 1.25E-16 2.00E-14 5.00E-15 1.09E-16 9.00E-13 2.25E-13 3.14E-15 6.00E-13 1.50E-13 4/1/2002 4.77E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 5.00E-15 1.96E-16 9.00E-13 2.25E-13 8.61E-15 6.00E-13 1.50E-13 7/1/2002 3.68E-16 9.00E-14 2.25E-14 4.41E-16 2.00E-14 S.OOE-15 1.76E-16 9.00E-13 2.25E-13 8.20E-15 6.00E-13 1.50E-13 9/30/2002 3.67E-16 9.00E-14 2.25E-14 5.60E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-13 5.55E-15 6.00E-13 1.50E-13 12/30/2002 1.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 1.67E-16 9,00E-13 2.25E-13 1.35E-14 6.00E-13 1.50E-13 3/31/2003 1.98E-16 9.00E-14 2.25E-14 1.68E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.77E-15 G.OOE-13 1.50E-13 6/30/2003 1.18E-16 9.00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.92E-15 6.00E-13 1.50E-13 9/29/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l .OOE-16 9.00E-13 2.25E-13 8.30E-15 6.00E-13 1.50E-13 12/29/2003 l.OOE-16 9.00E-14 2.25E-14 1.36E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.66E-15 6.00E-13 1.50E-13 3/29/2004 'l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.17E-15 6.00E-13 1.50E-13 6/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.55E-15 6.00E-13 1.50E-13 9/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.38E-16 Z.OOE-14 5.00E-15 l.OOE-16 S.OOE-13 2.25E-13 1.22E-14 6.00E-13 1.50E-13 12/27/2004 1.05E-16 9.00E-14 2.25E-14 1.72E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.52E-14 6.00E-13 1.50E-13 3/28/2005 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1,00E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13 6/29/2005 1.28E-16 9.00E-14 2.25E-14 1.01E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.85E-15 6.00E-13 1.50E-13 9/26/2005 1.98E-16 9.00E-14 2.25E-14 5.98E-16 2.00E-14 S.OOE-15 3.55E-16 9.00E-13 2.25E-13 1.71E-14 6.00E-13 1.50E-13 1/3/2006 7.67E-16 9.00E-14 2.25E-14 2.88E-16 2.00E-14 S.OOE-15 3.60E-15 9.00E-13 2.25E-13 4.85E-14 6.00E-13 1.50E-13 4/3/2006 2.92E-16 9.00E-14 2.25E-14 2.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 7/3/2006 3.25E-16 9.00E-14 2.25E-14 2.36E-16 2.00E-14 S.OOE-15 1.08E-16 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 10/2/2006 5.03E-16 9.00E-14 2.25E-14 1.49E-16 2.00E-14 S.OOE-15 1.19E-16 9.00E-13 2.25E-13 2.13E-15 6.00E-13 1.50E-13 1/1/2007 8.31E-16 9.00E-14 2.25E-14 2.49E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 4/2/2007 5.36E-16 9.00E-14 2.25E-14 3.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.43E-14 6.00E-13 1.50E-13 7/2/2007 1.08E-15 9.00E-14 2,25E-14 2.18E-16 2.00E-14 5.00E-15 1.54E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 9/30/2007 3.92E-16 9.00E-14 2.25E-14 1.02E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.38E-15 6.00E-13 1.50E-13 12/31/2007 2.92E-15 9.00E-14 2.25E-14 1.55E-15 2.00E-14 5.00E-15 3.16E-16 9.00E-13 2.25E-13 9.19E-15 6.00E-13 1.50E-13 3/31/2008 4.34E-16 9.00E-14 2.25E-14 3.51E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.99E-15 6.00E-13 1.50E-13 6/3102008 1.88E-15 9.00E-14 2.25E-14 9.00E-16 2.00E-14 5.00E-15 4.04E-16 9.00E-13 2.25E-13 7.41E-15 6.00E-13 1.50E-13 Date Effluent Concentration limit= 9E-14 uCi/ml BHV-6U Effluent Concentration limit= 2E-14 uCi/ml 8HV-6T Effluent Concentration limit= 9E-13 uCi/ml BHV-6R Effluent Concentration limit = 6E-13 uCi/ml BHV-6PB AlARAGoal= 2.25E-14 uCi/ml AlARAGoal= SE-13 uCi/ml ALARAGoal= Z.25E-13 uCi/ml AlARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-ll uCi/ml Pre 1994 MPC limit= SE-14 uCi/ml pre 1994 MPC limit= ZE-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL = l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 12/31/2008 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/15/2009 2.77E-15 9.00E-14 2.25E-14 1.01E-15 2.00E-14 5.00E-15 7.82E-16 9.00E-13 2.25E-13 6.46E-15 6.00E-13 1.50E-13 6/15/2009 1.41E-16 9.00E-14 2.25E-14 2.67E-16 2.00E-14 S.OOE-15 1.81E-16 9.00E-13 2.25E-13 5.76E-15 6.00E-13 1.50E-13 9/15/2009 4.87E-15 9.00E-14 2.25E-14 4.32E-16 2.00E-14 S.OOE-15 2.23E-16 9.00E-13 2.25E-13 8.98E-15 6.00E-13 1.50E-13 12/15/2009 9.24E-15 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.15E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13 3/31/2010 9.63E-15 9.00E-14 2.25E-14 1.82E-16 2.00E-14 5.00E-15 2.06E-16 9.00E-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13 6/30/2010 3.62E-15 9.00E-14 2.25E-14 3.94E-16 2.00E-14 5.00E-15 4.89E-16 9.00E-13 2.25E-13 4.30E-15 6.00E-13 1.SOE-13 9/30/2010 5.42E-15 9.00E-14 2.25E-14 1.08E-15 2.00E-14 S.OOE-15 5.68E-16 9.00E-13 2.25E-13 3.98E-15 6.00E-13 1.50E-13 12/31/2010 1.24E-14 9.00E-14 2.25E-14 1.21E-15 2.00E-14 5.00E-15 1.00E-15 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 4/4/2011 2.70E-15 9.00E-14 2.25E-14 4.62E-16 2.00E-14 5.00E-15 6.51E-16 9.00E-13 2.25E-13 1.29E-14 6.00E-13 1.50E-13 7/4/2011 3.01E-15 9.00E-14 2.25E-14 7.07E-16 2.00E-14 5.00E-15 5.75E-16 9.00E-13 2.25E-13 7.97E-15 6.00E-13 1.50E-13 9/28/1981 10/1/1984 i 9/9/1987 iil :::1 c:· 3 z a ~8/13/1990 !£. + -i ~8/10/1993 .... c:· 3 "' w 0 + 8/5/1996 :D D> 0. c:· 3 ~/27/1999 0) + r co ~/30/2002 I 1\:) ..... 0 9/26/2005 9/30/2008 IJl ..... (X) - - - ..... m I ..... -.,j .. m I ..... m i::'3lll ~ ~ r: ~ ~ ~.:: ~ -=:: ~ (Log Scale) ~ ~ ~ ~~ -~ ~~ ~~ ~ ~ "'~ 14 ..... m I ..... (]1 ~ • ~ ~ : ~ ~ I• ~~ 'Ill I m I ..... ~ ~ ~ 1-+ ~ ~ ~ ~ -t:: m I ..... w ..... m I ..... 1\:) aJ ::I: ~ 0) JJ I» a. c;· ~ c n a. CD (") 0 ~ n CD ~ -., I» -c;· ~ C/1 -c (") ~ - 1.00E-11 1.00E-12 1.00E-13 w en (.) U)1.00E-14 Ol 0 :::::!- 1.00E-15 1.00E-16 1.00E-17 - ,.... <X) 0) ,.... -... <X) ~ O'l Effluent Concentration Limit= 9E-14 uCilml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E·12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml '' '. """ 1'-0 <X) <X) 0) 0) 0) O'l ,.... ,.... ,.... -... as -... ,.... cY) ..._ as 0 ,.... -... <X) ''' cY) 0) O'l ,.... 0 ,.... (i5 BHV-6 Uranium-Natural Concentrations (uCi/ml) i -J • ' ... • T \J1 'Ill: r • • ~·~ ""' I , j V' V\ .. J ' ' ' co 0) C\J 1.0 <X) 0) 0) 0 0 0 O'l O'l 0 0 0 ,.... ,.... ~ ~ ~ -... ;::::: 1.0 0 0 -... ~ cY) ~ ~ <X) -... O'l 0) O'l en c: 0 ·.;; f! -c: C1) (J c: 0 0 0 ('I) C'll I E :::::J 'i: 0 .c 1- (0 ::> :I: m ,.... .--w 0 0 .-- C\J C') .--.--I I UJ UJ 0 0 ~ ~ , ' ~ r.. 1.-- """ L() .--.--I w UJ 0 0 ~ ~ (a1eos 6o1) .-- It .... ~ It I~ ~ 800c/0£/6 t=ft ~~ i::::="" p. ~~ 900c/9c/6 I~ 14~ ~ ~r-., ~ ~ I• li ~ cOOc/08/6 666~/LG/6 966 ~/9/8 - -£66 ~/0 ~/8 - 066 ~I£ ~/8 -L86 ~/6/6 --"1786 ~/~/0~ - -~86 ~/8c/6 <D 1'-,.... .-- I I w UJ 0 0 ~ ~ ,...- 1.00E-11 1.00E-12 1.00E-13 Q) (ii u UJ1.00E-14 Cl 0 ~ 1.00E-15 1.00E-16 1.00E-17 T""" co ()) T""" ....... co ~ ()) Effluent Concentration Limit= 9E-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml Pre 1994 MPC Limit= 2E-12uCi/ml Pre 1994 ALARA Goal= SE-13 uCi/ml ""'" I'-0 co co ()) ()) ()) ()) T""" T""" T""" ....... ....... ....... T""" ()) C') ....... ....... T""" 0 ()) ....... co \ ~ T 'I I I I I C') ()) ()) T""" ....... 0 T""" ....... co BHV-6 Radium-226 Concentrations (uCi/ml) ft lTT \ I ' ' ' <D ()) ()) ()) ()) ()) T""" T""" ....... ....... LO I'-....... C\1 co ....... ()) N\ C\1 0 0 ~ 0 C') ....... ()) J LO 0 0 ~ ~ ..... r A lA.JJV co 0 0 ~ 0 ~ ()) .... T I ~. 1 ·v 1.00E-11 1.00E-12 1.00E-13 Q) (ij (.) 001.00E-14 0> 0 _J - 1.00E-15 1.00E-16 1.00E-17 - - ,...- CD 0) ,...-...... CD ~ 0) Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCi/ml Pre 1994 ALARA Goal= 1E-12 uCi/ml ' '' """ r--CD CD 0) 0) ,...-,...-...... ...... 0) ,...-...... ...... 0 0) ' 0 0) 0) ,...-...... (Y) ,...-...... CD I (Y) 0) 0) ,...-...... 0 ,...-...... CD BHV-6 Lead-21 0 Concentrations (uCi/ml) <D 0) 0) ,...-...... ~ CD ~ C\J 0 0 ~ ~ 0) II ..... 1\J l.M 4 t ~ .... • CD ATTACHMENT C AIR PARTICULATE LABORATORY RESULTS AND QAJQC EI\ERGY • ,'\:~_)I-t •• 1 o : . ) www.energylab.com ~ Exu//111&1 Slnu 1152 Helen&, MT 877-472-0711 • Billings, MT 800-735·4489 • Casper, WY 888-235·0515 Gillette, WY 8&6-686·7175 • Rapid City, SD 888·&72-1225 • College Station, TX 888-690·221 8 May 29, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11040259 ANALYTICAL SUMMARY REPORT Project Name: 1st Quarter BHV Air 2011 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 4/7/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 040259-001 BHV-1 04/04/11 00:00 04/07/11 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C11 040259-002 BHV-2 04/04/11 00 :00 04/07/11 Filter Same As Above C11 040259-003 BHV-4 04/04/11 00 :00 04/07/11 Filter Same As Above c 11 040259-004 BHV-5 04/04/11 00:00 04/07/11 Filter Same As Above C11 040259-005 BHV-6 04/04/11 00:00 04/07/11 Filter Same As Above C11 040259-006 Blank 04/04/11 00:00 04/07/11 Filter Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: . ,/' .' ~j/-,L_ r-(;1:!7"-"" t t{'vv~ ' Interim Branch Manager Digitally signed by Steve Carlston Date: 2011.05.29 17:45:42-06:00 Page 1 of 22 www.energylab.com Anl/ytlc.l &c.IIMI:1 Slncl IW Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WV 8&6-886-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-221 B CLIENT: Denison Mines USA Corp Project: 1st Quarter BHV Air 2011 Report Date: 05/29/11 Sample Delivery Group: C11 040259 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g-Energy Laboratories, Inc.-Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER : The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 EN:RGY t~;\r. .... :· r · ...... 1 ,-:-: L::; , . www.energylab.com ~ lHIIIIm:l Sine. ti5Z Helena, MT 1177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 IITGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-1 Quarter/Date Sampled Radionuclide Concentration Air Volume !!CilmL C 1104025 9-00 I nalu 9.01E-16 First Quarter 20 II 230Th 1.90E-16 Air Volume in mLs 226Ra 3.64E-16 1.35E+II 210Pb 1.09E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thoriurn-230 Week for Radium-226 Day for Lead-210 Counting Precision MDC1JCilmL 1JCilmL N/A N/A 2E-17 3E-18 2E-17 2E-18 IE-16 8E-17 L.L.D/ Effluent Cone.* %Effluent 1JCilmL !!CilmL Concentration lE-16 9E-14 l.OOE+OO lE-16 3E-14 6.32E-Ol IE-16 9E-13 4.04E-02 2E-15 6E-13 1.82E+00 Page 3 of 22 EI\ERGY Li'.-~~H. I C:,..;t-4..! www.energylab.com Anllyllr:.l Exc.llltwl Sblu 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-186-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1st Quarter BHV Air 2011 C11 040259-001 Client Sample ID BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result 0.179 121 1470 19 11 49.1 2.0 0.3 26 2.6 0.35 MDC -Minimum detectable concentration Units mgffiner pCi/Filter pCiiFilter pCi/Filter pCi/Filter pCiiFilter pCi/Filter pCi!Filter pCi/Filter pCi/Filter pCi!Filter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 04113111 18:40 I sml SW6020 04113111 18:40 I sml E909.0 05117111 05:59 I eli-cs E909.0 05117111 05:59 I eli-cs E909.0 05117111 05:59 I eli-cs E903.0 04125111 23:45 I Irs E903.0 04125111 23:45 I trs E903.0 04125111 23:45 I trs E908.0 05102111 13:56 I dmf E908.0 05102111 13:56 I dmf E908.0 05102111 13:56 I dmf MCL -Maximum contaminant level. ND-Not detected at the reporting limit. Page 4 of 22 EI\ERGY :_,\L1 r)l.( .... l L,i-,1 ·-~:. www.energylab.com ~llxulllnuShlu 1112 Helena, MT 877-472-0711 • Billings, MT 800-735•4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-2 Quarter/Date Sampled Radionuclide Concentration Air Volume J.!CilmL Cll040259-002 nalu 3.79E-16 First Quarter 20 II 23oTh 4.01E-17 Air Volume in mLs 226Ra 9.11E-17 1.31E+ll 210Pb 1.06E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Counting Precision MDCJ.!CilmL J.!CilmL N/A N/A 6E-18 2E-18 SE-18 2E-18 IE-16 8E-17 L.L.D.+ Effluent Cone.* %Effluent J.!CilmL 11CilmL Concentration lE-16 9E-14 4.21E-Ol lE-16 3E-14 1.34E-Ol IE-16 9E-13 l.OIE-02 2E-15 6E-13 1.76E+00 Page 5 of 22 EI\ERGY '-,\ .~ . J I\~ '.) ..(I• www.energylab.com AM/ylfc./Exuh.Sii!U 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid Clly, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1st Quarter BHV Air 2011 C11 040259-002 Client Sample 10 BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result 0.0735 49.8 1390 17 9.9 12.0 1.0 0.3 5.3 0.83 0.29 MDC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCVFilter pCi/Filter pCVFilter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCLI QCL Method Analysis Date I By SW6020 04/13/11 18:45/ sml SW6020 04/13/11 18:45/ sml E909.0 05/17/11 12:36 I eli-cs E909.0 05117111 12:36 I eli-cs E909.0 05117111 12:36 I eli-cs E903.0 04125111 23:45 I Irs E903.0 04125/11 23:45 I trs E903.0 04125111 23:45 I trs E908.0 05102/11 13:56 I dmf E908.0 05102/11 13:56 I dmf E908.0 05/02/11 13:56/ dmf MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 6 of 22 EN:RGY L:,L::..:~r /I: .:-,IL ~ .. WI'IW.energylab.com Au/rlial Exe.t~tt~u ShJct 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-686-7175 • Rapid City, SIJ 888-672-1225 • College Station, 1X 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-4 Counting Quarter/Date Sampled Concentration Radionuclide Precision Air Volume !!CilmL Cll040259-003 ""u 1.29E-15 First Quarter 20 II 23oTh 1.40E-16 Air Volume in mLs 226Ra l.58E-16 1.25E+11 210Pb l.IIE-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21 0 !!CilmL N/A 2E-17 lE-17 lE-16 MDCj!CilmL N/A 3E-18 3E-18 8E-17 L.L.D .... Effluent Cone.* %Effluent !!CilmL JJCilmL Concentration lE-16 9E-14 1.44E+00 IE-16 3E-14 4.66E-Ol 1E-16 9E-13 1.75E-02 2E-l5 6E-13 l.86E+00 Page 7 of 22 EN:RGY ;\~:::>1 .-1''·,!":.'. www.energylab.com ~lfxt:~HIIIIt:ISinlll 11/M Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235·0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-672·1225 • College Station, TX 888-690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1st Quarter BHV Air 2011 C11 040259-003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. OCL -Quality control limit. Result 0.239 162 1400 17 9.9 19.7 1.4 0.4 18 2.0 0.35 MDC -Minimum detectable concentration Units mglfilter pCiiFilter pCi/Filter pCiiFilter pCiiFilter pCVFilter pCi/Filter pCi/Filter pCi/Filter pCiiFilter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 04113111 18:491 sml SW6020 04113111 18:491 sml E909.0 05117111 14:47 I eli-cs E909.0 05117111 14:47 I eli-cs E909.0 05117111 14:47 I eli-cs E903.0 04125111 23:45 I trs E903.0 04125111 23:451 trs E903.0 04125111 23:45 1 trs E908.0 05102/11 13:561 dmf E908.0 05102/11 13:561 dmf E908.0 05102111 13:56 I dmf MCL -Maximum contaminant level. ND-Not detected at the reporting limit. Page 8 of 22 EI\ERGY l1• .;-.::. f, I''''JL..'- www.energylab.com AMf!bl ExuHMIU Shtu 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29, 2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-5 Quarter/Date Sampled Radionuclide Concentration Air Volume 11CilmL Cl 1040259-004 natu 3.20E-15 First Quarter 20 II noTh 8.89E-l6 Air Volume in mLs 226Ra l.lOE-15 1.32E+11 210Pb 1.48E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year forThorium-230 Week for Radium-226 Day for Lead-210 Counting Precision MDC11CilmL ,..cilmL N/A N/A SE-17 3E-18 3E-l7 2E-18 2E-16 7E-17 L.L.D.+ Effluent Cone.* %Effluent 11CilmL ,..cilmL Concentration IE-16 9E-l4 3.56E+00 1E-16 3E-14 2.96E+00 IE-16 9E-13 1.22E-01 2E-15 6E-13 2.46E+00 Page 9 of 22 EN:RGY 1_/\ '.:..~~)( 't 1. I ('''I '"~'-' www.energylab.com AM/yllc;ll EJtulilflCI Sine. ll!t Helena, Mf 877-472-0711 • Billings, Mf 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LabiD: Denison Mines USA Corp 1st Quarter BHV Air 2011 C11 040259-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL · Analyte reporting limit. QCL -Quality control limit. Result 0.624 423 1950 20 9.9 145 3.6 0.3 117 10 0.38 MDC -Minimum detectable concentration Units mg/Mer pCiiFilter pCi!Filter pCi/Filter pCi!Filter pCi!Filter pC i!Filter pCi!Filter pCi!Filter pCi!Filter pCiiFilter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 04113111 19:091 sml SW6020 04113111 1 9:09 I sml E909.0 05117111 16:59 1 eli-cs E909.0 05117111 16:59 I eli-cs E909.0 05117111 16:59 I eli-cs E903.0 04125111 23:45 1 trs E903.0 04125111 23:45 I trs E903.0 04125111 23:45 I trs E908.0 05102111 13:56 I dmf E908.0 05102111 13:56 I dmf E908.0 05102111 13:56 I dml MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 10 of 22 EN:RGY l. :-.e..._; j:.,;.. f'_.: -!It.:~ www.energylab.com AM{JIJW Exu/1Hc1 S/nCI I 152 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SIJ 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29,2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: BHV-6 Quarter/Date Sampled Radionuclide Concentration Air Volume J.!CilmL Cll040259-005 natu 2.70E-15 First Quarter 20 II 23t>rh 4.62E-16 Air Volume in mLs 226Ra 6.51E-16 1.32E+l1 210Pb l.29E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Counting Precision MDCJ.!CilmL J.!CilmL N/A N/A 4E-17 3E-18 2E-17 2E-18 lE-16 7E-17 L.L.D.+ Effluent Cone.* %Effluent J.!CilmL J.!CilmL Concentration IE-16 9E-14 3.00E+00 IE-16 3E-14 1.54E+00 1E-16 9E-13 7.24E-02 2E-15 6E-13 2.14E+00 Page 11 of 22 E~RGY ... ,\~:..)[ ~1.1 ( .. 1-;..:; www.energylab.com Alll/ytlell Exullent:l SiRe. I !IJ2 Helena, liT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1st Quarter BHV Air 2011 C11 040259-005 Client Sample ID BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result 0.527 356 1700 19 9.8 86.0 2.8 0.3 61 5.8 0.37 MDC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi!Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 04113111 19:131 sml SW6020 04113111 19:13 I sml E909.0 05117111 19:11 I eli-cs E909.0 05/1 7/1 1 19:11 I eli-cs E909.0 05117111 19:11 I eli-cs E903.0 04125111 23:45 I Irs E903.0 04125111 23:45 I trs E903.0 04125111 23:45 I trs E908.0 05102111 13:56 I dmf E908.0 05102111 13:56 I dmf E908.0 05102111 13:56 I dmf MCL-Maximum contaminant level. ND -Not detected at the reporting limit. Page 12 of 22 EN:RGY L/\·.~on .... ,, ;:~.:L~: www.energylab.com Agfyt~QI Ex"ll~ta Slnt:~ 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, Sl) 888-672-1225 • College Station, TX 888-690-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 29,2011 PROJECT: 1st Quarter BHV Air 2011 SAMPLE ID: Blank Quarter/Date Sampled RadionucUde Concentration Air Volume J.1Ci/mL Cll040259-006 nntu 1.22E-17 First Quarter 2011 2J~h 5.84E-19 Air Volume in mLs 226Ra 5.16E-18 1.36E+l1 210Pb -4.51E-17 Counting Precision JLCilmL NIA 2E-18 2E-18 4E-17 Note: This sample uses 136,000,000 L of a1r volume for compar1son purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJ.iCilmL N/A 3E-18 3E-18 7E-17 L.L.D! Effluent Cone."' %Effluent 11CilmL 11CilmL Concentration lE-16 9E-14 1.35E-02 1E-16 3E-14 1.95E-03 lE-16 9E-13 5.73E-04 2E-15 6E-13 -7.51E-03 Page 13 of 22 EN:RGY ,1'\'.0::.:.i l "d () ,')l-,:~ www.energylab.com Atu/ytic61Ex~.smc. 1/W Helena, MT 877 ·472-0711 • Billings, MT BOD· 735-4489 • Casper, WY 888-235·0515 Gillette, WY 866-686-7175 • Rapid C~y. SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LabiD: Denison Mines USA Corp 1st Quarter BHV Air 2011 c 11 040259-006 Client Sample ID Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL · Analyte reporting limit. QCL -Quality control limit. Result 0.0024 1.7 ·6 5.8 9.9 0.7 0.3 0.3 0.08 0.30 0.37 MDC · Minimum detectable concentration Units mg/fiHer pCiiFilter pCiiFilter pCi/Filter pCiiFilter pCiiFilter pCiiFilter pCi!Filter pCi/Filter pCi!Filter pCiiFilter Report Date: 05/29/11 Collection Date: 04/04/11 DateReceived: 04/07/11 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date I By u u 0.0003 SW6020 0.2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCL-Maximum contaminant level. NO -Not detected at the reporting limit. 04113111 19:17 I sml 0411311119:17 I sml 05117111 21:23 I eli-cs 05117111 21 :23 I eli-cs 05117111 21 :23 I eli-cs 04125111 23:45 I Irs 04125111 23:45/trs 04125111 23:45 I Irs 05102/11 13:56 I dmf 05102/11 13:56 I dmf 05102/11 13:56 I dml U -Not detected at minimum detectable concentration Page 14 of 22 EI\ERGY _ ,-,:-.·~)I <f, ~ I (::,-•;t:,.' ~ www.energylab.com AM/ytlm EzuiiiiiiCI Shiel IW Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, W'f 888-235-0515 Gillette, WY 8&&-686-7175 • Rapid City, SD 888-672-1225 • Collage Station, TX 888-690-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1st Quarter BHV Air 2011 Analyte Count Result Units Method: E903.0 Sample ID: LCS-29538 Radium 226 Sample ID: MB-29538 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C11040296-001HMS Radium 226 Sample 10: C11040296-001HMSD Radium226 Qualifiers: RL-Analyte reporting limit. 3 MDC -Minimum detectable concentration Laboratory Control Sample 12.2 pCi/Filter Method Blank 0.03 pCi/Filter 0.1 pCi/Filter 0.2 pCi/Filter Sample Matrix Spike 10 pCi/L Sample Matrix Spike Duplicate 9.2 pCi/L Report Date: 05/29/11 Work Order: C11 040259 RL %AEC Low Limit High Limit Run: TENNELEC-3_11 0419A 101 70 130 Run: TENNELEC-3_110419A Run: TENNELEC·3_110419A 101 70 130 Run: TENNELEC-3_110419A 93 70 130 ND-Not detected at the reporting limit. RPD RPDLimit Qual 8.7 Batch: R145159 04/25/11 23:45 04/25/11 23:44 u 04/26/11 01 :24 04/26/11 01 :24 24.1 U -Not detected at minimum detectable concentration Page 15 of 22 EI\ERGY -' • '); ' I I~ ( www.energylab.com Alulytfal Elui/IIJCI Slnctl 1151 Helena, MT 871-472-0711 • Billings, MT B00-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&86-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1st Quarter BHV Air 2011 Analyte Count Result Units Method: E908.0 Sample ID: LCS-29538 Thorium 230 Sample ID: MB-29538 Thorium 230 Thorium 230 precision(±) Thorium 230 MDC Sample ID: C11040257-001AMS Thorium 230 Sample ID: C11040257-001AMSD Thorium 230 Qualifiers: RL-Analyte reporting limit. Laboratory Control Sample 10.9 pCi/Filter 3 Method Blank -0.08 pCi/Filter 0.07 pCi/Filter 0.1 pCi/Filter Sample Matrix Spike 56.4 pCi/Filter Sample Matrix Spike Duplicate 57.7 pCi/Filter MDC -Minimum detectable concentration Report Date: 05/29/11 Work Order: C11 040259 RL %REC Low Limit High Limit Run: EGG-ORTEC_11 0428B 111 70 130 Run: EGG-ORTEC_110428B Run: EGG-ORTEC_11 0428B 109 70 130 Run: EGG-ORTEC_11 0428B RPD RPDLimit Qual Batch: R145606 05/02111 13:56 05/02111 13:56 u 05/02111 13:56 112 70 130 2.4 05/02111 13:56 31.8 ND-Not detected at the reporting limit. U-Not detected at minimum detectable concentration Page 16 of 22 EI\ERGY 1.,\-~Cll ,< I'_.. ,,;__ '~ www.energyla b.com AM/ytla/ fxCI/m111:1 S/nCII 1/152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-&8&-7175 • Rapid Cl1y, SD 888-&72-1225 • College Station, TX 888-690-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1st Quarter BHV Air 2011 Analyte Count Result Units Method: E909.0 Sample ID: C11040259-001AMSD Lead 210 Sample ID: C11040259-001AMS Lead 210 Sample Matrix Spike Duplicate 2250 pCi/Filter Sample Matrix Spike 2160 pCi/Filter RL %REC 73 65 Report Date: 05/29/11 Work Order: C11 040259 Low Limit High Limit RPD RPDLimit Qual Batch: T _13784 Run: SUB-T40416 05/17/11 10:24 70 130 4.4 13.6 Run: SUB-T40416 05/17/11 08:11 70 130 s -Spike response is outside of the acceptance range for this analysis. Since the LCS and the RPD for the MS MSD pair are acceptable, the response is considered to be matrix related. The batch is approved. Sample ID: LCS-13784 Lead 210 Sample ID: MB-13784 Lead 210 Lead 210 precision (±) Lead210 MDC Qualifiers: RL-Analyte reporting limit. Laboratory Control Sample 279 pCi/Filter 3 Method Blank -4 pCi/Filter 6 pCi/FIIter 10 pCi/Filter MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration 80 Run: SUB-T40416 70 Run : SUB-T40416 130 ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 05/17/11 03:47 05/17/11 01 :35 u Page 17 of 22 EN:RGY ~t\'-~Uh·Ar~f('; •,-_ ~ www.energylab.com AMifllt:M fzu11Hc1 Sl1lcil 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Gasper, WY 888-235-0515 Gillette, WY 866-886-7175 • Rapid City, SO 888-672-1225 • College Station, lX 888-690-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 05/29/11 Project: 1st Quarter BHV Air 2011 Work Order: C11040259 Analyte Count Result Units RL %REC Low Limit High Limit APD A PO Limit Qual Method: SW6020 Batch: 29538 Sample ID: MB-29538 Method Blank Run: ICPMS4-C_11 0413A 04/13/11 18:28 Uranium 4E-05 mg/filter Sample ID: LCS2-29538 Laboratory Control Sample Run: ICPMS4-C_110413A 04/13/11 18:32 Uranium 0.107 mg/filter 0.00030 107 85 115 Sample ID: C11 040259-006AMS Sample Matrix Spike Run: ICPMS4-C_110413A 04/13/11 19:21 Uranium 0.0588 mg/filter 0.00030 113 75 125 Sample ID: C11 040259-006AMSD Sample Matrix Spike Duplicate Run: ICPMS4-C_110413A 04/13/11 19:26 Uranium 0.0585 mg/fiiter 0.00030 112 75 125 0.4 20 Qualifiers: RL-Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 18 of 22 ~N www.energylab.com ~ ~/Excsllem:fSIIICI/162 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 886-686-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218 Workorder Receipt Checklist 11111111 ~~ IIIII I~~~~~ ~111111 ~IIIIi~ 111111 Denison Mines USA Corp C11040259 Login completed by: Halley Ackerman Date Received: 4/7/2011 Reviewed by: BL2000\kschroeder Received by: ha Reviewed Date: 4/14/2011 Carrier 2Day name: Shipping container/cooler in good condition? Yes 0 NoD Not Present D Custody seals intact on shipping container/cooler? Yes D No 0 Not Present 0 Custody seals intact on sample bottles? Yes D NoD Not Present 0 Chain of custody present? Yes 0 NoD Chain of custody signed when relinquished and received? Yes 0 No 0 Chain of custody agrees with sample labels? Yes 0 NoD Samples in proper container/bottle? Yes 0 NoD Sample containers intact? Yes 0 NoD Sufficient sample volume for indicated test? Yes 0 NoD All samples received wilhin holding time? Yes 0 NoD ContainerfTemp Blank temperature: NA"C Water-VOA vials have zero headspace? Yes 0 No 0 NoVOA vials submitted 0 Water-pH acceptable upon receipt? Yes D NoD Not Applicable 0 Contact and Corrective Action Comments: None Page 19 of 22 "U Ill co CD N 0 0 -N N Chain of Custody and Analytical Request Record PLEASE PRINT (Provide as much information as possible.) Company Name: <.,_\')t'_,,}! :;,D,J tYlt~eS Project Name, PWS, Permit, Etc. Sample Origin J S"1' tdtA;z.n te_ State: {,A._'/ Contact Name: Phone/Fax: Email: ~~ ~lwt61L 61%-zt·z/ Invoice Address: / Invoice Contact & Phone: Purchase Order: --St ""'-c ~~ Page_f_ot__i_:_ EPA/State Compliance: • Yes~ NoD Sampler: (Please Print) -r:;hrlrt~ 1/#:L Quote/Bottle Ordel:f./ Special Report/Formats: .. Contact Ell prior to Shipped by: .1'6 -~-7j)'PJ D ow D EDD/EOT(Eiectronic Data) 0 P01WNVWTP Format: ____ _ D State: ___ _ n Other: 0 LEVEL IV n NELAC -----\-3 ~ ~ ~"'"'\'! t-----SA_M_P_L_E_I_D_EN-T-IF_I_CA-T-IO-N-.-C-o-11-ec-tio-n----.-C-o-llec-tio-n-t--M-A-T-R-I-X-l ~ -S:f-ic--3 ~ {Name, Location. Interval. etc.) Date Time ~~ ~ 7 9 10 cUstody Relinquished by ('R'tt. Detem me: //bt;; 0 ~ w c I -o (.) § <( e I-~ ~ ~ w "E W ro en -g .!!! C/) R u 5 H RUSH sample submittal for charges and scheduling -See Instruction Page Comments: Cboler ID(s): 1JJ~ Receipt Temp ~/\)('(..\ On Ice: Custody Seal On Bottle On Cooler Intact Signature Match ~ lnnn I~ Srgnature; oc vQb y N 0 N (3N (9N R Tc? •. A,.J VA-t~'" /1_ f · 5 za !l ecord ~Re~~~~Q~~~s~hoo~b-y w~n~'nt~t ~~---~D;a~l~~m~r~~. ~--------~~~~=---------~~~~~~--------~~~--------------~s~~~na7tu~m-:------------l MUST bet------------------------------------~~~~~--~~~--------~'~------~ Sl·gned l'~'Nu:e=.l\_ ""• ~ Sample Disposal: Return to Client: ~D JVI.V - In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested, This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.enerqylab.com for additional information, downloadable fee schedule, forms, and links. EI\ERGY -. \_ (. _. ~ www.energylab.com AM/ytlt2l r-IIHc. SIIIU 11152 Helena, MT 877-472-0711 • Billings, MT 800· 735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 ANAL VTICAL SUMMARY REPORT August 07, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11070215 Project Name: 2nd Quarter BHV Air 2011 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 7/7/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 070215-001 BHV-1 07/04/11 00:00 07/07/11 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C11 070215-002 BHV-2 07/04/11 00:00 07/07/11 Filter Same As Above C11 070215-003 BHV-4 07/04/11 00:00 07/07/11 Filter Same As Above C11 070215-004 BHV-5 07/04/11 00:00 07/07/11 Filter Same As Above C11 070215-005 BHV-6 07/04/11 00:00 07/07/11 Filter Same As Above C11 070215-006 Blank 07/04/11 00:00 07/07/11 Filter Same As Above This report was prepared by Energy Laboratories , Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as received basis unless otherwise indicated. Samples corrected for dry weight indicate units that have -dry appended. If you have any questions regarding these test results, please call. / / Report Approved By: r-:{7/-t,;'"'b:. n~ / Interim Branch Manager Digitally signed by Steve Carlston Date: 2011.08.07 13:58:26 -06:00 Page 1 of 22 www.energylab.com AM/flkMEzdn&ISillu IIISZ Helena, MT877-472-0711 • Billings, MTBOD-735-4489 • Casper, WY888-235-D515 Gillette, WY 8&&-18&-7175 • Ra id C , SD 888-672-1225 • Colle e Station, TX 888-&ID-2218 CLIENT: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Report Date: 08/07/11 Sample Delivery Group: C11 070215 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun . GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g-Energy Laboratories, Inc.-Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc. -Rapid City, SO eli-t-Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871017; California: 0211BCA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER : The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the cl ient may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab .com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 EN:RGY , /',U-:JIJ,..\iLH1l'j www.energylab.com AMI1tfalba'*-SIIIci115Z Halena, MT 877-472-0111 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-688-7175 • Rapid Ctty, SD 818-&72-1225 • Collage Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLffiNT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-1 Quarter/Date Sampled Radio nuclide Concentration Air Volume JiCi/mL C11040259-001 nalu 9.01E-16 First Quarter 2011 23oTh l.90E-16 Air Volume in mLs 226Ra 3.64E-16 1.35E+11 2toPb l.09E-14 Counting Precision JiCilmL N/A 2E-17 2E-17 1E-16 Counting Quarter/Date Sampled Concentration Radionuclide Precision Air Volume JiCi/mL C11070215-001 nalu l.59E-!5 Second Quarter 20 II 23oTh 5.31E-16 Air Volume in mLs 226Ra 4.99E-16 1.38E+ll 2toPb 8.38E-15 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 JiCilmL N/A SE-17 2E-17 2E-16 MDCJ1CilmL N/A 3E-18 2E-18 8E-17 MDCJiCi/mL N/A 4E-18 3E-18 1E-16 L.L.D.+ Eftluent Cone.* % Eftluent JiCi/mL JiCilmL Concentration 1E-16 9E-14 l.OOE+OO 1E-16 3E-14 6.32E-Ol 1E-16 9E-13 4.04E-02 2E-15 6E-13 1.82E+00 L.L.D.+ Effluent Cone.* %Effluent JiCilmL JiCilmL Concentration IE-16 9E-14 1.77E+00 IE-16 3E-14 1.77E+00 1E-16 9E-13 5.54E-02 2E-15 6E-13 l.40E+00 Page 3 of 22 EI\ERGY /\~01 ~/,1 (.)1~1:.."..... www.energylab.com AM/tfJg( Izulltt!ct ~ IW Helena, MT 817·472-11711 • Billings, MT BG0-735-4489 • Casper, W'f 888·235-8515 Gillette, WY 88&-188· 7175 • Rapid City, SD 188-172-1225 • College Station, TX 888-8911-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11 070215-001 Client Sample ID BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result 0.323 219 1150 23 14 68.8 2.8 0.4 73 7.2 0.60 MDC-Minimum detectable concentration Units mglfilter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 07/13/11 15:22 I sml SW6020 07113111 15:22 I sml E909.0 07/28111 16:54 I eli-cs E909.0 07128/11 16:54 I eli-cs E909.0 07128/11 16:54 I eli-cs E903.0 07120111 21 :55 I trs E903.0 07/20111 21 :55 I trs E903.0 07120111 21 :55 I trs E908.0 07126111 15:46 I dmf E908.0 07126111 15:46 I dmf E908.0 07126111 15:46 I dmf MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 4 of 22 EI\ERGY l 1\: iCH4/\I '~.HIE~ em·· www.energylab.com Allllftlal ~ Sllru riU Helene, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-188-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-2 Quarter/Date Sampled Radionuclide Concentration Air Volume 11CilrnL c 11040259-002 nalu 3.79E-16 First Quarter 20 11 230Th 4.01E-17 Air Volume in mLs 226Ra 9.11E-17 1.31E+l1 210Pb 1.06E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume J1Ci/mL Cll070215-002 nalu 3.07E-16 Second Quarter 20 11 23oTh 8.54E-17 Air Volume in mLs 226Ra 9.2!E-17 1.38E+ll 210Pb 7.21E-15 +l.LD's are from Reg. Guide 4.14 Counting Precision J1CilmL N/A 6E-18 SE-18 lE-16 Counting Precision 11CilmL NIA 1E-17 9E-18 1E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJ1Ci/mL N/A 2E-18 2E-18 8E-17 MDCJ1CilmL N/A 3E-18 3E-18 9E-17 L.L.D.+ Effluent Cone.* %Effluent 11CilmL 11CilmL Concentration 1E-16 9E-14 4.21E-01 1E-16 3E-14 1.34E-01 lE-16 9E-13 l.OIE-02 2E-15 6E-13 1.76E+00 L.L.D.+ Effluent Cone.* %Effluent 11CilmL J1Ci/mL Concentration lE-16 9E-14 3.4IE-Ol lE-16 3E-14 2.85E-Ol IE-16 9E-13 1.02E-02 2E-15 6E-13 1.20E+00 Page 5 of 22 EI'ERGY l /\•:il...>ll•\1 {_~)Ill_ ..... www.energylab.com AM/yflal w.u.-SbiU IW Helena, MT8l7·472-D711 • Billings, MT BGD-735-4489 • Casper, WY 881-235-0515 Gillette, WY 816-886-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&80-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11 070215-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision(±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result 0.0625 42.3 994 19 12 12.7 1.3 0.4 12 1.7 0.46 MDC - Minimum detectable concentration Units mg/filter pCi!Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filler pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW602D 07/13/11 15:39 / sml SW6020 07/13/11 15:39/ sml E909.0 07/28/11 20:12 / eli-cs E909.0 07/28/11 20:12 / eli-cs E909.0 07/28/11 20:12 / eli-cs E903.0 07/20/11 21 :55 / trs E903.0 07/20/11 21 :55/Irs E903.0 07/20/11 21 :55 /Irs E908.0 07/26/11 15:46 / dmf E908.0 07/26/11 15:46 / dmf E908.0 07/26/11 15:46 / dmf MCL -Maximum contaminant level. ND-Not detected at the reporting limit. Page 6 of 22 EN:RGY l l\~lUft/,1 :._ l <~ll ~~ www.energylab.com AM~Jt~ai~Sha rm Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-188-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-680-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLED>: BHV-4 Quarter/Date Sampled Radionuclide Concentration Air Volume pCilmL c 11040259-003 natu 1.29E-15 First Quarter 2011 23~h 1.40E-16 Air Volume in rnLs 226Ra l.SSE-16 1.25E+ll 21oPb l.l!E-14 Quarter/Date Sampled Concentration Radio nuclide Air Volume pCilmL Cll070215-003 nalu 3.30E-15 Second Quarter 20 II 23oTh 5.44E-16 Air Volume in mLs 226Ra 4.18E-16 1.17E+ll 210Pb 8.26E-15 +LLD's are from Reg. Guide 4.14 Counting Precision 11CilmL N/A 2E-17 IE-17 IE-16 Counting Precision 11CilmL N/A SE-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCpCi/mL N/A 3E-18 3E-18 8E-17 MDCpCilmL N/A 6E-18 4E-18 1E-16 L.L.D.+ Effluent Cone.* %Effluent pCilmL !ICilmL Concentration 1E-16 9E-14 1.44E+00 lE-16 3E-14 4.66E-Ol IE-16 9E-13 1.75E-02 2E-15 6E-13 1.86E+00 L.L.D.+ Effluent Cone.* %Effluent pCilmL !ICilmL Concentration lE-16 9E-14 3.66E+00 lE-16 3E-14 l.81E+00 lE-16 9E-13 4.65E-02 2E-15 6E-13 1.38E+00 Page 7 of 22 EI\ERGY /\l"i(.)l ~i\1 Cl IlL:..... •' www.energylab.com AnMytlai~SIIIu 1111 Helena, MTBH-472-0711 • Billings, MT 800-735-4488 • Caspar, WY 888-235-0515 Gillette, WY 88&-188-7175 • Rapid City, SD 188-&72-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11 070215-003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision(±) Lead210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result 0.571 386 967 19 12 49.0 2.5 0.4 64 6.1 0.73 MDC -Minimum detectable concentration Units mgitiner pCi/Filter pCi/Filter pCVFilter pCi/Filter pCi/Filter pCi/Filter pCi!Filter pCi!Filter pCi!Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 07/13/11 15:43 I sml SW6020 0711311115:43 I sml E909.0 07128111 21 :18 I eli-cs E909.0 07128111 21 :18 I eli-cs E909.0 07128/11 21 :18 I eli-cs E903.0 07120111 21 :55 /Irs E903.0 07120111 21 :55 /Irs E903.0 07/20/11 21 :55/ trs E908.0 07/26111 15:46/ dmf E908.0 07126/11 15:46 I dmf E908.0 07/26/11 15:46 I dmf MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 8 of 22 EI\ERGY • ;-.~ ~ ,...d 4/\1 c • ~~~ ·_. www.energylab.com AN/Jfla/ Emlllta Slnu 11!2 Helena, MT 817-472-0711 • Billings, MT BCI0-735-4489 • Gasper, WY 888-235-0515 Gillette, WY 8&&-186-7175 • Rapid City, SD 818-172-1225 • College Station, TX 888-680-221 B ffiGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-5 Quarter/Date Sampled Radionuclide Concentration Air Volume J!CilrnL C11040259-004 nalu 3.20E-15 First Quarter 20 II 23oTh 8.89E-16 Air Volume in mLs 226Ra l.lOE-15 1.32E+11 210Pb 1.48E-14 Quarter/Date Sampled Concentration Radio nuclide Air Volume J!CilmL Cll070215-004 nalu 6.98E-15 Second Quarter 2011 230Th 2.03E-15 Air Volume in mLs 226Ra 2.52E-15 1.38E+11 210Pb 1.08E-14 +liD's are from Reg. Guide 4.14 Counting Precision J!CilmL N/A 8E-l7 3E-l7 2E-16 Counting Precision J!CilmL N/A 2E-16 SE-17 2E-16 *Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21 0 MDC J!CilrnL N/A 3E-18 2E-18 7E-17 MDCJ!CilmL N/A 6E-18 3E-18 8E-l7 L.L.D.+ Effluent Cone.* %Effluent JiCilrnL J!CilrnL Concentration 1E-l6 9E-14 3.56E+00 IE-16 3E-14 2.96E+00 1E-16 9E-13 1.22E-01 2E-15 6E-13 2.46E+00 L.L.D.+ Effluent Cone.* %Effluent 11CilmL J!CilmL Concentration 1E-16 9E-l4 7.75E+00 lE-16 3E-14 6.76E+00 lE-16 9E-13 2.80E-01 2E-15 6E-13 1.81E+00 Page 9 of 22 EI\ERGY /\t:l._)I C/\I ' • .JI~l~ ~ www.energylab.com Alul!l/f;M ~ Slltu 1151 Helena, MT877-472-0711 • Billings, MT 800-735·4489 • CaspBt, WY 888·235·0515 Gillette, WY 886·186-7175 • Rapid City, SD 888-672-1225 • Collage Station, TX 888-&90-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11 070215-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision (±) Lead 210MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result 1.42 962 1490 23 12 347 6.6 0.4 280 25 0.88 MDC -Minimum detectable concentration Units mg/fi~er pCi!Filter pCi!Filter pCi/Filter pCi!Filter pCi!Filter pCi!Filter pCVFilter pCi!Filter pCi!Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCLJ QCL Method Analysis Date I By SW6020 07/13/11 16:03 I sml SW6020 07113/11 16:03 I sml E909.0 07/28111 22:24 I eli-cs E909.0 07128111 22:24 I eli-cs E909.0 07128/11 22:24 I eli-cs E903.0 07120111 21 :55 I Irs E903.0 07120111 21 :55 I trs E903.0 07120111 21 :55 I trs E908.0 07126111 15:46 I dmf E908.0 07/26111 15:46 I dmf E908.0 07/26/11 15:46 I dmt MCL -Maximum contaminant level. ND-Not detected at the reporting limit. Page 10 of 22 EN:RGY l /, J •• J z,..:,i:: h'!l ~ www.energylab.com ,..,_, bc.llttfu smc. tl5t Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WV 888-188-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-610-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: BHV-6 Quarter/Date Sampled Concentration Air Volume Radionuclide 11CilmL CII040259-00S nalu 2.70E-15 First Quarter 20 II 2JOTh 4.62E-16 Air Volume in mL~ 226Ra 6.51E-16 1.32E+ll 2wPb 1.29E-14 Quarter/Date Sampled Concentration Air Volume Radionuclide 11CilmL Cll070215-005 natu 3.01E-15 Second Quarter 2011 2JoTh 7.07E-16 Air Volume in mLs 226Ra 5.75E-16 1.38E+ll 210Pb 7.97E-15 +LLD's are from Reg. Guide 4.14 Counting Precision 11CilmL N/A 4E-17 2E-17 lE-16 Counting Precision 11CilmL N/A 7E-17 2E-17 IE-16 *Effluent Concentration from the NEW I 0 CFR Part 20-Appendix B -Table 2 Year for Natural Uranium Year forThorium-230 Week for Radium-226 Day for Lead-210 MDC11CilmL N/A 3E-18 2E-18 7E-17 MDC11CilmL N/A SE-18 3E-18 9E-17 L.L.D.+ Effluent Cone.* %Effluent 11CilmL 11CilmL Concentration lE-16 9E-14 3.00E+00 IE-16 3E-14 1.54E+00 IE-16 9E-13 7.24E-02 2E-15 6E-13 2.14E+00 L.L.D.+ Effluent Cone.* %Effluent 11CilmL 11CilmL Concentration IE-16 9E-14 3.35E+00 lE-16 3E-14 2.36E+00 IE-16 9E-13 6.39E-02 2E-IS 6E-13 1.33E+00 Page 11 of 22 EI\ERGY _ ,\l~{.)l l.~, I C l ~~ .... J www.energylab.com AM/fllul Fmo-SlRU IIJ1 Helena, MT877-47Z-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235·1515 Gillette, WY 88&-888-7115 • Rapid City, SO 888-&72-1225 • College Station, TX 881-690-221 8 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11 070215-005 Client Sample 10 BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision(±) Lead210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result 0.613 415 1100 20 12 79.2 3.1 0.4 97 9.3 0.75 MDC -Minimum detectable concentration Units mg/fiker pCi/Filter pCi/Filter pCi/Fiiter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pC i/Filter pCi/Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 07/13/11 16:07 I sml SW6020 07/13/11 16:07 I sml E909.0 07/28/11 23:30 I eli-cs E909.0 07/28/11 23:30 I eli-cs E909.0 07/28/11 23:30 I eli-cs E903.0 07/20/11 21:55/ trs E903.0 07/20/11 21 :55 / trs E903.0 07/20/11 21 :55/ trs E908.0 07/26/11 15:46/ dmf E908.0 07/26/11 15:46 / dmf E908.0 07/26/11 15:46 I dmf MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 12 of 22 EN:RGY L /\tJ;::J"./d Ul <IL:... www.energylab.com AR~yt~a~~smc. rw Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-886-7175 • Rapid City, SD 888-812-1225 • College Statlon,TX 888-610-2218 IDGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 7, 2011 PROJECT: 2nd Quarter BHV Air 2011 SAMPLE ID: Blank Quarter/Date Sampled Radionuclide Concentration Air Volume 1JCi/mL CII040259-006 nalu 1.22E-17 First Quarter 2011 23UTh 5.84E-19 Air Volume in mLs 226Ra 5.16E-18 1.36E+Il liUpb -4.51E-17 Counting Precision 11CilmL N/A 2E-18 2E-18 4E-17 Note: Th1s sample uses 136 000,000 L of a•r volume for compnnson purposes ' Counting Quarter/Date Sampled Concentration Radionuclide Precision Air Volume 1JCilmL J.!Ci/mL CII070215-006 natu l.OSE-17 N/A Second Quarter 20 II 23'Th 6.69E-18 2E-l8 Air Volume in mLs 226Ra -4.89E-20 2E-18 1.36E+ll 210Pb -8.89E-18 SE-17 Note: This sample uses 136,000,000 L of a1r volume for compar~son purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC!JCilmL N/A 3E-18 3E-18 7E-17 MDC!JCilmL N/A 2E-18 3E-18 9E-17 L.L.D.+ Efnuent Cone.* %Effluent 1JCilmL 1JCilmL Concentration IE-16 9E-14 1.35E-02 IE-16 3E-14 l.95E-03 IE-16 9E-13 5.73E-04 2E-15 6E-13 -7.51E-03 L.L.D.+ Effluent Cone.* %Effluent J.!CilmL J.!CilmL Concentration IE-16 9E-14 l.17E-02 lE-16 3E-14 2.23E-02 lE-16 9E-13 -5.43E-06 2E-15 6E-13 -1.48E-03 Page 13 of 22 EI\ERGY r,l:lUl ti\1 O t.CIL:.., www.energylab.com AM/yiii:M~Sit/M 1151 Halena, MT8l7·472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515 Gillette, WY 88&-188-7175 • Rapid City, SD 888-872·1225 • College Station, 1X 888-890-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter BHV Air 2011 C11 070215-006 Client Sample ID Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result 0.0021 1.4 -1 7.1 12 -0.007 0.3 0.5 0.91 0.34 0.34 MDC -Minimum detectable concentration Units mg/fi~er pCiiFilter pCi!Filter pCiiFilter pCiiFilter pCiiFilter pCi!Filter pCiiFilter pCiiFilter pCiiFilter pCi!Filter Report Date: 08/07/11 Collection Date: 07/04/11 DateReceived: 07/07/11 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date I By 0.0003 SW6020 0711311116:121sml 0.2 SW6020 0711311116:121sml u E909.0 07129111 00:37 I eli-cs E909.0 07129111 00:37 I eli-cs E909.0 07129111 00:37 I eli-cs u E903.0 07120111 21 :55 I trs E903.0 07120111 21 :55 I trs E903.0 07120111 21 :55 I trs E908.0 07126111 15:461 dmf E908.0 07126111 15:461 dmf E908.0 07126111 15:46 I dmf MCL -Maximum contaminant level. ND -Not detected at the reporting limit. U-Not detected at minimum detectable concentration Page 14 of 22 EN:RGY 1\t •..,)1/,d ( .~Jl •, www.energylab.com Anl/ytkll Exullltw• sau 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-188-7175 • Rapid City, SD 888-812-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: E903.0 Sample ID: MB-30350 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample ID: LCS-30350 Radium 226 Sample ID: C11061115-001HMS Radium 226 Sample ID: C11061115-001HMSD Radium 226 Qualifiers: RL-Analyte reporting limit. 3 Method Blank -0.1 pCi/Filter 0.1 pCi/Filter 0.3 pCi/Filter Laboratory Control Sample 23.8 pCi/Filter Sample Matrix Spike 24 pCi/L Sample Matrix Spike Duplicate 24 pCi/L MDC -Minimum detectable concentration Report Date: 08/07/11 Work Order: C11 070215 RL %REC Low Limit High Limit RPD RPDLimit Qual Run: BERTHOLD 770-2_11 0715A Run: BERTHOLD 770-2_11 0715A 101 70 130 Run: BERTHOLD 770-2_110715A 99 70 130 Run: BERTHOLD 770-2_11 0715A 103 70 130 1.4 ND-Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: R148357 07/20/11 17:30 u 07/20/11 17:30 07/20/11 17:30 07/20/11 17:30 21.5 Page 15 of 22 EN:RGY www.energylab.com Helena, Mr 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-888-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 1\'~~)).,IIOI<'It ~ Atv/ytJM:I EtuUIIICI Sl.lu IW QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: E908.0 Sample ID: C11070215-002AMS Thorium 230 Sample ID: C11070215-002AMSD Thorium 230 Sample ID: LCS-30397 Thorium 230 Sample ID: MB-30397 Thorium 230 Thorium 230 precision(±} Thorium 230 MDC Qualifiers: RL-Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike 1 08 pCi/Filter Sample Matrix Spike Duplicate 11 0 pCi/Filter Laboratory Control Sample 10.9 pCi/Filter Method Blank 0.2 pCi/Filter 0.1 pCi/Filter 0.1 pCi/Filter Report Date: 08/07/11 Work Order: C11 070215 RL %REC Low Limit High Limit Run: EGG-ORTEC_11 0722A 101 70 130 Run: EGG-ORTEC_110722A 103 70 130 Run: EGG-ORTEC_110722A 110 70 130 Run: EGG-ORTEC_110722A ND-Not detected at the reporting limit. RPD RPDLimit Qual 1.4 Batch: 30397 07/26/11 15:46 07/26/11 15:46 29.5 07/26/11 15:46 07/26/11 15:46 Page 16 of 22 EN:RGY AI,JI,,"l.j(_;HrL:..J www.energylab.com AMiyllai~S/Ru 11!2 Helena, MT 877·472-0711 • Billings, MT 800-735-4489 • Casper, WY 888·235-0515 Gillette, WY 8&&·88&· 7175 • Rapid City, SD 888-&72-1225 • Collaga Station, 1X 888-&&D-221 8 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: E909.0 SampleiD: C11 070215·001 AMSD Sample Matrix Spike Duplicate Lead 210 2450 pCi/Filter Sample ID: C11 070215-001 AMS Sample Matrix Spike Lead 210 2340 pCi/Filter Sample ID: LCS-14463 Laboratory Control Sample Lead 210 337 pCi/Filter SampleiD: MB-14463 3 Method Blank Lead 210 0.5 pCi/Filter Lead 210 precision (±) 7 pCi/Filter Lead 210 MDC 10 pCi/Filter Qualifiers: RL-Analyte reporting limit. MDC -Minimum detectable concentration RL %REC 121 117 95 Report Date: 08/07/11 Work Order: C11 070215 Low Limit High Limit RPD RPDLimit Qual Batch: T _14463 Run: SUB-T41490 07/28/11 19:06 70 130 4.8 14.5 Run: SUB-T41490 07/28/11 18:00 70 130 Run: SUB-T41490 07/28/11 15:48 70 130 Run: SUB-T41490 07/28/11 14:42 u ND-Not detected at the reporting limit. U-Not detected at minimum detectable concentration Page 17 of 22 EI\ERGY 1\ ~ ! () J 4 , \ I C II < 1 t " www.energylab.com AMiyfJm ~ Silla III!Z Helena, MT 877-472-11711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-188-7175 • Rapid Ctty, SD 188-872-1225 • College Station, TX 888-690-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter BHV Air 2011 Analyte Count Result Units Method: SW6020 Sample ID: MB-30397 Method Blank Uranium 0.0001 mg/filter Sample ID: LCS2-30397 Laboratory Control Sample Uranium 0.109 mg/filter Sample ID: C11 070228-003AMS Sample Matrix Spike Uranium 9.48E-09 mglfilter Sample ID: C11 070228-Q03AMSD Sample Matrix Spike Duplicate Uranium 9.43E-09 mg/filter Qualifiers: RL-Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 08/07/11 Work Order: C11 070215 RL %REC Low Limit High Limit Run: ICPMS4-C_110713A Run: ICPMS4-C_11 0713A 0.00030 109 85 115 Run: ICPMS4-C_11 0713A 0.00030 117 75 125 Run: ICPMS4-C_11 0713A 0.00030 116 75 125 ND -Not detected at the reporting limit. RPD RPDLimit Qual Batch: 30397 07/13/1115:10 07/13/11 15:14 07/13/11 16:32 07/13/11 16:36 20 Page 18 of 22 EN:RGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 l.-\•)r,t-<••11 II'' •_, AMJyllul Cn&&.,_Sitlu ICZ Gillatta, WY 818-688-7175 • Rapid City, SD 188-872-1225 • Collega Station, TX 881-690-2218 Workorder Receipt Checklist 111111111111111111111/I~IIIIIIIIIIIIIUI~IIIIIIIIII Denison Mines USA Corp C11 070215 Login completed by: Debra Williams Reviewed by: BL2000\kschroeder Reviewed Date: 7/7/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custocy agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Container/Temp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes D Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 'C NA Yes D Yes D Date Received: 7/7/2011 Received by: ckw NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Carrier 2nd Day Air name: Not Present D Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 19 of 22 "U Dl (C CD N 0 0 -N N Chain of Custody and Analytical Request Record Page_\_ of _t_'_ LABORATORIES PLEASE PRINT (Provide as much information as possible.) Company Name: De.niso() M~11~ Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: :;2. n d.. ~o..r-\er .;1..01\ State: \AT Yes 0' NoD Report Mail Address: po B O)C B 1"'(\a~~'~"' v.."T Contact Name: Phone/Fax: Email: Sampler: (Please Print) Invoice Address: -......J .St,),JY)c:. Invoice Contact & Phone: .s~tv'l(. Purchase Order: Quote/Bottle Order: Special Report/Formats: s: 0 ~ .. Contact Ell prior to RUSH sample submittal for charges and scheduling -See Instruction Page ttP0'~, ~0 U)~ ~ID~OI :U Cooler ID(s): ~ Dow D POTWMJWTP D State: ___ _ D Other: ----- 0 EDD/EDT(Eiectronic Data) Format: ____ _ 0 LEVEL IV D NELAC ·->~ >-rn ~U)"<i5rns: 0:>= ~ Ol u:>oo., "0 <( ~1iiir ~ ~ ~"* 5t§ ~~116' :i~~~~~ \-9 ..J~· g ~ >I .!or-\' I UJ ~<i " f---SAM--PL-E-ID_E_N-TI-F-IC_A_T-IO_N_-._C_o_lle_c_tio-n----.--C-o-llec-ti-on-+-----1 :5 E ~ ~ (Name, Location, Interval, etc.) Date Time MATRIX I 0 UJ I (_) ~ t-<( UJ w (/) ~ !;;: R t:.. "0 c :::l u 0 (ij Comments: On Ice: E :::J Custody Seal f-s 'E On Bottle On Cooler <tl "0 c Intact s H rJ) Signature Match 1 B~\J -I ~~ \3-A "1-lr 'A 1"1. I~ y~ ® y N y N 6 BlMk L\/Li%~111 \3-A "/. "'f. ~'-t-1~-t--+--+----+--i---t--t---t---------til~=----1 7 I I ~. 8 9 10 Date/Tim&: Signature: Custody _!!!!lnqurshed by !P~!ft. oaremme: slgn•'t'r: 11 1 -lt\MU ~jj;J~,y 7/!:,/:J/J\1 \100 ..:lMJI.VTC.. ~ Rece1Yad by (prfrt): Record Relinquished by (print~ , Oatetnm~: Sig....alure; (j Received by (print): MUSTbe~------------------------------~~~~~~~~~~~--~~~~-------4 Signed 1 Sample Disposal: Return to Client: Lab Disposal: ~ ~"-1,16:./ J ~ 'l,j} ;oognaiUre: Daternme: Signature: In certain circumstances, sam pi~ submitted to Energy Laborat~rie~, Inc. may be subcontract~d to ~certified laboratories in ~rder to complete the analysis requested. Thrs serves as not1ce of thrs possrbrllty. All sub-contract data Will be clearly notated on your analytrcal report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA HOl/S/9 HOl/S/S HOl/S/tl HOl/S/E HOl/S/l HOl/S/T. OT.Ol/S/lT. OT.Ol/S/H -OT.Ol/S/OT. M 1.0 I E OT.Ol/S/6 > ::c ........ co QO OT.Ol/S/8 1 E -OT.Ol/S/L Ll') QO > c: OT.Ol/S/9 ::c ·-co "'C + "' OT.Ol/S/S 0 ...... OT.Ol/S/tl <:t I GJ > ::c ...., OT.Ol/S/E co "' + -::s OT.Ol/S/l u ·-N ...., OT.Ol/S/T. I .... > "' ::c co 0.. 600l/S/lT. + c: 600l/S/n 0 ·-...... ...., 600l/S/OT. I "' > ::c ...., co V) 600l/S/6 + .... ·-<C 600l/S/8 600l/S/L 600l/S/9 600l/S/S 600l/S/tl 600l/S/E 600l/S/l 600l/S/T. 0 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 .-i c:i c:i c:i c:i 0 0 !=> 0 0 ...... ...... 0 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 D:J J: 10/5/2009 < I ...,a. 11/5/2009 ""C 12/5/2009 QJ ~ -· 1/5/2010 n c - + 2/5/2010 QJ ,... c;:l 3/5/2010 tD ::r: r-< I 4/5/2010 0 ...... QJ 5/5/2010 a. :::::s 6/5/2010 OQ -7/5/2010 3 O'Q 8/5/2010 ........ 3 9/5/2010 w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 0 0 !=> ~ 0 0 ~ 0 0 ~ 0 0 ~ 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 o:J :I: 10/5/2009 < I N 11/5/2009 "'C 12/5/2009 ll.) ..., r"'t' -· 1/5/2010 n c: - + 2/5/2010 ll.) r"'t' OJ 3/5/2010 tD I r-< I 4/5/2010 0 N ll.) 5/5/2010 c. :l 6/5/2010 OQ -7/5/2010 3 OQ 8/5/2010 ....... 3 9/5/2010 w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 0 0 0 p 1-' 0 0 0 1-' 0 0 0 1-' 0 0 0 1-' 0 0 0 1-' 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 O::J :I: 10/5/2009 < I ~ 11/5/2009 "'C 12/5/2009 S» ~ -· 1/5/2010 n t: - + 2/5/2010 S» "' OJ 3/5/2010 tD ::r: r-< .{:. 4/5/2010 0 S» 5/5/2010 c.. ::::J 6/5/2010 OQ -7/5/2010 3 OQ 8/5/2010 ........ 3 9/5/2010 w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 ~~ 6/5/2011 0 0 !=' 1-' 0 0 1-' 0 0 1-' 0 0 1-' 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 Cl :I: 10/5/2009 < I U1 11/5/2009 -a 12/5/2009 QJ '"'I ,.... -· 1/5/2010 n c + 2/5/2010 QJ ,.... Ill 3/5/2010 tD I r-< I 4/5/2010 0 U"' QJ 5/5/2010 c. -· ::::J 6/5/2010 OQ -7/5/2010 3 OQ 8/5/2010 ........ 3 9/5/2010 w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 0 0 !=' 1-' 0 0 1-' 0 0 1-' 0 0 1-' 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 Ol :I: 10/5/2009 < I 0\ 11/5/2009 "'C 12/5/2009 DJ ~ -· 1/5/2010 n c - + 2/5/2010 DJ .... OJ 3/5/2010 tD :I: r--;:: O'l 4/5/2010 0 DJ 5/5/2010 a.. -· ::::s 6/5/2010 O'Q -7/5/2010 3 O'Q 8/5/2010 ......... 3 9/5/2010 w - 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 Week It I 2 3 4 5 6 7 8 9 10 II 12 13 Week # 1 2 3 4 5 6 7 8 9 10 11 12 13 Week # 1 2 3 4 5 6 7 8 9 10 11 12 13 Week # 1 2 3 4 5 6 7 8 9 10 11 12 13 Period: January 4, 2011 through AprilS, 2011 (1st Quarter 2010) BHV-1 on stream% Filter Number 8400769 8153706 8153701 8400764 8400757 8400751 8400745 8400739 8400733 8400727 8153893 8153889 8153882 Totals Start D ate 3-Jan-1 I 10-Jan-11 17-Jan-1 I 24-Jan-ll 31-Jan-11 07-Feb-ll 14-Feb-11 22-Feb-11 28-Feb-1 I 07-Mar-1 I 14-Mar-1 I 21-Mar-1 I 28-Mar-11 91 BHV-2 on stream % Filter Start Number Date 8400768 03-Jan-11 8153707 10-Jan-11 8153702 17-Jan-11 8400763 24-Jan-11 8400756 31-Jan-11 8400750 07-Feb-11 8400744 14-Feb-11 8400738 22-Feb-11 8400732 28-Feb-11 8400726 07-Mar-11 8153895 14-Mar-11 8153890 21-Mar-11 8153883 28-Mar-1 1 Totals 91 BHV-4 on stream % Filter Start Number Date 8400767 03-Jan-1 1 8153708 1(}-Jan-11 8153703 17-Jan-11 6400762 24-Jan-1 1 6400755 31-Jan-11 6400749 07-Feb-11 8400743 14-Feb-11 8400737 22-Feb-11 8400731 28-Feb-11 8400725 07-Mar-11 8153896 14-Mar-11 8153891 21-Mar-11 8153884 28-Mar-11 Totals 91 BHV-5 on stream % Filter Start Number Date 6400766 03-Jan-1 1 8153709 10-Jan-11 6153899 17-Jan-1 1 6400761 24-Jan-11 8400754 31-Jan-11 8400748 07-Feb-11 8400742 14-Fetr11 6400736 22-Feb-11 6400730 28-Feb-11 8400724 07-Mar-11 8153697 14-Mar-11 8153692 21-Mar-11 8153885 28-Mar-11 Totals 91 98.9% Stop D ate 10-Jon-1 I 17-Jan-I 1 24-Jan-11 31-Jan-11 7-Feb-ll 14-Feb-11 22-Ftlrll 28-Feb-11 7-Mar-1 I 14-Mar-11 21-Mar-11 28-Mar-11 4-Apr-11 2184.0 96.1% Stop Date tO-Jan-11 17-Jan-11 24-Jan-11 31-Jan-11 07-Fetr11 14-Feb-11 22-Fet>-1 1 28-Feb-11 07-Mar-11 14-Mar-11 21-Mar-11 28-Mar-11 04-Apr-11 2184.0 91.8% Stop Date 10-Jan-11 17-Jan-1 1 24-Jan-11 31-Jan-11 07-Feb-1 1 14-Feb-11 22-Felrt 1 28-Feb-11 07-Mar-11 14-Mar-11 21-Mar-1t 28-Mar-11 04-Apr-11 2184.0 96.7% Stop Date 10-Jan-11 17-Jan-11 24-Jan-11 31-Jan-11 07-Feb-11 14-Feb-1 1 22-Feb-11 28-Feb-11 07-Mar-11 14-Mar-11 21-Mar-11 28-Mar-11 04-Apr-11 2184.0 Gross Tare Net 4.3737 4.2875 0.0862 4.5015 4.4591 0.0424 4.5169 4.4726 0.0443 4.3489 4.2843 0.0646 4.3670 4.2963 0.0707 4.3523 4.2764 0.0759 4.5413 4.3123 0.2290 4.4408 4.3215 0.1 193 4.4423 4.3350 0.1073 4.5000 4.4026 0.0974 4.8345 4.5073 0.3272 4.8549 4.5269 0.3280 4.7049 4.5399 0.1650 4.5214615 4.3862846 0.1352 Gross Tare Net 4.3712 4.2694 0.1018 4.5262 4.4670 0.0592 4.5282 4.4970 0.0312 4.4544 4.3125 0.1419 4.4422 4.3025 0.1397 4.5059 4.3179 0.1 880 4.6270 4.3174 0.3096 4.4864 4.3244 I 0.1620 4.5879 4.3425 0.2454 4.5913 4.3908 0.2005 4.9000 4.5298 0.3702 4.9993 4.4944 0.5049 4.8264 4.5088 0.3176 4.60357 4.39034 ' 0.21 32 Gross Tare Net 4.3533 4.2769 I 0.0764 4.4982 4.4817 0,0165 4.5059 4.4946 0.0113 4.3469 4.2909 0.0560 4.3436 4.2679 0.0756 4.3748 4.3028 0.0720 4.5247 4.3257 0.1990 4.3452 4.2963 0.0489 4.4019 4.3119 0.0900 4.5626 4.4265 0.1361 4.8648 4.5081 0.3567 49032 4.5259 0.3773 4.6763 4.5130 0.1633 4.51546 4.38632 0.1292 Gross Tare Net 4.4122 4.3042 I 0.1080 4.5390 4.4721 0.0669 4.6295 4.5336 0.0959 4.3723 4.2642 0.1081 4.4108 4.2917 0.1191 4.4055 4.2802 0.1253 4.6162 4.3224 0.2958 4.4709 4.3306 0.1401 4.4675 4.3450 0.1225 4.5826 4.4312 0.1516 4.8945 4.5262 I 0.3683 4.9667 4.5254 0.4413 4.7820 4.5161 0.2659 4.58092 4.39562 0.1653 Stop n me 26673.8 26838.4 27006.1 27172.9 27345.7 27513.3 27677.7 27845.4 28015.6 28180.0 28345.6 28514.6 28683.6 Stop Tlme 36802.9 37029.8 37195.4 37362.7 37534.8 37702.0 37866.8 36034.2 38204.8 38368.8 38534.8 38703.6 38872.7 Stop Time 12474.7 12568.6 12688.3 12856.6 13027.7 13196.3 13361.0 13528.6 t3699.3 13663.1 14029.0 14197.0 14364.9 Stop Time 36193.2 36328.5 36482.6 36650.9 36822.0 36990 5 37154.7 37322.3 37492.6 37657.2 37822.7 37990.7 38158.1 BHV-1 Start Time 26524.4 26673.8 26838.4 27006.1 27172.9 27345.7 27513.3 27677.7 27845.4 28015.6 28180.0 28345.6 28514.6 BHV-2 Start Time 36712.9 36862.9 37029.8 37195.4 37362.7 37534.8 37702.0 37866.8 38034.2 38204.8 38368.8 38534.8 38703.6 BHV-4 Start Time 12359.4 12474.7 12568.6 12666.3 12656.8 13027.7 13196.3 13361.0 13528.6 13699.3 13663.1 14029,0 14197.0 BHV-5 Start Time 36045.4 36193.2 36328.5 36482.6 36650.9 36822.5 36990.5 37154.7 37322.3 37492.8 37657.0 37822.7 37990.7 Total T I me 8962.8 9876.6 10062.6 10006.2 10365.0 10059.6 9863.4 10062.6 10210.2 9867.6 9933.6 10137.0 10144.2 129551.4 Total Time 5402.4 10011.6 9936.6 10042.8 10324.8 10033.2 9888.0 10039.8 10238.4 9840.0 9957.0 10132.8 10144.2 125991.6 Total Time 6917.4 5634.0 7179.0 10109.4 10254.0 10119.0 9882.6 10057.2 10240.2 9824 4 9956.4 10080.0 10074.0 120327.6 Total Time 8868.6 8116.2 9246.0 10101.6 10267.8 10080.0 9855.6 10054.8 10228.8 9867.6 9939.0 10081.2 10045.8 126753 Total Volume: 4.76E+06 Total L' 1ters 9.263.636 10,347,944 10.542.821 10,483,729 10,859,652 10.539.678 10,306,184 10,514,327 10.668.553 10,226.747 10.238.892 10,448,543 10.455.964 134,896,670 Loading, Per Cent I IT1Qim3 On Stream 0.0093 88.9% 0.0041 98.0% 0.0042 99.8% 0.0062 99.3% 0.0065 102.8% 0.0072 99.8% 0.0222 85.6% 0.0113 116.5% 0.0101 101.3% 0.0095 97.9% 0.0320 98.5% 0.0314 100.6% 0.0158 100.6% 0.0131 99.2% Total Volume: 4.63E+06 Total Loading, Per Cent Liters mg/m3 On Stream 5,583,731 0.0182 53.6% 10,489,387 0.0056 99.3% 10,410,808 0.0030 98.6% 10,522,076 0.0135 99.6% 10,817,534 0.0129 102.4% 10,512,018 0.0179 99.5% 10.331 ,889 0.0300 85.8% 10,490,503 0.0154 116.2% 10,698,019 0.0229 101.6% 10,198,t43 0.0197 97.6% 10,263,011 0.0361 98.8% 10,444.214 0.0483 100.5% 10,455,964 0.0304 100.6% 131.217.295 0.0211 96.5% Total Volume: 4.42E+06 Total Loading, Per Cent Liters mg/m3 On Stream 7, t49,582 0.0107 68.6% 5,902.673 0.0026 55.9% 7.521 ,606 0.0015 71 .2% 10,591,654 0.0053 100.3"/o 10,743,355 0.0070 101.7% 10,601,912 0.0068 100.4% 10,326,246 0.0193 85.8% 10,508,684 0.0047 t16.4% 10,699.900 0.0084 101.6% 10,181,975 0.0134 97.5% 10,262,392 0.0348 98.8% 10,389.791 0.0363 100.0% 10.383,607 0.0157 99.9% 125,263,778 0.0128 92.2% Total Volume: 4.66E+06 Total Loading, Per Cent Liters mg/m3 On Stream 9,166,274 0.0118 88.0% 6,503,532 0.0079 80.5% 9,687,250 0.0099 91.7% 10.583,682 0.0102 100.2% 10,757,814 0.0111 101 .9% 10,561 ,051 0.0119 100.0% 10,298,034 0.0267 85.6% 10,506,177 0.0133 116.4% 10,687,966 0.0115 101.5% 10,226,747 0.0148 97.9% 10,244,458 0.0360 98.6% 10,391,026 0.0425 100.0% 10,354.540 0.0257 99.7% 131 ,966,574 0.0181 97.1% Page 21 of 22 Page 1 SC M F 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 .16.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 Period: January 4, 2011 through AprilS, 2011 (1st Quarter 2010) BHV-6 on stream % Week Filter Start # Number Date 1 8400765 03-Jan-11 2 6153710 10-Jan-11 3 6153704 17-Jan-11 4 6400760 24-Jan-11 5 8400753 31-Jan-11 6 8400747 07-Feb-11 7 8400741 14-Fab-11 8 8400735 22-Feb-11 9 8400729 28-Feb-11 10 8400723 07-Mar-11 11 8153898 14-Mar-11 12 8153888 21-Mar-11 13 8153886 28-Mar-11 Totals 91 ALL BHV on stream % Week II Blanks Start Date 1 8153705 03-Jan-11 2 8153900 10-Jan-11 3 8400759 17·Jan-11 4 8400758 24-Jan-11 5 8400752 31-Jan-11 6 8400746 07-Feb-11 7 8400740 14-Feb-11 8 8400734 22-Feb-11 9 8400728 28-Fetr-11 10 8153894 07-Mar-11 11 8153887 14-Mar-11 12 8153881 21-Mar-11 13 8153675 28-Mar-11 Totals 91 96.7% Stop Data 10-Jan-11 17-Jan-11 24-Jan-11 31-Jan-11 07-Feb-11 14-Fetr-11 22-Feb-11 28-Fab-11 07-Mar-11 14-Mar-11 21-Mar-11 28-Mar-11 04-Apr-11 2184.0 96,1% Stop Date 10-Jan-11 17-Jan-11 24-Jan-11 31-Jan-11 07-Feb-11 14-Feb-11 22-Feb-11 28-Feb-11 07-Mar-11 14-Mar-11 21-Mar-11 28-Mar-11 04-Apr-11 2184.0 Gross 4.3800 4.4979 4.5260 4.3556 4.4589 4.4284 4.5313 4.4723 4.5319 4.5567 4.9076 4.9254 4.8300 4.56954 Net 4.4871 4.4808 4.2868 4.2449 4.3191 4.3180 4.3201 4.3008 4.3325 4.5203 4.4993 4.5035 4,5082 4.3940 Stop Tare Net Time 4.2809 0.0991 1973.2 4.4556 0.0423 2108.6 4.4790 0.0490 2263.2 4.3033 0.0523 2431 .3 4.3259 0.1330 2602.4 4.3027 0.1257 2770.9 4,2819 0.2494 2935.3 4.3251 0.1472 3102.9 4.3962 0.1357 3273.5 4 4225 0.1342 3437.6 4.5278 0.3798 3603.2 4.5292 0.3962 3771.3 4.5168 0.3132 3938.2 4.39592 0.1736 Page2 BHV·6 Total Volume: 4.66E+06 Start Total Total Loading, Per Cent Time Time Liters mg/m3 On Stream SCFM 1825.3 8872.8 9,170,615 0.0108 88.0% 36.5 1973.2 8122.2 8,509,819 0.0050 60.6% 37.0 2106.6 9280.8 9,723,711 0.0050 92.1% 37.0 2263.2 10084.2 10,565,452 0.0050 100.0% 37.0 2431 .3 10263.6 10,753,413 0.0124 101.8% 37.0 2602.4 10108.8 10,591,226 0.0119 100.3% 37.0 2770.9 9867.6 10,310,573 0.0242 85.7% 36.9 2935.3 10056.0 10,507,430 0.0140 116.4% 36.9 3102.9 10235.4 10,694,884 0.0127 101.5% 36.9 3273.5 9848.4 10,206,848 0.0131 97.7% 36.6 3437.6 9936.0 10,241,365 0.0371 98.6% 36.4 3603.2 10080.6 10,390,409 0.0381 100.0% 36.4 3771 .3 10017.6 10.325,473 0.0303 99.4% 36.4 126774 131,991,218 0.0169 97.1% 36.8 Page 22 of 22 Period: April 5, 2011 through July 5, 2011 (2nd Quarter 2011) Page 1 BHV·1 on stream% 101.0% BHV-1 Total Volume: 4.67E+06 Week Filter Start Stop Stop Start Total Total Loading, Per Cent • Number Date Date Gross Tare Net Time Time Time Uters mQ/m3 On Stream SCFM I 8153876 4-Apr·ll 11-Apr-11 5.0637 4.4850 0.5787 28850.1 28683.6 9988.8 10,324,073 0.0.~61 99.1% 36.5 2 8153870 11-Apr-11 18-Apr-11 4.7359 4.5115 0.2244 29018.4 28850.1 10096 2 10,578.024 0.0212 100.2% 37.0 3 8400721 18-Apr-11 25-Apr-11 4.6449 4.4479 0.1970 29186.1 29018.4 10063.2 10,543,450 0.0187 99.8% 37.0 4 8400715 25-Apr-11 2-May-11 4.5507 4.4261 0.1246 29355.1 29186.1 10137.6 10,621,400 0.0117 100.6% 37.0 5 8400709 02-May-11 9-May-11 4.6184 4.3763 0.2421 29522.1 29355.1 10024.2 10,502,588 0.0231 99.4% 37.0 6 8400702 09-May-1 1 16-May-1 1 4.5690 4.3920 0,1770 29688.9 29522.1 10006.8 10,484,358 0.0169 99.3% 37.0 7 8400997 16-May-11 23-May-11 4.5190 4.3382 0.1808 29857.8 29688.9 10133.4 10.588,305 0.0171 100.5% 36.9 8 8400991 23-May-11 30-May-11 5.0540 4.3246 0.7294 30049.7 29857.8 11514.6 12,031,509 0.0606 114.2% 369 9 8400985 30-May·ll 6-Jun-1 I 4.5512 4.3075 0.2437 30194.9 30049.7 8714.4 9,105.604 0.0268 86.5% 369 10 8153864 06-Jun-11 I 3-Jun-11 4.8220 4.5244 0.2976 30361.7 30194.9 10002.6 10,366,661 0.0287 99.2% 36.6 II 81.53858 13-Jun-1 I 20--Jun-11 4.6910 4.5195 0.1715 30529.7 30361 .7 10080.0 10,389,791 0.0165 100.0% 36.4 12 8400977 20-Jun-LL 27-Jun-1 I 4.4738 4.3369 0.1369 30697.1 30529.7 10049.4 10.358,251 0.0132 99.7% 36.4 13 8400971 27-Jun-11 4-Ju1-11 4.6759 4.2996 0.3763 30890.6 30697.1 11604.6 11,961,247 00315 115.1% 36.4 Tolals 91 2184.0 4.6899615 4.4068846 0.2831 132415.8 137,855.26 I 0.0263 101.0% 36.8 BHV-2 on slream % 101.0% BHV-2 Total Volume: 4.87E+06 Week Finer Start Stop Stop Start Total Total Loading, Per Cent II Number Daie Date Gross Tare Net Time Time Time Uters mg(m3 On Stream SCFM 1 8153877 04-Apr-1 1 11-Apr-11 5.2444 4.5078 0.7366 39039.4 38672.7 10002.6 10,336,336 0.0712 99.2% 36.5 2 8153871 11-Apr-11 18-Apr-11 4.6957 4.5359 0.3598 39207.5 39039.4 10087.2 10,568,595 0.0340 100.1% 37.0 3 8400720 16-Apr-11 25-Apr-11 4.7165 4.4149 0.3016 39374.8 39207.5 10035.6 10,514,532 0.0267 99.6% 37.0 4 8400714 25-Apr-11 02-May-1 I 4.5849 4.4433 0.1416 39544.3 39374.9 10165.2 10,650,317 0.0133 100.6% 37.0 5 8400708 02-May-1 1 09-May-11 4.7269 4.4315 0.2954 39710.7 39544.3 9982.2 10,456,584 0.0262 99.0% 37.0 6 6400703 09-May-11 16-May-11 4.6369 4.3846 0.2541 39878.1 39710.7 10047.0 10,526,476 0.0241 99.7% 37.0 7 8400996 16-May-11 23-May-11 4.5604 4.3334 0.2270 40046.4 39678.1 10098.6 10,551,943 0.0215 100.2% 36.9 9 8400990 23-May-11 30-Mey-11 5.1102 4.3271 0.7631 40238.3 40046.4 ll511.2 12,029,002 0.0651 114.2% 36.9 9 6400984 30·May·11 06-Jun-11 4.6406 4.3157 0.3249 40363.0 40238.3 8680.2 9,069,669 0.0356 86.1% 36.9 10 8153665 06-Jun-11 13-Jun-11 4.9004 4.5266 0.3738 40550.9 40383.0 10076.4 10,443,147 0.0356 100.0% 36.6 11 6153859 13-Jun-11 2Q-Jun-11 4.7116 4.4667 0.2229 40716.3 40550.9 10042.2 10,350,829 0.0215 99.6% 36.4 12 8400976 20-Jun-11 27-Jun-11 4.6200 4.3166 0.3020 40685.8 40716.3 100~1.2 10,360,100 0.0292 99.7% 36.4 13 8400973 27-Jun-11 04-Jul-11 4.6613 4.3177 0.5436 41079.3 40865.6 11610.0 11,966,613 0.0454 115.2% 36.4 Totals 91 2184.0 4.78557 4.41123 0.3743 132390.6 137.826,549 0.0349 101.0"/o 36.8 BHV-4 on stream % 65.9% BHV-4 Tolat Volume: 4.14E+06 Week Filler Start Stop Stop Start Total Total loading, Per Cent • Numbe.r Date Date Gross Tare Net Time Time Time UlerB mi:Vm3 On Stream SCFM 1 6153878 04-Apr-11 11-Apr-11 4.9000 4.5215 0.3765 14530.8 14364.9 9952.8 10,286,865 0.0368 98.7% 365 2 9153872 11-Apr-11 18-Apr-11 4.5120 4.5036 0.0084 14536.9 14530.8 487.2 510,451 O.D165 4.8% 37.0 3 8400719 16-Apr-11 25-A~r-11 4.6179 4.3733 0.2446 14703.6 14538.9 9896.4 10.368,689 0.0236 96.2% 37.0 4 8400713 25-Apr-11 02-May-11 4.6332 4.4070 0.2262 14674.3 14703.8 10229.4 10,717,561 0.0211 101.5% 37.0 5 8400707 02-May-11 09-May-11 4.4075 4.4192 ·0.0117 15041.0 14674.3 10002.6 10,479,957 ·0.0011 99.2% 37.0 6 8400704 09-May-11 16-May-11 4.5617 4.3967 0,1850 15207.9 15041.0 10012.2 10,490,016 0.0176 99.3% 37.0 7 8400995 16-May-11 23-May-11 4.4659 42669 0.1990 15376,6 15207.9 t0134.6 10,569,559 0.0166 100.5% 36.9 6 6400989 23-May-11 30-May-11 5.0686 4.3346 0.7642 15568.7 15376.8 I 1515.8 12,032,763 0.0627 114.2% 36.9 9 8400963 30-May-11 06-Jun-11 4.6341 4.3246 0.3095 15713.4 15566.7 8679.6 9,069,242 0.0341 86.1% 36.9 10 8153866 06-Jun-11 13-Jun-11 4.7811 4.4954 0.2857 15879.9 15713.4 9987.6 10,351,115 0.0276 99.1% 36.6 11 8153860 13-Jun-11 20-Jun-11 4.4954 4.5011 --0.0057 15879.9 15879.9 0.6 618 -9.2167 0.0% 36.4 12 8400975 2Q-Jun·11 27-Jun-11 4.3639 4.2779 0.0860 16047.5 15879.9 10058.4 10,367,527 0.0063 99.8% 36.4 13 8400969 27-Jun-11 04-Jul-11 4.7065 4.2765 0.4300 16240.0 16047.5 11546.4 11,901.258 0.0361 114.5% 36.4 Totals 91 2184.0 4.62985 4.39218 0.2377 112503.6 ~117,165,641 -0.6857 85.9% 36.8 BHV-5 on stream % 101.1% BHV-5 Total Volume: 4.B7E+06 Week Filter Start Stop Stop Start Total Total Loading, Per Cent • Number Date Date Gross Tare Net Time Time Time Uters mllfm3 On Stream SCFM 1 8153879 04-Apr-11 11-Apr-11 5.2932 4.5170 0.7762 38325.1 38158.1 10020.6 10,356,941 0.0749 99.4% 36.5 2 8153873 11-Apr-11 18-Apr-11 4.8720 4.5025 0.3695 38494.1 38325.1 10136.4 10,620,143 0.0348 100,8% 37.0 3 6400716 18--Apr-1 1 25-Apr-1 1 4.7131 4.4456 0.2675 38660.5 38494.1 9985.8 10,462,356 0.0256 99.1% 37.0 4 6400712 25-Apr-11 02-Ms.y-11 4.6483 4.4225 0.2256 38830.9 38660.0 10251.0 10,740,212 0.0210 101.7% 37.0 5 8400706 02-May-11 09-May-11 4.9720 4.3985 0.5735 36998.2 38830.9 10038.6 10,517,676 0.0545 99.6% 37.0 6 6401000 09-May-11 16-May-11 4.6046 4.3493 0.2553 39164.6 38998.2 9988.2 10,464,870 0.0244 99.1% 37.0 7 8400994 16-May-11 23-May-11 4.5646 4.3331 0.2316 39333.4 39164.6 10124.4 10,578,901 0.0219 100.4% 36.9 B 6400988 23-May-11 30-May-11 5.3001 4.2786 1.0215 39525.3 39333.4 ll517.0 12,034,017 0.0849 114.3'Yo 36.9 9 8400982 3G-May-11 06-Jun-11 4.6633 4.3127 0.3506 39670.0 39525.3 8682.6 9,072,376 0.0386 86.1% 36.9 10 6153867 06-Jurt-11 13-Jun-11 4.8722 4.5326 0.3396 39636.6 39670.0 9993.6 10,357,333 0.0328 99.1% 36.6 11 8153661 13-Jun-11 20-Jun-11 4.6331 4.5085 0.3246 40005.6 39636.8 10143.0 10,454,727 0.0310 100.6% 36.4 12 8400979 20-Jun-11 27-Jurt-11 4.4222 4.3139 0.1063 40172.7 40005.6 10020.6 10,328,565 0.0105 99.4% 36.4 13 6400974 27-Jun-11 04-Jul-11 4.7935 4.3273 0.4662 40365.4 40172.7 11562.6 11,917,956 0.0391 114.7% 36.4 Totals 91 2164.0 4.61171 4.40324 0.4085 7797800 132464.4 137,906,073 0.0380 101.1% 36.8 Pa g eLl OT L Period: AprilS, 2011 through July 5, 2011 (2nd Quarter 2011) BHV-6 on stream % Week Filter Start " Number Date 1 6153880 04-Apr-11 2 8153874 11-Apr-11 3 8400717 16-Apr-11 4 6400711 25-Apr-11 5 8400705 02-May-11 6 8400999 09-May-11 7 8400993 16-May-11 8 8400987 23-May-11 9 8400981 30-May-11 10 8153868 06-Jun-1 1 11 8153862 13-Jun-11 12 8400980 20-Jun-11 13 8400972 27-Jun-11 Totals 91 ALL BHV on stream % Week # Blanks Start Date 1 8153869 04-Apr-11 2 6400722 11-Apr-11 3 8400716 1 8-Apr-11 4 8400710 25-Apr-11 5 8400701 02-May-11 6 6400998 09-May-11 7 8400992 16-May-11 6 8400966 23-May-11 9 8153863 30-May-11 10 8153857 06-Jun-11 11 8400978 13-Jun-11 12 8400970 20-Jun-11 13 6153851 27-Jun-11 Totals 91 101.1% Stop Date 11-Apr-11 18-Apr-11 25-Apr-11 02-May-1 t 09-May-11 16-May-11 23-May-11 30-May-11 0&-Jun-11 13-Jun-11 20-Jun-11 27-Jun-11 04-Jul-11 2184.0 98.0% Stop Date 11-Apr-11 18-Apr-11 25-Apr-11 02-May-11 09-May-11 16-May-11 23-May-11 30-May-11 06-Jun-11 13-Jun-11 2Q-Jun-11 27-Jun-11 04-Jul-1 1 2184.0 Gross 5.0261 4.8707 4.6669 4.6318 4.6670 4.4694 4.4807 4.9981 4.5186 4.7920 4.6950 4.4575 4.6210 4.68575 Net 4.4960 4.4061 4.4186 4.4222 4.4305 4.3180 4.2608 4.3208 4.5047 4.5049 4.3089 4.3220 4.5145 4.4036 Stop Tare Nel Tlme 4.4999 0.5262 4105.4 4.5197 0.3510 4274.6 4.4378 0.2291 4441.4 4.4340 0.1978 4611.5 4.3952 0.2718 4778.2 4.3056 0.1836 4945.2 4.3315 0.1492 5114.0 4.3260 0.6721 5305.9 4.2751 0.2435 5450.3 4.5267 0.2653 5617.0 4.5055 0.1695 5785.7 4.3186 0.1367 5953.2 4.2719 0.3491 6145.6 4.39599 0.2898 Page2 BHV·6 Total Volume: 4.67E+OB Start Total Total Loading, Per Cent Time Time Uters ma/m3 On Stream SCFM 3938.2 10033.2 10,369,964 0.0507 99.5% 36.5 4105.4 10150.2 10,634,601 0.0330 100.7% 370 4274.6 10008.6 10,486,244 0.0218 99.3% 37 0 4441.4 10205.4 10,692,436 0.0165 101.2% 37 0 4611 .5 10001.4 10,478,700 0.0259 99.2% )7 0 4778.2 10020.6 10,498,816 0.0175 99.4% 37.0 4945.2 10126.2 10,580,782 0.0141 100.5% 36.9 6114.0 11517.6 12,034,644 0.0568 114.3% 36.9 5305.9 8662.8 9,051,687 0.0269 85.9% 36.9 5450.3 9999.6 10,363,551 0.0256 99.2% 36.6 5617.0 10120.8 10,431,645 0.0182 100.4% 36 4 5765.7 IOOSS.4 10,364,435 0.0134 99.6% 36.4 5953.2 11542.8 11,897.548 0.0293 114.5% 36.4 132444.6 137,885,253 0.0270 101.1% 36.8 Page 22 of 22 ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA 50.00 45.00 40.00 35.00 30.00 10.00 5.00 0.00 I White Mesa Mill Ambient Gamma Levels Over Time I 10-ll-·wr-92 Background (BHV-3) subtracted from BHV-1, BHV-2, BHV-4, BHV-5, and BHV--6 --BHV-1 .--aHV-2 --BHV-3 --BHV-4 ---BHV-5 -BHV-61 ..... Q) "t Cl3 :J 0" ........ E Q) a: E 50.00 45.00 40.00 35.00 30.00 25.00 20.00 15.00 30-<-'-'eP-8t Ol-o Ct-85 09-o Cf-87 I White Mesa Mill Ambient Gamma Levels Over Time BHV-1 I 30-0ct-89 30-se 'P-91 8-0ct-93 Background (BHV-3) Subtracted from BHV-1 ---BHV-1 to .•• 'VOif-97 1.2-o Ct-99 .24-0ct -01 17-o t c-os Jo.o Cf-0? .2-0ct-09 I White Mesa Mill Ambient Gamma Levels Over Time BHV-21 30.00 ..... Q) t:: 25.00 cu ~ 0" -E Q) 20.00 a: E 15.00 Background (BHV-3) Subtracted from BHV-2 I White Mesa Mill Ambient Gamma Levels Over Time BHV-31 50.00 45.00 40.00 35.00 30.00 ...... Q) t:: 25.00 ctl :::::1 .!;!' E Q) 20.00 a: E 4 ~~-~ 4 ~ I ~ ~ --~ -~--i -- ~~ -~ r. • " ~~· -!~~;,, -9'1 ~ ~v 4~~ ~l 1 • ~ - \f.tJ ~ ~ 4 il \.1 'J 41 • '1 ... 15.00 ~ 4 10.00 5.00 0.00 . . . ... ... Background (BHV-3) --BHV-3 I White Mesa Mill Ambient Gamma Levels Over Time BHV-4 1 30.00 ...... Q) t::: 25.00 ctS ::J 0" --E Q) 20.00 a: E 15.00 3o.8 03-o 01.0 09.0 3o.0 3o.8 8-ocr ep.81 Ct-83 Ct-8S Ct-87 Ct-89 ep.91 ·93 Background (BHV-3) Subtracted from BHV-4 -BHV-4 I White Mesa Mill Ambient Gamma Levels Over Time BHV-sl 30.00 ,_ Q) t 25.00 ro ::J 0" -E Q) C( 20.00 E 15.00 3o.se 03-o t O?.o t 09-o t 3o.o t 3o.se 8-0ct 9 16-0ct.nr:: 10.A•a".9-. 12-0ct-99 24-0ct-01 3-0ct-03 'P·8t c ·83 c -8s c ·8? c ·89 'll-91 • 3 ~... •v, Y • r 1?.0ct-os 30-0ct-o? 2-0ct-og Background (BHV-3) Subtracted from BHV-5 .........-sHV-5 I White Mesa Mill Ambient Gamma Levels Over Time BHV-61 50.00 45.00 40.00 35.00 30.00 .... Q) 25.00 t (1j :::l 0" E 20.00 Q) a: E 15.00 10.00 5.po 0.00 ~ A_.] ·---~ .. . ' .. .. ''. '' --- Background (BHV-3) Subtracted from BHV-6 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 White Mesa Mill First Quarter 2011 Environmental Gamma Monitor Results Mean Total Days Ambient Date Date Badge at Dose mRem I mRem I mRem I Location Issued Returned WMM Equivalent hour Day Week Administration Vault 117/2011 4128/2011 111 38.9 0.01 0.350 2.45 V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Y ellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Corner Ore Pad Met. Lab Filter Press Room BHV-1 BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control# 2 Vault 117/2011 4/28/2011 I /7/20 11 4/28/20 II I /7/20 1 I 4/28/20 I I 1/7/2011 4/28/201 I 117/2011 4/28/20 I I l/7/2011 4/28/2011 117/20 11 4/2 8/20 I I 1/7/2011 4/28/2011 11712011 4/28/2011 1/7/2011 4/28/2011 1/7/2011 4/28/2011 1/7/2011 4/28/2011 1/7/2011 4/28/2011 117/2011 4/28/2011 1/7/2011 4/28/2011 1/7/2011 4/28/2011 11712011 4/28/2011 1/7/2011 4/28/2011 117120 11 4/28/2011 117120 11 4/2 8/20 11 11712011 4/28/2011 11712011 4/28/2011 1/7/2011 4/28/20 11 11712011 4/28/2011 11712011 4/28/2011 1/7/2011 4/28/2011 1/7/2011 4/28/2011 1/7/2011 4/28/20 11 1 17120 11 4/28/20 I 1 1/7/2011 4/28/201 I I 1712011 4/28/20 11 11712011 4/28/20 I I 1/7/2011 4/28/2011 11712011 4/28/2011 1/7/2011 4/28/2011 11712011 4/28/20 II 11712011 4/28/2011 I 1712011 4/28/20 II 11712011 4/28/20 II 11712011 4/28/2011 111 111 111 111 111 111 I 11 111 I 11 111 Ill Ill 111 Ill 111 Ill Ill Ill 111 Ill Ill Ill 111 I 11 I 11 I I 1 111 11 I 111 Ill Ill Ill 111 111 111 I 1 I Ill 111 Ill I I I 59.8 32.7 96I 119 165.4 297.8 357.7 125.4 98.8 337.3 215 85.4 2I4.6 41.7 34.3 34 38.2 42.2 471.1 144.6 89.I 102.8 49.9 106 87I.4 421.9 112.8 65.7 180.1 60.4 447.1 233.4 370.9 232.8 284 142.9 172 40.6 37.9 39 0.02 0.01 0.36 0.04 0.06 0.11 0.13 0.05 0.04 0.13 0.08 0.03 0.08 0.02 0.01 0.01 0.01 0.02 0.18 0.05 0.03 0.04 0.02 0.04 0.33 0.16 0.04 0.02 0.07 0.02 0.17 0.09 0.14 0.09 0.11 0.05 0.06 0.02 0.01 0.01 0.539 0.295 8.658 1.072 1.490 2.683 3.223 1.130 0.890 3.039 1.937 0.769 1.933 0.376 0.309 0.306 0.344 0.380 4.244 1.303 0.803 0.926 0.450 0.955 7.850 3.801 1.016 0.592 1.623 0.544 4.028 2.103 3.341 2.097 2.559 1.287 1.550 0.366 0.341 0.351 3.77 2.06 60.60 7.50 10.43 18.78 22.56 7.91 6.23 21.27 13.56 5.39 13.53 2.63 2.16 2.I4 2.41 2.66 29.71 9.12 5.62 6.48 3.15 6.68 54.95 26.61 7.11 4.14 11.36 3.81 28.20 14.72 23.39 14.68 17.91 9.01 10.85 2.56 2.39 2.46 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 *Lost Badge White Mesa Mill Second Quarter 2011 Environmental Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Y ellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Corner Ore Pad Met. Lab Filter Press Room BHV-1 BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit-North North Control# 1 North Control# 2 Date Issued 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4/28/2011 4128/2011 4128/2011 Date Returned 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/612011 7/612011 7/612011 7/612011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 7/6/2011 Total Days Badge at WMM 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 Ambient Dose Equivalen t 27.7 34.9 24.8 487.9 71.5 162.2 220.9 73.7 60.6 225.9 49 143.3 26 24.2 22.4 21.5 25.6 282.1 90.9 55.7 65.2 27.8 66.6 623.7 220.1 75.2 44.7 104.3 38.3 284.5 152.4 244.1 246.4 126 33.4 56.1 25.1 21.3 mRem/ hour 0.02 0.02 0.01 0.29 0.04 0.10 0.00 0.13 0.04 0.04 0.14 0.00 0.03 0.09 0.02 0.01 O.Ql 0.01 0.02 0.17 0.05 0.03 0.04 0.02 0.04 0.38 0.13 0.05 0.03 0.06 0.02 0.17 0.09 0.15 0.15 0.08 0.02 0.03 0.02 0.01 mRem/Day 0.401 0.506 0.359 7.071 1.036 2.351 0.000 3.201 1.068 0.878 3.274 0.000 0.710 2.077 0.377 0.351 0.325 0.312 0.371 4.088 1.317 0.807 0.945 0.403 0.965 9.039 3.190 1.090 0.648 1.512 0.555 4.123 2.209 3.538 3.571 1.826 0.484 0.813 0.364 0.309 mRem/ Week 2.81 3.54 2.52 49.50 7.25 16.46 0.00* 22.41 7.48 6.15 22.92 0.00* 4.97 14.54 2.64 2.46 2.27 2.18 2.60 28.62 9.22 5.65 6.61 2.82 6.76 63.27 22.33 7.63 4.53 10.58 3.89 28.86 15.46 24.76 25.00 12.78 3.39 5.69 2.55 2.16 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC 0 0 0 0 m m I I 0 0 CXl ""'-~ 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 - 8/27/1987 8/27/1988 - 8/27/1989 8/27/1990 8/27/1991 8/27/1992 8/27/1993 f 8/27/1994 z 8/27/1995 m t 8/27/1996 8/27/1997 z ~ 8/27/1998 f 8/27/1999 (/) 8/27/2000 ~ 8/27/2001 8/27/2002 8/27/2003 8/27/2004 - 8/27/2005 8/27/2006 - 8/27/2007 8/27/2008 8/27/2009 8/27/2010 (Log Scale) 0 0 0 0 0 0 m m m I I 6 0 0 0> CJ1 .j:>. 0 0 0 0 m m I I 0 0 Ct.> 1\) -t: 0 ::::.: " (.Q - (Log Scale) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I 6 I 0 0 0 0 0 0 co -....1 en 01 .j::. c..v 1\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 ., C" I 8/27/1989 N ...... 0 8/27/1990 0 0 8/27/1991 ::::J n CD 8/27/1992 -::::J ... """' Q) 8/27/1993 ... s· f 8/27/1994 ::::J tn z 8/27/1995 -3' m < CD f 8/27/1996 (Q CD ... 8/27/1997 -Q) ... z s· :E 8/27/1998 ::::J -s::::: f 8/27/1999 0 ::::::: (/) 8/27/2000 "' :E (Q -8/27/2001 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 (Log Scale) ...... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 00 -...,J ()) 01 .j:>. w 1\) 01-Jan-81 - 01-Jan-82 -:e :::I 01-Jan-83 -~ m 01-Jan-84 s m 01-Jan-85 CJ) )> 01-Jan-86 -s r-01-Jan-87 -r- 01-Jan-88 z 0 01-Jan-89 :xJ -4 :::I 01-Jan-90 -m )> 01-Jan-91 CJ) -4 01-Jan-92 -0 t ., 01-Jan-93 -s :u r- Sll 01-Jan-94 --r-"' ~:xJ I" 0) 01-Jan-95 -_,D) -I 1 "N 01-Jan-96 (QN -0) -u D) cr 01-Jan-97 -::::J "' ~ c. 0 01-Jan-98 ""C C" I 01-Jan-99 N ...a. 0 01-Jan-00 (') 0 01-Jan-01 ::::J () C'D 01-Jan-02 ::::J -.., 01-Jan-03 D) -c;· 01-Jan-04 ::::J en 01-Jan-05 ::::J < 01-Jan-06 C'D (Q C'D 01-Jan-07 -D) -01-Jan-08 c;· ::::J 01-Jan-09 01-Jan-10 01-Jan-11 (Log Scale) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m I I 0 0 ()) -....1 m m I I 0 0 c.u 1\) m m m 6 I I 0 0 0) 01 .J:>. 01-Jan-81 =E 01-Jan-82 ::I: =i 01-Jan-83 m s: 01-Jan-84 -m en 01-Jan-85 )> s: 01-Jan-86 r-r- 01-Jan-87 -z 01-Jan-88 -0 :::c 01-Jan-89 -4 ::I: 01-Jan-90 =E m en 01-Jan-91 -4 0 t 01-Jan-92 01-Jan-93 :D "T1 s: r- If 1\) 01-Jan-94 1\) ()) f 01-Jan-95 01-Jan-96 ""0 C" "' 01-Jan-97 ~ c• o:::c -·m -. ~I\) CCN -0) D) :::l a. 0 01-Jan-98 ""C C" I 1\) 01-Jan-99 ...... 0 01-Jan-00 0 0 01-Jan-01 :::l (") tD 01-Jan-02 :::l -""'' D) 01-Jan-03 -s· 01-Jan-04 :::l en 01-Jan-05 -:::l < 01-Jan-06 tD cc tD 01-Jan-07 -D) -01-Jan-08 s· :::l 01-Jan-09 01-Jan-1 0 - 01-Jan-11 - 0 0 m I 0 CXl 01-Jan-81 01-Jan-82 01-Jan-83 - 01-Jan-84 01-Jan-85 01-Jan-86 - 01-Jan-87 01-Jan-88 - 01-Jan-89 01-Jan-90 01-Jan-91 - 01-Jan-92 01 -Jan-93 - 01-Jan-94 01-Jan-95 01-Jan-96 - 01-Jan-97 01-Jan-98 01-Jan-99 01-Jan-00 01-Jan-01 01-Jan-02 01-Jan-03 01-Jan-04 01-Jan-05 01 -Jan-06 - 01-Jan-07 - 01-Jan-08 - 01-Jan-09 01-Jan-10 01-Jan-11 0 0 m I 0 ......, (Log Scale) 0 0 0 0 0 0 m m m 6 6 I 0 0) 01 ~ 0 0 m I 0 w 0 0 m ~ 0 0 m I 0 0 0 m + 0 0 :e :J: =t m s:: m C/) )> s:: -r-r- C/) 0 c: -4 :J: :E m ~ 0 "TT s:: r-c• o:c =::.:'P ~N CCN -0) Q) :::l a. "tJ C" I N ...... 0 0 0 :::l (') CD :::l -Cil -a· :::l tn :r < CD (Q CD -Q) -a· :::l WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED QTR. SAMPLED DATE 3rd'81 27-Aug-81 4th '81 20-0ct-81 2nd'82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd'83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd'84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd'86 10-Jul-86 4th '86 18-Dec-86 2nd'87 20-Apr-87 3rd'87 05-Jun-87 4th '87 22-Dec-87 2nd'88 19-Apr-88 3rd'88 28-Jul-88 2nd'89 07-Apr-89 3rd'89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd'90 20-Jun-90 3rd'90 17-0ct-90 1st '91 10-Apr-91 2nd '91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd'93 26-Jun-93 3rd '93 12-0ct-93 1st '94 11-May-94 2nd'94 19-Jul-94 3rd'94 28-Nov-94 1st '95 11-Apr-95 2nd '95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd'96 14-Nov-96 lst'97 21-Apr-97 3rd '97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd'99 07-Jul-99 4th '99 02-Dec-99 2nd'OO 21-Apr-00 2nd'OO 22-Jun-00 Ra-226 VALUE (uCi/Kg) 3.90E-04 1.40E-04 1.31E-04 1.60E-04 2.67E-06 9.36E-05 1.12E-04 1.09E-04 3.47E-04 5.61E-04 1.05E-03 8.20E-05 1.15E-04 5.72E-04 5.01E-04 8.70E-04 5.90E-04 1.60E-04 2.10E-04 4.50E-04 3.20E-05 5.60E-04 1.50E-04 6.00E-04 2.60E-04 1.80E-04 1.60E-04 1.20E-04 9.10E-05 4.50E-04 3.60E-05 l.OOE-05 7.90E-05 3.70E-05 3.00E-05 6.60E-05 1.80E-04 1.71E-05 2.40E-04 6.70E-05 1.SOE-05 5.50E-05 5.20E-05 3.00E-05 l.lOE-05 1.10E-05 8.00E-06 <9.10E-05 1.80E-05 5.70E-05 2.00E-04 6.03E-05 2.30E-05 1.50E-04 1.20E-06 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCI/Kg) ERROR (uCi/Kg) uCi/Kg (l.OE-06) l.OE-05 5.0E-08 1.10E-03 l.OE-04 l.OE-06 l.OE-05 5.0E-08 6.80E-04 8.0E-05 l.OE-06 1.3E-05 l.OE-06 4.90E-04 7.0E-05 8.0E-05 1.0E-05 5.0E-08 8.00E-04 1.7E-04 l.OE-07 l.lE-06 l.OE-06 1.08E-04 9.0E-06 l.OE-05 6.2E-06 8.0E-09 4.97E-04 9.3E-05 l.OE-04 1.2E-05 6.0E-06 1.84E-04 1.2E-05 l.OE-06 8.0E-06 4.0E-06 7.80E-04 6.2E-05 6.0E-05 1.2E-05 2.0E-09 3.75E-03 1.6E-04 4.0E-08 2.0E-04 2.0E-07 7.82E-03 3.3E-04 7.0E-08 3.0E-05 2.0E-06 3.22E-03 1.4E-04 2.0E-05 7.0E-06 3.0E-06 7.70E-04 1.3E-04 2.0E-04 1.0E-05 3.0E-06 5.10E-04 3.0E-05 2.0E-05 2.1E-05 4.0E-06 2.49E-03 l.OE-04 l.OE-05 1.3E-05 3.0E-06 1.57E-03 1.7E-03 2.0E-04 5.0E-05 3.0E-06 6.80E-04 3.0E-05 3.0E-06 7.0E-05 5.0E-08 1.50E-03 l.OE-04 l.OE-06 3.0E-05 5.0E-08 9.50E-04 4.0E-05 1.0E-06 4.0E-05 5.0E-08 1.70E-03 l.OE-04 1.0E-06 7.0E-05 5.0E-08 1.40E-03 1.0E-04 l.OE-06 2.2E-05 5.0E-08 1.50E-04 4.4E-04 l.OE-06 4.0E-05 *** l.lOE-03 l.OE-01 ••• 2.0E-05 *** 2.30E-04 2.0E-05 *** 5.0E-05 7.0E-06 2.04E-03 7.0E-05 1.4E-05 3.0E-05 4.0E-06 3.30E-04 2.0E-05 2.2E-05 2.0E-05 5.0E-08 3.20E-04 2.0E-05 l.OE-06 2.0E-05 5.0E-08 3.30E-04 2.0E-05 1.0E-06 2.0E-05 5.0E-06 3.00E-04 2.0E-05 l.OE-06 1.6E-05 2.0E-07 1.90E-04 2.0E-05 2.0E-07 4.0E-05 5.0E-08 1.09E-03 5.0E-05 l.OE-06 l.OE-05 2.0E-06 l.SOE-04 2.0E-05 l.OE-05 7.0E-06 2.0E-07 7.SOE-05 2.0E-05 l.OE-06 3.5E-05 3.0E-06 7.10E-04 7.0E-05 2.0E-05 2.2E-05 3.0E-06 2.80E-04 3.0E-05 2.0E-05 1.5E-05 3.0E-06 4.30E-05 3.SE-05 Z.OE-05 2.7E-05 3.0E-06 5.30E-04 6.0E-05 2.0E-05 4.0E-05 3.0E-05 4.40E-04 6.0E-05 2.0E-04 1.2E-06 9.0E-08 3.00E-05 6.1E-06 4.5E-06 1.5E-05 1.7E-07 1.70E-04 l.lE-05 8.3E-07 5.4E-06 1.6E-07 1.40E-04 1.3E-05 7.9E-07 1.5E-06 1.5E-07 5.10E-05 4.5E-06 7.6E-07 5.0E-06 1.8E-07 6.70E-05 l.OE-05 8.8E-07 2.5E-06 1.5E-07 3.20E-05 4.5E-06 1.8E-07 2.5E-06 1.8E-07 1.40E-04 7.1E-06 9.3E-07 4.7E-07 1.2E-07 4.10E-05 3.6E-06 6.1E-07 4.3E-07 1.3E-07 2.10E-05 7.3E-07 6.7E-07 1.2E-06 5.6E-07 1.40E-04 4.6E-06 l.lE-07 9.1E-05 9.1E-05 <4.50E-04 4.5E-04 4.SE-04 1.2E-06 6.3E-08 4.00E-05 1.8E-06 3.2E-07 l .OE-06 8.2E-08 8.70E-05 5.0E-06 4.1E-07 3.0E-06 1.2E-07 3.00E-04 l.OE-05 6.0E-05 1.4E-06 8.3E-08 1.40E-04 4.7E-06 4.2E-07 l.OE-06 2.3E-07 2.10E-05 l.OE-06 l.lE-06 3.0E-06 1.2E-07 1.60E-04 8.0E-06 5.9E-07 l.OE-07 2.8E-07 1.60E-04 l.OE-05 1.4E-06 4th '00 21-Dec-00 1.60E-06 1.1E-06 3.7E-07 S.10E-OS S.OE-06 1.9E-06 1st '01 30-Apr-01 l.OOE-06 1.0E-07 2.4E-07 <1.2E-06 l.OE-07 2.4E-07 2nd '01 14-Jun-01 2.30E-06 2.0E-07 9.9E-08 3.80E-06 2.0E-07 S.OE-07 4th '01 17-Dec-01 9.10E-06 2.4E-06 1.2E-07 3.S7E-OS 3.0E-06 6.0E-07 1st '02 07-May-02 3.30E-OS 1.8E-06 7.6E-07 4.SOE-OS 2.6E-06 l.OE-OS 2nd'02 07-Jul-02 S.SSE-OS 2.8E-06 7.6E-07 S.31E-OS 3.9E-06 l.OE-OS 4th '02 1S-Dec-02 7.7SE-OS 3.6E-06 7.6E-07 1.29E-04 6.2E-06 l.OE-OS 1st '03 21-Mar-03 9.10E-06 1.3E-06 3.6E-07 1.13E-OS 1.6E-06 3.4E-06 2nd'03 10-Jun-03 2.SOE-OS 1.3E-06 3.6E-07 3.26E-06 2.0E-06 7.4E-08 4th '03 20-Nov-03 S.70E-OS 3.5E-06 l.SE-07 4.0SE-OS S.8E-06 8.3E-07 1st '04 08-Apr-04 9.38E-OS 3.7E-06 1.1E-07 S.88E-OS 3.0E-06 S.SE-07 2nd '04 12-Jun-04 S.63E-OS 3.4E-06 1.8E-07 6.42E-OS S.9E-06 9.0E-07 4th '04 30-Nov-04 8.41E-OS S.SOE-06 2.00E-08 2.48E-04 1.40E-OS 3.00E-07 1st 'OS 21-Apr-OS S.60E-OS 3.00E-06 1.40E-07 S.80E-OS 4.00E-06 6.90E-07 2nd'OS 13-Jun-OS 9.10E-06 l.SOE-06 1.80E-07 l.lOE-OS 1.20E-OS 9.00E-07 4th 'OS 10-Nov-OS 6.00E-OS 3.00E-06 l.lOE-10 1.70E-06 6.40E-07 S.SOE-10 1st '06 03-Apr-06 8.00E-OS S.OOE-06 S.OOE-08 3.40E-04 1.20E-OS l.OOE-06 2nd '06 16-Jun-06 4.10E-OS 3.10E-06 S.OOE-08 1.16E-04 6.10E-06 l.OOE-06 4th '06 28-Nov-06 1.17E-04 4.60E-06 1.90E-07 3.28E-04 9.50E-06 9.50E-07 1st '07 30-Mar-07 9.70E-OS 4.40E-06 1.90E-07 3.40E-04 8.70E-06 8.4-07 2nd'07 1-Jun-07 1.30E-OS 1.60E-06 1.90E-07 1.20E-04 6.60E-06 9.70E-07 4th '07 23-Nov-07 7.00E-OS 8.20E-06 2.00E-07 S.OOE-04 2.00E-OS 1.20E-06 1st '08 22-Apr-08 3.6E-06 3.00E-06 S.20E-07 2.3E-04 1.40E-OS l.OOE-06 2nd'08 18-Jun-08 3.2E-OS 3.20E-06 1.80E-06 6.9E-OS 3.SOE-OS S.SOE-OS 4th '08 12-Dec-08 1st '09 28-Apr-09 S.9E-04 1.3SE-OS l.SOE-06 3.4E-04 1.30E-OS l.SOE-06 2nd '09 17-Jun-09 1.9E-OS 1.4SE-06 4.90E-07 3.6E-OS l.lOE-OS 1.80E-OS 4th '09 18-Dec-09 1.7E-04 S.90E-06 4.8E-04 1.20E-OS 1st '10 13-May-10 2.2E-04 7.20E-06 l.lOE-06 1.9E-04 1.90E-OS 2.90E-OS 2nd'10 18-Jun-10 6.SE-OS 3.40E-06 7.60E-07 1.4E-04 1.90E-OS 2.90E-OS 4th '10 20-Dec-10 2.3E-OS 1.70E-06 S.20E-07 l.OE-OS 1.SOE-06 2.30E-06 2nd '11 23-Jun-11 2.4E-07 1.4E-07 1.8E-07 <2.9E-06 1.7E-06 2.9E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd'82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd'83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd'86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd'87 20-Apr-87 3rd '87 05-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd '91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 11-May-94 2nd'94 19-Jul-94 3rd '94 28-Nov-94 1st '95 11-Apr-95 2nd '95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jui-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd'97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd'99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 2.73E-03 2.00E-04 1.04E-04 2.00E-05 2.36E-06 8.58E-05 1.19E-04 9.78E-05 2.08E-04 6.05E-04 l.lOE-04 6.10E-05 1.07E-04 8.86E-04 6.66E-04 5.20E-04 4.10E-04 1.60E-04 3.60E-04 2.60E-04 3.10E-05 6.20E-04 3.40E-04 S.lOE-04 3.60E-04 1.70E-04 8.80E-05 3.00E-04 3.10E-04 5.00E-04 2.00E-05 6.50E-06 1.20E-04 1.80E-05 5.20E-05 5.10E-05 1.20E-04 3.73E-05 2.40E-04 8.40E-05 1.90E-05 1.20E-04 8.30E-05 3.60E-05 3.30E-05 5.40E-06 8.90E-06 <9.20E-05 < 6.50E-08 4.20E-05 6.20E-OS 5.45E-05 1.10E-04 3.70E-05 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCI/Kg) uCi/Kg (l.OE-06) 5.0E-05 5.0E-08 7.10E-03 3.0E-04 l.OE-06 l.OE-05 5.0E-08 8.30E-04 5.0E-05 l.OE-06 9.0E-06 7.0E-06 6.40E-04 5.0E-05 4.0E-05 1.0E-05 5.0E-08 2.20E-04 9.0E-05 l.OE-07 9.5E-07 l.OE-06 8.00E-05 l.OE-05 l.OE-05 1.4E-05 2.0E-08 3.53E-04 1.9E-05 1.0E-05 1.1E-05 5.0E-06 1.58E-04 1.3E-05 1.0E-05 7.0E-06 2.0E-06 2.16E-03 3.4E-04 3.0E-04 l.OE-05 3.0E-09 1.60E-03 7.0E-05 3.0E-08 1.6E-04 2.0E-07 2.58E-03 1.1E-04 3.0E-08 8.0E-06 3.0E-06 8.63E-04 4.2E-05 3.0E-05 6.0E-06 2.0E-06 5.40E-04 5.0E-05 5.0E-05 6.0E-06 2.0E-06 3.80E-04 3.0E-05 2.0E-05 1.8E-05 2.0E-06 4.40E-03 1.9E-04 3.0E-05 1.8E-05 3.0E-06 4.78E-03 2.1E-04 6.0E-05 1.0E-04 3.0E-06 1.70E-03 l.OE-04 6.0E-05 l.OE-04 5.0E-08 1.60E-03 1.0E-04 1.0E-06 3.0E-05 5.0E-08 5.50E-04 4.0E-05 l.OE-06 S.OE-05 5.0E-08 1.80E-03 l.OE-04 l.OE-06 5.0E-05 5.0E-08 1.90E-03 1.0E-04 1.0E-06 1.9E-05 5.0E-08 1.60E-04 4.0E-05 l.OE-06 5.0E-05 *** 1.70E-03 l.OE-04 *** 3.0E-05 *** 7.40E-04 3.0E-05 *** 6.0E-05 7.0E-06 l.OOE-03 7.0E-05 1.4E-05 3.0E-05 4.0E-06 4.80E-04 2.0E-05 2.2E-05 2.0E-05 5.0E-08 3.20E-04 2.0E-05 l.OE-06 1.6E-05 5.0E-08 2.90E-04 2.0E-05 l.OE-06 3.0E-05 5.0E-06 4.10E-04 2.0E-05 l.OE-06 3.0E-05 2.0E-07 4.70E-04 2.0E-05 2.0E-07 4.0E-05 5.0E-08 1.50E-03 l.OE-04 l.OE-06 8.0E-06 2.0E-06 9.60E-05 1.4E-05 l.OE-05 6.0E-06 2.0E-06 1.20E-04 2.0E-05 l.OE-06 4.0E-05 3.0E-06 1.21E-03 8.0E-05 2.0E-05 1.7E-05 3.0E-06 2.10E-04 3.0E-05 2.0E-05 1.9E-05 3.0E-06 1.70E-05 3.6E-05 2.0E-05 2.3E-05 3.0E-06 7.10E-04 6.0E-05 2.0E-05 l.OE-05 3.0E-05 9.80E-04 1.6E-04 2.0E-04 1.6E-06 8.4E-08 7.80E-05 7.1E-06 4.2E-07 1.5E-05 1.7E-07 2.60E-04 1.3E-05 8.3E-07 6.1E-06 1.5E-07 1.20E-04 l.lE-05 7.5E-05 1.5E-06 1.4E-07 4.50E-05 4.3E-06 7.2E-07 6.8E-06 1.4E-07 l.OOE-05 5.8E-06 7.1E-07 3.3E-06 1.9E-07 6.80E-05 6.3E-06 1.8E-07 2.5E-06 1.6E-07 8.50E-05 5.6E-06 8.4E-07 2.3E-06 1.7E-07 4.40E-05 4.8E-06 8.4E-07 3.5E-07 1.6E-07 3.20E-05 9.0E-07 7.8E-07 7.2E-07 5.4E-07 3.40E-04 6.7E-06 1.1E-07 9.2E-05 9.2E-05 <4.60E-04 4.6E-04 4.6E-04 6.5E-08 6.5E-08 <3.20E-07 3.2E-07 3.2E-07 1.0E-06 l.lE-07 1.70E-04 l.OE-05 5.5E-07 l.OE-06 l.OE-07 1.40E-04 7.0E-06 l.OE-07 1.4E-06 8.3E-08 9.20E-05 4.0E-06 4.2E-07 3.0E-06 2.2E-07 2.80E-05 1.0E-06 l.lE-06 1.0E-06 2.4E-07 2.70E-04 l.OE-05 1.2E-06 2nd'OO 22-Jun-00 2.90E-OS l.OE-06 3.3E-07 2.80E-04 2.0E-OS 1.7E-06 4th '00 21-Dec-00 2.30E-06 1.4E-06 3.7E-07 3.30E-04 S.OE-OS 1.9E-06 1st '01 30-Apr-01 2.10E-OS l.OE-06 1.SE-07 <7.6E-07 N/A 7.6E-07 2nd '01 14-Jun-01 1.30E-06 4.0E-08 1.2E-07 1.80E-06 3.0E-08 S.9E-07 4th '01 17-Dec-01 3.70E-OS 7.67E-07 8.30E-08 6.72E-OS 2.62E-06 6.00E-07 1st '02 07-May-02 4.90E-OS 2.40E-06 7.60E-07 1.28E-04 S.61E-06 l.OOE-OS 2nd'02 07-Jul-02 8.88E-OS 4.32E-06 7.60E-07 8.33E-05 4.32E-06 l.OOE-OS 4th '02 1S-Dec-02 l.SOE-04 6.2E-06 7.60E-07 3.16E-04 1.07E-OS l.OE-OS 1st '03 21-Mar-03 S.OOE-05 3.4E-06 2.71E-06 <4.2e-6 4.20E-06 2nd'03 10-Jun-03 S.60E-OS 2.0E-06 4.10E-07 1.88E-04 5.14E-06 8.2E-08 4th '03 20-Nov-03 3.20E-04 8.2E-06 1.70E-07 4.89E-04 1.25E-OS 8.3E-07 1st '04 08-Apr-04 6.29E-OS 4.1E-06 2.00E-07 1.94E-OS 4.00E-06 1.0E-06 2nd '04 12-Jun-04 6.S1E-OS 3.4E-06 1.30E-07 1.87E-OS 3.90E-06 6.5E-07 4th '04 30-Nov-04 7.SOE-OS 4.6E-06 2.0E-08 4.4SE-04 1.40E-OS 3.0E-07 1st 'OS 21-Apr-05 4.90E-OS 2.70E-06 1.30E-07 1.27E-04 4.80E-06 6.SOE-07 2nd 'OS 13-Jun-OS 2.30E-OS 2.10E-06 1.50E-07 4.70E-OS 5.10E-06 7.60E-07 4th 'OS 10-Nov-05 7.40E-OS 3.50E-06 1.20E-10 2.40E-06 8.10E-08 5.80E-10 1st '06 03-Apr-06 l.OOE-04 6.00E-06 5.00E-08 6.S4E-04 l.SOE-OS l.OOE-06 2nd'06 16-Jun-06 9.SOE-OS S.90E-06 5.00E-08 4.48E-04 1.40E-05 l.OOE-06 4th '06 28-Nov-06 8.13E-OS 4.10E-06 2.20E-07 3.2SE-04 1.12E-06 l.OOE-OS 1st '07 30-Mar-07 4.30E-OS 2.60E-06 1.70E-07 2.64E-04 7.20E-06 8.60E-07 2nd'07 1-Jun-07 S.10E-OS 3.20E-06 2.30E-07 S.30E-04 1.40E-06 1.20E-06 4th '07 23-Nov-07 7.30E-OS 6.6E-06 5.0E-08 7.00E-04 2.20E-OS l.lOE-06 1st '08 22-Apr-08 2.8E-06 2.8E-06 7.20E-07 4.40E-04 2.0E-05 l.OE-06 2nd '08 18-Jun-08 3.2E-06 3.3E-06 1.80E-06 1.40E-04 3.3E-05 S.SE-OS 4th '08 12-Dec-08 7.3E-OS 3.2E-06 7.40E-07 4.40E-04 2.5E-05 3.2E-OS 1st '09 28-Apr-09 S.3E-OS 3.6E-06 1.10E-06 1.90E-04 l.SE-05 2.2E-OS 2nd '09 17-Jun-09 2.3E-OS 1.6E-OS 5.2E-07 4.30E-OS l.OOE-OS 1.7E-OS 4th '09 18-Dec-09 5.SOE-OS 3.SOE-06 3.0E-04 l.lOE-05 1st '10 13-May-10 1.9E-04 6.10E-06 9.40E-07 S.1E-04 2.40E-OS 3.10E-OS 2nd'10 18-Jun-10 2.3E-OS 2.00E-06 7.70E-07 8.3E-OS 1.80E-OS 2.90E-OS 4TH '10 20-Dec-10 8.6E-06 9.10E-07 3.90E-07 l.lE-07 6.80E-07 l.lOE-06 2nd'11 23-Jun-11 2.1E-07 1.20E-07 1.40E-07 <2.2E-06 1.30E-06 2.20E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd'83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd'87 20-Apr-87 3rd '87 05-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd'88 28-Jul-88 2nd'89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd'90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd'91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd'92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd'93 26-Jun-93 3rd '93 12-0ct-93 1st '94 11-May-94 2nd'94 19-Jul-94 3rd '94 28-Nov-94 1st '95 11-Apr-95 2nd'95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 9.50E-04 3.00E-05 1.37E-05 3.40E-04 1.75E-05 7.13E-04 5.39E-05 6.40E-05 8.27E-05 2.72E-04 4.73E-04 6.60E·05 2.83E·04 1.57E-04 3.78E-04 2.60E-04 4.10E-04 2.90E-04 1.80E-04 2.30E-04 1.50E-04 3.10E-04 1.30E-04 4.30E-04 2.50E-04 l.lOE-04 6.10E-OS 3.40E-OS 8.00E-05 6.50E-05 l.GOE-05 1.90E-05 l.GOE-05 2.60E-05 3.00E-05 3.10E-05 2.00E-05 1.75E-05 l.OOE-04 1.70E-05 6.40E-06 2.30E-05 4.20E-05 2.10E-05 5.50E-06 S.30E-06 2.50E-OS <7.90E-05 3.60E-07 4.30E-05 2.40E-05 2.23E-OS 1.50E-04 l.OOE-04 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCI/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06) 2.0E-05 5.0E-08 1.50E-04 l.OE-05 l.OE-06 3.0E-06 5.0E-08 1.50E-04 2.0E-05 l.OE-06 3.0E-06 3.0E-06 3.80E-04 4.0E-05 4.0E-05 2.0E-05 5.0E-08 3.68E-03 2.7E-04 l.OE-07 3.0E-06 2.0E-06 7.92E-04 4.0E-06 2.0E-05 7.3E-05 9.0E·08 2.51E-03 3.0E-04 3.0E·04 4.5E-06 2.0E-06 6.88E-04 4.3E-05 4.0E-05 7.0E-06 4.0E-06 1.20E-03 l.OE-04 4.0E-05 6.3E-06 3.0E-09 1.80E-03 l.OE-04 9.0E-08 1.5E-04 2.0E-07 4.70E-03 7.2E-04 3.0E-07 1.6E-07 3.0E-06 7.07E-04 3.6E-05 3.0E-05 7.0E-06 4.0E-06 4.90E-04 3.0E-05 3.0E-05 2.0E-05 7.0E-06 1.50E-03 l.OE-04 7.0E-05 l.OE-05 4.0E-06 4.14E-03 1.8E-04 3.0E-05 l.OE-05 2.0E-06 1.65E-02 7.0E-04 l.OE-04 2.0E-05 2.0E-06 1.70E-03 1.0E·04 l.OE-04 7.0E-05 5.0E-08 2.20E-03 1.0E-04 l.OE-06 4.0E-05 5.0E·08 7.50E-04 5.0E-05 l.OE-06 3.0E-05 5.0E-08 2.40E-03 1.0E-04 l.OE-06 5.0E-05 5.0E-08 2.90E-03 l.OE-04 l.OE-06 3.0E-05 5.0E-08 4.30E-03 2.0E-04 l.OE-06 4.0E-05 ... 4.20E-03 l.OE-04 *** 2.0E-05 ••• 1.50E-03 l.OE-04 ••• 5.0E-05 1.4E-05 3.50E-03 1.4E-04 2.7E-05 3.0E-05 5.0E-06 2.39E-03 5.0E-05 2.5E-05 2.0E-05 5.0E-08 6.60E-04 3.0E-05 l.OE-06 1.4E-05 5.0E-08 6.10E-04 3.0E-05 l.OE-06 1.1E-05 5.0E-06 2.20E-04 1.0E-05 l.OE-06 6.0E-06 2.0E-07 1.20E-04 l.OE-05 2.0E-07 1.4E-05 5.0E-08 9.10E-04 5.0E-05 l.OE-06 7.0E-06 2.0E-06 3.20E-04 2.0E-05 l.OE-05 1.0E-05 2.0E-07 2.20E-04 2.0E-05 l.OE-06 1.8E-05 3.0E-06 7.60E-04 6.0E-05 2.0E-05 2.0E-05 3.0E-06 3.40E-04 3.0E-05 2.0E-05 1.4E-05 3.0E-06 O.OOE+OO 3.0E-05 2.0E-05 1.6E-05 3.0E-06 4.20E-04 G.OE-05 2.0E-05 5.0E-06 3.0E-05 3.90E-04 8.0E-05 2.0E-04 1.7E-06 7.6E-08 1.30E-04 7.8E-06 3.8E-07 9.0E-06 1.5E-07 2.60E-04 1.2E-05 7.4E-07 1.5E-06 1.6E-07 1.60E-04 1.5E-05 8.1E-07 6.0E-07 1.4E-07 4.40E-05 4.2E-06 7.0E-07 2.2E-06 1.7E-07 6.60E-05 9.6E-06 8.3E-07 2.2E-06 1.7E-07 l.OOE-04 6.7E-06 1.8E-07 2.0E-06 1.6E-07 1.90E-04 7.3E-06 8.2E-07 4.2E-07 1.4E-07 3.30E-05 3.9E-06 7.0E-07 3.2E-07 1.3E-07 1.90E-05 6.9E-07 6.3E-07 9.5E-07 5.9E-07 1.30E-04 4.7E-06 1.2E-07 7.9E-05 7.9E-05 <3.90E-04 3.9E-04 3.9E-04 1.4E-07 3.3E-08 <1.7E-07 1.7E-07 1.7E-07 l.OE-06 7.6E-08 2.50E-04 l.OE-05 3.8E-07 l.OE-06 1.2E-07 1.70E-04 8.0E-06 6.2E-07 8.6E-07 1.2E-07 2.30E-04 7.0E-06 5.9E-07 3.0E-06 2.0E-07 1.70E-05 l.OE-06 l.OE-06 2.0E-06 1.2E-07 l.lOE-04 7.0E-06 6.1E-07 2nd'OO 22-Jun-00 1.30E-06 l .OE-07 2.4E-07 2.00E-04 l.OE-OS 1.2E-06 4th '00 21-Dec-00 1.20E-06 9.0E-07 2.4E-07 1.20E-04 3.0E-OS 1.2E-06 1st '01 30-Apr-01 1.80E-06 l.OE-07 1.7E-07 <8.3E-07 N/A 8.3E-07 2nd'01 14-Jun-01 2.60E-06 2.0E-07 9.9E-08 l.lOE-06 2.0E-08 S.OE-07 4th '01 17-Dec-01 2.63E-06 4.6E-OS 1.2E-07 9.40E-OS 3.7E-06 6.0E-07 1st '02 07-May-02 3.50E-05 2.2E-06 7.6E-07 1.36E-04 S.GE-06 1.0E-OS 2nd'02 07-Jul-02 4.02E-OS 2.3E-06 7.6E-07 7.04E-OS 4.1E-06 l .OE-05 4th '02 1S-Dec-02 8.10E-OS 3.9E-06 7.6E-07 2.87E-04 8.5E-06 l.OE-OS 1st '03 21-Mar-03 3.70E-OS 2.6E-06 2.4E-06 2.69E-OS 2.0E-06 3.7E-06 2nd'03 10-Jun-03 1.30E-OS l.OE-06 S.2E-07 <l.OOE-07 1.0E-07 4th '03 20-Nov-03 1.60E-04 1.3E-OS 1.2E-07 1.42E-04 6.4E-06 5.9E-07 1st '04 08-Apr-04 1.40E-04 7.7E-06 l.lE-07 6.10E-06 2.7E-06 S.SE-07 2nd'04 12-Jun-04 6.S1E-OS 3.2E-06 l.SE-07 S.27E-OS 4.9E-06 7.6E-07 4th '04 30-Nov-04 8.40E-OS S.7E-06 3.0E-08 3.39E-04 1.6E-OS 3.0E-07 1st 'OS 21-Apr-OS 1.70E-OS 1.6E-06 1.3E-07 4.50E-OS 3.SE-06 6.SE-07 2nd'OS 13-Jun-05 l.SOE-OS 1.6E-06 1.4E-07 7.00E-05 S.1E-06 6.9E-07 4th 'OS 10-Nov-OS 3.80E-OS 2.1E-06 8.6E-10 1.20E-06 4.8E-08 4.3E-10 1st '06 03-Apr-06 1.00E-04 6.0E-06 S.OE-08 3.30E-04 1.1E-OS l.OE-06 2nd'06 16-Jun-06 3.40E-OS 2.SE-06 S.OE-08 1.37E-04 6.0E-06 l.OE-06 4th '06 28-Nov-06 7.31E-OS 3.20E-06 1.60E-07 2.98E-04 8.SOE-06 8.20E-07 1st '07 30-Mar-07 3.00E-OS 2.20E-06 1.70E-07 3.20E-04 7.90E-06 8.40E-07 2nd '07 1-Jun-07 1.10E-04 4.60E-06 2.3-07 3.20E-04 1.10E-05 l.lOE-06 4th '07 23-Nov-07 S.60E-OS S.20E-06 S.OOE-08 6.40E-04 1.90E-0S l.OOE-06 1st '08 22-Apr-08 3.20E-OS 2.30E-06 7.20E-07 2.30E-04 l.SOE-05 l.OOE-06 2nd '08 18-Jun-08 1.2SE-OS 2.20E-06 1.80E-06 S.OOE-OS 3.00E-05 4.80E-03 4th '08 12-Dec-08 1st '09 28-Apr-09 2.60E-OS 2.90E-06 1.40E-06 3.70E-OS 1.50E-06 2.SOE-05 2nd '09 17-Jun-09 2.40E-OS 1.40E-06 3.90E-07 3.SOE-OS 7.90E-06 1.30E-05 4th '09 18-Dec-09 3.1E-OS 2.30E-06 2.1E-04 8.40E-06 1st '10 13-May-10 2.0E-OS 2.10E-06 9.40E-07 S.6E-OS 1.50E-OS 2.40E-05 2nd '10 18-Jun-10 l.lE-05 1.30E-06 6.60E-07 7.8E-OS 1.60E-OS 2.SOE-OS 4th '10 20-Dec-10 6.7E-06 9.10E-07 4.80E-07 8.0E-07 7.90E-07 1.30E-06 2nd '11 23-Jun-11 <1.7E-07 6.9E-08 1.7E-07 <2.5E-06 l.SE-06 2.5E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a d1saster area due to drought, no samples were collected dunng th1s penod EI\ERGY ,'\:.'H"'/\ICH:_:.... www.energy1ab.com AMIJtkll £m~~~~g Sl17c. IW Helena, MT 877-472-0711 • Billings, MT BG0-735-4489 • Casper, WY 888-235-0515 Gilletta, WY 11&-686-7175 • Rapid City, SO 888-172-1225 • College Station, TX 888-690-2218 August 02, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11 061059 ANALYTICAL SUMMARY REPORT Project Name: Late Spring Vegetation Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 6/24/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 061059-001 North East 06/23/11 9:00 06/24/11 Vegetation Digestion, Radiochemistry Lead 210 Rad ium 226 C11 061059-002 North West 06/23/11 9:45 06/24/11 Vegetation Same As Above C11 061059-003 South West 06/23/11 1 0:15 06/24/11 Vegetation Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as received basis unless otherwise indicated. Samples corrected for dry weight indicate units that have -dry appended. If you have any questions regarding these test results, please call. Report Approved By: o¥~ £) wb!~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.08.02 15:46:38 -06:00 Page 1 of 9 www.energylab.com AM/yflr:6l bulllltJI:t Slllu 11$2 Helena, MT 871-472-0711 • Billings, MT 800-735·4489 • Casper, WY 888-235·0515 GllleHe, WY 888·886·7175 • Ra ld City, SO 888-672-1225 • Collage Station, TX 888-&80-2218 CLIENT: Denison Mines USA Corp Project: Late Spring Vegetation Report Date: 08/02/11 Sample Delivery Group: C11 061059 CASE NARRATIVE BRANCH LABORATORY SUBCONTRACT ANALYSIS Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc.-Rapid City, SD eli-t-Energy Laboratories, Inc.-College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001 ; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 9 EI\ERGY J\• _L•I.' d Ll-.:" ~ www.energylab.com ~~Situ11U Helena, MT 877-472-0711 • Billings, MT BG0-735-4489 • Casper, WY 888-235-8515 Gillette, WY 886-888-7175 • Rapid City, SD 188-672-1225 • College Station, TX 188-610-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Late Spring Vegetation C11 061059-001 Client Sample ID: North East Analyses RADIONUCLIDES-TOTAL Lead 210 Lead 210 precision(±) Lead 210 MDC Lead 21 0 altu Lead 21 0 precision (±) altu Lead 210 MDC altu Radium 226 Radium 226 precision (±) Radium 226 MDC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -3.0E-08 1.7E-06 2.9E-06 -0.030 1.7 2.9 2.4E-07 1.4E-07 1.8E-07 0.24 0.14 0.18 Units uCilkg uCilkg uCilkg pCilkg pCilkg pCilkg uCilkg uCilkg uCilkg pCilkg pCilkg pCilkg MDC -Minimum detectable concentration Report Date: 08/02/11 Collection Date: 06/23/11 09:00 DateReceived: 06/24/11 Matrix: Vegetation MCU Qualifier RL QCL Method Analysis Date I By u E909.0 07128111 08:01 I eli-cs E909.0 07128111 08:01 I eli-cs E909.0 07128111 08:01 I eli-cs u E909.0 07128111 08:01 I eli-cs E909.0 07128111 08:01 I eli-cs E909.0 07128111 08:01 I eli-cs E903.0 07120111 23:32/trs E903.0 07120111 23:321 trs E903.0 07120111 23 :32 /Irs E903.0 07120111 23:32 / trs E903.0 07/20/11 23:32 / trs E903.0 07/20/11 23:32/trs MCL -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 3 of 9 -. EI\ERGY .'\1 J'Jli/\l' Ut '• www.energylab.com AM/ytJcll rxuu-t Sltlct ISS/ Helena, MT877-472-0711 • Billings, MT BOD-735·4488 • Casper, WY 888-235-0515 Gillette, WY 8&6·886-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-680-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LabiD: Denison Mines USA Corp Late Spring Vegetation C11 061059-002 Client Sample ID: North West Analyses RADIONUCLIDES ·TOTAL Lead 210 Lead 21 0 precision (±) Lead 210 MDC Lead 21 0 altu Lead 21 0 precision (±) altu Lead 21 0 MDC altu Radium 226 Radium 226 precision (±) Radium 226 MDC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -3.3E-07 1.3E-06 2.2E-06 -0.33 1.3 2.2 2.1E-07 1.2E-07 1.4E-07 0.21 0.12 0.14 Units uCilkg uCilkg uCilkg pCilkg pCilkg pCilkg uCilkg uCi/kg uCilkg pCilkg pCilkg pCilkg MDC -Minimum detectable concentration Report Date: 08/02/11 Collection Date: 06/23/11 09:45 DateReceived: 06/24/11 Matrix: Vegetation MCLI Qualifier RL QCL Method Analysis Date I By u E909.0 07128111 11 :01 I eli-cs E909.0 07128111 11 :01 I eli-cs E909.0 07128111 11 :01 I eli-cs u E909.0 07128111 11 :01 I eli-cs E909.0 07128111 11 :01 I eli-cs E909.0 07128111 11 :01 I eli-cs E903.0 07120111 23:32 I Irs E903.0 07120111 23 :32 1 Irs E903.0 07120111 23:32 1 trs E903.0 07120111 23 :321 trs E903.0 07120111 23:32/trs E903.0 07120111 23:32 I trs MCL -Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 4 of 9 EN:RGY ,.,. 'lJt-:i,j tjl•l' '-' ftW.energylab.com Alu(yticll ~ ~•1151 Helena, MT 877-472-0711 • Billings, MT BOD-735-4489 • Casper, WY 888-235-0515 Gillette, WY 886·888-7175 • Rapid City, Sll 888-&72-1225 • College Station, TX 888-&90-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Late Spring Vegetation C11 061059-003 Client Sample ID: South West Analyses RADIONUCLIDES ·TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Lead 21 0 altu Lead 21 0 precision (±) altu Lead 21 0 MDC altu Radium 226 Radium 226 precision (±) Radium 226 MDC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -7.3E-07 1.5E-06 2.5E-06 -0.73 1.5 2.5 -8.9E-08 6.9E-08 1.7E-07 -0.089 0.069 0.17 Units uCi/kg uCi!kg uCilkg pCilkg pCilkg pCilkg uCilkg uCilkg uCilkg pCilkg pCilkg pCilkg MDC-Minimum detectable concentration Report Date: 08/02/11 Collection Date: 06/23/11 10:15 DateReceived: 06/24/11 Matrix: Vegetation MCL/ Qualifier RL QCL Method Analysis Date I By u E909.0 07128111 12:01 I eli-cs E909.0 07/28/1 1 12:01 I eli-cs E909.0 07128111 12:01 I eli-cs u E909.0 07128/11 12:01 I eli-cs E909.0 07128111 12:01 I eli-cs E909.0 07128111 12:01 I eli-cs u E903.0 0712011 1 23 :32 I trs E903.0 07120111 23 :32 I trs E903.0 0712011 1 23:32 I trs u E903.0 07120111 23:32 I trs E903.0 0712011 1 23:32 I trs E903.0 07120/11 23:32 I trs MCL -Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 5 of 9 EI\ERGY ,"'> 1 ::. i ~ J' I '-I "I > ', www.entrgylab.com MMJIICIII&ulltia~ 11112 Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 8118-235-0515 Gillette, WY 1186-888-7175 • Rapid City, SD 8118-672-1225 • College Station, 1X 81111-610-2218 Client: Denison Mines USA Corp Project: Late Spring Vegetation QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 08/02/11 Work Order: C11 061059 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E903.0 Sample ID: MB-30410 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample ID: LCS-30410 Radium 226 Sample ID: C11061059-002AMS Radium 226 Sample ID: C11061059-002AMSD Radium 226 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Method Blank 2E-07 uCi/kg 2E-07 uCi/kg 3E-07 uCi/kg Laboratory Control Sample 3.0E-05 uCi/kg Sample Matrix Spike 2.5E-05 uCi/kg Sample Matrix Spike Duplicate 2.6E-05 uCi/kg Run: BERTHOLD 770-1 _110715A Run: BERTHOLD 770-1 _11 0715A 116 70 130 Run: BERTHOLD 770-1 _110715A 109 70 130 Run: BERTHOLD 770-1 _110715A 111 70 130 3.3 ND -Not detected at the reporting limit. Batch: 30410 07/20/11 23:32 u 07/20/11 23:32 07/20/11 23:32 07/20/11 23:32 20.7 U -Not detected at minimum detectable concentration Page 6 of 9 EN:RGY / Jl' I\ I',, .I! . www.energylab.com IM/ftlal~ltlu Jet Helena, MT 177-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Glllalte, WY 88&-88&-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-610-2218 Client: Denison Mines USA Corp Project: Late Spring Vegetation QAIQC Summary Report Prepared by Casper, WY Branch Report Date: 08/02/11 Work Order: C11 061 059 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E909.0 Sample ID: C11061059-001AMSD Lead 210 Sample ID: C11061059-001AMS Lead 210 Sample ID: LCS-14459 Lead 210 Sample ID: MB-14459 Lead 210 Lead 210 precision (±) Lead 210 MDC Qualifiers: RL-Analyte reporting limit. 3 MDC - Minimum detectable concentration Sample Matrix Spike Duplicate 0.00023 uCi/kg Sample Matrix Spike 0.00020 uCilkg Laboratory Control Sample 0.00030 uCi/kg Method Blank 2E-06 uCi/kg 7E-06 uCi/kg 1E-05 uCi/kg Batch: T_14459 Run: SUB-T41494 07/28/11 10:01 95 70 130 10 18.3 Run: SUB-T41494 07/28/11 09:01 83 70 130 Run: SUB-T41494 07/28/11 07:01 81 70 130 Run: SUB-T41494 07/28/11 06:01 u NO -Not detected at the reporting limit. U-Not detected at minimum detectable concentration Page 7 of 9 EI\ERGY ! / i( ll • ,-,., I(' '• www.energylab.com ~~Sillclll51 Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-1515 Gillatte, WY 888-186-7171 • Rapid City, SO 888-&72-1225 • Collage Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 111~111 ~11111111111111111~111111111111!111~11111 C11061059 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 6/28/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Container!Temp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Received 2 samples on 6-27-11 . Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 "C NA Yes 0 Yes 0 Date Received: 6/24/2011 Received by: dw Carrier NDA name: No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present O Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 8 of 9 Chain of Custody and Analytical Request Record Page _L off-__ l AI:JORATORIFS PLEASE PRINT (Provide as much information as ll_ossible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: De~rsoJ rYJ ,~~ / ,J.r ~/) .... ~c. It< /£dr,',.. State: bt'i Yes~ No 0 Report Mail ~d~res{.g~ ~O '1 cot::~m~z-.r len;;:~ ~ZGI Email: Sampler: (Please Print) Pfi;nudtvtG IAL ,Q;L{_~-// ~WI;.. 41wvt/'" Invoice Address: / Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: _...-Sk~ :C;u .A/ Special Report/Formats: ?: ~[1, \?@0@ [M~@(!JJ~[]:[Q) .. Contact Ell prior to Sh~ rum 0 .... RUSH sample submittal ~0 .,~ for charges and Cooler lD(s): ~ R Cl(~ ~co;go1 Qi 0 <{ scheduling -See Dow 0 EDD/EDT(Eiectronic Data) ]i>~i;-ni w c. Instruction Page s:;W Cfl ~?: I "0 0 POTW/WWTP os:=a "' ~ (.) s:: Comments: • :]W_ Format: u <((1)10 ·-:J u -051-"" <{ e r'e-~~(7~ oc 0 State: 0 LEVEL IV O .. li) c::·§ .... <D -o o I-(ll 0 Other: 0 NELAC 1l c.."'r~ I-s:: E~m . ~ <( 5 :A~~ On Ice: y N :J!I2 ~1~?: ~ 1-5 za. cu e ~ w 'E "?--7-~ q t~' Custody Seal @ ~ >1 ~ UJ (ll On Bottle {/J u y N (/) c On Cooler r4 (ll ~ U5 H Intact y) N SAMPLE IDENTIFICATION Collection Collection MATRIX Signature )N (Name, Location, Interval, etc.) Date Time Match ly I t/z,J/t;l/ 1-1/ IX X Llfihtrll? .u 1 r ti'f!J() ~ 2 AM rt.;lt.. JN e,j 1 lt/t}/t#l I ()'/'!~" /-1/ X X ~ 3 ~v.:lhl»ar ~/Z '!>/7/11 )!};~ "!-V A X. IQ) nnn 4 ' I , ~ 5 ~ 6 ~ 7 ~ 8 ~ 9 , k.?. , \0 ~·~Iff~ !6 57 Custody R~~~ by IPJ.!.L..... Datelll"ll!: j/Jt:) ~ Recerved by (prlniJ· Date!Time: Signature: ...... 'A .... ,..... t /25/:?t!/IJ Record RelinquiShed by (prinl] DateJlirne· D "'9'""'"'"· Recervetl by (prlnt): Oate!Time. Signature: MUST be Signed ft:i/0 y\ -{ lfh.v ,~":2:4':1 I 02~ "lllna ure; Sample DisQosal: Return to Client: Lab Disposal: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontr~~ othe;-"certified laboratories in order to complete the analysis requested. This serves as notice of this possibilit . AU sub-contract data e clearl notated on your anal tical report. y y y Visit our w<>h site at www.aner~lYiab.l<QID for additional information, downloadable fee schedule, forms. and links. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: FIRST QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORATION NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH February 15~16, 2011 by: TETCO 391 East 620 South American Fork, UT 84003 Phone. (801) 492-9106 Fax (801) 492-9107 fax Denison Mines Corporation 6425 SHwy91 Blanding, Utah 84511 Date of Report: May 31,2011 CERTIFICA TlON OF REPORT INTEGRITY "e:chnical Emission Testing Company (T TC ) certitie that thi report represents the truth as well as can be derived by the methods employed. Every effort was mad I. obtain ac urate and repre. enlali ve data and to comply with procedur s . et forth in the Federal R gister. Mike McNamara Reviewer: __ ___,1#jc.:...L.,__-~,_· __________ _ Datc: _______ S'_/"l:>_l_(_,_' _______ _ Dean A Kitchen R view 1·: ~t>~ ------~~~~~-.?---~---- Dat : _______ .f"'_-...,..,)::....1(_.-_1~/'-------- ii TABLE OF CONTENTS Introduction Test Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Test Location and Type of Process .......................................... 1 Test Dates ............................................................. 1 Pollutants Tested and Methods Applied ...................................... 1 Test Participants ......................................................... 2 Deviations From EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Summary of Results Emission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 3 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sampling and Analysis Procedures Sampling Port Location ................................................... 6 Sampling Point Location .................................................. 6 Sampling Train Description ................................................ 6 Sampling and Analytical Procedures ......................................... 7 Quality Assurance ....................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table 1 Measured Radionuclide Emissions .......................................... 3 II Percent Isokinetics ....................................................... 4 lli Sampling Point Location .................................................. 6 IV Complete Results, North Yellow Cake Scrubber ...................... Appendix A V Complete Results, Yellow Cake Dryer Baghouse ...................... Appendix A LIST OF FIGURES Figure 1 Facility Schematic Repre entation North Yellow Cake Scrubber .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... App ndix D 3 Schematic ofMethod 5/114 Sampling Train .......................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the North Yell ow Cake Scrubber and the Yell ow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat only. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 and 2 in Appendix D. Test Dates One test run was completed on the NYC Dryer February 15, 2011 and one run on February l61h. One run was completed on the Dryer Baghouse February 15, 2011. PoJlutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. 1 Test Participants Test Facility State Agency TETCO Ryan Palmer None Doug Olsen Kawai McNamara Deviations From EPA Methods None Quality Assurance Mike McNamara Testing procedure and ample recovery techniques were according to those outlined in the Federal Register and the Quality A urance Handbook for Air PoLlution Mea urement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VI in Appendix A have more detailed information. North Yellow Cake Scrubber Yellow Cake Dryer Run # Baghouse Process Data 1 2 AVE pCi/dscf 1.419E+02 1.042E+02 1.230E+02 pCi/hr pCi/dscf pCilhr 1.143E +07 8.224E+Ol 1.050E+07 6.951E+06 9.190E+06 8.224E+Ol 1.050E+07 The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test filters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for the Yell ow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. Discussion of Errors or Irreeularities None 3 Percent Isok:inetic Sampline Each of the tests were isokinetic within the ± I 0% of l 00% cliterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokinetic sampling poinl by point. Isokinetic values for each test run are presented in Table 11. e fl. Pe cent l North Yellow Cake Run# Scrubber 96 2 99 4 Yellow Cake Dryer Baghouse 98 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse Llp readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Samplin~: Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Samplin2 Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Sample Point 2 3 4 5 6 7 8 Samplin2 Train Description Distance (inches) from Inside Wall 0.58 0.70 1.89 3.49 5.81 12.19 14.51 16.11 17.42 2.34 4.74 11.26 13.66 15.30 To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. 6 The tack analyzers used to conduct Method 1-5/114 are con tructed to meet the pecificati.on outlined in the CFR. The temperatme en ors are K-type thermocouples. Heater vacuum and pi tot line connections have been designed to be interchangeable with all unit used by the tester. A 316 tainle s steel probe liner was used for the tests. Figure 4 in Appendix E i a ketch of the Methods 5/114 ampling train. Sample boxes were prepared forte ting by following the prescribed procedures outlined in Methods 5/114. Sampline and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CPR 60, Appendix A, Methods 5/114. Qualitv Assurance All equipment et-up, sampling procedures ample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality A ·surance Handbook for Air Pollution Mea urement System . 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Nomenclature Sample Equations A TABLE IV NYC Scrubber COMPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol DescriEtion Dimensions Run#1 Run#2 Date 2/15/11 2/16/11 Filter# 5714 5617 Begin Time Test Began 8:06 7:40 End Time Test Ended 16:17 15:55 Pbm Meter Barometric Pressure In. Hg. Abs 24.50 24.35 ~H Orifice Pressure Drop In. H20 1.288 0.934 y Meter Calibration Y Factor dimensionless 0.993 0.993 Vm Volume Gas Sampled-Meter Conditions cf 355.420 307.159 Tm Avg Meter Temperature "F 97.1 95.4 ...J~p Sq Root Velocity Head Root ln. H20 0.2694 0.2224 Wl:wc Weight Water Collected Grams 855.7 572.3 Tt Duration of Test Minutes 480 480 cp Pi tot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.3805 0.3805 C02 Volume % Carbon Dioxide Percent 3.00 3.00 02 Volume% Oxygen Percent 17.00 16.90 N2 &CO Volume % Nitrogen and Carbon Monoxide Percent 80.00 80.10 Vm,td Volume Gas Sampled (Standard) dscf 274.962 236.648 Vw Volwne Water Vapor scf 40.346 26.984 Bws (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.128 0.102 Bws (saturnted) Fraction H20 in Stack Gas (Saturated) Fraction 0.060 0.055 Bws Fraction H20 in Stack Gas * Fraction 0.060 0.055 xd Fraction of Dry Gas Fraction 0.940 0.945 Md Molecular Wt. Dry Gas lb/lbmol 29.16 29.16 Ms Molecular Wt. Stack Gas lb/lbmol 28.49 28.54 %I Percent Isokinetic Percent 95.5 99.2 AVG Ts Avg Stack Temperature 'F 90.9 88.1 89.5 A. Stack Cross Sectional Area Sq. Ft. 1.767 1.767 Po Stack Static Pressure In. H20 -0.050 -0.050 PbP Sample Port Barometric Pressure In. Hg. Abs 24.43 24.28 Ps Stack Pressure In. Hg. Abs 24.426 24.276 Q. Stack Gas Volumetric Flow Rate (Std) dscfin 1.34E+03 1.11E+03 1.23E+03 Qa Stack Gas Volumetric Flow Rate (Actual) cfin 1.82E+03 l.51E I 03 1.67E+03 v. Velocity of Stack Gas fjlm !.03E+03 8.52E+02 9.43E+02 Curies Radionuclides per sample pCi 39021.0 24649.0 Crad Concentration of Radionuclides pCildscf 141.914 104.159 123.037 ERrad Emission Rate of Radionuelides pCilhr 1.143E+07 6.95!E+06 9.190E+06 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CPR 60, Method 4, Section 12.1.7). Dryer Bagllousa TABLEV COMPLETE RESULTS, PM DENISON MINES CORPORATION YELLOW CAKE DRYER BAGHOUSE Symbol DescriEtion Dimensions Run#l Date Date 2/15/11 Filter# 5715 Begin Time Test 13cgnn 9:23 End Time Test l!ndcd 11:25 Pbm Meter Barometric Pressure ln. lig. Abs 25.50 Llli Orifice Pressure Drop ln. lilO 1.303 y Meter Cnlibrntion Y Factor dimcnsionle.o;s 1.001 Vm Volume Gos S~tmplcd-Mctcr ConditioM cf 91.348 Tm Avg Meter Tcmpcmrurc "F 97.5 ...JM> Sq Root Velocity Head Root ln. H10 0.5056 Wtwc Weight Water Collected Gmms 18.2 Tt Dumtion ofTc~t MiJtutos 120 cjl l'itot l'ubc Coefficient Dimensionless 0.84 Dn NoZ1'1c Din meter Inches 0.2758 C02 Volume % CArbon Dioxide l'crccm 0.00 02 Volume % Oxygen Percent 20.90 N2 &CO Volume% Nltrog>:n and C:ubon Monoxide P~'1"Ccnt 79.10 Vm.td Volume Gns Sru:nplcd (Stnndnrd) dscr 74.085 Vw Volume Wnter Vopc.r scr 0.858 Bw, fn:tetion H10 in Stnck Gos Fraction O.Oil J4 fraction of Dry Gas Fraction 0.989 Md Molecular Wt. Dry Gus lbllbmol 28.84 M. M.olecufllr Wt. Stnck Gns lbllbmol 28.71 %1 Percent lsokinclic Percent 97.6 T. Avg Stock Tcmpcrnturc •r 89.8 A. Stock Cross Sectional Arcn Sq. Ft. 1.396 Pa Stack Static Pressure ln. H10 -0.18 Pbp Sample l'ort B~ramntrlc Pressure ln. Jig, Abs 25.43 P. Stack Pressure ln. Hg. Abs 25.417 Q. Stock Gas Volumetric Flow Rllto (Stl.l) dscfm 2.13E+03 Q. Stnck Gas Volumetric Flow Rate (Actual) clm 2.64E+03 v. Velocity ofStnck Gns l'pm 1.89E+03 Curies Rndionuclides per sample pCI 6093.0 Crad Conccnm11lon ofRndlwutclides pCi/dscf 82.2433 ERrad Emission Role of Radionuclidcs pCi/hr .1.050£+07 %1 = percent isokinetic, percent As= stack cross-sectional area (ft3) ASAP = see ..J t.P M5 Nomenclature Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas C8 = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cr = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) cmetal = concentration of metals (ppm, f.lg/fe, etc.) atomic symbol replaces "metal" C02 = percent carbon dioxide in the stack gas cp = pitot tube coefficient (0.84) Cx (avg) = species symbol replaces x. Cx (corr) = actual gas concentration corrected to required percent 0 2 t.H = orifice pressure drop (inches H20) t.H@ = orifice pressure (inches H20) t.P = stack flow pressure differential (inches H20) Ds = diameter ofthe stack (feet) Dn = nozzle diameter (inches) EA = percent excess air ER8 = emission rate of back half particulate (lb/hr) ERF = emission rate of front half particulate (lblhr) ERmmBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point t.P to determine test point t.H L = length of rectangular stack (inches) mBtu = thousand Btu Mct = molecular weight of stack gas, dry basis (lb/lb-mol) MF = mass of particulate on filter (mg) MFr = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mr = mass of particulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmol) N2 = percent nitrogen in the stack gas 0 2 = percent oxygen in the stack gas ..Jt.P = average of the square roots of t.P (may also be referred to as ASt.P) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) PbP = absolute barometric pressure at the sample location (inches Hg) PG = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) 8 = time of test (minutes) Q. = stack gas volumetric flow rate (acfm) Os = stack gas volumetric flow rate ( dscfm) Ow= wet stack gas std. volumetric flow ere /min, wscfm) Ts = stack temperature (°F) Tstd = absolute temperature at standard conditions (528°R) Tt = see 8 M5 Nomenclature Um = mean molecular speed (cm/s) Vm = sample volume (n3) at meter conditions Vmstd = volume standard (dsct), sample volume adjusted to 68°F and 29.92 inches Hg. Vs = velocity of stack gas (fpm) v w.: = volume water vapor (set) at 68"F and 29.92 inches Hg. W = Width of rectangular stack (inches) Wtwc = weight of the condensed water collected (grams) xd = fraction of dry gas Y = meter calibration Y -factor (dimensionless) Method 5 %1 = Vffisrd • (Ts .J 460) • 1039 / (9 • V5 • Ps • Xd • D/) As = (Ds2 I 4) • rr Bws = Vw I (Vm,1d +V w) C6 = M13 • 0.01543 1 Vmsrd Cr= Mrp • 0.01543 I Yrnsrd C,v ccurrl = Cx cavtll • (20.9 -desired %02) I (20.9 -actual %02) Deq = 2 • L • W I (L + W) Dndes = ..J{0.0269 • (Pbm + 0.0735) I [(Tm + 460) • Cp • Xd • ..J[(Ts + 460) • M,) I (P5 • L\P)]} EA = (%02 -0.5 %CO) I [0.264 %N2 -(%02 -0.5 %CO)] ERe = Cu • Os • 0.00857 ERr= Cr • Os • 0.00857 ERmmBru = ERx I (mmBlu I hr) 4 2 2 K-facl = 846.72 • Dn • 6H® • C1, • Xd • Md • P5 • (T m + 460) I [M5 • (Ts + 460) • (Pbrn + 611 I 13.6)] Md = C02 • 0.44 + 0 2 • 0.32 + N2 •0.28 Ms = (Md • XJ + (18 • B,-s) Ps= Php +{PGI 13.6) Qa= Vs•As Os = Qa • Xd • Ps • T3rd I [(Ts + 460) • P Sid] Ow= Os/Xd Vmstd = Vm • Y • T!td • (Pbm + Lili I 13.6) I (P~1d • (T01 + 460)] Y8 = 85.49 • 60 • Cp • "tJ.'> • ..J [(Ts + 460) I (Ps • M5)] Ywc = Wlwc • 0.04715 Xd= I -Bws APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Denison Mines Stack ldentification North Yellow Cake Scrubber Date r B;uometric Pressure Pbrn in Hg Pbn in Hg N 80 Static Pressure (P 0) in H20 Estimated Moisture (Bw,) % Sample Height from Ground feet A Comments: Stack Dia. 18 Reference: 0 Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbonce Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F I 3.2 0.58 0.58 2 10.5 1.89 1.89 3 19.4 3.49 3.49 4 32.3 5.81 5.81 5 67.7 12.19 12.19 6 80.6 14.51 14.51 7 89.5 16.11 16.11 8 96.8 17.42 17.42 Averages: Ts L.Fiow ---- 1'\P ..JL'l.P -------- KEY=> t'\P L.Fiowl Field Data Sheet ~TETCO (_ Filter ~Jj.., le Box __ _:_ __ _ Plant: Deniso~~nes Date. 1, \\) , ( ' I' Location: North Yellowcake Dryer Scrubber Op<!rator. 0:/\ r\ T111vcrsc Time lf---~-H-i-clo_;_H,O.:_I ~I Vacuum lf----,--T_e-r'mp'-er_att_tre,s ',.,., ----r----11-..;;;..DG~M.:...:T-r•m=p~(T,""-") '"' "''" Desired Actual '"' "•' Stack (T,) Probe Pcobo Ou• Filter Effluent Out In DGM Poont Clock Min (0) Totai Average Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate {tetmin) DGM After Leak Check Yac ("Hg) (9 -tv . oo~ (, 10. "L-(0~ "',f(. Page _.L_of_~ Run #_\_ i ·O N A Pon Reference _ 0.0" _ Assumed Moisture 4-13 % Probe Z.. 1--~ Cp 0.84 Nozzle Calibration "7 (" I C / ~ $& () ~ 3_l7_ A~,n.X"'~ Gas Bag -o ~ Console___;~-'~: Y-factor , ~ J t>H@ 1 . (. r:)(n H2o Barometric Pret.;;ks~O Pbm ~ __ inHg Pb., ·1z.J,: 1~ inHg 2."{.'1) Pc;-~ 0 _s-in H;O c).O . -z..S" Water Collected _____ & Time Sampled ---r-f1-::1----m"' Review Zq K= K= Rate (tetmin) _L Field Data Sheet Plant DenisoJ Minep Date Z. 1 ~ J t I Trsvers= Po1nt ~1 u.- Jo ~~ ~ rJtr rs- .50 '{~ (, a<:;) 11"'. ro '{ ,o J e, l..(r- T 6o !~ '30 '-Is- 1 2 2 3 3 4 4 5 5 6 6 7 7 8 8 Total Time Clock Min (0) 12: I 'i" 240 255 270 285 300 315 330 345 360 375 390 405 420 435 450 465 480 DGM .{I:· <., JO. 'l''f't (D~J • n-v- &1'?-~t.~ ~.;!,5 -:}I u ·41 z.. "1 t/>Q • w I¥' -:: ~~ ".ILS"" 'flJ' f..(a(,¥, ~ ·0~~ ~ Jll,;(J(IIfJ 1-f7.!ov j.q~ ./~'1 ~01:>"·?..-$') <6 1t?. ~()t,- !&2~0) '63t;. '1A \ fs'SO·tfiD rrct.~ 11 1 1s-:vo'1 -,~ r '-'\tv ~!1 • 6P ~H (mH70l tWiH;OJ Desired Actual -016~ '·'{'i !·._(, .Qi'~ l:Ao)j l·'i., · u11) 1-~t. )-~z, 'D 1:5 J·<;~ I . '1-t..- "'-~t-I·D"! 1·&'1 . o'i z.., \ •'-\,w \. '-1.11 .o'S" I· ~Z.. } -~Z . 01"':> I· )l> 1·70 .o sS' t.uz. (·()(... .05"7 l·u't 1-u'tf ·obf' 1·1.--\ !·"tv \ . ol9S" /-W l· vc ·o~o \ . \' I· I\ ·o--¥7 I·'>~ II-t,'1 -l)(,s-l.h) I·'UD O~.:; l• \I H\ ~~~~ ...{(,t? TETCO (_ Filter~ Sample Box __ Vacuum Temperatures C'rl fmli&J Stack (T,) Probe Probe Out Filter Effluent -z, "10 1..,.,S'V 'V ,.., l 'Z.-7D 'PZ-; ~-tql '2[,) 2-Yt 'L)) $'l1 £., <ofJ "2.,.(,~ 'Z.4 > 'Z.")'i ~( ~ [.,; -iY' l.,';(, 'L5'l. "'Z..y~_ s+ !,.. ~1.1 2(,~ zs~ 'l>J.,."'' s<6 '1 Ott) 1}Jf; ~,-c., ts~ lA () ~ 'io -tr "t-5'1 t.ss-~1,.... '.7 "1,... {;'f.l t'-{1 'J..t..f!. 5). s ,1, '7,)'1 '7,..t<( z~t. s-3 '> O,f 1.. 40 l'i~ 7. ~c, S-7, l ql 1..':i. 'U;'Z. 'V-\<t ~ ltJ C\1 t.>) 1. f;"f_ ly~ ::;-1.. 0 '1~ ~'-'' z..sv -z_.) _) G'Y u c; '1' '2-~t' --z.,S-"1. ~5"i [p0 C/, a t-1A.P'I '[.(il.-'lS'J {p6 y c;v "Z. l9'1 Z.u~.> ~~I (g -v L jO~ f -/ . 'l. (J11 \.t.-~~ 9c-~ Average Additional (Extra) Leak Check lnfonnation DGM before Leak Check Vac ("Hg) Rate (te/min) DGM After Leak.fheck G 1-o · -vc.y ~ -q.c _ ·r ., 1 DGM T •mp (T,.) Out In C,<f &7t.. t!cl{ ~Y' c:>t'J e;,y '\I qq -13 161 """' ~4 "1(., to> cr~ I" "S "'" /0) ~I. I I) 'C. ~1-I ~~...J ~~ l 01:.1 qq I o ltJ !oC tor l () \ J D"J 10" tiD ~ i- Vac ("Hg) Page_C_of C Run#J _ i N A Stack Diameter 18"_ Port Reference 0.0"_ Ports are Ports are 9.5' Upstream from next disturbance 9,5' Downstream from last disturbance Assumed Moisture 4-13 % Probe Z "1-b Cp 0.84 Nozzle Calibration · 3 ~0 · J}-o · 3H , 3 So-f Avg D., . ~ ~C>S;~ -- Gas Bag C-t'Sb Console (.p Y-Factor • '-\ "t '3 6Hi!l I · ~ :>ifih..r,o Leak Check ftJ/nun vac in Jig P1tot R3te lnH,O Barometric Pressures Pb., Z... '-t · ~D in Hg Pb, _'Z "f • .. "~in Hg Pu_.=. • 0' 5 in H20 Pre 005! O~bV . 00 5" -t't-I~ o.o J· 0 ·1..,.s-• "!.. ..5 Water Collected 8~S • ':r Time Sampled il\~y-o Review K~ @Tm K= @Tm Rate (ft3/min) g min _5 _Field Data Sheet Plant: DeniSOij Mines Date ?.. \ \v [ L I Traver31:! Time DGM b.P b.H (in H,OJ Po1nt Clock Min (e) (f!)) lt11H10) Desired Actual 1 :t:L/,D 0 ~s l.\o\ -r:H,6 -13 ·1') 1 15 "s-~.4'10 -0'1) -~/) -~V 2 30 Cis'~ • .£'~ 1 ·0§ ~~~ • <6 3- 2 45 bT1-. <-1 1 ) ·0'-f> -~v -~q ____l._ 60 1<6 (p(o . ; 35"" -D~ u -1-'-1 -1'"1 3 75 '('ft./.~ ¥Y ·Oi) . i' 0 ·<(() 4 90 c; D7-~ '}\ •()'-{~ -~0 ·&-{) 4 105 9 /~6~ . av.; -~'\ ·y'i 5 120 "'11-l.:'Jc.S ·oYt -~'\ -yC, 5 135 q;,t."'f!O ·o'-fs -$-~ ·9-5' 6 150 V!I.{O.lJL[~ -f)S) I · 11•1 i .o-f 6 165 t1 s-o.;t. D ;-0~ ),ovj \ ... o/l 7 180 q[#u.~· '\ -05"} J •60 f ·oO 7 195 lt;+o_t'V'6 ,0.5'7 , . .,{) I·P t) 8 210 q<(O -L~ . 11ti5' ! ·o"f I -o v! 8 225 qt?-0 . '5' ~., --o5"+ J.b t-t. 0 1-'-- 11: <-fo 240 I 0" D . G'£1 I I'{ '1 . 1,--'lb Total Average Additional (Extra} Leak Check Information OGM before Leak Check Vac ("Hg) t 6DD· >-'1 r t TETCO Filter S"'b I . Sample Box__f-__ _ rt.t?i ___ _ Location: NortlfYellowcake Dryer Scrubber ~ :t» \ Operator: _ _,1'---+------- Vacuum Temperatures c~> {inHQ) Stack (T,) Probe Probi:!Out Filter Eftluent '{./ ~5' 'L ~6 t"J"':}-1.)"V '1)' v ~(o &'-{"\ 'Z-4.{ '2--1..> Yt 1/ ~(p 1.-'1:.> 2-"{f t.t.il ~<i -I/ ~1--z~ "l--'1_~ 1J-(_j 5t "'Z/ ~(( Z. "\I 1.5'1 tll'"'\ 61) "'V ~q 1-?'i t. 35-~5) Gt ~-a1 ~Z-'1 -zso zc..,l~ ~-z._ ~ 9f({ ~-v"' Zl<~ t---1$ ~~ '--\ 55J -z,;c z·-n-Z'i) $), l7 ~t-·J).J5 7('~ tY.Y ~'1 c;-l6-<=t t-tf r 2,5\ z,--t5 S3. 5' cgvt 1/f-r "' '-l '1 Z..,'-{~ S'\ ~ ~<j ~lJ 7 u-o. ~\.{~ 5V (., <6~ '2--~) 'Z-5~ 1.-{ ~ 5'3 l/J -6-<6' zt? Zs;-v t:-11 so -r ~~ t.L\l-\ ~~0 1..« .. , 5'"D Rate rretmin) DGM After Leak Check I Cal, 005- DGM Temp (T mJ Out In {,I f.t-z, (f{p --rt 1'tl <is'O -1-Y <:$<-/ ~"Zt ~'f ~s-C?D $1 ~I 'b-Y ')1- '?o 15"" qj ~~ qJ '1(, q) '1~ ct·c.j ,:11 q~ lo/ ')<} tv I 6j1 to3 Vac ("Hg) Page _\_of_ ?::.... Run ;i .j2. i N A Stack Diameter 18" Port Reference _0,0"_ Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-1 3 % Probe 2 1--G Cp 0.84 Nozzle Calibration -3~0 -3~0 .3.Y( 3~1 Avg D" '3 }=().)-inches ---·e-Gas Bag {;; -C> J Console (p Y-Factor j "rJ 6H@ { (,Gl--inH,O Barometric Pressur..s Pb., l c..i. } $" _in Hg Pb 2 .... , . 2. ~ in Hg .-!'TJ Pc,; • S __ inH10 Led< C'hoe ~ Post ~_) i111min 0 ·0 <3 0 ·0° I >r.nHa 2\ Z: I Pito!Rato \J· 0 0 · D In H20 ,2.t5 , L s Rata (ft3/min) Water Coilected ______ g Time Sampled /\ min Review ~ K= K= --~-Field Data Sheet Plant: Denison Minc:;s Date· Z., i I t.l 1/ Traverse Time DGM I'>P 6H {mH,OJ Pomr Clock Min (8) (L,J.J (\oH,<lJ Desired Actu!U f>O 1 11:rr 240 ~. S"o\ l@.o5 -"'-f -"' "'L IC 1 255 ((.-z..1.) -o5 . tlv( A --{ 3Z> 2 270 z.D ·"\ 5 "{ ,o"-\ q . "i C) ·'1:.0 41)-2 285 ,o.~o~ oc.f'6' ·"tt .q () .-c;. 3 300 L{O-o rl .051) -~~ . ") ~ 15-3 315 L{q.~~s :~sV '1y ·'\) 5>'1 Att>S""" w -CV{) .&-tD ,. 4 330 .() "''S"' 4 345 (t/'1 . 'ZA(i, . o::(l .q }-.c;-1 -or> 5 360 ¥ .o;~ 05''1 1 ·t->"'7 J.b) JS 5 375 <(" 0 2-'l .o()) I .J y f. {tj ~ 6 390 '1" . "t1r \ 'D:J--<f I· l o 1·1 0 -4-S: 6 405 I! D ·1..& ~ . 0.0" [-0~ {. () ..> 0~ 7 420 1 2 O.jf,\ d7S'5 /-o.) { ·o'J lo 7 435 1~·4&'~ -b'5D '"s-.e; c,- ~0 8 450 f,J.O.~oO ·04. ~ -Dtl -c-tl l..i.S" 8 465 jtfq. l t) C( ·O"lY -~d .t:t I IS·~ 480 ,qq. 'J'TU l§r_ t?C. 1 1'-l'j.l.&rD Total Average )oi-. \5'1 ,, 1--l \ ~~ ~-z '1-'6<~ v' , ~ '0~1 , q ·r"'l Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) t Db\_ oo) . TETCO Filter 5b I r Sample Box __ _ Location: North ~llowcake Dryer Scrubber Operator· ,i:L/1 I Va~uum Temperatures <'F: (Jill-iU Stack (T,) Probe Probe Out Filter Effluent "?,-4 Cf -2,1£> u?J tZ~ 5"'1 "7/ ss-T-' t-1-1 L'7"'[ -z-;.> s { 2.--~(p z.~s 1..f·-fb t-'13 5? 3 ~(o 1-=fO 1..~'Z--e.\~ ~..., ~ ~"' ltiO 1.--i.O 1-/(p s·~ 3 ~--r zs-~ 23~ Z'Jl S"lf ? '?!+-~ ~31-'Z'}) ~ '7 ~(Q .Z-0 z;:;. ~~~ §h y tlS' 23D t..~ ~Vf S'"; q Q''l;j U$ ~4 '2. 33 S'""Z- ~5"" tjO "2. (p(.:l ~ \.{ 1 Z.'-tl ;-s, $:. C)o 2. <-t'~ 1M,0 1.)) {;'-f 0 Gj'l/ '2. '1.5 2-3~ z_ ~ l S i L;, qz.,-'Z}{'L---'l-2-'1 lsi ¢'<-/ f.o ~) "21.-{~ "2-'-ti Z,--tZ. 5'3; (p '1'1.--t5(p 1-.W 1.~ t 5"") Rate (tetmin) DGM After Leak Check DGM Temp (T .J Out In eJ '-/ q-z.. '1s-{6 ( 1:]-Ib~ .!1't>' ID ~ '1'f lo5' 70 {d:J to't.-/o fe, Jot. I 0 1-" Jo> Jo:J /o1. to 1- I oz. !o1- !oZ. /o¥ /o"?:> tor I o<.. JoV {bj t nr 1()') 1 o){ Vac ("Hg) Page Z-_of ~ Run#_~ i N A Stack Diameter 18"_ Port Reference _ 0.0"_ Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe 2 1-b Cp 0.84 Nozzle Calibration ·. 3 ~o .3~o .:s~r .3 fl Avg D, • ~ ~oS~hes Gas Bag }:: -o5 Console_v_= Y-Factor .'1 q 3 t>H@ ( • (;S ~ HP BarQrne1r4 Pressures Pb,. .!' ' ~ 0 _in Hg Pb -t,., .z-r-. H . ~---r-'" g P;f" ~ __ inH,o ' Leak Chock: Pre ~ L f fi'/mm ().0 0 T Q • y() l vacin Hg 1. I I <; PitotR.ate (1.'0 Q.'(j !nH:O z~ Z,:)- Water Collected ..,.--7-? 3 :J ~v Time Sampled ~0 Review K= @T"' K= @Tm Rate (ft3/min) g mln Yell ow Cake Dryer Baghouse Prelim 6 pts blank Facility Denison Mines Stack Identification North Yellow Cake Dryer Baghouse Date r Barometric Pressure 8 Pb0 , in Hg PbP in 1-Jg 0 N Static Pressure (PG) inHp A Estimated Moisture (BwJ I % Sample Height from Ground feet Comments : Stac.k Din 16 Referen~e: 0 Ports arc 57" Upstream !'rom next disturhanc~ Ports <ire 468" Downstn~wn from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F I 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11 .26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 Averages: Ts ___ _ L folow ---- L\P ___ _ -.JtlP ----- KEY=> ___ Field Data Sheet Plant: Denisrm Mines nate: '-f ,)z 1 \ Traverse-Time Point Clnck Min (6) 1 l't: 'Z.3 0 2 lO 3 "2:0 4 )0 5 l.ftJ 6 So 1 &o:'l.{ ~0 2 70 3 ~0 4 ~0 5 loO 6 ~ :o u:z.{ l't"C Total " \crnyc . C'om11t:t1W Time q I A.( • I.) ~··~6'. K>l.D6' lO \ ttlo DGM aP it'l''l (iftii,.Ui 11"·001-• 'Z.Z.. l%'"1..'-\{t:. 11.3 \"\o.<-1.~ •'Z.3 l"ilaSZ.) i t~ 2ot."l'1o <H l.l~. 140 I ':I\ z.t.L 1~>3 •'t\ H.<"t. ~'iO '1.o Z'l'-· o1(' •'Zo 2.Lt3.ol{ 1'7.." "Z.Sl 110 • "}..? 2.-f'i.J~) •)O 2{, 7. 35o ' Baghouse 6P 1... \ 2.·~ ~. \ 1:.~ TETCO Filter_ S 11 S Sample Box_Q ..1H t~HPJ V:1cuum Desired Actual (m IIIJJ) l.( '2.-l.l 'Z-:> \,fl \ .(1 3 lol) l.t"") 3 I. '1) •·tt) 'i l·ff l•J{ '+ I·Jl l.)1 4 I·Of L.el 3 t .oL l· t>'t. r; l-.;:,'t. [.~t.. I{ 1.•n l·'i1 '"' ~.of'-1.)2.. l.{ t. {z.. l, )l,. "{ Time Sag house Ll.P 10'.:1(, 3·9 \~;o~ j,, Location: North Y cllowcake Dryer Baghousc Operator M · 1'1 St-.J.~ "'- Temperatures ,~11 Stack (T,) Probe Probe Out Filter Emuent '05 "2.&.~ l.(jV 27~ "''"* fn l.l'\ 2'lk? 2_~" s~ Be (1'0 Z.~!o Vel 57 l3e 2-?C 2.qJ lb.} S7 ~0 7.~1"" 2<t't 2~) 58 ~t Zz) l.I{L l<Gl '-! qf "Z. ~1. z.•-rt C'"-"2.. (§/ '1'0 1_(1 "lt'o '2.f2 scr ~l 2.")1 "l..'·l.j 2. 1't sea 9l '2. "H. -z.">e U8 Coo '~ N:> l<{! '-'.t '-o CtJ Z.o.tl 2'io lbD bO ' ' e~n'"'.S DGM Tomp (T,.J Out In 77 1 1 '3?.. '6<..{ '¥;1 9 1 ~a 7e 1lf ~~<) 'i!.. t o~ C{(, lol '1'7 toe \00 Ito /(Jo llo joe U{ lei tu Pa~e _!____of __ l_ Run#_(_ i B N Stack Diameter 16" Port Reference _0 0"_ Pons are 57" Upstream from next disturbance Ports are 468" Downstream from last disturbance Assumed Moisture _ __..:.__% Prube I~-(.:> Cp 0.84 Nozzle Calibration ., • .,-,z.7(,p .z.1'(.. •l."Tk- Avg D, • -z,{8 inches Oos Llag Ambient Air Console S Y-Factor I· 1:10 l 6H~ l • ~6C.inH,O Barometric Pressures Pbm -z-,... _;) .") in Hg l'b, '2.-l·"f~ in Hg Po -.1e _in H20 Leak Check Pre Post n·'tmin 0 ·00] va;::m Hg 2.\:>60 o.oo'Z. Pi rot ~ate 0• '0 ~.u,o q.o ).D o.o 9.·~ ,.., ~~/(.... Water Collected ______ _ l'Z.O Time Sampled ___ ..:...-=:..:..... __ Review K= K--- ~ @T,,. (<VT ~IT; g mtn North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yell ow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analy i APPENDIXC c North Yellow Cake Dryer Scrubber METHOD 5 Date: Facility: Denison Mine Stack Identification: NYC Scrubber ------- IM.PINGERS IMPlNGERS IMPINGERS ---------------------------------- Final (g) Initial (g) Net (g) Run: I - drop out ' 7f1J '-, Lf13.o ~11...\1 Run: drop out ' Final (g) g1 0 • D Initial (g) l..l11. ~ Net (g) _5~L · Run: drop out ' l Sample Box: lmpinger Number I :3 I 4 I s lnilinl Volume of liquid (l·hO) in impingers, (rnl) I too I 100 I : ' I ' Bt><T. ~ 15c.t.'-{ "Zl.'\ ~l<-l.( St~. :1 {..'(fl.( f.o{/0. ~ lov4~l Z.f06 ·0 r,f. 3 I~ .l 10'0 Total (g) e 5 5 • ";:}- Sample Box: lmpinger Numbet· 2 -I 3 I 4 I 2.. Initial Volume ofliquid (1110) in imping~rs, (ml) Sample Box: lmpinger Number .z_ I 3 I 4 I 5 Initial Volume ofliquid (1-110) in impingers, (ml) I too I 1oo I 6 Silica Gel . 859.~ <.'H •. (; I ~3.0 (_ 6 Silica Gel 6 Silica Gel Final (g) -------r------+------;-------r------+------- Initial (g) _____ _,_ ______ +-------11------r----1------- Net (g) ====================================±======= Total (g) ======= IMPINGERS Run: Sample Box: Impmger Number ..L ..t. I 3 I 4 I s 6 lulunl Volume of liquid (H10) in impingcrs, (ml) drop out I 1oo I 1oo I Silica Gel I Final (g) -------+-----+-------1-------r-----+------ lnitial (g) ------+------1--------1------r------+------ Net (g) ======~=================*============ Total (g) ====== 7../ IS/Il Plant--''""V_f_Y!_1-'•7<--C>-fl\ _________ _ !.,u\f( 'Ser-'"" Location __ l_'VI .L/_-_________ _ Analytical Method. __ ..::~:...___ ________ _ Dom 1i:f Test No. Gas Bag No, -6 Ambient Temp -~ Opemtur --J; Date 1../1 ~ ) d Test No. -.....,~..,;;,~_,0_1?,.,. .. ~ Gas Bag No. !;: -2 Ambient Temp -~~Jt-=:O,-­ Operator __ 0.,, -'~'--- Date ----- Test No.----- Gas Bag No.----- Ambient Temp----- Operator ____ _ RUN 2 Ac:cual Net t\ctuat Net Gas Rt:o1ding Read in~ COz 5 ·() ?.o 5.0 5.0 0 2 (Net is Actual 0 2 Reading Minus Actual ~{).b ~-0 ( -:f.cj '?c){\ C02 Reading). N2 (Net is 100 Minus Actual 0 2 Reading). RUN I 2 Actual Net Actual Net Gas Rending Reading C02 3'6 ~·c) 3-o ~-0 0 1 (Net is Actual 0 2 Reading Minus Actual 11·1 16·1 I '1 ·j /6 ·'7 C02 Reading). N2 (Net is 100 Minus ~.z:y; .. ...,'~:' ·~-~~ Actual 0 2 Reading). ~~~ (. ,,._ .. :t.;: ' p RUN 2 Actual Reading AciUal Not Gas 0 1 (Net is Actual 0 2 Reading Minus Actual COl Reading). N2 (Net is 100 Minus Actual 0 2 Reading). Reading • 0 1 was dctcm1ined using a gas analyzer CO is not measl!red, as it has the same molecular weight as N2 3 Actu•l Net Reading ?.c ~() -zo·ll t1.o 3 ActuaJ Net Rending .S·o $.C) } c;. J I&·[ • 3 Actu•l Nel Readiug Average Net Volume ~-0 ' 'f.(j Average Net Volume J-u U·j A\•erage Net Volume Yell ow Cake Dryer Baghouse NYC Baghouse M5 Facility: Denison Mines Date: L(l ( // { Stack Identification: ..:.N.;...Y:.....:C::....:::B.::Jag'-h:.::o.=.:us:.:e ____________ _ JMPINGERS IMPINGERS IMPINGERS Final (g) Initial (g) Net (g) Run: Sample Box: lmpinger Number 2 I ..L I 4 I s luitinl Volume of li•]uid (H20) in illl!lin~crs. (ml) 100 100 I I SilicaGd ] ' I 1 ' . < &cr~.'1 (,Cf8 ·z..__ ~ I~{. 1 P)l L .. ) I JO./ (o Of o. 4 t, oc.,. I tJ,~~-~ .. 13.1-l.~ s·. (, tS.o Total (g) Run: Sample Box: lmpmger Number 2 I 3 I 4 I s Initial Volume ofliqmd (Hi)) in impingers, (ml) 100 100 I I SilicaGel I 6 ' 6 Final (g) ------1----.J.----+-----1-----+----- Initial (g) ___ --11-----1----+----1-----1----- Net (g) ============================~======~====== Total (g) ======= Run: Sample Box: lmpinger Number 2 ..L I 4 I s 6 Initial Volume of liquid (H20) in impingcrs, (ml) 100 I 00 ] I Silica Gel I Final (g) -----11-------1----+----+----1----- lnitial (g) -------11-----1----+----+----+----Net (g) ======~====~====~====~======b====== Total (g) ====== JMPINGERS Run: Sample Box: lmpinger Number ...!_ 2 3 I 4 I s 6 Initi~l Volume of liquid (lllO) in impingcrs, (ml) I 00 I 00 I I Silica Gel I Final (g)----.---11-----1----+----+----+---- Initial (g) ------11--------1-----+----+----1-----Net (g) ======~====~=====k====~======~===== Total (g) ======= Chain of Custody Record ~ CJtfJnr Tetco Address 391 East 620 South Cfty American Fork I ~~e 1z::~~3 F'l'tMCI Nt!me and Llr.sdon IStat!<) Denison Mine 20111st Quarter Conlmct/Purc/la~ Omel'fOul>lc No. --Sample J.D. No. and DescriptiOn Date (Con~alrlers fer eacn samp/9 may b~ comblneti on one line) Rl Baghouse filter 15715) and beaker 2/15/2011 -Rl NYC filters t5714,5716) and beaker 2/15/2011 R2 NYC filters (5717.5718) and beaker 2/16/2011 . .. --··---- POSSiblo HazuirJ fqc<rlffica5on D Non·Hezarri 0 Flflf11mebftl D SKin Irritant D Poiocn D Thrn ArtW!ld Tlme Rr;qulre<l 0 24Hcurs 2. 2. Rs!Jr.auislled By ecmn:9flts Temperature on Re"...e/pt __ _ Test America Drinking water? YesO NoD THE LEADER IN ENVIRONMENTAL TESTING PtC/u;ll'll!wlaer-'Dale Cbalrt of CW>!Odv /'Jumbe; Dean Kitchen 2/18/2011 oOill(>hono Numb6t tAtea Co:zG)/F:JX /'lwr"l'..cr L.o.b Numb~tr 801-492-9106 Page o[ ·-Sire Ccntact Lai>CW/tar:r Analysis (Artach lisl If Scott ctnisten$en,Ryan Palmer mora spac& Is nssded) CHniettWaybi!l Nuw!Jer Speclaf /nstruct/ons/ I Containers & Conditions of Receipt Matrix 0 Pre9ervstives c "' ... iO m ... N .,; l ~~ l ~ ~ ':' N s ~ § ~~ ..... ,;, .. Time j l )_ :::> p:; "' ~ I ~ :l1 ....:.! r----1 r-·-· 1...:::.. --' ! I 1o:oo X X ----,... -I 1 s:oo X X 8:00 X X I r I I I l ' I ! ! : l ' I I l I ' I i I I l ! I 1 I I --- t.wp..! Urspa..~ D.u~ D.B.ruun.ra Client 0 Di$J]08818y Lab 0 Archille For ___ Mo.'llhs (A fee may be os:;essed if ~e!J ere; rer11ined A ,., QC P.Q4111rcmsr.ts {Spedly) 3.~ed8y I longer thaJt 1 J71Cf)lh) ODto ifuno I OaJp lnme When Complete Email to: Dean or Paul tetco@tetco-ut.com DiSTRiBUTION: WHITE· P.JJtvmud tr; ~~ .. .;~~: ~P 4' CAI\!ARY-S.:.ys wiln tr.e ~,PI!J; PINK· P.okt 0;,py SDGNo. Order No. 42802 TestAmerica rptSTLRchTitle v3.73 TestAmerica Laboratories, Inc. Analytical Data Package Prepared For Denison Mines (USA) Corp. Denison Mine 20111st Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 14 Pages Report No.: 46110 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID R1 BAGHOUSE FILTER J1 8240526-1 METXG1AA 9METXG10 (5715) & BE R1 NYC FILTERS J1 8240526-2 METXV1AA 9METXV10 (5714,5716) & B R2 NYC FILTERS J1 8240526-3 METX21AA 9METX210 (5717,5718) & B Batch No. 1055400 1055400 1055400 Test America THE LEADER IN ENVIRONMENTAL TESTING Certificate of Analysis March 31, 2011 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction February 22, 2011 Denison Mine 2011 1st Quarter Three (3) Stack Filter Samples 42802 CASE NARRATIVE On February 22, 2011, three stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J1B240526. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: Alpha Spectroscopy Uranium-234, -235, -238 by method RL-ALP-004 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. TestAmerica Laboratories, Inc. 2 Denison Mine (USA) Corp March 3 I 20 L1 V. Comments Alpha Spectroscopy Uranium-234, 235. 238 The LC recovery yield ex.ceeds acceptance criteria. The LCS was recounted and is now within acceptance limits. The achieved MDA ofth batch exceeds the detection limit from reduced aliquot sizes taken due to hi torical proces knowledge. The sample activity exceeds the MDA and detection limit for the ample · and the batch blank activity is below lbe sample and the LC . Data i ac epted. Ex.cept a noted the LCS batch blank, sample and sample duplicate result are within acceptance limits. 1 certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC both technically and for completene , for other than lhe conditions detailed above. The Laborato1y Manager or a de ignee, a verified by lhe following igllalure ha authorized release of the data contained in thi hard copy data package. Reviewed and approved: Erika Jordan Customer Service Manager Te lAmerica Laboratories, Inc. 3 Referenced Method EPA 901.1 EPA 900.0 EPA 00-02 EPA 903.0 EPA 903.1 EPA 904.0 EPA 905.0 ASTM D5174 EPA 906.0 Drinking Water Method Cross References I DRINKING WATER ASTM METHOD CROSS REFERENCES lsotope(s) TestAmerica Richland's SOP N Cs-134, 1-131 RL-GAM-001 Alpha & Beta RL-GPC-001 Gross Alpha (Coprecipitation) RL-GPC-002 Total Alpha Radium (Ra-226) RL-RA-002 Ra-226 RL-RA-001 Ra-228 RL-RA-001 Sr-89/90 RL-GPC-003 Uranium RL-KPA-003 Tritium RL-LSC-005 Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S/?n), where Sis the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation of the general "Law of Propagation of Errors" equations and specific example are available on request. ------------------- TestAmerica rptGenerallnfo v3. 72 TestAmerica Laboratories, Inc. 4 o. Action Lev Batch Bias COCNo Count Error (#s) Total Uncert (#s) lie_ Combined Uncertainty. (#s), Coverage Factor CRDL (RL) Lc Lot-Sample No MDCIMDA Primary Detector Ratio U-234/U-238 Rst/MDC Rst/TotUcert Report DB No RER SDG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmerica Report Definitions An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by the equation (Result/Expected)-! as defined by ANSI Nl3.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, ue the combined uncertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width of the confidence interval, I, 2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default" nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 * Sqrt(2*(BkgmdCnt/BkgmdCntMin)/SCntMin)) * (Convfct/(Eff*Yld*Abn*Vol) * Ingrfct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume with a Type I and II error probability of approximately 5%. MDC= ( 4.65 * Sqrt((BkgmdCnt/BkgmdCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn *Vol)* lngrfct). For LSC methods the batch blank is used as a measure of the background variability. The instmment identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is 1.038. Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than l may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order Number. The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd2)) as defined by !CPT BOA where S is the original sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results are in the same units. The LIMS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. rptGenerallnfo v3.72 TestAmerica Laboratories, Inc. 5 Report No. : 46110 Client ld Batch Work Order Parameter 1055400 FFSR R1 BAGHOUSE FILTER (5715) & BE METXG1AA U-234 U-235 U-238 R1 NYC FILTERS (5714,5716) & B METXV1AA U-234 U-235 U-238 R2 NYC FILTERS (5717,5718) & B METX21AA U-234 U-235 U-238 No. of Results: 9 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample ID. Result+-Uncertainty { 2s) Qual Units 2.87E-03 +-5.3E-04 UCI/SA 1.23E-04 +-6.2E-05 UCI/SA 3.10E-03 +-5.7E-04 UCI/SA 1.90E-02 +-3.0E-03 UCI/SA 6.21E-04 +-1.5E-04 UCIISA 1.94E-02 +-3.1E-03 UCIISA 1.23E-02 +-2.0E-03 UCI/SA 3.49E-04 +-1.1 E-04 UCI/SA 1.20E-02 +-2.0E-03 UCI/SA Date: 31-Mar-11 SDG No: 42802 Tracer MDC or Yield MDA CRDL RER2 94% 3.90E-05 9.00E-15 94% 3.15E-05 9.00E-15 94% 3.15E-05 9.00E-15 95% 3.35E-05 9.00E-15 95% 2.70E-05 9.00E-15 95% 4.40E-05 9.00E-15 100% 2.95E-05 9.00E-15 100% 2.38E-05 9.00E-15 100% 2.95E-05 9.00E-15 TestAmerica RER2 -Replicate Error Ratio = (S-D)/Isqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA. rptSTLRchSaSum mary2 V5.2.12 A2002 TestAmerica Laboratories, Inc. 6 Report No.: 46110 Batch Work Order Parameter FFSR 1055400 BLANK QC, MEVA41AA U-234 U-235 U-238 1055400 LCS, MEVA42AC U-234 U-238 No. of Results: 5 QC Results Summary TestAmerica Ordered by Method, Batch No, QC Type,. Result+-Uncertainty ( 2s) Qual Units 7.28E-09 +-1.5E-08 u UCI/SA -5.83E-1 0 +-1.5E-08 u UCI/SA -5.83E-10 +-1.5E-08 u UCI/SA 1.11 E-06 +-2.6E-07 UCI/SA 1.24E-06 +-2.8E-07 UCI/SA TestAmerica Bias -(Result/Expected)-1 as defined by ANSI N13.30. Date: 31-Mar-11 SDG No.: 42802 Tracer LCS Yield Recovery Bias MDCIMDA 93% 2.93E-08 93% 2.93E-08 93% 2.93E-08 72% 113% 0.1 3.83E-08 72% 121% 0.2 4.52E-08 rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit crHeria is less than the Mdc/Mda/Mdl, Total Uocert, CRDL, RDL or mary V5.2.12 not identified by gamma scan software. A2002 TestAmerica Laboratories, Inc. 7 Lab Name: TestAmerica Lot-Sample No.: J1 8240526-1 Client Sample ID: R1 BAGHOUSE FILTER (5715) & BE Denison Mine 2011 1st Quarter FORM I SAMPLE RESULTS SDG: 42802 Report No. : 46110 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Parameter Batch: 1 055400 U-234 U-235 U-238 No. of Results: 3 Qual Error { 2 s) FFSR 2.87E-03 2.8E-04 1.23E-04 5.9E-05 3.10E-03 2.9E-04 Comments: Uncert{ 2 s) Action Lev Lc CRDL{RL) Rst/TotUcert Work Order: METXG1AA Report DB 10: 9METXG10 5.3E-04 3.90E-05 UCI/SA 94% (73.5) 1.02E-05 9.00E-15 (10.8) 6.2E-05 3.15E-05 UCI/SA 94% (3.9) 6.42E-06 9.00E-15 (4.) 5.7E-04 3.15E-05 UCI/SA 94% (98.4) 6.42E-06 9.00E-15 (10.9) Ratio U-234/238 = 0.9 Date: 31-Mar-11 Collection Date: 2/15/2011 10:00:00 AM Received Date: 2/22/2011 10:00:00 AM Matrix: OTHER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 3/30/11 04:48 a 3/30/11 04:48 a 3/30/11 04:48 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00101 Sample 0.00101 Sample 0.00101 Sample Primary Detector ALP213 ALP213 ALP213 TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.12 A2002 TestAmerica Laboratories, Inc. 8 Lab Name: TestAmerica Lot-Sample No.: J1B240526-2 Client Sample ID: R1 NYC FILTERS (5714,5716) & B Denison Mine 2011 1st Quarter FORM I SAMPLE RESULTS SDG: 42802 Report No. : 46110 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Parameter Batch: 1055400 U-234 U-235 U-238 No. of Results: 3 Qual Error ( 2 s) FFSR 1.90E-02 6.4E-04 6.21E-04 1.2E-04 1.94E-02 6.5E-04 Comments: Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Work Order: METXV1AA Report DB ID: 9METXV1 0 3.0E-03 3.35E-05 UCI/SA 95% (566.3) 9.42E-06 9.00E-15 (12.6) 1.5E-04 2.70E-05 UCI/SA 95% (23.) 6.17E-06 9.00E-15 (8.2) 3.1 E-03 4.40E-05 UCI/SA 95% (440.1) 1.47E-05 9.00E-15 (12.6) Ratio U-234/238 = 1.0 Date: 31-Mar-11 Collection Date: 2/15/2011 8:00:00 AM Received Date: 2/22/2011 10:00:00 AM Matrix: OTHER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 3/30/11 04:48 a 3/30/11 04:48 a 3/30/11 04:48 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00115 Sample 0.00115 Sample 0.00115 Sample Primary Detector ALP214 ALP214 ALP214 TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.12 A2002 TestAmerica Laboratories, Inc. 9 Lab Name: TestAmerica Lot-Sample No.: J1B240526-3 Client Sample ID: R2 NYC FILTERS (5717,5718) & B Denison Mine 2011 1st Quarter FORM I SAMPLE RESULTS SDG: 42802 Report No. : 46110 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Parameter Batch: 1 055400 U-234 U-235 U-238 No. of Results: 3 Qual Error ( 2 s) FFSR 1.23E-02 5.4E-04 3.49E-04 9.1 E-05 1.20E-02 5.3E-04 Comments: Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Work Order: METX21AA Report DB ID: 9METX210 2.0E-03 2.95E-05 UCI/SA 100% (415.7) 6.74E-06 9.00E-15 (12.3) 1.1 E-04 2.38E-05 UCI/SA 100% (14.7) 3.89E-06 9.00E-15 (6.6) 2.0E-03 2.95E-05 UCIISA 100% (407.7) 6.74E-06 9.00E-15 (12.3) Ratio U-2341238 = 1.0 Date: 31-Mar-11 Collection Date: 2/16/2011 8:00:00 AM Received Date: 2/22/2011 10:00:00 AM Matrix: OTHER Ordered by Client Sample ID, Batch No. Analysis, Prep Date 3/30/11 04:48 a 3/30/11 04:48 a 3/30/11 04:48 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00116 Sample 0.00116 Sample 0.00116 Sample Primary Detector ALP215 ALP215 ALP215 TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdciMda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.12 A2002 TestAmerica Laboratories, Inc. 10 Lab Name: TestAmerica Matrix: OTHER Count Total Parameter Result Qual Error ( 2 s) Uncert( 2 s) Batch: 1055400 FFSR Work Order: U-234 7.28E-09 u 1.5E-08 1.5E-08 U-235 -5.83E-10 u 1.5E-08 1.5E-08 U-238 -5.83E-10 u 1.5E-08 1.5E-08 No. of Results: 3 Comments: FORM II BLANK RESULTS MDCIMDA, Rpt Unit, Lc CRDL Yield Rst/MDC, Rst/TotUcert MEVA41AA Report DB ID: MEVA41AB 2.93E-08 UCI/SA 93% 0.25 4.79E-09 9.00E-15 0.99 2.93E-08 UCI/SA 93% -0.02 4.79E-09 9.00E-15 -0.08 2.93E-08 UCI/SA 93% -0.02 4.79E-09 9.00E-15 -0.08 SDG: 42802 Report No.: 46110 Analysis, Total Sa Prep Date Size 3/30/11 04:48 a 1.0 Sample 3/30/11 04:48 a 1.0 Sample 3/30/11 04:48 a 1.0 Sample Ratio U-234/238 = -12.5 MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Date: 31-Mar-11 Aliquot Primary Size Detector 1.0 ALP216 Sample 1.0 ALP216 Sample 1.0 ALP216 Sample TestAmerica rptSTLRchBiank V5.2.12 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 11 Lab Name: TestAmerica Matrix: OTHER Count Total Parameter Result Qual Error ( 2 s) Uncert( 2 s) Batch: 1055400 FFSR Work Order: U-234 1.11 E-06 1.9E-07 2.6E-07 U-238 1.24E-06 2.0E-07 2.8E-07 No. of Results: 2 Comments: TestAmerica Bias -(Result/Expected)-1 as defined by ANSI N13.30. rptSTLRchlcs V5.2.12A2002 TestAmerica Laboratories, Inc. MDCIMDA FORM II LCS RESULTS Report Unit Yield MEVA42AC Report DB ID: 3.83E-08 UCI/SA 72% Rec Limits: 4.52E-08 UCI/SA 72% Rec Limits: 12 Expected Expected Uncert MEVA42CS 9.84E-07 3.05E-08 75 125 1 .03E-06 3.20E-08 75 125 SDG: 42802 Report No. : 4611 0 Recovery, Analysis, Bias Prep Date 113% 3/31/11 04:13 a 0.1 121% 3/31/11 04:13 a 0.2 Date: 31-Mar-11 Aliquot Primary Size Detector 1.0 ALP12 Sample 1.0 ALP12 Sample Chain of Custody Record Temperature on Receipt ---Test America lllllllllllllllllllllllllllllll J1B240526 Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING "!N.-412~ (10071 Clfenr i Project. ManB._Qer Da:e ~LCusJod.I'.IYumb~ Tetco I Dea_n Kitc_hen I l 211st2o11 Mmess[ J seJephone Ny~r {A-Code}/Fax Number UzbNumbf:r 391 East 620 South ' ' 801--492-9106 ' Page of ; Ci1y I American Fork I I_Sia~ ~~~ Site Conracc Lab Contacc Analysis (Attach Jist if Jj_t_ ~ 84003 Stott Christcnsen,Rpn Palmer mors spac9 Is n9ed9d) It f.-, Pro/~ NMic enrJ Lr=liorr fS/atel I CamerJ.Waybill' Number Denison Mine 2011lst Quarter ~ Special InstructionS. C<:Jnuncf/Putcnase OrrJa/fQuoto No. Containers & ei ConamonsotRece~t MatriX Preservatives 0 "' ... -N "' "' M .,:, Gbt:A2 l "' ~ ~ Sample l.D. No. and Desclfptlon ~ !! g ~ ei ~5 z :I:; .. "' Time :::. ., Date -g 15 1 ! ~ H "' --' (Co.~~rs for each samp/9 may ba combinsrf on aneline) i _, i!-~ ~ ::!! "' "" "' ">I -- _ l_z(1Sf Z011 ; ! I _) ~ 10 7 !)' K._...; I t. J =Z:~~ _-(_Jf~ Rl Baghouse filter (5715) and beaker 10:00 X X ___j '--· .. _, r -l &:OO : I ~ ~ 1£ f1 IX \ V' ( r~ ):5I' .i/fJ , R1 NYC filters 15714,5716) and beaker ! 2./15/2011 ---' X: I J ) I RZ 1 2./16/2.011 ' l7 I I l I I ·A r1 It:, r7 v..,.. 1/~.. ,-''Pj)tt/7_-·_'<.-2 NYC filters (5717,5718) and beaker 8:00 I X .)( I I I! lr==J I I I L I r I ! I I I I I L_ ..... ,_ . I I' J I I I ! -I. I r II . It ! I ! I I i I I I Possible HllZ.Illd ldstlJifiClltion I SlllllPI<! ()fspaSBI (A fee may be assessed if samples are millirltld 0 Non-H<rzarr:i D Flammabl" 0 Skin Irrill1nl D PoisonS 0 Unkrlovm 0 Retum To Client 0 DlsposaiByLab 0 Archive For ___ MoTllhs /Mgor th:m 1 mJnlh) -oum Around Time Rsqulred 0 24Hours 0 14Days 0 21 Days Time /0/l??"l.., T/mo 3. R<1(11lqulshed By 1 Time Commsms When Complete Email to: Dean or Paul tetco@tetco-ut.com DISTRIBUTION; WHITE-Returned to Cfietrl wiUr Report; CANARY-Stays with tile Sample; FINK-Aefrl Copy TestAmerica ~ -nE Li:.ADER !N ~NYIROI"-11-.AENTAL Ti:.SIING Sample Check-in List Drne!Tllnofu>oeivod' ..2 • 22-.;:1:1 ~...20A'2f' GM Sc.o,nR'""' (om) _ ___,,~·'(?~-(U:) t ~ Jnitic.lll(lb Client: :V-erv ~DG~: ~802-!\A[] SA.F;';': ________ !.\A[j -\-:,:o::k Order :!\i.:.;:!be~ -;::;t::.:::z6ZYQ S 2.6:f~o ::,f C'.lS~::Jc:,: == ----------- Shipp~g Container ID: ~ . .o.ir Bill;';' ---------------->6j Iten 1 drrougD. S for ship?iDg com2.iner only. l:J.itiai Eppropriae :espoz.se. l. 2. Custody Sec.ls cllited and signed? Chain of Cuswdy resod present~ 4. Cooler te:mpe:ram::e: ____ K.~ \'esi()J No [ \'es1) ] ~o [ ~"io Cuswdy Se2.l L 5.Ve:.:niculi1e1packmg maeri<:.l.5 is 2':A [ hem 6 ;:h;ough 10 for sampies. Ini1ial 2-ppropr-ia.te response. 6. 7. 8. 9. 10. 11. 12. Number of samples in shipping container (Each sample m<:.y contain multiple bottles): Sample holding times exceeded? ~leshe.ve: ~tape __ custody seals NA[ ] Yes [ hazard labels .L§wropnate sample labels 3 V 2 C6J1&~tPJ ] No.vtj jYL{ ~-/'~. III/IIIII/ 111111111111111111111 J1t3240526 S~les: (if:;/ L A • ) ~are .in. good condition ,; 'fVtJ __ are leaking __ are broken ~ __ have air bubbles (Only for samples requiring no head space) Sample pH appropriate for analysis requested Yes [ ] No [ ] N/A rA1 (Note discrepancies in #13) (If acidification necessary, then document sample ID, initial pH, ~~t ofHN03 added and pH after addition) RPL ID #of preservative used : _______________________________ _ Sample Location, Sample Collector Listed? * *For documentation only. No conective action needed. ~No[] Were any anomalies identified in sample receipt? Yes[] N~ 13. Description of anomalies (include sample numbers): NA [ ], _____________________ _ Client Informed on. _________ by __________ Person contacted. __________ _ [~No action necessary; process as is Project Manager 2~.9. , q {J'tdf)~ Date,--=~:._-_1_,=--L..!....{ ~( / _____ _ TestAmerica h~bQM:o¥re'S·, irtc.l 0/10 14 APPENDIX D North Yellow Cake Scrubber Figure I. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Process Data (Retained by Denison Mines) D Faoility Denison Mines t y stackidentification: North Yellow Cake Scrubber a: Distance upstream from next disturbance, feet 9.5' ----------------- ~: Distance downstream from last disturbance, feet 9.5' 65' y: Distance of Sample Level to Ground, feet ______ :..:... _____ _ 0: Stack Inside Diameter, inches 18" -------------- Estimated Moisture, percent 8-15% 100-120 Estimated Temperature, °F ___ __:..:....:......;;.;;;.:. __ _ 1100 Estimated Velocity, :tpm -----~;;..;;,.,;;_ ___ _ Control Unit Type: Scrubber Number of Ports 2 Figure I. Facility Schematic Representation Process Type: Yell ow Cake Processing Focility Denison Mines t y stack Identification: Baghouse a: Distance upstream from next disturbance, inches 57" ----------------- !3: Distance downstream from last disturbance, inches 454" y: Distance of Sample Level to Ground, feet _______ 6_5_' ______ _ 0: Stack Inside Diameter, inches 16" ----------------- Estimated Moisture, percent 0-2% Estimated Temperature, "F 125 ----------------- Estimated Velocity, tpm ____ l .... 4_0_0 __ _ Control Unit Type: Baghouse Number of Ports 2 Fi e 2. Facili Schematic Representation Process Type: Yell ow Cake Processing Denison Mine Process Data J I Source: Nmih Yellow Cake Date: Z-l ,,~/i( Scrubber Flow GPM Time #1 #2 L\P ~-,' DD c::1 ~ \ Ll · I ~ r ::.}- ~.·st.) s~ i L\. \ -~I '1 CJ 00 ~ ~-1 ,~. { ).cd "} . -~ i) q ,( \>· ~ ;.(, IV -D D c, ' ( I~-(... ~-·s (()· ~() 01-t-\ ~-&, )·~ {I: 6C> q.t_ /")•~ '~-0 11 . ~ /) "t '._j t).y '7' t, t-z :OO v\. sr r?·1 ~·~ (l! )V Oj.s-tY -0 ?· (, r ) ~ () /) Ct·) (4' \ ·-:1 ~ :)· \ 7: 31.) c,. ~ ~ ~t I I '-"" ~.G, t'-(v oD ?\·? I'-(· 0 S·Ct, IY• ~D ~·tf ( 31-~·~ 1>: t)D 0 -~ . ? 13·~ .? . s.-- ( ~-~ "?0 0 · ·z._ I). 1 ).G, j{p'. (.JD 'f1'. \ t~· ~ -~.~ I&: 'Jl) Oj.( { ~.) s· ~ D ·son Mines Process Data em f:~ .. ~] ·-(. I f Source: North Yellow Cake Date: Z ~~ II Scrubber Flow GPM Time #1 #2 ~p r "5 () £1.) l ~· y ~· ~ ~>:, (.) t) ~-1 ( <;. 1-).3 l"; ?V c?j.L) I)· & )·) '1~oi> ~-'1 l~·'Z. ~·> C4: '?o '1 ·7 ~~.q 3. z. tt.J ~o D c;1' s \~.0 7 ·Z: to:>o c1 (, ;Yt0 )·1 11 :a 0 ~-1-,_J •• ~ ~.) \ c ·.jo Cl·--:1_ tU· 3 5·' tz:oa q.Co t l-~ . r -;. ~ l'l~ }0 ?t· s l L.( ' 0 '$. '1j t ): D o tf-5 lY-0 ~·3 l-"?: 3(.) Cj. (t 1 J f I '>r z_.. r1;1.)c> t1·(p lt1 ' ( ~. -z. IL-l·. Jo CJ.& t ' ( • \ ~·Z.. l )' ()0 C,. ')' L L~ I \ ~·I I ( J D 0·~ \ l..\ r -z_ ~· \ / G : uo £1.-:f JY·--s 1·Z f(;: ·;D APPENDIX£ Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the flfst page of the field data sheets. Figure 3 Schematic of Method 5/ I 14 Sampling Train Meter Box CaJibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms TypeS Pitot Tube Inspection Data Sample Box Temperature Sensor Calibrati on E Temperature Sensor ' ~Probe TypeS Pitot Tube GooseneckTe~~~~~t~~re Nozzle t-W Tra:.ed ~ ~ / ~ TypeS Pitot Tube Temperature Sensor Glass Filter Holder Hea.ted Area lmpingerTrain Optional, May Be Replaced SJ An Et;.uivalent Conilenser l Temperature Sensor ,-------------- lmpingers Stack Wall Manometer Orifice Dry Gas Meter Air-Tight Pump Figure 3 Schematic of Method 51114 Sampling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL#: 1-....;;.;==---; CRITICAL ORIFICE SET SERIAL#: L--__;_=:.._....1 EQUIPMENT ID #: K' RUN# (AVG) 2 3 2 3 2 3 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 TESTED (In Hg) 12 155.004 12 161.521 12 168.043 13 136.700 13 142.672 13 148.297 13 116.20 13 125.809 13 131.075 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 161.521 168.043 174.568 142.672 148.297 153.926 125.809 131.075 136.357 6.517 6.522 6.525 5.972 5.625 5.629 9.609 5.266 5.282 74 82 74 83 74 83 74 81 74 80 74 81 74 76 74 78 74 80 83 89 83 93 83 96 80 84 81 86 82 88 78 77 80 80 81 81 93 96 99 86 88 89 80 81 84 DGM AVG 86.75 88.75 90.25 82.75 83.75 85.00 77.75 79.75 81.50 FINAL 25.10 ELAPSED 6.00 6.00 6.00 22.00 12.00 12.00 AVG(P,.) 25.10 ~ 4.5978 4.5905 ~ 4.3273 4.3264 2011 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED l 5.3045 !!.i!l 5.3045 !J!!!l! 5.3045 1.002 AVG= !J!!!l! 4.9104 1.004 4.6215 1.005 4.6215 1.007 AVG= ~ 7.9047 0.997 ~ 0,996 4.3117 0.997 AVG= 0.997 1.532 1.529 1.526 !,ill 1.432 !,ill The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical orifice, Va (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.001 (1) (2) (3) V: K V: Pbar + (llH /13.6) m(std) = I* m• Tm Pbar *E> Vcr<.~rdl = K'* ~ ~Tamb = Net volume of gas sample passed through DGM, corrected to standard conditions K1 = 17.64 'Riin. Hg (English), 0.3858 'Kimm Hg (Metric) T m = Absolute DGM avg. temperature ('R-English, 'K-Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T...., = Absolute ambient temperature ('R-English,"'<-Metric) y = Vcr1,dl Vm(srd) K' = Average K' factor from Critical Orifice Calibration = DGM calibration factor AVERAGE AH@ =J 1.485 Temperature Sensors Reference In Out OF 32 72 203 "F 32 73 201 "F 32 73 202 Pre 2011 5 console METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL#:~ CRITICAL ORIFICE SET SERIAL#:~ EQUIPMENT ID #: K' TESTED .------r---1 FACTOR VACUUM RUN# 2 3 2 3 2 3 (AVG) (In Hg) 0.8137 13 0.8137 13 0.8137 13 0.5317 12 0.5311 12 0.5317 12 0.3307 12 0.3307 12 0.3307 12 443.725 449.104 454.492 460.802 466.60 471.872 477.70 482.955 488.227 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 449.104 454.492 459.885 466.60 471.872 477.157 482.955 488.227 493.613 5.379 5.388 5.393 5.798 5.272 5.285 5.255 5.272 5.386 71 73 71 79 71 82 72 78 72 80 72 81 72 78 72 79 72 82 79 73 82 73 85 73 80 75 81 75 81 75 79 76 82 77 82 78 73 73 74 75 75 76 77 78 80 DGM AVG 74.5 76.75 78.5 77.00 77.75 78.25 77.50 79.00 80.50 FINAL AVG (P..,) 25.20 25.20 ELAPSED TJME(MIN) e 12.00 12.00 12.25 1.20 1.20 1.20 4.5153 4.5039 ~ ~ ~ ~ ~ 4.3559 4.4378 2011 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALl BRA TED ~ ~ ~ AVG= ~ 4.3581 ~ AVG= 4.3370 ~ ~ AVG= 0.986 0.988 0.990 0.988 !bill. ~ 0.994 J!:m J!.l!l!§ 0.996 0.998 ~ 1 :!!:§1 lb.!!! The following equations are used to calculate the standard vokJmes of air passed through the DGM, V m (std}, and the critical orifice, V" (std), and the DGM caibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 0.993 (1) (2) (3) V =K *l": *Pbar+(6.H!I3.6) mt.nd> l m Tm v. --K'* Pbar * E> cr(."dl .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K1 = 17,64 "Rlin. Hg (English), 0.3858 "K!mm Hg (Metric) T m = Absolute DGM avg. temperature ('R-English, 'K-Metric) =Volume of gas sample passed through the critical orifice, corrected to standard conditions T,.,.. =Absolute ambient temperature ('R-English. 'K-Metric) K' = Average K' factor from Critical Orifice Calibration Vcl(.ud) Y=--= DGM calibration factor Vm<,dl AVERAGE AH111 =I 1.657 ( 0.75 9 )2 AH ('!_m(std)) V.,(std) \ v,. Temperature Sensors Reference In Out "F 33 68 202 "F 33 67 202 "F 34 67 202 PRE Console 110 Calibration 2011 U!!!! ~ !,ill 1.662 ~ !,§! 1.534 1.530 1.526 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range 2) Record barometric pressure before and after calibration procedure, 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. Facility Denison NYC Baghouse 4) Record data and information in the GREEN cells, YELLOW cells are calculated. K' TESTED r-----.----l FACTOR VACUUM RUN# (AVG) (in Hg) 0.5317 15 269.70 0.5317 15 274.838 0.5317 15 280.035 USING THE CRITICAL ORIFICES AS CALl BRA liON STANDARDS: 2.74.838 280.035 285.285 5.138 5.197 5.250 .0 .0 .0 .0 .o .0 72 72 72 I I S4 59 59 64 64 69 I I I I I S4 64 64 73 73 78 I I I I DGM AVG 57.75 65 71 0.00 0.00 0.00 0.00 0.00 o.oo FINAL 25.45 ELAPSED TIME (MIN) e 7.75 7.75 7.75 AVG(P..,.) 25.45 §§ §§ 4.4733 4.4621 4.4566 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECAUBRATED 1 ~ 1MI 4.5481 ~ 4.5481 1J!ll AVG= 1...Q1! 0.00 AVG= AVG= The following equations are used to calculate the standard V<Jiumes of air passed through the DGM. V, (std). and the critical orif~e. V" (std) and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y = 11.019 I (1) (2) 131 Vm = K • Vm• Pbar+(.Mf /13.6) ·:.ri:J) ' Tm V = K'* Pbar * 0 cr(J'.d) -• ./Tamb = Net volume of gas sample passed through DGM, corrected to standard ccndrtions K, = 17 64 'Riin Hg (English), 0 3858 'Kimm Hg (Metric) T m = Absolute DGM avg temperature ('R • Engli•h. 'K ·Metric) = Volume of gas sample passed through the critical orifice, ccrrected to standard ccnditions Tam~= Absoluti! arnb1ent temperature ()R-English, cK ·Metric) K' = A~erage K' factor fram Cnt1ca1 Orifice Calibratior = DGM calibration factor AVERAGE t.H® :1 1 . 684 1 t.H~ = ( 0.75 6 ) 2 t.H /'!_m(std)) V0,(Std) \ Vm .1,IQ§ ~ 1.664 POST Console #5 Calibration 2010 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated METER SERIAL#: 1--="--'-'------l CRITICAL ORIFICE SET SERIAL#: '-------' EQUIPMENT ID #: K' TESTED ~---~---1 FACTOR VACUUM (AVG) (in Hg) 0_5317 15 0.!5317 15 0.5317 15 161.753 186.777 166.777 171.877 171.877 177.041) 5.024 5.10 5.163 57 67 67 42 47 56 47 55 56 63 64 75 63 75 81 .0 .0 .0 I I I I I I USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: .D .0 .0 I I I I I DGM AVG 51.75 60.25 69 0.00 0.00 0.00 o.oo o.oo o.oo FINAL 25.45 ELAPSED TIME(MIN) 6 7..50 7.50 7,50 § § AVG(P.,,) 25.45 1.20 1.20 1.20 § § Denison NYC Scrubber 4.4253 4.418!! !Jill IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALl BRA TED 4.4222 ~ 4.4222 1.2!!.1 4.4222 1.005 AVG" 1J!Q! !!J!Q AVG= AVG= The following equations are used lo calculate the standard volumes of air passed through the DGM, Vm (std), and lhe critical orifice. V" (stO), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.002 (1) (2) (3) V: = K * V * Pbar + (t:.H 113.6) n1,.s,d) 1 m Tm __ K'* Pbar * 8 Vcri.srdl .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K1 : 17.64 'Rfln. Hg (English), 0 3B58 'Kimm Hg (Metric) T ~: Absolute DGM avg. temperature ('R-English, 'K-Metric) = Volume of gas sample passed through the critical orifioe, corrected to standard conditions T,m, = Absolu1e ambient temperature ("R-English, 'K-Metric) K' : Average K' !actor from Critical Orifice Calibration = DGM calibration factor AVERAGE llHI! =f 1.882 2 ~H® = ( 0.75 9 ) llH (Vm(std)) V"(std) V,. Temperature Sensors Reference In Out 33 67 121 "F 34 66 120 34 65 120 Post test Console #6 1.710 1.682 .1,lli Date: l PA ' t PB Type S Pitot Tube Inspection Data Pitot Tube l<kntiftcation: __ c;r___:_-..!f__:t':__ _____ _ Dt= . ~-)5-in Is P,.. = P8 ? _ _.Y_e.,':....S.,_ ___ _ PA = .4S-0 m . Is I. 05 • D, ~ D, :S 1.50 • D, ? __ 'y~......=:-c...--:::.......5..__ ___ _ Pa = • l( (:,-() In ((' < 10° ctr= a2 < 10° al= 'l.. p, <so p,= _____ _ Z50.125 in Z= · 0l"·:.J_. in W 50 03125 in. W=_ . ()0'2._in. W > 3 inches W= (9 I /1. ., in. Z > 3/4 inch Z = -~/_~ in. Ill. The pi tot tube meets the specifications for a calibration factor ofO 84? Temperature Sensor Calibration Reference Temperature Temperature Tcmp~mturc Source Reference Sensor Difference (Medium) ("F) ("F) (•F) AIR lO ""'1 0 (''") Probe Continuity ·~------.., WI/~ Heat Check 248 ---? -\f~<:> -r-<t l") AIR tO -,o 7') ICE WATER -stt ~() r Stack BOll. WATER w t.r '1..(') ·~ I SILICONE OIL y Dat<!: Dl Type S Pitot Tube Inspection Data Pilot Tube Id~ntilication: _'(..._.::;_"'\_-__ 6( ______ _ Technician: K • ~\..~~ Dt=.~~~ in~ ..:..p .. ~=--· _'-....:./_t.....l..t_.s"'-----111 _P,_a = __ .___J{f~lJ__.z'--__ in n 1 <10" a,< to• p, <5" Z s 0.125 in a, = __ 7.--:---- a, = ___ 1:..._ __ Z = _ • Q (} Z.. _in. .. -· ~-~:=:=t .. __ w Ws003125in. W = . 6 DJ in. W = __ -3-= ___ in Z = __ ..___ ___ in. Y = ---'3=-_J_'/_'f-'---_in The pilot tube meets the specifications for a calibration factor ofO 84° Temperature Sensor Calibration Reference· Temperatl!fe Temperature Tcmp..:raturc: Source Reference Sensor Difference (Medium) ("F) ("F) ("F) AIR tV (Qcr ( Probe Continuity -(' YvS H~at Check 248 _q '-r e.~ 2.. fs·O AIR (0 ()(o '1 I ICE WATER "::> -~ 3 ,_"? {) Stack BOIL WATER cDS V?;(" n SILICONE OIL TETCO Sample Box Temperature Sensor Calibration Date: 12/29/1 0 Calibrator: Mike MeN amara Reference: Omega CL3512A Thermocouple Temperature Temperature Temp. Diff. Unit ID Location Source Reference Sensor or Result (Medium) ("F) ("F) ("F), P/F Oven Water 34 34 0 Water 203 203 0 A Probe Out Water 34 33 1 Water 203 204 -1 Water 34 36 -2 Impinger Out Water 203 203 0 Oven Water 32 34 -2 Water 203 204 -1 B Probe Out Water 32 33 -1 Water 202 204 -2 Impinger Out Water 31 31 0 Water 203 205 -2 Oven Water 34 36 -2 Water 204 205 -1 c Probe Out Water 34 36 -2 Water 203 205 -2 Impinger Out Water 34 36 -2 Water 203 201 2 Oven Water 33 33 0 Water 203 203 0 D Probe Out Water 33 33 0 Water 202 203 -1 Impinger Out Water 33 33 0 Water 203 201 2 Oven Water 33 34 -1 Water 203 203 0 E Probe Out Water 33 34 -1 Water 203 204 -1 Impinger Out Water 33 33 0 Water 203 204 -1 Oven Water 33 33 0 Water 203 202 1 F Probe Out Water 33 33 0 Water 203 201 2 Impinger Out Water 33 34 -1 Water 203 201 2 1r Impinger Out G Water~ 33 34 -1 Water 203 202 1 ll Impinger Out H Water 33 35 -2 Water 203 202 1 Impinger Out I Water 33 33 0 I ~ Water 203 204 -1 Impinger Out J Water 33 33 0 Water 203 204 -1 APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. Prepared for: SECOND QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORATION NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE GRIZZLY BAGHOUSE BLANDING, UTAH May24-27 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines CorporatiQn 6425 s llwy9l Blanding, Utah 84511 Date of Report: July 18, 2011 ERTif'T AT£0 OF R ·P RT tNT · ,RITY Technical ·missions Testing ompany (TET 0) ce rtities that this report represent-s the truth <, well a· an be derive I by them thods emp(()ye I. ~· ry effort was made to obtain accurate and repres ·ntati e data and to compl with proc dures set forth in th e Federal Register. D an Kitchen Revi w r: ____ --""~:::......:.~..s.:::...;::...._-/«--x;:..t..=.:.L-.:.,....-'----.---- Oatc: _____ __._l_-.L.../.L..f_'~--_(_( ____ _ ~ Jo eph Kit ·hen R view "J ~ ~...__ D~1te: _,( ~-I ]5 ~ \\ ii TABLE OF CONTENTS Introduction Test Purpose ............................................................ 1 Test Location and Type of Process .......................................... 1 Test Dates ............................................................. 1 Pollutants Tested and Methods Applied ...................................... 1 Test Participants ......................................................... 2 Deviations From EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Summary of Results Emission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 4 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sampling and Analysis Procedures Sampling Port Location ................................................... 6 Sampling Point Location .................................................. 6 Sampling Train Description ................................................ 7 Sampling and Analytical Procedures ......................................... 7 Quality Assurance ....................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measured Radionuclide Emissions .......................................... 3 II Percent Isokinetics ....................................................... 4 III Sampling Point Location .................................................. 6 IV Complete Results, North Yell ow Cake Scrubber ...................... Appendix A V Complete Results, Yellow Cake Dryer Baghouse ...................... Appendix A VI Complete Results, Gtizzly Bagbouse ............................... Appendix A LIST OF FIGURES Figure 1 Facility Schematic Representation North Yellow Cake Scrubber .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D 3 Facility Schematic Representation Grizzly Baghouse ................... Appendix D 4 Schematic ofMethod 5/1 14 Sampling Train .......................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the North Yellow Cake Scrubber, Yellow Cake Dryer Baghouse, and Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat and Th-230 on the Grizzly Baghouse and U-Nat, Th-230, Ra-226, and Pb-210 on the North Yellow Cake Scrubber and Yellow Cake Dryer Baghouse. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yell ow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 though 3 in Appendix D. Test Dates One run was completed on the Grizzly Baghouse May 24,2011. One test run was completed on the NYC Dryer May 25 2011 and one run on the 26th. One run was completed on the Dryer Baghouse May 27, 2011. Pollutants Tested and Methods Applied The tests were a determination ofradionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. 1 Test Participants Test Facility State Agency TETCO Ryan Palmer None Paul Kitchen Mike McNamara Deviations From EPA Methods None Quality Assurance Joseph Kitchen Testing procedures and sample recovery techruques were according to tho e outlined in the Federal Register and the Quality Assurance Handbook for Air Pollution Mea ·urement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the fmdings ofthe test in Curies per dry standard cubic foot. Tables IV-VII in Appendix A have more detailed information. Table I. Measured Radionuclide .Emissions North Yellow Cake Yellow Cake Dryer Grizzly Baghouse Run # Scrubber Baghouse pCildscf pCi/hr pCildscf pCilhr pCi/dscf pCi/hr 1 498.4 3.3IOE+07 243.5 2.969E+07 0.277 2.158E+04 2 436.7 2.738E+07 AVE 467.5 3.024E+07 243.5 2.969E+07 0.277 2.158E+04 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test filters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for the Yell ow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. The test filters for the Grizzly Baghouse were had no visible particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities 3 None Percent Isokinetic SampJing Each of the tests were isokinetic within the ±10% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokinetic sampling point by point. !so kinetic values for each test run are presented in Table II. North Yell ow Yell ow Cake Run# Cake Scrubber Dryer Baghouse 1 2 99 100 99 4 Grizzly Baghouse 100 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow pressure and baghouse p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9 .5 feet) upstream from the next disturbance. Figure 1 in Appendix D is a schematic ofthe stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. The inside diameter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch diameter sample ports located 2.56 diameters (48 inches) downstream from the last disturbance and 1.31 diameters (24.5 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Sample Point 1 2 3 4 5 6 7 8 9 10 11 '12 0.58 1.89 3.49 5.81 12.19 14.51 6 0.70 2.34 4.74 11.26 13.66 15.30 0.50 1.26 2.21 3.32 4.69 6.68 12.08 14.06 15.43 16.54 17.48 18.25 Sampling Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment set-up, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook for Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake D1yer Bagbouse Table VI Complete Results, Grizzly Baghouse Nomenclature Sample Equations A TABLE IV NYC Scrubber COMPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol DescriEtion Dimensions Run#! Run#2 Date 5/25/11 5/26/11 Filter# 5786 5770 Begin Time Test Began 8:15 8:08 End Time Test Ended 16:27 20:27 Pbm Meter Barometric Pressure IlL Hg. Abs 24.50 24.35 8H Orifice Pressure Drop ln. H20 0.820 0.770 y Meter Calibration Y Factor dimensionless 1.001 1.001 Vm Volume Gas Sampled-Meter Conditions cf 301.880 288.884 Tm Avg Meter Temperature "F 100.6 101.4 .V8P Sq Root Velocity Head Root ln. H20 0.2375 0.2255 Wtwc Weight Water Collected Grams 719.0 737.2 Tt Duration ofTest Minutes 480 480 cp Pitot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.3795 0.3795 C02 Volume% Carbon Dioxide Percent 2.80 3.80 02 Volwne% Oxygen Percent 16.40 16.60 N2 &CO Volume% Nitrogen and Carbon Monoxide Percent 80.80 79.60 Vmstd Volume Gas Sampled (Standard) dscf 233 .627 221.853 Vw Volume Water Vapor scf 33.901 34.759 Bws (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.127 0.135 Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.114 0.114 Bws Fraction H20 in Stack Gas * Fraction 0.114 0.114 xd Fraction of Dry Gas Fraction 0.886 0.886 Md Molecular Wt. Dry Gas lb/lbmol 29.10 29.27 M, Molecular Wt. Stack Gas lb/lbmol 27.84 27.98 %1 Percent lsokinetic Percent 98.9 99.5 AVG T, Avg Stack Temperature "F 112.4 112.3 112.4 A, Stack Cross Sectional Area Sq. Ft. 1.767 1.767 Po Stack Static Pressure In. H20 -0.065 -0.065 PbP Sample Port Barometric Pressure ln. Hg. Abs 24.43 24.28 P, Stack Pressure ln. Hg. Abs 24.425 24.275 Qs Stack Gas Volumetric Flow Rate (Std) dscfin 1.11E+03 1.04E+03 1.08E+03 Qa Stack Gas Volumetric Flow Rate (Actual) cfin 1.66E+03 1.58E+03 1.62E+03 v, Velocity of Stack Gas tpm 9.39E+02 8.92E+02 9.15E+02 Curies Radionuclides per sample pCi 116431.6 96883.3 Crad Concentration of Radionuclides pCildscf 498.366 436.700 467.533 ERr ad Emission Rate ofRadionuc1ides pCilhr 3.310E+07 2.738E+07 3.024E+07 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1.7). Symbol Date Filter# Begin End Pbm H. y Vm Tm ..Jt:.P w".., T, p Dn Oz 02 2 &CO Vm&ld Vw Bw, xd Md M, %1 T. As Po Pbp P. Q. Oa v, Curies rad ERrad DescriEtion Date Time Test Began Time Test Ended Meter lluromemc l'rcssure Orifice Pressure Drop Meier CuJibrntion Y Pnctor Volume Gns Sumplcd-lcter Conditions 1\''8 Meter Tcmpcrnturc q Root Velocity Head Weight Water Collected Durotion ofTcst Pilot Tube Coefficient Noule Oinmetcr Volume % Carbon Di11.'<ido Volume% O~ygtn TABLE V COMPLETE RESULT , PM DE NI ON MTNE CORPORATIO 1 YELLOW CAKE DRYER BAGI-IOU E Dimensions Run#1 5/27/11 5769 7:17 9:20 ln. Hg. 1\bs 24.35 ln. HlO 1.3[2 dimensionless 1.004 cr 88.585 or 84.3 Root ln. H,O 0.5033 Gmms 26.3 Mlnulcs 120 Dimcnsiruolcss 0.84 Inches 0.2740 Percent 0.00 Pcrocnl 20.90 Volume% Nitmgen nnd Carbon Monoxide Percent 79.10 Voluoltc Ons nmpled ( tandnrd) dscf 70.493 Volume Wntcr Vnpor .. r 1.240 FraClion H,O n t~ck Gns Fraction 0.017 Frnction of Dry Ons Fraction 0.9&3 Molcculnr Wt. Dry Gas lbllbmol 28.84 Moleoulnr Wt. Stook Gas lbllbmol 28.65 P=cntlsokinctic Percent 98.6 A vg Slack Temperature •r 105.4 Smck Cross Sectional Arcn Sq. Ft. 1.396 Sllock Static Pl'tssure ln.I.J,O ·0.18 Snmpl• Port Dnrometric l'ressurc ln. Hg, Abs 24.28 Stnck Pressure ln. Hg. Abs 24.267 rock Gas Volumetric Plow Rate (Std) dscfin 2.03 ·+03 Smck Gas Vol.liiTICtric Flow Rurc (Actual) cmo 2.73E+03 Velocity ofStnc Gas fpm 1.96 ·+03 Rndionuclidcs per sample pCi 17164.8 Concentration of Rndionudid pCildscf 243.4970 ·missoon Rme ofRndoonuclidcs pCilhr 2.9696+07 Dryer Baghouso ymbol Description Date Date Filter# Begin nne Test B<:Jl8n End Time Te t Ended Pbm Motor llnron~etri~ Prf:S$ura H Orifice Pn:sstln> Drop Y Meter Collbmtion Y !'actor Vm Volnmo Gas nmpted-Mc1cr C(lndidons T 01 Av& MC!cr Tempernturc ,,t,p s~ Root Volocity Hond Wlv,., Weight Wmcr Collcc:tcd T, Du111tion o TC>I CP l'itot Tube CocOicil:m Dn Nozz.le Dlomcter C02 Volwnc% Corbun Dio~idc 02 Volume% O~ygen N2 & 0 Volmnc% Nitrogen ond Corbon Mono><ida Vmstd Volume Gas Sampled (Silutdord) Vw Volume WAter Vnpor B W 5 Frnction HJO ln Slack Oos Xd l'racliou of Dry Gas M d lolc<:ulnr W1. DryGns M, Molcculnr Wt. Stock Gas o/ol Percent lsokinatic T ~ A vg Sleek Tcmpcmum: A. tnck Cross Scctionnl A,-,.a P G tack Slntic Prfo.'isa"" Pbp Snmplc Por1 Borometric Prcssun:. P, tnck Ptossure Q,_ mek GtlS Volumetric rio• Role (Std) Q,. Stack Gas Volurm;tric Flow Rme (t\ctunl) V 5 Velocity of Steck OM uries Rndionndidcs per :snmplo Crad Conccntmtion ofRndionuclidcs ERrao Emission Rnta ofRodion~clidcs TABLE Vl COMPLETE RESULTS, PM D NT ON MINE CORPORA TI'O GRlZZL Y BAGHOU E Dimensions h Hg. Abs ln.l-1,0 dimensionless cr "F Root ln. 11,0 Grnm• Minutes Di.trensimolcss lneh~s Percent Percent dscf scf f'roction Fmction lb/lbiTI(II lbllbmol Percent •F Sq.l't. ln. 11,0 ln. Hg, Abs ln. Hg. i\bs d.<cfin cfm fplll pCi pCildsof pCilhr Run #l 5/24/1 1 5785 7:53 15:58 24.20 0.863 1.001 310.106 88.7 0.2257 50.7 480 0.84 0.3700 0.00 20.90 79.10 242.234 2.391 0.0 10 0.990 28.84 28.73 99.9 71.1 1.917 -0.03 24.17 24.168 l.30E+OJ l.63E+03 8.SlE+02 67.2 0.2774 2.158E+04 Gnzzly %I = percent isokinetic, percent A,= stack cross-sectional area (fe) AS~P = see ...J~p M5 Nomenclature Btu= unit heat value (British thermal unit) Bws = fraction of water in stack gas C8 = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cr = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) Cmetal = concentration of metals (ppm, IJ.g/ft3, etc.) atomic symbol replaces "metal" C02 = percent carbon dioxide in the stack gas cp = pitot tube coefficient (0.84) C -species symbol replaces x . X (avg)- Cx (corrJ = actual gas concentration corrected to required percent 0 2 ~H = orifice pressure drop (inches H20) ~H@ = orifice pressure (inches H20) ~p = stack flow pressure differential (inches H20) D, = diameter of the stack (feet) Dn = nozzle diameter (inches) EA = percent excess air ER8 = emission rate ofback half particulate (lblhr) ERF = emission rate of front half particulate (lblhr) ERmmBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point ~p to determine test point ~H L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lb/lb-mol) MF = mass of particulate on filter (mg) MFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe (mg) M, = molecular weight of stack gas, wet basis (g/gmol) N2 = percent nitrogen in the stack gas 0 2 = percent oxygen in the stack gas ...J~p = average of the square roots of ~p (may also be referred to as AS~P) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) PbP = absolute barometric pressure at the sample location (inches Hg) P 0 = stack static pressure (inches H20) P, = absolute stack pressure (inches Hg) P,1d = absolute pressure at standard conditions (29.92 inches Hg.) 8 = time of test (minutes) Q. = stack gas volumetric flow rate (acfm) Q, = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (fe /min, wscfm) T, = stack temperature CF) T,1d = absolute temperature at standard conditions (528°R) Tt = see 8 M5 Nomenclature um = mean molecular speed (cmls) Ym = sample volume (ftJ) at meter conditions Ymsld = volume standard (dscf), sample volume adjusted to 68~ and 29.92 inches Hg. Y5 = velocity of stack gas (fpm) V we= volume water vapor (sef) at 68°f and 29.92 inches Hg. W = Width of rectangular stack (inches) Wlwc = weight of the condensed water collected (grams) XcJ = fraction of dry gas Y = meter calibration Y-factor (dimensionless) Method 5 %1 = Vffisrd • {T, + 460) • I 039 I (8 • Vs • P, • Xd • Dn2) As= (Ds2 I 4) • 1t Bws = V w I (Vmstd +V w) C6 = M6 • 0.0 1543 I Vm51d Cr= Mrp • 0.01543 I Vm$1d Cx (corr) = Cx (avg) • (20.9-desired %0~ I (20.9-actual %02) D~ = 2 • L • W I (L + W) Dndcs = ...J{0.0269 • (Pb,n + 0.0735) I [(T m + 460) • CP • ~ • ...J[(Ts + 460) • MJ I (P, • 6 P)]} EA = (%02 -0.5 %CO) I [0.264 %N2 -(%02 -0.5 %CO)] ERe= Ce • Qs • 0.00857 ERF = Cr • Q5 • 0.00857 ER nunBtu = ERx I (mmBtu I hr) K-fact = 846.72 • Do4 • 6 H(al • C/ • Xd2 • Md • P, • ('1'111 + 460) I [Ms • (T5 + 460) • (Pb'" + 6.H I 13.6)] Md = C02 • 0.44 + 0 2 • 0.32 + N2 •0.28 Ms = (Md • Xu) + ( 18 • Bws) Ps= Pbp +(Pol 13.6) Qa= V, • As Qs = Qa • Xd • Ps • T51d I [(Ts + 460) • P51d) Qw = Q,IXd Vmsrd = Vm • Y • Tsrd • (Pbm + 6 H I 13.6) I [P51d • (Trn + 460)] V~ = 85.49 • 60 • Cp • ..JtlP • ...J [(T5 + 460) I (Ps • M,)] Vwc= Wlwe • 0.04715 Xd= I -Bws APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Field Data Sheet Y eUow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Field Data Grizzly Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Denison Mines Stack Identification North Yellow Cake Scrubber Date /IYl t?-,. :z ~ w ' I i Barometric Pressure Pbrn .l<J. .~ inHg Pb~ .?.C...f. <(.!, in Hg N Bo Static Pressure (P0) '7o&!.S. in H20 Estimated Moisture (Bw,) % Sample Height from Ground tO feet A Comments: Stack Dia. 18 Reference: 0 Ports arc 9.5' Upstream lrom next disturbance Ports are 9.5' Do"11strcam from last disturb~ nee Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F 1 3.2 0.5 8 0.58 Ill 2 10.5 1.89 1.89 .04/ 3 19.4 3.49 3.49 Ill ,os~ 4 32.3 5.81 5.81 Ill .o&Z... 67.7 12.19 12.19 [I() 5 '0 (p(p 6 80.6 14.51 14.51 110 , o~'f 7 89.5 16.11 16.11 110 ,O(,O 8 96.8 17.42 17.42 I Averages: Ts ___ _ LF!ow ---- ~P __ _ ..J~p ---- KEY=> ~~T-s--~6~P_L __ F_Io_w~~ n:rco filt~r 5 7S '{ Sample Box _ V Page _/ of ),. Run ~ L Plam Denison Mines l.ocation North Yellowcake Drver Scruhh.:r Operator {'<\ • M ~rJ~('o--. Date ----'-'m-"g"'-."<;Y'--""2'-"'S:....,,I-· Z"""'o_,_/'-1 ----- Tw-.crsc Time DGM .. ~:J, I 1\H ~~r. -1;:.'1) V3cuum Temperatures 1"h DGM Tconp!TF! Point Clock Min (ll) .•. Dt::Strt!d Actuol 'l'l llji.i Stack IT) Probe !!rob.: Out F!lter E!11uent Out In ~ 1 o~:1) 0 (.,oz. .o~t .o"iS . "~ ·~~ 2.. Ill. z. 7)"' lri 27\ t..4. (,.3 (.3 i B 0 A N 1 15 ~ l o, "i'l""L oo)'l ·1) t7) 1... 11'3 £.1! 27-f' l"'1) ~<1 b§ /{ Port R('f~rence 0 0" . Stack Diameter _lS"_ 2 30 {.f 1. t 'f'-\ •<>{~ ,1} til 3 il3 Z)£3 ?.I~ C::l,y {.,(.( 1 1.{ S l Pons are 9.5' Upstr~am from next disturbance 2 45 '-'-B' i1 :> .o)L IT~ ·13 4 !I"Z.. (.(;.~ 2. -n '21\ l...o Ro ~ Ports 3r~ 9.5' Downstreom from last disturbance 3 60 "37,0G.1.-·o5'"\ n1 ,,, '-1 llC.. 2"'11 z.n_ 21L. St) 6'1 qc_ Assumed Moosture 4-13 I)JQ __2...._ 75 (.~~. )l..:S' .~;, '7 '0 n~ 5 II~ 23~ L!.~ l<.,(o 5ct '0'1 '1~ 4 90 c.. 5 ') ·U.t(l •oS" .oao .eo 5 II'\ Z.'-/IQ 'Z..b) l.\o)-"0 '11 )Of) Probe ;.r-4-Cp 0.84 Noale CaiJb rauon 4 105 C..'-'1· 13'{ ·oiO 1·00 loOO l' II'\ Z.{L Zb"'"'t 'Zfol 59 1~ l Os ~ .;aQ .. ';'=/4 .~8'0 5 120 <,1).1o!{ • o<.~ I Cf(. I '/'L 7 II~ z..-to 'Z.bl 't. I. I Col Cf) lob Avg D, ·"':79<f-2 inches 5 135 C.<a5. H.z.. ro(,!O ·9 {' ,q-{ e ll8 Zl~ ?..7o Z..7o (,'?..-11 to0 Ga.5 8Jg ~~os- 6 150 C..'f5. ~'{~ ,cl.') I '1_( .q( 10 \\ 1" "2.1(' z,r z-,r-"i '1~ 110 C\1n:-oh:! s 6 165 loS'. 3S"i .a(,( I 10 '0 ,?J'() l{) lt'J 2l"Z.. Z.l) 213 55 100 ItO Y·factor [.oo I 7 180 llS ,l.l'l. 1oJb .~\ .<a t l\ \1'-\ '2"1 c ~~ 'll<.f )(, I Clo ItO ''H© '-'(8 (p in H,O 7 195 !l.'-\. !.C.l . ·~>S<> .~~ ·'al u / lq no L1'i '2.'1'-t 59 teo 1[0 Barometnr Pressures 8 210 13 't.t{L q,~c. .~l , o( L'Z-~l) '2..70 1. 71{ 2rr..t (.( \CO (o'{ Ph"'-~ .so 1n Hg 8 225 "7 'i~ 0,6' .,~{ •q,i:l ,·so l3 l t ) 254-'Z!"l 7 1'1 (,£.. 'f'l Jo0 Pb, .7-4.4} on Hg \7.\ 11 240 =J of!> .~:Js r \lf'\. p . -. 0 s in H:O ~~), o'OI ''''""" D .. ooz..-o. ooL ,.,c;o H,; Z.o.:;' S,o p;.,,R'" 0.00 (}, DO In H,o • 2.~ 1-r;' Water Collected------- Time S"npled _______ mon Total / '1""'-\S l.'Jsr/ ~-S L~o 13.!{0/ 1gy{ / Rcvii!W 1 ')\.oSo -J ,1 'J41-• 81 (,l \If. 3 Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate (tetminl DGM After Leak Check Vac ("Hg) Rate (tetminl L I'-\. Field D•ta Sheet Plant: Denison Mines Date: S l 'L. 5 J ll Travetle Time DGM ~ AH''"" Point Clock Min (9) \llJi ,,,, Desired Actual 1 12:1.1 240 15~. Sol • .. .(o( • 'l 1 255 IC.Z.. o'1) •0 11'-1 ,,~ 'Z 270 110, t.{~ .o)t... ,,) ·l)' 2 285 17'1. ,So .t>(t.. II '"I ·1'-1 3 300 181? ,qc;<., oc$'1 tl} :73 3 315 lf1· S1o .o$! t1? 11?' 4 330 ?Jo<.. g l~ .c.)~ I lJ 111 4 345 l ~llo 0,3 •oC.t.f ,qZ.. 'Cf-z_ 5 360 82.._{. '1t..'1 ,oC.) • ~Ia ·'i'~ 5 375 €3<o. o'H •ot.,f ,qt;. ,q" 6 390 <3"{(g. 'Bj .c,c ·'fO ."to 6 405 t~s-b. t'il 'o(..t "\[ r<\( 7 420 l f3{c,[...or..~ '~'5 .b . !3'\ . ~i.{ 7 435 87L7o1 • o)fo , Stk .~u s 450 ig25. 3l:.e . 0$6 ·Btt ,gq 8 465 ~'1_5, Ol3 I fjj" .s~ ,g'{ 11:. .n 480 ~-o"t·lo 3 t 1.0~0 Vacwm {JJI!g) "L :s > ~ 5 5 (p I q q 10 ·~ 10 1\. d \'L TETCO Filter )7'6G Sample Box_~ Location: North Yellowcake Dryer Scrubber Operator: M• M Ltk--Mq....l£--- Temperatures..,,,, Stack (1',) lll..f ll"\ 1\'( tiLl lll3 t08 li'J ll, liO lbl.. !O( ,oj' lo:J \ () :) IQ..( lor) l?:l ") \ \)) ) 5'1~ Prob~ "1..3\ zro ""l.~{ 1"-o Zf) Z.1[ IT) lb~ 1 '\~ lb'l lC."\ ~!'f "lZ't -z.M5 Z~) Z.Col I tl.. &.\ / Prnb.:Ou! Filta "'l)l '2.n 'Z.)'t lSL\ z,.; l.C. ') ZG.L{ uu. Z"i l.C.t 7TL 'Z.IZ.. ?.7) z_-r) l13 ~~3 27o Z.70 2n. ZTL ll\ Zll '2"'tt l11 I,{,L-£..1,?... ~~'3 z.t.S [[\,_ 2.1 \. 1..'70 lr-o Effluent b$ C.. I 5'1 ~?.. bo rot J,2. (,3 G:.3 'l. (.,~ (p"i Cot /o( ~'- ~'{ Additional (Extra) Leak Check Information • 8'2..0) o/ DGM before Leak Check Vac (''Hg) Rate (te/min) DGM After Leak Check DGM Ten1p (T ml Out '" q" 'f'f 91 lo3 qcr lot qq to~ £1R to I Cf'i to€> LOZ... (1 0 lb£._ l\l lo1.... 113 IcC. 112. IOJ t ILj ~oR Ill {OGt 115 ll\ llO 1/Z... )Z..f) liZ... 17-V Vac ("Hg) Page _]_ of "Z. _ Run I! l i N A Stack Diameter _IS"_ Port Reference _0,0"_ Pons arc Ports are 9.5' Upstream from ne>.l disturbance 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe 11 (z Cp 0.84 No72le Calibration .)19 ·3~0 ,:P"< ,~:C~ AvgD, •11'\J i:;:-- Gas Bag E.-o) Console -=5:___--:- y ·Factor ~ • JO l Ll.H~ 1 '-l~~mHp Barometnc Pressures Pb,. L 1..4, )'0 in Hg Pb, 1. '-l · 4 ) in llg Pc;, __ -_ • ..:..O..:(.....::>_in H20 Leak Che<k ft:./min 9 . oef v:u.:inHg 2..0•5 Po~t 0 oo 2-. 5.v PioooRate 0·0 0 >0 lnH,O (),as O•tf Water Collected __ r..c...l_Cf..,.. • .c::.O __ g Time Sampled 4 fJ'O min Review· K= K= @T'" @Tr:. Rate (ft3/min) _j__l_ ':':\_ Field Data Sheet Plant Denison Mines Date: __ Vk------'"'-'f'-'i'---~--'-'-'-2-c---'t-'-t ----- Tmver:,c "filTH! DUM CIP llH """·"" Polnt Clock Min (8) dl\ ··~~~~~~~· Desired Actual 1 g:Ofj 0 'tos. 1. '-! f ,0'7 0 .~-r ,s-'J. 1 15 '112.-Cft.{O ,O(ji:> .si .5? 2 30 'lz.o . £',& 'l ,0'-("Z--~0 .G,o 2 45 .. <t.z.s' 5Z_~ .o<l.S' . (,'{ • (,Cf 3 60 't3"'. 8<-t f ,I:)Lf') .c.,& .&(p 3 75 f1"<i~, :).~..t~ ,aut;; -&~ . (,';i' 4 90 9:53. ~1-•OSS" .~o .go 4 105 'tG.1.li3 .0~-. €0 -8'0 5 120 'i'11. Cfi-~ r0$8 t8'1 .f'{ 5 135 crs L '-~gc=t o58 .3<1 . 8lf 6 150 '1ctl 0~~ ost-.g_q tflj 6 165 JOOD.SLZ.. ·O(gO 'Eff . 8'€ 7 180 toto. ;s-o .o~ .13 .ffi 7 ¥ 195 tD l't. !J 30 .ooe •81 ·81 8 210 \o L9.o9'1. dJ:)\ Ill ~-n 8 225 'o3 8. t'{(q •o'(S '"J ,(.[ 240 l o'{ ~ .G.eS ~ Total l4l, )bl) l s:ftS Additional (Extra} Leak Check Information DGM before Leak Check Vac ("Hg) 5? 1o TETCO (S Filter . Sample Flox Locat10n: North Yellowcakt: Dryer Scrubber Operator· •~ ( ~. f<t fcJ, o 7 Vaclmm femperatures r 1, •II'H!:'i Stack (TJ Probe Prvb.:Out Fdter Eft1uent z..o /}t_ 23."' 2..3~ 2,~:, (.,.,3 2.-0 /l'?J :2.~ J-45" J.l./l{ 1D.o 3.o /13 zro t Jv2 ;l(p2.. &t.t 'f.o lf3 2-S0 ;l.SB I ..<.53_ (.,o 5.0 It'{ ~-.:; '2-SO 2S'"o ( .. Z... 5.0 fl.$' 23~ z.s-h ZS'-(D'-f 1-.o (I~ J.~f,; :z.sz... 2-52-&~ 'i.o f{(p )-(pC( ?41. Zf./P. &I 8.0 IN ;;H~<t ~'{[ J.-4.0 (..2... ~~ II 'f ?-&Z. Ub IU) ~2 /O.i> /13 ~&(o ~SB 2.58 G,3 /2..0 Ill d[,'f 2.5() ~SI !...::- (2..0 !lO -z..~o 2..>2:. 2-S'Z-CP'Z.- ll.o ~Cf 2.5'( 2.-5) 2-55" Ul-2..- ll-0 lo!;. 211 Z'io Z.'ia {p(p \2..0 lo'l Z.'Z.t6 2<-\) Z'-1) &>~ Rate (fe/min) DGM After Leak Check DGM l":mp (T~l Out In (,1 t..b 7f-t =!3 :n-83 ~3 "to ~(s, ?s- <to loo 'TZ /lJ'Z- ~'-I tOY 9':l /I){;> 't:C, {tJf_ ?8 __!!2E_ 17 liD tao /£( too iLl 'if q'-{ q., t o~ 3oco,., Vac {"Hg) rage _ / of_~ Run "_L i N A Stack Dtameter 18" Port Reference _0 0"_ Ports are 9.5' Upstream from next disturbance Ports ar< 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe Cp 0.84 Nozzk Calibration .:lli_ . :l i?o .:...l1i__ . J ~ 0 Avg 011 ~,'¥is-inch~s GasBag {5-0~ Console s- Y-Fact\>r {.oo I :\H@ (. 'IS"<Q in H,O Barometric Pressures Pbm _.2_~--m Hg Pb, .2 '-f. l-f{ in Hg p,. -: 0(,~ m H"O L~k n.~d.. rre n 1:'min o~ OOY "'" ir. Hg Zo. -; f'o~t o.oo'2.. 5.o Pi!ot R'"" Q. OQ 0 • \!(} lnH:O ,Z.S • '1-5 W:llor Collcctcd ______ g Tun<e Smnpled ______ rmn Rate {ft3/min) ){ '5 kvt J~f! ll ~ '14 ,t)r't er? s~.,-\ d~" R£5T~fl (.M~ \'5:to ~ F1eld Oata Sheet Plant: Denison Mines Date: fl.\ ~--{ ):_(, 1 Io II Tr.aversc Time DGM !'lP ll.H ('OH,O) Poant Clock Min (9) (r.}) (inH:.O~ Desired Actual 1 1117:~ 240 5l. l '{5 , oS" ,Js c}S 1 255 &; O.).v._c{ •O:!J-~ -s>3 .(/3 2 270 (pCj .7~" .oss -~3 -83 2 285 _11_. Z-€4 ·~5'i'" -R~ -9'3> 3 300 ga .~z..~ -o~r-·tZ. ~r"L 3 315 "H. :f'1o .o~r .8f-·'81- 4 330 /Ot. '('{"Z, .oS) .8'{ .ev 4 345 !'" .ttz& ,o~) _'('-{ ~gc.r 5 360 /)..(g, '{1<4 .OI.J~ .&,'1 .&'t 5 375 !3S.Df~ .rt. ).~~ lvS3 6 390 II.-{€ -l-'tt ,o<{$"" ,{,~ .t.-9 6 405 LST. ot8 .()t.f5' .f.:, 'i .(,C[ 7 420 l(p[;. f(.{O ,0<-{0 .~( .. (, ( 7 435 l[), q4'S •0~( . ":. ·~3 8 450 [g'Z..J-'2;'-{ ·O"I I ·~3 . '!, 8 465 t'iD.(., rs-rOllO . (,I • lt;( Zo'.t..1"' 480 tq~ tA'-- Total L ~~ .t~8L1 /-r ~-&~cts Average v (t.7..5{/ Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Va.:uum \uiHI!J 3-1) <.f,r; "f.o <t.o 'f.o 5.D 5.0 S.o i..o q__D 1--o 1.0 :t.o 1 .o 7-o f-.z:> TETCO Filter 5?1l . SampleHox_B __ Location· North Yellowcake Dryer Scrubber Opemmr: I'\:"'-£ Mu-J.o...Mo-.f""-- Temperatures ~r, Stack{T,) Probe Probe Out Filter Eflluent Jt'1 ;;'-~B :l:jo ;J.«J-9 Cpf- 113 2~6 ~G.<t .;}.(p'f ~(a 113 ~'-{'} ~0 J4z. (;~- /(If 2S/ ~(pC( ~'-S ros- /1.5 ;J. t:fD 2--5"3 ;) '10 (.;,~ /Is-).l.{o ;((.(I :2•-lO ~'I _lj0 ;).1./"l.. ;l(s.lf .?.48 (9.'{ It~ .lito~ !;:;t{)B J-&3 !R3 /I 'I ,;2-3(o d-so [')...1.../0 ~J I cz .. z..Sc;l 2#Cf 2..5' { (,.t) IL3 )..~!./ .24!1 2?>1-&o l1L,... 153 ~I 1..;2'lr ~ !13 ~f.,Z... 27-0 2..S'~ ~( 11'2.. Z:)q '1..60 t.I..O (..(.. /11., ut_q ~0"8 J.'-J(p ~3 lfL/ 21-1 U..Z-l-SZ... &3 Rate (tetmin) DGM After Leak Check DGM1'mtp(T,.I Out In f? ?9 lot (o(o loS Jj_3 lo& /Jb Lc:;7-118" ,~::; /( t tr~r /I~ /Of£> ti&> /O(p j 11 /o5 {(.{ ;os-,u lOS lib (a<( !I¥ lo·) Ll?... /oL I !.I I o l-/I I lo(.'f / Vac ("Hg) Page __3:__of '-Run# )._ i N A Stack Diameter 18" Port Reference 0.0" Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-13 Probe 2.1 ~ Cp Nozzle Calibration ,}"19_ .,3So l37<1 Avg 0, , ~ 1'1.) inches GasBag £cf Console __:5:::..__ Y-Factor ~-oo l ,~H@ ~-.<-!~'=> mH00 Barometric Pressures ,., Pb,. 2..4.~) Pb. 'l.'{, 'l..-~ Po -• c.) % 0.84 ,3\30 inHg in Hg inH,O Leok Choc~ Pre Eru! ft1im1n 0 .00-:; V3C in Hg W.c Pltot R.!te 0 ·00 lnH.:O ."L~ Water Collected Time Sampled Review Rate (ft3/min) e_t:d{ {-();() Q-Ob .tS ?31--2- ~~D PRK. K ~ K= g min Yellow Cake Dryer Baghouse Prelim G pts blank I" Facility Denison Mines Stack fdentitication North Yellow Cake Dryer Bn~hou~e Date s (1.1../1[ i Barometric l'ressure B Pbm l.'4.'\i"' in Hg Pb" ~ ... ,~ in Hg N 0 Static Pressure (PG) ~Hi) -.18 A Estimated Moisture (Bw,) I '}.~) Sample Height from Ground feet Comments: Staek Din 16 Reference: 0 Ports are 57" Upstremn lrom next disturbance f'orts are 468" Downstream from last disturbanee fllff. Traverse Percent Distance From: Ports Point Diameter lD Reference A B C-& D E F 1 4.4 0.70 0.70 2 14.6 2.34 2.34 'l) • t:~l no .I'\ ] 29.6 4.74 4.74 4 70.4 11.26 11 .26 ·n ,.,, Ill ,1.1 5 85.4 13.66 13.66 8:1 '"' lit. 6 95.6 15.30 15.30 ,t, Averages: Ts II\ L Fiow 6P ,&..l\,"3 '>i6P [Ts KEY => L Flow! 6P • o'L' Field Data Sheet Plant: Denison Mines Date: ~ ( 'L, f U Tmvcrsc Tin1e Point Clock... Min (fl) 1 ~ 0 2 tO 3 1.0 4 "30 5 4.c 6 Sc 1 8!2D loo 2 10 3 eo 4 qo 5 iffo 6 i[O <1:-z..o !1-D DGM (tl1) 39 . .n'i 4b. zc.z. S"">.,l(O o~,'iSC\ f..lh LoO -n-t.r.crs 8!..1."10 89.5~'2. q(, ·1" lo<{.5S€ 112., '\o'\ (l.O.I2.l 11.,.,\'f i'IP ~H lioH~OJ ~ .. 11,0! Desired Actual .l.l L•<::>""l 1.~-, t"tl l..o"T 1·~, ~ Z..l V<>t>'l. I •~D1 t"Z.g ,.~( ltl!S" l'l..'i 1 .--to i•<.f.o .~'", \• )4_ !tJ"\ ,"2.'{ l' "l.'{ 1,-z.'"\ I 1.(0 II)( lr3f l"t(. Ill) l, ~"5' ~"t.q l•JO t,{o 1'1.7 l•'-10 i•/.(0 l"t~ /,q'( j, '"{"") - TETCO (- Filter 57 C.~ Sample Box - Ya-ctwm ) 1.... 3 3 '-{ _L.j '{ tt _'-i '-1 '{ '"i '{ Location: North Yellowcake Dryer 13aghouse Operator: M ·I~ ~N I'J.,.'fi/\.(J...( cr- Temperalures ,~, l Stack (T,) Probe ProbcOul Filkr EOluenl !O I "Z7~ 21"o zeo b1 I C"L. 1.12. 1...?0 1.1o ~" lcl '2.1{ l1{ "2..11" S(, let{ 777-Z7o 1.70 51 IO'i 110 l1f" (., 1"1' sco lo~ 1.(..:; t"1) 1.1)_.. 5tl lo~ 7..1"5 t 1 C!l 2<0 1.:>0 l of., 1...10 1.1") 21"1 55 lol H>} 1.1 I 2.. il 51 ! e"l "'t.t..<-1. "'Z.!ol 2(:.1 ~~ 1 o9 "lf:,} "l(C Z5o 5~ 110 zn Z;)l z.n .59 To till Bs~ 5SS.,; (,. o'io l \S ·l!.(o/ i £.laS/ ~.So?>:; L-~12-. IOS·ll Comments, Time I Bag house aP Time Baghouse aP l>ll 4.1 8'.)41 DGM "I cmp IT~) Out In lc_ ""l.l 1f 1) l~ ,., Bo sz. !~~ 8.b ~ ID B1 S{c; 'fj~ -g-9; ~8 '"to 'fo -q'- 9! ~3 ~" '15" Page ( of_(_ Run# L i B I N Ao Slack Diameler _16" Por1 Reference _ 0.0"_ Ports are Por1> ore 57" lJ p;tream l"rom next disturbance 468" Downstream from last dosturbance Assumt::d Moisture ,, _....;__" Probe 18 (:, Cp 0.84 Nozzle Calobration .Zl) .17:} 1"2.7'-i ,t_")'t Avg o, • t 7'-io inches Gas Bag Ambient Air Console ..3 Y -Factor I, .10 't i'IH® It (,~iij on H20 BaromeHic Pressures Pb,, "Z.Gj , 3 5 in Hg Pbr "2 ~..z£ in Hg P«. -• I e in H10 l.eeik Chock Pre fr"/mm 0. 00 4 va::mHE 20,0 Pilot Raoe 0 • 0 OrO ~~o q.o 5·~ Water Collected ). b 3 !: Time Sampled _______ min K~ K- @Tn~ @T.,. Grizzly Baghouse Prelim 12 pts blank Facility Denison Mines Stack Identification Grizzly Baghouse Date I'V!ll'A j ;;v..t 1o il i Barometric Pressure Pbm d-J1 . z..o in Jig Pbp ;) l./. I f-in I Ig N AO B Static Pressure (Pc;) --03 inHP Estimated Moisture (BwJ 1 o;., Sample Height from Ground so feet Comments: Stack Oia. 18.75 Rdeocnce: 3.0 Must use 36" Erobe or lon!l:er to kecE box outside handrail Pools are 24.5" Upstream from next disturbonct• f'orts arc 48 " Downstream from last disturbance Traverse J>crcent Distance From: Ports Point Diameter ID Reference A B c D E F I 2.1 0.50 3.50 2 6.7 1.26 4.26 (,'/ -,()4~ 3 11.8 2.21 5.21 4 17.7 3.32 6.32 ·~·.t t?l/8 5 25.0 4.69 7.69 6 35.6 6.68 1<1'1 ,.. 9.68 .o~ 7 64.4 12.08 15.08 8 75.0 14.06 17.06 c,'-1 • ,o~.r 9 82.3 15.43 18.43 10 88.2 16.54 19.54 (,</ I tJ$2-- II 93.2 17.48 20.48 12 97.9 18.25 21.25 Averages: T s ___ _ LFiow ----- -iL'!P ----t'1P ___ _ KEY=> _ _jj_'{__ fidd 0 Jta She~• Plont D~Itl~on Mm~s Tt:i\'::t4 Tlln~ DGM -~P .o:\H ~H::IJ P~1Jnl Clock Min (0) ... •IIJt D~sired Aclual 1 1-:s3 0 JqL. I?JB rOSO • i? 1--.gz.. 2 z...o 3o3.5:J-tf .o'fe ·1-~ • ?-<j 3 40 3rS'". gof -0'18 .go ·80 4 {#0 ~Z-~. 2-(Q .osv . St{ ·8<( 5 go 3'-iD. 813 .osO , 8't • &'f 6 to-o 3'5 3 • .55"8 -OS~ .~<1 , 8"1 7 /'Vv ~ G 19 .i..Z-Co ,os~ -87 . €'t 8 ~'-(0 -;:t-9. t..?'tL/ ,fJ.S5 .qz_ qz__ 9_ ti.:IO ?l<t3.~~ ,o~o • !? .,;--~S 10 [~0 l.jOb·~.a -o£'3 ,'i(J ·7-o 11 U>C '-lt'i.)..'-1.0 Q)Q ·8s-85 12 '2-"tO :43Z... }~1--.Ds:o , g 5"' -85"' A 1 lt:5B .l-:..{f) 4 4 5. tr '-1 ·04) ,?-7 .:n 2 'J-~ 4~-'f-. '3~9 .O<f~ d2.. .&>'2.. 3 :tgb '-( "f-0. {) L(2, .o4.g .<g't ,g-z._ 4 ~00 '-1'82.. 1S& .cS8 I '?Cf .99 5 "JW 4. q 0. s<tCJ? .os~)' .'f<-( .Cit{ 6 '3'-10 z; tf>. oq~ os-5 . 9'lf . ?'-f 7 1/iQ 5'1.3-~tl .053 ,qo . '1-0 8 7:J<3'0 s 3(&.801 ,0'{~ • 8'-.82..- 9 t-too 5 qq. soS' 'o'ig < g 't--~2- 10 1.-fW 5(uL. 11.1 ,o~:; ,'i'l) ,q() 11 1./l.jD 575. 'l.O~ .0.$3 ,'1?) .q'O 12 l.f(/0 S'K& Lt 8(o ,()9) ,'07) ~~s- !5:53 '1g[) uo l. ;)._l..t L{ Totai Average TErCO Filter~f8J ___ Sampi<Box _£_ Locat1on: Griuly !3aghouse Op~rator: P.w! ]?_ K L-k..Re-n Y3C.:\1Utn T .:-m pcTJ.tures \ 1 1 .u, Stack (T,) Probe Prub.:Out Filter <t.o (,~ ,).<.j/ d(,(o ~~~0 'f.o (p~ -;)..{.,0 ;.:;.o 2S3 L(.o '.41-~ lP"' "}_[vo 2 !.{0 </.0 ~~ ).. '{ z._. ::Z.&t ).<;11 l..f.b Jo ~4 (p :U09 ).'{[3 4.o :f.'!, ;z.un ,v t-5<:) 250 <(.b 1'3 ;;. t{O ;l..Slf Z'!>S lf-o :r'{ ZSb 2-&b 2.-3" "--/.() f'Z.. .24.0 )ll5 l-30 Lf.o :;.&; Z.s-(a .2"( :;_'tO t..f.o 1-3 J,.-)'-1 J:s"B .2~2 '-f.v rs 2'il--2.-53 2.30 3.0 :n ).f-1 2-5'-{ 2..3D '-{.V ?'f Z£0 2-S(g z.:'l:. r '-j.O ~7 2•-d .Z'I"t 22~ 4.D t r ,;_:;-( ~'t J..t-IGP ~.0 i-'? P&r ;1v,) '2.38 t;.o +3 2..32-d-<-tF5 ;2.30 '(.0 .Jo ~-?JZ-Z.)L. Zl8 'f.o l.e+-1.2'-lO J..'-f~ "ZZ;I Lf.D &l ?..-SD &so 'Z.-'33 !.{O ~~ ?--(.;3 J..&3 I :Z<fo '-{.o 1-1 J~'=t 2S'6 )35" 'f.D 1'2---z.sg .?.'-6 ~~'1 DG~-1 T<mp (1 ,.,) Eftluent Oul In So &1-&.'f Ltg ::;z_ tl 5o n -8S" 53 n '82 '-'0 ~I 18? S'f-gz_ [Cj{ St &?3 <t3 57 fs-~Cf 5'8 ~& ~b tuo ~t '7b f~ () 71 IIOD (so Cfl f t}f) lP3 ~8 '73 Sl-JX7 't'-1 s-c 72-?8 So Cf l ~8 ::,3 8i 9(0 53 ~~ 90 53 g:r 9s 5'3 9.0 r1- S3 f?r 9-5: 53 Ys-!l_Z, 53 88 95' 5~ ~& qc.; Pag< ~~ _oi~l _ Run " __ L i N Stack Diam~l~r 1 8 7 5" Port Rt:lt:.n:ncc ___LQ::,_ Ports arc 24.5'' Upsu~am from nt:.Xl di~turbam:~ Ports .::!Te 48" Downstream from la~t di~lurbancc Assumed Mo1sture Probe S l ({ -'!J Cp 0.84 Nozzk Cali bratlrm ~ .!hl:Q_ -~ 1-'V .3 -=ro Avg D, ,Y{OO inches Gas Bag Amb1ent A1r C'onsok 5 __:<.__ Y-Fa~10r [.OC ( :c\H@ /. 't~ in H,O Baromli!tric Pr~:::surt!s Pb., _;;. • z._-o Pb0 ~'{.!'} Pr; _ __:-, 0 3_ L'•k ('hoc' Pre n'1min D .003 vacmt-l,) Z.{, 0 Potcl Ro" 0 .00 lr.H,O ,z..~ m Hg in H,g inH;O f2s Q .OO ( l.,..c Wat<r C'olkcled S'O.f-g Time Sampled_=-4......,$....:D;__ __ min Review f'K,'t< K ·- K~ North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Grizzly Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIXC c North Yellow Cake Dryer Scrubber METHOD 5 Date: Facility: Denison Mine -------- Stack Identification: NYC S.c v"J 4~c..fL TMPINGERS IMPINGERS IMPINGERS CJ<t:r""'- Sample Box: J3/ j Run: lmpinger Number· ·1 I 3 I 4 l 2.. (j -Initial Volume of liquid (H10 ) in imJlit\[:~rs. (ml) I 1oo I 1oo I Silica Gel Total (g) I I 'I • 0 ----···------··------- Run: L-Sample Box: lj / J Impinger Number 2 I ..L I ...!.I...i. Initial Volume of liquid (H20) in impinscrs, (ml) Silica Gel Final (gJ __._~_...!..-+..J-~.~~-t-i-:...3""'.)"---'. 0~, -+"'-'-'"-=;__-t=----"''-t__;_~,;_::~ Initial (gl ~"??.I ~-=-~~-~-r----;=~~-~~~--r-~~-- Net (g) :~!>~. ~ ====================================~~~ Total (g) 7 3 ~1-. L =========== --------- Run: Sample Box: llllpinger· N umber 1 .l...l..l..l...!.l 5 6 Initial Volume of llq,uitl (H!O) in i111pingors, ml) drop out I 1oo I too I Silica Gel I Final (g) ___ -+----+-----t----+----+------ Initial (g) ----+----t-----t-----i-----1----- Net (g) =====~============================= Total (g) ========= Run: Sample Box: Impinger Number .1. I ...L I ...!. I s 6 Initial Volume of liquid (H,O) in impingcr.;, (ml) drop out I too I too I Silica Gel I Final (g) ----+----t-----1-----i-----1----- Initial (g) ------+----~---;------+-----~----Net (g) =========================================== Total (g) ====== ------·-----·-----··---- ~ I ··._. l ~ II --;/' .. ;--_;.,.···if Date s-las-11! Test No.--'---- Gas Bag No. t5.-o§ "'> -""' A Ill h icnt Temp __,r:...,lc_:So<...-__ Operator (Jf._K, Date 5/ Z ft, /1 I Test No. '2. Gas Bag No. -l_,.,.__::o_?-;-- Arnbient Temp 1 B Operator M 5 M Date -----Test No. ____ _ Gas Bag No. -----Ambient Temp ____ _ Operator ----- Ga.~ co1 02 (Net is Actual 0 2 Reading Minus Actual C02 Reading). N2 (Net is I 00 Minus Actual 0 2 Reading). Gas C02 0 2 (Net is Actual 0 2 Reading Minus Actual C02 Reading). N2 (Net is I 00 Minus Actual 0 2 Reading). Ga.~ 0 2 (Net is Actual 02 Reading Minus Actual C01 Reading). N2 (Net is 100 Minus Actual 0 2 Reading). Actual Rrading z.co l''\o'2. ~jj: ~~~; I ~ " Actual Reatliug ~.fb 'ZO· "t ''•"' ;· Mx.:!ol_ 1-~4rll Arlual Reading I I RUN 2 i'lirt Actual Net Re.atling z. e 2.8 z.s l<o.l{ 1'{,1... llDA e". e, ;~1~ 80·8 ·-'A"~?'/1'/F,Cl RUN 2 i'liet Actual Net Reading ~-6 :).8 3.8 J(o.(o I.o.'-\ l~·(. 1'1.1o ~1~1:~~-"1lf. b ' • RUN 2 Net Actual "•t Re•ding C'O is nul measured. as il has the same molecular wetght as N1 3 Actulll Read in~ z.e lq.z.... 1'(\j,·;•;\~·~( ~ '-~-~ ... * ~ l d~" 3 Actual Reading 3.8 2o.'-\ -· ~ !t :*~~(i ·-~· ~ .:7-i~·{~~ Actual Reading 3 Net z.e llo,~ 8o.e Net 3·B \ b." {q.0 i\cl Avcrag;l' Net Volurnc 2,B ( ~ .t.l f)o.£3 Average Net Volume 3.9 \to,~ 79. h Average Net Volume Yellow Cake Dryer Baghouse Dryer Baghouse Facility: Denison Mines Date: S /:J.=i-/11 Stack Identitication: Yellow Cake Dryer Bughouse IMPINGERS Filter Number: ij'N;,q IMPINGERS Filter Number: IMPJNGERS Filter Number: Final (g) Initial (g) Net(g) Run: I Sample Box: I? lmpingcr Numbe r ..L I ..i.. I s .!.. I -2 Initial Volume nrliquid (Hl()) in imf!ill!:~rs, (mil I 00 I 00 I I SG I I ' 1 ' ' . t-o c;. o 03t.! .IP &N ·S"" q43. z.. 1 ol, l. c Z.B~b G ('?>. t cr z:p 'l ..... 3, (tJ c,.o /.'I "ll . .;- Total (gl===Z::::::<e~·~3~== Run: Sample Box: liupingcr Number ~ I 3 I .1-I ~ Initial Volume ofliquid (HPJ in i111pingcrs. (ml) I 00 1 00 I I SG I Final (g) -----+----+----+----+-----1----- lnitial (gl ___ --+----1------+-----1-----1----- Nel (g) ======~====~====~====~====db===== Total (g)======== Run: Sample Box: lmpinger Number 3 I ..!!-I 5 -2 -Initial Volume of liquid (Hl()) in imping~rs. (ml) I 00 I 00 I I SG I Final (g) ----~----+---~---+----+------- lnitial (g) ------4------+---~---+----+----- Net (g)===:::=!===::::!:===:!:::===:::!:::===='==== Total (g) ====== Grizzly Baghouse NYC Baghuus-e M5 Facility: Denison Mines Date: ------------ Stack Identification: ~en=4-!~~--'l..:.::Z-::..~_)+Y------------- - -G R' IMPINGERS IMPINGERS Final (g) Initial (g) Net(g) Run: ( Sample Box: E IFF ..L Impinge•· Number ...L I..:LI..2.. _£_ Initial Volume of liquid (H20) in im1>ingcrs, (ml) I 00 1 00 I I Silica Gel I I ~ I . ' . {,~f.;) I !o lJ.C/ ("I 'f_(i!) lq 90 -tO 70 7.0 IC£ tflt'. I ~o&f. I 91../o.q -Z.t.$ '~-0 ~-' qe;, ~ Total (gl -5D-r ====::::!:==== Run : Sample Box: lmpmge•· Number I -..1. I ..1... I 4 I ~ lr1itial Volume oflitiUid (H20) in impingcrs, (ml) I 00 l 00 I I Silica Gel I Final (g) -----11-----l----~----+----+---­ Initial (g) -----1,....._----l----+----+----+---- Net (g) =====b=====b=====b=====~==~======= Run: ..L Total (g) ==~===== Sample Box: Impinge•· Numbe1· ,]__ I 3 I ...!. I -.L Initial Volume of lrqu id (H~O) in irnpingers, (rnl) 100 100 I J Silica Gel I 6 Final (gl ____ ,__ __ --11------4----1----1---- Initial (g) ____ ,__ __ --lf-------i----1----1---- Net (g) ======~==========~===========k===== IMPINGERS Run: Sample Box: Impinge•· Number 1 -..l..l--1-l 4 I..L Initial Volume ofliqu itl (11.0) in in111ingcrs, (ml) I 00 I 00 I I Silica Gel I Final (g) _____ l------t'"----1----1--------1.---- Initial (g) ----f-------t'-------+----1----1---- Nct (g) ======~==========~====~=====k===== Total (g) ====== Chain of Custody Record Temperature on Receipt ---Test America Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TES'fJNG TAL-4124 (1007) Cliem Proieot Meno.aer oa:c C!Jain of Cusfadr Number Tetco Dean Kitchen 5/31/2011 --Address -i8!Sphone Numb6r V\f9i! Cooo)/Fax Mmi!:Jcr I.AbNumiJ~r 391 East 620 South 801-492.-9106 Page of Cit}· l~a; IZ:4~3 ---Site Contact. Lab Cor.ta<:~ Analysis (Attach lisz if American Fork Scott Chrinensc:n,R'I'&" P11lmer mora spac9 16 needed) Praiect N1>me u.d LOCIJti<m fS:St!!l Camer/WaytJe/ Nw 1ber Denison Mine 2011 2nd Quarter Special Instructions/ i...'ontract/Pvrcna~e 0rtk;rf01.."0to Na. Container.; 8 Conditions of Receipt Matrix Preservatives 0 "' s 10 1 "' "' ~ ---~ , "'0 Sample I. D. No. and DescriptiOn l ~ ~ 0 z .. Date Time ~ ~ ~~ ::, ::z: .. ~ (Coma/nets tor osch sampto may b~ combinB<i on ona line) .~ ~ -g ~ ~ ~ 2 <: ~~ '""' "' <( "' 5785 Rl Grizzly filter and beaker 5/24/11 i 8:00 X x'f<. I j . ---"' 'r.. 5784, 5786 Rl NYC filters and beaker 5/25/11 ! 8:00 X I " 'f.. 5770, 5771 R2 NYC fi lters and beaker 5/26/11 8:00 X I '1'1 X X X 5769 Bag house Filter and beaker 5/27/11 8:00 X ! X, " KA I -- -. I . I I I ' I ! ~· -· l I ·-· I l'o$sible 1·/szard /dc(;tlf.clltion lflllllP~~sal (A fee msy be ass~d r. fJ131YlP/es aJe rs~inEd 0 Non-Hazard 0 Flammeb.'e 0 SiM ll'liWnt 0 Po/S".At 9 0 Un&llDWTI 0 Relum To Client D Disp0681 By LaiJ 0 Ardrive Far ___ hfDnths /oo;JBIIh;m 1 manf/1) ilnn Around 1 m11 Rsqufrvi! . 0 24 Houts 0 48 Hou"' 0 7 Days 0 74 Days 0 21 Days Time 2. 1 Timo a.~By 1 71me Commenrs When Complete Email to: Dean or Paul tetco@tetco·ut.com liiSTRIB(ffibN: WriiTe • Rillumed o detii.Wif: F!ttpatt· CANAi'IY-S:..ys wllll rr.e Swnp/11; FJNf( • F'~lrt <;r.,py SDGNo. Order No. 43264 TestAmerlca rptSTLRchTitle v3.73 TestAmerica Laboratories, Inc. Analytical Data Package Prepared For Denison Mines (USA) Corp. Denison Mine 20112nd Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 19 Pages Report No.: 47442 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID ------------~ ---------5769 BAGHOUSE FILTER J1 F080456-4 MJ3XW1AA 9MJ3XW10 & BEAKER 5769 BAG HOUSE FILTER J1 F080456-4 MJ3XW1AE 9MJ3XW10 & BEAKER 5769 BAGHOUSE FILTER J1 F080456-4 MJ3XW1AC 9MJ3XW10 & BEAKER 5769 BAG HOUSE FILTER J1 F080456-4 MJ3XW1AD 9MJ3XW10 & BEAKER 5770, 5771 R2 NYC J1 F080456-3 MJ3XQ1AA 9MJ3XQ10 FILTERS & BE 5770, 5771 R2 NYC J1 F080456-3 MJ3XQ1AE 9MJ3XQ10 FILTERS & BE 5770, 5771 R2 NYC J1 F080456-3 MJ3XQ1AC 9MJ3XQ10 FILTERS & BE 5770, 5771 R2 NYC J1 F080456-3 MJ3XQ1AD 9MJ3XQ10 FILTERS& BE 5784, 5786 R1 NYC J1 F080456-2 MJ3XM1AA 9MJ3XM10 FILTERS & BE 5784, 5786 R1 NYC J1 F080456-2 MJ3XM1AE 9MJ3XM10 FILTERS & BE 5784, 5786 R1 NYC J1 F080456-2 MJ3XM1AC 9MJ3XM10 FILTERS& BE 5784, 5786 R1 NYC J1 F080456-2 MJ3XM1AD 9MJ3XM10 FILTERS & BE 5785 R1 GRIZZLY FILTER J1 F080456-1 MJ3XF1AA 9MJ3XF10 & BEAKE 5785 R1 GRIZZLY FILTER J1 F080456-1 MJ3XF1AC 9MJ3XF10 &BEAKE Batch No. 1161154 1161156 1161158 1161160 1161154 1161156 1161158 1161160 1161154 1161156 1161158 1161160 1161154 1161156 Test America THE LEADER IN ENVIRONMENTAL TESTING Certificate of Analysis July 15, 2011 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction June 3, 2011 Denison Mine 2011 1st Quarter Four (4) Stack Filter Samples 43264 CASE NARRATIVE On June 3, 2011, four stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers JIF080456. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: TestAmerica Laboratories, Inc. Alpha Spectroscopy Thorium-228, -230, -232 by method RL-ALP-001 Uranium-234, -235, -238 by method RL-ALP-004 Gamma Spectroscopy Pb-210 by method RL-GA-001 Alpha Scintillation Radium-226 by method RL-RA-001 2 Denison Mines (USA) Corp July 15, 2011 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments'' section. V. Comments Alpha Spectroscopy Thorium-228, 230, 232 The achieved MDA of the samples exceeds the detection limit. However, in most cases, the activity of the samples exceeds the MDA and detection limit. The data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Uranium-234, 235, 238 The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA and detection limit for three of the four samples. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Gamma Spectroscopy Pb-210 The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. The LCS recovery yield is just above acceptance limits. There is no sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Alpha Scintillation Radium-226 The achieved MDA exceeds the detection limit due to sample volume available for analysis. Sample activity exceeds MDA and detection limit for all of the samples. Data is accepted. Except as noted, the LCS, batch blank and sample results are within acceptance limits. I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan Customer Service Manager TestAmerica Laboratories, Inc. 3 Drinking Water Method Cross References DRINKING WATERASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) TestAmerica Richland's SOP N EPA 901.1 Cs-134, 1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM D5174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R =constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (u;) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. UnceJiainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S/? n), where S is the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation of the general "Law of Propagation of Errors" equations and specific example are available on request. TestAmerica rptGenerallnfo v3.72 TestAmerica Laboratories, Inc. 4 o. 1""""'7'"-.--:--------:---.,----.---:--:;--,,--:Rc..:.e=,.,~ort Definitions Action Lev An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. Batch Bias COCNo Count Error (#s) Total Uncert (#s) u, _Combined U11certainty. (#s), Coverage Factor CRDL(RL) Lc Lot-Sample No MDCJMDA Primary Detector Ratio U-234/U-238 Rst/MDC Rst/TotUcert Report DB No RER SDG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmerica The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by the equation (Result/Expected)-! as defined by ANSI N 13.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, uc the combined uncertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width of the confidence interval, I, 2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica ·'defaulf' nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=( 1.645 * Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) * (ConvFcti(Eff"'Yld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume with a Type I and n error probability of approximately 5%. MDC = ( 4.65 * Sqrt((BkgrndCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn *Vol)* IngrFct). For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321 Cis 1.038. Ratio of the Result to the MDC. A value greater than I may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than 1 may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order Number. The equation Replicate Error Ratio= (S-D)/[sqrt(TPUs2+ TPUd2)] as defined by !CPT BOA where Sis the original sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results are in the same units. The LIMS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. rptGenerallnro v3.72 TestAmerica Laboratories, Inc. 5 Sample Results Summary Date: 15-Jul-11 TestAmerica Ordered by Method, Batch No., Client Sample ID. Report No.: 47442 SDG No: 43264 Client ld Tracer MDC or Batch Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield MDA CRDL RER2 1161154 RICHRC5011 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AA TH-228 1.68E-07 +-4.9E-08 UCI/SA 108% 1.84E-08 TH-230 3.87E-05 +-6.0E-06 UCI/SA 108% 1.78E-08 3.00E-15 TH-232 4.02E-07 +-8.8E-08 UCI/SA 108% 1.78E-08 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AA TH-228 6.59E-08 +-3.5E-08 UCI/SA 69% 2.85E-08 TH-230 1.31 E-05 +-2.1 E-06 UCI/SA 69% 2.76E-08 3.00E-15 TH-232 1.35E-07 +-S.OE-08 UCI/SA 69% 2.76E-08 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AA TH-228 4.14E-08 +-2.8E-08 UCI/SA 68% 2.77E-08 TH-230 1.15E-05 +-1.9E-06 UCI/SA 68% 2.68E-08 3.00E-15 TH-232 1.46E-07 +-5.3E-08 UCI/SA 68% 2.68E-08 5785 R1 GRIZZLY FILTER & BEAKE MJ3XF1AA TH-228 3.06E-09 +-2.2E-08 u UCI/SA 64% 4.31E-08 TH-230 6.85E-07 +-1.4E-07 UCI/SA 64% 3.18E-08 3.00E-15 TH-232 5.61 E-08 +-2.8E-08 UCI/SA 64% 2.17E-08 1161156 FFSR 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AE U-234 8.56E-03 +-2.0E-03 UCI/SA 91% 3.73E-05 9.00E-15 U-235 2.44E-04 +-9.7E-05 UCI/SA 91% 3.16E-05 9.00E-15 U-238 8.32E-03 +-1.9E-03 UCI/SA 91% 4.53E-05 9.00E-15 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AE U-234 4.75E-02 +-1.0E-02 UCI!SA 83% 1.40E-04 9.00E-15 U-235 2.42E-03 +-7.1 E-04 UCI/SA 83% 9.99E-05 9.00E-15 U-238 4.69E-02 +-9.9E-03 UCI/SA 83% 1.45E-04 9.00E-15 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AE U-234 5.65E-02 +-1.3E-02 UCI/SA 76% 2.21E-04 9.00E-15 U-235 3.37E-03 +-9.7E-04 UCI/SA 76% 1.46E-04 9.00E-15 U-238 5.65E-02 +-1.3E-02 UCI/SA 76% 2.44E-04 9.00E-15 5785 R1 GRIZZLY FILTER & BEAKE MJ3XF1AC U-234 3.32E-05 +-3.8E-05 u UCI/SA 107% 6.71E-05 9.00E-15 U-235 1.41 E-05 +-2.7E-05 u UCI/SA 107% 5.72E-05 9.00E-15 U-238 1.92E-05 +-3.6E-05 u UCI/SA 107% 7.68E-05 9.00E-15 1161160 RICHRC5011 TestAmerica RER2 -Replicate Error Ratio= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))[ as defmed by ICPT BOA. rptSTLRchSaSum U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda!Mdl, Total Uncert, CRDL, RDL or mary2 V5.2.15 not identified by gamma scan software. A2002 TestAmerica Laboratories, Inc. 6 Report No. : 47442 Client ld Batch Work Order Parameter 1161160 RICHRC5011 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AD Pb-210 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AD Pb-210 5784, 5786 R1 NYC FILTERS & BE MJ3XM1AD Pb-210 1161158 RL-RA-001 5769 BAG HOUSE FILTER & BEAKER MJ3XW1AC RA-226 5770, 5771 R2 NYC FILTERS & BE MJ3XQ1AC RA-226 5784, 5786 R1 NYC FILTERS & BE MJ3XM1 AC RA-226 No. of Results: 30 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample ID. Result+-Uncertainty ( 2s) Qual Units 1.66E-06 +-4.8E-07 UCI/SA 4.99E-05 +-8.4E-06 UCI!SA 4.98E-05 +-8.4E-06 UCI!SA 3.91 E-07 +-8.9E-08 3.01 E-07 +-7.9E-08 2.78E-07 +-7.2E-08 Date: 15-Jul-11 SDG No: 43264 Tracer MDC or Yield MDA CRDL RER2 69% 5.89E-07 6.00E-14 79% 5.15E-07 6.00E-14 83% 4.59E-07 6.00E-14 100% 2.70E-08 9.00E-14 77% 6.78E-08 9.00E-14 69% 4.78E-08 9.00E-14 TestAmerica rptSTLRchSaSum mary2 V5.2.15 A2002 RER2 -Replicate Error Ratio= (S-D)/Isqrt(sq(TPUs)+sq(TPUd))J as defmed by ICPT BOA. TestAmerica Laboratories, Inc. 7 QC Results Summary Date: 15-Jul-11 TestAmerica Ordered by Method, Batch No, QC Type,. Report No. : 47442 SDG No.: 43264 Batch Tracer LCS Work Order Parameter Result +-Uncertainty ( 2s) Qual Units Yield Recovery Bias MDCIMDA RICHRC5011 1161154 BLANK QC, MJ56F1AA TH-228 7.05E-09 +-1.2E-08 u UCI/SA 86% 2.18E-08 TH-230 6.58E-08 +-2.8E-08 UCI/SA 86% 2.11 E-08 TH-232 2.72E-08 +-1.7E-08 UCI/SA 86% 1.67E-08 1161154 LCS, MJ56F1AC TH-230 1.97E-06 +-3.4E-07 J UCI/SA 60% 86% -0.1 2.66E-08 FFSR 1161156 BLANK QC, MJ56H1AA U-234 O.OOE+OO +-S.OE-08 u UCI/SA 93% 1.17E-07 U-235 -4.87E-09 +-S.OE-08 u UCI/SA 93% 1.17E-07 U-238 9.73E-08 +-9.9E-08 u UCI/SA 93% 1.17E-07 1161156 LCS, MJ56H1AC U-234 3.37E-06 +-7.9E-07 UCI/SA 89% 93% -0.1 1.21 E-07 U-238 3.88E-06 +-8.7E-07 UCI/SA 89% 102% 0.0 1.21 E-07 RICHRC5011 1161160 BLANK QC, MJ56M1AA Pb-210 3.04E-07 +-3.2E-07 u UCI/SA 76% 5.48E-07 1161160 LCS, MJ56M2AC Pb-210 1.15E-05 +-2.0E-06 UCI/SA 79% 127% 0.3 4.63E-07 RL-RA-001 1161158 BLANK QC, MJ56J1AA RA-226 1.32E-08 +-2.8E-08 u 83% 4.74E-08 1161158 LCS, MJ56J1AC RA-226 9.07E-06 +-2.1E-06 J 100% 91% -0.1 4.18E-08 No. of Results: 13 Bias -(Result/Expected)-I as defined by ANSI Nl3.30. TestAmerica rptSTLRchQcSum mary V5.2.15 A2002 J Qual-No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda!Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 8 FORM I Date: 15-Jul-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/27/2011 8:00:00 AM Lot-Sample No.: J1 F080456-4 Report No.: 47442 Received Date: 6/3/2011 11:00:00 AM Client Sample ID: 5769 BAGHOUSE FILTER & BEAKER COC No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered b~ Client Sample ID, Batch No. Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstiTotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XW1AA Report DB ID: 9MJ3XW10 TH-228 1.68E-07 4.2E-08 4.9E-08 1.84E-08 UCI/SA 108% (9.1) 6/27/11 10:47 p 1.0 0.99001 ALP175 5.82E-09 (6.8) Sample Sample TH-230 3.87E-05 6.1 E-07 6.0E-06 1.78E-08 UCI/SA 108% (2169.7) 6/27/11 10:47 p 1.0 0.99001 ALP175 5.64E-09 3.00E-15 (12.8) Sample Sample TH-232 4.02E-07 6.3E-08 8.8E-08 1.78E-08 UCI/SA 108% (22.6) 6/27/11 10:47 p 1.0 0.99001 ALP175 5.64E-09 (9.1) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XW1AE Report DB ID: 9MJ3XW10 U-234 8.56E-03 4.8E-04 2.0E-03 3.73E-05 UCI/SA 91% (229.6) 6/16/11 06:37 p 1.0 0.00103 ALP? 9.71E-06 9.00E-15 (8.8) Sample Sample U-235 2.44E-04 B.OE-05 9.7E-05 3.16E-05 UCI/SA 91% (7. 7) 6/16/11 06:37 p 1.0 0.00103 ALP? 6.87E-06 9.00E-15 (5.) Sample Sample U-238 8.32E-03 4.7E-04 1.9E-03 4.53E-05 UCI/SA 91% (183.4) 6/16/11 06:37 p 1.0 0.00103 ALP? 1.37E-05 9.00E-15 (8.8) Sample Sample Ratio U-234/238 = 1.0 Batch: 1161158 RL-RA-001 Work Order: MJ3XW1AC Report DB ID: 9MJ3XW10 RA-226 3.91 E-07 4.0E-08 8.9E-08 2.70E-08 100% (14.5) 7/7/11 05:32 p 1.0 0.99 ASCJMB 1.23E-08 9.00E-14 (8.8) Sample Sample Batch: 1161160 RICHRC5011 Work Order: MJ3XW1AD Report DB ID: 9MJ3XW10 Pb-21 0 1.66E-06 3.9E-07 4.8E-07 5.89E-07 UCI/SA 69% (2.8) 7/7/11 06:38 a 1.0 0.99001 GPC31D 2.87E-07 6.00E-14 (6.9) Sample Sample TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 9 Lab Name: TestAmerica Lot-Sample No.: J1 F080456-4 FORM I SAMPLE RESULTS Client Sample ID: 5769 BAGHOUSE FILTER & BEAKER Denison Mine 2011 2nd Quarter SDG: 43264 Report No.: 47442 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst!TotUcert No. of Results: 8 Comments: Date: 15-J ul-11 Collection Date: 5/27/2011 8:00:00 AM Received Date: 6/3/2011 11:00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample 10, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 10 FORM I Date: 15-Jul-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/26/2011 8:00:00 AM Lot-Sample No.: J1F080456-3 Report No.: 47442 Received Date: 6/3/2011 11:00:00 AM Client Sample ID: 5770, 5771 R2 NYC FILTERS & BE COC No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered bl Client Sample I D. Batch No. Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XQ1AA Report DB ID: 9MJ3XQ10 TH-228 6.59E-08 3.3E-08 3.SE-08 2.8SE-08 UCI/SA 69% (2.3) 6/27/1110:47p 1.0 0.98995 ALP174 9.02E-09 (3.8) Sample Sample TH-230 1.31E-05 4.4E-07 2.1 E-06 2.76E-08 UCI/SA 69% (472.4) 6/27/1110:47 p 1.0 0.98995 ALP174 8.73E-09 3.00E-1S (12.4) Sample Sample TH-232 1.35E-07 4.6E-08 S.OE-08 2.76E-08 UCI/SA 69% (4.9) 6/27/11 10:47 p 1.0 0.98995 ALP174 8.73E-09 (5.4) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XQ1AE Report DB ID: 9MJ3XQ10 U-234 4.75E-02 2.2E-03 1.0E-02 1.40E-04 UCI/SA 83% (338.8) 6/16/11 OS:21 p 1.0 0.00101 ALPS 3.40E-OS 9.00E-1S (9.5) Sample Sample U-235 2.42E-03 S.1 E-04 7.1 E-04 9.99E-OS UCI/SA 83% (24.3) 6/16/11 OS:21 p 1.0 0.00101 ALPS 1.39E-OS 9.00E-1S (6.8) Sample Sample U-238 4.69E-02 2.2E-03 9.9E-03 1.4SE-04 UCI/SA 83% (322.7) 6/16/11 OS:21 p 1.0 0.00101 ALPS 3.67E-OS 9.00E-1S (9.5) Sample Sample Ratio U-2341238 = 1.0 Batch: 1161158 RL-RA-001 Work Order: MJ3XQ1AC Report DB ID: 9MJ3XQ10 RA-226 3.01E-07 S.4E-08 7.9E-08 6.78E-08 77% (4.4) 7/7/11 OS:31 p 1.0 0.99 ASC2HA 3.24E-08 9.00E-14 (7.6) Sample Sample Batch: 1161160 RICHRC5011 Work Order: MJ3XQ1AD Report DB ID: 9MJ3XQ10 Pb-21 0 4.99E-05 1.0E-06 8.4E-06 S.1SE-07 UCI/SA 79% (96.9) 7/7/11 06:38 a 1.0 0.98995 GPC31C 2.S1 E-07 6.00E-14 (11.9) Sample Sample TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. VS.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 11 Lab Name: TestAmerica Lot-Sample No.: J1 F080456-3 FORM I SAMPLE RESULTS Client Sample ID: 5770,5771 R2 NYC FILTERS & BE Denison Mine 2011 2nd Quarter SDG: 43264 Report No.: 47442 COC No.: Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert No. of Results: 8 Comments: Date: 15-Jul-11 Collection Date: 5/26/2011 8:00:00 AM Received Date: 6/3/2011 11:00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample ID, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 12 FORM I Date: 15-Jul-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/25/2011 8:00:00 AM Lot-Sample No.: J1 F080456-2 Report No.: 47442 Received Date: 6/3/2011 11:00:00 AM Client Sample ID: 5784, 5786 R1 NYC FILTERS & BE COC No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered by Client Sample ID, Batch No. Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL{RL) Rst/TotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XM1AA Report DB ID: 9MJ3XM10 TH-228 4.14E-08 2.7E-08 2.8E-08 2.77E-08 UCI/SA 68% (1.5) 6/27/11 10:47 p 1.0 0.99003 ALP173 8.76E-09 (3.) Sample Sample TH-230 1.15E-05 4.1 E-07 1.9E-06 2.68E-08 UCI/SA 68% (428.3) 6/27/11 10:47 p 1.0 0.99003 ALP173 8.48E-09 3.00E-15 (12.4) Sample Sample TH-232 1.46E-07 4.7E-08 5.3E-08 2.68E-08 UCI/SA 68% (5.4) 6/27/11 10:47 p 1.0 0.99003 ALP173 8.48E-09 (5.6) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XM1AE Report DB ID: 9MJ3XM10 U-234 5.65E-02 2.6E-03 1.3E-02 2.21 E-04 UCI/SA 76% (256.3) 6/16/11 05:21 p 1.0 0.00104 ALP4 6.91E-05 9.00E-15 (9.) Sample Sample U-235 3.37E-03 6.4E-04 9.7E-04 1.46E-04 UCI/SA 76% (23.1) 6/16/11 05:21 p 1.0 0.00104 ALP4 3.17E-05 9.00E-15 (6.9) Sample Sample U-238 5.65E-02 2.6E-03 1.3E-02 2.44E-04 UCI/SA 76% (231.8) 6/16/11 05:21 p 1.0 0.00104 ALP4 8.08E-05 9.00E-15 (9.) Sample Sample Ratio U-2341238 = 1.0 Batch: 1161158 RL-RA-001 Work Order: MJ3XM1AC Report DB ID: 9MJ3XM10 RA-226 2.78E-07 4.6E-08 7.2E-08 4.78E-08 69% (5.8) 7/7/11 05:34 p 1.0 0.99 ASC1MB 2.22E-08 9.00E-14 (7.8) Sample Sample Batch: 1161160 RICHRC5011 Work Order: MJ3XM1AD Report DB ID: 9MJ3XM10 Pb-210 4.98E-05 1.0E-06 8.4E-06 4.59E-07 UCI/SA 83% (108.6) 7/7/11 06:38 a 1.0 0.99003 GPC31B 2.23E-07 6.00E-14 (11.9) Sample Sample TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 13 Lab Name: TestAmerica Lot-Sample No.: J1 F080456-2 FORM I SAMPLE RESULTS Client Sample ID: 5784, 5786 R1 NYC FILTERS & BE Denison Mine 2011 2nd Quarter SDG: 43264 Report No.: 47442 CCC No.: Result Count Total MDC(MDA, Rpt Unit, Yield Rst/MDC, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert No. of Results: 8 Comments: Date: 15-Jul-11 Collection Date: 5/25/2011 8:00:00 AM Received Date: 6/3/2011 11:00:00 AM Matrix: Analysis, Prep Date AIR FILTER Ordered by Client Sample I D. Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDC(MDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual-No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 14 FORM I Date: 15-Jul-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 43264 Collection Date: 5/24/2011 8:00:00 AM Lot-Sample No.: J1 F080456-1 Report No.: 47442 Received Date: 6/3/2011 11:00:00 AM Client Sample ID: 5785 R1 GRIZZLY FILTER & BEAKE COC No.: Matrix: AIR FILTER Denison Mine 2011 2nd Quarter Ordered bl Client Sample 10, Batch No. Result Count Total MDCIMDA, Rpt Unit, Yield Rst/MDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 1161154 RICHRC5011 Work Order: MJ3XF1AA Report DB ID: 9MJ3XF10 TH-228 3.06E-09 u 2.2E-08 2.2E-08 4.31 E-08 UCI/SA 64% 0.07 6/27/11 10:47 p 1.0 0.98932 ALP171 1.74E-08 0.28 Sample Sample TH-230 6.85E-07 9.1 E-08 1.4E-07 3.18E-08 UCI/SA 64% (21.6) 6/27/11 10:47 p 1.0 0.98932 ALP171 1.19E-08 3.00E-15 (9.8) Sample Sample TH-232 5.61E-08 2.7E-08 2.8E-08 2.17E-08 UCI/SA 64% (2.6) 6/27/11 10:47 p 1.0 0.98932 ALP171 6.87E-09 (4.) Sample Sample Batch: 1161156 FFSR Work Order: MJ3XF1AC Report DB ID: 9MJ3XF10 U-234 3.32E-05 u 3.7E-05 3.8E-05 6.71 E-05 UCI/SA 107% 0.5 6/16/11 06:36 p 1.0 0.00095 ALP3 2.49E-05 9.00E-15 (1.8) Sample Sample U-235 1.41 E-05 u 2.7E-05 2.7E-05 5.72E-05 UCI/SA 107% 0.25 6/16/11 06:36 p 1.0 0.00095 ALP3 2.00E-05 9.00E-15 (1.) Sample Sample U-238 1.92E-05 u 3.6E-05 3.6E-05 7.68E-05 UCI/SA 107% 0.25 6/16/11 06:36 p 1.0 0.00095 ALP3 2.97E-05 9.00E-15 (1.1) Sample Sample Ratio U-234/238 = 1.7 No. of Results: 6 Comments: TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No Ul< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.15 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 15 FORM II Date: 15-Jul-11 BLANK RESULTS Lab Name: TestAmerica SDG: 43264 Matrix: AIR Report No.: 47442 Count Total MDCIMDA, Rpt Unit, Rst/MDC, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield Rst/TotUcert Prep Date Size Size Detector Batch: 1161160 RICHRC5011 Work Order: MJ56M1AA Report DB ID: MJ56M1AB Pb-210 3.04E-07 u 3.2E-07 3.2E-07 5.48E-07 UCI/SA 76% 0.56 7/7/11 06:38 a 1.0 1.0 GPC32A 2.67E-07 6.00E-14 (1 .9) Sample Sample Batch: 1161158 RL-RA-001 Work Order: MJ56J1AA Report DB ID: MJ56J1AB RA-226 1.32E-08 u 2.8E-08 2.8E-08 4.74E-08 83% 0.28 7/7/11 05:31 p 1.0 1.0 ASCKMF 2.23E-08 9.00E-14 0.94 Sample Sample Batch: 1161156 FFSR Work Order: MJ56H1AA Report DB ID: MJ56H1AB U-234 O.OOE+OO u O.OE+OO 5.0E-08 1.17E-07 UCI/SA 93% 0. 6/16/11 06:38 p 1.0 0.25 ALP9 2.53E-08 9.00E-15 0. Sample Sample U-235 -4.87E-09 u 5.0E-08 5.0E-08 1.17E-07 UCI/SA 93% -0.04 6/16/11 06:38 p 1.0 0.25 ALP9 2.53E-08 9.00E-15 -0.2 Sample Sample U-238 9.73E-08 u 9.8E-08 9.9E-08 1.17E-07 UCI/SA 93% 0.84 6/16/11 06:38 p 1.0 0.25 ALP9 2.53E-08 9.00E-15 (2.) Sample Sample Batch: 1161154 RICHRC5011 Work Order: MJ56F1AA Report DB ID: MJ56F1AB TH-228 7.05E-09 u 1.2E-08 1.2E-08 2.18E-08 UCI/SA 86% 0.32 6/27/1110:47p 1.0 1.0 ALP176 7.73E-09 (1 .1) Sample Sample TH-230 6.58E-08 2.6E-08 2.8E-08 2.11 E-08 UCI/SA 86% (3.1) 6/27/11 10:47 p 1.0 1.0 ALP176 7.47E-09 3.00E-15 (4.7) Sample Sample TH-232 2.72E-08 1.7E-08 1.7E-08 1.67E-08 UCI/SA 86% (1 .6) 6/27/11 10:47 p 1.0 1.0 ALP176 5.28E-09 (3.1) Sample Sample No. of Results: 8 Comments: TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBiank V5.2.15 A2002 U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 16 Lab Name: TestAmerica Matrix: AIR Count Parameter Result Qual Error ( 2 s) Batch: 1161160 RICHRC5011 Pb-210 1.15E-05 5.4E-07 Batch: 1161158 RL-RA-001 RA-226 9.07E-06 1.7E-07 Batch: 1161 156 FFSR U-234 3.37E-06 5.8E-07 U-238 3.88E-06 6.3E-07 Batch: 1161154 RICHRC5011 TH-230 1.97E-06 1.5E-07 No. of Results: 5 Comments: FORM II LCS RESULTS Total Report Expected Uncert(2 s) MDCIMDA Unit Yield Expected Uncert Work Order: MJ56M2AC Report DB ID: MJ56M2CS 2.0E-06 4.63E-07 UCI/SA 79% 9.07E-06 1.52E-07 Rec Limits: 20 115 Work Order: MJ56J1AC Report DB ID: MJ56J1CS 2.1 E-06 4.18E-08 100% 9.95E-06 1.01 E-07 Rec Limits: 70 130 Work Order: MJ56H1AC Report DB ID: MJ56H1CS 7.9E-07 1.21E-07 UCI/SA 89% 3.64E-06 1.13E-07 Rec Limits: 70 130 8.7E-07 1.21E-07 UCI/SA 89% 3.81 E-06 1.18E-07 Rec Limits: 70 130 Work Order: MJ56F1AC Report DB ID: MJ56F1CS 3.4E-07 2.66E-08 UCI/SA 60% 2.28E-06 4.63E-08 Rec Limits: 70 130 TestAmerica rptSTLRchlcs V5.2.15 A2002 Bias -(Result!Expected)-1 as defined by ANSI Nl3.30. TestAmerica Laboratories, Inc. 17 Date: 15-J ul-11 SDG: 43264 Report No.: 47442 Recovery, Analysis, Aliquot Primary Bias Prep Date Size Detector 127% 7/8/11 07:51 a 1.0 GPC31B 0.3 Sample 91% 7/7/11 05:32 p 1.0 ASCPMD -0.1 Sample 93% 6/16/11 06:38 p 0.27 ALP10 -0.1 Sample 102% 6/16/11 06:38 p 0.27 ALP10 0.0 Sample 86% 6/27/11 10:47 p 1.0 ALP177 -0.1 Sample 00 . .. . :··~;.: .. -~·~~~- Chain of Custody Record Cileor Tetco Address 391 East 620 South Cily -I State l Z!D Code American Fork .Ut "84003 Ptoi~ct N4.7le er.d l.cc1Won fSEful Denison Mine 2011 2nd Quarter Comm:t!Purc/loSC Cr.JertQuoic No. ---Sample I.D. No. 2nd oeseriprlon Date (Coma/nets for e2oh s:ampl~> may /:19 c;ombinl>d on an9 flnil) 5785 Rl Grizzly filter and beaker 5/24/11 -. - 5784, 5786 Rl NYC filters and beaker 5/25/11 5770, 5771_ ~2 NYC filters and b~aker i 5/26/11 ---·----- 5769 Saghouse Filter and beaker 5/27/11 - (\)lA~. ~ -·~~-;!1-:.r- ~Oblk LJ~"'/ LOt d} ;:T/PWDLl~ IQ ./',y}fj{-\'! '-::t I ( o/JL ,;M~DFJJ - - - Tem:::>erature on Receipt __ _ Test America Drin.'<ing Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING ProF-tX Mantt~;er Da:~ Ch6in of Cuslccl\• rtutr.bet. Dean Kitchen . 5/3112011 I I To.Jephone Num!Jer tArea Cl>CG)J.=a.~ Mim':>al UlbNrmwer 1801-492-9106 . Page of -Site Con!'!ICC Lab Corrtac:r AP.afy&is (Ariach lisJ if S(ott Chri.stl!:nsen,Ry;l"' Palmer moro sPaC$ is needed) .. -.. Carrier, Waybill Number r 'I I I Specia/lnsU'Jct~nsl Containers & i 0 Conamons ot Receipt Matrix Preservatives O l ~, ;j ';;; ~ N ' i i "' i 8 ~ ~~ z ~ ~ Time e ::. , ~ a.f I ~ -g 'i; ~ ~ ~ ~ t-c: _.J" <( ;n "' "'"' I Jl 8:00 X I X 'fci I /VtJ3X~ I .· i -.11 8:00 .,X; • 'f..,) -i ' I [~{~XAI\ ----l 1 I 1\,. I s:oo I l '!\ x· X ;~ !/I~Q X i 1 8:oo -X~ I 1\ 'A "f.: ''A I I I I i /I/\ ·:rz.x \tv' : I . ' l I I ! t I I I I ! 111111~11111111111111111111111 J1 080456 I I ; l ! I i I I I I I ! -POS$'1J/e F/aza,d ldsnlilicalion 0 Non-fitlzarri 0 Flammable 0 Skin lrriltult l S.amp;e Dispose] 0 Poison 9 · 0 Unknavtn 1 0 Retum Ta Client (A fee may ce assessed ff ssmpfr:llate retained 0 Disposal By Lab 0 Archive Far ___ Marrlhs longer rhm 1 month) 0 7 Days 0 14 Days 0 21 Days rn:re /I Cl0 3. R'J/inquisr.ed 8y 1 Time I C<Jmm.,ms When Complete Email to: Dean or Paul tetco@tetco-ut.com fiiSTRIBVTION; WHITE-Re!umed t:> C!iel;l ~-/..fit P,a~ ~nY-Sl:Jtfl ~·;t.b tile Sur.p~ PINK-,~ui ~~ Test America ~~·-?l!?k&'i!ilfiimiZK-G'i~.:E!I 7HE LEADER IN ~I'·NIR.ONM~NTAl TCSTII'JG Sample Check-in List Date/Time Received:..f/3JJ~/~()~Q>£-___ GM Screen Result (om) _I_,(:;__ (in), __ ~--'~c-......,.~-InitialsffL Client ()c"'ksoVI SDG #: Lj 3)~q NA [] SAF ~: NA [] \Vork Order Number: ..J /)=C)6QI..lG7R Chain of Custody#------·--------- Shippi.r'.g Container ID: ___________ ____:~-t;, ~ir Bill'!=--------------------~A t*-(_ l:em l through 5 for sr.ippi..'1g ::om:aine:-only. e:,i~ic.! appro;nic.te response. l. 3. 4. Cuswcy Sec.ls on shipping conrziner intact? Yes [ Cusmciy Seals ciarcd and sign.od? Yes [ }\o [ ~o Custocv Seal ~ ~o Custody Sea~ Chc.in of Cusmdy record present? Yes ~o [ ] Coole: te:;nperarure: ____ "'\A [~~-5 \'e:-:niculne·packi.P.g mate:-;c.ls lS :\A [ Item 6 through iO for samples. b.itial appropriare response. 6. ~umber of samples in shipping container (Each sample may contain multiple bottles): Y.(j) J hee./£e/(<f¥j I b }~ 7. Sample holding times exceeded? NA [ ] Yes [ ] No r{-j-f--' 8. 9. Samples have: tape ==custody seals ~~II!f>les : ~--in good condition are broken ~h~ardlabe~ ~appropriate sample labels __ are leaking __ have air bubbles (Only for samples requiring no head space) 10. Sample pH appropriate for analysis requested Yes [ ] No [ ] N/A }J f l J.;l<Jote discrepancies in #13) (If acidification necessary, then document sample ID, initial pH, ~'~fHN03 added and pH after addition) RPL ID #of preservati-ve used:. _______________________________ _ 11. j:)ample Location, Sample Collector Listed? * *For documentation only. No conective action needed. 12. Were any anomalies identified in sample receipt? Yes [ ] No ~-~V'· 13 , Description of anomalies (include sample numbers): NA [ ) ____________________ _ -{-Soe oth<rr <ide foe ad_clitional oomment< SampleCustodian -~-<' l1_~ Date:G/¥Hll-------- Cllent Informed on by Person contacted. __________ _ [~No action necessary; process as is Project Manager 8 ;:.£, o C)~ LS-023, Rev. 12, 10/10 TestAmerica Laboratories, Inc. 19 Date._~..:_/q...:.-..L.-/J:....J../ ____ _ APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Grizzly Baghouse Figure 3. Facility Schematic Representation Production and Control Equipment Data Nmth Yellow Cake (Scrubber Flow Rate(s) Yellow Cake Dryer Baghouse (8 baiTels filled during test) Grizzly (tpb of material and belt speed) D Facility. Denison Mines t a l y stackidentification: North Yellow Cake Scrubber a : Distance upstream from next disturbance, feet ----------------- ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet ______ ___;_;_ ______ _ Estimated Moisture, percent Estimated Temperature, "F Control Unit Type: Scrubber Number of Ports ----------------- Figure 1. Facility Schematic Representation Process Type: Yell ow Cake Processing Facility. Denison Mines t a y Stackldentification: yellow Cake Dryer Baghouse a: Distance upstream from next disturbance, inches 5~ ---- !3: Distance downstream from last disturbance, inches 45 y: Distance of Sample Level to Ground, feet 6: 0: Stack Inside Diameter, inches 1 ( Estimated Moisture, percent 0-~ 1~ Estimated Temperature, °F ----- Estimated Velocity, fpm 1,4 -------"- Control Unit Type: Baghouse Number of Ports 2 Figure 2. Facility Schematic Representati' Facility. Denison Mines t a ! 'Y stackidentification: Grizzly Baghouse a: Distance upstream from next disturbance, inches 24. ----- ~: Distance downstream from last disturbance, inches 4~ y: Distance of Sample Level to Ground, feet 2: ----- 0: Stack Inside Diameter, inches 18.' ----- Estimated Moisture, percent 1 ~ Estimated Temperature, °F Aml ----- 7~ Estimated Velocity, fpm ___ ___;.....; Control Unit Type: Baghouse Number of Ports 2 Figure 3. Facility Schematic Representati' Denison Mine Process Data Source: North Yellow Cake Date: SI2S'/!~ Scrubber Flow GPM Time #I #2 ~p e: t t. 4·ct !Z.,o 1ro e: L\) q,'Q Jt.'f '3, 0 '1: 1. c 0·6 lo, :;z_ :.,,v C\'.)0 q, ") 1l,L..__ 3,o ro:L.u c; ,, 0 tLo ),0 IO'.'fO 9, E \'2.,D J,0 \I'. {.Q \a.o t-z..,o 3,0 \ l '. ) 0 \0, l \(_,(_ ~tO tJ...'. J.o I 0' l \2,2. 3,0 \~foO 'lrl \( .l 1.o I:S: 3 o lO ·l n .. 2 J,o L'-\ ·, 00 lo, \ 17.., & s,o /t.(~ J() 't" I Z., o 3.o If: oo Cf,~ \\,9 )rO !).'Jo 18 11, ( 3 tl ii;,~ \ (.,' !)D 9,3 \1, (_ JrO Denison Mines Process Data Source: North Yellow Cake Date: J¥1 Cj_ '1 ,')...~ / z 0 If Scrubber Flow GPM Time #1 #2 t:lP g ~o') /6. I rz,z_ 1...1 s:3s ;b .o I 2. ( L~C,- "'/., l7 <' . , ' IQ,D I~. ( )._ I '-T '/:3) '1, &? l!.) '2_ • "-7 (r . o -.5. ), 1' (. • ·P I I-f-l.'l J () ! ~· ,5'" 9.9 t ?_. / 2' -~, 1/.'oS" q.J 1/. 7-Z,9 5 ~IV t-P OUc\ {\ I .~ I ,_. t6,--l I 0 I'), rs I 0 ~) 1 0 \ ~,./ 1 5 · ·>, r:; I ._} _ __,/ 0 'l ()r !O, ~3 3,{ l/ . ·f? ·)0 1.3 //,(J 'Z_, GJ 11-:oo ~(.? ls.o 3.0 11:3o '7, I I z.. z.. z.cr !& : ~0 cr.t-r?, 1J 5.o !8 ~Clt) c;.(R /'Z-·(_ 7 .Cf J9·'0D ~.~ !"3 .z__ ~.Q tq ~30 q.-r I~. v z.. <i 'Lo ·. o o 'f.~ ~~ ,-z._ ~-0 1o ··~t q,t l ~' ( l.~Gt Denison Mines Process Data Source: Grizzly BaQhouse Date: mt:kt ~t~ zotl Time T<> VI .> TPII r: PYVI. :f;so (jgqqs-t~S 101·3 e;2_3 tf-90({5" 130 /69-b 8: 5'0 111o9o I 35"' /01.& cJ\ lO tf-9!4-s 3>30 /67.~ r..y. -c . ,) 1 :rcr z_po I I 5--I o'f, t ttJ~i(z.o ( :pl2 LfV / (),~~ !O? 7- /O:GO t19 2-'c? 0 L[,;-;ocr .s- !/.: 2-o (7-c; )l~-/DO /O J: 3 II. :;o 1 }9 :) f5 &D ) 6'1. (p /2: ?.,[) IF11/25 !20 ;o;: .:;,-- ,t:sv (J1ct 1-D Lff] C• f I o f. · 13 ~ z.o f +'7 SOD tS I 0 (!.(, C( l:s '.SD tlY s--s-o ;IJO I() ?. ~-- I~ ', 2.:0 It cr 59'o 5-.S~ I0 °!w 1'-\ :50 t7-CJ (~ l.._') (#() !0 <'f.(o iS-·, ?._D 17-CJt,ls '60 /D1 f 1 !)-: S'O t1-'J/30 I 40 (De{. f APPENDIXE Calibration of the console dry ga meter(s), pitot tube , nozzles diameters, and temperature sensors were carried out in accordance witb the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-te t Dry Gas Meter Calibration Data Forms TypeS Pi tot Tube Inspection Data Sample Box Temperature Sensor Calibration E Temperature Sensor + ~Probe TypeS Pitot Tube Temperature Sensor GooseneckTe~~~~~~~re Nozzle t-e:tTra:ed ~ ~ Glass Filter / ~ Holder TypeS Pitot Heated Area Tube Stack Wall Manometer Orifice ICJllinger Train Optional, May Be Replaced By M. Equivalent Condenser I Temperature Sensor ,-------------- lmpingers Air-Tight Pump Figure 4 Schematic ofMethod 51114 Sampling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL W: 11522588 I CRITICAL ORIFICE SET SERIAL#: 14535 EQUIPMENT ID #: K' TESTED ,--------r----~ FACTOR VACUUM RUN# (AVG) (in Hg) 0.8137 13 896.006 2 0.8137 13 901.301 3 0.8137 13 906.609 0.5317 13 912.40 0.5317 13 917.596 0.5317 13 922.809 0.3307 13 928.304 0.3307 13 933.524 0.3307 13 938.841 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 901.301 906.609 911.936 917.596 922.809 928.018 933.524 938.841 944.055 5.295 5.308 5.327 5.196 5.213 5.209 5.220 5.317 5.214 74 74 74 76 74 79 74 79 74 80 74 82 74 82 74 81 74 83 76 70 79 70 80 72 80 75 82 74 83 77 83 78 83 79 84 80 70 72 73 82 77 78 79 80 80 DGM AVG 72.5 74.25 76.00 79.00 78.25 80.00 80.50 80.75 81.75 Facility fiNAL AVG (P .. ,) 25.30 25.3 ELAPSED 12.00 12.25 12.00 New Calibration 2011 4.4778 !lli1 ~ 4.3198 ~ ~ ~ 4.3964 4.3032 IF Y VARIATION EXCEEDS 2.00'/• ORIFICE SHOULD BE RECALIBRATED ~ 4.3672 ~ AVG = ~ ~ AVG = 1 The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std). and the critical orifice, Va{std), and the DGM calibt'afion factor, Y. These equations are automatically calculated in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.004 (1) (2) (3) V: _ K • V: * Pbar+ (M//13.6) m(.\'ld) -I m Tm Pbar * El Vcr = K'*--==~ (."JJ .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K1 = 17.64 'Riin. Hg (English), 0.3858 'Kimm Hg (Metric) Tm =Absolute DGM avg. temperature (0R-English, °K-Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb =Absolute ambient temperature (0R-English, °K-Metric) K' = Average K' factor from Critical Orifice Calibration y = Vcr{:.ud) Vm(sld) = DGM calibration factor Pre Calibration 2008 AVERAGE AH@ =I 1.649 AH@ = ( 0.75 9 )2 AH (Vm(std)\ Vc,(std) Vm } Temperature Sensors Reference In Out 34 67 202 OF 34 67 202 35 67 204 !ill !.Ill .lll2 ~ ~ !:.§g METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feel 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL#:~ CRITICAL ORIFICE SET SERIAL 11:~ EQUIPMENT ID #: K' TESTED ;------.---!FACTOR VACUUM RUN II (AVG) (in Hg) 2 3 2 3 2 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 12 12 12 13 13 13 13 13 13 155.004 161.521 168.043 136.700 142.672 148.297 116.20 125.809 131.075 USING THE CRITICAL ORIFICES AS CALl BRA TION STANDARDS: 161.521 168.043 174.568 142.672 148.297 153.926 125.809 131.075 136.357 6.517 6.522 6.525 5.972 5.625 5.629 9.609 5.266 5.282 74 82 74 83 74 83 74 81 74 80 74 81 74 76 74 78 74 80 83 89 83 93 83 96 80 84 81 86 82 88 78 77 80 80 81 81 93 96 99 86 88 89 80 81 84 DGM AVG 86.75 88.75 90.25 82.75 83.75 85.00 77.75 79.75 81.50 FINAL 25.10 ELAPSED TIME(MIN) e 6.00 6.00 6.00 22.00 12.00 12.00 AVG(P.,,) 25.10 7.9255 4.3273 ~ 2011 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 ~ ~ ~ 1.000 ~ ~ AVG= 1&l!ll -0.09 4.9104 1.004 !&ill ~ 4.6215 1J!l!I AVG= ~ 0.47 7.9047 !!.l!l!I 4.3117 !!.Jm2 4.3117 !!.l!l!I AVG= !!.l!l!I 1:.§§. ~ 1.489 1.532 !.ill 1.526 L!ll 1.432 1.428 The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifiCe, Va (std), and the DGM calibration factOf, Y These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.001 (1) (2) (3) V =K •V *Pbar+( H /1 3.6) m(.•td) ' m Tm Pbar * E> Vcr""") = K'• .,/Tamb = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17.64 'RI1n. Hg (English), 0.3858 'Kimm Hg (Metric) T m = Absolute DGM avg. temperature ('R-English, 'K-Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T""" = Absolute ambient temperature ('R-English, 'K-Metric) K' = Average K' factor from Critical Orifice Calibration y =Vert·""' Vm<..:,J> = DGM calibration factor AH@ = ( 0.75 9 ) 2 AH (Vm(std)) V .. (std) Vm Temperature Sensors Reference In Out 32 72 203 OF 32 73 201 OF 32 73 202 Pre 2011 5 console METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic teet 4) Record data and information 1n the GREEN cells, YELLOW cells are calculated OATE:t-=="--l METER PART ;1:'-===..::....J METER SERIAL #:1-===---1 CRITICAL ORIFICE SET SERIAL#:,___....:..:==---' EQUIPMENT ID #: K' TESTED FACTOR VACUUM RUN # (AVG) (In Hg) 0.5:117 13 0.~317 13 0.&317 1l 53.103 6.2.654 62.654 11.213 71.213 18.444 9,551 8.559 7.231 69 57 69 72 69 75 72 72 75 75 78 80 75 80 8l .0 .0 .0 I I I I I I USING THE CRITICAL ORIFICES AS CAUBRATION STANDARDS: .0 .0 .0 I I I I I I INITIAL DGM AVG 71.50 75.50 79.00 0.00 0.00 0.00 0.00 0.00 0.00 Facility FINAL 25.20 ELAPSED TIME(MIN) a 14.00 12.50 10.50 AVG(P"") 25.20 §§ §§ DENNISON MINES 8.0184 71319 5.&862 IF Y VARIATION EXCEEDS 2.0~, ORIFICE SHOULO BE RECALIBRATEO l 8.1582 1.017 7.2841 .1m §..11§! 1J!ll AVG= .1lli M2 AVG: The fcUc~ing equations sre usa,j to caltulatE the standard volumes of air passed ~hwugli the DGM, Vn: (std). and the critical orifu, V :r (std), and the DGM calibration factor, Y These equations are automatically calculatad in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y; I 1.020 (1) (2) (3) = Net volume of gas sample passed through DGM. corrected to standard conditions K1 = 17 64 'Rfln Hg (English), o 3B58 'Kimm Hg (Metric) T m =Absolute DGM avg temperature (0R-English, "K-Metric) = Volume of gas sampJe passed through the critical orifice, corrected to standard conditions T~:rro = Absolute ambient temperature (=R-English, '~K-Metric) K' = Average K' ~actor from Critical OrifiCe Cal'lbrat;on = DGM calibratiOn factor Pre Calibration 2008 AVERAGE .iHe =I 1.519 ~ 1.518 .1,_lli METHOD 5 DRY GAS METER CALl BRA TION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Reccrd barometric pressure before and after caltbration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells. YELLOW cells are calculated. METER SERIAL t:c=J CRITICAL ORIFICE SET SERIAL ~~ EQUIPMENT ID ~: K' TESTED RUN# (AVG) (in Hg) 0.4238 12 205.301 210.826 5.525 70 67 70 70 0.4238 12 210.825 217.220 6.394 70 70 73 75 0.4238 12 217.220 222.801 5.581 70 73 75 78 Facility FINAL 25.30 ELAPSED DGM TIME(MIN) AVG a 75 70.50 10.00 78 74.00 11.50 81 76.75 10.00 UhkWUblkA;tiMt·'mw; Denison Mines AVG(P..,) 25.30 4.6598 5.3573 lllli IF V VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 4.6588 1.&!!!! 5.3576 1.&!!!! ~ .1Qll AVG= 1..QQQ 0.00 .0 I I I I I I .0 .0 0.00 §§ 0.00 0.00 AVG~ I I I I I I .0 .0 .0 0.00 § § 0.00 0.00 AVG= USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: The followl!:g ~qua!iO!'lS art:! u~ed tc ca~:~late !he standard volumes of air pa::;sed through the DGM, Vm (std}, and ths clif.ca! orifice, V~ (std) and the DGM caflbralion factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y = 11.000 I (1) (2) (3) Vm =K•Vm•PIJar+(6H /13.6) ,slii) t Tm = Net volume of gas sample passed through DGM, corrected to standard conditions K, ~ 17.64 'Riin Hg (English), 0 3858 'Kimm Hg (Metric) T m = Absolule DGM avg temperature ('R ·English, 'K • Metnc) ~ Volume of gas sample passed through the critical orifice, corrected to standard conditions T~mb == Abso,ute ambu:n! temperature {0R-Englitih, "K-Metric) Y-Vo;""' Vm,,4, K' ~ Average .K' factor from Cri!i::::al Otifica Calibration = DGM calibration factor AVERAGE <l.Hl! =/1.456 U§!! 1.455 1Ml POST Console #5 Calibration 2010 Dat~· 01 I I TypeS Pitot Tube Inspection Data Pi tot Tube Jdontitication: __ d'f __ -_,f'--f'--------- nchnician: K . /Vt c. NC! t.tLt>.Fr>--.. Dt= . ~-,s-in. Is PA=Pa? __ ~V~e~5~------ PA"" . t..t s 0 Ill. Is 1.05 • D, s; D, s; 1.50 • 0 1 ? __ y..__,-c:...-=-..,5...._ ___ _ p" = L({;;() in a 1 < 10° a.,= u, < 10' al= '1.. "' < 5' (!,= _____ _ ~' = __ ®_,__ __ Z s0.125 in. Z= W s 0.03125 in W = _ .. oo'c._in_ W > 3 inches W = ~ I /1 -in Z > 314 inch Z = -7/_ ¥:-in. . .,. •• ,. ~~ ¥2:3 inches ~,:-----in The pi tot tube m~cts the specifications for a calibration factor ofO 84' Temp<>raturc Sensor Calibration Rete renee Temperature Temperature Tempcr.nure Source Ref~ renee Sensor Difference (Medium) ("F) ("F) !'Fl AlR lO ""1 0 D Probe Continuity ......... --..-----.....__ -------_, \J.{I/'j Heat Check 248 -·-J Y-<.<<:> 1_, (,( l2 AIR lo ID t) !C£WATF.R ~~ .~0 I Stack BOIL WATER W Lr_ 1--___b_ 't,. \ SILICONE OIL Type S Pitot Tube Inspection Data Date: _\_1_r _, ___ (_{? __ Pi tot Tube Identification _"1,_.::__"'\_-_CJr ______ _ 0< Technician: K • ~~ Dt=. S 7 ~ '"· Is p A= Pn ? r -c ";::> Is 1.05 • D, :S D, ::; 1.50 • D,? ~~:v:-e..-:::~-<£>~~~~~~~= PA = f-/L( ~ in. Pa = (j_ 9. z_ m a1 < 10° a,'= a ,< JO" (l2= ~. < 5" pI =----'---- p,= 0 Z,;: 0 125 in Z=_ .OQ Z.. _in. W,;: o 03125 in. W= .oo-3 in. W > 3 inches W= -.3 in. Z > 3/4 inch Z= in. The pi tot tulle meet.:; the specifications for a calibration factor ofO 84° Temperature Sensor Calibration Reference· Temperature Temperature Temperature Source Referen ce Sensor Din·erence ' !Medium) ("F) (''F) C"Fl AIR lv ~or ( Probe Continuity --r Yr/ S Heat Check 248 --9 '-r e.'i::> "2.. ~-(.) AIR 10 ~(i>"' I ICE WATER "5~ 3 -.'? () Stack BOIL WATER "CDS zj)c; f) SILICONE OIL Type S Pitot Tube Inspection Data Date: \ "\_, -1J) •' \0 Pi tot Tube Jdcntiflcation·_l;.>.::,..._(L.--~(A:...!... __ ~:.._ ___ _ Dt Technician J.{. N\ yM"'-.W'lacC"\ . ~ I t :: r . '!> 7S HI Is P A = Ps ? -"'yc...:-{.../:~.c:::_9;,_:::__ ___ _ Js 1.05 • D, :5: D, :5: 1.50 • D,? \ I :-<..--~ -""'>,~~-=::..._ __ 8:: ~,, '-..!._ 62 ~P A~=__._, _l:{.Ll.f...L-u..5/ ___ in CL1 < JO' a, < I o• 1), <5' a, = __ "'Z.-_::_ __ _ a, = __ ...;J.___ __ fit =---=0~-­ p, = _ _,!'2..-~-- Z,; 0 \25 in r-·-z = • () "":> S in W $0 03125 in W= . Q(" en I W > 3 inches W= 1-:t., Z > 314 inch Z= '1~, . . "11-4='--..-: _____ Y ~ _, inches I Y= 3 f-t_ The pi tot tube m~ets the specifications for a calibration factor of0.84~ 'y e.---5 Tem perature Se1lsor Calibration Reference· Ten1perature T~moc:rattlr<: Temperature Source Reference Sensor Difference (Mcd1urn) ("F) ("F) ("F) AlR ((J 7{ (;~ C> Probe Continuity -----Y b-.:!> Heat Check 248 ----7 y~ Tc;D AIR I ra~ to~ 0 ICE WATER s ?J ~L 0 Stack BOIL WATER l?o(....f ·z_. QCJ{ D SILICONE OIL in in in Ill TETCO Sample Box Temperature Sensor Calibration Date: 12/29/l 0 Calibrator: Mike McNamara Reference: Ome~a CL3512A Thermocouple Temperature Temperature Temp. Diff. Unit 1D Location Source Reference Sensor or Result (Medium) ("F) ("F) ("F), P/F Oven Water 34 34 0 Water 203 203 0 A Water 34 33 I Probe Out Water 203 204 -I Water 34 36 -2 Impinger Out Water 203 203 0 Oven Water 32 34 -2 Water 203 204 -1 B Water 32 33 -I Probe Out Water 202 204 -2 Water 31 31 0 Impinger Out Water 203 205 -2 Water 34 36 -2 Oven Water 204 205 -I c Water 34 36 -2 Probe Out Water 203 205 -2 Water 34 36 -2 [mpinger Out Water 203 20I 2 Oven Water 33 33 0 Water 203 203 0 D Water 33 33 0 Probe Out Water 202 203 -1 Water 33 33 0 Impinger Out Water 203 201 2 Water 33 34 -1 Oven Water 203 203 0 E Water 33 34 -1 Probe Out Water 203 204 -1 Impinger Out Water 33 33 0 Water 203 204 -1 Oven Water 33 33 0 Water 203 202 I F Water 33 33 0 Probe Out Water 203 201 2 Water 33 34 -1 lmpinger Out Water 203 201 2 I I mpinger Out G Water 33 34 -1 Water 203 202 1 I lmpinger Out H Water 33 35 -2 er 203 202 1 I Impinger Out I Water I 33 33 0 I Water 203 204 -1 I lmpinger Out J Water I 33 33 0 Water 203 204 -1 APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. ATTACHMENT H SURFACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-05 1.00E-06 1.00E-07 -Cll (ij ~.OOE-08 C'l 0 ...J - 1.00E-09 1.00E-1 0 1.00E-11 ..... .... • • . -• ---·---- Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) • ... .... • ... • ~ .... • ·~ .. ---- • • .... .. = -..... ......__. --------------------------------- + U-N at. • Th-230 .6. Ra-226 - .. "' ---- 1.00E-06 1.00E-07 1.00E-08 -.!! cu ~1 .00E-09 Cl 0 ..J - 1.00E-1 0 1.00E-11 1.00E-12 fb<o "QS ~~ .... • = -•• • si-~"QS cy_fl,~ Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) • -• -• ~ • ... • ... ... ~· ..... •• .... • ... -"-= • ----• -== == • • • ==-= •• ·--• 4 .. • • • • • • • --~ - ~~ ~~ ~<o ~co !:.)" ~ !:.)(() !:.)0; Q) "Q) ~"Q) ~"Q) ~ ~ ~ ~ ~" ~rv (\~ r}rv ~'); ~ ~ ..... ~ cy."t;;:j rJ n}rv ~rv cb''V n} "rv " • U-Nat. •Th-230 •Ra-226 1 EN:RGY ;\~ ~)J , \1\....·t~ •• ._, www.energylab.com AMiyl/l:tll ER~&Ww ._ 'au Helena, MT 877-472-0711 • Billings, MT BQI-735-4489 • Caspar, W'i 888-235-0515 Gillette, W'i 11&-688-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-819-2218 March 25, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11030344 ANAL VTICAL SUMMARY REPORT Project Name: 1st Quarter Surface Water 2011 Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 3/11/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 030344-001 Cottonwood 03/09/11 11 :05 03/11 /11 Aqueous Solids, Total Dissolved Solids, Total Suspended C11 030344-002 Temp Blank 03/09/11 0:00 03/11 /11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: o¥~ J) tJtJ.Jy Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011 .03.25 10:04:52 -06:00 Page 1 of 8 EN:RGY "=~ i\•l'-11•/\l (,!d ' ~ wv.w.energylab.com AMiyfltM Em11N1:1 Slllu IW Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette WY 866-186-7175 • Ra ld Cl SO 188·872-1225 • Colla e Stall on IX 881~690-2218 CLIENT: Denison Mines USA Corp Project: 1st Quarter Surface Water 2011 Report Date: 03/25/11 Sample Delivery Group: C11 030344 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELl reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELl's certification coverage by visiting www.energylab.com ELl appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 8 EI\ERGY ,~,.,, )f (,1\ I ( ! •1 _ .- www.energylab.com Alulybl Elu/IMel Sblc• IW Halena, lilT 877-47HI711 • Billings, MT BOI-735-4489 • Casper, WY 811-235-8515 Gillette, WY 888-186-7175 • Rapid City, SO 188-172-1225 • Collage Station, lX 811-110-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab ID: 1st Quarter Surface Water 2011 C11 030344-001 Client Sample ID: Cottonwood Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS@ 180 C Solids, Total Suspended TSS@ 105 C Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result 425 7 Units mg/L mg/L Qualifiers RL 10 4 Report Date: 03/25/11 Collection Date: 03/09/11 11 :05 DateReceived: 03/11/11 Matrix: Aqueous MCL/ QCL Method Analysis Date I By A2540 C 03/11/11 15:45 I lr A2540 D 03/11/11 16:40 lime MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 8 EN:RGY ,. .'\' ()f ·~\I Olll. ·~ www.energylab.com ~I~U.OC.~ IIJ1 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 88&-18&-7175 • Rapid Ci1y, SD 888-&72-1225 • College Station, TX888-69D-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1st Quarter Surface Water 2011 C11 030344-002 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 2.0 Qualifiers RL Report Date: 03/25/11 Collection Date: 03/09/11 Date Received: 03/11 /11 Matrix: Aqueous MCL/ QCL Method Analysis Date I By E170.1 03111111 09:00 I kbh MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 4 of 8 EN:RGY '\1 ~ H u ~ I :f,IJ '- www.energylab.com Alu/fflt:M~SIIcl' rw Helena, MT 817-472.0711 • Billings, MT 800-735-4481 • Casper, WY 888-235-1515 Gillette, WY 88&-888· 7175 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-810-221 8 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1st Quarter Surface Water 2011 Analyte Count Result Units Method: A2540 C Sample ID: MBLK1_110311 Solids, Total Dissolved TDS@ 180 C Method Blank ND mg/L Sample ID: LCS1_110311 Laboratory Control Sample Solids, Total Dissolved TDS@ 180 C 984 mg/L Sample 10: C11030313·002AMS Sample Matrix Spike Solids, Total Dissolved TDS@ 180 C 2590 mg/L Sample ID: C11030344-001ADUP Sample Duplicate Solids, Total Dissolved TDS@ 180 C 410 mg/L Qualifiers: RL-Analyte reporting limit. Report Date: 03/25/11 Work Order: C11 030344 RL %REC Low Limit High Limit Run: BAL-1_110311A 4 Run: BAL-1 _110311A 10 98 90 110 Run: BAL-1 _110311A 10 102 90 110 Run: BAL-1 _110311A 10 ND -Not detected at the reporting limit. RPD RPDLimit Qual Batch: 110311_1_SLDS-TDS-W 03/11/11 15:40 03/11/11 15:40 03/11 /11 15:44 03/11/11 15:46 3.4 10 Page 5 of 8 EN:RGY ,-,. ,r )f-;, 1 t .I l: •• www.energylab.com AM/yf/M Elui1Mn SS.. IIU Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-1515 Gillette, WY 88&-18&-7175 • Rapid City, so 188-672-1225 • College Station, 1X BBHBD-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1st Quarter Surface Water 2011 Analyte Count Result Units Method: A2540 D Sample ID: MBLK1_ Solids, Total Suspended TSS@ 105 C Method Blank ND mg/L Sample ID: LCS1_ Laboratory Control Sample Solids, Total Suspended TSS@ 105 C 150 mg/L Sample ID: C11030372·003ADUP Sample Duplicate Solids, Total Suspended TSS @ 105 C ND mg/L Qualifiers: RL-Analyte reporting limit. Report Date: 03/25/11 Work Order: C 11 030344 RL %REC Low Limit High Limit Run: BAL-1 _110311B 6 Run: BAL-1_110311B 12 75 60 110 Run: BAL-1_110311B 4.0 ND -Not detected at the reporting limit. RPD RPDLimit Qual Batch: R143577 03/11/11 16:40 03/11/11 16:40 03/11/11 16:42 10 Page 6 of 8 EN:RGY • : •.. ·1·/·1 Ci~ll ~ www.energyleb.com Atu/fllal £Ja/law S/IIa 1/ISZ Helena, MT 877~72-0711 • Billings, MT 801-735-44811 • Casper, WV 888-235-0515 Gillatta, WV 18&-888-7175 • Rapid City, SO 118-172-1225 • College Station, TX 888-&10-2218 Workorder Receipt Checklist Denison Mines USA Corp lllllllllllll~ 1111 IIIII 1~1~1 C11030344 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 3/15/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Containerffemp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.0'C On Ice Yes D Yes 0 Date Received: 3/11/2011 Received by: ha Carrier name: FedEx NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Not Present D Not Present D Not Present 0 NoVOA vials submitted 0 Not Applicable D Page 7 of 8 ""0 Ill (C CD co 0 -co Chain of Custody and Analytical Request Record Page _l _of _j_ LABOIU't TOI?It:!> PLEASE PRINT {Provide as much information as possible.) Company Name: M; (\e.~ Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: D~n-;.S Dfl j5T G\Au.rl-~ (' st>..Mc-.<-e We...+e.• State: l(l Yes g" No 0 Report Mail Address: fO ~O')< ~Ot{ Contact Name: Phone/Fax: Email: Sampler: (Please Print) <Q\Mc}:dW\ LX\" ~1..\~i\ R~l).t\ ?o-.\me.r L\3..'S 6 7g ~\ i\jt>-n Po..l~er Invoice Address: --....J Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: ~N'"I\e ~tflt. Special Report/Formats: ~ ~YT®O® ~®JD~rniiD .. Contact ELl prior to ~<it¥-c ~ RUSH sample submittal ~oell~ ~ for charges and Cooler ll(s}: ~OJ~ OJ (D 0 R scheduling -See ~ oow D EDD/EDT(Eiectronic Data) ]i> c55 iO <6 w t:. Instruction Page c<n<Js l:l ~ I -o 0 POlWN-IWTP Format: (33:'5 gj g' (.) c Comments: Receipt Temp :1 u ..... <co'mt::>< <t: e "0 oc 0 State: 0 LEVEL IV 0 ~ c "-wm c: ·.:::: 1--m lS 0.''\g Cl c D Other: 0 NELAC 1--..... On lee: (!}N E~m, <t: ::;) ::::1..92~1~~ I-s zo.. Q>Cl ~ w "E Custody Seal E >I ~ w m On Bottle y N "' rn -o ffi: en c: On Cooler r \-~ H Intact (/) SAMPLE IDENTIFICATION Collection Collection MATRIX Signature Q)N (Name, Location, Interval, etc.) Date Time Match , ~ o-tf-a()\JJCO~ ~-q-j.J)I\ uo~ \ -\J '/. 'i ~ 2 ...., ~ ~~ - 3 \~o 't-.\ClA'C...-~ 4 ~ 5 ~ 6 ~ 7 ~ 8 I ~ 0 9 aa ~ 10 l'=tr~&J~ Y~ Custody ReUnqulshed by (pr;rn); Date/Time: l03o ~""~~~:"'naMJ~~~J Reoo!Ved by (Pflot) Dale/TWne: Slgn11ture: -l,...nPr ·~o\ \ :!L\.u ~-l~.:l.OjJ Record Reifl(juished by (prinl): d Dale/Time: Sognatul'll: -..J Received by (print): Date/Tme: Signature: MUST be Signed ruoCOIV"" oy L.IDOraLOry; sr:'\r· COt) .l~~()~ Sample Disposal: Return to Client: lab Disposal: ·t -\\ In certain circumstances, samples submitted to Energy laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated oo your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. EN:RGY .•,: i>I;;.\I CHL~ www.energylab.com AMiybl~au 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatte, WY 8&8-888-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 ANAL VTICAL SUMMARY REPORT June 23, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11050696 Quote ID: C1640-POC Wells Project Name: Semi-Annual Surface Water 2011 Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 5/20/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 050696-001 Cottonwood Creek 05/18/11 8:30 05/20/11 Aqueous Metals by ICP/ICPMS, Dissolved Sample Filtering Uranium, Suspended Digestion, Total Metals Gross Alpha minus Rn222 and Uranium Radium 226, Dissolved Radium 226, Suspended Thorium, Isotopic Thorium, Suspended Isotopic Solids, Total Dissolved Solids, Total Suspended C11 050696-002 Temp Blank 05/18/11 0:00 05/20/11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~ £J LJtA!Jy Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011 .06.23 14:38:43 -06:00 Page 1 of 12 www.enugy1ab.com AMIIf/l:tll ~ 1/RU 1151 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515 Gillette, WY 8&&-186-7175 • Ra id City, SO 188-&72-1225 • Colle e St.alion, TX 888-690-2218 CLIENT: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Report Date: 06/23/11 Sample Delivery Group: C11 050696 CASE NARRATIVE TH230 ANALYSIS USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency prior to using these results for compliance purposes. RA226 ANALYSIS USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency prior to using these results for compliance purposes. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t-Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EI\ERGY /\ I : ) I j ;', I ' ~ l ~ ' • www.energylab.com ~rm.u.-smc. rm Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Semi-Annual Surface Water 2011 C11 050696-001 Client Sample ID: Cottonwood Creek Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS@ 180 C Solids, Total Suspended TSS@ 105 C METALS-DISSOLVED Uranium METALS-SUSPENDED Uranium RADIONUCLIDES-DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC RADIONUCLIDES -SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC -See Case Narrative regarding Ra226 analysis. -See Case Narrative regarding Th230 analysis. Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 463 mg/L ND mgll 10.2 ugll ND ugll 0.2 pCill 0.2 pCi/L 0.3 pCill 0.06 pCill 0.13 pCi/L 0.21 pCill 0.07 pCill 0.1 pCill 0.2 pCill -0.2 pCi/L 0.18 pCi/L 0.45 pCill 0.2 pCi/L 0.2 pCill 0.3 pCill MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Report Date: 06/23/11 Collection Date: 05/18/11 08:30 DateReceived: 05/20/11 Matrix: Aqueous MCL/ Qualifier RL QCL Method Analysis Date I By D u u u u u 10 6 0.3 0.30 A2540 C A2540 D E200.8 E200.8 E900.1 E900.1 E900.1 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. 05120111 14:19/lmc 05120111 15 :00 l ime 06122/11 13 :02 1 sml 0513111118:21 1sml 06116111 11 :13 I ep 06116111 11 :13 1 ep 06116111 11 :13 I ep 05131111 12:051 trs 05/31/11 12:051 trs 05/31111 12:05 I trs 06/14/11 08:49 1 dmf 06114111 08:491 dmf 06114/1 1 08:49 1 dmf 05131111 17:25 1 trs 05131111 17:25 1 trs 05131111 17:25/trs 06109111 11 :02 I dml 06109111 11 :02 I dmf 06109111 11 :02 I dml Page 3 of 12 ---~ EN:RGY .. 1\t-1: 'l~n l LHI '> www.enefgylab.com AM/ytlal~stlu IIU Helena, liT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-680-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Semi-Annual Surface Water 2011 C11 050696-002 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 4.0 Qualifier RL Report Date: 06/23/11 Collection Date: 05/18/11 DateReceived: 05/20/11 Matrix: Aqueous MCU QCL Method Analysis Date I By E170.1 05120111 08:50 I kbh MCL-Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 12 EI\ERGY 1\tJ ~f;,·,ICHit •3 www.energylab.com Wlfl/,.1 Exu/IMJ~ Slnu flU Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-886-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QAIQC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Ana lyle Count Result Units Method: A2540 c Sample 10: MBLK1_ Method Blank Solids, Total Dissolved TDS @ 180 C ND mg/L Sample ID: LCS1_ Laboratory Control Sample Solids, Total Dissolved TDS@ 180 C 1010 mg/L Sample ID: C11050660-002ADUP Sample Duplicate Solids, Total Dissolved TDS@ 180 C 1750 mg/L Sample ID: C11050712-001BMS Sample Matrix Spike Solids, Total Dissolved TDS@ 180 C 2430 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 4 10 10 10 Report Date: 06/23/11 Work Order: C11 050696 %REC Low Limit High Limit RPD RPDLimit Qual Batch: R146206 Run: BAL-1_11 0520B 05/20/11 14:14 Run: BAL-1_11 0520B 05/20/11 14:14 101 90 110 Run: BAL-1 _110520B 05/20/1114:12 0.1 10 Run: BAL-1_110520B 05/20/11 14:22 100 90 110 ND-Not detected at the reporting limit. Page 5 of 12 EN:RGY J\\ ·'--'1 ~/\1 Ci~ll ', www.energylab.com Wlftlal Elullellu StiiU 111f1 Helena, MT 877-472-0711 • Billings, MT 800-735-448! • Casper, WY 888-235-0515 Gillette, WY 88&-&8&-7175 • Rapid CHy, SD 818-872-1225 • College Station, lX 888-610-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Report Date: 06/23/11 Work Order: C11 050696 --------------- Analyte Count Result Units Method: A2540 D Sample ID: MBLK1_ Method Blank Solids, Total Suspended TSS@ 105 C ND mg/L Sample ID: LCS1_ Laboratory Control Sample Solids, Total Suspended TSS@ 1 OS C 144 mg/L Sample ID: C11050687-001ADUP Sample Duplicate Solids, Total Suspended TSS@ 105 C 184 mg/L Qualifiers: RL -Analyte reporting limit. MDC-Minimum detectable concentration RL %REC Low Limit High Limit Run: BAL-1_11 0520A 2 Run: BAL-1_110520A 12 72 60 110 Run: BAL-1 _11 0520A 24 ND -Not detected at the reporting limit. RPD RPDLimit Qual 0.0 Batch: R146133 05/20/11 14:59 05/20/11 14:59 05/20/11 15:00 10 Page 6 of 12 EN:RGY 1\fJOJ~, ~r· ...... ll·r-·_. www.energylab.com IMJttlal buiiMu S/lla 19!2 Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 886-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-680-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Count Result Units Method: E200.8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: C11050696-001BMS4 Uranium Sample 10: C11050696-001BMSO Uranium Method: E200.8 Sample 10: MB-29928 Uranium Sample 10: LCS2-29928 Uranium Sample 10: C11050675-001HMS Uranium Sample 10: C11050675-001HMSO Uranium Qualifiers: RL-Analyte reporting limit. MDC -Minimum detectable concentration Method Blank 5E-05 mg/L Laboratory Fortified Blank 0.0524 mg/L Sample Matrix Spike 0.0636 mg/L Sample Matrix Spike Duplicate 0.0701 mg/L Method Blank ND mg/L Laboratory Control Sample 0.102 mg/L Sample Matrix Spike 0.00500 mg/L Sample Matrix Spike Duplicate 0.00514 mg/L Report Date: 06/23/11 Work Order: C11 050696 RL %REC Low Limit High Limit Run: ICPMS2-C_11 0622A 1E-05 Run: ICPMS2-C_11 0622A 0.00030 105 85 115 Run: ICPMS2-C_11 0622A 0.00030 107 70 130 Run: ICPMS2-C_11 0622A 0.00030 120 70 130 Run: ICPMS4-C_11 0531 A 7E-05 Run: ICPMS4-C_11 0531 A 0.00030 102 85 115 Run: ICPMS4-C_11 0531 A 0.00030 105 70 130 Run: ICPMS4-C_11 0531 A 0.00030 109 70 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual 9.7 2.9 Batch: R147252 06/22/11 11 :41 06/22/11 11 :44 06/22/11 13:05 06/22/11 13:07 20 Batch: 29928 05/31/11 18:16 05/31/11 18:18 05/31/11 18:29 05/31/11 18:30 20 Page 7 of 12 EN:RGY ,\i ,::_'Jl/\1 GHil •, www.energytab.com MMtl/ai~SfliU 1M2 Helena, 1\fT 177-472-0711 • Billings, 1\fT BDD-735-4489 • Gasper, WY 811-235-0515 Gillette, WY 118-188-7175 • Rapid City, SO 888-872-1225 • Collage Station, TX 888-810-2218 QAIQC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Method: E900.1 Sample ID: MB-GA-0440 Gross Alpha minus Rn & U Count Result 3 Method Blank 0.1 Gross Alpha minus Rn & U Precision (±) 0.5 Gross Alpha minus Rn & U MDC 0.8 Units pCi/L pCi/L pCi/L Sample ID: LCS-GA-D440 Gross Alpha minus Rn & U Laboratory Control Sample Sample ID: C11050582-010CMS Gross Alpha minus Rn & U Sample ID: C11050582-Q10CMSD Gross Alpha minus Rn & U Qualifiers: RL-Analyte reporting limit. MDC - Minimum detectable concentration 22.6 pCi/L Sample Matrix Spike 44.8 pCi/L Sample Matrix Spike Duplicate 44.3 pCi/L Report Date: 06/23/11 Work Order: C11 050696 RL %REC Low Limit High Limit Run: G542M_11 0613A Run: G542M_110613A 106 70 130 Run: G542M_110613A 95 70 130 Run: G542M_110613A 94 70 130 NO -Not detected at the reporting limit. RPD RPDLimit Qual 1.1 Batch: GA-0440 06/15/11 16:01 u 06/15/11 16:01 06/16/1111:13 06/16/1111:13 26 U -Not detected at minimum detectable concentration Page 8 of 12 EN:RGY ;\ I , \. ~ J I • ; '__, www.energylab.com Ml/fiJal Ixu/llnu Slltu 19!2 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-680-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Count Result Units Method: E903.0 Sample ID: C11050640-D03EMS Radium 226 Sample ID: C11050640-003EMSD Radium 226 Sample ID: MB-RA226-5375 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample ID: LCS-RA226-5375 Radium 226 3 Sample Matrix Spike 13 pCi/L Sample Matrix Spike Duplicate 13 pCi/L Method Blank -0.04 pCi/L 0.1 pCi/L 0.2 pCi/L Laboratory Control Sample 7.5 pCi/L Report Date: 06/23/11 Work Order: C11 050696 RL %REC Low Limit High Limit RPD RPDLimit Qual Run: BERTHOLD 770·1_110520A 103 70 130 Run: BERTHOLD 770-1_110520A 100 m 1~ 3.1 Run: BERTHOLD 770-1 _110520A Run: BERTHOLD 770-1 _110520A 119 85 115 Batch: RA226-5375 05/31/11 10:32 05/31/11 10:32 24.6 05/31 /11 12:05 u 05/31 /11 12:05 s -LCS response is outside of the acceptance range for this analysis. Since the MB, MS, and MSD are acceptable the batch is approved. Method: E903.0 Sample ID: C11050675-001HDUP Radium 226 Radium 226 precision (±) Radium 226 MDC Sample ID: C11050696-001DMS Radium 226 Sample ID: LCS-29926 Radium 226 Sample ID: MB-29928 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 Sample Duplicate -0.041 pCi/L 0.047 pCi/L 0.11 pCi/L Sample Matrix Spike 20 pCi/L Laboratory Control Sample 12 pCi/L 3 Method Blank -0.1 0.1 0.3 pCI/L pCI/L pCi/L MDC-Minimum detectable concentration U -Not detected at minimum detectable concentration 98 102 Run: BERTHOLD 770-2_11 0525A 150 Run: BERTHOLD 770-2_11 0525A 70 130 Run: BERTHOLD 770-2_11 0525A 85 115 Run: BERTHOLD 770-2_110525A NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Batch: RA226-5384 05/31 /11 17:25 379.3 u 05/31 /11 17:25 05/31/11 17:25 05/31/11 17:25 u Page 9 of 12 EI\ERGY , l ~' [?' I ~ •, ,~ www.energylab.com Atll/ftiul fxultllm• SIRu I 151 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&86-7175 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water 2011 Analyte Count Result Units Method: E908.0 Sample ID: C11050675-002HMS Thorium 230 Sample ID: C11050675-002HMSD Thorium 230 Sample ID: LCS-29928 Thorium 230 Sample ID: MB-29928 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Method: E908.0 Sample ID: LCS-RA-TH-IS0-1403 Thorium 230 Sample ID: C11060153-012DMS Thorium 230 Sample ID: C11060153-012DMSD Thorium 230 Sample ID: MB-RA-TH-IS0-1403 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL-Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Sample Matrix Spike 7.9 pCi/L Sample Matrix Spike Duplicate 8.5 pCi/L Laboratory Control Sample 8.5 pCi/L Method Blank 0.04 pCi/L 0.1 pCi/L 0.3 pCi/L Laboratory Control Sample 6.0 pCi/L Sample Matrix Spike 12 pCi/L Sample Matrix Spike Duplicate 15 pCi/L Method Blank -0.02 pCi/L 0.09 pCiiL 0.2 pCi/L Report Date: 06/23/11 Work Order: C11 050696 RL %REC Low Limit High Limit RPD RPDLimit Qual Batch: 29928 Run: EGG-ORTEC_110607A 06/09/11 11 :02 91 70 130 Run: EGG-ORTEC_110607A 100 70 130 7.9 06/09/11 11 :02 37.7 Run: EGG-ORTEC_110607A 87 70 130 Run: EGG-ORTEC_110607A Run: EGG-ORTEC_110610A 102 70 130 Run: EGG-ORTEC_11 061 OA 94 70 130 Run: EGG-ORTEC_11 061 OA 06/09/11 11 :02 06/09/11 11 :02 u Batch: RA-TH-IS0-1403 06/14/11 08:49 06/14/11 13:20 115 70 130 19 06/14/11 13:20 38.9 Run: EGG-ORTEC_11 061 OA ND-Not detected at the reporting limit. 06/14/11 13:20 u U -Not detected at minimum detectable concentration Page 10 of 12 EN:RGY •q,('J 1'\1, I•' '• www.energytab.com AalytiQJ r.xr.u.-Sltlu 1151 Helene, MT 877 ... 72-0711 • Billings, MT 800-735·4489 • Caspar, WY 888-235·0515 Gillette, WY 866·686· 7175 • Rapid City, SO 888-672-1225 • Collage Station, TX 888·690·2218 Workorder Receipt Checklist Denison Mines USA Corp 11111111~111111111111111111111111111~111~111111~11 C11050696 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 5/20/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water-pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0 Yes 0 Yes O Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 4.0'C On Ice Yes 0 Yes 0 Date Received: 5/20/2011 Received by: em Carrier FedEx name: NoD No 0 No 0 No 0 NoD NoD NoD No 0 No 0 NoD NoD No 0 Not Present 0 Not Present D Not Present 0 NoVOA vials submitted 0 Not Applicable O Sample split, filtered, and preserved as necessary for dissolved and suspended analysis. Page 11 of 12 "U Ill 10 (!) ...... N 0 - Chain of Custody and Analytical Request Record Page of LA RO RA TORIES PL J: A~l= PRINT {Provide as much infor m:ttiOn as possible.} -- -- Cv•••j.IOIIIJ Name: Project N8me, PWS Permit, Etc. Sample Origin EPA/State Compliance: Dat;so" f-;n<:S Sem; A11nW>.' 5u.c+'Q.cc. lJtA.+er ~Oil State: w Yes !2( No 0 Report Mail Address: fO flOX fSOCf Contact Name: Phone/Fax: Email: Sampler: (Please Print) Blcw!~n_q UT fSLi5ll R ~ o..n f' ")mer "135 '78 ~a~ I 1--r ~l)et" H611: ~ '1 Invoice Address: InvoiCe Contact & Phone: Purchase Order: Quote/Bottle Order: .scJ.fWl(.. ~,.,~ Special Report/Formats: ~ ~[b W@D@ ~(g@QDl3@'U'l§[Q) .. Contact ELl prior to ~;;;v li> . RUSH sample submittal ~O<n.s::. ~ i=' R for charges and Cooter ID(s): jgcn~Oilii Cl ~ scheduling-See ~~f/n./ ·-> 0 >-iii w Instruction Page Dow 0 EDD/EDT(Eiectronic Data) fl Ul en ro 5: ~ c: :!?1 ~ 1 ~ I 05:--«< -~ ~ "0 Reeei;;emp 0 C 0 POTWNVWTP ~ j 0 c Comments: Format: u <(~1-!2 :i2 :::J u o .._lXII c: <( 0 0 State: 0 LEVEL IV ~ ~ .. FJ,,g (§ : 1--ro 0 Other: 0 NELAC ~ 1--c G)N ~ro· ~ ~ :z: <( 5 On Ice: :J Q)-= a; 3: l-,_ s 2 -o.<lg>o -~ w "E custody sur ·c § >I ~ ~ ~ ... ~ w rn ,._a 1 (/J ""0 (/) j ~ c: On Cooler l-~ •) ) .ll! H Intact y ... en Collection Collection MATRIX J, Signature • N (Name, Location, Interval, etc.) Date Time Match ,c_.U. ,,...,..I Lrul< 'S/IfJ./11 og~o l-W y._ ~ ')L.. ')oL "'-')L' ~ 2 ~/)ADiilt ~ 3 , ~ 4 ~ 5 --= ;:::, 6 7 ~ 8 ~ 9 ! 1/lx'cl.#i 10 <::::: C• .... ...." ..loy ir:il; Date/Tl~ Yfj;.'L f~by(prlnl); uatelllme: :>tgt181 re; -·--IY :f ~n'r :"il;! • .a ~/1·/~ll lO~ _! .. nun Record I by (print): '-.) Dalem me: · SigNJture: '-' R.O<:eived by (print): Oat efT IItle Signaruro: MUST h~:~~ Signed Ke<:e1Vetfby~ '1'11/lJ/meJ'oD;J; !ku ;)I!INJIUre· Sample ni<:nno::>~l· Return to Client: Lab In certain circumstances. samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QNQC Soil samples are collected during the third quarter. This Attachment has been deliberately left blank.