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HomeMy WebLinkAboutDDW-2025-010425October 09, 2025 Dear John Steffan: Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 9/30/25 11:24 am and logged in under work order II05940. All testing is performed according to our current TNI accreditations unless otherwise noted . This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH28005RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE-NOT RELINQUISHED RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: II05940-01 Name: Sampled: Received: 09/30/25 11:24 09/29/25 11:25 SS988-SAMPLING STATION - 01 02 03 Reg ID:Drinking Water - Regular SampleMatrix:UTAH28005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA10/07/25 02:29 EJBU1.910.9 < 0.4 ng/L EPA 533PFMPA10/07/25 02:29 EJBU1.910.4 < 0.5 ng/L EPA 533PFPeA10/07/25 02:29 EJBU1.910.5 < 0.5 ng/L EPA 533PFBS10/07/25 02:29 EJBU1.910.5 < 0.4 ng/L EPA 533PFMBA10/07/25 02:29 EJBU1.910.4 < 0.5 ng/L EPA 533PFEESA10/07/25 02:29 EJBU1.910.5 < 0.3 ng/L EPA 533HFPO-DA 10/07/25 02:29 EJBU1.910.3 < 0.4 ng/L EPA 533NFDHA10/07/25 02:29 EJBU1.910.4 < 0.4 ng/L EPA 5334:2 FTS 10/07/25 02:29 EJBU1.910.4 < 0.4 ng/L EPA 533PFHxS10/07/25 02:29 EJBU1.910.4 < 0.5 ng/L EPA 533PFHpA10/07/25 02:29 EJBU1.910.5 < 1.0 ng/L EPA 533PFHxA10/07/25 02:29 EJBU1.911.0 < 0.5 ng/L EPA 533ADONA10/07/25 02:29 EJBU1.910.5 < 0.5 ng/L EPA 533PFPeS10/07/25 02:29 EJBU1.910.5 < 0.5 ng/L EPA 5336:2 FTS 10/07/25 02:29 EJBU1.910.5 < 0.7 ng/L EPA 533PFOA10/07/25 02:29 EJBU1.910.7 < 0.6 ng/L EPA 533PFHpS10/07/25 02:29 EJBU1.910.6 < 0.5 ng/L EPA 533PFOS10/07/25 02:29 EJBU1.910.5 < 0.5 ng/L EPA 533PFNA10/07/25 02:29 EJBU1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 10/07/25 02:29 EJBU1.910.6 < 0.5 ng/L EPA 5338:2 FTS 10/07/25 02:29 EJBU1.910.5 < 0.4 ng/L EPA 533PFDA10/07/25 02:29 EJBU1.910.4 < 0.5 ng/L EPA 533PFUnA10/07/25 02:29 EJBU1.910.5 < 0.5 ng/L EPA 53311Cl-PF3OUdS 10/07/25 02:29 EJBU1.910.5 < 0.5 ng/L EPA 533PFDoA10/07/25 02:29 EJBU1.910.5 Surrogate: 13C4-PFBA-SURR 97 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C5-PFPeA-SURR 97 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C3-PFBS-SURR 92 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C2-4:2FTS-SURR 105 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C5-PFHxA-SURR 89 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 90 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C4-PFHpA-SURR 90 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C3-PFHxS-SURR 92 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C2-6:2FTS-SURR 96 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C8-PFOA-SURR 88 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C9-PFNA-SURR 84 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C8-PFOS-SURR 94 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C2-8:2FTS-SURR 106 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C6-PFDA-SURR 79 %50-200 10/07/25 02:29 EJB EPA 533 Surrogate: 13C7-PFUnA-SURR 82 %50-200 10/07/25 02:29 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: II05940-01 Name: Sampled: Received: 09/30/25 11:24 09/29/25 11:25 SS988-SAMPLING STATION - 01 02 03 Reg ID:Drinking Water - Regular SampleMatrix:UTAH28005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 95 %50-200 10/07/25 02:29 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B544307 - EPA 533 - EPA 533 Blank (B544307-BLK1)Prepared: 10/01/25 Analyzed: 10/06/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 41.0 ng/L 40.00 103 50-200 Surrogate: 13C5-PFPeA-SURR 39.8 ng/L 40.00 100 50-200 Surrogate: 13C3-PFBS-SURR 36.9 ng/L 37.28 99 50-200 Surrogate: 13C2-4:2FTS-SURR 154 ng/L 150.4 102 50-200 Surrogate: 13C5-PFHxA-SURR 38.8 ng/L 40.00 97 50-200 Surrogate: 13C3-HFPOA-DA-SURR 40.7 ng/L 40.00 102 50-200 Surrogate: 13C4-PFHpA-SURR 39.0 ng/L 40.00 97 50-200 Surrogate: 13C3-PFHxS-SURR 37.4 ng/L 37.92 99 50-200 Surrogate: 13C2-6:2FTS-SURR 153 ng/L 152.0 101 50-200 Surrogate: 13C8-PFOA-SURR 38.4 ng/L 40.00 96 50-200 Surrogate: 13C9-PFNA-SURR 38.9 ng/L 40.00 97 50-200 Surrogate: 13C8-PFOS-SURR 40.3 ng/L 38.32 105 50-200 Surrogate: 13C2-8:2FTS-SURR 158 ng/L 153.6 103 50-200 Surrogate: 13C6-PFDA-SURR 33.4 ng/L 40.00 84 50-200 Surrogate: 13C7-PFUnA-SURR 28.8 ng/L 40.00 72 50-200 Surrogate: 13C2-PFDoA-SURR 35.5 ng/L 40.00 89 50-200 LCS (B544307-BS1)Prepared: 10/01/25 Analyzed: 10/06/25 PFBA 72 ng/L 80.00 90 70-130 PFMPA 67 ng/L 80.00 83 70-130 www.pacelabs.comCustomer #: 72-106174 Page 6 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B544307-BS1)Prepared: 10/01/25 Analyzed: 10/06/25 PFPeA 67 ng/L 80.00 84 70-130 PFBS 61 ng/L 80.00 76 70-130 PFMBA 58 ng/L 80.00 73 70-130 PFEESA 57 ng/L 80.00 72 70-130 NFDHA 62 ng/L 80.00 77 70-130 HFPO-DA 61 ng/L 80.00 76 70-130 4:2 FTS 73 ng/L 80.00 91 70-130 PFHxS 63 ng/L 80.00 79 70-130 PFHpA 61 ng/L 80.00 77 70-130 PFHxA 65 ng/L 80.00 81 70-130 ADONA 62 ng/L 80.00 77 70-130 PFPeS 69 ng/L 80.00 87 70-130 6:2 FTS 72 ng/L 80.00 90 70-130 PFOA 63 ng/L 80.00 79 70-130 PFHpS 61 ng/L 80.00 76 70-130 PFOS 58 ng/L 80.00 72 70-130 PFNA 63 ng/L 80.00 79 70-130 9Cl-PF3ONS 64 ng/L 80.00 80 70-130 8:2 FTS 76 ng/L 80.00 95 70-130 PFDA 64 ng/L 80.00 80 70-130 PFUnA 65 ng/L 80.00 81 70-130 11Cl-PF3OUdS 63 ng/L 80.00 79 70-130 PFDoA 60 ng/L 80.00 75 70-130 Surrogate: 13C4-PFBA-SURR 37.7 ng/L 40.00 94 50-200 Surrogate: 13C5-PFPeA-SURR 36.4 ng/L 40.00 91 50-200 Surrogate: 13C3-PFBS-SURR 35.8 ng/L 37.28 96 50-200 Surrogate: 13C2-4:2FTS-SURR 159 ng/L 150.4 106 50-200 Surrogate: 13C5-PFHxA-SURR 34.6 ng/L 40.00 87 50-200 Surrogate: 13C3-HFPOA-DA-SURR 35.8 ng/L 40.00 89 50-200 Surrogate: 13C4-PFHpA-SURR 35.0 ng/L 40.00 88 50-200 Surrogate: 13C3-PFHxS-SURR 36.0 ng/L 37.92 95 50-200 Surrogate: 13C2-6:2FTS-SURR 154 ng/L 152.0 101 50-200 Surrogate: 13C8-PFOA-SURR 34.8 ng/L 40.00 87 50-200 Surrogate: 13C9-PFNA-SURR 34.3 ng/L 40.00 86 50-200 Surrogate: 13C8-PFOS-SURR 37.5 ng/L 38.32 98 50-200 Surrogate: 13C2-8:2FTS-SURR 163 ng/L 153.6 106 50-200 Surrogate: 13C6-PFDA-SURR 34.1 ng/L 40.00 85 50-200 Surrogate: 13C7-PFUnA-SURR 35.1 ng/L 40.00 88 50-200 Surrogate: 13C2-PFDoA-SURR 43.0 ng/L 40.00 107 50-200 Matrix Spike (B544307-MS1)Sample: II05264-01 Prepared: 10/01/25 Analyzed: 10/06/25 PFBA 79 ng/L 80.58 ND 98 70-130 PFMPA 78 ng/L 80.58 ND 96 70-130 PFPeA 72 ng/L 80.58 ND 90 70-130 PFBS 68 ng/L 80.58 ND 84 70-130 PFMBA 63 ng/L 80.58 ND 78 70-130 PFEESA 63 ng/L 80.58 ND 78 70-130 NFDHA 69 ng/L 80.58 ND 86 70-130 www.pacelabs.comCustomer #: 72-106174 Page 7 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B544307-MS1)Sample: II05264-01 Prepared: 10/01/25 Analyzed: 10/06/25 HFPO-DA 68 ng/L 80.58 ND 85 70-130 PFHxS 67 ng/L 80.58 ND 84 70-130 4:2 FTS 79 ng/L 80.58 ND 98 70-130 PFHpA 69 ng/L 80.58 ND 86 70-130 PFHxA 71 ng/L 80.58 ND 88 70-130 PFPeS 75 ng/L 80.58 ND 94 70-130 ADONA 72 ng/L 80.58 ND 89 70-130 6:2 FTS 79 ng/L 80.58 ND 98 70-130 PFOA 73 ng/L 80.58 ND 90 70-130 PFHpS 69 ng/L 80.58 ND 86 70-130 PFOS 64 ng/L 80.58 ND 80 70-130 PFNA 72 ng/L 80.58 ND 90 70-130 9Cl-PF3ONS 66 ng/L 80.58 ND 82 70-130 8:2 FTS 80 ng/L 80.58 ND 99 70-130 PFDA 69 ng/L 80.58 ND 86 70-130 PFUnA 71 ng/L 80.58 ND 88 70-130 11Cl-PF3OUdS 62 ng/L 80.58 ND 77 70-130 PFDoA 64 ng/L 80.58 ND 79 70-130 Surrogate: 13C4-PFBA-SURR 35.0 ng/L 40.29 87 50-200 Surrogate: 13C5-PFPeA-SURR 39.8 ng/L 40.29 99 50-200 Surrogate: 13C3-PFBS-SURR 34.9 ng/L 37.55 93 50-200 Surrogate: 13C2-4:2FTS-SURR 161 ng/L 151.5 107 50-200 Surrogate: 13C5-PFHxA-SURR 35.0 ng/L 40.29 87 50-200 Surrogate: 13C3-HFPOA-DA-SURR 36.7 ng/L 40.29 91 50-200 Surrogate: 13C4-PFHpA-SURR 34.2 ng/L 40.29 85 50-200 Surrogate: 13C3-PFHxS-SURR 35.9 ng/L 38.20 94 50-200 Surrogate: 13C2-6:2FTS-SURR 156 ng/L 153.1 102 50-200 Surrogate: 13C8-PFOA-SURR 32.7 ng/L 40.29 81 50-200 Surrogate: 13C9-PFNA-SURR 32.1 ng/L 40.29 80 50-200 Surrogate: 13C8-PFOS-SURR 34.7 ng/L 38.60 90 50-200 Surrogate: 13C2-8:2FTS-SURR 155 ng/L 154.7 100 50-200 Surrogate: 13C6-PFDA-SURR 30.3 ng/L 40.29 75 50-200 Surrogate: 13C7-PFUnA-SURR 29.0 ng/L 40.29 72 50-200 Surrogate: 13C2-PFDoA-SURR 36.8 ng/L 40.29 91 50-200 www.pacelabs.comCustomer #: 72-106174 Page 8 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 9 of 12 Page 10 of 12 Page 11 of 12 Page 12 of 12