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HomeMy WebLinkAboutDRC-2012-002402 - 0901a068803258c2DRC-2012-00a402 Energy Fuels Resources (USA) Inc, 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www energyfuels com November 26,2012 Sent VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West P O Box 144850 Salt Lake City, UT 84114-4820 Re: Transmittal of 3rd Quarter 2012 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr Lundberg Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitonng Report for the 3rd Quarter of 2012 as required by the Groundwater Quality Discharge Pernut UGW370004, as well as two CDs each containing a word searchable electronic copy of the report If you should have any questions regarding this report please contact me Yours very truly, ENERGY FUELS RESOURCES (USA) INC. Jo Ann Tischler Director, Compliance CC David C Frydenlund Harold R Roberts David E Turk Katherine A Wemel Central Files ...... ~- /" 2]' P- I lJI:N:RGYFUELS November 26, 2012 Sent VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84114-4820 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 3039742140 www.energyfuels.com Re: Transmittal of 3rd Quarter 2012 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 3rd Quarter of 2012 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly,/ _ • L)i2--~ ENERGY FUELS RESOURCES (USA) INC. JoAnn Tischler Director, Compliance cc: David C. Frydenlund Harold R. Roberts David E. Turk Katherine A. Weinel Central Files White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 3rd Quarter (July through September) 2012 Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 November 26, 2012 TABLE OF CONTENTS 1.0 IN"TRODUCTION ................................................................................................... 1 1.1 Groundwater Discharge Permit Modifications during the Quarter ...................... 1 2.0 GROUNDWATER MONITORING ....................................................................... 1 2.1 Samples and Measurements Taken During the Quarter ....................................... 1 2.1.1 Groundwater Compliance Monitoring .......................................................... 1 2.1.2 Accelerated Groundwater Monitoring .......................................................... 2 2.1.3 Background Well Monitoring ....................................................................... 2 2.1.4 Parameters Analyzed .................................................................................... 3 2.1.5 Groundwater Head Monitoring ..................................................................... 3 2.2 Field Data ............................................................................................................. 3 2.3 Laboratory Results -Quarterly Sampling ........................................... ~ ................ 4 2.3.1 Copy of Laboratory Results .......................................................................... 4 2.3.2 Regulatory Framework and Groundwater Background ................................ 4 2.4 Laboratory Results -Accelerated Monitoring ..................................................... 5 2.4.1 Copy of Laboratory Results .................. ~ ....................................................... 5 2.4.2 Regulatory Framework and Groundwater Background ................................ 5 2.4.3 Compliance Status .............................................................................. -.......... 5 2.5 Depth to Groundwater and Water Table Contour Map ........................................ 6 3.0 QUALITY ASSURANCE AND DATA VALIDATION ....................................... 6 3.1 Field QC Samples ................................................................................................. 6 3.2 Adherence to Mill Sampling SOPs ...................................................................... 7 3.3 Analyte Completeness Review ............................................................................. 7 3.4 Data Validation .................................................................................................... 7 3.4.1 Field Data QAlQC Evaluation ...................................................................... 8 3.4.2 Holding Time Evaluation ............................................................................ 10 3.4.3 Receipt Temperature Evaluation ...................................... : .......................... 10 3.4.4 Analytical Method Checklist ...................................................................... 10 3.4.5 Reporting Limit Evaluation ........................................................................ 10 3.4.6 Trip Blank Evaluation ................................................................................. 11 3.4.7 QAlQC Evaluation for Routine Sample Duplicates ................................... 11 3.4.8 Radiologics Counting Error and Duplicate Evaluation .............................. 11 3.4.9 Other Laboratory QAlQC ........................................................................... 12 4.0 CORRECTIVE ACTION REPORT ...................................................................... 14 5.0 TIME CONCENTRATION PLOTS .................................................. ~ ................... 15 6.0 ELECTRONIC DATA FILES AND FORMAT ................................................... 16 7.0 SIGNATURE AND CERTIFICATION ................................................................ 17 Table 1 Table 2 Table 3 LIST OF TABLES Summary of Well Sampling for the Period Exceedances and ,Acceleration Requirements GWCL Exceedances Through Third Quarter 2012 Under the July 14, 2011 and August 24, 2012 GWDP i INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-IAIB G-2AIB G-3AIB G-4AIB G-SAIB G-6AIB G-7AIB G-8AIB G-9AIB Field Data QAlQC Evaluation Holding Time Evaluation Laboratory Receipt Temperature Check Analytical Method Check Reporting Limit Check Trip Blank Evaluation QAlQC Evaluation for Sample Duplicates Radiologics Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter ii 1.0 INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under Part I.F.1 of State of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the third quarter of 2012 (the "quarter") for Energy Fuels Resources (USA) Inc's. ("EFRI's") White Mesa Uranium Mill (the "Mill"). As required under Parts I.E.1, I.E.2 and I.E.5 of the GWDP this Report includes all recorded field measurements and laboratory analyses for well monitoring conducted during the quarter. 1.1 Groundwater Discharge Permit Modifications during the Quarter During the third quarter of 2012, the approved July 14, 2011 GWDP was revised on August 24,2012. The revision incorporated the EFRI name change from Denison Mines (USA) Corp. No changes were issued to the Groundwater Compliance Limits ("GWCLs") specified in Table 2 or to the groundwater monitoring program described herein. 2.0 GROUNDWATER MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, chloroform contaminant investigation wells and nitrate contaminant investigation wells is attached under Tab A. Groundwater samples and measurements were taken during this reporting period (July through September), as discussed in the remainder of this section. 2.1.1 Groundwater Compliance Monitoring Groundwater samples and field measurements collected during the quarter included quarterly, semi-annual and accelerated monitoring. Accelerated monitoring is discussed below in Section 2.1.2. In the narrative in Sections 2 and 3 of this quarterly report, samples classified as being collected quarterly include those wells which are sampled every quarter and the wells sampled semi-annually. Wells which are sampled routinely every quarter and semi-annually were analyzed for the parameters listed in Table 2 and Part I.E.I.c) 2) ii of the GWDP dated July 14, 2011 and August 24,2012. Table 1 of this report provides an overview of all wells sampled during the current period, along with the required sampling frequency applicable to each well during the current monitoring period, the date samples were collected from each well, and the date(s) analytical data were received from the contract laboratory(ies). Table 1 also indicates which sample numbers are associated with the required duplicates. During this quarter, three wells and one duplicate were resampled. The following is a list of wells which were resampled and the reason for the resampling effort: 1 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc • MW -26 and MW -65 (duplicate of MW -26) were resampled for volatile organic compounds ("VOCs") due to a laboratory issue which resulted in poor agreement between the sample (MW-26) and the duplicate (MW-65) . • MW-28 was resampled for manganese. Manganese exceeded the GWCL in MW- 28 in second quarter 2012. MW-28 was accelerated for manganese in third quarter 2012. The second sample collected for MW-28 during the third quarter was analyzed for manganese. • MW-29 was resampled for Total Dissolved Solids ("TDS") and manganese. Manganese and TDS exceeded their respective GWCLs in MW-29 in second quarter 2012. MW-29 was accelerated for manganese and TDS in third quarter 2012. The second sample collected for MW-29 during the third quarter captured manganese and TDS. 2.1.2 Accelerated Groundwater Monitoring. Accelerated monthly sampling was also performed (quarterly wells accelerated to monthly), and results reported, for the wells indicated in Table 1. The accelerated sampling frequency, analyte list and well list were determined based on the previous analytical results as shown in Table 2. Table 1 provides an overview of the wells sampled for the accelerated monthly program along with the routine sampling frequency as well as the accelerated sampling frequency, the date samples were collected from each well, the associated duplicates and the date( s) which analytical data were received from the contract laboratory(ies). 2.1.3 Background Well Monitoring A requirement was added to the GWDP on February 15,2011, which required the Mill to begin quarterly sampling of wells MW-35, MW-36 and MW-37 to develop eight quarters of background data. MW-35, which was installed in the third quarter 2010, has been sampled quarterly since the fourth quarter of 2010. With the third quarter 2012 sample, eight full quarters of data have been collected for MW -35. Preliminary statistical analysis of the MW-35 data showed extremes in the TDS data. Per the logic flow diagram included as Figure 17 of the New Wells Background Report (INTERA, 2008), extreme values are excluded from the background calculations. The removal of the extremes resulted in less than the eight required data points needed for background calculations. DRC personnel agreed via telephone on October 3, 2012 that EFRI should delay the submission of the MW -35 background report until at least eight quarters of usable data, suitable for background calculations, were collected for all constituents. DRC and EFRI agreed that the background report for MW-35 would be submitted in first quarter 2013 if· at least eight quarters of data were collected for every constituent by that time. If there are not eight data points for each constituent, DRC and EFRI would discuss an alternate schedule or further actions. MW-36 and MW-37, which were installed during the second quarter of 2011, were sampled for the first time during the second quarter of 2011. Quarterly samples will 2 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc continue to be collected until 8 quarters of data are available to complete the background report as required by the GWDP. 2.1.4 Parameters Analyzed All routine quarterly and semi-annual groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E.I.c) 2) ii of the GWDP dated July 14,2011 and August 24, 2012. The accelerated monitoring samples were analyzed for a more limited and specific parameter list as shown in Table 2. 2.1.5 Groundwater Head Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.2 of the GWDP dated February IS, 2011: • The quarterly groundwater compliance monitoring wells (including, MW-34). • Existing monitoring well MW -4 and all of the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3, P-4 and P-S. • Nitrate monitoring wells. • The DR piezometers which were installed during the Southwest Hydrogeologic Investigation. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All water levels used for groundwater contour mapping were measured and recorded within S calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies of all field data sheets recorded in association with the quarterly effort (sampled in July) for the groundwater compliance monitoring wells referred to in paragraph 2.1.1, above. Sampling dates are listed in Table 1. Tab B also includes field data sheets for all resampling efforts conducted during this quarter. Attached under Tab C are copies of all field data sheets recorded in association with the August and September 2012 accelerated monitoring and sampling efforts. 3 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc 2.3 Laboratory Results -Quarterly Sampling 2.3.1 Copy of Laboratory Results All analytical results are provided by one of the Mill's two contract analytical laboratories EL or A W AL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well. Results from analysis of samples collected under the GWDP (i.e:, all regular quarterly and semi-annual samples are provided in Tab E. Also included under Tab E are the results of analyses for duplicate samples as identified in Table 1. The laboratory report dates for samples collected for the August and September accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Table 1. Results from analysis of samples collected for the August and September accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Tab F. Also included under Tab F are the results of analyses for duplicate samples for this sampling effort, as identified in Table 1. Copies of laboratory QAlQuality Control ("QC") Summaries are included with the reported data under their corresponding Tabs. 2.3.2 Regulatory Framework and Groundwater Background Under the GWDP dated July 14, 2011 and August 24, 2012 background groundwater quality has been determined on a well-by-well 'basis, as defined by the mean plus second standard deviation concentration or the equivalent. GWCLs that reflect this background groundwater quality have been set for all monitoring wells except MW-35. It is important to note that the GWDP dated February 15,2011 also set GWCLs for MW-35. The GWCLs for MW-35 have been set at one-quarter of the Utah Groundwater Quality Standard ("GWQS"), pending determination of background for the well, and are not based on eight quarters of data from that well. A background report for MW-35 will be completed after the collection of eight quarters of data for all constituents. Exceedances of the GWCLs determined the accelerated monthly monitoring program implemented during this quarter as noted in Tables 1 and 2. Exceedances of the GWCLs for this quarter are listed in Table 2 for sampling required under the revised GWDP July 14, 2011 and August 24, 2012. Table 3 shows the accelerated sampling program which started in the second quarter 2010 and shows the results and frequency of the accelerated sampling conducted since that time. 4 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW,doc It should be noted, however, that, because the GWCLs have been set at the mean plus second standard deviation, or the equivalent, un-impacted groundwater would normally be expected to exceed the GWCLs approximately 2.5% of the time. Therefore, exceedances are expected in approximately 2.5% of all sample results, and do not necessarily represent impacts to groundwater from Mill operations. 2.4 Laboratory Results -Accelerated Monitoring 2.4.1 Copy of Laboratory Results The analytical results for the accelerated monthly monitoring of the various constituents in certain monitoring wells for the quarter are provided at Tab F. 2.4.2 Regulatory Framework and Groundwater Background As a result of the issuance of a revised GWDP on January 20, 2010, which sets revised GWCLs, all requirements to perform accelerated monitoring under Part I.G.1 of the previous GWDP ceased effective on January 20, 2010, and the effect of the issuance of the revised GWDP was to create a "clean slate" for all constituents in all wells going , forward. This means that accelerated monitoring during this quarter was required under the revised GWDP for only those constituents that exceeded the GWCLs since January 20,2010. 2.4.3 Compliance Status Analytes which have exceeded the GWCLs set forth in the GWDP are summarized in Table 2. The analytes which exceeded their respective GWCLs during the quarter will be sampled on an accelerated schedule as noted in Table 2. Analytes which exceeded their respective GWCLs during 2010 are currently sampled on an accelerated schedule. A review of the accelerated data collected during the quarter indicate that several analytes have exceeded their respective GWCLs for two consecutive sampling periods as reported in EFRI's letter to DRC on November 15, 2012. Table 3 summarizes the results of the accelerated sampling program from first quarter 2010 through third quarter 2012. Part I.G.1 c) of the GWDP states, with respect to exceedances of GWCLs, "that the Permittee shall prepare and submit within 30 calendar days to the Executive Secretary a plan and a time schedule for assessment of the sources, extent and potential dispersion of the contamination, and an evaluation of potential remedial action to restore and maintain groundwater quality to insure that Permit limits will not be exceeded at the compliance monitoring point and that DMT or BAT will be reestablished." EFRI submitted an exceedance notice on November 15, 2012 for the third quarter 2012 results. The summary in the Exceedance Notice includes, for each exceedance, a brief discussion of whether such a plan and schedule is required at this time in light of other actions currently being undertaken by EFRI, as determined by DRC Staff and stated In 5 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc teleconferences with EFRI on April 27 and May 2, 2011 and the Stipulated Consent Agreement ("SCA") dated July 12, 2012. 2.5 Depth to Groundwater and Water Table Contour Map As stated above, a listing of groundwater level readings for the quarter (shown as depth to groundwater in feet) is included under Tab D. The data from Tab D has been interpreted (kriged) and plotted in a water table contour map, provided under Tab H. The water table contour map provides the location and identity of all of the wells and piezometers for which depth to groundwater is recorded. The groundwater elevation at each well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the quarter's sampling event are displayed on the map. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager performed a QAlQC review to confirm compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is' provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QAlQC are discussed in Sections 3.4.4 through 3.4.10 below. The Analytical Laboratories have provided summary reports of the analytical QAlQC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The analytical laboratory QAlQC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tabs E and F. Results of review of the laboratory QAlQC information are provided under Tab G and discussed in Section 3.4, below. 3.1 Field QC Samples The following field QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program: Two duplicate samples were collected during quarterly sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same parameters as permit-required samples. 6 N:\WMM\Required Reports\Groundwater QUaIterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc One duplicate sample was collected during each month of accelerated sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and anal yzed for the same accelerated parameters as the parent sample. Three trip blanks were provided by EL and returned and analyzed with the quarterly monitoring samples. One trip blank per month was provided by EL and returned and analyzed with the accelerated monthly monitoring samples. Two trip blanks were provided by AWAL and returned and analyzed with the quarterly monitoring samples. Accelerated monthly monitoring was no longer required for tetrahydrofuran ("THF") in MW-11 after April 2012, per DRC correspondence dated April 16,2012, therefore, an accelerated monthly sample and the associated trip blank were not necessary in the August and September 2012 monthly sampling events. Rinsate samples were not collected during the quarter because all equipment used during sample collection was dedicated and did not require decontamination. All wells except MW-37 have dedicated pumps for purging and sampling and as such no rinsate blanks samples are required. MW-37 was sampled with a disposable bailer and no rinsate blank was required. A deionized field blank (DIFB) was not required because equipment decontamination was not required and deionized water was not used during this sampling event. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QAlQC requirements established in the QAPs were being adhered to and that the SOP's were implemented, except as described below. 3.3 Analyte Completeness Review All analyses required by the GWDP for the quarterly and semi-annual wells were performed. The accelerated sampling for the semi-annual wells (semi-annual to quarterly) was completed as required by the GWDP and as shown in Tables 2 and 3. The accelerated quarterly sampling (quarterly to monthly) required for this quarter, as shown in Tables 2 and 3, was performed as required. 3.4 Data Validation The QAPs and GWDP identify the data validation steps and data quality control checks required for the groundwater monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QAlQC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting 7 N:\WMM\Required Reports\Groundwater QUaiterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc limit check, a trip blank check, a QAlQC evaluation of routine sample duplicates, a QAlQC evaluation of accelerated sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QAlQC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab G. 3.4.1 Field Data QAlQC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and the stability of the following field parameters (based upon the purging method chosen): conductance, pH, temperature, redox potential, and turbidity. Stability of field parameters and well sampling techniques are dependent on the purging technique employed. Review of the Depth to Water data confirms that all depth measurements were conducted within a five- day period. The results of this quarter's review are provided in Tab G. There are three purging strategies specified in Revision 7.2 of the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% RPD) 3. Purging a well to dryness and stability of a limited list of field parameters after recovery During both the third quarter sampling event and the two monthly events, the purging technique used was two casing volumes with stable field parameters (pH, Conductivity, Redox, temperature and turbidity) except for the following four wells that were purged to dryness: MW-03A, MW-23, MW-24, and MW-37. Based upon the review of the Field Data Sheets, all quarterly and semi-annually sampled locations conformed to the QAP requirement for purging using the two casing volume technique except for MW-37. This well was evacuated to dryness before two casing volumes could be removed. MW -37 has insufficient water to purge using a pump. Due to the small volume of water present, this well is purged and sampled using a disposable bailer. MW-37 conformed to the QAP, Revision 7.2 requirement for sampling low yield wells which includes the collection of three field parameters (pH, specific conductance ["conductivity"] and temperature) immediately prior to and immediately following sample collection. Stabilization of pH, conductivity and temperature were within the QAP, Revision 7.2 required 10% RPD. Review of field sheets indicated that MW-03A, MW-23 and MW-24 were purged dry after two casing volumes were removed. Because these wells were purged dry, the requirements for sampling low yield wells which includes the collection of three field 8 N:\WMM\Required Reports\Oroundwater Quatterly Monitoring Report\2012 Q3\3rd Qtr 2012 OW.doc parameters (pH, specific conductance ["conductivity"] and temperature) immediately prior to and immediately following sample collection was employed. Stabilization of pH, conductivity and temperature were within the QAP, Revision 7.2 required 10% RPD. Additionally, two casing volumes were not purged from MW-26, prior to sampling because MW-26 is a continuously pumped well. If a well is continuously pumped, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if apumping well has been out of service for 48 hours or more, EFRI will follow the purging requirements outlined in Attachment 2-3 of the QAP. The review of the field sheets for compliance with QAP, Revision 7.2 requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least two consecutive measurements. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Turbidity measurements were less than 5 NTU for all of the quarterly and semi- annual wells except MW-12, MW-25, MW-29, MW-29 resample, MW-32 and MW-37. Per the QAP, Revision 7.2, Attachment 2-3, Turbidity measurements prior to sampling were within a 10% RPD for all quarterly and semi -annual wells except MW-03A, MW-23 , MW-24, and MW-37. In all instances these wells were purged to dryness either before two casing volumes were removed (MW-37) or immediately after two casing volumes were removed. Because these wells were purged to dryness, per the QAP, Revision 7.2 Attachment 2-3 turbidity is not required to be measured. The turbidity measurement is provided for information purposes only. • Turbidity measurements were less than 5 NTU for all of the August and September accelerated sampling wells except MW -31 in the September monthly event. As previously stated, the QAP does not require that turbidity be less than 5 NTU. Turbidity measurements prior to sampling were within a 10% RPD for all accelerated sampling wells All other field parameters (conductance, pH, redox potential, and temperature) for all wells were within the required RPD for the quarterly, semi-annual and accelerated sampling. During review of all of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly, semi-annual and accelerated sampling programs to the nearest 0.01 foot. 9 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc EFRI's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspondence dated June 1,2010 and June 24, 2010, EFRI has completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. DRC responded to the redevelopment report via letter on November 15, 2012. Per the DRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab G. All samples were received and analyzed within the required holding time except the VOCs in the September monthly sample of MW-26 and the associated trip blank, which, due to laboratory error, were analyzed outside of the holding time. Corrective actions for this deviation are discussed in Section 4.0. 3.4.3 Receipt Temperature Evaluati~n Chain of Custody sheets (for AWAL) and temperature blank data sheets (for EL) were reviewed to confirm compliance with the QAP requirement in Table 1 that samples be received at 6°C or lower. Sample receipt temperature checks are provided under Tab G. All quarterly, semi -annual and accelerated samples were received within the required temperature limit. It is important to note that per Table 1 in the approved QAP, samples submitted for metals and gross alpha analyses do not have a sample temperature requirement. The metals and gross alpha analyses were shipped with analyses that do have a temperature requirement and as such were shipped on ice. 3.4.4 Analytical Method Checklist All analytical methods reported by both laboratories were checked against the required methods specified in the appropriate revision of Table 1 of the QAP. Analytical method check results are provided in Tab G. The review indicated that all quarterly, semi-annual and accelerated samples were analyzed in accordance with the QAP. 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by both laboratories were checked against the reporting limits specified in the QAP Table 1. Reporting limit evaluations are provided in Tab G. All analytes were measured and reported to the required reporting limits except that several sets of quarterly, semi-annual and accelerated sample results had the reporting limit raised for at least one analyte due to matrix interference and/or 10 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc -lJ sample dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was -higher than the increased detection limit. 3.4.6 Trip Blank Evaluation All trip blank results were reviewed to identify any VOC sample contamination which is the result of sample handling and shipment. Trip blank evaluations are provided in Tab G. All trip blank results associated with both the quarterly, semi-annual and accelerated samples were less than detection level for all VOCs. 3.4.7 QAlQC Evaluation for Routine Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All duplicate results were within a 20% RPD in the quarterly and semi-annual samples. Results of the RPD test are provided under Tab G. All duplicate results were within a 20% RPD in the accelerated samples. Results of the RPD test are provided under Tab G. 3.4.8 Radiologies Counting Error and Duplicate Evaluation Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to or greater than the GWCL shall have a counting variance that is equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. Results of quarterly, semi-annual, and accelerated radiologic sample QC are provided under Tab G. All quarterly, semi-annual, and accelerated radiologic sample results met the counting error requirements specified in the QAP. 11 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc 3.4.9 Other Laboratory QAlQC. Section 9.2 of all revisions of the QAP require that the laboratory's QAlQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab G. All lab QAlQC results from both EL and A W AL samples for compounds regulated under the GWDP met these requirements. There were QC results which did not meet laboratory established acceptance limits, as identified in Tab G and described below. Multiple sets of quarterly, semi-annual and accelerated sample results had the reporting limit raised for at least one analyte due to matrix interference and/or sample dilution. In all cases the reported value for the analyte was higher than the increased detection limit. Data are qualified by the laboratory with a "D" flag when the reporting limit is raised due to dilution or matrix interferences. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • For method E900.1, used to determine gross alpha, a sample duplicate was used instead of a MSD. All qualifiers, and the corresponding explanations reported in the QAlQC Summary Reports for any of the check samples for any of the analytical methods were reviewed by the QA Manager. The QAP, Section 8.1.2 require that a MSIMSD pair be analyzed with each analytical batch. The QAPs do not specify acceptance limits for the MSIMSD pair, and the QAP does not specify that the MSIMSD pair be prepared on EFRI samples only. Acceptance limits for MSIMSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the requirements in the QAP, to analyze a MSIMSD pair with each analytical batch, were met. While the QAP does not 12 N:\WMM\Required Reports\Oroundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 OW.doc require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QAlQC Summary Reports indicates that the MSIMSDs recoveries and the associated RPDs for all quarterly and semi-annual samples were within acceptable laboratory limits for all regulated compounds except as indicated in Tab G. The EL MS recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference. Matrix interferences are applicable to the individual sample results only. Furthermore, several of the MSIMSD samples in Work Order Numbers C12070448, C12070741, C12080830, and C12080143, which were spiked for the MSIMSD analyses, were not collected at the Mill, and as such the matrix interference is not applicable to the Mill samples reported herein. The requirement in the QAP to analyze a MSIMSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QAlQC Summary Reports indicates that the MSIMSDs recoveries and the associated RPDs for all accelerated samples were within acceptable laboratory limits for all regulated compounds except as indicated in Tab G. The recoveries and RPDs which are outside of the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above the acceptance limits are indicative of matrix interference. Furthermore, the MSIMSD sample in Work Order Number C12090804 that was spiked for the MSIMSD analyses, were not collected at the Mill, and as such the matrix interference is not applicable to the Mill samples reported herein. The requirement in the QAP to analyze a MSIMSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses but the QAP does not specify acceptance limits for surrogate recoveries. The information from the Laboratory QAlQC Summary Reports indicates that the surrogate recoveries for all quarterly, semi -annual and accelerated samples were within acceptable laboratory limits for all surrogate compounds except as indicated in Tab G. The surrogate compounds outside of acceptance limits, are most likely the result of laboratory spiking compound degradation. This is apparent because the same surrogate compound was outside of compliance limits in all samples analyzed within a specific period of time and in the same Work Order. There is no effect on the quality or usability of the data because there are multiple surrogates added to each sample and all other surrogates were within limits. Furthermore, there are no requirements in the QAP for surrogate recoveries. Since surrogate compounds were added to all of the organic analyses as required by the QAP, the data are compliant with the requirements in the QAP. The information from the Laboratory QAlQC Summary Reports indicates that the LCS recoveries for both the quarterly and accelerated samples were within acceptable laboratory limits for all LCS compounds except as noted in Tab G. As indicated on Tab 13 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc G, the LCS recoveries which were outside of acceptance limits were noted for the same analysis within the same month. The LCS recoveries outside of acceptance limits are most likely due to poor spiking techniques. It is important to note that there is no requirement in the QAP for LCS recovery assessment. All revisions of the QAP, Section 8.1.2 requires that each analytical batch shall be accompanied by a method blank. All analytical batches routinely contain a blank, which is a blank sample made and carried through all analytical steps. For the Mill samples, a method blank was prepared for all analytical methods. Per the approved QAP, contamination detected in analysis of method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. QAP Revision 7.2 states that non-conformance conditions will exist when contaminant levels in the samples(s) are not order of magnitude greater than the blank result. One analyte was reported in the method blanks from EL for the quarterly samples. Method blank results are included in Tab E. In all cases where the associated sample reported a positive detection, the method sample results were greater than an order of magnitude relative to the method blank results reported, that is the detections meet the QAP criteria. The method blank detections reported by EL do not affect the quality or usability of the data due to the high level of the constituents in the samples relative to the associated method blank concentrations. Additionally, blank detections are indicative of a false positive or high bias to the sample results as the laboratory contribution to the results would likely cause higher sample results. The requirement in the QAP to analyze a method blank with each batch and evaluate the results has been completed as required. 4.0 CORRECTIVE ACTION REPORT There is one corrective action resulting from third quarter 2012 groundwater sampling event. Necessary corrective actions identified during the current monitoring period are described below, in accordance with Part I.F.1.e of the GWDP Identification and Definition of the Problem The September monthly VOC sample from MW-26 and the associated trip blank were analyzed outside of the required holding time. All other samples were analyzed within the required holding time. This deviation was due to laboratory error. EFRI was not informed by the laboratory of the holding time issue until October 12, 2012 which prevented resampling of the September monthly compliance sample. Assignment of Responsibility for Investigation of the Problem The problem has been investigated by the QA Manager. 14 N:\WMM\Required Reports\Oroundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 OW.doc Investigation and Determination of Cause of the Problem The samples were collected on September 19, 2012 and were received by the laboratory on September 21, 2012 which is more than sufficient time to analyze two samples from this sampling event within the required holding time, i.e. the monthly sampling events conducted by EFRI contain only one groundwater sample and one trip blank for the analysis of VOCs. The samples were analyzed on October 6, 2012. Determination of a Corrective Action to Eliminate the Problem The samples were analyzed outside of the required holding time due to laboratory error. The samples were received with more than sufficient time to complete the analysis of two samples within the required holding time. EFRI has determined this issue is related to the laboratory and not due to the action or inaction of EFRI. In order to prevent the recurrence of these types of laboratory errors which have increased in recent periods, EFRI has decided to change analytical laboratories. EFRI has completed negotiations with alternate Utah-certified laboratories and has changed laboratories for the fourth quarter 2012 sampling event. Assigning and Accepting Responsibility for Implementing the Corrective Action It will be the joint responsibility of the Director, Compliance and the Quality Assurance Manager to contract alternate Utah-certified laboratories. Implementing the Corrective Action and Evaluating Effectiveness EFRI has contacted the current laboratory to make them aware of the issues. In addition, EFRI has contracted with alternate Utah-certified laboratories for the fourth quarter 2012 sampling event. The sample receipt data will be assessed as samples are received at the new laboratories to determine if any further action is necessary. Verifying That the Corrective Action Has Eliminated the Problem Verification that samples are analyzed within required holding time, will occur during the assessment of data collected from the fourth quarter 2012 sampling event. 5.0 TIME CONCENTRATION PLOTS Time concentration plots for each monitoring well for the following constituents: chloride, fluoride, sulfate, and uranium, are included under Tab I. All data points collected to date are reflected on the plots. Time concentration plots included in groundwater reports prior to and including first quarter 2012 did not include data which were determined to be outliers using the statistical methods used for the background determinations at the Mill. Based on 15 N:\WMM\Required Reports\Oroundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 OW.doc conversations with DRC, all data have been included in the current quarterly time concentration plots. All future time concentration plots will include all data points. 6.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Executive Secretary electronic copies of all laboratory results from groundwater quality monitoring conducted during the quarter in Comma Separated Values ("CSV") format. A copy of the transmittal e-mail is included under Tab J. 16 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc I 7.0 SIGNATURE AND CERTIFICATION This document was prepared'by Energy Fuels Resources (USA) Inc. on November 26, 2012. ENERGY FUELS RESOURCES (USA) INC. By: David . F yden und Senior Vice Pres· dent, Regulatory Affairs and General Counsel 17 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant pen a ties for submitting false information, including the possibility of fine and r kno lng violations. Davi Senior Vice Presi ent, Regulatory Affairs and General Counsel Energy Fuels Resources (USA) Inc. 18 N:\WMM\Required Reports\Groundwater Quarterly Monitoring Report\2012 Q3\3rd Qtr 2012 GW.doc Tables Table 1: Summary of Well Sampling for Q3 2012 . Purpose for Sampling Well Normal Frequency. this Quarter Sample Date .Date of Lab Report . Quarterly Samples MW-ll Quarterly Quarterly 7111/2012 8110/2012 [8/28/2012] MW-14 Quarterly Quarterly 7/11/2012 8110/2012 [8/28/2012] MW-25 Quarterly Quarterly 711012012 8110/2012 [8/28/2012] MW-26 Quarterly Quarterly 7/1112012 8110/2012 [8/28/2012] MW-26 resample* Quarterly Quarterly 8116/2012 8/30/2012 MW-30 Quarterly Quarterly 7110/2012 8110/2012 [8/28/2012] MW-31 Quarterly Quarterly 7/912012 8110/2012 [8/28/2012] MW-35 Quarterly Background 711012012 8/10/2012 [8/28/2012] MW-36 Quarterly Background 711112012 8/10/2012 [8/28/2012] MW-37 Quarterly Background 7/3012012 8/24/2012 [8114/2012] MW-65 1 per Batch Duplicate of MW-26 711112012 8/10/2012 [8/28/2012] MW-65 resample* 1 per Batch Duplicate of MW-26 8116/2012 8/30/2012 . Accelerated Samples Accelerated Quarterly Samples MW-2 Semi-annually Accelerated 7116/2012 8114/2012 MW-3 Semi-annually Accelerated 7118/2012 8114/2012 MW-3A Semi-annually Accelerated 711912012 8114/2012 MW-5 Semi-annually Accelerated 7116/2012 8114/2012 MW-12 Semi-annually Accelerated 711712012 8114/2012 MW-15 Semi -annually Accelerated 711712012 8114/2012 MW-18 Semi -annually Accelerated 7118/2012 8114/2012 MW-19 Semi-annually Accelerated 711912012 8114/2012 MW-23 Semi-annually Accelerated 7117/2012 8114/2012 MW-24 Semi -annually Accelerated 7118/2012 8/14/2012 MW-27 Semi -annually Accelerated 711612012 8114/2012 MW-28 Semi -annually Accelerated 7/1612012 8/14/2012 MW-28 Resample Semi-annually Accelerated 81112012 8/24/2012 MW-29 Semi-annually Accelerated 711012012 8/10/2012 MW-29 Resample Semi -annually Accelerated 81112012 8/24/2012 MW-32 Semi -annually Accelerated 7/912012 8/10/2012 MW-70 1 per Batch Duplicate of MW-03 711812012 8/14/2012 Accelerated August Monthly MW-11 Monthly Accelerated 817/2012 915/2012 MW-14 Monthly Accelerated 81712012 91512012 MW-25 Monthly Accelerated 8/612012 9/5/2012 MW-26 Monthly Accelerated 8/8/2012 9/5/2012 MW-30 Monthly Accelerated 81712012 915/2012 MW-3l Monthly Accelerated 8/6/2012 9/5/2012 MW-35 Monthly Accelerated 8/8/2012 9/5/2012 MW-65 1 per Batch Duplicate of MW-14 817/2012 915/2012 Accelerated September Monthly MW-ll Monthly Accelerated 9/1912012 lO/1712012 MW-14 Monthly Accelerated 911812012 lOI17120l2 MW-25 Monthly Accelerated 9/1812012 lOI17/2012 MW-26 Monthly Accelerated 911912012 lOI17/2012 MW-30 Monthly Accelerated 911912012 lO/17/2012 MW-31 Monthly Accelerated 9118/2012 lOI17/2012 MW-35 Monthly Accelerated 9/1912012 lOI17/20l2 MW-65 1 per Batch Duplicate ofMW-35 9/1912012 lOI17/2012 Notes: Date in brackets depicts the date that tetrahydrofuran and tin were reported from American West Analytical Laboratories. All other VOCs and metals were reported from Energy Laboratories. * MW-26 and MW-65 were resampled for VOCs only due to poor samplelduplicate agreement. Table 2 " " First Result Monitoriilg Well Constituent Exceeding GWCL GWCLin Exceeding the Routine Sample (Water Class) 'Current,GWDP Frequency GWCL Quarterly Wells Accelerated to MoniWy Samplingl MW-11 (Class II) Manganese (ugIL) 131.29 134 Quarterly MW-14 (Class Ill) Manganese (ugIL) 2230.30 2360 Quarterly Field pH (S.U.) 6.5 - 8.5 6.45 Quarterly MW-25 (Class Ill) Uranium (ug/L) 6.5 6.57 Quarterly MW -26 (Class Ill) Nitrate + Nitrite (as N) (mgIL) 0.62 1.3 Quarterly Uranium (ugIL) 41.8 58.7 Quarterly Chloroform (ug/L) 70 700 Quarterly Chloride (mg/L) 58.31 72 Quarterly Methylene Chloride (ug/L) 5 9.9 Ouarterly Field pH (S.U.) 6.74 -8.5 6.59 Quarterly MW-30 (Class II) Nitrate + Nitrite (as N) (mgIL) 2.5 16.1 Quarterly Chloride (mgIL) 128 134 Quarterly Uranium (ugIL) 8.32 9.83 Quarterly Selenium (ugIL) 34 35.3 Quarterly MW-31 (Class Ill) Nitrate + Nitrite (as N) (mgIL) 5 21.7 Quarterly TDS (mgIL) 1320 1330 Quarterly Sulfate (mgIL) 532 539 Quarterly Selenium (ugIL) 71 74 Quarterly Chloride (mglL) 143 145 Quarterly MW-35 (Class II) Uranium (uglL) 7.5 21.7 Quarterly Thallium (uglL) 0.5 1.14 Quarterly Selenium (uglL) 12.5 19.7 Quarterly Gross Alpha minus Rn & U (pCiIL) 3.75 4.5 Quarterly Manganese (uglL) 200 369 Quarterly Semi-Annual Wells Accelerated to Quarterly Samplingl Monitoring Well Constituent Exceeding GWCL GWCLin First Result Sample MW-2 (Class Ill) Gross Alpha minus Rn & U (pCiIL) 3.2 3.5 Semi-Annually MW-3 (Class III) Selenium (ugIL) 37 37.2 Semi-Annually Field pH (S.U.) 6.5 -8.5 6.14 (6.25) Semi-Annually Fluoride (mgIL) 0.68 0.71 Semi-Annually MW-3A (Class III) Field pH (S.U.) 6,5 - 8.5 6.23 (6.24) Semi-Annually Sulfate (mg/l) 3640 3680 Semi-Annually TDS (mg/L) 5805 5860 Semi-Annually Selenium (ugIL) 89 94.8 Semi-Annually MW-5 (Class II) Uranium (ugJLl 7.5 11.6 Semi-Annually MW-12 (Class Ill) Field pH (S.U.) 6.5 -8.5 6.47 Semi-Annually Selenium (ugIL) 25 25.7 Semi-Annually MW-15 (Class III) Selenium (ugIL) 128.7 152 Semi-Annually Iron (uglL) 81.7 137 Semi-Annually MW-18 (Class Ill) Thallium (ugIL) 1.95 3.73 Semi-Annually Sulfate (mgIL) 1938.9 1950 Semi-Annually Field pH (S.U.) 6.25-8.5 6.2 Semi-Annually TDS (mg/L) 3198.77 3280 Semi-Annually MW-19 (Class Ill) Nitrate + Nitrite (as N) (mgIL) 2.83 4 Semi-Annually Field pH (S.U.) 6.78-8.5 6.61 (6.66) Semi-Annually MW -23 (Class III) Manganese (ug/L) 550 551 Semi-Annually Field pH (S.U.) 6.5 -8.5 6.18 Semi-Annually MW-24 (Class Ill) Cadmium (ugIL) 2.5 4.28 Semi-Annually Thallium (ug/L) 1 1.3 Semi-Annually Field pH (S.U.) 6.5 - 8.5 5.91 (5:78) Semi-Annually MW -27 (Class III) Nitrate + Nitrite (as N) (mgIL) 5.6 5.8 Semi-Annually Chloride (mgIL) 38 42 Semi-Annually Gross Alpha minus Rn & U (pCiIL) 2 2.4 Semi-Annually Sulfate (mgIL) 462 469 Semi-Annually Field pH (S.U.) 6.5 -8.5 6.39 Semi-Annually TDS (mgIL) 1075 1160 Semi-Annually MW -28 (Class Ill) Chloride (mgIL) 105 108 Semi-Annually Manganese (ugIL) 1837 1850 Semi-Annually Field pH (S.U.) 6.1-8.5 5.67 Semi-Annually MW-29 (Class Ill) Field pH (S.U.) 6.46 - 8.5 6.17 Semi-Annually Manganese (ugIL) 5624 6140 Semi-Annually TDS (mgIL) 4400 4600 Semi-Annually Iron (ugIL) 1869 3010 Semi-Annually MW-32 (Class III) Gross Alpha minus Rn & U (pCiIL) 3.33 5.4 Semi-Annually Field pH (S.U.) 6.4 -8.5 6.03 Semi-Annually Notes: I GWCL Values are taken from July 14,_2011 and August 24, 2012 y~rsion~ of the GWI?p. sample period. Accelerated Exceedance ' Start of Accelerated Frequency Sample Period Monitoring , , Monthly Q12010 May 2010 Monthly Q22012 August 2012 Monthly Q12010 May 2010 Monthly Q32010 January 2011 Monthly Q12010 May 2010 Monthly Q12010 May 2010 Monthly Q12010 May 20 10 Monthly Q12010 May 2010 Monthly Q22010 June 2010 Monthly Q12010 May 2010 Monthly Q12010 May 2010 Monthly Q12011 May 2011 Monthly Q42011 March 2012 Monthly Q22010 July 2010 Monthly Q12010 May 2010 Monthly Q32010 January 2011 Monthly Q42010 March 2011 Monthly Q32012 December 2012 Monthly Q12011 May 2011 Monthly Q32011 July 2011 Monthly Q42011 July 2011 Monthly Q12012 June 2012 Monthly Q32011 Q42011 Monthly Q32011 July 2011 Accelerated Exceedance Start of Accelerated Quarterly Q42010 Q12011 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q42010 Q12011 Ouarterly 042010 012011 Quarterly Q42010 Q12011 Quarterly Q22010 Q32010 Quarterly Q22012 Q32012 Quarterly Q42011 Q12012 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q42011 Q12012 Quarterly Q22010 Q32010 Quarterly Q42011 012012 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q42010 Q12011 Quarterly Q22010 Q32010 Quarterly Q32011 Q42011 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 Quarterly Q22012 Q32012 Quarterly Q22010 Q32010 Quarterly Q42010 Q22011 Quarterly Q22012 Q32012 Quarterly Q22012 Q32012 Quarterly Q32011 Q42011 Quarterly Q22010 Q32010 Quarterly Q22010 Q32010 a e -xcee ances T bl 3 GWCLE d Th' dQ Ir uarter 2 012 4 under theAugust 2 ,201 2G WDP ~j i!iIIOoll' III, ,.,Q12010 Results ,'4l ,1Ili ff III Q2 2010 Results ·111 .. IIIIi !Ii Q3 2010 Results r<i ~ liS "II 101'" Q4 2010 Results 0 .1ilI1'll '" .J ... 'i, .. '"" " Monitoring ~. :, I!i " . 111_' 1 0 .... ... A:gusflbl0 :.'< • '!. ~ October:t o ." .. "II Constituent Exceeding . GWCLin . Ql 2010 Sample Q12010 Q22010 Q22010 May 2010 o May, 2010 June 2010 June 2010 July 2010 July 2010 .~ October 2010 Q42010 December 2010 December 2010 Well (Water August 24, 2012 Monthly Monthly " Monthly Monthly Monthly . Monthl~ S'(onthly August 2010 Q32010 ~ Q32010 Monthly Q4 2010 . t~Mo thly Sample .~ . GWCL Date Result Sample Date : Result Monthly Result Sample Date Ii Result Monthly Sam Ie Sample Date '" Result Monthly Result Class) GWDP Sample Date Result Sample Dat: R~,u1t Sample Date Result Sample I?ate Date !II Result Date '. I' ~ ~, 0 ~ ,.; ,~ ,C" -11', II Required Quarterly Sampling Wells .... $;. ~, II II .... 1i'I.,III .. .11 ." <, ~ MW-11 (Class Manganese (ug/L) 131.29 2/10/10 134 4/28/10 137 5/24/10 122 6116/10 99 II) 7120110 123 8/25/10 138 9/8/10 128 10/20/10 141 11111110 133 12/15/10 158 MW-14 (Class Manganese (ug/L) 2230.30 2060 2070 NA NA NA NA 1920 NA 1980 NA ill) 2/2/10 4/21/10 5/21/10 6/16/10 7120110 8125/10 9/8/10 10/20/10 11110/10 12/15/10 Field pH (S.U.) 6.5 -8.5 6.45 6.29 6.36 6.45 7.19 6.48 6.51 6.60 6.37 6.47 MW-25 (Class Field pH (S.U.) 6.5 -8.5 6.53 7.2 NS NA NS NA NS NA NS NA 6.58 NS NA 6.36 NS NA ill) 2/26/2010 4/28/2010 9/8/2010 11110/10 Uranium 6.5 5.93 6.43 NS NA NS NA NS NA NS NA 6.57 NS NA 5.89 NS NA Nitrate + Nitrite (as N) 0.62 1.3 2 0.3 0.4 0.6 0.6 0.7 0.4 0.2 0.4 (mg/L) Uranium (ug/L) 41.8 58.7 66.7 37.4 36.6 34.4 71.8 72.7 37.5 30.4 29.6 Chloroform (ug/L) 70 700 1700 800 940 900 2800 2100 1000 1900 1400 MW-26 (Class Chloride (mg/L) 58.31 72 57 80 47 52 49 64 52 48 52 ill) 2/2/10 4/22110 5/21/10 6116110 7/21110 8116/10 9/26/10 10/20/10 11115/10 12/15110 Field pH (S.U.) 6.74 -8.5 6.59 7.18 6.36 6.98 6.45 6.39 6.60 6.61 6.49 6.45 Dichloromethane (Methylene Chloride) 5 1 9.9 NR 2.2 12 24 45 5.5 16 1.2 (ug/L) IDS (mg/L) 3284.19 3100 ~ 3280 NS NS NS NS 3440 NS 3140 NS Nitrate + Nitrite (as N) 2.5 16.1 15.8 17 15.3 7/21110 16 8/24110 16 15 15 /5 16 (mg/L) MW-30 (Class Chloride (mg/L) 128 127 97 NS NS NS NS NS NS III NS 126 NS II) Field pH (S.U.) 6.5 -8.5 2/9/10 6.81 4/27110 6.55 5/21/10 6.62 6115/10 7.47 7/21/2010 6.82 8/24/10 6.73 9/14/10 6.80 10/19/10 6.77 1119/10 6.75 12/14/10 6.65 Uranium (ug/L) 8.32 6.82 6.82 NS NS NS NS NS NS 7.10 NS 6.64 NS Selenium (ug/L) 34 32 35.3 NS NS 7/27/10 33.5 8124/10 35.6 32.6 32.4 32.2 30.5 Nitrate + Nitrite (as N) 5 21.7 22.5 5/21/10 23 6115/10 21.1 7/21/10 20 8/24110 22 21 10/19/10 20 20 20 (mg/L) IDS (mg/L) 1320 1150 1220 NS NA NS NA NS NA NS NA 1330 NS NA 1320 NS MW-31 (Class Chloride (mg/L) 143 2/9110 128 128 NS NA NS NA NS NA NS NA 139 NS NA 138 NS ill) Selenium (ug/L) 71 4/20/10 9/13/10 1119/10 12/14/10 60.8 59.6 NS NA NS NA NS NA NS NA 64.4 NS NA 60 NS Field pH (S.U.) 6.5 -8.5 . 6.96 7.38 5/21/10 6.95 6115110 7.01 7121/10 7.8 8124/10 7.1 7.66 10/19/10 6.92 6.98 6.95 Sulfate (mg/L) .532 507 522 NS NA NS NA NS NA NS NA 527 NS NA 539 NS Manganese (ug/L) 200 NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA 698 NS NA Thallium (ug/l) 0.5 NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA 1.14 NS NA MW-35 (Class Gross Alpha minus Rn & U 3.75 NS NA NS NA NS NA NS NA NS NS 2.6 NS NA II) (pCi/L) NA NS NA NS NA NA 11130/10 Selenium (ug/L) 12.5 NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA ND NS NA Uranium (ug/L) 7.5 NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA 27.2 NS NA '" (f; " 'Required Semi-Annual Sampling Wells II II III ", .. i '"" " MW-2 (Class Gross Alpha minus Rn & U 3.2 NS NA 1.2 NS NA NS 3.5 NS ill) (pCi/L) NA NS NA NS NA NS NA NS NA NA Selenium (ug/L) 37 MW-3 (Class NS NA 37.2 NS NA NS NA NS NA NS NA 35.5 NS NA 38.8 NS NA ill) Field pH (S.U.) 6.5 -8.5 NS NA 5/3/10 6.14 (6.25) NS NA NS NA NS NA NS NA 9/20/10 6.39 NS NA 11/19/10 6.35 NS NA Fluoride (Mg/L) 0.68 NS NA 0.71 NS NA NS NA NS NA NS NA 0.63 NS NA 0.77 NS NA Field pH (S.U.) 6.5 -8.5 NS NA 6.23 (6.24) NS NA NS NA NS NA NS NA 6.42 NS NA 6.21 NS NA MW-3A (Class ill) Sulfate (mg/L) 3640 NS NA 5/4/10 3680 NS NA NS NA NS NA NS NA 9/21110 3630 NS NA 11122/10 3850 NS NA IDS (mg/L) 5805 NS NA 5860 NS NA NS NA NS NA NS NA 5470 NS NA 5330 NS NA Selenium (ug/L) 89 NS NA 81.4 NS NA NS NA NS NA NS NA NS NS NA 94.8 NS NA MW-5 (Class Uranium (ug/L) 7.5 NS NA II) 4/26/10 0.39 NS NA NS NA NS NA NS NA NS NA NS NA 11111/10 11.6 NS NA MW-12 (Class Field pH (S.U.) 6.5 -8.S NS NA 7.16 NS NA NS NA NS NA NS NA 6.62 NS NA 6.47 NS NA ill) Selenium (ug/L) 25 NS 4/27/10 9/20/10 11119/10 NA 25.7 NS NA NS NA NS NA NS NA 31.9 NS NA 27.6 NS NA MW-15 (Class Selenium (ug/L) 128.7 NS NA 100 NS NA NS NA NS NA NS NA NA NS NA 99.5 NS NA ill) 4/21110 NS 11111110 Iron (ug/L) 81.7 NS NA ND NS NA NS NA NS NA NS NA NA NS NA ND NS NA Thallium (ug/l) 1.95 NS NA 3.73 NS NA NS NA NS NA NS NA 3.64 NS NA 3.57 NS NA MW-18 (Class ill) Sulfate (mg/L) 1938.9 NS NA 5/4110 1950 NS NA NS NA NS NA NS NA 9115/10 1930 NS NA 11118/10 1910 NS NA Field pH (S.U.) 6.25-8.5 NS NA 6.2 NS NA NS NA NS NA NS NA 7.23 NS NA 6.37 NS NA IDS (mg/L) 3198.77 NS NA 3280 NS NA NS NA NS NA NS NA 3190 NS NA 3030 NS NA o _"" '" '" ..... '1:1 ~ ,: Q1 2010 Results ~JJ to! ~ Monitoring Constituent .Exceeding GWCLin Well (Water Ql Sample Date GWCE Current GWDP Class) !II • MW-19 (Class Field pH (S.U.) 6.78-8.5 Ill) Nitrate + Nitrite (as N) (mg/L) 2.83 MW-23 (Class Field pH (S.U.) 6.5 -8.5 Ill) Manganese (ug/L) 550 Cadmium (ug/L) 2.5 MW-24 (Class Thallium (ug/L) 1 Ill) Field pH (S.U.) 6.5 -8.5 Nitrate + Nitrite (as N) 5.6 (mg/L) Chloride (mg/L) 38 MW-27 (Class Sulfate (mg/L) 462 Ill) Field pH (S.U.) 6.5-8.5 IDS (mg/L) 1075 Gross Alpha minus Rn & U 2 (pCi/L) Chloride (mg/L) 105 MW-28 (Class Manganese (ug/L) 1837 Ill) Field pH (S.U.) 6.1 -8.5 Iron (ug/L) 1869 Manganese (ug/L) 5624 MW-29 (Class IDS (mg/L) 4400 Ill) Field pH (S.U.) 6.46 -8.5 Gross Alpha minus Rn & U 3.33 MW-32 (Class (pCi/L) Ill) Field pH (S.U.) 6.4 -8.5 Notes: GWCL values are taken from February 15, 2011 version of GWDP. NS = Not Required and Not Sampled NR = Required and Not Reported NA = Not Applicable Exceedances are shown in yellow .111 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Values in () parentheses are the field pH measurements for the resampled analyses. .. Ql Result Ii ~ ... J' NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ~~-.ti! .Ii "Q2 2010 ResultS "'!" W" 51. I?lI IJIEI. .. .. I~ II.lr '" I" Q2Sample " ~ May Monthly May June Monthly'" June Monthly , July, Monthly July Monthly I:!i.Q2Result .'" Monthly Date Sample Date I· Sample Date Result Sample Date Result Result iii , .. ... Kjii 'iI' ~ ~ . II Required Semi-Annual Sampling Wells, continued -~ ',~. 6.61 (6.66) NS NA NS NA NS NA 5/4/10 2.6 NS NA NS NA NS NA 4/22/10 6.18 NS NA NS NA NS NA 184 NS NA NS NA NS NA 4.28 NS NA NS NA NS NA 5/6/10 1.3 NS NA NS NA NS NA 5.91 (5.78) NS NA NS NA NS NA 5.8 NS NA NS NA NS NA 42 NS NA NS NA NS NA 469 NS NA NS NA NS NA 5/3/10 6.78 NS NA NS NA NS NA 1160 NS NA NS NA NS NA 1.6 NS NA NS NA NS NA 108 NS NA NS NA NS NA 1550 NS NA 4/19/10 NS NA NS NA 5.67 NS NA NS NA NS NA 1630 NS NA NS NA NS NA 4820 NS NA NS NA NS NA 4/27110 4400 NS NA NS NA NS NA 6.82 NS NA NS NA NS NA 4.5 NS NA NS NA NS NA 4120110 6.03 NS NA NS NA NS NA suant to the October 26, 2011 DRC letter gross alpha monitoring in MW -26 reterned to the routine frquency of quarteFly. These samples were inadvertantly collected and are for information only. Q3t~010 Resuits c;!1~'. III !t,,~ '" '-, PO 3' .. "!' ~ ., .... 1'1: Q4 2010 Results ,.-~ -'Ill' '-." 1ljI' ~ ... n ~ " ", I· ,~ August August Monthly .Q3Sample October III October. Q4Sample ' December ." 1111 December Monthly Q3Resuit Monthly Sample Monthly Q4'Resuit Monthly Sample Result 1'1' Date Result Date Date Monthly Result Sample Date '. Date I, 1\ ~ • ~ .1'1:0 .111 ~ ~ "'" !D !II I!I . ~ ." .. NS NA 6.93 NS NA 6.8 NS NA 9115/10 11/18/10 NS NA NS NA NA 2,4 NS NA NS NA 9/14/10 7.05 NS NA 6.44 NS NA 11/22110 NS NA NS NS NA 65 NS NA NS NA 5.06 NS NA 3.22 NS NA NS NA 9121/10 1.57 NS NA 11/17/10 1.09 NS NA NS NA 6.64 NS NA 6.1 NS NA NS NA 5.9 NS NA 5.7 NS NA NS NA 42 NS NA 45 NS NA NS NA 461 NS NA 452 NS NA NS NA 9114110 7.68 NS NA 11112110 6.89 NS NA NS NA 1060 NS NA 1110 NS NA NS NA NA NS NA 2.4 NS NA NS NA 106 NS NA 107 NS NA NS NA NA NS NA 1510 NS NA 9/14/10 11/12/10 NS NA 5.91 NS NA 5.72 NS NA NS NA NS NA 1490 NS NA NS NA .NS NA 4890 NS NA NS NA NS NA NS NA 1119/10 4390 NS NA NS NA NS NA 6.17 NS NA NS NA 2.9 NS NA 8.8 NS NA 9/13/10 11/10110 NS NA 6.33 NS NA 6.05 NS NA a e -xcee ances or II' uarter un ert e ugus , lit. .; . " jl! ~. Q120U Results.'" i1! ,. ·M 'is Q2,2011 Results: Il< j'l! ... .' ,.coQ3~I.l11Results .'" " ~. Q4 2011 Res.ults· '. "'-,:;,:, -" ". T bl 3 GWCLE d f Th' d Q 2012 d h A t 24 2012 GWDP s .... ~ .. March . . .. ' ~eptember . September ' ;... ..' . December . Monitoring. Con~tituei1t Exceeding GWCJi,iIi January 20U l'd anual'Y 2011' . ·Q12011 I ~ March 2011 Q220H~ May, 2011 'May 2oi1 JuIie2011 . June 2011 ,; July-20ll '. July 20ft . Q32011 Q;2011 November NovemtJer ' December Well (Water August 24, 'Monthly Monthly Sainple Sample Q'I: 2011 Monthly' 2011 Q220U Monthly . Monthly' Sample 2011 '. 2011 Monthly . Q42011 Q420n ~01l Monthly 2011 Monthly 2011 Monthly 2011 GWCL . Result MonthlY Sample Result · Monthly Monthly Monthly . Monthly Result Monthly Sample Date Result ,Monthly I'" 'Class) ~012,GWDP Sample Date ·Result Daie ' . .. Sample Date Date '. . 'oJ. Sample Date,' Result Sample Date' . Result Sample Date Result ; Date ' ,. SampJe Date Result ~ Sample' Date Result Sample Date Result . Result , . .:;' ,. : . ~ . . '" .Required Quarterly Sampling Wells , "". '.' ", . MW-11 Manganese (uglL) 131.29 7/6/2011 8/3/2011 118 91712011 106 10/4/2011 112 1119/2011 105 12114/2011 100 (Class II) 1/11111 121 2/2/11 145 3115/11 68 4/4/2011 148 5/10/2011 170 6/15/2011 121 151 8/30/11 MW-14 Manganese (uglL) 2230.30 NA 2020 NA 2140 NA NA NA 1990 NA 1960 NA NA (Class ill) 1/11111 217111 3/14/11 4/412011 5/10/2011 6/15/2011 7/512011 8/3/2011 6.23 9/8/2011 1014/2011 1119/2011 12112/2011 Field pH (S.U.) 6.5 -8.5 6.37 6.22 6.76 6.63 6.37 5.83 6.4 6.50 6.71 (6.82) 6.63 6.84 (6.41) MW-25 Field pH (S.U.) 6.5 -8.5 6.44 6.66 6.79 6.7 6.1 5.77 6.29 8/3/2011 6.42 6.54 6.6 6.51 6.87 (Class ill) 1/11/11 2/2/11 3/15/11 4/412011 5/1112011 6/20/2011 7/612011 8/30/11 (6.54) 91712011 10/4/2011 111912011 1212/2011 Uranium 6.5 7.02 4.77 6.8 5.56 6.72 7.06 6.74 8/312011 6.37 5.96 5.27 6.56 6.1 Nitrate + Nitrite (as N) 0.62 0.2 0.25 0.6 0.8 0.4 (mglL) 0.3 0.9 0.6 2.4 0.9 1.3 2.3 Uranium (uglL) 41.8 32 69.3 31.8 60.2 57.4 18.5 57.1 19.0 56.1 58.9 55.6 57 Chloroform (uglL) 70 800 730 1200 390 1900 730 300 1000 1300 440 1200 1400 MW-26 Chloride (mglL) 58.31 52 59 64 64 54 39 64 8/3/2011 60 66 61 55 62 (Class ill) 1/12/11 2116/11 3/15/11 411/2011 5110/2011 6/20/2011 7/612011 6.07 91712011 10112/2011 111912011 12/14/2011 Field pH (S.U.) 6.74 -8.5 6.83 6.06 6.89 6.22 6.43 6.52 6.35 8/30111 6.71 6.82 6.75 7.1 (6.58) Dieh loromethane (Methylene Chloride) 5 <1.0 10 14 3.1 20 7 2.4 10 7.9 2.6 8.9 11 (uglL) IDS (mglL) 3284.19 3100 3270 3140 3310 3140 3020 3270 3190 3200 3190 3220 3160 Nitrate + Nitrite (as N) 2.5 15 16 17 16 16 (mglL) 17 17 14 16 16 16 16 MW-30 Chloride (mglL) 128 NS 134 NS 134 128 127 127 126 145 129 122 124 (Class II) Field pH (S.U.) 6.5 -8.5 1110/11 6.65 2/1111 6.96 3/14/11 7.10 411112011 6.83 5/10/2011 6.7 6120/2011 5.66 7/5/2011 6.65 8/3/2011 6.61 91712011 6.80 10/4/2011 6.96 (6.73) 1118/2011 6.83 12/1212011 7.14 Uranium (uglL) 8.32 NS 5.97 NS 6.49 NS NS NS 8 NS 9.83 NS NS Selenium (uglL) 34 36.2 34.7 34 44.4 38.3 38.7 32.4 39.7 32.4 36.6 36.8 38 Nitrate + Nitrite (as N) 5 19 (mglL) 21 22 21 20 22 22 20 21 21 21 21 IDS (mglL) 1320 1240 1220 1250 1370 1290 1330 1280 1300 1300 1320 1290 1330 MW-31 Chloride (mglL) 143 NS 145 NS 143 143 145 148 148 148 145 1118/2011 145 12/12/2011 148 (Class ill) 1110111 2/1111 3/14111 4/112011 5/10/2011 6/20/2011 7/512011 8/2/2011 9/6/2011 10/3/2011 NS Selenium (uglL) 71 NS 64.6 NS 65.2 NS NS NS 66.2 NS 68.8 NS Field pH (S.U.) 6.5 -8.5 6.65 7.21 7.43 7.01 6.73 6.16 6.64 6.67 7.03 7.28 (7.34) 7.01 7.46 Sulfate (mglL) 532 NS 538 531 503 512 540 532 537 541 539 552 530 Manganese (uglL) 200 NS NA 248 NS NA 369 NS NA NS NA 348 267 270 271 283 247 Thallium (ugll) 0.5 NS NA <0.50 NS NA <0.50 NS NA NS NA NS 0.52 NS 0.57 <0.50 0.63 MW-35 Gross Alpha minus Rn 3.75 NS 4.5 NS 10/3/11 4.4 11/8/2011 4.7 12114/11 4.2 (Class II) & U (pCilL) NA 2/15/11 2.6 NS NA 6nl2011 3.7 NS NA NS NA 7/20/11 NS 8/30/2011 917111 Selenium (uglL) 12.5 NS NA ND NS NA ND NS NA NS NA NA 9.3 NA 10.5 NA NA Uranium (ug/L) 7.5 NS NA 12.7 NS NA 21.7 NS NA NS NA 24.2 18.3 22.3 20.1 24 23.6 .. ~ . 'S' Required Semi-Annual Sampling Wells " t,' 0' . i· , ~ . " MW-2 (Class Gross Alpha minus Rn 3.2 NS NA 1.1 NS NA 4112/2011 1.2 NS NA NS NA NS NA 8/8/2011 0.5 NS NA 10/5/2011 1.3 NS NA NS NA ill) & U (oCilL) MW-3 (Class Selenium (ug/L) 37 NS NA 40.5 NS NA 45.4 NS NA NS NA NS NA 46 NS NA 46.7 NS NA NS NA ill) Field pH (S.U.) 6.5 -8.5 NS NA 2/15/11 6.09 NS NA 4/1312011 6.46 NS NA NS NA NS NA 8110/2011 6.32 NS NA 1011012011 6.53 (6.83) NS NA NS NA Fluoride (Mg/L) 0.68 NS NA 0.69 NS NA 0.68 NS NA NS NA NS NA 0.96 NS NA 0.91 NS NA NS NA Field pH (S.U.) 6.5 -8.5 NS NA 6.05 MW-3A NS NA 6.58 NS NA NS NA NS NA 6.19 NS NA 6.5 (6.92) NS NA NS NA (Class ill) Sulfate (mg/L) 3640 NS NA 2/16/11 3730 NS NA 4/13/2011 3350 NS NA NS NA NS NA 811112011 3560 NS NA 10/1112011 3750 NS NA NS NA IDS (mglL) 5805 NS NA 5770 NS NA 5720 NS NA NS NA NS NA 5810 NS NA 5630 NS NA NS NA Selenium (ug/L) 89 NS NA 99 NS NA 85.8 NS NA NS NA NS NA 88.5 NS NA 95 NS NA NS NA MW-5 (Class Uranium (ug/L) 7.5 NS NA 2114/11 II) 29.5 NS NA 4112/2011 7.16 NS NA NS NA NS NA 8/9/2011 0.5 NS NA 10/10/2011 4.52 NS NA NS NA MW-12 Field pH (S.U.) 6.5 -8.5 NS NA 6.43 NS NA 6.67 NS NA NS NA NS NA 6.13 NS NA 6.7 (6.97) NS NA NS NA (Class ill) 2/15/11 4/512011 8/9/2011 1016/2011 Selenium (ug/L) 25 NS NA 39 NS NA 21.7 NS NA NS NA NS NA 25.4 NS NA 35.4 NS NA NS NA MW-15 Selenium (ug/L) 128.7 NS NA NA NS NA 116 NS NA NS NA NS NA NS NA NS NA 112 NS NA NS NA (Class ill) NS 4112/2011 10/10/2011 Iron (uglL) 81.7 NS NA NA NS NA <0.50 NS NA NS NA NS NA NS NA NS NA 137 NS NA NS NA Thallium (ugfl) 1.95 NS NA 3.49 NS NA 3.74 NS NA NS NA NS NA 4.0 3.39 NS NA 3.83 NS NA NS NA MW-1 8 (Class ill) Sulfate (mglL) 1938.9 NS NA 2/15111 1770 NS NA 4/6/2011 1780 NS NA NS NA NS NA 8/10/2011 1910 NS NA 10/1112011 2020 NS NA NS NA Field pH (S.U.) 6.25-8.5 9/21111 5.95 NA 6.55 (6.63) NS NA NS NA NS NA 6.27 NS NA 6.71 NS NA NS NA NS NA {Ii 1m NS IDS (mg/L) 3198.77 NS NA 3250 NS NA 3250 NS NA NS~ NA NS NA 3190 NS NA 3220 NS NA NS NA '!Iii, p~" ,', ',,' -,~ '&'. " ~ "', ,,' I," ,Monitoring Constituent ~xc~eding, GWCLin January 20i I, ,WeD (Water-Current Monthly GWCL 'x , ,Clas~) GWDP Sample' Date , , : ",-: l\l MW-19 Field pH (S.U.) 6.78-8.5 NS (Class ill) Nitrate + Nitrite (as N) 2.83 NS (mg/L) MW-23 Field pH (S.U.) 6.5 -8.5 NS (Class ill) Manganese (ug/L) 550 NS Cadmium (ug/L) 2.5 NS MW-24 Thallium (ug/L) (Class ill) 1 NS Field pH (S.U.) 6.5 -8.5 NS Nitrate + Nitrite (as N) 5.6 NS (mg/L) Chloride (mg/L) 38 NS MW-27 Sulfate (mg/L) 462 NS (Class ill) Field pH (S.U.) 6.5-8.5 NS IDS (mg/L) 1075 NS Gross Alpha minus Rn 2 NS & U (pCi/L) Chloride (mg/L) 105 NS MW-28 Manganese (ug/L) 1837 NS (Class ill) Field pH (S.u.) 6.1 -8.5 NS Iron (ug/L) 1869 NS Manganese (ug/L) 5624 NS MW-29 IDS (mg/L) 4400 NS (Class ill) Field pH (S.U.) 6.46 -8.5 NS Gross Alpha minus Rn 3.33 NS MW-32 & U (pCiIL) (Class ill) Field pH (S.U.) 6.4 -8.5 NS Notes: GWCL values are taken from July 14, 2011 version of GWDP. NS = Not Required and Not Sampled NR = Required and Not Reported NA = Not Applicable " ':. "' Q;J. 2011 Results , ,iI'! ' '0 • ~' , '1!l; " ,. c, -" .: ; . " M'llrch 2011 ';;March January 2011, Qi 2011 , ' Q22011 Monthly Sample Sample Q12011 Monthly .. 20U Sample ,Res~lt M~Iithly. Result Date. Sample Date Date , Result '-' ..::. " ,( F ' ,. NA 6.78 NS NA 2/2112011 4/5/2011 NA NS NS NA NA 6.13 NS NA 2/9/2011 4/5/2011 NA NS NS NA NA 2.78 NS NA NA 2/10/2011 1.42 NS NA 4/5/2011 NA 5.73 NS NA NA 6 NS NA NA 46 NS NA NA 455 NS NA NA 2/9/2011 6.71 NS NA 4/5/2011 NA 1090 NS NA NA 0.7 NS NA NA 114 NS NA NA NA NS NA 2/14/2011 4/11/2011 NA 5.69 NS NA NA NS NA NS NA NA NS NA NS NA NA NS NA NS NA 4/18/2011 NA NS NA NS NA NA 1.5 NS NA 2/9/2011 4/112011 NA 5.99 NS NA '1.:. . ,'!'Q2 20il Results . ' , ",' ," Q3 2011 Results 1iilI" , )4 ' " }i. Q4 2011 Results ~, .,3 ", '.0" ~, '. .1L-'" ;:; o ' ""-'" "11:! , I? ~v ' ji!I j-ifI , Q2201t gSeptember ' ' December ' J" May 2011 ,May 2011 Jun,e20lh j,une20H ' July 2Qll July ~OU, Q32011 September " Q42011 '~ovember November , December , 2011 -Monthly ' Monthly, Monthly ,Monthly , MOJIthly , ' Monthly. Sample Q32011 2Q11 " 2011 'Monthly Q42011 2011 Monthly 2011 Monthly 2011 Monthly , .Result , Result Monthly ' SlJmpleDate Result Monthly Sample Date, Re'sult ' Sample Date Resuit, , Sample Date, Result . Date ' Result ' Sample Date Result Sample Date Sample Date Result , "" ' I;,. , ,'. ~ -'S', -(, " c' .. " , '" Required Semi~Arinual Sampling Welis;continued ,,'" . t " ' " --", 7.03 NS NA NS NA NS NA 6.65 NS NA 6.88 (7.02) NS NA NS NA 7/20/3011 1011212011 2.6 NS NA NS NA NS NA NS NS NA 4.0 NS NA NS NA 7.14 NS NA NS NA NS NA 8/4/2011 6.38 NS NA 6.56 (6.77) NS NA NS NA 10/6/2011 32 NS NA NS NA NS NA NS NS NA 551 NS NA NS NA 2.61 NS NA NS NA NS NA 1.46 NS NA 1.78 NS NA NS NA 1.07 NS NA NS NA NS NA 8/4/2011 <0.50 NS NA 10/ll/2011 0.62 NS NA NS NA 6.12 NS NA NS NA NS NA 6.45 NS NA 6.44 NS NA NS NA 6.4 NS NA NS NA NS NA 6 NS NA 6.3 NS NA NS NA 43 NS NA NS NA NS NA 43 NS NA 44 NS NA NS NA 442 NS NA NS NA NS NA 424 NS NA 456 NS NA NS NA 6.79 NS NA NS NA NS NA 8/8/2011 6.39 NS NA 10/5/2011 7.17 (7.24) NS NA NS NA 1190 NS NA NS NA NS NA 1090 NS NA 1110 NS NA NS NA 1.1 NS NA NS NA NS NA 0.8 NS NA 1.5 NS NA NS NA 109 NS NA NS NA NS NA 105 NS NA 143 NS NA NS NA 1690 NS NA NS NA NS NA NA NS NA 1540 NS NA NS NA 8/8/2011 1015/2011 6.01 NS NA NS NA NS NA 5.78 NS NA 6.07 (6.11 ) NS NA NS NA 3010 NS NA NS NA NS NA 1080 NS NA 1220 NS NA NS NA 4900 NS NA NS NA NS NA NA NS NA 4800 NS NA NS NA 4080 NS NA NS NA NS NA 8/9/2011 NA NS NA 10/512011 4280 NS NA NS NA 6.45 NS NA NS NA NS NA 6.20 NS NA 6.52 NS NA NS NA 4.6 NS NA NS NA NS NA 1.9 NS NA 3.7 NS NA NS NA 8/212011 8130111 10/3/2011 6.14 NS NA NS NA NS NA 6.10 NS NA 6.35 NS NA NS NA (6.20) a e -xcee ances or Ir uarter un er t e ugust , T bl 3 GWCLE d f ThO dQ 2012 d h A 242012GWDP Ql 2012 Results Q2 2012 Results Q3 2012 Results -, January 2012 March 2012 April 2012 June 2012 June 2012 August August September September Monitoring Well Constituent GWCL in August January 2012 Q1 2012 Sample March 2012 April 2012 Monthly Q22012 Q22012 Q32012 Q32012 2012 2012 2012 2012 Sample (Water Class) Exceeding GWCL 24, 2012 GWDP Monthly Sample Monthly Result Date Q1 2012 Result Monthly Sample Monthly Result Monthly Result Sample Date Result Monthly Monthly Sample Date Result Monthly Monthly Monthly Monthly Frequency Date Date Sample Date Sample Date Result Sample Result Sample Result ~ Required Quarterly Sampling Wells ~ MW-11 (Class II) Manganese (ug/L) 131.29 1126/2012 102 2/13/2012 154 3/13/2012 121 4/10/2012 132 5/8/2012 127 6/19/2012 122 7/11/2012 135 81712012 166 9/19/2012 130 Quarterly Manganese (ug/L) 2230.30 NA 1790 NA NA 2360 NA 2100 2300 2140 Quarterly MW-14 (Class ill) 1124/2012 2/2112012 3114/2012 4/12/2012 5/9/2012 6/19/2012 7/11/2012 81712012 9/1812012 Field pH (S.U.) 6.5 -8.5 6.36 6.57 6.51 6.97 6.73 6.90 6.89 6.58 7.08 Quarterly MW-25 (Class ill) Field pH (S.U.) 6.5 -8.5 6.63 6.83 6.55 6.58 6.73 6.99 6.88 6.55 6.54 Quarterly 1/2512012 211412012 3114/2012 4/9/2012 5/2/2012 6/18/2012 711012012 816/2012 9/18/2012 Uranium 6.5 6.6 6.5 6.93 6.52 5.90 7.6 6.45 6.72 6.01 Quarterly Nitrate + Nitrite (as 0.62 1.9 211512012 1.2 3 3.4 2.9 2.3 1.9 1.6 1.8 Quarterly N) (mg/L) 7/11/2012 Uranium (ug/L) 41.8 64.6 2/2112012 59.4 31.2 42.2 18.2 66.0 28.4 67.4 64.9 Quarterly Chloroform (ug/L) 70 1900 3300 2900 2900 1700 2400 8/16/2012 970 2200 2300 Quarterly Chloride (mg/L) 2115/2012 58.31 68 40 74 82 51712012 74 85 711112012 78 78 67 Quarterly MW -26 (Class ill) 1125/2012 2115/20122/2112012 3/14/2012 4/1112012 6119/2012 7/11/2012 7.10 8/812012 9119/2012 Field pH (S.U.) 6.74 -8.5 6.59 6.72 (6.91) (6.71) 6.39 6.88 6/26/2012 7.00 (7.01) 7.00 6.60 7.40 Quarterly 3/8/2012 8/16/2012 (6.80) Dichloromethane (Methylene Chloride) 5 13 24 27 20 10 16 8116/2012 4.9 17 9.8 Quarterly (ug/L) 2/15/2012 IDS (mg/L) 3284.19 3250 3150 3220 3140 3240 3200 7/11/2012 3060 3210 NS Quarterly Nitrate + Nitrite (as 2.5 17 17 18 17 16 15 17 18 16 Quarterly N) (mg/L) Chloride (mg/L) 128 1124/2012 124 126 128 128 124 131 128 139 130 Quarterly MW-30 (Class II) Field pH (S.U.) 6.5 -8.5 6.52 2114/2012 7.12 3114/2012 6.86 4/10/2012 7.66 5/2/2012 6.95 6118/2012 7.10 7110/2012 7.25 81712012 6.95 9/19/2012 7.85 Quarterly Uranium (ug/L) 8.32 NS NA 7.42 8.38 7.84 6.81 7.8 7.64 8.04 7.67 Quarterly Selenium (ug/L) 34 1124/2012 33.3 35 39.5 39.1 32.3 37 38.5 38.4 41.9 Quarterly Nitrate + Nitrite (as 5 21 21 22 21 20 21.6 21 21 21 Quarterly N) (mg/L) IDS (mgIL) 1320 1360 1240 1400 1380 1410 1460 1400 1400 1460 Quarterly MW-31 (Class ill) Chloride (mg/L) 143 155 150 152 160 151 6/18/2012 138 161 175 911812012 172 Quarterly Selenium (ug/L) 1124/2012 2/1312012 3/13/2012 41912012 5/2/2012 6/29/2012 7/9/2012 8/6/2012 NS NS Quarterly 71 NS 67.8 NS NS 70.2 NS 74 Field pH (S.U.) 6.5 -8.5 6.78 7.37 7.13 7.14 7.19 7.28 7.53 6.96 7.10 Quarterly 7.63 Sulfate (mg/L) 532 539 538 517 547 532 497 529 571 561 Quarterly Manganese (ug/L) 200 264 253 269 277 258 304 272 273 283 Quarterly Thallium (ug/l) 0.5 <0.50 0.65 0.71 0.59 0.66 <0.50 0.57 0.61 0.54 Quarterly 1124/2012 3/13/12 MW-35 (Class II) Gross Alpha minus 3.75 6.5 2/14/12 4.1 6.2 411012012 4.1 5/2/2012 4.5 6/19/2012 4.9 7/1012012 3.5 8/8/2012 4.2 9/19/2012 5.4 Quarterly Rn & U (pCi/L) Selenium (ug/L) 12.5 NS NA 19.7 NS NA NS 11.4 7.0 15.9 18.8 8.2 Quarterly Uranium (ug/L) 7.5 1124/2012 16.1 24.7 3/13112 24.9 22.4 22.2 22.5 24.5 26.2 22.9 Quarterly Required Semi-Annual Sampling Wells MW-2 (Class ill) Gross Alpha minus 3.2 NS NA 2/22/2012 0.6 NS NA NS NA 5/9/2012 0.6 NS NA 7/16/2012 0.9 NS NA NS NA Semi-Annually Rn & U (pCi/L) Selenium (ug/L) 37 NS NA 43.1 NS NA NS NA 52.8 NS NA 51.1 NS NA NS NA Semi-Annually MW-3 (Class ill) Field pH (S.U.) 6.5 - 8.5 NS NA 2/29/2012 6.63 NS NA NS NA 5/14/2012 6.67 NS NA 711812012 6.99 NS NA NS NA Semi-Annually Fluoride (Mg/L) 0.68 NS NA 0.86 NS NA NS NA 1.04 NS NA 0.96 NS NA NS NA Semi-Annually Field pH (S.U.) 6.5 -8.5 NS NA 6.46 NS NA NS NA 6.68 NS NA 7.01 NS NA NS NA Semi-Annually MW-3A (Class ill) Sulfate (mgIL) 3640 NS NA 3/112012 3020 NS NA NS NA 5/15/2012 3220 NS NA 7/19/2012 3700 NS NA NS NA Semi-Annually IDS (mg/L) 5805 NS NA 5690 NS NA NS NA 5730 NS NA 5720 NS NA NS NA Semi-Annually Selenium (ug/L) 89 NS NA 65.8 NS NA NS NA 85.1 NS NA 99.3 NS NA NS NA Semi-Annually MW-5 (Class II) Uranium (ug/L) 7.5 NS NA 2/28/2012 18.6 NS NA NS NA 5/9/2012 1.23 NS NA 7/16/2012 0.75 NS NA NS NA Semi-Annually MW-12 (Class ill) Field pH (S.U.) 6.5 - 8.5 NS NA 6.81 NS NA NS NA 6.91 NS NA 6.98 NS NA NS NA Semi-Annually Selenium (ugIL) 2/29/2012 5/1012012 7/17/2012 25 NS NA 27.2 NS NA NS NA 19.6 NS NA 20.7 NS NA NS NA Semi-Annually MW-15 (Class ill) Selenium (ugIL) 128.7 NS NA NA NS NA NS NA 152 NS NA 120 NS NA NS NA Semi-Annually 2/22/2012 5/912012 7/17/2012 Iron (ug/L) 81.7 NS NA <30 NS NA NS NA <30 NS NA <30 NS NA NS NA Semi-Annually Thallium (ug/l) 1.95 NS NA 3.63 NS NA NS NA 3.51 NS NA 3.73 NS NA NS NA Semi-Annually MW-18 (Class ill) Sulfate (mg/L) 1938.9 NS NA 2/27/2012 1920 NS NA NS NA 4/30/2012 1790 NS NA 7/18/2012 1900 NS NA NS NA Semi-Annually Field pH (S.U.) 6.25-8.5 NS NA 6.6 NS NA NS NA 6.59 NS NA 6.64 NS NA NS NA Semi-Annually IDS (mg/L) 3198.77 NS NA 3230 NS NA NS NA 3280 NS NA 3220 NS NA NS NA Semi-Annually ~ Ql 2012 Results " -~ January 2012 March 2012 April 2012 Monitoring Well Constituent GWCL in Current January 2012 Q1 2012 Sample March 2012 April 2012 Monthly (Water Class) Exceeding GWCL GWDP Monthly Sample Monthly Result Date Q1 2012 Result Monthly Sample Monthly Result Monthly Result Date Date Sample Date Required Semi-Annual Sampling Wells, continued MW-19 (Class ill) Field pH (S.U.) 6.78-8.5 Nitrate + Nitrite (as N) (mg/L) 2.83 MW-23 (Class ill) Field pH (S.U.) 6.5 - 8.5 Manganese (ug/L) 550 Cadmium (ug/L) 2.5 MW -24 (Class ill) Thallium (ug/L) 1 Field pH (S.U.) 6.5 -8.5 Nitrate + Nitrite (as 5.6 N) (mg/L) Chloride (mg/L) 38 MW-27 (Class ill) Sulfate (mg/L) 462 Field pH (S.U.) 6.5-8.5 IDS (mg/L) 1075 Gross Alpha minus 2 Rn & U (pCi/L) Chloride (mg/L) 105 MW-28 (Class ill) Manganese (ug/L) 1837 Field pH (S.U.) 6.1 -8.5 Iron (ug/L) 1869 Manganese (ug/L) 5624 MW-29 (Class ill) IDS (mg/L) 4400 Field pH (S.U.) 6.46-8.5 Gross Alpha minus 3.33 MW-32 (Class ill) Rn & U (pCi/L) Field pH (S.U.) 6.4 -8.5 Notes: GWCL values are taken from February 15, 2011 version of GWDP. NS = Not Required and Not Sampled NR = Required and Not Reported NA = Not Applicable Exceedances are shown in yellow NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Values in () parentheses are the field pH measurements for the resampled analyses. NA 6.83 NS 2/28/2012 NA 3.9 NS NA 2/20/2012 6.61 NS NA 51 NS NA 2.25 NS NA 2/23/2012 0.96 NS NA 6.03 NS NA 6.4 NS NA 45 NS NA 451 NS NA 2/28/2012 7.24 NS NA 1140 NS NA 2.3 NS NA 109 NS NA NA NS 2/28/2012 NA 6.22 NS NA 1310 NS NA NA NS NA 2/22/2012 NA NS NA 7.12 NS NA l.8 NS 212112012 NA 6.57 NS rsuant to the August 28,2012 DRC letter, IDS monitoring in MW-26 returned to the routine frquency of quarterly. No sample was required for this sampling eriod. NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA rsuant to the Au ust 28, 2012 DRC letter field pH will no longer be tracked on the exceedance sheet after the 3rd quarter 2012 because 8 or more consecutive results are within the GWCL limits. NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA Q2 2012 Results ,," Q3 2012 Results w August September June 2012 June 2012 2012 August 2012 September Q22012 Q22012 Q32012 Q32012 2012 2012 Sample Sample Date Result Monthly Monthly Sample Date Result Monthly Monthly Monthly Monthly Frequency Sample Date Result Sample Result Sample Result Date Date 6.86 NS NA 7.21 NS NA NS NA Semi-Annually 511612012 7/1912012 3.7 NS NA 4 NS NA NS NA Semi-Annually 6.74 NS NA 7.10 NS NA NS NA Semi-Annually 5/16/2012 7117/2012 49 NS NA 117 NS NA NS NA Semi-Annually 2.01 NS NA 4.7 NS NA NS NA Semi-Annually 5/1012012 0.74 NS NA 7/18/2012 1.36 NS NA NS NA Semi-Annually 6.21 NS NA 6.45 NS NA NS NA Semi-Annually 6.2 NS NA 6.7 NS NA NS NA Semi-Annually 46 NS NA 47 NS NA NS NA Semi-Annually 446 NS NA 453 NS NA NS NA Semi-Annually 5/112012 7.03 NS NA 7/16/2012 7.40 NS NA NS NA Semi-Annually 1170 NS NA 1150 NS NA NS NA Semi-Annually 0.8 NS NA l.2 NS NA NS NA Semi-Annually 114 NS NA 7116/2012 105 NS NA NS NA Semi-Annually 1850 NS NA 8/112012 1660 NS NA NS NA Semi-Annually 5/812012 6.15 NS NA 7/16/2012 6.38 NS NA NS NA Semi-Annually 8/112012 (5.81) 1400 NS NA 7116/2012 1270 NS NA NS NA Semi-Annually 6140 NS NA 8/112012 5190 NS NA NS NA Semi-Annually 5/812012 4600 NS NA 8/112012 4420 NS NA NS NA Semi-Annually 6.47 NS NA 7116/2012 6.68 NS NA NS NA Semi-Annually 8/112012 (6.45) 2.4 NS NA 1.4 NS NA NS NA Semi-Annually 4/30/2012 7/912012 6.40 NS NA 6.72 NS NA NS NA Semi-Annually INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab C 1 Field Data Worksheets Accelerated Monitoring, August 2012 Tab C2 Field Data Worksheets Accelerated Monitoring, September 2012 Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab F1 Laboratory Analytical Reports -Accelerated Monitoring, August 2012 Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, September 2012 Tab G Quality Assurance and Data Validation Tables G-1AIB G-2AIB G-3AIB G-4AIB G-SAIB G-6AIB G-7AIB G-8 AlB G-9AIB Field Data QAlQC Evaluation Holding Time Evaluation Laboratory Temperature Check Anal ytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QAlQC Evaluation for Sample Duplicates Radiologics Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site MW-5 • perched monitoring well TW4-12 o temporary perched monitoring well TWN-l0 9 temporary perched nitrate monitoring well PIEZ-l ~ TW4-27 ~ perched piezometer temporary perched monitoring well installed October, 2011 RUIN SPRING 6 seep or spring HYDRO GEO CHEM, INC. APPROVED WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS DATE REFERENCE H:/718000/mayl21Uwelloc12.srf FIGURE A-1 TabB Field Data Worksheets Quarterly Sampling Mill '-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r····_···············_····_··_················_·····_······_···· __ ··_····--····1 I OENlsONI)~~1 t MINI:S . Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 3 ra Q::;:().'fi"er" Cr1'OVVlo.vJC1..'ter ~Ol~ ~ See instruction Location (well name): 1-1 _}I\_W_-_O_Q. __________ --' Sampler Name and initials: 1 Mr'lner Ho 11;J~j/-m Field Sample ID Date and Time for Purging 1 7/ J b 1:2D 1'2 and Sampling (if different) ,-I .;...1'I_Ii_jg ________ --J Well Purging Equip Used: [![]pump or [QJ bailer Well Pump (if other than Bennet) QED '---------~ Purging Method Used: l'tl 12 casings [QJ3 casings 1. I NvJ-1fS Sampling Event 1 ~+t:rU:::l &W Prevo Well Sampled in Sampling Event '-_________ ---J pH Buffer 7.0 /.0 pH Buffer 4.0 Y.D Specific Conductance r....1 ....;.4'1_1=---___ ---11 !lMHOS/ cm Well Depth(O.Olft): 1 \~g. gO Depth to Water Before Purging 1 \ o~. g3 4" well:I I~.~ 1(·653h) 3" Well: 0 (.367h) '---___ --J Casing Volume (V) Conductance (avg) 1-.1 -=3:.....;7;..::3:::::;...(,~ _____ --I pH of Water (avg) Well Water Temp. (avg) 1 \5. E>~ Redox Potential (Eh)1 36~ TurbiditylL--0 __ ---J Weather cond'l '--_C_l_0_\A_~_~ ________ --' Ext'l Amb. Temp. O( (prior sampling event)Ir....:2_li..;..o_. _---J Time 1 JQ..~D Gal. Purged 1 2 9. 'is Time lr....l:....-~_y..;..J _----.I Gal. Purged 1 2.5. 17 Conductance pH 1'1.2 4 Conductance pH 1 7,%3 Temp.oC lSJ;1 Temp.oC 1 LS.50 Redox Potential Eh (m V) Redox Potential Eh (m V) 1-.1 ..;...3_D_g __ --J Turbidity (NTU) D Turbidity (NTU) o Time 1124;[ Gal. Purged 1 2$.3f) Time 1);2. Y3 Gal. Purged 1:2.S . "b Conductance 5735 pH 7.2Y Conductance pH 1 7·43 Temp.oC Temp.oC 115,52 Redox Potential Eh (mV) '500 Redox Potential Eh (m V) 1-.1 ~_13 __ ----.I Turbidity (NTU) o Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I U.O~ gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = ...... 1 _-_2_17 ___ --1 T = 2V /Q = I 114.1,(; I Number of casing volumes evacuated (if other than two) 6 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs ...... 1 _/1./....<./'.....;,4"--_____ ----' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha r$ 0 1,000 ml IE 0 HN03 ~ Other (specify) 0 0 Sample volume 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth 1119, OS Sample Time .... 1 _l2.._ti5 ___ ----' Comment ~ See instruction Af'ri\led 0.\\ ~j1-e lA.-t loLJO, ""-;"nrlU ~n~ ~f(~" pfc::.s(!~t &r ?"'f'~e a.f\d ~o.Mf 1~n~ ~\)-e(]t.. t>""'("~G b~~V'I ",1-~ot..\5. fv..r~e~ VJc::.\\ .,ror t?--+c+"" 1 of' \ 20 M~nv'+C~_ ~1-if 10 .... 5. ckc..r .f-hro v. ~ ).., o \At-h " f'uJ'~ ". Y' \ArE!::.'" e" J.e j OI.n A SC( ""p)~ Gone0+~~ ~ ).2.115.. Le.-ft-~;tc 0\.1-)Q.S2. MW-0207-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 0 2of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r~~~I~~J)~ll WHIT:~:S~~~~~MILL L~ MINES_~I FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I ',Sri.l Q"'tk1'~.e("" G-('OlA.~J \Na-.+ef" ~O 12 ~ See instruction Location (well name): ..... 1 ..f-B....:....W~--=();,-.3..L.-________ ---I Sampler Name and initials: I~"ne,... fJ6}Jitllit~/lH Field Sample ill I MvJ-03_0718~Ol<' Date and Time for Purging I 7/181 flD 1':2 and Sampling (if different) I,--"--~-,-~_:t). _______ ----, Well Purging Equip Used: [![]pump or [QJ bailer Well Pump (if other than Bennet) ..... I Q~~_p _____ ---' Purging Method Used: ~2 casings [QJ3 casings Sampling Event I Q",q,r-tGr-B G-w Prevo Well Sampled in Sampling Event I ..... _i'1_W_-_lg ______ ..... pH Buffer 7.0 1.0 pH Buffer 4.0 I £i.o Specific Conductance l ..... q.L..:~_~ ____ --'1 ~MHOS/ cm Well Depth(O.O 1ft): '---'-17_,_D_b __ ----.... Depth to Water Before Purging I ff34 :;""0 Casing Volume (V) 4" well:1 6 1(.653h) 3" Well:I-!,;-.-o-~----I.(.367h) Conductance (avg) 5b8& '--"--~---------' pH of Water (avg) Well Water Temp. (avg) l Ib, leg Redox Potential (Eh)IL--3_J_J _---' TurbiditYL-1 ..;:::0 __ ---' Weather Condo I c "'::>V\.\'l{)~ Ext'l Amb. Temp. O( (prior sampling event)L-1 Zl_1_o __ .....1 "----~---------~ Conductance Temp.oC Gal. Purged I 14 :st pH 1/.0c Redox Potential Eh (mV) 32.1 "-------' Turbidity (NTU) D Time 1 0 q:S::I Gal. Purged I ) y. 97 Conductance Temp.oC Redox Potential Eh (m V) Turbidity (NTU) 6 White Mesa Mill Field Data Worksheet for Groundwater 1 Time I O~5) Gal. Purged I lL/. 70{, Conductance Temp.oC Redox Potential Eh (mV) ..... 1 _3_1Q.-"--_---' Turbidity (NTU) o Time 16953 Gal. Purged 1 15.1 g Conductance 1 51./1 b pH I b·'(1 Temp. °C L-I ...;..;;It~, 1....:.'_---' Redox Potential Eh (mV) L-I .,:::3;....,:0..5=-_---' Turbidity (NTU) 6 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged 1£·bO gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1,---' ~_O_~ ___ ---, T = 2V/Q = 1 yg.f/1 I Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs ,-k_"''j._~ _______ --I Sample Taken Sample Vol (indicate Filtered Preservati ve Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs D D 3x40 ml D D HCL D D Nutrients D D 100 ml D D H2SO4 D D Heavy Metals CJ D 250ml ~ 0 HN03 'r!J D All Other Non Radiologics D D 250ml r D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) !J D Sample volume D ~ D ~ 1=1 0 u..r'J 4e. If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 q~. 7..5 Sample Time Comment ~ See instruction A rr i ~eJ. 0 l\ f. rho "'+ 0835. --f .. /ln~'" ""ItA &"cr; f\ rf'e5e"} -to' r f'''''''~''' ....... 1 .s "'" pl:,'j 'P \A.r~~ bC~iAn (h+ o&t.\6 . PV'.r6~J well +or ~ +o+-~l 0+ 75 M ~nL\,+es.. l.V~i-~r t..)a.,S Cle4r. P\'\I~C ~Y1ae~ o..n ~ S~(V1p)~ col1ec.tcd ~J-oq55 , ~-eW SITe ~t I)J-' MW-0307-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) I!>E NI~~~ij~~1 WHIT: ~~~~~~~ MILL J MINI:S ~ FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 3 t"3 Q v.o-.4t:r G-rou.t\J\ l,UoJi,... ;:2.0 J!2.. ~ See instruction Location (well name): L-I _}JI_W_~_O_3_~ ________ ----I Sampler Name and initials: 1 ~r") ne.--Ho J Ji ao.~111:! Field Sample ID Date and Time for Purging 1 7/181.:2..01.2.. and Sampling (if different) ..... 1 7....&...£-1 -'-1t{ ..... 1_~_.:....1~-'--____ --I Well Purging Equip Used: 11:1 Ipump or [QJ bailer Well Pump (if other than Bennet) L-I Q_E._D _____ ----' Purging Method Used: ~2 casings [QJ3 casings Sampling Event I QUCA.(fcr8 ~\,O Prevo Well Sampled in Sampling Event I L-_M_W_-_O_3 ______ __' pH Buffer 7.0 /,0 pH Buffer 4.0 I q.~ Specific Conductance ..... 1 _4q_q ____ --I1 ~MHOS/ cm Well Depth(O.O 1 ft):1 r.... !:J...;...5_,_O_O __ ----' Depth to Water Before Purging I gS. is Casing Volume (V) 4" well:~-G-'y;3..s;;;;;;....---II(.653h) 3" Well:. 6 . (.367h) Conductance (avg) r.....-.....;5;;;;..t]...;.4..a.....:.4 _____ ----' pH of Water (avg) Well Water Temp. (avg) I AI. 'I" Redox Potential (Eh) ..... 1 ~_~_J_----' Turbiditylr....-° __ ---' Weather Condo Time ..... 1 ~_1 ...;;;15 __ --, Gal. Purged 1'b,s::t Conductance I SGfzt q pH Temp.oC Redox Potential Eh (m V) &....;1 3=-ifi~ __ .....1 Turbidity (NTU) o Time 1 ObSq Gal. Purged r....1 _~ ___ .....I Conductance 1 5460 pH 1/·0/ Temp.oC Redox Potential Eh (mV) 1L-3_;;3>~b __ ----, Turbidity (NTU) 1 0 White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event}IL-~_L1_o __ __' Time Gal. Purged Conductance pH 11..--__ --' Temp.oC Redox Potential Eh (mV) ..... 1 ___ ----' Turbidity (NTU) Time Conductance Temp.oC Gal. Purged Ir....-o __ ---' 5~1g I I~.ql pHI 1.01 Redox Potential Eh (m V) L-I .=3 =3::...;.0 __ --1 Turbidity (NTU) 1 D.q 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) [Se ~Of~e~=-=-__ --. Volume of Water Purged 1-1 _13_l_S_~ ___ --, gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I -;2.08 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I 6).84 I 10 1 1~.52.. Name of Certified Analytical Laboratory if Other Than Energy Labs II-N~I"A-~ ______ --I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs D D 3x40 ml D D HCL D Nutrients D D 100 ml D D H2SO4 D Heavy Metals 19 D 250 ml rn D HN03 ~ All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) ~ D Sample volume D ~ D SvJt~t~ If preservative is used, specify r-(D.S> Type and Quantity of Preservative: Final Depth 1.-1 ~_3_.l.S ___ ---, Sample Time 0700 See instruction Comment A r r ; "o~ On s;to ... + 08~. ""-;;:n ~ (f' "n J. Gur( II') fres.~ n}--To pI-' r ~e. well, t>~(~e b~D.." 6..+ )0,0 I P~M'~ -(.6. ~-ell -f"of" fA. ~o}O\l 6.r' bo.5 Wl"r1LA.tt.S, P\Af<jec\ wen ~r~ J. ~o..-te("" W!A..5.. G\~o..<". f~~-c:. enJeJ 1:\,+ J 1).5. Lc:.~ SI"fG ~+ 1116 Arr;'Jea 0"(\ ~:+~ lJ.:t Ob.'Sl . -rNlner ",na Go.rrif\ ffe"eot 1-0 LoII~C:-T .s~tYJp)es" Pe.p-1-h 10 \A)~+e, wo..s 88. 3S ~tJl.fVlp)e.s Gol1~c.:t~a ~-T D,D6, L~fr s/fe (A+ 070-5 MW-03A 07-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D lB 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) 1~~;'~~;Pi~l FIELDDA~i=l~~E:2:~DWATER ~ S •• instruction Description of Sampling Event: 1 '3 ('d\ G\I\.O..rt~r G-ro\J.YJd. w~+e'(" 2.61:2,. Sampler Name Location (well name): 1 MW .. 03 and initials: ~nf1~r HoIIJ~/7H Field Sample ID Date and Time for Purging 1 7/1 b / :;"'0 ]':2-and Sampling (if different) 1.-1 ~----.;VA~ _______ --, Well Purging Equip Used: ~pump or [gJ bailer Well Pump (if other than Bennet) 1.-1 G.~"::....;.D~ ____ ----, Purging Method Used: [!TI2 casings [gJ3 casings Sampling Event I Q"''''r-h .... Jj Cr YJ Prevo Well Sampled in Sampling Event I I.-M_w_ ..... _O_~ ______ --' pH Buffer 7.0 /,0 pH Buffer 4.0 Specific Conductance 1.-1 _t)_9--J~"--__ ---,1 ~MHOS/ em Well Depth(O.Olft): 1 \Sg .SO Depth to Water Before Purging 1 ] Db # LJ g Casing Volume (V) 4" well:1 ~D/1() 1(·653h) 3" Well: 0 (.367h) '--___ --I Conductance (avg) '---_~_q_:5_q-'--____ ____' pH of Water (avg) Well Water Temp. (avg) 1 \ b. 35 Redox Potential (Eh)1.-1 ,_'l.....;.~ __ --' TurbiditYI.-I _) ._5 __ --' Weather cond'l I.-__ G_}_D_"'_~_i _______ ~ Time I l~Sb Gal. Purged 1 92...:5~ Conductance 1 .2~3~ pH 17-54 Temp.oC 1 )h,3~ Redox Potential Eh (mV) I \~5 Turbidity (NTU) I l.S Time I ~qS2. Gal. Purged I \..\1 .7'1 Conductance I ;2...9"b'7 pH I 734 Temp.oC IJ~ ,~D Redox Potential Eh (m V) 1.-1 ..... J ~~5 __ ____, Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)1 ~ Y /) Time 1)451 Gal. Purged 1 Y2. 53 Conductance Temp.oC 11'·40 Redox Potential Eh (mV) L-I \7....;.;6~ __ --' Turbidity (NTU) Time I l~53 Conductance 1.2.. 491 Temp.oC l It; .?1J; Gal. Purged I 42..~b pH 1 /.'6 Redox Potential Eh (m V) 11.-'_bO ___ --I Turbidity (NTU) p.' 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged ~3.qD gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 11.....-. _:2._1/ ___ ---' Time to evacuate two casing volumes (2V) T = 2V/Q = 114::11 7l I Number of casing volumes evacuated (if other than two) D If well evacuated to dryness, number of gallons evacuated ~ arne of Certified Analytical Laboratory if Other Than Energy Labs .... 1 ;v~!J.:...;:'At~ _____ --, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 Heavy Metals 1!1 0 250 ml ~ 0 HN03 ~ All Other Non Radiologics 0 0 250 ml 0 D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) D D Sample volume D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I 12S.3l> Sample Time ...... 1 1~4~s5~ __ --' Comment ~ See instruction Arn'-.J(;d... on $11-C. q...1-ll~O. -r"nnc, ~()J. fr-rJ.rfl'n ~~.sen+-~r p\)..r8~ d\r"')a S't""'f}'j eU~J1+' Pv.r~e b~jQ.1"! A.} 1135. rvr<A.e~\Nel\ for " ~ot"'\ ~ ::too t"')!(\~-tc!:~, w~...j-cr wa.s yY10~lj Gle~r -}hro~o~ f~~e. PV\r~e. eV1tA~~ O\t 1~5,S. L~ sd-<-~ }liS7 MW-0507-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 D D D 2of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) OENISONr;)~~ ATTACHMENT 1-2 WHITE MESA URANIUM MILL MINl:S FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 ~' eX G",o..r:tc:r GrOlJ..nJ Wo-.+('r :;2.01:l- Location (well name): I~M_W_-_l_l _________ ----I Sampler Name and initials: Field Sample ID 1 j1\W -1\-DI \ 12.01~ Date and Time for Purging ..... 1 7_7_)\_7_2_0_1~ _____ --, and Sampling (if different) Well Purging Equip Used: [Q]pump or [gJ bailer Well Pump (if other than Bennet) See instruction 1 QED Purging Method Used: ~2 casings [gJ3 casings Sampling Event I Qv'.o.."t~o('l~ 6-w Prevo Well Sampled in Sampling Event I ..... _fII_w_-_4S _______ --' pH Buffer 7.0 7.0 pH Buffer 4.0 glQ Specific Conductance ..... 1 4_q_q=--___ ....... 1 ~MHOS/ cm Well Depth(O.Olft): 1:3,0, DO Depth to Water Before Purging 1 Kg, la. Casing Volume (V) ::: :::::I '~S~~' I~:~!~:i o.7.?>'l Conductance (avg) .......... ~_~...;....:S=-==:::'b~ _____ --I pH of Water (avg) Well Water Temp. (avg) 1 \1.0l1 Redox Potential (Eh) ..... 1 _l D_' __ --' Turbiditylr....-0 __ ---' Weather Condo l ___ ( __________ --' _ .,:)U\.tlni Ext'l Amb. Temp. O( (prior sampling event) ..... 12_1_0 __ ...... Time 1 \2..6S Conductance 1 9-b$1 Temp.oC 1 \1. \0 Redox Potential Eh (mV) Turbidity (NTU) Time ..... 11 2:_0_7 __ .....1 Conductance 1 ~ ... $OO Temp.oC 1 \1.05 Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Gal. Purged 1 S~ .5~ pH ,.79 10, o Gal. Purged 1 Sq .():;2.. pH /. 7k o Time I ' 2.D " Gal. Purged 1 58,go Conductance 1 ~73~ pHI 7.75 Temp.oC 1 17.0 y Redox Potential Eh (m V) 1 ..... _' 0_3 __ ----1 Turbidity (NTU) Time ~I \ 2._0..;:;g_---' Gal. Purged IS'l.2.'i Conductance 1 ;z:$4b pH 17/79 1 Temp.oC 1 \7,66 Redox Potential Eh (mV) ..... 1 ZJ ___ , __ ---' Turbidity (NTU) o 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= I '~)J Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I 2S:l.6.5 I D o N arne of Certified Analytical Laboratory if Other Than Energy Labs I/fWAi,. 1 set of'\JO~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs W D 3x40 ml D ~ HCL "tI Nutrients 1IJ D 100 ml D j!I H2SO4 'tI Heavy Metals ~ D 250ml I!J D HN03 'tJ All Other Non Radiologics 1tJ D 250 ml D ~ No Preserv. D Gross Alpha tJ D 1,000 ml ~ D HN03 If] Other (specify) 1$J D Sample volume D ~ D G-e.nefo..\ :r nOr~~f'I:L.s If preservative is used, specify Type and Quantity of Preservative: Final Depth I «g, 3 b Sample Time L..ol1 )~2=..:)...=:O~ __ ....J Comment ~ See instruction Ar1'\-.}e.a ol"l s.*c ~+ cr1:10. iAAner ().r,l\ G-()..("r~n ~'('e.~c!:nr -Fo,-'?~.~:("~~ o.r\~ ~G\.IV\'P) l::j e-ven-T f'u..,.~ bet:,"'" .J-C'2,S, f \M"~c\ \o.l<:\\ .r.r ~75 \'Vl:flv..-tes. I.J",--ter w~ deo. .... t),c0'0ho",+ the 'Pv.r~e . 'P\.A("~e e.l'l.aed o..no. ~~f"'\plt!.s. were col1ecte4 d.1-}2JO. L ~-8-~ lie (f;J 12.20 MW-11 07-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D ~ D YJ 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r~~;~~;i)~~1 Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 13r(); Q\A"-rte.r &f'ov.nJ G5&..'1>er ;2.0 l~ ~ See instruction Location (well name): ..... 1 _M.....;W_-_l_2.'---_________ --' Sampler Name and initials: I ~nn t!"( HolUJ"'!d/'flt Field Sample ID I tA;vJ ... \:L ... 07 \/:2..012,. Date and Time for Purging L-I ......:7.~/...;..17.;....;1 ...... ;L_O.....;J_:2. ____ ___1 and Sampling (if different) L-I ~_VA ________ ....J Well Purging Equip Used: [][]pump or [gJ bailer Well Pump (if other than Bennet) ..... 1 Q_-e_D _____ ----' Purging Method Used: It] 12 casings [gJ3 casings Sampling Event I G.",o.r::f<..r~ 6-W Prevo Well Sampled in Sampling Ev~ntl L-_M_W_-_:l_3 _____ ----' pH Buffer 7.0 7.0 Specific Conductance ..... 1 ~.:...Ci;....J~'----___ --I1 ~MHOS/ cm Depth to Water Before Purging I 'O!> .. Y.5 Conductance (avg) '--Y..LJ...) 1...:..':)=-_____ ---1 pH Buffer 4.0 Y.n Well Depth(O.Olft): 1130.'10 Casing Volume (V) pH of Water (avg) 4" well:1 14.33 ICo653h) 3" Well: ...... _0 __ ----'. (.367h) Well Water Temp. (avg) I Jb,D~ Redox Potential (Eh)1 ~Ci1 TurbiditylL-l.I_1_. b~_....1 Weather Condo I 'P",,-tltl CJo",d~ Time I Oq?JS. Gal. Purged I J-<6.:;2.' Conductance 917~ pH I 7.00 Temp.oC I )~ .07 Redox Potential Eh (m V) ..... 1 =~~'6 __ ....J Turbidity (NTU) Time I Qq31 Conductance I Y I 7 g Temp.oC I l t; . og I 1), 5 Gal. Purged I j$ . b 9 pH I ()·~1 Redox Potential Eh (mV) I '50:2: Turbidity (NTU) I 1 J . g White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event) ..... 1 _17_6 _--, Time IOGI3b I Gal. Purged 1 2.'6·l1~ I Conductance I L117~ I pH I b.Cffj I Temp.oC l ie. og I Redox Potential Eh (mV) I 310 I Turbidity (NTU) r 11.7 I Time I013p> I Gal. Purged 1 2g.~ I Conductance I G] /] I pH I "(,.9'8' I Temp.oC I 1(;.69 I Redox Potential Eh (mV) 12'1&' I Turbidity (NTU) I JI.' I 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = L-I ,_~_17 ___ ...... T = 2V/Q = I }:~;Zf 10 I Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs ..... 1..-v._1l_A _______ ...... Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs D D 3x40 ml D D HCL D D Nutrients D D 100 ml D D H2SO4 D D Heavy Metals ~ D 250ml 1:1 D HN03 ~ D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) D D Sample volume D D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I 1 ?-:1, \ D Sample Time IL-()----'~.....;~_() __ ---I See instruction Comment MW-12 07-17-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) f····-·--····-···············-·········-·············-.. --.. ------, IOENISONI)JJ I L_~NES ~............, Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER ~('()\ Qv--o..;::tC'(" Gro'-Af\iX 00..:;=8' 2ol!L ~ See instruction Location (well name): 1L..-""_w_ ... _'_9 __________ --' Sampler Name and initials: I=r:.t'ln(;r" Ho)ba~RH Field Sample ID I MW-14-OJ \1""'01'2: Date and Time for Purging 1L-7_/l_l_1 !2J_D_l ':l. _____ ......1 and Sampling (if different) 1-1 M_V._~ ________ .....I Well Purging Equip Used: ~pump or [QJ bailer Well Pump (if other than Bennet) ~ E. D '-----------' Purging Method Used: 11:1 12 casings [QJ3 casings Sampling Event I Qv\.o-."('"'""'c("~ G W Prevo Well Sampled in Sampling Event I-I_M_W_-_~ ______ ___' pH Buffer 7.0 pH Buffer 4.0 L1.D Specific Conductance. I I-q~q1-=--___ --,1 ~MHOS/ cm Well Depth(O.Olft): I l~g.70 Depth to Water Before Purging I }O:3>.'tO 4" well:l lb.lq 1(·653h) 3" Well: 0 (.367h) L--___ .....I Casing Volume (V) Conductance (avg) ~q'3>S ~--~-----~ pH of Water (avg) Well Water Temp. (avg) I lS,~\ Redox Potential (Eh)L-1 _~_,_---, TurbiditylL....:::O~ _ ___' Weather Condo Time 11235 Gal. Purged Conductance 1 3q~q pH Temp.oC 11S.hS Redox Potential Eh (mV) 1(4';)..7 Turbidity (NTU) 0 Time I )')52 Gal. Purged Conductance I ~~~~ pH Temp.oC 111.; .b~ Redox Potential Eh (mV) Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater 37. 'i"1 1 G;·8g I :3g.~Q ~,~'I Ext'l Amb. Temp. O( (prior sampling event)IL..-:;2_L)_O_---' Time L-P .2._3_] _--I Gal. Purged 1 35. I 'f Conductance 13 '130 pH 1 (c'.8<J Temp.oC 115.'0 Redox Potential Eh (mV) I .2;2.3 Turbidity (NTU) Cl Time 1'233 Conductance I 342& Temp.oC I }S.bD Gal. Purged I 37)' (,,:6. pH I b,81 Redox Potential Eh (m V) L-I _!J.._1_7 __ .....1 Turbidity (NTU) 10 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 ..;;;.3 .... Q'-'-",O::;...b=-__ --' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I ~_;2._1J ___ --I Time to evacuate two casing volumes (2V) T = 2V/Q = I l,-\q·~ I Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs IAY-lAL 1 ~a or '-'Ow I 1 Ji 1') Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs tIl 0 3x40 ml 0 ~ HCL "rJ Nutrients ]lj 0 100 ml 0 n H2SO4 I!j Heavy Metals ltl 0 250ml 1:1 0 HN03 ~ All Other Non Radiologics lfl 0 250 ml 0 l:J No Preserv. 0 Gross Alpha .it] 0 1,000 ml 1!:J 0 HN03 l!J Other (specify) nJ 0 Sample volume 0 1!J 0 {Ye'(lt«(A\ :rnor~t'l \0 If preservative is used, specify Type and Quantity of Preservative: Final Depth I lOl.j 1'30 Sample Time Comment ~ See instruction Arr\\le~ 0(\ S>tG ~-t OGl30 .)o..nr'\Gf"' a.n~ &().(,..;Y\ }>l'eSt!Y\f -for ?w~e (A()~ .s#\tv)p)~Z5 e\lGr\'1, Pv.r~c:: be~OV\ ~-t o~3S, 'P",,("~ca ~~l\ ~( CA. +o-hd of" ) gD m,'nu. t~s. l.Vo...+~r \,..)(i..5 G1eo..t'". fv.r~e: et1deJ anl ...5a.f'1'fdc..s G61Iec,f.!A tk.} 12.35. Let}!:, I1-C ~~ \2LlS MW-14 07-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 m 0 18 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) I--........ · .... --.-.--... -------~···-··-·--···-··-·-· I OENlsoNI)~~ ! MINI:S ~. , Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER ~'f'(J. Q~~=te:r G-rou,n():wo...fer ~61~ ~ See instruction Location (well name): L-I M;,.....;...;W----"-LS=-_________ ----' Sampler Name and initials: I ~1\ne("" ~~l1la~j)rJf Field Sample ID I MW-\S,..0717~OI'2.. Date and Time for Purging I 7/177:;"'Ol~ and Sampling (if different) ~.N;.L.yJ.r..;;;.(1~ ______ ----, Well Purging Equip Used: [f[]pump or @] bailer Well Pump (if other than Bennet) QED L--~ _____ ~ Purging Method Used: 002 casings @]3 casings Sampling Event I Q.,..(),.M-a-1~ G W Prevo Well Sampled in Sampling Event I ...... _M_W_-_l_d.. _____ ...... pH Buffer 7.0 /.0 pH Buffer 4.0 Y.o Specific Conductance ...... 1 ----=-q...;..~ 1..!-__ ----'1 !!MHOS/ cm Well Depth(O.Olft): I ]~7·6D Depth to Water Before Purging I] 0 b .4.5 Casing Volume (V) 4" well:1 J q 4 qy 1(·653h) 3" Well: 0 (.367h) '-------' Conductance (avg) , .... 1 _,-\..:..;~ ...... q-,--D _____ ~ pH of Water (avg) 7. oS '----------~ Well Water Temp. (avg) I S. ~ b Redox Potential (Eh)1 2.5& Turbidity ...... 1 D ___ --' Weather Condo Time ...... ll_D_YS __ ----' Gal. Purged ~Y1.0b Conductance I 111. ~ 7 pH 1,,05 Temp.oC \S.9t Redox Potential Eh (m V) 1 ..... _2._'_9 __ --' Turbidity (NTU) Time ...... 11 ...... 0.....;4 ....:.1 __ --' Conductance 1 QI ~t 1 0 Gal. Purged pH Temp.oC ...... 1 _15_.Y_' __ ...... 1 Redox Potential Eh (mV) 1259 Turbidity (NTU) D White Mesa Mill Field Data Worksheet for Groundwater /·05 Ext'l Amb. Temp. O( (prior sampling event}L-1 ..:...17;;....0 __ --' Time I 'OLI' Conductance I Y2Q.b Temp.oC 1\5.43 Gal. Purged I ~ 't .27 pH 1-"7·(b Redox Potential Eh (m V) 1 ..... 2_b_o __ --' Turbidity (NTU) Time I \oyg Gal. Purged 1 34 .71 Conductance 1 921q Temp. °C 1 l5·S::£ Redox Potential Eh (m V) IL.o25_:t __ ---' Turbidity (NTU) 1 0 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1,---~...;...2...;.r...:--J __ --I T = 2V /Q = I 193. 8(, I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated I lJ Name of Certified Analytical Laboratory if Other Than Energy Labs 1-1 ~_Y~ _______ --, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs D D 3x40 ml D D HCL D Nutrients D D 100 ml D D H2SO4 D Heavy Metals ~ D 250ml ~ D HN03 111 All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) D D Sample volume D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I lO~ .2b Sample Time 1-.1 _lO_5_0 ___ --I Comment ~ See instruction kr:~~'\ 0(\ !S..1-c::. ... t 07'10. ~r,"<r <\A6 6-"",6" prGSe"t--:t.r f'u.r~G din.! .s"JN1pl~ eve":!: P\Ar~c b~()f1 ~+ Otl.lS. P\).('~e.d WG1'.fot"" fA.. -i-c>1-CA 1 of"' J85 Mif)\A.+~S.. W~+er~!A.S dea.~. p \;\.r~G ~f"I~ect ~Y\t\.. ..$CA.Mp)('.. c.c,\lec;}-c:.l ~ JOsCJ. LLJ+-~I-t~ 0..+ 1 D 6~. MW-15 07-17-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D D 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) [_ ....•..... __ •...•....•....•...• _ ... __ ._._._._----, I OE~f~,,~J~ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 3? 6 QO\A.d..Aer Grou.nI1\Wo.,+er ~Ol~ ~ See instruction Location (well name): !'---P\_W_-_,g __________ ---' Sampler Name and initials: F!tI\.1\1)if Ao) II Jq~/Ttl Field Sample ID Date and Time for Purging L-!7_!_I_E._I ~_O_l Q. _____ --I and Sampling (if different) Well Purging Equip Used: []JJpump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: !ID !2 casings [QJ3 casings Sampling Event ! Q\A~,-"h~ ..... '.=3 6-W Prevo Well Sampled in Sampling Event I L-M_vJ_ ... _X_y ______ ...... pH Buffer 7.0 7.0 pH Buffer 4.0 '-1 .0 Specific Conductance ..... ! ~...;..q ...... j ____ ...... 1 ~MHOS/ cm Well Depth(O.Olft): ! )'3'1 ,00 Depth to Water Before Purging !70.} 0 Casing Volume (V) 4" well:1 til.72... 1(·653h) 3" Well: 0 (.367h) '--------I Conductance (avg) 1 ..... _~_=_l).L-l.:.....:lll..--___ ..,__----I ~~7\ pH of Water (avg) Well Water Temp. (avg) ...-! T"'"!S.".... ...... 9r-=l:-------. Redox Potential (Eh)1 21Y Turbidity! .2 .:3 WeatherCond. I Po.ri-t1 Gl0ua~ Time l~lD Gal. Purged g3.5Y Conductance I;; 1..\7'-'. pH I b.bl Temp.oC 1 \6 .00 Redox Potential Eh (m V) L-I D_:l_7 __ --I Turbidity (NTU) Time L-I '_3_l~ __ ----, Conductance 1 ':y .. ] 7 1 Temp.oC 1 :2..\ Gal. Purged 1 3:)t 17 pH 1 G.bl:( Redox Potential Eh (mV) 1"--2._1o __ ----' Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)! ..... l_8_o __ --' Time I r511 Gal. Purged I ~j, 7 b Conductance I :3 q 15 Temp.oC Redox Potential Eh (m V) ~I;L._J......;Y~_----, Turbidity (NTU) Time 1 131:S Conductance 13Y b1 Temp.oC I ls.'1E Gal. Purged 1 g4.) 9 pH 1 G .. 69 Redox Potential Eh (m V) ..... 1 ;t_D_7 __ ---' Turbidity (NTU) 1.2.9 1 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I .. 'J-11 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I .3SY .57 I 10 Name of Certified Analytical Laboratory if Other Than Energy Labs I ..... ""_1" _______ --' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 0 Heavy Metals 'tl 0 250 ml 'tl 0 HN03 W 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 'E 0 Sample volume 0 'i!1 0 ~ S",,\f'CAte If preservative is used, specify -rDS Type and Quantity of Preservative: Final Depth I 11 , l..5 Sample Time Comment ~ See instruction A(""rive~ 0)'\ si+<:.. 0..1 OG'-\ t. ~"flt,... d,:"~ G-o.(("'t'\ ffGSen-r ..ror-?v..r~-e ~n~ ..sG\M'Pl~~ -e~eY\l fv.(""~e 'bejo.n o..-t 06'1~, 'Pv..("~(:~ V:>e)I.rot fA totl1\) o-F 31D yv1;n IA.tG5. VJo..~( wo..s \'V'DS1-~\ Cl<ar -n ro~hov..1-+he. 'Pv..~~e. ?",rt1e en~ea (.{n~ So.M4'lc.) c.ollec.ic4 ~-t \~15. Le:f.r 5;t~ v.. t }31J MW-18 07-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r---·----------I OENISON')~~ MINI:S Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 3f"O QV\",;;fe.r &rolA~C1VJ~fer 20 J,2.. ~ See instruction Location (well name): I L...: M:...:,...'N.;,..-_l:.....l1 __________ ......1 Sampler Name ~ and initials: I ==r l.."nGf' H 0) J / /?HhJt Field Sample ID Date and Time for Purging I 7/Ig/.2ol~ and Sampling (if different) 7/11/.2D1:2.. ~---------......I Well Purging Equip Used: ~pump or [gJ bailer Purging Method Used: 00 2 casings [gJ3 casings Sampling Event L-I _Q-'-"'-...;..(}I.._t"_f _G_f"_lj...o..-_G-_W ___ --' pH Buffer 7.0 7.0 Specific Conductance ~I _9.:....1;....9~ __ ---J1 ~MHOS/ cm Depth to Water Before Purging I 5'3. 3S Conductance (avg) Well Pump (if other than Bennet) ~I Q __ E_D _____ --' I MW -D.3A Prevo Well Sampled in Sampling Event 1-_________ ......1 pH Buffer 4.0 LLo Well Depth(O.Olft): I )1, q. 00 Casing Volume (V) 4" well:1 ,;2.. liS IC.653h) 3" Well:l-. _O __ ---I.(.367h) pH of Water (avg) L-17_,2._] _____ ---J Well Water Temp. (avg) . I lY,g) Weather Condo I Do.. ... ~ I Cko..f" Redox Potential (Eh)~1 _~_I_)_----' Turbidity II-0=-__ --' Ext'l Amb. Temp. O( (prior sampling event) 1-1 ~_-o __ --, Time I 01$ Gal. Purged I} 2.C1 . II Time 10/.56 Gal. Purged 1129, 3~ Conductance I \, K'-\ Conductance 11..-\ _7_IJ.:..-_--' pH I ""1.20 Temp.oC I ''1 ~D Temp.oC Redox Potential Eh (mV) Redox Potential Eh (mV) ~I '3_,_'1 __ ---1 Turbidity (NTU) o Turbidity (NTU) o Time I 0157 Gal. Purged I 1.1.'1.5'1 Time ID75 & Gal. Purged 112.9.7-6 Conductance \7 g:L. pH I 7.2 :0 Conductance 117 bOO: pH I 7.2.1 Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) 1L.;;;3;;.,..O_' __ ---I Turbidity (NTU) o Turbidity (NTU) 10 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged J30.2() gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I ~ ~J ] T=2V/Q= I 575.bh I Number of casing volumes evacuated (if other than two) I e) If well evacuated to dryness, number of gallons evacuated I C) N arne of Certified Analytical Laboratory if Other Than Energy Labs 1 ..... /'/._7._~ _______ --' Sample Taken Sample Vol (indicate . Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 100 ml 0 ~ H2SO4 n 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250m! 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 0 0 Sample volume 0 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth ..... 1 _b"_.t_'D ___ --' Sample Time Comment ~ See instruction MW-19 07-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) ATTACHMENT 1-2 r-------------------------------------------------------------1 I OENISONI)~~ L MI""I:S _ I FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 3f'~ Q\.VI\rt(!r &rO\A.Y\~u.)~+~r ~OJ.:z ~ See instruction WHITE MESA URANIUM MILL Location (well name): 1L--..;...A~VJ_ ... _::l:3 __________ __I Sampler Name and initials: 1 ~t1n~r t1oJJ)a";1/77-J Field Sample ID f/lVJ-;)...3-071 b;2..0)~ Date and Time for Purging 1 ,/J'I:;...o]':2.. and Sampling (if different) 7 J 17/2019... L--~~ _______ ~ Well Purging Equip Used: [][]pump or [gJ bailer Well Pump (if other than Bennet) 1-1 Q_~_D ______ __I Purging Method Used: ~2 casings [gJ3 casings Sampling Event 1 Q v.<A.4-er" B & \I\S Prevo Well Sampled in Sampling Event I-1_)JI_vJ_ .... _D_'6 ______ ~ pH Buffer 7.0 pH Buffer 4.0 Specific Conductance .... 1 _4_q~ ____ ...... 1 !lMHOS/ cm Well Depth(O.Olft): 1 }.3~ .. OO Depth to Water Before Purging I l~'1.15 Casing Volume (V) 4" well:1 13 .. bl 1(.653h) 3" Well: 0 (.367h) L.--___ ~ Conductance (avg) '--..... 3==:;.:-t...1..-c...:::;;~ _____ ---' pH of Water (avg) f,.~b '-----------' Well Water Temp. (avg) 1 ~b,!l.l Redox Potential (Eh)1 ~2:!:> Turbidity I .... _]'_._b_~ WeatherCond. I ?M+b Glol>.~ Ext'l Amb. Temp. O( (prior sampling event) .... 1 ~~~_o_~ Time \S l.S Gal. Purged Time Gal. Purged Conductance ':>705 Conductance pH L-I __ ----I Temp.oC Temp.oC Redox Potential Eh (m V) .... 1 2-.;..2.....:3""--_--' Redox Potential Eh (m V) ..... 1 ___ ----' Turbidity (NTU) 1 1 b.O Turbidity (NTU) Time a....;;1 O;....7_3_1~_......I Gal. Purged 0 '-------' Time 1 0733 Gal. Purged ..... 1 _0 __ ----' Conductance 1 385' pH 17.0 8 Conductance 1 5& b I pH 1 7, ] 6 Temp.oC 117.7S Temp.oC I lg .:Ll Redox Potential Eh (m V) I-r~.....;~;......;:;b __ ~ Redox Potential Eh (m V) 1 .... 3..;;...1...::g:.....-_~ Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) l?:>e:\;{' e. It-\-+e., V olume of Water Purged 2.S.D~ gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I • ~~g Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V /Q = I )50.41 I 1.-//4 N arne of Certified Analytical Laboratory if Other Than Energy Labs 1-1 JV.---:..Z,;",:A:.....-_____ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs D D 3x40 ml D D HCL D D Nutrients D D 100 ml D D H2SO4 D D Heavy Metals 1:8 D 250 ml ~ D HN03 ~ D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) D D Sample volume D D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth &....;Il_:l_q _. C>_D __ ----I Sample Time Comment ~ See instruction Arr;"ea 01"1 );ite G.1-1::t5S. ~nner' B.J1:j~ p"e.setd-.£1" f\U~" ~(1a .s~"'P);~1 eve,,+. fv.."'~<:' be:~"'1\ OL.j-13M, ?"'r~~ well.for 0.. -;\-"t .. l .;; \35 Y'\.n.,d-.. ~. ?"'r~d ~~/I J.~l. f\At~e. t:Y\tk~ J-\5'b. V-J~~,r \N~~ M051~ Cle~(. Le1i-s~c 4 lS11 Arr; v-e~ 01\ sj+~ d 0-:/:;"7. TAnner o.('I~ &(Arr;" pf'C.s~n-t +0 60n~c.+ ~Mflt..s . t:)ep+~ +6 w~1-~r wo.~. };2.7. (;5 ~r"?'eS. Go\l~ct~j, ",-1 073~ L~ s.il-<:. ~ 013'5:, MW-23 07-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 I ~ ! o ~ .. .... S ... .. I ! MifI-Groundwiilter Discharge Permit Grou"ndwater M"onitoring Quality Assurance Plan (QAP) ATTACIDIENT 1-2 \VHlTE l\tIESA URANIU~f ~ULL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sam piing Event: I ?t~. G\J..o..(".t~(' &rov.n A Wc;..-ter . ~I::" Location (well name): 1-1 ...:...M..t..:Wr...;;.....s;il-2~lj~ ______ ~_.-I Field Sample ID I MW-).Li ... D11!5 ;l.Ol~ Sampler Name and initials: Date: 6/06/2012 Rev. 7.: Date and Tilne for Purging .... 1 ...:..J.~/J-.lf1~/{)..O~;:;...l,&.;;..o....~ ______ __ and Sampling (if different) .... 1 7~' '-/w/81L..bL>I!:;;:=..t.::J~~-.:... ___ ---.J Well Purging Equip Used: OOpump or @] bailer Welt Pump (if other than Bennet) 1-1 Q:::;)..:;€:;,..;D;:;...·_. ____ ---..I Purging Method Used: 002 casings @]3 casings Sampling Event I Qu..o..r4-erb G:W Prevo Well Sampled in Sampling Event I .... _M_W_-_l5_~ _______ ....J pH Buffer 7.0 ,.0 Specific Conductance 1-' .;...:.&f-t.'11-4--___ ...JIJiMHos/ em Depth to Water Before Purging [ )r~.~ ... -J Conductance (avg) L..\~L\t:t ~~~~--------~ pH Buffer 4.0 4.0 Well Depth(O.Olft): I t;tO.oc Casing Volume (V) 4ft wen:1 ~:b~(.653h) 3ft WeJl:r '0 =:==1(.36711) pH of Water (avg) t...1' -:'" ..;;.{,....;; . .:t_7..:..-. __ ..;....;...._ ..... Well Water Temp. (avg) f :t.c>.i"5 Redox Potential (Eh)1 :l..'1b TurbiditylL..,o,.;;;.,..... . .5=-_.....I Weather Cond. Ext'l Amb. Temp. ·C (prior sampling event)1.,.;1 ~~;.....o_-.J Time I 103Q I Gal. Purged [7.~~~~=:J Time I I Gal. Purged I I Conductance [q~3~:':::'::-:'.1 pH 16.~7 '1 Conductance I I pHI : I Temp.oC I 2D.I~ I Temp.oC I I Redox Potential Eh (m V) I :2~b I Redox Potential Eh (mV) I I Turbidity (NTU) I Q ~5 I T u~bidity (NTU) I I Time . r_9.~~.: J Gal. Purged I Q I :- Time I D6;~5 " l GaL Purged 1·0 . I Conductance I ".l.. , I pH I b.55 · I '1~O!> Conductance I ~~ Ll. I pH [~,,·::f5..:.:.-~:-.-.~J Temp.oC Db .~S: : ,:'] Temp.oC [ 'J~.-~:_~ : .~ . Redox Potential Eh (m V) I ~i:i I Redox Potential Eh. (m V) I ~O O I Turbidity (NTU) [.-O·.?{."- .~-" .... ,. ,~, ,] Turbidity (NTU)' I O~3 I White Mesa Mill Field Data Worksheet for Groundwater ~ lof2 capturx-COMPATIIHE WIn+/,--WU-li:---f'UN(,TlOHAl.IT MiII-Groundwater Discharge Permit . .... Date: 6/06/2012 Rev. 7 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q). in gpm. S/60 = I .. ~q;t Number of casing volumes evacuated (if oilier than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= r 38s~3 I I ;V/A I 17.(;,8 ~ Name of Certified Analytical Laboratory if Other Than Energy Labs I L!. ~';':''/,,.l;JA!...-_____ ---lI Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 0 0 3x40 ml 0 O · HCL ·0 ··· ·0 Nutrients 0 0 lOOmI 0 0 H2SO4 ·0 .. 0 Heavy Metals 1SiII·· 0 .250ml ·61 0 . RN03 :til . ··0 AU Other Non Radiologies 0 0 250m) ·0 .. 0 No Preserv. 0 ·0 .. . . Gross Alpha 0 0 I~OOO ml 0 O · HN03 0 ···0 · Other (specify) Sample volume ; .. 0 0 0 O· · .. 0 0 .. , If preservative is used, specify Type and Quantity of Preservative: .. Final Depth t 1.23. ,co Sample Time 0 630 I !comment See instruction " .. ~j.' Ar(,\\le~ on ~i+c o..--\-0<145. -r~I1,..er tA,..~ Cro.rr'" pr~Sfn-l ..R.t p ..... ~e. p ~ .. ~" he~"" ... -l:-oQ5Cl. f v..r ~eA we \ 1 -+;,.-If.. ta+", I e.f' ~ 6 1"1 ,nLA 1-eS. 'p u.~~"J ", .. II J~ \i-,)o...-t~('" \i..:)~ M05>-+!j (Ieo..r. ?""{'5e' enJecl. ~....r 1030. Le..+:r s ~+~ 1J...1-)C>3:;t j . \ d' J . De..p~ . A rl" V-e..Q.. Or"\ ~.le. <AT Obi". l~"'"(", '-'."t;\ &,,",r("~ f\ pr~~'T +0 c-clle.c.. + .5ArYtp1e... Pe.pth +c W,,-1e,... S4\,-..,p 1e (.¢UeGt~a 4.1 ~ Ob3f.> Le~ .s('+~ t-\..f. Ob3k . '.1'1.37 I..-_______ ----l. IDo not touch this eel] (SbeetName) White Mesa Mill Field Oata Worbheet tor Groundwater Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER I ~f""iX Q"",u"f""ter (;rov-",£}\ w~f~,.. 2.D)~ ~ See instruction Location (well name): 1-1 M_W_"'_~:S __________ ----I Sampler Name and initials: I-r;.t"l'\-t.f »0 1 h'J\~ IT» Field Sample ill Date and Time for Purging L-17_1_1D......;I_9-_0_,_'2 ____ --I and Sampling (if different) /V/fo '-----------~ Well Purging Equip Used: IT!Jpump or @] bailer Well Pump (if other than Bennet) L-I _Q_~_-_D _____ ----I Purging Method Used: [][]2 casings @]3 casings :r I MW-30 Sampling Event 1 6>"'~("Te.f'b c,..\J Prevo Well Sampled in Sampling Event '--_________ ~ pH Buffer 7.0 ;,D pH Buffer 4.0 L).O Specific Conductance L-I 9_~_~ ____ --I1 [lMHOS/ cm Well Depth(O.Olft): I 115. () 0 Depth to Water Before Purging 1 /:'.15 Casing Volume (V) 4" well:l 2-b/:.t3 IC.653h) 3" Well:L-__ o __ --I.c.367h) Conductance (avg) 1-1 ..... 322.S ________ ---' pH of Water (avg) Well Water Temp. (avg) 1 \5.77 Redox Potential (Eh)1 :35 , Turbidity 1 1 ) • E 0 Weather Condo I'--G_\_e_u.._( ___________ ~ Ext'l Amb. Temp. O( (prior sampling event) ...... 1 _:;1.._0_°_----' Time 1 j;2JS Gal. Purged 1 S~,S<j Time I l21k Gal. Purged I 5 ~ . ~ () Conductance 1 3':227 pH ~.l10 Conductance I '3'2.~' Temp.oC I \S :1'1 Temp.oC I 15.75 Redox Potential Eh (mV) Redox Potential Eh (m V) L-I 3_b_O __ --' Turbidity (NTU) Turbidity (NTU) Time I \211 Gal. Purged I 59 , O:J:: Time I )2.18 Gal. Purged I S9 :;2-Lj Conductance 1L-3_~_11 __ --I pH G.gg Conductance I 3!ZZ::t: Temp.oC I IS.go Temp.oC I IS.'7l1 Redox Potential Eh (m V) L.:I ~::;;........;R5~ __ --, Redox Potential Eh (m V) 1 ...... 3_3_0 __ ----' Turbidity (NTU) n. J Turbidity (NTU) I ll. g White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged IL-S_9_,_b_7 ___ --' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I _. _.J2..._'7 ___ ....J Time to evacuate two casing volumes (2V) T=2V/Q= 1?.9g.;tC; I 10 .- Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 10 N arne of Certified Analytical Laboratory if Other Than Energy Labs I fIwA L \ Sad a\O' v oc.s Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs 1J D 3x40 ml D 1tI HCL ~ D Nutrients t1 D 100 ml D t1 H2SO4 tJ D Heavy Metals ~ D 250 ml 'f] D HN03 f] D All Other Non Radiologics lJ D 250ml D "l] No Preserv. D ~ Gross Alpha 11 D 1,000 ml ~ D HN03 "'t1 D Other (specify) ~ D Sample volume D lJ D )J G-en~r6\l "'Inl:>r..5fA";c.> If preservative is used, specify Type and Quantity of Preservative: Final Depth I lS J S:l. Sample Time \ :l.'l.:D Comment ~ See instruction MW-25 07-10-2012 IDa not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater ~onitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 ~ See instruction ()ENISONr.J~~ WHITE MESA URANIUM MILL MINIES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 ~,.a ~w>"i:t(;r GrOU(\J w",fe;r ~01~ Location (well name): ..... 1 ...:..M.....:..W..;,.;;....-...:;,:;L_, _________ -----' Sampler Name and initials: 11O..nncr HbJ1l'J~ IrB Field Sample ID Date and Time for Purging 1 7/11 b 0 l:;l. and Sampling (if different) IV /,4 ~~~-------------~ Well Purging Equip Used: OOpump or @] bailer Well Pump (if other than Bennet) I L6(1+;nll\OU\,> Purging Method Used: @]2 casings @]3 casings Sampling Event 1 Qv..~f+~d~ G-w Prevo Well Sampled in Sampling Event I I.... __ M __ W __ -)_~ ____________ ___J pH Buffer 7.0 I .b pH Buffer 4.0 t4.D Specific Conductance 1....1 _~!....,;9:......j4'---______ .....I1 ~MHOS/ cm Well Depth(O.Olft): 1 \~1.~3 Depth to Water Before Purging I 6;2., Y () Casing Volume (V) 4" well:1 3g,t4Z 1(.653h) 3" Well: '6 (.367h) '---___ __oJ Conductance (avg) 1-1 ...;;;3~Y_'1~5 ______ __oJ pH of Water (avg) Well Water Temp. (avg) 11 b. ~D Redox Potential (Eh) 1,-_) g_.5 __ --1 Turbidity ,-I _0 __ ---1 Weather cond·1 ..... ___ S __ V\._n_f\_f __________________ ----' Ext'l Amb. Temp. O( (prior sampling event) 1-1 _!:L_'1_o_---I Time l oC}so Gal. Purged 1 L-_0 ______ -.....1 Time I I Gal. Purged I I Conductance 13QQS pH Conductance I I pHI I Temp.oC 1 b. :La Temp.oC I I Redox Potential Eh (m V) 1-1 ....:.\..:;.:g3~_---oJ Redox Potential Eh (mV) I I Turbidity (NTU) I 0 Turbidity (NTU) I I Time Gal. Purged Time I I Gal. Purged I I Conductance ·1 L-___ ~ pH Conductance I I pHI I Temp.oC ..... 1 ___ ---oJ Temp.oC I I Redox Potential Eh (m V) Redox Potential Eh (mV) I I Turbidity (NTU) Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged c gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I lD.E Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I b I I D b Name of Certified Analytical Laboratory if Other Than Energy Labs I AWAL , sJ of \JOG!> I 1 j;1l Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs m D 3x40 ml D ~ HCL rn D Nutrients [] D 100 ml D 121 H2SO4 Dr D Heavy Metals ~ D 250 ml 1!J D HN03 [:J D All Other Non Radiologics tEl D 250ml D rlI No Preserv. D r2f. Gross Alpha ~ D 1,000 ml L!J D HN03 Li D Other (specify) IJI D Sample volume D ~ D eli G-el'\ f! (6-' :tno!jo.n i c.~ If preservative is used, specify Type and Quantity of Preservative: Final Depth 1L-\..L..!l-.l.7..:... O::::;...J...' __ --' Sample Time Comment ~ See instruction ~(('\'\)ec\ On ~~+~ a...1' 0<:\3g, -r1)..'(\}'lerO\flJ. G-~r(";1) pre.!)eTlt +0 co\lt::c.1-5.~yY\pl~s. \J.)""te:(' wo...s c,leo,.('. .s"'1"')p)~ l:o)l~deJ ,,1' 04'5L L~+t .srt~ a..-t 100D MW-26 07-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) i----------------------------------------------------1 I OENISONI)~_ ~I I MINES __ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER I 3/A Qv-Ci\;:fer Gf"ov.na~4er 201.<., 1<e~O\r-Y'p}e ~ See instruction Location (well name): ...... 1 .;...f\..;..W_-2_k __________ ----J Sampler Name and initials: FG"ner JJ()}],;J~J-rH Field Sample ID Date and Time for Purging ...... 1 _g_I_I'_1_2_0_'_2 ____ ----' and Sampling (if different) ...v/,4 L--____________ ~ Well Purging Equip Used: [QJpump ~r @] bailer Well Pump (if other than Bennet) I ConfmlAOlA.$ Purging Method Used: @]2 casings @]3 casings Sampling Event I Q "",-<fer b G-vJ Prev. Well Sampled in Sampling Event I ...... _AJ_Y_A ______________ ~ pH Buffer 7.0 7.0 pH Buffer 4.0 I Y,O Specific Conductance 1,"---4_1_~ ___ --'I ~MHOS/ cm Well Depth(O.Olft): 1'--1_2.._1._3_""5 __ ----' Casing Volume (V) 4" well:1 ~ 7 ~50 1(·653h) 3" Well: 0 (.367h) a.....-___ ~ Depth to Water Before Purging I b3, q 0 Conductance (avg) 3Y~5 ~~~------~ 6.g0 pH of Water (avg) Well Water Temp. (avg) 1 ]4. £I; Redox Potential (Eh) 1L....-1S_LJ_----' Turbidity ...... 1 6 ___ ~ Weather Condo Ia.....-G_lo_\}.._d_U _________ ---I Ext'l Amb. Temp. O( (prior sampling event) ...... I'_CJ_o __ ...... Time I063Q Gal. Purged 0 Time Gal. Purged Conductance 13'i 2.S pH b·gO Conductance pHI Temp.oC Temp.oC Redox Potential Eh (m V) ...... 1 .;...lS.;...4..;...... __ ~ Redox Potential Eh (mV) I Turbidity (NTU) 10 Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pHI Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (mV)-1 Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged o gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1 \O.S Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 1 N arne of Certified Analytical Laboratory if Other Than Energy Labs .... 1 _N ...... /..;..;A _______ --' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs 'ill 0 3x40 ml 0 ~ HCL ~ Nutrients 0 0 100 ml 0 0 H2SO4 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 0 0 Sample volume 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth 1.-1 \_?._D_,_O_O __ --I Sample Time 1.-1 O=-bY..;..D ___ ....... Comment ~ See instruction p;«;'::'e.A Gn ~i+" ~ 0(,3,-\. --r.:nner ",",1 G-o..rr:YI 'f're.se.1l+ -fOy-PW"~< "",I. .s.:;,.,p'" €Ve,,7. Sb..)'V\pl('.5, were. (..ollec.-teJ 0\+ o~YO. W",-ter ~ cJeCkr. Le.++ .sifctd-D{,<-jS, MW-26 08-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 0 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) [·_····_······_···········_···_········_··_·_··---1 I OENISONl)j~ L_MINI:S I Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER ~ ('00 Q\.A,C\-r+er Grav.ndl \Ij~~('" .20 J.=l. ~ See instruction Location (well name): lL-iA:..-...W_~21_7 _________ ----I Sampler Name and initials: E;IV\e,r ijD l};J\0..!:3 /17}- Field Sample ID Date and Time for Purging 1 ..... 1....;/....;J_'=-..;../:J-L:>'---..... 1Q. _____ ...... and Sampling (if different) .... 1 _/'oI_I_I+ ________ .....J Well Purging Equip Used: IltJ Ipump or [QJ bailer Well Pump (if other than Bennet) Il--o._E_D ______ --' Purging Method Used: ~2 casings [QJ3 casings Sampling Event 1 ~uo..rtcrt1 &vJ Prevo Well Sampled in Sampling Event I .... _M_W_-,_Y _______ .....J pH Buffer 7.0 L-I _,_. _0 ___ ____1 pH Buffer 4.0 t\.O Specific Conductance .... 1 _q_q_~ ____ ..... 1 !!MHOS/ cm Well Depth(O.Olft): ..... 1 _<15_._0_0 __ ---' Depth to Water Before Purging 1 :5 \ \ 1:,5 4" well:1 Q.g. sb 1(·653h) 3" Well: 0 (.367h) L--___ --I Casing Volume (V) Conductance (avg) )S/~ pH of Water (avg) 7.-:SQ Well Water Temp. (avg) lS.0~ Redox Potential (Eh)IL-:s_6_~ _ ____I TurbiditYL-1 ...;:O~ _ ____I Weather Condo Time L-llll,.,;..,l _l D __ ---I Gal. Purged 57.5D Conductance pH 1 7.3~ Temp.oC 115.60 Redox Potential Eh (mV) Turbidity (NTU) o Time ..... 1 oI...L) 1..;..c12.::a-______ Gal. Purged 157. ~3 Conductance 158'0 pH 75"10 Temp.oC 15 .. 0::( Redox Potential Eh (mV) ~o!l 1--___ -....1 Turbidity (NTU) b White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( {prior sampling event}L,.;..llb_o __ --I Time ..... 1\_11_1 __ ...... Gal. Purged 1 S7.7:;Z Conductance 1 '57 ,\ Temp.oC I 15.6l Redox Potential Eh (mV) I '367 Turbidity (NTU) Time ...... 1 )L..:."ll:..;;;:::,"'--_ ...... Conductance IElE o Gal. Purged IS g . }:s pH I 7, Yo Temp.oC IS.01 Redox Potential Eh (m V) ..... 1 ~_'1_, __ ...... Turbidity (NTU) b 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged L-I .....;S;..;::g;.....,_S..,.j4L..--_----I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I _' :::L_17 __ ----I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I :2."-;)...7 D I I 0 10 N arne of Certified Analytical Laboratory if Other Than Energy Labs \..,;1 N:...:....!..iII3t...:::-______ ---I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs D D 3x40 ml D D HCL D Nutrients "£I D 100 ml D ~ H2SO4 ~ Heavy Metals D D 250 ml D D HN03 D All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha E D 1,000 ml tJ D HN03 "EI Other (specify) rs D Sample volume D ~ D ch'or-;l( If preservative is used, specify ~p.s Type and Quantity of Preservative: SV\~1( Final Depth 1.....:1 ~~'..:::;b"":'Y __ ----I Sample Time I L-..;..;..ll_l!) ___ --I Comment Arr-:\led,. 0(\ ~;te oJ 064D,-r-l\nn~r ~fla O-I\((;n fr~~efl+ f\A.r~~ b~,l'\ ~+ ObY.5, 'P \Ar~e~ \.\:Ie' I for ().. +o-r~-' of Gl-co.r ~r"v..~hov-.T-'P\A. .. ~c.. 'Pv\'i"~c=.. eYldej, fMJ... L~n-$1iG ~+ 11 ~3 . MW-27 07-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater ~ See instruction -tor p\.Ar~(.. ~t'\J.. .s~Mp),,~ e'0(.rlt. 2-70 tv) ;Y)(}\.+~. WO\.+cr Wo.,s ~~tyl p)~ Co) Ic~C'J t:t7-)))6, N D D D D D IlJ 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 r···_·········_············_···_·_-_··_·· __ ···_·······_ .................. _ .•.... OENISONI)~~ ~ See instruction WHITE MESA URANIUM MILL MINI:S FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 '3 r~ Q \Ao..-rfer GrOvyJ WO\I+t:f :;2..0 I:;L Location (well name): 1 L-...:.,M..;.,w_-.;;...;2.g-=-_________ --I Sampler Name and initials: I:::r;.nfl(:(' »oJ1;J~ftr.r Field Sample ID Date and Time for Purging 1 7/1f./2'/!)12 and Sampling (if different) #/A ~--------~ Well Purging Equip Used: [![]pump or [gJ bailer Well Pump (if other than Bennet) .... 1 _Q_EJ)~ ____ ----, Purging Method Used: ~2 casings [gJ3 casings Sampling Event 1 Q\AlA.(f crJ.j G-W Prevo Well Sampled in Sampling Event I .... __ M_W_ ... _2_~ _____ __' pH Buffer 7.0 Specific Conductance .... 1 ...:.~...;..q1oL.-___ -,1 !lMHOS/ cm Depth to Water Before Purging 1 7 ~ ,S7 Conductance (avg) 3q b 1 ~-=~~---------~ pH Buffer 4.0 Well Depth(O.O 1ft): 1 11 0.00 Casing Volume (V) 4" well:1 ~l. g~ IC.653h) 3" Well: ..... __ 6 __ --I.(.367h) pH of Water (avg) IL-b~, 3_4~ _____ --, Well Water Temp. (avg) .... 1 _lS_~_lg __ __, Redox Potential (Eh)1 ~5S Turbidity .... 1 _0 __ ---' Weather Condo Time .... 1'_0_3_0 __ -, Conductance 1 3~ 70 Temp.oC 1 \ S· \ll Gal.Purged 1 tl~.l.jg pH 1 '.L)~ Redox Potential Eh (m V) .... 1 ..;;;;;~;..;:::b:S=-_----, Turbidity (NTU) 1 6 Time 1103Z Conductance 1 30j bS Temp.oC 1 ]5 .. 19 Gal. Purged 1 Q9.9) pH ~.1><g Redox Potential Eh (m V) ...... 1 ~_5_& __ ---, Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater Ext" Amb. Temp. O( (prior sampling event) .... 1 _16_· __ --' Time 1....11_°=3...:...1_----' Gal. Purged 1 '-I '-i. 7(:) Conductance 1 ~'17~ Temp.oC Redox Potential Eh (m V) IL-3S~...:.1 __ --,1 Turbidity (NTU) I 0 I Time 1....11_0 ~-=-_---' Gal. Purged I 905.\3 Conductance 1 rsq 70 Temp.oC 115.17 Redox Potential Eh (m V) .... 13_&---.;. __ --' Turbidity (NTU) 10 1 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I '15.57 gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ,,:L\l Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I ~O 1. 14 I o N arne of Certified Analytical Laboratory if Other Than Energy Labs 1...1 _;V;_v,_Zl" ______ ----' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) m 0 Sample volume 0 ~ 0 [2] Gh lO(';j, If preservative is used, specify Type and Quantity of Preservative: ., Final Depth I 7tf. 7 0 Sample Time L..1~_J..~;.....;L='r;:;...· .. -___ ......I \035 Comment ~ See instruction A (-r~ "eA 01\ S itc ",} 0700, ~fI )'\c!t' 1'\'/'1 A &/Arr,'n prc~el'\} ~br f u,"'{j 'C. {Jtf\~ SC4W1pL'C,j ev-enT. f~r~.., b~"" .d-0705. PU('ff"-well ~,. "'-+0-1-... 1 of' !l.1O M .',., '" -1-es.. vl ... rer "'''6 d"'''''r. fv.<&(. e",c\.t~ Q.,f\~ So\fVlpl!.-w~.s. collt(,-t-t:a 1>..1-1035.. Le.~ ~\i-<: (A.-t lD-:>7 MW-28 07-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r~~:~~J).ill ;i~ MINES ~ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 13ri}\ Q\A~f"+(A' G-rD\A.fJ\ ~o..ter' :lOla... ~ See instruction Location (well name): ..... 1 M~W-=---;l..--=-g _________ ---I Sampler Name and initials: I-r;t\ner-Htl \h'J~.Im Field Sample ID Date and Time for Purging .... 1 .....;«;.:../_l _/~_o_I'2... _____ ...... and Sampling (if different) A//A L--_~ ______ ~ Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) .... 1 _G_E_D _____ --' Purging Method Used: ~2 casings [QJ3 casings Sampling Event I Q\kC'Ar""ter kl 6-\15 Prevo Well Sampled in Sampling Event I .... _N_y~ _______ ___I pH Buffer 7.0 1.0 pH Buffer 4.0 L.\.O Specific Conductance .... 1 _q..:..q~4L----__ ___I1 !lMHOS/ cm Well Depth(O.Olft): I )10. ()O Depth to Water Before Purging I 7 b. b~ Casing Volume (V) 4" well:1 2J:17 1(·653h) 3" Well: 6 (.367h) L--___ --' Conductance (avg) D~'1? L--_~~~ ____ ~ pH of Water (avg) Well Water Temp. (avg) I \5.11: Redox Potential (Eh)I ...... ~_\ t __ .....1 Turbidity ...... 1 O~ __ .....I Weather Condo Time 1L-.1 ~_5S __ ...... Gal. Purged Conductance pH 5.gb Temp.oC IS.7D Redox Potential Eh (m V) ...... 1 "3_!l----=.S __ .....I Turbidity (NTU) 1 0 Time I }~ 5"1 Gal. Purged 1 \401.25 Conductance 1:05199 pH 1 51 ~D Temp.oC Redox Potential Eh (mV) 31" Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)IL-~_l1_b_---, Time I) ~:S.6 Conductance 13'14LJ Temp.oC Gal. Purged I yq. tI'i pH I S.go Redox Potential Eh (m V) ..... 1 '3_'1:....-_---' Turbidity (NTU) Time 1 t35 B Gal. Purged I yq. Lji Conductance 1 3'131 pH &..;1 5_,_8_'_---' Temp.oC 1 ,5 .7.2 Redox Potential Eh (m V) ..... 1 5_1:Z __ ---'1 :3} ~ Turbidity (NTU) 10 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged LJ 1.1 J gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 12.\1 Time to evacuate two casing volumes (2V) T = 2V/Q = I ~OO.b.5 I Number of casing volumes evacuated (if other than two) I 0 If well evacuated to dryness, number of gallons evacuated I 0 N arne of Certified Analytical Laboratory if Other Than Energy Labs tllA ~--------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 0 Heavy Metals tJ 0 250ml 1!J 0 RN03 ~ 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 0 Other (specify) 0 0 Sample volume 0 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth ..... 17_1_,_K._<f __ ---1 Sample Time IL-\::....'-\.:-D_O~ __ --' Comment ~ See instruction MW-28 08-01-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill • Groundwater' Discharge Permit Date: 6/06/2012 Rev. 7.~ Groundwater Monitoring Quality Assurance Plan (QAP) , '. ATTACHl\tE1'71-2 ~()EN.SonA ~: "'RITE 1\tIESA lJRAJ~lU~I MILL ~t)i SeeUlstr\1l;!tion .~;~...,.~~!!'!!.L-"_~,_= .. ,l FIELD DATA \VORKSHEET FOR GROUND\VATER Description of Sampling Event: I ~ G~",Aer &(0 ''';''''0. v.-J",f er .2.01~ I ~". Sampler Name Location (well name): I MW ... .2.q and initials: '-:.J;'-.n~~~-'HeiJ~l~r;::rjl :,: =. J Field Sample ID Date and Time for Purging t-I J~/;....:I~D4.,;I2.0"";;;=".L.::;i ~~ ___ ----I and Sampling (if different) AJ/It ----~------------~ Well Purging Equip Used: [][]pump or [9] bailer Well Pump (if olher than Bennet) IL-Q~E..tl!;.D",,-____ -, Purging Method Used: [IDz casings [QJ3 casings Sampling Event I Q\A().:("~e(" t:1 G-~ Prevo Well Sampled in Sampling Event I t-_M __ w_, -_~_'5_-____ ~ pH Buffer 7JJI &,...;. ,_J.s..:, • .;;.,.C ___ -' pH ButTer 4,0 l.\.O Specific Conductance 1,--_'l~,\..:..t}~ __ ........ IJ1MHOS/ em Well Depth(O.Olft): ( )~"1.00 . Depth to Water Before Purging I lO~. Job Casing Volmnc (y) 4," well:1 \".o.~. 1(·653h) 311 WeU:_ 0 _(.367h) Conductance (avg) pH of Water (avg) ·1 Well Water Temp_ (avg) I ib,,4'~' Redox Potential (Eh)1 \ Z:l Turbid iry I .2-1.:3 Weather Condo l __ --.....;;....4. ________ ----' _ S v,t'\ t1:1 Ext" Amb. Temp. °C (prior sampling event)I......:;..;t....::;!:>;..Ci_--.-l .. 'I Gal. Purged I ~ i. lib Time 'l l'3l1 \ I Gal. Purged ( '31.b 8: I I ! pH I (,.(;7 Conductance Conductance [~k§:~= ~~:J pH I 6,~8 I a; . Temp.oC Temp.oC 1i~}15 ,I .. ~ Redox Potential Eh (mV) I-.J --Z...;:r ~~Lj ... ' _----' Redox Potential Ell (111 V) I hs9 I i Turbidity (NTU) I .:lJ .O I Turbidity (NTU) J:U5 J .! Time Gal. Purged G i=,i~~. TUne f ,t'!il~,,: ::] Gal. Purged 1,3a.J l I i j I Conductance YS,!,g pH I '.b& Conductance 1:1'-2.0 I pHn;:~]::J Temp.oC Temp.oC Ilb ~i I ,I Redox Potential Eh (mV) t g 2.. Redox Potential Eh (m V) I )gl I Turbidity (NTU) 1.2. i . ~ Turbidity (NTU) 12 i..S' I White Mesa Mill " Field Data Worksheet for Groundwater A 10f2 capturx· COMPATIBLE WITIi/,--IH~J&:r--fUNCTION"LIT Mill • Groundwate; O'scharge1'>ermit Oate: 6/06/2012 Rev. 7 .. Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ,.2.1 '1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate 1\\"0 casing volumes (2 V) T= 2V/Q:;; I P-l9 \'i ~ I I 0 10 Name of Certified Analytical Laboratory if Other Than Energy Labs I NIh, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N voes 0 0 3x40 m) 0 .0 HCL 0 0 Nutrients 0 0 100m} 0 0 H2SO4 0 0 Heavy Metals IKI 0 250ml 0 ijl HN03 t29 O · AU Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha O . 0 1,000 ml 0 '0 HN03 0 0 Other (specify) 0 0 Sample vo]ume 0 0 0 0 If preservative is ll$~d, specify Type and Quantity of Preservative: ~Final Depth I 10'1 .'1 t Sample Time [13'45--= U] ! Sec instruction 1comment 01\ 5. *e <>. t 111;:t. -r <>'M U "" a C-MrI" f< e "",n't tor ru'~~ IMl J.. ~",., f 1;~ "'\Jerri, ? vJ~ bt:~"'~ G\.1-\ \ \5 . ? v..("~~d vl~' \ ~~r tJ:-+0+0..1 rk' \ SO tr)l t1""i-es. v.)~tcr ho-c\ v... S j;~ht J. is':''''' icr. ·p",~e enJeA "",d. St\r>'\ pie c" lie d·eJ '" t-i3 't3 L-e.~ ~ A~e o(t ; ... I. ~ a ~ _______ --,IDO not touch this cell (SheetName) ~ on Ii. ~ .. White Mesa Mill Field Data Worksheet for Groundwater / i . : Mill • Groundwater Discharge Permit Groundw.rter Monit~;ing Quality Assurance Plan (O,AP) Date: 6/06J201i~ev. 7. j .... --.. , , '! i OENISOJ)·· : "'1!) MINES : . 'r·t.....~·.~ ............... ....,......, Description of Sam piing Event: AITAClBfENT 1-2 \VH1TE MESA URAt"lIUI\l ~IILL FIELD DATA \\'ORKSHEET FOR GROUI\'n\VATER I ~r3 QW).r't~r G-rc:JU(\4w~'fer . .::l.O};2.. ': .. Location (weB name): 1L........:;M_w_ ... ..:2.--.!.q __ ~ ______ -" Sampler Name and initials: . Field Sample ID " MvJ-2.'t-Ogoi.2.0)~ ~,(J. See mSfl'UCtion Dale and Time for Purging [~ -==:l and Sampling (if different) .... 1_M...;..r;.:...:I\~ ______ .....i . IJ~- Well Purging Eq~ip Used:@TIpumpor[9]bailerWellPump(ifotberthanBennet) &..." Q.....:....E _____ P_: ____ ___ Pu.rging Method Used: 002 casings [9]3 casings Sampling Event I Q~t"i(!r~ &W Prevo Well Sampled in Sampling Event. ~1..;...::J/l_vJ_-~_· _____ ___' pH Btlffcr 7.0 pH Buffer 4 0 y.o Specific Conductance .... 1 --.l.qq...;..t)~ __ --..IhtMHOSI em Well Depth(O.O 1ft): 112:"100 Depth to Water Before Purging I ) 02.. \ ~ Casing Volume (V) 4tf well:rl.:.f:,.:....a._.'1=--......;...~1(.653h) 3" Well:_" 0 . (.367h) Conductance (avg) I1Sgq ~~~----------~ pH of Water (avg) Well Water Temp. (avg) f is . '1 1 Redox Potential (Eh)la-....!.I-'"ttj""--_~ Turbidity,-I ..;..t~_.o_._---' Weather Condo Ext'l Amb. Temp. °C (prior sampling event)L-1 ~~y_(I _--I Time @2~~· .. 1 Gal. Purged I ~·~.'3 I Time 11'10" I Gal. Purged 1~~.8~ I Conductam:e 14b'l.D I pH I b.Y3 I Conductance [~siS ~. ] pH Jf.."'11 I Temp_ °c J lb ,Q3 I Temp_ °C 1\2/(1 I Redox Potential Eh (mV) [ l1J I Redox Potential Eh (m V) I l~!> I Turbidity (NTU) Il~J . I )4.D Turbidity (NTU) 1.\'.3 :Q · I Time ~1=:=] Gal. Purged J ~'i. Ob I Time II'3 0[S I .' Gal. Purged I ~~ ,::J.1{ I .' Conductance C9QK:·. ] pH I'.~ I Conductance ~:':::~:] pH I b·'15 I ,. Temp.oC 115.'11 I Temp.oC [~~~L-:::] Redox Potential Eh (mV) I }9 Q.· I Redox Potential Eh (mV) I I'll> ·1 Turbidity <NTU) f }~J I Turbidity (NTU) I Iq,Q, I .. White Mesa Mill Field Data Worksheet for Groundwater A 1 of: capturx-COM PATI 8 I.E' WITH/"'-'WU'-b-FO~I(:T10NALI' Mill -Gr0J.mdwater.Llischarge P~rmit Date: 6/06/2012 Rev. 1. Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged galJon{s) Pmnpillg Rate Calculation Flow Rate (Q), in gpm. 5/60 = I .. .2Ju1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness. number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2VlQ = I 141.1:3 I () " Name of Certified Analytical Laboratory if Other Than Energy Labs . ft...._~...:.:r.::..;.~_· _____ --I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if ot.her than as Preservative Type y N sped fled below) y N Y N VOCs '0 0 3x40 ml 0 0 HeL ,0 ' 0 Nutrjents 0 ', '0 ', 100mi ,:.0 . '0 H2SO4 0 " 0 Heavy Metals ~" 0 250ml :::~' :0 'HN03 ; till " 0-" All Other Non Radiologies 0 0 250ml 0 :' "0 No Prcserv. 0 0 Gross Alpha 0 --0 l,OOO ml ':0 ,' 'D ·' HN03 ,-0 0 Other (sped tY) Sample volume " m ' ':0 :, E1 ~:. 0 ; .,'0 -, " ... "TDS If prcsctvative is used, spcciry- Type and Quantity ofPrcsel'vative: .. Final Depth I lo'-t. '70 Srullple Time l~ lO I See instruction ~omment A ... ri~e.\ 0" s:;)-~ ",t leX!, '1N1ner <tIlJ G.,rrv. f'rek~ -torpvl'j<: ",..~ .$.""pji~ ~lIel1+: ., .. " . P",r~e, bc.~,,, • ..ct I03D, f''''r~e<\ ""~H.ror tJ-~~h\ of 1(,0 1"'1;" .. +':.5, vl"ter ~ #..,. Uft< J.rt:} . rv..r~e. er1ded MJ. -S4f"1fleS corlec1'"J d-+ )'3/0, Len s ;+c d.t )'31$ t---________ ....IIDo not touch this cen (SheetName) White Mesa Mil! : Field Data Worksheet for Groundwater A 2 of capturx· COMPATIBLE W1TH~""'Pk--FUH'TJONAlf' Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 f .. ··--.. ···-------·-.1 a)ENISONr;)~~ . MINIES . FIELD DATA WORKSHEET FOR GROUNDWATER WHITE MESA URANIUM MILL ~_.J See instruction Description of Sampling Event: 1 3 rdl QJ:o..r"te.1"'" Gfo\.J,.tl{}\ \I.S~=ter ao 1~ Location (well name): ..... 1 ..;...fV\_W_-_3_>O _________ ----' Sampler Name and initials: 1~t1(1e.r He, 1'la(A~ If).} Field Sample ill Date and Time for Purging 1 7/10 7~Olq, and Sampling (if different) L-I /'/.--...,;.i'A....::.-_______ ---' Well Purging Equip Used: [IDpump or [QJ bailer Well Pump (if other than Bennet) ..... 1 Q_E_D ______ ....... Purging Method Used: [][]2 casings [QJ3 casings Sampling Event IQv.~r:JOV=l.!:1 u.-.W Prevo Well Sampled in Sampling Event I ..... M_W_-_3_~ ______ ----' pH Buffer 7.0 L-I _7_,_0 ___ ----1 pH Buffer 4.0 Y.n Specific Conductance L-I _q_'l_~..s..-___ ....II flMHOS/ cm Well Depth(O.O 1ft): lL.--lI_o_.o_i'b __ ----I Depth to Water Before Purging 1 7 h. D..5 Casing Volume (V) 4" well:1 ::;L-;;2...1b 1(·653h) 3" Well: 0 (.367h) "--------' Conductance (avg) :;2.0S~ '-----~-----~ pH of Water (avg) L-I -LJ..:..." 2.1C:!.5~ _____ ----I Well Water Temp. (avg) 1 \ :'.56 Redox Potential (Eh)1 ?-.j\ TurbiditYa....1 -=0:....-_---' Weather cond'l L-_C_\elA; __ Y __________ ----I Ext'l Amb. Temp. O( (prior sampling event)a....1 _:J...()_iJ_----I Time 1 1055 Conductance 2..05,5, Temp.oC Redox Potential Eh (mV) Turbidity (NTU) Time I \bSI Conductance l ::.to 59 Temp.oC I 15.56 Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Gal. Purged 1 ,",\~,qo pH 1 7.~7 () Gal. Purged I c\'~. g3 pH 1 7 .q:s 6 Time I I05L Gal. Purged 1 y 3 . Co , Conductance 1 ~o bl.{ Temp.oC Redox Potential Eh (mV) I 2..Y3 Turbidity (NTU) o Time I \Osg Gal. Purged I q L). D S Conductance pHI 7,25 Temp.oC I 15.53 Redox Poterttial Eh (m V) L-I .2._35~_---, Turbidity (NTU) I 0 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I . 'J..Jl T = 2V/Q = I ;2.04.'32. I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o N arne of Certified Analytical Laboratory if Other Than Energy Labs I \ s.e.+ ~ '-l 0 CooS. A \V ~ 1.- Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs Hl D 3x40 ml D ~ HCL ~ D Nutrients III D 100 ml D ~ H2SO4 KI D Heavy Metals ~ D 250ml ~ D HN03 ff] D All Other Non Radiologics m D 250ml D m No Preserv. D 1)?J Gross Alpha ItI D 1,000 ml ~ D HN03 "iJ D Other (specify) ~ D Sample volume D tfJ D l$I &cnel'o.\ ~Y'\o~(J\.'t'\~GS If preservative is used, specify Type and Quantity of Preservative: Final Depth L-I 7_~_._b_' __ ---I Sample Time Comment ~ See instruction MW-30 07-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): ..... 1 _M_w_-_3_1 _________ ..... Sampler Name and initials: 11"C:(\(1e.r-Ro] h t.\~ /Tl1 Field Sample ID Date and Time for Purging 1 77 q / ::2.0 r'l and Sampling (if different) Well Purging Equip Used: [!TIpump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings [QJ3casings Sampling Event I (;)v-.o..rted;>i Gil\) Prevo Well Sampled in Sampling Event 1 M W-3?... pH Buffer 7.0 1.0 Specific Conductance 1-1 _~_Ci_q ____ ..... 1 ~MHOS/ cm Depth to Water Before Purging I bog .lD Conductance (avg) ) q ?,..S L..-~ __________ ~ pH Buffer 4.0 Li.D Well Depth(O.Olft): 1 130.00 Casing Volume (V) ~:: :::::1 '-\:.~ ;" t' pH of Water (avg) 7.SQ 1 (.653h) '-\ 0 . '-12., (.367h) Well Water Temp. (avg) I \S,X<t> Redox Potential (Eh)I-I:z.s __ \ __ --I Turbidity II-_0 ___ .....1 WeatherCond. 1 ?IA'}~ C\ouJ~ Ext'l Amb. Temp. O( (prior sampling event) .... I ~_()_O __ ....J Time 1 )330 Conductance Temp.oC \'i3D Gal. Purged 1 i 0 . :2.4 pH I /\S~ Redox Potential Eh (m V) 2., 0 Turbidity (NTU) Time 1 13~ Gal. Purged 1 ~O ./2.. Conductance pH 7.53 Temp.oC 15.30 Redox Potential Eh (mV) 1-1 _2:_9_9 __ --' Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater Time .... 11_'3_3_1_---1 Gal. Purged I ~O.50 Conductance Temp.oC 15.30 Redox Potential Eh (m V) lL-i0E):2:_· __ ---' Turbidity (NTU) o Time 1 \'333 Gal. Purged 1 <6('). t-til\ Conductance I-ll_q~~~1 _--' pH 17·053 Temp.oC 1 }S.2..7 Redox Potential Eh (m V) .... 1 :L_LtS _____ ---I Turbidity (NTU) 1 0 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = Lo.-I ,_2._\1 ___ --' T = 2V/Q = 13/2..5-"; I Number of casing volumes evacuated (if other than two) 1 0 If well evacuated to dryness, number of gallons evacuated 10 Name of Certified Analytical Laboratory if Other Than Energy Labs 1}S'WA1...) .s~+ '* \J 0 c.~ I J -r\ Y) Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ 0 3x40 ml 0 "fJ HCL t:I 0 Nutrients iLl 0 100 ml 0 ~ H2SO4 rtJ 0 Heavy Metals ~ 0 250ml -r:J 0 HN03 tJ 0 All Other Non Radiologies I!I 0 250ml 0 -t1 No Preserv. 0 ~ Gross Alpha rtJ 0 1,000 ml rJ 0 HN03 "1tJ 0 Other (specify) l!I 0 Sample volume 0 rb 0 '[] &d\eC"CA\ ~1"o("~IAf\'\ (5) If preservative is used, specify Type and Quantity of Preservative: Final Depth Lo.-I _{;Cf_, g_7 __ ----I Sample Time ..... 1 _\3_~ ___ ----, Comment ~ See instruction MW-31 07-09-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) [---·-·· .. ·-.. -· .... · .. -.. -· .. ··-· .. ·· .. ·······1 ji.·.OENISO. N. ~.4~1' . MI.NIES , Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER ~ r~ ~,,"(fGr G-rOUl'd W ~=fe,r' :;LC 1!2 ~ See instruction Location (well name): I ...... M_w_-_3...,;;:;l __________ ---' Sampler Name and initials: I ~Y\n~r" 110 11"J~hN Field Sample ID Date and Time for Purging I 71 ~ ):;"0 \ Q. and Sampling (if different) Well Purging Equip Used: IT[] pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings [QJ3 casings Sampling Event I Q"'lA,-+erl~ c;..W Prevo Well Sampled in Sampling Event L-1_N_f._Ii _______ -I pH Buffer 7.0 7,0 Specific Conductance L-I _---'q~4~g __ --II ~MHOS/ cm Depth to Water Before Purging I 1L\ .75 Conductance (avg) -:sq 07 ~-~------~ pH Buffer 4.0 Well Depth(O.Olft): I ' 3~\5 t) Casing Volume (V) pH of Water (avg) 4" well:1 ~ 7.71 I <.653h) 3" Well: ...... ---::.:;D __ -.l. (.367h) Co./3 Well Water Temp. (avg) I 15.1 g Redox Potential (Eh)1 J.K5 Weather Condo Time 1L-'_'3:>_H_5 _.....I Conductance Temp.oC Redox Potential Eh (mV) Turbidity (NTU) Time 1 13)~ Conductance I ':S~ VC; Temp.oC 1 1$ .llS Redox Potential Eh (mV) Turbidity (NTU) 1 White Mesa Mill Field Data Worksheet for Groundwater Gal. Purged I 77. D3 pH G,/3 19~ C;IS Gal. Purged I 77.LJt pH 1',71 1 lB'q (0,7 Ext'l Amb. Temp. O( (prior sampling event}L-1 ~~O_o ----';---I Time ..... 11_3_1_1 _~ Gal. Purged I 77,::2..5 Conductance I '31;)..2. Temp.oC Redox Potential Eh (mV) ..... 11.;....8_b __ -.I Turbidity (NTU) Time I 13 }3 Conductance 1 ;If J 0 Temp.oC 115 .19 Gal. Purged 177., G8 pH 1 tO~7:;;" Redox Potential Eh (mV) 1 .... 1-"g ..... Y _____ ----' Turbidity (NTU) 1 G.4 1 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged 7g.)~ gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ~ 2. )"7 Time to evacuate two casing volumes (2V) T = 2V/Q = I 3'"1'"1. Sb I Number of casing volumes evacuated (if other than two) I 0 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs .... 1 N--!...:,/ ~ _______ --I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 0 0 100ml 0 0 H2SO4 0 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha tfJ 0 1,000 ml ~ 0 HN03 ~ 0 Other (specify) 0 0 Sample volume 0 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth I is. 0 , 5 1 Sample Time &-1_'3--::'5=--__ ...... Comment ~ See instruction MW-32 07-09-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 MiII-Grol..':,\Jwater Discharge Permit GrOUndw;ter Monitoring Quality Assurance Plan (QAP) Date: 6/06/2012 Rev. 7.: : Jl LJ I " .; llENJSO ' ._ ._ i _ .. A TT ACIB-1ENT 1 ~2 \VIDTE l\fESA URAi"(JUM ~ULL , .;;'J~ Sec instruction -du_ A!J.~~~~~ FIELD DATA "'QRKSHEET FOR GROUND\V A TER Description of Sampling Event: Location (weI) name): W-3S ~~~~------------------~ Sampler Name and initials: I-r;:"\.nn(!('" Hpu;J;;; l rW Field Sample ID Date and Time for Purging '-lj....:./_)_O_/~_i .... ~~ ___ --' and Sampling (if different) I,-,/'J,--:...:.~A~ _________ .....I Well Purging Equip Used: OOpump or [9] bailer Well Pump (if other than Bennet) ,-I Q-=-~-=:D~ ____ ----, Purging Method Used: @]2 casings [9]3 casings Sampling Event I Gh~.,......ted 1 G~ Prev. Well Sampled in Sampling Event I,,--M_W_\-_~_~ _______ .....I pH Bll ffer 7.0 1s....._I...:.--. D ___ ---" pH Buffer 4.0 Specific Conduct~mce ~I _~...:.Ci...;..4~ __ ___"IJlMHos/ em Well Depth(O.Olft): 11~\j ,50 Depth to Water Before Purging W~l)=:J Casing Volume (V) 41t well:1 7 ~ 'lD 1(0653h) 3ft Well: 0 (.367h) ~---- Conductance (avg) J.-.-_4..a...;:;..O.:;..?J;;:.;;D~ ____ ..... pH of Water (avg) 1'-~'~!l.IooiSt.,,;;;;~~ ___ ----J Well Water Temp. (avg) I lb. tot , Redox Potential (Eh)~i&. . ____ 1 Turbid ity t-I _0 __ ----, Weather Condo Ext'l Amb. Temp. O( (prior sampling event)I ________ --' Time I ItjO.5 I Gal. Purged I \b.~] I Time I )liO~ . Gal. Purged []~:~D Conductance [~q~r=::=J pH IG.g£, I Conductance I ~4i.jLi . Temp.oC Ilb,qO I Temp.oC Redox Potential Ell (m V) I ::1...07 I Redox Potential Eh (mV) I 20,5 Turbidity (NTU) I 0 I Turbidity (NTU) I . c I Time I i~01 I GaL Purged L ~:J()_"_::'~':.-J Conductance 19lJi I pH [~;~:1 -= I Temp.oC I lb -'f ,", I Temp.oC Redox Potential Eh (mV) I ;Zoo I Redox Potential Eh (mV) &...1 .r..Jq~g"'---_----I Turbidity (NTU) I tl I Turbidity (NTU) White Mesa Mill field Data Worksheet for Gr<lundwClter Milt • Grolrzdwater ~jschafge Permit Date: 6/06/2012 Rev. 7. Groundwater Monitoring QualitV Assurance Plan (QAP} Volume of Water Purged Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-.1 -:;," ~......;.1....;;.·1 __ ---I gallon(s) Number of casing volumes evacuated (if other than two) If wcJl evacuated to dryness. number of gallons evacuated I e Name of Certified Analytica] Laboratory if Other Than Energy Labs [~A\.._i ~ 6£iio~1 ":f\ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample jf other than as Preservative Type y N specified below) Y N Y VOCs BI 0 3x40 mt 0 El.1 HCL Ei Nutrients ('B 0 lOOml 0 m . H2SO4 [B Heavy Metals Irl 0 250m) -m 0 HN03 ,Ill AU Other Non Radiologies [XI 0 250011 0 'S No Preserv. 0 Gross Alpha ~ 0 1,000 ml 1$1 0 HN03 fil Other (specify) m. 0 Sample volume '0 ~ 0 G-Gflef(>'\ ::rnor9~n',-.s If preservative is used. specii)t Type and Quantity of Preservative,~ .. Final Depth ~I -.....:1..;...V-')~..;..lJI-.·1'--. _ ..... I Sample Time ,~'; See instruction !comment .,:,:~ . A« i\led () l'\ ,,<1-e .... t \:2.'-15 . -''''''rler ~ 1'\6. G-",,, ; f\ P ce~,rI-.t'e.., pw~e. IAn A .so."'l' 1;0 e \l<!11 t P w-~ b~(.\" tXt-~')O . P 1M ~e<\ I.)t 11 -tor !J-. --\-ct... \ of' 80 M I f\ ",,+es . ~",ie(" ~C\~ LleC;\(r PtAr~e eY1J e d c.V)ct ..sl\rvlf"e~ (,OIle.l+~J. c~i t'iJD . LefT SJ;tc 1~~i , 0 .. .. i ~ ~ '--__________ ...... IDo not touch this ceH (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 'm 0 5J Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) I OENISONII).4~ r···_······_····· __ ··········_············_··_·_-_··_-.. ~ {MIN~S J Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 13('3\ QUOfA,..ft:r G-f"ov.(\d \f\)(A-rer 201=t See instruction Location (well name): .... 1 .:...M_W_-% ___________ ...... Sampler Name and initials: r~tlt1lr ~ol1ll4..jlt]t Field Sample ill Date and Time for Purging .... 11_1_1_\ 1_1..._D_12...;...... ____ ...... and Sampling (if different) ;VIA L--_________ ~ Well Purging Equip Used: rnupump or [gJ bailer Well Pump (if other than Bennet) I .... Q_E_D ______ __' Purging Method Used: [!JJ2 casings [gJ3 casings I Mw-I\ Sampling Event 1 QV-G\rt",r~ &\J Prevo Well Sampled in Sampling Event 1-_________ ----1 pH Buffer 7.0 pH Buffer 4.0 '-lot) Specific Conductance 1-1 _tj.;....q_~ ____ ...... 1 !lMHOS/ cm Well Depth(O.Olft): 1 J~ LbO Depth to Water Before Purging 11) 0,55 Casing Volume (V) 4" well:1 7.:2..1 ICo653h) 3" Well:L-. _() ___ ....... (.367h) Conductance (avg) L--y...::l.....;~_S....;;g~ _____ __' pH of Water (avg) Well Water Temp. (avg) 1 \5. tl1 Redox Potential (Eh) 1 3 g::; TurbiditYI,--_O __ ~ Weather Condo IL-__ <:.. ___________ ...... _ ~ v\')'\'"'~ Ext'l Amb. Temp. O( (prior sampling event)IL-:2_1_· __ ...... Time 1 O'ilD Conductance 1 ~qSb Temp.oC 1 \5.70 Redox Potential Eh (m V) Turbidity (NTU) Time 1 Oq\~ Conductance yq~O Temp.oC 15.bO Redox Potential Eh (m V) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Gal. Purged \J.~' pH I/.dJ :3~~ D Gal. Purged 111.111 pH 17.2.0 o Time 1 0 (.111 Gal. Purged 117,5J Conductance 1 y q !;3 pH 1-;.2.0 Temp.oC Redox Potential Eh (m V) L-I ~::;...;;;;.g7~_---, Turbidity (NTU) Time 1 0 4\3 Conductance 1 qq&3 Temp.oC I LS. t)l Gal. Purged I} B· 0 I pH 17.2.0 Redox Potential Eh (m V) &...:1 .3:::...77-=--__ --' Turbidity (NTU) 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged \~.'19 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ~ 217 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I "".50 I 10 Name of Certified Analytical Laboratory if Other Than Energy Labs I J.}WAL 1 .set or Vo (.s Sample Taken Sample Vol (indicate Filtered Preservati ve Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs ~ D 3x40 ml D III HCL EJ Nutrients [11 D 100 ml D ~ H2SO4 rn Heavy Metals rn D 250 ml rn D HN03 [1J All Other Non Radiologics r:E D 250ml D ~ No Preserv. D Gross Alpha ~ D 1,000 ml rn D HN03 rn Other (specify) nI D Sample volume D f£I D G-O"I~('(A' 'I~oreo.(\'(..> If preservative is used, specify Type and Quantity of Preservative: Final Depth I 111.~<b Sample Time I 641 S Comment ~ See instruction Af"t;\}t:.~ on ~;'h~ (1\-1 0"14S. -r"..f\1\t.r D\.n~ Crtl\rr1f\ p'('e$~n'; .t;,r ?",r8(;: ~nJ.. 5~fV)pl;n~ ?v-.r~e be8o.f\ oJ OJ5~. Pv.~~e~ ~e\\ ~(" #:... -totoJ ~ ~S Y\'l;l'\u:\e~, ~~+C(" w~~ Gle().(' thrbv..~~O\A.t th~ }>lAf6'· P~j~, e1Jded qf\tA So."""p}e.s <.ol1~c+tJ a..J-o CfJ5, L~+1 5\'te dl..t o~;22) MW-36 07-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D rn D m 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL r---------·-·-·~ i OENISONI)~~1 j .. ~INES _ FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 3f"J\ Q\A(A.('+ef" Gl'"au,(\a ~+e(" :!iO\.2. ~ See instruction Location (well name): 1-1 _M_W_-_3_7 _________ ---I Sampler Name and initials: 1 J~htr Hoi ha~7Ti-1 Field Sample ID Date and Time for Purging 1 71 \ ~ / Q..o )2.. and Sampling (if different) 1-1 _7_'I_:lO_J_.Q_,,_J_t< _____ ...... Well Purging Equip Used: [gJpump or CQ] bailer Well Pump (if other than Bennet) 1-1 M_Y;_~ ______ --I Purging Method Used: [QJ2 casings [gJ3 casings Sampling Event 1 Q\J\(AnGrG c;:W Prevo Well Sampled in Sampling Event I I-_M_W_-_l ~ ______ -I pH Buffer 7.0 7. () pH Buffer 4.0 q,Q Specific Conductance 1-1 _'1_£:f_q ___ -I1 ~MHOS/ cm Well Depth(O.Olft): I l~l . go Depth to Water Before Purging 1 107. 301 Casing Volume (V) 4" well:1 Q.'1D 1(.653h) 3" Well: 1-. _O __ -......I.(.367h) Conductance (avg) 1-1 _Y:,...Y.l.-Lf..;...2.. ______ --I pH of Water (avg) 7 ·'3k Well Water Temp. (avg) 1 1 q .t15 I Redox Potential (Eh)1 3£3 Turbidityl ~ .23,~ Weather Condo I fo..rll~ G10I.AJ~ Ext'l Amb. Temp. O( (prior sampling event)l .... l_7_o __ ....... Time I 0 b!L9 Gal. Purged 5 Time Gal. Purged Conductance 1 4q4 ~ pH 73& Conductance pH IL-__ ---' Temp.oC Temp.oC Redox Potential Eh (m V) .e:::;L2_b..;;;;.3 __ -......I Redox Potential Eh (m V) 1-1 ___ -......I Turbidity (NTU) 1 :2.3.~ Turbidity (NTU) Time 1 13 go 1 Gal. Purged o Time 1 1'~99 Gal. Purged ~O __ ---, Conductance 1 q Y BE pH Conductance 1 YQQ7 pH 1 G/IO Temp.oC ;X1·16 Temp.oC 1 Iq,80 Redox Potential Eh (m V) a:gc Redox Potential Eh (m V) 1-1 ;t---.;::5:....,.~ __ ...... Turbidity (NTU) 1 q, 1 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) C:>-e1-0~~ V olume of Water Purged "'-1 """T\-:-~:-------' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I'---_D ___ --' T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) I Lqg If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs ~\.JAl-I 5>e:t of 00(50 I -r;11 Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs '1J D 3x40 ml D li1 HCL ~ D Nutrients ~ D 100 ml D ~ H2SO4 129 D Heavy Metals ~ D 250 ml ~ D HN03 'E D All Other Non Radiologics ~ D 250 ml D LI No Preserv. D ~ Gross Alpha 1IJ D 1,000 ml '"1:J D HN03 ~ D Other (specify) [@ D Sample volume D 1EJ D AS! &~Y\er~ \ :!no'("cS (). n \ (.5, If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 ..... 1_;l._L....;;fo'--I __ ---' Sample Time )340 Comment ~ See instruction MW-37 07-19-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) rOE~,s~-~1j1~1 ( MIN~~ ,~ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 1 3r~ Q""o...1"'h·, GfOu..1'\~ lA)O\.t~r ..2,OJ?.. See instruction Location (well name): ..... 1 ..;...lJi..:....;W'----.=bS=-_________ ....... Sampler Name and initials: l~flTlt(" +JO]}J·JA~hr.r Field Sample ID Date and Time for Purging 1 7/ 11 !~O 1 <.. and Sampling (if different) 1#/,4 Well Purging Equip Used: [][]pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event 1 Q\ACArte.rl.;\ &W Prevo Well Sampled in Sampling Event II-_jVl_vJ_-_J_~ _____ ----I pH Buffer 7.0 7.0 pH Buffer 4.0 Specific Conductance 1-1 _'1_'...:..1 ___ ----J1 ~MHOS/ cm Well Depth(O.Olft): 1 '2.1. ~.3 Depth to Water Before Purging 1 ~2. Y l) Casing Volume (V) 4" well:1 ";>8. yg 1(·653h) 3" Well: 6 (.367h) '------_ ...... Conductance (avg) pH of Water (avg) 7.10 Well Water Temp. (avg) 1 1.b.~D Redox Potential (Eh)1 ) g 3 TurbiditYL-1 _0 __ ...... Weather Condo Ext'l Amb. Temp. O( (prior sampling event)L-I.Q_~_' _----I Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH L-.I __ ----I Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (mV) 1'----___ ...... Turbidity (NTU) Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pHL-I ___ ...... Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (mV) L-I ___ ----I Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged D gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I lO,S T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 1 0 Name of Certified Analytical Laboratory if Other Than Energy Labs I A\VAL 1 ~dOf \)0 Cs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs ':tJ D 3x40 ml D ~ HCL ~ D Nutrients !J D 100 ml D ..-f] H2SO4 eJ D Heavy Metals 1tI D 250 ml ~ D HN03 rJ D All Other Non Radiologics ~ D 250ml D ~ No Preserv. D ~ Gross Alpha lJ D 1,000 ml tl D HN03 'EJ D Other (specify) "[] D Sample volume D i9 D ~ (,.e(\~('~\ -:r:",O~l'\~(..S If preservative is used, specify Type and Quantity of Preservative: Final Depth 1-.1 ..a...;) 1...,;.7_. 0_' __ ----' Sample Time Comment ~ See instruction MW-65 07-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL ~ See instruction r------------------------------------------~--­I OENISONI)~.4 j MINIES FIELD DATA WORKSHEET FOR GROUNDWATER -.<----~----.-r"-="'...,O,\---,.....--..,.---"-----------.,,,.----t----------------. Description of Sampling Event: 13 ( Q",,,,,-t<.1" G-""O\U,J\w~+G(' -:l.CJ2,. 1<e.s~r"I1pJ~ Location (well name): ,-I _M_W_-_f:_S _________ ----I Sampler Name and initials: --r;.Ylfle-(" )O:)C)",'a~RH Field Sample ID Date and Time for Purging 1 gIl f:./2..Dl";.. and Sampling (if different) /J/A L--_________ ~ Well Purging Equip Used: ~pump or IT[] bailer Well Pump (if other than Bennet) ICllT1+U'hAOUS Purging Method Used: IT[] 2 casings IT[]3 casings Sampling Event 1 Gl.AlAlfe.d~ G-\J Prevo Well Sampled in Sampling Event I .... __ I\J_!_A _______ ~ pH Buffer 7.0 7.0 pH Buffer 4.0 Specific Conductance .... 1 _Gf_4_'t ____ ...J1 ~MHOS/ cm Well Depth(O.Olft): 1 };2..1.'63 Depth to Water Before Purging 1 ()3. q 0 Casing Volume (V) 4" well:1 3 7 . .5.6 1(.653h) 3" Well: 0 (.367h) '-------' Conductance (avg) ,-I _3_t4_~_5 ______ --, pH of Water (avg) Well Water Temp. (avg) 1 14·'105 Redox Potential (Eh)L-ll_5_9 __ --' TurbiditYL-1 _0 __ ----1 Weather Condo Ext'l Amb. Temp. O( (prior sampling event)I,--)'1_o __ ~ Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH L-I __ ----' Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) ,-I ___ ----' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pHL-I ___ -I Temp.oC Temp.oC Redox Potential Eh (m V) Redox Potential Eh (m V)I L-___ ~ Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged o gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I , 0 . SD T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs iVIA ~----------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs lJ 0 3x40 ml 0 II HCL t1 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 0 0 Sample volume 0 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 120.00 Sample Time 0640 Comment ~ See instruction MW-65 08-16-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) 1~~~~i).4]1 .~.INES . ....--J Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 1 3ra G5"'CA.r:t~r G('ou..J'\J\)j~fer ~c,::z:: ~ See instruction Location (well name): 1 .... _/JI_W_-_7_0 __________ ---I Sampler Name and initials: I :=:r~(\n~(" Hol]/a~/1'H Field Sample ID Date and Time for Purging 11--7 _1...;;1 g:;...;/_:2_D_l_Q. ____ ----I and Sampling (if different) I .... N_~_~ ________ .....I Well Purging Equip Used: [![]pump or @] bailer Purging Method Used: CQJ2 casings @]3 casings Sampling Event I Qv..().r+~rl.~ G-w pH Buffer 7.0 11..-_1._,0 ___ --1 Specific Conductance .... 1 ..... ~ .... ~~~ ___ ---'I !!MHOS/ cm Depth to Water Before Purging I g~·..20 Conductance (avg) r....;1 S=-~.....;:g:::;.;g=-_____ --I Well Pump (if other than Bennet) ,-I Q_~_D ______ ---I I MW-J8 Prevo Well Sampled in Sampling Event '-_________ -.....1 pH Buffer 4.0 I '1,0 Well Depth(O.O 1ft): II..-Q-,-7_, D_O ___ --I Casing Volume (V) pH of Water (avg) 4" well:1 0 IC.653h) 3" Well:1-5-~-0G---I.(.367h) Well Water Temp. (avg) I lb ,lg Redox Potential (Eh)L-1 ...:.,3;;.,..;1-1..1_----1 TurbiditYL-1 _0 __ ----1 Weather Condo Ext'\ Amb. Temp. O( (prior sampling event) .... Ia2_1_() __ --' Time Gal. Purged Time Gal. Purged Conductance pH Conductance pHI L-. __ ----I Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) 11..--___ .....1 Turbidity (NTU) Turbidity (NTU) Time Gal. Purged Time Gal. Purged . Conductance pH Conductance pHL-1 ___ .....I Temp.oC Temp.oC Redox Potential Eh (mV) Red"ox Potential Eh (m V) .... 1 ___ -.....I Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 15. 66 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= I ,,~~ Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I '1B.f,~ I l1g'b~ o o Name of Certified Analytical Laboratory if Other Than Energy Labs #/A ~----------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 0 Heavy Metals 111 0 250ml 1$1 0 HN03 [1J 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) TEl 0 Sample volume 0 ~ 0 m +10u.,~je. If preservative is used, specify Type and Quantity of Preservative: Final Depth I q~ 17..5 Sample Time I OCf.:!;5 Comment ~ See instruction MW-70 07-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 TabC Field DataWorksheets Accelerated Monitoring TabC1 Field Data Worksheets Accelerated Monitoring August 2012 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) ATTACHMENT 1-2 ,----------------------------------1 WHITE MESA URANIUM MILL OENISONI)~~I ~_~~.!!~n:~_~ ___ .,_J FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 Av~u~ t (V\ ~(\.t''''' \ Y &r-a ()V'v~ W D.J t-(..J("' 20) ~ Location (well name): 1&.....::..JV\---"\..a..o:,_..J....I.\ .... J _________ --' Sampler Name and initials: Field Sample ID Date and Time for Purging 1 liS I Q 7/2Q k ~ and Sampling (if different) Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) ~ See instruction .AlA I QEP Purging Method Used: [][]2 casings [QJ3 casings Sampling Event I M Q!I\ t"" 1 i 6m" .. ..A"",,,,fui Prev 0 Well Sampled in Sampling Event I M vJ ../ ;LS pH Buffer 7.0 7, 0 pH Buffer 4.0 1-i ,0 I Specific Conductance 1-1 _~.!-q..!...-!.Cj __ --'I ~MHos/ cm Depth to Water Before Purging I Conductance (avg) 2 ~ 7 q Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:1 '),7. $'l I <o653h) 3" W ell:L-. --'0""---_---'. (. 367h) 7~Y\ Well Water Temp. (avg) 1 16, ~6 I Redox Potential (Eh)1 ]:3 g Turbidity ...... 1 _~O~----I Weather Condo I 5 CJoI'vA.1 Ext'l Amb. Temp. O( (prior sampling event)lL..-...;..l -:.Cf_b_---' ~---------------' Time 112.1> Gal. Purged 1 SE ... 55 I Conductance 1 ~g7g pH 1 7J 3$ I Temp. °C I 1 b ... "3 g Redox Potential Eh (mV) 1""'---.....I.J=S...:.7_---' Turbidity (NTU) 22 Time 112g Gal. Purged Conductance Temp.oC 2<l76 I 1G.0,", 1 Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater pH £b qg 1-,'1:2-I Time I):; 7 Gal. Purged 5SJ 7t I Conductance 2~ 7q I pH 1 7, ~ ~ Temp.oC 1(,/37 I Redox Potential Eh (m V) I 1 '57 Turbidity (NTU) Time I 11 ~9 Conductance Temp.oC I Gal. Purged 2gg3 1 1 G .. ~7 1 Redox Potential Eh (m V) I 1 ')J I Turbidity (NTU) 0 I 1 of 2 -tJ Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I • 1. 17 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V /Q = I 25 ~,,1.>17 I AlA N arne of Certified Analytical Laboratory if Other Than Energy Labs 1L....L.;t/~A~ _____ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs D D 3x40 ml D D HCL D D Nutrients D D 100 ml D D H2SO4 D D Heavy Metals ~ D 250 ml ~ D HN03 ro D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) D D Sample volume D D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I gS. ~~ Sample Time 1136 See instruction Comment A,..r\v~~ 0""-.sit~ 0....+ 070f!, .. &a...t'~',A. !J..J./\.,,r.. 1p.,..1I\.N"--e..r' ff"'l.J~e,Ar-9t/r' (Jvr~f....J ~~ .s~~Pli~ Gve....-v+-. f\)r-'i>~ bv~t}...v'V o....-t--07~O.. Pvrbe..rA we../J pCJr-' ~60 ~;Y\.0 t~.s· Wc-f~r' W()....$ £ le.~t"' tk.'bVj\k. t7(/~ fvr1:>~' L.e..p~ s;-tr:.. A..-Y l )3S'. MW-11 08-07-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r"""" --... ----.-----.-.----.----.-----.... ---.--.----------.-----, iOENISONI)JJ j ATTACHMENT 1-2 WHITE MESA URANIUM MILL ~ See instruction ; MINES FIELD DATA WORKSHEET FOR GROUNDWATER ~escri;,t;; of S-ampling Event: I AY.b,Ut MDv\. J-:l,v\y G-,..o.!",,/)l\. . .Jc...tr-A ;;2,0/2 Sampler Name Location (well name): I f1 W .... I Y and initials: I bo..r11"", ee..lM(C /6 e Field Sample ID IMW-'J ~ ... O£072oI2. Date and Time for Purging I 6g /07 J 20 .;;L and Sampling (if different) ;VA Well Purging Equip Used: OOpump or [gJ bailer Well Pump (if other than Bennet) Purging Method Used: 00 2 casings [gJ3 casings Sampling Event I YVlOYl·H".1 t O..,.uMJ,w""f,jl Prevo Well Sampled in Sampling Event 1 !1 W~ '30 pH Buffer 7.0 Specific Conductance 1-1 _9_q .... q.a..-__ .....I1 ~MHOS/ cm Depth to Water Before Purging I 1 D 3 • $ b Conductance (avg) ~ gg~ "----~=-----------~ pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) 4" Well: I 3" Well: I G :2. "1..1 (.653h) (3 _(.367h) pH of Water (avg) L---S..6~'k...::~!::::...:!...J ____ --' Well Water Temp. (avg) I 16 .. () 2 I Redox Potential (Eh)1 .:3 7/:; I TurbiditYI'---...lo6~_.....I Weather Cond. I-1 __ 5_u_Y\_V\J_i.!......-_______ .....I Time 1:317 Gal. Purged Conductance I 387:2. pH Temp.oC Redox Potential Eh (mV) ZqJ Turbidity (NTU) o Time 1 1319 Gal. Purged Conductance '3 ? 1:L 1 pH Temp.oC 16. C'7 I Redox Potential Eh (mV) ;57b Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. °C (prior sampling event)1 '20 b Time 1"3) 8 Conductance Temp.oC Gal. Purged 3g<l£ I 16,103 1 Redox Potential Eh (m V) I .3 ~ I Turbidity (NTU) Time I I i3 fAb Conductance I Temp.oC I '" Gal. Purged :s&~:s I } b.,D I ·1 Redox Potential Eh (m V) I :3 5 tt Turbidity (NTU) Q I 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I t 2)"1 T = 2V/Q = I J Y Cf ( VI cr I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated /VA N arne of Certified Analytical Laboratory if Other Than Energy Labs AlA Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs D D 3x40 ml D D HCL D D Nutrients D D 100 ml D D H2SO4 D D Heavy Metals ~ D 250ml ~ D HN03 ~ D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) D D Sample volume D D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I 1 0 1../ .. ';3 D Sample Time Comment ~ See instruction A,\\ve;~ t/o/'... S~}e-c.-..t--\0:5£. 60...;-;\11\. ().,~ rtNAV\J~r ff"GI.st:.Af-' ~c>r fvr}j~ /J...NA S.o..VV\fl·\~. Pv,....,~e.. h6~t....N 1 £>~O .. PtJrf!:/~,;t we.Al 9'~ ~ 1-otA.\ of 16 ~ JIV\ ;"'LJ-re.sj. w~t(..(' -V>(,c..,J l--o~~evr-1--''''-''00..6'--0\.1+ f t>I"'!) e.. l.JL..-9.a-.s:~te.. ""-+-] "3;2.7r MW-14 08-07-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL i ------------------------j i OENISONr.J~~! I MINIES ! FIELD DATA WORKSHEET FOR GROUNDWATER _____ .. "' .... __ ~ ........ __ --.J Description of Sampling Event: I A\Aa""~+ &ro",,)J W(1\.tc-(" ~OJ~ ~ See instruction Location (well name): IL-..:..M.L..,;'\jJ_.-.::...:L!......;S~ ________ ----' Sampler Name and initials: 1-r;Y'lne,-)...Jon /da,:4 h'J-} Field Sample ID Date and Time for Purging ..... 1 __ 1s'=-",-!-=b-,-/_~_D_l_'l.. ___ ---, and Sampling (if different) Well Purging Equip Used: ~pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings [QJ3 casings Sampling Event I MD!'lthQl G-W Prevo Well Sampled in Sampling Event l~fo1_IAl_'-_3_1 _____ ----, pH Buffer 7.0 1L-1~\O ___ -.I pH Buffer 4.0 11.0 Specific Conductance ..... 1 ----:.q...:.~...:.q ___ ..... 1 ~MHOS/ cm Well Depth(O.Olft): ..... 1 _11_~_.O_'O __ -.I Depth to Water Before Purging 1 7~, 80 Casing Volume (V) 4" well:1 :2". q b 1(.653h) 3" Well: 0 (.367h) '-----_ ..... Conductance (avg) ~ ':l. ''-\ '---~~~----------~ pH of Water (avg) L_b_.5_::l ______ ..... Well Water Temp. (avg) 1 \S. ]q Redox Potential (Eh)1 ::,51 TurbiditYL-1 3_" 0 __ ..... Weather Condo Time ' ..... 1:..:..1OS=_-.I Gal. Purged l .s l.\" 2. S Conductance 1 ~202. pH Temp.oC 1 1S.~D Redox Potential Eh (mV) 3bB L........:=-=-=~_.....I Turbidity (NTU) I ~.) Time I 1101 Conductance Temp.oC Redox Potential Eh (m V) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Gal. Purged 1 set C)g pH 1 b15~ 'b'17 ~_D Ext'l Amb. Temp. O( (prior sampling event)1 ~O(5 Time r.....:.ll..;.::l D;....;;:b:::...--.I Gal. Purged 1 S 9 .Y.G Conductance 1 3;2.1lJ pH 1 ~-5~ Temp.oC 1 \S.g~ Redox Potential Eh (mV) I ~53 Turbidity (NTU) Time L-I \ ..... \D~8_-.....I Gal. Purged 15 LJ • 'l 0 Conductance 1 "J;2..2.Z pH 1 ",Sb Temp.oC 1 LS.7~ Redox Potential Eh (mV) ..... 1 ..;;;3;...;;,3_"1 __ .....1 Turbidity (NTU) 3.1 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 11--4-.;..2.._'--.;.7 __ ---1 T = 2V /Q = I7-S t L13 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs I ...... ~_/...;..'A-=--______ .....I Sample Taken Sample Vol (indicate Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients 0 0 100 ml Heavy Metals m 0 250 ml All Other Non Radiologics 0 0 250ml Gross Alpha 0 0 1,000 ml Other (specify) 0 0 Sample volume Final Depth I 7:5, &S Sample Time ....... I l...:...ll_b ___ --' Comment MW-25 08-06-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Filtered y N 0 0 0 0 [i. 0 0 0 0 0 0 0 Preservative Type Preservative Added Y HCL 0 H2SO4 0 HN03 ~ No Preserv. 0 HN03 0 0 If preservati ve is used, specify Type and Quantity of Preservative: 1:1 See instruction ~~ N 0 0 0 0 0 0 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) i--·--··-·----··--··--·· -........ -... ··-·-·····-1 i ()ENISONI)J~1 i MINI:S I ,----~---.- Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER I Au.~ 6-ro~nJl\No...Ter '2:01-:z... ~ See instruction Location (well name): II-JII_W_-_jJO ___________ ......I Sampler Name and initials: I:::r:.t'l(ler HoJ)iJ~/..-rH Field Sample ID Date and Time for Purging I 8/ cc>/ .2..0)0-and Sampling (if different) ,..;//1 ~~~-------~ Well Purging Equip Used: ~pump or [QJ bailer Well Pump (if other than Bennet) ICo(\+;t\lAOu..s Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event I Mo)'\=t"'8 &W Prevo Well Sampled in Sampling Event I I-M_W_-_'3.S ______ --l pH Buffer 7.0 7 .0 pH Buffer 4.0 Specific Conductance ..... 1 _'1,--~_~~ ___ ..... 1 ~MHOS/ cm Well Depth(O.Olft): I \.2.) .33 Depth to Water Before Purging 1 f, g , J 8 4" well:I 2:>~ .10 1(·653h) 3" Well: 0 (.367h) '------~ Casing Volume (V) Conductance (avg) 31.3f. '--~~~-----~ pH of Water (avg) Well Water Temp. (avg) 1 J5." Redox Potential (Eh)1 J 2..5 TurbiditYI-I _0 __ ----1 Weather Condo Ext'l Amb. Temp. O( (prior sampling event} 1-1 ?-_g_o __ ..... Time 1-11_3_W __ --' Gal. Purged Time Gal. Purged Conductance 1I-3....:)~3_b __ .....1 pH 1 ~.bO Conductance pH L..-I __ -----' Temp.oC 1 15.7J Temp.oC Redox Potential Eh (m V) 1L-1_?i5.....;;;.. __ -.....t Redox Potential Eh (m V) 1-1 ___ ---I Turbidity (NTU) 10 Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH 1-1 ___ --' Temp.oC Temp.oC Redox Potential Eh (m V) Redox Potential Eh (m V)I I-___ ---I Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 -~ Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ) O. G Time to evacuate two casing volumes (2V) T=2V/Q= [§ I Number of casing volumes evacuated (if other than two) ID If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs Io...."'-tJ.....;I_A ______ ----' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs ~ 0 3x40 ml 0 1!1 HCL J&l 0 Nutrients ~ 0 100 ml 0 '&l H2SO4 m 0 Heavy Metals ~ 0 250ml ~ 0 HN03 ~ 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ll3 0 Sample volume 0 ~ 0 IKl Ch'o('~J~ If preservative is used, specify lDS Type and Quantity of Preservative: Final Depth I l10, 0 \..1 Sample Time 11...--13_3...:.1 __ ----' Comment ~ See instruction MW-26 08-08-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 r ~~:;~-~:Ij~-~'I WHITE MESA URANIUM MILL __ ... !'lINES I FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 Av£)v.$.} ;v\oV'o.~v..,\'i &\,olJv''vAwov1'if Location (well name): L....I .:....M~W::::...-.... _3.:;...;O=--________ --' Sampler Name and initials: Field Sample ID IMW-::30_ D £072:0t2. Date and Time for Purging 1 D8 I/)7 I ~c> \ ~ and Sampling (if different) ~O\2 Well Purging Equip Used: OOpump or [gJ bailer Well Pump (if other than Bennet) ~ See instruction AI/A , QED Purging Method Used: 002 casings [gJ3 casings Sampling Event IMdIl'lY'v-.\'I G ... O!)~v..>c-+-d Prevo Well Sampled in Sampling Event I I-.L..M----=-=W:.....:.....-.....J_3---=--J ____ ---I pH Buffer 7.0 Specific Conductance 1-1 _.....I1~q!.-q-"--_--J1 ~MHOS/ cm Depth to Water Before Purging ' 75r'3 s? I Conductance (avg) pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) lID 4" well:1 ?:L'&J 1(·653h) 3" Well:L-. _~O __ .....1.(.367h) Well Water Temp. (avg) , J~" L12-Redox Potential (Eh), ..3 )8' Turbidity 10-1 ---:::D~_--, Weather Condo L....1_S_c..>_V\_V'l._'I ________ -----' Ext'l Amb. Temp. O( (prior sampling event) 1-1 ...:...1 q...:...o __ --' Time IQ~6 Gal. Purged Time I 16~1 1 Gal. Purged 1 Ll!:j! 70 1 Conductance pH Conductance 1 :2.0.613 1 pH I b.~~ 1 Temp.oC 16~63 Temp.oC I 15,65 I Redox Potential Eh (m V) Reltox Potential Eh (m V) I 32.~ I Turbidity (NTU) C2 Turbidity (NTU) I (1) I Time I 1 6 2. 2= _ I Gal. Purged Time I 10.23 I Gal. Purged I Y~d1 I Conductance pH Conductance I ~05~ I pH I I1wCjS I Temp.oC Temp.oC I J3.3F I Redox Potential Eh (m V) I ':3 J 3 Redox Potential Eh (m V) I "3O'Q I Turbidity (NTU) D Turbidity (NTU) I 0 I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I II ~17 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I :lOY, ltd I NA N arne of Certified Analytical Laboratory if Other Than Energy Labs '---__ N.;...:A ......... _____ --' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) VOCs D D 3x40 ml Nutrients ~ D 100 ml Heavy Metals ~ D 250 ml All Other Non Radiologics D D 250ml Gross Alpha D D 1,000 ml Other (specify) ~ D Sample volume 0~\ OI;~6 Final Depth I 7~ .. Oh Sample Time Comment A ""'\"";\)-0 rJ... OoA s; t~ 0.. ~ 0656, GtA.,... ..... ;lf\-o...rI\..~ -r &v~o/'VtA' e..ve,.V\v-h, fvr'5~ bt!J .!)~.N tl-,.4-' 66'5, We-t'e-r' WOwS We.\\ -Pt?f" ()... +c9+'e-1 t!JS? 2J.5 M\t\V+c..S. L~+' MW-30 08-07-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Work~heet for Groundwater Y N Y N D D HCL D D D ~ H2SO4 ~ D jgJ D HN03 ~ D D D No Preserv. D D D D HN03 D D D ~ D 181 If preservative is used, specify Type and Quantity of Preservative: ~ See instruction P"'~~AI ~ Po-r-P VI"'".b ~ o..~ .s~N'\.P\;~ t; \ Gc...t' -}k,rov~lA.o u+ P l/f'he.. Pt>rf>e..~ S~.re.. ~~ I ()36. 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) iJ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 1 A \A e \A~+ C; ("'O\AY"\o\ W fA. >ref' :.l.0] ~ ~ See instruction Location (well name): &....1 _M_W_-_3_\ _________ ----' Sampler Name and initials: 1 =rtJ\f)7'~r RolIJj~.<r Field Sample ID Date and Time for Purging 1 ZIC,I!l.012> and Sampling (if different) Well Purging Equip Used: I~ Ipump or [QJ bail.er Well Pump (if other than Bennet) Purging Method Used: [1[]2 casings [QJ3 casings Sampling Event I jAon+hld GW Prevo Well Sampled in Sampling Event 1&.....M_0-_~ _______ ----I pH Buffer 7.0 7.D pH Buffer 4.0 g.o Specific Conductance &....1 .....;q_ti...:.~ ___ ----II /lMHOS/ cm Well Depth(O.Olft): 1 ]30,00 Depth to Water Before Purging I b~. 1 ~ Casing Volume (V) 4" well:1 q O. '39 1(.653h) 3" Well: l) (.367h) '----_......I Conductance (avg) &....1 _]_42_15 _______ ...... pH of Water (avg) Well Water Temp. (avg) Redox Potential (Eh)IL-..'3_'_O_-......I TurbiditylL-2--:;;;;;·3 __ --' WeatherCond. I PO\rl-~ 610\Ad~ Time 1 r~10 Conductance Temp.oC 15. gZ1 Redox Potential Eh (mV) Turbidity (NTU) Time I r~Jx Conductance J':Z:5 Temp.oC Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Gal. Purged I gy. b3 pH 1 b :=]g Gal. Purged &5.06 pH 1'·92) I ;J.., '-J Ext'l Amb. Temp. °C (prior sampling event)&....1 ~_l> __ ......1 Time 1L-'_3_11~----, Gal. Purged 1 ~Y. gy Conductance ''107 pH I 6 .. 81 Temp.oC Redox Potential Eh (m V) ..... 1 ~_}_3 __ -......I Turbidity (NTU) Time I f::,:~~';!~~.) , I }~1~al. Purged I t'S.5OS Conductance 1'1::2..7 I pH I G·1G Temp.oC J5,gg Redox Potential Eh (m V) L..;;.1.2.----:;;43~_-......I Turbidity (NTU) 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged ~5 .71 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1 ,,:;2.17 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= 1 37~t30 I 6 C> N arne of Certified Analytical Laboratory if Other Than Energy Labs Is-M_Vi_fd ______ ----' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 1!1 0 100 ml 0 ~ H2SO4 ill 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 'r9 0 Sample volume 0 'ff;J 0 ~ TD~ If preservative is used, specify S"'W().~( Type and Quantity of Preservative: Gh 1oridc: Final Depth 10..-1 7_0_.q~1 __ ......I Sample Time 10..-1 ...:..)3---.;;..tS __ -----' See instruction Comment Arr~ve.J 0(\ S ;+~ . "'+ 0&35, t;..nner "',,;), & ... rf':" f'r~~n1 -For P"'''<3c:. ",nJ...s /AMf>llj evevr}. ?w·-~e. b~~OI.fl <1\+ D£LjD. H,.(~eO-\11\(.1\ +0, '" +01-."\ of' 3% y>1 l no.+es, W.Je,... V;')o..S. dear +)., .. o"'~), ov.t -the f''''(,~-e.. f'v..r~e en olea M J.. -SL!rr)pJ l'n,j +oov. ?'tA(e. 0..+ 13lS_ L-e,# ~Jie. ~ 1'311 MW-31 08-06-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 r'" -.-.. -............ -...... --..................... -.... -I WHITE MESA URANIUM MILL i OENISONI)~~, i MINI:S I FIELD DATA WORKSHEET FOR GROUNDWATER Descri~i~n of Sam~ii~g Event: 1 Av..'iJ~S:.f (rrov.r\c;twOvtef""' ~OlQ. Location (well name): .... 1 _M_W_ .... _6_S _________ ---' Field Sample ill Sampler Name and initials: ~ See instruction Date and Time for Purging 1 ~/~ /20)~ and Sampling (if different) ~/A '--~~---------' Well Purging Equip Used: [Qjpump or [gJ bailer Well Pump (if other than Bennet) 1...1 _Q_~-=D=-____ ----I Purging Method Used: ~2 casings [gJ3 casings Sampling Event I Moof\.. l::I 6-W Prevo Well Sampled in Sampling Event IL.-M_W_j_l ~ ______ ....... pH Buffer 7.0 7.0 Specific Conductance 1...1 _~.;....q~~ ___ ....J1 !lMHOS/ cm Depth to Water Before Purging 1 J 1 :l.. SS Conductance (avg) LJ I SD L--__ ~ ____________ ~ pH Buffer 4.0 Well Depth(O.Olft): 1 12'1.5 0 Casing Volume (V) pH of Water (avg) 4" well:~/_._t:f_3_----I1 (.653h) 3" Well:, 0 ,(.367h) 6,73 Well Water Temp. (avg) 1 lS.IS Redox Potential (Eh)1 2.-'l-Turbidity I ..... _6 __ ---' Weather cond·1 .... _G __ 'e_C\_( _____________ ---' Ext'l Amb. Temp. O( (prior sampling event) ..... 1 _~_()_b _-......i Time ID830 Gal. Purged 2.1.7 Conductance Temp.oC Redox Potential Eh (m V) ..... 1 _2._~ ..... 3,---_--, Turbidity (NTU) Time I Og3~ Conductance YISq Temp.oC Redox Potential Eh (m V) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 6 Gal. Purged 1 a...~, 13 pH b.i't D Time 10 831 Gal. Purged 12.1. 'f 1 Conductance ..... 1 ~_'_5_~_---, Temp.oC 11S,IS Redox Potential Eh (m V) 1L...:2=-'~1.J.-_----I Turbidity (NTU) Time 1 O~33 Conductance I LJ 1l{5 Temp.oC 1 15.15 o Gal. Purged 1 ~.33 pH 1 6.79 Redox Potential Eh (m V) 1L-:L--=..5 ,l...1 __ ....J Turbidity (NTU) 1 of 2 -iJ -iJ Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged ,;).:),.18 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I · ~17 T = 2V/Q = I "13.1:2-I Number of casing volumes evacuated (if other than two) I 0 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs IL-M_~_~ _______ --, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs D D 3x40 ml D D HCL D Nutrients D D 100 ml D D H2SO4 D Heavy Metals rE D 250 ml ~ D HN03 ~ All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha 'E1 D 1,000 ml tl D HN03 ~ Other (specify) D D Sample volume D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth 11)3.0 g Sample Time I O~3S Comment ~ See instruction Ar(;~ cd on ~ 11-G <At 0 b '-\.5, ~n her "'" J-6-MI';n preSGnt-.for pv.('~e o<1ld. .s."."., ?),~ e \Je,t. Pv.r~e. b~<>." ..... -r O{,5Q, r \A,~ed ~ell .for .... +0+" \ ot 16::' m:.,v..-Tes,. L0,,-+u W«..s clea ... 1-hfOUcl'0u"t" r)\A("~ Y\Ar"{)e. -ended. 4.f1~ SGMpk coll~~ka 0..+ D835. L-c.ft s}t~ a.t 0340 MW-35 08-08-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D D 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) [--.. ----.. -.-.-.-.. --.-.. --.--.-... --.----.....----1 ATTACHMENT 1-2 ~E~~liI)JJj FIELDDA~:r~~=::E~~~~~:O':;~DWATER ~ Seeinsttuction Description of Sampling Event: 1 A Jf,PJt MOrA. ~ \ 'I &(""l)~ W A,;.yd Za"} J). Sampler Name Location (well name): 1 JV\ W ...... b 5 and initials: &: Arlr r ivy P ty\lIVvk=C I () P Field Sample ID Date and Time for Purging 1 d <II CJ7 J 20 I 2. and Sampling (if different) AlA Well Purging Equip Used: [IDpump or @] bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings @]3 casings Sampling Event I..".. 0 VI H, 1 i ? r 0 Li"';' w ",,+;a Prev. Well Sampled in Sampling Event I jV\ t-J..J 36 pH Buffer 7.0 Specific Conductance ..... 1 _......:CJ:.-Cf..!..-LOf __ ...... 1 [!MHOS/ cm Depth to Water Before Purging I 10:>.; ~6 1 Conductance (avg) pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:1 1 t; 2~1(·653h) 3" Well:L... _~I2~_.....I.(.367h) ,4.61 Well Water Temp. (avg) Redox Potential (Eh)1 :375 Turbidity 1 Q Weather Condo 1L-__ 5_J_v\_vV~i ______ ---I Time 1 1 3 ) 7 Gal. Purged Conductance 1 "3 ~72 I pH Temp.oC J .5 .. q7 I Redox Potential Eh (mV) I ;39 I Turbidity (NTU) I Time I 1 '3) ~ Gal. Purged Conductance I p ~Of Z pH Temp.oC Redox Potential Eh (m V) :370 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater I :3ul.,66 1 6~y6 3LJ ,:;0 I 6*~~J Ext'l Amb. Temp. °C (prior sampling event)1 :zoe> Time I 13)g' I Gal. Purged I ~t..l, 2~1 Conductance I 3tg5 1 pH I 6 .. t>J q I Temp.oC I 16.,Q:5 I Redox Potential Eh (mV) I 2g1 I Turbidity (NTU) r C!> I Time I 13~Q I Gal. Purged I -::h!d Ii 7 ;2 1 Conductance I "3~g3 I pH I t"Sa' I Temp.oC I 16~(j.J I Redox Potential Eh (m V) I ~5~ I Turbidity (NTU) I 0 I 1 of 2 -'\J -'\J -'\J Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60= I A 2r7 T = 2V/Q = I p:fctt tj c:r I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Type of Sample if other than as y N specified below) VOCs D D 3x40 ml Nutrients D D 100 ml Heavy Metals ~ D 250ml All Other Non Radiologics D D 250ml Gross Alpha D D 1,000 ml Other (specify) D D Sample volume Final Depth I lOY J :3 0 Sample Time l32J Comment MW-65 08-07-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater AlA I /lJA I AlA Filtered Y N D D D D lL[ D D D D D D D Preservative Type Preservative Added Y HCL D H2SO4 D HN03 ~ No Preserv. D HN03 D D If preservative is used, specify Type and Quantity of Preservative: r-:J See instruction ~(}!l N D D D D D D 2 of 2 TabC2 Field Data Worksheets Accelerated Monitoring September 2012 -1, Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ,-----------------------------------------------------------------~-------I OENI'SONI)~~ i MINI:S '----. -".--~- Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 1 Sep6P'\be.r moY\+l-,b 6ToVV14} C5OJd" ::tOt;).. ~ See instruction Location (well name): ..... 1 _M_W_~J_l __________ .....I Sampler Name and initials: fiO.nner f.}OlIlW!'1t Field Sample ill INIW-)1-64\4 '2.D lQ... Date and Time for Purging I'---.q_/_I'f..;..../_:)./)_I_~ ____ ____' and Sampling (if different) 1-.1/V-i_~_A ________ --, Well Purging Equip Used: []I] pump or [gJ bailer Well Pump (if other than Bennet) I ..... G_f:._D _____ ____' Purging Method Used: ~2 casings [gJ3 casings Sampling Event I rv1 o1\-}b 10 G--W Prevo Well Sampled in Sampling Event I I-. M_W_-_~ ______ ____' pH Buffer 7.0 /.0 pH Buffer 4.0 y,o Specific Conductance 1-.1 _~;....'l_~ ___ ----'I ~MHOS/ cm Well Depth(O.Olft): I 1:)0·00 Depth to Water Before Purging I ~ 7 I ~ 4 Casing Volume (V) 4" well:I..2,·Y.b 1(·653h) 3" Well: D (.367h) '-----_ ...... Conductance (avg) L---.....:.2.,~g~-r..L::s=-____ ----I pH of Water (avg) ..... 1_7 _,4...;..7 ______ --1 Well Water Temp. (avg) I lS. ~'1 Redox Potential (Eh)1 75 TurbiditYI.-I 0 ___ .....1 Weather Condo IL--_G_)_c_a.._( _________ ---' Ext'l Amb. Temp. O( (prior sampling event) 1-.1 _18_b __ --I Time lL..-l.L::3~Y;""'{)_----J Gal. Purged 1 ~q.~ Conductance 1 Q.....87l pH I g.Dg Temp.oC 15,3"{: Redox Potential Eh (m V) go L--___ ...... Turbidity (NTU) o Time 1 l~ '"1 ~ GaL Purged 1 S'j, 6 g Conductance pH Temp.oC Redox Potential Eh (m V) ..... 1 _7_tt'---_---' Turbidity (NTU) 1 0 White Mesa Mill Field Data Worksheet for Groundwater Time 1.-11:...;:3::;...'1_'_---1 Gal. Purged 1 SLJ. L]Z Conductance I ~7~ Temp.oC Redox Potential Eh (m V) 1L--'_7 __ ____' Turbidity (NTU) Time 1 1~Y3 Conductance 1 ~S81 Temp.oC 1 \5, :sg D Gal. Purged 1 5'j ! 4 () pH 1 7.tfJ Redox Potential Eh (m V) 1 ...... 7_'a ___ --' Turbidity (NTU) D 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 55.33 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ,;2. 17 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I ;2..53.)3 I o Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type '-y N specified below) Y N Y VOCs D D 3x40 ml D D HCL D Nutrients D D 100 ml D D H2SO4 D Heavy Metals m D 250ml ~ D HN03 t3 All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) D D Sample volume D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I t,6· 6 f) Sample Time Comment ~ See instruction Arr:~tA 0\,\ ~~i-e. lkt D'l~S. -r/Mlt1lf ~Y1t1 G-o.r("i" prdc:rrf t,r ?\Af":~~r" ~J1a SUn') p))'~ e\Je!l+. f\A.r~e.J be~M ~ D'l3D. p~('~~c\ ~el\ tor If\. +e>1-A.\ of .:lS5 yY);..,v..+<:,s. \J..)O\.1-er \N~ G. '<'b..("". P"'r~~ ~n~ c,d. b\"~ s~ple c l11J~ G1t!A ~ 13 LJ5. Le,.&:'}-~ ~tG ~ 13t;1 MW-11 09-19-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D D 2 of 2 -lJ -tJ Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r------------------------------------------------------------------------------------, IOENISO. Nf)j. j l J M1"tI:S . .=J Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Se. ?!~ r-<bcr rVtoY'rl'l/\8 G-roun J W~+Gr- C:::~ See instruction Sampler Name and initials: 1-'1IA.Tll1e-r HoH,'Ja.;1 /r1t Location (well name): IL.-..:...M..;.-.vJ_-..:....)\1...1...-.-_________ --' Field Sample ill M w -114 _ OG\ \ g 26 l~ Date and Time for Purging 1.-1 _~...;../..;...:}g::...A/;....;;2...;..O_1_'2 ____ ____I and Sampling (if different) 1.-1 M_V~ ________ --, Well Purging Equip Used: []!]pump or [gJ bailer Well Pump (if other than Bennet) Q'E.D 1.--_______ --' Purging Method Used: 00 2 casings [gJ3 casings Sampling Event I yV)ont11~ &\J Prevo Well Sampled in Sampling Event I L-_M_W_ ... _J.S ______ ---' pH Buffer 7.0 7.'0 Specific Conductance I I.-_'f..:..~~~,---__ ---,I ~MHOS/ cm Depth to Water Before Purging 1 \ O?:>. q t) Conductance (avg) "3 ~ ~ I.-----------~ pH Buffer 4.0 9.D Well Depth(O.Olft): 1 l;tg'.7l) Casing Volume (V) pH of Water (avg) 4" well:r 1..;;;;.-b -L-" } q":'----II<.653h) 3" Well:. D .(.367h) 7.13 Well Water Temp. (avg) l Ib, 17 Redox Potential (Eh)1.-1 _fJ_Q. __ ......I TurbiditYI.-I _{) __ -......I Weather Condo iL--_C __ \ C_0--_6 ________ ---' Ext'l Amb. Temp. O( (prior sampling event) 1.-1 ~ __ o_---, Time I l~~S Gal. Purged Conductance pH 17,a:s Temp.oC 1$·\9 Redox Potential Eh (mV) 89 Turbidity (NTU) o Time I 13~7 Gal. Purged Conductance I '3121 pH 1 7 .10 Temp.oC J5114 Redox Potential Eh (m V) go '-----_......I Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater Time 1 14~b Conductance I '3 ~ 3~ Temp.oC Gal. Purged 1 -:s \ .. b g pH 1 7 .]) Redox Potential Eh (m V) 1.-1 _;g_~ __ -......I Turbidity (NTU) Q Time I 1 L1 2.g Gal. Purged I ~. 1 J Conductance I 3., Z8 pH 17. Q g Temp. °C ,,-I _,.:5 ___ 2_0_--, Redox Potential Eh (m V) L-I 7_1-'--__ ---' Turbidity (NTU) o 1 of 2 -iJ -iJ -~ -iJ Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I .. .,.J7 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V /Q = I \ Y C\ ,2S I o Name of Certified Analytical Laboratory if Other Than Energy Labs 1 .... r.l_IA _______ ....... Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 Heavy Metals lJ 0 250ml III 0 HN03 ~ All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 0 0 Sample volume 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth I \OS,S~ Sample Time IIo.....:..-IQ_3_0 __ ----' Comment ~ See instruction Arri\J-eA 'P"'r~e. P\J'f~e. on ~:·h~ ~.} \\'S7. l~nY)"C!r ~~ G-6.rr;f\ 'Pre~er7+ .foc ?",rje An" .slt/)'Jf)j~j even-f. bc:~(,..l') ~1-)2.Cb. ?v..("~cA well -for fA. -tato..\ at 15D yvl:rl"d .. o. ~~1~r w~.s c.\.e~( e(\~e~ 6:.'\1 St1\Mp'e (o\\~(.+<.~ lk-t l~~D. L~-tt ~,-tt:, 1\1-1430. MW-14 09-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 0 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ;_._ ... ------------------------:---------_., I OE ~F3ltl).4~ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Se.p\"eMbe.r jl\antJi )~ LrrouY)d V\SDvfer :2.01Q. ~ See instruction Location (well name): IL.-...;..A_\j\)_-_~ __________ ...... Sampler Name and initials: l--rO-fl n~r-Ho)} I a~ ITt} Field Sample ID Date and Time for Purging 1 '" 71 ~ 72.0 )?... and Sampling (if different) 11..-.M--..;...0_~ _______ ____I Well Purging Equip Used: IT!Jpump or @] bailer Well Pump (if other than Bennet) 1-1 d_'S_D _____ --I Purging Method Used: 00 2 casings @]3 casings Sampling Event I ]"\()nt~fu G-W Prevo Well Sampled in Sampling Event I I..-_M_W_-_~_I _____ ____I pH Buffer 7.0 7.D pH Buffer 4.0 4.0 Specific Conductance 1..-1 --.;4;..,..'\...,:.q ___ ----'1 ~MHOS/ cm Well Depth(O.Olft): 1 115.DD Depth to Water Before Purging 173, bD Casing Volume (V) 4" well:1 2:1.03 1(·653h) 3" Well: D (.367h) '---""-----' Conductance (avg) 1L..-~_2_2_ .. 7 ______ ----, pH of Water (avg) Well Water Temp. (avg) 1 \5.0D Redox Potential (Eh)1..-1 X_46 __ --' TurbiditYI..-I 0_·7 __ ...... Weather Condo Ext'l Amb. Temp. O( (prior sampling event) 1..-1 _15_°_---' Time 1..-1l_1 _~O __ -.....I Gal. Purged 1 Sb.Y Q.. Time 1-11;....1_5 _'_----' Gal. Purged 1 5,G, b3 Conductance 1 32~~ Conductance 32.Z~ Temp.oC 1 l~.O\ Temp.oC lS.OC Redox Potential Eh (mV) Redox Potential Eh (mV) 1..-1 .2_4'1 __ ----' Turbidity (NTU) 0.7 Turbidity (NTU) Time 1 L....: 1...;...15_":l. __ -.....I Gal. Purged 1 S6. is Time 1L.:..1.;..,..;J5;:;..3 __ --I Gal. Purged 157.07 Conductance pH 16SZ:: Conductance 1 322S Temp.oC 15.60 Temp.oC 1 \4. '11 Redox Potential Eh (mV) Redox Potential Eh (m V) L.,;.12S_~ __ ---I Turbidity (NTU) 0.7 Turbidity (NTU) 0.7 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 -'1> -1J -~ Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged 57,50 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I . .2.1/ Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I ,2L./4./{; I I 0 o Name of Certified Analytical Laboratory if Other Than Energy Labs IV/A ~--------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients 0 0 100 ml 0 0 H2SO4 0 Heavy Metals m 0 250ml I2l 0 HN03 ~ All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 0 0 Sample volume 0 0 0 If preservative is used, specify Type and Quantity of Preservative: Final Depth lL-l...;..S_, 6;;....D ___ --I Sample Time Comment ~ See instruction Ar,:ve:a ?IA{"~~ ?\J\.r~-e.. 01'\ ~irc. 0\.+ O-r2.Y. -(ru'W1~(" 1to\1:J~ fr~e'r:!-~r f~"'je.. (1.n~ .sG\fVlp}ir1~ evert1. ~~'" ~+ 0""130. 'f'.M~cA ~d\ tor "-to~ • ...\ or ;I.e..!) M;fI",-t<:.~. W ... +"...-WOoS-c1c"'f ~()~ej, tA¥)~ S~r)~'c. c.o\\e.c.t~ ~+-IlS~. Le-f}-~i+c. ~}-lIEL. MW-25 09-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 0 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 I:E~;~~~1)11 i~~_~INES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: , S.e?1"et1')be r YY1on1't1~ l1,.. b;)~ See instruction WHITE MESA URANIUM MILL ] Location (well name): ..... , _M_W_-AIo __________ -.J Sampler Name and initials: '~n"e.(" H~)JJa"'~/--rJ-} Field Sample ID Date and Time for Purging 'L---__ 4..1.'-/.....;1...l.1 .:../.;,..,.1...;.;;",O..;,..,I'2.. ___ .....J and Sampling (if different) Well Purging Equip Used: [][]pump or @] bailer Well Pump (if other than Bennet) Purging Method Used: @]2 casings @]3 casings Sampling Event 1m 011 til b G-I>J Prev. Well Sampled in Sampling Event 1L...-t1_W_-.....;ll~ _____ ...... pH Buffer 7.0 pH Buffer 4.0 g.D Specific Conductance ..... , _q_~_1 ____ ..... ' ~MHOS/ cm Well Depth(O.Olft): 'J.21.3'3 Depth to Water Before Purging '.5g .. ~O 4" well:1 Yl· 1.5 1(·653h) 3" Well: 0 (.367h) L...-___ .....I Casing Volume (V) Conductance (avg) L...-3_j....L.....,;lg~ _____ ---' pH of Water (avg) 7·YD Well Water Temp. (avg) ,):="q I Redox Potential (Eh) ..... ' _1_5_1 __ ..... Turbidity ..... ' _I._D __ --' Weather Condo C \-eiA/ Ext'l Amb. Temp. O( (prior sampling event)' ..... ;).._\.._'b __ .....1 Time L-'l_9_0~4 _-.....J Gal. Purged b Time Gal. Purged Conductance pH ,7.40 Conductance Temp.oC I rs.O\\ Temp.oC Redox Potential Eh (mV) \5\ Redox Potential Eh (m V) ..... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH ..... I ___ ...... Temp.oC Temp.oC Redox Potential Eh (m V) Redox Potential Eh (m V) I ..... ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged () gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ]0,5 Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated 6 N arne of Certified Analytical Laboratory if Other Than Energy Labs ..... I.,./,_'/_A-_______ --' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs ~ 0 3x40 ml 0 "tJ HCL ~ Nutrients tl 0 100 ml 0 t:I H2SO4 'El Heavy Metals tJ 0 250 ml a 0 HN03 ~ All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 ~ 0 C'" 'or-;b.( If preservative is used, specify Type and Quantity of Preservative: Final Depth IL-'_O_D.!-f qs~ __ ......J Sample Time 11-,.1;.....Y_lD ___ -......J See instruction Comment Arr;"c~ 0" 5\+<:. ~ S~f'Q (. o\l~(,4G~ \1.\0\, -)1\t'\1'\if ~na. 6-bJ'(;'" f'e.~ 1z> c.ol1-<.ct .$o\.~ples~ /k+ \'110. \N().1-er WD.b c ko.r . Lt:.-+t s~'h~ ~~ Jlj 13 MW-26 09-19-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 E 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 ~ See instruction j)ENISONl)j~ WHITE MESA URANIUM MILL MIN(;S FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 5e.preMbCI M~+h13 G"rOlAYlaCA)~+-cr ;20124 Location (well name): IL--M_\I\)_-_3_D _________ ----' Sampler Name and initials: 1~I171e"'" HoIIIJ~X+t Field Sample ID Date and Time for Purging ..... 1 tf..;.;..J_I't......;I'--2.D __ \2 _____ ...... and Sampling (if different) I ..... /\I_/,_~ _______ ----' Well Purging Equip Used: [J[]pump or @] bailer Well Pump (if other than Bennet) L...I 6<_E_D ______ -' Purging Method Used: [ID2 casings @]3 casings Sampling Event 1 rYlon=thll1 G-vJ Prevo Well Sampled in Sampling Event I L... M_W_-_l ~_~ ______ ......I pH Buffer 7.0 7.0 pH Buffer 4.0 g.o Specific Conductance ..... 1 ....;..~_q1..L..-___ ...... 1 ~MHOS/ cm Well Depth(O.Olft): I 110.00 Depth to Water Before Purging 1 75, 8S Casing Volume (V) 4" well:I .2.2,.,~'I 1<·653h) 3" Well:L-. _O ___ .......1.(.367h) Conductance (avg) 2-07b L--_~ ____________ ~ pH of Water (avg) L...-.I7..;.;... $..c::::; __________ -' Well Water Temp. (avg) 1 '5.3\ Redox Potential (Eh)1 1 gS Turbidity 1'----0 __ ----' Weather Condo Time 1 ..... _11_% __ ----' Gal. Purged 1 '-11.7'"\ Conductance pH I g,LS Temp.oC Redox Potential Eh (mV) \7/ L..-!.."":"'-__ ......I Turbidity (NTU) Time ..... 1 .J...:.]]~:L..;...;;7 __ -, Conductance Temp.oC 115,31 D Gal. Purged 1 4~, \7 pH 17.91 Redox Potential Eh (m V)I L-1;.....:4 ...;..1 __ -.......1 Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event) ..... 1 }_3_b __ --' Time 1 J }2...b Gal. Purged 1 Lf 7. iTs Conductance 1 ';)..073 Temp.oC Redox Potential Eh (mV) 1L....:\:..;;:g~9~_-.......I Turbidity (NTU) Time 1.....:11....:..;1 :2.;...;;:8~_.......I Conductance 1 :?-oG;4 Temp.oC 1 1S. ':YJ D Gal. Purged 1 y Z.3Gf pH 17-}3:5 Redox Potential Eh (m V) 1L--111_' __ -.......I Turbidity (NTU) o 1 of 2 -j., Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I ,2.17 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I ~05,5~ I 10 10 Name of Certified Analytical Laboratory if Other Than Energy Labs N/A ~--------------~ Sample Taken Sample Vol (indicate Filtered Preservati ve Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs D D 3x40 ml D D HCL D Nutrients 'lZ!l D 100 ml D ~ H2SO4 .B1 Heavy Metals E D 250 ml ~ D HN03 ~ All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) ~ D Sample volume D 181 D ChloJl'~-c If preservative is used, specify Type and Quantity of Preservative: Final Depth L-17.:...'l.:...:..~1j .... 4 __ ----' Sample Time Comment ~ See instruction Arr i u-e~ 01\ ~ ,-teo.,J-0,'-10. "";'nVlt:r-Nl a Ifnrr: "l P f>GSt:Y1-r -r;,..... p v.1'.j ~ "",,,( :s q,.., pJ/".j P"'r~e.-be~~t1. ~t 07'15. f \Ar~ .. J. 1iII-e1l ~o,... '" +,,-\-.. 1 "f' 22'S Mif\"'+~ V)o-.h" W% ckar. P"'r~~ ~YlJetl 1l\J'I~ Sa"'pJi::) cal1ed~~ ~t J)30 . L. e.f\-~l+ t:.. ~t-ll3Co . MW-30 09-19-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D ~ 2 of2 -/J -'iJ Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: SE.pfCM ber Jv\on+~8 &-ro~n~ wGtf~r .9-.01~ kl_J See instruction Location (well name): I...."M...:.w~ ... _3..;;...\ __________ ---' Sampler Name and initials: I""-;:nner HoJ1/J~~ 1m Field Sample ill Date and Time for Purging 1 ql If< /2..0\'< and Sampling (if different) I;-J/A Well Purging Equip Used: IT!J pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: ~2 casings [QJ3 casings Sampling Event I M 0 ",tb \'=1 (7 \J Prev 0 Well Sampled in Sampling Event II-_N_/t_~ _______ ----I pH Buffer 7.0 7.0 pH Buffer 4.0 1...1.0 Specific Conductance 1-1 -..Jql...l.~...1..1 ___ ----11 !!MHOS/ cm Well Depth(O.Olft): 1 13 O. DO Depth to Water Before Purging I b ~ , Cc Casing Volume (V) 4" well:1 tJ D}-lg ICo653h) 3" Well:l-. _D ___ --I.(.367h) Conductance (avg) I G1 Y 3 ~-~~-----~ pH of Water (avg) 7,JD Well Water Temp. (avg) I-I1_g_'~ __ ----I Redox Potential (Eh)l2. t..t b TurbiditYI-I ..;:;;:g~,7~_--, Weather Condo 1L--_~_1 _t::._o._r _________ ....... Ext'l Amb. Temp. O( (prior sampling event}lL-l:.-.;;S;;.-.6 __ --' Time Gal. Purged 1 gO. 2q Time Gal. Purged 1 gO.56 Conductance Conductance 1L-1.:...q=-.Y...:..q_----I pH I 7,10 Temp.oC Temp.oC 1 }Y,87 Redox Potential Eh (m V) 1a.....c;.;;6 ::...t4.=5 __ -I Redox Potential Eh (m V) 1-1 ..::;..:2.:.~~:..;::Io::::,,-_--, Turbidity (NTU) 1 g.£:, Turbidity (NTU) Time 1 )~:l7 Gal. Purged Time I 132.r Gal. Purged 1 to. CJ l..J Conductance ...... 1 __ 171 __ % __ ---' pH 7.10 Conductance 1454 pH I 7.10 Temp.oC Temp.oC 1 lY y Zf I Redox Potential Eh (mV) Redox Potential Eh (m V) 1-1 ~_Lf __ S __ --I Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 -iJ Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gl.37 gallon(s) Pumping Rate Calculation Flow Rate (Q), in 1pm. S/60 = I . ~ , Time to evacuate two casing volumes (2V) T=2V/Q=1373./Y I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs 1L-N._7._A ______ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients 'i;I 0 100 ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250 ml 0 0 HN03 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 19J 0 "lDS If preservative is used, specify S~\to:r~ Type and Quantity of Preservative: 0h\o,;ae Final Depth I 7 J • ;lS Sample Time Comment ~ See instruction Arr;\}e.~ on ~i+e.. 0..1-0/10. -rq..nnet' Ho\l;a~ y:>-r-e.-~ent f'o.,-?\.Ar~e "Vld. 's<XMpl:f1j evet1f . Pv..('~e., befJo..A fA.+ 0715. f",("~-e~ lNcdl -tor-"'-+01--0..) 0+ 375 m;Y1v..+~.s, w~+er wa..s yv10~1-'~ c.\co..c +~ro\A~~ov..~ ThG f>v\r~c. ?lAr~l:-endoJ. '\nA S4MpJe.,5 Go)1e.G-hJ, qt \ 3'3D. L~ ~l+c:, V\t )~'3'-t MW-31 09-18-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r············· .... ·········· .. ············ .. ······ .. 1 ATTACHMENT 1-2 WHITE MESA URANIUM MILL l OE~~~~.p.4~ FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 15ef)+-GMbe.r rYJontl1k1 6-t"O\AytJ lAh.-r-<,t" .2D12 Sampler Name ~ See instruction Location (well name): 11-l"1~w_ ..... _3S __________ ---I and initials: 1-rQ.Y111 ~r -B oj h'JJlf,~ft1± Field Sample ID Date and Time for Purging ! L-4...:.;../--.;.1....;..~.;..../ :;1._0_12. _____ --' and Sampling (if different) ! ..... _M_Y_~ _______ --, Well Purging Equip Used: IT!Jpump or @] bailer Well Pump (if other than Bennet)! L-_Q_&._.D _____ ....... Purging Method Used: 002 casings @]3 casings Sampling Event l 1Ylon-th1,j Crw Prevo Well Sampled in Sampling Event L-1_M_W_-'_3_D _____ ---I pH Buffer 7.0 1.0 Specific Conductance 1-1 --:,4_lf _~ ___ ---II ~MHOS/ cm Depth to Water Before Purging I /J~..33 Conductance (avg) pH Buffer 4.0 Well Depth(O.Olft): I ');i9,50 Casing Volume (V) pH of Water (avg) 4" W ell:~1-,-.---,~---"t1_--I1 (.653h) 3" Well:. 0 . (.367h) Well Water Temp. (avg) !14. ,6 Redox Potential (Eh)!I-J_h_8 __ ....... Turbidity ..... ! 0--..:.--/7 __ ....... 1 0.7 Weather Condo Ir....-C_kA_{ __________ --' Ext'l Amb. Temp. O( (prior sampling event)Ir....-13_" __ ...... Time O~ll) Conductance '"'\\1\ Temp.oC Redox Potential Eh (mV) Turbidity (NTU) Time 1 041l... Conductance I 9] Gt Gal. Purged I J6 .~7 I D.) I Gal. Purged 1 1 b .7b 1 pH I ".go Temp.oC lL\.C::b 1 Redox Potential Eh (mV) 1(5 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Time 1-1 O_<:f-:.'J_---I Gal. Purged I 16.41 Conductance I 11 l7 ~ Temp.oC Redox Potential Eh (m V) 1-1 .....I.)-.:..7....;;;;c:J~_ ....... Turbidity (NTU) Time I O~ 1:3 Gal. Purged I 1 b,q~ Conductance pH 1 (;.g) Temp.oC Redox Potential Eh (mV) 1-1 -..:i....;:::b=5 __ ....... Turbidity (NTU) 10.7 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged 17.'::>£:. gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1 • ;2.17 T = 2V/Q = 1 73.;t.9 I Number of casing volumes evacuated (if other than two) 1 0 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs /VIA ~--------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) VOCs D D 3x40 ml Nutrients D D 100 ml Heavy Metals ~ D 250 ml All Other Non Radiologics D D 250 ml Gross Alpha ~ D 1,000 ml Other (specify) D D Sample volume Final Depth 1 113. 5i Sample Time O'f IS Comment Y N D D D D ~ D D D KI D D D Y HCL D H2SO4 D HN03 ~ No Preserv. D HN03 ~ D If preservative is used, specify Type and Quantity of Preservative: r::;3 See instruction ~<Zl Arr'ue.A on .sij-e, .d--0150, -l.:l')n(/ "'1). G-eVril1 presurd---Qr pl..lQl"-t<YIJ .s ... mpU~ eW?t'/i 1"A(,~ hoSo..n (At 0755. 'P \Ar~e~ ~el\ -t6r t7v -t()t~l of go MJ'"v..tes. 1N000t~r w~ Glet>.r +1J r0't~ ),0"'+ pu.r~c:. 'P \Af.j eo -d1 tid IlfI A s'IJ-VlpJe (o}}edcd ~-t oq l.s, Lett S'1c O\.f 042( MW-35 09-19-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D D 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater M,onitoring Quality Assurance Plan (QAP) II ()ENISONl)j~ l---------------.-.-.-.. -.. -.-.-.-.----~·-·.-·--------.-.---.. -.. MINI:S t--, ____ .. Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER ,SoLptc.l"'\bc:r Mori+h8 6I'DU."a WCA..t~r ;:2.0\~ ~ See instruction Location (well name): 1-' _fJ._W_-_b_S _________ ---' Sampler Name and initials: 1 1~nne.r f}o}hdl~)fH Field Sample ID Date and Time for Purging ' ~ JI4/~O'2.. and Sampling (if different) ,I-.I0_VA-________ ---I Well Purging Equip Used: I]Dpump or @] bailer Well Pump (if other than Bennet) 1-' _Q_lt_D _____ ----I Purging Method Used: [!IJ 2 casings @]3 casings I ,MW-30 Sampling Event' M0r1+111~ rrW Prevo Well Sampled in Sampling Event 1-_________ ---1 pH Buffer 7.0 Specific Conductance 1-' ---..;q~'1_q ___ ---J1 ~MHOS/ cm Depth to Water Before Purging I 11~, '3:3> Conductance (avg) 1.1 1,0 '----~------------~ pH Buffer 4.0 I LJ, 0 Well Depth(O.Olft): I ,~q, Stl Casing Volume (V) pH of Water (avg) 4" well:1 ""1.'1'1 I <.653h) 3" Well:L-. _~ __ ---'.(.367h) Well Water Temp. (avg) , }I"L bO Redox Potential (Eh) , 1 b g Turbidity' 0., Weather Condo G\eCAf Ext'l Amb. Temp. O( (prior sampling event)L-' _'3.....,..-°_---' Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH L-I __ ----I Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) 1-1 ___ ---' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH L-1 ___ ......I Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) 11...-___ ......1 Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60= I '~17 T=2V/Q= I 13.~Y I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o Name of Certified Analytical Laboratory if Other Than Energy Labs ,.1\//11 ~----------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs D D 3x40 ml D D HCL D D Nutrients D D 100 ml D D H2SO4 D D Heavy Metals "tJ D 250 ml E D HN03 ~ D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha "EJ D 1,000 ml ..g] D HN03 "fI D Other (specify) D D Sample volume D D D D If preservative is used, specify Type and Quantity of Preservative: Final Depth I ) 13 ,S ~ Sample Time Comment ~ See instruction MW-65 09-19-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 TabD <:2uarterly Depth to Water TIME WELL 832 MW-1 1127 MW-2 1324 MW-3 1325 MW-3A 1032 MW-5 1027 MW-11 1036 MW-12 1009 MW-14 1011 MW-15 1331 MW-17 829 MW-18 759 MW-19 1308 MW-20 1300 MW-22 1043 MW-23 1124 MW-24 1005 MW-25 1103 MW-26 841 MW-27 1121 MW-28 1046 MW-29 1049 MW-30 1059 MW-31 1053 MW-32 1018 MW-33 1014 MW-34 1041 MW-35 1015 MW-36 1012 MW-37 Static level 64.30 109.80 83.11 85.15 106.45 87.85 108.49 103.71 106.45 74.36 70.17 54.19 85.63 67.05 114.15 114.25 73.55 74.59 51.46 76.45 101.95 75.82 67.81 74.36 dry 107.94 112.35 110.46 107.25 NAME: Tanner Holliday, Garrin Palmer DATE: 9/27/2012 TIME WELL 944 MW-4 942 TW4-1 945 TW4-2 938 TW4-3 949 TW4-4 935 TW4-5 948 TW4-6 943 TW4-7 940 TW4-8 937 TW4-9 932 TW4-10 947 TW4-11 952 TW4-12 954 TW4-13 956 TW4-14 1103 TW4-15 1101 TW4-16 1053 TW4-17 849 TW4-18 730 TW4-19 932 TW4-20 857 TW4-21 931 TW4-22 1055 TW4-23 929 TW4-24 845 TW4-25 1057 TW4-26 958 TW4-27 Static Level 72.04 64.85 67.26 50.15 70.13 56.81 69.74 68.17 66.55 54.67 55.95 56.96 41.09 46.90 86.45 74.59 59.37 74.36 57.30 59.99 59.95 54.19 53.10 64.45 54.70 49.31 63.11 82.35 TIME 801 756 752 1004 1001 847 842 746 750 834 824 837 826 804 822 818 815 807 810 821 814 811 743 1154 WELL PIEZ-1 PIEZ-2 PIEZ-3 PIEZ-4 PIEZ-5 TWN-1 TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 TWN-14 TWN-15 TWN-16 TWN-17 TWN-18 TWN-19 Static Level 62.08 27.04 41.47 47.74 42.75 53.06 23.66 34.00 43.40 69.55 75.17 87.86 62.20 62.60 80.85 69.50 27.34 45.81 62.46 91.91 47.71 33.79 57.95 52.50 TIME WELL Static Level NA DR-1 ABANDON NA DR-2 ABANDON 1203 DR-5 83.11 1207 DR-6 94.44 1021 DR-7 92.22 1216 DR-8 51.05 1212 DR-9 86.52 1210 DR-10 78.1 1317 DR-11 98.3 1321 DR-12 88.85 1328 DR-13 69.99 1227 DR-14 76.39 1312 DR-15 93 NA DR-16 ABANDON 1230 DR-17 64.97 NA DR-18 ABANDON 1234 DR-19 63.25 1245 DR-20 55.5 1251 DR-21 107.37 1238 DR-22 Dry 1248 DR-23 70.66 1241 DR-24 43.84 NA DR-25 ABANDON TabE Laboratory Analytical Reports -Quarterly Sampling EI\ERGY LABORATORIES WW\Y.energylab.com MaIyticaIExcsUBflC' Sines 1952 Helena, MT 877-412 .. 0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .. ~!lIefte, Wy 8&6.;6B6~7n5 • Rapid City, SO 888~612~1225 • College Station, IX 888~690~2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2012 C12070741 ~001 Client Sample 10: MW~02_07162012 Analyses RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.9 0.2 0.1 Units pCi/l pCi/l pCi/l MOC -Minimum detectable concentration Qualifier RL Report Date: 08/14/12 Collection Date: 07/16/12 12:45 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E900.1 08/01/1209:30/1bb E900.1 08/01/1209:30/1bb E900.1 08/01/1209:30/1bb MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 27 EN:RGY LABORATORIES www.energylab.com AliBlytical ExcsllBflCB Sines 1852 Helena, MT 877-472-0711 • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 gilletJ:B, WV866-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab 10: Client Sample 10: 3rd Quarter Groundwater 2012 C 12070741-002 MW-03_07182012 Analyses MAJOR IONS Fluoride METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.96 51 .1 Units mg/L ug/l Qualifier RL 0.10 5.0 Report Date: 08/14/12 Collection Date: 07/18/1209:55 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By A4500-F C 07/23/12 12:281 jba E200.8 08/05/1209:551 cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 27 EN:RGY LABORATORIES www.energylab.com Analytical ExCBnBflCI Sines 7952 Helena, MT877-412-0711 • Billingst MT 800-735-4489 · Casper, WV 888-235-0515 ~fllett'e,WY 8&6~686-7n~· Rapid City, S[} 888-672-1225 • College station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C 12070741-003 Client Sample ID: MW-03A_07192012 Analyses MAJOR IONS Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 3700 5720 99.3 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l Report Date: 08/14/12 Collection Date: 07/19/1207:00 DateReceived: 07/20/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By o 20 E300.0 07/25/1222:54/ wc 10 A2540 C 07/23/1209:201 ab 5.0 E200.8 08/13/12 13: 15 1 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 27 .1 I EN:RGY LABORATORIES WWiY.energylab.com Analytlt:al ExcsUBflCB Sines '951 Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WV 888-235-0515 ~Hlerle, WY8&6-&86~7175 • Rapid City, S[) 888-&72-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab 10: Client Sample 10: 3rd Quarter Groundwater 2012 C 12070741-004 MW-05_07162012 Analyses METALS -DISSOLVED Uranium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 0.75 ug/l Qualifier Rl 0.30 Report Date: 08/14/12 Collection Date: 07/16/12 14:55 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By E200.8 08/05/12 10:041 cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 6 of 27 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-001A Client Sample ID: MW-11_07112012 Collection Date: 711112012 1210h Received Date: 7/12/2012 1345h Analytical Results Analyzed: 7/13/2012841h Units: Jlg/L Compound Tetrahydrofuran Dilution Factor: Contact: Jo Ann Tischler VOAs by GC/MS Method 8260CIS030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 Surrogate CAS Result Amount Spiked %REC Limits Qual Surr: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 2037-26-5 1868-53-7 460-00-4 17060-07-0 50.2 54.2 53.0 54.9 50.00 100 77-129 50.00 108 80-124 50.00 106 80-128 50.00 110 72-151 Report Date: 7123/2012 Page 14 of 41 All analyses applicable to the CW A, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of t P 1 t . r 1 r f' . f i 'n . n ' . t . r f . f ' hi, . . 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ;:-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-001 Client Sample ID: MW-11_07112012 Collection Date: 7111/2012 1210h Received Date: 7112/2012 1345h Contact: Jo Ann Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mg/L 7/2112012 1734h E200.8 0.100 < 0.100 A _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. A Report Date: 8/28/2012 Page 5 of 41 All analyses applicable to the CW A, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of ~l1h5::p.nnp.nt 11~'" nfthp n:;tn,p nfthlc;;o "(\"""'T'HlIT'i'\1 nT' ~"nl ,..,..."'l"YIh .... ,.. "f'';to C!t"l.Ff" ..... ,.. ................. ..-1" .... +;,.... .... n.f'+l.~ ..... " ... " ............. '"' ....... "'''+~ ........ ~o.+t. +l.. ......... A" .......... ! _____ ... __ ... ~_ ... ! ______ 1 __ C' __ •• __ ~ .1._ ... _ ••.•••• _ • ____ • -.' ',1 ,1 1 t' • t".1 • , r • EI'-ERGY LABORATORIES www.energylab.com Ana/ytiC81 ExCl1nBfll:. Sines 1m c. . 'ffele,na, MT 877~412-011 f 11 Billings, MT 800-735-4489 • Casper,WY 888 .. 235-0515 ,., L J~i:r',~n~', WV.'~,6 .. ~B6~7115 • Rapid Ctty, SD 888-672-1225 • College Station, LX 888·690~2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C 12070448-003 Client Sample ID: MW-11_07112012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TOS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 374 66.5 39 0.48 19.6 0.66 ND 7.4 618 1080 2020 NO NO NO NO NO NO 204 NO 135 NO NO NO NO ND NO 0.73 NO NO 0.3 0.1 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCilL pCilL pCilL MOC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/11/1212:10 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By D A2320 B 07/13/1218:201 jba A2320 B 07/13/1218:201 jba 0.5 E200.7 07/18/12 14:551 sf A4500-CI B 07/19/12 14:441 wc 0.10 A4500-F C 07/13/12 13:581 jba 0.5 E200.7 07/18/12 14:551 sf 0.05 A4500-NH3 G 07/17/1212:48/1r 0.1 E353.2 07/16/12 11 :50 1 Ir 0.5 E200.7 07/18/1214:551 sf 0.5 E200.7 07/18/12 14:551 sf 50 A4500-S04 E 07/20/12 11 :52 1 ab 10 A2540 C 07/13/12 15:51 1 ab 5.0 E200.8 07/25/1207:141 cp 0.50 E200.8 08/01/1215:231 cp 0.50 E200.8 07/25/1207:141 cp 25 E200.8 07/25/1207:141 cp 10 E200.8 07/25/1207:141 cp 10 E200.8 07/25/1207:141 cp 30 E200.7 07/18/1214:55/sf 1.0 E200.8 07/25/1207:141 cp 10 E200.8 07/25/1207:141 cp 0.50 E200.8 08/01/12 15:231 cp 10 E200.8 07/25/1207:141 cp 20 E200.8 07/25/1207:141 cp 5.0 E200.8 07/25/1207:141 cp 10 E200.8 07/25/1207:141 cp 0.50 E200.8 07/25/1207:141 cp 0.30 E200.8 07/25/1207:141 cp 15 E200.8 07/25/1207:141 cp 10 E200.8 07/25/1207:141 cp E900.1 08/08/12 22:251 Ibb E900.1 08/08/12 22:251 Ibb E900.1 08/08/12 22:25 1 Ibb MCL -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix. Page 6 of 54 EN:RGY LABORATORIES www.energyJab.com AflBlytical ExCBllBflCB Sines 1!152 -Helena,MT 877-412~071 t • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 ; ~JlIe.jt~, WY8~6~686,;7115 • Rapid City, S[) 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/1212:10 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2012 C 12070448-003 Client Sample 10: MW-11_07112012 Analyses OAT A QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 3.65 29.8 32.1 2000 1.00 NO NO NO NO NO NO NO NO NO NO 92.0 92.0 80.0 91.0 MCL! Units Qualifier Rl QCl Method Analysis Date / By % A1030 E 08/08/1216:021 sdw meq/l A1030 E 08108/12 16:021 sdw meq/L A1030 E 08108/12 16:021 sdw mg/L A1030 E 08/08/12 16:021 sdw A1030 E 08/08/12 16 :02 1 sdw ug/L 20 SW8260B 07/24/12 00:161 jk ug/L 1.0 SW8260B 07/24/1200:161 jk ug/L 1.0 SW8260B 07/24/12 00:161 jk ug/L 1.0 SW8260B 07/24/1200:161 jk ug/L 1.0 SW8260B 07/24/1200:161 jk ug/L 20 SW8260B 07/24/1200:1 61 jk ug/L 1.0 SW8260B 07/24/1200:161 jk ug/L 1.0 SW8260B 07/24/1200:161 jk ug/L 1.0 SW8260B 07/24/1200:161 jk ug/L 1.0 SW8260B 07/24/1200:161 jk %REC 80-120 SW8260B 07/24/12 00:161 jk %REC 70-130 SW8260B 07/24/12 00:161 jk %REC 80-120 SW8260B 07/24/12 00:161 jk %REC 80-120 SW8260B 07/24/12 00:161 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 54 EI\ERGY LABORATORIES www.energyJab.com Analytical ExCBDBllCI Sines '952 Helena, MT 877 .. 472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 .'~i.II~~e, WY 86&-686-7115 • Rapid City. S[) 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C 12070741-005 Client Sample 10: MW-12_07172012 Analyses METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 20.7 ug/l Qualifier RL 5.0 Report Date: 08/14/12 Collection Date: 07/17/1209:40 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E200.8 08/05/12 10:091 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 27 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-002A Client Sample ID: MW-14_07112012 Collection Date: 7/1112012 1235h Received Date: 7/12/2012 1345h Analytical Results Analyzed: 7/13/20121133h Units: !J.g/L Dilution Factor: Contact: Jo Ann Tischler VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Compound Number Limit Result Qual Tetrahydrofuran Surrogate Surr: Toluene-d8 Surr: Dibromofluoromethane Surr: 4-Bromofluorobenzene Surr: 1,2-Dichloroethane-d4 CAS Result 2037-26-5 51.4 1868-53-7 54.8 460-00-4 55.2 17060-07-0 55.2 109-99-9 1.00 < 1.00 Amount Spiked %REC Limits Qual 50.00 103 77-129 50.00 110 80-124 50.00 110 80-128 50.00 110 72-151 Report Date: 7/23/2012 Page 15 of 41 .1 I 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-002 Client Sample ID: MW-14_07112012 Collection Date: 7/11/2012 1235h Received Date: 7/12/2012 1345h Contact: JoAnn Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mg/L 7121/2012 1739h E200.8 0.100 < 0.100 A _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. A Report Date: 8/28/2012 Page 6 of 41 ~.l~"~:.~:~:~.~~~l!:~~l::~~h: .. ~~~,_~~::,::~,.an.d.~~.~,are p;~o~~~ in accor~nce to ~LAC protocols. Pertinents.an:pling information is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of EI\ERGY LABORAT ORIES www.energylab.com Allalylh;al ExCIIUsnc. Sine, 7152 Helena, MT 877-472~071 t • Billings, MT 808~735~4489 • Casper, WY 888-235-0515 .. ~ . <~'!I'e.tta, WV e66~686~7n5 • Rapid City, S[) 888~672·1225 • College Station, IX 888-690~2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C 12070448-004 Client Sample ID: MW-14_07112012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TOS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO 466 494 19 0.15 151 NO NO 12.2 351 2070 3600 NO NO 1.26 NO NO NO NO NO 2100 NO NO NO NO NO NO 73.1 NO NO 0.2 0.1 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pC ilL pC ilL pCilL MOC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/11/1212:35 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By 0 A2320 B 07/13/1218:281 jba 1 A2320 B 07/13/1218:281 jba 0.5 E200.7 07/18/12 14:591 sf A4500-CI B 07/19/1214:45/wc 0.10 A4500-F C 07/13/1214:09/jba 0.5 E200.7 07/18/12 14:591 sf 0.05 A4500-NH3 G 07/17/12 12:50 /lr 0.1 E353.2 07/16/12 11 :57 /lr 0.5 E200.7 07/18/12 14:591 sf 0.5 E200.7 07/18/1214:591 sf 50 A4500-S04 E 07/20/12 11 :56 1 ab 10 A2540 C 07/13/12 15:51 1 ab 5.0 E200.8 07/25/1207:521 cp 0.50 E200.8 08/01/12 15:451 cp 0.50 E200.8 07/25/1207:521 cp 25 E200.8 07/25/12 07:521 cp 10 E200.8 07/25/1207:521 cp 10 E200.8 07/25/1207:521 cp 30 E200.7 07/18/12 14:591 sf 1.0 E200.8 07/25/1207:521 cp 10 E200.8 07/25/1207:521 cp 0.50 E200.8 08/01/1215:45/cp 10 E200.8 07/25/12 07:521 cp 20 E200.8 07/25/1207:521 cp 5.0 E200.8 07/25/1207:521 cp 10 E200.8 07/25/1207:521 cp 0.50 E200.8 07/25/1207:521 cp 0.30 E200.8 07/25/1207:521 cp 15 E200.8 07/25/1207:521 cp 10 E200.8 07/25/12 07:521 cp E900.1 08/08/1222:25/1bb E900.1 08/08/1222:25/1bb E900.1 08/08/12 22:251 Ibb MCL -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix. Page 8 of 54 EI'.ERGY LABORATORIES www.energyJab.com Analytical Ex~fIfIC. Sines 1m Helena, MT 877~472~0111 • Billings, MT 800~735-4489 . Casper, WY 888-235-0515 ~jll~~e, wy .8~& .. 686w711~ • Rapid Cfty, SO 888-672-1225 • College Station, IX. 888~690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/1212:35 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: Lab ID: 3rd Quarter Groundwater 2012 C 12070448-004 Client Sample ID: MW-14_07112012 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 1.23 51.4 52.7 3300 1.08 ND ND ND ND ND ND ND ND ND ND 99.0 96.0 85.0 104 MCL! Units Qualifier Rl QCl Method Analysis Date / By % A1030 E 08/08/1216:021 sdw meq/L A1030 E 08108/12 16 :02 1 sdw meq/L A1030 E 08/08/1216:021 sdw mg/L A1030 E 08/08/12 16 :02 1 sdw A1030 E 08/08/12 16:021 sdw ug/L 20 SW8260B 07/24/12 00:521 jk ug/L 1.0 SW8260B 07/24/12 00:52 1 jk ug/L 1.0 SW8260B 07/24/12 00 :52 1 jk ug/L 1.0 SW8260B 07/24/12 00:521 jk ug/L 1.0 SW8260B 07/24/12 00:52 1 jk ug/L 20 SW8260B 07/24/12 00:52/ jk ug/L 1.0 SW8260B 07/24/12 00:521 jk ug/L 1.0 SW8260B 07/24/12 00:52 1 jk ug/L 1.0 SW8260B 07/24/1200:521 jk ug/L 1.0 SW8260B 07/24/12 00:521 jk %REC 80-120 SW8260B 07/24/12 00:521 jk %REC 70-130 SW8260B 07/24/1200:521 jk %REC 80-120 SW8260B 07/24/12 00:521 jk %REC 80-120 SW8260B 07/24/12 00:521 jk MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 9 of 54 EI'.ERGY LABORATORIES www.energylab.com Analytical ExCBHBflCe Sincs '952 Helena, MT 877 .. 472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 :Gille.ria, WY8&6:"686~1115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C 12070741-006 Client Sample 10: MW-15_07172012 Analyses METALS -DISSOLVED Iron Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO 120 Units ug/l ug/l Qualifier Rl 30 5.0 Report Date: 08/14/12 Collection Date: 07/17/12 10:50 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By E200.7 07/23/12 14:561 sf E200.8 08/05/12 10:131 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 27 ,EI\ERGY LABORATORIES www.energylab.com Analytical ExcsJIBflCfI SiRes 1!152 Helena, MT 871 .. 472-0711 • Billings, MT 800-735-4489 11 Casper, WV 888-235-0515 _ ~ille.#.~, WY8&6"~B6"7115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C 12070741-007 Client Sample ID: MW-18_07182012 Analyses MAJOR IONS Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Thallium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1900 3220 3.73 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l Report Date: 08/14/12 Collection Date: 07/18/12 13:15 DateReceived: 07/20/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By D 8 E300.0 07/25/1223:121 wc 10 A2540 C 07/23/1209:201 ab 0.50 E200.8 08/05/12 10:181 cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 9 of 27 EN:RGY 1)151" _~nergy\ab.com ~ 'Heiena, MY 811-472-0711 • Billings, MY 881-735-4489 • Casper, WY 888-Us.B515 ~ AnalyticaIExcsUBllCiSi1/Clll!152 J...l .. ,;..:.~.:..;~;~ille.~~, WY8'6:-686~7115 • Rapid City, SI) 888-672-1225 • College Station, 1)( 888-690-2218 LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C 12070741 -008 Client Sample ID: MW -19_07192012 Analyses Result Units MAJOR IONS Nitrogen, Nitrate+Nitrite as N 4.0 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. o -Rl increased due to sample matrix. mg/l Report Date: 08/14/12 Collection Date: 07/19/12 08:00 DateReceived: 07/20/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By o 0.2 E353.2 07/25/1214:34/Ir MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 27 EI\ERGY L ABORATORIES Client: Project: LablD: www.energylab.comHelena.MY877-472-0711 .Billings.MT 800-735-4489 • Casper, WV 888-235-0515 Analylic;afEx~l1fICeSincg'852 ,:"~"",;~,,';~~~~,,~IJI~ffe, WY8&&-6B6-717~ • Rapi~ City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Denison Mines USA Corp 3rd Quarter Groundwater 2012 C12070741-010 Client Sample ID: MW-23_07172012 Report Date: 08/14/12 Collection Date: 07/17/1207:32 DateReceived: 07/20/12 Matrix: Aqueous Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 117 ug/l MCL! Qualifier Rl QCl Method Analysis Date 1 By 1.0 E200.8 08/10/12 09:21 1 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 27 EN:RGY LABORATORIES www.energylab.com AnalyticallxcBHBflCB $incs 1952 Helena, MT 877-472-0711 • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 ·~illefte, W'f8&&-~B6 .. 7175 • Rapid Cfty, SI} 88B-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C12070741-011 Client Sample ID: MW-24_07182012 Analyses METALS -DISSOLVED Cadmium Thallium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 4.70 1.36 Units ug/l ug/l Qualifier RL 0.50 0.50 Report Date: 08/14/12 Collection Date: 07/18/1206:30 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E200.8 08/05/12 10:50 1 cp E200.8 08/07/1204:43 1 cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 13 of 27 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-003A Client Sample ID: MW-25_07102012 Collection Date: 7/10/2012 1220h Received Date: 7/1212012 1345h Analytical Results Analyzed: 7113/20121230h Units: Jlg/L Dilution Factor: Contact: JoAnn Tischler VOAs by GC/MS Method 8260CIS030C Method: SW8260C CAS Reporting Analytical Compound Number Limit Result Qual Tetrahydrofuran Surrogate SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 CAS Result 2037-26-5 50.6 1868-53-7 55.2 460-00-4 53.6 17060-07-0 55.8 109-99-9 1.00 < 1.00 Amount Spiked %REC Limits Qual 50.00 101 77-129 50.00 110 80-124 50.00 107 80-128 50.00 112 72-151 Report Date: 7/23/2012 Page 16 of 41 All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of l 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-003 Client Sample ID: MW-25_07102012 Collection Date: 7110/2012 1220h Received Date: 7/12/2012 1345h Contact: Jo Ann Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mglL 7/2112012 1743h E200.8 0.100 < 0.100 /I. _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. /I. Report Date: 8/28/2012 Page 7 of 41 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use ofthe addressee. Privileges of EN:RGY LABORATORIES WWN.energylab.com Analytic;1I Ex~UBflCI Sine{llm Helena,. MT 877-412-071 1 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 _~ill~~e;, WY 866~6B6-7115 -Rapid Cfty, S[) 888-672-1225 • College Station, TX 888 .. 690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Lab 10: C12070448-005 Client Sample 10: MW-25_071 02012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 396 321 33 0.30 117 0.43 ND 9.3 290 1620 2780 ND ND 1.24 ND ND ND ND ND 1600 ND 11 ND ND ND 0.93 6.45 ND ND 0.7 0.2 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCilL pCilL MDC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/10/12 12:20 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By D A2320 B 07/13/12 18:36/ jba A2320 B 07/13/12 18:361 jba 0.5 E200.7 07/18/12 15:031 sf 1 A4500-CI B 07/19/12 14:551 wc 0.10 A4500-F C 07/13/1214:131 jba 0.5 E200.7 07/18/12 15:031 sf 0.05 A4500-NH3 G 07/17/12 12:521 Ir 0.1 E353.2 07/16/12 12:001 Ir 0.5 E200.7 07/18/12 15:031 sf 0.5 E200.7 07/18/12 15:031 sf 50 A4500-S04 E 07/20/12 12:241 ab 10 A2540 C 07/13/12 15:521 ab 5.0 E200.8 07/25/1207:561 cp 0.50 E200.8 08/01/1215:49/cp 0.50 E200.8 07/25/1207:561 cp 25 E200.8 07/25/1207:561 cp 10 E200.8 07/25/12 07:56 1 cp 10 E200.8 07/25/12 07:561 cp 30 E200.7 07/18/12 15:031 sf 1.0 E200.8 07/25/12 07:56 1 cp 10 E200.8 07/25/1207:561 cp 0.50 E200.8 08/01/1215:491 cp 10 E200.8 07/25/12 07:561 cp 20 E200.8 07/25/1207:561 cp 5.0 E200.8 07/25/12 07:561 cp 10 E200.8 07/25/12 07:561 cp 0.50 E200.8 07/25/1207:561 cp 0.30 E200.8 07/25/1207:561 cp 15 E200.8 07/25/1207:561 cp 10 E200.8 07/25/12 07:561 cp E900.1 08/08/12 22:251 Ibb E900.1 08/08/12 22:251 Ibb E900.1 08/08/12 22:251 Ibb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 10 of 54 EN:RGY LABORATORIES m~1" www.,nergyla~com 1"': '!;';-Helena, MT 877-472-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 . .., ~ Analytical ExcsllBflCB$lnc, 1952 ~. " 9i11e.~l!, Wy 8~6-$B6-7115 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/10/12 12:20 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: LablD: 3rd Quarter Groundwater 2012 C 12070448-005 Client Sample ID: MW-25_07102012 Analyses DATA QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -3.29 41.1 38.5 2600 1.07 ND ND ND ND ND ND ND ND ND ND 96.0 92.0 80.0 101 MCL! Units Qualifier RL QCL Method Analysis Date 1 By 0/0 A1030 E 08/08/12 16 :03 1 sdw meq/L A1030 E 08108/12 16:031 sdw meq/L A1030 E 08108/12 16:031 sdw mg/L A1030 E 08/08/12 16:031 sdw A1030 E 08/08/12 16:031 sdw ug/L 20 SW8260B 07/20/1206:51 1 jk ug/L 1.0 SW8260B 07/20/1206:51 1 jk ug/L 1.0 SW8260B 07/20/1206:51 1 jk ug/L 1.0 SW8260B 07/20/12 06:51 1 jk ug/L 1.0 SW8260B 07/20/12 06:51 1 jk ug/L 20 SW8260B 07/20/1206:51 1 jk ug/L 1.0 SW8260B 07/20/1206:51 1 jk ug/L 1.0 SW8260B 07/20/12 06:51 1 jk ug/L 1.0 SW8260B 07/20/1206:51 1 jk ug/L 1.0 SW8260B 07/20/12 06:51 1 jk %REC 80-120 SW8260B 07/20/1206:51 1 jk %REC 70-130 SW8260B 07/20/1206:51 1 jk %REC 80-120 SW8260B 07/20/1206:51 1 jk %REC 80-120 SW8260B 07/20/1206:51 1 jk MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 11 of 54 American West JI.NALYTICAl LABORATORIES 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80l) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-004A Client Sample ID: MW-26_07112012 Collection Date: 7/11 /2012 951h Received Date: 7/1212012 1345h Analytical Results Analyzed: 7/13/20l21249h Units: J.lg/L Compound Tetrahydrofuran Dilution Factor: Contact: JoAnn Tischler VOAs by GC/MS Method 8260CIS030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 Surrogate CAS Result Amount Spiked %REC Limits Qual SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 2037-26-5 1868-53-7 460-00-4 17060-07-0 49.6 55.5 53.2 55.2 50.00 99.2 77-129 50.00 111 80-124 50.00 106 80-128 50.00 110 72-151 Report Date: 7/23/2012 Page 17 of 41 All "n"lv."s "ooli,,"hlp. tn th" r.W A sow A "nn Rr.R A on, op.rfnnnen in "r.r.nrn"nr.p. tn NET ,Af: nrotncol~_ Pertinent samnlinl! infonnation is located on the attached COc. This reooct is orovided for the exclusive use of the addressee, Privileges of 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-rnail: awal@awal-Iabs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer -Il INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-004 Client Sample ID: MW-26_07112012 Collection Date: 7/1112012 0951h Received Date: 7/12/2012 1345h Analytical Results Date Compound Units Prepared Tin mg/L Date Analyzed 712112012 1748b Contact: JoAnn Tischler DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.100 < 0.100 1\ 1\ _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. Report Date: 8/2812012 Page 8 of 41 1.11 onol"opo onnlieohlp tn th,. rw A s.nw A ""n RrR A "r" n"rfnrmen in "~"nrnance to NELAC orotocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use ofthe addressee. Privileges of EI'£RGY LABORAT ORIES www.energylab.com A~IytiQ11 ExcsllBilCS Sincs 1951 :Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 -=. ~; _, .9i11e.JfEl:i wY ,866-&86~1115 • Rapid City, S(} 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C 12070448-006 Client Sample ID: MW-26_07112012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 382 493 78 0.29 152 0.22 1.9 9.5 189 1730 3060 ND ND ND ND ND ND 773 ND 1100 ND ND ND ND ND ND 28.4 ND ND 1.8 0.3 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/11/1209:51 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By D A2320 B 07/13/12 18:441 jba A2320 B 07/13/12 18:441 jba 0.5 E200.7 07/19/12 17:361 sf A4500-CI B 07/19/12 15:021 wc 0.10 A4500-F C 07/1 3/12 14:161 jba 0.5 E200.7 07/18/12 15:07 1 sf 0.05 A4500-NH3 G 07/17/12 12:541 Ir 0.1 E353.2 07/16/12 12:021 Ir 0.5 E200.7 07/18/1215:071 sf 0.5 E200.7 07/18/12 15:07 1 sf 50 A4500-S04 E 07/20/1212:261 ab 10 A2540 C 07/13/12 15:521 ab 5.0 E200.8 07/25/1208:01 1 cp 0.50 E200.8 08/01/1215:54/cp 0.50 E200.8 07/25/12 08:01 1 cp 25 E200.8 07/25/1208:01 1 cp 10 E200.8 07/25/12 08:01 1 cp 10 E200.8 07/25/12 08:01 1 cp 30 E200.7 07/18/12 15:07 1 sf 1.0 E200.8 07/25/1208:01 1 cp 10 E200.8 07/25/12 08:01 1 cp 0.50 E200.8 08/01/1215:541 cp 10 E200.8 07/25/1208:01 1 cp 20 E200.8 07/25/1208:01 1 cp 5.0 E200.8 08/01/12 15:541 cp 10 E200.8 07/25/1 208:01 1 cp 0.50 E200.8 07/25/1 2 08:01 1 cp 0.30 E200.8 07/25/12 08:01 1 cp 15 E200.8 07/25/12 08:01 1 cp 10 E200.8 07/25/12 08:01 1 cp E900.1 08/08/1 2 22 :25 1 Ibb E900.1 08/08/12 22 :25 1 Ibb E900.1 08/08/1222:25/1bb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 12 of 54 -b EN:RGY LABORAT ORIES WWN.energyi ab.com Analytical Excel/BIles Shlcs 1952 Hel",nar MT 877-472-0111 • Billings, MT 800 .. 735-4489 . Casper, WY 888-235-0515 ~'Ule~a, wY 8~&,;GB6~7175 • Rapip City, SO 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/12 09 :51 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2012 C 12070448-006 Client Sample 10: MW-26_07112012 Analyses OAT A QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.04 44.7 45.6 2900 1.07 MCL! Units Qualifier RL QCL Method Analysis Date / By % A1030 E 08/08/12 16:031 sdw meq/l A1030 E 08108/12 16:031 sdw meq/l A1030 E 08108/12 16:031 sdw mg/l A1030 E 08/08/12 16:031 sdw A1030 E 08/08/12 16:031 sdw MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 13 of 54 EI\ERGY LABORATORIES www.energylab.com Analytical Excsllsm:, smc, 1952 Heferta,M(8n~472.;0111 .. Billings,MT 800-735-4489 · Casper, W'{ 888-235-0515 ,"_Q!JIe,je~'WY;8'"6"QB6':711~" Rapid City, Sf} 888-672-1225 .. College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C12080830-001 Client Sample 10: MW-26_08162012 Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO 970 NO NO 4.9 NO NO NO 90.0 90.0 85.0 98.0 o -RL increased due to sample matrix. Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 08/30/12 Collection Date: 08/16/12 06:40 DateReceived: 08/17/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By 20 SW8260B 08/22/1220:51 1 jk 1.0 SW8260B 08/22/1220:51 1 jk 1.0 SW8260B 08/22/12 20:51 1 jk 0 25 SW8260B 08/29/12 05:31 1 jk 1.0 SW8260B 08/22/12 20:51 1 jk 20 SW8260B 08/22/1220:51 1 jk 1.0 SW8260B 08/22/1220:51 1 jk 1.0 SW8260B 08/22/1220:51 1 jk 1.0 SW8260B 08/22/12 20:51 1 jk 1.0 SW8260B 08/22/12 20:51 1 jk 80-120 SW8260B 08/22/12 20:51 1 jk 70-130 SW8260B 08/22/1220:51 1 jk 80-120 SW8260B 08/22/1220:51 1 jk 80-120 SW8260B 08/22/1220:51 1 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 12 E~RGY LABORATORIES WWN.energylab.com Analytical ExcsllBI/CB SiRes '952 Helena, MT 8.77-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 . '.~flle!t¢, Wy ~&6 .. GB6-7175 • Rapid City, SD 88B-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab ID: 3rd Quarter Groundwater 2012 C12070741-012 Client Sample ID: MW-27 _07162012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 47 6.7 453 1150 1.2 0.3 0.2 Units mg/L mg/L mg/L mg/L pC ilL pCi/L pC ilL MDC -Minimum detectable concentration Report Date: 08/14/12 Collection Date: 07/16/12 11 :15 DateReceived: 07/20/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By D D 1 0.5 4 10 E300.0 E353.2 E300.0 A2540 C E900.1 E900.1 E900.1 MCL -Maximum contaminant level. 07/25/1223:291 wc 07/25/1214:42 fir 07/25/1223:291 wc 07/23/12 09:201 ab 08/01/1209:30/1bb 08/01/1209:30/1bb 08/01/1209:30/Ibb ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 14 of 27 EN:RGY LABORATORIES www.energylab.com Analytical ExcaIIBflCI Sines 1952 ~elena, MT 877·412-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .~ille.tte,WY8~6-GB6-7n5 • Rapid City, S[) 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab 10: Client Sample 10: 3rd Quarter Groundwater 2012 C12070741-013 MW-28_07162012 Analyses MAJOR IONS Chloride Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 105 mg/l o -Rl increased due to sample matrix. Report Date: 08/14/12 Collection Date: 07/16/12 10:35 DateReceived: 07/20/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By o 4 E300.0 07/27/1214:01/wc MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 15 of 27 EN:RGY LABORAT O RIES WViW.energylab.com AnaIytitaIEmnsnc, Sh1C. 1952 . el~{\.a; Mt~811'~412~fi71 j • Billings, Ml 800* 135-4489 • Ca$per, WV 888~235-0515 '1~'~·i'~.;iHt· ~ap.ip.~ttY,:~9,88.:-6t2-J2i5 . Colleg~Stat!o:n, TX888 .. 6~O:,~2·18 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C12080143-001 Client Sample 10: MW-28_08012012 Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 1660 ug/l Qualifier Rl 10 Report Date: 08/24/12 Collection Date: 08/01/1214:00 DateReceived: 08/03/12 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By E200.8 08/20/1215:181 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Paae 3 of 26 r-AlI~"' ~~~-~"'_www~_.e_ner_gy_,a_b._co_m ___ ...::::i=};=~'=! =~::.;..~'. --",,~---:.:.~.H~ele~Qa_,._MT_8_7_7-_4_72_-0_7_1t_, .~' _Bi_lli_ng_s._M.:.-T 8_0_0_-7_35_-_44_8_9 =--e_c_as_pe_r,-=-.wv_' _88_8_"'2::...::3-=-5--=O=-51~5 ~ ~ _ _ = AtJaIytit:aI Ex~/hmcll SIne, 7152 ~ '~iII~tte, WY8~6-&86~117~ • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218 I LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/10/12 13:45 DateReceived: 07/13/12 Matrix: Aqueous ;\ient: ProieCit: LablP: -CUel'\\Sampie 10: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C12070448-001 MW-29_071 02012 ~~------------------------------------------------------------------------ MCL! Aiyses Result Units Qualifier Rl QCl Method Analysis Date / By ..I fTAU -DISSOL VEO on 1270 ug/l 30 E200.7 07/16/12 15:251 sf .. .....---------------------------------------------------------------------------._-------------------------------_._-----------------------------_._-_._-----------.------._--------------_ .. _- Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. MCl -Maximum contaminant level. NO -Not detected at the reporting limit. EN:RGY LABORATORIES wWw,energylab.~om AnaljticalExtJIIIsni:l Silics 1952. LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C 12080 143-002 Client Sample 10: MW-29_08012012 Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 4420 5190 Units mg/l ug/l Qualifier RL 10 10 Report Date: 08/24/12 Collection Date: 08/01 /1 2 1 3: 1 0 DateReceived: 08/03/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By A2540 C 08/06/12 13 :30 1 jz E200.8 08/20/12 15 :23 1 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 26 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer -iJ ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-005A Client Sample ID: MW-30_07102012 Collection Date: 711012012 1100h Received Date: 711212012 1345h Analytical Results Analyzed: 7/13/20121308h Units: J-lg/L Compound Tetrahydrofuran Dilution Factor: 1 Contact: Jo Ann Tischler VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 Surrogate CAS Result Amount Spiked %REC Limits Qual Surr: Toluene-d8 Surr: Dibromofluoromethane Surr: 4-Bromofluorobenzene Surr: 1,2-Dichloroethane-d4 2037-26-5 1868-53-7 460-00-4 17060-07-0 50.4 55.0 56.4 55.8 50.00 101 77-129 50.00 110 80-124 50.00 113 80-128 50.00 112 72-151 Report Date: 7/23/2012 Page 18 of 41 Ii 11 ,n,l"opo 'nnl;~,hlp tn thp rw Ii <:nUIIi on,j RrR Ii orp nprtM"-''',j ;n .~~nr,j.n~p tn NFl _Ar nTOtnro"1.< Pp.rtinp.nt s"",nlin17 information is lor,ated on the attached COc. This reoort is orovided for the exclusive use of the addressee. Privileges of 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-005 Client Sample ID: MW-30_07102012 Collection Date: 7/10/2012 1100h Received Date: 7112/2012 1345h Analytical Results Date Compound Units Prepared Tin mg/L Date Analyzed 712112012 1753h Contact: JoAnn Tischler DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.100 < 0.100 1\ 1\ _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. Report Date: 8/28/2012 Page 9 of 41 -1< EI\ERGY LABORATORIES (111" www ...... gylab.com F~··Ii.le~ MT 87H12-0711 • 8illlng~ 1M 800-735-4489 • CaspeF. WY 888-235-0515 ~ti:.J AnaIyti~'Ex~1If/C1 Sines 1$52 J.~ .. ~~:";,:= .;MI~jte, wY866 .. $86~7n~ • Rapip C[ty, SI) 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C 12070448-007 Client Sample ID: MW-30_071 02012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 182 246 128 0.33 65.9 ND 17 6.2 96.9 733 1570 ND ND ND ND ND ND 43 ND 31 ND ND ND 38.5 ND ND 7.64 ND ND 0.3 0.1 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 'ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/10/12 11 :00 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By D D A2320 B 07/13/12 18:521 jba 1 A2320 B 07/13/1218:52/jba 0.5 E200.7 07/18/12 15:181 sf A4500-CI B 07/19/12 15:031 wc 0.1 0 A4500-F C 07/13/1214:21 1 jba 0.5 E200.7 07/18/1215:18/sf 0.05 A4500-NH3 G 07/17/12 13:201 Ir E353.2 07/16/12 12:051 Ir 0.5 E200.7 07/18/1215:181 sf 0.5 E200.7 07/18/12 15:181 sf 20 A4500-S04 E 07/20/12 12:31 1 ab 10 A2540 C 07/13/12 15:521 ab 5.0 E200.8 07/25/1208:061 cp 0.50 E200.8 08/01/1215:58/cp 0.50 E200.8 07/25/12 08:06 1 cp 25 E200.8 07/25/12 08:061 cp 10 E200.8 07/25/12 08:061 cp 10 E200.8 07/25/12 08:061 cp 30 E200.7 07/18/1215:181 sf 1.0 E200.8 07/25/12 08:061 cp 10 E200.8 07/25/12 08:061 cp 0.50 E200.8 08/01/1215:58/cp 10 E200.8 07/25/12 08:061 cp 20 E200.8 07/25/12 08:061 cp 5.0 E200.8 07/25/12 08:061 cp 10 E200.8 07/25/12 08:061 cp 0.50 E200.8 07/25/12 08:061 cp 0.30 E200.8 07/25/12 08:061 cp 15 E200.8 07/25/12 08:061 cp 10 E200.8 07/25/12 08:061 cp E900.1 08/08/12 22:25 1 Ibb E900.1 08/08/12 22:25 1 Ibb E900.1 08/08/12 22:25 llbb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 14 of 54 EI\ERGY LABORATORIES www.energylab.com Analytical Exf;l1l1l1f1CfI SiRes 1m oil Helena, MT 871-472 .. 071 t • Billings, MT 800-735-4489 • Casper, WY 888 .. 235-0515 , ~iII~~El:, Wt~66.;$B6-'7n5 • Rapid Cfty, S() 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/1 0/12 Report Date: 08/09/12 Collection Date: 07/10/12 11 :00 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: Lab ID: 3rd Quarter Groundwater 2012 C 12070448-007 Client Sample ID: MW-30_071 02012 Analyses DATA QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -2.25 23.1 22.1 1500 1.08 NO NO NO NO NO NO NO NO NO NO 100 90.0 85.0 92.0 MCL! Units Qualifier Rl QCl Method Analysis Date / By 0/0 A1030 E 08/08/12 16:03/ sdw meq/l A1030 E 08108/12 16 :03 1 sdw meq/l A1030 E 08108/12 16:031 sdw mg/L A1030 E 08/08/12 16:031 sdw A1030 E 08/08/12 16:031 sdw ug/L 20 SW8260B 07/20/12 07:281 jk ug/L 1.0 SW8260B 07/20/12 07:281 jk ug/L 1.0 SW8260B 07/20/12 07:281 jk ug/L 1.0 SW8260B 07/20/12 07:281 jk ug/L 1.0 SW8260B 07/20/12 07:281 jk ug/L 20 SW8260B 07/20/12 07:28 1 jk ug/L 1.0 SW8260B 07/20/1207:281 jk ug/L 1.0 SW8260B 07/20/12 07 :28 1 jk ug/L 1.0 SW8260B 07/20/12 07:28 1 jk ug/L 1.0 SW8260B 07/20/1207:281 jk %REC 80-120 SW8260B 07/20/12 07:281 jk %REC 70-130 SW8260B 07/20/12 07:281 jk %REC 80-120 SW8260B 07/20/12 07:281 jk %REC 80-120 SW8260B 07/20/12 07:281 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 15 of 54 I I -iJ ORGANIC ANALYTICAL REPORT Client: Denison Mines Contact: JoAnn Tischler Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-006A Client Sample ID: MW-31_07092012 ANALYTICA L LAB ORATOR I ES Collection Date: 7/9/2012 1335h 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 7/12/2012 1345h Analytical Results Analyzed: 7/13/20121327h Units: J.lg/L Compound Tetrahydrofuran Dilution Factor: 1 VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 Surrogate CAS Result Amount Spiked %REC Limits Qual SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 2037-26-5 1868-53-7 460-00-4 17060-07-0 50.2 53.6 53.8 55.0 50.00 100 77-129 50.00 107 80-124 50.00 108 80-128 50.00 110 72-151 Report Date: 7/23/2012 Page 19 of 41 .\ 11 _ •• _f •• ____ ._ •• 1: __ 1..1.. "--... 1.._ r"nr A ('nUT /I. ....... ..1 Dr"D " ...... ,.... """'.4" ............... .oA ; ........ "' .... ~ ... A."n,... ... t,....l\w r &r nrAt",..."l" Pprhnpnt ctlmnlina infnrtl1;lt;rm ;~ lnr:~tp.n on thf': MtHcheci r.Or:. This renort lS nfovided for the exclusive use of the addressee. Privile es of ( American West ANALYTICAL LABORATORIES 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-006 Client Sample ID: MW-31_07092012 Collection Date: 7/9/2012 1335h Received Date: 7/12/2012 1345h Contact: JoAnn Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mg/L 712112012 1757h E200.8 0.100 < 0.100 1\ _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. 1\ Report Date: 8/28/2012 Page 10 of 41 All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinentsau:pling infonnation is located on th~ att~ched C<?c. This report is provided for the e~cl.usive us~.ofthe addr~ssee. Privileges of Ef\ERGY LABORATORIES www.energylab.com Analyti(;llf Ex~II(lflC1 Sincfll952 ,Helefl3" MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ",,,*~~~~ur~~e,wY866:'GB6~H75 • Rapid Cfty, SD888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Lab 10: C 12070448-008 Client Sample 10: MW-31_07092012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL .. Analyte reporting limit. QCL -Quality control limit. Result NO 202 189 161 0.78 90.1 NO 21 6.0 98.0 529 1400 NO NO NO NO NO NO NO NO NO NO NO NO 74.0 NO NO 8.17 NO NO 0.3 0.1 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC .. Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/09/12 13:35 DateReceived: 07/13/12 Matrix: Aqueous MCl! Qualifier RL QCL Method Analysis Date / By 0 0 A2320 B 07/13/12 19:21 / jba 1 A2320 B 07/13/12 19:21 1 jba 0.5 E200.7 07/18/12 15:221 sf A4500-CI B 07/19/12 15:061 wc 0.10 A4500-F C 07/13/12 14:241 jba 0.5 E200.7 07/18/12 15:221 sf 0.05 A4500-NH3 G 07/17/12 13:08 fir E353.2 07/16/12 12:07 1 Ir 0.5 E200.7 07/18/12 15:221 sf 0.5 E200.7 07/18/12 15:221 sf 10 A4500-S04 E 07/20/12 13:021 ab 10 A2540 C 07/13/12 15:521 ab 5.0 E200.8 07/25/1208:101 cp 0.50 E200.8 08/01/1216:03/cp 0.50 E200.8 07/25/1208:101 cp 25 E200.8 07/25/1208:101 cp 10 E200.8 07/25/1208:101 cp 10 E200.8 07/25/1208:101 cp 30 E200.7 07/18/1215:22/sf 1.0 E200.8 07/25/1208:101 cp 10 E200.8 07/25/1208:101 cp 0.50 E200.8 08/01/1216:03/cp 10 E200.8 07/25/1208:101 cp 20 E200.8 07/25/1208:101 cp 5.0 E200.8 07/25/1208:101 cp 10 E200.8 07/25/1208:101 cp 0.50 E200.8 07/25/1208:101 cp 0.30 E200.8 07/25/1208:101 cp 15 E200.8 07/25/1208:101 cp 10 E200.8 07/25/1208:101 cp E900.1 08/08/1222:25/1bb E900.1 08/08/12 22:251 Ibb E900.1 08/08/12 22 :25 1 Ibb MCL .. Maximum contaminant level. NO .. Not detected at the reporting limit. o .. RL increased due to sample matrix. Page 16 of 54 EN:RGY LABORATORIES www.energylab.com AnalYtical !xt;Bl!ffWi Sines '952 ijeiena, MT&77~472 .. 0711 • Billings, MT 800-735-4489 • Casper, WY 888 .. 235-0515 <,-~_gJUe,~~'t ~t8.;8 .. $86 .. H7~ • Rapid CIty, S[) 888-672-1225 • College Station, TX 888~690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Lab 10: C 12070448-008 Client Sample 10: MW-31_07092012 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 2.10 20.4 21 .3 1300 1.09 NO NO NO NO NO NO NO NO NO NO 94.0 90.0 78.0 94.0 Units % meq/L meq/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 08/09/12 Collection Date: 07/09/12 13:35 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By A1030 E 08/08/12 16:031 sdw A1030 E 08108/12 16:031 sdw A1030 E 08108/12 16:03 1 sdw A1030 E 08/08/12 16:031 sdw A1030 E 08/08/12 16:031 sdw 20 SW8260B 07/18/12 15:341 jk 1.0 SW8260B 07/18/12 15:341 jk 1.0 SW8260B 07/18/1215:34/jk 1.0 SW8260B 07/18/12 15:341 jk 1.0 SW8260B 07/18/1215:341 jk 20 SW8260B 07/18/12 15:341 jk 1.0 SW8260B 07/18/12 15:341 jk 1.0 -SW8260B 07/18/12 15:341 jk 1.0 SW8260B 07/18/12 15:341 jk 1.0 SW8260B 07/18/12 15:341 jk 80-120 SW8260B 07/18/12 15:341 jk 70-130 SW8260B 07/18/12 15:341 jk S 80-120 SW8260B 07/18/12 15:341 jk 80-120 SW8260B 07/18/12 15:34/ jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 17 of 54 EI\.ERGY LABORATORIES WWN.energylab.com AnatytH:aIEtt;BJ/mn;B SineIJ 1952 .. ; ......... Hel!lna, .MT 8n-472~0711 • Billings. MT 800-735-4489 -Casper, WV 888~235-0515 .. ~nlqge, '!l'f 8~8 .. 6B~w7n5 -Rapid C~ty, SD 888-672-1225 -College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/09/12 13:15 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: LablD: 3rd Quarter Groundwater 2012 C 12070448-002 Client Sample ID: MW-32_07092012 Analyses RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.4 0.2 0.2 Units pC ill pCi/l pC ill MOC -Minimum detectable concentration MCL! Qualifier Rl QCl Method Analysis Date / By E900.1 08/08/1222:25/1bb E900.1 08/08/12 22:251 Ibb E900.1 08/08/1222:25/1bb MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 54 ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-007A American West Client Sample ID: MW-35_07102012 ANALYTICAL LABO.RATORIES Collection Date: 7/10/2012 1410h 463 West 3600 South ;alt Lake City, UT 84115 Received Date: 711212012 1345h Analytical Results Analyzed: 7/13/2012 1346h Units: Jlg/L Compound Tetrahydrofuran Dilution Factor: Contact: JoAnn Tischler VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 Surrogate CAS Result Amount Spiked %REC Limits Qual ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dich1oroethane-d4 2037-26-5 1868-53-7 460-00-4 17060-07-0 50.8 50.00 102 77-129 55.1 50,00 110 80-124 55.3 50.00 111 80-128 55.7 50.00 111 72-151 Report Date: 7/23/2012 Page 20 of 41 All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of 1 1 f 1 ('Ii r t' t' p' (' •• • t . 1 .... ::. . t . 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-007 Client Sample ID: MW-35_07102012 Collection Date: 7/10/2012 1410h Received Date: 7/12/2012 1345h Contact: Jo Ann Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mg/L 712112012 1830h E200.8 0.100 < 0.100 A _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. A Report Date: 8128/2012 Page 11 of 41 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COe. This report is provided for the exclusive use of the addressee. Privileges of .f ; ("' f t' 'h' t f ,';n t', t p r 1 1 t , EN:RGY LABORATORIES www.energylab.com l e .... ·•· .. ··.·Hel ••.•• MTIi17-47.2"0711 .Billings.MT 881-735-4489. Casper, WY 888·23$--0515 AnaIyth;aIEtcsUBflC.Sint;s 1m . ~:~=: "-.~Uletfe, 'NY 866~~B6,~7n5 • Rapid City, SI) 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C 12070448-009 Client Sample ID: MW-35_071 02012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 400 504 64 0.35 150 0.08 ND 10.3 366 2230 3860 ND ND ND ND ND ND 131 ND 272 ND ND ND 15.9 ND 0.57 24.5 ND ND 3.5 0.3 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/10/1214:10 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By D D A2320 B 07/13/12 19:37 1 jba 1 A2320 B 07/13/12 19:37 1 jba 0.5 E200.7 07/18/12 15:27 1 sf A4500-CI B 07/19/12 15:081 wc 0.10 A4500-F C 07/13/1214:261 jba 0.5 E200.7 07/18/12 15:27 1 sf 0.05 A4500-NH3 G 07/17/1213:101lr 0.1 E353.2 07/16/1212:10/lr 0.5 E200.7 07/18/1215:271 sf 1 E200.7 07/18/12 15:27 1 sf 50 A4500-S04 E 07/20/1213:05/ ab 10 A2540 C 07/13/12 15:521 ab 5.0 E200.8 07/25/12 08:151 cp 0.50 E200.8 08/01/1216:21 1 cp 0.50 E200.8 07/25/12 08:151 cp 25 E200.8 07/25/12 08:151 cp 10 E200.8 07/25/1208:151 cp 10 E200.8 07/25/1208:151 cp 30 E200.7 07/18/1215:271 sf 1.0 E200.8 07/25/1208:151 cp 10 E200.8 07/25/1208:151 cp 0.50 E200.8 08/01/1216:21 / cp 10 E200.8 07/25/1208:151 cp 20 E200.8 07/25/1208:15/ cp 5.0 E200.8 07/25/1208:151 cp 10 E200.8 07/25/1208:151 cp 0.50 E200.8 07/25/1208:151 cp 0.30 E200.8 07/25/1208:151 cp 15 E200.8 07/25/1208:151 cp 10 E200.8 07/25/12 08:15/ cp E900.1 08/09/12 00:07 / Ibb E900.1 08/09/12 00:07 1 Ibb E900.1 08/09/12 00:07 / Ibb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 18 of 54 Ef\ERGY LABORATORiES www.energylab.com AI18Iyth;;aI Ex~f1:fIC(I s;m;, 1152 . Helell~r MT B77~472 .. 0111 • Billings. MT 800-135-4489 • Casper, WY 888 ... 235-0515 _~ill~j~,WY 8Q,&~GB6':7n~ • Rapip C[ty, SD 888-612-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C 12070448-009 Client Sample ID: MW-35_071 02012 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -0.973 54.8 53.7 3500 1.09 NO NO NO NO NO NO NO NO NO NO 94.0 84.0 75.0 95.0 Units % meq/L meq/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 08/09/12 Collection Date: 07/10/12 14:10 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By A1030 E 08/08/12 16:041 sdw A1030 E 08108/12 16:041 sdw A1030 E 08108/12 16:041 sdw A1030 E 08/08/12 16:041 sdw A1030 E 08/08/12 16:041 sdw 20 SW8260B 07/19/1218:061 jk 1.0 SW8260B 07/19/1218:061 jk 1.0 SW8260B 07/19/1218:06/jk 1.0 SW8260B 07/19/1218:06/jk 1.0 SW8260B 07/19/1218:06/jk 20 SW8260B 07/19/12 18:061 jk 1.0 SW8260B 07/19/12 18:061 jk 1.0 SW8260B 07/19/12 18:061 jk 1.0 SW8260B 07/19/1218:061 jk 1.0 SW8260B 07/19/1218:061 jk 80-120 SW8260B 07/19/1218:061 jk 70-130 SW8260B 07/19/1218:06/jk S 80-120 SW8260B 07/19/1218:061 jk 80-120 SW8260B 07/19/12 18:061 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 19 of 54 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-008A Client Sample ID: MW-36_07112012 Collection Date: 7/1112012 915h Received Date: 7/1212012 1345h Analytical Results Analyzed: 7/13/20121406h Units: J.lg/L Dilution Factor: Contact: Jo Ann Tischler VOAs by GC/MS Method 8260CIS030C Method: SW8260C CAS Reporting Analytical Compound Number Limit Result Qual Tetrahydrofuran Surrogate Surr: Toluene-d8 Surr: Dibromofluoromethane Surr: 4-Bromofluorobenzene Surr: 1,2-Dichloroethane-d4 CAS Result 2037-26-5 50.3 1868-53-7 55.1 460-00-4 54.5 17060-07-0 55.3 109-99-9 1.00 < 1.00 Amount Spiked %REC Limits Qual 50.00 101 77-129 50.00 110 80-124 50.00 109 80-128 50.00 111 72-151 tr Report Date: 7/23/2012 Page 21 of 41 All analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCO This report is provided for the exclusive use of the addressee. Privileges of t pr 'f of f 1 -1 (' po' t f 'f t' po n 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-008 Client Sample ID: MW-36_07112012 Collection Date: 711112012 0915h Received Date: 7112/2012 1345h Contact: Jo Ann Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mg/L 7/2112012 1835h E200.8 0.100 < 0.100 A _ Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. A Report Date: 8/28/2012 Page 12 of 41 All analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of • . 1".' 1",<' 1 ",,',. rot' l' 1'", " • ___ .. !_ .• ___ ~ •. ,_.1._ .1 ....... : _____ ._ .... ____ .. : ______ l __ ~_. __ . ___ ..l ___ .. ___________ ~_ ...... __ ... _.l.; .... _ ••. ; .. t..+t."'_ .... _ .. \..l; ...... ...: ............. f:+ .... ~ ....................... f: ....... n .... . ·1 EI'£RGY LABORATORIES www.energyJab.com AnalYtical Ex~UIIfWi $inc, 1952 Hel~na,MT 877-472-0711 • Billings, MT 801) .. 735-4489 • Casper, WY 888 .. 235-0515 \'~ilteJf~,,~¥8~G~QB6wln~ • Rapid City, SO 888~672~1225 • College Station, IX 888~690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C12070448-010 Client Sample ID: MW-36_07112012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Defin itions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 353 433 60 0.30 134 ND 0.2 8.8 635 2660 4420 ND ND ND ND ND ND ND ND ND ND ND ND 278 ND 0.98 26.5 ND ND 0.6 0.2 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pC ilL pC ilL pC ilL MDC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/11/1209:15 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By D D A2320 B 07/13/12 19:531 jba A2320 B 07/13/1219:531 jba 0.5 E200.7 07/18/1215:30/sf A4500-CI B 07/19/1215:11/wc 0.10 A4500-F C 07/13/1214:291 jba 0.5 E200.7 07/18/12 15:301 sf 0.05 A4500-NH3 G 07/17/1213:1211r 0.1 E353.2 07/16/1212:12/1r 0.5 E200.7 07/18/12 15:301 sf E200.7 07/18/12 15:301 sf 50 A4500-S04 E 07/20/12 13:27 1 ab 10 A2540 C 07/13/1215:53/ab 5.0 E200.8 08/01/1216:43/cp 0.50 E200.8 08/01/1216:43/cp 0.50 E200.8 08/01/1216:43/cp 25 E200.8 08/01/12 16:431 cp 10 E200.8 08/01/12 16:431 cp 10 E200.8 08/01/12 16:431 cp 30 E200.7 07/18/12 15:301 sf 1.0 E200.8 08/01/1216:431 cp 10 E200.8 08/01/12 16:431 cp 0.50 E200.8 08/01/12 16:431 cp 10 E200.8 08/01/12 16:431 cp 20 E200.8 08/01/1216:431 cp 5.0 E200.8 08/01/12 16:431 cp 10 E200.8 08/01/12 16:431 cp 0.50 E200.8 08/01/12 16:431 cp 0.30 E200.8 08/01/12 16:431 cp 15 E200.8 08/01/12 16:431 cp 10 E200.8 08/01/12 16:431 cp E900.1 08/09/12 00:07 1 Ibb E900.1 08/09/12 00:07 1 Ibb E900.1 08/09/12 00:07 1 Ibb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 20 of 54 EN:RGY L ABORATORIES www.energylab.com Analytical Extsllsnci Sines 1152 .' Helena, MT 877-472-071 t, • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 , .~,' "~iir~~~, wy 86.6~686~n75 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/1209:15 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2012 C 12070448-0 1 0 Client Sample 10: MW-36_07112012 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -1.96 62.9 60.5 4100 1.07 ND ND ND ND ND ND ND ND ND ND 97.0 93.0 83.0 95.0 MCL! Units Qualifier RL QCL Method Analysis Date / By 0/0 A1030 E 08/08/12 16:04/ sdw meq/L A1030 E 08/08/12 16:041 sdw meq/L A1030 E 08/08/12 16:041 sdw mg/L A1030 E 08/08/12 16 :04 1 sdw A1030 E 08/08/12 16:041 sdw ug/L 20 SW8260B 07/24/12 01 :28 1 jk ug/L 1.0 SW8260B 07/24/12 01 :28 1 jk ug/L 1.0 SW8260B 07/24/12 01 :28 1 jk ug/L 1.0 SW8260B 07/24/12 01 :28 1 jk ug/L 1.0 SW8260B 07/24/1201 :28 1 jk ug/L 20 SW8260B 07/24/12 01 :28 1 jk ug/L 1.0 SW8260B 07/24/1201 :28 1 jk ug/L 1.0 SW8260B 07/24/1201 :28 1 jk ug/L 1.0 SW8260B 07/24/1201 :28 1 jk ug/L 1.0 SW8260B 07/24/12 01 :28 1 jk %REC 80-120 SW8260B 07/24/12 01 :28 1 jk %REC 70-130 SW8260B 07/24/12 01 :28 1 jk %REC 80-120 SW8260B 07/24/12 01 :28 1 jk %REC 80-120 SW8260B 07/24/12 01 :28 1 jk MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 21 of 54 American West ANALYTICAL LABORATORIES 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: Semi Annual Ground Water Lab Sample ID: 1208066-001A Client Sample ID: MW-37 _07302012 Collection Date: 7/30/2012 1340h Received Date: 8/312012 Analytical Results Analyzed: 8/6/20128lIh Units: Jlg/L 1100h Dilution Factor: Contact: Jo Ann Tischler VOAs by GC/MS Method 8260CIS030C Method: SW8260C CAS Reporting Analytical Compound Number Limit Result Qual Tetrahydrofuran Surrogate Surr: Toluene-d8 Surr: Dibromofluoromethane Surr: 4-Bromofluorobenzene Surr: 1,2-Dichloroethane-d4 CAS Result 2037-26-5 50.4 1868-53-7 50.2 460-00-4 52.2 17060-07-0 5l.6 109-99-9 1.00 < 1.00 Amount Spiked %REC Limits Qual 50.00 101 77-129 50.00 100 80-124 50.00 104 80-128 50.00 103 72-151 Report Date: 8/14/2012 Page 6 of 17 All analyses applicable to the CW A, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of subsequent use oft~e name of this company or any member of its staff, or reproduction of this report in. c?nnection with the advertisement, pro.motion or sale .of any product or process, orin connection with the re.-publication oft?is report for any INORGANIC ANALYTICAL REPORT American West ANALYTICAL LABORATORIES 463 West 3600 South Client: Denison Mines Project: Semi Annual Ground Water Lab Sample ID: 1208066-001 Client Sample ID: MW-37_07302012 Collection Date: 7/30/2012 1340h Received Date: Analytical Results Compound 8/3/2012 Units 1100h Date Prepared ;alt Lake City, UT 84115 Tin mg/L Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer This sample was not digested pursuant to the client request. Date Analyzed 811312012 1530h Contact: Jo Ann Tischler Method Used E200.8 DISSOLVED METALS Reporting Limit 0.100 Analytical Result < 0.100 Qual Report Date: 8/1412012 Page 5 of 17 All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COe. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in. c?nnection with the advertisement, pro.motion or sale of any product or pro. cess, or in connection with the re.-publication of t!tisreport for any -"AI' EI\ERGY LABORATORIES wWw.ooergylab.~om Aliilytftal ~ Siflcg'1m ·.·.:··~~·';.H~I~'l,a.:'Mr 8':1~41,~ .. pl11 .·aiUingS~fdr800~735~44~9 · Casper, ~'888"235-0515 : ~iU~tt~i1t!&'"liB!:"lfll · .. R~p.id ~JtY,SP.888~'72-1225 . Colleg~ Statio'n, TX .8'8-6~O-i218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C12080143-003 Client Sample 10: MW-37 _07302012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 265 486 51 0.22 133 ND 0.8 15.1 575 2700 4090 ND ND ND ND ND ND ND ND ND ND ND ND 6.6 ND ND ND 12.4 ND 28 2.9 1.2 1.3 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC -Minimum detectable concentration Report Date: 08/24/12 Collection Date: 07/30/12 13:40 Date Received : 08/03/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By D D D A2320 B 08/06/12 16:55 1 jba 1 A2320 B 08/06/12 16:55 1 jba 0.5 E200.7 08/20/12 13:101 sf 4 E300.0 08/08/12 21 :29 1 wc 0.10 A4500-F C 08/06/12 13:301 jba 0.5 E200.7 08/20/12 13:101 sf 0.05 A4500-NH3 G 08/08/12 12:121 Ir 0.1 E353.2 08/06/12 12:53 fir 0.5 E200.7 08/20/12 13:101 sf 2 E200.7 08/20/12 13: 1 0 1 sf 20 E300.0 08/08/12 21 :29 1 wc 10 A2540 C 08/06/12 13:31 1 jz 5.0 E200.8 08/20/12 15:27 1 cp 0.50 E200.8 08/20/12 15 :27 1 cp 0.50 E200.8 08/20/12 15 :27 1 cp 25 E200.8 08/20/12 15:27 1 cp 10 E200.8 08/20/12 15:27 1 cp 10 E200.8 08/20/12 15 :27 1 cp 30 E200.7 08/20/12 13:101 sf 1.0 E200.8 08/20/12 15:27 1 cp 10 E200.8 08/20/12 15:27 1 cp 0.50 E200.8 08/20/12 15:27 1 cp 10 E200.8 08/20/12 15:27 1 cp 20 E200.8 08/20/12 15 :27 1 cp 5.0 E200.8 08/20/12 15 :27 1 cp 10 E200.8 08/20/12 15:27 1 cp 0.50 E200.8 08/20/12 15 :27 1 cp 100 E200.8 08/20/12 15 :27 1 cp 0.30 E200.8 08/20/12 15:27 1 cp 15 E200.8 08/20/12 15:27 1 cp 10 E200.8 08/20/12 15:27 1 cp E900.1 08/08/12 06 :49 1 Ibb E900.1 08/08/12 06:491 Ibb E900.1 08/08/12 06 :49 1 Ibb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 5 of 26 EN:RGY LABORATORIES wWw.energylab.com Analjlitll EmO. Sblcil 1m LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C 12080 143-003 Client Sample 10: MW-37 _07302012 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -1.17 62.0 60.6 4100 1.00 ND ND ND ND ND ND ND ND ND ND 104 102 118 115 Units 0/0 meq/L meq/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifier Rl 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 08/24/12 Collection Date: 07/30/12 13:40 DateReceived: 08/03/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By A1030 E 08/23/1207:341 kbh A1030 E 08123/12 07:341 kbh A1030 E 08123/12 07:341 kbh A1030 E 08/23/12 07:341 kbh A1030 E 08/23/12 07:341 kbh SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/1201 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk SW8260B 08/08/12 01 :46 1 jk MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 6 of 26 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-009A Client Sample ID: MW-65_07112012 Collection Date: 7/11/2012 951h Received Date: 7/12/2012 1345h Analytical Results Analyzed: 7113/20121425h Units: Jlg/L Compound Tetrahydrofuran Dilution Factor: Contact: Jo Ann Tischler VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 Surrogate CAS Result Amount Spiked %REC Limits Qual SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 2037-26-5 1868-53-7 460-00-4 17060-07-0 50.6 56.7 53.3 56.0 50.00 101 77-129 50.00 113 80-124 50.00 107 80-128 50.00 112 72-151 Report Date: 7/23/2012 Page 22 of 41 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of ,f t p f 't ~t' f; po (' po; • (' . t " t .. th' n 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water 2012 Lab Sample ID: 1207185-009 Client Sample ID: MW-65_07112012 Collection Date: 7111/2012 0951h Received Date: 7112/2012 1345h Contact: Jo Ann Tischler Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Tin mg/L 712112012 1839h E200.8 0.100 < 0.100 /\ -Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. This sample was not digested pursuant to the client request. /\ Report Date: 8128/2012 Page 13 of41 All analyses applicable to the CW A, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of (mhcpnl1pnt l1~P n.fthP ,.'HU"nP nf'tl,1<:' ('>{'\rnn;;lt", nr '.l"" mprrtlv.r I'\f;t" d?lff or rpnrt"'l(ln,..tTnn nfthl<:' rpnnrt 1n ('(\nnpr.t;nn with thp ~nvf"rti~f"mpnt nromntinn or s::Ile: of ::Inv nrnnnr.t or nrnr.p.ss or in ~nnnectl()n with the re-nllhlication o· fi V www.energylab.com ( ..,""' ....... ' . 'Helella" MT 877 .. 472-0711 • BiUings,MT 800-735-4489 . Casper, WY 888-235-0515 JltiJ"hL ,:"§ur~~~, WYU6~$86, .. 7115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 EN:RGY LABORATORIES Analytical ExCSUBflCB SiIlCI 1852 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C12070448-011 Client Sample ID: MW-65_07112012 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 390 463 74 0.29 161 0.22 2.1 10.4 201 1730 3130 ND ND ND ND ND ND 793 ND 1200 ND ND ND 5.1 ND ND 30.2 ND ND 2.0 0.3 0.2 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pC ilL pC ilL pC ilL MDC -Minimum detectable concentration Report Date: 08/09/12 Collection Date: 07/11/1209:51 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By D A2320 B 07/13/12 20:01 1 jba 1 A2320 B 07/13/1220:01 1 jba 0.5 E200.7 07/18/12 15:421 sf A4500-CI B 07/19/1215:12/wc 0.10 A4500-F C 07/13/1214:321 jba 0.5 E200.7 07/18/12 15:421 sf 0.05 A4500-NH3 G 07/17/12 13:14 fir 0.1 E353.2 07/16/12 12:151 Ir 0.5 E200.7 07/18/12 15:421 sf 0.5 E200.7 07/18/12 15:421 sf 50 A4500-S04 E 07/20/1213:291 ab 10 A2540 C 07/13/12 15:531 ab 5.0 E200.8 08/01/12 16:471 cp 0.50 E200.8 08/01/1216:471 cp 0.50 E200.8 08/01/1216:471 cp 25 E200.8 08/01/1216:471 cp 10 E200.8 08/01/12 16:471 cp 10 E200.8 08/01/1216:471 cp 30 E200.7 07/18/12 15:421 sf 1.0 E200.8 08/01/1216:471 cp 10 E200.8 08/01/1216:471 cp 0.50 E200.8 08/01/1216:471 cp 10 E200.8 08/01/12 16:471 cp 20 E200.8 08/01/1216:471 cp 5.0 E200.8 08/01/1216:471 cp 10 E200.8 08/01/1216:471 cp 0.50 E200.8 08/01/1216:471 cp 0.30 E200.8 08/01/1216:471 cp 15 E200.8 08/01/1216:471 cp 10 E200.8 08/01/1216:471 cp E900.1 08/09/12 00:07 1 Ibb E900.1 08/09/12 00:07 1 Ibb E900.1 08/09/12 00:07 1 Ibb MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 22 of 54 EI\ERGY LAEIORATORI ES www.energyJab.com Analytical ExtBlllHI&' Sines '852 Hil¢na, MTSn .. 472:..0111 • BUlings.MT 800-735-4489 • Casper, Wf 888 ... 235-0515 j!ill~~g;Wt8~6' .. $8~~1l1~ • Rapid Ctty, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/1209:51 DateReceived: 07/13/12 Matrix: Aqueous Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2012 C12070448-011 Client Sample 10: MW-65_07112012 Analyses OAT A QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.791 44.6 45.3 2800 1.10 MCL! Units Qualifier Rl QCl Method Analysis Date / By % A1030 E 08/08/12 16:04/ sdw meq/l A1030 E 08/08/12 16:04/ sdw meq/l A1030 E 08108/12 16:041 sdw mg/l A1030 E 08/08/12 16:041 sdw A1030 E 08/08/12 16:041 sdw MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 23 of 54 EI\ERGY LABORATORIES ~~~ www.energylab.com ~ Analytit:al ExCSUJflCB $Ince '652 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 «§~II~tt~~.~Y 8&&-686-7175 II Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C 12080830-002 Client Sample 10: MW-65_08162012 Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO 960 NO NO 5.2 NO NO NO 88.0 92.0 86.0 96.0 o -RL increased due to sample matrix. Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 08/30/12 Collection Date: 08/16/1206:40 DateReceived: 08/17/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By 20 SW8260B 08/22/12 20: 141 jk 1.0 SW8260B 08/22/1220:141 jk 1.0 SW8260B 08/22/1220:141 jk 0 25 SW8260B 08/29/12 06:081 jk 1.0 SW8260B 08/22/1220:141 jk 20 SW8260B 08/22/1220:141 jk 1.0 SW8260B 08/22/12 20:141 jk 1.0 SW8260B 08/22/1220:141 jk 1.0 SW8260B 08/22/1220:141 jk 1.0 SW8260B 08/22/1220:141 jk 80-120 SW8260B 08/22/1220:1 41 jk 70-130 SW8260B 08/22/1220:141 jk 80-120 SW8260B 08/22/1220:141 jk 80-120 SW8260B 08/22/1220:141 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 12 EN:RGY LABORATORIES www.energylab.com Analytical ExcsJIBflCI Sines 1952 Helena, MT 877 .. 472-0111 • Billings, MT 800 .. 735-4489 • Casper, WY 888 .. 235-0515 ~iUe.~¢, WY 86&·686~ 7115 • Rapid City, SO 888-672-1225 • College station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Lab 10: Client Sample 10: 3rd Quarter Groundwater 2012 C 12070741-009 MW-70_07182012 Analyses MAJOR IONS Fluoride METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.02 48.6 Units mg/l ug/l Qualifier Rl 0.10 5.0 Report Date: 08/14/12 Collection Date: 07/18/1209:55 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By A4500-F C 07/23/12 12:341 jba E200.8 08/05/12 10:41 1 cp MCl -Maximum contaminant level. ND - Not detected at the reporting limit. Page 11 of 27 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: Lab Sample ID: 3rd Quarter Ground Water 2012 1207185-010A Client Sample ID: Trip Blank Collection Date: 7/9/2012 Received Date: 7112/2012 1345h Analytical Results Analyzed: 7113/20121444h Units: Jlg/L Dilution Factor: Contact: JoAnn Tischler VOAs by GC/MS Method 8260CIS030C Method: SW8260C CAS Reporting Analytical Compound Number Limit Result Qual Tetrahydrofuran Surrogate SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 CAS 2037-26-5 1868-53-7 460-00-4 17060-07-0 Result 51.3 55.4 55.4 56.1 109-99-9 1.00 < 1.00 Amount Spiked %REC Limits Qual 50.00 103 77-129 50.00 111 80-124 50.00 111 80-128 50.00 112 72-151 Report Date: 7/23/2012 Page 23 of 41 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infommtion is located on the attached COCo This report is provided for the exclusive use ofthe addressee. Privileges of • 4 ~ • • ..,.., • _________ ! ___ . ___ ..... : ... _ ~_.; ... t. .l.. ........... -. .. hl~~ .. ..,; ......... "f'tJ..;", ... A ..... "rt .fnT' 'JOn, American West ANALYTICAL LABORATORIES 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines Semi Annual Ground Water 1208066-002A Client Sample ID: Trip Blank Collection Date: 7/30/2012 Received Date: 8/3/2012 1100h Analytical Results Analyzed: 8/6/2012 849h Units: Jlg/L Dilution Factor: Compound Tetrahydrofuran Surrogate SUIT: Toluene-d8 SUIT: Dibromofluoromethane SUIT: 4-Bromofluorobenzene SUIT: 1,2-Dichloroethane-d4 CAS 2037-26-5 1868-53-7 460-00-4 17060-07-0 Result 51.1 50.5 52.9 51.9 Contact: Jo Ann Tischler VOAs by GC/MS Method 8260CIS030C CAS Number 109-99-9 Method: Reporting Limit 1.00 Amount Spiked %REC 50.00 50.00 50.00 50.00 102 101 106 104 SW8260C Analytical Result < 1.00 Limits 77-129 80-124 80-128 72-151 Qual Qual Report Date: 8/14/2012 Page 7 of 17 All analyses applicable to the CW A, SOW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is lQcated on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of <l1h'POll",nt 11.'" ofth" nam" ofthis comnanv or anv member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale .of any product or process, or in connection with the re.-publication oft.his report for any EN:RGY LABORATORIES WWIY.energyJ ab.com AnalYtical ExtBlIsncs SinCi '952 Hel~na, MT 877-412-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 9jU~tte, WY8~6"G8~~111~ • Rapiej City, SI} 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2012 C 12070448-0 12 Client Sample 10: Trip Blank 6706 Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO NO NO NO NO NO NO NO 95.0 B9.0 7B.0 95.0 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 08/09/12 Collection Date: 07/09/12 DateReceived: 07/13/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By 20 SWB260B 07/19/1216:16/jk 1.0 SWB260B 07/19/12 16:161 jk 1.0 SWB260B 07/19/12 16:161 jk 1.0 SWB260B 07/19/12 16:161 jk 1.0 SWB260B 07/19/1216:161 jk 20 SWB260B 07/19/12 16:161 jk 1.0 SWB260B 07/19/12 16:161 jk 1.0 SWB260B 07/19/1216:16/jk 1.0 SWB260B 07/19/12 16:161 jk 1.0 SWB260B 07/19/1216:16/jk BO-120 SWB260B 07/19/1216:16/jk 70-130 SWB260B 07/19/1216:16/jk S BO-120 SWB260B 07/19/1216:16/jk BO-120 SWB260B 07/19/1216:16/jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 24 of 54 EN:RGY LABORATORIES wWw.energylab.com MstytitJ;1 Exci1/JBf1C8 SiilC, '952 ':ffbi~~,~f'@ '~1;1~41~~0711 .BillingstMl800 .. 135~4489 • Caspe,r,WY888 .. 235';0515 ''.l',6lJ8@~:lf1,5 ·~apig,~JtYl '~ll'888~'72~~ 225 -Collegtt Sf~tlDn, IX 888-6.0-~218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 LablD: C12080143-004 Client Sample ID: Trip Blank Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO NO NO NO NO NO NO NO 105 109 119 115 Units ug/l ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifier Rl 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 08/24/12 Collection Date: 07/30/12 DateReceived: 08/03/12 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By SW8260B 08/07/1218:46/jk SW8260B 08/07/1218:46/jk SW8260B 08/07/12 18:461 jk SW8260B 08/07/1218:46/jk SW8260B 08/07/12 18:461 jk SW8260B 08/07/1218:46/jk SW8260B 08/07/1218:461 jk SW8260B 08/07/1218:461 jk SW8260B 08/07/1218:461 jk SW8260B 08/07/1218:461 jk SW8260B 08/07/1218:46/jk SW8260B 08/07/12 18:461 jk SW8260B 08/07/1218:461 jk SW8260B 08/07/1218:461 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 26 PO .",:;<1 .. www.energylab.com ~-H~lena.MTB77-472~071t .Billings.MT 800 .. 135-4489 · Casper, WY 888-235-0515 -~ AnalyticalExCBIiBflCBSince ',!152 1~!~~ll,.·~n'e.~~J'~y,B§'& .. 6B6-71l5.. Rapid City, SD 888-672-1225 • College Statinn, TX 888-690-2218 EI\ERGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C 12080830-003 Client Sample 10: Trip Blank 6706 Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO NO NO NO NO NO NO NO 90.0 93.0 84.0 102 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifier Rl 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 08/30/12 Collection Date: 08/16/12 DateReceived: 08/17/12 Matrix: Aqueous MCL! QCl Method Analysis Date I By SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/1216:45 /jk SW8260B 08/27/1216:451 jk SW8260B 08/27/1216:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/12 16:451 jk SW8260B 08/27/1216:451 jk SW8260B 08/27/12 16:451 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 12 EI'l:RGY LABORATORIES www.energylab.com Analytical ExcsllBflC. Sincs 1952 Helena, MT 817-472-0111 • Billings. MT 800-135-4489 • Casper, WY 888-235-0515 '~jllette, WY866:-QB6~7n5 • Rapid City, S() 888-672-1225 • College Station, 1X 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2012 C12070741-014 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 1.6 Qualifier RL Report Date: 08/14/12 Collection Date: 07/19/12 DateReceived: 07/20/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E170.1 07/20/1209:551 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 16 of 27 E~RGY LABORATORIES Client: Project: LablD: M" www.~ab.com ~\ 0 °K,I,na. MT 817-472..jJ711 • Billings, MT 8011-7354489 • Casper. W'/888-235-8515 ~ AnalyticalExCBUBflCtlSincll 1!152 J; ... ~~~~'~".'§UI~tteJ -Ny :a66~686~7n5 • Rapid Ctty, SD 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Denison Mines USA Corp 3rd Quarter Groundwater 2012 C12070448-013 Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/12/12 DateReceived: 07/13/12 Client Sample ID: Temp Blank Matrix: Aqueous Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.0 MCL! Qualifier RL QCl Method Analysis Date / By E170.1 07/13/12 10:30/ kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 25 of 54 EN:RGY L ABORATORIES witrN:energyJab.com Anatytit,I 4cillsiu$$ItH;. 1952 n a "··st1~41~~o:1.H .BUJlng~tMr'O~-7~5-44B9 ·Casper,W¥ '88-235~0515 =,.~.".~1:17,l·.~~pi~'¢riv;~p:,iQj:'612.J226 · C~lleg~:St«lt!Dn, 1X 8.8~6QO .. 2218, LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C 12080 143-005 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 4.0 Qualifier RL Report Date: 08/24/12 Collection Date: 08/02/12 DateReceived: 08/03/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E170.1 08/03/12 09:501 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 26 J / 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-Iabs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer JoAnn Tischler Denison Mines 1050 17th Street, # 950 Denver, CO 80265 TEL: (303) 389-4132 RE: 3rd Quarter Ground Water 2012 Dear JoAnn Tischler: Lab Set ID: 1207185 American West Analytical Laboratories received 10 sample(s) on 7/12/2012 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Association Conference (NELAC) Institute in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. In addition, A W AL is also accredited by the American Analytical Laboratory Association (A2LA) on ISO IEC 17025:2005, Department of Defense (DOD), UST for the State of Wyoming, and the National Lead Laboratory Accreditation Program (NLLAP). All analyses were performed in accordance to The NELAC Institute andlor A2LA protocols unless noted otherwise. Accreditation documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. This is a revision to a report originally issued 7/23/2012. Pages 1 and 5-13 have been revised. Thank You, Approved by: Ky I e F. Digitally signed by Kyle F. Gross DN: cn=Kyle F. Gross, o=AWAL, " u=AWAL-Laboratory Director, G . email~kyle@awal-Iabs.com. c=US r OS S _~[)~te: 2'0T-l~pJ.28 14:34:27 -06'00' lr Laboratory Director or designee Report Date: 8/28/2012 Page 1 of 41 All analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive lise of the addressee. Privileges of s f 1 t " it ~ r , n t ' . r r r ;n t' t r ._ 1 1 SAMPLE SUMMARY Client: Denison Mines Contact: Jo Ann Tischler ANALYTICAL I.ABORATOR IES Project: 3rd Quarter Ground Water 2012 Lab Set ID: 1207185 Date Received: 711212012 1345h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 463 West 3600 South 1207185-001A MW-11 07112012 7/1112012 1210h Aqueous VOA by GC/MS Method ;alt Lake City, UT 84115 8260C/5030C 1207185-001B MW-11 07112012 7/11/2012 1210h Aqueous ICPMS Metals, Dissolved 1207185-002A MW-14 07112012 7/11/2012 1235h Aqueous VOA by GCIMS Method 8260C/5030C Phone: (801) 263-8686 1207185-002B MW-14 07112012 7/1112012 1235h Aqueous ICPMS Metals, Dissolved Toll Free: (888) 263-8686 1207185-003A MW-25 07102012 7/10/2012 1220h Aqueous VOA by GCIMS Method Fax: (801) 263-8687 8260C/5030C ~-mail: awal@awal-Iabs.com 1207185-003B MW-25 07102012 7/10/2012 1220h Aqueous ICPMS Metals, Dissolved 1207185-004A MW-26 07112012 7/11/2012 951h Aqueous VOA by GCIMS Method 8260C/5030C web: www.awal-Iabs.com 1207185-004B MW-26 07112012 7/1112012 951h Aqueous ICPMS Metals, Dissolved 1207185-005A MW-30 07102012 7/1012012 1100h Aqueous VOA by GCIMS Method 8260C/5030C Kyle F. Gross 1207185-005B MW-30 07102012 7/10/2012 1100h Aqueous ICPMS Metals, Dissolved Laboratory Director 1207185-006A MW-31 07092012 7/9/2012 1335h Aqueous VOA by GCIMS Method 8260C/5030C Jose Rocha 1207185-006B MW-31 07092012 7/9/2012 1335h Aqueous ICPMS Metals, Dissolved 1207185-007A MW-35 07102012 7110/2012 1410h Aqueous VOA by GCIMS Method QA Officer 8260C/5030C 1207185-007B MW-35 07102012 7/10/2012 1410h Aqueous ICPMS Metals, Dissolved 1207185-008A MW-36 07112012 7/11/2012 915h Aqueous VOA by GCIMS Method 8260C/5030C 1207185-008B MW-36 07112012 7/1112012 915h Aqueous ICPMS Metals, Dissolved 1207185-009A MW-65 07112012 7/1112012 951h Aqueous VOA by GCIMS Method 8260C/5030C 1207185-009B MW-65 07112012 7/1112012 951h Aqueous ICPMS Metals, Dissolved 1207185-010A Trip Blank 7/9/2012 Aqueous VOA by GCIMS Method 8260C/5030C Report Date: 7123/2012 Page 2 of 41 All analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of ___ 1. ----.•.•• ____ .C ... l. --------.c ... t...: ________ • _____ ._ ............... t... .... _ .... c :.,.. ,.. ... "'c/: ..... _ ........... _ .... ...In'''.; ............ ++h;ro .. "" ...... " .... ; ......... "' ......... o ..... t11"\ .... ,,'1t1, thpo "lorhrprtfcpt'npnt nT'f'ltTH"\tiAn (,\T' ,,~1,... nf ~n\l n,..,(vhu,t Or T"Irn(",p<:!c;: ()T';n ~()nnp.~tl()n with thf": re-nllhlica.tion of this renort for any 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Denison Mines JoAnn Tischler 3rd Quarter Ground Water 2012 1207185 7/12/2012 7/9, 7/10 & 7/1112012 Intact None Holding Time and Preservation Requirements: The analysis of all samples was performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. The samples were not digested pursuant to the client request. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Corrective Action: None required. Report Date: 7/23/2012 Page 3 of 41 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use ofthe addressee. Pl1vileges of .. Hk .... ",.nn"" ....... HC!'" ..... 4='t1-...o ............... ". nf"t'h;c "''''''''T'I<:)nv ..... r 'In,, n'p,.,., .... u",. ..... f;t" d~ff nr rpnT'n~l1rt;('\n nfth1<! Tf"nnrt -in ('.nnnpr':tinn with thp: anvertis,p.mf:nt nrmTIot.inn or sale of anv nroduct or nrocess. or in connection 'with the re-nublication of this report for any Volatile Case Narrative American West Client: ANALYTICAL LABORATORI ES Denison Mines JoAnn Tischler 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-rnail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Contact: Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 3rd Quarter Ground Water 2012 1207185 7112/2012 7/9, 7/10 & 7/1112012 Intact None SW -846 8260C/5030C Tetrahydrofuran General Set Comments: Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 7/23/2012 Page 4 of 41 All analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located 011 the attached COe. This report is provided for the exclusive use of the addressee. Privileges of .. ~.1.. ....................... H ............ .&:'+'k .................................. k; ...... " ......... ,., ...... ' ............... H ........ on-o'h""'''" ",f';t" ... t.,f'f' ",. f"pnT'I'V~l1rtll"\n "ftht<:' rp"nrt in ('{\nnpr.f;nn w;th thp. ~rlvp:rtispm~nt-nrnmotion or sale of anv nroduct or orocess. or in connection with the re-publication oftbis re ort for an Client: Denison Mines Lab Set ID: 1207185 Project: 3rd Quarter Ground Water 2012 Sample ID Analyte LCS VOC 071312 Tetrahydrofuran LCS VOC 071312 Surr: 1,2-Dichloroethane-d4 LCS VOC 071312 Surr: 4-Bromofluorobenzene LCS VOC 071312 Surr: Dibromofluoromethane LCS VOC 071312 Surr: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _Q_C ___ SlIM_MARX __ RE~Ql~~I __ Contact: Jo Ann Tischler Dept: MSVOA QC Type: LCS Amount Original Units Method Result Spiked Amount %REC Limits IlglL SW8260C 17.8 20.00 0 88.8 43-146 %REC SW8260C 55.2 50.00 110 76-138 %REC SW8260C 50.1 50.00 100 77-121 %REC SW8260C 55.0 50.00 110 67-128 %REC SW8260C 49.4 50.00 98.9 81-135 %RPD RPD Limit Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 7/13/2012 725h 7/13/2012 725h 7/13/2012 725h 7/13/2012 725h 7/1312012 725h Report Date: 7/23/2012 Page 24 of 41 nalyses applicable to the CWA, SDW A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any ber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility American West ANALYT !CAL LABORATOR I ES Client: Denison Mines Lab Set ID: 1207185 Project: 3rd Quarter Ground Water 2012 Sample ID Analyte MB VOC 071312A Tetrahydrofuran MB VOC 071312A Surr: 1,2-Dichloroethane-d4 MB VOC 071312A Surr: 4-Bromofluorobenzene MB VOC 071312A Surr: Dibromofluoromethane MB VOC 071312A Surr: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263 -8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com ~c SUMMARY REPOR.T Contact: Jo Ann Tischler Dept: MSVOA QC Type: MBLK Amount Original Units Method Result Spiked Amount %REC Limits IlglL SW8260C < 1.00 %REC SW8260C 54.8 50.00 110 76-138 %REC SW8260C 54.6 50.00 109 77-121 %REC SW8260C 54.6 50.00 109 67-128 %REC SW8260C 51.0 50.00 102 81-135 %RPD RPD Limit Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 7/13/2012 803h 7/13/2012 803h 7/13/2012 803h 7113/2012 803h 7/13/2012 803h Report Date: 7/23/2012 Page 25 of 41 analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any nber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility Client: Denison Mines Lab Set ID: 1207185 Project: 3rd Quarter Ground Water 2012 Sample ID Analyte 1207185-001AMS Tetrahydrofuran 1207185-001AMS Surr: 1,2-Dichloroethane-d4 1207185-001AMS Surr: 4-Bromofluorobenzene 1207185-001AMS Surr: Dibromofluoromethane 1207185-001AMS Surr: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com _Q~ ___ SJ1MMARY_REP.Q_R_I __ _ Contact: Jo Ann Tischler Dept: MSVOA QC Type: MS Amount Original Units Method Result Spiked Amount %REC Limits IlglL SW8260C 19.3 20.00 0 96.3 43-146 %REC SW8260C 55.9 50.00 112 72-151 %REC SW82.60C 51.3 50.00 103 80-128 %REC SW8260C 54.7 50.00 109 80-124 %REC SW8260C 49.6 50.00 99.3 77-129 %RPD RPD Limit Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 7113/2012 957h 7/13/2012 957h 7/13/2012 957h 7/13/2012 957h 7/13/2012 957h Report Date: 7/23/2012 Page 26 of 41 nalyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any ber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility American West ANALYT !CAL LABORATOR !ES Client: Denison Mines Lab Set ID: 1207185 Project: 3rd Quarter Ground Water 2012 Sample ID Analyte 1207185-001AMSD Tetrahydrofuran 1207185-001AMSD SUIT: 1,2-Dichloroethane-d4 1207185-001AMSD SUIT: 4-Bromofluorobenzene 1207185-001AMSD SUIT: Dibromofluoromethane 1207185-001 AMSD SUIT: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com _Q~BUMMARYREPQ_&_L Contact: Jo Ann Tischler Dept: MSVOA QC Type: MSD Amount Original Units Method Result Spiked Amount %REC Limits ~glL SW8260C 17.0 20.00 0 85.0 43-146 %REC SW8260C 55.1 50.00 110 72-151 %REC SW8260C 50.4 50.00 101 80-128 %REC SW8260C 54.1 50.00 108 80-124 %REC SW8260C 49.2 50.00 98.4 77-129 %RPD 12.5 RPD Limit 25 Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 7/13/2012 1017h 7/13/2012 1017h 7/13/2012 1017h 7/13/2012 1017h 7/13/2012 1017h Report Date: 7/23/2012 Page 27 of 41 analyses applicable to the CWA, SDW A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any .ber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J72L1851.D 13 Jul 2012 8:41 am 1207185-001A SAMP 5.0ML SB 7 Sample Multiplier: 1 Quant Time: Jul 13 08:54:32 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance 15000001 TIC: J72L 1851.0\data.ms 1450000j 1400000j i 13500001 13000001 I 1250000j i 1200000j ~ I ~ j ~ 11500001 D 110000011 1 1050000, I 10000001 I I 9500001 j I 9000001 ~ Iii! 8500001 (J) ai c: ~ c: Ql ..c e o 1 i 8000001 ,II III 1 II 750000j ~ I I! il 7000001 II II 6500001 I I 600000 j ~ (J) II II 550000',1 1 ~ ! I II I I I 500000 ~ ~ II I 1 ~ II ::::::1 i ~ I 350000j I I 3000001 I II I , 250000 i 1\ I II il 20oo00! 11:1 II III I II I I I 1500001 II 1111 : il I 100000j [I I II II I I ,I /1 I 'I'! I 500001 1 ' i; I'l'll II 1'\ 1\ "l I! I! I II o f-~~T 1\; 1-"-' -r-; -:; -r-:r{r::-:;:.:;--Fj'-;= =r'T"TT""T,-J 1 \'"""~ 1-; l--, -'",' ',-'-~'rL+-r-r",.,J+T"""rT_L~~r--;--f ~"""F",-'-11 Y"l"T"r~-Y'j ",[OfT f-FT;=T---~·-TT=;--r=-'-='T,.o.--=1' T'" T L50 2.90 2.5J> 3.00 3~§..Q 4:QO _,t~O 5.QO .~.§O 6.00 §.qO 7.00 . 7:50 !3.00 Jt50 9.00 . ~.50 tQ.O~_ 19.50 11.0.0 11.50 AFULLW_59.M Fri Jul 13 08:55:03 2012 Report Date: 7 /23/2<f1~gEPagdQ8 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J81L1852.D 13 Jul 2012 11:33 am 1207185-002A SAMP 5.0ML SB 16 Sample Multiplier: 1 Jul 13 13:08:10 2012 C:\MSDCHEM\1\METHODS\AFULLW_59.M VOA Calibration Wed Jun 27 10:22:19 2012 Initial Calibration (QT Reviewed) Abundance ----------TIC: J81 L 1852.D\data.ms 15000001 1450000j I 1400000j 13500001 1300000J i 12500001 12000001 1 1150000j I 1100000 1 10500001 1 I 10000001 9500001 I 900000j 8500001 8000001 7500001 I 700000j I 650000j 600000j 550000. i a; 5000001 ! 4500001 ~ 1 D ~ 4000001 ~ "'. 350000, ~ I ~ I 1,'l i I I I; 3000001, I I II I 250000J 1 , , III" II ',',I I i i\ !!I I I ! Ii I, il 2000001 r Ii I' Ii I I I II ':! 100000i I i!i I i,i, • 1500001 I II 1,1) I i",ll J' I II II I i Ii i i II II I q 5000:~~~rTr;Tr;=;'TTcCC;T~C JA~,~, ~~U,~' L'T~ ~r~TTTTT'T~T']~M Time--> 1 :?O __ ~.OO 2.50 3.99 ~._?9 _ 4.90 4~50 ~OO _ §.§Q 6.00 6:50 7 ~Q 1.50 8~00 8:?Q 9.00 ___ ~_.§Q _ 1,0.0_0 10·?9 11·Q9_ 1 U?Q AFULLW_59.M Fri Jul 13 13:08:37 2012 Report Date: 7 /23/2@1(~gEPagd29 of 41 I .1 I Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J84L1853.D 13 Jul 2012 12:30 pm 1207185-003A SAMP 5.0ML SB 19 Sample Multiplier: 1 Jul 13 13:11:01 2012 C:\MSDCHEM\1\METHODS\AFULLW_59.M VOA Calibration Wed Jun 27 10:22:19 2012 Initial Calibration (QT Reviewed) Abundance . 14500001 TIC: J84L1853.D\data.ms 1400000J 1350000 13000001 I 12500001 1200000j 11500001 I 11000001 10500001 1000000j 9500001 I 9000001 I 8500001 8000001 750000 AFULLW_59 .M Fri Jul 13 13:11:28 2012 f (I) :0 ~ d: :::l co I I I I ;;j "% c: CI> ~ CI> ..t .c ~ en "9 0 :g (I) :E c: (I) 0 (I) ~ N Cl c: (I) f0-CI> .c .c !Q ~ ~ 0 0 :::l :E 15 CJ ~ i5 i ~ :0 en Report Date: 7 /23/2@'1~gEl>agdBO of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via Abundance . 1.ae+07j I 1 1.7e+071 I 1.Se+07j I 1.se+07j I 1.4e+071 1.3e+07 I 1.2e+07j I 1.1e+071 I 1e+071 9000000 aoooooo I 7000000 SOOOOOO 50000001 I 4000000 3000000 1 2000000 1000000 Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J85L1854.D 13 Jul 2012 12:49 pm 1207185-004A SAMP 5.0ML SB 20 Sample Multiplier: 1 Jul 13 13:16:09 2012 C:\MSDCHEM\1\METHODS\AFULLW_59.M VOA Calibration Wed Jun 27 10:22:19 2012 Initial Calibration Q) "C .~ :E t) Q) s:: Q) ~ Q) :::!! oh-,-, -, -I 'r" iii I ' , i 'l""" , 1 ' Tin:!e--> 1.50 2.QQ ~~9 ;3.00 3:§0 AFULLW_59.M Fri Jul 13 13:16:35 2012 (QT Reviewed) Report Date: 7/23/2@1QgEPagdBl of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J86L1855.D 13 Jul 2012 1:08 pm 1207185-005A SAMP 5.0ML SB 21 Sample Multiplier: 1 Quant Time: Jul 13 13:22:53 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance TIC: J86L 1855.D\data.ms . i 1500000j 14500001 1400000j 13500001 i 1300000j I 12500001 i 12000001 I 1150000j 11000001 10500001 I 10000001 9500001 I 9000001 850000j 800000 j I 750000 j I 7000001 650000 550000 AFULLW_59.M Fri Jul 13 13:23:31 2012 Lli '9 ~ CD N <:: CD .Q E 0 :2 (,) 0 I-~ en cD <:: CD N <:: ~ CD .Q '9 e CD 0 <:: ::l CD 15 ~ E CD e .Q e m 0 !5 :2 0 en a ..1-. 0 I-~ Report Date: 7/23/201i2gEPkgdB2 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J87L1856.D 13 Jul 2012 1:27 pm 1207185-006A SAMP 5.0ML SB 22 Sample Multiplier: 1 Quant Time: Jul 16 07:09:38 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance 1450000j i 14000001 TIC: J87l1856.D\data.ms I 13500001 13000001 i 12500001 I ! 1200000 1 1 11500001 ! 11000001 I 1050000j 1 1000000 j I 950000 1 I 900000l I 850000j I 8000001 I 750000j 7000001 ! 6500001 I 600000i ~ Ii en C;!I t -I 550000 1 ~ ~ I: 5000001 1 I I 4500001 ] ~ I 400000j ~ ~ II ! f Ii f I I I I II iI ,I !I II II II I' II II I' II en 0) c CD N C CD ..c e o , I en II 350000 i j II ;; 300000 1 ~ II I Ii I I II II!I 250000i ': Ii II Ii j I Ii 'I II II I I II II II 200000i 11 11 I:,i.,1 ii' ,i,i", i I I I: I Ii 150000j I II il I II Ii ! I II II I II :1 l:::::L~~~-n~~T~lJ~LJLJl"'-'l ,-r.JUL~~Y~'''C~~'T~TrTT"Fprj''F' J ~5Q _2.00 .2.50 3.09 ~~§O 4.00 4~~Q ~OO 5.5Q 6.00 §"c-50 . TOg 7~~Q 8.00 8~59 _~~J)Q _~.~.o to.Q.Q 10 . .50 1 L Q..o. 1 L.50 AFULLW_59.M Mon Jul 16 07:10:13 2012 Report Date: 7/23/201ClgEPag~3 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J88L1857.D 13 Jul 2012 1:46 pm 1207185-007A SAMP 5 .0ML SB 23 Sample Multiplier: 1 Jul 16 07:10:42 2012 C:\MSDCHEM\1\METHODS\AFULLW_59.M VOA Calibration Wed Jun 27 10:22:19 2012 Initial Calibration (QT Reviewed) Abundance . I TIC: J88L 1857.D\data.ms 1 1350000 j i 13000001 I 12500001 1200000 1 I 1150000, I 11000001 10500001 I 10000001 I 9500001 I 900000 1 850000 j i 800000 j 750000 i I 700000 1 6500001 I AFULLW_59.M Mon Jul 16 07:11:04 2012 '" "'C cD c: ~ ~ c: 1 Q) ..GJ It: CD j as ~ i * :p I ~ .,f ~ c: I1:l c: Q) .Ll E ~ en (.) :g c Q) ..t_ ~ 0 Q) ~ .1:l E 0 :::> "6 E E aJ :; en I Report Date: 7/23/2@1QgEPage434 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J89L1858.D 13 Jul 2012 2:06 pm 1207185-008A SAMP 5.0ML SB 24 Sample Multiplier: 1 Quant Time: Jul 16 07:11:32 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance 14000001 TIC: J89L 1858.D\data.ms 1350000j 13000001 12500001 12000001 11500001 I 11000001 I 10500001 10000001 950000 9000001 ! 8500001 1 800000j ! 7500001 7000001 I 6500001 I cD c: ~ c: CD .l:l e o ::I iI o ~ 600000j I I il 550000 j ~ ~ II I ffi ~ II 500000 1 ~ 2l II 450000 11 i ~ Iii e ~ I 4000001 ~ ~ II ~ 1 It: CI) ~ 't :0 (/) Lri cD "C c: ..f CD cD N ~ c: c: CD CD ~ .l:l e ~ 1l 0 ~ ::I CD 'i5 .l:l e E .2 e .<: al 0 ::I i (/) 350000 j II I 3000001 I II I II I ~ I II Ii I 2500001 .11 II' III Ii I' I II I Iii II 200000j ,II "II' I I! : I :1 I I ,I 1500001 Ii I II I II I i 11 II I II I 100000j II I II I i II II I II Ii II II!I ; 5000:~4'rrrr"~ri","T~'rF,_~lJUL~~L~Trr~Ff"~~~'1~ Tlllle--> 1.:59 _ ?OO ?5Q .~t90 _ ~·§9 .. ~~.oO _.1:~Q . 5.QO§.~9 6.00 !L~O . ~.OO ?5Q 8.:00 . .?.!..50 ~.OO 9~§.0 _ 10.Q9_19.5Q 11.9~t t1.50 AFULLW_59.M Mon Jul 16 07:11:53 2012 Report Date: 7123/2<f1i2gEPagd6S of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J90L1859.D 13 Jul 2012 2:25 pm 1207185-009A SAMP 5.0ML SB 25 Sample Multiplier: 1 Quant Time: Jul 16 07:12:46 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance TIC: J90L1859.D\data.ms 1 1.ge+07i I 1.8e+071 1.7e+07! I 1.6e+07i i 1.5e+07j i 1.4e+07j I 1.3e+07j I 1.2e+071 1.1e+07j I 1e+07j I 9000000j I 8000000j I 7000000 j 6000000 I i 50000001 I w i ~ ~ 40000001 w ~ ~ i a> '" ~ Q) I ~ ~i ~ ~ 1 30000001 ~ ~ ~ ~ ~ '5 I e Q)~ ~ ~ E 1 ~ g ~~ 0 ~ 2000000j ~ 1 ~ ~ a3 ~ ~ ~ 100000:L"""" '~--"--'i --'.--"--';--'--TPTJl;. ,~~c~.J'Tm.L .~ml., ... " ""', .. ' .,. """',. , Time--> 1 ~5Q g~99 g~~Q 3 .. QQ. ~:..~Q . ~.OQ 1:~Q _ 5.00 .§.50 6~QQ 6.50 Z:09 Z.~Q 8.00 8:.5Q ~.QQ ___ ~.§Q 10.00 1 O.~Q 1J ·9Q. 1.L?9 AFULLW_59.M Mon Jul 16 07:13:11 2012 Report Date: 7/23/20'lclgEPkgdB6 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J91L8510.D 13 Jul 2012 2:44 pm 1207185-010A SAMP 5.0ML SB 26 Sample Multiplier: 1 Quant Time: Jul 16 07:13:41 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance TIC: J91 L8510.D\data.ms 1400000j I i 13500001 I 13000001 I 12500001 1 1200000j I 11500001 I 1100000j I I 1050000j 10000001 I 9500001 900000j I 850000j I 8000001 I 750000j 1 7000001 I 650000j ! I II I II 600000~ II I ~ wi 5500001 I g I 5000001 ) i III I g ~ I 450000 j ~ ~ II 4000001 ~ i ! 3500001 I ~ I I II 300000~ I I 1'1 I I, I ~ II I II 2500001 ·11 II i 1'\ i II I I I 2000001 I! /1 I ' Ii I I ~II 1\ I II 150000j ~ II II II II I I ~ II II ,I I II II 1000001 0 II II 1\ I II II 5000:~+~~T'=r~LuLLJUUl~'TR'~T'W~TrTT~ Ti!!1e--> 1:§Q . 2.0Q ~.5Q 3.0Q ].§_Q 4.0Q .4.§.Q 5:Q9 _ 5J>_9 ._ ~:..O_Q . §.:50 _ 7 :.QQ 7~§Q 8.09 '?:.~9 9.0Q ... ~.~ 1 0:Q9 _ 19·§.Q 11 J>Q. 11.50 AFULLW_59.M Mon Jul 16 07:14:02 2012 Report Date: 7/23/201ClgEPkgdB7 of 41 Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J68LCS20.D 13 Jul 2012 7:25 am LCS VOC 071312A (QT Reviewed) Data Path Data File Aeq On Operator Sample Mise LCS SEE COVERSHEET FOR ID AND AMOUNT JO ALS Vial 3 Sample Multiplier: 1 Quant Time: Jul 13 07:37 :18 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10 :22:19 2012 Response via Initial Calibration Abundance 25 2400000 2100000 2000000 : 18000001 ! 1700000; 1600000: 1500000 i 1400000! 1 1300000' 1200000: 1100000! 1000000: 9000001 I 800000: I 700000' I I 600000i 5000001 400000: I 300000: I 200000' I 100000: Ii AFULLW_59 .M Fri Jul 13 11:52:55 2012 TIC: J68LCS20.D\data.ms en I I Report Date: 7/23/2<f'li2gEPagd68 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via Abundance . I 15000001 I 1450000 ' 1400000 13500001 I 1300000 j 12500001 I 12000001 i 1150000 j I 1100000 1 10500001 I 1000000 1 I 950000 1 900000 j I 850000 1 8000001 i ! 750000 j ! 700000 J 650000 i 1 j 600000 l 5500001 500000i 4500001 400000 i I 350000j I 300000j ! 250000 i I 200000 j 150000i ! 100000j Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J70LMBLK.D 13 Jul 2012 8:03 am MB VOC MBLK 071312A 5.0ML JO 5 Sample Multiplier: 1 Jul 13 08:21:12 2012 C:\MSDCHEM\1\METHODS\AFULLW_59.M VOA Calibration Wed Jun 27 10:22:19 2012 Initial Calibration (QT Reviewed) TIC: J70LMBLK.D\data.ms ::::> en Ii !I I ~ cD c: CD N c: CD .Q E g iI 0 I-!!2 11 ; II ' !i rr.. a) 1 I t :c r \ en cD iii c: ..fC CD "0 N "9 cb c: CD CD c: .Q c: CD E CD N ~ c: 0 (I) ::::> CD .Q '5 .Q E E E .Q 0 .s:: E :E (.) III CJ 0 :s is I-..t. !!2 en 0 ~ 500001 Ii 11 Ii Ii iI II it o f:~::::-T':::;::f~~~T··:;::::l--=':-:::T::::;=;::,:r=-T'-'-::;:::"'=i·=T=r=r'T·T"'"f-""'-c-.~, ,J,l~T)IJ~-,p~"_'~TL~, ~, ~I .--~'~~r~,L~t""!""""";''T'T''''''-'f''''i~ri'~l=T=F·Ti~'T=F='=TT"="='T'r=r';=r"!'''r='Y'l'''T-T''i'''T''f''T [j'!l"e..::~;::.. J ~5Q .?-!QQ ,?§Q 3.QQ.~~§Q .4~QQ 1~!m _ ,§.Q.o .§~§'9 ,,§~Q9 , §:.?Q._ . Z:.QQ . ?§.Q ,~.-QO " ,~3,.5Q . ,~&Q . ~~§.9 1 Q~9_0"JQ.§'Q. JJ_.,QQ Jt.!5.Q_ AFULLW_59.M Fri Jul 13 08:21:38 2012 Report Date: 7/23/201clgEPage4W of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J76S1851.D 13 Jul 2012 9:57 am 1207185-001AMS MS 5.0ML 20F3 SB 11 Sample Multiplier: 1 Jul 13 10:09:56 2012 C:\MSDCHEM\1\METHODS\AFULLW_59.M VOA Calibration Wed Jun 27 10:22:19 2012 Initial Calibration (QT Reviewed) Abundance TIC: J76S1851.D\data.ms . I 1700000 j I I 1600000 1 15000001 I 14000001 I j AFULLW_59.M Fri Jul 13 12:52:49 2012 ai c ~ c ~ o ::;, Ii: u) "9 Q) c ~ c Q) .0 E o ::2 (,) o 1 i H Ii " I! Ii ! Ci: I ~ II II I IQ) ,e:: I ~ I e. 1c/5 IE Report Date: 7 /23/2<fJc~gEPage41.0 of 41 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL12-C\13JUL12\ J77D1851.D 13 Jul 2012 10:17 am 1207185-001AMSD MSD 5.0ML 30F3 SB 12 Sample Multiplier: 1 Quant Time: Jul 13 10:28:58 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_59.M Quant Title VOA Calibration QLast Update Wed Jun 27 10:22:19 2012 Response via Initial Calibration (QT Reviewed) Abundance 1800000 j TIC: J77D1851.D\data.ms I 17000001 i 1600000! 15000001 14000001 13000001 1200000! I 1100000 j I 10000001 i 900000 i 800000i i I 700000j I 600000j I i ! 5000001 1 I 4000001 3000001 I 200000i AFULLW_59.M Fri Jul 13 12:53:43 2012 u) "0 cb c: !!l c: Q) U) ~ cO e 0 ~ ~ Q) :::J ~ ~ :; 1 en ~ ..f' "9 Q) c: Q) en ~ Q) ai .J:l c: 0 Ii i C .JI) I a i I ~ ! Ci) Report Date: 7 /23/2@1~gEPage4\.1 of 41 American West Analytical Laboratories WORK ORDER Summary Client: Client ID: Denison Mines DENIOO Contact: JoAnn Tischler UL Denison Work Order: 1207185 Page 1 of 1 7/13/2012 Project: 3rd Quarter Ground Water 2012 QC Level: LEVEL III WO Type: Project Comments: PA Rush .. QC 3 & Summary. EDD-EIM into Locus Database. Report THF to 1 /lgIL. Samples were field filtered.; . e4Q, Sample ID Client Sample ID Collected Date 120718S-001A ~VV-ll_07112012 7/11/20121210h 120718S-00lB SEL Analytes: S~ 120718S-002A ~VV-14_07112012 7/1112012 1235h 1207185-002B SEL Analytes: SN 120718S-003A ~VV-2S_07102012 7110/20121220h 120718S-003B ~.EI.J Analytes: SN 1207185-004A ~VV-26_07112012 7/11120120951h 120718S-004B Received Date Date Due 7112/20121345h 7/23/2012 Matrix Aqueous Test Code 8260-VV 200.8-DIS 8260-VV 200.8-DIS 8260-W 200.S-DIS Sel Storage ~ VOCFridge ~ MET ~ VOCFridge ~ MET ~ -'VOCFridge ----~ MET 8260-VV ~ VOCFridge ----------------------200.8-DIS ~ MET .. SE!:_Analytes: SN .. ----------------------------.. _._---==:-~ 120718S-00SA ~VV-30_07102012 7/10/20121100h 8260-VV VOCFridge 120718S-00SB 200.8-DIS ~ MET SEL An~!ytes: SN 1207185-006A ~VV-31_07092012 7/9/20121335h 8260-VV ~ VOCFridge 1207185-006B ---------_._----= 200.8-DIS ~ MET SEL ~nalytes: SN 1207185-007A ~VV-35_07102012 7110/2012141011 8260-VV ~ VOCFridge --.. ---_ .. _- 120718S-007B 200.8-DIS MET SEL Allalytes: SN ... 1207185-008A ~-36_07112012 7/11120120915h 8260-VV ~ VOCFridge 1207185-008B 200.8-DIS ~ MET SEL Analytes: SN 120718S-009A ~W-6S_07112012 7/1112012095111 8260-VV ~ VOCFridge 1207 I 85-009B 200.8-DIS ~ MET .. _-SEL Analytes_~ .. ~.N -------_ .. ------. -1207185-01OA Trip Blank 7/9/2012 8260-VV ~ VOCFridge FOR LABORATORY USE ONLY [fill out on page 1]: %M!:V RT ~ CN tV TAT IV' QC V HOK~ HOK __ _ HOK __ 3 3 3 3 3 3 3 3 3 2 GC-~ , fLo, l <oS- TN, -s~lctrd \·0 vev 'Pygecf-A-c VI2(J2 OENISOJ)~ Sheet 1 of 1 MINES CHAIN OF CUSTODY Samples Shipped to: American West Analytical Lab 463 West 3600 South Contact: Garrin Palmer or David Turk Ph: 4356782221 Salt Lake City, Ut 84115 gpalmer@denisonmines.com dturk@denisonmines.com tholliday@denisonmines.com Chain of Custody/Sampling Analysis Request p . rOJect S amp ers N arne 5 amp ers S' Ignature 3rd Quarter Ground -::)IUWJ(., }/.l~~ 1 Water 2012 Tanner Holliday Date Time Sample 10 Collected Collected Laboratory Analysis Requested -MW .. 11 07112012 7/11/2012 1210 THF, TIN 'MW--14 07112012 7/11/2012 1235 THF, TIN . MW-25 07102012 7/10/2012 1220 THF, TIN MW-26 07112012 7/11/2012 951 THF, TIN MW-30 07102012 7/10/2012 1100 THF, TIN MW-31 07092012 7/9/2012 1335 THF, TIN MW-35 07102012 7/10/2012 1410 THF, TIN . MW-36 07112012 7/11/2012 915 THF, TIN MW-65 07112012 7/11/2012 951 THF, TIN Trip Blank 7/912012 III Please notify Garrin Palmer or Tanner HOII~Y'~dReciePt,~ae on these sample~ Immediately! Thank you. StAYnN_Q~ w·eYQ e.A\I , +\' ... ..A-e-' '/1'6/12-, Relinquished By':(~ignature) .'''''''' /,<,:,~ v~.:· {_<::l -~ .. C-:: "'v I //V Relinquished By:(Signature) Date/Time 1/n../J1: . \J.f~ Date/Time Lab Set ID: \2 ... Q:] \ l2>S Samples Were: COC Tape Was: Container Type: No. Ree. o Shipped By: Present on Outer p~ge -Q A W AL Supplied Plastic ~and Delivered DYes 0 No /A o ~L Supplied Clear Glass o AJJ.lbient Unbroken on Outer ~age o A WA~lied Amber Glass rn-thilled DYes 0 No /A o A WAL SUPPI::CITOX Vials Temperature \. '0 °C ", Present on sa~ o Amber 0 Clear 0 Heer ace DNo Headspace Rec. Broken/Leaking DYes ~o ON/A DYes 0 No /A o Non A WAL Supplied Con~ Notes: Unbroken on sa~ Notes: ~Ae..1/11 / DYes DNo /A Properly Preserved 1UIYes ONo ON/A Notes: Notes: / Rec. Within Hold Notes: Bottle Type Ammonia COD Cyanide Metals N02 &N03 Nutrients O&G Phenols Sulfide TKN TOC TP04 TPH Procedure: 1 ) 2) 3) 4) 5) 6) 7) &Yes DNo Discrepancies Between Labels and COC Preservative All pHs OK '-(X::)t -oOL pH <2 H2S04 pH <2 H2SO4 PH >12 NaOH pH <2 HN03 I"O:C; l~oS; pH <2 H2SO4 I I pH <2 H2SO4 pH <2HCL pH <2 H2SO4 pH> 9NaOH, ZnAC pH <2 H2SO4 pH <2 H3P04 pH <2 H2SO4 pH <2HCL Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid Notes: -CO~ --00+ -oos -OCXc> -oC~1 ,10& \19£ \/0;:; I\J-o£ \/0£ t v V I 7 If sample is not preserved properly list its extension and receiving pH in the appropriate column above Flag eoe and notify client for further instructions Place client conversation on coe Samples may be adjusted at client request -005 ~ I \IPS:' Ive&. , I DYes ~ /2. JoAnn Tischler Denison Mines 1050 17th Street, # 950 American West Denver, CO 80265 ANALYTI CAL LAB ORATORI ES 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer TEL: (303) 389-4132 RE: Semi Annual Ground Water Dear JoAnn Tischler: Lab Set ID: 1208066 American West Analytical Laboratories received 2 sample(s) on 8/3/2012 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Association Conference (NELAC) Institute in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. In addition, A W AL is also accredited by the American Analytical Laboratory Association (A2LA) on ISO IEC 17025:2005, Department of Defense (DOD), UST for the State of Wyoming, and the National Lead Laboratory Accreditation Program (NLLAP). All analyses were performed in accordance to The NELAC Institute and/or A2LA protocols unless noted otherwise. Accreditation documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: J'1 Ky I e F. Digitally signed by Kyle F. Gross DN: cn=Kyle F. Gross, o=AWAL, 0l;l=AWAL-Laboratory Director, G emaiJ=kyJe@awaJ-Jabs.com, c=US r OS S' Date: 2012.d~ 1414:22:01 -06'00' Laboratory Director or designee Report Date: 8/1412012 Page 1 of 17 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of subsequent useoft~e name of this comp'any or any member of its staff:: or reproduction of this report in. c?nnection v:ith the adverti~ement, pro.motion or saleof any product or process, orin connection with the re:publication of this report forany SAMPLE SUMMARY American West ANALYTICAL LABORATORIES 463 West 3600 South Client: Project: Lab Set ID: Denison Mines Semi Annual Ground Water 1208066 Date Received: 8/3/2012 1100h Lab Sample ID Client Sample ID 1208066-001A MW-37 07302012 ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer 1208066-001B MW-37 07302012 1208066-002A Trip Blank Contact: Jo Ann Tischler Date Collected Matrix Analysis 7/30/2012 1340h Aqueous VOA by GC/MS Method 8260C/5030C 7130/2012 1340h Aqueous ICPMS Metals, Dissolved 7/30/2012 Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 8/14/2012 Page 2 of 17 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COe. This report is provided for the exclusive use of the addressee. Privileges of subsequent use. oft~e name of this company or any member of its staff, or reproduction of this report in. connection with the advertisement, promotion or sale .of any product or pro?ess, or in connection with the re.-publication ofthisreport for any 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ;:-mail: awal@awal-Iabs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Denison Mines JoAnn Tischler Semi Annual Ground Water 1208066 8/03/2012 7/30/2012 Intact None Holding Time and Preservation Requirements: The analysis of all samples was performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. The samples were not digested pursuant to the client request. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Corrective Action: None required. Report Date: 8114/2012 Page 3 of 17 All analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COe. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in. connection \\lith the advertisement, pro.motion or sale .of any product or pro.cess, orin connection with the re.-publication of t?is report for any Volatile Case Narrative American West Client: ANALYTICAL LABORATORIES Denison Mines JoAnn Tischler 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ;:-mail: awal@awal-labs.com web: www.awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Contact: Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: Semi Annual Ground Water 1208066 8/03/2012 7/30/2012 Intact None SW -846 8260CIS030C Tetrahydrofuran General Set Comments: Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 8/1412012 Page 4 of 17 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in. c?nnection with the adverti~ement, promotion or sale.of any product or pro~ess, or in connection with the re:publication of t~isreport for any American West ANALYTICAL LABORATORIES Client: Denison Mines Lab Set ID: 1208066 Project: Semi Annual Ground Water Sample ID Analyte LCS VOC 08061 Tetrahydrofuran LCS VOC 08061 SUIT: 1,2-Dichloroethane-d4 LCS VOC 08061 SUIT: 4-Bromofluorobenzene LCS VOC 08061 SUIT: Dibromofluoromethane LCS VOC 08061 SUIT: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com _ .. QC SUM_MARY_RE_PQBI_ Contact: Jo Ann Tischler Dept: MSVOA QC Type: LCS Amount Original Units Method Result Spiked Amount %REC Limits IlglL SW8260C 16.0 20.00 0 80.2 43-146 %REC SW8260C 50.8 50.00 102 76-138 %REC SW8260C 49.3 50.00 98.5 77-121 %REC SW8260C 50.3 50.00 101 67-128 %REC SW8260C 49.9 50.00 99.8 81-135 %RPD RPD Limit Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 8/6/2012 714h 8/6/2012 714h 8/6/2012 714h 8/6/2012 714h 8/6/2012 714h Report Date: 8/14/2012 Page 8 of17 I analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility American West ANALYTI CAL LABORATORIES Client: Denison Mines Lab Set ID: 1208066 Project: Semi Annual Ground Water Sample ID Analyte MB VOC 08061 Tetrahydrofuran MB VOC 08061 SUIT: 1 ,2-Dichloroethane-d4 MB VOC 08061 SUIT: 4-Bromofluorobenzene MB VOC 08061 SUIT: Dibromofluoromethane MB VOC 08061 SUIT: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com _Q_C_~U_M_M_ARY lU3~_PQRI_ Contact: Jo Ann Tischler Dept: MSVOA QC Type: MBLK Amount Original Units Method Result Spiked Amount %REC Limits /lglL SW8260C < 1.00 %REC SW8260C 50.4 50.00 101 76-138 %REC SW8260C 51.6 50.00 103 77-121 %REC SW8260C 49.2 50.00 98.5 67-128 %REC SW8260C 50.0 50.00 100 81-135 %RPD RPD Limit Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 8/6/2012 752h 8/6/2012 752h 8/6/2012 752h 8/6/2012 752h 8/6/2012 752h Report Date: 8/14/2012 Page 9 of 17 I analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility Client: Denison Mines Lab Set ID: 1208066 Project: Semi Annual Ground Water Sample ID Analyte 1208066-001AMS Tetrahydrofuran 1208066-001AMS SUIT: 1 ,2-Dichloroethane-d4 1208066-001AMS SUIT: 4-Bromofluorobenzene 1208066-001 AMS SUIT: Dibromofluoromethane 1208066-001 AMS SUIT: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com _QC_SJJMMAJlY_REPDBI_ Contact: Jo Ann Tischler Dept: MSVOA QC Type: MS Amount Original Units Method Result Spiked Amount %REC Limits flglL SW8260C 14.5 20.00 0 72.7 43-146 %REC SW8260C 53.4 50.00 107 72-151 %REC SW8260C 49.3 50.00 98.5 80-128 %REC SW8260C 52.0 50.00 104 80-124 %REC SW8260C 49.6 50.00 99.1 77-129 %RPD RPD Limit Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 8/6/2012 908h 8/6/2012 908h 8/6/2012 908h 8/6/2012 908h 8/6/2012 908h Report Date: 8114/2012 Page 10 of 17 I analyses applicable to the CW A, SDW A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COc. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility Client: Denison Mines Lab Set ID: 1208066 Project: Semi Annual Ground Water Sample ID Analyte 1208066-001 AMSD Tetrahydrofuran 1208066-001AMSD SUIT: 1,2-Dichloroethane-d4 1208066-001 AMSD SUIT: 4-Bromofluorobenzene 1208066-001 AMSD SUIT: Dibromofluoromethane 1208066-001 AMSD SUIT: Toluene-d8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com ___ Q_C_~UMM_A_&Y_RE_P_QR_I_ Contact: Jo Ann Tischler Dept: MSVOA QC Type: MSD Amount Original Units Method Result Spiked Amount %REC Limits IlglL SW8260C 13.2 20.00 0 66.2 43-146 %REC SW8260C 52.1 50.00 104 72-151 %REC SW8260C 50.0 50.00 99.9 80-128 %REC SW8260C 51.6 50.00 103 80-124 %REC SW8260C 49.5 50.00 99.0 77-129 %RPD 9.28 RPD Limit 25 Kyle F. Gross Laboratory Director Jose Rocha QA Officer Qual Date Analyzed 8/6/2012 927h 8/6/2012 927h 8/6/2012 927h 8/6/2012 927h 8/6/2012 927h Report Date: 8/14/2012 Page 11 of 17 I analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached CDC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AUG12-C\06AUG12\ R32L0661.D 6 Aug 2012 8:11 am 1208066-001A SAMP 5.0ML 10F3 SB 6 Sample Multiplier: 1 Quant Time: Aug 06 08:23:50 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_60.M Quant Title VOA Calibration QLast Update Fri Jul 27 07:53:44 2012 Response via Initial Calibration (QT Reviewed) Abundance 15000001 TIC: R3'2L0661.D\data.ms 14500001 1400000! 13500001 13000001 1250000 1200000; I 1150000J 11000001 1050000j 1 000000 i I 950000j I I I 900000i 850000i 8000001 750000J 700000j 650000j 6000001 5500001 500000j 4500001 I 4000001 , 3500001 300000) 2500001 1 200000 150000i I 1000001 50000 1 tf) as ~ ii i f I I I I I " \ I '1 u; "0 cb c: (]) ~ (]) .c -v" e 0 "9 :E (]) t) c: en Ql Cl cD ~ ~ c: Ql ~ Q) .c N f c: CD (]) .c £ e 0 as :::J ~ t;:: 0 E co e l+-co ~ ~ I :::J en I ! 1 ) 11 ;i ,; " !I 0·:,;-:::-~1~~·:~.:::::1 .. :::::::.,::.~~;,:~\-.r-·:r-::::;=::~r::~:;,-,.-::·1::::::;::::;:::'::"-::;'::::~':'::::":':1-.····:·;::~:·;,~"",;."=·'f"""":. '.--;---. ',-'., -, i-,.-.,.''I"L..Li. -,----'. "U.~.L~-r-, -'. -, ,-, -I' ~";\'i'~'" '-f .. -,.~. ; '. L;.~_,-".U>-r--~. "t.t"u~"f":'''''f.'~'~'; .----------.-.. -.---.... ----.. ----,----.--~.~.-'-'"-... ,...:c'''''':~''''~=:;::~.,;,.?:::'P::·T~~::..=r-:::::f::::~::::::::::::::::::::=:::;:.7:-i" .. : .. .,.--, .... -, ..... , ...... ' ..... r·_··· .. ·T····T···-r-·'r--.,--r·-T·--i--·r····- Time--> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 AFULLW_60.M Mon Aug 06 08:24:29 2012 Report Date: 8114/201(2gEPage412 of 17 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AUG12-C\06AUG12\ R34L0662.D 6 Aug 2012 8:49 am 1208066-002A SAMP 5.0ML 10F3 SB 8 Sample Multiplier : 1 Quant Time: Aug 06 09:07:30 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_60.M Quant Title VOA Calibration QLast Update Fri Jul 27 07:53:44 2012 Response via Initial Calibration (QT Reviewed) Abundance TIC: R34L0662.D\data.ms 15000001 ! 14500001 14000001 13500001 j 13000001 I 12500001 12000001 11500001 , 1100000j 10500001 10000001 950000: 900000! 8500001 8000001 750000 ' 700000i 6500001 600000j 5500001 5000001 I 4500001 400000i I 350000j 3000001 2500001 2000001 150000j 100000 50000J 5 (J) t: ::> (J) If) as "0 d, c: ~ '0 f-t: ::> (J) cD c: Q) N c: Q) ..c e 0 .2 LL. 0 f-!a a.O (J) "0 d, cD c: c: ~ Q) II) N N V c: c: II) II) Q) ..c ..c c: e e ~ ..2 g c: .c: Q) 'E ..c 0 f 0 E ..2 f-e -£ !a co ~ qs (J) i tl; T I I I I I I O.\~:.T.";~::";::f.".(';.:::~:~l:."T::T::::::::;:::::;:=:'=T::T:::::;::::;::::r::'f''i'' •. ,......,_~~.:L;-_~-JU1,-:-. -. -. -, JL-"1~,~~,~~)li , , . ,1l-r~'.'T.""" Time--> 1.50 2.90 2.50 ~.OO 3.~0 4.0Q 4.50 5.00 5.50 6.00 6.50 7.00 7.~0 8:00 8.5~~::-;-;;;r"i:·;:I9T=~.:~~:~:~i:=,~~::~or.:.r~~:~~i:=:;~~~~~r AFULLW_60.M Mon Aug 06 09:08 :06 2012 Report Date: 8/14/2@1~gEPage413 of 17 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AUG12-C\06AUG12\ R29LCS20.D 6 Aug 2012 7:14 am LCS VOC 080612A LCS SEE COVERSHEET FOR ID AND AMOUNT JO 3 Sample Multiplier: 1 Quant Time: Aug 06 07:26:26 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_60.M Quant Title VOA Calibration QLast Update Fri Jul 27 07:53:44 2012 Response via Initial Calibration (QT Reviewed) Abundance 2700000 j TIC: R29LCS20.D\data.ms 2600000 1 1 i 2500000 1 2400000 1 2300000 ] , 2200000 1 2100000j 2000000 1 i 1900000 j 1800000 j 17000001 16000001 1500000 1400000 1 I 1300000 j 1 12000001 I 1100000 1 1 1000000 1 ! 900000 j i 800000 ! AFULLW_60.M Mon Aug 06 07:27:06 2012 ~ I i Report Date: 8/14/lOiwepa~ 1 of17 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AUG12-C\06AUG12\ R31LMBLK.D 6 Aug 2012 7:52 am MB MBLK 5 VOC 080612A 5.0ML JO Sample Multiplier: 1 Quant Time: Aug 06 08:09:20 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_60.M Quant Title VOA Calibration QLast Update Fri Jul 27 07:53:44 2012 Response via Initial Calibration (QT Reviewed) Abundance TIC: R31 LMBLK.D\data.ms 15000001 i 1400000i 13000001 I j 1200000j [ [ 1100000i I 10000001 I ! 9000001 800000 I 7000001 ! I 6000001 I 500000 1 I I 300000j ! i 2000001 I 1000001 Time--> AFULLW_60.M Mon Aug 06 08:09:51 2012 Report Date: 8/14/wge Pa~ 1 of 17 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AUG12-C\06AUG12\ R35S0661.D 6 Aug 2012 9:08 am 1208066-001AMS MS 5.0ML 20F3 SB 9 Sample Multiplier: 1 Quant Time: Aug 06 09:20:34 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_60.M Quant Title VOA Calibration QLast Update Fri Jul 27 07:53:44 2012 Response via Initial Calibration (QT Reviewed) Abundance 27000001 TIC: R35S0661.D\data.ms 26000001 i 25000001 I 24000001 I 23000001 ! 22000001 1 2100000j i 20000001 ! 1 1900000j 1800000j 1700000J 1 16000001 ! 15000001 14000001 1300000: 1200000! 11000001 10000001 1 I 9000001 j 8000001 I 700000j 6000001 500000 1~ ,eu 1£ iQ) IE 400000i§ a: boP.. l;;:~ 300000111 l~ ~ 200000t ~ 10000011 1 0\)L-- Time--> 1.50 AFULLW_60.M Mon Aug 06 09:21:26 2012 u1 "0 d> c: I en cD c: '" ~ as "9 Q) ..c Q) e c: Q) 0 :::l :::l ~ '5 E ~ e :::l ~ rn III II :s Ii en !I Report Date: 8/14/2@1<lgEPage416 of 17 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AUG12-C\06AUG12\ R36D0661.D 6 Aug 2012 9:27 am 1208066-001AMSD MSD 5.0ML 30F3 SB 10 Sample Multiplier: 1 Quant Time: Aug 06 09:39:37 2012 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_60.M Quant Title VOA Calibration QLast Update Fri Jul 27 07:53:44 2012 Response via Initial Calibration (QT Reviewed) Abundance TIC: R36D0661.D\data.ms 2800000~ 27000001 26000001 25000001 24000001 2300000: 22000001 21000001 2000000j 19000001 1800000j 17000001 i 16000001 i 15000001 i 14000001 1 1300000i 1 1200000i 1100000; 10000001 9000001 800000j I 7000001 ! I 600000 i :C1l 500000j~ :'iil iE 400000ie '!b ~~ 3000001~ ~ ~~ 200000ji:5 ~ AFULLW_60.M Mon Aug 06 09:40:38 2012 II) as "C ell c: ~ (5 I-1;: :::l en II) "9 (I) c: (I) N c: (I) .c e :i I r I .1 ~~ "(I) ~ Co ell iE Report Date: 8/14/2@'I~gEPage417 of 17 American West Analytical Laboratories WORK ORDER Summary Client: Client ID: Project: Denison Mines DENIOO Semi Annual Ground Water Contact: Jo Ann Tischler QC Level: LEVEL III Comments: PA Rush. QC 3 & Summary. EDD-EIM into Locus Database. Report THF to 1 flg/L.; Sample ID Client Sample ID Collected Date Received Date Date Due 1208066-001 A ~VV-37_07302012 7/30/2012134011 8/3/20121100h 8/14/2012 1208066-001B SEL Analytes: SN 1208066-002A Trip Blank 7/30/2012 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT 0 QC 0 HOK __ _ UL Denison Worl\. Order: 1208066 Page 1 of 1 8/3/2012 WOType: Project Matrix Test Code Sel Storage Aqueous 8260-W ~ VOCFridge 3 200.8-DlS ~ MET -8260-W ~ VOCFridge 3 HOK __ _ HOK __ Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: American West Analytical Lab 463 West 3600 South Salt Lake City, Ut 84115 Contact: Garrin Palmer or David Turk Ph: 4356782221 apalmer@denisonmines.com dturk@denisonmines.com tholl iday@denisonmines.com Chain of Custody/Sampling Analysis Request p . t rOJec S amp ers N arne S amp ers S· t Igna ure 3rd Quarter Ground /I~ Water 2012 Tanner Holliday ""-hA1/111' I I J Date Time Sample ID Collected Collected Laboratory Analysis Requested MW-37 07302012 7/30/2012 1340 THF, TIN Trip Blank 7/30/2012 TI-/ F " Please notify Garrin Palmer or Tanner Holliday of Reciept tempature on these samples Immediately! Thank you. Relinquished By:(Signature) Date/Time Received By:(Signature) Date/Time ::jdJfUC-}J~ 812.!2012 1100 Relinquished By:(Signature) Date/Time 0dl=re) ~me '7' /100 \J ! Samples Were: COC Tape Was: ~Shipped By: 'reV( -X Present on Outer Package o Hand Delivered r $Yes DNo ON/A o Ambient Unbroken on Outer package JirChilled ~ ,let... Jf(Yes DNa ON/A If Temperature L., °C Present on Sample Rec. Broken/Leaking DYes %No DN/A DYes DNo ~/A Notes: Properly Preserved Notes: Rec. Within Hold Notes: Bottle Type Aml1'lOnia COD Cyanide Metals N02 &N03 Nutrients O&G Phenols Sulfide TKN TOC TP04 TPH Procedure: Unbroken on S~Ple DYes DNo N/A )4'Yes ONo DN/A Notes: I fo"Yes ONo /\ Preservative All pHs OK I pH <2 H2SO4 pH <2 H2SO4 PH>12 NaOH pH <2 HN03 Yef\ pH <2 H2SO4 II pH <2 H2SO4 pH<2HCL pH <2 H2SO4 pH> 9NaOH, ZnAC pH <2 H2SO4 pH <2 H3P04 pH <2 H2SO4 pH<2HCL Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid l~o?o{J1h Lab Set ID: _________ _ . Container Type: ~ W AL Supplied Plastic o A W~ Supplied Clear Glass o AWAL's'1.l.Pplied Amber Glass o A WAL SU~~OAlTOC/TOX Vials o Amber 0 Clear Headspace 0 No Headspace o Non A WAL Suppli~Container Notes: ~ ~ Discrepancies Between Labels and cac Notes: 1) 2) 3) 4) 5) 6) 7) If sample is notpreserved properly list its extension and receiving pH in the appropriate column above Flag eoe and notify client for further instructions . Place client conversation on eoe Samples may be adjusted at client request No. Rec. DYes &No I , www.energylab.com EN:RGY LAElORATORI E5 Analytltal £XcslhHlcB SinCIJ 1952 :tf.~!eQa, MT 817~472 .. 0711 • Billings. MY 800-735-4489 • Casper, W,{ 888-235-0515 .. :;ili~~~/wy,8Q6"Q86"71 7~ (I Rapid City, Sll 888 .. 612-1225 • College Station, IX 888~690-2218 ANALYTICAL SUMMARY REPORT August 10, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12070448 Quote 10: C1640 -POC Wells Project Name: 3rd Quarter Groundwater 2012 Energy Laboratories, Inc. Casper WY received the following 13 samples for Denison Mines USA Corp on 7/13/2012 for analysis. Sample ID Client Sample ID C12070448-001 MW-29_071 02012 C12070448-002 MW-32_07092012 C12070448-003 MW-11_07112012 C12070448-004 MW-14_07112012 C12070448-005 MW-25_071 02012 C12070448-006 MW-26_07112012 Collect Date Receive Date Matrix Test 07/10/12 13:45 07/13/12 Aqueous Metals by ICP/ICPMS, Dissolved 07/09/1213:15 07/13/12 Aqueous Gross Alpha minus Rn222 and Uranium 07/11/1212:10 07/13/12 Aqueous Alkalinity QA Calculations Chloride Fluoride Metals by ICP, Dissolved Metals by ICP-MS, Dissolved Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Solids, Total Dissolved -Calculated Sulfate SW8260B VOCs, Standard List 07/11/12 12:35 07/13/12 Aqueous Same As Above 07/10/12 12:20 07/13/12 Aqueous Same As Above 07/11/129:51 07/13/12 Aqueous Alkalinity QA Calculations Chloride Fluoride Metals by ICP, Dissolved Metals by ICP-MS, Dissolved Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Solids, Total Dissolved -Calculated Sulfate Page 1 of 54 EI\ERGY LA80RATORI ES C 12070448-007 C 12070448-008 C 12070448-009 C12070448-010 C 1 2070448-011 C12070448-012 C12070448-013 ~'" www.energylab.com ~ Analytical Excs/lsnl:B Sines 7152 Helel\3, MT 877-472-0711 • Billings, MT 800 .. 735-4489 • Casper, WY 888-235-0515 ~i1.1~tt~, WY8&6-686 .. 71 15 • Rapid City, SI) 888-672-1225 • College Station, IX 888-690-2218 ANAL VTICAL SUMMARY REPORT MW-30_071 02012 07/10/12 11 :00 07/13/12 Aqueous Alkalinity QA Calculations Chloride Fluoride Metals by ICP, Dissolved Metals by ICP-MS, Dissolved Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Solids, Total Dissolved -Calculated Sulfate SW8260B VQCs, Standard List MW-31_07092012 07/09/1213:35 07/13/12 Aqueous Same As Above MW-35_071 02012 07/10/1214:1007/13/12 Aqueous Same As Above MW-36_07112012 07/11/129:15 07/13/12 Aqueous Same As Above MW-65_07112012 07/11/129:51 07/13/12 Aqueous Alkalinity QA Calculations Chloride Fluoride Metals by ICP, Dissolved Metals by ICP-MS, Dissolved Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Solids, Total Dissolved -Calculated Sulfate Trip Blank 6706 07/09/12 0:00 07/13/12 Aqueous SW8260B VQCs, Standard List Temp Blank 07/12/12 0:00 07/13/12 Aqueous Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 , unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601 , unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: c5¥~D LJDl~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.08.10 10:55:13 -06:00 Page 2 of 54 WWN.energylab.com Analytical ExcsllsncB Sines 1$52 ~elena,. MT 811-412 .. 0111 • Billings,MT 800-735-4489 . Casper. W'f 888~235-0515 'GUletta. WY.866-686-7175 • Rapid City, SO 888-672·J225 • College Station, IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Sample Delivery Group: C12070448 REVISED/SUPPLEMENTAL REPORT Revised Date: 08/10/12 Report Date: 08/09/12 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on August 10,2012 to remove the VOC's from samples MW-26 and MW-65. The data presented here reflects this change. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002; Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that c.ertain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 3 of 54 EN:RGY www.energylab.com . . .. Helena,. MT 877-472-D71 1 • Billings, MT 800-735 .. 4489. Casper, WV 888-235-0515 AnaIytll;aI£XCSIISflCIlSincs 1952 ._ ,~m~1f~"W¥8~6-6B6-7175 • Rapid City, S[) 888-&72-1225. College Station, IX 888-690-2218 L.ABORATORI ES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 LablD: C12070448-003 Client Sample ID: MW-11_07112012 Analyses PHYSICAL PROPERTIES pH Lab ID: C12070448-004 Client Sample ID: MW-14_07112012 Analyses PHYSICAL PROPERTIES pH LablD: C 12070448-005 Client Sample ID: MW-25_07102012 Analyses PHYSICAL PROPERTIES pH LablD: C12070448-006 Client Sample ID: MW-26_07112012 Analyses PHYSICAL PROPERTIES pH Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. Result Units 7.76 s.U. Result Units 6.91 s.u. Result Units 6.94 s.U. Result Units 7.00 s.U. H -Analysis performed past recommended holding time. Qualifiers Rl H 0.01 Qualifiers Rl H 0.01 Qualifiers Rl H 0.01 Qualifiers Rl H 0.01 Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/1212:10 DateReceived: 07/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-H B 07/13/12 13:57 1 ab Collection Date: 07/11/12 12:35 DateReceived: 07/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-H B 07/13/1213:591 ab Collection Date: 07/10/12 12:20 DateReceived: 07/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By MeL! A4500-H B 07/13/12 14:021 ab Collection Date: 07/11/1209:51 DateReceived: 07/13/12 Matrix: Aqueous Qel Method Analysis Date 1 By A4500-H B 07/13/12 14:051 ab MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 26 of 54 EN:RGY LABORATORIES www.energyJab.comHelen~ •. MT877 .. 472-0711.Billings.MT 800-735-4489 • Casper, WY888-235-0515 Ana~/Ex"JJsncIlSil1Cs 1952 b,~,,;Mj!6lf,.wY 8'~& .. 686-7t75. • Rapid City, Sf) 888-672-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Lab ID: C12070448-007 Client Sample ID: MW-30_071 02012 Analyses PHYSICAL PROPERTIES pH LablD: C 12070448-008 Client Sample ID: MW-31_07092012 Analyses PHYSICAL PROPERTIES pH LablD: C 12070448-009 Client Sample ID: MW-35_071 02012 Analyses PHYSICAL PROPERTIES pH LablD: C 12070448-0 1 0 Client Sample ID: MW-36_07112012 Analyses PHYSICAL PROPERTIES pH Report RL -Analyte reporting limit. Definitions: QCl -Quality control limit. Result Units 7.17 S.u. Result Units 7.48 S.u. Result Units 6.94 S.u. Result Units 7.18 S.u. H -Analysis performed past recommended holding time. Qualifiers Rl H 0.01 Qualifiers Rl H 0.01 Qualifiers Rl H 0.01 Qualifiers Rl H 0.01 Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/10/12 11 :00 DateReceived: 07/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-H B 07/13/1214:071 ab Collection Date: 07/09/12 13:35 DateReceived: 07/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By MeL! A4500-H B 07/13/1214:101ab Collection Date: 07/10/12 14:10 DateReceived: 07/13/12 Matrix: Aqueous Qel Method Analysis Date 1 By A4500-H B 07/13/1214:131 ab Collection Date: 07/11/1209:15 DateReceived: 07/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-H B 07/13/1214:15/ab MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 27 of 54 EN:RGY LABORATORIES www.energylab.com Aflalytica/ ExcsIJsncB SilICa '952 H,elena, MT 877 .. 472-0711 • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 .~ii.!e.~e, Wv 8&&-~B~-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Lab 10: C12070448-011 Client Sample 10: MW-65_07112012 Analyses PHYSICAL PROPERTIES pH Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. Result Units 7.03 s.U. H -Analysis performed past recommended holding time. MCLI Revised Date: 08/10/12 Report Date: 08/09/12 Collection Date: 07/11/1209:51 DateReceived: 07/13/12 Matrix: Aqueous Qualifiers RL QCL Method Analysis Date / By H 0.01 A4500-H B 07/13/1214:18/ ab MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 28 of 54 EN:RGY LABORATORIES www.energylab.com ~/yticI1 Ext;BUBflCB Si11C8 1952 f He"lena, Mt877~472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ ~)illette,WV 866~$B6-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C 12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A2320 B Sample 10: MBLK Alkalinity, Total as CaC03 Carbonate as C03 Bicarbonate as HC03 Sample 10: LCS-6677 Alkalinity, Total as CaC03 Sample 10: C12070448-008AOUP Alkalinity, Total as CaC03 Carbonate as C03 Bicarbonate as HC03 Sample 10: C12070448-009AMS Alkalinity, Total as CaC03 Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Method Blank ND mg/L ND mg/L ND mg/L Laboratory Control Sample 201 mg/L Sample Duplicate 172 mg/L ND mg/L 210 mg/L Sample Matrix Spike 458 mg/L RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R161902 Run: MANTECH_120713B 07/13/1215:28 5.0 1.0 1.0 Run: MANTECH_120713B 07/13/12 15:44 5.0 100 90 110 Run: MANTECH 120713B 07/13/12 19:29 - 5.0 3.9 10 5.0 10 5.0 3.9 10 Run: MANTECH_120713B 07/13/12 19:45 5.0 105 80 120 ND -Not detected at the reporting limit. Page 29 of 54 EI\ERGY LABORATORiES www.energyJab.com Allatytit;al Ex~nsnCB $fRcg 1952 ; ,He.iella, MT871-472-011 t " Billings. MT 800-735-4489 • Casper, WY 888-235-0515 9i1i~iite:,WV86$~686 .. 7n5 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A2540 C Sample 10: MB-1_120713A Method Blank Solids, Total Dissolved TDS @ 180 C NO mg/L Sample 10: LCS-2_120713A Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1090 mg/L Sample 10: C12070433-001A MS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 2180 mg/L Sample 10: C12070448-003A OUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 2020 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: TDS120713A Run: BAL-1_120713A 07/13/12 15:40 10 Run: BAL-1_120713A 07/13/12 15:40 10 98 90 110 Run: BAL-1 120713A 07/13/12 15:49 10 101 90 110 Run: BAL-1 120713A 07/13/1215:51 10 0.3 5 NO -Not detected at the reporting limit. Page 30 of 54 EN:RGY LABORATORIES www.energylab.com Ana/ytil;aIEx~UI1fWII Sines '952 Helena,. MTB77-472-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 _ ,~jlle#e, wY 866-686-7175 .. Rapid City, Sf) 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4500-CI B Sample 10: MBLK9-120719 Chloride Sample 10: C12070244-001AMS Chloride Sample 10: C12070244-001AMSO Chloride Sample 10: C12070448-006AMS Chloride Sample 10: C12070448-006AMSO Chloride Sample 10: LCS35-120719 Chloride Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank ND mg/L Sample Matrix Spike 44.7 mg/L Sample Matrix Spike Duplicate 44.7 mg/L Sample Matrix Spike 259 mg/L Sample Matrix Spike Duplicate 255 mg/L Laboratory Control Sample 3620 mg/L RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: 120719-CL-TTR-W Run: TITRATION_120719A 07/19/1214:05 1.0 Run: TITRATION_120719A 1.0 100 90 110 Run: TITRATION 120719A 1.0 100 90 110 Run: TITRATION 120719A 1.0 102 90 110 Run: TITRATION 120719A - 1.0 100 90 110 Run: TITRATION_120719A 1.0 102 90 110 ND -Not detected at the reporting limit. 0.0 1.4 07/19/12 14:49 07/19/12 14:50 10 07/19/12 15:23 07/19/12 15:24 10 07/19/12 15:28 Page 31 of 54 EN:RGY LABORATORIES www.energylab.com Ana~1 Ext;8HI1f1&B $inC8 1952 Helena, MTB77-472-0711 • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 _. ~_, _~ille~Q, WY 86&-686-7175 • Rapid Cfty, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Method: A4S00-F C Sample 10: MBLK Fluoride Sample 10: LCS-6892 Fluoride Sample 10: C12070448-003AMS Fluoride Sample 10: C12070448-003AMSO Fluoride Qualifiers: RL -Analyte reporting limit. Count Result Units Method Blank NO mg/L Laboratory Control Sample 1.96 mg/L Sample Matrix Spike 2.38 mg/L Sample Matrix Spike Duplicate 2.38 mg/L MDC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R161878 Run: MANTECH_120713A 07/13/12 11 :08 0.10 Run: MANTECH_120713A 07/13/12 11 :12 0.10 98 90 110 Run: MANTECH 120713A 07/13/1214:01 - 0.10 95 80 120 Run: MANTECH 120713A 07/13/12 14:06 - 0.10 95 80 120 0.0 10 NO -Not detected at the reporting limit. Page 32 of 54 www.energylab.com . '" " Helena,MtB77:..412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 EI\ERGY LABORATORIES Allalytit;al Ex"IIIHICB Sines 1952 S""'" ,_ ',. ,~ill~lfe, 'III '66-.86-71 75 • Rapid GIly, SD 88l-672-1225 • CQllege Sialion, TIC 888-698-2218 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: A4500-H B Sample 10: pH 6.86 pH Sample 10: pH 6.86 pH Method: A4500-H B Sample 10: C12070448-011AOUP pH Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 6.85 S.u. 0.010 100 Initial Calibration Verification Standard 6.85 S.u. 0.010 100 Sample Duplicate 6.99 s.u. 0.010 98 98 Analytical Run: PHSC_101-C_120713A 07/13/1208:52 102 102 0.6 07/13/12 13:17 Batch: R161844 07/13/12 14:21 3 NO -Not detected at the reporting limit. Page 33 of 54 EN:RGY LABORATORIES www.energyJab.com ~Iytic;aIExt;8'IBIICIJ $i1I~ 1952 ,' ..•.. ' .. , ' ..• H~lena, MT877-472-0711.-Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ... ~'§j)t~tt~;;Wy8~$~~86-n 75 • Rapid City, SO 888-672-1225 • College Station,lX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4500-NH3 G Sample 10: MBLK-1 Method Blank Nitrogen, Ammonia as N NO mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Ammonia as N 1.92 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Ammonia as N 1.99 mg/L Sample 10: C12070412-002CMS Sample Matrix Spike Nitrogen, Ammonia as N 1.92 mg/L Sample 10: C12070412-002CMSO Sample Matrix Spike Duplicate Nitrogen, Ammonia as N 1.96 mg/L Sample 10: C12070448-007CMS Sample Matrix Spike Nitrogen, Ammonia as N 2.04 mg/L Sample 10: C12070448-007CMSO Sample Matrix Spike Duplicate Nitrogen, Ammonia as N 2.06 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL O/OREC Low Limit High Limit RPO RPOLimit Qual Batch: R162001 Run: TECHNICON_120717A 07/17/12 10:56 0.050 Run: TECHNICON_120717A 07/17/12 10:58 0.050 96 90 110 Run: TECHNICON_120717A 07/17/12 11 :00 0.050 102 80 120 Run: TECHNICON_120717A 07/17/12 12:34 0.050 98 90 110 Run: TECHNICON_120717A 07/17/12 12:36 0.050 100 90 110 2.1 10 Run: TECHNICON_120717A 07/17/1213:22 0.050 103 90 110 Run: TECHNICON_120717A 07/17/12 13:24 0.050 104 90 110 1.0 10 NO -Not detected at the reporting limit. Page 34 of 54 EI'.ERGY LABORATORIES www.energylab.com mtytit;af Ex~UIlflt;B SInes 1952 Hel~l1a, MlB77-472-0711 -Billings, MT 800-735-4489 '" Casper, WY 888-235-0515 ",~'§!II~~~,'#r86&-6S6~7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4S00-S04 E Sample 10: LCS-1_120720 Sulfate Sample 10: MBLK-1_120720 Sulfate Sample 10: C12070448-011AMS Sulfate Sample 10: C12070448-011AMSO Sulfate Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Laboratory Control Sample 4600 mg/L Method Blank ND mg/L Sample Matrix Spike 2660 mg/L Sample Matrix Spike Duplicate 2640 mg/L RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: 120720_1_S04-TURB-W Run: TURB-2_120720A 07/20/12 11 :43 100 96 90 110 Run: TURB-2_120720A 07/20/12 11 :46 10 Run: TURB-2_120720A 07/20/12 13:35 50 98 90 110 Run: TURB-2_120720A 07/20/12 13:47 50 95 90 110 0.9 10 ND -Not detected at the reporting limit. Page 35 of 54 EI'fRGY L ABORATORIES www.energylab.com r'; .... Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~/yIWIIEx",UsnCB SiwJ 1952 1. '." '" ~' J iUel:fe, WY 866.;686-1175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C 12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: E200.7 Result Units RL Sample 10: ICV Initial Calibration Verification Standard Calcium 48.8 mg/L 0.50 Sample 10: ICSA Interference Check Sample A Calcium 483 mg/L 0.50 Sample 10: ICSAB Interference Check Sample AB Calcium 478 mg/L 0.50 Method: E200.7 Sample 10: MB-120719A Method Blank Calcium ND mg/L 0.50 Sample 10: LFB-120719A Laboratory Fortified Blank Calcium 47.6 mg/L 0.50 Sample 10: C12070448-006BMS2 Sample Matrix Spike Calcium 709 mg/L 0.50 Sample 10: C12070448-006BMSO Sample Matrix Spike Duplicate Calcium 727 mg/L 0.50 Method: E200.7 Sample 10: ICV Initial Calibration Verification Standard Iron 5.04 mg/L 0.030 Sample 10: ICSA Interference Check Sample A Iron 176 mg/L 0.030 Sample 10: ICSAB Interference Check Sample AB Iron 174 mg/L 0.030 Method: E200.7 Sample 10: MB-120716A Method Blank Iron ND mg/L 0.030 Sample 10: LFB-120716A Laboratory Fortified Blank Iron 0.970 mg/L 0.030 Sample 10: C12070492-001 BMS2 Sample Matrix Spike Iron 0.865 mg/L 0.030 Sample 10: C12070492-001 BMSO Sample Matrix Spike Duplicate Iron 0.887 mg/L 0.030 Qualifiers: %REC Low Limit High Limit 98 95 105 97 80 120 96 80 120 Run: ICP2-C_120719A Run: ICP2-C_120719A 95 85 115 Run: ICP2-C 120719A - 85 70 130 Run: ICP2-C _120719A 92 70 130 101 95 105 88 80 120 87 80 120 Run: ICP4-C_120716A Run: ICP4-C_120716A 97 85 115 Run: ICP4-C 120716A - 85 70 130 Run: ICP4-C 120716A - 87 70 130 RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration RPO RPOLimit Qual Analytical Run: ICP2-C_120719A 07/19/12 11 :32 07/19/1212:18 07/19/12 12:22 Batch: R162123 07/19/12 12:42 07/19/12 12:46 07/19/12 17:56 07/19/12 18:01 2.5 20 Analytical Run: ICP4-C_120716A 07/16/12 14:12 07/16/12 14:26 07/16/12 14:30 Batch: R161962 07/16/12 14:34 07/16/12 14:38 07/16/12 15:37 07/16/12 15:41 2.5 20 Page 36 of 54 www.energyJab.com mlytical ~lIl1f1cB SiIws 1m ' ...... ' .. " '~ele~a, Ml877~412-0711 "Billings, MT 800~735-4489 " Casper, WY 888-235-0515 c_gi!.l~fite, w.~ .86.&"686-"7175 • Rapiq City, SD 888-672-1225 • College Station, TX 888-690-2218 ENERGY LABORATORIES QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.7 Analytical Run: ICP4-C_120718A Sample 10: ICV 5 Initial Calibration Verification Standard 07/18/1214:12 Calcium 49.9 mg/L 0.50 100 95 105 Iron 5.00 mg/L 0.030 100 95 105 Magnesium 50.1 mg/L 0.50 100 95 105 Potassium 49.4 mg/L 0.50 99 95 105 Sodium 50.4 mg/L 0.50 101 95 105 Sample 10: ICSA 5 Interference Check Sample A 07/18/12 14:26 Calcium 455 mg/L 0.50 91 80 120 Iron 176 mg/L 0.030 88 80 120 Magnesium 517 mg/L 0.50 103 80 120 Potassium -0.0109 mg/L 0.50 Sodium 0.422 mg/L 0.50 Sample 10: ICSAB 5 Interference Check Sample AB 07/18/12 14:30 Calcium 451 mg/L 0.50 90 80 120 Iron 177 mg/L 0.030 88 80 120 Magnesium 514 mg/L 0.50 103 80 120 Potassium -0.0228 mg/L 0.50 Sodium 0.352 mg/L 0.50 Method: E200.7 Batch: R162060 Sample 10: MB-120718A 5 Method Blank Run: ICP4-C_120718A 07/18/12 14:34 Calcium NO mg/L 0.50 Iron NO mg/L 0.030 Magnesium ND mg/L 0.50 Potassium NO mg/L 0.50 Sodium NO mg/L 0.50 Sample 10: LFB-120718A 5 Laboratory Fortified Blank Run: ICP4-C_120718A 07/18/12 14:38 Calcium 48.3 mg/L 0.50 97 85 115 Iron 0.959 mg/L 0.030 95 85 115 Magnesium 47.9 mg/L 0.50 96 85 115 Potassium 48.4 mg/L 0.50 97 85 115 Sodium 48.2 mg/L 0.50 96 85 115 Sample 10: C12070448-010BMS2 5 Sample Matrix Spike Run: ICP4-C -120718A 07/18/12 15:34 Calcium 638 mg/L 0.50 80 70 130 Iron 4.58 mg/L 0.030 90 70 130 Magnesium 366 mg/L 0.50 91 70 130 Potassium 229 mg/L 0.50 86 70 130 Sodium 826 mg/L 1.0 75 70 130 Sample 10: C12070448-010BMSO 5 Sample Matrix Spike Duplicate Run: ICP4-C_120718A 07/18/12 15:38 Calcium 648 mg/L 0.50 84 70 130 1.5 20 Iron 4.72 mg/L 0.030 93 70 130 2.9 20 Magnesium 373 mg/L 0.50 94 70 130 1.9 20 .-~--~--.-.------------.---.------.------.--.---.---------_._----_._---.---------.. _------------_._-----------_._--------_ .. _---------_._-"-_ .. _--------_ .. _---_._---_._----_._----.--------_._----_._-----"----------_._-------_._----------_._------.-•. _------_._--_._----------------_._-_.--------_._---------_.---_.- Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 37 of 54 ·EN:RGY LABORATORIES www.energylab.com AnalyticilExCll/ltmcll ~ 1952 Helena" MT 877-472-0111 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 _;~ilIette" WY 866 .. $86-1175 • Rapid City, SD' 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C 12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: E200.7 Result Units Sample 10: C12070448-010BMSO 5 Sample Matrix Spike Duplicate Potassium 237 mg/L Sodium 857 mg/L ----------.----------------.------------------------------- Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit 0.50 1.0 89 87 Run: ICP4-C _120718A 70 130 70 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 3.3 3.6 Batch: R162060 07/18/12 15:38 20 20 Page 38 of 54 EN:RGY LABORATORIES W " -_gyl.b.com ~ •. ··~·H~.n., 1oI1"871-472·D711 • Billings, MT 800-735-4489 • Casper, WY 888·235·0515 ...., ~ ~~/ExCBUBfl~BSincs'852 J-,-l2::~~..1' ~'~iile#e, 'NY 866-&86-7175 • Rapid Cfty, Sf) 888-&72-1225 • College Station,lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Client: Denison Mines USA Corp Report Date: 08/09/12 Project: 3rd Quarter Groundwater 2012 Work Order: C12070448 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.8 Analytical Run: ICPMS4-C_120724A Sample 10: ICV 15 Initial Calibration Verification Standard 07/24/12 13:32 Arsenic 0.0514 mg/L 0.0010 103 90 110 Cadmium 0.0520 mg/L 0.0010 104 90 110 Chromium 0.0504 mg/L 0.0010 101 90 110 Cobalt 0.0522 mg/L 0.0010 104 90 110 Copper 0.0530 mg/L 0.0010 106 90 110 Lead 0.0503 mg/L 0.0010 101 90 110 Manganese 0.0511 mg/L 0.0010 102 90 110 Molybdenum 0.0501 mg/L 0.0010 100 90 110 Nickel 0.0522 mg/L 0.0010 104 90 110 Selenium 0.0513 mg/L 0.0010 103 90 110 Silver 0.0209 mg/L 0.0010 105 90 110 Thallium 0.0513 mg/L 0.0010 103 90 110 Uranium 0.0506 mg/L 0.00030 101 90 110 Vanadium 0.0505 mg/L 0.0010 101 90 110 Zinc 0.0529 mg/L 0.0010 106 90 110 Method: E200.8 Batch: R162369 Sample 10: LRB 15 Method Blank Run: ICPMS4-C_120724A 07/24/12 14:09 Arsenic NO mg/L 0.0050 Cadmium NO mg/L 0.00050 Chromium NO mg/L 0.020 Cobalt NO mg/L 0.010 Copper NO mg/L 0.010 Lead NO mg/L 0.0010 Manganese NO mg/L 0.010 Molybdenum NO mg/L 0.010 Nickel NO mg/L 0.020 Selenium NO mg/L 0.0050 Silver NO mg/L 0.010 Thallium NO mg/L 0.00050 Uranium NO mg/L 0.00030 Vanadium NO mg/L 0.010 Zinc NO mg/L 0.010 Sample 10: LFB 15 Laboratory Fortified Blank Run: ICPMS4-C_120724A 07/24/12 14:13 Arsenic 0.0524 mg/L 0.0010 105 85 115 Cadmium 0.0533 mg/L 0.0010 107 85 115 Chromium 0.0522 mg/L 0.0010 104 85 115 Cobalt 0.0537 mg/L 0.0010 107 85 115 Copper 0.0531 mg/L 0.0010 106 85 115 Lead 0.0511 mg/L 0.0010 102 85 115 Manganese 0.0536 mg/L 0.0010 107 85 115 Molybdenum 0.0520 mg/L 0.0010 104 85 115 Nickel 0.0528 mg/L 0.0010 106 85 115 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 39 of 54 EI'ERGY LABORATORIES """ www.ellOlZYlab.com r ' .. K,len.,.MT 817-412-0711 • Billings, MT 808-135-4489· Casper, WY 888-235-8515 .~~ AImlytJt;alExuJIBIWaSinu 1m J.E:".~~ ,~~J~iIf~fte, wy 86S .. 686-7U5 • Rapid Cfty, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: E200.8 Result Units Sample 10: LFB Selenium 15 Laboratory Fortified Blank Silver Thallium Uranium Vanadium Zinc Sample 10: C12070448-003BMS Arsenic Cadmium Chromium Cobalt Copper Lead Manganese Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc 0.0531 mg/L 0.0210 mg/L 0.0523 mg/L 0.0510 mg/L 0.0524 mg/L 0.0537 mg/L 15 Sample Matrix Spike 0.0531 mg/L 0.0466 mg/L 0.0524 mg/L 0.0490 mg/L 0.0469 0.0552 0.188 0.0558 0.0486 0.0510 0.0168 0.0526 0.0652 0.0543 0.0450 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample 10: C12070448-003BMSO 14 Sample Matrix Spike Duplicate Arsenic 0.0525 mg/L Cadmium 0.0457 mg/L Chromium 0.0523 mg/L Cobalt 0.0478 mg/L Copper Lead Manganese Molybdenum Nickel Silver Thallium Uranium Vanadium Zinc Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.0468 mg/L 0.0541 mg/L 0.185 mg/L 0.0548 mg/L 0.0485 mg/L 0.0162 mg/L 0.0515 mg/L 0.0630 mg/L 0.0543 mg/L 0.0447 mg/L RL %REC Low Limit High Limit 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 106 105 105 102 105 107 105 93 105 96 94 110 107 107 96 102 84 105 129 109 89 104 91 105 94 94 108 101 105 95 81 103 125 109 89 Run: ICPMS4-C_120724A 85 115 85 115 85 115 85 85 85 115 115 115 Run: ICPMS4-C_120724A 70 130 70 130 70 130 70 130 70 70 70 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 130 130 130 Run: ICPMS4-C_120724A 70 130 70 130 70 130 70 130 70 70 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 130 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 1.1 2.1 0.2 2.4 0.2 1.9 1.7 1.8 0.3 3.1 2.1 3.5 0.1 0.6 Batch: R162369 07/24/12 14:13 07/25/1207:1 9 07/25/12 07:42 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Page 40 of 54 EN:RGY LABORAT ORIES ,"" www.energyJab.com Ana~1 Ex~/SfI&IJ Sines 1,952 Helena, MT871-412-0711 • Billings, MT 800~735-4489 • Casper, WV 888 ... 235-0515 Gi!J~tte; 'Wy, 866-6~6~7175 • Rapid City, SI} 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: E200.8 Result Prepared by Casper, WY Branch Units RL %REC Low Limit Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C 12070448 High Limit RPO RPOLimit Qual Analytical Run: ICPMS4-C_120801A Sample 10: ICV 17 Initial Calibration Verification Standard 08/01/1210:16 Arsenic 0.0504 mg/L 0.0010 101 90 110 Beryllium 0.0516 mg/L 0.0010 103 90 110 Cadmium 0.0505 mg/L 0.0010 101 90 110 Chromium 0.0484 mg/L 0.0010 97 90 110 Cobalt 0.0514 mg/L 0.0010 103 90 110 Copper 0.0513 mg/L 0.0010 103 90 110 Lead 0.0491 mg/L 0.0010 98 90 110 Manganese 0.0504 mg/L 0.0010 101 90 110 Mercury 0.00512 mg/L 0.0010 102 90 110 Molybdenum 0.0466 mg/L 0.0010 93 90 110 Nickel 0.0507 mg/L 0.0010 101 90 110 Selenium 0.0531 mg/L 0.0010 106 90 110 Silver 0.0206 mg/L 0.0010 103 90 110 Thallium 0.0499 mg/L 0.0010 100 90 110 Uranium 0.0507 mg/L 0.00030 101 90 110 Vanadium 0.0479 mg/L 0.0010 96 90 110 Zinc 0.0518 mg/L 0.0010 104 90 110 Method: E200.8 Batch: R162678 Sample 10: LRB 17 Method Blank Run: ICPMS4-C_120801A 08/01/1210:52 Arsenic NO mg/L 0.0050 Beryllium NO mg/L 0.00050 Cadmium NO mg/L 0.00050 Chromium NO mg/L 0.020 Cobalt NO mg/L 0.010 Copper NO mg/L 0.010 Lead NO mg/L 0.0010 Manganese NO mg/L 0.010 Mercury NO mg/L 0.00050 Molybdenum NO mg/L 0.010 Nickel NO mg/L 0.020 Selenium NO mg/L 0.0050 Silver NO mg/L 0.010 Thallium NO mg/L 0.00050 Uranium NO mg/L 0.00030 Vanadium NO mg/L 0.010 Zinc NO mg/L 0.010 Sample 10: LFB 17 Laboratory Fortified Blank Run: ICPMS4-C_120801A 08/01/12 10:56 Arsenic 0.0518 mg/L 0.0010 103 85 115 Beryllium 0.0524 mg/L 0.0010 105 85 115 Cadmium 0.0518 mg/L 0.0010 104 85 115 Chromium 0.0503 mg/L 0.0010 101 85 115 Cobalt 0.0527 mg/L 0.0010 105 85 115 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 41 of 54 EI'ERGY LABORATORIES www.energylab.com Ana~1 ExI;8IIBfWIl Sines 1952 ,Heiena, MTB77-412-0711 • Billings,. MT 800-735-4489 • Casper, WY 888-235-0515 . ~ __ .:.~:¢iIl~tta, WY 866-686-7175 • Rapid Cfty, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: E200.8 Result Units Sample 10: LFB Copper 17 Laboratory Fortified Blank Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc Sample 10: C12070448-008BMS Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc 0.0522 mg/L 0.0510 mg/L 0.0524 mg/L 0.00502 mg/L 0.0476 mg/L 0.0519 mg/L 0.0515 mg/L 0.0206 mg/L 0.0520 mg/L 0.0514 mg/L 0.0494 mg/L 0.0544 mg/L 17 Sample Matrix Spike 0.0589 mg/L 0.0508 mg/L 0.0515 0.0560 0.0567 0.0532 0.0574 0.0590 0.00537 0.0554 0.0550 0,135 0.0165 0.0578 0.0692 0.0563 0.0538 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample 10: C12070448-008BMSO 17 Sample Matrix Spike Duplicate Arsenic 0.0573 mg/L Beryllium 0.0515 mg/L Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.0519 0.0544 0.0573 0.0515 0.0580 0.0588 0.00543 0.0563 0.0527 0.135 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L RL %REC Low Limit High Limit 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 104 102 105 100 95 104 103 103 104 103 99 109 117 102 103 112 112 106 115 118 107 104 108 119 83 115 121 112 107 114 103 104 109 113 103 116 117 109 105 103 118 Run: ICPMS4-C_120801A 85 115 85 115 85 85 85 85 85 85 85 85 85 85 115 115 115 115 115 115 115 115 115 115 Run: ICPMS4-C_120801A 70 130 70 130 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 Run: ICPMS4-C_120801A 70 130 70 130 70 70 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 130 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual 2.7 1.3 0.7 2.8 1.1 3.2 0.9 0.4 1.1 1.6 4.2 0.1 Batch: R162678 08/01/1210:56 08/01/1216:07 08/01/1216:12 20 20 20 20 20 20 20 20 20 20 20 20 Page 42 of 54 EN:RGY LABORATORIES www.energyJab.com Ana~/£X~lllNIca Sin~ 1952 .~elel1a. MT877"472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 _~iU~t:te, WY866~686-7175 • Rapid City, SI) 888-672-1225 • College station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: E200.8 Result Units Sample 10: C12070448-008BMSO 17 Sample Matrix Spike Duplicate Silver 0.0163 mg/L Thallium 0.0583 mg/L Uranium 0.0695 mg/L Vanadium 0.0547 mg/L Zinc 0.0518 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R162678 Run: ICPMS4-C_120801A 08/01/1216:12 0.0010 81 70 130 1.6 20 0.0010 116 70 130 0.8 20 0.00030 122 70 130 0.5 20 0.0010 109 70 130 2.9 20 0.0010 103 70 130 3.7 20 ND -Not detected at the reporting limit. Page 43 of 54 www.energylab.com Analyth;al Exf;SHIHWIl $inf;g 1952 ENaRGY LABORATORI ES ~ele'la, tdT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ., :GiUef;ts"Wf,S'&&-.G. 86;-7175 .• • Rapid City, Sf) 888-&72-1225 • College Station, 'IX 888-690-2218 ~ ~"~.": ~~",,.' ", ' '- QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N NO mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.56 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 1.85 mg/L Sample 10: C12070448-003CMS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 2.01 mg/L Sample 10: C12070448-003CMSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 2.03 mg/L Sample 10: C12070452-001CMS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 7.43 mg/L Sample 10: C12070452-001CMSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 7.38 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R161946 Run: TECHNICON_120716A 07/16/12 11 :07 0.10 Run: TECHNICON_120716A 07/16/12 11 :10 0.10 102 90 110 Run: TECHNICON_120716A 07/16/12 11 :12 0.10 94 90 110 Run: TECHNICON_120716A 07/16/12 11 :52 0.10 103 90 110 Run: TECHNICON_120716A 07/16/1211 :55 0.10 104 90 110 1.0 10 Run: TECHNICON_120716A 07/16/12 12:30 0.20 105 90 110 Run: TECHNICON_120716A 07/16/12 12:32 0.20 104 90 110 0.7 10 NO -Not detected at the reporting limit. Page 44 of 54 EI\ERGY LABORATORIES www.energylab.com Allalytit;al £X~8nIJflCB SiIJu 1152 Helena, MT877"472-0711 .. Billings, MT 800-735-4489 • Casper, WY 888-235-0515 W~$,fj-686 .. 7J75 It Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: E900.1 Sample 10: LCS-GA-0547 Gross Alpha minus Rn & U Sample 10: MB-GA-0547 Gross Alpha minus Rn & U Laboratory Control Sample 20.9 pCi/L 3 Method Blank -0.0401 Gross Alpha minus Rn & U Precision (±) 0.174 pCi/L pCi/L pCi/L Gross Alpha minus Rn & U MDC 0.314 Sample 10: C12070454-007GMS Gross Alpha minus Rn & U Sample 10: C12070454-007GMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Sample Matrix Spike 37.4 pCi/L Sample Matrix Spike Duplicate 38.8 pCi/L RL %REC Low Limit High Limit Run: G5000W_120717A 101 70 130 Run: G5000W_120717A Run: G5000W _1 20717 A 92 70 130 Run: G5000W _120717 A 94 70 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 3.7 Batch: GA-0547 08/08/1222:25 08/08/12 22:25 U 08/09/12 00:07 08/09/12 00:07 21.6 U -Not detected at minimum detectable concentration Page 45 of 54 EI\ERGY LABORATORIES www.energylab.com AnalytlcafExcsllSllCIl Sines 1152 -i) 'Hele~.a, MT877"472 ... 0711 • Billings. MT 800-735-4489-Casper,WV 888 ... 235-051 5 ,jm~!te, WY,.O_6"'_686.n75 " Rapid City, SO 888-672-1225 " College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: SW8260B Sample 10: 071812_LCS_ 4 16 Laboratory Control Sample Acetone 97 ug/L Benzene 9.3 ug/L Carbon tetrachloride 8.5 ug/L Chloroform 9.4 ug/L Chloromethane 8.9 ug/L m+p-Xylenes 19 ug/L Methyl ethyl ketone 98 ug/L Methylene chloride 10 ug/L Naphthalene 10 ug/L o-Xylene 10.0 ug/L Toluene 10 ug/L Xylenes, Total 29 ug/L Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Sample 10: 071812_MBLK_6 16 Method Blank Acetone NO ug/L Benzene NO ug/L Carbon tetrachloride NO ug/L Chloroform NO ug/L Chloromethane NO ug/L m+p-Xylenes NO ug/L Methyl ethyl ketone NO ug/L Methylene chloride NO ug/L Naphthalene NO ug/L o-Xylene NO ug/L Toluene NO ug/L Xylenes, Total NO ug/L Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: C12070337-004AMS 16 Sample Matrix Spike Acetone 1800 ug/L Benzene 170 ug/L Carbon tetrachloride 160 ug/L Chloroform 170 ug/L Chloromethane 160 ug/L m+p-Xylenes 330 ug/L Methyl ethyl ketone 1800 ug/L Methylene chloride 180 ug/L Naphthalene 160 ug/L RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R 162082 Run: SATURNCA_120718C 07/18/12 11 :07 20 97 70 130 1.0 93 70 130 1.0 85 70 130 1.0 94 70 130 1.0 89 70 130 1.0 94 70 130 20 98 70 130 1.0 101 70 130 1.0 102 70 130 1.0 100 70 130 1.0 101 70 130 1.0 96 70 130 1.0 106 80 120 1.0 86 70 130 1.0 87 80 130 1.0 104 80 120 Run: SATURNCA_120718C 07/18/12 12:20 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 98 80 120 1.0 88 70 130 1.0 79 80 120 S 1.0 96 80 120 Run: SATURNCA_120718C 07/18/12 18:50 200 88 70 130 10 87 70 130 10 81 70 130 10 84 70 130 10 80 70 130 10 82 70 130 200 90 70 130 10 90 70 130 10 80 70 130 ----."------_._-_._-----_._-----------------------._------_._._--_._-_ .. _---_._--------_._--------------------... _---.".-----------------_._------.----.. _--------_.---------------------"----------------_ .. _------_._----_. __ ._---._---_._--_ .. _-------------_._----_._-_._--_._--_._._-_._-----------_._-------------_._------_._--- Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 46 of 54 EI'-ERGY LABORATORI ES www.energylab.com AnatyticalExcsHsncll ~ 1952 Hel~!1a, MT87l·472-0711 • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 . i".J;'nt~tt~r WY.B,6S ... j86"7175 • Ra()ip City, SI) 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C 12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: SW8260B Result Units Sample 10: C12070337-004AMS o-Xylene 16 Sample Matrix Spike Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: C12070337-004AMSO Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Qualifiers: RL -Analyte reporting limit. 180 ug/L 170 ug/L 500 ug/L 16 Sample Matrix Spike Duplicate 2100 ug/L 190 ug/L 200 ug/L 190 ug/L 190 ug/L 380 ug/L 1900 ug/L 210 ug/L 200 ug/L 190 ug/L 180 ug/L 570 ug/L MDC -Minimum detectable concentration RL %REC Low Limit High Limit Run: SATURNCA_120718C 10 88 70 130 10 86 70 130 10 84 70 130 1.0 92 80 120 1.0 88 70 130 1.0 82 80 120 1.0 98 80 120 Run: SA TU RNCA_120718C 200 105 70 130 10 94 70 130 10 98 70 130 10 95 70 130 10 93 70 130 10 95 70 130 200 97 70 130 10 106 70 130 10 102 70 130 10 96 70 130 10 88 70 130 10 96 70 130 1.0 105 80 120 1.0 94 70 130 1.0 100 80 120 1.0 90 80 120 ND -Not detected at the reporting limit. R -RPD exceeds advisory limit. RPO RPOLimit Qual Batch: R162082 07/18/1218:50 07/18/12 19:26 18 20 7.5 20 19 20 12 20 14 20 15 20 7.7 20 16 20 25 20 R 8.2 20 2.3 20 13 20 0.0 10 0.0 10 0.0 10 0.0 10 Page 47 of 54 EN:RGY LABORATORIES www.energylab.com Analytical !xCIII/snell SiIlcs 1.152 Helen~, :MTS17:..412-0111 .. Billings. MT 800-735-4489 " Casper, WY 888-235-0515 .=, ,,~iJl~ti:e', WY,8'$' ... 86~7n5 • Rapi!f Cfty, Sf) 888-672-1225 .. College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: SW8260B Result Units Sample 10: C12070448-009EMS Acetone 16 Sample Matrix Spike Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 1400 ug/L 160 ug/L 150 ug/L 160 140 320 1600 170 170 160 160 480 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Sample 10: C12070448-009EMSO 16 Sample Matrix Spike Duplicate Acetone 1600 ug/L Benzene Carbon tetrachloride Chloroform Chlorom ethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Sample 10: 071912_LCS_7 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene Qualifiers: RL -Analyte reporting limit. 180 170 180 180 350 1800 190 190 180 180 540 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 16 Laboratory Control Sample 92 ug/L 8.8 ug/L 8.2 ug/L 8.5 ug/L 8.2 18 91 9.4 10 ug/L ug/L ug/L ug/L ug/L MDC -Minimum detectable concentration RL %REC Low Limit High Limit 200 10 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 200 10 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 72 79 75 78 71 80 82 84 86 82 78 80 98 87 85 95 82 90 84 92 88 89 89 96 94 92 90 90 92 87 88 93 92 88 82 85 82 91 91 94 101 Run: SATURNCA_120719A 70 130 70 130 70 130 70 70 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 130 130 120 130 120 120 Run : SATURNCA_120719A 70 130 70 70 70 70 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 130 130 130 130 120 130 120 120 Run: SATURNCA_120719A 70 130 70 130 70 130 70 130 70 70 70 70 70 130 130 130 130 130 NO -Not detected at the reporting limit. R -RPD exceeds advisory limit. RPO RPOLimit Qual 12 13 12 16 21 10 7.9 13 9.3 12 14 11 0.0 0.0 0.0 0.0 Batch: R162128 07/19/12 19:19 07/19/12 19:56 20 20 20 20 20 20 20 20 20 20 20 20 10 10 10 10 R 07/19/12 13:33 Page 48 of 54 EI'.ERGY LABORATORIES www.energyiab.com ANIyticaI ExCIIHBfWII SiJ1u 1952 ffelell3, Mt 877 .. 412-0711 • Billings, MY 800-735-4489 • Casper, WY 888-235-0515 ,jdiile~e:rW~_a6$-686~7n5 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: SW8260B Prepared by Casper, WY Branch Result Units RL %REC Low Limit Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C 12070448 High Limit RPO RPOLimit Qual Batch: R162128 Sample 10: 071912_LCS_7 16 Laboratory Control Sample Run: SATURNCA_120719A 07/19/12 13:33 o-Xylene 9.3 ug/L 1.0 93 70 130 Toluene 9.0 ug/L 1.0 90 70 130 Xylenes, Total 27 ug/L 1.0 92 70 130 Surr: 1,2-0ichlorobenzene-d4 1.0 104 80 120 Surr: Oibromofluoromethane 1.0 88 70 130 Surr: p-Bromofluorobenzene 1.0 88 80 130 Surr: T oluene-d8 1.0 101 80 120 Sample 10: 071912_MBLK_9 16 Method Blank Run: SATURNCA_120719A 07/19/12 14:47 Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 o-Xylene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1,2-0ichlorobenzene-d4 1.0 99 80 120 Surr: Oibromofluoromethane 1.0 86 70 130 Surr: p-Bromofluorobenzene 1.0 81 80 120 Surr: T oluene-d8 1.0 98 80 120 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 49 of 54 EN:RGY LABORATORI ES www.energylab.com Analytical ExQlllsncB $IRes 7952 Hefena, MT'B77-472-0711 • BUlings, MT 800-735-4489 • Casper, W'f 888-235-0515 . ",-.~illette, Wy866~6B6 .. 7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: SW8260B Result Units Sample 10: C12070468-001 EMS Acetone 16 Sample Matrix Spike Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 1400 ug/L 180 ug/L 170 ug/L 180 ug/L 180 ug/L 380 ug/L 1600 ug/L 180 190 190 180 580 ug/L ug/L ug/L ug/L ug/L Sample 10: C12070468-001 EMSO 16 Sample Matrix Spike Duplicate Acetone 1400 ug/L Benzene 160 ug/L Carbon tetrachloride 170 ug/L Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: 072312_LCS_4 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene Qualifiers: RL -Analyte reporting limit. 160 180 340 1500 170 170 170 170 510 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 16 Laboratory Control Sample 91 ug/L 8.6 ug/L 7.9 ug/L 8.4 ug/L 8.9 ug/L 17 ug/L 97 ug/L 9.5 ug/L 9.2 ug/L MDC -Minimum detectable concentration RL %REC Low Limit High Limit 200 10 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 200 10 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 69 91 84 90 92 96 79 92 93 96 88 96 98 88 91 96 68 82 83 80 91 85 73 87 86 86 83 85 98 87 86 95 91 86 79 84 89 83 97 95 92 Run: SATURNCA_120723B 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 70 70 70 70 80 70 80 80 130 130 130 130 130 120 130 120 120 Run: SATURNCA_120723B 70 130 70 130 70 130 70 70 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 130 130 120 130 120 120 . Run: SATURNCA_120723B 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. RPO RPOLimit Qual 1.7 11 1.0 12 1.3 12 7.9 5.4 8.0 11 6.1 12 0.0 0.0 0.0 0.0 Batch: R162289 07/23/1221 :14 S 07/23/1221 :50 20 S 20 20 20 20 20 20 20 20 20 20 20 10 10 10 10 07/23/12 13:08 Page 50 of 54 E~RGY LABORATORIES www.energyJab.com Ana~1 ExeslJBflCB Sines '952 ~elena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 -.~illeft:~, Wy _866-~86-1l75 • Rapid Ctty, SD 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 08/10/12 Report Date: 08/09/12 Work Order: C12070448 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Method: SW8260B Result Units Sample 10: 072312_LCS_ 4 16 Laboratory Control Sample o-Xylene 8.7 ug/L Toluene 8.4 ug/L Xylenes, Total 25 ug/L Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane . Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: 072312_MBLK_6 16 Method Blank Acetone NO ug/L Benzene NO ug/L Carbon tetrachloride NO ug/L Chloroform NO ug/L Chloromethane NO ug/L m+p-Xylenes NO ug/L Methyl ethyl ketone NO ug/L Methylene chloride NO ug/L Naphthalene NO ug/L o-Xylene NO ug/L Toluene NO ug/L Xylenes, Total NO ug/L Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Qualifiers: RL -Analyte reporting limit. MOC - Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R 162289 Run: SATURNCA_120723B 07/23/12 13:08 1.0 87 70 130 1.0 84 70 130 1.0 85 70 130 1.0 100 80 120 1.0 88 70 130 1.0 82 80 130 1.0 95 80 120 Run: SATURNCA_ 120723B 07/23/12 14:21 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 94 80 120 1.0 84 70 130 1.0 78 80 120 S 1.0 94 80 120 NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 51 of 54 EN:RGY LABORATORIES www.energylab.com Analytical ExuIIBllCf Sines 1952 Helena,MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 >" :~iIIe~~,wy 86&~686~7175 • Rapid City, Si1888-672-1225 • College Station, IX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, a" samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Denison Mines USA Corp Login completed by: Kathryn (Kate) L. Miller Reviewed by: BL2000\kschroeder Reviewed Date: 7/18/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? A" samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.0"C On Ice Yes 0 Yes 0 C12070448 Date Received: 7/13/2012 Received by: dw Carrier FedEx name: No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0 No VOA vials submitted D Not Applicable D Page 52 of 54 EN:RGY mJ Chain of Custody and Analytical Request Record page~of~ --------,--~ ~ -------------~ -------~ ---- Company Name: D . M;(1 c:,-S Project Name, PWS, Permit, Etc. Sample Origin EPNState Compliance: , e"I~0(l ~ra o.v..o.rter (!""rC'~nJ. w{"~h:,,r :2.0 i.1.. State: lXT" Yes ~ No 0 Report Mail Address: Contact Name: Phone/Fax: Email: Sampler: (Please Print) p~ BC"X 8C1 ~'\C\'t1,1, ¥lc.\ \.-\, 84511 Cr-C\(1'" i" Pc\ll'Y)er Y3S b7 g :2.-2. 2.! ·-r:;:~t1c:.r He it't;\aj Invoice Addre~: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: _S~'fV)e O('.\I'c.:\ ·.,-v.r \( .. .J .... !) I.."~ ~ ,) ~ /~ 21:21 Special Report/Formats: $: ~[S )7~O@ [llirn@llD~§[Q) .. Contact ELI prior to ~:ed~ £ Cl .... RUSH sample submittal ~o (/)J!. for charges and Cooler"1b(s): <lJ -0-.... j::' R scheduling -See C-Ij~ c:al=OI.s 0 ~ '-> 0 >-ro W Instruction Page o OW 0 EDD/EDT(Electronic Data) ~C/)~ ~ 3: 0 J: "C o POTWIWWTP Format: o$:= ro 0) T U c: Comments: ReeeiptTemp U «~I.Q ~ :::J U 1..0 ~ <: 0 °c o State: 0 LEVEL IV '0 ,-£01 c ~ ~ "-Qj~ C'L: -~ I-ea -~ o..rol,£ 0 '..) c: D Other: 0 NELAC ~ l.-On Ice: (Y')N E~ro I r-:::J ;:, Q,).!:::!i> 3; ~ ~ l-S ZCi.<X:1 aro LU "E Custody Seal ~ ~ >1 W ro On Bottle N '}) ~ 5 en '0 On Cooler N C/) .. ~ c ea oJ .~ US H Intact y SAMPLE IDENTIFICATION Collection Collection "5 \.., \- MATRIX () ~ 'r~ Signature y (Name, Location, Interval, etc.) Date Time Match 1 MVJ-:lq_OlI0~Cl&.l. 1hc/1A 134~ )-w '/.. I~ 2,\\W" 3:l_C70'1.20\;1... 7/:l, II')... \'3'5 )·-w )( I~ 3 t .. ~ Vv -11-07 \ I ~c -il 7/'1/)~ 1;2.10 b··~vJ )( \9J Innn 4 7!1J/L'l.. 123:=, b'~VV )( ~ /vl W -1L.i _ t.71 , ~O i.l. 5 l5 7/)C/11.. "W )( ~ /,\vJ-';I __ C71C~GI1. \.2"1.0 ~-~ 6 fv'W -:t~~.C711 '1.012 7/i1/L~ CC1S) b-vJ 'X ~ 7 /~l y-J-30-(;7 iC'2C '.l... -, ,. ~/~:l... 1100 br-W )( I~' r71)1di'iK i.' Ie I· 8/';1 vJ -3" _C70t]'J4)i;l. 7/1h~ l ·3:.~S b--W X I~ 9 /v\VV-35_C7IC~C,~ 1,/lC/12 )410 ~--w X ~ I 1~1\i1 W -3G:" (",11;2.0 \ ~ 7/) "/l~ 0'1/5 b-W IX I~ I Custody Relinquished b~rint): DatelTime: Signature: Received by (print): DatelTime: Signa ure: rr:,t)t\~.r 'wl1:(\,,~ 7/)2/2(;\2 Cr,(,.--I\ :)"'IlN~ ,L/.;/d.:,L-Record RelinqUished by (print): 0 DatelTime: Signature: ... Received by (print): DatefTime: Signature: MUST be Signed Il~ Dy L3D07Jn DatelTlme: I ~ ':) 'ne~D Sample Disposal: Return to Client: Lab Disposal: ( , 1 .. ~~-...~ ~-J -:/ In certain circumstances. samples submitted to Energy Laboratories, Inc. may be sUbcontract~~~ther certified laboratories in order to complete the analysis requested. This serves as notice of this Dossibilitv. All sub-contract data will learlv notated on your analvtical report. \Ii<>it ru,r ,.,on C!it.:.::.t ".IIA/W pnprovl::th.com for additional information. downloadable fee schedule, forms, and links. EI\ERGY ~'" ua.fI Chain of Custody and Analytical Request Record Page~of Q.., ----~---... ----... ----, ... -.. ---.. .....-.......... --..... -----.. ---..... ------... , Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: State: Yes 0 No 0 Report Mail Address: ./ Contact Name: Phone/Fax: Email: Sampler: (Please Print) ~<Ar he . (.\S PCildp J Invoice Address: Invoice Contact & Phone: "J Purchase Order: Quote/Bottle Order: Special Report/Formats: ~ &~~ '\1@U® oo(g@QJJ~rn[Q) • Contact ELI prior to sF:;;;,~£ 0 .... RUSH sample submittal ~OCl)~ ~ for charges and CoolerlD(s): ~m~OI <i> ~ 0 R scheduling -See GI;~ ._> 0 >.10 W t-I nstruction Page Dow D EDD/EDT(Electronic Data) ~en~ ms: :r: --03:= ~ 0) '0 Receipt Temp DpOTWIWWTP Format: u 0oe: ~ U c: Comments: :l U "'.0 ...... <enl.-32 \} « e °c o State: o LEVEL IV o .... COI c •• (I) c:--r-m .... 8:ro.2 0 c o Other: o NELAC ~~Iro I ~ ~ :J On Ice: (SN ~ (I).:: a; ~ t-5 zo.<Ig>Cl '#. W "E Custody Seat ~ ~ >1 W m On Bottle N -C en .;,) (/) C On Cooler Y N ~ .m H Intact Y N G (J) SAMPLE IDENTIFICATION Collection Collection MATRIX Signature Y N (Name, Location, Interval, etc.) Date Time Match 1 Jv\W-~,_07H 10".2 7 III /J.2.. 095i f --wW )( ~ 2~\O 'F,)~t\k {Dlt2;. ·~/d/·~ ( t · I .~ I~ 3 I ~ Ii 1lQ) ·1?-mn' .Jt\ flnn 4 y '-' I~ ,~ 5 I~ ~ 6 ~ 7 ~(~l1D7d1"tk I 8 ~ I 0) 9 l~ I 10 1t::JJ I Custody Relinquished by \t~~ . J. OatelTime: Signature: d.~ Received by (print): DatelTime: Signature: '~N,\~ ,i L dl.\ ~ ·7/r1./'2.0 U V ~C() :-\ JUf4~~ r-l' Record Relinquished by (print): ...,j DatelTime: "Signature: J Received by (print): DatelTime: Signature: MUST be Signed ~e~v;a :Y,L37r(f; , Uatefllme: ,_ ,/~ t} ~J"rJre2-,< Sample Disposal: Return to Client: Lab Disposal: .... ..... --/ . .. --- \li",i ..... , ... u /Qh cito :::It www A",,'!mvl~h.c()m for additional information. downloadable fee schedule, forms, and links. r - EI\ERGY LABORATORIES www.energylab.com Analytical Excsllsm:s Sim;g 1952 Helena, MT 877~472~0711 • Billings, MT 800 .. 735-4489 • Casper, WY 888-235-0515 ~il/~ffe,WY US .. &B6 .. 7175 • Rapid City, SI} 888-672-1225 • College Station, TX 888 ... 690-2218 ANALYTICAL SUMMARY REPORT August 14, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12070741 Quote 10: C1640 -POC Wells Project Name: 3rd Quarter Groundwater 2012 Energy Laboratories, Inc. Casper WY received the following 14 samples for Denison Mines USA Corp on 7/20/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12070741-001 MW-02_07162012 07/16/12 12:45 07/20/12 Aqueous Gross Alpha minus Rn222 and Uranium C 12070741-002 MW-03_07182012 07/18/129:55 07/20/12 Aqueous Fluoride Metals by ICP-MS, Dissolved C 12070741-003 MW-03A_07192012 07/19/127:00 07/20/12 Aqueous E300.0 Anions Metals by ICP-MS, Dissolved Solids, Total Dissolved C 12070741-004 MW-05_07162012 07/16/12 14:55 07/20/12 Aqueous Metals by ICP-MS, Dissolved C 12070741-005 MW-12_07172012 07/17/12 9:40 07/20/12 Aqueous Same As Above C 12070741-006 MW-15_07172012 07/17/1210:50 07/20/12 Aqueous Metals by ICP, Dissolved Metals by ICP-MS, Dissolved C 12070741-007 MW-18_07182012 07/18/12 13:15 07/20/12 Aqueous E300.0 Anions Metals by ICP-MS, Dissolved Solids, Total Dissolved C 12070741-008 MW-19_07192012 07/19/128:00 07/20/12 Aqueous Nitrogen, Nitrate + Nitrite C 12070741-009 MW-70_07182012 07/18/129:55 07/20/12 Aqueous Fluoride Metals by ICP-MS, Dissolved C12070741-010 MW-23_07172012 07/17/127:32 07/20/12 Aqueous Metals by ICP-MS, Dissolved C12070741-011 MW-24_07182012 07/18/126:30 07/20/12 Aqueous Same As Above C12070741-012 MW-27 _07162012 07/16/12 11 :15 07/20/12 Aqueous E300.0 Anions Nitrogen, Nitrate + Nitrite Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved C12070741-013 MW-28_07162012 07/16/12 10:35 07/20/12 Aqueous E300.0 Anions C12070741-014 Temp Blank 07/19/12 0:00 07/20/12 Aqueous Temperature ------------------------------._----_._--------------------------------------------------------------- The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601 , unless ot~erwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~D LJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.08.1412:04:16 -06:00 Page 1 of 27 I www.energylab.com H.elena, MT 877 .. 472 .. 0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Analytical Excsllsncs Sines 1952 so 888-672-1225 • IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Report Date: 08/14/12 Sample Delivery Group: C12070741 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 27 EN:RGY LABORATORIES www.energylab.com Analytical ExesllsncB Sines 1952 Helena, MT877-472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 ,~inette, ~y 866.;686-7175 • Rapid CIty, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 08/14/12 Project: 3rd Quarter Groundwater 2012 Work Order: C12070741 Analyte Count Result Units R.L %REC Low Limit High Limit RPO RPOLimit Qual Method: A2540 C Batch: TDS120723A Sample 10: MB-1_120723A Method Blank Run: BAL-1_120723A 07/23/1208:22 Solids, Total Dissolved TDS @ 180 C NO mg/L 10 Sample 10: LCS-2_120723A Laboratory Control Sample Run: BAL-1_120723A 07/23/1208:22 Solids, Total Dissolved TDS @ 180 C 1100 mg/L 10 99 90 110 Sample 10: C12070741-003A OUP Sample Duplicate Run: BAL-1 120723A 07/23/12 09:20 Solids, Total Dissolved TDS @ 180 C 5880 mg/L 10 2.7 5 Sample 10: C12070741-007A MS Sample Matrix Spike Run: BAL -1_120723A 07/23/1209:20 Solids, Total Dissolved TDS @ 180 C 7300 mg/L 10 102 90 110 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 17 of 27 EN:RGY L ABORATORIES www.energylab.com Analytical ExCSUsnCB Sines 1952 Helen~, MT 877 .. 472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 _~illette, 'NY 86&-&86-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4500-F C Sample 10: MBLK Fluoride Sample 10: LCS-6892 Fluoride Sample 10: C12070726-001 AMS Fluoride Sample 10: C12070726-001 AMSO Fluoride Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank NO mg/L Laboratory Control Sample 1.89 mg/L Sample Matrix Spike 6.44 mg/L Sample Matrix Spike Duplicate 6.56 mg/L Report Date: Work Order: RL O/OREC Low Limit High Limit RPO Run: MANTECH_120723A 0.10 Run: MANTECH_120723A 0.10 92 90 110 Run: MANTECH 120723A - 0.10 98 80 120 Run: MANTECH_120723A 0.10 104 80 120 1.8 NO -Not detected at the reporting limit. 08/14/12 C12070741 RPOLimit Qual Batch: R 162238 07/23/1208:31 07/23/1208:35 07/23/12 12:12 07/23/12 12:16 10 Page 18 of 27 EI'ERGY www.energylab.com Analytical ExCl1//sn&B Sinu 1952 " " ,}Ie!ena, Mr'811~472-0711 • Bming~, MT 800-735-4489 • Casper, WY 888-235-0515 ,9.fn~ff¢l' Wv866"Q86-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888 .. 690-2218 LABORATORIES QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Report Date: 08/14/12 Work Order: C12070741 Analyte Count Result Units RL %REC Low Limit High Limit Method: E200.7 Sample 10: ICV Iron Initial Calibration Verification Standard Sample 10: ICSA Iron Sample 10: ICSAB Iron Method: E200.7 Sample 10: MB-120723A Iron Sample 10: LFB-120723A Iron Sample 10: C12070662-001 BMS2 Iron Sample 10: C12070662-001 BMSO Iron Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 5.15 mg/L Interference Check Sample A 185 mg/L Interference Check Sample AB 185 mg/L Method Blank ND mg/L Laboratory Fortified Blank 0.906 mg/L Sample Matrix Spike 46.1 mg/L Sample Matrix Spike Duplicate 46.8 mg/L 0.030 103 95 105 0.030 93 80 120 0.030 93 80 120 Run: ICP2-C_120723A 0.030 Run: ICP2-C_120723A 0.030 90 85 115 Run: ICP2-C_120723A 0.064 90 70 130 Run: ICP2-C_120723A 0.064 92 70 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual Analytical Run: ICP2-C_120723A 07/23/12 11 :35 07/23/12 12:15 07/23/12 12:19 Batch: R162266 07/23/12 12:39 07/23/12 12:43 07/23/12 16:45 07/23/12 16:49 1.6 20 Page 19 of 27 E~RGY www.energylab.com , 'Helena, Mt 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 LABORATORIES Analytical ExC8lJSflCB Sines 1952 :Giile,ttslWY 8&6~686-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Report Date: 08/14/12 Work Order: C 12070741 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.8 Sample 10: ICV Cadmium Selenium Thallium Uranium Method: E200.8 Sample 10: LRB Cadmium Selenium Thallium Uranium Sample 10: LFB Cadmium Selenium Thallium Uranium Sample 10: C12070456-007CMS4 Cadmium Selenium Thallium Uranium Sample 10: C12070456-007CMSO Cadmium Selenium Thallium Uranium Method: E200.8 Sample 10: ICV Thallium Method: E200.8 Sample 10: LRB Thallium Sample 10: LFB Thallium Sample 10: C12070971-006CMS4 Thallium Sample 10: C12070971-006CMSO Thallium Qualifiers: 4 Initial Calibration Verification Standard 4 4 4 0.0519 mg/L 0.0010 0.0513 mg/L 0.0513 mg/L 0.0517 mg/L Method Blank ND mg/L ND mg/L ND mg/L ND mg/L Laboratory Fortified Blank 0.0522 mg/L 0.0534 mg/L 0.0520 mg/L 0.0520 mg/L Sample Matrix Spike 0.0470 mg/L 0.0550 mg/L 0.0572 mg/L 0.0706 mg/L 0.0010 0.0010 0.00030 0.00050 0.0050 0.00050 0.00030 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.00050 0.00030 4 Sample Matrix Spike Duplicate 0.0449 mg/L 0.0010 0.0507 mg/L 0.0010 0.0553 mg/L 0.00050 0.0685 mg/L 0.00030 Initial Calibration Verification Standard 0.0514 mg/L 0.0010 Method Blank ND mg/L 0.00050 Laboratory Fortified Blank 0.0514 mg/L 0.0010 Sample Matrix Spike 0.0531 mg/L 0.00050 Sample Matrix Spike Duplicate 0.0524 mg/L 0.00050 104 103 103 103 104 107 104 104 94 110 114 119 90 101 111 115 103 103 106 Analytical Run: ICPMS4-C_120805A 90 110 90 110 90 110 90 110 Run: ICPMS4-C_120805A Run: ICPMS4-C_120805A 85 115 85 115 85 115 85 115 Run: ICPMS4-C 120805A - 70 130 70 130 70 130 70 130 Run: ICPMS4-C_120805A 70 130 70 130 70 130 70 130 4.5 8.1 3.3 3.0 08/05/12 00:45 Batch: R 162835 08/05/12 01 :20 08/05/12 01 :25 08/05/12 14:53 08/05/1214:57 20 20 20 20 Analytical Run: ICPMS4-C_120806A 08/06/12 11 :36 90 110 Run: ICPMS4-C_120806A Run: ICPMS4-C_120806A 85 115 Run: ICPMS4-C_120806A 70 130 Run: ICPMS4-C_120806A Batch: R 162953 08/06/12 12:17 08/06/12 12:21 08/07/12 14:58 105 70 130 1.3 08/07/12 15:02 20 RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 20 of 27 EN:RGY www.energylab.com Helena, Mt 877-472-071 t • Billings, MT 800 .. 735~44B9 • Casper, WY 888-235-0515 billetie,!NY 866 .. 686-7115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORIES Analytical ExcsIJSfI&1I Sines 1952 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Report Date: 08/14/12 Work Order: C12070741 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.8 Sample 10: ICV Manganese Method: E200.8 Sample 10: LRB Manganese Sample 10: LFB Manganese Sample 10: C12080099-027BMS4 Manganese Sample 10: C12080099-027BMSO Manganese Method: E200.8 Sample 10: ICV Selenium Method: E200.8 Sample 10: LRB Selenium Sample 10: LFB Selenium Sample 10: C12070781-001 BMS4 Selenium Sample 10: C12070781-001 BMSO Selenium Initial Calibration Verification Standard 0.0506 mg/L 0.0010 Method Blank NO mg/L 0.0010 Laboratory Fortified Blank 0.0529 mg/L 0.0010 Sample Matrix Spike 0.446 mg/L 0.0010 Sample Matrix Spike Duplicate 0.446 mg/L 0.0010 Initial Calibration Verification Standard 0.0524 mg/L 0.0010 Method Blank NO mg/L 0.0050 Laboratory Fortified Blank 0.0535 mg/L 0.0010 Sample Matrix Spike 0.0502 mg/L 0.0010 Sample Matrix Spike Duplicate 0.0516 mg/L 0.0010 101 Analytical Run: ICPMS4-C_120809A 08/09/12 10:18 90 110 Run: ICPMS4-C_1 20809A Run: ICPMS4-C_120809A Batch: R1631 00 08/09/12 10:53 08/09/12 10:58 106 85 115 Run: ICPMS4-C_120809A 70 130 Run: ICPMS4-C_120809A 70 130 0.0 08/10/1203:42 A 08/10/1203:46 20 A Analytical Run: ICPMS4-C_120813A 08/13/12 11 :46 105 90 110 Run: ICPMS4-C_1 20813A Run: ICPMS4-C_120813A 107 85 115 Run: ICPMS4-C_120813A 100 70 130 Run: ICPMS4-C_120813A 103 70 130 2.7 Batch: R163189 08/13/12 12:21 08/13/12 12:26 08/13/12 12:39 08/13/12 12:44 20 ------------------------------------------------------ Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. A -The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. MDC -Minimum detectable concentration Page 21 of 27 EI\ERGY LABORATORIES www.energylab.com Analytical Excslhmcil Sim:8 1952 Helena, MlB77-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ... ~iUefte, WY 8&&-.86-7175 • Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Report Date: 08/14/12 Work Order: C12070741 Analyte Count Result Units RL %REC Low Limit High Limit Method: E300.0 Sample 10: ICV-072S1 2-10 Chloride Sulfate Method: E300.0 Sample 10: ICB-072S1 2-11 Chloride Sulfate Sample 10: LFB-072S12-13 Chloride Sulfate Sample 10 : LFBO-072S12-1 4 Chloride Sulfate Sample 10: C12070713-01 3AMS Chloride Sulfate Sample 10: C1207071 3-013AMSO Chloride Sulfate Method: E300.0 Sample 10 : ICV-072712-10 Chloride Method: E300.0 Sample 10 : ICB-07271 2-11 Chloride Sample 10: LFB-072712-12 Chloride Sample 10: C12070800-002AMS Chloride Sample 10: C12070800-002AMSO Chloride Qualifiers: RL -Analyte reporting limit. 2 2 2 2 2 2 MDC -Minimum detectable concentration Initial Calibration Verification Standard 9.85 mg/L 1.0 98 90 110 40.3 mg/L 1.0 101 90 110 Method Blank Run: IC1-C_120725A ND mg/L 1.0 ND mg/L 20 Laboratory Fortified Blank Run: IC1-C_120725A 9.77 mg/L 1.0 98 90 110 40.1 mg/L 1.0 100 90 110 Laboratory Fortified Blank Duplicate Run: IC1-C -120725A 9.92 mg/L 1.0 99 90 110 40.9 mg/L 1.0 102 90 110 Sample Matrix Spike Run: IC1-C -120725A 239 mg/L 4.2 98 90 110 3220 mg/L 17 104 90 110 Sample Matrix Spike Duplicate Run: IC1 -C -120725A 241 mg/L 4.2 99 90 110 3210 mg/L 17 102 90 110 Initial Calibration Verification Standard 9.04 mg/L 1.0 90 90 110 Method Blank Run: IC1-C_120727A ND mg/L 1.0 Laboratory Fortified Blank Run: IC1-C_120727A 9.08 mg/L 1.0 91 90 110 Sample Matrix Spike Run: IC1-C -120727A 389 mg/L 2.1 97 90 110 Sample Matrix Spike Duplicate Run: IC1-C_120727A 382 mg/L 2.1 91 90 110 ND -Not detected at the reporting limit. RPO RPOLimit Qual Analytical Run: IC1-C_120725A 07/25/12 15:04 Batch: R 162404 07/25/12 15:22 07/25/12 15:57 07/25/12 16:14 07/25/1220:53 07/25/1221 :10 1.1 10 0.4 10 Analytical Run: IC1-C_120727A 07/27/12 10:32 Batch: R162492 07/27/12 10:49 07/27/12 11 :07 07/27/12 12:16 07/27/12 12:34 1.7 10 Page 22 of 27 EI'ERGY LABORATORIES www.energylab.com Analytical ExCS/JsnCfI SinCJl1952 ~elena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 . ,~illeti:e,wy_866-6B6-7175 • Rapid City, SO 888-&72-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 08/14/12 Project: 3rd Quarter Groundwater 2012 Work Order: C12070741 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E353.2 Batch: R162361 Sample 10: MBLK-1 Method Blank Run: TECHNICON_120725A 07/25/12 11 :34 Nitrogen, Nitrate+Nitrite as N NO mg/L 0.20 Sample 10: LCS-2 Laboratory Control Sample Run: TECHNICON_120725A 07/25/12 11 :37 Nitrogen, Nitrate+Nitrite as N 2.49 mg/L 0.10 100 90 110 Sample 10: LFB-3 Laboratory Fortified Blank Run: TECHNICON_120725A 07/25/12 11 :39 Nitrogen, Nitrate+Nitrite as N 2.12 mg/L 0.10 108 90 110 Sample 10: C12070741-012CMS Sample Matrix Spike Run: TECHNICON_120725A 07/25/12 14:44 Nitrogen, Nitrate+Nitrite as N 17.2 mg/L 0.50 108 90 110 Sample 10: C12070741-012CMSO Sample Matrix Spike Duplicate Run: TECHNICON_120725A 07/25/12 14:47 Nitrogen, Nitrate+Nitrite as N 17.2 mg/L 0.50 108 90 110 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 23 of 27 EI\ERGY LABORATORIES www.energylab.com Analytical ExcsHsnCB Sines 1952 Helena, MT 877-472-071 t • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 . =.~ 5: ~ .~iIlette, wy 86&-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: E900.1 Sample 10: LCS-GA-0551 Gross Alpha minus Rn & U Sample 10: MB-GA-0551 Gross Alpha minus Rn & U Laboratory Control Sample 22.4 pC ilL 3 Method 81ank 0.126 Gross Alpha minus Rn & U Precision (±) 0.144 pC ilL pC ilL pC ilL Gross Alpha minus Rn & U MDC 0.212 Sample 10: C12070710-006GMS Gross Alpha minus Rn & U Sample 10: C12070710-006GMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Sample Matrix Spike 42.0 pC ilL Sample Matrix Spike Duplicate 44.7 pC ilL Report Date: 08/14/12 Work Order: C12070741 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: 8ERTHOLD 770-2_1207238 109 70 130 Run: 8ERTHOLD 770-2_1207238 Run: 8ERTHOLD 770-2_1207238 100 70 130 Run: 8ERTHOLD 770-2_1207238 104 70 130 6.1 NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration 8atch: GA-0558 08/01/1209:30 08/01/1209:30 U 08/01/1213:12 08/01/1213:12 19.2 Page 24 of 27 EN:RGY LABORATORIES ~..www.energylab.com ~ Allllyf:lcal ExcBJlsoCliSincs 1952 Heiena, MT 877-472-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ilIe~e1 Wy'866-686-71l5 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Den ison Mines USA Corp Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 7/24/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Yes [{1 Yes [{1 Yes D Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 1.6OC On Ice Yes D Yes [{1 C12070741 Date Received: 7/20/2012 Received by: th No D No D No D No D No D No D No D No D No D No D No D No D Carrier FedEx name: Not Present D Not Present D Not Present [{1 No VOA vials submitted [{1 Not Applicable D Page 25 of 27 "U Q) o ct> I\) (j) o -I\) -.....J EI\ERGY ~,'-,~ ~ Chain of Custody and Analytical Request Record Page --L-of ~ Company Name: '0"'" jJ.: ,,~S e.nI.S()ft Report Mail Address: Po 130)(' gOq B\OJ1d.;~ Ul gyS}\ I nvoice Address: SC\m£ Special Report/Formats: DoW D EDD/EDT(Electronic Data) o POTWNVWTP Format:. ___ _ o State: D LEVEL IV o Other: ----D NELAC 2 ---- SAMPLE IDENTIFICATION (Name, Location, Interval, etc.) Mw-0:1._0-' \b2.0 \:1. MW-03_ (7)8;t61:2,. 3MvJ"03A_01}q~ot~ 4 N.W-OS_QJ16201~ 5 MW -12... 67 \7.20 1~ 6MW -l5 _ 07 \7 :;;"0 \2 7 MW"'I~-071~~\~ 8M W-\Q ... Ol ~~O\~ 9rJ\W-iD_Cl}g2D l:l.. 12...........L. fO\n-""'(7 Custody Relinquished b¥ (prin:): R d -r:. \ ecor Relinquished by (print): Collection Date __ 7/](.JJ~ 7/IKJj~ Collection Time 12.l.{~ o't~S "7/ r'\ Ie.. I 6700 7lJiJl~ I l'1SS 1/17/1':2... loq'10 11171 r:L 110'!)O 1711YJbl. 1135 tJiB!J2. 10lSOO 1711&LJ::t I 095S PLEASE PRI NT (Provide as much information as possible.) Project Name, PWS, Permit, Etc. I Sample Origin :./~ QWJ-rt~r &ro,""",tl WO-+t..r 2.0 l:t State: u,..,- EPA/State Compliance: Yes iii No 0 Contact Name: Phone/Fax: Cre-.. ff' \ f\ 'P ("'Mtr \.r:~.S b'" () ::D.:::2.1 InVOice Contact & Phone: D",-v~~ ~~ Y3S ~7~ ZZ2.\ ~ &rm&[b W@O@ OO[g®M§@l?@:@ o L... ~O(J)~ 2;!cc;GOI Q5 ._> 0 >-m Bt'"Cfl ro:> C:"'''en (J):> O~= ~ 0> U<~I.Q·= '0 ~CCI-E ~ Q,i-S c: 'C ~~I·go E~> ro I ;:, <I,).!:: 1i:) s: Za.<tl~a ~ >1 (/) MATRIX \ .. w ~-vJ 2-W I-wi l-W l-W' ~-w \-vv ;L.-vJ ti I~ 1/\ Xl 1'X1~ -r-----r-r I '/. x )< X 11< 1 I IX x ~ l-x I' Received by (print): Received by (print): [ "0 c: :::l e ro c: \,., :::l I- "E ro "0 c t5 Email: Sampler: (Please Print) ~rlll~r Ho" ... A~'f Purchase Order: Quote/Bottle Order: .. R u 5 H DatefTime: DatefTime: Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page Comments: cl~~-d-' ReceiptT ernp l,fo °c On Ice: (j) N Custody Seal On Bottle Y N On Cooler Intact Signature Match I~ I~ ~ ~ I'=' ,~ tgs; (9) ~ ~ ~ 51 I~ v): ( V N ....., l~o74.{ Signafure: Signature: MUSTbe~------------------------------~~~~~~ __ ~~ __ ~ ____ ~~ ______ ~ Signed Sample Dispo~ Return to Client: Lab Disposal: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to othet. certkied laboratories in order to co~plete the analysis requested, This serves as notice of this possibility. All sub-contract data will be clearl~ated on your analytical report. \/idt nllr WAh ~itA::Jt www.eneravlab.com for additional information. downloadable fee schedule, forms, and links. "'U Ol :c (1) I\.) -.....I o -I\.) -.....I EI\ERGY , . .. --... _--m2 Chain of Custody and Analytical Request Record Page 2 Of~ ---... -...... ,. ------... __ ••.... _ ..... __ ._ .. ---.... _ ......... _ • ....r., Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: / State: Yes 0 No 0 Report Mail Address: ~ Contact Name: 0-Shon~~ Elnail: Sampler: (Please Print) ~ rf\~ /"\ .c::> Invoice Address: ~ Invoice Contact & Phone: CA.tj"-" P rchase Order: Quote/Bottle Order: Special Report/Formats: &JKJ&[b \'7@O® OOrn®(1Drn®l:rrnrID .. Contact ELI prior to Shipped by: 3: RUSH sample submittal 0 (i) for charges and Cooler 10(s): ~o~£ ~ R c co,-=Ol Q) Cl scheduling -See ._> 0 >-ro w t-Instrudion Page Dow o EDD/EDT(Electronic Data) J9 Cf) Cf) ct'l :s: -C (/J (I) J: 03:= ~ 0> ~ "C ReceiptTemp o POTWNVWTP () c Comments: Format: u <c75t.Q ~ :J U '0 .... 1ll1 c " <t:: 0 °c o State: o LEVEL IV .~ f$' .... ~Qj~§(§ ~ r-aj ~ Q.ct'l._ ~ J-c: o Other: o NELAC ~Iro I ~ :( :s On Ice: Y N :J (]).!::: CD ~ ~ ~ ~ « I- Z Ci. 4:1 ar o ~ " :: + V <f! cJ W "E 5 Custody Seal ~ >1 7~ , .! ~ ~ W ('Q On Bottle Y N '(, ~ CJ) -0 Cf) ~ -~ c: On Cooler Y N ~ :& <) ~ ~ H Intact 'Y N ~ ~ '"' ~ (/) SAMPLE IDENTIFICATION Collection Colledion MATRIX ~ .~ "t 'Jl Signature (Name, Location, Interval, etc.) Date Time \.J <. Match Y N 1 }tvJ-~_ 0,1,2.0\':).. 7/17/12. 07~ }-w X ~ 2 MW-2.4_ D1Ig.2.,C\Q.. II / j~/);2 0630 l-W ~ 'f I~ 3MW -:2.,1_ 07lb2..0 1J.. ,/ltd J:J... lJ IS 3-W X X ~ 'f.. ~ ~ Innn 411W " 2g_011 b2.C):l 7/1&/ll 1035 \-\J ~ ~ i 51p rv'\JJ E K1r1 '< I~ 6 1 -~ 7 ~ ~ 8 I~ 0) 9 Iron 1~~fL. 10 I~ );).Q)01Q( Custody Relinquished by (print): Datemme: llOO :)~fJ~ Received by (print): Daternme: Signature: '"IN'\ne.(" "~\ \; do.\k i / llf /1.lJ~:l Record Relinquished by {print):..j Date/Time: Signature: V Received by (print): DatelTime: Signature: MUST be ..... Signed Sample Disposal: Return to Client: Lab Disposal: Re<;elveObY{Y;~/~. 71 w II ::1-~lgtr~S , pOSSIbility. All SUD-comract aata Will De ClearlY notatea--.oA' your analY \/;,,;. ,..., , .. ",,,h ... i+o ",t ""'/'AI an':>I"n\lbh f'nm fnr ~rlrlitional information, downloadable fee schedule, forms, and links. EI\ERGY LABORATORIES wWw~netgylab~~om Mlljtltfi/~ SjRis1152 ANALYTICAL SUMMARY REPORT August24,2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12080143 Quote ID: C1640 -POC Wells Project Name: 3rd Quarter Groundwater 2012 Energy Laboratories, Inc. Casper WY received the following 5 samples for Energy Fuels Resources (USA) Inc on 8/3/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12080143-001 MW-28_08012012 08/01/12 14:00 08/03/12 Aqueous Metals by ICP-MS, Dissolved C12080143-002 MW-29_08012012 08/01/12 13:10 08/03/12 Aqueous Metals by ICP-MS, Dissolved Solids, Total Dissolved C12080143-003 MW-37 _07302012 07/30/12 13:40 08/03/12 Aqueous Alkalinity QA Calculations Fluoride E300.0 Anions Metals by ICP, Dissolved Metals by ICP-MS, Dissolved Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Solids, Total Dissolved -Calculated SW8260B VOCs, Standard List C12080143-004 Trip Blank 07/30/120:00 08/03/12 Aqueous SW8260B VOCs, Standard List C12080143-005 Temp Blank 08/02/12 0:00 08/03/12 Aqueous Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ D uJtA1~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.08.24 15:43:35 -06:00 Page 1 of 26 wWW.energyl~~.coin klal;tital ExcBI_~ SintS'952 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Report Date: 08/24/12 Sample Delivery Group: C12080143 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 26 EN:RGY LABORATORIES wYm.energylab.com AlIaIjtitaIEx~ smc. 7952 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Lab 10: C12080143-003 Client Sample 10: MW-37 _07302012 Analyses PHYSICAL PROPERTIES pH Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 7.23 S.u. H -Analysis performed past recommended holding time. Report Date: 08/24/12 Collection Date: 07/30/12 13:40 DateReceived: 08/03/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By H 0.01 A4500-H B 08/06/12 10:29/ jz MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 26 EI\l:RGY '", LABORATORIES wViW.eriergylab,.com 'Mi~iExclllsncB SinCI·I952 ~"8._. C-~SpeJrWV.88~235-0515 • Co.llege:Sfat!qn, T.X'888"6QO~221' QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Method: A2320 B Sample 10: MBLK Alkalinity, Total as CaC03 Carbonate as C03 Bicarbonate as HC03 Count Result 3 Method Blank ND ND 1.52 Units mg/L mg/L mg/L Sample 10: LCS-6677 Laboratory Control Sample Alkalinity, Total as CaC03 206 mg/L Sample 10: C12080120-001AOUP 3 Sample Duplicate Alkalinity, Total as CaC03 1600 mg/L Carbonate as C03 Bicarbonate as HC03 Sample 10: C12080121-001 BMS Alkalinity, Total as CaC03 Qualifiers: RL -Analyte reporting limit. MDC - Minimum detectable concentration 754 mg/L ND mg/L Sample Matrix Spike 329 mg/L RL 5.0 1.0 1.0 5.0 5.0 5.0 5.0 5.0 Report Date: 08/24/12 Work Order: C12080143 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R162889 Run: MANTECH_120806B 08/06/12 14:23 Run: MANTECH_120806B 08/06/12 14:39 103 90 110 Run: MANTECH 120806B 08/06/12 15:05 - 4.5 10 0.3 10 10 Run: MANTECH_120806B 08/06/12 15:23 96 80 120 ND -Not detected at the reporting limit. Page 10 of 26 EN:RGY LABORATORIES m.energylab.coltl Analjtii:,iExesllsi1CdinegJl52 :OU.IlIIJi:;l'I.·III.1 DIIIU-' .ila-.... D::I· • C'llSper.)W 888 .. 235-~51 ~ Stat!~n; rx88,Q"6~O:,22t8 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A2540 C Sample 10: MB-1_120803A Solids, Total Dissolved TDS @ 180 C Method Blank NO mg/L Sample 10: LCS-2_120803A Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1100 mg/L Sample 10: C12080143-002A OUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 4480 mg/L Sample 10: C12080143-003A MS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 7870 mg/L Qualifiers: RL -Analyte reporting limit. MOC -Minimum detectable concentration Report Date: 08/24/12 Work Order: C12080143 RL %REC Low Limit High Limit Run: BAL-1_120806A 10 Run: BAL-1_120806A 10 99 90 110 Run: BAL-1 120806A 10 Run: BAL-1_120806A 10 94 90 110 NO -Not detected at the reporting limit. RPO RPOLimit Qual 1.3 Batch: TOS120806A 08/06/12 13:30 08/06/12 13:30 08/06/12 13:30 5 08/06/12 13:31 Page 11 of 26 .. EI\ERGY LABORATORIES m.energylab.Com Alialjtical.ExullsnclI smc. 1m ;' 'dl~JI;ijW~87;t~41.i,~p,l11 .Billing~. MJ 800-7~5~4489 • C~sper,WY888-235-0515 :(~ti~ftJ~l;':'~~~lp,,¢,rty,~sn il8.~~612.;12Z5 . C~lIegeStatio:n, IX 8.8-6~O-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4500-F C Sample 10: MBLK Method Blank Fluoride ND mg/L Sample 10: LCS-6892 Laboratory Control Sample Fluoride 1.93 mg/L Sample 10: C12080142-001AMS Sample Matrix Spike Fluoride 1.82 mg/L Sample 10: C12080142-001AMSO Sample Matrix Spike Duplicate Fluoride 1.86 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 0.10 0.10 0.10 0.10 Report Date: 08/24/12 Work Order: C12080143 O/OREC Low Limit High Limit RPO RPOLimit Qual Batch: R162868 Run: MANTECH_120806A 08/06/12 09:41 Run: MANTECH_120806A 08/06/12 09:44 96 90 110 Run: MANTECH_120806A 08/06/1213:12 88 80 120 Run: MANTECH 120806A 08/06/12 13:15 - 90 80 120 2.2 10 ND -Not detected at the reporting limit. Page 12 of 26 EI'.ERGY L ABORATORIES m.energylab.com Anat;t/l:aIExesn."c.SincI,m 'B!lli.ng!;t;Mn'OO-131'~44~18 · C~sper;WVa8~ .. 235~~~15 r>_':"iJ '·"" ••. '''''' t.x88.;.6~O~~2l8 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4500-H B Report Date: 08/24/12 Work Order: C12080143 RL %REC Low Limit High Limit RPO RPOLimit Qual Sample 10: pH 6.86 Initial Calibration Verification Standard Analytical Run: PHSC_101 -C_120806A 08/06/12 08:58 pH Method: A4500-H B Sample 10: C12080143-003AOUP pH Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 6.84 S.u. Sample Duplicate 7.22 S.u. 0.010 100 98 102 Run: PHSC_101-C_120806A 0.010 NO -Not detected at the reporting limit. 0.1 Batch: R162839 08/06/12 10:31 3 Page 13 of 26 EN:RGY LABORATORIES m.energylab.com AfilI;tii:aIExCBlJsrlc; SInCs '952 .. Jfel~~a~MTJllqli~o711 .:BUling~.MT 800-7~5~44'9 . C/iSper.WV 8.8~ .. 235-~515 . jYJ§t£({§~lJJ~§~R.~~id,City;SD.8'8~&.72:.j 2t 5.· College StatIon, 1X 8~8 .. 6~O-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: A4500-NH3 G Sample 10: MBLK-1 Method Blank Nitrogen, Ammonia as N ND mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Ammonia as N 2.05 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Ammonia as N 1.93 mg/L Sample 10: C12080142-001 EMS Sample Matrix Spike Nitrogen, Ammonia as N 1.94 mg/L Sample 10: C12080142-001 EMSO Sample Matrix Spike Duplicate Nitrogen, Ammonia as N 1.93 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 0.050 0.050 0.050 0.050 0.050 Report Date: 08/24/12 Work Order: C12080143 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R163000 Run: TECHNICON_120808A 08/08/12 11 :56 Run: TECHNICON_ t20808A 08/08/12 11 :58 102 90 110 Run: TECHNICON_120808A 08/08/12 12:00 98 80 120 Run: TECHNICON_120808A 08/08/12 12:04 99 90 110 Run: TECHNICON_120808A 08/08/12 12:06 98 90 110 0.5 10 ND -Not detected at the reporting limit. Page 14 of 26 EN:RGY L ABORATORIES wWW~n~rgylab.cgm Ana1YllCiliEXcslhmcfI SIi1is 1152 QA/QC Summary Report Prepared by Casper, WY Branch C~~per,WYl88-235~'51$ ., Txa8 ... $Qo~2218 Client: Energy Fuels Resources (USA) Inc Report Date: 08/24/12 Project: 3rd Quarter Groundwater 2012 Work Order: C12080143 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.7 Analytical Run: ICP2-C_120820A Sample 10: ICV 5 Initial Calibration Verification Standard 08/20/12 12:02 Calcium 50.8 mg/L 0.50 102 95 105 Iron 5.15 mg/L 0.030 103 95 105 Magnesium 50.6 mg/L 0.50 101 95 105 Potassium 47.3 mg/L 0.50 95 95 105 Sodium 51.7 mg/L 0.50 103 95 105 Sample 10: ICSA 5 Interference Check Sample A 08/20/12 12:34 Calcium 504 mg/L 0.50 101 80 120 Iron 188 mg/L 0.030 94 80 120 Magnesium 506 mg/L 0.50 101 80 120 Potassium 0.00170 mg/L 0.50 Sodium 0.0408 mg/L 0.50 Sample 10: ICSAB 5 Interference Check Sample AB 08/20/12 12:38 Calcium 508 mg/L 0.50 102 80 120 Iron 188 mg/L 0.030 94 80 120 Magnesium 522 mg/L 0.50 104 80 120 Potassium 0.00270 mg/L 0.50 Sodium -0.0536 mg/L 0.50 Method: E200.7 Batch: R163499 Sample 10: MB-120820A 5 Method Blank Run: ICP2-C_120820A 08/20/12 12:58 Calcium NO mg/L 0.50 Iron NO mg/L 0.030 Magnesium NO mg/L 0.50 Potassium NO mg/L 0.50 Sodium NO mg/L 2.0 Sample 10: LFB-120820A 5 Laboratory Fortified Blank Run: ICP2-C_120820A 08/20/12 13:02 Calcium 49.8 mg/L 0.50 100 85 115 Iron 0.978 mg/L 0.030 98 85 115 Magnesium 48.2 mg/L 0.50 96 85 115 Potassium 45.4 mg/L 0.50 91 85 115 Sodium 48.9 mg/L 0.50 98 85 115 Sample 10: C12080143-003BMS2 5 Sample Matrix Spike Run: ICP2-C_120820A 08/20/1213:14 Calcium 708 mg/L 0.50 87 70 130 Iron 5.05 mg/L 0.030 99 70 130 Magnesium 380 mg/L 0.50 97 70 130 Potassium 247 mg/L 0.50 91 70 130 Sodium 799 mg/L 1.6 88 70 130 Sample 10: C12080143-003BMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_120820A 08/20/1213:18 Calcium 716 mg/L 0.50 90 70 130 1.0 20 Iron 5.09 mg/L 0.030 100 70 130 0.8 20 Magnesium 385 mg/L 0.50 99 70 130 1.1 20 -----------------_._----------------------------------------------------------- Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 15 of 26 EI'.ERGY LABORATORIES wWw;~neT&yla~.coin MiIyt!§,.~Ci1lJsi1CtI~SJiiij"52 MnSUD"'n. ll.' .".4 .4 .• ! .1.9 ... • C~~per •. W{ 8.8 .... 2~~~O~1~ • G~II~g4l;St~t'on! TX a8Q .. ~~O~~2t8 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: E200.7 Sample 10: C12080143-003BMSO 5 Sample Matrix Spike Duplicate Potassium 248 mg/L Sodium 797 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 08/24/12 Work Order: C12080143 RL %REC Low Limit High Limit 0.50 1.6 91 87 Run: ICP2-C_120820A 70 130 70 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual 0.4 0.3 Batch: R 163499 08/20/1213:18 20 20 Page 16 of 26 -J. I EN:RGY L ABORATORIES wWw.energylab.com Malyl/(:aiExuHIlflCB SinclI1952 Helena, Mf811M41.2:.Dl11 .~mings, rtf 800-7~5-4489 . Casper; WY 888 .. 235-0515 '-::jj~,,$j~1;li5 -~-R,Cl~ig;~ity,~n 86,8~$f2~'1 ~25 • Co_lI~geStat~on,TX' 888-6QO:,2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Method: E200.8 Units RL %REC Low Limit Report Date: 08/24/12 Work Order: C12080143 High Limit RPO RPOLimit Qual Analytical Run: ICPMS4-C_120820A Sample 10: ICV 18 Initial Calibration Verification Standard 08/20/12 10:27 Arsenic 0.0497 mg/L 0.0010 99 90 110 Beryllium 0.0496 mg/L 0.0010 99 90 110 Cadmium 0.0509 mg/L 0.0010 102 90 110 Chromium 0.0469 mg/L 0.0010 94 90 110 Cobalt 0.0517 mg/L 0.0010 103 90 110 Copper 0.0506 mg/L 0.0010 101 90 110 Lead 0.0487 mg/L 0.0010 97 90 110 Manganese 0.0502 mg/L 0.0010 100 90 110 Mercury 0.00506 mg/L 0.0010 101 90 110 Molybdenum 0.0489 mg/L 0.0010 98 90 110 Nickel 0.0504 mg/L 0.0010 101 90 110 Selenium 0.0502 mg/L 0.0010 100 90 110 Silver 0.0217 mg/L 0.0010 108 90 110 Thallium 0.0496 mg/L 0.0010 99 90 110 Tin 0.0497 mg/L 0.0010 99 90 110 Uranium 0.0496 mg/L 0.00030 99 90 110 Vanadium 0.0471 mg/L 0.0010 94 90 110 Zinc 0.0512 mg/L 0.0010 102 90 110 Method: E200.8 Batch: R163583 Sample 10: LRB 18 Method Blank Run: ICPMS4-C_120820A 08/20/12 11 :03 Arsenic NO mg/L 0.0050 Beryllium NO mg/L 0.00050 Cadmium NO mg/L 0.00050 Chromium NO mg/L 0.020 Cobalt NO mg/L 0.010 Copper NO mg/L 0.010 Lead NO mg/L 0.0010 Manganese NO mg/L 0.010 Mercury NO mg/L 0.00050 Molybdenum NO mg/L 0.010 Nickel NO mg/L 0.020 Selenium NO mg/L 0.0050 Silver NO mg/L 0.010 Thallium NO mg/L 0.00050 Tin NO mg/L 0.10 Uranium NO mg/L 0.00030 Vanadium NO mg/L 0.010 Zinc NO mg/L 0.010 Sample 10: LFB 18 Laboratory Fortified Blank Run: ICPMS4-C_120820A 08/20/12 11 :07 Arsenic 0.0528 mg/L 0.0010 106 85 115 Beryllium 0.0509 mg/L 0.0010 102 85 115 Cadmium 0.0527 mg/L 0.0010 105 85 115 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 17 of 26 EI'.ERGY LABORATORIES WWW.energylab.com Aliat;tif:aIExUosiic, SJi1U 1952 'Hil~q:~>J,fr-Jlt.;tt~dj1.'1 • B(lilngll, MT QOO~735"44'9 • Casper, WY.8~-23~-O~15 ~86.$,jI.~I~~ljI5.~·ij,i!~JaJ;,itYi S(j;8.'~'72-12~5 . ColiegeSt~tion, IX 8.'-6QO-22.18 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Method: E200.8 Sample 10: LFB Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc Sample 10: C12070995-006BMS4 Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc Count Result Units 18 Laboratory Fortified Blank 0.0498 mg/L 0.0530 mg/L 0.0528 mg/L 0.0524 0.0530 0.00488 0.0508 0.0526 0.0525 0.0214 0.0530 0.0517 0.0522 0.0494 0.0552 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 18 Sample Matrix Spike 0.0514 mg/L 0.0488 mg/L 0.0487 mg/L 0.0517 mg/L 0.0503 mg/L 0.0472 mg/L 0.0504 mg/L 0.0522 mg/L 0.00460 mg/L 0.0488 mg/L 0.0481 mg/L 0.136 mg/L 0.0198 mg/L 0.0510 mg/L 0.0481 mg/L 0.119 mg/L 0.0517 mg/L 0.0503 mg/L Sample 10: C12070995-006BMSO 18 Sample Matrix Spike Duplicate Arsenic 0.0515 mg/L Beryllium 0.0478 mg/L Cadmium 0.0482 mg/L Chromium 0.0524 mg/L Cobalt 0.0501 mg/L Copper Lead Manganese Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.0482 mg/L 0.0504 mg/L 0.0514 mg/L Report Date: 08/24/12 Work Order: C12080143 RL %REC Low Limit High Limit RPO RPOLimit Qual 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 0.0010 0.0010 0.00010 0.0010 0.0050 0.0010 0.0010 0.00050 0.0010 0.00030 0.010 0.010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 0.0010 0.0010 100 106 106 105 106 98 101 105 105 107 106 103 104 99 110 102 98 97 98 100 94 101 102 92 97 95 94 99 102 96 100 100 99 102 96 96 100 100 96 101 101 Run: ICPMS4-C_120820A 85 115 85 115 85 115 85 85 85 85 85 85 85 85 85 85 85 85 115 115 115 115 115 115 115 115 115 115 115 115 Run: ICPMS4-C 120820A 70 130 70 130 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 Run: ICPMS4-C_120820A 70 130 70 130 70 130 70 130 70 130 70 70 70 130 130 130 ND -Not detected at the reporting limit. 0.1 2.0 1.0 1.3 0.4 2.1 0.0 1.4 Batch: R 163583 08/20/12 11 :07 08/21/12 01 :56 08/21/12 02:01 20 20 20 20 20 20 20 20 Page 18 of 26 Ef\ERGY LABORATORIES WWW.energylab.com AliBlytlCai ~"1Isi1cB SInes 1952 n.~~,Mfll1;.4t~~Plll . Bining~ • .r(f.OO-7~5-44~~. Casper"WY ~~@ .. 235-~~15 . ~1~.a~lf~,§ __ ·~;~Rig~gitY,'SIf.8.8'-672-j225,. Coll~ge:Sfati'm, IX ,88~-6QO-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Method: E200.8 Units Sample 10: C12070995-006BMSO 18 Sample Matrix Spike Duplicate Mercury 0.00484 mg/L Molybdenum 0.0488 mg/L Nickel 0.0482 mg/L Selenium 0.131 mg/L Silver 0.0204 mg/L Thallium 0.0512 mg/L Tin 0.0479 mg/L Uranium 0.120 mg/L Vanadium 0.0518 mg/L Zinc 0.0508 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 0.00010 0.0010 0.0050 0.0010 0.0010 0.00050 0.0010 0.00030 0.010 0.010 %REC Low Limit Report Date: 08/24/12 Work Order: C12080143 High Limit RPO RPOLimit Qual Batch: R 163583 Run: ICPMS4-C_120820A 08/21/1202:01 97 70 130 5.1 20 97 70 130 0.0 20 95 70 130 0.3 20 85 70 130 3.5 20 102 70 130 3.1 20 102 70 130 0.2 20 96 70 130 0.4 20 100 70 130 0.1 20 100 70 130 0.2 20 100 70 130 0.9 20 NO -Not detected at the reporting limit. Page 19 of 26 iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiOiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiini EI'I:RGY LABORATORIES m;~nergyla~.com Atialyt/l;alixeI/JsiJCs SiniS 1m , " ,':, ;',' '" ffel~n'~I,,·~t:~~l"~l:~ .. D~~ i • 'Bini~gs, MT B.O~-7~5~448~. Casper, WY 888 .. 235".~,15 dillett!!~,,8)J:i~@.;ljt§ ·,~;~pJq,~fty; Sp,888-'7~:'225 • ColI~ge:Sfa.tip'n, rX88P-6QO~2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Report Date: 08/24/12 Work Order: C12080143 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E300.0 Analytical Run: IC2-C_120808A Sample ID: ICV-OBOB12-10 2 Initial Calibration Verification Standard 08/08/12 18:18 Chloride 10.1 mg/L 1.0 101 90 110 Sulfate 41.0 mg/L 1.0 102 90 110 Method: E300.0 Batch: R163035 Sample ID: ICB-OBOS12-11 2 Method Blank Run: IC2-C_120808A 08/08/12 18:35 Chloride NO mg/L 4.0 Sulfate NO mg/L 20 Sample ID: LFB-OSOS12-12 2 Laboratory Fortified Blank Run: IC2-C_120808A 08/08/12 18:53 Chloride 10.1 mg/L 1.0 101 90 110 Sulfate 40.8 mg/L 1.0 101 90 110 Sample ID: C120B0125-001BMS 2 Sample Matrix Spike Run: IC2-C_120808A 08/08/12 19:45 Chloride 122 mg/L 2.1 100 90 110 Sulfate 1200 mg/L 8.3 102 90 110 Sample I D: C120B0125-001 BMSD 2 Sample Matrix Spike Duplicate Run: IC2-C_120808A 08/08/12 20:02 Chloride 120 mg/L 2.1 98 90 110 1.8 10 Sulfate 1190 mg/L 8.3 99 90 110 1.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 20 of 26 EI'.ERGY L ABORATORIES ,.; m.energylabiom MI1yt1t:aIExUUsiJ&, SltiUrm QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N ND mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.55 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 2.01 mg/L Sample 10: C12080155-0010MS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 18.1 mg/L Sample 10: C12080155-0010MSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 17.8 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 0.10 0.10 0.10 0.50 0.50 Report Date: 08/24/12 Work Order: C12080143 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R162867 Run: TECHNICON_120806A 08/06/12 11 :43 Run: TECHNICON_120806A 08/06/12 11 :46 102 90 110 Run: TECHNICON_120806A 08/06/12 11 :48 103 90 110 Run: TECHNICON_120806A 08/06/12 13:06 102 90 110 Run: TECHNICON_120806A 08/06/12 13:08 99 90 110 1.7 10 ND -Not detected at the reporting limit. Page 21 of 26 EN:RGY LABORATORIES wWw.energylab.~om AniIjtIt;aIExcsJJsnc, $inU 1m ., '.: ~~e!ei!a~:Mf:·8lJ,~4:j~-P:7ti ~· Bj(ling~,MT 80~-735~448~. C~sperf wY8i8 .. 23~-O~15 'ill~!~~'!JY~@!j~jD~lf~l ·g~p.J~ ,¢t~,S~.,888:-~72-J 225 • CQllege:station, IX a88"6~O-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Method: E900.1 Sample 10: LCS-GA-0562 Gross Alpha minus Rn & U Count Result Units Laboratory Control Sample 27.4 pCi/L Report Date: 08/24/12 Work Order: C12080143 RL %REC Low Limit High Limit Run:G5000VV_120807A 131 70 130 RPO RPOLimit Qual Batch: GA-0562 08108/12 06:49 S -LCS response i~ outside of the acceptance range for this analysis, Since the MB, MS, and MSD are acceptable the batch is approved. Sample 10: MB-GA-0562 Gross Alpha minus Rn & U 3 Method Blank -0.242 Gross Alpha minus Rn & U Precision (±) 0.729 Gross Alpha minus Rn & U MDC 1.34 pCi/L pCi/L pCi/L Sample 10: C12080110-001HMS Gross Alpha minus Rn & U Sample Matrix Spike Sample 10: C12080110-001HMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 54.4 pC ilL Sample Matrix Spike Duplicate 50.3 pC ilL U -Not detected at minimum detectable concentration Run:G5000VV_120807A Run:G5000VV_120807A 119 70 130 Run: G5000VV 120807A - 107 70 130 NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 7.9 08/08/12 06:49 U 08108/12 06:49 08/08/12 06:49 31 Page 22 of 26 EN:RGY LABORATORIES wWW~nergyl~b.C9m MiIytWaIEi_~' SJnCi 1m -448~. C~sper. WV8.~'"23~~O~15 • ~l!lIege:Stat!pn, TK .. 8a~ .. 6~b~~21a QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 08/24/12 Project: 3rd Quarter Groundwater 2012 Work Order: C12080143 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R162997 Sample 10: 07-Aug-12_LCS_ 4 16 Laboratory Control Sample Run: 5975VOC1 -120807B 08/07/1213:09 Acetone 73 ug/L 20 73 70 130 Benzene 11 ug/L 1.0 106 70 130 Carbon tetrachloride 9.3 ug/L 1.0 93 70 130 Chloroform 8.7 ug/L 1.0 87 70 130 Chloromethane 8.9 ug/L 1.0 89 70 130 m+p-Xylenes 22 ug/L 1.0 108 70 130 Methyl ethyl ketone 99 ug/L 20 99 70 130 Methylene chloride 7.2 ug/L 1.0 72 70 130 Naphthalene 13 ug/L 1.0 127 70 130 o-Xylene 11 ug/L 1.0 112 70 130 Toluene 11 ug/L 1.0 108 70 130 Xylenes, Total 33 ug/L 1.0 109 70 130 Surr: 1 ,2-0ichlorobenzene-d4 1.0 103 80 120 Surr: Oibromofluoromethane 1.0 102 70 130 Surr: p-Bromofluorobenzene 1.0 116 80 130 Surr: T 0luene-d8 1.0 115 80 120 Sample 10: 07-Aug-12_MBLK_7 16 Method Blank Run: 5975VOC1 120807B 08/07/12 15:29 Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 o-Xylene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1 ,2-0ichlorobenzene-d4 1.0 103 80 120 Surr: Oibromofluoromethane 1.0 102 70 130 Surr: p-Bromofluorobenzene 1.0 117 80 120 Surr: Toluene-d8 1.0 114 80 120 Sample 10: C12070956-003JMS 16 Sample Matrix Spike Run: 5975VOC1 120807B 08/07/1222:15 Acetone 1500 ug/L 200 76 70 130 Benzene 200 ug/L 10 97 70 130 Carbon tetrachloride 170 ug/L 10 86 70 130 Chloroform 160 ug/L 10 82 70 130 Chloromethane 350 ug/L 10 83 70 130 m+p-Xylenes 400 ug/L 10 98 70 130 Methyl ethyl ketone 1900 ug/L 200 96 70 130 Methylene chloride 150 ug/L 10 68 70 130 S Naphthalene 230 ug/L 10 113 70 130 -------------------------------------_._-------------------------------------------- Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 23 of 26 EN:RGY LABORATORIES wWw~nergylab.com Aiii1Ytk:alExUlJsncd/m '·952 ,DUIIJIIXlI.·m.1 tlIJIU-I;iI:I .. ~~tl9,· Clisper,W¥ 8,8-235.;0515 •• C~lleg~:Stat!~n, TX ;8 .... 6.0-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 08/24/12 Project: 3rd Quarter Groundwater 2012 Work Order: C12080143 Analyte Count Result Units RL O/OREC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R 162997 Sample 10: C12070956-003JMS 16 Sample Matrix Spike Run: 5975VOC1_120807B 08/07/1222:15 o-Xylene 200 ug/L 10 102 70 130 Toluene 210 ug/L 10 98 70 130 Xylenes, Total 600 ug/L 10 100 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 103 80 120 Surr: Dibromofluoromethane 1.0 102 70 130 Surr: p-Bromofluorobenzene 1.0 116 80 120 Surr: Toluene-d8 1.0 116 80 120 Sample 10: C12070956-003JMSO 16 Sample Matrix Spike Duplicate Run: 5975VOC1 120807B 08/07/1222:50 Acetone 1400 ug/L 200 70 70 130 7.7 20 Benzene 200 ug/L 10 96 70 130 0.8 20 Carbon tetrachloride 170 ug/L 10 86 70 130 0.0 20 Chloroform 160 ug/L 10 81 70 130 1.5 20 Chloromethane 330 ug/L 10 74 70 130 4.9 20 m+p-Xylenes 400 ug/L 10 99 70 130 0.8 20 Methyl ethyl ketone 1800 ug/L 200 92 70 130 4.3 20 Methylene chloride 150 ug/L 10 65 70 130 4.2 20 S Naphthalene 230 ug/L 10 113 70 130 0.3 20 o-Xylene 200 ug/L 10 102 70 130 0.4 20 Toluene 210 ug/L 10 99 70 130 0.8 20 Xylenes, Total 610 ug/L 10 100 70 130 0.7 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 104 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 101 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 117 80 120 0.0 10 Surr: Toluene-d8 1.0 115 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 24 of 26 EN:RGY LABORATORIES Standard Reporting Procedures :.H{'·na;J4"(811~412·,:oitj ··BilUng~, MT,O~"735w4489 . Casper,WY888-235 .. 0515 &~!~~=7J15: ~,~~~i~C·ijy;Sit'~8~ .. ~12-12~5 • CQllege.StatiD,n, Ix 88.-690~U18, Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 8/8/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContainerlT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 4.0'C On Ice Yes 0 Yes 0 C12080143 Date Received: 8/3/2012 Received by: tj No D No D No D No D No D No D No D No D No D No D No D No D No D Carrier FedEx name: Not Present D Not Present D Not Present 0 Not Applicable D No VOA vials submitted D Not Applicable D Page 25 of 26 ""U Q) co (1) I\) 0> o -I\) 0> EN:RGY , , mD" Chain of Custody and Analytical Request Record Page _, _ of --1- ---------- -~ - --......... ---.,.-.......... -""'---... . --Company Name: 'F\Ae.l~ Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: ~ rJC.IS'd 3 iJ Q~r·1-e.(" G-ro"",J Wl1\ter .:4o.~ State: V\"f" Yes ® No 0 Report Mail Address: pO SO ')( gOG} Contact Name: Phone/Fax: Email: Sampler: (Please Print) ~)~t\J ;..,~ U.,-8YSil (fr:J..ifl11 f'",Jme.r t.13h 67g .2.22.1 ~nfle'" Uo)I.JG4f Invoice Address: ......., Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: SI'\h;te. O(-\,,\'c\ -!v..rK Y3:5 b78 .u21 Special Report/Formats: ~ &rm&[1S7@O@ OO~@M~Ii[ID • Contact ELI prior to Sh~'1b~ 0 .... RUSH sample submittal r-' --,. -E.~ ~o (I)~ for charges and Cooler IDCa); , ~cc ;gOI CU C ~ R scheduling.-See v{~~ ._> 0 >.(6 W t:. Instruction Page o OW 0 EDD/EDT(Electronic Data) ~(/)~ m ~ 03:= ~ Ol ~ :c "'0 Receipt Temp o POTWMlWTP Format: () c Comments: ~«~I.Q~ ~ 5 U 4,0 ocA.j D State: 0 'LEVEL IV o .... all c: &.. ~ .... Qj.$! a'C ....... C'CI . ~J ~ ~~I~~ ~ ~ c ~ D Other: 0 NELAC ,i '-Mw ,·37 On Ice: ::J ::J (I).: Q) :s: ~ t-5 zo.«lg>o ~ W "E '']:'ncl~~ Cuatody Seal ~ >1 +! ~ ~ W as On Bottle ·N II (JJ 'C I~ c: ple~e On Cooler 0 .5 H '~N Intact 'S ~ C/) SAMPLE IDENTIFICATION Collection Collection MATRIX 0 ~ <: SIgnature (Name, Location, Interval, etc.) Date Time Match 1 1-J\\ W -~. {))<.o \:AU '~:l. g/t/2.0\2 ~40D )-VJ ~. 2 M \/Y-;l.Cf_O[(Ol 'J..Oi:J. ~1l1 ;J.0i2 I~\O 2-W X X ~ 3 7!30/-;Al".. )3LtO fo-W X ~ Ftw-~7_ 0730.2.0tl [nnn 4 :Tr, t> .~ \ o..r\X 71 '-30 /;l(Ji~ ECJ.:2~O' 4~: ~ 5 J f'=' ~ 6 ~ 7 ~ 8 ~ 01 9 i' 10 b:;n Custody Relinquished by (print): Daterrime: Signature: Received by (print): Daterrime: Signa ure: rknl\~'" UcH~JG.tl g/~/~)J.. HOD "::),.,n.J1k fl· JJ'L. .A Record Relinquished by (print): J Daterrime: Signature: ,-' Received by (print): Datafflme: Signature: MUST be . Signed KecelVeu uy LaDOrawry: ' Datelltme: / , ~ ~TI;;'~, II~ Sample Disposal: Return to Client: Lab Disposal: ~':~-}::L In certain circumstances. samples submitted to Energy laboratories, Inc. may be subcontracted to other certified laboratories in order to ~tmplete the analysis .... 1 ~ if This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. -"";''J fOCJ Visit our web site at www.energylab.comfor additional information, downloadable fee schedule. forms, and links. EN:RGY LABORATORIES www.energylab.com (.....Hel!lna.Mr.817 .. 412-0711 -Billings.MT 800-735-4489 · Gasper, WV 888 .. 235 .. 0515 An,lyticalucsUIHII:BSi11Cl11952 " ~'_"" §iO~tt~, WY,8$& .. $86 .. 1175 • Rapid City, Sf} 888~'12-1225 . College Station, IX 888-690 .. 2218 August30,2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C 12080830 ANALYTICAL SUMMARY REPORT Quote 10: C1640 -POC Wells Project Name: 3rd Quarter Groundwater 2012 Energy Laboratories, Inc. Casper WY received the following 3 samples for Energy Fuels Resources (USA) Inc on 8/17/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12080830-001 MW-26_08162012 08/16/126:40 08/17/12 Aqueous SW8260B VOCs, Standard List C12080830-002 MW-65_08162012 08/16/12 6:40 08/17/12 Aqueous Same As Above C12080830-003 Trip Blank 6706 08/16/12 0:00 08/17/12 Aqueous Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 , unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601 , unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~D uJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.08.30 13:12:37 -06:00 Page 1 of 12 www.energylaib.com AflBtytical ExcsIlIHlCB Sines 1952 ~~!ena; MT8n .. 412 .. 071 t • Billings,MT 800-735-4489 • Casper, WY 888-235-0515 " t',Gille6e, wY',866-6B6-7175 • Ra id City; SI} 888-672-1225 • College Station, IX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Report Date: 08/30/12 Sample Delivery Group: C12080830 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTI FICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. 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Page 2 of 12 E~RGY LABORAT ORIES www.energyla.b.com AIl8IyticaI Excslhmca ~ 1952 ~'HeI~na, Mt'871-472~(J711 " Billings, MT 800-735,.4489 " Casper, WY888 .. 235-0515 il~~e;WY8B, &~6,.,. 86-7175 " Rapid City, SI} 888-672-1225 " College Station, IX 888-690-221,8 ~ ...• :--':'",<" .;>........ ., QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Method: SW8260B Sample 10: C12080808-001 KMS Benzene Carbon tetrachloride Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Count Result Units 14 Sample Matrix Spike 210 ug/L 180 ug/L 370 360 2100 190 170 200 220 560 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Sample 10: C12080808-001 KMSO 14 Sample Matrix Spike Duplicate Benzene 230 ug/L Carbon tetrachloride 200 ug/L Chloromethane 370 ug/L m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Sample 10: 082212_LCS_6 Benzene Carbon tetrachloride Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Qualifiers: RL -Analyte reporting limit. R -RPD exceeds advisory limit. 420 2200 210 210 240 230 660 ug/L ug/L ug/L ug/L ug/L ug/L ug/L 14 Laboratory Control Sample 11 ug/L 9.8 ug/L 10 ug/L 20 120 9.4 10 11 11 31 ug/L ug/L ug/L ug/L ug/L ug/L ug/L Report Date: 08/30/12 Work Order: C12080830 RL %REC Low Limit High Limit RPO RPOLimit Qual 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 101 92 85 88 107 89 83 100 104 92 91 91 90 102 112 101 84 102 109 98 103 122 109 109 93 92 9'1 98 110 98 101 101 116 94 100 112 106 104 87 89 86 Run: SATURNCA_120822A 70 130 70 130 70 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 130 120 130 120 120 Run: SATURNCA_120822A 70 130 70 130 70 130 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 120 130 120 120 Run: SATURNCA_120822A 70 130 70 130 70 130 70 70 70 70 70 70 70 80 70 80 130 130 130 130 130 130 130 120 130 130 ND -Not detected at the reporting limit. 9.8 8.7 0.4 15 1.5 9.4 21 19 3.9 17 0.0 0.0 0.0 0.0 Batch: R163670 08/22/1222:04 08/22/1222:40 20 20 20 20 20 20 20 20 20 20 10 10 10 10 R 08/22/12 14:18 Page 6 of 12 E~RGY LABORAT ORIES www.energyJab.com Analytfcal ExCSliBnCB Sines 1952 Helena, MT'S71·472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ' .. ~~ __ ~m~tie., w-r 866-.~.8a-7175 • Rapid City, SO 888-672-1225 • Col/ege Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Method: SW8260B Units Sample 10: 082212_LCS_6 Surr: Toluene-d8 14 Laboratory Control Sample Sample 10: 082212_MBLK_8 Benzene Carbon tetrachloride Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Qualifiers: RL -Analyte reporting limit. 14 Method Blank NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L Report Date: 08/30/12 Work Order: C12080830 RL %REC Low Limit High Limit RPO RPOLimit Qual 1.0 98 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 91 1.0 90 1.0 87 1.0 92 Run: SATURNCA_120822A 80 120 Run: SATURNCA_120822A 80 70 80 80 120 130 120 120 NO -Not detected at the reporting limit. Batch: R163670 08/22/12 14:18 08/22/12 15:31 Page 7 of 12 EI'.ERGY LABORATORIES www.energylab.com Analytical ExcsllSIICB Sincg 1952 ... :,H~fe,~a,MrB77;'472-0711 • Billings, MY 800-735-4489 11 Casper, WY 888 .. 235-0515 'WYI6~,,:'B5-1n5 • Rapid crty, so 888-612-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Method: SWS260B Sample 10: C120S0960-0031MS Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: C120S0960-0031MSO Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Sample 10: OS2712_LCS_ 4 Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes, Total Qualifiers: RL -Analyte reporting limit. Count Result Units 15 Sample Matrix Spike 210 ug/L 200 ug/L 200 210 380 2100 190 180 210 220 600 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 15 Sample Matrix Spike Duplicate 240 ug/L 220 ug/L 230 ug/L 250 ug/L 420 2500 220 210 230 230 650 ug/L ug/L ug/L ug/L ug/L ug/L ug/L 15 Laboratory Control Sample 11 ug/L 10 ug/L 11 ug/L 11 21 130 10 11 12 11 33 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Report Date: 08/30/12 Work Order: C12080830 RL %REC Low Limit High Limit 10 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 10 10 10 10 10 200 10 10 10 10 10 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 106 100 99 106 95 103 96 91 107 108 99 88 92 89 102 119 111 114 124 105 125 109 106 116 116 109 92 96 89 101 110 103 109 107 103 127 101 107 120 112 109 Run: SATURNCA_120827A 70 130 70 130 70 70 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 130 130 120 130 120 120 Run: SATURNCA_120827A 70 130 70 130 70 130 70 130 70 70 70 70 70 70 70 80 70 80 80 130 130 130 130 130 130 130 120 130 120 120 Run: SATURNCA_120827A 70 130 70 130 70 130 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 12 11 14 16 9.8 19 12 15 7.9 7.5 9.1 0.0 0.0 0.0 0.0 Batch: R163830 08/27/1221 :37 08/27/1222:13 20 20 20 20 20 20 20 20 20 20 20 10 10 10 10 08/27/12 14:06 Page 8 of 12 ------==== EI'.ERGY LABORATORIES www.energyJab.com Allalytical ExcsDsnCB SincIJ 1952 '::, ,H;leQ,t!, MT 87,1~4l,2-0711 • Billings, MT 800-735-4489 " Casper, W'f 888-235-0515 \i!!:~~e; Wt'~6~§~6-1J15 • Rap,ip Gfty, 50,888-672-1225 -College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Method: SW8260B Units Sample 10: 082712_LCS_ 4 15 Laboratory Control Sample Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: 082712_MBLK_6 15 Method Blank Benzene NO ug/L Carbon tetrachloride NO ug/L Chloroform NO ug/L Chloromethane NO ug/L m+p-Xylenes NO ug/L Methyl ethyl ketone NO ug/L Methylene chloride NO ug/L Naphthalene NO ug/L o-Xylene NO ug/L Toluene NO ug/L Xylenes, Total NO ug/L Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Qualifiers: RL -Analyte reporting limit. RL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Report Date: 08/30/12 Work Order: C12080830 %REC Low Limit High Limit RPO RPOLimit Qual 90 90 91 100 87 92 84 99 Run: SATURNCA_120827A 80 120 70 130 80 130 80 120 Run: SATURNCA_120827A 80 120 70 130 80 120 80 120 Batch: R 163830 08/27/12 14:06 08/27/12 15:32 NO -Not detected at the reporting limit. Page 9 of 12 ~~~~~~-----------------------------------------------EN:RGY LABORATORIES www.energylab.com Analytical ExcsH8IlCfI SJm:g 1952 , Helena, Mr877~72-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 ~,~"'=C .Jg~II~~Ji~ WYS6&-$B6-7175 • Ra~i~ City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Groundwater 2012 Analyte Count Result Units Method: SW8260B Sample 10: 082812_MBLK_6 5 Method Blank Chloroform NO ug/L Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: C12081068-003CMS 5 Sample Matrix Spike Chloroform 240 ug/L Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Sample 10: C12081068-003CMSO 5 Sample Matrix Spike Duplicate Chloroform 240 ug/L Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Sample 10: 082812_LCS_ 4 5 Laboratory Control Sample Chloroform 10 ug/L Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Qualifiers: RL -Analyte reporting limit. RL 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 1.0 1.0 10 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Report Date: 08/30/12 Work Order: C 12080830 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R163906 Run: SATURNCA_120828A 08/28/12 12:50 90 80 120 94 70 130 86 80 120 101 80 120 Run: SATURNCA_120828A 08/28/12 19:49 120 70 130 94 80 120 99 70 130 94 80 120 99 80 120 Run: SATURNCA_120828A 08/28/12 20:25 119 70 130 0.7 20 88 80 120 0.0 10 94 70 130 0.0 10 88 80 120 0.0 10 103 80 120 0.0 10 Run: SATURNCA_120828A 08/28/12 11 :37 104 70 130 93 80 120 92 70 130 91 80 130 99 80 120 NO -Not detected at the reporting limit. Page 10 of 12 --------========== EI\ERGY, LAS ORATORIES www.energylab.com Analytical ExCBI/snCB SiIlCB 1!152 MT 877-472-0711 • Billings, MT 800-735-4489 .. Casper, WY 888-235-0515 'Gm8tte':WY'I!66·;&B61~7n5 • Rapip City, SO 888~672-1225 If College Station, IX 888~690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Tracy Judge Reviewed by: BL2000\kschroeder Reviewed Date: 8/21/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContaineriT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes [{1 Yes [{1 Yes D Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 Yes [{1 3.2"C On Ice Yes [{1 Yes D C12080830 Date Received: 8/17/2012 Received by: km Carrier NDA name: No D No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present [{1 Not Applicable D No VOA vials submitted D Not Applicable [{1 Page 11 of 12 --EN:RGY m1 Chain of Custody and Analytical Request Record Page_J _of_l_ ------~-.... --_ .... -.. ,.. ----.... _-.. ~ ... -.... __ ._ ... -.... --_ .. _._., Company Name: f~e\s Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: I E1\U~~ 3t'ci ()\,)..orter G-roUllJWC\.+er .'l.OI~ State: lA"""r Yes f5if No 0 ~ Report Mail Address: PO gcq Contact Name: Phone/Fax: Email: Sampler: (Please Print) I ~O)( .22:2.1 ';t1"~r »oILd~ i 5\OJ)dinE\ txr 845i1 GrlXf"'t' in l' ~ N1eC'" 4315 G78 I nvoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: I SG\.rr"Ic. St,.r'1< Special Report/Formats: S ~[b W®O@ ~rn®OIJ~Lf@:1ID .. Contact ELI prior to s~p;:);M 0 (i) RUSH sample submittal Cooler lots): ~o (/)..t.= ~ R for charges and ~co~OI (i) Cl scheduling -See ctV ._> 0 >om w t:. Instruction Page Dow o EDD/EDT(Electronic Data) B U) (/) co S: c:: ()s (/) :r: 0s:= m 0> "0 Receipt Temp o POTWIWWTP () c Comments: Format: u<c73,.Q~ ::J U i.2-'0 L.. CDI c: « ° °C o State: o LEVEL IV .... mel> c '-I-ea ] o.~rgo ~ c (!)N o Other: o NELAC L-On Ice: E~rn ' :::J ::l el>'!:::C)s I- zo..<laro W "0 5 Custody Seal l-E >1 W ea On Bottle Y N C'il CJ) "0 ~: (/) >1\ c On Gooier \,..) ro 0 en H Intact SAMPLE IDENTIFICATION Collection Col/ection MATRIX > Signature (Name, Location, Interval, etc.) Date Time Match 1 MvJ-'l.' .. 08 1~201Q.. gil ,1:1.0\'2. Cb~D 3-W ~ ~ 2 '6/1 (,/:10 \~ ~-w y. I~ MW-bS_DSlb~O);:t Db4() 3 -r'rj 0 Rlo-nk ({7fJJ [(Q) Inn" 4 I \ I~ I~ 5 I~ ~ I 6 ~ 7 ~ j 8 ~ I , 9 ~ I 10 ~ I Custody ~;~;; by"~ni\ 1'1,.~ OaterTime: ~~tAl~ Received by (print): OaterTime: Signature: g/lb/.:t(j(~ 1100 Record Relinquished by (print): \J OatelTime: Signature: --Received by (print): DaterTime: Signature: MUST be . Signed ~~l'H;T~ DatefTIme: rg..J1 6 Signature: Sample Disposal: Return to Client: Lab Disposal: Acrr7J_~ j ~ 10 .. A-I 1_,,, In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. TabF Laboratory Analytical Reports -Accelerated Monitoring r - TabF1 Laboratory Analytical Reports -Accelerated Monitoring August 2012 00' www~n"gylal>.com r--Helena, MI 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ AnatyticalExcsUBflCISincB 7!152 J ... _~illette, WY 8&6-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 EN:RGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C 12080469-003 Client Sample ID: MW-11_08072012 Report Date: 09/05/12 Collection Date: 08/07/12 11 :30 DateReceived: 08/10/12 Matrix: Aqueous Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 166 ug/L MCL! Qualifier RL QCL Method Analysis Date 1 By 10 E200.8 08/27/12 17:291 cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 5 of 21 EI\ERGY LABORATORIES wwwienergylab.com Analytical ExCSUIMCB Sines '152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&86-7175 • Rapid City, SI) 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Lab 10: C 12080469-004 Client Sample 10: MW-14_08072012 Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2300 ug/l Qualifier Rl 10 Report Date: 09/05/12 Collection Date: 08/07/12 13:21 DateReceived: 08/1 0/12 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By E200.8 08/27/12 17:34/ cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 21 EN:RGY L ABORATORIES www.energyJab.com Analylical ExcsllBm:" Sines 7852 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C 12080469-002 Client Sample ID: MW-25_08062012 Analyses METALS -DISSOLVED Uranium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 6.72 ug/l Qualifier RL 0.30 Report Date: 09/05/12 Collection Date: 08/06/12 11:10 DateReceived: 08/10/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E200.8 08/27/1217:251 cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 21 EI'.ERGY LABORATORIES www.energylab.com AnalYtical ExCBIism;s Sines '152 L Helena, MT 877-472 .. 0711 • Billings, MT 800-735-4489 • Casper, WY 888 .. 235-0515 '~illetta, WY 866 .. 686 .. 7175 • Rapid City, S[) 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C 12080469-005 Client Sample ID: MW-26_08082012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N PHYSICAL PROPERTIES Solids, Total Dissolved TOS @ 180 C METALS -DISSOLVED Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 78 1.6 3210 67.4 NO NO NO 2200 NO NO 17 NO NO NO 90.0 96.0 93.0 93.0 o -RL increased due to sample matrix. Units mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 09/05/12 Collection Date: 08/08/12 13:31 DateReceived: 08/10/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By 0 4 E300.0 08/14/12 04:01 1 Ijl 0.1 E353.2 08/13/12 16:31 fir 10 A2540 C 08/10/12 15:08 1 ab 0.30 E200.8 08/27/1217:381 cp 20 SW8260B 08/14/1219:18/jk 1.0 SW8260B 08/14/1219:181 jk 1.0 SW8260B 08/14/1219:181 jk 0 500 SW8260B 08/14/1218:41 1 jk 1.0 SW8260B 08/14/1219:181 jk 20 SW8260B 08/14/1219:181 jk 1.0 SW8260B 08/14/1219:181 jk 1.0 SW8260B 08/14/1219:181 jk 1.0 SW8260B 08/14/1219:181 jk 1.0 SW8260B 08/14/1219:181 jk 80-120 SW8260B 08/14/1219:181 jk 70-130 SW8260B 08/14/1219:181 jk 80-120 SW8260B 08/14/1219:181 jk 80-120 SW8260B 08/14/1219:181 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 21 EN:RGY LABORATORIES www~energylab.com Analytical UCSUBflCB Sines 7952 Helena, MT 877 .. 472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~il!ette, WY866 .. 6B6-7175 • Rapid City, SO 888-672-1225 • Colleg~ Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C 12080469-006 Client Sample ID: MW-30_08072012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N METALS -DISSOLVED Selenium Uranium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 139 18 38.4 8.04 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l Report Date: 09/05/12 Collection Date: 08/07/1210:25 DateReceived: 08/1 0/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By D 2 E300.0 08/14/12 04:181 Ijl D 2 E353.2 08/13/12 16:38 1 Ir 5.0 E200.8 08/27/1218:00/cp 0.30 E200.8 08/27/1218:00/cp MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 8 of 21 EI\ERGY LABORATORIES www.energylab.com Analytical Excstlsnc. Sinc, '952 Helena, MT 877-472 .. 0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86S .. 686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Lab ID: C 12080469-00 1 Client Sample ID: MW-31_08062012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 175 21 571 1400 0-Rl increased due to sample matrix. Units mg/l mg/l mg/l mg/l Report Date: 09/05/12 Collection Date: 08/06/12 13:15 DateReceived: 08/10/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date I By o o 2 4 10 E300.0 E353.2 E300.0 A2540 C MCl -Maximum contaminant level. 08/14/12 03:431 Ijl ' 08/13/12 16:231 Ir 08/14/12 03:431 Ijl 08/10/12 15:08 1 ab NO -Not detected at the reporting limit. Page 3 of 21 EN:RGY LABORATORIES WWN.energyJab.com Analytical ExcsJlsnc, Sines 7952 Helena, MT 871-472-0711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C 12080469-007 Client Sample ID: MW-35_08082012 Analyses METALS -DISSOLVED Manganese Selenium Thallium Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 273 ug/l 18.8 ug/l 0.61 ug/l 26.2 ug/l 4.2 pCi/l 0.5 , pCi/l 0.2 pCi/l MOC -Minimum detectable concentration Qualifier Rl 10 5.0 0.50 0.30 Report Date: 09/05/12 Collection Date: 08/08/1208:35 DateReceived: 08/1 0/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By E200.8 08/27/1218:051 cp E200.8 08/27/1218:051 cp E200.8 08/27/1218:051 cp E200.8 08/27/1218:051 cp E900.1 08/30/12 21 :38 1 Ibb E900.1 08/30/12 21 :38 1 Ibb E900.1 08/30/12 21 :38 1 Ibb MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 21 EN:RGY LABORATORIES www.energyJab.com Analytical ExCBIIenc. Sines '152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Lab 10: C 12080469-008 Client Sample 10: MW-65_08072012 Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2250 ug/l Qualifier Rl 10 Report Date: 09/05/12 Collection Date: 08/07/12 13:21 DateReceived: 08/1 0/12 Matrix: Aqueous MCL! QCl Method Analysis Date I By E200.8 08/27/1218:091 cp MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 21 EN:RGY LABORATORIES www.energylab.com Analytical ExC8llBIICB Sincs 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, S[) 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C12080469-009 Client Sample ID: Trip Blank 6746 Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L 90.0 %REC 97.0 %REC 81.0 %REC 93.0 %REC Qualifier Rl 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/05/12 Collection Date: 08/08/12 DateReceived: 08/10/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:55 1 jk SW8260B 08/14/12 16:55/ jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:55/ jk SW8260B 08/14/12 16:55/ jk SW8260B 08/14/12 16:551 jk SW8260B 08/14/12 16:551 jk MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 11 of 21 EI'I:RGY LABORATORIES www.energylab.com AnalYtical ExC8llBflCf Sincs 1952 Helena, MT 877-472-0111 • Billings, MT 800-135-4489 • Casper, WV 888-235-0515 ~illette, WY 86&-686-1115 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 LablD: C12080469-010 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.0 Qualifier RL Report Date: 09/05/12 Collection Date: 08/09/12 DateReceived: 08/1 0/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By E170.1 08/10/12 12:46/ kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 12 of 21 EN:RGY LABORATORIES www.energyiab.com Analytical ExesllBfiCf Sines '952 Helena, MT 877 .. 472 .. 0111 • Billings, MT 800-735 .. 4489 . Casper, WV 888-235 .. 0515 '~Ulet±e, WV 866~6B6· 7175 • Rapid City, S[} 888-672·1225 • College Station, IX 888-690-2218 ANAL VTICAL SUMMARY REPORT September 05, 2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12080469 Quote ID: C1640 -POC Wells Project Name: August Monthly Groundwater 2012 Energy Laboratories, Inc. Casper WY received the following 10 samples for Energy Fuels Resources (USA) Inc on 8/10/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix . Test C12080469-001 MW-31_08062012 08/06/12 13:15 08/10/12 Aqueous E300.0 Anions Nitrogen, Nitrate + Nitrite Solids, Total Dissolved C 12080469-002 MW-25_08062012 08/06/12 11 :10 08/10/12 Aqueous Metals by ICP-MS, Dissolved C 12080469-003 MW-11_08072012 08/07/12 11 :30 08/10/12 Aqueous Same As Above C 12080469-004 MW-14_08072012 08/07/12 13:21 08/10/12 Aqueous Same As Above C 12080469-005 MW-26_08082012 08/08/12 13 :31 08/10/12 Aqueous E300.0 Anions Metals by ICP-MS, Dissolved Nitrogen, Nitrate + Nitrite Solids, Total Dissolved SW8260B VOCs, Standard List C12080469-006 MW-30_08072012 08/07/12 10:25 08/10/12 Aqueous E300.0 Anions Metals by ICP-MS, Dissolved Nitrogen, Nitrate + Nitrite C 12080469-007 MW -35_08082012 08/08/128:35 08/10/12 Aqueous Metals by ICP-MS, Dissolved Gross Alpha minus Rn222 and Uranium C 12080469-008 MW-65_08072012 08/07/12 13:21 08/10/12 Aqueous Metals by ICP-MS, Dissolved C 12080469-009 Trip Blank 6746 08/08/120:00 08/10/12 Aqueous SW8260B VOCs, Standard List C12080469-010 Temp Blank 08/09/120:00 08/10/12 Aqueous Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ D uJtAi~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.09.05 11: 16:53 -06:00 Page 1 of 21 www.energylab.com (' Analytical ExcsllsnclJ Sines 1952 Helena, MT 877 .. 472-0111 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Ra id Ci ,SD 888-672-1225 • Colle e Station TX888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Report Date: 09/05/12 Sample Delivery Group: C12080469 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 21 EI'.ERGY LABORATORIES www.energylab.com I Analytical Excsll8llcB Sines 1952 J _ Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Analyte Count Result Units Method: A2540 C Sample 10: MB-1_120S10A Solids, Total Dissolved TDS @ 180 C Method Blank NO mg/L Sample 10: LCS-2_120S10A Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1090 mg/L Sample 10: C120S041S-007A OUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 1140 mg/L Sample 10: C120S041S-00SA MS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 18200 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 09/05/12 Work Order: C 12080469 RL %REC Low Limit High Limit Run: BAL-1_120810A 10 Run: BAL-1_120810A 10 98 90 110 Run: BAL-1 120810A 10 Run: BAL-1_120810A 10 99 90 110 NO - Not detected at the reporting limit. RPO RPOLimit Qual 0.2 Batch: TDS120810A 08/10/12 12:31 08/10/12 12:31 08/10/12 12:55 5 08/10/12 12:55 Page 13 of 21 EI'.ERGY LABORATORIES www.energyJab.com Analytical ExcslisnclJ SiRcIJ '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • Col/ege Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA)' Inc Project: August Monthly Groundwater 2012 Analyte Count Result Method: E200.8 Units RL %REC Low Limit Report Date: 09/05/12 Work Order: C 12080469 High Limit RPO RPOLimit Qual Analytical Run: ICPMS4-C_120827A Sample 10: ICV 4 Initial Calibration Verification Standard 08/27/1220:03 Manganese 0.0495 mg/L Selenium 0.0507 mg/L Thallium 0.0501 mg/L Uranium 0.0507 mg/L Method: E200.8 Sample 10: C12080469-008AMS 4 Sample Matrix Spike Manganese 2.19 mg/L Selenium 0.0552 mg/L Thallium 0.0564 mg/L Uranium 0.120 mg/L Sample 10: C12080469-008AMSO 4 Sample Matrix Spike Duplicate Manganese 2.26 mg/L Selenium 0.0559 mg/L Thallium 0.0594 mg/L Uranium 0.126 mg/L Sample 10: LRB 4 Method Blank Manganese NO mg/L Selenium NO mg/L Thallium NO mg/L Uranium NO mg/L Sample 10: LFB 4 Laboratory Fortified Blank Manganese 0.0528 mg/L Selenium 0.0516 mg/L Thallium 0.0537 mg/L Uranium 0.0525 mg/L Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. 0.0010 99 90 110 0.0010 101 90 110 0.0010 100 90 110 0.00030 101 90 110 Batch: R163876 Run: ICPMS4-C_120827A 08/27/1218:14 0.0010 70 130 A 0.0010 110 70 130 0.0010 112 70 130 0.00030 100 70 130 Run: ICPMS4-C_120827A 08/27/1218:18 0.0010 70 130 2.8 20 A 0.0010 111 70 130 1.2 20 0.0010 118 70 130 5.2 20 0.00030 112 70 130 4.9 20 Run: ICPMS4-C_120827A 08/27/1220:25 0.010 0.0050 0.00050 0.00030 Run: ICPMS4-C_120827A 08/27/1220:29 0.0010 106 85 115 0.0010 103 85 115 0.0010 107 85 115 0.00030 105 85 115 A -The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. MDC -Minimum detectable concentration Page 14 of 21 I EN:RGY L ABORATORIES www.energylab.com Analytical ExC81IsncB Sines '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Analyte Count Result Method: E300.0 Units RL Sample 10: ICV-OB1112-10 2 Initial Calibration Verification Standard Chloride 9.84 mg/L 1.0 Sulfate 40.0 mg/L 1.0 Method: E300.0 Sample 10: ICB-OB1112-11 2 Method Blank Chloride NO mg/L 1.0 Sulfate NO mg/L 4.0 Sample 10: LFB-OB1112-12 2 Laboratory Fortified Blank Chloride 9.98 mg/L 1.0 Sulfate 40.1 mg/L 1.0 Sample 10: C120B0462-003AMS 2 Sample Matrix Spike Chloride 13.3 mg/L 1.0 Sulfate 47.6 mg/L 1.0 Sample 10: C120B0462-003AMSO 2 Sample Matrix Spike Duplicate Chloride 13.2 mg/L 1.0 Sulfate 47.6 mg/L 1.0 Qualifiers: Report Date: 09/05/12 Work Order: C12080469 %REC Low Limit High Limit RPO RPOLimit Qual Analytical Run: IC1-C_120811A 08/11/1218:51 98 90 110 100 90 110 Batch: R163208 Run: IC1-C_120811A 08/11/12 19:09 Run: IC1-C_120811A 08/11/12 19:26 100 90 110 100 90 110 Run: IC1-C_120811A 08/14/12 01 :42 105 90 110 102 90 110 Run: IC1-C_120811A 08/14/12 01 :59 103 90 110 1.0 10 102 90 110 0.1 10 RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 15 of 21 EN:RGY L ABORATORIES www.energylab.com Analytical Exes/lsneB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N ND mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.42 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 1.93 mg/L Sample 10: C12080469-005CMS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 3.69 mg/L Sample 10: C12080469-005CMSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 3.61 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 0.10 0.10 0.10 0.10 0.10 Report Date: 09/05/12 Work Order: C12080469 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R163181 Run: TECHNICON_120813A 08/13/12 10:48 Run: TECHNICON_120813A 08/13/12 10:51 97 90 110 Run: TECHNICON_120813A 08/13/1210:53 98 90 110 Run: TECHNICON_120813A 08/13/12 16:33 106 90 110 Run: TECHNICON_120813A 08/13/12 16:36 102 90 110 2.2 10 ND -Not detected at the reporting limit. Page 16 of 21 EN:RGY LABORATORIES www.energylab.com Analytical Excs/lsncB Sines 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-&86-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: August Monthly Groundwater 2012 Analyte Method: E900.1 Sample 10: LCS-GA-OS70 Gross Alpha minus Rn & U Count Result Units Laboratory Control Sample 15.7 pCi/L Report Date: 09/05/12 Work Order: C12080469 RL O/OREC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-1_120820B 78 80 120 Batch: GA-0580 08/30/12 21 :38 S -LCS response is outside of the acceptance range for this analysis. Since the MS, MS, and MSD are acceptable the batch is approved. Sample 10: MB-GA-OS70 Gross Alpha minus Rn & U 3 Method Blank -0.137 Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC 0.195 0.395 pCi/L pCi/L pCi/L Sample 10: C12080464-002EMS Sample Matrix Spike Gross Alpha minus Rn & U 77.2 pCi/L Sample 10: C12080464-002EMSO Sample Matrix Spike Duplicate Gross Alpha minus Rn & U 77.9 pCi/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Run: BERTHOLD 770-1_120820B Run: BERTHOLD 770-1_120820B 123 70 130 Run: BERTHOLD 770-1 120820B - 123 70 130 0.9 NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 08/30/12 21 :38 U 08/30/12 21 :38 08/30/1221 :38 22.4 Page 17 of 21 EN:RGY LABORATORIES www.energylab.com Analytical ExcsllsncB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~mette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/05/12 Project: August Monthly Groundwater 2012 Work Order: C12080469 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R163298 Sample 10: 081312_LCS_ 4 16 Laboratory Control Sample Run: SATURNCA_120814C 08/14/12 12:01 Acetone 110 ug/L 20 109 70 130 Benzene 10 ug/L 1.0 102 70 130 Carbon tetrachloride 8.7 ug/L 1.0 87 70 130 Chloroform 9.0 ug/L 1.0 90 70 130 Chloromethane 8.3 ug/L 1.0 83 70 130 m+p-Xylenes 17 ug/L 1.0 83 70 130 Methyl ethyl ketone 110 ug/L 20 107 70 130 Methylene chloride 7.5 ug/L 1.0 75 70 130 Naphthalene 9.3 ug/L 1.0 93 70 130 o-Xylene 10 ug/L 1.0 104 70 130 Toluene 10 ug/L 1.0 100 70 130 Xylenes, Total 27 ug/L 1.0 90 70 130 Surr: 1 ,2-0ichlorobenzene-d4 1.0 93 80 120 Surr: Oibromofluoromethane 1.0 92 70 130 Surr: p-Bromofluorobenzene 1.0 93 80 130 Surr: Toluene-d8 1.0 102 80 120 Sample 10: 081312_MBLK_6 16 Method Blank Run: SATURNCA_120814C 08/14/1213:14 Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 o-Xylene NO ug/L 1.0 Toh.Jene NO ug/L 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1 ,2-0ichlorobenzene-d4 1.0 91 80 120 Surr: Oibromofluoromethane 1.0 89 70 130 Surr: p-Bromofluorobenzene 1.0 90 80 120 Surr: T oluene-d8 1.0 92 80 120 Sample 10: C12080469-0050MS 16 Sample Matrix Spike Run: SATURNCA_120814C 08/14/12 19:54 Acetone 100000 ug/L 10000 104 70 130 Benzene 11000 ug/L 500 111 70 130 Carbon tetrachloride 10000 ug/L 500 100 70 130 Chloroform 13000 ug/L 500 109 70 130 Chloromethane 10000 ug/L 500 102 70 130 m+p-Xylenes 18000 ug/L 500 . 91 70 130 Methyl ethyl ketone 99000 ug/L 10000 99 70 130 Methylene chloride 8300 ug/L 500 83 70 130 Naphthalene 8700 ug/L 500 87 70 130 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 18 of 21 EN:RGY LABORATORIES www.energylab.com Analytical ExcsllsncB Sines 1952 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/05/12 Project: August Monthly Groundwater 2012 Work Order: C12080469 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R 163298 Sample 10: C12080469-0050MS 16 Sample Matrix Spike Run: SATURNCA_120814C 08/14/12 19:54 o-Xylene 11000 ug/L 500 111 70 130 Toluene 11000 ug/L 500 109 70 130 Xylenes, Total .29000 ug/L 500 97 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 90 80 120 Surr: Dibromofluoromethane 1.0 92 70 130 Surr: p-Bromofluorobenzene 1.0 97 80 120 Surr: Toluene-d8 1.0 98 80 120 Sample 10: C12080469-0050MSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_120814C 08/14/12 20:30 Acetone 100000 ug/L 10000 105 70 130 0.8 20 Benzene 11000 ug/L 500 111 70 130 0.0 20 Carbon tetrachloride 10000 ug/L 500 100 70 130 0.8 20 Chloroform 13000 ug/L 500 104 70 130 3.8 20 Chloromethane 11000 ug/L 500 107 70 130 5.4 20 m+p-Xylenes 19000 ug/L 500 97 70 130 6.4 20 Methyl ethyl ketone 100000 ug/L 10000 101 70 130 1.6 20 Methylene chloride 8800 ug/L 500 88 70 130 6.1 20 Naphthalene 10000 ug/L 500 100 70 130 14 20 o-Xylene 11000 ug/L 500 114 70 130 2.5 20 Toluene 11000 ug/L 500 107 70 130 1.8 20 Xylenes, Total 31000 ug/L 500 102 70 130 4.9 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 93 80 . 120 0.0 10 Surr: Dibromofluoromethane 1.0 91 70 130 0.0 10 Surr: p'~Bromofluorobenzene 1.0 95 80 120 0.0 10 Surr: Toluene-d8 1.0 97 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 19 of 21 EI'.ERGY LABORATORIES ~J'" www.~nergylab.com ~ Analytical ExcsUsnce Sines 7952 Helena, MT 877 -472-0711 .. Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gifle~e, WY 866-686-7175 • Rapid City, S[) 888-672-1225 . College Station, TX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 8/10/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper containeribottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ) (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 'fes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.0'C Yes 0 Yes 0 C12080469 Date Received: 8/10/2012 Received by: th No D No D No D No D No D No D No D No D No D No D No D No D No D Carrier FedEx name: Not Present D Not Present D Not Present 0 Not Applicable D No VOA vials submitted D Not Applicable D Page 20 of 21 EN:RGY mJ" Chain of Custody and Analytical Request Record PLEASE PRI NT lfrovide as much information _as possibfe.l Page _1_ of _1 _ Company Nam~(1Gr ~ "F" v-el s. Project Name, PWS, Permit, Etc. I Sample Origin A V\~~~+ Mo()+h~ G~rc.}l.AndlN~et State: U"'- EPA/State Compliance: Yes ~ No 0 Report Mail Address: pO J3.0X 80C{ 51~t)dl"~ UI ~ Y5lt Invoice Address: s.t\me ~ Special ReporVFormats: DDW o EDD/EDT(Electronic Data) o POTVVNVWTP Format: ___ _ o State: D LEVEL IV D Other: ----D NELAC Contact Name: (,."".-('; f\ f 0..\ ,.,... er Invoice Contact & Phone: Phone/Fax: t435 b 7g ..2:2..2.' D"v ~J -f",rk L\3S b 78 .:2:2:21 3: ~ W@O@ OO~@QD~rn[Q) Cl .... ~o (I)~ ~a.l;gOI <u C ._> ° >om Bcncnro~ W c "U5(1» :r: o~= ~ 0) '" u>Ooc: ....., '0 « ~Iffil ~ « ... (Jj S c: -;;:: ../ .-: ~ Cl. col~ Cl ',::) I-E~j9 I ,C « :::I 0)--CI.> 3: v z 15.:«1 arc V -w E >1 .-t-: ~ w ~ 6 .... '-.J,lC/) i-------------,-------r------t----1 t+ 0 .~ £ -s:. 4,.. oS SAMPLE IDENTIFICATION MATRIX 1 . == (Name, Location, Interval, etc.) \J ~ M\V-3LD~O~.2DI~ 18'/~/20)21_13)S I ~-W I~L2<J)(1 j( I I I I I If Mw-;l'5_CgO':;tO'~ 1&/b/~11 )110 11 '-W :x 3~h"'''H ... 0&0720,2. Ig/7/;2.0j~ll l30 It ... vJ :i M W ")4~~071.c>r2.. _ Ig/7/.z.o)::2.ll~1 1)-W x 5f4W-.l(;,_DgOg2.0\~ Ig/g/2.0\:2II33\ I&-w xiI< ~I~ X I.· 6MW---=3CLOgcn~or:t IWj/~OI:lI\D.J.S 13-w II< ~I~ )( :N) vJ -~S_OftOg;2.0l:2. --' g/g/:tol2..1 08:35 11-W )( LX L IX IX~ Email: Sampler: (Please Print)· --r;.nnu tio}} I;)'" if Purchase Order: Quote/Bottle Order: • ~I R ... -"C c: e I U ro c '-:::::I ~ 1 5 ro "C c: ~I H Contact ELI prior to RUSH sample submittal for charges and scheduling -See I nstruction Page Comments: ReceiPtT'tB tlti z;c On Ice: (jJN Custody Seal OnBottle ~ N On Cooler N Intact N Signature Y N Match ~ !~ ~ ~ I~ ~. ~ I~ 8M\U-b~-_O~0720tl Ig/7/2J)12i132.1 11-W [Xl .. d£cICnh~d;~ I:?a\ber -14&>/:;l. &-J l[£ (6l "U I~if Blo..l1l5. (071./ ~ IKlfS/.:l..GJ2. ~ 10 t!P~b'J~q (l) I\.) .... o -Custody I Relinquished by (prin~): DatelTime: ·Sign~ure: "'-;'n(h~r ~on,rllA.U~,.Ot2. 'DOC _}I.IA~'11' lL/J.L Received by (print): DatelTime: Signafure: Oate/Time: ; Record Relinquished by (print): :oJ DatelTime: . ~~Signature: 0 ReC9ived ~ IMUSTbe~--------------------------------~~~~~~--~~------~~~~~~~~ Ime" bv (Drint): Signed Sample Disposal: Retur~!Q Client: Lab Disposal: . In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to c~e the-anal;SiS r~qUeS~ed. This serves as notice of this possibility. All sub·contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule. forms, and links. TabF2 Laboratory Analytical Reports -Accelerated Monitoring September 2012 EN:RGY LABORATORIES www.energylab.com Analytical ExCllHBfIC. Sincs '952 Hale,na, MT 877~472"D711 • Billings, MT 800-735-4489 • Casper, WY 888 .. 235-0515 A~ille.~a, W:Y8.6~&86·7n5 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 LablD: C12090804-001 Client Sample ID: MW-11_09192012 Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 130 ug/l Qualifier RL 10 Report Date: 10/17/12 Collection Date: 09/19/12 13:45 DateReceived: 09/21/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E200.8 10105/12 13:181 smm MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 22 M · WWN.energylab.com ~ H.elen .•• Mf 611472-0711 • Billings, Mf 801·7354489 • Casper, W'/ 888·235-0515 ~ Analytical ExCBHBilCfI Sines '952 L~ -~ill~~a, WY8~6~6B6-7175 • Rapid City, SI} 888-672-1225 • College Station, TX 888-690-2218 EI\ERGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Lab 10: C 12090804-002 Client Sample 10: MW-14_09182012 Report Date: 10/17/12 Collection Date: 09/18/12 14:30 DateReceived: 09/21/12 Matrix: Aqueous Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2140 ug/l MCL! Qualifier RL QCL Method Analysis Date 1 By 10 E200.8 10/05/12 13 :23 1 smm MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 22 EN:RGY LABORATORIES www.energyJab.com Analytical Excsnsnc. Sines '152 'Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 ;~ijle,ti:Q, WY866~686-7n5 • Rapid City, SI} 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Lab ID: C 12090804-003 Client Sample ID: MW-25_09182012 Analyses METALS -DISSOLVED Uranium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 6.01 ug/l Qualifier RL 0.30 Report Date: 10/17/12 Collection Date: 09/18/12 11 :55 DateReceived: 09/21/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By E200.8 10105/12 12:141 smm MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 50f22 El\.ERGY LABORATORIES www.energylab.com Analytical ExcsUsnc. Sines ,m Helena, MT 877-472-0711 • Billings, MT 800 .. 735-4489 • Casper, WY 888-235-0515 ~flle.ttQ, Wy 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 LablD: C 12090804-004 Client Sample ID: MW-26_09192012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N METALS -DISSOLVED Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 67 1.8 64.9 NO NO NO 2300 NO NO 10 NO NO NO 104 108 111 114 0-RL increased due to sample matrix. Units mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 10/17/12 Collection Date: 09/19/12 14:10 DateReceived: 09/21/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By 0 2 E300.0 09/25/12 20:21 1 wc 0.1 E353.2 09/27/1216:08 fiji 0.30 E200.8 10105/12 12:161 smm H 20 SW8260B 10106/12 06:501 jlr H 1.0 SW8260B 10106/12 06:50 1 jlr H 1.0 SW8260B 10106/1206:501 jlr OH 100 SW8260B 10104/1203:141 jk H 1.0 SW8260B 10106/12 06:501 jlr H 20 SW8260B 10106/12 06:501 jlr H 1.0 SW8260B 10106/12 06:501 jlr H 1.0 SW8260B 10106/12 06:50 1 jlr H 1.0 SW8260B 10106/12 06:50 1 jlr H 1.0 SW8260B 10106/1206:501 jlr H 80-120 SW8260B 10106/12 06:501 jlr H 70-130 SW8260B 10106/12 06:501 jlr H 80-120 SW8260B 10106/12 06:501 jlr H 80-120 SW8260B 10106/12 06:501 jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. H -Analysis performed past recommended holding time. Page 60f22 EN:RGY LABORATORIES www.energyJab.com Analytical ExCSnBflCi Sines 1m Helena, MT 817-472-0711 • Billings, MY 800~735-448g • Casper, W'f 888-235-0515 :~iII~tt~, wY8GS .. &86·7115 • Rapid City, SI} 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Lab 10: C 12090804-005 Client Sample 10: MW-30_09192012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N METALS -DISSOLVED Selenium Uranium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 130 16 41.9 7.67 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l Report Date: 10/17/12 Collection Date: 09/19/12 11 :30 DateReceived: 09/21/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date I By E300.0 1 0/15/12 22 :41 1 wc D 2 E353.2 09/27/12 16:11 Iljl 5.0 E200.8 10105/1213:271 smm 0.30 E200.8 10105/12 13:27 1 smm MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 7of22 EN:R(iY LABORATORIES www.energylab.com Analytical ExCSnBflCB Sincs 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 .. ;§i!leJte, WYB66-686-7175 • Rapid City, Sf} 888-&12-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 LablD: C 12090804-006 Client Sample ID: MW-31_09182012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Sulfate PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 172 mg/l 21 mg/l 561 mg/l 1460 mg/l o -Rl increased due to sample matrix. Report Date: 10/17/12 Collection Date: 09/18/12 13:30 DateReceived: 09/21/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By o o 2 4 10 E300.0 E353.2 E300.0 A2540 C MCl -Maximum contaminant level. 09/25/12 20:561 wc 09/27/1216:13/1jl 09/25/12 20:56 1 wc 09/24/12 16:051 ab NO -Not detected at the reporting limit. Page 80f22 EI\ERGY LABORATORIES www.energylab.com Analytical ExCBJIBilC. Sincs , d52 Helena, MY 871-472-071 f • Billings, MT 800 .. 735-4489 " Casper, WV 888-235-0515 '§illefte, WY86& .. 686~7n5 • Rapid City, 51) 888-672-1225 • College station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 LablD: C12090804-007 Client Sample ID: MW-35_09192012 Analyses METALS -DISSOLVED Manganese Selenium Thallium Uranium . RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 283 ug/l 8.2 ug/l 0.54 ug/l 22.9 ug/l 5.4 pCi/l 0.6 pCi/l 0.2 pCi/l MOC -Minimum detectable concentration Qualifier RL 10 5.0 0.50 0.30 Report Date: 10/17/12 Collection Date: 09/19/12 09:15 DateReceived: 09/21/12 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By E200.8 10105/12 13:32 I smm E200.8 10105/12 13:32 I smm E200.8 10105/12 13:32 I smm E200.8 10105/12 13:32 I smm E900.1 1 0104/12 08 :32 I Ibb E900.1 10104/12 08:32 I Ibb E900.1 10104/12 08:32 I Ibb MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 22 EI\ERGY LABORATORIES www.energylab.com AnaIytiCliI Excsllsnc. Sincs '952 Helena, Mt 877-412-0711 • Billings. MT 800-735-4489 . Casper, WY 888-235-0515 '~i·lIe.jfe, wy 866~686~7n5 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Lab ID: C 12090804-008 Client Sample ID: MW-65_09192012 Analyses METALS -DISSOLVED Manganese Selenium Thallium Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 273 ug/l 9.7 ug/l NO ug/l 22.6 ug/l 6.0 pC ill 0.6 pCi/l 0.2 pCi/l MOC -Minimum detectable concentration Qualifier Rl 10 5.0 0.50 0.30 Report Date: 10/17/12 Collection Date: 09/19/12 09:15 DateReceived: 09/21/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By E200.8 10105/12 13:36 1 smm E200.8 10105/12 13:361 smm E200.8 10105/12 13:361 smm E200.8 10105/12 13:361 smm E900.1 1 0104/12 08 :32 1 Ibb E900.1 1 0104/12 08 :32 1 Ibb E900.1 10104/12 08:321 Ibb MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ExCSOIfflCB Sincs 7952 _Helena,MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, W'{ 888-235-0515 '~ille.t;ta, ¥lYSi6-G86-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 LablD: C 12090804-009 Client Sample ID: Trip Blank 6746 Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L 102 %REC 102 %REC 107 %REC 117 %REC H -Analysis performed past recommended holding time. Report Date: 10/17/12 Collection Date: 09/19/12 DateReceived: 09/21/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By H 20 SW8260B 10105/12 16:221 jlr H 1.0 SW8260B 10105/12 16:221 jlr H 1.0 SW8260B 10105/12 16 :22 1 jlr H 1.0 SW8260B 10105/12 16 :22 1 jlr H 1.0 SW8260B 10105/12 16:221 jlr H 20 SW8260B 10105/12 16:22 1 jlr H 1.0 SW8260B 10105/12 16:22 1 jlr H 1.0 SW8260B 10105/12 16:221 jlr H 1.0 SW8260B 10105/12 16:221 jlr H 1.0 SW8260B 10105/12 16:221 jlr H 80-120 SW8260B 10/05/12 16:22/ jlr H 70-130 SW8260B 10/05/12 16:22/ jlr H 80-120 SW8260B 10/05/12 16:22/ jlr H 80-120 SW8260B 10/05/12 16:22/ jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 11 of 22 EI\ERGY LABORATORIES www.energylab.com Analytical ExcsHBfIC' Sines J952 Helena, MY 877-472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 ~il,Ie.#e, WY866~686~7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Lab 10: C12090804-010 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.0 Qualifier RL Report Date: 10/17/12 Collection Date: 09/20/12 DateReceived: 09/21/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E170.1 09/21/1209:30/ kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Extsllsnl:s SiOCll 1952 Helena,. MT 877 .. 472 .. 0711 • Billings, MT 800 .. 735-4489 • Casper, WY 888-235-0515 ~iO~#e, WY~8.6 .. 686 .. 7175 • Rapid City, SI} 888-672-1225 • College Station, IX 888-690 .. 2218 ANALYTICAL SUMMARY REPORT October 17, 2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12090804 Quote ID: C1640 -POC Wells Project Name: September Monthly Groundwater 2012 Energy Laboratories, Inc. Casper WY received the following 10 samples for Energy Fuels Resources (USA) Inc on 9/21/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12090804-001 MW-11_09192012 09/19/1213:45 09/21/12 Aqueous Metals by ICP-MS, Dissolved C 12090804-002 MW-14_09182012 09/18/12 14:30 09/21/12 Aqueous Same As Above C 12090804-003 MW-25_09182012 09/18/12 11 :55 09/21/12 Aqueous Same As Above C 12090804-004 MW-26_09192012 09/19/1214:10 09/21/12 Aqueous E300.0 Anions Metals by ICP-MS, Dissolved Nitrogen, Nitrate + Nitrite SW8260B VOCs, Standard List C 12090804-005 MW-30_09192012 09/19/12 11 :30 09/21/12 Aqueous E300.0 Anions Metals by ICP-MS, Dissolved Nitrogen, Nitrate + Nitrite C12090804-006 MW -31_09182012 09/18/12 13:30 09/21/12 Aqueous E300.0 Anions Nitrogen, Nitrate + Nitrite Solids, Total Dissolved C12090804-007 MW-35_09192012 09/19/12 9:15 09/21/12 Aqueous Metals by ICP-MS, Dissolved Gross Alpha minus Rn222 and Uranium C12090804-008 MW-65_09192012 09/19/12 9:15 09/21/12 Aqueous Same As Above C 12090804-009 Trip Blank 6746 09/19/12 0:00 09/21/12 Aqueous SW8260B VOCs, Standard List C12090804-010 Temp Blank 09/20/12 0:00 09/21/12 Aqueous Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ D LJtA1~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.10.17 14:06:51 -06:00 Page 1 of 22 www.energylab.com Analytical ExC81fsnCB Sim;s 1852 Helena, MT 877 .. 472 .. 0711 • Billings, MT 800 .. 735-4489 • Casper, WY 888-235-0515 -~·illette,WY866 .. 686-7175 • Ra id City, so 888-&72-1225 • College Station, IX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Report Date: 10/17/12 Sample Delivery Group: C12090804 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4CC (±2CC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 22 EN:RGY LABORATORIES www.energyJab.com Analytical Excslillflca Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888 .. 235-0515 .~illettl!, WY 866-686-7175 • Rapid City, SI) 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Analyte Count Result Units Method: A2540 C Sample 10: MB-1_120924A Method Blank Solids, Total Dissolved TDS @ 180 C ND mg/L Sample 10: LCS-2_120924A Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 990 mg/L Sample 10: C12090797-011A OUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 349 mg/L Sample 10: C12090797-012A MS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 1210 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 10 10 10 10 Report Date: 10/17/12 Work Order: C12090804 O/OREC Low Limit High Limit RPO RPOLimit Qual Batch: TDS 120924A Run: BAL-1_120924B 09/24/12 15:39 Run: BAL-1_120924B 09/24/12 15:40 99 90 110 Run: BAL-1 120924B 09/24/12 16:04 1.7 5 Run: BAL-1_120924B 09/24/12 16:04 97 90 110 ND -Not detected at the reporting limit. Page 13 of 22 EI'.ERGY www.energyJab.com ~ Helena, MlB77-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ) ...... ~_~::L. .~illett-e, WY .&& ... 686-7175 • Rapid City, SO 888-672-1225 • College Station, lX 888-690-2218 LABORATORIES Analyt/csl ExCIII/enc, SinClI '952 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Report Date: 10/17/12 Work Order: C 12090804 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.8 Sample 10: ICV Uranium Method: E200.8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: C12090801-0040MS Uranium Sample 10: C12090801-0040MSO Uranium Method: E200.8 Sample 10: ICV Manganese Selenium Thallium Uranium Method: E200.8 Sample 10: LRB Manganese Selenium Thallium Uranium Sample 10: LFB Manganese Selenium Thallium Uranium Sample 10: C12090617-003BMS4 Manganese Selenium Thallium Uranium Sample 10: C12090617-003BMSO Manganese Selenium Thallium Uranium Qualifiers: RL -Analyte reporting limit. 4 4 4 4 4 MDC -Minimum detectable concentration Analytical Run: ICPMS2-C _121 005A Initial Calibration Verification Standard 10/05/12 11 :51 0.0537 mg/L 0.00030 107 90 110 Batch: R 165485 Method Blank Run: ICPMS2-C_121005A 10/05/12 12:05 NO mg/L 0.00030 Laboratory Fortified Blank Run: ICPMS2-C_121005A 10/05/1212:06 0.0519 mg/L 0.00030 104 85 115 Sample Matrix Spike Run: ICPMS2-C_121005A 10/05/12 15:35 0.0784 mg/L 0.00030 109 70 130 Sample Matrix Spike Duplicate Run: ICPMS2-C_121005A 10/05/12 15:37 0.0778 mg/L 0.00030 108 70 130 0.9 20 Analytical Run: ICPMS4-C_121005A Initial Calibration Verification Standard 10/05/12 12:30 0.0496 mg/L 0.0010 99 90 110 0.0514 mg/L 0.0010 103 90 110 0.0503 mg/L 0.0010 101 90 110 0.0503 mg/L 0.00030 101 90 110 Batch: R165489 Method Blank Run: ICPMS4-C_121005A 10/05/12 13:05 NO mg/L 0.010 NO mg/L 0.0050 NO mg/L 0.00050 NO mg/L 0.00030 Laboratory Fortified Blank Run: ICPMS4-C_121005A 10/05/12 13:10 0.0518 mg/L 0.0010 104 85 115 0.0527 mg/L 0.0010 105 85 115 0.0514 mg/L 0.0010 103 85 115 0.0514 mg/L 0.00030 102 85 115 Sample Matrix Spike Run: ICPMS4-C_121005A 10/05/12 18:52 0.0855 mg/L 0.0010 93 70 130 0.0447 mg/L 0.0010 89 70 130 0.0534 mg/L 0.00050 107 70 130 0.0565 mg/L 0.00030 111 70 130 Sample Matrix Spike Duplicate Run: ICPMS4-C_121005A 10/05/12 18:56 0.0827 mg/L 0.0010 87 70 130 3.3 20 0.0446 mg/L 0.0010 89 70 130 0.3 20 0.0525 mg/L 0.00050 105 70 130 1.9 20 0.0552 mg/L 0.00030 108 70 130 2.2 20 NO -Not detected at the reporting limit. Page 14 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ExCSI/snCII Sines 1952 f Helena, MTB77-472-D711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~illet:t~, 'NY 8&6-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Report Date: 10/17/12 Work Order: C12090804 Analyte Count Result Units RL %REC Low Limit High Limit Method: E300.0 Sample 10: ICV-092412-10 Chloride Sulfate Method: E300.0 Sample 10: ICB-092412-11 Chloride Sulfate Sample 10: LFB-092412-13 Chloride Sulfate Sample 10: LFBO-092412-14 Chloride Sulfate Sample 10: C12090797-012AMS Chloride Sulfate Sample 10: C12090797-012AMSO Chloride Sulfate Method: E300.0 Sample 10: ICV Chloride Method: E300.0 Sample 10: ICB Chloride Sample 10: LFB Chloride Sample 10: C12100562-001AMS Chloride Sample 10: C12100562-001AMSO Chloride 2 Initial Calibration Verification Standard 9.74 mg/L 1.0 40.3 mg/L 1.0 2 Method Blank ND mg/L 1.0 ND mg/L 4.0 2 Laboratory Fortified Blank 9.65 mg/L 1.0 39.8 mg/L 1.0 2 Laboratory Fortified Blank Duplicate 9.64 mg/L 1.0 39.7 mg/L 1.0 2 Sample Matrix Spike 11.4 mg/L 1.0 58.8 mg/L 1.0 2 Sample Matrix Spike Duplicate 11.8 mg/L 1.0 60.4 mg/L 1.0 Initial Calibration Verification Standard 9.99 mg/L 1.0 Method Blank ND mg/L 1.0 Laboratory Fortified Blank 10.0 mg/L 1.0 Sample Matrix Spike 26.2 mg/L 1.0 Sample Matrix Spike Duplicate 26.3 mg/L 1.0 97 101 97 100 96 99 99 101 103 106 100 100 98 99 90 90 110 110 Run: IC2-C_120924B Run: IC2-C_120924B 90 110 90 110 Run: IC2-C_120924B 90 110 90 110 Run: IC2-C_120924B 90 110 90 110 Run: IC2-C_120924B 90 110 90 110 90 110 Run: IC2-C_121015A Run: IC2-C_121015A 90 110 Run: IC2-C_121015A 90 110 Run: IC2-C 121015A - 90 110 RPO RPOLimit Qual Analytical Run: IC2-C_120924B 09/24/12 17:03 3.3 2.7 Batch: R 165020 09/24/12 17:21 09/24/12 17:56 09/24/12 18:13 09/25/12 19:29 09/25/12 19:46 10 10 Analytical Run: IC2-C_121 015A 10/15/12 12:09 Batch: R 165865 10/15/12 12:25 10/15/12 12:40 10/15/12 23:59 10/16/12 00:14 0.4 10 -------------_._-----------_._-------------_._----------------------------------------------- Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 15 of 22 EN:RGY LABORATORIES www.energylab.com ~Helena.MT877-472-0711 .Billings.MT 800-735-4489 . Casper, WV 888-235-0515 AnaIyticaIExcsllsncBSincs1952 L .'1.,;:i .:§ille,:te, %.'.866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N ND mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.56 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 2.01 mg/L Sample 10: C12090797-0090MS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 36.5 mg/L -Matrix spike recoveries outside the acceptance range are considered matrix-related. Sample 10: C12090797-0090MSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 35.8 mg/L -Matrix spike recoveries outside the acceptance range are considered matrix-related. Qualifiers: RL -Analyte reporting limi!. MDC -Minimum detectable concentration Report Date: 10/17/12 Work Order: C 12090804 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R165111 Run: TECHNICON_120927A 09/27/12 11 :36 0.10 Run: TECHNICON_120927A 09/27/12 11 :38 0.10 102 90 110 Run: TECHNICON_120927A 09/27/12 11 :41 0.10 102 90 110 Run: TECHNICON_120927A 09/27/1215:56 1.0 116 90 110 S Run: TECHNICON_120927A 09/27/12 15:58 1.0 113 90 110 1.9 10 S ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 16 of 22 EN:RGY LABORATORIES ~ ___ I www.energylab.com Analytical ExcsUSflca Sines 1952 Helena, MTB77-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~illette, WY 866-&86-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: September Monthly Groundwater 2012 Analyte Count Result Units Method: E900.1 Sample 10: LCS-GA-0587 Gross Alpha minus Rn & U Sample 10: MB-GA-0587 Gross Alpha minus Rn & U Laboratory Control Sample 19.4 pCi/L 3 Method Blank 0.141 Gross Alpha minus Rn & U Precision (±) 0.312 pCi/L pCi/L pCi/L Gross Alpha minus Rn & U MDC 0.497 Sample 10: C12090790-0020MS Gross Alpha minus Rn & U Sample 10: C12090790-0020MSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Sample Matrix Spike 42.9 pCi/L Sample Matrix Spike Duplicate 40.5 pCi/L Report Date: 10/17/12 Work Order: C12090804 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_120927A 93 80 120 Run: BERTHOLD 770-2_120927 A Run: BERTHOLD 770-2_120927A 105 70 130 Run: BERTHOLD 770-2_120927A 96 70 130 5.7 NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: GA-0599 10104/1206:56 10104/12 06:56 U 10104/12 06:56 10104/12 06:56 25.5 Page 17 of 22 EN:RGY LABORATORIES www.energyJab.com AnalyticalExcsllBflcB Sines '.952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .·~iil~~~, 'NY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 10/17/12 Project: September Monthly Groundwater 2012 Work Order: C12090804 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R165488 Sample 10: 05-0ct-12_LCS_ 4 15 Laboratory Control Sample Run: GCMS2_121 005A 10/05/12 14:04 Benzene 11 ug/L 1.0 109 70 130 Carbon tetrachloride 11 ug/L 1.0 110 70 130 Chloroform 10 ug/L 1.0 103 70 130 Chloromethane 12 ug/L 1.0 122 70 130 m+p-Xylenes 21 ug/L 1.0 105 70 130 Methyl ethyl ketone 80 ug/L 20 80 70 130 Methylene chloride 9.6 ug/L 1.0 96 70 130 Naphthalene 11 ug/L 1.0 112 70 130 o-Xylene 11 ug/L 1.0 111 70 130 Toluene 11 ug/L 1.0 115 70 130 Xylenes, Total 32 ug/L 1.0 107 70 130 Surr: 1 ,2-0ichlorobenzene-d4 1.0 96 80 120 Surr: Oibromofluoromethane 1.0 97 70 130 Surr: p-Bromofluorobenzene 1.0 98 80 130 Surr: T 0luene-d8 1.0 113 80 120 Sample 10: 05-0ct-12_MBLK_6 15 Method Blank Run: GCMS2_121005A 10/05/12 15:13 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 o-Xylene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1 ,2-0ichlorobenzene-d4 1.0 103 80 120 Surr: Oibromofluoromethane 1.0 95 70 130 Surr: p-Bromofluorobenzene 1.0 106 80 120 Surr: Toluene-d8 1.0 118 80 120 Sample 10: C12090918-004AMS 15 Sample Matrix Spike Run: GCMS2 -121005A 10/05/12 21 :00 Benzene 220 ug/L 10 108 70 130 Carbon tetrachloride 230 ug/L 10 114 70 130 Chloroform 210 ug/L 10 107 70 130 Chloromethane 220 ug/L 10 110 70 130 m+p-Xylenes 400 ug/L 10 101 70 130 Methyl ethyl ketone 1600 ug/L 200 78 70 130 Methylene chloride 200 ug/L 10 98 70 130 Naphthalene 200 ug/L 10 100 70 130 o-Xylene 210 ug/L 10 107 70 130 Toluene 240 ug/L 10 118 70 130 Xylenes, Total 620 ug/L 10 103 70 130 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 18 of 22 EN:RGY LABORATORIES www.energyJab.com Analytical ExcsllsncB SInes '952 Helena, MT 877'-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~Gillet,i:e, Wv 866 .. 686-7175 • Rapid City, SO 888-672-1225 • Coilege Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 10/17/12 Project: September Monthly Groundwater 2012 Work Order: C12090804 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R 165488 Sample 10: C12090918-004AMS 15 Sample Matrix Spike Run: GCMS2_121 005A 10/05/12 21 :00 Surr: 1 ,2-Dichlorobenzene-d4 1.0 97 80 120 Surr: Dibromofluoromethane 1.0 102 70 130 Surr: p-Bromofluorobenzene 1.0 98 80 120 Surr: Toluene-d8 1.0 115 80 120 Sample 10: C12090918-004AMSO 15 Sample Matrix Spike Duplicate Run: GCMS2 -121005A 10/05/1221 :35 Benzene 220 ug/L 10 110 70 130 2.2 20 Carbon tetrachloride 230 ug/L 10 115 70 130 0.7 20 Chloroform 220 ug/L 10 109 70 130 1.5 20 Chloromethane 230 ug/L 10 116 70 130 5.3 20 m+p-Xylenes 400 ug/L 10 101 70 130 0.2 20 Methyl ethyl ketone 1600 ug/L 200 79 70 130 2.0 20 Methylene chloride 200 ug/L 10 101 70 130 3.2 20 Naphthalene 240 ug/L 10 119 70 130 18 20 o-Xylene 220 ug/L 10 108 70 130 0.7 20 Toluene j 240 ug/L 10 118 70 130 0.3 20 Xylenes, Total 620 ug/L 10 103 70 130 0.4 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 98 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 98 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 100 80 120 0.0 10 Surr: Toluene-d8 1.0 112 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 19 of 22 EI'.ERGY LABORATORIES www.energylab.com Analytical Excs/lsncB Sinu 1952 Helena, MlB77-412-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 ,:ijIlJe#Bc, wx ,866 .. 686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 10/17/12 Project: September Monthly Groundwater 2012 Work Order: C12090804 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R165644 Sample 10: 100312_LCS_11 5 Laboratory Control Sample Run: SATURNCA_121003B 10103/12 23:02 Chloroform 10 ug/L 1.0 105 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 100 80 120 Surr: Oibromofluoromethane 1.0 106 70 130 Surr: p-Bromofluorobenzene 1.0 102 80 130 Surr: Toluene-d8 1.0 102 80 120 Sample 10: 100312_MBLK_19 5 Method Blank Run: SATURNCA_121003B 10104/1200:14 Chloroform ND ug/L 1.0 Surr: 1 ,2-Dichlorobenzene-d4 1.0 98 80 120 Surr: Dibromofluoromethane 1.0 108 70 130 Surr: p-Bromofluorobenzene 1.0 96 80 120 Surr: Toluene-d8 1.0 99 80 120 Sample 10: C12090804-0040MS 5 Sample Matrix Spike Run: SATURNCA_121003B 10104/1203:50 Chloroform 4200 ug/L 100 96 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 106 80 120 Surr: Dibromofluoromethane 1.0 113 70 130 Surr: p-Bromofluorobenzene 1.0 107 80 120 Surr: T 0luene-d8 1.0 100 80 120 Sample 10: C12090804-0040MSO 5 Sample Matrix Spike Duplicate Run: SATURNCA_121003B 10104/12 04:26 Chloroform 4400 ug/L 100 106 70 130 4.6 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 98 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 111 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 98 80 120 0.0 10 Surr: Toluene-d8 1.0 103 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 20 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ExCS08llCf SInes '.852 Helen,a; MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515 :9i11~!f~;WY8.6-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Kerri Schroeder Reviewed by: BL2000\smead Reviewed Date: 9/24/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes III Yes III Yes 0 Yes III Yes III Yes III Yes III Yes III Yes III Yes III Yes III 2.0'C Yes III Yes III C12090804 Date Received: 9/21/2012 Received by: ks No 0 No 0 No 0 No 0 No 0 No 0 No D No 0 No 0 No 0 No 0 No 0 No 0 Carrier NDA name: Not Present 0 Not Present 0 Not Present III Not Applicable 0 No VOA vials submitted 0 Not Applicable 0 Page 21 of 22 "U Dl co CD N N Q, N N EI\ERGY mJ-Chain of Custody and Analytical Request Record Page_l_of_' _ ----------- ------------" Company Name: Project Name, PWS, Permit, Etc. ~t:l Sample Origin EPNState Compliance: 'Ener~~ 1=~e.\S S~p+e.mber M,on+~~ G-roV\nd lAJ~ter State: l..tT Yes ~ No 0 Report Mail Address: 1'0 BO)C 80,\ Contact Name: Phone/Fax: Email: Sampler: (Please Print) &\"-t1a;n~ ~T £<LlS\I G-t;\.-rr\ 1\ ? ~ me. J4~5 b78 .22J..1 "1::n n er J.j" JJ /JII,1 Invoice Address;-l Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: -S~'rv1~ P~\)i~ lv.r1( L\3!) b 18 .2.2~J Special Report/Formats: $: ~&lb W®D® OO~®QD~~[Q) .. Contact ELI prior to It;lJo, ,l/bI o .... RUSH sample submittal . ~O(l)~ [ for charges and Cooler 10(s): ' ~(O~OI t C R scheduling -See V/;'tY!i-._> 0 >.15 D OW D EOD/EOT(Electronic Data) ~(/)~ m $: w I nstruction Page a$:= ~ Ol .\1 e J: -0 Receipt Tamp D POTWMlWTP Format: ~~ () t: Comments: ~«~I-g~ ::l U ~,~<T!3 0c o State: D LEVEL IV o .... (01 C -S. « e .... i:ti$§·c ~. -:1; ~ .... ro t: o Other: D NELAC ~ a.cul~ 0 ~ ,.,.. .... r-On Ice: (1)N E~ro I ~ ~ -~C f « ::J ::J (\).~ Q) $: l-S Zo..«1 arc S::"3 .,.-4 ~ ~ (W "E Custody Seal ~ >1 ~~. _.\1 ..... ,_ '$ W ro ~& •• (jN -0 en s: S;1 ~~:E 1f1~~1 c: On Cooler Y N ro C ~-I-..2.£: .. ~A~ en H Intact Y N SAMPLE IDENTIFICATION Collection Collection MATRIX ~ ~ ~ -;5 '\J") 'f. Signature N (Name, Location, Interval, etc.) Date Time Match 1 )-w '" ~ MW"'lt.O'1IC{;lOI2 1'1114/1:1 l~LiS I~ 2AvJ -)Lt_Qq tS<2!)\-:t Iq/IYl2 lL-l ~O . \.-YJ X ~ c~ 3~W-;l.5_0q '~.2.0'2 ' q/If~/l~ )15~ i ~ W\J ~ (Q) Innn lAW-~~q }qtJ.Dl:L. 9/j~/lJ. )'iIO b-W 1-. I~ y.. X ~ 5 /ttw-3tJ. Oqlq~12 Iq /)'\/l:t lj'~ ~-W y.. X i.. ~ I~ ~ 6MvJ -3)_ Dt1I!20\::l. q IJtJ/ll. 1~-;O ~-vJ " 1-"X I~ ~ 7"'W-~_Oq,q2.0a. I~ IIq/l~ OQI.5 )-w 'X ~ X I~ I~ ~ 8MW-b5_ D'lt12£>I:l. qllq/IA IO~'~ ,-w )( )( )( X X ~ ~~'C '&)4.nk (.11'4' 1'1llq~:t I~ I::? 101( ~o1?1&lll ~J~~2t?d-~ I~ Custotty h!;:~bU;\f;~l1 q/~/~i2 JlOtl .:-\ Signatureu b·/ Received by (print): Datemme: Signa ure: Record hA~1fl I \ I Relinquished by (print): '-l DatefTime: Signature: .-.J Received by (print): Datemme: Signature: 1 MUST be ~ ~ ~ Signed P;;:ZJ1I'I};7});A4-Uqpj J/~ tJ~:3() Sign8fure: Sample Disposal: Return to Client: Lab Disposal: I " / In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information. downloadable fee schedule, forms, and links. TabG Quality Assurance and Data Validation Tables G-1A: Routine Field Data QNQC Evaluation , Time Req'd for 2 Time Pumped Amount Well Sample Date . Casings (min) Sufficient? Conductance RPD(%) pH RPD(%) Temll CC) RPD(%) Redox Potential (Eh) RPD(%) . Turbidity (NTU) MW-2 7116/2012 114.16 120 Y 3735 3732 0.08 7.24 7.23 0.14 15.55 15.52 0.19 300 293 2.36 0 0 MW-3 7118/2012 48.69 75 Y 5685 5690 0.09 6.99 6.99 0.00 16.17 16.19 0.12 308 305 0.98 0 0 MW-3A 7119/2012 61.84 65 Pumped dry 5960 5978 0.30 7.07 7.01 0.85 16.52 16.41 0.67 336 330~ 1.80 0 0.9 MW-5 7/16/2012 192.71 200 Y 2937 2941 0.14 7.59 7.6 0.13 16.3 16.26 0.25 163 160 . 1.86 1.6 1.6 MW-11 7/1112012 252.05 275 Y 2800.0 2846.0 1.63 7.76 7.74 0.26 17.03 17.00 0.18 99 97 2.04 0 0 MW-12 7/1712012 132.10 135 Y 4178 4171 0.17 6.99 6.98 0.14 16.08 16.09 0.06 302 298 1.33 11.8 11.6 MW-14 7/11/2012 149.25 180 Y 3935 3928 0.18 6.89 6.89 0.00 15.61 15.60 0.06 218 217 0.46 0 0 MW-15 7/17/2012 183.86 185 Y 4286 4294 0.19 7.05 7.05 0.00 15.46 15.52 0.39 254 252 0.79 0 0 MW-18 7118/2012 384.57 390 Y 3471 3469 0.06 6.64 6.64 0.00 15.94 15.98 0.25 210 207 1.44 2.4 2.4 MW-19 7/19/2012 575.66 598 Y 1782 1782 0.00 7.20 7.21 0.14 14.77 14.85 0.54 310 306 1.30 0 0 MW-23 7/17/2012 130.91 135 Pumped dry 3856 3861 0.13 7.08 7.10 0.28 17.78 18.21 2.39 336 318. 5.50 4.2 4.9 MW-24 7118/2012 38.33 40 Pumped dry 4405 4412 0.16 6.55 6.45 1.54 16.55 16.35 1.22 314 300! 4.56 0.2 0.3 MW-25 7/10/2012 248.26 275 Y 3217 3222 0.16 6.88 6.88 0.00 15.80 15.79 0.06 345 335 2.94 11.7 11.8 MW-26 711112012 Continuously pumped well 3445 NC 7.10 NC 16.20 NC 183 NC 0 MW-26 Resample 8/1612012 Continuously pumped well 3425 NC 6.80 NC 14.95 NC 154 NC 0 MW-27 7/16/2012 262.70 270 Y 1580 1578 0.13 7.40 7.40 0.00 15.02 15 .01 0.07 302 299 1.00 0 0 MW-28 7/16/2012 201.19 210 Y 3965 3970 0.13 6.38 6.38 0.00 15.18 15.17 0.07 358 352 1.69 0 0 MW-28 Resample 8/112012 200.65 230 Y 3944 3939 0.13 5.80 5.81 0.17 15.75 15.72 0.19 316 312 1.27 0 0 MW-29 7/1012012 149.49 150 Y 4598 4620 0.48 6.68 6.68 0.00 16.45 16.41 0.24 182 181 0.55 21.2 21.5 MW-29 Resample 81112012 149.73 160 Y 4578 4585 0.15 6.44 6.45 0.16 15.97 15.89 0.50 192 190 1.05 14.1 14.2 MW-30 7110/2012 204.32 205 Y 2054 2062 0.39 7.25 7.25 0.00 15.50 15.53 0.19 238 235 1.27 0 0 MW-31 7/9/2012 372.54 375 Y 1923 1921 0.10 7.53 7.53 0.00 15.30 15.27 0.20 249 243 2.44 0 0 MW-32 7/9/2012 347.56 360 Y 3906 3910 0.10 6.74 6.72 0.30 15.18 15.19 0.07 184 184 0.00 6.7 6.9 MW-35 7110/2012 72.82 80 Y 4117 4023 2.31 6.87 6.87 0.00 16.94 16.89 0.30 200 198 1.01 0 0 MW-36 7/11/2012 66.50 85 Y 4960 4963 0.06 7.20 7.20 0.00 15.60 15.61 0.06 382 377 1.32 0 0 MW-37 7/3012012 NA 4488 4497 0.20 6.96 6.90 0.87 21.10 19.80 6.36 280 259\ 7.79 4.9 24.5 ifhe QAP states that turbidity should be less than 5 Nephelometric Turbidity .Units ("NTU") prior to sampling unless the well is characterized bywater that has a higher turbidity. The QAP does not require thatturbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. MW-26 IS a contmuously pumped well. Per the QAP, only one set of parameters are required to be collected from continuously pumped wells. ell was Qurged Qry. N I A = The amount of water in the well was insufficient to pump. The pump was not able to operate due to the minimal amount of water. The well was purged and sampled with a bailer. NC = Not calculated. >5NTU RPD(%) N 0.00 N 0.00 N 200.00 N 0.00 N 0.00 Y NC N 0.00 N 0.00 N 0.00 N 0.00 N 15.38 N 40.00 Y 0.85 N NC N NC N 0.00 N 0.00 N 0.00 Y 1.41 Y 0.71 N 0.00 N 0.00 Y 2.94 N 0.00 N 0.00 Y 133.33 RPD >10%. Per the revised QAP Revision 7.2, Attachment 2-3, when a well is purged to dryness, only pH, temperature and specific conductance parameters are required to be within 10% RPD. Redox potential and turbidity paramters are measured for information purposes only and as such are not required to meet the 10% RPD criteria used for pH, specific conductance and temperature .. G-IB: Acelerated Field Data QA/QC Evaluation Time Req'd for 2 Time Pumped Amount Well Sample Date Casings (min) Sufficient? Conductance RPD(%) pH Accelerated January Monthly MW-ll 817/2012 252.5 260 Y 2876 2883 0.24 7.42 7.43 MW-14 817/2012 149.5 161 Y 3892 3883 0.23 6.54 6.58 MW-25 8/6/2012 251.4 255 Y 3221 3226 0.16 6.52 6.55 MW-26 8/8/2012 Continuously pumped well 3136 NC 6.6 MW-30 817/2012 204.7 215 Y 2057 2054 0.15 6.92 6.95 MW-31 8/6/2012 372.3 395 Y 1925 1927 0.10 6.95 6.96 MW-35 8/8/2012 73.1 105 Y 4154 4145 0.22 6.74 6.74 Accelerated March Monthly MW-ll 9119/2012 253.1 255 Y 2876 2881 0.17 7.96 MW-14 9118/2012 149.3 150 Y 3929 3928 0.03 7.10 MW-25 9/18/2012 249.2 265 Y 3235 3225 0.31 6.56 MW-26 9119/2012 Continuously pumped well 3418 NC 7.40 MW-30 9/19/2012 205.5 225 Y 2066 2069 0.15 7.91 MW-31 9/18/2012 373.1 375 Y 1946 1939 0.36 7.10 MW-35 9/19/2012 73.2 80 Y 4166 4172 0.14 6.80 .. .. " " The QAP states that turbIdity should be less than 5 NephelometrIC TurbIdIty Umts ( NTU ) prIor to samplIng unless the well IS characterIzed by water that has a 'higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. MW-26 is a continuously pumped well. 7.91 7.08 6.54 7.85 7.10 6.81 RPD(%) Temp rC) RPD(%) Redox Potential (Eh) RPD(%) Turbidity (NTU) .<5 (NTU) RPD(%) 0.13 16.02 16.27 1.55 134 127 5.36 0 0 y 0.00 0.61 16.07 16.01 0.37 370 359 3.02 0 0 y 0.00 0.46 15.78 15.79 0.06 347 337 2.92 3.0 3.1 Y 3.28 NC 15.71 NC 125 NC 0 Y NC 0.43 15.39 15.38 0.06 313 304 2.92 0 0 y 0.00 0.14 15.90 15.88 0.13 305 295 3.33 2.4 2.4 Y 0.00 0.00 15.15 15.13 0.13 263 251 4.67 0 0 y 0.00 0.63 15.33 15.34 0.07 74 72 2.74 0 0 y 0.00 0.28 15.14 15.20 0.40 80 79 1.26 0 0 y 0.00 0.31 15.00 14.99 0.07 251 253 0.00 0.7 0.7 Y 0.00 NC 15.91 NC 151 NC 1.0 Y NC 0.76 15.31 15.30 0.07 191 196 2.58 0 0 y 0.00 0.00 14.93 14.91 0.13 247 248 0.40 8.9 8.9 N 0.00 0.15 14.60 14.60 0.00 165 165 0.00 0.7 0.7 Y 0.00 G-2A: Holding Time Evaluation ':, <:<" :,' , -<, " e, , , QAPHolding MW-2 MW-3 MW-3A ' Mw-5 Constituent Time 7116/20i2 7/18/2012 711912012 7/16/2012 2-Butanone (MEK) 14 days -------- Acetone 14 days -------- Ammonia (as N) 28 days -------- Arsenic 6 months -------- Benzene 14 days -------- Beryllium 6 months -------- Cadmium 6 months -------- Carbon Tetrachloride 14 days -------- Chloride (mgIL) 28 days -------- Chloroform 14 days -------- Chloromethane 14 days -------- Chromium 6 months -------- Cobalt 6 months -------- Copper 6 months -------- Dichloromethane (Methylene Chloride) 14 days -------- Fluoride (Mg/L) 28 days --5 days ---- Gross Alpha minus Rn & U MDC 6 months 16 days ------ Gross Alpha minus Rn & U Precision (±) 6 months 16 days ------ Gross Alpha minus Rn & U 6 months 16 days ------ Iron 6 months -------- Lab pH (S.u.) ---------- Lead 6 months -------- Manganese 6 months -------- Mercury 28 days -------- Molybdenum 6 months -------- Naphthalene 14 days -------- Nickel 6 months -------- Nitrate +<Nitrite (as N) 28 days -------- Selenium 6 months --18 days 25 days -- Silver 6 months -------- Sulfate (mg/L) 28 days ----6 days -- TDS (mg/L) 7 days ----4 days -- Tetrahydrofuran 14 days -------- Thallium 6 months -------- Tin 6 months -------- Toluene 14 days -------- Uranium 6 months ------20 days Vanadium 6 months -------- Xylenes (total) 14 days -------- Zinc 6 months -------- AlC Balance (± 5) BALANCE-W ---------- Anions BALANCE-W ---------- Bicarbonate as HC03 14 days -------- Calcium 6 months -------- Carbonate as C03 14 days -------- Cations BALANCE-W ---------- Magnesium 6 months -------- Potassium 6 months -------- Sodium 6 months -------- G-2A: Holding Time Evaluation QAPHolding MW-ll MW-12 MW-14 MW-IS Constituent Time 7/11/2012 7117/2012 ·7/11/2012 7117/2012 2-Butanone (MEK) 14 days 13 days --13 days -- Acetone 14 days 13 days --13 days -- Ammonia (as N) 28 days 6 days --6 days -- Arsenic 6 months 14 days --14 days -- Benzene 14 days 13 days --13 days -- Beryllium 6 months 21 days --21 days -- Cadmium 6 months 14 days --14 days -- Carbon Tetrachloride 14 days 13 days --13 days -- Chloride (mg/L) 28 days 8 days --8 days -- Chloroform 14 days 13 days --13 days -- Chloromethane 14 days 13 days --13 days -- Chromium 6 months 14 days --14 days -- Cobalt 6 months 14 days --14 days -- Copper 6 months 14 days --14 days -- Dichloromethane (Methylene Chloride) 14 days 13 days --13 days -- Fluoride (MgIL) 28 days 2 days --2 days -- Gross Alpha minus Rn & U MDC 6 months 28 days --28 days -- Gross Alpha minus Rn & U Precision (±) 6 months 28 days --28 days -- Gross Alpha minus Rn & U 6 months 28 days --28 days -- Iron 6 months 7 days --7 days 6 days Lab pH (S.U.) --2 days --2 days -- Lead 6 months 14 days --14 days -- Manganese 6 months 14 days --14 days -- Mercury 28 days 21 days --21 days -- Molybdenum 6 months 14 days --14 days -- Naphthalene 14 days 13 days --13 days -- Nickel 6 months 14 days --14 days -- Nitrate + Nitrite (as N) 28 days 5 days --5 days -- Selenium 6 months 14 days 19 days 14 days 19 days Silver 6 months 14 days --.14 days -- Sulfate (mg/L) 28 days 9 days --9 days -- TDS (mgIL) 7 days 2 days --2 days -- Tetrahydrofuran 14 days 2 days --2 days -- Thallium 6 months 14 days --14 days -- Tin 6 months 1 days --I days -- Toluene 14 days 13 days --13 days -- Uranium 6 months 14 days --14 days -- Vanadium 6 months 14 days --14 days -- Xylenes (total) 14 days 13 days --13 days -- Zinc 6 months 14 days --14 days -- AlC Balance (± 5) BALANCE-W --28 days --28 days -- Anions BALANCE-W --28 days --28 days -- Bicarbonate as HC03 14 days 2 days --2 days -- Calcium 6 months 7 days --7 days -- Carbonate as C03 14 days 2 days --2 days -- Cations BALANCE-W --28 days --28 days -- Magnesium 6 months 7 days --7 days -- Potassium 6 months 7 days --7 days -- Sodium 6 months 7 days --7 days -- G-2A: Holding Time Evaluation . , ." , - , ~ QAP Holding. MW-18 MW-19 MW-23 MW-24 Constituent Time 7/18/2012 7119/2012 7117/2012 7118/2012 2-Butanone (MEK) 14 days -------- Acetone' 14 days -------- Ammonia (as N) 28 days -------- Arsenic 6 months ------ Benzene 14 days -------- Beryllium 6 months -------- Cadmium 6 months ------18 days Carbon Tetrachloride 14 days -------- Chloride (mg/L) 28 days -------- ChlQroform 14 days -------- Chloromethane 14 days -------- Chromium 6 months -------- Cobalt 6 months -------- Copper 6 months -------- Oichloromethane (Methylene Chloride) 14 days -------- Fluoride (MglL) 28 days -------- Gross Alpha minus Rn & U MOC 6 months -------- Gross Alpha minus Rn & U Precision (±) 6 months -------- Gross Alpha minus Rn & U 6 months -------- Iron 6 months -------- Lab pH (S.U.) ---------- Lead 6 months -------- Manganese 6 months ----24 days -- Mercury 28 days -------- Molybdenum 6 months -------- Naphthalene 14 days -------- Nickel 6 months -------- Nitrate + Nitrite (as N) 28 days --6 days ---- Selenium 6 months -------- Silver 6 months -------- Sulfate (mg/L) 28 days 7 days ------ TOS (mgIL) 7 days 5 days ------ Tetrah ydrofuran 14 days -------- Thallium 6 months 18 days ----20 days Tin 6 months -------- Toluene 14 days -------- Uranium 6 months -------- Vanadium 6 months -------- Xylenes (total) 14 days -------- Zinc 6 months -------- AlC Balance (± 5) BALANCE-W ---------- Anions BALANCE-W ---------- Bicarbonate as HC03 14 days -------- Calcium 6 months -------- Carbonate as C03 14 days ------. -- Cations BALANCE-W ---------- Magnesium 6 months -------- Potassium 6 months -------- Sodium 6 months -------- G-2A: Holding Time Evaluation .J .1 \ QAPHolding MW-2S MW-26 MW-26 . MW-27 . Constituent Time 7110/2012 7ill/2012 8/16/2012 7/16/2012 2-Butanone (MEK) 14 days 10 days --6 days -- Acetone 14 days 10 days --6 days -- Ammonia (as N) 28 days 7 days 6 days ---- Arsenic 6 months 15 days 14 days ---- Benzene 14 days 10 days --6 days -- Beryllium 6 months 22 days 21 days ---- Cadmium 6 months 15 days 14 days ---- Carbon Tetrachloride 14 days 10 days --6 days -- Chloride (mglL) 28 days 9 days 8 days --9 days Chloroform 14 days 10 days --13 days -- Chloromethane 14 days 10 days --6 days -- Chromium 6 months 15 days 14 days ---- Cobalt 6 months 15 days 14 days ---- Copper 6 months 15 days 14 days ---- Dichloromethane (Methylene Chloride) 14 days 10 days --6 days -- Fluoride (MglL) 28 days 3 days 2 days ---- Gross Alpha minus Rn & U MDC 6 months 29 days 28 days --16 days Gross Alpha minus Rn & U Precision (±) 6 months 29 days 28 days --16 days Gross Alpha minus Rn & U 6 months 29 days 28 days --16 days Iron 6 months 8 days 7 days ---- Lab pH (S.u.) . --3 days 2 days ---- Lead 6 months 15 days 14 days ---- Manganese 6 months 15 days 14 days ---- Mercury 28 days 22 days 21 days ---- Molybdenum 6 months 15 days 14 days ---- Naphthalene 14 days 10 days --6 days -- Nickel 6 months 15 days 14 days ---- Nitrate + Nitrite (as N) 28 days 6 days 5 days --9 days Selenium 6 months 15 days 21 days ---- Silver 6 months 15 days 14 days ---- Sulfate (mgIL) 28 days 10 days 9 days --9 days TDS (mgIL) 7 days 3 days 2 days --7 days Tetrahydrofuran 14 days 3 days 2 days ---- Thallium 6 months 15 days 14 days ---- Tin 6 months 2 days 1 days ---- Toluene 14 days 10 days --6 days -- Uranium 6 months 15 days 14 days ---- Vanadium 6 months 15 days 14 days ---- Xylenes (total) 14 days 10 days --6 days -- Zinc 6 months 15 days 14 days ---- AlC Balance (± 5) BALANCE-W --29 days 28 days ---- Anions BALANCE-W --29 days 28 days ---- Bicarbonate as HC03 14 days -3 days 2 days ---- Calcium 6 months 8 days 8 days ---- Carbonate as C03 14 days 3 days 2 days ---- Cations BALANCE-W --29 days 28 days ---- Magnesium 6 months 8 days 7 days ---- Potassium 6 months 8 days 7 days ---- Sodium 6 months 8 days 7 days ---- G-2A: Holding Time Evaluation , -. QAPHolding MW-28 MW-28 MW-29 MW~29 Constituent Time 7116/2012 8/112012 7110/2012 8/112012 2-Butanone (MEK) 14 days -------- Acetone 14 days -------- Ammonia (as N) 28 days -------- Arsenic 6 months -------- Benzene 14 days -------- Beryllium 6 months -------- Cadmium 6 months -------- Carbon Tetrachloride 14 days -------- Chloride (mgIL) 28 days 11 days ------ Chloroform 14 days -------- Chloromethane 14 days -------- Chromium 6 months -------- Cobalt 6 months -------- Copper 6 months -------- Dichloromethane (Methylene Chloride) 14 days -------- Fluoride (Mg/L) 28 days -------- Gross Alpha minus Rn & U MDC 6 months -------- Gross Alpha minus Rn & U Precision (±) 6 months -------- Gross Alpha minus Rn & U 6 months -------- Iron 6 months ----6 days -- Lab pH (S.u.) ---------- Lead 6 months -------- Manganese 6 months --19 days --19 days Mercury 28 days -------- Molybdenum 6 months -------- Naphthalene 14 days -------- Nickel 6 months -------- Nitrate + Nitrite (as N) 28 days -------- Seleniuni 6 months -------- Silver 6 months -------- Sulfate (mgIL) 28 days -------- TDS (mgIL) 7 days ------5 days Tetrahydrofuran 14 days -------- Thallium 6 months -------- Tin 6 months -------- Toluene 14 days -------- Uranium 6 months ------' -- Vanadium 6 months -------- Xylenes (total) 14 days -------- Zinc 6 months -------- NC Balance (± 5) BALANCE-W ---------- Anions BALANCE-W ---------- Bicarbonate as HC03 14 days -------- Calcium 6 months -------- Carbonate as C03 14 days -------- Cations BALANCE-W ---------- Magnesium 6 months -------- Potassium 6 months -------- Sodium 6 months -------- G-2A: Holding Time Evaluation , QAPHolding MW-30 MW-31 MW-32 ',MW;.3S' , Constituent Time' 7110/2012 7/9/2012 7/9/2012 7/10/2012 2-Butanone (MEK) 14 days 10 days 9 days --9 days Acetone 14 days 10 days 9 days --9 days Ammonia (as N) 28 days 7 days 8 days --7 days Arsenic 6 months 15 days 16 days --15 days Benzene 14 days 10 days 9 days --9 days Beryllium 6 months 22 days 23 days --22 days Cadmium 6 months 15 days 16 days --15 days Carbon Tetrachloride 14 days 10 days 9 days --9 days Chloride (mg/L) 28 days 9 days 10 days --9 days Chloroform 14 days 10 days 9 days --9 days Chloromethane 14 days 10 days 9 days --9 days Chromium 6 months 15 days 16 days --15 days Cobalt 6 months 15 days 16 days --15 days Copper 6 months 15 days 16 days --15 days Dichloromethane (Methylene Chloride) 14 days 10 days 9 days --9 days Fluoride (Mg/L) 28 days 3 days 4 days --3 days Gross Alpha minus Rn & U MDC 6 months 29 days 30 days 30 days 30 days Gross Alpha minus Rn & U Precision (±) 6 months 29 days 30 days 30 days 30 days Gross Alpha minus Rn & U 6 months 29 days 30 days 30 days 30 days Iron 6 months 8 days 9 days --8 days Lab pH (S.U.) --3 days 4 days --3 days Lead 6 months 15 days 16 days --15 days Manganese 6 months 15 days 16 days --15 days Mercury 28 days 22 days 23 days --22 days Molybdenum 6 months 15 days 16 days --15 days Naphthalene 14 days 10 days 9 days --9 days Nickel 6 months 15 days 16 days --15 days Nitrate + Nitrite (as N) 28 days 6 days 7 days --6 days Selenium 6 months 15 days 16 days --15 days Silver 6 months 15 days 16 days --15 days Sulfate (mg/L) 28 days 10 days 11 days --10 days TDS (mg/L) 7 days 3 days 4 days --3 days Tetrah ydrofuran 14 days 3 days 4 days --3 days Thallium 6 months 15 days 16 days --15 days Tin 6 months 2 days 3 days --2 days Toluene 14 days 10 days 9 days --9 days Uranium 6 months 15 days 16 days --15 days Vanadium 6 months 15 days 16 days --15 days Xylenes (total) 14 days 10 days 9 days --9 days Zinc 6 months 15 days 16 days --15 days AlC Balance (± 5) BALANCE-W --29 days 30 days --29 days Anions BALANCE-W --29 days 30 days --29 days Bicarbonate as HC03 14 days 3 days 4 days --3 days Calcium 6 months 8 days 9 days --8 days Carbonate as C03 14 days 3 days 4 days --3 days Cations BALANCE-W --29 days 30 days --29 days Magnesium 6 months 8 days 9 days --8 days Potassium 6 months 8 days 9 days --8 days Sodium 6 months 8 days 9 days --8 days G-2A: Holding Time Evaluation ,. , '. QAP Holding MW-65 MW-65 · -MW-70 Constituent Time 7/11/2012 811612012 . -7118/2012 - 2-Butanone (MEK) 14 days --6 days -- Acetone 14 days --6 days -- Ammonia (as N) 28 days 6 days ---- Arsenic 6 months 21 days ---- Benzene 14 days --6 days -- Beryllium 6 months 21 days ---- Cadmium 6 months 21 days ---- Carbon Tetrachloride 14 days --6 days -- Chloride (mg/L) 28 days 8 days ---- Chloroform 14 days --13 days -- Chloromethane 14 days --6 days -- Chromium 6 months 21 days ---- Cobalt 6 months 21 days ---- Copper 6 months 21 days ---- Dichloromethane (Methylene Chloride) 14 days --6 days -- Fluoride (Mg/L) 28 days 2 days --5 days Gross Alpha minus Rn & U MDC 6 months 29 days ---- Gross Alpha minus Rn & U Precision (±) 6 months 29 days ---- Gross Alpha minus Rn & U 6 months 29 days ---- Iron 6 months 7 days ---- Lab pH (S.u.) --2 days ---- Lead 6 months 21 days ---- Manganese 6 months 21 days ---- Mercury 28 days 21 days ---- Molybdenum 6 months 21 days ---- Naphthalene 14 days --6 days -- Nickel 6 months 21 days ---- Nitrate + Nitrite (as N) 28 days 5 days ---- Selenium 6 months 21 days --18 days Silver 6 months 21 days ---- Sulfate (mg/L) 28 days 9 days ---- TDS (mg/L) 7 days 2 days ---- Tetrahydrofuran 14 days 2 days ---- Thallium 6 months 21 days ---- Tin 6 months 1 days ---- Toluene 14 days --6 days -- Uranium 6 months 21 days ---- Vanadium 6 months 21 days ---- Xylenes (total) 14 days --6 days -- Zinc 6 months 21 days ---- AlC Balance (± 5) BALANCE-W --28 days ---- Anions BALANCE-W --28 days ---- Bicarbonate as HC03 14 days 2 days ---- Calcium 6 months 7 days ---- Carbonate as C03 14 days 2 days ---- Cations BALANCE-W --28 days ---- Magnesium 6 months 7 days ---- Potassium 6 months 7 days ---- Sodium 6 months 7 days ---- G-2B: Holding Time Evaluation -Accelerated samples '," !' QAPHolding MW-14 Constituent Time MW-1181712012 817/2012 MW -25 8/6/2012 2-Butanone (MEK) 14 days ------ Acetone 14 days ------ Ammonia (as N) 28 days ------ Arsenic 6 months ------ Benzene 14 days ------ Beryllium 6 months ------ Cadmium 6 months ------ Carbon Tetrachloride 14 days ------ Chloride (mg/L) 28 days ------ Chloroform 14 days ------ Chloromethane 14 days ------ Chromium 6 months ------ Cobalt 6 months ------ Copper 6 months ------ Dichloromethane (Methylene Chloride) 14 days ------ Field pH (S.U.) Immediate Fluoride (Mg/L) 28 days ------ Gross Alpha minus Rn & U MDC 6 months ------ Gross Alpha minus Rn & U Precision (±) 6 months ------ Gross Alpha minus Rn & U 6 months ------ Iron 6 months ------ Lab pH (S.U.) -------- Lead 6 months ------ Manganese 6 months 20 days 20 days -- Mercury 28 days ------ Molybdenum 6 months ------ Naphthalene 14 days ------ Nickel 6 months ------ Nitrate + Nitrite (as N) 28 days ------ Selenium 6 months ------ Silver 6 months ------ Sulfate (mg/L) 28 days ------ TDS (mg/L) 7 days ------ Tetrahydrofuran 14 days ------ Thallium 6 months ------ Tin 6 months ------ Toluene 14 days ------ Uranium 6 months ----21 days Vanadium 6 months ------ Xylenes (total) 14 days ------ Zinc 6 months ------ AlC Balance (± 5) BALANCE-W -------- Anions BALANCE-W -------- Bicarbonate as HC03 14 days ------ Calcium 6 months ------ Carbonate as C03 14 days ------ Cations BALANCE-W -------- Magnesium 6 months ------ Potassium 6 months ------ Sodium 6 months ------ G-2B: Holding Time Evaluation -Accelerated samples ". , .... QAP Holding Constituent 'Time MW-268/8/2012 . . MW-30 81712012 MW ~31 816/2012 2-Butanone (MEK) 14 days 6 days ---- Acetone 14 days 6 days ---- Ammonia (as N) 28 days ------ Arsenic 6 months ------ Benzene 14 days 6 days ---- Beryllium 6 months ------ Cadmium 6 months ------ Carbon Tetrachloride 14 days 6 days ---- Chloride (mg/L) 28 days 6 days 7 days 8 days Chloroform 14 days 6 days ---- Chloromethane 14 days 6 days ---- Chromium 6 months ------ Cobalt 6 months ------ Copper 6 months ------ Dichloromethane (Methylene Chloride) 14 days 6 days ---- Field pH (S.U.) Immediate Fluoride (Mg/L) 28 days ------ Gross Alpha minus Rn & U MDC 6 months ------ Gross Alpha minus Rn & U Precision (±) 6 months ------ Gross Alpha minus Rn & U 6 months ------ Iron 6 months ------ Lab pH (S.U.) -------- Lead 6 months ------ Manganese 6 months ------ Mercury 28 days ------ Molybdenum 6 months ------ Naphthalene 14 days 6 days ---- Nickel 6 months ------ Nitrate + Nitrite (as N) 28 days 5 days 6 days 7 days Selenium 6 months --20 days -- Silver 6 months ------ Sulfate (mg/L) 28 days ----8 days TDS (mg/L) 7 days 2 days --4 days Tetrahydrofuran 14 days ------ Thallium 6 months ------ Tin 6 months ------ Toluene 14 days 6 days ---- Uranium 6 months 19 days 20 days -- Vanadium 6 months ------ Xylenes (total) 14 days 6 days ---- Zinc 6 months ------ AlC Balance (± 5) BALANCE-W -------- Anions BALANCE-W -------- Bicarbonate as HC03 14 days ------ Calcium 6 months ------ Carbonate as C03 14 days ------ Cations BALANCE-W -------- Magnesium 6 months ------ Potassium 6 months ------ Sodium 6 months ------ G-2B: Holding Time Evaluation -Accelerated samples , , QAPHolding , ,MW-ll MW-14 Constituent Time MW -35 8/8/2012 9119/2012 9118/2012 2-B utanone (MEK) 14 days ------ Acetone 14 days ------ Ammonia (as N) 28 days ------ Arsenic 6 months ----"\ -- Benzene 14 days ------ Beryllium 6 months ------ Cadmium 6 months ------ Carbon Tetrachloride 14 days ------ Chloride (mg/L) 28 days ------ Chloroform 14 days ------ Chloromethane 14 days ------ Chromium 6 months ------ Cobalt 6 months ------ Copper 6 months ------ Dichloromethane (Methylene Chloride) 14 days ------ Field pH (S.U.) Immediate Fluoride (Mg/L) 28 days ------ Gross Alpha minus Rn & U MDC 6 months 22 days ---- Gross'Alpha minus Rn & U Precision (±) 6 months 22 days ---- Gross Alpha minus Rn & U 6 months 22 days ---- Iron 6 months ------ Lab pH (S.U.) -------- Lead 6 months ------ Manganese 6 months 19 days 16 days 17 days Mercury 28 days ------ Molybdenum 6 months ------ Naphthalene 14 days ------ Nickel 6 months ------ Nitrate + Nitrite (as N) 28 days ------ Selenium 6 months 19 days ---- Silver 6 months ------ Sulfate (mg/L) 28 days ------ TDS (mg/L) 7 days ------ Tetrahydrofuran 14 days ------ Thallium 6 months 19 days ---- Tin 6 months ------ Toluene 14 days ------ Uranium 6 months 19 days ---- Vanadium 6 months ------ Xylenes (total) 14 days ------ Zinc 6 months ------ NC Balance (± 5) BALANCE-W -------- Anions BALANCE-W -------- Bicarbonate as HC03 14 days ------ Calcium 6 months ------ Carbonate as C03 14 days ------ Cations BALANCE-W -------- Magnesium 6 months ------ Potassium 6 months ------ Sodium 6 months ------ G-2B: Holding Time Evaluation -Accelerated samples , ,,', ,,' . "', QAPHolding MW-2S MW-.26 MW-30 Constituent Time 9/18/2012 9/19/2012 9/~9/2012 2-Butanone (MEK) 14 days --17 days -- Acetone 14 days --17 days -- Ammonia (as N) 28 days ------ Arsenic 6 months ------ Benzene 14 days --17 days -- Beryllium 6 months ------ Cadmium 6 months ------ Carbon Tetrachloride 14 days --17 days -- Chloride (mg/L) 28 days --6 days 26 days Chloroform 14 days --15 days -- Chloromethane 14 days --17 days -- Chromium 6 months ------ Cobalt 6 months ------ Copper 6 months ------ Dichloromethane (Methylene Chloride) 14 days --17 days -- Field pH (S.U.) Immediate Fluoride (Mg/L) 28 days ------ Gross Alpha minus Rn & U MDC 6 months ------ Gross Alpha minus Rn & U Precision (±) 6 months ------ Gross Alpha minus Rn & U 6 months ------ Iron 6 months ------ Lab pH (S.U.) -------- Lead 6 months ------ Manganese 6 months ------ Mercury 28 days ------ Molybdenum 6 months ------ Naphthalene 14 days --17 days -- Nickel 6 months ------ Nitrate + Nitrite (as N) 28 days --8 days 8 days Selenium 6 months ----16 days Silver 6 months ------ Sulfate (mglL) 28 days ------ TDS(mglL) 7 days ------ Tetrahydrofuran 14 days ------ Thallium 6 months ------ Tin 6 months ------ Toluene 14 days --17 days -- Uranium 6 months 17 days 16 days 16 days Vanadium 6 months ------ Xylenes (total) 14 days --17 days -- Zinc 6 months ------ AlC Balance (± 5) BALANCE-W -------- Anions BALANCE-W -------- Bicarbonate as HC03 14 days ------ Calcium 6 months ------ Carbonate as C03 14 days ------ Cations BALANCE-W -------- Magnesium 6 months ------ Potassium 6 months ------ Sodium 6 months ------ G-2B: Holding Time Evaluation -Accelerated samples QA.P Holding MW;.31 . MW-35 Constituent . Time 9/18/2012 9/19/2012 2-Butanone (MEK) 14 days ---- Acetone 14 days ---- Ammonia (as N) 28 days ---- Arsenic 6 months ---- Benzene 14 days ---- Beryllium 6 months ---- Cadmium 6 months ---- Carbon Tetrachloride 14 days ---- Chloride (mg/L) 28 days 7 days -- Chloroform 14 days ---- Chloromethane 14 days ---- Chromium 6 months ---- Cobalt 6 months ---- Copper 6 months ---- DichlorOIhethane (Methylene Chloride) 14 days ---- Field pH (S.U.) Immediate Fluoride (Mg/L) 28 days ---- Gross Alpha minus Rn & U MDC 6 months --IS days Gross Alpha minus Rn & U Precision (±) 6 months --IS days Gross Alpha minus Rn & U 6 months --IS days Iron 6 months ---- Lab pH (S.U.) ------ Lead 6 months ---- Manganese 6 months --16 days Mercury 28 days ---- Molybdenum 6 months ---- Naphthalene 14 days ---- Nickel 6 months ---- Nitrate + Nitrite (as N) 28 days 9 days -- Selenium 6 months --16 days Silver 6 months ---- Sulfate (mg/L) 28 days 7 days -- TDS (mg/L) 7 days 6 days -- Tetrahydrofuran 14 days ---- Thallium 6 months --16 days Tin 6 months ---- Toluene 14 days ---- Uranium 6 months --16 days Vanadium 6 months ---- Xylenes (total) 14 days ---- Zinc 6 months ---- AlC Balance (± 5) BALANCE-W ------ Anions BALANCE-W ------ Bicarbonate as HC03 14 days ---- Calcium 6 months ---- Carbonate as C03 14 days ---- Cations BALANCE-W ------ Magnesium 6 months ---- Potassium 6 months ---- Sodium 6 months ---- G-3A: Laboratory Receipt Temperature Check Sampl~ Batch Wells in Batch Temperature MW -02, MW -03, MW -03A, MW -05, 2.4 °C EL -C12070741 MW-12, MW-15, MW-18, MW-19, MW-23, MW-24, MW-27, MW-28, MW-70 MW-11,MW-14,MW-25,MW-26, 1.6°C EL -C12070448 MW-30,MW-31,MW-35,MW-65, MW-29, MW-32, Trip Blank EL -C 12080830 MW -26 Resample, MW -65 Resample, 3.2°C Trip Blank EL -C12080143 MW-28 Resample, MW-29 Resample, 4.0°C MW-37, Trip Blank MW-11,MW-14, MW-25, MW-26, 1.8°C AWAL -1207185 -THF and Tin MW-30,MW-31,MW-35,MW-65, Trip Blank A W AL -1208066 -THF and Tin MW-37, Trip Blank 2.7°C ·i G-3B: Laboratory Receipt Temperature Check -Accelerated Samples . Sample Batch Wells in Batch Ii . Temperature ~VV-11,~VV-25 ,~VV-26,~VV-30,~VV-2.0°C EL -C 120080469 31, ~VV-35, ~VV-65, Trip Blank ~VV-11,~VV-25,~VV-26,~VV-30,~VV-2.0°C EL - C 12090804 31, ~VV-35, ~VV-65, Trip Blank G-4A: Analytical Method Check . Parameter QAPMethod* Method Used by Lab Ammonia (as N) A4500-NH3 G or E350.1 A4500-NH3 G Nitrate + Nitrite (as N) E353.1 or E353.2 E353.2 Metals Except Mercury E200.7 or E200.8 E200.8 Mercury E245.1 or E200.7 or E200.8 E200.8 Gross Alpha E900.0 or E900.1 E900.1 VOCs SW8260B or SW8260C SW8260B Chloride A4500-CI B or A4500-CI E or E300.0 A4500-CIB Fluoride A4500-F C or E300.0 A4500-FC Sulfate A4500-S04 E or E300.0 A4500-S04 E TDS A2540C A2540 C Carbonate as C03, Bicarbonate as HC03 A2320 B A2320B Iron, Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 Tetrahydrofuran and tin were analyzed by American West Analytical Laboratories. All other constituents were analyzed by Energy Laboratories. G-4B: Analytical Method Check -Accelerated Samples Parameter QAPMethod , Method Used by Lab Nitrate + Nitrite (as N) E353.1 or E353.2 E353.2 Metals Except Mercury E200.7 or E200.8 E200.8 Gross Alpha E900.0 or E900.1 E900.1 VOCs SW8260B or SW8260C SW8260B Chloride A4500-Cl B or A4500-Cl E or E300.0 E300.0 Sulfate A4500-S04 E or E300.0 E300.0 TDS A2540C A2540C Iron, Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 G-5A: Routine Reporting Limit Check , '." 'MW-2 " -MW-J " I" --"' 7116/2012 ~ 711S/20l2 , - , QAP Reporting Constituent , Limit ' RL .Qualifier RL Qualifier 2-B utanone (MEK) 20 !!g/L -------- Acetone 20 !!g/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 !!g/L -------- Benzene 1.0 !!g/L -------- Beryllium 0.50 !!glL -------- Cadmium 0.50 !!g/L -------- Carbon Tetrachloride 1.0 !!g/L -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 !!g/L -------- Chloromethane 1.0 !!g/L -------- Chromium 25 !!g/L -------- Cobalt 10 !!g/L ---- ---- Copper 10 !!g/L -------- Dichloromethane (Methylene Chloride) 1.0 !!g/L ---- ---- Fluoride (Mg/L) 0.1 mg/L ----0.1 mg/L Gross Alpha minus Rn & U MDC 1.0 pCiIL o pCiIL -- Iron 30 !!g/L -------- Lead 1.0 !!g/L -------- Manganese 10 !!g/L ---- ---- Mercury 0.50 !!g/L ---- ---- Molybdenum 10 !!g/L -------- Naphthalene 1.0 !!g/L -------- Nickel 20 !!g/L -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5 !!g/L ----5 ug/L Silver 10 !!g/L -------- Sulfate (mg/L) 1 mg/L ---- ---- TDS (mg/L) 10 mg/L -------- Tetrahydrofuran 1.0 !!g/L -------- Thallium 0.50 !!g/L -------- Tin 100 !!g/L -------- Toluene 1.0 !!g/L -------- Uranium 0.30 !!g/L -------- Vanadium 15 !!g/L -------- Xylenes (total) 1.0 !!g/L -------- Zinc 10 !!g/L -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check MW~3A ., .'MW-5 . 7119/2012 7116/2012 " . " " . QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 Ilg/L -------- Acetone 20 Ilg/L -- ------ Ammonia (as N) 0.05 mg/L -------- Arsenic 5 Ilg/L -------- Benzene 1.0 Ilg/L -------- Beryllium 0.50 Ilg/L -------- Cadmium 0.50 Ilg/L -------- Carbon Tetrachloride 1.0 Ilg/L -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 Ilg/L -------- Chloromethane 1.0 Ilg/L -------- Chromium 25 Ilg/L -------- Cobalt 10 Ilg/L -------- Copper 10 Ilg/L -- ------ Dichloromethane (Methylene Chloride) 1.0 Ilg/L -------- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCiIL ---- Iron 30 Ilg/L -------- Lead 1.0 Ilg/L -------- Manganese 10 Ilg/L -------- Mercury 0.50 Ilg/L -------- Molybdenum 10 Ilg/L -- ------ Naphthalene 1.0 Ilg/L -- ------ Nickel 20 Ilg/L -- ------ Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5 Ilg/L 5 ug/L ---- Silver 10 Ilg/L -------- Sulfate (mg/L) 1 mg/L 20mg/L D ---- TDS (mg/L) 10 mg/L 10MG/L ---- Tetrahydrofuran 1.0 Ilg/L -------- Thallium 0.50 Ilg/L -- ------ Tin 100 Ilg/L -------- Toluene 1.0 Ilg/L -- ------ Uranium 0.30 Ilg/L ----0.3 ug/L Vanadium 15 Ilg/L -------- Xylenes (total) 1.0 Ilg/L -------- Zinc 10 Ilg/L -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -- ------ Carbonate, as C03 1 mg/L -- ------ Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -- --.---- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check MW-l1 MW-12 . . 7111/2012. 7117/2012 , , QAP Rep~rting Constituent Limit RL . Qualifier RL Qualifier 2-B utanone (MEK) 20 ~g/L 20 ug/L U ---- Acetone 20 ~g/L 20 ug/L U ---- Ammonia (as N) 0.05 mg/L 0.05 mg/L ---- Arsenic 5 ~g/L 5 ug/L U ---- Benzene 1.0 ~g/L 1 ug/L U ---- Beryllium 0.50 ~g/L 0.5 ug/L U ---- Cadmium 0.50 ~g/L 0.5 ug/L U ---- Carbon Tetrachloride 1.0 ~g/L 1 ug/L U ---- Chloride (mg/L) 1 mg/L 1 mg/L ---- Chloroform 1.0 ~g/L 1 ug/L U ---- Chloromethane 1.0 ~g/L 1 ug/L U ---- Chromium 25 ~g/L 25 ug/L U ---- Cobalt 10 ~g/L 10 ug/L U ---- Copper 10 ~g/L 10 ug/L U ---- Dichloromethane (Methylene Chloride ) 1.0 ~g/L 1 ug/L U ---- Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L ---- Gross Alpha minus Rn & U MDC 1.0 pCiIL o pCi/L -- Iron 30 ~g/L 30 ug/L ---- Lead 1.0 ~g/L 1 ug/L U ---- Manganese 10 ~g/L 10 ug/L ---- Mercury 0.50 ~g/L 0.5 ug/L U ---- Molybdenum 10 ~g/L 10 ug/L U ---- Naphthalene 1.0 ~g/L 1 ug/L U ---- Nickel 20 ~g/L 20 ug/L U ---- Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L U ---- Selenium 5 ~g/L 5 ug/L U 5 ug/L Silver 10 ~g/L 10 ug/L U ---- Sulfate (mg/L) 1 mg/L 50 mg/L D ---- TDS (mg/L) 10 mg/L 10MG/L ---- Tetrahydrofuran 1.0 ~g/L Oug/L ---- Thallium 0.50 ~g/L 0.5 ug/L U ---- Tin 100 ~g/L Oug/L ---- Toluene 1.0 ~g/L 1 ug/L U ---- Uranium 0.30 ~g/L 0.3 ug/L ---- Vanadium 15 ~g/L 15 ug/L U , ---- Xylenes (total) 1.0 ~g/L 1 ug/L U ---- Zinc 10 ~g/L 10 ug/L U ---- Bicarbonate as HC03 1 mg/L 1 mg/L ---- Calcium 0.5 mg/L 0.5 mg/L ---- Carbonate as C03 1 mg/L 1 mg/L U ---- Magnesium 0.5 mg/L 0.5 mg/L ---- Potassium 0.5 mg/L 0.5 mg/L ---- Sodium 0.5 mg/L 0.5 mg/L ---- G-5A: Routine Reporting Limit Check MW-14 . t, MW-15 '". 'c, 7/11/2012 7/17/2012 . QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 !!g/L 20 ug/L 'U ---- Acetone 20 !!g/L 20 ug/L U ---- Ammonia (as N) 0.05 mg/L 0.05 mg/L U ---- Arsenic 5 !!g/L 5 ug/L U ---- Benzene 1.0 !!g/L 1 ug/L U ---- Beryllium 0.50 !!g/L 0.5 ug/L U ---- Cadmium 0.50 !!g/L 0.5 ug/L ---- Carbon Tetrachloride 1.0 !!g/L 1 ug/L U ---- Chloride (mg/L) 1 mg/L 1 mg/L ---- Chloroform 1.0 !!g/L 1 ug/L U ---- Chloromethane 1.0 !!g/L 1 ug/L U ---- Chromium 25 !!g/L 25 ug/L U ---- Cobalt 10 !!g/L 10 ug/L U ---- Copper 10 !!g/L 10 ug/L U ---- Dichloromethane (Methylene Chloride) 1.0 !!g/L 1 ug/L U ---- Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L ---- Gross Alpha minus Rn & U MDC 1.0 pCi/L o pCi/L -- Iron 30 !!g/L 30 ug/L U 30 ug/L U Lead 1.0 !!g/L 1 ug/L U ---- Manganese 10 !!g/L 10 ug/L ---- Mercury 0.50 !!g/L 0.5 ug/L U ---- Molybdenum 10 !!g/L 10 ug/L U ---- Naphthalene 1.0 !!g/L 1 ug/L U ---- Nickel 20 !!g/L 20 ug/L U ---- Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L U ---- Selenium 5 !!g/L 5 ug/L U 5 ug/L Silver 10 !!g/L 10 ug/L U ---- Sulfate (mg/L) 1 mg/L 50 mg/L D ---- TDS (mg/L) 10 mg/L 10MG/L ---- Tetrahydrofuran 1.0 !!g/L Oug/L ---- Thallium 0.50 !!g/L 0.5 ug/L U ---- Tin 100 !!g/L Oug/L ---- Toluene 1.0 !!g/L 1 ug/L U ---- Uranium 0.30 !!g/L 0.3 ug/L ---- Vanadium 15 !!g/L 15 ug/L U ---- Xylenes (total) 1.0 !!g/L 1 ug/L U ---- Zinc 10 !!g/L 10 ug/L U ---- Bicarbonate as HC03 1 mg/L 1 mg/L ---- Calcium 0.5 mg/L 0.5 mg/L ---- Carbonate as C03 1 mg/L 1 mg/L U ---- Magnesium 0.5 mg/L 0.5 mg/L ---- Potassium 0.5 mg/L 0.5 mg/L ---- Sodium 0.5 mg/L 0.5 mg/L ---- G-5A: Routine Reporting Limit Check MW-18 MW-19 7118/2012 7119/20i2 . QAP Reporting Constituent Limit RL .' Qmilifier RL .. Qualifier 2-B utanone (MEK) 20 ~g/L -------- Acetone 20 ~g/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 ~g/L -------- Benzene 1.0 ~g/L -------- Beryllium 0.50 ~g/L -------- Cadmium 0.50 ~g/L -------- Carbon Tetrachloride 1.0 ~g/L -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 ~g/L -------- Chloromethane 1.0 ~g/L -------- Chromium 25 ~g/L -------- Cobalt 10 ~g/L -------- C~pper 10 ~g/L -------- DichloroIhethane (Methylene Chloride) 1.0 ~g/L -------- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCi/L ---- Iron 30 ~g/L -------- Lead 1.0 ~g/L -------- Manganese 10 ~g/L -------- Mercury 0.50 ~g/L -------- Molybdenum 10 ~g/L -------- Naphthalene 1.0 ~g/L -------- Nickel 20 ~g/L -------- Nitrate + Nitrite (as N) 0.1 mg/L ----0.2 mg/L D Selenium 5 ~g/L -------- Silver 10 ~g/L -------- Sulfate (mg/L) 1 mg/L 8mg/L D ---- TDS (mg/L) 10 mg/L 10MG/L ---- Tetrahydrofuran 1.0 ~g/L -------- Thallium 0.50 ~g/L 0.5 ug/L ---- Tin 100 ~g/L -------- Toluene 1.0 ~g/L -------- Uranium 0.30 ~g/L -------- Vanadium 15 ~g/L -------- Xylenes (total) 1.0 ~g/L -------- Zinc 10 ~g/L . -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check -' 'M-W-23 MW-24 , 7117/2012 7/18/2012 .' QAP Reporting' . Constituent Limit RL 'QuaHfier RL Qualifier 2-B utanone (MEK) 20 !lg/L -------- Acetone 20 !lg/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 !lg/L -------- Benzene 1.0 !lg/L -------- Beryllium 0.50 !lg/L -------- Cadmium 0.50 !lg/L ----0.5 ug/L Carbon Tetrachloride 1.0 !lg/L -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 !lg/L -------- Chloromethane 1.0 !lg/L -------- Chromium 25 !lg/L -------- Cobalt 10 !lg/L -------- Copper 10 !lg/L -------- Dichloromethane (Methylene Chloride) 1.0 !lg/L -------- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCi/L ---- Iron 30 !lg/L -------- Lead 1.0 !lg/L -------- Manganese 10 !lg/L 1 ug/L ---- Mercury 0.50 !lg/L -------- Molybdenum 10 !lg/L -------- Naphthalene 1.0 !lg/L -------- Nickel 20 !lg/L -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5 !lg/L -------- Silver 10 !lg/L -------- Sulfate (mg/L) 1 mg/L -------- TDS (mg/L) 10 mg/L -------- Tetrahydrofuran 1.0 !lg/L -------- Thallium 0.50 !lg/L ----0.5 ug/L Tin 100 !lg/L -------- Toluene 1.0 !lg/L -------- Uranium 0.30 !lg/L -------- Vanadium 15 !lg/L -------- Xylenes (total) 1.0 !lg/L -------- Zinc 10 !lg/L -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check ", , MW-25 MW-26 " , 7/10/2012 ,7/1112012 c' " . QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 "",gIL 20 uglL U ---- Acetone 20 "",gIL 20 uglL U ---- Ammonia (as N) 0.05 mglL 0.1 mglL 0.05 mglL Arsenic 5 "",gIL 5 uglL U 5 uglL U Benzene 1.0 "",gIL 1 uglL U ---- Beryllium 0.50 "",gIL 0.5 uglL U 0.5 uglL U Cadmium 0.50 "",gIL 0.5 uglL 0.5 uglL U Carbon Tetrachloride 1.0 "",gIL 1 uglL U ---- Chloride (mglL) 1 mglL 1 mglL 1 mglL Chloroform 1.0 "",gIL 1 uglL U ---- Chloromethane 1.0 "",gIL 1 uglL U ---- Chromium 25 "",gIL 25 uglL U 25 uglL U Cobalt 10 "",gIL 10 uglL U 10 uglL U Copper 10 "",gIL 10 uglL U 10 uglL U Dichloromethane (Methylene Chloride) 1.0 "",gIL 1 uglL U ---- Fluoride (MglL) 0.1 mglL 0.1 mglL 0.1 mglL Gross Alpha minus Rn & U MDC 1.0 pCilL o pCilL o pCiIL Iron 30 "",gIL 30 uglL U 30 uglL Lead 1.0 "",gIL 1 uglL U 1 uglL U Manganese 10 "",gIL 10 uglL 10 uglL Mercury 0.50 "",gIL 0.5 uglL U 0.5 uglL U Molybdenum 10 "",gIL 10 uglL 10 uglL U Naphthalene 1.0 "",gIL 1 uglL U ---- Nickel 20 "",gIL 20 uglL U 20 uglL U Nitrate + Nitrite (as N) 0.1 mglL 0.1 mglL U 0.1 mglL Selenium 5 "",gIL 5 uglL U 5 uglL U Silver 10 "",gIL 10 uglL U 10 uglL U Sulfate (mglL) 1 mglL 50 mglL D 50 mglL D TDS (mglL) 10 mglL 10MGIL 10MGIL Tetrahydrofuran 1.0 "",gIL OuglL OuglL Thallium 0.50 "",gIL 0.5 uglL 0.5 uglL U Tin 100 "",gIL OuglL OuglL Toluene 1.0 "",gIL 1 uglL U ---- Uranium 0.30 "",gIL 0.3 uglL 0.3uglL Vanadium 15 "",gIL 15 uglL U 15 uglL U Xylenes (total) 1.0 "",gIL 1 uglL U ---- Zinc 10 "",gIL 10 uglL U 10 uglL U Bicarbonate as HC03 1 mglL 1 mglL 1 mglL Calcium 0.5 mglL 0.5 mglL 0.5 mglL Carbonate as C03 1 mglL 1 mglL U 1 mglL U Magnesium 0.5 mglL 0.5 mglL 0.5 mglL Potassium 0.5 mglL 0.5 mglL 0.5 mglL Sodium 0.5 mglL 0.5 mglL 0.5 mglL G-5A: Routine Reporting Limit Check MW-26 MW~27 " -8/16/2012 7116/2012 / ,- QAP Reporting Constituent r' Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 !-lg/L 20 ug/L U ---- Acetone 20 !-lg/L 20 ug/L U ---- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 !-lg/L -------- Benzene 1.0 !-lg/L 1 ug/L U ---- Beryllium 0.50 !-lg/L -------- Cadmium ' 0.50 !-lg/L -------- Carbon Tetrachloride 1.0 !-lg/L 1 ug/L U ---- Chloride (mg/L) 1 mg/L ----I mg/L Chloroform 1.0 !-lg/L 25 ug/L D ---- Chloromethane 1.0 !-lg/L 1 ug/L U ---- Chromium 25 !-lg/L -------- Cobalt 10 !-lg/L -------- Copper 10 !-lg/L -------- Dichloromethane (Methylene Chloride) 1.0 !-lg/L 1 ug/L ---- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCi/L --o pCi/L Iron 30 !-lg/L -------- Lead 1.0 !-lg/L -------- Manganese 10 !-lg/L -------- Mercury 0.50 !-lg/L -------- Molybdenum 10 !-lg/L , -------- Naphthalene 1.0 !-lg/L 1 ug/L U ----, Nickel 20 !-lg/L -------- Nitrate + Nitrite (as N) 0.1 mg/L ----0.5 mg/L D Selenium 5 !-lg/L -------- Silver 10 !-lg/L -------- Sulfate (mg/L) 1 mg/L ----4mg/L D TDS (mg/L) 10 mg/L ----10 MG/L Tetrahydrofuran 1.0 !-lg/L -------- Thallium 0.50 !-lg/L -------- Tin 100 !-lg/L -------- Toluene 1.0 !-lg/L 1 ug/L U ---- Uranium 0.30 !-lg/L -------- Vanadium 15 !-lg/L -------- Xylenes (total) 1.0 !-lg/L 1 ug/L U ---- Zinc 10 !-lg/L -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check " ;, MW~28 MW-28 7/16/2012 811/2012 , Q~P Reporting Constituent Limit RL Qualifier RL ' <' Qualifier , 2-Butanone (MEK) 20 Ilg/L -------- Acetone 20 Ilg/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 Ilg/L -------- Benzene 1.0 Ilg/L -------- Beryllium 0.50 Ilg/L -------- Cadmium 0.50 Ilg/L -------- Carbon Tetrachloride 1.0 Ilg/L -------- Chloride (mg/L) 1 mg/L 4mg/L D ---- Chloroform 1.0 Ilg/L -------- Chloromethane 1.0 Ilg/L -------- Chromium 25 Ilg/L -------- Cobalt 10 Ilg/L -------- Copper 10 Ilg/L -------- Dichloromethane (Methylene Chloride) 1.0 Ilg/L -------- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCiIL ---- Iron 30 Ilg/L -------- Lead 1.0 Ilg/L -------- Manganese 10 Ilg/L ----10 ug/L Mercury 0.50 Ilg/L -------- Molybdenum 10 Ilg/L -------- Naphthalene 1.0 Ilg/L -------- Nickel 20 Ilg/L -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5 Ilg/L -------- Silver 10 Ilg/L -------- Sulfate (mg/L) 1 mg/L -------- TDS (mg/L) 10 mg/L -------- Tetrahydrofuran 1.0 Ilg/L -------- Thallium 0.50 Ilg/L -------- Tin 100 Ilg/L -------- Toluene 1.0 Ilg/L -------- Uranium 0.30 Ilg/L -------- Vanadium 15 Ilg/L -------- Xylenes (total) 1.0 Ilg/L -------- Zinc 10 Ilg/L -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L --------, Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check MW-29 " MW-29 " . 7110/2012 8111201Z ,. QAP Reporting " Constituent Limit RL Qualifier RL . Qualifier 2-B utanone (MEK) 20 ~g/L -------- Acetone 20 ~g/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 ~g/L -------- Benzene 1.0 ~g/L -------- Beryllium 0.50 ~g/L -------- Cadmium 0.50 ~g/L -------- Carbon Tetrachloride 1.0 ~g/L -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 ~g/L -------- Chloromethane 1.0 ~g/L -------- Chromium 25 ~g/L -------- Cobalt 10 ~g/L -------- Copper 10 ~g/L -------- Dichloromethane (Methylene Chloride) 1.0 ~g/L -------- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCi/L ---- Iron 30 ~g/L 30 ug/L ---- Lead 1.0 ~g/L -------- Manganese 10 ~g/L ----10 ug/L Mercury 0.50 ~g/L -------- Molybdenum 10 ~g/L -------- Naphthalene 1.0 ~g/L -------- Nickel 20 ~g/L -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5 ~g/L -------- Silver 10 ~g/L -------- Sulfate (mg/L) 1 mg/L -------- TDS (mg/L) 10 mg/L ----10MG/L Tetrahydrofuran 1.0 ~g/L -------- Thallium 0.50 ~g/L -------- Tin 100 ~g/L -------- Toluene 1.0 ~g/L -------- Uranium 0.30 ~g/L -------- Vanadium 15 ~g/L -------- Xylenes (total) 1.0 ~g/L -------- Zinc 10 ~g/L -------- Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5A: Routine Reporting Limit Check " , MW-30 MW-31 . . 7/10/2012 .7/9/2012 QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20/lg/L 20 ug/L U 20 ug/L U Acetone 20/lg/L 20 ug/L U 20 ug/L U Ammonia (as N) 0.05 mg/L 0.05 mg/L U 0.05 mg/L U Arsenic 5 /lg/L 5 ug/L U 5 ug/L U Benzene 1.0/lg/L 1 ug/L U 1 ug/L U Beryllium 0.5O /lg/L 0.5 ug/L U 0.5 ug/L U Cadmium 0.50/lg/L 0.5 ug/L U 0.5 ug/L U Carbon Tetrachloride 1.0/lg/L 1 ug/L U 1 ug/L U Chloride (mg/L) 1 mg/L 1 mg/L 1 mg/L Chloroform 1.0/lg/L 1 ug/L U 1 ug/L U Chloromethane 1.0/lg/L 1 ug/L U 1 ug/L U Chromium 25 /lg/L 25 ug/L U 25 ug/L U Cobalt 10/lg/L 10 ug/L U 10 ug/L U Copper 10/lg/L 10 ug/L U 10 ug/L U Dichloromethane (Methylene Chloride) 1.0/lg/L 1 ug/L U 1 ug/L U Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L 0.1 mg/L Gross Alpha minus Rn & U MDC 1.0 pCiIL o pCiIL o pCi/L Iron 30/lg/L 30 ug/L 30 ug/L U Lead 1.0/lg/L 1 ug/L U 1 ug/L U Manganese 10/lg/L 10 ug/L 10 ug/L U Mercury 0.50/lg/L 0.5 ug/L U 0.5 ug/L U Molybdenum 10/lg/L 10 ug/L U 10 ug/L U Naphthalene 1.0/lg/L 1 ug/L U 1 ug/L U Nickel 20/lg/L 20 ug/L U 20 ug/L U Nitrate + Nitrite (as N) 0.1 mg/L 1 mg/L D 1 mg/L D Selenium 5 /lg/L 5 ug/L 5 ug/L Silver 10/lg/L 10 ug/L U 10 ug/L U Sulfate (mg/L) 1 mg/L 20 mg/L D 10 mg/L D TDS (mg/L) 10 mg/L 10MG/L 10MG/L Tetrahydrofuran 1.0/lg/L Oug/L Oug/L Thallium 0.50/lg/L 0.5 ug/L U 0.5 ug/L U Tin · 100/lg/L Oug/L Oug/L Toluene 1.0/lg/L 1 ug/L U 1 ug/L U Uranium 0.30/lg/L 0.3 ug/L 0.3 ug/L Vanadium . 15 /lg/L 15 ug/L U 15 ug/L U Xylenes (total) 1.0/lg/L 1 ug/L U 1 ug/L U Zinc 10/lg/L 10 ug/L U 10 ug/L U Bicarbonate as HC03 1 mg/L 1 mg/L 1 mg/L Calcium 0.5 mg/L 0.5 mg/L 0.5 mg/L Carbonate as C03 1 mg/L 1 mg/L U 1 mg/L U Magnesium 0.5 mg/L 0.5 mg/L 0.5 mg/L Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L Sodium 0.5 mg/L 0.5 mg/L 0.5 mg/L G-5A: Routine Reporting Limit Check , -, ; MW~32 ' , , 'MW-35 " " 7/9/2012 " " 7/10/2012 " , " " ' QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-B utanone (MEK) 20 !!g/L ----20 ug/L U Acetone 20 !!g/L ----20 ug/L U Ammonia (as N) 0.05 mg/L ----0.1 mg/L Arsenic 5 !!g/L ----5 ug/L U Benzene 1.0 !!g/L ----I ug/L U Beryllium 0.50 !!g/L ----0.5 ug/L U Cadmium 0.50 !!g/L ----0.5 ug/L U Carbon Tetrachloride 1.0 !!g/L ----I ug/L U Chloride (mg/L) 1 rng/L ----I mg/L Chloroform 1.0 !!g/L ----I ug/L U Chloromethane 1.0 !!g/L ----I ug/L U Chromium 25 !!g/L ----25 ug/L U Cobalt 10 !!g/L ----10 ug/L U Copper 10 !!g/L ----10 ug/L U Dichloromethane (Methylene Chloride) 1.0 !!g/L ----I ug/L U Fluoride (Mg/L) 0.1 mg/L ----0.1 mg/L Gross Alpha minus Rn & U MDC 1.0 pCi/L o pCi/L o pCi/L Iron 30 !!g/L ----30 ug/L Lead 1.0 !!g/L ----I ug/L U Manganese 10 !!g/L ----10 ug/L Mercury 0.50 !!g/L ----0.5 ug/L U Molybdenum 10 !!g/L ----10 ug/L U Naphthalene 1.0 !!g/L ----I ug/L U Nickel 20 !!g/L ----20 ug/L U Nitrate + Nitrite (as N) 0.1 mg/L ----0.1 mg/L U Selenium 5 !!g/L ----5 ug/L Silver 10 !!g/L ----10 ug/L U Sulfate (mg/L) 1 mg/L ----50 mg/L D TDS (mg/L) 10 mg/L ----10MG/L Tetrahydrofuran 1.0 !!g/L ----Oug/L Thallium 0.50 !!g/L ----0.5 ug/L Tin 100 !!g/L ----o ug/L Toluene 1.0 !!g/L ----I ug/L U Uranium 0.30 !!g/L ----0.3 ug/L Vanadium 15 !!g/L ----IS ug/L U Xylenes (total) 1.0 !!g/L ----I ug/L U Zinc 10 !!g/L ----10 ug/L U Bicarbonate as HC03 1 mg/L ----I mg/L Calcium 0.5 mg/L ----0.5 mg/L Carbonate as C03 1 mg/L ----I mg/L U Magnesium 0.5 mg/L ----0.5 mg/L Potassium 0.5 mg/L ----0.5 mg/L Sodium 0.5 mg/L ----I mg/L D G-5A: Routine Reporting Limit Check MW-36 MW-37 , -7/1112012 7/30/2012 QAP Reporting 1'- Constituent , Limit RL Qualifjer RL Qualifier 2-B utanone (MEK) 20 !!g/L 20 ug/L U 20 ug/L U Acetone 20 !!g/L 20 ug/L U 20ug/L U Ammonia (as N) 0.05 mg/L 0.1 mg/L U 0.1 mg/L U Arsenic 5 !!g/L 5 ug/L U 5 ug/L U Benzene 1.0 !!g/L 1 ug/L U 1 ug/L U Beryllium 0.50 !!g/L 0.5 ug/L U 0.5 ug/L U Cadmium 0.50 !!g/L 0.5 ug/L U 0.5 ug/L U Carbon Tetrachloride 1.0 !!g/L 1 ug/L U 1 ug/L U Chloride (mg/L) 1 mg/L 1 mg/L 4mg/L D Chloroform 1.0 !!g/L 1 ug/L U 1 ug/L U Chloromethane 1.0 !!g/L 1 ug/L U .1 ug/L U Chromium 25 !!g/L 25 ug/L U 25 ug/L U Cobalt 10 !!g/L 10 ug/L U 10 ug/L U Copper 10 !!g/L 10 ug/L U 10 ug/L U Dichloromethane (Methylene Chloride) 1.0 !!g/L 1 ug/L U 1 ug/L U Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L 0.1 mg/L Gross Alpha minus Rn & U MDC 1.0pCi/L o pCi/L o pCiIL Iron 30 !!g/L 30 ug/L U 30 ug/L U Lead 1.0 !!g/L 1 ug/L U 1 ug/L U Manganese 10 !!g/L 10 ug/L U 10 ug/L U Mercury 0.50 !!g/L 0.5 ug/L U 0.5 ug/L U Molybdenum 10 !!g/L 10 ug/L U 10 ug/L U Naphthalene 1.0 !!g/L 1 ug/L U 1 ug/L U Nickel 20 !!g/L 20 ug/L U 20 ug/L U Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L 0.1 mg/L Selenium 5 !!g/L 5 ug/L 5 ug/L Silver 10 !!g/L 10 ug/L U 10 ug/L U Sulfate (mg/L) 1 mg/L 50 mg/L D 20 mg/L D TDS (mg/L) 10 mg/L 10MG/L 10MG/L Tetrahydrofuran 1.0 !!g/L o ug/L 0.1 ug/L Thallium 0.50 !!g/L 0.5 ug/L 0.5 ug/L U Tin 100 !!g/L o ug/L 0.6 ug/L Toluene 1.0 !!g/L 1 ug/L U 1 ug/L U Uranium 0.30 !!g/L 0.3 ug/L 0.3 ug/L Vanadium 15 !!g/L 15 ug/L U 15 ug/L U Xylenes (total) 1.0 !!g/L 1 ug/L U 1 ug/L U Zinc 10 !!g/L 10 ug/L U 10 ug/L Bicarbonate as HC03 1 mg/L 1 mg/L 1 mg/L Calcium 0.5 mg/L 0.5 mg/L 0.5 mg/L Carbonate as C03 1 mg/L 1 mg/L U 1 mg/L U Magnesium 0.5 mg/L 0.5 mg/L 0.5 mg/L Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L Sodium 0.5 mg/L 1 mg/L D 2mg/L D G-5A: Routine Reporting Limit Check MW-65 -:. MW-65 ."' . 7/11/2012 '. i" 8/16/2012 '." . , QAP Reporting Constituent Limit . -: RL Qualifier RL Qualifier · 2-Butanone (MEK) 20 !!g/L ----20 ug/L U Acetone 20 !!g/L ----20 ug/L U Ammonia (as N) 0.05 mg/L 0.1 mg/L ---- Arsenic 5 !!g/L 5 ug/L U ---- Benzene 1.0 !!g/L ----I ug/L U Beryllium 0.50 !!g/L 0.5 ug/L U ---- Cadmium 0.50 !!g/L 0.5 ug/L U ---- Carbon Tetrachloride 1.0 !!g/L ----I ug/L U Chloride (mg/L) 1 mg/L 1 mg/L ---- Chloroform 1.0 !!g/L ----25 ug/L D Chloromethane 1.0 !!g/L ----I ug/L U Chromium 25 !!g/L 25 ug/L U ---- Cobalt 10 !!g/L 10 ug/L U ---- Copper 10 !!g/L 10 ug/L U ---- Dichloromethane (Methylene Chloride) 1.0 !!g/L ----I ug/L Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L ---- Gross Alpha minus Rn & U MDC 1.0 pCiIL o pCi/L -- Iron 30 !!g/L 30 ug/L ---- Lead 1.0 !!g/L 1 ug/L U ---- Manganese 10 !!g/L 10 ug/L ---- Mercury 0.50 !!g/L 0.5 ug/L U ---- Molybdenum 10 !!g/L 10 ug/L U ---- Naphthalene 1.0 !!g/L ----I ug/L U Nickel 20 !!g/L 20 ug/L U ---- Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L ---- Selenium 5 !!g/L 5 ug/L ---- Silver 10 !!g/L 10 ug/L U ---- Sulfate (mg/L) 1 mg/L 50 mg/L D ---- TDS (mg/L) 10 mg/L 10MG/L ---- Tetrahydrofuran 1.0 !!g/L Oug/L ---- Thallium 0.50 !!g/L 0.5 ug/L U ---- Tin 100 !!g/L Oug/L ---- Toluene 1.0 !!g/L ----I ug/L U Uranium 0.30 !!g/L 0.3 ug/L ---- Vanadium 15 !!g/L 15 ug/L U ---- Xylenes (total) 1.0 !!g/L ----I ug/L U Zinc 10 !!g/L 10 ug/L U ---- Bicarbonate as HC03 1 mg/L 1 mg/L ---- Calcium 0.5 mg/L 0.5 mg/L ---- Carbonate as C03 1 mg/L 1 mg/L U ---- Magnesium 0.5 mg/L 0.5 mg/L ---- Potassium 0.5 mg/L 0.5 mg/L ---- Sodium 0.5 mg/L 0.5 mg/L ---- G-5A: Routine Reporting Limit Check . " . !' > 'MW.;70 7118/2012 ",' QAP Reporting Constituent Limit RL . Qualifier 2-B utanone (MEK) 20 ""gIL ---- Acetone 20 ""gIL ---- Ammonia (as N) 0.05 mglL ---- Arsenic 5 ""gIL ---- Benzene 1.0 ""gIL ---- Beryllium 0.50 ""gIL ---- Cadmium 0.50 ""gIL ---- Carbon Tetrachloride 1.0 ""gIL ---- Chloride (mglL) 1 mglL ---- Chloroform > 1.0 ""gIL ---- Chloromethane 1.0 ""gIL ---- Chromium 25 ""gIL ---- Cobalt 10 ""gIL ---- Copper 10 ""gIL ---- Dichloromethane (Methylene Chloride) 1.0 ""gIL ---- Fluoride (MglL) 0.1 mglL 0.1 mglL Gross Alpha minus Rn & U MDC 1.0 pCilL -- Iron 30 ""gIL ---- Lead 1.0 ""gIL ---- Manganese 10 ""gIL ---- Mercury 0.50 ""gIL ---- Molybdenum 10 ""gIL ---- Naphthalene 1.0 ""gIL ---- Nickel 20 ""gIL ---- Nitrate + Nitrite (as N) 0.1 mglL ---- Selenium 5 ""gIL 5 uglL Silver 10 ""gIL ---- Sulfate (mglL) ImglL ---- TDS (mglL) 10 mglL ---- Tetrahydrofuran . 1.0 ""gIL ---- Thallium 0.50 ""gIL ---- Tin 100 ""gIL ---- Toluene 1.0 ""gIL ---- Uranium 0.30 ""gIL ---- Vanadium 15 ""gIL ---- Xylenes (total) 1.0 ""gIL ---- Zinc 10 ""gIL ---- Bicarbonate as HC03 1 mglL ---- Calcium 0.5 mglL ---- Carbonate as C03 1 mglL ---- Magnesium 0.5 mglL ---- Potassium 0.5 mglL ---- Sodium 0.5 mglL ---- G-5B: Accelerated Reporting Limit Check " .. .,' 'MW-ll 8/7/2012 MW-148/7/2012 , . QAJ> It.epo~ting Constituent Limit RL Qualifier RL Qualifier. 2-Butanone (MEK) 20 f..lglL -------- Acetone 20 f..lg/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5f..lglL -------- Benzene 1.0 f..lg/L -------- Beryllium 0.50 f,tg/L -------- Cadmium 0.50 f..lg/L -------- Carbon Tetrachloride 1.0 f..lglL -------- Chloride (mglL) 1 mglL -------- Chloroform 1.0 f..lglL -------- Chloromethane 1.0 f..lg/L -------- Chromium 25 f..lglL -------- Cobalt 10 f,tg/L -------- Copper 10 f..lglL -------- Dichloromethane (Methylene Chloride) 1.0 f,tglL -------- Fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCilL ------ Gross Alpha minus Rn & U Precision (±) 1.0pCiIL ------ Gross Alpha minus Rn & U 1.0pCilL ------ Iron 30 f..lglL -------- Lead 1.0 f,tg/L -------- Manganese 10 f,tglL 10 ug/L --10 ug/L Mercury 0.50 f..lglL -------- Molybdenum 10 f,tglL -------- Naphthalene 1.0f,tg/L -------- Nickel 20 f..lglL -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5f,tglL -------- Silver 10 f..lglL -------- Sulfate (mg/L) 1 mg/L -------- TDS (mg/L) 10 mg/L -------- Tetrahydrofuran 1.0 f..lglL -------- Thallium 0.50 f..lg/L -------- Tin 100 f..lg/L -------- Toluene 1.0 f..lg/L -------- Uranium 0.30 f..lglL -------- Vanadium 15 f,tg/L -------- Xylenes (total) 1.0 f..lg/L -------- Zinc 10 f,tglL -------- AlC Balance (± 5) BALANCE-W -------- Anions BALANCE-W -------- Bicarbonate as HC03 1 mglL -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mglL -------- Cations BALANCE-W -------- Magnesium 0.5 mg/L -------- Potassium 0.5 mglL -------- Sodium 0.5 mglL -------- G-5B: Accelerated Reporting Limit Check . MW-2S ~/6/2012 .. l\'IW -26 8/8/2012 ,. QAP Reporting · Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 !J,gIL ----20 ugIL U Acetone 20 !J,glL ----20 ugIL U Ammonia (as N) 0.05 mg/L -------- Arsenic 5!J,glL -------- Benzene 1.0 !J,g/L ----I ugIL U Beryllium 0.50 f,lg/L -------- . Cadmium 0.50 !J,glL -------- Carbon Tetrachloride 1.0 !J,glL ----I ugIL U Chloride (mg/L) 1 mgIL ----4mg/L D Chloroform 1.0 !J,glL ----500 uglL D Chloromethane 1.0f,lglL ----I ugIL U Chromium 25 !J,g/L --.~ ------ Cobalt 10 f,lgIL -------- Copper 10 !J,g!l -------- Dichloromethane (Methylene Chloride) 1.0 !J,g/L ----I ugIL Fluoride (MgIL) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCi/L --. -- Gross Alpha minus Rn & U Precision (±) 1.0pCilL ---- Gross Alpha minus Rn & U 1.0 pCi/L ---- Iron 30 !J,g!L -------- Lead 1.0 !J,g/L -------- Manganese 10 f,lg/L -------- Mercury 0.50 !J,g/L -------- Molybdenum 10 !J,g/L -------- Naphthalene 1.0f,lglL ----1uglL U Nickel 20 !J,glL -------- Nitrate + Nitrite (as N) 0.1 mglL ----OJ mg/L Selenium 5 f,lgIL -------- Silver 10 !J,glL -------- Sulfate (mg/L) 1 mglL -------- TDS (mg/L) 10 mglL ----lOMG/L Tetrahydrofuran 1.0 f,lglL -------- Thallium 0.50 !J,g/L -------- Tin 100 f,lglL -------- Toluene 1.0f,lg/L ----I ug/L U Uranium 0.30 !J,g/L 0.3 ug/L 0.3 ugIL Vanadium 15 f,lg/L -------- Xylenes (total) 1.0 !J,g/L ----I ug/L U Zinc 10 !J,g/L ------ AlC Balance (± 5) BALANCE-W ---- Anions BALANCE-W ---- Bicarbonate as HC03 1 mg/L ------ Calcium 0.5 mglL ------ Carbonate as C03 1 mg/L ------ Cations BALANCE-W ---- Magnesium 0.5 mg/L ------ Potassium 0.5 mgIL ------ Sodium 0.5 mglL ------ G-5B· Accelerated Reporting Limit Check MW -30 8/7/2012 MW-318/6/2012 QAP Reporting . Constituent Limit RL Qualifier RL Quaiifier 2-Butanone (MEK) 20 Ilg/L -------- Acetone 20 J.lg/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5 Ilg/L -------- Benzene 1.0 J.lg/L -------- Beryllium 0.50 IlglL -------- Cadmium 0.50 Ilg/L -------- Carbon Tetrachloride 1.0 J.lg/L -------- Chloride (mg/L) 1 mglL 2mg/L D 1 mg/L Chloroform 1.0 Ilg/L -------- Chloromethane 1.0 Ilg/L -------- Chromium 25 Ilg/L -------- Cobalt 10 J.lg/L -------- Copper 10 IlglL -------- Dichloromethane (Methylene Chloride) 1.0 Ilg/L -------- Fluoride (Mg/L) 0.1 mglL -------- Gross Alpha minus Rn & U MDC 1.0 pCi/L ---- Gross Alpha minus Rn & U Precision (±) 1.0 pCi/L ---- Gross Alpha minus Rn & U 1.0 pCi/L ---- Iron 30 IlglL -------- Lead 1.0 IlgIL -------- Manganese 10 J.lglL -------- Mercury 0.50 Ilg/L -------- Molybdenum 10 Ilg/L -------- Naphthalene 1.0 J.lg/L -------- Nickel 20 Ilg/L -------- Nitrate + Nitrite (as N) 0.1 mg/L 2mg/L D 2mg/L D Selenium 5J.lglL 5 ug/L ---- Silver 10 Ilg/L -------- Sulfate (mg/L) 1 mg/L ----4mg/L D TDS (mg/L) 10 mg/L ----lOMG/L Tetrahydrofuran 1.0 Ilg/L -------- Thallium 0.50 Ilg/L -------- Tin 100 J.lglL -------- Toluene 1.0 Ilg/L -------- Uranium 0.30 Ilg/L 0.3 ug/L ---- Vanadium 15 J.lg/L -------- Xylenes (total) 1.0 Ilg/L -------- Zinc 10 Ilg/L -------- AlC Balance (± 5) BALANCE-W ------ Anions BALANCE-W ------ Bicarbonate as HC03 1 mg/L -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Cations BALANCE-W ------ Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-5B: Accelerated Reporting Limit Check MW-358/8/2012 -MW ·65 81712012 QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 !lg/L -------- Acetone 20 !lg/L -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5!lg/L -------- Benzene 1.0 !lg/L -------- Beryllium 0.50 !lg/L -------- Cadmium 0.50 !lg/L -------- Carbon Tetrachloride 1.0 !lg/L -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 !lg/L -------- Chloromethane 1.0 ug/L -------- Chromium 25 !lg/L -------- Cobalt 10 !lg/L -------- Copper 10 !lg/L ----. ---- Oichloromethane (Methylene Chloride) 1.0 !lg/L -------- F1uoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MOC 1.0pCilL o pCilL ---- Gross Alpha minus Rn & U Precision (±) 1.0pCilL o pCiIL ---- Gross Alpha minus Rn & U 1.0 pCi/L 0.2 pCi/L ---- Iron 30 !lg/L -------- Lead 1.0 !lg/L -------- Manganese 10 !!g/L 10 ug/L 10 ug/L -- Mercury 0.50 !lg/L -------- Molybdenum 10 ug/L -------- Naphthalene 1.0 ug/L -------- Nickel 20 !lg/L -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5!!g/L 5 ug/L ---- Silver 10 !lg/L -------- Sulfate (mg/L) 1 mg/L -------- TOS (mg/L) 10 mg/L -------- Tetrahydrofuran 1.0 !lg/L -------- Thallium 0.50 !lg/L 0.5 ug/L ---- Tin 100 !!g/L --------- Toluene 1.0 !lg/L -------- Uranium 0.30 !lg/L O.3Ug/L ---- Vanadium 15 !!g/L -------- Xylenes (total) 1.0 !lg/L -------- Zinc 10 !lg/L ------ AlC Balance (± 5) BALANCE-W ------ Anions BALANCE-W ------ Bicarbonate as HC03 1 mg/L ------ Calcium 0.5 mg/L ------ Carbonate as C03 1 mg/L ------ Cations BALANCE-W ------ Magnesium 0.5 mg/L ------ Potassium 0.5 mg/L ------ Sodium 0.5 mg/L ------ G-5B· Accelerated Reporting Limit Check ,: MW -11 9(19/2012 MW-149/18/2012 ( QAPReporting ~ Constituent Limit RL Qualifier RL . -Qualifier 2-Butanone (MEK) 20 ~g/L -------- Acetone 20 [.tg/L -------- Ammonia (as N) 0.05 mgIL -------- Arsenic 5 ~gIL -------- Benzene 1.0 [.tgIL -------- Beryllium 0.50 ~gIL -------- Cadmium 0.50 ~gIL -------- Carbon Tetrachloride 1.0 [.tglL -------- Chloride (mg/L) 1 mg/L -------- Chloroform 1.0 ~glL -------- Chloromethane 1.0 ~gIL -------- Chromium 25 ~glL -------- Cobalt 10 [.tg/L -------- Copper 10 uglL -------- Oichloromethane (Methylene Chloride) 1.0 [.tWL -------- Fluoride (MgIL) 0.1 mgIL -------- Gross Alpha minus Rn & U MOC 1.0 pCiIL ---- Gross Alpha minus Rn & U Precision (±) 1.0 pCi/L ---- Gross Alpha minus Rn & U 1.0 pCilL ---- Iron 30 ~g/L -------- Lead 1.0 [.tgIL -------- Manganese 10 ~g/L 10 ugiL -- Mercury 0.50 ~g/L -------- Molybdenum 10 [.tg/L -------- Naphthalene 1.0 ~gIL -------- Nickel 20 ~glL -------- Nitrate + Nitrite (as N) 0.1 mg/L -------- Selenium 5~glL -------- Silver 10 ~g/L -------- Sulfate (mwL) 1 mg/L -------- TOS (mg/L) 10 mgIL -------- Tetrahydrofuran 1.0 ~g/L -------- Thallium 0.50 ~glL -------- Tin 100 [.tg/L -------- Toluene 1.0 ~g/L -------- Uranium 0.30 !LglL -------- Vanadium 15 [.tglL -------- Xylenes (total) 1.0 ~g/L -------- Zinc 10~glL -------- NC Balance (± 5) BALANCE-W ------ Anions BALANCE-W ------ Bicarbonate as HC03 1 mglL -------- Calcium 0.5 mglL -------- Carbonate as C03 1 mglL -------- Cations BALANCE-W ------ Magnesium 0.5 mgIL -------- Potassium 0.5 mg/L -------- Sodium 0.5 mglL -------- G-5B' Accelerated Reporting Limit Check MW-2S 9/18/2012. MW -269/19/2012 QAP Reporting Constifuen~ Limit RL Qualifier. RL Qualifier 2-Butanone (MEK) 20 flglL ----20 ugiL UH Acetone 20 flg/L ----20 ug/L UH Ammonia (as N) 0.05 mg/L ------ Arsenic 5flglL -------- Benzene 1.0 flg/L ----lug/L UH Beryllium 0.50 flg/L -------- Cadmium 0.50 f.,tg/L -------- Carbon Tetrachloride 1.0 flg/L ----I ug/L UH Chloride (mglL) 1 mg/L ----2mg/L D Chloroform 1.0 flg/L ----100 ugiL DH Chloromethane LOflglL ----I ug/L UH Chromium 25 flg/L -------- Cobalt 10 f.,tg/L -------- Copper 10 flg/L -------- Dichloromethane (Methylene Chloride) 1.0 f.,tg/L ----lugiL H Fluoride (MglL) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1,0 pCi/L ---- Gross Alpha minus Rn & U Precision (±) 1,0 pCi/L ---- Gross Alpha minus Rn & U 1,0 pCi/L ---- Iron 30 flg/L -------- Lead 1.0 f.,tg/L -------- Manganese 10 flg/L -------- Mercury 0.50 flglL -------- Molybdenum 10 flg/L -------- Naphthalene 1,0 flg/L ----lug/L UH Nickel 20 flg/L -------- Nitrate + Nitrite (as N) 0.1 mg/L ----OJ mg/L Selenium 5 flg/L -------- Silver 10 flg/L -------- Sulfate (mg/L) 1 mg/L -------- TDS (mg/L) 10 mg/L -------- Tetrahydrofuran 1.0 flg/L ------,-- Thallium 0.50 flg/L -------- Tin 100 flg/L -------- Toluene 1.0 flglL ----I ug/L UH Uranium 0.30 f.,tg/L 0.3 ug/L 0.3 ugiL Vanadium 15 flg/L -------- Xylenes (total) 1.0 flg/L ----I ug/L UH Zinc 10 flg/L ------ AlC Balance (± 5) BALANCE-W ---- Anions BALANCE-W ---- Bicarbonate as HC03 1 mg/L ------ Calcium 0.5 mg/L ------ Carbonate as C03 1 mglL ------ Cations BALANCE-W ---- Magnesium 0.5 mg/L ------ Potassium 0.5 mglL ------ Sodium 0.5 mglL ------ G-SB: Accelerated Reporting Limit Check , MW -30 9/19/2012 MW-319/18/2012 "I QAP Reporting Constituent Limit RL Qualifier RL Qualifier 2-Butanone (MEK) 20 ftglL -------- Acetone 20 ftg/L -------- Ammonia (as N) O.OS mglL -------- Arsenic SftglL -------- Benzene 1.0 ftg/L -------- Beryllium 0.50 ug/L -------- Cadmium 0.50ftglL -------- Carbon Tetrachloride 1.0 ftg/L -------- Chloride (mg/L) 1 mglL 1 mg/L 1 mg/L Chloroform 1.0 ftglL -------- Chloromethane 1.0 ftglL -------- Chromium 2SIlg!l -------- Cobalt 10 Ilg/L -------- Copper 10 ftg/L -------- Dichloromethane (Methylene Chloride) 1.01lg/L -------- fluoride (Mg/L) 0.1 mg/L -------- Gross Alpha minus Rn & U MDC 1.0 pCiIL ---- Gross Alpha minus Rn & U Precision (±) 1.0 pCilL ---- Gross Alpha minus Rn & U 1.0 pCi/L ---- Iron 30 ftglL -------- Lead 1.0 Ilg/L -------- Manganese 10 Ilg/L -------- Mercury O.SO ftglL -------- Molybdenum 10 Ilg/L -------- Naphthalene 1.0 Ilg/L -------- Nickel 20 ftglL -------- Nitrate + Nitrite (as N) 0.1 mg/L 2mgIL D 2mglL D Selenium S Ilg/L S uglL ---- Silver 10 ftglL -------- Sulfate (mg/L) 1 mg/L ----4mgIL D TDS (mglL) 10 mglL ----lOMGIL Tetrahydrofuran 1.0 ug/L -------- Thallium 0.50ftglL -------- Tin 100 Ilg/L -------- Toluene 1.0 ftglL -------- Uranium 0.30 Ilg/L 0.3 ugIL ---- Vanadium IS Ilg/L -------- Xylenes (total) 1.0 ftg/L -------- Zinc 10 Ilg/L -------- NC Balance (± S) BALANCE-W ------ Anions BALANCE-W ------ Bicarbonate as HC03 1 mg/L -------- Calcium O.S mg/L -------- Carbonate as C03 1 mgIL -------- Cations BALANCE-W ------ Magnesium O.S mg/L -------- Potassium O.S mglL -------- Sodium O.S mglL -------- G-5B: Accelerated Reporting Limit Check " '-' e' MW."35 9/19/2012' . MW-65 9/1912012 .' .-. " " , QAP Reporting' ConstitUent ,. Limit RL Qualifier RL Qualifier ' 2-Butanone (MEK) 20/-lg/L -------- Acetone 20/-lglL -------- Ammonia (as N) 0.05 mg/L -------- Arsenic 5/-lg/L -------- Benzene 1.0/-lg/L -------- Beryllium 0.50/-lg/L -------- Cadmium 0.50/-lgiL -------- Carbon Tetrachloride 1.0/-lg/L -------- Chloride (mgIL) 1 mg/L -------- Chloroform 1.0/-lg/L -------- Chloromethane 1.0/-lglL -------- Chromium 25/-lgiL -------- Cobalt 10/-lg/L -------- Copper 10 /-lgiL -------- Oichloromethane (Methylene Chloride) 1.0/-lg/L -------- Fluoride (MglL) 0.1 mg/L -------- Gross Alpha minus Rn & U MOC 1.0 pCi/L o pCilL o pCi/L Gross Alpha minus Rn & U Precision (±) 1.0 pCi/L o pCi/L o pCilL Gross Alpha minus Rn & U 1.0 pCilL 0.2 pC ilL 0.2 pCilL Iron 30/-lg/L -------- Lead 1.0/-lg/L -------- Manganese 10 /-lg/L 10 ug/L 10 ug/L Mercury 0.50 ug/L -------- Molybdenum 10/-lg/L --/ ------ Naphthalene 1.0/-lg/L -------- Nickel 20/-lgiL -------- Nitrate + Nitrite (as N) O.l mglL -------- Selenium 5/-lg/L 5 ug/L 5 ug/L Silver 10 /-lg/L -------- Sulfate (mglL) 1 mg/L -------- TOS (mglL) 10 mg/L -------- Tetrahydrofuran 1.0/-lg/L -------- Thallium 0.50/-lglL 0.5 ug/L 0.5 ug/L U Tin 100/-lg/L -------- Toluene 1.0/-lg/L -------- Uranium 0.30/-lglL 0.3 ug/L 0.3 ug/L Vanadium 15 uglL -------- Xylenes (total) 1.0/-lg/L -------- Zinc 10 /-lg/L -------- NC Balance (± 5) BALANCE-W ------ Anions BALANCE-W ------ Bicarbonate as HC03 1 mglL -------- Calcium 0.5 mg/L -------- Carbonate as C03 1 mg/L -------- Cations BALANCE-W ------ Magnesium 0.5 mg/L -------- Potassium 0.5 mg/L -------- Sodium 0.5 mg/L -------- G-6A: Trip Blank Evaluation All trip blanks for the 2012 Third Quarter samples were nondetect. Blank Sample Date Laboratory EL -C12070448 7/13/2012 Energy Laboratories EL -C12080830 8/16/2012 Energy Laboratories EL -C12080143 8/3/2012 Energy Laboratories AWAL -1207185 -THF and Tin 7/9/2012 American West Analytical Laboratories A W AL -1208066 -THF and Tin 7/30/2012 American West Analytical Laboratories G-6B: Trip Blank Evaluation All trip blanks for the Accelerated samples were non detect. Blank Sample Date Laboratory 1 8/812012 Energy Laboratories 2 9/1912012 Energy Laboratories G-7 A: QAlQC Evaluation for Routine Sample Duplicates ... Constituent MW-26 MW-65 %RPD Nitrate + Nitrite (as N) 1.9 2.1 10.00 Iron 773 793 2.55 Manganese 1100 1200 8.70 Selenium 5 5.1 1.98 Uranium 28.4 30.2 6.14 Chloroform 970 960 1.04 Dichloromethane (Methylene Chloride) 4.9 5.2 5.94 Chloride (mg/L) 78 74 5.26 Field pH (S.U.) 7.1 6.72 5.50 TDS (mgIL) 3060 3130 2.26 Bicarbonate as HC03 382 390 2.07 Calcium 493 463 6.28 Cations BALANCE-W 45.6 45.3 0.66 Magnesium 152 161 5.75 Potassium 9.5 10.4 9.05 Sodium 189 201 6.15 Radiologic Duplicate Tests Gross Alpha minus Rn & U MDC 0.2 0.2 0.00 Gross Alpha minus Rn & U* 1.8 2 0.471 Gross Alpha minus Rn & U Precision (±) 0.3 0.3 * Duplicate checks reported for gross alpha minus RN and U are not %RPD. Calculated values are based on the formula in the approved QAP. Constituent MW-03 MW-70 %RPD Selenium 51.1 48.6 5.02 Fluoride (MgIL) 0.96 1.02 6.06 G-7B: QAlQC Evaluation for Accelerated Sample Duplicates :, < 'c MW-14 .. MW-65 •... " Constituent 817/2012 817/2012' .%RPD Manganese 2300 2250 2.20 MW-35 MW-65 · Constituent 9/19/2012 9/19/2012 %RPD Manganese 283 273 3.60 Selenium 8.2 9.7 16.76 Thallium 0.54 0.5 7.69 Uranium 22.9 22.6 1.32 Radiologic RPD Tests Gross Alpha minus Rn & U MDC 0.2 0.2 0.00 Gross Alpha minus Rn & U 5.4 6 0.71 Gross Alpha minus Rn & U Precision (±) 0.6 0.6 G-8A: Radiologics Counting Error '" Gross Alpba Gross Alpha minusRn&U Counting , Well . Sample Date minus Rn & U Precision (±) ... Error ~'20% . MW-02 7/1612012 0.9 0.2 N MW-11 711112012 0.3 0.1 N MW-14 711112012 0.2U 0.1 N MW-25 711012012 0.7 0.2 N MW-26 711112012 1.8 0.3 Y MW-27 711612012 1.2 0.3 N MW-30 711012012 0.3 0.1 N MW-31 7/912012 0.3 0.1 N MW-32 7/912012 1.4 0.2 Y MW-35 7/1012012 3.5 0.3 Y MW-36 7/1112012 0.6 0.2 N MW-37 7/3012012 2.9 1.2 N MW-65 7/1112012 2 0.3 Y N/A -the counting error is less than 20% of the activity as required by the GWDP. The value is above the GWCL and this check column is not applicable. NC -Sample results were nondetect and as such the check is not applicable .' Within GWCL GWCL? 3.2 Y 3.75 Y 7.5 NC 7.5 Y 4.69 Y 2 Y 3.75 Y 7.5 Y 3.33 Y 3.75 NA No GWCLs have been set 4.69 Y G-8B: Radiologies Counting Error for Accelerated Samples Gross Alpha Counting Gross Alpha minusRn&U Error~ Well Sample Date . minus Rn' & tJ Precision (±) 20% MW-35 8/8/2012 4.2 0.5 Y MW-35 9/19/2012 5.4 0.6 Y N/A -the counting error is less than 20% of the activity as required by the GWDP. The value is above the GWCL and this check column is not applicable. GWCL NA NA G-9A: Laboratory Matrix QC Matrix Spike % Recovery Comparison 'MSD Lab Report Well Analyte MS %REC %REC REC Range ,-R;PD C12070448 NA Naphthalene 80 102 70 -130 25 C12070448 MW-35 Chloromethane 71 88 70 -130 21 C12070448 NA Acetone 69 68 70 -130 1.7 C12070741 NA Manganese* NC NC 70 -130 NC C12080830 NA Naphthalene 83 103 70 -130 21 C12080143 NA Methylene Chloride 68 65 70 -130 4.2 NA = MS samples were not Denison samples. *= Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike level. Surrogate % Recovery Lab Specifi.ed QAP Surrogate REC · ' Required Lab 'Report WelVSample Analyte %REC Range ' Range C12070448 MW-31 p-Bromofluorobenzene 78 80 -120 None C12070448 MW-35 p-Bromofluorobenzene 75 80 -120 None C12070448 Trip Blank p-Bromofluorobenzene 78 80 -120 None C12070448 Method Blank p-Bromofluorobenzene 79 80 -120 None C12070448 Method Blank p-Bromofluorobenzene 78 80 -120 None LCS % Recovery ,. QAP t" . Lab Specified 'Required Lab Report Analyte LCS %REC REC Range Range C1208143 Gross Alpha 131 70 -130 None Method Blank detections QAP Reported Required Lab Report WelVSample ' 'Analyte Concentration RL C12080143 Method Blank Bicarbonate 1.52 mg/L 1.0mg/L G-9B: Accelerated Laboratory Matrix QC M 0 S ok ~ R C atrIX 'pl e o ecovery omparIson L~b'Report Well Analyte MS%REC ',' MW-65 (duplicate of C12080469 -August Accelerated MW-14) Manganese* NC C12090804 -September Accelerated NA Nitrate+Nitrite as N 116 *= Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike level. NA = MS samples were not Denison samples. Laboratory Control Sample Lab Report Analyte '·LCS %REC C12080469 -August Accelerated Gross Alpha 78 Surrogate % Recovery All surrogate recoveries were witin the laboratory established recovery ranges. Lab Specified .RECRange 80 -120 'MSD %REC NC 113 QAPRequired Range None RECRange RPD% 70-130 NC 90 -110 1.9 TabH Kriged Current Quarterly Groundwater Contour Map @ estimated dry area M.W-S perched monitoring well showing 5503 elevation in feet amsl TW04-12 temporary perched monitoring well 5583 showing elevation in feet amsl TWN-10 A 5586 temporary perched nitrate monitoring V well showing elevation in feet amsl PIEZ-1 perched piezometer showing ~ 5593 elevation in feet amsl TW4-27 temporary perched monitoring well ~ 5526 installed October, 2011 showing elevation in feet amsl RUIN SPRING 6 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are pumping wells KRIGED 3rd QUARTER, 2012 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H :/718000/nov121UwI0912.srf H-l Tab I Groundwater Time Concentration Plots =r ....... til) .§. CII :'5! 0 ::E u =r bo .§. CII :'5! 0 :J u::: Time concentration plots for MW-01 Chloride in MW-Ol 60 ~--------------------------------------------------------~ sO t----------1-----------------------------------------------J 40 30 20 10 Sample Date Fluoride in MW-Ol 0.6 0.5 0.4 0.3 0.2 0.1 o ~----~----~----~----~----~----~----~------~---J Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non"Detected Values 5000 4500 4000 3500 :J' 3000 "D:o E i 2500 J!! ~ 2000 1500 1000 Time concentration plots for MW-01 Sulfate in MW-Ol - • ~ ..... ---JIll -.... --~ ........ ~ ----..... -r .. ... U -..,... ....,... r r I 4 500 Sample Date Uranium in MW-Ol 12 r-------------------------------------------------------~ 10 t-r---------------------------------------------------~ 8 t1t---------------------------------------------~ :J' ~ § 6t-1t--------------------------------------------------J 'c IV => 4 ~Hr---1t--Jt~--~-1r--f~-----------------------~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-02 Chloride in MW-02 80 r-------------------------------------------------------~ 70 r----------1r------------------------------------------------J 60 r----------1t------------------------------------------------J ~ so r-----------1r---------------------------------------------------J "aD .s ~ 40 r-----------1t---------------------------------------------------J o ::c u 30 r-----------tt---------------------------------------------------J 2°tl~~n_--tt~------------------------------------------J 10 0.9 0.8 0.7 0.6 ~ "aD .s 0.5 Q.I 'a .~ 0.4 ::l u::: Sample Date Fluoride in MW-02 A ~/ ~ lIlA...&. _ 0.3 ~f\ V ~. 0.2 0.1 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Nan-Detected Values Time concentration plots for MW-02 Sulfate in MW-02 2500 r-------------------------------------------------------------~ ~ 1500 r111N1------1--------------6----------------------------------~ co .§. .2! J!! ~ 1000 rt~g---------------------------------------------------------~ 500 ~~r---------------------------------------------------------J 20 18 16 14 ~ 12 co -= E 10 ::s ·c ~ 8 ::J f-~ I 14 6 4 2 .A .( \ ~ 0 ~"> ~ 0 I ~ ~,,>'\ ~o Sample Date Uranium in MW-02 ~ I~ \ \ Sample Date ~ r ". lj \1 - d / \/ V Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non·Detected Values Time concentration plots for MW-03 Chloride in MW-03 160 140 . 120 ::i' 100 -lID .§. <II 80 "a "§ ::c u 60 40 20 0 (;,,0, 9J'? ~ 0 '>v Sample Date Fluoride in MW-03 1.2 r--------------------~--------. 1 r-------------------------------.--~------------J 0.8 ,------------------... ------'-LJ ::i' "Qo .§. ~ 0.6 r-1Ie;~==~------------------------------Jl------~--~~~-J (; ::l i!: 0.4 0.2 r--r---------------------------J Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-03 Sulfate in MW-03 4500 4000 3500 3000 ::J -~ 2500 .2l J!! 2000 :; III 1500 1000 500 0 -\0) (f 0 Sample Date Uranium in MW-03 80 r-----------------------------------------------------~ 70 t-------~~----------------------------------------~ 60 t---------t------------------------------------------------J ::J 50 t----------lH-----------------------------------------------------J ~ § 4°t---------tt--------------~Ir----~----~~~~-,~----~ 'c f! ~ 3°t----------t1~~~t~~ .. a__i~~~~------------II~~----~ 20 10 Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-03A Chloride in MW-03A 80 .r-------------------------------------------------------~ 70 -t---.---4l----- ~ 50 r--------------------------.----~f_---\--~------------------------J Qo .s ~ 40 r---------------------------------------~-------------------J o ::c u 30 r---------------------------------------------------------------------J 20 T--------------------------.----- 10 r---------------------------------.----------------------- Sample Date Fluoride in MW-03A 1.8 r -------------------------------. 1.6 ..... ----------- 1.4 n-~~-------:iir----j~-=--~-----·------I 1.2 t1rt---1r-=:::;;;;~=---"""'r__J~----\----4~~------J ~ -r 1 t-~----~-1~-----------~~--------~~~~-------~~::~ Qj "a "g 0.8 r------~t-t-----------------------------------------I i:i: 0.6 t--"-----hl----·------------------- 0.4 ,------1rt-------------------------1 0.2 ,-----1t-------------------------I Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-03A Sulfate in MW-03A 4500 r-------------------------------------------------------------~ 4000 ~----------------------------------------------------------~ 3500 t7~ ................. -~L. 3000 r-----------------------------------------------------------------J ::i" -~ 2500 ~------------------------------------------------------------~ CI.l ~ 2000 :; VI 1500 ~------------------------------------------------------------~ 1000 r---------------.----------------------------~--------------~ 50:t-·-· Sample Date Uranium in MW-03A 40 35 30 ::i" 25 -3 E 20 ::J '2 "' ::l 15 I I\. , J '---. , ./ 1 , --f ---~ ~ 10 I I 5 0 ~ !:)~ ~ ..... ~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values ::i" -QO .§. Qj ~ 0 ::c u ::i" -QO .§. Qj ~ 0 :J u::: Time concentration plots for MW-05 Chloride in MW-OS 140 120 100 80 60 40 20 t-1t--------------------------------------------------------~ 1.8 1.6 1.4 1.2 1 0.8 0.6 0.4 0.2 0 .xCbt:> ~'? (f ~'b <::)'1; Sample Date Fluoride in MW-OS Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Vafl:Je5 Time concentration plots for MW-05 Sulfate in MW-OS 9000 8000 7000 6000 :::i -~ 5000 CII .i 4000 "'5 11'1 3000 _A I . ---A. ..... --2000 -,. ..-, v ' -1000 Sample Date Uranium in MW-OS 35 r-----------------------------~----------------------~ 30 t---------------------------------------------------~~ 25 t------------------------------------------------------J--J :::i ~ 20 t-------------------------------------------------------------~-J E ::J ·c ~ 15 t-------------------------------------------------------------Jl-IU :::) 10 t---,---------------------------------------------------~~ 5 t-----------------------OF----------------------~~~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values 80 70 60 ~ 50 ...... QII .5- Qj 40 :2 (; :E u 30 20 10 0 9;,'1.-(f ~e; 0.8 0.7 0.6 ~ 0.5 ti.o .5- Qj 0.4 "t:J ";: o = ii: 0.3 0.2 0.1 Kq,~ ~'b Time concentration plots for MW-11 Chloride in MW-ll Sample Date Fluoride in MW-ll Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 ..... lJ ~1 ~Jt r\ ."'1" Detected Values • Non-Detected Values Time concentration plots for MW-11 Sulfate in MW-ll 2500 r-------------------------------------------------------------~ 2000 r-1t------------------------------------------------------------J ~ 1500 t-.r-----------------1t----------------------------------------~ tio E. ~ J!! ~ 1000 ~l1~liiJ"iP,.~~.,~~~~lL==~~~--------~~~~~~--~ 500 r-----U---------------------------------------------------~ Sample Date Uranium in MW-ll 4.5 r---------------------------------------------------------~ 4 T---------------------.~---- 3.5 r---------.----------~-------------------------------------J 3 t---------------~----------~~----------------~ ~ tio ~2.5 r------------..------ti---------------~~--------------------~ E :::J .~ 2 t------------t----~~~-----------,~----------------------J ~ 1.5 r-----:It----f-t-1t--.;-:I-----IHlt-..J·--------! Sample Date Detected Value~ White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected. Values Time concentration plots for MW-12 Chloride in MW-12 160 140 120 1-----1r---------------------------------------------------1 ::! 100 ........ tl.D .§. CIJ 80 "a "t:; 0 ~ u 60 40 20 0 ~ .xCO ~'b' Sample Date ._-----------------------------....., Fluoride in MW-12 0.4 r -------------------------------. 0.35 +------ ::! 0.25 ;---------- 'iio .§. ~ 0.2 ;-------- "t:; o :::s u:: 0.15 -------------------------------------- 0.1 r--------------------------------------------------~ 0.05 ,----------------------------------1 O +-----~----~------r_----~----_.----~---- .xCO'? ~'b' Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non·Oetected Values 9000 8000 7000 6000 ::::J -~ 5000 QI ~ 4000 :i VI 3000 2000 1000 --- ...I -- Time concentration plots for MW-12 Sulfate in MW-12 ... -AlII .... . ..... ~~ y ...... -)I V' ~ ..a... ....... ~ --• - Sample Date Uranium in MW-12 25 r-------------------------------------------------------~ 20 t-----~~----------~--~----------~~~~-----ll-----~~~ 5 +---~------------, Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Va'lues I I Time concentration plots for MW-14 Chloride in MW-14 40 35 30 ::J 25 "Qa .s cv 20 :2 0 :i: u 15 10 5 0 ,¥q,o, '" ,¥o,':I< ~ (Jo,o, ~o, ~o, ~o ~'rI ~o ~'rI ()'l; Sample Date Fluoride in MW-14 0.3 0.25 0.2 ::J -a.o .s cv 0.15 "t:J ";:: 0 :s u::: 0.1 0.05 o +-----~------~----~------~----_r------~----~ ~o,o, ~'rI Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Values Time concentration plots for MW-14 Sulfate in MW-14 2500 r-------------------------------------------------------------~ 2000 lIt1~~_1t_----------------~~~~~-------I~~----~UL------J ~ 1500 tID E.. ~ ~ ~ 1000 t---------------------------------------------------------------J =r '-~ E ::J ·c ~ ::J 500 t-----------------------------------------------------------~ O +-----~--~----~----~----~----~----~----~--~ ~q;,0) ~o 120 100 80 40 Sample Date Uranium in MW-14 20 ~---------tt-----------------------------~----------~ 0 +-----1----~----~----~----~----~----~--~-----J ~q;,0) or.; Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Nan-Detected Va·lues Time concentration plots for MW-15 Chloride in MW-1S 60 50 40 :::i' liD ..s Qj 30 :5! 0 :c u 20 10 t-------------------------------------------------------J 0 ~c:oo, '" ~o,~ ~ ~o,o, $)'" ~~ sY-~o, ~o, ~~o, ~v ~o ~'li ~o ~'li ~o ~~ ~o ~"t>..J\ ~o ~'li Sample Date Fluoride in MW-1S 0.4 .,----------------------------...., 0.35 ,----,--------------iii"---------------1 :::i' 0.25 ,------1r--t------~ ....... ~,c:.~ .... ---'r-----:::---:---.------:lIa--I liD ..s ~ 0.2 1-------t--t--------------------·-----1 .~ ~ u::: 0.15 ,--.-----4H-------------------------I 0.1 j------.t---------------------1 0.05 1-------------------------------1 o +----.... .. ---,.---....---r------..-- ~o,o, ~'li Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-15 Sulfate in MW-lS 3000 r-----------------------------------------------------------~ 2500 1tir--------.-a-------------------------------~~----·------~ 2000 1tt1t-------------~------------------------------------------J ~ 'Qa E i 1500 llr-------------------------------------------·----------------·~ ~ :; \I) 1000 t----------------------------------------------------------------J 500 r----------------------------------------------------------~ 0 ~tpO) '" ~O)'i>< C\ ~O)O) ~'" ~~ C\ ;:>:.0) ;:>:.0) i) ~r;:,0) ;:>:.V' ~o ~rt; ~o ~rt; ~o ~'l>~ ~o ~rt; ~o ~'l> Sample Date Uranium in MW-lS 70 r-------------------------------------------------------~ 60 ~----------------------------------------------------~ ~ ~40 t-~_tt_~t_--_tlf~~~~tI~-----------I---------~~--------~~ E :::J .~ 30 t-~r__t-"'rt...!!!..------=------------------I~------l :; 20 ~--------~t---------.--------------------------------~ 10 t-"----------ir-------------------------------------------J O +-----~--~----~----~----~----~----~--- Sample Date Detected Value~ White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values ~ aa .5- QI :2 0 ::2 u Time concentration plots for MW-17 Chloride in MW-17 60 50 40 30 20 10 t------------------------------~--.----------------------------~ O +-----~-----~----~------r_----~----~----_r----~----~ ,¥OJ'" ~o Sample Date Fluoride in MW-17 0.45 ,-------------------------------....., 0.4 t-------------------------------~~~---------------------~ 0.35 t---~~----------------f----\------------I 0.3 t-7~---... -.. IIIiiiO:=-------=--:~--\----:::---------~ ~ aa .5-0.25 t---------------------=------------...--:~~~~-=:~ QI "tS .~ 0.2 -t---------------- :::J u::: 0.15 -t----------.------ 0.1 t------------------------------------------------------~ 0.05 t---------------------------------~ Sample Date Detected Value~ White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-17 Sulfate in MW-17 3500 ~----------------------------------------------------------------~ 3000 T-----------------------------------------------------' ~ ~ 2000 ~-tt---1r--~-----------------------------------------------------1 .§. ~ ~ 3 1500 \I) 1000 t----------1~------------------,----------------------.------------~ 500 t-----------------------------------------------------------------~ 0 ~?>", ~ 9)'\ !') ~ .... 5:>'" ~<, ~'b ~-$ '), ~~ ;:1\05 ~ ~O5 c.,~<'i ~o~ c «,qJ1 ;:1\ .... ~~ \V ~v <:)q; ~~ ~~ Sample Date Uranium in MW-17 50 45 40 35 ~ 30 ~ E 25 ::J 'c ~ 20 :::) 15 10 5 0 ~?>", ~ ~ ;:1\05 ~ ~~ ~~ \V Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-18 Chloride in MW-18 80 70 60 ':J' 50 "-a.o .5. GI 40 ~ 0 :c u 30 20 10 0 ~'i'J'? ~ -xOj ~'b ~'b Sample Date Fluoride in MW-18 0.45 1 -----------------------------..... 0.4 TIIiii~=_---------------------------J 0.35 I---~:_------::;,;i~~-\-----------------I 0.3 I-·---~ ...... II!!::...-----_\_-___,~------------J ':J' a:o .5. 0.25 I----------------\;~,L--.:~-----------I GI ~ '§ 0.2 +----- ~ u::: 0.15 1-----------------------1-1-------1 0.1 r-------------------------------~---------J 0.05 r-------------------------I~------I Sample Date Dete(:ted Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-18 Sulfate in MW-18 2500 r-----------------------------------------------------------~ 2000 +----- ~ 1500 ~~~----------------~~~~L---------------------------------J .§. ~ ~ ~ 1000 r---------------------------------------------------------------J 500 t-----------------------------------------------J Sample Date Uranium in MW-18 60r-------------------------------------------------------~ 50 1-------------------------------------------------------=----~ 40 ::::J -~ E 30 ::J 'c ~ :) 20 10 t-~t\--~~------------------------------------------~ Sample Date Detec.ted Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • NOll-Detected Values Time concentration plots for MW-19 Chloride in MW-19 100 90 80 70 :J' 60 ~ .5- Qj 50 ~ 0 ::c 40 u 30 20 10 L:~~ n ~ ~'li ;:xOj r:f ~~ ,;<> Sample Date Fluoride in MW-19 1.6 -,---------------------------....... 1.4 r---------------------...------------I 1.2 ,------------------1--4 -----.:-------1 :J' 1 t--------------~ .. _.~---------~~--------~~=1~~~~~~~1 ~ .5- Qj 0.8 ~-----------.-------------_I_I_------I ~ I o :::J ~ 0.6 r------------------------------------------~~----------~ 0.4 1----------------~---_I_-----1 0.2 I--------------------~I_------I o +-------r------~-------_r-------r_------r_----~----___._-----~------4 ;:xOjOj ~~ Sample Date Detected Value!; White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Nan-Detected Values Time concentration plots for MW-19 Sulfate in MW-19 3000 r---------------------------------------------------------------- 2500 t-~r-------------------------------------------~---------------J 2000 +-~~------------~~~~~----------------------------------~ ::; 'Qa E i 1500 ,---t-------~~-------------l~~~----.------------------------J ~ :; \I) ::; ....... ~ E ::J ·c ~ ::l 1000 t----1~~--------------------~~------~~----~------------llJ 500 t-----------------------------~-----------=~~~~~~~~~ 0 ~?J", n ~ P} ~"y ~", ~<, ~<tJ ~~ ;:xOj ~ ~Oj "e~ ~o~ G «.~ ~"yf::> ;:xV ~~ ".;:). ~.;:). <::)q; ~~ ~~ Sample Date Uranium in MW-19 30 25 20 15 10 5 t----------------------------------------------------~ 0 ~OJ'" n ~ ~OJOJ ~"y ,¥f::>'" ~" ~'tJ ~~ lj ~ "e~ G «.~ ~~ ;:xV ~~ ".;:). ~.;:). ~o <::)q; ~~ ~~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-20 Chloride in MW-20 80 r-----------------------------------------------------------~ 70 t---------------------------------------------------~~-----J 60 t-----------------------------~~--~=---------~~~1l~~~ ~ 50 r----------==-__ --~---------------------------------------------J liD .§. ~ 40 r----------------------------------------------------------------J .~ :E u 30 r-------------------------------------------------------------.---J 20 t-------------------------------------------------------------J 10 t------------------------------------------------------------J Sample Date Fluoride in MW-20 0.4 r------------------------------------------------------------ 0.35 +---------------:~~~~~~ .... .-------~ 0.3 t-------:7 ....... 1--4------------------------~-----------.... ~ 0.25 t:::;;;r/F-------------------. ---------------------------.~,...",..~:.-.-___I liD .§. ~ 0.2 r-------------------------------------------------I (; ::l u::: 0.15 +-______ . 0.1 +-------------- 0.05 +----. Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non"Detected Values 4500 4000 3500 3000 :::J "'-~ 2500 ~ J!! 2000 :; I/) 1500 1000 500 0 co,~ ,>'/; 40 35 30 :::J 25 "'-l1li ..:!: E 20 ~ 'c E :::> 15 10 5 0 co,~ ,>'/; ~o,fo ~o ~o,fo ~o Time concentration plots for MW-20 !b (Yo, 0 Sulfate in MW-20 Sample Date Uranium in MW-20 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Values Time concentration plots for MW-22 r-----------------------------------------------------.--------~ 80 70 60 ::J 50 tiD E. Qj 40 ~ o ~ u 30 20 10 o .---- ....... Chloride in MW-22 --,(J A 1 .----'vr ~y .---- Sample Date Fluoride in MW-22 6 r-----------------------------------------------~ 5 +------ 4 r---------------------------~------------~---------J 2 t----------------------------.----------------------------~ o +-----~------~----_.------~----- Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected. Values Time concentration plots for MW-22 Sulfate in MW-22 7000 r-----------------------------------------------------------~ 6000 r-------------------------------------------------~----------~l 5000 r---------------------------------------~~~~~~~~~-l~ ~ Qo 4000 t----------"",..."..II!!!!!!==----. .§. ! ~ J 3000 t---------------------------------------------J 2000 r-----------------------------------------------------------------J 1000 r-------------------------------------------------------------J Sample Date Uranium in MW-22 60 ~----------------------------------------------------------------------------------------------------~ 40 ~ "-~ E 30 ::::s ·c I! ::J 20 10 t--------------------------------------------------------------~ 0 .,-- ~O)t;,. ~O)fo ~O)CQ t;::,t:::> t;::,'" ~ ~t:::>fo t;::,CQ ~..."t:::> ~v ()'l' ~o 0(.; c.,e~ c.,e~ ~'V ~ ~oS "oS "oS ~~ ~~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-23 Chloride in MW-23 35 30 j-----------------------------~------- 25 r--------------------------i~-------------------------------J :J -~ 20 t--------------------------~Hr·----------------------------------j .§. GI 't:J "§ 15 t--------------------------1H~--------------------------------j ~ u 10 r-------------------~~-~~~~-------------------------J 5 r-------------.----~----~--~--~~--~--------~-J 0.9 0.8 0.7 0.6 :J 'liD .§. 0.5 GI 't:J "§ 0.4 :;, u:: 0.3 0.2 0.1 o 1-- " "-I \/ I • r Sample Date Fluoride in MW-23 \~ ....... ----.... ......... ..-....4 .. - i i i i Sample Date Detected Values: White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Va'lues ~ 'be E Time concentration plots for MW-23 Sulfate in MW-23 3000 r-------------------------------------------------------------~ 2500 r-----------------~~--~~----------~----------------------~ 2000 ~1r--ir\1--------------------------------------------~~~~~! i 1500 -ri hr------------------------- J!! "3 \I) 1000 r---1I----------------------------------------------·-------~ 500 r-----------------------------------------------------------~ Sample Date Uranium in MW-23 90 80 ~ 70 60 ~ -~ 50 E ~ 'c 40 III :s 30 20 ill V~ - 10 0 ..... -~ ...... --,---i i i Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 ~ /~ --- i Detected Values • Non-Detected Values Time concentration plots for MW-24 Chloride in MW-24 80 r---------------------------------------------------------~ 70 ,..--------- 60 T1r-------.-il----------------------------. ~50 t-~~_=-irt----------------------------------~----------~ tiD .§. ~ 40 t-----~tl~--------------~~~----~I-------------~~--~~ "§ :c u 30 t--------4~--------------------------------------------J 20 t------------------.------------------------- 10 r----------------------------------------------------------J Sample Date Fluoride in MW-24 0.4 r --------------------------------------------------------..... 0.35 r --------·----------------------lt---l 0.3 n -----·--jl------------·------------·--,I-...L· ~ 0.25 Ir---Jt-T--------------------------I--~'--1 tiD .§. ~ 0.2 1""'-,----~'rI~~--_jt_--------------I------\-I o :s u:::: 0.15 1-... ------------li1r--\----::::----__ --~~-·--------1I 0.1 1---------=------~~f_ .... ----------1 0.05 ,-----------------------------------1 Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-24 Sulfate in MW-24 3500 r-----------------------------------------------------------~ 3000 -r----------------,----x------------I 2500 ~--~~(j~~~----~~---------------~~--~~~ .. ----~ :J' ~2000 t-----------------------------------J .§. ~ IV 3 1500 t----------------------------------------J V) 1000 t---------------------------------------~ 500 t------------------------------------------J 250 200 ~ 150 ~ E ~ ·c g 100 50 o Sample Date Uranium in MW-24 4 --~ - Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Nan-Detected Values 40 35 30 ~ 25 -tl.O .§. Q.l 20 'tl .~ 0 :E u 15 10 5 0 ~" ~ ..... ~ 0.5 0.45 0.4 0.35 ~ 0.3 -tl.O .§. Q.l 0.25 :E 0 :s 0.2 u::: 0.15 0.1 0.05 0 ~" ~ ..... ~ Time concentration plots for MW-25 Chloride in MW-2S --r--- ~ ~\:)IO ~~ ~ ..... '1> ~IO ~' ~~ Sample Date Fluoride in MW-2S Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Values Time concentration plots for MW-25 Sulfate in MW-2S 1900 r -------------------------------. 1850 i-...... ----t-1k'---... -----------------------I 1800 r-~t1r----t-1r---t1r---------.-------------------------J ::::J ~ 1750 r--t-1r--t---~~-l~-jt---~~---------.I~-----------~ .s ~ .e ~ 1700 r-lt--~~-t-------~--~-iL--ir-~--------JL-l--------------~ 1600 ,-------1t---------------~-----~-------------------~ 1550 \:)" ~f:::Iro ~ ~ \:)q, ;:xf:::IOJ ~:$> ~f:::I ~...,. 'X~ t::.< ,,'1>~ ..: ~ "..:$ ~~ or.; ~ c.,e~ ~..:$ ~'1> ~'lj <::)/l} "..:$ Sample Date Uranium in MW-2S 8 r---------------------------------------------------~ 7 -t------------------' ::::J 5 .----------------------------------------~~--~~---J } § 4 t-------------------------------------------------------~ ·c III ~ 3 -t--------------------------------- 2 r------------------------------------------------------------------~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-26 Chloride in MW-26 90 ~--------------------------------------------------------~ 80 t----------------------------------------------.----------JUU 70 t---------------------------------__ --------~~~---------L~ 30 r-----------------------------------------------------------J 20 t----------------------------------------------------------J 10 r-------------------------------------------------------------J O +-------~----~----_r----_r----~----~-----~~----~--~ Sample Date Fluoride in MW-26 0.9 r----------~t_--------------------------------1 0.8 r--------~~-i_--------------------------------------1 0.7 t-------~------t---------------------------------~-------J ~ 0.6 ,---1"------+------------Q.O .§. ~ 0.5 o IE 0.4 f---------4t------------------..:..---------JUI 0.2 r-----------------------------~------------------------~---~ 0.1 r-------------------------------------------------~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-26 r--------------.-----------------------------------------------------~ Sulfate in MW-26 2500 r-----------------------------------------------------------~ 2000 ~----=--~-.~ ~ 1500 r-----------------------------------------------------------------J lID .§. ~ ~ ~ 1000 r-------------~---------------------------------------------------~ 500 r-----------.------------------------------------------------~ O +---~~--~------~----~----~--~r----~-----~--~ Sample Date Uranium in MW-26 140 120 100 ::i -80 ~ E ::l ·c 60 IV ~ 40 20 Sample Date Detected Valueli White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values 50 45 40 35 ::J 30 "aD .§. CII 25 ~ 0 ~ 20 u 15 10 5 0 I \:)" ~ \.::> 0.9 0.8 0.7 0.6 ::J ...... Il.O .§. 0.5 CII ~ 0 0.4 . ::J u::: 0.3 0.2 0.1 0 \:)" ~ \.::> ~<::>'o ~ \:)'0 ~ ~~ Time concentration plots for MW-27 ~ \~~ Chloride in MW-27 Sample Date Fluoride in MW-27 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Values Time concentration plots for MW-27 Sulfate in MW-27 600 r-------------------------------------------------------------~ 500 r----------------------------------------------------------------J 400 r-.. ~~--~--------~~-----------=------------------------.---J ::i -a:o E i 300 t-----------------------------------------------~-----------------J ~ :i \I) 200 1------------ 100 r-------------------------------------------.------------------~ 0 !:)<.:> t.:f;JO ~ ~ !:)'b ::1\(;)0, t.:-$J ~ t<:"""" ~v ~ ~ t<: ~'>¢O ';~ ~q \'li of,; ~ ~'li ~'li <:.)'li of,; \~ Sample Date Uranium in MW-27 34 33 32 ::i ~ 31 E ::l '2 30 ~ => 29 28 27 !:)<.:> t.:(;)fo !:)fo t<:(;)/I, ~ ~ \~ ~'li <:.)'li of,; Sample Date Detected Values: White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-28 Chloride in MW-28 160 140 120 ~ 100 -QO .§. QI 80 ~ 0 :c u 60 40 20 0 ~" do ~ ~ ~ .... 'b~ .... .;:> ~q Sample Date Fluoride in MW-28 0.8 ,------------------------------ 0.7 ~=---------------------------------------------------~------J 0.6 +----1~~ ~ 0.5 r---------------------------------------------------------------~ QO .§. ~ 0.4 t-----------------------------------------------------------------J o ::l ~ 0.3 t----------------------------------------------------------------J 0.2 t--------------------------------------------------------J 0.1 t--------------------------------------------------------J Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values ~ -tI.O Time concentration plots for MW-28 Sulfate in MW-28 3000 r-------------------------------------------------------------~ 2500 r---~----~~~--~~--------------~------------------------~ 2000 r-------------------------------,------"----------------~--------J E i 1500 t-------------------------------------------------------------~ J!! -; V) 1000 r---------------------------------------------------------------J 500 r----------------------------------------------------------~ Sample Date Uranium in MW-28 6 r-------------------------------------------------~ 5 r------.--------------------------------------~~ 4 t-~~t-1r----~~--------------------------------~ ~ ~ § 3 t-----------~~-------=--~------~---------------=~~~ "2 ~ ::> 2 t---------------------------~--------------------~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-29 Chloride in MW-29 45 40 35 30 ::i' -,g 25 GI 't:I '§ 20 :i: u 15 10 · 5 0 5:)<' 5:)'0 ~ f:f ~'1><: f:f 'i;s \'l> Sample Date Fluoride in MW-29 1.2 r ------------------------------. ..... 0.8 r~~~-r-------l~~~~ ..... --.;e;;;;;;;;;:::::=--7~;;J Qo E. ~ 0.6 t-------.----------------------------------------------------------J o ;:, i!: 0.4 1 ----------------------------.-J 0.2 ,-----------------------------J o +------.------r--~------r------._----~------- Sample Date Detected Value!> White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values 3000 2950 2900 2850 :J -r 2800 ~ ~ 2750 :; \I) 2700 2650 2600 2550 ~<, ~ ...,.;s 60 50 40 :J -bII -= E 30 ::s 'c III :; 20 10 j .r 0 ~<, ~ ...,.;s Time concentration plots for MW-29 ~(::,'o ~ ...,~<:f ~7i ....... ~ .,. I I Sulfate in MW-29 ~ (f 0 Sample Date Uranium in MW-29 ...... .A\, I I Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 ........ - Detected Values • Non-Detected Values Time concentration plots for MW-30 Chloride in MW-30 180 160 140 120 :J" -,g 100 cu " "§ 80 T-------------------------------------------------------------~ ::E u 60 40 20 0 ~<, f:)'o &-,i" ~ f.: '>~~ ,>V ..,.~ ~o Sample Date Fluoride in MW-30 0.6 ,----------------------------- 0.5 r-----.r---------,---------------1 0.4 Mr----r---....::::!!I,------------:#-----------I :J" 'aD .s ~ 0.3 I--------------..... ~--------------------------------J o ~ u::: 0.2 I------~----------------------- 0.1 r--------------------------------------------------------J 0 f:)<' f:)'o &-~ f:)CO o:X~O) f.:""~ (f~ ~..., ~ f.: '>~~ (:f~ ~ ~v '>v ..,.~ 0 ..,.v ~'" ~'" ~Il/ c.,eq \V Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values ~.~ I.n--~-' 1.11:,&& ~~ Time concentration plots for MW-30 Sulfate in MW-30 1200 1000 800 ~ ...... QO .s 600 ~ ~ :; V) 400 200 a ~<, ~'):)fo &> &> ~'b ;:1\(;:)0, ~o$' eJo$' !)."" ~.y, ~ \..::i ~~ \'l)<f (f ~ 0 ~..::i ~'l) ~'t> ()'l' "e~ \..::i Sample Date Uranium in MW-30 12 r---------------------------------------------------------~ 10 t-----------------------~----------------.------~~--~ ...J ~ § 6 ~----------------------~--------------~~--------~ ·2 ~ :::> 4 t---.--------------------------------------------~ 2t---------------------------------------------------J Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-31 Chloride in MW-31 200 180 160 140 ~ 120 Il.D .§. Qj 100 ~ 0 ::c 80 u 60 40 20 0 !;:)'> ~r:::,V:J ~ \V 'fI?-'J Sample Date Fluoride in MW-31 1.4 r ------------------------------ l.2 ,-----.r---------..,...----------------I ::J -~ 0.8 t---------------------------~i-~~--------~--~~~~~~~~~ Qj ~ g 0.6 u::: 0.4 t---------------------------~f------------------------- 0.2 ,----------------------------------------------------1 0 .......--i - !;:)'> !;:)V:J ~ ~ !b o:\r:::,O) ~""r:::, ~ :-,."" ~v ~ ~ ~ ~ ~t;;j \V 'fI?-'J OV (J \~ '!?-V ~~ ~~ <:;>'l/ ",e'J \V Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-31 Sulfate in MW-31 600 r------------------------------------------------------------ 400 r-----------------------------------------------------------~ :::r 'Qo E i 300 r-----------------------------------------------------------------~ ~ :; V) 200 t----------------------------. 100 r-------------------------------------------------------------~ Sample Date Uranium in MW-31 10 r-----------------------------------------------------~ 9 r-----JM~------------.----------------------~--~ 8 r---~--~=-------------------------------~~~-i :::r 6 t----------------------------~----------------~Jl----------J 'Qo -= § s r---------------------------------------------------~ 'c IU ~ 4 t---~---------------------------------------------------J 3 r-----------------------------------------------~ Sample Date ~---------------------------------------------~------------~ White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 Detected Values • Non-Detected Values Time concentration plots for MW-32 Chloride in MW-32 60 50 40 ~ 'Qa .5- CII 30 ~ 0 ::c u 20 10 Sample Date Fluoride in MW-32 0.4 ,-----------------------------. 0.35 r--------------:.------------------J 0.3 ~:-----------,-t\--A-·--....:..-------------I ~ 0.25 'Qa .5-:2 0.2 r--------~~---t~-..!L-\-~~ ..... ~~~. o ::l u:: 0.15 r-------~~r-------------------J 0.1 ,-----------------------------1 0.05 ,------------------------------I Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values Time concentration plots for MW-32 Sulfate in MW-32 3000 r-----------------------------------------------------------~ 2000 t-------------------------------------------~----------------J ~ "Qa E i 1500 ;------------------------------------1 J!! ~ 11'1 1000 t-------------~------------------------------------------------J 500 r---------------------------------------------------------~ Sample Date Uranium in MW-32 7 r-----------------------------------------------~ 6 r-------------~----------------------------------~ 5 t-------------i-,---------------------------------~ ..... ~4 t-------It---Jf--~~------------------------------~ E :::l .~ 3 t--------1-~~--~------~~~----------------------------------~ ~ 2 ~~------------------------------~~~~~~~--~ Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values 80 70 60 ~ 50 -~ C1/ 40 ~ o ::c u 30 20 10 0.45 0.4 0.35 0.3 ~ 'iio ..§. 0.25 C1/ 't:J ':5 0.2 ~ i:i: 0.15 0.1 0.05 o Time concentration plots for MW-35 Chloride in MW-35 \ ----\ /' ..... V 4"'-~ ~ Sample Date Fluoride in MW-35 ~ - i i i Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 ........... i ~ i i Detected Values • Non-Detected Values ~ 'Qa E 3000 2500 2000 \ Time concentration plots for MW-35 Sulfate in MW-35 ---/ \ / V i 1500 J!! '3 \I) ~ -III) ..= E ::J ·c nI ~ 1000 500 Sample Date Uranium in MW-35 30 r------------------------------------------------------- 25 t\~----------------~---------------------~---------=~ 20 15 10 5 Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values 80 70 60 ,.. ::::;-50 tiD .§. Qj 40 "tl .~ I :E u 30 20 10 I o I 0.335 0.33 0.325 ::::;-0.32 tiD .§. Qj 0.315 :2 (; ::l u:: 0.31 0.305 0.3 0.295 ~~~ ~..:> i ~~ c.,e'i Time concentration plots for MW-36 i ~ t? 0 Chloride in MW-36 ~ ~ ~ i I I I Sample Date Fluoride in MW-36 ~~~ ~o Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 ... Detected Values • Non-Detected Va'lues Time concentration plots for MW-36 Sulfate in MW-36 2900 r-----------------------------------------------------------~ 2850 r-------~~~--------------------------------------------------J ::i' 2800 t--,-------3i~----.:..-------------------l tiD .§. ~ ~ ~ 2750 ]r-----------------~~------------------------------J 2700 r--------------------------~~::;;;;~----~~~-------~ 2650 +------.------.------.-----.------.-----~------~----_.----~ ~..."..." ~.;s Sample Date Uranium in MW-36 27 26.5 26 / ::i' 25.5 / / tiD ~ E 25 ::s ·c E ;:) 24.5 24 23.5 / / ,.. / ~ -..... 23 I I ..." ~..." ~.;s Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Values ~ ...... Q.O .§. QI "'C .~ :c u ~ "aD .§. QI :2 0 :::J u:: Time concentration plots for MW-37 Chloride in MW-37 60 50 40 30 20 10 o +-----~----~--~~--~----~----~--.--~----~----~ 0.35 0.3 0.25 "" "-...... 0.2 0.15 0.1 0.05 o Sample Date Fluoride in MW-37 -- ~ Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 ~ Detected Value!' • Non-Detected Va'lues Time concentration plots for MW-37 Sulfate in MW-37 2750 r-----------------------------------------------------------~ 2700 r-----------------------------------------------------------~ 2650 r-----------------------------------------------------------~~ ::J Q:o 2600 r------J~-~~--------------------~t--J .s ~ ~ ~ 2550 r-----~r--------------~~-------------------------J~---J 2500 r-~~----------------------------~~~~------------,t--------j 2450 ~--------------------------------------------------~----------J 2400 +------r------r-----.-r----~r_----,_----~------~----~.------J "" ~"" ~.;s Sample Date Uranium in MW-37 20 18 16 14 ~ ~ ::J 12 Q:o ~ .-.fI ---............ ~ ........ E 10 := 'c IV :; 8 6 4 2 o Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2012 • Non-Detected Va'lues TabJ CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Monday, November 26, 2012 12:54 PM 'rlundberg@utah.gov' 'Phillip Goble'; Thomas Rushing iii; Harold Roberts; David Frydenlund; Jo Ann Tischler; David Turk; N. Tanner Holliday; Garrin Palmer; Jaime Massey Transmittal of CSV Files White Mesa Mill 2012 03 Groundwater Monitoring C12080469.csv; C12080830.csv; C12090804.csv; 1207185.csv; 1208066.csv; C12070448.csv; C12070741.csv; C12080143.csv Attached to this e-mail is an electronic copy of laboratory results for groundwater monitoring conducted at the White Mesa Mill during the third quarter of 2012, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel 1