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HomeMy WebLinkAboutDRC-2013-003161 - 0901a068803be970Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.com VIA EMAIL AND OVERNIGHT DELIVERY September 20, 2013 Mr. Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84116-4850 Re: Inspection Conducted June 13,2013; Notice of Violation: Radioactive Materials License Number UT1900479 Division of Radiation Control ("DRC") Letter Dated August 22, 2013 Dear Mr. Lundberg: This letter responds to the above-referenced DRC letter of August 22, 2013. Energy Fuels Resources (USA) Inc. ("EFRI") received a Notice of Violation ("NOV"), on July 8, 2013, which lists two violations of the Utah Radiation Control Rules, based on an inspection of the White Mesa Mill (the "Mill") conducted by representatives of the Utah Division of Radiation Control ("DRC") on June 13, 2013. EFRI responded by letter on August 6, 2013, requesting that Violation 2, regarding EFRI shipping sewage to an off-site treatment facility without radiological characterization be rescinded. As a result of a telephone conversation with Mr. Phil Goble and Mr. Kevin Carney on August 19, 2013, EFRI withdrew its contention that Violation 2 should be rescinded. This letter responds to DRC's August 22, 2013 letter which required that EFRI provide a response containing the following items for Violation 2: 1) The corrective actions which have been taken and the results achieved; 2) The corrective steps which have been taken to prevent recurrence; and 3) The date full compliance will be achieved. Violation 1 was fully addressed in our letter of August 6, 2013. The root cause of Violation 2 was also addressed in the same letter. The response below summarizes the root cause, and addresses the three remaining items listed above, for Violation 2. Violation 2 10 CFR 20 Appendix B, Radionuclide Table lists the Effluent Concentration Limit, Annual Limit of Intake and Derived Air Concentration for radionuclides. Each radionuclide listed includes three (3) tables: Table 1, Occupational Values; Table 2, Effluent Concentrations (air and water); and Table 3, N:\WMM\Inspections and NOVs\RML Inspections and NOVs\07.08.13 RML Insp ltr NOVA09.20.13 response to 07.02.13 mspctn NOV ltr.doc "DRC-2013-003161" he JF ENEi ENERGYFUELS Received SEP 2013 Division of Waffon Control Letter to Rusty Lundberg September 20, 2013 Page 2 of 4 ) Releases to Sewers. Utah Rule R313-15-1 003, Disposal by Release into Sanitary Sewerage states, in part: "(1) A licensee or registrant may discharge licensed or registered material into sanitary sewerage if each of the following conditions is satisfied: (a) The material is readily soluble, or is readily dispersible biological material, in water; and (b) The quantity of licensed or registered radioactive material that the licensee or registrant releases into the sewer in one month divided by the average monthly volume of water released into the sewer by the licensee or registrant does not exceed the concentration listed in Table HI of Appendix B of 10 CFR 20.1001 to 20.2402,(201 0), which is incorporated by reference" Utah Rule R313-15-501. Surveys and Monitoring - General states, in part: "(I) Each licensee or registrant shall make, or cause to be made, surveys that: (a) Are necessary for the licensee or registrant to comply with Rule R313-15; and (b) Are necessary under the circumstances to evaluate: (i) The magnitude and the extent of radiation levels; and (H) Concentrations or quantities of radioactive material; and (Hi) The potential radiological hazards. " Contrary to the above requirements, the DRC inspector found, based on a records review, that on March 1, 2013, a contractor had entered the Mill's Restricted Area (RA) to pump out the Office Building's Sewage Vault. Although the vault's contents are from the rest rooms located outside of the RA, the vault itself resides inside of the RA. A review of the release form for this event entitled the 'Radiation Survey of Equipment Released for Unrestricted Use' shows that the contents that were removed from the vault and pumped into the contractor's truck were only surveyed for dose rate. The release form contains a comment that reads, "Material was wet, did not take an alpha reading. The inspector agrees that since the material was volumetric in nature, (i.e., liquid, sludge and/or soil-like material), an alpha scan or swipe sample would not be an appropriate survey method. However, this type of material would necessitate bulk sampling and analysis to determine its isotopic concentrations. The truck was released with an external alpha survey and documented on the form entitled 'Daily Vehicle Scan for Vehicles Leaving the Restricted Area'. Although process knowledge would assume that the material inside the truck was radiologically releasable, radioanalysis of the material was not conducted to confirm this prior to it being released from the RAfor unrestricted use. As a follow up, I asked a member of Energy Fuels' staff to contact the contractor to determine where the material was taken. Via email from the Energy Fuels' staff member on June 19, 2013, the DRC was informed that the material was taken, "directly to the sewer lagoons." This would confirm that the material was released to sanitary sewerage which is defined by 10 CFR 20.1003 as, "a system of public sewers for carrying off waste water and refuse, but excluding sewage treatment facilities, septic tanks, v Letter to Rusty Lundberg September 20, 2013 Page 3 of 4 and leachfields owned or operated by the licensee. The violations of Utah Rule R313-15-501, Utah Rule R313-15-1003 and 10 CFR 20 Appendix B identified during the June 13, 2013 inspection have been characterized as Severity Level IV. The base penalty for this Severity Level is $750. Level IV Violations are of more than a minor concern; however, if left uncorrected, could lead to a more serious concern. In this case, the DRC does not believe that radioactive material had been released for unrestricted use. However, the Mill made no effort to verify that the material was suitable for release. If left uncorrected, similar materials that contain significant radioactive concentrations may unknowingly be released to the general public. EFRI Response Root Cause of Noncompliance A review of the circumstances indicates that the event on March 1, 2013 was the first time in the history of the Mill that the main office septic leachfield required pumping out by vacuum truck. Since the off-site shipment is such an untypical activity (that is, has never occurred before), neither the RSO and radiation staff, nor the Mill management were aware that additional requirements beyond release surveys were applicable to the shipment. Corrective Actions Which Have Been Taken and the Results Achieved As discussed with DRC during our phone call on August 19, 2013, EFRI has agreed to perform sampling and radiological analysis of the main office sewage vault. Preparations for sampling of the main office sewage vault are underway. The Mill Environmental Management has reviewed Utah State Health Department regulations to determine what immunizations are required for workers in potential contact with human sewage. The designated sample team is scheduled to begin the series of hepatitis injections beginning the week of September 23, 2013. Sampling is scheduled to begin during or after the first week in October 2013. As discussed with Kevin Carney of DRC on September 16, 2013, samples will be analyzed for the same radionuclides of concern as monitored and reported in the Mill's Semi-Annual Effluent Report, specifically: • Pb-210 • Ra-226 • Th-230 • U-nat Corrective Steps Which Have Been Taken to Prevent Recurrence To prevent a recurrence, EFRI has made the following steps: 1. Language has been added to the Mill's Radiation Protection Manual, Section 2.7, requiring that prior to shipment of any sewage or recyclable fluids off-site from the Mill, samples will be collected and analyzed for radionuclide content, for the same radionuclides of concern as monitored and reported in the Mill's Semi-Annual Effluent Report. The revision to Section 2.7 Letter to Rusty Lundberg September 20, 2013 Page 4 of 4 of the RPM is provided in Attachment 1 to this letter. 2. In addition to sampling of the Main office sewage vault, the Mill has scheduled sampling of the remaining four septic sewage vaults on site. All five septic sewage vaults will be resampled and analyzed periodically to ensure relatively current radionuclide data is available for each vault in the event of a future need to evacuate and ship any sewage vault contents. 3. The Mill Manager, Environmental manager, RSO and radiation technicians have been re- educated regarding the need for radiological characterization (in addition to vehicle surveys) of materials leaving the Mill's restricted area. Date Full Compliance Will Be Achieved. Compliance will be achieved when analytical data is received from the laboratory confirming that the radionuclides of interest are at or below the limits in 10 CFR 20 Appendix B for the four radionuclides of concern listed above for the samples from the Main Office sewage vault. EFRI expects that the data will be available by early to mid-November 2013. A copy of the radiological results will be available at the Mill for DRC review at that time. As mentioned in our letter of August 6, 2013, a copy of the NOV has been posted in the Administration Building, in accordance with R313-18-1 l(l)(d). Please contact me if you have any questions or require any further information. Yours very truly, ENERGY FUELS RESOURCES (USA) INC. Jo Ann Tischler Manager, Compliance and Licensing cc David C. Frydenlund Phil Goble, Utah DRC Dan Hillsten Kevin Carney, Utah DRC • Ronnie Nieves Harold R. Roberts David E. Turk Kathy Weinel Attachments ATTACHMENT 1 I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/133 Revision: EFR 34 Page 1 of 17 2.0 RADIATION MONITORING - AREA 2.1 HIGH VOLUME AIRBORNE AREA AIR SAMPLING Area air sampling involves passing a representative sample of air through a filter paper disc via an air pump for the purpose of determining the concentration of uranium in breathing air at that location. Although the process is only measuring airborne concentrations at a specific place and at a specific time, the results can often be used to represent average concentration in a general area. A high volume sampler or similar high volume pump will be used for this purpose. Samples will be analyzed as per standard gross alpha analysis procedures using a sensitive alpha detector. 2.1.1 Equipment Monitoring equipment will be capable of obtaining an air sample flow rate of 40 1pm or greater for one hour or longer. A variety of equipment may be used for area air sampling, however normally the equipment used is an Eberline RAS-1, Scientific Industries Model H25004, or equivalent. Equipment is calibrated prior to each usage as per Section 3.6 of this manual. 2.1.2 Frequency/Locations Area dust monitoring frequency is monthly for the locations shown in Table 2.1.2-1. Table 2.1.2-1 Airborne Radiation Sample Locations Code BA1 BA2 BA6 BA7 BA8 BA9 BA10 BA11 BA12 BA12A BA12B BA13 BA13A BA14 BA15 Location/Description Ore Scalehouse Ore Storage Sample Plant SAG Mill Area Leach Tank Area Washing Circuit CCD Thickness Solvent Extraction Building/Stripping Section Solvent Extraction Building/Control Room Yellowcake Precipitation & West Storage Area North Yellowcake Dryer Enclosure South Yellowcake Dryer Enclosure Yellowcake Drying & Packaging Area Yellowcake Packaging Enclosure Packaged Yellowcake Storage Room Metallurgical Laboratory Sample Preparation Room I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 2 of 17 Code Location/Description BA16 Lunch Room Area (New Training Room) BA17 Change Room BA18 Administrative Building BA19 Warehouse BA20 Maintenance Shop BA21 Boiler BA22 Vanadium Panel BA22A Vanadium Dryer BA23 Filter Belt/Rotary Dryer BA24 Tails BA25 Central Control Room BA26 Shifter's Office BA27 Operator's Lunch Room BA28 Dump Station BA29 Emergency Generator Station BA30 Truck Shop B A31 Women's Locker Room BA32 Oxidation BA33A AF South Pad BA33B AF North Pad Areas BA-10 and BA-12 are soluble uranium exposure areas. These areas are areas where the uranium compounds that are produced are soluble in lung fluids and are comparatively quickly eliminated from the body. All the other areas are insoluble exposure areas. Insoluble uranium areas are areas where the uranium compounds are not readily soluble in lung fluids and are retained by the body to a higher degree. Temperature of drying operations has a significant impact on solubility of uranium compounds. High drying temperatures produce insoluble uranium compounds. Area uranium dust monitoring, during production periods, is weekly in the designated yellowcake production areas. Monitoring increases to weekly in other monitored areas with the observance of levels exceeding 25% of 10 CFR 20 limits and reverts to monthly upon a continued observance of levels below 25% of 10 CFR 20 limits as determined by the RSO. The RSO may also perform any additional samplings at his or her discretion. The RSO will designate those areas involved in area monitoring during non-production periods. Non-production period monitoring becomes effective one month following the cessation of production. Annually, the licensee shall collect, during mill operations, a set of air samples covering eight hours of sampling, at a high collection flow rate (i.e., greater than or equal to 40 liters per minute), in routinely or frequently occupied areas of the mill. These samples shall be analyzed for gross alpha. In addition, with each change in mill feed material or at N WVMMMnsnections and NQVsXRML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocFVMill SOP Mooter CopyVBook09_Radiation Prot Manual\07 Liccnoo Rcncwal\EFR\Soct2 AppDRPM WMMSOPrev I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 3 of 17 least annually, the licensee shall analyze the mill feed of production product for U-Nat, Ra-226 and PB-210 and use the analysis and results to assess the fundamental constituent composition of air sample particulates. 1. A RAS-1 or similar high volume pump shall be used for area grab sampling. Insure the pump has been recently calibrated within the past month. 2. The locations selected for area air samples should be representative of exposures to employees working in the area. 3. For routine sampling, the sampling period should be for a minimum collection duration of 60 minutes at a flow of 401pm or greater. 4. Insert a clean filter into the filter holder on the sampler. Note start time of pump and record unusual mill operating conditions if they exist. A. Stop sample collection and note time. Normally, an automatic timer is connected to the sampler and a 1 hour sample collection time is used. 6. Remove the filter from the sampler and place in a clean glassine envelope or the package supplied by the manufacturer for delivery to the Radiation Department. 7. Count the sample by gross alpha counting techniques and enter the result and sampling information into the record. 2.1.4 Calculations Perform calculations as specified in Section 4.0. 2.1.5 Records Logs of all samples taken are filed in the Radiation Safety Officer's files. Data is utilized to calculate radiation exposures as specified in Section 4.0. 2.1.6 Quality Assurance Calibration checks on each air sampler are made at least monthly to ensure accurate airflow volumes are being collected. Usage of tweezers and new filter storage containers minimizes contamination potential. Field logging of data during sampling and logging of identifying data on sampled filter containers minimizes sample transposition. Samples N \WMM\Inspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP Master Copy\Book 09_Radiation Prot Monuol\07 License Roncwal\EFR\Sect2 AppD RPM WMMSOP rov 3 doo 2.1.3 Sampling Procedures I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 4 of 17 may periodically be submitted for chemical analysis and a comparison of these results to the radiometric measurements will be made. Review of data by the RSO and by the ALARA audit committee further assure quality maintenance. 2.2.1 Definitions Working Level: A. The exposure to 1.3E + 05 MEV of alpha energy or the potential alpha energy in one liter of standard air containing 100 pCi each of RaA (Polonium-218), RaB (Lead-214), RaC (Bismuth-214), and RaC prime (Polonium-214). (Exposure level, not a dose rate) Kusnetz Method: Method of radon progeny measurement and calculation based upon a 10 liter sample and at least 40 minutes decay time before counting. 2.2.2 Equipment The equipment utilized consists of the following, or appropriate equivalents: • Portable personal sampler • Gelman 25 mm filter holder with end cap, or equivalent • Gelman Type A/E 25 mm diameter glass fiber filters, or equivalent • Counter-Sealer - Eberline MS-3 with SPA-1 probe, or equivalent 2.2.3 Frequency/Location Radon progeny samples are obtained monthly at those locations included for area particulate uranium monitoring during production periods. Monitoring is increased to weekly upon observance of levels exceeding 25% of 10 CFR 20 limits. Monitoring is reduced to monthly upon the continued observance of levels belovy 25% of 10 CFR 20 limits. During non-production periods, monitoring is done monthly for only those locations occupied by personnel where exposures may have the potential of exceeding 25% of 10 CFR 20 limits. The RSO shall so designate those areas to be monitored during non-production periods. 2.2.4 Procedures The procedures to be utilized are as follows: 2.2 RADON PROGENY N \WMM\Inspecfaons and NQVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP Master CopyNBook 09_Radiation Prot Manual\07 License Rcncwal\EFR\Scct2 AppD RPM WMMSOP rev I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 5 of 17 1. Assemble filter trains. 2. Ensure pump batteries are fully charged. 3. Calibrate pump (see Section 3.5). 4. Attached filter trains at sample locations; disconnect end plug. 5. Collect sample in the breathing zone of the employee. 6. Collect sample for five minutes at 4.01pm. 7. Log sample site, time started, time stopped, and filter pump number prior to leaving each site on the field log notebook. 8. Samples are counted between 40 minutes and 90 minutes after collection using sensitive alpha detector. 9. Check the calibration and function check information to ensure the detector is calibrated and operating. 10. If the calibration check correlates, proceed with sample analysis. 11. Radon progeny samples are normally counted for three minutes, however any sample count time may be selected for counting. 12. Run background detector count prior to running sampled filters. 13. After counting, calculate working levels. Equation: (CPM - Bkg) (oceff) (20 liters) (Time Factor) = W.L. Where: CPM - sample count per minute Bkg - counter-detector background count per minute a Efficiency - The efficiency of the counting system (See Section 3.2.3.3) Time Factor - Values determined from Kusnetz method (See attached Table 2.2.4-1) W.L. - Working Levels N \WMM\Inspections and NOVs\RML Inspections and NQVs\07 08 13 RML Insp Itr NOV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP Master CopyNBook 09_Radiation Prot Manual\07 License Renowal\EFR\Soct2 AppD RPM WMMSOPrev White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 6 of 17 TABLE 2.2.4-1 Time Factors Min. Factor Min. Factor 40 150 71 89 41 148 72 87 42 146 73 85 43 144 74 84 44 142 75 83 45 140 76 82 46 138 77 81 47 136 78 78 48 134 79 76 49 132 80 75 50 130 81 74 51 128 82 73 52 126 83 71 53 124 84 69 54 122 85 68 55 120 86 66 56 118 87 65 57 116 88 63 58 114 89 61 59 112 90 60 60 110 61 108 62 106 63 104 64 102 65 100 66 98 67 96 68 94 69 92 70 90 2.2.5 Exposure Calculations The personnel exposure calculations are a job-weighted average of those areas and concentrations that an individual is exposed to. The procedure is: 1. Determine areas and durations (hrs.) each individual worked during the period (month and quarter). N \WMM\Inspections and NQVsVRML Inspections and NQVs\07 08 13 RML Insp ltr NOV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFldocF \Mill SOP Mooter Copy\Book OQ.Radiation Prot Manual\07 License Ronowal\EFR\Scct2 AppD RPM WMMSOP rev White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 7 of 17 2. Determine monitored concentrations (W.L.) for each area so noted. 3. The multiplication of the hours worked in each area by the area concentration (W.L.) noted is added to the result for each area involved in the period. 4. The result is the Working Level Hours exposed (WLH) for the period. 5. The working level hours (WLH) divided by 173 (30 CFR 57.5-40 note); or hours per month gives the working level months (WLM) exposure. (The limit is 4 working level months exposure per year.) 6. If calculated per quarter, the working level hours summed for the quarter are divided by 519 (173 X 3) to obtain the working level quarter exposure. See Section 4.0 for details on how to perform exposure calculations and maintain the exposure records. 2.2.6 Records Data records, which are filed in the Radiation Safety files, include: 1. Sample location 2. Date and time of sample 3. Time on and off of sample pump 4. Counts per minute of sample 5. Elapsed time after sampling 6. Background detector count 7. Appropriate Kusnetz time factor 8. Working level 9. Sampler identification Employee exposure records include: 1. Month monitored 2. Areas and duration worked 3. Employee identification 4. Concentrations (W.L.) observed 5. Calculated WLMs 2.2.7 Quality Assurance N \WMMMnspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 APPD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP Master Copy\Book 09_Radiation Prot Manual\07 License Ronowal\EFR\Soct2 AppD RPM WMMSOP rev White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 8 of 17 Calibration checks each month assure proper calibration of the counting equipment. Documented semi-annual calibrations of the counting equipment using certified alpha calibration and pulse meter sources ensure proper calibration of the equipment over the anticipated ranges. The air sampling system has documented calibration prior to each use, ensuring sampling the appropriate air volumes. Duplicate counts of select data may be counted to assure instrument precision. Field documentation is maintained for each sample during monitoring. This methodology provides assurance in data quality. Review of data by the RSO and the ALARA audit committee further assures quality maintenance. 2.3 ALPHA SURVEYS 2.3.1 Equipment Equipment to be utilized in area alpha surveys is shown in Appendix 1. Pre-use function checks will be performed on all radiation survey equipment as specified in Section 3.1.2.3.2. 2.3.2 Frequency/Locations Fixed and removable alpha surveys are made at those general locations on the Table 2.3.2-1, "Alpha Area Survey Locations." Surveys are completed weekly during production periods. During non-production periods, only those areas designated by the RSO as authorized lunchroom/break areas are monitored. Designated eating areas are listed in Table 2.3.2-2. Table 2.3.2-1 White Mesa Mill Alpha Area Survey Locations Scale House Table Warehouse Office Desks Maintenance Office Desks Change Room Benches Maintenance Lunchroom Tables CCR Tables Metallurgical Laboratory Desks Chemical Laboratory Desks Administrative Break Room Counter Administrative Office Desks N \WMM\Inspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp Itr NOV\Sect2 AppD RPM WMMSQP rev 4 JAT DCRdocF \Mill SOP Mooter CopyvBook 09_Radiation Prot Manuol\07 License Ronowal\EFR\Soot2 AppD RPM WMMSOP rev 3 doo I White Mesa Mill - Standard Operating Procedures Date: 4309/133 Revision: EFR-34 SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Page 9 of 17 Table 2.3.2-2 White Mesa Mill Designated Eating Area Locations Maintenance Supervisor Break Room Main Lunch/Training Room Administrative Break/Conference Rooms Administrative Office Desks 2.3.3 Procedures 2.3.3.1 Respirators Respirators are monitored utilizing a removable alpha smear that is read using alpha scaler meter such as a Ludlum Model 2200 or other equivalent radiological instruments. Readings exceeding 100 dpm/100 cm2 result in re-cleaning or discarding of the respirator. Respirator cleaning and monitoring is a function of the Radiation Safety staff assigned to this duty. The meter's performance is checked prior to each use period. 2.3.3.2 Fixed Alpha Surveys Alpha surveys for fixed alpha contamination are performed using a variety of alpha detecting instruments, as listed in Appendix 1. Each instrument is checked using a calibrated alpha source for proper function and operation prior to use, as described in Section 3.1.2.3.2. Adjustments to the surface area being measured must be made to convert from the particular detector's surface area to the commonly used surface area of 100 square centimeters. Therefore when converting a measurement to the commonly used unit of dpm/100cm2, a multiplying area factor must be applied to the measurement. For the Ludlum instrument with a 43-1 detector of 75 cm2 surface, multiply the value by 1.33 (i.e. 100cm2 divided by 75cm2). The procedures are: 1. Turn the meter on and check the meter battery condition. 2. Check alpha detector mylar surface for pinholes, etc. Replace if necessary and repeat calibration. 3. As specified in Section 3.1.2.3.2, perform a function calibration check using calibrated alpha source. N \WMMMnspections and NQVsVRML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP Master CopyvBook 09_Radmtion Prot Monual\07 Liconoo Roncwal\EFR\Scct2 AppD RPM WMMSOP rev I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 10 of 17 4. If check is acceptable, proceed with monitoring. 5. At each designated site, monitor designated surfaces, table tops, etc., holding within lA inch of the surface. 6. Record data, location, cpm/cm2 monitored on data sheet. 7. At the conclusion of the survey, transpose results to the file log, correcting to dpm/100 cm2, using correction for detector's surface area and cpm/dpm conversion factor. 2.3.3.3 Removable Alpha Surveys The Ludlum Model 2200 scaler with 43-17 detector, or a variety of other sensitive alpha detection instruments such as Model 2929 or equivalent, counts wipe samples collected during removable alpha surveys. Glass fiber filters, sized to fit the detector sample slot, are utilized as the wipe medium. A template having a 100 square centimeter surface area maybe used to standardize the surface area wiped. The procedure is: 1. Perform function check calibration of the sealer/detector. Ensure that this measurement is within ± 10% of the value obtained from the calibration laboratory. 2. If so proceed with the survey and counting. 3. Obtain clean filters and clean envelopes for filter storage. 4. At a location to be surveyed, remove the filter from the envelope and wipe the surface covering approximately 100 cm2. This is easily accomplished by making a "S" shaped smear for approximately 10 inches using normal swipes (approximately 2.5 cm diameter). 5. Record on envelope the date and location of the sample. 6. Upon returning to counting lab, place an unused filter in the counting unit for at least 1 minute and obtain a background count rate. 7. Repeat procedure for each used filter, extracting filter from envelope, immediately prior to counting, using tweezers and placing in the detector slot with the wiped surface facing the detector, and count for at least 1 minute. N \WMM\Inspections and NOVs\RML Inspections and NQVs\07 08 13 RML Insp Itr NOV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP Master CopyNBoolc 09_Radiation prot Manual\07 Lioonoo Rcnewal\EFR\Soct2 AppD RPM WMMSOP rev I White Mesa Mill - Standard Operating Procedures Date: 4309/123 Revision: EFR-34 SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Page 11 of 17 8. Convert results from cpm/filter to dpm/filter (100 cm2 wiped) after subtracting the blank background count. 9. Record on the alpha survey form the following information: A. Sample location and conditions B. Sample date C. Sampler identification D. Wipe count dpm/100 cm2 10. Discard the filters and envelopes 2.3.4 Action Limits 2.3.4.1 Respirators Levels greater than 100 dpm/100 cm2 squared require re-cleaning or discarding of a respirator. 2.3.4.2 Fixed Alpha Surveys Levels greater than 1,000 dpm/100 cm2 squared require remedial action by management. ALARA criterion ensures that the RSO takes action where necessary to maintain levels as low as reasonably achievable. 2.3.4.3 2.3.4.3 Removable Alpha Surveys Levels greater than 1,000 dpm/100 cm2 squared require remedial action and decontamination. ALARA criteria ensures that the RSO takes action where necessary to maintain levels as low as reasonably achievable. 2.3.5 Records Records of fixed and removable alpha surveys are maintained in the Radiation Safety office files. Records include: 1. Sample location/conditions 2. Sample date 3. Sampler identification 4. Fixed alpha determination - dpm/100 cm 5. Removable alpha determination - dpm/100 cm2 6. Remedial action taken, where necessary N \WMM\Inspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NOV\Sect2 APPD RPM WMMSQP rev 4 JAT DCFdocF \Mill SOP Master CopyVBook 09_Radiation Prot ManuoJ\07 Liconoo Ronowai\EFR\Soct2 AppD RPM WMMSOP rev 3 doo White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 12 of 17 2.3.6 Quality Assurance Calibration function checks of detector performance and visual observation of detector surfaces prior to each survey ensures counting reliability and consistency. Usage of clean containers and tweezers minimizes contamination of wipe samples. Field logs of sample LD.'s on sample containers minimizes transposition of samples. Data review by the RSO and by the Audit Committee further assures quality maintenance. Beta/Gamma surveying instruments used for beta-gamma surveys are listed in Appendix 1 and the sources used are listed in Appendix 2. Some instruments read directly in mrem/hour while others read in cpm (with a conversion to mrem/hour). The model 44-6 detector has a removable beta shield allowing discrimination between beta and gamma contributions. Each instrument has a manufactures user's manual which describes the function, use and capability of each instrument. These manuals must be understood before surveying proceeds. Calibration of Beta/Gamma and functional checks are performed using calibrated Cs-137 or Sr-Y 90 sources 2.4.2 Frequency/Locations The sites noted on Table 2.4.2-1 are monitored on a monthly basis by of the Radiation Safety staff during production periods. During non-production periods, only areas routinely occupied by personnel are monitored as designated by the RSO. 2.4 BETA-GAMMA SURVEYS 2.4.1 Equipment Table 2.4.2-1 Beta-gamma Survey Locations Description of Possible Identification Number Source of Area of Exposure Mill Feed Hopper & Transfer Chute SAG Mill Intake-Feed Chute Screens-Area Floor Between Screen Leach Operator's Desk Leach Tank Vent #3 Leach Tank #3-Wall CCD Thickeners Pumphouse Tailings Discharge Oxidant Makeup Room-Sump Pump Shift Foreman's Office-Work Desk Distance from Source in cm WM-1 WM-2 WM-3 WM-4 WM-5 WM-6 WM-7 WM-8 WM-9 WM-10 N \WMM\Inspections and NQVsNRML Inspections and NQVs\07 08 13 RML Insp ltr NOV\Sect2 AppD RPM WMMSQP rev 4 JAT DCFdocF\Mill SOP MooterCopy\Book09_Radiation Prot Manual\07 License Rcncwal\EFR\Scct2 AppD RPM WMMSOP rev 3 doc White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/133 Revision: EFR-34 Page 13 of 17 Description of Possible Identification Number Source of Area of Exposure Distance from Source in cm WM-11 SX Operator's Area 1 WM-12 Precipitation Tanks #1 Tank; Wall 1 WM-13 Precipitation Section "Lab Bench" 1 WM-14 Precipitation Vent 1 WM-15 Yellowcake Thickener #1; Wall 1 WM-16 Centrifuge Discharge-Chute Wall 1 WM-17 Yellowcake Thickener #2; Wall 1 WM-18 Yellowcake Packaging Room 1 WM-19 Yellowcake Dryer 1 WM-20 Yellowcake Dust Collector 1 WM-21 SX Uranium Mixer # 1 Extractor 1 WM-22 SX Uranium Mixer #1 Stripping 1 WM-23 SX Vanadium Mixer #1 Stripping 1 WM-24 Vanadium Dryer 1 WM-25 Mill Laboratory Fume Hood 1 WM-26 Chemical Laboratory Work Area 1 WM-27 Metallurgical Laboratory Work Area 1 WM-28 Lunchroom Eating Area 1 WM-29 Lunchroom Wash Area 1 WM-30 Maintenance Shop - Work Area 1 WM-31 Maintenance Shop - Rubber Coating 1 WM-32 Tailings Impoundment Discharge 1 WM-33 Tailings Impoundment Dike 1 1 WM-34 Tailings Impoundment Dike 2 1 WM-35 Tailings Impoundment Dike 3 1 WM-36 Scalehouse 1 WM-37 Tailings Impoundment Dike 4 1 2.4.3 Procedures The monitoring procedures are: 1. Check meter battery condition. 2. Check detector using a check source. 3. If the calibration function check indicates that the instrument is operating within calibration specifications, proceed with monitoring. 4. Survey each designated location on Table 2.4.2-1 and record in the field log: A. Site location/condition B. Date C. Instrument used N \WMM\Inspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp Itr NQV\Sect2 AppD RPM WMMSOP rev 4 JAT DCFdocFVMiU SOP Master Copy\Boolc 09_Radiation Prot Manual\07 License Ronowal\EFR\Soct2 AppD RPM WMMSOP rev J White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/133 Revision: EFR-34 Page 14 of 17 D. Sampler's initials E. Meter reading (beta + gamma) F. Meter reading (gamma) 5. Upon returning to the office, record the mr/hr reading into a permanent file which is maintained for beta-gamma exposure evaluation. 2.4.4 Action Levels The ALARA concept is utilized in action levels. Responses include operative cleaning of the area or isolation of the source. The Radiation Safety Department will ensure levels ALARA. 2.4.5 Records Records maintained in the Radiation Safety office files include: 1. Date monitored 2. Site location/condition 3. Instrument used 4. Sampler's initials 5. Beta/Gamma level, mr/hr 6. Remedial action taken, if necessary 2.4.6 Quality Assurance Quality of data is maintained with routine calibration and individual function checks of meter performance. Personnel utilizing equipment are trained in its usage. Records of the operational checks and calibrations are maintained in the files. The RSO routinely reviews the data and the ALARA audit committee periodically analyzes the performance of the management of the monitoring and administrative programs. 2.5 EXTERNAL GAMMA MONITORING External gamma area monitoring is conducted at various locations around the Mill site in order to provide Radiation Safety Staff with area-specific gamma measurements. The procedures applicable to such monitoring are set out in Section 4.3 of the Mill's Environmental Protection Manual. N \WMMMnspections and NQVsVRML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSOP rev 4 JAT DCFdocFAMill SOP Master Copy\Book 09_Radiation Prot Manual\07 License Rcnewal\EFR\Scct2 AppD RPM WMMSOP rev I White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 15 of 17 2.6 EQUIPMENT RELEASE SURVEYS 2.6.1 Policy Materials leaving a Restricted Area going to unrestricted areas for usage must meet requirements of NRC guidance for "Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use" (dated May 1987). All material originating within the restricted area will be considered contaminated until checked by the Radiation Safety Department. All managers who desire to ship or release material from the facility will inform the RSO of their desires. The RSO has the authority to deny release of materials exceeding NRC guidance for "Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use" (dated May, 1987). No equipment or materials will be released without documented release by the RSO or his designee. 2.6.2 Limits The release limits for unrestricted use of equipment and materials is contained in the NRC guidance listed above in Section 2.6.1 and are summarized as follows: Limits for Alpha emissions for U-Nat and its daughter products are: Average 5,000 dpm/100 cm2 Maximum 15,000 dpm/100 cm2 Removable 1,000 dpm/100 cm2 Limits for Beta-gamma emissions (measured at a distance of one centimeter) for Beta/Gamma emitting radioisotopes are: Average 0.2 mr/hr or 5,000 dpm/100 cm2 Maximum 1.0 mr/hr or 15,000 dpm/100 cm2 2.6.3 Equipment Radiological survey instruments are listed in Appendix 1. 2.6.4 Procedures Upon notification that materials are requested for release, the Radiation Safety Department shall inspect and survey the material. Surveys include fixed and removable alpha surveys and beta-gamma surveys. An equipment inspection and release form is to be prepared and signed by the RSO or his designee. Any material released from the mill N \WMM\Inspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSOP rev 4 JAT DCFdocF\Mill SOP Master CopyVBook 09_Radiation Prot Manual\07 Liconso Ronowal\EFR\Soot2 AppD RPM WMMSOP rev 3 doc White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 16 of 17 will be accompanied with the appropriate release form. If contamination exceeds levels found in NRC guidance "Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use", dated May, 1987, then decontamination must proceed at the direction of the RSO. If the material cannot be decontaminated, then it will not be released. 2.6.5 Records Documented records for each released item are filed in the Radiation Safety Department files. 2.6.6 Quality Assurance The RSO and the ALARA Audit Committee periodically review the policy and documented release forms to ensure policy and regulatory compliance. 2.7 PRODUCT SHIPMENT SURVEYS 2.7.1 Policy The Radiation Safety Department, prior to shipment release, will survey product shipments from the facility. Product shipments include uranium concentrate and solid vanadium products. The Radiation Safety Department is to be notified in advance of each shipment. The shipment will not be released prior to the Radiation Safety Department's authorization. 2.7.2 Equipment Equipment used for product shipment surveys is the same as equipment used for material release surveys and is listed in Appendices 1 and 2. 2.7.3 Frequency All barrels are fixed alpha and gamma scanned prior to shipment. A minimum of 25 percent of the barrels consigned are also wipe tested. 2.7.4 Solid Vanadium Shipments The procedure to be followed for solid vanadium shipments were detailed in the Radiation Safety Manual in Section 2.7.4. These procedures have been replaced with procedures No.: PBL-15 Book 10, "Release and Shipping of Vanadium Blackflake". N \WMMMnspections and NQVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSOP rev 4 JAT DCFdocF\Mill SOP Mooter CopyVBook 09_Radmtion Prot Manual\07 License Ronowal\EFR\Soct2 AppD RPM WMMSOP rev 3 doc f* White Mesa Mill - Standard Operating Procedures Date: 4309/123 Revision: EFR-34 SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Page 17 of 17 2.7.5 Uranium Concentrate Shipments The procedures for exclusive use uranium concentrate shipments are: 1. Inspect each product barrel that makes up the consigned shipment for leaks, holes in the barrels, cleanliness, etc. 2. Barrels requiring repair shall be repaired prior to the radiation survey. 3. Perform a total and removable alpha survey of each barrel, using the procedures and equipment specified in Section 6.0. The release limits for total and removable alpha radiation contamination is an average of 5,000 dpm/100 cm2 and a maximum of 15,000 dpm/100 cm2. Any barrel that exceeds 1,000 dpm/100 cm2 total alpha radiation contamination requires a removable alpha smear/wipe test to be performed. Perform a removable alpha survey of each barrel exceeding 1,000 dpm/100 cm2 total alpha contamination. The release limit for removable alpha radiation contamination is 1,000 dpm/100 cm2. Perform a smear/wipe test and analyze filters for removable alpha on 25% of the barrels at a minimum, and perform a smear/wipe test and analyze the filters for removable alpha on any barrels that exceed 1,000 dpm/100 cm2 total alpha contamination. 2.7.6 Records The attached form servos as a record of shipment and is retained in the Radiation Safety files. 2.7.7 Quality Assurance Periodic reviews of transport forms and policies by the RSO and the ALARA Audit Committee ensures quality assurance for product shipment surveys. 2.7.6$ Miscellaneous Releases The Radiation Safety Department will monitor, prior to leaving the Restricted Area, any material that will shipped off siter not permit any sewage or recyclable fluids to leave the Restricted Area unless (a) a characterization sample of the sewage or fluid, which is analyzed for Ra-226. Pb-210. U-nat, and Th-230. is taken or is on file at the Mill: and (b) based on the results of the sample, the release is in compliance with the requirements of R313-15-1003 and R313-15-302(2)(fr)(T,. as applicable. A copy of the results of each characterization sample will be maintained on file at the Mill. This includes, but not limited to. sewage and oil. Along with radiological survey information, these materials N \WMMMnspections and NQVsNRML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSOP rev 4 JAT DCFdocFVMill SOP Master CopyxBoolc 09_Radiation Prot Manual\07 License Rcnowal\EFR\Scct2 AppD RPM WMMSOP rov White Mesa Mill - Standard Operating Procedures SOP PBL-RP-2 Book: Radiation Safety Manual, Section 2 Date: 4309/123 Revision: EFR-34 Page 18 of 17 will also havo laboratory analysis performed for a sot list of radioisotopes as specified by Corporate Management and a copy of thoso results maintained on filer 2.7.7 Records The attached form serves as a record of shipment and is retained in the Radiation Safety files. 2.7.8 Quality Assurance Periodic reviews of transport forms and policies by the RSO and the ALARA Audit Committee ensures quality assurance for product shipment surveys. N \WMM\Inspections and NOVs\RML Inspections and NQVs\07 08 13 RML Insp ltr NQV\Sect2 AppD RPM WMMSOP rev 4 JAT DCFdocF VMill SOP Master CopyVBook 09_Radiation Prot Manual\07 Lioonao Rcncwal\EFR\Scct2 AppD RPM WMMSOP rev