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HomeMy WebLinkAboutDRC-2011-005790 - 0901a06880231e3aDENISO MINES Sent VIA Federal Express May 17, 2011 Mr. Rusty Lundberg | Co-Executive Secretary | Utah Water Quality Board Utah Department of Environmerital Quality 1^5 North 1950 West P.O, Box 144820 Salt Lake City, UT 84114-4820 Oo579Q Denison Mines (USA) Corp. 105017th Street, Suite 950 Denver, ^00 60265 USA Tel: 303 628-7798 Fax: 303 389^125 www.denisonmines.com Re: Re: Transmittal of 1st Quarter 2011 Nitrate Mo UDEQ Docket No. UGy-09--03-WW Dear Mr. Lundberg: I ! •'•••• Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 1st Quarter of 2011 as required by the January 2009 Stipulated Consent Agreement, UDEQ Docket No, UGW-09-03, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours. DENlgtoN JpiNES (USA) CORP. 4)/l^o AmTischkr Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel Central Files OENISOJ)~~ MINES Sent VIA Federal Express May 17,2011 Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Re: Re: Transmittal of lst Quarter 2011 Nitrate Monitoring Report UDEQ Docket No. UGW-09-03-White Mesa Uranium Mill Dear Mr. Lundberg: Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303628·7798 Fax: 3033894125 www.denisonmines.com Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 1st Quarter of2011 as required by the January 2009 Stipulated Consent Agreement, UDEQ Docket No. UGW-09-03, as well as two CDs each containing a word searchable electronic copy ofthe report. If you should have any questions regarding this report please contact me. t: D . ON iNEs (USA) CORP. 'fMo Ann Tischler Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel Central Files White Mesa Uranium Mill Nitrate Monitoring Report State of Utah Stipulated Consent Agreement, January 2009 Docket No. UGW09-03 lst Quarter (January through March) 2011 Prepared by: Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver CO 80265 May 17,2011 TABLE OF CONTENTS 1.0 INTRODUCTION .................................................................................................. 1 2.0 GROUNDWATER NITRATE MONITORING ................................................ 1 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 Nitrate Monitoring ...................................................................................... 2 2.1.2 Parameters Analyzed .................................................................................. 2 2.1.3 Groundwater Head and Level Monitoring .................................................. 2 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 3 2.2.1 Well Purging and Depth to Groundwater ................................................... 3 2.2.2 Sample Collection ....................................................................................... 4 2.3 Field Data ............................................................................................................ 5 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 5 2.5 Laboratory Results .............................................................................................. 6 2.5.1 Copy of Laboratory Results ........................................................................ 6 2.5.2 Regulatory Framework ............................................................................... 6 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 6 3.1 Field QC Samples ............................................................................................... 7 3.2 Adherence to Mill Sampling SOPs ..................................................................... 7 3.3 Analyte Completeness Review ........................................................................... 7 3.4 Data Validation ................................................................................................... 7 3.4.1 Field Data QAlQC Evaluation .................................................................... 8 3.4.2 Holding Time Evaluation ............................................................................ 9 3.4.3 Receipt Temperature Evaluation ................................................................. 9 3.4.4 Analytical Method Checklist ...................................................................... 9 3.4.5 Reporting Limit Evaluation ........................................................................ 9 3.4.6 QAlQC Evaluation for Sample Duplicates ............................................... 10 3.4.7 Rinsate Check ........................................................................................... 10 3.4.8 Other Laboratory QAlQC ......................................................................... 11 4.0 INTERPRETATION OF DATA ....................................................................... 11 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 11 4.1.1 Current Site Groundwater Contour Map ................................................... 11 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter ........................................................... 11 4.1.3 Hydrographs .............................................................................................. 12 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 12 4.2 Review of Analytical Results ............................................................................ 12 4.2.1 Current Nitrate and Chloride Isoconcentration Maps ............................... 12 4.2.2 Nitrate and Chloride Concentration Trend Data and Graphs .................... 12 4.2.3 Interpretation of Analytical Data .............................................................. 12 5.0 5.1 5.2 5.3 5.4 5.5 CORRECTIVE ACTION REPORT ................................................................. 13 Identification and definition of the problem ..................................................... 13 Assignment of Responsibility for Investigation ofthe Problem ....................... 13 Investigation and Determination of Cause of the Problem ............................... 13 Determination of a Corrective Action to Eliminate the Problem ..................... 14 Assigning and Accepting Responsibility for Implementing the Corrective Action ............................................................................................................... 14 5.6 5.7 5.8 6.0 7.0 8.0 Implementing the Correcti ve Action and Evaluating Effectiveness ................. 14 Verifying That the Corrective Action Has Eliminated the Problem ................. 14 Assessment of Previous Quarter's Corrective Actions ..................................... 14 CONCLUSIONS AND RECOMMENDATIONS ............................................ 15 ELECTRONIC DATA FILES AND FORMAT .............................................. IS SIGNATURE AND CERTIFICATION ........................................................... 16 11 LIST OF TABLES Table 1 Summary of Well Sampling and Constituents for the Period Table 2 Nitrate Percent Difference Table 3 Chloride Percent Difference INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-l Field Data QAlQC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QAlQC Evaluation for Sample Duplicates H-6 QC Control limits for Analysis and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Nitrate and Chloride Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Nitrate and Chloride Concentration Trend Graphs Tab L CSV Transmittal Letter iii 1.0 INTRODUCTION The Utah Department of Environmental Quality ("UDEQ") Division of Radiation Control ("DRC") noted in a Request dated September 30, 2008 (the "Request"), for a Voluntary Plan and Schedule to Investigate and Remediate Nitrate Contamination at the White Mesa Uranium Mill (the "Mill") (the "Plan"), that nitrate levels have exceeded the State water quality standard of 10 mglL in certain monitoring wells. As a result of the Request, Denison Mines (USA) Corp. ("DUSA") entered into a Stipulated Consent Agreement (the "Consent Agreement") with the Utah Water Quality Board in January 2009 which directed the preparation of a Nitrate Contamination Investigation Report ("CIR") and Quarterly Nitrate Monitoring Reports. A subsequent letter dated December 1, 2009, among other things, recommended that DUSA also address elevated chloride concentration in the Nitrate Monitoring Reports. The CIR was submitted to the Co-Executive Secretary of the Utah Water Quality Board (the "Co-Executive Secretary") on December 30, 2009. By a letter dated October 5, 2010, the Co-Executive Secretary notified DUSA of his determination that the CIR is incomplete. As a result of that letter, additional negotiations with UDEQ have been completed, and DUSA agreed to submit to the Co-Executive Secretary for approval a plan and schedule to perform further investigations in order to remedy deficiencies. DUSA and UDEQ entered into a tolling agreement on November 30, 2011, revised on April 28, 2011, to allow time to perform a multi-phased field investigation, evaluate a number of potential Mill-related and non-Mill sources, and to revise and update the CIR. The revised plan for Phase 1 of the field investigation was submitted to UDEQ on May 13, 2011. A Plan and Schedule for the remainder of the program will be submitted to UDEQ on June 3, 2011. This is the Quarterly Nitrate Monitoring Report, as required under the Consent Agreement, State of UDEQ Docket No. UGW-09-03 for the first Quarter of 2011 (the "Quarter"). 2.0 GROUNDWATER NITRATE MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Nitrate samples and measurements taken during this reporting period (January through March 2011), are discussed in the remainder of this section. 1 N:IRequired ReportslNitrate Quarterly Monitoring Report12011 QI12011 QI Nitrate Report text.doc 2.1.1 Nitrate Monitoring Quarterly sampling for nitrate monitoring parameters was perfonned in the following wells: TWN-1 TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 TWN-14 TWN-15 Piezometer 2 TWN -16 Piezometer 3 TWN-17 TWN-18 TWN-19 Upper Wildlife Pond ("UWLP") Piezometer 1 Table 1 provides an overview of all locations sampled during the current period, along with the date samples were collected from each location, and the date(s) upon which analytical data were received from the contract laboratory. Table 1 also identifies rinsate samples collected, as well as sample numbers associated with any required duplicates. As indicated in Table 1, nitrate monitoring was perfonned in all of the nitrate monitoring wells, the UWLP, and Piezometers 1, 2, and 3. Analytical data for all of the nitrate wells, piezometers and the UWLP are included in Tab G. Nitrate and chloride are also monitored in all of the Mill's groundwater monitoring wells and chlorofonn investigation wells. Data from those wells for the Quarter are incorporated in certain maps and figures in this report but are discussed in their respective programmatic reports. 2.1.2 Parameters Analyzed Locations sampled during this reporting period were analyzed for the following constituents: • Inorganic Chloride • Nitrate plus Nitrite as Nitrogen (referred to herein as nitrate) Use of analytical methods consistent with the requirements of the White Mesa Uranium Mill Groundwater Quality Assurance Plan, Revision 6, March 22, 2010 (the "QAP") was confinned for all analytes, as discussed later in this report. 2.1.3 Groundwater Head and Level Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the Groundwater Discharge Pennit (the "GWDP") (June 17, 2010 and as revised February 15, 2011): 2 N:IRequired ReportslNitrale Quarterly Monitoring Report12011 QII2011 QI Nitrate Report text doc • The quarterly groundwater compliance monitoring wells. • Existing well MW-4 and all of the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3, P-4 and P-5. • MW-20 and MW-22 • Nitrate monitoring wells. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. 2.2 Sampling Methodology and Equipment and Decontamination Procedures The QAP provides a detailed presentation of procedures utilized for groundwater sampling activities under the GWDP (June 17,2010 and as revised February 15, 2011). The sampling methodology, equipment and decontamination procedures that were performed for the nitrate contaminant investigation, as summarized below, are consistent with the QAP. 2.2.1 Well Purging and Depth to Groundwater A list of the wells in order of increasing nitrate contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all ofthe non-detect wells and then move to the more contaminated wells in order of nitrate contamination, starting with the wells having the lowest nitrate contamination. Before leaving the Mill office, the pump and hose are decontaminated using the cleaning agents described in Section 6.2.5 of the QAP. A rinsate blank is collected after the first pump decontamination of each day as described below. Mill personnel then proceed to the first well which is the well with the lowest concentration of nitrate based on the previous quarter's sampling results. Well depth measurements are taken and the two casing volumes are calculated (measurements are made using the same instrument used for the monitoring wells under the Mill's GWDP). The Grundfos pump (a 6 to 10 gallon per minute [gpm] pump) is then lowered to the bottom of the well and purging is begun. At the first well, the purge rate is established for the purging event by using a calibrated 5 gallon bucket. After the evacuation of the well has been completed, the well is sampled when possible, and the pump is removed from the well and the process is repeated at each well location moving from the least contaminated to most contaminated well. If sample collection is not possible due to the well being purged dry a sample is collected after recovery as described below. All wells are capped and secured prior to leaving the sampling location. 3 N:lRequired ReportslNitrate Quarterly Monitoring Rq,ort\2011 QI\2011 Ql Nitrate Report text.doc Decontamination of non-dedicated equipment, using the reagents in Section 6.2.5 of the QAP, is performed between each sample location, and at the beginning of each sampling day, in addition to the pre-event decontamination described above. 2.2.2 Sample Collection Wells Following the purging of a nitrate investigation well, the sampling takes place once stabilization has been achieved in accordance with Section 6.2.7 of the QAP. Prior to leaving the Mill office to sample, a cooler along with ice is prepared. A trip blank is not required as the sampling event does not include analyses for Volatile Organic Compounds ("VOCs"). Once Mill Personnel arrive at the well sites, labels are filled out for the various samples to be collected. All personnel involved with the collection of water and samples are then outfitted with rubber gloves to avoid sample contamination. Each sample collection event begins at the location least affected by nitrate (based on the previous quarter's sampling event) and proceeds by affected concentration to the most affected location. The dedicated portable pump is appropriately decontaminated prior to each sampling event, each sampling day, and between well samples. It is important to note that the rinsate blank sample frequency was modified during the fourth quarter 2010 as recommended by UDEQ personnel present on site for split sampling during the chloroform sampling program. Previously, a rinsate blank sample was collected after each decontamination of the nondedicated pump and prior to the next use of the pump. Per an e-mail from Mr. Phil Goble, dated, November 15, 2010, the decreased rinsate blank frequency implemented during the chloroform sampling program was acceptable for implementation on the nitrate sampling program. Based on the revised procedure, rinsate blank samples are only required at the beginning of the sampling event and at the beginning of each day of sampling. The frequency change was implemented during fourth quarter 2010. Samples are taken from the portable pump after stabilization has been achieved, unless the well is pumped dry. If the well is pumped dry, Mill personnel use a disposable bailer to sample the well after it has recovered in accordance with Section 6.2.7 of the QAP. The bailer is attached to a reel of approximately 150 feet of nylon rope and then lowered into the well. After coming into contact with the water, the bailer is allowed to sink into the water in order to fill. Once full, the bailer is reeled up out of the well. Sample bottles are filled as follows; • First, a 250 ml sample is collected for nitrate/nitrite. This sample is not filtered, but is preserved with H2S04. • Second, a 500 ml sample is collected for chloride. This sample is not filtered and is not chemically preserved. 4 N:IRequired ReportslNitrate Quarterly Monitoring Rcport12011 Ql12011 QI Nitrate Report text.doc After the samples have been collected for a particular well, the samples are placed into the cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. If a bailer has been used it is disposed of. Ponds Grab samples are taken from the UWLP using a disposable bailer. Sample bottles are filled in the same manner as for wells, as stated above. After the samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, Energy Laboratories ("EL"). Piezometers Samples are collected from Piezometers 1, 2 and 3, if possible. Samples are collected from piezometers using a disposable bailer following the procedures described for wells that have been pumped dry, above. However, due to the difficulty in obtaining samples from the piezometers, the purging protocols set out in the QAP are not followed. After samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, EL. 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the nitrate contaminant investigation monitoring wells, piezometers, and UWLP identified in Section 2.1.1 above, and Table 1. It is important to note that the field data sheet appearance was changed in the fourth quarter 2010 as a result of the implementation of an electronic data capture system. The field data sheets contain the same information as the approved field data sheet attached to the approved QAP in approximately the same location. The new data sheets allow the electronic capture of data while still maintaining the real-time recording of information manually in ink as required by UDEQ. The changes were made to accommodate the data recording and validation system. 2.4 Depth to Groundwater Data and Water Table Contour Map Depth-to-groundwater measurements which were utilized for groundwater contours are included on the Quarterly Depth to Water Sheet at Tab C of this Report along with the kriged groundwater contour map for the current quarter generated from this data. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each as indicated by the measurement dates in the summary sheet under Tab C. A copy of the kriged groundwater contour map generated from the previous quarter of2010 data is provided under Tab D. 5 N:\RcqtLired Report.INitrate Quarterly Monitoring Report120 II Q 1120 11 Q I Nitrate Report texLdoc 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results All analytical results were provided by EL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well or other sample. Results from analysis of samples collected for the first Quarter nitrate investigation are provided under Tab G of this Report. Also included under Tab G are the results of analyses for duplicate samples and rinsate samples for this sampling effort, as identified in Table 1. See the Groundwater Monitoring Report and Chloroform Monitoring Report for the first Quarter of 2011 for nitrate and chloroform analytical results for the groundwater monitoring wells and chloroform investigation wells not listed in Table 1. 2.5.2 Regulatory Framework As discussed in Section 1.0 above, the Request, Plan, and Agreements each triggered a series of actions on DUSA's part. Potential surficial sources of nitrate and chloride have been described in the December 30, 2009 Contamination Investigation Report and additional investigations into potential sources are planned for 2011. This quarterly report documents the continued monitoring consistent with the program described in the initial Nitrate Contamination Investigation Report submitted in 2009. The monitoring program and reporting requirements set forth in the 2009 Contamination Investigation report will remain in effect until further notice and completion of the additional studies described in the plan submitted May 6, 2011 are complete and subsequent negotiations with UDEQ are complete. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager performed a QAlQC review to confirm compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check field data QA/QC, holding times, receipt temperature and laboratory data QAlQC are discussed in Sections 304.1 through 3.4.7 below. The analytical laboratory has provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The Analytical Laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab G. Results of review of the laboratory QAlQC information are provided under Tab H and discussed in Section 304, below. 6 N:lRequired Report.INit",te Quarterly Monitoring Report\20 II Q 1\20 II QI Nitrate Report text.doc 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the nitrate investigation program consist of one field duplicate sample for each 20 samples, one DI Field Blank ("DIFB") and equipment rinsate samples. During the quarter, two duplicate samples were collected as indicated in Table 1. The duplicates were sent blind to the analytical laboratory and analyzed for the same parameters as the nitrate wells. Rinsate samples were also collected at the beginning of the sampling period and at the beginning of each day of sampling from the decontaminated pump used for purging and sampling. Rinsate samples were labeled with the name of the subsequently sampled well with a terminal letter "R" added (e.g. TWN-7R). The results of these analyses are included with the routine analyses under Tab G. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QAlQC requirements established in the QAP were being adhered to and that the SOPs were implemented, except as noted below. 3.3 Analyte Completeness Review All analyses required by the GWDP for nitrate monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP (June 17, 2010 and revised February 15, 2011) identify the data validation steps and data QC checks required for the nitrate monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QAlQC evaluation, a holding time evaluation, an analytical method check, a reporting limit evaluation, a QC evaluation of sample duplicates, a QC evaluation of control limits for analysis and blanks, a receipt temperature evaluation, and a rinsate evaluation. Because no VOCs are analyzed for the nitrate contamination investigation, no trip blanks are required in the sampling program. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab H. 7 N:\Required Rep<lrtslNitrate Quarterly Monitoring Rep<lrt120 II QlI20 II Ql Nitrate Report text.doc 3.4.1 Field Data QAlQC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period of each other. The results of this quarter's review are provided under Tab H. Based upon this review, all well locations conformed to the QAP requirement to evacuate two well casing volumes before sampling except TWN-2, TWN-3, TWN-7, TWN-9, TWN-10, TWN-12, TWN-14, TWN-15, TWN-17, AND TWN-19. These ten wells were all pumped to dryness before two casing volumes were evacuated. In each case, representative samples of formation water were collected after the wells were allowed to recover. Piezometers 1, 2, and 3 were not pumped, and were sampled directly after measurement of one set of parameters. Two casing volumes were pumped from TWN-5, TWN-8 and TWN-13 before they were purged to dryness. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly sampling programs to the nearest 0.01 foot. All field parameters for all wells were within the QAP required limits, as indicated below. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Section 6.2.7 specifically state that field parameters must have stabilized to within 10% over at least 2 consecutive measurements. The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU below are included for information purposes only. • Nineteen well measurements and the measurements from Piezometer 3 exceeded the QAP's 5 NTU turbidity goal as noted in Tab H. In addition, the turbidity measurements in eight wells (TWN-1, TWN-2, TWN-3, TWN-5, TWN-12, TWN-13, TWN-17, and TWN-19) exceeded the QAP's 10% RPD requirement as noted in Tab H. All eight wells were purged to dryness before the stabilization of turbidity and as such these wells are not subject to the QAP stabilization requirement of 10% RPD for turbidity. Additionally, five wells were purged to dryness before more than one set of field parameters could be collected. DUSA's letter to DRC of March 26,2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's 8 N:\Required ReportslNilrale Quarterly Moniloring Rcport12011 QI12011 QI Nilrale Report texl.doc subsequent correspondence dated June 1, 2010 and June 24, 2010, DUSA is currently implementing a monitoring well redevelopment program. The redevelopment program has reviewed the available turbidity data for the nitrate wells and has developed a list of wells that have undergone redevelopment utilizing several strategies. The redevelopment strategies include additional surging and bailing and overpumping as necessary. Surging and bailing and overpumping for the nitrate and chlorofonn wells is complete. Redevelopment of the groundwater wells is in progress. Data from the redevelopment of the nitrate wells will be reviewed with the data from the redevelopment of the chlorofonn and groundwater programs. A single report will be prepared at the completion of the redevelopment program for the wells in all three programs which is planned for submittal on or before the end of the third quarter 2011. DUSA will review the redevelopment data and summarize the status of the Mill wells. Redevelopment results will be discussed with DRC in an effort to come to a consensus regarding turbidity considerations for the nitrate wells at the Mill site. The conductivity RPD exceeded the QAP specified limit of 10% in TWN-3 because TWN-3 was pumped dry prior to stabilization of field parameters and as such the QAP requirement is not applicable. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab H. All samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confinn compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab H. All samples were received within the required temperature limit. 3.4.4 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the QAP. Analytical method checks are provided in Tab H. All methods were consistent with the requirements of the QAP. 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by the laboratory were checked against the reporting limits enumerated in the QAP. Reporting Limit Checks are provided in Tab H. All analytes were measured and reported to the required reporting limits, with the exception of eleven samples and one rinsate blank sample that had increased reporting limits due to matrix interference or required dilution due to the sample concentration. However, in all of those cases the analytical results were greater than the reporting limit used. 9 N:IRequired ReportslNitrate Quarterly Monitoring Report12011 Ql12011 Ql Nitrate Report textdoc 3.4.6 QAlQC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits. However, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All duplicate results were within a 20% RPD in the samples except for chloride in the duplicate pair UWLP/Pond D. These results are less than 5 times the required reporting limit and the RPDs greater than 20 percent are acceptable. Results of the RPD test are provided in Tab H. 3.4.7 Rinsate Check Rinsate checks are provided in Tab H. Of the five rinsate blanks collected, four rinsate blank samples had reported concentrations of nitrate. A DIFB was analyzed and was reported as nondetect for nitrate. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than that of the actual well -indicated that two of the rinsate blank samples with detections met this criterion and two of the rinsate blank samples with detections did not meet this criterion. The concentrations of nitrate contamination in the rinsate blanks rose during the first quarter 2011. An investigation into the rising concentrations this quarter by the QA Manager was completed. The investigation results showed that Field Staff were reusing the decontamination soap and nitric acid decontamination fluids for more than the one day currently permitted per a UDEQ November 15, 2010 e-mail. The results are noted in the rising concentrations noted on consecutive days that rinsate blanks were collected. The changed procedure was discussed with Field Personnel, and the procedure was changed to allow the reuse of decontamination fluids for only one day before disposal. Corrective action for this issue is discussed in Section 5. As noted in previous reports, low level detections of nitrate in the rinsate blanks have been reported. Due to the deviation from the routine procedure discussed above, it is not yet possible to assess the corrective actions taken to date to determine if these previous changes have been effective in eliminating the low level nitrate contamination in the rinsate blanks. The assessment is not possible as the higher concentrations due to reuse of the decontamination fluids has obscured the low level contamination previously reported. The investigation into the potential sources of the low level nitrate 10 N:\Required ReportslNitrate Quarterly Monitoring Report1201 1 QII2011 QI Nitrate Report text.doc contamination will continue if the rinsate blanks continue to show contamination in the next sampling event. Corrective actions for the deviation from routine procedures are described in Section 5. 3.4.8 Other Laboratory QAlQC Section 9.2 of the QAP requires that the laboratory's QAlQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate Analytical Laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab H. All lab QAlQC results met these requirements. 4.0 INTERPRETATION OF DATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab C. The data from this tab has been interpreted (kriged) and plotted in a water table contour map, provided under the same tab. The contour map is based on the February 28,2011 data for all wells. 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter A comparison of the water table contour maps for the first quarter of 2011 to the water table contour maps for the previous quarter (fourth quarter of 2010) indicates similar patterns of drawdown related to pumping of MW-4, MW-26 (TW4-15), TW4-4, TW4-19 and TW4-20. Water levels and water level contours for the site have not changed significantly since the last quarter, except for a few locations. Pumping at TW4-4, which began in the first quarter of2010, has depressed the water table near TW4-4, but does not yet appear to have measurably affected water levels at adjacent wells. A reported increase in water level of approximately 3 feet occurred in Piez-3. Reported decreases in water levels of approximately 5 feet occurred in well MW -18, of approximately 21 feet occurred in well TW 4-18, and of approximately 20 feet occurred in well TWN-18. A reported increase in water level of approximately 11 feet occurred in pumping well TW4-4, and a reported decrease in water level of approximately 18 feet 11 N:lRequired ReportslNitrate Quarterly Monitoring Report1201l Q 1\2011 Q I Nitrate Report text.doc occurred in pumping well TW4-19. Water level changes at other pumping wells were less than 5 feet. Water level fluctuations at pumping wells MW-4, MW-26 (TW4-15), TW4-4, TW4-19, and TW4-20 are due in part to fluctuations in pumping conditions just prior to and at the time the measurements are taken. The largest decrease (increase in drawdown) of approximately 18 feet occurred in well TW4-19 and the largest increase (decrease in drawdown), of approximately 11 feet, occurred at TW4-4. Water levels reported for TW4-18 and TWN-18 during the current quarter are more similar to historical measurements than those reported for the previous quarter. 4.1.3 Hydrographs Attached under Tab E are hydro graphs showing groundwater elevation in each nitrate contaminant investigation monitor well over time. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached in Tab F are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 4.2 Review of Analytical Results 4.2.1 Current Nitrate and Chloride Isoconcentration Maps Included under Tab I of this Report are current nitrate and chloride iso-concentration maps for the Mill site. Nitrate iso-contours start at 5 mg/L and chloride iso-contours start at 5 mg/L because those values appear to separate the plumes from background. All nitrate and chloride data used to develop these iso-concentration maps are from the first quarter 2011 sampling events. 4.2.2 Nitrate and Chloride Concentration Trend Data and Graphs Attached under Tab J is a table summarizing values for nitrate and chloride for each well over time. Some data (MW -18, MW -19 and the Frog Pond) were not sampled this period but the historical data are included for information purposes. Attached under Tab K are graphs showing nitrate and chloride concentration trends in each monitor well over time. 4.2.3 Interpretation of Analytical Data Generally, the shapes of the nitrate and chloride plumes appear to be stable and unchanged for the last six quarters. The nitrate and chloride plumes maintain their general geographic association and it is still possible to separate the plumes into a segment northeast of the wildlife ponds and a southwest segment near the mill site. Nitrate and chloride concentrations in samples from the downgradient edge of the plumes 12 N:\Required ReportslNitrate Quarterly Monitoring Rcport12011 QI12011 QI Nitrate Report text.doc (in the vicinity of tailings impoundment monitoring wells MW-30 and MW-31) have remained essentially unchanged (current concentration within one standard deviation of the average of the previous five quarters and within laboratory variation) and the plume does not appear to be migrating in the downgradient direction. In general, both nitrate and chloride concentrations in nitrate monitoring wells are similar to values from last quarter or have declined (Tables 2 and 3). Notable exceptions include nitrate concentrations in samples from TWN-12 which rose from 0.5 mg/L in the fourth quarter of 2009 to a high of 4.2 mg/L in the first quarter of 2011 (as noted in Table 2 and in Tab K). A similar, although less dramatic, pattern can be observed in the nitrate data for samples from TWN-13 (as noted in Table 2 and in Tab K). The concentration of nitrate from the first quarter 2011 sampling event was 1.6 mg/L while the nitrate concentration from the fourth quarter 2010 was 0.4 mg/L. The chloride concentration in TWN-13 also rose to a high of 103 mg/L in first quarter 2011. The increases in concentrations noted above occurred in wells up gradient of Mill activities. The current quarter's data continue to support the conclusion in the Nitrate Contamination Investigation Report that the nitrate and chloride are co-extensive and appear to originally come from the same source. 5.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below. 5.1 Identification and definition of the problem Nitrate Contamination in Rinsate Blanks During this reporting period the nitrate levels in the rinsate blanks rose significantly. 5.2 Assignment of Responsibility for Investigation of the Problem The problems have been investigated by the QA Manager. 5.3 Investigation and Determination of Cause of the Problem Rinsate Blank Sample Nitrate Levels Rose Upon review of the data, it was noted by the QA Manager that the rinsate blank detections rose significantly. Investigation into the sources revealed that the Field Staff reused the soap and nitric acid decontamination fluids for more than one day as required by the November 15, 2010 e-mail from UDEQ. The reuse of the fluids caused the soap fluid to become contaminated with the nitric acid from the previous decontamination step. It appears that nitric acid then caused increased nitrate concentrations in the rinsate blanks. 13 N:IRequired ReportslNitrate Quarterly Monitoring Report120 II Q 112011 Ql Nitrate Report text.doc 5.4 Determination of a Corrective Action to Eliminate the Problem Rinsate Blank Sample Nitrate Levels Field Personnel were retrained on the requirements of the procedure specified in the November 15, 2010 e-mail from UDEQ relating to the reuse of the decontamination fluids and were instructed to reuse the decontamination fluids for only one day of sampling. At the end of each day the decontamination fluids are to be disposed and the drums refilled the following day. 5.5 Assigning and Accepting Responsibility for Implementing the Corrective Action It will be the responsibility of the Director, Compliance and Permitting to implement the following corrective actions. 5.6 Implementing the Corrective Action and Evaluating Effectiveness Rinsate Blank Sample Nitrate Levels The corrected procedure has been implemented during the second quarter nitrate sampling event. If however, the low level detections return, the previous investigation will be restarted and additional steps to isolate the potential sources of the contamination will be taken. 5.7 Verifying That the Corrective Action Has Eliminated the Problem Nitrate Contamination in Rinsate Blanks Verification of the corrected procedure implementation was conducted in April 2011. The verification was completed by the QA Manager during a visit to the Mill. The QA Manager observed decontamination procedures during the second quarter 2011 event. Data from the second quarter 2011 will be assessed to determine if additional investigations into the low level contamination issue are warranted. 5.8 Assessment of Previous Quarter's Corrective Actions The fourth quarter 2010 report identified a corrective action, for nitrate contamination in the rinsate blanks. Nitrate contamination in the rinsate blanks is discussed above in Section 5.1. Assessment of the low level contamination was not possible this quarter due to field changes to the decontamination procedures. Assessment of the effectiveness of corrective actions to date to determine the sources of low level contamination will resume upon receipt of the second quarter 2011 sampling event data. 14 N:\Required Reports\Nitrate Quarterly Monitoring Report\2011 Q I \20 II QI Nitrate Report text.doc 6.0 CONCLUSIONS AND RECOMMENDATIONS Generally, the shapes of the nitrate and chloride plumes appear to be stable and unchanged for the last six quarters. The nitrate and chloride plumes maintain their general geographic association, and it is still possible to separate the plumes into a segment northeast of the wildlife ponds and a southwest segment near the mill site. Nitrate and chloride concentrations in samples from the downgradient edge of the plumes (in the vicinity of tailings impoundment monitoring wells MW-30 and MW-31) have remained essentially unchanged (current concentration within one standard deviation of the average of the previous five quarters and within laboratory variation) and the plume does not appear to be migrating in the downgradient direction. In general, both nitrate and chloride concentrations in nitrate monitoring wells are similar to values from last quarter or have declined (Tables 2 and 3). The current quarter's data continue to support the conclusion in the Nitrate Contamination Investigation Report that the nitrate and chloride are co-extensive and appear to originally come from the same source. 7.0 ELECTRONIC DATA FILES AND FORMAT DUSA has provided to the Co-Executive Secretary an electronic copy of all laboratory results for groundwater quality monitoring conducted under the nitrate contaminant investigation during the Quarter, in Comma Separated Values ("CSV") format. A copy of the transmittal e-mail is included under Tab L. 15 N:lRequired Report.INitrate Quarterly Monitoring Report120 II QI120 II Q J Nitrate Report text.doc 8.0 SIGNATURE AN D CERTIFICATION This document was prepared by Denison Mines (USA) Corp. on Mayl?, 2011 . (USA) CORP. Davi . Fry< cnlund Vice President, Regulatory Affairs and Counsel 16 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowled e and belief, true, accurate, and complete. I am aware that there are significant enalti for submitting false information, including the possibility of fine and nt for owing violations. 17 N:\Roqulre<! Reportsl IIMlle QuiU'lcrJy Moniloring Reportl20J 1 01\2011 OJ llro'c Report , .. ,-doc Tables Table 1 Summary of Well Sampling and Constituents for the Period Wen Sample CoUectionDate Date of Lab Report Piezometer 1 1/3112011 Piezometer 2 113112011 Piezometer 3 113112011 TWN-1 112612011 TWN-1R 1125/2011 TWN-2 2/112011 TWN-3 211/2011 TWN-4 1/25/2011 TWN-5 1/25/2011 TWN-6 1/26/2011 TWN-7 1127/2011 TWN-7R 1126/2011 TWN-8 1/25/2011 TWN-9 2/112011 TWN-10 1127/2011 TWN-11 1127/2011 TWN-11R 1126/2011 TWN-12 1/26/2011 TWN-13 1125/2011 TWN-13R 1124/2011 TWN-14 1/28/2011 TWN-15 1127/2011 TWN-16 1/27/2011 TWN-17 2/112011 TWN-18 1127/2011 TWN-19 2/1/2011 TWN-19R 1/3112011 TWN-65 1/25/2011 TWN-60 2/112011 PondD 113112011 UWLP 113112011 Note: All wells were sampled for Nitrate and Chloride TWN-60 is a DI Field Blank TWN-65 is a duplicate of TWN-5, and Pond D is a duplicate ofUWLP. UWLP is a sample from the Upper Wildlife Pond 2115/2011 2115/2011 2/15/2011 2/10/2011 2/10/2011 2/15/2011 2115/2011 211012011 2/10/2011 2/10/2011 2/10/2011 2/10/2011 2/10/2011 2115/2011 2/10/2011 2/15/2011 2110/2011 2/10/2011 2/10/2011 2110/2011 2/15/2011 2110/2011 2/15/2011 2115/2011 2115/2011 2/15/2011 2/15/2011 2/10/2011 2/15/2011 2/15/2011 2115/2011 4thQ 2ndQ Location lst Q 2010 2009 2010 Piez 1 NA NA 7.2 Piez 2 NA NA 0.6 Piez 3 NA 1.7 1.6 TWN1 0.5 0.5 0.6 TWN2 20.8 62.1 69 TWN3 29 25.3 26 TWN4 004 0.9 1 TWN5 0.2 0.3 0.3 TWN6 104 1.5 104 TWN7 0.1 0.8 1.2 TWN8 0.1 O.l O.l TWN9 12 7.6 7.7 TWNI0 104 1.5 1 TWN 11 1.3 104 1.3 TWN 12 0.5 0.7 0.8 TWN13 0.5 0.1 0.1 TWN14 304 2.9 2.9 TWN15 1.1 0.7 1 TWN16 1 1.2 1.3 TWN17 6.7 lOA 11 TWN18 1.3 1.6 1.8 TWN19 704 7.2 6.2 Red value indicates nondetect Table 2 Nitrate (mglL) 3rd Q 2010 4th Q 2010 6.8 6.5 0.6 0.2 1.8 1.8 0.6 0.6 69 48 27 24 0.9 1.0 0.3 0.3 104 1.2 1.6 1.0 0.1 O.l 10.7 8 0.2 1.3 104 104 0.7 0.7 0.2 004 3.5 4.2 1 1.2 2.6 2 8.9 8 1.8 1.6 7.2 7 % Difference 4th lst Q 2011 Q 2010 and lst Q 2011 7 8 0.3 50 1.8 0 0.5 -17 43 -10 24 0 0.9 -10 004 33 1.1 -8 1.3 30 0.1 0 9.5 19 0.3 -77 104 0 4.2 500 1.6 300 3.7 -12 104 17 4.6 130 8.6 8 104 -13 7 0 ls't'Q Location 4th Q 2009 2010 Piez 1 NA NA Piez2 NA NA Piez 3 NA 116 TWNI 18 17 TWN2 55 85 TWN3 106 111 TWN4 11 22 TWN5 48 43 TWN6 21 19 TWN7 7 6 TWN8 12 11 TWN9 205 183 TWNI0 26 54 TWNll 74 73 TWN12 109 113 TWN13 83 47 TWN14 32 24 TWN15 78 43 TWN16 39 35 TWN17 152 78 TWN18 57 42 TWN19 125 118 Table 3 Chloride (mg/L) 3rdQ 2nd Q 2010 2010 52 52 8 8 36 35 20 19 97 104 118 106 22 19 44 43 22 73 6 7 11 11 175 210 30 21 72 76 106 112 49 53 30 26 39 36 35 35 87 66 63 64 113 113 4th Q2010 60 6 25 14 93 117 21 45 21 4 9 172 28 72 103 57 28 38 30 65 59 107 % Difference 4th 1st Q 2011 Q 2010 and 1st Q 2011 60 0 9 50 40 60 17 21 93 0 138 18 21 0 47 4 18 -14 6 50 13 44 217 26 40 43 84 17 87 -16 103 81 24 -14 43 13 34 13 90 38 61 3 114 7 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and FieJd Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H~l Field Data QNQC Evaluation H~2 Holding Time Evaluation H-3 Receipt Temperature Check H-4 Analytical Method Check H-5 Reporting Limit Evaluation H-6 QNQC Evaluation for Sample Duplicates H-7 Rinsate Check H-8 QC Control Limits for Analyses and Blanks Tab I Kriged Current Quarter Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Concentration Trend Graphs Tab L CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site l 0 SCALE IN FEET EXPLANATION MW-20 • perched monitoring well TW4-19 0 temporary perched monitoring well PIEZ-1 perched piezometer Q TWN-1 temporary perched nitrate ~ monitoring well TW4-26 temporary perched monitoring well ~ installed May, 2010 MW-34 perched monitoring well installed -¢-August/September, 2010 PROPERTY BOUNDARY h II II (( ~ // /1 II II II II II ~ CELL NO.1 MW-01 • ~5 <> TWN-7 CELL NO.2 MW-03 • MW-20 • 3000 f wildlife pond HYDRO GEO CHEM, INC. MW-17 • 33 APPROVED SJS MW-18 • <> TWN-18 <> TWN-3 <> TWN-6 <> TWN-8 <> TWN-15 <> TWN-10 <> TWN-9 PIEZ-1 .. MW-19 • PIEZ-2 .. PIEZ-3 .. <> TWN-11 <> TWN-14 OTW4-1EbTW4_11 OTW4-13 TW4-7m-S OTW4-1 OTW4-40TW4_14 TW4-23 OTW4-6 o PIEZ-4 .. * PIEZ-5 .. T37S T38S ~TW4-26 MW-22 • 1/ // // // // // // // // // // SITE PLAN AND PERCHED WELL LOCATIONS WHITE MESA SITE DATE REFERENCE FIGURE H:/718000/may11 Iwelloc1 O.srf TabB Order of Sampling and Field Data Worksheets . .. Name Nitrate MilL lWN-8 NO .;. lWN-13 0.4 :Ji TWN-S 0.3 -~ TWN-l 0.6 ., TWN-12 .-0.7 ~ lWN-4 1 ~ TWN-7 1 -." TWN·1S 1.2 -..;. TWN-6 1.2 ~ TWN-IJI 1.3 ~ TWN-11 1.4 TWN-18 1.6 TWN-16 2 TWN-14 4.2 - ~ 7 TWN-17 8 - ~ 8 ~ 24 lWN~ 48 Piez 1 6.5 Piez 2 Plez 3 wildlire P'"~{ D 0.2 Total Depth Name Date Sample fil!~~~ Samples Date~-siilmple Depth Rlnsate Samples TIts-III 0 1'1 :?f) hi 'e.. 145.5 TWN·8R {I.t .r:;- 1J'l~/1f 0 , Lf/'J( 4-;'1L 2-120 lWN-13R l· ~&.l. Ll II"'~ .~ ( -1/'l~J/I 0 , Ift/S ll'.tk" 150 TWN-SR I~.H ~ ! f!f!I,/// 0 (3s( qr.7~ 112.5 TWN·IR II~'II 101 4 IfL~/1/ 0 /¥r(J :Jr. 7~ 110 TWN-12R 11 .. ~~.l\ 1 .. <2~-U 0 I~~~ ~7.~, 125.7 TWN-4R 11 -~.\1 0 lOS ":I'r, lWN-7R I ·~·'\ ~~&.I -0 155 TWN-15R 1'.~.ll '·!l'·d o 1!J.A7 71i 72-130 TWN-6R l .. TI~it 0 105 TWN-IOR 1.~"~1l J .. !l.7~ 1 \ o Oqof 6tt.'3 142 TWN-UR l .. fl.1f t'HJO~ I l ~.a.7.1 1 0 't')~~ (.,c I () 145 TWN·18R 1·]:7· It L~~7-l\ 0 \1..t.f~ L.t~ ~u 100 TWN-16R I. '1"i.1L , .. ~t ~ 1I 0 6J~~O 13S TWN·14R I~TI-TI rJ..I is j /11 0 0/""'1.:,. 5 ·.1.'lS 110 TWN-19R '-::31 ·H (')73b 1!l.11/n 0 nJ~(l ~~27 110 lWN-17R r. '1, . II I~' III 0 11)1D4 " .. ~, 97 TWN-9R I ·:j1-TI ~Jf lit o ~g2.1.. :!t1.1b 96 TWN-3R II~I -\\ 11.1, III olD'g~, 1'.4~ 96 TWN·2R i ·ji -l\ Silmplers: \\.f 1 1Jt,,,,-{) f) . .r g Jt"Wl h tJ r-r () * "" &.. So b L--WI... .s 1".;. pp ~J.. -MiII-Groondwl,i.n lJischarge Permit Date: 03/2'i./2010 Rev, 6 Groundwater Monitoring Quality Assurance Plan (QAP) I f i f IUNISOJ) J MINIS ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment I (' 1/ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event I'51-Gucs..ctf<C ..vi tCl:--tc .. (b::z,\ Location (well name) ; .... 1 ..... T-='-'A/""----IoI ________ ---' Sampler Name and initials: 1 (.zc;..I"I'"j& €CL.\Me.r-I ke Date and Time for Purgin~'-oI-l ~_2=-5,-· -..... 1 .... \ ____ --' and Sampling (if different) I 0112 b {20J/ Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) I GV < 6'" '" bS Sampling Event lOIN_duly N . tmtlJ Prevo Well Sampled in Sampling Event I'r W ),/ -S pH Buffer 7.0 t-17..JJ",;f ()~ __ --l pH Buffer 4.0 14,0 Specific Conductance!-I _9L.19L.J<11--__ --lIIlMHOSI em Well Depth(O.O1 ft): I II 2. s Depth to Water Before Purgin~ Y9t 1,...18 Casing Volume (V) 4" weU:14 L \3 1(·653h) 3" Wcll:a...;. 0=--____ . (.367h) Conductance (avg) !-I """[$=0 ..... 1'--____ -' pH of Water (avg) ,-17~, ..... O,-3.:;...... ____ --, Well Water Temp. (avg) 11'-L'1\ Redox Potential (Eh)I ..... 3=-:,1 ... 'l_-, Turbidity I t 0:3. 75 Weather Condo 11-5_' v_,.,.-.._y _________ -" Ext'l Amb. Temp. ·C (prior sampling event)I .3~," Time IIIQ.? 1 Gal. Purged I 1 '23 I Time 11\03 I Gal. Purged 1 I 7Q I Conductance I ~1 2 I pH1 7.0Y 1 Conductance ISQI I pH 17.03 I Temp.oC 113.'15 ] Temp.oC I IL.L!il I Redox Potential Eh (mV) 1.:3;2.Q I Rcdox Potential Eh (mV) I :319 I Turbidity (NTU) 13 .3. t 1 Turbidity (NTU) 176, q J Time 1110 '1 1 Gal. Purged 11 87 I Time 11 1£25 I Gal. Purged I ~Q'=! I Conductance I ::Z96 f pH I '2~ Q'1 1 . Conductance I 7~!l I pH I "7~O' I Temp.oC 1 jt-L38 I Temp,oC 1 l<1w3A I Rcdox Potential Eh (mV) 13;20 1 Redox Potential Eh (mV) I '3\8 I Turbidity (NTU) I l~~:L ~ 1 Turbidity (NTU) 1 L..j 9.9 1 White Mesa Mill Field Data Work~heet for Groundwater .A .. 10f2 capturx' COIIPAT'.LE WITH;""'-HUllir-ruNcTIONALITY Mill· Gr~undwilter Discharge Permit \ Date: 03/22/2010 Rev, 6 Groundwater Monitoring Quality Assur.mce Plan (QAP) , ~ Volume of Water Purged 1 ~09fr 7e Pumping Rate Calculation Flow Rate (Q), in gpm, S/60 = .... 1 ...... 1-1..1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T:;2V/Q:; 1 ~ 14~g3 Number of casing volumes evacuated (if other than two) Jfwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~LL.;#;..../uA:...!.-_____ ....J Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified below) Y N Type VOCs 0 0 3x40 ml 0 0 HCL Nutrients 51 0 lOOmi 0 IS H2SO4 Heavy Metals 0 0 250ml 0 0 HN03 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. Gross Alpha 0 0 1,000 mI 0 0 HN03 Other (specify) ~ 0 Sample volume 0 1)1 Preservative Added y N 0 0 IS 0 0 0 0 0 0 0 0 151 ( "'-\0'-, cl.. c-Ifpreservativc is used, specify Type and Quantity of Preservutive: ~Commel1f , See instruction <' I f Arc-'Iv".)... 0"'-' .s Ite..... t>-+, \ozg_ Ge-rhA. c..N:J... (L'i"-A S .. fr-~..>U'-+ ~vr pvr-be.. o........A .s~P\1 ~ e.-ve-I\,.'~. pv~e.~ \..<.?c:..1 1 ~(i.('" ()..... 'ro'\-"""\ c7f I{)-~1"'U+G.S eo.".,A :34 Se.{,O~. we.l\ t'6.N ar y, \....Io •• .+e.r L.v'"".s t:.-\t.a.-r" "'I,...I't>U~(.,...Ov t (Jv r:£>e.. P £l...1'C<.M-e-i U'> v/e.r-e... c"oflJ.. rro,"",,- Cive.r pVM,.fl~ .5""c:..~t" i..G-t+ >,te.. e..l JIIGf. ev,:!\i ~ b~"-I\., e...+ Il?S3 .. o.rr:w-cA -to Sa""1 t, ciT' 1:5 '-I 4 r Dep'lh we"S "J"eV/4.vv 'Iq l-i{ ~wfle.. ~/Iu1eJ d-'-/35 I SUWlflG-Ibllu'kd ~'( r2r~ f~tM.4l-r L--_______ ---JIDo not touch this cell (SheetName) White Mesa Mill Field Oata Work5heet for Groundwater A 20f2 capturx' ~O"""TIBLE WlTH~._Ji>--'UNCTION'LITY • Mill-Grou~-jwaterOischarge Permit O~te: 03/22/2010 Rev. 6 Groundwater MOllitoring Quality Assurance Pian (QAP) i ! I t e f ATTACHMENT 1 Attachment 1 OENISO,}), ~. WHITE I\JESA URANIUM MILL .j Se.: ins\nIclion MINES FIELD DATA WORKSHEET FOR GROUND WATER Dcscr~tion of Sampling Event: II st LXlllLtt:(;..r" Ali lre-tc.. :J.b\\ Sampler Name Location (well name):1 rWIl/-18--and initials: GtC crio pe.\,CAr"c / t.P Date and Time for Purgin~'-)'-'_2~5",-, 1&.61 ____ -...J and Sampling (if different) Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) Sampling Event 1 ay'g.. ... ~'"t'\y tV, l-ce-t c...1 Prevo Well Sampled in Sampling Event I·r """"..v-s pH Buffer 7.0 ,-17~_ Q""--__ _ pH Buffer 4.0 I L-i . 0 Specific Conductancel ......... 9 ..... 't'-q~ __ ..... 1 ).lMHOS! em Well Depth(O.Olft): ..... 1 #<...:;......</ ..... 4'--_---' Depth to Water Before Purgin~ AtjA Casing Volume (V) Conductance (avg) 1-1 +1 a~ ______ -l Well Water Temp. (avg) I?-o 1'1 Redox Potential (Eh)1 '30'3 Turbidityl'--'-'L....,D"'--_ .... Weather Condo 1...1 S_v_"'_"--=..i ________ -.I Ext'l Amb. Temp. ·C (prior sampling event)12D"- Time I ID l Y I Gal. Purged I 150 I Time I I Gal. Purged I I Conductance I 12. I pH 1 6. a~ I Conductance 1 I pHI I Temp.oC Il,l'1 I Temp.oC 1 I Redox. Potential Eh (mV) 1£ 0 9 I Redox Potential Eh (mV) I I Turbidity (N11J) I 1.0 I Turbidity (NTU) I I Time 1 I Gal. Purged 1 I Time I I GaL Purged I I Conductance 1 I pH 1 I Conductance I I pHI I Temp.oC 1 I Temp.oC 1 I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 capturx' ~o .. rATIaLE W'TH~W-'U"CTIONALITY Date: 03/22/2010 Rev, 6 11.0111-Groun.dwatfOr"Oischarge Permit ) Groundwater Monitoring Quality Assurance Plan (OAP) ~ ~ ~ Volume of Water Purged 1'--II_!?~e"--__ --I gallon(s) Pumping Rate Calculation Flow Rate (Q). in gpm, S/60= L-I ...J..J ~7 __ ----J Time to evacuate two casing volumes (2V) T=2V/Q= I AlA I Number of casing volumes evacuated (if other than two) I,~IIA Ifwell evacuated to dryness. number of gallons evacuated I AlIA Name of Certified Analytical Laboratory if Other Than Energy Labf'-"AI ......... /..LA..>.-____ --' Samp]e Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified below) Y N Type VOCs 0 0 3x40 ml 0 0 HCL Nutrients (gJ 0 lOOml 0 I8J H2SO4 Heavy Metals 0 0 250m! 0 0 HN03 All Other Non Radiologies 0 0 250ml 0 0 No Presel'V. Gross Alpha 0 0 1,000 ml 0 0 HN03 Other (specify) I5D 0 Sample volume 0 fSil Preservative Added y N 0 0 iii 0 0 0 0 0 0 0 0 1m I ...... t.... \or' fJ.e.. Ifprcscl'Yati\'c i!olliSed, !olpccitY Type and Quantity of Preservotiyc: ~ See instruction ~Comment A {"'II vc;..el (!){\. .$lte.... c<-.\--1000. b{!.. ... hA. ~ ~"I(h ...... .$" /JIA. .sHe.. ~()~ r-, .... >"...\-e.. ft.'i,A...s",",~G.-bc.~"'" bLr 100.5_ PVl'Apuk Sf) 6~IIC>A$ of' At.-'~ v&<-te..r-1 50 C..,..Li(;lA.,> O'·f.$cJ(;..p l#iA.+ e,il I>.~ £0 6-.1 'OA~ C1~ O. r. ;,..c/c.o-.... ~. 'T CD Y' S~t"'I-f' leo 0-.+ \en L-\. L.~,S t .> d'c.. lA.'\-\0 ~\. L-.. _______ -...IIDo not touch this cell (SheetName) White Mesa Mill Field O~t~ Worksheet for Gn;lundwi!ter A 2of2 capturx COMPATIBlE WITH~_ri;r--FU"CTIONAlITY Mill· Groundwater' Discharge Pe{mit ) Groundwatef Monitoring Quality Assurance Plan (QAP) -) Date: 03/22/2010 Rev. 6 i ! • ~ a ~ J ! I i t ATTACHME~T 1 Attachment 1 ()ENISO,.!)~ ~. WHITE MESA URANIUM MILL 'y Sel: instruclion MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: liSt Q v o..c k e,.r AI, ~ 1'0-. t k 'd.Q \ Sampler Name Location (well name):l T WN -'d.. and initials: (jo...rr-·I,(\. e.,.\Mt:cc Date and Time for Purgind OI/31/1Qi\ , and Sampling (if different) 10 'J-/o. 1/ :l" \ \ Well Purging Equip Used: [!]pump o@ bailer Well Pump (if other than Bennet) I (;I'"j)M~PS Sampling Ev,,"' QUI." t eel y N\ I-C'" h:_1 Prevo Well Sampled in Sampling Event IT \;J AI-3 pH Buffer 7.0 lL-:7...:...~O:..-_..-l Specific Conductance,-' .... 9 .... 9a..Q.L-__ --Ih,MHOSI em Depth to Water Before Purgin~ \5, 'to Conductance (avg) L-.l _.3::...:~c:....Ya..Y~ ___ ..-l pH Buffer 4.0 1 4 .0 Well Depth(O.O 1ft): ~I ...... 9 ...... 6 .... · __ ---' Casing Volume (V) 4" Wel1:~(.653h) 3" Wcl1:~(.367h) pH of Water (avg) Well Water Temp. (avg) I I,.. fit, Redox Potential (Eh)1 333 Turbidityl '21 t Y 6 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)1 OPe;. Time ll31K I Gal. Purged l 11 I Time 11.311 I Gal. Purged I ~4 I Conductance 13~3t I pH I 6.10 I Conductance 1 3~~~ I pH I 6 .. t>8' I Temp.oC I IJ. t:J. I . Temp.oC I 12.<Ja I Redox Potential Eh (mV) 1 7 ')..7 I Redox Potential Eh (mV) I ~:2g I Turbidity (NTU) 1-13,7.'-1 Turbidity (NTU) I :3 h. 4 I Time 1132-6 1 Gal. Purged I 51 I Time I I Gal. Purged I I Conductance 13~ I pHI 6 t II I Conductance I I pHI I Temp.oC I J >_ 0 '-I I Temp.oC 1 I Redox Potential Eh (mV) I 33g , Redox Potential Eh (mV) I I Turbidity (NTU) I :1.0. 6. 1 Turbidity (NTU) I I WhiteMe5<lMiU Field Data Worksheet for Groundwater A . 10f2 capturx· COM'''T1aLE WITH~"""W--'UNCTlONALITY Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev, 6 Groun-dwater Monftoring Quality Assurance Plan (QAP) Volume of Water Purged I I) L..f ~.51 gallon(s) Pumping Rate Calculation Flow Rote (Q), in gpm, S/60 = 1c........:I....:/ __ ---I Time to evacuate two casing volumes (2V) T=2V/Q= I ~ 1 6./S Number of casing volumes evacuated (if other than two) LOY If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory ifOthcr Than Energy Labf~-L-.;V:--L.I..L.A-,--____ ---, Sample Taken Samplc Vol (indicate Filtered Preservative Prcscrva ti vc Typc of Sample if other than as Added y N specified below) y N Type y N VOCs CI 0 3x40 mt CI CI HCL 0 0 Nutrients r!. 0 lOOmi 0 ~ H2SO4 fiD 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,OOOml 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 if 0 fil C. ~ \ C) r-', fAt> If pre!'Crv3tivc is used, specifY Type and Quantity or Preservative: g See instruction ~Comment Ar-r-\.I e..cl 00/\.. S'd .. I:.-l)...·\-I :f,S7.0C4f"r' ..... ().NJ... '(2.ij).~ $, O.,/\. Si te... ~ Pwt>~ o..AlA .s:().v"\fl ,~ e ve.-AL ~u~e,., b~o.oI\... o..-\--1317 .. PVMe f'"CW'\.-,~C<r .$ -I"\.A-;.) te..,$ a.NA :3\ .su:.-Cl.~S r,.Je.\~ ~c-.A tAr-y o PA.r~e,+~~ Were-·\-odC .. e" 'P ('oOJV\, over~"'Mp ~~ ·9i-c..lvl .s~. L e.'~+ ~I+ t.. Dv+-1..3~~ .. A ir--,Ve.t-ClI'-Si k ~~ c,... \-D'l'J..6, bM(\'i'-o..Nt (2.yA..A. S, Pre..s~~ ~ S'-M.{J\c..5 W"'f't-+o-.~ "" t c>g33. De-Pt-k. \-'0 ....... ,\...~e,..(' ~~_s 15,L-l3. t. t.~-t-S I tc.. t?-~ (/~3 6. '--_______ -..IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater A 20f2 capturx' COOlPATlBL! WITH/'"...u'nr---.UHCYlOHAlIfY Mill • Groundwater Discharge Permit ) ) Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance PI~n (QAP) GENISO,}) J I MINIES A IT ACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 "i' See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event I 1$+ Q 1/"," .\= tee NIt t e..J c.. ~ D l} Sampler Name Location (well name):l TWN -'3 and initials: Date and Time for Purgin~ C? 1/3 1/:bD i l and Sampling (if different) I 0 :&1 0' /1(), 1 Well Purging Equip Used: [!] pump o@ bailer Well Pump (if other than Bennet) I 0 t s>:'" ,C;; S Sampling Event OvCv(" t e.r\r ;V; ft&\e Prev, Well Sampled in Sampling Event I r wP -Of pH Buffer 7.0 ...... 1 ...!.7..::...~O __ ---I pH Buffer 4.0 4.0 Specific ConductanccL...1 9-,-Cf4..9....1.-__ ,...jI IlMHOSI em Well Depth(O.Olft): ...... 1 __ 9u6o:....· __ ---' Depth to Water Before Purging/ 31. 07 Casing Volume (V) 4" well :1 ~:2 .. 3g 1(·653h) 3" Wcll:. _ . (.367h) Conductance Cavg) pH of Water (avg) 6.06 Well Water Temp. (avg) I J ~ .$q Redox Potential (Eh)1 '37 7 I Turbidity I 16. Y ! J Weather Condo Time 1/1 5'1 I Conductance 11:l5Q Temp.oC I ILKft Redox Potential Eh (mV) I Gal. Purged I I pH I I '''lB.? I Turbidity (NTU) I .2t.1 .L-t I Time I I Gal. Purged I Conductance I I pHI Temp.oC I 1 Redox Potential Eh (mV) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 11 I 5.96 I I I Ext" Amb. Temp. ·C (prior sampling event>ll. C {.... I Time I Ja,Ob I Gal. Purged 1 3 Y I Conductance I ~~g5 I pH I 6 .2-.5 I Temp.oC I I 2. "1 1 I Redox Potential Eh (mV) I 36,7 I Turbidity (NTU) I g.;:, I Time I I Gal. Purged I I Conductance I I pHI I Temp.oC I 1 Redox Potential Eh (mY) I I Turbidity (NTU) I I Mill· Groundwater Discharge Permit • Groundwater Monitoring Quality Assurance Plan (QAP) Date: 03/12/2010 Rev. 6 Volume of Water Purged I y" _ )9 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 11--.1-\ 7..:-. __ --' Time to evacuate two casing volumes (2V) T = 2ViQ = I ii@ij) I L.t qg Number of casing volumes evacuated (if other than two) I .45 If well evacuated to dryness, number of gaUons evacuated I yq.2-9 I Name of Certified Analytical Laboratory if Other Than Energy Labj'--'ltV,.../""Ao....I-_____ --' Sample Taken Sample Vol (indicate Filtered Prcserva ti ve Preservative Type of Sample if other than as Addcd y N specified below) Y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients t8I 0 lOOml 0 ~ H2SO4 !Sit 0 Heavy Metals 0 0 250 rol 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1.000 ml 0 0 HN03 0 0 Othcr (specifY) ~ 0 Sample volume 0 621 0 ISiJ c..1A I t~ r-~ ile Ifpreservativc is used. !>pecify Type and Quantity of PreserVllliv~: !Comment See instruction AC-f" .. v~-L Cl""-.s d'"'-c.. £!..\..+ 1I3t. c,c..r~\A... o...l\.rA g yc.. ....... 5. pr-e..s~t .'\l()..l-' pv~e.. (A..r-.J.. 'sa..N'\f> l \ ~ e.v eA,;t, ~ V ~i-);. e....:\4"""'" tI.. + 115 g " P 'h'''''( f'A. tI\ f' o..r-2. ",,'oJ\. v of e oS ~ '37 $e.c..o~.s. We..ll r~A..tJ..t-'I ' Pa..I"Q....M-e.,·t u-.> vVe..re... ··tc .. t;.e,,,,, ~""O,v\.. +~~ (!1verp~Mf'lIIA. ~ie..."'cl S/.s..(/(;-L t.t-t:+-Stt<... Qv~ \ :J.tl7... -.....J An-w c..c\ CJo/'-S; I ~G...-~t O~'6. 6( .. c-I'-,J'. o..~ f-ye.."" S, Pl't..!> ~.,d. '>c..MP\e. oS We.,rt--tc\'/UV\.. ~t OgJ.~. D .. pi-\,... re> \ ... h\,.t~ c.,.Jt-.S ~L 70. L.~'~ $1 ~c..--~t Og,7.4 . '--_______ --JIDo not touch this cell (SheetName) White Mesa Mill Fi~Jd Datil Worksheet for Groundwater .A 20(2 capturx' (DIIPATlaU WITH./'-'-'U)Iir-FU"CTlO~ALlTY , Mill • Gro"'ndw~ter Discharge pl.rmlt ) Date: 03/22/2.010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) OENISOJ)~~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 --.. ' Sec in~lruclion MINES FIELD DATA WORKSHEET FOR GROUND WATER D~cr~~nof~m~~gEw~: 1~I~t~t~(~ll~/~~c~.~~~r~#~,u~~C~&~t~~~~~O~I\~~~~~~~~~~~~~~~~ Location (well name) :I .... T........,\.J"-"'AI-'--"kj'i-_~ __ ~~~-----' Sampler Name and initials: Date and Time for PllIgingj~.J..I-....u:.d.=-5~'-llL-l-\~~~~.-l Well Purging Equip Used: ~ pump o@ bailer Sampling Event 1 c:s "AC r~cj1 AI; ~ re..\eJ pH Buffer 7.0 .... 17.L&.J.O"'--__ --J Specific ConductllJlce L..I .....Io9.;.jq ....... 'JL--__ --J1 ~MHOSI em Depth to Water Before Purgin~ 37. f?\ Conductance (avg) 1 ..... 4-'1 e~w"",--____ ----, and Sampling (if different) L..-LNL.L.I Ac..JL---~ ___ -J Well Pump (if other than BeIll1et) I 12r=vAAfo.s Prevo Well Sampled in Sampling Event I Tw.N -1 2. pH Buffer 4.0 11.1 .0 Well Depth(O.Olft): I Il.s.7 Casing Volume (V) pH of Water (avg) 4" Wel1:~(.653h) 3" wcn:~(.367h) Well Water Temp. (avg) II Lf .. OZ Redox Potential (Eh)IL..o3.::;;....o"o18 __ ..... Turbidity 1 \ '-13. b Weather Condo Ext'l Amb. Temp. 'c (prior sampling event) I y"L Time 11'135 1 Gal. Purged I jl.38 1 Time 1/43 6 1 Gal. Purged I Us I Conductance I lO It~ I pH [ 6 .89 I Conductance 11(22.6 1 pH 16 sg I Temp.oC 11 ~.la I • Temp.oC 1 1£1.j3 I Redox Potential Eh (mV) I ~ 19 I Redox: Potential Eh (mV) I.> Ig 1 Turbidi~ ~) I I ~J~I I Turbidity (NTU) I llib . 0 I Time IIH37 I Gal. Purged I ;l7;J. I Time IIY3~ ~ GaL Purged 1 2S19 I Conductance I 1 Q:l.:l I pH I 6.!6 I Conductance I l"lO I pH I 6. 5TH I Temp.oC [ 1'>.9;), I Temp.oC 1 1;3-qO I Redox: Potential Eh (mV) I 3 1S' I Redox Potential Eh (mV) I ;3lg I Turbidity (NTU) I I ~ v!. 9 I Turbidity (NTU) 1 1!:j~~ 7 I White Mm Mitl Field Data Worksheet for Groundwater , -Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater M"onitoring Quality Assurance Plan (QAP) Volume of Water Purged I ;].9 (.:L JO Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1 ............. 1 7.&.--__ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q'=' ~ 16.7'1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated I A/IA ,; - Name of Certified Analytical Laboratory if Other Than Energy LabfL...Nz...4I.-4A...1-. ____ ---' Sample Taken Sample Vol (indicate Filtered Preservative Preservali vc Type of Sam pic if other than as Added y N specified below) Y N Type y VOCs 0 0 3x40ml 0 0 HCL 0 Nutrients IS 0 100m! 0 Ii H2SO4 fiI Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv, 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 Other (specify) Iir 0 Sample volume 0 Jil 0 c..k lor', d..t... If preservative i~ llsed, specity Type and Quantity or Preservative: ~ See instruction l: ~Comment Ac-r-IVc.J.. ~f/\-.>I-f"-v,;t 1"105 .. bfA-to,.: ..... MA ~Y"""" t. et"-$'-~e. ~o.r-fu~e. e..M 5IA.AP\i~ e.Vt-"t. Sh:.r-+eel pv';!>c... 0<-+-1'1071. P"'~c:..A W''-II ~c).(' A tot"",\ of 17 Mio'\.vt~.s ,;..~ '30 ;;'t..(..()~>. t.../ .... +oI!r" l.VA.}> c,,\(..~(" t~I'-C1~"'w+ e.ve..A.h f'a.('o..~tl!4'>' WG.rc.. ~pjuJ... . Pt'&).,v\. OLlU' PVlVlfl~ ,S",-"e..-+. t-e,..-Pt >~tc.. ~! 1"155. $a""'f Ie.. w~ ~ t lede d, (7o-1.J.w-_ pvo.vt t. tNw~ &vv..fldtJ CW'-e-( ftr4 ~ devf WeV'~ srA!k,. 3c...""'-f1ft. ~s t!JIe~IJ.J. cl1-I '-13 ~ 1 t '--_______ ---'100 not touch this cell (SheetName) White Me$a Mill N 0 0 0 0 0 ria Field Data Worl<sheet for Groundwater .A 2of2 capturx-CO"~"'TlPLE WIT"/'"HU'li:>--FUNCTlONALITY • Mili • Gr~un?w~sr Discharge Permit ) Groundwater Monitoring Quality Assurance Plan (QAP) Date: 03/22/2010 Rev. 6 I ~ I . OENISO,})J ~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 .> See ins1ruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: II Ii 1-Dup:-r hAt N . r tiCkle 20u Sampler Name Location (well name):1 T l.J AI -5 and initials: I Go.rt....... f>p,\MCc(" 6e Date and Time for Purging i ~;) S -~b'l --, and Snmpling (if different) Well Purging Equip Used:~pump o@ bailer Sampling Event I Q VA.du li N. teo?-tee I pH Buffer 7.0 1 ..... 7 ............ 0"--__ -' Specific Conductance ..... 19 ..... 9 .......... q ___ ....JI~MHOSf cm Depth to Water Before Purgin~ 69* s;? Conductance (avg) L...I $&<...L.JHL..:;y"--_____ --' Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event I, wi ,AI-\'3 pH Buffer 4.0 l1 .D Well Depth(O.O 1ft): L..1 .... 15..,0""'-__ ....... Casing Volume (V) 4" Well:~(.653h) 3" wcn:~(.367h) pH of Water (avg) 6.40 Well WalerTemp. (avg) 111;1.14., Redox Potential (Eh)I 785 TurbidityI 3;l.7 Weather Condo 1L..5_"_v_""_r\._1 _________ ---' Ext'l Amb. Temp. ·C (prior sampling event) I I 0 c. Time loaw; I Gal. Purged I 69 I Time l ~g45 I Gal. Purged 1 I f) a. I Conductance 13111 I pH 1 b .l '1 I Conductance 1311::1 I pH I 6_38 I Temp.oC 114,.lb I Temp. "C li4 ,Hi I Redox Potential Eh (mV) I 'J..B7 I Redox Potential Eh (mY) I :t=7OS I Turbidity (NTU) I.::n-/. q I Turbidity (NTU) I tl.! I Time I OS HJ I Gal. Purged Li.ii I Time IQ2'i9 I Gal. Purged I 170 I Conductance 13115 I pH 16. Y7 I Conductance 1 :311~ I pH 16.5;l I Temp.oC II Y!I ~ I Temp.oC !ILLi5 I Redox Potential Eh (mV) I ~gs I Redox Potential Eh (mV) I :iq b I Turbidity (NTU) 1,5.].6 I Turbidity (NTU) 1 ~f2 7 I White Me$a Mill FIeld Data Worksheet for Groundwater .A 1of2 capturx" C" .. ~.f'8L! WITH./'-.fU>lir--'UHCTlONALITY · Mill-GroundwatF," Discharge Permit ) Gr'oundwater MonitorinR Quality Assurance Plan (OAP) Date: 03/22/2010 Rev, 6 Volume of Water Purged 1 18'j1-0;;t-~ Pumping Rate Calculation Flow Rate (Q). in gem, S/60;:: ,--I ...... 17:....--__ .....l gallon{s) Time to evacuate two casing volumes (2V) T=2V/Q= I~ 16,.15 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labi ... ..<...AI.;......:...t/A-=--_____ ......I Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients iii 0 lOOml 0 JjSI H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 NoPreserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specilY) T2l 0 Sample volume 0 IiC 0 ~ Co\.... \ "I-J..L If prc~crvative is used, specify Type and Quantity of Presen'ative: See instruction Arr-,v"J.,. "A. ,S'jl,-0..+ 081;!.. 6(Jo.l'h >j\.. tMJ.. e.y"-1\.. $, OA 5'-\-e.. ~or pv~e... t>.1IA ~I""prt~ 'G-VGNt. PV'3t-b~v..~ "-t O})~'\. Put-b(..tl-wt..l\ ~vr "'" t-ot~\ ~ II yY\1v\.Vt-C.~ o..,J.... b Se,.c:.,t>~J...>" t.VGoIl I"'"~A. tA.r-y. \,c.I~+l.-1" "",,,,"'-oS 6-\:,!1Lo.-l DI"t?--"''''' ,"o\()-r e...~ e..... 1.-4-·H" ..... 1Ir)'-y ~ur-~~r..s"" oN'jJ\v-Ye..". wp.:"u-t"-t.A. "'\ULI'~ MA >~S4.ye.tJ.. "~u.;\. ~i...rc~tlv t . P~I'"""'Me..'h: .. r~ ...... e,,/"~ ('()P;'GorA (Jff.-Over'" pv ...... p ~~ S(.o.G-C,...t. Le..~·+-.s..t-e, 6.+-~ttiO D ~ k tAl s {b I/ee.kcf d,i / t; S-~ , 12e.:T . tUveD 011' ILllIS" ~(>'rl+ ",-,.,...S ~{fw......, '-9 .. !r y , eA.VI.A.(J 0-bis(){')":.Ab/~ (5o;!w trJ14..-S lASed l-() folkc-t ~ Sa~f-4-, '---_______ ---IIDo not touch this cell (SheetName) White Mesa Mill Field Dati! Worksheet for Groundwater .A 20f2 capturx COIOPATI"< wlnl~,...,.,w-'\INCTIDNALITY i ! I 1 = MIII· ... rou~atet Discharge Permit Groundwater'Monltoring Quality Assurance Plan (QAPJ Date: 03/22/2010 Rev. 6 , ATTACHMENT 1 OENISO.}) J WHITE MESA URANIUM. MiLL Attachment 1 ,'"j' Sec instruction t MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 \ $ t ex !)()..r h.c /\Ii \-cc..\ '= a.o , \ Location (well name):I-I..Lr-'W::.=.N.:.... ...... 6r.-. _______ --' Sampler Name and initials: Date and Time for Purgin~ 1 /.t: b / :f.,.O I \ and Sampling (if different) Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) Sampling Event Q ye..r ke.i \Y All ~r-~til Prevo Well Sampled in Sampling Event IT vJ IV' - \ S pH Buffer 7.0 1-.[ :Z-LL.-",Q~_----J pH Buffer 4.0 14.0 Specific Conductance 1-1 .....19.....1'11.,;;191--__ -11 J,lMHOS/ cm Well Depth(O.Olft): 1-1 ....;.I~~..::;l:' ___ -' Depth to Water Before PurgingJ 7£ t 7;2, Casing Volwne (V) 4" well:1 ~5. '1'2 1(·653h) 3" Well:. 0 . (.367h) Conductance (avg) 1-1 .LoIs .... • ..L7,..efl'--____ --' pH of Water (avg) 6.67 WeJl WalerTemp. (avg) I IH . 19 Redox Potential (Eh)1 3? Y Turbidity! 1(>97 Weather Condo L..1_S_v_""_f..,_'f _________ ... Ext" Amb. Temp. ·C (prior sampling event)1 3 0 '- Time 1 1 Q.5~ I Gal. Purged I i~) I Time Ilj.U> I Gal. Purged I '238 I Conductance I '~:Z9 I pH 16.68 I Conductance 1 1219 I pH 16.7Q I Temp.oC !' .... 17 I Temp.oC !'Y.:*,' I Redox Potential Eh (mV) 1 ;33'3 I Redox Potential Eh (mV) I 33'1 I Turbidity (NTU) 11 D~g: I Turbidity (NTU) I 111.2. I Time IIJ-,Sk I Gal. Purged 1 '165 I Time 1 1 ~1i7 I Gal. Purged I :2 J :J. I Conductance I I~"~ I pH 16.66 I Conductance I 1.576 I pHI 6.67 I Temp.oC I 14.1C? I Temp.oC 1'4 .. 20 I Redox Potential Eh (mV) I 335 I Redox Potential Eh (mV) I ;S36 I Turbidity (NTU) 1-111 0 I Turbidity (NTU) Illl~ I White Mesa Mill Field Oatil Worksheet for Groundwater A . 10f2 capturx' COM''''''8LE WITH/"'"_b-fUNCTIONALITV Mill -.GroUt,:~ater Oischilrge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring QUillity Assurance Plan (QAP) Volume of Water Purged I 27J. Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I ...L.1-t..J __ --, gallon(s) Time to evacuate two casing volumes (2V) T'=2V/Q= I ~ I L1.I(' Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~1...~AI~/...(.A...L-____ ---I Sample Taken Sample Vol (indicate Filtered Preservative Prcservative Typc of Samplc if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 N\lttients fi 0 lOOml 0 (if H2SO4 J8I Heavy Metals 0 0 250m! 0 0 HN03 0 All Other Non Radiologies 0 0 250ml 0 0 NoPreserv. 0 Gross Alpha 0 0 1,OOOml 0 0 HN03 0 Other (specify) 1m 0 Sample volume 0 tiD 0 L.j;..\ ~ r-11''A.e. Ifprcscrvativc is used, specifY Type and Quantity of Preservative: ! I ~ ~ See instruction :Comment Ar-hv~ Cll/'v >I·h: ... A+ IJ.IS. &~,..A o..~ e.yv....t\.. S. CA.. Si~e.. (!or fv~c.-~~ .sevv\,f'\\~ e..v~t. fu~e.. bc...-5o."" c..\-13-111. fUMpeA \,.A.Ic..\i for \6 M)v\.V~-c..>. 5~""fle....> we,:--e. tcd:"e.v'\. ,d-I;'> 7. fc).I"'C/.vV\e...~U'.s V'CA"C... +'C\.UA. ~I"OMt ~ve.r-pU..,A.p;~ ~; dj. £~a ... \-. L.l.,~+ ~i te... C<-+ \.3\:;l. 1......-_______ ....11 Do not touch this cell (SheetName) White Mesa Mill N 0 0 0 0 0 S Field Data Worksheet for Groundwater .A 20f2 capturx-CO"'~ATI.LE W1TH/""HU'W--.UHCTlDH",ITY Mill', Gr~nd~eler Discharge Permit ') GrIlundwat~r Monitoring Quality Assurance Plin (QAP) Date: 03/22/2010 Rev. 6 i ! l . ~ OENISOJ) ~: ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 "." See iLl~truclioJl I MIN!S FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I, 'i t DVAet""I=e..r Ali rte==t" .1.01\ Location (well name):I-1 :r ......... Wr..:o.LN:--_71--_______ --' Sampler Name nnd initials: Date and Time for Pu[gin~LEI ;§C'ili·r~'i=---___ ~ 1/~6,t~t\ Well Purging Equip Used: 00 pump o@ bailer Sampling Event I C.h?Ct.,(: b~<r\t #.+ O\iLI pH Buffer 7.0 1 ...... 7...,. ....... ""'""0 __ ---' Specific Conductance ... 1 q.J..;q~q ___ -II,",MHOSI em Depth to Water Before Purgin~ gq. 5& Conductance (avg) 1 .... .30e:::..r0o~ _____ -1 and Sampling (if different) I! 2 71 20 I l Well Pump (if other than Bennet) I Gr-qA.A"p" Prevo Well Sampled in Sampling Event I T \,J.AI -Y pH Buffer 4.0 y.Q Well Depth(O.Olft): II.....I.I.IO~5=-__ -I Casing Volume (V) pH of Water (avg) 4" Well:~(.653h) 3" Woll:~(.367h) 7.~.s Well Water Temp. favg) I 5. 7"3 Redox Potential (Eh)Il.-'&=....S ..... b_-"' Turbidityl 1 Q. '1 Weather Condo ... I S_"_v_V\_"'_Y_" _______ -1 Ext'l Amb. Temp. 'C (prior sampling event)I;}.~ "" Time IDqY I I Gal. Purged I fl I Time I I Gal. Purged I I Conductance 1312 I pH 17~?5 I Conductance I I pH I I Temp.oC 15,73 I Temp. "C I I Redox Potential Eh (mV) 1 ;ajih I Redox Potential Eh (mV) I I Turbidity (NTU) 110,1-I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI 1 Temp. "C I I Temp. "C I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater .A 10f2 capturx' CO" .... TI.L. W'TH/,""U'U'ri>--FU~CTlO"'''L'TY Mill-Groundwater Discharge Pl!t'mit G~oundWi,lter Monitoring Quality Assurance Plan (OAPI Date: 03/22/2010 Rev. 6 Volume of Water Purged I I.. ...:q:.Lr..:~:.o5,--__ -.J Pumping Rate Calculation Flow Rate (Q). in gpm. S/60 = ,-I ...... l ...... ]~ __ -J gallon($) Time to evacuate two casing volumes (2V) T=2V/Q= I~ I 1./g Number of casing volumes evacuated (if other than two) 1.917 I Q.35 If well evacuated to dryness. number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lnb~L£....#.:....AL:lL....-_____ .....J Sample Taken Sample Vol (indicate Filtered Preservative Preservative ! I = :: Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) t.:. ~ 1,,1" • .!e.. y Cl ~ 0 0 0 iii if other than as N specified below) 0 3,,40 ml 0 100 ml 0 250ml 0 250ml 0 1,000 ml 0 Sample volume Added Y N Type y Cl 0 HCL 0 0 IS H2SO4 1iD 0 0 HN03 0 0 0 No Preserv. 0 0 0 HN03 0 0 6!l 0 Ifprcscrvative is used, specifY Type und Quantity of Pl'esen'ative: ~ . / See instruction =Comment Art',vtJ.. o"'-.$i h .. v-'\--r;Cf·J.O~ G~r"'·, ...... 0..";'" '?-Y()..A..S. ~r-l.>~t ft>.r pury.. o...,J..-~"-""'''\Ir'\.-~ e.vt-Jd. fJv~e-b~yJ\. (). t-OCIY,I o..I\J.. t"'c..~ ~()r 33 s..e.WI'~r We..\\ r()..~ ~f"y£ l.Jv-.te.r U/(..> t:..\l.jl,i' H",te'v~l,..ev~ pU~ /...e-{:t site ~-\-(!)'lS3 .. C-C7{) I~ ~,c-..(",()"f"'\e.-ru> .~C"C:>""'" Collier PU"v...PI:3 ..s~£..d" A r-,.; v e.J-.. O.,A.. .s. " 4 ~ a... +-03 30 S~""'f'Ie...s 1,...0-1 e..r~ U;llfe.'-teJ-c..+-og36. '--_______ ---1100 not touch this cell (SheelName) White Mesa Mill N 0 0 0 0 0 til Field Data Worksheet for Groundwater A 2 of2 capturx· <OM.ATIB.E WITH/"IfOU'rir-.IIHCTlONALIn Mill· Grou7,dwaterDischarge Permit Date: 03/22/2010 Rev. 6 GrQUndWi :er MonitQring Quality Assurance Plan (OAP) Attachment 1 OENISO,}) ~, MINES ATTACHMENT 1 WHITE MESA URANIUM MiLL <t See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I I£t Qvtl:d:"r NIl·eM,==: ~')\I Sampler Name Location (well name):1 T I.J AI-7 B.. and initials: I {2Qo;t t ·,,1\. Be\"""'t-I"'" / 6 e Date and Time for Purgingj .... .:..I-..,.......d. .... p<...._-\ .... \ ____ -' !/J.6/~oll Well Purging"E"quip Used:~pump o@ bailer Sampling Event I QVQ.t tu\y ,.vi ttl>..h~ ... 1 pH Buffer 7.0 1L-7"","b;w,Q~ __ --I Specific Conductance 1-1 9....J....&9 -,Q ___ .....J1 ",MHOS/ em Depth to Water Before Purgind N /A Conductance (avg) I:S and Sampling (if different) Well Pump (if other than BeMet) Prevo Well Sampled in Sampling Event I Tj,J N-L1 pH Buffer 4.0 II1 .. D Well Depth(O.O 1 ft): L..I ~JV:....t'/...&;AI.--_--1 Casing Volume (V) pH ofWnter (avg) 4" Well:~(.653h) 3" Wcll:~(.367h) Well Water Temp. (avg) I 4.8;; Redox Potential (Eh)1 '2.86 Turbidityl .2 .3 Weather Condo Ext'l Amb. Temp. "C{prlor sampling event) 11 "c:. I Time I OCtal:( I Gal. Purged I 15D I Time I I Gal. Purged I I ! I Conductance I 15 I pH 1-1.13 I Conductance I I pHI I " ~ Temp.oC I 1.1. 9 $ I Temp.oC I I Redox Potential Eh (mV) t ~~tl I Redox Potential Eh (mV) 1 I Turbidity (NTIJ) 1~.3 I Turbidity (NTU) I I Time I 1 Gal. Purged I I Time I I GaL Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Me$i Mill Field Oatil Worksheet for Groundwater ..A 10f2 capturX" to,",'''TIDLE WITH/'".....,.n,--ruNCTlONA.,TV Mfll • GrouJdwater Discharge Permit Date; 03/22/2010 Rev. 6 Groundwater' MonitorIng Quality Assurance Plan (QAP) ! I Volume of Water Purged L..1..J,.1._!;>:I,oQ'--__ ....J gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. 5/60 = L-! ..&..1 J-'---__ --' Time to evacuate two casing volumes (2V) T=2V/Q= I /vIA I N umber of casing volumes evacuated (if other than two) INIA If well evacuated to dryness, number of gallons evacuated ! AI/A Name of Certified Analytical Laboratory jfOther Th3..U Energy LabfL~ALILLILA!-____ ...J Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified bclow) Y N Type VOCs CJ CJ 3x40 mt CJ 0 HCL Nutrients g 0 LOO ml 0 IS H2SO4 Heavy Metals 0 0 250 m1 0 0 HN03 All Other Non Radiologies 0 0 250 mJ 0 0 No Preserv. Gross Alpha 0 0 1,000 ml 0 0 HN03 Other (specify) ~ 0 Sample volume 0 ~ Preservative Added y N CJ 0 12§ 0 0 0 0 0 0 0 0 .J8. C \.... l"t".,)ll.. If preservative is used, specity Type tlnd Qunntityor Preservative: ~ See instruction ~Comment Ar-r-'. vt-rJ.. OJ\. Sit!. c.. ~ 0&50. bf)..fh./ ...... o..""~ e..ye..01\ S. pr-G-.sf.1l\~ ~w I"i~.s:",-~ t-. S to..d~J.. i"1{\>tl\-e.. cd-o 85f... f'VMru\ 56 G~1\{1~ of Ac"J... \,..<Jc...\e..r) 50 6~d\V~ eN 5ol).plo.~ Sf) 6~IID"'S ".f' 'c).'I. v-J< .... ~r!.r. ~'V\o>A. .. (., ~~eJ.. tLt CI'lV'1 ~ ~~CA..~PI~ '-""'e-re. "~"" c..ol'",d~vl.J (..(..(Jl ~il" ~+-DGIO. L..-_______ .......Jloo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater .A 2of2 capturx to ... ATl8LE WITH./"'~k-'UHCTlONAL'TY MifI-Gr~ur16wateilt1ischarge Permit ') • Groundwater Moni'toring Quality Assurance Plan (ClAP) Date: 03/22/2010 Rev. 6 ATTACHMENT 1 IOENISO,J). J WHITE MESA URANIUM MILL Attachment 1 :... See i05!IUClion ..l MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I I ~'( Q u..o..c r( r N ;t rl.4h:. ~ 0 II Location (well name): .... I----.;T:...;W:-;..N;:..---.:o.8'L-_______ .... Sampler Name and initials: 1 ~"I11:(, Hofl,J"*/rH Date and Time for Purgingj l/J..."1/~t:J I I Well Purging Equip Used: [!]pump o@ bailer Sampling Event pH Buffer 7.0 Specific Conductance! .... __ "l'\ ...... 5-'--_--'IIlMHOSI em Depth to Water Before Purgin~ (., \ ,lob Conductance (avg) and Sampling (if different) I I /J .ill;1 I ( Well Pump (if other than Bennet) bcu!)q\ ~b :;' Prevo Well Sampled in Sampling Event L..1_1tI_/_/~ _____ ----I pH Buffer 4.0 "1 .0 Well Depth(O.Olft): Casing Volume (V) 4lt well:j SLi .73 1(·653h) 3" W cll:,---,.:J~_-,. (.367h) pH of Water (avg) Well Waler Temp. (nvg) I /"1 .;17 Redox Potential (Eh)1 %4 Turbidityl 6595 Weather Condo Ext'l Amb, Temp. ac (prior sampling event)1 0 (t <. Time I i o::J ~ I Gal. Purged I ~O(.. I Time I 10 ]'5 I Gal. Purged I ')~;? I Conductance I :J.~~ I I pH I b.t(D I Conductance I ~j O~ I pHI b .M3 I Temp. DC t IY .IS I Temp. DC I \y .~ I Redox Potential Eh (m V) t ;as, I Redox Potcntial Eh (mV) I ~bc'.o I Turbidity (NTU) l i(b '4 I Turbidity (NTU) l \ O~ :2-I Time I \O~~ I Gal. Purged 11>1:\.0 I Time 110;2..1 I Gal. Purged I "3 51 I Conductance I ~Jqs I pH I b ~'3 I Conductance I ~~7~ I pH I Co. ~1 I Temp. DC I l; 3'l. I Temp. DC I 1'1 3S I Rcdox Potential Eh (mV) I ~b.l I Redox Potential Eh (mV) I ;:U;~ I Turbidity (NTU) I ~'I I Turbidity (NTU) I ~1 .' I White Mesa Mill Field Dilta Worksheet for Groundwater A 10f2 capturx' <D"~"T1nE W"H....--....... iV--'UNCTlDNAlITY MiII-Grounawate~l1i5charg~ Permit ) • GroundV:ater Monitoring Quality Assurance Plan IQAPI Date: 03/22/2010 Rev. 6 Volume of Water Purged I 3~ O . <§ gallon(s) Pumping Rate Calculntion Flow Rate (Q), in gpm. S/60 = I )1 Time to evacuate two casing volumes (2V) T;:2V/Q= I ~ I 6.4'3 Number of casing volumes evacunted (if other than two) Ifwell evacuated to dryness, number of gallons evacuated I '3~O.g Name of Certified Analytical Laboratory jfOther Than Energy Lab! .... _N_/-!~ _____ --, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs Cl CJ 3x40ml CJ Cl HCL Cl 0 Nutrients Ell 0 lOOmi Cl ~ H2SO4 61 Cl Heavy Metals 0 0 250 mI 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 D i,OOOml 0 0 HND3 0 0 Other (specify) ~ 0 Sample volume 0 IE 0 riI ("h\or-;,h Ifprc!lcrvntivc is used, specify Type and Quantity of Preserva live: § ~ See instruction I:, ~Conunent 1-..-_______ --IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater .A 20f2 capturx' COMPATIBlE WfTH~HU'~FUNC1IONAL1TY J .. J , • Mill • GJ'oundwClter Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan lQAP) ATTACHMENT 1 "ENISO..!)~ ~ ; WHITE MESA URANIUM MILL Attachment 1 :).' See ins.ruction M INES FIELD DATA WORKSHEET FOR CROUND WATER --- Description of Sampling Event: 1 Ie:.. t Q II L\ r tl.el' tI d -Ch k L 1.0 II Sampler Name Location (well name):1 'f w AI ~ 9 and initials; Date and Time for Pllrgin~ 0 I 1.3 11 -70 1 \ Well Purging Equip Used:~pump o@ bailer Sampling Event I Q ut'"' -te..r-\ 'I IV'. kv..\d pH Buffer 7.0 1-1 7-.:.....:... • .=O'---_----J Specific ConductanceI-I _Cf.t..9 ..... 9...1-__ ......I1 ""MHOS! em Depth to Water Before PurgingJ 63. g \ Conductance (avg) 1'-...:·;;2.;.......0<.."_4 ..... 6«-___ --1 and Sampling (if different) , Q¢-./D 1/2-0 I \ WeUPump(ifotherthanBennet) I (;tv M(1bS Prevo Well Sampled in Sampling Event I T WAI -, 7 pH Buffer 4.0 , t..!. Q Well Depth(O.Olft): '-, -9&..,7'------' Casing Volume (V) pH of Water (avg) 4" Well:~(.653h) 3" Wcll:u.z.==:=J(.367h) 6 .55 Well Water Temp. (avg) 1 13.) I Redox Potential (Eh) I :3, 4 Turbidity 1 10 I Weather Condo Ext'l Amb. Temp. ac (prior sampling event) 1 I U c.. Time I I DJ j.. I GaL. Purged I 17 I Time I I Gal. Purged I I Conductance 12~Y~ I pH I 6tSS I Conductance I I pHI I Temp.oC 111, \ I I Temp.oC I I Redox Potential Eh (mV) I :3 1 Y I Redox Potential Eh (mV) I I Turbidity (NTU) I 10. I I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater ~ 10f2 capturx ~O".ATIIU WIT~"""",",rir-PUNCTIONALITY Mlir • Grbundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater 'Monitorlng Quality Assurance Plan (QAP) ! Volume of Water Purged I ~O, 0 , Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ..... 1 ..L.1 7-1--__ --1 gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q"" 14:3S!'r I ~ .. SLi Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 1 '2-0.0 6 I Name of Certified Analytical Laboratory if Other Than Energy Labf .... -".x~6~A~ ____ --l Sample Taken Sample Vol (indicate Filtered Preservative Preservative Typc of Samplc if other than as Added y N specified below) y N Type Y N VOCs Cl 0 3x40 m1 Cl [J HCL 0 0 Nutrients Q! 0 100 mt 0 6!1 H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specifY) 1&1 0 Sample volume 0 ijl 0 5- ~t.... i£i r ', ~r" Ifprcscrvativc is used. specity Type and Quanllty of Preservative: See instruction aComment AC"f'.ve.J.. of'-,Sit!... a .. J Oqy'f. Go.t'~I"'" ctMl ~yfM\, 5. p(',,>c.-,-.~ ~~r-f v l'3e..-'I.~ >~,M~'\~ e..ve,,,,,-t. Pu~e-b~o.J\ t{t lOlL fvM.{) 1/:4.J\. ~f/,{' eJ./\.c.. Mi.Allte.--~Il-~ 1& ,S t-~o;vi. 5 . W cAl n ... A J.. toy, P ",r-e...M.(..-·t U-.> W"r e... +~ '? M.. .pro 01\1\.. \-~ t,... ~ V e.t P uMf, ~ \?i c,(.pt .s~ l-e.-+. /.-(.. f t-Sa!. ~ t-I 0 ~4. Arr·,IIc.A. 1>"-~, h-o...\-o~o'Z J f!.ytl..I\. S. £\.Nl b.:..t""tI. p"~s.e",·t ~tA.MpIU we,r't-h:~.""f!.,"'" o..t 080Ci. Ol!.-p~'" ~o w~t~ w~ G3.~I, L-~C; '" 5. ~t.r ~+-ortll. I I 1....-_______ -1100 not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater .A 2 of2 capturx' COMMTlaU ... 'TH.,..._tV--fUNCTlONAL'H , . Mill "J3rounlwater Discharge Permit Date: 03/22/2010 Rev. ~ 6roundwater Monitoring Quality Assurance Plan lOA?) ATIACHMENT I Attachment 1 OENISO..})~ J ~ WHITE MESA URANIUM MILL . ');; See iDSfnlClion M INES I FIELD DATA WORKSHEET FOR GROUl\'D WATER ---------~ Description of Sampling Evcnt: list C{vo....de.f' Ah ~r-tc-~k ~O\\ Sampler Name Location (well name):1 T W A! -I 0 and initials: G lbr61\: ecJt1(,.('" Date and Time for Purginm I! 261 ~ 0 I \ and Sampling (if different) I 1/27/20 I \ Wen Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) I G tVM ~6S Sampling Event I G v4.r r t.c\ y AI, ~ ~l eJ Prevo Well Sampled in Sampling Event I 'J tJ AI ~ 6 pH Buffer 7.0 1 .... 7,~( 0 ___ --' pH Buffer 4.0 4·0 Specific Conductaneel"'--1q~9 ..... q..o...-__ ...... IIJMHOSI em Well Depth(O.Olft): 1L--ll,::::,D_S=--_--' Depth to Water Before Purgin~ g1-. Y 7 Casing Volume (V) 4" well:1 tb,7 0 /(.653h) 3" Well:. _ .(.367h) Conductance (avg) 11o...=:;:J'~L1-=3~Y-L-.. ___ --J pH of Water (avg) ;?I O Well Water Temp. (avg) I I Y. 03 Redox Potential (Eh)1 y q ~ Turbidity I '3 q o. '3 Weather Condo Ext'l Amb. Temp. DC (prior sampling event) I 3 ()i:-I I Time I IL1 tjO I Gal. Purged I '1 I Time I I Gal. Purged I I Conductance 134 J,l..l I pH 13 ~1 0 I Conductance 1 I pH 1 I Temp.oC I ly,QJ, I Temp.oC I I Redox Potential Eh (mV) I H 9 b I Redox Potential Eh (mY) I I Turbidity (NTU) I 3CJO, 3 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I f Turbidity (NTU) I I Turbidity (NTlJ) I I White Mesa Mill Field Data Worksheet for Groundwater .A 10f2 capturx-COMPATilLE WITH,/"'-UU'b-FUNCTIONAlIYY MiII-Grou ndwiltl!f DiScharge Permit ) Date: 03/22/2010 Rev. 6 6roundwater Monitoring Quality Assurance Plan IQAP) Volume of Water Purged 1 ')...0. 'l' gallon(s) Pumping Rate Calculation Flow Rate (Q). in gpm. Time to evacuate two casing volumes (2V) S/60;:: ,-I --.:.-1 7 ____ ----' T=2V/Q=I~ IL73 Number of casing volumes evacuated (if other than two) !L YA Ifwell evacuated to dryness, number of gallons evacuated ! ~Of ql Name of Certified Analytical Laboratory if Other Than Energy Lab~L...c...N:...LI.!...A1--____ ---l Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Samplc if other than as Added y N specified below) Y N Type y N 'lacs 0 0 3x40 m! 0 0 HCL 0 0 Nutrients g 0 lOOml 0 R!':I H2SO4 jil 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All OLher Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 m1 0 0 HN03 0 0 Other (specify) I:l 0 Sample volume 0 ~-0 3 c..v..lc.r-i ~e. Ifprcscrvativc is u!\cd, spccify Type and Quantity of Preservative: ~ I . :: i :Comment See instruction Arr-,v'c:.{l Oil'-Si+e. 0.:+ ILilo. O~rt-,A. (l...J4l f?.y&<.oA $. 0 ...... >:-ift!.. ~or PU';,5e.. D4Aot $o.Mfl ·,~ e.ve..-..t, PV'3f.. b~"" A-+ IY;J.4. rv~~ v./e.I\ ~CN-\ W'-IIA..V·\e.. -:).S $l.{'-(} ... Js w~\1 r-e-,of\. rJ..r-y~ f .... rec..~(....t~ vvC-('f.. ~,,~e'(' ~:r-c1..v\, (!)vU" P()WlPI~ ~, e-lvt .>Lu.c..l. t.. c,.°f t So it '-c--:t P14 g: Ar-I"ve.-J... ~ ~l-tc. 0.-+ Og£:,CJ . .5o..-...pleJ v..>~L-1!..c>lIcde..A ~+ 68S!:> , '-_______ ----lloo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater A 20f2 capturx COM,ATlB •• WIT~../'-_"'~.IINCTIONAUTY . -~iII-Grou~Jwate~ ~SCh8rge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ()ENI50,!)~ ~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~' See inslrucliOil MINIS . -' FIELD DATA WORKSHEET FOR GROUND WATER D~criptionofSa~l~g~ent ~11~$~'~~=~~v~~~r~~~~~_~~i~~~~~~~(~<~~=O~\~\~~~~~~~~~~~~ Sampler Name Location (well name):IL-..L't...Jo1d=.44'II'----,-I l=---______ ---J and initials: 6 a.r6o\. p"\r"'e.-,-I up Date and Time for Purgin~ I 1 ';).]1 {kfJ l\ and Sampling (if different) Well Purging Equip Used:[g]pumpo@ bailer Well Pump (if other than Bennet) I GrVA(l.£o~ Sampling Event I 0." M } <r I 'I ,v; tc p. Ii] Prev. Wen Sampled in Sampling Event I X \J AI -\ t> pH Buffer 7.0 1-17--'--"-."""0 __ --1 Specific Conductance II-4~g .... '1_~~ ..... I ~MHOSI em Depth to Water Before PlIfgin~ 69. It '3 Conductance (avg) 1-1 .oz:2.",-7~'l_i.:j ..... · ____ ...... pH Buffer 4.0 Well Depth(O.OJft): ..... 1 """,I y~;l~----, Casing Volume (V) pH of Water (a"g) 4" Wel1:~(.(;53h) 3" Well:~(.367h) Well Water Temp. (avg) 1 t Li. ?.s Redox Potential fEh) 13;' at TurbidityllA. y Weather Cond. I L-S __ v_~_~~y ______________ -....I Ext" Amb. Temp. ·C (prior sampling event) 1 00'" Time 1 c'i ftb.8 I Gal. Purged I ').'3g I Time I (!?ifSlf I Gal. Purged I -;).55 I Conductance I ~71:J. 1 pH I 6. ;l,'l I Conductance I ~,~~ I pH I 6 .. :lCJ I Temp.oC II'1 y27 I Temp.oC 114,;16 I Redox Potential Eh (mV) I ~"3 1 Redox Potential Eh (mV) I 360 I Turbidity (NTU) 116 0 1 Turbidity (NTU) 111,.3 J Time l oqoQ I Gal. Purged 1 ').7;1. I Time IOgO\ I Gal. Purged I 2~'f I Conductance 1.l:2g3 I pH I be ;]..9' I Conductance 1 ~7gg I pH 16.$0 I Temp.oC I IY·l:S I Temp.oC I !L1 ,),Y I Redox Potential Eh (mV) 13.5 Cf I Redox Potential Eh (mV) I 359 I Turbidity (NTU) 1 1~16 I Turbidity (NTU) 116.. g I White Mesa Mill Field Data Worksheet for Groundwater A 10f2 capturx CONPATiDLE W'TH~ ...... rir--,uIICT,oH~L'n ,~ MiII-Grourrdwater Discharge Permit ) ) Date: 03/22/2010 Rev. 6 , Groun'dwater MOnitoring Quality Assurance Plan (OAP) Volume of Water Purged .... 1..z:l=::.:8.l..9;;.,.· __ ----J Pumping Rate Calculation Flow Rate (Q), in gpm, S/60 = L..I -L\ ..L7 __ -.I gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I ~ 15.55 Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated I.'&:/A Name of Certified Analytical Laboratory if Other Than Energy Lab~ ........ M---,I-,A~ ____ ----J Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y N VOCs Cl Cl 3x40 ml Cl Cl HCL 0 Cl Nutrients .t:i 0 lOOml Cl ~ H2SO4 ~ 0 Heavy Metals 0 0 250m} 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 NoPreserv, 0 0 Gross Alpha 0 0 I,OOOrnl 0 0 HN03 0 0 Other (specifY) ~ 0 Sample volume 0 fi'1 0 m ~ I a :i l IA\ O'r-I rJle IfprcseTYlltivc is used, specifY Type Ilnd Quantity of Preservative: i See instruction :SComment A rr.ve..&l tJ'I'v >, h ... 0.+ Oql~. G().rt-;.A-",-,..J.-eyt\. ..... s. C?",-~i +e.. .~o-T" pv~..5e-o..{'vtA .5Ck-,-A..Pl l ~ e.ve...A.+' PVl'-.£l,('" bG.h~oA. ~,'" O~L-j4. Pvr-,be,..}. \..V~~I eo!""" A -\,,\--p,l oY 17 """",A.V ,t-e-.5. Lo/.:...+t.r-wit.$ c:..\~r t\""rov~"'-~v* pv~e. . .s~p l e....s \A/c!../"e ·h; ... \'"-.:." ~t Oqt>L P~r-b-Ac:..~e.t-.s we-n-(..op.tJ., ~('C!""" ()VU"PV",,{J I~ +=ie..IA Slr'l.u... .... ~ L-d't $1 tL ",-'1- £'(.O\g ....... _______ --1IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater .A 2of2 capturx COMPATIBLE WIT~./'-~W--fUHCTIONALITY Mill· Jroul,dwaler Discharge Permit ") Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 Auaclunent 1 i)ENI$O ..1)~ ~; WHITE MESA URANIUM MILL ).' See insUUQlion ,MINES FIELD DATA WORKSHEET FOR GROUND WATER L ___ ~ .. ~_._ ... ~ ..... ___ ..-..... ~ Description of Sampling Event: ! 15 r ().. we... ('-t~r .&' t r-t'= • Go ;l ¢ 1\ Sampler Name Location (well name):1 r biN -I, B and initials: (2 e tt i "" pc..,\ Me." / 6 P Date and Time for Purgilld J /.262 .26 , I • Well Purging Equip Used:!1Dpump o@ bailer pH Buffer 7.0 L...! 7~t ~O __ ---I Specific ConductanceI1--&9....:Q...l'i ___ ....J1 ).1MHOSI em Depth to Water Before Purgin~ Al'LA Conductance (avg) ... 1 .:;;,;.:5:..-_____ ---1 and Sampling (if different) Well Pump (if other than Bennet) pH Buffer 4.0 Well Depth(O.O 1ft): .... 1 -Io/V..:;...z.../'-I.1 __ -J Casing Volume (V) 4" WcU:~(.653h) 3" Wcll:~(.367h) pH of Water (avg) '=1-) t? WeJl Water Temp. (avg) I E,5S Redox Potential (Eh) I 4 'is TurbidityL-1 L.' e2,--_~ Weather Condo Ext'l Amb. Temp. ac (prior sampling event) I 0 c> c:. Time 10801-;, I Gal. Purged 1 I~Q I Time I I Gal. Purged I I Conductance I 7,5 I pH ! L-J, jQ I Conductance I I pHI I Temp. cC I 5, ~~ I Temp.oC I I Redox Potential Eh (mV) I ~~~ I Redox Potential Eh (m V) I I Turbidity (NTU) I . 2: I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Me$a Mill Field Data Worksheet for Groundwater ~ 10F2 capturx CO"'~o\T"U Wll~~HU',p---.U .. CTloNALln Mill • Ground~ater Olscharge Pennit ) -Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged '-'-+-=lll=() __ ----I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 =;; 1-' ...... 1...:.7 __ ---' Time to evacuate two casing volumes (2V) T = 2V1Q =, ;VI A 1 Number of casing volumes evacuated (if other than two) ] f well evacuated to dryness, number of gallons evacuated , NIA I NIA Name of Certified Analytical Laboratory if Other Than Energy LabtL..-.£...tV:....+,.I....i,A...1..... ____ --J Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample jf other than as y N specified below) Y N Type VOCs [J 0 3x40 mI 0 0 HCL Nutrients 18' 0 100 ml 0 ~ H2SO4 Heavy Metals 0 0 250 ml 0 0 HN03 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. Gross Alpha 0 0 1,000 ml 0 0 HN03 Other (specify) ~ 0 Sample volume 0 ~ Date: 03/22/2010 Rev. 6 Preservative Added y N 0 0 Pif 0 0 0 0 0 0 0 0 £1 Lt,...l CIf':' (~ L Ifprcservativc is used, specify Type and Quantity of PreservatlVe: ~ See instruction aComment A 11"'\ V't.-'CI\. ClI/V > i t c.. 0... +-e; 7 L-l o· (" ..... to r ~ ,/\.. (,,, V'4~ (L i C ... A 5. P 1 ~s G.I\..... ..\:(10.(-f' 1 j\ S cd e. ... ..5 .rc..~reJ.. n,'\.>~te..-o..'r DiL16. fVMPe-c,l 50 b(..iloM of A,{.;.if.. vv ..... te..r1 f>o t>AllcAS' C'f.-SCO-f' \,....'o...t-er ()"Jl.fJ\. So G~ll{),I\.s 0 f D.:C. VV'e..+u . $a..Mf\t...s C"M"-pQ..r-A.M~\-2.3'~ 't..,e.re... ,t-e..~ c...r 0'730SIl.-l-~+ $d·f-~·Y(7l?15. 1....-_______ -IIDo not touch this cell (SheetName) White Mesa Mill Field Oata Worksheet for Groundwater A 2 of2 capturx' COMP.T.OL! W.TH/'-_~fUNtTIO".~.'rV " Mill, Grol1:ldwat!:~ischarge Permit ') Groundwater Mo~toring Quality Assurance Plan (QAPI ) Date: 03/22/2010 Rev. 6 I ! I ATTACHMENT 1 OENISO.}) i ; WHITE MESA URANIUM MILL Attachment I • j " See instruction M INES FIELD DATA WORKSHEET FOR GROUND WATER --- Description of Sampling Event: I l :e I: <3lw;,r-t~r Ali t r-e-h:< :20 ' \ Sampler Name Location (well nome):1 T W tJ -I;L and initials: 1 ...... 6 ....... ,;.:...t.L.,jt,ucA"--IeM'4 ... \a.<:n~"'....,..1'-4-1---""6 ..... P __ -1 Date and Time for Pl1rgin~,-.... I_~..,.'J.5=-~--'-1"1--___ -' Wen Purging Equip Used: 00 pump o@ bailer SamptingEvent 1 Q VII-!"tuly All l-cp..h: ... 1 pH Buffer 7.0 1L-/.....!-c... """O~_-.J Specific ConduetanccJ....1 q...!...l.9....&'l ___ ...... 1 "MHOS! em Depth to Water Before Purgin~ity .4D Conductance (avg) ...... 1 ""2-:::...Y ..... 't....l..4.I ____ ---1 and Sampling (if different) 1 I 12, 1.2 at! Well Pump (if other than Bennet) 1 G t l<'l"4r04 Prevo Well Sampled in Sampling Event L,.I ",-r--,v=-,,t/~'-,-l ___ ~ pH B\lffcr 4.0 L4 .Q Well Depth(O.Olft): 1...1 .1.JllLLoo"~ __ ",J Casing Volume (V) 4" Well:~(.653h) 3" Wc1J :~(.367h) pH of Water (avg) J....I ""6..&.t-t7_:3.L-___ --....I Well Water Temp. (avg) II Y. 13 Redox Potential (Eh)1 213 Turbidity I .58 :2 .:;l. Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)1 y " " Time I 1.3<23 1 Gal. Purged 15 t..j 1 Time 113()5 1 Gal. Purged I &8 I Conductance I ~5;).~ I pH I 6 -67 1 Conductance I :J-L.J. s.,S 1 pH 16.7 2 I Temp. "C 1 14:1. D7~ Temp.oC I IY.j e} I Redox Potential Ell (mV) 1220 I Redox Potential Eh (mV) 13' 7.$ I Turbidity (NTU) 1176 '1 I Turbidity (NIU) 1 5'1f<. ~ 1 Time II ~O b. " I Gal. Purged 1 ~5 I Time I I Gal. Purged I I Conductance 1:1.~I..~ I pH I 6 rifO I Conductance I I pHI I Temp.oC 1 I t.j-l t) I Temp.oC I I Redox Potential Eh (mV) I :kSY I Redox Potential Eh (mV) I I Turbidity (NTU) I ~li:,l:t I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater ~ 1 of2 capturx COM'~TI.L. WITH~HU'tV-ru .. tTlo.AlIn ·' Mill· GrotJndwau.r Discharge Permit Groundwater Monitoring Quality Assuran~e Plan lQAP) Volume of Water Purged I BC1. 76 Pumping Rate Calculation Flow Rate (Q), in gpm. SI60 = ..... 1 ..L,! 7.1--__ --1 gallon(s) Time to evacuate two casing volumes (2V) T = 2V /Q = 1 fIBt17Sr' 1 .5. gO Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L..L.lAl~A!--_____ -I Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified below) y N Type VOCs 0 0 3x40 ml Cl Cl HCL Nutrients ~ 0 lOOml Cl ~ H2SO4 Heavy Metals 0 0 250ml 0 0 HN03 All Other Non Radiologies 0 0 250m! 0 0 No Preserv. Gross Alpha 0 0 1,000 mt 0 0 RN03 Other (specify) Jii 0 Sample volume 0 ~ Date: 03/22/2010 Rev. 6 Preservative Added Y N Cl 0 .~. 0 0 0 0 0 0 0 0 fil (~ (..., t> .... , .-A.,. (fpreservative is l1~cd. !lpccit)r Type and Quantity of Preservative: ! See instruction ~Comment -. Af'f\\/~ CJ./'o.-~i~c.. &<-r 1;t4L1 . (;,(;f-h~ ()..,...A gy~.A~. p("c...seol'-t fo r-pu~e.. ()'rW.. ..sc..,v\fll ~ e;.VCoA t . .p v~e.-vl LJ (..1 \ ~¥ f>-\-0 to... \ CI of .5 M,,'l'I..vfe..> c........A. 1--f $(..(,OA.CA>. Wc..ll rc..~ rAr-y» VVo-+ e.r wcio-.s "-' tA()..r '(... ();eo.~e.... ,-"\,,,-ti-./"Ov,bkc.u+ pv~. Po...n;...M.e..tq s I,..VCAc:.. G-o('1 eJ... ~~vA eJVe.r puM-P I~ .s~a ... t .. t..,-,fl-SIlc.. c...r 1:3\'\" r()("~ $-tj),....('"-t~ c-I-I 3 {!.I \ w .2)a.\M-f>t~ wtd toilet-led ~I )'110. b er>)-H',PC,'r; 1-0 ifCA.lAAf{G t/le(n~ w"'-s .3'4. 7-~ ~Ci~ IE: fJ>l/a ft;:!. I:N /c....,"'.... VA-(~v" ,--_______ --,1 Do not touch this cell (SheetName) White Mesa Mill field Datil Worksheet for Groundwater A 2of2 capturx COMP"'"L! WITtI,;"'L..-u-n:--'UNCTIDNALlfY Mill -Groun}t\vilter rlr$charge Permit ') Date: o3/n/2fll0 Rev. 6 Groundwater Monitoring Quality Assurance Plan (CAP) ATTACHMENT 1 Attachment 1 . OENISOn~ J WHITE MESA URANIUM l\IILL yo S¢e instruclion MINI!S I FIELD DATA WORKSHEET FOR GROUND WATER Description ofSrunpling Event: list a IlQ"t tf.C Nd:C':;: t c. ~ 0)\ Sampler Name Location (well name):1 TW..v~ ,.& and initials: I b4.rr,'(\., P~lr)'I( C Date and Time for Purgin~ I a 1 12./) II ) J and Sampling (if different) Il,a 6/J.{J IJ We]] Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) l&uI\A fa~ Sampling Event IZJWil.f k~ N ilr.J.t... Prevo Well Sampled in Sampling Event I tWA! -8' pH Buffer 7.0 7. () pH Buffer 4.0 Specific Conductance! 911 II!MHOS/cm Well Depth(O.Olft): I lelO. " Depth to Water Before Purgin~ '16 ,( c;h I Casing Volume (V) 4" well:1 11:7 ,9 56 I (.653h) 3" Well: 0 (.367h) '-""'------' Conductance (avg) pH of Water (avg) 1 .... 7...L.&..' 5.L16"---____ ~ Well Water Temp. (avg) 11Y , 60 Redox Potential (Eh)! :;z.::I.I; Turbidity I pi, 6 Weather Condo Ext'l Amb. Temp. ·C {prior sampling event)! 3 l> G Time l'l5.2 I Gal. Purged I 1.3 6 I Time Ill54 I Gal. Purged I 17 a I Conductance I I !!I I pH 17 5 .~ I Conductance 11~6 I pH 1756 I Temp.oC 1 11..4 . '3 I Temp. <>C 1 ..... I(l I Redox Potential Eh (m V) 1 ;lDJ. I Redox Potential Eh (mV) 1 ~28 I Turbidity (NTU) I 11.£; , I Turbidity (NTU) 151., I Time 11 356 I Gal. Purged 1 20'1 I Time 1,,,sll I Gal. Purged I !lgS I Conductance lL1~11 I pH 17 .56 I Conductance I ll!:tQ I pH 17. " I Temp.oC 1 1'=1.11;-I Temp.oC 1''=1 ,79 I Redox Potential Eh (mY) 12=37 I Redox Potential Eh (mV) I ?oM I Turbidity (NTU) 1~C2. i I Turbidity (NTU) 139 •. 2, I White Mesa Mill Field Data Worksheet for Groundwater A lof2 capturx' CD"~~TI8Ll WITH~_n.--rUNtTION~LIH Miil -Groun~ater Oischarge Permit ') Groundwat;r Monitoring Quality Assurance Plan (QAP) Date: 03/22/2010 Rev. 6 Volume of Water Purged 1-1 Q.d-::....5.L.5..L· __ ---l gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ,-I -'-1...(.7 ___ -1 Time to evacuate two casing volumes (2V) T=2V1Q= I~ 15.63 Number of casing volumes evacuated (if other th.1n two) Ifwell evacuated to dryness, number of gallons evacuated 1.155 Name of Certified Analytical Laboratory if Other Than Energy LabL~ ~N.!!...LI.£.Al.-____ -I Sample Taken Sample Vol (indicate Filtered Preservative Prcscrva li vc Typc of Sample if othcrtban as Added y N specified below) Y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 3 0 100 ml 0 (8 H2SO4 1&1 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml 0 0 NoPreserv. 0 0 Gross Alpha 0 0 1,000 mI 0 0 HN03 0 0 Other (specify) l!I 0 Sample volume 0 IBI 0 ~ t. 1,..1 () ,.'1 fA/"'_ Ifpreserviltivc is used, !;pccify Type and Quantity of Preservative: g See instruction ~Comment '--_______ ---lIDo not touch this cell (SheetNarne) White Mesa Mill Field Data Worbheet for Groundwater A . 20f2 capturx' COMPATIeLE WIT~~_W-'UNCTIOH.LITY MIU-Groundwatsr Dlschalge Permit ') GroUndwater Monitoring Quality Assurance Plan (aAPI Date: 03/22/2010 Re". 6 I ! I i J I t .... I ATTACHMENT 1 Attachment 1 'GENISO,.}), J; WHITE MESA URANIUM MILL ' " Sec instruclion . M INtiS i FIELD DATA WORKSHEET FOR GROUND WATER '_.~ ...... _ .. _L~_.L., .. _."";~P.~ Description of Sampling Event: I , s t a lib (" t e. r AI i ... (" Ib t ~ '?-.o ' , Sampler Name Location (well name):1 TLVAI , 13R and initials: G~t1"1 6 Pa\MU I Gj? Date and Time for Purgin~ VJ&.f/2-61 , and Sampling (if different) '---'tY..:..J;t.LA""--__ ~ _ ___' Well Purging Equip Used: 00 pump o@ bailer Sampling Event I ,i lm. tie ely' lIi I:ca..td pH Buffer 7.0 1-1 :z....L.II.I .. O""'-__ ...-J Specific ConductancelL-q...I.;;;JQo..;;9.o.-__ ...... IIlMHOSf em Depth to Water Before Purgin~ N/A Conductance (avg) Well Pump (if other than Bennet) I GrvNl£«.S Prevo Well Sampled in Sampling Event I ILVN-8 pH Buffer 4.0 I Y.D Well Depth(O.Olft): 1 ......... 41Lo( ... "A~ __ -I Casing Volume (V) 4" well:~. (.653h) 3" Well:c=:=a=J(.367h) pH of Water (avg) 7 . :ill Well Water Temp. (avg) I 3 .. G Y Redox Potential (Eh)IL......L.16~1_--' Turbidityl1-' ..... ....,361&.-_-' Weather Condo ... 1_::>_· "'_"'_"'_> _________ ... Ext'l Amb. Temp. ·C (prior sampling event )1 ,c l: Time 1"45 I Gal. Purged I 15Q I Time I I Gal. Purged I I Conductance I 12 "1 I pH 17. 81 I Conductance I I pHI I Temp.oC IXiy I Temp.oC I I Redox Potential Eh (mV) I /61 I Redox Potential Eh (m V) I I Turbidity (NTU) I .6 I Tmbidity (NTU) I I Time I I Gal. Purged I I Time I I GaL Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh em V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater A 10f2 capturx' to"~AT'.LE wITH~_rir-FuNcTIDNALln Mill· Groundwatl!r OIKharge Permit Groundwater Monlltlrmg Quality AsStirance Pl~n ICAPI Date: 03/2U201Q Hey. 6 Volume of Water Purged 1'---11 ... 5"""". p ....... __ -' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60;:; L-I -1.1-£7 __ --' gaUon(s) Time to evacuate two casing volumes (2V) T;:;2V/Q = 1 NIA I Number of casing volumes evacuated (if other than two) I ;VIA AlIA If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL-_AI'L..:;....L.J...:.A-'--____ ......I Sample Taken Sample Vol (indicate Filtered Preservative Preservative ~ I ~ ~ Type of Sample VOCs N'utrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) c.t....l Ot" ,,Ap.- y 0 IX 0 0 0 ;a if other than as N specified below) 0 3x40ml 0 100 ml 0 250ml 0 250ml 0 1,000 ml 0 Sample volume Added y N Type y 0 0 HCL 0 0 J& H2SO4 1m 0 0 HN03 0 0 0 NoPreserv. 0 0 0 HN03 0 I" 0 IS 0 Ifprescrvative is used, spccity Type and Quantity of Preservalive: ~ See instruction S iiConunent Art"p . ./e-J... ~~ $/ t-v 0..+ 11'3.5. 6~n-\-A-c)..~ ey~", s. pre.-,e.A.ot ~£Ir ""'0'\.» \-c!:-.. ~it\.s~t.: .. be.~~,A.. ~t /1;'17. PUIAP(..~ ~17 6G1-lilJ~ of AC,i~ lA/e;..t~r) So 6;;...HcA-.!i "f .s".!t.P """,,tA-te.t-') 5.0 ?~'\1)r'\-5 o~ D.:r; .. wco..t~:-· e IA.s;e.te... ~AA c,;A..~ '';~MP\'".s ......,e.-rt:,..-G."I\~c..t-e.A ~f-\It.-\S. IG"" sHc.. At "~. '--_______ ---"DO not touch this cell (SheetName) White Me~a Min N 0 0 0 0 0 !if Field Data Worksheel for Groundwater .A 2of2 capturx CO"'.ATI.'~ YlllH/'"UU'W-.UNCTlONALITY "":').; 'Gr"unijwilterib~ch"rge Permit Date: O~/22/2010 Rev. Ii • Gro~lldwater Morlltoring Quality A$5urance Pliln (OAr) ! t i ! , . i :: A IT ACHMENT I WHITE MESA URANIUM l'dILL Attachment 1 , :> Sec in~tnIction nELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I \ s t Q LIe. t (!..(' /II . t-I"~ k e. ~O \ l Sampler Name Location (well name):1 r w)! -\ Y and initials: Date and Time for PW"gin~ 11 ;;"71 ¢o II • and Sampling (if different) I 0 \ l .w LiD It Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) I Gf"u....J..~l2£) Sampling Event Q wort V \i £, t MJ d Prevo Well Sampled in Srunpling Even! I T LJ A/-I ~ pH Buffer 7.0 ,-I 7-<..:..~O,---_-----, Specific Conductancc,-' 9 ......... 9 ..... 9 ______ ..... IIlMHOSl em Depth to Water Before Purgin~ 6.:3. (/ S· I Conductance (avg) 10.32 pH Buffer 4.0 4.0 Well Depth(O.Olft): L.I '-13,,5 ___ ...... Casing Volume (V) pH of Water (avg) 4" Well:[Y£ill(.653h) 3" Wcll:~(.367h) 7.1 7 Well Water Temp. (avg) II Li .. .36 Redox Potential (Eh)L..1 _3ul..L,\_~ Turbidity I I L E> Weather Condo E)(t'l Amb. Temp. °C (prior sampling event) 13" c.. I Time I I4.:iQQ I Gal. Purged I :3 Y I Time 1 I Gal. Purged 1 I Conductance I l Q3~ I pH !7 .17 I Conductance I I pHI I Temp. DC 1f!1 .36 I Temp.oC I I Redox Potential Eh (mV) I :31 1 I Redox Potential Eh (m V) I I Turbidity (NTU) III.~ I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp. DC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater A lof2 capturx COM'A""" W'TH/'-UU'..v--fUHCTlO" ... L'n ~ • ~ ~ Moll :.'Gr .. uniiwater t~~har81! Permit ) Groundwater Monitoring Qvality AssurancE! Plarl (QAP) Volume of Water Purged 1 4 L 1 Y Pumuing Rate Calculation Flow Rate (Q), in gpm, S/60 = 1,---,-' 7-<--__ ---1 gallon(s) \ / Time to evacuate two casing volumes (2V) T=2V/Q= I ~ 15.5~ Number of casmg volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated I 41, I Ij Name of Certified Analytical Laboratory jfOther Than Energy LabfL.. ...... A/~'-IAu-____ --1 Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified below) Y N Type VOCs 0 0 3x40ml 0 0 HCL Nutrients g 0 100 m1 0 9 H2SO4 Heavy Metals 0 0 250m! 0 0 HN03 All Other Non Radiologies 0 0 250ml 0 0 NoPreserv. Gross Alphll 0 0 1,000 mt 0 0 HN03 Other (specify) r&1 0 Sample volume 0 ~ Date: 03/22/2010 Rev, 6 Preservati ve Added y N CJ CJ ,1& 0 0 0 0 0 0 0 0 1m £:k lo,. i Ae. If preservative is used. speci1)r Type and Quantity of Preservative: See instruction §Comment I 1 , Ar-r-'\\J(!.,,-J.., 01\-$t l-e... o-• .\-13l-15, b()...r f"'/'.. tJ.,.,..,Q... ~yA'" !;,. pr-e...s;,-""t-~C)r fu~e... ()..."".;.,. 5A.,.vI.~r,~ e.\JeA.t. ~v'3e.... b~t\J\ Q...+ \3.s~¥ f'Vf"\f 1""'-11\ ~()-r-Q. M'l\.vte,,~ (A.tJ... . l.-\ \ !i.(.,UJ~S~ W~l r-c...1I\.. c). ry" P~r&\..~L\-'e.rJ we..r-('-+-~¥-M ~('(?"",," ()lIe..r~vf"'\.f'~ .f\ e-\£l S~ t-e... L. l-e.-f't $11 e.-0.-t-\1.{ , f . . A \ ,L 0 01 1) O .. o}iA.-t-c, vVc-l-er .....J?...S 6-::3·').5 , rrl v'/!O' O.A-S I te.... ~T lJ 10". '-1 So..~f lt.-.s vJ e.-re... ~e...~e-II\ ~ .... () ~;.O, ~ _______ ---IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for GroundwClter A 20f2 capturx COMPATIBLE WITH ............... b-ruNCTlOHALITY will· Groon.dw'ater DitchBrge P e!Tllit ) GroUlldwater Monitoring Quality Assurance plan (OAP) DatI!: 03/22/2010 Rev. r. i ! !i . ~ OENISO.}) ~ M INES ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~ .. ' See mstruCllon FIELD DATA WORKSHEET FOR CROUND WATER Description of Sampling Event: II s I-a v f>.. h ;.r At , k= t "= h:. ~ 0 \\ Sampler Name Location (well name):1 rWAI-15 nnd initials: Date and Time for Pllrgin~ t(fJ .$ z . ;iiti't I I /:J.6/·~' \ Well Purging Equip Used: ~ pump o@ bailer Sampling Event I Gllp:.dc<r\y N itrreh:..-I pH Buffer 7.0 L...17.L.:..J' OIoL.-__ --1 Specific Conductance ... ! -.Jg:...tg~'t~ __ ....J!IlMHOS/ em Depth to Water Before Purgin~ 'f 2. 3 9 Conductance (avs) ... 1 ..... 15~6~i:....-____ ---' and Sampling (if different) I I / :1.71 ';2.0 I \ Well Pump (if other than Belmet) I Gtllr,,15"w; Prevo Well Sampled in Sampling Event I T L.J A/-7 pH Buffer 4.0 4 ... 0 Well Depth(O.Olft): .... 1 ...... 15,.".· .... 5 __ ----' Casing Volume (V) pH of Water (avg) 4" well:1 ~ $7 1(·653h) 3" Well:t..l. r2~ __ ..... _ (.367h) 6,71 Well Water Temp. (avg) I 1$.79 Redox Potential (Eh)! :l q] Weather Condo Ext'l Amb. Temp. °C (prior sampling event)1 3 c>L Time I j052. I Gal. Purged I ;? 4 I Time I I Ga1. Purged I I .' Conductance I 15 -', I pH I 6.7l I Conductance I I pHI I Temp.oC 113,7Cf I Temp.°C. I I Redox Potential Eh (mV) r ?-'1} I Redox Potential Eh (m V) I I Turbidity (NTU) I B'tl ~. I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance ! I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Oatil Worksheet for Groundwater .A . 1 of2 capturx tOMPATlBLE WITH/",,_l'ir-FUNClIONALITY 1'4111 -Groun.dw~tl!r Dischilrge Permit ) oatt: Ol/22/2010 ~Y. 6 Groundwater Monitoring Quality Assu!"incl! PI~n (ClAP, Volume of Water Purged 1 $7. YD Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ..... 1 ....... 17..1--__ --1 gallon(s) Time to evacuate two c.asing volumes (2V) T = 2ViQ = I artj>ttHj! 1 I.·L $0 Number of casing volumes evacuated (if other than two) I.Cf(S Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL... ~...v~A!..-_____ --I Sample Taken Samplc Vol (indicate Filtered Preservative Preservative ~ ~ . !I !! Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) c.,h lo r-\ At S 3Comment y 0 ~ 0 0 0 JiI if other than as N specified below) 0 3x40ml 0 lOOml 0 250ml 0 250mJ 0 1,OOOml 0 Sample volume , y N 0 0 0 IS 0 0 0 0 0 0 0 9il I Added Type Y HCL 0 H2SO4 ;a HN03 0 NoPreserv. 0 HN03 0 0 Ifpreservative is used, specity Type and Quantity of Preserva live: See instruction i' A rrlve.-J. t> ..... ~., te. 0..+ 10.$0. G""rt"IA ()..NJ.. (Ly'""" s. 0"" ~H ,-~o(" (Jv~e, c..,..J... .s~f' II ~ e Lle. ...... + . ..5 h .. r-tt.J. pv~ c>-+ lObO. ~CA"'-pVr'-f f1C#" ~ M' ...... vtt-> "-~ ~ 5e.&lJ~. W G.-H r~oI'\.. ~r--'I. w""· ... et' VV'e-vS v~e..ev--.f-II..f'O~""oV+ .. {...up.e..J... pe.~"'ter.s ~HM , &v rr ptJo'I'\.fi~ ~i e.~ &l >h.u'" t. t..-~f \--S i ~ ~ Ow~ II 04 , Ar-Hve..tk. CIA.. s,-4e.. o...+-ag.sq . Sc.."",,-ples L.J e.r-(.. '-olt el-te.A 0-.. t-OqO <--\ '-_______ --IIDo not touch this cell (SheetName) White Mesa Mill N 0 0 0 0 0 ~ Field Data Worksheet for Groundwater A 2of2 capturx COMPATlBL! WITH/'-U'U'b-.UHCTIONALlTV . \ . . '" ill -Ground\J'at~r Di!th;:arge Permit ''. i (oun~w~'ter Monitoring QUllity Assurance PI.n (QAP/ Dare: 03/22/2010 Rh. 6 .... . ~ I f A IT ACHMENT 1 OENISO,}) ~ WHITE MESA URANIUM MILL Attachment I . ....j See Ulstftlction MINES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 Is t <)? VQ.~ te,c: All \-.f'Do-! e... Q..Q\\ Sampler Name Location (well name):1 r W.N' ~ 16 and initials: Date and Time for Purging/ I L).7/2-0i I and Sampling (if different) Well Purging Equip Used: [IDpump o@ bailer Well Pwnp (if other than Bennet) Samplmg Event I Q tJ/2.d: er \ 1 AI. + c .. teJ Prevo Well Sampled in Sampling Event I r I"; jI/-18 pH Buffer 7.0 1L..7~.r...lO~_--J Specific Conductanccl.,1 _9 .... 9.,&..;;.,191--_---J1 ~MHOS! em Depth to Water Before Purgin~ 4 fj ~ Y H Conductance (avg) .... 1 ..... 12..,::;...,S""'/~) ____ ---I pH Buffer 4.0 1 ~.O Well Depth(O.O 1 ft): 1-1 ...LIIoLOOIoL~ __ --J Casing Volume (V) 4" well:1 33. 6S 1(·653h) 3" Well:. (2 . (.367h) pH of Water (avg) L..I 4.Lb..tt.. .. 5...r;·..L'l ____ --J Well Water Temp. (avg) II Y • 7 $ Redox Potential (Eh)l 3Y 1.-1 I Turbidity 1 , ~. 7 Weather Condo Ext'l Amb. Temp. ·C (prior sampling eventl!"zO (.. 1 Time 1/ :l-YO I Gal. Purged I 170 I Time I llY\ I Gal. Purged I 181 I Conductance 1 13~6. I pH 16. $q I Conductance I \'~6l I pH I 6.60 1 Temp.oC 119.7.5 I Temp.oC 11y.75 I Redox Potential Elt (mV) I :3L1K I Redox Potential Eh (mY) 1 3 Y b I Turbidity (NTU) 1 1/7,.0 1 Turbidity (NTU) 115.3 1 Time 1!:tYa: I GaL Purged I ¢o y I Time 11.4'3 I Gal. Purged I ;).~ 1 J Conductance 1 1~!:f~ I pH 1 6. sq I Conductance I '~JI I pH I 6.~O I Temp.oC 1 1~.771 Temp.oC 11'1 ·7S I Redox Potential Elt (mV) I '549 I Redox Potential Eh (mV) I '3 Y \ I Turbidity (NTU) I l ~t .l-I Turbidity (NTU) 1 16~~ I White Mesa Mill Field Dala Worksheet for Groundwater ~ 1 of2 capturK (O"'ATI8Le ""TH~"""'W--'U"CT10"ALIT' ·MiII-·Gr6und~ ater Oi~(hi!flte Permit Date: 03/2212010 Re~. 6 .. 6rt'ur~ter Monitor;T18 Qua!lty A.lSuranCe Plan (QAP) Volume of Water Purged I 1= a. I Pwnping Rate Calculation Flow Rate (Q). in gpm. S/60 = 1-1 -Io'_71--_~ gallon(s) Time to evacuate two casing volumes (2V) T=2V1Q= I ~ I 3.q5 Number of easing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated AdA Name of Certified Analytical Laboratory if Other Than Energy Labt,-"",M~/",-A~ ____ ...... Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample VOCs Nutrients Heavy Metals All Otber Non Radiologies Gross Alph.'\ Other (specify) f_ \... \ 0 ... , ,:.te. a ~ 3Comment y 0 ~ 0 0 0 ~ if other than as N specified below) 0 3x40 m1 0 100 ml 0 250ml 0 250 rol 0 1,OOOml 0 Sample volume Added y N Type y N D D HCL 0 0 0 ~ H2SO4 ~ 0 0 0 HN03 0 0 0 0 NoPreserv. 0 0 0 0 HN03 0 0 0 ~ 0 JiSI [f preservative is used, specity Type and Quantity of Preservative: See instruction A (""1'"'\11 ul 0""' S,' te.-o...~ I :;totL 6(>..r~'A-o..~ ~'I~t/\.. ().A-S1-\-e IiVI' f'V~(... (J.,~ .sA.,.....fl\~ €;vl.-",J. 5 h.r-t~ euBc... ~~ I ?-30. 9l),v\.f f"lA,,,, .~o-t'"" 13 M. AV t"~. , S~le..$ \..1.Ie..r-e.... l-o\\,-c..te..J.-/l-·t t,l-iS" PA.r-~Me....ter~ v)u-e.. h .... t::-eA... .~('''M-bvu-pv'V\f'~ .~\ (.,~J. S~u.....\. t,. ~~ .... ~ ," t.. p...~ t,.S:t . ............. _______ --1IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater .A . 2of2 capturx' CO".ATlOLE WITH~YU'Ii:>--'U"CTlON"L'n I 3 i : Gr~ndwllle; Discharge Permit Date: 03/22/2010 AI!V. 6 <>roundwater ,""mitoring Quality Assurance Plln (QAP) OENISO,!) ~ MINES ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 Sc:e instructi(1n : -. ____ r _~ __ .. '.-.-_-"" ___ " ... u.-: .... -FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: l is t Q Vc,!..r-+e..r ; ....... A.t ~ ~"I\ Sampler Name Location (well name); .... 1 ·~r-,W=-:;V~-....I1 ...... 7t-.. ______ ----I and initials: 6~"r .A...-PA l M~ l op Date and Time for Purgind 0 1/31 / 2.0 i, and Sampling (if different) I Q ;;l /o l/ ;l Q I \ Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than BeImet) SamplingEvent I Q~Ar-t e..d >, #i +"'~~9 Prevo Well Sampled in Sampling Event I TwAl..-III pH Buffer 7.0 .... 1....l'"Z~{~Q:;......._----I Specific ConductanccL-I .... 9 .... Cf.J.....I.9 __ ---lIJ.lMHOSI em Depth to Water Before Purging/ :3 Y . 7Y I Conductance (avg) II ':II pH Buffer 4.0 Well Depth(O.Olft): 110 Casing Volume (V) pH of Water (avg) 4" Well:~(.653h) 3" Wcll:~(.367h) Well Water Temp. (avg) 1 13~.55 Redox Potential (Eh)1 2 W'l Turbidity I y 1 t 8 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)1 O"C I Time I D'f09 I Gal. Purged I 12 I Time [O't10 I Gal. Purged I 34 I Conductance I II ~.5 I pH I 6.95 I Conductance I 113 4 I pH I 6.90 I Temp.oC I 1.2. (.3 I Temp.oC I 13.70 I Redox Potential Eh (mV) I X it 7 I Redox Potential Eh (mV) I 2g~ I Turbidity (NTU) I 'l or 6 I Turbidity (NTU) I IS ?. I Time I Qqll I Gal. Purged I 51 I Time I I Gal. Purgcd I I Cond uctance I 11.s~ I pH I 6«qQL I Conductance I I pHI I Temp.oC I I y. 13 I Temp.oC I I Redox Potential Eh (mV) I ,2 Cf 1. I Redox Potential Eh (mV) I I Turbidity (NTU) I gO!t~ I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for GroundwClter A lof2 capturx' CoM.An ... WITH/'"~ri:>--FUNCTION .. LITY ;~ Gro~ndwa'!e~ Oim,arge Permit Date: 03/22/1010 Aell. 6 Groundwater Monitoring Quality A.sS\lr~f\c;e Plan «(lAP) Volume of Water Purged I SY .57 Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 ......i1w7t-_--I gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = I dIIliii 1 5" 8J Number of casing volumes evacuated (if other than two) LID If well evacuated to dryness, number of gallons evacuated I St.J.571 Name of Certified Analytical Laboratory if Other Than Energy Lab~,-~.N-,-loL.A.....!.-____ --I Sample Taken Samplc Vol (indicate Filtered Preservative Preservative Type of Sample if otber than as Added y N specified below) Y N Type y N VOCs 0 0 3x40ml 0 0 HCL 0 0 Nutrients fi'J 0 100 ml 0 fi H2SO4 iii 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Prescf'l. 0 0 Gross Alpha , 0 0 1,00000 0 0 HN03 0 0 Other (specify) t'iQ 0 Sample volume 0 til 0 lKI . C L,.1.,,...~cAi" Jfprcscrvalivc is used, speciJY Type and Quantity of Preservative: ! I i See instruction ~Comment A~""\vte.l ~-->I ·t~ A.t Of/57, b",-r.-.'A,. (J..~ ~yvV\. 5. f""e..s~t-~(N-pv.~e,.. o.;vJ... ">~.wP\'I~ c!.VG-",,-t .. f>v~v be-1)&.A,. M (!)etoS" P&J-M.{J f'"~ Q6r' ~ .,v\.:~te.s ~M. ~I .>evo:J.>. Wt..t l t"'tlo."'-J..~'(. P(l.I"~Me,..te..t-;$ lA./e-t-e,.. +'"-Ic:.~ ......... fr-eJ.v\.. .\-t.-..e, . ()ve.rp(/.,A.p,~ f'le..~~ '>IA.(;VL L-G-f · ... $~te.. ~+ e>~ 17_ A 1"1',1,1 ~~ Cil'-g<rl'e.. 0.. ~ 0 1_~ i . 5.~Mp\e..~ we.rG-\-OI..Y,,!..A. "'\-01SQ. Oe.H~ \-v ....... i!--\-e-r v./p...,S 3'-l .:;n. i..( .... ~t >i~e-o-.l-ogol. (;'';''tl',1\. A../4\.. (l.Y'VA. s:. ()1'c....!.iZ"J\t, '-_______ --I/DO not touch this cell (SheetName) White Mesa Mill Field Dal8 Worksneet for Groundwater .A 20f2 capturx COM'Arlel! WITH~_ti:r-'UNtTIO"AlI1Y , . Mitl -Groundwater bisd1ar~~ Permit Oate: 03/22/2010 Rt\I. 6 Groundwater Monitoring Qualltv Assurance Plan (QAPI I ! I I ! OENISOJ) J. ATTACHMENT 1 WHITE MESA URANIUM: MILL Attachment 1 MINES FIELD DATA WORKSHEET FOR GROUND WATER Description ofSnmpling Event: II $ t rluo..d"r AI,! ,../>..\ (... :,).01' Sampler Name Location (well name):1 r w AI -1 <J and initials: Date and Time for PUIgin~ II J 7/1,0 I' and Sampling (if different) Well Purging Equip Used: [![]pump o@ bailer Well Pump (if other than Bennet) ,J Sec iostruClion I GrvM:\-fos Prey. Well Sampled in Sampling Event IT LJ)J -\ \ pH Buffer 7.0 .... 17-<-<..,..::;0 __ ---' Specific Conductance .... 1 _":-'l .. 9-1-. __ ...... IJ.l.MHOSI em Depth to Water Before Purgin~ 58. I Q Conductance (avg) 1-'1 ~~g",,--,'1_L..j...a....-___ --, pH Buffer 4.0 y .o Well Dcpth(O.Olft): .... 1 .... 1 ..... y ..... 5:...· __ ...... Casing Volume (V) pH of Water (avg) 4" WelJ:~(.G53h) 3" Well:~(.3G7h) 6 , y~ Well Water Temp. (avg) I) 1.:\ t f2 $ I Redox Potential (Eh)1 30::t Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)l, &c, Time I I p.5 a.. I Gal. Purged 1 2:9' 'f I Time 11053 I Gal. Purged I '3 ~ 6 I Conductance 1:l~!12 I pH I t. yo I Conductance I -:l ;';l~ 2 I pHI b. Y¢= I Temp.OC 114" c26 I Temp.oC 11H .07 I Redox Potential Eh (mY) I :} 10 --I Redox Potential Eh (mY) J 30 Y I Turbidity (NTU) 120. tJ 1 Turbidity (NTU) I itt 7 I Time 1112.5 Y I Gal. Purged I .:3 :l3 I Time 110>6 I Gal. Purged I :;>y 0 I Conductance 11:a:g 6 I pH 1 6.L.j'=i 1 Conductance I :2l9~ I pH I 6. ys I Temp.oC 11'1.05 I Temp.oC I ltI.o~ I Rcdox Potential Eh (mY) C:foo I Redox Potential Eh (mV) I ?-~Q I Turbidity (NTU) I lq'·i I Turbidity (NTU) I 'J.O_I I White Mesa Mill Field Data Worksheet for Groundwater A 10f2 capturx CO"~ATI.l( WITH~.-nr--'UNC"ON"LlTV · .' Mill· Groundwater oischarge Permit Groundwater Monitoring Quality Assurance pl,m (QAPl ! I ~ I Volume of Water Purged 1 .... .::;..3;;...&... ..... 1...::;0 ___ -' Pumping Rate Calculation Flow Rate (Q), in gpm, 5/60 = 1-1 ..... 1-'-7 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = I l8flM1ip I 6 .. 67 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labf ......... /V--o.i.,Lfi:-"--____ --" Sample Taken Sample Vol (indicate filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 m1 0 tJ HCL 0 0 Nutrients t8 0 100 ml 0 rgt. H2SO4 1i'1 0 Heavy Metals 0 0 250ml 0 0 HN03 0 o .' All Other Non Radiologies 0 0 250m] 0 0 NoPreserv. 0 0 Gross Alpha 0 0 I,OOOml 0 0 HN03 0 0 Other (specifY) fi' 0 Sample volume 0 tif 0 ~ ~k '''' (", c.lc. If preservative is used, specifY Type and Quantity (If Preservative: See instruction aComment Arl"",v"et o~ >i~e. 0--1-\011 .. G~,.,.,.A-()..~ ltyf.io.A. S-tJIA.. Site... fferr ..$A. ....... pl ·l ~ G-Ve-At. pvroe... be.bCo..A. l)..-\-I 035~ pVMf f"A.A ~CH'"' ~O W"".> ",\e.Wi'" o\vt",~ ftltt;e... PA.-f'~jl\Ac,...ter.s WG-re.-.~"-?A (!r-~#\. (2ie...~J... $t,..,c..e,..~ .. t.~~~ Si~e.. ''It IllJ.s~ $j)..~~I~S vle..re. .~~e.A.-0...+-10554 L..-_______ -..Jloo not touch this cell (SheetName) White Mesa Mill fl.ll',be... ()..~ ~1V\.",vle->. we-.-\"e.r rk. CJver pv~(~ Field Data Worksheet for Groundwater 2 of2 capturx COMPAT'"LE WITH~ri>--.UNtTIO .. ALlTY Mill • r,rou~dw~te" DischargE! Permit ) Date: 03/22/2010 Rev. Ii Groundwater Monitoring QUillity Assurance Plan (CAP) I ! I I .1\ TT ACHMENT 1 Attachment I &lENISOn Ai WHITE MESA URANIUM MILL ,.. Soc inslrUclion \ M INES FIELD DATA WORKSHEET FOR GROUND WATER _.'-.. ---.\ ..... -,-.-.. -.,.~'-. -'-~ .... .,.,-.--- Description of Sampling Event: ! 1st Cl v y.r t'tr A!i t 'e t.e ~oH Sampler Name Location (well name):! i W A/ -I q and initials: C2,vt'jA. Pt..\ "1"'-I & P Date and Time for Pllrgin~ (;) i/3 1/20\\ and Sampling (if different) [ci).. LQ ll;t.o \\ Well Purging Equip Used: 00 pump o@ bailer Well Pump (if other than Bennet) I GCVA-Ato ... Sampling Event Q jlf.,ct?r\y Ali -tCAtel Prevo Well Sampled in Sampling Event I'r w..A/-I L.f pH Buffer 7.0 1,-7~~-""O,--_-" pH Buffer 4.0 '-i. 0 Specific Conductance ..... 1 "...:-&'1_q~ __ .... I~MHOSI em Well Depth(O.Olft): 1 .... ....:.\...;..\ 0"'--__ .... Depth to Water Before Purgin~ .5~ • .5 b Casing Volume (V) 4" well:I1J7. y'f 1<.653h) 3" Well:. _ .(.367h) Conductance (avg) pH of Water (avg) 6.70 Well Water Temp. (avg) I Ii .S4 Redox Potential (Eh)1 3~ Y TurbidityI3.3. l) Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 Ol'l, Time IOflrs I Gal. Purged I 17 I Time ! e>g"1 H I Gal. Purged I :3 L{ I Conductance 118Z~ I pH 10,70 I Conductance Ilg~~ I pH 16 .. 7 , I Temp.oC 11.2,lb I Temp.oC 112 . q 6 I Redox Potential Eh (m V) I .3;2 q I Redox Potential Eh (mV) I "324 I Turbidity (NTU) l 7.f) I Turbidity (NTU) I bO.Of I Time I I Gal. Purged I I Time 1 I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC 1 I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater .A ~ 10f2 capturx' (Q"P"TI.L~ WITH/,-~FUNCTJQNALITY · . Mill·· Grou~c!wate'( Orlcharge Permit I>~tt: 03/22/2010 Rev. 6 Sroundwater Monitoring Quality A15Ur.ln(e PI"n (OAP) Volume of Water Purged I 3g. 5 q Pumping Rate Calculation Flow Rate (Q), in gpm . S(60 =1 '---1-17.<......-_---' gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = I rIiIOft1t 1 I--j .. Y I Number of casing volumes evacuated (if other tban two) I LOa. I Z i$\Sql Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Thnn Energy Lab!\... ..... Afo::...LILA.!..--____ --I Sample Taken Sample Vol (indicatc Filtered Preservative Preservative ! I :: :: ~ Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) '-"",1 f7_6 J..e ~Comment if other than as y N specified below) CJ 0 3",40 m1 13 0 lOOml 0 0 250ml 0 0 250ml 0 0 1,000 mt riI 0 Sample volume Added y N Type y N [J 0 HCL [J 0 0 !;i H2SO4 Ii<I 0 0 0 HN03 0 D 0 0 NoPreserv. 0 0 0 0 HN03 0 0 0 6D 0 [g' If preservative is llsed, .~pcci IY Type and Quantity of Preservative: See instruction At"t-\vt.J... "A.. .s·it~ evt 0'75'\. Go..r,.;",-c..M:J... ~'1';:""'-s. p,.e..s.t...I\; ..... ~ r"~e.. c... >a.,.AP~i~ e..v~t, fJlI'rhe-P~A"-A,.'+ C>SI~. fJVMf (-4"" ~~ 0.. +0 h .. 1 ~~ 1... M.oI\.V +~$ o..~ 'l. -, .sc:..c.".~. v,Je.." r().A,. At-'1~ p.:..("~e..te"'.-' i,;V~f"e.-+-~\£..e."" f' r-t> v"'V .t-L--. to-I!' ve-r P v tV\. P i ~ 'J../ 1/ ;J.o i I Cre..1A ..st..-.-e-e..-t. J....eJi~ ~i'~(!, tt1"-C;>S~5. Ar(,\VtA,loA. .::,le... "-l 07'3$. Oe.pth. t-C' .J... '--_______ --'IDo not touch this cell (SheetName) WIllte Mesa Mill Ft!!lc! Data Worksheet for Groundwater .A 20f2 capturx to"p"Tla~t WITH~......,nr-FUHCTIOH~LITV Mill : Grolln~ater Discharge Permit Date! 03/22/2010 R\!v. 6 GrounawlIter Monitoring Quality Assurance Plan (lAP) ATTACHMENT 1 OENISO,}),4..4 : WHITE l\IESA URANIUM MILL Attachment 1 '/ See insU\lclion MINIS FIELD DATA WORKSHEET FOR GROUNDWATER Descriplion of Sampling Event: I 1 $. +-liLl{)..r t K Ali t Mire :lo 11 Sampler Name Location (well name):1 T ldlAl -\ q (t. and initials: ,-I ..... G~· ""o.:..,. ..... ('.n,oI\.""'--.Q....,'i.1.'-4I ...... vvl~ec~/-I6c....!-P_-J Date and Time for Pl.I[giD~ 01 /311 bt> 1\ Well Purging Equip Used: []!]pump o@ bailer Sampling Event I 0 IIAt k-c;.My /1/. l-c""te.1 pH Buffer 7.0 1 ..... ,7 ......... "",,0 __ -' Specific Conductance ..... ' _9 .... Cj ..... 9-'-__ --'IJ.lMHOSi cm Depth to Water Before Purgln~ IV/A Conductance (avg) 19 and Sampling (if different) Well Pump (if other than Bemlet) Prevo Well Sampled in Sampling Event I T W .N ~ ,y pH Buffer 4.0 Well Depth(O.Olft): I ALIA '--"J"-+, ........ __ -"' Casing Volume (V) 4" Well:~(.653h) 3" WeU:ca==J(,367h) pH of Water (avg) 6.5 6 Well Water Temp. (avg) Ie. q 7 Redox Potential (Eh)1 ;l L.j 9 Turbidityl ........ o~_---" Weather Condo I .1 ~.~~\D_V_~~t~ _____________ ~ Ext'J Amb. Temp. 'C (prior sampling event) I 0 0 c. Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I l~ I pH I 6.1:,6 I Conductance I I pHI I Temp. DC I ~,L '1'1 I Temp.oC I I Redox Potential Eh (mV) I ;l~9 I Redox Potential Eh (mV) I I Turbidity (NTU) I D I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pH I I Temp,oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mes~ Mill Field Oatil Worksheet for Groundwater A lof2 capturx' tOMPA",,' W'T"/'-HU'tT-'UNCTlDNALITY Mill -Groundwller 'Disch.argc,o Pl!rmll o.t.: 03/22/2010 Rev. 6 G,oun(!w"ter Monitoring Quality M!UfanCe Plan (QAp) Volume of Water Purged ~I .-.100\ 5,' .:;.0 __ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q). in ¥pm. 5/60;: ,-I ......... 17"'-_---' Time to evacuate two casing volumes (2V) T=2V/Q= [N IA I Number of casing volumes evacuated (if other than two) AILA If well evacuated to dryness, number of gallons evacuated IIILA Name of Certified Analytical LabomtOIY if Other Than Energy LabfL.--LN.z.-I./~A"--___ --I ~ , ~ :i . Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) '(k l D"", eA e. S =Comment Sample Taken y N 0 0 J2!l 0 0 0 0 0 0 0 ril 0 Sample Vol (indicate Filtered if other than as specified below) Y N 3x40 ml 0 0 lOOmi 0 fi?l 250 mJ 0 CJ 250ml 0 0 1,000 m1 0 0 Sample volume 0 ~ Arr--,ve.A ()A s.;~(, c..+-D71~. 6c..r-r,,, o-.Atl.. R.y'A..A. S. rr~e.A+ ~'Ir'\>e... te.. b~,ro. ~+ 07 ').7. ~vMf'e,'" 11;~ b"'-l\t,,,,,> () ~ Ac...J... o~ ~ vvI&o..iu\ Co...A.cA. 50 6~'l"-,,,.s o ,~ P.l='. w .... tt-f'. >"-Mple..,S. Soe;..p L.t.~4-Site. til1-0,'16. 1-_______ --1100 not tOllch this cell (SheetName) White Mesa Mill Preservative Preservative Added Type y HCL 0 H2SO4 6ll RN03 D No Preserv. 0 RN03 0 0 I f preservative is used. specify Type and Quantity of Preservative: See instruction ~ ~"'r I'" 1A,..;;e..1 e-. v-Jc..~e..rl 50 6~,\ul\h N 0 0 0 0 0 ~ . "' •. nA'L +-t\. k:-t.A. ~ t en 36, Field Oat;) WDrksheet fDr Groundwater ./I, , 2 of2 capturx COMPATI8Ll WITH/,"_~FUNCTlON"LITY 'Mill . Gro~ndwater Dis(har~ P"rml\ Date: 03/22/2010 RI!'V. 6 GrOtlndlNater Monitoring Quality As5urance Pl.n (QAP) AnACHf\lENT 1 · OENISO..!l J WHITE MESA URANlUl\1l\1ILL Attachment I ':1' See instrudion MINIES ! FIELD D.olTA WORKSHEET FOR GROUND WATER .-----.... ~~-.. .h _____ -.~-• ...., .. , .. _ ........... --- Description of Sampling Event: I I s, Q j4r1 rlec AI/lrde £ tJ 1/ Sampler Name Location (well nnme):L.1 ;.j.2--"-1/£~?~..L/ _______ .-.I1 and initials: I l<¥<d /J1mu: Date and Time for P\lrgin~1-_______ ---1 and Sampling (if different) 11-3l2tJ/I Well Purging Equip Used: [QJpump o~ IiYI bailer Well Pump (if other than Bennet) SampJingEvent IQ(Mrk.r, AII/x6k. pH Buffer 7.0 I 7J) Prevo Well Sampled in Sampling Event L..1 .... N'-.:...L./..Lti...;...... ____ ....J Specific Conductance I qqr IJ.lMHOS/cm Depth to Water Before Purgin~ 6/, I'LZ Conductance (nvg) pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) 4" WeIl:c===J(.653h) 3" WeU:c==J(.367h) pH ofWnter (avg) Well Water Temp. (avg) Redox Potential (Eb) .... 1 ___ --' TurbidityL-I ___ -' Ext'l Amb. Temp. °C (prior sampling event) I / ZI k I Time 11,2/2"1 I Gal. Purged I I Time I I Gal. Purged I I Conductance 1 ~3~ 7-I pH I C, ;2 SS' I Conductance I I pHI I Temp. DC 113··21 I Temp.oC I I Redox Potential Eh (m V) I .2 q 1 I Redox Potential Eh (mV) I I Turbidity (NTU) I IJ. I) I Turbidity (NTU) l ] Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. DC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater .A lof2 capturx-COM.A,la •• WI'H~ ....... n.--'UNCTIDN •• ,TY ~iU -Grollndw.t~r Discha~g~ P~rmit Date: 03/22/2010 Rev_ 6 Groundwater Monitoring QUAlity AssUrance Plln (QAP) Volume of Water Purged L...I ____ --.I gallon(s) Pumping Rate ClllcuJati.Q.n Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60= __ I ___ ----' T;2VlQ= 1 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labll-___ :...-___ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added . Type y N specified below) y N Y N VOCs 0 0 3x40ml 0 0 HCL 0 0 Nutrients JRI 0 100m! 0 !Sit H2SO4 ~ 0 Heavy Metals 0 0 250 nil 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 NoPreserv. 0 0 Gross Alpha 0 0 l,OOOml 0 0 HN03 0 0 Othl.tPe~ify) til 0 Sample volume 0 1flJ-0 !J L 'I1-~J~ Ifprcservativc is u!>Cd, specifY Type and Quantity of Preservative: ~ See instruction ~Comment I f Qr.6ve.J ciA //).SO ~~"'-po-(~(' ~ re.S (:",-1'"" ·fbr Sa.fI\;(fl/:J ~. ~t-.sor--q·F Petx"At'tt~5. ~{a.v...." Be>.: I~r IN~S. /ASt!e:( fa a-/led pQ<c:t~ ()I\o\ a, (Iwi-S~""'fl~.. ~S?tV'Af {1i ~t7Ifu,kj dt' 1305", t1ne.. i5~.lw N~ ~ rvt ~o'" ~ o-f /OS.7 d~j,U.-..J ~ JVt.-I/. 60-.k..... dbtv..-v welr. ~p,pf Be:..'.t~ j/O(fb '( ~ dlOt'fh1 '-_______ --'100 not touch this cell (SheetName) White Mesa Mill Field Oata Worksheet for Groundwater A 20f2 capturx' COMPMI8LE ""TH~_li:r-fUNCTIONALITY Mill Groundwate~ Discharge Permit 'Groundwater Monitoring Quality Assurance Plan (ClAP) ) " Dat~: 03/22/2010 Rev. 6 ATTACHMENT I Attachment 1 OENISO,.})J.4 WHITE MESA URANIUM MILL ." Seein~lruclion MINES FIELD DATA WORKSHEET FOR GROUND WATER _..--,.,... _ ... __ ... ~'?-_~ ___ ,.... --1 ...... -- Description of Sampling Event: [ IS r Q',{4"* v AhW. ,go /I Sampler Name Location (well name):[ P,t'<? 2. and initials: [J~"b-/hl~c Date and Time for Purgin{ 1· S , , <:II j( and Sampling (if different) Well Purging Equip Used: [gJpump o@ bailer Well Pump (if other than Bennet) Sampling Event [CQIM.<"r:~ AI /Io"./.t -< I pH Buffer 7.0 I .... lQ Prevo Well Sampled in Sampling Event '-I----'N_· .... (_(l-~ ____ _'" Specific Conductance I Qq'1 IIlMHOSicm Depth to Water Before Purgin~ It .. q1 I Conductance (avg) pH Buffer 4.0 'to 0 -I Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" Well:c=:=:=J(.653h) 3" Wcll:c=:=J(.367h) Well Water Temp. (avg) Redox Potential (Eh)IL-__ -..I Turbidityl-t "k Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I /.a c.. I Time I 13 3 7: I Gal. Purged I I Time I I Gal. Purged I I Conductance 1,5 'i.}( I pH I 7 .'/ I Conductance I I pHI I Temp.oC I g; 5"7 I Temp.oC I I Redox Potential Eh (mV) I ,S'25Z; I .-Redox Potential Eh (my) I I Turbidity (NTU) I fJ, () I Turbidity (NTU) I I Time I -I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet (or Groundwater .A 10f2 ca pturx Cc>.,'AT,"LE WITH ./'-WU'~'UNCTIC>NALITY Mill . Groundwat~r Discharge Permit Ollte: 03/22/2010 Rev. 6 "Groundwater Monitoring Quality Assurance Plan (QAPI Volume of Water Purged 1 '--------' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60:: .... 1 ___ --l T=2V1Q= 1 1 Number of easing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~,-_______ ---, Sample Taken Sample Vol (indicate Type of Sample if other than as y N specified below) VOCs 0 0 3x40 m1 Nutrients J<I 0 100 mt Heavy Metals 0 0 250ml All Other Non Radiologies 0 0 250 ml Gross Alpha 0 0 1,000 mJ Other (specify) ~ 0 Sample volume rJ:I~N'iA~ ~ I =Commel1t ttV''('I'",d oV'. '$ ,'+& ci.t 133 2 ~ Jdyc,;...-...!~ ~y" o\"\{, .5 ej-of p,:;vrG.-V1A-e..levs -b../~ ttvt +4 V'- '--_______ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Filtered Preservati ve Preservative Added y N Type y N 0 ·0 HCL 0 0 0 ~ H2SO4 .ti 0 0 0 HN03 0 0 0 0 No..Preserv. 0 0 0 0 HN03 0 0 0 .211 0 ,il IfpreservBtive is used, SpeCIfY Type and Quantity of PreselVlllive: j See instruction t/'~j~.,..;r .fw SttWlfll""'-J ~"t S~VfA(JIt:5 f1,11e~~l ~r 1.5'10. Mill· .C;roundwater Dls~harge Permit Oate: 03/22/l010 Rev. 6 Groul\dwater Monitoring Quality AjSuranCe Plan (OAP) i ! t ! i A IT ACHMENT 1 "EN' 50,!) j WHITE MESA URANIUM MILL Attachment I ,. See insl!u~liOJl MINES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event / 7 r (J()(4 ".kr: Al)'ktJ.f I ~ 0' ( Sampler Name Location (well name):1 P, e:c t:3 I and initials: 1 .... _12.=,'+!t4.......:..N.::....-..... tJ.-'A""' .... Imr.r; ..... L .... :r~_---' Date and Time for Purginm l 3 , 20 II Well Purging Equip Used:[9Jpump 000 bailer Sampling Event I QU4chw§ NNra k.. < pH Buffer 7.0 I 7 -0 I Specific Conductance I qq 1 IJ.lMHOS!cm Depth to Water Before Purgind "fq, L > Conductance (avg) and Sampling (if different) Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event , .... _______ --' pH Buffer 4.0 1(.0 Well Depth(O.Olft): Casing Volume (V) 4" Well:I==:=J(.653h) 3" Wcll:c===J(.367h) pH of Water (avg) Well Water Temp. (avg) Redox Potential (Eh} .... 1 ___ ..... Turbidity ..... 1 ___ .... Weather Condo Ext" Amb. Temp. ·C (prior sampling event)l:? "( Time I 135 I I Gal. Purged I I Time I I Gal. Purged I I Conductance 12 ql5" t/ I pHI 1.;l·3k I Conductance 1 I pHI I Temp.oC I q 11 I Temp.oC I I Redox Potential Eh (mV) I '·~.-C2 g I Redox Potential Eh (mV) I I Turbidity (NTU) If/J_~ . '-J Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conduct<lnce I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Oatll Worksheet for Groundwater .A . lof2 capturx' COYPUI'.! WITH~_~FU~CTIONALITV Mill ",Groundw.'I!' Dlscha,g. P.rmil ) Date: 03/22/2010 fie\<. 6 Gro~ndwater Monitorina QUllity luswance Plan (QAP) Volume of Water Purged ... 1 _____ --' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = .... 1 ___ ----I T=2V/Q= 1 I Number of casing volumes evacuated (if other than two) lfwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labl ... _______ -.J Sample Taken Sample Vol (indicate Type of Sample if other than as y N specified below) VOCs 0 CJ 3x40ml Nutrients j8J 0 100mi Heavy Metals D 0 250ml All Other Non Radiologies D 0 250ml Gross Alpha D 0 1,000 ml Other (specify) .r1lu) IAPJ P' 0 Sample volume ~Comment Filtered Y N 0 0 0 ~ 0 D 0 0 0 0 0 ~ Preservative Preservative Type Added y HeL 0 H2SO4 ~ HN03 D NoPreserv. 0 HN03 0 D If preservative is used, specifY Type and Quantity of Preservath'c: !. See instruction i ] N 0 0 0 0 0 $I ~t"AV'-fatvN!-f' pr-v~ ~ SaWl~/~ W~. O'lr!. Se.--f C/ f. aVlpl SA "f\Af/~ {jyllevfed o1-r 13SS" Th.,'!. bJ"'U )..fA.J Vl. VCJ h,l,~ f J,.. (,NtJvk.v tV4,~ O{M/ PVAi ".J..CFT"'~,> '-_______ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Diltil Worksheet for Groundwater .A 20f2 capturx COM,ATOILE WITH .......... ~ri:r--.UNCfIONALITY .. t... • _ Mill -Groul1dwat~r DI5<harg~ Permit Date: 03/22/2010 Rev. Ii GroUndwater Monitoring Qualitv Assilranc~ plan (QAPl ! I " : .; ! : OENISO.!l J MINfS ATT ACUMENT 1 WHITE l\'IESA URANIUM MILL Attaclunent 1 FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1/5 r Q'MC/.w N da;, £ d.a L.I Sampler Nnme Location (well name):L...1 -uU"",IAQ".l...J ... i ""'p ________ --II and initials: Date and Time for Purging .... _______ ---J and Sampling (if different) I , I i ,'?/· ,2.al/ Well Purging Equip Used: [QJpump 000 bailer Well Pump (if other than Bennet) Sampling Event 1 QUbatk(~ N,'{w-/i pH Buffer 7.0 I 7 . Q Prevo Well Sampled in Sampling Event 1-1 _______ ---' pH Buffer 4.0 Specific Conductanccl-I __ 1.A.....40'l_G&..t _....JI ~MHOS/ em Well Depth(O.O 1ft): Depth to Water Before Purgind'-......:...N(-,I/ut1~~ Casing Volume (V) 4" well :~----fI(.653h) 3" Well:. . (.367h) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) Redox Potential (Eh)L..1 ___ ...I TurbiditylL..-__ ---' Weather Condo Ext'l Amb. Temp. ·C (prior sampling event>1 () '(= Time I 13.1/ I Gal. Purged I I Time I I Gal. Purged I I Conductance 12.2K I pH 11< $2 I Conductance I I pHI I Temp. DC I 2.02 1 Temp.oC I 1 Redox Potential Eh (mV) I 2.~~ 1 Redox Potential Eh (m V) I I Turbidity (NTU) I a.o I Turbidity (NTU) I I Time I I Gal. Purged 1 1 Time I 1 Gal. Purged I I Conductance I I pHI I Conductance I 1 pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I 1 Redox Potential Eh (mV) I 1 Turbidity (NTU) I 1 Turbidity (NTU) I I White Mesa Mill Field Dilt~ Worksheet for Groundwater A lof2 capturx' t<)"'ATln~ W'TH,./'-U'U'nr--fUNtTiONALITY Mill· Groundwater Oischarge Permit Grou'"dwater MonitOring Quality Assurance Plan (OAPI ) Dare: 03/22/2010 Rev. 6 Volume of Water Purged 1 ........ ____ ----' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1-1 ___ -I T =2V/Q= 1 I Number of casing volumes evnc1.1ated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratol}' if Other Than Energy Labf .... _______ --' Sample Taken Sample Vol (indicate Typc of Sample if othcr than as y N specified below) VOCs 0 Cl 3x40m! Nutrients .1M 0 looml Heavy Metals 0 0 250m! All Other Non Radiologies 0 0 250ml Gross Alpha IJ 0 1,000 ml O~r (specify) iii 0 Sample volume ~"",,~/, Icomment Filtered y N Cl Cl 0 JQ 0 0 0 0 10 0 0 !Sit Preservative Preservative Type Added y HeL 0 H2SO4 JiJ HN03 0 NoPreserv. 0 HN03 0 0 ~ (fpreservative is used, specity Type and Quantity of Preserv8 tive: See instruction y N 0 0 0 0 0 .Rl c\VY;v-(.. cl;.1""" /3 {1-~ 'ki ~ p~l~ f'''''!l~ .{by S':::lN<p/~ . O"'-~ Sl/f 0-1 PO-y"~wt~hn. +a.,I~ Ci\. •• , • .A Sawf (in ~ ~ Iled-td d.-i ;.J3:2s-, 7~ (A.J~ ~ .. ~.!> St<.MpJt~ ~ '--_______ --'100 not touch this cell (SheetName) WhIte Mesa Mill Field Data Work~h eet for Groundwater .A 20f2 capturx' COMPATIBle WITII~~rir-'UHCTIDNALln .. .... . .. Mill : Groundwater Discharge Permit ) Date: 03/22{2010 Rev. 6 Groundwater tJ!onltoring Quality Assurance Plan (QAP) i ! • I f OENISO.!)~ ..4 M INES ATTACHMENT I WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUND WATER Description ;.: Sampling Event: I I S r (JUL«: r; M /YQ.l.t, .z. 6 tt Attachment J " See instruction Sampler Name Location (well name ):,-1 -'=-P ..... a ........... n04:c ... ( _1'>"-"""--------..11 and initials: 1L-~ia'-"fY""'idu;"""""--..,.a'-£4. .... LnA"",,,,,,e~,c ___ -, Date and Time for PlIcgingJ1-_______ --' Well Purging Equip Used: [gJpump o@ bailer Sampling Event Q....('~v~ f.)'\ro. h. pH Buffer 7:0 t·o Specific Conductance! 11 r II-'MHOS/cm Depth to Water Before PurgingJ1.-_N't_~_A_'___...., Conductance (avg) and Sampling (if different) /-s/ 2011 Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event L.I _______ -J pH Buffer 4.0 Well Dcpth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:1 1(.653h) 3" Well:t-: ----t:C.367h) Well Water Temp. (avg) Redox Potential (Eh)L-1 ___ ...J Turbidity 1 ... ___ -, Weather Condo I L-c.._lo_v.A_*_4 _1'i ..... ~:::..l" ...... ~K...._h_~_.,o_..:> _ ___' Ext'l Amb. Temp. °C (prior sampling event)1 o· c. Time I ,'.\~\ I Gal. Purged I I Time I I Gal. Purged I I Conductance I ~ I pH I i. "3::). I Conductance I I pH I I Temp.oC I p,.Qa. I Temp.oC I I Redox Potential Eh (mY) I ;tq~ I Redox Potential Eh (mV) I I Turbidity (NTU) I O.Q I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mY) I I Redox Potential Eh (mY) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater A 10f2 capturx' COM'ATla.E WITH~_rir--FUNCTIONALITY . "- Mill :Groundwater Dlsch~rge Permit Groundwater.Monltorlng o.uallty Assurance Plan (OAP) . Volume of Water Purged ,'-_____ ...1 Pumping Rate Calculation Date: 03/22/2010 Rev. 6 gallon(s} Flow Rate (Q). in gpm. Time to evacuate two casing volumes (2V) S/60 = IL..-___ -J T=2V/Q= I I Number of casing volumes evacuated (if other than two) If well evacuated to dryness. number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~I...... _______ -' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3",40 ml 0 0 HCL 0 0 Nutrients 611 0 100ml 0 IS H2SO4 Ii3 0 Heavy Metals 0 0 250m! 0 0 HN03 0 0 All Other Non Radiologies 0 0 250mi 0 0 NoPreserv. 0 0 Gross Alpha 0 0 1.000 m1 0 0 HN03 0 0 Other (specify) 121 0 Sample volume 0 m 0 ~ Lhlor;l<... Tfprescrvative is used, specifY Type and Quantity of Preservative; ! See instruction 3Comment '--_______ ---1100 not touch this cell (SheetName) White Mesa Mill Field Data Worksneet for Groundwater ~ 2 of2 capturx' to""AT1.l~ WITH"......""..,..li>--fUNCTIONAlITY . . -Mill· Gro\lndW8u!r Ois(harge Permit Dat~' 03/22/2010 Rev. 6 Groundwater Monitoring auallty Assurance plan (OAP I ATTACHMENT 1 OE NISO,.!)~ J I WHITE MESA URANIUM MILL Auachment I MINES FIELD DATA WORKSHEET FOR GROUND WATER . . Description of Sampling Event: I I S r Qw;vW AI, 'W I . 20 11 Sampler Name and initials: Locati on (well name): .... I_:G"""""i'll......:;..;Nz--•......... h'-"r:.L~ ______ --' Date and Time for PllrgingJ,,-~:J.r......;.... -4-1---.,fI<"1 ..... (~J1'+( __ ---' Wen Purging Equip Used: [QJpump o{Q] bailer Sampling Event .... 1 ..... f..'\o-~ '''''MA:J.I:'f'-'~'''''W'-~T-''-'A ....... b .... ·Ih'"''f&d.c~~<--' pH Buffer 7.0 7.. [2 Specific Conductance II-_-l1i-qof-~+-_ ........ IIlMI'IOSi em Depth to Water Before Purgin!?J1-___ ...J Conductance (avg) and Sampling (if different) Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event ,L...-_______ ...J Casing Volume (V) pH of Water (avg) 4" Well:c===J(.653h) 3" Wcll:c===J(.367h) Well Water Temp. (avg) Redox Potential (Eh) .... 1 ___ --' TurbidityL...1 ___ ~ Weather Condo E)(t'l Amb. Temp. e( (prior sampling event) .... 1 __ -' Time I !J&?£ I Gal. Purged 1 I Time I I Gal. Purged I I Conductance I l3 . ~ I pH I 1I.5'? I Conductance I I pHI I Temp.oC I Il·K I Temp.oC I I Redox Potential Eh (mV) I <;,2, ( -I Redox Potential Eh (mV) I I Turbidity (NTU) I fl. () I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Me5a Mill Field Oita Work5heet for Groundwater .A 10f2 capturx' CO"'ATlJL( WITH,,/L_n.-FUN(tIONAlIH • MiII -Grollnd~ter Oisch'arge Permit Groundwater Monitorina Quality Asiurance Plan (CAPI " I Volume of Water Purged 1-1 _____ ....1 Pumping Rate Calculation ) Date: 03/22/2010 Rev. 6 gallon{s) Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1.-1 ___ ~ T ;: 2V /Q:;; 1 I Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL--_______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 IOOmI 0 ijl H2SO4 }iii 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. I. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other~CCify) f1 '~J1;lJ~J ~ 0 Sample volume 0 jXJ 0 )? If preservative is used, specifY Type and Quantity of Preservative: ~ See instruction !1Comment I 1-.. _______ ---1100 not touch this cell (SheetName) White Mesa MlU Field Data Worksheet for Groundwater A 20f2 capturx' CO ... A1I8LE WITH~HUo'rir-'UNCTlONAlITY Mill. Groundw:ller Discharge Permit " I Date: 03/22/2010 Rev, 6 'Groundwater Monitoring Quality A5suriJnce plan (QAPI i ~ s ~ ATTACHMENTl OENISO~ .1.4..4 WHITE l\IESA URANIUM MILL Attachment 1 .,. See instruction MINES fIELD DATA WORKSHEET FOR GROUND WATER De~riptionof~~li~E~~: ~1~/_~_·~a~~M~r b~y~N~/~~u5~k~.~~~~~~~~~~~~~~~~~~ Sampler Name and initials: I .t?Y t4N /4Zm PtL. Location (well name):I,-~,-,z N~N..¥-._6~("L"--__ ~~ ___ --J Date and Time for Pllr8in~-+I;1.yj;?z>tf L~/I and Sampling (if different) 111.i?S/.2 (J If Well Purging Equip Used: [9] pump o@ bailer Well Pump (if other than Bennet) l/t£«ad Gs Sampling Event I Qwk(j N, 'frLJ.[, pH Buffer 7.0 I 10 I Prevo Well Sampled in Sampling Event 1'-_______ ----1 Specific Conductancel 111 I ~MHOS/cm Depth to Water Before Purging!1-___ -...I Conductance (avg) pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (nvg) 4" WeU:c===J(.653h) 3" Well:~(.367h) Well Waler Temp. (avg) Redox Potential (E~)~I ___ --' TurbiditylL-___ -' Weather Condo Ext" Amb. Temp. ·C (prior sampling event) 1-' __ ..... Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I , Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pH I I Temp.oC I I Temp,oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesil Mill Field Data Worksheet for Groundwater A 10f2 capturx' COII'ATltlE W"H,.,.,..~W--FUNCt'ONALlTY · . Mill . (jro~ndw.ter ~sch8rge Pt!(mit 'Groundwater Monitoring Quality Iusur;lnCe Plan (O,AP) Date: 03/22/2010 A,y. 6 Volume of Water Purged .... 1 _____ -' gallon(s) Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1..-1 ____ -' T=2V/Q= 1 I Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L.. _______ ---' : :Ii ~ Type of Sam pic VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specifY) d/(j(l.;J~ aComment Sample Taken Sample Vol (indicate if other than as y N specified below) D D 3x40ml iii 0 lOOml 0 0 250ml 0 0 250ml 0 0 1,000 mJ iii 0 Sample volume '--_______ --'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Filtered Preservative Preservative Added y N Type y N D 0 HCL 0 0 0 ~ H2SO4 ~ 0 0 0 RN03 0 0 0 0 No Preserv. 0 0 0 0 HN03 0 0 0 .m 0 a If preservative is used, specify Type and Quantity of Preservative: See instruction I A 20f2 capturx' CO ... ATlBU WIT"./'"UU'..v-.UHCTIONALITY TabC Kriged Current Quarter Groundwater Contour Map and Depth to Water Summary TIME WELL 1458 MW-1 839 MW-2 942 MW-3 943 MW-3A 912 MW-5 909 MW-11 915 MW-12 859 MW-14 857 MW-15 939 MW-17 1456 MW-18 1452 MW-19 1432 MW-20 1438 MW-22 842 MW-23 829 MW-24 903 MW-25 1252 MW-26 826 MW-27 834 MW-28 921 MW-29 922 MW-30 926 MW-31 934 MW-32 848 MW-33 853 MW-34 846 MW-35 Comments: Static level 65.29 109.93 83.50 85.55 106.09 89.37 108.76 104.00 106.75 76.04 74.90 51.30 83.97 67.32 117.43 114.81 74.91 78.68 51.09 77.29 102.58 76.83 69.03 76.56 Dry 108.20 112.67 Quarterly Depth to Water NAME: Garrin Palmer, Ryan Scheirman DATE: 2/28/2011 TIME WELL 1004 MW-4 1001 TW4-1 1007 TW4-2 900 TW4-3 1258 TW4-4 1012 TW4-5 956 TW4-6 1005 TW4-7 932 TW4-8 1010 TW4-9 1015 TW4-10 1016 TW4-11 906 TW4-12 909 TW4-13 912 TW4-14 1252 TW4-15 1020 TW4-16 934 TW4-17 1522 TW4-18 1320 TW4-19 1248 TW4-20 1524 TW4-21 1026 TW4-22 928 TW4-23 1024 TW4-24 925 TW4-25 952 TW4-26 Static Level 75.33 63.84 67.11 49.63 69.05 57.15 70.80 67.14 66.90 54.96 57.10 58.20 39.58 46.84 87.99 78.68 64.76 76.56 57.72 81.03 69.35 59.82 54.51 65.83 56.05 46.73 64.52 TIME 1447 1500 1503 932 934 1513 1000 1005 1406 1523 1039 1518 1021 1245 1250 1422 1418 1302 1311 1254 1407 1400 1012 1431 All depths were checked. WELL PIEZ-1 PIEZ-2 PIEZ-3 PIEZA PIEZ-5 TWN-1 TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 TWN-14 TWN-15 TWN-16 TWN-17 TWN-18 TWN-19 Static Level 62.04 17.20 41.96 48.92 43.91 49.80 16.05 31.61 38.18 70.10 74.78 89.58 61.81 63.91 81.38 69.57 33.89 46.68 62.79 92.45 48.50 34.59 58.10 52.87 o MW-22 .5450 0 5555 PIEZ-1 Q 5593 TWN-4 <> 5604 TW4-26 ~5537 MW-34 -9-5492 SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl PROPERTY BOUNDARY ~ MW-20 $.teO 57 3000 MW-01 e5582 MW-18 e5583 05586 lWN-10 05584 lWN-9 lWN-11 lWN.1i 1 ~1~ ~~ &6~O PIEZ-f1 ~---_--.u 115593 696'0 MW-22 ""- 50 '" II // // // // // // // // // // temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells temporary perched nitrate monitoring well showing elevation in feet amsl temporary perched monitoring well installed May, 2010 showing elevation in feet amsl perched monitoring well installed August/September, 2010 showing elevation in feet amsl HYDRO GEO CHEM,INC. APPROVED KRIGED 1 st QUARTER, 2011 WATER LEVELS WHITE MESA SITE DATE REFERENCE FIGURE SJS H:1718000/may11/wI0211.srf ( TabD Kriged Previous Quarter Groundwater Contour Map o MW-22 .5450 0 5555 PIEZ-1 ~ 5594 TWN-4 <> 5604 TW4-26 ~5537 MW-34 -9-5492 PROPERTY BOUNDARY TWN·11 TWN"i' , 0561~ 0 5'1 56'1.0 SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl MW-02 e5S03 ~ MW·20 ~PO e5457 u, 3000 temporary perched nitrate monitoring well showing elevation in feet amsl temporary perched monitoring well installed May, 2010 showing elevation in feet amsl perched monitoring well installed August/September, 2010 showin elevation in feet amsl MW-01 e55S2 MW·18 e5587 05586 TWN·10 05584 TWN·9 PIEZ·1 ~----.lJ. "5594 ~ ~12 05604 -4 ______ ---------55 b-=--=-"::::::..-------~ r/, -_____ _ ~~-::::-~ 8.,6'0 MW·22 ""-.5450 '\. II // // // // // // // // // // NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells HYDRO GEO KRIGED 4th QUARTER, 2010 WATER LEVELS WHITE MESA SITE CHEM, INC. APPROVED DATE REFERENCE FIGURE SJS H:/718000/feb11/wI1210.srf TabE Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells ~ ~/90/90 ~H9G/ZO -c. E o ~/O~/SO .c ~ -CD E i= o~/zO/9O ... CD > 0 -~ CD O~/Zlno ..J ... CD ... ~ / < ------"r"" • 60/v~/O~ Z ~ 60/90/LO - ao/sz/cO SO/s~/z~ .0 ~ / \ / • / ~ "" 1\ If V V ~ v o g It) ci It) N (}l o Depth Below Measuring Point (ft.) ...... (}l o t .~ " ~ II / ~ ~ o o - 12/18/08 03/28/09 07106/09 10/14/09 01/22/10 05/02/10 08/10/10 11/18/10 02/26/11 06/06/11 ~ Z I I\) :e a CD ~ I CD ~ -0 ~ ~ ::! 3 CD ~ C" -3 "'C - -c. E -.c ~ -CD E i= .... CD > a -CD > CD ..J .... 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E -Jl ~ -G) E .-O~/OHeO t-... ~ 0 a; > CD ..J .... 0~/ZO/9O CD .. ~ Q 'l""" • Z ~ O~/ZZHO 601vHO~ - 60/90lLO - 1\ '\ \ \ '" ~ ~ ~ co N co o M 00 -Q. E .c ;:: -CD E ~ ... CD > 0 -CD > CD ..J ... CD ... ~ or" or" I Z ~ ~ ~/90/90 ~ ~/9lll0 O~/9~H ~ O~/O~/9O O~/lO/9O O~/ll/~O 60/tr~/O ~ 60/901LO - - o a> <0 l / ~ 1\ t II ~ ~ ~ ~. ~ ~ ~ ~ a> 0 a ~ <0 ~ ~ ~ ("Jj) lU!Od 6u!Jnseew MOleg LlJde(] ~ ~/90/90 ~ -o ~/B ~n ~ - Q. E -.c = -CI) E .-O~/O~/9O .... ... CI) > 0 1\ CI) > CD ..J ... O~/ZO/9O CI) 'tU 3: N ... • Z ~ o ~/ZZHO ~ ~ ~ - 1\ 60Iv~/O~ eO/90/LO o 0 0 q 0 ~ ~ ~ 00 m M M M M M (':y) ~LJ!Od 6u!.Jnseell\l MOles lI~dea ~ ~/90/90 ~ ~/9Z/Z0 -/ -O~/B ~H ~ Q. E -.c = -CD E i= o ~/O ~/BO L. CD > 0 -CD > CD ...J L. 0~/Z0/90 CD -~ M or- ~ ~ . ~ ~ V -V V -~ ~ '" I Z ~ O~/ZZHO ~ ~ ~ ~ '"'...... 601v~/0 ~ 60/90lLO ~ ro m ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ('U) lU!Od BU!Jnseaw MOlag l,ndaa ~ ~/90/90 ~ ~/9lll0 -O~/IHH ~ Q. E ~ -..a ~ -(I) E t= O~/O~/9O ... (I) > 0 Ci) i; ..J ... 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CD i 05/02/10 It ..... r-~. !.. 0 < CD ... 08/10/10 ::! 3 CD ~ C" -3 "C 11/18/10 - 02/26/11 06/06/11 01 01 o Depth Below Measuring Point (ft.) " ~ ~ 01 W o - - - - - 07/06/09 10/14/09 01/22/10 ~ Z I ...Ii. co ~ .. 05/02/10 CD .., r CD < !!. 0 < CD ., 08/10/10 ::! 3 CD -= . cr -3 "C 11/18/10 - 02/26/11 06/06/11 TabF Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Water Levels and Data over Time White Mesa Mill -Well TWN-l Total 01' Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Dale Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,646.96 5,648.09 1.13 112.5 5,600.38 02/06/09 47.71 46.58 5,599.99 07/21109 48.10 46.97 5,600.26 09121/09 47.83 46.70 5,601.10 10128/09 46.99 45.86 5,602.59 12114/09 45.50 44.37 5,600.55 031'11/10 47.54 46.41 5,600.66 05/] 1110 47.43 46.30 5,599.18 09/29/10 48.91 47.78 5,598.92 12121/10 49.17 48.04 5,598.29 02/28/11 49.80 48.67 Water Levels and Data over Time White Mesa Mill-Well TWN-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water DepUIOr (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,625.75 5,626.69 0.94 95 5,611.37 02/06/09 15.32 14.38 5,610.63 07121109 16.06 15.12 5,609.73 09/21109 16.96 16.02 5,607.08 11102/09 19.61 18.67 5,606.57 12/14/09 20.12 19.18 5,612.45 0311 LllO 14.24 13.30 5,612.78 05/1lJ I0 13.91 12.97 5,611.37 09/29110 15.32 14.38 5610.24 12/21110 16.45 15.51 5,610.64 02128/11 16.05 15.11 Water Levels and Data over Time White Mesa Mill-Well TWN-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSn) Well 5,633.64 5,634.50 0.86 11 0 5,603.77 02/06/09 30.73 29.87 5,602.37 07121109 32.13 31.27 5,602.34 09121109 32.16 31.30 5,602.60 10128/09 31.90 31.04 5603.12 12/14/09 31.38 30.52 5602.90 03/11110 31.60 30.74 5,603.23 05/11110 3 1.27 30.41 5,602.86 09/29/10 3 1.64 30.78 5603.35 12121110 3 1.15 30.29 5602.89 02/28/11 31.61 30.75 Water Levels and Data over Time White Mesa Mill-Well TWN-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Deptb Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blwLSD) Well 5,641.04 5,641.87 0.83 136 5,601.47 02/06/09 40.40 39.57 5,604.26 07/21109 37.61 36.78 5,605.02 09/2 1/09 36.85 36.02 5,605.87 10/28/09 36.00 35.17 5,605.81 12114/09 36.06 35.23 5,605.31 03111 /10 36.56 35.73 5,605.36 05/11110 36.51 35.68 5,604.59 09129/)0 37.28 36.45 5,604.42 12/21110 37.45 36.62 5,603.69 02/28111 38.18 37.35 Water Levels and Data over Time White Mesa Mill-Well TWN-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Deptb Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.L D) Well 5,653.70 5,655.18 1.48 155 5,584.43 08/25109 70.75 69.27 5,584.51 09/21 /09 70.67 69.19 5,584.54 11 /10/09 70.64 69.16 5584.62 12114/09 70.56 69.08 5,584.97 03/11110 70.21 68.73 5,585.38 05/11110 69.8 68.32 5,585.35 09/29/10 69.83 68.35 5585.42 12/21110 69.76 68.28 5,585.08 02/28/1 J 70.1 68.62 Water Levels and Data over Time White Mesa Mill-Well TWN-6 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,663.03 5,664.94 1.91 135 5,589.52 08/25/09 75.42 73.51 5,589.46 09122/09 75.48 73.57 5,589.6J 1l!03/09 75.33 73 .42 5,589.92 12/14/09 75.02 73 .11 5,590.24 0311 1110 74.70 72.79 5,590.40 05/11/10 74.54 72.63 5,590.24 09/2911 0 74.70 72.79 5,590.49 12/2111 0 74.45 72.54 5,590.16 02128/11 74.78 72.87 Water Levels and Data over Time White Mesa Mill-Well TWN-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,647.39 5,649.26 1.87 120 5,552.56 08/25109 96.70 94.83 5,558.34 09121109 90.92 89.05 5,558.82 11 /10109 90.44 88.57 5,558.96 [2/14/09 90.30 88.43 5559.54 03/11110 89.72 87.85 5,559.60 05/11110 89.66 87.79 5,559.83 09/29/10 89.43 87.56 5,559.00 L2/21 /10 90.26 88.39 5559.68 02/28/1 I 89.58 87.71 Water Levels and Data over Time White Mesa Mill-Well TWN-8 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WeU 5,649.35 5,651.48 2.13 160 5,589.01 08/25/09 62.47 60.34 5,589.10 09/2Il09 62.38 60.25 5,589.09 11/03/09 62.39 60.26 5603.38 12/14/09 48.10 45.97 5589.68 03/11/10 61.80 59.67 5,589.95 05/11 /10 61.53 59.40 5,589.74 09129/10 61.74 59.61 5,589.97 12/2111 0 61.51 59.38 5589.67 02/28/U 61.8J 59.68 Water Levels and Data over Time White Mesa Mill-Well TWN-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WelJ 5,645.68 5,647.45 l.77 102.5 5,582.05 08125109 65.40 63.63 5,582.1 2 09/22/09 65.33 63.56 5,582.27 11110/09 65.18 63.41 5,582.53 12114/09 64.92 63.15 5,582.92 0311 1110 64.53 62.76 5,583.06 05/1111 0 64.39 62.62 5,583.25 09129/10 64.20 62.43 5,583.57 1212 1/10 63.88 62.1 1 5,583.54 02/28/11 63.91 62.14 Water Levels and Data over Time White Mesa Mill-Well TWN-IO Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Ele~ation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WeU 5,664.63 5,666.98 2.35 107.5 5584.18 08/25/09 82.80 80.45 5,584.40 09122/09 82.58 80.23 5,584.61 1)/)0/09 82.37 80.02 5,584.90 12/14/09 82.08 79.73 5,585.21 03/11110 81.77 79.42 5585.42 05/11/10 81.56 79.21 5,585.42 09/29/10 81 .56 79.21 5,585.68 12/21110 81.3 78.95 5585.60 02/28/11 81 .38 79.03 Water Levels and Data over Time White Mesa Mill-Well TWN-ll Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (bhv.LSD) Well 5,.683.16 5,684.53 1.37 147.5 5613.00 11 /03/09 71.53 70.16 5,613.88 12114/09 70.65 69.28 5,614.65 03/11 /10 69.88 68.51 5,615.16 05/11110 69.37 68 .00 5,614.93 09129110 69.60 68.23 5,615.09 12/21110 69.44 68.07 5,614.96 02/28111 69.57 68.20 Water Levels and Data over Time White MesaMill-Well TWN-12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth or (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WeU 5,667.03 5,668.24 1.21 115 5628.33 11103/09 39.91 38.70 5628.86 12114/09 39.38 38.17 5,630.27 03/11110 37.97 36.76 5631.64 05/11/10 36.60 35.39 5,633.73 09/29/10 34.51 33.30 5,633.43 12/21 /10 34.81 33.60 5,634.35 02/28/11 33.89 32.68 Water Levels and Data over Time White Mesa Mill -Well TWN-13 Total or Measuring Measured Total Water Land Point Depth to Deptb to Total Elevation Surface Elevation Length Of Date Of Water Water DeptllOf (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,633.04 5,634.32 1.2 120 5,586.95 11103/09 47.37 46.09 5,587.22 12/14/09 47.1 45.82 5,587.45 03/11 /10 46.87 45.59 5,587.64 05111/1 0 46.68 45.40 5587.37 09/29/10 46.95 45.67 5,587.77 12/21110 46.55 45.27 5,587.64 02/28/11 46.68 45.40 Water Levels and Data over Time White Mesa Mill-Well TWN-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water DepHt Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,647.80 5,649.53 1.73 135 5,586.18 11104/09 63.35 61.62 5,586.5 1 12114/09 63.02 61.29 5,586.71 03/11/10 62.82 61.09 5,586.72 05/11110 62.81 61.08 5,586.53 09129110 63.00 61.27 5,586.80 1212 1/10 62.73 6 1.00 5,586.74 02/28/11 62.79 6 1.06 Water Levels and Data over Time White Mesa Mill-Well TWN-15 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WelJ 5,675.01 5676.49 1.48 155 5,594.12 11 /10109 82.37 80.89 5,584.03 12/14/09 92.46 90.98 5584.10 03111110 92.39 90.91 5584.1 6 05/11 /10 92.33 90.85 5,584.26 09/29/10 92.23 90.75 5,584.30 12/21110 92.19 90.71 5,584.04 02/28/11 92.45 90.97 Water Levels and Data over Time White Mesa Mill-Well TWN-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Su.rface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSJ)) Well 5,651.07 5,652.70 1.63 100 5,603.34 11104/09 49.36 47.73 5,603.56 12/14/09 49.14 47.5l 5,603.84 03/11110 48.86 47.23 5,604.31 05/11110 48.39 46.76 5,604.28 09/29/10 48.42 46.79 5,604.39 12/21110 48.31 46.68 5,604.20 02/28/11 48.50 46.87 Water Levels and Data over Time White Mesa Mill-Well TWN-17 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Deptll Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WeU 5,639.73 5,641.55 1.82 100 5,605.96 11104/09 35.59 33.77 5,606.27 12/14/09 35.28 33.46 5,606.25 03/11/10 35.30 33.48 5,606.55 05111110 35.00 33.18 5,606.77 09129110 34.78 32.96 5,607.15 12121/10 34.40 32.58 5,606.96 02/28111 34.59 32.77 Water Levels and Data over Time White Mesa MiII-Well TWN -18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (bhv.MP) (blw.LSD) Well 5,643.95 5,645.45 1.50 100 5586.85 11102/09 58.60 57.10 5600.14 12/14/09 45.31 43.81 5,587.36 03/11/10 58.09 56.59 5,587.71 05/11110 57.74 56.24 5587.50 09/29110 57.95 56.45 5,607.66 12/21 /10 37.79 36.29 5,587.35 02/28111 58.10 56.60 Water Levels and Data over Time White Mesa Mill -Well TWN-19 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (bhv.MP) (blw.LSD) Well 5659.59 5,661.36 1.77 110 5,606.17 11102/09 55.19 53.42 5,606.70 12114/09 54.66 52.89 5,607.22 03/11110 54.14 52.37 5,607.89 05111110 53.47 51.70 5,607.98 09129/10 53.38 51.61 5,608.4 1 12/21110 52.95 51.18 5,608.49 02/28111 52.87 51.10 TabG Laboratory Analytical Reports --------------EI\ERGY ..... AUC"; '1/\'1 (11 ~ r. '':; ml" www.energylab.com AM/yticII Em/ltrlct Slm:.,11l2 Helena, MT 877·472·0711 • Billings, MT 800·735-4489 • Casper, WY 888·235-0515 Gillette, WV 116-&8&-7175 • Rapid City, SO 888-672·1225 • College station, 1X 888-&90-2218 February 15, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11020080 ANALYTICAL SUMMARY REPORT Quote ID: C3317 -Nitrate and Chloride Sampling Project Name: 1 st Quarter Nitrate 2011 Energy Laboratories, Inc. Casper WY received the following 17 samples for Denison Mines USA Corp on 2/2/2011 for analysis. Sample ID Client Sample 10 Collect Date Receive Date Matrix Test C11020080-001 TWN-11 01 /27/11 09:01 02/02/11 Aqueous Chloride Nitrogen, Nitrate + Nitrite C11020080-002 TWN-18 01/27/11 10:55 02/02/11 Aqueous Same As Above C11020080-003 Pond D 01 /31/11 13 :25 02/02/11 Aqueous Same As Above C11020080-004 TWN-16 01/27/11 12 :43 02/02/11 Aqueous Same As Above C11020080-005 TWN-14 01 /28/11 08 :20 02/02/11 Aqueous Same As Above ------- C11020080-006 TWN-19 0210 1111 07 :45 02/02 /11 Aqueous Same As Above C11020080-007 TWN-17 02/01/11 07 :59 02/02/11 Aqueous Same As Above C11020080-008 TWN-9 02/01 /11 08 :09 02/02/11 Aqueous Same As Above C 11020080-009 TWN-3 02/01/11 08 :22 02/02/11 Aqueous Same As Above C11 020080-01 0 TWN-2 02/01/11 08:33 02/02/11 Aqueous Same As Above C11020080-011 Piez 1 01/31/11 13 :05 02/02/11 Aqueous Same As Above C11020080-012 Piez 2 01/31/11 13:40 02/02 /11 Aqueous Same As Above C11020080-013 Piez 3 01 /31 /11 13 :55 02/02/11 Aqueous Same As Above C11020080-014 UWLP 01 /31/11 13 :25 02/02/11 Aqueous Same As Above C11020080-015 TWN-60 02/01 /11 08 :40 02/02/11 Aqueous Same As Above C11020080-016 TWN-19R 01 /31 /11 07 :36 02/02/11 Aqueous Same As Above C 11020080-017 Temp Blank 02/01 /11 00 :00 02/02/11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~J) uJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.02.1513:06:09 -07:00 Page 1 of 12 www.energylab.com AM/tfIaI EruIIftI:t .. 7151 Helena, MT B77-472-0711 • Billings, MT BOO-735-4489 • Caspar, WY 888-235-0515 Gillette WY 856-186-7175 . Ra Id CI so 888-672-1225 • Colle a Station TX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 1 st Quarter Nitrate 2011 Report Date: 02/15/11 Sample Delivery Group: C11020080 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EN:RGY :\I ,OIU ... 1CHII ! .. .' www.energylab.com ~~IhIt:.tm Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8BB-I8B-7175 . Rapid City, SD 188-672-1225 . CollegeStalion, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Site Name: 1 st Quarter Nitrate 2011 Lab ID: C11020080-001 Client Sample ID: TWN-11 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C11020080-002 Client Sample ID: TWN-18 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C11020080-003 Client Sample ID: Pond D Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C11020080-004 Client Sample ID: TWN-16 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report Rl -Analyte reporting limit. Definitions: QCl -Quality conlrollimit. Result 84 1.4 Result 61 1.4 Result 3 0.1 Result 34 4.6 D -Rl increased due to sample matrix. Units mg/l mg/l Units mg/l mg/l Units mg/l mg/l Units mg/l mg/l Report Date: 02/15/11 Collection Date: 01/27/11 09:01 DateReceived: 02/02/11 MeL! Qualifiers Rl Qel Method Analysis Date I By 1 A4500-CI B 02109/11 15:43/1r 0.1 E353.2 02/04/1115:19/dc Collection Date: 01/27/1110:55 DateReceived: 02/02/11 Mell Qualifiers Rl Qel Method Analysis Date I By 1 A4500-CI B 02/09/11 15:47/1r 0.1 E353.2 02/04/11 15:21 I dc Collection Date: 01/31/11 13:25 DateReceived: 02/02/11 MeL! Qualifiers Rl Qel Method Analysis Date I By A4500-CI B 02/09/11 15:50 Ilr 0.1 E353.2 02104/11 15:241 dc Collection Date: 01/27/1112:43 DateReceived: 02/02/11 MeL! Qualifiers Rl Qel Method Analysis Date I By A4500-CI B 02/09/11 15:52/1r D 0.5 E353.2 02/04/11 15:261 dc MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 12 EN:RGY •• '\{'()H':~I OHlI ~ www.energyiab.com WI!fIaI baJIHa SIIIu 1m Halena, lIT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WI( 888-235-0515 Gillette, WI( 8&6-186-7175 • Rapid City, SD 188-&12-122!1 • College StatiDn, TX 188-&10-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Lab 10: Denison Mines USA Corp 1 st Quarter Nitrate 2011 Cll020080-005 Client Sample 10: TWN-14 Matrix: Aqueous Analyses Result Units MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: Cl1020080-006 Client Sample 10: TWN-19 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: Cl1020080-007 Client Sample 10: TWN-17 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C 11020080-008 Client Sample 10: TWN-9 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. 24 3.7 Result 114 7.0 Result 90 B.6 Result 217 9.5 0-Rl increased due to sample matrix. mg/l mg/l Units mg/l mg/l Units mglL mg/l Units mg/L mg/L Qualifiers RL o 0.5 Qualifiers RL D 0.5 Qualifiers RL 1 D 0.5 Qualifiers RL 1 D 0.5 MCU Report Date: 02/15/11 Collection Date: 01/28/11 08:20 OateReceived: 02/02/11 QCL Method Analysis Date 1 By A4500-CI B 02/09/11 15:541 Ir E353.2 02/04/11 15:291 de Collection Date: 02/01/11 07:45 DateReceived: 02/02/11 MCL! QCL Method Analysis Date 1 By A4500-CI B 02/09/11 15:591 Ir E353.2 02/04/11 15:391 de Collection Date: 02/01/11 07:59 DateRecelved: 02/02/11 MCL! QCL Method Analysis Date 1 By A4500-CI B 02/09/11 16:031 Ir E353.2 02/04/11 15:411 de Collection Date: 02/01/11 08:09 DateReceived: 02/02/11 MCLI QCL Method Analysis Date 1 By A4500-CI B 02/09/11 16:051 Ir E353.2 02104/11 15 :46 1 de MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 12 EN:RGY • ;\1 !()I~/~rOIIIt.·, www.energylab.com Au/yfIaI r-IInI:I smc. 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-186-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 1 st Quarter Nitrate 2011 Lab ID: C11020080-009 Client Sample ID: TWN-3 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C11 020080-01 0 Client Sample ID: TWN-2 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C11020080-011 Client Sample ID: Piez 1 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C11020080-012 Client Sample ID: Piez 2 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. Result Units 138 mg/l 24 mg/l Result Units 93 mg/l 43 mg/l Result Units 60 mg/l 7 mg/l Result Units 9 0.3 mg/l mg/l D -Rl increased due to sample matrix. Qualifiers Rl D Qualifiers Rl D 2 Qualifiers Rl D Qualifiers Rl 0.1 Report Date: 02/15/11 Collection Date: 02/01/11 08:22 DateReceived: 02/02/11 MeL! Qel Method Analysis Date I By A4500-CI B 02109/11 16:07/1r E353.2 02/04/11 15:491 dc Collection Date: 02/01/11 08:33 DateReceived: 02/02/11 MeL! Qel Method Analysis Date I By A4500-CI B 02/09/1116:12/1r E353.2 02/04/11 15:511 dc Collection Date: 01/31/11 13:05 DateReceived: 02/02/11 Meu Qel Method Analysis Date I By A4500-CI B 02/09/11 16:18/1r E353.2 02/04/11 15:591 dc Collection Date: 01/31/1113:40 DateReceived: 02/02/11 MeU Qel Method Analysis Date I By A4500-CI B 02/09/11 16:20/1r E353.2 02/04/11 16:011 dc MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 5 of 12 EN:RGY • I\\--JOHf.' OHI' ...... www.energylab.com AM/tfIaI buIINI:t ~ '151 Helena, MT 877-472-0711 • Billings, MT 8OD-735-4489 • Casper, WY 88B-235-D515 Gillette, WY BI6-186-7175 • Rapid City, SO 888-&72-1225 • Coliege Station, 1X 888-&8D-221 a LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: LablD: Denison Mines USA Corp 1 st Quarter Nitrate 2011 C11020080-013 Client Sample ID: Piez 3 Matrix: Aqueous Analyses Result Units MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C11020080-014 Client Sample ID: UWLP Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N LablD: C11020080-015 Client Sample ID: TWN-60 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C11020080·016 Client Sample 10: TWN-19R Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report Rl -Analyte reporting limit. Definitions: QCL • Quality control limit. 40 1.8 mg/l mg/L Result Units 0.1 Result ND ND Result ND 0.8 mg/L mg/L Units mg/L mg/L Units mg/L mg/L D -RL increased due to sample matrix. Qualifiers RL D 0.2 Qualifiers RL 0.1 Qualifiers RL 0.1 Qualifiers RL 0.1 MCU Report Date: 02/15/11 Collection Date: 01/31/11 13:55 DateReceived: 02/02/11 QCL Method Analysis Date I By A4500-CI B 02/09/11 16:23 / Ir E353.2 02/04/11 16:041 dc Collection Date: 01 /31 111 1 3 :25 DateReceived: 02/02/11 MCU QCL Method Analysis Date I By A4500-CI B 02/09/11 16:25 Ilr E353.2 02/04/11 16 :06 / dc Collection Date: 02/01/11 08:40 DateReceived: 02/02/11 MCU QCL Method Analysis Date / By A4500-CI B 02/09/11 16:27/1r E353.2 02/04/11 16:091 dc Collection Date: 01/31 /11 07:36 DateRecelved: 02/02/11 MCU QCL Method Analysis Date I By A4500-CI B 02/09/11 16:28/1r E353.2 02/04/11 16:191 dc Mel -Maximum contaminant level. ND -Not detected at the reporting limit. Page 6 of 12 EN:RGY .' • ,\110r-~/\1 Of4lL: .. www.energy1ab.com AMIftkM~Sbtu 1151 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-D515 Gillette, WY 8&6-188-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-&9D-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Lab 10: Denison Mines USA Corp 1 st Quarter Nitrate 2011 C11020080-017 Client Sample 10: Temp Blank Matrix: Aqueous Analyses Result Units PHYSICAL PROPERTIES Temperature Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. 2.0 Qualifiers RL MCL! Report Date: 02/15/11 Collection Date: 02/01/11 DateReceived: 02/02/11 QCL Method Analysis Date / By E170.1 02/02/11 09:45 / kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 7 of 12 EN:RGY www.enefgylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GIIIBlta, WY 8&&-186-7175 • Rapid City, SO 188-&72-1225 . College Station, TX 888-&80-2218 /\1..0IU\i OJ"':! ~ AMlft/ClI EXulIatw SiIu 1151 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter Nitrate 2011 Analyte Count Result Units Method: A4500-C1 B Sample 10: MBLK9-110209 Chloride Sample 10: C11020080·009AMS Chloride Sample 10: C11020080·009AMSO Chloride Sample 10: C11020080·016AMS Chloride Sample 10: C11020080·016AMSO Chloride Sample 10: LCS35-110209 Chloride Qualifiers: RL -Analyte reporting limit. Method Blank ND mg/L Sample Matrix Spike 496 mg/L Sample Matrix Spike Duplicate 496 mg/L Sample Matrix Spike 35.5 mg/L Sample Matrix Spike Duplicate 35.1 mg/L Laboratory Control Sample 3580 mg/L Report Date: 02/15/11 Work Order: C11020080 RL %REC Low Limit High limit RPO RPOLimlt Qual Batch: 11 0209-CL-TTR-W Run: TITRATION_11 0209A 02109/11 15:23 0.5 Run : TITRATlON_110209A 02/09/11 16:08 1.0 101 90 110 Run: TITRATION_110209A 02/09/11 16:10 1.0 101 90 110 0.0 10 Run: TITRATION_110209A 02/09/11 16:30 1.0 100 90 110 Run : TITRATION_110209A 02/09/11 16:32 1.0 99 90 110 1.0 10 Run: TITRATION_110209A 02/09/11 16:34 1.0 101 90 110 ND -Not detected at the reporting limit. Page 8 of 12 EN:RGY • ,'\i .. DH.\.!\.:I-lIL ·: rmr Client: Denison Mines USA Corp Project: 1 st Quarter Nitrate 2011 --- Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SO 888-572-1225 • College Station, 1J( 888-610-2218 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 02/15/11 Work Order: C11020080 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual Method: E353.2 Batch: R142502 Sample 10: MBLK-1 Method Blank Run: TECHNICON_11 0204A 02/04/11 13:59 Nitrogen, Nitrate+Nitrite as N 0.07 mg/L 0.06 Sample 10: LCS-2 Laboratory Control Sample Run: TECHNICON_110204A 02104/11 14:01 Nitrogen, Nitrate+Nitrite as N 2.47 mg/L 0.10 96 90 110 Sample 10: C110200aO-OO3BMS Sample Matrix Spike Run: TECHNICON_11 0204A 02/04/1115:31 Nitrogen, Nitrate+Nitrite as N 2.06 mg/L 0.10 98 90 110 Sample 10: C110200aO-OO3BMSO Sample Matrix Spike Duplicate Run: TECHNICON_110204A 02/04/11 15:34 Nitrogen, Nitrate+Nitrite as N 2.03 mg/L 0.10 96 90 110 1.5 10 Sample 10: C110200aO-015BMS Sample Matrix Spike Run: TECHNICON_11 0204A 02104/11 16:11 Nitrogen, Nitrate+Nitrite as N 2.16 mg/L 0.10 104 90 110 Sample 10: C110200aQ-015BMSO Sample Matrix Spike Duplicate Run: TECHNICON_l1 0204A 02/04/11 16:14 Nitrogen, Nitrate+Nitrite as N 2.12 mg/L 0.10 102 90 110 1.9 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. Page 9 of 12 EI'-ERGY L AUOP/\l CJ ~11 ':.; www.energylab.com ~ £ruIII4u SUu 1/151 Helena, MT877-472-0711 • Billings, MTSOO-735-44S9 . Casper, WY 888-235-0515 Gillette, WY 86&-&86-7175 • Rapid City, SO 888-112-1225 . College Slalion,1X 888-&90-2218 Workorder Receipt Checklist Denison Mines USA Corp IIIII~IIIIIIII~ ~IIIIIIII~II ~IIIIIIIIIII~ II111II1 C11020080 Login completed by: Halley Ackerman Reviewed by: BL2000\kschroeder Reviewed Date: 2/3/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper containerlbottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water-pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes III Yes III Yes D Yes III Yes III Yes III Yes III Yes III Yes III Yes III 2"C On Ice Yes D Yes III Date Received: 2/2/2011 Received by: ha Carrier name: FedEx No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present III No VOA vials submitted III Not Applicable D Page 10 of 12 o -...... f\) LABOI?A TORIES PLEASE PRINT (Provide as much information as possible.) Chain of Custody and Analytical Request Record Page --I-of --..L com~~ame: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: . <.. 1 {;Ai ,'",o,J (V},:V~ J ~-r OL1t)~1w Af; Juk. 2&// State: £AI Yes ~ No 0 Contact Name: Phone/Fax: Email: Sampler: (Please Print) ReportMaii Addresk felt' -~~ >sur (2144,1.. {l4~ b rK' ("cZ-{ 'G;1lf(r J-i1AIIM JL . ttf'lJ/~l ui' gLj)/J Invoice Address: ( Invoide Contact & Phone: Purchase Order: QuotelBottle Order."" ~SC(II'-( . C;:.({ IA-<-- Special Report/Formats: ~ ~&[!, 'W@D@ ~rn@(![J~rn[ID .. Contact ELI prior to ~~<i~ 0 L. RUSH sample submittal ~o en~ i=' for charges and Cooler ID(9): ~[D;gOI Q; 0 <2: R scheduling -See G~ --> 0 >Oro W C Instruction Page Dow D EOO/EOT(Electronic Data) l!lCl)CI) m~ C en en I o~= ~ 0> ~ "0 Receipt Temp D POTWIWWTP <..> c Comments: Format: U <cbkQ .s ::l U 2. '0 L.[DI~ ~ ~ a °c D State: D LEVEL IV ~ Qj~ c-.:: iii ~o..moCl C D Other: D NELAC ~I~' r 5 On Ice: GJN ::l 0)-= Q) ~ <t: f-5 za.<CIg>Cl .,.. ~ W 'E Custody Seal 15 >1 W til On Bottl. Y N ~ (f) "0 §: U) I~ c On Cooler ~ til en H Intact SAMPLE IDENTIFICATION Collection Collection MATRIX Signature (Name, Location, Interval, etc_l Date Time Match 1 _lIvlV-/J I,LI·/f ()liIJ"I 1-W X-X ~ 2 J7.,,,vN -1}( 1-21--11 //J/)"S l.. -iAJ X X ~ apcnci D ',,"S/·1/ 13;t~ 2-rAJ X ,x g nnn 4 TlrJN -It ].21·/1 1243 :z.-w )( X ~ 5 '1JJN _I LJ f.J. f{. J I I1.k20 2-w X X ~- 6 lINN ~ Iq j.J . J I 1114S ~-vJ X V< ~ 7 TlvAl-13-1.././1 ~rS-1 :2.. -rAJ Ix X ~ B _TbfJJ-q X·/ ' II tJxtJ 1 {l-LV X lX ~ 0 9 ItVN ~ ~ It2. -/-Jl !JiZZ J:. -vJ X V\' 'ifa .~ ~ 10 7l~/\I -: 2-12-1· Jl IOt33 :2.. -lA.J X ~ t:::! Custody I Relin~~Y (PrintJ: f..tw,,·Da1~7 1'I(}I;l Si:': ReceIVed by (print): DaWlTime: Signature: I ~h. '4. , ,;).()/I R eco rd Relinquisheq by (print): D:nerTlme: '(1'ature: -Recel\W by (print): DateITrna: Signall/It!: MUST be Signed r<eC&lvea DY LaooralOry: ~~~~ ~'4") <t1\\L~ Sample Disposal: Return to Client: Lab Disposal: In certain Circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested, This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ': J jr11f7 ...... '" o ..... ...... '" I,UlM? Chain of Custody and Analytical Request Record PLEASE PRINT (Provide as much information as possible.) Page -L of .z.:... LASaRA TORIES EPNState Compliance: Yes t:J No 0 Project Na~PWS, Permit, Etc. Sample Origin / Yu Lvi~1w /U,'id/( £0 II State: GJ..--r Sampler: (Please Print) V\VJ'\( Idkt/ Report Mail Address: /) c--C; ~. v. I.:;UV)C 00! 'Sand,'u-t !AT 'xCfstl Contact Name: Phone/Fax: kv{(N A/WILy( 6."fIr /Z_2/ Email: Invoice Address: J $C(~ Invoic~ Contact & Phone: ...s~~ Quo~/Bottle Order: Purchase Order: Special Report/Formats: $: o .... t:!OCl>~ ~ t:C ;gol Q) .~;;~ rn~ ~ o EDD/EDT(Electronic Data) DDW .. 0 I=' R w ~ I Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page Cooler 10(5): ~\ D POlWlWWTP Format: ____ _ o State: o LEVEL IV o Other:----o NELAC o>=~C) ._ u> C c.!: 'k o<c~liDl~ :"" ~~t;l§(§ ~ t:~liil. .:: :J Q).!::: 1il:s: ..., ~ zCi.<Cl go J ~ !ij >1 I~ ~ (f) I_~N SAMPLE IDENTIFICATION Collection Collection MATRIX 'S:-~ (Name. Location, Interval, etc.) Date Time " ...... U « I-l-« W W en "0 c: :l U e ro Receipt Temp .? °c Comments: e: 5 l-S "E On Ice: C9 N Custody Seal ro "0 e: ro Ci5 H On BoUie V N On Cooler (r) N Intact ~ N Signature /"V., N Match \, 4 111J JL {5 1-31· II L>;<5 2 -v.J X '/. I ~ 7 1?-I.r I rl.~. \\ *: s1\' I~ 8 10 Ie::::! Stgnalure: Custody Rel~by(plintV I DateJTime: jitYO Signao/re: I -<1 MeN r 4!JJV ,r tR -/ -2..tJ/ , \ £t Receivetl by (prinll~ DatelTime: :~~r~e RelinquishfO by (print): DaleJTime: ~nature; Signed Sample Disposal: Return to Client: Lab Disposal: Signature: Received by (print): DatefTime: HeeclveO Dy Lal>Oratory: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information. downloadable fee schedule, forms, and links. Er\ERGY III I{ 'I, " I C I~' ',. www.energylab.com AIu/yffaI ~ SInw 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Caspar, WY 881-235-0515 Gillatte, WY 116-686-7175 • Rapid City, SD 888-&12-1225 • College Station, 1X 888-680-2218 February 10, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 WorkorderNo.: C11010840 Project Name: 1 st Quarter Nitrate ANALYTICAL SUMMARY REPORT Quote ID: C3317 -Nitrate and Chloride Sampling Energy Laboratories, Inc. Casper WY received the following 16 samples for Denison Mines USA Corp on 1/28/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C11 01 0840-001 TWN-8 01/25/11 14:3001/28/11 Aqueous Chloride Nitrogen, Nitrate + Nitrite C11 01 0840-002 TWN-13 01/25/1114:1801/28/11 Aqueous Same As Above C11 01 0840-003 TWN-5 01/25/11 14:4501/28/11 Aqueous Same As Above C11 01 0840-004 TWN-1 01/26/11 1 3 :51 01/28/11 Aqueous Same As Above C11 01 0840-005 TWN-12 01/26/11 14:1001/28/11 Aqueous Same As Above C11 01 0840-006 TWN-4 01/25/1114:3801/28/11 Aqueous Same As Above C11 01 0840-007 TWN-7 01/27/11 08:36 01/28/11 Aqueous Same As Above C11 01 0840-008 TWN-15 01/27/1109:0401/28/11 Aqueous Same As Above C11 01 0840-009 TWN-6 01/26/11 12:57 01/28/11 Aqueous Same As Above C11 01 0840-01 0 TWN-10 01/27/11 08:55 01/28/11 Aqueous Same As Above C11 01 0840-011 TWN-65 01/25/11 14:45 01/28/11 Aqueous Same As Above C11 01 0840-012 TWN-13R 01/24/1111 :4501/28/11 Aqueous Same As Above C11 01 0840-013 TWN-1R 01/25/11 10:1401/28/11 Aqueous Same As Above C11 01 0840-014 TWN-7R 01/26/11 09 :04 01/28/11 Aqueous Same As Above C11 01 0840-015 TWN-11R 01/27/11 08:05 01/28/11 Aqueous Same As Above C11 01 0840-016 Temp Blank 01 /27/11 00:00 01/28/11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: o¥~ £) tJtJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.02.10 15:58: 18 -07:00 Page 1 of 11 Helena, MT871·472-0711 • Billings, MT80a·135-44B9 . Casper, WY 888-235-0515 Gillette WY 866-&86·7175 • Ra Id Cit so 188-672-1225 • Colle e Slalion TX 888-&90-2218 CLIENT: Denison Mines USA Corp Project: 1 st Quarter Nitrate Sample Delivery Group: C11 01 0840 REVISED/SUPPLEMENTAL REPORT Revised Date: 02/10/11 Report Date: 02/09/11 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to a sample date correction for sample TWN-13R from 1/25/11 to 1/24/11 as per Kathy Weinel 2/10/11 . ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring . SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001 ; Utah: 3072350515; Virginia: 00057; Washington : C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 11 EI\ERGY ,'I. . )' ) F .;, I J ~ I • www.energylab.comHelena.tlT877-472-0711 .Bllllngs.MT 800-735-4489 • Casper, WY 888-235-0515 AIu/ttIIIM ~ SIIu 1m Gillette, WY 88&-&86-7175 • Rapid City, SD 888-&72-1225 • Collegs Station, IX 888-&ID-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 1 st Quarter Nitrate Lab ID: C11 01 0840-001 Client Sample ID: TWN-8 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-002 Client Sample 10: TWN-13 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11010840-003 Client Sample 10: TWN-5 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-004 Client Sample 10: TWN-1 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Report Definitions: RL -Analyte reporting limit. QCL -Quality controllimi!. Result Units 13 ND Result 103 1.6 mg/L mg/L Units mg/L mg/L Result Units 47 0.4 mg/L mg/L Result Units 17 0.5 mg/L mg/L D -RL increased due to sample matrix. Qualifiers Qualifiers D Qualifiers Qualifiers Rl 1 0.1 Rl 0.2 RL 0.1 Rl 1 0.1 MeL! Revised Date: 02/10/11 Report Date: 02/09/11 Collection Date: 01/25/11 14:30 DateRecelved: 01/28/11 Qel Method Analysis Date 1 By A4500-CI B 02/02/11 14:591 Ir E353.2 01 /31/11 13:421 de Collection Date: 01/25/11 14:18 DateRecelved: 01/28/11 MeL! Qel MeL! Method Analysis Date 1 By A4500-CIB 02/02111 15:01 /lr E353.2 01/31/11 13:441 de Collection Date: 01/25/11 14:45 OateReceived: 01/28/11 QeL Method Analysis Date 1 By A4500-CI B 02/02/11 15:031 Ir E353.2 01/31/11 13:471 de Collection Date: 01/26/11 13:51 OateRecelved: 01/28/11 MeL! Qel Method Analysis Date 1 By A4500-CI B 02/02/11 15:041 Ir E353.2 01/31/11 13:491 de MCL -Maximum contaminant level. ND -Not detected at the reporting limi!. Page 3 of 11 -. EI\ERGY .,\, ;lfl:.t cr"l. " www.energylab.com AMI!fIQ/ exuu-SitIu 1m Helena, tIT 877-472-0711 • Bllllng8, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-118-7175 • Rapid City, SD 188-&72-1225 • Colluge StatiDn, TX 888-610-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 1 st Quarter Nitrate Lab ID: C11 01 0840-005 Client Sample 10: TWN-12 Matrix: Aqueous Analyses Result Units MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-006 Client Sample 10: TWN-4 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-007 Client Sample ID: TWN-7 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-008 Client Sample 10: TWN-15 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 87 4.2 Result 21 0.9 Result 6 1.3 mgiL mg/L Units mg/L mg/L Units mg/L mg/L Result Units 43 1.4 mg/L mg/L D -RL increased due to sample matrix. Qualifiers RL D 0.2 Qualifiers Rl 1 0.1 Qualifiers RL 0.1 Qualifiers Rl , 0.1 MCL! Revised Date: 02/10/11 Report Date: 02/09/11 Collection Date: 01/26/1114:10 DateRecelved: 01/28/11 QCl Method Analysis Date 1 By A4500·CI B 02102/11 15:07 1 Ir E353.2 01 /31 /11 13 :521 de Collection Date: 01/25/11 14:38 DateRecelved: 01 /28/11 MeL! QeL Method Analysis Date 1 By A4500-CI B 02102/11 15 :09 Ilr E353.2 01/31/11 14:02 1 de Collection Date: 01/27/11 08:36 DateReceived: 01/28/11 MeL! Qel Method Analysis Date 1 By A4500-CI B 02/02/11 15:11 I lr E353.2 01/31/11 14:041 de Collection Date: 01 /27/11 09:04 DateRecelved: 01/28/11 MeL! Qel Method Analysis Date I By A4500-CI B 02/02/11 15:121 Ir E353.2 01/31 /11 14:07 1 de MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 11 EI\ERGY .\ ,,}Jjnl' HI 'J www.ellMgylab.com ~buIIa:II"'1U Helena, MT 877·472-0111 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, Yf'( 888-188-1115 • Rapid City, SD 888-&72·1225 • College Station, 1)( 888-88D-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Site Name: 1 st Quarter Nitrate Lab ID: C11 01 0840-009 Client Sample ID: TWN-6 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-01 0 Client Sample 10: TWN-10 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-011 Client Sample 10: TWN-65 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-012 Client Sample 10: TWN-13R Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result 18 1.1 Result 40 0.3 Result 45 0.4 Result NO NO Units mg/L mg/L Units mg/L mg/L Units mg/L mg/L Units mg/L mg/L Revised Date: 02/10/11 Report Date: 02/09/11 Collection Date: 01/26/11 12:57 DateRecelved: 01/28/11 MCL! Qualifiers Rl QCl Method Analysis Date! By 1 A4500-CI B 02102/11 15:1411r 0.1 E353.2 01/31/1114:09/dc Collection Date: 01/27/1108:55 OateRecelved: 01/28/11 MCL! Qualifiers Rl QCl Method Analysis Date 1 By A4500-CI B 02/02/11 15 :20 1 Ir 0.1 E353.2 01/31/1114:12/dc Collection Date: 01/25/11 14:45 DateReceived: 01/28/11 MCl! Qualifiers Rl QCl Method Analysis Date! By A4500-CI B 02/02/11 15:21 Ilr 0.1 E353.2 01/31/1114:19/dc Collection Date: 01/24/11 11 :45 OateRecelved: 01/28/11 MeLI Qualifiers Rl QCl Method Analysis Date 1 By A4500-CI B 02/02/11 15 :23 1 Ir 0.1 E353.2 01131/11 14:221 dc MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 11 EI\ERGY .. "I.; • ':)1 J ,r. r )11 • > www.energylab.com AMIytkM EzuIIfta SbIu 1m Helena, MT 817-472-0711 • BIllings, MT 800-735-4489 · Casper, WV 888-235-0515 Gillatta, WY 866-186-7175 • Rapid City, SD 188-&72-1225 • College Station, TX 888-&80-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Site Name: 1 st Quarter Nitrate Lab 10: C11 01 0840-013 Client Sample 10: TWN-1 R Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-014 Client Sample 10: TWN-7R Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nltrate+Nitrite as N Lab 10: C11 01 0840-015 Client Sample 10: TWN-11R Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C11 01 0840-016 Client Sample 10: Temp Blank Matrix: Aqueous Analyses PHYSICAL PROPERTIES Temperature Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. Result ND 0.5 Result ND 0.6 Result ND 1.4 Result 3.0 D -Rl increased due to sample matrix. Units mglL mg/l Units mg/l mg/l Units mg/l mgll Units 'C Revised Date: 02/10/11 Report Date: 02/09/11 Collection Date: 01/25/11 10:14 DateReceived: 01/28/11 MeL! Qualifiers Rl Qel Method Analysis Date 1 By , A4500-CI8 02/02111 15:241 Ir 0.1 E353.2 01 /31/11 14:241 dc Collection Date: 01/26/11 09:04 DateReceived: 01/28/11 MeL! Qualifiers Rl Qel Method Analysis Date 1 By 1 A4500-CI B 02/02111 15 :26 /lr 0.1 E353.2 01 /31 /11 14 :27 1 dc Collection Date: 01 /27/11 08:05 DateRecelved: 01/28/11 MeL! Qualifiers Rl Qel Method Analysis Date 1 By A4500-CI8 02/02/11 15:281 Ir 0 0.2 E353.2 01/3111114:29/dc Collection Date: 01/27/11 DateReceived: 01/28/11 MeL! Qualifiers Rl Qel Method Analysis Date 1 By E170.1 01/28/11 09:201 kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 6 of 11 EN:RGY www.energylab.com Helena, MT 877-472-0711 • Blilinga, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-188-7175 • Rapid City, SD 188-&72-1225 • College Station, TX 888-&80-2218 .\! I ,..-, f ~ ,I . I " " Au/yfIaI buIIat:t SbIu 1m Client: Denison Mines USA Corp Project: 1 st Quarter Nitrate Analyte Method: A4500-CI B Sample 10: MBLK9-110202 Chloride Sample 10: C11 01 0840·009AMS Chloride Sample 10: C11 01 0840-009AMSO Chloride Sample 10: LCS35-110202 Chloride Qualifiers: RL -Analyte reporting limit. QA/Qe Summary Report Prepared by Casper, WY Branch Revised Date: 02/10/11 Report Date: 02/09/11 Work Order: C11 01 0840 Result Units Method Blank NO mg/L Sample Matrix Spike 53.7 mg/L Sample Matrix Spike Duplicate 54.0 mg/L Laboratory Control Sample 3510 mg/L RL %REC Low Limit High Limit Run: TITRATION_110202A 0.5 Run: TITRATION_11 0202A 1.0 101 90 110 Run: TITRATION_110202A 1.0 102 90 110 Run: TITRATION_110202A 1.0 99 90 110 NO -Not detected at the reporting limit. RPO RPOLlmlt Qual Batch: 11 0202-CL· TTR-W 02/02/11 14:55 02/0211115:16 02/02/11 15:18 0.6 10 02/02111 15 :30 Page 7 of 11 Er\ERGY www.energylab.com Helena, lIT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WV 888-235-0515 Gillette, W'f 88B-888-7175 • Rapid City, so 188-&72-1225 • Collela Station, TX 888-610-221 B ~\I,~)r~\I '.lJI~ .~ AuIytk:M baIIHt:tI SIIIA '151 Client: Denison Mines USA Corp Project: 1 st Quarter Nitrate Analyte Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nitrate+Nitrite as N Sample 10: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample 10: C11010840-004BMS Nitrogen, Nitrate+Nitrite as N Sample 10: C11010840-004BMSO Nitrogen, Nitrate+Nitrite as N Sample 10: C11010840-014BMS Nitrogen, Nitrate+Nitrite as N Sample 10: C11010840-014BMSO Nitrogen, Nitrate+Nitrite as N Qualifiers: RL -Analyte reporting limit. QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 02/10/11 Report Date: 02/09/11 Work Order: C11 01 0840 Result Units RL %REC Low Limit High Limit RPO RPOLimlt Qual Batch: R142317 Method Blank Run: TECHNICON_ll0131A 01/31/1112:19 ND mg/L 0.06 Laboratory Control Sample Run: TECHNICON_ll0131A 01/31/11 12:22 2.42 mg/L 0.10 97 90 110 Sample Matrix Spike Run: TECHNICON_ll0131A 01/31/1113:54 2.51 mg/L 0.10 100 90 110 Sample Matrix Spike Duplicate Run: TECHNICON_l10131A 01/31/11 13:57 2.57 mg/L 0.10 103 90 110 2.4 10 Sample Matrix Spike Run: TECHNICON_ll0131A 01/31/11 14:47 2.71 mg/L 0.10 106 90 110 Sample Matrix Spike Duplicate Run: TECHNICON_ll0131A 01/31/1114:49 2.73 mg/L 0.10 107 90 110 0.7 10 ND -Not detected at the reporting limit. Page 8 of 11 EN:RGY • /~ • ( i .... , ... ,1'1' '. www.energyiab.com AMI!tIaI~S/Ja IUZ Helena, PiT 817--472-0711 • Billings, PiT 808-735-4488 • Cuper, WY 881-235-0515 Gillette, WY 18&-881-7175 • Rapid City, SD 818-172-1225 • College St8tlon, IX 881-&90-2218 Workorder Receipt Checklist Denison Mines USA Corp IIIIIII~IIIIII~ I~IIII~IIIIIIIII C11010840 Login completed by: Tabitha Edwards Reviewed by: BL2000\kschroeder Reviewed Date: 1/28/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper containerlbottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water-pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes It! Yes It! Yes 0 Yes It! Yes It[ Yes It! Yes It[ Yes It[ Yes It! Yes It! 3°C On Ice Yes 0 Yes It! Date Received: 1/28/2011 Received by: em Carrier name: Fed Ex No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present It! No VOA vials submitted It! Not Applicable 0 Page 9 of 11 Chain of Custody and Analytical Request Record L AGORA n JRIF<:; Comsme:, :uv-rS"",v rr;IN~> Report Mail Addresj: c:-t,. v . ~ (:> C~7 'AlA n ,/, ~ l7I:r g-l/ S' IL Invoice Address: 7 c5&»-<- PLEASE PRINT (Provide as much Information as possible.) Contact Name: Phone/Fax: Email: !4A-a~ l-;r zzz,( Involcb Contact & Phone: ~~~ Purchase Order: page-LofL EPNState Compliance: Yes ~ No 0 Sampler: (Please Print) 12~~4,~ Quofe/8ottle Order: Special Report/Formats: s ~ W@O@ oorn®[JJJ~[ID .. Contact Ell prior to sn~~ br RUSH sample submittal 1-::-~-11t~C'I~f!~\~..t"_----t a ~ "'O",~ ~aJ;gOllii ~ R for charges and Caoler 10(8): D ow D POTWflNWTP o State: ----o Other: ___ _ D EOO/EOT(Electronic Data) Format: ____ _ o LEVEL IV o NELAC ._> 0 >oro .19,,.(1) (11:::-C:VJUl ~:> -.,) 0s:'B (II g> ~ ~ « (l)1·Q :i2 _~ o ~ aJl '" ,"" ... ~~ § i§ "-s;: ~~I1il' '\ ~i~ll~ ~~.~ ~ ~ I ~ ... ..;:~-~\ SAMPLE IDENTIFICATION Collection Collection MATRIX ~ (Name, Location,lnterval. etc.) Date Time 4 TWA!, I J/2J/11 J3S/ g. ... w 1-1)( 91INw -h lJ2Jd II 1.2t;-;f 2-W X l)t 0 w I U « ..... ~ W W en Received by (prlnlr. t.. "0 c: ~ U (II c .. ::J l-S "0 .. t1l "0 c: t1l en H DateIT ....... : scheduling -See Instruction Page Comments: Rec""'JTemp ...:s 0c On lee: Custody Seal n OnBoltle r W" On Cooler t N Intact f'! N Signature ~ N M.tcll L ~ linn Signature: Custody Rel~'i~,(prit!/~ f/ir;;z:j /'fIlP .Y7~ ~~~r~e::R~:in:qu:.i~~(d:b:y(:pn:nn::.::===:~:!a:t~:r~~,e::===========~Oi~'na~u:~=: =========::R:6re:~:e:db:~:~n:'m:)::::=====:DB:t~:i:~::============:~:9M:t:ure::=========~~ S."gned l ... ecel~Y~~..q, 't'1~;;,me~1" "'. ~. "tgnaure: Sample Disposal: Return to Client: Lab Disposal: 1'--r~;'I(~'( /dD/P '7<~J In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information. downloadable fee schedule. forms, and links. Chain of Custody and Analytical Request Record Page LofL. I AI?()f?A TOfl/r~ Compa~e: -,,11 -Ut-jl/J5~".j If [ IIVrJ5 Invoice Address: / <-SA rM.-L.- Special Report/Formats: Dow o POTWMlWTP D State: o Other:---- O. EOD/EDT(Electronic Data) Format: ____ _ o LEVEL IV o NELAC SAMPLE IDENTIFICATION (Name. Location. Interval, etc.) Collection Date Collection Time }/2~/JI 1'1 Lf) I / 2~/1I JI'IS- PLEASE PRINT (Provide as much Information as possible.) Project Name, ~S, Permit, Etc. Sample Origin / <; l' V"UV/u-/t//rk~ State: fA. r EPA/State Compliance: Yes G-" No 0 Sampler: (Please Print) r24~ I2I~r Invoice Cohtact & Phone: Purchase Order: Quote/Bottle Order: 'i:MA' ./ .. 0 i=' R w ~ I " () C :l U c( 0 t-lU ~ c '-:l l-S W 'E W til CIJ " c g H (,/) l..-vJ Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page Comments: Cooler ID(sl: Receipt Temp 3. On Ice: (iN Custody Seal ~ ~=r 8Y~ Intact Y N Signature N Match ,JzilJf JlJfl.J2-1N 3 lI'.JAI _ J i2 yy.. IQJ Onn f • 7 8 9 10 1\ Signa "m: Custody Re~::/Y1JM/ 712.'1-;/( I¥v& s~ ~~~r~e~:~:in~qU~M~~~~D~Y:~:'n~t~~~:~~==o~~~em:~~~.~~=========~::~II=~=;===::=====:~~::il:~:~:~(p:rin:I):::::~~==~o:al:em:rne:~;====~~======~s:~:nM:~ro:;==========~ Sig ned I Sample Disposal: Return to Client: Lab Disposal: "ec.,\ "Y l"~ ~;kl. ua e' '~k ~/ 9. <r:l() <>ognawre; Recer.ed ~ (pnnt): atemrne: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All SUb-contract data will be clearly notated on your analytical report. VISit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. TabH Quality Assurance and Data Validation Tables H-1 Field Data QAlQC Evaluation Volume Location 2x Casing Volume Pumped Volume Check Conductivity RPD pH RPD Temp RPD Piezometer 1 -2327 -6.28 --13.59 -- Piezometer 2 --548 --7.61 --8.57 -- Piezometer 3 -2954 --12.36 -9.99 -- TWN-l 82.26 209.78 OK 796.0 795.0 0.13 7.02 7.03 0.14 14.38 14.39 0.07 TWN-2 104.56 54.57 Pumped Dry 3243.0 3253.0 0.31 6.08 6.11 0.49 12.92 13.04 0.92 TWN-3 84.76 40.29 PumJ.led Dry 1250.0 2685.0 72.94 5.86 6.25 6.44 11.88 13.91 15.74 TWN-4 114.74 294.10 OK 1022.0 1020.0 0.20 6.88 6.88 0.00 13.92 13.90 0.14 TWN-5 106.68 188.02 OK 3115.0 3115.0 0.00 6.47 6.52 0.77 14.14 14.15 0.07 TWN-6 70.86 272.00 OK 1579.0 1576.0 0.19 6.66 6.67 0.15 14.20 14.20 0.00 TWN-7 20.16 9.35 Pumped Dry 30.0 NA 7.25 NA 5.73 NA TWN-8 109.46 380.80 OK 2395.0 2378.0 0.71 6.83 6.81 0.29 14.32 14.35 0.21 TWN-9 43.32 20.06 Pumped Dry 2646.0 NA 6.55 NA 13.11 NA TWN-I0 29.40 20.91 Pumped Dry 3434.0 NA 3.10 NA 14.03 NA TWN-11 94.48 289.00 OK 2794.0 2798.0 0.14 6.29 6.30 0.16 14.25 14.24 0.07 TWN-12 98.70 89.76 Pumped Dry 2485.0 2463.0 0.89 6.72 6.80 1.18 14.19 14.15 0.28 TWN-13 95.84 255.00 OK 1240.0 1240.0 0.00 7.56 7.61 0.66 14.83 14.79 0.27 TWN-14 93.92 41.14 Pumped Dry 1032 NA 7.17 NA 14.36 NA TWN-15 81.74 37.40 Pumped Dry 1566 NA 6.71 NA 13.79 NA TWN-16 67.30 221.00 OK 1343.0 1331.0 0.90 6.59 6.60 0.15 14.77 14.75 0.14 TWN-17 98.86 54.57 Pumped Dry 1134.0 1154.0 1.75 6.90 6.92 0.29 13.70 14.13 3.09 TWN-18 113.44 340.00 OK 2296.0 2298.0 0.09 6.44 6.45 0.16 14.05 14.04 0.07 TWN-19 74.98 38.59 Pumped Dry 1872.0 1844.0 1.51 6.70 6.71 0.15 12.16 12.96 6.37 UWLP -228 NA 7.32 NA 2.02 NA Piezometers 1, 2, and 3 were not pumped, only one set of parameters were taken. TWN-2, TWN-3, TWN-7, TWN-9, TWN-lO, TWN-12, TWN-14, TWN-15,TWN-17 and TWN-19 were purged to dryness before 2 casing volumes were removed. TWN-l, TWN-5, TWN-8 and TWN-13 were purged to dryness after 2 casing volumes were removed. UWLP is a pond grab sample, no pumping was required and stabilization parameters are not applicable RPD > than 10% Redox Potential RPD Turbidity RPD 294 --0 -- 306 --0 -- 208 -6.1 -- 320 318 0.63 254.6 49.9 134.45 334 339 1.49 36.4 20.6 55.44 387 367 5.31 24.4 8.5 96.66 318 318 0.00 144.9 146.7 1.23 285 296 3.79 57.6 36.7 44.33 335 336 0.30 1110.0 1128.0 1.61 286 NA 10.2 NA 267 268 0.37 35.1 37.1 5.54 314 NA 10.1 NA 496 NA 390.3 NA 359 354 1.40 16.5 16.8 1.80 275 254 7.94 598.3 975.1 47.90 237 239 0.84 30.1 39.2 26.26 311 NA 11.8 NA 297 NA 58.2 NA 344 348 1.16 16.2 16.5 1.83 285 297 4.12 15.2 80.6 136.53 300 296 1.34 19.8 20.1 1.50 324 324 0.00 7.0 60.9 158.76 293 NA 0 NA e QAF states that turbidity should be less than 5 Nephelometric Turbidity Units ( NTV') prior to sampling unless the well is characterized by water that has a higher turbidity. The OAP does not require that turbidity mea urements be less than 5 NTU prior to sam ling. As such, thcnoted observations regarding turbidity measurements less than 5 NTU below are included for information ses only. H-2: Holding Time Evaluation Allowed' Holding Lab Analys;s Holding Time Location (I; ..... Sample Collection Date Dlifa Holding Time 1'lm:e Check Piezometer 1 Chloride 1131111 2/9/11 9.00 days 28 days OK Piezometer 1 Nitrogen 1131111 2/4/11 4.00 days 28 days OK Piezometer 2 Chloride 1/31111 2/9/11 9.00 days 28 days OK Piezometer 2 Nitrogen 1131111 2/4/11 4.00 days 28 days OK Piezometer 3 Chloride 1131111 2/9/11 9.00 days 28 days OK Piezometer 3 Nitrogen 1/31/11 2/4/11 4.00 days 28 days OK TWN-l Chloride 1126/11 2/2/11 7.00 days 28 days OK TWN-l Nitrogen 1126/11 1/31/11 5.00 days 28 days OK TWN-2 Chloride 2/1/11 2/9/11 8.00 days 28 days OK TWN-2 Nitrogen 2/1/11 2/4/11 3.00 days 28 days OK TWN-3 Chloride 2/1/11 2/9/11 8.00 days 28 days OK TWN-3 Nitrogen 2/1111 2/4111 3.00 days 28 days OK TWN-4 Chloride 1125/11 2/2/11 8.00 days 28 days OK TWN-4 Nitrogen 1/25/11 1/31111 6.00 days 28 days OK TWN-5 Chloride 1125111 2/2/11 8.00 days 28 days OK TWN-5 Nitrogen 1125/11 1131/11 6.00 days 28 days OK TWN-6 Chloride 1126/11 2/2/11 7.00 days 28 days OK TWN-6 Nitrogen 1126/11 1131/11 5.00 days 28 days OK TWN-7 Chloride 1127/11 2/2/11 6.00 days 28 days OK TWN-7 Nitrogen 1/27/11 1/31111 4.00 days 28 days OK TWN-8 Chloride 1125111 2/2111 8.00 days 28 days OK TWN-8 Nitrogen 1/25/11 1/31/11 6.00 days 28 days OK TWN-9 Chloride 2/1111 2/9/11 8.00 days 28 days OK TWN-9 Nitrogen 2/1/11 2/4/11 3.00 days 28 days OK TWN-I0 Chloride 1127/11 2/2111 6.00 days 28 days OK TWN-I0 Nitrogen 1/27/11 1131111 4.00 days 28 days OK TWN-l1 Chloride 1127/11 2/9111 13.00 days 28 days OK TWN-ll Nitrogen 1127/11 2/4/11 8.00 days 28 days OK TWN-12 Chloride 1/26111 2/2/11 7.00 days 28 days OK TWN-12 Nitrogen 1126111 1/31/11 5.00 days 28 days OK TWN-13 Chloride 1125/11 2/2/11 8.00 days 28 days OK TWN-13 Nitrogen 1125/11 1131111 6.00 days 28 days OK TWN-14 Chloride 1128/11 2/9/11 12.00 days 28 days OK TWN-14 Nitrogen 1128/11 2/4/11 7.00 days 28 days OK TWN-15 Chloride 1127/11 2/2/11 6.00 days 28 days OK TWN-15 Nitrogen 1127/11 1131/11 4.00 days 28 days OK TWN-16 Chloride 1127/11 2/9/11 13.00 days 28 days OK TWN-16 Nitrogen 1/27/11 2/4111 8.00 days 28 days OK TWN-17 Chloride 211111 2/9/11 8.00 days 28 days OK TWN-17 Nitrogen 2/1111 2/4111 3.00 days 28 days OK TWN-18 Chloride 1127/11 2/9111 13.00 days 28 days OK TWN-18 Nitrogen 1127/11 2/4/11 8.00 days 28 days OK TWN-19 Chloride 2/1111 2/9/11 8.00 days 28 days OK TWN-19 Nitrogen 2/1111 2/4/11 3.00 days 28 days OK TWN-65 Chloride 1125/11 2/2111 8.00 days 28 days OK TWN-65 Nitrogen 1125/11 1131111 6.00 days 28 days OK UWLP Chloride 1131111 2/9111 9.00 days 28 days OK UWLP Nitrogen 1131111 2/4/11 4.00 days 28 days OK PondD Chloride 1131/11 2/9/11 9.00 days 28 days OK PondD Nitrogen 1131/11 2/4/11 4.00 days 28 days OK H-3: Analytical Method Check Both Nitrate and Chloride were analyzed with the correct analytical method. H-4: Reporting Limit Evaluation Lab Rep~rting Rqd'Reporting Location Constituenf SampJi)!g Result Limit Limit QuaUfier Piezometer 1 Chloride 60 mg/L 1 mg/L 1 mg/L 1 mg/L Piezometer 1 Nitrogen 7 mg/L 1 mg/L 0.1 mg/L 0.1 mg/L D Piezometer 2 Chloride 9 mg/L 1 mg/L 1 mglL 1 mg/L Piezometer 2 Nitrogen 0.3 mg/L 0.1 mg/L 0.1 mg/L 0.1 mg/L Piezometer 3 Chloride 40 mg/L 1 mg/L 1 mg/L 1 mg/L Piezometer 3 Nitrogen 1.8 mg/L 0.2 mg/L 0.1 mglL 0.1 mg/L D TWN-l Chloride 17 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-l Nitrogen 0.5 mg/L 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-2 Chloride 93 mg/L 1 mg/L 1 mglL 1 mg/L TWN-2 Nitrogen 43 mg/L 2 mg/L 0.1 mg/L 0.1 mg/L D TWN-3 Chloride 138 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-3 Nitrogen 24 mg/L 1 mg/L 0.1 mglL 0.1 mg/L D TWN-4 Chloride 21 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-4 Nitrogen 0.9 mglL 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-5 Chloride 47 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-5 Nitrogen 0.4 mglL 0.1 mglL 0.1 mg/L 0.1 mg/L TWN-6 Chloride 18 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-6 Nitrogen 1.1 mg/L 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-7 Chloride 6 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-7 Nitrogen 1.3 mg/L 0.1 mg/L 0.1 mg/L 0.1 mglL TWN-8 Chloride 13 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-8 Nitrogen a mg/L 0.1 mg/L 0.1 mg/L 0.1 mg/L U TWN-9 Chloride 217 mg/L 1 mg/L 1 mglL 1 mg/L TWN-9 Nitrogen 9.5 mg/L 0.5 mglL 0.1 mg/L 0.1 mg/L D TWN-I0 Chloride 40 mg/L 1 mglL 1 mg/L 1 mglL TWN-lO Nitrogen 0.3 mg/L 0.1 mg/L 0.1 mglL 0.1 mg/L TWN-ll Chloride 84 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-l1 Nitrogen 1.4 mg/L 0.1 mg/L 0.1 mglL 0.1 mg/L TWN-12 Chloride 87 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-12 Nitrogen 4.2 mg/L 0.2 mg/L 0.1 mglL 0.1 mg/L D TWN-13 Chloride 103 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-13 Nitrogen 1.6 mglL 0.2 mg/L 0.1 mg/L 0.1 mg/L D TWN-14 Chloride 24 mg/L 1 mg/L 1 mglL 1 mg/L TWN-14 Nitrogen 3.7 mg/L 0.5 mg/L 0.1 mglL 0.1 mg/L D TWN-15 Chloride 43 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-15 Nitrogen 1.4 mg/L 0.1 mg/L 0.1 mglL 0.1 mg/L TWN-16 Chloride 34 mglL 1 mg/L 1 mglL 1 mg/L TWN-16 Nitrogen 4.6 mg/L 0.5 mg/L 0.1 mg/L 0.1 mg/L D TWN-17 Chloride 90 mg/L 1 mg/L 1 mg/L 1 mglL TWN-17 Nitrogen 8.6 mg/L 0.5 mg/L 0.1 mg/L 0.1 mg/L D TWN-18 Chloride 61 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-18 Nitrogen 1.4 mg/L 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-19 Chloride 114 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-19 Nitrogen 7 mg/L 0.5 mg/L 0.1 mg/L 0.1 mg/L D TWN-65 Chloride 45 mg/L 1 mg/L 1 mg/L 1 mg/L TWN-65 Nitrogen 0.4 mg/L 0.1 mg/L 0.1 mg/L 0.1 mg/L UWLP Chloride 1 mg/L 1 mg/L 1 mg/L 1 mg/L UWLP Nitrogen 0.1 mg/L 0.1 mglL 0.1 mg/L 0.1 mg/L PondD Chloride 3 mg/L 1 mg/L 1 mg/L 1 mg/L PondD Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mglL 0.1 mg/L U = Analyte was not detected at the RL D = RL was increased due to sample matrix or required dilution due to the sample concentration. In all cases the analytical results were greater than the reporting limit used. H-5 QAlQC valuation for Sample Duplicates C()nstituent UWLP PondD %RPD Chloride 1 3 100.00 Nitrogen 0.1 0.1 0.00 Constituent TWN-5 TWN-65 %RPD Chloride 47 4~ 4.35 Nitrogen 0.4 0.4 0.00 The QAP acceptance limits for RPDs between the duplicate and original field sampJe is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. These results are less than 5 times the required reporting limit and the RPDs greater than 20 percent are acceptable. H-6 QC Control Limits for Analysis and Blanks The percent recovery was within the limits for all lab control samples, matrix spikes. and matrix spike duplicates. The RPD was below acceptable limits for each sample matrix spike duplicate from Energy Labs. The Method Blanks had no reported detections of target analytes. H7R 't T -ecelpi empera turElt' e va ua ion Sample Batch Wells in Batch Temperature Cl1020080 Piezometer I ,Piezometer 2, Piezometer3, TWN-2, TWN-3, 2 "C TWN-9, TWN-ll, TWN-14,TWN-16, TWN-17, TWN-18, TWN-19, TWN-19R, TWN-60, UWLP,Pond D Sample Batch WeItJ, Dr Bateh Tempel'ature CI1010840 TWN-I, TWN-IR, TWN-3, TWN-4, TWN-5, TWN-6, TWN-7, 3"C TWN-7R, TWN-8, TWN-IO, TWN-llR, TWN-12, TWN-13, TWN-13R, TWN-15 H-8 Rinsate Evaluation Rinsate Sample Parameter Rinsate Result Sample R~Sltlt for Well TWN-lR Nitrogen 0.5 mglL TWN-1 0.5 mglL TWN-7R Nitrogen 0.6 mglL TWN-7 1.3 mglL TWN-11R Nitrogen 1.4 mglL TWN-ll 1.4 mglL TWN-13R Nitrogen ND mglL TWN-13 1.6 mglL TWN-19R Nitrogen 0.8 mg/L TWN-19 7 mg/L PreVlous well sampled IS the well that the pump was used to purge pnor to the nnsate sample. D = Reporting limit raised due to dilution/sample matrix. Rinsate Qualifier Reporting Limit 0.1 mglL 0.1 mglL D 0.2 mg/L D 0.1 mg/L D 0.1 mglL Tab I Kriged Current Quarter Isoconcentration Maps o MW-4 .4.6 0 6.6 PIEZ-1 ,.7 TWN-1 ~0.5 TW4-26 ~10 MW-34 '¢-0.3 SCALE IN FEET EXPLANATION perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L Mw-hs PROPERTY BOUNDARY 4'.3 CELL NO. 48 I MW-03 eNS MW-20 ".1 3000 -temporary perched nitrate monitoring well showing concentration in mg/L temporary perched monitoring well installed May, 2010 showing concentration in mg/L perched monitoring well installed August/September, 2010 II II II II II II II r CELL NO.1 MW-17 eNS ~1.4 TWN-1S ~1.4 TWN-11 ~3.7 TWN-14 MW-01 eNS ~.3 TWN-10 --- MW-1B eNS ~1 .4 ~1.3 TWN·1B ~1.1 TWN-6 ~D TWN-B " , / I I ~.5 , I TWN-9 I I I P~Ez-1 _ -I .. :1- MW-19 eNS TWN-7 ----, " , " , / \ I \ PIEZ-2 "0.3 I , MW- I I 33 ~.9 N-4 , , PIEZ-3 "1.B .... _07 M -26 " " 0 1.3 / .... , .5 '09' 03.5 / 06.5 \ , ',/ I I -L I I I " / , ,06.5 I S!T.S' , ~.§ft.w'-84 4:1f:s~ ND o PIEZ-S "NS 'f c07 00.7 TW4.-2.6 1l:f10 \ '6_ " T37S T38S MW-22 e2.S 01.8 II // // // // // // // // // // I I , I I I \ I I I I I I NOTES: NO = not detected, NS = not sam led HYDRO GEO CHEM, INC. APPROVED SJS KRIGED 1st QUARTER, 2011 NITRATE (mg/L) (NITRATE + NITRITE AS N) WHITE MESA SITE DATE REFERENCE FIGURE H :/718000/may11 Initrate/nit0211.srf ( \ PROPERTY BOUNDARY f' o MW-4 .40 0 41 PIEZ-1 Q 60 TWN-1 <>17 TW4-26 ~30 MW-34 -9-74 32 N SCALE IN FEET EXPLANATION perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L Mw·h5 11 CELL NO. 48 I MW~3 ~ry- MW-03 e NS MW·20 eG4 3000 temporary perched nitrate monitoring well showing concentration in mg/L temporary perched monitoring well installed May, 2010 showing concentration in mg/L perched monitoring well installed August/September, 2010 - II II II II II II II MW·17 eNS MW·01 eNS ~ 06 TWN·7 33 MW·18 018 eNS TWN·6 013 043 TWN·15 040 TWN·10 PIEZ·1 "60 MW·19 TWN-B eNS 061 TWN·18 44 o PIEZ·5 "NS PIEZ·2 "9 PIEZ·3 "40 034 041 062 023 031 041 040 TW4·26 ~30 025 T378 T388 MW·22 e57 084 TWN-11 024 TWN·14 II ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ NOTES: ND = not detected, NS = not sam led HYDRO GEO CHEM, INC. APPROVED SJS KRIGED 1 st QUARTER, 2011 CHLORIDE (mg/L) WHITE MESA SITE DATE REFERENCE FIGURE H :/718000/may11 /chloride/cI0211.srf ( \ TabJ Analyte Concentrations Over Time TWN-l li)atce 1:~6J2001 11'2.'1/1'00' '9121/2.009 10/28/2Q09 :1/1"1120:10 5/2"r):~OlQ 9/27/201.Q .l:2/7fj!()lfJ U2~l1011 Nitrate (mg/I)Chim'id.e C~wl,l) 0.7 ];,9 0.4 17 0.4 0.5 0.5 0.6 0.6 0.6 0.5 TWN-2 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 25.4 29 7/21/2009 25 25 9/21/2009 22.6 17 11/2/2009 20.8 55 3/24/2010 62.1 85 6/2/2010 69 97 9/29/2010 69 104 12/9/2010 48 93 2/1/2011 43 93 TWN -3 Date Nitrate (mgtl) Chloride (mgtl) 2/6/2009 23.6 96 7/21/2009 25 .3 96 9/21/2009 27 .1 99 11/2/2009 29 106 3/25/2010 25 .3 111 6/3/2010 26 118 7/15/2010 27 106 12/10/2010 24 117 2/1/2011 24 138 !rWN~j lJat~ i/6/2009 7f2'f.j2fJ&9 9/21/2009 'fQ1l8/2009 ~/~6taoaO ili'I2.0~Q 9:/l'JtICfJJJ 12/8/2010 lj2staa1li11 iNittate :('W1)gtl) eb~lf>fute;(im:I1IJ 1 .3J'~ O.e5: 12 tM is 0.4 1l. 0:8 U' l.Q !~ Q.S19 1 ~1 :&.9 )1 TWN-5 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 0.22 42 9/21/2009 0.5 45 11/10/2009 0.2 48 3/16/2010 0.3 43 5/26/2010 0.3 44 7/12/2010 0.3 43 12/7/2010 0.3 45 1/25/2011 0.4 47 TWN-6 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 3.2 32 9/22/2009 1.6 13 11/3/2009 1.4 21 3/23/2010 1.5 19 6/1/2010 1.4 22 7/13/2010 1.4 73 12/8/2010 1.2 21 1/26/2011 1.1 18 TWN-7 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 ND 11 9/21/2009 ND 7 11/10/2009 0.1 7 3/17/2010 0.8 6 5/28/2010 1.2 6 7/14/2010 1.6 7 12/10/2010 1 4 1/27/2011 1.3 6 TWN-8 Date Nitrate (mg/I) Chloride (mg/I) Notes 8/25/2009 0 11 Nitrate is ND 9/21/2009 0 12 Nitrate is ND 11/10/2009 0 12 Nitrate is ND 3/16/2010 0 11 Nitrate is ND 5/26/2010 0 11 Nitrate is ND 7/12/2010 0 11 Nitrate is ND 12/6/2010 0 9 Nitrate is ND 1/25/2011 0 13 Nitrate is ND TWN-9 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 9.3 169 9/22/2009 8.9 201 11/10/2009 12 205 3/23/2010 7.6 183 6/1/2010 7.6 175 7/15/2010 10.7 210 12/9/2010 8 172 2/1/2011 9.5 217 TWN-l0 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 1.1 19 9/22/2009 1.6 35 11/10/2009 1.4 26 3/23/2010 1.5 54 6/4/2010 1 30 7/14/2010 0.2 21 12/8/2010 1.3 28 1/27/2011 0.3 40 TWN-11 Date Nitrate (mg/I) Chloride (mg/I) 11/3/2009 1.3 74 3/17/2010 1.4 73 6/4/2010 1.3 72 9/27/2010 1.4 76 12/8/2010 1.4 72 1/27/2011 1.4 84 TWN-12 Date Nitrate (mg/I) Chloride (mg/I) 11/3/2009 0.5 109 3/17/2010 0.7 113 5/26/2010 0.8 106 7/12/2010 0.7 112 12/7/2010 0.7 103 1/26/2011 4.2 87 TWN-13 Date Nitrate (mg/I) Chloride (mg/I) Notes 11/4/2009 0.5 83 3/17/2010 0 47 Nitrate ND 5/26/2010 0.1 49 9/27/2010 0.2 53 12/7/2010 0.4 57 1/25/2011 1.6 103 TWN-14 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 3.4 32 3/24/2010 2.9 24 6/2/2010 2.9 30 7/15/2010 3.5 26 12/10/2010 4.2 28 1/28/2011 3.7 24 TWN-15 Date Nitrate (mg/I) 11/10/2009 1.1 3/18/2010 0.7 5/28/2010 1.0 7/13/2010 1.0 12/9/2010 1.2 1/27/2011 1.4 Chloride (mg/I) 78 43 39 36 38 43 TWN-16 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 1 39 3/17/2010 1.2 35 5/27/2010 0.2 35 9/27/2010 2.6 35 12/9/2010 2 30 1/27/2011 4.6 34 TWN-17 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 6.7 152 3/24/2010 lOA 78 6/3/2010 11 87 7/15/2010 8.9 66 12/10/2010 8 65 2/1/2011 8.6 90 TWN-18 Date Nitrate (mg/I) Chloride (mg/I) 11/2/2009 1.3 57 3/17/2010 1.6 42 6/1/2010 1.8 63 9/27/2010 1.8 64 12/9/2010 1.6 59 1/27/2011 1.4 61 TWN-19 Date Nitrate (mg/I) Chloride (mg/I) 11/2/2009 7.4 125 3/23/2010 7.2 118 6/1/2010 6.2 113 9/29/2010 7.2 113 12/9/2010 7 107 2/1/2011 7 114 Piezometer 1 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 6.8 NA 7/14/2009 6.8 60 9/22/2009 7.3 78 10/27/2009 7.4 61 6/2/2010 7.2 52 7/19/2010 6.8 52 12/10/2010 6.5 60 1/31/2011 7 60 Piezometer 2 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 0.5 NA 7/14/2009 0.5 7 9/22/2009 0.5 17 10/27/2009 0.6 7 6/2/2010 0.6 8 7/19/2010 0.6 8 12/10/2010 0.2 6 1/31/2011 0.3 9 Piezometer 3 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 0.7 NA 7/14/2009 0.8 12 9/22/2009 0.8 24 10/27/2009 1.2 19 3/24/2010 1.7 116 6/2/2010 1.6 36 7/19/2010 1.6 35 12/10/2010 1.8 25 1/31/2011 1.8 40 Piezometer 4 Date 7/14/2009 Nitrate (mg/I) Chloride (mg/I) 1.8 46 Piezometer 5 Date 7/14/2009 Nitrate (mg/I) 0.7 Chloride (mg/I) 18 MW-18 Date Nitrate (mg/I) Chloride (mg/I) 7/14/2009 ND 51 MW-19 Date Nitrate (mg/I) 7/14/2009 2.2 Chloride (mg/I) 24 Upper Wildlife Pond Date Nitrate (mg/I) Chloride (mgfl) Note 9/22/2009 0 5 Nitrate ND 10/27/2009 0 3 Nitrate ND 6/2/2010 0 0 Nitrate and Chloride ND 7/19/2010 0 0 Nitrate and Chloride ND 12/10/2010 0 1 Nitrate ND 1/31/2011 0.1 1 Frog Pond Date 10/14/09 Nitrate (mg/I) o Chloride (mg/I) o Notes Nitrate ND TabK Concentration Trend Graphs en c o ,'--l! -c B c o o ~ Z ~ • z ~ QO d .V· ~~ '1\ .~ V V' .V "'t: o (116w) ~ ~-unr O~-i\ON 0~-6n\t O~-AeV'J o~-uer -60-loa -60-JeV'J 90-03a O~-I\ON > 0 ~-5n'V . 60-lnr . 60-JeLt'J ~--------~---------4----------+---------~--------~-80-oaO IJ') N o N IJ') ...... o IJ') .0 ...... fI) c o ~ .. c G) u c o (J S I! .. .-z ~ z ~ o QO / / \ '" o (0 I '" '" • ~~ o N - - - o ~ ~-unr O ~-"ON 0~-6n\f o ~-uer 60-100 60-JeVII Bo-oaa U) c 0 ;; I! .... c CD u C 0 0 CD ~ ·c ~ .c 0 N I Z ~ o N ..- o o ..- o CX) o CO o v o N ~ ~-unr -0 ~-I\ON o~-5n'l -o~-lieV'oJ o~-uer 60-PO 60-JeV'oJ 90-0aa o en c o ~ .... c CD u c 8 .e ~ z CW) • z ~ o ("') 0 0 / / ~ ~ o N o ..- . o ~ ~-unr o~-6n\f O~-AeVII o~-uer 60-PO 60-JBVII ~ o ~ -C "(1) U C o (J ~ "C o .;C (J ~ z ~ o (0 '" a N ..- \ o o ..- • a co a (0 o "<:t a N - - - - - - a ~ ~-unr O~-flON o~-6n'V o ~-}i8VII O~-U8r 60-l~O 60-lnr 60-J8VII Bo-~ao ~ ~-unr O~-fION o ~-6n'v' fI) C 0 ;; ~ -0 ~-AeL"J .. c CD to) C 0 0 CD .. -o~-uer ~ ~ Z ,. Z ~ 60-l00 60-JeL"J N o o en c 0 i ... -c B c 0 (.) G) "C ·c 0 :E (.) .,. z ~ ~ ~-unr -O~-floN o ~ -6nv -0 ~-AeV'J -0 ~-uer 60-lO0 -60-lnr 60-JeV'J ~--------~--------~----------+---------~---------+ Bo-~aa 1.0 N o N U) ..... o o ..... O~-AON o ~-6n'v' en C 0 :,c; ca .... -C G) U C O~-AeV'J 0 0 .! ~ z II) I Z ~ o~-uer -60-l~O f-----+------+--------4----+-----+------+ 60-lnr N o o O~-I\ON o ~-5n\l (I) r:::: ,2 1U ~ Q) u c o ~-AeVIJ 0 0 Q) "tJ 'C .2 oJ: (J an I Z ~ o ~-uer 60-l0a 1-----I----+----I-----1----+----l-----\----l--60-lnr In C o ~ -c C\) CJ C o (.) S l! ~ z CO • Z ~ ..- ~ ~ L--I ~ LO N N ~ ~ ~. LO o - o O~-I\ON o~-6n'V o ~-AeVII o~-uer 60-PO en r:: 0 ~ ... -C CI) u r:: 0 U CI) 'U "C .2 .c (,) '9 z ~ O~-AON o~-6n\l O~-AeV'J o ~-uer 60-l00 f----+----+----+-----l----f----+----+----+ 60-lnr o CX) o ID o 1.0 o "<t (1/6W) o N o ..-o ~ ~-uer O~-"ON o~-das fI) o ~-5n'v' c 0 .. e -c CI) u c o~-unr 0 0 s e ~ z -O~-Ae~ ,.... I Z ~ O~-Je~ o~-uer 60-lO0 CC! .~ ~ C'! ...... co ~ ~ N a ...... ...... ...... ...... 0 a a 0 (1/6W) O~-i\ON o~-6nv en c: 0 ;i 1! -c CD U c O~-AeVII 0 (.) CD "C -C 0 .c (.) ~ Z ~ o~-uer L..----+-----+-------4----+-----+-----l-60-lnr a co o ...... ...... 1 0.9 0.8 0.7 0.6 -...J C, .s 0.5 0.4 0.3 0.2 0.1 o 0) o , :5 -:I ... T ~ T 0) o , t5 o "" TWN-8 Nitrate Concentrations TWN-8 Nitrate Concentrations are all Non Detect o ..-, c ro -:I "" o ..-~ :2 "" .... o ..-, Ol :::J « T o ..-> o Z I I ..-..-, .D Q) lL O~-i\ON o ~-6n'v' fI) 6 .. I! -r:::: 0 CI) u r:::: o~-liew 0 (.,) CI) "C "C .2 ~ .,c (.,) cp z ~ o~-uer 60-t00 1-----1------+----4----1-----+----4----+ 60-lnr o o ..- ~ ~-unr O~-AON I/) c 0 ~ o~-6n\f .b c CD CJ C 0 0 CD -f! o ~-Aev-J :t:= Z ~ Z ~ -o~-uer f-----+----+--------+---+-----+---+----+ 60-]nr co o en c 0 .. ~ -c CD CJ C 0 0 CD 'C 'C ~ .c 0 ~ Z ~ ~ ~-unr -0 ~-J\ON o ~-6n'v' o ~-Aer.J o~-uer 60-100 1------1-----+-----+------+-----1-60-lnr o lO N o o N o o .- o lO o O~-I\ON o ~-6n'it In C 0 :t:i f! -c CD U C o ~-AeV'J 0 (.) CD 11 ... ~ Z 0 "r"" • Z ~ -o~-uer 60-PO 60-lnr ~ CO "<:I: "! ....... CO cq "<:I: N 0 ....... ....... ....... ....... 0 0 0 0 (116w) en c 0 ~ -c CI) u c 0 (J CI) "C 'i: ~ .c (J c 'r" I Z ~ o (0 o It) o C") C1,6w) o N o ..-o ~ ~-qa.:l O~-AON o~-6n\f o ~-AeV\l o~-uer 60-toO ~ ~-uer O~-J\ON o ~-das 0~-5nv en c 0 .. ca ... o ~-unr -c 3 c 0 <J .s l! o ~-AeV'J :!:! Z ... ... I o ~-JeV'J Z ~ o~-uer 60<)ao 60-100 60-5nV N "': ex> <D ~ N ~ ex> "': ..-~ ~ ~ ('t) ..-"! ..-...-..-.... (116w) en c: 0 .. 1! -c: B c: 0 0 cu "tI 'C .2 .c: 0 --I Z ~ co co v co co ..... N ..... ~ ~-U8r -O~-AON O~-das 0~-5n'lj o~-unr 0~-A8V11 O~-JeV\l -0 ~-uer -60-090 60-PO 60-5n'lj en c o ~ ... -c 8 c 8 j Z N "II"" I Z ~ ....... ------------. ----. ----------.. ~ ~ LO a - a ~ ~-uer O~-AON o~-das o~-6nV' o~-unr o ~-;;eV'J o~-uer 60-PO 60-6nv ~ o ~ .... c ~ c o o CD " ·c .2 .t: o N -• Z ~ o N J ~ ~ ~ ~ / ( o o o 00 o v - - - o ~ ~-uer O~-I\ON o~-das o ~-6nV o ~-unr o ~-lieV\l o ~-uer 60-oaa 60-6nV -~~-uer O~-AON o~-das o~-6nv I/) C 0 ;; l! -o~-unr C CD U C 0 0 S O ~-AeVII l! -2 M 'I"" I Z o ~-JeVII ~ -o~-uer 60<)90 60-lO0 60-6nv ~ ~ -.:t: C'! ..-co co -.:t: N 0 ..-..-..-..-0 a 0 a (1/6w) en c o ~ -c CI) u c o (.) 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C) ~ u.. 60-AON ~~ 60-lO0 60-deS -60-das f-60-6nV o en c o .. ~ c CD CJ C o U CD " 'C ..2 .c u " c o 0. C) ~ LL 0> ci co ci ~~ q o 60-J\ON 60-lO0 60-deS 60-des 60-6nv 60-lnr TabL CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel FridaYi May 13, 2011 10:08 AM rlundberg@utah.gov Jo Ann Tischler; David Frydenlund Transmittal of CSV Files White Mesa Mill 2011 Q1 Nitrate Monitoring C11010840_R1.csv; C11020080(1 ).CSV Attached to this e-mail i's an electronic copy of laboratory results for nitrate monitoring conducted at the White Mesa Mill during the first quarter of 2011, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel Denison Mines (USA) Corp. Quality Assurance Manager 1