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HomeMy WebLinkAboutDRC-2012-001470 - 0901a068802dd059n « DENISON 7 Denison Mines (USA) Corp, 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel 303 628-7798 Fax : 303 389-4125 www.denisonmlnes.com Sent VIA Federal Express May 31, 2012 Mr. Rusty Lundberg Director, Division of Radiation Control Utah Department ofEnvironmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Re: Transmittal of 1st Quarter 2012 Nitrate Monitoring Report UDEQ Docket No. UGVV-09-03 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies ofthe Wliite Mesa Uranium Mill Nitrate Monitonng Report for the 1st Quarter of 2012 as required by the January 2009 Stipulated Consent Agreement. UDEQ Docket No. UGW-09-03, as well as two CDs each containing a word searchable electronic copy of the report. Ifyou should have any questions regarding this report please contact me. Yours very truly, DEMSON MINES (USA) CORP. Jo Ami Tischler Director, Comphance and Permitting CC: Ron F Hochstein David C FPf'denlund Harold R Roberts David E Turk Kathy Weinel Central Files OENISOJ)~~ MINES Sent VIA Federal Express May 31,2012 Mr. Rusty Lundberg Director, Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Re: Transmittal of 1st Quarter 2012 Nitrate Monitoring Report UDEQ Docket No. UGW-09-03 White Mesa Uranium Mill Dear Mr. Lundberg: Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303 628-7798 Fax: 303 389-4125 www.denisonmines.com Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 1st Quarter of2012 as required by the January 2009 Stipulated Consent Agreement, UDEQ Docket No. UGW-09-03, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, al0AAAA. ~ 7n~;;~~-~INES (USA) CORP. JoAnn Tischler Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel Central Files White Mesa Uranium Mill Nitrate Monitoring Report State of Utah Stipulated Consent Agreement, January 2009 Docket No. UGW09-03 1st Quarter (January through March) 2012 Prepared by: Denison Mines (USA) Corp. 1050 1 i h Street, Suite 950 Denver CO 80265 May 31, 2012 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................. 4 2.0 GROUNDWATER NITRATE MONITORING ................................................ 4 2.1 Samples and Measurements Taken During the Quarter ..................................... 4 2.1.1 Nitrate Monitoring ...................................................................................... 4 2.1.2 Parameters Analyzed .................................................................................. 5 2.1.3 Groundwater Head and Level Monitoring .................................................. 5 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 5 2.2.1 Well Purging and Depth to Groundwater ................................................... 6 2.2.2 Sample Collection ....................................................................................... 6 2.3 Field Data ............................................................................................................ 8 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 8 2.5 Laboratory Results .............................................................................................. 8 2.5.1 Copy of Laboratory Results ........................................................................ 8 2.5.2 Regulatory Framework ............................................................................... 9 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 9 3.1 Field QC Samples ............................................................................................... 9 3.2 Adherence to Mill Sampling SOPs ................................................................... 10 3.3 Analyte Completeness Review ......................................................................... 10 3.4 Data Validation ................................................................................................. 10 3.4.1 Field Data QA/QC Evaluation .................................................................. 10 3.4.2 Holding Time Evaluation .......................................................................... 11 3.4.3 Receipt Temperature Evaluation ............................................................... 11 3.4.4 Analytical Method Checklist .................................................................... 12 3.4.5 Reporting Limit Evaluation ...................................................................... 12 3.4.6 QAlQC Evaluation for Sample Duplicates ............................................... 12 3.4.7 Rinsate Check ........................................................................................... 12 3.4.8 Other Laboratory QAlQC ......................................................................... 13 4.0 INTERPRETATION OF DATA ....................................................................... 14 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 14 4.1.1 Current Site Groundwater Contour Map ................................................... 14 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter ........................................................... 15 4.1.3 Hydrographs .............................................................................................. 15 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 15 4.2 Review of Analytical Results ............................................................................ 16 4.2.1 Current Nitrate and Chloride Isoconcentration Maps ............................... 16 4.2.2 Nitrate and Chloride Concentration Trend Data and Graphs .................... 16 4.2.3 Interpretation of Analytical Data ............................................................ ,. 16 5.0 CORRECTIVE ACTION REPORT ................................................................. 17 5.1 Identification and Definition of the Problem ......................................................... 17 5.2 Assignment of Responsibility for Investigation of the Problem ....................... 17 5.3 Investigation and Determination of Cause of the Problem ............................... 17 5.4 Determination of a Corrective Action to Eliminate the Problem ..................... 17 5.5 Assigning and Accepting Responsibility for Implementing the Corrective Action ............................................................................................................... 17 1 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 Ql\2012 Ql Nitrate Report text.docx 5.6 5.7 5.8 6.0 7.0 8.0 Implementing the Corrective Action and Evaluating Effectiveness ................. 17 Verifying That the Corrective Action Has Eliminated the Problem ................. 17 Assessment of Previous Quarter's Corrective Actions ..................................... 18 CONCLUSIONS AND RECOMMENDATIONS ............................................ 18 ELECTRONIC DATA FILES AND FORMAT .............................................. 19 SIGNATURE AND CERTIFICATION ........................................................... 20 2 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 Ql\2012 QI Nitrate Report text.docx LIST OF TABLES Table 1 Summary of Well Sampling and Constituents for the Period Table 2 Nitrate Percent Difference Table 3 Chloride Percent Difference INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-l Field Data QAlQC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QAlQC Evaluation for Sample Duplicates H-6 QC Control limits for Analysis and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Nitrate and Chloride Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Nitrate and Chloride Concentration Trend Graphs Tab L CSV Transmittal Letter 3 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx 1.0 INTRODUCTION The Utah Department of Environmental Quality ("UDEQ") Division of Radiation Control ("DRC") noted in a Request dated September 30, 2008 (the "Request"), for a Voluntary Plan and Schedule to Investigate and Remediate Nitrate Contamination at the White Mesa Uranium Mill (the "Mill") (the "Plan"), that nitrate levels have exceeded the State water quality standard of 10 mg/L in certain monitoring wells. As a result of the Request, Denison Mines (USA) Corp. ("DUSA") entered into a Stipulated Consent Agreement (the "Consent Agreement") with the Utah Water Quality Board in January 2009 which directed the preparation of a Nitrate Contamination Investigation Report ("CIR") and Quarterly Nitrate Monitoring Reports. A subsequent letter dated December 1, 2009, among other things, recommended that DUSA also address elevated chloride concentration in the Nitrate Monitoring Reports. The Consent Agreement ("CA") was amended in August 2011. Under the amended Consent Agreement, DUSA submitted a Corrective Action Plan ("CAP"), pursuant to the requirements of the Utah Groundwater Quality Protection Rules [UAC R317-6-6.15(C -E)] on November 29, 2011 and revised versions of the CAP on February 27,2012 and May 7, 2012. This is the Quarterly Nitrate Monitoring Report, as required under the Consent Agreement, State ofUDEQ Docket No. UGW-09-03 for the first quarter of2012. 2.0 GROUNDWATER NITRATE MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Nitrate samples and measurements taken during this reporting period (January through March 2012), are discussed in the remainder of this section. 2.1.1 Nitrate Monitoring Quarterly sampling for nitrate monitoring parameters was performed in the following wells: TWN-l TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-I0 TWN-ll TWN-12 TWN-13 TWN-14 TWN -15 Piezometer 2 TWN -16 Piezometer 3 TWN-17 TWN-18 TWN-19 Upper Wildlife Pond ("UWLP") Piezometer 1 Table 1 provides an overview of all locations sampled during the current period, along with the date samples were collected from each location, and the date( s) upon which 4 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx analytical data were received from the contract laboratory. Table 1 also identifies rinsate samples collected, as well as sample numbers associated with any required duplicates. As indicated in Table 1, nitrate monitoring was performed in all of the nitrate monitoring wells, the UWLP, and Piezometers 1, 2, and 3. Analytical data for all of the nitrate wells, piezometers and the UWLP are included in Tab G. Nitrate and chloride are also monitored in all of the Mill's groundwater monitoring wells and chloroform investigation wells. Data from those wells for this quarter are incorporated in certain maps and figures in this report but are discussed in their respective programmatic reports. 2.1.2 Parameters Analyzed Locations sampled during this reporting period were analyzed for the following constituents: • Inorganic Chloride • Nitrate plus Nitrite as Nitrogen (referred to herein as nitrate) Use of analytical methods consistent with the requirements of the White Mesa Uranium Mill Groundwater Quality Assurance Plan, Revision 6, March 22, 2010 (the "QAP") was confirmed for all analytes, as discussed later in this report. 2.1.3 Groundwater Head and Level Monitoring Depth to groundwater was measured in the following wells andlor piezometers, pursuant to Part I.E.3 of the Groundwater Discharge Permit (the "GWDP") (dated July 14,2011): • The quarterly groundwater compliance monitoring wells. • Existing well MW -4 and all of the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3, P-4 and P-S. • MW-20, MW-22, and MW-34. • The DR piezometers which were installed during the Southwest Hydrogeologic Investigation. • Nitrate monitoring wells. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within S calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. 2.2 Sampling Methodology and Equipment and Decontamination Procedures S N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx The QAP provides a detailed presentation of procedures utilized for groundwater sampling activities under the GWDP (July 14,2011). The sampling methodology, equipment and decontamination procedures that were performed for the nitrate contaminant investigation, as summarized below, are consistent with the QAP. 2.2.1 Well Purging and Depth to Groundwater A list of the wells in order of increasing nitrate contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all of the non-detect wells and then move to the more contaminated wells in order of nitrate contamination, starting with the wells having the lowest nitrate contamination. Before leaving the Mill office, the pump and hose are decontaminated using the cleaning agents described in Section 6.2.5 of the QAP. A rinsate blank is collected after the first pump decontamination of each day as described below. Mill personnel then proceed to the first well which is the well with the lowest concentration of nitrate based on the previous quarter's sampling results. Well depth measurements are taken and the two casing volumes are calculated (measurements are made using the same instrument used for the monitoring wells under the Mill's GWDP). The Grundfos pump (a 6 to 10 gallon per minute [gpm] pump) is then lowered to the bottom of the well and purging is begun. At the first well, the purge rate is measured for the purging event by using a calibrated 5 gallon bucket. After the evacuation of the well has been completed, the well is sampled when possible, and the pump is removed from the well and the process is repeated at each well location moving from the least contaminated to most contaminated well. If sample collection is not possible due to the well being purged dry a sample is collected after recovery as described below. All wells are capped and secured prior to leaving the sampling location. Decontamination of non-dedicated equipment, using the reagents in Section 6.2.5 of the QAP, is performed between each sample location, and at the beginning of each sampling day, in addition to the pre-event decontamination described above. . 2.2.2 Sample Collection Wells Following the purging of a nitrate investigation well, the sampling takes place once stabilization has been achieved in accordance with Section 6.2.7 of the QAP. Prior to leaving the Mill office for sampling, Mill Personnel prepare a cooler with ice. A trip blank is not required as the sampling event does not include analyses for Volatile Organic Compounds ("VOCs"). Once Mill Personnel arrive at the well sites, labels are filled out for the various samples to be collected. All personnel involved with the collection of water and samples are then outfitted with rubber gloves to avoid sample contamination. 6 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx Each sample collection event begins at the location least affected by nitrate (based on the previous quarter's sampling event) and proceeds by affected concentration to the most affected location. The dedicated portable pump is appropriately decontaminated prior to each sampling event, each sampling day, and between well samples. It is important to note that the rinsate blank sample frequency was modified during the fourth quarter 2010 as recommended by UDEQ personnel present on site for split sampling during the chloroform sampling program. Previously, a rinsate blank sample was collected after each decontamination of the nondedicated pump and prior to the next use of the pump. Per an e-mail from Mr. Phil Goble, dated, November 15, 2010, the decreased rinsate blank frequency implemented during the chloroform sampling program was acceptable for implementation on the nitrate sampling program. Based on the revised procedure, rinsate blank samples are only required at the beginning of the sampling event and at the beginning of each day of sampling. The frequency change was implemented during fourth quarter 2010. The rinsate blank sample frequency will be modified again during the third quarter 2012 sampling event pursuant to UDEQ approval of the Groundwater QAP, Revision 7.1 on May 30, 2012. The frequency for rinsate blank samples will be one rinsate blank sample for every 20 field samples. Samples are taken from the portable pump after stabilization has been achieved, unless the well is pumped dry. If the well is pumped dry, Mill personnel use a disposable bailer to sample the well after it has recovered in accordance with Section 6.2.7 of the QAP. The bailer is attached to a reel of approximately 150 feet of nylon rope and then lowered into the well. After coming into contact with the water, the bailer is allowed to sink into the water in order to fill. Once full, the bailer is reeled up out of the well. Sample bottles are filled as follows: • First, a 250 ml sample is collected for nitrate/nitrite. This sample is not filtered, but is preserved with H2S04• • Second, a 500 ml sample is collected for chloride. This sample is not filtered and is not chemically preserved. After the samples have been collected for a particular well, the samples are placed into the cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. If a bailer has been used it is disposed of. Ponds Grab samples are taken from the UWLP using a disposable bailer. Sample bottles are filled in the same manner as for wells, as stated above. After the samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, Energy Laboratories ("EL"). 7 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx Piezometers Samples are collected from Piezometers 1, 2 and 3, if possible. Samples are collected from piezometers using a disposable bailer following the procedures described for wells that have been pumped dry, above. However, due to the difficulty in obtaining samples from the piezometers, the purging protocols set out in the QAP are not followed. After samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, EL. 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the nitrate contaminant investigation monitoring wells, piezometers, and UWLP identified in Section 2.1.1 above, and Table 1. It is important to note that the field data sheet appearance was changed in the fourth quarter 2010 as a result of the implementation of an electronic data capture system. The field data sheets contain the same information as the approved field data sheet attached to the approved QAP in approximately the same location. The new data sheets allow the electronic capture of data while still maintaining the real-time recording of information manually in ink as required by UDEQ. The changes were made to accommodate the data recording and validation system. Revised field forms will be used during the third quarter 2012 sampling event. The revised field forms are based on the changes approved in the Groundwater QAP, Revision 7.1. Approval of the QAP, Revision 7.1 was received May 30, 2012. 2.4 Depth to Groundwater Data and Water Table Contour Map Depth-to-groundwater measurements which were utilized for groundwater contours are included on the Quarterly Depth to Water Sheet at Tab C of this Report along with the kriged groundwater contour map for the current quarter generated from this data. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each as indicated by the measurement dates in the summary sheet under Tab C. A copy of the kriged groundwater contour map generated from the previous quarter's data is provided under Tab D. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results All analytical results were provided by EL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well or other sample. Results from analysis of samples collected for this quarter's nitrate investigation are provided under Tab G of this Report. Also included under Tab G are the results of analyses for duplicate samples and rinsate samples for this sampling effort, as identified in Table 1. See the Groundwater Monitoring Report and Chloroform Monitoring Report 8 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx for this quarter for nitrate and chloroform analytical results for the groundwater monitoring wells and chloroform investigation wells not listed in Table 1. 2.5.2 Regulatory Framework As discussed in Section 1.0 above, the Request, Plan, and Consent Agreement each triggered a series of actions on DUSA's part. Potential surficial sources of nitrate and chloride have been described in the December 30, 2009 CIR and additional investigations into potential sources were completed. Pursuant to the Consent Agreement, the most recent version of the CAP was submitted to the Co-Executive Secretary on May 7, 2012. The CAP will describe future activities associated with the nitrate in groundwater. This quarterly report documents the continued monitoring consistent with the program described in the initial Nitrate Contamination Investigation Report submitted in 2009. The monitoring program and reporting requirements set forth in the 2009 Contamination Investigation report will remain in effect until further notice and completion of the CAP. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager performed a QAIQC review to confirm compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check field data QAlQC, holding times, receipt temperature and laboratory data QAlQC are discussed in Sections 3.4.1 through 3.4.7 below. The analytical laboratory has provided summary reports of the analytical QAlQC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The Analytical Laboratory QAIQC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab G. Results of review of the laboratory QAIQC information are provided under Tab H and discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the nitrate investigation program consist of one field duplicate sample for each 20 samples, one DI Field Blank ("DIFB") and equipment rinsate samples. 9 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx During the quarter, two duplicate samples were collected as indicated in Table 1. The duplicates were sent blind to the analytical laboratory and analyzed for the same parameters as the nitrate wells. Rinsate samples were also collected at the beginning of the sampling period and at the beginning of each day of sampling from the decontaminated pump used for purging and sampling. Rinsate samples were labeled with the name of the subsequently sampled well with a terminal letter "R" added (e.g. TWN-7R). During the quarter three rinsate samples were collected and were sent to the analytical laboratory and analyzed for the same parameters as the nitrate wells. The results of these analyses are included with the routine analyses under Tab G. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QAlQC requirements established in the QAP were being adhered to and that the SOPs were implemented, except as noted below. 3.3 Analyte Completeness Review All analyses required by the GWDP for nitrate monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP (July 14, 2011) identify the data validation steps and data QC checks required for the nitrate monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QAlQC evaluation, a holding time evaluation, an analytical method check, a reporting limit evaluation, a QC . evaluation of sample duplicates, a QC evaluation of control limits for analysis and blanks, a receipt temperature evaluation, and a rinsate evaluation. Because no VOCs are analyzed for the nitrate contamination investigation, no trip blanks are required in the sampling program. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab H; 3.4.1 Field Data QAJQC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period of each other. The results of this quarter's review are provided under Tab H. 10 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 Ql\2012 Ql Nitrate Report text.docx Based upon this review, all well locations conformed to the QAP requirement to evacuate two well casing volumes before sampling except TWN-2, TWN-3, TWN-7, TWN-9, TWN-14, TWN-15, and TWN-17. These seven wells were all pumped to dryness before two casing volumes were evacuated and more than one set of field parameters could be collected. In each case, representative samples of formation water were collected after the wells were allowed to recover. Piezometers 1, 2, and 3 were not pumped, and were sampled directly after measurement of one set of parameters. Two casing volumes were pumped from TWN-I0 before it was purged to dryness; however, only one set of field parameters were collected prior to TWN -10 being pumped dry. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly sampling programs to the nearest 0.01 foot. All field parameters for all wells were within the QAP required limits, as indicated below. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Section 6.2.7 specifically state that field parameters must have stabilized to within 10% over at least 2 consecutive measurements. The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements must be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU below are included for information purposes only. • Fifteen well measurements and the measurements from Piezometers 2 and 3 exceeded the QAP's 5 NTU turbidity goal as noted in Tab H. All turbidity RPD's met the QAP Requirement to stabilize within 10%. DUSA's letter to DRC of March 26,2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspondence dated June 1,2010 and June 24, 2010, DUSA has completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. Redevelopment results will be discussed with DRC in an effort to come to a consensus regarding turbidity considerations for the nitrate wells at the Mill site. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab H. All samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation 11 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab H. All samples were received within the required temperature limit. 3.4.4 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the QAP. Analytical method checks are provided in Tab H. All methods were consistent with the requirements of the QAP. 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by the laboratory were checked against the reporting limits enumerated in the QAP. Reporting Limit Checks are provided in Tab H. All analytes were measured and reported to the required reporting limits, with the exception of 9 samples (8 samples and 1 duplicate) that had increased reporting limits due to matrix interference or required dilution due to the sample concentration. However, in all of those cases the analytical results were greater than the reporting limit used. 3.4.6 QAlQC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994,9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits. However, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All duplicate results were within a 20% RPD. Results of the RPD test are provided in Tab H. 3.4.7 Rinsate Check Rinsate checks are provided in Tab H. A review of the analytical results reported for rinsate samples indicated that one of the rinsate samples had a low level detection of nitrate at 0.2 mg/L nitrate. A comparison of the rinsate sample concentration levels to the QAP requirements --that rinsate sample concentrations be one order of magnitude lower than that of the actual well --indicated that the rinsate sample had concentrations of nitrate above this conformance level. 12 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx The nitrate concentration in the rinsate sample is just slightly above the detection limit and is not dependent on or affected by the previous sample concentrations. This indicates that the contamination is due to some external factor such as the nitric acid rinse during the decontamination process rather than cross-contamination from the purging process. However, based on the above findings, for this current quarter's data, the presence of nitrate in the rinsate sample does not affect the validity or utility of the groundwater data for the following reasons: • F or the one well in which the preceding rinsate sample levels exceeded the conformance criterion, the nitrate concentrations in the well and the rinsate samples were significantly lower than the GWDP GWCL of 10.0 mg/L for nitrate. • Low level rinsate samples are indicative of potential false positive results in the low level sample results. Higher level sample results could potentially be biased high. Both situations are a more conservative approach to the assessment of sample results because a high bias means that reported results for this analyte will tend to be more conservative or higher than actual concentrations. Complete assessment of the nitrate detections in the rinsate samples cannot be completed until the nitric acid rinse is removed from the decontamination process. To address the likely nitric acid contamination, DUSA has submitted a revised QAP (Revision 7.1) in which the nitric acid rinse step has been removed from the decontamination procedure when samples are not collected for heavy metals. UDEQ provided approval of QAP, Revision 7.1 on May 30, 2012. DUSA will remove the nitric acid step from the decontamination procedure and has initiated the assessment of the effect of this removal as of May 31,2012. If nitrate is detected in rinsate samples after the removal of the nitric acid wash from the decontamination procedure an investigation into the possible causes will be completed including but not limited to review of the laboratory procedures, split analysis of rinsate samples, and an investigation into the DI system. It is important to note that an appropriate DI system has been identified. Installation is scheduled to follow construction of other capital improvements in the Mill in late 2012 or early 2013. Corrective actions for this issue are described in Section 5.1. 3.4.8 Other Laboratory QAlQC Section 9.2 of the QAP requires that the laboratory's QAlQC Manager check the following items in developing data reports: (l) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate Analytical Laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm 13 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab H. All lab QAlQC results met these specified acceptance limits except as noted below. The QAP Section 8.1.2 requires that an MS/MSD (referred to as Duplicate Spike [Matrix spike] in the QAP) pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on DUSA samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze an MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review, and the results of this review are provided for information only. The information from the Laboratory QAlQC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for all quarterly nitrate samples are within acceptable laboratory limits for all regulated compounds as indicated in Tab H. The QAP requirement to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QAIQC Summary Reports indicates that the LCS recovenes were acceptable which indicate that the analytical system was operating properly. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. All analytical batches routinely contain a blank, which is a blank sample made and carried through all analytical steps. F or the Mill samples, a method blank is prepared for all analytical methods. The information from the Laboratory QAlQC Summary Reports indicates that the method blanks did not contain detections of any target analytes above the RL. 4.0 INTERPRETATION OF DATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab C. The data from this tab has been interpreted (kriged) and plotted in a water table contour map, provided under the same tab. The contour map is based on the current quarter's data for all wells. 14 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter The groundwater contour maps for the Mill site for the previous quarter, as submitted with the Nitrate Monitoring Report for the previous quarter, are attached under Tab D. A comparison of the water table contour maps for the current (first) quarter of2012 to the water table contour maps for the previous quarter (fourth quarter of 2011) indicates similar patterns of drawdown related to pumping of MW -4, MW -26, TW 4-4, TW 4-19 and TW4-20. Water levels and water level contours for the site have not changed significantly since the last quarter, except for a few locations. As discussed in Section 4.1.1, pumping at TW4-4, which began in the first quarter of 2010, has depressed the water table near TW4-4, but a well-defined cone of depression is not yet evident, likely due to variable permeability conditions near TW 4-4 and the low water level at adjacent well TW4-14. Reported increases in water levels of approximately 7 feet occurred in recently installed well TW4-27 and of approximately 5 feet occurred in well MW-37. Reported increases in water levels of approximately 9 feet occurred in pumping well TW 4-20 and of approximately 8 feet occurred in pumping well MW-26. The water level changes at pumping wells MW-4, TW4-4, and TW4-19 were less than 5 feet. Water level fluctuations at pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4- 20 are due in part to fluctuations in pumping conditions just prior to and at the time the measurements are taken. The largest decrease (increase in drawdown) of approximately 1 foot occurred in well TW 4-4 and the largest increase (decrease in drawdown), of approximately 9 feet, occurred in well TW4-20. The reported water level at well MW-37 during the current quarter is similar to the reported third quarter, 2011 water level, and the water level at TW4-27 is similar to that reported at the time of installation. Reported water levels at both wells in the previous quarter were lower than typical. The decrease in water level in TW4-27 in the fourth quarter of 2011 is due to the fact that the water level in that well was measured immediately following development activities prior to complete stabilization of the water level in the well. 4.1.3 Hydrographs Attached under Tab E are hydro graphs showing groundwater elevation in each nitrate contaminant investigation monitor well over time. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached in Tab F are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 15 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx 4.2 Review of Analytical Results 4.2.1 Current Nitrate and Chloride Isoconcentration Maps Included under Tab I of this Report are current nitrate and chloride iso-concentration maps for the Mill site. Nitrate iso-contours start at 5 mg/L and chloride iso-contours start at 100 mg/L because those values appear to separate the plumes from background. All nitrate and chloride data used to develop these iso-concentration maps are from the current quarter's sampling events. 4.2.2 Nitrate and Chloride Concentration Trend Data and Graphs Attached under Tab J is a table summarizing values for nitrate and chloride for each well over time. Some data (MW -18, MW -19 and the Frog Pond) were not sampled this period but the historical data are included for information purposes. Attached under Tab K are graphs showing nitrate and chloride concentration plots in each monitor well over time. 4.2.3 Interpretation of Analytical Data Generally, the shapes of the nitrate and chloride plumes appear to be stable and unchanged for the last nine quarters. The nitrate and chloride plumes maintain their general geographic association and it is still possible to separate the plumes into a segment northeast of the wildlife ponds and a southwest segment at the mill site. Nitrate and chloride concentrations in samples from the downgradient edge of the plumes (in the vicinity of tailings impoundment monitoring wells MW -30 and MW -31) have remained essentially unchanged (current concentration within one standard deviation of the average of the previous eight quarters and within laboratory variation) and the plume does not appear to be migrating in the downgradient direction. In general, nitrate concentrations in nitrate monitoring wells are similar to values from last quarter or have declined (Table 2). The nitrate concentration measured in TWN-10 of 0.8 mg/L is 300% higher than the 0.2 mg/L measured last quarter but lower than the 1.5 mg/L concentration that has previously been measured in samples from this well. Some chloride concentrations are up slightly from last quarter but, with one exception, are within the range of previously measured concentrations. The measured chloride concentration in PIEZ-1 of 78 mg/L is higher than the previous high of 60 mg/L (Table 3). The current quarter's data continue to support the conclusion in the Nitrate Contamination Investigation Report that the nitrate and chloride at the Mill site are co- extensive and appear to originally come from the same source. Note that samples from recently installed chloroform monitoring wells TW 4-26 and TW 4-27 had measured nitrate concentrations that are higher than 10 mg/L. However, nitrate concentrations in these wells are clearly separated from the nitrate/chloride plume at the Mill site by many wells that are below 10 mg/L or are nondetect for nitrate, 16 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx including but not limited to, TW4-23, MW-32 and TW4-16. Thus, nitrate in TW4-26 and TW4-27 appears to be isolated from the plume at the Mill site, in the same way that the relatively small nitrate plumes at TWN-09 and TWN-17 are isolated from the plume at the Mill site. 5.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below. 5.1 Identification and Definition of the Problem Rinsate Nitrate Levels One rinsate sample has nitrate levels that most likely result from decontamination procedures. 5.2 Assignment of Responsibility for Investigation of the Problem The problem has been investigated by the QA Manager. 5.3 Investigation and Determination of Cause of the Problem To address the nitric acid contamination, DUSA requested in the revised QAP the removal of the nitric acid rinse step when samples are not collected for heavy metals. DUSA received approval of the revised QAP on May 30, 2012. 5.4 Determination of a Corrective Action to Eliminate the Problem The corrective action is the removal of the nitric acid rinse from the decontamination procedures when samples are not collected for heavy metals. 5.5 Assigning and Accepting Responsibility for Implementing the Corrective Action It will be the responsibility of the Director, Compliance and Permitting to implement the following corrective action. The corrective action is the removal of the nitric acid rinse from the decontamination procedures when samples are not collected for heavy metals. 5.6 Implementing the Corrective Action and Evaluating Effectiveness Removal of the nitric acid rinse from the decontamination procedure has been implemented as of May 31, 2012. 5. 7 Verifying That the Corrective Action Has Eliminated the Problem 17 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx Verification that nitrate source(s) have been removed is underway. DUSA is currently evaluating whether the removal of the nitric acid rinse from the decontamination procedure has effectively removed the nitrate source in the rinsate blank samples. 5.8 Assessment of Previous Quarter's Corrective Actions Chloride was present in the rinsate blanks and in the DIFB for the fourth quarter 2011. To address previous nitrate contamination in the nitrate and chloroform sampling programs, an additional rinse with 55-gallons of DI water has previously been added to the decontamination process. DUSA believes that the source for the chloride present in the rinsate blanks in the fourth quarter appears to be related to the increasing volume of DI water used in the rinsate process due to the second 55-gallon rinse of the portable pump with DI water. The chloride present in the rinsate blanks is present in the DI water and is not the result of inadequate decontamination of the purging pump. The chloride contamination in the DI water is most likely the result of chlorination of the intake water (from the potable water supply source) used for the DI system. At high volume use rates, the DI system appears to be unable to remove all of the chloride introduced with the DI intake (supply) water. To address the issue, the QA Manager and the mill staff have identified an appropriate DI system. Installation is scheduled to follow construction of other capital improvements in the Mill in late 2012 or early 2013. Verification that chloride contamination has been eliminated will occur upon completion of the system upgrades and receipt of at least the two quarters of data. If chloride contamination persists then additional sources will be researched and the investigation will continue. 6.0 CONCLUSIONS AND RECOMMENDATIONS Generally, the shapes of the nitrate and chloride plumes appear to be stable and unchanged for the last nine quarters. The nitrate and chloride plumes maintain their general geographic association and it is still possible to separate the plumes into a segment northeast of the wildlife ponds and a southwest segment at the mill site. Nitrate and chloride concentrations in samples from the downgradient edge of the plumes (in the vicinity of tailings impoundment monitoring wells MW -30 and MW -31) have remained essentially unchanged (current concentration within one standard deviation of the average of the previous eight quarters and within laboratory variation) and the plume does not appear to be migrating in the downgradient direction. The current quarter's data continue to support the conclusion in the Nitrate Contamination Investigation Report that the nitrate and chloride at the Mill site are co- extensive and appear to originally come from the same source. 18 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 Ql\2012 Ql Nitrate Report text.docx 7.0 ELECTRONIC DATA FILES AND FORMAT DUSA has provided to the Co-Executive Secretary an electronic copy of all laboratory results for groundwater quality monitoring conducted under the nitrate contaminant investigation during the Quarter, in Comma Separated Values ("CSV") format. A copy of the transmittal e-mail is included under Tab L. 19 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx 8.0 SIGNATURE AND CERTIFICATION This document was prepared by Denison Mines (USA) Corp. on May 31,2012. DENISON MINES (USA) CORP. By: C. Fry enlund Vice President, Regulatory Affairs and Counsel 20 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and ent £ r knowing violations. Davi , . Vice President, Regulatory Affairs and Counsel Denison Mines (USA) Corp. 21 N:\Required Reports\Nitrate Quarterly Monitoring Report\2012 QI\2012 QI Nitrate Report text.docx Tables Table 1 Piezometer 03 111112012 TWN-03 1112/2012 TWN-06 1110/2012 TWN-OSR 119/2012 TWN-11 1110/2012 TWN-13 119/2012 TWN-16 1110/2012 TWN-17 1112/2012 TWN-19 1110/2012 Note: All wells were sampled for Nitrate and Chloride TWN-60 is a DI Field Blank TWN-65 is a duplicate of TWN-IO, and TWN-70 is a duplicate ofTWN-ll. UWLP is a sample from the Upper Wildlife Pond 1/23/2012 112312012 1123/2012 1/23/2012 1/23/2012 112312012 1123/2012 1123/2012 1123/2012 Table 2 -6 o 300 o 15 8 Red value indicates nondetect Table 3 Chloride (mg/L) 13 11 o o 10 20 -4 -3 6 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-l Field Data QAlQC Evaluation H-2 Holding Time Evaluation H-3 Receipt Temperature Check H-4 Analytical Method Check H-5 Reporting Limit Evaluation H -6 QAlQC Evaluation for Sample Duplicates H -7 Rinsate Check H-8 QC Control Limits for Analyses and Blanks Tab I Kriged Current Quarter Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Concentration Trend Graphs Tab L CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site MW-5 • perched monitoring well TW4-12 o temporary perched monitoring well TWN-10 ~ temporary perched nitrate monitoring well PIEZ-1 ~ TW4-27 ~ perched piezometer temporary perched monitoring well installed October, 2011 RUIN SPRING b seep or spring HYDRO GEO CHEM, INC. WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS DATE REFERENCE H:/718000/may121Uwelloc12.srf FIGURE A-1 TabB Order of Sampling and Field Data Worksheets o Nitrate Order 15+" Quarter __ ~Ol ~ Nitrate Samples p---------------------~ Rinsate Samples Nitrate Mg/l Name Previous Qrt. Date/Purge sample Depth Total Depth Name Date Sample TWN·8 0.1 TWN·13 0.1 TWN·I0 0.2 TWN-S 0.3 TWN-1 0.5 TWN-4 0.9 TWN-12 1.2 TWN-15 1.3 TWN-6 1.4 TWN-ll 1.6 TWN·18 1.9 TWN·7 2.2 TWN·16 2.6 TWN·14 3.9 TWN-19 6.5 TWN-17 8,1 TWN-9 10.9 TWN·3 25.0 TWN-2 33.0 Piezl 6.6 Piez 2 0.1 Piez 3 1.7 wildlife ND '-('WN bS f v.J,.J 1D TVJN ,-,0 \,-'1 . J;t 0 loS:l. \ ... (.\ -i;t 0 \~()'1 ',-iO-l~ 0 O~~O 1-'1 · t::l o (:):.t5 \ ~G\ -I'~ 0 ,Ybi l-t::t ·· i:l.. o \'1!)~ I~a;·\::.t.. 0 O'~I \ .• H "", lB.. 0 Oq:)y l·~fC-I~'2. o 0"111 1""lt -J:l o \OCr) \· .. }o -1'1.. o \O~':l. 1 ~\I ·~ o 0 '14"1 \·-lC ·-l~ 0 I~'-I.L. )··11 -I~'l... o bqh5 \ -10-\').. 0 \~I~ \-iA-I:l. 0 Dbba \ -p..\~ 0 1.)700 \-\:l. .. J~ o 07\() 1-\).,-\A o D1 \'6 \-\1-\d-.. \~\u \-\\. \1 \'}.?--.;' \-u -I;).. 0 \1.\0 11 -\\-\:2,. \~4 \-tC-l-:t I -10 -15.. I -I ~ -,~ Ob30 \003 .... twA} H \.') 'So 145.5 TWN-SR .-4"1& ,... 120 TWN-13R 105 TWN·I0R 150 TWN-5R 112.5 TWN-1R 125.7 TWN-4R 110 TWN-12R l -IC .. I~ 0,J5 155 TWN-15R 130 TWN-6R 142 TWN·llR 145 TWN·18R 105 TWN-7R 100 TWN-16R 135 TWN·14R 110 TWN·19R 110 TWN·17R l-u .. ij~ 01 iO 97 TWN·9R 96 TWN-3R 96 TWN·2R Samplers: Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) 1-------------------------------------------, IOENlsoJ)jjj ATTACHMENT 1 Attachment 1 C~ See instruction WHITE MESA URANIUM MILL ~t~.~_-__ J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I \ ST QV\.()..r+er N ,'1-('",,+-<:. ;l.O\R Location (well name ):_1 _Ll_W_L_P _________ ..... Sampler Name and initials: I ~nfl~t"" -l1 0 IlliJo.~/111 Date and Time for Purgin~ \-) 1-~o I~ and Sampling (if different) NIh '----------------~ Well Purging Equip Used:@]pump o@ bailer Well Pump (if other than Bennet) Sampling Event I Q\I\o.r+erl~ N,4("C\,+(; I p~c"Z .. O~ Prevo Well Sampled in Sampling Event '"-_______ ----' pH Buffer 7.0 1.0 pH Buffer 4.0 Specific Conductance I .... _It_'1.-;~~ __ ----II ~MHOS/ cm Well Depth(O.Olft): ..... 1 _0 ____ --1 Depth to Water Before Purgin~ ..... _O __ ----' 4" well:~O ___ -II (.653h) 3" Well:. 0 . (.367h) Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) I s -'-l ~ Redox Potential (Eh)1 ?~'1 Turbidityl ~ ~·5 Weather Condo IS 1\ . \A.n~ "\.1\Ch Wh\a.~ Ext'l Amb. Temp. °C (prior sampling event) 1_'_°_----' Time I J ?-3S Gal. Purged ..... 1 _D __ ---I Time Gal. Purged I .... ___ ----' Conductance 1 ';l4 ~ pH I g t! 7.2 I Conductance pH ,,--I __ ~ Temp.OC 1 p"yg I Temp.oC Redox Potential Eh (m V) 1 2. Y lj Redox Potential Eh (mV) _I ___ ----' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged , _____ -..1 Time Gal. Purged I'--___ ~ Conductance pH ..... I ___ -..I Conductance .... 1 ___ ----I pH ,"-I ___ --' Temp.oC Temp.oC " .... I ___ -....t Redox Potential Eh (m V) I _____ l-..l Redox Potential Eh (mV) .... 1 ___ ----' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Gr6'undwater lof2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged IL-__ o ___ ___ gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I () T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) () If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~,-N--L.V...;.~ _______ ...J Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 I!I H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 'gJ 0 Sample volume 0 ~ 0 ehl~r/de. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arri\led on ~ ,'1-<. ""t \~?·.oL <T""Y)"e.f q..,,,cA (n~("r;V) P('GSeJft t~ c...o)]-e.&+ SIAM pIes. tJ G-rcJ> Sa./"'I(>les.. ~"-1Vlp1G0 we.re: GolJ(.Gtcd oJ-l~'3Y )~35. ld..}.. :to bf"eJ'AK. ,u; 1-0 b" ~bk -to Sf4MfJ-c· ~i~1-v-r b~ wQ,-f(;r 0\. b0. \A)Q-te( J'n /1 ... &.....-________ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) 1·.··.···-··--····.·.··-··--······.·-·-········· ••• -··_ ..•.•.. -... , IOENIS.OJ)JJ , ATTACHMENT 1 Attachment 1 l:~ See instruction WHITE MESA URANIUM MILL "L-__ MINES w.~_~ FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 1 ~1 &\J\O\rf~r j\J \4(:(i>.,-T"<... :;;"'01:1\ Location (well name): .... 1 p_\-G_7.._-_0_\ ________ ---' Sampler Name and initials: l==t tV'\n-t:..r lJo 1} 1'J<\d/11:1 Date and Time for PurgingfL-)_7_1_1 _1~_O_)~ ____ ----I and Sampling (if different) .... 1 M_v4 ______ ---' Well Purging Equip Used: [gJpump 000 bailer Sampling Event 1 Q",,,,rtc.rb .N ~:tf""+C. pH Buffer 7.0 Specific Conductance .... 1 _4_q_4 _____ ---'I ~MHOS/ cm Depth to Water Before Purginm b,. bO Conductance (avg) Well Pump (if other than Bennet) r....1 ~_~_I'.f _____ ...... I \.AW\.. P Prevo Well Sampled in Sampling Event .... _______ ---' pH Buffer 4.0 LLO Well Depth(O.Olft): 11..--0 ____ ...... Casing Volume (V) 4" well:1 0 I <o653h) 3" Well:.1-6:r----...... (.367h) pH of Water (avg) I r.... _'_"_7_1 _____ ----1 Well Water Temp. (avg) I \ J,J ~l.. Weather Condo 1 .s,"'11~ c..nJ. w~nJ1 Redox Potential (Eh)1 ~ 75 TurbiditY L-13_. _b __ ...... Ext'l Amb. Temp. O( (prior sampling event) .... Il_d _---' Time Gal. Purged 1'-'0 __ ---' Time Gal. Purged 11..--__ ---.1 Conductance pH IJ.79 Conductance pH &.-1 __ ----' Temp.oC / 11.g~ Temp.oC Redox Potential Eh (m V) &....;/ ~_"7_S~_----I Redox Potential Eh (m V) .... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged .... 1 ___ ----I Time Gal. Purged .... 1 ___ ----I Conductance pH L-1 ___ ...... Conductance pH L-I ___ ...... Temp.oC Temp.oC Redox Potential Eh (m V) IL--___ ..... Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1'--_0 ____ ....... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I D T=2V/Q= I 6 I Number of casing volumes evacuated (if other than two) ~I _0 ___ -......1 If well evacuated to dryness, number of gallons evacuated ~I _D ___ ---' Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... _M_'f._ft _______ ...... Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 ttl H2SO4 ~ Heavy Metals 0 0 250 ml 0 0 RN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 Other (specify) E 0 Sample volume 0 19 0 C~) O(~ ~<. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A ('r " v <!J on ~ ,!h: .d-1~ '-11. -r /JI1111 ~ r ()JJ J. 6-1:>. •• :1') p1'e~el')t +0 Go 1 led-$. CA.,... flee, . ~AA"f1~ we,r-e, 6~~\~a (At 1~'-1b. L~ ~J1<' lA.1-1~L1~ '---________ ...... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 II 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r·----.·.·-·······.·-.. -.·-·.-·.··--·-·····--· .I ~E~~~~JJ I ATTACHMENT·1 WHITE MESA URANIUM MILL Attachment 1 ~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: "~,.. Q V\().. ... =te (" N:-l-Y'"o..f~ a.. 0 1';)... Location (well name):ll-.-f_1_e."'l.._ ... _O_A ________ --' Sampler Name and initials: , ~nY\ Gr"" R () 11,'J~Jrn Date and Time for Purgind 1-"-~ 0 l~ and Sampling (if different) ..... 1 /\/._'IA-______ ----' Well Purging Equip Used: [gJpump o@ bailer pH Buffer 7.0 7·0 Specific Conductance ..... 1 _4..;..~;....;~=---__ ...... 1 ~MHOS/ cm Depth to Water Before Purginm ) Ci • :3 '() Conductance (avg) Well Pump (if other than Bennet) I pjc;z~ 03 Prevo Well Sampled in Sampling Event 1... _______ ----' pH Buffer 4.0 11.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:~_o __ -II (.653h) 3" Well:. 0 . (.367h) Well Water Temp. (avg) I \, .70 Redox Potential (Eh)--.'_\_1_~ __ ...... Turbidity 1...' ...;...~_.7 __ ...... Weather Condo I I . S\An~ ~na \,0;(lUlt Time 1 tZ.;z.;.:::::::,-Gal. Purged --.1 _C~_. _~ __ ...... Conductance pH 1.-.' __ ----' Temp.oC Redox Potential Eh (m V) ..... 1 ___ --I Turbidity (NTU) Time 1 )~ Conductance Temp.oC 1 S~.Cj 1 J\.1() Gal. Purged IL--b ___ ...... pH 1 g ·'\7 Redox Potential Eh (m V) --.1 '_,_1;: __ ----1 Turbidity (NTU) I 8·, White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. °C (prior sampling event) ..... ' _,'1)_----' Time Gal. Purged a....1 ___ ...... Conductance pH 1.-.1 __ -----' Temp.oC Redox Potential Eh (mV) ..... 1 ___ --I Turbidity (NTU) Time Gal. Purged ..... 1 ___ ----' Conductance pH a....I ___ ...... Temp.oC Redox Potential Eh (m V) ..... 1 ___ ----' Turbidity (NTU) 1 of 2 I Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged II...-__ D ___ --.. gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = , 0 T=2V/Q=' D , Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L....-N.....:1,--A _______ .... Sample Taken Sample Vol (indicate Filtered Type of Sample if other than as y N specified below) y VOCs 0 0 3x40 ml 0 Nutrients 1!J 0 100ml 0 Heavy Metals 0 0 250ml 0 All Other Non Radiologics 0 0 250ml 0 Gross Alpha 0 0 1,000 ml 0 Other (specify) 1B 0 Sample volume 0 c, ~ \ C-r~ ~C Comment A~Y"'~~eJ. on f.;t~ 0-...1 ':2.1c!. -r;nner (AncA 6-d\fr:¥l pf'tr&C117 ='''''''ples lNere bo..;lco. ()...-T lX2.S. L~B-~ih: IA..t Ill7 I...-________ ...,,'Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 ~ 0 0 0 ~ Preservative Preservati ve Added Type y N HCL 0 0 H2SO4 ~ 0 HN03 0 0 No Preserv. 0 0 HN03 0 0 0 ~ If preservative is used, specify Type and Quantity of Preservative: ~ See instruction 2 of2 " Mill -Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 03/22/2010 Rev. 6 'c r .. _··· .. ··_··· .. · .... ·········· .. ········ ....... _._ ......... _ ............... "-"J'. II OENISONr:>~~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 L4~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER t-..;;-__ .. _~~.z.:,_~""_~~ ....... ~....,_ Description of Sampling Event: 1L-__ l_~.-__ Q_v.._()..._rt_G_(""_N_'=t_1'"_~_:\-_<.._?-_O_)_~ _____________ --I Sampler Name Location (well name):L-1 _P_\e_-z._-_O~3~ _______ ---1 and initials: I ~nn~;, 80 11;J\6\.cl /r1t Date and Time for Purgind 1 J 11 / ~o l":l.. Well Purging Equip Used: [QJ pump o@ bailer pH Buffer 7.0 7, "D Specific ConductancelL-_q-.:.....:.~...:.4 ___ ...... I ~MHOS/ cm Depth to Water Before Purgin~ '10· \....,~ Conductance (avg) and Sampling (if different) ,1\//.4-L--_____________ ~ Well Pump (if other than Bennet) I /II/A I ---:r wN'" O~ Pre v . Well Sampled in Sampling Event L--______________ ~ pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:~_o __ --1I (.653h) 3" Well:. D . (.367h) Well Water Temp. (avg) I 10.4'0 Redox Potential (Eh) L-I _1_t1_:, __ ~ Turbidityl-l_1_7_.1 __ ...... Weather Condo ILl \ . .:>v.."'(\~ (At'\ A '-'J ~ t\ fA '3 Ext'l Amb. Temp. °C (prior sampling event)L-1 _1 b_~ Time Gal. Purged 1-1 _0 __ ----' Time Gal. Purged 11.-___ ...... Conductance Conductance Temp.oC Temp.oC Redox Potential Eh (mV) 1-1 ...:.)...:.1"3"""-_----" Redox Potential Eh (m V) 1&....-___ --' Turbidity (NTU) I \/~ I Turbidity (NTU) Time Gal. Purged 1&.... ___ ----" Time Gal. Purged .... 1 ___ ~ Conductance pH 1'--__ ----' Conductance pH 1.-1 ___ -oJ Temp.oC Temp.oC Redox Potential Eh (m V)I I-___ ----" Redox Potential Eh (mV) ..... 1 ____ ----" Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 _0 ____ ...... -1 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1 D T = 2V/Q = 1 0 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Lab~ ..... _.tJ_/ 11 _______ ..... Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) Y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) rB 0 Sample volume 0 []a 0 Gh\or~c\( If preservative is used, specify Comment Type and Quantity of Preservative: ~ See instruction A (( ; '-l d 0 1\ ~ ;.t c: ~ t \:to 4. --r6.1\f\ Col" o.J\) (to.rr j (\ p r <:.serfl-11) [,01\ ed .. ~6.,Mp le.s, ~o'Mpb 'N-Gl"e bo.l'J~ ".,.} 1~1 0_ PH wc..s 1-l1~).,­ L -e+t 5:> \~+ C. cd ':2..)S L--________ ...... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater - N 0 0 0 0 0 ~ 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) f ...... ·········-·······--.. -··· ... -.---•• ----------_····· .. ···---1 I OENISoJ)A~1 ATTACHMENT 1 Attachment 1 b~ See instruction WHITE MESA URANIUM MILL L~_~IN!.~_.~_~_J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 11 ~-r D)uo..rTc, N .'+r,.+<.. ;J..j:) ,:2.. Location (well name): .... 1 _-r_W_N_-_O_' ________ ....J Sampler Name and initials: EGn"~'" Ho11;J~hH Date and Time for PurgingJ \ -G\ -;to'~ and Sampling (if different) '-I.;;.../IJ....;../~AL--_____ ...... Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) lG-rVlT1ir~ Prey . Well Sampled in Sampling Event I '-,_W;J __ -_Q5 _____ ....... pH Buffer 7.0 .... 1 _7_-_0 ___ ...... pH Buffer 4.0 L].a Specific ConductanceL...I....:Gf_'1...:...1 ___ ----II ~MHos/ cm Well Depth(O.Olft): 1 11;:l~ .so Depth to Water Before Purgind 5 1, ~ g 4" well:13 4 .10 g I (.653h) 3 " Well: 0 (.367h) L...-___ ...... Casing Volume (V) Conductance (avg) pH of Water (avg) 7.17 Well Water Temp. (avg) 1 14. ~3 Redox Potential (Eh)r....1 ~_8q __ ...... Turbiditylr....l_4_6 __ ......... Weather Condo Time )1..\04 Conductance Temp.oC I ~s 1 14.f:,7 Gal. Purged 1r....5_0 __ -.....I pH 17 .\7 Redox Potential Eh (mV) I ~b Turbidity (NTU) Time I )\j0Co Conductance Temp.oC 1 13k' Gal. Purged .... 1 _7_7 __ ...... pH 1 f.lg' Redox Potential Eh (mV) ,-I _;t_&_t.t~_--, Turbidity (NTU) I 14} White Mesa Mill Field'Data Worksheet for Groundwater Ext'l Amb. Temp. DC (prior sampling event)'-Iy_"_---' Time 111.1 oS Conductance Temp.oC 1 )Lj"7 Gal. Purged r....1 6_6 __ -.....1 pH 17 .}'7 Redox Potential Eh (mV) ,-I ~_8_q __ ---, Turbidity (NTU) Time L...oII ) ...... y...;;.,D_I _-----' Conductance Temp.oC I lYO Gal. Purged lr....g~8 __ -........I pH 1'0 )<1 Redox Potential Eh (m V) 1,-?-_8_~ __ ....... Turbidity (NTU) 1 1Y~ 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 11....-__ 8..;.,5 __ _____ Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ..... 1 _1_1 __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q=I /.I~ I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L-v'l/._~_I1 _______ ---, Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as y N specified below) y VOCs D D 3x40 ml D Nutrients ~ D 100ml D Heavy Metals D D 250ml D All Other Non Radiologics D D 250 ml D Gross Alpha D D 1,000 ml D Other (specify) rtI D Sample volume D C~lor;lc Comment Arr;\Jt;J on .s,=te tAt 1?>5 b . PU.(~-e. bej~t) 0..+ 1'354. Pv-."'~GJ. Y'1inv..-tes>. W"Jer ~~ MlAr\j. l\"'r~~ -ef){JeJ ~t1tA tiflllVlpl(1-s WCr-6 D'Gf~ +b ~~"h~(' \0a,.,S 7.5 .. 51J L~..fT S'+G t\.t JLJJD '---________ ...... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet fo(Groundwater N D 19 D D D ~ Added Type y HCL D H2SO4 E HN03 D No Preserv. D RN03 D D If preservative is used, specify Type and Quantity of Preservative: I:"2i See instruction ~ w ~I1 -For fA. +o-r~J of" g ~ol/ecr~J, a..-t }'-Io7, N D D D D D 8 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 ,----------------------------! lOENISOJ).4 .4 1 MINES ...__._J FIELD Dt TA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 b(~ See instruction Description of Sampling Event: 11 s O",-o..'ri"'er j'J\fr~f~ ~Ol':i Location (well name): .... 1 l1_W_N_-_O_~ ________ --1 Sampler Name and initials: rr~nt\e.r-Ho)1IJ~~/f)-j· Date and Time for Purgind l-1) -2D J'd-... and Sampling (if different) 11-tl-20 \~ Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) 1 (j.rtAt1Mb.s Sampling Event 1 Q\A~rf-t:.('G AJHrCf..fc.. Prev. Well Sampled in Sampling Event l,-w AJ ~ 03 pH Buffer 7.0 j.D pH Buffer 4.0 ~.o Specific Conductance .... 1 _~_~_q ___ --II ~MHOS/ cm Well Depth(O.Olft): 1 9b.O() Depth to Water Before Purgind ~ .. '37 4" well:1 LJg.O& I (.653h) 3 " Well: D (.367h) L--___ ...." Casing Volume (V) Conductance (avg) L--_~_b_~-'"il _____ ...." pH of Water (avg) Well Water Temp. (avg) '3.84 Redox Potential (Eh) .... 1 ..;..~_q_fo __ --I Turbidity I \ l. {, Weather Condo Ext'l Amb. Temp. O( (prior sampling event) .... 1 0_"_--, Time .... 1 b_~_lj+--_--1 Gal. Purged ..... 1 =SS __ ---I Time Gal. Purged ...... 1 ___ --' Conductance Conductance pH 1r--__ ....... Temp.oC Temp.oC Redox Potential Eh (mV) I ;Lq G Redox Potential Eh (m V) .... 1 ___ --II Turbidity (NTU) I 11.' Turbidity (NTU) I I Time Gal. Purged ..... 1 ___ --' Time Gal. Purged .... 1 ___ ---' Conductance pH ...... I ___ --' Conductance pH ...... I ___ --' Temp.oC Temp.oC Redox Potential Eh (mV) ..... 1 ___ --' Redox Potential Eh (m V) .... 1 ___ --' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 MiII-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) -Volume of Water Purged ..... 1 -.;55=-___ ----1 gallon(s) - Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 1) T=2V/Q= I ~./L1 I Number of casing volumes evacuated (if other than two) I \. }Y If well evacuated to dryness, number of gallons evacuated 155 Name of Certified Analytical Laboratory if Other Than Energy Lab~,--_/\I._1~ _______ --, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ffi 0 100ml 0 g H2SO4 l!I 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) iii 0 Sample volume 0 I:B 0 ~ c.~ \D'; cJe If preservative is used, specify Type and Quantity of ~ Preservative: Comment ~ See instruction A (I'" i \l e ~ 0(1 S ffe uJ M II. ~n n if "'h J.. G-0. rt',' r') pr e-.se.,J ..Qr l.'j.::j-e. Pv.~~ b~..." 01.-1 o'Wt fv-("~ea ~6\\ .for (}... +0+0-.' 6-\ b ~i(l~e.? P\A.r8t:~ W-e 11 dr~1 \t.:)Ov-t<=r ~a..$ M o.s-.t)~ c.1~~J\ PVJ"'~e enW ~ O'f11. L.J} &iJG ~ Oq~ Itrr;'\J-eA 01" s,"t" 17\.+ 0'11'3, ~hner c>..nrA Gd\. rfl'~ pr~a'\+ 10 coHe.d ~"fl~-Jep}tl it:> v>.a..t-er vJ~ ~.)D. ~o.Mp\es 1.Ne:,(t:.. b~I\)ecl ~+ 071g~ Le..~ ~fk d\,t D7~ L...-_______ ----I1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ()ENISOJ)j~1 [ ....... _ ............ __ .-... _ ........ -... _ ...... _ .... __ ._ ....... _-_._., ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~~ See instruction _._ .. ~MIN ES_~_~J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 l~'" Q",O\.(+o--.N ,'tf IJ\.+~ a.O 1:1. Location (well name):I'--~_vJ_N_-_O......;3~ _______ ----' Sampler Name and initials: l j6.nn'Cr" 8oll"J~ /rJ.t Date and Time for Purgin~"--1~_'_1 _-2._0_1;....a~ ___ --..I and Sampling (if different) a....1 ,_-..... 1~_.-_2_0_)_;).. ____ --' Well Purging Equip Used:OO pump o r@] bailer Well Pump (if other than Bennet) 1 G-rv..l"\tA.f'o-s Sampling Event I QVl.o..rtuk! N;O}r""t< Prevo Well Sampled in Sampling Event I TlIVfiJ-0'1 pH Buffer 7.0 7.0 pH Buffer 4.0 Specific Conductance'--I_1.:...q......;<4 ___ ---'I ~MHOS/ cm Well Depth(O.Olft): 1 q ".00 Depth to Water Before Purgin~ '3~.04 4" well:1 g 1.68 1(·653h) 3" Well:"b (.367h) L---___ __I Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 1 13.li'J Redox Potential (Eh) 1,,--~_":7_'t __ __I TurbidityL-l_l00 ___ __I Weather Condo l __ I __ ~ _______ ---, _ :::::'~f\n1 Time I 0 ~ I..\'J-.. Gal. Purged ...... 1 .-3~4i---_--I Conductance Temp.oC Redox Potential Eh (mV) L-I =-A;:...-:7_q~ _ __I Turbidity (NTU) Time Conductance Temp.oC I 100 Gal. Purged I"--__ ~--I pH IL--__ ----' Redox Potential Eh (mV) 1"--___ __1 Turbidity (NTU) White Mesa Mill Field DataWorksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)1 0 b Time Gal. Purged ...... 1 ___ __I Conductance pH ....... 1 __ ----' Temp.oC Redox Potential Eh (mV) L-I ___ ---I Turbidity (NTU) Time Gal. Purged L-I ___ ---' Conductance pH ...... I ___ __I Temp.oC Redox Potential Eh (m V) L-I ___ ---' Turbidity (NTU) 1 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 --=3:;....4"--__ ---1 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = ...... 1 __ ll __ ---' T = 2V/Q = 1-r·Y{' 1 Number of casing volumes evacuated (if other than two) 1 ..... ·_9_9 __ ---1 If well evacuated to dryness, number of gallons evacuated ..... 1 _~_~ __ --' Name of Certified Analytical Laboratory if Other Than Energy Lab~I-_N_I_A _______ ..." Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 100ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) [!] 0 Sample volume 0 m 0 ~ G hor'\~{ If preservative is used, specify Type and Quantity of Preservative: See instruction Comment Arr;~ e! 0 n ~ i+t: 0..+ () 836, ~"ner M.1. (,..0.,.: n f"'e~"...t -Po r f'\.\r~ e . P -.or~..,. l,~ "'" '" + 0 8 ~ 1 ? .... r~".,), we.ll.fo,-"" h+ ... 1 o.f' '3. ",,/lIlAtQ ....,,J. '35 S"'GonJ$. l\ ... .-~e~ W&l1 J.,..~. f v-r~ c cnd..:Jv {),.-t 0 8l.\~ . 1A)J. 0-w~ \'l'llAr 11<:'}_ LeA!5. ,'+<: .J-0 8tjIl . Afr\\)~ on S\1-~ 0...1 o.o~. -r'o.(\\"I'(,J'" ~}'\~ frt.1,.rr;f\ prc,seytt" to ~llcd-.5()1.YI'lples. Depfh--h wo..Tcr V\)"'~ 3~. ~ ..so..\'np\~ wc::,r~ ~a<.a tcl-b71D. Le..t:'~ ~~'k o.:} 67Jd-. L--________ ..."IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 1~~:~~~J5ii l WHITE MESA URANIUM MILL Attachment 1 ~; See instruction -l_ MI~~~,_._.....J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I \ ~=r Q\A.~("fc(' /V (tcO\f-e. ~O \ 'd-.. Location (well name): ...... 1 _T_W_N_-_O_Li ________ ----' Sampler Name and initials: 1==t:.t\nGY" l"Jolh'a~ JrH- Date and Time for Purgind ,-4 -~o la and Sampling (if different) L.--/V_Y;_~ ______ --, Well Purging Equip Used: [][]pump o@ bailer Well Pump (if other than Bennet) I G--rMiA:Po...s Sampling Event I Q", j),.,-h:c ~ )'\) ;.} r", f <! Prev 0 Well Sampled in Sampling Event! Tw AI -0 \ pH Buffer 7.0 Specific Conductance ...... 1 _Ci_'t_~ ___ ----II ~MHOS/ cm Depth to Water Before Purgin~ '-\0. ~O Conductance (avg) J01~ pH Buffer 4.0 \ .. tD Well Depth(O.Olft): I '2.5. 7D Casing Volume (V) pH of Water (avg) 4" well:! ..9>$.3 !(o653h) 3" Well:. 0 . (.367h) I.()O Well Water Temp. (avg) 1 1~.:;l3{ Redox Potential (Eh) 1 ...... :t._'_1 __ .....I Turbidity I ~ 'tS Weather Condo Ext'l Amb. Temp. °C (prior sampling event)IL-3_o_--, Gal. Purged .... 1 ...;;..41..1.--_----1 Conductance \O~O pH I 7.00 Temp.oC 1y.~g Redox Potential Eh (m V) I g:7~ Turbidity (NTU) Conductance Temp.oC Gal. Purged .... 1 _l _;t~l _----I pH I 7.00 Redox Potential Eh (mV) I ')..7, Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Time 1 1Y~ Gal. Purged· ...... h;...l(} ___ --' Conductance 10\8 Temp.oC Redox Potential Eh (m V) ...... 1 .:;..;;;....,.;-:7;...:.1 __ --' Turbidity (NTU) Time t.....;11....;.L.J=..5....1.Y_----I Conductance I '6 'L:\ Temp.oC I a.4.5 Gal. Purged ...... 1 J:...;;~;;.;;;Dt~_----' pH I,.()'O Redox Potential Eh (mV) 1L...I;?~7_1 __ --, Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 -:..1...;;;;3 _g... ___ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-.1 _'_1 __ ---1 Time to evacuate two casing volumes (2V) T = 2V/Q = I \0. t5 I Number of casing volumes evacuated (if other than two) 1 p/~ If well evacuated to dryness, number of gallons evacuated I ,AJ/A Name of Certified Analytical Laboratory if Other Than Energy Lab~ L. ~tJ_I_A~ ______ .....I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100ml D ~ H2SO4 ~ D Heavy Metals D D 250ml D D RN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D RN03 D D Other (specify) ~ D Sample volume D ~ D ~ G""or~Je If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction L--________ .......IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater "2of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r-------~-----------------1 ATTACHMENT 1 lOE1lJ~~~~ ~ FIELD DA~~~::S~E~I~~R~~;D WATER Attachment 1 b.<~ See instruction Description of Sampling Event: I ) £T Q\)..o...r+<...-Y" N;.tr ""+ G ;2. 0 I ~ Location (well name): .... I -_~ _v.'_N_-_O_6 _________ .... Sampler Name and initials: 1 ')A.n(\U" flo) t;J ~ /""1"tt Date and Time for Purginm , .... t\ -26 , ~ and Sampling (if different) ..... 1 M--:...;I'A~ _____ ---, Well Purging Equip Used: [ff] pump o@ bailer Well Pump (if other than Bennet) Prev. Well Sampled in Sampling Event 1 ..... -r_W_tJ_ ..... _l_D ____ .... pH Buffer 7.0 I __ /~' _0 ___ ...... pH Buffer 4.0 Specific Conductance ..... 1 _4.:...:~...L.q ___ ---'I ~MHOS/ cm Well Depth(O.Olft): 1 18'D·Ob Depth to Water Before Purgin~ b 'f '/~ 4" well:I .5~·t..1.3 i(·653h) 3" Well: () (.367h) '"----_ ...... Casing Volume (V) Conductance (avg) pH of Water (avg) .... 1_b_._Q; ______ ...... Well Water Temp. (avg) I lL{.4Q Redox Potential (Eh) ..... 1 3_0_5~_ ...... Turbidity .... 1 ~_.Cj __ ---, Weather Condo I 0 , o..("-i-G (J () v.. ~ ~ L--____ ~ ______ ~~ ______ --' Time Conductance Temp.oC 13D78 11L\ .50 Gal. Purged 1L--7...;.7 __ ...... Redox Potential Eh (mV) 1 ::So 7 Turbidity (NTU) Time 1'--1-=3.;....;a.~-'--_ ...... Gal. Purged ..... 1 9.1....l1'---_--' Conductance 1 '::>071 pH I C.b" Temp.oC Redox Potential Eh (mV) 1 ~65 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. °C (prior sampling event)I ..... Y_'_---' Time Conductance Temp.oC 13b 75 1 1'1· q1 Gal. Purged ..... 1 8;;....;;g~_--' Redox Potential Eh (m V) .... 1 '3_°_, __ ...... Turbidity (NTU) Time &...II )-=~;.:;.;tS=-_---, Conductance Temp.oC 1'3 0 7[;"" I ,q.41 1 5·0 Gal. Purged .... 1 J;..;..J {)~ __ .... Redox Potential Eh (mV) I :305 Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 _'_I_D ___ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = ...... 1 _1 1 ___ --' T=2V/Q= 1 CJ.53 1 Number of casing volumes evacuated (if other than two) NIII If well evacuated to dryness, number of gallons evacuated 1 ..v/,4 Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... ~_V_A _______ ~ Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs D D 3x40 ml D D HCL D Nutrients ~ D 100ml D ~ H2SO4 ~ Heavy Metals D D 250ml D D HN03 D All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) "2j D Sample volume D ~ D G~ \ o(',Jc If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A (p";; ed. on ~ ,'+ e .d 1'3.11. -r", '11\ ~ r "''' ~ G-... rr; ~ f'" e.serrY .to r f Vcr ~ e.. o..n J s '1M f 1 i2j -e v e .,+. ?"'ft.Q. be'~o.n 0..+ 1'2> ,~. ?"'('SG~ \N-G\I .tor '" 1-6+J or \C> M;r\Vv1e,s~ W().l+~r (,.)CA.5. G1eCA.r-~ P'-A.~j~ "encJ.ul (AI'\~ ~o..l'V\p)~ W~(e GolteG~J o,.-t )3~. PC:F~ +0 l".)D\.+G..-Wo.s 83.11 Le.f\-~ltC. ~ )3.2..8 '--________ ...... IDo not touch this cell (SheetName) White Mesa Mill Field Data WorKsheet for Groundwater N D D D D D 111 " 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) 1 ·_· __ ·-. __ ._--.----_._------_._._--.. _---_ ... _---- OENISOJ)jjl L.~_IN,~_~~ __ .~J ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 [_.~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 \ ~T G v.~rfY'" ..N ,JY·o..ii ~o JR Location (well name ): .... I-r_W_N_-'"_D_" ________ ----' Sampler Name and initials: I=t:n"u Ii oI1IJ~~ /-rij- Date and Time for PurgingJ.,-'_~_l_()_-:1.._0 _1 ':l. ____ --' and Sampling (if different) &.-.1 _1\1_/...;,A ______ ...... Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) I c:rtJIn&f'o..s Sampling Event 1 Q~('fd'~ IV ;·h··J-e. Prev. Well Sampled in Sampling Event I TvJAJ-1.5 pH Buffer 7.0 &.-.1 _7_, D ___ ---I pH Buffer 4.0 Specific Conductance&.-.I ...;.4q..;...~~ __ ----,1 ~MHOS/ cm Well Depth(O.Olft): I \3D.OO Depth to Water Before Purgind 15. ~ b Casing Volume (V) 4" well:1 ~S. 7 J 1(·653h) 3" Well: 0 (.367h) '--------' Conductance (avg) pH of Water (avg) Well Water Temp. (avg) I ILl .. 33 Redox Potential (Eh)L-13_5_0 __ --I TurbiditYL-1 _'4 __ ----' Weather Condo Ext'l Amb. Temp. °C (prior sampling event)I-:t° Time &.-.1 o_q_D_~_--, Gal. Purged &.-.1 _'1_4 __ --' Time &.-.1 D_'l_O-'-:t_---' Gal. Purged &.-.15_5 __ ---' Conductance I ) b ;;, ~ Conductance 1 H;l) q Temp.oC Temp.oC 1 }4.3~ Redox Potential Eh (mV) &.-.1 3_55 __ --' Redox Potential Eh (m V) &.-.1 3_5_Y~_--, Turbidity (NTU) Turbidity (NTU) 1 J'1 Time 091Q Gal. Purged I ...... _b_' __ ....... Time ...... 1 0_'1...;.,..1..a...1 _--' Gal. Purged 1 ...... 7 ........... 7 __ --' Conductance 1\573 pH I b·iLI Conductance IISbg pH 1'·25 Temp.oC I l,\.sq Temp.oC ny.'S::> Redox Potential Eh (mV) ...... 1 ':S_q_9 __ --' Redox Potential Eh (m V) ...... 1 :5_11_8 __ ....... Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged 1-1 _....;.1.....;1'--__ -..1 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 11 T = 2V/Q = I (;. '-\ 'i 1 Number of casing volumes evacuated (if other than two) 1-1 --.;;;..0 __ ----' If well evacuated to dryness, number of gallons evacuated 1 L-_b ___ ....... N arne of Certified Analytical Laboratory if Other Than Energy Lab~L-#._1 .4 _______ ---1 Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 RN03 D All Other Non Radiologics 0 D 250ml 0 D No Preserv. D Gross Alpha 0 0 1,000 ml 0 D RN03 0 Other (specify) 1E1 0 Sample volume 0 ~ 0 Ch'or~de If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A ..-r;\Jea on ~l+e.. 0\+ o~ 01. \",nn-er "'-'lot G-fA.(r in yre,sen,f ~ (" pu..r~~ Af\,A ~r'V\f'l~ e\)e",t. ?w-~e b~ .. .f\ ... ~ 0'10'1. f'u..r~""\ ...:,<>11 -tor .... +0+.0..\ of' I Mifl",tc.s. U)o..-j--v W,,", MO.s+l d G~e~~" 'PlA.r~e., e"ttea 6;.f'I~ ~fAlY)plt!$ ~er( to JI~G+--eJ oJ-D'fll. Depth n u)Cl.+-er W4S f5~~o" Left-srt--e., ~i 09lLf ~ ________ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Data WorRsheet for Groundwater N D D D D D ~ .' 2··of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ,···---···-----·----------------.. · .. 1 ATTACHMENT 1 I OENMI.SINO'ENsl)~ ~ ': WHITE MESA URANIDM MILL Attachment 1 b.4;<,~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 1~'" Q '-\o..,.-t-e.r ,tV ~·+r(.\.fG ?.Ol~ Location (well name): .... 1 _'"f~W_N_-_O_I _______ __' Sampler Name and initials: I~nn-e(' HolJJOJ~/TJt Date and Time for Purginm 1 -1 0 .. :2..01 A and Sampling (if different) 1-) 1-20 l~ Well Purging Equip Used: []I] pump o@ bailer Well Pump (if other than Bennet) 1 z;::t:'-\1\J"Po ~ Sampling Event Qv.tA.rh::rl~ IV ~\1-,.o..f<. Prev . Well Sampled in Sampling Event I L-'_W_N_-_l 8 ____ ---' pH Buffer 7.0 1r..........J7L.:..,_O __ ----' pH Buffer 4.0 4.0 Specific Conductance .... I--:..4q_q ___ ---II ~MHOS/ cm Well Depth(O.Olft): 1 lOb .00 Depth to Water Before Purgin~ 8.8, ~o Casing Volume (V) 4" well:l lO,70 I (.653h) 3 " Well: () (.367h) '----_ ..... Conductance (avg) .... 1_1_1_C_l.f ______ ..... pH of Water (avg) Well Water Temp. (avg) 1 rS.JJ Redox Potential (Eh) 1 3Y7 Turbidity 1 18 ~ Weather Condo I P 0 .. r1'1oj Col 0 IAcl1 Ext'l Amb. Temp. O( (prior sampling event) .... I.2_o ______ Time I) ?.O3, Gal. Purged &...1 -.;;g~_----, Time Gal. Purged &...1 ___ ~ Conductance pH 1 c.t'iJ Conductance pH ,,--I __ ----' Temp.oC r~.77 Temp.oC Redox Potential Eh (m V) L-I _3_4_' __ --' Redox Potential Eh (m V) 1'--___ ..... Turbidity (NTU) 1 I~·S Turbidity (NTU) Time 'L-, ___ ---I Gal. Purged ,L--___ ~ Time Gal. Purged .... 1 ___ ---' Conductance pH ,1.--__ --' Conductance pH .... I ___ ....... Temp.oC Temp.oC Redox Potential Eh (mV) L-I ___ ---' Redox Potential Eh (m V) .... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater .. 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged It.-.----.;;.g_-___ ....... Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 11..--_11 __ --' gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = 1 1. qlf I Number of casing volumes evacuated (if other than two) I ~ gg If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L-/V---';'j,_'A _______ ....... Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml '0 ~ H2SO4 "fJ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 Other (specify) ~ 0 Sample volume 0 1lI 0 Gh\or\Jc If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arr;u~a Of' ~ft~ 0.:+ \200. -rArlner tAh,).. 6-Arritl pr-eSe'1-t-+or rV\r~'(!. ?\.-\~<-b~~ ~.} ,~o:>. 'Pu.r~-eJ well fOr '" +d"J ~ 45. S~Gon4s. Pv.r~..,.~ woll J.r~. \.:l.J-..-v=.S 1Y)6~!j (,Je~r, p ~(' ~e" -G1'\Jd, oJ.-1 ~o L) ~ \...eJ:} 5 ~t c, ~ 1.:2.0 ~ Ar(j\le..d. on ~,h:, IA.r 01SYO. ~hn-G( ~ntA &(J..'((;" flr~s.en+ tb (.611"vt-SCtw1pJe.S. Dep+h to ~(Att1" \,.:)~~ 4 J. ~ g~ ~{i\J'V\pl<;.S \N e(<.. 'oo.;lt.t\ I\. t-otf U . \...e:f! S lIte £Itt 0'1 YL. L--________ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r·--···-··----·-···---.......... ---.. -, . ATTACHMENT 1 I OENISO. ,!)~ ~ I WHITE MESA URANIUM MILL Attachment 1 [~ See instruction L-M!N!~_._ .. _ .. _~J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 11 Sf" Q",a-.r+<r N,'·h"o.-t~ ~C> 1:J,. Sampler Name and initials: '~nne« Holll'J~ /rH Location (well name ):IL.--r_W_N_"'_O_8~ _______ ---, Date and Time for Purgind ,-~ -:2.01::l and Sampling (if different) .... 1 N--=-./....;:4 ______ .....I Well Purging Equip Used:OOpump o@ bailer pH Buffer 7.0 -1.0 Specific Conductance,--' _q_q_1"-__ ---'I ~MHOS/ cm Depth to Water Before Purgind b I" f,<1 Conductance (avg) Well Pump (if other than Bennet) . , G-"'lA.n~-Fo..s Prevo Well Sampled in Sampling Event I TWtJ-6g R pH Buffer 4.0 Well Depth(O.Olft): '\'4 S. SO Casing Volume (V) 4" well:IS'"I.7.?-Y 653h) 3" Well:. b _ (.367h) pH of Water (avg) L.-17_.9,5 ______ ---' Well Water Temp. (avg) '\'-l.~g Redox Potential (Eh) 1L-\_.5_Gf~_--, Turbidity ..... I.2_·_LJ __ --' Weather Condo Time 1L.-_1 {)_l..\_~ __ --, Conductance Temp.oC 1 ~"'!>4 Z 1 14.?~ Gal. Purged &...., _g...;;;l>~_ ...... Redox Potential Eh (mV) 1 1 fA Turbidity (NTU) Time .... 1 l_{)-=~;...;.-._---, Gal. Purged .... 1 _l.;...IO __ ---' Conductance Temp.oC Redox Potential Eh (mV) 1 \ St{ Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater .' Ext'l Amb. Temp. O( (prior sampling event) .... 1 _D_D_--, Time .... 1 _1 <5_5_0 __ --' Gal. Purged 1........:-'1 q~_---, Conductance Temp.oC I 14 .2.'1 Redox Potential Eh (m V) 1-1 _1..:;;;S ... j __ .....I Turbidity (NTU) Time 1 )05~ Gal. Purged .... 1 '_~_l __ -.....I Conductance pH I 7.:2.;).. Temp.oC 1 1q.~j Redox Potential Eh (m V) &....1 .=J5;.....'1:....--_.....I Turbidity (NTU) :;t.y 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 11....---:.,1_"_] __ ----I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1,,----,1....;....1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I q.q.s I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... N---,-!_A;...-.. ______ ....I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 100ml 0 ~ H2SO4 rgJ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) m 0 Sample volume 0 ~ 0 I2g o h 1 t>\~'c\~ If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction L...-________ .....I1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2' Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r----------------.. -.-.--... -.-.... -----.. --.------·····---·-·1 I OENISONr;,~ ~I ATTACHMENT 1 Attachment 1 l:~ See instruction WHITE MESA URANIUM MILL L ____ M~~!.~ .. ~~~~_ FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 U?>T Qv..o..f"i-~(" N ;t-ru.. fG ~o \~ Location (well name ): .... 1 _T_'N_N_-_O_~_R ________ ...I Sampler Name and initials: 1 ~t'\ne.'" Holt ;JA~ /rtf Date and Time for PurgingJ 1-Gl-;1.0 1 ~ . Well Purging Equip Used: [IDpump o@ bailer pH Buffer 7.0 7.0 Specific Conductance .... 1 _'1_~..-;.4 ___ ...... 1 !lMHOS/ cm Depth to Water Before PurgingJI-_O __ --' Conductance (avg) Well Water Temp. (avg) 1 ~~ q and Sampling (if different) .AI/ ~ "---------------~ Well Pump (if other than Bennet) I ,/'-1/11 Prevo Well Sampled in Sampling Event ..... __ -----------------1 pH Buffer 4.0 Ll. D Well Depth(O.Olft): o Casing Volume (V) pH of Water (avg) 4" well:~_o __ --II (.653h) 3" Well:. <> . (.367h) TurbiditY L-1 _0 __ ---1 Weather Condo .... I _~_' o_v..._cA....;:j~ _______ ---I Ext'l Amb. Temp. °C (prior sampling event)l -LJ () Time Gal. Purged 1-.1 _17;......0 __ --' Time Gal. Purged 1-1 ___ ----' Conductance S.b Conductance pH L..-I __ ----' Temp.oC Temp.oC Redox Potential Eh (mV) I q b g Redox Potential Eh (m V) 1-1 ___ --' Turbidity (NTU) o Turbidity (NTU) Time Gal. Purged 1"--___ --' Time Gal. Purged 1-' ___ ---' Conductance pH I'---__ ~ Conductance pH 1-.1 ___ --' Temp.oC Temp.oC Redox Potential Eh (m V) 1-' ___ --' Redox Potential Eh (mV) 1-1 ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater -. lof2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 _~_O_o ___ --, Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = \L.o-1_1 __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I D I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated D Name of Certified Analytical Laboratory if Other Than Energy Labf ..... _~_/_It _______ -I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients ~ 0 100ml Heavy Metals 0 0 250ml All Other Non Radiologics 0 0 250ml Gross Alpha 0 0 1,000 ml Other (specify) ~ 0 Sample volume Chlorla~ Comment y N 0 0 0 ~ 0 0 0 0 0 0 0 ~ Added Type y HCL 0 H2SO4 1!1 HN03 0 No Preserv. 0 HN03 0 0 If preservative is used, specify Type and Quantity of Preservative: r-:-.J. See instruction ~ Af"r:veo.. on ~l1-~ a-.-r Ob~7. -rl1\n1'\e~ CAn;" O-iXr,..in rre.se.I)T -t:"'or r,'11S01+e. p.;ns.~-tc. b~j~f\ ~+ HYOS. \J\MV\pe~ SO &Ct..l'o~ or A~IJ. WA.~(,(', 50 ~""lJon..s ~ou,.f' W",t-er 1 IDe, & ... ]Idn.!. 6f' j) 1:. wc...+er-. R;n.s",t-e. ~"JeJ a",J ~Q"1pl~ Wt;'(.., Gol\-e.c:..~A ~t 1o~. Le-B-.5J:g..~ ""t 10~7_ L...-________ ..... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 r:E~~~~jjlll WHITE MESA URANIUM MILL Attachment 1 ~ See instruction l _-_!AI~E~_~ ____ ..... _.J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 $oT Gh ..... o..,...+er'" .N ,W ... ",i=<. ~ol~ Location (well name):I .... 1'_vJ_N_-....;;Q;....;:q:....-________ --' Sampler Name and initials: I M1\t1~r Noll ,lJo.1:1/'fIJ Date and Time for Purgind \ -, 1 ~ ~ 0 I ~ and Sampling (if different) l-I:2.-~o\~ Well Purging Equip Used:OO pump o@ bailer Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event 1 .... _tw_N_-_1_7 ____ --I pH Buffer 7.0 7.b pH Buffer 4.0 Specific Conductance .... 1 _~_q....:..1 ___ --II !lMHOS/ cm Well Depth(O.Olft): ...... 1 _Q7_,_o_o __ --a Depth to Water Before Purgin~ b ~. 0 b 4" well:1 ~. U. i(·653h) 3" Well: c> (.367h) L--___ ...... Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 1 13.13 Redox Potential (Eh) 1 -:3~ Turbidity .... 1 -'II1II'3=6;.;...;..1_---' Weather Condo I ( ~ \A..Y'\l"\t L--___________ ---' Ext'l Amb. Temp. O( (prior sampling event) 1 .... _0_°_ ...... Time 1 O~D:S Gal. Purged ...... 1 ;;4_'d... __ --a Time Gal. Purged 11-.-__ ---' Conductance I ~b Conductance pH 11-.-__ --1 Temp.oC 1 \'3.13 Temp.oC Redox Potential Eh (m V) 1 3~S Redox Potential Eh (m V) .... 1 ___ --I Turbidity (NTU) Turbidity (NTU) Time Gal. Purged &....1 ___ ---' Time Gal. Purged .... 1 ___ ---I Conductance pH .... I ___ ..... Conductance pH ...... I ___ ...... Temp.oC Temp.oC Redox Potential Eh (m V) &....1 ___ ---I Redox Potential Eh (mV) .... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater -1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) -Volume of Water Purged 1L....-_2_2......:.-__ ---J Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I _~\ __ -J gallon(s) - Time to evacuate two casing volumes (2V) T = 2V/Q = I L\.()~ I Number of casing volumes evacuated (if other than two) I ·119 If well evacuated to dryness, number of gallons evacuated I ~ Name of Certified Analytical Laboratory if Other Than Energy Lab~L....IV_:/._~ _______ ---I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients lJ 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,OOOml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 T1 0 Lydor~~f If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arrivc.d 01'\ Si-t~ ~-t OgOOJr-r~t1(le,.. (WId.. 6-o.'t'(ill pl"t.SGT\+ -For pv..('~e . P\A""'~' b~~Y1 ",t ()g03 P\A~~ «cl. \,)(',11 .for fA. -1-01-,,) ot 2. M i fl...tCS . "P ... r~.,J, W ell J.r~. ?ur{l <:. end"J. ..:T 08 a.5. v:>~ lNCt.S MtA.r'"k~. Left-~rtG ~-t-0808 Arr;~e~ on ~rt~ 0...+ Dbs~. --rb.nt)er AAJ. ~()..rr"V\ p re.sey\-t -to GolJe,c.t S~.rl"'P]~ Pe~ -b vJ()\.ivr ~00 ~3,~O. S"-Mr\e.s Wert.. bCl\ile.d ~t 0100, L~ ~~ ~616~. L..-________ --IIDo not touch this cell (SheetName) White Mesa Mill -Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 WHITE MESA URANIUM MILL -Attachment 1 b(~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: / ,~,.. Qv..~r+~r-N ;·h-o.-t-G ;2.0 \~ Sampler Name Location (well name):/ --rWN-" \0 and initials: l --rAnn~r HDJl.cJCA.1d /TId- Date and Time for Purgingj 1-E\..> 20 I ~ and Sampling (if different) / \ --l 0 -:2.. 0 I ~ Well Purging Equip Used: IT[] pump o@ bailer Well Pump (if other than Bennet) / (j.r~J~s Prevo Well Sampled in Sampling Event 1-"",.AlA» 13 pH Buffer 7.0 7.0 pH Buffer 4.0 Specific Conductance 1....../ _1_'f~1"--__ ---'/ ~MHOS/ cm Well Depth(O.Olft): loS.e;!:> Depth to Water Before Purgind ~ I . DJ.. Casing Volume (V) 4" well:1 Ls. bE I (.653h) 3" Well: b (.367h) "------' Conductance (avg) pH of Water (avg) 3. ':;2.. Well Water Temp. (avg) I \~. bq Redox Potential (Eh)/ q, J Turbidity,--/ _) ,_, __ -' Weather Condo Ext'l Amb. Temp. O( (prior sampling event)_/ Y.......:.......D_-, Time I )~43 Conductance Temp.oC / Gal. Purged /'---'-', 6:.--_ ......... I ~bg7 1 1'3,'Q Redox Potential Eh (m V) 1 411 Turbidity (NTU) ItG Time Gal. Purged _I ___ ----' Conductance pH '--I ___ ....... Temp.oC Redox Potential Eh (m V) _I ___ ----' Turbidity (NTU) White Mesa Mill Field Data WorksheedorGroundwater Time Gal. Purged / _____ -' Conductance pH ........ 1 __ -----I Temp.oC Redox Potential Eh (m V) .... 1 ___ ---' Turbidity (NTU) Time Gal. Purged .... 1 ___ ---' Conductance pH ,--I ___ -' Temp.oC Redox Potential Eh (m V) 1 _____ -' Turbidity (NTU) 1 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I 1 b . 5 D Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I _...;....) J __ --I -gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I 2.'8~ I Number of casing volumes evacuated (if other than two) 1)·05 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labf,-..;;..;V...:..Y,.;..::I9~ ______ ....J Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Type Added y N specified below) y N Y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 100ml 0 IZi H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 NoPreserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) !J tsJ Sample volume 0 rl9 0 ~ L'h \ Or \'J,e. If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction ,--________ ..... 1 Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r O~:~~~Jj~ ~ I ATTACHMENT 1 Attachment 1 WHITE MESA URANIUM MILL L._~.M!'~_~~ __ 4.~_~~J FIELD DATA WORKSHEET FOR GROUND WATER btl] See instruction Description of Sampling Event: I ' ~-r ~o..rW N ,=Ff"o-.fG ~o~~ Location (well name): .... I -ri_W~;J_ ... _l_1 _________ ..... Sampler Name and initials: 1 :::Y:I'\I\~' 1J6J11~~/1"'J Date and Time for PUrginm \-lO-;2.01-:l.,. and Sampling (if different) &.-1 N......;;,;....;.~~ _____ -....I Well Purging Equip Used: IT!Jpump o@ bailer Well Pump (if other than Bennet) 1 &(1At'lJ.ro~ Sampling Event I ~+.er~ .N'+r~-t<. l -rvJN-Db Prevo Well Sampled in Sampling Event &.-_______ -....1 pH Buffer 7.0 &.-1 --"7:..-• ..:;;..0 ___ ....1 pH Buffer 4.0 Specific Conductance .... 1 _~_'f_q ___ -'I !lMHOS/ cm Well Depth(O.Olft): 1 't;2.00 Depth to Water Before Purgin~ -r D .1>0 4" well:1 ~.(,.82. 1(·653h) 3" Well: D (.367h) L--~ __ ....I Casing Volume (V) Conductance (avg) 2.f,5~ pH of Water (avg) b·S~ Well Water Temp. (avg) 1 t~.45 Redox Potential (Eh) ,,-I -=3~O;......;/~_....I TurbiditYL-1 ~_,1 __ ....1 Weather Condo Time "-11_0_0_0 __ --1 Gal. Purged 11.--'_7 __ --1 Conductance Temp.oC 1 2~bS 1 13·~1 Redox Potential Eh (mV) 1 30'1 Turbidity (NTU) 1 2..1 pH I G:,.S~ Time 1 1 0 o~ Gal. Purged ,,-I _1 ...... q~_---' Conductance 2.bS 0 pH I b .53 Temp.oC Redox Potential Eh (m V) 1 ~OD Turbidity (NTU) 1 2.. J White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)IL--0_b_....I Time )001 Gal. Purged &.-1 &_g __ ---I Conductance Temp.oC I :;lb53 1 13·1..\1 Redox Potential Eh (m V) I '30~ Turbidity (NTU) 1 Q./ pH I b.5.3 Time 11DD:) Gal. Purged 1t.....:}~}D~_---I Conductance I :2.&SO pH 1 b .5:5 Temp.oC I 13.Y\ Redox Potential Eh (m V) ,,-I _:1.._'1.;..,;;&;.....-._....1 Turbidity (NTU) 2.1 .' 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I L... ----I}_1_D ___ ...... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I ,A,J I \' T = 2V /Q = I ~,6J I Number of casing volumes evacuated (if other than two) I c> If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L..~........;..1...;..A _______ ....I Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as y N specified below) y VOCs 0 0 3x40 ml 0 Nutrients Eil1 0 100ml 0 Heavy Metals 0 0 250ml 0 All Other Non Radiologics 0 0 250ml 0 Gross Alpha 0 0 1,000 ml 0 Other (specify) ~ 0 Sample volume 0 Ch\O(;J( Comment A rr; \Jed 0 n .oS.+ e"d-' D'l'l "l . "G""..,... ~"r.I v",rr i" p"~(!4 ..fOr p ""('~"C kj"-" o..t ~53, f\,.~~<,a I..)e\l -tor a.. to-l-",' o*' \0 ? '""(~~ cf\c'-G~ 0..1'\0. h~Mp}~ ~-Gr~ LoH-c(.,+e~ ~+ lO()~ L c.f\-~ltt: ~t )001 L....-________ ...... 1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Grounawater Added N Type y 0 HCL 0 r&I H2SO4 ~ 0 HN03 0 0 No Preserv. 0 0 HN03 0 ~ 0 If preservative is used, specify Type and Quantity of Preservati ve: ~ See instruction p<Af{jG "I.n.l .s.D.""?!!:] <:lJe4 M ;t'")I.A.1-es, w~+"cf' W~ c1<..o..r. N 0 0 0 0 0 ~ DG?ft;, -t~ LV~+Gr W~ q~ .-:Sl 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ,-... __ ...................... --.. -.... -.. -.. -_ .. -.... _-, ATTACHMENT 1 rE'tlf3E~ FIELD DA~~~:i~:E~~I~~R~~:;D WATER Attachment 1 ~~ See instruction Description of Sampling Event: 1 \ ~T Q v..o..rf;;".-;V i+.,.. o...te, ~o I'd... Location (well name):I ..... T_W_AJ_--:.,~~ _______ ----I Sampler Name and initials: I -tD-YlY\ e., Ho)J(J ~(1 /'Itt Date and Time for Purgind \ -, 0 .... .2..0 I?. and Sampling (if different) "vIA L--______________ ~ Well Purging Equip Used: IT!Jpump o@ bailer Well Pump (if other than Bennet) Prev. Well Sampled in Sampling Event I Tv...) AJ -1:;t. R. pH Buffer 7.0 7.0 pH Buffer 4.0 ti.O Specific ConductancelL--Q...;...9.:..,..'\I....-__ ---I1 ~MHOS/ cm Well Depth(O.Olft): 1 1) o.ot> Depth to Water Before Purgingf ?-.q, ,~ Casing Volume (V) 4" well:i E~. ~\ i(·653h) 3" Well: '() (.367h) I...-..,..;~-----' Conductance (avg) pH of Water (avg) I,,--b_, q_8 _____ ----I Well Water Temp. (avg) I '3~ ~E; Weather Condo I ?",A"tj '::"OIA.~'d Redox Potential (Eh)1 ~"5 Turbidity ..... 1 _15_' _----I Ext'l Amb. Temp. O( (prior sampling event)I .... \...) b Time 07'38 Gal. Purged 1~8_g __ --II Time 1 D734 Gal. Purged 1 ..... ".:.....1'11-.-_----' Conductance pH I Co.qg Conductance 1 ,;4.:1 ~ pH I b·/-lCf Temp.oC Temp.oC Redox Potential Eh (m V) I 7J...7d-.. Redox Potential Eh (m V) I ';4b' Turbidity (NTU) Turbidity (NTU) Time I {) /YO Gal. Purged L...l1 1~) O¥--_----' Time a.....;1 0;;,-.7_4:...:,.}_----' Gal. Purged L...:.11....;:Q.u...1 __ --' Conductance Conductance 1;2..l.\ bY, Temp.oC Temp. °C I 1;' 357 Redox Potential Eh (m V) ..... 1 _%----:.~_----' Redox Potential Eh (mV) ..... 1 ';"'~~~_----' Turbidity (NTU) Turbidity (NTU) 1'153 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged &...1 _1 :l._1 ___ --.I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1 ...... _1_1 __ -----' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I Z\~~D I Number of casing volumes evacuated (if other than two) I N/A If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labf .... _;fV_I"A _______ ---I Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 'E:1 0 Sample volume 0 ~ 0 G hlor,cl'( If preservative is used, specify Type and Quantity of Preservati ve: See instruction Comment Arr .. i"GJ. on f. itc I>v"t 07:2..5. 1"'1'\11 Gr 0lI'l,)., (;.UI,-r-r:YJ P f"'eS-en t -r. r }>\)I '(j ~ "\n"'-.1:."-"'1 f J ''yj 6v6rrr.. PUf'~~ b e.a. ~h ~-t' 0'1 ~t> ~ Pv.;Dl.e..£\ v:k::J\' ..rot' 6... .} '-\ (' '\ " ..l.... <.J ~ "-l O'T(M 6-t-I ~1(\v.."'C~. \))~Ie(' \J~.s "'-1\ or-o.n~G Go\or .. ~.. ",ot\u-~'()~~ G\av-e~ ~~roud'0VvY ,?w-~~ b",,~ 1'I(.Vif -1--o+-"1 ~ C-),:/I"ca)., ?\J..('~c.. C:r'ld.<A. MA ..5t;,,1VI p ~ vJ-e-re Lo\l.::cteJ. 074 L DepTh ftl w,.%,- 'vVo-b ) () \. 3' . L-e..+1-~ rt~ ~ ('-7 "1l.\ L....-________ ..... 1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) c·_·-······_·····-······_·················· __ ·_·····_·_ .. _ .. _··_····_-1 ,[I OENISONI)~ ~J' ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 [6£1 See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER _._,~ ......... ,.....o.;..._.........,:._ Description of Sampling Event: I '~'" Q~t).r+er-)\) ltf"t'l.te ~o 1 ~ Location (well name):IL-T_vJ_N_-_\.;...;.~--.:..R..:..-______ ~ Sampler Name and initials: Date and Time for PurgingJ 1 -\ 0 -'J-D' :l.. and Sampling (if different) &....;../'J.~Y...;..,jAi--_____ --I Well Purging Equip Used: [![]pump o@ bailer pH Buffer 7.0 7.0 Specific Conductance L...1 _Ci_q;...;q~ __ ...... 1 ~MHOS/ cm Depth to Water Before PurgingJ .... __ 6 __ ...... Conductance (avg) Well Pump (if other than Bennet) 1 &r(}.'11 ~fD.s Prev. Well Sampled in Sampling Event l,w,tV-0'1 pH Buffer 4.0 '-).0 Well Depth(O.Olft): b Casing Volume (V) pH of Water (avg) 4" well:~_O __ --1I (.653h) 3" Well:. a . (.367h) s.og Well Water Temp. (avg) 1 q,;lS Redox Potential (Eh) 1 '--\t1b TurbiditYL-1 _0 __ ----1 Weather Condo Time I 071~ Conductance Temp.oC 1 131qb 1 qt:AS Gal. Purged 1,---' 8;.....b __ ...... pH I S.Og Redox Potential Eh (m V) 1,"--l1_Y_G __ ......I Turbidity (NTU) o Time Gal. Purged .... 1 ___ -......I Conductance pH ..... I ___ ...... Temp.oC Redox Potential Eh (m V) .... 1 ___ -......I Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)l-b 0 Time Gal. Purged L...1 ___ ----I Conductance pH ,--I __ ----' Temp.oC Redox Potential Eh (m V) 1'"--___ ...... Turbidity (NTU) Time Gal. Purged 1'"--___ -' Conductance pH L-1 ___ ...... Temp.oC Redox Potential Eh (mV) L...1 ___ -......I Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 11-._~_o_O ___ -oI gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = L-I _,\ ___ -.J T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Lab~L-_;J,_V_A _______ ...... Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients m 0 100ml 0 ~ H2SO4 gj Heavy Metals 0 0 250ml 0 0 RN03 0 All Other Non Radiologics 0 0 250ml 0 0 NoPreserv. 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 Other (specify) ~ 0 Sample volume 0 m 0 Ch ) ()r~cle. If preservative is used, specify Type and Quantity of Preservative: Comment ~. See instruction Arf\\1ea on ~l+e. ~t ObS\. ~Y\ner o..flJ &()..rrl't1 'Fre~~nt hr f"1'n.$o-.,TG. RI·nSo..tc ~+o..('+e~ 0...+ O&5~. 'Pv..rvlpecl So &()Jll)n~ or Ac\'d tNCAter, so G-fA.J101'1j of' Soo..p ~te(J o.(\J. 100 &CT..lI()n~ o.f' DI vJ~+er. R;.,.s",+e etlJeJ o..Ylc,/ SC\Mfl~ w(:,f-ei GDlle,c+~~ ~1-071S" Le.++ ~I+e. ~t 0717 P ~ W()..S 0-.. ,;\·H-c. LoY:). L""b ~s 6h"~;~ OlA.1-\JI F;H"els~ 1...-________ ...... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 k<~~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 \ ~T Q"'t)..("te(' N 1~,~tG .2..0 1~ Location (well name ):I-I-r_W_N_-_l_0 ________ --I Sampler Name and initials: 1 ~Yll'lG'" 1=1'6\ l,'J4~/""l+ Date and Time for Purgind ,-4 -~C>1", and Sampling (if different) a.....1 .;....,tJ~/_A ______ --' Well Purging Equip Used: [QJpump o r@] bailer Well Pump (if other than Bennet) Prev. Well Sampled in Sampling Event I1\.VN -08 pH Buffer 7.0 pH Buffer 4.0 y.u Specific Conductance L-l...;.q...;.q ..:l..~ ___ ____II !lMHOS/ cm Well Depth(O.Olft): 1 \?..O.OD Depth to Water Before Purgind L\ b~~b Casing Volume (V) 4" well:1 4 g.1j I (.653h) 3" Well: b (.367h) 1....-___ --' Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 1 \4 .'-l'i Redox Potential (Eh)a.....1_2_1_' __ --' Turbidity ..... 1 _5_8 __ --, Weather Condo Time Gal. Purged 1.........,;.,77"';"-'_--1 l?.C>t; Conductance Il-l..;....~_1_1 __ ..... Temp.oC IlY.U Redox Potential Eh (mV) 1-1 _~..;....1 ..;;;.g __ ..... Turbidity (NTU) 1 S fa Time I l~O<" Gal. Purged ..... 1 ....l...~j"'--_----I Conductance 1 \:2.~3 pH 17.bS Temp.oC 1 lq·':5~ Redox Potential Eh (m V) 1 ~o z Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)Ia.....3_o _--, Time Gal. Purged 1"'--88 __ ---' Conductance pH 1 7.t,~ Temp.oC Redox Potential Eh (mV) L-I _::1._1_3 __ ..... 1 Turbidity (NTU) Time ~h~~=..L1 __ ....... Conductance 1 \~3D Temp.oC I 57 I Gal. Purged a....;ll~l ..;;..b __ ....... pH 17 . .({ Redox Potential Eh (mV) 1 ~~7 Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I ..... _\...;..;1 o~ __ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= L-I _1.;.......;..1 __ --1 Time to evacuate two casing volumes (2V) T=2V/Q= 18:7' I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated rI/A Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... ;V._Y,_'P., _______ --I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients IE 0 100ml 0 ~ H2SO4 l5J 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) lEI 0 Sample volume 0 ~ 0 !E Gh \Dr~ ~6 If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction 1....-________ -oIIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater "2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 Attachment 1 b~ See instruction WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUND WATER Location (well name ):I,"-~ ___ -fi_VJ_tJ_-_14 _____ ---, Sampler Name and initials: fGJ111er +l~ H ,;.l4.cj.!rH "TWA) -14 Date and Time for Purgingj t -10 ... ;2.o~:;;l. and Sampling (if different) 1 1-11..;;)..61~ Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) 1 G(,W4A~s I -rwAJ -).(, Prev. Well Sampled in Sampling Event '"-_______ ----" pH Buffer 7.0 pH Buffer 4.0 Specific Conductance I .... _~~~,--q ___ ...... I!lMHOS/ cm Well Depth(O.Olft): 115"C>.oc> Depth to Water Before Purgind b~ .2>S 4" well:1 Yb.7g I (.653h) 3" Well: D (.367h) L..-___ --' Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 1 JL.j. J~ Redox Potential (Eh) 1 3J~ TurbiditylL.--5 _' ._J _---' Weather Condo Time I \ 32-:J Conductance Temp.oC 1 \ L\, ''6 Gal. Purged ..... 1 y-'-y+--_---I pH 17.51 Redox Potential Eh (mV) I ~lS Turbidity (NTU) 1 :s~.l Time Gal. Purged &....1 ___ ----" Conductance pH .... I ___ ...... Temp.oC Redox Potential Eh (m V)I I-___ --.....I Turbidity (NTU) White Mesa Mill "Field Data Worksheet for Groundwater Ext'l Amb. Temp. °C (prior sampling event) &....1 Ll_tJ_---' Time Gal. Purged .... 1 ___ ...... Conductance pH ..... 1 __ ----I Temp.oC Redox Potential Eh (m V) &....1 ___ ----" Turbidity (NTU) Time Gal. Purged &....1 ___ ---' Conductance pH 1 .... ___ --, Temp.oC Redox Potential Eh (m V) 1-1 ___ --.....I Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 _11.....;'1~ ___ ....... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I \I T=2V/Q= I g,50 I Number of casing volumes evacuated (if other than two) I . 14 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~I-_~_I_A _______ ..... Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 RN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 Other (specify) ~ 0 Sample volume 0 [2] 0 0hlDridc If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction A ,1" i \leJ Of\ ~rt" ",-r 1:3;1.}, ~ nn"r "'" J G-... ,(" In pr es",nt..[61 pw <'l~' p", r c ~j"" ... t 13 :;!.;~ ? "d' j d v)e)\ .for .... -1-o+..J of" '1 \'V1 ;fl~ 0::>. P "'( tl eA ~., 11 d,. ~. vJ /1..1-c~ h .. 'IS fA. S l.~ l\:I- ai~uD)()(". Pv..(~-<:. ~YlJ~J, At l3;A1 Le-'t s)'.}~ ~'t l'31>D Arr,veJ on ~;tc 0\+ O'f50. "-lA"n~ ""nt! (J-o.r'r,''1 Fesen+ }o C6/}'(!d-SctfJl]p/t:.S . Weprh to \,;)~ ~o..s. b'3. bO. ~~""f'\a. v.:>ere-bO\.ile4 ~+ 0 '15 5. LJ1-~/tG ~i-oq57 L--. ________ ..... 1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 af2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r .. ···_··········_ .... ··· .............. -'·""·1 ATTACHMENT 1 i Il)j j I WHITE MESA URANIUM MILL l.~~_~~~~~ ___ ~_ FIELD DATA WORKSHEET FOR GROUND WATER Attachment 1 L~ See instruction Description of Sampling Event: I \ $T Q"'-O..("ler AJ I·+ro..+~ ~o I~ Sampler Name Location (well name):L..I-r_w...;.]J_-_~ _________ ....... and initials: I ~t'\ner W b 1 bJAej /T1t Date and Time for Purginm '~1 0 ~ ~ 0 1~ Well Purging Equip Used: [1!J pump o@ bailer pH Buffer 7.0 1.0 Specific ConductanceL..I_'1_1_1 ___ ....... I ~MHOS/ cm Depth to Water Before Purgind 41.7 g Conductance (avg) 1,-\0) and Sampling (if different) I '-1\ -;2. 0 1~ Well Pump (if other than Bennet) I frrlAfl d+'o..s Prevo Well Sampled in Sampling Event 1 -1 vJAl-l~ pH Buffer 4.0 Well Depth(O.Olft): I '55. O£) Casing Volume (V) pH of Water (avg) 4" well:1 '1D_"-9-IC.653h) 3" Well:. b . (.367h) Well Water Temp. (avg) I \4-bY Redox Potential (Eh) r...:;;10;.....0~b_-......I TurbiditY,--1 ~_3_._\_-......I Weather Condo 1 ? u..A-\ il L. \ 0 V.a~ Ext'l Amb. Temp. °C (prior sampling event)I -3~ Time I 08:2.1$ Gal. Purged I 'i ~ Time Gal. Purged I Conductance 11YD) pH I bJ7.b Conductance pH I Temp.oC I IQ .oq Temp.oC Redox Potential Eh (mV) I 37" Redox Potential Eh (m V) I Turbidity (NTU) I ~'3..1 Turbidity (NTU) Time Gal. Purged I Time Gal. Purged I ] Conductance pH I Conductance pH I Temp.oC Temp.oC Redox Potential Eh (mV) I Redox Potential Eh (mV) I Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field'nata Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I .... _L\...:..g~ ___ ...... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I ' I T=2V/Q=1 7.3~ I Number of casing volumes evacuated (if other than two) I Llg) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L....rI_,/_A ______ .--I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients 1!1 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 ~ 0 Gh\oc~dc If preservati ve is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction A-'(r;~e~ 0(\ s.'ite .... + 0 &:;1.0. -'1"",1\6(' cknJ G-... r~i" rr~e"t +" r",rl\~ -r-.)J\l-IS. 'Pu.r(l<-h"j"" 0..1-C~.2..~. p""rp.-ea ~-6l\ .ror IA.. }o-\-t1..\ t:S' ~ yV\11(}",,+~.s '6 ;2..0 $ -' ,. I \ cr \..) d~l>n~. 'Pv.t"'~d we,) dlr~ .. \".)~ e( \...)~ rtll)..~~~ PW~G O'I~eJ. ~T 68:lfr Le.fi-' sr-tc. 0..+ Og~4. A(1"~\lea on f,itt! ""t 0430~ ~1\nc( O\f\Cl &0"(11(\ ?(C$cnt +0 Go1\ec-t .s~lV)p/-eS. D e.p -1-\, +0 \i)o,.+u" 1Nu..s '1~.Oo. SIl,rV\ p Ie::. ~erG b",nd ",:t oq~4 1--e..f't ~)tc. tA.t oQ3S . L....-_______ ---I1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet fo(GroundiNater N 0 0 0 0 0 ~ 2 of 2 .. Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 1-·-·-·-·······.--·:--·-·.-···.·· .... ····. -----···-···1 I OENISOJ)~J ! WHITE MESA URANIUM MILL Attachment 1 ~~ See instruction L-MIN'!~" __ ~ ___ .~=_J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 1~'" QV\.~r+~t'" AJ ,·h,-¢+e. 201~ Location (well name):L...I _-r=--W~N_----=--}b _________ .... Sampler Name and initials: 1 ~f\ne[ Ro/J,'d~/71t Date and Time for Purginm 1-10 -~(') IQ and Sampling (if different) 1 .... N_/A ______ ---' Well Purging Equip Used:OOpump o@ bailer pH Buffer 7.0 L-1--.-.;../.:...;,o~ __ .....1 Specific Conductance .... l.....;q'--"q ..... 1 ___ ---'I ~MHOS/ cm Depth to Water Before Purgind 4~. Sb Conductance (avg) Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event I-r-WAl -07 pH Buffer 4.0 Y.O Well Depth(O.Olft): 1 10().oc Casing Volume (V) pH of Water (avg) 4" well:i 33.'~ i(·653h) 3" Well: 6 (.367h) '----_ ...... Well Water Temp. (avg) 1 lY.7'i Redox Potential (Eh) 1 ..... .-;,3_o_\ _-.....I Turbidity 1 l~" 6 Weather Condo l_~ __ ~ __ ' __ --'dJ ____ .....I _ f"" Ni1t Clov.,a~ Ext'l Amb. Temp. DC (prior sampling event) 1-1 3_°_ ...... Time '--\~_'1_3_-----'1 Gal. Purged L-I _y_'-l __ --' Conductance Temp.oC Redox Potential Eh (m V) 1 ~3'"5 Turbidity (NTU) }?.. \ Time 1-1'_;).._4_5 __ ...... Gal. Purged I ..... _b;,-.b __ --' Conductance 17b5 Temp.oC Redox Potential Eh (m V) I 1;7::15 Turbidity (NTU) 1 1,.. \ White Mesa Mill Field Data Worksheet for Groundwater Time Gal. Purged ..... 1 5_5 __ -.....1 Conductance Temp.oC I 14. 74 Redox Potential Eh (mV) 1 '333 Turbidity (NTU) Time 1 1 ~ '"\ '=- Conductance Temp.oC 1 I 7~l:J 1:2:·0 Gal. Purged .... I'..:.,.7..L.-__ -' pH I '·87 Redox Potential Eh (mV) I "33 0 ~ Turbidity (NTU) 1:2... ) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged &...1 _7_1 ___ _____ Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1'---_1_\ __ .....J gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 b.1 1 I Number of casing volumes evacuated (if other than two) C> If well evacuated to dryness, number of gallons evacuated D Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... /\J_~_~ _______ ....I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients ~ 0 100ml Heavy Metals 0 0 250ml All Other Non Radiologics 0 0 250ml Gross Alpha 0 0 1,000 ml Other (specify) ~ 0 Sample volume G\1 lorld( Comment Y N 0 0 0 ~ 0 0 0 0 0 0 0 ~ Added Type y HCL 0 H2SO4 ~ HN03 0 No Preserv. 0 HN03 0 0 If preservative is used, specify Type and Quantity of Preservative: I:'l See instruction ~ A(,(";\Je.~ O}"l srt-e td' l~".--r~n(Jer 0\.rlJ. G-~('r;n f>~.setrt +6,-f\'\"'J-e cf\."c,\ SC\)'YIr1i17<) e\Je,,+, 'F' v.r 6~ b"'j""..r \:),'3'1. "f' ",,..tl~ '" ell ~,... "" + at ",I ~f' 7 M i"..r..,.s. · w ... +er w'l.S "".0 f,1-1 G let>,.(". ? u. r~& entleJ. Nl J. .$t4Mples u)ere. Go ))","~4 "I.t 12.'1 b . 0 c=p-tt.. +0 lA'J.d-er 2~ Y '1. 55 Le~ ~rtc ~ ,~50 ___________ ....JIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r---............... _ .. __ ... _. __ ._... ..-.-_ .. _.-_.. --I IOENISOJ)JJi ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 b~ See instruction : .. __ ._~I~!~_~~. ____ J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I l~T Qv...o.~te.r A.);1-rd'-ofe. ~o'J... Sampler Name Location (well name ): ..... 1 _T_w_}J_~_1_7 ________ ---I and initials: 14'"""1\"(\-(,(' BollI aA~ /71t Date and Time for PurgingJ'---l-_l_l-_:).._o_,;t ____ ---" Well Purging Equip Used: []!] pump o@ bailer Sampling Event 1 Q\A.CA.r+e4""(;1 .N l~rt~ ... t<: pH Buffer 7.0 Specific Conductance ..... 1 _q;....q_~ ___ ----II ~MHOS/ cm Depth to Water Before Purgind ;:, 4. L\ '0 Conductance (avg) ll~7 and Sampling (if different) 1 \-'~-').o\6 Well Pump (if other than Bennet) Prev. Well Sampled in Sampling Event Ilw.N-n R pH Buffer 4.0 '1.0 Well Depth(O.Olft): 1 no.oo Casing Volume (V) pH of Water (avg) 4" well:1 q 'I. 3b 1(·653h) 3" Well: l) (.367h) '------_ ....... 7.17 Well Water Temp. (avg) 1 IL\ .OJ Redox Potential (Eh) ..... 1 _32_7 __ --' TurbiditYL-1 7_~_._1 _----, Weather Condo ..... 1_G_'_e_O"'_I ________ ----' Time 1 O,~S Conductance Temp.oC lJ~7 119· C) 1 Gal. Purged IL..:S::;....0~_----' pH I 7,)7 Redox Potential Eh (mV) ..... 1 ~ __ J __ ....... Turbidity (NTU) 1 7~,J Time Gal. Purged 1.-1 ___ ---" Conductance pH ~I ___ ....... Temp.oC Redox Potential Eh (m V) 1.-1 ___ ----I Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)1 -lb Time Gal. Purged ..... 1 ___ ----' Conductance Temp.oC Redox Potential Eh (m V) ..... 1 ___ ---' Turbidity (NTU) Time Gal. Purged ..... 1 ___ ----I Conductance pH L-I ___ --' Temp.oC Redox Potential Eh (mV) 1.-1 ___ ---' Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged 1-1 _5_3 ____ ...... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I n T = 2V/Q = I g,q, I Number of casing volumes evacuated (if other than two) 11.0"1 If well evacuated to dryness, number of gallons evacuated 150 Name of Certified Analytical Laboratory if Other Than Energy Labfl-A_I A _______ ---I Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 rnl 0 0 HCL 0 0 Nutrients ~ 0 100 rnl 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250 rnl 0 0 HN03 0 0 All Other Non Radiologics 0 0 250 rnl 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 rnl 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 ~ 0 ~ Gh lor~J< If preservative is used, specify Type and Quantity of Preservative: See instruction Comment L...-________ .....J1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r ---------------------------------1 ATTACHMENT 1 I_ OENMI_IS_NOEN~~~, ~ ,I' WHITE MESA URANIUM MILL Attachment 1 6<:_..1 See instruction I_.--J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 11 ~1' Q",,~{"fe"" -",.'+ro...fe. ~o l~ Location (well name): .... 1 ~_'vJ_JJ_-_l_7_R..~ _______ ---I Sampler Name and initials: 1 ~J'\ne( Hldl/J.D.~J-rH Date and Time for Purgind ~J 11 /:;LO 1~ and Sampling (if different) .... 1 _N_/,4 ______ ---1 Well Purging Equip Used:~pump or@] bailer Sampling Event I Q"'~r+er~ /\J:·'fro..f< pH Buffer 7.0 7.0 ] Specific Conductance .... 1 _t1_~_i ___ ...... 1 ~MHOS/ cm Depth to Water Before Purgin~ .... _O ___ ...... Conductance (avg) Well Pump (if other than Bennet) . . l-rwtJ-\'f Prevo Well Sampled III Sampl~ng Event .... _______ ---1 pH Buffer 4.0 Y.O J Well Depth(O.Olft): .... 1 _0 ___ -.1 Casing Volume (V) pH of Water (avg) 4" well:~_O~_--II (.653h) 3" Well:. {) . (.367h) 7."3.D Well Water Temp. (avg) I,.s';)... Redox Potential (Eh)1 '5 \~ Turbidity .... 1 _0 ___ .....1 Weather Condo I? u-r\-}j c.1 ov..J ~ Ext'l Amb. Temp. °C (prior sampling event)I .... -_l_B_.....I Time I o/og Gal. Purged ..... 1 ...;...;\ 8;...-D __ .....I Time Gal. Purged IL--___ ...... Conductance D pH 17.30 Conductance pH L...I __ --' Temp.oC 7.D~ Temp.oC Redox Potential Eh (m V) 1 "> 13 Redox Potential Eh (mV) .... 1 ___ ----" Turbidity (NTU) Turbidity (NTU) Time Gal. Purged .... 1 ___ -.....I Time Gal. Purged .... 1 ___ ---I Conductance pH 1 ..... ___ ...... Conductance pH ..... I ___ .....I Temp.oC Temp.oC Redox Potential Eh (mV) .... 1 ___ -.....I Redox Potential Eh (m V) IL--___ ..... Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 _~_O_D ___ ........ Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = &.-1 _'_1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 I Number of casing volumes evacuated (if other than two) /) '----_ ........ If well evacuated to dryness, number of gallons evacuated ..... [1_0 ___ ........ Name of Certified Analytical Laboratory if Other Than Energy Labl ..... _;J_I._~ _______ ....I Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) tl 0 Sample volume 0 ~ 0 c>h \ b(,~ Je If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A('('~ve.lJ, on s,tt:: ObYS.~n1\e. M~ (r""n''';t\ pre$e(l1--f;r ("~n~+e. Rins.od"'e. ,b~v." ~ 0650 P\A.('~eo.· SO &O\l\o~ of A£.l·~ WCAtl!'I", 50 &",Jlo t1j 6f'6o~f ~Q.,t-er\ 100 &~)Ion~ o.r OJ: tA'>a.1er. R;r'I~~1<= en~ea O\.(\d ~~Mpl(;s Wet'(: GoJleG+~~ ~+ 6Jl()~ L-e..fT ~l'tC, ~t o11;J,. '--________ .... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 I1r . 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) " OENISO'Nl)j J r····_····· __ ····_·············_-_· ............. -.-.~.---.... _.-ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 b~ See instruction ,MINES FIELD DATA WORKSHEET FOR GROUND WATER l-..-.....~ ............ ~ __ _ Description of Sampling Event: 11 S'1' (;)",o..rt-ef /\J :t1"lA.+~ ;2..01~ Location (well name):L-1 _i_W_N_-_)g ________ ---' Sampler Name and initials: 1 -r6.nr'\~r'" Hc}lh'J~~ht3 Date and Time for PurgingJ ) -10 -2D \~ and Sampling (if different) L-I #_1_1-\ ______ ---' Well Purging Equip Used: [QJpump o@ bailer Well Pump (if other than Bennet) I -rWN-l1 Prevo Well Sampled in Sampling Event L-_______ ---' pH Buffer 7.0 7.0 pH Buffer 4.0 Specific ConductanceL-1 _q.;....q-'-j ___ ---'I ~MHOS/ cm Well Depth(O.Olft): 1 11.\5.00 Depth to Water Before Purgin~ 57. ~ L\ Casing Volume (V) 4" well:15 b.t.l) 1(.653h) 3" Well: 0 (.367h) "-------' Conductance (avg) L....-_2.;...1_I _b _____ ....... I ' pH of Water (avg) Well Water Temp. (avg) 11Y .11 Redox Potential (Eh) IL--~_I~.....:..-_ ....... Turbidity &....1 J_O_::3 __ ....... Weather Condo Time Gal. Purged &....1 ......;8;..-g __ ....... Conductance &....1 :2._\_b_~_---, Temp.oC 1 1'1. \1 Redox Potential Eh (mV) &....1 ...;;;?>...;.1q~_ ....... Turbidity (NTU) 100 Time &....I...:,.l b~E,;....;.1_---, Conductance 1 ~ 1 79 Temp.oC I 1 q. \ I Gal. Purged &....11.:...;.).;;,..0 __ ....... pH I 6.710 Redox Potential Eh (mV) 1 ~l~ Turbidity (NTU) 1100 White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. °C (prior sampling event) ..... l l_o_ ....... Time 1 &.... 1_b_5_o_---' Gal. Purged ..... 1 " ...... 1'--'_---' Conductance 1 ,;2..' 77 pH 1 b.7-.5 Temp.oC 11Q·17 Redox Potential Eh (mV) ..... 1 _3_r_3 _ ....... 1 Turbidity (NTU) Time 1 'On~ Conductance 1 ~J g;;C Temp.oC I lq·17 I lO~ I Gal. Purged ..... 1 )r.;..~...:...J __ ..... pH 1 b·7' Redox Potential Eh (mV) ..... 1 3_1al __ ...... Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 _1 ~_} ___ ----' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1,--_1...;..) __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 10.~4 1 Number of casing volumes evacuated (if other than two) L-I 0 ___ ----1 If well evacuated to dryness, number of gallons evacuated .... 1 b ___ ----' Name of Certified Analytical Laboratory if Other Than Energy Lab~L-_#_YA-_______ --I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients rn 0 100ml 0 ~ H2SO4 Ili Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 ~ 0 G1,1or,'de., If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Ard"Ga on Slt~ ""+ lO~~. \<>..nnG~ Q\"r'\o. G-~('ril'\ ?l"'-eSGrrt -Fo,.. pUT'~-e c:U\a So.Mpl~ -ev<'f)7. p v.r~-e beL,\"", ~t 10"'\1. ?~(~e.d. \Nel\ -to( fA. 1"0+0"\ or \\ yV'Iil1v-.tes, wo.1-er v.)~ ty)", r'k~j' ?v..r~-e..:. -e,'lde.c\. ~1'\~ ~""W\'p\~~ \...)Gre. t.olle..G+t::..~ 0..+ lbb~. D-e'f'th +c Wt),:Y--U- V:>~ b\.~O~ Le# Sl-t<.l ~+ ,OSb_ '--________ ...... IDo not touch this cell (SheetName) White Mesa Mill -Field Data Worksheet for Groundwater . N 0 0 0 0 0 ~ 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r-.-··.------.·-... -...... _ ...•......................... -. -.. , I OENISONr;)~~1 ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 b~ See instruction .......... M I ~ E~~ ___ ~~_._",--.J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I \ S1 Q",o..r+eT )\Jl:tr<ktc... ;1.0 I ~ Location (well name):,--I _-r:_...N_N_-_l~ ________ ---, Sampler Name and initials: Date and Time for Purginm ,-IO"';l..o IQ.. and Sampling (if different) Well Purging Equip Used: [![] pump or@] bailer Well Pump (if other than Bennet) =t'l1\.nnv H6 \!tJlI\~7;+l 1 /V/~ Sampling Event 1 Q\I\fA.r+Gf"'b .N ,:t(",,=t< I -rvJtJ ... lL) Prevo Well Sampled in Sampling Event ..... _______ ---' pH Buffer 7.0 I.b pH Buffer 4.0 Y.O Specific Conductance .... 1 _,,_~_1 ___ ----'I ~MHOS/ cm Well Depth(O.Olft): 1 \ 10. D'D Depth to Water Before Purgin~ s;2·S ~ 4" well:13 7. '-1q 1(.653h) 3" Well: 0 (.367h) 1-.-___ ..... Casing Volume (V) Conductance (avg) pH of Water (avg) ,.13 Well Water Temp. (avg) 114..50 Redox Potential (Eh)I ..... ~ __ f... __ ..... Turbidityl ..... ~_7 __ --' Weather Condo Time IL...-l"_l~~_ ...... Gal. Purged ..... 1 ......;'1_t1 __ ...... Conductance pH 1 7.1"3> Temp.oC Redox Potential Eh (mV) I ~~g Turbidity (NTU) Time ...... 1 }-.....z4...,;..;1 8I0Il:..-_ ...... Conductance \~70 Temp.oC I Ab·1 Gal. Purged ..... 1 ...::b~b:"'-_---I pH I /·JY Redox Potential Eh (m V) I ~ Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. °C (prior sampling event) .... 1 4_6 _ ..... Time ..... 11:....1..);....17 __ -" Gal. Purged ..... 1 S_6~_--, Conductance pH 1 /.13 Temp.oC Redox Potential Eh (m V) I ..... -:s=~~b __ ..... Turbidity (NTU) Time L..L11......;'-\:..;..1~~_ ...... Conductance Temp.oC Gal. Purged 1L.,..7:....J1L--_--' pH 17·J3 Redox Potential Eh (m V) ..... 13_?...;:~=-_---' Turbidity (NTU) 1 of 2 . Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 __ 7...;..--:.7 __ _____ gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1 \ \ T = 2V/Q = 1 b.81 I Number of casing volumes evacuated (if other than two) L..1 _0 ___ ......1 If well evacuated to dryness, number of gallons evacuated _ ..... 1 _0 ___ -"' N arne of Certified Analytical Laboratory if Other Than Energy Lab~ ..... ....;.tV-..;...1 f}. _______ ......1 Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Type Added y N specified below) Y N y VOCs D D 3x40 mI D D HCL D Nutrients E D 100mI D if] H2SO4 ~ Heavy Metals D D 250mI D D HN03 D All Other Non Radiologics D D 250mI D D -No Preserv. D Gross Alpha D D 1,000 mI D D HN03 D Other (specify) ~ D Sample volume D ~ D L..\"lor;Je If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A ( r \\le.a on ~;1-G 0..+ 1'"\ 0'\. -r: tlI'\O' ..... n t1 G-... u; 1\ p< esen-1-..f'or fU.£ ~<. "''' a. ~o.N\flj ~"en1. H ... ~e. b~"", d\.4 IY l~. p",~~ w .. 11 ~r' '" -h'+",1 0.[' 7 ,....,;n",+c.s.. o-.Hc( 5 ..-.\." ",t~~ i-h" \':)d/ S-t",rtd -tt> ~r",+Ter b""t 1<er-1 \A p ~r' -h:.11 7 "";'-.4.+"..5-~A.1er Wo.s " 1;-N1c WI", ... ~. D-cptJ.., tb wo-.·1e.r wo"s. 101.10 ?w~e. -GYl~-6~ ~y\~ f9.mplc Leo+! 5J·t~ ~t \'1~~. ~!.((J LO))~Gt~~ ~-f 1'-\ lQ. L...-________ ......IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D ~ 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) 1--. _ .. _ .. __ .-_._.-.. __ .. ----....... --. I, OENISONl)j~ ATTACHMENT 1 Attachment 1 . bt'~ See instruction WHITE MESA URANIUM MILL L-..--~J..NE~ __ ~ FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 ,~,. Qv..o..r~ef"" ,N,'tr()\.tc. ~Ol~ Location (well name): .... I_-r_'vJ_Al_-_b_6 ________ ---' Sampler Name and initials: I -("Ar'\l1~r l1c) 11 ,'J A:Q /I'J+ Date and Time for Purgind ..... '....;./_'_'"'-I 'J._C....;.\ l.~ ___ ---, and Sampling (if different) AJ/It L..-~~ _______ ~ Well Purging Equip Used: [gJ pump o@ bailer pH Buffer 7.0 /. () Specific Conductance ..... 1 _9_~.....;~=--__ ----II ~MHOS/ cm Depth to Water Before Purgin~ ..... _O __ ----' Conductance (avg) O.S Well Pump (if other than Bennet) .... 1 M_~~4 ________ ....... Prey . Well Sampled in Sampling Event I .... _p_;_~_-z.._-_()_l ________ ---I pH Buffer 4.0 Well Depth(O.Olft): ..... 1 _0 ____ ---1 Casing Volume (V) pH of Water (avg) 4" well:~_o __ --iI(.653h) 3" Well:. b . (.367h) 71'37 Well Water Temp. (avg) 1 '~·:2..4 Redox Potential (Eh) 1i-~_7_8 __ ----I Turbidity .... 1 _0 ___ ...... Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 ~1° Time 1.-11;...;;;;'1>...::..,) lJ....L.-_ ...... Gal. Purged i-I 0 ___ ----' Time Gal. Purged 1.-1 ___ ...... Conductance Conductance pH L....1 -----' Temp.oC \'3. !:l9 Temp.oC Redox Potential Eh (mV) 1 ?.7 g Redox Potential Eh (m V) 110-..-___ ...... Turbidity (NTU) Turbidity (NTU) Time Gal. Purged 110-..-___ ..... Time Gal. Purged 11.--___ ...... Conductance pH IL....-__ ----I Conductance pH I.-I ___ ....... Temp.oC Temp.oC Redox Potential Eh (m V) .... 1 ___ ---' Redox Potential Eh (m V) .... 1 ___ ----' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Gr6undwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..1 __ "C> ___ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I c> T=2V/Q= I 6 I Number of casing volumes evacuated (if other than two) 0 1...-___ ...... If well evacuated to dryness, number of gallons evacuated I L... b ___ --' Name of Certified Analytical Laboratory if Other Than Energy Lab~L..._,Al._~_A _______ -J Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100ml D ~ H2SO4 ~ D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) lE D Sample volume D ~ D ~ L-h'D\,de, If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A(r'i ve4 \1'\ Lo-b ",1-\'30 g. Io.nn"," lio ))"J:J pr-e..sent 1<> 6>1 Jed "- So...rY\f>1~ w-c:.n: ~on~d-d 6-.-Y )'31S_ Le,.f1-L~b c:A..+ l~ 17. Dr L...-________ -.l1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r--··-·-·-~--.... -.... --.~.----.. :---··-1 ~E~s~l~~~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 b~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 1 ~-r Qv..CN""t~,... "AJ:i-ro,.'+-e. ::z..Ol'.:.\. Location (well name ):L-I"i'_W_N_-_b_.5 ________ ---1 Sampler Name and initials: I-;;"nne.r J..1011''cl~~.frH Date and Time for PurgingJ ..... l_-_q_-_~_O_l ~ ____ ----' and Sampling (if different) 1 , -I 0-~Ol~ Well Purging Equip Used:OOpump o r@] bailer Well Pump (if other than Bennet) Prev . Well Sampled in Sampling Event I TW.N -13 pH Buffer 7.0 1.0 pH Buffer 4.0 Specific Conductancel-l_4.....;.q.....;.9 ___ ~I ~MHOS/ cm Well Depth(O.Olft): I 10~. 00 Depth to Water Before PurgingJ ~ 1, O:l. 4" well:1 tb. bS 1(·653h) 3" Well: 0 (.367h) L...-~ __ """ Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 113. bq Redox Potential (Eh) 1-1 ~_I_I __ ~ TurbiditYL.,.11_b_b __ ~ Weather Condo Ext'l Amb. Temp. °C (prior sampling event) ..... 1 q_o_ ...... Time Gal. Purged IL..--__ ----I Time Gal. Purged L-I ___ ---' Conductance pH IL...--__ ....... Conductance pH 1"--__ ----' Temp.oC Temp.oC Redox Potential Eh (m V) ..... 1 ___ -.....I Redox Potential Eh (m V) ..... 1 ___ -.....I Turbidity (NTU) Turbidity (NTU) Time Gal. Purged ..... 1 ___ -.....I Time Gal. Purged 1-1 ___ ----' Conductance pH I-...I ___ ...... Conductance pH L.,.I ___ --' Temp.oC Temp.oC Redox Potential Eh (m V) ..... 1 ___ ---I Redox Potential Eh (m V) IL...-___ ...... Turbidity (NTU) . 1 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater lof 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 ) b. S t> Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1'-----_'_1 __ --" gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = 1 ;2... g Y 1 Number of casing volumes evacuated (if other than two) J.OS If well evacuated to dryness, number of gallons evacuated 1 b..50 N arne of Certified Analytical Laboratory if Other Than Energy Labf,--~_v._:4 ______ ----, Sample Taken Sample Vol (indicate Filtered Preservative Pre s ervati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 100ml 0 ~ H2SO4 EJ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) E 0 Sample volume 0 ~ 0 ~ {,hlor~Je.. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--________ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) [:~:,~~JjT-1 WHITE ~i:;~=~~ MILL ~.M.~~ES~.,. __ ::J FIELD DATA WORKSHEET FOR GROUND WATER Attachment 1 b<)J See instruction Description of Sampling Event: 1 151 Qv..Q.("'ter"' N l~f1"~t~.9;6-1) ~D \a Location (well name):1-1 _1_W_Al_ ... .-.;.7_b _______ ----' Sampler Name and initials: l-r;.rH'\-c;r ~o\l"Jl-.jJ-rH Date and Time for Purgin~ 1-10 .... ~D 1~ and Sampling (if different) .AI/A '---------~ Well Purging Equip Used:~pump or@] bailer Well Pump (if other than Bennet) . I Grv.f\a-f~5 Prevo Well Sampled in Sampling Event 1,---n_W_)J_-_O_6 ___ ~ pH Buffer 7.0 I.b pH Buffer 4.0 Specific Conductance ll-~_q_Cf ____ ....II !lMHOS/ cm Well Depth(O.Olft): 114:;l..OO Depth to Water Before Purgin~ 7() .. 3 b 4" well:i '1.b, g~ i(·653h) 3" Well: l> (.367h) '----_....I Casing Volume (V) Conductance (avg) pH of Water (avg) c::.s~ Well Water Temp. (avg) r 13.l..\S Redox Potential (Eh)L-1 '3~b_'_----, Turbidity ,--I _;2._J __ ...... Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 0 6 Time Gal. Purged 1'--___ ...... Time Gal. Purged 1-1 ___ ----' Conductance Conductance pH ,1.-. __ ---1 Temp.oC Temp.oC Redox Potential Eh (mV) 11-___ ---' Redox Potential Eh (m V) 1-1 ___ ---' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged 1-1 ___ ---' Time Gal. Purged 1-1 ___ ---' Conductance pH ,--I ___ --' Conductance pH '--I ___ ...... Temp.oC Temp.oC Redox Potential Eh (m V) 1-1 ___ ---' Redox Potential Eh (mV) 1-1 ___ ----' Turbidity (NTU) Turbidity. (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..1 .....I)I....l.'_D ___ ---I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 =1 L-_'_1 __ ----1 gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 18.5 1 I Number of casing volumes evacuated (if other than two) L-I _o ___ ~ If well evacuated to dryness, number of gallons evacuated L-I _D ___ ~ Name of Certified Analytical Laboratory if Other Than Energy Lab~L...AJ_~_A _______ ..... Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients C29 0 100ml 0 ~ H2SO4 00 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 (!3 0 ~ C ~ lor I'Je:. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--________ ..... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 TabC Kriged Current Quarter Groundwater Contour Map and Depth to Water Summary NAME: Tanner Holliday, Garrin Palmer DATE: 3/27/2012 TIME WELL Static level TIME WELL Static Level TIME WELL Static Level TIME 911 MW-1 64.59 1253 MW-4 71.11 851 PIEZ-1 61.59 1213 MW-2 109.70 1249 TW4-1 64.94 856 PIEZ-2 21.20 1201 MW-3 83.20 1256 TW4-2 66.86 1000 PIEZ-3 40.25 1202 MW-3A 85.23 1259 TW4-3 50.30 1222 PIEZ-4 47.60 1313 MW-5 106.13 1246 TW4-4 70.01 1226 PIEZ-5 43.11 1351 1243 MW-ll 88.11 1301 TW4-5 56.81 1348 1309 MW-12 108.45 1245 TW4-6 70.05 1011 TWN-1 51.55 1300 1247 MW-14 103.64 1251 TW4-7 67.90 1006 TWN-2 21.00 1343 1249 MW-15 106.37 1258 TW4-8 66.55 1003 TWN-3 32.80 1340 1156 MW-17 74.86 1303 TW4-9 54.75 957 TWN-4 41.05 1336 909 MW-18 70.20 1305 TW4-10 56.35 916 TWN-5 69.57 1212 853 MW-19 52.14 1255 TW4-11 57.81 904 TWN-6 74.60 1209 1402 MW-20 84.47 1237 TW4-12 47.16 914 TWN-7 88.34 1206 1257 MW-22 66.89 1235 TW4-13 47.15 906 TWN-8 61.63 1328 1307 MW-23 114.55 1233 TW4-14 86.89 848 TWN-9 62.89 1333 1210 MW-24 114.36 1235 TW4-15 68.15 859 TWN-10 80.82 1239 MW-25 73.78 1226 TW4-16 60.26 835 TWN-ll 69.42 1326 1235 MW-26 68.15 1224 TW4-17 74.93 832 TWN-12 28.55 1203 MW-27 51.04 1012 TW4-18 56.65 846 TWN-13 46.00 1313 1207 MW-28 76.55 929 TW4-19 58.99 843 TWN-14 62.46 1312 1216 MW-29 102.00 1235 TW4-20 61.80 901 TWN-15 92.02 1304 1219 MW-30 75.96 1016 TW4-21 54.11 839 TWN-16 47.86 1221 MW-31 68.10 1233 TW4-22 53.39 840 TWN-17 33.88 70.6 1224 MW-32 74.93 1244 TW4-23 64.78 954 TWN-18 58.40 43076 1256 MW-33 Dry 1230 TW4-24 54.80 925 TWN-19 52.49 1254 MW-34 107.84 1009 TW4-25 47.50 1304 MW-35 112.24 1241 TW4-26 63.50 1257 MW-36 110.35 1230 TW4-27 83.10 1251 MW-37 110.58 We split up to complete depth checks so some of the times may be the same. Protective casing needs to be placed around TW4-2. TW4-27 needs to be painted and labeled. WELL DR-1 DR-2 DR-5 DR-6 DR-7 DR-8 DR-9 DR-10 DR-ll DR-12 DR-13 DR-14 DR-15 DR-16 DR-17 DR-18 DR-19 DR-20 DR-21 DR-22 DR-23 DR-24 DR-25 Static Level ABANDON ABANDON 83.14 94.36 92.20 50.91 86.51 78.07 98.38 88.21 69.93 76.35 92.95 ABANDON 64.63 ABANDON 63.35 55.22 107.40 Dry 70.60 43.76 ABANDON ."" «..'" Estimated dry area M.W-S perched monitoring well showing 5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5577 showing elevation in feet amsl TWN-10 ~5586 temporary perched nitrate monitoring well showing elevation in feet amsl PIEZ-1 perched piezometer showing Q 5594 elevation in feet amsl TW4-27 temporary perched monitoring well ~ 5525 installed October, 2011 showing elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are pumping wells KRIGED 1st QUARTER, 2012 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/may121UwI0312.srf C-l TabD Kriged Previous Quarter Groundwater Contour Map @ Estimated dry area M~-5 perched monitoring well showing -5503 elevation in feet amsl TW04.12 temporary perched monitoring well 5584 showing elevation in feet amsl TWN·10 ¢'5586 temporary perched nitrate monitoring well showing elevation in feet amsl PIEZ-1 perched piezometer showing @ 5594 elevation in feet amsl TW4·27 temporary perched monitoring well ~ 5518 installed October, 2011 showing elevation in feet amsl RUIN SPRING 0 5380; seep or spring showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are pumping wells KRIGED 4th QUARTER~ 2011 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/feb12/UwI1211.srf D-l TabE Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells .-.. C. E .c ..: 't-~ CI) E ~ ~ CI) > 0 Ci) > CI) ..J ~ CI) ... ~ ,.... I Z 3: t- C ~/8 ~/O ~ --.-------r----r------r-----,----...,.-----,-----. C ~/~0/170 ~ ~/17 ~/60 ~ ~/9clcO o ~/O ~/80 O~/ccHO 60/90lLO 80/8 ~/c ~ 80/~0/90 +-----+----l----+-----+----I-----l----! o o L() T""" L() q C\J L() ..-.. C. E .c ~ ~ ---(1) E i= J.. (1) > 0 (1) > (1) ...J J.. (1) ... CO == C\I I Z == .... G ~/8 ~/O ~ .-------r------.,.------.,....------r---------, G ~/~OlvO ~ ~/v ~/60 ~ ~/9G/GO o ~/O ~/80 o ~/GG/~O 6 0/90lL 0 80/8 ~/G ~ 80/~0/90 --l------+-----.j...-----~------}------! o o q LO o o C\I o Lri C\I .-.. a. E .c ..; 'I-"'-' CD E i= J.. CD > 0 CD > CD ..J J.. CD ... 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G ~/O ~/LO -r--------r----.,-----.,.------r-----,.----_r-----....., G ~/~O/vO ~ ~/v ~/60 ~ ~/90/90 ~ ~/9G/GO O~/B ~H ~ o ~/O ~/BO o ~/GO/90 O~/GGHO 60/v~/0~ 60/90/LO -!------I-----I----+-----+-----I-----+------4 o N LO LO N LO o M LO LO M LO o ~ LO LO ~ LO o ui LO ~ LO LO TabF Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Water Levels and Data over Time White Mesa Mill-Well TWN-l Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,646.96 5,648.09 1.13 112.5 5,600.38 02/06/09 47.71 46.58 5,599.99 07/21109 48.10 46.97 5,600.26 09/21109 47.83 46.70 5,601.10 10/28/09 46.99 45.86 5,602.59 12/14/09 45.50 44.37 5,600.55 03/11110 47.54 46.41 5,600.66 05/11110 47.43 46.30 5,599.18 09/29/10 48.91 47.78 5,598.92 12/21110 49.17 48.04 5,598.29 02/28111 49.80 48.67 5,597.80 06/21111 50.29 49.16 5,597.32 09/20/11 50.77 49.64 5,597.15 12/21111 50.94 49.81 5,596.54 03/27112 51.55 50.42 Water Levels and Data over Time White Mesa Mill-Well TWN-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,625.75 5,626.69 0.94 95 5,611.37 02/06/09 15.32 14.38 5,610.63 07/21/09 16.06 15.12 5,609.73 09/21/09 16.96 16.02 5,607.08 11/02/09 19.61 18.67 5,606.57 12114/09 20.12 19.18 5,612.45 03111110 14.24 13.30 5,612.78 05111110 13.91 12.97 5,611.37 09/29110 15.32 14.38 5,610.24 12/21110 16.45 15.51 5,610.64 02/28111 16.05 15.11 5,609.78 06/21/11 16.91 15.97 5609.79 09/20111 16.90 15.96 5609.72 12/21111 16.97 16.03 5,605.69 03/27112 21.00 20.06 Water Levels and Data over Time White Mesa Mill-Well TWN-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,633.64 5,634.50 0.86 110 5,603.77 02/06/09 30.73 29.87 5,602.37 07/21/09 32.13 31.27 5,602.34 09/21/09 32.16 31.30 5,602.60 10/28/09 31.90 31.04 5,603.12 12/14/09 31.38 30.52 5,602.90 03/11110 31.60 30.74 5,603.23 05111/10 31.27 30.41 5,602.86 09/29110 31.64 30.78 5,603.35 12/21110 31.15 30.29 5,602.89 02/28111 31.61 30.75 5,602.75 06/21/11 31.75 30.89 5,602.40 09/20/11 32.10 31.24 5,602.40 12/21111 32.10 31.24 5,601.70 03/27112 32.80 31.94 Water Levels and Data over Time White Mesa Mill-Well TWN-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,641.04 5,641.87 0.83 136 5,601.47 02/06/09 40.40 39.57 5,604.26 07121109 37.61 36.78 5,605.02 09121109 36.85 36.02 5,605.87 10128/09 36.00 35.17 5,605.81 12/14/09 36.06 35.23 5,605.31 03/11110 36.56 35.73 5,605.36 05111110 36.51 35.68 5,604.59 09129/10 37.28 36.45 5,604.42 12121110 37.45 36.62 5,603.69 02128111 38.18 37.35 5,603.36 06121111 38.51 37.68 5,602.82 09120111 39.05 38.22 5,602.79 12121111 39.08 38.25 5,600.82 03127/12 41.05 40.22 Water Levels and Data over Time White Mesa Mill-Well TWN-S Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,653.70 5,655.18 1.48 155 5,584.43 08125/09 70.75 69.27 5,584.51 09121109 70.67 69.19 5,584.54 11110109 70.64 69.16 5,584.62 12114/09 70.56 69.08 5,584.97 03111110 70.21 68.73 5,585.38 05/11110 69.80 68.32 5,585.35 09129/10 69.83 68.35 5,585.42 12121110 69.76 68.28 5,585.08 02128111 70.10 68.62 5,585.38 06121111 69.80 68.32 5,585.51 09120111 69.67 68.19 5,585.76 12121/11 69.42 67.94 5,585.61 03127/12 69.57 68.09 Water Levels and Data over Time White Mesa Mill-Well TWN-6 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,663.03 5,664.94 1.91 135 5,589.52 08/25/09 75.42 73.51 5,589.46 09/22/09 75.48 73.57 5,589.61 11/03/09 75.33 73.42 5,589.92 12114/09 75.02 73.11 5,590.24 03/11110 74.70 72.79 5,590.40 05111110 74.54 72.63 5,590.24 09/29110 74.70 72.79 5,590.49 12/21/10 74.45 72.54 5,590.16 02/28/11 74.78 72.87 5,590.44 06/21111 74.50 72.59 5,590.35 09/20111 74.59 72.68 5,590.67 12/21111 74.27 72.36 5,590.34 03/27112 74.60 72.69 Water Levels and Data over Time White Mesa Mill -Well TWN-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,647.39 5,649.26 1.87 120 5,552.56 08125/09 96.70 94.83 5,558.34 09121109 90.92 89.05 5,558.82 11110109 90.44 88.57 5,558.96 12114/09 90.30 88.43 5,559.54 03/11/10 89.72 87.85 5,559.60 05111110 89.66 87.79 5,559.83 09/29/10 89.43 87.56 5,559.00 12121/10 90.26 88.39 5,559.68 02128/11 89.58 87.71 5,560.43 06121111 88.83 86.96 5,560.46 09120/11 88.80 86.93 5,560.78 12121111 88.48 86.61 5,560.92 03127112 88.34 86.47 Water Levels and Data over Time White Mesa Mill -Well TWN-8 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,649.35 5,651.48 2.13 160 5,589.01 08/25/09 62.47 60.34 5,589.10 09/21/09 62.38 60.25 5,589.09 11103/09 62.39 60.26 5,603.38 12114/09 48.10 45.97 5,589.68 03111110 61.80 59.67 5,589.95 05/11110 61.53 59.40 5,589.74 09/29110 61.74 59.61 5,589.97 12/21110 61.51 59.38 5,589.67 02/28111 61.81 59.68 5,589.96 06/21111 61.52 59.39 5,589.82 09/20111 61.66 59.53 5,590.18 12/21111 61.30 59.17 5,589.85 03/27/12 61.63 59.50 Water Levels and Data over Time White Mesa Mill -Well TWN-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,645.68 5,647.45 1.77 102.5 5,582.05 08125/09 65.40 63.63 5,582.12 09122/09 65.33 63.56 5,582.27 11110109 65.18 63.41 5,582.53 12114/09 64.92 63.15 5,582.92 03111110 64.53 62.76 5,583.06 05111110 64.39 62.62 5,583.25 09129110 64.20 62.43 5,583.57 12121110 63.88 62.11 5,583.54 02128/11 63.91 62.14 5,583.92 06121111 63.53 61.76 5,584.04 09120111 63.41 61.64 5,587.42 12121111 60.03 58.26 5,584.56 03127112 62.89 61.12 Water Levels and Data over Time White Mesa Mill -Well TWN-IO Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,664.63 5,666.98 2.35 107.5 5,584.18 08/25/09 82.80 80.45 5,584.40 09/22/09 82.58 80.23 5,584.61 11110109 82.37 80.02 5,584.90 12114/09 82.08 79.73 5,585.21 03111110 81.77 79.42 5,585.42 05111110 81.56 79.21 5,585.42 09/29110 81.56 79.21 5,585.68 12/21110 81.30 78.95 5,585.60 02/28111 81.38 79.03 5,585.95 06/21111 81.03 78.68 5,585.92 09/20111 81.06 78.71 5,586.22 12/21111 80.76 78.41 5,586.16 03/27/12 80.82 78.47 Water Levels and Data over Time White Mesa Mill-Well TWN-ll Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,683.16 5,684.53 1.37 147.5 5,613.00 11103/09 71.53 70.16 5,613.88 12114/09 70.65 69.28 5,614.65 03111110 69.88 68.51 5,615.16 05111110 69.37 68.00 5,614.93 09/29/10 69.60 68.23 5,615.09 12/21/10 69.44 68.07 5,614.96 02/28111 69.57 68.20 5,615.12 06/21111 69.41 68.04 5,614.96 09/20/11 69.57 68.20 5,615.18 12/21111 69.35 67.98 5,615.11 03/27/12 69.42 68.05 Water Levels and Data over Time White Mesa Mill -Well TWN-12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,667.03 5,668.24 1.21 115 5,628.33 11103/09 39.91 38.70 5,628.86 12114/09 39.38 38.17 5,630.27 03/11110 37.97 36.76 5,631.64 05111110 36.60 35.39 5,633.73 09/29/10 34.51 33.30 5,633.43 12/21/10 34.81 33.60 5,634.35 02/28111 33.89 32.68 5,635.95 06/21111 32.29 31.08 5,636.44 09/20111 31.80 30.59 5,638.93 12/21/11 29.31 28.10 5,639.69 03/27/12 28.55 27.34 Water Levels and Data over Time White Mesa Mill-Well TWN-13 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,633.04 5,634.32 1.28 120 5,586.95 11103/09 47.37 46.09 5,587.22 12/14/09 47.10 45.82 5,587.45 03111110 46.87 45.59 5,587.64 05/11110 46.68 45.40 5,587.37 09/29110 46.95 45.67 5,587.77 12/21/10 46.55 45.27 5,587.64 02/28111 46.68 45.40 5,587.89 06/21111 46.43 45.15 5,588.03 09/20111 46.29 45.01 5,588.30 12/21/11 46.02 44.74 5,588.32 03/27112 46.00 44.72 Water Levels and Data over Time White Mesa Mill -Well TWN-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,647.80 5,649.53 1.73 135 5,586.18 11104/09 63.35 61.62 5,586.51 12114/09 63.02 61.29 5,586.71 03111110 62.82 61.09 5,586.72 05111110 62.81 61.08 5,586.53 09/29/10 63.00 61.27 5,586.80 12/21110 62.73 61.00 5,586.74 02/28111 62.79 61.06 5,586.84 06/21/11 62.69 60.96 5,586.73 09/20/11 62.80 61.07 5,586.98 12/21111 62.55 60.82 5,587.07 03/27112 62.46 60.73 Water Levels and Data over Time White Mesa Mill-Well TWN-IS Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,675.01 5,676.49 1.48 155 5,594.12 11/10109 82.37 80.89 5,584.03 12114/09 92.46 90.98 5,584.10 03111110 92.39 90.91 5,584.16 05/11110 92.33 90.85 5,584.26 09/29/10 92.23 90.75 5,584.30 12/21110 92.19 90.71 5,584.04 02/28111 92.45 90.97 5,584.30 06/21/11 92.19 90.71 5,584.37 09/20/11 92.12 90.64 5,584.49 12/21111 92.00 90.52 5,584.47 03/27112 92.02 90.54 Water Levels and Data over Time White Mesa Mill-Well TWN-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,651.07 5,652.70 1.63 100 5,603.34 11104/09 49.36 47.73 5,603.56 12/14/09 49.14 47.51 5,603.84 03/11110 48.86 47.23 5,604.31 05111110 48.39 46.76 5,604.28 09/29/10 48.42 46.79 5,604.39 12/21110 48.31 46.68 5,604.20 02/28111 48.50 46.87 5,604.55 06/21111 48.15 46.52 5,604.74 09/20111 47.96 46.33 5,604.94 12/21111 47.76 46.13 5,604.84 03/27112 47.86 46.23 Water Levels and Data over Time White Mesa Mill-Well TWN-17 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,639.73 5,641.55 1.82 100 5,605.96 11104/09 35.59 33.77 5,606.27 12/14/09 35.28 33.46 5,606.25 03111110 35.30 33.48 5,606.55 05111110 35.00 33.18 5,606.77 09/29/10 34.78 32.96 5,607.15 12/21/10 34.40 32.58 5,606.96 02/28111 34.59 32.77 5,607.22 06/21111 34.33 32.51 5,607.40 09/20111 34.15 32.33 5,607.85 12/21111 33.70 31.88 5,607.67 03/27112 33.88 32.06 Water Levels and Data over Time White Mesa Mill-Well TWN -18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,643.95 5,645.45 1.50 100 5,586.85 11102/09 58.60 57.10 5,600.14 12/14/09 45.31 43.81 5,587.36 03/11110 58.09 56.59 5,587.71 05/11110 57.74 56.24 5,587.50 09/29/10 57.95 56.45 5,607.66 12/21110 37.79 36.29 5,587.35 02/28111 58.10 56.60 5,587.71 06/21111 57.74 56.24 5,587.65 09/20111 57.80 56.30 5,587.95 12/21111 57.50 56.00 5,587.05 03/27/12 58.40 56.90 Water Levels and Data over Time White Mesa Mill -Well TWN -19 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,659.59 5,661.36 1.77 110 5,606.17 11/02/09 55.19 53.42 5,606.70 12114/09 54.66 52.89 5,607.22 03111110 54.14 52.37 5,607.89 05111110 53.47 51.70 5,607.98 09/29110 53.38 51.61 5,608.41 12/21/10 52.95 51.18 5,608.49 02/28/11 52.87 51.10 5,608.60 06/21/11 52.76 50.99 5,609.17 09/20111 52.19 50.42 5,608.90 12/21111 52.46 50.69 5,608.87 03/27112 52.49 50.72 TabG Laboratory Analytical Reports EN:RGY www.energyiab.com ,h.~j~nA'J,Mf·'77;'472"0711 -Billings, MT 800·735·4489 -Casper, WY 888-235-0515 AnalyticalExtllllellCBSinCf 7952 W1GJ~gB~ .. 7.n~ -Rapid Citv,·,SI)888-672~1225 • College Station. IX 888-690-2218 LABORATORIES ~==============~---------------= April 09, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12010435 ANAL VTICAL SUMMARY REPORT Quote ID: C3317 -Nitrate and Chloride Sampling Project Name: 1 st Quarter Nitrate 2012 Energy Laboratories, Inc. Casper WY received the following 30 samples for Denison Mines USA Corp on 1/13/2012 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C1201'0435-001 TWN-08R 01/09/12 10:25 01/13/12 Aqueous Chloride Nitrogen, Nitrate + Nitrite C 1 201 0435-002 TWN-12R 01/10/127:15 01/13/12 Aqueous Same As Above C 120 1 0435-003 TWN-17R 01/11/127:10 01/13/12 Aqueous Same As Above C 120 1 0435-004 TWN-08 01/09/1210:52 01/13/12 Aqueous Same As Above C12010435-005 TWN-13 01/09/12 12:07 01/13/12 Aqueous Same As Above C 120 1 0435-006 TWN-10 01/10/12 6:30 01/13/12 Aqueous Same As Above C 120 1 0435-007 TWN-05 01/09/12 13:25 01/13/12 Aqueous Same As Above C 120 1 0435-008 TWN-01 01/09/12 14:07 01/13/12 Aqueous Same As Above C12010435-009 TWN-04 01/09/1214:54 01/13/12 Aqueous Same As Above C1201 0435-01 0 TWN-12 01/10/127:41 01/13/12 Aqueous Same As Above C12010435-011 TWN-15 01/11/129:34 01/13/12 Aqueous Same As Above C12010435-012 TWN-06 01/10/129:11 01/13/12 Aqueous Same As Above C12010435-013 TWN-11 01/10/1210:0301/13/12 Aqueous Same As Above C12010435-014 TWN-18 01/10/1210:52 01/13/12 Aqueous Same As Above C12010435-015 TWN-07 01/11/129:44 01/13/12 Aqueous Same As Above C12010435-016 TWN-16 01/10/1212:46 01/13/12 Aqueous Same As Above C12010435-017 TWN-14 01/11/129:55 01/13/12 Aqueous Same As Above C12010435-018 TWN-19 01/10/1214:19 01/13/12 Aqueous Same As Above ---------------_._-_.-------_._--_._------------_. __ .-------_.---------------_._------------------------------_._----------------------------_._-------"-----------_._---_. __ ._-------- C12010435-019 TWN-17 01/12/126:50 01/13/12 Aqueous Same As Above ._--------_._---------------------------------------------------------------------------------------------------------------------------------------------~----~-------------------~--------- C12010435-020 TWN-09 01/12/127:00 01/13/12 Aqueous Same As Above --~--~-----~------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- C12010435-021 TWN-03 01/12/127:10 01/13/12 Aqueous Same As Above C 120 1 0435-022 TWN-02 01/12/127:18 01/13/12 Aqueous Same As Above C12010435-023 Piez-01 01/11/1212:4601/13/12 Aqueous Same As Above C12010435-024 Piez-02 01/11/12 12:25 01/13/12 Aqueous Same As Above -------------------------- C 120 1 0435-025 Piez-03 01/11/1212:1001/13/12 Aqueous Same As Above C 120 1 0435-026 UWLP 01/11/1212:3401/13/12 Aqueous Same As Above C12010435-027 TWN-60 01/11/1213:50 01/13/12 Aqueous Same As Above Page 1 of 17 EN:RGY LABORAT ORIES www.energyiab.com Analytical Excs/Ien&B SiIlCll 1!152 . . .. .. .He!ena"Mf817.~412"Oll t -Billings, MT 800 .. 735-4489 -Casper, WY 888-235-0515 ·~i~~¢, ~,,8'6"Q86';7Jl5 • Rapid CiW, SI) 888-672-1225 -College Station, IX 888-690-2218 ANAL VTICAL SUMMARY REPORT C12010435-028 TWN-65 01/10/12 6:30 01/13/12 Aqueous Same As Above C 120 1 0435-029 TW N-70 01/10/1210:03 01/13/12 Aqueous Same As Above C12010435-030 Temp Blank 01/12/12 0:00 01/13/12 Aqueous Temperature The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: cS¥~D tJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.04.09 10:32:52 -06:00 Page 2 of 17 www.energylab.com Analytical ExcslJsncB Sines 7852 >·;:R~I<~n.a;'~r8n"412-0111 .BUlings1MT800"735"4489 • Casper,WY 888-235-051.5 ~;~(m';fej::<wy {68;.686'..7115 -Raid C[ ,s~ 888-672,;.1225 -College Station, 1X 888-690-2218 CLIENT: Denison Mines USA Corp Project: 1 st Quarter Nitrate 2012 Sample Delivery Group: C12010435 REVISED/SUPPLEMENTAL REPORT Revised Date: 04/09/12 Report Date: 01/23/12 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on April 9, 2012 for the correction of the collection time on sample TWN-65. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 3 of 17 EN:RGY LABORAT ORIES www.energylab.com · . .-...:Hel~na.MT877 .. 412-0711 .Billings.MT 800-735-4489 . Casper, WY 888-235-0515 Analytical ExcslJsnl:lI Sines 1952 ~=~~ __ :~l!!~jt~~ 'Y!i _8~J';6.86-7175 • Rapid City, SI} 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 Lab ID: C12010435-001 Client Sample ID: TWN-OBR Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C 120 1 0435-002 Client Sample ID: TWN-12R Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C12010435-003 Client Sample ID: TWN-17R Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C12010435-004 Client Sample ID: TWN-OB Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result Units NO mg/L NO mg/L Result Units NO 0.2 mg/L mg/L Result Units NO NO mg/L mg/L Result Units 11 NO mg/L mg/L Qualifiers Qualifiers Qualifiers Qualifiers Rl 0.1 Rl 1 0.1 Rl 0.1 Rl 0.1 Revised Date: 04/09/12 Report Date: 01 123/1 2 Collection Date: 01/09/1210:25 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date I By A4500-CI B 01/17/1210:58f1r E353.2 01/16/1213:19/dc Collection Date: 01/10/1207:15 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date I By A4500-CI B 01/17/12 11 :00 fir E353.2 01/16/1213:271 dc Collection Date: 01/11/1207:10 DateReceived: 01/13/12 Matrix: Aqueous Mell Qel Method Analysis Date I By MeL! A4500-CI B 01/17/12 11 :02 fir E353.2 01/16/12 13:341 dc Collection Date: 01/09/12 10:52 DateReceived: 01/13/12 Matrix: Aqueous Qel Method Analysis Date I By A4500-CI B 01/17/12 11 :04 1 Ir E353.2 01/16/1213:371 dc MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 17 EN:RGY www.energylab.com .Hel~n.a,_.Mr~n .. 412-0711 -Billings, MT 800-735-4489 . Casper, WY 888-235-0515 LABORAT ORIES Analytical manlOClI Sine, 1952 ,~t.t¢!wy~n~~:~8~-:n7~ -Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 LablD: C12010435-005 Client Sample ID: TWN-13 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C 120 1 0435-006 Client Sample ID: TWN-10 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C12010435-007 Client Sample ID: TWN-05 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C12010435-008 Client Sample ID: TWN-01 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result Units 46 mg/L ND mg/L Result Units 44 0.8 mg/L mg/L Result Units 45 0.2 mg/L mg/L Result Units 15 0.6 mg/L mg/L Qualifiers Qualifiers Qualifiers Qualifiers Rl 0.1 Rl 0.1 Rl 0.1 Rl 1 0.1 Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/09/12 12:07 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-CI B 01/17/1211:06/1r E353.2 01/16/1213:391 dc Collection Date: 01/10/12 06:30 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-CI B 01/17/12 11 :09 /lr E353.2 01/16/12 13:421 dc Collection Date: 01/09/1213:25 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By MeL! A4500-CI B 01/17/12 11 :12 /lr E353.2 01/16/1213:44/dc Collection Date: 01/09/12 14:07 DateReceived: 01/13/12 Matrix: Aqueous Qel Method Analysis Date 1 By A4500-CI B 01/17/12 11 :13 1 Ir E353.2 01/16/1213:47/dc MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 5 of 17 EN:RGY LABORATORIES www.energylab.comHelen~.MT877;.472.;011t .Billings.MT 800-735-4489 . Casper, WY 888-235-0515 Analytical £XCIII/snell Sines '952 ;-_~il!~~e! wy -86&-&Be~1115 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 Lab ID: C12010435-009 Client Sample ID: TWN-04 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C1201 0435-01 0 Client Sample ID: TWN-12 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C12010435-011 Client Sample ID: TWN-15 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C12010435-012 Client Sample ID: TWN-06 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result Units 20 mg/L 0.9 mg/L Result Units 104 mg/L 0.9 mg/L Result Units 38 1.5 mg/L mg/L Result Units 20 1.2 mg/L mg/L Qualifiers Rl 0.1 Qualifiers Rl 0.1 Qualifiers Rl 0.1 Qualifiers Rl 0.1 Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/09/12 14:54 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-CI B 01/17/12 11 :22 fir E353.2 01/16/1213:49/dc Collection Date: 01/10/12 07:41 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-CI B 01/17/12 11 :26 fir E353.2 01/16/12 13:521 dc Collection Date: 01/11/12 09:34 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By MeL! A4500-CI B 01/17/12 11 :29 fir E353.2 01/16/1213:54/dc Collection Date: 01/10/1209:11 DateReceived: 01/13/12 Matrix: Aqueous Qel Method Analysis Date 1 By A4500-CI B 01/17/1211:31/1r E353.2 01/16/12 14:041 dc MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 17 '. EN:RGY LABORATORIES www.energylab.com .Helena.MI··B77~412-071t .Billings.MT 800-735-4489 • Casper, WY 888-235-0515 AnaIyticaIExcsJI8flCBSincs 1952 ..l!leftet wt8.6" .. 6'8~-111~ • Rapid City, so 888-672-1225 • College Station, IX 888 .. 690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 Lab 10: C12010435-013 Client Sample 10: TWN-11 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-014 Client Sample 10: TWN-18 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-015 Client Sample 10: TWN-07 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-016 Client Sample 10: TWN-16 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result Units 69 mg/L 1.6 mg/L Result Units 64 1.9 mg/L mg/L Result Units 5 2.3 mg/L mg/L Result Units 33 2.8 mg/L mg/L Qualifiers RL 0.1 Qualifiers RL 0.1 Qualifiers RL 0.1 Qualifiers RL 0.1 Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/10/1210:03 DateReceived: 01/13/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By A4500-CI B 01/17/1211 :35/1r E353.2 01/16/1214:121 dc Collection Date: 01/10/12 10:52 DateReceived: 01/13/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By A4500-CI B 01/17/12 11 :38 1 Ir E353.2 01/16/1214:14/dc Collection Date: 01/11/1209:44 DateReceived: 01/13/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By MCL! A4500-CI B 01/17/12 11 :41 fir E353.2 01/16/1214:171 dc Collection Date: 01/10/1212:46 OateReceived: 01/13/12 Matrix: Aqueous QCL Method Analysis Date I By A4500-CI B 01/17/12 11 :43 fir E353.2 01/16/1214:19/dc MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 17 EI'.ERGY LABORATORIES www.energylab.com ·H~!~n;J._.MT877 .. 472-D711 .Billings.MT 800-735-4489 • Casper, WY 888-235-0515 Analytical £Xc.HeneB Sines 1952 _~:~ -_ §1!1~tt~~,WY QQ>6 .. 68G-711~ • Rapid City, 51) 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 Lab 10: C12010435-017 Client Sample 10: TWN-14 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-018 Client Sample 10: TWN-19 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-019 Client Sample 10: TWN-17 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-020 Client Sample 10: TWN-09 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result 26 3.5 Result 114 7.0 Result 79 8.7 Result 202 12.2 D -RL increased due to sample matrix. Units mg/L mg/L Units mg/L mg/L Units mg/L mg/L Units mg/L mg/L Qualifiers Rl 0.1 Qualifiers Rl D 0.5 Qualifiers Rl D 0.5 Qualifiers Rl 1 D 0.5 MeL! Qel Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/11/1209:55 DateReceived: 01/13/12 Matrix: Aqueous Method Analysis Date / By A4500-CI B 01/17/1211:45/Ir E353.2 01/16/1214:22/dc Collection Date: 01/10/1214:19 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date / By A4500-CI B 01/17/1211:49/1r E353.2 01/17/1212:34/dc Collection Date: 01/12/1206:50 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date / By A4500-CI B 01/17/1212:01 fir E353.2 01/17/1212:37/dc Collection Date: 01/12/1207:00 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date / By A4500-CI B 01/17/12 12:03 fir E353.2 01/17/1212:39/dc MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 8 of 17 EI\ERGY www.energylab.com 'H.B"I~na, ,MT~11;'412-071 t • Billings. MT 800-735-4489 • Casper, WY 888-235-0515 LABORATORIES Analytk:al ExcsHIHICB Sinclll952 "", _~llj~tt~, Wt~_Q$~.86,"7l15 • Rapid City, S() 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 Lab 10: C12010435-021 Client Sample 10: TWN-03 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-022 Client Sample 10: TWN-02 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-023 Client Sample 10: Pie,z-01 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-024 Client Sample 10: Piez-02 Result 143 25 Result 86 31 Result 78 7.1 Units mg/L mg/L Units mg/L mg/L Units mg/L mg/L Analyses Result Units MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. 9 0.1 o -RL increased due to sample matrix. mg/L mg/L Qualifiers 0 Qualifiers 0 Qualifiers 0 Qualifiers RL 2 RL 2 RL 1 0.5 RL 1 0.1 Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/12/1207:10 DateReceived: 01/13/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By A4500-CI B 01/17/1212:05/1r E353.2 01/17/12 12:421 dc Collection Date: 01/12/1207:18 DateReceived: 01/13/12 Matrix: Aqueous MCL! QCL Method Analysis Date I By A4500-CI B 01/17/1212:08/1r E353.2 01/17/1212:441 dc Collection Date: 01/11/12 12:46 DateReceived: 01/13/12 Matrix: Aqueous MeL! QCL MCL! Method Analysis Date I By A4500-CI B 01/17/1212:101lr E353.2 01/17/1212:471 dc Collection Date: 01/11/12 12:25 DateReceived: 01/13/12 Matrix: Aqueous QCL Method Analysis Date I By A4500-CI B 01/17/1212:12 fir E353.2 01/17/1212:49/dc MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 17 EN:RGY ~~ www.energylab.com .. .. <...~H~t~nJIJMTI71 .. 472-071t .BillingS.MT 800-735-4489 -Casper, WY 888-235-0515 .., ~ AnalyticalExcslJ(1IICBSincs 1852 ,iru!I~!1~,'yrt 8&6~.B6-7J7~ • Rapip City, SO 888-672-1225 -College Station, lX 888-6~D-2218 LABORAT ORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Nitrate 2012 Lab 10: C 120 1 0435-025 Client Sample 10: Piez-03 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-026 Client Sample 10: UWLP Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C 120 1 0435-027 Client Sample 10: TWN-60 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C12010435-028 Client Sample 10: TWN-65 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 20 mg/l 1.8 mg/l Result Units 2 NO mg/l mg/l Result Units NO NO mg/l mg/l Result Units 40 0.7 mg/l mg/l Qualifiers Qualifiers Qualifiers Qualifiers Rl 0.1 Rl 1 0.1 Rl 0.1 Rl 0.1 Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/11/12 12:10 Date Received : 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-CI B 01/17/1212:28/1r E353.2 01/17/1212:52/dc Collection Date: 01/11/1212:34 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By A4500-CI B 01/17/12 12:301 Ir E353.2 01/17/12 12:541 dc Collection Date: 01/11/12 13:50 DateReceived: 01/13/12 Matrix: Aqueous MeL! Qel Method Analysis Date 1 By MeL! A4500-CI B 01/17/1212:321 Ir E353.2 01/17/1213:021 dc Collection Date: 01/10/12 06:30 DateReceived: 01/13/12 Matrix: Aqueous Qel Method Analysis Date 1 By A4500-CI B 01/17/12 12:36 /lr E353.2 01/17/1213:09/dc MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 17 EN:RGY www.energylab.com ; .... Hel,~n.~, MT871-472-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 AnalyticalExcs/lsncllSincs 1952 .lml~t!~::W-i.~Q~-QB~-717~ • Rapid City, SO 888-672-1225 . College Station, TX 888-6~D-2218 LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter Nitrate 2012 C12010435-029 Client Sample 10: TWN-70 Analyses Result MAJOR IONS Chloride 74 Nitrogen, Nitrate+Nitrite as N 1.6 Lab 10: C 120 1 0435-030 Client Sample 10: Temp Blank Units mg/L mg/l Analyses Result Units PHYSICAL PROPERTIES Temperature Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. 2.4 Qualifiers RL 0.1 Qualifiers RL Revised Date: 04/09/12 Report Date: 01/23/12 Collection Date: 01/10/12 10:03 DateReceived: 01/13/12 Matrix: Aqueous MCL! QCL MCL! Method Analysis Date I By A4500-CI B 01/17/1212:4211r E353.2 01/17/12 13:12 I dc Collection Date: 01/12/12 DateReceived: 01/13/12 Matrix: Aqueous QCL Method Analysis Date I By E170.1 01/13/1210:001 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 11 of 17 EN:RGY www.energyiab.com . . fte!e!la, MT877-472-0711 • Billings, MT 800-735-4489 . Casper, W'f 888-235-0515 =~:M!e,t!~~ WY86,6 .. ~~6~jn5 • Rapip City, SO 888-672-1225 • College Station, lX 688-690-2218 LABORATORIES Analytft;al Excsl/sn&s Sines '952 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 04/09/12 Report Date: 01/23/12 Work Order: C12010435 Client: Denison Mines USA Corp Project: 1 st Quarter Nitrate 2012 Analyte Count Result Units Method: A4500-CI B Sample 10: MBLK9-120117A Method Blank Chloride ND mg/L Sample 10: C12010435-008AMS Sample Matrix Spike Chloride 51.4 mg/L Sample 10: C12010435-008AMSO Sample Matrix Spike Duplicate Chloride 51.8 mg/L Sample 10: C12010435-018AMS Sample Matrix Spike Chloride 294 mg/L Sample 10: C12010435-018AMSO Sample Matrix Spike Duplicate Chloride 292 mg/L Sample 10: LCS35-120117A Laboratory Control Sample Chloride 3560 mg/L Sample 10: C12010435-028AMS Sample Matrix Spike Chloride 128 mg/L Sample 10: C12010435-028AMSO Sample Matrix Spike Duplicate Chloride 129 mg/L Sample 10: C12010435-029AMS Sample Matrix Spike Chloride 254 mg/L Sample 10: C12010435-029AMSO Sample Matrix Spike Duplicate Chloride 257 mg/L Qualifiers: RL -Analyte reporting limit. RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: 120117A-CL-TTR-W Run: TITRATION_120117A 01/17/1210:45 1.0 Run: TITRATION_120117A 01/17/1211:15 1.0 103 90 110 Run: TITRATION 120117A 01/17/1211 :17 - 1.0 104 90 110 0.7 10 Run: TITRATION_120117A 01/17/12 11 :50 1.0 101 90 110 Run: TITRATION_120117A 01/17/1211:52 1.0 100 90 110 0.6 10 Run: TITRATION 120117A 01/17/1211 :54 - 1.0 100 90 110 Run: TITRATION_120117A 01/17/1212:38 1.0 99 90 110 Run: TITRATION 120117A 01/17/1212:40 - 1.0 100 90 110 0.7 10 Run: TITRATION_120117A 01/17/1212:45 1.0 101 90 110 Run: TITRATION_120117A 01/17/1212:48 1.0 103 90 110 1.4 10 ND -Not detected at the reporting limit. Page 12 of 17 EN:RGY www.energylab.com , .. ....'He.le.~~, tdtS77;.412-Q711 • Billings, MT 80~-735-4489 • Casper, WY 888-235-0515 LABORATORIES Anllytit;al Ex~UBIICa Sines 1852 ~~a;il _:JmI!~~/wk:8&6.J86-n15 • Ra~id City, Sf} 88B-672-1225 • College Statinn, TX 888-690-2218 Client: Denison Mines USA Corp Project: 1 st Quarter Nitrate 2012 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 04/09/12 Report Date: 01/23/12 Work Order: C12010435 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E353.2 Batch: R155395 Sample 10: MBLK-1 Method Blank Run: TECHNICON_120116A 01/16/12 12:44 Nitrogen, Nitrate+Nitrite as N NO mg/L 0.10 Sample 10: LCS-2 Laboratory Control Sample Run: TECHNICON_120116A 01/16/1212:47 Nitrogen, Nitrate+Nitrite as N 2.44 mg/L 0.10 98 90 110 Sample 10: LFB-3 Laboratory Fortified Blank Run: TECHNICON_120116A 01/16/1212:49 Nitrogen, Nitrate+Nitrite as N 1.96 mg/L 0.10 100 90 110 Sample 10: C12010435-002BMS Sample Matrix Spike, Run: TECHNICON_120116A 01/16/1213:29 Nitrogen, Nitrate+Nitrite as N 2.22 mg/L 0.10 105 90 110 Sample 10: C12010435-002BMSO Sample Matrix Spike Duplicate Run: TECHNICON_120116A 01/16/12 13:32 Nitrogen, Nitrate+Nitrite as N 2.26 mg/L 0.10 107 90 110 1.8 10 Sample 10: C12010435-012BMS Sample Matrix Spike Run: TECHNICON_120116A 01/16/12 14:07 Nitrogen, Nitrate+Nitrite as N 3.20 mg/L 0.10 106 90 110 Sample 10: C12010435-012BMSO Sample Matrix Spike Duplicate Run: TECHNICON_120116A 01/16/1214:09 Nitrogen, Nitrate+Nitrite as N 3.15 mg/L 0.10 103 90 110 1.6 10 Method: E353.2 Batch: R155429 Sample 10: MBLK-1 Method Blank Run: TECHNICON_120117A 01/17/1212:19 Nitrogen, Nitrate+Nitrite as N NO mg/L 0.10 Sample 10: LCS-2 Laboratory Control Sample Run: TECHNICON_120117A 01/17/1212:22 Nitrogen, Nitrate+Nitrite as N 2.55 mg/L 0.10 102 90 110 Sample 10: LFB-3 Laboratory Fortified Blank Run: TECHNICON_120117A 01/17/1212:24 Nitrogen, Nitrate+Nitrite as N 2.00 mg/L 0.10 102 90 110 Sample 10: C12010435-027BMS Sample Matrix Spike Run: TECHNICON_120117A 01/17/1213:04 Nitrogen, Nitrate+Nitrite as N 2.05 mg/L 0.10 105 90 110 Sample 10: C12010435-027BMSO Sample Matrix Spike Duplicate Run: TECHNICON_120117A 01/17/1213:07 Nitrogen, Nitrate+Nitrite as N 2.10 mg/L 0.10 107 90 110 2.4 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 13 of 17 ~1'" www.energylab.com ~ Analytical ExcsJlsncs Sincs 1852 . . .' "~elena, Mi 817-472 .. 0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~_c. ~1~~e!.'ffY .8Q$-6..B6-1175 • Rapid City, SD888-672-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 11II11111 ~IIIIIIIIII ~IIIIII ~II ~IIIIIII C12010435 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 1/13/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes D Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 2.4<C Yes D Yes 0' Date Received: 1/13/2012 Received by: em Carrier FedEx name: No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0' No VOA vials submitted 0' Not Applicable D Page 14 of 17 -u ' Q.) co CD 01 o .-"--lo. !---.J Chain of Custody and Analytical Request Record Page ---L of ~ cU;{i,ev MM':l.»Z'Z.jil1.. . ., -PLEASE PRINT (Provide as much information as possible.) Company Name: D' fA t Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: enl~OI\ lr"GS I!)I Q~"t"k NA·r~(; 'ZOl:l. State: \A'"\ Yes t;)?J No 0 Report Mail Address: 'PD BCJX 309 Contact Na~e: Phone/Fax: Email: Sampler: (Please Print) '[)l~r1d~t1q iA\ 84511 ~t\,,~r Ho H;j~ 4~:5 67~ ZZ2J ~"ne:r ~oH;J(;l'l Invoice Address: """'-J Invoice Contact & Pnone: Purchase Order: . Quote/Bottle Order: ~rv\e.. D~\J';c\ 'u.rl< ~\:.\~ b78 ;2:l~\ Special Report/Formats: $: &GfI&[b W@O@ OO~®QD~@1J~@ .. Contact ELI prior to . Shipped}Y~ _ / ,/ 1/ o ..... RUSH sample submittal I---=---:-~~' ~'tJI.:...!!:!Iou.et~r-J ~ 0 en 1? _ for charges and Cooler10(s): ~ en;g 01 ~ Cl ~ R scheduling -See ~. '-> 0 >-ro I-j D OW 0 EDD/EDT . ~CI)~ ~ $: ~ W --Instruction Page ,tl1· (ElectroOic Data) 0::;... -en ...... ~ " I "0 R • T O ::> '0 co •.• n -, 'c Ct· eC81p-t emp POTWMlWTP Format-U «enl.Q ·£ f) "-' ~ U ommen s. ol ,. / O D · '0 ... C:OI~ N\ « e '....., 0 C State: LEVEL IV ... ~'* § (§ \' ..... ~ .... o Other: 0 NELAC ~~I~' \j ~ :; On Ice: &,IN :::J (I).: Q) 3: .u. I-5 z -a «I arc -'tt W "E Custody Seal A ~ >1 ~ W ~ On Bottle o· l'V en .-r (j) ~ On Cooler , N. 1------------.-----. --r----. -+-------1 ~ ti5 H Intact Y. N SAMPLE IDENTIFICATION Collection Collection MATRIX 0 Signature (Name. Location, Interval. etc.) Date Time Match Y N 1 tWN --O~ 1\ l··q-\~ loJ..b :J-.-W rx I~ 2 Tv.J.AJ -~ l' \-\()-\':l ()71S ~-W "t I~ 3 TwJJ-)'7 R \-U .. t2 0'710 ~-vJ '} i~ 4 TwN "Ol> ,\;<\--l;l.. \05:2. ;)....-\J '1 ~ 5 JwN-)3 1\-<-1-1:2.. \':J-D7 ~-W I) ~ 6 JwfJ -)0 \-\O-t:t Ob~O ~-vJ "! ~" 7 J\NAJ-DE:, \-q·-l:l. ,~ ·;L-W ''I I~ 8TWN~O\ \ .. q-\:t )YO'7 ;L-vJ I~ ~i&'o/tiV3r i 9~AJ_ Ot..t '-~'''\2 l~S~ ;;..-w I~~ I~ 10 TWA) .. ):1. 1-tO ·I:L. 074 t ;;..,-'tJ ~r\ I~ Custody Relinquished by (print): DalelTime: Sip~tlJ'7 .... / ~ Received by (print): Date/Time: Signature: R n-MnGl »~\I;1.\l \ fl.v~OI~ HD() '"-__ tL/ttC~_ .1.L_.h~ ecord Relinquished by (print): (J DatelTime: Signature: 'J Received by (print): DatelTime: Signature: MUST be ; • rteCGlvea DY La ~ &$ DatelTlm1 / J 3. / . /.Ii . ~ 71gnature: Signed Sample Disposal: Return to Client: Lab Disposal: "( h7'l~r/.,J;'l / I \ Y Icl / {/. iff In certain circumstances. samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links. "U Q) CO CD ~ (j) o --.....J l;{g;{({"y Chain of Custody and Analytical Request Record Page 2.,. of~ a';7.»z".»»aw PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sam pie Origin EPA/State Compliance: State: Yes 0 No 0 Report Mail Address: S fA h1f'/ Contact N't) Phone/Fax: ) Email: Sampler: (Please Print) fA .~ ~ '/AI1~ Invoice Address: ~V'V -...... l'1Tlvoice Cor tact ~Pfione Purchase Order: Quote/Bottle Order: " Special ReporUFormats: ~ ~&[b W@O® OO§@@~~[]) .. Contact ELI prior to ~2~/ 0 Q; RUSH sample submittal ~ooler1l:jfsf. ...,. ~OU'J..£::. ~ for charges and ~CD~OI ~ Q <{ R scheduling -See ~~,,#/ ._> 0 >.1tj 1:: w t:, Instruction Page D OW 0 EOO/EDT(Electronic Data) ~ CJ) CJ) (IJ :s: C en (f.) J: 035:= ~ 0> ~ "C Receipt Temp o POlWMlWTP Format: () c: Comments: ~«~1.2 ~ :::l U ~c,/ °c « 0 D State: D LEVEL IV o ..... COI c: Co l... Q:j~ c: 0i:: \j I-~ o..tO.2 0 E o Other: D NELAC l-On Ice: 61N E~I(tj • « :::l ::J <D-~ 1D ~ ~ l-S ZCi«I~o W 12 Custody Seal (f( ~ >1 ~ W ro 00 __ {) (J) "C On Cooler Y N CJ) c: J ro ...... H Intact Y N SAMPLE IDENTIFICATION Collection Collection C/) MATRIX Signature N (Name, Location, Interval, etc.) Date Time Match 1 tw.A) ... lS '" l .. lt-l~ o~~y :;;t.-\J ~ 2 . ':J.-vJ \. ~ "-WN -Ob \~lO"'~ O'Ul 3 TWM-it )-iQ-iJ.. lDD3 :l. -vJ '\, (Q) nnn 4 "TwN -t8 :2-vJ \,1 ~ \-l()-i~ 105:1.. I~ 5 :l-W \. lo;;;::J TWN-07 \-H .\~ O~L..\4 ~ 6 lWAJ _ \b \-iO-I:t )2.~b ~-W ~ ~ 7 nJN-14 OQE>5 ~-W .. ~ I~ , .. H-i.:l 8 "TWIJ "'lQ 11-ID-l~ 141'1 2-vJ 'f 1~~~3) 9 Db5D ~:-vJ .~ :~ 1\VN-,"7 \"\2-\2-I~ 10 TwAl-09 l-p--l2 0,00 2-YJ ~ Id Custody Relinquished \\:rint): DatelTime: . '-\11.\hs:n1rl~~ Received by (print): DatelTime: Signature: -k1\1\ (1 '\ I ~ d 4,..,\ \/iJ./~r~ \ tOll) Record RelinqUIshed by (print): U Date/Time: Signature: V Received by (print): Dateffime: Signature: ~ ./ MUST be Signed Sample Disposal: Return to Client: Lab Disposal: ( K9Cp:7 ~R/f D17J31L, / J' ff ""SIgnature: pies SUbmlttea to energy LaboratOries, Inc. may be SUbcontractea to otner certified laboratOries 11"1" oraer to camp This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. y q "'U Ol ' e CD -......J sa, -lo. -......J Chain of Custody and Analytical Request Record Pagelofl '«gm{tfty .. m.'~JI1I1.»»a. PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: State: Yes 0 No 0 I Report Mail Address: ~r~n1C Contact Nam~ Phone/Fax: /, Email: Sampler: (Please Print) A S J G~q e" -=f-.. Invoice Address: --Invoice Contact & Ph~j Purchase Order: Quote/Bottle Order: Special Report/Formats: s: £[}!]&[b W®O® 1M~@l!D~®lJ~@ .. Contact ELI prior to ~ Cl "-RUSH sample submittal ~o (/)jg ~ R for charges and 960ler ID(sr r ~CO~OI (fi 0 « scheduling -See (~ltI'41 ._> 0 >'ro \' w C I nstruction Page Dow o EOO/EOT(Electronic Data) .!9C/)Wn:'ls: c ~(/) I os::=: ~ 0> ~ "0 Rq1ytP 0c o POTWIWWTP Format: u 0o.s () c: Comments: ::J U o«~Iii:iI~ « e D State: D LEVEL IV .... Q).$ c: .;:: \) I-m ~ ~ o.n:'Il:8 0 c D Other: D NELAC ~n:'I · I-~ On Ice: U/N ~ <I,).!:::: Q) 3: ~ <t l-S zo..<l~o ~ W 'E Custody Seal (;J' ~ >1 W co 00 Bo"'. 6 (J) "0 On Cooler N C/) ~ c: ro U5 H Intact Y N SAMPLE I DENTI FICATION Collection Collection MATRIX a Signature N JName, Location, Interval, etc.) Date Time Match 1 -rvJt\J~ 03 \-\2-~ DitO :2-W Y. ~ 2 TwN-O~ \-\:2--\~ Ottg ~-W y. ~ 3 P\'C-z-01 \~ \1-lJ. ,~l{,", :J..-W 'f.. g nnn 4 Plc'Z.-o~ \-U-l:2 \~S ::;..-vJ ~ W) ~ 5 Pi e.:z..-D :> \.~ \t-t~ 1~() :;"-'W "" ~ ~ 6 U. \A)L 'P ) .. H-l~ )2'3,1..\ ~-v.J ~ ~ 7 IwtJ-bO \-\ \ .. ,?.. \~S6 :J.-W 1-~ , 8 TW.N-b.S ·~-\O'·l;t Ob36 :;..-w ~ I~ 9IWN-7D '\-10 .. \J. 'O()~ ?--w ~ ~ WtVO/tJ18 .r 10 -t:ih? D Ah1AA'~ c::::~ Custody ~';;:;edW:\\71Vw~ l/t~:~i;: l\o() __ ~SiJJ. ,/ld-'7 Received by (print): DaterTime: Signa1ure: Record Relinquished by (print): U DatelTime: Signature: V Received by (print): Date/Time: Signature: MUST be . ~ J' Signed Sample Disposal: Return to Client: Lab Disposal: KececZ?~~;!te/llme: Ij;..:i ~ /tf,jtJignature: In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. TabH Quality Assurance and Data Validation Tables H-1 Field Data QAJQC Evaluation : ,volume :;'Wiii: ,~~ , 1" ''', ~";;:;" I~' , ~ '. ",; ~'JiIffl "" '!<i " iJi}t~~" Ill;!: ~,'-ii J',.",~ 'i ~¥'~~ ~ , , ,I~~RP:Q " Ji~ RPIil .. " 'fenm~ "L:'" , ~ Redox Pot~nti Location " 2x Casing Volume Pumped Volume Check "~<:~~0nductiv.ity'<,, ~ if 'j)1!~ "" IQlD ~, '_'"~ , rJi'urlJidity _~" 11 R~ll- Piezometer 1 --2155.0 NC 7.79 NC 11.82 NC 275 NC 3.6 NC Piezometer 2 --532.9 NC 8.97 NC 11.70 NC 172 NC 8.7 NC Piezometer 3 --3071.0 NC 11.88 NC 10.40 NC 193 NC 17.1 NC TWN-1 39.58 79.16 88.00 OK 838.0 838.0 0.00 7.18 7.19 0.14 14.60 14.60 0.00 284 282 0.71 141.0 142.0 0.71 TWN-2 48.08' 96.16 ' 55.00 Pumped pry 2667.0 NC 6.40 NC , 13.84 , 'NC 296 ':i NC .. 11.6 NC TWN-3 ~ 41.08 82.16 39.00 Pumped,Dry 2268.0 NC ' 6.65 . Nt ' 13.49 0, NC 279' " NC 100.0 , NC i" TWN-4 55.83 111.66 132.00 OK 1018.0 1019.0 0.10 7.00 7.00 0.00 14.28 14.28 0.00 271 271 0.00 290.0 295.0 1.71 TWN-5 52.43 104.86 110.00 OK 3071.0 3072.0 0.03 6.66 6.67 0.15 14.49 14.49 0.00 305 303 0.66 2.9 2,9 0.00 TWN-6 35.71 71.42 77.00 OK 1573.0 1568.0 0.32 6.74 6.75 0.15 14.34 14.33 0.07 349 348 0.29 19.0 18.0 5.41 TWN-7 10.7 21.40 -'8:00 Pumped Dry 1164.0 NC 6.91 ' NC '13.77 ' , NC ' 347 ' NC-18.5 0 NC ' TWN-8 54.72 109.44 121.00 OK 2369.0 2399.0 1.26 7.24 7.22 0.28 14.29 14.29 0.00 159 159 0.00 2.4 2.4 NC TWl'f~9 22.16 .," 44.32 22.00 ' Pumped Dry 2286.0 NC 6.50 NC '13.73 NC \' , 325 NC 36.1 'NC TWN-lO ' 15.65 3i.30 16.50 Pumped Dry 2687.0 NC 3.62 NC 13.69 NC 471 " ";, 'NC ' 166.0 ' NC ,- TWN-11 46.82 93.64 110.00 OK 2650.0 2650.0 0.00 6.53 6.53 0.00 13.43 13.41 0.15 300 298 0.67 2.1 2.1 0.00 TWN-12 52.81 105.62 121.00 OK 2458.0 2454.0 0.16 6.99 6.98 0.14 13.87 13.87 0.00 264 258 2.30 i51.0 153.0 1.32 TWN-13 48.19 96.38 110.00 OK 1223.0 1230.0 0.57 7.65 7.66 0.13 14.38 14.38 0.00 208 207 0.48 59.0 ,-60.0 1.68 TWN-14 46.78 , ~93,.56 44.00 Pumped Dry 999.7 ' NC 7.51 NC 14:12 NC 313 NC II 56.1 NC TWN-15 40.62 81.24 48.06 PuinpedDiy -i401.0 NC ," 6.76 NC 14.04 NC 376 ''', NC , '33.1 NC TWN-16 33.62 67.24 77.00 OK 1765.0 1739.0 1.48 6.87 6.87 0.00 14.80 14.80 0.00 330 330 0.00 ,J2.1 ", I 12.i 0.00 TWN-f7 , 49.36 ,98.72 53:00 Pumped Dry , 1127;0 NC < ' 7.17 ' NC 14.07 NC ',"; 327 NC 79~1 ~ NC TWN-18 56.91 113.82 121.00 OK 2179.0 2182.0 0.14 6.76 6.76 0.00 14.17 14.17 0.00 312 312 0.00 105.0-106.01f 0.95 TWN-19 37.49 74.98 77.00 OK 1970.0 1972.0 0.10 7.14 7.13 0.14 14.50 14.51 0.07 325 325 0.00 2.8 2.8 0.00 ~p 7f:"" III ',' --, ,W"" 248.0 . Ne ll g,.1g ~ NC I~ 5.48 ", ~ • NC 244 J '" NC 2.5 .,;,,"'! ; NC Ill! ,7 Piezometers 1, 2, and 3, were not ]Ju~ped, only one set of parameter~ were taken. " , , . ' 'TWN-2, TwN-3, TWN-7, TWN-:9, TWN-14, TWN-15, and TWN-17 were purged to dryness befor~2 casing volumes were'removed. TWN-10 waspurged to dryness after 2 casing volumes Iwere rem'oved. -" , ' , , ' ' The QA-'R states that tnrbidity should be less than 5 Ne,helometric Turbidity Units (''NTU'') prior to sampling unless the well is characterized by water that has a higher turbidity. 'The QAP does not require that turbidit s~ling. As such, the noted observations regarding turbidity measUrements less than 5 NTU below are included for information oses oIlI . H-2: Holding Time Evaluation ~~"'I:~> ~ W., '. I" .} .' 'ih,il~ Analys .. Im~< ,. Data ~Ii"t~. =. J-ocati6Q: _i/j ,,~ Uon~titti ,;.. , >$a t~ Piezometer 01 Chloride ' 1111112 1117/12 6.00 days 28 days OK Piezometer 01 Nitrogen 1111112 1117/12 6.00 days 28 days OK Piezometer 02 Chloride 1111112 1117112 6.00 days 28 days OK Piezometer 02 Nitrogen 1111112 1117112 6.00 days 28 days OK Piezometer 03 Chloride 1111112 1117112 6.00 days 28 days OK Piezometer 03 Nitrogen 1111112 1117112 6.00 days 28 days OK TWN-01 Chloride 119/12 1117112 8.00 days 28 days OK TWN-01 Nitrogen 119112 1116/12 7.00 days 28 days OK TWN-02 Chloride 1112112 1117/12 5.00 days 28 days OK TWN-02 Nitrogen 1112/12 1117/12 5.00 days 28 days OK TWN-03 Chloride 1112/12 1117/12 5.00 days 28 days OK TWN-03 Nitrogen 1112/12 1117112 5.00 days 28 days OK TWN-04 Chloride 119112 1117112 8.00 days 28 days OK TWN-04 Nitrogen 119/12 1116112 7.00 days 28 days OK TWN-05 Chloride 119/12 1117/12 8.00 days 28 days OK TWN-05 Nitrogen 119112 1116/12 7.00 days 28 days OK TWN-06 Chloride 1110/12 1117/12 7.00 days 28 days OK TWN-06 Nitrogen 1110/12 1116112 6.00 days 28 days OK TWN-07 Chloride 1111112 1117112 6.00 days 28 days OK TWN-07 Nitrogen 1111112 1116/12 5.00 days 28 days OK TWN-08 Chloride 119/12 1117/12 8.00 days 28 days OK TWN-08 Nitrogen 119112 1116/12 7.00 days 28 days OK TWN-09 Chloride 1112/12 1117/12 5.00 days 28 days OK TWN-09 Nitrogen 1112/12 1117/12 5.00 days 28 days OK TWN-10 Chloride 1110112 1117112 7.00 days 28 days OK TWN-10 Nitrogen 1110112 1116/12 6.00 days 28 days OK TWN-11 Chloride 1110112 1117/12 7.00 days 28 days OK TWN-11 Nitrogen 1110/12 1116/12 6.00 days 28 days OK TWN-12 Chloride 1110/12 1117/12 7.00 days 28 days OK TWN-12 Nitrogen 1110/12 1116/12 6.00 days 28 days OK TWN-13 Chloride 119112 1117112 8.00 days 28 days OK TWN-13 Nitrogen 119/12 1116112 7.00 days 28 days OK TWN-14 Chloride 1111112 1117112 6.00 days 28 days OK TWN-14 Nitrogen 1111112 1116/12 5.00 days 28 days OK TWN-15 Chloride 1111112 1117/12 6.00 days 28 days OK TWN-15 Nitrogen 1111112 1116/12 5.00 days 28 days OK TWN-16 Chloride 1110112 1117112 7.00 days 28 days OK TWN-16 Nitrogen 1110112 1116112 6.00 days 28 days OK TWN-17 Chloride 1112/12 1117/12 5.00 days 28 days OK TWN-17 Nitrogen 1112/12 1117/12 5.00 days 28 days OK TWN-18 Chloride 1110112 1117/12 7.00 days 28 days OK TWN-18 Nitrogen 1110112 1116/12 6.00 days 28 days OK TWN-19 Chloride 1110112 1117112 7.00 days 28 days OK TWN-19 Nitrogen 1110112 1117112 7.00 days 28 days OK TWN-65 Chloride 1110/12 1117/12 7.00 days 28 days OK TWN-65 Nitrogen 1110/12 1117/12 7.00 days 28 days OK UWLP Chloride 1111112 1117112 6.00 days 28 days OK UWLP Nitrogen 1111112 1117112 6.00 days 28 days OK TWN-70 Chloride 1110112 1117112 7.00 days 28 days OK TWN-70 Nitrogen 1110/12 1117/12 7.00 days 28 days OK H-3: Analytical Method Check A4500-CI B A4500-CI B Both Nitrate and Chloride were analyzed with the correct analytical method. H-4: Reporting Limit Evaluation ~.I' Flt.~~. ab~R~pfi) g?' kepoFtift OJ I~ ~:~ Co ",lam.p)i 'f;-~ .Jlkilnil" . K ~it Piezometer 01 Chloride 78 mg/L 1 mg/L 1 mg/L Piezometer 01 Nitrogen 7.1 mg/L 0.5 mg/L 0.1 mg/L D Piezometer 02 Chloride 9 mg/L 1 mg/L 1 mg/L Piezometer 02 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L Piezometer 03 Chloride 20 mg/L 1 mg/L 1 mg/L Piezometer 03 Nitrogen 1.8 mg/L 0.1 mg/L 0.1 mg/L TWN-Ol Chloride 15 mg/L 1 mg/L 1 mg/L TWN-Ol Nitrogen 0.6 mg/L 0.1 mg/L 0.1 mg/L TWN-02 Chloride 86 mg/L 1 mg/L 1 mg/L TWN-02 Nitrogen 31 mg/L 2 mg/L 0.1 mg/L D TWN-03 Chloride 143 mg/L 1 mg/L 1 mg/L TWN-03 Nitrogen 25 mg/L 2 mg/L 0.1 mg/L D TWN-04 Chloride 20 mg/L 1 mg/L 1 mg/L TWN-04 Nitrogen 0.9 mg/L 0.1 mg/L 0.1 mg/L TWN-05 Chloride 45 mg/L 1 mg/L 1 mg/L TWN-05 Nitrogen 0.2 mg/L 0.1 mg/L 0.1 mg/L TWN-06 Chloride 20 mg/L 1 mg/L 1 mg/L TWN-06 Nitrogen 1.2 mg/L 0.1 mg/L 0.1 mg/L TWN-07 Chloride 5 mg/L 1 mg/L 1 mg/L TWN-07 Nitrogen 2.3 mg/L 0.1 mg/L 0.1 mg/L TWN-08 Chloride 11 mg/L 1 mg/L 1 mg/L TWN-08 Nitrogen o mg/L 0.1 mg/L 0.1 mg/L U TWN-09 Chloride 202 mg/L 1 mg/L 1 mg/L TWN-09 Nitrogen 12.2 mg/L 0.5 mg/L 0.1 mg/L D TWN-I0 Chloride 44 mg/L 1 mg/L 1 mg/L TWN-I0 Nitrogen 0.8 mg/L 0.1 mg/L 0.1 mg/L TWN-ll Chloride 69 mg/L 1 mg/L 1 mg/L TWN-ll Nitrogen 1.6 mg/L 0.1 mg/L 0.1 mg/L TWN-12 Chloride 104 mg/L 1 mg/L 1 mg/L TWN-12 Nitrogen 0.9 mg/L 0.1 mg/L 0.1 mg/L TWN-13 Chloride 46 mg/L 1 mg/L 1 mg/L TWN-13 Nitrogen o mg/L 0.1 mg/L 0.1 mg/L U TWN-14 Chloride 26 mg/L 1 mg/L 1 mg/L TWN-14 Nitrogen 3.5 mg/L 0.1 mg/L 0.1 mg/L TWN-15 Chloride 38 mg/L 1 mg/L 1 mg/L TWN-15 Nitrogen 1.5 mg/L 0.1 mg/L 0.1 mg/L TWN-16 Chloride 33 mg/L 1 mg/L 1 mg/L TWN-16 Nitrogen 2.8 mg/L 0.1 mg/L 0.1 mg/L TWN-17 Chloride 79 mg/L 1 mg/L 1 mg/L TWN-17 Nitrogen 8.7 mg/L 0.5 mg/L 0.1 mg/L D TWN-18 Chloride 64 mg/L 1 mg/L 1 mg/L TWN-18 Nitrogen 1.9 mg/L 0.1 mg/L 0.1 mg/L TWN,.19 Chloride 114 mg/L 1 mg/L 1 mg/L TWN-19 Nitrogen 7 mg/L 0.5 mg/L 0.1 mg/L D TWN-65 Chloride 40 mg/L 1 mg/L 1 mg/L TWN-65 Nitrogen 0.7 mg/L 0.1 mg/L 0.1 mg/L UWLP Chloride 2 mg/L 1 mg/L 1 mg/L UWLP Nitrogen o mg/L 0.1 mg/L 0.1 mg/L U TWN-70 Chloride 74 mg/L 1 mg/L 1 mg/L TWN-70 Nitrogen 1.6 mg/L 0.1 mg/L 0.1 mg/L U = Analyte was not detected at the RL D = RL was increased due to sample matrix or required dilution due to the sample concentration. In all cases the analytical results were greater than the reporting limit used. CI20I0435 Piezometer I,Piezometer 2, Piezometer 3, TWN-I,TWN-2, TWN-3,TWN-4,TWN-5,TWN-6,TWN-7,TWN-8,TWN-8R, TWN-9,TWN-I0, TWN-ll ,TWN-12,TWN-12R,TWN-13, TWN-14,TWN-15,TWN-16, TWN-17,TWN-17R TWN-18, TWN-19, TWN-60,TWN-65,TWN-70,UWLP H -8 Rinsate Evaluation Previous Rinsate Sample Parameter Rinsate Result Well Sample TWN-8R Nitrogen ND mglL N/A TWN-8R Chloride ND mglL N/A TWN-12R Nitrogen 0.2 mglL TWN-04 TWN-12R Chloride ND mglL TWN-04 TWN-17R Nitrogen ND mglL TWN-19 TWN-17R Chloride ND mglL TWN-19 TWN-60 Nitrogen ND mglL Piez-01 TWN-60 Chloride ND mglL Piez-01 The Rmsate sample IdentIfied m Column 1 was collected after the pump was used to purge the well identified as "Previous Well Sampled" in Column 4 D = Reporting limit raised due to dilution/sample matrix. Reporting Result for Well Qualifier Limit NA 0.1 mglL NA 1mgIL 0.9 mglL 0.1 mglL 20 mglL 1mgIL 7 mglL D 0.1 mglL 114 mglL 1mgIL 7.1 mglL D 0.1 mglL 78 mglL 1mgIL Tab I Kriged Current Quarter Isoconcentration Maps NS = not sampled; ND = not detected '-10 l1li MW-4 .4.8 TW4-1 0 6.8 TWN-1 0 0.6 PIEZ-1 ~ 7.1 TW4-27 ~24 kriged nitrate isocon and label kriged nitrate isocon and label (extent uncertain) perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched monitoring well installed October 2011 showing concentration in mg/L HYDRO GEO CHEM, INC. KRIGED 1st QUARTER, 2012 NITRATE (mg/L) (NITRATE + NITRITE AS N) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H :/718000/may12/nitrate/Unt0312c2.srf I-I NS = not sampled; NO = not detected MW-4 .41 TW4-1 0 38 TWN-1 ~15 PIEZ-1 'ii) 78 TW4-27 ~ 11 perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched monitoring well installed October, 2011 showing concentration in mg/L HYDRO GEO CHEM, INC. KRIGED 1 st QUARTER, 2012 CHLORIDE (mg/L) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/may121chloride/Ucl0312.srf I-2 TabJ Analyte Concentrations Over Time TWN-l Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 0.7 19 7/21/2009 0.4 17 9/21/2009 0.4 19 10/28/2009 0.5 18 3/17/2010 0.5 17 5/26/2010 0.6 20 9/27/2010 0.6 19 12/7/2010 0.6 14 1/26/2011 0.5 17 4/20/2011 0.5 19 7/26/2011 0.5 14 10/17/2011 0.5 10 1/9/2012 0.6 15 TWN-2 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 25.4 29 7/21/2009 25 25 9/21/2009 22.6 17 11/2/2009 20.8 55 3/24/2010 62.1 85 6/2/2010 69 97 9/29/2010 69 104 12/9/2010 48 93 2/1/2011 43 93 4/28/2011 40 85 7/28/2011 33 74 10/20/2011 33 76 1/12/2012 31 86 TWN-3 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 23.6 96 7/21/2009 25.3 96 9/21/2009 27.1 99 11/2/2009 29 106 3/25/2010 25.3 111 6/3/2010 26 118 7/15/2010 27 106 12/10/2010 24 117 2/1/2011 24 138 4/28/2011 26 128 7/29/2011 25 134 10/20/2011 25 129 1/12/2012 25 143 TWN-4 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 1 13 7/21/2009 0.05 12 9/21/2009 0.4 13 10/28/2009 0.4 11 3/16/2010 0.9 22 5/27/2010 1.0 22 9/27/2010 0.9 19 12/8/2010 1 21 1/25/2011 0.9 21 4/20/2011 0.9 21 7/26/2011 1.1 35 10/18/2011 0.9 20 1/9/2012 0.9 20 TWN-5 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 0.22 42 9/21/2009 0.5 45 11/10/2009 0.2 48 3/16/2010 0.3 43 5/26/2010 0.3 44 7/12/2010 0.3 43 12/7/2010 0.3 45 1/25/2011 0.4 47 4/20/2011 0.3 44 7/26/2011 0.3 44 10/17/2011 0.3 45 1/9/2012 0.2 45 TWN-6 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 3.2 32 9/22/2009 1.6 13 11/3/2009 1.4 21 3/23/2010 1.5 19 6/1/2010 1.4 22 7/13/2010 1.4 73 12/8/2010 1.2 21 1/26/2011 1.1 18 4/20/2011 1.5 22 7/27/2011 1.1 17 10/18/2011 1.4 21 1/10/2012 1.2 20 TWN-7 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 ND 11 9/21/2009 ND 7 11/10/2009 0.1 7 3/17/2010 0.8 6 5/28/2010 1.2 6 7/14/2010 1.6 7 12/10/2010 1 4 1/27/2011 1.3 6 4/21/2011 1.7 6 7/29/2011 0.7 5 10/19/2011 2.2 6 1/11/2012 2.3 5 TWN-8 Date Nitrate (mg/I) Chloride (mg/I) Notes 8/25/2009 0 11 Nitrate is ND 9/21/2009 0 12 Nitrate is ND 11/10/2009 0 12 Nitrate is ND 3/16/2010 0 11 Nitrate is ND 5/26/2010 0 11 Nitrate is N D 7/12/2010 0 11 Nitrate is N D 12/6/2010 0 9 Nitrate is ND 1/25/2011 0 13 Nitrate is ND 4/18/2011 0 10 Nitrate is ND 7/26/2011 0 18 Nitrate is ND 10/17/2011 0 10 Nitrate is N D 1/9/2012 0 11 Nitrate is ND TWN-9 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 9.3 169 9/22/2009 8.9 201 11/10/2009 12 205 3/23/2010 7.6 183 6/1/2010 7.6 175 7/15/2010 10.7 210 12/9/2010 8 172 2/1/2011 9.5 217 4/28/2011 10 192 7/29/2011 11 208 10/20/2011 10.9 134 1/12/2012 12.2 202 TWN-l0 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 1.1 19 9/22/2009 1.6 35 11/10/2009 1.4 26 3/23/2010 1.5 54 6/4/2010 1 30 7/14/2010 0.2 21 12/8/2010 1.3 28 1/27/2011 0.3 40 4/21/2011 1.2 28 7/27/2011 0.1 28 10/18/2011 0.2 33 1/10/2012 0.8 44 TWN-ll Date Nitrate (mg/I) Chloride (mg/I) 11/3/2009 1.3 74 3/17/2010 1.4 73 6/4/2010 1.3 72 9/27/2010 1.4 76 12/8/2010 1.4 72 1/27/2011 1.4 84 4/26/2011 1.4 76 7/27/2011 0.1 76 10/17/2011 1.6 76 1/10/2012 1.6 69 TWN-12 Date Nitrate (mg/I) Chloride (mg/I) 11/3/2009 0.5 109 3/17/2010 0.7 113 5/26/2010 0.8 106 7/12/2010 0.7 112 12/7/2010 0.7 103 1/26/2011 4.2 87 4/26/2011 1 109 7/26/2011 0.6 102 10/17/2011 1.2 87 1/10/2012 0.9 104 TWN-13 Date Nitrate (mg/I) Chloride (mg/I) Notes 11/4/2009 0.5 83 3/17/2010 0 47 Nitrate ND 5/26/2010 0.1 49 9/27/2010 0.2 53 12/7/2010 0.4 57 1/25/2011 1.6 103 4/26/2011 0 49 Nitrate ND 7/26/2011 0.1 49 10/17/2011 0 48 Nitrate ND 1/9/2012 0 46 Nitrate ND TWN-14 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 3.4 32 3/24/2010 2.9 24 6/2/2010 2.9 30 7/15/2010 3.5 26 12/10/2010 4.2 28 1/28/2011 3.7 24 4/27/2011 3.5 30 7/29/2011 3.5 25 10/19/2011 3.9 27 1/11/2012 3.5 26 TWN-15 Date Nitrate (mg/I) Chloride (mg/I) 11/10/2009 1.1 78 3/18/2010 0.7 43 5/28/2010 1.0 39 7/13/2010 1.0 36 12/9/2010 1.2 38 1/27/2011 1.4 43 4/27/2011 1.6 49 7/28/2011 1.6 47 10/19/2011 1.3 38 1/11/2012 1.5 38 TWN-16 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 1 39 3/17/2010 1.2 35 5/27/2010 0.2 35 9/27/2010 2.6 35 12/9/2010 2 30 1/27/2011 4.6 34 4/27/2011 1.6 39 7/27/2011 2.4 31 10/18/2011 2.6 34 1/10/2012 2.8 33 TWN-17 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 6.7 152 3/24/2010 10.4 78 6/3/2010 11 87 7/15/2010 8.9 66 12/10/2010 8 65 2/1/2011 8.6 90 4/28/2011 9 81 7/29/2011 8.5 74 10/20/2011 8.1 71 1/12/2012 8.7 79 TWN-18 Date Nitrate (mg/I) Chloride (mg/I) 11/2/2009 1.3 57 3/17/2010 1.6 42 6/1/2010 1.8 63 9/27/2010 1.8 64 12/9/2010 1.6 59 1/27/2011 1.4 61 4/26/2011 1.8 67 7/28/2011 1.8 65 10/18/2011 1.9 60 1/10/2012 1.9 64 TWN-19 Date Nitrate (mg/I) Chloride (mg/I) 11/2/2009 7.4 125 3/23/2010 7.2 118 6/1/2010 6.2 113 9/29/2010 7.2 113 12/9/2010 7 107 2/1/2011 7 114 4/28/2011 6.9 120 7/28/2011 7.1 113 10/18/2011 6.5 108 1/10/2012 7 114 Piezometer 1 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 6.8 NA 7/14/2009 6.8 60 9/22/2009 7.3 78 10/27/2009 7.4 61 6/2/2010 7.2 52 7/19/2010 6.8 52 12/10/2010 6.5 60 1/31/2011 7 60 4/25/2011 6.8 58 7/25/2011 7 53 10/19/2011 6.6 55 1/11/2012 7.1 78 Piezometer 2 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 0.5 NA 7/14/2009 0.5 7 9/22/2009 0.5 17 10/27/2009 0.6 7 6/2/2010 0.6 8 7/19/2010 0.6 8 12/10/2010 0.2 6 1/31/2011 0.3 9 4/25/2011 0.3 8 7/25/2011 0.1 9 10/19/2011 0.1 8 1/11/2012 0.1 9 Piezometer 3 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 0.7 NA 7/14/2009 0.8 12 9/22/2009 0.8 24 10/27/2009 1.2 19 3/24/2010 1.7 116 6/2/2010 1.6 36 7/19/2010 1.6 35 12/10/2010 1.8 25 1/31/2011 1.8 40 4/25/2011 1.7 35 7/25/2011 1.8 61 10/19/2011 1.7 12 1/11/2012 1.8 20 Piezometer 4 Date 7/14/2009 Nitrate (mg/I) Chloride (mg/I) 1.8 46 Piezometer 5 Date 7/14/2009 Nitrate (mg/I) 0.7 Chloride (mg/I) 18 MW-18 Date Nitrate (mg/I) Chloride (mg/I) 7/14/2009 ND 51 MW-19 Date Nitrate (mg/I) Chloride (mg/I) 7/14/2009 2.2 24 Upper Wildlife Pond Date Nitrate (mg/I) Chloride (mg/I) Note 9/22/2009 0 5 Nitrate ND 10/27/2009 0 3 Nitrate ND 6/2/2010 0 0 Nitrate and Chloride ND 7/19/2010 0 0 Nitrate and Chloride ND 12/10/2010 0 1 Nitrate ND 1/31/2011 0.1 1 4/25/2011 0 0 Nitrate and Chloride ND 7/25/2011 0 0 Nitrate and Chloride ND 10/19/2011 0 0 Nitrate and Chloride ND 1/11/2012 0 2 Nitrate ND Frog Pond Date 10/14/09 Nitrate (mg/I) o Chloride (mg/I) o Notes Nitrate ND TabK Concentration Trend Graphs fn c:: 0 ".;:::i ca :... ... c:: CI) (,) c:: 0 0 CI) ... ca :... 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(1) a. a. ::J o ~-Aell\J o ~-uer 60-PO I-------!-----+-----+----+------+-----+ 60-lnr L.{) C\I o 60-J\ON ~~ 60-PO 60-deS 60-des 60-5nV 60-lnr (j) co C\I o o o o tn c: o ~ CO 10. ... c: G> o c: o o G> "C ";: o .c: o "C c: o C- O') o 10. LL 0'> o co o ~~ o o 50-AON 50-l0Q 50-deS 50-deS 50-5nv TabL CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Tuesday, May 29, 2012 1 :38 PM 'rlundberg@utah.gov' 'Pgoble@utah.gov'; 'TRUSHING@utah.gov'; Ron Hochstein; David Frydenlund; Jo Ann Tischler; Harold Roberts; David Turk; N. Tanner Holliday; Garrin Palmer Transmittal of CSV Files White Mesa Mill 2012 Q1 Nitrate Monitoring C12010435_R1.csv Attached to this e-mail is an electronic copy of laboratory results for nitrate monitoring conducted at the White Mesa Mill during the first quarter of 2012, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel Denison Mines (USA) Corp. Quality Assurance Manager 1