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HomeMy WebLinkAboutDDW-2025-009370September 18, 2025 Dear John Steffan: Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 8/27/25 10:00 am and logged in under work order IH05123. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH15005RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IH05123-01 Name: Sampled: Received: 08/27/25 10:00 08/26/25 12:10 WS005-HIGHLANDS WELL #1 Reg ID:Drinking Water - Regular SampleMatrix:UTAH15005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA09/15/25 14:02 EJBU1.910.9 < 0.4 ng/L EPA 533PFMPA09/15/25 14:02 EJBU1.910.4 < 0.5 ng/L EPA 533PFPeA09/15/25 14:02 EJBU1.910.5 < 0.5 ng/L EPA 533PFBS09/15/25 14:02 EJBU1.910.5 < 0.4 ng/L EPA 533PFMBA09/15/25 14:02 EJBU1.910.4 < 0.5 ng/L EPA 533PFEESA09/15/25 14:02 EJBU1.910.5 < 0.3 ng/L EPA 533HFPO-DA 09/15/25 14:02 EJBU1.910.3 < 0.4 ng/L EPA 533NFDHA09/15/25 14:02 EJBU1.910.4 < 0.3 ng/L EPA 5334:2 FTS 09/15/25 14:02 EJBU1.910.3 < 0.4 ng/L EPA 533PFHxS09/15/25 14:02 EJBU1.910.4 < 0.5 ng/L EPA 533PFHpA09/15/25 14:02 EJBU1.910.5 < 1.0 ng/L EPA 533PFHxA09/15/25 14:02 EJBU1.911.0 < 0.5 ng/L EPA 533ADONA09/15/25 14:02 EJBU1.910.5 < 0.5 ng/L EPA 533PFPeS09/15/25 14:02 EJBU1.910.5 < 0.5 ng/L EPA 5336:2 FTS 09/15/25 14:02 EJBU1.910.5 < 0.7 ng/L EPA 533PFOA09/15/25 14:02 EJBU1.910.7 < 0.6 ng/L EPA 533PFHpS09/15/25 14:02 EJBU1.910.6 < 0.5 ng/L EPA 533PFOS09/15/25 14:02 EJBU1.910.5 < 0.5 ng/L EPA 533PFNA09/15/25 14:02 EJBU1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 09/15/25 14:02 EJBU1.910.6 < 0.5 ng/L EPA 5338:2 FTS 09/15/25 14:02 EJBU1.910.5 < 0.4 ng/L EPA 533PFDA09/15/25 14:02 EJBU1.910.4 < 0.5 ng/L EPA 533PFUnA09/15/25 14:02 EJBU1.910.5 < 0.5 ng/L EPA 53311Cl-PF3OUdS 09/15/25 14:02 EJBU1.910.5 < 0.5 ng/L EPA 533PFDoA09/15/25 14:02 EJBU1.910.5 Surrogate: 13C4-PFBA-SURR 93 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C5-PFPeA-SURR 97 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C3-PFBS-SURR 91 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C2-4:2FTS-SURR 90 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C5-PFHxA-SURR 88 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 91 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C4-PFHpA-SURR 88 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C3-PFHxS-SURR 90 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C2-6:2FTS-SURR 83 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C8-PFOA-SURR 84 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C9-PFNA-SURR 82 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C8-PFOS-SURR 91 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C2-8:2FTS-SURR 91 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C6-PFDA-SURR 77 %50-200 09/15/25 14:02 EJB EPA 533 Surrogate: 13C7-PFUnA-SURR 72 %50-200 09/15/25 14:02 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IH05123-01 Name: Sampled: Received: 08/27/25 10:00 08/26/25 12:10 WS005-HIGHLANDS WELL #1 Reg ID:Drinking Water - Regular SampleMatrix:UTAH15005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 75 %50-200 09/15/25 14:02 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B541534 - EPA 533 - EPA 533 Blank (B541534-BLK1)Prepared: 08/28/25 Analyzed: 09/15/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 40.8 ng/L 40.00 102 50-200 Surrogate: 13C5-PFPeA-SURR 48.1 ng/L 40.00 120 50-200 Surrogate: 13C3-PFBS-SURR 38.9 ng/L 37.28 104 50-200 Surrogate: 13C2-4:2FTS-SURR 181 ng/L 150.4 121 50-200 Surrogate: 13C5-PFHxA-SURR 38.6 ng/L 40.00 97 50-200 Surrogate: 13C3-HFPOA-DA-SURR 38.9 ng/L 40.00 97 50-200 Surrogate: 13C4-PFHpA-SURR 39.0 ng/L 40.00 97 50-200 Surrogate: 13C3-PFHxS-SURR 37.6 ng/L 37.92 99 50-200 Surrogate: 13C2-6:2FTS-SURR 172 ng/L 152.0 113 50-200 Surrogate: 13C8-PFOA-SURR 38.2 ng/L 40.00 96 50-200 Surrogate: 13C9-PFNA-SURR 38.7 ng/L 40.00 97 50-200 Surrogate: 13C8-PFOS-SURR 38.4 ng/L 38.32 100 50-200 Surrogate: 13C2-8:2FTS-SURR 186 ng/L 153.6 121 50-200 Surrogate: 13C6-PFDA-SURR 38.5 ng/L 40.00 96 50-200 Surrogate: 13C7-PFUnA-SURR 36.0 ng/L 40.00 90 50-200 Surrogate: 13C2-PFDoA-SURR 37.1 ng/L 40.00 93 50-200 LCS (B541534-BS1)Prepared: 08/28/25 Analyzed: 09/15/25 PFBA 77 ng/L 80.00 96 70-130 PFMPA 74 ng/L 80.00 93 70-130 www.pacelabs.comCustomer #: 72-106174 Page 6 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B541534-BS1)Prepared: 08/28/25 Analyzed: 09/15/25 PFPeA 70 ng/L 80.00 88 70-130 PFBS 71 ng/L 80.00 88 70-130 PFMBA 63 ng/L 80.00 79 70-130 PFEESA 66 ng/L 80.00 82 70-130 HFPO-DA 66 ng/L 80.00 83 70-130 NFDHA 67 ng/L 80.00 84 70-130 PFHxS 74 ng/L 80.00 93 70-130 4:2 FTS 80 ng/L 80.00 100 70-130 PFHpA 69 ng/L 80.00 87 70-130 PFHxA 70 ng/L 80.00 88 70-130 ADONA 70 ng/L 80.00 88 70-130 PFPeS 76 ng/L 80.00 95 70-130 6:2 FTS 75 ng/L 80.00 93 70-130 PFOA 68 ng/L 80.00 85 70-130 PFHpS 65 ng/L 80.00 81 70-130 PFOS 73 ng/L 80.00 91 70-130 PFNA 69 ng/L 80.00 86 70-130 9Cl-PF3ONS 69 ng/L 80.00 86 70-130 8:2 FTS 80 ng/L 80.00 100 70-130 PFDA 68 ng/L 80.00 85 70-130 PFUnA 70 ng/L 80.00 87 70-130 11Cl-PF3OUdS 69 ng/L 80.00 86 70-130 PFDoA 69 ng/L 80.00 86 70-130 Surrogate: 13C4-PFBA-SURR 36.9 ng/L 40.00 92 50-200 Surrogate: 13C5-PFPeA-SURR 36.9 ng/L 40.00 92 50-200 Surrogate: 13C3-PFBS-SURR 37.7 ng/L 37.28 101 50-200 Surrogate: 13C2-4:2FTS-SURR 151 ng/L 150.4 101 50-200 Surrogate: 13C5-PFHxA-SURR 35.6 ng/L 40.00 89 50-200 Surrogate: 13C3-HFPOA-DA-SURR 37.1 ng/L 40.00 93 50-200 Surrogate: 13C4-PFHpA-SURR 34.3 ng/L 40.00 86 50-200 Surrogate: 13C3-PFHxS-SURR 37.3 ng/L 37.92 98 50-200 Surrogate: 13C2-6:2FTS-SURR 151 ng/L 152.0 99 50-200 Surrogate: 13C8-PFOA-SURR 34.5 ng/L 40.00 86 50-200 Surrogate: 13C9-PFNA-SURR 33.8 ng/L 40.00 84 50-200 Surrogate: 13C8-PFOS-SURR 37.3 ng/L 38.32 97 50-200 Surrogate: 13C2-8:2FTS-SURR 161 ng/L 153.6 105 50-200 Surrogate: 13C6-PFDA-SURR 32.9 ng/L 40.00 82 50-200 Surrogate: 13C7-PFUnA-SURR 34.4 ng/L 40.00 86 50-200 Surrogate: 13C2-PFDoA-SURR 36.8 ng/L 40.00 92 50-200 Duplicate (B541534-DUP1)Sample: IH04891-01 Prepared: 08/28/25 Analyzed: 09/15/25 PFBA 2 ng/L 2 2 30J PFMPA < 0.4 ng/L ND 30U PFPeA 0.7 ng/L 0.7 3 30J PFBS 1 ng/L 1 3 30J PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 7 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B541534-DUP1)Sample: IH04891-01 Prepared: 08/28/25 Analyzed: 09/15/25 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L 0.4 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 1.0 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.6 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 37.4 ng/L 38.33 98 50-200 Surrogate: 13C5-PFPeA-SURR 47.6 ng/L 38.33 124 50-200 Surrogate: 13C3-PFBS-SURR 32.1 ng/L 35.72 90 50-200 Surrogate: 13C2-4:2FTS-SURR 199 ng/L 144.1 138 50-200 Surrogate: 13C5-PFHxA-SURR 33.7 ng/L 38.33 88 50-200 Surrogate: 13C3-HFPOA-DA-SURR 33.6 ng/L 38.33 88 50-200 Surrogate: 13C4-PFHpA-SURR 35.1 ng/L 38.33 92 50-200 Surrogate: 13C3-PFHxS-SURR 33.2 ng/L 36.34 91 50-200 Surrogate: 13C2-6:2FTS-SURR 162 ng/L 145.6 111 50-200 Surrogate: 13C8-PFOA-SURR 34.1 ng/L 38.33 89 50-200 Surrogate: 13C9-PFNA-SURR 34.6 ng/L 38.33 90 50-200 Surrogate: 13C8-PFOS-SURR 33.0 ng/L 36.72 90 50-200 Surrogate: 13C2-8:2FTS-SURR 153 ng/L 147.2 104 50-200 Surrogate: 13C6-PFDA-SURR 31.8 ng/L 38.33 83 50-200 Surrogate: 13C7-PFUnA-SURR 29.7 ng/L 38.33 77 50-200 Surrogate: 13C2-PFDoA-SURR 29.2 ng/L 38.33 76 50-200 Matrix Spike (B541534-MS1)Sample: IH05117-01 Prepared: 08/28/25 Analyzed: 09/15/25 PFBA 79 ng/L 76.54 ND 104 70-130 PFMPA 77 ng/L 76.54 ND 101 70-130 PFPeA 71 ng/L 76.54 ND 92 70-130 PFBS 73 ng/L 76.54 ND 95 70-130 PFMBA 64 ng/L 76.54 ND 84 70-130 PFEESA 67 ng/L 76.54 ND 87 70-130 NFDHA 70 ng/L 76.54 ND 92 70-130 HFPO-DA 70 ng/L 76.54 ND 92 70-130 PFHxS 77 ng/L 76.54 ND 100 70-130 4:2 FTS 81 ng/L 76.54 ND 106 70-130 PFHpA 70 ng/L 76.54 ND 92 70-130 PFHxA 72 ng/L 76.54 ND 95 70-130 www.pacelabs.comCustomer #: 72-106174 Page 8 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B541534-MS1)Sample: IH05117-01 Prepared: 08/28/25 Analyzed: 09/15/25 ADONA 71 ng/L 76.54 ND 93 70-130 PFPeS 77 ng/L 76.54 ND 101 70-130 6:2 FTS 80 ng/L 76.54 ND 105 70-130 PFOA 70 ng/L 76.54 ND 91 70-130 PFHpS 66 ng/L 76.54 ND 86 70-130 PFOS 75 ng/L 76.54 ND 98 70-130 PFNA 71 ng/L 76.54 ND 92 70-130 9Cl-PF3ONS 73 ng/L 76.54 ND 95 70-130 8:2 FTS 87 ng/L 76.54 ND 113 70-130 PFDA 68 ng/L 76.54 ND 88 70-130 PFUnA 73 ng/L 76.54 ND 95 70-130 11Cl-PF3OUdS 73 ng/L 76.54 ND 95 70-130 PFDoA 70 ng/L 76.54 ND 92 70-130 Surrogate: 13C4-PFBA-SURR 35.9 ng/L 38.27 94 50-200 Surrogate: 13C5-PFPeA-SURR 37.3 ng/L 38.27 97 50-200 Surrogate: 13C3-PFBS-SURR 33.9 ng/L 35.67 95 50-200 Surrogate: 13C2-4:2FTS-SURR 142 ng/L 143.9 99 50-200 Surrogate: 13C5-PFHxA-SURR 35.1 ng/L 38.27 92 50-200 Surrogate: 13C3-HFPOA-DA-SURR 36.4 ng/L 38.27 95 50-200 Surrogate: 13C4-PFHpA-SURR 34.6 ng/L 38.27 90 50-200 Surrogate: 13C3-PFHxS-SURR 33.5 ng/L 36.28 92 50-200 Surrogate: 13C2-6:2FTS-SURR 129 ng/L 145.4 89 50-200 Surrogate: 13C8-PFOA-SURR 34.7 ng/L 38.27 91 50-200 Surrogate: 13C9-PFNA-SURR 34.3 ng/L 38.27 90 50-200 Surrogate: 13C8-PFOS-SURR 32.9 ng/L 36.66 90 50-200 Surrogate: 13C2-8:2FTS-SURR 132 ng/L 147.0 90 50-200 Surrogate: 13C6-PFDA-SURR 35.3 ng/L 38.27 92 50-200 Surrogate: 13C7-PFUnA-SURR 34.4 ng/L 38.27 90 50-200 Surrogate: 13C2-PFDoA-SURR 36.4 ng/L 38.27 95 50-200 www.pacelabs.comCustomer #: 72-106174 Page 9 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 10 of 13 Page 11 of 13 Page 12 of 13 Page 13 of 13