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HomeMy WebLinkAboutDDW-2025-009282September 18, 2025 Dear John Steffan: Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 8/28/25 9:56 am and logged in under work order IH05299. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH26069RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IH05299-01 Name: Sampled: Received: 08/28/25 09:56 08/27/25 11:15 TP001-LITTLE DEER CREEK WTP Reg ID:Drinking Water - Regular SampleMatrix:UTAH26069 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 1.0 ng/L EPA 533PFBA09/16/25 00:12 EJBU2.011.0 < 0.4 ng/L EPA 533PFMPA09/16/25 00:12 EJBU2.010.4 < 0.5 ng/L EPA 533PFPeA09/16/25 00:12 EJBU2.010.5 < 0.5 ng/L EPA 533PFBS09/16/25 00:12 EJBU2.010.5 < 0.4 ng/L EPA 533PFMBA09/16/25 00:12 EJBU2.010.4 < 0.5 ng/L EPA 533PFEESA09/16/25 00:12 EJBU2.010.5 < 0.4 ng/L EPA 533HFPO-DA 09/16/25 00:12 EJBU2.010.4 < 0.5 ng/L EPA 533NFDHA09/16/25 00:12 EJBU2.010.5 < 0.4 ng/L EPA 5334:2 FTS 09/16/25 00:12 EJBU2.010.4 < 0.4 ng/L EPA 533PFHxS09/16/25 00:12 EJBU2.010.4 < 0.6 ng/L EPA 533PFHpA09/16/25 00:12 EJBU2.010.6 < 1.0 ng/L EPA 533PFHxA09/16/25 00:12 EJBU2.011.0 < 0.5 ng/L EPA 533ADONA09/16/25 00:12 EJBU2.010.5 < 0.6 ng/L EPA 533PFPeS09/16/25 00:12 EJBU2.010.6 < 0.5 ng/L EPA 5336:2 FTS 09/16/25 00:12 EJBU2.010.5 < 0.7 ng/L EPA 533PFOA09/16/25 00:12 EJBU2.010.7 < 0.6 ng/L EPA 533PFHpS09/16/25 00:12 EJBU2.010.6 < 0.5 ng/L EPA 533PFOS09/16/25 00:12 EJBU2.010.5 < 0.5 ng/L EPA 533PFNA09/16/25 00:12 EJBU2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 09/16/25 00:12 EJBU2.010.7 < 0.5 ng/L EPA 5338:2 FTS 09/16/25 00:12 EJBU2.010.5 < 0.5 ng/L EPA 533PFDA09/16/25 00:12 EJBU2.010.5 < 0.5 ng/L EPA 533PFUnA09/16/25 00:12 EJBU2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 09/16/25 00:12 EJBU2.010.6 < 0.6 ng/L EPA 533PFDoA09/16/25 00:12 EJBU2.010.6 Surrogate: 13C4-PFBA-SURR 96 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C5-PFPeA-SURR 98 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C3-PFBS-SURR 97 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C2-4:2FTS-SURR 95 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C5-PFHxA-SURR 91 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 93 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C4-PFHpA-SURR 89 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C3-PFHxS-SURR 91 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C2-6:2FTS-SURR 89 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C8-PFOA-SURR 88 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C9-PFNA-SURR 90 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C8-PFOS-SURR 92 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C2-8:2FTS-SURR 90 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C6-PFDA-SURR 85 %50-200 09/16/25 00:12 EJB EPA 533 Surrogate: 13C7-PFUnA-SURR 79 %50-200 09/16/25 00:12 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IH05299-01 Name: Sampled: Received: 08/28/25 09:56 08/27/25 11:15 TP001-LITTLE DEER CREEK WTP Reg ID:Drinking Water - Regular SampleMatrix:UTAH26069 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 81 %50-200 09/16/25 00:12 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B541620 - EPA 533 - EPA 533 Blank (B541620-BLK1)Prepared: 08/29/25 Analyzed: 09/15/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 43.2 ng/L 40.00 108 50-200 Surrogate: 13C5-PFPeA-SURR 42.6 ng/L 40.00 107 50-200 Surrogate: 13C3-PFBS-SURR 40.3 ng/L 37.28 108 50-200 Surrogate: 13C2-4:2FTS-SURR 147 ng/L 150.4 98 50-200 Surrogate: 13C5-PFHxA-SURR 41.5 ng/L 40.00 104 50-200 Surrogate: 13C3-HFPOA-DA-SURR 44.8 ng/L 40.00 112 50-200 Surrogate: 13C4-PFHpA-SURR 42.0 ng/L 40.00 105 50-200 Surrogate: 13C3-PFHxS-SURR 39.6 ng/L 37.92 104 50-200 Surrogate: 13C2-6:2FTS-SURR 146 ng/L 152.0 96 50-200 Surrogate: 13C8-PFOA-SURR 40.4 ng/L 40.00 101 50-200 Surrogate: 13C9-PFNA-SURR 40.5 ng/L 40.00 101 50-200 Surrogate: 13C8-PFOS-SURR 40.8 ng/L 38.32 106 50-200 Surrogate: 13C2-8:2FTS-SURR 157 ng/L 153.6 102 50-200 Surrogate: 13C6-PFDA-SURR 40.7 ng/L 40.00 102 50-200 Surrogate: 13C7-PFUnA-SURR 38.2 ng/L 40.00 96 50-200 Surrogate: 13C2-PFDoA-SURR 40.0 ng/L 40.00 100 50-200 LCS (B541620-BS1)Prepared: 08/29/25 Analyzed: 09/15/25 PFBA 205 ng/L 200.0 103 70-130 PFMPA 199 ng/L 200.0 99 70-130 www.pacelabs.comCustomer #: 72-106174 Page 6 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B541620-BS1)Prepared: 08/29/25 Analyzed: 09/15/25 PFPeA 186 ng/L 200.0 93 70-130 PFBS 184 ng/L 200.0 92 70-130 PFMBA 167 ng/L 200.0 84 70-130 PFEESA 174 ng/L 200.0 87 70-130 HFPO-DA 177 ng/L 200.0 89 70-130 NFDHA 184 ng/L 200.0 92 70-130 4:2 FTS 207 ng/L 200.0 103 70-130 PFHxS 199 ng/L 200.0 100 70-130 PFHxA 188 ng/L 200.0 94 70-130 PFHpA 186 ng/L 200.0 93 70-130 ADONA 197 ng/L 200.0 98 70-130 PFPeS 197 ng/L 200.0 98 70-130 6:2 FTS 198 ng/L 200.0 99 70-130 PFOA 187 ng/L 200.0 93 70-130 PFHpS 177 ng/L 200.0 89 70-130 PFOS 194 ng/L 200.0 97 70-130 PFNA 185 ng/L 200.0 92 70-130 9Cl-PF3ONS 186 ng/L 200.0 93 70-130 8:2 FTS 215 ng/L 200.0 108 70-130 PFDA 184 ng/L 200.0 92 70-130 PFUnA 188 ng/L 200.0 94 70-130 11Cl-PF3OUdS 185 ng/L 200.0 93 70-130 PFDoA 185 ng/L 200.0 93 70-130 Surrogate: 13C4-PFBA-SURR 38.3 ng/L 40.00 96 50-200 Surrogate: 13C5-PFPeA-SURR 38.9 ng/L 40.00 97 50-200 Surrogate: 13C3-PFBS-SURR 37.7 ng/L 37.28 101 50-200 Surrogate: 13C2-4:2FTS-SURR 161 ng/L 150.4 107 50-200 Surrogate: 13C5-PFHxA-SURR 36.9 ng/L 40.00 92 50-200 Surrogate: 13C3-HFPOA-DA-SURR 39.7 ng/L 40.00 99 50-200 Surrogate: 13C4-PFHpA-SURR 34.9 ng/L 40.00 87 50-200 Surrogate: 13C3-PFHxS-SURR 37.6 ng/L 37.92 99 50-200 Surrogate: 13C2-6:2FTS-SURR 158 ng/L 152.0 104 50-200 Surrogate: 13C8-PFOA-SURR 34.5 ng/L 40.00 86 50-200 Surrogate: 13C9-PFNA-SURR 34.1 ng/L 40.00 85 50-200 Surrogate: 13C8-PFOS-SURR 37.0 ng/L 38.32 97 50-200 Surrogate: 13C2-8:2FTS-SURR 148 ng/L 153.6 97 50-200 Surrogate: 13C6-PFDA-SURR 34.3 ng/L 40.00 86 50-200 Surrogate: 13C7-PFUnA-SURR 33.5 ng/L 40.00 84 50-200 Surrogate: 13C2-PFDoA-SURR 34.9 ng/L 40.00 87 50-200 Duplicate (B541620-DUP1)Sample: IH05299-01 Prepared: 08/29/25 Analyzed: 09/15/25 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 7 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B541620-DUP1)Sample: IH05299-01 Prepared: 08/29/25 Analyzed: 09/15/25 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 1.0 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.6 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 39.6 ng/L 40.62 98 50-200 Surrogate: 13C5-PFPeA-SURR 41.1 ng/L 40.62 101 50-200 Surrogate: 13C3-PFBS-SURR 37.7 ng/L 37.86 100 50-200 Surrogate: 13C2-4:2FTS-SURR 148 ng/L 152.7 97 50-200 Surrogate: 13C5-PFHxA-SURR 38.1 ng/L 40.62 94 50-200 Surrogate: 13C3-HFPOA-DA-SURR 40.6 ng/L 40.62 100 50-200 Surrogate: 13C4-PFHpA-SURR 37.8 ng/L 40.62 93 50-200 Surrogate: 13C3-PFHxS-SURR 36.3 ng/L 38.51 94 50-200 Surrogate: 13C2-6:2FTS-SURR 141 ng/L 154.3 92 50-200 Surrogate: 13C8-PFOA-SURR 37.2 ng/L 40.62 92 50-200 Surrogate: 13C9-PFNA-SURR 37.6 ng/L 40.62 92 50-200 Surrogate: 13C8-PFOS-SURR 36.4 ng/L 38.91 94 50-200 Surrogate: 13C2-8:2FTS-SURR 143 ng/L 156.0 92 50-200 Surrogate: 13C6-PFDA-SURR 34.7 ng/L 40.62 85 50-200 Surrogate: 13C7-PFUnA-SURR 33.6 ng/L 40.62 83 50-200 Surrogate: 13C2-PFDoA-SURR 34.6 ng/L 40.62 85 50-200 Matrix Spike (B541620-MS1)Sample: IH05309-01 Prepared: 08/29/25 Analyzed: 09/15/25 PFBA 201 ng/L 189.8 1 105 70-130 PFMPA 205 ng/L 189.8 ND 108 70-130 PFPeA 180 ng/L 189.8 2 94 70-130 PFBS 176 ng/L 189.8 2 92 70-130 PFMBA 168 ng/L 189.8 ND 89 70-130 PFEESA 168 ng/L 189.8 ND 89 70-130 NFDHA 175 ng/L 189.8 ND 92 70-130 HFPO-DA 167 ng/L 189.8 ND 88 70-130 4:2 FTS 200 ng/L 189.8 ND 105 70-130 PFHxS 188 ng/L 189.8 1 99 70-130 PFHpA 180 ng/L 189.8 0.8 94 70-130 PFHxA 184 ng/L 189.8 2 96 70-130 www.pacelabs.comCustomer #: 72-106174 Page 8 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B541620-MS1)Sample: IH05309-01 Prepared: 08/29/25 Analyzed: 09/15/25 PFPeS 188 ng/L 189.8 ND 99 70-130 ADONA 186 ng/L 189.8 ND 98 70-130 6:2 FTS 187 ng/L 189.8 ND 98 70-130 PFOA 179 ng/L 189.8 2 93 70-130 PFHpS 169 ng/L 189.8 ND 89 70-130 PFOS 182 ng/L 189.8 1 95 70-130 PFNA 175 ng/L 189.8 ND 92 70-130 9Cl-PF3ONS 176 ng/L 189.8 ND 93 70-130 8:2 FTS 201 ng/L 189.8 ND 106 70-130 PFDA 173 ng/L 189.8 ND 91 70-130 PFUnA 186 ng/L 189.8 ND 98 70-130 11Cl-PF3OUdS 171 ng/L 189.8 ND 90 70-130 PFDoA 172 ng/L 189.8 ND 90 70-130 Surrogate: 13C4-PFBA-SURR 36.4 ng/L 37.97 96 50-200 Surrogate: 13C5-PFPeA-SURR 41.5 ng/L 37.97 109 50-200 Surrogate: 13C3-PFBS-SURR 34.7 ng/L 35.38 98 50-200 Surrogate: 13C2-4:2FTS-SURR 167 ng/L 142.7 117 50-200 Surrogate: 13C5-PFHxA-SURR 34.4 ng/L 37.97 90 50-200 Surrogate: 13C3-HFPOA-DA-SURR 38.9 ng/L 37.97 102 50-200 Surrogate: 13C4-PFHpA-SURR 33.2 ng/L 37.97 87 50-200 Surrogate: 13C3-PFHxS-SURR 36.3 ng/L 35.99 101 50-200 Surrogate: 13C2-6:2FTS-SURR 156 ng/L 144.3 108 50-200 Surrogate: 13C8-PFOA-SURR 31.2 ng/L 37.97 82 50-200 Surrogate: 13C9-PFNA-SURR 27.1 ng/L 37.97 71 50-200 Surrogate: 13C8-PFOS-SURR 35.0 ng/L 36.37 96 50-200 Surrogate: 13C2-8:2FTS-SURR 146 ng/L 145.8 100 50-200 Surrogate: 13C6-PFDA-SURR 24.8 ng/L 37.97 65 50-200 Surrogate: 13C7-PFUnA-SURR 25.0 ng/L 37.97 66 50-200 Surrogate: 13C2-PFDoA-SURR 29.6 ng/L 37.97 78 50-200 www.pacelabs.comCustomer #: 72-106174 Page 9 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 10 of 13 Page 11 of 13 Page 12 of 13 Page 13 of 13