DERR-2025-006039

Limited Site Investigation
Salt Lake City Fleet Yard
800 South 325 West, Salt Lake City, Utah
Facility ID 4000835, Release ID IEQ
June 22, 2016
Terracon Project No. AL137118B
Prepared for:
Salt Lake City Corporation
Salt Lake City, Utah
Prepared by:
Terracon Consultants, Inc.
Salt Lake City, Utah
Terracon Consultants, Inc .6949 South High Tech Drive Midvale , Utah 84047
P [phone] F [phone] terracon.com
June 22, 2016
Salt Lake City Corporation
451 South State Street
Salt Lake City, Utah 84114
Attn:Mr. J. Todd Reeder
E:[e-mail]
Re:Limited Site Investigation
Fleet Management Yard
800 South 325 West
Salt Lake City, Utah
Facility Identification No. 4000835, Release ID IEQ
Terracon Project No. AL137118B
Dear Mr. Reeder:
Terracon is pleased to provide this report documenting follow-up investigation activities conducted
at the above-referenced site. Terracon has performed this work pursuant to Terracon's Utah
Department of Environmental Quality, Division of Environmental Response & Remediation (DERR)-
approved Work Plan IEQ-18, dated March 30, 2016.
We appreciate the opportunity to have performed these services for you. Please contact our
office at [phone] if you have questions regarding this information or if we can provide any
other services.
Sincerely,
Terracon Consultants, Inc.
Andy R. King, P.G.Benjamin B. Bowers
Senior Project Manager Environmental Department Manager
Environmental Services Authorized Project Reviewer
ARK/BBB/ta
Attachments
Copies:Addressee (Electronic); Hong-Lei, Utah DEQ/DERR (Electronic)
TABLE OF CONTENTS
Page
1.0 INTRODUCTION .............................................................................................................1
1.1 Site Description ....................................................................................................1
1.2 Project Background ..............................................................................................1
1.3 Scope of Work .....................................................................................................2
1.4 Standard of Care..................................................................................................2
1.5 Additional Scope Limitations ................................................................................2
1.6 Reliance ...............................................................................................................3
2.0 LIMITED SITE INVESTIGATION .....................................................................................3
2.1 Environmental Soil Borings ..................................................................................3
2.2 Subsurface Soil Sampling ....................................................................................4
2.4 Groundwater Sampling ........................................................................................4
3.0 LABORATORY ANALYTICAL METHODS .....................................................................4
4.0 DATA EVALUATION ......................................................................................................5
4.1 Soil Sample Results .............................................................................................5
4.2 Groundwater Sample Results ..............................................................................5
5.0 FINDINGS AND CONCLUSIONS ...................................................................................5
APPENDICES
Appendix A Exhibits
Exhibit 1 - Topographic Map
Exhibit 2 - Site Plan
Exhibit 3 - Site Diagram with Recent Boring Locations
Exhibit 4 – Site Diagram with ISL Exceedances
Appendix B Tables
Table 1 - Corrective Action and Follow-up Soil Sample Analytical Results
Table 2 - Corrective Action and Groundwater Monitoring Analytical Results
Appendix C Soil Boring Logs
Appendix D Chain of Custody and Laboratory Data Sheets
LIMITED SITE INVESTIGATION
Salt Lake City Fleet Yard
800 South 325 West
Salt Lake City, Utah
Facility Identification No. 4000835, Release Site IEQ
Terracon Project No. AL137118B
June 22, 2016
Responsive ■ Resourceful ■ Reliable
1.0 INTRODUCTION
1.1 Site Description
Site Name Salt Lake City Fleet Yard
Site Location/Address 800 South 325 West, Salt Lake City, Utah
General Site Description
The site was formerly used as a Salt Lake City fleet vehicle fueling and
maintenance facility. It is currently used by Salt Lake City’s Police
Department as a training facility and the Fire Department for equipment
storage.
Exhibit 1 (Appendix A) presents a topographic map of the area. Exhibit 2 is a diagram that
indicates the approximate location of the investigation area in relation to the overall site.
1.2 Project Background
A fuel release associated with a system of four underground storage tanks (USTs) was initially
discovered in 1993. Subsurface investigations and periodic groundwater monitoring were
conducted between 1993 and 2011, and the four USTs were removed in 2011. In 2013, soil and
groundwater impacts were identified at concentrations above screening levels at locations
surrounding the former tank basin. In early 2014, Terracon conducted corrective action in the
vicinity of the former tank basin, under the DERR-approved Work Plan IEQ-15. The corrective
action included over-excavation and removal of the identified impacted soils for off-site disposal,
removal of impacted groundwater from the open-excavation, and a limited application of chemical
oxidation reagents to treat residual petroleum-impacted groundwater in the excavation area prior
to backfilling.
Terracon subsequently installed six groundwater monitoring wells under Work Plan IEQ-16 and
conducted a groundwater sampling event to evaluate concentrations of petroleum hydrocarbons
remaining in the area of the former UST basin and dispensers. The results indicated that
concentrations of dissolved petroleum hydrocarbons remained above screening levels at the site,
and the extent of impacts was not defined. Under Work Plan IEQ-17, Terracon advanced four
additional soil borings for soil sampling, completed the borings as monitoring wells, and conducted
an additional round of post-corrective action groundwater sampling. Results from these two
groundwater sampling events indicated that dissolved petroleum hydrocarbons, specifically TPH-
Limited Site Investigation
Fleet Management Yard ■ Salt Lake City, Utah
June 22, 2016 ■ Terracon Project No. AL137118B
Responsive ■ Resourceful ■ Reliable 2
DRO and benzene, remained above DERR Initial Screening Levels (ISLs) south of the former
tank basin.
This report documents the results of Work Plan IEQ-18, which was developed to further define
the extent of impacts south of the former tank basin.
1.3 Scope of Work
Work Plan IEQ-18 included the advancement of seven additional soil borings at locations that
were selected with input from DERR; two soil samples and one groundwater sample were
collected from each of the borings.
The results of this Limited Site Investigation (LSI) will be used to develop a Corrective Action
Work Plan. The overall project goal is to meet regulatory screening levels, less than Initial
Screening Levels (ISLs) for unrestricted land use, and receive a “No Further Action” status for
Release ID IEQ.
1.4 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time
period. Please note that Terracon does not warrant the work of laboratories, regulatory agencies
or other third parties supplying information used in the preparation of the report. These services
were performed in accordance with the scope of work agreed with you, our client, as reflected in
our proposal, and were not restricted by ASTM E1903-11.
1.5 Additional Scope Limitations
Findings, conclusions and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work. Such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, non-detectable or not present during these services, and we cannot
represent that the site contains no hazardous substances, toxic materials, petroleum products, or
other latent conditions beyond those identified during this investigation. Subsurface conditions
may vary from those encountered at specific borings or wells or during other surveys, tests,
assessments, investigations or exploratory services; the data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.
Limited Site Investigation
Fleet Management Yard ■ Salt Lake City, Utah
June 22, 2016 ■ Terracon Project No. AL137118B
Responsive ■ Resourceful ■ Reliable 3
1.6 Reliance
This report has been prepared for the exclusive use and reliance of the Salt Lake City Corporation
and government entities having jurisdiction over the site. Use or reliance by any other party is
prohibited without the written authorization of the Salt Lake City Corporation and Terracon.
Reliance on the report by the client and all authorized parties will be subject to the terms, conditions
and limitations stated in the proposal, report, and Terracon’s Terms and Conditions. The limitation
of liability defined in the Terms and Conditions is the aggregate limit of Terracon’s liability to the client
and all relying parties.
2.0 LIMITED SITE INVESTIGATION
2.1 Environmental Soil Borings
Prior to drilling, the public utility location service (Blue Stakes) was notified at least 48 hours prior
to drilling as required by law. In addition, a subcontracted private utility location service was used
to identify and mark subsurface utilities in the area of each boring location. The boring locations
were adjusted in the field as needed to avoid buried utilities or other obstacles.
Terracon’s field activities were conducted on April 28, 2016. Seven borings (B-9 through B-15)
were advanced for soil and groundwater sampling at the approximate locations shown on Exhibit
3 (Appendix A). The borings were advanced to a maximum depth of approximately 15 feet below
the ground surface (bgs). Mechanized drilling services were performed by a State of Utah-
licensed Monitoring Well Driller, using a direct push drilling rig under the supervision of Terracon
field professionals. All environmental samples were collected by Mark Lilly, Utah UST
Groundwater and Soil Sampler (#GS-449). Mechanized drilling equipment was cleaned, using a
high-pressure washer prior to beginning the project and before beginning the soil boring. Soil
samples were collected continuously from the boring using a five-foot macro-core sampler.
Soil cores were observed to document soil types, color, moisture content, and sensory evidence
of environmental impacts. The soil samples were also field-screened using a portable
photoionization detector (PID) – Mini Rae 2000 PID to determine the potential presence of total
volatile organic compounds (TVOCs). The subsurface soil types encountered during sample
collection varied between borings but generally consisted of silty gravel fill materials underlain by
silty clays. PID readings ranging from non-detect to a maximum of 55 parts per million (ppm).
Groundwater was typically encountered at depths of approximately 8 feet bgs. Detailed
lithological descriptions and PID readings are presented on the soil boring logs included in
Appendix C.
Limited Site Investigation
Fleet Management Yard ■ Salt Lake City, Utah
June 22, 2016 ■ Terracon Project No. AL137118B
Responsive ■ Resourceful ■ Reliable 4
2.2 Subsurface Soil Sampling
In accordance with Work Plan IEQ-18, two soil samples were collected from each boring. One
soil sample was collected from the interval displaying the highest impacts, or, if impacts were not
observed, from the soil-groundwater interface. To assess the vertical extent of impacts, one soil
sample was also collected from the total depth of the boring or from the underlying interval that
appeared to be free of contaminants.
2.4 Groundwater Sampling
Terracon collected one groundwater sample from each of the seven borings (converted to
temporary groundwater sampling points), using a low-flow peristaltic pump and new polyethylene
tubing. Prior to sampling, the temporary sampling point was developed and purged, using the
peristaltic pump to reduce turbidity.
The groundwater gradient was not measured during field activities, as none of the monitoring
wells were accessed as part of this LSI. Gradient measurements during previous groundwater
monitoring events have consistently indicated an overall south-southeasterly groundwater flow
direction at the site.
3.0 LABORATORY ANALYTICAL METHODS
The soil and groundwater samples were collected and placed in laboratory-prepared containers,
labeled, and placed on ice in a cooler. The samples and completed chain-of-custody forms were
shipped via overnight courier to Environmental Science Corporation analytical laboratory in Mt.
Juliet, Tennessee (a Utah Certified Laboratory).
All samples were analyzed by laboratory test methods as appropriate for the type(s) of
contaminants most likely to be associated with the former UST systems: methyl tert-butyl ether
(MTBE), benzene, toluene, ethylbenzene, xylenes, and naphthalene (BTEXN), total petroleum
hydrocarbons in the gasoline range (TPH-GRO), and total petroleum hydrocarbons in the diesel
range (TPH-DRO) with silica gel treatment. Samples were analyzed using the following methods:
Analysis Sample Type No. of Samples Laboratory Method
BTEXN, MTBE and
TPH-GRO Soil 14 EPA Method 8260
TPH-DRO Soil 14 EPA Method 8015
BTEXN, MTBE and
TPH-GRO Groundwater 7 EPA Method 8260
TPH-DRO Groundwater 7 EPA Method 8015
The executed chain-of-custody form and laboratory data sheets are provided in Appendix D.
Limited Site Investigation
Fleet Management Yard ■ Salt Lake City, Utah
June 22, 2016 ■ Terracon Project No. AL137118B
Responsive ■ Resourceful ■ Reliable 5
4.0 DATA EVALUATION
Please refer to Table 1 (Appendix B) for a summary of the laboratory analytical results for
historical excavation confirmation soil samples and follow-up soil samples, including those
collected during this investigation. Please refer to Table 2 (Appendix B) for a summary of the
laboratory analytical results for groundwater samples. Tables 1 and 2 include regulatory
screening levels for comparative purposes.
4.1 Soil Sample Results
Soil samples collected from borings B-9 through B-15 did not report any petroleum constituent
concentrations above ISLs, with one exception. At boring B-11, the soil sample collected from a
depth of 9-10 feet bgs reported a TPH-DRO concentration of 1,080 milligrams per kilogram
(mg/kg), which is above the ISL of 500 mg/kg but below the Tier 1 Screening Level of 5,000
mg/kg.
4.2 Groundwater Sample Results
Groundwater samples collected from borings B-9 through B-15 did not report any petroleum
constituent concentrations above ISLs, with one exception. The groundwater sample collected
from boring B-11 reported a TPH-DRO concentration of 2.10 milligrams per liter (mg/l), which is
above the ISL of 1 mg/l but below the Tier 1 Screening Level of 10 mg/l.
5.0 FINDINGS AND CONCLUSIONS
Based on the results of this LSI and recent investigations conducted under Work Plans IEQ-16
and IEQ-17, residual petroleum impacts to soil with ISL exceedances appear to be confined to a
relatively small area in the vicinity of boring B-11. At this location, which is within the footprint of
an existing building, only one constituent (TPH-DRO) was identified at a concentration above an
ISL.
Residually impacted groundwater with ISL exceedances appears to be somewhat more
widespread, based on the results of groundwater samples collected during this LSI and in 2015
under Work Plans IEQ-16 and IEQ-17. Dissolved TPH-DRO and benzene concentrations
exceeding ISLs appear to extend from the former UST basin southward to boring B-11 (within an
existing building), but not to the southern property boundary.
Locations of the remaining ISL exceedances in soil and groundwater are indicated on Exhibit 4
(Appendix A). The lateral extent of the plume of residually impacted groundwater is now defined
by the borings advanced during this LSI and by the existing monitoring well network. Under
separate cover, Terracon will develop a Corrective Action Work Plan to address the remaining
impacts to soil and groundwater, consistent with the planned site redevelopment.
Limited Site Investigation
Fleet Management Yard ■ Salt Lake City, Utah
June 22, 2016 ■ Terracon Project No. AL137118B
Responsive ■ Resourceful ■ Reliable 6
Terracon appreciates being of service to you on this project. If you have any questions, require
additional information, or need additional assistance, please contact us.
APPENDIX A
Exhibits
TOPOGRAPHIC MAP IMAGE COURTESY OF
THE U.S. GEOLOGICAL SURVEY
QUADRANGLES INCLUDE: SALT LAKE CITY
NORTH, UT (1/1/1998), FORT DOUGLAS, UT
(1/1/1998), SALT LAKE CITY SOUTH, UT
(1/1/1999) and SUGAR HOUSE, UT (1/1/1998).
TOPOGRAPHIC MAP
SLC - Fleet Management Yard
800 South 325 West
Salt Lake City, UT
640 E. Wilmington Ave.
Salt Lake City, UT 84106
AL137118B
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES
Project Manager:
Drawn by:
Checked by:
Approved by:
JK
ABF
ABF
ABF
Ex 1
04-08-15
Project No.
File Name:
Date:
1
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EXHIBITProject No.:
Reviewed By:
Date:
Drawn By:JK
ABF
06/14/16
6949 South High Tech Drive Midvale, UT 84047
PH. [phone] terracon.com
3
N:\Projects\2013\AL137118B\Working Files\Diagrams-Drawings-Figures\GIS\AL137118B_Ex_3_2016.mxd
NOTES: This Product is intended for informational purposes only and may not be suitable for legal, engineering, or surveying purposes.
DATA SOURCES: Aerial Photography provided by AGRC (2012 HRO).
SLC - Fleet Management Yard800 South 325 WestSalt Lake City, Utah
AL137118B
Lege nd
@A Recent Boring Locations
@A Monitoring Wells
Groundwater Isocontours (0.2' Contour Interval)
Approx Groundwater Flow Direction (09/10/15)
Excavation Area (2014)
SITE DIAG RAM WITHRECENT BORING LOCATIONS
0 40 8020Feet1 inch = 40 feet
900 South
87.97'
87.42'87.39'
87.28'
87.61'
87.55'87.59'
87.96'87.94'
87.93'87.93'
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87.80'
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SITE DIAG RAM WITHISL EXCEEDANCES
900 South
APPENDIX B
Tables
TPH-
DRO
TPH-
GRO Benzene Toluene Ethylbenzene Total Xylenes Napthalene MTBE
500 150 0.2 9 5 142 51 0.3
5,000 1,500 0.9 25 23 142 51 0.3
NW-1 @10'1/23/2014 10 256 193 <0.0643 <0.129 0.728 0.411 2.49 <0.129 3,993
NW-2 @9'1/23/2014 9 513 506 <0.0641 <0.128 2.13 1.44 4.67 <0.128 3,924
NW-3 @10'1/31/2014 10 <25.1 0.340 <0.00317 <0.00634 <0.00634 <0.00634 <0.00634 <0.00634 97
NW-4 @9'1/31/2014 9 37.6 5.8 <0.00311 <0.00623 <0.00623 <0.00623 0.197 <0.00623 569
EW-1 @9'1/24/2014 9 160 131 <0.0637 <0.127 0.309 0.371 1.18 <0.127 3,216
EW-2 @9'1/24/2014 9 60.9 6.95 0.0400 <0.00693 0.0213 0.00991 0.400 <0.00693 2,972
SW-1 @10'1/29/2014 10 32.4 1.19 0.1050 <0.00702 <0.00702 <0.00702 0.0556 <0.00702 128
SW-2 @10'1/29/2014 10 <31.2 0.471 0.00828 <0.00796 <0.00796 <0.00796 <0.00796 <0.00796 32
WW-1 @10'1/29/2014 10 55.1 5.60 <0.00344 <0.00689 <0.00689 <0.00689 <0.00689 <0.00689 217
WW-2 @10'1/29/2014 10 38.6 11.90 <0.00373 <0.00747 <0.00747 <0.00747 0.00751 <0.00747 1,313
FS-1 @13'1/28/2014 13 46.1 128 <0.0670 <0.134 <0.134 <0.134 <0.134 <0.134 44
F-2 @10'1/24/2014 10 83.3 101 0.367 <0.126 0.379 0.436 0.489 <0.126 698
FS-2 @12'1/31/2014 12 <24.0 <0.0605 <0.00303 <0.00605 <0.00605 <0.00605 <0.00605 <0.00605 5
F-3 @10'1/24/2014 10 26.1 14.6 0.00422 <0.00639 0.0284 0.0470 0.191 <0.00639 1,967
FS-4 @10'1/29/2014 10 <29.8 13.2 0.0106 <0.00784 0.0383 <0.00784 0.249 <0.00784 1,628
PZ-1 @10'2/5/2014 10 25.6 <0.0619 <0.00310 <0.00619 <0.00619 <0.00619 <0.00619 <0.00619 ND
MW-6 @10'2/5/2014 10 146 77.4 <0.0129 0.0291 0.200 0.0596 1.33 <0.0258 2,362
SS-1 2/10/2014 9 1.8 <3.2 <0.0064 <0.032 <0.0064 <0.019 0.018 <0.0064 na
SS-2 2/10/2014 9 6.4 2.3 <0.0063 <0.032 0.002 0.0069 0.014 <0.0063 na
T-7 @ 6'6/10/2015 6 6.7 <3.34 <0.00667 <0.0334 <0.00667 <0.0200 <0.0334 <0.00667 ND
T-8 @ 9'6/10/2015 9 2.6 <3.30 <0.00661 <0.0330 <0.00661 <0.0198 <0.0330 <0.00661 1.2
T-9 @ 5'6/10/2015 5 1.3 <3.51 <0.00702 <0.0351 <0.00702 <0.0211 <0.0351 <0.00702 3.4
T-10 @ 5'6/10/2015 5 2.4 <3.49 <0.00697 <0.0349 <0.00697 <0.0209 <0.0349 <0.00697 6.0
B-9 9.5-10FT 4/28/2016 9.5-10 7.9 4.21 <0.00642 <0.0321 <0.00642 <0.0193 <0.0321 <0.00642 55
B-9 14.5-15FT 4/28/2016 14.5-15.5 <5.56 <3.47 <0.00694 <0.0347 <0.00694 <0.0208 <0.0347 <0.00694 0.5
B-10 8FT 4/28/2016 8 <4.9 <3.06 <0.00613 <0.0306 <0.00613 <0.0184 <0.0306 <0.00613 ND
B-10 14FT 4/28/2016 14 <5.13 <3.21 <0.00642 <0.0321 <0.00642 <0.0193 <0.0321 <0.00642 1.0
B-11 9-10FT 4/28/2016 9-10 1,080 8.19 <0.00619 <0.0309 <0.00619 <0.0186 3.17 <0.00619 35
B-11 14.5FT 4/28/2016 14.5 <5.22 <3.26 <0.00652 <0.0326 <0.00652 <0.0196 0.00728 <0.00652 2
B-12 9FT 4/28/2016 9 <4.83 <3.02 <0.00604 <0.0302 <0.00604 <0.0181 <0.0302 <0.00604 ND
B-12 13FT 4/28/2016 13 <4.94 <3.09 <0.00618 <0.0309 <0.00618 <0.0185 <0.0309 <0.00618 ND
B-13 5-6FT 4/28/2016 5-6 113.0 <3.21 <0.00641 <0.0321 <0.00641 <0.0192 <0.0321 <0.00641 0.3
B-13 11-12FT 4/28/2016 11-12 <5.04 <3.15 <0.0063 <0.0315 <0.0063 <0.0189 <0.0315 <0.0063 0.2
B-14 7-8FT 4/28/2016 7-8 <5.17 <3.23 <0.00646 <0.0323 <0.00646 <0.0194 <0.0323 <0.00646 ND
B-14 11-12FT 4/28/2016 11-12 <5.08 <3.17 <0.00635 <0.0317 <0.00635 <0.019 <0.0317 <0.00635 ND
B-15 7-8FT 4/28/2016 7-8 <5.34 <3.34 <0.00668 <0.0334 <0.00668 <0.02 <0.0334 <0.00668 ND
B-15 11-12FT 4/28/2016 11-12 <5.04 <3.15 <0.0063 <0.0315 <0.0063 <0.0189 <0.0315 <0.0063 ND
NOTES:mg/kg Milligrams per kilogram DRO Diesel Range Organics ND -Not Detected
TPH Total Petroleum Hydrocarbons GRO Gasoline Range Organics na -not available
ppm Parts per million PID Photoionization detector
Values in bold exceed DERR Initial Screening Levels
Values in underlined bold exceed DERR Tier 1 Screening Criteria
Terracon Project No. AL137118B
Table 1 - Corrective Action and Follow-up Soil Sample Analytical Results
Fleet Management Yard
Salt Lake City, Utah
Facility Identification No. 4000835, Release Site IEQ
Sample ID Date
Collected
Sample
Depth
(feet)
Laboratory Results (mg/kg)PID
Reading
(ppm)
DERR Initial Screening Levels (mg/kg)
DERR Tier 1 Screening Criteria (mg/kg)
PZ-1 Excavation
Extent of Excavation Samples
MW-6 Excavation
Additional LSI June 2015
Orphaned UST
Additional LSI April 2016
These soils were removed as part of the 2014 excavation and are no longer present.
1 1 0.005 1 0.7 10 0.7 0.2
10 10 0.3 3 4 10 0.7 0.2
FS-1-GW 2/3/2014 (excavation)A 6.6 6.0 0.032 0.033 0.062 0.14 0.04 <0.01
FS-2-GW 2/3/2014 (excavation)A 7.8 6.9 0.029 0.025 0.11 0.23 0.081 <0.01
FS-3-GW 2/3/2014 (excavation)A 5.7 4.7 0.44 0.0098 0.13000 0.1900 0.11 <0.01
FS-4-GW 2/3/2014 (excavation)A 7.1 5.7 0.013 <0.05 0.041 0.021 0.086 <0.01
PZ-1 GW 2/5/2014 (excavation)A 1.6 <0.50 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
MW-6 GW 2/5/2014 (excavation)A 4.1 0.46 0.0086 <0.005 0.0035 0.0021 0.014 <0.001
MW-4 9/10/2015 8.48 0.0615 <0.5 <0.001 <0.0005 <0.001 <0.003 <0.005 <0.001
MW-5 9/10/2015 8.00 0.129 <0.5 <0.001 <0.0005 <0.001 <0.003 <0.005 <0.001
T-1 3/15/2015 7.18 0.54 <0.5 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
9/10/2015 7.12 0.44 <0.5 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
T-2 3/15/2015 7.91 0.9 <0.5 0.000787 <0.005 0.00189 0.00287 0.00119 <0.001
9/10/2015 7.66 0.921 <0.5 0.00162 0.000966 0.00274 0.00481 0.0019 <0.001
T-3 3/15/2015 8.15 1.6 <0.5 0.103 0.0037 0.0387 0.0391 0.0183 <0.001
9/10/2015 7.91 1.84 <0.5 0.104 0.0037 0.038 0.0444 0.0191 <0.001
T-4 3/15/2015 8.33 1.1 <0.5 0.0016 <0.005 0.0041 0.00244 0.00348 <0.001
9/10/2015 8.09 1.33 <0.5 0.00283 0.00125 0.00724 0.00462 0.00631 <0.001
T-5 3/15/2015 7.96 0.4 <0.5 0.0044 0.00889 0.00771 0.0243 0.0048 <0.001
9/10/2015 7.73 0.462 <0.5 0.00487 0.00888 0.0081 0.0265 0.00663 <0.001
T-6 3/15/2015 7.87 1.2 0.445 0.121 0.000807 0.00686 0.00113 0.00192 0.000507
9/10/2015 7.94 1.87 0.624 0.0302 <0.005 <0.001 <0.003 <0.005 0.000683
T-7 6/12/2015 7.13 <0.100 <0.5 <0.001 <0.005 <0.001 <0.003 <0.005 0.00054
9/10/2015 8.61 0.377 <0.5 <0.001 <0.005 <0.001 <0.003 <0.005 0.000449
T-8 6/12/2015 6.82 0.073 <0.5 0.0125 <0.005 <0.001 <0.003 <0.005 0.00218
9/10/2015 8.29 1.22 <0.5 0.0242 <0.005 <0.001 <0.003 <0.005 0.00161
T-9 6/12/2015 7.08 0.1 0.375 <0.001 <0.005 <0.001 <0.003 <0.005 0.000636
9/10/2015 8.54 1.7 0.333 <0.001 <0.005 <0.001 <0.003 <0.005 0.000491
T-10 6/12/2015 6.72 0.046 <0.5 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
9/10/2015 8.18 0.805 <0.5 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
B-9 4/28/2016 8.5B 0.15 0.75 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
B-10 4/28/2016 8B 0.588 0.504 <0.001 <0.005 <0.001 <0.003 <0.005 <0.001
B-11 4/28/2016 8B 2.10 0.221 J <0.001 <0.005 <0.001 <0.003 0.0327 <0.001
B-12 4/28/2016 8B 0.693 0.263 J <0.001 <0.005 <0.001 <0.003 0.00264 J <0.001
B-13 4/28/2016 8B 0.446 0.289 J <0.001 <0.005 <0.001 <0.003 <0.005 0.000872 J
B-14 4/28/2016 8B 0.148 0.214 J <0.001 <0.005 <0.001 <0.003 <0.005 0.00228
B-15 4/28/2016 8B 0.183 0.207 J <0.001 <0.005 <0.001 <0.003 <0.005 0.000522 J
NOTES:
mg/L - Milligrams per liter DRO-Diesel Range Organics A-groundwater sample collected from floor of excavation during soil removal
TPH - Total Petroleum Hydrocarbons GRO-Gasoline Range Organics B-groundwater sample collected from soil boring; depth approximate
Values in bold exceed DERR Initial Screening Levels J-Estimated value below the lowest calibration point
LSI April 2016
Depth to
Groundwater
(feet)MTBE
DERR Initial Screening Levels (mg/L)
DERR Tier 1 Screening Criteria (mg/L)
Excavation Groundwater Samples
PZ-1 Excavation Groundwater
MW-6 Excavation Groundwater
Sample ID Date Collected
Laboratory Results (mg/L)
TPH-DRO TPH-GRO Benzene Toluene
Monitoring Well Samples
Ethyl-
benzene
Total
Xylenes Naphthalene
Table 2 - Corrective Action and Groundwater Monitoring Analytical Results
Salt Lake City Fleet Yard
Salt Lake City, Utah
Facility Identification No. 4000835, Release Site IEQ
Terracon Project No. AL137118B
APPENDIX C
Soil Boring Logs
0.5
2.0
6.0
8.0
9.3
10.5
12.8
13.3
15.0
Groundwater at ~ 8.5 feet
Asphalt
FILL - , Silty Gravel Fill
SILT (ML), dark brown, moist, soft, loose
SILTY CLAY (CL-ML), brown, wet, soft, loose
SILTY CLAY (CL-ML), light brown, moist, stiff, dense
SILTY CLAY (CL-ML), gray, moist, stiff, dense, Staining and Petro Odor
SILTY CLAY (CL-ML), dark brown, wet, medium stiff, medium dense, more silt than clay
SILTY SAND (SM), gray, wet, loose to medium dense
LEAN CLAY (CL), gray, wet, stiff, dense
Boring Terminated at 15 Feet
SS
SS
0.3
0.5
1.0
1.3
1.5
1.5
2.0
7.0
30
55
31
5.0
2.0
0.5
0.5
0.5
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
A
P
H
I
C

L
O
G
See Exhibit A-2
TH
I
S

B
O
R
I
N
G

L
O
G

I
S

N
O
T

V
A
L
I
D

I
F

S
E
P
A
R
A
T
E
D

F
R
O
M

O
R
I
G
I
N
A
L

R
E
P
O
R
T
.

E
N
V
I
R
O
N
M
E
N
T
A
L

S
M
A
R
T

L
O
G

0
0
A
A
G
I
N
T

B
H

S
L
C
F
M
Y

4
-
2
9
-
1
6
.
G
P
J

T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T

5
/
1
1
/
1
6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-9
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-1
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
p
p
m
)
DE
P
T
H

(
f
t
)
5
10
15
WA
T
E
R

L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
SA
M
P
L
E

T
Y
P
E
WATER LEVEL OBSERVATIONS
70
90
100
RE
C
O
V
E
R
Y

(
%
)
0.5
4.0
8.0
11.3
12.8
14.8
15.0
Groundwater at ~ 8 feet
Asphalt
FILL - , Silty Gravel Fill
SILTY CLAY (CL-ML), dark brown, moist, soft, loose
LEAN CLAY (CL), light brown, wet, medium stiff, dense
SILTY CLAY (CL-ML), brown, wet, soft
WELL GRADED SAND (SW), gray, wet, Slight Petro Odor
LEAN CLAY (CL), grayish-brown, wet, stiff, dense
Boring Terminated at 15 Feet
SS
SS
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.1
0.1
0.2
0.3
0.5
1.0
0.5
0.0
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
A
P
H
I
C

L
O
G
See Exhibit A-2
TH
I
S

B
O
R
I
N
G

L
O
G

I
S

N
O
T

V
A
L
I
D

I
F

S
E
P
A
R
A
T
E
D

F
R
O
M

O
R
I
G
I
N
A
L

R
E
P
O
R
T
.

E
N
V
I
R
O
N
M
E
N
T
A
L

S
M
A
R
T

L
O
G

0
0
A
A
G
I
N
T

B
H

S
L
C
F
M
Y

4
-
2
9
-
1
6
.
G
P
J

T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T

5
/
1
1
/
1
6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-10
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-2
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
p
p
m
)
DE
P
T
H

(
f
t
)
5
10
15
WA
T
E
R

L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
SA
M
P
L
E

T
Y
P
E
WATER LEVEL OBSERVATIONS
50
70
90
RE
C
O
V
E
R
Y

(
%
)
0.5
6.0
9.5
10.5
14.5
15.0
Groundwater at ~ 8 feet
Concrete
FILL - , Silty Gravel Fill
SILTY CLAY (CL-ML), dark brown, moist, medium stiff
LEAN CLAY (CL), gray, moist, medium stiff, dense, Slight Petro Odor
SILTY CLAY (CL-ML), brown, wet, stiff, dense
LEAN CLAY (CL), gray, wet, stiff, dense
Boring Terminated at 15 Feet
SS
SS
0.0
0.0
0.2
0.3
4.0
4.0
4.0
15
35
17
10
4.0
3.0
2
2
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
A
P
H
I
C

L
O
G
See Exhibit A-2
TH
I
S

B
O
R
I
N
G

L
O
G

I
S

N
O
T

V
A
L
I
D

I
F

S
E
P
A
R
A
T
E
D

F
R
O
M

O
R
I
G
I
N
A
L

R
E
P
O
R
T
.

E
N
V
I
R
O
N
M
E
N
T
A
L

S
M
A
R
T

L
O
G

0
0
A
A
G
I
N
T

B
H

S
L
C
F
M
Y

4
-
2
9
-
1
6
.
G
P
J

T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T

5
/
1
1
/
1
6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-11
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-3
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
p
p
m
)
DE
P
T
H

(
f
t
)
5
10
15
WA
T
E
R

L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
SA
M
P
L
E

T
Y
P
E
WATER LEVEL OBSERVATIONS
80
10
100
RE
C
O
V
E
R
Y

(
%
)
0.5
3.0
6.0
8.0
10.0
12.0
13.0
14.7
15.0
Groundwater at ~ 8 feet
Concrete
FILL - , Silty Gravel Fill
SILT (ML), dark brown, moist, medium stiff
SILTY CLAY (CL-ML), dark brown, wet, soft, loose
LEAN CLAY (CL), grayish-brown, wet, stiff, dense
SILTY CLAY (CL-ML), brown, wet, soft
LEAN CLAY (CL), grayish-brown, wet, medium stiff, medium dense
SILTY SAND (SM), grayish-brown, wet, medium stiff, medium dense, Very Fine Sand, Tight
LEAN CLAY (CL), gray, wet, stiff, dense
Boring Terminated at 15 Feet
SS
SS
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
A
P
H
I
C

L
O
G
See Exhibit A-2
TH
I
S

B
O
R
I
N
G

L
O
G

I
S

N
O
T

V
A
L
I
D

I
F

S
E
P
A
R
A
T
E
D

F
R
O
M

O
R
I
G
I
N
A
L

R
E
P
O
R
T
.

E
N
V
I
R
O
N
M
E
N
T
A
L

S
M
A
R
T

L
O
G

0
0
A
A
G
I
N
T

B
H

S
L
C
F
M
Y

4
-
2
9
-
1
6
.
G
P
J

T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T

5
/
1
1
/
1
6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-12
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-4
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
p
p
m
)
DE
P
T
H

(
f
t
)
5
10
15
WA
T
E
R

L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
SA
M
P
L
E

T
Y
P
E
WATER LEVEL OBSERVATIONS
50
80
90
RE
C
O
V
E
R
Y

(
%
)
0.5
4.2
7.0
9.0
12.0
14.5
15.0
Groundwater at ~ 8 feet
Asphalt
FILL - , Silty Gravel Fill
SILT (ML), dark brown, moist, stiff
SILTY CLAY (CL-ML), brown, moist, soft, loose
LEAN CLAY (CL), brown, moist, medium stiff, medium dense
SILTY SAND (SM), grayish-brown, wet, medium stiff, medium dense, Very Fine Sand
LEAN CLAY (CL), grayish-brown, wet, stiff, dense
Boring Terminated at 15 Feet
SS
SS
0.0
0.4
0.5
0.8
0.3
0.7
0.2
0.1
0.1
0.1
0.2
0.2
0.0
0.0
0.0
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
A
P
H
I
C

L
O
G
See Exhibit A-2
TH
I
S

B
O
R
I
N
G

L
O
G

I
S

N
O
T

V
A
L
I
D

I
F

S
E
P
A
R
A
T
E
D

F
R
O
M

O
R
I
G
I
N
A
L

R
E
P
O
R
T
.

E
N
V
I
R
O
N
M
E
N
T
A
L

S
M
A
R
T

L
O
G

0
0
A
A
G
I
N
T

B
H

S
L
C
F
M
Y

4
-
2
9
-
1
6
.
G
P
J

T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T

5
/
1
1
/
1
6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-13
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-5
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
p
p
m
)
DE
P
T
H

(
f
t
)
5
10
15
WA
T
E
R

L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
SA
M
P
L
E

T
Y
P
E
WATER LEVEL OBSERVATIONS
60
70
90
RE
C
O
V
E
R
Y

(
%
)
1.0
4.0
6.5
11.0
13.5
15.0
Groundwater at ~ 8 feet
Grass Surface and Top Soil
FILL - , Silty Gravel Fill
SILT (ML), dark brown, moist, soft, loose
SILTY CLAY (CL-ML), dark brown, moist, medium stiff, medium dense
SANDY SILTY CLAY/SILTY CLAYEY SAND (CL-ML), grayish-brown, wet, medium stiff, medium dense
LEAN CLAY (CL), light gray, wet, medium stiff, medium dense
Boring Terminated at 15 Feet
SS
SS
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
A
P
H
I
C

L
O
G
See Exhibit A-2
TH
I
S

B
O
R
I
N
G

L
O
G

I
S

N
O
T

V
A
L
I
D

I
F

S
E
P
A
R
A
T
E
D

F
R
O
M

O
R
I
G
I
N
A
L

R
E
P
O
R
T
.

E
N
V
I
R
O
N
M
E
N
T
A
L

S
M
A
R
T

L
O
G

0
0
A
A
G
I
N
T

B
H

S
L
C
F
M
Y

4
-
2
9
-
1
6
.
G
P
J

T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T

5
/
1
1
/
1
6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-14
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-6
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
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(
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5
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SA
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P
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WATER LEVEL OBSERVATIONS
80
70
90
RE
C
O
V
E
R
Y

(
%
)
1.0
4.5
7.5
8.8
9.5
12.3
13.5
15.0
Groundwater at ~ 8 feet
Grass Surface and Top Soil
FILL - , Silty Gravel Fill
SILT (ML), dark brown, moist, soft, loose
LEAN CLAY (CL), light brown, moist, stiff, dense
SILTY SAND (SW-SM), light gray, wet
LEAN CLAY (CL), grayish-brown, wet, medium stiff, medium dense
SILTY SAND (SW-SM), light gray, wet
LEAN CLAY (CL), light gray, wet, medium stiff, medium dense
Boring Terminated at 15 Feet
SS
SS
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
LOCATION
DEPTH
The stratification lines represent the approximate transition between differing soil types and/or rock
types; in-situ these transitions may be gradual or may occur at different depths than shown.
GR
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L
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G
See Exhibit A-2
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5
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6
800 S. 325 W.
Salt Lake City, Utah
SITE:
Page 1 of 1
Advancement Method:
Direct Push
Abandonment Method:
Borings backfilled with bentonite chips upon completion
6949 S High Tech Dr Ste 100
Midvale, UT
Notes:
Project No.: AL137118B
Drill Rig: Geoprobe
Boring Started: 4/28/2016
BORING LOG NO. B-15
DEQ DERR
Salt Lake City, Utah
Driller: DPS
Boring Completed: 4/28/2016
Exhibit:
CLIENT:
B-7
PROJECT: SLC - Fleet Management Yard
MATERIAL DESCRIPTION
Sa
m
p
l
e
PI
D

(
p
p
m
)
DE
P
T
H

(
f
t
)
5
10
15
WA
T
E
R

L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
SA
M
P
L
E

T
Y
P
E
WATER LEVEL OBSERVATIONS
40
80
100
RE
C
O
V
E
R
Y

(
%
)
APPENDIX D
Chain of Custody and Laboratory Data Sheets
ANALYTICAL REPORT
May 13, 2016
Terracon - Salt Lake City, UT
Sample Delivery Group:L832782
Samples Received:05/02/2016
Project Number:AL137118B
Description:SLC - Fleet Management Yard
Report To:Wynn John and Jeff Kolmel
6949 South High Tech Drive
Midvale, UT 84047
Entire Report Reviewed By:
May 13, 2016
[Preliminary Report]
Daphne Richards
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
May 13, 2016
Daphne Richards
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 6
⁵Sr: Sample Results 7
B-9 9.5-10FT L832782-01 7
B-9 14.5-15FT L832782-02 8
B-9 L832782-03 9
B-10 8FT L832782-04 10
B-10 14FT L832782-05 11
B-10 L832782-06 12
B-11 9-10FT L832782-07 13
B-11 14.5FT L832782-08 14
B-11 L832782-09 15
B-12 9FT L832782-10 16
B-12 13FT L832782-11 17
B-12 L832782-12 18
B-13 5-6FT L832782-13 19
B-13 11-12FT L832782-14 20
B-13 L832782-15 21
B-14 7-8FT L832782-16 22
B-14 11-12FT L832782-17 23
B-14 L832782-18 24
B-15 7-8FT L832782-19 25
B-15 11-12FT L832782-20 26
B-15 L832782-21 27
⁶Qc: Quality Control Summary 28
Total Solids by Method 2540 G-2011 28
Volatile Organic Compounds (GC/MS) by Method 8260B 30
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 36
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO 37
⁷Gl: Glossary of Terms 38
⁸Al: Accreditations & Locations 39
⁹Sc: Chain of Custody 40
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B-9 9.5-10FT L832782-01 Solid Mark Lilly 04/28/16 10:15 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 10:46 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 14:20 ACG
Collected by Collected date/time Received date/time
B-9 14.5-15FT L832782-02 Solid Mark Lilly 04/28/16 10:20 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 11:20 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 14:44 ACG
Collected by Collected date/time Received date/time
B-9 L832782-03 GW Mark Lilly 04/28/16 10:38 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 12:04 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 04:27 05/11/16 04:27 DAH
Collected by Collected date/time Received date/time
B-10 8FT L832782-04 Solid Mark Lilly 04/28/16 11:07 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 11:31 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 15:09 ACG
Collected by Collected date/time Received date/time
B-10 14FT L832782-05 Solid Mark Lilly 04/28/16 11:11 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 11:43 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 15:33 ACG
Collected by Collected date/time Received date/time
B-10 L832782-06 GW Mark Lilly 04/28/16 11:25 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 12:20 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 04:47 05/11/16 04:47 DAH
Collected by Collected date/time Received date/time
B-11 9-10FT L832782-07 Solid Mark Lilly 04/28/16 11:52 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 5 05/09/16 21:56 05/10/16 12:28 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 15:57 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG871995 100 05/12/16 14:27 05/12/16 18:44 LRL
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B-11 14.5FT L832782-08 Solid Mark Lilly 04/28/16 12:00 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 12:05 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG870889 5 05/09/16 08:42 05/09/16 13:05 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 16:22 ACG
Collected by Collected date/time Received date/time
B-11 L832782-09 GW Mark Lilly 04/28/16 12:13 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 12:37 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 05:07 05/11/16 05:07 DAH
Collected by Collected date/time Received date/time
B-12 9FT L832782-10 Solid Mark Lilly 04/28/16 12:47 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 12:16 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 16:46 ACG
Collected by Collected date/time Received date/time
B-12 13FT L832782-11 Solid Mark Lilly 04/28/16 12:51 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 12:39 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 17:11 ACG
Collected by Collected date/time Received date/time
B-12 L832782-12 GW Mark Lilly 04/28/16 13:00 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 12:53 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 05:27 05/11/16 05:27 DAH
Collected by Collected date/time Received date/time
B-13 5-6FT L832782-13 Solid Mark Lilly 04/28/16 13:36 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 20 05/09/16 21:56 05/10/16 13:47 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 17:35 ACG
Collected by Collected date/time Received date/time
B-13 11-12FT L832782-14 Solid Mark Lilly 04/28/16 13:41 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 12:50 JM
Total Solids by Method 2540 G-2011 WG869596 1 05/03/16 15:23 05/03/16 15:39 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 21:42 ACG
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B-13 L832782-15 GW Mark Lilly 04/28/16 14:00 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 13:10 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 05:47 05/11/16 05:47 DAH
Collected by Collected date/time Received date/time
B-14 7-8FT L832782-16 Solid Mark Lilly 04/28/16 14:24 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 13:02 JM
Total Solids by Method 2540 G-2011 WG869600 1 05/03/16 15:42 05/03/16 15:51 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 22:06 ACG
Collected by Collected date/time Received date/time
B-14 11-12FT L832782-17 Solid Mark Lilly 04/28/16 14:32 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 13:13 JM
Total Solids by Method 2540 G-2011 WG869600 1 05/03/16 15:42 05/03/16 15:51 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 22:30 ACG
Collected by Collected date/time Received date/time
B-14 L832782-18 GW Mark Lilly 04/28/16 14:51 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 13:26 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 06:07 05/11/16 06:07 DAH
Collected by Collected date/time Received date/time
B-15 7-8FT L832782-19 Solid Mark Lilly 04/28/16 15:11 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 13:24 JM
Total Solids by Method 2540 G-2011 WG869600 1 05/03/16 15:42 05/03/16 15:51 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 22:55 ACG
Collected by Collected date/time Received date/time
B-15 11-12FT L832782-20 Solid Mark Lilly 04/28/16 15:15 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO WG871131 1 05/09/16 21:56 05/10/16 13:35 JM
Total Solids by Method 2540 G-2011 WG869600 1 05/03/16 15:42 05/03/16 15:51 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG871516 5 05/10/16 22:39 05/11/16 23:19 ACG
Collected by Collected date/time Received date/time
B-15 L832782-21 GW Mark Lilly 04/28/16 15:28 05/02/16 09:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG869930 1 05/04/16 20:36 05/05/16 13:43 JNS
Volatile Organic Compounds (GC/MS) by Method 8260B WG871498 1 05/11/16 06:27 05/11/16 06:27 DAH
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Daphne Richards
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Daphne Richards
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L832782
B-9 9.5-10FT
Collected date/time: 04/28/16 10:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.9 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction 4.21 1.17 3.21 5 05/11/2016 14:20 WG871516
Benzene U 0.00173 0.00642 5 05/11/2016 14:20 WG871516
Ethylbenzene U 0.00190 0.00642 5 05/11/2016 14:20 WG871516
Methyl tert-butyl ether U 0.00136 0.00642 5 05/11/2016 14:20 WG871516
Naphthalene U 0.00642 0.0321 5 05/11/2016 14:20 WG871516
Toluene U 0.00279 0.0321 5 05/11/2016 14:20 WG871516
Xylenes, Total U 0.00448 0.0193 5 05/11/2016 14:20 WG871516
(S) Toluene-d8 104 88.7-115 05/11/2016 14:20 WG871516
(S) Dibromofluoromethane 102 76.3-123 05/11/2016 14:20 WG871516
(S) a,a,a-Trifluorotoluene 106 87.2-117 05/11/2016 14:20 WG871516
(S) 4-Bromofluorobenzene 104 69.7-129 05/11/2016 14:20 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT 7.94 0.987 5.13 1 05/10/2016 10:46 WG871131
(S) o-Terphenyl 82.0 50.0-150 05/10/2016 10:46 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L832782
B-9 14.5-15FT
Collected date/time: 04/28/16 10:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 72.0 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.27 3.47 5 05/11/2016 14:44 WG871516
Benzene U 0.00188 0.00694 5 05/11/2016 14:44 WG871516
Ethylbenzene U 0.00206 0.00694 5 05/11/2016 14:44 WG871516
Methyl tert-butyl ether U 0.00147 0.00694 5 05/11/2016 14:44 WG871516
Naphthalene U 0.00694 0.0347 5 05/11/2016 14:44 WG871516
Toluene U 0.00301 0.0347 5 05/11/2016 14:44 WG871516
Xylenes, Total U 0.00485 0.0208 5 05/11/2016 14:44 WG871516
(S) Toluene-d8 105 88.7-115 05/11/2016 14:44 WG871516
(S) Dibromofluoromethane 103 76.3-123 05/11/2016 14:44 WG871516
(S) a,a,a-Trifluorotoluene 105 87.2-117 05/11/2016 14:44 WG871516
(S) 4-Bromofluorobenzene 101 69.7-129 05/11/2016 14:44 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 1.07 5.56 1 05/10/2016 11:20 WG871131
(S) o-Terphenyl 79.5 50.0-150 05/10/2016 11:20 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L832782
B-9
Collected date/time: 04/28/16 10:38
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.750 0.108 0.500 1 05/11/2016 04:27 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 04:27 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 04:27 WG871498
Methyl tert-butyl ether U 0.000367 0.00100 1 05/11/2016 04:27 WG871498
Naphthalene U 0.00100 0.00500 1 05/11/2016 04:27 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 04:27 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 04:27 WG871498
(S) Toluene-d8 103 90.0-115 05/11/2016 04:27 WG871498
(S) Dibromofluoromethane 104 79.0-121 05/11/2016 04:27 WG871498
(S) 4-Bromofluorobenzene 95.5 80.1-120 05/11/2016 04:27 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 0.150 0.0247 0.100 1 05/05/2016 12:04 WG869930
(S) o-Terphenyl 93.9 50.0-150 05/05/2016 12:04 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L832782
B-10 8FT
Collected date/time: 04/28/16 11:07
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.6 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.12 3.06 5 05/11/2016 15:09 WG871516
Benzene U 0.00165 0.00613 5 05/11/2016 15:09 WG871516
Ethylbenzene U 0.00181 0.00613 5 05/11/2016 15:09 WG871516
Methyl tert-butyl ether U 0.00130 0.00613 5 05/11/2016 15:09 WG871516
Naphthalene U 0.00613 0.0306 5 05/11/2016 15:09 WG871516
Toluene U 0.00266 0.0306 5 05/11/2016 15:09 WG871516
Xylenes, Total U 0.00428 0.0184 5 05/11/2016 15:09 WG871516
(S) Toluene-d8 104 88.7-115 05/11/2016 15:09 WG871516
(S) Dibromofluoromethane 97.9 76.3-123 05/11/2016 15:09 WG871516
(S) a,a,a-Trifluorotoluene 104 87.2-117 05/11/2016 15:09 WG871516
(S) 4-Bromofluorobenzene 103 69.7-129 05/11/2016 15:09 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.943 4.90 1 05/10/2016 11:31 WG871131
(S) o-Terphenyl 81.4 50.0-150 05/10/2016 11:31 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L832782
B-10 14FT
Collected date/time: 04/28/16 11:11
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.9 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.17 3.21 5 05/11/2016 15:33 WG871516
Benzene U 0.00173 0.00642 5 05/11/2016 15:33 WG871516
Ethylbenzene U 0.00190 0.00642 5 05/11/2016 15:33 WG871516
Methyl tert-butyl ether U 0.00136 0.00642 5 05/11/2016 15:33 WG871516
Naphthalene U 0.00642 0.0321 5 05/11/2016 15:33 WG871516
Toluene U 0.00279 0.0321 5 05/11/2016 15:33 WG871516
Xylenes, Total U 0.00448 0.0193 5 05/11/2016 15:33 WG871516
(S) Toluene-d8 102 88.7-115 05/11/2016 15:33 WG871516
(S) Dibromofluoromethane 98.1 76.3-123 05/11/2016 15:33 WG871516
(S) a,a,a-Trifluorotoluene 107 87.2-117 05/11/2016 15:33 WG871516
(S) 4-Bromofluorobenzene 101 69.7-129 05/11/2016 15:33 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.987 5.13 1 05/10/2016 11:43 WG871131
(S) o-Terphenyl 69.6 50.0-150 05/10/2016 11:43 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L832782
B-10
Collected date/time: 04/28/16 11:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.504 0.108 0.500 1 05/11/2016 04:47 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 04:47 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 04:47 WG871498
Methyl tert-butyl ether U 0.000367 0.00100 1 05/11/2016 04:47 WG871498
Naphthalene U 0.00100 0.00500 1 05/11/2016 04:47 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 04:47 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 04:47 WG871498
(S) Toluene-d8 104 90.0-115 05/11/2016 04:47 WG871498
(S) Dibromofluoromethane 102 79.0-121 05/11/2016 04:47 WG871498
(S) 4-Bromofluorobenzene 88.7 80.1-120 05/11/2016 04:47 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 0.588 0.0247 0.100 1 05/05/2016 12:20 WG869930
(S) o-Terphenyl 90.9 50.0-150 05/05/2016 12:20 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L832782
B-11 9-10FT
Collected date/time: 04/28/16 11:52
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.8 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction 8.19 1.13 3.09 5 05/11/2016 15:57 WG871516
Benzene U 0.00167 0.00619 5 05/11/2016 15:57 WG871516
Ethylbenzene 0.00267 J 0.00183 0.00619 5 05/11/2016 15:57 WG871516
Methyl tert-butyl ether U 0.00131 0.00619 5 05/11/2016 15:57 WG871516
Naphthalene 3.17 0.124 0.619 100 05/12/2016 18:44 WG871995
Toluene U 0.00268 0.0309 5 05/11/2016 15:57 WG871516
Xylenes, Total 0.00769 J 0.00432 0.0186 5 05/11/2016 15:57 WG871516
(S) Toluene-d8 105 88.7-115 05/11/2016 15:57 WG871516
(S) Toluene-d8 100 88.7-115 05/12/2016 18:44 WG871995
(S) Dibromofluoromethane 104 76.3-123 05/12/2016 18:44 WG871995
(S) Dibromofluoromethane 98.6 76.3-123 05/11/2016 15:57 WG871516
(S) a,a,a-Trifluorotoluene 104 87.2-117 05/11/2016 15:57 WG871516
(S) a,a,a-Trifluorotoluene 113 87.2-117 05/12/2016 18:44 WG871995
(S) 4-Bromofluorobenzene 112 69.7-129 05/12/2016 18:44 WG871995
(S) 4-Bromofluorobenzene 155 J1 69.7-129 05/11/2016 15:57 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT 1080 4.75 24.7 5 05/10/2016 12:28 WG871131
(S) o-Terphenyl 189 J1 50.0-150 05/10/2016 12:28 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L832782
B-11 14.5FT
Collected date/time: 04/28/16 12:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.6 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.19 3.26 5 05/11/2016 16:22 WG871516
Benzene U 0.00176 0.00652 5 05/11/2016 16:22 WG871516
Ethylbenzene U 0.00193 0.00652 5 05/11/2016 16:22 WG871516
Methyl tert-butyl ether U 0.00138 0.00652 5 05/11/2016 16:22 WG871516
Naphthalene 0.00728 J 0.00652 0.0326 5 05/09/2016 13:05 WG870889
Toluene U 0.00283 0.0326 5 05/11/2016 16:22 WG871516
Xylenes, Total U 0.00455 0.0196 5 05/11/2016 16:22 WG871516
(S) Toluene-d8 108 88.7-115 05/11/2016 16:22 WG871516
(S) Toluene-d8 102 88.7-115 05/09/2016 13:05 WG870889
(S) Dibromofluoromethane 105 76.3-123 05/09/2016 13:05 WG870889
(S) Dibromofluoromethane 101 76.3-123 05/11/2016 16:22 WG871516
(S) a,a,a-Trifluorotoluene 103 87.2-117 05/11/2016 16:22 WG871516
(S) a,a,a-Trifluorotoluene 96.5 87.2-117 05/09/2016 13:05 WG870889
(S) 4-Bromofluorobenzene 96.4 69.7-129 05/09/2016 13:05 WG870889
(S) 4-Bromofluorobenzene 99.8 69.7-129 05/11/2016 16:22 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 1.00 5.22 1 05/10/2016 12:05 WG871131
(S) o-Terphenyl 76.8 50.0-150 05/10/2016 12:05 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L832782
B-11
Collected date/time: 04/28/16 12:13
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.221 J 0.108 0.500 1 05/11/2016 05:07 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 05:07 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 05:07 WG871498
Methyl tert-butyl ether U 0.000367 0.00100 1 05/11/2016 05:07 WG871498
Naphthalene 0.0327 0.00100 0.00500 1 05/11/2016 05:07 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 05:07 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 05:07 WG871498
(S) Toluene-d8 103 90.0-115 05/11/2016 05:07 WG871498
(S) Dibromofluoromethane 107 79.0-121 05/11/2016 05:07 WG871498
(S) 4-Bromofluorobenzene 93.9 80.1-120 05/11/2016 05:07 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 2.10 0.0247 0.100 1 05/05/2016 12:37 WG869930
(S) o-Terphenyl 103 50.0-150 05/05/2016 12:37 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L832782
B-12 9FT
Collected date/time: 04/28/16 12:47
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.8 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.11 3.02 5 05/11/2016 16:46 WG871516
Benzene U 0.00163 0.00604 5 05/11/2016 16:46 WG871516
Ethylbenzene U 0.00179 0.00604 5 05/11/2016 16:46 WG871516
Methyl tert-butyl ether U 0.00128 0.00604 5 05/11/2016 16:46 WG871516
Naphthalene U 0.00604 0.0302 5 05/11/2016 16:46 WG871516
Toluene U 0.00262 0.0302 5 05/11/2016 16:46 WG871516
Xylenes, Total U 0.00422 0.0181 5 05/11/2016 16:46 WG871516
(S) Toluene-d8 107 88.7-115 05/11/2016 16:46 WG871516
(S) Dibromofluoromethane 97.3 76.3-123 05/11/2016 16:46 WG871516
(S) a,a,a-Trifluorotoluene 103 87.2-117 05/11/2016 16:46 WG871516
(S) 4-Bromofluorobenzene 102 69.7-129 05/11/2016 16:46 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.929 4.83 1 05/10/2016 12:16 WG871131
(S) o-Terphenyl 76.7 50.0-150 05/10/2016 12:16 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L832782
B-12 13FT
Collected date/time: 04/28/16 12:51
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.0 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.13 3.09 5 05/11/2016 17:11 WG871516
Benzene U 0.00167 0.00618 5 05/11/2016 17:11 WG871516
Ethylbenzene U 0.00183 0.00618 5 05/11/2016 17:11 WG871516
Methyl tert-butyl ether U 0.00131 0.00618 5 05/11/2016 17:11 WG871516
Naphthalene U 0.00618 0.0309 5 05/11/2016 17:11 WG871516
Toluene U 0.00268 0.0309 5 05/11/2016 17:11 WG871516
Xylenes, Total U 0.00431 0.0185 5 05/11/2016 17:11 WG871516
(S) Toluene-d8 101 88.7-115 05/11/2016 17:11 WG871516
(S) Dibromofluoromethane 96.7 76.3-123 05/11/2016 17:11 WG871516
(S) a,a,a-Trifluorotoluene 103 87.2-117 05/11/2016 17:11 WG871516
(S) 4-Bromofluorobenzene 100 69.7-129 05/11/2016 17:11 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.950 4.94 1 05/10/2016 12:39 WG871131
(S) o-Terphenyl 70.9 50.0-150 05/10/2016 12:39 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L832782
B-12
Collected date/time: 04/28/16 13:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.263 J 0.108 0.500 1 05/11/2016 05:27 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 05:27 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 05:27 WG871498
Methyl tert-butyl ether U 0.000367 0.00100 1 05/11/2016 05:27 WG871498
Naphthalene 0.00264 J 0.00100 0.00500 1 05/11/2016 05:27 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 05:27 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 05:27 WG871498
(S) Toluene-d8 103 90.0-115 05/11/2016 05:27 WG871498
(S) Dibromofluoromethane 103 79.0-121 05/11/2016 05:27 WG871498
(S) 4-Bromofluorobenzene 90.5 80.1-120 05/11/2016 05:27 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 0.693 0.0247 0.100 1 05/05/2016 12:53 WG869930
(S) o-Terphenyl 92.0 50.0-150 05/05/2016 12:53 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L832782
B-13 5-6FT
Collected date/time: 04/28/16 13:36
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.0 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.17 3.21 5 05/11/2016 17:35 WG871516
Benzene U 0.00173 0.00641 5 05/11/2016 17:35 WG871516
Ethylbenzene U 0.00190 0.00641 5 05/11/2016 17:35 WG871516
Methyl tert-butyl ether U 0.00136 0.00641 5 05/11/2016 17:35 WG871516
Naphthalene U 0.00641 0.0321 5 05/11/2016 17:35 WG871516
Toluene U 0.00278 0.0321 5 05/11/2016 17:35 WG871516
Xylenes, Total U 0.00448 0.0192 5 05/11/2016 17:35 WG871516
(S) Toluene-d8 107 88.7-115 05/11/2016 17:35 WG871516
(S) Dibromofluoromethane 103 76.3-123 05/11/2016 17:35 WG871516
(S) a,a,a-Trifluorotoluene 106 87.2-117 05/11/2016 17:35 WG871516
(S) 4-Bromofluorobenzene 98.8 69.7-129 05/11/2016 17:35 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT 113 19.8 103 20 05/10/2016 13:47 WG871131
(S) o-Terphenyl 0.000 J7 50.0-150 05/10/2016 13:47 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Salt Lake City, UT AL137118B L832782 05/13/16 13:09 19 of 42
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L832782
B-13 11-12FT
Collected date/time: 04/28/16 13:41
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.4 1 05/03/2016 15:39 WG869596
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.15 3.15 5 05/11/2016 21:42 WG871516
Benzene U 0.00170 0.00630 5 05/11/2016 21:42 WG871516
Ethylbenzene U 0.00186 0.00630 5 05/11/2016 21:42 WG871516
Methyl tert-butyl ether U 0.00134 0.00630 5 05/11/2016 21:42 WG871516
Naphthalene U 0.00630 0.0315 5 05/11/2016 21:42 WG871516
Toluene U 0.00273 0.0315 5 05/11/2016 21:42 WG871516
Xylenes, Total U 0.00440 0.0189 5 05/11/2016 21:42 WG871516
(S) Toluene-d8 104 88.7-115 05/11/2016 21:42 WG871516
(S) Dibromofluoromethane 101 76.3-123 05/11/2016 21:42 WG871516
(S) a,a,a-Trifluorotoluene 100 87.2-117 05/11/2016 21:42 WG871516
(S) 4-Bromofluorobenzene 97.0 69.7-129 05/11/2016 21:42 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.969 5.04 1 05/10/2016 12:50 WG871131
(S) o-Terphenyl 75.1 50.0-150 05/10/2016 12:50 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L832782
B-13
Collected date/time: 04/28/16 14:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.289 J 0.108 0.500 1 05/11/2016 05:47 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 05:47 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 05:47 WG871498
Methyl tert-butyl ether 0.000872 J 0.000367 0.00100 1 05/11/2016 05:47 WG871498
Naphthalene U 0.00100 0.00500 1 05/11/2016 05:47 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 05:47 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 05:47 WG871498
(S) Toluene-d8 104 90.0-115 05/11/2016 05:47 WG871498
(S) Dibromofluoromethane 102 79.0-121 05/11/2016 05:47 WG871498
(S) 4-Bromofluorobenzene 87.1 80.1-120 05/11/2016 05:47 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 0.446 0.0247 0.100 1 05/05/2016 13:10 WG869930
(S) o-Terphenyl 95.9 50.0-150 05/05/2016 13:10 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L832782
B-14 7-8FT
Collected date/time: 04/28/16 14:24
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.4 1 05/03/2016 15:51 WG869600
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.18 3.23 5 05/11/2016 22:06 WG871516
Benzene U 0.00174 0.00646 5 05/11/2016 22:06 WG871516
Ethylbenzene U 0.00191 0.00646 5 05/11/2016 22:06 WG871516
Methyl tert-butyl ether U 0.00137 0.00646 5 05/11/2016 22:06 WG871516
Naphthalene U 0.00646 0.0323 5 05/11/2016 22:06 WG871516
Toluene U 0.00280 0.0323 5 05/11/2016 22:06 WG871516
Xylenes, Total U 0.00451 0.0194 5 05/11/2016 22:06 WG871516
(S) Toluene-d8 107 88.7-115 05/11/2016 22:06 WG871516
(S) Dibromofluoromethane 104 76.3-123 05/11/2016 22:06 WG871516
(S) a,a,a-Trifluorotoluene 106 87.2-117 05/11/2016 22:06 WG871516
(S) 4-Bromofluorobenzene 96.7 69.7-129 05/11/2016 22:06 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.994 5.17 1 05/10/2016 13:02 WG871131
(S) o-Terphenyl 77.8 50.0-150 05/10/2016 13:02 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L832782
B-14 11-12FT
Collected date/time: 04/28/16 14:32
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.8 1 05/03/2016 15:51 WG869600
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.16 3.17 5 05/11/2016 22:30 WG871516
Benzene U 0.00171 0.00635 5 05/11/2016 22:30 WG871516
Ethylbenzene U 0.00188 0.00635 5 05/11/2016 22:30 WG871516
Methyl tert-butyl ether U 0.00135 0.00635 5 05/11/2016 22:30 WG871516
Naphthalene U 0.00635 0.0317 5 05/11/2016 22:30 WG871516
Toluene U 0.00275 0.0317 5 05/11/2016 22:30 WG871516
Xylenes, Total U 0.00443 0.0190 5 05/11/2016 22:30 WG871516
(S) Toluene-d8 105 88.7-115 05/11/2016 22:30 WG871516
(S) Dibromofluoromethane 102 76.3-123 05/11/2016 22:30 WG871516
(S) a,a,a-Trifluorotoluene 105 87.2-117 05/11/2016 22:30 WG871516
(S) 4-Bromofluorobenzene 100 69.7-129 05/11/2016 22:30 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.976 5.08 1 05/10/2016 13:13 WG871131
(S) o-Terphenyl 87.1 50.0-150 05/10/2016 13:13 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L832782
B-14
Collected date/time: 04/28/16 14:51
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.214 J 0.108 0.500 1 05/11/2016 06:07 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 06:07 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 06:07 WG871498
Methyl tert-butyl ether 0.00228 0.000367 0.00100 1 05/11/2016 06:07 WG871498
Naphthalene U 0.00100 0.00500 1 05/11/2016 06:07 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 06:07 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 06:07 WG871498
(S) Toluene-d8 105 90.0-115 05/11/2016 06:07 WG871498
(S) Dibromofluoromethane 106 79.0-121 05/11/2016 06:07 WG871498
(S) 4-Bromofluorobenzene 89.9 80.1-120 05/11/2016 06:07 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 0.148 0.0247 0.100 1 05/05/2016 13:26 WG869930
(S) o-Terphenyl 91.7 50.0-150 05/05/2016 13:26 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L832782
B-15 7-8FT
Collected date/time: 04/28/16 15:11
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.9 1 05/03/2016 15:51 WG869600
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.22 3.34 5 05/11/2016 22:55 WG871516
Benzene U 0.00180 0.00668 5 05/11/2016 22:55 WG871516
Ethylbenzene U 0.00198 0.00668 5 05/11/2016 22:55 WG871516
Methyl tert-butyl ether U 0.00142 0.00668 5 05/11/2016 22:55 WG871516
Naphthalene U 0.00668 0.0334 5 05/11/2016 22:55 WG871516
Toluene U 0.00290 0.0334 5 05/11/2016 22:55 WG871516
Xylenes, Total U 0.00466 0.0200 5 05/11/2016 22:55 WG871516
(S) Toluene-d8 104 88.7-115 05/11/2016 22:55 WG871516
(S) Dibromofluoromethane 96.9 76.3-123 05/11/2016 22:55 WG871516
(S) a,a,a-Trifluorotoluene 105 87.2-117 05/11/2016 22:55 WG871516
(S) 4-Bromofluorobenzene 102 69.7-129 05/11/2016 22:55 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 1.03 5.34 1 05/10/2016 13:24 WG871131
(S) o-Terphenyl 80.4 50.0-150 05/10/2016 13:24 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L832782
B-15 11-12FT
Collected date/time: 04/28/16 15:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.3 1 05/03/2016 15:51 WG869600
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/MS) Low Fraction U 1.15 3.15 5 05/11/2016 23:19 WG871516
Benzene U 0.00170 0.00630 5 05/11/2016 23:19 WG871516
Ethylbenzene U 0.00187 0.00630 5 05/11/2016 23:19 WG871516
Methyl tert-butyl ether U 0.00134 0.00630 5 05/11/2016 23:19 WG871516
Naphthalene U 0.00630 0.0315 5 05/11/2016 23:19 WG871516
Toluene U 0.00274 0.0315 5 05/11/2016 23:19 WG871516
Xylenes, Total U 0.00440 0.0189 5 05/11/2016 23:19 WG871516
(S) Toluene-d8 103 88.7-115 05/11/2016 23:19 WG871516
(S) Dibromofluoromethane 98.0 76.3-123 05/11/2016 23:19 WG871516
(S) a,a,a-Trifluorotoluene 105 87.2-117 05/11/2016 23:19 WG871516
(S) 4-Bromofluorobenzene 97.8 69.7-129 05/11/2016 23:19 WG871516
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
DRO W/ SGT U 0.969 5.04 1 05/10/2016 13:35 WG871131
(S) o-Terphenyl 81.7 50.0-150 05/10/2016 13:35 WG871131
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L832782
B-15
Collected date/time: 04/28/16 15:28
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
TPH (GC/MS) Low Fraction 0.207 J 0.108 0.500 1 05/11/2016 06:27 WG871498
Benzene U 0.000331 0.00100 1 05/11/2016 06:27 WG871498
Ethylbenzene U 0.000384 0.00100 1 05/11/2016 06:27 WG871498
Methyl tert-butyl ether 0.000522 J 0.000367 0.00100 1 05/11/2016 06:27 WG871498
Naphthalene U 0.00100 0.00500 1 05/11/2016 06:27 WG871498
Toluene U 0.000780 0.00500 1 05/11/2016 06:27 WG871498
Xylenes, Total U 0.00106 0.00300 1 05/11/2016 06:27 WG871498
(S) Toluene-d8 104 90.0-115 05/11/2016 06:27 WG871498
(S) Dibromofluoromethane 105 79.0-121 05/11/2016 06:27 WG871498
(S) 4-Bromofluorobenzene 90.9 80.1-120 05/11/2016 06:27 WG871498
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
DRO w/ SGT 0.183 0.0247 0.100 1 05/05/2016 13:43 WG869930
(S) o-Terphenyl 95.8 50.0-150 05/05/2016 13:43 WG869930
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG869596
Total Solids by Method 2540 G-2011 L832782-01,02,04,05,07,08,10,11,13,14
Method Blank (MB)
(MB) R3133460-1 05/03/16 15:39
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000600
L832782-02 Original Sample (OS) • Duplicate (DUP)
(OS) L832782-02 05/03/16 15:39 • (DUP) R3133460-3 05/03/16 15:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 72.0 73.2 1 1.65 5
Laboratory Control Sample (LCS)
(LCS) R3133460-2 05/03/16 15:39
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG869600
Total Solids by Method 2540 G-2011 L832782-16,17,19,20
Method Blank (MB)
(MB) R3133468-1 05/03/16 15:51
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000700
L832786-06 Original Sample (OS) • Duplicate (DUP)
(OS) L832786-06 05/03/16 15:51 • (DUP) R3133468-3 05/03/16 15:51
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 80.9 81.1 1 0.279 5
Laboratory Control Sample (LCS)
(LCS) R3133468-2 05/03/16 15:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG870889
Volatile Organic Compounds (GC/MS) by Method 8260B L832782-08
Method Blank (MB)
(MB) R3135003-3 05/09/16 10:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Naphthalene U 0.00100 0.00500
(S) Toluene-d8 101 88.5-111
(S) Dibromofluoromethane 106 78.3-121
(S) a,a,a-Trifluorotoluene 98.1 85.0-114
(S) 4-Bromofluorobenzene 96.4 71.0-126
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3135003-1 05/09/16 08:22 • (LCSD) R3135003-2 05/09/16 08:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.0250 0.0205 0.0212 81.9 84.6 69.9-132 3.28 20
(S) Toluene-d8 101 101 88.5-111
(S) Dibromofluoromethane 105 106 78.3-121
(S) a,a,a-Trifluorotoluene 99.3 98.5 85.0-114
(S) 4-Bromofluorobenzene 94.0 95.9 71.0-126
L834097-41 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L834097-41 05/09/16 13:45 • (MS) R3135003-4 05/09/16 14:25 • (MSD) R3135003-5 05/09/16 14:45
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.0250 U 0.00790 0.00452 31.6 18.1 1 18.4-145 J3 J6 54.4 34
(S) Toluene-d8 102 102 88.5-111
(S) Dibromofluoromethane 108 107 78.3-121
(S) a,a,a-Trifluorotoluene 96.8 96.5 85.0-114
(S) 4-Bromofluorobenzene 93.3 95.7 71.0-126
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG871516
Volatile Organic Compounds (GC/MS) by Method 8260B L832782-01,02,04,05,07,08,10,11,13,14,16,17,19,20
Method Blank (MB)
(MB) R3136024-5 05/11/16 12:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/MS) Low Fraction U 0.183 0.500
Benzene U 0.000270 0.00100
Ethylbenzene U 0.000297 0.00100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
Toluene U 0.000434 0.00500
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 106 88.7-115
(S) Dibromofluoromethane 98.9 76.3-123
(S) a,a,a-Trifluorotoluene 108 87.2-117
(S) 4-Bromofluorobenzene 98.3 69.7-129
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3136024-1 05/11/16 09:23 • (LCSD) R3136024-2 05/11/16 09:48
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Benzene 0.0250 0.0222 0.0227 88.9 91.0 72.6-120 2.33 20
Ethylbenzene 0.0250 0.0261 0.0269 104 107 78.6-124 3.05 20
Methyl tert-butyl ether 0.0250 0.0231 0.0227 92.3 90.9 70.2-122 1.51 20
Naphthalene 0.0250 0.0288 0.0275 115 110 69.9-132 4.63 20
Toluene 0.0250 0.0229 0.0232 91.6 92.6 76.7-116 1.16 20
Xylenes, Total 0.0750 0.0766 0.0821 102 109 78.1-123 6.96 20
(S) Toluene-d8 102 102 88.7-115
(S) Dibromofluoromethane 99.6 101 76.3-123
(S) a,a,a-Trifluorotoluene 103 106 87.2-117
(S) 4-Bromofluorobenzene 101 102 69.7-129
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3136024-3 05/11/16 10:12 • (LCSD) R3136024-4 05/11/16 10:36
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/MS) Low Fraction 5.00 6.00 6.01 120 120 61.5-138 0.190 20
(S) Toluene-d8 104 106 88.7-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG871516
Volatile Organic Compounds (GC/MS) by Method 8260B L832782-01,02,04,05,07,08,10,11,13,14,16,17,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3136024-3 05/11/16 10:12 • (LCSD) R3136024-4 05/11/16 10:36
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
(S) Dibromofluoromethane 93.8 94.9 76.3-123
(S) a,a,a-Trifluorotoluene 102 104 87.2-117
(S) 4-Bromofluorobenzene 107 108 69.7-129
L832782-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L832782-01 05/11/16 14:20 • (MS) R3136024-6 05/11/16 17:59 • (MSD) R3136024-7 05/11/16 18:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/MS) Low Fraction 6.42 4.21 36.1 38.1 99.4 106 5 10.0-147 5.36 26.4
(S) Toluene-d8 102 104 88.7-115
(S) Dibromofluoromethane 101 96.9 76.3-123
(S) a,a,a-Trifluorotoluene 101 106 87.2-117
(S) 4-Bromofluorobenzene 105 105 69.7-129
L832782-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L832782-01 05/11/16 14:20 • (MS) R3136024-8 05/11/16 18:48 • (MSD) R3136024-9 05/11/16 19:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Benzene 0.0321 U 0.124 0.122 77.0 76.2 5 47.8-131 1.07 22.8
Ethylbenzene 0.0321 U 0.134 0.136 83.6 84.9 5 44.8-135 1.60 26.9
Methyl tert-butyl ether 0.0321 U 0.123 0.116 76.7 72.2 5 50.4-131 5.95 24.8
Naphthalene 0.0321 U 0.150 0.142 93.3 88.4 5 18.4-145 5.40 34
Toluene 0.0321 U 0.122 0.122 76.2 76.3 5 47.8-127 0.100 24.3
Xylenes, Total 0.0963 U 0.397 0.406 82.5 84.4 5 42.7-135 2.25 26.6
(S) Toluene-d8 101 104 88.7-115
(S) Dibromofluoromethane 102 101 76.3-123
(S) a,a,a-Trifluorotoluene 102 105 87.2-117
(S) 4-Bromofluorobenzene 105 102 69.7-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG871995
Volatile Organic Compounds (GC/MS) by Method 8260B L832782-07
Method Blank (MB)
(MB) R3136367-5 05/12/16 16:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Naphthalene U 0.00100 0.00500
(S) Toluene-d8 98.6 88.7-115
(S) Dibromofluoromethane 106 76.3-123
(S) a,a,a-Trifluorotoluene 112 87.2-117
(S) 4-Bromofluorobenzene 99.9 69.7-129
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3136367-1 05/12/16 14:11 • (LCSD) R3136367-2 05/12/16 14:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.0250 0.0302 0.0294 121 117 69.9-132 2.98 20
(S) Toluene-d8 100 98.7 88.7-115
(S) Dibromofluoromethane 112 106 76.3-123
(S) a,a,a-Trifluorotoluene 116 113 87.2-117
(S) 4-Bromofluorobenzene 91.3 98.6 69.7-129
L833688-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L833688-17 05/12/16 19:02 • (MS) R3136367-6 05/12/16 17:17 • (MSD) R3136367-7 05/12/16 17:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.0303 0.00634 0.170 0.148 108 93.8 5 18.4-145 13.8 34
(S) Toluene-d8 96.6 98.5 88.7-115
(S) Dibromofluoromethane 111 109 76.3-123
(S) a,a,a-Trifluorotoluene 110 112 87.2-117
(S) 4-Bromofluorobenzene 90.1 94.8 69.7-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG871498
Volatile Organic Compounds (GC/MS) by Method 8260B L832782-03,06,09,12,15,18,21
Method Blank (MB)
(MB) R3135639-5 05/11/16 01:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/MS) Low Fraction 0.272 0.108 0.500
Benzene U 0.000331 0.00100
Ethylbenzene U 0.000384 0.00100
Methyl tert-butyl ether U 0.000367 0.00100
Naphthalene U 0.00100 0.00500
Toluene U 0.000780 0.00500
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 106 90.0-115
(S) Dibromofluoromethane 104 79.0-121
(S) 4-Bromofluorobenzene 90.2 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3135639-1 05/10/16 23:06 • (LCSD) R3135639-2 05/10/16 23:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Benzene 0.0250 0.0234 0.0235 93.4 94.0 73.0-122 0.620 20
Ethylbenzene 0.0250 0.0237 0.0235 95.0 93.9 80.9-121 1.12 20
Methyl tert-butyl ether 0.0250 0.0231 0.0227 92.3 90.6 70.1-125 1.88 20
Naphthalene 0.0250 0.0230 0.0236 92.0 94.3 69.7-134 2.45 20
Toluene 0.0250 0.0241 0.0240 96.3 95.9 77.9-116 0.480 20
Xylenes, Total 0.0750 0.0715 0.0700 95.3 93.4 79.2-122 2.06 20
(S) Toluene-d8 99.1 101 90.0-115
(S) Dibromofluoromethane 103 104 79.0-121
(S) 4-Bromofluorobenzene 96.8 95.1 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3135639-3 05/10/16 23:46 • (LCSD) R3135639-4 05/11/16 00:06
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
TPH (GC/MS) Low Fraction 5.00 5.52 5.38 110 108 62.3-131 2.51 20
(S) Toluene-d8 105 102 90.0-115
(S) Dibromofluoromethane 99.3 94.4 79.0-121
(S) 4-Bromofluorobenzene 102 98.5 80.1-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG871498
Volatile Organic Compounds (GC/MS) by Method 8260B L832782-03,06,09,12,15,18,21
L832782-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L832782-03 05/11/16 04:27 • (MS) R3135639-6 05/11/16 01:27 • (MSD) R3135639-7 05/11/16 01:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Benzene 0.0250 U 0.0215 0.0203 86.1 81.3 1 58.6-133 5.79 20
Ethylbenzene 0.0250 U 0.0214 0.0207 85.5 82.9 1 62.7-136 3.00 20
Methyl tert-butyl ether 0.0250 U 0.0227 0.0217 91.0 86.9 1 61.4-136 4.64 20
Naphthalene 0.0250 U 0.0212 0.0213 84.7 85.2 1 61.8-143 0.550 20
Toluene 0.0250 U 0.0226 0.0210 90.3 83.8 1 67.8-124 7.46 20
Xylenes, Total 0.0750 U 0.0635 0.0612 84.7 81.7 1 65.6-133 3.69 20
(S) Toluene-d8 103 102 90.0-115
(S) Dibromofluoromethane 103 106 79.0-121
(S) 4-Bromofluorobenzene 97.6 95.5 80.1-120
L832782-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L832782-03 05/11/16 04:27 • (MS) R3135639-8 05/11/16 02:07 • (MSD) R3135639-9 05/11/16 02:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
TPH (GC/MS) Low Fraction 5.00 0.750 5.94 6.19 104 109 1 44.3-147 4.05 20
(S) Toluene-d8 102 104 90.0-115
(S) Dibromofluoromethane 99.3 99.6 79.0-121
(S) 4-Bromofluorobenzene 94.7 108 80.1-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG869930
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L832782-03,06,09,12,15,18,21
Method Blank (MB)
(MB) R3134266-1 05/05/16 11:14
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
DRO W/ SGT U 0.0247 0.100
(S) o-Terphenyl 87.8 50.0-150
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3134266-2 05/05/16 11:31 • (LCSD) R3134266-3 05/05/16 11:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
DRO W/ SGT 1.50 1.56 1.60 104 107 70.0-130 2.74 20
(S) o-Terphenyl 93.7 94.0 50.0-150
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG871131
Semi-Volatile Organic Compounds (GC) by Method 3546/DRO L832782-01,02,04,05,07,08,10,11,13,14,16,17,19,20
Method Blank (MB)
(MB) R3135372-1 05/10/16 09:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
DRO W/ SGT U 0.769 4.00
(S) o-Terphenyl 83.1 50.0-150
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3135372-2 05/10/16 09:17 • (LCSD) R3135372-3 05/10/16 09:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
DRO W/ SGT 60.0 51.2 49.4 85.3 82.4 50.0-150 3.45 20
(S) o-Terphenyl 90.5 81.7 50.0-150
L832782-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L832782-01 05/10/16 10:46 • (MS) R3135372-4 05/10/16 10:58 • (MSD) R3135372-5 05/10/16 11:09
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
DRO W/ SGT 77.0 7.94 71.3 73.5 82.3 85.2 1 50.0-150 3.04 20
(S) o-Terphenyl 71.6 83.7 50.0-150
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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