Loading...
HomeMy WebLinkAboutDDW-2025-006902July 16, 2025 Dear John Steffan: Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 6/27/25 10:45 am and logged in under work order IF05743. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH13003RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IF05743-01 Name: Sampled: Received: 06/27/25 10:45 06/25/25 13:06 SS973-GROUP SOURCE SAMPLING STATION SS973 Reg ID:Drinking Water - Regular SampleMatrix:UTAH13003 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA07/11/25 15:00 MAB3U1.710.9 < 0.4 ng/L EPA 533PFMPA07/11/25 15:00 MAB3U1.710.4 < 0.4 ng/L EPA 533PFPeA07/11/25 15:00 MAB3U1.710.4 < 0.4 ng/L EPA 533PFBS07/11/25 15:00 MAB3U1.710.4 < 0.3 ng/L EPA 533PFMBA07/11/25 15:00 MAB3U1.710.3 < 0.5 ng/L EPA 533PFEESA07/11/25 15:00 MAB3U1.710.5 < 0.3 ng/L EPA 533HFPO-DA 07/11/25 15:00 MAB3U1.710.3 < 0.4 ng/L EPA 533NFDHA07/11/25 15:00 MAB3U1.710.4 < 0.3 ng/L EPA 5334:2 FTS 07/11/25 15:00 MAB3U1.710.3 < 0.4 ng/L EPA 533PFHxS07/11/25 15:00 MAB3U1.710.4 < 0.5 ng/L EPA 533PFHpA07/11/25 15:00 MAB3U1.710.5 < 0.9 ng/L EPA 533PFHxA07/11/25 15:00 MAB3U1.710.9 < 0.5 ng/L EPA 533ADONA07/11/25 15:00 MAB3U1.710.5 < 0.5 ng/L EPA 533PFPeS07/11/25 15:00 MAB3U1.710.5 < 0.4 ng/L EPA 5336:2 FTS 07/11/25 15:00 MAB3U1.710.4 < 0.6 ng/L EPA 533PFOA07/11/25 15:00 MAB3U1.710.6 < 0.5 ng/L EPA 533PFHpS07/11/25 15:00 MAB3U1.710.5 < 0.4 ng/L EPA 533PFOS07/11/25 15:00 MAB3U1.710.4 < 0.5 ng/L EPA 533PFNA07/11/25 15:00 MAB3U1.710.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 07/11/25 15:00 MAB3U1.710.6 < 0.4 ng/L EPA 5338:2 FTS 07/11/25 15:00 MAB3U1.710.4 < 0.4 ng/L EPA 533PFDA07/11/25 15:00 MAB3U1.710.4 < 0.4 ng/L EPA 533PFUnA07/11/25 15:00 MAB3U1.710.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 07/11/25 15:00 MAB3U1.710.5 < 0.5 ng/L EPA 533PFDoA07/11/25 15:00 MAB3U1.710.5 Surrogate: 13C4-PFBA-SURR 94 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 94 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 94 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 88 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 95 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 96 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 94 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 95 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 90 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 95 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 94 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 94 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 96 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 83 %50-200 07/11/25 15:00 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 2 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IF05743-01 Name: Sampled: Received: 06/27/25 10:45 06/25/25 13:06 SS973-GROUP SOURCE SAMPLING STATION SS973 Reg ID:Drinking Water - Regular SampleMatrix:UTAH13003 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C7-PFUnA-SURR 82 %50-200 07/11/25 15:00 MAB3 EPA 533 Surrogate: 13C2-PFDoA-SURR 95 %50-200 07/11/25 15:00 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 3 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B537217 - EPA 533 - EPA 533 Blank (B537217-BLK1)Prepared: 07/08/25 Analyzed: 07/11/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 36.8 ng/L 40.00 92 50-200 Surrogate: 13C5-PFPeA-SURR 37.0 ng/L 40.00 92 50-200 Surrogate: 13C3-PFBS-SURR 34.7 ng/L 37.28 93 50-200 Surrogate: 13C2-4:2FTS-SURR 134 ng/L 150.4 89 50-200 Surrogate: 13C5-PFHxA-SURR 36.9 ng/L 40.00 92 50-200 Surrogate: 13C3-HFPOA-DA-SURR 37.8 ng/L 40.00 95 50-200 Surrogate: 13C4-PFHpA-SURR 36.4 ng/L 40.00 91 50-200 Surrogate: 13C3-PFHxS-SURR 35.8 ng/L 37.92 94 50-200 Surrogate: 13C2-6:2FTS-SURR 138 ng/L 152.0 91 50-200 Surrogate: 13C8-PFOA-SURR 36.2 ng/L 40.00 91 50-200 Surrogate: 13C9-PFNA-SURR 34.6 ng/L 40.00 86 50-200 Surrogate: 13C8-PFOS-SURR 36.0 ng/L 38.32 94 50-200 Surrogate: 13C2-8:2FTS-SURR 148 ng/L 153.6 97 50-200 Surrogate: 13C6-PFDA-SURR 29.2 ng/L 40.00 73 50-200 Surrogate: 13C7-PFUnA-SURR 30.4 ng/L 40.00 76 50-200 Surrogate: 13C2-PFDoA-SURR 36.6 ng/L 40.00 91 50-200 LCS (B537217-BS1)Prepared: 07/08/25 Analyzed: 07/11/25 PFBA 81 ng/L 80.00 101 70-130 PFMPA 82 ng/L 80.00 103 70-130 www.pacelabs.comCustomer #: 72-106174 Page 4 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B537217-BS1)Prepared: 07/08/25 Analyzed: 07/11/25 PFPeA 73 ng/L 80.00 91 70-130 PFBS 69 ng/L 80.00 86 70-130 PFMBA 67 ng/L 80.00 84 70-130 PFEESA 69 ng/L 80.00 87 70-130 HFPO-DA 70 ng/L 80.00 88 70-130 NFDHA 73 ng/L 80.00 92 70-130 PFHxS 70 ng/L 80.00 88 70-130 4:2 FTS 84 ng/L 80.00 104 70-130 PFHpA 73 ng/L 80.00 92 70-130 PFHxA 75 ng/L 80.00 93 70-130 ADONA 76 ng/L 80.00 96 70-130 PFPeS 74 ng/L 80.00 92 70-130 6:2 FTS 78 ng/L 80.00 97 70-130 PFOA 72 ng/L 80.00 90 70-130 PFHpS 67 ng/L 80.00 84 70-130 PFOS 67 ng/L 80.00 84 70-130 PFNA 72 ng/L 80.00 91 70-130 9Cl-PF3ONS 69 ng/L 80.00 86 70-130 8:2 FTS 84 ng/L 80.00 105 70-130 PFDA 72 ng/L 80.00 90 70-130 PFUnA 69 ng/L 80.00 86 70-130 11Cl-PF3OUdS 74 ng/L 80.00 92 70-130 PFDoA 70 ng/L 80.00 87 70-130 Surrogate: 13C4-PFBA-SURR 36.6 ng/L 40.00 91 50-200 Surrogate: 13C5-PFPeA-SURR 38.1 ng/L 40.00 95 50-200 Surrogate: 13C3-PFBS-SURR 37.2 ng/L 37.28 100 50-200 Surrogate: 13C2-4:2FTS-SURR 150 ng/L 150.4 100 50-200 Surrogate: 13C5-PFHxA-SURR 37.9 ng/L 40.00 95 50-200 Surrogate: 13C3-HFPOA-DA-SURR 38.7 ng/L 40.00 97 50-200 Surrogate: 13C4-PFHpA-SURR 37.4 ng/L 40.00 93 50-200 Surrogate: 13C3-PFHxS-SURR 38.6 ng/L 37.92 102 50-200 Surrogate: 13C2-6:2FTS-SURR 150 ng/L 152.0 99 50-200 Surrogate: 13C8-PFOA-SURR 37.2 ng/L 40.00 93 50-200 Surrogate: 13C9-PFNA-SURR 35.3 ng/L 40.00 88 50-200 Surrogate: 13C8-PFOS-SURR 38.1 ng/L 38.32 99 50-200 Surrogate: 13C2-8:2FTS-SURR 160 ng/L 153.6 104 50-200 Surrogate: 13C6-PFDA-SURR 30.3 ng/L 40.00 76 50-200 Surrogate: 13C7-PFUnA-SURR 31.4 ng/L 40.00 78 50-200 Surrogate: 13C2-PFDoA-SURR 35.8 ng/L 40.00 89 50-200 Duplicate (B537217-DUP1)Sample: IF05674-01RE1 Prepared: 07/08/25 Analyzed: 07/11/25 PFBA < 0.9 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.4 ng/L ND 30U PFMBA < 0.3 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.3 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 5 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B537217-DUP1)Sample: IF05674-01RE1 Prepared: 07/08/25 Analyzed: 07/11/25 NFDHA < 0.4 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.3 ng/L ND 30U PFHpA < 0.5 ng/L ND 30U PFHxA < 0.9 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.5 ng/L ND 30U 6:2 FTS < 0.4 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.5 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.6 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.4 ng/L ND 30U PFUnA < 0.4 ng/L ND 30U 11Cl-PF3OUdS < 0.5 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 33.1 ng/L 35.49 93 50-200 Surrogate: 13C5-PFPeA-SURR 33.9 ng/L 35.49 96 50-200 Surrogate: 13C3-PFBS-SURR 31.2 ng/L 33.07 94 50-200 Surrogate: 13C2-4:2FTS-SURR 120 ng/L 133.4 90 50-200 Surrogate: 13C5-PFHxA-SURR 33.6 ng/L 35.49 95 50-200 Surrogate: 13C3-HFPOA-DA-SURR 34.6 ng/L 35.49 97 50-200 Surrogate: 13C4-PFHpA-SURR 33.6 ng/L 35.49 95 50-200 Surrogate: 13C3-PFHxS-SURR 31.8 ng/L 33.64 94 50-200 Surrogate: 13C2-6:2FTS-SURR 124 ng/L 134.8 92 50-200 Surrogate: 13C8-PFOA-SURR 34.2 ng/L 35.49 96 50-200 Surrogate: 13C9-PFNA-SURR 34.2 ng/L 35.49 96 50-200 Surrogate: 13C8-PFOS-SURR 32.3 ng/L 34.00 95 50-200 Surrogate: 13C2-8:2FTS-SURR 129 ng/L 136.3 94 50-200 Surrogate: 13C6-PFDA-SURR 29.9 ng/L 35.49 84 50-200 Surrogate: 13C7-PFUnA-SURR 29.8 ng/L 35.49 84 50-200 Surrogate: 13C2-PFDoA-SURR 33.1 ng/L 35.49 93 50-200 Matrix Spike (B537217-MS1)Sample: IF05675-01RE1 Prepared: 07/08/25 Analyzed: 07/11/25 PFBA 97 ng/L 83.33 ND 117 70-130 PFMPA 98 ng/L 83.33 ND 118 70-130 PFPeA 88 ng/L 83.33 ND 106 70-130 PFBS 85 ng/L 83.33 ND 102 70-130 PFMBA 80 ng/L 83.33 ND 96 70-130 PFEESA 84 ng/L 83.33 ND 101 70-130 NFDHA 87 ng/L 83.33 ND 105 70-130 HFPO-DA 85 ng/L 83.33 ND 102 70-130 PFHxS 85 ng/L 83.33 ND 103 70-130 4:2 FTS 101 ng/L 83.33 ND 121 70-130 PFHpA 88 ng/L 83.33 ND 105 70-130 PFHxA 89 ng/L 83.33 ND 106 70-130 www.pacelabs.comCustomer #: 72-106174 Page 6 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B537217-MS1)Sample: IF05675-01RE1 Prepared: 07/08/25 Analyzed: 07/11/25 ADONA 92 ng/L 83.33 ND 110 70-130 PFPeS 89 ng/L 83.33 ND 107 70-130 6:2 FTS 95 ng/L 83.33 ND 115 70-130 PFOA 87 ng/L 83.33 ND 104 70-130 PFHpS 77 ng/L 83.33 ND 92 70-130 PFOS 78 ng/L 83.33 ND 93 70-130 PFNA 87 ng/L 83.33 ND 104 70-130 9Cl-PF3ONS 79 ng/L 83.33 ND 95 70-130 8:2 FTS 102 ng/L 83.33 ND 122 70-130 PFDA 87 ng/L 83.33 ND 105 70-130 PFUnA 81 ng/L 83.33 ND 97 70-130 11Cl-PF3OUdS 83 ng/L 83.33 ND 99 70-130 PFDoA 84 ng/L 83.33 ND 101 70-130 Surrogate: 13C4-PFBA-SURR 37.6 ng/L 41.67 90 50-200 Surrogate: 13C5-PFPeA-SURR 38.2 ng/L 41.67 92 50-200 Surrogate: 13C3-PFBS-SURR 36.5 ng/L 38.83 94 50-200 Surrogate: 13C2-4:2FTS-SURR 150 ng/L 156.7 95 50-200 Surrogate: 13C5-PFHxA-SURR 38.7 ng/L 41.67 93 50-200 Surrogate: 13C3-HFPOA-DA-SURR 39.1 ng/L 41.67 94 50-200 Surrogate: 13C4-PFHpA-SURR 38.1 ng/L 41.67 91 50-200 Surrogate: 13C3-PFHxS-SURR 37.7 ng/L 39.50 95 50-200 Surrogate: 13C2-6:2FTS-SURR 149 ng/L 158.3 94 50-200 Surrogate: 13C8-PFOA-SURR 38.3 ng/L 41.67 92 50-200 Surrogate: 13C9-PFNA-SURR 39.4 ng/L 41.67 95 50-200 Surrogate: 13C8-PFOS-SURR 39.4 ng/L 39.92 99 50-200 Surrogate: 13C2-8:2FTS-SURR 158 ng/L 160.0 99 50-200 Surrogate: 13C6-PFDA-SURR 35.6 ng/L 41.67 86 50-200 Surrogate: 13C7-PFUnA-SURR 36.3 ng/L 41.67 87 50-200 Surrogate: 13C2-PFDoA-SURR 39.3 ng/L 41.67 94 50-200 www.pacelabs.comCustomer #: 72-106174 Page 7 of 12 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 8 of 12 Page 9 of 12 Page 10 of 12 Page 11 of 12 Page 12 of 12