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HomeMy WebLinkAboutDERR-2025-005537 WASATCH ENVIRONMENTAL, INC. ENVIRONMENTAL SCIENCE AND ENGINEERING 2410 WEST CALIFORNIA AVENUE SALT LAKE CITY, UTAH 84104 PHONE (801) 972-8400 e-mail: wei@wasatch-environmental.com www.wasatch-environmental.com SAMPLING AND ANALYSIS PLAN AIRPORT WEST VCP - PHASE I AREA SALT LAKE CITY, UTAH VOLUNTARY CLEANUP PROGRAM SITE #C092 Project No. 1660-005F Prepared for: Utah Department of Environmental Quality Division of Environmental Response and Remediation Voluntary Cleanup Program Mr. Bill Rees, Section Manager 195 North 1950 West Salt Lake City, Utah 84114 Prepared by: Wasatch Environmental, Inc. 2410 West California Ave. Salt Lake City, Utah 84104 July 28, 2025 Sampling and Analysis Plan Airport West VCP – Phase I Area Wasatch Environmental, Inc. Table of Contents Page i TABLE OF CONTENTS Section Page No. 1. INTRODUCTION .............................................................................................................................. 1 2. SITE DESCRIPTION ........................................................................................................................ 1 3. BACKGROUND ............................................................................................................................... 1 4. PROJECT OBJECTIVES ................................................................................................................. 2 5. SAMPLING ACTIVITIES .................................................................................................................. 2 6. SAMPLING METHODS.................................................................................................................... 2 7. ANALYTICAL METHODS ................................................................................................................ 3 8. QUALITY ASSURANCE AND QUALITY CONTROL ...................................................................... 3 9. REPORTING .................................................................................................................................... 4 10. HEALTH AND SAFETY ................................................................................................................... 4 FIGURES Figure 1 – Phase I Site Map Figure 2 – Typical Sample Location Map APPENDICES Appendix A – Standard Operating Procedures SOP 1 – Soil Sampling Procedure SOP 2 – Sample Documentation and Handling SOP 3 – Chain-of-Custody Documentation SOP 4 – Equipment and Materials Appendix B – Table 2 Analyte Lists and Soil Confirmation Screening Levels Appendix C – November 8, 2022, Project Design Contingency Plan, Airport West VCP Sampling and Analysis Plan Airport West VCP – Phase I Area Wasatch Environmental, Inc. Page 1 SAMPLING AND ANALYSIS PLAN AIRPORT WEST VCP – PHASE I AREA SALT LAKE CITY, UTAH VOLUNTARY CLEANUP PROGRAM SITE #C092 1. INTRODUCTION This Sampling and Analysis Plan (SAP) describes the methods and procedures for collecting, handling, and analyzing environmental confirmation soil samples from the Airport West - Phase I Area site (Phase I Area) for the initial phase of the North Temple Landfill (NTL) clean-up effort. All personnel involved with the collection and handling of samples shall be required to read this plan, and a copy of this plan will be available in the field during all sampling activities. This SAP is intended to be used in conjunction with the December 2022 Remedial Action Plan (RAP) and the July 31, 2022, Quality Assurance Project Plan (QAPP). If there are any discrepancies between the RAP or QAPP and this approved SAP, the means and methods of sample collection and sample analysis will follow this SAP. 2. SITE DESCRIPTION The Phase I Area is located between downtown Salt Lake City and the Great Salt Lake, along US Interstate 80 (I‐80) on the North Temple Frontage Road between approximately 6100 West and 7500 West, within the northwest portion of Salt Lake County, Utah (Figure 1). The Phase I Area is approximately 150-acres of the larger 770-acre NTL. The NTL is a closed municipal landfill that was operated by Salt Lake City Corporation from 1959 until 1979. The topography of the landfill is relatively flat, with mounding and depressions due to trenching cell construction and varying landfill practices during operation. 3. BACKGROUND As discussed above, the Phase I Area is approximately 150-acres of the 770-acre NTL which was operated as a trench landfill. The landfill operation began in the eastern portion of the landfill and moved west as the landfilling operation extended across the site. During the life of the landfill, the site received the majority of Salt Lake City’s municipal waste stream. This waste stream consisted primarily of household municipal waste, commercial waste and construction debris. In 2017, Utah’s School and Institutional Trust Land Administration (SITLA) obtained title from SLR to a 770-acre parcel that encompasses the footprint of the old landfill with the intent to redevelop the parcel under a brownfield development concept whereby the landfill would be remediated in a series of phases with waste being consolidated on-site to allow for future development. The remediation efforts would be undertaken in close coordination with Utah Department of Environmental Quality (UDEQ) Division of Environmental Response & Remediation (DERR) under the UDEQ Voluntary Cleanup Program (VCP). A Remedial Action Plan (RAP) was subsequently prepared and approved for the initial phase of the site remediation, the “Phase I Remedial Action Plan.” This SAP has been developed to further identify various means and methods set forth in the Phase I RAP necessary to effectuate the successful remediation of the Phase I area. The new property owner, Utah’s Inland Port Authority, by virtue of their entrance into the VCP as co - applicant with SITLA has adopted the Phase I RAP and this Sampling and Analysis Plan for the work effort for the property. Information regarding the project can be found on DERR’s website under the names Airport West and North Temple Landfill. Sampling and Analysis Plan Airport West VCP – Phase I Area Wasatch Environmental, Inc. Page 2 4. PROJECT OBJECTIVES To collect confirmation soil samples to confirm completion of the waste excavation efforts for each of the individual waste cells. Confirmation sample results will be compared against site-specific action/cleanup levels for the project specified in the RAP and QAPP. 5. SAMPLING ACTIVITIES The RAP and QAPP provide details regarding the objectives, methods, and sampling locations. Sampling activities are planned to meet the project objectives in the RAP and detailed in this SAP. This SAP sets forth the confirmation soil sampling protocol to be conducted in conjunction with Phase I remediation of this VCP Site. All sampling activities will be conducted in accordance with this SAP. Any deviations will be immediately communicated to both the applicant and VCP project manager and will be subject to their approvals. 6. SAMPLING METHODS The specific sampling methods and field procedures Wasatch anticipates utilizing are presented as standard operating procedures (SOPs) contained in Appendix A of this SAP. If sampling methods become beneficial or necessary that are not included in the SOPs, an SOP will be developed for such sampling methods. The new SOPs will be presented in the applicable work plan(s) and amended to the SAP. Confirmation soil samples will be collected from each waste cell at a frequency of one sample per every 300 linear feet of cell excavation. As depicted on Figure 2, for cells that run south to north, sampling will begin at 150 feet from the south wall of the cell. Samples will be collected at 150 feet, 450 feet, 750 feet, etc. For cells that run east to west, sampling intervals will be measured from the eastern wall. If the remainder of a cell (northern extent for cells extending south to north, and western extent for cells extending east to west) measures less than 300 feet, but more than 150 feet, an additional soil confirmation sample will be collected. The sample will be collected from within the remaining portion of the cell, approximately two feet from the northern or western wall of the excavation. For irregularly shaped waste cells such as Cell 199, the sampling intervals will be measured from south to north. Furthermore, given that the average width of the waste cells in the Phase I Area is 150 feet, the irregularly shaped cells will be divided into sections extending from the south wall of the excavation. The 150 foot wide sections will be measured from the east wall of the excavation (see Figure 2). In cells that extend less than 300 feet, at a minimum, one confirmation soil sample will be collected. The samples will be collected by the bucket of the track excavator from the native soil in the base of the cell. The sample location latitude and longitude will be recorded in field notes. Soil from the sample location will be collected with the track excavator bucket and which will be brought to the side of the excavation. The soil may not be dumped onto the ground prior to sampling. In accordance with SOP 1, samples will be collected by removing 4-ounce portions of soil from the bucket and in a manner to be representative of collecting the soil sample within 6 inches of the top of the native soil layer. Each of the 4-ounce samples will be placed into laboratory-supplied glass sample jars and identified by a unique sample ID (SOP 2). The sample ID will include the cell number, sampling interval, and sequential sample ID , and be identified as a soil confirmation sample (Cell Number – 300 foot interval [300, 600, 900] – 1). In irregularly shaped cells, sample IDs will be sequential and will be assigned from east to west (see Figure 2). A photograph of each sample with soil in the bucket will be taken. Samples will be logged in field notes and on the Chain-of-Custody documentation in the field in accordance with SOP 3. Sample jars will be immediately placed in a baggie and into an iced cooler. If constituents in a confirmation soil sample do not meet site-specific cleanup levels, additional soil removal and sampling may be necessary. If a subsequent confirmation soil sample at the over-excavated area at a sample location is necessary, the confirmation soil sample ID will be designated with an A (207-300- 1A). Sampling and Analysis Plan Airport West VCP – Phase I Area Wasatch Environmental, Inc. Page 3 For field screening purposes only, a portion of each soil sample will be placed into a plastic baggie and allowed to come to ambient temperature to facilitate volatilization. A Multi Gas Meter Photoionization Detector (PID) will then be used to measure volatile organic compounds (VOC), hydrogen sulfide (H2S), and lower explosive limit (LEL) concentrations in the soil sample. The readings for each sample will be recorded in field notes. Equipment and materials that may be used in execution of field activities are identified in SOP 4. 7. ANALYTICAL METHODS Target analytes and laboratory analytical methods are summarized in Table 1. Table 1 is consistent with Table 2 in Appendix A-29 of the approved RAP, which is presented in Appendix B of this SAP. Table 2 contains a full list of analytical methods, analytes, and soil confirmation screening levels. Laboratory turnaround times will be determined on a case by case basis. As the soil confirmation sampling continues over the course of the remediation this list of compounds may be reduced based on analytical trends, such as the lack of detections of a specific constituent. Prior to a reduction in compound analysis, approval by DERR will be obtained. Table 1 Summary of Laboratory Analytical Methods Target Analytes Environmental Media Laboratory Analytical Methods Volatile Organic Compounds Soil SW-846 Method 8260D (Full list plus total petroleum hydrocarbons as gasoline range organics and TPH fractionation) Semi-Volatile Organic Compounds Soil SW-846 Method 8270E (Full list including 1,4-dioxane) Polycyclic Aromatic Hydrocarbons Soil SW-846 Method 8270E Total Petroleum Hydrocarbons as Diesel-Range Organics (TPH-DRO) with Silica Gel Treatment (SGT) Soil SW-846 Method 8270E (TPH fractionation) Metals Soil SW-846 Method 6020B (As, Ba, Cd, Pb, Se, Ag) SW-846 Method 3060ª/7196ª (Cr VI) HG-S-7471B (Hg) Confirmation soil samples will be delivered under Chain-of-Custody protocol to Chemtech-Ford Laboratories (Chemtech) except for the samples collected for hexavalent chromium analysis which will be shipped overnight under Chain-of-Custody protocol to Pace Analytical (Pace). Chemtech and Pace are Utah-certified laboratories. 8. QUALITY ASSURANCE AND QUALITY CONTROL Quality assurance and quality control (QA/QC) procedures will be maintained throughout the duration of the project. QA/QC procedures are specified in detail in the QAPP. One field duplicate will be collected for every 10 confirmation soil samples and analyzed for the same parameters listed for other media samples. Duplicate samples will be collected by filling alternate sample containers. Field duplicate samples will receive an entirely separate sample identification number such as 207-300-2. A Level III data quality package will be indicated on the Chain-of-Custody documentation. The Chain-of- Sampling and Analysis Plan Airport West VCP – Phase I Area Wasatch Environmental, Inc. Page 4 Custody Record will be used to indicate what analyses are required. Laboratory prepared trip blanks will be included in the cooler with samples to be analyzed for VOCs and will be analyzed for VOCs using U.S. EPA Method SW-846 8260D. No field equipment will be used to collect soil samples; therefore, no field equipment blanks will be collected. Soil samples (including trip blanks) may be transferred to a sample refrigerator located in the field office. The sample refrigerator may not be used for anything other than storing samples. The refrigerator temperature will be set to 39o Fahrenheit (4o Celsius). Samples must always remain at a temperature of 4o C ± 2o. When samples (including the original trip blanks) are prepared for delivery to the laboratory, they will be placed into a clean iced cooler for transportation. If placed into the refrigerator, the sampler will relinquish the samples to the team member that will deliver the samples to the laboratory. This will be recorded on the Chain-of-Custody documentation in accordance with SOP 3. Agency split samples will be coordinated with the DERR representative. Agency Split samples will be incorporated into the SAP and arranged in advance with the DERR PM to schedule the selected sample locations for the split samples. 9. REPORTING Analytical testing data results will be compiled into a table and a sample location map will be prepared and provided to DERR as part of the regular project weekly reporting update. A summary of all confirmation sample results will be presented in a final confirmation soil sampling report once all confirmation samples have been collected, and data validation has been completed. 10. HEALTH AND SAFETY A site-specific health and safety plan (HASP) is presented in Appendix C (C-1) of the RAP. A copy of the HASP will be on-Site at all times during field activities. Daily health and safety tailgate meetings will be conducted each morning during field activities. The use or reuse of this information is restricted to the referenced document unless otherwise authorized. Wasatch Environmental Copyright 2006 AIRPORT WEST VCP - PHASE 1 C092 WEI 1660-005F Figure 1Phase I Site Map The use or reuse of this information is restricted to the referenced document unless otherwise authorized. Wasatch Environmental Copyright 2006 AIRPORT WEST VCP - PHASE 1 C092 WEI 1660-005F Figure 2Typical Sample Location MapSample Location 207-150-1 207-750-1 207-1050-1 220-150-1220-450-1 15 0 ’ 30 0 ' 30 0 ' 30 0 ' 207-450-1 150’300'300' 220-750-1 15 0 ’ 30 0 ' 30 0 ' 199-750-4 199-450-4 199-150-4 199-750-3 199-750-1 150’150’150’150’ 199-750-2 199-150-3 199-450-3 199-450-2 199-450-1 Appendix A Standard Operating Procedures Revision 1.0: 3/31/2017 SOP 1–SOIL SAMPLING PROCEDURES Soil samples will be collected with gloved hands into laboratory-supplied 4 ounce glass jars. The soil samples will be packed into the laboratory supplied jars in a manner as not to leave any headspace to reduce the potential for the loss of volatile organic compounds. Samples collected from the excavator bucket shall be taken in a manner to be representative of collecting the soil sample within 6 inches of the top of the native soil layer. The samples shall be collected from material that has not had contact with the bucket walls and in a manner to prevent inclusion of materials that may have fallen from above the desired sampling interval. Field measurements will be recorded on the Field Forms and will include the type of sampling, time, sample description, and volume and number of containers. All entries will be made in ink, and erasures will not be made. If an incorrect entry is made, the information will be crossed out with a single line. Whenever a sample is collected or a measurement made, a detailed description of the sample location shall be recorded. All equipment used to make measurements will be identified. The latitude and longitude of each sample location will be recorded. Samples will be packed, sealed, and transported in accordance with the Sample Documentation and Handling SOP. Revision 1.0: 3/31/2017 SOP 2 – SAMPLE DOCUMENTATION AND HANDLING Sample collection information will be entered into field notebooks. Prior to laboratory shipment, each sample will be logged on a Chain-of-Custody (COC) Form. The COC form will be placed in a cooler and will accompany the analytical samples during shipment or transport to the laboratory. Once sealed, sample bottles will be labeled and placed in an iced cooler. Coolers to be shipped via courier will be lined with a plastic bag and packed with packing material surrounding the bottles to prevent breakage during shipment. Additionally, the drain spout of the cooler will be taped shut. Ice will be sealed in plastic bags to prevent melted ice from soaking the packing material. A temperature blank may be included in each cooler. A COC form will be enclosed in sealed plastic bags and taped to the underside of the cooler lid. Coolers will be secured with strapping tape and custody seals. The custody seals will be affixed to each sample cooler (not each bottle). The coolers will be shipped or delivered to the appropriate laboratory, by the field technician or overnight courier, so they will arrive for analysis within 3 days of sample collection. Revision 1.0: 3/31/2017 SOP 3 – CHAIN-OF-CUSTODY DOCUMENTATION A required part of any sampling and analytical program is a system for sample control from collection to data reporting. This includes the ability to trace the possession and handling of samples from the time of collection through analysis and final deposition. This system also ensures against tampering or contamination of samples. The documentation of the sample's history is referred to as the chain of custody (COC). Initially after collection, a sample is considered to be under a person' s custody if it fits the following criteria: • In an individual’s possession • In view of the individual after that person has taken possession • Secured by the person so that no one can tamper with the sample The field technician will use COC forms that are equivalent to the U.S. EPA Office of Enforcement COC forms. The sequence for transferring samples from the possession of the sampler, as cited above, to the contract laboratory is as follows: When the sample containers are delivered from the laboratory, both the sender and receiver sign and date the COC form as well as specifying on the form what has changed hands. From that point on, every time the sample bottles change hands (whether empty or full) both parties sign and date the transfer. However, some sample containers are stored at Wasatch and no COC is required for the acquisition of the sample bottles. The following information is included on the COC: • Project number • Project name • Sample ID number (as noted in the field log book) secured by that person so no one can tamper with the sample • Signature of sampler • Date and time of collection (time logged in field log book) • Type and matrix of sample • Number of containers • Preservative • Requested analyses • QC Level • Reporting Limits (MDL) • Inclusive dates of possession • Signature of receiver In addition to the COC form, other components of the COC will include sample labels, custody seals (if shipping the samples to a laboratory), and field notebook, as summarized below: Sample Label. A sample label will be affixed to each sample bottle to provide information regarding the sample ID, sampler’s initials, preservative information, date, and time of sample collection. Custody Seals. Two custody seals will be affixed to each sample shipping container (not each bottle). These seals will show a sampler’s (or person in possession of the samples) name, and date sealed. The seals will be taped onto the sample shipping container or lid of the shipping container prior to sample shipment, and will be broken at the laboratory under COC procedures. Revision 1.0: 3/31/2017 SOP 4 – EQUIPMENT AND MATERIALS Equipment used in the execution of field activities will be inspected, maintained, and calibrated by Wasatch field personnel per manufacturer’s instructions. All field equipment will be inspected before and after each use. Equipment requiring calibration will be calibrated, according to the manufacturer’s instructions, before each use. Field equipment will be recalibrated as necessary if field readings appear to be abnormal. Equipment calibration will be documented in field notes or on an equipment calibration log. Any reusable field equipment that will come into contact with sampled environmental media will be decontaminated before each use. Equipment that repeatedly malfunctions or is significantly damaged will be removed from service, and a replacement provided, until it has been properly repaired. The following equipment may be used during investigation activities: •Multi Gas Meters – will be used to monitor oxygen, carbon monoxide, hydrogen sulfide, VOCs, and explosive gas levels in the atmosphere at the excavations and during soil sample collection. •Niton XL2 950 GOLDD Portable X-ray Fluorescence (XRF) - the XRF analyzer (or equivalent) will be used following the U.S. EPA Method 6200 (Field Portable X-ray Fluorescence Spectrometry for the Determination of Elemental Concentrations in Soil and Sediment) for in situ soil screening. The handheld meter will be used to directly measure the concentrations of the metals of concern in soil. •Personal Protective Equipment (PPE) – will be used in accordance with the site-specific health and safety plan (HASP). Field personnel will be equipped with protective clothing, gloves, hearing protection, eye protection, respiratory protection, safety glasses, safety-toed boots, and hard hats as dictated by site conditions and the HASP. At a minimum level D PPE will be used during all field activities. Appendix B Table 2 Analyte Lists and Soil Confirmation Screening Levels TABLE 2  SOIL CONFIRMATION  SCREENING LEVELS ‐ VOC PHASE 1 AREA AIRPORT WEST VCP JULY 2022 8/1/2022 1:40 PM Matrix TestCode Units Analyte CAS Action Level Acetone 67‐64‐1 1050000 Benzene 71‐43‐2 423 Bromobenzene 108‐86‐1 1780 Bromochloromethane 74‐97‐5 628 Bromodichloromethane 75‐27‐4 128 Bromoform 75‐25‐2 8570 Bromomethane 74‐83‐9 30.1 Butylbenzene, n‐104‐51‐8 58400 Butylbenzene, sec‐135‐98‐8 117000 Butylbenzene, tert‐98‐06‐6 117000 Carbon disulfide 75‐15‐0 3470 Carbon tetrachloride 56‐23‐5 287 Chlorobenzene 108‐90‐7 1330 Chloroethane 75‐00‐3 22700 Chloroform 67‐66‐3 138 Chloromethane 74‐87‐3 463 Chlorotoluene, o‐95‐49‐8 23400 Chlorotoluene, p‐106‐43‐4 23400 cis‐1,2‐Dichloroethene 156‐59‐2 2340 cis‐1,3‐Dichloropropene 10061‐01‐5 309 Cyclohexane 110‐82‐7 27400 Dibromo‐3‐chloropropane, 1,2‐96‐12‐8 6.43 Dibromobenzene, 1,4‐106‐37‐6 11700 Dibromochloromethane 124‐48‐1 3890 Dibromoethane, 1,2‐106‐93‐4 15.9 Dibromomethane (Methylene Bromide) 74‐95‐3 98.9 Dichloro‐2‐butene, trans‐1,4‐110‐57‐6 3.25 Dichlorobenzene, 1,2‐95‐50‐1 9330 Dichlorobenzene, 1,4‐106‐46‐7 1140 Dichlorodifluoromethane 75‐71‐8 368 Dichloroethane, 1,1‐75‐34‐3 1550 Dichloroethane. 1,2‐107‐06‐2 137 Dichloroethene, 1,1‐75‐35‐4 995 Dichloropropane, 1,2‐78‐87‐5 66.3 Dichloropropane, 1,3‐142‐28‐9 23400 Dichloropropene, 1,3‐542‐75‐6 309 Dioxane, 1,4‐123‐91‐1 2450 Ethylbenzene 100‐41‐4 2540 Hexanone, 2‐591‐78‐6 1340 Isopropylbenzene 98‐82‐8 9950 Methyl Acetate 79‐20‐9 1170000 Methyl Ethyl Ketone (2‐Butanone)78‐93‐3 193000 Methyl tert‐butyl ether 1634‐04‐4 20500 Methyl‐2‐pentanone, 4‐108‐10‐1 139000 Methylcyclohexane 108‐87‐2NE Methylene chloride 75‐09‐2 3160 Naphthalene 91‐20‐3 585 Propyl benzene 103‐65‐1 24300 Styrene 100‐42‐5 34800 Tetrachloroethane, 1,1,1,2‐630‐20‐6 875 Tetrachloroethane, 1,1,2,2‐79‐34‐5 267 Tetrachloroethene 127‐18‐4 389 Toluene 108‐88‐3 46800 trans‐1,2‐Dichloroethene 156‐60‐5 302 trans‐1,3‐Dichloropropene 10061‐02‐6 309 Trichloro‐1,2,2‐trifluoroethane, 1,1,2‐76‐13‐1 28100 Trichlorobenzene, 1,2,3‐87‐61‐6 934 Trichlorobenzene, 1,2,4‐120‐82‐1 256 Trichloroethane, 1,1,1‐71‐55‐6 35600 Trichloroethane, 1,1,2‐79‐00‐5 6.31 Trichloroethene 79‐01‐6 18.7 Trichlorofluoromethane 75‐69‐4 350000 Trimethylbenzene, 1,2,4‐95‐63‐6 1770 Trimethylbenzene, 1,3,5‐108‐67‐8 1510 Trimethylpentene, 2,4,4‐25167‐70‐8 11700 Vinyl chloride 75‐01‐4 168 Xylene, m‐108‐38‐3 2370 Xylene, p‐106‐42‐3 2420 Xylenes 1330‐20‐7 2490 So i l 82 6 0 D ‐S mg / k g ‐dr y 10‐4 screening levelsjul2022.xlsx Page 1 of 5 821AR00940 TABLE 2 SOIL CONFIRMATION  SCREENING LEVELS ‐ SVOC PHASE I AREA AIRPORT WEST VCP JULY 2022 8/1/2022 1:43 PM Matrix TestCode Units Analyte CAS Action Level Acetophenone 98‐86‐2 117000 Atrazine 1912‐24‐9 999 Biphenyl, 1,1´‐92‐52‐4 200 Bis(2‐chloroethoxy)methane 111‐91‐1 2460 Bis(2‐chloroethyl) ether 111‐44‐4 103 Bis(2‐ethylhexyl) phthalate 117‐81‐7 16400 Butyl benzyl phthalate 85‐68‐7 121000 Caprolactam 105‐60‐2 398000 Chloro‐3‐methylphenol, 4‐59‐50‐7 82100 Chloroaniline, 4‐106‐47‐8 410 Chloronaphthalene, 2‐91‐58‐7 60300 Chlorophenol, 2‐95‐57‐8 5840 Dibenzofuran 132‐64‐9 1170 Dichlorobenzidine, 3,3´‐91‐94‐1 511 Dichlorophenol, 2,4‐120‐83‐2 2460 Diethyl phthalate 84‐66‐2 657000 Dimethylphenol, 2,4‐105‐67‐9 16400 Di‐n‐butyl phthalate 84‐74‐2 82100 Dinitro‐2‐methylphenol, 4,6‐534‐52‐1 65.7 Dinitrophenol, 2,4‐51‐28‐5 1640 Dinitrotoluene, 2,4‐121‐14‐2 737 Dinitrotoluene, 2,6‐606‐20‐2 154 Di‐n‐octyl phthalate 117‐84‐0 8210 Hexachlorobenzene 118‐74‐1 11.7 Hexachlorobutadiene 87‐68‐3 526 Hexachlorocyclopentadiene 77‐47‐4 7.45 Hexachloroethane 67‐72‐1 460 Isophorone 78‐59‐1 164000 Methylphenol, 2‐95‐48‐7 41000 Methylphenol, 3&4‐(blank) 821 Nitroaniline, 2‐88‐74‐4 7990 Nitroaniline, 4‐100‐01‐6 3280 Nitrobenzene 98‐95‐3 1290 N‐Nitrosodi‐n‐propylamine 621‐64‐7 32.8 N‐Nitrosodiphenylamine 86‐30‐6 46900 Oxybis(1‐chloropropane), 2,2´‐108‐60‐1 46700 Pentachlorophenol 87‐86‐5 397 Phenol 108‐95‐2 246000 Tetrachlorobenzene, 1,2,4,5‐95‐94‐335 Tetrachlorophenol, 2,3,4,6‐58‐90‐2 24600 Trichlorophenol, 2,4,5‐95‐95‐4 82100 Trichlorophenol, 2,4,6‐88‐06‐2 821 So i l 82 7 0 E ‐S mg / k g ‐dr y 10‐4 screening levelsjul2022.xlsx 2 OF 5 821AR00460 TABLE 2 SOIL CONFIRMATION  SCREENING LEVELS ‐ RCRA METALS PHASE 1 AREA AIRPORT WEST VCP JULY 2022 8/1/2022 1:45 PM Matrix TestCode Units Analyte CAS Acton Level Arsenic 7440‐38‐2 300 Barium 7440‐39‐3 217000 Cadmium 7440‐43‐9 99.7 Lead 7439‐92‐1 800 Selenium 7782‐49‐2 5840 Silver 7440‐22‐4 5840 3060A/7196A Chrom VI 18540‐29‐9 633 HG‐S‐7471B Mercury 7439‐97‐6 45.6 60 2 0 B ‐S mg / k g ‐dr y 10‐4 screening levelsjul2022.xlsx 3 of 5 819AR00640 TABLE 2 SOIL CONFIRMATION  SCREENING LEVELS ‐ TPH/PAH PHASE I AREA AIRPORT WEST VCP JULY 2022 8/1/2022 1:47 PM Matrix Units Type TestCode Analyte CAS Action  Level Acenaphthene 83‐32‐9 45200 Anthracene 120‐12‐7 226000 Benz[a]anthracene 56‐55‐32060 Benzo(e)pyrene 192‐97‐273.4 Benzo(j)fluoranthene 205‐82‐3 176 Benzo[a]pyrene 50‐32‐8 211 Benzo[b]fluoranthene 205‐99‐22110 Benzo[k]fluoranthene 207‐08‐9 21110 Chloronaphthalene, Beta‐91‐58‐7 60300 Chrysene 218‐01‐9 211000 Dibenz[a,h]anthracene 53‐70‐3 211 Dibenzo(a,e)pyrene 192‐65‐417.6 Dimethylbenz(a)anthracene, 7,12‐57‐97‐60.844 Fluoranthene 206‐44‐0 30100 Fluorene 86‐73‐7 30100 Indeno[1,2,3‐cd]pyrene 193‐39‐52110 Methylnaphthalene, 1‐90‐12‐07270 Methylnaphthalene, 2‐91‐57‐63010 Naphthalene 91‐20‐3 585 Nitropyrene, 4‐57835‐92‐4 176 Pyrene 129‐00‐0 22600 Benzene 71‐43‐2 423 Ethylbenzene 100‐41‐42540 Methyl tert‐Butyl Ether (MTBE)1634‐04‐4 20500 Naphthalene 91‐20‐3 585 Toluene 108‐88‐3 46800 Xylenes, total 1330‐20‐72490 Total Petroleum Hydrocarbons (Aliphatic Low)2180 Total Petroleum Hydrocarbons (Aliphatic Medium)440 Total Petroleum Hydrocarbons (Aliphatic High)3500000 Total Petroleum Hydrocarbons (Aromatic High)30100 Total Petroleum Hydrocarbons (Aromatic Low)423 Total Petroleum Hydrocarbons (Aromatic Medium)561 8270 8260 8260 TPH Fractionation 8270 TPH Fractionation NA So i l mg / k g ‐dr y PAH TPH‐GRO TPH‐DRO 10‐4 screening levelsjul2022.xlsx 4 of 5 819AR00640