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HomeMy WebLinkAboutDDW-2025-005683June 02, 2025 Dear John Steffan: Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 5/21/25 2:00 pm and logged in under work order IE04496. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH02043RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IE04496-01 Name: Sampled: Received: 05/21/25 14:00 05/20/25 10:30 SS268-GROUP SOURCE SAMPLING STATION SS268 Reg ID:Drinking Water - Regular SampleMatrix:UTAH02043 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 1.0 ng/L EPA 533PFBA05/29/25 14:17 MAB3U2.011.0 < 0.4 ng/L EPA 533PFMPA05/29/25 14:17 MAB3U2.010.4 < 0.5 ng/L EPA 533PFPeA05/29/25 14:17 MAB3U2.010.5 < 0.5 ng/L EPA 533PFBS05/29/25 14:17 MAB3U2.010.5 < 0.4 ng/L EPA 533PFMBA05/29/25 14:17 MAB3U2.010.4 < 0.5 ng/L EPA 533PFEESA05/29/25 14:17 MAB3U2.010.5 < 0.4 ng/L EPA 533HFPO-DA 05/29/25 14:17 MAB3U2.010.4 < 0.5 ng/L EPA 533NFDHA05/29/25 14:17 MAB3U2.010.5 < 0.4 ng/L EPA 5334:2 FTS 05/29/25 14:17 MAB3U2.010.4 < 0.4 ng/L EPA 533PFHxS05/29/25 14:17 MAB3U2.010.4 < 0.6 ng/L EPA 533PFHpA05/29/25 14:17 MAB3U2.010.6 < 1.0 ng/L EPA 533PFHxA05/29/25 14:17 MAB3U2.011.0 < 0.5 ng/L EPA 533ADONA05/29/25 14:17 MAB3U2.010.5 < 0.6 ng/L EPA 533PFPeS05/29/25 14:17 MAB3U2.010.6 < 0.5 ng/L EPA 5336:2 FTS 05/29/25 14:17 MAB3U2.010.5 < 0.7 ng/L EPA 533PFOA05/29/25 14:17 MAB3U2.010.7 < 0.6 ng/L EPA 533PFHpS05/29/25 14:17 MAB3U2.010.6 < 0.5 ng/L EPA 533PFOS05/29/25 14:17 MAB3U2.010.5 < 0.5 ng/L EPA 533PFNA05/29/25 14:17 MAB3U2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 05/29/25 14:17 MAB3U2.010.7 < 0.5 ng/L EPA 5338:2 FTS 05/29/25 14:17 MAB3U2.010.5 < 0.5 ng/L EPA 533PFDA05/29/25 14:17 MAB3U2.010.5 < 0.5 ng/L EPA 533PFUnA05/29/25 14:17 MAB3U2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 05/29/25 14:17 MAB3U2.010.6 < 0.6 ng/L EPA 533PFDoA05/29/25 14:17 MAB3U2.010.6 Surrogate: 13C4-PFBA-SURR 92 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 95 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 95 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 96 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 94 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 92 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 96 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 91 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 91 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 87 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 89 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 91 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 96 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 82 %50-200 05/29/25 14:17 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 74 %50-200 05/29/25 14:17 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IE04496-01 Name: Sampled: Received: 05/21/25 14:00 05/20/25 10:30 SS268-GROUP SOURCE SAMPLING STATION SS268 Reg ID:Drinking Water - Regular SampleMatrix:UTAH02043 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 76 %50-200 05/29/25 14:17 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B533850 - EPA 533 - EPA 533 Blank (B533850-BLK1)Prepared: 05/28/25 Analyzed: 05/29/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 21.7 ng/L 40.00 54 50-200 Surrogate: 13C5-PFPeA-SURR 23.0 ng/L 40.00 58 50-200 Surrogate: 13C3-PFBS-SURR 33.9 ng/L 37.28 91 50-200 Surrogate: 13C2-4:2FTS-SURR 138 ng/L 150.4 92 50-200 Surrogate: 13C5-PFHxA-SURR 26.0 ng/L 40.00 65 50-200 Surrogate: 13C3-HFPOA-DA-SURR 22.9 ng/L 40.00 57 50-200 Surrogate: 13C4-PFHpA-SURR 28.7 ng/L 40.00 72 50-200 Surrogate: 13C3-PFHxS-SURR 34.3 ng/L 37.92 90 50-200 Surrogate: 13C2-6:2FTS-SURR 140 ng/L 152.0 92 50-200 Surrogate: 13C8-PFOA-SURR 28.2 ng/L 40.00 70 50-200 Surrogate: 13C9-PFNA-SURR 30.5 ng/L 40.00 76 50-200 Surrogate: 13C8-PFOS-SURR 35.3 ng/L 38.32 92 50-200 Surrogate: 13C2-8:2FTS-SURR 146 ng/L 153.6 95 50-200 Surrogate: 13C6-PFDA-SURR 28.0 ng/L 40.00 70 50-200 Surrogate: 13C7-PFUnA-SURR 26.7 ng/L 40.00 67 50-200 Surrogate: 13C2-PFDoA-SURR 29.6 ng/L 40.00 74 50-200 LCS (B533850-BS1)Prepared: 05/28/25 Analyzed: 05/29/25 PFBA 215 ng/L 200.0 107 70-130 PFMPA 213 ng/L 200.0 106 70-130 www.pacelabs.comCustomer #: 72-106174 Page 6 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B533850-BS1)Prepared: 05/28/25 Analyzed: 05/29/25 PFPeA 201 ng/L 200.0 100 70-130 PFBS 195 ng/L 200.0 97 70-130 PFMBA 179 ng/L 200.0 90 70-130 PFEESA 194 ng/L 200.0 97 70-130 HFPO-DA 184 ng/L 200.0 92 70-130 NFDHA 192 ng/L 200.0 96 70-130 PFHxS 196 ng/L 200.0 98 70-130 4:2 FTS 219 ng/L 200.0 109 70-130 PFHpA 191 ng/L 200.0 95 70-130 PFHxA 200 ng/L 200.0 100 70-130 ADONA 188 ng/L 200.0 94 70-130 PFPeS 210 ng/L 200.0 105 70-130 6:2 FTS 207 ng/L 200.0 103 70-130 PFOA 194 ng/L 200.0 97 70-130 PFHpS 192 ng/L 200.0 96 70-130 PFOS 179 ng/L 200.0 90 70-130 PFNA 190 ng/L 200.0 95 70-130 9Cl-PF3ONS 184 ng/L 200.0 92 70-130 8:2 FTS 218 ng/L 200.0 109 70-130 PFDA 185 ng/L 200.0 92 70-130 PFUnA 182 ng/L 200.0 91 70-130 11Cl-PF3OUdS 193 ng/L 200.0 97 70-130 PFDoA 185 ng/L 200.0 93 70-130 Surrogate: 13C4-PFBA-SURR 31.6 ng/L 40.00 79 50-200 Surrogate: 13C5-PFPeA-SURR 33.0 ng/L 40.00 82 50-200 Surrogate: 13C3-PFBS-SURR 36.6 ng/L 37.28 98 50-200 Surrogate: 13C2-4:2FTS-SURR 167 ng/L 150.4 111 50-200 Surrogate: 13C5-PFHxA-SURR 32.2 ng/L 40.00 80 50-200 Surrogate: 13C3-HFPOA-DA-SURR 30.5 ng/L 40.00 76 50-200 Surrogate: 13C4-PFHpA-SURR 32.2 ng/L 40.00 81 50-200 Surrogate: 13C3-PFHxS-SURR 36.8 ng/L 37.92 97 50-200 Surrogate: 13C2-6:2FTS-SURR 163 ng/L 152.0 107 50-200 Surrogate: 13C8-PFOA-SURR 30.6 ng/L 40.00 76 50-200 Surrogate: 13C9-PFNA-SURR 31.1 ng/L 40.00 78 50-200 Surrogate: 13C8-PFOS-SURR 36.8 ng/L 38.32 96 50-200 Surrogate: 13C2-8:2FTS-SURR 164 ng/L 153.6 107 50-200 Surrogate: 13C6-PFDA-SURR 29.8 ng/L 40.00 74 50-200 Surrogate: 13C7-PFUnA-SURR 27.6 ng/L 40.00 69 50-200 Surrogate: 13C2-PFDoA-SURR 28.4 ng/L 40.00 71 50-200 Duplicate (B533850-DUP1)Sample: IE04492-01 Prepared: 05/28/25 Analyzed: 05/29/25 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 7 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B533850-DUP1)Sample: IE04492-01 Prepared: 05/28/25 Analyzed: 05/29/25 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 1.0 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.6 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 36.2 ng/L 39.09 93 50-200 Surrogate: 13C5-PFPeA-SURR 36.8 ng/L 39.09 94 50-200 Surrogate: 13C3-PFBS-SURR 34.7 ng/L 36.43 95 50-200 Surrogate: 13C2-4:2FTS-SURR 143 ng/L 147.0 97 50-200 Surrogate: 13C5-PFHxA-SURR 37.2 ng/L 39.09 95 50-200 Surrogate: 13C3-HFPOA-DA-SURR 35.7 ng/L 39.09 91 50-200 Surrogate: 13C4-PFHpA-SURR 37.8 ng/L 39.09 97 50-200 Surrogate: 13C3-PFHxS-SURR 35.0 ng/L 37.06 94 50-200 Surrogate: 13C2-6:2FTS-SURR 143 ng/L 148.6 97 50-200 Surrogate: 13C8-PFOA-SURR 35.1 ng/L 39.09 90 50-200 Surrogate: 13C9-PFNA-SURR 35.8 ng/L 39.09 92 50-200 Surrogate: 13C8-PFOS-SURR 35.7 ng/L 37.45 95 50-200 Surrogate: 13C2-8:2FTS-SURR 149 ng/L 150.1 99 50-200 Surrogate: 13C6-PFDA-SURR 33.6 ng/L 39.09 86 50-200 Surrogate: 13C7-PFUnA-SURR 31.5 ng/L 39.09 81 50-200 Surrogate: 13C2-PFDoA-SURR 34.1 ng/L 39.09 87 50-200 Matrix Spike (B533850-MS1)Sample: IE04494-01 Prepared: 05/28/25 Analyzed: 05/29/25 PFBA 217 ng/L 185.3 2 116 70-130 PFMPA 315 ng/L 185.3 ND 170 70-130Q1 PFPeA 199 ng/L 185.3 2 106 70-130 PFBS 192 ng/L 185.3 2 103 70-130 PFMBA 177 ng/L 185.3 ND 96 70-130 PFEESA 189 ng/L 185.3 ND 102 70-130 NFDHA 190 ng/L 185.3 ND 103 70-130 HFPO-DA 179 ng/L 185.3 ND 96 70-130 PFHxS 199 ng/L 185.3 5 104 70-130 4:2 FTS 214 ng/L 185.3 ND 115 70-130 PFHpA 185 ng/L 185.3 0.9 99 70-130 PFHxA 196 ng/L 185.3 3 104 70-130 www.pacelabs.comCustomer #: 72-106174 Page 8 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B533850-MS1)Sample: IE04494-01 Prepared: 05/28/25 Analyzed: 05/29/25 ADONA 184 ng/L 185.3 ND 99 70-130 PFPeS 206 ng/L 185.3 ND 111 70-130 6:2 FTS 204 ng/L 185.3 ND 110 70-130 PFOA 191 ng/L 185.3 2 102 70-130 PFHpS 192 ng/L 185.3 ND 104 70-130 PFOS 180 ng/L 185.3 5 94 70-130 PFNA 185 ng/L 185.3 0.8 100 70-130 9Cl-PF3ONS 183 ng/L 185.3 ND 99 70-130 8:2 FTS 211 ng/L 185.3 ND 114 70-130 PFDA 180 ng/L 185.3 ND 97 70-130 PFUnA 173 ng/L 185.3 ND 93 70-130 11Cl-PF3OUdS 188 ng/L 185.3 ND 102 70-130 PFDoA 178 ng/L 185.3 ND 96 70-130 Surrogate: 13C4-PFBA-SURR 33.8 ng/L 37.06 91 50-200 Surrogate: 13C5-PFPeA-SURR 57.6 ng/L 37.06 155 50-200 Surrogate: 13C3-PFBS-SURR 34.5 ng/L 34.54 100 50-200 Surrogate: 13C2-4:2FTS-SURR 166 ng/L 139.4 119 50-200 Surrogate: 13C5-PFHxA-SURR 34.0 ng/L 37.06 92 50-200 Surrogate: 13C3-HFPOA-DA-SURR 33.1 ng/L 37.06 89 50-200 Surrogate: 13C4-PFHpA-SURR 33.8 ng/L 37.06 91 50-200 Surrogate: 13C3-PFHxS-SURR 34.4 ng/L 35.14 98 50-200 Surrogate: 13C2-6:2FTS-SURR 158 ng/L 140.8 112 50-200 Surrogate: 13C8-PFOA-SURR 30.0 ng/L 37.06 81 50-200 Surrogate: 13C9-PFNA-SURR 28.7 ng/L 37.06 78 50-200 Surrogate: 13C8-PFOS-SURR 33.7 ng/L 35.51 95 50-200 Surrogate: 13C2-8:2FTS-SURR 158 ng/L 142.3 111 50-200 Surrogate: 13C6-PFDA-SURR 23.9 ng/L 37.06 65 50-200 Surrogate: 13C7-PFUnA-SURR 20.0 ng/L 37.06 54 50-200 Surrogate: 13C2-PFDoA-SURR 21.6 ng/L 37.06 58 50-200 www.pacelabs.comCustomer #: 72-106174 Page 9 of 11 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers Q1 Matrix Spike failed % recovery acceptance limits. The associated blank spike recovery was acceptable. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 10 of 11 Page 11 of 11