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HomeMy WebLinkAboutDDW-2025-005070May 14, 2025 Dear John Steffan: Please find enclosed the analytical results for the 4 sample(s) the laboratory received on 5/9/25 10:00 am and logged in under work order IE01961. All testing is performed according to our current TNI accreditations unless otherwise noted . This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH18011RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IE01961-01 Name: Sampled: Received: 05/09/25 10:00 05/08/25 09:37 WS014-HERCULES TANK WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH18011 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA05/13/25 15:11 MAB3U1.910.9 < 0.4 ng/L EPA 533PFMPA05/13/25 15:11 MAB3U1.910.4 < 0.5 ng/L EPA 533PFPeA05/13/25 15:11 MAB3U1.910.5 < 0.5 ng/L EPA 533PFBS05/13/25 15:11 MAB3U1.910.5 < 0.4 ng/L EPA 533PFMBA05/13/25 15:11 MAB3U1.910.4 < 0.5 ng/L EPA 533PFEESA05/13/25 15:11 MAB3U1.910.5 < 0.3 ng/L EPA 533HFPO-DA 05/13/25 15:11 MAB3U1.910.3 < 0.4 ng/L EPA 533NFDHA05/13/25 15:11 MAB3U1.910.4 < 0.3 ng/L EPA 5334:2 FTS 05/13/25 15:11 MAB3U1.910.3 < 0.4 ng/L EPA 533PFHxS05/13/25 15:11 MAB3U1.910.4 < 0.5 ng/L EPA 533PFHpA05/13/25 15:11 MAB3U1.910.5 < 1.0 ng/L EPA 533PFHxA05/13/25 15:11 MAB3U1.911.0 < 0.5 ng/L EPA 533ADONA05/13/25 15:11 MAB3U1.910.5 < 0.5 ng/L EPA 533PFPeS05/13/25 15:11 MAB3U1.910.5 < 0.5 ng/L EPA 5336:2 FTS 05/13/25 15:11 MAB3U1.910.5 < 0.7 ng/L EPA 533PFOA05/13/25 15:11 MAB3U1.910.7 < 0.6 ng/L EPA 533PFHpS05/13/25 15:11 MAB3U1.910.6 < 0.5 ng/L EPA 533PFOS05/13/25 15:11 MAB3U1.910.5 < 0.5 ng/L EPA 533PFNA05/13/25 15:11 MAB3U1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 05/13/25 15:11 MAB3U1.910.6 < 0.5 ng/L EPA 5338:2 FTS 05/13/25 15:11 MAB3U1.910.5 < 0.4 ng/L EPA 533PFDA05/13/25 15:11 MAB3U1.910.4 < 0.4 ng/L EPA 533PFUnA05/13/25 15:11 MAB3U1.910.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 05/13/25 15:11 MAB3U1.910.5 < 0.5 ng/L EPA 533PFDoA05/13/25 15:11 MAB3U1.910.5 Surrogate: 13C4-PFBA-SURR 89 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 83 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 91 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 91 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 94 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 83 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 91 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 89 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 90 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 83 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 89 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 90 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 95 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 84 %50-200 05/13/25 15:11 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 82 %50-200 05/13/25 15:11 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IE01961-01 Name: Sampled: Received: 05/09/25 10:00 05/08/25 09:37 WS014-HERCULES TANK WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH18011 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 90 %50-200 05/13/25 15:11 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IE01961-03 Name: Sampled: Received: 05/09/25 10:00 05/08/25 09:23 TP018-D ZONE SOURCES BLEND Reg ID:Drinking Water - Regular SampleMatrix:UTAH18011 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA 1.5 ng/L EPA 533PFBA05/13/25 15:35 MAB3J2.011.0 < 0.4 ng/L EPA 533PFMPA05/13/25 15:35 MAB3U2.010.4 < 0.5 ng/L EPA 533PFPeA05/13/25 15:35 MAB3U2.010.5 < 0.5 ng/L EPA 533PFBS05/13/25 15:35 MAB3U2.010.5 < 0.4 ng/L EPA 533PFMBA05/13/25 15:35 MAB3U2.010.4 < 0.5 ng/L EPA 533PFEESA05/13/25 15:35 MAB3U2.010.5 < 0.4 ng/L EPA 533HFPO-DA 05/13/25 15:35 MAB3U2.010.4 < 0.5 ng/L EPA 533NFDHA05/13/25 15:35 MAB3U2.010.5 < 0.4 ng/L EPA 5334:2 FTS 05/13/25 15:35 MAB3U2.010.4 < 0.4 ng/L EPA 533PFHxS05/13/25 15:35 MAB3U2.010.4 < 0.6 ng/L EPA 533PFHpA05/13/25 15:35 MAB3U2.010.6 < 1.0 ng/L EPA 533PFHxA05/13/25 15:35 MAB3U2.011.0 < 0.5 ng/L EPA 533ADONA05/13/25 15:35 MAB3U2.010.5 < 0.6 ng/L EPA 533PFPeS05/13/25 15:35 MAB3U2.010.6 < 0.5 ng/L EPA 5336:2 FTS 05/13/25 15:35 MAB3U2.010.5 < 0.7 ng/L EPA 533PFOA05/13/25 15:35 MAB3U2.010.7 < 0.6 ng/L EPA 533PFHpS05/13/25 15:35 MAB3U2.010.6 < 0.5 ng/L EPA 533PFOS05/13/25 15:35 MAB3U2.010.5 < 0.5 ng/L EPA 533PFNA05/13/25 15:35 MAB3U2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 05/13/25 15:35 MAB3U2.010.7 < 0.5 ng/L EPA 5338:2 FTS 05/13/25 15:35 MAB3U2.010.5 < 0.5 ng/L EPA 533PFDA05/13/25 15:35 MAB3U2.010.5 < 0.5 ng/L EPA 533PFUnA05/13/25 15:35 MAB3U2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 05/13/25 15:35 MAB3U2.010.6 < 0.6 ng/L EPA 533PFDoA05/13/25 15:35 MAB3U2.010.6 Surrogate: 13C4-PFBA-SURR 92 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 133 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 95 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 99 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 94 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 83 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 94 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 97 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 99 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 89 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 87 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 93 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 103 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 71 %50-200 05/13/25 15:35 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 70 %50-200 05/13/25 15:35 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 6 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IE01961-03 Name: Sampled: Received: 05/09/25 10:00 05/08/25 09:23 TP018-D ZONE SOURCES BLEND Reg ID:Drinking Water - Regular SampleMatrix:UTAH18011 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 81 %50-200 05/13/25 15:35 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 7 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B532482 - EPA 533 - EPA 533 Blank (B532482-BLK1)Prepared: 05/12/25 Analyzed: 05/13/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 39.1 ng/L 40.00 98 50-200 Surrogate: 13C5-PFPeA-SURR 36.8 ng/L 40.00 92 50-200 Surrogate: 13C3-PFBS-SURR 37.8 ng/L 37.28 101 50-200 Surrogate: 13C2-4:2FTS-SURR 151 ng/L 150.4 101 50-200 Surrogate: 13C5-PFHxA-SURR 40.6 ng/L 40.00 101 50-200 Surrogate: 13C3-HFPOA-DA-SURR 35.3 ng/L 40.00 88 50-200 Surrogate: 13C4-PFHpA-SURR 40.2 ng/L 40.00 100 50-200 Surrogate: 13C3-PFHxS-SURR 37.6 ng/L 37.92 99 50-200 Surrogate: 13C2-6:2FTS-SURR 153 ng/L 152.0 100 50-200 Surrogate: 13C8-PFOA-SURR 38.1 ng/L 40.00 95 50-200 Surrogate: 13C9-PFNA-SURR 40.2 ng/L 40.00 100 50-200 Surrogate: 13C8-PFOS-SURR 38.2 ng/L 38.32 100 50-200 Surrogate: 13C2-8:2FTS-SURR 162 ng/L 153.6 105 50-200 Surrogate: 13C6-PFDA-SURR 37.9 ng/L 40.00 95 50-200 Surrogate: 13C7-PFUnA-SURR 36.9 ng/L 40.00 92 50-200 Surrogate: 13C2-PFDoA-SURR 39.2 ng/L 40.00 98 50-200 LCS (B532482-BS1)Prepared: 05/12/25 Analyzed: 05/13/25 PFBA 77 ng/L 80.00 96 70-130 PFMPA 90 ng/L 80.00 113 70-130 www.pacelabs.comCustomer #: 72-106174 Page 8 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B532482-BS1)Prepared: 05/12/25 Analyzed: 05/13/25 PFPeA 72 ng/L 80.00 89 70-130 PFBS 68 ng/L 80.00 84 70-130 PFMBA 66 ng/L 80.00 82 70-130 PFEESA 65 ng/L 80.00 82 70-130 HFPO-DA 65 ng/L 80.00 82 70-130 NFDHA 65 ng/L 80.00 81 70-130 PFHxS 69 ng/L 80.00 86 70-130 4:2 FTS 82 ng/L 80.00 103 70-130 PFHpA 67 ng/L 80.00 84 70-130 PFHxA 70 ng/L 80.00 87 70-130 ADONA 69 ng/L 80.00 86 70-130 PFPeS 72 ng/L 80.00 90 70-130 6:2 FTS 78 ng/L 80.00 98 70-130 PFOA 81 ng/L 80.00 102 70-130 PFHpS 71 ng/L 80.00 89 70-130 PFOS 64 ng/L 80.00 80 70-130 PFNA 76 ng/L 80.00 95 70-130 9Cl-PF3ONS 66 ng/L 80.00 82 70-130 8:2 FTS 84 ng/L 80.00 105 70-130 PFDA 67 ng/L 80.00 84 70-130 PFUnA 66 ng/L 80.00 82 70-130 11Cl-PF3OUdS 73 ng/L 80.00 91 70-130 PFDoA 64 ng/L 80.00 81 70-130 Surrogate: 13C4-PFBA-SURR 34.2 ng/L 40.00 86 50-200 Surrogate: 13C5-PFPeA-SURR 33.0 ng/L 40.00 83 50-200 Surrogate: 13C3-PFBS-SURR 36.2 ng/L 37.28 97 50-200 Surrogate: 13C2-4:2FTS-SURR 153 ng/L 150.4 102 50-200 Surrogate: 13C5-PFHxA-SURR 35.6 ng/L 40.00 89 50-200 Surrogate: 13C3-HFPOA-DA-SURR 31.8 ng/L 40.00 80 50-200 Surrogate: 13C4-PFHpA-SURR 35.2 ng/L 40.00 88 50-200 Surrogate: 13C3-PFHxS-SURR 37.1 ng/L 37.92 98 50-200 Surrogate: 13C2-6:2FTS-SURR 152 ng/L 152.0 100 50-200 Surrogate: 13C8-PFOA-SURR 33.7 ng/L 40.00 84 50-200 Surrogate: 13C9-PFNA-SURR 34.1 ng/L 40.00 85 50-200 Surrogate: 13C8-PFOS-SURR 36.6 ng/L 38.32 95 50-200 Surrogate: 13C2-8:2FTS-SURR 158 ng/L 153.6 103 50-200 Surrogate: 13C6-PFDA-SURR 28.2 ng/L 40.00 70 50-200 Surrogate: 13C7-PFUnA-SURR 25.2 ng/L 40.00 63 50-200 Surrogate: 13C2-PFDoA-SURR 29.9 ng/L 40.00 75 50-200 Duplicate (B532482-DUP1)Sample: IE01343-03 Prepared: 05/12/25 Analyzed: 05/13/25 PFBA 3 ng/L 3 0.4 30 PFMPA < 0.4 ng/L ND 30U PFPeA 0.5 ng/L ND 30J PFBS 1 ng/L 1 1 30J PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.3 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 9 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B532482-DUP1)Sample: IE01343-03 Prepared: 05/12/25 Analyzed: 05/13/25 NFDHA < 0.4 ng/L ND 30U PFHxS 0.6 ng/L 0.6 3 30J 4:2 FTS < 0.3 ng/L ND 30U PFHpA < 0.5 ng/L ND 30U PFHxA < 1.0 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.5 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA 2 ng/L 2 10 30J PFHpS < 0.6 ng/L ND 30U PFOS 2 ng/L 2 0.5 30J PFNA 0.5 ng/L 0.5 0.9 30J 9Cl-PF3ONS < 0.6 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.4 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.5 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 35.2 ng/L 37.84 93 50-200 Surrogate: 13C5-PFPeA-SURR 42.9 ng/L 37.84 113 50-200 Surrogate: 13C3-PFBS-SURR 33.9 ng/L 35.26 96 50-200 Surrogate: 13C2-4:2FTS-SURR 140 ng/L 142.3 98 50-200 Surrogate: 13C5-PFHxA-SURR 36.6 ng/L 37.84 97 50-200 Surrogate: 13C3-HFPOA-DA-SURR 31.8 ng/L 37.84 84 50-200 Surrogate: 13C4-PFHpA-SURR 35.3 ng/L 37.84 93 50-200 Surrogate: 13C3-PFHxS-SURR 34.2 ng/L 35.87 95 50-200 Surrogate: 13C2-6:2FTS-SURR 141 ng/L 143.8 98 50-200 Surrogate: 13C8-PFOA-SURR 33.2 ng/L 37.84 88 50-200 Surrogate: 13C9-PFNA-SURR 34.3 ng/L 37.84 91 50-200 Surrogate: 13C8-PFOS-SURR 33.9 ng/L 36.25 94 50-200 Surrogate: 13C2-8:2FTS-SURR 145 ng/L 145.3 100 50-200 Surrogate: 13C6-PFDA-SURR 29.4 ng/L 37.84 78 50-200 Surrogate: 13C7-PFUnA-SURR 25.6 ng/L 37.84 68 50-200 Surrogate: 13C2-PFDoA-SURR 28.4 ng/L 37.84 75 50-200 Matrix Spike (B532482-MS1)Sample: IE01343-06 Prepared: 05/12/25 Analyzed: 05/13/25 PFBA 70 ng/L 73.58 ND 95 70-130 PFMPA 83 ng/L 73.58 ND 113 70-130 PFPeA 65 ng/L 73.58 ND 88 70-130 PFBS 61 ng/L 73.58 ND 84 70-130 PFMBA 59 ng/L 73.58 ND 80 70-130 PFEESA 59 ng/L 73.58 ND 80 70-130 NFDHA 60 ng/L 73.58 ND 81 70-130 HFPO-DA 60 ng/L 73.58 ND 82 70-130 PFHxS 62 ng/L 73.58 ND 85 70-130 4:2 FTS 76 ng/L 73.58 ND 103 70-130 PFHpA 61 ng/L 73.58 ND 82 70-130 PFHxA 64 ng/L 73.58 ND 88 70-130 www.pacelabs.comCustomer #: 72-106174 Page 10 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B532482-MS1)Sample: IE01343-06 Prepared: 05/12/25 Analyzed: 05/13/25 ADONA 63 ng/L 73.58 ND 85 70-130 PFPeS 65 ng/L 73.58 ND 88 70-130 6:2 FTS 70 ng/L 73.58 ND 95 70-130 PFOA 75 ng/L 73.58 1 100 70-130 PFHpS 62 ng/L 73.58 ND 85 70-130 PFOS 57 ng/L 73.58 ND 77 70-130 PFNA 69 ng/L 73.58 ND 94 70-130 9Cl-PF3ONS 59 ng/L 73.58 ND 80 70-130 8:2 FTS 74 ng/L 73.58 ND 100 70-130 PFDA 60 ng/L 73.58 ND 81 70-130 PFUnA 59 ng/L 73.58 ND 80 70-130 11Cl-PF3OUdS 63 ng/L 73.58 ND 85 70-130 PFDoA 58 ng/L 73.58 ND 79 70-130 Surrogate: 13C4-PFBA-SURR 33.3 ng/L 36.79 90 50-200 Surrogate: 13C5-PFPeA-SURR 33.2 ng/L 36.79 90 50-200 Surrogate: 13C3-PFBS-SURR 32.5 ng/L 34.29 95 50-200 Surrogate: 13C2-4:2FTS-SURR 137 ng/L 138.3 99 50-200 Surrogate: 13C5-PFHxA-SURR 34.5 ng/L 36.79 94 50-200 Surrogate: 13C3-HFPOA-DA-SURR 30.3 ng/L 36.79 82 50-200 Surrogate: 13C4-PFHpA-SURR 33.7 ng/L 36.79 92 50-200 Surrogate: 13C3-PFHxS-SURR 33.0 ng/L 34.88 95 50-200 Surrogate: 13C2-6:2FTS-SURR 137 ng/L 139.8 98 50-200 Surrogate: 13C8-PFOA-SURR 31.4 ng/L 36.79 85 50-200 Surrogate: 13C9-PFNA-SURR 32.5 ng/L 36.79 88 50-200 Surrogate: 13C8-PFOS-SURR 32.6 ng/L 35.25 93 50-200 Surrogate: 13C2-8:2FTS-SURR 141 ng/L 141.3 100 50-200 Surrogate: 13C6-PFDA-SURR 31.1 ng/L 36.79 85 50-200 Surrogate: 13C7-PFUnA-SURR 30.2 ng/L 36.79 82 50-200 Surrogate: 13C2-PFDoA-SURR 32.0 ng/L 36.79 87 50-200 www.pacelabs.comCustomer #: 72-106174 Page 11 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 12 of 15 Page 13 of 15 Page 14 of 15 Page 15 of 15