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HomeMy WebLinkAboutDAQ-2025-0026221 DAQC-509-25 Site ID 16168 (B4) MEMORANDUM TO: STACK TEST FILE – CRUSOE ENERGY SYSTEMS INC. – Residue Booster Facility THROUGH: Rik Ombach, Minor Source Oil and Gas Section Manager FROM: Paul Bushman, Environmental Scientist DATE: May 23, 2025 SUBJECT: Sources: Six (6) Waukesha 9394 GSI generator engines; SN’s: 1656720, 1651133, 1651138, 1658743, 1658713, 1662642 Contact: Kaitlin Meszaros: 631-245-0308 Location: Approximately 6 miles northwest of Myton, Duchesne County, Utah Test Contractor: Great Plains Analytical Services, Inc. Permit/AO#: DAQE-AN161680001-23 dated November 7, 2023 Action Code: TR Subject: Review of stack test report dated May 14, 2025 On May 15, 2025, Utah Division of Air Quality (DAQ) received a test report for six (6) Waukesha 9394 GSI generator engines located at Crusoe Energy Systems, Inc. Residue Booster Facility, Duchesne County, Utah. Testing was performed April 21, 2025, through April 25, 2025, to demonstrate compliance with the emission limits found in condition II.B.2.a of Approval Order DAQE-AN161680001-23 and 40 CFR Part 60, Subpart JJJJ. The calculated test results are: Source Test Date Test Method Pollutant Tester Results DAQ Results Limits Waukesha 9394 GSI; Unit ID: 2026-06 SN: 1656720 April 21, 2025 ASTM D6348- 03 NOx 4.005 ppmvd@15%O2 0.070 g/hp-hr 4.006 ppmvd@15%O2 0.071 g/hp-hr 82 ppmvd@15%O2 0.15 g/hp-hr CO 20.270 ppmvd@15%O2 0.217 g/hp-hr 20.270 ppmvd@15%O2 0.218 g/hp-hr 270 ppmvd@15%O2 0.30 g/hp-hr VOC 0.387 ppmvd@15%O2 0.007 g/hp-hr 0.387 ppmvd@15%O2 0.007 g/hp-hr 60 ppmvd@15%O2 0.03 g/hp-hr Waukesha 9394 GSI; Unit ID: 1349 SN: 1651133 April 25, 2025 ASTM D6348- 03 NOx 2.594 ppmvd@15%O2 0.057 g/hp-hr 2.594 ppmvd@15%O2 0.058 g/hp-hr 82 ppmvd@15%O2 0.15 g/hp-hr CO 0.894 ppmvd@15%O2 0.012 g/hp-hr 0.894 ppmvd@15%O2 0.012 g/hp-hr 270 ppmvd@15%O2 0.30 g/hp-hr VOC 0.216 ppmvd@15%O2 0.005 g/hp-hr 0.216 ppmvd@15%O2 0.005 g/hp-hr 60 ppmvd@15%O2 0.03 g/hp-hr Waukesha 9394 GSI; Unit ID: 1350 SN: 1651138 April 21, 2025 ASTM D6348- 03 NOx 2.345 ppmvd@15%O2 0.048 g/hp-hr 2.346 ppmvd@15%O2 0.049 g/hp-hr 82 ppmvd@15%O2 0.15 g/hp-hr CO 12.626 ppmvd@15%O2 0.157 g/hp-hr 12.626 ppmvd@15%O2 0.159 g/hp-hr 270 ppmvd@15%O2 0.30 g/hp-hr VOC 0.487 ppmvd@15%O2 0.010 g/hp-hr 0.487 ppmvd@15%O2 0.010 g/hp-hr 60 ppmvd@15%O2 0.03 g/hp-hr 2 Source Test Date Test Method Pollutant Tester Results DAQ Results Limits Waukesha 9394 GSI; Unit ID: 1455 SN: 1658743 April 23, 2025 ASTM D6348- 03 NOx 2.387 ppmvd@15%O2 0.042 g/hp-hr 2.387 ppmvd@15%O2 0.044 g/hp-hr 82 ppmvd@15%O2 0.15 g/hp-hr CO 0.682 ppmvd@15%O2 0.007 g/hp-hr 0.682 ppmvd@15%O2 0.008 g/hp-hr 270 ppmvd@15%O2 0.30 g/hp-hr VOC 0.490 ppmvd@15%O2 0.008 g/hp-hr 0.490 ppmvd@15%O2 0.009 g/hp-hr 60 ppmvd@15%O2 0.03 g/hp-hr Waukesha 9394 GSI; Unit ID: 2026-05 SN: 1658713 April 24, 2025 ASTM D6348- 03 NOx 2.502 ppmvd@15%O2 0.035 g/hp-hr 2.502 ppmvd@15%O2 0.035 g/hp-hr 82 ppmvd@15%O2 0.15 g/hp-hr CO 1.508 ppmvd@15%O2 0.013 g/hp-hr 1.508 ppmvd@15%O2 0.013 g/hp-hr 270 ppmvd@15%O2 0.30 g/hp-hr VOC 0.262 ppmvd@15%O2 0.003 g/hp-hr 0.262 ppmvd@15%O2 0.004 g/hp-hr 60 ppmvd@15%O2 0.03 g/hp-hr Waukesha 9394 GSI; Unit ID: 2026-07 SN: 1662642 April 22, 2025 ASTM D6348- 03 NOx 3.034 ppmvd@15%O2 0.051 g/hp-hr 3.034 ppmvd@15%O2 0.053 g/hp-hr 82 ppmvd@15%O2 0.15 g/hp-hr CO 0.466 ppmvd@15%O2 0.005 g/hp-hr 0.466 ppmvd@15%O2 0.005 g/hp-hr 270 ppmvd@15%O2 0.30 g/hp-hr VOC 0.243 ppmvd@15%O2 0.004 g/hp-hr 0.243 ppmvd@15%O2 0.004 g/hp-hr 60 ppmvd@15%O2 0.03 g/hp-hr DEVIATIONS: None. CONCLUSION: The stack test report appears to be acceptable. RECOMMENDATION: The emissions from the six (6) Waukesha 9394 GSI generator engines should be considered to have been in compliance with the emission limits of DAQE-AN161680001-23 and 40 CFR Part 60, Subpart JJJJ during testing. ATTACHMENTS: DAQ stack test review excel spreadsheets, Crusoe Energy Systems Inc. stack test report. Emissions Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-06 SN:1656720 Test Date: 4/21/2025 Run #1 2 3 Average Start Time 13:39 14:47 15:55 Stop Time 14:39 15:47 16:55 Sample Duration (minutes)60 60 60 BHP Engine Load (hp) 1950 1975 1975 1967 DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.6481 0.6557 0.6557 0.6532 CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99 TS Stack Temperature (°F)837 841 840 840 Pbar Barometric Pressure (mbar)1010 1009 1008 1009 Pbar Barometric Pressure (" Hg)29.82 29.80 29.78 29.80 Ps Stack Pressure ('' H2O)0.42 0.43 0.43 0.43 O2%vd O2 (%vd)0.00 0.00 0.00 0.0 CO2%vd CO2 (%vd)12.4 12.4 12.5 12.4 N2%vd N2 (%vd)87.6 87.6 87.5 87.6 dry NOX (ppmvd)16.9 14.5 11.2 14.2 dry CO (ppmvd) 72.2 73.9 69.3 71.8 wet TVOC (ppmvw as C3H8)1.0 1.1 1.3 1.1 Run #1 2 3 Average Bws Measured Moisture Content (%/100)0.173 0.174 0.173 0.173 Bws Saturated Moisture Content (%/100)413.919 421.986 420.561 418.822 Bws Actual Moisture Content (%/100)0.173 0.174 0.173 0.173 MD Molecular Weight Dry (lb/lb-mole)29.98 29.99 29.99 29.99 MA Molecular Weight Wet (lb/lb-mole)27.91 27.91 27.92 27.91 VS Gas Velocity (ft/sec)68.4 69.38 69.4 69.1 FACFM Gas Flow (acfm)8959 9082 9080 9040 FDSCFM Gas Flow (dscfm)3007 3035 3036 3026 FWSCFM Gas Flow (wscfm)3638 3674 3674 3662 FKWSCFH Gas Flow (kwscfh)218 220 220 220 FKWSCFM Gas Flow (kwscfm)4 4 4 4 lb/hr Gas Flow (lb/hr) 15813 15969 15972 15918 Fo Fo (unitless)1.685 1.684 1.677 1.682 wet O2 (%vw)0.0 0.0 0.0 0.0 wet CO2 (%vw)10.3 10.3 10.3 10.3 wet NOX (ppmvw)13.942 11.993 9.261 11.732 15 NOX (ppmvd @ 15% O2)4.759 4.096 3.162 4.006 82.0 lb/hr NOX (lb/hr)0.363 0.315 0.243 0.307 g/bhp-hr NOX (g/bhp-hr)0.084 0.072 0.056 0.071 0.15 wet CO (ppmvw) 59.721 61.108 57.275 59.368 15 CO (ppmvd @ 15% O2)20.386 20.872 19.553 20.270 270.0 lb/hr CO (lb/hr) 0.946 0.978 0.916 0.947 g/bhp-hr CO (g/bhp-hr) 0.220 0.225 0.210 0.218 0.30 dry NMEOC (ppmvd as C3H8)1.163 1.322 1.627 1.371 15 NMEOC (ppmvd as C3H8 @ 15% O2)0.328 0.373 0.459 0.387 60 lb/hr NMEOC (lb/hr as C3H8)0.024 0.028 0.034 0.028 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.006 0.006 0.008 0.007 0.03 g/bhp-hr HC+NOX (g/bhp-hr)0.090 0.079 0.064 0.077 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-06 SN:1656720 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 Linearity Bias (Zero) 0.0 Linearity Bias (Span) 10.6 % 0.00 10.73 21.04 0.0 10.6 20.7 0.0 0.2 0.3 0.0 0.00% 0.19% 1.62% Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias 4 Difference 1 4 Response 1 2 Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value Page 2 of 5 Run 1 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-06 SN:1656720 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 0.0 10.3 0.0% 1.2% 0.0% 1.0% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Page 3 of 5 Run 2 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-06 SN:1656720 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 0.0 10.3 0.0% 1.2% 0.0% 1.0% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Page 4 of 5 Run 3 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-06 SN:1656720 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 0.0 10.3 0.0% 1.2% 0.0% 1.0% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Page 5 of 5 Emissions Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1349 SN:1651133 Test Date: 4/25/2025 Run #1 2 3 Average Start Time 7:12 8:22 9:29 Stop Time 8:12 9:22 10:29 Sample Duration (minutes)60 60 60 BHP Engine Load (hp) 2200 2225 2275 2233 DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.9381 0.9644 0.9798 0.9607 CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99 TS Stack Temperature (°F)891 894 892 893 Pbar Barometric Pressure (mbar)1014 1014 1013 1014 Pbar Barometric Pressure (" Hg)29.94 29.94 29.91 29.93 Ps Stack Pressure ('' H2O)0.88 0.93 0.96 0.92 O2%vd O2 (%vd)0.00 0.00 0.00 0.0 CO2%vd CO2 (%vd)12.5 12.5 12.4 12.5 N2%vd N2 (%vd)87.5 87.5 87.6 87.5 dry NOX (ppmvd)8.9 8.9 9.8 9.2 dry CO (ppmvd) 2.0 2.0 5.5 3.2 wet TVOC (ppmvw as C3H8)0.7 0.6 0.6 0.6 Run #1 2 3 Average Bws Measured Moisture Content (%/100)0.175 0.175 0.176 0.175 Bws Saturated Moisture Content (%/100)524.491 531.202 527.305 527.666 Bws Actual Moisture Content (%/100)0.175 0.175 0.176 0.175 MD Molecular Weight Dry (lb/lb-mole)30.00 30.00 29.99 30.00 MA Molecular Weight Wet (lb/lb-mole)27.90 27.91 27.88 27.90 VS Gas Velocity (ft/sec)100.9 103.79 105.5 103.4 FACFM Gas Flow (acfm)13203 13586 13806 13532 FDSCFM Gas Flow (dscfm)4265 4382 4448 4365 FWSCFM Gas Flow (wscfm)5174 5312 5401 5296 FKWSCFH Gas Flow (kwscfh)310 319 324 318 FKWSCFM Gas Flow (kwscfm)5 5 5 5 lb/hr Gas Flow (lb/hr) 22480 23088 23453 23007 Fo Fo (unitless)1.671 1.669 1.680 1.673 wet O2 (%vw)0.0 0.0 0.0 0.0 wet CO2 (%vw)10.3 10.3 10.3 10.3 wet NOX (ppmvw)7.305 7.383 8.048 7.579 15 NOX (ppmvd @ 15% O2)2.500 2.525 2.757 2.594 82.0 lb/hr NOX (lb/hr)0.270 0.281 0.311 0.287 g/bhp-hr NOX (g/bhp-hr)0.056 0.057 0.062 0.058 0.15 wet CO (ppmvw) 1.689 1.644 4.502 2.612 15 CO (ppmvd @ 15% O2)0.578 0.562 1.542 0.894 270.0 lb/hr CO (lb/hr) 0.038 0.038 0.106 0.061 g/bhp-hr CO (g/bhp-hr) 0.008 0.008 0.021 0.012 0.30 dry NMEOC (ppmvd as C3H8)0.829 0.743 0.720 0.764 15 NMEOC (ppmvd as C3H8 @ 15% O2)0.234 0.210 0.203 0.216 60 lb/hr NMEOC (lb/hr as C3H8)0.024 0.022 0.022 0.023 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.005 0.005 0.004 0.005 0.03 g/bhp-hr HC+NOX (g/bhp-hr)0.061 0.062 0.066 0.063 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1349 SN:1651133 Test Date: 4/25/2025 O2 21.0 10.73 0.0 10.6 Linearity Bias (Zero) 0.0 Linearity Bias (Span) 10.6 % 0.00 10.73 21.04 0.0 10.6 20.9 0.0 0.1 0.1 0.0 0.00% 0.05% 0.67% Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value 4 Difference 1 4 Response 1 2 Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias Page 2 of 5 Run 1 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1349 SN:1651133 Test Date: 4/25/2025 O2 21.0 10.73 0.0 10.6 0.0 10.6 0.0% 0.0% 0.0% 0.1% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Page 3 of 5 Run 2 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1349 SN:1651133 Test Date: 4/25/2025 O2 21.0 10.73 0.0 10.6 0.0 10.6 0.0% 0.0% 0.0% 0.1% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Page 4 of 5 Run 3 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1349 SN:1651133 Test Date: 4/25/2025 O2 21.0 10.73 0.0 10.6 0.0 10.6 0.0% 0.0% 0.0% 0.1% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Page 5 of 5 Emissions Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1350 SN:1651138 Test Date: 4/21/2025 Run #1 2 3 Average Start Time 7:43 8:51 10:00 Stop Time 8:43 9:51 11:00 Sample Duration (minutes)60 60 60 BHP Engine Load (hp) 2425 2425 2450 2433 DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.9539 0.9747 0.9747 0.9678 CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99 TS Stack Temperature (°F)903 905 906 905 Pbar Barometric Pressure (mbar)1014 1014 1012 1014 Pbar Barometric Pressure (" Hg)29.95 29.95 29.89 29.93 Ps Stack Pressure ('' H2O)0.91 0.95 0.95 0.94 O2%vd O2 (%vd)0.00 0.00 0.00 0.0 CO2%vd CO2 (%vd)12.5 12.6 12.6 12.6 N2%vd N2 (%vd)87.5 87.4 87.4 87.5 dry NOX (ppmvd)9.4 8.9 6.7 8.3 dry CO (ppmvd) 39.9 45.7 48.5 44.7 wet TVOC (ppmvw as C3H8)1.7 1.2 1.4 1.4 Run #1 2 3 Average Bws Measured Moisture Content (%/100)0.174 0.174 0.174 0.174 Bws Saturated Moisture Content (%/100)551.847 556.310 559.906 556.021 Bws Actual Moisture Content (%/100)0.174 0.174 0.174 0.174 MD Molecular Weight Dry (lb/lb-mole)30.00 30.01 30.01 30.01 MA Molecular Weight Wet (lb/lb-mole)27.91 27.92 27.92 27.92 VS Gas Velocity (ft/sec)103.0 105.28 105.4 104.6 FACFM Gas Flow (acfm)13481 13781 13800 13687 FDSCFM Gas Flow (dscfm)4323 4413 4407 4381 FWSCFM Gas Flow (wscfm)5238 5347 5340 5308 FKWSCFH Gas Flow (kwscfh)314 321 320 319 FKWSCFM Gas Flow (kwscfm)5 5 5 5 lb/hr Gas Flow (lb/hr) 22768 23250 23219 23079 Fo Fo (unitless)1.672 1.663 1.661 1.665 wet O2 (%vw)0.0 0.0 0.0 0.0 wet CO2 (%vw)10.3 10.4 10.4 10.4 wet NOX (ppmvw)7.782 7.309 5.493 6.861 15 NOX (ppmvd @ 15% O2)2.660 2.499 1.878 2.346 82.0 lb/hr NOX (lb/hr)0.292 0.280 0.210 0.260 g/bhp-hr NOX (g/bhp-hr)0.055 0.052 0.039 0.049 0.15 wet CO (ppmvw) 32.986 37.747 40.070 36.934 15 CO (ppmvd @ 15% O2)11.275 12.905 13.698 12.626 270.0 lb/hr CO (lb/hr) 0.753 0.879 0.932 0.855 g/bhp-hr CO (g/bhp-hr) 0.141 0.164 0.173 0.159 0.30 dry NMEOC (ppmvd as C3H8)2.046 1.452 1.672 1.724 15 NMEOC (ppmvd as C3H8 @ 15% O2)0.578 0.410 0.472 0.487 60 lb/hr NMEOC (lb/hr as C3H8)0.061 0.044 0.051 0.052 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.011 0.008 0.009 0.010 0.03 g/bhp-hr HC+NOX (g/bhp-hr)0.066 0.061 0.048 0.058 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1350 SN:1651138 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 Linearity Bias (Zero) 0.0 Linearity Bias (Span) 10.6 % 0.00 10.73 21.04 0.0 10.6 20.7 0.0 0.2 0.3 0.0 0.00% 0.19% 1.62% Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias 4 Difference 1 4 Response 1 2 Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value Page 2 of 5 Run 1 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1350 SN:1651138 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 0.0 10.4 0.0% 1.0% 0.0% 0.8% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Page 3 of 5 Run 2 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1350 SN:1651138 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 0.0 10.4 0.0% 1.0% 0.0% 0.8% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Page 4 of 5 Run 3 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1350 SN:1651138 Test Date: 4/21/2025 O2 21.0 10.73 0.0 10.5 0.0 10.4 0.0% 1.0% 0.0% 0.8% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Page 5 of 5 Emissions Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1455 SN:1658743 Test Date: 4/23/2025 Run #1 2 3 Average Start Time 7:27 8:35 9:44 Stop Time 8:27 9:35 10:44 Sample Duration (minutes)60 60 60 BHP Engine Load (hp) 2050 2075 2075 2067 DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.7071 0.7348 0.7416 0.7279 CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99 TS Stack Temperature (°F)881 904 906 897 Pbar Barometric Pressure (mbar)1011 1010 1009 1010 Pbar Barometric Pressure (" Hg)29.85 29.83 29.81 29.83 Ps Stack Pressure ('' H2O)0.50 0.54 0.55 0.53 O2%vd O2 (%vd)0.01 0.00 0.00 0.0 CO2%vd CO2 (%vd)12.5 12.6 12.6 12.6 N2%vd N2 (%vd)87.5 87.4 87.4 87.4 dry NOX (ppmvd)10.9 9.2 5.2 8.5 dry CO (ppmvd) 2.2 3.0 2.0 2.4 wet TVOC (ppmvw as C3H8)0.9 1.6 1.8 1.4 Run #1 2 3 Average Bws Measured Moisture Content (%/100)0.175 0.174 0.174 0.174 Bws Saturated Moisture Content (%/100)504.282 556.901 561.817 541.000 Bws Actual Moisture Content (%/100)0.175 0.174 0.174 0.174 MD Molecular Weight Dry (lb/lb-mole)30.00 30.01 30.01 30.01 MA Molecular Weight Wet (lb/lb-mole)27.91 27.93 27.93 27.92 VS Gas Velocity (ft/sec)75.9 79.54 80.4 78.6 FACFM Gas Flow (acfm)9934 10412 10518 10288 FDSCFM Gas Flow (dscfm)3222 3321 3349 3297 FWSCFM Gas Flow (wscfm)3906 4023 4055 3995 FKWSCFH Gas Flow (kwscfh)234 241 243 240 FKWSCFM Gas Flow (kwscfm)4 4 4 4 lb/hr Gas Flow (lb/hr) 16976 17493 17637 17369 Fo Fo (unitless)1.671 1.663 1.661 1.665 wet O2 (%vw)0.0 0.0 0.0 0.0 wet CO2 (%vw)10.3 10.4 10.4 10.4 wet NOX (ppmvw)9.016 7.630 4.297 6.981 15 NOX (ppmvd @ 15% O2)3.085 2.607 1.468 2.387 82.0 lb/hr NOX (lb/hr)0.252 0.220 0.125 0.199 g/bhp-hr NOX (g/bhp-hr)0.056 0.048 0.027 0.044 0.15 wet CO (ppmvw) 1.778 2.514 1.692 1.995 15 CO (ppmvd @ 15% O2)0.608 0.859 0.578 0.682 270.0 lb/hr CO (lb/hr) 0.030 0.044 0.030 0.035 g/bhp-hr CO (g/bhp-hr) 0.007 0.010 0.007 0.008 0.30 dry NMEOC (ppmvd as C3H8)1.130 1.948 2.131 1.736 15 NMEOC (ppmvd as C3H8 @ 15% O2)0.319 0.550 0.602 0.490 60 lb/hr NMEOC (lb/hr as C3H8)0.025 0.044 0.049 0.039 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.006 0.010 0.011 0.009 0.03 g/bhp-hr HC+NOX (g/bhp-hr)0.061 0.058 0.038 0.052 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1455 SN:1658743 Test Date: 4/23/2025 O2 21.0 10.73 0.0 10.6 Linearity Bias (Zero) 0.0 Linearity Bias (Span) 10.6 % 0.00 10.73 21.04 0.0 10.6 20.8 0.0 0.2 0.2 0.0 0.00% 0.05% 1.00% Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value 4 Difference 1 4 Response 1 2 Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias Page 2 of 5 Run 1 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1455 SN:1658743 Test Date: 4/23/2025 O2 21.0 10.73 0.0 10.6 0.0 10.5 0.0% 0.3% 0.0% 0.2% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Page 3 of 5 Run 2 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1455 SN:1658743 Test Date: 4/23/2025 O2 21.0 10.73 0.0 10.6 0.0 10.5 0.0% 0.3% 0.0% 0.2% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Page 4 of 5 Run 3 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 1455 SN:1658743 Test Date: 4/23/2025 O2 21.0 10.73 0.0 10.6 0.0 10.5 0.0% 0.3% 0.0% 0.2% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Page 5 of 5 Emissions Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-05 SN:1658713 Test Date: 4/24/2025 Run #1 2 3 Average Start Time 7:15 8:23 9:32 Stop Time 8:15 9:23 10:32 Sample Duration (minutes)60 60 60 BHP Engine Load (hp) 2075 2100 2125 2100 DS Stack Diameter (inches)18.0 18.0 18.0 18.0PAVG Average (Delta P)½ (" H2O)½0.6856 0.6782 0.7141 0.6926 CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99 TS Stack Temperature (°F)876 881 883 880 Pbar Barometric Pressure (mbar)1009 1011 1011 1010 Pbar Barometric Pressure (" Hg)29.81 29.85 29.84 29.83 Ps Stack Pressure ('' H2O)0.47 0.46 0.51 0.48 O2%vd O2 (%vd)0.01 0.00 0.00 0.0 CO2%vd CO2 (%vd)12.6 12.5 12.5 12.5 N2%vd N2 (%vd)87.4 87.5 87.5 87.5 dry NOX (ppmvd)8.8 8.0 9.8 8.9 dry CO (ppmvd) 3.9 6.5 5.6 5.3 wet TVOC (ppmvw as C3H8)0.7 0.9 0.7 0.8 Run #1 2 3 Average Bws Measured Moisture Content (%/100)0.175 0.175 0.175 0.175 Bws Saturated Moisture Content (%/100)494.071 504.332 508.848 502.417 Bws Actual Moisture Content (%/100)0.175 0.175 0.175 0.175 MD Molecular Weight Dry (lb/lb-mole)30.01 30.00 30.00 30.01 MA Molecular Weight Wet (lb/lb-mole)27.91 27.90 27.90 27.91 VS Gas Velocity (ft/sec)73.5 72.80 76.7 74.3 FACFM Gas Flow (acfm)7792 7719 8135 7882 FDSCFM Gas Flow (dscfm)2533 2501 2631 2555 FWSCFM Gas Flow (wscfm)3071 3035 3193 3100 FKWSCFH Gas Flow (kwscfh)184 182 192 186 FKWSCFM Gas Flow (kwscfm)3 3 3 3 lb/hr Gas Flow (lb/hr) 13348 13187 13873 13470 Fo Fo (unitless)1.665 1.668 1.669 1.667 wet O2 (%vw)0.0 0.0 0.0 0.0 wet CO2 (%vw)10.4 10.3 10.3 10.3 wet NOX (ppmvw)7.292 6.580 8.060 7.311 15 NOX (ppmvd @ 15% O2)2.496 2.252 2.759 2.502 82.0 lb/hr NOX (lb/hr)0.160 0.143 0.184 0.162 g/bhp-hr NOX (g/bhp-hr)0.035 0.031 0.039 0.035 0.15 wet CO (ppmvw) 3.258 5.367 4.591 4.405 15 CO (ppmvd @ 15% O2)1.115 1.837 1.572 1.508 270.0 lb/hr CO (lb/hr) 0.044 0.071 0.064 0.059 g/bhp-hr CO (g/bhp-hr) 0.010 0.015 0.014 0.013 0.30 dry NMEOC (ppmvd as C3H8)0.897 1.073 0.814 0.928 15 NMEOC (ppmvd as C3H8 @ 15% O2)0.253 0.303 0.230 0.262 60 lb/hr NMEOC (lb/hr as C3H8)0.016 0.018 0.015 0.016 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.003 0.004 0.003 0.004 0.03 g/bhp-hr HC+NOX (g/bhp-hr)0.038 0.035 0.042 0.039 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-05 SN:1658713 Test Date: 4/24/2025 O2 21.0 10.73 0.0 10.5 Linearity Bias (Zero) 0.0 Linearity Bias (Span) 10.5 % 0.00 10.73 21.04 0.0 10.5 20.8 0.0 0.2 0.2 0.0 0.00% 0.00% 1.14% Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value 4 Difference 1 4 Response 1 2 Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias Page 2 of 5 Run 1 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-05 SN:1658713 Test Date: 4/24/2025 O2 21.0 10.73 0.0 10.5 0.0 10.5 0.0% 0.2% 0.0% 0.2% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Page 3 of 5 Run 2 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-05 SN:1658713 Test Date: 4/24/2025 O2 21.0 10.73 0.0 10.5 0.0 10.5 0.0% 0.2% 0.0% 0.2% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Page 4 of 5 Run 3 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-05 SN:1658713 Test Date: 4/24/2025 O2 21.0 10.73 0.0 10.5 0.0 10.5 0.0% 0.2% 0.0% 0.2% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Page 5 of 5 Emissions Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-07 SN:1662642 Test Date: 4/22/2025 Run #1 2 3 Average Start Time 7:15 8:23 9:32 Stop Time 8:15 9:23 10:32 Sample Duration (minutes)60 60 60 BHP Engine Load (hp) 2325 2350 2300 2325 DS Stack Diameter (inches)21.0 21.0 21.0 21.0PAVG Average (Delta P)½ (" H2O)½0.6856 0.7141 0.7211 0.7069 CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99 TS Stack Temperature (°F)886 897 898 894 Pbar Barometric Pressure (mbar)1016 1015 1013 1014 Pbar Barometric Pressure (" Hg)29.99 29.96 29.92 29.96 Ps Stack Pressure ('' H2O)0.47 0.51 0.52 0.50 O2%vd O2 (%vd)0.00 0.00 0.00 0.0 CO2%vd CO2 (%vd)12.6 12.5 12.6 12.6 N2%vd N2 (%vd)87.4 87.5 87.4 87.5 dry NOX (ppmvd)10.6 11.3 10.3 10.7 dry CO (ppmvd) 0.9 1.9 2.2 1.7 wet TVOC (ppmvw as C3H8)0.7 0.8 0.7 0.7 Run #1 2 3 Average Bws Measured Moisture Content (%/100)0.174 0.174 0.174 0.174 Bws Saturated Moisture Content (%/100)512.981 538.231 541.227 530.813 Bws Actual Moisture Content (%/100)0.174 0.174 0.174 0.174 MD Molecular Weight Dry (lb/lb-mole)30.01 30.00 30.01 30.01 MA Molecular Weight Wet (lb/lb-mole)27.92 27.92 27.92 27.92 VS Gas Velocity (ft/sec)73.5 76.94 77.8 76.1 FACFM Gas Flow (acfm)10611 11104 11223 10979 FDSCFM Gas Flow (dscfm)3447 3575 3607 3543 FWSCFM Gas Flow (wscfm)4176 4331 4368 4292 FKWSCFH Gas Flow (kwscfh)251 260 262 258 FKWSCFM Gas Flow (kwscfm)4 4 4 4 lb/hr Gas Flow (lb/hr) 18159 18829 18996 18661 Fo Fo (unitless)1.664 1.668 1.664 1.665 wet O2 (%vw)0.0 0.0 0.0 0.0 wet CO2 (%vw)10.4 10.4 10.4 10.4 wet NOX (ppmvw)8.747 9.358 8.531 8.879 15 NOX (ppmvd @ 15% O2)2.989 3.198 2.915 3.034 82.0 lb/hr NOX (lb/hr)0.261 0.290 0.267 0.273 g/bhp-hr NOX (g/bhp-hr)0.051 0.056 0.053 0.053 0.15 wet CO (ppmvw) 0.751 1.536 1.807 1.365 15 CO (ppmvd @ 15% O2)0.257 0.525 0.617 0.466 270.0 lb/hr CO (lb/hr) 0.014 0.029 0.034 0.026 g/bhp-hr CO (g/bhp-hr) 0.003 0.006 0.007 0.005 0.30 dry NMEOC (ppmvd as C3H8)0.828 0.939 0.816 0.861 15 NMEOC (ppmvd as C3H8 @ 15% O2)0.234 0.265 0.230 0.243 60 lb/hr NMEOC (lb/hr as C3H8)0.020 0.023 0.020 0.021 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.004 0.004 0.004 0.004 0.03 g/bhp-hr HC+NOX (g/bhp-hr)0.055 0.060 0.057 0.057 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-07 SN:1662642 Test Date: 4/22/2025 O2 21.0 10.73 0.0 10.6 Linearity Bias (Zero) 0.0 Linearity Bias (Span) 10.6 % 0.00 10.73 21.04 0.0 10.6 20.8 0.0 0.1 0.3 0.0 0.00% 0.10% 1.38% Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value 4 Difference 1 4 Response 1 2 Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias Page 2 of 5 Run 1 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-07 SN:1662642 Test Date: 4/22/2025 O2 21.0 10.73 0.0 10.6 0.0 10.5 0.0% 0.8% 0.0% 0.7% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Page 3 of 5 Run 2 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-07 SN:1662642 Test Date: 4/22/2025 O2 21.0 10.73 0.0 10.6 0.0 10.5 0.0% 0.8% 0.0% 0.7% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Page 4 of 5 Run 3 Crusoe Energy Systems, Inc. Residue Booster Facility Duchesne County, Utah Waukesha 9394 GSI Unit 2026-07 SN:1662642 Test Date: 4/22/2025 O2 21.0 10.73 0.0 10.6 0.0 10.5 0.0% 0.8% 0.0% 0.7% Corrected O2 % 0.0 Run Length (Minutes) Uncorrected O2 % 60 0.0 Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Page 5 of 5 303 West 3rd Street ● Elk City, Oklahoma 73644 ● 580-225-0403 GAS Inc. www.gasinc.us May 14, 2025 Utah Department of Environmental Quality State Office Building – Air Quality Division 195 North 1950 West Salt Lake City, Utah 84114 RE: Crusoe Energy Systems, Inc. 40 CFR Part 60 Subpart JJJJ – Test Report SubmiWal To Whom It May Concern, Please find enclosed the performance tesYng reports for 40 CFR Subpart JJJJ on behalf of Crusoe Energy Systems, Inc. Please see below for the informaYon perYnent to the tesYng. Please see below for the informaYon perYnent to the enclosed reports. TesYng took place the week of April 21, 2025. Facility Unit # Serial # Loca1on Residue Booster Station 2026-06 1658720 Duchesne County, Utah Residue Booster Station 1350 1651138 Duchesne County, Utah Residue Booster Station 2026-07 1662642 Duchesne County, Utah Residue Booster Station 1455 1658743 Duchesne County, Utah Residue Booster Station 2026-05 1658713 Duchesne County, Utah Residue Booster Station 1349 1651133 Duchesne County, Utah For informaYon regarding the performance test, you can contact me by email at mholsapple@gasinc.us or by phone at 580-225-0403. For informaYon regarding engine or locaYon informaYon, please contact Kaitlin Meszaros by email at meszaros@pinyon-env.com or by phone at (631)-245-0308. Regards, Macie Holsapple Client Services Supervisor GAS Inc. Performance Test Report Test Type: Annual Test Date: 4/21/2025 Waukesha 9394 GSI Rich Burn (4 Cycle) 303 W. 3rd St Elk City , OK 73644(580) 225-0403 Test Started:Test Completed:01:39 PM 05:08 PM Source: Unit Number: 2026-06 Serial Number: 1656720 Engine Hours:12496 Permit #: #DAQE-AN161680001-23 Location: Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, Inc. Residue Booster Station 40 CFR Part 60 Subpart JJJJ CO NOx NMNEHC 71.802 14.189 1.370 2.000 0.300 1.000 0.150 0.700 0.030 0.217 0.070 0.007 Pass Pass Pass Pass Pass Pass Federal State Federal State Federal State Results ppmvd Results g/hp-hr Permit g/hp-hr PASS ALL Index Tables Figures Appendices Table 5.1 (Run Summaries)................................................................ Table 6.1 (Volumetric Flow Rate Data)............................................... Table 6.2 (Stack Gas Measurements)................................................. Table 8.1 (Oxygen Calibration)........................................................... Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... Annex Table 1.2.2 (Measurement System Capabilities)..................... Annex Table 1.3.1 (Test Specific Target Analytes)............................. Annex Table 4.1 (Measure System Capabilities)................................ Figure 6.1 (Location of Traverse Points per Method 1)....................... Annex Figure 1.4.1 (Sampling Train).................................................. Annex Figure 1.4.2 (Sampling Points)................................................. Annex Figure 1.4.3 (Sampling Port Locations).................................... Certified Calibration Bottle Certificates................................................ Tri Probe Certification via GD-031...................................................... GAS ALT 141_FTIR EPA.................................................................... Tester Qualifications (resume)............................................................ Raw Data............................................................................................ 27 Key Personnel.............................................................................1.0 3 Sampling System........................................................................2.0 3 Methods Used.............................................................................3.0 3 Test Summaries..........................................................................4.0 5 Run Summaries..........................................................................5.0 6 6 Volumetric Flow Rate Data.........................................................6.0 7 7 7 7 Calculations................................................................................7.0 8 9 12 12 13 15 13 14 14 20 25 28 29 Oxygen Calibration.....................................................................9 Engine Parameter Data Sheet....................................................10 QA/QC Results............................................................................11 Signature Page...........................................................................12.0 Appendices.................................................................................13.0 Bottle Certs.................................................................................2014.0 Tri Probe Certification via GD-031..............................................2515.0 GAS ALT 141_FTIR EPA............................................................16.0 Tester Qualifications (resume)....................................................2817.0 D6348 Annexes..........................................................................1211.0 18 19 26 8.0 9.0 10.0 Raw Data....................................................................................2918.0 1.0 Key Personnel GAS Crusoe Energy Systems, Inc. 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A EPA Method 2 & 2C EPA Method 3A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. ASTM D6348-03 Jason Woolley 3 Cooper Green GAS 4.0 Test Summary T e s t S u m m a r y Site Verification Photos GAS Unit 2026-06 with a serial number of 1656720 which is a Waukesha 9394 GSI engine located at Residue Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/21/2025 by Cooper Green with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 1967 BHP and 1200 RPM which is 78.67% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 2026-06 is authorized to operate under permit #DAQE-AN161680001-23. 4 4.0 Test Summary Engine/Compressor Specs Residue Booster StationLocation 2026-06Unit ID Make Waukesha Site Elevation ft.5460 Model 9394 GSI Atmospheric Pressure psi.12.04 Serial Number 1656720 Stack Diameter in.20 mfg. rated hp 2500 Yes 1200 Date of Manufacture Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1 Test Horsepower 1950 1975 1975 1967 1200 1200 1199 1200 Percent Load % Intake Manifold Pressure (hg) 78.00%79.00%79.00%78.67% 89.91 91.54 91.34 90.93 Intake Manifold Temperature (F)120.60 120.00 120.90 120.50 Ambient Conditions Ambient Temperature Dry (F)65.00 65.00 65.00 65.00 Exhaust Flow Data Q Stack (dscfh) Q Stack (dscm/hr) 180599.19 179783.27 179875.05 180085.83 5113.95 5090.85 5093.45 5099.42 Moisture Fraction Bws Fuel Consumption (Btu/h[-hr) 0.17 0.17 0.17 0.17 0 0 0 0 Fuel Flow (dscfh) Fuel (btu/scf)1020 1020 1020 1020 O2 F factor 8710.0 8710 8710 8710 Results Method 3A Corrected O2% Dry Moisture %17.30%17.35%17.31%17.32% T e s t S u m m a r y mfg. rated rpm Test RPM 0.00%0.00%0.00%0.00% Permitted Standards Results 5 Catalyst Run 1 Run 2 Run 3 3 Run Average Pass Permits 01:39 PM 02:47 PM 03:55 PM 4/21/2025 State NOx (mol wt) 46.01 0.962 1.093 1.345 1.133NMNEHC (ppmvw) 1.163 1.322 1.626 1.370NMNEHC (ppmvd) NMNEHC (mol wt) 44.10 328.192 373.146 458.984 386.774 FailNMNEHC (ppbvd) @15% O2 0.006 0.006 0.008 0.0070.700 0.030 PassNMNEHC (g/hp-hr) 0.328 0.373 0.459 0.387 FailNMNEHC (ppmvd) @15% O2 0.2080.222CO (g/hp-hr)0.220 0.2172.000 0.300 Pass CO (ppmvw)59.721 61.108 57.275 59.368 CO (ppmvd)72.211 73.935 69.262 71.802 CO (mol wt) 28.01 CO (ppmvd) @15% O2 20.385 20.872 19.552 20.270 Fail CO (ppbvd) @15% O2 20384.792 20871.597 19552.319 20269.569 Fail NOx (g/hp-hr)0.085 0.072 0.055 0.0701.000 0.150 Pass NOx (ppmvw)13.942 11.993 9.261 11.732 NOx (ppmvd)16.858 14.510 11.199 14.189 NOx (ppbvd) @15% O2 4758.875 4096.070 3161.512 4005.486 Fail NOx (ppmvd) @15% O2 4.759 4.096 3.162 4.005 Fail GAS GAS 5.0 Run Summaries Summary Source Run 1 R u n Table 5.1 Run Summaries S u m m a r i e s 6 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture % 59.72 0.40 13.36 0.58 13.94 0.00% 0.00% 0.00% 17.30% 12.92 0.52 0.00%17.25% 26.86 4.25 0.00%15.80% 13.80 0.64 0.00%17.34% 0.14 0.00 0.14 0.00%0.04% Avg. Wet NO Summary Source Run 2 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 0.29 0.14 0.00 0.14 0.00%0.04% 58.03 11.09 0.95 12.05 0.00%17.35% 109.56 25.19 1.63 26.82 0.00%15.90% 64.18 10.69 1.25 11.94 0.00%17.35% 0.53 0.18 0.00 0.18 0.00%0.04% Avg. Wet 61.11 10.89 1.10 11.99 1.09 0.00%17.35% NO2NO 0.68 0.91 24.20 1.28 0.78 Summary Source Run 3 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 53.32 7.98 0.27 8.26 0.00%17.30% 101.35 23.94 1.58 25.53 0.00%15.63% 61.23 10.12 0.15 10.27 0.00%17.32% 0.21 0.00 0.00 0.00 0.00%0.02% 0.53 0.18 0.00 0.18 0.78 0.00%0.04% Avg. Wet 57.27 9.05 0.21 9.26 1.34 0.00%17.31% NO2NO 0.72 1.39 24.17 1.30 NMNEHC 0.61 NO2 0.000.28 1.18 18.97 0.75 0.68 0.96 0.40 13.44 31.11 14.44 58.54 60.90 0.29 91.15 6.0 Volumetric Flow Rate Data Volumetric Flow Rate Data .99 Table 6.1. Data used for volumetric flow rate (Method 2) Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet Run 1 Average Pitot Tube Coefficient Cp(std)= H2O CO2 O2 CO Molecular Weight Stack Gas dry basis (Md) Molecular Weight Stack Gas wet basis (Ms) Stack Static Pressure (Pg) Stack Static Pressure (Pg) Atmospheric Pressure at Location (Pbar) Atmospheric Pressure at Location (Pbar) Absolute Stack Pressure (Ps) Stack Temperature Stack Temperature Stack Temperature Stack Gas Velocity Stack Flow Rate Q Stack Gas Wet Volmetric Flow Rate Stack Gas Dry Volumetric Flow Rate Sample after Back Purge: Within 5% of Last Δpstd reading: Stack Diameter (inches) Inches upstream from disturbance Inches downstream from disturbance scf/hr 0.38 Yes 20.00 18.00 16.00 scf/hr cfs ft/sec Deg R Deg F Deg C "Hg "Hg MBAR "Hg "H20 g/g mole g/g mole %d %d %d %17.30 29.98 0.42 Inches 3.34 10 16.66 Vo l u m e t r i c F l o w Ra tes Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 Figure 6.1 16 Traverse Points Were Used Emissions Sampling Points - 3 point long line sampling probe First Sampling Point Taken @ 16.7% of Stack Diameter Second Sampling Point Taken @ 50% of Stack Diameter Third Sampling Point Taken @ 83.3% of Stack Diameter 12.40 0.00 0.01 1009.82 0.03 29.83 29.86 837.25 1296.92 447.36 27.91 68.42 149.29 218368.14 180599.19 Run 2 17.35 29.99 0.43 12.41 0.00 0.01 1009.14 0.03 29.81 29.84 841.25 1300.92 449.58 27.91 69.67 149.27 217520.98 179783.27 Run 3 17.31 30.00 0.43 12.46 0.00 0.01 1008.47 0.03 29.79 29.82 840.38 1300.05 449.10 27.92 69.35 149.27 217521.49 179875.05 17.32 29.99 0.43 12.42 0.00 0.01 1009.14 0.03 29.81 29.84 839.63 1299.30 448.68 27.91 69.15 149.27 217803.54 180085.83 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets. * Cyclonic Flow Check (Pass/Fail): PASS Δpstd (in) H2O 0.36 Exhaust Temp F 837.00 Pitot Tube Sampling Points (Velocity) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Δpstd Average= Run 1 Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate 0.35 0.35 0.35 837.00 837.00 838.00 0.36 0.42 0.44 837.00 837.00 837.00 0.44 0.41 0.45 838.00 837.00 837.00 0.51 837.00 0.50 0.49 0.48 838.00 837.00 837.00 0.41 0.47 0.42 837.00 838.00 837.25 Δpstd = Velocity head measured by the standard pitot tube, (in.) H2O.Run 3 Δpstd (in) H2O 0.47 Exhaust Temp F 840.00 0.47 0.50 0.47 840.00 841.00 841.00 0.41 0.49 0.41 840.00 840.00 841.00 0.45 0.39 0.42 841.00 840.00 840.00 0.42 840.00 0.40 0.42 0.39 841.00 841.00 840.00 0.39 0.38 840.00 840.00 840.380.43 Run 2 Δpstd (in) H2O 0.38 Exhaust Temp F 841.00 0.35 0.41 0.40 841.00 841.00 842.00 0.41 0.37 0.41 842.00 841.00 841.00 0.46 0.48 0.46 841.00 842.00 841.00 0.40 841.00 0.46 0.55 0.41 841.00 842.00 841.00 0.56 0.43 841.00 841.00 0.43 841.25 Pass Strat Check 10.210Check 1 10.267Check 2 10.282Check 3 CO2Gas Used Pass/Fail 7 GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate *Note- Use of this method negates the need for any fuel related numbers for emissions calculations Nomenclature Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293°K (528 °R). Vs = Average stack gas velocity, m/sec (ft./sec). *(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1 Md = .44(12.396)+ .32(0)+ .28(87.597+.007) = 29.98 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO) 12.5 Molecular Weight of Stack Gas. Equation 2-6 Ms = 29.98(1 -.17296)+ 18.0(.17296) = 27.91 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws) 12.6 Average Stack Gas Velocity. Equation 2-7 Vs = 85.49*.99*√.42*√(1296.92/(29.86*27.91)) = 68.42 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms)) 12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8 Qsd = 3600(1-.17296)68.42*2.182((528*29.86)/ (1296.92*29.92)) = 180599.19 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd)) *Standard conversion from feet to meters Q = 180599.187/35.315 = 5113.951 DSCM/HRQ = Qsd/35.315 Emission Rates (Examples use CO Run 1) Nomenclature CO corrected @ 15% O2 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ER = Emission rate of (CO) in g/HP-hr. F(d )= Volumes of combustion components per unit of heat content, scm/J (scf/million Btu). Q = Stack gas volumetric flow rate, in standard cubic meters per hour, dry basis LB/HR.= Emission rate of (CO) in LB/HR. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) O2 = Concentration of oxygen on a dry basis, percent. ppm= Parts Per Million (CO) ppm@15% O2= PPM corrected to 15% O2 Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (DSCF/HR.). Run Time = Run Time in Minutes TPY= Tons per Year Mol wt.= Mol Weight of CO (28.01) Vs = Average stack gas velocity, m/sec (ft./sec). ppm @ 15% O2 = 72.211*(20.9-15)/(20.9-0%)) = 20.385 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2)) G/HP HR from 40 CFR Part 60 Subpart JJJJ (72.211*(1.164*10^-3)*5113.951*(Run Time/60))/1950 = .22 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR LB/HR from Grams LB/HR = .22*1/453.6*1950 = .948 LB/HRlb/hr = ER*1/453.6*BHP-HR TPY TPY = .948*4.38 = 4.152 TPYTPY = LB/HR. *4.38 Horsepower HP Provided On Site Wet to Dry PPM 72.21 = 59.721*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry 8 Cp(std) = Standard pitot tube coefficient; use 0.99 GAS 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span. 8.0 Oxygen Calibration 8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases. (1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration EPA Method 3A QA Worksheet (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Certified Gas Concentraion Low-Level (%) 0.00% Certified Gas Concentraion Mid-Level (%) Certified Gas Concentraion High-Level (%) (DIRECT) Analyzer Calibration Error (≤ 2%) Certified Concentration Value (%) Direct Calibration Response (%) Absolute Difference (%) Analyzer Calibration Error (%)Analyzer Direct Calibration Response Certified bottle value % 0.00% 0.00% 0.00% Zero Gas % Mid-Level Gas % High-Level Gas % Bias Pre Initial Value Bias Post Inital Values System Calibrations Response Pre (%) 0.00% System Bias (% of Span) Pre System Calibration Response Post (%) System Bias (% of Span) Post Drift (% of Span) 0.00%0.00%0.00%0.00% (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Avg. Gas Concentration (Run 1) Avg. Gas Concentration (Run 2) Avg. Gas Concentration (Run 3) Effluent Gas (Cgas) Run 1 Effluent Gas (Cgas) Run 2 Effluent Gas (Cgas) Run 3 Linearity Check 0.00%0.00%0.00% Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Upscale Gas Analyzer Calibration Response (%) Zero Gas Upscale Gas EPA Method 3A QA Worksheet Zero Gas Mid-Level Gas High-Level Gas 100% Nitrogen O2 QA/QC Zero Gas %0.00% Mid-Level Gas % High-Level Gas % System Calibration Response Pre (%) System Calibration Response Post (%) Zero Gas % Upscale Cal Zero Gas % Upscale Cal Upscale Used Upscale Used 10.56% 20.70% 10.52% 10.31% 10.73% 10.73% 10.31%10.52% 10.56% 20.70% 10.73% 21.04% 10.73% 21.04% 10.73%21.04% 0.00% 10.73% 21.04% 0.17% 0.34% 0.79% 1.63% 10.73% Span Zero Offset 0.00% 21.04 0.00% 10.56%0.20%1.19%0.01% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 9 GAS 990.0 988.0 988.0 1020.0 1022.0 1020.7 4.4 4.4 4.4 9.0 Engine Parameter Data Sheet Company Site Elevation (ft) Facility Unit ID Date Make Crusoe Energy Systems, Inc. Residue Booster Station 4/21/2025 5460 2026-06 Waukesha Model Serial Number 9394 GSI 1656720 Technician Cooper Green Run Start Times 01:39 PM 02:47 PM 03:55 PM 05:08 PM Run 1 Run 2 Run 3 Completed Engine Parameter Data Run 1 Engine Speed (RPM)1200.0 1200.0 1199.0 1199.7 Engine Hours 12493 12494 12495 12496 Intake Manifold Pressure (psi)56.2 57.0 56.9 56.7 Intake Manifold Temp °F 120.6 120.0 120.9 120.5 Engine Load (BHP)1950.0 1975.0 1975.0 1966.7 Ambient Temp °F 65.0 65.0 65.0 65.0 Humidity %14.0 14.0 14.0 14.0 Dew Point °F 14.0 15.0 15.0 14.7 Waukesha Yes 2 2 2 2# of Catalyst Installed Catalyst (Yes or No) AFR Setting (Target Left Bank) AFR Setting (Target Right Bank) AFR Manufacturer/Type Waukesha Waukesha Waukesha 10 Run 3 AverageRun 2 Discharge Pressure (psi) Suction Pressure (psi) 986.0 1020.0 4.4Catalyst Pressure Drop H2O Catalyst Outlet Temp °F Catalyst Inlet Temp °F GAS 10.0 QA/QC Results Average:Carbon monoxide CO Gas, Inc. 0.06 R e s u l t s Average:Nitrogen monoxide NO 0.21 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.20 Average:VOC 0.08 Average:Oxygen 0.00 Pre-test Baseline Results Time: Q A / Q C Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.60 Tolerance 2.00% Difference between measured and expected 1.40% CTS Direct to Analyzer Time: Average:Carbon monoxide CO 0.49 Average:Nitrogen monoxide NO 0.19 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.19 Average:VOC 0.71 Average:Oxygen 0.00 Pre-test System Zero Time: Mechanical Response Time 45 seconds Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.40 Tolerance 5.00% Difference between measured and expected 1.60% Pre-test System CTS & Mechanical Response Time 55 secondsEquilibration Response Time Value:Spike Reported 251.83 Value:Spike Expected 253.10 System (Equilibration) Response Time Target (Spike) 45 secondsSystem Zero Response Time 61 secondsSystem Response Time System (Zero) Response Time 11 11.0 D6348 Annexes 1-8 D6348 Annexes 1. Test Plan Requirements Annex 1.2 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration NO2 Ethylene SF6 O2 (%) CC524639 12/30/2027 103.00 10.73% CC252676 10/17/2032 100.00 CC433538 8/5/2032 21.04% Cylinder # SG9132842BAL Expiration: 8-20-2032 Propane CO NO SF6 Bottle Value 253.10 497.30 252.90 9.95 Analyzer System Response 251.83 488.59 247.39 9.74 Percent Difference 0.50%1.75%2.18%2.14% Annex Table 1.2.2 Measurement System Capabilities SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.604 4.930 Spike Direct Propane 252.583 Mechanical Response Time SF6 9.798 CO 492.402 NO 249.887 Ethylene 98.403 36 seconds Analyzer Response Propane 251.825 SF6 9.741 CO 488.590 NO 247.390 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 251.416 CO 483.431 NO 246.272 55 seconds 40 seconds 7.04% 8.85% 8.71% 97.27% 99.20% 98.67% 9.721 12 GAS Annex 1.3 Compounds Infrared Analysis Region (cm-1) Expected Concentration Range Measurement System Achievable Minimum Detectable Concentrations Required Measurement System Accuracy and Precision for Test Application CO 2000-2200 0-1200 ppm NO 1875-2138 NO2 2700-2950 VOC 2600-3200 910-1150 2550-2950 CH2O 2550-2850 Interfering Compounds * CO is analyzed in a separate analysis region than CO2 and H2O CO2 Water Vapor 926-1150 3200-3401 Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives 0.16267 ppm 4 ppm 0-1000 ppm 0.4007 ppm 2 ppm 0-100 ppm 0.4899 ppm 2 ppm 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC 0-100 ppm 0.7878 ppm 1 ppm 0-10% 0-22% 0% 0.20% n/a n/a * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. Annex 1.4 Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 13 GAS Sampling Point Locations in Inches 16.7%3.340 50%10.000 83.3%16.660 Figure Annex 1.4.3 Sample Port Location Figure Annex 1.4.2 Sampling Points Interior Stack Diameter (inches): Inches Upstream: Inches Downstream: 20 18 16 14 Stack Gas Dry Volumetric Flow Rate (scf/hr): 180085.83 H2O%d @ Sampling Point:17.32 CO2%d @ Sampling Point:12.42 Pressure @ Sampling Point (Pg "H2O):0.43 Temperature @ Sampling Point (Deg F):839.63 GAS D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1) Target Analyte Results (ppm) CO 0.1627 NO 0.4007 NO2 0.4899 Ethylene 0.3782 Propane 0.4351 Hexane 0.2233 Acetaldehyde 0.8152 Formaldehyde 0.7878 D6348 Annex 3. FTIR Reference Spectra Calibration Transfer Standard Expected Measured Path Length Validated Ethylene 100 98.6 4.93 Passed D6348 Annex 4. Required Pre-Test Procedures Annex Table 1.2.2 Measurement System Capabilities 15 SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.604 4.930 Spike Direct Propane 252.583 Mechanical Response Time SF6 9.798 CO 492.402 NO 249.887 Ethylene 98.403 36 seconds Analyzer Response Propane 251.825 SF6 9.741 CO 488.590 NO 247.390 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 251.416 CO 483.431 NO 246.272 55 seconds 40 seconds 7.04% 8.85% 8.71% 97.27% 99.20% 98.67% 9.721 GAS D6348 Annex 5. Analyte Spiking Technique Propane Spike Direct SF6 CO NO 253.100 9.954 497.300 252.900 252.583 9.798 492.402 249.887 0.20% 1.57% 0.98% 1.19% +/- 2% +/- 2% +/- 2% +/- 2% Pass Pass Pass Pass Parameter Gas Concentration Measured % Difference Specification Validated 0.054 0.000 Spike Average 17.381 0.690 Dilution Factor 7.042% Expected 17.869 % Recovery 97.270% Specification 70-130% <10% Spike Run 1 via the System Source Output Propane SF6 D6348 Annex 6. Determination of System Performance Parameters Noise Equivalent Absorbance (NEA) RMS High RMS Mid RMS Low Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%) 0.000 Spike Average 0.867 Dilution Factor 8.849% Expected % Recovery Specification 70-130% <10% Spike Run 2 via the System Source Output Propane SF6 0.000 Spike Average 0.853 Dilution Factor 8.706% Expected % Recovery Specification 70-130% <10% Spike Run 3 via the System Source Output Propane SF6 0.070 21.816 22.109 98.670% 0.000091 0.000174 0.000368 0.009 22.228 22.407 99.200% Line Position Difference:Resolution Difference to Reference0.00%Pass Pass3.49% 16 GAS Resolution The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. Detector Linerarity The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. D6348 Annex 7. Preparation of Analytical Quantification Algorithm The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 Regression Slope:-4.61332418 Pass Line Position Difference:Resolution Difference to Reference 3.49% D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures CTS Bottle Concentration: CTS Sample Concentration Average: Difference between measured and expected: Tolerance: 100.00 98.58 1.44% 5.00% POST CTS System Check: Run 1 Points 1 & 2 on CO/NO/Propane Run 2 Points 1 & 2 on CO/NO/Propane Run 3 Points 1 & 2 on CO/NO/Propane Run Data Validation - Automated vs Manual Reading Validated Comments All within 20% All within 20% All within 20% Passed Passed Passed Demonstrates no interferences observed. Demonstrates no interferences observed. Demonstrates no interferences observed. 17 GAS 12.0 Signature Page Job/File Name: We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Crusoe Energy Systems, Inc.; Residue Booster Station; 2026-06; JJJJ 18 Company: Print Name: Signature: Title: Phone Number: Date: Company:G.A.S. Inc.Date: Print Name: Title: 4/21/2025 Emissions Specialist Company:G.A.S. Inc.Date: Print Name: Title: Signature: Phone Number: Travis Hartley Director of Stack Testing 580-225-0403 4/21/2025 Cooper Green GAS Appendices GAS GAS Spike (5 Gas) GAS 9% O2/NO2 GAS Ethylene Only GAS BIP GAS 21% O2 Tri Probe Certification ” ‡ ƒ – Ž ƒ ‹ • • • ƒ Ž › – ‹ … ƒ Ž ‡ ” ˜ ‹ … ‡ • ͵Ͳ͵͵”†–Ž‹–›ǡǡ͹͵͸ͶͶ ȋͷͺͲȌʹʹͷǦͲͶͲ͵ ƒšǣȋͷͺͲȌʹʹͷǦʹ͸ͳʹ &(57,),&$7(2)$1$/<6,6 *UDGHRI3URGXFW&(57,),('67$1'$5'352%( 3DUW1XPEHU65HIHUHQFH 1XPEHU  /DERUDWRU\*$6,1&6WDFN'LDPHWHU $QDO\VLV'DWH7DUJHW)ORZ 5DWH /PLQ /271XPEHU 61 $ $6 1XPEHURI 3RLQWV  3URGXFWSHUIRUPDQFHYHULILHGE\GLUHFWFRPSDULVRQWRFDOLEUDWLRQVWDQGDUGVWUDFHDEOHWR1,67  7KHSUREHOLVWHGRQWKLVIRUPPHHWVWKHPXOWLSRLQWWUDYHUVHUHTXLUHPHQWRI(3$0HWKRGH VHFWLRQDVVKRZQLQWKHDFFRPSDQ\LQJGDWD0HWKRGHVHFWLRQVWDWHVWKDWWKHPXOWLSRLQW WUDYHUVHUHTXLUHPHQWFDQEHVDWLVILHGE\VDPSOLQJYLD³DPXOWLKROHSUREHGHVLJQHGWRVDPSOHDW WKHSUHVFULEHGSRLQWVZLWKDIORZSHUFHQWRIPHDQIORZUDWH´ $1$/<7,&$/5(68/76 ZƵŶηdŽƚĂů&ůŽǁ ;>ͬŵͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϭͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϮͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϯͿ 0HDQ3UREH 3RUW6DPSOHG )ORZ /P  5XQ/30  䧮    䧮    䧮   5XQ/30  䧮    䧮    䧮    &DOLEUDWLRQFRQGXFWHGLQDFFRUGDQFHZLWK(PLVVLRQ0HDVXUHPHQW&HQWHU*XLGHOLQH'RFXPHQW±(0&*' 1RWHV BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB $SSURYHGIRU5HOHDVH'DWH 2/17/2022 Probe size: 20S Mr. Jordan Williamson CEO GAS Inc. 303 W. 3rd Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. March 15, 2021 Sincerely, Steffan M. Johnson, Group Leader Measurement Technology Group If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. cc: Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leather.james@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Heather Sessing, Oklahoma DEQ, (Heather.sessing@deq.ok.gov) Cooper Green GAS Type of Sources Tested: info@gasinc.us Stationary Internal Combustion Engines • 4 Stroke Rich Burn Engines • 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods: • EPA Method 1 & 1A – Sampling & Traverse Points • EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream • EPA Method 3A – Oxygen • EPA Method 7E – NOX • EPA Method 10 – Carbon Monoxide • EPA Method 25A – Volatile Organic Compounds • ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. • Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Types of Analyzers: • Gasmet DX4000 FTIR • Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory • Testo 350 • Flame Ionization Detector 580-225-0403 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 1 Minute Average Data Sheet Crusoe Energy Systems, Inc.Client: Residue Booster Station Unit Number: 2026-06 Make:Waukesha Location:9394 GSIModel: 1656720Serial Number: RAW Result Data Stability 4/21/2025 05:38 0.7590.053-0.003 0.006 0.1950.000 0.000 0.014 0.0170.0080.451 0.209 0.0000.000 0.000 844.00.260.175 0.001 0.81 0.00 180.0 Pre Test Baseline Direct 4/21/2025 05:46 0.0000.4090.003 0.006 0.0000.105 0.007 0.000 0.1130.0000.209 0.000 0.1000.161 0.000 844.00.100.000 0.000 0.41 0.00 180.0 4/21/2025 05:46 0.0000.0000.000 0.000 0.0760.064 0.001 0.000 0.2490.0990.174 0.000 0.0730.063 0.009 844.00.100.015 0.000 0.00 0.00 180.0 4/21/2025 05:47 0.0000.205-0.001 0.000 0.0000.000 0.000 0.029 0.0000.0020.043 0.000 0.0190.000 0.000 844.00.030.023 0.000 0.20 0.00 180.0 CTS Direct 4/21/2025 05:48 0.0000.2320.013 0.016 0.0000.000 0.010 0.000 0.3020.0130.000 98.620 0.0000.000 0.021 844.065.820.037 0.028 0.23 0.00 179.0 4/21/2025 05:49 0.0000.0000.010 0.015 0.0000.000 0.000 0.063 0.3510.0000.000 98.596 0.0000.072 0.027 844.065.830.059 0.026 0.00 0.00 180.0 4/21/2025 05:49 0.2300.1310.009 0.012 0.0000.000 0.000 0.000 0.3640.0660.000 98.596 0.0000.167 0.000 844.065.730.000 0.028 0.36 0.00 180.0 High O2 Direct 4/21/2025 05:55 0.0000.5000.002 0.000 0.2710.000 0.007 0.163 0.1280.0000.403 0.000 0.0800.000 0.018 844.00.120.000 0.000 0.50 20.68 180.0 4/21/2025 05:56 0.0000.4890.002 0.000 0.0000.000 0.000 0.053 0.1780.0150.592 0.000 0.1320.054 0.035 844.00.380.267 0.000 0.49 20.68 180.0 4/21/2025 05:56 0.0000.3780.000 0.000 0.0000.000 0.000 0.188 0.3370.0001.029 0.000 0.0000.000 0.000 844.00.000.000 0.000 0.38 20.73 180.0 NO2/Mid O2 Direct 4/21/2025 06:00 102.6300.2140.002 0.000 0.6300.000 0.978 0.000 1.1840.0000.000 0.000 0.0000.000 0.000 844.00.000.000 0.000 102.84 10.56 180.0 4/21/2025 06:00 102.0910.176-0.001 0.000 0.2210.000 0.965 0.000 0.5680.0000.000 0.000 0.0000.000 0.000 844.00.000.000 0.000 102.27 10.58 180.0 4/21/2025 06:01 102.9110.0000.000 0.000 0.3090.000 0.969 0.000 0.8950.0000.387 0.000 0.0000.081 0.000 844.00.000.000 0.000 102.91 10.55 180.0 Spike Direct 4/21/2025 06:04 0.000249.9380.000 4.949 4.497491.809 1.801 2.267 0.7370.2880.000 0.956 252.4650.000 0.915 844.0256.732.692 9.795 249.94 0.00 180.0 4/21/2025 06:04 0.000250.7170.000 4.945 5.271492.798 1.784 1.990 0.9090.2170.500 0.955 252.2940.335 0.862 844.0256.282.436 9.794 250.72 0.00 180.0 4/21/2025 06:05 0.000249.006-0.002 4.946 4.985492.600 1.775 1.887 0.6480.1500.817 0.956 252.9900.322 0.835 844.0257.032.593 9.804 249.01 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline System 4/21/2025 06:07 0.0000.0000.009 0.020 0.0000.560 0.000 0.089 0.1590.0000.891 0.000 0.3020.000 0.166 844.00.680.073 0.000 0.00 0.00 180.0 4/21/2025 06:08 0.0000.4290.007 0.015 0.0000.452 0.000 0.150 0.0000.0000.943 0.000 0.2750.000 0.173 844.00.820.301 0.000 0.43 0.00 180.0 4/21/2025 06:08 0.0000.1390.011 0.016 0.0000.466 0.000 0.167 0.0000.0030.774 0.000 0.1600.000 0.167 844.00.640.219 0.000 0.14 0.00 180.0 CTS System with Response Time 4/21/2025 06:09 0.0000.0000.014 0.018 0.0000.134 0.000 0.000 0.1070.0000.000 98.253 0.0000.000 0.204 844.065.910.000 0.024 0.00 0.00 180.0 4/21/2025 06:10 0.0000.0000.013 0.024 0.0000.177 0.000 0.000 0.0000.0000.000 98.475 0.0000.185 0.180 844.066.010.000 0.024 0.00 0.00 180.0 4/21/2025 06:10 0.0000.0000.016 0.027 0.0000.110 0.000 0.000 0.0310.0000.000 98.480 0.0000.000 0.195 844.066.050.000 0.022 0.00 0.00 180.0 NO2/Mid O2 System with Response Time 4/21/2025 06:12 100.3532.8110.011 0.020 0.0000.834 0.979 0.044 0.0000.0000.338 0.000 0.0000.418 0.096 844.00.190.000 0.000 103.16 10.48 180.0 4/21/2025 06:13 100.6553.5200.003 0.004 0.2580.248 1.015 0.000 0.1880.0000.000 0.000 0.1180.000 0.057 844.00.260.037 0.000 104.17 10.54 180.0 4/21/2025 06:13 100.2862.7140.006 0.012 0.0000.672 0.972 0.107 0.0000.0000.000 0.000 0.1910.000 0.080 844.00.350.000 0.000 103.00 10.54 180.0 Spike System with Response Time 4/21/2025 06:15 0.000247.0980.001 4.926 4.715488.605 1.811 1.908 0.4610.0220.357 1.061 251.0620.081 0.996 844.0255.432.498 9.740 247.10 0.00 180.0 4/21/2025 06:15 0.000247.4500.006 4.928 4.874488.974 1.742 1.924 0.6660.0180.439 1.065 252.3020.000 0.815 844.0256.182.301 9.739 247.45 0.00 180.0 4/21/2025 06:16 0.000247.6220.003 4.941 5.005488.190 1.795 2.263 0.3190.0430.049 1.069 252.1110.000 0.914 844.0256.092.157 9.743 247.62 0.00 180.0 Baseline System with Response Time 4/21/2025 06:20 0.0000.4380.008 0.029 0.1660.415 0.000 0.101 0.0000.0000.392 0.000 0.1990.000 0.102 844.00.570.247 0.000 0.44 0.00 180.0 4/21/2025 06:20 0.0000.7630.003 0.011 0.1640.156 0.003 0.102 0.0000.0030.251 0.000 0.3620.000 0.037 844.00.630.291 0.000 0.76 0.00 180.0 4/21/2025 06:20 0.0000.0000.002 0.010 0.0000.282 0.031 0.070 0.4040.0000.016 0.000 0.3320.000 0.060 844.00.630.270 0.000 0.00 0.00 180.0 Run 1 - A 30minute/60min 4/21/2025 13:39 1.9467.01717.216 10.187 37.11453.344 2.313 43.613 0.9490.0440.700 0.000 0.1640.517 0.304 832.01.120.522 0.000 8.96 0.00 180.0 4/21/2025 13:40 0.0005.86017.215 10.230 44.82358.010 2.618 37.169 0.9690.0040.676 0.000 0.0690.827 0.353 832.01.310.808 0.000 5.86 0.00 179.0 4/21/2025 13:41 0.00010.15717.253 10.190 46.28468.264 4.249 50.838 0.9110.0210.000 0.000 0.0250.775 0.355 832.01.190.688 0.000 10.16 0.00 180.0 4/21/2025 13:42 0.00013.07517.224 10.223 40.30168.955 4.431 60.721 0.6000.0430.000 0.000 0.0450.969 0.405 832.01.230.563 0.000 13.07 0.00 180.0 4/21/2025 13:43 0.0009.77017.258 10.252 39.36057.608 3.828 48.483 0.5960.0360.000 0.000 0.0310.953 0.369 832.01.290.790 0.000 9.77 0.00 180.0 4/21/2025 13:44 0.00012.20917.255 10.198 39.68362.780 4.399 53.691 0.4530.0190.000 0.000 0.0550.795 0.343 832.01.120.568 0.000 12.21 0.00 180.0 4/21/2025 13:45 1.11815.60317.262 10.199 38.63960.365 4.730 56.656 0.4210.0000.000 0.000 0.1790.844 0.386 832.01.430.713 0.000 16.72 0.00 180.0 4/21/2025 13:46 1.55410.58917.230 10.229 35.36449.624 3.509 48.838 0.1910.0110.000 0.000 0.1700.866 0.364 832.01.330.654 0.000 12.14 0.00 179.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 13:47 0.00011.13417.262 10.320 36.61647.111 3.871 45.822 0.1980.0080.000 0.000 0.0340.780 0.349 832.01.180.672 0.000 11.13 0.00 180.0 4/21/2025 13:49 0.00012.04517.247 10.288 37.24150.509 4.478 47.397 0.4120.0200.000 0.000 0.0910.798 0.350 832.01.260.709 0.000 12.04 0.00 180.0 4/21/2025 13:50 1.77710.73117.278 10.288 35.95547.043 3.546 44.932 0.2470.0040.346 0.000 0.1660.674 0.384 832.01.460.786 0.000 12.51 0.00 180.0 4/21/2025 13:51 0.00010.62417.242 10.317 35.86947.169 3.348 47.141 0.2960.0100.000 0.000 0.0420.790 0.408 832.01.270.617 0.000 10.62 0.00 180.0 4/21/2025 13:52 1.7239.10217.212 10.348 42.49257.694 3.738 41.539 0.4020.0340.305 0.000 0.2060.691 0.387 832.01.480.751 0.000 10.83 0.00 180.0 4/21/2025 13:53 1.05212.17517.225 10.230 40.78160.595 4.660 47.721 0.4610.0030.222 0.000 0.1700.842 0.363 832.01.370.713 0.000 13.23 0.00 180.0 4/21/2025 13:54 0.00012.96217.222 10.256 44.54267.712 5.062 50.296 0.4050.0050.151 0.000 0.0001.061 0.379 832.01.130.551 0.000 12.96 0.00 180.0 4/21/2025 13:55 0.88216.88617.289 10.230 40.42159.543 5.257 52.761 0.2970.0140.125 0.000 0.1200.880 0.393 832.01.550.965 0.000 17.77 0.00 180.0 4/21/2025 13:56 0.00015.38617.241 10.213 38.42654.235 4.791 47.979 0.4910.0000.485 0.000 0.0170.822 0.321 832.01.180.783 0.000 15.39 0.00 179.0 4/21/2025 13:57 0.00014.40717.224 10.316 37.65754.713 4.583 50.041 0.0880.0400.000 0.000 0.0030.870 0.365 832.01.220.727 0.000 14.41 0.00 180.0 4/21/2025 13:58 0.00012.53917.266 10.251 37.42249.892 4.022 47.938 0.2720.0000.423 0.000 0.0000.689 0.317 832.01.130.739 0.000 12.54 0.00 180.0 4/21/2025 13:59 0.00011.38617.282 10.210 40.28357.261 4.394 46.706 0.1700.0000.655 0.000 0.0000.778 0.330 832.01.090.642 0.000 11.39 0.00 180.0 4/21/2025 14:00 0.93211.43617.246 10.267 39.95457.765 4.772 44.358 0.0000.0100.277 0.000 0.0000.732 0.261 832.00.940.624 0.000 12.37 0.00 180.0 4/21/2025 14:01 0.00016.99617.212 10.282 41.35065.482 5.878 51.866 0.0380.0340.013 0.000 0.0000.706 0.343 832.01.090.614 0.000 17.00 0.00 180.0 4/21/2025 14:02 0.00014.73017.267 10.236 43.28862.693 4.994 48.638 0.3000.0000.558 0.000 0.0420.669 0.276 832.01.000.612 0.000 14.73 0.00 180.0 4/21/2025 14:03 0.86117.64917.276 10.213 40.91457.554 5.579 50.364 0.2750.0000.971 0.000 0.0000.533 0.289 832.01.020.665 0.000 18.51 0.00 180.0 4/21/2025 14:04 0.72113.21417.296 10.279 38.60552.872 4.619 43.513 0.0000.0030.733 0.000 0.0000.744 0.305 832.01.140.791 0.000 13.94 0.00 180.0 4/21/2025 14:05 0.50113.28617.260 10.285 43.14865.603 5.022 48.487 0.2610.0030.653 0.000 0.0000.595 0.305 832.01.080.708 0.000 13.79 0.00 180.0 4/21/2025 14:06 0.00017.07917.271 10.203 40.90765.656 5.721 52.899 0.1840.0000.887 0.000 0.0000.515 0.267 832.00.980.665 0.000 17.08 0.00 180.0 4/21/2025 14:07 0.17417.04317.221 10.182 40.24063.512 5.242 52.649 0.3490.0000.788 0.000 0.0000.774 0.261 832.01.030.754 0.000 17.22 0.00 179.0 4/21/2025 14:08 0.78715.66217.250 10.283 46.21272.807 5.381 52.770 0.3260.0100.342 0.000 0.0000.797 0.251 832.00.830.490 0.000 16.45 0.00 180.0 4/21/2025 14:09 1.61116.86317.241 10.245 40.02559.869 5.727 50.930 0.2350.0010.972 0.000 0.0000.662 0.225 832.00.870.635 0.000 18.47 0.00 180.0 0.52112.92117.248 10.248 40.13158.541 4.492 48.892 0.3600.0130.343 0.000 0.0540.765 0.334 832.001.1770.684 0.000 13.442 0.000 179.9Avg. Spike 1 4/21/2025 14:11 4.25326.86015.802 9.711 38.62291.149 5.076 45.833 0.9840.0001.500 0.957 17.3810.436 0.322 832.018.970.458 0.690 31.11 0.00 180.0 Run 1 - B 30minute/60min 4/21/2025 14:13 0.47316.13017.319 10.247 42.51661.574 5.490 49.527 0.4610.0001.090 0.000 0.0000.412 0.214 832.00.810.570 0.000 16.60 0.00 180.0 4/21/2025 14:14 0.62712.11317.362 10.276 38.26248.606 3.938 41.721 0.1370.0001.552 0.000 0.0000.666 0.216 832.00.870.655 0.000 12.74 0.00 180.0 4/21/2025 14:15 0.64511.47817.359 10.268 48.70961.041 4.272 38.580 0.3870.0001.095 0.000 0.0000.895 0.220 832.00.790.517 0.000 12.12 0.00 180.0 4/21/2025 14:16 0.30614.77417.376 10.242 45.03370.314 5.514 50.982 0.4740.0010.789 0.000 0.0000.842 0.181 832.00.830.699 0.000 15.08 0.00 180.0 4/21/2025 14:17 0.97618.74917.354 10.227 43.01763.384 5.919 52.034 0.4430.0030.927 0.000 0.0000.561 0.186 832.00.740.553 0.000 19.72 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 14:18 0.90614.47717.354 10.231 40.95562.309 5.148 48.653 0.2130.0021.056 0.000 0.0000.762 0.197 832.00.860.696 0.000 15.38 0.00 180.0 4/21/2025 14:19 0.38818.19217.329 10.255 43.08063.660 5.693 52.857 0.3920.0000.755 0.000 0.0000.973 0.165 832.00.670.512 0.000 18.58 0.00 180.0 4/21/2025 14:20 0.95815.95717.338 10.318 40.88259.671 5.478 50.293 0.4090.0190.468 0.000 0.0000.845 0.159 832.00.640.490 0.000 16.91 0.00 180.0 4/21/2025 14:21 0.83215.48317.298 10.255 43.55362.893 5.292 48.149 0.3850.0030.957 0.000 0.0000.708 0.172 832.00.640.451 0.000 16.32 0.00 180.0 4/21/2025 14:22 0.88617.29417.301 10.239 41.31452.246 5.501 46.073 0.5760.0191.351 0.000 0.0000.546 0.159 832.00.790.709 0.000 18.18 0.00 180.0 4/21/2025 14:23 0.00011.87817.278 10.263 39.96550.113 4.609 42.872 0.3170.0140.932 0.000 0.0000.958 0.161 832.00.840.776 0.000 11.88 0.00 179.0 4/21/2025 14:24 0.01114.92917.346 10.325 42.51556.511 5.402 49.229 0.5270.0730.354 0.000 0.0000.920 0.143 832.00.710.631 0.000 14.94 0.00 180.0 4/21/2025 14:25 0.84314.36717.350 10.304 40.07951.756 4.995 47.118 0.4060.0611.095 0.000 0.0000.692 0.170 832.00.750.606 0.000 15.21 0.00 180.0 4/21/2025 14:26 0.00012.25417.389 10.265 39.66246.422 4.348 42.986 0.6830.0001.493 0.000 0.0000.967 0.142 832.00.680.595 0.000 12.25 0.00 180.0 4/21/2025 14:27 0.33110.98317.341 10.223 41.91154.826 4.387 47.171 0.7810.0001.471 0.000 0.0000.963 0.114 832.00.650.629 0.000 11.31 0.00 180.0 4/21/2025 14:29 1.02210.98617.341 10.253 41.23560.834 4.826 51.151 0.4610.0120.739 0.000 0.0000.594 0.155 832.00.750.657 0.000 12.01 0.00 180.0 4/21/2025 14:30 0.87413.22817.349 10.262 42.20459.450 5.031 52.256 0.6960.0181.027 0.000 0.0000.746 0.132 832.00.630.548 0.000 14.10 0.00 180.0 4/21/2025 14:31 0.75813.91217.367 10.226 41.45260.907 4.745 56.222 0.5910.0570.664 0.000 0.0000.838 0.116 832.00.590.541 0.000 14.67 0.00 180.0 4/21/2025 14:32 0.84511.24717.393 10.279 39.64448.395 3.996 46.529 0.7710.0011.080 0.000 0.0000.624 0.110 832.00.750.788 0.000 12.09 0.00 180.0 4/21/2025 14:33 0.4198.48717.365 10.279 41.53749.275 3.712 39.168 0.7210.0281.378 0.000 0.0000.765 0.107 832.00.640.636 0.000 8.91 0.00 179.0 4/21/2025 14:34 0.62411.29217.313 10.245 45.43660.504 4.845 47.439 0.6590.0000.970 0.000 0.0000.782 0.127 832.00.660.617 0.000 11.92 0.00 180.0 4/21/2025 14:35 0.41110.10917.323 10.296 51.22159.934 4.204 38.144 0.6590.0001.550 0.000 0.0000.834 0.164 832.00.630.458 0.000 10.52 0.00 180.0 4/21/2025 14:36 0.52714.35917.327 10.280 64.46071.747 4.846 40.299 1.7340.0061.577 0.000 0.0000.931 0.173 832.00.950.899 0.000 14.89 0.00 180.0 4/21/2025 14:37 0.94713.63517.361 10.241 44.51360.096 4.884 48.083 1.0130.0001.338 0.000 0.0000.830 0.104 832.00.670.690 0.000 14.58 0.00 180.0 4/21/2025 14:38 0.00013.43317.360 10.289 57.19271.450 5.008 45.686 1.3810.0001.415 0.000 0.0000.895 0.166 832.00.900.857 0.000 13.43 0.00 180.0 4/21/2025 14:39 1.52615.44017.397 10.257 43.80469.905 5.811 54.399 0.7120.0030.520 0.000 0.0000.740 0.143 832.00.820.797 0.000 16.97 0.00 180.0 4/21/2025 14:40 0.87914.13517.333 10.216 51.80672.697 4.875 47.849 1.2390.0121.156 0.000 0.0000.891 0.173 832.00.790.666 0.000 15.01 0.00 180.0 4/21/2025 14:41 1.05718.29117.349 10.180 46.94177.265 5.596 58.074 1.2010.0000.852 0.000 0.0170.731 0.189 832.00.880.734 0.000 19.35 0.00 180.0 4/21/2025 14:42 0.80514.11517.306 10.158 41.13666.831 5.057 55.331 0.7530.0000.754 0.000 0.0000.653 0.152 832.00.700.590 0.000 14.92 0.00 179.0 4/21/2025 14:43 0.35312.30217.337 10.273 45.51372.409 4.881 51.837 0.9580.0300.644 0.000 0.0001.006 0.179 832.00.740.575 0.000 12.66 0.00 180.0 0.64113.80117.344 10.256 44.31860.901 4.943 48.024 0.6710.0121.035 0.000 0.0010.786 0.160 832.000.7460.638 0.000 14.442 0.000 179.9Avg. 0.58113.36117.296 10.252 42.22459.721 4.718 48.458 0.5160.0120.689 0.000 0.0270.775 0.247 832.000.9610.661 0.000 13.942 0.000 179.9Run 1 Avg: Baseline 1 4/21/2025 14:45 0.0000.1380.040 0.029 0.0000.290 0.034 1.311 0.0000.0000.000 0.000 0.1950.000 0.052 832.00.680.571 0.000 0.14 0.00 180.0 Run 2 - A 30minute/60min 4/21/2025 14:47 1.16916.95317.093 10.125 45.73676.201 5.906 56.434 0.9880.0020.702 0.000 0.0000.509 0.212 832.00.920.737 0.000 18.12 0.00 179.0 4/21/2025 14:48 1.30314.00917.302 10.298 40.23458.775 4.866 49.434 0.9900.0210.608 0.000 0.0000.772 0.151 832.00.680.560 0.000 15.31 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 14:49 0.70213.77917.327 10.232 40.35461.383 5.316 53.291 0.9690.0140.684 0.000 0.0000.881 0.177 832.00.720.556 0.000 14.48 0.00 180.0 4/21/2025 14:50 1.29110.94717.343 10.233 39.29858.215 4.845 48.266 0.9030.0050.612 0.000 0.0000.797 0.152 832.00.830.795 0.000 12.24 0.00 180.0 4/21/2025 14:51 1.06313.06917.381 10.259 40.68163.077 5.093 54.426 0.8650.0000.453 0.000 0.0000.528 0.174 832.00.830.729 0.000 14.13 0.00 180.0 4/21/2025 14:52 0.7658.29717.364 10.345 51.48063.726 3.498 38.408 1.4360.0001.404 0.000 0.0000.684 0.182 832.00.870.756 0.000 9.06 0.00 180.0 4/21/2025 14:53 1.52814.43917.350 10.266 46.53075.150 6.041 56.250 0.9750.0070.447 0.000 0.0000.843 0.229 832.00.980.781 0.000 15.97 0.00 180.0 4/21/2025 14:54 0.68912.05617.361 10.313 47.98170.998 5.104 47.053 1.2520.0060.793 0.000 0.0000.630 0.191 832.00.900.774 0.000 12.75 0.00 180.0 4/21/2025 14:55 1.96717.77517.395 10.284 42.54071.329 6.169 58.657 1.0750.0000.662 0.000 0.0000.861 0.179 832.00.840.724 0.001 19.74 0.00 180.0 4/21/2025 14:56 0.46313.79517.316 10.239 40.15661.196 5.254 51.367 1.0900.0000.376 0.000 0.0000.960 0.155 832.00.760.678 0.000 14.26 0.00 180.0 4/21/2025 14:57 0.09013.02817.316 10.229 39.51758.936 5.061 54.489 1.0210.0020.828 0.000 0.0000.742 0.203 832.00.840.645 0.000 13.12 0.00 180.0 4/21/2025 14:58 1.0739.99417.281 10.193 42.09063.792 4.733 50.528 1.2940.0000.905 0.000 0.0000.786 0.215 832.00.920.737 0.000 11.07 0.00 179.0 4/21/2025 14:59 0.88413.60617.327 10.269 42.92567.981 5.558 56.029 1.3550.0120.200 0.000 0.0000.611 0.193 832.00.810.638 0.000 14.49 0.00 180.0 4/21/2025 15:00 1.09312.12817.295 10.213 39.60057.991 5.160 51.366 1.1210.0030.377 0.000 0.0150.747 0.227 832.00.920.683 0.000 13.22 0.00 180.0 4/21/2025 15:01 1.23710.26217.306 10.267 41.71766.581 4.342 49.365 1.1770.0031.029 0.000 0.0000.747 0.197 832.00.790.595 0.000 11.50 0.00 180.0 4/21/2025 15:02 0.84214.47717.330 10.283 39.33854.270 5.005 53.839 1.2840.0000.515 0.000 0.0050.940 0.200 832.00.900.738 0.000 15.32 0.00 180.0 4/21/2025 15:03 0.0008.42917.340 10.244 40.67756.215 4.041 45.896 0.9170.0000.845 0.000 0.0000.762 0.230 832.00.910.675 0.000 8.43 0.00 180.0 4/21/2025 15:04 0.7199.76417.380 10.258 40.79156.313 4.605 44.318 0.9580.0140.931 0.000 0.0000.741 0.218 832.00.800.548 0.000 10.48 0.00 180.0 4/21/2025 15:05 0.90311.89717.351 10.311 38.27945.092 4.451 45.261 1.1320.0070.620 0.000 0.0000.713 0.201 832.00.920.770 0.000 12.80 0.00 179.0 4/21/2025 15:06 0.9997.94817.371 10.340 39.10744.725 3.851 40.261 0.8240.0010.853 0.000 0.0000.722 0.218 832.00.920.720 0.000 8.95 0.00 179.0 4/21/2025 15:07 0.6798.61617.412 10.301 38.47546.091 4.027 42.219 0.9510.0370.334 0.000 0.0000.901 0.224 832.00.860.617 0.000 9.30 0.00 180.0 4/21/2025 15:08 0.2057.87517.429 10.302 42.29451.074 4.074 43.418 1.1600.0020.933 0.000 0.0000.941 0.225 832.01.030.876 0.000 8.08 0.00 180.0 4/21/2025 15:09 1.0978.60017.343 10.210 40.76552.557 3.979 45.683 1.1720.0230.793 0.000 0.0000.743 0.208 832.00.920.753 0.000 9.70 0.00 180.0 4/21/2025 15:11 1.1188.48617.375 10.202 39.84756.050 4.436 48.278 1.0770.0000.245 0.000 0.0000.605 0.273 832.00.920.562 0.000 9.60 0.00 180.0 4/21/2025 15:12 1.2939.70617.397 10.232 41.67656.321 4.633 49.800 0.8640.0000.626 0.000 0.0000.950 0.240 832.01.050.861 0.000 11.00 0.00 180.0 4/21/2025 15:13 1.01310.24117.385 10.235 41.77254.324 4.468 51.050 0.9870.0000.348 0.000 0.1040.830 0.252 832.01.170.838 0.000 11.25 0.00 180.0 4/21/2025 15:14 1.0469.33617.402 10.216 40.79651.041 4.356 49.720 1.0610.0040.000 0.000 0.0080.780 0.254 832.01.020.750 0.000 10.38 0.00 180.0 4/21/2025 15:15 1.0369.21217.397 10.253 39.40644.489 3.731 46.460 1.0810.0230.049 0.000 0.0000.855 0.245 832.01.030.807 0.000 10.25 0.00 180.0 4/21/2025 15:16 0.9605.83817.376 10.217 43.16747.501 2.695 39.873 1.2660.0000.717 0.000 0.1040.774 0.251 832.01.170.839 0.000 6.80 0.00 180.0 4/21/2025 15:17 1.3328.26817.385 10.183 40.26849.552 4.000 49.198 1.1780.0040.262 0.000 0.0270.735 0.266 832.01.030.713 0.000 9.60 0.00 180.0 0.95211.09417.348 10.252 41.58358.032 4.643 49.021 1.0810.0060.605 0.000 0.0090.770 0.211 832.000.9090.715 0.000 12.047 0.000 179.9Avg. Spike 2 4/21/2025 15:20 1.63125.19415.897 9.736 42.771109.559 3.883 46.369 0.9910.0010.881 0.846 22.2280.678 0.309 832.024.201.191 0.867 26.82 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Run 2 - B 30minute/60min 4/21/2025 15:22 1.57512.87417.399 10.224 42.16069.351 5.454 60.772 1.2090.0000.000 0.000 0.2620.817 0.327 832.01.510.889 0.003 14.45 0.00 180.0 4/21/2025 15:23 0.90511.09017.413 10.215 40.90166.503 4.954 56.006 1.0430.0000.155 0.000 0.0750.783 0.309 832.01.070.566 0.000 11.99 0.00 180.0 4/21/2025 15:24 0.55010.51017.375 10.277 38.19648.556 4.018 46.950 1.2590.0010.479 0.000 0.0740.916 0.271 832.01.100.719 0.000 11.06 0.00 179.0 4/21/2025 15:25 1.1547.86017.383 10.283 40.82558.372 4.422 49.261 0.8340.0150.000 0.000 0.0000.686 0.284 832.01.080.771 0.000 9.01 0.00 180.0 4/21/2025 15:26 0.8729.67817.416 10.245 40.62359.597 4.343 53.966 1.2240.0000.173 0.000 0.1300.695 0.301 831.01.360.939 0.000 10.55 0.00 180.0 4/21/2025 15:27 1.1699.18117.361 10.279 42.18865.465 4.533 52.615 0.9940.0000.000 0.000 0.0520.810 0.323 832.01.110.613 0.000 10.35 0.00 180.0 4/21/2025 15:28 0.66511.83817.346 10.222 38.92153.043 4.496 52.282 1.0980.0000.000 0.000 0.0920.749 0.280 831.01.150.752 0.000 12.50 0.00 180.0 4/21/2025 15:29 0.6186.72417.336 10.320 43.67459.104 3.678 44.468 1.0150.0000.131 0.000 0.0180.726 0.300 831.01.150.790 0.000 7.34 0.00 180.0 4/21/2025 15:30 1.01911.98117.315 10.274 41.85364.237 5.070 56.521 1.1340.0000.000 0.000 0.0780.964 0.321 831.01.160.664 0.000 13.00 0.00 180.0 4/21/2025 15:31 1.4418.26717.333 10.254 42.33761.175 3.954 49.509 1.1650.0070.000 0.000 0.0730.916 0.300 831.01.150.719 0.000 9.71 0.00 180.0 4/21/2025 15:32 1.0219.44817.322 10.311 45.12366.828 4.227 48.921 0.9120.0000.000 0.000 0.0390.664 0.313 831.01.190.793 0.000 10.47 0.00 180.0 4/21/2025 15:33 1.26911.53017.322 10.202 43.72069.901 5.537 56.994 1.0300.0000.000 0.000 0.1500.378 0.305 831.01.390.952 0.000 12.80 0.00 180.0 4/21/2025 15:34 2.70216.03317.344 10.254 41.92458.383 5.786 54.836 1.0760.0000.000 0.000 0.0160.494 0.304 831.01.120.751 0.005 18.74 0.00 180.0 4/21/2025 15:35 0.9298.23717.334 10.245 39.05249.402 3.983 46.616 0.8000.0010.121 0.000 0.0030.606 0.329 831.01.200.811 0.000 9.17 0.00 180.0 4/21/2025 15:36 1.3666.72717.380 10.294 38.97657.811 4.011 50.375 0.7930.0000.000 0.000 0.0000.780 0.325 831.01.070.626 0.000 8.09 0.00 180.0 4/21/2025 15:37 1.3289.75117.361 10.237 40.96455.262 4.528 50.177 1.2050.0000.000 0.000 0.1280.758 0.274 831.01.371.043 0.000 11.08 0.00 180.0 4/21/2025 15:38 1.5876.49717.367 10.240 40.28755.206 4.123 48.563 0.8970.0000.000 0.000 0.0750.804 0.293 832.01.110.678 0.000 8.08 0.00 180.0 4/21/2025 15:39 0.9948.63617.344 10.245 42.38359.299 4.490 50.745 0.9550.0050.000 0.000 0.0290.598 0.337 832.01.240.811 0.000 9.63 0.00 180.0 4/21/2025 15:40 1.1729.51917.406 10.289 44.83064.290 4.625 47.269 1.1610.0000.000 0.000 0.1300.928 0.324 831.01.380.898 0.000 10.69 0.00 180.0 4/21/2025 15:41 0.46811.21017.389 10.257 48.43167.600 4.933 49.638 1.3830.0000.000 0.000 0.1030.908 0.320 831.01.330.888 0.000 11.68 0.00 180.0 4/21/2025 15:42 1.44110.37217.445 10.308 43.39568.198 5.046 53.136 0.9370.0060.000 0.000 0.1150.830 0.322 831.01.270.771 0.000 11.81 0.00 180.0 4/21/2025 15:43 0.9509.70817.373 10.257 45.37069.454 4.527 49.809 1.1090.0000.000 0.000 0.1830.600 0.298 831.01.521.111 0.000 10.66 0.00 180.0 4/21/2025 15:44 1.96511.14817.338 10.240 46.72779.702 5.577 59.027 1.1840.0000.000 0.000 0.1440.269 0.310 831.01.400.960 0.005 13.11 0.00 180.0 4/21/2025 15:45 2.13218.78117.299 10.211 45.22880.303 6.763 66.570 0.8880.0000.000 0.000 0.0760.463 0.393 831.01.360.747 0.006 20.91 0.00 180.0 4/21/2025 15:46 0.4389.72217.303 10.264 44.49569.595 5.156 52.447 0.9130.0000.000 0.000 0.1170.842 0.351 831.01.440.925 0.000 10.16 0.00 180.0 4/21/2025 15:47 2.10612.20017.312 10.205 42.67974.838 5.727 59.714 1.0970.0000.000 0.000 0.0680.475 0.361 831.01.410.931 0.006 14.31 0.00 180.0 4/21/2025 15:48 1.58915.17917.305 10.215 44.06282.437 6.567 66.986 1.0670.0000.000 0.000 0.1340.513 0.354 831.01.460.926 0.000 16.77 0.00 180.0 4/21/2025 15:49 1.62214.44317.310 10.234 41.01869.567 5.696 58.922 1.0100.0000.000 0.000 0.1540.744 0.334 831.01.531.055 0.000 16.07 0.00 180.0 4/21/2025 15:50 1.44012.04817.296 10.244 40.30564.225 5.105 56.728 0.8730.0000.000 0.000 0.1680.846 0.344 831.01.460.898 0.000 13.49 0.00 180.0 4/21/2025 15:51 0.9839.46317.283 10.327 38.62757.802 4.947 51.852 0.9040.0000.000 0.000 0.0410.703 0.323 831.01.180.742 0.000 10.45 0.00 180.0 1.24910.68917.350 10.256 42.30964.184 4.876 53.389 1.0390.0010.035 0.000 0.0910.709 0.318 831.231.2760.825 0.001 11.938 0.000 180.0Avg. 1.10010.89117.349 10.254 41.94661.108 4.760 51.205 1.0600.0040.320 0.000 0.0500.739 0.265 831.621.0920.770 0.000 11.992 0.000 179.9Run 2 Avg: GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline 2 4/21/2025 15:54 0.0000.1790.039 0.034 0.0000.530 0.029 1.308 0.0000.0000.000 0.000 0.1990.000 0.079 831.00.780.639 0.000 0.18 0.00 180.0 Run 3 - A 30minute/60min 4/21/2025 15:56 0.00012.00716.903 10.064 41.28569.041 6.283 53.731 0.6590.0120.000 0.000 0.1000.538 0.376 831.01.300.677 0.000 12.01 0.00 180.0 4/21/2025 15:57 0.5589.10317.234 10.270 40.19055.383 4.586 45.424 0.9570.0000.000 0.000 0.1060.724 0.328 831.01.501.110 0.000 9.66 0.00 180.0 4/21/2025 15:58 0.00010.90317.317 10.269 40.84462.763 5.912 52.840 0.7270.0000.000 0.000 0.0740.418 0.361 831.01.210.620 0.000 10.90 0.00 180.0 4/21/2025 15:59 0.7448.01517.356 10.321 39.62356.112 4.425 48.070 0.8450.0000.000 0.000 0.1410.978 0.334 831.01.390.871 0.000 8.76 0.00 180.0 4/21/2025 16:00 0.0009.27117.322 10.352 37.56343.942 4.365 44.089 0.4360.0000.000 0.000 0.0860.622 0.356 831.01.250.677 0.000 9.27 0.00 180.0 4/21/2025 16:01 0.0007.83617.357 10.349 39.34447.878 4.270 45.110 0.7570.0000.000 0.000 0.0350.940 0.343 831.01.130.619 0.000 7.84 0.00 180.0 4/21/2025 16:02 0.0007.06717.381 10.315 37.66546.976 3.788 46.035 0.6250.0000.000 0.000 0.0760.894 0.349 831.01.200.639 0.000 7.07 0.00 180.0 4/21/2025 16:03 0.0006.72417.351 10.356 37.60040.155 3.044 38.924 0.9630.0000.000 0.000 0.0280.765 0.339 831.01.340.951 0.000 6.72 0.00 180.0 4/21/2025 16:04 0.0006.72817.354 10.313 42.19555.893 4.492 48.199 0.7160.0000.000 0.000 0.0000.760 0.353 831.01.250.818 0.000 6.73 0.00 180.0 4/21/2025 16:05 0.0006.44517.378 10.327 40.00353.928 4.262 47.897 0.6900.0010.000 0.000 0.0220.762 0.359 831.01.170.638 0.000 6.44 0.00 180.0 4/21/2025 16:06 0.0009.42417.385 10.289 38.36646.416 4.196 49.740 0.7830.0000.000 0.000 0.0490.782 0.331 831.01.230.785 0.000 9.42 0.00 180.0 4/21/2025 16:07 0.0004.63617.408 10.391 39.23343.927 2.317 37.668 0.7170.0000.000 0.000 0.0960.654 0.360 831.01.400.871 0.000 4.64 0.00 180.0 4/21/2025 16:08 0.0006.31117.376 10.313 41.62858.985 4.277 48.966 0.6160.0000.000 0.000 0.0380.776 0.337 831.01.140.647 0.000 6.31 0.00 180.0 4/21/2025 16:09 0.0009.94217.310 10.276 40.46657.561 4.609 52.639 0.6480.0000.000 0.000 0.0410.747 0.373 831.01.350.844 0.000 9.94 0.00 180.0 4/21/2025 16:10 0.0007.79617.257 10.292 40.04056.058 4.775 52.973 0.6050.0000.000 0.000 0.0450.722 0.379 831.01.300.737 0.000 7.80 0.00 179.0 4/21/2025 16:11 0.0007.33117.282 10.325 38.64047.826 4.049 47.304 0.4330.0000.000 0.000 0.0180.719 0.366 831.01.230.715 0.000 7.33 0.00 180.0 4/21/2025 16:12 0.9917.07117.279 10.307 38.37946.790 3.162 44.857 0.7110.0000.000 0.000 0.2040.656 0.339 831.01.601.082 0.000 8.06 0.00 180.0 4/21/2025 16:13 0.0007.22717.272 10.320 42.21161.306 4.792 53.349 0.6650.0000.000 0.000 0.0130.747 0.345 831.01.220.773 0.000 7.23 0.00 180.0 4/21/2025 16:14 0.9675.95917.295 10.303 38.02553.519 3.785 45.771 0.6610.0000.000 0.000 0.1620.705 0.329 831.01.390.859 0.000 6.93 0.00 180.0 4/21/2025 16:15 0.00010.14217.311 10.312 40.15458.469 5.107 56.090 0.5310.0000.000 0.000 0.0000.931 0.388 831.01.160.571 0.000 10.14 0.00 180.0 4/21/2025 16:16 0.4908.86817.304 10.349 37.15649.139 3.923 49.149 0.6900.0000.000 0.000 0.1840.769 0.310 831.01.541.107 0.000 9.36 0.00 180.0 4/21/2025 16:17 0.0004.71517.309 10.341 38.51949.941 2.383 43.318 0.7590.0000.000 0.000 0.0790.682 0.324 831.01.300.855 0.000 4.71 0.00 180.0 4/21/2025 16:18 1.5238.01817.331 10.320 39.82050.732 4.158 47.812 0.5950.0010.000 0.000 0.0120.556 0.374 831.01.280.787 0.000 9.54 0.00 180.0 4/21/2025 16:19 0.0005.79717.298 10.280 42.30365.206 4.276 51.341 0.5820.0010.000 0.000 0.0380.961 0.356 831.01.090.507 0.000 5.80 0.00 180.0 4/21/2025 16:20 1.1289.77117.264 10.306 37.11345.636 4.019 49.721 0.7200.0000.000 0.000 0.1600.701 0.360 831.01.490.909 0.000 10.90 0.00 180.0 4/21/2025 16:21 0.0007.60517.201 10.293 38.89850.522 3.989 47.256 0.4860.0000.000 0.000 0.0670.661 0.380 831.01.420.888 0.000 7.60 0.00 179.0 4/21/2025 16:22 1.2636.80017.252 10.378 38.71548.571 3.798 42.843 0.7610.0000.000 0.000 0.1820.663 0.323 831.01.531.056 0.000 8.06 0.00 180.0 4/21/2025 16:23 0.5138.75617.284 10.287 40.91362.515 5.185 55.009 0.6890.0000.000 0.000 0.0220.998 0.357 831.01.270.796 0.000 9.27 0.00 180.0 4/21/2025 16:24 0.0007.63917.296 10.262 39.59759.410 4.495 51.947 0.6800.0030.000 0.000 0.0260.822 0.371 831.01.220.679 0.000 7.64 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 16:25 0.00011.55617.256 10.284 39.37554.956 5.071 54.743 0.7500.0000.000 0.000 0.0000.844 0.341 831.01.210.787 0.000 11.56 0.00 180.0 0.2737.98217.297 10.305 39.52953.319 4.260 48.427 0.6820.0010.000 0.000 0.0700.750 0.351 831.001.3040.796 0.000 8.255 0.000 179.9Avg. Spike 3 4/21/2025 16:27 1.58423.94415.626 9.733 36.501101.353 4.224 45.433 0.5790.0000.000 0.803 21.8160.508 0.437 831.024.171.420 0.853 25.53 0.00 180.0 Run 3 - B 30minute/60min 4/21/2025 16:29 0.0007.64917.308 10.297 48.57067.230 4.952 47.255 0.8380.0000.000 0.000 0.0850.815 0.409 831.01.410.758 0.002 7.65 0.00 180.0 4/21/2025 16:30 0.00010.86917.342 10.312 49.75973.733 5.627 52.493 1.0020.0000.000 0.000 0.1260.384 0.387 831.01.540.953 0.000 10.87 0.00 180.0 4/21/2025 16:31 1.59814.23017.344 10.339 43.89469.797 5.798 55.519 0.9400.0000.000 0.000 0.1430.295 0.377 831.01.641.122 0.000 15.83 0.00 180.0 4/21/2025 16:32 1.30914.66717.251 10.268 46.49769.103 6.043 52.721 1.0650.0000.000 0.000 0.2410.195 0.385 831.01.741.090 0.000 15.98 0.00 180.0 4/21/2025 16:33 0.00011.20317.211 10.249 47.17468.970 5.095 50.952 1.1010.0000.000 0.000 0.0880.262 0.398 831.01.480.903 0.000 11.20 0.00 180.0 4/21/2025 16:34 1.44913.22717.246 10.307 42.83165.257 6.227 55.367 0.9970.0000.000 0.000 0.1620.366 0.339 831.01.611.157 0.000 14.68 0.00 180.0 4/21/2025 16:36 0.00012.52517.214 10.257 42.05761.850 5.840 53.169 0.6200.0000.000 0.000 0.0950.503 0.337 831.01.380.918 0.000 12.53 0.00 180.0 4/21/2025 16:37 0.00013.11817.249 10.295 41.01458.208 5.896 54.416 0.6910.0000.000 0.000 0.0290.468 0.373 831.01.290.767 0.000 13.12 0.00 180.0 4/21/2025 16:38 0.0006.66317.307 10.314 41.98058.194 4.416 47.777 0.5180.0000.000 0.000 0.0610.730 0.414 831.01.370.724 0.000 6.66 0.00 180.0 4/21/2025 16:39 0.00012.33017.323 10.234 42.87267.837 6.397 60.278 0.6150.0000.000 0.000 0.0030.496 0.357 831.01.140.639 0.000 12.33 0.00 180.0 4/21/2025 16:40 0.00010.74117.337 10.345 43.18658.628 5.205 48.809 0.6820.0000.000 0.000 0.0000.942 0.383 831.01.250.726 0.000 10.74 0.00 180.0 4/21/2025 16:41 0.0009.80717.356 10.309 43.32362.549 5.879 51.521 0.6320.0000.000 0.000 0.0100.447 0.377 831.01.190.641 0.000 9.81 0.00 180.0 4/21/2025 16:42 0.00011.03717.318 10.281 41.98861.235 5.604 52.193 0.7630.0000.000 0.000 0.1000.535 0.342 831.01.390.908 0.000 11.04 0.00 180.0 4/21/2025 16:43 0.0009.61917.333 10.330 44.66167.124 5.436 51.867 0.8440.0000.000 0.000 0.0000.738 0.412 831.01.370.826 0.000 9.62 0.00 180.0 4/21/2025 16:44 0.0009.99317.283 10.283 43.50065.796 5.173 50.877 0.4650.0000.000 0.000 0.0740.714 0.415 831.01.360.679 0.000 9.99 0.00 180.0 4/21/2025 16:45 0.00014.00117.273 10.255 44.12274.071 6.477 59.157 0.7630.0000.000 0.000 0.0910.360 0.362 831.01.290.715 0.000 14.00 0.00 180.0 4/21/2025 16:46 0.00011.37017.253 10.334 39.58651.423 5.459 48.081 0.6410.0000.000 0.000 0.0570.344 0.412 831.01.490.909 0.000 11.37 0.00 180.0 4/21/2025 16:47 0.00011.85517.314 10.308 39.49042.101 5.260 42.461 0.6500.0000.000 0.000 0.0810.886 0.336 831.01.310.841 0.000 11.86 0.00 180.0 4/21/2025 16:48 0.0007.11817.396 10.355 37.85036.545 3.494 36.593 0.5740.0000.000 0.000 0.0640.806 0.395 831.01.320.700 0.000 7.12 0.00 180.0 4/21/2025 16:49 0.0005.19317.399 10.351 47.36659.772 3.748 45.243 0.6550.0010.000 0.000 0.0000.927 0.397 831.01.290.741 0.000 5.19 0.00 180.0 4/21/2025 16:50 0.0006.20317.424 10.352 39.73151.865 3.760 45.570 0.4780.0000.000 0.000 0.0370.850 0.390 831.01.290.716 0.000 6.20 0.00 180.0 4/21/2025 16:51 0.0006.87317.434 10.355 43.05562.983 5.092 51.815 0.4600.0000.000 0.000 0.0670.829 0.399 831.01.390.790 0.000 6.87 0.00 180.0 4/21/2025 16:52 0.0008.14717.369 10.368 42.25958.986 4.580 52.259 0.6920.0000.000 0.000 0.0940.753 0.378 831.01.450.894 0.000 8.15 0.00 180.0 4/21/2025 16:53 0.0007.77717.357 10.264 41.95456.654 4.733 49.396 0.6600.0000.000 0.000 0.0000.838 0.369 831.01.310.860 0.000 7.78 0.00 180.0 4/21/2025 16:54 0.0007.34017.288 10.307 48.48163.977 4.607 46.328 0.7870.0000.000 0.000 0.0150.766 0.380 831.01.330.826 0.000 7.34 0.00 180.0 4/21/2025 16:55 0.00012.81917.266 10.293 40.15248.818 5.164 50.704 0.4510.0000.000 0.000 0.1020.791 0.390 831.01.410.790 0.000 12.82 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 16:56 0.0006.11017.301 10.327 42.41851.263 3.429 41.324 0.4020.0000.000 0.000 0.0700.875 0.393 831.01.340.723 0.000 6.11 0.00 180.0 4/21/2025 16:57 0.0006.22517.337 10.314 54.87467.773 4.478 42.387 0.7620.0000.000 0.000 0.0100.853 0.444 831.01.330.654 0.000 6.22 0.00 180.0 4/21/2025 16:58 0.00012.43617.367 10.276 43.74869.933 6.146 55.912 0.6970.0000.000 0.000 0.0310.673 0.381 831.01.220.638 0.000 12.44 0.00 180.0 4/21/2025 16:59 0.00012.48217.307 10.280 42.21765.232 5.820 52.949 0.6740.0000.000 0.000 0.1440.388 0.359 831.01.621.137 0.000 12.48 0.00 180.0 0.14510.12117.317 10.305 43.68761.230 5.195 50.180 0.7040.0000.000 0.000 0.0690.628 0.383 831.001.3850.825 0.000 10.267 0.000 180.0Avg. 0.2099.05217.307 10.305 41.60857.274 4.727 49.303 0.6930.0000.000 0.000 0.0700.689 0.367 831.001.3440.810 0.000 9.261 0.000 180.0Run 3 Avg: Baseline 3 4/21/2025 17:02 0.0000.0000.019 0.018 0.0000.206 0.015 0.939 0.0000.0000.000 0.000 0.1050.000 0.112 831.00.720.591 0.000 0.00 0.00 180.0 Post CTS 4/21/2025 17:04 0.0000.7880.025 0.023 0.0000.000 0.016 0.476 0.0000.0000.000 98.013 0.0000.000 0.156 831.065.850.283 0.016 0.79 0.00 180.0 4/21/2025 17:04 0.0000.0000.020 0.024 0.0000.000 0.036 0.467 0.0000.0000.000 98.579 0.0000.000 0.138 831.066.340.507 0.012 0.00 0.00 180.0 4/21/2025 17:04 0.0000.3580.019 0.030 0.0000.000 0.000 0.464 0.1810.0000.000 99.162 0.0000.000 0.200 831.066.580.110 0.018 0.36 0.00 180.0 Post NO2/Mid O2 4/21/2025 17:06 97.2004.0650.009 0.019 0.0720.426 0.997 0.404 0.1990.0000.355 0.000 0.0000.000 0.105 831.00.290.125 0.000 101.26 10.31 180.0 4/21/2025 17:06 98.4954.2670.004 0.000 0.1390.395 0.985 0.227 0.0480.0100.000 0.000 0.0900.667 0.091 831.00.630.542 0.000 102.76 10.29 180.0 4/21/2025 17:06 98.6605.3250.007 0.001 0.0000.728 0.975 0.266 0.0100.0000.000 0.000 0.0000.046 0.144 831.00.540.377 0.000 103.99 10.34 180.0 Post 5-Gas 4/21/2025 17:07 0.000243.8500.017 4.894 6.438476.960 1.493 2.169 2.1500.6480.507 1.322 249.7920.000 0.624 831.0254.423.755 9.653 243.85 0.00 180.0 4/21/2025 17:07 0.000246.2850.006 4.910 4.300483.552 1.643 2.324 0.5350.2930.000 1.160 250.8820.360 0.860 831.0255.262.824 9.714 246.29 0.00 180.0 4/21/2025 17:07 0.000246.6020.003 4.946 5.386484.055 1.578 1.976 1.7300.2161.629 1.174 251.5100.000 0.649 831.0255.442.774 9.728 246.60 0.00 180.0 4/21/2025 17:07 0.000246.4230.013 4.911 4.816484.382 1.621 2.351 0.2520.1730.574 1.131 251.3220.000 0.802 831.0255.452.653 9.747 246.42 0.00 180.0 4/21/2025 17:08 0.000247.5650.008 4.898 4.752485.418 1.598 2.154 0.7130.2410.457 1.140 252.0000.162 0.838 831.0256.212.667 9.742 247.56 0.00 180.0 4/21/2025 17:08 0.000246.9040.010 4.874 0.645486.217 1.676 2.398 1.4820.2990.760 1.143 252.9910.000 1.288 831.0258.052.584 9.740 246.90 0.00 180.0 End of Test Purge 4/21/2025 17:09 0.0000.7340.001 0.013 0.2881.156 0.000 0.157 0.0750.0030.154 0.000 0.6540.000 0.197 831.01.490.662 0.012 0.73 0.00 180.0 4/21/2025 17:09 0.0000.0000.002 0.003 0.0001.484 0.006 0.213 0.0020.0000.000 0.000 0.5580.000 0.136 831.01.360.797 0.000 0.00 0.00 180.0 4/21/2025 17:10 0.0001.2040.001 0.029 0.0000.597 0.015 0.177 0.0000.0070.000 0.000 0.7440.071 0.056 831.01.210.534 0.000 1.20 0.00 180.0 4/21/2025 17:10 0.0000.4550.002 0.020 0.0000.605 0.036 0.358 0.2960.0000.000 0.000 0.3240.245 0.071 831.00.900.647 0.004 0.45 0.00 180.0 4/21/2025 17:10 0.0001.3860.002 0.001 0.0000.572 0.058 0.000 0.3400.0370.000 0.000 0.2200.000 0.116 831.01.070.923 0.000 1.39 0.00 180.0 4/21/2025 17:10 0.0000.163-0.000 0.021 0.3220.915 0.043 0.105 0.3000.0000.000 0.000 0.3410.000 0.066 831.00.840.546 0.000 0.16 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 17:10 0.0000.1190.007 0.006 0.0000.955 0.023 0.338 0.0000.0000.000 0.000 0.1290.055 0.171 831.00.980.763 0.000 0.12 0.00 180.0 4/21/2025 17:10 0.0000.000-0.000 0.030 0.0001.000 0.023 0.220 0.5350.0010.034 0.000 0.4420.000 0.085 831.01.090.719 0.000 0.00 0.00 180.0 4/21/2025 17:10 0.0000.0100.007 0.021 0.0000.576 0.000 0.289 0.0000.0000.116 0.000 0.2660.000 0.077 831.00.580.235 0.000 0.01 0.00 180.0 GAS Performance Test Report Test Type: Annual Test Date: 4/25/2025 Waukesha 9394 GSI Rich Burn (4 Cycle) 303 W. 3rd St Elk City , OK 73644(580) 225-0403 Test Started:Test Completed:07:12 AM 10:40 AM Source: Unit Number: 1349 Serial Number: 1651133 Engine Hours:12554 Permit #: #DAQE-AN161680001-23 Location: Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, Inc. Residue Booster Station 40 CFR Part 60 Subpart JJJJ CO NOx NMNEHC 3.168 9.188 0.764 2.000 0.300 1.000 0.150 0.700 0.030 0.012 0.057 0.005 Pass Pass Pass Pass Pass Pass Federal State Federal State Federal State Results ppmvd Results g/hp-hr Permit g/hp-hr PASS ALL Index Tables Figures Appendices Table 5.1 (Run Summaries)................................................................ Table 6.1 (Volumetric Flow Rate Data)............................................... Table 6.2 (Stack Gas Measurements)................................................. Table 8.1 (Oxygen Calibration)........................................................... Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... Annex Table 1.2.2 (Measurement System Capabilities)..................... Annex Table 1.3.1 (Test Specific Target Analytes)............................. Annex Table 4.1 (Measure System Capabilities)................................ Figure 6.1 (Location of Traverse Points per Method 1)....................... Annex Figure 1.4.1 (Sampling Train).................................................. Annex Figure 1.4.2 (Sampling Points)................................................. Annex Figure 1.4.3 (Sampling Port Locations).................................... Certified Calibration Bottle Certificates................................................ Tri Probe Certification via GD-031...................................................... GAS ALT 141_FTIR EPA.................................................................... Tester Qualifications (resume)............................................................ Raw Data............................................................................................ 27 Key Personnel.............................................................................1.0 3 Sampling System........................................................................2.0 3 Methods Used.............................................................................3.0 3 Test Summaries..........................................................................4.0 5 Run Summaries..........................................................................5.0 6 6 Volumetric Flow Rate Data.........................................................6.0 7 7 7 7 Calculations................................................................................7.0 8 9 12 12 13 15 13 14 14 20 25 28 29 Oxygen Calibration.....................................................................9 Engine Parameter Data Sheet....................................................10 QA/QC Results............................................................................11 Signature Page...........................................................................12.0 Appendices.................................................................................13.0 Bottle Certs.................................................................................2014.0 Tri Probe Certification via GD-031..............................................2515.0 GAS ALT 141_FTIR EPA............................................................16.0 Tester Qualifications (resume)....................................................2817.0 D6348 Annexes..........................................................................1211.0 18 19 26 8.0 9.0 10.0 Raw Data....................................................................................2918.0 1.0 Key Personnel GAS Crusoe Energy Systems, Inc. 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A EPA Method 2 & 2C EPA Method 3A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. ASTM D6348-03 JD Herbert 3 Cooper Green GAS 4.0 Test Summary T e s t S u m m a r y Site Verification Photos GAS Unit 1349 with a serial number of 1651133 which is a Waukesha 9394 GSI engine located at Residue Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/25/2025 by Cooper Green with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2233 BHP and 1200 RPM which is 89.33% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1349 is authorized to operate under permit #DAQE-AN161680001-23. 4 4.0 Test Summary Engine/Compressor Specs Residue Booster StationLocation 1349Unit ID Make Waukesha Site Elevation ft.5455 Model 9394 GSI Atmospheric Pressure psi.11.96 Serial Number 1651133 Stack Diameter in.20 mfg. rated hp 2500 Yes 1200 Date of Manufacture Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1 Test Horsepower 2200 2225 2275 2233 1200 1200 1199 1200 Percent Load % Intake Manifold Pressure (hg) 88.00%89.00%91.00%89.33% 105.55 106.77 109.21 107.18 Intake Manifold Temperature (F)115.90 118.60 118.00 117.50 Ambient Conditions Ambient Temperature Dry (F)41.00 48.00 53.00 47.33 Exhaust Flow Data Q Stack (dscfh) Q Stack (dscm/hr) 256176.05 255737.50 255472.96 255795.51 7254.03 7241.61 7234.12 7243.25 Moisture Fraction Bws Fuel Consumption (Btu/h[-hr) 0.18 0.17 0.18 0.18 0 0 0 0 Fuel Flow (dscfh) Fuel (btu/scf)1020 1020 1020 1020 O2 F factor 8710.0 8710 8710 8710 Results Method 3A Corrected O2% Dry Moisture %17.52%17.47%17.59%17.53% T e s t S u m m a r y mfg. rated rpm Test RPM 0.00%0.00%0.00%0.00% Permitted Standards Results 5 Catalyst Run 1 Run 2 Run 3 3 Run Average Pass Permits 07:12 AM 08:22 AM 09:29 AM 4/25/2025 State NOx (mol wt) 46.01 0.684 0.613 0.593 0.630NMNEHC (ppmvw) 0.829 0.743 0.720 0.764NMNEHC (ppmvd) NMNEHC (mol wt) 44.10 234.112 209.676 203.134 215.641 FailNMNEHC (ppbvd) @15% O2 0.005 0.004 0.004 0.0050.700 0.030 PassNMNEHC (g/hp-hr) 0.234 0.210 0.203 0.216 FailNMNEHC (ppmvd) @15% O2 0.0200.008CO (g/hp-hr)0.008 0.0122.000 0.300 Pass CO (ppmvw)1.689 1.644 4.502 2.612 CO (ppmvd)2.048 1.992 5.463 3.168 CO (mol wt) 28.01 CO (ppmvd) @15% O2 0.578 0.562 1.542 0.894 Fail CO (ppbvd) @15% O2 578.092 562.329 1542.176 894.199 Fail NOx (g/hp-hr)0.056 0.056 0.059 0.0571.000 0.150 Pass NOx (ppmvw)7.305 7.383 8.045 7.577 NOx (ppmvd)8.857 8.945 9.762 9.188 NOx (ppbvd) @15% O2 2500.275 2525.178 2755.672 2593.709 Fail NOx (ppmvd) @15% O2 2.500 2.525 2.756 2.594 Fail GAS GAS 5.0 Run Summaries Summary Source Run 1 R u n Table 5.1 Run Summaries S u m m a r i e s 6 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture % 1.69 0.30 7.16 0.15 7.31 0.00% 0.00% 0.00% 17.52% 6.40 0.20 0.00%17.50% 29.36 0.00 0.00%15.85% 7.92 0.10 0.00%17.55% 0.00 0.00 0.00 0.00%0.04% Avg. Wet NO Summary Source Run 2 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 0.00 0.00 0.00 0.00 0.00%0.04% 1.73 7.22 0.06 7.28 0.00%17.45% 54.50 29.30 0.53 29.83 0.00%15.71% 1.56 7.41 0.08 7.49 0.00%17.49% 0.00 0.00 0.00 0.00 0.00%0.04% Avg. Wet 1.64 7.31 0.07 7.38 0.61 0.00%17.47% NO2NO 0.44 0.64 26.86 0.59 0.49 Summary Source Run 3 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 2.37 7.52 0.14 7.65 0.00%17.59% 52.92 60.05 1.37 61.41 0.00%16.08% 6.64 8.20 0.24 8.44 0.00%17.60% 0.00 0.00 0.00 0.00 0.00%0.04% 0.00 0.00 0.00 0.00 0.49 0.00%0.04% Avg. Wet 4.50 7.86 0.19 8.04 0.59 0.00%17.59% NO2NO 0.30 0.61 26.12 0.57 NMNEHC 0.54 NO2 0.000.16 0.62 26.27 0.75 0.44 0.68 0.30 6.59 29.36 8.02 1.35 2.03 0.00 54.82 6.0 Volumetric Flow Rate Data Volumetric Flow Rate Data .99 Table 6.1. Data used for volumetric flow rate (Method 2) Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet Run 1 Average Pitot Tube Coefficient Cp(std)= H2O CO2 O2 CO Molecular Weight Stack Gas dry basis (Md) Molecular Weight Stack Gas wet basis (Ms) Stack Static Pressure (Pg) Stack Static Pressure (Pg) Atmospheric Pressure at Location (Pbar) Atmospheric Pressure at Location (Pbar) Absolute Stack Pressure (Ps) Stack Temperature Stack Temperature Stack Temperature Stack Gas Velocity Stack Flow Rate Q Stack Gas Wet Volmetric Flow Rate Stack Gas Dry Volumetric Flow Rate Sample after Back Purge: Within 5% of Last Δpstd reading: Stack Diameter (inches) Inches upstream from disturbance Inches downstream from disturbance scf/hr 1.05 Yes 20.00 5.00 33.00 scf/hr cfs ft/sec Deg R Deg F Deg C "Hg "Hg MBAR "Hg "H20 g/g mole g/g mole %d %d %d %17.52 30.00 0.88 Inches 3.34 10 16.66 Vo l u m e t r i c F l o w Ra tes Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 Figure 6.1 16 Traverse Points Were Used Emissions Sampling Points - 3 point long line sampling probe First Sampling Point Taken @ 16.7% of Stack Diameter Second Sampling Point Taken @ 50% of Stack Diameter Third Sampling Point Taken @ 83.3% of Stack Diameter 12.51 0.00 0.00 1013.89 0.07 29.95 30.02 891.25 1350.92 477.36 27.90 100.83 220.01 310599.25 256176.05 Run 2 17.47 30.00 0.93 12.52 0.00 0.00 1013.89 0.07 29.95 30.02 894.25 1353.92 479.03 27.90 103.63 219.98 309868.42 255737.50 Run 3 17.59 29.99 0.96 12.44 0.00 0.00 1012.87 0.07 29.92 29.99 892.31 1351.98 477.95 27.88 105.41 219.98 310002.38 255472.96 17.53 30.00 0.92 12.49 0.00 0.00 1013.55 0.07 29.94 30.01 892.60 1352.27 478.11 27.90 103.30 219.98 310156.68 255795.5 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets. * Cyclonic Flow Check (Pass/Fail): PASS Δpstd (in) H2O 0.86 Exhaust Temp F 891.00 Pitot Tube Sampling Points (Velocity) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Δpstd Average= Run 1 Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate 0.82 0.85 0.97 891.00 891.00 892.00 0.89 0.95 0.84 891.00 891.00 891.00 0.92 0.90 0.89 892.00 891.00 891.00 0.91 891.00 0.87 0.86 0.79 892.00 891.00 891.00 0.80 0.92 0.88 891.00 892.00 891.25 Δpstd = Velocity head measured by the standard pitot tube, (in.) H2O.Run 3 Δpstd (in) H2O 0.95 Exhaust Temp F 892.00 0.95 0.93 1.04 892.00 893.00 892.00 0.99 0.92 1.00 892.00 892.00 893.00 1.02 1.00 0.94 893.00 892.00 892.00 1.01 892.00 0.95 0.83 0.87 893.00 892.00 892.00 0.90 1.05 892.00 893.00 892.310.96 Run 2 Δpstd (in) H2O 0.80 Exhaust Temp F 894.00 0.86 0.94 0.99 894.00 894.00 895.00 0.90 0.97 0.92 894.00 894.00 894.00 0.92 0.95 0.96 895.00 894.00 894.00 0.93 894.00 0.98 0.85 0.92 895.00 895.00 894.00 0.99 0.96 894.00 894.00 0.93 894.25 Pass Strat Check 10.365Check 1 10.326Check 2 10.369Check 3 CO2Gas Used Pass/Fail 7 GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate *Note- Use of this method negates the need for any fuel related numbers for emissions calculations Nomenclature Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293°K (528 °R). Vs = Average stack gas velocity, m/sec (ft./sec). *(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1 Md = .44(12.506)+ .32(0)+ .28(87.494+0) = 30 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO) 12.5 Molecular Weight of Stack Gas. Equation 2-6 Ms = 30(1 -.17522)+ 18.0(.17522) = 27.9 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws) 12.6 Average Stack Gas Velocity. Equation 2-7 Vs = 85.49*.99*√.88*√(1350.92/(30.02*27.9)) = 100.83 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms)) 12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8 Qsd = 3600(1-.17522)100.83*2.182((528*30.02)/ (1350.92*29.92)) = 256176.05 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd)) *Standard conversion from feet to meters Q = 256176.049/35.315 = 7254.029 DSCM/HRQ = Qsd/35.315 Emission Rates (Examples use CO Run 1) Nomenclature CO corrected @ 15% O2 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ER = Emission rate of (CO) in g/HP-hr. F(d )= Volumes of combustion components per unit of heat content, scm/J (scf/million Btu). Q = Stack gas volumetric flow rate, in standard cubic meters per hour, dry basis LB/HR.= Emission rate of (CO) in LB/HR. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) O2 = Concentration of oxygen on a dry basis, percent. ppm= Parts Per Million (CO) ppm@15% O2= PPM corrected to 15% O2 Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (DSCF/HR.). Run Time = Run Time in Minutes TPY= Tons per Year Mol wt.= Mol Weight of CO (28.01) Vs = Average stack gas velocity, m/sec (ft./sec). ppm @ 15% O2 = 2.048*(20.9-15)/(20.9-0%)) = .578 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2)) G/HP HR from 40 CFR Part 60 Subpart JJJJ (2.048*(1.164*10^-3)*7254.029*(Run Time/60))/2200 = .008 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR LB/HR from Grams LB/HR = .008*1/453.6*2200 = .038 LB/HRlb/hr = ER*1/453.6*BHP-HR TPY TPY = .038*4.38 = .166 TPYTPY = LB/HR. *4.38 Horsepower HP Provided On Site Wet to Dry PPM 2.05 = 1.689*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry 8 Cp(std) = Standard pitot tube coefficient; use 0.99 GAS 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span. 8.0 Oxygen Calibration 8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases. (1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration EPA Method 3A QA Worksheet (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Certified Gas Concentraion Low-Level (%) 0.00% Certified Gas Concentraion Mid-Level (%) Certified Gas Concentraion High-Level (%) (DIRECT) Analyzer Calibration Error (≤ 2%) Certified Concentration Value (%) Direct Calibration Response (%) Absolute Difference (%) Analyzer Calibration Error (%)Analyzer Direct Calibration Response Certified bottle value % 0.00% 0.00% 0.00% Zero Gas % Mid-Level Gas % High-Level Gas % Bias Pre Initial Value Bias Post Inital Values System Calibrations Response Pre (%) 0.00% System Bias (% of Span) Pre System Calibration Response Post (%) System Bias (% of Span) Post Drift (% of Span) 0.00%0.00%0.00%0.00% (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Avg. Gas Concentration (Run 1) Avg. Gas Concentration (Run 2) Avg. Gas Concentration (Run 3) Effluent Gas (Cgas) Run 1 Effluent Gas (Cgas) Run 2 Effluent Gas (Cgas) Run 3 Linearity Check 0.00%0.00%0.00% Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Upscale Gas Analyzer Calibration Response (%) Zero Gas Upscale Gas EPA Method 3A QA Worksheet Zero Gas Mid-Level Gas High-Level Gas 100% Nitrogen O2 QA/QC Zero Gas %0.00% Mid-Level Gas % High-Level Gas % System Calibration Response Pre (%) System Calibration Response Post (%) Zero Gas % Upscale Cal Zero Gas % Upscale Cal Upscale Used Upscale Used 10.61% 20.90% 10.62% 10.60% 10.73% 10.73% 10.60%10.62% 10.61% 20.90% 10.73% 21.04% 10.73% 21.04% 10.73%21.04% 0.00% 10.73% 21.04% 0.12% 0.14% 0.56% 0.68% 10.73% Span Zero Offset 0.00% 21.04 0.00% 10.61%0.05%0.08%0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 9 GAS 1081.0 1083.0 1081.3 1054.0 1058.0 1055.3 6.0 6.0 6.0 9.0 Engine Parameter Data Sheet Company Site Elevation (ft) Facility Unit ID Date Make Crusoe Energy Systems, Inc. Residue Booster Station 4/25/2025 5455 1349 Waukesha Model Serial Number 9394 GSI 1651133 Technician Cooper Green Run Start Times 07:12 AM 08:22 AM 09:29 AM 10:40 AM Run 1 Run 2 Run 3 Completed Engine Parameter Data Run 1 Engine Speed (RPM)1200.0 1200.0 1199.0 1199.7 Engine Hours 12551 12552 12553 12554 Intake Manifold Pressure (psi)63.8 64.4 65.6 64.6 Intake Manifold Temp °F 115.9 118.6 118.0 117.5 Engine Load (BHP)2200.0 2225.0 2275.0 2233.3 Ambient Temp °F 41.0 48.0 53.0 47.3 Humidity %70.0 58.0 50.0 59.3 Dew Point °F 32.0 34.0 34.0 33.3 Waukesha Yes 2 2 2 2# of Catalyst Installed Catalyst (Yes or No) AFR Setting (Target Left Bank) AFR Setting (Target Right Bank) AFR Manufacturer/Type Waukesha Waukesha Waukesha 10 Run 3 AverageRun 2 Discharge Pressure (psi) Suction Pressure (psi) 1080.0 1054.0 6.0Catalyst Pressure Drop H2O Catalyst Outlet Temp °F Catalyst Inlet Temp °F GAS 10.0 QA/QC Results Average:Carbon monoxide CO Gas, Inc. 0.00 R e s u l t s Average:Nitrogen monoxide NO 0.00 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.00 Average:VOC 0.11 Average:Oxygen 0.00 Pre-test Baseline Results Time: Q A / Q C Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 99.04 Tolerance 2.00% Difference between measured and expected 0.96% CTS Direct to Analyzer Time: Average:Carbon monoxide CO 0.28 Average:Nitrogen monoxide NO 0.10 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.10 Average:VOC 0.59 Average:Oxygen 0.00 Pre-test System Zero Time: Mechanical Response Time 45 seconds Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.54 Tolerance 5.00% Difference between measured and expected 1.46% Pre-test System CTS & Mechanical Response Time 45 secondsEquilibration Response Time Value:Spike Reported 253.06 Value:Spike Expected 253.10 System (Equilibration) Response Time Target (Spike) 59 secondsSystem Zero Response Time 59 secondsSystem Response Time System (Zero) Response Time 11 11.0 D6348 Annexes 1-8 D6348 Annexes 1. Test Plan Requirements Annex 1.2 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration NO2 Ethylene SF6 O2 (%) CC524639 12/30/2027 103.00 10.73% CC252676 10/17/2032 100.00 CC433538 8/5/2032 21.04% Cylinder # SG9132842BAL Expiration: 8-20-2032 Propane CO NO SF6 Bottle Value 253.10 497.30 252.90 9.95 Analyzer System Response 253.06 488.07 248.21 9.82 Percent Difference 0.01%1.86%1.85%1.31% Annex Table 1.2.2 Measurement System Capabilities SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 99.042 4.952 Spike Direct Propane 254.668 Mechanical Response Time SF6 9.890 CO 492.978 NO 249.932 Ethylene 98.541 22 seconds Analyzer Response Propane 253.064 SF6 9.824 CO 488.073 NO 248.214 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 253.431 CO 481.637 NO 246.675 33 seconds 59 seconds 9.76% 9.88% 9.89% 97.03% 99.25% 97.00% 9.808 12 GAS Annex 1.3 Compounds Infrared Analysis Region (cm-1) Expected Concentration Range Measurement System Achievable Minimum Detectable Concentrations Required Measurement System Accuracy and Precision for Test Application CO 2000-2200 0-1200 ppm NO 1875-2138 NO2 2700-2950 VOC 2600-3200 910-1150 2550-2950 CH2O 2550-2850 Interfering Compounds * CO is analyzed in a separate analysis region than CO2 and H2O CO2 Water Vapor 926-1150 3200-3401 Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives 0.16267 ppm 4 ppm 0-1000 ppm 0.4007 ppm 2 ppm 0-100 ppm 0.4899 ppm 2 ppm 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC 0-100 ppm 0.7878 ppm 1 ppm 0-10% 0-22% 0% 0.20% n/a n/a * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. Annex 1.4 Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 13 GAS Sampling Point Locations in Inches 16.7%3.340 50%10.000 83.3%16.660 Figure Annex 1.4.3 Sample Port Location Figure Annex 1.4.2 Sampling Points Interior Stack Diameter (inches): Inches Upstream: Inches Downstream: 20 5 33 14 Stack Gas Dry Volumetric Flow Rate (scf/hr): 255795.5 H2O%d @ Sampling Point:17.53 CO2%d @ Sampling Point:12.49 Pressure @ Sampling Point (Pg "H2O):0.92 Temperature @ Sampling Point (Deg F):892.6 GAS D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1) Target Analyte Results (ppm) CO 0.1627 NO 0.4007 NO2 0.4899 Ethylene 0.3782 Propane 0.4351 Hexane 0.2233 Acetaldehyde 0.8152 Formaldehyde 0.7878 D6348 Annex 3. FTIR Reference Spectra Calibration Transfer Standard Expected Measured Path Length Validated Ethylene 100 99.04 4.952 Passed D6348 Annex 4. Required Pre-Test Procedures Annex Table 1.2.2 Measurement System Capabilities 15 SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 99.042 4.952 Spike Direct Propane 254.668 Mechanical Response Time SF6 9.890 CO 492.978 NO 249.932 Ethylene 98.541 22 seconds Analyzer Response Propane 253.064 SF6 9.824 CO 488.073 NO 248.214 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 253.431 CO 481.637 NO 246.675 33 seconds 59 seconds 9.76% 9.88% 9.89% 97.03% 99.25% 97.00% 9.808 GAS D6348 Annex 5. Analyte Spiking Technique Propane Spike Direct SF6 CO NO 253.100 9.954 497.300 252.900 254.668 9.890 492.978 249.932 0.62% 0.64% 0.87% 1.17% +/- 2% +/- 2% +/- 2% +/- 2% Pass Pass Pass Pass Parameter Gas Concentration Measured % Difference Specification Validated 0.000 0.000 Spike Average 23.970 0.965 Dilution Factor 9.757% Expected 24.703 % Recovery 97.030% Specification 70-130% <10% Spike Run 1 via the System Source Output Propane SF6 D6348 Annex 6. Determination of System Performance Parameters Noise Equivalent Absorbance (NEA) RMS High RMS Mid RMS Low Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%) 0.000 Spike Average 0.977 Dilution Factor 9.879% Expected % Recovery Specification 70-130% <10% Spike Run 2 via the System Source Output Propane SF6 0.000 Spike Average 0.978 Dilution Factor 9.889% Expected % Recovery Specification 70-130% <10% Spike Run 3 via the System Source Output Propane SF6 0.000 24.281 25.032 97.000% 0.000076 0.000038 0.000197 0.000 24.819 25.006 99.250% Line Position Difference:Resolution Difference to Reference0.00%Pass Pass4.16% 16 GAS Resolution The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. Detector Linerarity The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. D6348 Annex 7. Preparation of Analytical Quantification Algorithm The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 Regression Slope:-7.34958771 Pass Line Position Difference:Resolution Difference to Reference 4.16% D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures CTS Bottle Concentration: CTS Sample Concentration Average: Difference between measured and expected: Tolerance: 100.00 99.63 0.38% 5.00% POST CTS System Check: Run 1 Points 1 & 2 on CO/NO/Propane Run 2 Points 1 & 2 on CO/NO/Propane Run 3 Points 1 & 2 on CO/NO/Propane Run Data Validation - Automated vs Manual Reading Validated Comments All within 20% All within 20% All within 20% Passed Passed Passed Demonstrates no interferences observed. Demonstrates no interferences observed. Demonstrates no interferences observed. 17 GAS 12.0 Signature Page Job/File Name: We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Crusoe Energy Systems, Inc.; Residue Booster Station; 1349; JJJJ 18 Company: Print Name: Signature: Title: Phone Number: Date: Company:G.A.S. Inc.Date: Print Name: Title: 4/25/2025 Emissions Specialist Company:G.A.S. Inc.Date: Print Name: Title: Signature: Phone Number: Travis Hartley Director of Stack Testing 580-225-0403 4/25/2025 Cooper Green GAS Appendices GAS GAS Spike (5 Gas) GAS 9% O2/NO2 GAS Ethylene Only GAS BIP GAS 21% O2 Tri Probe Certification ” ‡ ƒ – Ž ƒ ‹ • • • ƒ Ž › – ‹ … ƒ Ž ‡ ” ˜ ‹ … ‡ • ͵Ͳ͵͵”†–Ž‹–›ǡǡ͹͵͸ͶͶ ȋͷͺͲȌʹʹͷǦͲͶͲ͵ ƒšǣȋͷͺͲȌʹʹͷǦʹ͸ͳʹ &(57,),&$7(2)$1$/<6,6 *UDGHRI3URGXFW&(57,),('67$1'$5'352%( 3DUW1XPEHU65HIHUHQFH 1XPEHU  /DERUDWRU\*$6,1&6WDFN'LDPHWHU $QDO\VLV'DWH7DUJHW)ORZ 5DWH /PLQ /271XPEHU 61 $ $6 1XPEHURI 3RLQWV  3URGXFWSHUIRUPDQFHYHULILHGE\GLUHFWFRPSDULVRQWRFDOLEUDWLRQVWDQGDUGVWUDFHDEOHWR1,67  7KHSUREHOLVWHGRQWKLVIRUPPHHWVWKHPXOWLSRLQWWUDYHUVHUHTXLUHPHQWRI(3$0HWKRGH VHFWLRQDVVKRZQLQWKHDFFRPSDQ\LQJGDWD0HWKRGHVHFWLRQVWDWHVWKDWWKHPXOWLSRLQW WUDYHUVHUHTXLUHPHQWFDQEHVDWLVILHGE\VDPSOLQJYLD³DPXOWLKROHSUREHGHVLJQHGWRVDPSOHDW WKHSUHVFULEHGSRLQWVZLWKDIORZSHUFHQWRIPHDQIORZUDWH´ $1$/<7,&$/5(68/76 ZƵŶηdŽƚĂů&ůŽǁ ;>ͬŵͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϭͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϮͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϯͿ 0HDQ3UREH 3RUW6DPSOHG )ORZ /P  5XQ/30  䧮    䧮    䧮   5XQ/30  䧮    䧮    䧮    &DOLEUDWLRQFRQGXFWHGLQDFFRUGDQFHZLWK(PLVVLRQ0HDVXUHPHQW&HQWHU*XLGHOLQH'RFXPHQW±(0&*' 1RWHV BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB $SSURYHGIRU5HOHDVH'DWH 2/17/2022 Probe size: 20S Mr. Jordan Williamson CEO GAS Inc. 303 W. 3rd Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. March 15, 2021 Sincerely, Steffan M. Johnson, Group Leader Measurement Technology Group If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. cc: Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leather.james@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Heather Sessing, Oklahoma DEQ, (Heather.sessing@deq.ok.gov) Cooper Green GAS Type of Sources Tested: info@gasinc.us Stationary Internal Combustion Engines • 4 Stroke Rich Burn Engines • 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods: • EPA Method 1 & 1A – Sampling & Traverse Points • EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream • EPA Method 3A – Oxygen • EPA Method 7E – NOX • EPA Method 10 – Carbon Monoxide • EPA Method 25A – Volatile Organic Compounds • ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. • Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Types of Analyzers: • Gasmet DX4000 FTIR • Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory • Testo 350 • Flame Ionization Detector 580-225-0403 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 1 Minute Average Data Sheet Crusoe Energy Systems, Inc.Client: Residue Booster Station Unit Number:1349 Make:Waukesha Location:9394 GSIModel: 1651133Serial Number: RAW Result Data Stability 4/25/2025 05:46 0.2600.2320.000 0.006 0.0000.136 0.017 0.000 0.0000.1160.000 0.309 0.0700.321 0.023 845.00.320.000 0.003 0.49 0.00 180.0 Pre Test Baseline Direct 4/25/2025 05:53 0.0000.0000.000 0.000 0.2220.000 0.000 0.122 0.3300.1390.000 0.000 0.0000.010 0.000 845.00.250.372 0.000 0.00 0.00 180.0 4/25/2025 05:53 0.0000.0000.002 0.000 0.0740.000 0.004 0.082 0.1080.1120.281 0.000 0.0250.163 0.018 845.00.060.000 0.000 0.00 0.00 180.0 4/25/2025 05:54 0.0000.000-0.004 0.000 0.2820.000 0.001 0.102 0.0760.1600.396 0.000 0.0000.000 0.007 845.00.010.000 0.000 0.00 0.00 180.0 CTS Direct 4/25/2025 05:56 0.0000.3800.012 0.008 0.0000.000 0.000 0.000 0.3850.0000.000 98.756 0.0000.208 0.000 845.065.880.066 0.027 0.38 0.00 180.0 4/25/2025 05:56 0.0000.0000.009 0.014 0.0000.000 0.000 0.000 0.4140.0000.000 99.064 0.0000.079 0.005 845.066.060.000 0.025 0.00 0.00 180.0 4/25/2025 05:57 0.0000.2350.010 0.010 0.0000.000 0.000 0.000 0.5820.0000.000 99.306 0.0000.093 0.000 845.066.350.221 0.027 0.24 0.00 180.0 High O2 Direct 4/25/2025 06:01 0.0000.0000.003 0.000 0.0000.000 0.000 0.072 0.0300.0000.568 0.000 0.0000.000 0.000 845.00.060.083 0.000 0.00 20.87 180.0 4/25/2025 06:02 0.0000.0000.004 0.000 0.0350.000 0.000 0.133 0.0010.0000.587 0.000 0.0000.352 0.004 845.00.050.065 0.000 0.00 20.90 180.0 4/25/2025 06:02 0.0000.000-0.006 0.000 0.0000.000 0.000 0.072 0.0000.2830.678 0.000 0.0000.119 0.000 845.00.000.000 0.000 0.00 20.92 180.0 NO2/Mid O2 Direct 4/25/2025 06:05 103.5270.446-0.001 0.000 0.0000.000 0.931 0.000 0.4290.0000.431 0.000 0.0000.148 0.000 845.00.000.000 0.000 103.97 10.62 180.0 4/25/2025 06:05 103.7710.705-0.003 0.000 0.0340.000 0.959 0.000 0.8300.0030.526 0.000 0.0000.295 0.000 845.00.000.000 0.000 104.48 10.60 180.0 4/25/2025 06:05 103.4910.000-0.000 0.000 0.0000.000 0.952 0.000 0.5700.0570.174 0.000 0.0000.037 0.000 845.00.000.000 0.000 103.49 10.62 180.0 Spike Direct 4/25/2025 06:08 0.000249.620-0.004 4.960 5.766491.266 1.867 2.200 1.5680.3560.000 0.867 253.8270.440 0.885 845.0258.042.793 9.884 249.62 0.00 180.0 4/25/2025 06:08 0.000249.504-0.003 4.956 5.467492.701 1.809 2.326 1.1820.2630.000 0.927 254.9130.231 0.820 845.0259.042.803 9.889 249.50 0.00 180.0 4/25/2025 06:09 0.000250.673-0.003 4.949 5.323494.967 1.792 2.386 1.1760.1460.191 0.949 255.2640.007 0.801 845.0259.442.908 9.897 250.67 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline System 4/25/2025 06:11 0.0000.3050.008 0.021 0.0000.616 0.000 0.124 0.0000.0000.663 0.000 0.4730.000 0.053 845.00.850.414 0.003 0.31 0.00 180.0 4/25/2025 06:11 0.0000.0000.005 0.006 0.2760.138 0.004 0.192 0.1600.0000.420 0.000 0.1040.124 0.055 845.00.450.349 0.000 0.00 0.00 180.0 4/25/2025 06:11 0.0000.0000.003 0.001 0.1800.079 0.000 0.181 0.2200.0000.192 0.000 0.1520.435 0.035 845.00.460.351 0.000 0.00 0.00 180.0 CTS System with Response Time 4/25/2025 06:13 0.0000.0000.011 0.017 0.0000.000 0.000 0.000 0.3310.0000.000 98.469 0.0000.000 0.033 845.065.820.154 0.024 0.00 0.00 180.0 4/25/2025 06:13 0.0000.0000.014 0.023 0.0000.000 0.000 0.000 0.7920.0130.000 98.521 0.0000.048 0.023 845.065.730.000 0.022 0.00 0.00 180.0 4/25/2025 06:14 0.0000.0000.011 0.025 0.0000.000 0.000 0.000 0.5000.0010.000 98.633 0.0000.002 0.023 845.065.800.000 0.023 0.00 0.00 180.0 NO2/Mid O2 System with Response Time 4/25/2025 06:15 100.6992.387-0.000 0.000 0.4850.209 0.993 0.086 0.2340.0090.000 0.000 0.0000.000 0.011 845.00.020.000 0.000 103.09 10.62 180.0 4/25/2025 06:16 101.1302.7580.005 0.000 0.1060.286 0.991 0.023 0.0000.0000.000 0.000 0.0000.469 0.000 845.00.000.000 0.000 103.89 10.62 180.0 4/25/2025 06:16 101.5562.6810.002 0.000 0.3540.016 0.998 0.112 0.0910.0000.000 0.000 0.0580.508 0.011 845.00.080.000 0.000 104.24 10.63 180.0 Spike System with Response Time 4/25/2025 06:18 0.000249.603-0.000 4.932 4.428490.329 1.892 2.212 0.5480.1290.142 1.008 252.8740.298 0.945 845.0257.102.499 9.817 249.60 0.00 180.0 4/25/2025 06:18 0.000247.3680.002 4.928 4.711487.570 1.837 2.364 0.9450.0440.000 1.056 252.9650.501 0.965 845.0257.242.466 9.818 247.37 0.00 180.0 4/25/2025 06:19 0.000247.672-0.000 4.923 5.209486.320 1.802 2.291 0.8020.0440.035 0.965 253.3520.212 0.849 845.0257.562.804 9.837 247.67 0.00 180.0 Baseline System with Response Time 4/25/2025 06:21 0.0000.8030.001 0.013 0.0000.241 0.000 0.113 0.0000.0070.587 0.000 0.1720.344 0.030 845.00.360.195 0.002 0.80 0.00 180.0 4/25/2025 06:22 0.0000.0000.001 0.005 0.0000.141 0.022 0.082 0.0000.0000.659 0.000 0.3910.092 0.000 845.00.780.579 0.001 0.00 0.00 180.0 4/25/2025 06:22 0.0000.1010.002 0.009 0.0250.098 0.002 0.109 0.0740.0010.331 0.000 0.2590.449 0.002 845.00.470.309 0.000 0.10 0.00 180.0 Run 1 - A 30minute/60min 4/25/2025 07:13 1.3325.26816.493 10.447 51.1630.888 1.033 0.164 1.4250.0824.507 0.000 0.0140.993 0.122 833.00.560.453 0.000 6.60 0.00 180.0 4/25/2025 07:14 0.0006.88417.366 10.320 44.5870.974 1.456 0.000 0.9410.0752.122 0.000 0.0001.100 0.077 833.00.650.743 0.000 6.88 0.00 180.0 4/25/2025 07:15 0.5526.10517.899 10.232 42.8780.677 0.878 0.000 1.0710.0152.078 0.000 0.0000.814 0.050 833.00.530.648 0.000 6.66 0.00 180.0 4/25/2025 07:16 0.6296.88117.842 10.199 48.0850.812 1.371 0.000 1.2620.0052.504 0.000 0.0000.999 0.078 833.00.600.670 0.000 7.51 0.00 179.0 4/25/2025 07:17 0.0007.24717.824 10.301 56.0841.471 1.529 0.000 1.1210.0695.397 0.000 0.0001.019 0.078 833.00.670.775 0.000 7.25 0.00 180.0 4/25/2025 07:18 0.0006.30717.933 10.273 60.3841.360 1.550 0.000 1.3560.1075.596 0.000 0.0001.096 0.058 833.00.530.625 0.000 6.31 0.00 180.0 4/25/2025 07:19 0.7326.62317.951 10.264 59.1541.148 1.564 0.048 1.8180.0325.338 0.000 0.0001.074 0.057 833.00.750.952 0.000 7.35 0.00 180.0 4/25/2025 07:20 0.0008.18817.812 10.335 69.6312.391 2.074 0.112 2.2340.0045.385 0.000 0.0000.908 0.046 833.00.821.091 0.000 8.19 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/25/2025 07:21 0.5594.43717.647 10.409 66.8651.944 1.692 0.397 1.8230.0576.308 0.000 0.0001.122 0.125 833.00.770.785 0.000 5.00 0.00 180.0 4/25/2025 07:22 0.0004.43617.572 10.401 59.4031.062 0.837 0.393 1.7780.0426.472 0.000 0.0000.851 0.006 833.00.380.557 0.000 4.44 0.00 180.0 4/25/2025 07:23 0.0904.15117.439 10.378 56.1911.305 1.306 0.431 1.7310.0135.911 0.000 0.0000.805 0.096 833.00.710.778 0.000 4.24 0.00 180.0 4/25/2025 07:24 0.0006.61717.382 10.349 48.6041.273 1.514 0.286 1.2040.0403.354 0.000 0.0000.899 0.041 833.00.670.880 0.000 6.62 0.00 180.0 4/25/2025 07:25 0.0006.19317.387 10.361 56.9171.049 1.775 0.242 1.7020.0913.758 0.000 0.0000.950 0.030 833.00.470.616 0.000 6.19 0.00 180.0 4/25/2025 07:26 0.0005.97917.397 10.320 54.8611.044 1.315 0.253 1.6770.0043.886 0.000 0.0000.758 0.021 833.00.620.873 0.000 5.98 0.00 180.0 4/25/2025 07:27 0.0006.68917.405 10.350 41.3051.503 1.720 0.162 1.1650.0983.337 0.000 0.0000.841 0.027 833.00.510.676 0.000 6.69 0.00 180.0 4/25/2025 07:28 0.3515.11017.448 10.368 45.3161.426 0.565 0.389 1.2540.0755.076 0.000 0.0000.982 0.067 833.00.650.775 0.000 5.46 0.00 180.0 4/25/2025 07:29 0.0008.56217.428 10.365 47.5081.631 1.709 0.304 1.3050.0063.578 0.000 0.0000.807 0.070 833.00.821.022 0.000 8.56 0.00 180.0 4/25/2025 07:30 0.0005.91717.396 10.326 54.7691.474 1.581 0.293 1.5260.0013.525 0.000 0.0000.910 0.036 833.00.450.575 0.000 5.92 0.00 179.0 4/25/2025 07:31 0.0007.73717.371 10.369 56.9501.643 1.740 0.250 1.9120.0373.102 0.000 0.0000.697 0.029 833.00.550.738 0.000 7.74 0.00 180.0 4/25/2025 07:32 0.0005.65817.411 10.347 58.8941.492 1.968 0.308 1.6030.0123.463 0.000 0.0000.864 0.080 833.00.800.965 0.000 5.66 0.00 180.0 4/25/2025 07:33 0.0005.72317.380 10.339 62.2421.245 1.877 0.209 1.7220.0043.877 0.000 0.0000.916 0.051 833.00.670.853 0.000 5.72 0.00 179.0 4/25/2025 07:34 0.7124.07017.413 10.420 47.5350.889 0.904 0.302 1.2310.0864.520 0.000 0.0000.751 0.084 833.00.720.833 0.000 4.78 0.00 180.0 4/25/2025 07:35 0.2505.50817.454 10.363 57.9780.887 0.706 0.291 1.7070.0275.240 0.000 0.0000.893 0.070 833.00.550.621 0.000 5.76 0.00 180.0 4/25/2025 07:36 0.0007.95817.479 10.289 52.9200.907 1.706 0.147 1.4330.0003.950 0.000 0.0000.529 0.043 833.00.771.026 0.000 7.96 0.00 180.0 4/25/2025 07:37 0.0006.45317.411 10.339 51.9641.486 1.277 0.132 1.5060.0293.438 0.000 0.0000.806 0.021 833.00.500.691 0.000 6.45 0.00 179.0 4/25/2025 07:38 0.3104.71717.447 10.390 46.2921.354 1.210 0.316 1.0410.0454.689 0.000 0.0001.009 0.081 833.00.720.844 0.000 5.03 0.00 180.0 4/25/2025 07:39 0.0096.57917.453 10.352 55.4012.154 1.317 0.235 1.7060.0023.717 0.000 0.0001.019 0.045 833.00.690.894 0.000 6.59 0.00 180.0 4/25/2025 07:40 0.0729.58717.469 10.335 54.2522.399 2.291 0.251 1.7240.0163.677 0.000 0.0000.787 0.035 833.00.670.906 0.000 9.66 0.00 180.0 4/25/2025 07:41 0.2528.73217.453 10.310 26.2751.312 1.625 0.222 0.7240.0302.771 0.000 0.0000.770 0.000 833.00.380.571 0.000 8.98 0.00 180.0 4/25/2025 07:42 0.0007.60317.520 10.274 26.3991.273 0.846 0.141 0.6320.0022.981 0.000 0.0000.731 0.016 833.00.340.466 0.000 7.60 0.00 180.0 0.1956.39717.496 10.338 52.0271.349 1.431 0.209 1.4440.0374.119 0.000 0.0000.890 0.055 833.000.6170.763 0.000 6.593 0.000 179.9Avg. Spike 1 4/25/2025 07:46 0.00029.35815.850 9.745 62.47454.820 1.617 0.480 0.8340.0173.782 1.208 23.9700.802 0.337 833.026.271.228 0.965 29.36 0.00 180.0 Run 1 - B 30minute/60min 4/25/2025 07:48 0.0008.23217.516 10.298 54.3901.706 1.586 0.214 0.9840.0023.603 0.000 0.0001.100 0.091 833.00.760.869 0.000 8.23 0.00 180.0 4/25/2025 07:49 0.0007.75217.470 10.319 56.0271.223 1.458 0.128 1.0020.0003.640 0.000 0.0000.915 0.072 833.00.780.950 0.000 7.75 0.00 180.0 4/25/2025 07:50 0.0008.05117.493 10.309 61.4531.778 1.877 0.239 1.2050.0393.747 0.000 0.0001.049 0.069 833.00.740.896 0.000 8.05 0.00 180.0 4/25/2025 07:52 0.0007.91217.516 10.298 62.1621.945 1.902 0.205 1.5890.0013.700 0.000 0.0000.787 0.028 833.00.600.812 0.000 7.91 0.00 180.0 4/25/2025 07:53 0.4517.33417.526 10.256 58.9402.840 1.816 0.265 1.2160.0033.556 0.000 0.0000.810 0.057 833.00.620.754 0.000 7.78 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/25/2025 07:54 0.3627.92217.507 10.297 43.2281.433 1.586 0.237 0.6210.0333.052 0.000 0.0000.889 0.073 833.00.660.780 0.000 8.28 0.00 180.0 4/25/2025 07:55 0.0008.04817.519 10.319 57.0331.614 1.682 0.209 0.9820.0003.292 0.000 0.0000.689 0.081 833.00.730.846 0.000 8.05 0.00 180.0 4/25/2025 07:56 0.0008.52817.539 10.274 51.0261.669 1.370 0.090 0.6970.0013.279 0.000 0.0000.865 0.045 833.00.580.736 0.000 8.53 0.00 180.0 4/25/2025 07:57 0.0008.14217.532 10.260 57.2711.866 1.477 0.157 0.8940.0053.393 0.000 0.0000.879 0.094 833.00.700.768 0.000 8.14 0.00 180.0 4/25/2025 07:58 0.0007.73317.528 10.293 67.1102.093 1.875 0.119 1.3910.0003.651 0.000 0.0001.118 0.073 833.00.680.803 0.000 7.73 0.00 180.0 4/25/2025 07:59 0.3838.28717.518 10.297 67.5731.781 2.045 0.188 1.4740.0113.631 0.000 0.0000.960 0.094 833.00.790.909 0.000 8.67 0.00 180.0 4/25/2025 08:00 0.0007.68817.515 10.279 56.2571.469 1.439 0.226 0.9150.0003.609 0.000 0.0000.981 0.077 833.00.710.836 0.000 7.69 0.00 180.0 4/25/2025 08:01 0.0007.88817.497 10.276 64.8871.676 1.714 0.213 1.2690.0003.805 0.000 0.0000.866 0.090 833.00.820.963 0.000 7.89 0.00 180.0 4/25/2025 08:02 0.0007.92317.521 10.312 45.9781.912 1.562 0.189 0.5770.0323.003 0.000 0.0000.740 0.105 833.00.760.817 0.000 7.92 0.00 180.0 4/25/2025 08:03 0.0247.85717.548 10.276 57.7063.305 1.803 0.271 1.2880.0053.284 0.000 0.0000.541 0.106 833.00.860.971 0.000 7.88 0.00 180.0 4/25/2025 08:04 0.0007.75317.551 10.262 49.2882.511 1.408 0.311 0.6090.0013.488 0.000 0.0000.788 0.090 833.00.740.845 0.000 7.75 0.00 179.0 4/25/2025 08:05 0.0008.55917.576 10.335 63.6022.015 2.071 0.285 1.3780.0003.494 0.000 0.0000.806 0.097 833.00.921.089 0.000 8.56 0.00 180.0 4/25/2025 08:06 0.9638.10117.609 10.311 46.1561.660 1.448 0.272 0.4770.0093.267 0.000 0.0000.687 0.121 833.00.730.732 0.000 9.06 0.00 180.0 4/25/2025 08:07 0.0007.62317.615 10.322 55.0521.563 1.481 0.207 0.8570.0023.467 0.000 0.0000.672 0.105 833.00.710.752 0.000 7.62 0.00 180.0 4/25/2025 08:08 0.0008.09017.646 10.312 52.5281.503 1.300 0.175 0.7730.0143.621 0.000 0.0000.791 0.060 833.00.710.890 0.000 8.09 0.00 180.0 4/25/2025 08:09 0.0007.86817.585 10.266 48.9091.495 1.285 0.163 0.5670.0033.293 0.000 0.0001.032 0.083 833.00.650.723 0.000 7.87 0.00 180.0 4/25/2025 08:10 0.0527.77717.582 10.280 57.9291.881 1.642 0.164 0.9720.0023.119 0.000 0.0000.828 0.113 833.00.770.823 0.000 7.83 0.00 180.0 4/25/2025 08:11 0.3037.91517.591 10.267 54.8661.965 1.226 0.159 0.9540.0013.317 0.000 0.0000.525 0.102 833.00.820.931 0.000 8.22 0.00 180.0 4/25/2025 08:12 0.1557.71317.599 10.239 68.6713.024 1.788 0.227 1.6270.0003.644 0.000 0.0000.871 0.124 833.00.710.687 0.000 7.87 0.00 180.0 4/25/2025 08:13 0.0007.45717.587 10.266 64.9092.044 1.865 0.244 1.3740.0003.431 0.000 0.0000.841 0.117 833.00.820.873 0.000 7.46 0.00 180.0 4/25/2025 08:14 0.1687.42317.605 10.293 70.5102.605 1.947 0.238 1.7080.0063.518 0.000 0.0001.001 0.093 833.00.770.880 0.000 7.59 0.00 180.0 4/25/2025 08:15 0.0008.01517.574 10.320 56.9281.646 1.710 0.213 1.0530.0003.563 0.000 0.0000.725 0.125 833.00.880.940 0.000 8.02 0.00 180.0 4/25/2025 08:16 0.0007.92517.549 10.290 69.0923.078 1.838 0.232 1.5040.0003.706 0.000 0.0000.928 0.110 833.00.890.999 0.000 7.92 0.00 180.0 4/25/2025 08:17 0.0007.87617.536 10.287 67.6533.334 2.138 0.385 1.5490.0003.757 0.000 0.0000.788 0.067 833.00.780.967 0.000 7.88 0.00 180.0 4/25/2025 08:18 0.1408.13817.476 10.319 62.2922.237 2.013 0.342 1.2750.0413.563 0.000 0.0000.557 0.095 833.00.850.984 0.000 8.28 0.00 180.0 0.1007.91817.548 10.291 58.3142.029 1.678 0.219 1.0930.0073.483 0.000 0.0000.834 0.089 833.000.7510.861 0.000 8.017 0.000 180.0Avg. 0.1487.15717.522 10.314 55.1711.689 1.555 0.214 1.2690.0223.801 0.000 0.0000.862 0.072 833.000.6840.812 0.000 7.305 0.000 179.9Run 1 Avg: Baseline 1 4/25/2025 08:20 0.0000.0000.044 0.041 0.0000.000 0.000 0.143 0.0000.0120.663 0.000 0.2240.170 0.000 833.00.440.318 0.000 0.00 0.00 180.0 Run 2 - A 30minute/60min 4/25/2025 08:22 0.1007.45217.270 10.236 54.0832.448 1.599 0.311 0.9510.0172.825 0.000 0.0000.878 0.112 833.00.770.812 0.000 7.55 0.00 180.0 4/25/2025 08:23 0.3307.35717.485 10.292 58.4352.279 1.950 0.211 1.1570.0033.485 0.000 0.0000.896 0.100 833.00.680.719 0.000 7.69 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/25/2025 08:24 0.0007.68917.460 10.304 58.7331.540 1.516 0.190 0.9630.0003.699 0.000 0.0000.677 0.088 833.00.790.918 0.000 7.69 0.00 180.0 4/25/2025 08:25 0.0007.63917.432 10.371 59.5781.063 1.872 0.165 0.9100.0013.406 0.000 0.0000.742 0.114 833.00.931.049 0.000 7.64 0.00 180.0 4/25/2025 08:26 0.1908.02217.439 10.345 48.9091.637 1.649 0.143 1.1760.0003.203 0.000 0.0000.801 0.082 833.00.841.018 0.000 8.21 0.00 179.0 4/25/2025 08:27 0.0505.32917.500 10.319 46.1860.929 0.294 0.244 0.7010.0006.240 0.000 0.0000.625 0.122 833.00.880.954 0.000 5.38 0.00 180.0 4/25/2025 08:28 0.0007.88617.397 10.312 56.8041.613 1.645 0.125 1.0590.0003.634 0.000 0.0000.928 0.086 833.00.820.972 0.000 7.89 0.00 179.0 4/25/2025 08:29 0.0006.37517.412 10.395 50.7251.575 1.204 0.303 0.5530.0254.714 0.000 0.0000.945 0.138 833.00.750.705 0.000 6.38 0.00 180.0 4/25/2025 08:30 0.6906.22117.408 10.398 53.5801.792 0.998 0.317 1.0170.0204.421 0.000 0.0000.920 0.082 833.00.520.537 0.000 6.91 0.00 180.0 4/25/2025 08:31 0.0008.31117.460 10.298 52.4281.811 1.721 0.090 0.8990.0073.475 0.000 0.0000.839 0.037 833.00.430.541 0.000 8.31 0.00 180.0 4/25/2025 08:33 0.0007.24317.482 10.256 50.7381.684 1.321 0.045 0.7370.0003.772 0.000 0.0000.797 0.048 833.00.560.701 0.000 7.24 0.00 179.0 4/25/2025 08:34 0.0007.52017.485 10.364 41.7280.894 1.220 0.135 0.4150.0023.120 0.000 0.0000.756 0.051 833.00.630.795 0.000 7.52 0.00 180.0 4/25/2025 08:35 0.0005.82317.498 10.346 51.9761.781 0.810 0.140 0.8320.0025.123 0.000 0.0000.747 0.062 833.00.580.683 0.000 5.82 0.00 180.0 4/25/2025 08:36 0.0007.35617.524 10.355 46.9651.469 1.340 0.135 0.8050.0003.551 0.000 0.0000.721 0.020 833.00.460.629 0.000 7.36 0.00 180.0 4/25/2025 08:37 0.0005.05017.542 10.349 45.2431.061 0.656 0.147 0.5810.0004.985 0.000 0.0000.918 0.060 833.00.610.738 0.000 5.05 0.00 180.0 4/25/2025 08:38 0.1394.86117.522 10.343 54.9161.478 0.860 0.127 0.8630.0025.186 0.000 0.0000.949 0.036 833.00.350.409 0.000 5.00 0.00 180.0 4/25/2025 08:39 0.0007.63317.432 10.339 56.1231.894 1.645 0.072 1.0420.0153.314 0.000 0.0000.871 0.083 833.00.740.867 0.000 7.63 0.00 180.0 4/25/2025 08:40 0.3417.43617.446 10.308 51.5741.684 1.688 0.087 0.8990.0083.603 0.000 0.0000.875 0.066 833.00.590.684 0.000 7.78 0.00 180.0 4/25/2025 08:41 0.0008.00617.449 10.354 34.3450.518 1.244 0.024 0.2520.0013.122 0.000 0.0000.748 0.071 833.00.660.786 0.000 8.01 0.00 180.0 4/25/2025 08:42 0.0007.46417.474 10.339 43.2502.810 0.900 0.008 0.5480.0093.204 0.000 0.0000.790 0.064 833.00.600.705 0.000 7.46 0.00 180.0 4/25/2025 08:43 0.0007.71717.449 10.329 44.7263.801 1.535 0.232 0.6740.0042.696 0.000 0.0000.800 0.048 833.00.530.647 0.000 7.72 0.00 180.0 4/25/2025 08:44 0.0007.60017.464 10.355 50.1502.798 1.900 0.313 1.2000.0423.447 0.000 0.0000.722 0.000 833.00.540.810 0.000 7.60 0.00 180.0 4/25/2025 08:45 0.0007.64117.440 10.347 44.1551.903 1.729 0.189 0.8970.0133.045 0.000 0.0000.956 0.027 833.00.410.533 0.000 7.64 0.00 180.0 4/25/2025 08:46 0.0007.13317.458 10.280 45.5641.405 1.205 0.172 0.6960.0073.586 0.000 0.0000.639 0.059 833.00.720.902 0.000 7.13 0.00 180.0 4/25/2025 08:47 0.0007.74417.413 10.322 56.9571.019 1.617 0.161 1.0810.0073.375 0.000 0.0000.718 0.056 833.00.690.871 0.000 7.74 0.00 180.0 4/25/2025 08:48 0.0137.69617.454 10.354 52.4322.764 1.513 0.023 1.0790.0093.481 0.000 0.0000.745 0.019 833.00.390.527 0.000 7.71 0.00 180.0 4/25/2025 08:49 0.0007.49117.441 10.327 62.3412.550 1.965 0.142 1.5110.0073.768 0.000 0.0000.887 0.062 833.00.730.905 0.000 7.49 0.00 180.0 4/25/2025 08:50 0.0007.45117.483 10.356 58.0992.400 2.206 0.126 1.6340.0003.505 0.000 0.0000.752 0.000 833.00.570.859 0.000 7.45 0.00 180.0 4/25/2025 08:51 0.0008.09417.422 10.347 61.9520.665 1.595 0.161 1.7900.0003.810 0.000 0.0000.731 0.019 833.00.590.827 0.000 8.09 0.00 180.0 4/25/2025 08:52 0.0007.26917.452 10.351 51.4720.697 1.486 0.040 0.9450.0003.669 0.000 0.0000.484 0.046 833.00.791.044 0.000 7.27 0.00 180.0 0.0627.21717.453 10.333 51.4721.732 1.429 0.153 0.9290.0073.749 0.000 0.0000.795 0.062 833.000.6380.772 0.000 7.279 0.000 179.9Avg. Spike 2 4/25/2025 08:54 0.52629.30115.711 9.779 47.59554.501 1.311 0.296 0.8080.0353.692 1.150 24.8190.655 0.199 833.026.861.312 0.977 29.83 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Run 2 - B 30minute/60min 4/25/2025 08:56 0.0187.58117.434 10.331 57.2631.281 1.822 0.134 1.3590.0013.808 0.000 0.0000.942 0.105 833.00.690.719 0.000 7.60 0.00 180.0 4/25/2025 08:57 0.0007.33117.466 10.324 49.5091.703 1.769 0.098 1.0170.0483.027 0.000 0.0000.719 0.046 833.00.670.862 0.000 7.33 0.00 179.0 4/25/2025 08:58 0.0005.35317.501 10.346 56.6411.250 0.663 0.224 1.2960.0025.204 0.000 0.0000.864 0.012 833.00.380.539 0.000 5.35 0.00 180.0 4/25/2025 08:59 0.0477.48817.479 10.340 39.3231.386 1.499 0.015 0.7900.0063.292 0.000 0.0000.623 0.063 833.00.801.007 0.000 7.53 0.00 180.0 4/25/2025 09:00 0.0007.98817.423 10.334 51.2273.098 1.458 0.123 1.1560.0133.145 0.000 0.0000.779 0.007 833.00.380.551 0.000 7.99 0.00 180.0 4/25/2025 09:01 0.0008.58217.429 10.353 42.5652.675 1.952 0.316 0.9070.0113.171 0.000 0.0000.759 0.044 833.00.730.968 0.000 8.58 0.00 180.0 4/25/2025 09:02 0.0007.33117.484 10.334 52.5512.250 1.734 0.361 1.1570.0283.299 0.000 0.0000.883 0.058 833.00.620.751 0.000 7.33 0.00 180.0 4/25/2025 09:03 0.3027.53217.480 10.325 42.3911.913 1.648 0.315 0.7820.0023.502 0.000 0.0000.847 0.067 833.00.740.917 0.000 7.83 0.00 180.0 4/25/2025 09:04 0.1857.62817.461 10.369 58.5481.928 1.832 0.259 1.6200.0023.480 0.000 0.0000.953 0.035 833.00.650.866 0.000 7.81 0.00 180.0 4/25/2025 09:05 0.2517.73717.450 10.325 51.2421.768 1.738 0.285 1.3600.0193.368 0.000 0.0000.726 0.044 833.00.680.893 0.000 7.99 0.00 180.0 4/25/2025 09:06 0.0007.56017.451 10.301 54.8231.561 1.802 0.148 1.3970.0033.411 0.000 0.0000.886 0.026 833.00.520.706 0.000 7.56 0.00 180.0 4/25/2025 09:07 0.0337.51017.460 10.325 38.8981.624 1.168 0.122 0.7530.0012.968 0.000 0.0000.761 0.042 833.00.530.666 0.000 7.54 0.00 180.0 4/25/2025 09:08 0.4187.04117.472 10.330 60.6512.574 1.883 0.253 1.3540.0023.675 0.000 0.0001.061 0.067 833.00.560.644 0.000 7.46 0.00 180.0 4/25/2025 09:09 0.0007.67917.459 10.331 55.5161.826 1.821 0.216 1.5490.0223.671 0.000 0.0000.877 0.000 833.00.530.798 0.000 7.68 0.00 180.0 4/25/2025 09:10 0.0008.22417.445 10.346 61.6221.093 1.784 0.173 1.4680.0153.585 0.000 0.0000.859 0.069 833.00.790.972 0.000 8.22 0.00 180.0 4/25/2025 09:11 0.0008.17217.424 10.318 45.4321.333 1.484 0.128 0.7140.0063.492 0.000 0.0000.886 0.060 833.00.590.699 0.000 8.17 0.00 179.0 4/25/2025 09:12 0.1985.57817.434 10.314 47.9510.907 0.765 0.269 1.1300.0035.394 0.000 0.0000.792 0.024 833.00.500.672 0.000 5.78 0.00 179.0 4/25/2025 09:14 0.0445.73317.494 10.366 36.5250.755 0.440 0.136 0.6690.0375.206 0.000 0.0000.722 0.053 833.00.650.816 0.000 5.78 0.00 180.0 4/25/2025 09:15 0.0467.94617.518 10.340 44.7392.042 1.280 0.017 1.0760.0173.219 0.000 0.0000.831 0.033 833.00.530.698 0.000 7.99 0.00 180.0 4/25/2025 09:16 0.0007.00617.530 10.313 57.6071.848 1.456 0.113 1.3800.0003.786 0.000 0.0000.985 0.001 833.00.440.653 0.000 7.01 0.00 180.0 4/25/2025 09:17 0.0007.55017.551 10.378 47.0521.426 1.778 0.100 1.1310.0173.302 0.000 0.0001.106 0.001 833.00.400.595 0.000 7.55 0.00 180.0 4/25/2025 09:18 0.0045.22217.577 10.375 46.6030.953 0.652 0.253 0.9910.0035.004 0.000 0.0000.812 0.068 833.00.660.786 0.000 5.23 0.00 180.0 4/25/2025 09:19 0.0007.41917.521 10.321 57.3451.362 1.710 0.062 1.2750.0043.556 0.000 0.0000.815 0.045 833.00.720.941 0.000 7.42 0.00 180.0 4/25/2025 09:20 0.0009.03017.484 10.281 43.8621.168 1.230 0.133 1.0400.0003.500 0.000 0.0000.524 0.007 833.00.620.906 0.000 9.03 0.00 180.0 4/25/2025 09:21 0.0007.49117.529 10.301 41.6380.957 1.282 0.072 0.9590.0233.502 0.000 0.0000.897 0.006 833.00.500.730 0.000 7.49 0.00 180.0 4/25/2025 09:22 0.1548.15217.525 10.326 44.2091.179 1.553 0.000 1.0120.0143.360 0.000 0.0000.914 0.027 833.00.470.621 0.000 8.31 0.00 180.0 4/25/2025 09:23 0.5657.87517.510 10.264 41.2810.899 1.261 0.090 0.8100.0023.347 0.000 0.0000.644 0.033 833.00.570.758 0.000 8.44 0.00 180.0 4/25/2025 09:24 0.0007.32917.525 10.268 47.7720.881 1.063 0.107 1.1500.0333.534 0.000 0.0000.963 0.028 833.00.430.557 0.000 7.33 0.00 180.0 4/25/2025 09:25 0.0217.97817.508 10.319 35.1640.979 1.084 0.019 0.6540.0132.890 0.000 0.0000.832 0.067 833.00.670.798 0.000 8.00 0.00 180.0 4/25/2025 09:26 0.0007.24617.524 10.301 51.8162.055 1.535 0.067 1.0260.0203.221 0.000 0.0000.817 0.042 833.00.620.807 0.000 7.25 0.00 180.0 0.0767.41017.485 10.327 48.7261.556 1.438 0.154 1.0990.0123.631 0.000 0.0000.836 0.039 833.000.5880.763 0.000 7.486 0.000 179.9Avg. 0.0697.31317.469 10.330 50.0991.644 1.434 0.153 1.0140.0093.690 0.000 0.0000.816 0.051 833.000.6130.767 0.000 7.382 0.000 179.9Run 2 Avg: GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline 2 4/25/2025 09:28 0.0000.0000.041 0.043 0.0000.000 0.000 0.143 0.0000.0000.788 0.000 0.2820.000 0.000 833.00.490.314 0.000 0.00 0.00 180.0 Run 3 - A 30minute/60min 4/25/2025 09:30 0.0007.13217.360 10.170 47.6551.535 1.670 0.104 1.2560.0022.933 0.000 0.0000.803 0.033 833.00.560.738 0.000 7.13 0.00 180.0 4/25/2025 09:31 0.0008.38517.509 10.230 50.5511.270 1.461 0.110 1.1890.0003.393 0.000 0.0000.874 0.021 833.00.470.645 0.000 8.38 0.00 180.0 4/25/2025 09:32 0.0007.37617.516 10.277 52.4521.234 1.583 0.111 1.3330.0073.424 0.000 0.0000.886 0.009 833.00.480.693 0.000 7.38 0.00 180.0 4/25/2025 09:33 0.4077.23617.570 10.258 40.8590.942 1.537 0.000 1.0990.0063.204 0.000 0.0000.908 0.034 833.00.440.556 0.000 7.64 0.00 180.0 4/25/2025 09:34 0.3046.78317.601 10.252 37.5482.694 0.719 0.049 0.8340.0042.935 0.000 0.0000.858 0.000 833.00.500.754 0.000 7.09 0.00 180.0 4/25/2025 09:35 0.1497.54717.616 10.276 30.2813.747 1.354 0.190 0.5870.0092.743 0.000 0.0000.833 0.054 833.00.570.692 0.000 7.70 0.00 180.0 4/25/2025 09:36 0.1628.32717.614 10.254 51.2997.998 1.076 0.512 1.4540.0083.457 0.000 0.0000.895 0.017 833.00.590.829 0.000 8.49 0.00 180.0 4/25/2025 09:37 0.0007.85417.588 10.264 55.9486.879 2.147 0.956 1.6870.0332.811 0.000 0.0000.947 0.030 833.00.670.915 0.000 7.85 0.00 179.0 4/25/2025 09:38 0.0008.57917.657 10.360 42.1482.953 2.225 0.725 1.1290.0452.376 0.000 0.0000.621 0.000 833.00.470.712 0.000 8.58 0.00 180.0 4/25/2025 09:39 0.2527.45817.674 10.325 40.3792.223 1.154 0.461 1.1420.0103.080 0.000 0.0000.632 0.033 833.00.640.869 0.000 7.71 0.00 180.0 4/25/2025 09:40 0.0006.80917.684 10.257 53.1162.163 1.530 0.443 1.4100.0033.335 0.000 0.0000.890 0.000 833.00.510.764 0.000 6.81 0.00 180.0 4/25/2025 09:41 0.2486.32417.596 10.190 44.5922.596 0.873 0.366 1.2970.0193.377 0.000 0.0000.983 0.005 833.00.440.653 0.000 6.57 0.00 180.0 4/25/2025 09:42 0.0007.00617.574 10.244 59.6565.084 1.813 0.711 1.8050.0003.164 0.000 0.0000.783 0.028 833.00.660.907 0.000 7.01 0.00 180.0 4/25/2025 09:43 0.0006.98817.601 10.234 40.4682.003 1.559 0.530 0.8230.0293.192 0.000 0.0000.970 0.040 833.00.450.552 0.000 6.99 0.00 180.0 4/25/2025 09:44 0.3316.62517.606 10.234 45.4161.607 1.279 0.366 1.4410.0482.913 0.000 0.0000.890 0.032 833.00.630.845 0.000 6.96 0.00 180.0 4/25/2025 09:45 0.0006.66217.605 10.236 53.1041.022 1.541 0.297 1.6730.0113.345 0.000 0.0000.950 0.014 833.00.520.737 0.000 6.66 0.00 180.0 4/25/2025 09:46 0.0009.66217.607 10.207 46.3920.425 1.439 0.256 1.2140.0013.298 0.000 0.0001.021 0.039 833.00.560.728 0.000 9.66 0.00 180.0 4/25/2025 09:47 0.0946.24617.592 10.199 38.2491.465 0.867 0.192 0.9200.0022.822 0.000 0.0000.942 0.052 833.00.580.710 0.000 6.34 0.00 179.0 4/25/2025 09:48 0.3876.36117.610 10.244 41.2022.283 1.131 0.267 1.2500.0162.843 0.000 0.0000.732 0.066 833.00.710.872 0.000 6.75 0.00 180.0 4/25/2025 09:49 0.0125.98617.587 10.218 61.5354.679 1.386 0.539 1.6490.0063.496 0.000 0.0001.021 0.098 833.00.790.884 0.000 6.00 0.00 180.0 4/25/2025 09:50 0.0008.40117.613 10.219 59.2194.050 2.352 0.696 1.9040.0212.918 0.000 0.0000.791 0.031 833.00.480.625 0.000 8.40 0.00 180.0 4/25/2025 09:51 0.0005.98117.597 10.259 49.9082.228 1.258 0.506 1.4750.0193.184 0.000 0.0000.649 0.029 833.00.490.650 0.000 5.98 0.00 180.0 4/25/2025 09:52 0.0906.78417.581 10.272 54.7332.401 1.897 0.497 1.6820.0073.554 0.000 0.0001.018 0.050 832.00.700.898 0.000 6.87 0.00 180.0 4/25/2025 09:53 0.0006.32517.536 10.259 54.7880.878 1.357 0.438 1.2470.0003.496 0.000 0.0000.809 0.090 833.00.851.002 0.000 6.32 0.00 180.0 4/25/2025 09:55 0.0006.41517.580 10.291 67.5580.817 1.895 0.406 1.8600.0014.016 0.000 0.0001.025 0.090 832.00.871.028 0.000 6.41 0.00 180.0 4/25/2025 09:56 0.0448.90017.557 10.315 46.3851.330 1.586 0.343 1.2950.0253.425 0.000 0.0000.858 0.020 832.00.600.838 0.000 8.94 0.00 180.0 4/25/2025 09:57 0.2278.45817.602 10.331 52.8701.611 1.515 0.206 1.4470.0203.338 0.000 0.0000.958 0.026 832.00.470.621 0.000 8.68 0.00 180.0 4/25/2025 09:58 0.2787.70917.509 10.228 34.8330.835 1.577 0.248 0.9440.0122.905 0.000 0.0000.833 0.008 832.00.570.826 0.000 7.99 0.00 179.0 4/25/2025 09:59 1.1028.93617.600 10.264 17.3360.895 1.106 0.104 0.6020.0212.095 0.000 0.0000.778 0.031 832.00.490.642 0.000 10.04 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/25/2025 10:00 0.00012.29217.629 10.214 27.2921.111 1.981 0.023 0.6950.0012.603 0.000 0.0000.658 0.014 832.00.410.574 0.000 12.29 0.00 180.0 0.1367.51817.586 10.253 46.5922.365 1.496 0.355 1.2780.0133.123 0.000 0.0000.861 0.033 832.770.5720.759 0.000 7.654 0.000 179.9Avg. Spike 3 4/25/2025 10:02 1.36960.04616.084 9.587 12.08152.918 4.758 0.379 0.3270.0072.896 1.030 24.2810.872 0.302 832.026.120.813 0.978 61.41 0.00 180.0 Run 3 - B 30minute/60min 4/25/2025 10:04 0.8767.09017.737 10.136 11.82716.653 0.396 0.000 0.4210.0003.183 0.000 0.0000.556 0.113 832.00.720.733 0.000 7.97 0.00 180.0 4/25/2025 10:05 0.6427.89217.781 10.142 20.04833.394 0.822 0.079 0.4780.0102.511 0.000 0.0000.581 0.033 832.00.400.496 0.000 8.53 0.00 180.0 4/25/2025 10:06 0.0007.17017.753 10.161 30.90329.547 1.312 0.061 0.7040.0152.784 0.000 0.0000.790 0.009 832.00.410.581 0.000 7.17 0.00 180.0 4/25/2025 10:07 0.0347.19217.704 10.175 38.86519.692 1.511 0.176 1.1350.0172.747 0.000 0.0001.012 0.029 832.00.460.608 0.000 7.23 0.00 180.0 4/25/2025 10:08 0.0008.05217.662 10.123 44.36412.452 1.990 0.183 1.2450.0003.621 0.000 0.0000.879 0.018 832.00.590.823 0.000 8.05 0.00 179.0 4/25/2025 10:09 0.01010.05217.714 10.169 28.6143.966 2.028 0.265 0.4680.0272.891 0.000 0.0000.932 0.055 832.00.640.800 0.000 10.06 0.00 180.0 4/25/2025 10:10 1.39011.62617.782 10.136 15.2481.568 1.797 0.101 0.5510.0312.969 0.000 0.0000.640 0.041 832.00.580.746 0.000 13.02 0.00 180.0 4/25/2025 10:11 0.5658.52817.802 10.140 23.6983.321 0.929 0.048 0.5050.0282.506 0.000 0.0000.747 0.039 832.00.530.671 0.000 9.09 0.00 180.0 4/25/2025 10:12 0.1607.84617.753 10.157 40.0318.890 0.804 0.190 0.7810.0203.032 0.000 0.0000.827 0.047 832.00.600.756 0.000 8.01 0.00 180.0 4/25/2025 10:13 0.0007.39317.657 10.201 66.78915.998 1.309 0.614 1.4570.0053.469 0.000 0.0000.718 0.055 832.00.730.935 0.000 7.39 0.00 180.0 4/25/2025 10:14 0.0008.43217.594 10.214 72.72413.075 2.446 1.211 1.9950.0053.596 0.000 0.0000.789 0.042 832.00.710.936 0.000 8.43 0.00 180.0 4/25/2025 10:15 0.0007.96417.552 10.240 87.4168.118 3.180 1.194 1.7160.0003.651 0.000 0.0000.888 0.107 832.00.830.925 0.000 7.96 0.00 180.0 4/25/2025 10:16 0.0008.95217.534 10.277 43.3753.666 2.363 0.885 0.7000.0042.859 0.000 0.0001.025 0.042 832.00.570.735 0.000 8.95 0.00 180.0 4/25/2025 10:17 0.0007.64317.526 10.284 53.0702.849 1.548 0.522 1.2560.0003.373 0.000 0.0000.904 0.000 833.00.510.762 0.000 7.64 0.00 180.0 4/25/2025 10:18 0.0008.38417.558 10.294 57.3641.958 2.077 0.380 1.3780.0043.261 0.000 0.0000.895 0.020 832.00.490.676 0.000 8.38 0.00 180.0 4/25/2025 10:19 0.0008.74617.576 10.323 31.3781.365 1.897 0.250 0.4160.0013.163 0.000 0.0000.885 0.021 832.00.530.729 0.000 8.75 0.00 180.0 4/25/2025 10:20 0.2078.40717.628 10.317 35.9251.582 1.061 0.186 0.4330.0053.270 0.000 0.0000.613 0.064 832.00.660.805 0.000 8.61 0.00 180.0 4/25/2025 10:21 0.0007.38017.632 10.328 42.0982.152 1.274 0.127 0.6000.0123.104 0.000 0.0000.903 0.073 832.00.630.728 0.000 7.38 0.00 180.0 4/25/2025 10:22 0.0008.02917.539 10.287 53.9452.245 2.016 0.215 1.0920.0003.235 0.000 0.0000.811 0.043 832.00.660.854 0.000 8.03 0.00 180.0 4/25/2025 10:23 0.5748.05817.496 10.301 37.8671.576 1.401 0.190 0.7930.0032.569 0.000 0.0000.709 0.031 832.00.540.720 0.000 8.63 0.00 180.0 4/25/2025 10:24 0.2817.74117.528 10.275 45.0891.174 1.442 0.100 0.5800.0003.250 0.000 0.0000.618 0.086 832.00.800.941 0.000 8.02 0.00 180.0 4/25/2025 10:25 0.0008.66117.538 10.288 36.7500.952 1.332 0.046 0.4370.0002.872 0.000 0.0000.851 0.053 832.00.640.796 0.000 8.66 0.00 180.0 4/25/2025 10:26 0.0007.89317.512 10.325 44.2541.295 1.290 0.109 0.5260.0002.853 0.000 0.0000.769 0.052 832.00.670.851 0.000 7.89 0.00 180.0 4/25/2025 10:27 0.2958.23917.488 10.285 54.4801.300 1.563 0.031 1.0670.0033.303 0.000 0.0000.821 0.080 832.00.710.831 0.000 8.53 0.00 180.0 4/25/2025 10:28 0.0007.79117.484 10.279 53.9681.288 1.620 0.085 0.7620.0023.399 0.000 0.0000.840 0.059 832.00.650.800 0.000 7.79 0.00 180.0 4/25/2025 10:29 0.5728.32717.468 10.301 48.6961.068 1.525 0.000 0.6930.0072.874 0.000 0.0000.694 0.102 832.00.730.783 0.000 8.90 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/25/2025 10:30 0.5518.58917.450 10.313 33.5490.835 1.490 0.003 0.3790.0002.510 0.000 0.0000.781 0.089 832.00.600.634 0.000 9.14 0.00 180.0 4/25/2025 10:31 0.0008.27417.456 10.307 36.3381.714 1.064 0.015 0.4340.0002.523 0.000 0.0000.847 0.059 832.00.600.727 0.000 8.27 0.00 180.0 4/25/2025 10:32 0.0417.27917.467 10.297 61.1173.155 1.787 0.023 1.2490.0003.318 0.000 0.0000.837 0.068 832.00.630.748 0.000 7.32 0.00 180.0 4/25/2025 10:33 0.9408.31617.482 10.321 44.3922.333 2.073 0.169 0.6240.0112.963 0.000 0.0000.861 0.099 832.00.600.605 0.000 9.26 0.00 180.0 0.2388.19817.595 10.247 43.1396.639 1.578 0.249 0.8290.0073.055 0.000 0.0000.801 0.054 832.030.6140.758 0.000 8.435 0.000 180.0Avg. 0.1877.85817.590 10.250 44.8664.502 1.537 0.302 1.0540.0103.089 0.000 0.0000.831 0.044 832.400.5930.758 0.000 8.045 0.000 179.9Run 3 Avg: Baseline 3 4/25/2025 10:36 0.0000.0000.042 0.033 0.0000.000 0.000 0.109 0.0000.0000.708 0.000 0.1210.000 0.000 832.00.300.268 0.000 0.00 0.00 180.0 Post CTS 4/25/2025 10:37 0.0000.0000.023 0.062 0.0000.000 0.000 0.000 0.0000.0000.000 99.197 0.0000.000 0.058 832.066.420.261 0.020 0.00 0.00 180.0 4/25/2025 10:37 0.0000.0000.024 0.051 0.0000.000 0.011 0.000 0.5600.0000.000 99.780 0.0000.000 0.006 832.066.540.000 0.019 0.00 0.00 180.0 4/25/2025 10:37 0.0000.0000.023 0.030 0.0000.000 0.010 0.000 0.9490.0270.000 99.900 0.0000.482 0.031 832.066.670.000 0.032 0.00 0.00 180.0 Post NO2/Mid O2 4/25/2025 10:39 98.8275.7350.007 0.016 0.0000.131 1.010 0.046 0.0120.0050.000 0.000 0.1170.184 0.000 832.00.120.000 0.000 104.56 10.57 180.0 4/25/2025 10:39 99.2334.5860.006 0.000 0.2180.301 1.006 0.191 0.1800.0000.000 0.000 0.0500.259 0.034 832.00.120.000 0.000 103.82 10.61 180.0 4/25/2025 10:39 99.6154.5800.001 0.000 0.7560.000 0.960 0.132 0.0450.0000.000 0.000 0.0830.000 0.037 832.00.160.000 0.001 104.20 10.61 180.0 Post 5-Gas 4/25/2025 10:40 0.000243.8640.008 4.839 5.428477.495 1.730 2.021 1.5920.2070.387 1.217 251.2380.873 0.870 832.0255.332.312 9.750 243.86 0.00 180.0 4/25/2025 10:40 0.000246.5180.011 4.897 4.407480.508 1.779 2.175 0.3870.0380.008 1.132 253.2140.788 0.857 832.0257.092.102 9.793 246.52 0.00 180.0 4/25/2025 10:40 0.000246.0160.004 4.900 4.395482.975 1.686 2.238 0.5360.0000.000 1.135 254.4230.000 0.601 832.0258.342.936 9.813 246.02 0.00 180.0 4/25/2025 10:40 0.000247.4110.003 4.899 3.779484.141 1.786 2.116 0.8510.0700.000 1.160 253.3260.000 0.965 832.0257.642.417 9.820 247.41 0.00 180.0 4/25/2025 10:40 0.000248.3650.003 4.916 6.220480.559 1.612 2.075 1.4590.0190.000 1.161 254.4320.609 0.656 832.0258.522.995 9.835 248.37 0.00 180.0 4/25/2025 10:40 0.000247.8780.002 4.924 4.375484.146 1.710 2.128 0.0000.2040.000 1.115 253.9520.225 0.820 832.0257.692.039 9.837 247.88 0.00 180.0 End of Test Purge 4/25/2025 10:42 0.0000.096-0.000 0.031 0.0560.578 0.000 0.125 0.1150.0630.000 0.000 0.4630.588 0.086 832.00.640.000 0.017 0.10 0.00 180.0 4/25/2025 10:42 0.0000.730-0.000 0.020 0.0000.353 0.020 0.119 0.0000.0660.000 0.000 0.5320.000 0.023 832.00.810.354 0.007 0.73 0.00 180.0 4/25/2025 10:42 0.0000.889-0.000 0.028 0.0000.154 0.016 0.075 0.0000.0000.395 0.000 0.5430.000 0.000 832.00.790.374 0.001 0.89 0.00 180.0 4/25/2025 10:42 0.0000.1990.008 0.039 0.6610.467 0.031 0.000 0.0000.0000.125 0.000 0.4450.000 0.000 832.00.640.288 0.000 0.20 0.00 179.0 4/25/2025 10:43 0.0000.8540.006 0.021 0.0000.259 0.018 0.000 0.0000.0000.634 0.000 0.3060.431 0.042 832.00.410.038 0.001 0.85 0.00 180.0 4/25/2025 10:43 0.0001.0790.004 0.018 0.0040.261 0.035 0.201 0.0000.0000.480 0.000 0.4750.298 0.053 832.00.730.220 0.000 1.08 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/25/2025 10:43 0.0000.5040.002 0.014 0.0000.229 0.029 0.000 0.2490.1420.812 0.000 0.2380.000 0.049 832.00.910.863 0.000 0.50 0.00 180.0 4/25/2025 10:43 0.0000.3530.006 0.010 0.0000.351 0.000 0.016 0.0000.0000.212 0.000 0.0660.000 0.040 832.00.150.000 0.000 0.35 0.00 180.0 4/25/2025 10:43 0.0000.948-0.000 0.013 0.2080.000 0.000 0.000 0.3210.0030.430 0.000 0.3240.000 0.000 832.00.650.490 0.001 0.95 0.00 180.0 GAS Performance Test Report Test Type: Annual Test Date: 4/21/2025 Waukesha 9394 GSI Rich Burn (4 Cycle) 303 W. 3rd St Elk City , OK 73644(580) 225-0403 Test Started:Test Completed:07:43 AM 11:12 AM Source: Unit Number: 1350 Serial Number: 1651138 Engine Hours:12287 Permit #: #DAQE-AN161680001-23 Location: Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, Inc. Residue Booster Station 40 CFR Part 60 Subpart JJJJ CO NOx NMNEHC 44.724 8.308 1.724 2.000 0.300 1.000 0.150 0.700 0.030 0.157 0.048 0.010 Pass Pass Pass Pass Pass Pass Federal State Federal State Federal State Results ppmvd Results g/hp-hr Permit g/hp-hr PASS ALL Index Tables Figures Appendices Table 5.1 (Run Summaries)................................................................ Table 6.1 (Volumetric Flow Rate Data)............................................... Table 6.2 (Stack Gas Measurements)................................................. Table 8.1 (Oxygen Calibration)........................................................... Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... Annex Table 1.2.2 (Measurement System Capabilities)..................... Annex Table 1.3.1 (Test Specific Target Analytes)............................. Annex Table 4.1 (Measure System Capabilities)................................ Figure 6.1 (Location of Traverse Points per Method 1)....................... Annex Figure 1.4.1 (Sampling Train).................................................. Annex Figure 1.4.2 (Sampling Points)................................................. Annex Figure 1.4.3 (Sampling Port Locations).................................... Certified Calibration Bottle Certificates................................................ Tri Probe Certification via GD-031...................................................... GAS ALT 141_FTIR EPA.................................................................... Tester Qualifications (resume)............................................................ Raw Data............................................................................................ 27 Key Personnel.............................................................................1.0 3 Sampling System........................................................................2.0 3 Methods Used.............................................................................3.0 3 Test Summaries..........................................................................4.0 5 Run Summaries..........................................................................5.0 6 6 Volumetric Flow Rate Data.........................................................6.0 7 7 7 7 Calculations................................................................................7.0 8 9 12 12 13 15 13 14 14 20 25 28 29 Oxygen Calibration.....................................................................9 Engine Parameter Data Sheet....................................................10 QA/QC Results............................................................................11 Signature Page...........................................................................12.0 Appendices.................................................................................13.0 Bottle Certs.................................................................................2014.0 Tri Probe Certification via GD-031..............................................2515.0 GAS ALT 141_FTIR EPA............................................................16.0 Tester Qualifications (resume)....................................................2817.0 D6348 Annexes..........................................................................1211.0 18 19 26 8.0 9.0 10.0 Raw Data....................................................................................2918.0 1.0 Key Personnel GAS Crusoe Energy Systems, Inc. 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A EPA Method 2 & 2C EPA Method 3A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. ASTM D6348-03 Jason Woolley 3 Cooper Green GAS 4.0 Test Summary T e s t S u m m a r y Site Verification Photos GAS Unit 1350 with a serial number of 1651138 which is a Waukesha 9394 GSI engine located at Residue Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/21/2025 by Cooper Green with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2433 BHP and 1200 RPM which is 97.33% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1350 is authorized to operate under permit #DAQE-AN161680001-23. 4 4.0 Test Summary Engine/Compressor Specs Residue Booster StationLocation 1350Unit ID Make Waukesha Site Elevation ft.5455 Model 9394 GSI Atmospheric Pressure psi.11.96 Serial Number 1651138 Stack Diameter in.20 mfg. rated hp 2500 Yes 1200 Date of Manufacture Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1 Test Horsepower 2425 2425 2450 2433 1200 1200 1199 1200 Percent Load % Intake Manifold Pressure (hg) 97.00%97.00%98.00%97.33% 114.71 115.12 116.54 115.46 Intake Manifold Temperature (F)116.60 118.90 119.30 118.27 Ambient Conditions Ambient Temperature Dry (F)40.00 47.00 58.00 48.33 Exhaust Flow Data Q Stack (dscfh) Q Stack (dscm/hr) 259727.37 259250.34 258549.89 259175.87 7354.59 7341.08 7321.25 7338.97 Moisture Fraction Bws Fuel Consumption (Btu/h[-hr) 0.17 0.17 0.17 0.17 0 0 0 0 Fuel Flow (dscfh) Fuel (btu/scf)1020 1020 1020 1020 O2 F factor 8710.0 8710 8710 8710 Results Method 3A Corrected O2% Dry Moisture %17.41%17.43%17.42%17.42% T e s t S u m m a r y mfg. rated rpm Test RPM 0.00%0.00%0.00%0.00% Permitted Standards Results 5 Catalyst Run 1 Run 2 Run 3 3 Run Average Pass Permits 07:43 AM 08:51 AM 10:00 AM 4/21/2025 State NOx (mol wt) 46.01 1.690 1.199 1.381 1.423NMNEHC (ppmvw) 2.046 1.452 1.672 1.724NMNEHC (ppmvd) NMNEHC (mol wt) 44.10 577.615 409.916 472.101 486.544 FailNMNEHC (ppbvd) @15% O2 0.011 0.008 0.009 0.0100.700 0.030 PassNMNEHC (g/hp-hr) 0.578 0.410 0.472 0.487 FailNMNEHC (ppmvd) @15% O2 0.1690.161CO (g/hp-hr)0.141 0.1572.000 0.300 Pass CO (ppmvw)32.986 37.747 40.070 36.934 CO (ppmvd)39.936 45.714 48.523 44.724 CO (mol wt) 28.01 CO (ppmvd) @15% O2 11.274 12.905 13.698 12.626 Fail CO (ppbvd) @15% O2 11273.922 12904.829 13697.941 12625.564 Fail NOx (g/hp-hr)0.055 0.051 0.038 0.0481.000 0.150 Pass NOx (ppmvw)7.782 7.309 5.493 6.861 NOx (ppmvd)9.421 8.852 6.651 8.308 NOx (ppbvd) @15% O2 2659.594 2498.812 1877.636 2345.347 Fail NOx (ppmvd) @15% O2 2.660 2.499 1.878 2.345 Fail GAS GAS 5.0 Run Summaries Summary Source Run 1 R u n Table 5.1 Run Summaries S u m m a r i e s 6 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture % 32.99 0.40 6.97 0.82 7.78 0.00% 0.00% 0.00% 17.41% 7.32 0.52 0.00%17.35% 29.19 2.05 0.00%15.96% 6.61 1.11 0.00%17.46% 0.00 0.00 0.00 0.00%0.05% Avg. Wet NO Summary Source Run 2 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 0.62 0.00 0.00 0.00 0.00%0.05% 38.62 7.70 0.39 8.09 0.00%17.43% 74.66 28.98 2.25 31.23 0.00%15.87% 36.88 6.13 0.40 6.53 0.00%17.43% 0.94 0.16 0.00 0.15 0.00%0.03% Avg. Wet 37.75 6.91 0.40 7.31 1.20 0.00%17.43% NO2NO 0.90 1.42 22.04 0.98 1.02 Summary Source Run 3 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 38.22 5.11 0.83 5.93 0.00%17.45% 99.97 27.14 1.42 28.56 0.00%15.90% 41.92 4.13 0.92 5.05 0.00%17.40% 0.62 0.00 0.00 0.00 0.00%0.05% 0.94 0.16 0.00 0.15 1.02 0.00%0.03% Avg. Wet 40.07 4.62 0.87 5.49 1.38 0.00%17.42% NO2NO 0.92 1.49 24.29 1.27 NMNEHC 0.61 NO2 0.000.28 1.64 23.45 1.74 0.90 1.69 0.40 7.84 31.24 7.72 26.62 39.35 0.62 87.09 6.0 Volumetric Flow Rate Data Volumetric Flow Rate Data .99 Table 6.1. Data used for volumetric flow rate (Method 2) Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet Run 1 Average Pitot Tube Coefficient Cp(std)= H2O CO2 O2 CO Molecular Weight Stack Gas dry basis (Md) Molecular Weight Stack Gas wet basis (Ms) Stack Static Pressure (Pg) Stack Static Pressure (Pg) Atmospheric Pressure at Location (Pbar) Atmospheric Pressure at Location (Pbar) Absolute Stack Pressure (Ps) Stack Temperature Stack Temperature Stack Temperature Stack Gas Velocity Stack Flow Rate Q Stack Gas Wet Volmetric Flow Rate Stack Gas Dry Volumetric Flow Rate Sample after Back Purge: Within 5% of Last Δpstd reading: Stack Diameter (inches) Inches upstream from disturbance Inches downstream from disturbance scf/hr 1.16 Yes 20.00 5.00 32.00 scf/hr cfs ft/sec Deg R Deg F Deg C "Hg "Hg MBAR "Hg "H20 g/g mole g/g mole %d %d %d %17.41 30.00 0.91 Inches 3.34 10 16.66 Vo l u m e t r i c F l o w Ra tes Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 Figure 6.1 16 Traverse Points Were Used Emissions Sampling Points - 3 point long line sampling probe First Sampling Point Taken @ 16.7% of Stack Diameter Second Sampling Point Taken @ 50% of Stack Diameter Third Sampling Point Taken @ 83.3% of Stack Diameter 12.50 0.00 0.00 1014.22 0.07 29.96 30.03 903.31 1362.98 484.06 27.91 102.96 224.66 314458.95 259727.37 Run 2 17.43 30.01 0.95 12.57 0.00 0.00 1014.22 0.07 29.96 30.03 905.25 1364.92 485.14 27.92 105.25 224.63 313968.83 259250.34 Run 3 17.42 30.01 0.95 12.58 0.00 0.00 1012.19 0.07 29.90 29.97 906.31 1365.98 485.73 27.92 105.47 224.63 313097.79 258549.89 17.42 30.01 0.94 12.55 0.00 0.00 1013.54 0.07 29.94 30.01 904.96 1364.63 484.98 27.92 104.56 224.63 313841.86 259175.87 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets. * Cyclonic Flow Check (Pass/Fail): PASS Δpstd (in) H2O 0.83 Exhaust Temp F 903.00 Pitot Tube Sampling Points (Velocity) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Δpstd Average= Run 1 Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate 0.94 1.02 1.03 903.00 904.00 903.00 0.89 0.73 0.78 903.00 903.00 904.00 0.89 0.82 0.92 904.00 903.00 903.00 1.04 903.00 0.94 0.94 0.91 904.00 903.00 903.00 0.85 0.95 0.91 903.00 904.00 903.31 Δpstd = Velocity head measured by the standard pitot tube, (in.) H2O.Run 3 Δpstd (in) H2O 0.90 Exhaust Temp F 906.00 0.97 0.83 0.95 906.00 907.00 906.00 0.99 0.91 0.87 906.00 906.00 907.00 1.11 0.97 0.86 907.00 906.00 906.00 0.94 906.00 0.90 0.85 1.04 907.00 906.00 906.00 0.97 1.16 906.00 907.00 906.310.95 Run 2 Δpstd (in) H2O 0.96 Exhaust Temp F 905.00 0.95 1.03 0.99 905.00 906.00 905.00 0.99 0.89 0.96 905.00 905.00 906.00 0.97 0.96 0.97 905.00 905.00 905.00 0.95 906.00 0.93 0.88 0.83 905.00 905.00 905.00 0.92 1.02 906.00 905.00 0.95 905.25 Pass Strat Check 10.329Check 1 10.330Check 2 10.337Check 3 CO2Gas Used Pass/Fail 7 GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate *Note- Use of this method negates the need for any fuel related numbers for emissions calculations Nomenclature Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293°K (528 °R). Vs = Average stack gas velocity, m/sec (ft./sec). *(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1 Md = .44(12.504)+ .32(0)+ .28(87.492+.004) = 30 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO) 12.5 Molecular Weight of Stack Gas. Equation 2-6 Ms = 30(1 -.17405)+ 18.0(.17405) = 27.91 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws) 12.6 Average Stack Gas Velocity. Equation 2-7 Vs = 85.49*.99*√.91*√(1362.98/(30.03*27.91)) = 102.96 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms)) 12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8 Qsd = 3600(1-.17405)102.96*2.182((528*30.03)/ (1362.98*29.92)) = 259727.37 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd)) *Standard conversion from feet to meters Q = 259727.37/35.315 = 7354.591 DSCM/HRQ = Qsd/35.315 Emission Rates (Examples use CO Run 1) Nomenclature CO corrected @ 15% O2 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ER = Emission rate of (CO) in g/HP-hr. F(d )= Volumes of combustion components per unit of heat content, scm/J (scf/million Btu). Q = Stack gas volumetric flow rate, in standard cubic meters per hour, dry basis LB/HR.= Emission rate of (CO) in LB/HR. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) O2 = Concentration of oxygen on a dry basis, percent. ppm= Parts Per Million (CO) ppm@15% O2= PPM corrected to 15% O2 Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (DSCF/HR.). Run Time = Run Time in Minutes TPY= Tons per Year Mol wt.= Mol Weight of CO (28.01) Vs = Average stack gas velocity, m/sec (ft./sec). ppm @ 15% O2 = 39.936*(20.9-15)/(20.9-0%)) = 11.274 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2)) G/HP HR from 40 CFR Part 60 Subpart JJJJ (39.936*(1.164*10^-3)*7354.591*(Run Time/60))/2425 = .141 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR LB/HR from Grams LB/HR = .141*1/453.6*2425 = .754 LB/HRlb/hr = ER*1/453.6*BHP-HR TPY TPY = .754*4.38 = 3.303 TPYTPY = LB/HR. *4.38 Horsepower HP Provided On Site Wet to Dry PPM 39.94 = 32.9855*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry 8 Cp(std) = Standard pitot tube coefficient; use 0.99 GAS 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span. 8.0 Oxygen Calibration 8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases. (1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration EPA Method 3A QA Worksheet (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Certified Gas Concentraion Low-Level (%) 0.00% Certified Gas Concentraion Mid-Level (%) Certified Gas Concentraion High-Level (%) (DIRECT) Analyzer Calibration Error (≤ 2%) Certified Concentration Value (%) Direct Calibration Response (%) Absolute Difference (%) Analyzer Calibration Error (%)Analyzer Direct Calibration Response Certified bottle value % 0.00% 0.00% 0.00% Zero Gas % Mid-Level Gas % High-Level Gas % Bias Pre Initial Value Bias Post Inital Values System Calibrations Response Pre (%) 0.00% System Bias (% of Span) Pre System Calibration Response Post (%) System Bias (% of Span) Post Drift (% of Span) 0.00%0.00%0.00%0.00% (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Avg. Gas Concentration (Run 1) Avg. Gas Concentration (Run 2) Avg. Gas Concentration (Run 3) Effluent Gas (Cgas) Run 1 Effluent Gas (Cgas) Run 2 Effluent Gas (Cgas) Run 3 Linearity Check 0.00%0.00%0.00% Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Upscale Gas Analyzer Calibration Response (%) Zero Gas Upscale Gas EPA Method 3A QA Worksheet Zero Gas Mid-Level Gas High-Level Gas 100% Nitrogen O2 QA/QC Zero Gas %0.00% Mid-Level Gas % High-Level Gas % System Calibration Response Pre (%) System Calibration Response Post (%) Zero Gas % Upscale Cal Zero Gas % Upscale Cal Upscale Used Upscale Used 10.56% 20.70% 10.52% 10.35% 10.73% 10.73% 10.35%10.52% 10.56% 20.70% 10.73% 21.04% 10.73% 21.04% 10.73%21.04% 0.00% 10.73% 21.04% 0.17% 0.34% 0.79% 1.63% 10.73% Span Zero Offset 0.00% 21.04 0.00% 10.56%0.20%1.01%0.01% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 9 GAS 1078.0 1078.0 1080.3 1096.0 1096.0 1097.0 -6.0 -6.0 -6.0 9.0 Engine Parameter Data Sheet Company Site Elevation (ft) Facility Unit ID Date Make Crusoe Energy Systems, Inc. Residue Booster Station 4/21/2025 5455 1350 Waukesha Model Serial Number 9394 GSI 1651138 Technician Cooper Green Run Start Times 07:43 AM 08:51 AM 10:00 AM 11:12 AM Run 1 Run 2 Run 3 Completed Engine Parameter Data Run 1 Engine Speed (RPM)1200.0 1200.0 1199.0 1199.7 Engine Hours 12284 12285 12286 12287 Intake Manifold Pressure (psi)68.3 68.5 69.2 68.7 Intake Manifold Temp °F 116.6 118.9 119.3 118.3 Engine Load (BHP)2425.0 2425.0 2450.0 2433.3 Ambient Temp °F 40.0 47.0 58.0 48.3 Humidity %53.0 39.0 31.0 41.0 Dew Point °F 24.0 24.0 27.0 25.0 Waukesha Yes 2 2 2 2# of Catalyst Installed Catalyst (Yes or No) AFR Setting (Target Left Bank) AFR Setting (Target Right Bank) AFR Manufacturer/Type Waukesha Waukesha Waukesha 10 Run 3 AverageRun 2 Discharge Pressure (psi) Suction Pressure (psi) 1085.0 1099.0 -6.0Catalyst Pressure Drop H2O Catalyst Outlet Temp °F Catalyst Inlet Temp °F GAS 10.0 QA/QC Results Average:Carbon monoxide CO Gas, Inc. 0.06 R e s u l t s Average:Nitrogen monoxide NO 0.21 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.20 Average:VOC 0.08 Average:Oxygen 0.00 Pre-test Baseline Results Time: Q A / Q C Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.60 Tolerance 2.00% Difference between measured and expected 1.40% CTS Direct to Analyzer Time: Average:Carbon monoxide CO 0.49 Average:Nitrogen monoxide NO 0.19 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.19 Average:VOC 0.71 Average:Oxygen 0.00 Pre-test System Zero Time: Mechanical Response Time 45 seconds Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.40 Tolerance 5.00% Difference between measured and expected 1.60% Pre-test System CTS & Mechanical Response Time 55 secondsEquilibration Response Time Value:Spike Reported 251.83 Value:Spike Expected 253.10 System (Equilibration) Response Time Target (Spike) 45 secondsSystem Zero Response Time 61 secondsSystem Response Time System (Zero) Response Time 11 11.0 D6348 Annexes 1-8 D6348 Annexes 1. Test Plan Requirements Annex 1.2 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration NO2 Ethylene SF6 O2 (%) CC524639 12/30/2027 103.00 10.73% CC252676 10/17/2032 100.00 CC433538 8/5/2032 21.04% Cylinder # SG9132842BAL Expiration: 8-20-2032 Propane CO NO SF6 Bottle Value 253.10 497.30 252.90 9.95 Analyzer System Response 251.83 488.59 247.39 9.74 Percent Difference 0.50%1.75%2.18%2.14% Annex Table 1.2.2 Measurement System Capabilities SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.604 4.930 Spike Direct Propane 252.583 Mechanical Response Time SF6 9.798 CO 492.402 NO 249.887 Ethylene 98.403 36 seconds Analyzer Response Propane 251.825 SF6 9.741 CO 488.590 NO 247.390 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 251.416 CO 483.790 NO 246.352 55 seconds 40 seconds 8.19% 8.05% 8.74% 100.43% 98.84% 99.93% 9.726 12 GAS Annex 1.3 Compounds Infrared Analysis Region (cm-1) Expected Concentration Range Measurement System Achievable Minimum Detectable Concentrations Required Measurement System Accuracy and Precision for Test Application CO 2000-2200 0-1200 ppm NO 1875-2138 NO2 2700-2950 VOC 2600-3200 910-1150 2550-2950 CH2O 2550-2850 Interfering Compounds * CO is analyzed in a separate analysis region than CO2 and H2O CO2 Water Vapor 926-1150 3200-3401 Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives 0.16267 ppm 4 ppm 0-1000 ppm 0.4007 ppm 2 ppm 0-100 ppm 0.4899 ppm 2 ppm 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC 0-100 ppm 0.7878 ppm 1 ppm 0-10% 0-22% 0% 0.20% n/a n/a * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. Annex 1.4 Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 13 GAS Sampling Point Locations in Inches 16.7%3.340 50%10.000 83.3%16.660 Figure Annex 1.4.3 Sample Port Location Figure Annex 1.4.2 Sampling Points Interior Stack Diameter (inches): Inches Upstream: Inches Downstream: 20 5 32 14 Stack Gas Dry Volumetric Flow Rate (scf/hr): 259175.87 H2O%d @ Sampling Point:17.42 CO2%d @ Sampling Point:12.55 Pressure @ Sampling Point (Pg "H2O):0.94 Temperature @ Sampling Point (Deg F):904.96 GAS D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1) Target Analyte Results (ppm) CO 0.1627 NO 0.4007 NO2 0.4899 Ethylene 0.3782 Propane 0.4351 Hexane 0.2233 Acetaldehyde 0.8152 Formaldehyde 0.7878 D6348 Annex 3. FTIR Reference Spectra Calibration Transfer Standard Expected Measured Path Length Validated Ethylene 100 98.6 4.93 Passed D6348 Annex 4. Required Pre-Test Procedures Annex Table 1.2.2 Measurement System Capabilities 15 SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.604 4.930 Spike Direct Propane 252.583 Mechanical Response Time SF6 9.798 CO 492.402 NO 249.887 Ethylene 98.403 36 seconds Analyzer Response Propane 251.825 SF6 9.741 CO 488.590 NO 247.390 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 251.416 CO 483.790 NO 246.352 55 seconds 40 seconds 8.19% 8.05% 8.74% 100.43% 98.84% 99.93% 9.726 GAS D6348 Annex 5. Analyte Spiking Technique Propane Spike Direct SF6 CO NO 253.100 9.954 497.300 252.900 252.583 9.798 492.402 249.887 0.20% 1.57% 0.98% 1.19% +/- 2% +/- 2% +/- 2% +/- 2% Pass Pass Pass Pass Parameter Gas Concentration Measured % Difference Specification Validated 0.214 0.000 Spike Average 21.016 0.802 Dilution Factor 8.185% Expected 20.926 % Recovery 100.430% Specification 70-130% <10% Spike Run 1 via the System Source Output Propane SF6 D6348 Annex 6. Determination of System Performance Parameters Noise Equivalent Absorbance (NEA) RMS High RMS Mid RMS Low Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%) 0.000 Spike Average 0.789 Dilution Factor 8.053% Expected % Recovery Specification 70-130% <10% Spike Run 2 via the System Source Output Propane SF6 0.000 Spike Average 0.856 Dilution Factor 8.736% Expected % Recovery Specification 70-130% <10% Spike Run 3 via the System Source Output Propane SF6 0.174 22.263 22.279 99.930% 0.000091 0.000174 0.000368 0.226 20.343 20.582 98.840% Line Position Difference:Resolution Difference to Reference0.00%Pass Pass3.49% 16 GAS Resolution The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. Detector Linerarity The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. D6348 Annex 7. Preparation of Analytical Quantification Algorithm The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 Regression Slope:-4.61332418 Pass Line Position Difference:Resolution Difference to Reference 3.49% D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures CTS Bottle Concentration: CTS Sample Concentration Average: Difference between measured and expected: Tolerance: 100.00 97.48 2.58% 5.00% POST CTS System Check: Run 1 Points 1 & 2 on CO/NO/Propane Run 2 Points 1 & 2 on CO/NO/Propane Run 3 Points 1 & 2 on CO/NO/Propane Run Data Validation - Automated vs Manual Reading Validated Comments All within 20% All within 20% All within 20% Passed Passed Passed Demonstrates no interferences observed. Demonstrates no interferences observed. Demonstrates no interferences observed. 17 GAS 12.0 Signature Page Job/File Name: We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Crusoe Energy Systems, Inc.; Residue Booster Station; 1350; JJJJ 18 Company: Print Name: Signature: Title: Phone Number: Date: Company:G.A.S. Inc.Date: Print Name: Title: 4/21/2025 Emissions Specialist Company:G.A.S. Inc.Date: Print Name: Title: Signature: Phone Number: Travis Hartley Director of Stack Testing 580-225-0403 4/21/2025 Cooper Green GAS Appendices GAS GAS Spike (5 Gas) GAS 9% O2/NO2 GAS Ethylene Only GAS BIP GAS 21% O2 Tri Probe Certification ” ‡ ƒ – Ž ƒ ‹ • • • ƒ Ž › – ‹ … ƒ Ž ‡ ” ˜ ‹ … ‡ • ͵Ͳ͵͵”†–Ž‹–›ǡǡ͹͵͸ͶͶ ȋͷͺͲȌʹʹͷǦͲͶͲ͵ ƒšǣȋͷͺͲȌʹʹͷǦʹ͸ͳʹ &(57,),&$7(2)$1$/<6,6 *UDGHRI3URGXFW&(57,),('67$1'$5'352%( 3DUW1XPEHU65HIHUHQFH 1XPEHU  /DERUDWRU\*$6,1&6WDFN'LDPHWHU $QDO\VLV'DWH7DUJHW)ORZ 5DWH /PLQ /271XPEHU 61 $ $6 1XPEHURI 3RLQWV  3URGXFWSHUIRUPDQFHYHULILHGE\GLUHFWFRPSDULVRQWRFDOLEUDWLRQVWDQGDUGVWUDFHDEOHWR1,67  7KHSUREHOLVWHGRQWKLVIRUPPHHWVWKHPXOWLSRLQWWUDYHUVHUHTXLUHPHQWRI(3$0HWKRGH VHFWLRQDVVKRZQLQWKHDFFRPSDQ\LQJGDWD0HWKRGHVHFWLRQVWDWHVWKDWWKHPXOWLSRLQW WUDYHUVHUHTXLUHPHQWFDQEHVDWLVILHGE\VDPSOLQJYLD³DPXOWLKROHSUREHGHVLJQHGWRVDPSOHDW WKHSUHVFULEHGSRLQWVZLWKDIORZSHUFHQWRIPHDQIORZUDWH´ $1$/<7,&$/5(68/76 ZƵŶηdŽƚĂů&ůŽǁ ;>ͬŵͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϭͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϮͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϯͿ 0HDQ3UREH 3RUW6DPSOHG )ORZ /P  5XQ/30  䧮    䧮    䧮   5XQ/30  䧮    䧮    䧮    &DOLEUDWLRQFRQGXFWHGLQDFFRUGDQFHZLWK(PLVVLRQ0HDVXUHPHQW&HQWHU*XLGHOLQH'RFXPHQW±(0&*' 1RWHV BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB $SSURYHGIRU5HOHDVH'DWH 2/17/2022 Probe size: 20S Mr. Jordan Williamson CEO GAS Inc. 303 W. 3rd Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. March 15, 2021 Sincerely, Steffan M. Johnson, Group Leader Measurement Technology Group If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. cc: Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leather.james@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Heather Sessing, Oklahoma DEQ, (Heather.sessing@deq.ok.gov) Cooper Green GAS Type of Sources Tested: info@gasinc.us Stationary Internal Combustion Engines • 4 Stroke Rich Burn Engines • 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods: • EPA Method 1 & 1A – Sampling & Traverse Points • EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream • EPA Method 3A – Oxygen • EPA Method 7E – NOX • EPA Method 10 – Carbon Monoxide • EPA Method 25A – Volatile Organic Compounds • ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. • Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Types of Analyzers: • Gasmet DX4000 FTIR • Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory • Testo 350 • Flame Ionization Detector 580-225-0403 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 1 Minute Average Data Sheet Crusoe Energy Systems, Inc.Client: Residue Booster Station Unit Number:1350 Make:Waukesha Location:9394 GSIModel: 1651138Serial Number: RAW Result Data Stability 4/21/2025 05:38 0.7590.053-0.003 0.006 0.1950.000 0.000 0.014 0.0170.0080.451 0.209 0.0000.000 0.000 844.00.260.175 0.001 0.81 0.00 180.0 Pre Test Baseline Direct 4/21/2025 05:46 0.0000.4090.003 0.006 0.0000.105 0.007 0.000 0.1130.0000.209 0.000 0.1000.161 0.000 844.00.100.000 0.000 0.41 0.00 180.0 4/21/2025 05:46 0.0000.0000.000 0.000 0.0760.064 0.001 0.000 0.2490.0990.174 0.000 0.0730.063 0.009 844.00.100.015 0.000 0.00 0.00 180.0 4/21/2025 05:47 0.0000.205-0.001 0.000 0.0000.000 0.000 0.029 0.0000.0020.043 0.000 0.0190.000 0.000 844.00.030.023 0.000 0.20 0.00 180.0 CTS Direct 4/21/2025 05:48 0.0000.2320.013 0.016 0.0000.000 0.010 0.000 0.3020.0130.000 98.620 0.0000.000 0.021 844.065.820.037 0.028 0.23 0.00 179.0 4/21/2025 05:49 0.0000.0000.010 0.015 0.0000.000 0.000 0.063 0.3510.0000.000 98.596 0.0000.072 0.027 844.065.830.059 0.026 0.00 0.00 180.0 4/21/2025 05:49 0.2300.1310.009 0.012 0.0000.000 0.000 0.000 0.3640.0660.000 98.596 0.0000.167 0.000 844.065.730.000 0.028 0.36 0.00 180.0 High O2 Direct 4/21/2025 05:55 0.0000.5000.002 0.000 0.2710.000 0.007 0.163 0.1280.0000.403 0.000 0.0800.000 0.018 844.00.120.000 0.000 0.50 20.68 180.0 4/21/2025 05:56 0.0000.4890.002 0.000 0.0000.000 0.000 0.053 0.1780.0150.592 0.000 0.1320.054 0.035 844.00.380.267 0.000 0.49 20.68 180.0 4/21/2025 05:56 0.0000.3780.000 0.000 0.0000.000 0.000 0.188 0.3370.0001.029 0.000 0.0000.000 0.000 844.00.000.000 0.000 0.38 20.73 180.0 NO2/Mid O2 Direct 4/21/2025 06:00 102.6300.2140.002 0.000 0.6300.000 0.978 0.000 1.1840.0000.000 0.000 0.0000.000 0.000 844.00.000.000 0.000 102.84 10.56 180.0 4/21/2025 06:00 102.0910.176-0.001 0.000 0.2210.000 0.965 0.000 0.5680.0000.000 0.000 0.0000.000 0.000 844.00.000.000 0.000 102.27 10.58 180.0 4/21/2025 06:01 102.9110.0000.000 0.000 0.3090.000 0.969 0.000 0.8950.0000.387 0.000 0.0000.081 0.000 844.00.000.000 0.000 102.91 10.55 180.0 Spike Direct 4/21/2025 06:04 0.000249.9380.000 4.949 4.497491.809 1.801 2.267 0.7370.2880.000 0.956 252.4650.000 0.915 844.0256.732.692 9.795 249.94 0.00 180.0 4/21/2025 06:04 0.000250.7170.000 4.945 5.271492.798 1.784 1.990 0.9090.2170.500 0.955 252.2940.335 0.862 844.0256.282.436 9.794 250.72 0.00 180.0 4/21/2025 06:05 0.000249.006-0.002 4.946 4.985492.600 1.775 1.887 0.6480.1500.817 0.956 252.9900.322 0.835 844.0257.032.593 9.804 249.01 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline System 4/21/2025 06:07 0.0000.0000.009 0.020 0.0000.560 0.000 0.089 0.1590.0000.891 0.000 0.3020.000 0.166 844.00.680.073 0.000 0.00 0.00 180.0 4/21/2025 06:08 0.0000.4290.007 0.015 0.0000.452 0.000 0.150 0.0000.0000.943 0.000 0.2750.000 0.173 844.00.820.301 0.000 0.43 0.00 180.0 4/21/2025 06:08 0.0000.1390.011 0.016 0.0000.466 0.000 0.167 0.0000.0030.774 0.000 0.1600.000 0.167 844.00.640.219 0.000 0.14 0.00 180.0 CTS System with Response Time 4/21/2025 06:09 0.0000.0000.014 0.018 0.0000.134 0.000 0.000 0.1070.0000.000 98.253 0.0000.000 0.204 844.065.910.000 0.024 0.00 0.00 180.0 4/21/2025 06:10 0.0000.0000.013 0.024 0.0000.177 0.000 0.000 0.0000.0000.000 98.475 0.0000.185 0.180 844.066.010.000 0.024 0.00 0.00 180.0 4/21/2025 06:10 0.0000.0000.016 0.027 0.0000.110 0.000 0.000 0.0310.0000.000 98.480 0.0000.000 0.195 844.066.050.000 0.022 0.00 0.00 180.0 NO2/Mid O2 System with Response Time 4/21/2025 06:12 100.3532.8110.011 0.020 0.0000.834 0.979 0.044 0.0000.0000.338 0.000 0.0000.418 0.096 844.00.190.000 0.000 103.16 10.48 180.0 4/21/2025 06:13 100.6553.5200.003 0.004 0.2580.248 1.015 0.000 0.1880.0000.000 0.000 0.1180.000 0.057 844.00.260.037 0.000 104.17 10.54 180.0 4/21/2025 06:13 100.2862.7140.006 0.012 0.0000.672 0.972 0.107 0.0000.0000.000 0.000 0.1910.000 0.080 844.00.350.000 0.000 103.00 10.54 180.0 Spike System with Response Time 4/21/2025 06:15 0.000247.0980.001 4.926 4.715488.605 1.811 1.908 0.4610.0220.357 1.061 251.0620.081 0.996 844.0255.432.498 9.740 247.10 0.00 180.0 4/21/2025 06:15 0.000247.4500.006 4.928 4.874488.974 1.742 1.924 0.6660.0180.439 1.065 252.3020.000 0.815 844.0256.182.301 9.739 247.45 0.00 180.0 4/21/2025 06:16 0.000247.6220.003 4.941 5.005488.190 1.795 2.263 0.3190.0430.049 1.069 252.1110.000 0.914 844.0256.092.157 9.743 247.62 0.00 180.0 Baseline System with Response Time 4/21/2025 06:20 0.0000.4380.008 0.029 0.1660.415 0.000 0.101 0.0000.0000.392 0.000 0.1990.000 0.102 844.00.570.247 0.000 0.44 0.00 180.0 4/21/2025 06:20 0.0000.7630.003 0.011 0.1640.156 0.003 0.102 0.0000.0030.251 0.000 0.3620.000 0.037 844.00.630.291 0.000 0.76 0.00 180.0 4/21/2025 06:20 0.0000.0000.002 0.010 0.0000.282 0.031 0.070 0.4040.0000.016 0.000 0.3320.000 0.060 844.00.630.270 0.000 0.00 0.00 180.0 Run 1 - A 30minute/60min 4/21/2025 07:43 0.0008.88515.962 10.125 51.40534.582 0.452 0.524 0.0000.13122.238 0.000 5.1060.823 1.028 832.07.330.254 0.000 8.88 0.00 180.0 4/21/2025 07:44 0.2897.47617.364 10.302 55.52725.834 0.972 1.139 0.9620.0443.206 0.000 0.3290.805 0.479 832.01.830.821 0.000 7.77 0.00 180.0 4/21/2025 07:45 0.0007.42617.512 10.281 58.95826.017 0.836 1.761 0.9150.0473.124 0.000 0.0720.868 0.387 832.01.250.609 0.000 7.43 0.00 180.0 4/21/2025 07:46 0.8267.73617.546 10.278 59.72325.039 0.948 3.447 0.9770.0012.935 0.000 0.2690.884 0.446 833.01.941.170 0.000 8.56 0.00 180.0 4/21/2025 07:47 0.0007.36317.414 10.302 55.11422.285 1.051 3.748 0.8970.0006.493 0.000 0.1320.919 0.326 833.01.390.907 0.000 7.36 0.00 180.0 4/21/2025 07:48 0.0007.38417.349 10.299 51.57123.130 1.019 3.343 0.9480.0145.150 0.000 0.0380.865 0.355 833.01.160.615 0.000 7.38 0.00 179.0 4/21/2025 07:49 0.0007.38317.384 10.325 49.94122.972 0.934 3.699 0.8820.0084.440 0.000 0.0260.776 0.338 833.01.170.704 0.000 7.38 0.00 180.0 4/21/2025 07:50 0.0007.50217.385 10.326 52.49822.944 1.121 3.921 0.5640.0284.257 0.000 0.0170.734 0.382 833.01.420.959 0.000 7.50 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 07:51 0.0007.52817.391 10.278 55.55825.898 0.757 4.942 1.0340.0004.454 0.000 0.0450.836 0.407 833.01.350.742 0.000 7.53 0.00 180.0 4/21/2025 07:52 0.0006.93417.379 10.303 60.70924.844 0.880 5.424 1.1260.0063.851 0.000 0.0790.809 0.381 833.01.270.644 0.000 6.93 0.00 180.0 4/21/2025 07:53 0.0007.41017.373 10.351 57.52332.195 0.987 6.764 1.0350.0013.510 0.000 0.0000.904 0.417 833.01.290.689 0.000 7.41 0.00 180.0 4/21/2025 07:54 0.0007.97717.369 10.323 60.88129.656 0.860 6.173 1.0290.0343.909 0.000 0.0270.957 0.430 833.01.410.784 0.000 7.98 0.00 180.0 4/21/2025 07:55 0.0007.19517.367 10.377 53.99834.217 1.257 7.371 0.9540.0313.343 0.000 0.0000.940 0.446 833.01.340.670 0.000 7.19 0.00 180.0 4/21/2025 07:56 0.0007.32817.412 10.369 45.49138.798 1.467 8.786 0.6260.0022.728 0.000 0.0000.913 0.440 833.01.290.611 0.000 7.33 0.00 180.0 4/21/2025 07:57 0.9217.28817.409 10.389 55.54432.902 0.857 4.547 1.2220.0312.779 0.000 0.0000.917 0.459 833.01.290.562 0.000 8.21 0.00 180.0 4/21/2025 07:58 0.0007.37117.381 10.361 51.00124.778 1.282 6.093 0.9190.0063.051 0.000 0.0000.775 0.456 833.01.320.617 0.000 7.37 0.00 180.0 4/21/2025 07:59 1.5027.05517.374 10.344 53.82927.805 0.939 5.183 1.0430.0002.765 0.000 0.0000.771 0.489 833.01.460.721 0.000 8.56 0.00 180.0 4/21/2025 08:00 1.4947.73117.369 10.380 46.41822.163 1.431 5.947 0.8170.0022.353 0.000 0.0000.920 0.483 833.01.450.732 0.000 9.23 0.00 180.0 4/21/2025 08:01 0.0007.40217.366 10.349 52.64318.640 0.881 3.848 0.8080.0072.462 0.000 0.0000.700 0.502 833.01.540.802 0.000 7.40 0.00 180.0 4/21/2025 08:02 1.7376.84417.409 10.337 54.20415.889 1.027 3.563 1.1450.0002.736 0.000 0.0000.869 0.509 833.01.440.640 0.000 8.58 0.00 180.0 4/21/2025 08:03 1.3256.68917.423 10.374 44.28322.247 1.038 3.701 0.6380.0022.263 0.000 0.0000.833 0.540 833.01.570.736 0.000 8.01 0.00 180.0 4/21/2025 08:05 2.3466.73517.418 10.372 48.60623.848 1.136 4.170 0.8120.0022.389 0.000 0.0000.858 0.504 833.01.470.701 0.000 9.08 0.00 180.0 4/21/2025 08:06 0.0007.93617.431 10.310 46.24826.704 0.777 4.456 0.2180.0012.721 0.000 0.0000.962 0.481 833.01.570.911 0.000 7.94 0.00 180.0 4/21/2025 08:07 1.0217.57617.382 10.302 52.86122.421 0.876 4.673 0.5980.0102.514 0.000 0.0000.958 0.523 833.01.660.927 0.000 8.60 0.00 180.0 4/21/2025 08:08 1.8527.26617.381 10.359 42.49424.146 1.548 5.666 0.7630.0052.056 0.000 0.0000.930 0.496 833.01.460.702 0.000 9.12 0.00 180.0 4/21/2025 08:09 0.0008.76817.395 10.273 41.05325.173 0.987 4.505 0.6840.0092.127 0.000 0.0490.911 0.488 833.01.420.591 0.000 8.77 0.00 180.0 4/21/2025 08:10 2.3856.24817.388 10.219 38.56926.580 1.317 6.110 0.7750.0002.248 0.000 0.1840.714 0.464 833.01.600.733 0.000 8.63 0.00 179.0 4/21/2025 08:11 0.0006.58917.407 10.342 28.28129.635 1.536 6.783 0.0000.0071.082 0.000 0.0050.891 0.492 833.01.500.772 0.000 6.59 0.00 180.0 4/21/2025 08:12 0.0006.72317.418 10.359 38.00034.534 1.019 5.401 0.1560.0001.513 0.000 0.0150.942 0.466 833.01.550.907 0.000 6.72 0.00 180.0 4/21/2025 08:13 0.0005.81417.463 10.283 50.36032.772 0.947 4.830 0.8910.0011.994 0.000 0.0330.737 0.489 833.01.480.696 0.000 5.81 0.00 180.0 0.5237.31917.354 10.320 50.44326.622 1.038 4.684 0.7810.0143.690 0.000 0.2140.857 0.470 832.901.6410.731 0.000 7.842 0.000 179.9Avg. Spike 1 4/21/2025 08:16 2.04729.18915.961 9.836 37.36387.087 1.165 7.440 0.6050.0071.742 1.273 21.0160.832 0.497 833.023.450.887 0.802 31.24 0.00 180.0 Run 1 - B 30minute/60min 4/21/2025 08:18 1.2297.62017.442 10.273 34.69040.749 1.380 7.843 0.4560.0011.775 0.000 0.5000.743 0.346 833.01.780.876 0.000 8.85 0.00 180.0 4/21/2025 08:19 1.9596.25617.393 10.312 39.97941.986 1.000 6.636 0.7910.0011.353 0.000 0.3330.696 0.466 833.01.830.847 0.000 8.21 0.00 180.0 4/21/2025 08:20 0.5817.08317.456 10.302 26.48548.046 2.426 12.606 0.0000.0271.297 0.000 0.2750.680 0.390 833.01.660.907 0.000 7.66 0.00 180.0 4/21/2025 08:21 1.0495.80817.446 10.287 28.62736.956 0.888 5.952 0.4450.0001.666 0.000 0.2900.914 0.433 833.01.540.569 0.000 6.86 0.00 180.0 4/21/2025 08:22 0.7395.76217.427 10.315 35.03745.861 1.345 7.419 0.0000.0031.574 0.000 0.1010.965 0.466 833.01.500.708 0.000 6.50 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 08:23 1.0275.84417.433 10.329 31.15544.520 1.512 8.539 0.1280.0071.328 0.000 0.3270.709 0.454 833.01.890.983 0.000 6.87 0.00 180.0 4/21/2025 08:24 1.9446.78617.438 10.329 44.28442.734 0.746 5.546 0.5240.0131.601 0.000 0.3480.705 0.452 833.01.860.909 0.000 8.73 0.00 180.0 4/21/2025 08:25 1.0207.73817.383 10.330 45.65534.792 1.480 7.817 0.6600.0001.425 0.000 0.4200.875 0.441 833.02.031.094 0.000 8.76 0.00 180.0 4/21/2025 08:26 1.6205.70017.406 10.377 33.18353.991 1.442 9.290 0.4930.0270.989 0.000 0.3340.811 0.459 833.01.700.669 0.000 7.32 0.00 180.0 4/21/2025 08:27 1.3655.20217.412 10.328 43.97246.253 0.912 7.297 0.9510.0002.021 0.000 0.3220.867 0.410 833.01.660.784 0.000 6.57 0.00 180.0 4/21/2025 08:28 1.5658.15317.422 10.299 34.38041.735 2.131 10.703 0.6510.0001.387 0.000 0.4010.764 0.427 833.01.690.658 0.000 9.72 0.00 179.0 4/21/2025 08:29 1.4556.46617.436 10.424 26.65254.331 1.823 9.506 0.0000.0350.673 0.000 0.3650.660 0.346 833.01.630.860 0.000 7.92 0.00 180.0 4/21/2025 08:30 1.7425.54417.484 10.314 46.54937.485 0.629 4.324 0.4430.0002.044 0.000 0.4760.964 0.381 833.01.760.779 0.000 7.29 0.00 180.0 4/21/2025 08:31 0.6616.31517.480 10.290 36.66136.541 1.444 7.782 0.3260.0001.877 0.000 0.4430.628 0.326 833.01.740.967 0.000 6.98 0.00 180.0 4/21/2025 08:32 1.8246.55217.460 10.382 32.21940.141 1.436 7.159 0.3330.0031.191 0.000 0.4350.796 0.314 833.01.590.785 0.000 8.38 0.00 180.0 4/21/2025 08:33 1.5055.90017.447 10.364 40.38637.587 1.185 6.182 0.6560.0061.109 0.000 0.4570.712 0.404 833.01.840.863 0.000 7.41 0.00 180.0 4/21/2025 08:34 1.6196.03817.445 10.334 45.26434.536 1.117 6.096 0.5630.0171.694 0.000 0.2940.725 0.465 833.01.720.743 0.000 7.66 0.00 180.0 4/21/2025 08:35 1.0317.83417.441 10.325 47.14326.917 1.027 6.110 0.6380.0091.848 0.000 0.4510.716 0.417 834.01.780.735 0.000 8.87 0.00 180.0 4/21/2025 08:36 0.7816.98017.463 10.377 45.84122.657 1.472 6.237 1.0450.0032.029 0.000 0.4320.812 0.425 834.01.870.882 0.000 7.76 0.00 180.0 4/21/2025 08:37 0.5106.29017.503 10.356 35.69623.229 1.248 5.894 0.1400.0041.666 0.000 0.5400.879 0.348 833.01.850.926 0.000 6.80 0.00 180.0 4/21/2025 08:38 0.5757.78817.506 10.333 34.73028.245 1.347 6.553 0.0780.0092.023 0.000 0.4280.887 0.504 833.02.020.876 0.000 8.36 0.00 179.0 4/21/2025 08:39 1.8546.44017.468 10.397 43.39126.109 1.232 4.651 0.0440.0221.066 0.000 0.3480.836 0.387 833.01.630.762 0.000 8.29 0.00 180.0 4/21/2025 08:40 0.3317.07317.427 10.385 41.30931.921 1.629 7.167 0.0000.0280.867 0.000 0.5090.927 0.329 833.01.770.906 0.000 7.40 0.00 180.0 4/21/2025 08:41 0.8106.14517.498 10.266 40.43735.587 1.041 7.243 0.2260.0002.340 0.000 0.4950.881 0.315 833.01.530.603 0.000 6.96 0.00 180.0 4/21/2025 08:42 0.7357.73917.502 10.277 35.66741.680 1.433 8.358 0.1820.0001.593 0.000 0.5410.703 0.312 833.01.700.799 0.000 8.47 0.00 180.0 4/21/2025 08:43 0.1886.70517.513 10.375 39.85642.568 1.625 7.935 0.7690.0091.387 0.000 0.4130.867 0.447 833.01.880.853 0.000 6.89 0.00 180.0 4/21/2025 08:45 0.6816.69317.513 10.359 30.89141.905 1.500 8.140 0.0190.0071.458 0.000 0.4280.878 0.369 833.01.630.701 0.000 7.37 0.00 180.0 4/21/2025 08:46 0.6247.18017.504 10.334 31.90748.709 1.830 10.417 0.1530.0001.806 0.000 0.4520.802 0.311 833.01.610.807 0.000 7.80 0.00 180.0 4/21/2025 08:47 0.8956.37717.472 10.340 30.33546.666 1.038 6.784 0.3390.0001.689 0.000 0.4300.832 0.303 833.01.630.890 0.000 7.27 0.00 180.0 4/21/2025 08:48 1.3746.31517.462 10.333 35.62746.028 1.457 7.832 0.5550.0171.728 0.000 0.3790.703 0.406 833.01.850.990 0.000 7.69 0.00 180.0 1.1106.61117.456 10.335 37.26739.349 1.359 7.467 0.3870.0081.550 0.000 0.3990.798 0.395 833.071.7390.824 0.000 7.721 0.000 179.9Avg. 0.8176.96517.405 10.327 43.85532.985 1.199 6.076 0.5840.0112.620 0.000 0.3070.828 0.433 832.981.6900.778 0.000 7.781 0.000 179.9Run 1 Avg: Baseline 1 4/21/2025 08:50 0.0000.0000.048 0.043 0.0000.618 0.000 0.477 0.0000.0000.000 0.000 0.5630.000 0.034 833.00.900.397 0.000 0.00 0.00 180.0 Run 2 - A 30minute/60min 4/21/2025 08:52 1.3445.92116.826 9.980 36.41639.763 0.951 5.019 0.3180.0591.963 0.000 0.4560.829 0.275 833.01.610.909 0.000 7.26 0.00 180.0 4/21/2025 08:53 0.9946.85717.460 10.322 42.92243.263 1.515 7.376 0.5820.0012.146 0.000 0.3690.744 0.417 833.01.790.872 0.000 7.85 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 08:54 1.0247.68917.504 10.351 30.90148.754 1.920 10.198 0.0000.0041.920 0.000 0.3720.674 0.316 833.01.500.742 0.000 8.71 0.00 180.0 4/21/2025 08:55 0.8277.71617.500 10.380 26.47645.865 1.520 8.435 0.0000.0041.709 0.000 0.4350.557 0.266 833.01.490.789 0.000 8.54 0.00 180.0 4/21/2025 08:56 0.3517.67517.519 10.375 32.59946.750 1.778 9.157 0.2980.0191.882 0.000 0.4000.544 0.365 833.01.770.963 0.000 8.03 0.00 180.0 4/21/2025 08:57 0.6736.94417.551 10.355 28.66149.416 1.154 7.919 0.0000.0192.279 0.000 0.3590.762 0.234 833.01.501.011 0.000 7.62 0.00 180.0 4/21/2025 08:58 0.5067.32317.531 10.370 35.10038.557 1.199 6.805 0.2530.0002.481 0.000 0.3020.960 0.330 833.01.520.837 0.000 7.83 0.00 180.0 4/21/2025 08:59 0.6227.83017.455 10.360 34.22045.100 1.819 9.874 0.1450.0002.040 0.000 0.2730.817 0.384 833.01.570.787 0.000 8.45 0.00 179.0 4/21/2025 09:00 0.6727.46017.445 10.386 41.47838.282 0.973 5.951 0.0000.0002.154 0.000 0.1890.785 0.375 833.01.510.853 0.000 8.13 0.00 180.0 4/21/2025 09:01 0.1367.19117.435 10.362 44.96929.930 1.128 5.916 0.5460.0002.289 0.000 0.2880.771 0.367 833.01.680.994 0.000 7.33 0.00 180.0 4/21/2025 09:02 0.6788.29417.430 10.365 33.95333.551 1.891 8.288 0.0880.0002.009 0.000 0.3570.681 0.384 833.01.620.747 0.000 8.97 0.00 180.0 4/21/2025 09:03 0.3317.30617.440 10.396 46.95033.165 0.943 5.490 0.1700.0122.279 0.000 0.2570.906 0.399 833.01.680.934 0.000 7.64 0.00 180.0 4/21/2025 09:04 0.1517.52817.393 10.314 57.76729.241 1.043 8.234 0.7440.0002.922 0.000 0.3710.685 0.421 833.01.951.101 0.000 7.68 0.00 179.0 4/21/2025 09:05 0.0008.32517.417 10.396 45.07834.566 1.468 8.039 0.3790.0042.132 0.000 0.1430.755 0.298 833.01.310.863 0.000 8.32 0.00 180.0 4/21/2025 09:06 0.0006.55217.425 10.406 32.24535.364 0.942 8.146 0.0000.0093.203 0.000 0.0130.827 0.334 833.01.170.730 0.000 6.55 0.00 180.0 4/21/2025 09:07 0.7497.76417.418 10.356 44.16831.488 1.019 5.594 0.6490.0012.302 0.000 0.3150.709 0.335 833.01.570.869 0.000 8.51 0.00 180.0 4/21/2025 09:08 0.1757.88417.437 10.314 49.46129.244 1.087 7.862 0.3530.0003.172 0.000 0.2550.850 0.352 833.01.651.045 0.000 8.06 0.00 180.0 4/21/2025 09:09 0.6679.38217.404 10.372 34.51534.734 2.190 9.830 0.3570.0002.169 0.000 0.2030.827 0.317 833.01.390.826 0.000 10.05 0.00 180.0 4/21/2025 09:10 0.2948.03817.442 10.387 27.84335.639 1.460 7.634 0.0000.0002.142 0.000 0.1530.695 0.308 833.01.531.147 0.000 8.33 0.00 180.0 4/21/2025 09:11 0.6517.75417.470 10.347 32.17135.712 1.239 7.239 0.4090.0032.591 0.000 0.2950.624 0.260 833.01.480.997 0.000 8.40 0.00 180.0 4/21/2025 09:12 0.0008.39917.457 10.380 42.57937.032 1.554 9.006 0.3830.0002.184 0.000 0.1170.734 0.277 833.01.391.072 0.000 8.40 0.00 180.0 4/21/2025 09:13 0.0008.08217.487 10.399 31.26440.407 1.189 7.506 0.1380.0102.134 0.000 0.1430.891 0.268 833.01.401.083 0.000 8.08 0.00 180.0 4/21/2025 09:14 0.2038.07217.468 10.390 40.29138.684 1.758 9.822 0.4660.0002.611 0.000 0.1880.699 0.318 833.01.400.858 0.000 8.28 0.00 180.0 4/21/2025 09:15 0.0007.41217.443 10.372 32.51046.332 1.325 8.231 0.2640.0002.415 0.000 0.1000.817 0.206 833.00.980.699 0.000 7.41 0.00 180.0 4/21/2025 09:16 0.0009.20817.414 10.385 24.12844.189 2.467 12.505 0.0050.0072.311 0.000 0.0860.888 0.215 833.00.930.621 0.000 9.21 0.00 180.0 4/21/2025 09:17 0.1808.36317.409 10.392 23.32047.867 1.819 10.265 0.2270.0192.182 0.000 0.1571.025 0.195 833.01.080.801 0.000 8.54 0.00 180.0 4/21/2025 09:18 0.3457.17617.400 10.368 34.15440.839 1.120 7.162 0.0000.0002.338 0.000 0.0410.884 0.203 833.01.060.926 0.000 7.52 0.00 180.0 4/21/2025 09:19 0.0007.32417.416 10.385 49.81431.753 0.898 5.649 0.7730.0043.086 0.000 0.0700.722 0.207 833.00.970.727 0.000 7.32 0.00 180.0 4/21/2025 09:20 0.0887.60517.427 10.379 44.40333.269 1.372 9.201 0.7670.0002.439 0.000 0.0340.752 0.229 833.01.050.833 0.000 7.69 0.00 180.0 4/21/2025 09:21 0.0007.92617.452 10.392 33.07039.731 1.813 11.196 0.0000.0332.240 0.000 0.0380.905 0.230 833.01.050.823 0.000 7.93 0.00 180.0 0.3897.70017.429 10.358 37.11438.616 1.418 8.118 0.2770.0072.324 0.000 0.2260.777 0.303 833.001.4200.882 0.000 8.088 0.000 179.9Avg. Spike 2 4/21/2025 09:23 2.25328.98115.874 9.835 40.10274.661 1.524 7.798 0.7840.0003.249 0.791 20.3430.573 0.276 833.022.040.919 0.789 31.23 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Run 2 - B 30minute/60min 4/21/2025 09:26 0.96810.58117.452 10.382 20.61944.775 2.686 12.791 0.0160.0002.167 0.000 0.2600.734 0.254 833.01.270.748 0.000 11.55 0.00 180.0 4/21/2025 09:27 0.0447.22817.409 10.367 21.04031.365 0.145 6.265 0.2440.0005.202 0.000 0.1580.866 0.212 833.01.180.897 0.000 7.27 0.00 179.0 4/21/2025 09:28 0.2114.86017.483 10.386 25.71547.133 0.455 7.417 0.2220.0005.258 0.000 0.0230.403 0.223 833.00.920.676 0.000 5.07 0.00 180.0 4/21/2025 09:29 0.0657.18017.417 10.368 22.99648.651 1.030 7.371 0.3490.0002.549 0.000 0.1270.765 0.189 833.01.020.781 0.000 7.24 0.00 180.0 4/21/2025 09:30 0.0893.71317.424 10.380 46.00041.293 0.000 5.879 0.3860.0015.198 0.000 0.0120.631 0.284 833.01.210.946 0.000 3.80 0.00 180.0 4/21/2025 09:31 0.0006.89717.424 10.405 56.53530.413 0.752 5.743 1.3180.0002.998 0.000 0.0040.785 0.213 833.00.930.744 0.000 6.90 0.00 180.0 4/21/2025 09:32 0.7167.03017.425 10.418 44.38630.421 1.641 10.489 1.0110.0002.574 0.000 0.0820.853 0.264 833.01.110.753 0.000 7.75 0.00 180.0 4/21/2025 09:33 0.0007.09417.415 10.384 37.73137.697 1.487 9.271 0.5230.0012.513 0.000 0.0000.934 0.110 833.00.830.922 0.000 7.09 0.00 180.0 4/21/2025 09:34 0.0006.75317.363 10.356 39.81938.057 1.074 8.023 0.7480.0002.641 0.000 0.1791.047 0.129 833.01.010.865 0.000 6.75 0.00 179.0 4/21/2025 09:35 0.6186.23817.404 10.400 23.96937.061 1.863 12.309 0.4930.0013.419 0.000 0.1040.803 0.194 833.01.050.833 0.000 6.86 0.00 180.0 4/21/2025 09:36 0.3316.58217.411 10.397 23.61243.801 1.149 9.525 0.2980.0173.351 0.000 0.0570.753 0.210 833.00.830.523 0.000 6.91 0.00 180.0 4/21/2025 09:37 0.9659.23517.437 10.391 17.35835.913 2.039 9.621 0.5550.0002.363 0.000 0.1240.644 0.196 833.01.010.742 0.000 10.20 0.00 180.0 4/21/2025 09:38 0.6304.63517.439 10.401 18.90042.184 0.387 7.285 0.4460.0005.063 0.000 0.0950.675 0.186 833.00.880.624 0.000 5.26 0.00 180.0 4/21/2025 09:39 1.0594.77117.441 10.442 21.93442.201 0.978 8.063 0.2060.0153.439 0.000 0.0000.725 0.194 833.00.700.463 0.000 5.83 0.00 180.0 4/21/2025 09:40 0.1695.67817.436 10.385 30.20036.170 0.000 5.264 0.6190.0005.023 0.000 0.1540.801 0.157 833.01.060.881 0.000 5.85 0.00 179.0 4/21/2025 09:41 0.0005.17217.473 10.417 28.95738.136 0.863 8.931 0.5050.0003.450 0.000 0.0000.936 0.193 833.00.720.504 0.000 5.17 0.00 180.0 4/21/2025 09:42 0.3346.13117.449 10.424 19.91337.444 1.525 10.470 0.3210.0003.118 0.000 0.0510.773 0.190 833.00.830.605 0.000 6.46 0.00 180.0 4/21/2025 09:43 0.3107.36817.400 10.398 18.29734.850 1.453 7.210 0.5370.0011.887 0.000 0.1430.802 0.191 833.01.030.756 0.000 7.68 0.00 180.0 4/21/2025 09:44 0.7265.04817.423 10.380 28.45535.336 0.000 5.026 0.6430.0005.038 0.000 0.1160.956 0.208 833.01.020.739 0.000 5.77 0.00 180.0 4/21/2025 09:45 0.6896.00617.393 10.398 31.49138.698 0.984 8.637 0.6610.0023.431 0.000 0.0000.800 0.220 833.00.880.655 0.000 6.69 0.00 180.0 4/21/2025 09:46 0.4788.51617.415 10.400 18.38232.096 2.366 9.022 0.5600.0032.051 0.000 0.1441.092 0.184 833.01.000.733 0.000 8.99 0.00 180.0 4/21/2025 09:47 0.0005.68917.412 10.364 21.55033.187 0.768 5.103 0.2580.0012.143 0.000 0.0160.646 0.214 833.00.870.641 0.000 5.69 0.00 179.0 4/21/2025 09:48 0.2333.63317.434 10.430 26.51242.641 0.345 6.582 0.5500.0014.476 0.000 0.0001.063 0.201 833.00.820.626 0.000 3.87 0.00 180.0 4/21/2025 09:49 1.1714.54417.472 10.428 51.97829.778 0.052 4.957 1.4530.0004.989 0.000 0.0180.747 0.230 833.01.020.820 0.000 5.72 0.00 180.0 4/21/2025 09:50 0.5106.65617.498 10.411 25.74327.410 1.285 8.468 0.7250.0004.039 0.000 0.0510.861 0.197 833.00.840.598 0.000 7.17 0.00 180.0 4/21/2025 09:51 0.1084.47517.402 10.375 27.76432.020 0.000 4.889 0.7300.0034.654 0.000 0.1840.879 0.219 833.01.210.879 0.000 4.58 0.00 180.0 4/21/2025 09:52 0.3885.48217.422 10.405 23.79828.589 0.943 6.710 0.5440.0003.262 0.000 0.1140.852 0.230 833.01.100.783 0.000 5.87 0.00 180.0 4/21/2025 09:53 0.3214.11117.413 10.391 30.78336.751 0.465 6.726 0.6500.0014.464 0.000 0.1110.908 0.248 833.01.110.749 0.000 4.43 0.00 180.0 4/21/2025 09:54 0.0008.22517.431 10.377 21.43735.607 1.888 9.548 0.5680.0051.841 0.000 0.0870.457 0.201 833.00.870.569 0.000 8.23 0.00 180.0 4/21/2025 09:55 0.9864.25817.420 10.375 31.78036.621 0.140 5.710 0.6940.0054.806 0.000 0.0940.905 0.240 833.01.000.632 0.000 5.24 0.00 180.0 0.4046.12617.428 10.395 28.58836.877 0.959 7.777 0.5610.0023.580 0.000 0.0840.803 0.206 833.000.9780.723 0.000 6.530 0.000 179.9Avg. 0.3966.91317.429 10.376 32.85137.746 1.189 7.948 0.4190.0042.952 0.000 0.1550.790 0.254 833.001.1990.802 0.000 7.309 0.000 179.9Run 2 Avg: GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline 2 4/21/2025 09:58 0.0000.1550.031 0.054 0.0000.936 0.015 0.415 0.0000.0000.000 0.000 0.6120.000 0.059 833.01.020.438 0.000 0.15 0.00 180.0 Run 3 - A 30minute/60min 4/21/2025 10:00 1.1465.79017.229 10.303 28.46534.875 1.705 5.501 0.9220.0141.711 0.000 0.2210.852 0.259 833.01.330.887 0.000 6.94 0.00 180.0 4/21/2025 10:01 0.1125.82917.363 10.367 23.20737.529 1.787 7.544 0.4970.0001.613 0.000 0.0970.783 0.279 833.00.980.488 0.000 5.94 0.00 180.0 4/21/2025 10:02 0.5855.08617.405 10.400 19.84641.201 1.536 7.622 0.5650.0001.529 0.000 0.0780.581 0.274 833.01.050.642 0.000 5.67 0.00 180.0 4/21/2025 10:03 0.5165.83017.443 10.403 20.99337.986 1.718 6.814 0.6020.0001.606 0.000 0.2290.736 0.270 833.01.210.656 0.000 6.35 0.00 180.0 4/21/2025 10:04 0.0008.20717.465 10.397 17.85439.667 1.756 8.710 0.4530.0001.475 0.000 0.1151.020 0.263 833.01.170.789 0.000 8.21 0.00 180.0 4/21/2025 10:05 0.2784.54317.411 10.347 18.71729.562 0.645 6.362 0.4470.0002.878 0.000 0.2611.040 0.288 833.01.260.637 0.000 4.82 0.00 179.0 4/21/2025 10:06 1.1023.95017.401 10.426 29.30526.042 0.110 4.283 0.9680.0043.915 0.000 0.1680.493 0.247 833.01.260.896 0.000 5.05 0.00 179.0 4/21/2025 10:08 1.1094.14617.445 10.474 32.10039.439 0.650 6.779 0.6960.0242.671 0.000 0.1630.683 0.316 833.01.280.721 0.000 5.25 0.00 180.0 4/21/2025 10:09 1.2395.37617.457 10.400 26.76334.388 1.662 7.604 0.7820.0001.872 0.000 0.1900.763 0.268 833.01.441.079 0.000 6.62 0.00 180.0 4/21/2025 10:10 0.3413.64417.465 10.417 22.94045.486 0.985 8.348 0.6320.0032.982 0.000 0.1391.003 0.274 833.01.120.650 0.000 3.98 0.00 180.0 4/21/2025 10:11 1.8454.15317.465 10.441 21.93743.049 1.215 8.863 0.7060.0022.649 0.000 0.1700.756 0.271 833.01.250.805 0.000 6.00 0.00 180.0 4/21/2025 10:12 0.9593.95817.503 10.372 20.60627.306 0.750 6.645 0.7050.0003.341 0.000 0.1510.741 0.258 833.01.240.854 0.000 4.92 0.00 180.0 4/21/2025 10:13 1.3453.78817.511 10.379 27.76532.980 0.658 6.415 0.7910.0003.243 0.000 0.2180.664 0.275 833.01.250.720 0.000 5.13 0.00 180.0 4/21/2025 10:14 0.6525.59317.487 10.410 16.45821.088 1.110 6.323 0.5140.0232.861 0.000 0.1230.677 0.278 833.01.100.627 0.000 6.24 0.00 180.0 4/21/2025 10:15 0.4265.32717.428 10.392 20.09134.826 0.773 5.384 0.5290.0001.506 0.000 0.2090.801 0.292 833.01.350.833 0.000 5.75 0.00 180.0 4/21/2025 10:16 0.6735.20717.464 10.333 26.76848.822 1.134 7.812 0.8470.0001.699 0.000 0.2850.790 0.295 833.01.390.775 0.000 5.88 0.00 180.0 4/21/2025 10:17 0.1394.57917.453 10.389 27.85347.453 1.121 7.079 0.6100.0001.643 0.000 0.1240.791 0.322 833.01.260.745 0.000 4.72 0.00 180.0 4/21/2025 10:18 0.6565.80017.428 10.404 19.56236.494 1.953 8.670 0.4860.0001.304 0.000 0.1390.748 0.329 833.01.250.684 0.000 6.46 0.00 180.0 4/21/2025 10:19 0.9665.51317.431 10.364 27.28838.606 1.020 5.597 0.8510.0001.402 0.000 0.2910.605 0.287 833.01.430.842 0.000 6.48 0.00 180.0 4/21/2025 10:20 0.2055.75617.441 10.355 21.20639.692 1.517 7.603 0.6990.0001.332 0.000 0.1880.857 0.272 833.01.320.885 0.000 5.96 0.00 180.0 4/21/2025 10:21 1.0205.01717.469 10.363 24.92838.387 1.366 6.752 0.7060.0001.448 0.000 0.2170.402 0.283 833.01.320.810 0.000 6.04 0.00 180.0 4/21/2025 10:22 1.2834.50917.472 10.388 30.29047.091 1.269 7.409 0.7170.0001.085 0.000 0.0680.720 0.320 833.01.190.718 0.000 5.79 0.00 180.0 4/21/2025 10:23 1.0334.60717.503 10.409 40.45035.599 0.787 5.438 1.0590.0031.470 0.000 0.2460.579 0.309 833.01.370.764 0.000 5.64 0.00 180.0 4/21/2025 10:24 1.4175.38017.455 10.322 37.70034.415 1.223 7.263 0.9830.0001.981 0.000 0.2600.654 0.306 833.01.420.829 0.000 6.80 0.00 180.0 4/21/2025 10:25 1.1796.36817.423 10.337 21.51235.921 2.405 10.525 0.6520.0001.231 0.000 0.1030.771 0.296 833.01.240.822 0.000 7.55 0.00 179.0 4/21/2025 10:26 0.0005.14917.467 10.400 16.23627.980 1.630 6.885 0.2830.0031.133 0.000 0.1150.875 0.292 833.01.190.738 0.000 5.15 0.00 180.0 4/21/2025 10:27 1.6275.65117.489 10.372 19.63836.267 1.138 6.238 0.6320.0031.080 0.000 0.1170.602 0.300 833.01.260.814 0.000 7.28 0.00 180.0 4/21/2025 10:28 1.1064.90417.461 10.357 29.01442.836 0.793 5.478 0.8030.0001.485 0.000 0.2290.760 0.325 833.01.490.915 0.000 6.01 0.00 180.0 4/21/2025 10:29 1.0795.01217.479 10.353 27.81047.985 1.472 9.077 0.8700.0001.223 0.000 0.1690.441 0.347 833.01.470.906 0.000 6.09 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 10:30 0.7114.60217.464 10.382 20.84763.578 2.015 12.563 0.6360.0090.824 0.000 0.1240.742 0.323 833.01.190.630 0.000 5.31 0.00 180.0 0.8255.10917.446 10.382 24.60538.218 1.263 7.253 0.6880.0031.873 0.000 0.1740.731 0.291 833.001.2690.772 0.000 5.934 0.000 179.9Avg. Spike 3 4/21/2025 10:32 1.42127.14215.897 9.802 20.82499.966 1.506 8.920 0.5740.0001.614 0.944 22.2630.427 0.380 833.024.290.950 0.856 28.56 0.00 179.0 Run 3 - B 30minute/60min 4/21/2025 10:34 1.4103.09317.437 10.385 29.11851.263 0.547 8.582 1.1430.0013.047 0.000 0.3680.824 0.365 833.01.600.747 0.001 4.50 0.00 180.0 4/21/2025 10:35 0.2785.68117.433 10.415 22.69552.516 1.643 9.341 0.5920.0001.030 0.000 0.1840.763 0.366 833.01.430.779 0.000 5.96 0.00 180.0 4/21/2025 10:36 1.3292.19117.499 10.395 32.17743.652 0.191 6.221 0.8600.0004.262 0.000 0.1170.769 0.340 833.01.380.876 0.000 3.52 0.00 180.0 4/21/2025 10:37 1.3582.83717.522 10.446 29.83446.414 0.671 8.560 0.9740.0002.827 0.000 0.1700.742 0.341 833.01.581.092 0.000 4.19 0.00 180.0 4/21/2025 10:38 1.3294.33117.423 10.425 23.21747.038 1.882 9.873 0.7660.0001.170 0.000 0.1600.672 0.329 833.01.300.727 0.000 5.66 0.00 180.0 4/21/2025 10:39 1.3925.57017.368 10.361 24.24549.203 1.700 9.287 0.7930.0001.223 0.000 0.1530.843 0.347 833.01.350.750 0.000 6.96 0.00 179.0 4/21/2025 10:40 1.6305.75517.394 10.418 24.12838.149 1.276 7.207 0.7030.0001.025 0.000 0.1120.824 0.399 833.01.460.821 0.000 7.38 0.00 180.0 4/21/2025 10:41 1.1255.17917.377 10.418 24.68240.417 1.467 7.931 0.7830.0000.949 0.000 0.0640.795 0.370 833.01.260.691 0.000 6.30 0.00 180.0 4/21/2025 10:42 1.1535.03517.396 10.386 29.20234.536 1.248 6.464 0.8380.0001.305 0.000 0.1380.698 0.395 833.01.520.890 0.000 6.19 0.00 180.0 4/21/2025 10:43 0.7946.95517.404 10.403 20.03136.100 2.489 10.596 0.3310.0000.935 0.000 0.0910.418 0.425 833.01.260.478 0.000 7.75 0.00 180.0 4/21/2025 10:44 1.0665.55017.392 10.406 18.98238.301 1.504 7.685 0.5040.0000.864 0.000 0.0600.672 0.392 833.01.260.630 0.000 6.62 0.00 180.0 4/21/2025 10:45 0.5722.05717.382 10.381 27.91641.450 0.037 6.143 0.6300.0003.786 0.000 0.1190.894 0.420 833.01.460.746 0.000 2.63 0.00 180.0 4/21/2025 10:46 1.2853.10317.395 10.371 26.93336.744 0.783 7.491 0.7510.0002.699 0.000 0.1320.880 0.418 833.01.450.729 0.000 4.39 0.00 179.0 4/21/2025 10:47 1.6312.61817.392 10.403 25.39242.031 0.843 8.504 0.6890.0002.329 0.000 0.2050.697 0.402 833.01.530.778 0.000 4.25 0.00 180.0 4/21/2025 10:48 0.3444.83217.391 10.415 24.01644.771 1.205 7.231 0.5630.0000.711 0.000 0.1670.853 0.419 833.01.440.650 0.000 5.18 0.00 180.0 4/21/2025 10:50 1.3981.86717.370 10.391 31.74434.531 0.661 7.226 0.9030.0002.330 0.000 0.1950.774 0.409 833.01.640.935 0.000 3.27 0.00 180.0 4/21/2025 10:51 1.1032.67517.351 10.378 23.78343.985 1.343 11.122 0.7260.0002.688 0.000 0.1340.451 0.365 833.01.420.838 0.000 3.78 0.00 180.0 4/21/2025 10:52 0.0002.31817.351 10.399 24.22433.711 0.464 6.727 0.4790.0003.894 0.000 0.0190.683 0.326 833.01.160.735 0.000 2.32 0.00 180.0 4/21/2025 10:53 1.2765.70317.382 10.398 28.13726.814 1.894 6.081 0.7700.0001.124 0.000 0.2140.915 0.396 833.01.450.665 0.000 6.98 0.00 180.0 4/21/2025 10:54 0.8574.84117.368 10.400 22.25233.550 1.046 5.502 0.6730.0011.082 0.000 0.2450.682 0.365 833.01.550.856 0.000 5.70 0.00 180.0 4/21/2025 10:55 0.5495.45017.373 10.388 20.42729.056 1.813 6.753 0.6140.0000.757 0.000 0.2620.846 0.358 833.01.490.763 0.000 6.00 0.00 180.0 4/21/2025 10:56 0.6904.83917.438 10.363 19.83330.018 1.702 6.419 0.6310.0021.110 0.000 0.3550.872 0.322 833.01.590.882 0.000 5.53 0.00 180.0 4/21/2025 10:57 0.3166.11217.392 10.381 16.39638.200 1.397 6.919 0.5590.0001.001 0.000 0.3600.900 0.370 833.01.590.733 0.000 6.43 0.00 180.0 4/21/2025 10:58 0.5565.18417.400 10.412 19.98046.323 1.246 6.901 0.5220.0000.781 0.000 0.3750.562 0.357 833.01.700.908 0.000 5.74 0.00 180.0 4/21/2025 10:59 0.5201.51817.432 10.387 22.14259.885 0.763 9.341 0.5850.0002.265 0.000 0.3560.771 0.342 833.01.570.797 0.000 2.04 0.00 180.0 4/21/2025 11:00 0.3081.48717.436 10.392 20.09350.583 0.619 9.326 0.5130.0002.259 0.000 0.2890.859 0.363 833.01.570.834 0.000 1.80 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 11:01 1.2944.12617.365 10.403 35.22344.221 1.013 6.091 0.7710.0001.026 0.000 0.3330.430 0.365 833.01.680.925 0.000 5.42 0.00 180.0 4/21/2025 11:02 1.0575.23817.367 10.393 23.88150.800 1.677 10.668 0.7710.0000.882 0.000 0.3330.696 0.364 833.01.741.018 0.000 6.29 0.00 180.0 4/21/2025 11:03 0.9384.64517.380 10.392 23.76447.937 1.480 8.874 0.6340.0000.795 0.000 0.3500.667 0.337 833.01.600.864 0.000 5.58 0.00 180.0 4/21/2025 11:04 0.1233.05417.324 10.415 24.72445.416 0.805 8.432 0.7380.0002.083 0.000 0.3860.782 0.355 833.01.761.003 0.000 3.18 0.00 180.0 0.9234.12817.398 10.397 24.63941.921 1.180 7.917 0.6940.0001.741 0.000 0.2150.741 0.371 833.001.4930.805 0.000 5.051 0.000 179.9Avg. 0.8744.61917.422 10.390 24.62240.069 1.222 7.585 0.6910.0021.807 0.000 0.1940.736 0.331 833.001.3810.788 0.000 5.493 0.000 179.9Run 3 Avg: Baseline 3 4/21/2025 11:06 0.0000.0000.048 0.053 0.0000.616 0.002 0.544 0.0000.0020.000 0.000 0.4790.000 0.046 833.00.920.518 0.000 0.00 0.00 180.0 Post CTS 4/21/2025 11:08 0.0000.8860.032 0.052 0.0000.437 0.020 0.162 0.0000.0000.000 96.996 0.0000.000 0.179 833.065.130.161 0.026 0.89 0.00 180.0 4/21/2025 11:08 0.0000.0000.031 0.053 0.0000.329 0.001 0.209 0.3240.0000.000 97.637 0.0000.268 0.173 833.065.700.381 0.021 0.00 0.00 180.0 4/21/2025 11:08 0.0000.1690.021 0.046 0.0000.405 0.000 0.182 0.0000.0000.000 97.815 0.0000.104 0.198 833.065.660.077 0.013 0.17 0.00 180.0 Post NO2/Mid O2 4/21/2025 11:10 98.5633.5860.014 0.039 0.0000.464 0.990 0.181 0.0000.0000.000 0.000 0.2020.456 0.111 833.00.500.113 0.000 102.15 10.37 180.0 4/21/2025 11:10 99.5153.4380.010 0.023 0.4790.602 1.005 0.154 0.2290.0270.000 0.000 0.4930.344 0.018 833.00.610.127 0.000 102.95 10.30 179.0 4/21/2025 11:10 99.5774.0490.012 0.046 0.0200.508 0.986 0.189 0.1630.0000.000 0.000 0.5030.000 0.031 833.01.090.792 0.000 103.63 10.38 179.0 Post 5-Gas 4/21/2025 11:11 0.000245.4350.011 4.884 3.845481.990 1.724 2.280 0.9290.0360.292 1.187 250.3760.488 0.875 833.0254.552.451 9.676 245.43 0.00 180.0 4/21/2025 11:11 0.000245.8850.013 4.878 1.262485.911 1.795 2.125 0.1770.0880.758 1.119 251.0010.269 0.959 833.0255.172.257 9.706 245.89 0.00 180.0 4/21/2025 11:11 0.000246.4920.009 4.884 4.699482.850 1.673 2.402 0.6670.0740.000 1.054 251.3080.175 0.862 833.0255.522.682 9.741 246.49 0.00 180.0 4/21/2025 11:12 0.000247.1890.007 4.908 5.022485.148 1.638 2.126 0.3630.0970.000 1.075 251.8680.439 0.936 833.0256.663.304 9.743 247.19 0.00 180.0 4/21/2025 11:12 0.000246.611-0.000 4.928 5.898482.872 1.611 2.437 1.4480.0130.781 1.036 251.8360.000 0.794 833.0256.533.618 9.742 246.61 0.00 180.0 4/21/2025 11:12 0.000246.5000.001 4.964 4.537483.967 1.680 2.189 1.2260.0190.000 1.144 252.1040.000 0.915 833.0256.993.445 9.750 246.50 0.00 180.0 End of Test Purge 4/21/2025 11:14 0.0001.3710.008 0.032 0.0001.386 0.000 0.216 0.0000.0000.000 0.000 1.0740.319 0.009 833.01.650.832 0.009 1.37 0.00 180.0 4/21/2025 11:14 0.0000.5980.014 0.017 0.2611.319 0.000 0.040 0.0000.0000.000 0.000 1.0720.000 0.045 833.01.720.845 0.000 0.60 0.00 179.0 4/21/2025 11:14 0.0000.6230.004 0.028 0.0000.903 0.000 0.000 0.3160.0000.000 0.000 0.7960.000 0.079 833.01.350.591 0.000 0.62 0.00 180.0 4/21/2025 11:14 0.0000.2730.006 0.027 0.0001.097 0.000 0.084 0.0000.0000.000 0.000 0.6810.000 0.051 833.01.180.603 0.000 0.27 0.00 180.0 4/21/2025 11:14 0.0000.7090.006 0.016 0.2090.854 0.000 0.132 0.2570.0000.000 0.000 0.5360.000 0.082 833.01.090.589 0.000 0.71 0.00 180.0 4/21/2025 11:14 0.0000.000-0.000 0.020 0.0000.552 0.023 0.040 0.0000.0830.000 0.000 0.7200.000 0.037 833.01.110.471 0.000 0.00 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/21/2025 11:14 0.0000.3670.004 0.042 0.0001.287 0.032 0.273 0.0000.0000.000 0.000 0.4360.000 0.150 833.01.010.410 0.000 0.37 0.00 180.0 4/21/2025 11:14 0.0000.0950.022 0.045 0.0000.650 0.000 0.163 0.0280.0070.273 0.000 0.6050.000 0.099 833.00.970.252 0.000 0.09 0.00 180.0 4/21/2025 11:14 0.0000.0000.010 0.040 0.0790.778 0.007 0.023 0.0000.0000.000 0.000 0.7600.000 0.000 833.01.080.480 0.000 0.00 0.00 180.0 GAS Performance Test Report Test Type: Annual Test Date: 4/23/2025 Waukesha 9394 GSI Rich Burn (4 Cycle) 303 W. 3rd St Elk City , OK 73644(580) 225-0403 Test Started:Test Completed:07:27 AM 10:57 AM Source: Unit Number: 1455 Serial Number: 1658743 Engine Hours:12448 Permit #: #DAQE-AN161680001-23 Location: Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, Inc. Residue Booster Station 40 CFR Part 60 Subpart JJJJ CO NOx NMNEHC 2.414 8.453 1.736 2.000 0.300 1.000 0.150 0.700 0.030 0.007 0.042 0.008 Pass Pass Pass Pass Pass Pass Federal State Federal State Federal State Results ppmvd Results g/hp-hr Permit g/hp-hr PASS ALL Index Tables Figures Appendices Table 5.1 (Run Summaries)................................................................ Table 6.1 (Volumetric Flow Rate Data)............................................... Table 6.2 (Stack Gas Measurements)................................................. Table 8.1 (Oxygen Calibration)........................................................... Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... Annex Table 1.2.2 (Measurement System Capabilities)..................... Annex Table 1.3.1 (Test Specific Target Analytes)............................. Annex Table 4.1 (Measure System Capabilities)................................ Figure 6.1 (Location of Traverse Points per Method 1)....................... Annex Figure 1.4.1 (Sampling Train).................................................. Annex Figure 1.4.2 (Sampling Points)................................................. Annex Figure 1.4.3 (Sampling Port Locations).................................... Certified Calibration Bottle Certificates................................................ Tri Probe Certification via GD-031...................................................... GAS ALT 141_FTIR EPA.................................................................... Tester Qualifications (resume)............................................................ Raw Data............................................................................................ 27 Key Personnel.............................................................................1.0 3 Sampling System........................................................................2.0 3 Methods Used.............................................................................3.0 3 Test Summaries..........................................................................4.0 5 Run Summaries..........................................................................5.0 6 6 Volumetric Flow Rate Data.........................................................6.0 7 7 7 7 Calculations................................................................................7.0 8 9 12 12 13 15 13 14 14 20 25 28 29 Oxygen Calibration.....................................................................9 Engine Parameter Data Sheet....................................................10 QA/QC Results............................................................................11 Signature Page...........................................................................12.0 Appendices.................................................................................13.0 Bottle Certs.................................................................................2014.0 Tri Probe Certification via GD-031..............................................2515.0 GAS ALT 141_FTIR EPA............................................................16.0 Tester Qualifications (resume)....................................................2817.0 D6348 Annexes..........................................................................1211.0 18 19 26 8.0 9.0 10.0 Raw Data....................................................................................2918.0 1.0 Key Personnel GAS Crusoe Energy Systems, Inc. 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A EPA Method 2 & 2C EPA Method 3A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. ASTM D6348-03 Jason Woolley 3 Cooper Green GAS 4.0 Test Summary T e s t S u m m a r y Site Verification Photos GAS Unit 1455 with a serial number of 1658743 which is a Waukesha 9394 GSI engine located at Residue Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/23/2025 by Cooper Green with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2067 BHP and 1199 RPM which is 82.67% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1455 is authorized to operate under permit #DAQE-AN161680001-23. 4 4.0 Test Summary Engine/Compressor Specs Residue Booster StationLocation 1455Unit ID Make Waukesha Site Elevation ft.5455 Model 9394 GSI Atmospheric Pressure psi.11.98 Serial Number 1658743 Stack Diameter in.20 mfg. rated hp 2500 Yes 1200 Date of Manufacture Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1 Test Horsepower 2050 2075 2075 2067 1199 1200 1198 1199 Percent Load % Intake Manifold Pressure (hg) 82.00%83.00%83.00%82.67% 95.73 96.96 96.75 96.48 Intake Manifold Temperature (F)117.50 118.80 119.70 118.67 Ambient Conditions Ambient Temperature Dry (F)46.00 52.00 58.00 52.00 Exhaust Flow Data Q Stack (dscfh) Q Stack (dscm/hr) 193537.30 190270.45 189946.94 191251.56 5480.31 5387.81 5378.65 5415.59 Moisture Fraction Bws Fuel Consumption (Btu/h[-hr) 0.17 0.17 0.17 0.17 0 0 0 0 Fuel Flow (dscfh) Fuel (btu/scf)1020 1020 1020 1020 O2 F factor 8710.0 8710 8710 8710 Results Method 3A Corrected O2% Dry Moisture %17.46%17.39%17.36%17.41% T e s t S u m m a r y mfg. rated rpm Test RPM 0.01%0.00%0.00%0.00% Permitted Standards Results 5 Catalyst Run 1 Run 2 Run 3 3 Run Average Pass Permits 07:27 AM 08:35 AM 09:44 AM 4/23/2025 State NOx (mol wt) 46.01 0.933 1.609 1.761 1.434NMNEHC (ppmvw) 1.130 1.948 2.131 1.736NMNEHC (ppmvd) NMNEHC (mol wt) 44.10 319.192 549.968 601.579 490.246 FailNMNEHC (ppbvd) @15% O2 0.006 0.009 0.010 0.0080.700 0.030 PassNMNEHC (g/hp-hr) 0.319 0.550 0.602 0.490 FailNMNEHC (ppmvd) @15% O2 0.0060.009CO (g/hp-hr)0.007 0.0072.000 0.300 Pass CO (ppmvw)1.778 2.514 1.692 1.994 CO (ppmvd)2.154 3.043 2.047 2.414 CO (mol wt) 28.01 CO (ppmvd) @15% O2 0.608 0.859 0.578 0.682 Fail CO (ppbvd) @15% O2 608.106 859.132 577.837 681.692 Fail NOx (g/hp-hr)0.056 0.046 0.026 0.0421.000 0.150 Pass NOx (ppmvw)9.016 7.630 4.297 6.981 NOx (ppmvd)10.924 9.236 5.199 8.453 NOx (ppbvd) @15% O2 3084.492 2607.817 1467.737 2386.682 Fail NOx (ppmvd) @15% O2 3.084 2.608 1.468 2.387 Fail GAS GAS 5.0 Run Summaries Summary Source Run 1 R u n Table 5.1 Run Summaries S u m m a r i e s 6 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture % 1.78 0.28 8.71 0.30 9.02 0.00% 0.00% 0.00% 17.46% 9.12 0.22 0.00%17.46% 29.20 0.28 0.00%16.07% 8.31 0.39 0.00%17.46% 0.12 0.00 0.12 0.00%0.05% Avg. Wet NO Summary Source Run 2 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 0.23 0.12 0.00 0.12 0.00%0.05% 3.59 8.30 1.01 9.32 0.00%17.40% 49.83 25.92 0.75 26.67 0.00%15.87% 1.44 5.09 0.85 5.94 0.00%17.39% 0.17 0.01 0.00 0.01 0.00%0.05% Avg. Wet 2.51 6.70 0.93 7.63 1.61 0.00%17.39% NO2NO 0.77 1.42 25.24 1.80 0.74 Summary Source Run 3 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 1.62 3.06 0.39 3.45 0.00%17.34% 51.42 29.68 0.23 29.91 0.00%15.75% 1.76 4.50 0.64 5.14 0.00%17.38% 0.00 0.17 0.00 0.17 0.00%0.02% 0.17 0.01 0.00 0.01 0.74 0.00%0.05% Avg. Wet 1.69 3.78 0.51 4.30 1.76 0.00%17.36% NO2NO 0.75 1.85 25.66 1.68 NMNEHC 0.63 NO2 0.000.23 0.89 25.10 0.97 0.77 0.93 0.28 9.34 29.48 8.69 2.00 1.56 0.23 51.17 6.0 Volumetric Flow Rate Data Volumetric Flow Rate Data .99 Table 6.1. Data used for volumetric flow rate (Method 2) Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet Run 1 Average Pitot Tube Coefficient Cp(std)= H2O CO2 O2 CO Molecular Weight Stack Gas dry basis (Md) Molecular Weight Stack Gas wet basis (Ms) Stack Static Pressure (Pg) Stack Static Pressure (Pg) Atmospheric Pressure at Location (Pbar) Atmospheric Pressure at Location (Pbar) Absolute Stack Pressure (Ps) Stack Temperature Stack Temperature Stack Temperature Stack Gas Velocity Stack Flow Rate Q Stack Gas Wet Volmetric Flow Rate Stack Gas Dry Volumetric Flow Rate Sample after Back Purge: Within 5% of Last Δpstd reading: Stack Diameter (inches) Inches upstream from disturbance Inches downstream from disturbance scf/hr 0.63 Yes 20.00 5.00 32.00 scf/hr cfs ft/sec Deg R Deg F Deg C "Hg "Hg MBAR "Hg "H20 g/g mole g/g mole %d %d %d %17.46 30.01 0.50 Inches 3.34 10 16.66 Vo l u m e t r i c F l o w Ra tes Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 Figure 6.1 16 Traverse Points Were Used Emissions Sampling Points - 3 point long line sampling probe First Sampling Point Taken @ 16.7% of Stack Diameter Second Sampling Point Taken @ 50% of Stack Diameter Third Sampling Point Taken @ 83.3% of Stack Diameter 12.58 0.01 0.00 1010.84 0.04 29.86 29.90 881.25 1340.92 471.81 27.91 75.86 165.53 234482.66 193537.30 Run 2 17.39 30.01 0.54 12.57 0.00 0.00 1010.16 0.04 29.84 29.88 904.31 1363.98 484.62 27.92 79.85 165.50 230332.11 190270.45 Run 3 17.36 30.02 0.55 12.62 0.00 0.00 1009.48 0.04 29.82 29.86 906.25 1365.92 485.69 27.93 80.28 165.50 229851.44 189946.94 17.41 30.01 0.53 12.59 0.00 0.00 1010.16 0.04 29.84 29.88 897.27 1356.94 480.71 27.92 78.67 165.50 231555.41 191251.56 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets. * Cyclonic Flow Check (Pass/Fail): PASS Δpstd (in) H2O 0.52 Exhaust Temp F 881.00 Pitot Tube Sampling Points (Velocity) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Δpstd Average= Run 1 Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate 0.56 0.59 0.61 881.00 881.00 882.00 0.55 0.53 0.48 881.00 881.00 881.00 0.48 0.53 0.47 882.00 882.00 881.00 0.45 881.00 0.42 0.40 0.43 881.00 882.00 881.00 0.49 0.52 0.50 881.00 881.00 881.25 Δpstd = Velocity head measured by the standard pitot tube, (in.) H2O.Run 3 Δpstd (in) H2O 0.45 Exhaust Temp F 906.00 0.44 0.48 0.50 906.00 906.00 907.00 0.50 0.48 0.55 906.00 906.00 906.00 0.55 0.57 0.58 907.00 907.00 906.00 0.59 906.00 0.62 0.62 0.60 906.00 907.00 906.00 0.63 0.63 906.00 906.00 906.250.55 Run 2 Δpstd (in) H2O 0.53 Exhaust Temp F 904.00 0.47 0.48 0.43 905.00 904.00 904.00 0.47 0.51 0.56 904.00 905.00 904.00 0.56 0.58 0.56 905.00 904.00 904.00 0.58 904.00 0.59 0.58 0.59 905.00 904.00 904.00 0.62 0.60 904.00 905.00 0.54 904.31 Pass Strat Check 10.323Check 1 10.400Check 2 10.401Check 3 CO2Gas Used Pass/Fail 7 GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate *Note- Use of this method negates the need for any fuel related numbers for emissions calculations Nomenclature Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293°K (528 °R). Vs = Average stack gas velocity, m/sec (ft./sec). *(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1 Md = .44(12.577)+ .32(.005)+ .28(87.418+0) = 30.01 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO) 12.5 Molecular Weight of Stack Gas. Equation 2-6 Ms = 30.01(1 -.17462)+ 18.0(.17462) = 27.91 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws) 12.6 Average Stack Gas Velocity. Equation 2-7 Vs = 85.49*.99*√.5*√(1340.92/(29.9*27.91)) = 75.86 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms)) 12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8 Qsd = 3600(1-.17462)75.86*2.182((528*29.9)/ (1340.92*29.92)) = 193537.3 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd)) *Standard conversion from feet to meters Q = 193537.298/35.315 = 5480.314 DSCM/HRQ = Qsd/35.315 Emission Rates (Examples use CO Run 1) Nomenclature CO corrected @ 15% O2 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ER = Emission rate of (CO) in g/HP-hr. F(d )= Volumes of combustion components per unit of heat content, scm/J (scf/million Btu). Q = Stack gas volumetric flow rate, in standard cubic meters per hour, dry basis LB/HR.= Emission rate of (CO) in LB/HR. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) O2 = Concentration of oxygen on a dry basis, percent. ppm= Parts Per Million (CO) ppm@15% O2= PPM corrected to 15% O2 Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (DSCF/HR.). Run Time = Run Time in Minutes TPY= Tons per Year Mol wt.= Mol Weight of CO (28.01) Vs = Average stack gas velocity, m/sec (ft./sec). ppm @ 15% O2 = 2.154*(20.9-15)/(20.9-.01%)) = .608 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2)) G/HP HR from 40 CFR Part 60 Subpart JJJJ (2.154*(1.164*10^-3)*5480.314*(Run Time/60))/2050 = .007 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR LB/HR from Grams LB/HR = .007*1/453.6*2050 = .03 LB/HRlb/hr = ER*1/453.6*BHP-HR TPY TPY = .03*4.38 = .131 TPYTPY = LB/HR. *4.38 Horsepower HP Provided On Site Wet to Dry PPM 2.15 = 1.7775*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry 8 Cp(std) = Standard pitot tube coefficient; use 0.99 GAS 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span. 8.0 Oxygen Calibration 8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases. (1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration EPA Method 3A QA Worksheet (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Certified Gas Concentraion Low-Level (%) 0.00% Certified Gas Concentraion Mid-Level (%) Certified Gas Concentraion High-Level (%) (DIRECT) Analyzer Calibration Error (≤ 2%) Certified Concentration Value (%) Direct Calibration Response (%) Absolute Difference (%) Analyzer Calibration Error (%)Analyzer Direct Calibration Response Certified bottle value % 0.00% 0.00% 0.00% Zero Gas % Mid-Level Gas % High-Level Gas % Bias Pre Initial Value Bias Post Inital Values System Calibrations Response Pre (%) 0.00% System Bias (% of Span) Pre System Calibration Response Post (%) System Bias (% of Span) Post Drift (% of Span) 0.00%0.00%0.00%0.00% (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Avg. Gas Concentration (Run 1) Avg. Gas Concentration (Run 2) Avg. Gas Concentration (Run 3) Effluent Gas (Cgas) Run 1 Effluent Gas (Cgas) Run 2 Effluent Gas (Cgas) Run 3 Linearity Check 0.00%0.00%0.00% Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Upscale Gas Analyzer Calibration Response (%) Zero Gas Upscale Gas EPA Method 3A QA Worksheet Zero Gas Mid-Level Gas High-Level Gas 100% Nitrogen O2 QA/QC Zero Gas %0.00% Mid-Level Gas % High-Level Gas % System Calibration Response Pre (%) System Calibration Response Post (%) Zero Gas % Upscale Cal Zero Gas % Upscale Cal Upscale Used Upscale Used 10.58% 20.83% 10.57% 10.52% 10.73% 10.73% 10.52%10.57% 10.58% 20.83% 10.73% 21.04% 10.73% 21.04% 10.73%21.04% 0.00% 10.73% 21.04% 0.15% 0.21% 0.71% 1.01% 10.73% Span Zero Offset 0.00% 21.04 0.00% 10.58%0.03%0.29%0.00% 0.01% 0.00% 0.00% 0.01% 0.00% 0.00% 9 GAS 1020.0 1018.0 1016.3 1060.0 1056.0 1054.3 5.6 5.6 5.6 9.0 Engine Parameter Data Sheet Company Site Elevation (ft) Facility Unit ID Date Make Crusoe Energy Systems, Inc. Residue Booster Station 4/23/2025 5455 1455 Waukesha Model Serial Number 9394 GSI 1658743 Technician Cooper Green Run Start Times 07:27 AM 08:35 AM 09:44 AM 10:57 AM Run 1 Run 2 Run 3 Completed Engine Parameter Data Run 1 Engine Speed (RPM)1199.0 1200.0 1198.0 1199.0 Engine Hours 12445 12446 12447 12448 Intake Manifold Pressure (psi)59.0 59.6 59.5 59.4 Intake Manifold Temp °F 117.5 118.8 119.7 118.7 Engine Load (BHP)2050.0 2075.0 2075.0 2066.7 Ambient Temp °F 46.0 52.0 58.0 52.0 Humidity %34.0 25.0 19.0 26.0 Dew Point °F 19.0 18.0 16.0 17.7 Yes 2 2 2 2# of Catalyst Installed Catalyst (Yes or No) AFR Setting (Target Left Bank) AFR Setting (Target Right Bank) AFR Manufacturer/Type 10 Run 3 AverageRun 2 Discharge Pressure (psi) Suction Pressure (psi) 1011.0 1047.0 5.6Catalyst Pressure Drop H2O Catalyst Outlet Temp °F Catalyst Inlet Temp °F GAS Waukesha Waukesha Waukesha Waukesha 10.0 QA/QC Results Average:Carbon monoxide CO Gas, Inc. 0.00 R e s u l t s Average:Nitrogen monoxide NO 0.00 Average:Nitrogen dioxide NO2 0.01 Average:NOx 0.01 Average:VOC 0.04 Average:Oxygen 0.00 Pre-test Baseline Results Time: Q A / Q C Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 99.02 Tolerance 2.00% Difference between measured and expected 0.98% CTS Direct to Analyzer Time: Average:Carbon monoxide CO 0.43 Average:Nitrogen monoxide NO 0.14 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.14 Average:VOC 0.62 Average:Oxygen 0.00 Pre-test System Zero Time: Mechanical Response Time 45 seconds Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.41 Tolerance 5.00% Difference between measured and expected 1.59% Pre-test System CTS & Mechanical Response Time 75 secondsEquilibration Response Time Value:Spike Reported 251.70 Value:Spike Expected 253.10 System (Equilibration) Response Time Target (Spike) 45 secondsSystem Zero Response Time 75 secondsSystem Response Time System (Zero) Response Time 11 11.0 D6348 Annexes 1-8 D6348 Annexes 1. Test Plan Requirements Annex 1.2 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration NO2 Ethylene SF6 O2 (%) CC524639 12/30/2027 103.00 10.73% CC252676 10/17/2032 100.00 CC433538 8/5/2032 21.04% Cylinder # SG9132842BAL Expiration: 8-20-2032 Propane CO NO SF6 Bottle Value 253.10 497.30 252.90 9.95 Analyzer System Response 251.70 489.12 246.88 9.74 Percent Difference 0.55%1.65%2.38%2.15% Annex Table 1.2.2 Measurement System Capabilities SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 99.024 4.951 Spike Direct Propane 252.068 Mechanical Response Time SF6 9.789 CO 491.628 NO 248.703 Ethylene 98.415 40 seconds Analyzer Response Propane 251.704 SF6 9.740 CO 489.116 NO 246.876 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 251.165 CO 480.713 NO 245.396 75 seconds 13 seconds 9.20% 9.04% 9.16% 99.42% 99.86% 99.92% 9.730 12 GAS Annex 1.3 Compounds Infrared Analysis Region (cm-1) Expected Concentration Range Measurement System Achievable Minimum Detectable Concentrations Required Measurement System Accuracy and Precision for Test Application CO 2000-2200 0-1200 ppm NO 1875-2138 NO2 2700-2950 VOC 2600-3200 910-1150 2550-2950 CH2O 2550-2850 Interfering Compounds * CO is analyzed in a separate analysis region than CO2 and H2O CO2 Water Vapor 926-1150 3200-3401 Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives 0.16267 ppm 4 ppm 0-1000 ppm 0.4007 ppm 2 ppm 0-100 ppm 0.4899 ppm 2 ppm 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC 0-100 ppm 0.7878 ppm 1 ppm 0-10% 0-22% 0% 0.20% n/a n/a * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. Annex 1.4 Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 13 GAS Sampling Point Locations in Inches 16.7%3.340 50%10.000 83.3%16.660 Figure Annex 1.4.3 Sample Port Location Figure Annex 1.4.2 Sampling Points Interior Stack Diameter (inches): Inches Upstream: Inches Downstream: 20 5 32 14 Stack Gas Dry Volumetric Flow Rate (scf/hr): 191251.56 H2O%d @ Sampling Point:17.41 CO2%d @ Sampling Point:12.59 Pressure @ Sampling Point (Pg "H2O):0.53 Temperature @ Sampling Point (Deg F):897.27 GAS D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1) Target Analyte Results (ppm) CO 0.1627 NO 0.4007 NO2 0.4899 Ethylene 0.3782 Propane 0.4351 Hexane 0.2233 Acetaldehyde 0.8152 Formaldehyde 0.7878 D6348 Annex 3. FTIR Reference Spectra Calibration Transfer Standard Expected Measured Path Length Validated Ethylene 100 99.02 4.951 Passed D6348 Annex 4. Required Pre-Test Procedures Annex Table 1.2.2 Measurement System Capabilities 15 SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 99.024 4.951 Spike Direct Propane 252.068 Mechanical Response Time SF6 9.789 CO 491.628 NO 248.703 Ethylene 98.415 40 seconds Analyzer Response Propane 251.704 SF6 9.740 CO 489.116 NO 246.876 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 251.165 CO 480.713 NO 245.396 75 seconds 13 seconds 9.20% 9.04% 9.16% 99.42% 99.86% 99.92% 9.730 GAS D6348 Annex 5. Analyte Spiking Technique Propane Spike Direct SF6 CO NO 253.100 9.954 497.300 252.900 252.068 9.789 491.628 248.703 0.41% 1.66% 1.14% 1.66% +/- 2% +/- 2% +/- 2% +/- 2% Pass Pass Pass Pass Parameter Gas Concentration Measured % Difference Specification Validated 0.050 0.000 Spike Average 23.196 0.901 Dilution Factor 9.204% Expected 23.330 % Recovery 99.420% Specification 70-130% <10% Spike Run 1 via the System Source Output Propane SF6 D6348 Annex 6. Determination of System Performance Parameters Noise Equivalent Absorbance (NEA) RMS High RMS Mid RMS Low Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%) 0.000 Spike Average 0.885 Dilution Factor 9.041% Expected % Recovery Specification 70-130% <10% Spike Run 2 via the System Source Output Propane SF6 0.000 Spike Average 0.897 Dilution Factor 9.163% Expected % Recovery Specification 70-130% <10% Spike Run 3 via the System Source Output Propane SF6 0.309 23.445 23.465 99.920% 0.000084 0.000121 0.000380 0.291 23.113 23.145 99.860% Line Position Difference:Resolution Difference to Reference0.00%Pass Pass3.10% 16 GAS Resolution The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. Detector Linerarity The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. D6348 Annex 7. Preparation of Analytical Quantification Algorithm The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 Regression Slope:-5.28734532 Pass Line Position Difference:Resolution Difference to Reference 3.10% D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures CTS Bottle Concentration: CTS Sample Concentration Average: Difference between measured and expected: Tolerance: 100.00 99.31 0.70% 5.00% POST CTS System Check: Run 1 Points 1 & 2 on CO/NO/Propane Run 2 Points 1 & 2 on CO/NO/Propane Run 3 Points 1 & 2 on CO/NO/Propane Run Data Validation - Automated vs Manual Reading Validated Comments All within 20% All within 20% All within 20% Passed Passed Passed Demonstrates no interferences observed. Demonstrates no interferences observed. Demonstrates no interferences observed. 17 GAS 12.0 Signature Page Job/File Name: We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Crusoe Energy Systems, Inc.; Residue Booster Station; 1455; JJJJ 18 Company: Print Name: Signature: Title: Phone Number: Date: Company:G.A.S. Inc.Date: Print Name: Title: 4/23/2025 Emissions Specialist Company:G.A.S. Inc.Date: Print Name: Title: Signature: Phone Number: Travis Hartley Director of Stack Testing 580-225-0403 4/23/2025 Cooper Green GAS Appendices GAS GAS Spike (5 Gas) GAS 9% O2/NO2 GAS Ethylene Only GAS BIP GAS 21% O2 Tri Probe Certification ” ‡ ƒ – Ž ƒ ‹ • • • ƒ Ž › – ‹ … ƒ Ž ‡ ” ˜ ‹ … ‡ • ͵Ͳ͵͵”†–Ž‹–›ǡǡ͹͵͸ͶͶ ȋͷͺͲȌʹʹͷǦͲͶͲ͵ ƒšǣȋͷͺͲȌʹʹͷǦʹ͸ͳʹ &(57,),&$7(2)$1$/<6,6 *UDGHRI3URGXFW&(57,),('67$1'$5'352%( 3DUW1XPEHU65HIHUHQFH 1XPEHU  /DERUDWRU\*$6,1&6WDFN'LDPHWHU $QDO\VLV'DWH7DUJHW)ORZ 5DWH /PLQ /271XPEHU 61 $ $6 1XPEHURI 3RLQWV  3URGXFWSHUIRUPDQFHYHULILHGE\GLUHFWFRPSDULVRQWRFDOLEUDWLRQVWDQGDUGVWUDFHDEOHWR1,67  7KHSUREHOLVWHGRQWKLVIRUPPHHWVWKHPXOWLSRLQWWUDYHUVHUHTXLUHPHQWRI(3$0HWKRGH VHFWLRQDVVKRZQLQWKHDFFRPSDQ\LQJGDWD0HWKRGHVHFWLRQVWDWHVWKDWWKHPXOWLSRLQW WUDYHUVHUHTXLUHPHQWFDQEHVDWLVILHGE\VDPSOLQJYLD³DPXOWLKROHSUREHGHVLJQHGWRVDPSOHDW WKHSUHVFULEHGSRLQWVZLWKDIORZSHUFHQWRIPHDQIORZUDWH´ $1$/<7,&$/5(68/76 ZƵŶηdŽƚĂů&ůŽǁ ;>ͬŵͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϭͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϮͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϯͿ 0HDQ3UREH 3RUW6DPSOHG )ORZ /P  5XQ/30  䧮    䧮    䧮   5XQ/30  䧮    䧮    䧮    &DOLEUDWLRQFRQGXFWHGLQDFFRUGDQFHZLWK(PLVVLRQ0HDVXUHPHQW&HQWHU*XLGHOLQH'RFXPHQW±(0&*' 1RWHV BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB $SSURYHGIRU5HOHDVH'DWH 2/17/2022 Probe size: 20S Mr. Jordan Williamson CEO GAS Inc. 303 W. 3rd Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. March 15, 2021 Sincerely, Steffan M. Johnson, Group Leader Measurement Technology Group If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. cc: Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leather.james@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Heather Sessing, Oklahoma DEQ, (Heather.sessing@deq.ok.gov) Cooper Green GAS Type of Sources Tested: info@gasinc.us Stationary Internal Combustion Engines • 4 Stroke Rich Burn Engines • 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods: • EPA Method 1 & 1A – Sampling & Traverse Points • EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream • EPA Method 3A – Oxygen • EPA Method 7E – NOX • EPA Method 10 – Carbon Monoxide • EPA Method 25A – Volatile Organic Compounds • ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. • Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Types of Analyzers: • Gasmet DX4000 FTIR • Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory • Testo 350 • Flame Ionization Detector 580-225-0403 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 1 Minute Average Data Sheet Crusoe Energy Systems, Inc.Client: Residue Booster Station Unit Number:1455 Make:Waukesha Location:9394 GSIModel: 1658743Serial Number: RAW Result Data Stability 4/23/2025 05:41 0.4870.000-0.004 0.000 0.0000.000 0.000 0.000 0.0000.1040.000 0.000 0.0000.227 0.000 843.00.210.315 0.000 0.49 0.00 179.0 Pre Test Baseline Direct 4/23/2025 05:48 0.0000.0000.004 0.000 0.1750.000 0.000 0.095 0.0000.1480.104 0.000 0.0080.000 0.000 843.00.010.000 0.000 0.00 0.00 180.0 4/23/2025 05:48 0.0000.0000.004 0.000 0.0790.000 0.000 0.019 0.1300.0000.177 0.000 0.0760.000 0.000 843.00.080.000 0.000 0.00 0.00 180.0 4/23/2025 05:49 0.0220.000-0.001 0.000 0.2160.000 0.012 0.116 0.0380.1640.403 0.000 0.0110.000 0.004 843.00.020.000 0.000 0.02 0.00 180.0 CTS Direct 4/23/2025 05:51 0.0000.3250.012 0.014 0.0000.000 0.000 0.000 0.4780.0980.000 98.961 0.0000.108 0.000 843.066.120.214 0.025 0.33 0.00 180.0 4/23/2025 05:51 0.0000.5810.009 0.010 0.0000.000 0.000 0.000 0.1900.1110.000 99.004 0.0000.000 0.036 843.066.180.152 0.024 0.58 0.00 180.0 4/23/2025 05:51 0.0000.1320.012 0.007 0.0000.000 0.000 0.000 0.3320.0000.000 99.107 0.0000.128 0.000 843.066.130.080 0.022 0.13 0.00 180.0 High O2 Direct 4/23/2025 05:57 0.0000.0000.000 0.000 0.0290.000 0.000 0.084 0.1430.0000.755 0.000 0.0000.000 0.000 843.00.020.024 0.000 0.00 20.82 180.0 4/23/2025 05:57 0.0000.0000.001 0.000 0.3450.000 0.000 0.003 0.1980.1320.714 0.000 0.0000.000 0.014 843.00.160.200 0.000 0.00 20.81 180.0 4/23/2025 05:57 0.0000.1410.001 0.000 0.0000.000 0.000 0.139 0.1190.0770.465 0.000 0.0300.000 0.000 843.00.060.044 0.000 0.14 20.85 180.0 NO2/Mid O2 Direct 4/23/2025 06:00 101.7270.452-0.002 0.000 0.0000.000 0.956 0.000 0.6780.0290.479 0.000 0.0000.000 0.000 843.00.000.000 0.000 102.18 10.60 180.0 4/23/2025 06:00 102.6140.1470.003 0.000 0.1030.000 0.958 0.000 0.6140.1050.417 0.000 0.0000.000 0.000 843.00.000.000 0.000 102.76 10.56 180.0 4/23/2025 06:01 102.5400.0000.004 0.000 0.0180.000 0.962 0.000 0.8080.0250.409 0.000 0.0000.000 0.000 843.00.000.000 0.000 102.54 10.58 180.0 Spike Direct 4/23/2025 06:04 0.000248.2420.003 4.958 5.449490.584 1.911 2.055 0.4430.4210.000 0.903 251.6600.431 0.970 843.0255.762.340 9.785 248.24 0.00 180.0 4/23/2025 06:04 0.000248.8880.005 4.945 5.080491.927 1.913 2.324 0.7090.4980.000 0.932 252.0660.682 0.889 843.0255.902.160 9.785 248.89 0.00 180.0 4/23/2025 06:05 0.000248.9790.008 4.917 5.146492.374 1.832 2.234 0.3230.3090.272 0.953 252.4780.399 0.923 843.0256.422.184 9.796 248.98 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline System 4/23/2025 06:07 0.0000.2600.012 0.054 0.0000.895 0.000 0.129 0.0000.0010.415 0.000 0.6070.149 0.054 843.00.790.111 0.006 0.26 0.00 180.0 4/23/2025 06:07 0.0000.0000.005 0.015 0.4090.240 0.018 0.179 0.0000.0210.000 0.000 0.3650.000 0.043 843.00.660.307 0.000 0.00 0.00 180.0 4/23/2025 06:07 0.0000.1460.010 0.013 0.1540.168 0.015 0.101 0.0000.0000.036 0.000 0.2080.000 0.042 843.00.420.199 0.000 0.15 0.00 180.0 CTS System with Response Time 4/23/2025 06:09 0.0000.0000.017 0.036 0.0000.000 0.000 0.000 0.1950.0010.000 98.261 0.0000.047 0.094 843.065.700.000 0.025 0.00 0.00 180.0 4/23/2025 06:09 0.0000.0000.011 0.028 0.0000.000 0.000 0.000 0.0000.0060.000 98.463 0.0000.000 0.066 843.065.840.088 0.023 0.00 0.00 180.0 4/23/2025 06:09 0.0000.0000.014 0.039 0.0000.000 0.000 0.000 0.4380.0000.000 98.520 0.0000.049 0.053 843.065.930.213 0.023 0.00 0.00 180.0 NO2/Mid O2 System with Response Time 4/23/2025 06:11 99.5982.8480.007 0.020 0.0740.471 0.988 0.034 0.0000.0000.309 0.000 0.0000.000 0.056 843.00.110.000 0.002 102.45 10.59 180.0 4/23/2025 06:12 100.0882.7060.007 0.006 0.4240.462 0.985 0.016 0.0000.0030.010 0.000 0.2070.000 0.000 843.00.210.000 0.000 102.79 10.60 180.0 4/23/2025 06:12 99.8183.5170.002 0.012 0.5550.240 1.003 0.002 0.0000.0010.000 0.000 0.1010.000 0.024 843.00.150.000 0.000 103.33 10.53 180.0 Spike System with Response Time 4/23/2025 06:14 0.000247.1560.006 4.925 2.448488.852 1.835 1.908 0.4450.1130.216 1.020 252.1760.320 0.798 843.0255.922.205 9.750 247.16 0.00 180.0 4/23/2025 06:15 0.000247.2700.007 4.882 4.455490.926 1.836 2.190 0.2560.0370.000 1.084 251.3710.337 0.897 843.0255.232.018 9.736 247.27 0.00 180.0 4/23/2025 06:15 0.000246.2020.004 4.941 2.676487.571 1.842 2.276 0.0000.1260.000 1.074 251.5650.150 0.904 843.0255.762.513 9.735 246.20 0.00 180.0 Baseline System with Response Time 4/23/2025 06:18 0.0000.0000.008 0.023 0.1690.190 0.019 0.000 0.0000.0050.625 0.000 0.3490.000 0.007 843.00.600.358 0.000 0.00 0.00 180.0 4/23/2025 06:19 0.0000.1770.005 0.015 0.4830.178 0.005 0.141 0.0760.0190.622 0.000 0.3850.000 0.000 843.00.550.251 0.000 0.18 0.00 180.0 4/23/2025 06:19 0.0000.6740.005 0.007 0.2530.317 0.019 0.072 0.0000.0030.272 0.000 0.3940.038 0.000 843.00.740.522 0.000 0.67 0.00 180.0 Run 1 - A 30minute/60min 4/23/2025 07:28 0.9886.53615.906 10.418 59.5551.820 0.647 0.210 1.8520.0216.094 0.000 0.3940.646 0.271 831.01.500.853 0.000 7.52 0.00 180.0 4/23/2025 07:29 0.0009.56617.852 10.341 57.4991.798 1.282 0.906 1.5030.1342.905 0.000 0.0090.908 0.214 831.01.020.876 0.000 9.57 0.00 180.0 4/23/2025 07:30 0.0006.99617.023 10.437 69.1972.269 0.859 0.639 2.0700.0995.250 0.000 0.0610.881 0.179 831.00.700.417 0.000 7.00 0.00 180.0 4/23/2025 07:31 0.0008.79016.667 10.472 63.6772.303 0.924 0.332 1.8040.0274.934 0.000 0.0890.744 0.180 831.00.780.498 0.000 8.79 0.00 180.0 4/23/2025 07:32 0.0009.43817.602 10.363 56.9372.275 1.279 0.200 1.5740.1346.262 0.000 0.0600.673 0.184 831.01.030.897 0.000 9.44 0.00 180.0 4/23/2025 07:33 0.01610.76818.376 10.245 59.3222.057 1.407 0.653 1.9460.0756.869 0.000 0.1171.036 0.203 831.01.291.154 0.000 10.78 0.04 179.0 4/23/2025 07:34 0.3227.70617.424 10.482 57.1041.632 0.915 0.416 1.5380.1966.254 0.000 0.0000.674 0.190 831.00.920.806 0.000 8.03 0.00 180.0 4/23/2025 07:35 0.4817.63517.440 10.431 55.9181.509 0.637 0.280 1.4970.1726.150 0.000 0.0000.988 0.194 831.00.910.787 0.000 8.12 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/23/2025 07:36 0.0008.04717.458 10.374 52.3471.523 0.377 0.426 1.3580.0165.370 0.000 0.1000.623 0.111 831.00.810.734 0.000 8.05 0.04 180.0 4/23/2025 07:37 0.00010.24017.813 10.352 57.5801.698 1.331 0.358 1.5020.0514.514 0.000 0.0000.972 0.189 831.00.860.729 0.000 10.24 0.00 179.0 4/23/2025 07:38 0.0009.92518.603 10.300 56.9952.429 1.531 0.895 2.0000.3074.353 0.000 0.0001.023 0.141 831.00.870.889 0.000 9.92 0.00 180.0 4/23/2025 07:39 0.00010.58617.451 10.350 54.1222.886 1.445 0.643 1.4250.0433.853 0.000 0.0000.634 0.144 831.00.790.748 0.000 10.59 0.00 180.0 4/23/2025 07:40 0.0009.13917.351 10.259 55.7882.593 1.292 0.604 1.6460.0274.749 0.000 0.0690.732 0.102 831.00.820.819 0.000 9.14 0.04 178.0 4/23/2025 07:41 0.0007.56617.339 10.396 52.2671.139 0.682 0.575 1.2980.1145.366 0.000 0.0000.743 0.131 831.00.740.716 0.000 7.57 0.00 180.0 4/23/2025 07:42 0.1588.04617.391 10.399 61.9002.026 0.858 0.595 1.8570.0955.669 0.000 0.0580.691 0.154 831.00.890.779 0.000 8.20 0.00 180.0 4/23/2025 07:43 0.2509.14917.466 10.323 53.6361.719 0.989 0.369 1.3260.0624.178 0.000 0.0000.901 0.167 831.00.870.811 0.000 9.40 0.00 180.0 4/23/2025 07:44 0.3119.90617.406 10.400 54.8302.152 1.445 0.383 1.6050.0733.300 0.000 0.0000.798 0.121 831.00.890.975 0.000 10.22 0.00 180.0 4/23/2025 07:45 0.0068.53617.390 10.401 58.5242.181 0.792 0.484 1.9880.1555.008 0.000 0.0040.738 0.169 831.00.740.603 0.000 8.54 0.00 180.0 4/23/2025 07:46 0.13810.19017.368 10.344 56.7981.854 1.523 0.410 1.9540.0563.810 0.000 0.0000.636 0.145 831.00.830.809 0.000 10.33 0.00 179.0 4/23/2025 07:47 0.0007.64217.457 10.364 52.4291.594 0.619 0.543 1.3740.1355.413 0.000 0.0070.863 0.110 831.00.590.538 0.000 7.64 0.00 180.0 4/23/2025 07:48 0.15310.58117.399 10.381 50.0482.159 1.308 0.454 1.4300.0253.254 0.000 0.0340.441 0.133 831.00.790.740 0.000 10.73 0.00 180.0 4/23/2025 07:49 1.02610.33217.443 10.392 50.5001.949 1.315 0.313 1.5860.0623.166 0.000 0.0260.912 0.136 831.00.810.776 0.000 11.36 0.00 180.0 4/23/2025 07:50 0.1939.83017.499 10.376 57.1751.913 1.357 0.307 1.8980.0673.596 0.000 0.0580.769 0.131 831.00.850.801 0.000 10.02 0.00 180.0 4/23/2025 07:51 0.0006.97817.539 10.365 58.1631.851 0.504 0.352 1.8670.0685.248 0.000 0.0000.875 0.126 831.00.780.787 0.000 6.98 0.04 180.0 4/23/2025 07:52 0.20010.09117.506 10.395 55.5432.006 1.491 0.307 1.8070.0203.482 0.000 0.1010.909 0.140 831.00.980.900 0.000 10.29 0.04 180.0 4/23/2025 07:54 0.2099.99117.508 10.378 53.4721.915 1.533 0.443 1.8810.0583.576 0.000 0.0000.873 0.124 831.00.921.016 0.000 10.20 0.00 180.0 4/23/2025 07:55 0.3529.71217.571 10.400 54.4072.205 1.254 0.496 1.8470.1933.512 0.000 0.0820.823 0.158 831.00.990.890 0.000 10.06 0.04 180.0 4/23/2025 07:56 0.2989.72217.549 10.379 46.8401.515 1.363 0.465 1.3210.0563.551 0.000 0.0230.766 0.126 831.00.900.942 0.000 10.02 0.00 180.0 4/23/2025 07:57 0.4439.89117.560 10.362 48.9712.593 1.061 0.422 1.4970.1183.645 0.000 0.0000.675 0.113 831.00.710.731 0.000 10.33 0.00 180.0 4/23/2025 07:58 1.03210.06117.560 10.391 50.4552.324 1.345 0.582 1.6640.0893.006 0.000 0.2010.798 0.137 831.01.221.121 0.000 11.09 0.00 180.0 0.2199.12017.464 10.376 55.7331.996 1.112 0.469 1.6640.0924.545 0.000 0.0500.792 0.154 831.000.8930.805 0.000 9.339 0.008 179.8Avg. Spike 1 4/23/2025 08:00 0.28029.20416.070 9.841 51.16951.167 1.270 0.801 1.4270.0373.572 1.138 23.1960.771 0.128 831.025.101.336 0.901 29.48 0.00 180.0 Run 1 - B 30minute/60min 4/23/2025 08:02 0.0007.71017.518 10.419 46.9821.319 0.566 0.695 1.4310.1635.242 0.000 0.0000.897 0.093 831.00.640.678 0.000 7.71 0.00 180.0 4/23/2025 08:03 0.1187.91117.499 10.383 50.3551.131 0.616 0.648 1.6430.1365.245 0.000 0.1731.013 0.114 831.00.950.820 0.000 8.03 0.00 180.0 4/23/2025 08:04 0.6577.18217.524 10.387 37.4131.176 0.288 0.620 1.0470.0635.649 0.000 0.0630.756 0.092 831.00.760.773 0.000 7.84 0.03 180.0 4/23/2025 08:05 0.1458.20417.531 10.411 46.7251.979 0.491 0.614 1.5020.1505.683 0.000 0.0000.927 0.125 831.00.760.760 0.000 8.35 0.00 180.0 4/23/2025 08:06 0.5757.39617.572 10.401 48.8691.749 0.393 0.646 1.8640.1125.738 0.000 0.0840.835 0.117 831.00.840.780 0.000 7.97 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/23/2025 08:07 0.1247.21817.530 10.404 53.3501.469 0.749 0.707 1.7790.0614.455 0.000 0.0960.842 0.125 831.00.890.820 0.000 7.34 0.00 180.0 4/23/2025 08:08 0.0007.29517.501 10.408 47.7241.285 0.559 0.616 1.3370.1684.975 0.000 0.0000.557 0.056 831.00.590.722 0.000 7.29 0.00 180.0 4/23/2025 08:09 0.3847.63117.484 10.389 42.3071.071 0.395 0.594 1.3180.0615.669 0.000 0.0320.668 0.120 831.00.830.842 0.000 8.01 0.00 180.0 4/23/2025 08:10 0.0009.67917.466 10.381 50.4851.915 1.211 0.338 1.6580.0542.734 0.000 0.0000.903 0.068 831.00.670.799 0.000 9.68 0.00 180.0 4/23/2025 08:11 0.1999.29817.479 10.378 61.4821.809 1.299 0.416 2.1840.0933.547 0.000 0.0730.830 0.130 831.00.950.920 0.000 9.50 0.00 180.0 4/23/2025 08:12 0.5989.20417.457 10.402 48.2141.511 1.306 0.417 1.5460.0683.155 0.000 0.0200.914 0.118 831.00.780.783 0.000 9.80 0.00 180.0 4/23/2025 08:13 0.7169.62517.433 10.379 50.3061.733 1.170 0.290 1.8790.1032.946 0.000 0.0000.736 0.119 831.00.800.848 0.000 10.34 0.00 180.0 4/23/2025 08:14 0.0009.72817.475 10.379 56.0471.813 1.249 0.280 1.9460.1223.183 0.000 0.0050.873 0.096 831.00.720.792 0.000 9.73 0.00 180.0 4/23/2025 08:15 0.2799.47417.447 10.386 58.8102.275 1.461 0.334 2.2180.0853.339 0.000 0.0001.066 0.136 831.00.750.711 0.000 9.75 0.00 180.0 4/23/2025 08:16 0.4178.94017.451 10.377 57.5462.471 1.486 0.530 2.2520.1393.329 0.000 0.1490.829 0.132 831.01.201.176 0.000 9.36 0.00 180.0 4/23/2025 08:17 0.2888.85317.467 10.341 58.9282.097 1.430 0.609 2.2920.1413.543 0.000 0.2101.059 0.127 831.01.221.140 0.000 9.14 0.00 180.0 4/23/2025 08:18 0.0009.40317.463 10.378 51.0151.600 1.242 0.515 1.7830.1043.139 0.000 0.0000.938 0.092 831.00.810.938 0.000 9.40 0.00 180.0 4/23/2025 08:19 0.0079.21517.442 10.388 53.3901.795 1.275 0.431 2.0770.1133.688 0.000 0.1061.013 0.133 831.00.890.781 0.000 9.22 0.00 180.0 4/23/2025 08:20 0.5579.27817.405 10.395 47.5231.727 1.446 0.481 1.8740.0542.804 0.000 0.1010.729 0.090 831.00.930.970 0.000 9.83 0.00 180.0 4/23/2025 08:21 0.2899.27917.402 10.390 45.7121.386 1.261 0.461 1.5230.0422.535 0.000 0.1100.794 0.179 831.01.241.149 0.000 9.57 0.00 180.0 4/23/2025 08:22 0.3359.29917.402 10.376 44.9591.298 1.251 0.434 1.4650.1082.653 0.000 0.0730.765 0.176 831.01.030.901 0.000 9.63 0.00 180.0 4/23/2025 08:23 0.6048.72617.405 10.376 47.7480.903 1.135 0.304 1.8450.0492.801 0.000 0.2880.734 0.111 831.01.301.181 0.000 9.33 0.00 180.0 4/23/2025 08:24 0.4548.08017.438 10.410 49.5471.597 1.154 0.276 1.9490.0792.929 0.000 0.1340.921 0.137 831.01.141.105 0.000 8.53 0.00 180.0 4/23/2025 08:25 0.4608.84117.422 10.388 44.6931.192 1.322 0.333 1.7100.1102.559 0.000 0.1851.012 0.147 831.01.281.203 0.000 9.30 0.00 180.0 4/23/2025 08:26 0.8778.15217.444 10.393 47.8081.110 1.067 0.245 1.6500.1433.072 0.000 0.1200.748 0.176 831.00.990.770 0.000 9.03 0.00 180.0 4/23/2025 08:27 0.2496.05517.443 10.389 53.8000.896 0.437 0.326 1.9160.0755.466 0.000 0.1220.915 0.195 831.01.221.053 0.000 6.30 0.00 180.0 4/23/2025 08:28 0.7277.29417.419 10.351 55.8811.419 0.399 0.366 2.3410.0835.461 0.000 0.2331.030 0.198 831.01.341.072 0.000 8.02 0.00 180.0 4/23/2025 08:29 1.4588.09017.442 10.369 46.7631.967 1.101 0.353 1.8390.0362.923 0.000 0.1430.919 0.191 831.01.150.932 0.000 9.55 0.00 180.0 4/23/2025 08:30 0.4176.09317.426 10.360 57.1271.675 0.688 0.654 2.3820.0425.223 0.000 0.3201.032 0.185 831.01.350.997 0.000 6.51 0.00 180.0 4/23/2025 08:31 0.6516.08817.432 10.400 54.1981.388 0.557 0.581 2.0130.0394.884 0.000 0.1280.693 0.210 831.01.170.935 0.000 6.74 0.00 180.0 0.3868.30817.461 10.386 50.5241.559 0.967 0.470 1.8090.0933.952 0.000 0.0990.865 0.133 831.000.9730.912 0.000 8.693 0.001 180.0Avg. 0.3038.71417.462 10.381 53.1281.777 1.039 0.470 1.7360.0924.248 0.000 0.0740.828 0.144 831.000.9330.858 0.000 9.016 0.005 179.9Run 1 Avg: Baseline 1 4/23/2025 08:33 0.0000.1230.045 0.049 0.0180.231 0.021 0.075 0.0000.0000.674 0.000 0.3390.000 0.000 831.00.770.652 0.000 0.12 0.00 180.0 Run 2 - A 30minute/60min 4/23/2025 08:35 1.59442.08517.333 10.254 17.2760.000 5.634 0.365 0.5980.1212.011 0.000 0.1350.836 0.166 831.00.920.674 0.000 43.68 0.00 180.0 4/23/2025 08:37 1.37710.40417.503 10.338 8.3891.331 0.912 0.181 1.0980.0251.711 0.000 0.1380.808 0.138 831.01.050.956 0.000 11.78 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/23/2025 08:38 0.7078.44217.494 10.358 11.8279.339 0.718 0.181 0.5100.1421.515 0.000 0.2450.573 0.170 831.01.140.826 0.000 9.15 0.00 180.0 4/23/2025 08:39 1.5736.92017.471 10.340 23.16821.713 0.630 0.379 0.9560.0622.158 0.000 0.2620.935 0.191 831.01.260.921 0.000 8.49 0.00 180.0 4/23/2025 08:40 1.0438.12117.482 10.367 32.35220.847 1.274 0.754 1.2080.0261.772 0.000 0.2840.587 0.266 831.01.440.941 0.000 9.16 0.00 180.0 4/23/2025 08:41 1.3988.25417.560 10.382 28.7478.415 1.097 0.827 1.4140.0751.740 0.000 0.1410.939 0.179 831.01.140.956 0.000 9.65 0.00 180.0 4/23/2025 08:42 0.4857.17517.568 10.403 45.0927.695 1.199 1.065 1.6490.0251.864 0.000 0.0920.856 0.220 831.01.140.910 0.000 7.66 0.00 180.0 4/23/2025 08:43 0.4675.99317.561 10.428 62.8496.579 0.774 1.378 2.5630.0693.465 0.000 0.3540.951 0.265 831.01.530.968 0.000 6.46 0.00 180.0 4/23/2025 08:44 0.8736.10617.498 10.409 65.1264.919 0.871 1.369 2.9630.0813.882 0.000 0.3420.916 0.255 831.01.430.860 0.000 6.98 0.00 180.0 4/23/2025 08:45 1.0467.51817.423 10.378 59.5612.807 1.549 1.147 2.7420.0252.467 0.000 0.4070.843 0.253 831.01.601.027 0.000 8.56 0.00 180.0 4/23/2025 08:46 0.5187.05117.388 10.331 52.5931.658 1.125 0.820 2.2180.0182.419 0.000 0.3110.766 0.222 831.01.421.004 0.000 7.57 0.04 180.0 4/23/2025 08:47 0.7567.27017.363 10.385 49.9511.464 1.252 0.659 2.2610.0192.629 0.000 0.2580.796 0.232 831.01.451.089 0.000 8.03 0.00 180.0 4/23/2025 08:48 0.8726.98317.346 10.394 52.6061.530 1.164 0.580 2.1840.0342.172 0.000 0.3920.793 0.220 831.01.500.999 0.000 7.85 0.00 180.0 4/23/2025 08:49 1.4476.83117.370 10.369 45.7361.039 1.195 0.515 1.6020.0052.465 0.000 0.2920.806 0.271 831.01.430.899 0.000 8.28 0.00 180.0 4/23/2025 08:50 0.7527.14217.356 10.367 42.5921.254 1.021 0.455 1.8390.0042.492 0.000 0.3000.842 0.224 831.01.611.299 0.000 7.89 0.00 180.0 4/23/2025 08:51 0.8865.90417.369 10.387 48.2621.088 0.430 0.538 1.8820.0484.466 0.000 0.3570.732 0.246 831.01.521.005 0.000 6.79 0.00 180.0 4/23/2025 08:52 1.0307.26917.393 10.388 45.4230.905 1.141 0.360 1.7980.0262.428 0.000 0.2560.816 0.258 831.01.410.956 0.000 8.30 0.00 180.0 4/23/2025 08:53 0.7527.95217.396 10.358 54.9271.041 1.005 0.363 2.2310.0072.536 0.000 0.3460.953 0.266 831.01.500.940 0.000 8.70 0.00 180.0 4/23/2025 08:54 1.5937.07017.316 10.403 51.1781.175 1.256 0.310 1.9030.0332.383 0.000 0.2730.693 0.246 831.01.340.862 0.000 8.66 0.00 180.0 4/23/2025 08:55 1.2625.85017.334 10.348 51.9070.958 0.448 0.431 2.1150.0224.451 0.000 0.2710.793 0.269 831.01.420.916 0.000 7.11 0.00 180.0 4/23/2025 08:56 1.2476.79817.328 10.387 44.7351.321 1.026 0.354 1.8330.0422.410 0.000 0.2901.034 0.249 831.01.380.886 0.000 8.05 0.00 180.0 4/23/2025 08:57 1.6816.55917.338 10.364 48.5831.344 1.147 0.312 1.8630.0212.371 0.000 0.3950.845 0.283 831.01.560.893 0.000 8.24 0.00 180.0 4/23/2025 08:58 1.1136.32517.349 10.406 46.0141.178 1.096 0.280 1.7920.0021.951 0.000 0.2880.674 0.250 831.01.430.968 0.000 7.44 0.00 180.0 4/23/2025 08:59 0.5866.28817.326 10.404 52.8061.634 1.324 0.333 2.2170.0042.235 0.000 0.4341.040 0.276 831.01.570.880 0.000 6.87 0.00 180.0 4/23/2025 09:00 0.7148.05317.347 10.361 49.3871.471 0.988 0.385 1.9170.0032.169 0.000 0.3270.850 0.280 831.01.510.931 0.000 8.77 0.04 180.0 4/23/2025 09:01 1.0996.52817.312 10.366 47.4571.567 1.188 0.420 1.8240.0011.942 0.000 0.3730.700 0.320 831.01.660.971 0.000 7.63 0.00 179.0 4/23/2025 09:02 0.8005.62717.347 10.391 54.7461.008 0.516 0.569 2.0330.0073.763 0.000 0.3330.757 0.319 831.01.590.936 0.000 6.43 0.00 180.0 4/23/2025 09:03 1.1026.84317.371 10.394 48.8941.113 1.154 0.375 1.8280.0182.152 0.000 0.3161.058 0.294 831.01.480.863 0.000 7.94 0.00 180.0 4/23/2025 09:04 0.5817.80017.392 10.390 50.4810.968 1.143 0.364 1.7240.0012.202 0.000 0.2520.823 0.296 831.01.671.240 0.000 8.38 0.00 180.0 4/23/2025 09:05 1.0117.93317.420 10.362 40.0610.318 0.260 0.460 1.5020.0054.294 0.000 0.2760.862 0.259 831.01.380.886 0.000 8.94 0.00 180.0 1.0128.30317.402 10.374 44.4243.589 1.151 0.551 1.8090.0322.551 0.000 0.2910.829 0.246 831.001.4160.949 0.000 9.315 0.003 180.0Avg. Spike 2 4/23/2025 09:08 0.75125.91615.865 9.894 40.27749.825 1.171 0.610 1.1710.0002.011 0.951 23.1130.654 0.324 831.025.241.271 0.885 26.67 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Run 2 - B 30minute/60min 4/23/2025 09:10 0.6897.37017.408 10.385 40.6551.070 0.810 0.292 1.5080.0001.574 0.000 0.2750.808 0.284 831.01.450.912 0.000 8.06 0.00 180.0 4/23/2025 09:11 1.4427.71617.376 10.354 46.6761.506 1.198 0.311 1.8480.0001.780 0.000 0.2690.823 0.311 831.01.591.056 0.000 9.16 0.00 180.0 4/23/2025 09:12 1.3547.50817.375 10.389 43.7581.120 1.127 0.280 1.5530.0191.751 0.000 0.2850.906 0.345 831.01.600.938 0.000 8.86 0.00 180.0 4/23/2025 09:13 2.0717.18817.401 10.353 47.8771.121 0.941 0.287 1.4800.0241.658 0.000 0.3041.001 0.332 831.01.550.880 0.004 9.26 0.00 180.0 4/23/2025 09:14 1.0657.07017.422 10.361 47.7071.115 1.054 0.274 1.8240.0031.682 0.000 0.3460.827 0.303 830.01.560.914 0.000 8.13 0.00 180.0 4/23/2025 09:15 1.5666.99417.406 10.399 51.1211.655 1.161 0.352 1.9410.0011.953 0.000 0.3630.939 0.325 831.01.701.035 0.000 8.56 0.00 180.0 4/23/2025 09:16 0.3976.87917.416 10.372 52.9351.202 1.219 0.281 1.6160.0181.707 0.000 0.3820.816 0.332 831.01.801.126 0.000 7.28 0.00 180.0 4/23/2025 09:18 0.4516.06817.426 10.364 60.2962.216 1.058 0.476 2.0230.0002.056 0.000 0.4740.840 0.332 831.01.871.096 0.000 6.52 0.00 180.0 4/23/2025 09:19 0.6547.59617.441 10.404 41.9001.619 1.495 0.554 1.2310.0081.503 0.000 0.5200.775 0.341 830.02.051.266 0.000 8.25 0.00 180.0 4/23/2025 09:20 0.5127.07517.379 10.379 46.5843.598 0.887 0.734 1.5050.0261.221 0.000 0.4080.838 0.358 830.01.740.922 0.000 7.59 0.00 180.0 4/23/2025 09:21 1.1816.65617.397 10.381 54.7252.884 1.468 1.026 1.9200.0001.358 0.000 0.4920.841 0.413 830.02.081.136 0.000 7.84 0.00 180.0 4/23/2025 09:22 1.0945.87917.409 10.410 62.0282.143 1.329 0.898 2.5320.0271.165 0.000 0.4210.769 0.344 830.01.861.118 0.000 6.97 0.00 180.0 4/23/2025 09:23 0.5186.15517.405 10.407 65.2581.881 1.467 0.850 2.6330.0051.540 0.000 0.4220.873 0.341 830.01.821.080 0.000 6.67 0.00 180.0 4/23/2025 09:24 0.6626.20717.439 10.412 53.5701.372 1.299 0.627 1.8770.0181.875 0.000 0.4020.774 0.382 830.01.921.133 0.000 6.87 0.00 180.0 4/23/2025 09:25 0.9783.27517.438 10.401 56.2031.221 0.426 0.761 1.9040.0153.375 0.000 0.3361.056 0.378 830.01.710.928 0.000 4.25 0.00 180.0 4/23/2025 09:26 1.0683.50817.447 10.395 53.6970.944 0.292 0.759 1.9480.0003.553 0.000 0.3450.741 0.329 830.01.691.035 0.000 4.58 0.00 180.0 4/23/2025 09:27 0.9303.07817.448 10.388 57.1061.023 0.489 0.667 1.9590.0024.107 0.000 0.3870.886 0.413 830.01.860.967 0.000 4.01 0.04 180.0 4/23/2025 09:28 0.5795.87317.361 10.415 48.5301.536 0.979 0.455 1.5290.0081.171 0.000 0.4230.800 0.378 830.01.800.926 0.000 6.45 0.00 180.0 4/23/2025 09:29 0.3993.19817.361 10.361 55.3871.421 0.513 0.658 1.9300.0023.165 0.000 0.5290.833 0.378 830.01.971.023 0.000 3.60 0.00 180.0 4/23/2025 09:30 0.6223.58017.354 10.408 56.5211.169 0.569 0.602 2.0210.0012.831 0.000 0.4910.725 0.368 830.01.971.119 0.000 4.20 0.04 180.0 4/23/2025 09:31 0.4472.68217.361 10.398 47.1350.734 0.341 0.512 1.4620.0043.834 0.000 0.4020.920 0.353 830.01.811.048 0.000 3.13 0.00 180.0 4/23/2025 09:32 0.5742.94417.357 10.381 48.2171.282 0.225 0.547 1.3520.0003.546 0.000 0.3950.783 0.378 830.01.821.002 0.000 3.52 0.00 180.0 4/23/2025 09:33 0.8443.83217.351 10.442 48.7431.235 0.529 0.629 1.6050.0402.443 0.000 0.4450.628 0.383 830.01.921.068 0.000 4.68 0.03 180.0 4/23/2025 09:34 0.9433.45617.325 10.406 47.7271.364 0.373 0.689 1.4400.0003.615 0.000 0.4830.786 0.363 830.01.891.024 0.000 4.40 0.00 180.0 4/23/2025 09:35 0.1456.23917.321 10.408 51.3851.924 1.327 0.623 1.8370.0001.017 0.000 0.6130.801 0.375 830.02.181.223 0.000 6.38 0.00 180.0 4/23/2025 09:36 0.3752.70617.335 10.407 56.8951.288 0.514 0.833 2.0630.0001.894 0.000 0.4060.594 0.372 830.01.961.212 0.000 3.08 0.00 180.0 4/23/2025 09:37 1.3472.80117.344 10.419 52.6571.050 0.408 0.653 1.6530.0033.340 0.000 0.4230.963 0.384 830.01.820.941 0.000 4.15 0.00 180.0 4/23/2025 09:38 0.5382.88317.347 10.439 52.1530.787 0.355 0.574 1.5410.0003.376 0.000 0.3640.783 0.365 830.01.710.930 0.000 3.42 0.00 180.0 4/23/2025 09:39 0.5552.94817.356 10.434 50.6620.714 0.402 0.524 1.6090.0123.742 0.000 0.3160.672 0.361 830.01.670.954 0.000 3.50 0.00 180.0 4/23/2025 09:40 1.6203.31517.349 10.451 46.7020.956 0.283 0.513 1.2720.0013.423 0.000 0.3290.838 0.373 830.01.680.909 0.000 4.94 0.00 180.0 0.8545.08917.385 10.397 51.4941.438 0.818 0.575 1.7540.0082.375 0.000 0.4020.821 0.356 830.231.8021.031 0.000 5.944 0.004 180.0Avg. 0.9336.69617.393 10.386 47.9592.514 0.985 0.563 1.7810.0202.463 0.000 0.3470.825 0.301 830.621.6090.990 0.000 7.629 0.003 180.0Run 2 Avg: GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline 2 4/23/2025 09:42 0.0000.0120.047 0.053 0.0000.170 0.023 0.069 0.0000.0260.216 0.000 0.3020.000 0.000 830.00.740.653 0.000 0.01 0.00 180.0 Run 3 - A 30minute/60min 4/23/2025 09:44 0.7315.27717.146 10.368 50.9341.792 1.109 0.489 1.4910.0020.055 0.000 0.3830.839 0.353 830.01.821.092 0.000 6.01 0.00 180.0 4/23/2025 09:45 0.0003.11217.262 10.388 58.9211.766 0.592 0.617 1.7990.0002.458 0.000 0.3810.961 0.286 830.01.691.107 0.002 3.11 0.00 180.0 4/23/2025 09:46 0.3802.67817.314 10.395 55.3391.125 0.427 0.658 1.6730.0003.508 0.000 0.3890.838 0.379 830.01.831.023 0.000 3.06 0.00 180.0 4/23/2025 09:47 0.7342.52817.313 10.411 47.6800.760 0.310 0.544 1.1890.0033.087 0.000 0.3240.720 0.345 830.01.640.942 0.000 3.26 0.00 180.0 4/23/2025 09:48 0.6032.72917.333 10.444 51.1531.045 0.513 0.496 1.1190.0041.870 0.000 0.4230.799 0.371 830.01.790.932 0.000 3.33 0.00 180.0 4/23/2025 09:49 0.2832.92717.369 10.447 46.0030.756 0.453 0.475 1.0450.0242.580 0.000 0.3230.639 0.338 830.01.731.102 0.000 3.21 0.00 180.0 4/23/2025 09:50 0.6343.40317.368 10.401 38.6492.289 0.032 0.441 0.9890.0002.853 0.000 0.2850.664 0.319 830.01.701.165 0.000 4.04 0.00 180.0 4/23/2025 09:51 0.3143.72517.352 10.457 48.5181.991 0.478 0.619 1.4050.0232.567 0.000 0.3870.791 0.362 830.01.791.024 0.000 4.04 0.00 180.0 4/23/2025 09:52 0.4173.40417.348 10.494 43.7651.369 0.641 0.594 1.1940.0160.922 0.000 0.3710.743 0.360 830.01.821.091 0.000 3.82 0.00 180.0 4/23/2025 09:53 0.6763.07717.357 10.461 51.1821.067 0.585 0.613 1.4720.0261.739 0.000 0.3280.911 0.365 830.01.720.990 0.000 3.75 0.00 180.0 4/23/2025 09:54 0.3402.97717.344 10.385 49.4411.580 0.186 0.588 1.5390.0243.313 0.000 0.3450.705 0.312 830.01.791.239 0.000 3.32 0.00 179.0 4/23/2025 09:55 0.4623.69717.370 10.513 55.0271.476 0.671 0.622 1.7360.0151.439 0.000 0.2520.705 0.320 830.01.721.242 0.000 4.16 0.00 180.0 4/23/2025 09:56 0.2943.25417.368 10.526 53.7561.654 0.647 0.586 1.6240.0061.016 0.000 0.3030.820 0.341 830.01.691.053 0.000 3.55 0.00 180.0 4/23/2025 09:57 0.3953.16317.414 10.462 48.2071.092 0.491 0.598 1.2540.0072.645 0.000 0.2160.703 0.321 830.01.531.015 0.000 3.56 0.00 180.0 4/23/2025 09:58 0.3833.06817.402 10.415 39.6550.578 0.230 0.590 0.8810.0002.858 0.000 0.2090.594 0.310 830.01.551.074 0.000 3.45 0.00 180.0 4/23/2025 10:00 0.7831.87117.380 10.430 47.0513.764 0.008 0.596 1.0330.0002.753 0.000 0.2930.724 0.341 830.01.630.984 0.001 2.65 0.00 180.0 4/23/2025 10:01 0.0002.86417.378 10.433 45.2232.330 0.618 0.866 0.8490.0360.108 0.000 0.2210.652 0.310 830.01.521.024 0.000 2.86 0.00 180.0 4/23/2025 10:02 0.0002.85817.346 10.450 51.8341.920 0.651 0.948 1.4090.0110.935 0.000 0.2300.791 0.292 830.01.581.147 0.000 2.86 0.00 180.0 4/23/2025 10:03 0.2683.81417.331 10.421 49.9491.294 0.555 0.838 1.3790.0000.823 0.000 0.2780.644 0.319 830.01.671.131 0.001 4.08 0.00 180.0 4/23/2025 10:04 0.0002.43417.368 10.400 35.8201.011 0.241 0.690 0.7370.0022.293 0.000 0.1330.694 0.266 830.01.411.120 0.001 2.43 0.00 180.0 4/23/2025 10:05 1.0633.01517.361 10.422 46.6292.855 0.265 0.730 1.1110.0051.681 0.000 0.2110.609 0.309 830.01.571.114 0.000 4.08 0.00 180.0 4/23/2025 10:06 0.2293.16317.405 10.447 40.6211.573 0.754 0.965 0.9650.0390.466 0.000 0.3470.850 0.329 830.01.751.121 0.000 3.39 0.00 180.0 4/23/2025 10:07 0.8643.11617.389 10.410 41.0401.587 0.208 0.733 0.9330.0081.746 0.000 0.3490.731 0.332 830.01.711.047 0.000 3.98 0.00 180.0 4/23/2025 10:08 0.4212.00417.429 10.433 51.2831.676 0.463 0.794 1.4920.0002.576 0.000 0.3850.919 0.292 830.01.540.858 0.000 2.43 0.00 180.0 4/23/2025 10:09 0.0002.88717.379 10.477 49.6121.281 0.560 0.678 1.0730.0321.423 0.000 0.2220.761 0.315 830.01.571.077 0.000 2.89 0.00 180.0 4/23/2025 10:10 0.4443.02917.271 10.443 44.1132.072 0.405 0.766 1.1810.0261.710 0.000 0.2670.654 0.348 830.01.691.091 0.000 3.47 0.00 180.0 4/23/2025 10:11 0.0002.94817.291 10.389 51.1552.111 0.552 1.085 1.1560.0001.130 0.000 0.4130.808 0.262 830.01.691.138 0.000 2.95 0.00 180.0 4/23/2025 10:12 0.7713.18217.285 10.413 46.2041.387 0.354 0.903 1.2110.0052.439 0.000 0.3410.755 0.310 830.01.721.134 0.001 3.95 0.00 180.0 4/23/2025 10:13 0.1282.81017.296 10.482 60.2172.264 0.610 0.916 1.9940.0011.090 0.000 0.4220.928 0.406 830.01.961.094 0.000 2.94 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/23/2025 10:14 0.0002.89117.280 10.414 50.3111.204 0.472 0.885 1.0890.0022.537 0.000 0.2470.773 0.313 830.01.490.922 0.000 2.89 0.04 180.0 0.3873.06417.342 10.434 48.3101.622 0.469 0.697 1.2670.0111.887 0.000 0.3090.758 0.328 830.001.6771.070 0.000 3.451 0.001 180.0Avg. Spike 3 4/23/2025 10:17 0.23229.67715.748 9.941 48.92951.423 1.297 0.758 1.2550.0010.051 0.843 23.4450.479 0.360 830.025.661.393 0.897 29.91 0.00 180.0 Run 3 - B 30minute/60min 4/23/2025 10:19 1.0832.78217.341 10.413 50.6630.661 0.202 0.544 1.3040.0013.646 0.000 0.4800.897 0.447 830.02.101.091 0.000 3.86 0.00 180.0 4/23/2025 10:20 0.0002.72917.357 10.455 50.2820.772 0.286 0.505 1.1350.0003.532 0.000 0.3370.963 0.305 830.01.631.021 0.000 2.73 0.00 180.0 4/23/2025 10:21 0.2032.84817.353 10.429 54.8130.926 0.425 0.518 1.7180.0003.570 0.000 0.4390.867 0.372 830.01.921.103 0.000 3.05 0.00 180.0 4/23/2025 10:22 0.7855.91717.312 10.439 48.9751.028 0.977 0.280 1.3450.0000.548 0.000 0.4980.810 0.397 830.02.011.069 0.000 6.70 0.00 180.0 4/23/2025 10:23 0.0943.17617.318 10.432 50.8470.608 0.426 0.479 1.5250.0523.292 0.000 0.5560.814 0.367 830.02.031.103 0.000 3.27 0.00 180.0 4/23/2025 10:24 0.4536.42017.336 10.424 40.4070.223 0.334 0.482 1.0460.0003.079 0.000 0.4830.767 0.397 830.01.930.978 0.000 6.87 0.00 180.0 4/23/2025 10:25 0.0542.50617.379 10.414 42.9471.183 0.096 0.463 1.1400.0003.465 0.000 0.4840.827 0.394 830.01.951.024 0.000 2.56 0.00 180.0 4/23/2025 10:26 1.1666.48217.396 10.447 34.8460.424 0.701 0.522 0.7390.0002.452 0.000 0.3460.815 0.397 830.01.780.954 0.000 7.65 0.00 180.0 4/23/2025 10:27 0.8642.97617.400 10.477 39.1110.988 0.090 0.438 1.0290.0002.992 0.000 0.4240.734 0.336 830.01.791.044 0.000 3.84 0.00 180.0 4/23/2025 10:28 0.8743.31717.402 10.439 43.1201.203 0.090 0.501 1.2960.0013.459 0.000 0.4750.712 0.327 830.01.821.043 0.000 4.19 0.00 180.0 4/23/2025 10:29 0.2382.44217.437 10.428 58.5672.335 0.440 0.764 1.9670.0003.356 0.000 0.4900.803 0.408 830.02.031.089 0.000 2.68 0.00 180.0 4/23/2025 10:30 0.8355.35117.416 10.462 36.8610.779 0.883 0.814 1.1020.0001.880 0.000 0.4460.792 0.355 830.01.690.795 0.000 6.19 0.00 180.0 4/23/2025 10:31 0.9993.13817.397 10.438 26.5602.384 0.000 0.600 0.5920.0013.392 0.000 0.3820.740 0.347 830.01.670.899 0.000 4.14 0.00 180.0 4/23/2025 10:32 0.9036.35617.315 10.416 43.7756.399 1.103 1.111 1.1170.0000.352 0.000 0.4730.668 0.376 830.01.870.970 0.000 7.26 0.00 180.0 4/23/2025 10:33 0.5215.85217.344 10.402 52.4533.477 1.264 1.325 1.6960.0020.694 0.000 0.4910.776 0.391 830.01.991.080 0.000 6.37 0.00 180.0 4/23/2025 10:34 0.4256.40217.347 10.420 44.5851.570 1.487 0.997 1.3810.0000.348 0.000 0.4890.791 0.370 830.01.961.102 0.000 6.83 0.00 180.0 4/23/2025 10:35 0.6493.12317.325 10.419 46.3252.070 0.184 0.980 1.4300.0003.078 0.000 0.5260.572 0.358 830.01.900.994 0.000 3.77 0.00 180.0 4/23/2025 10:36 0.1737.30917.354 10.421 41.4842.098 1.649 1.141 1.4290.0060.176 0.000 0.5870.940 0.384 830.01.960.913 0.000 7.48 0.00 180.0 4/23/2025 10:37 0.3123.13517.365 10.403 40.3195.471 0.006 1.389 1.2790.0253.105 0.000 0.4550.703 0.375 830.01.770.853 0.000 3.45 0.00 180.0 4/23/2025 10:38 1.1124.12217.357 10.423 48.8313.840 0.679 1.931 1.8940.0162.167 0.000 0.5960.898 0.369 830.01.980.968 0.000 5.23 0.00 180.0 4/23/2025 10:39 0.9433.99417.371 10.410 46.1531.437 0.580 1.322 1.5590.0001.916 0.000 0.5420.798 0.373 830.01.810.781 0.000 4.94 0.00 180.0 4/23/2025 10:40 0.0006.48217.379 10.429 46.4381.371 1.266 0.854 0.8320.0000.727 0.000 0.3160.848 0.296 830.01.560.975 0.000 6.48 0.00 180.0 4/23/2025 10:41 1.2994.47417.384 10.454 42.1850.792 0.546 0.757 1.0970.0222.144 0.000 0.3710.855 0.369 830.01.550.664 0.000 5.77 0.00 180.0 4/23/2025 10:43 0.1557.06417.399 10.398 36.5330.299 0.176 0.624 1.2280.0003.847 0.000 0.5010.773 0.335 830.01.921.123 0.000 7.22 0.00 180.0 4/23/2025 10:44 0.6806.50917.415 10.429 46.9240.919 0.869 0.450 1.3960.0001.376 0.000 0.4750.706 0.323 830.01.770.975 0.000 7.19 0.00 180.0 4/23/2025 10:45 1.1314.04617.401 10.454 59.5701.342 0.442 0.514 1.9760.0083.846 0.000 0.4520.978 0.373 830.01.800.904 0.000 5.18 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/23/2025 10:46 0.4974.50217.413 10.445 56.7771.647 0.564 0.666 1.9330.0033.454 0.000 0.4850.848 0.344 830.01.730.842 0.000 5.00 0.00 180.0 4/23/2025 10:47 0.7814.32517.455 10.392 49.8050.831 0.519 0.758 1.8600.0002.459 0.000 0.4460.861 0.343 830.01.790.982 0.000 5.11 0.00 180.0 4/23/2025 10:48 0.9524.00217.459 10.415 40.2802.193 0.040 0.673 1.1330.0063.964 0.000 0.4490.703 0.341 830.01.720.888 0.000 4.95 0.00 180.0 4/23/2025 10:49 1.0843.22917.459 10.457 58.6223.567 0.394 0.981 2.1030.0013.142 0.000 0.5340.842 0.366 830.01.920.982 0.000 4.31 0.00 180.0 0.6424.50017.380 10.429 45.9691.761 0.557 0.779 1.3760.0052.515 0.000 0.4680.803 0.365 830.001.8450.974 0.000 5.142 0.000 180.0Avg. 0.5153.78217.361 10.432 47.1391.692 0.513 0.738 1.3220.0082.201 0.000 0.3880.780 0.346 830.001.7611.022 0.000 4.297 0.001 180.0Run 3 Avg: Baseline 3 4/23/2025 10:52 0.0000.1740.024 0.051 0.0420.000 0.006 0.083 0.0000.0030.409 0.000 0.4090.000 0.009 830.00.750.488 0.000 0.17 0.00 180.0 Post CTS 4/23/2025 10:53 0.0000.4220.021 0.039 0.0000.000 0.016 0.000 0.0000.0020.000 98.163 0.0000.000 0.115 830.065.780.164 0.022 0.42 0.00 180.0 4/23/2025 10:53 0.0000.0000.022 0.072 0.0000.000 0.001 0.000 0.0000.0000.000 99.808 0.0000.000 0.141 830.066.860.058 0.024 0.00 0.00 180.0 4/23/2025 10:53 0.0000.0000.030 0.037 0.0000.000 0.022 0.000 0.0000.0000.000 99.957 0.0000.026 0.122 830.066.930.062 0.028 0.00 0.00 180.0 Post NO2/Mid O2 4/23/2025 10:55 98.2254.4640.004 0.017 1.0200.056 1.001 0.066 0.7000.0650.000 0.000 0.0000.197 0.000 830.00.000.000 0.004 102.69 10.55 180.0 4/23/2025 10:55 98.1964.9690.009 0.033 0.9790.074 1.000 0.186 0.8010.0000.000 0.000 0.0460.000 0.014 830.00.070.000 0.000 103.17 10.52 180.0 4/23/2025 10:55 99.4785.1190.016 0.040 0.3470.292 1.013 0.187 0.0000.0000.000 0.000 0.4910.000 0.000 830.00.650.231 0.000 104.60 10.49 180.0 Post 5-Gas 4/23/2025 10:56 0.000244.3520.014 4.903 4.356481.399 1.701 2.176 1.0100.2130.000 1.120 250.5580.290 0.864 830.0254.902.793 9.713 244.35 0.00 180.0 4/23/2025 10:57 0.000245.8270.012 4.907 5.085477.995 1.715 2.265 1.1590.2090.975 1.089 250.9060.000 0.817 830.0254.892.439 9.726 245.83 0.00 180.0 4/23/2025 10:57 0.000245.6800.007 4.917 4.972481.065 1.705 2.188 0.8010.0830.000 1.069 251.4730.233 0.705 830.0255.532.905 9.724 245.68 0.00 180.0 4/23/2025 10:57 0.000245.1930.014 4.884 4.883481.935 1.743 2.291 1.1330.0400.000 1.085 250.9240.257 0.855 830.0255.042.527 9.734 245.19 0.00 180.0 4/23/2025 10:57 0.000244.2050.007 4.933 5.036481.601 1.688 2.031 0.9160.0020.000 1.022 251.5260.274 0.750 830.0255.632.880 9.748 244.20 0.00 180.0 4/23/2025 10:57 0.000247.1180.010 4.899 5.199480.280 1.695 2.162 0.8140.0001.255 1.074 251.6000.281 0.753 830.0255.692.807 9.736 247.12 0.00 180.0 End of Test Purge 4/23/2025 10:59 0.0000.0000.010 0.031 0.0001.413 0.000 0.048 0.0000.0000.532 0.000 1.0590.000 0.000 830.01.390.491 0.013 0.00 0.00 180.0 4/23/2025 10:59 0.0000.9630.005 0.041 0.3680.680 0.000 0.000 0.0240.1550.384 0.000 0.5890.000 0.025 830.00.970.492 0.000 0.96 0.00 180.0 4/23/2025 10:59 0.0000.3730.012 0.045 0.0000.983 0.035 0.000 0.1580.0320.307 0.000 0.6610.000 0.000 830.01.010.521 0.000 0.37 0.00 180.0 4/23/2025 10:59 0.0001.0400.015 0.043 0.9430.692 0.000 0.084 0.0000.0180.021 0.000 0.5940.000 0.062 830.01.030.472 0.000 1.04 0.00 180.0 4/23/2025 10:59 0.0000.9860.006 0.026 0.2660.442 0.000 0.002 0.0000.0000.464 0.000 0.6010.000 0.061 830.01.310.877 0.000 0.99 0.00 180.0 4/23/2025 10:59 0.0000.2160.005 0.017 0.5490.625 0.004 0.000 0.0300.0010.082 0.000 0.4720.532 0.060 830.00.980.577 0.000 0.22 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/23/2025 10:59 0.0000.0000.013 0.030 0.0000.574 0.002 0.119 0.0770.0050.108 0.000 0.6530.000 0.000 830.01.050.599 0.000 0.00 0.00 180.0 4/23/2025 10:59 0.0000.3150.014 0.035 0.1310.529 0.000 0.056 0.0000.0020.507 0.000 0.5050.000 0.002 830.00.830.474 0.000 0.32 0.00 180.0 4/23/2025 11:00 0.0000.6980.006 0.019 0.3450.550 0.002 0.042 0.0000.0010.300 0.000 0.6430.243 0.000 830.00.940.454 0.000 0.70 0.00 179.0 GAS Performance Test Report Test Type: Annual Test Date: 4/24/2025 Waukesha 9394 GSI Rich Burn (4 Cycle) 303 W. 3rd St Elk City , OK 73644(580) 225-0403 Test Started:Test Completed:07:15 AM 10:43 AM Source: Unit Number: 2026-05 Serial Number: 1658713 Engine Hours:12425 Permit #: #DAQE-AN161680001-23 Location: Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, Inc. Residue Booster Station 40 CFR Part 60 Subpart JJJJ CO NOx NMNEHC 5.340 8.863 0.928 2.000 0.300 1.000 0.150 0.700 0.030 0.013 0.035 0.003 Pass Pass Pass Pass Pass Pass Federal State Federal State Federal State Results ppmvd Results g/hp-hr Permit g/hp-hr PASS ALL Index Tables Figures Appendices Table 5.1 (Run Summaries)................................................................ Table 6.1 (Volumetric Flow Rate Data)............................................... Table 6.2 (Stack Gas Measurements)................................................. Table 8.1 (Oxygen Calibration)........................................................... Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... Annex Table 1.2.2 (Measurement System Capabilities)..................... Annex Table 1.3.1 (Test Specific Target Analytes)............................. Annex Table 4.1 (Measure System Capabilities)................................ Figure 6.1 (Location of Traverse Points per Method 1)....................... Annex Figure 1.4.1 (Sampling Train).................................................. Annex Figure 1.4.2 (Sampling Points)................................................. Annex Figure 1.4.3 (Sampling Port Locations).................................... Certified Calibration Bottle Certificates................................................ Tri Probe Certification via GD-031...................................................... GAS ALT 141_FTIR EPA.................................................................... Tester Qualifications (resume)............................................................ Raw Data............................................................................................ 27 Key Personnel.............................................................................1.0 3 Sampling System........................................................................2.0 3 Methods Used.............................................................................3.0 3 Test Summaries..........................................................................4.0 5 Run Summaries..........................................................................5.0 6 6 Volumetric Flow Rate Data.........................................................6.0 7 7 7 7 Calculations................................................................................7.0 8 9 12 12 13 15 13 14 14 20 25 28 29 Oxygen Calibration.....................................................................9 Engine Parameter Data Sheet....................................................10 QA/QC Results............................................................................11 Signature Page...........................................................................12.0 Appendices.................................................................................13.0 Bottle Certs.................................................................................2014.0 Tri Probe Certification via GD-031..............................................2515.0 GAS ALT 141_FTIR EPA............................................................16.0 Tester Qualifications (resume)....................................................2817.0 D6348 Annexes..........................................................................1211.0 18 19 26 8.0 9.0 10.0 Raw Data....................................................................................2918.0 1.0 Key Personnel GAS Crusoe Energy Systems, Inc. 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A EPA Method 2 & 2C EPA Method 3A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. ASTM D6348-03 Jason Woolley 3 Cooper Green GAS 4.0 Test Summary T e s t S u m m a r y Site Verification Photos GAS Unit 2026-05 with a serial number of 1658713 which is a Waukesha 9394 GSI engine located at Residue Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/24/2025 by Cooper Green with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2100 BHP and 1199 RPM which is 84.00% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 2026-05 is authorized to operate under permit #DAQE-AN161680001-23. 4 4.0 Test Summary Engine/Compressor Specs Residue Booster StationLocation 2026-05Unit ID Make Waukesha Site Elevation ft.5450 Model 9394 GSI Atmospheric Pressure psi.11.99 Serial Number 1658713 Stack Diameter in.18 mfg. rated hp 2500 Yes 1200 Date of Manufacture Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1 Test Horsepower 2075 2100 2125 2100 1199 1200 1198 1199 Percent Load % Intake Manifold Pressure (hg) 83.00%84.00%85.00%84.00% 97.14 96.93 98.56 97.55 Intake Manifold Temperature (F)116.40 118.00 119.80 118.07 Ambient Conditions Ambient Temperature Dry (F)58.00 51.00 55.00 54.67 Exhaust Flow Data Q Stack (dscfh) Q Stack (dscm/hr) 152070.34 151630.34 151380.66 151693.78 4306.11 4293.65 4286.58 4295.45 Moisture Fraction Bws Fuel Consumption (Btu/h[-hr) 0.17 0.18 0.18 0.18 0 0 0 0 Fuel Flow (dscfh) Fuel (btu/scf)1020 1020 1020 1020 O2 F factor 8710.0 8710 8710 8710 Results Method 3A Corrected O2% Dry Moisture %17.48%17.53%17.54%17.52% T e s t S u m m a r y mfg. rated rpm Test RPM 0.01%0.00%0.00%0.00% Permitted Standards Results 5 Catalyst Run 1 Run 2 Run 3 3 Run Average Pass Permits 07:15 AM 08:23 AM 09:32 AM 4/24/2025 State NOx (mol wt) 46.01 0.740 0.885 0.671 0.765NMNEHC (ppmvw) 0.897 1.073 0.813 0.928NMNEHC (ppmvd) NMNEHC (mol wt) 44.10 253.218 302.925 229.554 261.899 FailNMNEHC (ppbvd) @15% O2 0.003 0.004 0.003 0.0030.700 0.030 PassNMNEHC (g/hp-hr) 0.253 0.303 0.230 0.262 FailNMNEHC (ppmvd) @15% O2 0.0130.015CO (g/hp-hr)0.010 0.0132.000 0.300 Pass CO (ppmvw)3.258 5.367 4.591 4.405 CO (ppmvd)3.948 6.507 5.567 5.340 CO (mol wt) 28.01 CO (ppmvd) @15% O2 1.115 1.837 1.572 1.508 Fail CO (ppbvd) @15% O2 1114.671 1836.887 1571.612 1507.723 Fail NOx (g/hp-hr)0.035 0.031 0.038 0.0351.000 0.150 Pass NOx (ppmvw)7.292 6.580 8.060 7.311 NOx (ppmvd)8.837 7.978 9.774 8.863 NOx (ppbvd) @15% O2 2495.220 2252.253 2759.437 2502.303 Fail NOx (ppmvd) @15% O2 2.495 2.252 2.759 2.502 Fail GAS GAS 5.0 Run Summaries Summary Source Run 1 R u n Table 5.1 Run Summaries S u m m a r i e s 6 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture % 3.26 0.41 6.97 0.32 7.29 0.00% 0.00% 0.00% 17.48% 6.90 0.34 0.00%17.50% 24.67 1.26 0.00%15.85% 7.04 0.30 0.00%17.46% 0.00 0.00 0.00 0.00%0.04% Avg. Wet NO Summary Source Run 2 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 0.15 0.00 0.00 0.00 0.00%0.04% 5.93 4.84 0.57 5.41 0.00%17.48% 49.19 25.79 0.33 26.13 0.00%15.88% 4.81 7.34 0.41 7.75 0.00%17.58% 0.27 0.17 0.00 0.17 0.00%0.04% Avg. Wet 5.37 6.09 0.49 6.58 0.89 0.00%17.53% NO2NO 0.50 1.10 24.45 0.67 0.32 Summary Source Run 3 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 5.02 7.68 0.29 7.98 0.00%17.59% 48.58 29.49 1.29 30.78 0.00%15.91% 4.17 7.67 0.48 8.15 0.00%17.49% 0.00 0.00 0.00 0.00 0.00%0.04% 0.27 0.17 0.00 0.17 0.32 0.00%0.04% Avg. Wet 4.59 7.68 0.38 8.06 0.67 0.00%17.54% NO2NO 0.21 0.73 22.62 0.61 NMNEHC 0.59 NO2 0.000.33 0.72 22.80 0.76 0.50 0.74 0.41 7.24 25.93 7.34 2.74 3.78 0.15 47.50 6.0 Volumetric Flow Rate Data Volumetric Flow Rate Data .99 Table 6.1. Data used for volumetric flow rate (Method 2) Stack diameter =18 Inches or:1.5 feet or:1.77 Square feet Run 1 Average Pitot Tube Coefficient Cp(std)= H2O CO2 O2 CO Molecular Weight Stack Gas dry basis (Md) Molecular Weight Stack Gas wet basis (Ms) Stack Static Pressure (Pg) Stack Static Pressure (Pg) Atmospheric Pressure at Location (Pbar) Atmospheric Pressure at Location (Pbar) Absolute Stack Pressure (Ps) Stack Temperature Stack Temperature Stack Temperature Stack Gas Velocity Stack Flow Rate Q Stack Gas Wet Volmetric Flow Rate Stack Gas Dry Volumetric Flow Rate Sample after Back Purge: Within 5% of Last Δpstd reading: Stack Diameter (inches) Inches upstream from disturbance Inches downstream from disturbance scf/hr 0.52 Yes 18.00 20.00 19.00 scf/hr cfs ft/sec Deg R Deg F Deg C "Hg "Hg MBAR "Hg "H20 g/g mole g/g mole %d %d %d %17.48 30.01 0.47 Inches 3.01 9 14.99 Vo l u m e t r i c F l o w Ra tes Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 Figure 6.1 16 Traverse Points Were Used Emissions Sampling Points - 3 point long line sampling probe First Sampling Point Taken @ 16.7% of Stack Diameter Second Sampling Point Taken @ 50% of Stack Diameter Third Sampling Point Taken @ 83.3% of Stack Diameter 12.55 0.01 0.00 1009.48 0.03 29.82 29.85 876.25 1335.92 469.03 27.91 73.47 129.82 184283.01 152070.34 Run 2 17.53 30.01 0.46 12.53 0.00 0.00 1010.84 0.03 29.86 29.89 881.25 1340.92 471.81 27.91 72.87 129.83 183852.30 151630.34 Run 3 17.54 30.00 0.51 12.52 0.00 0.00 1010.50 0.04 29.85 29.89 883.25 1342.92 472.92 27.90 76.32 129.83 183578.49 151380.66 17.52 30.01 0.48 12.53 0.00 0.00 1010.27 0.03 29.84 29.88 880.25 1339.92 471.25 27.91 74.23 129.83 183904.6 151693.78 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets. * Cyclonic Flow Check (Pass/Fail): PASS Δpstd (in) H2O 0.47 Exhaust Temp F 876.00 Pitot Tube Sampling Points (Velocity) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Δpstd Average= Run 1 Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate 0.51 0.46 0.51 876.00 877.00 876.00 0.51 0.45 0.38 876.00 876.00 877.00 0.45 0.48 0.57 876.00 876.00 876.00 0.47 877.00 0.46 0.46 0.45 876.00 876.00 876.00 0.46 0.40 0.47 877.00 876.00 876.25 Δpstd = Velocity head measured by the standard pitot tube, (in.) H2O.Run 3 Δpstd (in) H2O 0.49 Exhaust Temp F 883.00 0.50 0.51 0.48 883.00 883.00 884.00 0.49 0.50 0.51 884.00 883.00 883.00 0.55 0.55 0.46 883.00 884.00 883.00 0.50 883.00 0.49 0.52 0.42 883.00 884.00 883.00 0.59 0.52 883.00 883.00 883.250.51 Run 2 Δpstd (in) H2O 0.48 Exhaust Temp F 881.00 0.49 0.54 0.47 881.00 881.00 882.00 0.42 0.34 0.38 882.00 881.00 881.00 0.41 0.43 0.42 881.00 882.00 881.00 0.48 881.00 0.53 0.51 0.49 881.00 882.00 881.00 0.48 0.51 881.00 881.00 0.46 881.25 Pass Strat Check 10.353Check 1 10.369Check 2 10.358Check 3 CO2Gas Used Pass/Fail 7 GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate *Note- Use of this method negates the need for any fuel related numbers for emissions calculations Nomenclature Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293°K (528 °R). Vs = Average stack gas velocity, m/sec (ft./sec). *(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1 Md = .44(12.546)+ .32(.005)+ .28(87.449+0) = 30.01 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO) 12.5 Molecular Weight of Stack Gas. Equation 2-6 Ms = 30.01(1 -.1748)+ 18.0(.1748) = 27.91 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws) 12.6 Average Stack Gas Velocity. Equation 2-7 Vs = 85.49*.99*√.47*√(1335.92/(29.85*27.91)) = 73.47 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms)) 12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8 Qsd = 3600(1-.1748)73.47*1.767((528*29.85)/ (1335.92*29.92)) = 152070.34 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd)) *Standard conversion from feet to meters Q = 152070.34/35.315 = 4306.112 DSCM/HRQ = Qsd/35.315 Emission Rates (Examples use CO Run 1) Nomenclature CO corrected @ 15% O2 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ER = Emission rate of (CO) in g/HP-hr. F(d )= Volumes of combustion components per unit of heat content, scm/J (scf/million Btu). Q = Stack gas volumetric flow rate, in standard cubic meters per hour, dry basis LB/HR.= Emission rate of (CO) in LB/HR. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) O2 = Concentration of oxygen on a dry basis, percent. ppm= Parts Per Million (CO) ppm@15% O2= PPM corrected to 15% O2 Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (DSCF/HR.). Run Time = Run Time in Minutes TPY= Tons per Year Mol wt.= Mol Weight of CO (28.01) Vs = Average stack gas velocity, m/sec (ft./sec). ppm @ 15% O2 = 3.948*(20.9-15)/(20.9-.01%)) = 1.115 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2)) G/HP HR from 40 CFR Part 60 Subpart JJJJ (3.948*(1.164*10^-3)*4306.112*(Run Time/60))/2075 = .01 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR LB/HR from Grams LB/HR = .01*1/453.6*2075 = .044 LB/HRlb/hr = ER*1/453.6*BHP-HR TPY TPY = .044*4.38 = .193 TPYTPY = LB/HR. *4.38 Horsepower HP Provided On Site Wet to Dry PPM 3.95 = 3.2575*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry 8 Cp(std) = Standard pitot tube coefficient; use 0.99 GAS 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span. 8.0 Oxygen Calibration 8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases. (1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration EPA Method 3A QA Worksheet (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Certified Gas Concentraion Low-Level (%) 0.00% Certified Gas Concentraion Mid-Level (%) Certified Gas Concentraion High-Level (%) (DIRECT) Analyzer Calibration Error (≤ 2%) Certified Concentration Value (%) Direct Calibration Response (%) Absolute Difference (%) Analyzer Calibration Error (%)Analyzer Direct Calibration Response Certified bottle value % 0.00% 0.00% 0.00% Zero Gas % Mid-Level Gas % High-Level Gas % Bias Pre Initial Value Bias Post Inital Values System Calibrations Response Pre (%) 0.00% System Bias (% of Span) Pre System Calibration Response Post (%) System Bias (% of Span) Post Drift (% of Span) 0.00%0.00%0.00%0.00% (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Avg. Gas Concentration (Run 1) Avg. Gas Concentration (Run 2) Avg. Gas Concentration (Run 3) Effluent Gas (Cgas) Run 1 Effluent Gas (Cgas) Run 2 Effluent Gas (Cgas) Run 3 Linearity Check 0.00%0.00%0.00% Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Upscale Gas Analyzer Calibration Response (%) Zero Gas Upscale Gas EPA Method 3A QA Worksheet Zero Gas Mid-Level Gas High-Level Gas 100% Nitrogen O2 QA/QC Zero Gas %0.00% Mid-Level Gas % High-Level Gas % System Calibration Response Pre (%) System Calibration Response Post (%) Zero Gas % Upscale Cal Zero Gas % Upscale Cal Upscale Used Upscale Used 10.54% 20.80% 10.54% 10.49% 10.73% 10.73% 10.49%10.54% 10.54% 20.80% 10.73% 21.04% 10.73% 21.04% 10.73%21.04% 0.00% 10.73% 21.04% 0.19% 0.24% 0.92% 1.14% 10.73% Span Zero Offset 0.00% 21.04 0.00% 10.54%0.03%0.21%0.00% 0.01% 0.00% 0.00% 0.01% 0.00% 0.00% 9 GAS 1033.0 1036.0 1031.7 1053.0 1054.0 1051.3 5.6 5.6 5.5 9.0 Engine Parameter Data Sheet Company Site Elevation (ft) Facility Unit ID Date Make Crusoe Energy Systems, Inc. Residue Booster Station 4/24/2025 5450 2026-05 Waukesha Model Serial Number 9394 GSI 1658713 Technician Cooper Green Run Start Times 07:15 AM 08:23 AM 09:32 AM 10:43 AM Run 1 Run 2 Run 3 Completed Engine Parameter Data Run 1 Engine Speed (RPM)1199.0 1200.0 1198.0 1199.0 Engine Hours 12422 12423 12424 12425 Intake Manifold Pressure (psi)59.7 59.6 60.4 59.9 Intake Manifold Temp °F 116.4 118.0 119.8 118.1 Engine Load (BHP)2075.0 2100.0 2125.0 2100.0 Ambient Temp °F 58.0 51.0 55.0 54.7 Humidity %19.0 39.0 33.0 30.3 Dew Point °F 16.0 27.0 27.0 23.3 Yes 2 2 2 2# of Catalyst Installed Catalyst (Yes or No) AFR Setting (Target Left Bank) AFR Setting (Target Right Bank) AFR Manufacturer/Type 10 Run 3 AverageRun 2 Discharge Pressure (psi) Suction Pressure (psi) 1026.0 1047.0 5.2Catalyst Pressure Drop H2O Catalyst Outlet Temp °F Catalyst Inlet Temp °F GAS Waukesha Waukesha Waukesha Waukesha 10.0 QA/QC Results Average:Carbon monoxide CO Gas, Inc. 0.01 R e s u l t s Average:Nitrogen monoxide NO 0.09 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.09 Average:VOC 0.08 Average:Oxygen 0.00 Pre-test Baseline Results Time: Q A / Q C Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.25 Tolerance 2.00% Difference between measured and expected 1.75% CTS Direct to Analyzer Time: Average:Carbon monoxide CO 0.23 Average:Nitrogen monoxide NO 0.06 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.06 Average:VOC 0.38 Average:Oxygen 0.00 Pre-test System Zero Time: Mechanical Response Time 45 seconds Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 97.60 Tolerance 5.00% Difference between measured and expected 2.40% Pre-test System CTS & Mechanical Response Time 49 secondsEquilibration Response Time Value:Spike Reported 250.86 Value:Spike Expected 253.10 System (Equilibration) Response Time Target (Spike) 62 secondsSystem Zero Response Time 62 secondsSystem Response Time System (Zero) Response Time 11 11.0 D6348 Annexes 1-8 D6348 Annexes 1. Test Plan Requirements Annex 1.2 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration NO2 Ethylene SF6 O2 (%) CC524639 12/30/2027 103.00 10.73% CC252676 10/17/2032 100.00 CC433538 8/5/2032 21.04% Cylinder # SG9132842BAL Expiration: 8-20-2032 Propane CO NO SF6 Bottle Value 253.10 497.30 252.90 9.95 Analyzer System Response 250.86 486.99 246.87 9.74 Percent Difference 0.88%2.07%2.38%2.18% Annex Table 1.2.2 Measurement System Capabilities SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.254 4.913 Spike Direct Propane 252.908 Mechanical Response Time SF6 9.834 CO 494.149 NO 250.401 Ethylene 97.595 45 seconds Analyzer Response Propane 250.862 SF6 9.737 CO 486.986 NO 246.870 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 250.162 CO 479.907 NO 246.129 49 seconds 62 seconds 8.63% 9.06% 8.39% 96.35% 98.05% 97.77% 9.700 12 GAS Annex 1.3 Compounds Infrared Analysis Region (cm-1) Expected Concentration Range Measurement System Achievable Minimum Detectable Concentrations Required Measurement System Accuracy and Precision for Test Application CO 2000-2200 0-1200 ppm NO 1875-2138 NO2 2700-2950 VOC 2600-3200 910-1150 2550-2950 CH2O 2550-2850 Interfering Compounds * CO is analyzed in a separate analysis region than CO2 and H2O CO2 Water Vapor 926-1150 3200-3401 Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives 0.16267 ppm 4 ppm 0-1000 ppm 0.4007 ppm 2 ppm 0-100 ppm 0.4899 ppm 2 ppm 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC 0-100 ppm 0.7878 ppm 1 ppm 0-10% 0-22% 0% 0.20% n/a n/a * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. Annex 1.4 Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 13 GAS Sampling Point Locations in Inches 16.7%3.006 50%9.000 83.3%14.994 Figure Annex 1.4.3 Sample Port Location Figure Annex 1.4.2 Sampling Points Interior Stack Diameter (inches): Inches Upstream: Inches Downstream: 18 20 19 14 Stack Gas Dry Volumetric Flow Rate (scf/hr): 151693.78 H2O%d @ Sampling Point:17.52 CO2%d @ Sampling Point:12.53 Pressure @ Sampling Point (Pg "H2O):0.48 Temperature @ Sampling Point (Deg F):880.25 GAS D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1) Target Analyte Results (ppm) CO 0.1627 NO 0.4007 NO2 0.4899 Ethylene 0.3782 Propane 0.4351 Hexane 0.2233 Acetaldehyde 0.8152 Formaldehyde 0.7878 D6348 Annex 3. FTIR Reference Spectra Calibration Transfer Standard Expected Measured Path Length Validated Ethylene 100 98.25 4.913 Passed D6348 Annex 4. Required Pre-Test Procedures Annex Table 1.2.2 Measurement System Capabilities 15 SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.254 4.913 Spike Direct Propane 252.908 Mechanical Response Time SF6 9.834 CO 494.149 NO 250.401 Ethylene 97.595 45 seconds Analyzer Response Propane 250.862 SF6 9.737 CO 486.986 NO 246.870 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 250.162 CO 479.907 NO 246.129 49 seconds 62 seconds 8.63% 9.06% 8.39% 96.35% 98.05% 97.77% 9.700 GAS D6348 Annex 5. Analyte Spiking Technique Propane Spike Direct SF6 CO NO 253.100 9.954 497.300 252.900 252.908 9.834 494.149 250.401 0.08% 1.21% 0.63% 0.99% +/- 2% +/- 2% +/- 2% +/- 2% Pass Pass Pass Pass Parameter Gas Concentration Measured % Difference Specification Validated 0.005 0.000 Spike Average 21.050 0.849 Dilution Factor 8.633% Expected 21.847 % Recovery 96.350% Specification 70-130% <10% Spike Run 1 via the System Source Output Propane SF6 D6348 Annex 6. Determination of System Performance Parameters Noise Equivalent Absorbance (NEA) RMS High RMS Mid RMS Low Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%) 0.000 Spike Average 0.891 Dilution Factor 9.060% Expected % Recovery Specification 70-130% <10% Spike Run 2 via the System Source Output Propane SF6 0.000 Spike Average 0.825 Dilution Factor 8.389% Expected % Recovery Specification 70-130% <10% Spike Run 3 via the System Source Output Propane SF6 0.000 20.762 21.235 97.770% 0.000163 0.000241 0.000508 0.123 22.593 23.042 98.050% Line Position Difference:Resolution Difference to Reference0.00%Pass Pass4.58% 16 GAS Resolution The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. Detector Linerarity The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. D6348 Annex 7. Preparation of Analytical Quantification Algorithm The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 Regression Slope:-6.64362982 Pass Line Position Difference:Resolution Difference to Reference 4.58% D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures CTS Bottle Concentration: CTS Sample Concentration Average: Difference between measured and expected: Tolerance: 100.00 98.72 1.29% 5.00% POST CTS System Check: Run 1 Points 1 & 2 on CO/NO/Propane Run 2 Points 1 & 2 on CO/NO/Propane Run 3 Points 1 & 2 on CO/NO/Propane Run Data Validation - Automated vs Manual Reading Validated Comments All within 20% All within 20% All within 20% Passed Passed Passed Demonstrates no interferences observed. Demonstrates no interferences observed. Demonstrates no interferences observed. 17 GAS 12.0 Signature Page Job/File Name: We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Crusoe Energy Systems, Inc.; Residue Booster Station; 2026-05; JJJJ 18 Company: Print Name: Signature: Title: Phone Number: Date: Company:G.A.S. Inc.Date: Print Name: Title: 4/24/2025 Emissions Specialist Company:G.A.S. Inc.Date: Print Name: Title: Signature: Phone Number: Travis Hartley Director of Stack Testing 580-225-0403 4/24/2025 Cooper Green GAS Appendices GAS GAS Spike (5 Gas) GAS 9% O2/NO2 GAS Ethylene Only GAS BIP GAS 21% O2  ”‡ƒ–Žƒ‹•ƒŽ›–‹…ƒŽ‡”˜‹…‡• ͵Ͳ͵͵”†– Ž‹–›ǡǡ͹͵͸ͶͶ ȋͷͺͲȌʹʹͷǦͲͶͲ͵ ƒšǣȋͷͺͲȌʹʹͷǦʹ͸ͳʹ &(57,),&$7(2)$1$/<6,6 *UDGHRI3URGXFW&(57,),('67$1'$5'352%( 3DUW1XPEHU/5HIHUHQFH 1XPEHU  /DERUDWRU\*$6,1&6WDFN'LDPHWHU $QDO\VLV'DWH7DUJHW)ORZ 5DWH /PLQ /271XPEHU 61 $ $/ 1XPEHURI 3RLQWV  3URGXFWSHUIRUPDQFHYHULILHGE\GLUHFWFRPSDULVRQWRFDOLEUDWLRQVWDQGDUGVWUDFHDEOHWR1,67  7KHSUREHOLVWHGRQWKLVIRUPPHHWVWKHPXOWLSRLQWWUDYHUVHUHTXLUHPHQWRI(3$0HWKRGH VHFWLRQDVVKRZQLQWKHDFFRPSDQ\LQJGDWD0HWKRGHVHFWLRQVWDWHVWKDWWKHPXOWLSRLQW WUDYHUVHUHTXLUHPHQWFDQEHVDWLVILHGE\VDPSOLQJYLD³DPXOWLKROHSUREHGHVLJQHGWRVDPSOHDW WKHSUHVFULEHGSRLQWVZLWKDIORZSHUFHQWRIPHDQIORZUDWH´ $1$/<7,&$/5(68/76 ZƵŶηdŽƚĂů&ůŽǁ ;>ͬŵͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϭͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϮͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϯͿ 0HDQ3UREH 3RUW6DPSOHG )ORZ /P  5XQ/30  䧮    䧮    䧮   5XQ/30  䧮    䧮    䧮    &DOLEUDWLRQFRQGXFWHGLQDFFRUGDQFHZLWK(PLVVLRQ0HDVXUHPHQW&HQWHU*XLGHOLQH'RFXPHQW±(0&*' 1RWHV BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB $SSURYHGIRU5HOHDVH'DWH 2/17/2022 Mr. Jordan Williamson CEO GAS Inc. 303 W. 3rd Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. March 15, 2021 Sincerely, Steffan M. Johnson, Group Leader Measurement Technology Group If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. cc: Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leather.james@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Heather Sessing, Oklahoma DEQ, (Heather.sessing@deq.ok.gov) Cooper Green GAS Type of Sources Tested: info@gasinc.us Stationary Internal Combustion Engines • 4 Stroke Rich Burn Engines • 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods: • EPA Method 1 & 1A – Sampling & Traverse Points • EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream • EPA Method 3A – Oxygen • EPA Method 7E – NOX • EPA Method 10 – Carbon Monoxide • EPA Method 25A – Volatile Organic Compounds • ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. • Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Types of Analyzers: • Gasmet DX4000 FTIR • Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory • Testo 350 • Flame Ionization Detector 580-225-0403 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 1 Minute Average Data Sheet Crusoe Energy Systems, Inc.Client: Residue Booster Station Unit Number:2026-05 Make:Waukesha Location:9394 GSIModel: 1658713Serial Number: RAW Result Data Stability 4/24/2025 05:44 0.0000.0000.001 0.005 0.2480.000 0.000 0.000 0.0480.0000.779 0.058 0.0360.082 0.003 842.00.080.000 0.000 0.00 0.00 180.0 Pre Test Baseline Direct 4/24/2025 05:53 0.0000.233-0.006 0.000 0.0000.025 0.012 0.045 0.0000.0000.004 0.000 0.0000.016 0.000 842.00.060.088 0.000 0.23 0.00 180.0 4/24/2025 05:54 0.0000.046-0.002 0.000 0.0000.000 0.008 0.114 0.0000.1050.113 0.000 0.0000.019 0.000 842.00.050.072 0.000 0.05 0.00 180.0 4/24/2025 05:54 0.0000.0000.001 0.000 0.0000.000 0.016 0.046 0.0000.0350.153 0.000 0.0000.099 0.000 842.00.130.196 0.000 0.00 0.00 180.0 CTS Direct 4/24/2025 05:56 0.0001.0260.010 0.016 0.0000.000 0.000 0.000 0.0690.0750.000 98.400 0.0000.064 0.016 842.065.740.149 0.027 1.03 0.00 180.0 4/24/2025 05:56 0.0000.3580.012 0.017 0.0000.000 0.003 0.000 0.6830.0000.000 98.206 0.0000.000 0.000 842.065.480.013 0.027 0.36 0.00 180.0 4/24/2025 05:57 0.0000.4230.011 0.012 0.0000.000 0.000 0.000 0.3140.0890.000 98.156 0.0000.000 0.000 842.065.450.011 0.028 0.42 0.00 180.0 High O2 Direct 4/24/2025 06:01 0.0000.000-0.002 0.002 0.0000.000 0.000 0.016 0.0580.0000.015 0.000 0.0240.000 0.009 842.00.110.099 0.000 0.00 20.80 180.0 4/24/2025 06:02 0.0000.0000.001 0.001 0.0000.000 0.001 0.000 0.0440.0000.005 0.000 0.0520.000 0.017 842.00.120.057 0.000 0.00 20.81 180.0 4/24/2025 06:02 0.0000.1560.003 0.004 0.0390.000 0.000 0.036 0.0000.0000.000 0.000 0.0000.202 0.007 842.00.030.032 0.000 0.16 20.79 180.0 NO2/Mid O2 Direct 4/24/2025 06:05 102.2230.3130.002 0.000 0.0780.000 0.971 0.000 0.5640.0540.000 0.000 0.0000.084 0.000 842.00.000.000 0.000 102.54 10.50 180.0 4/24/2025 06:06 102.0580.0890.002 0.000 0.2310.000 0.968 0.000 0.6630.0000.000 0.000 0.0000.000 0.000 842.00.000.000 0.000 102.15 10.56 180.0 4/24/2025 06:06 102.5170.0000.002 0.000 0.3020.000 0.987 0.000 0.7580.0730.000 0.000 0.0000.000 0.000 842.00.000.000 0.000 102.52 10.55 180.0 Spike Direct 4/24/2025 06:09 0.000250.276-0.004 4.973 4.470493.072 1.976 2.416 0.5090.1420.028 0.829 252.6430.000 0.858 842.0256.191.923 9.828 250.28 0.00 180.0 4/24/2025 06:09 0.000250.717-0.000 4.981 5.722494.539 1.935 2.377 0.3010.3050.000 0.870 253.0500.609 0.863 842.0256.621.895 9.835 250.72 0.00 180.0 4/24/2025 06:10 0.000250.211-0.002 4.984 4.890494.836 1.891 2.283 0.3680.2380.036 0.838 253.0300.252 0.871 842.0256.812.215 9.840 250.21 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline System 4/24/2025 06:11 0.0000.1840.008 0.042 0.2310.616 0.013 0.000 0.0000.0000.000 0.000 0.3930.058 0.077 842.00.550.000 0.001 0.18 0.00 180.0 4/24/2025 06:12 0.0000.0000.006 0.018 0.1840.052 0.010 0.139 0.0000.0170.000 0.000 0.1970.372 0.038 842.00.360.135 0.000 0.00 0.00 180.0 4/24/2025 06:12 0.0000.0000.007 0.027 0.0000.027 0.009 0.103 0.0000.0010.000 0.000 0.0000.185 0.063 842.00.240.175 0.000 0.00 0.00 180.0 CTS System with Response Time 4/24/2025 06:14 0.0000.0000.013 0.027 0.0000.000 0.000 0.000 0.0000.0000.000 97.495 0.0000.168 0.109 842.065.220.000 0.022 0.00 0.00 180.0 4/24/2025 06:14 0.0000.3860.012 0.026 0.0000.000 0.008 0.000 0.0000.0020.000 97.588 0.0000.120 0.085 842.065.230.000 0.025 0.39 0.00 180.0 4/24/2025 06:14 0.0000.4450.014 0.034 0.0000.000 0.000 0.000 0.0000.0000.000 97.703 0.0000.000 0.058 842.065.290.055 0.023 0.44 0.00 180.0 NO2/Mid O2 System with Response Time 4/24/2025 06:16 100.0263.1520.002 0.004 0.1170.134 0.990 0.107 0.0000.0000.000 0.000 0.0720.000 0.081 842.00.230.000 0.000 103.18 10.53 180.0 4/24/2025 06:17 100.4073.0970.001 0.003 0.0590.213 1.013 0.039 0.1490.0000.000 0.000 0.0960.000 0.024 842.00.140.000 0.000 103.50 10.51 180.0 4/24/2025 06:17 100.2502.818-0.000 0.002 0.2100.000 1.016 0.000 0.0000.0010.000 0.000 0.1480.257 0.021 842.00.190.000 0.000 103.07 10.59 180.0 Spike System with Response Time 4/24/2025 06:19 0.000246.983-0.000 4.948 5.054487.593 1.758 2.156 0.6670.1170.000 1.056 251.0830.246 0.945 842.0255.262.374 9.746 246.98 0.00 180.0 4/24/2025 06:19 0.000246.5650.001 4.937 5.125485.721 1.844 2.199 0.0000.0590.000 1.083 250.6640.054 0.924 842.0254.982.621 9.715 246.57 0.00 179.0 4/24/2025 06:20 0.000247.063-0.000 4.944 4.865487.645 1.851 2.356 0.5850.0370.051 0.973 250.8400.553 0.985 842.0254.992.298 9.749 247.06 0.00 180.0 Baseline System with Response Time 4/24/2025 06:23 0.0001.0770.003 0.013 0.0000.405 0.007 0.096 0.0490.0030.000 0.000 0.3560.138 0.016 842.00.620.353 0.000 1.08 0.00 180.0 4/24/2025 06:23 0.0000.0000.002 0.020 0.3260.273 0.032 0.000 0.0000.0000.000 0.000 0.3930.304 0.002 842.00.710.469 0.001 0.00 0.00 180.0 4/24/2025 06:23 0.0000.1460.003 0.021 0.0000.310 0.038 0.000 0.2020.0150.000 0.000 0.2780.000 0.000 842.00.440.238 0.001 0.15 0.00 180.0 Run 1 - A 30minute/60min 4/24/2025 07:16 0.2645.99715.745 10.553 73.1462.874 1.825 0.250 1.9830.0625.580 0.000 0.0880.818 0.207 830.00.890.586 0.000 6.26 0.00 180.0 4/24/2025 07:17 0.0007.57917.052 10.325 92.8852.703 3.683 0.158 2.0660.0648.312 0.000 0.0000.756 0.139 830.00.860.873 0.000 7.58 0.00 179.0 4/24/2025 07:18 1.1968.33818.007 10.330 55.6252.242 2.340 0.316 1.5340.1237.643 0.000 0.0000.908 0.091 830.00.620.658 0.000 9.53 0.00 180.0 4/24/2025 07:19 0.5858.41917.428 10.379 71.4743.099 2.001 0.549 2.2190.0116.178 0.000 0.0001.022 0.083 830.00.660.744 0.000 9.00 0.00 180.0 4/24/2025 07:20 0.0007.86618.969 10.180 83.6032.627 2.746 1.255 1.7950.0127.630 0.000 0.0000.793 0.120 830.00.830.890 0.000 7.87 0.00 180.0 4/24/2025 07:21 0.7806.12217.650 10.356 76.1841.885 1.930 1.164 2.2980.0974.671 0.000 0.0000.982 0.146 830.00.710.623 0.000 6.90 0.00 180.0 4/24/2025 07:22 0.0004.13217.543 10.473 90.0472.062 2.431 1.007 1.6880.1026.633 0.000 0.0000.792 0.133 830.00.740.715 0.000 4.13 0.00 180.0 4/24/2025 07:23 0.3384.00017.612 10.406 73.5391.845 2.395 1.060 2.3900.1265.904 0.000 0.0001.007 0.119 830.00.560.479 0.000 4.34 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/24/2025 07:24 0.7798.55917.714 10.327 56.7790.856 2.870 0.703 1.6460.0394.340 0.000 0.0000.792 0.069 830.00.600.695 0.000 9.34 0.00 179.0 4/24/2025 07:25 0.5747.88317.804 10.353 54.3101.460 1.344 0.570 1.1650.0624.805 0.000 0.0001.072 0.068 830.00.550.620 0.000 8.46 0.04 180.0 4/24/2025 07:26 0.7948.16517.807 10.369 61.4132.856 1.601 0.667 1.5810.0734.237 0.000 0.0000.691 0.086 830.00.720.817 0.000 8.96 0.00 180.0 4/24/2025 07:27 0.0008.10217.812 10.358 88.8925.191 1.972 1.500 1.7150.0144.368 0.000 0.0000.785 0.104 830.00.850.969 0.000 8.10 0.00 180.0 4/24/2025 07:28 0.0007.87917.741 10.311 97.1544.068 3.191 1.640 2.4690.0015.117 0.000 0.0000.812 0.089 830.00.780.902 0.000 7.88 0.00 180.0 4/24/2025 07:29 0.7498.40117.661 10.374 76.1742.861 2.547 1.243 2.5510.0174.610 0.000 0.0000.966 0.101 830.00.680.717 0.000 9.15 0.00 180.0 4/24/2025 07:30 0.3777.99217.580 10.370 85.9683.400 2.758 1.593 1.6640.0164.508 0.000 0.0680.793 0.153 830.00.880.755 0.000 8.37 0.00 180.0 4/24/2025 07:31 0.0006.64717.501 10.314 108.0264.149 2.770 2.016 2.8290.0555.699 0.000 0.0000.714 0.160 830.00.890.856 0.000 6.65 0.00 180.0 4/24/2025 07:32 0.0958.13317.366 10.306 77.9754.024 4.113 1.935 2.7370.0284.473 0.000 0.0000.884 0.156 830.00.750.657 0.000 8.23 0.00 179.0 4/24/2025 07:33 0.8563.81617.412 10.401 77.0623.380 2.455 1.761 2.2230.0494.892 0.000 0.0000.867 0.105 830.00.610.602 0.000 4.67 0.05 180.0 4/24/2025 07:34 0.0007.56317.426 10.358 92.9962.650 3.380 1.487 2.0910.0164.681 0.000 0.0000.861 0.082 830.00.720.839 0.000 7.56 0.00 180.0 4/24/2025 07:35 0.0008.01317.415 10.382 83.5602.521 3.350 1.454 1.8380.0024.091 0.000 0.0000.883 0.089 830.00.820.960 0.000 8.01 0.00 180.0 4/24/2025 07:36 0.1254.29617.424 10.426 75.8622.540 3.206 1.791 2.6700.0205.250 0.000 0.0000.876 0.094 830.00.720.794 0.000 4.42 0.00 180.0 4/24/2025 07:37 0.5323.63117.486 10.376 77.6271.538 2.336 1.406 2.5740.0115.553 0.000 0.0001.015 0.099 830.00.620.630 0.000 4.16 0.00 180.0 4/24/2025 07:38 0.0007.81017.365 10.364 83.4531.578 3.096 1.162 1.6520.0164.050 0.000 0.0000.529 0.092 830.00.810.942 0.000 7.81 0.00 179.0 4/24/2025 07:39 0.0003.85417.381 10.376 85.9871.027 2.582 1.066 1.5850.0225.265 0.000 0.0000.783 0.078 830.00.670.771 0.000 3.85 0.00 180.0 4/24/2025 07:40 1.0515.97417.380 10.406 72.0390.862 1.784 0.888 2.1270.0205.177 0.000 0.0000.838 0.073 830.00.670.791 0.000 7.02 0.00 180.0 4/24/2025 07:41 0.2169.35217.426 10.370 72.0431.632 2.501 0.779 2.2350.0164.072 0.000 0.0000.875 0.062 830.00.550.639 0.000 9.57 0.00 180.0 4/24/2025 07:42 0.0137.53317.341 10.381 79.6345.277 2.519 1.492 2.5940.0043.505 0.000 0.0001.028 0.089 831.00.720.813 0.000 7.55 0.00 180.0 4/24/2025 07:43 0.1823.82917.355 10.394 75.2884.295 2.243 1.867 2.3150.0104.997 0.000 0.0000.970 0.085 830.00.590.633 0.000 4.01 0.00 180.0 4/24/2025 07:44 0.2847.77517.338 10.394 77.6134.323 3.227 1.874 2.6050.0033.705 0.000 0.0000.851 0.108 831.00.740.790 0.000 8.06 0.00 180.0 4/24/2025 07:45 0.5359.31217.327 10.361 70.8252.337 3.859 1.617 2.5600.0023.483 0.000 0.0000.915 0.067 831.00.700.846 0.000 9.85 0.00 180.0 0.3446.89917.502 10.369 78.2392.739 2.635 1.209 2.1130.0365.114 0.000 0.0050.863 0.105 830.100.7170.754 0.000 7.243 0.003 179.9Avg. Spike 1 4/24/2025 07:47 1.26424.66515.849 9.848 46.82647.496 1.466 0.972 1.2510.0003.487 1.032 21.0500.544 0.262 831.022.800.813 0.849 25.93 0.00 180.0 Run 1 - B 30minute/60min 4/24/2025 07:49 0.0007.76117.416 10.341 99.1626.404 2.549 1.980 2.3580.0074.360 0.000 0.0000.676 0.121 831.00.880.952 0.000 7.76 0.00 180.0 4/24/2025 07:51 0.1663.62217.476 10.350 73.1892.700 2.343 1.646 2.3680.1124.809 0.000 0.0001.052 0.114 830.00.630.607 0.000 3.79 0.00 180.0 4/24/2025 07:52 0.4764.99517.475 10.322 78.6202.134 1.214 1.394 2.9040.0115.368 0.000 0.0140.879 0.051 831.00.650.808 0.000 5.47 0.00 180.0 4/24/2025 07:53 0.0007.27017.479 10.354 93.6012.418 3.234 1.302 2.1480.0034.295 0.000 0.0000.787 0.097 831.00.830.951 0.000 7.27 0.00 180.0 4/24/2025 07:54 0.0007.71117.452 10.379 75.6771.494 2.740 1.114 2.3670.0283.641 0.000 0.0000.971 0.045 831.00.650.837 0.000 7.71 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/24/2025 07:55 0.0008.16917.423 10.352 70.5000.983 2.375 0.857 2.0930.0233.358 0.000 0.0000.808 0.051 831.00.640.810 0.000 8.17 0.00 180.0 4/24/2025 07:56 0.3527.08017.423 10.319 67.1361.265 1.520 0.710 1.8490.0023.557 0.000 0.0000.773 0.073 831.00.690.817 0.000 7.43 0.00 180.0 4/24/2025 07:57 0.0007.18617.431 10.312 91.5181.909 2.205 0.868 2.2460.0013.778 0.000 0.0380.886 0.016 831.00.520.676 0.000 7.19 0.00 180.0 4/24/2025 07:58 0.5207.70317.443 10.358 76.1181.858 2.697 0.942 2.3900.0043.320 0.000 0.0000.851 0.111 831.00.740.771 0.000 8.22 0.00 180.0 4/24/2025 07:59 0.0007.84817.423 10.335 78.9061.152 2.733 0.783 2.4860.0083.764 0.000 0.0000.910 0.127 831.00.820.844 0.000 7.85 0.00 180.0 4/24/2025 08:00 0.0007.50517.440 10.348 84.4200.903 2.328 0.709 1.7240.0243.860 0.000 0.0000.724 0.082 831.00.800.960 0.000 7.50 0.00 180.0 4/24/2025 08:01 0.00010.57117.443 10.346 85.8080.405 2.449 0.511 1.6280.0124.337 0.000 0.0000.623 0.086 831.00.740.856 0.000 10.57 0.00 180.0 4/24/2025 08:02 0.1477.15617.411 10.350 74.2772.121 1.595 0.617 2.3040.0063.902 0.000 0.0000.920 0.097 831.00.710.777 0.000 7.30 0.00 180.0 4/24/2025 08:03 0.5977.14317.422 10.325 80.1025.766 2.299 1.607 2.6980.0123.911 0.000 0.0001.018 0.105 831.00.760.821 0.000 7.74 0.00 180.0 4/24/2025 08:04 0.1287.18817.442 10.346 67.8474.305 2.285 1.692 2.2930.0193.381 0.000 0.0000.988 0.083 831.00.670.760 0.000 7.32 0.00 180.0 4/24/2025 08:05 0.0007.53417.439 10.384 85.9723.871 3.212 1.850 1.8880.0063.689 0.000 0.0000.728 0.106 831.00.810.891 0.000 7.53 0.05 180.0 4/24/2025 08:06 0.0006.82917.460 10.364 87.0283.990 2.584 1.620 1.8730.0003.785 0.000 0.0000.769 0.118 831.00.880.964 0.000 6.83 0.06 180.0 4/24/2025 08:07 0.0004.21417.484 10.339 87.3183.446 2.633 2.056 2.0540.0095.450 0.000 0.1140.662 0.075 831.00.981.071 0.000 4.21 0.06 180.0 4/24/2025 08:08 0.6267.11317.400 10.368 76.0542.036 3.767 1.373 2.9190.0223.477 0.000 0.0000.956 0.162 831.00.810.729 0.000 7.74 0.00 180.0 4/24/2025 08:09 0.3657.62917.421 10.374 42.2910.922 2.292 0.893 1.1060.0132.688 0.000 0.0000.753 0.108 831.00.770.830 0.000 7.99 0.00 180.0 4/24/2025 08:10 1.12512.12317.471 10.321 28.7070.190 1.933 0.516 0.4820.0142.983 0.000 0.0000.707 0.092 831.00.660.719 0.000 13.25 0.00 180.0 4/24/2025 08:11 0.4386.42717.477 10.287 28.3723.976 0.477 0.396 0.6840.0013.528 0.000 0.0000.611 0.076 831.00.700.821 0.000 6.86 0.00 180.0 4/24/2025 08:12 0.7007.87017.483 10.312 45.20610.979 0.715 1.093 0.7940.0472.491 0.000 0.0000.898 0.117 831.00.650.621 0.000 8.57 0.00 180.0 4/24/2025 08:13 0.6175.89817.491 10.332 62.51312.572 1.124 1.919 1.8030.0102.880 0.000 0.0000.935 0.098 831.00.600.606 0.000 6.52 0.00 180.0 4/24/2025 08:14 0.8985.54217.513 10.324 79.32113.183 1.487 2.729 2.4260.0143.448 0.000 0.0000.820 0.107 831.00.820.913 0.000 6.44 0.00 180.0 4/24/2025 08:15 0.0005.87117.505 10.295 96.9739.196 2.390 2.532 2.2950.0003.483 0.000 0.0000.784 0.116 831.00.890.993 0.000 5.87 0.00 180.0 4/24/2025 08:16 0.0006.03017.450 10.288 98.9555.406 2.598 2.149 2.5690.0004.014 0.000 0.0000.900 0.125 831.00.880.946 0.000 6.03 0.00 179.0 4/24/2025 08:17 0.0006.15617.501 10.333 93.4303.755 3.278 1.756 2.3320.0093.468 0.000 0.0360.811 0.160 831.00.950.893 0.000 6.16 0.00 180.0 4/24/2025 08:18 0.7156.60317.514 10.302 70.5231.951 2.828 1.600 2.3090.0003.657 0.000 0.0320.982 0.143 831.00.810.738 0.001 7.32 0.00 180.0 4/24/2025 08:19 1.1136.52117.521 10.341 69.0692.001 2.404 1.337 2.4010.0123.296 0.000 0.0430.756 0.143 831.00.940.923 0.001 7.63 0.00 180.0 0.2997.04217.458 10.337 74.9543.776 2.276 1.352 2.0600.0143.733 0.000 0.0090.831 0.100 830.970.7630.830 0.000 7.341 0.006 180.0Avg. 0.3226.97117.480 10.353 76.5973.258 2.456 1.280 2.0870.0254.423 0.000 0.0070.847 0.103 830.530.7400.792 0.000 7.292 0.004 179.9Run 1 Avg: Baseline 1 4/24/2025 08:21 0.0000.0000.043 0.052 0.0000.149 0.038 0.184 0.0000.0000.000 0.000 0.2510.000 0.000 831.00.500.367 0.000 0.00 0.00 180.0 Run 2 - A 30minute/60min 4/24/2025 08:24 0.5367.27617.434 10.339 58.2612.510 3.222 1.507 1.9240.0172.498 0.000 0.0081.077 0.166 831.00.820.723 0.000 7.81 0.00 180.0 4/24/2025 08:25 0.6256.35517.469 10.309 60.3252.098 2.001 1.411 2.1020.0023.094 0.000 0.0000.667 0.123 831.00.840.894 0.000 6.98 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/24/2025 08:26 0.5157.12317.528 10.299 57.4961.842 1.632 1.128 1.7710.0072.998 0.000 0.0000.949 0.166 831.00.780.664 0.000 7.64 0.00 180.0 4/24/2025 08:27 1.0685.43217.542 10.341 71.6882.516 1.772 1.117 2.4620.0113.138 0.000 0.0000.847 0.166 831.00.860.797 0.000 6.50 0.00 180.0 4/24/2025 08:28 0.4595.89617.540 10.365 87.0975.757 2.517 2.206 2.0680.0153.175 0.000 0.0891.013 0.216 831.01.150.945 0.000 6.36 0.00 180.0 4/24/2025 08:29 0.0006.71117.513 10.318 89.8906.495 2.640 2.615 2.2440.0003.509 0.000 0.0890.725 0.180 831.01.100.978 0.000 6.71 0.00 179.0 4/24/2025 08:30 0.0002.93917.524 10.376 94.1293.794 2.967 2.340 2.5790.0154.389 0.000 0.0600.785 0.172 831.01.030.935 0.000 2.94 0.00 180.0 4/24/2025 08:31 0.7882.83917.524 10.403 90.7701.993 2.324 1.403 2.3850.0004.541 0.000 0.0000.961 0.212 831.01.030.912 0.000 3.63 0.00 180.0 4/24/2025 08:33 0.0006.70817.568 10.380 98.1551.875 3.121 1.203 2.3340.0123.887 0.000 0.1010.794 0.222 831.01.000.686 0.000 6.71 0.00 180.0 4/24/2025 08:34 0.6346.50517.581 10.355 78.3112.252 2.958 1.435 3.0180.0143.704 0.000 0.2880.893 0.206 831.01.290.892 0.000 7.14 0.00 180.0 4/24/2025 08:35 1.0622.04517.545 10.348 74.8952.649 2.173 1.904 2.7120.0084.463 0.000 0.2480.882 0.210 831.01.290.934 0.000 3.11 0.00 180.0 4/24/2025 08:36 1.2942.30717.500 10.348 78.1371.848 2.111 1.589 2.9230.0054.404 0.000 0.1720.853 0.195 831.01.200.958 0.000 3.60 0.00 180.0 4/24/2025 08:37 1.0273.89517.474 10.326 73.8911.325 1.508 1.341 2.7680.0004.251 0.000 0.1550.987 0.178 831.01.130.924 0.000 4.92 0.00 180.0 4/24/2025 08:38 0.0006.22217.444 10.311 87.4902.024 2.927 1.456 2.0250.0133.525 0.000 0.1570.771 0.191 831.01.281.111 0.000 6.22 0.00 179.0 4/24/2025 08:39 1.9665.73517.468 10.353 58.4180.884 3.482 1.176 1.8690.0002.693 0.000 0.2400.824 0.208 831.01.250.896 0.009 7.70 0.00 179.0 4/24/2025 08:40 1.2014.48717.495 10.368 23.6523.506 0.662 0.710 0.5240.0001.656 0.000 0.1840.713 0.195 831.01.080.764 0.000 5.69 0.00 180.0 4/24/2025 08:41 1.3134.88617.457 10.349 48.33319.260 0.503 1.516 1.2990.0002.282 0.000 0.1060.827 0.183 831.01.100.934 0.000 6.20 0.00 180.0 4/24/2025 08:42 0.4663.63917.483 10.365 70.36542.405 0.704 3.244 2.1500.0033.105 0.000 0.1071.130 0.250 831.01.160.829 0.000 4.10 0.00 180.0 4/24/2025 08:43 0.1244.94617.444 10.389 83.52035.256 1.702 5.482 1.6290.0072.724 0.000 0.2070.843 0.276 831.01.420.986 0.000 5.07 0.00 180.0 4/24/2025 08:44 0.0006.37417.422 10.395 90.17818.686 2.525 4.690 2.0520.0023.203 0.000 0.2130.729 0.178 831.01.311.112 0.000 6.37 0.00 180.0 4/24/2025 08:45 0.2075.89717.432 10.358 85.4387.937 3.625 3.422 2.3020.0112.991 0.000 0.2960.857 0.284 831.01.480.930 0.002 6.10 0.00 180.0 4/24/2025 08:46 0.0002.13117.398 10.336 88.9313.227 3.246 2.277 2.3030.0064.541 0.000 0.2340.802 0.189 831.01.381.157 0.000 2.13 0.00 180.0 4/24/2025 08:47 0.8282.77617.400 10.347 65.2671.221 2.471 1.601 2.2920.0004.254 0.000 0.2300.984 0.220 831.01.220.832 0.000 3.60 0.00 180.0 4/24/2025 08:48 0.8043.76417.412 10.337 74.7250.693 1.730 1.273 2.6590.0084.103 0.000 0.1451.007 0.216 831.01.170.896 0.000 4.57 0.00 180.0 4/24/2025 08:49 0.4923.80017.451 10.353 69.2400.645 1.418 1.034 2.2900.0024.516 0.000 0.0670.996 0.203 831.00.890.619 0.000 4.29 0.00 180.0 4/24/2025 08:50 0.1874.31917.477 10.360 73.9430.682 1.762 0.978 2.9110.0104.700 0.000 0.1061.121 0.181 831.00.930.698 0.000 4.51 0.00 180.0 4/24/2025 08:51 0.0006.69817.412 10.350 85.3831.249 2.735 0.832 1.9330.0123.508 0.000 0.0610.966 0.191 831.01.080.951 0.000 6.70 0.00 179.0 4/24/2025 08:52 0.2375.52117.445 10.384 75.5081.379 2.643 0.748 2.7240.0273.103 0.000 0.1140.908 0.157 831.01.080.975 0.000 5.76 0.00 180.0 4/24/2025 08:53 0.5123.00617.438 10.372 78.7880.743 2.065 0.811 2.8380.0144.692 0.000 0.0000.937 0.167 831.00.710.572 0.000 3.52 0.00 180.0 4/24/2025 08:54 0.6664.96417.457 10.363 67.1371.000 1.515 0.945 2.2430.0044.530 0.000 0.0040.768 0.147 831.00.830.802 0.000 5.63 0.00 180.0 0.5674.84017.476 10.353 74.6455.925 2.222 1.780 2.2440.0083.606 0.000 0.1230.887 0.195 831.001.0960.877 0.000 5.407 0.000 179.9Avg. Spike 2 4/24/2025 08:56 0.33425.79115.877 9.869 74.75749.193 1.992 0.720 2.3490.0003.332 0.962 22.5930.872 0.206 831.024.451.206 0.891 26.13 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Run 2 - B 30minute/60min 4/24/2025 08:58 0.4626.76917.453 10.356 55.0541.206 1.775 0.474 1.9190.0143.335 0.000 0.1980.669 0.113 831.01.080.982 0.002 7.23 0.00 180.0 4/24/2025 08:59 0.3366.63517.456 10.367 64.1972.026 1.375 0.561 2.0900.0023.754 0.000 0.0000.846 0.094 831.00.750.838 0.000 6.97 0.00 180.0 4/24/2025 09:00 0.4248.87117.464 10.398 76.8332.859 1.995 0.834 2.6380.0013.400 0.000 0.0000.972 0.118 831.00.620.573 0.000 9.29 0.00 180.0 4/24/2025 09:01 0.8117.22717.483 10.363 59.9831.530 2.392 0.860 2.1020.0003.105 0.000 0.1300.937 0.094 831.00.991.007 0.000 8.04 0.00 180.0 4/24/2025 09:02 0.0636.37417.507 10.347 56.6472.734 0.996 0.774 1.5130.0002.734 0.000 0.0000.832 0.090 831.00.620.665 0.000 6.44 0.00 180.0 4/24/2025 09:03 0.7776.67717.541 10.353 72.0864.490 2.076 1.585 2.2550.0063.343 0.000 0.0000.980 0.096 831.00.600.611 0.000 7.45 0.00 180.0 4/24/2025 09:04 0.3837.15417.565 10.391 61.4212.479 2.081 1.034 1.6820.0003.097 0.000 0.0000.694 0.108 831.00.740.790 0.000 7.54 0.00 180.0 4/24/2025 09:05 0.8397.46617.596 10.364 62.3312.297 2.424 1.027 1.7390.0113.082 0.000 0.0000.757 0.078 831.00.600.669 0.000 8.31 0.00 180.0 4/24/2025 09:06 0.9407.55917.582 10.330 31.9771.449 1.361 0.726 1.0050.0002.354 0.000 0.0000.555 0.042 831.00.550.705 0.000 8.50 0.00 180.0 4/24/2025 09:07 0.8867.01117.626 10.326 45.3093.855 0.765 0.717 1.0140.0002.850 0.000 0.0140.878 0.067 831.00.520.556 0.000 7.90 0.00 180.0 4/24/2025 09:08 0.6376.85317.610 10.333 65.3827.246 1.340 1.743 1.7560.0012.929 0.000 0.0000.674 0.093 831.00.640.681 0.000 7.49 0.00 180.0 4/24/2025 09:09 0.7086.65217.586 10.299 71.6105.002 1.694 1.808 2.0780.0053.069 0.000 0.0000.672 0.112 831.00.680.684 0.000 7.36 0.00 180.0 4/24/2025 09:10 0.6327.84517.589 10.301 69.2813.875 2.405 1.722 2.1510.0023.031 0.000 0.0000.856 0.113 831.00.700.705 0.000 8.48 0.00 180.0 4/24/2025 09:11 0.5636.65217.608 10.282 59.4056.405 1.261 2.139 1.7960.0002.954 0.000 0.0000.796 0.041 831.00.610.785 0.000 7.21 0.00 180.0 4/24/2025 09:12 0.4457.25917.570 10.264 77.8096.542 2.365 2.592 2.4900.0003.604 0.000 0.0001.100 0.079 831.00.660.747 0.000 7.70 0.00 179.0 4/24/2025 09:14 0.0437.71417.594 10.311 75.3704.181 2.359 1.912 2.4210.0023.350 0.000 0.0000.903 0.073 831.00.600.680 0.000 7.76 0.00 180.0 4/24/2025 09:15 0.5607.19717.630 10.291 72.5682.251 2.704 1.432 2.3090.0003.397 0.000 0.0000.892 0.086 831.00.690.780 0.000 7.76 0.00 180.0 4/24/2025 09:16 0.1816.97717.660 10.292 60.5092.063 1.292 0.967 1.4980.0033.246 0.000 0.0000.859 0.060 831.00.600.714 0.000 7.16 0.00 180.0 4/24/2025 09:17 0.0006.46017.630 10.295 86.9104.496 1.606 1.451 1.4680.0053.405 0.000 0.0000.723 0.076 831.00.730.868 0.000 6.46 0.00 180.0 4/24/2025 09:18 0.0007.60117.631 10.308 93.5386.314 2.343 2.647 1.8920.0013.664 0.000 0.0000.739 0.087 831.00.710.809 0.000 7.60 0.00 180.0 4/24/2025 09:19 0.0009.07617.585 10.298 98.7296.359 2.800 2.427 2.1670.0003.652 0.000 0.0000.760 0.089 831.00.800.939 0.000 9.08 0.00 180.0 4/24/2025 09:20 0.0007.88217.571 10.297 97.1345.526 3.056 2.420 2.2560.0014.087 0.000 0.0000.728 0.129 831.00.850.882 0.000 7.88 0.00 180.0 4/24/2025 09:21 0.0007.35917.573 10.304 91.4986.690 3.017 2.654 1.9320.0093.615 0.000 0.0000.850 0.109 831.00.750.794 0.000 7.36 0.00 180.0 4/24/2025 09:22 0.0007.39217.538 10.267 97.3575.356 4.275 2.633 2.4820.0004.221 0.000 0.0000.809 0.096 831.00.840.977 0.000 7.39 0.00 179.0 4/24/2025 09:23 0.0007.38917.591 10.344 72.7662.444 2.528 1.545 2.1500.0003.573 0.000 0.0000.768 0.044 831.00.580.746 0.000 7.39 0.00 180.0 4/24/2025 09:24 0.4787.94917.594 10.335 69.3862.052 2.424 1.144 2.1040.0043.728 0.000 0.0000.930 0.052 831.00.600.740 0.000 8.43 0.00 180.0 4/24/2025 09:25 0.3859.07417.587 10.275 49.3861.491 2.827 1.156 1.4440.0003.258 0.000 0.0050.773 0.058 831.00.590.701 0.000 9.46 0.00 180.0 4/24/2025 09:26 0.7417.05917.636 10.302 22.7455.412 0.584 0.862 0.3280.0002.195 0.000 0.0000.559 0.053 831.00.490.583 0.000 7.80 0.00 180.0 4/24/2025 09:27 0.7616.70217.619 10.326 45.68525.733 0.849 2.520 0.7890.0132.834 0.000 0.0000.648 0.057 831.00.490.564 0.000 7.46 0.00 180.0 4/24/2025 09:28 0.2557.44617.631 10.302 53.6519.865 1.431 2.735 1.5650.0342.845 0.000 0.0000.876 0.061 831.00.540.628 0.000 7.70 0.00 180.0 0.4107.34317.577 10.321 67.2194.808 2.013 1.570 1.8340.0043.257 0.000 0.0120.801 0.082 831.000.6740.747 0.000 7.753 0.000 179.9Avg. 0.4896.09117.526 10.337 70.9325.366 2.118 1.675 2.0390.0063.431 0.000 0.0670.844 0.139 831.000.8850.812 0.000 6.580 0.000 179.9Run 2 Avg: GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline 2 4/24/2025 09:30 0.0000.1730.042 0.039 0.0000.274 0.051 0.223 0.0000.0000.056 0.000 0.1960.000 0.000 831.00.320.192 0.000 0.17 0.00 179.0 Run 3 - A 30minute/60min 4/24/2025 09:32 0.1707.37417.296 10.089 67.2452.233 1.721 1.123 1.9170.0353.650 0.000 0.0000.718 0.100 831.00.740.808 0.000 7.54 0.00 180.0 4/24/2025 09:33 0.0007.33417.610 10.243 86.7862.969 2.157 1.115 1.4030.0133.997 0.000 0.0000.769 0.084 831.00.690.784 0.000 7.33 0.00 180.0 4/24/2025 09:34 0.2388.53317.601 10.283 74.5212.234 3.224 1.221 2.5300.0023.817 0.000 0.0000.957 0.090 831.00.690.766 0.000 8.77 0.00 180.0 4/24/2025 09:35 0.3157.76917.616 10.295 53.0071.780 1.621 0.995 1.2500.0083.164 0.000 0.0000.807 0.093 831.00.780.888 0.000 8.08 0.00 180.0 4/24/2025 09:36 0.3057.71517.676 10.293 67.2862.534 1.667 1.102 1.8730.0003.373 0.000 0.0000.928 0.057 831.00.650.800 0.000 8.02 0.04 180.0 4/24/2025 09:37 0.4158.16217.674 10.305 70.8921.798 2.264 1.065 1.6870.0003.740 0.000 0.0000.998 0.086 831.00.520.517 0.000 8.58 0.00 179.0 4/24/2025 09:38 0.1978.07717.677 10.335 75.1781.992 2.083 0.903 1.7370.0213.660 0.000 0.0001.050 0.098 831.00.570.560 0.000 8.27 0.00 180.0 4/24/2025 09:39 0.0007.70517.628 10.331 91.8923.889 2.048 1.323 1.5910.0583.488 0.000 0.0000.888 0.098 831.00.680.722 0.000 7.71 0.00 180.0 4/24/2025 09:40 0.1547.54017.601 10.322 107.5855.966 3.096 1.743 2.6450.0023.988 0.000 0.0000.875 0.103 831.00.580.561 0.000 7.69 0.00 180.0 4/24/2025 09:41 0.0007.99217.605 10.316 84.7593.289 3.781 1.439 1.5120.0303.321 0.000 0.0000.867 0.089 831.00.530.527 0.000 7.99 0.00 180.0 4/24/2025 09:42 0.0006.86317.624 10.263 64.9191.848 1.530 0.987 1.3690.0023.474 0.000 0.0000.926 0.090 831.00.550.551 0.000 6.86 0.00 180.0 4/24/2025 09:43 0.0007.03017.596 10.280 89.9133.462 1.861 1.266 1.7110.0004.183 0.000 0.0000.726 0.028 831.00.600.812 0.000 7.03 0.00 180.0 4/24/2025 09:44 0.0008.36617.561 10.317 93.7903.477 3.219 1.307 2.2200.0003.545 0.000 0.0000.848 0.072 831.00.800.980 0.000 8.37 0.00 180.0 4/24/2025 09:45 0.4637.91717.593 10.323 73.5012.090 2.497 1.091 1.8510.0003.488 0.000 0.0000.775 0.082 831.00.530.540 0.000 8.38 0.00 180.0 4/24/2025 09:46 0.7477.12917.597 10.303 70.5791.846 1.532 0.892 2.2680.0003.828 0.000 0.0000.870 0.045 831.00.480.584 0.000 7.88 0.00 180.0 4/24/2025 09:47 0.0007.40717.617 10.309 88.5252.852 2.117 1.053 1.8340.0003.879 0.000 0.0000.736 0.024 831.00.440.591 0.000 7.41 0.00 180.0 4/24/2025 09:48 0.2767.28317.582 10.316 86.3873.341 3.134 1.266 1.8680.0283.382 0.000 0.0001.056 0.096 831.00.520.484 0.000 7.56 0.00 180.0 4/24/2025 09:49 0.0007.05617.596 10.304 88.6382.892 2.326 1.183 1.6490.0003.831 0.000 0.0000.842 0.072 831.00.670.789 0.000 7.06 0.00 180.0 4/24/2025 09:50 0.0006.82817.563 10.312 86.8612.568 2.796 1.338 1.5250.0253.690 0.000 0.0000.840 0.096 831.00.770.872 0.000 6.83 0.00 180.0 4/24/2025 09:51 0.8957.47417.582 10.335 74.8981.975 2.723 1.170 2.1640.0003.694 0.000 0.0001.039 0.101 831.00.630.646 0.000 8.37 0.00 180.0 4/24/2025 09:52 0.8687.65717.613 10.318 63.2131.076 2.167 0.732 1.9960.0013.382 0.000 0.0000.865 0.048 831.00.560.695 0.000 8.52 0.00 180.0 4/24/2025 09:53 0.4307.27117.628 10.311 48.5002.662 0.857 0.631 0.9950.0023.683 0.000 0.0000.771 0.026 831.00.420.555 0.000 7.70 0.00 180.0 4/24/2025 09:55 0.0006.82117.590 10.354 79.58616.945 1.024 2.468 2.0600.0023.663 0.000 0.0000.958 0.071 831.00.680.813 0.000 6.82 0.00 180.0 4/24/2025 09:56 0.4088.31617.636 10.352 50.0658.286 2.272 3.125 1.0280.0092.998 0.000 0.0000.983 0.080 831.00.600.664 0.000 8.72 0.00 180.0 4/24/2025 09:57 0.2477.99917.528 10.324 61.86631.079 0.787 3.534 1.3100.0143.328 0.000 0.0001.103 0.102 831.00.570.550 0.000 8.25 0.00 179.0 4/24/2025 09:58 0.7488.83617.495 10.354 64.72316.718 2.947 5.091 1.7060.0003.027 0.000 0.0000.973 0.076 831.00.530.567 0.000 9.58 0.00 180.0 4/24/2025 09:59 0.6609.05017.549 10.304 41.5153.322 2.316 1.976 0.5680.0002.944 0.000 0.0000.768 0.103 831.00.660.676 0.000 9.71 0.00 180.0 4/24/2025 10:00 0.6597.79517.562 10.259 43.5662.585 1.097 1.128 0.6650.0032.862 0.000 0.0000.648 0.067 831.00.520.580 0.000 8.45 0.00 179.0 4/24/2025 10:01 0.6207.76417.613 10.324 60.4093.320 1.337 1.282 1.3840.0033.149 0.000 0.0000.644 0.074 831.00.580.646 0.000 8.38 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/24/2025 10:02 0.0007.39617.580 10.316 95.2939.464 1.583 2.575 1.8210.0003.949 0.000 0.0000.799 0.058 831.00.760.962 0.000 7.40 0.00 180.0 0.2947.68217.590 10.303 73.5305.016 2.126 1.537 1.6710.0093.539 0.000 0.0000.868 0.077 831.000.6100.683 0.000 7.975 0.001 179.9Avg. Spike 3 4/24/2025 10:04 1.28629.49415.907 9.705 72.09948.581 2.754 1.991 2.1940.0003.814 1.151 20.7620.578 0.211 831.022.620.998 0.825 30.78 0.00 180.0 Run 3 - B 30minute/60min 4/24/2025 10:06 0.5669.44117.556 10.326 66.7512.851 2.004 0.976 1.7570.0013.374 0.000 0.2370.785 0.236 831.01.220.760 0.012 10.01 0.00 180.0 4/24/2025 10:07 0.0007.94817.600 10.343 92.3352.707 2.446 1.318 1.5930.0003.645 0.000 0.0000.479 0.090 831.00.820.963 0.000 7.95 0.00 180.0 4/24/2025 10:08 0.0008.32017.607 10.377 90.7352.324 2.764 1.135 1.3000.0004.009 0.000 0.0000.686 0.126 831.00.870.921 0.000 8.32 0.00 180.0 4/24/2025 10:09 0.0003.95417.590 10.388 103.8633.692 2.353 1.454 2.4090.0005.349 0.000 0.0000.489 0.093 831.00.911.087 0.000 3.95 0.00 180.0 4/24/2025 10:10 0.0004.08717.605 10.398 84.0901.882 2.849 1.440 1.3370.0005.296 0.000 0.0000.646 0.109 831.00.700.729 0.000 4.09 0.00 180.0 4/24/2025 10:11 0.7037.81717.471 10.355 54.3944.209 1.445 1.170 0.8780.0002.948 0.000 0.0000.696 0.091 831.00.590.610 0.000 8.52 0.00 179.0 4/24/2025 10:12 1.4218.08517.428 10.343 72.9877.239 2.246 2.797 1.8130.0003.253 0.000 0.0000.920 0.153 831.00.700.590 0.000 9.51 0.00 180.0 4/24/2025 10:13 0.4598.33717.446 10.349 62.5713.367 2.414 1.491 1.3660.0003.146 0.000 0.0000.729 0.143 831.00.760.713 0.000 8.80 0.00 180.0 4/24/2025 10:14 0.7118.58217.465 10.356 61.4282.455 2.489 1.320 1.2360.0223.238 0.000 0.0000.695 0.148 831.00.690.583 0.000 9.29 0.00 180.0 4/24/2025 10:15 0.5498.34417.458 10.378 66.8682.692 1.815 1.146 1.5750.0013.215 0.000 0.0000.961 0.155 831.00.800.730 0.000 8.89 0.04 180.0 4/24/2025 10:16 0.0008.52017.501 10.334 65.7263.025 3.171 1.448 1.5680.0003.369 0.000 0.0000.708 0.102 831.00.580.562 0.000 8.52 0.00 180.0 4/24/2025 10:17 0.5398.30217.545 10.365 41.6612.171 1.365 0.955 0.4510.0002.767 0.000 0.0000.789 0.116 831.00.520.426 0.000 8.84 0.00 180.0 4/24/2025 10:18 0.4545.74517.466 10.372 73.1967.464 0.479 2.012 1.5290.0005.696 0.000 0.0000.925 0.156 832.00.630.471 0.000 6.20 0.00 180.0 4/24/2025 10:19 0.3788.17517.443 10.376 84.2129.077 2.760 2.773 1.1220.0003.339 0.000 0.0000.624 0.152 831.00.710.608 0.000 8.55 0.00 180.0 4/24/2025 10:20 0.4497.96717.417 10.357 80.3606.293 2.953 2.427 2.2500.0013.183 0.000 0.0000.723 0.170 832.00.690.518 0.000 8.42 0.00 180.0 4/24/2025 10:21 0.0008.22517.408 10.323 79.6133.966 4.014 1.917 2.2120.0003.746 0.000 0.0000.705 0.170 832.00.610.404 0.000 8.23 0.00 180.0 4/24/2025 10:22 1.0394.55917.429 10.370 67.3081.767 1.987 1.318 1.6390.0064.645 0.000 0.0000.891 0.177 832.00.730.561 0.000 5.60 0.00 180.0 4/24/2025 10:23 1.2159.14117.452 10.345 40.9361.481 2.576 0.888 0.3420.0192.687 0.000 0.0000.668 0.152 832.00.660.542 0.000 10.36 0.00 180.0 4/24/2025 10:24 0.7498.56817.507 10.308 36.1741.515 1.151 0.583 0.2300.0003.023 0.000 0.0000.711 0.143 832.00.570.424 0.000 9.32 0.00 180.0 4/24/2025 10:25 0.9577.87217.524 10.337 52.2214.434 0.763 0.564 0.6910.0013.502 0.000 0.0000.686 0.126 832.00.590.512 0.000 8.83 0.00 180.0 4/24/2025 10:26 0.9787.95617.510 10.351 76.49412.422 1.634 2.250 1.4960.0003.387 0.000 0.0000.748 0.163 832.00.590.389 0.000 8.93 0.00 180.0 4/24/2025 10:27 0.2266.04517.473 10.358 64.4466.024 0.810 2.175 1.3080.0044.097 0.000 0.0000.544 0.176 832.00.780.648 0.000 6.27 0.00 180.0 4/24/2025 10:28 0.0008.03017.423 10.375 93.22610.445 2.536 3.139 1.5680.0023.287 0.000 0.0000.799 0.195 832.00.900.766 0.000 8.03 0.00 180.0 4/24/2025 10:29 0.0008.38517.433 10.340 72.8285.473 3.568 2.492 2.2800.0003.403 0.000 0.0000.778 0.158 832.00.750.653 0.000 8.39 0.00 180.0 4/24/2025 10:30 0.0008.99617.450 10.346 58.0153.246 2.783 1.612 1.0640.0002.742 0.000 0.0000.656 0.165 832.00.750.623 0.000 9.00 0.00 180.0 4/24/2025 10:31 1.2386.20617.491 10.358 43.0761.826 1.016 1.294 0.3000.0003.928 0.000 0.0000.598 0.184 832.00.810.670 0.000 7.44 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/24/2025 10:32 1.0728.03917.520 10.332 52.9401.849 1.757 0.911 0.7840.0002.877 0.000 0.0000.907 0.161 832.00.640.471 0.000 9.11 0.00 180.0 4/24/2025 10:33 0.0008.57517.427 10.249 51.5401.063 1.903 0.756 0.8800.0002.878 0.000 0.0000.551 0.135 832.00.760.735 0.000 8.58 0.00 179.0 4/24/2025 10:34 0.5327.62217.532 10.323 48.8172.475 0.922 0.568 0.6350.0072.959 0.000 0.0000.513 0.130 832.00.650.592 0.000 8.15 0.00 180.0 4/24/2025 10:35 0.0008.24117.479 10.318 85.8795.519 1.871 1.152 1.0500.0003.241 0.000 0.0000.725 0.212 832.00.960.803 0.000 8.24 0.00 180.0 0.4757.66917.489 10.348 67.4904.165 2.095 1.516 1.2890.0023.541 0.000 0.0080.711 0.150 831.570.7310.635 0.000 8.145 0.001 179.9Avg. 0.3847.67617.539 10.326 70.5104.591 2.110 1.527 1.4800.0053.540 0.000 0.0040.789 0.113 831.280.6710.659 0.000 8.060 0.001 179.9Run 3 Avg: Baseline 3 4/24/2025 10:38 0.0000.0000.041 0.027 0.0000.000 0.000 0.089 0.0000.0020.000 0.000 0.1240.000 0.000 832.00.210.126 0.000 0.00 0.00 180.0 Post CTS 4/24/2025 10:39 0.2360.0000.020 0.013 0.0000.000 0.000 0.000 0.2910.2200.000 97.604 0.0000.000 0.066 832.065.480.416 0.039 0.24 0.00 180.0 4/24/2025 10:39 0.0000.0000.027 0.050 0.0000.000 0.000 0.000 0.0000.0010.000 99.256 0.0000.000 0.057 832.066.480.292 0.019 0.00 0.00 180.0 4/24/2025 10:39 0.0000.0000.023 0.045 0.0300.171 0.030 0.000 0.3330.0000.000 99.308 0.0000.000 0.035 832.066.280.000 0.019 0.00 0.00 180.0 Post NO2/Mid O2 4/24/2025 10:41 98.3465.0980.011 0.010 0.4050.022 1.027 0.000 0.0000.2840.000 0.000 0.1260.270 0.064 832.00.250.000 0.000 103.44 10.51 180.0 4/24/2025 10:41 99.0614.8030.010 0.018 0.3150.152 1.018 0.000 0.0000.0300.000 0.000 0.2170.061 0.040 832.00.300.000 0.000 103.86 10.48 180.0 4/24/2025 10:41 99.6184.7160.002 0.000 0.7550.000 0.983 0.000 0.0000.0030.000 0.000 0.2431.062 0.021 832.00.290.000 0.000 104.33 10.49 180.0 Post 5-Gas 4/24/2025 10:42 0.000245.1200.003 4.890 5.859474.002 1.675 2.311 0.9780.1370.000 1.199 249.2640.830 0.820 832.0253.372.496 9.647 245.12 0.00 180.0 4/24/2025 10:42 0.000245.8530.006 4.918 5.091480.795 1.763 2.366 0.9180.2500.660 1.117 250.3130.150 0.781 832.0254.272.477 9.702 245.85 0.00 180.0 4/24/2025 10:42 0.000246.0950.010 4.855 6.267479.482 1.744 2.298 1.4390.0000.000 1.113 250.0450.523 0.825 832.0254.272.749 9.718 246.09 0.00 180.0 4/24/2025 10:42 0.000247.0440.005 4.934 4.140481.522 1.796 2.136 0.0000.0270.526 1.154 250.3170.000 0.880 832.0254.742.840 9.679 247.04 0.00 179.0 4/24/2025 10:43 0.000246.2670.011 4.861 5.203481.676 1.838 2.164 0.5910.2110.133 1.089 250.7980.411 0.866 832.0254.622.040 9.732 246.27 0.00 180.0 4/24/2025 10:43 0.000246.3920.008 4.863 4.508481.963 1.718 2.097 2.1280.0020.711 1.100 250.2340.000 0.759 832.0254.352.794 9.724 246.39 0.00 180.0 End of Test Purge 4/24/2025 10:44 0.0000.8800.003 0.010 0.0001.381 0.000 0.110 0.0000.2020.000 0.000 0.8080.000 0.042 832.00.950.082 0.019 0.88 0.00 180.0 4/24/2025 10:44 0.0001.0110.004 0.006 0.3381.094 0.022 0.217 0.0000.0000.000 0.000 0.6830.000 0.036 832.00.870.170 0.009 1.01 0.00 180.0 4/24/2025 10:44 0.0000.725-0.000 0.000 0.0000.437 0.006 0.110 0.0510.0010.445 0.000 0.5910.000 0.033 832.00.690.044 0.008 0.72 0.00 180.0 4/24/2025 10:45 0.0001.0340.002 0.000 0.0000.370 0.033 0.097 0.0760.0000.000 0.000 0.2640.000 0.096 832.00.710.386 0.006 1.03 0.00 180.0 4/24/2025 10:45 0.5330.618-0.000 0.020 0.0000.485 0.000 0.054 0.0800.0000.000 0.000 0.3790.000 0.000 832.00.580.302 0.006 1.15 0.00 180.0 4/24/2025 10:45 0.2850.0000.011 0.015 0.2870.705 0.010 0.105 0.0000.0000.000 0.000 0.3410.000 0.104 832.00.550.000 0.000 0.28 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/24/2025 10:45 0.6050.000-0.000 0.012 0.1470.341 0.033 0.020 0.0000.0000.000 0.026 0.2990.960 0.000 832.00.320.000 0.000 0.61 0.00 180.0 4/24/2025 10:45 0.0001.0020.005 0.004 0.0000.491 0.007 0.004 0.0990.0290.000 0.000 0.1260.000 0.074 832.00.370.140 0.000 1.00 0.00 180.0 4/24/2025 10:45 0.0000.3310.006 0.002 0.0000.494 0.066 0.226 0.2190.0740.000 0.000 0.0890.974 0.000 832.00.090.000 0.000 0.33 0.00 180.0 GAS Performance Test Report Test Type: Annual Test Date: 4/22/2025 Waukesha 9394 GSI Rich Burn (4 Cycle) 303 W. 3rd St Elk City , OK 73644(580) 225-0403 Test Started:Test Completed:07:35 AM 11:14 AM Source: Unit Number: 2026-07 Serial Number: 1662642 Engine Hours:12331 Permit #: #DAQE-AN161680001-23 Location: Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, Inc. Residue Booster Station 40 CFR Part 60 Subpart JJJJ CO NOx NMNEHC 1.652 10.748 0.861 2.000 0.300 1.000 0.150 0.700 0.030 0.005 0.051 0.004 Pass Pass Pass Pass Pass Pass Federal State Federal State Federal State Results ppmvd Results g/hp-hr Permit g/hp-hr PASS ALL Index Tables Figures Appendices Table 5.1 (Run Summaries)................................................................ Table 6.1 (Volumetric Flow Rate Data)............................................... Table 6.2 (Stack Gas Measurements)................................................. Table 8.1 (Oxygen Calibration)........................................................... Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... Annex Table 1.2.2 (Measurement System Capabilities)..................... Annex Table 1.3.1 (Test Specific Target Analytes)............................. Annex Table 4.1 (Measure System Capabilities)................................ Figure 6.1 (Location of Traverse Points per Method 1)....................... Annex Figure 1.4.1 (Sampling Train).................................................. Annex Figure 1.4.2 (Sampling Points)................................................. Annex Figure 1.4.3 (Sampling Port Locations).................................... Certified Calibration Bottle Certificates................................................ Tri Probe Certification via GD-031...................................................... GAS ALT 141_FTIR EPA.................................................................... Tester Qualifications (resume)............................................................ Raw Data............................................................................................ 27 Key Personnel.............................................................................1.0 3 Sampling System........................................................................2.0 3 Methods Used.............................................................................3.0 3 Test Summaries..........................................................................4.0 5 Run Summaries..........................................................................5.0 6 6 Volumetric Flow Rate Data.........................................................6.0 7 7 7 7 Calculations................................................................................7.0 8 9 12 12 13 15 13 14 14 20 25 28 29 Oxygen Calibration.....................................................................9 Engine Parameter Data Sheet....................................................10 QA/QC Results............................................................................11 Signature Page...........................................................................12.0 Appendices.................................................................................13.0 Bottle Certs.................................................................................2014.0 Tri Probe Certification via GD-031..............................................2515.0 GAS ALT 141_FTIR EPA............................................................16.0 Tester Qualifications (resume)....................................................2817.0 D6348 Annexes..........................................................................1211.0 18 19 26 8.0 9.0 10.0 Raw Data....................................................................................2918.0 1.0 Key Personnel GAS Crusoe Energy Systems, Inc. 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A EPA Method 2 & 2C EPA Method 3A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. ASTM D6348-03 Jason Woolley 3 Cooper Green GAS 4.0 Test Summary T e s t S u m m a r y Site Verification Photos GAS Unit 2026-07 with a serial number of 1662642 which is a Waukesha 9394 GSI engine located at Residue Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/22/2025 by Cooper Green with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2325 BHP and 1199 RPM which is 93.00% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 2026-07 is authorized to operate under permit #DAQE-AN161680001-23. 4 4.0 Test Summary Engine/Compressor Specs Residue Booster StationLocation 2026-07Unit ID Make Waukesha Site Elevation ft.5456 Model 9394 GSI Atmospheric Pressure psi.11.96 Serial Number 1662642 Stack Diameter in.21 mfg. rated hp 2500 Yes 1200 Date of Manufacture Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1 Test Horsepower 2325 2350 2300 2325 1198 1198 1200 1199 Percent Load % Intake Manifold Pressure (hg) 93.00%94.00%92.00%93.00% 109.82 112.06 110.43 110.77 Intake Manifold Temperature (F)120.00 123.80 126.00 123.27 Ambient Conditions Ambient Temperature Dry (F)41.00 48.00 54.00 47.67 Exhaust Flow Data Q Stack (dscfh) Q Stack (dscm/hr) 206986.47 205222.21 204825.01 205677.90 5861.15 5811.19 5799.94 5824.09 Moisture Fraction Bws Fuel Consumption (Btu/h[-hr) 0.17 0.17 0.17 0.17 0 0 0 0 Fuel Flow (dscfh) Fuel (btu/scf)1020 1020 1020 1020 O2 F factor 8710.0 8710 8710 8710 Results Method 3A Corrected O2% Dry Moisture %17.40%17.39%17.38%17.39% T e s t S u m m a r y mfg. rated rpm Test RPM 0.00%0.00%0.00%0.00% Permitted Standards Results 5 Catalyst Run 1 Run 2 Run 3 3 Run Average Pass Permits 07:35 AM 08:43 AM 10:01 AM 4/22/2025 State NOx (mol wt) 46.01 0.684 0.776 0.674 0.711NMNEHC (ppmvw) 0.828 0.939 0.816 0.861NMNEHC (ppmvd) NMNEHC (mol wt) 44.10 233.615 265.028 230.297 242.980 FailNMNEHC (ppbvd) @15% O2 0.004 0.004 0.004 0.0040.700 0.030 PassNMNEHC (g/hp-hr) 0.234 0.265 0.230 0.243 FailNMNEHC (ppmvd) @15% O2 0.0060.005CO (g/hp-hr)0.003 0.0052.000 0.300 Pass CO (ppmvw)0.751 1.536 1.807 1.364 CO (ppmvd)0.909 1.859 2.187 1.652 CO (mol wt) 28.01 CO (ppmvd) @15% O2 0.257 0.525 0.617 0.466 Fail CO (ppbvd) @15% O2 256.686 524.758 617.258 466.234 Fail NOx (g/hp-hr)0.051 0.054 0.050 0.0511.000 0.150 Pass NOx (ppmvw)8.747 9.358 8.531 8.878 NOx (ppmvd)10.589 11.328 10.326 10.748 NOx (ppbvd) @15% O2 2989.483 3197.931 2914.932 3034.115 Fail NOx (ppmvd) @15% O2 2.989 3.198 2.915 3.034 Fail GAS GAS 5.0 Run Summaries Summary Source Run 1 R u n Table 5.1 Run Summaries S u m m a r i e s 6 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture % 0.75 0.00 8.57 0.17 8.75 0.00% 0.00% 0.00% 17.40% 8.21 0.20 0.00%17.38% 25.99 2.26 0.00%14.39% 8.94 0.15 0.00%17.43% 0.00 0.00 0.00 0.00%0.04% Avg. Wet NO Summary Source Run 2 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 0.00 0.00 0.00 0.00 0.00%0.04% 2.25 11.29 0.22 11.51 0.00%17.42% 47.66 26.27 0.54 26.81 0.00%15.84% 0.82 6.80 0.41 7.21 0.00%17.37% 0.00 0.00 0.00 0.00 0.00%0.04% Avg. Wet 1.54 9.04 0.31 9.36 0.78 0.00%17.39% NO2NO 0.61 0.75 23.47 0.80 0.75 Summary Source Run 3 Baseline Source Spike Source Baseline PPM Wet CO NOx Oxygen %Moisture %NMNEHC 2.23 9.04 0.40 9.43 0.00%17.38% 46.87 26.89 0.60 27.49 0.00%15.87% 1.38 7.36 0.27 7.63 0.00%17.39% 0.00 0.00 0.00 0.00 0.00%0.04% 0.00 0.00 0.00 0.00 0.75 0.00%0.04% Avg. Wet 1.81 8.20 0.33 8.53 0.67 0.00%17.38% NO2NO 0.50 0.67 23.02 0.68 NMNEHC 0.58 NO2 0.000.00 0.68 25.12 0.69 0.61 0.68 0.00 8.41 28.24 9.09 0.70 0.80 0.00 50.78 6.0 Volumetric Flow Rate Data Volumetric Flow Rate Data .99 Table 6.1. Data used for volumetric flow rate (Method 2) Stack diameter =21 Inches or:1.75 feet or:2.41 Square feet Run 1 Average Pitot Tube Coefficient Cp(std)= H2O CO2 O2 CO Molecular Weight Stack Gas dry basis (Md) Molecular Weight Stack Gas wet basis (Ms) Stack Static Pressure (Pg) Stack Static Pressure (Pg) Atmospheric Pressure at Location (Pbar) Atmospheric Pressure at Location (Pbar) Absolute Stack Pressure (Ps) Stack Temperature Stack Temperature Stack Temperature Stack Gas Velocity Stack Flow Rate Q Stack Gas Wet Volmetric Flow Rate Stack Gas Dry Volumetric Flow Rate Sample after Back Purge: Within 5% of Last Δpstd reading: Stack Diameter (inches) Inches upstream from disturbance Inches downstream from disturbance scf/hr 0.57 Yes 21.00 20.00 15.00 scf/hr cfs ft/sec Deg R Deg F Deg C "Hg "Hg MBAR "Hg "H20 g/g mole g/g mole %d %d %d %17.40 30.01 0.47 Inches 3.51 10.5 17.49 Vo l u m e t r i c F l o w Ra tes Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 Figure 6.1 16 Traverse Points Were Used Emissions Sampling Points - 3 point long line sampling probe First Sampling Point Taken @ 16.7% of Stack Diameter Second Sampling Point Taken @ 50% of Stack Diameter Third Sampling Point Taken @ 83.3% of Stack Diameter 12.56 0.00 0.00 1015.58 0.03 30.00 30.03 886.25 1345.92 474.58 27.92 73.51 176.79 250595.01 206986.47 Run 2 17.39 30.00 0.51 12.53 0.00 0.00 1014.56 0.04 29.97 30.01 897.25 1356.92 480.69 27.91 76.60 176.81 248428.98 205222.21 Run 3 17.38 30.01 0.52 12.56 0.00 0.00 1013.21 0.04 29.93 29.97 898.25 1357.92 481.25 27.92 77.61 176.81 247915.15 204825.01 17.39 30.01 0.50 12.55 0.00 0.00 1014.45 0.04 29.97 30.00 893.92 1353.59 478.84 27.92 75.92 176.81 248979.71 205677.9 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets. * Cyclonic Flow Check (Pass/Fail): PASS Δpstd (in) H2O 0.47 Exhaust Temp F 886.00 Pitot Tube Sampling Points (Velocity) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Δpstd Average= Run 1 Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate 0.46 0.41 0.42 886.00 887.00 886.00 0.45 0.46 0.44 886.00 886.00 887.00 0.44 0.49 0.49 886.00 886.00 887.00 0.47 886.00 0.52 0.57 0.47 886.00 886.00 887.00 0.43 0.47 0.47 886.00 886.00 886.25 Δpstd = Velocity head measured by the standard pitot tube, (in.) H2O.Run 3 Δpstd (in) H2O 0.62 Exhaust Temp F 898.00 0.57 0.58 0.53 898.00 898.00 899.00 0.48 0.47 0.46 898.00 898.00 898.00 0.48 0.55 0.55 899.00 898.00 898.00 0.49 898.00 0.49 0.48 0.50 899.00 898.00 898.00 0.47 0.57 898.00 899.00 898.250.52 Run 2 Δpstd (in) H2O 0.54 Exhaust Temp F 897.00 0.55 0.52 0.45 897.00 897.00 898.00 0.48 0.54 0.46 898.00 897.00 897.00 0.47 0.52 0.51 897.00 898.00 897.00 0.46 897.00 0.50 0.49 0.55 897.00 898.00 897.00 0.55 0.50 897.00 897.00 0.51 897.25 Pass Strat Check 10.382Check 1 10.357Check 2 10.374Check 3 CO2Gas Used Pass/Fail 7 GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate *Note- Use of this method negates the need for any fuel related numbers for emissions calculations Nomenclature Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293°K (528 °R). Vs = Average stack gas velocity, m/sec (ft./sec). *(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1 Md = .44(12.56)+ .32(.001)+ .28(87.439+0) = 30.01 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO) 12.5 Molecular Weight of Stack Gas. Equation 2-6 Ms = 30.01(1 -.17402)+ 18.0(.17402) = 27.92 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws) 12.6 Average Stack Gas Velocity. Equation 2-7 Vs = 85.49*.99*√.47*√(1345.92/(30.03*27.92)) = 73.51 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms)) 12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8 Qsd = 3600(1-.17402)73.51*2.405((528*30.03)/ (1345.92*29.92)) = 206986.47 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd)) *Standard conversion from feet to meters Q = 206986.466/35.315 = 5861.149 DSCM/HRQ = Qsd/35.315 Emission Rates (Examples use CO Run 1) Nomenclature CO corrected @ 15% O2 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ER = Emission rate of (CO) in g/HP-hr. F(d )= Volumes of combustion components per unit of heat content, scm/J (scf/million Btu). Q = Stack gas volumetric flow rate, in standard cubic meters per hour, dry basis LB/HR.= Emission rate of (CO) in LB/HR. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) O2 = Concentration of oxygen on a dry basis, percent. ppm= Parts Per Million (CO) ppm@15% O2= PPM corrected to 15% O2 Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (DSCF/HR.). Run Time = Run Time in Minutes TPY= Tons per Year Mol wt.= Mol Weight of CO (28.01) Vs = Average stack gas velocity, m/sec (ft./sec). ppm @ 15% O2 = .909*(20.9-15)/(20.9-0%)) = .257 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2)) G/HP HR from 40 CFR Part 60 Subpart JJJJ (.909*(1.164*10^-3)*5861.149*(Run Time/60))/2325 = .003 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR LB/HR from Grams LB/HR = .003*1/453.6*2325 = .014 LB/HRlb/hr = ER*1/453.6*BHP-HR TPY TPY = .014*4.38 = .061 TPYTPY = LB/HR. *4.38 Horsepower HP Provided On Site Wet to Dry PPM .91 = .751*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry 8 Cp(std) = Standard pitot tube coefficient; use 0.99 GAS 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span. 8.0 Oxygen Calibration 8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases. (1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration EPA Method 3A QA Worksheet (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Certified Gas Concentraion Low-Level (%) 0.00% Certified Gas Concentraion Mid-Level (%) Certified Gas Concentraion High-Level (%) (DIRECT) Analyzer Calibration Error (≤ 2%) Certified Concentration Value (%) Direct Calibration Response (%) Absolute Difference (%) Analyzer Calibration Error (%)Analyzer Direct Calibration Response Certified bottle value % 0.00% 0.00% 0.00% Zero Gas % Mid-Level Gas % High-Level Gas % Bias Pre Initial Value Bias Post Inital Values System Calibrations Response Pre (%) 0.00% System Bias (% of Span) Pre System Calibration Response Post (%) System Bias (% of Span) Post Drift (% of Span) 0.00%0.00%0.00%0.00% (SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%) Avg. Gas Concentration (Run 1) Avg. Gas Concentration (Run 2) Avg. Gas Concentration (Run 3) Effluent Gas (Cgas) Run 1 Effluent Gas (Cgas) Run 2 Effluent Gas (Cgas) Run 3 Linearity Check 0.00%0.00%0.00% Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Upscale Gas Analyzer Calibration Response (%) Zero Gas Upscale Gas EPA Method 3A QA Worksheet Zero Gas Mid-Level Gas High-Level Gas 100% Nitrogen O2 QA/QC Zero Gas %0.00% Mid-Level Gas % High-Level Gas % System Calibration Response Pre (%) System Calibration Response Post (%) Zero Gas % Upscale Cal Zero Gas % Upscale Cal Upscale Used Upscale Used 10.63% 20.75% 10.61% 10.46% 10.73% 10.73% 10.46%10.61% 10.63% 20.75% 10.73% 21.04% 10.73% 21.04% 10.73%21.04% 0.00% 10.73% 21.04% 0.10% 0.29% 0.49% 1.38% 10.73% Span Zero Offset 0.00% 21.04 0.00% 10.63%0.07%0.81%0.01% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 9 GAS 1020.0 1022.0 1017.7 1063.0 1063.0 1060.7 6.0 6.0 6.0 9.0 Engine Parameter Data Sheet Company Site Elevation (ft) Facility Unit ID Date Make Crusoe Energy Systems, Inc. Residue Booster Station 4/22/2025 5456 2026-07 Waukesha Model Serial Number 9394 GSI 1662642 Technician Cooper Green Run Start Times 07:35 AM 08:43 AM 10:01 AM 11:14 AM Run 1 Run 2 Run 3 Completed Engine Parameter Data Run 1 Engine Speed (RPM)1198.0 1198.0 1200.0 1198.7 Engine Hours 12328 12329 12330 12331 Intake Manifold Pressure (psi)65.9 67.0 66.2 66.4 Intake Manifold Temp °F 120.0 123.8 126.0 123.3 Engine Load (BHP)2325.0 2350.0 2300.0 2325.0 Ambient Temp °F 41.0 48.0 54.0 47.7 Humidity %42.0 34.0 25.0 33.7 Dew Point °F 20.0 21.0 19.0 20.0 Waukesha Yes 2 2 2 2# of Catalyst Installed Catalyst (Yes or No) AFR Setting (Target Left Bank) AFR Setting (Target Right Bank) AFR Manufacturer/Type Waukesha Waukesha Waukesha 10 Run 3 AverageRun 2 Discharge Pressure (psi) Suction Pressure (psi) 1011.0 1056.0 6.0Catalyst Pressure Drop H2O Catalyst Outlet Temp °F Catalyst Inlet Temp °F GAS 10.0 QA/QC Results Average:Carbon monoxide CO Gas, Inc. 0.00 R e s u l t s Average:Nitrogen monoxide NO 0.00 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.00 Average:VOC 0.10 Average:Oxygen 0.00 Pre-test Baseline Results Time: Q A / Q C Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 98.90 Tolerance 2.00% Difference between measured and expected 1.10% CTS Direct to Analyzer Time: Average:Carbon monoxide CO 0.00 Average:Nitrogen monoxide NO 0.00 Average:Nitrogen dioxide NO2 0.00 Average:NOx 0.00 Average:VOC 0.58 Average:Oxygen 0.00 Pre-test System Zero Time: Mechanical Response Time 45 seconds Value:CTS Bottle Concentration 100.00 Value:CTS Compound Concentration Avg 97.96 Tolerance 5.00% Difference between measured and expected 2.04% Pre-test System CTS & Mechanical Response Time 79 secondsEquilibration Response Time Value:Spike Reported 251.54 Value:Spike Expected 253.10 System (Equilibration) Response Time Target (Spike) 50 secondsSystem Zero Response Time 79 secondsSystem Response Time System (Zero) Response Time 11 11.0 D6348 Annexes 1-8 D6348 Annexes 1. Test Plan Requirements Annex 1.2 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration NO2 Ethylene SF6 O2 (%) CC524639 12/30/2027 103.00 10.73% CC252676 10/17/2032 100.00 CC433538 8/5/2032 21.04% Cylinder # SG9132842BAL Expiration: 8-20-2032 Propane CO NO SF6 Bottle Value 253.10 497.30 252.90 9.95 Analyzer System Response 251.54 485.93 247.28 9.73 Percent Difference 0.62%2.29%2.22%2.29% Annex Table 1.2.2 Measurement System Capabilities SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.902 4.945 Spike Direct Propane 252.513 Mechanical Response Time SF6 9.789 CO 490.549 NO 251.228 Ethylene 97.963 36 seconds Analyzer Response Propane 251.541 SF6 9.726 CO 485.931 NO 247.275 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 250.532 CO 477.717 NO 245.621 79 seconds 50 seconds 9.50% 8.72% 8.57% 97.98% 98.62% 98.17% 9.694 12 GAS Annex 1.3 Compounds Infrared Analysis Region (cm-1) Expected Concentration Range Measurement System Achievable Minimum Detectable Concentrations Required Measurement System Accuracy and Precision for Test Application CO 2000-2200 0-1200 ppm NO 1875-2138 NO2 2700-2950 VOC 2600-3200 910-1150 2550-2950 CH2O 2550-2850 Interfering Compounds * CO is analyzed in a separate analysis region than CO2 and H2O CO2 Water Vapor 926-1150 3200-3401 Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives 0.16267 ppm 4 ppm 0-1000 ppm 0.4007 ppm 2 ppm 0-100 ppm 0.4899 ppm 2 ppm 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC 0-100 ppm 0.7878 ppm 1 ppm 0-10% 0-22% 0% 0.20% n/a n/a * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. Annex 1.4 Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 13 GAS Sampling Point Locations in Inches 16.7%3.507 50%10.500 83.3%17.493 Figure Annex 1.4.3 Sample Port Location Figure Annex 1.4.2 Sampling Points Interior Stack Diameter (inches): Inches Upstream: Inches Downstream: 21 20 15 14 Stack Gas Dry Volumetric Flow Rate (scf/hr): 205677.9 H2O%d @ Sampling Point:17.39 CO2%d @ Sampling Point:12.55 Pressure @ Sampling Point (Pg "H2O):0.5 Temperature @ Sampling Point (Deg F):893.92 GAS D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1) Target Analyte Results (ppm) CO 0.1627 NO 0.4007 NO2 0.4899 Ethylene 0.3782 Propane 0.4351 Hexane 0.2233 Acetaldehyde 0.8152 Formaldehyde 0.7878 D6348 Annex 3. FTIR Reference Spectra Calibration Transfer Standard Expected Measured Path Length Validated Ethylene 100 98.9 4.945 Passed D6348 Annex 4. Required Pre-Test Procedures Annex Table 1.2.2 Measurement System Capabilities 15 SF6 Parameter Measured Gas Concentration (ppm)Path Length Equilibration Time Dilution Factor % Recovery Path Length Ethylene 98.902 4.945 Spike Direct Propane 252.513 Mechanical Response Time SF6 9.789 CO 490.549 NO 251.228 Ethylene 97.963 36 seconds Analyzer Response Propane 251.541 SF6 9.726 CO 485.931 NO 247.275 Analyte Spike Recovery Propane & SF6 System Zero Nitrogen Post Spike System Propane 250.532 CO 477.717 NO 245.621 79 seconds 50 seconds 9.50% 8.72% 8.57% 97.98% 98.62% 98.17% 9.694 GAS D6348 Annex 5. Analyte Spiking Technique Propane Spike Direct SF6 CO NO 253.100 9.954 497.300 252.900 252.513 9.789 490.549 251.228 0.23% 1.66% 1.36% 0.66% +/- 2% +/- 2% +/- 2% +/- 2% Pass Pass Pass Pass Parameter Gas Concentration Measured % Difference Specification Validated 0.000 0.000 Spike Average 23.559 0.930 Dilution Factor 9.500% Expected 24.045 % Recovery 97.980% Specification 70-130% <10% Spike Run 1 via the System Source Output Propane SF6 D6348 Annex 6. Determination of System Performance Parameters Noise Equivalent Absorbance (NEA) RMS High RMS Mid RMS Low Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%) 0.000 Spike Average 0.854 Dilution Factor 8.724% Expected % Recovery Specification 70-130% <10% Spike Run 2 via the System Source Output Propane SF6 0.000 Spike Average 0.839 Dilution Factor 8.571% Expected % Recovery Specification 70-130% <10% Spike Run 3 via the System Source Output Propane SF6 0.000 21.294 21.691 98.170% 0.000088 0.000056 0.000150 0.000 21.765 22.070 98.620% Line Position Difference:Resolution Difference to Reference0.00%Pass Pass4.14% 16 GAS Resolution The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. Detector Linerarity The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. D6348 Annex 7. Preparation of Analytical Quantification Algorithm The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 Regression Slope:-6.98592026 Pass Line Position Difference:Resolution Difference to Reference 4.14% D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures CTS Bottle Concentration: CTS Sample Concentration Average: Difference between measured and expected: Tolerance: 100.00 99.42 0.58% 5.00% POST CTS System Check: Run 1 Points 1 & 2 on CO/NO/Propane Run 2 Points 1 & 2 on CO/NO/Propane Run 3 Points 1 & 2 on CO/NO/Propane Run Data Validation - Automated vs Manual Reading Validated Comments All within 20% All within 20% All within 20% Passed Passed Passed Demonstrates no interferences observed. Demonstrates no interferences observed. Demonstrates no interferences observed. 17 GAS 12.0 Signature Page Job/File Name: We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Crusoe Energy Systems, Inc.; Residue Booster Station; 2026-07; JJJJ 18 Company: Print Name: Signature: Title: Phone Number: Date: Company:G.A.S. Inc.Date: Print Name: Title: 4/22/2025 Emissions Specialist Company:G.A.S. Inc.Date: Print Name: Title: Signature: Phone Number: Travis Hartley Director of Stack Testing 580-225-0403 4/22/2025 Cooper Green GAS Appendices GAS GAS Spike (5 Gas) GAS 9% O2/NO2 GAS Ethylene Only GAS BIP GAS 21% O2 Tri Probe Certification ” ‡ ƒ – Ž ƒ ‹ • • • ƒ Ž › – ‹ … ƒ Ž ‡ ” ˜ ‹ … ‡ • ͵Ͳ͵͵”†–Ž‹–›ǡǡ͹͵͸ͶͶ ȋͷͺͲȌʹʹͷǦͲͶͲ͵ ƒšǣȋͷͺͲȌʹʹͷǦʹ͸ͳʹ &(57,),&$7(2)$1$/<6,6 *UDGHRI3URGXFW&(57,),('67$1'$5'352%( 3DUW1XPEHU65HIHUHQFH 1XPEHU  /DERUDWRU\*$6,1&6WDFN'LDPHWHU $QDO\VLV'DWH7DUJHW)ORZ 5DWH /PLQ /271XPEHU 61 $ $6 1XPEHURI 3RLQWV  3URGXFWSHUIRUPDQFHYHULILHGE\GLUHFWFRPSDULVRQWRFDOLEUDWLRQVWDQGDUGVWUDFHDEOHWR1,67  7KHSUREHOLVWHGRQWKLVIRUPPHHWVWKHPXOWLSRLQWWUDYHUVHUHTXLUHPHQWRI(3$0HWKRGH VHFWLRQDVVKRZQLQWKHDFFRPSDQ\LQJGDWD0HWKRGHVHFWLRQVWDWHVWKDWWKHPXOWLSRLQW WUDYHUVHUHTXLUHPHQWFDQEHVDWLVILHGE\VDPSOLQJYLD³DPXOWLKROHSUREHGHVLJQHGWRVDPSOHDW WKHSUHVFULEHGSRLQWVZLWKDIORZSHUFHQWRIPHDQIORZUDWH´ $1$/<7,&$/5(68/76 ZƵŶηdŽƚĂů&ůŽǁ ;>ͬŵͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϭͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϮͿ DĞĂƐƵƌĞĚ&ůŽǁ WŽƌƚ;>ͬŵͿ ;ĞůƚĂƋϯͿ 0HDQ3UREH 3RUW6DPSOHG )ORZ /P  5XQ/30  䧮    䧮    䧮   5XQ/30  䧮    䧮    䧮    &DOLEUDWLRQFRQGXFWHGLQDFFRUGDQFHZLWK(PLVVLRQ0HDVXUHPHQW&HQWHU*XLGHOLQH'RFXPHQW±(0&*' 1RWHV BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB $SSURYHGIRU5HOHDVH'DWH 2/17/2022 Probe size: 20S Mr. Jordan Williamson CEO GAS Inc. 303 W. 3rd Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. March 15, 2021 Sincerely, Steffan M. Johnson, Group Leader Measurement Technology Group If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. cc: Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leather.james@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Heather Sessing, Oklahoma DEQ, (Heather.sessing@deq.ok.gov) Cooper Green GAS Type of Sources Tested: info@gasinc.us Stationary Internal Combustion Engines • 4 Stroke Rich Burn Engines • 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods: • EPA Method 1 & 1A – Sampling & Traverse Points • EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream • EPA Method 3A – Oxygen • EPA Method 7E – NOX • EPA Method 10 – Carbon Monoxide • EPA Method 25A – Volatile Organic Compounds • ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. • Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Types of Analyzers: • Gasmet DX4000 FTIR • Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory • Testo 350 • Flame Ionization Detector 580-225-0403 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 1 Minute Average Data Sheet Crusoe Energy Systems, Inc.Client: Residue Booster Station Unit Number:2026-07 Make:Waukesha Location:9394 GSIModel: 1662642Serial Number: RAW Result Data Stability 4/22/2025 05:40 0.4310.800-0.002 0.000 0.0001.998 0.000 0.000 0.0000.0480.000 0.795 0.3320.112 0.035 845.00.930.005 0.018 1.23 0.00 180.0 Pre Test Baseline Direct 4/22/2025 05:47 0.0000.000-0.001 0.000 0.0580.000 0.000 0.094 0.1340.0580.212 0.000 0.0430.000 0.012 845.00.130.094 0.000 0.00 0.00 180.0 4/22/2025 05:48 0.0000.0000.003 0.000 0.2240.000 0.000 0.120 0.0670.0000.213 0.000 0.0000.000 0.000 845.00.130.194 0.000 0.00 0.00 180.0 4/22/2025 05:48 0.0000.0000.000 0.000 0.0000.000 0.000 0.098 0.0000.0000.422 0.000 0.0000.000 0.000 845.00.050.074 0.000 0.00 0.00 180.0 CTS Direct 4/22/2025 05:50 0.0000.0000.009 0.001 0.0000.000 0.000 0.000 0.2660.0000.000 98.971 0.0000.000 0.000 845.066.140.239 0.014 0.00 0.00 180.0 4/22/2025 05:50 0.0000.0230.010 0.000 0.0000.000 0.000 0.000 0.7400.0700.000 98.709 0.0000.000 0.000 845.066.040.344 0.013 0.02 0.00 180.0 4/22/2025 05:51 0.0000.0000.010 0.010 0.0000.000 0.000 0.000 0.3380.0920.000 99.027 0.0000.098 0.004 845.066.130.152 0.014 0.00 0.00 180.0 High O2 Direct 4/22/2025 05:56 0.0000.0000.001 0.000 0.0000.000 0.000 0.131 0.0000.0610.795 0.000 0.0000.000 0.013 845.00.080.074 0.000 0.00 20.76 180.0 4/22/2025 05:56 0.0000.000-0.002 0.000 0.0000.000 0.000 0.169 0.0000.0000.445 0.000 0.0000.000 0.008 845.00.090.113 0.000 0.00 20.73 180.0 4/22/2025 05:56 0.0000.000-0.002 0.000 0.0000.000 0.000 0.243 0.0580.0000.392 0.000 0.0000.008 0.021 845.00.070.041 0.000 0.00 20.76 180.0 NO2/Mid O2 Direct 4/22/2025 06:00 101.6300.000-0.003 0.000 0.0000.000 0.934 0.000 0.4750.0000.319 0.000 0.0000.000 0.000 845.00.000.000 0.000 101.63 10.65 180.0 4/22/2025 06:01 102.3000.0000.001 0.000 0.5740.000 0.913 0.000 0.3960.0000.250 0.000 0.0000.000 0.000 845.00.000.000 0.000 102.30 10.62 180.0 4/22/2025 06:01 101.4530.000-0.002 0.000 0.2910.000 0.917 0.000 0.7670.0000.320 0.000 0.0000.000 0.000 845.00.000.000 0.000 101.45 10.61 180.0 Spike Direct 4/22/2025 06:03 0.000251.3890.000 4.950 5.505489.859 1.820 2.193 0.8250.2940.000 0.939 252.3160.197 0.787 845.0256.242.580 9.791 251.39 0.00 180.0 4/22/2025 06:03 0.000250.5260.002 4.949 4.780491.272 1.817 2.154 0.9440.3520.000 0.975 252.6240.418 0.845 845.0256.522.327 9.789 250.53 0.00 180.0 4/22/2025 06:03 0.000251.7680.001 4.946 4.469490.515 1.827 2.248 0.4530.3990.000 0.967 252.5980.168 0.930 845.0256.782.513 9.788 251.77 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline System 4/22/2025 06:06 0.0000.0000.006 0.003 0.0000.000 0.000 0.402 0.0000.0000.000 0.000 0.2730.019 0.052 845.00.700.477 0.000 0.00 0.00 180.0 4/22/2025 06:06 0.0000.0000.010 0.010 0.0000.000 0.000 0.274 0.0000.0000.000 0.000 0.2790.013 0.028 845.00.610.411 0.000 0.00 0.00 180.0 4/22/2025 06:06 0.0000.0000.011 0.002 0.0000.000 0.000 0.255 0.0000.0000.000 0.000 0.0620.000 0.080 845.00.430.318 0.000 0.00 0.00 180.0 CTS System with Response Time 4/22/2025 06:08 0.0000.0000.015 0.020 0.0000.000 0.000 0.022 0.0800.0000.000 97.876 0.0250.000 0.032 845.065.420.109 0.013 0.00 0.00 180.0 4/22/2025 06:08 0.0000.0000.021 0.030 0.0000.000 0.000 0.000 0.0000.0020.000 98.156 0.0000.089 0.068 845.065.660.128 0.012 0.00 0.00 180.0 4/22/2025 06:08 0.0000.0000.016 0.027 0.0000.000 0.000 0.002 0.0310.0000.000 97.858 0.0000.000 0.065 845.065.420.066 0.013 0.00 0.00 179.0 NO2/Mid O2 System with Response Time 4/22/2025 06:11 99.5711.9080.006 0.004 0.1360.000 0.985 0.220 0.2630.0000.000 0.000 0.0590.193 0.010 845.00.080.000 0.000 101.48 10.60 180.0 4/22/2025 06:11 99.7572.2330.002 0.005 0.4740.000 0.930 0.234 0.1560.0000.000 0.000 0.0760.426 0.008 845.00.090.000 0.000 101.99 10.63 180.0 4/22/2025 06:11 100.4951.6320.008 0.000 0.0000.000 0.967 0.161 0.0000.0000.000 0.000 0.0460.077 0.018 845.00.090.014 0.000 102.13 10.61 180.0 Spike System with Response Time 4/22/2025 06:14 0.000247.2560.003 4.917 4.443484.643 1.867 2.295 0.0000.2020.255 1.034 251.6480.315 0.804 845.0255.322.065 9.727 247.26 0.00 180.0 4/22/2025 06:14 0.000247.5520.007 4.876 1.740487.799 1.869 2.264 0.1150.0560.000 1.064 251.6270.080 0.850 845.0255.402.039 9.727 247.55 0.00 180.0 4/22/2025 06:14 0.000247.0160.002 4.930 4.260485.351 1.923 2.331 0.0410.1410.000 1.060 251.3470.000 0.951 845.0255.362.109 9.725 247.02 0.00 180.0 Baseline System with Response Time 4/22/2025 06:17 0.0000.0000.007 0.015 0.0000.000 0.000 0.189 0.0000.0000.000 0.000 0.2790.000 0.051 845.00.620.354 0.000 0.00 0.00 180.0 4/22/2025 06:17 0.0000.0000.003 0.008 0.0450.000 0.000 0.287 0.0000.0070.000 0.000 0.3490.145 0.002 845.00.630.410 0.000 0.00 0.00 180.0 4/22/2025 06:18 0.0000.0000.007 0.008 0.0000.000 0.000 0.246 0.0000.0270.049 0.000 0.2240.000 0.003 845.00.490.384 0.000 0.00 0.00 180.0 Run 1 - A 30minute/60min 4/22/2025 07:35 0.0004.82517.350 10.384 48.4442.432 2.186 2.275 0.8350.0563.756 0.000 0.0000.667 0.134 833.00.790.780 0.000 4.83 0.00 180.0 4/22/2025 07:36 0.0005.51017.415 10.363 56.5760.306 2.715 2.167 1.1550.0553.552 0.000 0.0000.742 0.112 833.00.810.887 0.000 5.51 0.00 180.0 4/22/2025 07:37 0.0006.01817.390 10.368 57.3630.000 2.951 2.109 1.4010.0723.573 0.000 0.0000.794 0.081 833.00.871.071 0.000 6.02 0.00 180.0 4/22/2025 07:38 0.42911.38317.421 10.365 27.8430.000 2.382 1.774 0.5980.0522.844 0.000 0.0000.743 0.045 833.00.600.766 0.000 11.81 0.00 180.0 4/22/2025 07:39 0.7706.07917.426 10.379 34.8652.565 1.079 1.669 0.5510.0313.214 0.000 0.0000.635 0.084 833.00.640.711 0.000 6.85 0.00 180.0 4/22/2025 07:40 0.0009.81417.451 10.371 36.4301.292 2.476 2.164 0.5560.0053.050 0.000 0.0000.555 0.044 833.00.590.755 0.000 9.81 0.00 180.0 4/22/2025 07:41 0.26610.82617.429 10.392 27.4390.000 2.076 1.684 0.5260.0474.468 0.000 0.0000.733 0.075 833.00.730.872 0.000 11.09 0.00 179.0 4/22/2025 07:42 0.0008.06317.461 10.489 36.9900.000 2.038 1.544 0.4730.0394.075 0.000 0.0000.889 0.061 833.00.550.639 0.000 8.06 0.02 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/22/2025 07:43 0.3507.05217.496 10.450 42.6800.000 2.209 1.419 0.8660.0674.517 0.000 0.0000.715 0.108 833.00.760.812 0.000 7.40 0.00 180.0 4/22/2025 07:44 0.0008.05417.428 10.388 46.5460.000 2.058 1.369 0.9030.0154.487 0.000 0.0000.674 0.055 833.00.730.929 0.000 8.05 0.00 180.0 4/22/2025 07:45 0.0118.19217.367 10.411 38.1580.000 2.124 1.252 0.7970.0084.272 0.000 0.0000.591 0.062 833.00.650.793 0.000 8.20 0.00 180.0 4/22/2025 07:46 0.0006.17717.375 10.382 48.8480.000 2.339 1.157 0.8980.0054.540 0.000 0.0000.595 0.060 833.00.630.761 0.000 6.18 0.00 180.0 4/22/2025 07:47 0.00011.24117.352 10.357 41.9010.000 2.527 0.971 0.7210.0033.132 0.000 0.0000.633 0.052 833.00.640.801 0.000 11.24 0.00 180.0 4/22/2025 07:49 0.0005.52517.360 10.374 50.8000.000 2.069 1.036 1.2880.0154.715 0.000 0.0000.704 0.061 833.00.821.046 0.000 5.52 0.00 180.0 4/22/2025 07:50 0.3614.79817.388 10.393 54.3530.000 2.599 0.958 1.5090.0364.540 0.000 0.0000.771 0.072 833.00.710.845 0.000 5.16 0.00 180.0 4/22/2025 07:51 0.00012.11117.387 10.416 29.5610.000 2.505 0.865 0.8060.0043.886 0.000 0.0000.814 0.000 833.00.440.667 0.000 12.11 0.00 180.0 4/22/2025 07:52 0.53721.60417.410 10.451 16.6640.000 2.812 0.864 0.5880.0413.227 0.000 0.0000.658 0.036 833.00.510.659 0.000 22.14 0.00 180.0 4/22/2025 07:53 0.2307.48117.394 10.448 19.1923.473 1.332 0.753 0.6850.0013.592 0.000 0.0000.639 0.047 833.00.660.855 0.000 7.71 0.00 180.0 4/22/2025 07:54 0.0006.02517.343 10.388 32.0137.674 1.536 0.954 0.7580.0133.675 0.000 0.0000.781 0.031 833.00.510.674 0.000 6.03 0.00 180.0 4/22/2025 07:55 0.0006.72617.320 10.317 41.0272.716 2.231 1.100 1.1950.0003.892 0.000 0.0000.766 0.029 833.00.480.635 0.000 6.73 0.00 180.0 4/22/2025 07:56 0.0006.97317.336 10.386 35.8100.626 1.800 1.165 0.7530.0443.630 0.000 0.0000.860 0.067 833.00.690.834 0.000 6.97 0.00 180.0 4/22/2025 07:57 0.3577.36417.336 10.403 39.0120.000 2.126 1.107 0.8900.0053.686 0.000 0.0000.850 0.116 833.00.790.841 0.000 7.72 0.00 180.0 4/22/2025 07:58 0.1926.88917.344 10.320 55.6290.000 2.745 1.022 1.7380.0004.443 0.000 0.0000.817 0.112 833.00.810.877 0.000 7.08 0.00 180.0 4/22/2025 07:59 0.0006.42017.328 10.363 58.0140.000 2.981 1.125 1.8720.0044.429 0.000 0.0000.706 0.072 833.00.740.895 0.000 6.42 0.00 180.0 4/22/2025 08:00 0.2465.84917.349 10.417 45.1290.000 2.098 0.849 1.1620.0323.710 0.000 0.0000.886 0.086 833.00.760.880 0.000 6.10 0.00 180.0 4/22/2025 08:01 0.3088.79017.318 10.351 30.8470.000 1.998 0.833 0.7610.0153.803 0.000 0.0000.853 0.108 833.00.760.824 0.000 9.10 0.00 180.0 4/22/2025 08:02 0.7399.98717.333 10.402 29.9850.000 1.670 0.897 0.6630.0143.066 0.000 0.0000.842 0.076 833.00.630.714 0.000 10.73 0.00 180.0 4/22/2025 08:03 0.3477.57217.353 10.413 39.1610.000 1.659 0.757 1.0290.0083.416 0.000 0.0000.596 0.080 833.00.780.924 0.000 7.92 0.00 180.0 4/22/2025 08:04 0.16310.69817.385 10.390 32.5170.000 2.766 0.843 0.8340.0003.621 0.000 0.0000.780 0.045 833.00.630.808 0.000 10.86 0.00 180.0 4/22/2025 08:05 0.6988.10017.336 10.316 28.6310.000 1.249 0.763 0.6250.0073.862 0.000 0.0000.780 0.073 833.00.670.792 0.000 8.80 0.00 180.0 0.2008.20517.379 10.388 39.4140.703 2.178 1.248 0.9150.0233.822 0.000 0.0000.736 0.069 833.000.6790.812 0.000 8.405 0.001 180.0Avg. Spike 1 4/22/2025 08:07 2.25725.98614.394 9.137 34.34950.778 2.514 1.088 1.4840.0112.553 0.669 23.5590.561 0.212 833.025.121.032 0.930 28.24 0.00 180.0 Run 1 - B 30minute/60min 4/22/2025 08:09 0.00015.38717.380 10.356 25.4150.000 2.734 0.915 0.9970.0003.325 0.000 0.0000.523 0.014 833.00.600.865 0.000 15.39 0.00 180.0 4/22/2025 08:10 0.43111.47917.414 10.410 21.1250.000 1.767 0.796 0.4320.0062.989 0.000 0.0000.586 0.081 833.00.670.768 0.000 11.91 0.00 180.0 4/22/2025 08:11 0.3976.97017.473 10.322 35.9373.619 1.590 0.918 0.6270.0113.961 0.000 0.0000.779 0.072 833.00.630.723 0.000 7.37 0.00 180.0 4/22/2025 08:12 0.0008.67017.500 10.323 39.6730.319 2.325 1.054 0.8760.0004.025 0.000 0.0000.688 0.021 833.00.480.651 0.000 8.67 0.00 180.0 4/22/2025 08:13 0.8679.99017.503 10.411 30.1910.332 1.815 0.892 0.7790.0043.543 0.000 0.0000.727 0.017 833.00.560.784 0.000 10.86 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/22/2025 08:14 0.0009.14617.510 10.420 35.6190.000 2.105 0.903 0.6150.0003.365 0.000 0.0000.778 0.078 833.00.730.866 0.000 9.15 0.02 180.0 4/22/2025 08:15 0.0008.32417.572 10.388 40.1000.000 2.330 0.888 0.9170.0003.833 0.000 0.0000.688 0.041 833.00.690.907 0.000 8.32 0.00 180.0 4/22/2025 08:16 0.0007.46217.600 10.345 48.9200.000 1.753 0.821 0.9170.0004.222 0.000 0.0000.662 0.045 833.00.600.764 0.000 7.46 0.00 180.0 4/22/2025 08:17 0.37311.52417.416 10.354 52.8850.000 3.700 0.726 1.0870.0112.525 0.000 0.0000.782 0.102 833.00.790.884 0.000 11.90 0.00 180.0 4/22/2025 08:18 0.00010.35517.420 10.368 41.9890.718 2.355 0.608 1.2100.0022.519 0.000 0.0000.850 0.000 833.00.520.787 0.000 10.35 0.00 180.0 4/22/2025 08:19 0.0008.33417.432 10.342 67.5053.925 3.756 1.089 1.7030.0002.988 0.000 0.0000.760 0.105 833.00.780.850 0.000 8.33 0.00 180.0 4/22/2025 08:20 0.0618.30017.425 10.362 44.8370.000 2.809 1.164 0.9460.0003.976 0.000 0.0000.799 0.084 833.00.750.871 0.000 8.36 0.00 180.0 4/22/2025 08:21 0.0564.94417.417 10.370 53.2672.399 2.004 1.093 1.0430.0003.494 0.000 0.0000.841 0.133 833.00.850.875 0.000 5.00 0.00 180.0 4/22/2025 08:22 0.6919.24117.403 10.355 59.2570.839 3.383 1.033 1.6990.0012.692 0.000 0.0000.887 0.059 833.00.650.799 0.000 9.93 0.00 180.0 4/22/2025 08:23 0.00010.58917.418 10.322 48.5100.000 2.957 0.859 0.9120.0002.495 0.000 0.0000.670 0.049 833.00.610.765 0.000 10.59 0.00 180.0 4/22/2025 08:24 0.0004.88817.398 10.346 57.2930.000 2.243 0.836 1.1250.0004.467 0.000 0.0000.830 0.079 833.00.730.860 0.000 4.89 0.00 180.0 4/22/2025 08:25 0.0007.04217.422 10.365 42.6260.000 2.045 0.758 0.4440.0003.900 0.000 0.0000.642 0.122 833.00.800.831 0.000 7.04 0.00 180.0 4/22/2025 08:26 0.0009.32417.430 10.360 38.9020.000 1.842 0.717 0.4020.0003.825 0.000 0.0000.824 0.120 833.00.660.627 0.000 9.32 0.00 180.0 4/22/2025 08:27 0.0566.77917.411 10.377 43.6183.380 1.351 0.752 0.6200.0003.709 0.000 0.0000.724 0.089 833.00.690.766 0.000 6.84 0.00 180.0 4/22/2025 08:28 0.0009.48317.391 10.346 51.1561.636 3.249 0.965 0.9940.0002.701 0.000 0.0000.700 0.121 833.00.790.821 0.000 9.48 0.00 180.0 4/22/2025 08:30 0.03511.69317.394 10.359 48.0710.000 2.995 0.798 0.8510.0132.329 0.000 0.0000.691 0.122 833.00.750.757 0.000 11.73 0.00 180.0 4/22/2025 08:31 0.0006.53617.380 10.364 45.6540.000 2.036 0.810 0.7190.0003.964 0.000 0.0000.695 0.088 833.00.650.707 0.000 6.54 0.00 180.0 4/22/2025 08:32 0.0008.00217.412 10.338 39.3180.000 1.465 0.713 0.5670.0003.777 0.000 0.0000.718 0.054 833.00.680.856 0.000 8.00 0.00 180.0 4/22/2025 08:33 0.0006.33817.328 10.314 49.1400.000 2.149 0.672 0.8990.0044.655 0.000 0.0000.661 0.083 833.00.730.853 0.000 6.34 0.00 179.0 4/22/2025 08:34 0.5527.01017.361 10.364 47.1040.000 2.148 0.735 0.7690.0023.593 0.000 0.0000.786 0.127 833.00.760.761 0.000 7.56 0.00 180.0 4/22/2025 08:35 0.0009.75117.369 10.361 36.3800.000 2.402 0.724 0.4080.0033.293 0.000 0.0000.487 0.076 833.00.700.816 0.000 9.75 0.00 180.0 4/22/2025 08:36 0.0279.06517.374 10.361 40.8474.243 2.010 0.616 0.6530.0002.554 0.000 0.0000.691 0.060 833.00.700.863 0.000 9.09 0.00 180.0 4/22/2025 08:37 0.43710.98017.401 10.357 38.4242.139 2.696 0.975 0.4850.0002.213 0.000 0.0000.642 0.101 833.00.670.696 0.000 11.42 0.00 180.0 4/22/2025 08:38 0.0167.50717.398 10.383 47.5010.415 2.689 1.025 0.8370.0323.474 0.000 0.0000.623 0.132 833.00.770.759 0.000 7.52 0.00 180.0 4/22/2025 08:39 0.47913.03817.400 10.350 39.7590.000 2.728 0.794 0.5060.0002.415 0.000 0.0000.691 0.088 833.00.650.708 0.000 13.52 0.00 180.0 0.1498.93817.425 10.360 43.7010.799 2.381 0.855 0.8350.0033.361 0.000 0.0000.714 0.079 833.000.6880.795 0.000 9.088 0.001 180.0Avg. 0.1758.57217.402 10.374 41.5580.751 2.279 1.052 0.8750.0133.592 0.000 0.0000.725 0.074 833.000.6840.803 0.000 8.746 0.001 180.0Run 1 Avg: Baseline 1 4/22/2025 08:41 0.0000.0000.044 0.029 0.0000.000 0.000 0.173 0.0000.0020.317 0.000 0.1090.000 0.075 833.00.610.528 0.000 0.00 0.00 180.0 Run 2 - A 30minute/60min 4/22/2025 08:43 0.45811.58317.156 10.237 41.7190.000 2.245 0.717 0.5260.0022.039 0.000 0.0000.740 0.108 833.00.600.579 0.000 12.04 0.00 180.0 4/22/2025 08:44 0.32911.32517.359 10.303 43.7040.000 2.587 0.608 0.7790.0002.686 0.000 0.0000.784 0.120 833.00.840.906 0.000 11.65 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/22/2025 08:45 0.00012.26917.408 10.328 43.1960.329 2.885 0.602 0.5920.0003.034 0.000 0.0000.652 0.073 833.00.750.911 0.000 12.27 0.00 180.0 4/22/2025 08:46 0.0007.78917.403 10.365 45.0960.000 1.723 0.742 0.7430.0003.488 0.000 0.0000.704 0.066 833.00.740.920 0.000 7.79 0.00 180.0 4/22/2025 08:47 0.51711.13617.469 10.357 55.4720.257 3.272 0.666 1.2330.0043.249 0.000 0.0000.856 0.113 833.00.850.935 0.000 11.65 0.00 180.0 4/22/2025 08:48 0.05012.38417.466 10.339 31.4170.000 2.041 0.659 0.1040.0002.751 0.000 0.0000.477 0.142 833.00.880.894 0.000 12.43 0.00 180.0 4/22/2025 08:49 0.0006.97717.475 10.371 45.2560.360 2.035 0.821 0.6210.0003.671 0.000 0.0000.647 0.087 833.00.780.907 0.000 6.98 0.00 180.0 4/22/2025 08:50 0.0008.81917.455 10.356 39.9560.000 1.963 0.739 0.5190.0003.423 0.000 0.0000.564 0.075 833.00.710.836 0.000 8.82 0.00 179.0 4/22/2025 08:51 0.5088.71017.516 10.426 36.5980.280 1.506 0.629 0.5040.0013.898 0.000 0.0000.879 0.077 833.00.630.707 0.000 9.22 0.00 180.0 4/22/2025 08:52 0.19510.34717.425 10.382 49.6971.462 3.310 0.671 0.8700.0002.340 0.000 0.0000.568 0.110 833.00.840.924 0.000 10.54 0.00 180.0 4/22/2025 08:53 0.00010.72017.435 10.309 46.9790.000 2.484 0.635 0.6930.0003.088 0.000 0.0000.404 0.095 833.00.820.941 0.000 10.72 0.03 180.0 4/22/2025 08:54 0.0008.70817.436 10.310 59.0390.453 3.161 0.613 1.4090.0023.210 0.000 0.0000.711 0.105 833.00.830.931 0.000 8.71 0.03 180.0 4/22/2025 08:55 0.7135.26017.434 10.355 58.2410.000 2.253 0.712 1.1250.0083.725 0.000 0.0000.466 0.154 833.00.940.955 0.000 5.97 0.00 180.0 4/22/2025 08:56 0.0006.30117.427 10.346 47.9060.000 2.234 0.753 0.9380.0004.019 0.000 0.0000.504 0.091 833.00.851.001 0.000 6.30 0.00 180.0 4/22/2025 08:57 0.03211.01217.407 10.300 43.3330.000 2.098 0.528 0.8320.0003.005 0.000 0.0000.680 0.097 833.00.770.867 0.000 11.04 0.00 179.0 4/22/2025 08:58 0.00014.16917.383 10.308 52.9730.357 3.377 0.486 1.0940.0003.114 0.000 0.0000.767 0.100 833.00.750.827 0.000 14.17 0.00 179.0 4/22/2025 08:59 0.45234.02117.424 10.289 17.1820.000 5.002 0.582 0.0590.0002.153 0.000 0.0000.636 0.079 833.00.430.408 0.000 34.47 0.00 180.0 4/22/2025 09:00 0.53013.17617.453 10.309 14.2661.116 1.953 0.402 0.0270.0001.851 0.000 0.0000.775 0.102 833.00.710.765 0.000 13.71 0.00 180.0 4/22/2025 09:01 0.4738.82317.443 10.335 28.00515.378 2.147 0.662 0.4500.0141.900 0.000 0.0000.701 0.087 833.00.660.723 0.000 9.30 0.00 180.0 4/22/2025 09:02 0.00012.12717.376 10.358 40.55211.939 3.772 1.318 0.8320.0001.942 0.000 0.0000.535 0.091 833.00.790.907 0.000 12.13 0.00 180.0 4/22/2025 09:03 0.37510.67017.384 10.354 40.6352.054 3.036 1.072 0.7760.0181.934 0.000 0.0000.694 0.122 833.00.790.816 0.000 11.05 0.00 180.0 4/22/2025 09:04 0.39410.17317.416 10.324 42.7670.523 2.619 0.863 0.6480.0002.107 0.000 0.0000.601 0.114 833.00.770.813 0.000 10.57 0.00 180.0 4/22/2025 09:05 0.33413.32017.441 10.352 34.6200.000 2.616 0.765 0.6200.0002.146 0.000 0.0000.675 0.086 833.00.780.906 0.000 13.65 0.00 180.0 4/22/2025 09:06 0.3098.79917.474 10.369 31.9370.000 1.257 0.723 0.7700.0043.238 0.000 0.0000.859 0.026 833.00.490.663 0.000 9.11 0.00 180.0 4/22/2025 09:07 0.00020.71317.466 10.349 45.8941.986 3.889 0.859 1.0940.0012.547 0.000 0.0000.814 0.032 833.00.500.648 0.000 20.71 0.00 180.0 4/22/2025 09:08 0.29512.11717.418 10.319 16.4580.768 1.936 0.696 0.0870.0261.640 0.000 0.0000.585 0.125 833.00.760.762 0.000 12.41 0.00 179.0 4/22/2025 09:09 0.2667.98517.405 10.363 37.71015.271 2.238 1.087 0.6830.0002.044 0.000 0.0000.770 0.084 833.00.710.819 0.000 8.25 0.00 180.0 4/22/2025 09:11 0.25611.42317.397 10.368 49.0658.734 3.730 2.139 1.1040.0022.222 0.000 0.0000.505 0.107 833.00.810.894 0.000 11.68 0.00 180.0 4/22/2025 09:12 0.0009.75817.382 10.343 49.3272.386 3.293 1.658 1.1030.0002.500 0.000 0.0000.634 0.152 833.00.900.894 0.000 9.76 0.00 180.0 4/22/2025 09:13 0.0008.11617.380 10.356 56.5783.950 3.281 1.861 1.3960.0002.936 0.000 0.0000.693 0.149 833.00.900.911 0.000 8.12 0.00 180.0 0.21611.29117.417 10.339 41.5192.253 2.665 0.842 0.7410.0032.730 0.000 0.0000.663 0.099 833.000.7530.832 0.000 11.507 0.002 179.9Avg. Spike 2 4/22/2025 09:15 0.54326.26915.837 9.859 49.70547.662 2.879 1.330 1.3960.0002.567 0.568 21.7650.716 0.259 833.023.471.207 0.854 26.81 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Run 2 - B 30minute/60min 4/22/2025 09:17 0.1556.74417.403 10.335 49.1940.000 2.282 0.923 1.2970.0004.208 0.000 0.0000.669 0.154 833.00.870.837 0.000 6.90 0.00 180.0 4/22/2025 09:18 0.7867.71817.393 10.367 39.5680.000 1.374 0.834 0.8570.0013.519 0.000 0.0000.653 0.087 833.00.740.849 0.000 8.50 0.00 180.0 4/22/2025 09:19 0.0008.05217.389 10.386 44.7380.000 1.985 0.848 1.0330.0123.647 0.000 0.0000.691 0.063 833.00.690.850 0.000 8.05 0.00 180.0 4/22/2025 09:20 0.7786.49417.431 10.388 42.8930.000 2.017 0.967 1.0450.0193.857 0.000 0.0000.529 0.093 833.00.790.906 0.000 7.27 0.00 180.0 4/22/2025 09:21 0.1524.26217.401 10.340 60.2300.991 2.308 0.990 1.6280.0004.300 0.000 0.0000.776 0.134 833.00.870.901 0.000 4.41 0.00 180.0 4/22/2025 09:22 0.1187.18817.393 10.365 52.9710.363 3.007 1.372 1.4800.0003.764 0.000 0.0000.829 0.126 833.00.810.836 0.000 7.31 0.00 180.0 4/22/2025 09:23 0.0708.26717.383 10.381 37.3890.000 2.564 1.118 0.8530.0003.840 0.000 0.0000.709 0.159 833.00.830.771 0.000 8.34 0.00 180.0 4/22/2025 09:24 0.2176.87617.376 10.345 42.6584.560 1.765 0.913 1.0290.0012.368 0.000 0.0000.721 0.105 833.00.790.862 0.000 7.09 0.00 180.0 4/22/2025 09:25 0.0008.53717.379 10.362 46.9822.002 2.643 1.388 1.1580.0012.333 0.000 0.0000.636 0.113 833.00.840.916 0.000 8.54 0.00 180.0 4/22/2025 09:26 0.4327.25117.381 10.364 45.7880.425 2.551 1.320 1.1630.0013.530 0.000 0.0000.761 0.123 833.00.730.727 0.000 7.68 0.00 180.0 4/22/2025 09:27 0.9808.14017.407 10.368 35.0190.000 1.632 0.967 0.7320.0073.582 0.000 0.0000.634 0.094 833.00.650.696 0.000 9.12 0.00 180.0 4/22/2025 09:28 0.0004.73517.385 10.333 65.3242.975 1.894 1.109 1.9790.0004.226 0.000 0.0000.868 0.128 833.00.830.855 0.000 4.73 0.00 179.0 4/22/2025 09:29 0.1533.99617.416 10.404 58.1631.145 2.827 1.723 1.6820.0004.037 0.000 0.0000.968 0.148 833.00.830.798 0.000 4.15 0.00 180.0 4/22/2025 09:30 0.4015.90417.347 10.359 52.1900.000 2.584 1.458 1.4220.0003.995 0.000 0.0000.741 0.110 833.00.880.991 0.000 6.30 0.00 180.0 4/22/2025 09:31 0.7736.89817.382 10.349 41.3950.000 1.510 1.018 1.0170.0003.592 0.000 0.0000.736 0.119 833.00.720.721 0.000 7.67 0.00 180.0 4/22/2025 09:32 0.8507.87817.356 10.349 39.8990.000 1.641 0.889 1.0000.0113.727 0.000 0.0000.608 0.103 833.00.790.869 0.000 8.73 0.00 180.0 4/22/2025 09:33 0.2585.55617.360 10.313 44.6293.911 1.377 0.896 1.2250.0003.528 0.000 0.0000.864 0.101 833.00.690.735 0.000 5.81 0.00 180.0 4/22/2025 09:34 0.1644.29317.358 10.382 46.4690.902 2.209 1.403 1.2050.0003.502 0.000 0.0000.802 0.105 833.00.670.688 0.000 4.46 0.00 180.0 4/22/2025 09:35 0.6059.26017.341 10.401 35.2540.000 1.907 0.939 0.9490.0013.314 0.000 0.0000.692 0.127 833.00.870.920 0.000 9.86 0.00 180.0 4/22/2025 09:36 0.1158.19817.310 10.356 31.7230.200 0.952 0.863 0.8280.0043.478 0.000 0.0000.676 0.118 833.00.770.799 0.000 8.31 0.00 180.0 4/22/2025 09:37 0.6155.20417.318 10.354 47.7351.309 2.131 1.032 1.2710.0003.521 0.000 0.0000.621 0.130 833.00.800.812 0.000 5.82 0.00 180.0 4/22/2025 09:38 0.3477.81217.343 10.378 37.6520.089 1.432 1.006 0.9530.0003.499 0.000 0.0000.807 0.134 833.00.750.717 0.000 8.16 0.00 180.0 4/22/2025 09:39 0.6138.51417.311 10.317 31.5210.000 1.525 0.893 0.9380.0003.362 0.000 0.0000.582 0.127 833.00.820.856 0.000 9.13 0.00 179.0 4/22/2025 09:40 0.3878.33517.357 10.427 44.3020.438 1.652 0.763 1.1320.0003.133 0.000 0.0000.654 0.170 833.00.870.802 0.000 8.72 0.00 180.0 4/22/2025 09:41 0.8546.94617.390 10.436 48.0540.000 1.760 0.772 1.3180.0083.200 0.000 0.0000.568 0.152 833.00.800.749 0.000 7.80 0.00 180.0 4/22/2025 09:42 0.7586.38617.328 10.311 48.6850.000 2.507 0.793 1.5570.0004.002 0.000 0.0000.722 0.147 833.00.840.819 0.000 7.14 0.00 180.0 4/22/2025 09:43 0.6037.57017.341 10.319 36.5970.000 1.021 0.678 0.8580.0004.179 0.000 0.0000.618 0.146 833.00.760.704 0.000 8.17 0.00 180.0 4/22/2025 09:44 0.3234.40217.331 10.399 52.3252.060 2.174 0.921 1.8070.0153.521 0.000 0.0000.909 0.116 833.00.820.877 0.000 4.72 0.00 180.0 4/22/2025 09:45 0.3378.63517.347 10.376 30.0400.000 1.440 0.866 0.9310.0093.380 0.000 0.0000.591 0.160 833.00.900.873 0.000 8.97 0.00 180.0 4/22/2025 09:46 0.5093.86717.343 10.308 50.5313.180 1.441 0.851 1.4630.0093.590 0.000 0.0000.671 0.155 833.00.930.924 0.000 4.38 0.00 179.0 0.4126.79717.367 10.362 44.6640.818 1.937 1.017 1.1940.0033.591 0.000 0.0000.710 0.125 833.000.7980.822 0.000 7.208 0.000 179.9Avg. 0.3149.04417.392 10.351 43.0921.536 2.301 0.930 0.9670.0033.161 0.000 0.0000.686 0.112 833.000.7760.827 0.000 9.358 0.001 179.9Run 2 Avg: GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) Baseline 2 4/22/2025 09:48 0.0000.0000.044 0.038 0.0000.000 0.000 0.232 0.0000.0000.221 0.000 0.1170.007 0.079 833.00.750.713 0.000 0.00 0.00 180.0 Run 3 - A 30minute/60min 4/22/2025 10:02 0.2228.89017.357 10.315 45.3194.920 3.625 2.350 1.3910.0002.573 0.000 0.0000.625 0.126 833.00.820.844 0.000 9.11 0.00 179.0 4/22/2025 10:03 0.8946.77217.321 10.378 49.1543.746 3.452 2.358 1.8350.0003.660 0.000 0.0000.595 0.081 833.00.790.936 0.000 7.67 0.00 180.0 4/22/2025 10:04 0.4154.63017.343 10.376 47.1150.869 2.547 1.888 1.2820.0163.485 0.000 0.0000.638 0.170 833.00.860.787 0.000 5.05 0.00 180.0 4/22/2025 10:05 0.50212.74317.344 10.355 42.1280.231 3.323 1.347 1.1670.0002.279 0.000 0.0000.758 0.137 833.00.830.832 0.000 13.25 0.00 180.0 4/22/2025 10:06 0.4228.60017.341 10.331 40.3740.000 1.890 1.082 1.1470.0023.708 0.000 0.0000.616 0.109 833.00.800.867 0.000 9.02 0.00 179.0 4/22/2025 10:07 0.9458.56217.353 10.483 39.2580.000 1.876 1.001 0.9690.0332.564 0.000 0.0000.562 0.104 833.00.770.842 0.000 9.51 0.00 180.0 4/22/2025 10:08 0.6409.48017.389 10.443 28.7270.000 1.674 0.884 0.8250.0132.611 0.000 0.0000.698 0.105 833.00.760.826 0.000 10.12 0.00 181.0 4/22/2025 10:09 0.62612.07517.373 10.324 36.5430.000 2.292 0.674 1.0740.0002.605 0.000 0.0000.581 0.065 833.00.720.883 0.000 12.70 0.00 180.0 4/22/2025 10:10 0.0009.82217.349 10.331 41.8901.664 1.988 0.776 1.1930.0002.026 0.000 0.0000.619 0.069 833.00.670.793 0.000 9.82 0.00 179.0 4/22/2025 10:11 0.2965.29617.367 10.398 47.0880.728 1.968 1.077 1.1440.0043.301 0.000 0.0000.623 0.117 833.00.730.741 0.000 5.59 0.00 180.0 4/22/2025 10:12 0.0005.00617.362 10.376 62.2151.794 2.969 1.442 2.0900.0003.984 0.000 0.0000.707 0.093 833.00.830.959 0.000 5.01 0.00 180.0 4/22/2025 10:13 0.0006.02517.345 10.279 51.1040.000 2.191 1.273 1.4240.0004.313 0.000 0.0000.728 0.060 833.00.700.868 0.000 6.03 0.00 179.0 4/22/2025 10:14 0.4897.36617.347 10.367 40.7940.203 1.227 0.799 0.9430.0003.464 0.000 0.0000.779 0.076 833.00.670.784 0.000 7.85 0.00 179.0 4/22/2025 10:15 0.3004.33917.391 10.440 53.9931.132 2.155 1.124 1.5180.0203.493 0.000 0.0000.598 0.107 833.00.770.834 0.000 4.64 0.00 180.0 4/22/2025 10:16 0.6397.63617.380 10.363 42.5730.000 1.941 0.811 1.1680.0293.473 0.000 0.0000.682 0.089 833.00.710.791 0.000 8.28 0.00 180.0 4/22/2025 10:17 1.0798.11517.333 10.307 34.9450.000 1.312 0.800 0.8790.0033.793 0.000 0.0000.403 0.069 833.00.750.911 0.000 9.19 0.00 179.0 4/22/2025 10:18 0.13217.20217.378 10.378 23.7890.000 2.749 0.728 0.3760.0002.863 0.000 0.0000.737 0.028 833.00.400.517 0.000 17.33 0.00 180.0 4/22/2025 10:19 0.0005.91117.382 10.391 22.8027.951 0.790 0.723 0.4300.0002.894 0.000 0.0000.673 0.052 833.00.560.687 0.000 5.91 0.00 180.0 4/22/2025 10:20 0.0007.20617.402 10.319 34.0517.894 1.398 1.197 0.7710.0003.560 0.000 0.0000.624 0.046 833.00.670.865 0.000 7.21 0.00 180.0 4/22/2025 10:21 0.00014.13217.442 10.386 23.0910.000 2.026 1.065 0.6850.0053.068 0.000 0.0000.818 0.019 833.00.430.588 0.000 14.13 0.00 180.0 4/22/2025 10:22 0.4977.59317.339 10.379 26.4861.683 1.011 0.840 0.7680.0033.099 0.000 0.0000.533 0.018 833.00.520.720 0.000 8.09 0.00 180.0 4/22/2025 10:23 0.5968.68917.403 10.349 37.6533.535 2.008 1.242 0.7940.0023.417 0.000 0.0000.652 0.090 833.00.650.713 0.000 9.28 0.00 180.0 4/22/2025 10:24 0.3238.13517.409 10.361 32.8743.697 1.581 1.022 0.9460.0002.078 0.000 0.0000.532 0.060 833.00.660.811 0.000 8.46 0.00 180.0 4/22/2025 10:26 0.5588.66717.407 10.384 40.2590.000 2.720 1.456 0.9250.0013.411 0.000 0.0000.383 0.081 833.00.720.844 0.000 9.22 0.00 180.0 4/22/2025 10:27 0.33824.25317.424 10.390 24.9920.000 3.757 1.053 0.6920.0022.733 0.000 0.0000.620 0.028 833.00.490.642 0.000 24.59 0.00 180.0 4/22/2025 10:28 0.25010.29317.407 10.370 17.2913.307 1.502 0.701 0.6110.0001.552 0.000 0.0000.652 0.045 833.00.610.779 0.000 10.54 0.00 180.0 4/22/2025 10:29 0.0269.24517.389 10.364 37.48616.443 2.483 1.324 0.9350.0051.445 0.000 0.0000.562 0.060 833.00.550.649 0.000 9.27 0.00 180.0 4/22/2025 10:30 0.2727.73417.388 10.366 38.0942.962 2.016 1.423 0.7400.0003.178 0.000 0.0000.695 0.067 833.00.700.845 0.000 8.01 0.00 180.0 4/22/2025 10:31 0.5406.74317.408 10.344 41.7953.617 1.511 1.436 0.7920.0003.831 0.000 0.0000.686 0.093 833.00.680.744 0.000 7.28 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/22/2025 10:32 0.8939.97017.406 10.357 38.8260.566 2.271 1.285 0.6550.0002.362 0.000 0.0000.333 0.044 833.00.650.838 0.000 10.86 0.00 180.0 0.3969.03817.376 10.367 38.0902.231 2.142 1.173 1.0060.0053.027 0.000 0.0000.624 0.077 833.000.6820.791 0.000 9.434 0.000 179.8Avg. Spike 3 4/22/2025 10:35 0.59926.89015.866 9.849 40.06046.870 2.179 0.972 0.8400.0012.351 0.596 21.2940.466 0.266 833.023.021.191 0.839 27.49 0.00 180.0 Run 3 - B 30minute/60min 4/22/2025 10:37 0.03610.27717.390 10.368 42.7600.777 2.945 0.708 1.1790.0002.160 0.000 0.0000.791 0.096 832.00.740.816 0.000 10.31 0.00 180.0 4/22/2025 10:38 0.6629.82617.359 10.332 46.1274.420 2.979 1.274 1.1480.0002.128 0.000 0.0000.561 0.085 833.00.690.778 0.000 10.49 0.00 179.0 4/22/2025 10:39 0.00610.87617.392 10.365 31.8450.000 1.855 1.078 0.5210.0123.556 0.000 0.0000.524 0.052 833.00.680.863 0.000 10.88 0.00 180.0 4/22/2025 10:40 0.8216.23417.433 10.346 32.3312.599 0.952 0.899 0.5190.0053.619 0.000 0.0000.625 0.035 832.00.430.540 0.000 7.06 0.00 180.0 4/22/2025 10:41 0.0006.37117.393 10.362 45.3391.843 1.668 1.079 0.7950.0003.474 0.000 0.0000.534 0.049 832.00.710.912 0.000 6.37 0.00 180.0 4/22/2025 10:42 0.2544.99817.423 10.381 53.2382.767 2.630 1.709 1.2960.0193.910 0.000 0.0000.692 0.095 832.00.690.754 0.000 5.25 0.00 180.0 4/22/2025 10:43 0.0005.12317.384 10.349 68.9116.947 4.067 3.213 2.4970.0004.130 0.000 0.0000.747 0.087 833.00.660.735 0.000 5.12 0.00 180.0 4/22/2025 10:44 0.0007.47817.365 10.359 62.1972.451 4.556 2.750 2.0310.0004.088 0.000 0.0000.676 0.108 832.00.810.892 0.000 7.48 0.00 180.0 4/22/2025 10:45 0.0006.61817.366 10.396 55.2260.860 3.233 2.034 1.4130.0023.860 0.000 0.0000.589 0.122 832.00.810.844 0.000 6.62 0.00 180.0 4/22/2025 10:46 0.2486.96217.388 10.387 48.3970.000 2.079 1.393 1.2370.0063.790 0.000 0.0000.627 0.061 832.00.620.750 0.000 7.21 0.00 180.0 4/22/2025 10:47 0.1595.80017.401 10.358 59.5290.000 2.113 1.173 1.4130.0114.310 0.000 0.0000.817 0.114 832.00.720.731 0.000 5.96 0.00 180.0 4/22/2025 10:48 0.3214.95017.372 10.384 57.1840.575 2.973 1.084 1.4300.0004.192 0.000 0.0000.719 0.110 832.00.740.784 0.000 5.27 0.00 180.0 4/22/2025 10:49 0.0005.99117.336 10.441 50.7061.069 1.785 1.078 1.2260.0003.209 0.000 0.0000.651 0.046 832.00.710.924 0.000 5.99 0.00 180.0 4/22/2025 10:50 0.0007.14117.409 10.401 38.3010.000 2.104 1.085 0.7660.0113.543 0.000 0.0000.797 0.036 832.00.410.514 0.000 7.14 0.00 180.0 4/22/2025 10:51 0.0005.60617.476 10.414 44.4951.626 2.093 1.133 0.8560.0003.543 0.000 0.0000.915 0.066 832.00.580.671 0.000 5.61 0.00 180.0 4/22/2025 10:52 0.5997.10917.437 10.461 41.5900.652 1.574 1.220 0.7600.0013.420 0.000 0.0000.445 0.093 832.00.780.896 0.000 7.71 0.00 180.0 4/22/2025 10:53 0.3416.56317.379 10.378 43.5000.008 2.275 1.081 0.9910.0113.609 0.000 0.0000.469 0.079 832.00.680.775 0.000 6.90 0.00 180.0 4/22/2025 10:54 0.6148.93617.416 10.376 31.8420.000 1.775 0.814 0.3710.0003.338 0.000 0.0000.663 0.075 832.00.550.608 0.000 9.55 0.00 180.0 4/22/2025 10:55 1.0927.49217.344 10.398 39.6610.251 1.102 0.696 0.6670.0003.929 0.000 0.0000.716 0.093 832.00.790.898 0.000 8.58 0.00 180.0 4/22/2025 10:56 0.2955.31417.385 10.391 51.5781.301 2.359 0.935 1.0600.0013.715 0.000 0.0000.604 0.085 832.00.700.792 0.000 5.61 0.00 180.0 4/22/2025 10:57 0.1899.95017.415 10.387 42.5700.000 2.421 0.740 0.7230.0042.213 0.000 0.0000.696 0.087 832.00.620.669 0.000 10.14 0.00 180.0 4/22/2025 10:58 0.6546.02417.397 10.386 53.4550.000 1.605 0.712 1.0450.0003.691 0.000 0.0000.751 0.098 832.00.700.754 0.000 6.68 0.00 180.0 4/22/2025 10:59 0.0006.90017.355 10.419 50.6980.767 2.887 0.912 1.4090.0033.609 0.000 0.0000.791 0.079 832.00.700.805 0.000 6.90 0.00 180.0 4/22/2025 11:00 0.54516.91317.351 10.373 18.4620.000 2.328 0.592 0.0520.0001.587 0.000 0.0000.519 0.088 832.00.630.686 0.000 17.46 0.00 180.0 4/22/2025 11:01 0.0006.99217.357 10.352 34.3156.035 0.569 0.697 0.4820.0003.793 0.000 0.0000.623 0.085 832.00.700.793 0.000 6.99 0.00 180.0 4/22/2025 11:02 0.7246.24717.338 10.392 44.1405.311 2.149 1.398 1.0680.0003.341 0.000 0.0000.600 0.069 832.00.750.920 0.000 6.97 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/22/2025 11:03 0.2916.47517.348 10.417 45.8870.744 1.683 1.057 0.8850.0003.268 0.000 0.0000.520 0.086 832.00.760.874 0.000 6.77 0.00 180.0 4/22/2025 11:04 0.1456.02917.377 10.374 51.2120.362 2.181 1.044 1.0370.0003.994 0.000 0.0000.572 0.089 832.00.690.762 0.000 6.17 0.00 180.0 4/22/2025 11:05 0.0008.20517.385 10.341 33.9890.000 1.696 0.925 0.5640.0093.584 0.000 0.0000.773 0.031 832.00.400.506 0.000 8.21 0.00 179.0 4/22/2025 11:06 0.0007.44817.447 10.463 33.6430.094 1.302 0.705 0.2140.0003.166 0.000 0.0000.789 0.061 832.00.530.609 0.000 7.45 0.00 180.0 0.2677.36217.387 10.385 45.1041.382 2.198 1.174 0.9890.0033.459 0.000 0.0000.660 0.079 832.100.6660.762 0.000 7.628 0.000 179.9Avg. 0.3328.20017.382 10.376 41.5971.807 2.170 1.173 0.9970.0043.243 0.000 0.0000.642 0.078 832.550.6740.777 0.000 8.531 0.000 179.9Run 3 Avg: Baseline 3 4/22/2025 11:08 0.0000.0000.043 0.023 0.0000.000 0.000 0.223 0.0000.0000.049 0.000 0.0460.000 0.086 832.00.500.420 0.000 0.00 0.00 180.0 Post CTS 4/22/2025 11:10 0.0000.0000.024 0.042 0.0000.000 0.000 0.000 0.0000.0000.000 99.566 0.0000.064 0.164 832.066.920.311 0.013 0.00 0.00 180.0 4/22/2025 11:10 0.0000.0000.028 0.031 0.0080.000 0.000 0.000 0.6370.0000.000 99.017 0.0000.000 0.000 832.066.010.000 0.012 0.00 0.00 180.0 4/22/2025 11:10 0.0000.0000.018 0.049 0.0000.000 0.000 0.000 0.4470.0020.000 99.691 0.0000.302 0.103 832.066.940.411 0.015 0.00 0.00 180.0 Post NO2/Mid O2 4/22/2025 11:12 98.8123.1520.007 0.004 0.0010.000 0.987 0.094 0.1590.0000.000 0.000 0.0000.331 0.032 832.00.060.000 0.000 101.96 10.48 180.0 4/22/2025 11:12 98.5052.8510.016 0.017 0.5290.000 0.935 0.210 0.0000.0400.000 0.000 0.0000.000 0.079 832.00.270.165 0.000 101.36 10.43 180.0 4/22/2025 11:12 98.8913.8820.004 0.000 0.3010.000 1.012 0.085 0.0000.0000.000 0.000 0.0000.000 0.064 832.00.130.011 0.000 102.77 10.46 180.0 Post 5-Gas 4/22/2025 11:13 0.000242.6250.019 4.825 4.587473.445 1.746 2.249 1.7700.4990.000 1.253 247.9090.554 0.931 832.0252.132.280 9.612 242.63 0.00 179.0 4/22/2025 11:13 0.000245.3210.012 4.877 4.579476.190 1.757 2.115 0.5660.4180.000 1.152 250.6471.138 1.064 832.0255.222.516 9.681 245.32 0.00 180.0 4/22/2025 11:14 0.000245.3480.008 4.857 4.283478.686 1.843 2.216 0.8240.5400.000 1.083 250.5270.000 0.930 832.0254.622.264 9.710 245.35 0.00 180.0 4/22/2025 11:14 0.000245.4880.011 4.866 4.250479.960 1.836 2.213 0.0000.5600.000 1.078 251.0940.732 0.904 832.0254.711.637 9.718 245.49 0.00 180.0 4/22/2025 11:14 0.000247.8570.009 4.894 5.031479.302 1.881 2.085 0.5020.0440.000 1.063 251.2050.841 0.829 832.0254.972.091 9.721 247.86 0.00 180.0 4/22/2025 11:14 0.000247.0880.010 4.890 5.262478.720 1.779 2.253 0.3060.2710.000 1.090 251.8090.236 0.696 832.0255.472.305 9.722 247.09 0.00 180.0 End of Test Purge 4/22/2025 11:16 0.0000.3960.010 0.021 0.0000.080 0.035 0.164 0.0000.0880.000 0.000 0.5050.000 0.048 832.00.950.524 0.000 0.40 0.00 180.0 4/22/2025 11:16 0.0000.333-0.000 0.003 0.0000.000 0.028 0.066 0.3360.0000.161 0.000 0.2320.000 0.153 832.00.890.532 0.000 0.33 0.00 180.0 4/22/2025 11:16 0.0000.0000.019 0.021 0.0000.000 0.000 0.255 0.0000.0060.000 0.000 0.4800.235 0.045 832.00.610.058 0.000 0.00 0.00 180.0 4/22/2025 11:16 0.0000.955-0.000 0.007 0.3730.000 0.000 0.180 0.2920.0090.000 0.000 0.0390.000 0.164 832.00.810.660 0.000 0.96 0.00 180.0 4/22/2025 11:16 0.0000.0000.001 0.002 0.1920.000 0.034 0.164 0.1400.0000.000 0.000 0.1510.599 0.112 832.00.460.129 0.000 0.00 0.00 180.0 4/22/2025 11:16 0.0000.0000.004 0.003 0.0000.000 0.000 0.000 0.0000.0120.107 0.000 0.0000.000 0.118 832.00.300.101 0.000 0.00 0.00 180.0 GAS Date Time H2O (%) CO2 (%) CO (ppmvw) NO (ppmvw) NO2 (ppmvw) CH4 (ppmvw) N2O (ppmvw) NH3 (ppmvw) SO2 (ppmvw) C2H4 (ppmvw) HCL (ppmvw) HF (ppmvw) C2H6 (ppmvw) C3H8 (ppmvw) C6H14 (ppmvw) C2H4O (ppmvw) SF6 (ppmvw) Nox (ppmvw) VOC (ppmvw) Oxygen (%) Cell Temp (C). Ambient Press. (mbar) 4/22/2025 11:16 0.0000.0000.008 0.000 0.0000.000 0.077 0.056 0.0130.0010.000 0.000 0.2770.000 0.082 832.00.970.793 0.000 0.00 0.00 180.0 4/22/2025 11:16 0.0000.0000.001 0.011 0.1030.000 0.000 0.087 0.3560.0000.000 0.000 0.0000.159 0.081 832.00.460.439 0.000 0.00 0.00 180.0 4/22/2025 11:16 0.0000.0000.007 0.010 0.0000.000 0.017 0.087 0.0000.0280.000 0.000 0.0510.000 0.172 832.00.880.727 0.000 0.00 0.00 180.0 GAS