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DAQ-2024-007209
rnostardi e platt Gontinuous Emissions Monitoring System Relative Accuracy Test Audit Report Ash Grove Gement Company rLeamington Gement Plant Main Kiln Stack Leamington, Utah June 20,2023 Report Submittal Date August 10,2023 @ Copyright2023 Allrights reserved in Mostardi Platt Project No. M2325124 TABLE OF CONTENTS 1.0 EXECUTTVE SUMMARY............... ............................1 2.0 TEST METHODOLOGY............ ...........2 Method 1 Sample and Velocity Traverse Determination................. ...............2 Method 2 and 2H Volumetric Flow Rate Determination ................. ................2 Method 3A Oe Determination...... ........3 Method 4 Moisture (HzO) Determination ................3 Method 25A Total Hydrocarbon (THC) Determination ................. ..................3 Method 30B Hg Determination ................. ..............3 Method 3201321 HCl, COz, HzO, NOx, and CO Determination ................. .........................4 3.0 TEST RESULT SUMMARIES ..............5 4.0 CERTIFICATION APPENDICES Appendix A - Test Section Diagrams ...................17 Appendix B - Sample Train Diagrams............... .......................20 Appendix C - Calculation Nomenclature and Formulas ...........25 Appendix D - Reference Method Test Data .........36 Appendix E - CEMS and Plant Operating Data............ ..........., 64 Appendix F - Field Data Sheets ........90 Appendix G - Calibration and Response Time Data ........... ....................... 132 Appendix H - Calibration Gas Cylinder Data ......148 Appendix l- Mercury QA Data...... .....................156 Project No. M232512A Main Kiln Stack @Mostardi Platt 1.0 EXECUTIVE SUMMARY Mostardi Platt conducted a Continuous Emissions Monitoring System (CEMS) Relative Accuracy Test Audit (RATA) for Ash Grove Cement Company at the Leamington Cement Plant in Leamington, Utah, on the Main Kiln Stack on June 20,2023. This report summarizes the results of the test program and test methods. The test location, test date, and test parameters are summarized below. The purpose of the test program was to demonstrate the relative accuracies of the Main Kiln Stack NOx, CO, COz, Oz, THC, Hg, HCl, and volumetric flow analyzers during the specified operating condition. The test results from this program indicate that each CEMS meets the United States Environmental Protection Agency (USEPA) annual performance specification for relative accuracy as published in 40 Code of Federal Regulations Part 60 (40CFR60) and 40 CFR 63 Subpart LLL. Note that all reference method data is one hour ahead of plant CEMS time. RATA TEST INFORMATION Test Location Test Date Test Parameters Main Kiln Stack June 20,2023 Carbon Dioxide (COz), Oxygen (Oz), Nitrogen Oxides (NOx), Carbon Monoxide (CO), Total Hydrocarbons (THC), Mercury (Hg), Volumetric Flowrate (VFR), and Hydrogen Chloride (HCl) RATA RESULTS Test Location Parameter Units Relative Accu racy Acceptance Criteria Relative Accuracy (RA) Main Kiln Stack NOx ppmvw 320.0o/o of the mean reference value 15.06% NOx lb/hr <20.0% of the mean reference value 15.64Yo co ppmvw 3 10.0Yo of the mean reference value 5.69% co lb/hr 3 20.0o/o of the mean reference value 6.1'.t% COz o/o wal 3 20.0o/o of the mean reference value 6.94Yo Oz o/o dry < 20.0% of the mean reference value 2.360/o VFR scfh 310.0o/o of the mean reference value 1.41% THC ppmvd@7o/oOz 3 10.0o/o of the applicable performance standard of 24 ppmvd @7% Oz 1.41o/o Hg ug/wscm s 1.0 ug/wscm + confidence coefficient (cc) for sources s5.0 ug/wscm 0.234 mean difference + cc HCt ppmvd@3%Oz < 15.0% of the applicable performance standard of 3.0 ppmvd @7o/o Oz 7.73o/o Project No. M2325124 Main Kiln Stack 1 of 166 @Mostardi Platt TEST PERSONNEL INFORMATION Location Address Contact Test Facility Ash Grove Cement Company ur-132 Leamington, UT 84638 Mr. Cody Watkins Environmental Manager (43s) 857-1212 Codv.watkins@ashorove.com Testing Company Representative MostardiPlatt SSS lndustrial Drive Elmhurst, 1160126 Mr. Richard J. Sollars ll RegionalManager (630) e93-2100 rsollars@mp-mail.com www.mostardiplaft.com The identifications of the individuals associated with the test program are summarized below. The test crew consisted of W. Petrovich, S. McGough, T. Magana, B. Alba, and R. Sollars of Mostardi Platt. 2.0 TEST METHODOLOGY Emission testing was conducted following the USEPA methods specified in 40CFR60, Appendix A in addition the Mostardi Platt Quality Manual. Schematics of the test section diagrams and sampling trains used are included in AppendixAand B respectively. Calculation nomenclature are included in Appendix C. Copies of analyzer print-outs for each test run are included in Appendix D. CEM data and process data as provided by Ash Grove Cement Company are also included in Appendix E. The following methodologies were used during the test program: Method 1 Sample and Velocity Traverse Determination Test measurement points were selected in accordance with USEPA Method 1, 40CFR60, Appendix A. The characteristics of the measurement location is summarized below. Method 2 and 2H Volumetric Flow Rate Determination Gas velocity was measured following USEPA Method 2, 40CFR60, Appendix A, for purposes of calculating stack gas volumetric flow rate and emission rates on a lb/hr basis. An 8-foot long S- type pitot tube, 0-10 inch differential pressure gauge, and K-type thermocouple and temperature readout were used to determine gas velocity at each sample point. ln accordance with Method 2H, a default wall affect adjustment factor of 0.995 was used for non-brick and mortar stacks. All of the equipment used was calibrated in accordance with the specifications of the Method. Copies Poject No. M232512A Main Kiln Stack SAMPLE POINT SELECTION Test Location Stack Diameter Upstream Distance Downstream Distance Test Parameters Number of Sampling Points Main Kiln Stack 132 lnches 4.09 Diameters 5.05 Diameters Oz,COz, NOx, CO, THC, Hg 3 Volumetric Flowrate 16 2 of 166 OMostardi Plaft of field data sheets are included in Appendix F. Calibration data are presented in Appendix G. This testing met the performance specifications as outlined in the Method. Method 3A Oz Determination Stack gas Oz concentrations and emission rates were determined in accordance with USEPA Method 3A, 40CFR60, Appendix A. A Thermo analyzer was used to determine the Oz concentrations in the manner specified in the Method. The instrument has a paramagnetic detector and operates in the nominal range of 0% to 25% with the specific range determined by the high-level calibration gas. High-range calibrations were performed using USEPA Protocolgas. Zero nitrogen (a low ppm pollutant in balance nitrogen calibration gases)was introduced during other instrument calibrations to check instrument zero. High- and a mid-range % Oz levels in balance nitrogen were also introduced. Zero and mid-range calibrations were performed using USEPA Protocol gas. Copies of the gas cylinder certifications are found in Appendix H. This testing met the performance specifications as outlined in the Method. Method 4 Moisture (HzO) Determination Stack gas moisture content was determined using a Method 4 sampling train. ln this technique, stack gas is drawn through a series of four impingers. The first two impingers are each charged with 100 mls of deionized, distilled water. lmpinger three is left empty and impinger four is charged with clean, dried silica gel. The entire impinger train is measured or weighed before and after each test run to determine the mass of moisture condensed. During testing, the sample train was operated in the manner specified in USEPA Method 4. All of the data specified in Method 4 (gas volume, delta H, impinger outlet well temperature, etc.)was recorded on field data sheets. All of the equipment used is calibrated in accordance with the specifications of the Method. Calibration data can be found in Appendix G. Method 25A Total Hydrocarbon (THC) Determination THC concentrations and emission rates were determined in accordance with Method 25A. A Thermo Fisher 51i analyzer was used to determine THC concentrations. Stack gas was delivered to the system via a Teflon@ sampling line, heated to a temperature of 375"F. The system was calibrated using certified calibration gases of propane. A list of calibration gases used and the results of all calibration and other required quality assurance checks can be found in Appendix G. Copies of calibration gas certifications can be found in Appendix H. Method 308 Hg Determination Paired trains were utilized sampling three test points per test run at the Main Kiln Stack. Per Method 30B sampling, each sample was collected on the paired in-situ sorbent traps. A tube of silica was used to capture remaining moisture prior to the sample reaching the gas metering system. The sample train used for this test program was designed by APEX, lnc. and meets all requirements for Method 308 sampling. Samples were analyzed onsite utilizing an Ohio Lumex, lnc. analyzer for total gaseous mercury. Sample analysis data and mercury quality assurance and control data are found in Appendix l. All of the equipment used was calibrated in accordance with the specifications of the Method. Project No. M2325124 Main Kiln Stack 3 of 166 @Mostardi Platt Method 32A1321 HGl, COz, HzO, NOx, and CO Determination Extractive Fourier transform infrared (FTIR) spectrometry following USEPA Method 320 and Method 321 will be performed for determination of HCl, COz, HzO, NOx, and CO. FTIR technology works on the principle that most gases absorb infrared light. This is true for all compounds with the exception of homonuclear diatomic molecules and noble gases such as: Nz, Oz, Hz, He, Ne, and Ar. Vibrations, stretches, bends, and rotations within the bonds of a molecule determine the infrared absorption distinctiveness. The absorption creates a "fingerprint" which is unique to each given compound. The quantity of infrared light absorbed is proportional to the gas concentration. Most compounds have absorbencies at different infrared frequencies, thus allowing the simultaneous analysis of multiple compounds at one time. The FTIR software compares each sample spectrum to a user-selected list of calibration references and concentration data is generated. FTIR data will be collected using an MKS MultiGas 2030 FTIR spectrometer. Analyte spiking with HCI and SFo gas will assure the ability of the FTIR to quantify analytes in the presence of effluent gas. Ethylene gas will be used as the calibration transfer standard. All analyte spikes will be introduced using an instrument grade stainless steel rotometer. All QA/QC procedures will be within the acceptance criteria allowance of Methods 320 and 321. Project No. M2325'l2A Main Kiln Stack 4 of 166 @Mostardi Platt 3.0 TEST RESULT SUMMARIES Client Ash Grow Cement Company Location: Main Kiln Stack Facility: Leamington Cement Plant Datel.6120123 Project #: M232512 Te$ Method: 320 NOx oPmvw RATA 1=accept 0=reject Te$ Run Clinker ton/hr Iest Date Start Time End Time RM NOx Ppmw, CEM NOx ppmvw (RMCEM) Difference (dt) (RM€EM) Difference2 (di2) 0 1 '117.5 06120123 7:30 7:59 197.6 228.8 -31.2 973.M 1 2 118.4 06t20t23 8:07 8:36 208.3 238.9 -30.6 936.36 1 3 114.7 06120t23 8:43 9:12 209.7 240.0 -30.3 918.09 1 4 119.1 06120t23 q.35 '10:04 195.6 225.4 -29.8 888.04 I 5 119.1 06120t23 10:12 1O:4'l 192.8 222.6 -29.8 888.04 1 6 119.3 06t20t23 10:48 '11:17 207.8 238.0 -30.2 912.U 1 7 119.3 06120t23 11:38 12:07 200.1 229.3 -29.2 852.64 1 8 119.5 o6t20t23 12:.13 12:42 198.1 226.7 -28.6 817.96 1 9 119.0 06t20t23 12:50 13:19 210.3 240.0 -29.7 882.09 10 1't8.6 06120t23 13:40 14:09 193.9 220.1 -26.2 686.,14 n 9 (0.s75)2.306 Mean Reference Method Value 201.84 RM avg Mean GEM Value 231.222 3EM avg Sum of Differencer -264.400 I Mean Difference a9.378 Sum of Differences Squared 7781.700 ,i2 Standard Deviatior 1.333 ld Confi de nce Coeffi cl e nt 2.5oh Error (1 -tall'1.025 gc Relative Accuracl 15.06 RA Project No. M2325124 Main Kiln Stack 5 of 166 @Mostardi Platt Client: Ash Grow Cement Company Facility: Leamington Cement Plant Proiect #: M232512 Location: Main Kiln Stack Test Method: 320, 2 NO,lb/hr RATA 1=accept 0=reject Te* Run Clinker ton/hr Iesil Date Start Time End Time RM NO, lb/hr CEM NO, lb/hr (RM-CEM) Difference (di) (RMCEM) Difference2 (di2) 1 1 117.5 06t20t23 7;30 7:59 270.63 295.62 -24.99 624.5001 1 2 118.4 06t20t23 8:07 8:36 279.72 310.25 30.53 932.0809 1 3 114.7 06120123 8:43 9:12 276.18 312.57 -36.39 1324.2321 1 4 119.1 06t20t23 9:35 10:04 255.74 298.89 43.15 1861 .9225 1 5 119.1 06120123 10'.12 10:-41 260.06 298.88 -38.82 1506.9924 0 6 119.3 06120t23 1O:.48 11:17 272.24 318.28 46.04 2119.6816 1 7 119.3 06t20t23 11:38 12:07 263.61 307.60 43.99 1935."t201 I I 119_5 06120123 12:13 12:42 262.10 304.26 42.16 1777.4656 1 9 119.0 06t20123 12:50 13:19 283.02 321.87 -38.8s 1509.3225 1 10 118.6 06120123 13:40 14:09 261 .15 296.51 35.36 1250.3296 n 9 t(0.975)2.306 Mean Reference Method Value 268.023 RM avg Mean CEM Value 305.{6'l iEM avq Sum of Differencer -33/..240 da Mean Difference -37.138 d Sum of Differences Squareo 12721.966 di2 Standard Deviation 6.215 sd Confi de nce Coeffi cie nt 2.5o/o Error (1 -tail 4.777 cc Relative Accuracv 15.64 RA Project No. M2325124 Main Kiln Stack 6 of 166 OMostardi Platt Client: Ash Grore Cement Company Location: Main Kiln Stack Facility: Leamington Cement Plant Dale:6120123 Project #: M232512 Test Method: 320 CO pomvw RATA 1=accept 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM CO ppmvw CEM CO ppmvw (RM.CEM) Difference (di) (RMCEM) Difference2 (di1 1 1 117.5 06t20t23 7:30 7:59 1021.0 985.1 35.9 1288.81 1 2 118.4 06120t23 8:07 8:36 'l 185.8 1225.6 -39.8 1584.04 1 3 114.7 o6t20t23 8:43 9:12 1253.7 t286.8 33.'l 1095.61 1 4 119.1 06t20t23 9:35 10:04 1488.8 1566.4 -77.6 6021.76 I 5 119.1 06t20123 1O:12 1O:41 577.9 529.2 48.7 2371.69 1 6 119.3 06t20t23 10:48 11'.17 44't.1 4U.4 6.7 44.89 1 7 119.3 o6t20t23 11:38 12:O7 455.6 468.0 -12.4 153.76 1 8 119.5 06t20t23 12:13 12:42 465.1 470.4 -5.3 28.09 0 I 119.0 06t20t23 12:50 13:19 618.6 697.8 -79.2 6272.64 1 10 118.6 06t20t23 13:40 14:09 538.4 595"7 -57.3 3283.29 n 9 (0.975)2.306 Mean Reference Method Value 825.267 RM avq Mean CEM Value 840.178 CEM avq Sum of Differences -134.200 di Mean Difference -14.911 d Sum of Differences Squared 1s871.940 di2 Standard Deviation 41.640 sd Confi de nce Coefficie nt 2.5o/o Enor 11 -laill 32.007 cc Relative Accurac 5.69 RA Project No. M2325124 Main Kiln Stack 7 of '166 @Mostardi Platt Client Ash Grow Cement Company Facility: Leamington Cement Plant Project #: M232512 Location: Main Kiln Stack TeS Method: 320, 2 GO lb/hr RATA l=accept 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM CO lb/hr CEM GO lb/hr (RM.cEM) Difference (di) (RM4EM) Difference2 (di2) 1 1 117.5 06120123 7:30 59 851.'t5 775.53 75.62 5718.38/,4 1 2 118.4 06t20t23 8:07 36 968.83 968.55 0.28 0.07u 1 3 114.7 06t20t23 8:43 9:12 1004.69 1020.09 -15.40 237.1600 1 4 1't9.1 06t20t23 9:35 10:04 1184.30 1264.87 40.57 6491 .5249 I 5 119.1 06120t23 1O:12 1O:'41 474.32 432.85 41.47 1719.7609 b 1't9.3 06t20t23 10:48 11:17 351.72 353.53 1.8'1 3.2761 7 't 19.3 06120123 11:38 12:07 365.1 9 382.30 -17.11 292.7521 1 8 1 19.5 06120t23 12:13 12:42 374.52 3U.49 -s.97 99.4009 0 I 119.0 06t20123 12:50 13: 19 506.55 569.95 63.40 4019.5600 10 118.6 06120t23 13:40 14:09 441.37 488.09 46.72 2182.758/. n I (0.97s)2.306 Mean Reference Method Value 668.454 RM avo Mean CEM Value 674.478 CEM avE Sum of Differencer 4.210 di Mean Difference 6.023 d Sum of Differences Souarec 16745.096 di2 Standard Deviatior 45.303 sd Confi dence Coefficient 2.5o/o Error 11 -lai 34.82t cc Relative Accuracl 6.11 RA Project No. M232512A Main Kiln Stack 8 of '166 OMostardi Platt Clienf Ash Grow Cement Company Facility: Leamington Cement Plant Project#: M232512 Location: Main Kiln Stack Te* Method: 320 CO2% (wet) RATA 'l=accepl 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM CO2 % (wet) CEM CO2o/o (wet) (RM.CEM) Difference (di) (RMCEM) Difference2 (di1 1 1 117.5 06120t23 7:30 7:59 12.7 13.6 {.9 0.81 1 2 118.4 06t20t23 8:07 8:36 12.8 13.5 4.7 0.49 1 3 114.7 06120123 8:43 9:12 12.8 13.7 4.9 0.81 1 4 1 19.1 06124t23 9:35 10:04 12.5 13.3 {.8 0.64 1 5 1 19.1 06t20t23 10:12 10:41 12.5 13.3 4.8 0.64 1 6 1 19.3 06t20t23 1o.4R 1'.l 17 12.5 13.4 4.9 0.81 1 7 1 19.3 06t20t23 '11:38 '12:O7 12.5 '13.3 4.8 0.& 1 8 1 19.5 06t20123 12:13 12:42 12.5 13.3 {.8 0.64 1 I 1 19_0 06t20t23 12:50 13:19 12.5 't3.3 -0.8 0.& 0 10 118.6 06t20t23 13:40 14:09 12.5 13.4 4.9 0.81 n I (0.9751 2.306 Mean Reference Method Value 12.589 RM avo Mean CEM Value 13.411 CEM avE Sum of Differences -7.400 di Mean Difference 4.822 d Sum of Differences Squared 6.120 di2 Standard Deviation 0.067 Bd Confidence Coefficient 2.5% Error (1-tail 0.051 CG Relative Accuracy 6.94 RA Project No. M2325124 Main Kiln Stack 9 of '166 @Mostardi Platt Client: Ash Grow Cement Company Location: Main Kiln Stack Facility: Leamington Cement Plant DaE:6120123 Project #: M232512 Tesil Method: 34 02 % (wet) RATA 1=accept 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM02% (wet) cEM 02 % (wet) (RM-CEM) Difference (di) (RMCEM) Difference2 (di2) 1 1 117.5 06120t23 7:30 7:59 9.2 9.0 o.2 0.04 0 2 118.4 06t20123 8:07 8:36 9.4 8.9 0.5 0.25 1 3 114.7 06t20t23 8:43 9:12 9.3 8.8 0.5 0.25 1 4 1 19.1 06t20t23 9:35 10:04 9.0 9.0 0.0 0.00 1 5 119.1 06t20t23 10:12 1O:41 9.0 9.1 {.1 0.01 1 6 119.3 06120123 10:48 11:.17 9.1 9.1 0.0 0.00 1 7 119.3 o6t20t23 1 1:38 12:07 9.2 9.1 0.1 0.01 1 8 119.s 06t20t23 12:.13 12'.42 9.0 9.1 {.1 0.01 1 I 1 19.0 06120123 12:50 13:19 9_1 9.2 {.1 0.01 1 10 118.6 06t20t23 13:40 14:09 9.2 9.1 0.1 0.01 n I t(0.97!2.306 Mean Refurence Method Value 9.122 RM avq Mean CEM Value 9.056 CEM avq Sum of Differences 0.600 di Mean Difference 0.067 d Sum of Differences Squared 0.340 di2 Standard Deviation 0.194 sd Confi de nce Coefficie nt 2.5o/o Error 11 -lai 0.149 cc Relative Accuracy 2.35 RA Project No. M232512A Main Kiln Stack 10 of 166 @Mostardi Platl Client: Ash Grole Cement Company Location: Main Kiln Stack Facility: Leamington Cement Plant Test ltr/lethod: 25A, 34 Projec{ #: l.v1232512 Applicable Standard: 24 THC oomvd @ 7oh 02 RATA 1=accept 0=reject Test Run Glinker ton/hr Test Date Start Tirne End Time RM THC ppmvd @ 7% 02 CEM THC ppmvd@7o/o 02 (RM-CEM) Difference (di) (RM-CEM) Difference2 (di2) 0 1 117.533 06120t23 7:30 7:59 13.7 13.1 0.6 0.41 1 2 118.437 06120123 8:07 8:36 18.9 18.6 0.3 0.08 1 3 114.737 06120123 8:43 9'.12 13.3 12.8 0.5 0.30 1 4 1't9.067 06t20t23 9:35 10:04 13.3 12.8 0.5 0.21 1 5 119.14 06120123 10:12 10:41 13.2 13.2 0.0 0.00 1 6 119.287 06t20t23 10:48 11:17 13.3 13.5 -0.2 0.05 1 7 119.3 06t20t23 11:38 12:07 13.6 13.7 -0.1 0.01 1 8 119.473 06t20t23 12:13 12:42 12.9 13.6 -o.7 0.42 1 I 1 19.003 06120123 12:5O 13:19 '13.3 13.4 -0.1 0.00 I 10 118.613 06t20123 13:40 14:09 12.7 13.2 -0.5 0.23 n 9 r(0.975)2.306 llllean Reference Method Value 13.833 RM avq Itllean CEM Value 13.861 CEM avq Sum of Differences -0.247 di lllean Difference -0.027 d Sum of Differences Squarec 1.312 di2 Standard Deviatior 0./O4 sd Confidence Coefiicient 2.5% Error (1-tail)0.310 GC Relative Accuracy - APS 1.41 RA o Relatile accuracy based upon +t- 10% of applicable standard of 24 ppmvd @7o/" 02 Project No. M2325124 Main Kiln Stack 11 of 166 @Mostardi Platt Glient Ash Grow Cement Company Plant Leamington Cement Plant Project #: M232512 Location: Main Kiln Stack Dale:6120123 Te$ Method: Sorbent Hg (308) Ho uo/wscm F{ATA 1=accept 0=reject Tesil Run Test Date Start Time End Time RM ug/wscm CMMS ug/wscm (RMCMMS) Difference (di) (RMCMMS) Difference2 (di2) 1 1 06t20t23 07:30 08:00 0.496 0.547 4.051 0.003 1 2 06t21t22 08:07 08:37 0.463 0.501 -0.038 0.001 1 3 06120t23 08:43 09:1 3 0.460 0.510 4.050 0.003 1 4 06120t23 09:35 10:05 0.623 0.795 4.172 0.029 1 5 06120123 1O:12 10:42 o.977 1.261 4.2U 0.081 0 6 06t20t23 10:48 11:18 0.985 1.421 4.436 0.190 1 7 06120t23 1 1:38 12:08 0.990 1.100 {.110 o.012 1 8 06t20t23 12:13 12:43 0.806 1.03s 4.229 0.053 1 9 06120123 12:50 13:20 0.655 0.894 4.239 0.057 1 10 06120t23 13:40 14:10 0.677 0.934 4.257 0.066 (0.025) Mean Reference Method Value Mean CMM Value Sum of Differences Mean Difference Sum of Differences Squared Standard Deviation Confi dence Coefficient 2.5oh Error (1 -tail) Relative Accuracv{PS 9 2.306 0.683 RM avq 0.u2 CMM avq -1.430 di {.159 d 0.305 di2 0.098 Bd 0.076 GG 0.234 RAA A Relative Accuracy based on rrean difference of +A1 .0 ug/w scm plus @ f or enission sources <5.0 ug/w scm of rercury Project No. M232512A Main Kiln Stack 12 of '166 @Mostardi Platl Client: Ash Grore Cernent Company Location: Main Kiln Stack Facility: Leamington Cement Plant Test tUlethod: 321, 34 Project #: t/€32512 Applicable Standard: 3 HClppmvd @7% 02 RATA 1=accept 0=rejec-t Test Run Clinker ton/hr fest Date Start Tirne End Time RM HCI ppmvd@7% 02 CEM HCI pprvd @ 7% 02 (RM-CEM) Difference (di) (RM-CEM) Difference2 (di2l 1 1 117.5 06t20t23 7:30 7:59 0.7 0.3 0.4 0.16 1 2 118.4 06t20t23 8:07 8:36 0.3 0.2 0.1 0.01 I 3 114.7 06t20t23 8:43 9'.12 0_5 0.4 0.1 0.01 0 4 119.'t o6t20t23 9:35 10:M 0.7 0.3 0.4 0.16 1 5 119.1 06t20t23 1O:.12 1O:41 0.4 0.4 0.0 0.00 1 6 119.3 06t20t23 10:48 11:17 0.0 0.4 -0.4 0.16 1 7 1't9.3 06t20t23 11:38 12:07 0.6 0.3 0.3 0.09 1 8 119.5 06t20t23 12'.13 12:42 0.'l 0.4 -0.3 0.09 1 I 119.0 06120t23 12:50 13:19 0.1 0.3 -0.2 0.04 I 10 118.6 06t20t23 13:40 14:09 0.6 0.4 o.2 0.04 n 9 (0.975)2.306 Illlean Refurence lJlethod Value 0.367 RM avq Ittuan CEM Value 0.344 CEM avg Sum of Differences 0.200 di Mean Difierence 0.022 d Sum of Difierences Squared 0.600 di2 Standard Deviation 0.273 sd Confidence Goefficient 2.5% Error (l-tail)0.210 cc Relative Accuracv - APS 7.73 RA A Relatire accuracy based upon +l- 15o/o of applicable standard of 3 ppnM @7% 02 Project No. M2325124 Main Kiln Stack 'l 3 of 166 @Mostardi Platt Client Ash Grow Cement Company Test Location: Main Kiln Stack Facility: Leamington Cement Plant Test Date: 612012023 Project #: M232512 Test Method: 2, D2H WAF: 0.995 Volunrctric Eow RATA - tSrnnl Load 1=accept 0=reject Tes{ Run Test Date Start Time End Time Wall Effect Adjusted Reference Method Flow SCFH CEM Flow SCFH (RM4EM) Difference (di) (RMCEM) Difference 2 (di2) 0 1 06120t23 07:30 07:59 1 t,473,000 10.821,600 651,400 424.321.960.000 1 2 06120123 08:07 08:36 11.245.000 10.877.200 367.800 13s.276.840.000 1 3 06120t23 08:43 09:12 11.02S.000 10.907.800 121.200 14.689.440.000 1 4 o6t20123 09:35 1O:04 10.948.000 1 .1 1 't .000 -163,000 26.569.000.000 ,|5 o6t20t23 10:12 1O:41 11,297.000 11,247,400 49,600 2.460.160.000 ,|6 06t20t23 10:48 11:17 11,019,000 1 'l ,196,200 -177,200 31.399.840.000 1 7 06120123 11:38 12:07 11.032.000 11,236,400 -204.400 41.779.360.000 1 8 06t20123 12:13 12:42 11.082.000 11.236.200 -1il.200 23.777.640.000 1 I 06120t23 12:50 13:19 'fi.270.000 11.235.800 34.200 1.169.640.000 1 10 06120123 13:40 14:09 11.282.000 11.242.OOO 0 0 n 9 (0.025)2.306 Mean Reference Method Value 11133777.778 RM avq Mean CEM Value 11147777.778 UEM AVO Sum of Differencer -126000.000 di Mean Diffurence -14000.000 d Sum of Differences Souared 277121920000.000 di2 Standard Deviation 185525.578 ed ]onfi de nce Coefficie nt 2.5o/o Enor 11 -Lail 142607.327 Relative Accurac!1.41 RA Project No. M232512A Main Kiln Stack 14 of '166 @Mostardi Platt 4.0 CERTIFIGATION Mostardi Platt is pleased to have been of service to Ash Grove Cement Company. !f you have any questions regarding this test report, please do not hesitate to contact us at 630-993-2100. As the program manager, I hereby certify that this test report represents a true and accurate summary of emissions test results and the methodologies employed to obtain those results. The test program was performed in accordance with the test methods and the Mostardi Platt Quality Manual, as applicable. MOSTARDI PLATT (al "/= S{t- prosram Manaser Richard J. Sollars ll *J,w Eric L. Ehlers Project No. M2325124 Main Kiln Stack Quality Assurance 15 of 166 @Mostardi Platt APPENDICES Project No. M2325124 Main Kiln Stack '16 of 166 @Mostardi Platt Appendix A - Test Section Diagrams Project No. M2325124 Main Kiln Stack 17 of 166 @Mostardi Platt GASEOUS TRAVERSE FOR ROUND DUCTS (Oz, COz, NOx, CO, THC, Hg, HCI) Project:Ash Grove Cement Company Leamington Cement Plant Leamington, Utah Main Kiln Stack June 20,2023 3 132 lnches 94.99 Square Feet 4.09 5.45 Length > 1l2Dia.T Length > 2Dia.I Test Location: Test Date: No. Sample Points: Stack Diameter: Stack Area: Upstream Diameters: Downstream Diameters: Project No. M2325124 Main Kiln Stack 18 of 166 OMostardi Plaft EQUAL AREA TRAVERSE FOR ROUND DUGTS (Volumetric Flow Rate) Length > 112Dia.T Length > 2Dia.I Test Date: Test Location: Stack Diameter: Stack Area: Upstream Diameters: Downstream Diameters: Ash Grove Cement Company Leamington Cement Plant Leamington, Utah June20,2023 Main Kiln Stack 132 lnches 94.99 Square Feet 4.09 5.45 Project No. M2325124 Main Kiln Stack 4 3 2 1 1234 1 2 3 4 @Mostardi Platt Appendix B - Sample Train Diagrams Project No. M232512A Main Kiln Stack 20 of 166 @Mostardi Platt 7.62 cm (3 in.). 1.90-2.54 cm (0.75 -1.0 in.). Flexible Tubing (0.25 in.) USEPA Method 2-Type S Pitot Tube Manometer Assembly "Suggested (lnterference Free) Pitot tube/ Thermocouple Spacing ATD-001 USEPA Method 2 Rev. 1.2 'U1t2021 Project No. M2325124 Main Kiln Stack 21 of 166 @Mostardi Platt USEPA Method 4- Moisture Content Sample Train Diagram Vacuum Gauge ATD-032 USEPA Method 4 Project No. M232512A Main Kiln Stack Rev. 1.2 22 of '166 @Mostardi Platt USEPA Methods 3A, 25A, and3201321 - Sample Train Diagram r -+-- III5ffi1 I lg:'J- ATD-081C USEPA Method 3/2SA/320 Project No. M2325124 Main Kiln Stack Rev.0.1 23 of 166 7/tl2O2t @Mostardi Platt USEPA Method 30B- Mercury Sorbent Trap Sampling Train ATD-071 USEPA Method 308 Project No. M232512A Main Kiln Stack 24 of 166 @Mostardi Platt Appendix C - Galculation Nomenclature and Formulas Project No. M232512A Main Kiln Stack 25 of 166 OMostardi Platt Cliont: Ash Grove Cement Company Faclllty: Leamington Cement Plant Prcleca*t M232512 Tost Lo€tlon: Main Kiln Stack Oalet 6120123 FTIR Samole CalculaUons Dircct Recovory % ot Calibr.lion Tmnsisr Standard DRo= Dr x100 Cma Cma- 100.2 DR6= 99.E% Rocovory % with Calibration Transfer Standard Systom Purge Rd= SYrd x 100 Dd Syr*= 100.0 Rcn = 1OO'/. Direct Recovory % of Analyte Spiko Gas sF6 D&ir Ds x100 Cma D&t' 96.7'/o Dllutlon Factor for AnsMe Splking DFr Spks D6 Spkd. 0.3!t6 DF = 0.082 R.covery'/6 forAnah e Splko Wth HCI &= sPk, sp& = 2.8 DF = 0.082 MGtardi Platt Project No. M232512A Main Kiln Stack Da= 100.0 Dor = 100.0 Do- 4.8 D.r= 4.833 &e 101.5 wherc: DRd = Recovery % ofthe clibration transfer sbndard direcdy to the aml}rzs Cma = certified @ncentrauon of clibratim gas, ppm D6 = Concfibation of the calibraton tansfer standard gas dire€tly to the analfzer. ppm &b. Recovery % of the callbration kansfer standard hrough the smpling q/Sm Sysa = Concenbation ofthe clibration Earder standard gas through the system, ppm DF . Dilution Factor of analyte spike gas Spk.c r SF6 @nentrauon in effiuent during spiking Spk, - 53y" -n."nb'afion in emuent during spiklng Dq = Concentration of the analyte spike gas direcuy to tfie anatfzer, ppm Ds r Concentration of the SF6 dkectly to the anal)raer, ppm R, . Rtrorery % of the analyte spike gas N, = NaWe effluent (HO) concentrauon prior to analyte spike Nr= Dq'29.1 v5.0 26 of 166 RATA Extractive 4/16/20 @Mostardi Platt Client: Ash Grove Cement ComPany Facility: Leamington Cement Plant Project#: M232512 Test Location: Main Kiln Stack Oale:6120123 Run: 1 Sample Calculations ( 11.30 o/o - 0.00 o/o) x O2o/o (dry) Lt.06 o/o = 11.31 o/o 11.05 o/o - 0.00 o/o THC ppmvd @ 7o/o 02 7.7 ppmvw / (1- 0.188) x ((20.9 -7.0)1Q0.9 - 11.3) = 13.7 THC ppmvd @7o/oO2 HCI ppmvd @ 7o/o 02 0.4 ppmvw / (1- 0.188) x ((20.9 - 7.0)l(20.9 - 11.3) = 0.7 HCI ppmvd @ 7o/o 02 NOx lb/hr 197.6 NOx ppm x (1.194*E10^-7) x 11473000 = 270.63 NOx lb/hr SO2lb/hr 0.2 SO2 ppm x (1.66*E10^-7) x 11473000 = 0.40 SO2 lb/hr CO lb/hr 1,021.0 CO ppm x (7.266*E10^-8) x 11473000 = 851.15 CO lb/hr Q*=(C-Q) x C," C,-Co where: Q", = Effluent gas concentration, dry basis, ppm or 0/o C = Average gas concentration indicated by gas analyzer, dry basis, ppm or o/o Q = Average of initial and final system calibration bias check responses for the zero gas, ppm or 0/o C, = Average of initital and final system calibration bias check responses for the upscale calibration gas, ppm or 7o C,a = Actual concentration ofthe upscale calibration gas, ppm or o/o Mostardi Plaft Project No. M2325124 Main Kiln Stack v5.0 27 ot 166 RATA Extractive 41 16120 oMostardi Platt Volumetric Flow Rate Client: Ash Grove Cement Company Plant Leamington Cement Plant Location: Main Kiln Stack Run: Normal Load, Run 1 Date: 06120123 Moisture Content Bws = e' - AP (t-t') P where: e' = saturated vapor pressure of water, in. Hg, at the wet bulb temperature, t' A = 3.67 x 10-4(1+0.00064 (t'-32)) P = absolute pressure/ in. Hg, in the duct t = dry bulb temperature, oF t'= wet bulb temperature,oF Bws = 0.188 Dry Molecular Weight Md=0.44x(o/oCoj + 0.32x(o/ooj + 0.28xoloN2 o/oCO2 = 15.6 o/oO2= 11.3 o/oN2 = 73.1 Md = 30.95 Wet Molecular Weight Ms = Md x (1-Bws) + (18.0 x Bws) Md = 30.95 Bws = 0.188 Ms = 28.51 Average Duct Velocity Vs = 85.49 x Cp x Sqrt AP (avg) x (Ts (avg) + 460/ (Ps x Ms))1/2 Cp = 0.840 Ts (avg) = 206.6 Sqrt AP avg: 0.736 Ps = 24.84 Ms = 28.51 Vs = 51.25 Volumetric Flow Rate Q (Actual Basis)= Vs x A x 60 vs= 51.25 [= 95.030 Q= 292,229 acfm Qs (Standard Basis;= t7.647 x a x Ps 460 + Ts (avg) Q = 292,229 Ps = @ Ts (avg) = 206.6 Qs = 19&170 scfm Qs (Standard Basis)= scfm x 60 min/hr Qs = 11,530,221 sdtr FT-004 MP Pitot Project No. M232512A Main Kiln Stack vl3.1 28 of 166 11t6t2020 OMostardi Platt Mercury Meter Volume at Standard Conditions (Liters) Pbar Vm= Tm= Tm 30.026 517.67 25.436 (ng of Hg /1xl0e) x (0.002046226/Vm(std)*0.0353)"385x1061200.59*1000 15.4 Vm(std) =25.435792 0.073 (total ng of Hg on trap/l000)/Vm(std)/1000 0.605 ug/dscm*(1-Bws) 0.491 B = (ng ofsection 2 / ng ofsection 1) x 100 l= 2.67% Paired Trap Agreement: RD= RD= Test Location: Main Kiln Stack Glient: Plant: Run: Date: Vm(std) = Vm(std) = Hg Concentration: PPb Hg = Total ng Hg = ppb Hg = ug/dscm = ug/dscm = ug/wscm = ug/wscm = % Breakthrough: FT-008 Hg Template Project No. M2325124 Main Kiln Stack Ash Grove Cement Company Leamington Cement Plant 1A 6t2012023 17.647xYxVmx f = 0.996 v5.0 29 of 166 10131117 @Mostardi Platt ontraoa-total of 0.9 % MOSTARDI PLATT Method 30B Determination of Vapor Phase Mercury Nomenclature B = Breakthrough (%). Bws = Moisture content of sample gas as measured by Method 4, percenV1OO. Ca = Concentration of Hg for the sample collection period, for sorbent trap "a" (pg/dscm). Cb = Concentration of Hg for the sample collection period, for sorbent trap "b"(pg/dscm). Cd = Hg concentration, dry basis (pg/dscm). Crec = Concentration of spiked compound measured (pg/m3). Cw = Hg concentration, wet basis (pg/m3). m1 = Mass of Hg measured on sorbent trap section 1 (pg). m2 = Mass of Hg measured on sorbent trap section 2 (pg). mrecovered= Mass of spiked Hg recovered in Analytical Bias or Field Recovery Test (pg). ms = Total mass of Hg measured on spiked trap in Field Recovery Test (pg). mspiked = Mass of Hg spiked in Analytical Bias or Field Recovery Test (pg). mu = Total mass of Hg measured on unspiked trap in Field Recovery Test (pg). R = Percentage of spiked mass recovered (%). RD = Relative deviation between the Hg concentrations from traps "a" and "b" (7o). vs = Volume of gas sampled, spiked trap in Field Recovery Test (dscm). Vt = Total volume of dry gas metered during the collection period (dscm); for the purposes of this method, standard temperature and pressure are defined as 20" C and 760 mm Hg, respectively. vu = Volume of gas sampled, unspiked trap in Field Recovery Test (dscm). CN&F-043 308 Nomenclature Rev. 1.2 1l'U2021 Project No. M232512A Main Kiln Stack 30 of 166 @Mostardi Platt MOSTARDI PLATT Volumetric Air FIow Calculations vm (std) = 17 .647 x vm xl%P-l "' Vw (std) = 0.047LxVlc r Vw (std\ IBws=lffia*n*r"all Md = (0.44xo/oC}) + (0.32 x0/oO2) + [0.28 x (100 -o/oC)z-o/o0)] Ms : Md x (1- Bws) + (18 x Bws) (rs + a60) MsxPs x tlDF x Cp x 85.49 Acfm = 7s x Area(of stack or duct) x 60 Scfm: AcfmxL7.647 t [nufu] mtn Scf h -- Scfm x 60 ttr Dscfm=Scfmx(1-Bws) CN&F-031 Volumetric Flow Calcs Project No. M2325124 Main Kiln Stack Rev. 1.2 1t112021 31 of 166 @Mostardi Platt MOSTARDI PLATT Volumetric Flow Nomenclature A = Cross-sectional area of stack or duct, ft2 Bws = Water vapor in gas stream, proportion by volume Cp = Pitot tube coefficient, dimensionless Md = Dry molecular weight of gas, lb/lb-mole Ms = Molecular weight of gas, wet basis, lb/lb-mole Mw = Molecular weight of water, 18.0 lb/lb-mole Pbar = Barometric pressure at testing site, in. Hg Pg = Static pressure of gas, in. Hg (in. H2O/13.6) DH= Static pressure of gas, in.H2O Ps = Absolute pressure of gas, in. Hg = Pbar + Pg Pstd = Standard absolute pressure, 29.92 in. Hg Acfm = Actual volumetric gas flow rate Scfm= Volumetric gas flow rate, corrected to standard conditions Dscfm = Standard volumetric flow rate, corrected to dry conditions R = ldeal gas constant, 21.85 in. Hg-ft3/'R-lb-mole Ts = Average stack gas temperature, 'F Tm = Average dry gas meter temperature, oF Tstd = Standard absolute temperature, 528"R vs = Gas velocity, fUsec Vm(std)= Volume of gas sampled, corrected to standard conditions, scf Vw(std) = Volume of water vapor in gas sample, corrected to standard conditions, scf Vlc= Volume of liquid collected Y = Dry gas meter calibration factor Ap = Velocity head of gas, in. H2O K1 = 17.647 'R/in. Hg o/oEA = Percent excess air %COz = Percent carbon dioxide by volume, dry basis o/oO2 = Percent oxygen by volume, dry basis %N2 = Percent nitrogen by volume, dry basis 0.264 = Ratio of 02 to N2 in air, v/v 0.28 = Molecular weight of N2 or CO, divided by 100 0.32= Molecularweight of 02 divided by 100 0.44 = Molecular weight of CO2 divided by 100 13.6 = Specific gravity of mercury (Hg) CN&F-024 Nomenclature Pitot Rev. 1.2 1t1t2021 Project No. M2325124 Main Kiln Stack 32 of 166 OMostardi Platt MOSTARDI PLATT Pollutant Concentration CorrectionToh for Percent Orygen 20.9 - 70/o uadj - Ld 20.9 - o/o02 where: C"oi = Pollutant concentration corrected to percent Oz 20.9 -7o/o = Percent Oz, the defined Oz correction value, percent 20.9 = Percent Oz in air o/oO2= Measured Oz concefltration dry basis, percent Co = Pollutant concentration measured, dry basis, ppm. CN&F-007 Correction of Pollutant to %O2 Rev.2.2 1t1t2021 Project No. M2325124 Main Kiln Stack 33 of 166 @Mostardi Platt 1. 2. 3. 4. 5. MOSTARDI PLATT ppmv to lb/hr Conversion Calculations - lbs /SO"ppm 502 x 1.660 x L0-' = +scI lbs SOz scf 60 min lbs SO2 scf min hr hr - lbs/NO-"ppmNOrxl.t94x10-l=#scl lbs NO* scf 60 min lbs NO, scf min hr hr ^ lbs/COppmCO x7.266 x 10-u scf lbs CO scf 60 min lbs CO scf min hr hr - lbsC"H"ppm qHs x 1.742 x 10-/ = --#scI lbs qHs scf 60 min lbs CsHs scf min hr hr - lbs /CH^ppmCHax4.164x10-u = - scl lbs CHa scf 60 mtn lbs CHav_v_scf min hr hr ppmNMHC as C3Hsx9.3427 X 10-8 = lbs C lbsscf 60 min lbs C -v v_scf min hr hr lbs C trf6. CN&F-028 ppmv to lb per hr conv form Project No. M232512A Main Kiln Stack Rev. '1.2 1t1t2021 34 of 166 @Mostardi Platt MOSTARDI PLATT Relative Accuracy Test Audit (RATA) Calculations Mean Difference IL1st4=_) di TL /-t i=1 Standard Deviation ,o=l-"'q;ff|''' Sd l,u - Lo,g75- vn Gonfidence Goefficient Relative Accuracv *=Wx1oo CN&F-029 Part 60 RA Calcs Rev. 1.2 35 of 166 1n/2421 @Mostardi PlattProject No. M2325124 Main Kiln Stack Appendix D - Reference Method Test Data Project No. M232512A Main Kiln Stack 36 of 166 OMostardi Platt NN ,(E =(LTLE<Etso<od= @ lEtr.ECL(! ElEE.u Es=io -(, ll,()6:=I E,t EI E= EEJ P l ootIlt ooo- (f)i.. sf_ ooo- rosfo{ ooo- o)(\lo- ooq @to)o ooo 'riO)N" ooortF- o)-o oo c>_ N(.,o- ooo_ (\t @o_ ooqot-N. ooo- N@o{ s o :, ,9o = s*q @ so)ao) s ro ot slr)ao) soao) s O)ro ot sro c? o) ssf(o ot s @|r) ot sono, @., 6EoE ESo. t- .L \o a?o lt) ci \o ao qo (.o ci c;o qo t,> c.lEO C-ao.a HeF Nri o?o (o <'i c? (') q CO c? (f) q (t, ol c\t (o ai N N i Eoo o IF t- F-c,N l.- ro F- ro t- it l'- ro F. 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N ]l El*-- Fr 66@ o@FN@ rNs@Nots-@Ns9{O@ O O N N F n - F F O ts @ O OO@ N S O @ O O o slrcidN tsN d@ tsFN N N ts o<i ii@@tsN dNE9loit oN EA<qqqqqqqqEBqqqq?Eqq?aEeqEq Sl- - e- t- - -NIot o , d, o oo dFL ii=EEoio:eCcooc EO ;39 Eob o :ENc 5 Ee:8 P}SSSi 5# !.uo=;.:ao6$BE" o-J 6oF (o(o oFri!>UFt N tr) NRx>5 oa7C r ijY,Q oaI O'6E o->G o Glient: Facility: Test Location: Project #: Test Method: Test Engineer: Test Technician: Temp lD: Meter lD: Pitot lD: Pitot Type: Pitot Tube Coefficient: Probe Length: Sample Plane: Port Length: Port Size (diameter): Port Type: Duct Shape: Diameter: Duct Area: Upstream Diameters: Downstream Diameters: Number of Ports Sampled: Number of Points per Port: Total Number of Traverse Points: Operating Level: Moisture Balance lD: Stack Liner Material: Default WAF: Type of WAF Applied: ActualWAF Applied to all runs: Point Markings (including port length): Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack M232512 2 (RArA) TWM BAA F4 F4 4036 S-Type 0.84 8.0 Horizontal 7.00 6.00 FIange Circular 11 95.03 4.100 5.500 4 4 16 Normal FTIR S 0.995 D 0.995 Point # 1 2 3 4 tn. ln. lnches 11.224 20.86 32.608 49.636 ft Sq. Ft. 11t6t2020 @Mostardi Platt FT-004 MP Pitot Project No. M232512A Main Kiln Stack v13.1 48 of 166 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 I Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 1 6t20t2023 7:30 7:59 TWM Test Tech: BM 7 Port Point 11 12 13 14 DP (in. H2O) 0.58 0.63 0.55 0.35 Sqrt. DP 0.7616 0.7937 0.7416 0.5916 Temp ("F) 208.0 209.0 208.0 207.0 Veloclty M 53.12 55.40 51.73 41.23 55.94 53.90 55.32 47.82 Point 1 2 3 4 DP (in. H2O) 0.58 0.55 0.51 0.40 0.63 0.60 0.57 0.42 Sqrt. DP 0.7616 0.7416 0.7141 0.6325 0.7937 0.7746 0.7550 0.6481 292,229 '155,965 192,170 11,530,221 11.472,570 Port 3 3 3 3 Temp Velocity fF) (v) 202.0 52.88 206.0 51.65 207.0 49.77 207.0 44.08 0.65 0.60 0.63 0.47 0.8062 0.7746 0.7937 0.6856 Test Parameters P6", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O Ps - Absolute stack pressure, inches Hg ! - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2325124 Main Kiln Stack 2 2 2 2 1 2 3 4 201.0 205.0 207.0 208.O o/o CO2 15.60 o/o 02 11.30 % Nz 73.10 Md - dry basis lb/lb mole 30.95 Ms - wet basis lbilb mole 28.509 Bws . Moisture content fraction Moisture determined by wb/db? 55.32 54.03 52.66 45.17 't1t6t2020 @Mostardi Platt 4 4 4 4 ,| 2 3 4 207.0 208.0 208.0 207.0 24.88 -0.60 24.84 206.6 Circular 11 95.03 0.5450 0.7356 51.252 0.'t884 N O -ACFM Qsd - DSCFM Os - SCFM Qs - SCFH Qs - WAF adjusted SCFH v13.1 49 of 166 METHOO 2 VOLUMETRIC FLOW DATA Proiect Number: Glient: Facility: Test Location: Pitot lD: Pitot Goefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No,: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 2 6t2012023 8:07 8:36 TWM TestTech: BAA 7 Port Point 11 12 13 14 DP (in. H2O) 0.57 0.59 0.46 0.35 0.61 0.58 0.52 0.44 Sqrt. DP 0.7550 0.7681 o.6782 0.5916 Temp (oF) 207.0 208.0 208.0 203.0 206.0 207.0 207.0 206.0 Veloclty M 52.65 53.60 47.33 41.13 54.42 53.11 50.29 46.22 DP (in. H2O) 0.58 0.55 0.45 0.37 Sqrt. DP 0.7616 0.7416 0.6708 0.6083 0.7937 o.7874 0.7550 0.6928 286,508 151,645 188,356 't't,301,u2 11,244,83s 285,O76 1 2 3 4 0.7810 0.7616 0.7211 0.6633 Test Parameters P6"r - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O P" - Absolute stack pressure, inches Hg L - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M232512A Main Kiln Stack I 2 3 4 4 4 4 4 2 2 2 2 Port Point 31 32 33 34 0.63 0.62 0.57 0.48 Q - ACFM Qsd. DSCFM Qs - SCFM Os - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM Temp Velocity fF) M 205.0 53.03 206.0 51.68 208.0 46.81 207.0 42.42 207.0 208.0 208.0 207.0 55.35 54.95 52.69 48.31 11t6t2020 @Mostardi Platt 24.88 -0.60 24.84 206.8 Circular 11 95.03 0.5231 0.7207 50.249 o/o CO2 15.90 o/o 02 11.70 % Nz 72.40 Md - dry basis lb/lb mole 31.01 Ms - wet basis lb/lb mole 28.476 Bws - Moisture content fraction 0.1949 Moisture determined by wb/db (Y or N) N v13.1 50 of 156 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No,: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 3 6t20t2023 8:43 9:12 TWM TestTech: BAA 7 Port Point 't1 12 13 14 DP (ln. HrO) 0.61 0.58 0.54 0.33 0.57 0.55 0.53 0.43 Sqrt. DP 0.7810 0.7616 0.7348 0.5745 Temp ("F) 208.0 208.0 208.0 203.0 Velocity (v) 54.51 53.15 51.29 39.94 52.58 51.72 50.81 45.70 DP (in. H2O) 0.57 0.54 0.46 0.37 Sqrt. DP 0.7550 0.7348 0.6782 0.6083 0.7681 0.7483 0.6928 0.5916 281,054 148,694 184,736 11,084,133 11,028,713 279,649 2 2 2 2 0.7550 0_7416 0.7280 0.6557 Test Parameters P6", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2325124 Main Kiln Stack 1 2 3 4 4 4 4 4 1 2 3 4 205.0 207.0 208.0 206.0 Port Point 31 32 33 34 0.59 0.56 0.48 0.35 O - ACFM Qsd - DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM Temp Velocity ('F) (v) 208.0 52.69 208.0 51.29 208.0 47.U 207.0 42.42 208.0 208.0 208.0 202.0 53.61 52.23 48.36 41.',t1 11t6t2020 @Mostardi Platt 24.88 -0.60 24.84 206.9 Circular 11 95.03 0.5038 0.7068 49.292 % co2 15.90 Yo Oz 11.60 % Nz 72.50 Md - dry basis lb/lb mole 31.01 Ms - wet basis lbilb mole 28.470 Bws - Moisture content fraction 0,1951 Moisture determined by wb/db (Y or N) N v1 3.1 51 of 166 METHOD 2 VOLUMETRIC FLOW DATA Project Numberz M232512 Operating Level: Normal Client: Ash Grove Cement Company Run No.: 4 Facility: Leamington Cement Plant T6st Dat6: 612012023 Test Location: Main Kiln Stack Start Time: 9:35 Pitot lD: 4036 End Time: 10:04 Pitot Coefficient: 0.840 Test Engineer: TWM Test Tech: BM Probe Length, Feet: 8 Port Length, lnches: 7 DP Sqrt. Temp Velocity DP Sqrt. Temp Velocity Port Point (in. H2O) DP CF) M Port Point (in. H2O) DP fF) M 1 ',t 0.59 0.7681 209.0 53.70 3 I 0.59 0.7681 208.0 53.66 1 2 0.56 0.7483 209.0 52.32 3 2 0.52 0.7211 210.0 50.46 1 3 0.47 0.6856 209.0 47.93 3 3 0.48 0.6928 210.0 48.48 1 4 0.30 0.5477 202.0 38.09 3 4 0.40 0.6325 209.0 44.22 2 1 0.62 0.7874 205.0 54.83 4 1 0.60 0.7746 208.0 54.'t2 2 2 0.56 0.7483 208.0 52.28 4 2 0.52 0.7211 209.0 50.42 2 3 0.52 0.7211 209.0 50.42 4 3 0.50 0.7071 210.0 49.48 2 4 0.37 0.6083 202.0 42.31 4 4 0.35 0.5916 208.0 41.33 Test Parameters Po,, - Barometric pressure, inches Hg 24.88 o/o CO2 15.50 Pn - Stack Pressure, inches of H2O -0.60 o/o 02 11.20 P" - Absolute stack pressure, inches Hg 24.84 % Nz 73.30 t" - Average stack temperature, oF 207.8 Md - dry basis lb/lb mole 30.93 Duct Shape: Circular Ms - wet basis lb/lb mole 28.4'14 Diameter, Feet 11 Bws - Moisture content fraction 0.1945 cross sectional Area of stack, Ft2 95.03 Moisture determined by wb/db (y or N) N Method 2 Resuhs Average DP 0.4969 Q - ACFM 279,399 Average Sqrt DP 0.7015 Qsd - DSCFM 147,720 Average Velocity Vs (fUsec) 49.002 Qs - SCFM 183,389 Os-SCFH 11,003,364 Qs - WAF adjusted SCFH 10,948,348 Q - WAF adjusted ACFM 278p02 FT-004 MP Pitot Project No. M232512A Main Kiln Stack v13.'l 52 of 166 11t6t2020 @Mostardi Plaft METHOD 2 VOLUMETRIC FLOW DATA Proiect Number: Glient: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 5 6t20t2023 10:12 10:41 TWM TestTech: BAA 7 Port Point 11 12 t3 14 1 2 3 4 DP (in. HrO) 0.58 0.60 0.54 0.36 Sqrt. DP 0.7616 0.7746 0.7348 0.6000 Temp cF) 210.0 210.0 210.0 203.O 209.0 209.0 209.0 205.0 Veloclty (v) 53.29 54.20 51.42 41.76 54.16 53.25 52.32 42.97 DP (in. H2O) 0.56 0.60 0.52 0.37 4 4 4 4 2 2 2 2 Port Point 31 32 33 34 1 2 3 4 0.58 0.61 0.59 0.42 Q - ACFM Qsd - DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM Sgrt. DP 0.7483 0.7746 0.7211 0.6083 0.76't6 0.7810 0.7681 0.6481 288,397 152,420 189,225 11,353,482 1',t,296,714 286,955 Temp Velocity fF) (v) 207.0 52.24 208.0 54.12 209.0 50.42 206.0 42.43 208.0 209.0 209.0 208.O 0.60 0.58 0.56 0.38 0.7746 0.76't6 0.7483 0.6164 Test Parameters Pp", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area ofStack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2325124 Main Kiln Stack 24.88 -0.60 24.84 208.1 Circular 11 95.03 0.5281 0.7239 50.s80 o/o CO2 15.50 o/o 02 11.20 o/o N2 73.30 Md - dry basis lb/lb mole 30.93 Ms - wet basis lb/lb mole 28.414 Bws - Moisture content fraction 0'1945 Moisture determined by wb/db (Y or N) N 53.21 54.61 53.70 45.28 1'16t2020 @Mostardi Platt vl3. t 53 of 166 METHOD 2 VOLUMETRIC FLOW DATA Project Number: M232512 Operating Level: Normal Client: Ash Grove Cement Company Run No.: 6 Facility: Leamington Cement Plant Test Date: 612012023 Test Location: Main Kiln Stack Start Time: 10:48 Pitot lD: 4036 End Time: 'l'l:'17 Pitot Coefficient: 0.840 Test Engineer: TWM Test Tech: BAA Probe Length, Feet: 8 Port Length, lnches: 7 DP Sqrt. Temp Velocity DP Sqrt. Temp Vetoclty Port Polnt (in. H2O) OP fF) M porr poinr (in. HrO) Dp ('F) M 1 1 0.60 0.7746 210.0 54.21 3 I 0.59 0.768.t 209.0 53.72 1 2 0.58 0.7616 210.0 53.30 3 2 0.55 0.7416 210.0 51.90 , 3 0.54 0.7348 210.0 51.43 3 3 0.47 0.6856 210.0 47.98 1 4 0.33 0.5745 208.0 40.14 3 4 0.26 0.5099 200.0 35.42 2 1 0.57 0.7550 209.0 52.80 4 I 0.60 0.7746 205.0 54.01 2 2 0.57 0.7550 209.0 52.80 4 2 0.63 0.7937 209.0 55.51 2 3 0.54 0.7348 209.0 51.39 4 3 0.52 0.7211 209.0 50.43 2 4 0.34 0.5831 200.0 40.50 4 4 0.39 0.6245 206.0 43.58 Test Parameters Ps", - Barometric pressure, inches Hg 24.88 o/o CO2 15.50 Pn - Stack Pressure, inches of H2O -0.60 o/o 02 1 1.30 P" - Absolute stack pressure, inches Hg 24.84 % Nz 73.20 t - Average stack temperature, oF 207.7 Md - dry basis lb/lb mole 30.93 Duct Shape: Circular Ms - wet basis lb/lb mole 28.399 Diameter, Feet 11 Bws - Moisture content fraction 0.1959 cross sectional Area of stack, Ft2 95.03 Moisture determined by wb/db (y or N) N Method 2 Results Average DP 0.5050 Q - ACFM 2A1j57 Average Sqrt DP 0.7058 Osd - DSCFM 148,419 Average Velocity Vs (fusec) 49.310 Qs - SCFM 1U,578 Qs - SCFH 'l 1,074,696 Qs - WAF adjusted SCFH I 1 ,019,323 Q - WAF adjusted ACFM 279,752 FT-004 MP Pitot Project No. M232512A Main Kiln Stack v13.1 54 of 166 11t6t2020 @Mostardi Platt METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Temp ("F) 210.0 210.0 2',t0.0 206.0 208.0 209.0 210.0 207.0 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 7 6120t2023 11:38 12:37 TWM TestTech: BAA 7 Port Point 11 12 l3 14 Sqrt. DP 0.7874 0.76'16 0.7000 0.5831 1 2 3 4 0.62 0.58 0.60 0.36 0.7874 0.7616 0.7746 0.6000 Test Parameters P6", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O P, - Absolute stiack pressure, inches Hg L - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2325124 Main Kiln Stack 2 2 2 2 DP (in. H2O) 0.62 0.58 0.49 0.34 Velocity (v) 55.07 53.27 48.96 40.66 54.99 53.23 54.1 8 41.87 DP (in. H2O) 0.57 o.52 0.48 0.27 Port Point 31 32 33 34 0.60 0.55 0.55 0.38 O - ACFM Qsd - DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH O - WAF adjusted ACFM Sqrt. DP 0.7550 0.7211 0.6928 0.5196 0.7746 0.7416 0.7416 0.6164 281,791 149,031 1U,787 11,087,216 1 I ,031,780 280,382 Temp Velocity fF) (v) 208.0 52.73 211.0 50.48 211.0 48.50 200.0 36.07 209.0 210.O 210.0 206.0 24.88 -0.60 24.84 208.4 Circular 1'.! 95.03 0.5069 0.7074 49.421 4 4 4 4 1 2 3 4 o/o CO2 15.50 o/o 02 11.40 % Nz 73.10 Md - dry basis lb/lb mole 30.94 Ms - wet basis lb/lb mole 28.433 Bws . Moisture content fraction 0.1935 Moisture determined by wb/db (Y or N) N 54.14 51.87 51.87 42.95 11t6t2020 @Mostardi Platt v13.1 55 of 166 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 8 6t20t2023 12:'13 12:42 TWM TestTech: BAA 7 Port Point 11 12 13 11 ,| 2 3 4 DP (ln. H2O) 0.60 0.58 0.55 0.43 Sqrt. DP o.7746 0.7616 0.7416 0.6557 Temp ("F) 211.0 211.0 211.0 210.0 209.0 210_O 210.0 202.O Velocity (v) 54.22 53.31 51.92 45.87 55.04 53.73 s',t.40 36.79 Port Point 3l 32 33 34 DP (in. H2O) 0.57 0.51 0.48 0.35 0.60 0.57 0.52 0.38 Sqrt. DP 0.7550 0.7141 0.6928 0.5916 o.7746 0.7550 0.7211 0_6164 283,313 149,728 185,628 11,137,694 11,082,005 281,896 Temp Velocity fF) M 209.0 52.77 209.0 49.92 210.0 48.46 208.0 41.32 0.62 0.s9 0.il 0.28 0.7874 0.7681 o.7348 0.5292 Test Parameters P6u, - Barometric pressure, inches Hg Pn - Stack Pressure, inches of HrO P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fVsec) FT-004 MP Pitot Project No. M232512A Main Kiln Stack I 2 3 4 2 2 2 2 4 4 4 4 207.0 209.0 210.0 208.0 54.06 52.77 50.44 43.06 11t6t2020 @Mostardi Platt 24.88 -0.60 24.84 209.0 Circular 11 95.03 0.5'106 0.7109 49.688 o/o CO2 15.50 o/o 02 11.20 % Nz 73.30 Md - dry basis lb/lb mole 30.93 Ms - wet basis lb/lb mole 28.428 Bws - Moisture content fraction 0.1934 Moisture determined by wb/db (Y or N) N O -ACFM Qsd - DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH O - WAF adjusted ACFM v'13.1 56 of 166 METHOD 2 VOLUMETRTC FLOW DATA Project Number: Client: Facility: Test Location: Pitot !D: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 I Operating Level: Run No.: Test Oate: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 9 6t20t2023 12:5Q 13:19 TWM TestTechl BM 7 Port Point 't1 12 13 14 DP (ln. H2O) 0.61 0.56 0.58 0.39 Sqrt. DP 0.7810 0.7483 0.7616 0.6245 Temp ("F) 210.0 210.O 211.O 211.0 208.0 210.O 211.0 210.O Velocity ry) 54.66 52.37 53.34 43.74 54.13 52.U 52.41 44.26 DP (in. H2O) 0.59 0.56 0.52 0.37 2 2 2 2 1 2 3 4 4 4 4 4 1 2 3 4 Port Point 31 32 33 34 0.63 0.57 0.56 0.36 O - ACFM Osd - DSCFM Os - SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM Sqrt. DP 0.7681 0.7483 0.721',! 0.6083 o.7937 0.7550 o.7483 0.6000 288,511 15't,809 188,770 11,326,197 11,269,566 287,069 Temp Velocity fF) (v) 206.0 53.60 211.0 52.41 211.0 50.50 21't.0 42.60 21',t.0 211.0 211.0 206.0 0.60 0.57 0.56 0.40 0.7746 0.7550 0.7483 0.6325 Test Parameters P6", - Barometric pressure, inches Hg P, - Stack Pressure, inches of H2O P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2325124 Main Kiln Stack 24.88 -0.60 24.84 209.9 Circular 11 95.03 0.5269 0.7230 50.600 o/o CO2 15.50 o/o 02 11.30 % Nz 73.20 Md - dry basis lb/lb mole 30.93 Ms - wet basis lb/lb mole 28.400 Bws - Moisture content fraction 0.1958 Moisture determined by wb/db (Y or N) N 55.59 52.88 52.41 41.87 11t6t2020 @Mostardi Platt v13.1 57 of 166 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M232512 Ash Grove Cement Company Leamington Cem6nt Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 10 6t20t2023 13:40 14:09 TWM TestTech: BAA 7 Port Point 11 12 t3 14 2 2 2 2 DP (in. H2O) 0.61 0.57 0.5'l 0.36 Sqrt. DP 0.7810 0.7550 0.7141 0.6000 Temp fF) 211.O 211.0 211.0 207.0 Velocity M 54.68 52.85 49.99 41.88 55.48 53.77 51.92 43.55 Port Point 31 32 33 34 1 2 3 4 DP (in. H2O) 0.60 0.53 0.54 0.40 0.62 0.59 0.56 0.40 Sqrt. DP 0.7746 o.7280 0.7348 0.6325 0.7874 0.7681 0.7483 0.6325 288,699 152,319 188,981 1 1,338,876 1',t,282,18'l 287,256 Temp Velocity fF) M 209.0 54.14 210.0 50.93 2'.t1.0 51.44 210.0 44.24 0.63 0.59 0.55 0.39 0.7937 0.7681 0.7416 0.6245 Test Parameters Pbar - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O Ps - Absolute stack pressure, inches Hg t - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M232512A Main Kiln Stack 4 4 4 4 1 2 3 4 209.0 211.0 211.0 206.0 210.0 211.O 211.0 205.0 55.08 53.77 52.39 44.08 11t6t2020 @Mostardi Plaft 24.88 -0.60 24.84 209.6 Circular 11 95.03 0.5281 0.7240 50.633 o/o CO2 15.50 o/o 02 11.40 o/o N2 73.10 Md - dry basis lb/lb mole 30.94 Ms - wet basis lb/lb mole 28.426 Bws - Moisture content fraction 0.1940 Moisture determined by wb/db (Y or N) N O - ACFM QSd. DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM v13.1 58 of '166 Test No,Date Start Time End Time Vm (standard L)nq detected DOb uq/dscm ug/w3cm paired trap agrO€mentl o/o difference Breakthrouqh ol 1A 612012023 7:30 8:00 25.436 15_4 0.073 0.605 0.491 2.67 1B 25.47'l 15.7 0.074 0.616 0.500 5.37 Averag6 25.453 15_6 0.073 0.611 0.496 o.90 2A 6t2012023 8:07 8:37 25.310 14.9 0.071 0.589 0.474 2.76 28 25.337 14.2 0.067 0.560 0.451 1.43 Averaqe 25.324 14.6 0.069 0.575 0.463 2.46 3A 6t20t2023 8:43 9:13 25.146 14.6 0.070 0.581 0.467 0.69 3B 25.225 14.2 0.067 0.563 0.453 4.4',1 Averaqe 25.186 14.4 0.069 0.572 0.460 1.55 tlA 6120t2023 9:35 10:05 2s.059 21.0 0.100 0.838 0.675 '1.94 4B 25.',t47 17.8 0.085 0.708 0.570 0.23 Average 25.103 19.4 0.093 0_773 0.623 8.42 5A 6DO12023 10'.'t2 10:42 25.O22 30.2 45 1.207 0 973 1.68 5B 25.056 30.5 0.46 1.217 0.981 1.09 Average 25.039 30.4 0. 45 1.212 0.977 0.43 6A 6t2012023 10:48 11:18 24.935 32.3 0. 55 1.295 't.o42 0.94 6B 24.953 28.8 0.38 1.154 0.928 0.94 Averaqe 24_944 30.6 0. 47 1.225 0.985 5.76 7A 6t20t2023 1 1:38 12:08 24.837 29.8 0.44 1.200 0.968 0.34 7B 24.859 31.2 0.50 1.255 1.012 '1.63 Average 24.848 30.5 0.47 '1.227 0.990 2.25 8A 6t20t20?3 12:13 12:43 24.717 24.6 0.19 0.995 0.803 0.41 8B 24.748 24.8 20 1.002 0.808 0.00 Average 24.732 24.7 0.120 0.999 0.806 0_34 9A 612012023 12:50 13:20 24.656 19.5 0.095 0.791 0.636 1.04 9B 24.685 20.7 0.101 0.839 0.a74 0.49 Averaqe 24.671 20.1 0.098 0.8't5 0.655 2.93 10A 6t20t2023 13:40 14:10 24.626 20.4 0.099 0.828 0.668 2.s',i, 't0B 24.655 21.0 0.102 0.852 0.687 1.45 Averag€24.640 20.7 0.101 0.840 0.677 1.39 FT-008 Hg Template Project No. M2325124 Main Kiln Stack Method 30B (Sorbent Trap) Mercury Test Results Summary Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack v5.0 59 of '166 10131117 @Mostardi Platt Proiect#: M232512 Client: Ash Grove Cement Company Faclllty: Leamlngton Cement Plant Analyzer lD: 1423 METHOD 3OB TEST RESULTS Hs (ns): Meter Temperature (oF): Meter lD: Meter Calibratlon (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): He (ppb): Hg (ug/dscm): Hg (ug/wscm): Location: Main Kiln Stack Condition: Mill On DataTaken By: SMCG 15.4 57.67 MM2A 0.996 0 30.026 25.436 0.073 0.605 0.491 Start Timo: End Time: Pressure, Barometric(Hg"l: Water Vapor lh Flue Gas (Bws): 7:30 8:00 24.950 0.188 Meter Temperature (oF): Metor lD: Meter Callbratlon (Y): lnitial Volume (liters): FinalVolume (liters|: Mote, Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): 15.7 57.67 MM2B 0.997 0 30.037 25.471 0.074 0.616 0.500 rap Start Time: End Time: Pressure, Barometric(H g"): Water Vapor ln Flue Gas (Bws): Hs (ng): Meter Temperalure (oF): Meter lD: Meter Callbratlon (Y): lnitial Volume (liters): FinalVolums (liters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): Hg (ng): 14.2 MeterTemperature(oF): 60.50 Meter lD: MM2B Meter Calibration (Y): 0.997 lnitial Volume (liters): 0 Final Volume (liters): 30.043 Meter Volumo (Standard liters): 25.337 Hs (ppb): 0.067 Hg (ug/dscm): 0.560 Hg (ugArscm): 0-451 8:07 8:37 24.950 0.195 14.9 60.50 MM2A 0.996 0 30.041 25.310 0.071 0.589 0.474 Start Time: End Time: Pressure, Barometric(Hg"): Waler Vapor in Flue Gas (Bws): 8:43 9:'13 24.950 0.195 Hs (ns): Meter Temperature (oF): Meter lD: Meter Callbratlon (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard litersl: Hs (ppb): Hg (ug/dscm): Hg (ug/wscml: 14.6 64.00 MM2A 0.996 0 30.047 25.146 0.070 0.581 0.467 Hg (ns): 14.2 MeterTomperaturo(oF): 63.00 Meter lD: MM2B Meter Callbratlon (Y): 0.997 lnitialVolume(literc): 0 Final Volume (liters): 30.054 Meter Volume (Standard liters): 25.225 Hg (ppb): 0.067 Hg (ug/dscm): 0.563 Hg (ugirscm): 0.453 FT-008 Hg Template Project No. M232512A Main Kiln Stack v5.0 60 of 166 10131117 OMostardi Platt METHOD 3OB TEST RESULTS Project#: M232512 Client: Ash Grove Cement Gompany Facility: Leamington Cement Planl Analyzer lD: 1423 Location: Main Kiln Stack Gondition: Mill On Data Taken By: SMCG Dato: Start Time: End Time: Pressuro, Barometric(Hg"): Water Vapor in Flue Gas (Bws): 4A Trap Hs (ns): Meter Temperature fF): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): 6t20t2023 9:35 10:05 24.950 0.195 21.0 65.50 MM2A 0.996 0 30.029 25.059 0.100 0.838 0.675 oLcl 561 89 17.8 64.50 MM2B 0.997 0 30.046 25.147 0.085 0.708 0.570 25 48 Trap lD: Hg (ng): Meter Temperaturs fF): Metsr lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hg (ppb): Hg (ug/dscm): Hg (ug/wscm): Spikod Trap Run: Splke Concentration: Start Time: End Time: Pressure, Barometric(Hg"): Water Vapor in Flue Gas (Bws): Date: 612012023 10i12 10i42 24.950 0.194 Hs (ng): Meter Temperature fF): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hg (ppb): Hg (ug/dscm): Hg (ug/wscm): 30.2 66.50 MM2A 0.996 0 30.041 25.022 0.145 1.207 0.973 o1c156360 30.5 66.5 MM2B 0.997 0 30.052 25.056 0.'t46 1.217 0.981 25 58 Trap lD: Hg (ng): Meter Temperature fF): Meter lD: Meter Calibration 00: lnitial Volume (liters): Final Volume (liters): M6ter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): Spiked Trap Run: Spike Concentration: Start Time: End Time: Pressure, Barometric(Hg"): Wator Vapor in Flue Gas (Bws): 6A Trap lD: Hs (ng): Met6r Temperature fF): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hg (ppb): Hg (ug/dscm): Hg (ug/wscm): 10:48 11:18 24.950 0.196 o1607149 32.3 68.50 MM2A 0.996 0 30.051 24.935 0.155 1.295 1.042 Trap lD:oLcl 75835 Hg (ng): 2B.a Meter Temporature fF): 68.50 Meter lD: MM2B Meter Calibration (Y): 0.997 lnitialVolume(liters): 0 Final Volume (liters): 30.042 Meter Volume (Standard liters): 24.953 Hg (ppb): 0.138 Hg (ug/dscm): 1.154 Hg (ug/wscm): 0.928 Spiked Trap Run: Y Spike Concentration: 25 FT{08 Hg Template Project No. M2325124 Main Kiln Stack vs.0 61 of 166 10131117 OMostardi Platt METHOD 3OB TEST RESULTS Project#: M232512 Client: Ash Grove Cement Company Facility: Leamington Cement Plant Analyzer lD: 1423 Location: Main Kiln Stack Condition: Mill On Data Taken By: SMCG Start Time: End Time: Pressure, Barometric(Hg'): Water Vapor in Flue Gas (Bws): 7A Trap ID: Hg (ns): Meter Temperature ("F): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Flnal Volume (llters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): 78 Trap tD: Hs (ng): Meter Temperature (oF): Meter lD: Meter Calibration (Y): !nitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): 6t20t2023 1 1:38 12:OB 24.950 0.194 o1C182607 29.8 70.50 MM2A 0.996 0 30.046 24.837 0.144 1.200 0.968 oLc122435 31.2 70.50 MM2B 0.997 0 30.042 24.959 0.150 1.255 1.012 Start Time: End Time: Pressure, Barometric(Hg"): Water Vapor in FIuo Gas (Bws): Hs (ns): Meter Temperature fF): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): Hg (ng): 24.8 Meter Temperature (oF): 73.00 Meter lD: MM2B Meter Calibration (Y): 0.997 lnitial Volume (liters): 0 Final Volume (liters): 30.049 M6ter Volume (Standard llters): 24.748 Hg (ppb): 0.120 Hg (ug/dscm): 1.002 Hg (ug/wscm): 0.808 12:13 12:43 24.950 0.193 24.6 73.00 MM2A 0.996 0 30.041 24.717 0.1 19 0.995 0.803 Start Time: End Time: Pressure, Barometric(Hg"): Water Vapor in Flue Gas (BrYs): Hg (ng): Meter Temperature fF): Meter lD: Meter Calibration 04: lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard Iiters): Hg (ppb): Hg (ug/d3cm): Hg (ug/wscm): 98 Trap lD: Hs (ns): Meter Temperaturo f F): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard literc): Hg (ppb): Hg (ug/dscm): Hg (ug/wscm): '12:50 13:20 24.950 0.196 oL607249 19.5 74.50 MM2A 0.996 0 30.052 24.656 0.095 0.791 0.636 o1607096 20.7 74.50 MM2B 0.997 0 30.057 24.685 0.101 0.839 0.674 FT408 Hg Template Project No. M232512A Main Kiln Stack vs.0 62 of 166 10131117 OMostardi Platt METHOD 3OB TEST RESULTS Project#: t1232512 Client: Ash Grove Cement Company Facility: Leamington Cement Planl Analyzer lD: 1423 Location: lrain Kiln Stack Condition: Mill On Data Taken By: SMcG Date: Start Time: End Time: Pressure, Baromotric(Hg"): Water Vapor in Flue Gas (Bws): Hg (ng): Meter Temperature fF): Meter tD: Meter Galibration (Y): lnltlal Volume (litorc): Final Volume (llters): Meter Volumo (Standard liters): Hg (ppb): Hg (ug/dscm): Hg (ug/wscm): v5.0 63 of 166 6t20t2023 13:40 '14:10 24.950 0.194 20.4 75.00 MM2A 0.996 0 30.043 24.626 0.099 0.828 0.668 oL607247 21.0 75.00 MM28 0.997 0 30.048 24.65s 0.102 0.852 0.687 108 Trap lD: Hg (ns): Meter Temperature fF): Meter lD: Meter Calibration (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard lite6): Hg (ppb): Hg (ug/dscm): Hg (ug/wscm): FT{08 Hg Template Project No. M2325124 Main Kiln Stack 10131117 @Mostardi Platt Appendix E - CEMS and Plant Operating Data Project No. M2325124 Main Kiln Stack 64 of 166 @Mostardi Platt NN Ss -ouo-trELL6 <E KBt- IEI .Eo Eo-Er AcL(E;-EO- cOsl'E(JtrOO E H# EE6E=6 sY Pg -g,fi '*0.==ii ,nEe;E 'no-J o o J L.E co(J Il!oo i -9l! oo(o- N @-o oo N^t\ F- @-o oo @- F*o Or-o ooo- - oo $_t-*N. ooc\l @o,-- oo\f_ (o(9o{ oool @ (f) c\l oo @- 1r)(t e\l ooo_ Noc\t o Eso = O)a @ sod o,rr) ci F-q o, o,q @ (f)F @ o,n @ F-d N6 6 (o @ @ Q)N630rEs o- Fr EL c?o c!o no c?o no -to (o ci ao c?o ao t,>NEO CL -oaL o\ 9E (o q @ oq N oq N N c.j ro c'j t\ c.i (o ci n (f, 6l (t) ils O o, q @ oq co q O)o,o, o; o; c\l O)6) sc NOoi (o d lJ) (o F- (f) (o c.j (f)ri t (f) (f, ai C9 crt c) c.j n cf, € xoz oeo oqo oqo oqo oqo oqo oco oco oqo oqo =Eqo oo ro @o, q rONN oq (o6N a(o @r() (\t ooira $ $(Y)$ o oO(os aoIr* oqt-o)(o \ro O)rO *lOFzdo @dNN o? @(f)N qosN Ir{)N(\t q c!N(\l o @(o(\I (f) o,N(\T F* (oNN qo$N oNN o E i= Ec UJ o) Y?N (o (Y) dd N .t?o *o t*:t-IN N1N o, c.i o,Ito, o .EFt.llo o q? t- t-I @ (f) T @ rr)eo) N o @so @e (o c.,i o Y?N on (f) o (lto (f) NoNoN (o cf)NoNoN (o (r)NoNoN (o (f,NoNoN(o NCNcN (c (f)NoNoN @ (o NoNoN @ (oNoNoN (o (r)NoNoN (o (oNoNoN(o 3e N cf)I rO @ I\@ o)o (ooPrri x>;(o N 66t(?) -SEfr ^U,(E;- L tY EFgao Date/Time CLINKER (TNHR) Expression Value KILN: CO (PPM) Raw Value KILN: CO2 (PCT) Raw Value co_MAss (LBHR) Expression Value law :uGscM) :xpressiOn y'alue (LN: NOX ,PPM) J(pression /alue \ox_MAss :LBHR) lpression y'alue KILN: 02 (PCr) Raw Value )6/20/2023 07:30 1 7.6 1262.8 3.53 1003.2 0.470 200.6 261.8 9.01 )6/20/2023 07:31 1 7.6 1174.7 3.40 929.1 0.560 192.5 250.2 8.92 16/20/2023 07:32 7.2 935.6 3.80 737.6 0.630 200.0 259.1 9.03 )6/20/2023 07:33 t8.2 740.7 3.22 58r'.2 0.680 223,2 289.3 9.00 )G120/2023 07:34 1 7.1 645.4 3.59 507.1 0.620 230.4 297.4 9.10 X612012023 07:35 7.3 948.9 3.8s 747.2 0.550 204.6 2U.7 9.01 )6/20f2023 O7:36 1 7.1 1361.3 4.03 1073.7 0.470 206.0 267.0 8.96 )6/20/2023 O7:37 1 8.5 1309.3 4.08 1027.0 0.420 216.4 278.9 8.85 )6/2012023 07:38 1 8.0 823.2 3.60 641.8 0.500 224.1 287.1 8.99 )6/2012023 O7:39 7.6 584.8 3.24 460 0 0.580 241.5 312.1 8.98 )6/20/2023 07:40 7.7 1008.2 3.39 797.9 0.560 254.6 33'1.0 8.96 )6/20/2023 07:41 1 7.3 1305.3 3.27 1034.1 0.530 258.4 336.4 9.00 )6/2012023 07:42 1 7.3 1288.2 3.40 1026.2 0.490 246.3 322.4 8.99 )6/20/2023 07:43 1 6.9 1 123.9 3.56 897.3 0.470 223.5 293.2 8.93 )6/20/2023 07:44 1 6.1 8s3.6 3.68 673.7 0.540 219.7 284.9 8.88 )6/20/2023 07:45 1 6.4 596.3 3.70 467.2 0.590 231.1 297.5 8.95 )6/20/2023 07:46 1 7.3 565.4 3.19 440.5 0.530 271.6 347.7 9.02 06/20/2023 07:47 1 7.6 M5.0 3.67 s00.9 0.470 279.1 3s6.1 9.08 06120/2023 07:48 1 7.6 1067.7 3.34 838.0 0.470 276.1 356.0 9.16 A6/20/2023 07:49 1 7.4 1597.4 3.59 1269.0 0.500 261.O 340.7 8.90 06/20/2023 07:50 1 7.1 1483 4 4.48 1172.0 0.660 222.2 288.4 8.78 06/20/2023 07151 1 7.7 1048.9 4.08 824.1 0.770 203.3 262.s 8.89 06/20/2023 07:52 1 7.3 312.6 3.98 245.2 0.620 225.2 290.2 9.08 06/20/2023 07:53 1 7.4 508.5 3.50 397 1 0.490 258.3 331.4 905 06/20/2023 07:54 1 7.8 1357.3 4.06 1 061 .1 0.420 239.4 307.5 9.02 06/20/2023 07:55 1 8.4 1542.7 3.63 1204.7 0.380 218.3 280.1 8.8s O6/20/2023 07:56 1 8.1 1121.7 4.29 869.6 0.s60 187.5 238.8 8.96 06/20/2023 07:57 1 8.5 698.4 3.16 542.0 0.700 192.0 2M.B 8.99 06/20/2023 07:58 1 8.2 597.8 3.18 470.2 0.630 228.1 294.8 9.05 )6/20/2023 07:59 I 7.7 1044.3 3.42 824.2 0.550 228.7 296.6 8.99 AVERAGE L1 7.5 985.1 3.53 775.s3 o.547 224.8 295.62 8.98 Project No. M2325124 Main Kiln Stack 66 of 166 @Mostardi Platl 7.0 11.28 10932000.0 7.2 13.0 7.0 11.21 10884000.0 7.2 12.9 7.O 1 1.35 10848000.0 7.3 13.4 7.0 1 1.33 10854000.0 7.3 13.4 7.0 't1.44 10812000.0 7.1 't3.1 7.0 11.32 10836000.0 7.1 12.9 7.O 11.25 10854000.0 7.1 12.8 7.0 1 1.10 10794000.0 7.3 13.0 7.0 1 1.28 1 0728000.0 7.4 13.4 7.0 11.27 10824000.0 7.2 13.0 7.0 11.24 1 0890000.0 7.3 13.2 7.0 1 1.30 10902000.0 7.1 12.9 7.0 11.27 1 0962000.0 7.1 12.8 7.0 11.17 1 0985000.0 7.4 13.3 7.0 11.11 10850000.0 7.4 13.2 7.0 11.26 1 0782000.0 7.2 13.1 7.0 1 1.36 10722000.0 7.3 13.4 7.0 11.43 10686000.0 7.2 13.4 7.0 1't.52 10800000.0 7.2 13.5 7.0 11.15 10932000.0 7.1 12.7 7.0 1 1.00 10872000.0 7.2 12.6 7.0 11 16 10812000.0 7.4 13.3 7.0 11.41 10794000.0 7.2 13.2 7.0 11.40 10746000.0 7.1 13.0 7.0 11.34 10758000.0 7.0 12.8 7.0 1 1.08 10746000.0 7.0 12.5 7.0 11.26 10558000.0 7.2 13.1 7.0 11.25 10580000.0 7.3 13.1 7.0 1 1.35 10824000.0 7.1 13.0 7.0 11.28 10860000.0 7.1 12.9 7.0 1,-.27 10821600.0 7.2 13.1 Project No. M2325124 Main Kiln Stack 67 of 166 @Mostardi Plaft Date/Time :LINKER :TNHR) ixpression y'alue KILN:CO (PPM) Raw Value KILN: CO2 (PCT) Raw Value CO-MASS (LBHR) Expression Value Raw (uGscM) Expression Value KILN: NOX (PPM) Expression Value !ox_MAss ,LBHR) xpression /alue KILN:02 (PCr) Raw Value )6/2012023 O8:O7 117.2 1393.7 3.9s 1088.4 0.620 222.6 28s.6 8.73 )6/20/2023 08:08 116.7 981.2 3.92 760.2 0.620 210.3 267 7 8.80 )6/2012023 08:09 118.2 613 2 3.67 478.1 0.620 228.s 292.7 9.05 )6120/2023 08:10 1 17.0 79s.6 3.02 625.1 0.540 241.6 3'l 1.9 8.97 06/20/2023 08:11 118.4 1343.1 3.01 1059.4 0.480 227.2 294.4 8.95 06/20/2023 O8:12 1 18.9 1574.3 3.25 1241.1 0.500 207.9 269.3 8.90 06/20/2023 08:13 1 18.8 1398.8 3.M 1097.8 0.s30 212.6 274.2 8.98 06/20/2023 08:14 1 19.8 1222.3 3.38 96s.7 0.520 203.2 263.8 8.90 06/20/2023 08:15 119.2 1 31 3.3 3.60 1038.2 0.s20 2149 279.1 844 06/20/2023 08:16 1 18.5 1454.O 3.68 1129.7 0.570 252.7 322.6 7.87 06/20/2023 08:17 1 19.5 1590.9 3.33 1227.1 0.500 270.7 343.1 8.82 06/20/2023 08:18 117.9 1409.3 3.46 1098.7 0.520 2s0.2 320.5 9.22 X6/20/2023 08t19 117.1 1431.4 3.46 1 134.0 o420 234.0 304.6 9.26 16/20/2023 O8:20 117.5 17?2.6 3.07 1370.7 0.320 237.3 31 0.3 9.02 X6/20/2023 08:21 117.0 1622.6 3.1 6 1288.3 0.260 225.2 293.8 8.90 )6/20/2023 08:22 1 18.0 1334.3 3.79 1055.9 0.400 198.6 258.2 8.95 )6/20/2023 08:23 1 18.2 758.9 3.66 603.9 0.520 205.4 268.5 9.03 )6124/2023 08:24 117.9 796.9 3.52 638.6 0.480 228.9 301.4 9.O4 )6/20/2023 08:25 1 17.8 1196.7 3.22 958.0 0.450 230.5 303.2 9.02 )5/2012023 08:?6 1 19.0 1203.2 3.17 964.3 0.530 236.9 311.9 8.96 )6/20/2023 08:27 118.2 101 5.4 13.54 812.0 0.600 228.5 300.2 9.00 )6/20/2023 08:28 118.7 916.5 3.46 725.7 0.620 227.5 296.O 8.9s )6/20/2023 08:29 1 19.0 1 1 16.0 3.02 887.1 o.620 240.6 314.2 9.00 )6120/2023 08:30 1i9.0 1439.0 3.16 1148.2 0.500 246.1 322.6 8.99 06/2012023 08:31 1 18.3 1332.3 3.92 1061.9 0.400 2767 362.4 9.03 06/20/2023 08:32 1 19.6 1235.5 3.43 98s.8 0,410 272.5 357.3 8.96 )6/20/2023 08:33 119.4 1239.0 3.46 9897 0.430 268.0 351.7 8.82 06/20/2023 08:34 119.4 1245.2 3.9s 989.5 0.M0 270.1 352.4 8.76 06/20/2023 08:35 119.8 1014.2 3.72 800.4 0.470 284.3 368.5 8.76 )6/20/2023 08:36 119.1 1056.5 3.79 832.9 0.520 312.8 405.2 8.85 AVERAGE 118.4 L225.6 3.47 968.55 0.501 238.9 310.25 8.90 Project No. M232512A Main Kiln Stack 68 of 166 @Mostardi Platl oz_coRR_7 (PCI) Raw Value )2-DRY :PCT) :XpreSSlOn ,/alue STK-FLOW (scFH) Expression Value KILN: THC (PPM) Ritw .1:,: . Value rHc_coRR :PPM) :xpression /alue 7.0 10.95 0746000.0 7.4 13.0 7.0 11.07 0662000.0 7.4 13.2 7_O 11.41 0728000.0 7.2 13.3 7.0 11.28 081 2000.0 7.2 13.1 7.0 11.22 0854000.0 7.1 12.8 7.0 11.14 0848000.0 7.2 12.8 7.0 11.23 0800000.0 7.2 12.9 7.0 11.1s 0872000.0 7.2 12.8 7.0 10.57 1 0878000.0 8.2 13.9 7.O 9.89 1 0592000.0 89.9 142.5 7.0 13 10514000.0 24.1 43.3 7.0 .62 1 0728000.0 9.7 8.3 7.0 61 1 0902000.0 7.5 4.1 7.0 .27 1 09s0000.0 7.3 3.1 7.0 12 1 0926000.0 7.4 3.1 7.0 20 1 0890000.0 7.5 3.5 7.0 34 1 0950000.0 7.4 3.s 7.0 36 1 1 028000.0 7.1 3.0 7.0 .29 11016000.0 7.2 3.0 7.0 21 1 1028000.0 7.2 2.9 7.0 26 1 1004000.0 7.2 3.0 7.0 21 1 0896000.0 7.3 3.1 7.0 .29 1 0938000.0 7.2 3.0 7.0 26 1 0980000.0 7.3 3.1 7.0 32 1 0968000.0 7.2 3.1 7.0 24 1 0980000.0 7.2 3.0 7.0 .05 1 0992000.0 7.3 2.8 7.0 0.98 1 0925000.0 7.4 3.0 7.0 0.99 1 0860000.0 75 3.2 7.0 12 1 0848000.0 7.3 3.1 7.O tL.2 LOA77200.0 LO.7 18.5 Pro.iect No. M2325124 Main Kiln Stack 69 of 166 @Mostardi Platt Date/Time CLINKER ONHR) Expression Value (lLN: CO :PPM) law y'alue KILN: CO2 (PCr) Raw Value co_MAss (LBHR) Expression Value law :uGscM) !xpression y'alue KILN: NOX (PPM) Expression Value NOX_MASS (LBHR) Expression Value KILN: 02 (PCT) Raw Value )6/20/2023 08:43 7.3 481.8 14.05 382.5 0.590 259.8 338.9 8.90 16/20/2023 08:44 8.2 11 10.8 14.11 883.9 0.490 265.5 347.1 9.05 )6/20/2023 08:45 8.3 131 3.1 3.41 1043.7 o.420 251 8 328.9 9.09 )6/20/2023 08:46 18.0 1073.6 3.47 854.3 0.460 243.9 318.9 8.98 )6/20/202308]r'.7 8.5 948.2 3.75 754.5 0.490 254.7 333.0 8.82 )6/20/2023 O8:48 8.6 693.4 3.93 548.1 0.580 270.6 351.5 892 )6/20/2023 08:49 7.3 806.6 3.36 639.0 0.630 295.2 384.3 8.92 )6/20/2023 08:50 8.9 1420.6 3.6s 1129.2 0.500 291.3 380.4 9.01 )5/20/2023 08:51 8.8 1s83.3 3.44 1257.1 0.400 264.5 345.1 8.91 )6/20/2023 08:52 8.4 1527.1 3.39 1208.5 0.s20 254.3 330.7 8.80 )6/20/2023 08:53 8.5 1527.2 3.38 1202.6 0.610 246.5 31 8.9 8.74 )6/20/2023 08:54 8.0 1342.0 3.76 1062.0 0.530 231 300.s 8.8s )6/20/2023 08:55 8.3 1121.4 3.80 889.4 0.470 2M.3 31 8.4 8.67 06/20/2023 08:56 63.0 9928 414 781.8 0.530 268.1 346.9 8.62 06/20/2023 08:57 59.2 866.7 4.04 680.6 0.580 263.5 340.0 9.00 06/20/2023 08:58 6.9 1264.1 3.46 1008.6 0.490 255.5 335.0 9.05 06/20/2023 08:59 7.5 1993.7 3.04 1593.4 0.430 242.1 317.9 8.97 06/20/2023 09:00 83 1622.1 3.42 1281.6 0.480 222.2 288.4 8.82 06/20/2023 09:01 9.6 1128.4 3.50 892.5 0.530 21't.5 274.9 8.85 06/20/2023 09:02 9.0 1374.3 3.15 1082.8 0.540 210.7 272.8 8.63 06/20/2023 09:03 9.5 1737.7 3.78 1 366.1 0.s60 200.3 258.7 8.M 05/20/2023 09:04 9.1 1857.0 3.90 1476.9 0.540 184.7 241.4 8.47 06/20/2023 09:05 9.5 1657.6 13.61 1324.1 0.s30 184.9 242.7 8.73 06/20/2023 o9:06 20.1 1 307.1 3.60 1043.0 0.550 196.2 257.2 8.68 06/20/2023 09:07 9.0 1320.4 3.76 1 051.3 0.570 202.1 264.4 8.73 )6/20/2023 09:08 9.0 1 63s.1 3.96 1290.4 0.s00 209.2 271.3 8.60 )6120/2023 09:09 8.2 1721.2 3.91 1355.4 0.420 215.7 279.1 880 )6120/2023 09:10 8.4 1 1 99.1 3.70 951.6 0.450 227.4 296.5 8.73 )6/20/2023 09:11 9.3 1078.8 3.71 855.6 0.460 252.6 329.2 8.80 )6/20/2023 09:12 19.4 898.3 3.80 712.1 0.440 279.6 364.2 8.98 AVERAGE L.t4.7 1286.8 3.67 1020.09 0.510 240.0 3L2.57 8.83 Project No. M232512A Main Kiln Stack 70 of 166 @Mostardi Platt )2_CORR_i :PCI {aw r'alue O2-DRY (PCr) Expression Value ;TK-FLOW scFH) :Xpression /alue KILN: THC (PPM) Raw Value THC-CORR (PPM) Expression Value ' 7.0 11.2s 1 0926000.0 7.1 13.0 7.0 1 1.38 1 0950000.0 7.0 12.8 7.0 11.37 1 0938000.0 7.0 12.8 7.0 11.26 1 0950000.0 7.2 13_0 7.0 1 1.04 1 0950000.0 7.3 12.8 7.0 11.21 1 0878000.0 7.2 12.9 7.0 11.20 1 0902000.0 7.1 12.8 7.0 1 1.33 1 0938000.0 6.9 12.6 7.0 1 1.18 1 0926000.0 7.0 12.6 7.0 1 1.05 1 0890000.0 7.0 't2.4 7.0 1 1.00 1 0836000.0 7.O 12.4 7.0 11 14 1 0890000.0 7.2 13.0 7.0 10.91 10914000.0 7.3 12.8 7.0 10.84 1 0836000.0 7.4 12.8 7.0 1 1.33 1 0806000.0 7.1 12.9 7.0 11.39 1 0980000.0 7.0 12.9 7.0 11.27 1 0998000.0 6.8 12.3 7.0 1 1.08 1 0872000.0 7.1 't2.6 7.0 11 14 1 0884000.0 7.O 12.5 7.0 10.89 1 0842000.0 7.2 12.6 7.0 10.90 1 081 8000.0 7.1 12.5 7.0 10.58 10944000.0 7.4 12.6 7.0 11.00 1 0992000.0 7.3 12.9 7.0 10.93 10980000.0 7.2 12.7 7.0 11 00 10955000.0 7.3 12.9 7.0 10.84 1 0860000.0 7.3 12.7 7.0 'l 1.08 1 0836000.0 7.2 12.9 7.0 10.99 10920000.0 7.4 13.0 7.0 11.07 10914000.0 7.2 12.9 7.0 11.34 1 0908000.0 7.1 13.1 7.O 11.1 10907800.0 7.L L2.8 Poect No. M2325124 Main Kiln Stack 71 of 166 @Mostardi Platt Date/Time CLINKER ONHR) Expression Value KILN: CO (PPM) Raw Value KILN: CO2 (PCT) Raw Value co_MAss (LBHR) Expression Value Raw (ucscM) Expression Value KILN: NOX (PPM) Expression Value NOX_MASS (LBHR) Expression Value )6/20/2023 09:35 18.6 167s.1 13.60 1338.1 o.720 261.8 343.6 X6/20/2023 09:36 19.2 16s4.8 13.71 1321.1 0.740 235.6 309.0 J6/2A/2023 09:37 18.6 1568.7 13.39 1252.4 0.760 233.0 30s.5 X6/20/2O23 09:38 19.4 1594.4 1 3.31 1280.5 0.760 228.1 301.0 X6/20/2023 09:39 '18.4 1620.2 '13.84 1305.5 0.770 217.6 288.1 X6/20/2023 09:40 19.0 2306.4 13.70 1859.4 0.770 217.8 288.s J6/2012023 09:41 18.s 2086.0 13.46 't 670.8 0.770 225.4 296.6 J6/20/2023 09:42 19.0 708 5 13.27 1357.3 0.810 236.4 308.6 )6/20/2023 09:43 18.6 362.4 13.15 108s.3 0.840 245.8 321.7 )6DA/2O23O9:M 18.6 453.5 13.O2 1171.2 0.790 241.0 3 19.1 X6/20/2A23 09:45 20.1 858.3 13.08 1528.1 0 730 227.1 306.8 )6/20/2023 09:46 20.0 781.4 12.80 1451.8 0.760 221.2 298.2 )6/20/2023 09:47 19.8 710.5 1 3.10 387.2 0.780 222.4 296.3 )6/20/2023 09:48 19.3 677 9 13.38 3s8 6 0 820 212.7 283.0 )6/20/2023 09:49 18.7 677.8 13.45 362.2 0.860 200.6 267.6 )6/20/2023 09:50 18.6 595.s 13.33 299.5 0.820 202.6 271.1 )6/20/2023 09:51 19.1 369.4 13.26 111.2 0.780 200.9 267.8 )6/20/2023 09:52 18.4 263.2 13.08 022.2 0.840 209.4 278.4 )6/20/2023 09:53 19.0 445.O 13.20 1624 0.890 220.6 291.6 )6120/2023 09:54 18.8 731.6 13.33 399.0 0.800 214.4 284.6 )612O/2023 09:SS 19.2 691.4 13.14 374.7 0 720 214.0 285.8 )6/20/208 A9:56 18.9 461.5 12.94 187.8 0.750 218.6 291.9 06120/2023 09:57 19.4 380.6 13.17 122.7 0.780 220.2 294.2 06120/2023 09:58 18.6 3U.6 13.61 126.5 0.790 228.6 305.5 06/20/208 A9:59 19.4 32s.6 13.57 073.3 0.790 239.0 318.0 06/20/2023 10:00 18.8 377.6 13.M 'l t 1.8 0.800 236.7 31 3.9 06/20/202310:01 19.4 468.7 13.52 184.1 0.810 226.3 299.8 06/20/202310:02 19.7 171.2 13.50 941.2 0.860 225.2 297 3 06/20/202310:03 19.2 1 15.0 13.33 897.5 0.900 238.1 31s 7 06/20/202310:04 19.7 476.3 12.99 1192.8 0.830 239.0 317 3 AVERAGE ,19.1 1566.4 L3.32 L264.87 o.795 225.4 298.89 Project No. M2325124 Main Kiln Stack 72 of 166 @Mostardi Plaft KILN: 02 (PCD Raw Value o2_coRR_7 (PCr) Raw Value O2-DRY (PCr) Expression Value STK-FLOW (scFH) Expression Value (lLN: THC ,PPM) law y'alue tHc_coRR ,PPM) :xpression /alue 8.86 7.0 1 14 1 0992000.0 7.0 2.s 8.83 7.0 1 13 1 0986000.0 7.1 2.7 8.80 7.0 1 10 1 0985000.0 7.2 2.9 9.03 7.0 1 39 1 052000.0 7.O 2.9 8.84 7.0 1 13 1 088000.0 7.3 3.1 8.85 7.O 1 17 1 094000.0 7.1 2.9 8.85 7.0 1 17 1 022000.0 7.O 2.6 8.89 7.0 1 21 1 0932000.0 7.2 31 8.89 7.0 1 ,22 1 0962000.0 7.2 3.1 8.96 7.O 1 .30 1 088000.0 7.1 3.0 9.12 7.0 1 .47 1 316000.0 3.1 9.11 7.0 1 .40 1 292000.0 7.0 2.9 9.00 7.0 1 .26 1 1 60000.0 7.0 2.7 9.10 7.0 1 .43 1 142000 0 7.0 2.9 9.09 7.0 1 41 1 172000.0 7.0 29 9.06 7.0 11.35 1 1 208000.0 7.0 2.8 9.08 7.0 1 .39 1 1 56000.0 AA 2.9 9.08 7.0 1 .41 1 135000.0 6.9 2.7 9.03 7.0 1 35 1 070000.0 7.1 3.0 8.94 an 11.24 1 1 1 18000.0 7.1 2.8 9.07 7.0 1 .39 1 184000.0 7.0 2.9 9.11 7.0 1 42 1 184000.0 7.1 3.0 9.09 7.O 1 .39 1 1 90000.0 6.9 2.6 9.06 7.0 1 37 1 196000.0 7.0 2.8 8.93 7.0 11.22 1 142000.0 7.1 2.8 8.93 7.0 1 .23 1 106000.0 AA 2.6 8.85 7.0 1 16 1 094000.0 7.0 2.6 8.85 7.0 'I 17 1 0s8000.0 70 2.6 8.93 7.0 1 29 1 076000.0 7.0 2.7 9.00 7.0 1 38 ,l 1 18000.0 71 3.1 8.98 7.O L 1.3 11111000.0 7.L 2.8 Project No. M2325124 Main Kiln Stack 73 of 166 @Mostardi Platt )atefime :LINKER :rNHR) :xpression y'alue (lLN: CO :PPM) law r'alue (LN: CO2 :PCT) law y'alue :o_MASS :LBHR) :xpression y'alue law ,uGscM) *pression /alue (LN: NOX :PPM) lpression /alue !ox_MAss ,LBHR) :xpreSsiOn /alue )6120/2023 1O:12 19.4 529.0 3.21 433.6 .080 201.1 271.7 05/20/2023 10:13 19.1 725.4 3.09 594.6 .070 193.6 260.7 06/20/2023 10:,14 19.2 403.0 2.80 328.9 120 205.0 274.9 06/20/2023 10:15 19.2 588.3 3.18 481.2 170 219.4 294.9 06/20/2023 10:16 19.3 758.3 3.04 625.2 160 188.9 255.9 06/20/2023 10:17 18.9 471.9 3.19 386.8 140 199 8 269.1 06/20/2023 10:18 20.3 539.8 3.26 439.0 130 199.5 266.5 06/20/2023 1O:19 18.2 3847 3.71 310.8 110 178.2 236.6 O5/20/2023 10:20 19.1 312 3 3.51 254.5 150 198.3 265.5 06/20/2023 1O:21 18.1 5s3.0 3.15 454.0 190 222.5 300.1 06/20/202310:22 '18.8 312.4 3.M 254.4 170 235.9 315.7 06/20/202310:23 19.0 595.7 2.74 485.0 150 231.9 31 0.8 06/20/?023 '.10:'24 19.2 587.6 3.sB 481.7 .350 199.7 269.0 06/20/202310:25 19.0 417.7 3.86 340.8 550 222.1 297.7 i6/20/202310:26 19.2 382.4 3.M 310.6 470 232.0 309.6 J6/20/202310:27 21.8 369.4 3.70 302.3 .400 219.7 295.4 X6/20/2023 10:28 18.5 525.5 3.38 431.0 .400 220.9 297.7 )6/2012023 10:.29 20.0 583.6 3.86 558.6 .400 250.2 335.9 )6/20/202310:30 19.4 483.4 3.48 394.1 .270 250.3 33s.3 )6/20/20?310:31 19.1 367.1 3.46 299.2 1.140 260.4 348.7 )6/20/2023 10:32 18.0 565.8 3.50 462.1 1.150 258.6 347.0 )6120/2O23 1O:.33 18.4 591 2 3.24 484.1 1.170 238.0 320.2 )6/20/2023 10:34 19.4 471.6 3.3s 385.3 1.200 236.2 317.1 )6/20/2023 1435 '18.5 351.2 13.21 285.6 1.220 253.1 338.2 16/20/2O23 1O:36 188 538.9 13.53 438.2 1 210 258.7 345.6 06/20/202310:37 19.2 714.3 13.41 584.9 '1.200 242.6 326.4 06/20/2023 10:38 19.6 866.5 13.32 711.8 1.370 215.6 291.0 06/20/2023 1O:39 19.7 65s.0 13.51 536.9 1.540 200.s 270.0 A6/20/2023 10:40 '18.9 533.4 13.26 437.5 1.560 215.7 290.7 06/20/2023 10:41 18.9 598.2 12.86 491.9 1.580 228.4 308.6 AVERAGE 19.1 529.2 13.35 432.85 t.267 222.6 298.88 Project No. M232512A Main Kiln Stack 74 of 166 OMostardi Platt (lLN: 02 PCD law /alue )2_CORR_7 PCT) law /alue O2-DRY (PCT) Expression Value STK-FLOW (scFH) Expression Value (lLN: THC :PPM) law y'alue rHc_coRR :PPM) :xpreSsion y'alue 8.96 7.O 1.33 1280000.0 6.9 12.6 9.04 7.0 1.47 1 280000.0 7.1 13.3 9.18 AA 1.59 1232000.0 6.9 13.0 9.08 ai 1.47 1256000.0 6.9 12.8 9.05 7.0 1.40 1346000.0 7.0 12.9 9.03 7.0 1.38 1280000.0 7.1 1 3.1 9.07 7.0 1.44 1 190000.0 7.1 13.2 9.12 7.0 1.47 1118000.0 7.1 1 3.1 9.04 7.O 1.40 1214000.0 7.0 12.9 9.08 7.0 1.47 1 298000.0 7.0 13.0 9.09 7.0 147 1 208000.0 7.1 13.3 9.05 7.0 1.40 1 226000.0 7.2 13.3 9.13 7.O 1.50 1 280000.0 7.0 13.0 9.04 7.0 1.43 1 226000.0 7.2 13.4 9.12 7.0 1.48 1 178000.0 7.1 13.1 9.09 7.O 1.46 1262000.0 7.0 13.0 9.08 7.0 1.45 1286000.0 7.2 13.4 9.07 7.0 1.42 1244000.O 7.1 13.0 9.05 7.0 1.43 1220000.0 7.2 13.4 9.11 7.O 1.50 1214000.0 7.0 13.0 9.17 7.0 1.58 1238000.0 7.1 13.4 8.90 7.O 1 .19 1268000.0 7.4 13.3 9.0s 7.0 1.38 1244000.O 7.2 13.3 9. 16 7.0 1.56 1 190000.0 7.2 13.5 9.25 7.O 1.65 1 190000.0 7.2 137 9.08 t.u 1.42 1268000.0 7.2 13.3 9.07 7.0 1.40 1304000.0 7.3 13.5 9.10 7.0 1.43 1280000.0 7.2 13.2 9.14 ai 1.50 1 1286000.0 7.3 13.6 9.11 7.0 1.49 1316000.0 7.2 13.4 9.08 7.O 1.5 L247400.O 7.L Lt.2 Project No. M2325124 Main Kiln Stack 75 of 166 @Mostardi Platt Date/Time :LINKER JNHR) :xpression /alue (lLN: CO PPM) law /alue KILN: CO2 (PCI Raw Value co_MAss (LBHR) Expression Value law uGscM) upression /alue KILN: NOX (PPM) Expression Value NOX_MASS (LBHR) Expression Value 06/20/202310:48 119.3 s82.1 13.57 476.4 1.410 232.5 312.6 06/20/2023 10:49 1 19.8 509.3 13.39 414.6 1.490 200.4 268.0 06/20/2023 1O:50 119 2 379.2 13.06 307.5 1.460 207.0 275.8 06/20/2023 10:51 1 18.9 294.7 13.66 238.0 1.430 225.2 298.8 )6/20/2023 10:52 1 18.8 457.8 13.81 369.1 1.380 218.7 289.7 X6l2Ol2O23 10:53 118 4 643.6 13.83 522.0 1320 213.0 283.8 )6/20/2023 1O:54 1 19.9 539.3 13.95 439.0 1.260 213.3 285.3 )6/20/2A2310:55 1 18.5 460.1 13.75 374.5 1.210 194.2 2s9.7 )6/20/2023 10:56 1 19.0 396.4 1 3.16 322.5 1.360 182.5 2M.0 )612012O23 10:57 1 19.9 321.0 13.38 261.3 1.5 10 '185.7 248.4 )6/20/2023 10:58 1 19.0 416.4 13.89 339.s 1.510 19s.2 261.5 )6/20/2023 fi:59 119.1 325.9 13.1 5 266.2 1.510 205.1 275.2 )6/20/2023 11:00 119.1 318.1 13.27 257.0 1.560 201.3 267.2 )6/20/2023 11:41 1 19.8 287.8 't3.06 231.4 1.620 219.2 289.6 )5/20/202311:02 1 18.8 326.1 13.32 263.9 1.550 219.1 291.3 )6/20/2023 11:03 120.4 358.4 13.64 291.0 1.480 264.0 352.2 06/20/2023 11:M 119.2 216.0 12.99 175.6 1.520 272.6 364.2 )6/20/2023 '11:05 118.9 157.1 13.55 128.6 1.550 308.8 415.5 X6/20/202311:06 120.0 233.s 13.97 193.0 1.290 334.4 454.2 )6/20/2023 11:07 1 19.8 382.8 13.69 3r3.0 1.010 326.0 437.9 )6/20/202311:08 119.2 419.3 13.28 340.2 1.140 31 s.5 420.8 )6/20/2023 11:09 1 18.8 435.6 13.35 354.6 1.270 321.4 429.9 )6/20/202311:10 1 19.3 397.5 13.37 325.0 1.310 293.2 393.8 )6/20/2023 11:11 120.2 690.3 13.68 560.4 1.350 255.5 340.8 )6/20/2023 11:12 1 19.0 466.8 13.15 3784 1.660 188.9 251.6 )6/20/202311:13 119.2 675.7 13.10 551.5 1.960 212.3 2U.7 06/20/2O23 1'l:14 1 19.5 765.6 12.96 627.9 1.620 217.3 292.8 06/20/?023 11:15 119.8 606.3 13.06 4949 1.280 221.8 297.5 06/20/2023 11:16 1 18.6 525.6 13.70 426.7 1.300 243.0 324.1 06/20/2023 11:17 1 19.1 M5.1 13.45 362.1 310 252.5 337.5 AVERAGE 119.3 434.4 13.44 353.53 t.42L 238.0 318.28 Project No. M232512A Main Kiln Stack 76 of 166 @Mostardi Platt (lLN:02 :PCT) law y'alue l2-coRR_7 ,PCT) law /alue C2-DRY (PCr) Expression Value STK-FLOW (scFH) Expression Value (LN: THC :PPM) law y'alue IHC-CORR (PPM) Expression Value 9.09 7.0 1.44 11262000.0 7.4 3.7 9.1 6 7.0 1.54 1 1202000.0 7.4 3.8 9.05 7.O 1.38 11150000.0 7.3 34 9.10 7.0 1.45 111 12000.0 7.3 3.5 9.06 t.u 1.41 'I 1094000.0 7.3 1.5 9.14 7.O 1.51 1't 160000.0 7.2 3.5 9.12 7.0 I.48 1 1 202000.0 7.2 3.4 9.12 7.0 1.47 1 1 202000.0 7.1 3.1 9.18 7.0 1.57 1 1 1 96000.0 7.3 3.7 9.06 7.0 1.39 1 1 202000.0 7.2 3.3 9.'10 7.0 1.45 1 1 220000.0 7.3 3.5 9.16 7.0 1.55 1 1 238000.0 7.2 3.5 924 7.0 1.65 1 1 1 18000.0 7.1 3.4 9.19 7.0 1.58 1 1064000.0 7.2 3.6 9.12 7.0 1.45 1 1 135000.0 7.3 3.5 9.07 7.O 1.42 1 1 t72000.0 7.3 3.5 9.12 7.0 1 .51 1 1 1 90000.0 74 5.O 9.13 7.0 1.52 1 1268000.0 7.3 3.6 9.26 7.0 1.67 1 1375000.0 7.2 ).t 9.32 7.0 1.74 1 1 250000.0 7.3 4.0 9.34 7.0 1.74 1 1 166000.0 7.2 3.7 9.36 7.0 1.75 1 1202000.0 7.2 1.7 9.08 7.0 1.43 1 1 250000.0 7.2 3.4 8.79 7.0 1.10 1 1 172000.0 7.4 3.2 8.97 7.0 1.33 1 1154000.0 7.4 3.5 908 7.0 1.49 1 1232000.0 7.2 3.4 9.07 7.0 1.45 1 1286000.0 7.2 3.4 9.01 7.0 1.37 1 1232000.0 7.3 3.4 8.97 7.0 1.33 11172000.0 7.4 3.5 9.02 7.0 1.42 1 'l 196000.0 7,4 3.8 9.L2 7.O 11.5 11196200.0 7.3 13.5 Project No. M2325124 Main Kiln Stack 77 ot 166 @Mostardi Platt Date,/Time CLINKER ONHR) Expression Value KILN: CO (PPM) Raw Value KILN: CO2 (PCD Raw Value co_MAss (LBHR) Expression Value Raw (uGscM) Expression Value KILN: NOX (PPM) Expression Value NOX_MASS (LBHR) Expression Value 16/20/202311:38 1 18.8 575.3 13.48 468.1 1.000 252.4 337.4 )6/2012023 11:39 1 19.1 454.7 13.61 369.4 1.000 254.4 339.s 16/2012023 11:40 1 19.3 432.2 1 3.51 349.2 1.020 271.8 350.8 )6/20/202311:41 119.2 508.1 1 3.19 414.1 1.030 261.1 349.6 )6/20/2023 11:42 120.1 626.9 13.76 511.7 1.240 212.6 285.'l )6/2012023 11:43 120.2 526.9 13.89 425.2 1.M0 181 .3 240.9 J6/20/202? 11:44 1 19.3 398.7 13.43 32s.3 1.230 203.0 272.1 )6/20/2023 11:45 1 19.5 477.7 13.15 394.9 ''t.030 189.0 2s6.7 )6/20/202311:46 1 18.8 608.3 '13.09 500.5 1.120 201.8 272.8 )6/20/2023 11:47 1 18.9 721.6 13.24 587.7 1.210 225.0 301.1 )6/20/2023 11:48 119.2 440.2 13.72 358.3 1.250 227.6 304.4 )6/20/2023 11:49 1 19.5 327.8 13.26 268.8 1.300 228.7 308.2 )6/20/2023 11:50 119.1 3s2.2 12.97 288.9 1.180 226.0 304.5 06/20/20?311:51 120.1 270.s 13.33 222.'l '1.070 234.4 316.2 06/20/2023 11:52 119.1 602.4 13.24 494.3 1.170 224.1 302.1 06/20/2023 11:53 1 '19.5 699.3 12.89 571 4 1.280 241.1 323.7 06/20/2023 11:54 'I 19.5 526.9 13.38 430.1 1.1?0 248.1 332.7 06/20/2023 11:55 117 8 363.3 13.26 296.1 0.950 248.8 333.1 06/20/2023 11:56 1 18.8 244.2 13.67 197.6 1.080 254.3 338.1 06/20/2023 11:57 1 18.6 236.9 13.63 19'1.8 1.200 223.2 296.9 06/20/202? 11:58 119.1 390.7 12.81 31 8.6 1.200 195.3 261.6 06/20/2023 11:59 119.1 378.3 13.43 309.4 1.200 209.0 280.9 16/20/202312:00 120.0 642.2 13.46 526.4 1.180 198.0 266,7 J6/20/2023 12:01 120.7 687.5 12.86 5M.8 1.160 202.5 273.3 )6/20/202312:02 119.1 581.8 12.88 476.9 1.160 213.6 287.7 )6/20/202312:03 1 19.0 327.4 13.57 268.4 1.1 50 234.4 315.7 )6120/2023 12:,04 'I 18.5 533.7 1315 437.0 1.050 245.6 330.4 )6120/2023 12:OS 1 19.6 426.9 13.16 347.3 1.050 245.9 328.7 )6/20/202312:06 119.2 31 6.5 13.26 258.1 1.050 263.s 353.0 )6/20/2023 12:07 1 19.5 362.2 13.01 296.3 1.050 262.5 352.8 AVERAGE 119.3 458.0 13.3 382.32 1.139 229.3 307.s5 Project No. M232512A Main Kiln Stack 78 of 156 @Mostardi Platt KILN: 02 (PCT) Raw Value f,2_CORR_7 :PCT law y'alue O2-DRY (PCT} Expression Value ;TK-FLOW :scFH) :xpression y'alue KILN: THC (PPM) Raw Value THC_CORR (PPM) Expression Value 9.26 7.0 .66 1 96000.0 7.3 3.8 9.18 7.0 56 1 78000.0 7.2 3.5 9.16 7.0 56 1 18000.0 7.3 3.7 8.92 7.0 .25 214000.0 7.4 3.4 8.88 7.0 .22 232000.0 7.4 3.5 9.09 7.0 50 1 1 130000.0 74 3.9 9.25 7.0 71 226000.0 7.2 3.8 9.26 7.0 .67 376000.0 7.2 3.7 9.1 5 7.0 .49 1 1 322000.0 7.2 3.3 9.08 7.0 .41 208000.0 7.2 3.2 9.11 7.0 45 202000.0 7.3 3.5 9.10 7.0 .48 285000.0 7.3 3.5 9.20 7.0 59 286000.0 7.3 3.7 9.13 7.0 .49 298000.0 7.5 3.Y 9.18 7.0 56 292000.0 7.2 3.5 9.10 7.0 .43 244000.0 7.3 3.5 9.17 7.O 52 232000.0 7.3 3.6 9.10 7.0 48 214000.0 7.4 3.7 9.04 7.0 1 1.40 136000.0 7.5 3.9 9.04 7.0 .43 142000.0 7.4 3.8 9.05 7.O 45 220000.0 74 3.7 9.11 7.O .49 2s6000.0 7.4 5.t 9.'t4 7.0 52 280000.0 7.4 3.8 9.07 7.0 .45 304000.0 7.4 3.7 9.18 7.0 56 280000.0 7.4 3.8 9.17 7.0 54 280000.0 7.3 3.7 9.11 7.0 .45 268000.0 7.4 3.7 9.10 7.0 .46 1 96000 0 7.5 3.8 9.15 7.0 54 220000 0 7.5 4.1 9.20 7.0 .61 256000.0 7.6 4.4 9.L2 7.O .1.5 I r.235400.0 7.4 L3.7 Project No. M2325124 Main Kiln Stack 79 of '166 @Mostardi Platt )atelTime :LINKER ,rNHR) ixpression y'alue (lLN: CO :PPM) law r'alue (LN: CO2 :PCT) law y'alue co_MAss (LBHR) Expression Value Raw (uGscM) Expression Value (LN: NOX :PPM) ixpression r'alue NOX_MASS (LBHR) Expression Value )6120/202312:13 't 19.0 425.4 13.29 348.7 1.130 212.9 286.7 )5/2012023 12:14 1 18.9 493.5 13.22 405.8 1 140 199.8 270.0 )5/20/2023 12:15 119.2 747.5 12.91 616.0 1.150 198.5 268.9 )6/20/2023 12:16 1 15.6 703.2 13.69 574,9 1.220 199.4 267.8 J6/20/2023 12:17 120.2 525.8 13.62 425.3 1.290 201.2 267.4 )6/24/2023 12:18 119.4 400.1 13.18 323.6 1.160 209.3 278.1 )6/20/202312:19 1 18.9 453.8 13.25 370.6 1.030 219.8 294.9 )6/20/202312:20 119.6 511.4 13.34 419.6 1.040 223.9 301.9 )6/20/202312:21 1 19.8 348.4 13.77 2U.4 1.040 210.9 282.8 )6/20/202312:22 1 19.6 235.4 13.82 191.5 1.120 202.5 270.7 )6/20/202312:23 1 19.6 277.4 13.48 225.5 1.200 210.7 281.4 06/20/2023 12:24 120.3 444.4 13.59 359.2 1 130 211.8 281.3 06/20/2023 12:25 1 19.5 560.5 13.20 453.3 1.070 206.9 275.0 06/20/20?312:26 120.4 584.4 '13.58 473.9 0.990 224.8 299.5 06/20/2023 12:27 1 19.3 402.7 13.55 326.2 0.910 229.6 305.5 06/20/2023 12:28 1 18.9 259.3 13.08 208.9 0.970 229.7 304.1 06/2Q/2023 12:29 1 19.6 290.8 13.32 234.7 1.020 243.7 323.2 )6/201202312:30 1 18.8 456.8 14.07 371.9 1.000 241.4 322.9 J6/20/2023 12:31 119.s 618.2 13.51 509.2 0.980 246.1 333.0 )6/20/202312:32 119 4 599.6 13.07 493.6 0.870 243.8 329.8 )6/20/202312:33 1 19.5 655.4 13.1 5 539.2 0.770 231.2 312.s )6/20/2023 12:34 1 19.5 599.2 13.55 494.6 0.900 2413 331.3 )6/2012023 12:35 1 19.3 409.6 13.27 339.3 1.040 252.7 3M.0 J6/20/202312:36 1 18.8 369.8 12.66 304.1 0.980 276.2 373.2 )6/20/2023 12:37 1 16.0 374.9 13.15 305.7 0.920 273.1 355.9 )61201202312:38 114.3 445.6 13.22 3il.3 0.940 263.5 3s3.9 06/20/202312:39 123.9 590.'r '12.74 4U.0 0.9s0 254.4 342.8 06/20/202312:40 122.9 602.9 13.32 490.5 1.010 207.1 276.9 06/20/2023 12:41 122.9 2M.3 12.89 1 99.1 1.050 217.1 290.7 06/20/2023 12:42 121.5 483.0 13.64 397.2 1.030 215.9 291.7 {VERAGE 119.5 470.4 t3.34 384.49 1.035 226.1 304.26 Project No. M232512A Main Kiln Stack 80 of 166 @Mostardi Platt KILN: 02 (PCr) Raw Value o2_coRR_7 (PCT) Raw Value O2-DRY (PCT) Expression Value STK-FLOW (scFH) Expression Value (lLN: THC PPM) law /alue THC-CORR (PPM) Expression Value 9.13 7.0 1 .49 280000.0 7.4 3.7 9.15 7.0 1 52 316000.0 7.3 3.6 911 7.0 1 ,48 340000.0 7.4 ].7 9.02 7.0 1 .38 2s0000.0 7.2 3.3 9.09 7.0 1 130000.0 7.4 3.7 9.08 7.0 ,l .46 1 1 1 30000.0 7.3 3.5 9.19 7.O 1 58 238000.0 7.2 3.6 9.08 7.0 1 .43 292000.0 7.4 3.7 9.01 7.0 1 36 232000.0 7.3 3.4 8.97 7.0 1 34 1 1 1 96000.0 74 aa 9.09 70 1 .50 r 84000.0 7.3 3.6 9.10 7.0 1 50 124000.0 7.2 3.5 9.10 7.0 1 51 1 30000.0 7.3 3.6 908 7.0 1 .50 1 60000.0 7.3 3.6 9.09 7.0 .49 148000.0 7.3 3.6 9.04 7.0 1 39 088000.0 7.4 3.6 9.09 7.0 1 .45 1 1 1 06000.0 7.2 3.4 9.12 7.O 1 .49 202000.0 7.3 3.6 9.28 7.0 1 .58 334000.0 7.2 3.7 9.1 5 7.0 1 50 328000.0 7.2 3.3 9.03 7.0 1 33 322000.0 7.2 3.1 9.17 7.O 1 54 3s8000.0 7.3 3.7 9.04 7.0 38 400000.0 7.4 3.6 9.26 7.0 1 .64 31 6000.0 7.2 3.7 9.24 7.0 1 .62 220000.0 7.2 3.6 9.27 7.0 1 .63 250000.0 7.2 3.5 9.04 7.0 35 286000.0 7.2 3.1 9.09 7.O 45 196000.0 7.4 3.7 9.06 7.0 .39 214000.0 7.4 3.6 9.14 7.0 1 52 316000.0 7.2 3.5 9.LL 7.O 1.5 1 236200.O 7.3 r3.5 Project No. M2325124 Main Kiln Stack 81 of 166 OMostardi Platt )ate/Time CLINKER GNHR) Expression Value KILN: CO (PPM) Raw Value KILN: CO2 (PCD Raw Value co_MAss (LBHR) Expression Value Raw (uGscM) Expression Value KILN: NOX (PPM) Expression Value NOX-MASS (LBHR) Expression Value 16/20/202312:50 18.s 951 .5 14.40 771.7 1.000 237.1 31 5.9 )6/20/202312:51 18.6 453.2 14.44 366.6 1.140 254.3 337.9 )6/20/2023 12:52 18.9 282.7 13.34 229.3 0.940 270.5 360.4 06/2OD023 12:53 18.0 197.O 13.04 159.9 0.740 287.8 383.9 06/20/2023 12:94 18.7 155.6 13.16 126.8 0.730 283.9 380.1 06/2012023 12:55 17.6 380.3 13.05 311.2 0.720 277.1 372.6 05/20/202312:56 17.9 420.5 1 3.16 341.8 0.720 269.0 3s9.2 )6/20/202312:,57 17.8 651 .9 13.12 s30.1 0.710 251 .8 336.4 06/20/202312:58 18.5 581.9 12.95 478.O 0.810 233.7 31 5.4 )G12012023 12:59 19.3 661.7 r 3.05 543.0 0.900 241.5 325.6 )Gl2O/2023 13:O0 20.3 724.2 13.06 589.5 0.880 237.0 317.0 )6/20/2023 13:01 19.2 538.5 1 3.31 439.1 0.870 234.4 314.O )6/20/202313:02 19.5 678.3 13.43 556.5 0.870 240.7 324.5 )6/20/202313:03 19.6 8946 13.07 732.9 0.880 243.3 327.5 J6/20/202313:M 18.9 i 053.6 13.14 860.4 0.870 228.5 306.6 )6/20/202313:05 18.4 1214.1 13.41 992.0 0.850 224.4 301.3 06/20/202313:06 18.8 827.6 '13.57 675.9 0.930 232.2 31 1.6 06/20/202313:07 19.9 51 9.8 13.54 424.5 1.010 240.1 322.2 06/20/202313:08 19.2 499.5 13.63 410.5 0.910 239.6 323.6 06ftA/202313:09 18.5 724.8 13.s3 593.5 0.820 226.0 304.1 06/20/2023 13:'10 18.s 1096.9 13.29 895.8 0.830 223.4 299.8 06/20/2023 13:11 20.o 1197.3 1 3.31 981.4 0.840 230.6 31 0.6 06/20/2023 13:12 20.5 822.7 13.42 676.2 0.890 230.2 310.9 C6/2A/2023 13:13 18.s 591.3 13.53 485.0 0.950 229.7 309.5 16/20/2023 13:14 19.5 840.5 13.08 686.0 0.9s0 237.4 318.4 J6/20/2023 13:15 18.7 1057.8 13.00 857.4 0.930 224.7 299.3 )G120/2023 13:16 18.8 808.5 13.45 659.2 ''t.000 214.9 287.9 )6/20/2023 13:17 20.0 539.8 13.32 442.2 1.100 215.4 290.0 )6/2O/2023 13:18 199 740.0 13 19 60s.6 't.040 222.3 298.9 )6/2012023 13:19 19.5 829.2 12.93 676.5 0.970 217.2 291.1 AVERAGE 19.0 597.8 13.33 569.95 0.894 240.O 32t.87 Project No. M232512A Main Kiln Stack 82 of 166 @Mostardi Platt KILN: 02 (PCD Raw Value o2_coRR_7 (PCT) Raw Value O2-DRY (PCD Expression Value STK-FLOW (scFH) Expression Value KILN: THC (PPM) Raw Value tHc_coRR :PPM) :xpression y'alue 8.74 7.0 10.94 1 1 60000.0 7.5 3.1 881 7.O 1 1.08 1 1 30000.0 7.5 3.3 8.93 7.0 11 22 1 1 60000.0 7.4 3.4 9.10 7.0 11,46 1 172000.0 7.3 3.5 9.22 AA 1 1.63 1 214000.0 7.4 3.9 9.27 7.0 11.64 1 262000.0 7.3 3.8 9.32 7,0 11.71 'I 184000.0 7.3 3.9 9.23 7.0 11.61 1 190000.0 7.2 3.6 9.23 7.0 11.61 1 304000.0 7.2 3.6 9.20 7.O 1 1.55 1 292000.0 7.2 3.4 9.23 7.0 11.58 1 202000.0 7.2 3.4 9.26 7.0 11.64 1 220000.0 7.1 3.4 9.26 7.0 11.63 1 292000.0 7.1 3.3 9.30 7.0 1 1.69 1 274000.0 7.1 4.4 9.1 0 7.0 11.43 1 238000.0 7.2 3.2 9.1 5 7.0 1 1.50 11244000.0 7.2 3.3 9.11 7.0 11.45 1 238000.0 7.1 3.1 9.20 7.0 11 57 1 238000.0 7.1 3.3 9.33 7.0 11.77 1 310000.0 7.1 ).t 9.32 7.0 11.73 1 268000.0 7.0 3.3 9.23 7.O 1 1.58 1 238000.0 7.0 3.1 9.23 7.O 1 1.58 1 280000.0 6.9 3.0 9.27 7.0 1 1.53 310000.0 7.2 3.5 9.25 7.0 11.60 1 286000.0 7.1 3.3 9.15 7.0 11.46 1 232000.0 7.0 3.0 9.13 7.0 11.46 'I 154000.0 7.1 3.1 9.11 7.0 11.46 1 220000.0 7.2 3.4 9.18 7.0 11.54 1 274000.o 7.2 3.5 9.19 7.0 1 1.54 1 262000.0 7.2 3.4 9.01 7.0 11 31 1 226000.0 7.O 2.8 9.L7 7.O 11.5 11 235800.0 7.2 3.4 Project No. M2325124 Main Kiln Stack 83 of 166 @Mostardi Platt Date/Time CLINKER ONHR) Expression Value KILN: CO (PPM) Raw Value KILN: CO2 (PCI Raw Value co_MAss (LBHR) Expression Value Raw (ucscM) Expression Value (LN: NOX IPPM) :xpression y'alue \ox_MAss :LBHR) ixpression r/alue X6/20/202313:40 17.6 1026.4 3.32 837.3 0.920 202.8 271.8 )6/20/2023 13:41 18.5 736.3 3.55 599.1 0.920 210.2 281.0 )6/2012023 13:42 18.8 768.4 3.99 624.2 0.910 211.9 282.8 )6/20/2023 13:43 19.3 695.5 3.58 568.6 0.900 211.9 2U.6 16/20/2023 13:4 '19.0 417.7 3.49 342.9 0.970 213.1 287.5 )6/20/2023 13:45 18.4 674.0 3.74 550.7 1.040 229.3 307.8 )612012023 13:46 19.2 68s.3 3.s2 558.2 1.030 228.7 3 06.1 )6/20/202313:47 18.4 729.3 3.s2 59s.3 1.000 223.4 299.6 )6/20/2023 13:48 19.2 783.s 3.54 u2.9 1.020 214.4 289.1 )6/2O12023 13:49 18.2 545 7 3.27 448.7 1.040 206.4 278.9 )6/20/2023 13:50 18.0 489.3 3.60 404.7 1.060 210.8 286.s )5/20/202313:51 18.2 583.0 3.77 482.2 1.080 219.7 298.6 )6/20/202313:52 18.9 473.7 2.84 389.s 1.030 229.9 310.6 )6/20/2023 13:53 19.2 u6.7 2.86 528.1 0.970 228.7 306.9 )6/20/202313:54 18.5 647.8 2.89 527.6 0.910 217.9 291.6 )6/?0/2023 13:55 17.9 u1.7 3.12 517.9 0.840 210.7 279.4 06120/2023 13:56 18.4 546.1 3.36 441.7 0.900 216.9 288.2 06/20/2023 13:57 18.3 420.6 3.67 342.8 1.000 237.5 318.0 06/20/2023 13:58 18.4 375.0 3.34 308.0 1.000 245.1 330 8 06/20/202313:59 19.2 397.6 2.85 327.8 1.000 246.8 334.3 06/2012023 M:ao 19.4 532.8 3.03 435.4 0.910 2M.1 327.7 06/20/202314:01 19.2 635.7 2.97 517.5 0.790 221.5 296.3 06/20/202314:02 18.5 573.6 3,25 470.9 0.840 210.7 284.2 o5/20/202314:03 18.4 401.4 3.56 329.4 0.930 217.1 292.7 06/20/2023 14:04 18 5 508.8 3.46 418.2 0.890 217.5 293.7 06/20/202314:05 18.5 661.2 3.s1 545.7 0.820 211.3 286.6 06/20/2023 14:06 18.3 631.5 3.30 522.1 0.810 209.7 2U.8 06/20/2023 14:07 18.5 546.1 3.15 454.1 0.820 221.3 302.3 06/20/2023 14:08 19.0 631.6 3.5 5 527.1 0.830 223.9 307.0 06/20/202314:09 18.s 464.0 3.50 384.0 0.850 210.3 286.0 AVERAGE 18.6 595.7 3.37 488.09 0.934 220.L 296.5L Project No. M2325124 Main Kiln Stack 84 of 166 @Mostardi Platt KILN: 02 (PCr) Raw Value 02_coRR_7 (PCT) Raw Value O2-DRY (PCT Expression Value STK-FLOW (scFH) Expression Value KILN: THC (PPM) Raw Value THC-CORR (PPM) Expression Value 8.90 7.0 1.25 1 226000.0 7.2 3.1 8.97 7.0 1.35 1 '196000.0 7.1 3.1 9.02 7.0 1.42 1 1 78000.0 7.0 3.0 9.07 7.0 1.45 1 2s0000.0 7.2 3.4 9.10 7.0 '1.48 1 298000.0 7.0 3.0 9.22 7.0 1.60 1 24/'000.0 7.0 3.2 9.1 3 7.0 1.49 1 208000.0 71 3.1 9.18 7.0 1.55 1 232000.0 7.0 3.1 9.07 7.0 1.41 1 292000.0 7.2 3.3 9.05 7.0 1.38 1 316000.0 71 3.0 9.04 7.0 1.39 1 382000.0 7.1 3.0 9.22 7.0 1.63 1 382000.0 7.1 3.5 9.1 3 7.0 1.50 1 31 6000.0 7.1 3.2 920 7.0 1.58 1 238000.0 7.0 3.1 9.11 7.0 148 1 208000.0 7.0 3.0 9.15 7.0 1.54 1 106000.0 7.O 3.1 9.17 7.0 1.55 1 130000.0 7.1 3.2 9.24 7.O 1.63 1 214000.0 71 3.3 9.24 7.0 1.62 1 304000.0 7.1 3.3 9.33 7.0 1.73 1 346000.0 an 3.3 9.28 7.0 1.67 1 244000.0 7.0 3.3 9.17 7.O 1.53 1 202000.0 7.0 3.1 9.09 7.0 1.42 298000.0 7.3 3.5 9.13 7.0 1.47 1 292000.0 7.1 3.1 9.19 7.0 1.57 1 310000.0 7.1 3.3 9.15 7.0 1.48 'I 3s8000.0 7.1 f-I 9.27 7.0 1.64 1 376000.0 7.1 3.4 9.22 70 1.56 11442000.0 7.1 3.2 9.13 7.0 1.45 t484000.0 7.1 3.1 9.09 7.0 1.45 388000.0 7.1 3.1 9.14 7.O 1.5 11282000.0 7.L .3.2 Project No. M2325124 Main Kiln Stack 85 of 156 @Mostardi Platt RUN 1 Datefiime lCL_CORR ,PPM) :xpression ,/alue )6/20/2023 07:30 0.0 )6/20/2023 07:31 0.4 )6/20/2023 07:32 01 )6/20/2023 07:33 0.6 )6120/2023 07:34 0.1 )6120/2021 07:35 0.1 )6/20/2023 07:36 0.7 )6/20/2023 07:37 o4 )6/20/2023 07:38 00 )6/20/2023 07:39 0.1 )6/20120z-3 07:40 -0.1 )6/20/2023 07:41 0.0 )6f20/2023 07:42 0.9 )6/2012023 O7:43 0.9 )6120/2023 07:44 0.9 )612012023 07:45 1.2 )512017021 07:46 0.0 \6/20/2023 07:47 0.4 t6/20/2023 07:48 t.5 l6/2Q/2023 07:49 09 16120/2O23 07:5O 0.0 t6/20/2023 07:51 0.1 t6/20/2023 07:52 0.7 t6/2O/2023 07:33 -0 1 )6120/2023 O7:54 0.0 )6aODO23 07:55 0.4 )G12012023 07:56 -0.4 )G12012023 A7:57 o.4 1612012o23 O7:Sa 0.0 )6/2012023 07:59 0.4 \vera9e v1 ax vl in :ount 0.3 'l.3 -0.4 30 RUN 2 )ate/Time rcL_coRR PPM) lpression /alue )6/20/2023 08:07 -0.1 )6/20/2023 08:08 -0.1 )6/2012023 08:09 0.0 )6/20/2023 O8:10 0.1 )6/20/2023 08:11 0.7 )6/20/2023 08:1?0.4 )6/20/?023 08:13 0.0 )6/20t2023 08"14 0.6 )6/20f2023 08:1s 0.5 )6/20/2023 08:.16 0.'l $124/2023 08:17 0.0 t6/20f2023 08:18 0.0 \6/20/2023 08:19 0.0 )6/20/?02308:20 0.1 t6/20/2023 08:21 0.3 t6/20/2023 08:22 0.4 t6/20/2023 08:23 0.4 t6/20/2023 08:.24 1.2 t6/20/2023 08:2s 0.4 t6/201?023 08.'25 0.0 )6/20/2023 08:27 0.0 )6/20/202308:28 0.4 )6/2012023 O8:29 0.4 )6/20/202308:3a 0.0 ,6120/2023 08:,31 0.0 )6/20/2023 08:32 0.0 )6120/202308:33 -0.4 )6/20/202308:34 -0.4 ,6/20/202308:35 0.0 \6/20/2023 08:35 0.6 \verage vlax v1 in :ount 0.2 1.2 -0.a 30 RUN 3 )ate^ime {cL_coRR PPM) :xpression /alue )6120/2023 08:43 -0.1 )6/20/2023 08:44 -0.1 )6/2012023 08:45 0.7 )6/2012023 08:46 0.4 \6n012023 08:47 0.0 )612012023 08:48 0.7 )6/20t2023 08"49 0.6 )6/2012023 08:50 0.7 \6/20/2023 08:51 0.7 16/2012023 08:52 0.7 \6/2012023 08:53 0.'l 16/2012023 08:54 0.6 15/2012023 08:55 0.6 16/2012023 O8:56 -0.1 16/20/2023 08:57 0.7 16/?0/2023 08:58 0.9 t6120/2023 08:59 0.1 )6/20/2023 09:00 0.0 )6/2012023 09:01 0.6 )6/20/2023 09:0?0.4 )6/20/2023 09:03 0.4 )6/20/?0?3 09:M 0.5 )6/20n023 09:05 o.4 )6/20/2023 09:06 o.4 )6/2012023 09:07 0.4 )6/2U2A23 09:08 0.0 16120/2023 09:09 -0.'1 \6120/2023 09:10 0.4 )G120120?3 09:11 0.6 16/20/2023 09:12 o.7 Average Max Min Count 0.4 0.9 -0.1 30 Project No. M232512A Main Kiln Stack 86 of 166 @Mostardi Platt RUN 4 )atelTime {cL_coRR .PPM) xpression lalue t6/2o/2023 09i35 -0.1 t6170/2023 09:36 0.4 t6/20/2023 09:37 0.4 16120/2023 09:38 0.4 t6120/2023 09:39 0.4 t6/20/20?3 09:40 0.4 16120/2023 09:41 0.1 t6lZ0/2023 O9:42 0.4 t6120/2O23 09:43 0.1 16/20/2023 09t44 0.6 16120/2023 09:45 0.4 16/20/?023 09:46 0.0 16/20/20?3 09:47 0.4 16/20/2023 09:48 0.4 t6/20/2023 09:49 0.0 16/20/2023 O9:50 0.1 t6/20/2023 09:51 0.6 t6/2012023 09t52 1.2 16120/2023 09:53 0.7 16/20/2023 09:54 0.0 1612012023 09:55 0.0 t6/20/2023 09i56 0.0 t6/20/2023 09:57 0.0 t6/20/2023 09:58 0.0 t6/20/2021 09:59 0.4 t6t20t2021 10..00 0.4 $l2A/202310:01 0.4 t6t2it2023 10:02 0.1 1612012023 10:03 0.6 16/20/2073 10.04 0.0 wera9e v4 ax vl in :ount 0.3 1.2 -0.1 30 RUN 5 )ate/Time HCL-CORR (PPM) Expression Value )6/20/2023 0:.12 0.9 t6t20t2023 0:13 0.4 \6/20t7023 0:14 1.5 )6/20/2023 0:15 0.0 )6t20t2023 0:16 0.0 )6not2023 O:17 -0.4 )6/20n023 0:18 0.1 )6/2012023 0:19 0.9 t6/20/2023 0:20 -0.4 ,6t20t2023 0'.21 0.1 )6t70/2023 0..22 0.7 ,5t20/2023 0:23 0.4 ,5/24t2023 0.24 0.'t )6t20no23 0:25 0.1 ,5t?o/2023 0:26 0.7 )6t20t2021 0'.27 0.9 )5/20/2023 0:28 0.1 ,6t20/2023 0:29 0.9 )6t20t2023 0:30 0.4 ,6t20/2023 0:31 0.0 16t20t2023 0:32 0.1 )6t20t2023 0:33 0.6 )6t20t2023 0:34 0.9 )6/?0t2073 0:35 0.7 ,6t?o/2023 0:36 0.6 )6/2012023 0:37 0.7 ,6/ZO/?023 0:38 0.6 )6/20t2023 0:39 0.0 )6/?0/2023 0:40 0.0 )6/20/2023 o..41 0.4 Average Max Min Count Q,4 1.5 -0.4 30 RUN 5 Date/Time .{cL_coRR .PPM) /alue x6/20/2023 10'.48 0.0 16/20/20?3 '10i49 0.6 )6/20/2023 10:50 1.2 16/20/2023 10:51 0.1 06/20/2023 10:52 0.4 \6/20/2023 10:53 0.6 )6/2012023 10:54 0.6 16/20/2023 10:.55 0.9 \6/20/2023 10t56 06 16/?012023 10:57 0.4 ,612012023 10t58 0.6 16/20/2023 10:59 0.7 ,6/20/2023 1:00 0.8 t6t20/2023 1:01 -0.4 \6/20/20?3 1:02 0.0 )6t20/20?3 1:03 0.0 )6/2A/7023 1:04 0.1 t6t?0t?02?l:05 -0 1 )6120/2023 1:05 0.0 t6/20/2023 1:07 0.6 )6t20/2023 'l:08 1.5 t6t20t2023 1:09 0.5 t6t20t2023 1:10 0.0 \6/20/2023 l:11 0.4 t6/20t2021 1..12 0.'l \6t20t2023 1:13 0.4 \6/20t2023 l:14 -0.1 )6t20t2023 1:15 0.9 )6/20t2023 li16 0.6 )6/20t2023 1:17 0.4 \verage \,1 ax \,lin :ount 0.4 1.5 -0.4 30 Project No. M2325124 Main Kiln Stack 87 of 166 OMostardi Platt RUN 7 RUN 8 RUN 9 Project No. M2325'l2A Main Kiln Stack 88 of 166 OMostardi Platt RUN 10 Project No. M2325124 Main Kiln Stack 89 of 166 @Mostardi Platt Project No. M232512A Main Kiln Stack Appendix F - Fleld Data Sheets AU0 21 M DIVISION OFAIR QUATITY 90 of 166 @Mostardi Platt Project Number: Client: Test Location: Source Condition: Test Engineer: Test Number StartTime: End Time: Test Tech: '?z/Z f tru /Nl/ 4uf Duct Diamete-r // n Upstream Distufiance, Diamelers ruv !'^FlueArea ffi? t( DilrrnstreaqDisturtance,DiameieflFzu,t SS Port-Length zrr " Portsize-..16o0t'PottTyp;&*r- PitotlD f"rc pitotGmdent(C) O-OztoPwUlE"Hg COz olo _ Wet Sulb Temp _ Leak C]rqpfs P,ss€d@Statc@"H2O Oz% DryBulbTemp _ pre Sfl tnctresH2O P. ?,t/.){ "Hg Meter No. Ft Fluke # Umbiticat lD _ a?.4,4 g.*4 Port- Polnt #AP Temp. OF ',8 Null Polnt Angle, Ilegrees Port- Polnt#AP Temp. OF .IaP Null Polnt Angle, DegrceE D.56 zo7 5 ,-t o.ffi 202 v -7-o.bo 7r)v -?Q.52 706 Z->o..5q tu 7 s"8 zo7 a -.1 n"a.?n7 -<(rc7 z Z-/ *; ?ix Z A-l o.bo %:5hz1e)fi5?3 O.SZL zog I -1 D_{7 2oB 44o..15 207 ,-.1 U.'IZ 7D7 Averaqe A,r.U -iL-h ,44 xOOzi| + .32 x Oz% + .28 x tlz% = _ (lld) Md , _18ws) + (18 x_Bun) = t; 85-49 x coxE-Y Msx _Ps -(Ms) -',,F: sctnx60=_scfi Rev. 1.3 91 of 166 VSx_FluoAEalSQ= 8cftn 17.641 x acfnr Ps =-TsoR DS{01 Method 2 Pltot Sheet Project No. M2325124 Main Kiln Stack 1n*2022 @Mostardi Platt ft/sec(vs) Project Number: Client: Test Location: Source Condition: Test Engineer: 85.49 x DS{01 Method 2 Pitot Sheet Project No. M2325124 Main Kiln Stack VolumeElc Flow Rate Determlna0on Fleld Data Sheet. Strad Time: End Time: Test Tech: Pfl:i;:ry&# H3ik?[#'Ji$,1lT;i:Trtr"#_t Port Lengrth ?.do ' ponsizelfuro I eontwe_@_m,iofrlL-p?ffimoe rt(c) o.frloe-* Z'l.lr!'Hg co".h Jl,stati@a,n:o o,%T "Wl:r#iY"-"'"ffi,ffi* iw;i' kn.& h*-Y- urs,i,carrD .4 x COz% + .32 x Ozgo + .28 x ilz% = _ (l{d) Md '_18nrs) + (18 x_Brs) = _ (Ms) Vsx_FlueAreax60= acfn 17.il7 x acfn' P?=- =_sctrn x60=_sdhTsR Rar. 1.3 92 of 166 1t2tr202. @Mostardi Platl -ru,n Port. Point #AP Temp. OF .tr Null Polnt Angle, Degrees Port. Polnt #AP Temp. OF .laP Null Polnt Angle, Degrcea o.{,722 -7-a.<<zob-r A<t LrlZ-1 o.qa .u'7 ?_-0.L5 zo7'7-O,/all ZoB--I n <-i 7A4-q 2.e{-7 7)t /1 4 7-o-t Average (/sec(vs) Project Number Client: Test Location: Source Conditbn: Test Engineen Date: f ,,' . TestNumber: T Stail Time: 0:36T Duc{ Dameter;L!_! Upstream Disturbanca, Daametem V,(plusArca 'l5a? ff Dorrvnsfeam Disturbance. Olameters7F lortlgqCtl -r.4o' PortSize_/..rp,. 'PortTypeft.*, pttotiO_111 pFotCoemc1errt(C) s.7vop_w4 "Hg co2o/o tL weteubremp - teakclreqli'paEe-@ Static 'Ho Nz% n { q. o./tu pogt,37tncfies H;o P, off;Hg- u[ter NoZ Huke # umbnicat tD _ Volumetrlc Flow Rate Determlnatlon Fleld Data Sheet End Time: Test Tech: .44xCOz% + .32xOz0lo + .28 x Nz% = _ (Md) Md x _18u,s) + (18 x_Burs) =_(Ms) g5.4ex cprm--.,8F: _Vs x _ Flue Area x 60 = 17.647 x -.,pcfin , Ps = Ts oR DS.O01 Method 2 Pltot Sheet Project No. M2325124 Main Kiln Stack ar{rrr scfin x50 =_scfti Rev. 1.3 93 of 166 1n5n0a2 @Mostardi Platt Port- Polnt #AP Temp. "F .@ Null Polnt Angle, Degrees Port- Polnt #AP Temp. "F arE Null Polnt Angle, Degrces ['/06'7 ba 5-/n.18 905-7 o.lfE UR -,7 ll.L)2oh -l '../h ,fr <4.45 zot o.7a 20,-gr'n 3-l 10) Z--/0,L4 2ltt 4-/0. h'zo'1.,D-58 o-,-7 t) /n?-za9 -7 n.57 ton -3 fr.:4 o.,14 206 n '41 Averaoe n/sec(vs) Volumetrlc Flow Rate Determlnaflon Fhld Datahtrzrrz Date:w tVo- t as-4ex cp'ffi" SheetProiect Number: Client: Test Locatbn: Source Conditbn: Ted Engineer _Vsx_FlueAreaxd)= 17.il7 x acfrn, PE =TeoR D9001 MGthod 2 pnot Shcer Project No. M232512A Main Kiln Stack P#,&:Lffif 8,ffi#Htr*#ffi"€ Port Longth _?.oo " port Size/-q_, port fype:&|*_-pi[i6ffi-'-rut%rnasil (cJ ,.lpePy u-ott "Hs cor%J:!- Eaffi'Terp---+ t"ak clre*;pass€d@Sratic'c.r,c ,Hzo g\ -4 Dry Butb rem; - ;f -ifil*o ,roh-# kn^,#- Fr";{= - fi*,3#,*esxio Td Nunbel: Start Time: End Time: TcstTech: .F: .4 x Coz% +,32 x Oz% + .28 x Nz% = _ (ilH) ( lld x_t.Brvs) + (18 x Brc) =_(Ms) scfii x6o =_8dtr Rov. 1.3 94 of 166 1nq20ia2 @Mostardi Platt Poil- Po{nt#AP Temp..F .m Null Polnt Angle, Degroes Port- Polnt#AP Temp..F ./aP Null Polnt Angle, Degrees , \,1 .bt Z t-/fl-rri zoo7uibn€q 7l .?og ffibttl %st-q o.?7)i -q 9/ 'r -l o.5-l zo5 v-/a.t ?)-?ffi -4D -z o{L qA-t 2t*J zf o"./-r{'/, t/'4 zo?a -.1 o.35 202 _Avenge n/sec(vs) Proiect Number: Client: Test locafion: Soure Condition: Telt Engineen Vs x _FlueArca x 60 = '17.47 x ac.fn * PE =Ts'R DS-001 Mrthod 2 Pltd Sh6€t Project No. M2325124 Main Kiln Stack Volumetrlc Flow Rate lletermlnaton Fleld Data Sheet hrr.ftz He: Te$ Number: StartTime: EndTime: TestTech: ft.l cr*u lr*\LH. Nr'-l.r4 1l/ttt Dncl Diameter lt f! Upsteam Etistrbaru, Oiameters 4.t FlueArca r.or ff Dirnsteam Didubanca, Diamaers-lr Pod-Langth :-ro r Portsize-341'pqttywJa*f pitotiD ".ra pT6i6moent(ce) arre 7n?q_,Hg coz% wd6hTemp - r-ear<crpltir@ .4 xCOz% + .32 xOz% + .28 x Nz% = _ (irH) ( ttd x _18wt) + (18 x_.---..;Bws) =_ (il6) Es.49x cp-.@-\l Msx Ps .F: gcfrn x6o =_tcfll Rorr, t.3 95 of 166 1n*202it @Mostardi Platt Port Pold #AP Temp. OF .lAP Null Polnt Angle, Degraeo Poil- Polnt#AP Temp. cF .lAP Null Polnt Angle, Degrceg l'l 0-51 q-oq t-/n-69-t 5b %g -2 7,?ro .Y1 zlb9 -?.a zton3,o Lo2 .J ,l 2o9 z-t \.r;4. I lrr 7InD z l-f tD nf,.-,t-4 Lo? I eoq J?o6L LO - arl D^' 7D1L >g rr 3,?,/fr, Averaqe n/aec(ve) Volumetrlc Flow Rate DetermlnaUon Fleld Data Sheet Projeci Number Client: Teet Location: Source Condition: Test Engineen n'Il{ttt k< co-,- l^*t.+l*k&t {l"h StartTime: End Time: TeetT€ch: Wd BulbTerp q- Fluke # Port Lengffr >.o ," Pod SizeJt&_' portTWelfuHrot iD_rbrta p6i6maent $) e,Aw Dare: //ar'zlt , -, --TcgtNr.rmbcc T lfr'.t?- t0:41 3*a Upotraam Disturbance, Uamaersq,rlt(-tt.\ tlornsfream Disturbance, Dhmeters Xl SS LeakClteq|s Pass6d@ Pr€ 3.cl narrsn.opa,&tnctreg4o UrDllklallD_ Dud Diameter t/ ft Hueeree QfiFif Py ?ta? ,Hg Sfrc:!.(a'WStatic 'Hg P,2l-0!L+tg co2%_ Ne% MeterNo.-.fL Port- Polnt#AP Temp. "F .E Null Polnt Angle, Degreec Port Polnt#AP Temp..F "rffi Null Polnt Angle, Degnes 0.fi UO f-r t.1b fr$zZ AJ-o '.t D '2 W??5U Jt2 -? -,f '4f n rc5 '&It 7-/i)7.r?7 v -/n{9 ?tn.?01 7t)V -,n.b(7D9 -t €-fr,-,a.E7 tu9-9 /,',b5 -T n4z ZAB Average .44xCOz% + .3:l xO2% + .2E x Nz% =_(ilrl) (_ Md x _l€ua) + (18 x_$rvs) = _ (Ms) 8s.4ex cp'mx-rf,IF: -Vsx-FlcArsax60=17.&7 x-iacfin * Ps =-gcfrnx60=-gcfrrTs"R DS{01 lrdlod 2 Ptld Sh.€t Project No. M232512A Main Kiln Stack Rev. 1.3 96 of 166 1n5f2022 @Mostardi Platt Itlscc(vs) Prctject Number: Client: Test Location: Source Condition: Test Engineer: Volumetric Flow Rate Determinatlon Fleld Data Sheet h.t"rf)z Date: L $tq q..t lb-,tVl- nR Start Time: End Time: Test Tech: P.en./ Vatq Duct Dameter ll \ Upstream Disturbance, Diameters -'l(( .r.r* r{,r FlueArea T.g? tr Downstream Disturbance, oiametersEr^ gS [::iffi 'r"'"nsfT"#_ortrvoe;ffi *i''-to"'t_*'Tili3tffi Static "Ho N, % B* eost fltncfres H2o P. LlT"ag' u'"rcr rt Ftuke # UmbiticanD _ Date: b/t/ef Test Numbec ' Q fite Port- Polnt #AP Temp. OF ar6 Null Polnt Angle, Degrees Port- Polnt #AP Temp. oF .@ Null Polnt Angle, Ilegrees t-0.bi ?to 3-/o.57 zoq -Z 0/(c< Ot tt t/7. <5 2t t)-(?t -5 ().({-l 2p r? ?l ?o6 -7 o. z(o ?nD z-l f) <7 2-o1 r-/o.ha zib zJ s*7 7aQ -z O./"b Za7 vtq -,o.qz ?o7.Y o3r loo -Y o.99 26 Averaoe .44 x COzolo + .32 x Oz% + .28 x Nz% = _ (tftt) Md x -l€nr) + (18 x_Brvs) = as.49x cp-.@- Y _Ms x _Ps - (Ms) scfrn x00 =_scfi'l Rev. 1.3 97 of 166 ',,m: Vs x_FlueArea x 60 = affi 17.&47 x acfin , PS = Ts oR D$001 Method 2 Pitot Sheet Project No. M2325124 Main Kiln Stack 1n1nt2:L @Mostardi Platt ft/sec(vs) Proiec't Number Client: Test Locatbn: Source Condition: Test Engineen Volumetslc Flow Rate Determlnatlon Fleld Data Shest . .,fi?lZrtc Date: 0''- " I4A G.a {.htu*L Test Numben ? StartTime: End Time: TestTech: DrHDiameter ll i UpstrreamDisturtance,Diameters -f*f - q,f rue a'rla qlTf ff Dirwnsfiea4-Dishrrbance, oiameLrs$ ii PortLene6h ?-'-i-portsize-.t[-o 'Po1rvw-fi4-PitdtD-fla pr"tco"r6nt(ce) r.atcPvl{-l?l'yg co2yo- weellufemp - l-eakchodkjpasseogStratcrse"l-l2o q% DryBulbTemp _ prc 9,1 tn*l€H;OStalic_'Hg Nz% _ B," pogt 8.9 lncfresl-l2oP.21.r'l +19 lbterNo. F? Fluke# UmU[cailD_ llz38 th{'frt I l2:07T1(/t/tu, Port Polnt#AP Temp. cF .m Null Polnt Angle, Ihgreeo Port Pdnt#AP Temp. OF ar6 Null Polnt Anglq Degrees /s ?**Lto '4-t n5-t 20D -7 u oto r)D.57-2rt -?'lw\irto I l-r lf'{0 I z.t 1 -Y ) l)t/7st{o 4.7.?2oo Z-l 0-o?-k)D / a/il.bo 7D? , n.4^fr,D- s5 ,70 'S lf) /o2 7tD tJ o- 5<7rOn).4(o z0-7 tU 0-56 7r*- Averaoe .4 x COz% + .32 x Oz% + .28 x Nz% = _ (iid) (_ ird x _18ue) + (18 x_Blr) = _ (Ms) as.49x c:p'-@* .l;;-:T MEx _Ps _ Vs x _ Flue Arpa x 60 = acfin 17.647 x acfnr t=P1- =-sclh x6O =-scrhTst OS.001 M€tlod 2 PltotShod Project No. M232512A Main Kiln Stack R6rr. t.3 98 of 166 1nsnox, @Mostardi Platt ttlsec(vs) Proiect Number: Client: Test Location: Source Conditbn: Test Engineel: P. ?itr( "Hg MelerNo'??Fluke # .4 xCOz%+ .32 x Oz% + .26 x Nz% = - (Md) ( iid x -18tt) + ('18 x-Bns) = StartTime: End Time: Test Tech: Umtillcal lD- -(Ms)_.l F : _ilsec(vs) Dud Danrcter lt ft Upstraam Disturbance, Diameters lt!31r"^ {.1- rueRrea gFer ff Do,rrnstream Disturbance, oiamaers:L(+^rr 55 port teng'th-z.r-' Port Size-.gg' PotlTyp-ft+-Pitoll} Stcr7 pitA-Coefriern.(C) 0.1'top*l(.Eyag cozo/o- wetEulbTemp - LeakcjtgxsPassed@ SraUi vca 'rLo o2% Dry Bulb TEmp Pre .lrflnches l-l2O Static 'Hg Nzo6 B* Pwl .fo!.hdns H2O 85.49 x CP x Vsr-FlueAreax60= ecfin 11.&47x acfn, Ps =-scfinx60=-scfii Ts oR DS401 Method 2 Pitot SlPet Project No. M2325124 Main Kiln Stack Rev. 1.3 99 of 166 1n*2022 @Mostardi Platt TI'/' Port- Polnt#AP Temp. "F .aF Null Polnt Angle, Degrces Port- Polnt #AP Temp. OF .IAP Null Polnt Angle, Degreee PI o.@ z((4 0.51 ZU) .?A <f)zr/.?o.6t za? rl 0.55 zlt 'a qu-?-to -4 o h.T 2tt)a 0..r5 2aR /-/U.GZT,=E t0/U-(rO ?t r)lm '7 /t.5-7 Zo9 -l (/,s'4 Zo -?%*#,]o '7 n1b ?ttL -u 2d9 Averaqe Volumeklc Flw Rate Determlnatlon Fleld Data Sheet Proiect Numbcn Client: Tqsl Locatbn: Source Condition: Tet Engineer rtt?,rirz Date: fo/Zo/Zq TestNumber: TStartTime: 1/,:dO EndTime: TTestToch: tfiA t{.t ,.e Pibt Coefidenl (CJ &l{o L€akGheds Passed@ F[,#;mffi UmbilkellD_ Upstream Disturbance, Dlametera j{(l-;11r;. t),ornsream Disturbance, Diameb(fl.on sc'linx60=_8cfri Rcv. 1.3 100 of 166 Duct Diarneter / fl Flue Area x,-tl ff PsA*8 "Hg caz%_W€[ Bulb Terp _ Dry Bulb Temp -q. Fluke # glgtic'0fo "H2O q% Stdic "Hg Nz%P,!j:H_,Hg Meter .44 x COz% + .32 x Oz0lo + .28 x Ne% = _ (ttld) (_ ttld x _l8rm) + (18 x_Bws) =_ (irls) Bs.4sx cp-m--1F: _ Vs x _ Flue Area x 60 - __-_ecfir ik'] 17.847 x acfin , PS = Ts oR DS{01 Mctrcd 2 PltctSlEct Project No. M2325124 Main Kiln Stack tninoin @Mostardi Platt Port- Polnt#AP Temp. OF .laP Null Polnt Angle, Degreeo Port Polnt#AP Temp. OF .fi,P Null Pdnt Angle, Degr€eo lzf Ol t ?op 7-/u51 '?*^ -c m z ,-Z 05d al/ -,2t A, .<z zt( u(l 4,n37 7-Cl Z-/l-lat zwl ?-/46,)n.€" ?// -Z '.92 7ro -/Llt L Z ,-l er.>G 0. ?c z// ) !/o ?).-{,,,,,,.%,.- Averaoe ftlsec(vs) Volumetrlc Flow Rate Determinatlon Fleld Data Sheet Project Number: Clbnt: Test Location: Source Condition: ilurnl End Time: 14:09 Test Engineer. 77ffi TestTech: Vs x _ Flue Area x 60 = 17.647 x acfrnr,,,Ps =-scfrnx60=-scfi1Ts"R Date: l/t,/zt TestNumber: T StartTime: ffi n/Qr/?wHT Duc{ Diamete, lL I Upstream Disturbance, Diameters J&f'rr^r". ut.L FlueArea qtAT-t Dbwnstrsam-Disturbance, Oiarneters&"-. f-9 lortjglglh '?oo t PortSize-jfo 'PortTypeifuaPltdlDtdlL pitoiGmc*ent(Cl tlv. PvZf.V? "Hg Cozo/o - w€{ Bllb Temp - Leak Q!e{s Passed@ stiatic-46 "H2o ozo/o DryBulbremp pre o.8 lnchesl-l2o Static , "Hg Nz o6 8." Posi. q. I lnches H2O P.2/.3'{ "Hg MeterNo._flf Fhke# UmbiticailD_ .44 xCOz% + .32 xOz% + .28 x Nz% = _ (ttld) (- Md , _18ns) + ('18 ,_Bws) = _ (Ms) 85.49* cp-!---.,'zF : -rv'sec(vs) DS-001 Method 2 Pltot Sheet Project No. M2325124 Main Kiln Stack R6v. 1.3 10'l of 166 1nq2022 OMostardi Platt Port- Polnt#AF Temp. OF .ffi Null Point Angle, Degrees Port- Polnt #AP Temp. "F .@ Null Polnt Angle, Degree tlh I Ltl /1 h0 tu9 -1 n_17 ? tl -?4.55 vto.?o.5l ?tl .,n)_ eq 7JtqONazb-)4 o..{o 7o 4-/0-lo-ZffI q-t D.6t /to *,4 zu -7 o.57 .Ztrzl/-t o-SG 1t "t/0.\q zob ry o..{o ,,lr< Average Date: l,-2O- V Source Condition Run Number: prssu,", ZEFF- Notes; Dry Gas Meter No.lUa: Traln A: Traln B: Ds-02 I Eeri?gt ffif ffi ffi1 r'o Main Kiln Stack i:=Ifi liff l-:#:I;j;::""rff ?, ( M ust be l l 5" H s ) Fr,l;::ltrlfff:l;;::," ,,11r (u,ustber is"Hg) testengineer: StacE--r".r y= Dry Gas ttrebr No. Pl l,l ? y = O g 1-l 102 6ts168.1 or{ffilurl Platt Ohio Lumex Co., lnc' Hg Sorbent Trap Chain of Custody Form Trap lD ilililllllililll[lil]l o1647045 QA/QC Signature ffrapAsa,erv)i ,%Z r EI UNSPIKED Production Lot U-1128 Carbon Lot 19 QA/QC Signature tsot l: tr SPIKED AT: Spike Date: SpikeTime: tr High Florr tr FluffyPrefilter El 185mm tr Static Prefilter tr AGS tr 300 mm TypeofTraP: 308 tr 240nun tr 450nm SAMPLING INFORMATION Facility / Source: Boiler lD: Sampling Location: Run Number (OPtional): Sampling Train: eb trB PRE-Run LeakCheck tr PASS Run Start Date/Tims Run End Date/Time: Run Number (optionaD: . " POST.RUNLCAKChECK trPASS tr FAIL I ". _. t.*. " ." O FAIL SAMPLING OONDITIONS AND PARAMETERS Avg. DuctTemP{F"): Avg. Trap TemP (F'): Avg. Flow Rate (cc/min): TotalVolume (L):or (dscm) Estimated Avg. Hg Concentration (Ug/dscm] Event Occuned During Sampling: tr Startup tr Sttutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNTNG TO OHIO LUMEX lfl€:lnatlar.di,rrtin rar{B nf,0c$rbss.d- o*, J.iJi^z ilne lerrl,rsycsi hJoau*irr*4r"i, Phasecotf,act us f}q',"qilss*{trGatintli{dt/6 t'lp' CHAIN OF CUSTODY @bn.is_a maiorcalsc measurerEnt sdb€rlr trap6 and En-srre sampiffi-condfiions prevent misture corld€nsaton mrE Irap rHB' Mq5turswr*.- Mr E e $.fiiriil;tffi'cad vap", roscpim v]i rt'plnger spargi'q certried rcruracv t tolt' TtaceaHe to N|S.r Best Before: June 2025 ,\ 30350 Bruce lrcf,icHElUPheu.V Cleveland, oH 44139 USAwwwCIli8fdrQfrx.com mail@ohiolumex.com lf applldPlacechahof $Jstody seal ttere- (see secrrity seal instnrtion sheet) \rrflfitrlHg'aflgl$::"" Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form uttilriiliililtltultl oL607247 E UNSPIKED D SPIKED AT: Production Lot U-11DA SPike Date: Carbon Lot 4C Spike Time: QA/QC Signature 1sp,rc1: SAMPLING INFORMATION QA/QCSignaturecrnpA:*muy)i (\/ tr High Flow tr Fluffy Pre-filter tr Static Prefilter tr AGS TypeofTrap: 308 El 185 mm tr 240 mm O 3fi) mm tr 450 mm Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: O A SAMPUNG CONDITIONS AND PARAITIETERS @ PRE-Run LeakCheck tr PASS Run Staft Date/Time: Run End Date/Time: POST-RunLeaKCheck trPASS I I tr FAIL tr FAIL Avg. Duct Temp (F'): Avg. Trap Temp (F"): Avg. Flow Rate (cclmin): TotalVolume (L): Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tl Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling:or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAI}.I OF CUSTODY condilions prerent moislurs ctndensatioo in the lrap media. Mol$ure condensation is E mea9uremenl traps and should be nrev€nted Spiking Method Cold Vapor Adso.ption Vra ln{ringer Sparglng Certified Accuracy t 1 0%, Traceable to N IST Best Before: January 2026 30350 Bruce tnffitU$f5'tltBlfll Cleveland, OH i14139 USA',*r.o1t*6RJ,{rQt..o*mail@ohiolumex.cclm ? lf applicable place chain of custody seal here. (see security seal instruction sheet) Seal intact as received: ves E ruo[ \ flEf$t$,ffiffilH. MERCURY SORBENT TRAP FIELD D4TA SHEET Project Namer/Number: 23esi 2 Sampling LocaUon: Dat6: L-)o'a' Source Condition: Ory Gas Moter No. DryGas uebrNo. w\h? v=O,{$F rrap Numberi$Il-Cl _ Spil<e Value ng Nobs: Traln A: Traln B: Pre-TestLeakCheck-Pass @ lb "Hg (MustbeI l5"Hg) Poet-Test Leak Check - Pass @-L6 "Hg Pre-Test Leak Check- Pass O-Tq "Hg (Must be 2 {5"H9) Pct-Test Leak Gheck - Pass @i-}-"Hg Sample Traln A , tet r Voluma ,v-l lthn xat rTomp. (b, .F tetarVacuum, 1{q sbrDeilr6pt ITomP. I'f ____l Stacl Temp. rF g.i D-]tf Eq q zb5 201 q'l ?q.ol?GO ?62 2oLt 8'. r-1 l 6 .6L4 (,O (?f,"1 zo6 9,.a2 lq"o60 bt (7bl ?'c1 n. 7_-I 2,0.o5 r.l 6r s 2(,'0 ?-o t R --1,2 z( ^ o?(L2 5 "-a o ?,OG 9.1"-1 '\o- ott t TdalrAvertge Lo. {205 Sample Traln B ChckTlme ,lhilr t brvolum. ,1,-l lll.B llcbrTemP. (r.) .F XobrVrcuum, 'l{a 5li n-l b 5q 5 8'. l?9.o35 GO S P'- \-1 io.0?-l 60 S l{.," z lB.03tD (6l 5 5tz'l -t-O.6:.1 5 (ol 5 l'. "?LS.O\q tu?5 ':t-1 10. r":i\ TdaUAvenge [oO.( os{pvafl sffi ?ff 36rocnt rrap 105 of '16ftEy. 2.1 @Mostd{lill0Et Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form il|liltfliltilililffilt[ o1607094 E UNSPIKED tr SPIKED AT: Production Lot U-'11D9 Spike Date: Carbon Lot 19-.. -* _.- ._ Spike Time: QA/QC Signature oiur: SAMPLING TNFORMATION QA/QC Signature rrapAsrcntry)r h4 tr Hph Flow tr Fluffu pre-filter tr Static Prefilter tr AGS TypeofTrao: 308 tr 185mm U 240mm tr 300mm tr 450 mm a Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: tr PASS --".-.-"..-- _ I. _ _ "_t. tr FAIL SamplingTrain: ttrA/ trB'\-/ SAMPLING CONDTTTONS AND PARAMETERS POST-RunLeakCheck trPASS tr FAIL Avg. Duct Temp (F'):Estimated Avg. Hg Concentration (Ug/dscm): _ _ Event Occuned During Sampling: tr Startup tr Shutdown CEMENT ONLY: Avg. Trap Temp (F'): Avg. Flow Rate (cclmin):_ _ IotalVolume (L):---. , __.._.. or (dscm) #of RAW MILL OFF events during sampling: REQUIRED IFRETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OFCUSTODY :i:1 1"_ :Tp,'nl:c?ndr,ons pr spmng lvtenod cold vapor AdsoQtbn Via lmpinger Sparghg cenrfied Accuracy r t ore, tncreaote to t tist measureman be treveflted. 106 of 166 www.ohiolumex.com mail@ohiolumex.com @Mostardi Platt O 30350 Bruce lndustrial Phry.V Cleveland, OH 44139 USA lf appllcaUc place ctrain of custody wl here. (see security seal instnrtion sheet) Seal intact as receirred: ves El No fl Sample(s) received by lab \ fffigBffi+HY4ffi"" Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form Trap lD ilililttlilililIililtil o1c182028 til A UNSPIKED Production Lot U-l1DA Carbon Lot 4C QA/QC Signature Fpik ): SAMPLING INFORMATION tr SPIKED AT: Spike Date: Spike Time: QA/QC Si gnatu re Orae asccntry): tr High Flow tr FluffoPre-fitter E 18Smm tr Static Prefilter tr AGS tr 300 nrn TypeofTrap: 308 tr240mm tr 450 mm Facility / Sourcs Boiler lD Sampling Location: Run Number (Optional): Sampling Train. tr A SAMPLING CONDITIONS AND PARAMETERS PRE.Run LeaKCheck tr PASS Run Start Date/Time: Run End Date/Time: POST.RunLeaKChecK EPASS I I D FAIL tr FAIL Avg. Duct Temp (F'): Avg. Trap Temp (F"): Avg. Flow Rate (cc/min): TotalVolume (L):or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CIJSTODY measu,efipnt sorbent traps and Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: 107 of 166 www.ohiolumex.com mail@ohiolumex.com Best Before: January 2026 OMostardi Platt 30350 Bruce lndustrial Pkwy. Cleveland. OH t14139 ti-qAI lf appficable place chain of custo{ seal here. (see security seal instruction sh€eq Seal intact as received: ves El ruo EI ves E ruoE intact as receit/ed: ves EI No El tffia?fr362611toll free Sampling Location: o",". 6-ao_13 Projecl Name/Number MERCURY SORBENT TRAP F DATA SHEETz Run Number: 3 Presrure: zqg-T- TestEngineen Stnccr -r,"prU-rrnU"t@ Sample Traln A Clock Tlmc )/, han* HeterVolumc A/-l llhr lt t tT.mp.(t).c l/htar Vacuum,rl.la Sodcnt fr.pc Temp..c Strck Tcmp .E R: LIT o b7 5 z 6-t zorl RiLIg 5,Ozcl furll 26U 20H 8: 6",I O. A?-1 (^Ll q z@l z orl a : qFt lq ot{I (^Ll s ?(ol 20 t{ (lcq ",0'e frH#Gr.l q z,60 zott:ort 25.66t t^5 -1 zbo 2-O I '.la ?0. ott'l ToleuAvDr.go d"q,U 2.oq Notes: Traln A: Train B: Pre-Test Leak Check - Pass @ l'1 :'Hg (Must be l l6"Hg) Post-Test Leak Gheck - Pass @[(?]'ttg Ds-0r'Uacffi0d. 308310 &$ent Trap Main Kiln Stack DryGasueerNo.M.Fa v=-Qjsl-rrapNrru", OL{r\1J'}5 sp$<evalrr-..pg Samole Train B CbckTimc 2a ho.rr IetprVolune lv-l lll.a t LrTomp. (r.) aF htotVacuum,iUa x'.Lt?o (oZ g, 8'.r{ I b.Dtlla Io>q R. ('!ro.os I bi 5 r:sR.1s350 ba Eqi0".2r. ot{?(o3,5q:oP L9_o 3 I (ort q q'-ta sC).o SLI TotauAvertgo G),o Pre-Test Leak Check - Pass @ I Q "Hg (Must be 2 t5"Hg) Poet-Test Leak Check - Pass @-l-b-"Hg 108 of 1Bv.2.1 @Mostfft292lt Onr UMEX Ohio Lumex Co., !nc. Hg Sorbent Trap Chain of Custody Form B UNSPIKED tr SPIKH) AT: Production Lot U-11DA SPike Date: Carbon Lot 4C SPikeTime: QA/QC Signature (spit et: SAMPLTNG INFORMATION QA/QC Signature ffoe Arsnt]v): tr High Flow tr FluffY Prefilter tr Static Prefilter tl AGS TypeofTrap: 308 mmruillfiIiilfttuttttu o1c181888 E 185mm tr3fi)mm tr 240mm D 450mm Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: - tr PASS _t I tr FAIL SamplingTrain: F Avg. Duct TemP (F ): Avg.Trap Ternp (F ): Avg. Flow Rate (cc/min): TotalVolume (L): trB POST-RunLeakCheck trPASS T] FAIL SAMPLING CONDITIONS AND PARAMETERS Estimated Avg. Hg Concentration (pg/dscm): Event Occuned During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling:or (dscm) REQUIRH' IF RETURNI}S TO OHIO LUMEX Estimated Hg Mass in Section 1 of SorbentTrap (ng): -.-'-.--'iloteAn4arce5rd,r"rgErdbesetb.scda, rr&,oL'&iirg t* 0rl{,tnsyrallhod{r{ffii.a.rrdr Ressmttd'8tr}q',uqi?<*r'-tc!Gsli?ulil9rnbEtr CHAIN OF CUSTODY rEa$refirent Stfiill;fril";ilUil*fi6iio.,ni rmpit'serspatsl"ecertified accurrvt loeLrraceablcto Nlsr Best Before: January 2026 30350 Bruce r rffi #Ufl P?tnry' Cleveland, OH 44139 USA ***.t9?i8[,.1&%,..o, mail@ohiolumex.com ? lf ryficaUe Place chain of custoryseal hre. (see security seal instruction sheet) . Proiect No. M232512At , rAif,40e6Gffioo office*' 1 888 87Gzo1l tollfree ilffiililrilf,fulurln oL647LO4 QA/QC Signature firapAss$pry)l ,/ffi f QA/QC Signature cpir"l: tr Hiqh Flo/', tr Fluffo Prefilter El 185 mm tr 240 mm tr Static Pre-filter tr AGS tr 300 mm E 450 mm TypeofTrap: 30B SAMPLING INFORMATION Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form E UNSPIKED Production Lot U--11?B_ " Carbon Lot 4C tr SPIKED AT: Spike Date: Spike Time: Facility / Source: Boiler lD: Sampling Location: Run Number(Optional): Sampling Train: tr A SAMPLING CONDITIONS @ PRE-Run Leak Check Run Start Date/Time: Run End Date/Timq Run Number (optionat): POST-Run Leak Check tr PASS tr PASS tr FAIL tr FAIL AND PARAMETERS Avg. Duct Temp (F'):Estimated Avg. Hg Concentration (pg/dscm): Avg. Trap Temp (F'): Avg. Flow Rate (cclmin): Total Volume (L): Event Occuned During Sampling: O Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling:or (dscm) REQUIRED IF RETURNING TO OHIO LUMEI( Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CT,,STODV moisture condercation ln the lrap rnedia Moisture condensatbn is a rEuor cause measure{nent Spiking Method Cold vapor Adsorption via lmpingEr Sparglog Cfiifled AcairBey r 10*. Traceable to NIST Best Before: June 2025 30350 Bruce t n&lUffikriltB{dl Cleveland, OH it4139 USA **r.dt1&RJ,1&.com mail@ohiolumex.com I lf apdcaUe place chain of custody seal here. (see security seal instruction sheet) Courier/Other (if applicable) S€al intact as received: ves E NoE Seal intact as received: ves E r.ro I \ fr'tr$ilnB,l€ffifi1h" Projecl Name/Number MERCURY SORBENT TRAP FIELD DATA SHEET Run Number: t{ Source Gondition: DryGasMeterNo. l1n?- Train A: Train B: De02 1 0{61€e0 fl $ffin$effi r rnp Main Kiln Stack PrdTest Leak Check - Pass @ I (o "Hg (Must be 2 l6',Hg) Post-Test Leak Check - Pass @j=G_-"Hg Pre-Test Leak Check- Pass @ | b "Hg (Must be l 15,,Hg) Poet-Test Leak Check - Pasr @-I-b "Hg Notes: Sample Traln A Glock Tlme 2ilhout iloter Votum. lV-l lllnn Heter T.mp.(t) .F ilebr Vrcuunq 'tI^ SorDant TrlPa T.mp. .F Stack Tcmp. .Fq'.B5 o b5 5 Z(oO "-o sq:qo 5. Oqt b*t;zb0 2oqq.'Ll5 t0. o50 (.5 5 ?r0 2 65q:so l< bql L(^s "lo C 20Lq:.((,zo,o q\G s L60 ?-o Glo:oo ZE-ot{q Gb 9 '?-t Q '?ab lo"05 3O. o29 TotaUAverege br-t ZoS.S DrvcastutebrNo.tlhl- v-!"!8L-Topr.rurr"r OLclS{o181 spkevar,e 25 ng Samole Traln B CbctTlme 2{ hour llctar Volume lV-l lllna t brTemp. (t.).t lLoarYacuun\ 'llort 135 o 6r 5 :Ll o 5.o3-r (or{sq:q 5 lo,oz?(rLl :.qo I 5, O3q ^5 gqigs "o.oLtG G9 5 ,d:,0A zs_o s2 u5 5 lo: Dq 30, otlG To,teUAvrltge b'1.5 111 oRC852.l oMsftmflflatt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form iltttilliliifiif,rlttlr oL6072L0 E 185 mm tr 240 mm tr300mm tr 450mm B UNSPIKED tr SPIKED AT: Production Lot U-t 1DA Spike Date: Carbon Lot 4C Spike Time: QA/QC Signature 1sp*e1: SAT'PLING INFORMATION QA/QC Signature flropAc*rbry)i A./ tr High Flow O Fluffoprefitta O Static Prefilter tr AGS TypeofTrap: 308 Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: h PRE-Run LeakCheck tr PASS Run Staft Date/Time: Run End Date/Time: tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutd;;; CEMENT ONLY: # of RAW MILL OFF events during sampling: I I P0ST-RunLeakCheck trPASS tr FAIL s_lMl! NG cO N-D-|_T! ONS AN D PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cclmin): TotalVolume (L):or (dscm) REQUNEI) IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section I of Sorbent Trap (ng): CHAIN OFCUSTODY prevent moishre meas!rafEnt in $rbent lraps andspking Melhod cold vapor Adsorption via lmpinger sparging certiried Acc1mcy r lot, Traceable to Nlsr Best Before: January 2026 trB \1BtmeA6get{X}?fir&t r Ua8'tSe 9tsf[ totl free www.ohldfuftllfi$om mail@ohiolumex.com lf appllcable place chain of custody seal here- (see security seal instnrction sheet) O 3o3so Bruce tndu$flftltffiatt? Cleveland, OH 44139 USA Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form mruffiffifiilifirrm 8 UNSPIKED Production Lot -U-1 1-28- Carbon Lot 4C QA/QC Signature &*o): SAMPLING INFORMATION tr SPIKED AT: Spike Date: Spike Time: oL649725 QA/QC Signatu re (rrap Aoarmpty)i 4M( tr High Flow tr Flufff Pre-filter E 185 mm tr 240 mm tr Static Prefilter tr AGS tr 3(D mm El 450 mm Type of Trap: -3,0I Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: tr A SAMPLING CONDITIONS AND PARAMETERS PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: " Run Number (optionat): POST-Run Leak Check T] PASS tr PASS I I tr FAIL tr FAIL Avg. Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cc/min): TotalVolume (L): Estimated Avg. Hg Concentration (U0/dsc1! Event Occured During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling:or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OFCUSTODY prerrent h the rap media. Md$ure coftlensathn ls a major caus€measuement in sooent traps drd $rorJld be D.e1€oted. Best Before: June 2025 Spiking Nlethod Cold Vapor Adsorplbn Via rnpinOer SparghO C€rtified Accuracy r t 01. Traceabh b N|ST 113of166 www.ohiolumex.com mail@ohiolumex.com OMostardi Platt 30350 Bruce lndustrial Pkwy. Cleveland, OH 44139 USAI lf aptcaHe place chain of custody seal here. (see security seal instruction sheet) \ I,Hfr{i$ft1ffY#;. MERCURY SORBENT TRAP DATA SHEET Projeci Name/Numben Sampling Location: Run Numbel: Source Condition: Preesure: 2{, TestEngineer: SF[d(+DryGas*nt*o' ilapnumue,: oLroo DrvGasiiirebrNo.nh? v= 0-QQJ rr+Nrro"r@spikcvabe 2B ng Traln A: Traln B: Ds{21 }fGlbod n0PltEQcEm rrap Main Kiln Stack Sample TralnE Clock Tlnr. ?.1lratt llcbrVohm ru-l llhr IclarTamp.(t) }F frterVrcuun,riad lO: t2 6 (ob sl0:ll 5.06S bG 5l0:zz l0.0Ar2 blo s 10"> r l5.o.q8 G-l s lo:12 zo.o5 0 b s r0"31 zs_oq I b'Sio:rl?.a0.o 52 Tot UAvengo bb,5 Notes: Pre-Test Leak Check-- pass @15_..Hg (llust be I i5,,Hg)Post-Test Leak Check - pass-@-Tg 'ni Pre-Test Leak Check_- pass eEui ffiust be I tE,,Hg)Post-Test Leak Check - easc-@ T6-Hg ' 114 {d0.Q.1 orvlffEfilfratt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form ilffiulmnffilmlt oL647L47 A UNSPIKED Production Lot: Carbon Lot 4C tr SPIKED AT: U-1128 Spike Date: Spike Time: eA/ec Signature nrapAsmny)i A# ( tr High Flow tr FluffY Prefilter tr Static Pre-filter tr AGS Type of Trap: 3-0_p . . E 185mm tr 240mm tr 300 mm El 450 mm QA/QC Signature ppn.l: SAMPLING INFORMATION Facility / Source: Boiler lD: Sampling Location: PRE-Run Leak Check Run Start Date/Time: Run End Date/Time: Run Number (optionat): POST-Run Leak Check tr PASS tr FAIL I I _" tr FAIL Run Number (OPtional): i Sampling Train: €) SAMPLING CONDITTONS AND PARAMETERS OB tr PASS Avg. Duct Temp (F ): Avg. Trap Temp (F"): Avg. Flow Rate (cc/min): TotalVolume (L):or (dscm) _ Estimated Avs. Hg c"i.:"ggps/dscm): Event Occuned During Sampling: tr Staftup tr Shutdown CEMENT ONLY: #of RAW MILL OFF events during sampling: REQUTRED rF REIUINlN9_T9_oltlo_l9Ig _ " EstimatedHgMassinSection1ofSorbentTrap(ng):...,.;'-* ilotsAns4zcror6,eir raF rilb.r.t06rGd- uxr *i.iJi,g u,'s ud*m.yrBut'l otofs6ratbnssin*r plcsaco*act rsifrqrltqi".$rirtte cstiml'v lh's |6t€' CHATN OF CUST(DY rEasuremefil taps Best Before: June 2025 'r*.11t8[J'$Er..o,mail@ohiolumex.com 30350 Bruce I n9UkFfl#Rta$' Cleveland, OH 44139 USAI tf adit$e Place chain of custodY seal here. (see security seal instruction sheet) Seal intact as received: ves E ruo El - Proiect No. M232512A\ . 1AilA0r3€G3F00 office-' 1888 B7o26t7 toll free Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form tr UNSPIKED Production Lot 9_1F6_7 Carbon Lot 4C QA/QC Signature 6p,r*1: SAMPLING INFORMANON A SHKED AT: 25ns_ _ spike Date: 6t23t2022 Spike Time: 0922 \1 --- ililtiluiilffiffm!il o1c155189 QA/QC Signature firap rsranprg: 0 High Flow u Fluffy Prefitter E 185 mm tr Stath Pre-filter D AGS tr 300 mm Type of Trap' 99.q_ _ tr 240 mm O 450mm Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: tr A SAMPLING CONDITIONS AND PARAMETERS PRE-Run LeakCheck U PASS Run Start Date/Time: Run End Date/Time: Run Number (opto."D: POST-RunLeakCheck trPASS "t I E FAIL tr FAIL Avg. Duct Temp (F ): Avg. Trap Temp (F"): Avg. Flow Rate (cclmin): Totalvolume (L):or (dscm) REQUIRE} IF REIURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CUSTODY sampling cofilitiofis preve.t fixisture cmdensatam ln the rap meda. Mc,isture condensation is a measurernenl in sorb€nt traps Spikino Method Cold Vapor Adsorptbfl Vh lmpinoer Sparging Certified Accuracy t 'l Ot. Tra]Ebte to N|ST Estimated Avg. Hg Con_centration (pg/dscm): Event Occrned During Sampling: tr Startup tr Strutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: ,r**.otli6r${rffiP.com mail@ohiolumex.com Best Before: June 2A25 30350 Bruce r nu &IhtlT*rfilBtt Cleveland, OH 44139 USAI lf applicable place chain of custody selhere. (see security seal instnrction sheet) Seal intact as received: ves E HoEf \ . re+re.r6t0.lgeg5lf,**' rNhlB6ho93oh tor free MERCURY SORBENT TRAP FIELD DATA SHEET Sampting Location: I.rl f Sied Projed Name/Number Date: 0 -rO-1 Run NunDer: 6 Pressure: 2{.q S Dry Gas Meter No. Sample Traln A Clock Tlmc 2llhout lllsterVolume lV-l lftrn Ueter Tcmp. (h) .F iietcrVacuum, 'lla Sorbant Tttp. Tcmp.l:St ckTemp. .F lo: rt R o G8 s z(0,t 20t I O'.53 6.031 (og 5 21|*^6 ?-o (oloisSlo,or{?(^g ,?(ah 2o(,.ll:oq t5,oq5 bq 5 ?-(.(\zoltlio8,zo,os-l bq 5 zbo 2-o1 '. lr 26-1\rrt{b\9 ".60 ?-0-7 '.1 *30.()51 TdaUAverage (aa.q ZOtc,g Notes: Pre-Test Leak Check - Pass @ ,'Hg (Must be I l5"Hg) Post-Test Leak Check - Pass DryGasueerxo.!1ltt'l y=qqf7 rrapr,rumuer OLc t]S&3S spikevarue 25 ng Sample Train B Cloct Tlmc 2ll hour Uet rvolumr lV-l llhn inlCf lamp. (t-) .F karYacurm,rfan lo:q8 0 t.o8i 5 I a'^ (n g -0t{ (.68 s Ir\'-(R lo.o|.lq 6*sll'.o3 l S.oLto bq s I l'. o8 -LO,OLI 1o (oq 5 ll". r 3 2-5.03 t (,q (. ll'.lg ?o,oH 2 TotallAvcnge (oq.t> Train A: Traln B: Ds-021il6&Fhe#l*hft!hF0t rrap Main Kiln Stack Pre-Test Leak Gheck- Pass @ lJ "Hg (Must be l i6"Hg) Post-Test Leak Check - Pass ql5 'Xg 1'17 oRH!62.1 oM?rbt6[fratt il||tiluililil]fiiltil]t A UNSPIKED Production Lot _V:11 D9-* Carbon Lot 4C QA/QC Signature tsp*cl: SAMPLING INFORMATION tr SPIKED AT: . Spike Date: Spike Time: Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form 01607152 QA/QC Signature FrapA*sc'nbry)i -,CSo1. tr High Flow tr Fluffy Pr*filter E 185 mm tr 240 mm tr Static Pr*filter tr AGS tr 300 mm tr 4S0 mm TypeofTrap: 308 Facility / Source:PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: tr PASS tr FAIL Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: (f,a trB SAMPUNG CONDITIONS AND PARAMETERS POST-Run LeakCheck tr PASS tr FAIL Avg. Duct Temp (F'): Avg. Trap Temp (F"): Estimated Avg. Hg Concentration (pg/dscm): Event Occured During Sampling: tr Startup CEMENT ONLY: tr Shutdown Avg. Flow Rate (cclmin): Total Volume (L): _--_"_---- or (dscm)#of RAW MILL OFF events during sampling: REQUIRED IFRETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): l./p,tq Wzs @&,alidr rilgE ri, 6. sl bascd fi lh6 Et c torvitg 0& e* ,ra, ,Esul h arada&rsrsl sarFir Pi.asa cs|tact ti6 irf FU Ggt r sssirlae ast nalirg lrrC r,'t,c CHAIN OF CUSTODY Ensue samplmg @ndlrcns pruvsrt moasture condensation in the trap media. Moisture condensatbn is a rnaior cause Spikiog Mclhod Cold Vapor Adsoetion Ma lnpingEr Sparoing hified Acqxacy r t0ith Traeabh to NIST measuremenl Prdje0tffi4 eE€0ofre il88&i768eill tollfree www.dtbbrm.com mail@ohiolumex.com 30350 Bruce lndrtd*8|rou Cleveland, OH 44139 USAI lf applhable place chah of custod seal here. (see security seal instruction sheet) Seal intact as received: ves E HoE Sample(s) received by lab Seal intact as received ves E noE Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form D UNSPIKED Production Lot S-4€F,A Carbon Lot 4C _ QA/QC Signature (spirc): SAMPLING INFORi'ATION tr SPIKED AT: _?9""n9 Spike Date: *gg!osA-022* - SpikeTime 1401 ililtilililrififfirulillil o1c156360 QA/QC Signature Fr+esccrnpry): fJ tr High Flow tr Fluffy prefilter tr Static Prefilter tr AGS TypeofTrap: 308 tr 185mm tr240nrn tr 300 mm tl 450 mm Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: D A SAMPLING CONDTTIONS AND PARAMETMS PRE-Run LeakCheck fl PASS Run Start Date/Time: Run End Date/Time: Run Number (optionat): POSTflunLeakCheck trPASS I I tr FAIL tr FAIL Avg. Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cclmin): TotalVolume (L):or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): No,ie,r1€lyzqcdl&$tirrt {Erilrbes.t6as€da,ddeEht4iudistffimtyrsthanofs{bralrmanrhJrrPh6sccdflci.rrff}6ur,ccuiesssisirE Gtindiudri,}.f: CHAIN OF GUSTODY * Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: #of RAW MILL OFF events during sampling: lf applicaHe place chain of o.rstody sealhee. (see seonity seel instrwtlm sheet) BestBefore:June 2025 9\1il{pAn62800zt'fgn 1t888 trI5g6eE tollfree www.ohldflnfrtf,ftom mail@ohiolumex.com 30350 Bruce I n d Etf ffitfldhP/3tr Cleveland, OH 44139 USA Sampling Location: Source Condition: Dry Gas Mebr No, Run Number metricPrsssurc, 2{.ol9 -_ -totengtn*r F- Trap Number OLC I82 (l0'I Nobs: Train A: Traln B: Pre-Test Leak Check-- pass @__lE_'Hg (Must be 2l5"Hg)Post-Test Leak Check - pass-@ Iil ,i; Pre-Test Leak Gheck; pSss @- -tf "x! 6lust be l ls,,Hg)Post-Test Leak Check - paos-@-T5 .,9; ' Ds.021 pr€r'odrirSl[,ilbtgmt rrae Main Kiln Stack DryGasttlebrNo.ldh? V=O-C|Q1 TnpN*ra.@Sp*eValrn rU Samok Traln B Gtock Tlm. 2llran hrrVolumo lV-l lbr ildcrTomp. (bl .F Iabrvecuum,rlla I r'.RA o -to 5 I t'.u\5'.0 r{ 1 -?o Iil .,r{8 lo, oq o -1t\9 I I'. S'{.19.o3 I '1 r S I t'st ?,,o5z -ll sDiO".2s.o35 -1 r q l)-'- aQ ?o,b{? TotaUAy.r.ge -10, I 120 oFw62.r @MSfimflatt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form ililtiltililililililuilil 01607149 A UNSPIKED Production Lot: Carbon Lot: 4C tr SPIKED AT: U-l1D9 Spike Date; QA/QC Signature rspr,el: SAMPLING INFORMATION Spike Time: QA/QC Signatures.pe'emuy)r h& _ tr High Flow tr Fluffo prefilter E .tB5 mm tr 240 mm tr Static Pr+filter tr AGS tr 3(x) nrn tr 4li0 mm TypeofTrap: 308 Facility / Source: Sampling Location: Run Number (Optional): PRE-Run LeakCheck tr PASS Run Start Date/Time: __- _t Run End Date/Time: -"__. .. _ l-__ POST-RunLeakCheck trPASS tr FAIL Boiler lD: Sampling Train: G) tr BL-,, SAMPLING CONDTTIONS AND PARAMETERS tr FAIL Avg, Duct Temp (F'):-. Avg. Trap Temp (F"): Estimated Avg. Hg Concentration fug/dscm): Event Occuned During Sampling: tr Startup CEMENT ONLY: tr Shutdown Avg. Flow Rate (cc/min): Total Volume (L): ._-.---_ or (dscm) REQUIRED IFRETURNING TO OHIO LUMEX #of RAW MILL OFFevents during sampting: Estimated Hg Mass in Section 't of Sorbent Trap (ng); CHAIN OFCUSTODY Ensure samptng condttions prevent rnoisture condensatrm spikhg Merhod cord vapff Adsorprion via tmpinger sparling Certih& accuracy t r ot rraceabte ro lt rsr measurernefit h sorbeflt traps be prg/cnted. 1n&26|flr@Effita 1ffi'8ft fiHgttoil free www.oni&l8{Jf.to, mail@ohiolumex.com 30350 Bruce I nd rglyEltti8l,Pyl'n Cleveland, OH 44139 USAI lfapplcabh pbce chah of oJst@sealhere. (see security seal instruction shee$ Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form ilffiililffrfinmlttr o1c175835 tr UNSPIKED Production Lot S-4FF4 Carbon Lot 4C QA/QC Signature rser.r: E SPIKED AT: 2sl!s_ Spike Date: t/15/2OZz SpikeTime: 1303 Y- QA/Qc signatureo.pAssnpn: X[4r tr High Flow tr Ftuffu prefitter El 1BS mm tr 2l() mmtr Stath Prefilter Cl AGS tr 300 mm D 4S0 mm TypeofTrap: 308 SAMPLING INFORMATION Facility / Source: Boiler lD: Sampling Location: Run Number(0ptional): Sampling Train: tr A Avg. Duct Temp (F'): Avg, Trap Temp(F'): Avg. Flow Rate (cclmin): TotalVolume (L): PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: tr FAIL *t " . t_ tr PASS POST-RunLeakCheck trPASS tr FAIL IAMllllglglgtnoNs AND PARAMETERS Estimated Avg. Hg Concentration (;ig/dscm): Event Occured Ouring Sampling: tr Startup CEMENT ONLY: d Srrutoown or (dscm) #of RAW MILL OFF events during sampling: RFgy-l|Pll-lErg$ltrtg ro oHro LUrrrEx Estimated Hg Mass in Section 1 of Sorbent Trap (ng):l@e:A*lyt.,cdf'o,,,o'reF''/'rb'sclbtscdaurrwiaic,irg&ttrkrrarayJi-rJdi--"1""-a*r.o,r*r^rr..rre$/i!a$brrceasrinsr*Eo& yrrrr. CHAIN OF CUSTODY i lf +plixble ptace chain of custqdy seal here. (see security seal instruction street) Sample(s) prepared for shipment by Ensure sarnplino condifi ms Dfewnl mo spiking Meihod cord vapor Adsorptbn via rmprngei spirlirs d;it &crra"y , r o{, iEiii'itfi ruisr \1ndOe26{eflEBAfiI2A 1 8B'8f,b S&Et totl free Best Before:July 2025 o 3o3so srr." rnarr@#3i'F[lfi]"nv Cleveland, OH 44139 USA 15 www.ohiUG8{eif.8o, '*' mail@ohiolumex.com MERCURY SORBENT TRAP FIELD DATA SHEET Project NameNumber Sampling Location: t1K Saetk Run Number: A Source Condition: Dry Gas Meter No. p*ssur€: 1ul .f < TestErgineer: Snz6 TrapNumbff OLOO'I13O Nobs: Train A: Train B: Pre-Test Leak Check - Pass @ lb "Hg (Must be I {6"Hg} Post-Test Leak Check - Pass @_jJ "Hg Pre-Test Leak Check - Pass @ l9 "Hg (Must be 2 l5"Hg) Post-Test Leak Check - Pass @_19_"Hg D$02tl[regIl$fo9ffi gffi6arrao Main Kiln Stack Samole Traln A Cbck fime 2a hout illobrVolume lV-l lltaa reror ramp. (t-) .F lletarVacuum, n{a itorDant I ttpt T.mp. .9 Strck Temp. .F l2: lq b -7 ?_5 'Lb I 2 oca. i2.-t 8 6.de I 'rB s 2,Gt 208 l?'.?.3 to , o?tl -?i s >G2 26R l?',1.8 t5.o3l '1B s 26t 208 l2ig5 20.O3f,1q s LGt ?oa 12138 zs.oqLt -? l.l I zGl zaR i2ir.l\3r).or{ I TotaUAvorage l3 2-A I DryGasMeterNo.@y=0.qq1 TrapNumber OL(oO'?li I Spikevatue_ng Sample Train B Clock Time tebrVolume lV-lllbn Meler rtmp. (t-l .F mebrVrcuun,rtla t).la o -'t ?5 t7'.Ig g.o5 t.'-li g rLzl lo.o 5 0 -7'R S tz:2R l5.oqD.'?B 5 tz:91 2.o.Obtl -l'i 5 l2'.in z5,osG -1 tt (, lz:t|)30. oqq TotaUAverage t.} rzs offt6 2.1 outd{l#llF0tatt Our Trao lD iltIiltffiIiltlilililtililtilt oLcL82607 UMEX Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form A UNSPIKED tr SPIKED AT: Production Lot U-11DA Spike Date: Carbon Lot 4C Spike Time: QA/QC Signature 6pr4: SAMPLING INFORMATION QA/QC Si gnature frrap Asacmbry)i tr High Flow tr Fluffy Prefiher tr Static Pre-filter B AGS TypeofTrap: 30B E 185mm tr 24omm tr 300 mm E 450 mm Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: tr PASS tr FAIL POST.Run LeaKChecK O PASS tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occuned During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: I I ,\ Sampling Train: qJ trB SAMPLING CONDITIONS AND PARAT'ETERS Avg. Duct Temp (F"): Avg. Trap Temp (F'): Avg. Flow Rate (cc/min): TotalVolume (L):or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CUSTODY Ensjre sampling conditions prerrent rnoisture condensatioo ln the trag measuremeot in sorbent traps and sfpuld be Spikln0 Method Cold v@or Mso$tion yla lmpinoer Sparging Certified Accuracf t 10%, Traceable to NIST Best Before: January 2026 *rr'r.oilfr1,f&/"98.o, mail@ohiolumex.c0m lf appficable place chain of cust@ seal here. (see security seal instruction sheet) Seal intact as received: ves E NoE Seal intact as received: ves E NoE \ rffiBff4H{ff#*"" (! 3o3so Bruce rndrglYhsl$f,\f{rttY Cleveland, OH 44139 USA Trap lD illllililril]ll]llIllllllll oLcl2243sSorbent Trap Chain of CustodY Form Ohio Lumex Co., lnc. I Unspiked tr Spiked At: Spiking Method Cold Vapor Adsorptlon vla lmpinger Spar8ln8 Crrtifled Aocufircy i 10t6, Traceable to NIST Production 1s1; U-FD8 Carbon Lot: 4C Spike Date:Spike Time: AA/QC Sign atu re ffrap Assemb[]L OA/aC Signature (spike)- Type ofTrap: trHlBh Flow Dcoil Pre'fllter E2{l mm Estatic Pr*fiher DaGs 03(E mm tr Fluffy Pre.fitter 8185 mm E45o mm 308 PlanVSource: TO BE FIU.ED OUT BY SAMPUNG TECHNICIAN PRE-Run Leak Check (circle one): PASS FAIL Boiler lD:Run START: Sampling Locatlon: (stock, FGD tnlet, etc,) Run Number(optional): Run END: .-........-.-."- -----';- sampringTrain (circte one): A @ posr-Run Leak check (circle one): PAss FAIL Notes: SAMPUNG CONDTTIONS AND PARAMETERIi Ave DuctTemp (F'): Ave Trap Temp (F"): Estimated Ave Hg Concentration (Ug/dscm): Circle Event if Occurred During Sampling: STARruP SHUTDOI^IN Flow Rate (cclmin):r For CEMENT KII,NS ONIY otalVotume (L) or(dscm):No. of RAW Ml l'l- OFF Events Duri ng Sa mpli ng: REGTUIRED IF REruRNING TO OHIO LUMEX FOR ANALYSIS Estimated Hg Mass in Section l of Sorbent Trap (ng): NoteAnotyfrcottbrouonronOcwtttbel,el.bagidonthtswtue. Lavtngthlsbtonkmoyrgljuttlnout'oficoltbfotionanolyslt Pla*Gontoctutil"ou Oraln Of lf Appllcable Place Chain of Custody seal here (See SecuritY Seal Seal intact as received Seal intact as received Seal intact as received Seal intact as received yes ff r.ro EJTrap analyzed by @. prilari rnobtuna coatdatE fon ln ol. mp lmor, uollru]l qEnxrpr rnd rhould br prwrntod rt rli co"tr D€actlveted d.3t lnd d.s.t wool lmPrc$a6d Acivrted Catbon - R'fet to SDS Best Before: June 2024 #?ffl#"#ffiT#,4 1888 876 2611tollfree ***.otfr3?uot{rt99.o* mail@ohiolumex.com 30350 Bruce 116$ffiqfl1fi|att Cleveland, OH 44139 USA? &vcasrftbrxo'!1hl v=O,Q{J rnp*umber@sprtevahr ng Sample Traln B CbcInm. 2ahorr lh{erVolumc lV-l lkra rDrTamp. (t-) )F t Ervftllm 't{a t 2:86 0 -l{5le'. ss 5^OBL 1r{5l'i'-oo lo.bs f{'1 Y g ta'.o E l5.b 5'l .?S sll'-t 6 2'0, oq-l 'rs 5ri'- t 6 z9.o(. I -?5 st?'.2-6 30,o51 TotalrAwrlgc 1'{.q tlobs: Traln A: Train B: D$02 1 pf8jBef, ffl .Sffi lgffi r rnc Main Kiln Stack rqi*ff:L"#:lJ;::"""=filf,[i'ust be r I E'Hs) Pre-Test Leak check.- p:cs @E' Hg (Must be I l5,,Hg)Post-Teet Leak Check - pass-g TFr; ' 126 oR6002.r @t\4fflaulflatt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form illliluililililililIiltil 01607130 E UNSPIKED tr SPIKED AT: Production Lor U-l1D9 Spike Date: Carbon Lot 4C Spike Time: QA/QC Signature epu,cl: SAMPUNG INFORMATTON QA/QC Signature Fraprssernbry): e" 4 [1 High Florv tr Fluffy prefilter B tBS mm tr Static Pre-filter tr AGS O 300mm TypeofTrap: 308 tr 240mm tr 450 mm Facility / Source:PRE-Run LeaKCheck tr PASS Run Start Date/Time: Run End Date/Time: *.-"_l POST-Run LeakCheck tr PASS tr FAIL Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: @ SATT,PLING CONDITIONS AND PARAIUETERS trB tr FAIL Avg. Duct Temp (F"): Avg. Trap Temp (F): _tr Shutdown Avg. Flow Rate (cc/min): ____*- ___ Total Volume (L): _-------- or (dscm) # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OFCUSTODY crsuE Errrpug qonol[|ons pracftt moslurt @nden$tion in lhe trap medla. Moisture condensatirn is aspiking lvhhod cord v4or Msorptixr vra l,nplrocr sparging centinea tcuracy t tot, rraceaoCto utsr Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup CEMENT ONLY: www.ot{nlumscom mail@ohiolumex.com 30350 Bruce lnd@il{el4$ffFtt Cleveland, OH /t4139 USA9 !f appllcabh place chain of custod seal here. (see security seal instruction sheet) yes E NoEI ves E NoE r hfn#tm;9mtffffi"" Oxt Trap lD ilililililfi]il]ilt 01607191 UMEX Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form il A UNSPIKED tr SPIKED AT: Production Lot U-l1DA Spike Date: Carbon Lot: 4C Spike Time: QA/QC Signature eiul: SAMPLING INFORMATION QA/QCsignatureonpAsaenrbry)i / tr High Flor tr Fluffy prefilter E 1BS mm tr 240 mmtr Static Pr+filter tr AGS tr 300 mm tr 450 mm TypeofTrap: 308 Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: tr A Bnsure samptng condit,ons prsent rnoislure cilEensatioo in@ spiking Method cord vapo, Adso.ptior yra hpinoer sparging cenifiA Accura"y t r orr, iirc.ror"- to Nisi PRE-Run LeakCheck: tr PASS Run Start Date/Time: Run End Date/Time: D FAIL t. I POST-RunLeakCheck trPASS tr FAIL SAI,IPLING CONDTTTONS AND PARAilETERS Avg. Duct Temp (F"): Av!. rrap Temp (F"): Avg. Flow Rate (cclmin): TotalVolume (L):or (dscm) REQUIRED tF RETURI{ING TO OHIO LUMEI( Estimated Hg Mass in Section 't of Sorbent Trap (ng): __Nde:An*zet .dffibn ra"g.wifbeselbss€do m niniaiinrrrcur*qyrcoilr;"f*h.r-r;"4"" mr*oorr*r L,rp,lrrgui,reassrsra,ce*tir*hgrtir rdr CHAIN OF CUSTODY Estimated Avg. Hg Concentration (pg/dscm): Event 0ccuned During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: oEaS[rretTEnt in sofbent traps and I Best Before: January 2026 @Mostardi Platt 30350 Bruce tndustrial pkwy. Cleveland, OH 44139 USA lf applicable placc chain of custody seal here. (see security seal instruction shee0 Sample(s) received by lab \ lffiffi$ffif#ifl. 128 of 16675 www.ohiolumex,comrj/ mail@ohiolumex.com MERCURY SORBENT TRAP FIELD DATA SHEET Source Condition: Pressura: z,{ 4( TestEngln€en SF4CG .DryGasMeterNo. t4h? y= Oiqb - Topiu6".@ Semple Train A Glock Tlne 2l horr lletrrVdume lV-l lltnn ilet r T.mp. (r.) .F lletrrVrcuum, "l{a soilant Tr.pr Tcmp. .F Stack Tcmp. .Elj:tr I o 16 5 z6b 2 orq lSirr 5 5.051 '?q 5 260 208l3:50 to.or{'I 14 5 260 20813.56 r5.o3q 1s 5 2-6 0 zoR l{',O()zo.o 52.-15 5 zLO zo8 tqioS 25, O q(-15 5 z6h zo3; Itf it (3o,ot{'{ TotauAvgrag€.I5 2on DrvGasMeterNo.t4lull v= o,dlQJ rraprurro"r oL60?2{J spikeValue ng Sample Traln B Clock Tlmc )l lsrtt I6t!r Volume l1/-l liira tsE?Tsmp.(t) .F IetcrVrcuum,rlla l3:\ b 0 -r5 5 l3'.q q 5.06'I -?5 5 i3'- so io.oqq th c) Its:55 t5.066 'r5 5 irt.,oo ".o. o5R -?s 5 lLt .'o 5 z(.o5R 'r<\l{'.1b 30.ar{R, TotaUAverago -16 Notes: Traln A: Train B: Pre-Test Leak ChEck- Pass @ l6 '.Hg (Must be I 15,,Hg) Poet-Test Leak Check - Pass @JE ,'Hg Pre-Test Leak ChEck- Pass @ lf, ,,Hg (Must be t iS"Hg) Post-Test Leak Check- Pass fulla-],Hg Ds-02 lPMfe*ftTt,'lg ggPt r',"' Main Kiln Stack rzs oFS62.l @Mdflfloeplatt Ohio Lumex Co., tnc. Hg Sorbent Trap Chain of Custody Form Trao lD illliltfltililililr oL60724 A UNSPIKED tr SPIKED AT: Production Lot U-11DA Spike Date: Carbon LoI 4C Spike Time: QA/QC Signature €pike): SAMPLING INFORITIATION Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): samplinsrrain: GD SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cc/min): Total Volume (L):or (dscm) trHighFlow trFluffypr+filter tr tgsmm tr240mm tr Static Pre-fitter E AGS tr 300 mm tr 450 mm TypeofTrap: 308 QA/QCSignaturefinpAssartry): ^/ PRE-Run LeakCheck tr PASS Run Start Date/Time: Run End Date/Time: _ I] FAIL I I trB POST-Run LeakCheck tr PASS tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: u startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CUSTODY L,nsure sampling conditions pr€l,enl. moislure condensation ln spiking Method cold vapo.Adsorption \4a lmpinger spa.qlng cenifir'd nccuracy r toji rraceable ro Nisi ,**.otit18,8{e1f.Bo, mail@ohiolumex.com Best Before: January 2026 O 3o3so srr." rnorro#3?ttilli:"tv Cleveland, OH 44139 USA measufanent in sorbent traps and sharU be lf apdlcable place chain of custody seal here. (see sectrity sed instruction sheeD Sample(s) received by tab \ . r EmztusdutrtffiSA-' 18trdrtsiffif tou free A UNSPIKED Production Lot U-l'lDA Carbon Lot 4C QA/QC Signature (sp&e): SA[,lPLlNc INFORMATION tr SPIKED Spike Date: Spike Time: QA/QC Signature firsp l"snuy)i tr High Flow tr Fluffy Prefilter tr Static Prefilter tr AGS TypeofTrap: 308 ililttttfrffiilfirrtln o1507096 /::\ E 185mm tr240mm tr300 nrn tl 450 mm Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form Facility / Source: Boiler lD: Sampling Location: Run Number (Optional): Sampling Train: tr A SATTIPLING CONDITIONS AND PARAMETERS 6 PRE-Run LeakCheck tr PASS Run Start Date/Time: I Run End Date/Time: _ - I POST-RunLeakCheck trPASS tr FAIL tr FAIL Avg. Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cclmin): TotalVolume (L):or (dscm) REQUIRED IF RETURNIilG TO OHIO TUMEI( Estimated Hg Mass in Section 1 of Sorbent Trap (ng): __ CHAIN OF CUSTODY nrishre cmdensation i8a measurerneflt traps Spikino ^retEd Cold Vapo. Adsorpiion Vle tmpinger Spargino CenfEd Accuracy r I 01, Traccable to NtgI Best Before: January 2A26 Estimated Avg. Hg Concentration (pg/dscm): Event Occuned During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: \***.onltlr?I199.o, mail@ohiolumex.com 30350 Bruce', o 8lf f.Tfil'ifl :t' Cleveland, OH 44139 USAI Sample(s) taken by lf apflixHe plaechain of custody seal here. (see security seal instnrction sheet) Sample(s) received by lab tQr*rgqe!ffi?ftt&t 1Us8ff BlBf[ torrr'ee @ Appendix G - Galibration and Response Time Data Project No. M2325124 Main Kiln Stack 132 ot 166 @Mostardi Platt Cl.nt Ash ODve coment Cmpany Frdlity: Leamington Comfft Pbnl Prcr.d* M232512 TBt Ldbn: Main Kih Sb* O*t 6nU2O23ombr R. solb6 op.6ung condltlon MIN On S.mpb sfbm: kob bngffi: Prcbe Typ: S.mpl. Pl.n.: Pon Longlh: Pd Slz. (dl.mcbr): PonTr: Dud Sh.p.: Dbmataa: Dudk.r up.hm Olm.i.B: OomframDlffih: Numh.d Poi.8.m9l.d: iumbr ot Pd6 p.r Pot Idl NmhrdTd.E. Polnb: FTIR 8.0 nlR Hotonhl 3 3 Flangs Ci@k 11 Polnt* 1 ln. 2 ln. 3 Pold t.ftln$ (lncludlne pod hngth): lnchat 18.75 il21 a1 71 ft 9c. Ft95.03 4.1 I 3 3 Mlnimum UFEh Ol*ne Mlnimum Dilmtream Dlsbnca lded UFtroam Dlsbn6 ld.d tumsham Dblene 5.5 Fs€t 2-0 F*t 22 O Fo6l S.0 F66t Callbrallon Gase3 fr Sdlng Cyllndn D Cyllffir Vdu.frdqlndf%dhrgh Fhat Bo& 02 TF Sdlng Cyllnd.r E Cyllnd.r Valu.Pr.dhd V.ls Dil fHC ppmw {09 9S2 9I tm% 30.1 1 Typ.CmFund qdhsr D Cyllnd.r V.tu.kplrilon D& are Gaa f,tuog.n Zeo Nltw6n 0.0m >500 ESyhn.xc02s592B 1m.2 u112030 cc510322 11t1012023 M6Eda Plat Project No. M2325124 Main Kiln Stack v5.0 '133 of 166 MTA flIR IX22 @Mostardi Platt Client: Ash Grove Cement Company Facllity: Leamington Cement Plant Proiect lt M232512 Concentration of Cal Gas C = Average value of test ,erage Pre and P6t Span Cqas = Corected gas value of t6t Mostardi Platl Project No. M2325'l2A Main Kiln Stack TGst Location: Main Kiln Stack Dato: 6/20/23 oporator: R. sollars 02 % Corection: 7 Co=Average Pre and Post Zero CalibEtlon Con€ct6d and Calculatod Oata v50 134of166 RATA FTIR 1/1/22 OMostardi Platt -o 4 6 19.95 19.98 19.94 {.01 {.01 -0.01 19.98 8 1.4 0.90 o.00 21 C /19.95 -0.0'l 5 c o.33 I 6 19.95 20.04 20.08 0.04 o.08 0.08 20.08 I.24 1.3 0.57 o.00 -0.57 0.00 19.95 20.08 20.04 0.08 o.08 0.08 20.08 7.43 7.4 0.57 0.00 -0.57 0.00 10 19.95 20-08 20.o2 0.08 -0.01 0.04 20.05 6.99 7.0 o.77 t).20 -o.27 {.30 Run il Run Date Start Time End Tlme NOx ppmw so2 ppmw co co2% (drv)O2oh ldtyl lf,olsturc Y.THC ppmw HCI ppmw Flow, SCFtI 6t20t23 7:30 197.6 o.2 1021.O 7.7 0.4 8:07 8:36 204.3 0-3 1 185.8 10.1 o.2 6t20t23 8:43 12 209.7 o.2 1253.7 7.2 o.2 4 6t20123 9:35 1O:04 1S5.6 -0.3 1 484.8 7.5 0.4 6120t23 1O:12 10:4'1 192.4 .0.4 577.9 7.5 o.2 6 6not23 10:48 11..17 207 A 4.4 M1.1 7.4 0.0 6120t23 1 1:38 12'.O7 200.'l -0.6 455.6 03 E 6not23 12'.42 1 98.1 -0.5 465.1 7.3 0.1 6120t23 12:50 13:19 210.3 "0.5 518.6 7.4 0.0 10 6120t23 '13i40 14:09 193 I -06 538 4 70 Run *Run Data Start Time End Time Clinker Production Rate NOx lb/hr co rbrhr 02v" (wet) co20/. (wet) TtlC ppmvd @7o/o02 HCI ppmvd @ 7v6 02 r':1o 2 6DOt)3 807 8l l1a 4 g4 1'3 3 6DND3 Ra3 9.12 114 7 1)5 l{r 41 l lq l lq .12 t.19 Client Ash Grove Cement Company Facllity: Leamington Cement Plant Test Location: Main Kiln Stack Date= 6120123 Project #: M232512 Time 6:21 6:22 6:23 6:24 6:25 6:26 6:27 6:28 6:29 6:30 6:31 6:32 6:33 6:34 6:35 7:00 7:01 7:02 7:03 7:04 7:05 7:06 7:07 7:08 7:09 7:10 7:11 7:12 7:13 7:14 MostardiPlatt Project No. M2325124 Main Kiln Stack Linearity Gal/Pre I Cal O2olo ldrvl THC ppmvw 30.32 30.11 22.38 1.66 -0.08 -0.09 8.79 21.11 20.98 20.25 19.13 3.58 9.41 9.89 10.11 22.20 22.10 9.60 0.00 19.20 1 1.10 11.10 11.10 0.00 0.00 0.00 11.20 1 1.30 1 1.30 11.30 ih az lm v5.0 135 of 166 RATA FTIR 111122 OMostardi Plaft Glient: Ash Grove Cement Company Facility: Leamington Cement Plant Project #: M232512 Test Location: Main Kiln Stack Date: 612o123 Post l/Pre 2 02% ldwl 0.000.00 z 1.30 10.9011.00 m 20.60 20.60 20.70 20.70 Post 2/Pre 3 Time 9:23 9:24 9:25 9:26 9:27 9:28 9:29 9:30 9:31 Time 9:23 9:24 9:25 9:26 9:27 9:28 9:29 9:30 9:31 Time 9:23 9:24 9:25 9:26 9:27 9:28 9:29 9:30 9:31 THC ppmvw 8.44 -0.29 0.35 2.01 0.09 12.08 19.37 20.19 20.09 O2o/o (drvl 0.00 0.00 1.30 10.90 11.00 20.60 20.60 20.70 20.70 THG ppmvw 8.44 -0.29 0.35 2.01 0.09 12.08 19.37 20.19 20.09 Post 3/Pre 4 O2o/o (drvl 0.000.00 z 1.30 10.9011.00 m 20.60 20.60 20.70 20.70 Post 4/Pre 5 THC ppmvw 8.44 -0.29 0.35 2.01 0.09 12.08 19.37 20.19 20.09 02% (dwl 0.00 0.00 0.00 11.10 11.10 20.20 20.80 20.90 20.90 21.00 THG ppmvw 2.31z 0.39 -0.01 -0.01m -0.01 0.00 4.65 10.97 19.88 19.98 Time 11:25 11:26 11:27 11:28 11:29 11:30 11:31 11:32 11:33 11:34 Mostardi Platt Project No. M232512A Main Kiln Stack v5.0 136 of 166 RATA FTIR 111122 @Mostardi Platt Glient: Ash Grove Cement Company Facility: Leamington Cement Plant Project #: M232512 Test Location: Main Kiln Stack Date:6120123 Post S/Pre 6 02%(dll THC ppmvw 0.00 2.31 0.00 z 0.39 0.00 -0.01 11.10 -0.01 1 1.10 m -0.01 20.20 0.00 20.80 4.6s 20.90 10.97 20.90 19.88 21.00 19.98 Post 6/Pre 7 Time 11:25 11:26 11:27 11:28 11:29 11:30 11:31 11:32 1 1:33 11:34 Tlme 13:27 13:28 13:29 13:30 13:31 13:32 13:33 13:34 13:35 13:36 Time 11:25 11:26 11:27 1'l:28 11:29 11:30 11:31 11:32 11:33 11:34 Time 13:27 13:28 13:29 13:30 13:31 13:32 13:33 13:34 13:35 13:36 02%@rvl 0.00 0.00 0.00 10.90 11.00 11.00 11.30 20.60 20.60 20.70 O2o/o (dryl 0.00 0.00 0.00 11.10 1'1.10 20.20 20.80 20.90 20.90 21.00 THC ppmvw 2.31 0.39 -0.01 -0.01 -0.01 0.00 4.65 10.97 19.88 19.98 Post 7/Pre 8 O2o/, (drvl 0.000.00 z 0.00 10.9011.00 m 1 1.00 11.30 20.60 20.60 20.70 Post 8/Pre 9 THC ppmvw 0.21 0.01 0.01 0.77 0.08 0.11 0.21 2.54 19.99 20.08 THC opmvw 0.21 0.01 0.01 0.77 0.08 0.11 0.21 2.54 19.99 20.08 MostardiPlatt Project No. M2325124 Main Kiln Stack v5.0 137 of 166 RATA FTIR 111122 @Mostardi Platt Client: Ash Grove Cement Company Facility: Leamington Cement Plant Project #: M232512 Test Location: Main Kiln Stack Date:6120123 Time 13:27 13:28 13:29 13:30 13:31 13:32 13:33 13:34 13:35 13:36 Time 14:16 14:17 14:18 14:19 14:20 14:21 14:22 14:23 14:24 14:25 Post 9/Pre 10 O2o/o (dwl 0.000.00 z 0.00 10.9011.00 m 11.00 11.30 20.60 20.60 20.70 THC opmvw 0.21 0.01 0.01 0.77 0.08 0.11 0.21 2.54 19.99 20.08 Post 10 02 % (drvl 0.000.00 z 0.00 10.9011.00 m 11.10 20.50 20.50 20.40 20.40 THC ppmvw 0.31 0.05 -0.01 -o.02 -0.01 0.00 3.11 12.98 19.98 20.02 MostardiPlaft Project No. M232512A Main Kiln Stack v5.0 138 of 166 RATA FTIR 111122 OMostardi Plaft i c.E!s6 tI Y (E oo o (o(o 9oo)(") c 3 6 T ii!E TBIgglt!! 5E ! l- 3gE5 ;6: Ed:ET :,!!i 5isis Io.i3i g-'i IEIi1 (\l roN(.)v N7i =Eou)7Ct9Or0"6Ed> Et : El36 E(L E (E oo @ (0 @ 9oost ao n s 3 iBBi SSaE5il{ ! IEi a n& iE 59 r!ii t:E!ot95 I 6 N loN(o-c.t6>g du)7C 6EOa 96Fd= T e : s(Eto- E(E oo o (o(o go $ -rl I ,:lil r:lrat tt .rl EI ;$:t:lEI _ltsH -ll!l &t 8il u 5il Irl ! t z I N loN(r)- N?i>5 oa7C E9Oa 0"6Ed> E* = ?d E iE!E El.I 5t'lEI 5E i sti3 3? a Fi :lti !:E!6l *5 a MOSTARDI PLATT Procedures for Method 5 and Flow Calibration Dry Gas Meters The test meters are calibrated according to Method 5, Section 10.3 and 16.1. and "Procedures for Calibrating and Using Dry Gas Volume Meters as Calibration Standards" by P.R. Westlin and R.T. Shigehara, March 10, 1978. Temperature Sensing Devices The potentiometer and thermocouples are calibrated utilizing a NIST traceable millivolt source. Pitot Tubes The pitot tubes utilized during this test program are manufactured according to the specification described and illustrated in the Code of Federal Regulations, Title 40, Part 60, Appendix A, Methods 1 and 2.Ihe pitot tubes comply with the alignment speciflcations in Method 2, Section 10.1; and the pitot tube assemblies are in compliance with specifications in the same section. CN&F-002 Cal Procedures M5 & flow Rev.2.2 1t1t2021 Project No. M2325124 Main Kiln Stack 142 of 166 @Mostardi Platt Dry Gas Meter/Control Module Calibration Diagram ATD-090 Dry Gas Meter Calibration Project No. M2325124 Main Kiln Stack Rev. 1.2 1t112021 143 of 166 @Mostardi Platt (! d E (E oo o (o @ o $s N lr) Nc/, vN7i =E6@7C 6=Oa0'6d= zo F e. @ J a g. u.tF IJJ = d Y G oo o (o(o o lr)$ N lo N(f)v N7i>E 6u)7C 6=()a 0'6d> 3 ooqo @o, o?o Noqo6 ooo)olr) oo,qo() o6qoo oo @c! 6 @ oNd @ ooq <fN (o N co o?* NN:l ! @F.\NN q F-N C C oq N oq N G c G o r g E ots EgEEE}5f Eo E G e E6o o o = o( G so6 o =o t E!dlE,! FL o o o ti6l6,1 F! E (( o; -oi= o = 9-5* a=l E o E OE E!! OE E eo o OE E.-6E o E o o- ooF o = a26E(,.o ' ooEo,ro o o o =ooo o o>*E EAe6 o o2CE(,,o o E i: / !ooo! uJ .E E o o ! oo o E3 oo r)\ 9(5 \ a 6l co E c6) aoo Y E E @ No @oN oL o Eo- o o Eo 6l0 N n hooq 2 = o o6r Go-I zo F- d. @ J ot lrJ UJ = Stack Temperature Sensor Calibration Temperature lD :526 Name:Rods Ambient Temperature, '82.5 Date:May 25,2023 National lnstitute of Standards and Technology (NIST ference Source Temoerature (o Test Thermometer Temperature (o F)Difference 96 0 0 0.0 250 250 0.0 600 600 0.0 1200 1204 0.2 (Ref. Temp.. "F + 460) - (.Test Therm. Temp.. "Ell60) * 100 <: 1.5 % Ref. Temp., "F + 460 Project No. M2325124 Main Kiln Stack 146 of 166 @Mostardi Platt S TYPE PITOT TUBE INSPECTION WORKSHEET Pitot Tube No: 4036 Dale: 5/2412023 lnspectoB Nam€Rods ryp€orProbe:(circtaon") f-;I-;T;;l ProbeLeneth: 8 ft.I-t-T--l NOTEI F.os q<rr <r.s DL "^ '"" il ffi[ i '11 1l v-----------t)t,' I#tl lr0\ii I \__1-_._l_ i i -'xMi9l$l ' * Z--...-- dJ__=Jp:::::_ cy' Pitot lub€ assmbly level? Pitot tub€ openings damaged? X y6s _no -Yes (sxPlain b€bw) 6r= br= O "(<10") s.= g o(<10) 2 '(s5') br= 1 o (<so) 3 . 0= _L A= 0.94s (in.) Xno 0.049 (in.): (s0.125 in.) 0.01649 (in.); (10.03125 in.) 0.473 (n.), PB = 0.473 (n')' D' = 0.375 (in.) Rev. 1.0 147 ot 166 --I-no z=Asiny= w=Asin0= CalibEtion required? PIS-001 S Typ€ Pilot Tuh bsdid Fm Project No. M232512A Main Kiln Stack a1712020 @Mostardi Platt Appendix H - Calibration Gas Gylinder Data Project No. M232512A Main Kiln Stack '148 of 1 66 @Mostardi Platl CERTIFICATE OF AI\IALYSIS Grade of Product: E03N!78E15A0225 cc41il70 124 - Los Angetes (SAp) - CA 832022 CO2,02,BALN AiIUAS. an Alrllquiclo cmDely Alrgac Specldty Gascs Airgas USALLC rtTu S, Alameda Strea Loe Angeles, C,A9ooS9 Airyas.com Part Number: Cylinder Numben Laboratory: PGVP Number: Gas Code: Trlad Data Avaltable Upon Requ$t EPA PROTOCOL STAhIDARI) Reference Number: 4g-4O2ST4T1g_1CylinderVotume: iS2.0CF Cyllnder Pressure: 20lS pSlG Valve Ouflet: Cedification Date: 590 M.28,2022 CARBON DIOXDE OXYGEN NITROGEN 11.00 % 11.00 % Balanca 11.,t7 % 11.w%+l-0.7% NIST TraceaHe CALIBRATION SI]ANDARILS Concentrallon NTRM NTRM 13068t32 98051002 cc!.13737 SG915O866BAL +/- 0.6% +l-0.7% NDIR PARAMAGNETIC M.17,2A2 @13,2022 149 of 166 ottrostap$falt,, Aitgas. anAhuqidccoqqny AfryreSpcdrlryCeces AirgasUSAHX rrTu S. Alrncda Street laAngde+CA9oo59 AlrS!..q Part Number Cylinder Numben Laboratory: PGVP Number: Gas Code: EPA PROTOCOL STAhIDARI) Reference Number:,18-40?49596&l CylinderVolunn: 162.0CF Cylinder Pressurs: 201S pSlG Valve Ouflet S90 CertmcatbnDate: JulZ5.,2tZ, Dats: Co'tflcen prtumrd h md.cr $h..SeU.q.+q.tyffiffiffiffi,g3o r_;""m"a.@{itr6rr*r""uorr,q/Hulrc.dak*ve.d&duer*riiruo,ceta,uac#.it"rl-e,!;-dirffir,iffi;i;il;ffij#ffi;;Hffi#HffiHffii,ffi" molr/hdc br.b unl$r ofi!iltsr,pbd. CERTIFICATE OF AhIALYSIS Grade of Product: E03N!56E15A1055 cc21763 124 - Los Angetes (SAp) - CA 8,32022 CO2,02,BALN Rcqucctcd Goncanffion A}*A#rflC'ALRESI LT]S '- =.-"* zL@* 22.@* Babnco +/-0.6%NISTTrffi +/-0.3tt NlSTTrMle LotlD Cyllnd.rilo Conc.ntrrton Unc.]t toty NTRM NTRII 12061540 1XfrMN cc,3si{m cf3,d]tffit +r- 0.696 +l-02cfi ANALYIIANL EQTIIPME}IT SIEMENS 6E CO2 SIEMENS OXY}IAT6 Trlad D& Avr[aHc Upon R.$Et 150 of 166 @uostarfiHtfl of t CERTIFICATE OF AI\ALYSIS Grade of Product: EPA PROTOCOL STANDARD MOSTARDI PLATT, E02At99El 5 4'.1734 cc140776 124 - Pasadena (SG06) - TX A32022 PPN,BALA Airgas. an Air Uquide company Airgas Specialty Gases Airgas USA LLC 98ro BAYAREABLVD Pasadena, TX 75o7 Airgas.com Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: Certification Date: 163-402353480-1 146.2 CF 2015 PSIG 590 Feb 22,2022 Expiration Date: Feb 22,2030 Certmcation performed in accordance with 'EPA Traceabilily Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)' document EPA 6OO/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated balow with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture- All concentrations are on a mole/mole basis unless othenrvise noted. Do Not Use This below 100 osio. i.e.0.7 Triad Data Available Upon Request Sionature on file Project No. trl&Prged for Release Main Kiln Stack ANALYTICAL RESULTS Actua! Protoco!Concentration Method PROPANE 1O.OO PPM 9.902 PPM AIR Balance G1 +l- 1.4o/o NIST Traceable 0212U2022 CALIBRATION STANDARDS No Concentration NTRM 17061006 ND61234 49.13 PPM PROPANE/AIR +l-0.40/o Jul 24,2023 AIYALYTICAL EQUIPMENT Analytical Principle C3H8-XL-N ICOLET iSsO AUP2O1O248 FTIR Feb20,2022 15'l of 166 @Mostardi PFSge I of 1 CERflFICATE OF AIVALYSIS Grade of Product: MOSTARDI PLATT, EO2AI99E15AO1H9 cc733760 124 -Paeadena (SG06) - TX 13,2023 PPN,BAI-A 1ffigas. an Alr Liquidc company Custornen Part Numbel: Cylinder Number: Laboratory: PGVP Number: Gas Code: Alrrlr speddtyGeccc AirgasUSALI,C 98To BAYAREABLT/D Pasadena, TXZSoz Airlu.com EPA PROTOCOL STAI{DARI) Referene Numben 16U0267776*1 CyllnderVdume: 146.0CF Cylinder Pmssure: 2015 PSIG Valve Outet 590 CertificationData: Mar24,2023 Date: Clmcetbn perbmreO ln mdanccwlh'EPATrmrbilty fficdforAgyud Cgdlcdon dcrour Cahrlton Stendadr 0iery2012)'do<ltmort EPA 6qlR-lzlxrt. u*E fio arqay pooodurlr lbbd. Analyd0d lu€&odology docE not ro$dr! aonlcfron b andidcal mcrb'lncc. Thh qllndcr har a bbl analytlcrl unc..ffiy E ttdrd b.low wlur . conlucnc. lcvol d 9li%. Thoo er! no rtr{llcfl hrp.Jdhr llddr dt d th. u!. of ttdt calbraUon mlxurc. AI cono.rlr.llorE ar! o.r I moHooabd.-rrltrr-0&lf'i&a lpbd-Il}3 rqq&l Ghta gdy h.Jh. lqm bqhd" IDo t{ot t,!b Thh c!,{ndd bdox, l0o Tdad DdArallable Upon Request Project No. M2325124 Main Kiln Stack AIYALYTICAL REST'LIS Actual Pr6cdGoncentrrtlon tothod PROPAI{E 2O.OO PPM I9.9{i PPM AIR Balance Gt +l-1.o% NlsTTraceable 03n4mn CALIBRATION STAITDARDS LotlD OrllnderNd Concenffion, NTRII ,8068-12 61620701 29.99 PPM PROPN,IEAIR +14.1'lc Jtn 14,2025 ANALYMC.AL EQUIPMENT c3lt8fi.t tcotET ts50 AUP20 r 0248 FTIR Mat?il,zoz3 Approved for Release 152 of 166 @Mostardi Pl$rgo t of t Airgas. an Air Liquide company Airgas Specialty Gases Airgas USA" LLC rrTrr S. Alameda Street los Angeles, CA 9oo59 Airgas.com Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: CERTIFICATE OF A]\IALYSIS Grade of Product: EPA Protocol E02Ar99E15A0705 E80086790 124 - Los Angeles (SAP) - CA 832021 PPN,BALA Expiration Date: Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: Certification Date: Mar 22.2029 48-402058889-1 146.2 CF 2015 PS|G 590 Mar 22,2021 Certification performed in accordance with 'EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)' document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confldence level of 95%. There are no signilicant impurities which affect the use of this calibration mixture. All concentrations are on a Triad Data Available Upon Request Sionature on file Project Nord,PPtOfgSd for Release Main Kiln Stack mole/mole basis unless otherwise noted. Do Not Use This Component Requested Concentration ANALYTICAL RESULTS Actual ProtocolConcentration Method Total Relative Uncertainty Assay Dates PROPANE 3O.OO PPM 30.06 PPM G1 +l- 0.60/o NIST Traceable 0312212021 AIR Balance CALIBRATION STANDARDS Type Lot lD Cylinder No Concentration Uncertainty Expiration Date NTRM '16061117 E80081910 50.06 PPM PROPANE/AIR +l-0.50/o Jul 26,2022 InstrumenUMake/Model AIVALYTICAL EQI IIPMBNT Analytical Principle Last Multipoint Calibration MKS FTIR C3H8 01833582,1 FTIR Mar 09,2021 153 of 166 Pa$}10daa88m058889-1 lituas. en Aruqlld! oofiiprry Part Number: Cylinder Number: Laboratory: Analysis Date: Lot Number: .tUrCrr Spedal$ carer Airgas USAtrc uru S. Alam€da S.treet LosAqeles, C,rt9oo59 Arrta,com CERTTFICATE OF AI\IALYSIS GrAdC Of PrOdUCh CERIIEIED STAAIDARD-SPECx02Nt99crsAl268XCOeSS_gii-.,-*_ Refercnce Number: 4g{[)*fitzi3l1 ff:*;;weres(sAp)-cA .S,filriig:ffi, i*;'r$;''-$,ioiii;X,.l vrlve ouiler 3s0 Explnrton Date: Aug Ol, ZOSO Produd compo$tbn rcr,fied Or r,rO F______ Gas Mi:rrfire,€ftrence materhls. Component Req Gone ATYATM Analytical Uncertainty Actual Concenhrfion ([oh t6) ET}IYLENE 100.0 PPM BahnceNIIROGEN 100.2 PPM +t-2% OMostardi Platt P.gplotl Proiect No. 1 54 of 166 Main Kitn Stack Approved for Reteass [i]ga$. m AlrLhuldc cqnpany efrgs Spedrttycacc, AiryasUS&IIC 6Ur Eastoo Boad Bldg2 Plumsteadvile PA18949 Airyas.com CERTIFICAIE OF AI$ALYSE Grade of Product: CERTIFIED STANDARD-SPEC Part Number: Cylinder Number: Laboratory: Analysis Date: Lot Number x03Nt99C15\4,0045 cc510322 124-Plumsteadvilh-PA Nov 10,2021 Rebrence Numben Cylinder Volume: Cylinder Pressure: Valve Ouflet: 16040,?272370.1 129.6 Cubic Feet 1800 PSIG 330 16040?272370-1 Expiraffon Date: Nov {0,2023 Product compositlon veriffed by direct omparison to calibraton standards traeaHe to N.I.S.T. weights and/or N.I.S.T. C'as Mirfure reference materlals. Component AI{ALI.ITCAL RESIILTS Req Conc ActualConcentration (I{ole %) Analytical Uncertainty SULFUR HDGFLUORIDE HYDROGEN CHLORIDE NITROGEN 5.0@PPM 50.00 PPM Balance 5.000 PPM 47.92PPM +r-5% +l-2Yt P.go I ot l60402ZI?it7O-1 @Mostardi PlattProject No. Main Kiln Stack for Release 155 of 166 *"*"--...-. Appendix l- Mercury Analyses and QA Data Project No. M232512A Main Kiln Stack 156 of 166 @Mostardi Platt Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 6/20/2023 Description Area Maximum Time Std_100n9 HP 19000 Std_50n9 HP 9690 Std_25ng HP 5130 Std_250ng HP 48400 Std_10n9 HP 1990 Std_SOng RICCA ICV 9100 AGC Leamington Kiln Run 1a Section 1 2890 Run 1a Section 2 79 Run 1b Section 7 2870 Run 1b Section 2 160 Run 2a Section I 28tO Run 2a Section 2 82 Run 2b Section 7 2700 Run 2b Section 2 48 Std_25ng CCV 4620 Run 3a Section 1 2800 Run 3a Section 2 l0 Run 3b Section 7 2620 Run 3b Section 2 ll0 Run 4a Section 1 3990 Run 4a Section 2 7L Run 4b Section 1 8250 Run 4b Section 2 28 Std_25n9 HP 4690 Run 5a Section 1 5730 Run 5a Section 2 89 Run 5b Section 1 10600 Run 5b Section 2 tLB Run 6a Section 1 6190 Run 6a Section 2 66 Run 6b Section 1 10300 Run 6b Section 2 IOL Std_25n9 HP 4530 Run 7a Section L 5740 Run 7a Section 2 25 Run 7b Section 1 5930 Run 7b Section 2 87 Run 8a Section L 4730 Run 8a Section 2 12 Run 8b Section 1 4800 Run 8b Section 2 4 Std_25 ng HP 4580 Run 9a Section L 3720 Run 9a Section 2 36 Run 9b Section 1 3980 Run 9b Section 2 25 Blank -2 Run 10a Section 1 3850 Run 10a Section 2 87 Run 1Ob Section 1 4000 Run 10b Section 2 67 Std_25ng HP 4810 1800 78L 425 4770 160 715 253 3 99 t4 143 4 L28 3 449 246 1 247 5 335 2 584 19 328 68s 6 594 6 662 4 961 6 453 651 4 605 5 555 2 381 3 4t9 424 2 381 3 0 447 727 406 3 765 9:37:44 AM 9:40:13 AM 9:42:30 AM 9:44:43 AM 9:47:36 AM 10:15:38 AM 10:18:43 AM 10:20:49 AM 10:23:17 AM 10:25:25 AM 10:54:18 AM 10:55:12 AM 10:58:27 AM 11:00:22 AM 11:04:16 AM 11:51:42 AM 11:53:40 AM 11:58:14 AM 12:00:17 PM !2:22:!8PM t2:24:2LPM 12:28:50 PM 12:31:03 PM L2:36:22PM 12:55:25 PM 12:58:32 PM 1:02:34 PM 1:04:32 PM 1:31:54 PM 1:33:49 PM 1:37:21 PM 1:39:13 PM 1:41;39 PM 2:22:35 PM 2:24:40PM 2:28:55 PM 2:30:52 PM 2:58:22PM 3:00:26 PM 3:06:01 PM 3:08:05 PM 3:10:51 PM 3:34:56 PM 3:35:53 PM 3:41:40 PM 3:43:36 PM 4:19:11 PM 4:21:38 PM 4:23:38 PM 4:27:32PM 4:30:01 PM 4:32:43 PM Project No. M2325124 Main Kiln Stack '157 of '166 @Mostardi Platt Project#: M232512 Client: Ash Grove Cement Company Facility: Leamington Cement Plant Analyzer lD: 1423 METHOD 3OB CALIBRATION SUMMARY Location: Condition: Data Taken By: Main Kiln Stack Mill On SMcG Calibration lD:CAL{1 Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (7o) 100 19000 98.33 'l.670/o 50 9690 50.15 0.30% 25 5130 26.55 6.20% 250 48400 250.47 0.19% 10 1990 10.30 3.00% Slope 0.005175 0.00500 RSquared:0.999860 Enter Lowest Calibration Point Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (%) 10 't990 9.95 0.5oo/o lndependent Galibration Verifi cation Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (ohl 50 9100 47.09 5.82o/o Continuing Galibration Verifi cation Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (ohl 25 4620 23.91 4.360/o 25 4690 24.27 2.92o/o 25 4530 23.44 6.24o/o 25 4580 23.7 5.20o/o 25 4810 24.89 0.44% FT-008 Hg Template Project No. M232512A Main Kiln Stack v5.0 158 of 166 't0t31t17 @Mostardi Platt Project#: ?0232512 Cllent: Agh Grove Cement Company Facility: Leamington Cement Plant Analfzer lD: 1423 METHOD 3OB TEST RESULTS v5.0 159 of 166 Location: Main Kiln Stack Condltlon: Mill On Data Taken By: SMcG FT-008 Hg Template Project No. M2325124 Main Kiln Stack 10131117 @Mostardi Platt Cal Curve Run lD Trap lD Section )hio Lumex Response (Area) Hg Mass (ns)Cal Curvo Run lD Trap lO Section )hio Lumax Response (Area) Hg Mass (ns) cAL-o1 1A o1607094 l-SamDlo 2890 15.0 cAL-01 7A oLCl 82607 1-Semble 5740 29.7 2-Breakthrouoh 79 0.4 2-Breakthrouoh 25 0.'l cAL-o1 'lB oLc'182028 1-Samole zato 't4.9 cAL-01 7B oLc122435 l€amole 5930 30.7 2-Breaklhrouoh 't60 0.8 2-Breakthrcuoh a7 0.5 cAL-01 2A oLc181888 1-Samola 2810 14.5 CAL-01 8A o1607130 1-Samole 4730 24.5 rouoh a2 o.4 .Breakthrouoh 12 o.1 cAL-01 28 o1647104 l-Samole 2700 14.0 cAL-o1 8B 01607191 'l -Samole 4800 24.E 2-Breakthrouqh 48 o.2 2€reaKhrouqh 4 oo cAL-o1 3A 01607210 l-Samole 2800 '14.5 cAL-o1 9A o1607249 I -SamDle 3720 19.3 Z-Breakthrouoh 10 01 2-Br6akthrouqh 36 o2 cAL-o1 3B o1649725 l-SamDle 2620 13.6 cAL-o1 9B o1607096 I -Samole 3980 20.6 Z-Breakthrouoh 110 0.6 Z-Breakthrouqh 25 cAL-01 4A oLM7147 t-Samole 3990 20.6 cAL-o1 10A 01647045 I -Samole 38s0 '19.9 2-Breakthrouoh 1 o.4 2-Breakthrouqh 87 0.5 cAL-o1 48 oLc't56189 l-Sample 4250 42.7 cAL-o'l 10B oL607247 l-Sample 4000 20.7 2-Breakthrouoh 2A 0.1 2-Breakthrouoh 67 0.3 cAL-o1 5A 01607152 1€amole 5730 297 2-Breallhrouoh 89 0.5 cAL-o1 5B o1c156360 1-Sample 10600 549 2-Breaklhrouoh 114 0.6 cAL-o1 6A 01607149 1-Samole 61 90 32.0 2-Breakthrouoh 66 0.3 cAL-01 6B o1c175835 'l €amolo 10300 s3.3 2-Breakthrouqh 'to'l 05 FT-008 Hg Template Project No. M232512A Main Kiln Stack Method 30B Spike Recovery Summary Leamington Cement Plant Main Kiln Stack v5.0 160 of 166 10t31t17 @Mostardi Platl Test Run Date Start Time End Time AGIUat ConcGnlration. no Expecleo uprxe Concentration. no Recovew o/o 4A 6t20t2023 9:35 10:05 21.0 N/A 25.059 86.914842.8 25 25.147 5A 6120t2023 10:12 '10:42 30.2 N/A 25.022 101.03 5B 55.5 25 25.056 5A 6120t2023 10:48 '1't:18 32.3 N/A 24.935 8s.91 6B 53.8 25 24.953 Spike RecoveryAverage, % 91.28 Ohio Lum6x - Analytical Bias Test Analtzer No. 1423 IUinimum Mass Sample Determination Test Run Test Time Fraction ACrUat Concentration, nq EIPesrsq aPric Concentration, nq Recovery ol ,|8:38 Hq'10 10 't00.00 2 8:44 Hg"10 10 100.00 3 8:49 Ho'10 10 100.00 1 8:41 HgClz 10 10 100.00 2 8:47 HgCl2 10 10 100.00 3 8:5'1 HgCl2 10 10 100.00 0.000 0.000 o LOD = 3-o Maximum Mass Samole Determination Test Run Test Time Fraction Actual Concentration. no Expected Spike Concentration. no Recovery o/o 1 9:32 H(1 960 2000 98.00 2 9'.41 Hr 1 930 2000 96.50 3 9:51 H(2010 2000 100.50 1 9:38 HgClz 1980 2000 99.00 2 9:47 HgCl2 1940 2000 97.00 3 9:55 HgCl2 1 950 2000 97.50 Prcject No. M2325124 Main Kiln Stack 161 of 156 OMostardi Platt tphHH 7221 lnvestment Drive . North Charleston, SC 29418 843.767.7900.info@highpuritystandards.com.www.highpuritystandards.com Product Description: Product Number: Lot Number: Matrix: Density: Certilied Value: BWWH ACCiEDI'EO _---I- mgmE6 ISO '17034:2016 (RMP) Accreditation Certifi€te Number AR-'1436 Ag7 Al <0.4 As na Au <0.02 B<l Ba <0.02 Be <0.02 Bi <0.02 Ca <l cd <0.2 Ce <0.02 Co <0.05 Cr <0.05 Cs na Shipped Date: Expiration Date: Certificate Issue Date: Cu <0.02 Dy <0.02 Er <0.02 Eu <0.02 Fe <1 Ga <0.02 Gd <0.02 Ge <0.02 Hf <0.02 HgM Ho <0.02 In <0.02 Ir <0.02 K<l Element Hg ltg/mL 1000 + 6 <0.02 <0.02 <0.02 <0.5 <0.05 <0.02 <3 <0.02 <0.02 <0.02 <0.02 <5 <0.02 <0.02 SRM ID 3133 -1 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0. I <5 <0.02 <0.5 <0.02 <0.02 <0.02 La Li Lu Mg Mn Mo Na Nb Nd Ni 0s Pb Pd Pr Pt Rb Re Rh Ru Sb Sc Se si Sm Sn Sr Ta Tb Te <0.02 Th <0.02 Ti <0.02 Tl <0.02 Tm <0.02 u <0.05 v <0.05 w <0.02 Y <0.02 Yb <0.02 Zn <0.02 Zr <0.02 Packaging and Storage Conditions: The standard is packaged in a pre-cleaned polyethylene bottle. To maintain the integrity ofthis product, the solution should be kept tightly capped and stored under normal laboratory conditions. Expiration Information: The expiry date is guaranteed to be valid for eighteen months from the shipping date provided and is guaranteed through the month of expiration. For this reason, standards from the same lot may have different exptation dates. October 2022 April30,2024 J.uly 21,2022 m-t" Tf\ufufuww Moven Mututuvari, Ph. D, VP Manufacturing ReviriilUsQardi Ptatr Page I of2 @efiittcste of flnil[yrir Certified Reference Material Mercury 100033-l-100 22tE940-100 2% HNO3 1.012 gtnJ- + 0.002 elllaL @ 21.6oC t 0.3oC The Certified value is based on gravimetric and volumetric preparation, and verified against NIST SRM 3100 series when available via inductively coupled plasma optical emission spectrometry (ICP-OES) and/or inductively coupled plasma mass spectrometry (CP-MS) using an internal laboratory-developed method. The uncertainty in the certified value is calculated for a95Yo confidence interval and coverage factor k is about 2. * Refer to Traceability lnformation, Section 4 Uncertified Values: Trace Metal Impurity Scan: The data reported are based upon a scan of this specific lot via ICP-OES/ICP-MS analysis. The values are reported in pgll-. L$l8HBh${b?11921&.l* lf,milflmffinl[ilr 162 of 166 Preparation Information: This Certified Reference Material is prepared using 99.99930/o pure Mercury Metal which was purchased from a qualified vendor per ISO 9001 guidelines and assayed by analytical methods for conformity prior to use. This standard was manufactured under appropriate laboratory conditions using the methods developed at NIST for SRM Spectrometric Standard Solutions. Sub-boiling distilled high-purity acid has been used to place the materials in solution and stabilize the standard. The matrix is as noted above in l8 megaohm deionized water. Stability of this product is based upon rigorous short-term and long-term testing of the solution for the certified value. This testing includes, but is not limited to, the effect of temperature and packaging on the product. If, during the period of validity, a recall is instituted due to substantial changes in the stability of this product, the purchaser will be notified. Ifomogeneity: This product is determined to be homogeneous following in-house procedures developed in accordance with the requirements of ISO 17034 and ISO Guide 35. Intended Use: This product is intended for use as a calibration standard, quality control standard, and/or for the validation of analytical methods. The standard is confirmed homogeneous; therefore, the minimum sample size should be consistent with the end user's measurement capabilities. Traceability Information: The traceability of this standard is maintained through an unbroken chain of comparisons to appropriate standards with suitable procedure and measurement uncertainties. The maintenance of the base and derived units of lntemational System of Units (SI) with traceability of measurement results (contemporary metrology) to SI ensures their comparability over time as follows. 1. Standard Weight and Analytical Balance The standard weights (NBS weights Inventory No 20231A) are calibrated every two years by South Carolina Metrology Laboratory that is a participant in TIIST Weights and Measures Measurement Assurance Program' with a certificate of measurement traceability to NIST primary standards. The balances are calibrated yearly by the ISO 17025 acuedited metrology service, and are verified weekly by an in-house method using standard weights. 2. Volumetric Device The calibrations of volumetric vessels are verified using the ASTM method E542. 3. Thermometer The standard thermometers are calibrated every year by the ISO 17025 accredited metrology service. The thermometers used in-house are verified against the standard thermometers yearly. 4. CalibrationStandards The Calibration Standard is traceable to SRM 3100 Series Spectrometric Standard Solutions. If an SRM is not available, a second source standard or independent lot is used. Refer to Safety Datasheet (SDS) for hazardous information. NOTICE: HPS products ile intended for laboratory use only. All products should be handled md Ned by trained professional persomel. The responsibility for the safe hmdling md use of these products rests solely with thc buyer md/or user. The data and infomation 6 stated was fumished by the manufactuer of the product. The infomation provided in this certificate pertains only to the lot number specified. None ofthe infomation provided in this certificate may be used, reproduced or trmsmitted in my fom or by any mems without uitten approval ftom High-Purity Stardtrds. Rev{iiffibQardi Ptatt Page 2 of 2 163 of 166 m RrccA cHEMTcAL coMPANY' -Certificate of Analysis 1490 Lammers Pike Batesville, IN 47006 http :7***.riccachemical. com 1-888-GO-RICCA customerservice@riccachemical. com Mercury ICP Standard, 1000 ppm Hg in 8% HNO, Int Numberz 42OgD27 h,oduct Nunber: PHGlKN Manufacture Date: SEP L4, 2022 &pirationDatd MAR 2024 The certified value for this product is confirmed in independent testing by a second qualilied chemist. The uncertainty associated with the certifiec value is + 0.5% relative, which is the sum of the estimated errors due to the purity of the raw material, the volumetric preparation of the solution,and transpiration of the solution through the container wall. The final solution concentration is confirmed by AA, ICP, or ICP'MS, and is traceable to NIST Standard Beference Material 3133. All trace Ievel elements were determined by ICP or ICP-MS. Water Nit"i" a.ia Mercury 7732-18-5 7697-37-2 7439-97-6 Appearance Assay (vs. Potassium Thiocyanate/Volhard's cqlqrlqry liqqi.4 . 995-1005 ppm Hg Beqqs4... " 1000 ppm Hg 999 Indicator) Trace Elements by ICP or ICP'MS All values reported in mgll, (ppm) Iron (Fe)< 0.001 ppm Lanthanum(Ld 0.0001ppm I=Spectral Interference N=NotTested Aluminum (Al) Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Bismuth (Bi) Boron (B) Cadmium (CO Calcium (Ca) Cerium (Ce) Cesium (Cs) Chromium (Cr) Cobalt (Co) Copper (Cu) Dysprosium Oy) Erbium (Er) Europium (Eu) Gadolinium (Gd) Gallium (Ga) Germanium (Ge) Gold (Au) Hafnium (H0 Holmium (Ho) Indium (In) Iridium 0r) < 0.0009 ppm 0.0666 ppm 0.0022 ppm < 0.0001 ppm 0.0017 ppm 0.0082 ppm I 0.0373 ppm N < 0.00003 ppn 0.0061ppm < 0.00006 ppn < 0.00002 ppn < 0.00005 ppn < 0.0001 ppm N 0.0001ppm < 0.0002 ppm 0.0022 ppm 0.0096 ppm < 0.0005 ppm 0.0044 ppm < 0.0001 ppm < 0.00003 ppn < 0.00007 ppn Lead (Pb) Lithium (Lil < 0.00003 ppn < 0.03 ppm Silver (Ag) Sodium (Na) Strontium (Sr) Sulfur (S) Tantalum (Ta) Tellurium (Te) Terbium (Tb) Thallium (Tl) Thorium (Th) Thulium (Tm) Tin (Sn) Titanium (Til Tungsten (W) Uranium (U) Vanadium (V) Ytterbium (Yb) Yttrium (Y) Zinc (Zn) Zirconium (Zr) 0.1710 ppm < 0.02 ppm < 0.00006 ppn I 0.0140 ppm 0.1464 ppm N 0.0802 ppm 0.0035 ppm 0.0001ppm 0.0014 ppm < 0.001 ppm 0.0541 ppm 0.0004 ppm < 0.00004 ppn < 0.001 ppm < 0.00009 ppn < 0.0003 ppm 0.0653 ppm Lutetium (Ld < 0.0003 ppm Magnesium (Mg) < 0.0007 ppm Manganese (Md o.oo25 ppm Molybdenum (Mo) 0.0203 ppm Neodymium (N0 < 0.0002 ppm Nickel (Nil < 0.0001 ppm Niobium (Nb) 0.0011ppm Osmium (Os) < 0.003 ppm Palladium (PO 0.0503 ppm Phosphorus (P) < 0.02 ppm Platinum (Pt) 0.01?1 ppm Potassium (K) N Praseodymium (Pr) N Bhenium (Re) < 0.00003 ppn Rhodium (Rh) < 0.00003 ppn Rubidium (Rb) < 0.00004 ppn Ruthenium (Rd 0.0013 ppm Samarium (Sm) < 0.002 ppm Scandium (Sc) 0.0048 ppm Selenium (Se) 0.0981 ppm Silicon (Sil < 0.007 ppm Version: 1.5 LtNumbo:4209D27 h,oductNumbc: PHG1KN 164 of 166 Page L of 2 @Mostardi PlaftProject No. M232512A Main Kiln Stack Mercury ICP Standard, 1 mL = 1 mB Hg (1,000 ppm Hg) Hg in 3% HNOs tni, "i".ra"tJ i" go"r"rri""a io be stable and ".".rrut" p"o.riaed the o."a"" ir t"o, tightiv cappetl and sto.ed under normal laboratory conditions. Balances are calibrated using MST traceable weights whose veri.fication of maintenance and recalibration is documented per in-house Standard Operating Procedures. Class A glassware is aleo calibrated and routinely rechecked per in-house Standard Operating Procedures. Tlace metal analyzed acids and Trace Metals Analyzed Water are used in the manufacture ofthis product. Triple cleaned containers are used in the manufacture of this product. EPA (200.7) PHGfKN l9q Recommmded Storage: 15oC ' 30oC 100 mL natural LDPE 18 months (59"F - 86.F) ,QeA^"t'-- Paul Brando n @g t tU zozz) Production Manager This Certificate of Analysis is designed to comply with ISO Guide 31 "Reference Materials -- Contents of Certificates and Labels." This test report shall not be reproduced, except in full, without the written approval ofRicca Chemical Company. IatNnnbc:42O9D27Version: 1.5 Project No. M2325124 Main Kiln Stack hroductNunbe: PHG1KN 165 of 166 Page2 of 2 @Mostardi Platt END OF THE REPORT .. TAH DEPARTMENT OFENVIRONMENTAL QUALITY Ai,r; ,ri :r.j DIVIS,ON OF AIR QUALITY Project No. M2325124 Main Kiln Stack @Mostardi Platt