DAQ-2025-002502

1

DAQC-463-25
Site ID 11532 (B4)

MEMORANDUM

TO: STACK TEST FILE – MOUNTAINWEST PIPELINE, LLC

THROUGH: Harold Burge, Major Source Compliance Section Manager

FROM: Robert Sirrine, Environmental Scientist

DATE: May 14, 2025

SUBJECT: Source: Waukesha L7044GSI CE ICE-4 (Unit #9)
Location: Kastler Marushack Compressor Station, Daggett County, Utah
Contact: Dani Baldwin, 801-201-0595
Tester: Oasis Emission Consultants, Inc. Chris Knott 307-382-3297
FRS Site ID #: UT0000004900900001
Permit #: Title V permit 900001005, dated September 26, 2022, last revised
October 31, 2023
Subject: Review of Pretest Protocol dated May 6, 2025

On May 9, 2025, the Utah Division of Air Quality (DAQ) received a pretest protocol for the
MountainWest Pipeline – Kastler Marushack Compressor Station Waukesha L7044GSI CE ICE-4 (Unit
#9) located in remote Daggett County, Utah. Testing will be performed on June 11, 2025, to demonstrate
compliance with emission limits found in EPA 40 CFR 60, Subpart JJJJ and permit Conditions II.B.4.a
and II.B.4.b for NOX, CO, and VOC defined as NMHC emissions.

PROTOCOL CONDITIONS:

1. RM 1 used to determine sample velocity traverses: OK
2. RM 2 used to determine stack gas velocity and volumetric flow rate: OK
3. RM 3A used to determine dry molecular weight of the gas stream: OK
4. RM 4 used to determine moisture content: OK
5. RM 7E used to determine NOX concentrations of emissions: OK
6. RM 10 used to determine CO concentrations of emissions: OK
7. RM 18 used to determine VOC NMNEHC concentrations of emissions: OK
8. RM 25A used to determine VOC concentrations of emissions: OK

* - / $ - - $ )
2

DEVIATIONS: None.

CONCLUSION: The pretest protocol appears to be acceptable.

RECOMMENDATION: Send protocol review and test date confirmation notice.

HPV: No.

ATTACHMENTS: Pretest protocol dated May 6, 2025.
winiffii.
Vio Certilied Moil MountainWest Pipeline, LLC
650 South Main Street, 3'd Floor
Salt Lake City, Utah 8410 I
5EP:F:A-Rr-MENI-9i
ewrfiourclru ql^tnY
llAY - I 2025
uYlsm of An oJrrfl
RE:
May 6, 2025
Utah Division of Air Quality
Attn: Director, NSR Section
P.O. Box 144820
salt Lake city, UT 841L4-4820
MountainWest Pipeline. LLC
Kastler Marushack Compressor Station
Title V Operatine Permit Number 900001005
Performance Test Notification for the ICE-4 Ensine
Dear Mr. Bird:
The purpose of this correspondence is to provide notification that Kastler Marushack Compressor
Station will be conducting a performance test on the Waukesha 7044GSl engine, ICE-4. Nitrogen
oxides (NOx), carbon monoxide (CO), and volatile organic compounds (VOC) emissions testing
will be performed in accordance with both the Operating Permit Number 900001005 and 40 CFR
60 (NSPS) Subpart JJJJ. The performance test is scheduled for June 7L,2025, between the hours
of 7:00 A.M. and 7:00 P.M. However, in the event of unforeseen circumstances, or as operational
conditions dictate, testing may extend past 7:00 P.M.
Questions regarding this submittal should be referred to
dani.baldwin @williams.com.
Sincerely,
Baldwin at [phone] or
Dani Baldwin
Environmental Specialist
Enclosure
Utoh Deportment of Environmentol Quolity
Division of Air Quolity
Source Test Protocol
Title V Operoting Permit # 900001005
ond EPA 40 CFR 60 (NSPS), Subport JJJJ
Engine: Woukesho [7044GS1
Compressor Engine
Compony Unil ID: Pork & Loon (Unit #9)
Permil Unit lD: ICE-4
MountoinWest Pipeline, [[C
Kostler Morushoc k Compressor Stolion,
Doggett County, Uloh
April 22,2025
Prepored By:
Oosis Emission Consultonts, lnc.
2730 Commerciol Woy
Rock Springs, WY 8290,|
UTAH DFPARTMENT OF
ENVIRONMENTAL QUALITY
CERTIFICATION STATEMENT
This statement certifies that "to the best of their knowledge," based on State and Federal
regulations, operating permits, plan approvals applicable to each source or control device to be
tested, and reasonable inquiry, the statements and information presented in the attached
document are true, accurate, and complete. If the information herein is found to be inaccurate or
incomplete by any participant, the protocol will be reviewed and all reasonable measures will be
taken to make necessary changes.
WAUKESHA L7O44GSI COMPRESSOR ENGINE
COMPANY UNIT ID: PARK & LOAN (UNIT #9) / PERMIT UNIT ID: ICE-4
CONTINUING COMPLIANCE TEST PROTOCOL
MOUNTATNWEST PIPELINE, LLC
KASTLER MARUSHACK COMPRESSOR STATION / DAGGETT COUNTY / UTAH
Name: Shawna O'Brien
Title: Sr. Environmental Scientist
Signature:
Daz) Ea.Urrit
Date: Aoril22nd.2025
Company: Oasis Emission Consultants. Inc.
5t612025
Dani Baldwin
Environmental Special ist
MountainWest Pipel ine, LLC
Date
APPENDIX A:
APPENDIX B:
Example Calculations
Sample Calibration Sheets
1.0 lntroduction
The purpose of this document is to provide relevant information pertaining to proposed periodic
emissions testing at MountainWest Pipeline, LLC's Kastler Marushack Compressor Station
(Company Unit ID: Park & Loan (Unit #9); Permit Unit ID: ICE-4) in Daggett County, Utah.
Emissions testing will be conducted in accordance with Utah Department of Environmental
Quality (UDEQ) Title V Operating Permit # 900001005 (lssuance Date: September 26,2022,
Date of Last Revision: October 3l,2023) and EPA 40 CFR 60, Subpart JJJJ (I{SPS Subpart
JJJJ). Testing will be conducted by Oasis Emission Consultants, Inc.
1.1 Test Program Organization
Title V Operating Permit:
Federal Regulation:
Facility / Location:
Permit ID:
900001005
EPA 40 CFR 60. Subpart JJJJ
Kastler Marushack Comnressor Station
The Kastler Marushack Compressor Station is located in Section
16, Township 3N, Range 24F,, in Daggett County, Utah.
UTM Coordinates: 650,257 m Easting, 4,539,784 m Northing
ICE-4: Internal Combustion Engine- Controlled
The pipeline quality natural gas-fired Waukesha L7044GSI,
four stroke rich burn (4SRB), reciprocating internal combustion
engine (lCE) is rated at 1,680 horsepower (hp). The engine is used
to compress gas and is equipped with a NSCR catalyst. The engine
was manufactured in2022 and is subject to the test requirements
listed in NSPS Subpart JJJJ 60.4243(bx2xii). Additionally, the
Waukesha L7044GSI is located at a remote area source of HAP
under EPA 40 CFR 63, Subpart ZZZZ (NESHAP Subpart ZZZZ).
The owner / operator must comply with NESHAP Subpart ZZZZby
maintaining the engine according to the requirements of Subpart
ZZZZ Table 2d Condition I l.
Client Owner / Operator:
Address:
Contact:
Email:
Cell.:
650 S. Main Street, 3rd Floor
Salt Lake city, UT 84101
Dani Baldwin, Environmental Specialist
Dani.Baldwin@wil liams.com
(80r) 201-Oses
Test Company:Oasis Emission Consultants. Inc.
Address: 2730 Commercial Way
Rock Springs, WY 82901
Contact: Chris Knott, P.Eng., Director, Engineering & Operations
Phone: [phone]
Fax: [phone]
MW Servicesl
Address: 4980 State Highway 374
Green River, WY 82935Phone: (307\352-7292
Utah Department Of Environmental OualiW
Address: PO Box 144820
Salt Lake ciry, uT 84114-4820
Contact: Rik Ombach, Minor Source Compliance ManagerEmail: [e-mail]: [phone]
Stack Test Report Submission:
https://utahgov.co I .qualtrics.comljfelformlSV_3dSxfTJSzy4jwGh
Laboratory:
State Authority:
I MW Services will only be utilized if Method l8 Gas Chromatography is deemed necessary to determine the ethane
concentrations for the measurement of VOC (as NMNEHC).
1.2 Test Project Objective(s)
The purpose of the periodic emissions compliance demonstration is to satisfy the requirements of
UDEQ Title V Operating Permit # 900001005 (lssuance Date: September 26,2022, Date of Last
Revision: October 3l ,2023) and NSPS Subpart JJJJ. According to Condition II.A.5, the internal
combustion Waukesha L7044GSI engine is permitted as Unit ICE-4. The engine has the
Company Unit lD of Park & Loan (Unit #9).
As required by the UDEQ Operating Permit # 900001005 Conditions II.B.4.a.l, II.B.4.b.l and
NSPS Subpart JJJJ, testing to demonstrate ongoing compliance will be conducted for nitrogen
oxides OO*), carbon monoxide (CO) and volatile organic compounds (VOC), defined as non-
methane hydrocarbons QTIMHC) emissions. Three, one hour test runs for NO*, CO and VOC will
be conducted using EPA Test Methods l-4,7F,,10 and 25A with a Hydrocarbon Cutter. EPA's
Method l8 may also be employed to account for ethane levels. If Method l8 is employed, VOC
levels will be reported as non-methane, non-ethane hydrocarbons (NMNEHC). Testing to
demonstrate compliance with the permitted limits and the NSPS Subpart JJJJ standards will be
conducted concurrently.
The WaukeshaLT044GSI natural gas-fired 4SRB engine (Park & Loan (Unit #9); ICE-4) has a
maximum horsepower of I ,680. In accordance with 40 CFR 60.4244(a), it is expected that the
performance test will be conducted within +109io of 100% peak, or the highest achievable load.
The actual tested horsepower will be included in the test report. As stipulated by UDEQ
Operating Permit # 900001005 Conditions II.B.4.a.l.l(e) and II.B.4.b.l(e), the production rate
during all compliance testing will be no less lhan90o/o of the maximum production achieved in
the previous three years.
The test report will show results in accordance with NSPS Subpart JJJJ Table I and Table I
Footnote a. Footnote a allows owners and operators of stationary non-certified SI engines to
choose to comply with the standards in units of either grams per brake-horsepower hour (g/Bhp-
hr) or units of parts per million dry volume standardized to l5yo oxygen (ppmdv @ 15% O).
Results from the continuing NSPS Subpart JJJJ compliance test will be reported in ppmdv @
l5Yo Oz and g/Bhp-hr. Results to show compliance with the UDEQ Operating Permit #
900001005 limits will be reported in units of pounds per hour (lb/h$.
Process parameters expected to be collected during the performance testing include, but are not
limited to: atmospheric pressure, atmospheric temperature, engine RPM, manifold pressure,
manifold temperature, airlfuel ratio setting(s), O2%o and COz%o. The process parameters will be
recorded on the engine test sheet and provided in the test report.
1.3 Facility Description
MountainWest Pipeline, LLC operates the Kastler Marushack Compressor Station in Daggett
County, Utah. The Kastler Marushack Compressor Station is used to compress natural gas for
injection and delivery into a natural gas reservoir. The compressor station consists of
reciprocating internal combustion engines and gas turbines that are utilized to drive compressors
in the station. The station also includes the Clay Basin Dew Point (CBDP) Process Unit. The
CBDP process unit receives and processes natural gas from a storage reservoir and from the
main lines. The CBDP process unit includes an ethylene glycol regenerator, liquid hydrocarbon
loading rack and miscellaneous process stream equipment.
2.0 Source Test Program Description
2.1 Test Contractor
All source emission tests will be performed by Oasis Emission Consultants, Inc., based out of
Rock Springs and Sheridan, Wyoming. Processed test results and all raw data captured during
the tests are forwarded to Chris Knott, P.Eng., Director of Engineering and Operations and/or
Charles Chapman, Manager of Technical Services, for quality control and data checking. Once
approved, tests are forwarded to the client.
2.2Test Date
Emissions testing is currently scheduled to be conducted and completed on June 11,2025.
2.3 Time
Testing is currently scheduled to be conducted between the hours of 7:00 A.M. and 7:00 P.M.
However, in the event of unfbreseen circumstances, or as operational conditions dictate, testing
may extend past 7:00 P.M.
2.4 Report Date
The compliance test report will be submitted to the UDEQ no later than 60 days following the
compliance test.
2.5 Test Report Format
The following table illustrates the format used for reports submitted.
Table Re rtConten
Content Descrintion
Cover The cover will contain the air testing company
information, facility name and source summary.
Introduction The introduction will include the test objective
and descriptions of the source and control
equipment (as applicable).
Stack Sampling Location The stack sampling location details the sampling
site location.
Discussion of Test Results The test results provide the results for each test
run.
ts.
Stack Sampling Methods and
Procedures
The stack sampling methods and procedures will
include a detailed description of the methods
utilized in the testing process and any deviations
from the submitted protocol.
Equipment Utilization The equipment utilization provides a list of the
test equipment employed in conjunction with the
samplinq test methods.
Process Parameters Process parameters summarizes the source
parameters recorded during the test runs.
Quality Assurances Quality assurance and quality control procedures
pertaining to the methods and equipment
calibrations will be included in the emission
source test report.
Appendices The report's appendices will contain test data,
quality assurance/calibration data, example
equations and field notes.
3.0 Testing Methodology and Procedures
3.1 Permitted Limits and Standards
The purpose of the compliance test on the WaukeshaLT044GSI engine (Park & Loan (Unit #9);
ICE-4) is to demonstrate continuing compliance for NO* and CO with permit limits and the
NSPS Subpart JJJJ standards for NO*, CO and VOC. Permitted limits for each constituent and
the NSPS Subpart JJJJ standards can be found in the following tables.
3.1.1 UDEQ Title V Operating Permit # 900001005 Limits
3.1.2 EPA 40 CFR 60, Subpart JJJJ
Table 2: Source Summary and Permitted Limitations.
Permit Unit
ID
Company
Unit ID
Engine Serial Number HP Max.
Allowable
NO".
Max.
Allowable
CO
ICE-4 Park & Loan
(Unit #9)
Waukesha
L7044GSt
wAU-r 670836 1,680 3.70 tbthr 3.70|b/hr
Table 3: NSPS Subpart JJJJ Standards.
Engine Maximum
Ensine Power
Manufacture
Date
RICE
Confisuration
EPA Standard
NO'
EPA Standard
CO
EPA Standard
voc
Waukesha
L7O44GSI
1,680 HP 2022 4SRB 82 ppmdv
@'ts%02,
1.0 s/BHp-hr
270 ppmdv
@ 15o/o 02,
2.0 s/BHo-hr
60 ppmdv
@ l5o/o 02,
0.7 dBHp-hr
EPA 40 CFR 60, Subpart JJJJ Table I Footnote a allows owners and operators to choose to
comply with the emission standards in units of either g/BHp-hr or ppmdv at l5 percent 02.
Results from the periodic compliance test will be reported in ppmdv at l5%o Oz and g/Bhp-hr.
3.2 Sampling Matrix
Table 4: Sampli Matrix.
Method Title Parameter Reference Number of
Tests
EPA 40 CFR 60
Appendix A, Method I
Sample and l'elocity
Trave rse s for S tationary
Sources
Sampling Point
Determination
https ://www.epa.gov/syste
m/fi les/docum entsl 2023 -
0912023%20Fina1%20MS
o/o20o/o20 M etho do/o20 I _0 .p
df
EPA 40 CFR 60
Appendix A, Method 2
Determination of Stack
Gas llelocily and
l'olumelric Flov Rale
Stack Gas
Flow Rate
https ://www.epa. gov/s ites/
default/fi les/20 I 7-
08/doc uments/method_2.p
df
EPA 40 CFR 60
Appendix A, Method 3A
De te r minat i o n of Oxyge n
and Carbon Dioxide
Concenlrations in
Emissions From
Slationaty Sources
(lnstrumental Analyzer
Procedure)
02, Dry
Volumetric
FIow Rate
https ://www.epa.gov/sites/
default/fi les/20 I 7-
08/documents/method_3a.
pdf
EPA 40 CFR 60
Appendix A, Method 4
Determinalion Of
Moisture Contenl
In Stack Gases
Moisture
Content
https ://www.epa. gov/sites/
default/fi les/2020-
I 2/documents/method_4.p
df
3xlhr
EPA 40 CFR 60
Appendix A, Method 7E
De te rminatio n of N itroge n
Oxides Emissions From
Slationary Sources
( [ nslrttme nt al A na lyze r
Procedure)
NO*https://www.epa.gov/s ites/
default/fi les/2020-
I 2/documentsimethod_7e_
2.pdf
3xlhr
EPA 40 CFR 60
Appendix A, Method l0
De t e r mi nat ion Of C arb on
h4onoxide Emissions From
Stationary Sources
(lnstrumental Analyzer
Procedure)
CO https ://www.epa. gov/s ites/
default/files/201 7-
08/documents/method_ I 0.
pdf
3xlhr
EPA 40 CFR 60
Appendix A, Method l8-
Optional
It4 e asure me nt of G ase ous
Organic (.ompound
Iimissions by Gas
('hromalography
Ethane
Concentrations
For
Determination
ofVOC
defined as
NMNEHC
https ://www.epa. gov/syste
m/fi les/docum entsl 2025 -
04/m-l 8-040 I 2025_0.pdf
3xlhr
(Optional)
EPA 40 CFR 60
Appendix A, Method
254
(With a Hydrocarbon
Cutter)
Delermination of Total
Gaseous Organic
Concenlralion Llsing a
Flame lonization Analyzer
VOC defined
as NMHC
https ://www.epa.gov/s ites/
default/files/20 I 7-
0 8/documents/method_25 a
.pdf
3xlhr
U.S. Environmental Protection Agency. "EMC Promulgated Test Methods." Air Emission
Measurement Center (EMC). l9 March 2025. Web. 22 April2025. <https:llwww.epa.gov/
emc/emc-prom ulgated-test-methodP.
U.S. Environmental Protection Agency. "Subpart JJJJ-Standards of Performance for
Stationary Spark lgnition Internal Combustion Engines." Code of Federal Regulatio,ns. Title 40.
Chapterl. SubchapterC.Part60.SubpartJlJl.73FR359l,Jan. l8,2008.Washinglon:GPO.
l8 April 2025. Web. 22 April2025. <https:l/ecfr.federalregister.gov/current/title-40/chapter-l/subchapter-
C/part-60/subpart-J JJJ>.
3.3 Stack Sampling Location
The inner exhaust stack diameter for the WaukeshaLT044GSI was previously measured as l6
inches. The sampling ports for flow, NO*, CO and VOC measurements are approximately 2.6
pipe diameters downstream from the nearest flow disturbance and 2.4 pipe diameters upstream
from the nearest disturbance. The test location will be verified during the test program to meet
the minimum specifications of a sampling location as defined by EPA Method l. An aerial lift
will be utilized, if needed, to conduct sampling.
The WaukeshaLT044GSI engine (Park & Loan (Unit #9); ICE-4) is a rich burn engine that
employs a NSCR catalyst to regulate NO*, CO and VOC emission levels.
+_16,'______+
::l
{
tlt
Exhaustias Flou
f
I.IUFFLER
;-'ii*+NSCR
CATALYST
PORTS
EXHAUST
GAS FLO\
Figure l: Sample Location Diagram.
3.4 Emission Measurement Methodologies
Testing will be performed and calculated in accordance with EPA Test Methods l-4, 78, 10 and
25A with a Hydrocarbon Cutter. EPA's Method l8 may also be used to deduct the ethane
content of the effluent gas from the NMHC levels recorded by our analyzer. Three, one hour test
runs will be conducted on the Waukesha L7044GSI compressor engine (Park & Loan (Unit #9);
ICE-4) for NO*, CO and VOC.
3.5 Equipment Utilization
Oasis Emission Consultants Inc. will utilize the following gas analyzers and associated
equipment for this testing:
o API 300M CO NDIR Analyzer. API 2004.H NO*/Oz Chemiluminescent/Paramagnetic Analyzer
o CAI600HFID Analyzer, c/w Hydrocarbon Cuttero 75 ft. Heated Sample Line. Universal Analyzer 3040SSP Sample Gas Conditioner. Standard or S-Type Pitot Tube clw 20 ft. Heated Sample Liner Method 4 Impinger System c/w Ice Box Tray. Integrated Method l8 Collection System With Tedlar Bags (Optional)o Apex MC-170 Meter Boxo Fyrite Analyzer for Carbon Dioxide Measuremento EPA Gl Protocol Calibration Gaso Laptop Computer To Download Raw Analyzer Data
The schematics for our sampling system are shown on the following pages.
L- Chrr V--
glrrldr6.fil P.df6.VYIr fr?. IItItrEaq*
ft O.a
l(lrclqalrEror
srttir LrI
\
ff.E &r ^..-aat
a
D, Gr lL..
llrr vr.
Vrurr\G.ll. EganYar lrrp Lgry
ouAtSOjrrq,!ArO| *a*r-ltt;tarst*
t\__
EPA Mothods t,2.E 4
tampling trein schemstic
Figure 2: EPA Methods 1,2 and 4 Sampling Train Schematic.
Argr.. vrL
a
)--.--_-i_-;\l _l
l0
/'__/
CrbratimGr
7'iu,nir,t PFA Heded Sanph Line/t.
t
Wel SrrplcTo HFIO
Punp
'I
J
Oooo.rd.
T.db'B.e Enc&.rr.
I
Enemd Gr Sarrgrng Pr.rr? iArllr e Yrter :/
Vrurm / Rclrrclcr
\,
Urn Eril An hra, 3OaOSSP Serplc 6l Coneoiiar
mer*oU ne*rc Rcgi.rdo, A Prurrlrc Gu4c
i
Samd. Conlroa VrlYrf-i\;fr-. 0---._=
I ur len co ror trrq
aE lnot rGUo? chiaFda , llElil .rurE
CA ofl)}lFlo An.itr r. c/v, lt,oocrbn C{rrt t
EPA Methods 3A, 7E.1 0,t 8, & 2SA
sampling train schematic
Figure 3: EPA Methods 3A,7E,l8 and 25A Sampling Train Schematic.
3.6 Test Quality Assurance Procedures
3.6.1 Sampling Protocol
Precautions are taken to keep the gas analyzer in a clean, thermally stable, vibration free
environment to minimize analyzer drift and associated errors. Pre test calibrations and post test
operations are performed within the testing trailer environment.
Samples are taken according to EPA Methods l-4,78,10,25A and 40 CFR 60.4244 Q{SPS
Subpart JJJJ). The data from the samples are converted directly into computer language and
recorded in the Compliance Specialist's laptop computer. This eliminates the need for sample
labeling and secures the preservation of the data while reducing human error.
If Method I 8 is utilized to determine the ethane concentration for the measurement of VOC as
non-methane, non-ethane hydrocarbons (NMNE HC), the gas sample will be collected in a
Tedlar bag for the test run. The sample will be labeled with the client company's name, facility
name, test run and date. The sample bag will be properly sealed so that any evidence of
tampering may be readily observed. A chain-of-custody form will accompany the test to the
designated lab. The sample will be taken to MW Services for analysis. Each time the sample
transfer possession, the transferee will sign and record the date and time on the chain-of-custody
form.
Linearity checks are performed using certified calibration gases to ensure that the zero, mid, and
upscale calibrations are within the certified calibration level and zero. Pre-test calibrations are
then conducted on the zero and selected mid or upscale calibration gas determined by observing
the native concentration of the target analytes in the sampled exhaust. After each test run the
same zero and selected mid or upscale calibration gas are analyzed to verify they are within the
required specifi cations.
Sample times for stratification will be determined by observing the sample response time for the
oxygen to reach a stable level for low and upscale calibration gas concentrations. The time will
then be doubled and during stratification, each sample point will use this dwell time to determine
the concentration.
3.6.2 Equipment Galibration and Measurement
Preventive diagnostic functions are built directly into the equipment utilized for the testing. This
diagnostic function provides the Compliance Specialist with failure warnings allowing the
determination of when repairs are necessary without performing painstaking preventative
maintenance procedures. However, equipment is inspected regularly by the Compliance
Specialists to guarantee maximum operational status. The process involved with equipment
calibration ensures that there is no divergence from the manufacturer's specifications.
3.7 Engine Operating Parameters
Engine operating parameters, where applicable, will be recorded for each test which may include
atmospheric pressure, atmospheric temperature, engine RPM, manifold pressure, manifold
temperature, airlfuel ratio setting(s), 02% and CO2%o.
t2
3.8 Engine Load Approximation
Oasis Emission Consultants lnc. will approximate the engine load using the measured process
parameters, such as gas throughput, suction/discharge pressure/temperature; by correlating the
intake manifold conditions with the engine manufacture heat balance data; by correlating the
measured engine speed with the manufacturer's performance curve; the engine load; or, the
readings obtained from the panel.
The Waukesha L7044GSI engine has a maximum horsepower of 1,680. In accordance with 40
CFR60.4244(a), it is expected that the performance test will be conducted within +llyo of 100%
peak, or the highest achievable load. The production rate during all compliance testing will be no
less than 90% of the maximum production achieved in the previous three years.
3.9 Test Methods
Oasis Emission Consultants, Inc. will employ EPA 40 CFR 60 (A) methods as required by
UDEQ Operating Permit # 900001 005 and NSPS Subpart JJJJ. These methods are described
below.
r EPA 40 CFR 60 Appendix A, Method 1: Method I requires measurement of the various
physical attributes of a stack to establish appropriate sampling locations. An Oz stratification
check will be performed according to 8.1.2 of Method 7E prior to testing to determine
sampling location for engines with stack diameters greater than 6 inches, but less than 12
inches. For stacks equal to or greater than I 2 inches in diameter, if the sampling port locations
meet the minimum Method I criterion for distance from disturbances, sampling may be
conducted atthree points. If sampling ports do not meet Method I criterion fordistance from
disturbances,stacksequaltoorgreaterthan l2inchesindiameterwill haveanOzstratification
check performed to determine sampling locations. An Oz stratification is not required for
engines with a stack diameter less than 4 inches.
o EPA 40 CFR 60 Appendix A, Method 2: Method 2 provides the means to calculate the
average wet velocity for the exhaust effluent gas. This method employs the use of a standard or
S-type pitot tube, a thermometer and an inclined manometer. The temperature, static &
differential pressures are all used to calculate the average wet velocity. This value may be used
in conjunction with the known stack diameter, and measured moisture content, to approximate
the average dry volumetric flow rate.. EPA 40 CFR 60 Appendix A, Method 3A: Method 34, provides the means to calculate the
dry molecular weight of the effluent gas. After passing through a gas condenser, 02 gas
concentrations from the effluent stream are measured by an instrumental analyzer.
Measurements will be taken in conjunction with those from Method 2.The dry molecular
weight will be calculated for each of the test runs. The Oz levels will also be used to allow for
the correction to ppmdv at l5oh C7.
o EPA 40 CFR 60 Appendix A, Method 4: Method 4 allows for the evaluation of the moisture
content within the effluent stream. A sample of the effluent stream is extracted at a constant
rate. The water is condensed from the stream through a series of impingers surrounded by an
ice bath. The total mass of the water condensed and the total volume of gas measured are used
l3
to calculate the moisture content within the exhaust effluent stream. Moisture content will be
calculated for each of the test runs.
o EPA 40 CFR 60 Appendix A, Method 7E: Method 7E is the instrumental method for
measuring the NO* concentration in the effluent stream. After passing through a sample
conditioning system, NO* concentration is measured by a chemiluminescent gas analyzer. The
analyzer is calibrated using EPA Protocol G I gas before and after each one hour test run.
o EPA 40 CFR 60 Appendix A, Method 10: Method l0 is the instrumental method for
measuring the CO concentration in the effluent stream. After passing through a sample
conditioning system, CO concentration is measured by an NDIR gas analyzer. The analyzer is
calibrated using EPA Protocol Gl gas before and after each one hour test run.
o EPA 40 CFR 60 Appendix A, Method 18- Optionalz Method l8 may be used to determine
the ethane concentration. Method l8 employs an integrated grab bag sampling system.
o EPA 40 CFR 60 Appendix A, Method 25A: Non - Methane Hydrocarbons will be measured
on a hot-wet basis by using a Flame Ionization Analyzer equipped with a Hydrocarbon Cutter.
The FID analyzer will measure levels of both THC and Methane. The NMHC levels are
automatically measured and output by the analyzer by subtracting the measured Methane levels
from the Total Hydrocarbon levels. This analyzer will be calibrated using EPA Protocol Gl
Propane (C3) gas before and after the one hour test.
l4
APPENDIX A
Example Calculations:
The following is a step-by-step example of the calculations that will be utilized for each test run.
Test Parameters
o Stack Diametero Traverse Pointso Portsr Barometric Pressureo Average Ozo Average COz. Load Approximation
EPA Melhods 1-4: Determination of Stack Gas Velocitv and Flow Rate
Absolute Temperature at Meter (oR) : (Tmi(start) * Tmi(final) * Tmo(start) * T6616na11) / 4
Where:
Tmi(start) - Gas meter inlet start temperature
Tmi(finat) - Cas meter inlet final temperature
Tmo(start) - Cas meter outlet start temperature
Tmo(final)- Gas meter outlet final temperature
Dry Gas Volume (dcf): DMr1c - DMrr_c
Where:DMlc- Final Volume indicated on dry gas meter (dcf)
DMrr_c- lnitial Volume indicated on dry gas meter (dcf)
Dry Gas Volume corrected to standard conditions (dscf) = Ka * Y * ((V. * Pm) / Tm)
Where:
Ka - Gas volume constant
Y - Gas meter constant
V, - Dry gas volume measured by dry gas meter
P, - Absolute pressure at the dry gas meter
T', - Absolute temperature at meter
Moisture Volume (sc| = (0.04715) * Vrc * (0.04715) * Vsc
Where:
Vp6- Volume indicated by mass liquid condensed H2O (g):
(Final Mass Liquid HzO - lnitial Liquid H2O)
Vs6- Volume indicated by mass Iiquid collected in silica gel HzO (g):
(Final Mass Silica Gel - Initial Mass Silica Gel)
0.04715 - Correction factor to standard conditions for mass liquid
Moisture Content (o/o) = Vwrsmr / (Vwrsml + Vr,rrsrol) * 100
Where:
Vw(sro)- Volume of moisture collected as a gas at standard conditions (scf;
Vr,,1(sror- Volume of gas through dry gas meter (corrected dry scf)
Dry Molecular Weight (lbflbmol) = (0.44 * 0ACO) + (0.32 't' o/oOz) + ((0.28 * (%Nz + %CO))
Where:
%oCOz- Carbon Dioxide Content Of The Gas
YoOz- Oxygen Content Of The Gas
%Nz-Nitrogen Content Of The Gas
%CO - Carbon Monoxide Content Of The Gas
Wet Molecular Weight (lbflbmol) = Mo * (l-B*s) + (18) * Bws
Where:
Me- Molecular Weight Of The Dry Gas (lb/lbmol)
Bys - Moisture Content Of The Gas (%/100)
AverageStackGasVelocity(ftisec)=Co*(85.49)*r/APouo*{(Tr/(((Psl13.6)+PB)*MJ)
Where:
Cp- Pitot tube constant (unitless)
.hPouo - Average square root of the stack gas pitot DP (inches water)
Ts- Average stack temperature (oR)
Ps- Barometric pressure (in Hg)
Ps- Stack pressure relative to barometric pressure (inches water)
Ma- Molecular weight of the wet gas (lb/lbmol)
AverageDryFlowrate(dscfm):60*(l-Bws)*Vs* tr*(((Ds l2)l1D)\* T5p/Ts*(PB+(Ps/
13.6)) 12e.92
Where:
D5- Diameter of the stack (inches)
Byy5 - Moisture content of the gas (%)
Tsro - Standard temperature (528"R)
Ts- Average stack temperature (oR)
Ps- Barometric pressure (in Hg)
Ps- Stack pressure relative to barometric pressure (inches water)
Vs- Average Stack gas velocity (fVsec)
Corrected Flue Gas Concentration (PPM) : (Cn - Co) * Cvu / (CM - Co)
Where:
Cp- Average flue gas concentration indicated by gas analyzer (ppm)
Cs- Average of initial and final zero system bias checks (ppm)
Cy - Average of initial and final span system bias checks (ppm)
Cyu - Actual concentration of span gas (ppm)
NO* Emission Rate (lb/hr): PPMo * Qo * MW * 60 / (385.3 * 1000000)
Where:
NO*-Nitrogen Oxides
PPM9 - Average Concentration Of Corrected Pollutant At Outlet
Qo - Volumetric Flow Rate At Outlet (dscfm)
MW- Molecular Weight = 46.01
60- Conversion Factor (Minutes per Hour)
385.3 - Volume Occupied By One Pound Of Gas At Standard Condition (dscf/lb-mole)
1000000 - Conversion Factor (PPM To Mole Fraction)
N0, Emission Rate (g/BHp-hr) = lb/hr * 454 I BHp
Where:
NO*- Nitrogen Oxides
454 - Conversion factor (lb to grams)
BHp - Unit Brake Horsepower
NO,Correction to lsoh 02 = PPM6 * (20.9 - l5) / (20.9 -O2yo)
Where:
NO*- Nitrogen Oxides
PPM9 - Average Concentration Of Corrected Pollutant At Outlet
02 - Oxygen Concentration in Exhaust Stream (%)
CO Emission Rate (lb/hr): PPMo * Qo * MW * 60 / (385.3 * 1000000)
Where:
CO- Carbon Monoxide
PPM9 - Average Concentration Of Corrected Pollutant At Outlet
Q6 - Volumetric Flow Rate At Outlet (dscfm)
MW- Molecular Weight = 28.01
6G- Conversion Factor (Minutes per Hour)
385.3 - Volume Occupied By One Pound Of Gas At Standard Condition (dscf/lb-mole)
1000000 - Conversion Factor (PPM To Mole Fraction)
CO Emission Rate (g/BHp-hr) = lb/hr * 454lBHp
Where:
CO- Carbon Monoxide
454 - Conversion factor (lb to grams)
BHp - Unit Brake Horsepower
CO Correction to 157o Oz: PPMo * (20.9 - l5) / (20.9-02)
Where:
CO- Carbon Monoxide
PPM9 - Average Concentration Of Corrected Pollutant At Outlet
02 - Oxygen Concentration in Exhaust Stream (%)
VOC Correction to Dry Concentration : PPM*u/ [ - (B*, / 100)]
Where:
VOC- Volatile Organic Compounds (NMHC)
PPM*5- Average concentration of corrected pollutant at outlet (wet basis)
B*, - Moisture content (oZ)
VOC Emission Rate (lbihr) = PPMo * Qo * MW * 60 / (385.3 * 1000000)
Where:
VOC - Volatile Organic Compounds (NMHC)
PPM9 - Average concentration of corrected pollutant at outlet (ppm)
Qe - Volumetric flow rate at outlet (dscfm)
MW - Molecular Weight : 44.11
60 - Conversion factor (minutes per hour)
385.3 - Volume occupied by one pound of gas at standard conditions (dscf/lb-mole)
1000000 - Conversion factor (ppm to mole fraction)
VOC Emission Rate (g/BHp-hr): lb/hr * 454lBHp
Where:
VOC - Volatile Organic Compounds (NMHC)
454 - Conversion factor (lb to grams)
BHp - Unit Brake Horsepower
VOC Correction to lSVo 02 = PPMo * (20.9 - l5) / (20.9-O2)
Where:
VOC- Volatile Organic Compounds (NMNEHC C3)
PPM6 - Average Concentration Of Corrected Pollutant At Outlet
02 - Oxygen Concentration in Exhaust Stream (%)
Method 18 (Optional): NMHC Correction to NMNEHC (lbs/hr) : ENMHC -Ec:su
Where:
ENuHc - NMHC emission rate (lbs/hr)
EcrHu - Ethane emission rate (lbsihr)
APPENDIX B
Airsa$.
an Alr Llqulde company
I
II efrgas Specialty GasesI eiryas USA LLC
I saillottlt Industrial Loop Road
I Tooele, UT84o74
I Airgas,com
i
i
ICERTIFICATE OF ANALYSIS
I
Grade of Produbt: npe PROTOCOL STAIIDARD
IE02N199E15A3614 i neference Number: 153402554364-1CC128868 | Cylinder Volume: 144.0 CF
124 - Tooele (SAP) - UT i Cylinder Pressure: 2015 PSlc872022 | Valve Outlet 660NO,NOX,BALN I Certification Date: OclO7,2O22
Expiratioh Date: Oct 02. 2030
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
e,€rlification pErformed in accordance wiih 'EPA Tracsablltt, Protocol for Assay and Cortificalion of Gaseous Callbrauon Standards (May 2012I document EPA
600/R-'12/531, uslng the assay procedures listed. Analylicsl +,lelhodology does not roquire correctlon for anaMlcal intertorance, This cylinder has a total analytical
uncerlsinty as statsd bslow with a conlldence level of 9506. Theio are no signlficant lmpurilles wtrich affect the use of thls calibratlon mixlure. All concenlrations are on a
Do Not Use'Thls below '100 osio. l.e.
Trlad Data Available Upon Request
It
mole/mole basls unless othenrvise noted.
Actual I
Concentrdtion
Protocol Total RelativeMethod Uncertainty
NOX
NITRIC OXIDE
NITROGEN
250.0 PPM
250.0 PPM
Balance
250.4 PPM I
250.4 PPM
I
G1
G,I
+l- 0.9Yo NIST Traceable
+l- 0.9o/o NIST Traceable
a9 t3012022, 1 0 to7 t2022
0913012022, 10n7n022
CALIBRATION STANDARDS
Hil. i:ffi:;:,,,., sffi^;l)GMIS 1534012021103 NErrc012
The SRM, PRM or RGM noted above is only in rcference to lhe
Oct 1S, 2026
Fab 02,2022
Apr 30, 2024
Feb 17,2023
Jun 15,2025
lnstrumenUMake/Model
YTICAL EQUIPMENT
Last Multipoint Catlbratlon
Nicolet lS50 4UP2010228 NO MNO Oct06,2022
od.06,2022Nicolet iS50 AUP2010228 NO2
Atrgas
an Air Ljquid€ company
ai-d*usi-iri" -
5e5 North Industrial hop Road
Tooele, UT 84o74
Airgas.com
CERTIFICATE OF A]\IALYSIS
Grade of Product: EPA PROTOCOL STAI{DARI)
Part Number: E02N199E15A0919
Cylinder Number: CC277490Laboratory: 124 - Tooele (SAP) - UT
PGVP Number: 872021
Gas Code: NO,NOX,BALN
Reference Number: 153402288874-1
Cylinder Volume: 144.4 CF
Cylinder Pressure: 2015 PSIG
Valve Outlet: 660
Certification Date: Dec 06, 2021
Expiratlon Date: Dec 06. 2029
Certification performed in accordanca wlth "EPA Traceabili:y Protocol for A$ay and Certlfication of GasoouG Callbration Standsrds (May 2012)' documenl EPA
600/R-12/531, using the assay procedures listod. Analytical Methodology does nol roquir€ corection for enalytlcal intorfer€nc€. This cylinder has a totral analylical
uncerlainty e8 statod below wllh a conridence l6v€l of 9506. There are no significsnt impurities which atfect the us€ of this calibralion mixture. All conc€ntrations are on a
Triad Data Available Upon Request (ff
mole/mole basis unl€ss otharwis€ noled.
ANALYTICAL RESULTS
Actual Protocol Total Relative
NOX
NITRIC OXIDE
NITROGEN
500.0 PPM
500.0 PPM
Balance
502.3 PPM
500.8 PPM
G1
G1
+l 0.6% NIST Traceable
+/- 0.60/o NIST Traceable
f P9n021,12106n021
1 1 t2912021, 12106t2021
CALIBRATION STAI\IDARDSpe Lot lD Cylinder No Concentration Uncertalnty Explratlon Date
NTRM 15010110PRM 12386
GMIS 401648675102
Aug 16. 2027
Feb 20, 2020
Feb 01, 2023
The SRM, PRM or RGM noted abovo ls
Nicolet iS50 AUP2110269 NO MNO FTIR
FTIR NO2
Nov 17, 2021
Nov 17, 2021Nicolet iS50 AUP2110269 NO2 i
Approved for Release Page 1 of '153,{02288874.1
Airga$,
an Air Uqulde company
Airgas Specialty Gase.s
Airgas USA LLC
52S North tndustrial Laop Road
Tooele, UT 84o74
Nrgos.com
CERTIFICATE OF AI\IALYSIS
Grade of Product: EPA PROTOCOL STANDARD
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
EO2Nt99E 15A3168
xco1 21 388
124 - Tooele (SAP) - UT
872023
CO,BALN
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certilication Date:
153402679334-1
144.0 CF
2015 PS|G
350
Mar 03, 2023
Expiration Date: Mar 03, 2031
Codifioatlon pedormed ln accordance wilh 'EPA Trac€ablllty Protocol for Assay snd Cerlilicatlon of GaEeous Calib.ation Standards (May 2012)'documont EPA
6004-i2/63'1, uslng th€ assay Eocedu.es listed. Analytlc€l M€lhodology does not requi.o conectlon lor analyllcal intorrercnco. Thls cylinder has a total analytical
uncartainty as stalsd bebw wilh a conlidence l6vol of 950/.. There are no slgnmcant impurili€s which aftect the use ol thls callbratlon mixture. All conconlrations aro on a
Not Use This bolow 100 peig, Le. 0.7
Trlad Data Available Upon Request flt
Total Relatlve
Uncertainty
CARBON MONOXIDE 500.0 PPM 498.2 PPM G1 +l- o,4% NIST Traceable O3103t2023NITROGEN Balance
CALIBRATION STANDARDS
Lot lD Gyllnder No Goncentration Uncertainty Explratlon Date
NTRM 210601-11 .3 31.2027
Nicolet lS50 AUP2O10228 CO
Page 1 of 1
Airgas
an Air Liquido company
Airgas Spccialty Gases
AiTg6 USA LLC
525 North Industrial tnop Road
Tooclc, UT 84o74
Ai rg,ar. conr
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARD
Part Number: E02N199E15A0979
CylinderNumber: XCO091078Laboratory: 124 - Tooele (SAP) - UT
PGVP Number: 872022
Gas Code: CO,BALN
Reference Number: 153*402538506-1
Cylinder Volume: 144.0 CF
Cylinder Pressure: 2015 PSIG
Valve Outlet: 350
Certification Date; Sep 12,2022
Expirauon Date: Sep 12.2030
Certlllcalion psrtomod ln accordancs with ''EPA Traceabillty Protocol for Assay and Cerllllc€lion of Gaseous Callbralion Stand6rds (May 2012)'dooment EPA
600/R-12/531, using the assay procedures listed. Analytical Mothodology doss not require correction for analytical interferenco. This cylinder has a total analytical
uncertainly as statod below with a conlid€nco lovel of 950/0. There are no signmcant impunt€s which afioct lh6 us€ of this calibration mrxture. All concentratrons ara on a
Triad Data Available Upon Request flt
mole/mole basis unless olherwise noled.
Component Requested
Concentration
ANALYTICAL RESULTS
Actual ProtocolConcentration Method
Total Relative
Uncertalnty
Assay
Dates
CARBON MONOXIOE 1200 PPM 1199 PPM Gl +l-0.4o/o NlsTTraceable 0911212022NITROGEN Balance
CALIBRATION STANDARDS
Type Lot lD Cylinder No Concentration Uncertalnty Expiratlon Date
NTRM 210601-1 1 ^G0 -7.3 pprrIRBON INO-OGI| 0.- Auq 31.2027
I
Last M[ioolnt CatibrationrnsrrumenuMake/Moder .\ lIHfit"J SFur-
NicdetlSsoAUPzolO2zSCOHlLJt ilRI U I I Eo,h
Page I of 1
Airgas
an Alr Llquido company
Airgas Specialty Gasqs
Airgas USA LtC
525 North Industrial lnop Road
Tooclc, UT 84o74
Ai rga-s. conr
Part Number:
Cylinder Number
Laboratory:
PGVP Number:
Gas Code:
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARD
E03N180E15A0138 Reference Number: 153-402554387-1CC349454 Cylinder Volume: 141.0 CF
124 - Tooele (SAP) - UT Cylinder Pressure: 2015 PSIG872022 Valve Outlet: 590CO2,O2,BALN Certification Date: Sep27,2022
ration Date: Seo 27
Cortification performed in accordanco wiih "EPA Traceability Protocol lor A6say and Certilication ot Gaseous Calibratlon Standards (May 20'1 2)" document EPA
6OO/R-12/531, using the assay procedures lislod. Analytical Methodology doos nol requlre corectlon for analytical inlerferenc€. This cylinder has a total analytical
uncertainty as stated b€low wilh a conlidence levol ol95%. There aro no significanl impurilies which afl6cl the use of this cslibration mixture. All concentrations aro on a
Triad Data Available Upon Request
ll
mole/mole basis unless otherwise noted,
Do Not Use This below 100 i.e.0.
ANALYTICAL RESULTS
Actua! ProtocolConcentntion Method
Total Relatlve
Uncertalnty
Component Requested
Goncentration
Assay
Dates
+l- 1 .2o/o NIST Traceable
+l- O.7o/o NIST Traceable
CARBON DIOXIDE
OXYGEN
NITROGEN
'10.00 %
10.00 %
Balance
9.924 %
10.09 %
G'l
G1
09t27t2022
0s127t2022
CALIBRATION STANDARDS
Type LotlD Cy[IAo 1 Conc]ration 1
-.
I Uncllil Expiration Date
0.69
0.79
-
NTRM
NTRM
1 3060405
98051 01 0 S*^.fY::r boAl 7N]TR May 14,2025
Oec 14,2023t-.R
rnstrumenuMake/Moder \r, f*,H'I*,ff '*u"k^,tm,,o',oon
Sep 14,2022
Sep 14,2022
CO2 NDIR (Dixon)
O2 Paramagnelic (Mason)
Horiba VIA-S10 SV4MEUTJ CO2
Horiba MPA-510 \ /503MM58 02
ary,
Approved for Relea(e--l Page 1 of 1
Airua$"
an Alr Llqulde company
Airgas SpcclaltY Ga6cs
Airgas USA LtC
525 North Industrial laoP Road
Tooele, UT 84o74
Airgas.com
CERTIFICATE, OF ANALYSIS
Grade of Product: EPA PROTOCOL STAMARD
Reference Number: 153-402910964-1
Cylinder Volume: 159.6 CF
Cylinder Pressure: 2015 PSIG
Valve Outlet 590
Certilication Date: Dec 1 1, 2023
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
E03N160E15A0286
ca702344
124 - Tooele (SAP) - UT
872023
C02,02,BALN
ANALYTICAL RESULTS
Actual Protocol
Concentration Method
2O.OO "/r
20.00 %
+l- 0.7o/o NIST Traceable
+ t - o -5o/o N IST Traceable
1211112023
1211112023
Dec 11 , 2025
lnstrumenUMake/Model Ana
Horiba MA-S10 SV4MEUTJ CO2
Horiba MPA-510 !!603MM58 02
Nov '15, 2023
Nov 1 5, 2023
Triad Data Avallable UPon Request
ll
Page 1 of 1
Airgas
an Alr LiquidB company
Airgas Spccialty Culics
Airgas USA LtC
525 North Indu.strial toop Road
Tooclc, UT 84o74
CERTIFICATE OFANALYSIS
ffi;I#'-+ ,I
Grade of Product: EPA PROTOCOL STANDARD
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
E02N199E15A0681
cc709863
124 - Tooele (SAP) - UT
872022
PPN,BALN
ExpiraU:n Date:
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
Nov 07. 2030
1 53-402586702-1
144.0 CF
2015 PSIG
350
Nov 07, 2022
C€rtilicstion porformod in accordanco wlth'EPA Tracoabi ity Prolocol tor Assay and Certilicstion of Gasoous Calibration Standards (May 2012)'document EPA
600/R-l 2:/531, using lh€ asssy procedures lisied. Analylicd Methodology does nol require corection for anslylical lnterforonca. This cyhnder hss a lotral analytlc€t
uncanainty as stated b€low wlth a confidonco lowl of 95%. Tl€re aro no signlflcant lmpuritiss which afloct tho use ol lhis csllbratlon mixtura. AJI concent aiions arg on a
mol€/mol€ basls unless olherwiso noted. The resulls relate onl) lo the ltems tssted. Th€ roport thall not be roproducod except in lull withoul approval ol tho laboraiory. Oo
This Cylindor
Trlad Daia Available Upon Request
Not Uso bolow 100 psig, i.e.0.7
Component Requested
Concentration
ANALYTICAL RESULTSActual ProtocolConcentration Method
Total Relative
Uncertalnty
Assay
Dates
PROPANE 3OO.O PPM 301.4 PPM
NITROGEN Balance
+ l- O.9o/o NIST Traceable 1110712022G'1
CALIBRATION STANDARDSTvpe Lot lD Cvlinder No Goncentration Uncertainty Explration Date
NTRM 12010923 ^-ID46382 I I PPM PrAIE 10.6% I 4pr21.2o24
rns,umenuMake/Moder H A*lf!#f"ilrygll r"",Iil;:Htca,ibration
Nicorelis50AUP2r10269CsHltE3H, ! lFIl U7 ,,-oa,nltz,t-
Page I
Aitga$.
an Alr Llquide oompany
Airgas SpeeialtyGases
Aitgas USA LLiC
rzizS.Wentworth Ave. f
Chicago, IL6o6z8 iAirgas.cont I
CERTIFICATB OF AIVALYSIS
Grade of Product: EPA PROTOCOL STAIIDARI)
Part Number: E02A199E15A0332
CylinderNumber: CC89102Laboratory: 124 - Chicago (SAP) - lL
PGVP Number: 812023
Gas Code: PPN,BALA
Reference Number: 54402768752-1
Cylinder Volume: 146.0 CF
Cylinder Pressure: 2015 PSIG
Valve Outlet: 590
Certification Date: Jun 12,2023
Explration Date: Jun '12, 2031
Certllicatlon perfomed ln accordancs wlth 'EPA Trac€abillty Protocol br A$ay and C€rtllication of Gas€ou8 Calibralion Stsndards (May 2012)' documonl EPA
600/R-12/531, using tho assay proceduros llstod. Analytlcal Methodology does not require correction for analytlcal interlerence. This cylinder has a total snalytical
uncertainty as stated bolow with a confidence level of 95%. There aro no signlficant impuritles which affEc't the use of thls calibratlon mixture. All concentrations aro on a
mole/mols basis unlegs othgrwise noted, Tho results relats only to tho itsms lested. ThB reporl shall not bo reproduced oxcEpt In lull without approval of the laboratory. Do
Not Us6 Thls below 100 osh. l.€.0.7
Triad Data Available Upon Request rlt
tilorryY/
PROPANE 500.0 PPM 502.0 PPM G1 +/- 1% NIST Traceable 0011212023
AIR Balance
CALIBRATION STANDARDS
Concentratlon
Nicolet iS50 AUP21 1 0277
Approved for Release Page 1 of I
Airgas.
an Air Liquide company
Airgas Specialty Gases
Airgas USA, LLC
525 North Industrial toop Road
Tooele, UT 84o74
Airgas.com
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
CERTIFICATE OF ANALYSIS
Grade of Product: EPA Protocol
E02A199E15A0333 Reference Number:ALM014418 CylinderVolume:
124 -Tooele (SAP) - UT Cylinder Pressure:872019 Valve Outlet:PPN,BALA Certification Date:
Expiration Date: Apr 05,2027
153401464128-1
146.3 CF
2015 PSIG
590
Apr 05, 2019
Certification performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA
600i R-1 2/531 , using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concontralions are on a
100 osio. i.e.0.7
Triad Data Available Upon
Sionalrrrc on file
mole/mole basis unless otherwise noted
ANALYTICAL REST'LTS
Actual ProtocolConcentration Method
PROPANE 850.0 PPM 85,I.4 PPM
AIR Balance
+l- O.8o/o NIST Traceable 0410512019
CALIBRATION STANDARDS
Lot lD Cylinder No Concentration
NTRM 01010307 K010660 499.3 PPM PROPANE/AIR 0.6%Jun 02,2024
Nicolet 6700 AMP09001'19 C3HB
Approved for Release Page I of {53-401464128-1
APEX INSTRUMENTS METIJOD 5 POST.TEST CONSOLE CAUBRATION
USING CALIBMTED CRTNCAL ORIFICES
tdu Cffiol. Hmrdd
iz)sn
onela Sd f,umba
XrI kdd Nmh.il't0
)OU 8crl.l Nm!.r t1705
Ollmonhdhr
t-_-1LF.L2l 12:A
l.6md. tuur.b."
Ihcodel Cilc.lhcuuill 11)hh
Ddid Rosil6
facbrrroonml@
524
2992 hk
17.u7
lFor valld brl Hulta, tha Act!.|v.csum ahould ba I to 2ln. Hg gErtarlhan tta Thaodtcat crltcal vacuum ahqn abM.
Dr, G.. M.lG
cduc.r onno Flomt ^{60.75 SCFM(o"il)fn (AY)tegl (e@,
h H20
4g 0.628 a-s o.s87 4m o6m t.410 OG'
0.4@ llp 0-986 {m!0.62 t-259 {tm
aA9 0-357 a 279 0.ffi offi 0.357 1im oMa
o.m ts a8O Ave@a
Prrl 80. uting th. Pr.ciliq Wct Tesl M6ttr t 1 lAl
.bl6 to tho Nrllml Buoau of Shnd.rdr (N.l.S.T.).'-a5
Monthly Celibr.tlon for February 14 2025
APEX INSTRUMENTS METHOD 5 PRE-TEST CONSOLE CALIBR.ATION
USING CALIBRATED CRITIC,A,L ORIFICES
Mdcr Const.ldo|mlton
h&1. fdd ilucb.r i22
bnd s.drt Numb.r 412(N1
i1 r0
reU g.rl4 ilumb.r tv705lForvrlld t6at c!ult!, th.Acturl Vacuum rhould bc I to 2 ln- Hg greabrtTh. Cidc.t Orlfic. hdct.d x, 6r.r M .nr.d lltan the Th.o.rtlcal Ciucal Vacuun !hom abov!.
qllbndon Csddoc
trb 1,,.to.t6
komtr Prolen DI hHo
tuodc.t Crltlc.l v.Gu@r 11.3 ln Ho
Dauld Ro.eh.
16 LmD 534
29.92
I 7.8,(8 om Ho
a M!qr@r, UFR 4u pm @, ulrno Da precision w6t T3l Mdqt l lAtFl0T,which b tceabtatotha Natiomt Bu@uotsl,andad! (N.i.S.T.).
@Ae^{,
Methane Response Factor And Non-Methane Cutter Penetration Factor Determination
1065.360 (d)1-10 CH4 Response Factor Determination for FID1. C3H8 Span Gas Value (As C1)2. CH4 Span Gas Value
3. lnsure Analyzer Flow/Pressure/Temps Ok
4. lnsure FID Analyzer Calibrated using C3HB to C1 Value5. Zero FID Analyzer6. Span FID Analyzerwith C3H8 Gas Listed in (1) Above
7. Arithmetic Mean of 30 Seconds of Sampling CH4 Span Gas
8. Determine CH4 Response Factor by Dividing Step 7. by 2.
1 065. 365(e) Non-Metha ne C ulter Penetration Factor Determi nation
1506.00
513.00
yes
yes
lero=().oo
SPan=15Uo.UU
M€?ll pg sec CH4l=518.00
RFCH4[THC-FlD]=1.010
Pass
Pass
Pass
1.
2.
3.
4.
5.
b.
7.
8.
9.
10.
11.
12.
13.
14.
15.
CH4 Span Gas Value
C2HO Span Gas Value (As C1)
C3HB Span Gas Value (As C1)
Zero FID ln THC Mode
Span FID with C3HB in THC Mode (As Cl)
C3HB Span Gas in CH4 Mode
C3HB Penetration Factor by Dividing Sfep 6. by Step 5.
C2H6 Span Gas in THC Mode
C2HO Span Gas in CH4 Mode
C2HO Penetration
CH4 Span Gas in
CH4 Span Gas in CH4
CH4 Penetration
Check Zero
Check C3H8 Span
Pass
Pass
Pass
Pass
Pass
Methane Penetration
Ethane Penetration
Penetration
513.00
1UU I.4U
1 506 00
Zero=0.00
SPan=1506.00
-5.00
Pl- csueMuc-Hol=-0.0033
1110.0C
7.0c
aPF cznatt-t 0.00eII=557.0C
F 515.0C
PF nu,,,1 .,n,=0.924
-ioffiF
-2.0c
Span Check=1501.0C
NMHC FID Response & Penetration Factors
Iest Result Pass
Airga$"
an Ah Uqulde company
Airgas Specialty Gases
Airyas USA LLC
525 North Industrial L,oop Rood
Tooele, [If 84o74
Airgos.mm
CBRTIFICATB OF ANALYSIS
Grade of Products EPA PROTOCOL STANDARD
Part Number;
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
E02N199E3sW0001
D496872
124 - Tooele (SAP) - UT
872022
NO2,BALN
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
'153402620036-1
24.5 CF
1700 PStc
660
Dec28,2A22
Date:
Certlllcatlm porformed ln accordance wlln :gpe
HjnJ?::l;5i1,t51',,'^'llm",jff,l]1,Y:*"jff,^ytf-.l"qy_tS llt*y|o oo"ectonio'en"ryrcalrniaierence. ir,ri iyino"r. r,"s. toraranarylcaruncorralntv as statod bslow wlth a conlidenco lovel of 95%. rhere are no iilnificant lmpuirtrei wrrit;fffi'd;;#;t6ffi;iilTi ii4?::X,i f#?:1,;13'fJf, .
PERMANENT NOTES:OXYGEN ADDED To MAINTAIN STABILITY
+rt
Nol Uso
te ute rrqlns tesleo' I no repon snsll not b6 roproducBd cxcept In full wlthout approval of lhe laboratory, DoTh16 Cyllnder b€low 100 oslo. 1.6.0.7 meoFbas.rta
Component
-
Requesied
Concontration
ANAL]MICAL RESULTSActual Protocol Totat RetaflveConcentratlon Method Uncertalnty
Assay
Dates
NITROGEN DIOXIDE 150,0 PPM 145.2 PPM +l- 2,0o/o NIST Traceable 1 2 I 1 9 t2A22, 1 2t2812022
Uncertalnty Explration DateTYP"Lot lD Cylinder No ConcentrationL',M. 15340120215."Gpff,, ":iiltfiFiilmrynPRM 12397
The SRM, NTRM, PRM, or RGM
--
,n"nur"nr*rn.roO", 9
MKU l- t tH Noz 01E143349 FTIR Dec OS, ,02,
Triad Data Available Upon Request
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