DAQ-2025-002473

1

DAQC-438-25
Site ID 16140 (B4)

MEMORANDUM

TO: STACK TEST FILE – CRUSOE ENERGY SYSTEMS INC. – Mullins Tap Facility

THROUGH: Rik Ombach, Minor Source Oil and Gas Section Manager

FROM: Paul Bushman, Environmental Scientist

DATE: May 8, 2025

SUBJECT: Sources: Five (5) Waukesha 9394 GSI generator engines; SN’s:
WAU-1632087, WAU-1651084, WAU-1651075,
WAU-1641324, WAU-1651044
Contact: Kaitlin Meszaros: 631-245-0308
Location: 2 miles northwest of Myton, Duchesne County, Utah
Test Contractor: Great Plains Analytical Services, Inc.
Permit/AO#: DAQE-AN161400001-23 dated August 9, 2023
Action Code: TR
Subject: Review of stack test report dated April 29, 2025
On April 30, 2025, Utah Division of Air Quality (DAQ) received a test report for five (5) Waukesha 9394
GSI generator engines located at Crusoe Energy Systems, Inc. Mullins Tap Facility, Duchesne County,
Utah. Testing was performed March 31, 2025, through April 2, 2025, to demonstrate compliance with the
emission limits found in condition II.B.2.a of Approval Order DAQE-AN161400001-23 and 40 CFR Part
60, Subpart JJJJ. The calculated test results are:

Source Test Date Test
Method Pollutant Tester Results DAQ Results Limits
Waukesha 9394
GSI;
Unit ID: 1320
SN:
WAU-1632087
March 31,
2025
ASTM
D6348-03
NOx
6.355
ppmvd@15%O2
0.110 g/hp-hr
0.527 lb/hr
6.355
ppmvd@15%O2 0.106 g/hp-hr
0.511 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
0.658
ppmvd@15%O2
0.007 g/hp-hr
0.033 lb/hr
0.658
ppmvd@15%O2
0.007 g/hp-hr
0.032 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.397
ppmvd@15%O2
0.007 g/hp-hr
0.032 lb/hr
0.397
ppmvd@15%O2
0.006 g/hp-hr
0.030 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha 9394
GSI;
Unit ID: 1454
SN:
WAU-1651084

April 1,
2025
ASTM
D6348-03
NOx
4.919
ppmvd@15%O2
0.086 g/hp-hr
0.427 lb/hr
4.919
ppmvd@15%O2
0.085 g/hp-hr
0.421 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
8.165
ppmvd@15%O2
0.087 g/hp-hr
0.432 lb/hr
8.165
ppmvd@15%O2
0.086 g/hp-hr
0.426 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
2

Source Test Date Test
Method Pollutant Tester Results DAQ Results Limits
VOC
0.523
ppmvd@15%O2
0.009 g/hp-hr
0.044 lb/hr
0.523
ppmvd@15%O2
0.009 g/hp-hr
0.043 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha 9394
GSI;
Unit ID: 1453
SN:
WAU-1651075
April 1,
2025
ASTM
D6348-03
NOx
4.607
ppmvd@15%O2
0.070 g/hp-hr
0.340 lb/hr
4.607
ppmvd@15%O2
0.070 g/hp-hr
0.337 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
0.387
ppmvd@15%O2
0.004 g/hp-hr
0.017 lb/hr
0.387
ppmvd@15%O2
0.004 g/hp-hr
0.017 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.345
ppmvd@15%O2
0.005 g/hp-hr
0.024 lb/hr
0.345
ppmvd@15%O2
0.005 g/hp-hr
0.024 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha 9394
GSI;
Unit ID:
2026-01
SN:
WAU-1641324
April 2,
2025
ASTM
D6348-03
NOx
2.609
ppmvd@15%O2
0.039 g/hp-hr
0.183 lb/hr
2.609
ppmvd@15%O2
0.039 g/hp-hr
0.183 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
0.109
ppmvd@15%O2
0.001 g/hp-hr
0.005 lb/hr
0.109
ppmvd@15%O2
0.001 g/hp-hr
0.005 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.462
ppmvd@15%O2
0.007 g/hp-hr
0.031 lb/hr
0.462
ppmvd@15%O2
0.007 g/hp-hr
0.032 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha 9394
GSI;
Unit ID:1452
SN:
WAU-1651044
April 2,
2025
ASTM
D6348-03
NOx
4.006
ppmvd@15%O2
0.068 g/hp-hr
0.332 lb/hr
4.006
ppmvd@15%O2
0.068 g/hp-hr
0.334 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
14.894
ppmvd@15%O2
0.153 g/hp-hr
0.752 lb/hr
15.088
ppmvd@15%O2
0.156 g/hp-hr
0.765 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.508
ppmvd@15%O2
0.008 g/hp-hr
0.040 lb/hr
0.508
ppmvd@15%O2
0.008 g/hp-hr
0.041 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr

DEVIATIONS: None.

CONCLUSION: The stack test report appears to be acceptable.

3

RECOMMENDATION: The emissions from the five (5) Waukesha 9394 GSI generator engines
should be considered to have been in compliance with the emission
limits of DAQE-AN161680001-23 and 40 CFR Part 60, Subpart JJJJ
during testing.

ATTACHMENTS: DAQ stack test review excel spreadsheets, Crusoe Energy Systems Inc.
stack test report.
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1320 SN:WAU-1632087
Test Date: 3/31/2025
Run #1 2 3 Average
Start Time 7:43 8:53 10:01
Stop Time 8:43 9:53 11:01
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2175 2175 2200 2183
DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.7211 0.6928 0.6782 0.6974
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)901 909 911 907
Pbar Barometric Pressure (mbar)1013 1012 1013 1012
Pbar Barometric Pressure (" Hg)29.92 29.88 29.91 29.90
Ps Stack Pressure ('' H2O)0.52 0.48 0.46 0.49
O2%vd O2 (%vd)0.0 0.0 0.0 0.0
CO2%vd CO2 (%vd)11.5 11.6 11.6 11.5
N2%vd N2 (%vd)88.5 88.5 88.4 88.5
dry NOX (ppmvd)22.7 21.2 23.6 22.5
dry CO (ppmvd) 2.0 1.5 3.4 2.3
wet TVOC (ppmvw as C3H8)0.9 1.1 1.4 1.2
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.171 0.172 0.171 0.171
Bws Saturated Moisture Content (%/100)548.145 567.979 572.182 562.768
Bws Actual Moisture Content (%/100)0.171 0.172 0.171 0.171
MD Molecular Weight Dry (lb/lb-mole)29.84 29.85 29.85 29.85
MA Molecular Weight Wet (lb/lb-mole)27.82 27.82 27.82 27.82
VS Gas Velocity (ft/sec)78.0 75.2 73.6 75.6
FACFM Gas Flow (acfm)10210 9846 9640 9899
FDSCFM Gas Flow (dscfm)3286 3142 3076 3168
FWSCFM Gas Flow (wscfm)3965 3796 3714 3825
FKWSCFH Gas Flow (kwscfh)238 228 223 230
FKWSCFM Gas Flow (kwscfm)4 4 4 4
lb/hr Gas Flow (lb/hr) 17179 16443 16094 16572
Fo Fo (unitless)1.817 1.810 1.806 1.811
wet O2 (%vw)0.0 0.0 0.0 0.0
wet CO2 (%vw)9.5 9.6 9.6 9.6
wet NOX (ppmvw)18.825 17.592 19.558 18.658
15 NOX (ppmvd @ 15% O2)6.408 5.995 6.662 6.355 82.0
lb/hr NOX (lb/hr)0.534 0.478 0.520 0.511 0.83
g/bhp-hr NOX (g/bhp-hr)0.111 0.100 0.107 0.106 0.15
wet CO (ppmvw) 1.698 1.255 2.841 1.931
15 CO (ppmvd @ 15% O2)0.578 0.428 0.968 0.658 270.0
lb/hr CO (lb/hr) 0.029 0.021 0.046 0.032 1.65
g/bhp-hr CO (g/bhp-hr) 0.006 0.004 0.009 0.007 0.30
dry NMEOC (ppmvd as C3H8)1.105 1.379 1.735 1.406
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.312 0.389 0.490 0.397 60
lb/hr NMEOC (lb/hr as C3H8)0.025 0.030 0.037 0.030 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.005 0.006 0.008 0.006 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.117 0.106 0.115 0.112
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1320 SN:WAU-1632087
Test Date: 3/31/2025
O2
20.9
10.58
0.0
10.2
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.5
%
0.00
10.58
20.92
0.0
10.5
20.7
0.0
0.1
0.2
0.0
0.00%
1.24%
0.91%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1320 SN:WAU-1632087
Test Date: 3/31/2025
O2
20.9
10.58
0.0
10.2
0.0
10.6
0.0%
0.5%
0.0%
1.8%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1320 SN:WAU-1632087
Test Date: 3/31/2025
O2
20.9
10.58
0.0
10.2
0.0
10.6
0.0%
0.5%
0.0%
1.8%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1320 SN:WAU-1632087
Test Date: 3/31/2025
O2
20.9
10.58
0.0
10.2
0.0
10.6
0.0%
0.5%
0.0%
1.8%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 14534SN:WAU-1651084
Test Date: 4/1/2025
Run #1 2 3 Average
Start Time 7:11 8:22 9:30
Stop Time 8:11 9:22 10:30
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2250 2250 2250 2250
DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.7616 0.7550 0.7416 0.7527
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)928 922 923 925
Pbar Barometric Pressure (mbar)1002 1002 1001 1002
Pbar Barometric Pressure (" Hg)29.60 29.60 29.58 29.59
Ps Stack Pressure ('' H2O)0.58 0.57 0.55 0.57
O2%vd O2 (%vd)0.0 0.0 0.0 0.0
CO2%vd CO2 (%vd)11.6 11.5 11.5 11.5
N2%vd N2 (%vd)88.4 88.5 88.6 88.5
dry NOX (ppmvd)16.2 16.2 19.9 17.4
dry CO (ppmvd) 45.4 15.0 26.4 28.9
wet TVOC (ppmvw as C3H8)1.7 1.3 1.6 1.5
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.173 0.173 0.172 0.173
Bws Saturated Moisture Content (%/100)619.743 604.494 607.557 610.598
Bws Actual Moisture Content (%/100)0.173 0.173 0.172 0.173
MD Molecular Weight Dry (lb/lb-mole)29.85 29.84 29.83 29.84
MA Molecular Weight Wet (lb/lb-mole)27.80 27.80 27.80 27.80
VS Gas Velocity (ft/sec)83.7 82.8 81.4 82.6
FACFM Gas Flow (acfm)10951 10833 10649 10811
FDSCFM Gas Flow (dscfm)3409 3389 3330 3376
FWSCFM Gas Flow (wscfm)4126 4099 4024 4083
FKWSCFH Gas Flow (kwscfh)248 246 241 245
FKWSCFM Gas Flow (kwscfm)4 4 4 4
lb/hr Gas Flow (lb/hr) 17864 17747 17420 17677
Fo Fo (unitless)1.803 1.813 1.825 1.814
wet O2 (%vw)0.0 0.0 0.0 0.0
wet CO2 (%vw)9.6 9.5 9.5 9.5
wet NOX (ppmvw)13.419 13.374 16.464 14.419
15 NOX (ppmvd @ 15% O2)4.582 4.564 5.612 4.919 82.0
lb/hr NOX (lb/hr)0.396 0.392 0.474 0.421 0.83
g/bhp-hr NOX (g/bhp-hr)0.080 0.079 0.096 0.085 0.15
wet CO (ppmvw) 37.541 12.410 21.828 23.926
15 CO (ppmvd @ 15% O2)12.819 4.235 7.440 8.165 270.0
lb/hr CO (lb/hr) 0.675 0.222 0.383 0.426 1.65
g/bhp-hr CO (g/bhp-hr) 0.136 0.045 0.077 0.086 0.30
dry NMEOC (ppmvd as C3H8)2.020 1.590 1.951 1.854
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.570 0.449 0.551 0.523 60
lb/hr NMEOC (lb/hr as C3H8)0.047 0.037 0.045 0.043 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.010 0.007 0.009 0.009 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.089 0.087 0.105 0.093
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 14534SN:WAU-1651084
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.6
%
0.00
10.58
20.92
0.0
10.6
21.1
0.0
0.0
0.2
0.0
0.00%
0.81%
0.91%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 14534SN:WAU-1651084
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
0.0
10.4
0.0%
1.0%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 14534SN:WAU-1651084
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
0.0
10.4
0.0%
1.0%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 14534SN:WAU-1651084
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
0.0
10.4
0.0%
1.0%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1453 SN:WAU-1651075
Test Date: 4/1/2025
Run #1 2 3 Average
Start Time 11:20 12:29 1:42
Stop Time 12:20 13:29 2:42
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2200 2200 2175 2192
DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.6403 0.6245 0.6403 0.6350
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)903 898 900 901
Pbar Barometric Pressure (mbar)1002 998 1008 1003
Pbar Barometric Pressure (" Hg)29.60 29.48 29.79 29.62
Ps Stack Pressure ('' H2O)0.41 0.39 0.41 0.40
O2%vd O2 (%vd)0.0 0.0 0.0 0.0
CO2%vd CO2 (%vd)11.3 11.4 11.3 11.3
N2%vd N2 (%vd)88.7 88.6 88.7 88.7
dry NOX (ppmvd)23.0 12.3 13.7 16.3
dry CO (ppmvd) 4.1 0.0 0.0 1.4
wet TVOC (ppmvw as C3H8)1.0 0.8 1.2 1.0
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.172 0.169 0.172 0.171
Bws Saturated Moisture Content (%/100)558.460 549.474 548.500 552.144
Bws Actual Moisture Content (%/100)0.172 0.169 0.172 0.171
MD Molecular Weight Dry (lb/lb-mole)29.81 29.82 29.81 29.81
MA Molecular Weight Wet (lb/lb-mole)27.78 27.82 27.78 27.79
VS Gas Velocity (ft/sec)69.7 68.0 69.4 69.1
FACFM Gas Flow (acfm)9129 8899 9090 9039
FDSCFM Gas Flow (dscfm)2897 2832 2909 2879
FWSCFM Gas Flow (wscfm)3502 3412 3516 3477
FKWSCFH Gas Flow (kwscfh)210 205 211 209
FKWSCFM Gas Flow (kwscfm)4 3 4 3
lb/hr Gas Flow (lb/hr) 15148 14781 15213 15047
Fo Fo (unitless)1.848 1.837 1.845 1.843
wet O2 (%vw)0.0 0.0 0.0 0.0
wet CO2 (%vw)9.4 9.5 9.4 9.4
wet NOX (ppmvw)19.025 10.175 11.362 13.521
15 NOX (ppmvd @ 15% O2)6.488 3.458 3.875 4.607 82.0
lb/hr NOX (lb/hr)0.477 0.248 0.286 0.337 0.83
g/bhp-hr NOX (g/bhp-hr)0.098 0.051 0.060 0.070 0.15
wet CO (ppmvw) 3.405 0.000 0.000 1.135
15 CO (ppmvd @ 15% O2)1.161 0.000 0.000 0.387 270.0
lb/hr CO (lb/hr) 0.052 0.000 0.000 0.017 1.65
g/bhp-hr CO (g/bhp-hr) 0.011 0.000 0.000 0.004 0.30
dry NMEOC (ppmvd as C3H8)1.255 0.963 1.447 1.222
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.354 0.272 0.409 0.345 60
lb/hr NMEOC (lb/hr as C3H8)0.025 0.019 0.029 0.024 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.005 0.004 0.006 0.005 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.103 0.055 0.066 0.075
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1453 SN:WAU-1651075
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.6
%
0.00
10.58
20.92
0.0
10.6
21.1
0.0
0.0
0.2
0.0
0.00%
0.81%
0.91%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1453 SN:WAU-1651075
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
0.0
10.4
0.0%
1.0%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1453 SN:WAU-1651075
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
0.0
10.4
0.0%
1.0%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1453 SN:WAU-1651075
Test Date: 4/1/2025
O2
20.9
10.58
0.0
10.4
0.0
10.4
0.0%
1.0%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1452 SN:WAU-1651044
Test Date: 4/2/2025
Run #1 2 3 Average
Start Time 6:55 8:04 9:12
Stop Time 7:55 9:04 10:12
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2225 2225 2225 2225
DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.7211 0.7211 0.7348 0.7257
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)928 925 922 925
Pbar Barometric Pressure (mbar)1010 1011 1010 1010
Pbar Barometric Pressure (" Hg)29.84 29.86 29.84 29.85
Ps Stack Pressure ('' H2O)0.52 0.52 0.54 0.53
O2%vd O2 (%vd)0.0 0.0 0.0 0.0
CO2%vd CO2 (%vd)11.3 11.4 11.3 11.3
N2%vd N2 (%vd)88.7 88.6 88.7 88.7
dry NOX (ppmvd)13.9 14.9 13.8 14.2
dry CO (ppmvd) 54.1 53.5 52.7 53.4
wet TVOC (ppmvw as C3H8)1.4 1.6 1.5 1.5
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.168 0.169 0.168 0.168
Bws Saturated Moisture Content (%/100)614.682 606.392 599.218 606.764
Bws Actual Moisture Content (%/100)0.168 0.169 0.168 0.168
MD Molecular Weight Dry (lb/lb-mole)29.81 29.82 29.81 29.81
MA Molecular Weight Wet (lb/lb-mole)27.83 27.83 27.83 27.83
VS Gas Velocity (ft/sec)78.9 78.7 80.2 79.3
FACFM Gas Flow (acfm)10323 10308 10495 10375
FDSCFM Gas Flow (dscfm)3261 3262 3330 3284
FWSCFM Gas Flow (wscfm)3920 3926 4004 3950
FKWSCFH Gas Flow (kwscfh)235 236 240 237
FKWSCFM Gas Flow (kwscfm)4 4 4 4
lb/hr Gas Flow (lb/hr) 16991 17015 17354 17120
Fo Fo (unitless)1.848 1.837 1.845 1.843
wet O2 (%vw)0.0 0.0 0.0 0.0
wet CO2 (%vw)9.4 9.5 9.4 9.4
wet NOX (ppmvw)11.555 12.368 11.494 11.806
15 NOX (ppmvd @ 15% O2)3.919 4.199 3.899 4.006 82.0
lb/hr NOX (lb/hr)0.324 0.347 0.329 0.334 0.83
g/bhp-hr NOX (g/bhp-hr)0.066 0.071 0.067 0.068 0.15
wet CO (ppmvw) 45.010 44.493 43.891 44.465
15 CO (ppmvd @ 15% O2)15.266 15.107 14.890 15.088 270.0
lb/hr CO (lb/hr) 0.769 0.761 0.765 0.765 1.65
g/bhp-hr CO (g/bhp-hr) 0.157 0.155 0.156 0.156 0.30
dry NMEOC (ppmvd as C3H8)1.740 1.882 1.773 1.798
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.491 0.531 0.500 0.508 60
lb/hr NMEOC (lb/hr as C3H8)0.039 0.042 0.040 0.041 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.008 0.009 0.008 0.008 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.074 0.079 0.075 0.076
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1452 SN:WAU-1651044
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.58
20.92
0.0
10.8
21.2
0.0
0.2
0.3
0.0
0.00%
1.39%
1.48%
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
4
Difference
1
4
Response
1
2
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1452 SN:WAU-1651044
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
0.0
10.5
0.0%
1.5%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1452 SN:WAU-1651044
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
0.0
10.5
0.0%
1.5%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1452 SN:WAU-1651044
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
0.0
10.5
0.0%
1.5%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-01 SN:WAU-1641324
Test Date: 4/2/2025
Run #1 2 3 Average
Start Time 11:01 12:12 13:20
Stop Time 12:01 13:12 14:20
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2100 2100 2125 2108
DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.6083 0.6325 0.6403 0.6270
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)893 896 890 893
Pbar Barometric Pressure (mbar)1001 1007 1005 1005
Pbar Barometric Pressure (" Hg)29.58 29.74 29.70 29.67
Ps Stack Pressure ('' H2O)0.37 0.40 0.41 0.39
O2%vd O2 (%vd)0.0 0.0 0.0 0.0
CO2%vd CO2 (%vd)11.7 11.6 11.6 11.7
N2%vd N2 (%vd)88.3 88.4 88.4 88.4
dry NOX (ppmvd)8.5 10.9 8.3 9.2
dry CO (ppmvd) 0.1 0.9 0.1 0.4
wet TVOC (ppmvw as C3H8)0.9 1.2 2.0 1.4
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.172 0.172 0.171 0.172
Bws Saturated Moisture Content (%/100)535.969 540.191 527.364 534.508
Bws Actual Moisture Content (%/100)0.172 0.172 0.171 0.172
MD Molecular Weight Dry (lb/lb-mole)29.88 29.85 29.86 29.86
MA Molecular Weight Wet (lb/lb-mole)27.83 27.82 27.84 27.83
VS Gas Velocity (ft/sec)66.0 68.5 69.2 67.9
FACFM Gas Flow (acfm)8635 8967 9061 8888
FDSCFM Gas Flow (dscfm)2759 2874 2917 2850
FWSCFM Gas Flow (wscfm)3334 3473 3520 3443
FKWSCFH Gas Flow (kwscfh)200 208 211 207
FKWSCFM Gas Flow (kwscfm)3 3 4 3
lb/hr Gas Flow (lb/hr) 14452 15046 15261 14919
Fo Fo (unitless)1.783 1.803 1.796 1.794
wet O2 (%vw)0.0 0.0 0.0 0.0
wet CO2 (%vw)9.7 9.6 9.7 9.7
wet NOX (ppmvw)6.996 9.056 6.911 7.654
15 NOX (ppmvd @ 15% O2)2.385 3.087 2.353 2.609 82.0
lb/hr NOX (lb/hr)0.167 0.225 0.174 0.189 0.83
g/bhp-hr NOX (g/bhp-hr)0.036 0.049 0.037 0.041 0.15
wet CO (ppmvw) 0.091 0.744 0.124 0.320
15 CO (ppmvd @ 15% O2)0.031 0.254 0.042 0.109 270.0
lb/hr CO (lb/hr) 0.001 0.011 0.002 0.005 1.65
g/bhp-hr CO (g/bhp-hr) 0.000 0.002 0.000 0.001 0.30
dry NMEOC (ppmvd as C3H8)1.103 1.419 2.387 1.636
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.311 0.401 0.674 0.462 60
lb/hr NMEOC (lb/hr as C3H8)0.021 0.028 0.048 0.032 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.005 0.006 0.010 0.007 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.041 0.055 0.047 0.048
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-01 SN:WAU-1641324
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.58
20.92
0.0
10.8
21.2
0.0
0.2
0.3
0.0
0.00%
1.39%
1.48%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-01 SN:WAU-1641324
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
0.0
10.5
0.0%
1.5%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-01 SN:WAU-1641324
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
0.0
10.5
0.0%
1.5%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-01 SN:WAU-1641324
Test Date: 4/2/2025
O2
20.9
10.58
0.0
10.5
0.0
10.5
0.0%
1.5%
0.0%
0.1%
Corrected O2 %
0.0
Run Length
(Minutes) Uncorrected O2 %
60 0.0
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
303 West 3rd Street ● Elk City, Oklahoma 73644 ● 580-225-0403

GAS Inc.
www.gasinc.us
April 29, 2025

Utah Department of Environmental Quality
State Office Building – Air Quality Division
195 North 1950 West
Salt Lake City, Utah 84114

RE: Crusoe Energy Systems, Inc.
40 CFR Part 60 Subpart JJJJ – Test Report SubmiVal

To Whom It May Concern,

Please find enclosed the performance tesXng reports for 40 CFR Subpart JJJJ/State Compliance
on behalf of Crusoe Energy Systems, Inc. Please see below for the informaXon perXnent to the
tesXng. Please see below for the informaXon perXnent to the enclosed reports. Test took place
the week of March 31, 2025.

Facility Unit # Serial # Loca1on
Mullins Tap Facility 1320 WAU-1632087 Duchesne County, Utah
Mullins Tap Facility 1454 WAU-1651084 Duchesne County, Utah
Mullins Tap Facility 1453 WAU-1651075 Duchesne County, Utah
Mullins Tap Facility 2026-01 WAU-1641324 Duchesne County, Utah
Mullins Tap Facility 1452 WAU-1651044 Duchesne County, Utah

For informaXon regarding the performance test, you can contact me by email at
[e-mail] or by phone at 580-225-0403. For informaXon regarding engine or
locaXon informaXon, please contact Kaitlin Meszaros by email at [e-mail] or
by phone at (631)-245-0308.

Regards,

Macie Holsapple
Client Services Supervisor
GAS Inc.
Performance Test Report
Test Type: Annual
Test Date: 3/31/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:07:43 AM 11:31 AM
Source:
Unit Number: 1320
Serial Number: WAU-1632087
Engine Hours:22131
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.033 0.527 0.032
2.330 22.511 1.406
2.000 0.300 1.000 0.150 0.700 0.030
0.007 0.110 0.007
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Lynn Huber
3
Hunter Newton
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 1320 with a serial number of WAU-1632087 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 3/31/2025 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2183 BHP and 1199 RPM which is 87.33% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1320 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1320Unit ID
Make Waukesha Site Elevation ft.5226
Model 9394 GSI Atmospheric Pressure psi.12.01
Serial Number WAU-1632087 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2175 2175 2200 2183
1200 1200 1197 1199
Percent Load %
Intake Manifold Pressure (hg)
87.00%87.00%88.00%87.33%
61.00 61.00 62.00 61.33
Intake Manifold Temperature (F)119.00 119.00 119.00 119.00
Ambient Conditions
Ambient Temperature Dry (F)35.00 35.00 38.00 36.00
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
197373.74 195705.59 195623.91 196234.41
5588.95 5541.71 5539.40 5556.69
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.17 0.17 0.17
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %17.07%17.16%17.13%17.12%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.00%0.00%0.00%0.00%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
07:43 AM 08:53 AM 10:01 AM 3/31/2025
State
NOx (mol wt) 46.01
0.916 1.142 1.438 1.165NMNEHC (ppmvw)
1.104 1.379 1.735 1.406NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
311.641 389.156 489.840 396.879 FailNMNEHC (ppbvd) @15% O2
0.005 0.006 0.008 0.0070.700 0.030 PassNMNEHC (g/hp-hr)
0.025 0.031 0.039 0.0320.170 PassNMNEHC (lbs/hr)
0.312 0.389 0.490 0.397 FailNMNEHC (ppmvd) @15% O2
0.0100.004CO (g/hp-hr)0.006 0.0072.000 0.300 Pass
CO (ppmvw)1.698 1.255 2.841 1.931
CO (ppmvd)2.048 1.515 3.428 2.330
CO (mol wt) 28.01
CO (ppmvd) @15% O2 0.578 0.428 0.968 0.658 Fail
CO (ppbvd) @15% O2 578.009 427.663 967.757 657.810 Fail
0.0490.022CO (lbs/hr)0.029 0.0331.650 Pass
NOx (g/hp-hr)0.112 0.103 0.114 0.1101.000 0.150 Pass
NOx (ppmvw)18.825 17.592 19.558 18.658
NOx (ppmvd)22.699 21.235 23.600 22.511
NOx (ppbvd) @15% O2 6407.965 5994.606 6662.061 6354.877 Fail
NOx (ppmvd) @15% O2 6.408 5.995 6.662 6.355 Fail
NOx (lbs/hr)0.535 0.496 0.551 0.5270.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
1.70
0.00
18.35 0.48 18.82
0.00%
0.00%
0.00%
17.07%
18.40 0.46 0.00%16.96%
37.35 0.00 0.00%15.40%
18.29 0.50 0.00%17.18%
0.00 0.60 0.60 0.00%0.00%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.60 0.60 0.00%0.00%
1.20 17.59 0.55 18.13 0.00%17.14%
44.28 30.11 0.00 30.11 0.00%14.77%
1.31 16.62 0.43 17.05 0.00%17.17%
0.00 0.00 0.57 0.57 0.00%0.03%
Avg. Wet 1.26 17.10 0.49 17.59 1.14 0.00%17.16%
NO2NO
0.46
1.00
20.72
1.28
0.56
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.75 15.86 0.47 16.32 0.00%17.13%
59.61 36.65 0.00 36.65 0.00%15.33%
4.93 22.44 0.36 22.79 0.00%17.13%
0.00 0.00 0.60 0.60 0.00%0.00%
0.00 0.00 0.57 0.57 0.56 0.00%0.03%
Avg. Wet 2.84 19.15 0.41 19.56 1.44 0.00%17.13%
NO2NO
0.43
1.53
26.76
1.35
NMNEHC
0.43
NO2
0.410.00
0.91
24.21
0.92
0.46
0.92
0.42
18.86
37.35
18.79
1.88
1.52
0.00
55.34
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.54
Yes
20.00
5.00
28.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%17.07
29.84
0.52
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.50
0.00
0.00
1012.87
0.04
29.92
29.96
901.25
1360.92
482.92
27.82
77.99
170.17
238000.41
197373.74
Run 2
17.16
29.85
0.48
11.55
0.00
0.00
1011.51
0.04
29.88
29.92
909.38
1369.05
487.43
27.82
75.44
170.15
236239.57
195705.58
Run 3
17.13
29.85
0.46
11.57
0.00
0.00
1012.53
0.03
29.91
29.94
911.38
1371.05
488.54
27.82
73.65
170.15
236052.64
195623.91
17.12
29.85
0.49
11.54
0.00
0.00
1012.30
0.04
29.90
29.94
907.33
1367.00
486.30
27.82
75.72
170.15
236764.21
196234.41
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.45
Exhaust Temp F
901.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.43
0.51
0.57
899.00
903.00
900.00
0.50
0.43
0.50
897.00
896.00
899.00
0.52
0.51
0.48
900.00
902.00
904.00
0.51 903.00
0.54
0.57
0.63
906.00
901.00
903.00
0.63
0.60
0.52
902.00
904.00
901.25
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.51
Exhaust Temp F
911.00
0.46
0.44
0.41
913.00
912.00
908.00
0.38
0.42
0.47
909.00
911.00
912.00
0.49
0.50
0.51
910.00
907.00
914.00
0.45 915.00
0.46
0.44
0.47
912.00
911.00
914.00
0.41
0.54
913.00
910.00
911.380.46
Run 2
Δpstd (in) H2O
0.44
Exhaust Temp F
909.00
0.41
0.47
0.48
910.00
913.00
907.00
0.52
0.55
0.50
908.00
909.00
906.00
0.51
0.48
0.49
911.00
910.00
909.00
0.43 908.00
0.48
0.55
0.53
912.00
911.00
909.00
0.42
0.47
908.00
910.00
0.48 909.38
Pass
Strat Check
74.045Check 1
74.982Check 2
73.604Check 3
MethaneGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.5)+ .32(0)+ .28(88.5+0) = 29.84 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.84(1 -.1707)+ 18.0(.1707) = 27.82 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.52*√(1360.92/(29.96*27.82)) = 77.99 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.1707)77.99*2.182((528*29.96)/ (1360.92*29.92)) = 197373.74 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 197373.74/35.315 = 5588.949 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 2.048*(20.9-15)/(20.9-0%)) = .578 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(2.048*(1.164*10^-3)*5588.949*(Run Time/60))/2175 = .006 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .006*1/453.6*2175 = .029 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .029*4.38 = .127 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
2.05 = 1.698*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.48%
20.73%
10.22%
10.59%
10.58%
10.58%
10.59%10.22%
10.48%
20.73%
10.58%
20.92%
10.58%
20.92%
10.58%20.92%
0.00%
10.58%
20.92%
0.10%
0.19%
0.49%
0.91%
10.58%
Span
Zero Offset 0.00%
20.92
0.00%
10.48%1.24%0.55%0.02%
0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
9
GAS
1076.0 1078.0 1076.7
1058.0 1058.0 1058.0
5.2 5.2 5.2
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
3/31/2025
5226
1320
Waukesha
Model
Serial Number
9394 GSI
WAU-1632087
Technician Hunter Newton
Run Start Times 07:43 AM 08:53 AM 10:01 AM 11:31 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1200.0 1197.0 1199.0
Engine Hours 22128 22129 22130 22131
Intake Manifold Pressure (psi)61.0 61.0 62.0 61.3
Intake Manifold Temp °F 119.0 119.0 119.0 119.0
Engine Load (BHP)2175.0 2175.0 2200.0 2183.3
Ambient Temp °F 35.0 35.0 38.0 36.0
Humidity %70.0 70.0 64.0 68.0
Dew Point °F 26.0 26.0 27.0 26.3
Waukesha
N/A
N/A
Yes
DCL DCL DCL DCL
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
Discharge Pressure (psi)
Suction Pressure (psi)
1076.0
1058.0
5.2Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
N/A N/A N/A N/A
N/A N/A N/A N/A
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.48
Average:NOx 0.48
Average:VOC 0.65
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 98.24
Tolerance 2.00%
Difference between measured and expected 1.33%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.10
Average:NOx 0.10
Average:VOC 0.38
Average:Oxygen 0.00
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 98.06
Tolerance 5.00%
Difference between measured and expected 1.52%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 251.19
Value:Spike Expected 249.80
System (Equilibration) Response Time Target (Spike)
45 secondsSystem Zero Response Time
51 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC507781 9/17/2027 102.10 10.58%
EB0115896 12/18/2027 99.57
CC440196 7/13/2032 20.92%
Cylinder # CC333629 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 249.80 501.50 254.60 9.99
Analyzer System Response 251.19 507.60 250.82 9.82
Percent Difference 0.56%1.22%1.49%1.70%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.244 4.933
Spike Direct
Propane 251.450
Mechanical
Response Time
SF6 9.840
CO 508.503
NO 252.938
Ethylene 98.061 25 seconds
Analyzer
Response
Propane 251.191
SF6 9.818
CO 507.596
NO 250.818
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 249.319
CO 504.318
NO 248.295
17 seconds
30 seconds
8.65%
7.16%
9.47%
102.71%
102.82%
100.84%
9.805
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
5
28
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
196234.41
H2O%d @ Sampling Point:17.12
CO2%d @ Sampling Point:11.54
Pressure @ Sampling Point (Pg "H2O):0.49
Temperature @ Sampling Point (Deg F):907.33
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 99.57 98.24 4.933 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.244 4.933
Spike Direct
Propane 251.450
Mechanical
Response Time
SF6 9.840
CO 508.503
NO 252.938
Ethylene 98.061 25 seconds
Analyzer
Response
Propane 251.191
SF6 9.818
CO 507.596
NO 250.818
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 249.319
CO 504.318
NO 248.295
17 seconds
30 seconds
8.65%
7.16%
9.47%
102.71%
102.82%
100.84%
9.805
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
249.800
9.988
501.500
254.600
251.450
9.840
508.503
252.938
0.66%
1.48%
1.40%
0.65%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.006
0.000
Spike Average
22.200
0.851
Dilution Factor
8.648%
Expected
21.614
% Recovery
102.710%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.705
Dilution Factor
7.165%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.932
Dilution Factor
9.472%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 23.854 23.656 100.840%
0.000705
0.000458
0.000315
0.000 18.390 17.886 102.820%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass1.24%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:37.8719096 Pass
Line Position Difference:Resolution Difference to Reference 1.24%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
99.57
97.25
2.39%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1320; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
3/31/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
3/31/2025
Hunter Newton
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1320
Make:Waukesha
Location:9394 GSIModel:
WAU-1632087Serial Number:
RAW Result Data
Stability
3/31/2025 06:28 0.9470.000-0.034 0.000 0.0000.000 0.000 1.139 0.0000.0020.000 0.000 0.0000.000 0.000 835.01.532.296 0.000 0.95 0.00 181.0
Pre Test Baseline Direct
3/31/2025 06:37 0.7160.0000.000 0.000 0.0000.000 0.000 0.978 0.0000.0290.000 0.000 0.0000.000 0.000 834.00.650.982 0.000 0.72 0.00 180.0
3/31/2025 06:37 0.7110.000-0.002 0.000 0.3320.000 0.000 0.824 0.0000.0000.000 0.000 0.0000.000 0.000 835.00.610.921 0.000 0.71 0.00 180.0
3/31/2025 06:38 0.0000.000-0.001 0.000 0.0000.000 0.000 0.867 0.0000.0000.000 0.000 0.0000.000 0.000 835.00.681.015 0.000 0.00 0.00 180.0
CTS Direct
3/31/2025 06:41 0.0000.0000.008 0.000 0.0000.000 0.000 0.279 0.0630.0430.000 96.694 0.0000.000 0.000 833.065.010.820 0.000 0.00 0.00 180.0
3/31/2025 06:42 0.0000.0000.010 0.000 0.0000.000 0.000 0.393 0.0430.0780.000 99.184 0.0000.000 0.000 832.066.690.840 0.000 0.00 0.00 181.0
3/31/2025 06:43 0.0000.0000.010 0.000 0.0000.000 0.000 0.302 0.0500.0060.000 98.855 0.0000.179 0.000 832.066.460.826 0.000 0.00 0.00 180.0
High O2 Direct
3/31/2025 06:52 0.6440.000-0.001 0.000 0.7420.000 0.000 0.967 0.0000.0530.000 0.000 0.0000.000 0.000 829.00.711.059 0.000 0.64 20.73 180.0
3/31/2025 06:53 0.6680.000-0.003 0.000 0.0000.000 0.000 0.961 0.0000.0970.000 0.000 0.0000.000 0.000 829.00.791.178 0.000 0.67 20.73 180.0
3/31/2025 06:53 0.6960.000-0.004 0.000 0.4380.000 0.000 0.975 0.0000.1180.000 0.000 0.0000.000 0.000 829.00.691.029 0.000 0.70 20.73 180.0
NO2/Mid O2 Direct
3/31/2025 07:00 100.8420.000-0.003 0.000 0.4750.000 0.394 0.394 0.0000.0300.000 0.000 0.0000.000 0.000 829.00.380.563 0.000 100.84 10.49 180.0
3/31/2025 07:00 101.4220.000-0.003 0.000 0.3030.000 0.388 0.561 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.500.750 0.000 101.42 10.47 180.0
3/31/2025 07:01 102.9920.000-0.006 0.000 0.2630.000 0.391 0.655 0.0000.0150.000 0.000 0.0000.000 0.000 829.00.550.829 0.000 102.99 10.47 180.0
Spike Direct
3/31/2025 07:06 0.000253.126-0.007 4.607 5.439508.860 2.930 2.594 2.2110.2360.000 0.339 251.3650.168 1.132 829.0255.482.435 9.841 253.13 0.00 180.0
3/31/2025 07:06 0.000252.865-0.008 4.608 5.362507.915 2.947 2.475 2.0440.4330.000 0.357 251.5170.188 1.149 829.0255.662.406 9.838 252.86 0.00 180.0
3/31/2025 07:07 0.000252.824-0.006 4.606 5.275508.734 2.927 2.561 2.1670.3260.000 0.352 251.4670.255 1.122 829.0255.582.446 9.841 252.82 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
3/31/2025 07:10 0.0300.000-0.000 0.000 1.0110.000 0.000 1.122 0.0000.0050.000 0.000 0.0000.000 0.000 829.00.320.477 0.000 0.03 0.00 180.0
3/31/2025 07:11 0.0000.000-0.000 0.000 0.0000.000 0.000 1.198 0.0000.0070.000 0.000 0.0000.000 0.000 829.00.380.565 0.000 0.00 0.00 180.0
3/31/2025 07:11 0.2730.000-0.000 0.000 0.2410.000 0.000 1.227 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.440.658 0.000 0.27 0.00 180.0
CTS System with Response Time
3/31/2025 07:13 0.0000.0000.006 0.000 0.0000.000 0.000 0.544 0.2200.0060.000 98.137 0.0000.000 0.000 829.065.810.575 0.000 0.00 0.00 180.0
3/31/2025 07:13 0.0000.0780.006 0.000 0.0000.000 0.000 0.432 0.1720.0000.000 98.034 0.0000.000 0.000 829.065.760.608 0.000 0.08 0.00 180.0
3/31/2025 07:14 0.0000.2160.005 0.000 0.0000.000 0.000 0.643 0.1570.0030.000 98.012 0.0000.000 0.000 829.065.760.619 0.000 0.22 0.00 180.0
NO2/Mid O2 System with Response Time
3/31/2025 07:16 100.5050.000-0.000 0.000 0.9670.000 0.427 1.101 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.540.814 0.000 100.51 10.00 180.0
3/31/2025 07:16 100.9630.000-0.000 0.000 0.1170.000 0.429 1.128 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.510.769 0.000 100.96 10.35 180.0
3/31/2025 07:17 101.5180.000-0.000 0.000 1.1860.000 0.427 1.115 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.530.802 0.000 101.52 10.30 180.0
Spike System with Response Time
3/31/2025 07:19 0.000250.617-0.000 4.584 4.972507.334 2.894 2.548 1.8750.1630.000 0.417 251.0820.260 1.178 829.0255.322.405 9.815 250.62 0.00 180.0
3/31/2025 07:19 0.000250.906-0.000 4.593 5.173507.707 2.909 2.463 2.0020.1430.000 0.361 251.2730.388 1.161 829.0255.482.462 9.829 250.91 0.00 180.0
3/31/2025 07:19 0.000250.932-0.000 4.587 4.976507.747 2.911 2.619 1.8470.1390.000 0.429 251.2190.122 1.176 829.0255.472.416 9.810 250.93 0.00 180.0
Baseline System with Response Time
3/31/2025 07:22 0.0000.000-0.000 0.000 0.2520.000 0.000 0.954 0.0000.0010.000 0.000 0.0000.000 0.000 829.00.370.556 0.000 0.00 0.00 180.0
3/31/2025 07:23 0.7070.000-0.000 0.000 0.4830.000 0.000 1.130 0.0000.0050.000 0.000 0.0000.000 0.000 829.00.440.656 0.000 0.71 0.00 180.0
3/31/2025 07:23 0.5360.000-0.000 0.000 0.2580.000 0.000 0.942 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.470.701 0.000 0.54 0.00 180.0
Run 1 - A 30minute/60min
3/31/2025 07:43 0.00026.75710.342 7.650 58.4070.000 1.723 2.611 2.1940.4190.000 0.000 0.1930.772 0.569 829.02.081.130 0.000 26.76 0.00 180.0
3/31/2025 07:44 0.00018.56915.798 9.559 91.5221.293 1.936 3.055 2.8160.1410.568 0.000 0.0000.512 0.068 829.01.201.596 0.000 18.57 0.00 180.0
3/31/2025 07:45 0.00017.74716.627 9.498 82.7700.754 2.030 3.124 2.3390.1480.482 0.000 0.0000.560 0.055 829.01.011.347 0.000 17.75 0.00 180.0
3/31/2025 07:46 0.78718.11917.145 9.457 67.3410.794 2.307 3.935 2.6390.1800.268 0.000 0.0000.688 0.009 829.00.881.295 0.000 18.91 0.00 180.0
3/31/2025 07:47 0.86519.46818.041 9.362 71.4081.241 1.653 4.975 3.1220.2060.206 0.000 0.0000.644 0.003 829.00.871.298 0.000 20.33 0.00 180.0
3/31/2025 07:48 0.47618.32117.803 9.448 75.5621.467 2.371 5.244 3.0440.1770.474 0.000 0.0000.726 0.003 829.00.781.165 0.000 18.80 0.00 180.0
3/31/2025 07:49 0.72718.50717.725 9.517 74.6271.387 1.986 5.243 3.2050.1060.341 0.000 0.0000.765 0.009 829.00.831.217 0.000 19.23 0.00 180.0
3/31/2025 07:50 0.47718.85717.632 9.548 73.4882.195 2.458 6.182 3.0680.1360.126 0.000 0.0000.651 0.000 829.00.871.303 0.000 19.33 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/31/2025 07:51 0.79419.12817.461 9.571 74.7827.858 1.964 9.122 3.3360.1280.155 0.000 0.0000.617 0.000 829.00.881.315 0.000 19.92 0.00 180.0
3/31/2025 07:52 0.58118.45817.221 9.561 77.75910.290 2.708 10.774 3.5400.1290.152 0.000 0.0000.750 0.026 829.00.821.154 0.000 19.04 0.00 180.0
3/31/2025 07:53 0.78618.25317.163 9.554 62.5952.425 2.370 6.863 2.3930.1330.000 0.000 0.0000.754 0.000 829.00.801.204 0.000 19.04 0.00 180.0
3/31/2025 07:54 0.55518.08217.150 9.569 77.9522.679 2.563 6.828 3.2470.1030.184 0.000 0.0000.744 0.000 829.00.841.253 0.000 18.64 0.00 180.0
3/31/2025 07:55 0.38118.34717.168 9.577 69.4961.445 2.397 6.211 2.7080.1120.000 0.000 0.0000.751 0.000 829.00.831.242 0.000 18.73 0.00 180.0
3/31/2025 07:56 0.42618.35417.157 9.565 75.6680.934 2.528 5.535 2.9800.1190.099 0.000 0.0000.673 0.000 829.00.831.246 0.000 18.78 0.00 180.0
3/31/2025 07:57 0.00818.87017.148 9.579 65.7881.431 1.943 5.244 2.6180.1240.000 0.000 0.0000.676 0.000 829.00.881.315 0.000 18.88 0.00 180.0
3/31/2025 07:58 0.70418.38817.154 9.584 79.4601.569 2.395 5.277 3.3040.1290.056 0.000 0.0000.730 0.000 829.00.841.257 0.000 19.09 0.00 180.0
3/31/2025 07:59 0.63718.15417.174 9.579 76.2120.756 2.332 4.808 3.1460.1130.000 0.000 0.0000.758 0.000 829.00.851.280 0.000 18.79 0.00 180.0
3/31/2025 08:00 0.64116.90617.141 9.565 65.1730.597 1.248 5.193 2.5440.1430.051 0.000 0.0000.727 0.000 829.00.861.294 0.000 17.55 0.00 180.0
3/31/2025 08:01 0.00017.05917.150 9.577 84.1041.655 1.626 5.625 2.7450.1730.334 0.000 0.0000.520 0.015 829.01.061.549 0.000 17.06 0.00 180.0
3/31/2025 08:03 0.00016.90017.143 9.569 88.9360.937 1.457 4.849 2.9220.1590.000 0.000 0.0000.579 0.038 829.00.951.307 0.000 16.90 0.00 180.0
3/31/2025 08:04 0.74416.92317.131 9.568 78.0960.947 1.551 5.163 3.2350.1500.076 0.000 0.0000.671 0.000 829.00.841.264 0.000 17.67 0.00 180.0
3/31/2025 08:05 0.64516.82517.152 9.568 77.8500.622 1.658 5.414 3.2150.0990.095 0.000 0.0000.659 0.000 829.00.751.130 0.000 17.47 0.00 180.0
3/31/2025 08:06 0.74019.74517.156 9.576 74.3520.390 1.583 5.434 3.0750.1080.246 0.000 0.0000.642 0.000 829.00.871.300 0.000 20.48 0.00 180.0
3/31/2025 08:07 0.47616.78017.181 9.572 75.4980.859 1.684 5.749 3.0600.1210.251 0.000 0.0000.639 0.000 829.00.781.174 0.000 17.26 0.00 180.0
3/31/2025 08:08 0.00017.00417.205 9.591 84.5411.329 1.706 5.914 2.5700.1400.378 0.000 0.0000.642 0.008 829.00.831.220 0.000 17.00 0.00 180.0
3/31/2025 08:09 0.48118.38417.158 9.586 69.9172.014 2.055 6.179 2.9420.0920.000 0.000 0.0000.677 0.000 829.00.781.173 0.000 18.86 0.00 180.0
3/31/2025 08:10 0.00018.29017.142 9.579 82.9202.046 2.303 5.167 2.5800.0970.108 0.000 0.0000.610 0.029 829.00.841.177 0.000 18.29 0.00 180.0
3/31/2025 08:11 0.64816.97017.144 9.573 77.5502.587 1.625 7.010 3.3230.1070.277 0.000 0.0000.748 0.000 829.00.831.251 0.000 17.62 0.00 180.0
3/31/2025 08:12 0.51718.87317.125 9.590 77.8242.286 2.568 6.640 3.3690.1720.063 0.000 0.0000.649 0.001 829.00.881.320 0.000 19.39 0.00 180.0
3/31/2025 08:13 0.61518.92817.103 9.575 77.3451.657 2.438 6.228 3.3240.1000.102 0.000 0.0000.608 0.000 829.00.881.327 0.000 19.54 0.00 180.0
0.45718.39916.961 9.489 75.6311.881 2.039 5.653 2.9530.1420.170 0.000 0.0060.671 0.028 829.000.9081.270 0.000 18.856 0.000 180.0Avg.
Spike 1
3/31/2025 08:16 0.00037.34715.400 9.120 76.02355.336 2.442 5.112 3.9970.1470.719 0.000 22.2000.593 0.455 829.024.211.656 0.851 37.35 0.00 180.0
Run 1 - B 30minute/60min
3/31/2025 08:19 0.29222.64616.907 9.608 81.2938.122 2.380 4.463 4.3090.1120.000 0.000 1.5480.732 0.381 829.03.181.303 0.021 22.94 0.00 180.0
3/31/2025 08:20 0.18817.03517.146 9.575 88.9041.125 1.370 5.235 2.8860.1200.105 0.000 0.0000.648 0.038 829.00.901.238 0.000 17.22 0.00 180.0
3/31/2025 08:21 0.66120.01617.123 9.587 76.2070.352 1.428 4.704 3.2750.1510.000 0.000 0.0000.677 0.000 829.00.851.268 0.000 20.68 0.00 180.0
3/31/2025 08:22 0.61117.39117.191 9.625 67.3260.606 1.551 5.003 2.7630.2410.000 0.000 0.0000.718 0.000 829.00.801.195 0.000 18.00 0.00 181.0
3/31/2025 08:23 0.63216.97517.235 9.610 77.3820.647 1.450 5.200 3.1590.1520.004 0.000 0.0000.703 0.000 829.00.841.266 0.000 17.61 0.00 181.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/31/2025 08:24 0.69217.18717.218 9.588 76.4740.908 1.468 5.678 3.2090.1140.308 0.000 0.0000.638 0.000 829.00.831.241 0.000 17.88 0.00 180.0
3/31/2025 08:25 0.00016.90217.232 9.586 83.9790.502 1.353 4.668 2.6810.1150.542 0.000 0.0000.594 0.011 829.00.871.274 0.000 16.90 0.00 180.0
3/31/2025 08:26 0.79620.32017.158 9.569 78.9740.464 1.637 4.809 3.3950.1130.384 0.000 0.0000.658 0.000 829.00.861.294 0.000 21.12 0.00 180.0
3/31/2025 08:27 0.86722.19317.169 9.578 76.4900.411 2.225 4.538 3.0100.1300.000 0.000 0.0000.667 0.000 829.00.801.196 0.000 23.06 0.00 180.0
3/31/2025 08:28 0.51216.98617.201 9.566 63.7700.516 1.281 5.230 2.4160.1440.000 0.000 0.0000.612 0.000 829.00.811.221 0.000 17.50 0.00 180.0
3/31/2025 08:29 0.72117.00117.222 9.573 71.3661.798 1.494 6.322 2.8240.1210.323 0.000 0.0000.724 0.000 829.00.781.176 0.000 17.72 0.00 180.0
3/31/2025 08:30 0.76316.69017.248 9.592 74.5092.444 1.503 6.662 3.0610.1070.147 0.000 0.0000.718 0.000 829.00.751.127 0.000 17.45 0.00 180.0
3/31/2025 08:31 0.00016.94817.218 9.586 85.2952.350 1.876 6.412 2.6960.1340.419 0.000 0.0000.545 0.020 829.00.941.358 0.000 16.95 0.00 180.0
3/31/2025 08:32 0.79417.15617.197 9.583 76.3300.996 1.352 5.704 3.2290.1140.185 0.000 0.0000.660 0.000 829.00.861.288 0.000 17.95 0.00 180.0
3/31/2025 08:33 0.00017.14717.236 9.601 88.0630.576 1.577 4.800 2.8730.1150.452 0.000 0.0000.580 0.016 829.00.911.321 0.000 17.15 0.00 180.0
3/31/2025 08:34 0.77117.13117.234 9.596 70.5643.442 1.147 6.521 3.1160.1470.107 0.000 0.0000.622 0.000 829.00.771.152 0.000 17.90 0.00 180.0
3/31/2025 08:35 0.13218.68917.154 9.586 85.7224.785 2.103 5.978 2.7220.1210.055 0.000 0.0000.563 0.012 829.00.931.353 0.000 18.82 0.00 180.0
3/31/2025 08:36 0.63318.67517.166 9.581 74.9822.248 2.627 5.842 3.0810.1240.080 0.000 0.0000.762 0.000 829.00.791.187 0.000 19.31 0.00 180.0
3/31/2025 08:37 0.08718.56617.156 9.578 87.0121.737 2.377 5.670 2.7290.1110.234 0.000 0.0000.646 0.016 829.00.881.279 0.000 18.65 0.00 180.0
3/31/2025 08:38 0.77519.85517.172 9.572 73.6040.361 1.333 4.839 2.9420.0870.199 0.000 0.0000.642 0.000 829.00.861.290 0.000 20.63 0.00 180.0
3/31/2025 08:39 0.71619.48317.180 9.565 79.3290.429 1.536 4.818 3.2590.1040.310 0.000 0.0000.703 0.000 829.00.811.216 0.000 20.20 0.00 180.0
3/31/2025 08:40 0.72819.38417.213 9.583 66.9130.000 1.230 4.481 2.5280.1320.001 0.000 0.0000.686 0.000 829.00.811.214 0.000 20.11 0.00 180.0
3/31/2025 08:41 0.59916.82717.224 9.597 74.0450.912 1.495 5.267 3.0880.0970.104 0.000 0.0000.629 0.000 829.00.871.303 0.000 17.43 0.00 180.0
3/31/2025 08:42 0.05419.50917.220 9.591 60.9260.217 1.301 4.778 2.3600.1420.000 0.000 0.0000.568 0.000 829.00.841.265 0.000 19.56 0.00 180.0
3/31/2025 08:43 0.63616.78817.245 9.602 73.7461.161 1.392 5.764 3.0020.0970.130 0.000 0.0000.730 0.000 829.00.821.228 0.000 17.42 0.00 180.0
3/31/2025 08:44 0.63416.91317.172 9.575 76.3271.215 1.599 5.240 3.2260.1220.022 0.000 0.0000.708 0.001 829.00.851.269 0.000 17.55 0.00 180.0
3/31/2025 08:45 0.00018.39717.150 9.574 81.6702.569 2.423 6.246 2.4900.1750.325 0.000 0.0000.630 0.018 829.00.931.336 0.000 18.40 0.00 180.0
3/31/2025 08:46 0.77718.45017.154 9.566 69.2531.250 2.565 5.897 2.7300.1370.000 0.000 0.0000.781 0.002 829.00.831.243 0.000 19.23 0.00 180.0
3/31/2025 08:47 0.69918.24817.123 9.558 76.3522.165 2.535 6.614 3.1450.1330.002 0.000 0.0000.703 0.000 829.00.871.303 0.000 18.95 0.00 180.0
3/31/2025 08:48 0.26919.22417.148 9.567 54.6641.147 1.927 5.940 2.0610.1210.000 0.000 0.0000.674 0.000 829.00.841.256 0.000 19.49 0.00 180.0
0.50118.29117.180 9.584 75.7161.515 1.718 5.444 2.9420.1280.148 0.000 0.0520.664 0.017 829.000.9231.255 0.001 18.793 0.000 180.1Avg.
0.47918.34517.071 9.536 75.6741.698 1.878 5.549 2.9480.1350.159 0.000 0.0290.668 0.022 829.000.9151.263 0.000 18.824 0.000 180.0Run 1 Avg:
Baseline 1
3/31/2025 08:51 0.6030.0000.001 0.000 0.1340.000 0.000 1.166 0.0000.0080.000 0.000 0.0000.000 0.000 829.00.460.693 0.000 0.60 0.00 180.0
Run 2 - A 30minute/60min
3/31/2025 08:53 0.00017.36516.490 9.256 86.6541.431 2.244 4.389 2.7350.1370.000 0.000 0.0000.565 0.047 829.01.051.433 0.000 17.36 0.00 180.0
3/31/2025 08:55 0.69516.81317.151 9.565 65.3130.989 1.426 5.098 2.4640.2090.000 0.000 0.0000.705 0.000 829.00.841.253 0.000 17.51 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/31/2025 08:56 0.21216.51217.201 9.579 87.1913.288 1.762 6.862 2.6300.1480.175 0.000 0.0000.630 0.067 829.01.001.294 0.000 16.72 0.00 180.0
3/31/2025 08:57 0.23216.57917.234 9.595 83.9513.584 1.782 7.390 2.6830.1120.171 0.000 0.0000.649 0.032 829.00.951.329 0.000 16.81 0.00 180.0
3/31/2025 08:58 0.17216.75617.253 9.602 91.6733.364 1.855 6.866 2.9800.1700.455 0.000 0.0000.623 0.075 829.01.001.276 0.000 16.93 0.00 180.0
3/31/2025 08:59 0.81216.81917.204 9.578 64.3601.894 1.844 7.011 2.5630.1230.000 0.000 0.0000.670 0.000 829.00.821.233 0.000 17.63 0.00 180.0
3/31/2025 09:00 0.09816.25117.214 9.574 84.3843.473 1.399 7.135 2.5400.1110.246 0.000 0.0000.635 0.041 829.01.001.374 0.000 16.35 0.00 180.0
3/31/2025 09:01 0.77116.34617.260 9.605 76.3593.306 1.943 7.483 3.2570.1030.356 0.000 0.0000.699 0.005 829.00.871.284 0.000 17.12 0.00 180.0
3/31/2025 09:02 0.59016.41117.179 9.578 74.7372.548 1.506 7.186 3.1300.1350.000 0.000 0.0000.664 0.022 829.00.881.259 0.000 17.00 0.00 180.0
3/31/2025 09:03 0.93416.52117.163 9.567 71.1310.925 1.269 5.379 2.7960.1610.000 0.000 0.0000.672 0.012 829.00.871.270 0.000 17.45 0.00 180.0
3/31/2025 09:04 0.24116.44517.178 9.570 81.8621.518 1.636 5.714 2.2940.1530.092 0.000 0.0000.606 0.058 829.01.001.320 0.000 16.69 0.00 180.0
3/31/2025 09:05 0.00016.18017.184 9.571 81.3111.294 1.474 5.305 2.2290.1210.106 0.000 0.0000.592 0.042 829.00.971.326 0.000 16.18 0.00 180.0
3/31/2025 09:06 0.75118.97317.148 9.558 72.6640.338 1.437 4.878 2.8770.1300.000 0.000 0.0000.652 0.006 829.00.891.316 0.000 19.72 0.00 180.0
3/31/2025 09:07 0.41817.75317.118 9.575 83.1050.979 2.114 4.248 2.3120.0970.000 0.000 0.0000.718 0.045 829.01.011.383 0.000 18.17 0.00 180.0
3/31/2025 09:08 0.58417.43517.135 9.578 74.3451.167 2.189 4.757 3.0740.1580.000 0.000 0.0000.651 0.027 829.00.941.335 0.000 18.02 0.00 180.0
3/31/2025 09:09 0.60418.13717.150 9.555 66.9630.002 1.091 4.352 2.5840.1670.000 0.000 0.0000.593 0.009 829.00.971.422 0.000 18.74 0.00 180.0
3/31/2025 09:10 0.73018.63617.163 9.563 76.4400.345 1.506 4.501 3.1420.1520.051 0.000 0.0000.630 0.028 829.00.971.367 0.000 19.37 0.00 180.0
3/31/2025 09:11 0.80418.47817.164 9.570 63.5110.000 1.251 4.269 2.3500.1550.000 0.000 0.0000.642 0.023 829.00.971.381 0.000 19.28 0.00 180.0
3/31/2025 09:12 0.86618.73717.151 9.561 61.9180.000 0.923 4.272 2.3990.2330.000 0.000 0.0000.687 0.021 829.01.001.429 0.000 19.60 0.00 180.0
3/31/2025 09:13 0.68916.53717.142 9.557 68.1150.525 1.163 4.290 2.8190.2270.038 0.000 0.0000.698 0.037 829.01.061.484 0.000 17.23 0.00 180.0
3/31/2025 09:14 0.84218.61217.151 9.578 65.3381.085 1.930 4.358 2.5880.2030.000 0.000 0.0000.626 0.036 829.01.041.454 0.000 19.45 0.00 180.0
3/31/2025 09:15 0.19917.34517.139 9.570 85.4111.510 2.010 4.252 2.5490.1760.000 0.000 0.0000.642 0.074 829.01.171.537 0.000 17.54 0.00 180.0
3/31/2025 09:16 1.04418.66517.144 9.555 55.3500.000 0.913 3.625 2.1230.1940.000 0.000 0.0000.690 0.030 829.01.041.470 0.000 19.71 0.00 180.0
3/31/2025 09:17 0.98218.66117.145 9.563 68.2610.074 1.131 3.783 2.6140.2020.000 0.000 0.0000.722 0.048 829.01.081.481 0.000 19.64 0.00 180.0
3/31/2025 09:18 0.82216.38817.150 9.564 63.3941.316 1.190 5.304 2.4280.2150.000 0.000 0.0000.633 0.041 829.01.051.458 0.000 17.21 0.00 180.0
3/31/2025 09:19 0.55218.64317.148 9.564 66.2680.421 1.129 4.274 2.4370.1770.000 0.000 0.0000.663 0.059 829.01.101.475 0.000 19.19 0.00 180.0
3/31/2025 09:20 0.00018.43617.122 9.572 85.2420.705 1.799 3.502 2.4490.2040.000 0.000 0.0000.521 0.095 829.01.351.732 0.000 18.44 0.00 180.0
3/31/2025 09:21 0.86918.13417.142 9.562 74.1990.000 1.056 3.227 2.8610.0840.000 0.000 0.0000.688 0.044 829.01.001.370 0.000 19.00 0.00 180.0
3/31/2025 09:22 0.00021.46217.139 9.574 81.4340.000 1.614 2.813 2.1180.1140.000 0.000 0.0000.558 0.073 829.01.141.493 0.000 21.46 0.00 180.0
3/31/2025 09:23 0.91817.56517.159 9.554 77.7800.000 0.970 2.748 3.0050.1810.000 0.000 0.0000.689 0.050 829.01.071.451 0.000 18.48 0.00 180.0
0.54817.58717.144 9.560 74.6221.203 1.519 4.976 2.6340.1580.056 0.000 0.0000.647 0.038 829.001.0031.390 0.000 18.133 0.000 180.0Avg.
Spike 2
3/31/2025 09:25 0.00030.11414.769 8.686 66.94144.280 1.861 2.342 3.4490.1930.000 0.000 18.3900.450 0.582 829.020.721.749 0.705 30.11 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
3/31/2025 09:27 0.83820.52816.957 9.598 79.5045.219 1.803 2.324 4.0790.1590.000 0.000 0.2170.591 0.596 829.02.401.483 0.000 21.37 0.00 180.0
3/31/2025 09:28 0.72518.03517.145 9.565 71.5790.000 1.138 2.979 2.5860.2000.000 0.000 0.0000.669 0.081 829.01.121.435 0.000 18.76 0.00 180.0
3/31/2025 09:29 1.26517.46117.153 9.557 70.1120.000 0.882 2.704 2.4230.1760.000 0.000 0.0000.760 0.085 829.01.151.464 0.000 18.73 0.00 180.0
3/31/2025 09:30 0.73517.85517.181 9.580 78.2680.130 1.102 3.189 2.9200.2020.000 0.000 0.0000.737 0.098 829.01.161.440 0.000 18.59 0.00 180.0
3/31/2025 09:31 0.77218.09517.177 9.579 66.9780.306 1.082 3.533 2.3010.1460.000 0.000 0.0000.670 0.086 829.01.151.468 0.000 18.87 0.00 180.0
3/31/2025 09:32 0.65118.27917.202 9.584 72.3400.402 1.402 3.687 2.6310.2170.000 0.000 0.0000.636 0.094 829.01.141.428 0.000 18.93 0.00 180.0
3/31/2025 09:34 0.64315.72417.210 9.590 63.8240.724 0.894 3.673 2.2310.1960.000 0.000 0.0000.710 0.090 829.01.161.463 0.000 16.37 0.00 180.0
3/31/2025 09:35 0.62615.48517.191 9.583 75.9621.027 1.030 3.580 2.7710.2110.000 0.000 0.0000.632 0.097 829.01.181.473 0.000 16.11 0.00 180.0
3/31/2025 09:36 0.40617.87917.182 9.587 45.3730.000 0.946 3.158 1.3980.1850.000 0.000 0.0000.521 0.099 829.01.221.539 0.000 18.29 0.00 180.0
3/31/2025 09:37 0.59115.58817.194 9.589 68.4831.075 0.565 3.392 2.3190.2090.000 0.000 0.0000.626 0.081 829.01.141.475 0.000 16.18 0.00 180.0
3/31/2025 09:38 0.30515.60717.182 9.579 54.3141.176 0.779 3.427 1.6180.1960.000 0.000 0.0000.614 0.114 829.01.201.459 0.000 15.91 0.00 180.0
3/31/2025 09:39 0.20615.18517.165 9.568 85.4732.310 0.913 3.590 2.1410.1790.000 0.000 0.0000.588 0.137 829.01.221.416 0.000 15.39 0.00 180.0
3/31/2025 09:40 0.00017.66317.156 9.580 82.8351.142 1.920 3.047 2.0310.0940.000 0.000 0.0000.588 0.141 829.01.301.518 0.000 17.66 0.00 180.0
3/31/2025 09:41 0.16217.79817.165 9.569 63.6700.343 1.151 3.331 2.0050.1380.000 0.000 0.0000.578 0.112 829.01.131.354 0.000 17.96 0.00 180.0
3/31/2025 09:42 0.00015.16017.197 9.572 86.3602.526 1.310 4.996 2.2510.1130.000 0.000 0.0000.507 0.155 829.01.391.619 0.000 15.16 0.00 180.0
3/31/2025 09:43 0.82215.18217.208 9.576 73.7341.303 1.305 4.326 2.5740.2120.000 0.000 0.0000.665 0.100 829.01.131.400 0.000 16.00 0.00 180.0
3/31/2025 09:44 0.92116.17717.162 9.573 78.4121.698 2.219 4.120 2.9350.1710.000 0.000 0.0000.715 0.124 829.01.161.373 0.000 17.10 0.00 180.0
3/31/2025 09:45 0.45817.69617.143 9.581 47.5491.639 1.365 3.751 1.3410.2510.000 0.000 0.0000.632 0.120 829.01.171.389 0.000 18.15 0.00 180.0
3/31/2025 09:46 0.00015.11817.162 9.566 82.2223.732 1.173 5.180 1.9030.1870.000 0.000 0.0000.577 0.156 829.01.341.537 0.000 15.12 0.00 180.0
3/31/2025 09:47 0.00015.14617.155 9.558 84.4502.070 1.220 4.495 2.0460.1560.000 0.000 0.0000.601 0.177 829.01.351.495 0.000 15.15 0.00 180.0
3/31/2025 09:48 0.23917.56617.170 9.578 52.7221.800 1.586 3.852 1.5050.1390.000 0.000 0.0000.528 0.126 829.01.331.615 0.000 17.81 0.00 180.0
3/31/2025 09:49 0.16217.35417.207 9.580 61.0151.913 1.956 4.614 1.7970.1760.000 0.000 0.0000.578 0.130 829.01.251.478 0.000 17.52 0.00 180.0
3/31/2025 09:50 0.09814.91817.241 9.572 69.3260.828 1.232 4.497 2.1070.1420.000 0.000 0.0000.645 0.131 829.01.271.516 0.000 15.02 0.00 180.0
3/31/2025 09:51 0.23417.44517.189 9.571 55.3440.361 0.976 3.843 1.5390.1940.000 0.000 0.0000.562 0.124 829.01.251.505 0.000 17.68 0.00 180.0
3/31/2025 09:52 0.63615.20117.213 9.588 77.7391.083 1.210 4.092 2.5900.1450.000 0.000 0.0000.637 0.142 829.01.261.460 0.000 15.84 0.00 180.0
3/31/2025 09:53 0.28915.02317.177 9.574 57.1080.711 0.882 3.942 1.4940.1980.000 0.000 0.0000.674 0.141 829.01.271.487 0.000 15.31 0.00 180.0
3/31/2025 09:54 0.00017.16017.168 9.594 83.5812.337 1.948 4.181 1.9160.2050.000 0.000 0.0000.576 0.187 829.01.441.598 0.000 17.16 0.00 180.0
3/31/2025 09:55 0.52315.09317.192 9.589 76.2990.726 1.024 3.500 2.5960.1980.000 0.000 0.0000.600 0.159 829.01.341.531 0.000 15.62 0.00 180.0
3/31/2025 09:56 0.64417.36917.185 9.573 61.1330.304 1.092 3.361 1.7790.2260.000 0.000 0.0000.618 0.133 829.01.291.539 0.000 18.01 0.00 180.0
3/31/2025 09:57 0.00015.72817.173 9.595 82.3032.328 2.266 4.397 1.9690.1950.000 0.000 0.0000.507 0.176 829.01.511.733 0.000 15.73 0.00 180.0
0.43216.61717.173 9.578 70.2671.307 1.279 3.759 2.1930.1810.000 0.000 0.0070.618 0.140 829.001.2811.490 0.000 17.050 0.000 180.0Avg.
0.49017.10217.159 9.569 72.4451.255 1.399 4.367 2.4140.1690.028 0.000 0.0040.633 0.089 829.001.1421.440 0.000 17.592 0.000 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
3/31/2025 09:59 0.5660.0000.029 0.000 0.8020.000 0.000 1.359 0.0000.0060.000 0.000 0.0000.000 0.000 829.00.560.836 0.000 0.57 0.00 180.0
Run 3 - A 30minute/60min
3/31/2025 10:01 0.53316.49716.484 9.265 76.9490.781 1.799 2.936 2.7410.2630.000 0.000 0.0000.626 0.161 829.01.331.517 0.000 17.03 0.00 180.0
3/31/2025 10:02 0.17515.15317.123 9.561 66.4380.817 1.043 3.360 1.9980.2740.000 0.000 0.0000.633 0.168 829.01.421.625 0.000 15.33 0.00 180.0
3/31/2025 10:03 0.58314.93917.202 9.589 66.8150.606 1.106 3.553 1.9160.2680.000 0.000 0.0000.695 0.183 829.01.391.540 0.000 15.52 0.00 180.0
3/31/2025 10:04 0.68315.03717.181 9.583 76.9960.866 1.060 3.636 2.6190.2310.000 0.000 0.0000.511 0.152 829.01.361.580 0.000 15.72 0.00 180.0
3/31/2025 10:05 0.79114.72717.214 9.595 73.1611.332 1.200 3.958 2.4060.2590.000 0.000 0.0000.642 0.170 829.01.371.549 0.000 15.52 0.00 180.0
3/31/2025 10:06 0.37415.43817.229 9.596 55.7941.389 0.844 4.316 1.4780.3280.000 0.000 0.0000.623 0.185 829.01.441.601 0.000 15.81 0.00 180.0
3/31/2025 10:07 0.58315.25517.199 9.584 78.8852.105 1.475 4.980 2.7150.3330.000 0.000 0.0000.636 0.183 829.01.401.547 0.000 15.84 0.00 180.0
3/31/2025 10:09 0.68515.19517.183 9.574 71.0211.894 1.203 4.919 2.2110.2850.000 0.000 0.0000.672 0.183 829.01.401.558 0.000 15.88 0.00 180.0
3/31/2025 10:10 0.10015.00917.180 9.586 69.6670.714 1.323 4.032 2.1340.1760.000 0.000 0.0000.622 0.183 829.01.371.506 0.000 15.11 0.00 180.0
3/31/2025 10:11 0.29517.26817.178 9.591 58.5190.133 0.776 3.487 1.6830.2340.000 0.000 0.0000.611 0.168 829.01.321.475 0.000 17.56 0.00 180.0
3/31/2025 10:12 0.49714.74317.160 9.587 77.1721.020 1.363 3.928 2.5000.2190.000 0.000 0.0000.629 0.198 829.01.381.478 0.000 15.24 0.00 180.0
3/31/2025 10:13 0.24714.75917.157 9.589 61.0141.039 1.019 4.366 1.5990.2450.000 0.000 0.0000.703 0.158 829.01.221.350 0.000 15.01 0.00 180.0
3/31/2025 10:14 0.95615.68817.095 9.587 70.5331.800 1.501 4.644 2.3830.3690.000 0.000 0.0000.671 0.170 829.01.261.375 0.000 16.64 0.00 180.0
3/31/2025 10:15 0.50615.32017.149 9.619 72.9191.302 1.168 3.959 2.5090.2490.000 0.000 0.0000.766 0.180 829.01.301.405 0.000 15.83 0.00 181.0
3/31/2025 10:16 0.46215.27817.159 9.606 65.2201.382 0.883 3.912 2.0280.2430.000 0.000 0.0000.611 0.178 829.01.381.543 0.000 15.74 0.00 181.0
3/31/2025 10:17 0.77715.54517.153 9.573 71.9760.654 1.347 3.940 2.4140.2660.000 0.000 0.0000.627 0.172 829.01.371.537 0.000 16.32 0.00 180.0
3/31/2025 10:18 0.15217.64317.148 9.554 55.1160.000 1.056 3.280 1.5540.1850.000 0.000 0.0000.565 0.150 829.01.351.573 0.000 17.79 0.00 180.0
3/31/2025 10:19 0.28617.28517.183 9.569 57.6020.137 0.576 3.303 1.5990.1990.000 0.000 0.0000.634 0.165 829.01.291.435 0.000 17.57 0.00 180.0
3/31/2025 10:20 0.54415.21717.147 9.566 74.2981.502 1.161 3.922 2.5570.2190.000 0.000 0.0000.619 0.164 829.01.311.467 0.000 15.76 0.00 180.0
3/31/2025 10:21 0.20514.98117.156 9.569 63.2310.570 1.305 3.804 1.8310.2220.000 0.000 0.0000.689 0.179 829.01.301.408 0.000 15.19 0.00 180.0
3/31/2025 10:22 0.79117.21917.123 9.579 75.2620.000 0.768 2.962 2.4880.1750.000 0.000 0.0000.681 0.167 829.01.331.497 0.000 18.01 0.00 180.0
3/31/2025 10:24 0.28817.38717.123 9.580 52.3590.000 1.080 3.441 1.4180.2160.000 0.000 0.0000.630 0.169 829.01.291.432 0.000 17.67 0.00 180.0
3/31/2025 10:25 0.20416.94117.104 9.562 71.9190.122 0.942 3.059 2.1400.1500.000 0.000 0.0000.621 0.170 829.01.341.495 0.000 17.15 0.00 180.0
3/31/2025 10:26 0.20117.20717.120 9.578 64.2980.233 0.809 2.932 1.7370.2490.000 0.000 0.0000.557 0.185 828.01.351.474 0.000 17.41 0.00 180.0
3/31/2025 10:27 0.46815.10617.109 9.580 73.5810.737 1.236 3.273 2.3390.2030.000 0.000 0.0000.594 0.196 828.01.391.490 0.000 15.57 0.00 180.0
3/31/2025 10:28 0.28217.02617.121 9.589 55.1740.000 1.048 2.755 1.5410.2220.000 0.000 0.0000.549 0.172 828.01.351.511 0.000 17.31 0.00 180.0
3/31/2025 10:29 0.40516.66917.132 9.590 56.8070.000 0.662 2.815 1.4810.1820.000 0.000 0.0000.607 0.164 828.01.331.509 0.000 17.07 0.00 180.0
3/31/2025 10:30 0.63114.93117.135 9.598 77.3280.547 1.170 3.244 2.5740.2050.000 0.000 0.0000.609 0.181 828.01.351.477 0.000 15.56 0.00 180.0
3/31/2025 10:31 0.47917.31717.098 9.588 60.6070.314 1.346 3.290 1.6560.2040.000 0.000 0.0000.636 0.204 828.01.401.483 0.000 17.80 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/31/2025 10:32 0.79614.91017.094 9.583 68.6140.626 1.074 3.340 2.0840.2050.000 0.000 0.0000.661 0.186 828.01.391.525 0.000 15.71 0.00 180.0
0.46615.85617.128 9.572 67.3090.754 1.111 3.645 2.0780.2360.000 0.000 0.0000.631 0.175 828.771.3491.499 0.000 16.322 0.000 180.1Avg.
Spike 3
3/31/2025 10:36 0.00036.64715.333 9.131 66.98259.608 2.132 2.349 3.1000.2620.000 0.000 23.8540.408 0.767 828.026.762.061 0.932 36.65 0.00 180.0
Run 3 - B 30minute/60min
3/31/2025 10:38 0.32915.16717.093 9.608 70.1331.559 0.751 2.886 2.2340.2340.000 0.000 0.0000.609 0.293 828.01.631.563 0.000 15.50 0.00 180.0
3/31/2025 10:39 0.05414.89917.151 9.614 67.9080.806 1.426 3.334 1.9910.2390.000 0.000 0.0000.643 0.196 828.01.461.603 0.000 14.95 0.00 180.0
3/31/2025 10:40 0.56416.82817.169 9.608 69.8720.224 1.069 3.033 1.9780.2460.000 0.000 0.0000.590 0.224 828.01.451.496 0.000 17.39 0.00 180.0
3/31/2025 10:41 0.50915.21617.085 9.596 64.4800.888 1.987 3.305 1.7580.2490.000 0.000 0.0000.570 0.215 828.01.511.615 0.000 15.72 0.00 180.0
3/31/2025 10:43 0.44114.42617.089 9.575 71.6290.706 0.978 3.226 2.0690.2420.000 0.000 0.0000.674 0.201 828.01.391.489 0.000 14.87 0.00 180.0
3/31/2025 10:44 0.20920.03117.107 9.603 74.9120.487 1.566 2.711 2.2330.2840.000 0.000 0.0000.637 0.210 828.01.471.574 0.000 20.24 0.00 180.0
3/31/2025 10:45 0.09916.53817.132 9.584 71.0170.000 0.832 2.508 2.0000.2160.000 0.000 0.0000.594 0.215 828.01.461.543 0.000 16.64 0.00 180.0
3/31/2025 10:46 0.00016.39017.143 9.593 82.5980.000 0.740 2.323 1.5570.2120.000 0.000 0.0000.476 0.239 828.01.641.748 0.000 16.39 0.00 180.0
3/31/2025 10:47 0.49616.25717.158 9.604 72.0710.000 0.764 2.293 2.1450.1870.000 0.000 0.0000.582 0.225 828.01.491.560 0.000 16.75 0.00 180.0
3/31/2025 10:48 0.24316.26617.100 9.575 60.0390.000 0.858 2.346 1.5800.2340.000 0.000 0.0000.594 0.227 828.01.451.495 0.000 16.51 0.00 180.0
3/31/2025 10:49 0.14816.54717.104 9.578 71.7210.009 0.879 2.576 2.0100.2290.000 0.000 0.0000.664 0.217 828.01.451.516 0.000 16.69 0.00 180.0
3/31/2025 10:51 0.44016.93617.135 9.603 45.6190.000 0.690 2.612 0.9850.3030.000 0.000 0.0000.646 0.230 828.01.521.586 0.000 17.38 0.00 180.0
3/31/2025 10:52 0.473213.30417.244 9.509 40.8640.000 3.834 2.266 0.8670.2130.000 0.000 0.0000.588 0.236 828.01.411.414 0.000 213.78 0.00 180.0
3/31/2025 10:53 0.83518.15817.181 9.563 10.61830.941 0.917 2.716 0.1730.2850.000 0.000 0.0000.557 0.254 828.01.481.451 0.000 18.99 0.00 180.0
3/31/2025 10:54 0.59614.49517.196 9.583 26.95437.235 0.149 4.593 0.4090.2790.000 0.000 0.0000.566 0.305 828.01.601.479 0.000 15.09 0.00 180.0
3/31/2025 10:55 0.45614.73217.171 9.597 37.76131.061 0.728 4.321 0.6090.3170.000 0.000 0.0000.545 0.282 828.01.681.667 0.000 15.19 0.00 180.0
3/31/2025 10:56 0.34114.47217.224 9.608 57.31013.530 1.240 4.383 1.2900.2860.000 0.000 0.0000.620 0.249 828.01.501.498 0.000 14.81 0.00 180.0
3/31/2025 10:57 0.09515.07717.173 9.597 48.0925.387 0.863 3.931 1.0050.3390.000 0.000 0.0000.496 0.245 828.01.651.747 0.000 15.17 0.00 180.0
3/31/2025 10:58 0.38214.77117.178 9.604 58.9994.713 1.145 4.690 1.3720.2770.000 0.000 0.0000.591 0.247 828.01.541.561 0.000 15.15 0.00 180.0
3/31/2025 10:59 0.50714.88117.176 9.611 69.1323.485 1.321 4.595 2.0030.2560.000 0.000 0.0000.592 0.243 828.01.551.601 0.000 15.39 0.00 180.0
3/31/2025 11:00 0.53817.21317.100 9.596 40.0712.426 1.489 3.345 0.6990.3550.000 0.000 0.0000.573 0.283 828.01.601.552 0.000 17.75 0.00 180.0
3/31/2025 11:01 0.20715.11217.068 9.604 78.7977.113 2.044 5.870 2.4700.2700.000 0.000 0.0000.585 0.272 828.01.611.601 0.000 15.32 0.00 180.0
3/31/2025 11:02 0.17414.73817.090 9.597 68.1162.780 1.610 4.918 1.7450.2980.000 0.000 0.0000.556 0.270 828.01.601.586 0.000 14.91 0.00 180.0
3/31/2025 11:03 0.26514.80917.097 9.607 53.2850.722 0.925 3.510 1.2400.3040.000 0.000 0.0000.539 0.236 828.01.541.599 0.000 15.07 0.00 180.0
3/31/2025 11:04 0.44014.80317.082 9.610 73.3290.513 1.102 3.143 2.0480.2860.000 0.000 0.0000.556 0.259 828.01.521.509 0.000 15.24 0.00 180.0
3/31/2025 11:05 0.61216.71217.072 9.609 74.3640.447 1.108 3.042 2.0400.2280.000 0.000 0.0000.641 0.245 828.01.491.505 0.000 17.32 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/31/2025 11:06 0.02817.08317.068 9.634 55.8160.248 1.049 2.869 1.3340.3340.000 0.000 0.0000.565 0.244 828.01.511.535 0.000 17.11 0.00 180.0
3/31/2025 11:07 0.47215.35717.070 9.648 64.3111.373 1.264 3.882 1.6820.3230.000 0.000 0.0000.706 0.255 828.01.551.560 0.000 15.83 0.00 180.0
3/31/2025 11:08 0.49715.45317.078 9.634 73.1611.027 1.423 3.926 2.1610.3200.000 0.000 0.0000.587 0.248 828.01.581.624 0.000 15.95 0.00 180.0
3/31/2025 11:09 0.19116.51317.085 9.596 64.8280.150 1.108 3.072 1.5570.2940.000 0.000 0.0000.670 0.259 828.01.481.442 0.000 16.70 0.00 180.0
0.35522.43917.127 9.598 60.5944.928 1.195 3.408 1.5750.2710.000 0.000 0.0000.594 0.244 828.001.5271.557 0.000 22.793 0.000 180.0Avg.
0.41019.14817.128 9.585 63.9512.841 1.153 3.526 1.8260.2540.000 0.000 0.0000.612 0.209 828.381.4381.528 0.000 19.558 0.000 180.0Run 3 Avg:
Baseline 3
3/31/2025 11:23 0.6020.000-0.000 0.000 1.4190.000 0.000 1.418 0.0000.0040.000 0.000 0.0000.000 0.000 828.00.430.649 0.000 0.60 0.00 180.0
Post CTS
3/31/2025 11:26 0.0005.930-0.000 0.000 0.1310.000 0.000 0.745 0.4900.0260.000 95.570 0.0000.000 0.000 829.064.010.436 0.000 5.93 0.00 180.0
3/31/2025 11:27 0.0003.907-0.000 0.000 0.0000.000 0.000 0.244 0.2540.0120.000 98.033 0.0000.000 0.000 829.065.700.514 0.000 3.91 0.00 180.0
3/31/2025 11:27 0.0003.891-0.000 0.000 0.6120.000 0.000 0.371 0.5040.0000.000 98.145 0.0000.000 0.000 829.065.830.591 0.000 3.89 0.00 180.0
Post NO2/Mid O2
3/31/2025 11:29 100.1400.000-0.000 0.000 1.7490.000 0.430 1.380 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.450.673 0.000 100.14 10.58 180.0
3/31/2025 11:29 100.9210.000-0.000 0.000 1.4290.000 0.426 1.407 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.350.531 0.000 100.92 10.60 180.0
3/31/2025 11:29 100.7870.000-0.000 0.000 0.2960.000 0.425 1.189 0.0000.0070.000 0.000 0.0000.000 0.000 828.00.420.625 0.000 100.79 10.60 180.0
Post 5-Gas
3/31/2025 11:31 0.000248.109-0.000 4.537 6.051502.934 2.784 3.012 2.6450.2090.000 0.429 249.3400.003 1.297 824.0253.862.462 9.796 248.11 0.00 180.0
3/31/2025 11:31 0.000247.389-0.000 4.531 6.178503.477 2.767 2.905 3.0580.0930.000 0.461 249.4240.276 1.215 825.0253.912.619 9.820 247.39 0.00 180.0
3/31/2025 11:31 0.000247.559-0.000 4.518 5.959501.240 2.805 3.016 2.1520.1260.000 0.237 248.8450.213 1.548 826.0253.892.680 9.841 247.56 0.00 180.0
3/31/2025 11:31 0.000248.502-0.000 4.535 6.690504.078 2.807 3.104 2.4860.1930.000 0.357 248.9490.039 1.374 827.0253.612.513 9.780 248.50 0.00 180.0
3/31/2025 11:31 0.000248.766-0.000 4.554 5.819505.193 2.795 2.122 3.0820.1090.000 0.422 249.5840.180 1.203 828.0253.862.378 9.815 248.77 0.00 180.0
3/31/2025 11:31 0.000249.164-0.000 4.562 6.851505.746 2.770 2.192 4.5970.2180.000 0.663 250.2440.000 0.906 828.0254.272.653 9.760 249.16 0.00 180.0
3/31/2025 11:31 0.000248.475-0.000 4.537 6.076505.997 2.823 2.301 1.5990.0260.000 0.254 249.1170.230 1.554 828.0254.032.448 9.827 248.48 0.00 180.0
3/31/2025 11:31 0.000248.395-0.000 4.537 6.295505.878 2.850 2.153 2.4400.0580.000 0.310 249.0480.000 1.315 829.0253.422.299 9.802 248.39 0.00 180.0
End of Test Purge
3/31/2025 11:34 0.1090.000-0.000 0.000 1.1770.000 0.000 1.288 0.0000.0000.000 0.000 0.0000.000 0.000 833.00.260.389 0.000 0.11 0.00 180.0
3/31/2025 11:34 0.0000.000-0.000 0.000 0.9380.000 0.000 1.417 0.0000.0080.000 0.000 0.0000.000 0.000 833.00.280.419 0.000 0.00 0.00 180.0
3/31/2025 11:34 0.0690.000-0.000 0.000 1.7350.000 0.000 1.137 0.0000.0000.000 0.000 0.0000.000 0.000 833.00.230.342 0.000 0.07 0.00 180.0
3/31/2025 11:34 0.4040.000-0.000 0.000 1.3430.000 0.000 1.308 0.0000.0080.000 0.000 0.0000.000 0.000 833.00.280.420 0.000 0.40 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/31/2025 11:34 0.1350.000-0.000 0.000 0.4710.000 0.000 1.360 0.0000.0030.000 0.000 0.0000.000 0.000 833.00.410.620 0.000 0.13 0.00 180.0
3/31/2025 11:35 0.0000.000-0.000 0.000 0.8670.000 0.000 1.319 0.0000.0000.000 0.000 0.0000.000 0.000 833.00.290.436 0.000 0.00 0.00 180.0
3/31/2025 11:35 0.8630.000-0.000 0.000 1.1350.000 0.000 1.246 0.0000.0020.000 0.000 0.0000.000 0.000 833.00.290.441 0.000 0.86 0.00 180.0
3/31/2025 11:35 0.5570.000-0.000 0.000 0.8250.000 0.000 1.315 0.0000.0490.000 0.000 0.0000.000 0.000 833.00.290.430 0.000 0.56 0.00 180.0
3/31/2025 11:35 0.8690.000-0.000 0.000 0.3600.000 0.000 1.293 0.0000.0000.000 0.000 0.0000.000 0.000 833.00.320.476 0.000 0.87 0.00 180.0
3/31/2025 11:35 0.2720.000-0.000 0.000 0.4430.000 0.000 1.185 0.0000.0070.000 0.000 0.0000.000 0.000 833.00.420.636 0.000 0.27 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 4/2/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:06:55 AM 10:34 AM
Source:
Unit Number: 1452
Serial Number: WAU-1651044
Engine Hours:11520
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.752 0.332 0.040
52.760 14.191 1.798
2.000 0.300 1.000 0.150 0.700 0.030
0.153 0.068 0.008
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Lynn Huber
3
Hunter Newton
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 1452 with a serial number of WAU-1651044 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/2/2025 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2225 BHP and 1199 RPM which is 89.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1452 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1452Unit ID
Make Waukesha Site Elevation ft.5226
Model 9394 GSI Atmospheric Pressure psi.11.95
Serial Number WAU-1651044 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2225 2225 2225 2225
1200 1200 1198 1199
Percent Load %
Intake Manifold Pressure (hg)
89.00%89.00%89.00%89.00%
62.00 61.00 61.00 61.33
Intake Manifold Temperature (F)114.00 114.00 114.00 114.00
Ambient Conditions
Ambient Temperature Dry (F)21.00 24.00 31.00 25.33
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
195836.17 196183.32 196647.33 196222.27
5545.41 5555.24 5568.38 5556.34
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.17 0.17 0.17
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %16.77%16.86%16.79%16.81%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.00%0.00%0.00%0.00%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
06:55 AM 08:04 AM 09:12 AM 4/2/2025
State
NOx (mol wt) 46.01
1.448 1.565 1.475 1.496NMNEHC (ppmvw)
1.739 1.882 1.773 1.798NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
490.979 531.223 500.427 507.543 FailNMNEHC (ppbvd) @15% O2
0.008 0.009 0.008 0.0080.700 0.030 PassNMNEHC (g/hp-hr)
0.039 0.042 0.040 0.0400.170 PassNMNEHC (lbs/hr)
0.491 0.531 0.500 0.508 FailNMNEHC (ppmvd) @15% O2
0.1480.156CO (g/hp-hr)0.157 0.1532.000 0.300 Pass
CO (ppmvw)45.010 44.493 42.171 43.891
CO (ppmvd)54.081 53.516 50.682 52.760
CO (mol wt) 28.01
CO (ppmvd) @15% O2 15.267 15.108 14.307 14.894 Fail
CO (ppbvd) @15% O2 15266.979 15107.501 14307.454 14893.978 Fail
0.7240.763CO (lbs/hr)0.770 0.7521.650 Pass
NOx (g/hp-hr)0.066 0.071 0.066 0.0681.000 0.150 Pass
NOx (ppmvw)11.555 12.368 11.494 11.805
NOx (ppmvd)13.883 14.876 13.813 14.191
NOx (ppbvd) @15% O2 3919.180 4199.357 3899.427 4005.988 Fail
NOx (ppmvd) @15% O2 3.919 4.199 3.899 4.006 Fail
NOx (lbs/hr)0.325 0.348 0.324 0.3320.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
45.01
0.00
11.55 0.00 11.55
0.00%
0.00%
0.00%
16.77%
10.85 0.00 0.00%16.68%
31.65 0.00 0.00%15.22%
12.26 0.00 0.00%16.87%
0.00 0.00 0.00 0.00%0.02%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.00 0.00 0.00%0.02%
46.47 11.91 0.00 11.91 0.00%16.84%
87.15 29.31 0.00 29.31 0.00%15.32%
42.52 11.49 1.33 12.83 0.00%16.88%
0.00 0.00 0.00 0.00 0.00%0.04%
Avg. Wet 44.49 11.70 0.67 12.37 1.56 0.00%16.86%
NO2NO
0.49
1.45
23.75
1.68
0.47
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
44.31 11.41 0.01 11.42 0.00%16.77%
97.64 29.94 0.76 30.69 0.00%13.88%
40.03 11.56 0.00 11.56 0.00%16.82%
0.00 0.00 0.00 0.00 0.00%0.00%
0.00 0.00 0.00 0.00 0.47 0.00%0.04%
Avg. Wet 42.17 11.49 0.01 11.49 1.48 0.00%16.79%
NO2NO
0.47
1.48
25.91
1.47
NMNEHC
0.65
NO2
0.400.00
1.47
25.87
1.42
0.49
1.45
0.40
10.85
31.65
12.26
43.76
46.26
0.00
88.91
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.57
Yes
20.00
7.00
20.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%16.77
29.81
0.52
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.31
0.00
0.01
1010.16
0.04
29.84
29.88
928.31
1387.98
497.95
27.83
78.85
172.05
235303.65
195836.17
Run 2
16.86
29.82
0.52
11.38
0.00
0.01
1010.84
0.04
29.86
29.90
925.13
1384.80
496.18
27.83
78.40
172.03
235970.26
196183.32
Run 3
16.79
29.81
0.54
11.33
0.00
0.01
1010.16
0.04
29.84
29.88
922.06
1381.73
494.48
27.83
79.94
172.03
236335.08
196647.33
16.81
29.82
0.52
11.34
0.00
0.01
1010.39
0.04
29.85
29.89
925.17
1384.84
496.20
27.83
79.06
172.03
235869.67
196222.27
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.45
Exhaust Temp F
928.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.47
0.49
0.51
931.00
930.00
926.00
0.56
0.54
0.48
927.00
925.00
929.00
0.51
0.55
0.54
930.00
931.00
929.00
0.56 927.00
0.51
0.52
0.55
926.00
928.00
929.00
0.51
0.53
0.52
927.00
930.00
928.31
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.48
Exhaust Temp F
922.00
0.49
0.52
0.47
917.00
919.00
920.00
0.55
0.52
0.51
921.00
924.00
925.00
0.57
0.58
0.56
927.00
922.00
921.00
0.55 918.00
0.53
0.58
0.52
919.00
923.00
925.00
0.59
0.57
926.00
924.00
922.060.54
Run 2
Δpstd (in) H2O
0.56
Exhaust Temp F
925.00
0.52
0.55
0.48
927.00
922.00
921.00
0.44
0.49
0.51
926.00
925.00
930.00
0.56
0.58
0.53
920.00
921.00
927.00
0.55 928.00
0.55
0.49
0.46
929.00
930.00
921.00
0.48
0.50
926.00
924.00
0.52 925.13
Pass
Strat Check
120.971Check 1
124.414Check 2
121.898Check 3
MethaneGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.306)+ .32(0)+ .28(88.689+.005) = 29.81 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.81(1 -.16773)+ 18.0(.16773) = 27.83 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.52*√(1387.98/(29.88*27.83)) = 78.85 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.16773)78.85*2.182((528*29.88)/ (1387.98*29.92)) = 195836.17 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 195836.169/35.315 = 5545.41 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 54.081*(20.9-15)/(20.9-0%)) = 15.267 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(54.081*(1.164*10^-3)*5545.41*(Run Time/60))/2225 = .157 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .157*1/453.6*2225 = .77 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .77*4.38 = 3.373 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
54.08 = 45.01*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.79%
21.23%
10.50%
10.48%
10.58%
10.58%
10.48%10.50%
10.79%
21.23%
10.58%
20.92%
10.58%
20.92%
10.58%20.92%
0.00%
10.58%
20.92%
0.21%
0.31%
0.99%
1.48%
10.58%
Span
Zero Offset 0.00%
20.92
0.00%
10.79%1.39%1.47%0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
9
GAS
1067.0 1068.0 1068.0
1033.0 1034.0 1034.0
6.0 6.0 6.1
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
4/2/2025
5226
1452
Waukesha
Model
Serial Number
9394 GSI
WAU-1651044
Technician Hunter Newton
Run Start Times 06:55 AM 08:04 AM 09:12 AM 10:34 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1200.0 1198.0 1199.3
Engine Hours 11517 11518 11519 11520
Intake Manifold Pressure (psi)62.0 61.0 61.0 61.3
Intake Manifold Temp °F 114.0 114.0 114.0 114.0
Engine Load (BHP)2225.0 2225.0 2225.0 2225.0
Ambient Temp °F 21.0 24.0 31.0 25.3
Humidity %76.0 68.0 58.0 67.3
Dew Point °F 15.0 15.0 18.0 16.0
Waukesha
N/A
N/A
Yes
DCL DCL DCL DCL
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
Discharge Pressure (psi)
Suction Pressure (psi)
1069.0
1035.0
6.4Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
N/A N/A N/A N/A
N/A N/A N/A N/A
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.81
Average:NOx 0.80
Average:VOC 0.63
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 99.67
Tolerance 2.00%
Difference between measured and expected 0.10%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.95
Average:NOx 0.95
Average:VOC 0.75
Average:Oxygen 0.00
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 99.36
Tolerance 5.00%
Difference between measured and expected 0.21%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 247.83
Value:Spike Expected 249.80
System (Equilibration) Response Time Target (Spike)
45 secondsSystem Zero Response Time
45 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC507781 9/17/2027 102.10 10.58%
EB0115896 12/18/2027 99.57
CC440196 7/13/2032 20.92%
Cylinder # CC333629 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 249.80 501.50 254.60 9.99
Analyzer System Response 247.83 506.94 253.06 9.81
Percent Difference 0.79%1.08%0.60%1.82%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.668 5.005
Spike Direct
Propane 248.134
Mechanical
Response Time
SF6 9.830
CO 504.860
NO 252.157
Ethylene 99.356 33 seconds
Analyzer
Response
Propane 247.828
SF6 9.806
CO 506.939
NO 253.063
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 247.625
CO 505.347
NO 253.052
30 seconds
31 seconds
8.80%
8.04%
9.03%
106.28%
105.66%
104.11%
9.813
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
7
20
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
196222.27
H2O%d @ Sampling Point:16.81
CO2%d @ Sampling Point:11.34
Pressure @ Sampling Point (Pg "H2O):0.52
Temperature @ Sampling Point (Deg F):925.17
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 99.57 99.67 5.005 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.668 5.005
Spike Direct
Propane 248.134
Mechanical
Response Time
SF6 9.830
CO 504.860
NO 252.157
Ethylene 99.356 33 seconds
Analyzer
Response
Propane 247.828
SF6 9.806
CO 506.939
NO 253.063
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 247.625
CO 505.347
NO 253.052
30 seconds
31 seconds
8.80%
8.04%
9.03%
106.28%
105.66%
104.11%
9.813
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
249.800
9.988
501.500
254.600
248.134
9.830
504.860
252.157
0.67%
1.58%
0.67%
0.96%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
23.363
0.865
Dilution Factor
8.800%
Expected
21.982
% Recovery
106.280%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.790
Dilution Factor
8.037%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.888
Dilution Factor
9.034%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 23.483 22.557 104.110%
0.000320
0.000279
0.000510
0.000 21.220 20.084 105.660%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass2.37%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:40.0786404 Pass
Line Position Difference:Resolution Difference to Reference 2.37%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
99.57
99.11
0.46%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1452; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
4/2/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
4/2/2025
Hunter Newton
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1452
Make:Waukesha
Location:9394 GSIModel:
WAU-1651044Serial Number:
RAW Result Data
Stability
4/2/2025 05:54 1.2760.000-0.008 0.013 0.4042.745 0.000 0.000 0.0000.0591.387 4.679 1.8240.000 0.000 829.05.080.210 0.066 1.28 0.00 181.0
Pre Test Baseline Direct
4/2/2025 06:00 0.1630.0000.006 0.000 0.1870.000 0.000 0.887 0.0000.1230.000 0.000 0.0000.000 0.000 829.00.570.857 0.000 0.16 0.00 181.0
4/2/2025 06:00 1.1540.000-0.001 0.000 0.0810.000 0.000 0.808 0.0000.0070.000 0.000 0.0000.000 0.000 829.00.600.898 0.000 1.15 0.00 181.0
4/2/2025 06:01 1.0970.0000.001 0.000 0.0990.000 0.000 0.905 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.721.083 0.000 1.10 0.00 181.0
CTS Direct
4/2/2025 06:03 0.0000.0000.012 0.000 0.0870.000 0.000 0.309 0.0000.0000.000 99.539 0.0000.000 0.000 828.066.930.859 0.000 0.00 0.00 182.0
4/2/2025 06:04 0.0000.0000.010 0.000 0.1680.000 0.000 0.499 0.0000.0000.000 99.570 0.0000.000 0.000 828.066.980.902 0.000 0.00 0.00 181.0
4/2/2025 06:05 0.0000.0000.011 0.000 0.1340.000 0.000 0.428 0.0000.0000.000 99.895 0.0000.011 0.000 828.067.210.912 0.000 0.00 0.00 181.0
High O2 Direct
4/2/2025 06:09 1.3430.0000.002 0.000 0.1930.000 0.000 1.313 0.0000.0300.000 0.000 0.0000.000 0.000 827.00.861.284 0.000 1.34 21.18 181.0
4/2/2025 06:10 0.9550.0000.003 0.000 0.2870.000 0.000 1.334 0.0000.0420.000 0.000 0.0000.000 0.000 827.00.811.219 0.000 0.96 21.25 180.0
4/2/2025 06:10 1.1080.000-0.000 0.000 0.3300.000 0.000 1.274 0.0000.0510.000 0.000 0.0000.023 0.000 826.00.821.227 0.000 1.11 21.26 180.0
NO2/Mid O2 Direct
4/2/2025 06:14 102.5390.000-0.004 0.000 0.8600.000 0.378 1.125 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.721.082 0.000 102.54 10.82 180.0
4/2/2025 06:14 102.9190.000-0.006 0.000 0.9110.000 0.377 1.024 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.671.009 0.000 102.92 10.78 180.0
4/2/2025 06:15 104.4950.000-0.001 0.000 0.8290.000 0.304 0.997 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.721.085 0.000 104.49 10.76 180.0
Spike Direct
4/2/2025 06:18 0.000252.1670.007 4.396 5.528505.945 2.897 1.459 4.9620.4250.195 0.000 251.3140.133 0.209 823.0254.123.585 9.887 252.17 0.00 180.0
4/2/2025 06:18 0.000252.0420.002 4.540 5.694504.435 2.978 2.449 1.0370.3030.000 0.164 246.4160.479 1.514 823.0250.791.859 9.808 252.04 0.00 180.0
4/2/2025 06:19 0.000252.2620.002 4.552 5.978504.200 2.977 2.393 2.2380.2720.241 0.268 246.6730.380 1.279 823.0250.691.925 9.796 252.26 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
4/2/2025 06:22 0.9330.0000.033 0.000 0.3680.000 0.000 1.644 0.0000.0030.000 0.000 0.0000.000 0.000 823.00.721.074 0.000 0.93 0.00 180.0
4/2/2025 06:22 1.1570.0000.014 0.000 0.4800.000 0.000 1.406 0.0000.0080.000 0.000 0.0000.000 0.000 823.00.741.112 0.000 1.16 0.00 180.0
4/2/2025 06:23 0.7690.0000.008 0.000 0.5270.000 0.000 1.363 0.0000.0020.000 0.000 0.0000.000 0.000 823.00.801.195 0.000 0.77 0.00 181.0
CTS System with Response Time
4/2/2025 06:24 0.0000.0000.016 0.000 0.0880.000 0.000 0.530 0.0000.0060.000 99.267 0.0000.000 0.000 823.066.780.896 0.000 0.00 0.00 180.0
4/2/2025 06:25 0.0000.0000.016 0.000 0.0000.000 0.000 0.627 0.0000.0020.000 99.705 0.0000.000 0.000 823.067.070.896 0.000 0.00 0.00 180.0
4/2/2025 06:25 0.0000.0000.015 0.000 0.1330.000 0.000 0.302 0.0000.0120.000 99.096 0.0000.000 0.000 823.066.730.987 0.000 0.00 0.00 180.0
NO2/Mid O2 System with Response Time
4/2/2025 06:27 102.7540.000-0.000 0.000 0.0000.000 0.319 1.221 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.781.177 0.000 102.75 10.47 180.0
4/2/2025 06:28 101.4050.000-0.000 0.000 0.7330.000 0.400 1.275 0.0000.0010.000 0.000 0.0000.000 0.000 823.00.791.188 0.000 101.41 10.50 180.0
4/2/2025 06:28 101.5970.000-0.000 0.000 0.8090.000 0.328 1.316 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.711.063 0.000 101.60 10.52 180.0
Spike System with Response Time
4/2/2025 06:30 0.000252.8000.007 4.519 4.813506.870 2.791 2.114 1.4030.0860.191 0.369 247.5560.195 1.243 823.0251.611.985 9.796 252.80 0.00 180.0
4/2/2025 06:30 0.000253.0060.005 4.527 5.168506.971 2.804 2.134 1.6050.0850.256 0.386 248.0030.193 1.196 823.0252.062.107 9.814 253.01 0.00 180.0
4/2/2025 06:30 0.000253.1490.005 4.523 5.070506.901 2.816 2.268 1.4300.0920.315 0.417 247.8850.248 1.182 823.0251.831.949 9.804 253.15 0.00 180.0
4/2/2025 06:31 0.000253.2980.003 4.537 4.858507.013 2.808 2.249 1.5720.0910.101 0.402 247.8670.055 1.235 823.0251.871.890 9.808 253.30 0.00 180.0
Baseline System with Response Time
4/2/2025 06:33 0.0000.0000.001 0.000 0.7210.000 0.000 1.155 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.590.882 0.000 0.00 0.00 180.0
4/2/2025 06:34 0.5850.0000.002 0.000 0.5210.000 0.000 1.308 0.0000.0030.000 0.000 0.0000.000 0.000 823.00.660.992 0.000 0.59 0.00 180.0
4/2/2025 06:34 0.6060.0000.002 0.000 0.6270.000 0.000 1.157 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.701.055 0.000 0.61 0.00 180.0
Run 1 - A 30minute/60min
4/2/2025 06:55 0.00018.9858.612 7.639 97.15322.537 3.527 7.005 3.8260.3670.000 0.000 0.0000.571 0.407 823.01.410.895 0.000 18.98 0.00 180.0
4/2/2025 06:56 0.00010.70715.243 9.532 122.26239.593 4.532 13.586 5.8730.2100.309 0.000 0.0000.479 0.340 823.01.581.356 0.000 10.71 0.00 180.0
4/2/2025 06:57 0.0007.98815.647 9.503 117.37942.726 5.314 19.905 4.9190.2680.203 0.000 0.0000.520 0.290 824.01.461.317 0.000 7.99 0.00 180.0
4/2/2025 06:58 0.00012.05517.630 9.277 121.21245.517 4.713 25.818 5.8030.3410.563 0.000 0.0000.533 0.373 824.01.651.363 0.000 12.05 0.00 180.0
4/2/2025 06:59 0.00011.56316.649 9.427 119.79943.780 4.995 25.621 5.2360.2260.544 0.000 0.0000.531 0.313 824.01.581.433 0.000 11.56 0.00 180.0
4/2/2025 07:00 0.00011.59417.041 9.400 124.17349.680 4.178 26.113 5.9820.2540.673 0.000 0.0000.576 0.357 824.01.541.233 0.000 11.59 0.00 180.0
4/2/2025 07:01 0.00011.37717.200 9.379 116.96845.819 4.075 25.736 5.0820.2440.380 0.000 0.0000.586 0.329 824.01.471.217 0.000 11.38 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 07:02 0.00011.33317.425 9.361 123.21962.205 4.651 30.394 5.8890.2780.748 0.000 0.0000.521 0.377 824.01.651.350 0.000 11.33 0.00 180.0
4/2/2025 07:03 0.0007.93417.588 9.367 117.88242.259 4.989 28.404 5.1630.3390.597 0.000 0.0000.506 0.338 824.01.591.375 0.000 7.93 0.00 180.0
4/2/2025 07:04 0.00011.31717.616 9.380 116.38938.754 4.219 29.870 4.8360.2500.573 0.000 0.0000.520 0.302 824.01.521.372 0.000 11.32 0.00 180.0
4/2/2025 07:05 0.00011.07717.492 9.407 120.68953.512 4.767 30.154 5.5490.1950.464 0.000 0.0000.544 0.352 824.01.541.259 0.000 11.08 0.00 180.0
4/2/2025 07:06 0.00011.47717.336 9.443 122.88457.248 5.174 32.373 5.9760.2650.532 0.000 0.0000.564 0.373 824.01.471.083 0.000 11.48 0.00 180.0
4/2/2025 07:07 0.00011.91717.153 9.451 119.80651.485 5.281 30.562 5.6360.3660.185 0.000 0.0000.576 0.393 824.01.481.035 0.000 11.92 0.00 180.0
4/2/2025 07:08 0.1299.02817.058 9.435 118.99560.848 4.925 31.149 5.6150.3500.000 0.000 0.0000.630 0.383 824.01.431.004 0.000 9.16 0.00 180.0
4/2/2025 07:09 0.0008.69917.074 9.443 112.53542.644 5.706 32.014 4.7380.4100.000 0.000 0.0000.485 0.301 824.01.501.340 0.000 8.70 0.00 180.0
4/2/2025 07:10 0.0008.88017.089 9.453 120.97157.901 4.872 31.444 5.8350.3830.049 0.000 0.0000.540 0.380 824.01.581.231 0.000 8.88 0.00 180.0
4/2/2025 07:11 0.0008.79117.070 9.481 115.11236.190 4.816 25.162 5.0610.3990.086 0.000 0.0000.564 0.344 824.01.411.085 0.000 8.79 0.00 180.0
4/2/2025 07:12 0.0008.76017.022 9.479 121.89850.263 4.677 30.911 5.8050.2960.172 0.000 0.0000.547 0.387 824.01.551.161 0.000 8.76 0.00 180.0
4/2/2025 07:13 0.0008.89416.856 9.506 124.41445.700 4.725 23.989 6.3060.3060.402 0.000 0.0000.577 0.379 824.01.431.013 0.000 8.89 0.00 180.0
4/2/2025 07:14 0.0009.12816.818 9.482 125.27668.615 4.885 31.583 6.4920.2240.248 0.000 0.0000.608 0.443 823.01.530.972 0.000 9.13 0.00 180.0
4/2/2025 07:15 0.0008.94116.830 9.494 113.83432.024 5.049 22.535 4.8360.3410.195 0.000 0.0000.636 0.268 823.01.281.107 0.000 8.94 0.00 180.0
4/2/2025 07:16 0.00011.67416.852 9.487 118.68332.148 4.166 21.353 5.1360.2530.353 0.000 0.0000.616 0.273 823.01.291.114 0.000 11.67 0.00 180.0
4/2/2025 07:17 0.00012.04816.885 9.477 119.39138.563 4.391 24.494 5.2570.2460.376 0.000 0.0000.568 0.294 823.01.351.144 0.000 12.05 0.00 180.0
4/2/2025 07:18 0.00011.39616.879 9.449 121.29939.279 4.287 21.538 5.5640.2400.796 0.000 0.0000.678 0.301 824.01.371.152 0.000 11.40 0.00 180.0
4/2/2025 07:19 0.00011.40816.896 9.438 126.32940.296 4.390 21.510 6.2220.1770.819 0.000 0.0000.534 0.328 824.01.531.311 0.000 11.41 0.00 180.0
4/2/2025 07:20 0.00011.43516.898 9.456 129.10732.475 3.889 17.041 6.6990.0851.401 0.000 0.0000.563 0.348 824.01.431.097 0.000 11.43 0.00 180.0
4/2/2025 07:21 0.00011.48916.907 9.450 122.49632.057 4.240 18.174 5.7300.1410.891 0.000 0.0000.537 0.287 824.01.411.254 0.000 11.49 0.00 180.0
4/2/2025 07:23 0.00011.12816.890 9.439 124.26136.541 3.964 21.614 6.0480.1560.748 0.000 0.0000.540 0.298 824.01.451.283 0.000 11.13 0.00 180.0
4/2/2025 07:24 0.00012.21816.847 9.432 125.04445.388 4.465 22.924 6.0980.2300.724 0.000 0.0000.547 0.333 824.01.491.243 0.000 12.22 0.00 180.0
4/2/2025 07:25 0.00012.10616.873 9.437 118.00326.772 4.755 21.143 4.9650.1710.779 0.000 0.0000.563 0.220 824.01.241.193 0.000 12.11 0.00 180.0
0.00410.84516.679 9.380 119.91543.761 4.621 24.804 5.5390.2670.460 0.000 0.0000.559 0.337 823.801.4741.200 0.000 10.849 0.000 180.0Avg.
Spike 1
4/2/2025 07:28 0.00031.65215.222 8.992 115.60288.910 4.194 18.441 5.6830.1531.252 0.000 23.3630.424 0.679 824.025.871.719 0.865 31.65 0.00 180.0
Run 1 - B 30minute/60min
4/2/2025 07:30 0.00012.05716.797 9.522 126.34460.320 4.186 28.229 6.5860.1320.774 0.000 1.1580.521 0.659 824.03.421.412 0.000 12.06 0.00 180.0
4/2/2025 07:31 0.00012.40016.899 9.406 119.87155.080 4.902 33.753 5.3290.1130.486 0.000 0.0000.628 0.273 824.01.231.019 0.000 12.40 0.00 180.0
4/2/2025 07:32 0.00012.50716.935 9.414 119.39252.395 5.173 35.995 5.1420.1270.391 0.000 0.0000.512 0.257 824.01.301.182 0.000 12.51 0.00 180.0
4/2/2025 07:33 0.00012.54616.908 9.421 120.82149.137 4.588 28.622 5.6210.1300.863 0.000 0.0000.561 0.305 824.01.301.033 0.000 12.55 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 07:34 0.00012.43716.874 9.415 124.43448.964 4.471 26.732 6.0470.1240.898 0.000 0.0000.485 0.314 824.01.441.222 0.000 12.44 0.00 180.0
4/2/2025 07:35 0.00012.01216.893 9.411 126.56252.660 4.486 26.740 6.3480.1320.733 0.000 0.0000.607 0.331 824.01.300.965 0.000 12.01 0.00 180.0
4/2/2025 07:36 0.00012.73316.871 9.429 122.11550.536 4.542 29.163 5.7970.1340.957 0.000 0.0000.515 0.291 824.01.421.264 0.000 12.73 0.00 180.0
4/2/2025 07:37 0.00012.12716.898 9.426 121.07350.882 4.670 28.446 5.7380.1431.054 0.000 0.0000.592 0.312 824.01.260.959 0.000 12.13 0.00 180.0
4/2/2025 07:38 0.00012.22416.828 9.413 126.01660.870 4.696 29.049 6.4160.1050.743 0.000 0.0000.549 0.346 824.01.551.284 0.000 12.22 0.00 180.0
4/2/2025 07:39 0.00012.58716.818 9.445 127.03949.678 4.316 22.863 6.8390.1230.959 0.000 0.0000.514 0.356 824.01.631.384 0.000 12.59 0.00 180.0
4/2/2025 07:40 0.00012.04116.865 9.460 119.65340.791 4.442 24.195 5.6030.1520.997 0.000 0.0000.487 0.296 824.01.431.261 0.000 12.04 0.00 180.0
4/2/2025 07:41 0.00012.12816.842 9.442 122.80344.537 4.230 21.048 6.1760.1480.588 0.000 0.0000.547 0.320 824.01.471.243 0.000 12.13 0.00 180.0
4/2/2025 07:42 0.00012.08316.818 9.450 120.70636.664 4.337 22.241 5.6860.1740.715 0.000 0.0000.505 0.296 824.01.461.304 0.000 12.08 0.00 180.0
4/2/2025 07:43 0.00013.14716.799 9.452 125.29145.654 4.228 21.560 6.6270.1420.959 0.000 0.0000.534 0.349 824.01.591.345 0.000 13.15 0.00 180.0
4/2/2025 07:44 0.00012.45016.824 9.452 120.18428.861 4.697 20.935 5.5900.1320.898 0.000 0.0000.523 0.283 824.01.481.363 0.000 12.45 0.00 180.0
4/2/2025 07:45 0.00011.86816.877 9.456 120.67851.679 3.586 27.203 5.6770.1340.627 0.000 0.0000.587 0.286 824.01.240.995 0.000 11.87 0.00 180.0
4/2/2025 07:46 0.00012.22416.896 9.447 123.45348.881 4.602 25.845 5.9060.1381.027 0.000 0.0000.650 0.333 824.01.250.881 0.000 12.22 0.00 180.0
4/2/2025 07:47 0.00012.35516.846 9.432 119.82049.585 5.021 30.246 5.4400.1550.595 0.000 0.0000.577 0.279 824.01.281.079 0.000 12.36 0.00 180.0
4/2/2025 07:48 0.00012.98816.823 9.452 120.95245.102 4.948 26.486 5.7570.1160.884 0.000 0.0000.488 0.280 824.01.471.371 0.000 12.99 0.00 180.0
4/2/2025 07:49 0.00012.58716.861 9.449 110.49731.234 4.050 24.656 4.3760.1670.566 0.000 0.0000.529 0.226 824.01.261.219 0.000 12.59 0.00 180.0
4/2/2025 07:50 0.00011.60416.932 9.465 107.99042.726 2.848 25.156 4.2860.1320.437 0.000 0.0000.554 0.210 824.01.070.983 0.000 11.60 0.00 180.0
4/2/2025 07:51 0.00012.47416.907 9.470 116.96858.048 4.822 31.153 5.1800.1180.462 0.000 0.0000.536 0.258 824.01.361.261 0.000 12.47 0.00 180.0
4/2/2025 07:52 0.00012.28616.865 9.453 121.08838.292 4.802 24.792 5.7030.1430.589 0.000 0.0000.520 0.292 824.01.501.370 0.000 12.29 0.00 180.0
4/2/2025 07:53 0.00011.22816.917 9.442 125.97538.661 4.221 20.690 6.1640.1290.840 0.000 0.0000.572 0.322 824.01.321.018 0.000 11.23 0.00 180.0
4/2/2025 07:54 0.00011.87116.919 9.444 121.31845.431 4.116 24.574 5.6550.1870.754 0.000 0.0000.587 0.298 824.01.210.922 0.000 11.87 0.00 180.0
4/2/2025 07:55 0.00012.28416.841 9.415 115.17235.598 4.454 25.047 4.8940.1350.703 0.000 0.0000.482 0.222 824.01.361.375 0.000 12.28 0.00 180.0
4/2/2025 07:56 0.00012.20116.869 9.428 123.29951.236 4.645 28.866 5.9110.1120.736 0.000 0.0000.576 0.306 824.01.351.113 0.000 12.20 0.00 180.0
4/2/2025 07:57 0.00012.07816.907 9.441 120.67047.532 4.442 29.594 5.4830.2060.754 0.000 0.0000.554 0.275 824.01.231.018 0.000 12.08 0.00 180.0
4/2/2025 07:58 0.00012.46416.856 9.426 115.56831.334 4.497 22.226 5.0020.1660.732 0.000 0.0000.594 0.246 824.01.271.170 0.000 12.46 0.00 180.0
4/2/2025 07:59 0.00011.80816.866 9.407 118.60245.415 4.878 28.393 5.1720.1280.789 0.000 0.0000.578 0.262 824.01.180.989 0.000 11.81 0.00 180.0
0.00012.26016.868 9.440 120.81246.259 4.463 26.483 5.6720.1390.750 0.000 0.0390.549 0.303 824.001.4211.167 0.000 12.260 0.000 180.0Avg.
0.00211.55216.774 9.410 120.36445.010 4.542 25.644 5.6050.2030.605 0.000 0.0190.554 0.320 823.901.4471.183 0.000 11.555 0.000 180.0Run 1 Avg:
Baseline 1
4/2/2025 08:03 0.0000.0000.016 0.000 0.5970.000 0.000 1.786 0.0000.0010.000 0.000 0.0000.000 0.000 824.00.490.729 0.000 0.00 0.00 180.0
Run 2 - A 30minute/60min
4/2/2025 08:05 0.00011.30316.407 9.199 119.89151.786 4.511 24.321 5.4550.1640.225 0.000 0.0000.575 0.335 824.01.330.989 0.000 11.30 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 08:06 0.00011.97916.805 9.405 122.49048.294 4.740 24.625 5.7360.1500.533 0.000 0.0000.566 0.342 824.01.350.994 0.000 11.98 0.00 180.0
4/2/2025 08:07 0.00011.62716.805 9.422 123.21839.155 4.333 23.856 5.9610.1060.548 0.000 0.0000.415 0.313 824.01.551.379 0.000 11.63 0.00 180.0
4/2/2025 08:08 0.00012.54916.852 9.462 128.86052.675 4.451 20.158 6.8720.1600.832 0.000 0.0000.526 0.390 824.01.621.253 0.000 12.55 0.00 180.0
4/2/2025 08:09 0.00011.48716.893 9.466 124.09741.244 4.769 23.164 5.8190.1810.823 0.000 0.0000.628 0.323 824.01.280.957 0.000 11.49 0.00 180.0
4/2/2025 08:10 0.00011.94416.908 9.477 124.01848.273 4.667 22.874 5.9620.1710.548 0.000 0.0000.540 0.354 824.01.481.151 0.000 11.94 0.00 180.0
4/2/2025 08:11 0.00012.06216.812 9.451 118.56540.393 4.783 25.229 5.3070.1270.471 0.000 0.0000.427 0.272 824.01.461.374 0.000 12.06 0.00 180.0
4/2/2025 08:12 0.00011.81116.826 9.447 124.19142.832 4.712 25.047 6.1240.2020.566 0.000 0.0000.497 0.344 824.01.551.287 0.000 11.81 0.00 180.0
4/2/2025 08:13 0.00011.83916.878 9.456 125.79950.505 4.669 22.964 6.2910.1020.962 0.000 0.0000.527 0.347 824.01.491.199 0.000 11.84 0.00 180.0
4/2/2025 08:14 0.00011.52216.917 9.467 127.44959.554 4.351 24.131 6.7750.1730.798 0.000 0.0000.547 0.434 824.01.571.059 0.000 11.52 0.00 180.0
4/2/2025 08:15 0.00012.19516.892 9.472 123.27052.574 4.449 24.234 6.0510.1920.778 0.000 0.0000.551 0.342 824.01.361.017 0.000 12.19 0.00 180.0
4/2/2025 08:16 0.00012.24016.843 9.475 124.81545.459 4.132 20.316 6.3730.1250.702 0.000 0.0000.482 0.358 824.01.651.394 0.000 12.24 0.00 180.0
4/2/2025 08:17 0.00012.33116.854 9.466 120.02752.950 4.701 26.216 5.6490.1540.656 0.000 0.0000.547 0.321 824.01.471.243 0.000 12.33 0.00 180.0
4/2/2025 08:18 0.00011.78716.850 9.466 115.75942.222 4.036 22.567 5.4490.1410.616 0.000 0.0000.550 0.330 825.01.381.088 0.000 11.79 0.00 180.0
4/2/2025 08:19 0.00011.87516.834 9.475 119.28662.851 3.652 33.480 5.5750.1480.545 0.000 0.0000.476 0.302 824.01.481.308 0.000 11.88 0.00 180.0
4/2/2025 08:20 0.00012.53716.816 9.461 117.32863.615 4.889 37.556 5.4200.1570.294 0.000 0.0000.476 0.343 824.01.541.276 0.000 12.54 0.00 180.0
4/2/2025 08:21 0.00011.96916.867 9.478 110.65542.131 4.709 30.356 4.6210.2020.234 0.000 0.0000.605 0.279 824.01.251.033 0.000 11.97 0.00 180.0
4/2/2025 08:22 0.00012.19816.851 9.466 120.17153.005 4.740 29.462 6.0900.1720.585 0.000 0.0000.541 0.331 824.01.481.220 0.000 12.20 0.00 180.0
4/2/2025 08:23 0.00012.62916.824 9.491 123.09554.554 4.491 25.652 6.5480.2040.753 0.000 0.0000.489 0.397 824.01.711.371 0.000 12.63 0.00 180.0
4/2/2025 08:24 0.00012.35416.852 9.496 120.45452.570 4.493 24.114 6.3670.2200.757 0.000 0.0000.504 0.404 824.01.621.219 0.000 12.35 0.00 180.0
4/2/2025 08:25 0.00011.44816.849 9.468 103.85636.938 4.526 28.457 3.7410.1830.370 0.000 0.0000.633 0.244 824.01.120.950 0.000 11.45 0.00 180.0
4/2/2025 08:26 0.00011.68216.842 9.464 115.52137.939 4.656 26.587 4.9640.1600.523 0.000 0.0000.550 0.281 824.01.421.293 0.000 11.68 0.00 180.0
4/2/2025 08:27 0.00012.28916.837 9.483 119.32739.351 4.455 23.918 5.5090.1610.762 0.000 0.0000.476 0.314 824.01.551.390 0.000 12.29 0.00 180.0
4/2/2025 08:28 0.00011.62216.896 9.490 120.03943.770 4.079 23.198 5.5690.1700.517 0.000 0.0000.566 0.307 824.01.321.060 0.000 11.62 0.00 180.0
4/2/2025 08:29 0.00011.38616.914 9.487 113.99638.482 3.962 23.915 4.9790.1530.548 0.000 0.0000.589 0.270 824.01.261.077 0.000 11.39 0.00 180.0
4/2/2025 08:30 0.00012.29516.847 9.464 124.17951.737 4.069 22.776 6.4400.1410.818 0.000 0.0000.454 0.352 824.01.631.389 0.000 12.29 0.00 180.0
4/2/2025 08:31 0.00011.33916.865 9.447 122.86543.674 4.748 23.516 5.8540.1730.603 0.000 0.0000.642 0.331 824.01.310.966 0.000 11.34 0.00 180.0
4/2/2025 08:32 0.00011.94216.845 9.462 121.38634.169 4.065 20.324 5.7120.1110.827 0.000 0.0000.469 0.313 824.01.541.369 0.000 11.94 0.00 180.0
4/2/2025 08:33 0.00011.47016.882 9.459 112.44128.416 4.005 21.462 4.4100.1840.540 0.000 0.0000.558 0.245 824.01.171.016 0.000 11.47 0.00 180.0
4/2/2025 08:34 0.00011.53516.860 9.457 120.79643.009 3.886 23.985 5.6140.1380.604 0.000 0.0000.460 0.317 824.01.491.279 0.000 11.53 0.00 180.0
0.00011.90816.841 9.456 120.26146.471 4.424 24.949 5.7080.1610.611 0.000 0.0000.529 0.328 824.031.4481.187 0.000 11.908 0.000 180.0Avg.
Spike 2
4/2/2025 08:36 0.00029.31015.319 9.017 112.63987.154 4.307 22.179 5.3920.2430.899 0.000 21.2200.420 0.735 824.023.751.591 0.790 29.31 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
4/2/2025 08:38 0.00014.09116.747 9.479 122.53137.612 4.870 23.462 6.0710.1970.682 0.000 0.0850.243 0.731 824.02.271.082 0.000 14.09 0.00 180.0
4/2/2025 08:40 40.0277.61816.699 9.933 104.66629.678 4.264 31.137 10.6730.00086.679 0.000 0.0000.000 1.408 824.06.415.386 0.382 47.64 0.00 180.0
4/2/2025 08:41 0.00011.81416.903 9.465 124.74734.256 3.944 18.188 6.3580.2030.947 0.000 0.0000.492 0.371 824.01.601.284 0.000 11.81 0.00 180.0
4/2/2025 08:42 0.00011.44016.908 9.451 113.53933.113 3.459 23.138 4.5770.1970.606 0.000 0.0000.528 0.242 824.01.271.182 0.000 11.44 0.00 180.0
4/2/2025 08:43 0.00011.53616.921 9.465 118.07337.948 4.663 24.249 5.0500.1840.609 0.000 0.0000.619 0.314 824.01.391.143 0.000 11.54 0.00 180.0
4/2/2025 08:44 0.00011.75216.934 9.462 115.16738.224 4.665 27.985 4.6110.1890.274 0.000 0.0000.470 0.264 824.01.411.316 0.000 11.75 0.00 180.0
4/2/2025 08:45 0.00011.35116.883 9.442 114.36336.819 4.176 26.966 4.5440.1230.426 0.000 0.0000.630 0.286 824.01.281.066 0.000 11.35 0.00 180.0
4/2/2025 08:46 0.00011.60216.893 9.454 123.72442.310 4.286 21.287 6.0520.2260.721 0.000 0.0000.582 0.364 824.01.491.142 0.000 11.60 0.00 180.0
4/2/2025 08:47 0.00011.56116.898 9.460 121.77336.843 4.540 21.700 5.5970.1430.522 0.000 0.0000.479 0.303 824.01.541.401 0.000 11.56 0.00 180.0
4/2/2025 08:48 0.00011.49316.887 9.478 125.11439.753 4.031 20.365 6.1420.1630.555 0.000 0.0000.517 0.336 824.01.581.358 0.000 11.49 0.00 180.0
4/2/2025 08:49 0.00011.77216.859 9.492 130.66143.697 3.727 16.214 7.3790.1351.086 0.000 0.0000.422 0.436 824.01.791.370 0.000 11.77 0.00 180.0
4/2/2025 08:50 0.00011.86916.912 9.475 116.38043.738 3.501 21.444 5.4610.1810.577 0.000 0.0000.487 0.311 824.01.531.356 0.000 11.87 0.00 180.0
4/2/2025 08:51 0.00011.53616.947 9.456 116.97247.221 4.260 24.147 5.1970.1200.605 0.000 0.0000.525 0.304 824.01.401.193 0.000 11.54 0.00 180.0
4/2/2025 08:52 0.00011.86116.894 9.457 122.73649.888 3.228 21.412 6.0820.2120.811 0.000 0.0000.440 0.366 824.01.621.334 0.000 11.86 0.00 180.0
4/2/2025 08:53 0.00011.20016.923 9.470 125.95041.836 4.168 18.546 6.4670.1950.958 0.000 0.0000.517 0.407 824.01.621.215 0.000 11.20 0.00 180.0
4/2/2025 08:54 0.00011.78716.929 9.489 110.39530.276 3.834 14.801 5.4330.1150.748 0.000 0.0000.507 0.373 824.01.571.239 0.000 11.79 0.00 180.0
4/2/2025 08:55 0.00011.50016.899 9.457 95.42427.073 2.287 20.415 2.8230.1760.419 0.000 0.0000.514 0.195 824.01.301.366 0.000 11.50 0.00 180.0
4/2/2025 08:56 0.00011.19516.929 9.447 106.63050.007 2.316 26.991 4.0290.1950.364 0.000 0.0000.572 0.251 824.01.231.096 0.000 11.20 0.00 180.0
4/2/2025 08:57 0.00011.18516.921 9.458 124.95059.374 3.888 21.359 6.2740.1520.763 0.000 0.0000.582 0.394 824.01.501.063 0.000 11.18 0.00 180.0
4/2/2025 08:58 0.00012.01416.888 9.435 119.97954.666 4.242 24.785 6.0370.1440.427 0.000 0.0000.526 0.431 824.01.711.278 0.000 12.01 0.00 180.0
4/2/2025 08:59 0.00012.12616.879 9.435 97.04532.261 2.679 21.283 3.4150.2330.358 0.000 0.0000.540 0.227 824.01.331.314 0.000 12.13 0.00 180.0
4/2/2025 09:00 0.00010.97716.833 9.423 117.54167.021 2.818 29.891 5.1340.1860.337 0.000 0.0000.488 0.312 825.01.461.260 0.000 10.98 0.00 180.0
4/2/2025 09:01 0.00011.59016.845 9.426 121.87454.705 4.288 24.424 5.7790.1380.631 0.000 0.0000.519 0.383 825.01.621.278 0.000 11.59 0.00 180.0
4/2/2025 09:02 0.00011.27516.892 9.457 127.66457.731 4.158 21.778 6.7080.1680.572 0.000 0.0000.530 0.445 824.01.691.199 0.000 11.28 0.00 180.0
4/2/2025 09:03 0.00011.31916.903 9.465 117.36738.684 4.273 24.037 5.0700.1560.398 0.000 0.0000.542 0.311 824.01.481.295 0.000 11.32 0.00 180.0
4/2/2025 09:04 0.00011.46116.877 9.472 118.06340.413 3.923 21.313 5.3760.2010.526 0.000 0.0000.529 0.333 824.01.551.329 0.000 11.46 0.00 180.0
4/2/2025 09:05 0.00011.57116.857 9.464 106.51637.608 3.236 26.425 4.0630.2570.180 0.000 0.0000.480 0.268 824.01.441.351 0.000 11.57 0.00 180.0
4/2/2025 09:06 0.00011.46916.863 9.454 124.92760.781 3.751 23.173 6.2080.2330.508 0.000 0.0000.557 0.412 824.01.501.013 0.000 11.47 0.00 180.0
4/2/2025 09:07 0.00011.60916.824 9.447 120.92136.362 4.757 18.694 5.7040.2070.340 0.000 0.0000.528 0.366 825.01.571.251 0.000 11.61 0.00 180.0
4/2/2025 09:08 0.00011.20016.891 9.434 111.11335.554 4.591 29.887 4.4540.2740.142 0.000 0.0000.553 0.299 824.01.281.018 0.000 11.20 0.00 180.0
1.33411.49216.881 9.473 117.22742.515 3.894 22.983 5.5590.1773.426 0.000 0.0030.497 0.381 824.101.6811.373 0.013 12.827 0.000 180.0Avg.
0.66711.70016.861 9.465 118.74444.493 4.159 23.966 5.6330.1692.018 0.000 0.0010.513 0.355 824.071.5641.280 0.006 12.367 0.000 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
4/2/2025 09:11 0.0000.0000.040 0.000 0.6750.000 0.000 2.223 0.0000.0030.000 0.000 0.0000.000 0.000 824.00.470.708 0.000 0.00 0.00 180.0
Run 3 - A 30minute/60min
4/2/2025 09:13 0.0006.72215.031 8.546 115.50150.658 4.018 15.409 5.6810.2300.000 0.000 0.0000.408 0.452 824.01.651.120 0.000 6.72 0.00 180.0
4/2/2025 09:14 0.00011.15316.761 9.423 122.26337.327 4.330 17.580 5.6230.1940.245 0.000 0.0000.510 0.347 824.01.561.296 0.000 11.15 0.00 180.0
4/2/2025 09:15 0.00012.32616.788 9.435 119.75345.441 4.335 24.196 5.5790.2840.415 0.000 0.0000.411 0.334 824.01.611.406 0.000 12.33 0.00 180.0
4/2/2025 09:16 0.00011.99716.786 9.426 121.84153.913 4.274 26.056 5.8460.2800.386 0.000 0.0000.465 0.376 824.01.651.354 0.000 12.00 0.00 180.0
4/2/2025 09:17 0.00012.18816.824 9.473 108.74741.040 3.939 24.494 4.6340.2530.054 0.000 0.0000.359 0.329 824.01.531.306 0.000 12.19 0.00 180.0
4/2/2025 09:18 0.00011.57416.824 9.473 116.13054.131 3.214 24.308 5.2900.2700.336 0.000 0.0000.491 0.313 824.01.471.268 0.000 11.57 0.00 180.0
4/2/2025 09:19 0.00010.97816.864 9.464 118.08757.053 4.002 30.869 5.1440.2210.127 0.000 0.0000.576 0.337 824.01.290.931 0.000 10.98 0.00 180.0
4/2/2025 09:20 0.00411.29516.852 9.470 118.71450.345 4.528 26.704 5.4570.1890.097 0.000 0.0000.587 0.379 824.01.400.955 0.000 11.30 0.00 180.0
4/2/2025 09:21 0.38311.31916.889 9.483 123.41455.961 4.273 24.362 6.1450.1980.490 0.000 0.0000.567 0.428 824.01.470.914 0.000 11.70 0.00 180.0
4/2/2025 09:22 0.00011.24416.871 9.477 116.90232.691 4.813 22.642 4.9540.2000.377 0.000 0.0000.555 0.328 824.01.381.082 0.000 11.24 0.00 180.0
4/2/2025 09:23 0.00011.44816.833 9.461 117.07134.208 4.828 25.069 4.9510.2140.190 0.000 0.0000.550 0.306 824.01.531.381 0.000 11.45 0.00 180.0
4/2/2025 09:24 0.00011.83616.880 9.469 124.77345.725 4.164 22.466 6.1610.2060.584 0.000 0.0000.530 0.397 824.01.601.204 0.000 11.84 0.00 180.0
4/2/2025 09:25 0.00011.43416.810 9.448 122.36835.062 4.474 18.238 5.6400.2640.455 0.000 0.0000.541 0.367 825.01.511.162 0.000 11.43 0.00 180.0
4/2/2025 09:26 0.00011.38016.818 9.452 125.78338.600 4.335 20.350 6.1400.1850.627 0.000 0.0000.462 0.375 824.01.591.265 0.000 11.38 0.00 180.0
4/2/2025 09:27 0.00011.44216.832 9.437 120.14223.295 4.170 16.172 5.3930.1620.860 0.000 0.0000.630 0.309 824.01.311.042 0.000 11.44 0.00 180.0
4/2/2025 09:28 0.00011.36116.871 9.455 112.48721.752 4.786 17.771 4.3510.2280.281 0.000 0.0000.509 0.249 824.01.351.279 0.000 11.36 0.00 180.0
4/2/2025 09:29 0.00011.44316.832 9.452 93.15221.371 2.583 17.815 2.7830.1360.000 0.000 0.0000.542 0.171 824.01.211.297 0.000 11.44 0.00 180.0
4/2/2025 09:30 0.00011.66616.819 9.435 120.61955.959 3.108 29.646 5.4620.2470.142 0.000 0.0000.459 0.312 824.01.481.288 0.000 11.67 0.00 180.0
4/2/2025 09:31 0.00011.60416.778 9.425 118.28656.964 3.254 25.760 5.5370.1900.144 0.000 0.0000.551 0.347 824.01.561.296 0.000 11.60 0.00 180.0
4/2/2025 09:32 0.00011.61916.801 9.429 121.41956.073 4.158 25.830 5.7070.2130.194 0.000 0.0000.633 0.361 824.01.411.025 0.000 11.62 0.00 180.0
4/2/2025 09:33 0.00011.52816.801 9.433 129.01864.077 3.984 23.447 6.9660.2430.514 0.000 0.0000.590 0.457 824.01.621.061 0.000 11.53 0.00 180.0
4/2/2025 09:34 0.00012.38516.788 9.440 120.78345.210 3.702 18.369 6.2290.1740.615 0.000 0.0000.516 0.431 824.01.671.216 0.000 12.39 0.00 180.0
4/2/2025 09:35 0.00011.36516.817 9.431 118.34253.086 3.411 27.009 5.1630.2030.429 0.000 0.0000.524 0.314 824.01.421.191 0.000 11.36 0.00 180.0
4/2/2025 09:36 0.00011.62116.816 9.459 125.03540.865 4.269 18.397 6.3650.2790.483 0.000 0.0000.479 0.370 824.01.571.242 0.000 11.62 0.00 180.0
4/2/2025 09:37 0.00011.72916.815 9.466 119.64834.736 4.029 17.889 5.6750.2290.508 0.000 0.0000.492 0.307 824.01.531.371 0.000 11.73 0.00 180.0
4/2/2025 09:38 0.00011.07316.896 9.492 120.54442.320 3.572 19.625 5.7200.1330.405 0.000 0.0000.508 0.334 824.01.441.163 0.000 11.07 0.00 180.0
4/2/2025 09:39 0.00011.52516.877 9.475 121.93941.731 4.843 22.016 5.7330.2210.650 0.000 0.0000.535 0.333 824.01.461.193 0.000 11.53 0.00 180.0
4/2/2025 09:40 0.00011.56616.814 9.441 119.60041.035 4.448 23.981 5.3370.1800.535 0.000 0.0000.608 0.292 824.01.351.154 0.000 11.57 0.00 180.0
4/2/2025 09:41 0.00012.11716.854 9.466 100.72526.086 3.395 18.851 3.8690.1950.209 0.000 0.0000.574 0.241 824.01.221.100 0.000 12.12 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 09:42 0.00011.34716.863 9.445 113.18172.536 2.533 29.783 4.8620.2140.190 0.000 0.0000.572 0.294 824.01.281.041 0.000 11.35 0.00 180.0
0.01311.41016.770 9.423 118.20944.308 3.992 22.503 5.4130.2150.351 0.000 0.0000.524 0.340 824.031.4711.187 0.000 11.423 0.000 180.0Avg.
Spike 3
4/2/2025 09:43 0.75529.94013.877 8.277 103.06497.636 3.203 22.198 5.5770.2630.324 0.000 23.4830.297 0.746 824.025.911.394 0.888 30.69 0.00 180.0
Run 3 - B 30minute/60min
4/2/2025 09:47 0.00012.01816.825 9.443 122.02250.815 3.955 26.658 5.7060.1310.680 0.000 0.0000.479 0.327 824.01.491.248 0.000 12.02 0.00 180.0
4/2/2025 09:48 0.00012.27816.834 9.457 116.21546.294 4.638 25.534 4.9500.1350.435 0.000 0.0000.460 0.303 824.01.541.408 0.000 12.28 0.00 180.0
4/2/2025 09:49 0.00011.76416.853 9.453 115.85735.464 3.537 24.100 4.8970.1620.403 0.000 0.0000.460 0.273 824.01.381.251 0.000 11.76 0.00 180.0
4/2/2025 09:50 0.00011.85316.799 9.430 125.05546.680 4.057 20.280 6.2700.1300.595 0.000 0.0000.616 0.396 824.01.410.929 0.000 11.85 0.00 180.0
4/2/2025 09:51 0.00011.37816.768 9.402 115.09034.512 4.983 22.496 4.7250.1180.401 0.000 0.0000.505 0.295 824.01.381.179 0.000 11.38 0.00 180.0
4/2/2025 09:52 0.00011.35016.793 9.410 123.57037.627 3.740 21.193 6.0080.1680.790 0.000 0.0000.490 0.368 825.01.541.200 0.000 11.35 0.00 180.0
4/2/2025 09:53 0.0008.19116.775 9.414 122.31239.619 3.939 21.226 5.8460.1380.780 0.000 0.0000.391 0.348 825.01.581.331 0.000 8.19 0.00 180.0
4/2/2025 09:54 0.00011.12616.826 9.438 116.17932.221 4.048 18.172 5.1320.1290.514 0.000 0.0000.536 0.304 824.01.431.229 0.000 11.13 0.00 180.0
4/2/2025 09:55 0.00011.43416.830 9.460 119.98432.430 4.052 19.364 5.4980.1710.446 0.000 0.0000.488 0.319 824.01.541.349 0.000 11.43 0.00 180.0
4/2/2025 09:56 0.00011.95116.832 9.489 122.30436.542 4.106 17.828 5.9650.1420.606 0.000 0.0000.414 0.350 824.01.591.339 0.000 11.95 0.00 180.0
4/2/2025 09:57 0.00012.15116.842 9.487 125.56444.428 3.946 21.354 6.3350.1190.416 0.000 0.0000.511 0.371 824.01.651.357 0.000 12.15 0.00 180.0
4/2/2025 09:58 0.00011.78016.759 9.427 114.86734.339 4.421 23.525 4.7640.1480.372 0.000 0.0000.491 0.275 825.01.481.391 0.000 11.78 0.00 180.0
4/2/2025 09:59 0.00011.78516.773 9.430 125.48138.916 3.773 18.671 6.4670.1600.531 0.000 0.0000.474 0.395 825.01.681.342 0.000 11.79 0.00 180.0
4/2/2025 10:00 0.00011.99216.789 9.401 120.15651.352 4.827 31.126 5.4140.1730.339 0.000 0.0000.436 0.319 825.01.541.356 0.000 11.99 0.00 180.0
4/2/2025 10:01 0.00011.37116.790 9.417 120.02040.536 4.597 27.438 5.2990.1480.340 0.000 0.0000.513 0.277 825.01.441.329 0.000 11.37 0.00 180.0
4/2/2025 10:02 0.00012.29416.806 9.429 114.07646.870 4.875 28.143 4.9160.2090.274 0.000 0.0000.437 0.294 825.01.551.444 0.000 12.29 0.00 180.0
4/2/2025 10:03 0.00011.50516.801 9.427 122.27140.117 3.999 23.727 5.7440.1820.397 0.000 0.0000.408 0.333 825.01.591.391 0.000 11.50 0.00 180.0
4/2/2025 10:04 0.00012.12616.779 9.422 115.70332.816 4.041 21.659 5.2420.1420.415 0.000 0.0000.450 0.307 825.01.531.374 0.000 12.13 0.00 180.0
4/2/2025 10:05 0.00011.38116.837 9.433 116.60137.054 3.859 23.862 4.8390.1530.488 0.000 0.0000.505 0.275 825.01.421.300 0.000 11.38 0.00 180.0
4/2/2025 10:06 0.00011.56516.878 9.430 113.62033.913 4.598 27.141 4.4240.1870.361 0.000 0.0000.632 0.269 825.01.231.030 0.000 11.57 0.00 180.0
4/2/2025 10:07 0.00011.20616.890 9.447 123.31834.534 3.873 19.411 5.8600.1550.564 0.000 0.0000.538 0.323 825.01.411.138 0.000 11.21 0.00 180.0
4/2/2025 10:08 0.00011.76216.839 9.446 120.79935.600 3.916 19.102 5.6630.2040.637 0.000 0.0000.405 0.316 825.01.501.309 0.000 11.76 0.00 180.0
4/2/2025 10:09 0.00012.12716.815 9.427 112.60139.947 3.618 26.225 4.8680.1690.582 0.000 0.0000.504 0.302 825.01.521.372 0.000 12.13 0.00 180.0
4/2/2025 10:10 0.00011.39516.819 9.417 121.99953.167 3.760 24.754 5.5130.1500.674 0.000 0.0000.464 0.324 825.01.501.276 0.000 11.40 0.00 180.0
4/2/2025 10:11 0.00011.22016.819 9.411 118.47942.432 4.550 25.286 5.0960.1990.534 0.000 0.0000.643 0.315 825.01.280.980 0.000 11.22 0.00 180.0
4/2/2025 10:12 0.00011.50816.820 9.441 112.85832.026 3.539 20.631 4.7960.1870.393 0.000 0.0000.579 0.274 825.01.301.134 0.000 11.51 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 10:13 0.00011.69416.798 9.439 119.59540.718 3.410 22.352 5.4340.1310.458 0.000 0.0000.464 0.311 825.01.491.310 0.000 11.69 0.00 180.0
4/2/2025 10:14 0.00011.63416.817 9.447 118.37539.604 4.226 22.455 5.2330.1660.399 0.000 0.0000.490 0.322 825.01.531.324 0.000 11.63 0.00 180.0
4/2/2025 10:15 0.00011.63316.868 9.468 123.33539.103 4.188 20.355 6.0030.1820.447 0.000 0.0000.616 0.384 824.01.451.024 0.000 11.63 0.00 180.0
4/2/2025 10:16 0.00011.45816.831 9.451 123.41451.343 3.371 22.731 6.0670.1440.482 0.000 0.0000.589 0.385 825.01.390.935 0.000 11.46 0.00 180.0
0.00011.56416.817 9.436 119.39140.034 4.081 22.893 5.4320.1580.492 0.000 0.0000.500 0.322 824.671.4791.253 0.000 11.564 0.000 180.0Avg.
0.00611.48716.794 9.430 118.80042.171 4.037 22.698 5.4230.1860.422 0.000 0.0000.512 0.331 824.351.4751.220 0.000 11.494 0.000 180.0Run 3 Avg:
Baseline 3
4/2/2025 10:28 0.0000.0000.001 0.000 0.7410.000 0.000 1.471 0.0000.0140.000 0.000 0.0000.000 0.000 825.00.470.709 0.000 0.00 0.00 180.0
Post CTS
4/2/2025 10:29 0.0000.0000.014 0.000 0.0000.000 0.000 0.445 0.1730.0000.000 98.471 0.0000.000 0.000 825.066.000.532 0.000 0.00 0.00 180.0
4/2/2025 10:30 0.0000.0000.014 0.000 0.0000.000 0.000 0.737 0.2490.0180.000 99.404 0.0000.000 0.000 825.066.580.462 0.000 0.00 0.00 180.0
4/2/2025 10:30 0.0000.0000.015 0.000 0.1920.000 0.000 0.567 0.2570.0140.000 99.465 0.0000.000 0.000 825.066.410.139 0.000 0.00 0.00 180.0
Post NO2/Mid O2
4/2/2025 10:31 97.7770.0000.001 0.000 1.4680.000 0.293 1.295 0.0000.0010.000 0.000 0.0000.000 0.000 824.00.440.656 0.000 97.78 10.47 180.0
4/2/2025 10:31 100.2020.000-0.000 0.000 0.9840.000 0.388 1.427 0.0000.0130.000 0.000 0.0000.000 0.000 824.00.390.580 0.000 100.20 10.49 180.0
4/2/2025 10:32 99.2860.000-0.000 0.000 0.0000.000 0.383 1.537 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.320.476 0.000 99.29 10.47 180.0
4/2/2025 10:32 99.6020.000-0.000 0.000 0.0000.000 0.380 1.238 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.450.675 0.000 99.60 10.49 180.0
Post 5-Gas
4/2/2025 10:33 0.000251.3960.007 4.305 5.535503.508 2.746 1.471 5.2440.1540.000 0.000 249.9470.000 0.286 825.0252.993.702 9.865 251.40 0.00 180.0
4/2/2025 10:33 0.000252.2660.002 4.488 5.857505.529 2.740 2.077 3.6860.1470.121 0.493 247.1310.064 0.970 824.0250.942.318 9.795 252.27 0.00 180.0
4/2/2025 10:33 0.000252.7480.005 4.475 5.777504.596 2.763 2.376 3.0140.1490.345 0.443 246.6650.000 1.117 825.0250.431.851 9.798 252.75 0.00 180.0
4/2/2025 10:33 0.000252.2390.005 4.496 4.844505.638 2.715 2.130 3.3420.0850.159 0.460 247.5400.000 1.020 825.0251.412.280 9.825 252.24 0.00 180.0
4/2/2025 10:33 0.000252.7900.009 4.481 5.447505.926 2.728 2.256 3.1240.1840.722 0.440 247.2560.023 1.069 825.0251.022.007 9.809 252.79 0.00 180.0
4/2/2025 10:34 0.000255.3770.000 4.494 5.479506.192 2.740 2.245 3.4220.1030.219 0.434 247.7640.000 0.998 824.0251.492.156 9.821 255.38 0.00 180.0
4/2/2025 10:34 0.000254.5620.000 4.502 5.106504.754 2.729 2.156 3.2130.1150.047 0.472 247.0630.029 1.043 825.0250.842.070 9.792 254.56 0.00 180.0
4/2/2025 10:34 0.000253.0410.004 4.485 5.449506.635 2.756 2.307 2.6360.0500.262 0.468 247.6340.024 1.067 824.0251.422.014 9.795 253.04 0.00 180.0
End of Test Purge
4/2/2025 10:37 0.0000.000-0.000 0.000 1.0040.000 0.000 1.380 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.330.493 0.000 0.00 0.00 180.0
4/2/2025 10:37 0.2840.0000.004 0.000 0.7920.000 0.000 1.343 0.0000.0060.000 0.000 0.0000.000 0.000 825.00.330.501 0.000 0.28 0.00 180.0
4/2/2025 10:38 0.0000.0000.001 0.000 0.7370.000 0.000 1.368 0.0000.0020.000 0.000 0.0000.000 0.000 825.00.390.588 0.000 0.00 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 10:38 0.7120.0000.001 0.000 0.8750.000 0.000 1.411 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.280.427 0.000 0.71 0.00 180.0
4/2/2025 10:38 0.0000.0000.001 0.000 0.4670.000 0.000 1.358 0.0000.0040.000 0.000 0.0000.000 0.000 824.00.360.536 0.000 0.00 0.00 181.0
4/2/2025 10:38 0.0000.000-0.000 0.000 0.1550.000 0.000 1.412 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.370.555 0.000 0.00 0.00 180.0
4/2/2025 10:38 0.0000.000-0.000 0.000 0.6170.000 0.000 1.582 0.0000.0160.000 0.000 0.0000.024 0.000 824.00.380.573 0.000 0.00 0.00 180.0
4/2/2025 10:38 0.1820.0000.001 0.000 0.7940.000 0.000 1.310 0.0000.0020.000 0.000 0.0000.000 0.000 825.00.380.570 0.000 0.18 0.00 181.0
4/2/2025 10:38 0.3900.0000.001 0.000 0.8330.000 0.000 1.444 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.420.628 0.000 0.39 0.00 181.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 4/1/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:11:20 AM 03:07 PM
Source:
Unit Number: 1453
Serial Number: WAU-1651075
Engine Hours:11402
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.017 0.340 0.024
1.371 16.319 1.221
2.000 0.300 1.000 0.150 0.700 0.030
0.004 0.070 0.005
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Lynn Huber
3
Hunter Newton
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 1453 with a serial number of WAU-1651075 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/1/2025 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2192 BHP and 1200 RPM which is 87.67% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1453 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1453Unit ID
Make Waukesha Site Elevation ft.5226
Model 9394 GSI Atmospheric Pressure psi.12.05
Serial Number WAU-1651075 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2200 2200 2175 2192
1200 1200 1199 1200
Percent Load %
Intake Manifold Pressure (hg)
88.00%88.00%87.00%87.67%
62.00 62.00 62.00 62.00
Intake Manifold Temperature (F)120.00 118.00 119.00 119.00
Ambient Conditions
Ambient Temperature Dry (F)43.00 45.00 48.00 45.33
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
173864.62 174318.73 175300.44 174494.60
4923.25 4936.11 4963.91 4941.09
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.17 0.17 0.17
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %17.22%16.94%17.22%17.13%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.00%0.00%0.00%0.00%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
11:20 AM 12:29 PM 01:42 PM 4/1/2025
State
NOx (mol wt) 46.01
1.039 0.800 1.198 1.012NMNEHC (ppmvw)
1.255 0.963 1.447 1.221NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
354.299 271.740 408.369 344.803 FailNMNEHC (ppbvd) @15% O2
0.005 0.004 0.006 0.0050.700 0.030 PassNMNEHC (g/hp-hr)
0.025 0.019 0.029 0.0240.170 PassNMNEHC (lbs/hr)
0.354 0.272 0.408 0.345 FailNMNEHC (ppmvd) @15% O2
0.0000.000CO (g/hp-hr)0.011 0.0042.000 0.300 Pass
CO (ppmvw)3.405 0.000 0.000 1.135
CO (ppmvd)4.112 0.000 0.000 1.371
CO (mol wt) 28.01
CO (ppmvd) @15% O2 1.161 0.000 0.000 0.387 Fail
CO (ppbvd) @15% O2 1160.934 0.000 0.000 386.978 Fail
0.0000.000CO (lbs/hr)0.052 0.0171.650 Pass
NOx (g/hp-hr)0.098 0.053 0.060 0.0701.000 0.150 Pass
NOx (ppmvw)19.025 10.175 11.362 13.520
NOx (ppmvd)22.981 12.250 13.725 16.319
NOx (ppbvd) @15% O2 6487.350 3458.182 3874.479 4606.670 Fail
NOx (ppmvd) @15% O2 6.487 3.458 3.874 4.607 Fail
NOx (lbs/hr)0.477 0.255 0.287 0.3400.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
3.40
0.00
18.97 0.06 19.02
0.00%
0.00%
0.00%
17.22%
19.23 0.02 0.00%17.10%
32.44 0.00 0.00%14.31%
18.71 0.09 0.00%17.34%
0.00 0.58 0.58 0.00%0.03%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.58 0.58 0.00%0.03%
0.00 9.73 0.15 9.88 0.00%16.90%
38.85 30.46 0.00 30.46 0.00%15.11%
0.00 10.43 0.04 10.47 0.00%16.99%
0.00 0.00 0.33 0.33 0.00%0.00%
Avg. Wet 0.00 10.08 0.09 10.17 0.80 0.00%16.94%
NO2NO
0.24
0.78
20.64
0.82
0.22
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 9.63 0.01 9.64 0.00%16.93%
48.36 33.01 0.00 33.01 0.00%15.57%
0.00 13.08 0.00 13.08 0.00%17.51%
0.00 0.00 0.15 0.15 0.00%0.00%
0.00 0.00 0.33 0.33 0.22 0.00%0.00%
Avg. Wet 0.00 11.36 0.01 11.36 1.20 0.00%17.22%
NO2NO
0.21
1.26
24.02
1.14
NMNEHC
0.40
NO2
0.000.00
1.17
25.62
0.91
0.24
1.04
0.00
19.25
32.44
18.80
3.91
2.90
0.00
51.31
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.39
Yes
20.00
5.00
24.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%17.22
29.86
0.41
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.63
0.00
0.00
1002.03
0.03
29.60
29.63
903.06
1362.73
483.92
27.82
69.68
152.04
210019.47
173864.62
Run 2
16.94
29.87
0.39
11.68
0.00
0.00
997.97
0.03
29.48
29.51
898.25
1357.92
481.25
27.86
67.55
152.02
209880.96
174318.73
Run 3
17.22
29.87
0.41
11.66
0.00
0.00
1008.47
0.03
29.79
29.82
900.31
1359.98
482.40
27.83
69.11
152.02
211764.10
175300.44
17.13
29.86
0.40
11.66
0.00
0.00
1002.82
0.03
29.62
29.65
900.54
1360.21
482.52
27.83
68.80
152.02
210554.84
174494.6
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.37
Exhaust Temp F
903.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.36
0.39
0.38
899.00
898.00
904.00
0.45
0.44
0.42
909.00
901.00
902.00
0.47
0.46
0.44
897.00
898.00
904.00
0.43 906.00
0.44
0.37
0.35
909.00
903.00
902.00
0.33
0.39
0.41
908.00
906.00
903.06
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.44
Exhaust Temp F
900.00
0.38
0.35
0.41
903.00
901.00
900.00
0.46
0.36
0.38
897.00
898.00
901.00
0.41
0.44
0.47
900.00
903.00
898.00
0.38 897.00
0.40
0.39
0.42
900.00
903.00
901.00
0.43
0.39
900.00
903.00
900.310.41
Run 2
Δpstd (in) H2O
0.40
Exhaust Temp F
898.00
0.44
0.41
0.38
900.00
902.00
897.00
0.37
0.35
0.35
898.00
896.00
900.00
0.37
0.39
0.41
903.00
901.00
898.00
0.42 897.00
0.36
0.38
0.34
896.00
898.00
899.00
0.39
0.41
895.00
894.00
0.39 898.25
Pass
Strat Check
87.363Check 1
85.163Check 2
85.732Check 3
MethaneGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.63)+ .32(0)+ .28(88.37+0) = 29.86 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.86(1 -.17215)+ 18.0(.17215) = 27.82 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.41*√(1362.73/(29.63*27.82)) = 69.68 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.17215)69.68*2.182((528*29.63)/ (1362.73*29.92)) = 173864.62 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 173864.618/35.315 = 4923.251 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 4.112*(20.9-15)/(20.9-0%)) = 1.161 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(4.112*(1.164*10^-3)*4923.251*(Run Time/60))/2200 = .011 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .011*1/453.6*2200 = .052 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .052*4.38 = .228 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
4.11 = 3.4045*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.61%
21.11%
10.44%
10.41%
10.58%
10.58%
10.41%10.44%
10.61%
21.11%
10.58%
20.92%
10.58%
20.92%
10.58%20.92%
0.00%
10.58%
20.92%
0.03%
0.19%
0.13%
0.91%
10.58%
Span
Zero Offset 0.00%
20.92
0.00%
10.61%0.81%0.94%0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
9
GAS
1029.0 1027.0 1030.7
1009.0 1006.0 1011.0
5.6 5.6 5.6
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
4/1/2025
5226
1453
Waukesha
Model
Serial Number
9394 GSI
WAU-1651075
Technician Hunter Newton
Run Start Times 11:20 AM 12:29 PM 01:42 PM 03:07 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1200.0 1199.0 1199.7
Engine Hours 11399 11400 11401 11402
Intake Manifold Pressure (psi)62.0 62.0 62.0 62.0
Intake Manifold Temp °F 120.0 118.0 119.0 119.0
Engine Load (BHP)2200.0 2200.0 2175.0 2191.7
Ambient Temp °F 43.0 45.0 48.0 45.3
Humidity %43.0 42.0 43.0 42.7
Dew Point °F 22.0 28.0 30.0 26.7
Waukesha
N/A
N/A
Yes
DCL DCL DCL DCLCatalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
Discharge Pressure (psi)
Suction Pressure (psi)
1036.0
1018.0
5.6Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
N/A N/A N/A
N/A N/A N/A N/A
N/A
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.08
Average:NOx 0.08
Average:VOC 0.51
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 98.63
Tolerance 2.00%
Difference between measured and expected 0.95%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.11
Average:NOx 0.11
Average:VOC 0.58
Average:Oxygen 0.00
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 97.11
Tolerance 5.00%
Difference between measured and expected 2.47%
Pre-test System CTS & Mechanical Response Time
52 secondsEquilibration Response Time
Value:Spike Reported 252.46
Value:Spike Expected 249.80
System (Equilibration) Response Time Target (Spike)
45 secondsSystem Zero Response Time
52 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC507781 9/17/2027 102.10 10.58%
EB0115896 12/18/2027 99.57
CC440196 7/13/2032 20.92%
Cylinder # CC333629 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 249.80 501.50 254.60 9.99
Analyzer System Response 252.46 495.75 251.30 9.93
Percent Difference 1.07%1.15%1.30%0.62%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.628 4.953
Spike Direct
Propane 253.997
Mechanical
Response Time
SF6 9.896
CO 492.973
NO 250.793
Ethylene 97.110 36 seconds
Analyzer
Response
Propane 252.464
SF6 9.926
CO 495.754
NO 251.297
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 248.703
CO 491.469
NO 248.912
52 seconds
25 seconds
8.90%
7.04%
8.33%
105.94%
106.47%
103.56%
9.847
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
5
24
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
174494.6
H2O%d @ Sampling Point:17.13
CO2%d @ Sampling Point:11.66
Pressure @ Sampling Point (Pg "H2O):0.4
Temperature @ Sampling Point (Deg F):900.54
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 99.57 98.63 4.953 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.628 4.953
Spike Direct
Propane 253.997
Mechanical
Response Time
SF6 9.896
CO 492.973
NO 250.793
Ethylene 97.110 36 seconds
Analyzer
Response
Propane 252.464
SF6 9.926
CO 495.754
NO 251.297
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 248.703
CO 491.469
NO 248.912
52 seconds
25 seconds
8.90%
7.04%
8.33%
105.94%
106.47%
103.56%
9.847
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
249.800
9.988
501.500
254.600
253.997
9.896
492.973
250.793
1.68%
0.92%
1.70%
1.50%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
23.552
0.881
Dilution Factor
8.903%
Expected
22.232
% Recovery
105.940%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.697
Dilution Factor
7.043%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.824
Dilution Factor
8.327%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 21.549 20.808 103.560%
0.000345
0.000408
0.000351
0.000 18.723 17.586 106.470%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass1.10%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:38.6198488 Pass
Line Position Difference:Resolution Difference to Reference 1.10%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
99.57
97.92
1.68%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1453; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
4/1/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
4/1/2025
Hunter Newton
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1453
Make:Waukesha
Location:9394 GSIModel:
WAU-1651075Serial Number:
RAW Result Data
Stability
4/1/2025 06:00 1.9291.316-0.019 0.027 0.26511.305 0.000 0.000 0.0000.0010.000 4.981 1.5650.120 0.000 827.05.190.455 0.098 3.25 0.00 181.0
Pre Test Baseline Direct
4/1/2025 06:07 0.0000.0000.002 0.000 0.1610.000 0.000 0.797 0.0000.0000.000 0.000 0.0000.000 0.000 827.00.430.642 0.000 0.00 0.00 181.0
4/1/2025 06:07 0.0000.0000.001 0.000 0.1940.000 0.000 0.769 0.0000.0000.000 0.000 0.0000.000 0.000 827.00.550.824 0.000 0.00 0.00 181.0
4/1/2025 06:07 0.2330.000-0.000 0.000 0.3320.000 0.000 0.892 0.0000.0000.000 0.000 0.0000.000 0.000 827.00.560.846 0.000 0.23 0.00 180.0
CTS Direct
4/1/2025 06:09 0.0000.0000.011 0.000 0.0000.000 0.000 0.523 0.0000.0000.000 99.189 0.0000.000 0.000 827.066.730.894 0.000 0.00 0.00 181.0
4/1/2025 06:09 0.0000.0000.012 0.000 0.0000.000 0.000 0.417 0.0000.0000.000 98.455 0.0000.000 0.000 827.066.230.889 0.000 0.00 0.00 180.0
4/1/2025 06:10 0.0000.0000.010 0.000 0.0000.000 0.000 0.357 0.0000.0000.000 98.240 0.0000.000 0.000 827.066.120.929 0.000 0.00 0.00 180.0
High O2 Direct
4/1/2025 06:15 0.2570.0000.003 0.000 0.3460.000 0.000 1.069 0.0000.0030.000 0.000 0.0000.000 0.000 825.00.701.044 0.000 0.26 21.09 180.0
4/1/2025 06:15 0.0000.0000.003 0.000 0.0000.000 0.000 1.112 0.0000.0700.000 0.000 0.0000.000 0.000 825.00.711.068 0.000 0.00 21.11 180.0
4/1/2025 06:16 0.0000.0000.000 0.000 0.0000.000 0.000 1.127 0.0000.0450.000 0.000 0.0000.000 0.000 825.00.721.080 0.000 0.00 21.13 180.0
NO2/Mid O2 Direct
4/1/2025 06:21 100.5090.0000.002 0.000 0.2230.000 0.206 0.737 0.0000.0570.000 0.000 0.0000.000 0.000 824.00.310.462 0.000 100.51 10.62 180.0
4/1/2025 06:21 102.1030.0000.001 0.000 0.2100.000 0.212 0.848 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.370.551 0.000 102.10 10.60 180.0
4/1/2025 06:22 102.4060.000-0.000 0.000 0.1500.000 0.238 0.854 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.490.738 0.000 102.41 10.60 180.0
Spike Direct
4/1/2025 06:24 0.000250.4410.008 4.412 5.050492.188 2.922 1.521 3.4810.2810.000 0.000 254.8520.200 0.498 817.0258.273.636 9.884 250.44 0.00 180.0
4/1/2025 06:25 0.000250.8040.006 4.403 5.335492.338 2.909 1.574 3.8170.3480.261 0.000 255.0530.168 0.343 817.0258.223.720 9.897 250.80 0.00 180.0
4/1/2025 06:26 0.000251.1350.007 4.413 5.284494.392 2.864 1.450 4.3490.2820.000 0.000 252.0850.131 0.253 821.0255.153.839 9.906 251.14 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
4/1/2025 06:28 0.0000.0000.016 0.000 0.0000.000 0.000 1.293 0.0000.0000.000 0.000 0.0000.000 0.000 821.00.540.813 0.000 0.00 0.00 180.0
4/1/2025 06:29 0.1860.0000.010 0.000 0.7570.000 0.000 1.265 0.0000.0040.000 0.000 0.0000.000 0.000 820.00.590.883 0.000 0.19 0.00 180.0
4/1/2025 06:29 0.1450.0000.006 0.000 0.5630.000 0.000 1.178 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.610.917 0.000 0.14 0.00 180.0
CTS System with Response Time
4/1/2025 06:30 0.0000.0000.016 0.000 0.0000.000 0.000 0.568 0.0000.0040.000 96.937 0.0000.000 0.000 820.065.180.828 0.000 0.00 0.00 180.0
4/1/2025 06:31 0.0000.0000.017 0.000 0.0000.000 0.000 0.728 0.0000.0020.000 97.245 0.0000.000 0.000 820.065.410.858 0.000 0.00 0.00 180.0
4/1/2025 06:31 0.0000.0000.015 0.000 0.0000.000 0.000 0.641 0.0000.0040.000 97.148 0.0000.000 0.000 820.065.310.817 0.000 0.00 0.00 180.0
NO2/Mid O2 System with Response Time
4/1/2025 06:34 99.8960.000-0.000 0.000 0.0000.000 0.237 1.217 0.0000.0010.000 0.000 0.0000.000 0.000 820.00.510.764 0.000 99.90 10.43 181.0
4/1/2025 06:34 102.2520.000-0.000 0.000 1.1590.000 0.249 1.074 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.540.809 0.000 102.25 10.44 181.0
4/1/2025 06:34 102.0870.000-0.000 0.000 0.9340.000 0.364 1.244 0.0000.0020.000 0.000 0.0000.000 0.000 820.00.540.816 0.000 102.09 10.44 181.0
Spike System with Response Time
4/1/2025 06:37 0.000251.1000.010 4.407 5.416495.722 2.832 1.377 3.8790.0720.363 0.000 252.6240.220 0.327 820.0255.923.972 9.930 251.10 0.00 180.0
4/1/2025 06:37 0.000251.1210.009 4.416 5.423495.911 2.832 1.347 3.9600.1380.072 0.000 252.3550.030 0.304 820.0255.573.917 9.921 251.12 0.00 180.0
4/1/2025 06:37 0.000251.6710.009 4.406 5.372495.628 2.844 1.314 3.9550.1410.000 0.000 252.4120.040 0.362 820.0255.733.896 9.926 251.67 0.00 180.0
Baseline System with Response Time
4/1/2025 06:39 0.0000.0000.001 0.000 0.0280.000 0.000 1.223 0.0000.0030.000 0.000 0.0000.000 0.000 820.00.410.615 0.000 0.00 0.00 180.0
4/1/2025 06:40 0.0000.0000.002 0.000 0.0000.000 0.000 1.283 0.0000.0030.000 0.000 0.0000.000 0.000 820.00.380.563 0.000 0.00 0.00 180.0
4/1/2025 06:40 0.0000.0000.002 0.000 0.0000.000 0.000 1.270 0.0000.0020.000 0.000 0.0000.000 0.000 820.00.400.601 0.000 0.00 0.00 180.0
Run 1 - A 30minute/60min
4/1/2025 11:20 0.00022.54111.343 7.535 80.7470.000 4.640 2.995 2.9690.3390.000 0.000 0.0000.596 0.422 819.01.440.889 0.000 22.54 0.00 180.0
4/1/2025 11:21 0.00013.52916.284 9.678 79.9330.000 5.490 2.826 2.7540.1190.098 0.000 0.0000.521 0.181 819.01.261.348 0.000 13.53 0.00 180.0
4/1/2025 11:22 0.24313.55216.780 9.636 79.9630.000 4.604 3.459 2.6540.1350.120 0.000 0.0000.546 0.153 819.01.151.267 0.000 13.79 0.00 180.0
4/1/2025 11:23 0.00014.37017.117 9.623 89.8830.000 5.643 3.847 2.1720.1130.137 0.000 0.0000.392 0.185 819.01.351.468 0.000 14.37 0.00 180.0
4/1/2025 11:24 0.00013.82717.370 9.606 83.2630.000 4.999 3.957 1.7540.0840.000 0.000 0.0000.518 0.168 819.01.241.357 0.000 13.83 0.00 180.0
4/1/2025 11:25 0.00016.13017.442 9.633 100.0640.000 6.261 5.909 2.9500.0990.150 0.000 0.0000.343 0.211 819.01.431.513 0.000 16.13 0.00 180.0
4/1/2025 11:26 0.00013.41917.559 9.638 79.2020.000 5.729 4.504 2.5930.1080.176 0.000 0.0000.656 0.139 820.00.991.067 0.000 13.42 0.00 180.0
4/1/2025 11:27 0.00013.35217.594 9.676 91.3500.000 4.427 3.577 2.2190.0920.000 0.000 0.0000.415 0.160 819.01.321.495 0.000 13.35 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 11:28 0.00011.80817.623 9.664 95.2874.026 5.270 8.081 2.4450.0770.183 0.000 0.0000.448 0.158 819.01.261.414 0.000 11.81 0.00 180.0
4/1/2025 11:29 0.00013.78817.650 9.630 109.75948.592 6.882 27.111 4.3380.1290.197 0.000 0.0000.435 0.301 819.01.401.196 0.000 13.79 0.00 180.0
4/1/2025 11:31 0.00015.75217.456 9.599 92.9388.432 9.020 12.062 2.6920.1000.000 0.000 0.0000.354 0.212 819.01.391.448 0.000 15.75 0.00 180.0
4/1/2025 11:32 0.00016.51517.458 9.606 78.5120.000 6.268 8.835 2.7220.1120.042 0.000 0.0000.592 0.152 820.01.001.044 0.000 16.52 0.00 180.0
4/1/2025 11:33 0.00016.32417.408 9.599 91.2880.000 7.254 8.272 2.3500.1380.084 0.000 0.0000.562 0.199 819.01.191.187 0.000 16.32 0.00 180.0
4/1/2025 11:34 0.00016.00517.377 9.593 87.9290.000 6.439 7.994 1.9960.1250.098 0.000 0.0000.486 0.160 820.01.221.347 0.000 16.00 0.00 180.0
4/1/2025 11:35 0.00014.79817.381 9.627 91.1900.000 5.459 6.188 2.5150.1280.117 0.000 0.0000.475 0.175 819.01.261.368 0.000 14.80 0.00 180.0
4/1/2025 11:36 0.00016.43017.386 9.650 97.5470.000 6.304 7.335 3.0240.0990.222 0.000 0.0000.474 0.211 819.01.311.336 0.000 16.43 0.00 180.0
4/1/2025 11:37 0.20214.99217.410 9.682 79.4270.000 5.141 5.344 3.1310.1310.236 0.000 0.0000.644 0.151 819.01.061.137 0.000 15.19 0.00 180.0
4/1/2025 11:38 0.000139.33817.360 9.686 59.8290.000 8.812 4.235 2.1460.1340.000 0.000 0.0000.570 0.094 819.00.901.072 0.000 139.34 0.00 180.0
4/1/2025 11:39 0.00017.80017.231 9.688 12.8140.000 0.887 3.025 0.4180.2260.000 0.000 0.0000.384 0.116 819.00.971.112 0.000 17.80 0.00 180.0
4/1/2025 11:40 0.00012.76617.199 9.685 32.50520.811 2.021 3.450 0.9210.1840.000 0.000 0.0000.461 0.136 819.01.061.181 0.000 12.77 0.00 180.0
4/1/2025 11:41 0.00013.13217.160 9.623 56.22818.297 4.464 5.389 1.6080.1310.000 0.000 0.0000.573 0.126 821.00.981.094 0.000 13.13 0.00 180.0
4/1/2025 11:42 0.00013.74417.218 9.647 84.87410.453 6.387 7.247 2.0770.1400.017 0.000 0.0000.490 0.168 819.01.231.341 0.000 13.74 0.00 180.0
4/1/2025 11:43 0.00013.48817.251 9.656 82.8252.047 5.738 6.819 2.0970.2330.198 0.000 0.0000.552 0.164 819.01.201.311 0.000 13.49 0.00 180.0
4/1/2025 11:44 0.00016.48017.209 9.639 91.7550.000 6.800 6.338 2.4800.1380.417 0.000 0.0000.560 0.143 819.01.051.141 0.000 16.48 0.00 180.0
4/1/2025 11:45 0.00017.14617.227 9.629 83.0430.000 5.629 5.382 2.3860.1110.382 0.000 0.0000.506 0.158 819.01.181.297 0.000 17.15 0.00 180.0
4/1/2025 11:46 0.00016.37217.257 9.624 88.1440.000 6.169 6.860 2.2590.1280.467 0.000 0.0000.470 0.139 819.01.111.242 0.000 16.37 0.00 180.0
4/1/2025 11:47 0.00013.67117.249 9.622 103.2364.512 7.426 9.313 3.5050.1040.706 0.000 0.0000.540 0.176 819.01.151.192 0.000 13.67 0.00 180.0
4/1/2025 11:48 0.00015.87517.276 9.653 91.9930.000 7.354 7.383 2.4710.1100.798 0.000 0.0000.527 0.102 819.01.051.274 0.000 15.87 0.00 180.0
4/1/2025 11:49 0.25914.47317.286 9.646 76.9840.000 5.335 5.053 2.7870.1490.692 0.000 0.0000.617 0.095 819.00.850.986 0.000 14.73 0.00 180.0
4/1/2025 11:50 0.00015.43617.298 9.641 94.8880.000 5.640 5.940 2.7340.1120.882 0.000 0.0000.481 0.120 819.01.041.204 0.000 15.44 0.00 180.0
0.02319.22817.095 9.570 82.2473.906 5.750 6.624 2.4390.1340.214 0.000 0.0000.506 0.169 819.171.1681.244 0.000 19.252 0.000 180.0Avg.
Spike 1
4/1/2025 11:52 0.00032.43814.307 8.503 81.73751.305 6.760 4.682 4.2210.1450.944 0.000 23.5520.348 0.569 819.025.621.399 0.881 32.44 0.00 180.0
Run 1 - B 30minute/60min
4/1/2025 11:55 0.00013.80717.295 9.653 84.9540.000 5.279 4.207 1.9930.1190.857 0.000 0.0000.466 0.091 819.01.001.232 0.000 13.81 0.00 180.0
4/1/2025 11:56 0.00015.22617.275 9.646 92.5050.000 6.802 6.162 2.6810.1021.072 0.000 0.0000.489 0.085 819.01.011.261 0.000 15.23 0.00 180.0
4/1/2025 11:57 0.00015.49617.258 9.644 95.6550.000 6.170 5.483 2.9210.0991.088 0.000 0.0000.543 0.096 819.00.991.196 0.000 15.50 0.00 180.0
4/1/2025 11:58 0.00014.71917.260 9.641 84.2390.000 4.898 4.774 2.0830.1140.842 0.000 0.0000.487 0.076 819.00.951.191 0.000 14.72 0.00 180.0
4/1/2025 11:59 0.00015.55717.256 9.637 97.0600.000 6.044 5.464 3.0570.1241.258 0.000 0.0000.514 0.097 819.00.991.198 0.000 15.56 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 12:00 0.00014.96917.270 9.640 85.0400.000 5.496 4.686 2.1520.1080.952 0.000 0.0000.541 0.083 819.00.961.191 0.000 14.97 0.00 180.0
4/1/2025 12:01 0.00015.67117.299 9.657 103.0330.000 6.394 5.167 3.5960.1041.258 0.000 0.0000.507 0.099 819.00.991.187 0.000 15.67 0.00 180.0
4/1/2025 12:02 0.00015.88817.332 9.663 99.8310.000 7.037 5.491 3.2830.1541.439 0.000 0.0000.506 0.096 819.01.021.241 0.000 15.89 0.00 180.0
4/1/2025 12:03 0.00015.12217.298 9.640 91.7550.000 6.929 5.382 2.5580.1311.234 0.000 0.0000.490 0.081 819.00.961.200 0.000 15.12 0.00 180.0
4/1/2025 12:04 0.13314.99217.284 9.663 78.1130.000 5.732 5.124 2.8790.0921.116 0.000 0.0000.627 0.029 819.00.670.913 0.000 15.12 0.00 180.0
4/1/2025 12:05 0.00017.51717.284 9.633 86.1040.000 6.853 8.530 2.3400.1170.998 0.000 0.0000.440 0.053 819.00.901.185 0.000 17.52 0.00 180.0
4/1/2025 12:06 0.00017.38717.276 9.686 87.6520.000 6.651 7.133 2.4820.0921.231 0.000 0.0000.462 0.065 818.00.991.292 0.000 17.39 0.00 180.0
4/1/2025 12:08 0.00014.06117.203 9.717 99.58029.198 6.739 23.099 3.5130.1621.060 0.000 0.0000.458 0.116 816.01.051.221 0.000 14.06 0.00 180.0
4/1/2025 12:09 0.00017.69817.201 9.662 101.13322.878 9.665 17.905 3.8290.2121.280 0.000 0.0000.443 0.157 819.01.111.196 0.000 17.70 0.00 180.0
4/1/2025 12:10 0.00015.26617.261 9.659 98.2051.988 7.969 9.006 3.1700.1761.447 0.000 0.0000.411 0.121 819.01.051.212 0.000 15.27 0.00 180.0
4/1/2025 12:11 0.00018.16117.445 9.618 87.8420.000 7.941 7.418 2.7370.1231.182 0.000 0.0000.484 0.098 819.01.011.222 0.000 18.16 0.00 180.0
4/1/2025 12:12 0.56316.50217.280 9.660 78.4930.000 6.205 7.128 3.0690.1551.354 0.000 0.0000.598 0.044 819.00.761.006 0.000 17.06 0.00 180.0
4/1/2025 12:13 0.45895.61317.170 9.657 76.5360.000 11.166 6.045 3.2460.1711.294 0.000 0.0000.564 0.036 819.00.740.995 0.000 96.07 0.00 180.0
4/1/2025 12:14 0.37030.44417.238 9.694 11.1780.000 1.420 3.374 0.7040.2150.000 0.000 0.0000.414 0.000 819.00.590.892 0.000 30.81 0.00 180.0
4/1/2025 12:15 0.05912.27817.256 9.699 24.2054.082 0.762 3.141 1.0390.1390.000 0.000 0.0000.395 0.012 819.00.731.053 0.000 12.34 0.00 180.0
4/1/2025 12:16 0.00013.65017.216 9.682 55.64815.636 3.367 4.275 1.9290.1320.762 0.000 0.0000.468 0.031 819.00.781.078 0.000 13.65 0.00 180.0
4/1/2025 12:17 0.00015.46417.302 9.640 88.42313.319 6.870 8.114 2.4810.0941.143 0.000 0.0000.384 0.074 819.00.991.262 0.000 15.46 0.00 180.0
4/1/2025 12:18 0.52317.92317.547 9.780 69.2160.000 5.277 5.044 2.5980.1171.049 0.000 0.0000.520 0.030 807.00.791.098 0.000 18.45 0.00 180.0
4/1/2025 12:19 0.00016.96617.484 9.772 101.9890.000 6.248 4.780 3.5610.0821.528 0.000 0.0000.472 0.090 808.00.991.211 0.000 16.97 0.00 180.0
4/1/2025 12:20 0.50915.63917.590 9.808 80.6820.000 5.947 4.995 3.2840.1041.595 0.000 0.0000.596 0.019 805.00.700.991 0.000 16.15 0.00 180.0
4/1/2025 12:21 0.00015.30817.756 9.816 88.2270.000 5.689 4.096 2.4830.1111.383 0.000 0.0000.438 0.041 802.00.821.103 0.000 15.31 0.00 180.0
4/1/2025 12:22 0.00016.24517.699 9.825 97.1790.000 6.177 4.560 3.2610.0741.436 0.000 0.0000.424 0.087 803.00.971.200 0.000 16.25 0.00 180.0
4/1/2025 12:23 0.00014.68417.511 9.790 92.6420.000 5.204 3.570 2.6430.1101.488 0.000 0.0000.465 0.058 807.00.891.157 0.000 14.68 0.00 180.0
4/1/2025 12:24 0.00014.58117.222 9.647 90.3860.000 4.812 3.421 2.6440.1021.575 0.000 0.0000.464 0.053 819.00.951.274 0.000 14.58 0.00 180.0
4/1/2025 12:25 0.00014.43817.289 9.619 92.9830.000 5.088 3.498 2.9480.1491.593 0.000 0.0000.476 0.065 819.00.961.247 0.000 14.44 0.00 180.0
0.08718.70917.335 9.685 84.0162.903 6.028 6.369 2.7050.1261.150 0.000 0.0000.485 0.069 816.130.9101.157 0.000 18.797 0.000 180.0Avg.
0.05518.96917.215 9.628 83.1313.405 5.889 6.497 2.5720.1300.682 0.000 0.0000.496 0.119 817.651.0391.201 0.000 19.024 0.000 180.0Run 1 Avg:
Baseline 1
4/1/2025 12:27 0.5840.0000.034 0.000 0.7270.000 0.000 1.487 0.0000.0010.000 0.000 0.0000.000 0.000 819.00.240.363 0.000 0.58 0.00 180.0
Run 2 - A 30minute/60min
4/1/2025 12:29 0.55812.96216.594 9.372 74.2240.000 3.677 2.788 2.7550.1390.935 0.000 0.0000.529 0.000 819.00.811.209 0.000 13.52 0.00 180.0
4/1/2025 12:30 0.00013.82817.054 9.651 84.4160.000 5.025 2.858 2.2120.1651.526 0.000 0.0000.493 0.032 819.00.811.118 0.000 13.83 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 12:31 0.0008.63816.929 9.673 74.4630.000 3.610 2.658 2.6910.0801.329 0.000 0.0000.501 0.000 819.00.801.206 0.000 8.64 0.00 180.0
4/1/2025 12:32 0.04814.04016.994 9.670 76.2980.000 4.213 2.727 2.7800.1171.308 0.000 0.0000.475 0.000 819.00.821.224 0.000 14.09 0.00 180.0
4/1/2025 12:33 0.00014.13717.165 9.663 72.6910.000 5.327 2.609 2.5530.0841.195 0.000 0.0000.486 0.000 819.00.771.157 0.000 14.14 0.00 180.0
4/1/2025 12:34 0.0008.79416.979 9.712 71.3570.000 2.444 2.395 2.5360.0781.036 0.000 0.0000.437 0.000 819.00.861.288 0.000 8.79 0.00 180.0
4/1/2025 12:35 0.0008.84317.001 9.691 84.3580.000 4.165 2.607 2.1660.1371.100 0.000 0.0000.313 0.013 819.00.831.207 0.000 8.84 0.00 180.0
4/1/2025 12:36 0.4958.87417.018 9.702 80.4730.000 4.753 2.876 3.1620.1851.220 0.000 0.0000.647 0.000 819.00.610.917 0.000 9.37 0.00 180.0
4/1/2025 12:37 0.0009.38117.060 9.674 83.2070.000 5.061 3.224 2.1760.1211.000 0.000 0.0000.456 0.025 819.00.851.200 0.000 9.38 0.00 180.0
4/1/2025 12:38 0.0009.23016.854 9.731 72.6620.000 3.816 2.341 2.7080.1091.261 0.000 0.0000.494 0.000 819.00.831.247 0.000 9.23 0.00 180.0
4/1/2025 12:39 0.45614.01317.078 9.673 78.0580.000 5.452 2.479 2.9220.1751.365 0.000 0.0000.605 0.001 819.00.610.910 0.000 14.47 0.00 180.0
4/1/2025 12:40 0.0008.84116.785 9.740 76.4660.000 3.212 2.074 2.7270.0971.102 0.000 0.0000.484 0.000 819.00.761.144 0.000 8.84 0.00 180.0
4/1/2025 12:41 0.0008.81916.539 9.769 88.5290.000 3.867 1.993 2.4210.1221.194 0.000 0.0000.432 0.009 819.00.891.309 0.000 8.82 0.00 180.0
4/1/2025 12:42 0.3638.61016.333 9.776 80.0090.000 3.875 1.931 3.0780.1451.219 0.000 0.0000.515 0.002 819.00.801.196 0.000 8.97 0.00 180.0
4/1/2025 12:43 0.3888.55916.528 9.740 78.6930.000 4.100 2.328 2.9530.1361.183 0.000 0.0000.512 0.000 819.00.741.104 0.000 8.95 0.00 180.0
4/1/2025 12:44 0.0008.52516.926 9.724 90.8260.000 4.579 2.267 2.5570.1131.218 0.000 0.0000.524 0.021 819.00.811.148 0.000 8.53 0.00 180.0
4/1/2025 12:46 0.0009.04317.127 9.685 87.5840.000 4.312 2.404 2.4720.1231.376 0.000 0.0000.388 0.032 819.00.871.206 0.000 9.04 0.00 180.0
4/1/2025 12:47 0.0009.68217.061 9.701 88.3900.000 4.811 2.683 2.6550.1081.480 0.000 0.0000.351 0.026 819.00.921.307 0.000 9.68 0.00 180.0
4/1/2025 12:48 0.00010.02516.856 9.739 84.2170.000 4.823 2.827 2.4540.1031.125 0.000 0.0000.415 0.014 819.00.861.244 0.000 10.02 0.00 180.0
4/1/2025 12:49 0.0008.90816.844 9.723 85.9620.000 4.621 2.561 2.3050.1290.975 0.000 0.0000.437 0.011 819.00.861.254 0.000 8.91 0.00 180.0
4/1/2025 12:50 0.0009.21116.930 9.710 86.1020.000 4.751 2.471 2.4150.1281.175 0.000 0.0000.494 0.030 819.00.881.227 0.000 9.21 0.00 180.0
4/1/2025 12:51 0.7488.48617.378 9.672 79.2620.000 4.483 2.496 2.8980.1371.365 0.000 0.0000.601 0.005 819.00.600.884 0.000 9.23 0.00 180.0
4/1/2025 12:52 0.5318.35717.224 9.682 76.8480.000 3.549 2.035 2.7240.1551.292 0.000 0.0000.655 0.000 819.00.570.851 0.000 8.89 0.00 180.0
4/1/2025 12:53 0.4968.23416.774 9.739 77.0680.000 3.577 1.986 2.7850.1211.165 0.000 0.0000.605 0.000 819.00.590.883 0.000 8.73 0.00 180.0
4/1/2025 12:54 0.0008.63616.620 9.744 86.5120.000 4.469 2.233 2.3260.0971.299 0.000 0.0000.389 0.021 819.00.821.163 0.000 8.64 0.00 180.0
4/1/2025 12:55 0.0009.01516.683 9.742 89.3610.000 5.220 2.427 2.5480.1241.085 0.000 0.0000.414 0.034 819.00.841.151 0.000 9.02 0.00 180.0
4/1/2025 12:56 0.0009.05616.682 9.743 86.3760.000 5.232 2.598 2.2890.1171.150 0.000 0.0000.439 0.025 819.00.831.169 0.000 9.06 0.00 180.0
4/1/2025 12:57 0.0009.07016.871 9.727 86.3520.000 5.432 2.674 2.1720.1561.054 0.000 0.0000.505 0.048 819.00.891.192 0.000 9.07 0.00 180.0
4/1/2025 12:58 0.2869.16617.062 9.696 74.8730.000 4.611 2.440 2.6380.1661.200 0.000 0.0000.611 0.006 819.00.590.872 0.000 9.45 0.00 180.0
4/1/2025 12:59 0.0008.95116.966 9.705 93.7660.000 5.117 2.453 2.7290.1921.586 0.000 0.0000.610 0.048 819.00.781.026 0.000 8.95 0.00 180.0
0.1469.73116.897 9.699 81.6470.000 4.406 2.481 2.5940.1291.217 0.000 0.0000.494 0.013 819.000.7831.134 0.000 9.877 0.000 180.0Avg.
Spike 2
4/1/2025 13:01 0.00030.46015.109 9.276 71.28238.849 5.305 0.869 3.4360.1531.316 0.000 18.7230.320 0.457 819.020.641.496 0.697 30.46 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
4/1/2025 13:06 0.0009.93616.607 9.745 88.0360.000 5.717 2.740 2.5410.1501.300 0.000 0.0000.427 0.048 819.00.901.209 0.000 9.94 0.00 180.0
4/1/2025 13:07 0.5119.76616.842 9.723 80.4030.000 5.135 2.853 3.1000.1371.195 0.000 0.0000.556 0.000 819.00.610.918 0.000 10.28 0.00 180.0
4/1/2025 13:08 0.00010.00516.895 9.743 84.2900.000 4.329 2.496 2.4500.1521.162 0.000 0.0000.451 0.035 818.00.841.150 0.000 10.01 0.00 180.0
4/1/2025 13:09 0.0009.98116.925 9.751 89.9850.000 5.725 2.603 2.7190.1471.321 0.000 0.0000.444 0.041 819.00.841.146 0.000 9.98 0.00 181.0
4/1/2025 13:10 0.00010.44716.920 9.702 93.9240.000 6.491 2.883 2.9310.1581.579 0.000 0.0000.450 0.063 819.00.871.112 0.000 10.45 0.00 180.0
4/1/2025 13:11 0.00010.16417.018 9.688 83.4210.000 5.540 2.863 2.3540.1691.232 0.000 0.0000.532 0.016 819.00.700.999 0.000 10.16 0.00 180.0
4/1/2025 13:12 0.0009.42516.860 9.699 86.7650.000 5.397 2.648 2.4540.1021.563 0.000 0.0000.381 0.030 819.00.921.291 0.000 9.42 0.00 180.0
4/1/2025 13:13 0.00010.46516.860 9.711 86.3070.000 5.922 3.175 2.4670.0881.428 0.000 0.0000.396 0.005 819.00.791.172 0.000 10.47 0.00 180.0
4/1/2025 13:14 0.13110.12517.168 9.661 70.7910.000 4.449 3.239 2.7330.1661.279 0.000 0.0000.543 0.000 819.00.681.025 0.000 10.26 0.00 180.0
4/1/2025 13:15 0.0009.44317.094 9.665 82.7580.000 4.625 3.034 2.1720.1131.205 0.000 0.0000.445 0.017 819.00.791.130 0.000 9.44 0.00 180.0
4/1/2025 13:16 0.0009.60417.082 9.683 93.4640.000 4.966 2.847 2.8270.1121.402 0.000 0.0000.407 0.037 819.00.821.119 0.000 9.60 0.00 180.0
4/1/2025 13:17 0.00010.21116.848 9.717 83.2900.000 5.225 2.815 2.1890.0941.335 0.000 0.0000.408 0.001 819.00.751.127 0.000 10.21 0.00 180.0
4/1/2025 13:18 0.00010.36716.790 9.744 90.8470.000 5.995 3.000 2.5920.0781.350 0.000 0.0000.489 0.006 818.00.811.192 0.000 10.37 0.00 180.0
4/1/2025 13:19 0.00015.03817.934 9.575 93.5670.000 6.018 4.460 2.8920.0821.747 0.000 0.0000.448 0.028 819.00.871.225 0.000 15.04 0.00 180.0
4/1/2025 13:20 0.0009.71616.476 9.750 98.9240.000 6.235 2.904 3.1770.0811.694 0.000 0.0000.534 0.019 819.00.761.079 0.000 9.72 0.00 180.0
4/1/2025 13:21 0.0009.54416.466 9.739 86.0690.000 5.089 2.637 2.4970.1111.426 0.000 0.0000.434 0.033 819.00.741.016 0.000 9.54 0.00 180.0
4/1/2025 13:22 0.00010.20316.480 9.742 92.2540.000 5.850 2.915 2.8780.1431.638 0.000 0.0000.453 0.027 819.00.881.239 0.000 10.20 0.00 180.0
4/1/2025 13:24 0.52915.23917.773 9.592 75.2260.000 4.889 3.041 3.1190.1421.502 0.000 0.0000.529 0.000 819.00.771.154 0.000 15.77 0.00 180.0
4/1/2025 13:25 0.0009.69616.993 9.699 97.7380.000 5.736 3.529 3.1460.0711.716 0.000 0.0000.513 0.051 819.00.891.182 0.000 9.70 0.00 180.0
4/1/2025 13:26 0.0009.33916.710 9.755 96.4910.000 5.752 2.467 3.0430.1151.713 0.000 0.0000.461 0.038 819.00.811.095 0.000 9.34 0.00 180.0
4/1/2025 13:27 0.0009.30816.644 9.735 86.2130.000 5.610 2.426 2.1710.0811.513 0.000 0.0000.520 0.010 819.00.741.078 0.000 9.31 0.00 180.0
4/1/2025 13:28 0.0009.83216.533 9.727 86.5220.000 5.114 2.708 2.3860.0731.451 0.000 0.0000.482 0.024 819.00.841.187 0.000 9.83 0.00 180.0
4/1/2025 13:29 0.0009.45516.781 9.703 86.2080.000 5.379 2.608 2.5730.0571.594 0.000 0.0000.473 0.034 819.00.841.157 0.000 9.45 0.00 180.0
4/1/2025 13:30 0.0009.71416.712 9.702 89.0510.000 5.817 2.902 2.5520.0811.581 0.000 0.0000.368 0.042 819.00.891.214 0.000 9.71 0.00 180.0
4/1/2025 13:31 0.0009.16216.830 9.697 90.3960.000 6.456 2.917 2.5390.1051.451 0.000 0.0000.568 0.037 819.00.740.998 0.000 9.16 0.00 180.0
4/1/2025 13:32 0.00013.84519.222 9.426 90.8870.000 5.871 3.929 2.6250.0731.894 0.000 0.0000.512 0.068 819.00.981.266 0.000 13.84 0.00 180.0
4/1/2025 13:33 0.0009.01716.864 9.739 90.1140.000 5.392 2.745 2.4680.0571.472 0.000 0.0000.453 0.028 819.00.861.205 0.000 9.02 0.00 180.0
4/1/2025 13:34 0.0009.36116.663 9.743 69.4930.000 3.480 2.475 2.5210.0661.376 0.000 0.0000.469 0.010 819.00.771.127 0.000 9.36 0.00 180.0
4/1/2025 13:35 0.0009.32416.802 9.690 93.9050.000 6.137 3.179 2.6190.0711.404 0.000 0.0000.460 0.079 819.00.991.248 0.000 9.32 0.00 180.0
4/1/2025 13:36 0.00015.26517.949 9.568 69.0750.000 5.062 3.584 2.7230.0951.429 0.000 0.0000.549 0.036 819.00.781.058 0.000 15.26 0.00 180.0
0.03910.43316.991 9.694 86.8800.000 5.447 2.954 2.6490.1061.465 0.000 0.0000.472 0.029 818.930.8161.137 0.000 10.472 0.000 180.0Avg.
0.09210.08216.944 9.696 84.2640.000 4.926 2.718 2.6210.1171.341 0.000 0.0000.483 0.021 818.970.8001.136 0.000 10.175 0.000 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
4/1/2025 13:40 0.3250.0000.003 0.000 0.7910.000 0.000 1.373 0.0000.0040.000 0.000 0.0000.000 0.000 819.00.220.331 0.000 0.33 0.00 180.0
Run 3 - A 30minute/60min
4/1/2025 13:42 0.00011.07915.103 9.123 75.0330.000 4.131 2.896 2.6620.0940.401 0.000 0.0000.443 0.053 819.00.931.231 0.000 11.08 0.00 180.0
4/1/2025 13:43 0.0008.32416.624 9.717 86.6210.000 5.256 2.782 2.0590.0900.681 0.000 0.0000.405 0.097 819.01.081.333 0.000 8.32 0.00 180.0
4/1/2025 13:44 0.0008.14916.753 9.731 88.5070.000 4.763 2.668 2.1880.1000.695 0.000 0.0000.509 0.090 819.01.101.374 0.000 8.15 0.00 180.0
4/1/2025 13:45 0.0008.01316.703 9.747 88.9890.000 5.211 2.633 2.1290.1320.783 0.000 0.0000.429 0.080 819.01.091.389 0.000 8.01 0.00 180.0
4/1/2025 13:46 0.0007.57316.731 9.745 93.2890.000 4.665 2.390 2.4370.0900.779 0.000 0.0000.487 0.087 819.01.091.380 0.000 7.57 0.00 180.0
4/1/2025 13:47 0.0007.72316.728 9.766 70.4540.000 4.081 2.274 2.1680.0750.569 0.000 0.0000.536 0.056 819.00.961.268 0.000 7.72 0.00 180.0
4/1/2025 13:48 0.0007.20016.734 9.761 88.6730.000 4.395 2.207 2.1070.0740.613 0.000 0.0000.399 0.091 819.01.131.428 0.000 7.20 0.00 180.0
4/1/2025 13:49 0.0007.41616.633 9.773 86.5020.000 4.354 2.209 2.0300.1110.815 0.000 0.0000.391 0.097 819.01.121.389 0.000 7.42 0.00 180.0
4/1/2025 13:50 0.0007.66216.593 9.787 89.4180.000 4.805 2.177 2.2430.0870.748 0.000 0.0000.347 0.090 819.01.151.457 0.000 7.66 0.00 180.0
4/1/2025 13:51 0.0007.62716.692 9.792 91.0540.000 5.678 2.311 2.1060.0540.640 0.000 0.0000.456 0.091 819.01.091.354 0.000 7.63 0.00 180.0
4/1/2025 13:52 0.0008.33216.825 9.793 87.3630.000 5.497 2.488 1.9420.0970.614 0.000 0.0000.479 0.092 819.01.101.366 0.000 8.33 0.00 180.0
4/1/2025 13:53 0.0007.88516.730 9.753 85.1360.000 4.928 2.373 1.8630.0600.461 0.000 0.0000.421 0.100 819.01.141.418 0.000 7.89 0.00 180.0
4/1/2025 13:54 0.0007.40116.682 9.727 85.7320.000 5.159 2.284 1.7730.0930.354 0.000 0.0000.458 0.101 819.01.091.338 0.000 7.40 0.00 180.0
4/1/2025 13:55 0.0008.30416.564 9.765 87.3120.000 5.266 2.339 1.9240.1060.472 0.000 0.0000.435 0.114 819.01.141.376 0.000 8.30 0.00 180.0
4/1/2025 13:56 0.0007.36516.530 9.770 90.1430.000 4.833 2.234 2.0790.0710.443 0.000 0.0000.369 0.125 819.01.211.442 0.000 7.37 0.00 180.0
4/1/2025 13:57 0.0837.74816.509 9.768 77.1450.000 4.316 2.150 2.5340.0700.423 0.000 0.0000.510 0.092 820.01.031.266 0.000 7.83 0.00 180.0
4/1/2025 13:58 0.0008.20316.623 9.764 83.4060.000 6.481 2.509 1.8060.0840.486 0.000 0.0000.473 0.111 819.01.151.391 0.000 8.20 0.00 180.0
4/1/2025 13:59 0.2307.91416.939 9.744 73.0120.000 4.453 2.240 2.3820.0760.621 0.000 0.0000.551 0.104 819.01.051.263 0.000 8.14 0.00 180.0
4/1/2025 14:00 0.0007.63617.077 9.748 90.2320.000 4.637 2.322 2.1150.0610.439 0.000 0.0000.443 0.115 819.01.161.388 0.000 7.64 0.00 180.0
4/1/2025 14:01 0.0008.22117.164 9.722 87.0580.000 5.416 2.389 1.8660.1190.522 0.000 0.0000.443 0.126 819.01.171.381 0.000 8.22 0.00 180.0
4/1/2025 14:03 0.00014.14417.249 9.646 84.3740.000 5.335 2.646 1.9200.0810.563 0.000 0.0000.447 0.150 821.01.251.426 0.000 14.14 0.00 180.0
4/1/2025 14:04 0.0008.84717.116 9.662 91.0750.000 5.687 2.620 2.4000.0800.446 0.000 0.0000.491 0.149 819.01.211.366 0.000 8.85 0.00 180.0
4/1/2025 14:05 0.00013.40617.309 9.631 73.4120.000 5.404 2.465 2.4190.0910.378 0.000 0.0000.550 0.115 819.01.101.307 0.000 13.41 0.00 180.0
4/1/2025 14:06 0.00013.13817.515 9.591 84.2440.000 5.690 2.481 1.7910.1420.521 0.000 0.0000.468 0.140 820.01.181.343 0.000 13.14 0.00 180.0
4/1/2025 14:07 0.00013.11617.775 9.586 82.6060.000 5.553 2.548 1.7160.1070.498 0.000 0.0000.425 0.154 819.01.211.360 0.000 13.12 0.00 180.0
4/1/2025 14:08 0.00012.83517.835 9.575 82.5890.000 4.795 2.529 1.6210.1110.631 0.000 0.0000.469 0.151 820.01.231.389 0.000 12.84 0.00 180.0
4/1/2025 14:09 0.00013.96118.052 9.548 88.9570.000 6.925 3.467 2.1300.1110.742 0.000 0.0000.455 0.145 820.01.231.416 0.000 13.96 0.00 180.0
4/1/2025 14:10 0.00013.06017.467 9.621 86.9870.000 5.902 2.762 1.8710.0970.597 0.000 0.0000.436 0.161 820.01.261.400 0.000 13.06 0.00 180.0
4/1/2025 14:11 0.00013.25817.249 9.654 93.8420.000 6.518 2.894 2.3050.0850.676 0.000 0.0000.443 0.153 820.01.221.370 0.000 13.26 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 14:12 0.00013.47017.328 9.650 87.7310.000 6.020 2.732 1.9590.0760.322 0.000 0.0000.509 0.157 820.01.251.401 0.000 13.47 0.00 180.0
0.0109.63416.928 9.689 85.3630.000 5.205 2.501 2.0850.0910.564 0.000 0.0000.456 0.113 819.301.1371.367 0.000 9.644 0.000 180.0Avg.
Spike 3
4/1/2025 14:14 0.00033.00815.571 9.211 83.49748.359 7.672 2.220 3.9030.0780.803 0.000 21.5490.530 0.683 820.024.021.653 0.824 33.01 0.00 180.0
Run 3 - B 30minute/60min
4/1/2025 14:16 0.0008.48916.838 9.691 88.9120.000 6.382 3.338 1.9120.0810.010 0.000 0.0000.403 0.175 820.01.281.391 0.000 8.49 0.00 179.0
4/1/2025 14:17 0.0008.37716.907 9.706 87.0390.000 5.122 3.050 1.7780.1040.000 0.000 0.0000.491 0.176 820.01.271.379 0.000 8.38 0.00 180.0
4/1/2025 14:18 0.0008.23316.863 9.758 88.6640.000 5.811 2.996 1.8910.1410.000 0.000 0.0000.544 0.179 820.01.231.316 0.000 8.23 0.00 180.0
4/1/2025 14:19 0.0007.56516.949 9.698 84.4910.000 4.946 2.848 1.5470.1370.000 0.000 0.0000.534 0.164 820.01.211.320 0.000 7.57 0.00 180.0
4/1/2025 14:20 0.00012.85517.272 9.666 90.0230.000 5.650 2.592 1.9930.1180.252 0.000 0.0000.398 0.177 820.01.341.479 0.000 12.86 0.00 180.0
4/1/2025 14:21 0.00012.38117.443 9.644 89.7130.000 5.436 2.592 1.8730.1060.297 0.000 0.0000.453 0.175 820.01.231.320 0.000 12.38 0.00 180.0
4/1/2025 14:22 0.00013.54617.872 9.584 87.1400.000 5.728 2.932 2.0820.1230.359 0.000 0.0000.546 0.189 820.01.241.290 0.000 13.55 0.00 180.0
4/1/2025 14:23 0.00013.10717.565 9.654 79.2810.000 5.292 2.707 2.5760.0860.373 0.000 0.0000.495 0.139 820.01.161.327 0.000 13.11 0.00 180.0
4/1/2025 14:24 0.00012.73617.484 9.617 88.6320.000 6.319 2.662 1.9910.1330.418 0.000 0.0000.462 0.183 820.01.261.344 0.000 12.74 0.00 180.0
4/1/2025 14:25 0.00013.20317.381 9.646 76.0620.000 4.861 2.587 2.3110.1180.345 0.000 0.0000.500 0.141 820.01.211.394 0.000 13.20 0.00 180.0
4/1/2025 14:26 0.0007.32816.647 9.707 90.8470.000 5.700 2.669 1.9000.0940.000 0.000 0.0000.442 0.163 820.01.221.337 0.000 7.33 0.00 180.0
4/1/2025 14:27 0.00014.11017.130 9.603 88.3320.000 6.941 2.982 1.9260.1120.320 0.000 0.0000.406 0.178 820.01.341.469 0.000 14.11 0.00 180.0
4/1/2025 14:28 0.00014.23818.169 9.513 97.7650.000 5.890 3.102 2.7140.1080.566 0.000 0.0000.491 0.194 820.01.261.303 0.000 14.24 0.00 180.0
4/1/2025 14:29 0.00015.54018.732 9.467 97.8320.000 6.571 4.076 3.0670.1380.532 0.000 0.0000.490 0.228 820.01.321.290 0.000 15.54 0.00 180.0
4/1/2025 14:30 0.00013.53419.811 9.335 84.9390.000 5.013 4.369 1.7440.1510.508 0.000 0.0000.469 0.203 820.01.271.297 0.000 13.53 0.00 180.0
4/1/2025 14:31 0.00015.28018.286 9.494 103.5850.000 6.950 4.491 3.1870.1920.750 0.000 0.0000.562 0.212 820.01.121.049 0.000 15.28 0.00 180.0
4/1/2025 14:32 0.00013.18717.482 9.610 88.1370.000 5.430 3.956 1.8890.1450.357 0.000 0.0000.522 0.179 821.01.201.264 0.000 13.19 0.00 180.0
4/1/2025 14:33 0.00014.27217.491 9.629 91.6330.000 6.723 4.420 2.2570.0990.684 0.000 0.0000.555 0.174 820.01.181.248 0.000 14.27 0.00 180.0
4/1/2025 14:34 0.00015.55517.513 9.645 99.2480.000 5.782 4.185 3.0000.0990.719 0.000 0.0000.397 0.207 820.01.251.250 0.000 15.55 0.00 180.0
4/1/2025 14:35 0.00014.35417.441 9.597 103.1550.000 6.016 4.330 3.3900.1070.780 0.000 0.0000.428 0.210 820.01.321.356 0.000 14.35 0.00 180.0
4/1/2025 14:36 0.00014.11117.529 9.626 105.1280.000 5.453 3.670 3.4240.1200.886 0.000 0.0000.422 0.204 820.01.311.353 0.000 14.11 0.00 180.0
4/1/2025 14:37 0.00013.60617.530 9.639 91.2420.000 6.132 3.854 2.1730.1640.657 0.000 0.0000.482 0.173 820.01.231.321 0.000 13.61 0.00 180.0
4/1/2025 14:38 0.00013.79017.371 9.590 90.2540.000 5.264 3.655 2.3890.1310.689 0.000 0.0000.424 0.170 820.01.311.451 0.000 13.79 0.00 180.0
4/1/2025 14:40 0.00013.76817.400 9.608 96.8640.000 5.461 3.634 2.6080.1560.826 0.000 0.0000.510 0.191 820.01.281.351 0.000 13.77 0.00 180.0
4/1/2025 14:41 0.00016.05417.374 9.620 102.4070.000 6.253 4.728 3.0840.0930.850 0.000 0.0000.487 0.209 821.01.291.305 0.000 16.05 0.00 180.0
4/1/2025 14:42 0.00014.93617.336 9.612 96.5470.000 6.796 4.702 2.7200.1510.809 0.000 0.0000.487 0.202 820.01.321.378 0.000 14.94 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 14:43 0.00014.28717.356 9.615 93.4390.000 5.698 4.077 2.6030.1430.723 0.000 0.0000.510 0.177 820.01.251.347 0.000 14.29 0.00 180.0
4/1/2025 14:44 0.00013.97217.360 9.631 90.8010.000 4.944 3.776 2.2590.1070.666 0.000 0.0000.429 0.165 820.01.261.400 0.000 13.97 0.00 180.0
4/1/2025 14:45 0.00014.54917.408 9.639 99.8490.000 6.095 4.347 3.0210.1191.017 0.000 0.0000.478 0.184 820.01.291.388 0.000 14.55 0.00 180.0
4/1/2025 14:46 0.00015.38817.378 9.634 105.0280.000 6.133 5.007 3.3850.0740.954 0.000 0.0000.469 0.206 820.01.281.310 0.000 15.39 0.00 180.0
0.00013.07817.511 9.616 92.5660.000 5.826 3.611 2.4230.1220.512 0.000 0.0000.476 0.184 820.071.2581.334 0.000 13.079 0.000 180.0Avg.
0.00511.35617.219 9.652 88.9650.000 5.516 3.056 2.2540.1060.538 0.000 0.0000.466 0.149 819.681.1981.351 0.000 11.362 0.000 180.0Run 3 Avg:
Baseline 3
4/1/2025 14:59 0.1490.000-0.000 0.000 1.0280.000 0.000 1.339 0.0000.0040.000 0.000 0.0000.000 0.000 820.00.210.322 0.000 0.15 0.00 180.0
Post CTS
4/1/2025 15:01 0.0000.0000.006 0.000 0.8260.000 0.000 0.399 0.5330.0520.000 97.508 0.0000.000 0.000 820.065.040.050 0.000 0.00 0.00 180.0
4/1/2025 15:01 0.0000.0000.007 0.000 0.9890.000 0.000 0.467 0.5760.0000.000 97.698 0.0000.000 0.000 820.065.140.000 0.000 0.00 0.00 180.0
4/1/2025 15:01 0.0000.0000.007 0.000 0.8940.000 0.000 0.571 0.6330.0030.000 98.566 0.0000.000 0.000 820.065.710.000 0.000 0.00 0.00 180.0
Post NO2/Mid O2
4/1/2025 15:04 98.9610.000-0.000 0.000 1.5590.000 0.307 1.314 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.090.138 0.000 98.96 10.44 180.0
4/1/2025 15:04 101.6530.000-0.000 0.000 0.0350.000 0.317 1.229 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.240.361 0.000 101.65 10.43 180.0
4/1/2025 15:04 100.2520.000-0.000 0.000 0.3060.000 0.303 1.241 0.0000.0220.000 0.000 0.0000.000 0.000 819.00.190.286 0.000 100.25 10.36 180.0
Post 5-Gas
4/1/2025 15:06 0.000249.517-0.000 4.535 5.155491.823 2.969 2.739 2.5300.0320.065 0.205 246.4640.000 1.383 821.0250.671.953 9.817 249.52 0.00 180.0
4/1/2025 15:07 0.000248.8930.001 4.385 5.145491.958 2.925 1.842 3.9070.2090.010 0.000 250.7620.160 0.532 822.0254.173.518 9.888 248.89 0.00 180.0
4/1/2025 15:07 0.000250.0100.001 4.391 5.568492.204 2.905 1.458 6.1440.1200.340 0.000 250.6660.004 0.095 822.0253.133.413 9.890 250.01 0.00 180.0
4/1/2025 15:07 0.000248.694-0.000 4.505 5.608491.510 2.932 2.535 2.1200.1430.210 0.260 245.7730.311 1.352 823.0249.992.015 9.796 248.69 0.00 180.0
4/1/2025 15:07 0.000248.745-0.000 4.527 5.467490.147 2.914 2.235 2.3310.1700.000 0.276 245.8440.208 1.277 823.0250.012.145 9.785 248.75 0.00 180.0
4/1/2025 15:07 0.000248.742-0.000 4.372 5.519491.380 2.961 1.732 4.8290.0500.453 0.000 250.1310.203 0.482 823.0253.723.932 9.876 248.74 0.00 180.0
4/1/2025 15:07 0.000247.9280.000 4.374 5.196491.633 3.017 2.133 2.7390.1990.000 0.000 249.7280.092 0.903 823.0253.793.390 9.861 247.93 0.00 180.0
4/1/2025 15:07 0.000248.7640.000 4.391 5.450491.096 2.972 1.677 4.5650.0490.284 0.000 250.2540.000 0.483 823.0253.583.536 9.866 248.76 0.00 180.0
End of Test Purge
4/1/2025 15:09 0.0000.000-0.000 0.000 0.7320.000 0.000 1.185 0.0000.0050.000 0.000 0.0000.000 0.000 825.00.000.000 0.000 0.00 0.00 180.0
4/1/2025 15:09 0.0000.000-0.000 0.000 0.6950.000 0.000 1.162 0.0000.0080.000 0.000 0.0000.000 0.000 825.00.000.000 0.000 0.00 0.00 180.0
4/1/2025 15:10 0.0000.000-0.000 0.000 1.0540.000 0.000 1.187 0.0000.0000.000 0.000 0.0000.000 0.000 826.00.000.002 0.000 0.00 0.00 180.0
4/1/2025 15:10 0.0000.000-0.000 0.000 0.7680.000 0.000 1.357 0.0000.0050.000 0.000 0.0000.000 0.000 826.00.070.102 0.000 0.00 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 15:10 0.3840.000-0.000 0.000 1.2720.000 0.000 1.489 0.0000.0110.000 0.000 0.0000.000 0.000 826.00.070.106 0.000 0.38 0.00 180.0
4/1/2025 15:10 0.0000.000-0.000 0.000 1.0900.000 0.000 1.232 0.0000.0550.000 0.000 0.0000.000 0.000 826.00.050.082 0.000 0.00 0.00 180.0
4/1/2025 15:10 0.0000.000-0.000 0.000 0.0820.000 0.000 1.167 0.0000.0630.000 0.000 0.0000.049 0.000 826.00.140.211 0.000 0.00 0.00 180.0
4/1/2025 15:10 0.0000.000-0.000 0.000 0.1440.000 0.000 1.450 0.0000.0290.000 0.000 0.0000.000 0.000 826.00.120.175 0.000 0.00 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 4/1/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:07:11 AM 10:55 AM
Source:
Unit Number: 1454
Serial Number: WAU-1651084
Engine Hours:11452
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.432 0.427 0.044
28.923 17.426 1.853
2.000 0.300 1.000 0.150 0.700 0.030
0.087 0.086 0.009
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Lynn Huber
3
Hunter Newton
GAS
4.0 Test Summary
T
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Site Verification Photos
GAS
Unit 1454 with a serial number of WAU-1651084 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 4/1/2025 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2250 BHP and 1199 RPM which is 90.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1454 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1454Unit ID
Make Waukesha Site Elevation ft.5226
Model 9394 GSI Atmospheric Pressure psi.12
Serial Number WAU-1651084 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2250 2250 2250 2250
1200 1199 1197 1199
Percent Load %
Intake Manifold Pressure (hg)
90.00%90.00%90.00%90.00%
61.00 61.00 61.00 61.00
Intake Manifold Temperature (F)116.00 117.00 118.00 117.00
Ambient Conditions
Ambient Temperature Dry (F)34.00 35.00 37.00 35.33
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
204723.86 205738.01 205677.16 205379.68
5797.08 5825.80 5824.07 5815.65
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.17 0.17 0.17
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %17.33%17.28%17.18%17.26%
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mfg. rated rpm
Test RPM
0.00%0.00%0.00%0.00%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
07:11 AM 08:22 AM 09:30 AM 4/1/2025
State
NOx (mol wt) 46.01
1.670 1.315 1.616 1.533NMNEHC (ppmvw)
2.020 1.589 1.951 1.853NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
570.262 448.575 550.662 523.166 FailNMNEHC (ppbvd) @15% O2
0.010 0.008 0.009 0.0090.700 0.030 PassNMNEHC (g/hp-hr)
0.047 0.037 0.046 0.0440.170 PassNMNEHC (lbs/hr)
0.570 0.449 0.551 0.523 FailNMNEHC (ppmvd) @15% O2
0.0790.045CO (g/hp-hr)0.136 0.0872.000 0.300 Pass
CO (ppmvw)37.541 12.410 21.828 23.926
CO (ppmvd)45.411 15.002 26.356 28.923
CO (mol wt) 28.01
CO (ppmvd) @15% O2 12.819 4.235 7.440 8.165 Fail
CO (ppbvd) @15% O2 12819.280 4234.928 7440.161 8164.790 Fail
0.3940.224CO (lbs/hr)0.676 0.4321.650 Pass
NOx (g/hp-hr)0.080 0.080 0.098 0.0861.000 0.150 Pass
NOx (ppmvw)13.419 13.374 16.464 14.419
NOx (ppmvd)16.232 16.167 19.880 17.426
NOx (ppbvd) @15% O2 4582.241 4563.894 5611.949 4919.361 Fail
NOx (ppmvd) @15% O2 4.582 4.564 5.612 4.919 Fail
NOx (lbs/hr)0.397 0.397 0.488 0.4270.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
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Table 5.1 Run Summaries
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Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
37.54
0.00
13.42 0.00 13.42
0.00%
0.00%
0.00%
17.33%
13.22 0.00 0.00%17.33%
35.52 0.00 0.00%15.60%
13.62 0.00 0.00%17.33%
0.00 0.00 0.00 0.00%0.48%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.00 0.00 0.00%0.48%
13.74 13.28 0.00 13.28 0.00%17.31%
54.54 29.81 0.02 29.82 0.00%14.36%
11.08 13.47 0.00 13.46 0.00%17.25%
0.00 0.00 0.00 0.00 0.00%0.18%
Avg. Wet 12.41 13.37 0.00 13.37 1.31 0.00%17.28%
NO2NO
0.03
1.27
23.90
1.36
0.00
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
18.00 12.96 0.13 13.09 0.00%17.17%
66.88 30.50 0.00 30.50 0.00%14.36%
25.66 13.59 6.25 19.84 0.00%17.20%
0.00 0.00 0.17 0.17 0.00%0.00%
0.00 0.00 0.00 0.00 0.00 0.00%0.18%
Avg. Wet 21.83 13.28 3.19 16.46 1.62 0.00%17.18%
NO2NO
0.40
1.70
24.38
1.53
NMNEHC
0.40
NO2
0.000.00
1.90
26.50
1.44
0.03
1.67
0.00
13.22
35.52
13.62
46.21
28.87
0.00
119.04
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.52
Yes
20.00
7.00
23.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%17.33
29.85
0.58
Inches
3.34
10
16.66
Vo
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Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.59
0.00
0.00
1002.03
0.04
29.60
29.64
928.38
1388.05
497.99
27.80
83.66
182.55
247639.85
204723.86
Run 2
17.28
29.85
0.57
11.53
0.00
0.00
1002.03
0.04
29.60
29.64
922.25
1381.92
494.58
27.80
82.61
182.52
248704.14
205738.01
Run 3
17.18
29.83
0.55
11.45
0.00
0.00
1001.36
0.04
29.58
29.62
923.31
1382.98
495.17
27.80
81.53
182.52
248345.38
205677.16
17.26
29.84
0.57
11.52
0.00
0.00
1001.81
0.04
29.59
29.63
924.65
1384.32
495.91
27.80
82.61
182.52
248229.79
205379.68
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.60
Exhaust Temp F
928.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.56
0.57
0.51
930.00
929.00
927.00
0.58
0.59
0.60
931.00
926.00
929.00
0.62
0.55
0.60
928.00
931.00
932.00
0.59 930.00
0.56
0.52
0.60
929.00
926.00
927.00
0.60
0.56
0.58
925.00
926.00
928.38
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.52
Exhaust Temp F
923.00
0.55
0.54
0.51
924.00
922.00
918.00
0.48
0.56
0.53
919.00
925.00
923.00
0.58
0.56
0.56
925.00
926.00
927.00
0.59 924.00
0.62
0.61
0.58
923.00
922.00
925.00
0.53
0.52
923.00
924.00
923.310.55
Run 2
Δpstd (in) H2O
0.55
Exhaust Temp F
922.00
0.58
0.62
0.59
920.00
924.00
921.00
0.61
0.63
0.64
923.00
922.00
919.00
0.60
0.55
0.58
917.00
918.00
922.00
0.53 924.00
0.52
0.54
0.50
925.00
923.00
922.00
0.49
0.56
926.00
928.00
0.57 922.25
Pass
Strat Check
103.071Check 1
102.269Check 2
101.193Check 3
MethaneGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.592)+ .32(0)+ .28(88.403+.005) = 29.85 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.85(1 -.1733)+ 18.0(.1733) = 27.8 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.58*√(1388.05/(29.64*27.8)) = 83.66 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.1733)83.66*2.182((528*29.64)/ (1388.05*29.92)) = 204723.86 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 204723.864/35.315 = 5797.08 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 45.411*(20.9-15)/(20.9-0%)) = 12.819 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(45.411*(1.164*10^-3)*5797.08*(Run Time/60))/2250 = .136 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .136*1/453.6*2250 = .676 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .676*4.38 = 2.961 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
45.41 = 37.541*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.61%
21.11%
10.44%
10.41%
10.58%
10.58%
10.41%10.44%
10.61%
21.11%
10.58%
20.92%
10.58%
20.92%
10.58%20.92%
0.00%
10.58%
20.92%
0.03%
0.19%
0.13%
0.91%
10.58%
Span
Zero Offset 0.00%
20.92
0.00%
10.61%0.81%0.94%0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
9
GAS
1076.0 1080.0 1076.0
1036.0 1039.0 1036.0
6.0 6.0
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
4/1/2025
5226
1454
Waukesha
Model
Serial Number
9394 GSI
WAU-1651084
Technician Hunter Newton
Run Start Times 07:11 AM 08:22 AM 09:30 AM 10:55 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1199.0 1197.0 1198.7
Engine Hours 11449 11450 11451 11452
Intake Manifold Pressure (psi)61.0 61.0 61.0 61.0
Intake Manifold Temp °F 116.0 117.0 118.0 117.0
Engine Load (BHP)2250.0 2250.0 2250.0 2250.0
Ambient Temp °F 34.0 35.0 37.0 35.3
Humidity %79.0 77.0 64.0 73.3
Dew Point °F 28.0 28.0 26.0 27.3
Waukesha
N/A
N/A
Yes
DCL DCL DCL DCL
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
Discharge Pressure (psi)
Suction Pressure (psi)
1072.0
1033.0
6.0Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
6.0
N/A N/A N/A N/A
N/A N/A N/A N/A
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
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Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.08
Average:NOx 0.08
Average:VOC 0.51
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 98.63
Tolerance 2.00%
Difference between measured and expected 0.95%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.11
Average:NOx 0.11
Average:VOC 0.58
Average:Oxygen 0.00
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 97.11
Tolerance 5.00%
Difference between measured and expected 2.47%
Pre-test System CTS & Mechanical Response Time
52 secondsEquilibration Response Time
Value:Spike Reported 252.46
Value:Spike Expected 249.80
System (Equilibration) Response Time Target (Spike)
45 secondsSystem Zero Response Time
52 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC507781 9/17/2027 102.10 10.58%
EB0115896 12/18/2027 99.57
CC440196 7/13/2032 20.92%
Cylinder # CC333629 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 249.80 501.50 254.60 9.99
Analyzer System Response 252.46 495.75 251.30 9.93
Percent Difference 1.07%1.15%1.30%0.62%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.628 4.953
Spike Direct
Propane 253.997
Mechanical
Response Time
SF6 9.896
CO 492.973
NO 250.793
Ethylene 97.110 36 seconds
Analyzer
Response
Propane 252.464
SF6 9.926
CO 495.754
NO 251.297
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 250.628
CO 492.860
NO 251.887
52 seconds
25 seconds
8.93%
8.18%
8.28%
106.57%
106.48%
106.33%
9.893
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
7
23
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
205379.68
H2O%d @ Sampling Point:17.26
CO2%d @ Sampling Point:11.52
Pressure @ Sampling Point (Pg "H2O):0.57
Temperature @ Sampling Point (Deg F):924.65
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 99.57 98.63 4.953 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.628 4.953
Spike Direct
Propane 253.997
Mechanical
Response Time
SF6 9.896
CO 492.973
NO 250.793
Ethylene 97.110 36 seconds
Analyzer
Response
Propane 252.464
SF6 9.926
CO 495.754
NO 251.297
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 250.628
CO 492.860
NO 251.887
52 seconds
25 seconds
8.93%
8.18%
8.28%
106.57%
106.48%
106.33%
9.893
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
249.800
9.988
501.500
254.600
253.997
9.896
492.973
250.793
1.68%
0.92%
1.70%
1.50%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
23.772
0.884
Dilution Factor
8.933%
Expected
22.307
% Recovery
106.570%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.809
Dilution Factor
8.175%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.819
Dilution Factor
8.276%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 21.993 20.683 106.330%
0.000345
0.000408
0.000351
0.000 21.758 20.434 106.480%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass1.10%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:38.6198488 Pass
Line Position Difference:Resolution Difference to Reference 1.10%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
99.57
97.76
1.85%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1454; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
4/1/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
4/1/2025
Hunter Newton
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1454
Make:Waukesha
Location:9394 GSIModel:
WAU-1651084Serial Number:
RAW Result Data
Stability
4/1/2025 06:00 1.9291.316-0.019 0.027 0.26511.305 0.000 0.000 0.0000.0010.000 4.981 1.5650.120 0.000 827.05.190.455 0.098 3.25 0.00 181.0
Pre Test Baseline Direct
4/1/2025 06:07 0.0000.0000.002 0.000 0.1610.000 0.000 0.797 0.0000.0000.000 0.000 0.0000.000 0.000 827.00.430.642 0.000 0.00 0.00 181.0
4/1/2025 06:07 0.0000.0000.001 0.000 0.1940.000 0.000 0.769 0.0000.0000.000 0.000 0.0000.000 0.000 827.00.550.824 0.000 0.00 0.00 181.0
4/1/2025 06:07 0.2330.000-0.000 0.000 0.3320.000 0.000 0.892 0.0000.0000.000 0.000 0.0000.000 0.000 827.00.560.846 0.000 0.23 0.00 180.0
CTS Direct
4/1/2025 06:09 0.0000.0000.011 0.000 0.0000.000 0.000 0.523 0.0000.0000.000 99.189 0.0000.000 0.000 827.066.730.894 0.000 0.00 0.00 181.0
4/1/2025 06:09 0.0000.0000.012 0.000 0.0000.000 0.000 0.417 0.0000.0000.000 98.455 0.0000.000 0.000 827.066.230.889 0.000 0.00 0.00 180.0
4/1/2025 06:10 0.0000.0000.010 0.000 0.0000.000 0.000 0.357 0.0000.0000.000 98.240 0.0000.000 0.000 827.066.120.929 0.000 0.00 0.00 180.0
High O2 Direct
4/1/2025 06:15 0.2570.0000.003 0.000 0.3460.000 0.000 1.069 0.0000.0030.000 0.000 0.0000.000 0.000 825.00.701.044 0.000 0.26 21.09 180.0
4/1/2025 06:15 0.0000.0000.003 0.000 0.0000.000 0.000 1.112 0.0000.0700.000 0.000 0.0000.000 0.000 825.00.711.068 0.000 0.00 21.11 180.0
4/1/2025 06:16 0.0000.0000.000 0.000 0.0000.000 0.000 1.127 0.0000.0450.000 0.000 0.0000.000 0.000 825.00.721.080 0.000 0.00 21.13 180.0
NO2/Mid O2 Direct
4/1/2025 06:21 100.5090.0000.002 0.000 0.2230.000 0.206 0.737 0.0000.0570.000 0.000 0.0000.000 0.000 824.00.310.462 0.000 100.51 10.62 180.0
4/1/2025 06:21 102.1030.0000.001 0.000 0.2100.000 0.212 0.848 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.370.551 0.000 102.10 10.60 180.0
4/1/2025 06:22 102.4060.000-0.000 0.000 0.1500.000 0.238 0.854 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.490.738 0.000 102.41 10.60 180.0
Spike Direct
4/1/2025 06:24 0.000250.4410.008 4.412 5.050492.188 2.922 1.521 3.4810.2810.000 0.000 254.8520.200 0.498 817.0258.273.636 9.884 250.44 0.00 180.0
4/1/2025 06:25 0.000250.8040.006 4.403 5.335492.338 2.909 1.574 3.8170.3480.261 0.000 255.0530.168 0.343 817.0258.223.720 9.897 250.80 0.00 180.0
4/1/2025 06:26 0.000251.1350.007 4.413 5.284494.392 2.864 1.450 4.3490.2820.000 0.000 252.0850.131 0.253 821.0255.153.839 9.906 251.14 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
4/1/2025 06:28 0.0000.0000.016 0.000 0.0000.000 0.000 1.293 0.0000.0000.000 0.000 0.0000.000 0.000 821.00.540.813 0.000 0.00 0.00 180.0
4/1/2025 06:29 0.1860.0000.010 0.000 0.7570.000 0.000 1.265 0.0000.0040.000 0.000 0.0000.000 0.000 820.00.590.883 0.000 0.19 0.00 180.0
4/1/2025 06:29 0.1450.0000.006 0.000 0.5630.000 0.000 1.178 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.610.917 0.000 0.14 0.00 180.0
CTS System with Response Time
4/1/2025 06:30 0.0000.0000.016 0.000 0.0000.000 0.000 0.568 0.0000.0040.000 96.937 0.0000.000 0.000 820.065.180.828 0.000 0.00 0.00 180.0
4/1/2025 06:31 0.0000.0000.017 0.000 0.0000.000 0.000 0.728 0.0000.0020.000 97.245 0.0000.000 0.000 820.065.410.858 0.000 0.00 0.00 180.0
4/1/2025 06:31 0.0000.0000.015 0.000 0.0000.000 0.000 0.641 0.0000.0040.000 97.148 0.0000.000 0.000 820.065.310.817 0.000 0.00 0.00 180.0
NO2/Mid O2 System with Response Time
4/1/2025 06:34 99.8960.000-0.000 0.000 0.0000.000 0.237 1.217 0.0000.0010.000 0.000 0.0000.000 0.000 820.00.510.764 0.000 99.90 10.43 181.0
4/1/2025 06:34 102.2520.000-0.000 0.000 1.1590.000 0.249 1.074 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.540.809 0.000 102.25 10.44 181.0
4/1/2025 06:34 102.0870.000-0.000 0.000 0.9340.000 0.364 1.244 0.0000.0020.000 0.000 0.0000.000 0.000 820.00.540.816 0.000 102.09 10.44 181.0
Spike System with Response Time
4/1/2025 06:37 0.000251.1000.010 4.407 5.416495.722 2.832 1.377 3.8790.0720.363 0.000 252.6240.220 0.327 820.0255.923.972 9.930 251.10 0.00 180.0
4/1/2025 06:37 0.000251.1210.009 4.416 5.423495.911 2.832 1.347 3.9600.1380.072 0.000 252.3550.030 0.304 820.0255.573.917 9.921 251.12 0.00 180.0
4/1/2025 06:37 0.000251.6710.009 4.406 5.372495.628 2.844 1.314 3.9550.1410.000 0.000 252.4120.040 0.362 820.0255.733.896 9.926 251.67 0.00 180.0
Baseline System with Response Time
4/1/2025 06:39 0.0000.0000.001 0.000 0.0280.000 0.000 1.223 0.0000.0030.000 0.000 0.0000.000 0.000 820.00.410.615 0.000 0.00 0.00 180.0
4/1/2025 06:40 0.0000.0000.002 0.000 0.0000.000 0.000 1.283 0.0000.0030.000 0.000 0.0000.000 0.000 820.00.380.563 0.000 0.00 0.00 180.0
4/1/2025 06:40 0.0000.0000.002 0.000 0.0000.000 0.000 1.270 0.0000.0020.000 0.000 0.0000.000 0.000 820.00.400.601 0.000 0.00 0.00 180.0
Run 1 - A 30minute/60min
4/1/2025 07:12 0.00012.40816.089 9.621 107.30027.009 6.479 7.440 3.9570.2440.000 0.000 0.0000.475 0.399 820.01.901.651 0.000 12.41 0.00 180.0
4/1/2025 07:13 0.00012.08616.794 9.566 112.66532.591 5.419 7.022 4.8540.2760.000 0.000 0.0000.413 0.476 820.02.051.652 0.000 12.09 0.00 180.0
4/1/2025 07:14 0.00012.39717.255 9.525 112.88235.488 6.103 9.931 4.7040.2590.027 0.000 0.0000.452 0.478 820.02.001.571 0.000 12.40 0.00 180.0
4/1/2025 07:15 0.00012.22317.604 9.530 108.61224.106 5.534 10.334 4.1100.2410.000 0.000 0.0000.429 0.412 820.01.841.521 0.000 12.22 0.00 180.0
4/1/2025 07:16 0.00012.69317.804 9.514 103.44735.381 6.262 14.598 3.7050.2590.000 0.000 0.0000.414 0.409 820.01.861.562 0.000 12.69 0.00 180.0
4/1/2025 07:17 0.00012.94417.719 9.519 118.36047.885 5.952 13.134 5.2370.2300.162 0.000 0.0000.441 0.535 820.02.071.508 0.000 12.94 0.00 180.0
4/1/2025 07:18 0.00013.29417.620 9.541 103.91431.436 6.335 13.362 3.7380.2510.000 0.000 0.0000.460 0.420 820.01.851.523 0.000 13.29 0.00 180.0
4/1/2025 07:19 0.00013.11317.624 9.567 112.32045.362 6.120 15.970 4.7350.2540.032 0.000 0.0000.430 0.464 820.01.991.593 0.000 13.11 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 07:20 0.00012.33317.615 9.588 114.20540.277 5.731 12.345 4.9990.1930.046 0.000 0.0000.479 0.495 820.02.031.558 0.000 12.33 0.00 180.0
4/1/2025 07:21 0.00012.27717.573 9.585 111.27435.807 5.878 12.712 4.4990.2290.000 0.000 0.0000.451 0.452 820.01.941.551 0.000 12.28 0.00 180.0
4/1/2025 07:22 0.00012.15717.501 9.586 111.88132.536 5.579 11.531 4.5930.2290.000 0.000 0.0000.377 0.476 820.01.931.469 0.000 12.16 0.00 179.0
4/1/2025 07:23 0.00012.65717.536 9.662 111.17227.921 5.275 10.431 4.5050.2110.000 0.000 0.0000.365 0.432 820.01.851.476 0.000 12.66 0.00 180.0
4/1/2025 07:24 0.00012.48117.434 9.627 115.52237.193 5.470 10.688 5.2570.2580.000 0.000 0.0000.409 0.489 820.01.891.365 0.000 12.48 0.00 180.0
4/1/2025 07:25 0.00012.88517.344 9.605 112.29440.096 6.044 12.391 4.7550.2900.000 0.000 0.0000.365 0.455 820.01.851.408 0.000 12.89 0.00 180.0
4/1/2025 07:26 0.00012.84817.329 9.600 117.52846.706 5.592 13.940 5.2920.2480.000 0.000 0.0000.375 0.499 820.01.931.399 0.000 12.85 0.00 180.0
4/1/2025 07:27 0.00013.32617.283 9.588 119.20855.585 5.755 12.930 5.4840.2150.000 0.000 0.0000.438 0.527 820.01.961.360 0.000 13.33 0.00 180.0
4/1/2025 07:28 0.00013.03817.306 9.610 116.61549.772 5.178 12.256 5.2510.1930.000 0.000 0.0000.423 0.504 820.01.931.385 0.000 13.04 0.00 180.0
4/1/2025 07:29 0.00013.75317.268 9.583 117.57057.610 5.644 14.563 5.5060.2020.015 0.000 0.0000.431 0.522 820.01.991.416 0.000 13.75 0.00 180.0
4/1/2025 07:30 0.00014.13617.295 9.593 109.23350.466 6.045 17.413 4.5930.2090.000 0.000 0.0000.408 0.450 820.01.841.412 0.000 14.14 0.00 180.0
4/1/2025 07:31 0.00013.86817.271 9.592 111.71060.690 5.909 15.001 5.1020.1500.000 0.000 0.0000.432 0.456 820.01.861.423 0.000 13.87 0.00 180.0
4/1/2025 07:32 0.00014.38317.297 9.578 109.55782.043 6.369 25.787 4.5600.2340.000 0.000 0.0000.539 0.462 820.01.871.419 0.000 14.38 0.00 180.0
4/1/2025 07:33 0.00013.91717.283 9.592 119.73458.823 6.031 15.896 5.6230.2060.000 0.000 0.0000.425 0.510 820.01.871.283 0.000 13.92 0.00 180.0
4/1/2025 07:34 0.00013.91817.256 9.585 112.11053.677 5.809 16.374 4.9920.1810.100 0.000 0.0000.466 0.437 820.01.761.334 0.000 13.92 0.00 180.0
4/1/2025 07:35 0.00013.44717.216 9.575 108.17439.489 5.789 12.842 4.4000.1790.000 0.000 0.0000.401 0.430 820.01.781.375 0.000 13.45 0.00 180.0
4/1/2025 07:36 0.00013.18517.242 9.575 109.76938.429 5.700 14.507 4.6980.1460.029 0.000 0.0000.523 0.421 820.01.761.373 0.000 13.18 0.00 180.0
4/1/2025 07:37 0.00013.56617.257 9.568 118.00278.095 5.420 20.948 5.7500.1520.000 0.000 0.0000.444 0.535 820.01.971.354 0.000 13.57 0.00 180.0
4/1/2025 07:38 0.00015.11117.252 9.572 109.85359.433 6.276 17.350 4.8750.1340.079 0.000 0.0000.415 0.435 820.01.801.391 0.000 15.11 0.00 180.0
4/1/2025 07:39 0.00013.81017.284 9.577 116.81751.210 5.960 15.088 5.3050.1100.139 0.000 0.0000.484 0.463 820.01.881.428 0.000 13.81 0.00 180.0
4/1/2025 07:40 0.00014.15417.321 9.602 116.53151.109 5.858 14.120 5.3590.1560.282 0.000 0.0000.521 0.447 820.01.791.347 0.000 14.15 0.00 180.0
4/1/2025 07:41 0.00014.10817.316 9.594 114.94960.133 5.811 16.019 5.2390.1010.234 0.000 0.0000.435 0.449 820.01.831.400 0.000 14.11 0.00 180.0
0.00013.21717.333 9.581 112.77446.212 5.844 13.897 4.8560.2080.038 0.000 0.0000.437 0.465 820.001.8961.450 0.000 13.218 0.000 180.0Avg.
Spike 1
4/1/2025 07:44 0.00035.52415.602 9.144 102.219119.041 5.973 18.158 4.7640.1720.605 0.000 23.7720.224 0.738 820.026.501.872 0.884 35.52 0.00 180.0
Run 1 - B 30minute/60min
4/1/2025 07:49 0.00013.89717.273 9.580 104.34333.068 5.867 14.445 4.2020.1150.243 0.000 0.0000.417 0.341 820.01.591.369 0.000 13.90 0.00 180.0
4/1/2025 07:50 0.00013.76917.290 9.596 104.66328.258 5.476 12.306 4.0800.1550.108 0.000 0.0000.504 0.338 820.01.591.374 0.000 13.77 0.00 180.0
4/1/2025 07:51 0.00013.50917.341 9.616 109.15927.071 5.441 10.504 4.7420.0760.332 0.000 0.0000.472 0.365 820.01.631.342 0.000 13.51 0.00 180.0
4/1/2025 07:52 0.00013.40217.349 9.615 107.11831.152 4.936 10.824 4.6400.1130.665 0.000 0.0000.438 0.330 820.01.551.335 0.000 13.40 0.00 180.0
4/1/2025 07:53 0.00013.65317.297 9.572 104.23032.176 5.028 11.255 4.2690.0690.559 0.000 0.0000.491 0.345 820.01.591.351 0.000 13.65 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 07:54 0.00013.73517.299 9.585 111.53235.603 5.207 11.934 4.8140.0960.619 0.000 0.0000.502 0.367 820.01.581.266 0.000 13.74 0.00 180.0
4/1/2025 07:55 0.00013.61217.296 9.575 106.96637.904 5.510 13.965 4.5120.1000.533 0.000 0.0000.506 0.338 820.01.581.364 0.000 13.61 0.00 180.0
4/1/2025 07:56 0.00013.79617.301 9.594 108.14723.397 4.927 10.087 4.7850.1240.862 0.000 0.0000.471 0.323 820.01.561.374 0.000 13.80 0.00 180.0
4/1/2025 07:57 0.00013.80517.322 9.598 106.67537.165 5.558 12.604 4.6760.0770.733 0.000 0.0000.558 0.354 820.01.461.123 0.000 13.80 0.00 180.0
4/1/2025 07:58 0.00013.86817.354 9.610 102.16631.083 5.892 13.916 4.0330.0830.750 0.000 0.0000.454 0.283 820.01.451.321 0.000 13.87 0.00 180.0
4/1/2025 07:59 0.00013.98717.325 9.605 104.57328.901 5.456 12.114 4.3290.0860.684 0.000 0.0000.535 0.317 820.01.481.271 0.000 13.99 0.00 180.0
4/1/2025 08:00 0.00013.14917.304 9.604 103.64418.619 4.722 10.115 4.2020.0840.676 0.000 0.0000.446 0.262 820.01.421.346 0.000 13.15 0.00 180.0
4/1/2025 08:01 0.00014.28217.314 9.594 103.60234.941 5.983 14.105 4.2360.1230.705 0.000 0.0000.447 0.295 820.01.401.221 0.000 14.28 0.00 180.0
4/1/2025 08:02 0.00013.92117.292 9.576 107.46638.708 5.810 14.791 4.6570.0750.638 0.000 0.0000.482 0.325 820.01.491.262 0.000 13.92 0.00 180.0
4/1/2025 08:03 0.00013.35517.329 9.593 109.12932.704 4.768 11.863 5.0850.0730.814 0.000 0.0000.491 0.336 820.01.531.279 0.000 13.36 0.00 180.0
4/1/2025 08:04 0.00014.00717.298 9.574 108.07733.434 5.214 10.985 4.8940.0950.905 0.000 0.0000.508 0.332 820.01.511.266 0.000 14.01 0.00 180.0
4/1/2025 08:05 0.00014.47517.319 9.577 109.08954.513 5.195 13.940 5.2580.0810.988 0.000 0.0000.493 0.343 820.01.591.360 0.000 14.47 0.00 180.0
4/1/2025 08:06 0.00014.00717.326 9.586 101.82525.972 5.343 12.300 4.1000.0660.958 0.000 0.0000.508 0.261 820.01.371.267 0.000 14.01 0.00 180.0
4/1/2025 08:07 0.00013.63217.330 9.592 103.30222.734 5.178 9.899 4.1190.0550.938 0.000 0.0000.488 0.241 820.01.331.279 0.000 13.63 0.00 180.0
4/1/2025 08:08 0.00013.65817.353 9.591 109.09138.470 5.122 12.104 4.9960.0711.119 0.000 0.0000.471 0.313 820.01.431.214 0.000 13.66 0.00 180.0
4/1/2025 08:09 0.00013.58417.364 9.599 103.58023.475 5.237 10.357 4.2130.0680.958 0.000 0.0000.452 0.256 820.01.301.186 0.000 13.58 0.00 180.0
4/1/2025 08:10 0.00013.69217.372 9.604 114.37228.019 4.691 9.303 5.4580.0861.122 0.000 0.0000.455 0.334 820.01.491.236 0.000 13.69 0.00 180.0
4/1/2025 08:11 0.00013.64117.336 9.581 108.25530.626 5.244 9.455 4.8750.0371.075 0.000 0.0000.437 0.302 820.01.451.263 0.000 13.64 0.00 180.0
4/1/2025 08:12 0.00013.51417.314 9.562 101.42523.061 5.509 10.205 3.9050.0580.984 0.000 0.0000.560 0.232 820.01.191.089 0.000 13.51 0.00 180.0
4/1/2025 08:13 0.00012.98817.336 9.565 107.51118.374 4.811 8.263 4.6410.0701.227 0.000 0.0000.484 0.266 820.01.361.245 0.000 12.99 0.00 180.0
4/1/2025 08:14 0.00013.23917.343 9.559 95.77913.796 5.272 10.413 3.2180.1240.835 0.000 0.0000.511 0.175 820.01.181.249 0.000 13.24 0.00 180.0
4/1/2025 08:15 0.00013.13417.326 9.560 108.78523.081 4.661 9.317 4.7810.0571.232 0.000 0.0000.390 0.277 820.01.381.239 0.000 13.13 0.00 180.0
4/1/2025 08:16 0.00012.80017.350 9.553 108.08219.512 4.956 7.938 4.6770.0761.424 0.000 0.0000.538 0.272 820.01.321.161 0.000 12.80 0.00 180.0
4/1/2025 08:17 0.00013.22117.372 9.550 100.22322.402 5.945 11.379 3.7950.0401.377 0.000 0.0000.448 0.200 820.01.251.279 0.000 13.22 0.00 180.0
4/1/2025 08:18 0.00013.27417.382 9.575 102.29017.893 5.361 10.245 4.0180.0421.176 0.000 0.0000.508 0.206 820.01.281.304 0.000 13.27 0.00 180.0
0.00013.62017.327 9.585 105.83728.870 5.277 11.364 4.4740.0830.841 0.000 0.0000.482 0.298 820.001.4441.275 0.000 13.620 0.000 180.0Avg.
0.00013.41917.330 9.583 109.30537.541 5.561 12.631 4.6650.1450.440 0.000 0.0000.460 0.381 820.001.6701.362 0.000 13.419 0.000 180.0Run 1 Avg:
Baseline 1
4/1/2025 08:20 0.0000.0000.477 0.159 3.5920.000 0.000 1.974 0.2260.0120.000 0.000 0.0000.000 0.000 820.00.030.040 0.000 0.00 0.00 180.0
Run 2 - A 30minute/60min
4/1/2025 08:22 0.00012.65117.064 9.431 95.70515.069 4.262 7.217 3.5370.0670.659 0.000 0.0000.488 0.192 820.01.211.236 0.000 12.65 0.00 180.0
4/1/2025 08:23 0.00013.42217.308 9.539 107.25724.173 4.885 7.472 4.7240.0790.981 0.000 0.0000.498 0.276 820.01.381.236 0.000 13.42 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 08:24 0.00013.34717.323 9.557 95.33313.897 5.632 9.176 3.2470.0540.692 0.000 0.0000.471 0.179 820.01.181.235 0.000 13.35 0.00 180.0
4/1/2025 08:26 0.00013.50617.342 9.573 101.03212.834 5.663 8.281 3.8160.0520.933 0.000 0.0000.511 0.186 820.01.181.218 0.000 13.51 0.00 180.0
4/1/2025 08:27 0.00013.53117.341 9.564 108.70218.626 4.930 8.917 4.7450.0671.078 0.000 0.0000.527 0.230 820.01.311.275 0.000 13.53 0.00 180.0
4/1/2025 08:28 0.00013.39117.363 9.574 104.95516.107 4.865 8.525 4.2420.0861.079 0.000 0.0000.441 0.223 820.01.291.260 0.000 13.39 0.00 180.0
4/1/2025 08:29 0.00013.51117.356 9.578 105.7909.802 5.358 6.927 4.1970.0821.097 0.000 0.0000.478 0.196 820.01.191.198 0.000 13.51 0.00 180.0
4/1/2025 08:30 0.00013.30717.350 9.574 104.1379.387 4.357 5.973 4.3500.0741.251 0.000 0.0000.452 0.217 820.01.301.299 0.000 13.31 0.00 180.0
4/1/2025 08:31 0.00013.17017.367 9.551 107.66010.758 5.224 6.690 4.3880.0501.389 0.000 0.0000.495 0.221 820.01.211.153 0.000 13.17 0.00 180.0
4/1/2025 08:32 0.00013.54517.315 9.543 102.0428.810 5.085 6.712 3.9060.0631.378 0.000 0.0000.422 0.181 820.01.221.287 0.000 13.55 0.00 180.0
4/1/2025 08:33 0.00013.38417.310 9.542 106.43213.042 4.824 6.337 4.6270.0491.368 0.000 0.0000.389 0.218 820.01.331.345 0.000 13.38 0.00 180.0
4/1/2025 08:34 0.00013.29917.277 9.536 103.0719.392 4.871 6.430 4.0330.0501.302 0.000 0.0000.411 0.204 820.01.281.311 0.000 13.30 0.00 180.0
4/1/2025 08:35 0.00013.16617.352 9.539 107.23213.784 4.836 7.073 4.5750.0581.313 0.000 0.0000.471 0.238 820.01.281.202 0.000 13.17 0.00 180.0
4/1/2025 08:36 0.00013.34917.346 9.544 101.19310.691 5.254 6.774 3.8780.0451.196 0.000 0.0000.445 0.215 820.01.261.248 0.000 13.35 0.00 180.0
4/1/2025 08:37 0.00013.08917.337 9.540 102.26918.186 4.794 9.059 4.1370.0651.322 0.000 0.0000.414 0.213 820.01.281.282 0.000 13.09 0.00 180.0
4/1/2025 08:38 0.00013.79417.343 9.530 104.30320.369 6.065 10.857 4.0960.0391.381 0.000 0.0000.497 0.228 820.01.261.208 0.000 13.79 0.00 180.0
4/1/2025 08:39 0.00013.33617.327 9.532 109.91821.433 5.126 9.437 4.9270.0591.449 0.000 0.0000.370 0.270 820.01.411.298 0.000 13.34 0.00 180.0
4/1/2025 08:40 0.00013.29217.314 9.521 104.92421.228 5.695 9.602 4.1720.0521.203 0.000 0.0000.520 0.245 821.01.281.189 0.000 13.29 0.00 180.0
4/1/2025 08:41 0.00012.69117.314 9.525 95.4674.396 4.881 6.864 3.0520.0470.886 0.000 0.0000.487 0.185 821.01.221.275 0.000 12.69 0.00 180.0
4/1/2025 08:42 0.00012.67417.335 9.554 107.28815.130 4.624 7.081 4.3870.0611.201 0.000 0.0000.501 0.267 821.01.381.273 0.000 12.67 0.00 180.0
4/1/2025 08:43 0.00013.60517.240 8.549 102.9294.999 4.936 2.505 4.9360.4886.994 0.000 0.0000.429 0.054 820.00.310.308 0.000 13.61 0.00 180.0
4/1/2025 08:44 0.00012.81417.350 9.578 97.4864.988 4.498 5.531 3.2630.0590.710 0.000 0.0000.473 0.210 820.01.261.266 0.000 12.81 0.00 180.0
4/1/2025 08:45 0.00013.14417.324 9.565 105.81218.373 5.352 8.185 4.2190.0651.049 0.000 0.0000.439 0.248 821.01.351.276 0.000 13.14 0.00 180.0
4/1/2025 08:46 0.00013.70417.252 9.539 95.44515.077 5.466 10.941 3.2830.0840.760 0.000 0.0000.460 0.210 821.01.341.377 0.000 13.70 0.00 180.0
4/1/2025 08:47 0.00013.23617.253 9.556 103.12214.297 5.367 8.757 3.9690.0840.740 0.000 0.0000.484 0.258 821.01.391.312 0.000 13.24 0.00 180.0
4/1/2025 08:48 0.00013.26217.324 9.576 99.61413.701 5.370 9.151 3.4700.0790.815 0.000 0.0000.515 0.223 820.01.281.254 0.000 13.26 0.00 180.0
4/1/2025 08:49 0.00013.12017.301 9.566 107.49215.653 5.287 8.033 4.4660.0761.045 0.000 0.0000.466 0.273 820.01.441.339 0.000 13.12 0.00 180.0
4/1/2025 08:50 0.00013.62917.262 9.548 102.13118.954 5.957 10.490 3.9400.0750.925 0.000 0.0000.494 0.242 820.01.401.374 0.000 13.63 0.00 180.0
4/1/2025 08:51 0.00013.09517.264 9.546 103.03710.245 4.881 8.486 3.8090.0670.772 0.000 0.0000.418 0.253 820.01.351.272 0.000 13.09 0.00 180.0
4/1/2025 08:52 0.00013.46817.211 9.559 103.3278.891 5.063 6.608 3.9710.0940.990 0.000 0.0000.369 0.236 820.01.401.390 0.000 13.47 0.00 180.0
0.00013.28417.306 9.514 103.17013.743 5.114 7.803 4.0790.0791.265 0.000 0.0000.461 0.220 820.201.2661.240 0.000 13.284 0.000 180.0Avg.
Spike 2
4/1/2025 08:54 0.01629.80814.360 8.469 88.33254.537 4.458 4.736 3.9650.1260.533 0.000 21.7580.304 0.625 820.023.901.342 0.809 29.82 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
4/1/2025 08:56 0.00015.12417.221 9.628 109.40319.451 4.845 6.608 5.1970.0810.937 0.000 0.2250.190 0.589 820.02.271.295 0.000 15.12 0.00 180.0
4/1/2025 08:57 0.00013.26217.292 9.559 98.37813.285 5.458 7.242 3.4040.0480.847 0.000 0.0000.506 0.254 820.01.271.149 0.000 13.26 0.00 180.0
4/1/2025 08:58 0.00013.15417.246 9.550 101.93211.410 4.981 6.876 3.8160.0580.811 0.000 0.0000.579 0.261 820.01.201.013 0.000 13.15 0.00 180.0
4/1/2025 08:59 0.00012.79117.250 9.561 108.69413.441 5.043 6.070 4.6170.0720.958 0.000 0.0000.543 0.290 820.01.381.196 0.000 12.79 0.00 180.0
4/1/2025 09:00 0.00013.30617.252 9.569 104.95217.918 5.548 7.940 4.1230.0440.925 0.000 0.0000.581 0.274 820.01.261.061 0.000 13.31 0.00 180.0
4/1/2025 09:01 0.00013.29117.246 9.576 104.13210.375 5.602 8.228 4.0020.0710.934 0.000 0.0000.497 0.260 820.01.371.278 0.000 13.29 0.00 180.0
4/1/2025 09:02 0.00013.80317.214 9.574 100.57710.465 5.108 7.571 3.6550.0670.844 0.000 0.0000.437 0.232 820.01.371.358 0.000 13.80 0.00 180.0
4/1/2025 09:04 0.00013.93017.217 9.572 107.09919.716 5.552 8.344 4.6480.0661.062 0.000 0.0000.361 0.277 820.01.481.388 0.000 13.93 0.00 180.0
4/1/2025 09:05 0.00013.71017.246 9.571 99.05815.740 5.368 8.008 3.7580.0770.837 0.000 0.0000.432 0.251 820.01.351.277 0.000 13.71 0.00 180.0
4/1/2025 09:06 0.00013.37817.222 9.544 103.73917.881 5.014 8.906 4.1820.0840.932 0.000 0.0000.522 0.284 820.01.421.278 0.000 13.38 0.00 180.0
4/1/2025 09:07 0.00013.43417.239 9.535 92.72517.514 5.895 10.999 3.0030.0880.990 0.000 0.0000.495 0.227 820.01.221.150 0.000 13.43 0.00 180.0
4/1/2025 09:08 0.00013.40417.241 9.542 96.65910.964 5.411 9.427 3.3190.0761.064 0.000 0.0000.496 0.224 820.01.241.192 0.000 13.40 0.00 180.0
4/1/2025 09:09 0.00013.39217.236 9.562 100.96412.679 5.139 8.392 3.7130.0770.976 0.000 0.0000.410 0.249 820.01.341.266 0.000 13.39 0.00 180.0
4/1/2025 09:10 0.00013.82917.248 9.575 102.31613.227 5.738 8.438 3.9920.0320.933 0.000 0.0000.431 0.252 820.01.431.383 0.000 13.83 0.00 180.0
4/1/2025 09:11 0.00013.67317.179 9.550 102.81711.354 5.598 8.139 3.9360.0520.881 0.000 0.0000.460 0.226 820.01.391.405 0.000 13.67 0.00 180.0
4/1/2025 09:12 0.00014.06617.186 9.558 103.14610.646 5.210 7.554 4.1100.0501.052 0.000 0.0000.375 0.248 820.01.451.429 0.000 14.07 0.00 180.0
4/1/2025 09:13 0.00013.71517.204 9.564 106.9946.457 4.970 5.697 4.4850.0431.074 0.000 0.0000.423 0.233 820.01.461.491 0.000 13.71 0.00 180.0
4/1/2025 09:14 0.00013.65517.236 9.570 103.92013.910 5.412 7.408 4.2210.0621.127 0.000 0.0000.439 0.237 820.01.411.405 0.000 13.66 0.00 180.0
4/1/2025 09:15 0.00013.83617.231 9.569 103.62010.527 5.398 7.566 4.0590.0590.987 0.000 0.0000.364 0.234 820.01.421.434 0.000 13.84 0.00 180.0
4/1/2025 09:16 0.00013.23017.239 9.572 98.1191.764 4.368 5.125 3.5090.0490.825 0.000 0.0000.430 0.205 820.01.391.468 0.000 13.23 0.00 180.0
4/1/2025 09:17 0.00013.02417.261 9.569 105.4847.921 4.572 5.576 4.1710.0571.031 0.000 0.0000.555 0.241 820.01.211.094 0.000 13.02 0.00 180.0
4/1/2025 09:18 0.00013.43117.266 9.566 100.2905.112 5.291 5.942 3.3110.0611.117 0.000 0.0000.587 0.222 820.01.141.042 0.000 13.43 0.00 180.0
4/1/2025 09:19 0.00012.93717.264 9.552 98.6446.795 5.067 6.096 3.3780.0550.952 0.000 0.0000.515 0.188 820.01.201.245 0.000 12.94 0.00 180.0
4/1/2025 09:20 0.00013.24317.265 9.556 102.44210.642 4.651 6.590 3.9160.0630.895 0.000 0.0000.470 0.242 820.01.281.197 0.000 13.24 0.00 180.0
4/1/2025 09:21 0.00013.53017.261 9.577 102.2995.649 4.931 5.722 3.7020.0660.841 0.000 0.0000.415 0.228 820.01.341.324 0.000 13.53 0.00 180.0
4/1/2025 09:22 0.00013.29917.295 9.579 101.6206.012 5.336 6.475 3.6090.0461.069 0.000 0.0000.473 0.206 820.01.281.300 0.000 13.30 0.00 180.0
4/1/2025 09:23 0.00013.34617.302 9.571 102.70110.905 5.075 7.979 3.8060.0681.153 0.000 0.0000.395 0.238 820.01.351.315 0.000 13.35 0.00 180.0
4/1/2025 09:24 0.00013.24517.297 9.565 101.72310.235 5.291 8.133 3.6720.0670.811 0.000 0.0000.462 0.232 820.01.321.278 0.000 13.24 0.00 180.0
4/1/2025 09:25 0.00013.10217.274 9.552 98.0425.526 4.924 7.005 3.2720.0590.693 0.000 0.0000.428 0.212 820.01.331.356 0.000 13.10 0.00 180.0
4/1/2025 09:26 0.00012.80217.264 9.554 101.8924.791 4.345 5.712 3.7060.0601.022 0.000 0.0000.403 0.204 820.01.311.346 0.000 12.80 0.00 180.0
0.00013.46517.246 9.565 102.14611.077 5.171 7.326 3.8760.0620.953 0.000 0.0080.456 0.251 820.001.3631.280 0.000 13.464 0.000 180.0Avg.
0.00013.37517.276 9.540 102.65812.410 5.142 7.564 3.9780.0701.109 0.000 0.0040.458 0.235 820.101.3141.260 0.000 13.374 0.000 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
4/1/2025 09:28 0.0000.0000.182 0.000 1.2480.000 0.169 1.649 0.2490.0000.000 0.000 0.0000.000 0.000 820.00.000.000 0.000 0.00 0.00 180.0
Run 3 - A 30minute/60min
4/1/2025 09:30 0.00012.98614.514 8.236 91.1467.224 4.517 6.180 3.3490.1530.000 0.000 0.0000.346 0.269 820.01.431.339 0.000 12.99 0.00 180.0
4/1/2025 09:31 0.00012.77717.255 9.545 104.36511.713 5.109 6.099 4.0910.0570.675 0.000 0.0000.404 0.278 820.01.441.331 0.000 12.78 0.00 180.0
4/1/2025 09:32 0.00012.33917.319 9.561 104.69618.875 5.112 8.723 4.1220.0410.810 0.000 0.0000.457 0.276 820.01.461.360 0.000 12.34 0.00 180.0
4/1/2025 09:33 0.00012.67017.349 9.585 100.4748.781 5.213 6.771 3.4320.0650.631 0.000 0.0000.446 0.247 820.01.421.384 0.000 12.67 0.00 180.0
4/1/2025 09:34 0.00012.44517.385 9.587 105.03120.693 5.684 10.045 4.0920.0320.725 0.000 0.0000.433 0.284 820.01.511.407 0.000 12.45 0.00 180.0
4/1/2025 09:35 0.00012.39017.307 9.560 101.50116.599 5.615 10.493 3.5380.0580.642 0.000 0.0000.408 0.279 820.01.491.398 0.000 12.39 0.00 180.0
4/1/2025 09:36 0.00012.46517.327 9.590 103.18214.831 5.355 9.911 3.7730.1170.606 0.000 0.0000.457 0.289 820.01.521.414 0.000 12.47 0.00 180.0
4/1/2025 09:37 0.00012.63017.334 9.600 101.74113.561 4.993 8.669 3.7460.0610.649 0.000 0.0000.366 0.272 820.01.481.411 0.000 12.63 0.00 180.0
4/1/2025 09:38 0.00012.62617.296 9.573 106.25524.719 5.187 10.611 4.1710.0950.742 0.000 0.0000.376 0.334 820.01.631.438 0.000 12.63 0.00 180.0
4/1/2025 09:39 0.00012.80717.285 9.554 103.07121.307 5.879 11.830 3.8410.0950.514 0.000 0.0000.374 0.313 820.01.591.451 0.000 12.81 0.00 180.0
4/1/2025 09:40 0.00012.05917.255 9.566 101.6517.399 4.561 6.916 3.6010.0780.411 0.000 0.0000.393 0.284 820.01.521.430 0.000 12.06 0.00 180.0
4/1/2025 09:42 0.00011.92617.264 9.585 98.5595.395 4.394 5.832 3.2330.0960.332 0.000 0.0000.409 0.275 820.01.461.367 0.000 11.93 0.00 180.0
4/1/2025 09:43 0.00012.41317.271 9.590 109.24221.611 4.514 7.900 4.4810.0830.492 0.000 0.0000.422 0.371 820.01.661.371 0.000 12.41 0.00 180.0
4/1/2025 09:44 0.00012.94317.255 9.587 100.75816.696 5.847 9.272 3.6410.0820.389 0.000 0.0000.468 0.304 820.01.551.411 0.000 12.94 0.00 180.0
4/1/2025 09:45 0.00012.55217.284 9.597 98.00812.408 5.165 9.430 3.2340.1170.320 0.000 0.0000.439 0.272 820.01.511.448 0.000 12.55 0.00 180.0
4/1/2025 09:46 0.00013.11617.286 9.615 107.89820.589 5.053 8.376 4.4170.1160.309 0.000 0.0000.413 0.365 820.01.661.392 0.000 13.12 0.00 180.0
4/1/2025 09:47 0.00012.80917.269 9.591 105.29717.925 5.207 8.659 4.0640.0850.372 0.000 0.0000.400 0.333 820.01.651.480 0.000 12.81 0.00 180.0
4/1/2025 09:48 0.00012.40417.263 9.597 98.71710.475 4.599 6.900 3.5880.0990.000 0.000 0.0000.427 0.285 820.01.501.388 0.000 12.40 0.00 180.0
4/1/2025 09:49 0.00012.75417.258 9.585 106.01625.208 5.192 9.096 4.3430.0560.336 0.000 0.0000.503 0.355 820.01.611.352 0.000 12.75 0.00 180.0
4/1/2025 09:50 0.00012.32617.278 9.590 103.18419.334 5.392 9.028 3.7250.1240.397 0.000 0.0000.421 0.301 820.01.461.284 0.000 12.33 0.00 180.0
4/1/2025 09:51 0.00012.44817.268 9.609 102.92613.405 4.983 7.832 3.8090.1390.578 0.000 0.0000.381 0.303 820.01.491.320 0.000 12.45 0.00 180.0
4/1/2025 09:52 0.00013.20517.220 9.576 106.11436.369 5.188 10.428 4.3990.1410.512 0.000 0.0000.484 0.361 820.01.581.289 0.000 13.20 0.00 180.0
4/1/2025 09:53 0.00013.06317.221 9.578 107.14334.833 4.981 11.433 4.4310.1330.673 0.000 0.0000.474 0.366 820.01.531.205 0.000 13.06 0.00 180.0
4/1/2025 09:54 3.84821.35516.811 8.171 115.59325.407 5.284 7.231 2.3600.0002.128 0.000 0.0000.000 0.832 820.01.660.000 0.000 25.20 0.00 180.0
4/1/2025 09:55 0.00012.33617.220 9.586 93.66112.264 4.715 9.128 2.8970.0790.281 0.000 0.0000.444 0.245 820.01.461.461 0.000 12.34 0.00 180.0
4/1/2025 09:56 0.00012.90417.264 9.580 101.05620.009 5.662 10.358 3.6980.1170.560 0.000 0.0000.514 0.299 820.01.471.312 0.000 12.90 0.00 180.0
4/1/2025 09:57 0.00012.83217.235 9.600 92.95519.370 4.311 10.196 3.0720.0830.501 0.000 0.0000.421 0.276 820.01.541.476 0.000 12.83 0.00 180.0
4/1/2025 09:58 0.00013.47217.256 9.601 93.51727.288 4.952 10.847 3.1820.0850.215 0.000 0.0000.481 0.296 820.01.511.378 0.000 13.47 0.00 180.0
4/1/2025 09:59 0.00013.14917.187 9.577 98.34419.422 5.179 9.296 3.5980.1330.348 0.000 0.0000.329 0.301 820.01.591.478 0.000 13.15 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 10:00 0.00012.49417.235 9.599 102.76116.204 4.351 7.268 3.9650.1150.548 0.000 0.0000.440 0.315 820.01.561.394 0.000 12.49 0.00 180.0
0.12812.95717.166 9.492 102.16217.997 5.073 8.825 3.7300.0910.523 0.000 0.0000.411 0.319 820.001.5311.339 0.000 13.085 0.000 180.0Avg.
Spike 3
4/1/2025 10:02 0.00030.49514.362 8.533 92.75766.884 4.826 8.010 4.2890.1040.404 0.000 21.9930.347 0.692 820.024.381.507 0.819 30.50 0.00 180.0
Run 3 - B 30minute/60min
4/1/2025 10:04 0.00013.15517.222 9.617 94.0898.794 4.809 7.550 3.0620.1000.416 0.000 0.0000.372 0.291 819.01.521.400 0.000 13.16 0.00 180.0
4/1/2025 10:05 0.00013.34517.218 9.600 101.92621.308 5.553 9.527 3.8760.1050.500 0.000 0.0000.457 0.298 820.01.511.378 0.000 13.35 0.00 180.0
4/1/2025 10:06 0.00013.23617.231 9.603 98.81622.390 5.047 10.203 3.6790.1380.511 0.000 0.0000.401 0.307 820.01.531.367 0.000 13.24 0.00 180.0
4/1/2025 10:07 0.00013.80017.243 9.601 104.44829.545 5.780 13.680 4.0360.0860.652 0.000 0.0000.451 0.339 820.01.581.350 0.000 13.80 0.00 180.0
4/1/2025 10:08 0.00013.24117.219 9.592 106.51933.958 5.186 10.677 4.6500.0780.577 0.000 0.0000.438 0.375 820.01.651.356 0.000 13.24 0.00 180.0
4/1/2025 10:10 0.00012.93117.242 9.601 104.61024.501 5.288 11.436 4.0920.1030.562 0.000 0.0000.466 0.331 820.01.591.396 0.000 12.93 0.00 180.0
4/1/2025 10:11 0.00013.27017.219 9.607 98.93811.829 5.239 8.763 3.3940.1260.443 0.000 0.0000.346 0.282 820.01.491.391 0.000 13.27 0.00 180.0
4/1/2025 10:12 0.00013.52317.243 9.602 101.42427.325 5.333 12.345 3.7370.0910.657 0.000 0.0000.480 0.304 820.01.501.337 0.000 13.52 0.00 180.0
4/1/2025 10:13 0.00014.20417.248 9.592 103.13848.104 6.478 18.529 4.0210.1510.390 0.000 0.0000.505 0.349 820.01.561.301 0.000 14.20 0.00 180.0
4/1/2025 10:14 0.00013.82417.249 9.600 103.82831.928 5.370 14.119 4.2870.0930.758 0.000 0.0000.391 0.337 820.01.621.428 0.000 13.82 0.00 180.0
4/1/2025 10:15 0.00013.82617.253 9.598 102.13327.453 5.589 11.648 3.9890.0790.643 0.000 0.0000.454 0.323 820.01.571.391 0.000 13.83 0.00 180.0
4/1/2025 10:16 0.00013.45517.251 9.610 102.70926.478 5.149 11.046 3.9620.0740.675 0.000 0.0000.464 0.320 820.01.541.351 0.000 13.45 0.00 180.0
4/1/2025 10:17 0.00013.81017.232 9.595 101.32426.586 5.358 12.265 3.8920.1240.887 0.000 0.0000.535 0.318 820.01.551.376 0.000 13.81 0.00 180.0
4/1/2025 10:18 0.00013.70617.246 9.591 96.33622.015 4.998 12.692 3.3580.0830.730 0.000 0.0000.445 0.265 820.01.431.353 0.000 13.71 0.00 180.0
4/1/2025 10:19 0.00013.39017.264 9.609 105.36825.419 4.842 10.543 4.3690.0690.603 0.000 0.0000.453 0.324 820.01.541.338 0.000 13.39 0.00 180.0
4/1/2025 10:20 0.00014.29617.251 9.577 96.67038.784 5.356 16.115 3.4430.0690.713 0.000 0.0000.482 0.270 820.01.451.373 0.000 14.30 0.00 180.0
4/1/2025 10:21 0.00014.19017.228 9.573 94.80224.228 5.620 13.824 3.2550.0810.787 0.000 0.0000.487 0.260 820.01.441.374 0.000 14.19 0.00 180.0
4/1/2025 10:22 187.46312.37015.551 5.961 96.08539.167 7.014 17.275 12.9620.6290.000 0.353 0.1370.000 0.000 820.08.0011.441 0.051 199.83 0.00 180.0
4/1/2025 10:23 0.00013.68417.292 9.576 98.90727.941 4.800 13.215 3.5810.0630.770 0.000 0.0000.524 0.291 820.01.481.345 0.000 13.68 0.00 180.0
4/1/2025 10:24 0.00014.32117.258 9.572 103.35446.226 4.693 13.331 4.0780.0720.857 0.000 0.0000.541 0.309 820.01.491.315 0.000 14.32 0.00 180.0
4/1/2025 10:25 0.00014.15017.263 9.582 106.09233.637 5.190 10.401 4.3830.1231.063 0.000 0.0000.500 0.327 820.01.551.345 0.000 14.15 0.00 180.0
4/1/2025 10:26 0.00013.83317.255 9.598 107.72736.456 4.920 10.009 4.6240.1540.980 0.000 0.0000.610 0.335 820.01.411.112 0.000 13.83 0.00 180.0
4/1/2025 10:27 0.00014.27117.276 9.596 103.65126.972 5.693 11.376 3.9520.1150.903 0.000 0.0000.525 0.286 820.01.471.345 0.000 14.27 0.00 180.0
4/1/2025 10:28 0.00013.71017.256 9.601 105.13420.633 4.826 9.213 4.0930.1060.921 0.000 0.0000.603 0.284 820.01.361.193 0.000 13.71 0.00 180.0
4/1/2025 10:29 0.00013.35117.263 9.583 105.63923.257 5.248 9.206 4.1810.1361.090 0.000 0.0000.620 0.297 820.01.361.153 0.000 13.35 0.00 180.0
4/1/2025 10:30 0.00013.66017.294 9.581 100.98715.338 4.964 8.687 3.7510.0721.260 0.000 0.0000.559 0.242 820.01.361.309 0.000 13.66 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 10:31 0.00013.26017.325 9.583 100.2267.422 4.285 6.056 3.3630.1041.289 0.000 0.0000.621 0.236 820.01.301.246 0.000 13.26 0.00 180.0
4/1/2025 10:32 0.00013.09917.299 9.570 104.58610.120 4.298 5.903 3.9740.0861.454 0.000 0.0000.661 0.271 820.01.391.265 0.000 13.10 0.00 180.0
4/1/2025 10:33 0.00013.44217.242 9.561 99.99716.057 5.065 7.726 3.4210.0501.130 0.000 0.0000.702 0.243 820.01.341.281 0.000 13.44 0.00 180.0
4/1/2025 10:34 0.00013.47717.263 9.574 98.64315.883 5.132 9.622 3.2030.0391.202 0.000 0.0000.759 0.258 820.01.431.369 0.000 13.48 0.00 180.0
6.24913.59417.197 9.470 101.60425.658 5.237 11.233 4.1560.1130.781 0.012 0.0050.495 0.289 819.971.7001.666 0.002 19.843 0.000 180.0Avg.
3.18913.27517.181 9.481 101.88321.828 5.155 10.029 3.9430.1020.652 0.006 0.0020.453 0.304 819.981.6161.502 0.001 16.464 0.000 180.0Run 3 Avg:
Baseline 3
4/1/2025 10:46 0.1670.000-0.000 0.000 0.6340.000 0.000 1.373 0.0000.0040.000 0.000 0.0000.000 0.000 820.00.400.595 0.000 0.17 0.00 180.0
Post CTS
4/1/2025 10:49 0.0000.0000.014 0.000 0.0000.000 0.000 0.449 0.4070.0000.000 97.287 0.0000.000 0.000 820.065.080.329 0.000 0.00 0.00 180.0
4/1/2025 10:49 0.0000.0000.011 0.000 0.0000.000 0.000 0.515 0.0910.0140.000 98.110 0.0000.000 0.000 820.065.790.567 0.000 0.00 0.00 180.0
4/1/2025 10:49 0.0000.0000.011 0.000 0.0180.000 0.000 0.533 0.1900.0000.000 97.582 0.0000.000 0.000 820.065.060.000 0.000 0.00 0.00 180.0
4/1/2025 10:49 0.0000.0000.010 0.000 0.0000.000 0.000 0.662 0.1840.0620.000 98.053 0.0000.000 0.000 820.065.650.411 0.000 0.00 0.00 180.0
Post NO2/Mid O2
4/1/2025 10:52 101.0300.000-0.000 0.000 0.0060.000 0.334 1.288 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.190.280 0.000 101.03 10.42 180.0
4/1/2025 10:52 101.3770.000-0.000 0.000 0.5240.000 0.350 1.396 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.260.385 0.000 101.38 10.43 180.0
4/1/2025 10:52 101.4050.000-0.000 0.000 1.3680.000 0.330 1.161 0.0000.0060.000 0.000 0.0000.000 0.000 820.00.250.376 0.000 101.40 10.38 180.0
Post 5-Gas
4/1/2025 10:54 0.000251.6520.004 4.365 5.587493.186 2.811 1.450 4.2360.0560.134 0.000 251.6400.082 0.374 820.0254.793.606 9.918 251.65 0.00 180.0
4/1/2025 10:54 0.000251.680-0.000 4.522 5.165492.964 2.834 2.351 2.3540.0150.000 0.308 247.5300.000 1.177 820.0251.642.328 9.829 251.68 0.00 180.0
4/1/2025 10:54 0.000252.2460.002 4.396 5.532491.934 2.836 1.593 4.7350.0790.104 0.000 251.6050.062 0.319 820.0254.833.887 9.912 252.25 0.00 180.0
4/1/2025 10:54 0.000251.924-0.000 4.529 6.032492.034 2.775 2.770 2.6970.1270.125 0.318 247.4310.405 1.149 820.0251.552.418 9.828 251.92 0.00 180.0
4/1/2025 10:54 0.000251.5650.002 4.383 5.166493.169 2.837 1.579 4.2130.0220.000 0.000 251.7560.090 0.358 820.0254.813.510 9.921 251.56 0.00 180.0
4/1/2025 10:54 0.000251.7810.005 4.380 5.251494.053 2.835 1.459 4.4210.0690.054 0.000 251.6880.000 0.382 820.0255.053.891 9.910 251.78 0.00 180.0
4/1/2025 10:55 0.000251.9210.004 4.377 5.253493.472 2.812 1.635 4.5990.0840.000 0.000 251.8990.100 0.339 820.0255.183.910 9.909 251.92 0.00 180.0
4/1/2025 10:55 0.000252.3230.001 4.362 5.151492.065 2.862 1.643 4.5990.0610.000 0.000 251.4780.067 0.403 820.0254.933.973 9.915 252.32 0.00 180.0
End of Test Purge
4/1/2025 10:57 0.0000.000-0.000 0.000 0.1340.000 0.000 1.413 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.000.000 0.000 0.00 0.00 180.0
4/1/2025 10:57 0.0000.000-0.000 0.000 0.4280.000 0.000 1.229 0.0000.0140.000 0.000 0.0000.000 0.000 820.00.070.103 0.000 0.00 0.00 180.0
4/1/2025 10:57 0.0140.000-0.000 0.000 0.7120.000 0.000 1.277 0.0000.0150.000 0.000 0.0000.000 0.000 820.00.110.158 0.000 0.01 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/1/2025 10:57 0.0000.000-0.000 0.000 0.3980.000 0.000 1.395 0.0000.0060.000 0.000 0.0000.000 0.000 820.00.210.315 0.000 0.00 0.00 180.0
4/1/2025 10:58 0.0000.000-0.000 0.000 0.0040.000 0.000 1.318 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.110.169 0.000 0.00 0.00 180.0
4/1/2025 10:58 0.0000.000-0.000 0.000 0.2370.000 0.000 1.336 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.100.153 0.000 0.00 0.00 180.0
4/1/2025 10:58 0.0000.000-0.000 0.000 0.4650.000 0.000 1.164 0.0000.0000.000 0.000 0.0000.000 0.000 820.00.210.318 0.000 0.00 0.00 180.0
4/1/2025 10:58 0.0000.000-0.000 0.000 0.4540.000 0.000 1.123 0.0000.0000.000 0.000 0.0000.109 0.000 820.00.150.218 0.000 0.00 0.00 180.0
4/1/2025 10:58 0.0000.000-0.000 0.000 0.0000.000 0.000 1.237 0.0000.0110.000 0.000 0.0000.000 0.000 820.00.220.337 0.000 0.00 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 4/2/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:11:01 AM 02:46 PM
Source:
Unit Number: 2026-01
Serial Number: WAU-1641324
Engine Hours:10859
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.005 0.183 0.031
0.386 9.240 1.636
2.000 0.300 1.000 0.150 0.700 0.030
0.001 0.039 0.007
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Lynn Huber
3
Hunter Newton
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 2026-01 with a serial number of WAU-1641324 which is a Waukesha 9394 GSI engine located at
Crusoe Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of:
Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on
4/2/2025 by Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality
control tests were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2108 BHP and 1199 RPM which is 84.33% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 2026-01 is authorized
to operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 2026-01Unit ID
Make Waukesha Site Elevation ft.5226
Model 9394 GSI Atmospheric Pressure psi.12.04
Serial Number WAU-1641324 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2100 2100 2125 2108
1200 1200 1198 1199
Percent Load %
Intake Manifold Pressure (hg)
84.00%84.00%85.00%84.33%
59.00 59.00 58.00 58.67
Intake Manifold Temperature (F)124.00 125.00 124.00 124.33
Ambient Conditions
Ambient Temperature Dry (F)46.00 39.00 41.00 42.00
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
165660.25 166191.17 166887.02 166246.15
4690.93 4705.97 4725.67 4707.52
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.17 0.17 0.17
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %17.21%17.19%17.09%17.16%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.00%0.00%0.00%0.00%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
11:01 AM 12:12 PM 01:20 PM 4/2/2025
State
NOx (mol wt) 46.01
0.913 1.175 1.979 1.355NMNEHC (ppmvw)
1.102 1.419 2.386 1.636NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
311.136 400.539 673.679 461.785 FailNMNEHC (ppbvd) @15% O2
0.005 0.006 0.010 0.0070.700 0.030 PassNMNEHC (g/hp-hr)
0.021 0.027 0.046 0.0310.170 PassNMNEHC (lbs/hr)
0.311 0.401 0.674 0.462 FailNMNEHC (ppmvd) @15% O2
0.0000.002CO (g/hp-hr)0.000 0.0012.000 0.300 Pass
CO (ppmvw)0.091 0.744 0.124 0.319
CO (ppmvd)0.110 0.898 0.149 0.386
CO (mol wt) 28.01
CO (ppmvd) @15% O2 0.031 0.253 0.042 0.109 Fail
CO (ppbvd) @15% O2 31.028 253.448 42.052 108.843 Fail
0.0020.011CO (lbs/hr)0.001 0.0051.650 Pass
NOx (g/hp-hr)0.036 0.047 0.035 0.0391.000 0.150 Pass
NOx (ppmvw)6.996 9.056 6.911 7.654
NOx (ppmvd)8.450 10.935 8.336 9.240
NOx (ppbvd) @15% O2 2385.433 3087.050 2353.196 2608.559 Fail
NOx (ppmvd) @15% O2 2.385 3.087 2.353 2.609 Fail
NOx (lbs/hr)0.167 0.217 0.166 0.1830.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
0.09
0.00
6.06 0.94 7.00
0.00%
0.00%
0.00%
17.21%
4.96 1.08 0.00%17.10%
29.04 0.00 0.00%15.68%
7.15 0.80 0.00%17.32%
0.00 0.18 0.18 0.00%0.04%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.18 0.18 0.00%0.04%
0.00 5.08 1.37 6.44 0.00%17.09%
47.62 30.51 0.00 30.50 0.00%15.61%
1.49 10.87 0.81 11.67 0.00%17.29%
0.00 0.00 0.00 0.00 0.00%0.02%
Avg. Wet 0.74 7.97 1.09 9.06 1.18 0.00%17.19%
NO2NO
0.35
1.53
23.50
0.82
0.43
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 5.69 0.90 6.59 0.00%17.01%
44.66 29.26 0.00 29.26 0.00%15.60%
0.25 6.39 0.84 7.24 0.00%17.18%
0.00 0.00 0.01 0.01 0.00%0.00%
0.00 0.00 0.00 0.00 0.43 0.00%0.02%
Avg. Wet 0.12 6.04 0.87 6.91 1.98 0.00%17.09%
NO2NO
0.48
0.93
22.07
3.03
NMNEHC
0.65
NO2
0.400.00
1.14
21.86
0.69
0.35
0.91
0.40
6.04
29.04
7.95
0.00
0.18
0.00
50.08
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.35
Yes
20.00
10.00
21.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%17.21
29.88
0.37
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.72
0.00
0.00
1001.36
0.03
29.58
29.61
893.19
1352.86
478.44
27.84
65.95
143.90
200092.10
165660.25
Run 2
17.19
29.85
0.40
11.59
0.00
0.00
1006.77
0.03
29.74
29.77
896.31
1355.98
480.17
27.81
68.34
143.88
200682.47
166191.17
Run 3
17.09
29.86
0.41
11.64
0.00
0.00
1005.42
0.03
29.70
29.73
890.38
1350.05
476.88
27.83
69.07
143.88
201294.24
166887.01
17.16
29.86
0.39
11.65
0.00
0.00
1004.52
0.03
29.67
29.70
893.29
1352.96
478.50
27.82
67.82
143.88
200689.6
166246.15
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.38
Exhaust Temp F
893.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.36
0.41
0.37
891.00
890.00
898.00
0.38
0.37
0.35
895.00
893.00
892.00
0.35
0.40
0.34
891.00
890.00
894.00
0.36 896.00
0.41
0.34
0.34
894.00
895.00
893.00
0.36
0.35
0.37
892.00
894.00
893.19
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.34
Exhaust Temp F
890.00
0.39
0.39
0.44
887.00
889.00
892.00
0.42
0.46
0.37
891.00
890.00
887.00
0.35
0.40
0.44
888.00
893.00
894.00
0.43 891.00
0.47
0.48
0.42
892.00
893.00
887.00
0.38
0.35
889.00
893.00
890.380.41
Run 2
Δpstd (in) H2O
0.39
Exhaust Temp F
896.00
0.35
0.41
0.42
898.00
896.00
897.00
0.38
0.35
0.39
894.00
893.00
898.00
0.43
0.44
0.41
897.00
895.00
896.00
0.40 897.00
0.36
0.39
0.44
894.00
896.00
898.00
0.45
0.36
899.00
897.00
0.40 896.31
Pass
Strat Check
52.469Check 1
53.238Check 2
52.688Check 3
MethaneGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.722)+ .32(0)+ .28(88.278+0) = 29.88 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.88(1 -.17208)+ 18.0(.17208) = 27.84 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.37*√(1352.86/(29.61*27.84)) = 65.95 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.17208)65.95*2.182((528*29.61)/ (1352.86*29.92)) = 165660.25 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 165660.251/35.315 = 4690.932 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = .11*(20.9-15)/(20.9-0%)) = .031 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(.11*(1.164*10^-3)*4690.932*(Run Time/60))/2100 = 0 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = 0*1/453.6*2100 = .001 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .001*4.38 = .004 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
.11 = .091*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.79%
21.23%
10.50%
10.47%
10.58%
10.58%
10.47%10.50%
10.79%
21.23%
10.58%
20.92%
10.58%
20.92%
10.58%20.92%
0.00%
10.58%
20.92%
0.21%
0.31%
0.99%
1.48%
10.58%
Span
Zero Offset 0.00%
20.92
0.00%
10.79%1.39%1.52%0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
0.00%
9
GAS
1067.0 1069.0 1067.0
1035.0 1037.0 1035.0
-8.4 -8.4 -8.4
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
4/2/2025
5226
2026-01
Waukesha
Model
Serial Number
9394 GSI
WAU-1641324
Technician Hunter Newton
Run Start Times 11:01 AM 12:12 PM 01:20 PM 02:46 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1200.0 1198.0 1199.3
Engine Hours 10856 10857 10858 10859
Intake Manifold Pressure (psi)59.0 59.0 58.0 58.7
Intake Manifold Temp °F 124.0 125.0 124.0 124.3
Engine Load (BHP)2100.0 2100.0 2125.0 2108.3
Ambient Temp °F 46.0 39.0 41.0 42.0
Humidity %54.0 40.0 36.0 43.3
Dew Point °F 38.0 17.0 16.0 23.7
Waukesha
N/A
N/A
Yes
DCL DCL DCL DCL
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
Discharge Pressure (psi)
Suction Pressure (psi)
1065.0
1033.0
-8.4Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
N/A N/A N/A N/A
N/A N/A N/A N/A
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.81
Average:NOx 0.80
Average:VOC 0.63
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 99.67
Tolerance 2.00%
Difference between measured and expected 0.10%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.95
Average:NOx 0.95
Average:VOC 0.75
Average:Oxygen 0.00
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 99.57
Value:CTS Compound Concentration Avg 99.36
Tolerance 5.00%
Difference between measured and expected 0.21%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 247.83
Value:Spike Expected 249.80
System (Equilibration) Response Time Target (Spike)
45 secondsSystem Zero Response Time
45 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC507781 9/17/2027 102.10 10.58%
EB0115896 12/18/2027 99.57
CC440196 7/13/2032 20.92%
Cylinder # CC333629 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 249.80 501.50 254.60 9.99
Analyzer System Response 247.83 506.94 253.06 9.81
Percent Difference 0.79%1.08%0.60%1.82%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.668 5.005
Spike Direct
Propane 248.134
Mechanical
Response Time
SF6 9.830
CO 504.860
NO 252.157
Ethylene 99.356 33 seconds
Analyzer
Response
Propane 247.828
SF6 9.806
CO 506.939
NO 253.063
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 246.034
CO 501.557
NO 250.634
30 seconds
31 seconds
7.35%
8.12%
7.52%
107.02%
104.09%
104.40%
9.769
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
10
21
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
166246.15
H2O%d @ Sampling Point:17.16
CO2%d @ Sampling Point:11.65
Pressure @ Sampling Point (Pg "H2O):0.39
Temperature @ Sampling Point (Deg F):893.29
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 99.57 99.67 5.005 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.668 5.005
Spike Direct
Propane 248.134
Mechanical
Response Time
SF6 9.830
CO 504.860
NO 252.157
Ethylene 99.356 33 seconds
Analyzer
Response
Propane 247.828
SF6 9.806
CO 506.939
NO 253.063
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 246.034
CO 501.557
NO 250.634
30 seconds
31 seconds
7.35%
8.12%
7.52%
107.02%
104.09%
104.40%
9.769
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
249.800
9.988
501.500
254.600
248.134
9.830
504.860
252.157
0.67%
1.58%
0.67%
0.96%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
19.649
0.723
Dilution Factor
7.355%
Expected
18.360
% Recovery
107.020%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.798
Dilution Factor
8.118%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.739
Dilution Factor
7.518%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 19.612 18.785 104.400%
0.000320
0.000279
0.000510
0.000 21.113 20.284 104.090%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass2.37%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:40.0786404 Pass
Line Position Difference:Resolution Difference to Reference 2.37%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
99.57
99.83
0.26%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 2026-01; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
4/2/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
4/2/2025
Hunter Newton
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:2026-01
Make:Waukesha
Location:9394 GSIModel:
WAU-1641324Serial Number:
RAW Result Data
Stability
4/2/2025 05:54 1.2760.000-0.008 0.013 0.4042.745 0.000 0.000 0.0000.0591.387 4.679 1.8240.000 0.000 829.05.080.210 0.066 1.28 0.00 181.0
Pre Test Baseline Direct
4/2/2025 06:00 0.1630.0000.006 0.000 0.1870.000 0.000 0.887 0.0000.1230.000 0.000 0.0000.000 0.000 829.00.570.857 0.000 0.16 0.00 181.0
4/2/2025 06:00 1.1540.000-0.001 0.000 0.0810.000 0.000 0.808 0.0000.0070.000 0.000 0.0000.000 0.000 829.00.600.898 0.000 1.15 0.00 181.0
4/2/2025 06:01 1.0970.0000.001 0.000 0.0990.000 0.000 0.905 0.0000.0000.000 0.000 0.0000.000 0.000 829.00.721.083 0.000 1.10 0.00 181.0
CTS Direct
4/2/2025 06:03 0.0000.0000.012 0.000 0.0870.000 0.000 0.309 0.0000.0000.000 99.539 0.0000.000 0.000 828.066.930.859 0.000 0.00 0.00 182.0
4/2/2025 06:04 0.0000.0000.010 0.000 0.1680.000 0.000 0.499 0.0000.0000.000 99.570 0.0000.000 0.000 828.066.980.902 0.000 0.00 0.00 181.0
4/2/2025 06:05 0.0000.0000.011 0.000 0.1340.000 0.000 0.428 0.0000.0000.000 99.895 0.0000.011 0.000 828.067.210.912 0.000 0.00 0.00 181.0
High O2 Direct
4/2/2025 06:09 1.3430.0000.002 0.000 0.1930.000 0.000 1.313 0.0000.0300.000 0.000 0.0000.000 0.000 827.00.861.284 0.000 1.34 21.18 181.0
4/2/2025 06:10 0.9550.0000.003 0.000 0.2870.000 0.000 1.334 0.0000.0420.000 0.000 0.0000.000 0.000 827.00.811.219 0.000 0.96 21.25 180.0
4/2/2025 06:10 1.1080.000-0.000 0.000 0.3300.000 0.000 1.274 0.0000.0510.000 0.000 0.0000.023 0.000 826.00.821.227 0.000 1.11 21.26 180.0
NO2/Mid O2 Direct
4/2/2025 06:14 102.5390.000-0.004 0.000 0.8600.000 0.378 1.125 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.721.082 0.000 102.54 10.82 180.0
4/2/2025 06:14 102.9190.000-0.006 0.000 0.9110.000 0.377 1.024 0.0000.0000.000 0.000 0.0000.000 0.000 824.00.671.009 0.000 102.92 10.78 180.0
4/2/2025 06:15 104.4950.000-0.001 0.000 0.8290.000 0.304 0.997 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.721.085 0.000 104.49 10.76 180.0
Spike Direct
4/2/2025 06:18 0.000252.1670.007 4.396 5.528505.945 2.897 1.459 4.9620.4250.195 0.000 251.3140.133 0.209 823.0254.123.585 9.887 252.17 0.00 180.0
4/2/2025 06:18 0.000252.0420.002 4.540 5.694504.435 2.978 2.449 1.0370.3030.000 0.164 246.4160.479 1.514 823.0250.791.859 9.808 252.04 0.00 180.0
4/2/2025 06:19 0.000252.2620.002 4.552 5.978504.200 2.977 2.393 2.2380.2720.241 0.268 246.6730.380 1.279 823.0250.691.925 9.796 252.26 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
4/2/2025 06:22 0.9330.0000.033 0.000 0.3680.000 0.000 1.644 0.0000.0030.000 0.000 0.0000.000 0.000 823.00.721.074 0.000 0.93 0.00 180.0
4/2/2025 06:22 1.1570.0000.014 0.000 0.4800.000 0.000 1.406 0.0000.0080.000 0.000 0.0000.000 0.000 823.00.741.112 0.000 1.16 0.00 180.0
4/2/2025 06:23 0.7690.0000.008 0.000 0.5270.000 0.000 1.363 0.0000.0020.000 0.000 0.0000.000 0.000 823.00.801.195 0.000 0.77 0.00 181.0
CTS System with Response Time
4/2/2025 06:24 0.0000.0000.016 0.000 0.0880.000 0.000 0.530 0.0000.0060.000 99.267 0.0000.000 0.000 823.066.780.896 0.000 0.00 0.00 180.0
4/2/2025 06:25 0.0000.0000.016 0.000 0.0000.000 0.000 0.627 0.0000.0020.000 99.705 0.0000.000 0.000 823.067.070.896 0.000 0.00 0.00 180.0
4/2/2025 06:25 0.0000.0000.015 0.000 0.1330.000 0.000 0.302 0.0000.0120.000 99.096 0.0000.000 0.000 823.066.730.987 0.000 0.00 0.00 180.0
NO2/Mid O2 System with Response Time
4/2/2025 06:27 102.7540.000-0.000 0.000 0.0000.000 0.319 1.221 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.781.177 0.000 102.75 10.47 180.0
4/2/2025 06:28 101.4050.000-0.000 0.000 0.7330.000 0.400 1.275 0.0000.0010.000 0.000 0.0000.000 0.000 823.00.791.188 0.000 101.41 10.50 180.0
4/2/2025 06:28 101.5970.000-0.000 0.000 0.8090.000 0.328 1.316 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.711.063 0.000 101.60 10.52 180.0
Spike System with Response Time
4/2/2025 06:30 0.000252.8000.007 4.519 4.813506.870 2.791 2.114 1.4030.0860.191 0.369 247.5560.195 1.243 823.0251.611.985 9.796 252.80 0.00 180.0
4/2/2025 06:30 0.000253.0060.005 4.527 5.168506.971 2.804 2.134 1.6050.0850.256 0.386 248.0030.193 1.196 823.0252.062.107 9.814 253.01 0.00 180.0
4/2/2025 06:30 0.000253.1490.005 4.523 5.070506.901 2.816 2.268 1.4300.0920.315 0.417 247.8850.248 1.182 823.0251.831.949 9.804 253.15 0.00 180.0
4/2/2025 06:31 0.000253.2980.003 4.537 4.858507.013 2.808 2.249 1.5720.0910.101 0.402 247.8670.055 1.235 823.0251.871.890 9.808 253.30 0.00 180.0
Baseline System with Response Time
4/2/2025 06:33 0.0000.0000.001 0.000 0.7210.000 0.000 1.155 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.590.882 0.000 0.00 0.00 180.0
4/2/2025 06:34 0.5850.0000.002 0.000 0.5210.000 0.000 1.308 0.0000.0030.000 0.000 0.0000.000 0.000 823.00.660.992 0.000 0.59 0.00 180.0
4/2/2025 06:34 0.6060.0000.002 0.000 0.6270.000 0.000 1.157 0.0000.0000.000 0.000 0.0000.000 0.000 823.00.701.055 0.000 0.61 0.00 180.0
Run 1 - A 30minute/60min
4/2/2025 11:02 0.00018.25011.922 7.737 41.5670.000 3.746 3.051 0.6020.8610.000 0.000 0.0000.601 0.443 825.01.530.972 0.000 18.25 0.00 180.0
4/2/2025 11:03 1.2502.40816.955 9.704 58.0530.000 4.015 2.731 0.8270.3880.000 0.000 0.0000.701 0.187 825.01.231.283 0.000 3.66 0.00 180.0
4/2/2025 11:04 1.4443.06417.536 9.635 44.7340.000 3.811 2.686 0.4450.3910.000 0.000 0.0000.608 0.200 825.01.211.223 0.000 4.51 0.00 180.0
4/2/2025 11:05 1.1892.26117.623 9.636 61.0020.000 4.328 2.861 1.0370.4050.000 0.000 0.0000.601 0.150 825.01.131.251 0.000 3.45 0.00 180.0
4/2/2025 11:06 1.1702.92817.484 9.669 56.5530.000 5.073 2.995 0.9120.3650.000 0.000 0.0000.644 0.173 825.01.151.209 0.000 4.10 0.00 180.0
4/2/2025 11:07 1.4652.76517.301 9.707 47.7700.000 3.466 2.748 0.4870.2690.000 0.000 0.0000.572 0.184 825.01.221.273 0.000 4.23 0.00 180.0
4/2/2025 11:08 1.3722.96217.275 9.737 58.5590.000 4.848 2.787 0.8780.3570.000 0.000 0.0000.692 0.186 825.01.181.214 0.000 4.33 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 11:09 1.4273.40017.286 9.774 45.9870.000 4.549 2.778 0.4500.4180.000 0.000 0.0000.632 0.198 825.01.221.236 0.000 4.83 0.00 180.0
4/2/2025 11:10 1.2942.78417.289 9.769 60.1840.000 4.818 2.844 0.8940.4340.000 0.000 0.0000.672 0.176 825.01.201.272 0.000 4.08 0.00 180.0
4/2/2025 11:11 1.4012.66017.267 9.751 53.5600.000 4.262 2.696 0.7130.3490.000 0.000 0.0000.660 0.196 825.01.271.321 0.000 4.06 0.00 180.0
4/2/2025 11:12 1.3432.34317.277 9.755 54.7700.000 4.096 2.665 0.7760.3720.000 0.000 0.0000.688 0.184 825.01.231.294 0.000 3.69 0.00 180.0
4/2/2025 11:13 1.4803.60917.291 9.760 51.9010.000 4.731 2.712 0.7680.3570.000 0.000 0.0000.644 0.196 825.01.221.239 0.000 5.09 0.00 180.0
4/2/2025 11:14 1.4223.74217.265 9.750 58.4320.000 5.934 2.762 0.9590.4380.000 0.000 0.0000.662 0.200 825.01.231.237 0.000 5.16 0.00 179.0
4/2/2025 11:15 1.1318.68417.264 9.799 69.1230.000 8.128 3.993 1.7970.4590.000 0.000 0.0000.879 0.176 825.01.211.295 0.000 9.81 0.00 180.0
4/2/2025 11:16 1.2136.37917.247 9.792 52.1360.000 4.695 2.922 0.7180.5950.000 0.000 0.0000.694 0.214 825.01.251.226 0.000 7.59 0.00 180.0
4/2/2025 11:18 0.8556.77817.243 9.797 40.7010.000 4.245 2.667 0.4400.5580.000 0.000 0.0000.616 0.213 825.01.191.149 0.000 7.63 0.00 180.0
4/2/2025 11:19 1.2123.09017.254 9.789 65.0000.000 5.286 2.682 1.3580.4080.000 0.000 0.0000.680 0.155 827.01.111.197 0.000 4.30 0.00 181.0
4/2/2025 11:20 1.3083.42817.163 9.709 57.1090.000 5.073 2.590 0.9470.4120.000 0.000 0.0000.644 0.190 828.01.231.281 0.000 4.74 0.00 180.0
4/2/2025 11:21 1.2383.61617.177 9.733 52.6880.000 4.595 2.456 0.8340.3520.000 0.000 0.0000.636 0.163 825.01.171.261 0.000 4.85 0.00 179.0
4/2/2025 11:22 1.2736.09817.240 9.809 55.5090.000 4.703 2.388 0.8220.4900.000 0.000 0.0000.703 0.177 824.01.171.221 0.000 7.37 0.00 180.0
4/2/2025 11:23 0.6524.85417.221 9.814 53.3280.000 5.567 2.448 0.8610.5440.000 0.000 0.0000.726 0.150 825.01.061.145 0.000 5.51 0.00 180.0
4/2/2025 11:24 0.8394.45217.236 9.822 52.4690.000 5.001 2.399 0.7390.5090.000 0.000 0.0000.703 0.164 824.01.071.116 0.000 5.29 0.00 180.0
4/2/2025 11:25 0.7016.77117.265 9.809 52.7090.000 4.377 2.394 0.9280.4430.000 0.000 0.0000.690 0.141 824.01.061.173 0.000 7.47 0.00 180.0
4/2/2025 11:26 0.9137.24617.297 9.792 39.7920.000 4.010 2.431 0.5470.3630.000 0.000 0.0000.684 0.147 824.01.071.167 0.000 8.16 0.00 180.0
4/2/2025 11:27 0.8103.65117.282 9.763 47.2790.000 4.079 2.360 0.7100.3020.000 0.000 0.0000.704 0.132 824.01.061.194 0.000 4.46 0.00 180.0
4/2/2025 11:28 0.8306.33717.286 9.787 57.4270.000 5.152 2.344 1.2120.3690.000 0.000 0.0000.693 0.103 824.00.981.161 0.000 7.17 0.00 180.0
4/2/2025 11:29 0.7766.82417.234 9.776 56.7780.000 5.184 2.348 1.1200.3370.000 0.000 0.0000.718 0.072 824.00.871.092 0.000 7.60 0.00 180.0
4/2/2025 11:30 0.8456.73917.252 9.761 54.3140.000 4.753 2.283 1.0640.3270.000 0.000 0.0000.785 0.076 824.00.861.060 0.000 7.58 0.00 180.0
4/2/2025 11:31 0.7307.41017.249 9.767 50.7120.000 5.367 2.272 0.9460.3450.000 0.000 0.0000.667 0.082 824.00.881.075 0.000 8.14 0.00 180.0
4/2/2025 11:32 0.7433.40017.260 9.770 56.4070.000 4.112 2.195 1.1430.3200.000 0.000 0.0000.711 0.054 824.00.781.008 0.000 4.14 0.00 180.0
1.0784.96417.098 9.689 53.5520.000 4.733 2.650 0.8640.4180.000 0.000 0.0000.677 0.169 824.831.1351.195 0.000 6.042 0.000 180.0Avg.
Spike 1
4/2/2025 11:34 0.00029.03915.682 9.363 68.82450.080 6.776 1.817 3.5330.2800.000 0.000 19.6490.616 0.699 824.021.861.214 0.723 29.04 0.00 180.0
Run 1 - B 30minute/60min
4/2/2025 11:37 0.64318.80616.977 9.791 43.2171.958 8.049 0.802 2.2800.1600.000 0.000 1.7760.608 0.590 824.03.540.874 0.022 19.45 0.00 180.0
4/2/2025 11:38 0.8287.71417.317 9.735 22.1600.000 2.048 2.011 0.5180.1780.000 0.000 0.0000.499 0.055 824.00.801.031 0.000 8.54 0.00 180.0
4/2/2025 11:39 0.7864.29617.299 9.738 51.2330.000 4.567 2.096 1.1570.1180.000 0.000 0.0000.641 0.000 824.00.681.022 0.000 5.08 0.00 180.0
4/2/2025 11:40 0.9787.59517.318 9.729 48.2390.000 4.840 2.060 1.0710.1350.000 0.000 0.0000.622 0.000 824.00.630.945 0.000 8.57 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 11:41 0.8614.10417.348 9.731 49.0400.000 3.479 1.918 1.1280.1100.045 0.000 0.0000.657 0.000 824.00.640.961 0.000 4.97 0.00 180.0
4/2/2025 11:42 0.6724.52517.362 9.748 59.5690.000 6.135 2.430 1.5080.1140.244 0.000 0.0000.854 0.000 824.00.610.918 0.000 5.20 0.00 181.0
4/2/2025 11:43 0.7833.92017.338 9.721 52.9850.000 4.230 2.088 1.3990.1080.518 0.000 0.0000.613 0.000 824.00.610.909 0.000 4.70 0.00 180.0
4/2/2025 11:44 0.8424.42217.310 9.693 50.7800.000 5.129 2.122 1.2620.0800.315 0.000 0.0000.671 0.000 824.00.590.879 0.000 5.26 0.00 179.0
4/2/2025 11:45 0.7354.22117.329 9.727 54.2600.000 4.680 2.043 1.3840.0740.381 0.000 0.0000.657 0.000 825.00.600.897 0.000 4.96 0.00 180.0
4/2/2025 11:46 0.8477.53917.334 9.730 47.4390.000 4.246 2.003 1.2040.0790.150 0.000 0.0000.680 0.000 825.00.580.874 0.000 8.39 0.00 180.0
4/2/2025 11:47 0.5854.57317.361 9.727 36.3360.000 3.068 1.815 0.7870.0500.044 0.000 0.0000.531 0.000 824.00.620.925 0.000 5.16 0.00 180.0
4/2/2025 11:48 1.00310.06617.369 9.729 34.7450.000 4.886 2.135 1.0220.1470.113 0.000 0.0000.608 0.000 824.00.570.860 0.000 11.07 0.00 180.0
4/2/2025 11:49 0.8919.44717.329 9.689 45.7570.000 5.708 2.364 1.2790.0580.423 0.000 0.0000.619 0.000 824.00.570.857 0.000 10.34 0.00 180.0
4/2/2025 11:50 1.1138.87217.315 9.683 25.4230.000 3.543 1.956 0.7930.0700.000 0.000 0.0000.582 0.000 824.00.600.895 0.000 9.99 0.00 180.0
4/2/2025 11:51 0.4026.60717.354 9.679 60.6913.497 5.411 4.205 2.2740.0680.916 0.000 0.0000.636 0.000 824.00.560.845 0.000 7.01 0.00 180.0
4/2/2025 11:52 0.8619.73517.324 9.667 38.5710.000 5.388 2.779 1.0620.0430.623 0.000 0.0000.622 0.000 824.00.570.860 0.000 10.60 0.00 179.0
4/2/2025 11:53 0.7114.43617.325 9.696 54.1060.000 4.937 2.267 1.3980.0590.674 0.000 0.0000.656 0.000 824.00.550.828 0.000 5.15 0.00 180.0
4/2/2025 11:54 0.6444.73617.330 9.694 59.2640.000 4.807 2.208 1.7120.0830.865 0.000 0.0000.671 0.000 824.00.580.876 0.000 5.38 0.00 180.0
4/2/2025 11:55 1.0058.96117.353 9.705 46.4580.000 6.181 2.181 1.3090.0540.482 0.000 0.0000.702 0.000 824.00.570.848 0.000 9.97 0.00 180.0
4/2/2025 11:56 0.8094.58517.390 9.743 44.0210.000 3.558 1.932 1.2100.1190.259 0.000 0.0000.582 0.000 824.00.530.795 0.000 5.39 0.00 180.0
4/2/2025 11:57 0.8178.21917.318 9.723 65.4700.000 7.457 2.426 2.0090.1110.704 0.000 0.0000.930 0.000 824.00.600.896 0.000 9.04 0.00 180.0
4/2/2025 11:58 0.8167.86517.344 9.704 49.7050.000 4.745 2.168 1.2630.0750.358 0.000 0.0000.776 0.000 824.00.520.787 0.000 8.68 0.00 180.0
4/2/2025 11:59 0.8458.62017.333 9.701 40.4540.000 4.368 2.095 1.0740.0770.463 0.000 0.0000.643 0.000 824.00.570.855 0.000 9.47 0.00 180.0
4/2/2025 12:02 0.6354.63617.299 9.691 53.0700.000 3.979 2.105 1.4860.0760.659 0.000 0.0000.610 0.000 824.00.630.941 0.000 5.27 0.00 179.0
4/2/2025 12:03 0.8368.59917.323 9.725 50.0380.000 5.204 2.132 1.3890.0820.237 0.000 0.0000.711 0.000 824.00.530.788 0.000 9.43 0.00 180.0
4/2/2025 12:04 0.9948.02117.318 9.744 48.1760.000 3.888 1.882 1.2530.1140.000 0.000 0.0000.661 0.000 824.00.530.792 0.000 9.01 0.00 180.0
4/2/2025 12:05 0.7637.62517.294 9.738 63.7500.000 4.539 2.031 1.8620.1460.562 0.000 0.0000.751 0.000 824.00.540.806 0.000 8.39 0.00 180.0
4/2/2025 12:06 0.6348.62117.286 9.735 51.2050.000 4.818 2.036 1.3250.1840.232 0.000 0.0000.606 0.000 824.00.560.833 0.000 9.26 0.00 180.0
4/2/2025 12:07 0.8608.69817.308 9.735 40.5770.000 3.960 1.797 1.0050.1540.000 0.000 0.0000.586 0.000 824.00.590.883 0.000 9.56 0.00 180.0
4/2/2025 12:08 0.7254.48117.332 9.734 54.8070.000 4.179 1.932 1.5110.0910.585 0.000 0.0000.631 0.000 824.00.620.936 0.000 5.21 0.00 180.0
0.7977.15217.318 9.720 48.0520.182 4.734 2.134 1.3310.1010.328 0.000 0.0590.654 0.022 824.070.6900.881 0.001 7.950 0.000 179.9Avg.
0.9376.05817.208 9.704 50.8020.091 4.734 2.392 1.0980.2590.164 0.000 0.0300.665 0.095 824.450.9121.038 0.000 6.996 0.000 180.0Run 1 Avg:
Baseline 1
4/2/2025 12:10 0.1800.0000.040 0.000 0.4550.000 0.000 1.562 0.0000.0060.000 0.000 0.0000.000 0.000 824.00.350.521 0.000 0.18 0.00 179.0
Run 2 - A 30minute/60min
4/2/2025 12:12 0.16317.89913.042 7.771 47.0880.000 3.807 1.730 1.3340.4170.000 0.000 0.0000.640 0.000 824.00.460.687 0.000 18.06 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 12:13 1.1064.80417.243 9.687 46.2950.000 3.616 1.768 1.2170.1070.165 0.000 0.0000.637 0.000 824.00.620.923 0.000 5.91 0.00 180.0
4/2/2025 12:14 0.9815.18117.278 9.696 42.3100.000 3.839 1.706 1.1650.0740.399 0.000 0.0000.641 0.000 824.00.610.922 0.000 6.16 0.00 180.0
4/2/2025 12:15 1.0644.76017.333 9.696 39.7130.000 3.602 1.756 0.9980.0910.477 0.000 0.0000.584 0.000 824.00.540.812 0.000 5.82 0.00 180.0
4/2/2025 12:16 0.8233.93317.342 9.684 50.7840.000 3.841 1.810 1.2330.1100.775 0.000 0.0000.655 0.000 824.00.540.803 0.000 4.76 0.00 180.0
4/2/2025 12:17 17.1650.00014.484 5.656 87.2780.000 4.051 0.000 0.0000.0000.000 41.008 0.0000.000 0.000 824.027.340.000 0.000 17.17 0.00 180.0
4/2/2025 12:18 0.8254.73517.288 9.693 54.7330.000 4.110 1.870 1.5980.0900.821 0.000 0.0000.647 0.000 824.00.671.012 0.000 5.56 0.00 179.0
4/2/2025 12:19 0.8718.16117.310 9.741 58.2380.000 4.952 1.907 1.6060.1330.362 0.000 0.0000.660 0.000 824.00.550.831 0.000 9.03 0.00 180.0
4/2/2025 12:20 0.8898.35717.359 9.781 44.7340.000 4.495 1.849 1.1400.1080.000 0.000 0.0000.621 0.000 824.00.510.768 0.000 9.25 0.00 181.0
4/2/2025 12:21 0.8974.41617.384 9.736 59.1340.000 3.748 1.764 1.8020.0820.930 0.000 0.0000.666 0.000 824.00.580.866 0.000 5.31 0.00 181.0
4/2/2025 12:22 0.7974.49617.396 9.694 52.4570.000 4.254 1.846 1.5780.0751.209 0.000 0.0000.643 0.000 824.00.650.968 0.000 5.29 0.00 181.0
4/2/2025 12:23 0.5294.81017.346 9.632 37.1190.000 3.927 1.727 0.9960.0501.027 0.000 0.0000.498 0.000 825.00.691.039 0.000 5.34 0.00 180.0
4/2/2025 12:24 0.7276.64417.313 9.620 36.4630.000 2.477 1.679 0.9370.0630.999 0.000 0.0000.521 0.000 824.00.671.011 0.000 7.37 0.00 179.0
4/2/2025 12:25 0.7813.82417.326 9.661 60.7490.000 5.648 1.978 1.6870.0531.151 0.000 0.0000.923 0.000 824.00.660.984 0.000 4.61 0.00 180.0
4/2/2025 12:26 1.1434.46017.307 9.658 44.7450.000 4.376 1.885 1.0910.0760.658 0.000 0.0000.651 0.000 824.00.620.935 0.000 5.60 0.00 180.0
4/2/2025 12:27 0.6833.58117.362 9.689 61.0850.000 4.814 1.935 1.6850.0510.785 0.000 0.0000.659 0.000 822.00.660.995 0.000 4.26 0.00 180.0
4/2/2025 12:28 0.5473.58017.392 9.720 60.9680.000 4.692 1.894 1.6720.0800.779 0.000 0.0000.650 0.000 821.00.681.022 0.000 4.13 0.00 180.0
4/2/2025 12:29 0.7213.22917.328 9.678 50.3380.000 3.532 1.685 1.2220.0740.340 0.000 0.0000.610 0.000 824.00.691.029 0.000 3.95 0.00 180.0
4/2/2025 12:30 0.6953.98217.280 9.690 61.8440.000 4.602 1.884 1.7440.1450.682 0.000 0.0000.721 0.000 824.00.660.990 0.000 4.68 0.00 180.0
4/2/2025 12:31 0.9184.14817.284 9.687 51.6620.000 4.967 1.934 1.1820.1140.377 0.000 0.0000.666 0.000 824.00.660.982 0.000 5.07 0.00 180.0
4/2/2025 12:33 1.1904.73817.307 9.676 28.6930.000 2.903 1.752 0.5590.1050.000 0.000 0.0000.577 0.001 824.00.630.946 0.000 5.93 0.00 180.0
4/2/2025 12:34 0.8803.85517.310 9.671 45.1910.000 3.800 1.727 0.8940.0900.052 0.000 0.0000.761 0.000 824.00.640.957 0.000 4.73 0.00 180.0
4/2/2025 12:35 0.8814.49017.342 9.672 43.0780.000 3.427 1.742 0.9680.0770.099 0.000 0.0000.631 0.000 824.00.681.016 0.000 5.37 0.00 180.0
4/2/2025 12:36 0.6439.79017.320 9.675 59.9870.000 7.541 2.591 2.1570.1150.305 0.000 0.0000.751 0.006 824.00.610.893 0.000 10.43 0.00 180.0
4/2/2025 12:37 1.0314.37917.302 9.677 40.0390.000 3.736 1.854 0.7980.0960.000 0.000 0.0000.682 0.019 825.00.721.020 0.000 5.41 0.00 180.0
4/2/2025 12:38 0.7714.83517.323 9.671 39.7650.000 4.493 1.840 0.7860.1600.000 0.000 0.0000.679 0.014 825.00.680.970 0.000 5.61 0.00 180.0
4/2/2025 12:39 0.6373.64917.325 9.675 50.5360.000 4.158 1.774 1.1350.1010.091 0.000 0.0000.667 0.002 824.00.681.019 0.000 4.29 0.00 180.0
4/2/2025 12:40 0.9153.59217.331 9.696 54.7720.000 4.221 1.752 1.3010.1270.054 0.000 0.0000.718 0.000 824.00.671.011 0.000 4.51 0.00 180.0
4/2/2025 12:41 0.8713.83217.336 9.733 52.3160.000 4.682 1.792 1.1900.1540.000 0.000 0.0000.643 0.026 824.00.741.039 0.000 4.70 0.00 180.0
4/2/2025 12:42 0.7994.12517.302 9.728 54.3720.000 4.669 1.777 1.3090.2070.000 0.000 0.0000.649 0.024 824.00.741.033 0.000 4.92 0.00 180.0
1.3655.07617.087 9.491 50.5500.000 4.233 1.774 1.2330.1080.418 1.367 0.0000.635 0.003 823.931.5280.916 0.000 6.441 0.000 180.0Avg.
Spike 2
4/2/2025 12:44 0.00030.50515.610 9.283 51.32947.620 5.760 0.357 2.3770.1660.379 0.000 21.1130.523 0.700 824.023.501.480 0.798 30.50 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
4/2/2025 12:46 0.5443.66217.301 9.683 61.7020.000 3.434 1.596 1.7570.1340.025 0.000 0.0000.636 0.033 824.00.751.021 0.000 4.21 0.00 180.0
4/2/2025 12:47 0.5624.86217.311 9.699 72.9840.000 6.944 1.850 2.3070.1840.207 0.000 0.0000.754 0.027 824.00.720.999 0.000 5.42 0.00 180.0
4/2/2025 12:48 1.1008.90117.278 9.700 22.0270.000 3.667 1.732 0.5610.1790.000 0.000 0.0000.621 0.065 824.00.790.984 0.000 10.00 0.00 180.0
4/2/2025 12:49 1.22112.42717.300 9.703 22.2840.000 5.095 2.099 0.4900.1870.000 0.000 0.0000.651 0.068 824.00.800.993 0.000 13.65 0.00 180.0
4/2/2025 12:50 0.9087.94917.341 9.690 36.1780.000 3.993 1.715 0.7180.1150.000 0.000 0.0000.673 0.052 824.00.781.006 0.000 8.86 0.00 180.0
4/2/2025 12:51 0.7887.69217.370 9.688 43.4740.000 1.679 1.776 1.1320.1450.000 0.000 0.0000.598 0.052 824.00.831.083 0.000 8.48 0.00 180.0
4/2/2025 12:52 0.67714.05517.401 9.699 48.4845.267 8.953 4.213 2.0330.1020.000 0.000 0.0000.919 0.080 824.00.790.951 0.000 14.73 0.00 180.0
4/2/2025 12:53 0.68714.66817.345 9.688 48.1701.599 7.206 4.319 1.4380.0950.000 0.000 0.0000.680 0.042 824.00.771.030 0.000 15.35 0.00 179.0
4/2/2025 12:54 0.46122.82317.341 9.693 74.39610.327 10.633 6.486 2.7440.1270.231 0.000 0.0000.965 0.056 824.00.811.042 0.000 23.28 0.00 180.0
4/2/2025 12:55 1.1907.50017.331 9.704 27.4880.000 3.556 2.731 0.6130.1600.000 0.000 0.0000.628 0.072 824.00.810.991 0.000 8.69 0.00 180.0
4/2/2025 12:56 0.6754.53717.341 9.717 48.8330.000 4.680 2.382 1.1580.1480.000 0.000 0.0000.665 0.053 824.00.801.039 0.000 5.21 0.00 180.0
4/2/2025 12:57 0.7419.30617.349 9.716 47.1810.000 5.884 2.269 1.1730.1410.000 0.000 0.0000.643 0.059 824.00.831.072 0.000 10.05 0.00 180.0
4/2/2025 12:58 0.6035.56717.344 9.698 65.4571.400 5.771 4.323 2.1400.1540.115 0.000 0.0000.680 0.057 824.00.851.096 0.000 6.17 0.00 180.0
4/2/2025 12:59 0.8124.96217.286 9.681 54.9760.000 5.814 3.059 1.2050.2060.000 0.000 0.0000.659 0.063 824.00.790.990 0.000 5.77 0.00 180.0
4/2/2025 13:00 0.9417.93517.292 9.702 38.6850.000 4.097 2.323 0.6140.1380.000 0.000 0.0000.661 0.075 824.00.861.063 0.000 8.88 0.00 180.0
4/2/2025 13:01 0.6953.95817.297 9.703 51.4680.000 4.759 2.113 1.1010.1660.000 0.000 0.0000.581 0.073 824.00.871.087 0.000 4.65 0.00 180.0
4/2/2025 13:02 0.3905.76917.281 9.703 75.3550.000 6.303 3.308 2.3530.1360.306 0.000 0.0000.702 0.055 824.00.831.084 0.000 6.16 0.00 180.0
4/2/2025 13:03 0.57818.06517.290 9.713 61.5750.000 10.187 3.779 2.5920.1630.041 0.000 0.0000.909 0.092 824.00.830.964 0.000 18.64 0.00 180.0
4/2/2025 13:04 0.85710.20717.318 9.738 36.2120.000 6.356 3.063 0.5820.1940.000 0.000 0.0000.862 0.089 824.00.830.975 0.000 11.06 0.00 180.0
4/2/2025 13:05 0.7028.69017.218 9.705 47.5820.000 4.331 2.563 1.0330.2110.000 0.000 0.0000.579 0.069 824.00.871.101 0.000 9.39 0.00 180.0
4/2/2025 13:06 1.12614.52317.279 9.697 50.0440.000 8.236 2.276 1.4110.2030.000 0.000 0.0000.722 0.082 824.00.800.953 0.000 15.65 0.00 180.0
4/2/2025 13:08 0.82610.81317.269 9.709 22.6890.000 1.774 1.938 0.4720.1690.000 0.000 0.0000.531 0.092 824.00.981.194 0.000 11.64 0.00 180.0
4/2/2025 13:09 0.71810.26117.238 9.713 50.9960.000 6.309 3.280 1.2150.1670.000 0.000 0.0000.649 0.063 824.00.851.091 0.000 10.98 0.00 180.0
4/2/2025 13:10 0.60610.16917.214 9.711 65.42224.630 8.613 9.240 2.2170.1410.000 0.000 0.0000.966 0.085 824.00.841.011 0.000 10.77 0.00 180.0
4/2/2025 13:11 1.46430.25817.242 9.720 46.4550.000 13.367 5.455 1.3010.1670.000 0.000 0.0000.920 0.088 824.00.730.834 0.000 31.72 0.00 180.0
4/2/2025 13:12 0.98917.80217.256 9.721 34.1550.000 7.024 3.631 0.7030.1510.000 0.000 0.0000.832 0.079 824.00.831.001 0.000 18.79 0.00 180.0
4/2/2025 13:13 0.74315.75617.230 9.712 46.8611.386 8.142 4.396 1.1580.2160.000 0.000 0.0000.843 0.091 824.00.911.086 0.000 16.50 0.00 180.0
4/2/2025 13:14 0.73410.30817.200 9.715 41.7180.000 5.253 3.619 0.7870.1980.000 0.000 0.0000.570 0.078 824.00.891.103 0.000 11.04 0.00 180.0
4/2/2025 13:15 0.91813.51017.156 9.697 45.5710.000 9.178 4.983 1.0000.2230.000 0.000 0.0000.686 0.068 824.00.800.999 0.000 14.43 0.00 180.0
4/2/2025 13:16 0.9749.00117.186 9.720 37.2470.000 4.136 2.472 0.6320.1890.000 0.000 0.0000.693 0.088 824.00.820.962 0.000 9.97 0.00 180.0
0.80810.86517.287 9.705 47.5221.487 6.179 3.300 1.2880.1640.031 0.000 0.0000.716 0.068 824.000.8221.027 0.000 11.671 0.000 180.0Avg.
1.0867.97017.187 9.598 49.0360.743 5.206 2.537 1.2600.1360.224 0.683 0.0000.675 0.036 823.971.1750.971 0.000 9.056 0.000 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
4/2/2025 13:19 0.0000.0000.015 0.000 0.8130.000 0.000 1.308 0.0000.0060.000 0.000 0.0000.000 0.000 824.00.430.641 0.000 0.00 0.00 180.0
Run 3 - A 30minute/60min
4/2/2025 13:21 0.73511.50216.818 9.533 56.9290.000 7.654 2.054 1.3680.1670.000 0.000 0.0000.706 0.062 824.00.790.993 0.000 12.24 0.00 180.0
4/2/2025 13:22 0.8375.30317.148 9.657 42.9950.000 3.426 1.853 1.1600.1180.000 0.000 0.0000.605 0.064 824.00.901.155 0.000 6.14 0.00 180.0
4/2/2025 13:23 0.5665.95617.203 9.665 71.2380.000 7.348 3.435 2.1070.1070.184 0.000 0.0000.699 0.050 824.00.821.079 0.000 6.52 0.00 180.0
4/2/2025 13:24 0.8488.52717.210 9.703 45.9240.000 5.870 2.151 0.9780.1190.000 0.000 0.0000.618 0.069 824.00.821.031 0.000 9.37 0.00 180.0
4/2/2025 13:25 0.8704.30917.230 9.730 43.9980.000 2.860 1.924 0.8960.1180.000 0.000 0.0000.580 0.083 824.00.881.068 0.000 5.18 0.00 180.0
4/2/2025 13:26 0.8456.81717.255 9.740 74.8080.000 9.383 3.654 2.3110.1470.178 0.000 0.0000.779 0.054 824.00.811.053 0.000 7.66 0.00 180.0
4/2/2025 13:28 0.7835.12117.236 9.748 55.4300.000 5.982 2.405 1.2220.1730.000 0.000 0.0000.676 0.050 824.00.831.099 0.000 5.90 0.00 180.0
4/2/2025 13:29 1.10211.47817.253 9.768 18.6230.000 4.908 2.091 0.2840.2150.000 0.000 0.0000.547 0.113 824.00.951.081 0.000 12.58 0.00 180.0
4/2/2025 13:30 0.90511.45217.247 9.785 42.1540.000 5.719 2.824 0.8420.1580.000 0.000 0.0000.626 0.091 824.00.861.023 0.000 12.36 0.00 180.0
4/2/2025 13:31 0.65712.40117.224 9.773 59.3150.000 6.190 3.114 1.6420.2180.000 0.000 0.0000.662 0.069 824.00.901.148 0.000 13.06 0.00 180.0
4/2/2025 13:32 0.8976.37817.163 9.730 52.8040.000 6.391 2.375 0.9900.2200.000 0.000 0.0000.759 0.089 824.00.820.966 0.000 7.28 0.00 180.0
4/2/2025 13:33 1.6548.43017.183 9.735 43.3590.000 4.505 2.020 0.6240.2040.000 0.000 0.0000.590 0.102 824.00.891.022 0.000 10.08 0.00 180.0
4/2/2025 13:34 1.0178.85817.181 9.733 33.0420.000 4.043 1.908 0.5960.1960.000 0.000 0.0000.591 0.104 824.00.971.139 0.000 9.88 0.00 180.0
4/2/2025 13:35 0.9154.18817.221 9.748 32.0800.000 2.454 1.732 0.4350.1540.000 0.000 0.0000.586 0.109 824.00.941.080 0.000 5.10 0.00 180.0
4/2/2025 13:36 0.7433.72917.236 9.763 49.8600.000 3.891 1.791 0.8940.1240.000 0.000 0.0000.679 0.080 824.00.881.079 0.000 4.47 0.00 180.0
4/2/2025 13:38 0.0000.00011.549 4.930 73.8900.000 1.091 0.000 0.00018.69678.229 85.426 0.0000.000 0.000 824.065.0012.065 0.000 0.00 0.00 180.0
4/2/2025 13:39 0.9543.79117.179 9.732 45.4600.000 3.218 1.764 0.7710.1850.000 0.000 0.0000.699 0.091 824.00.871.038 0.000 4.74 0.00 180.0
4/2/2025 13:40 1.5323.80517.230 9.724 37.8610.000 3.525 1.700 0.4680.1980.000 0.000 0.0000.594 0.106 824.00.840.936 0.000 5.34 0.00 180.0
4/2/2025 13:41 0.9444.16417.206 9.722 32.8690.000 2.728 1.768 0.5210.1480.000 0.000 0.0000.608 0.099 824.00.931.099 0.000 5.11 0.00 180.0
4/2/2025 13:42 0.7573.21717.219 9.714 50.2980.000 3.712 1.768 0.9340.1790.000 0.000 0.0000.590 0.090 824.00.931.122 0.000 3.97 0.00 180.0
4/2/2025 13:43 0.7993.42317.216 9.704 49.3760.000 4.525 1.870 0.8410.1800.000 0.000 0.0000.572 0.101 824.00.951.128 0.000 4.22 0.00 180.0
4/2/2025 13:44 0.9492.98617.179 9.683 48.1380.000 3.300 1.746 0.9090.1720.000 0.000 0.0000.588 0.092 824.00.941.127 0.000 3.93 0.00 179.0
4/2/2025 13:45 0.5523.76517.154 9.721 66.4520.000 6.402 2.268 1.6300.1610.000 0.000 0.0000.686 0.058 824.00.911.190 0.000 4.32 0.00 180.0
4/2/2025 13:46 0.8983.45617.152 9.726 46.7970.000 3.730 1.820 0.7230.1970.000 0.000 0.0000.682 0.100 824.00.871.010 0.000 4.35 0.00 180.0
4/2/2025 13:47 0.8687.80217.154 9.750 44.5540.000 4.328 1.846 0.8970.2700.000 0.000 0.0000.584 0.104 823.01.001.185 0.000 8.67 0.00 180.0
4/2/2025 13:48 1.4343.70517.199 9.747 52.1090.000 3.823 1.648 1.0510.1500.000 0.000 0.0000.596 0.082 823.00.941.161 0.000 5.14 0.00 180.0
4/2/2025 13:49 0.7273.42617.230 9.747 53.6280.000 4.492 1.687 0.9640.1990.000 0.000 0.0000.696 0.072 824.00.810.994 0.000 4.15 0.00 180.0
4/2/2025 13:50 0.7464.51117.227 9.754 57.3420.000 5.952 1.907 1.5090.2200.000 0.000 0.0000.603 0.074 824.00.921.158 0.000 5.26 0.00 180.0
4/2/2025 13:51 1.6324.23117.254 9.762 44.8750.000 4.024 1.769 0.6030.1060.000 0.000 0.0000.712 0.079 824.00.901.115 0.000 5.86 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 13:52 0.7413.92617.331 9.783 60.1970.000 5.382 1.803 1.4730.1830.000 0.000 0.0000.701 0.075 823.00.871.075 0.000 4.67 0.00 180.0
0.8975.68917.010 9.567 49.5470.000 4.695 2.023 0.9880.7892.620 2.848 0.0000.620 0.080 823.903.0251.447 0.000 6.585 0.000 180.0Avg.
Spike 3
4/2/2025 13:54 0.00029.26315.601 9.327 36.81844.663 4.200 0.231 1.9080.1720.000 0.000 19.6120.381 0.764 823.022.071.398 0.739 29.26 0.00 180.0
Run 3 - B 30minute/60min
4/2/2025 13:56 0.3569.05017.018 9.801 58.7320.000 5.257 0.833 2.2030.2860.000 0.000 0.0000.752 0.545 824.01.600.760 0.000 9.41 0.00 180.0
4/2/2025 13:57 1.5194.15317.178 9.747 45.5540.000 4.144 1.570 0.6650.2290.000 0.000 0.0000.657 0.134 823.00.941.013 0.000 5.67 0.00 180.0
4/2/2025 13:58 0.54313.67017.172 9.730 69.9740.000 9.146 4.072 2.5240.1790.000 0.000 0.0000.943 0.088 823.00.851.016 0.000 14.21 0.00 180.0
4/2/2025 13:59 0.7568.13517.155 9.729 23.5440.000 3.108 2.081 0.3660.2110.000 0.000 0.0000.537 0.126 823.01.021.147 0.000 8.89 0.00 180.0
4/2/2025 14:00 0.6754.50517.170 9.721 48.4000.000 4.807 1.924 1.0150.1990.000 0.000 0.0000.596 0.068 823.00.931.188 0.000 5.18 0.00 180.0
4/2/2025 14:01 0.9713.94417.230 9.709 43.0280.000 3.458 1.748 0.7310.1850.000 0.000 0.0000.600 0.100 823.00.981.167 0.000 4.92 0.00 180.0
4/2/2025 14:02 0.4054.56017.248 9.722 73.1597.020 6.544 5.561 2.5190.1130.006 0.000 0.0000.700 0.119 823.00.890.984 0.000 4.97 0.00 180.0
4/2/2025 14:03 1.7356.72917.205 9.734 47.9330.000 6.721 2.914 0.8660.1180.000 0.000 0.0000.701 0.080 823.00.851.037 0.000 8.46 0.00 180.0
4/2/2025 14:04 1.7504.39917.193 9.758 48.8880.000 5.199 2.102 0.7990.1880.000 0.000 0.0000.665 0.107 823.00.901.032 0.000 6.15 0.00 180.0
4/2/2025 14:05 0.6304.90417.188 9.748 62.7430.000 5.035 2.427 1.5700.1830.000 0.000 0.0000.681 0.089 824.00.881.054 0.000 5.53 0.00 180.0
4/2/2025 14:07 0.58710.76617.216 9.756 71.5340.000 9.332 4.317 2.2910.2140.086 0.000 0.0001.010 0.081 823.00.841.016 0.000 11.35 0.00 180.0
4/2/2025 14:08 1.01112.73317.144 9.734 29.9190.000 7.026 2.319 0.5650.1710.000 0.000 0.0000.653 0.119 823.00.961.090 0.000 13.74 0.00 180.0
4/2/2025 14:09 0.6189.44817.135 9.727 30.2530.000 3.948 2.614 0.5750.2090.000 0.000 0.0000.538 0.103 824.00.971.142 0.000 10.07 0.00 180.0
4/2/2025 14:10 0.83313.54417.123 9.739 46.4730.000 7.225 2.974 1.1450.2460.000 0.000 0.0000.885 0.095 824.00.871.024 0.000 14.38 0.00 180.0
4/2/2025 14:11 0.8384.18817.132 9.754 54.1490.000 4.512 2.140 1.1370.2220.000 0.000 0.0000.652 0.084 824.00.871.056 0.000 5.03 0.00 180.0
4/2/2025 14:12 0.8304.46917.160 9.748 56.3480.000 5.526 2.047 1.2330.1530.000 0.000 0.0000.701 0.076 824.00.861.067 0.000 5.30 0.00 180.0
4/2/2025 14:13 0.8654.40417.212 9.763 51.6200.000 5.264 1.896 1.1660.1650.000 0.000 0.0000.657 0.079 823.00.911.128 0.000 5.27 0.00 180.0
4/2/2025 14:14 0.5914.71117.189 9.753 64.4470.000 5.109 2.332 1.7210.2340.000 0.000 0.0000.598 0.061 823.00.881.142 0.000 5.30 0.00 180.0
4/2/2025 14:15 0.52512.11717.168 9.732 78.2690.379 11.120 5.513 2.7110.1920.015 0.000 0.0000.961 0.059 824.00.871.128 0.000 12.64 0.00 180.0
4/2/2025 14:16 0.9817.16017.162 9.741 51.8500.000 7.033 2.502 0.9910.1720.000 0.000 0.0000.683 0.085 823.00.861.031 0.000 8.14 0.00 180.0
4/2/2025 14:17 0.9207.86517.160 9.729 50.0730.000 7.513 2.173 1.0570.1670.000 0.000 0.0000.692 0.087 823.00.851.017 0.000 8.79 0.00 180.0
4/2/2025 14:18 1.9104.10317.194 9.738 23.2620.000 2.087 1.901 0.3670.1320.000 0.000 0.0000.616 0.095 823.00.861.002 0.000 6.01 0.00 180.0
4/2/2025 14:19 0.7844.83217.179 9.751 40.9770.000 4.067 2.025 0.7890.1090.000 0.000 0.0000.643 0.072 823.00.941.187 0.000 5.62 0.00 180.0
4/2/2025 14:20 0.3073.94117.157 9.739 48.6660.000 3.773 1.854 0.8870.1430.000 0.000 0.0000.517 0.053 823.00.991.329 0.000 4.25 0.00 180.0
4/2/2025 14:21 0.5303.76117.171 9.743 46.2540.000 3.752 1.835 0.8710.1440.000 0.000 0.0000.544 0.082 823.01.051.335 0.000 4.29 0.00 180.0
4/2/2025 14:22 0.8923.49517.214 9.747 48.1370.000 4.005 1.832 1.0550.1660.000 0.000 0.0000.693 0.061 823.00.861.113 0.000 4.39 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 14:23 0.7653.91617.212 9.725 52.3010.000 4.712 1.958 1.1210.1370.000 0.000 0.0000.682 0.064 824.00.891.142 0.000 4.68 0.00 180.0
4/2/2025 14:24 0.8153.30517.215 9.718 47.5010.000 4.798 1.813 0.8560.1350.000 0.000 0.0000.610 0.083 823.00.901.102 0.000 4.12 0.00 180.0
4/2/2025 14:25 0.6595.70217.201 9.721 51.4520.000 4.712 1.813 0.9350.1050.000 0.000 0.0000.571 0.083 823.00.931.154 0.000 6.36 0.00 180.0
4/2/2025 14:26 0.6873.30317.215 9.745 54.1710.000 4.382 1.708 1.1120.1540.000 0.000 0.0000.629 0.088 823.00.951.164 0.000 3.99 0.00 180.0
0.8436.39417.177 9.740 50.6540.247 5.444 2.427 1.1950.1750.004 0.000 0.0000.679 0.102 823.270.9321.092 0.000 7.237 0.000 180.0Avg.
0.8706.04117.093 9.654 50.1000.123 5.070 2.225 1.0910.4821.312 1.424 0.0000.650 0.091 823.581.9781.270 0.000 6.911 0.000 180.0Run 3 Avg:
Baseline 3
4/2/2025 14:37 0.0130.0000.001 0.000 1.0160.000 0.000 1.308 0.0000.0060.000 0.000 0.0000.000 0.000 824.00.480.716 0.000 0.01 0.00 180.0
Post CTS
4/2/2025 14:40 0.0000.0000.018 0.000 0.3180.000 0.000 0.777 0.2240.0350.000 101.258 0.0000.000 0.000 825.067.540.048 0.000 0.00 0.00 180.0
4/2/2025 14:40 0.0000.0000.014 0.000 0.3090.000 0.000 0.276 0.1190.0210.000 99.657 0.0000.000 0.000 825.066.760.477 0.000 0.00 0.00 179.0
4/2/2025 14:40 0.0000.0000.015 0.000 0.4410.000 0.000 0.528 0.3800.0080.000 99.450 0.0000.000 0.000 824.066.330.035 0.000 0.00 0.00 180.0
4/2/2025 14:41 0.0000.0000.012 0.000 0.4120.000 0.000 0.275 0.2380.0140.000 98.962 0.0000.000 0.000 824.065.980.000 0.000 0.00 0.00 179.0
Post NO2/Mid O2
4/2/2025 14:43 100.3830.000-0.000 0.000 1.1420.000 0.303 1.582 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.370.556 0.000 100.38 10.47 179.0
4/2/2025 14:43 100.7600.000-0.000 0.000 0.2580.000 0.391 1.384 0.0000.0000.000 0.000 0.0000.000 0.000 825.00.400.603 0.000 100.76 10.50 179.0
4/2/2025 14:43 99.5490.000-0.000 0.000 0.0000.000 0.380 1.513 0.0000.0070.000 0.000 0.0000.000 0.000 825.00.340.511 0.000 99.55 10.42 179.0
4/2/2025 14:43 99.7920.000-0.000 0.000 0.0000.000 0.381 1.560 0.0000.0000.000 0.000 0.0000.000 0.000 826.00.410.615 0.000 99.79 10.48 179.0
Post 5-Gas
4/2/2025 14:45 0.000247.2790.007 4.276 6.111493.913 2.850 1.753 5.3170.1010.000 0.000 244.2130.353 0.633 828.0247.493.011 9.717 247.28 0.00 180.0
4/2/2025 14:45 0.000249.6300.008 4.299 6.262499.212 2.855 1.982 4.9490.3650.000 0.000 247.0070.323 0.631 828.0250.653.563 9.789 249.63 0.00 180.0
4/2/2025 14:45 0.000249.8090.004 4.475 5.880501.574 2.932 2.432 5.3520.1260.000 0.077 247.7200.239 0.605 828.0251.083.147 9.755 249.81 0.00 180.0
4/2/2025 14:45 0.000251.9230.003 4.488 5.682502.839 2.897 2.451 3.7910.0590.000 0.206 244.5590.057 1.223 828.0248.451.961 9.770 251.92 0.00 180.0
4/2/2025 14:45 0.000253.3420.000 4.487 5.373502.004 2.905 2.421 3.4320.0100.000 0.167 244.6380.213 1.277 828.0248.421.683 9.797 253.34 0.00 180.0
4/2/2025 14:45 0.000251.0380.003 4.516 5.995502.254 2.953 2.324 3.0830.0430.000 0.119 244.1900.223 1.440 829.0249.483.504 9.757 251.04 0.00 180.0
4/2/2025 14:45 0.000251.2280.003 4.457 5.814504.793 3.009 2.601 4.3140.1070.000 0.020 248.2360.584 0.984 829.0252.062.765 9.780 251.23 0.00 181.0
4/2/2025 14:45 0.000250.5740.005 4.476 5.460503.497 2.867 2.560 2.9050.0760.000 0.099 244.6290.024 1.385 829.0249.773.464 9.782 250.57 0.00 180.0
4/2/2025 14:46 0.000250.8790.004 4.462 5.474503.931 2.886 2.763 4.8280.0870.000 0.060 249.1100.058 0.602 829.0252.903.812 9.774 250.88 0.00 180.0
End of Test Purge
4/2/2025 14:47 0.0004.254-0.000 0.000 0.6770.000 0.379 1.060 2.1180.0120.000 0.000 0.4730.171 0.202 830.00.940.087 0.000 4.25 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
4/2/2025 14:47 0.0000.355-0.000 0.000 0.6940.000 0.054 1.375 0.4790.0080.000 0.000 0.0000.000 0.094 830.00.280.144 0.000 0.36 0.00 180.0
4/2/2025 14:48 0.0000.000-0.000 0.000 0.9590.000 0.000 1.209 0.0000.0370.000 0.000 0.0000.000 0.000 830.00.000.000 0.000 0.00 0.00 180.0
4/2/2025 14:48 0.0000.0000.001 0.000 0.7860.000 0.000 1.208 0.0000.0000.000 0.000 0.0000.000 0.000 830.00.000.000 0.000 0.00 0.00 180.0
4/2/2025 14:48 0.0000.0000.004 0.000 0.6870.000 0.000 1.483 0.0000.0010.000 0.000 0.0000.046 0.000 830.00.170.251 0.000 0.00 0.00 180.0
4/2/2025 14:48 0.0000.0000.001 0.000 0.9650.000 0.000 1.310 0.0000.0230.000 0.000 0.0000.000 0.000 830.00.140.217 0.000 0.00 0.00 180.0
4/2/2025 14:48 0.1530.000-0.000 0.000 1.2270.000 0.000 1.493 0.0000.0000.000 0.000 0.0000.061 0.000 830.00.160.241 0.000 0.15 0.00 180.0
4/2/2025 14:48 0.0000.0000.001 0.000 0.8290.000 0.000 1.217 0.0000.0000.000 0.000 0.0000.077 0.000 830.00.190.288 0.000 0.00 0.00 180.0
GAS