DAQ-2025-002457

1

DAQC-422-25
Site ID 16140 (B4)

MEMORANDUM

TO: STACK TEST FILE – CRUSOE ENERGY SYSTEMS INC. – Mullins Tap Facility

THROUGH: Rik Ombach, Minor Source Oil and Gas Section Manager

FROM: Paul Bushman, Environmental Scientist

DATE: May 2, 2025

SUBJECT: Sources: Five (5) Waukesha 9394 GSI generator engines; SN’s: 1658736,
1651147, 1651154, 1641331, 1641315
Contact: Kaitlin Meszaros: 631-245-0308
Location: 2 miles northwest of Myton, Duchesne County, Utah
Test Contractor: Great Plains Analytical Services, Inc.
Permit/AO#: DAQE-AN161400001-23 dated August 9, 2023
Action Code: TR
Subject: Review of stack test report dated April 29, 2025
On April 29, 2025, Utah Division of Air Quality (DAQ) received a test report for five (5) Waukesha 9394
GSI generator engines located at Crusoe Energy Systems, Inc. Mullins Tap Facility, Duchesne County,
Utah. Testing was performed March 24, 2025, through March 28, 2025, to demonstrate compliance with
the emission limits found in condition II.B.2.a of Approval Order DAQE-AN161400001-23 and 40 CFR
Part 60, Subpart JJJJ. The calculated test results are:

Source Test Date Test
Method Pollutant Tester Results DAQ Results Limits
Waukesha
9394 GSI;
Unit ID: 1351
SN: 1651147
March 25,
2025
ASTM
D6348-03
NOx
5.999
ppmvd@15%O2
0.084 g/hp-hr
0.411 lb/hr
5.999
ppmvd@15%O2
0.084 g/hp-hr
0.411 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
5.128
ppmvd@15%O2
0.044 g/hp-hr
0.214 lb/hr
5.128
ppmvd@15%O2
0.044 g/hp-hr
0.214 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.315
ppmvd@15%O2
0.004 g/hp-hr
0.021 lb/hr
0.315
ppmvd@15%O2
0.004 g/hp-hr
0.021 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha
9394 GSI;
Unit ID: 1352
SN: 1651154
March 26,
2025
ASTM
D6348-03
NOx
4.284
ppmvd@15%O2 0.048 g/hp-hr
0.242 lb/hr
4.285
ppmvd@15%O2 0.048 g/hp-hr
0.243 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
2.413
ppmvd@15%O2
0.016 g/hp-hr
0.083 lb/hr
2.413
ppmvd@15%O2
0.016 g/hp-hr
0.083 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
2

Source Test Date Test
Method Pollutant Tester Results DAQ Results Limits
VOC
0.267
ppmvd@15%O2
0.003 g/hp-hr
0.014 lb/hr
0.267
ppmvd@15%O2
0.003 g/hp-hr
0.015 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha
9394 GSI;
Unit ID: 1451
SN: 1658736
March 24,
2025
ASTM
D6348-03
NOx
4.945
ppmvd@15%O2
0.077 g/hp-hr
0.384 lb/hr
4.945
ppmvd@15%O2
0.077 g/hp-hr
0.383 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
0.484
ppmvd@15%O2
0.005 g/hp-hr
0.023 lb/hr
0.484
ppmvd@15%O2
0.005 g/hp-hr
0.023 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.316
ppmvd@15%O2
0.005 g/hp-hr
0.024 lb/hr
0.317
ppmvd@15%O2
0.005 g/hp-hr
0.023 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha
9394 GSI;
Unit ID:
2026-02
SN: 1641315
March 28,
2025
ASTM
D6348-03
NOx
3.972
ppmvd@15%O2
0.048 g/hp-hr
0.219 lb/hr
3.972
ppmvd@15%O2
0.048 g/hp-hr
0.222 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
8.878
ppmvd@15%O2
0.065 g/hp-hr
0.297 lb/hr
8.878
ppmvd@15%O2
0.066 g/hp-hr
0.302 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.513
ppmvd@15%O2
0.006 g/hp-hr
0.027 lb/hr
0.514
ppmvd@15%O2
0.006 g/hp-hr
0.027 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr
Waukesha
9394 GSI;
Unit ID:
2026-03
SN: 1641315
March 28,
2025
ASTM
D6348-03
NOx
4.636
ppmvd@15%O2
0.061 g/hp-hr
0.292 lb/hr
4.637
ppmvd@15%O2
0.063 g/hp-hr
0.302 lb/hr
82
ppmvd@15%O2
0.15 g/hp-hr
0.83 lb/hr
CO
2.305
ppmvd@15%O2
0.018 g/hp-hr
0.088 lb/hr
2.306
ppmvd@15%O2
0.019 g/hp-hr
0.091 lb/hr
270
ppmvd@15%O2
0.30 g/hp-hr
1.65 lb/hr
VOC
0.364
ppmvd@15%O2
0.005 g/hp-hr
0.022 lb/hr
0.364
ppmvd@15%O2
0.005 g/hp-hr
0.023 lb/hr
60
ppmvd@15%O2
0.03 g/hp-hr
0.17 lb/hr

DEVIATIONS: None.

CONCLUSION: The stack test report appears to be acceptable.

3

RECOMMENDATION: The emissions from the five (5) Waukesha 9394 GSI generator engines
should be considered to have been in compliance with the emission
limits of DAQE-AN161680001-23 and 40 CFR Part 60, Subpart JJJJ
during testing.

ATTACHMENTS: DAQ stack test review excel spreadsheets, Crusoe Energy Systems Inc.
stack test report.

Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1351 SN:1651147
Test Date: 3/25/2025
Run #1 2 3 Average
Start Time 7:37 8:51 10:10
Stop Time 8:37 9:51 11:10
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2225 2225 2225 2225
DS Stack Diameter (inches)18.0 18.0 18.0 18.0PAVG Average (Delta P)½ (" H2O)½0.7550 0.7416 0.7616 0.7527
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)921 936 955 937
Pbar Barometric Pressure (mbar)836 836 836 836
Pbar Barometric Pressure (" Hg)30.32 30.32 30.32 30.32
Ps Stack Pressure ('' H2O)0.57 0.55 0.58 0.57
O2%vd O2 (%vd)0.1 0.1 0.2 0.1
CO2%vd CO2 (%vd)12.2 12.3 12.3 12.3
N2%vd N2 (%vd)87.7 87.6 87.5 87.6
dry NOX (ppmvd)20.4 21.0 22.0 21.1
dry CO (ppmvd) 15.3 18.4 20.5 18.1
wet TVOC (ppmvw as C3H8)0.9 0.8 1.0 0.9
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.184 0.184 0.185 0.184
Bws Saturated Moisture Content (%/100)587.462 624.263 672.454 628.060
Bws Actual Moisture Content (%/100)0.184 0.184 0.185 0.184
MD Molecular Weight Dry (lb/lb-mole)29.96 29.97 29.98 29.97
MA Molecular Weight Wet (lb/lb-mole)27.77 27.77 27.77 27.77
VS Gas Velocity (ft/sec)81.8 80.8 83.5 82.0
FACFM Gas Flow (acfm)8672 8564 8853 8696
FDSCFM Gas Flow (dscfm)2744 2680 2732 2718
FWSCFM Gas Flow (wscfm)3364 3286 3352 3334
FKWSCFH Gas Flow (kwscfh)202 197 201 200
FKWSCFM Gas Flow (kwscfm)3 3 3 3
lb/hr Gas Flow (lb/hr) 14546 14212 14497 14418
Fo Fo (unitless)1.701 1.690 1.684 1.692
wet O2 (%vw)0.1 0.1 0.1 0.1
wet CO2 (%vw)10.0 10.0 10.0 10.0
wet NOX (ppmvw)16.642 17.152 17.928 17.241
15 NOX (ppmvd @ 15% O2)5.778 5.966 6.254 5.999 82.0
lb/hr NOX (lb/hr)0.401 0.403 0.430 0.411 0.83
g/bhp-hr NOX (g/bhp-hr)0.082 0.082 0.088 0.084 0.15
wet CO (ppmvw) 12.454 15.009 16.743 14.735
15 CO (ppmvd @ 15% O2)4.324 5.220 5.841 5.128 270.0
lb/hr CO (lb/hr) 0.182 0.215 0.244 0.214 1.65
g/bhp-hr CO (g/bhp-hr) 0.037 0.044 0.050 0.044 0.30
dry NMEOC (ppmvd as C3H8)1.122 1.030 1.177 1.110
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.318 0.292 0.335 0.315 60
lb/hr NMEOC (lb/hr as C3H8)0.021 0.019 0.022 0.021 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.004 0.004 0.004 0.004 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.086 0.086 0.092 0.088
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1351 SN:1651147
Test Date: 3/25/2025
O2
21.2
10.71
0.0
10.8
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.71
21.15
0.0
10.8
21.2
0.0
0.1
0.1
0.0
0.00%
0.05%
0.43%
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
4
Difference
1
4
Response
1
2
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1351 SN:1651147
Test Date: 3/25/2025
O2
21.2
10.71
0.0
10.8
0.0
10.8
0.0%
0.0%
0.0%
0.0%
Corrected O2 %
0.1
Run Length
(Minutes) Uncorrected O2 %
60 0.1
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1351 SN:1651147
Test Date: 3/25/2025
O2
21.2
10.71
0.0
10.8
0.0
10.8
0.0%
0.0%
0.0%
0.0%
Corrected O2 %
0.1
Run Length
(Minutes) Uncorrected O2 %
60 0.1
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1351 SN:1651147
Test Date: 3/25/2025
O2
21.2
10.71
0.0
10.8
0.0
10.8
0.0%
0.0%
0.0%
0.0%
Corrected O2 %
0.2
Run Length
(Minutes) Uncorrected O2 %
60 0.2
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1352 SN:1651154
Test Date: 3/26/2025
Run #1 2 3 Average
Start Time 7:27 8:59 10:14
Stop Time 8:27 9:59 11:14
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2300 2300 2300 2300
DS Stack Diameter (inches)18.0 18.0 18.0 18.0PAVG Average (Delta P)½ (" H2O)½0.6325 0.6325 0.6325 0.6325
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)956 967 979 967
Pbar Barometric Pressure (mbar)1020 1020 1018 1019
Pbar Barometric Pressure (" Hg)30.13 30.12 30.06 30.10
Ps Stack Pressure ('' H2O)0.40 0.40 0.40 0.40
O2%vd O2 (%vd)0.2 0.2 0.2 0.2
CO2%vd CO2 (%vd)12.1 12.1 12.2 12.1
N2%vd N2 (%vd)87.7 87.7 87.7 87.7
dry NOX (ppmvd)15.4 14.7 15.0 15.1
dry CO (ppmvd) 9.1 8.2 8.1 8.5
wet TVOC (ppmvw as C3H8)0.8 0.7 0.8 0.8
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.183 0.183 0.184 0.183
Bws Saturated Moisture Content (%/100)679.620 709.266 744.074 710.987
Bws Actual Moisture Content (%/100)0.183 0.183 0.184 0.183
MD Molecular Weight Dry (lb/lb-mole)29.95 29.95 29.95 29.95
MA Molecular Weight Wet (lb/lb-mole)27.77 27.76 27.76 27.76
VS Gas Velocity (ft/sec)69.6 69.9 70.3 69.9
FACFM Gas Flow (acfm)7380 7411 7450 7414
FDSCFM Gas Flow (dscfm)2265 2255 2243 2254
FWSCFM Gas Flow (wscfm)2774 2763 2749 2762
FKWSCFH Gas Flow (kwscfh)166 166 165 166
FKWSCFM Gas Flow (kwscfm)3 3 3 3
lb/hr Gas Flow (lb/hr) 11994 11944 11882 11940
Fo Fo (unitless)1.706 1.709 1.707 1.707
wet O2 (%vw)0.2 0.1 0.1 0.1
wet CO2 (%vw)9.9 9.9 9.9 9.9
wet NOX (ppmvw)12.580 12.029 12.282 12.297
15 NOX (ppmvd @ 15% O2)4.386 4.189 4.279 4.285 82.0
lb/hr NOX (lb/hr)0.250 0.238 0.242 0.243 0.83
g/bhp-hr NOX (g/bhp-hr)0.049 0.047 0.048 0.048 0.15
wet CO (ppmvw) 7.446 6.702 6.626 6.925
15 CO (ppmvd @ 15% O2)2.596 2.334 2.309 2.413 270.0
lb/hr CO (lb/hr) 0.090 0.081 0.079 0.083 1.65
g/bhp-hr CO (g/bhp-hr) 0.018 0.016 0.016 0.016 0.30
dry NMEOC (ppmvd as C3H8)0.942 0.909 0.966 0.939
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.268 0.258 0.275 0.267 60
lb/hr NMEOC (lb/hr as C3H8)0.015 0.014 0.015 0.015 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.003 0.003 0.003 0.003 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.052 0.050 0.051 0.051
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1352 SN:1651154
Test Date: 3/26/2025
O2
21.2
10.71
0.0
10.9
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.9
%
0.00
10.71
21.15
0.0
10.9
21.4
0.0
0.2
0.3
0.0
0.00%
0.09%
1.32%
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
4
Difference
1
4
Response
1
2
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1352 SN:1651154
Test Date: 3/26/2025
O2
21.2
10.71
0.0
10.9
0.0
11.0
0.0%
0.3%
0.0%
0.4%
Corrected O2 %
0.2
Run Length
(Minutes) Uncorrected O2 %
60 0.2
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1352 SN:1651154
Test Date: 3/26/2025
O2
21.2
10.71
0.0
10.9
0.0
11.0
0.0%
0.3%
0.0%
0.4%
Corrected O2 %
0.2
Run Length
(Minutes) Uncorrected O2 %
60 0.2
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1352 SN:1651154
Test Date: 3/26/2025
O2
21.2
10.71
0.0
10.9
0.0
11.0
0.0%
0.3%
0.0%
0.4%
Corrected O2 %
0.2
Run Length
(Minutes) Uncorrected O2 %
60 0.2
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1451 SN:1658736
Test Date: 3/24/2025
Run #1 2 3 Average
Start Time 9:01 10:44 12:00
Stop Time 10:01 11:44 13:00
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2250 2250 2250 2250
DS Stack Diameter (inches)20.0 20.0 20.0 20.0PAVG Average (Delta P)½ (" H2O)½0.7071 0.7071 0.6928 0.7023
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)922 942 941 935
Pbar Barometric Pressure (mbar)1025 1025 1025 1025
Pbar Barometric Pressure (" Hg)30.28 30.28 30.28 30.28
Ps Stack Pressure ('' H2O)0.50 0.46 0.48 0.48
O2%vd O2 (%vd)0.58 0.63 0.61 0.6
CO2%vd CO2 (%vd)11.9 12.0 11.9 11.9
N2%vd N2 (%vd)87.6 87.4 87.5 87.5
dry NOX (ppmvd)13.5 23.8 13.8 17.0
dry CO (ppmvd) 1.7 1.8 1.5 1.7
wet TVOC (ppmvw as C3H8)1.0 0.7 0.9 0.9
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.181 0.182 0.182 0.181
Bws Saturated Moisture Content (%/100)590.892 640.496 637.928 623.105
Bws Actual Moisture Content (%/100)0.181 0.182 0.182 0.181
MD Molecular Weight Dry (lb/lb-mole)29.92 29.94 29.92 29.93
MA Molecular Weight Wet (lb/lb-mole)27.77 27.77 27.75 27.76
VS Gas Velocity (ft/sec)76.7 77.24 75.7 76.5
FACFM Gas Flow (acfm)10038 10110 9905 10018
FDSCFM Gas Flow (dscfm)3181 3154 3092 3142
FWSCFM Gas Flow (wscfm)3885 3857 3782 3841
FKWSCFH Gas Flow (kwscfh)233 231 227 230
FKWSCFM Gas Flow (kwscfm)4 4 4 4
lb/hr Gas Flow (lb/hr) 16801 16680 16345 16608
Fo Fo (unitless)1.714 1.696 1.712 1.707
wet O2 (%vw)0.5 0.5 0.5 0.5
wet CO2 (%vw)9.7 9.8 9.7 9.7
wet NOX (ppmvw)11.028 19.457 11.261 13.915
15 NOX (ppmvd @ 15% O2)3.909 6.923 4.003 4.945 82.0
lb/hr NOX (lb/hr)0.307 0.537 0.305 0.383 0.83
g/bhp-hr NOX (g/bhp-hr)0.062 0.108 0.061 0.077 0.15
wet CO (ppmvw) 1.389 1.462 1.238 1.363
15 CO (ppmvd @ 15% O2)0.492 0.520 0.440 0.484 270.0
lb/hr CO (lb/hr) 0.024 0.025 0.020 0.023 1.65
g/bhp-hr CO (g/bhp-hr) 0.005 0.005 0.004 0.005 0.30
dry NMEOC (ppmvd as C3H8)1.256 0.860 1.150 1.089
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.365 0.250 0.335 0.317 60
lb/hr NMEOC (lb/hr as C3H8)0.027 0.019 0.024 0.023 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.006 0.004 0.005 0.005 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.067 0.112 0.066 0.082
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1451 SN:1658736
Test Date: 3/24/2025
O2
21.2
10.71
0.0
10.7
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.7
%
0.00
10.71
21.15
0.0
10.7
21.1
0.0
0.0
0.0
0.0
0.00%
0.24%
0.14%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1451 SN:1658736
Test Date: 3/24/2025
O2
21.2
10.71
0.0
10.7
0.0
10.9
0.0%
0.9%
0.0%
0.7%
Corrected O2 %
0.6
Run Length
(Minutes) Uncorrected O2 %
60 0.6
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1451 SN:1658736
Test Date: 3/24/2025
O2
21.2
10.71
0.0
10.7
0.0
10.9
0.0%
0.9%
0.0%
0.7%
Corrected O2 %
0.6
Run Length
(Minutes) Uncorrected O2 %
60 0.6
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 1451 SN:1658736
Test Date: 3/24/2025
O2
21.2
10.71
0.0
10.7
0.0
10.9
0.0%
0.9%
0.0%
0.7%
Corrected O2 %
0.6
Run Length
(Minutes) Uncorrected O2 %
60 0.6
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-02 SN:1641315
Test Date: 3/28/2025
Run #1 2 3 Average
Start Time 7:41 8:53 10:10
Stop Time 8:41 9:53 11:10
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2075 2075 2075 2075
DS Stack Diameter (inches)18.0 18.0 18.0 18.0PAVG Average (Delta P)½ (" H2O)½0.6245 0.6245 0.6403 0.6298
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)955 959 979 965
Pbar Barometric Pressure (mbar)1018 1007 1007 1011
Pbar Barometric Pressure (" Hg)30.06 29.75 29.75 29.85
Ps Stack Pressure ('' H2O)0.39 0.39 0.41 0.40
O2%vd O2 (%vd)0.49 0.46 0.49 0.5
CO2%vd CO2 (%vd)11.7 11.6 11.7 11.7
N2%vd N2 (%vd)87.8 87.9 87.8 87.8
dry NOX (ppmvd)13.8 14.0 13.4 13.7
dry CO (ppmvd) 27.3 30.9 33.9 30.7
wet TVOC (ppmvw as C3H8)1.4 1.4 1.6 1.5
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.179 0.178 0.178 0.178
Bws Saturated Moisture Content (%/100)679.077 696.869 751.972 709.306
Bws Actual Moisture Content (%/100)0.179 0.178 0.178 0.178
MD Molecular Weight Dry (lb/lb-mole)29.89 29.88 29.89 29.89
MA Molecular Weight Wet (lb/lb-mole)27.77 27.77 27.77 27.77
VS Gas Velocity (ft/sec)68.8 69.24 71.5 69.8
FACFM Gas Flow (acfm)7293 7341 7580 7405
FDSCFM Gas Flow (dscfm)2246 2234 2273 2251
FWSCFM Gas Flow (wscfm)2736 2718 2768 2741
FKWSCFH Gas Flow (kwscfh)164 163 166 164
FKWSCFM Gas Flow (kwscfm)3 3 3 3
lb/hr Gas Flow (lb/hr) 11834 11756 11970 11853
Fo Fo (unitless)1.743 1.756 1.746 1.748
wet O2 (%vw)0.4 0.4 0.4 0.4
wet CO2 (%vw)9.6 9.6 9.6 9.6
wet NOX (ppmvw)11.330 11.530 11.039 11.300
15 NOX (ppmvd @ 15% O2)3.986 4.048 3.883 3.972 82.0
lb/hr NOX (lb/hr)0.222 0.224 0.219 0.222 0.83
g/bhp-hr NOX (g/bhp-hr)0.048 0.049 0.048 0.048 0.15
wet CO (ppmvw) 22.460 25.450 27.852 25.254
15 CO (ppmvd @ 15% O2)7.901 8.936 9.797 8.878 270.0
lb/hr CO (lb/hr) 0.268 0.301 0.336 0.302 1.65
g/bhp-hr CO (g/bhp-hr) 0.059 0.066 0.073 0.066 0.30
dry NMEOC (ppmvd as C3H8)1.687 1.740 1.905 1.777
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.488 0.502 0.551 0.514 60
lb/hr NMEOC (lb/hr as C3H8)0.026 0.027 0.030 0.027 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.006 0.006 0.006 0.006 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.054 0.055 0.054 0.054
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-02 SN:1641315
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.71
21.15
0.0
10.8
21.1
0.0
0.1
0.1
0.0
0.00%
2.60%
0.47%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-02 SN:1641315
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
0.0
10.5
0.0%
1.5%
0.0%
1.1%
Corrected O2 %
0.5
Run Length
(Minutes) Uncorrected O2 %
60 0.5
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-02 SN:1641315
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
0.0
10.5
0.0%
1.5%
0.0%
1.1%
Corrected O2 %
0.5
Run Length
(Minutes) Uncorrected O2 %
60 0.5
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-02 SN:1641315
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
0.0
10.5
0.0%
1.5%
0.0%
1.1%
Corrected O2 %
0.5
Run Length
(Minutes) Uncorrected O2 %
60 0.5
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-03 SN:1641331
Test Date: 3/28/2025
Run #1 2 3 Average
Start Time 12:03 1:16 2:28
Stop Time 13:03 2:16 3:28
Sample Duration (minutes)60 60 60
BHP Engine Load (hp) 2175 2175 2175 2175
DS Stack Diameter (inches)18.0 18.0 18.0 18.0PAVG Average (Delta P)½ (" H2O)½0.7810 0.8246 0.8124 0.8060
CP Pitot Tube Constant (unitless)0.99 0.99 0.99 0.99
TS Stack Temperature (°F)993 1010 1007 1004
Pbar Barometric Pressure (mbar)1021 1021 1021 1021
Pbar Barometric Pressure (" Hg)30.17 30.17 30.17 30.17
Ps Stack Pressure ('' H2O)0.61 0.68 0.66 0.65
O2%vd O2 (%vd)2.3 2.3 2.6 2.4
CO2%vd CO2 (%vd)10.8 10.7 10.6 10.7
N2%vd N2 (%vd)86.9 86.9 86.8 86.9
dry NOX (ppmvd)14.8 15.4 13.4 14.5
dry CO (ppmvd) 8.2 7.3 6.2 7.2
wet TVOC (ppmvw as C3H8)1.1 1.0 0.8 1.0
Run #1 2 3 Average
Bws Measured Moisture Content (%/100)0.165 0.164 0.162 0.164
Bws Saturated Moisture Content (%/100)780.702 830.259 821.396 810.785
Bws Actual Moisture Content (%/100)0.165 0.164 0.162 0.164
MD Molecular Weight Dry (lb/lb-mole)29.82 29.81 29.79 29.81
MA Molecular Weight Wet (lb/lb-mole)27.87 27.87 27.88 27.87
VS Gas Velocity (ft/sec)86.8 92.2 90.7 89.9
FACFM Gas Flow (acfm)9208 9776 9620 9535
FDSCFM Gas Flow (dscfm)2818 2962 2928 2903
FWSCFM Gas Flow (wscfm)3378 3546 3496 3474
FKWSCFH Gas Flow (kwscfh)203 213 210 208
FKWSCFM Gas Flow (kwscfm)3 4 3 3
lb/hr Gas Flow (lb/hr) 14660 15392 15182 15078
Fo Fo (unitless)1.726 1.729 1.732 1.729
wet O2 (%vw)1.9 2.0 2.2 2.0
wet CO2 (%vw)9.0 9.0 8.8 8.9
wet NOX (ppmvw)12.340 12.841 11.255 12.145
15 NOX (ppmvd @ 15% O2)4.693 4.886 4.332 4.637 82.0
lb/hr NOX (lb/hr)0.298 0.326 0.282 0.302 0.83
g/bhp-hr NOX (g/bhp-hr)0.062 0.068 0.059 0.063 0.15
wet CO (ppmvw) 6.843 6.059 5.220 6.041
15 CO (ppmvd @ 15% O2)2.602 2.306 2.009 2.306 270.0
lb/hr CO (lb/hr) 0.101 0.094 0.079 0.091 1.65
g/bhp-hr CO (g/bhp-hr) 0.021 0.020 0.017 0.019 0.30
dry NMEOC (ppmvd as C3H8)1.285 1.175 0.962 1.141
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.408 0.374 0.310 0.364 60
lb/hr NMEOC (lb/hr as C3H8)0.025 0.024 0.019 0.023 0.17
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.005 0.005 0.004 0.005 0.03
g/bhp-hr HC+NOX (g/bhp-hr)0.067 0.073 0.063 0.068
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-03 SN:1641331
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.71
21.15
0.0
10.8
21.1
0.0
0.1
0.1
0.0
0.00%
2.60%
0.47%
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
4
Difference
1
4
Response
1
2
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
Page 2 of 5
Run 1
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-03 SN:1641331
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
0.0
10.5
0.0%
1.7%
0.0%
0.9%
Corrected O2 %
2.3
Run Length
(Minutes) Uncorrected O2 %
60 2.2
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Page 3 of 5
Run 2
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-03 SN:1641331
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
0.0
10.5
0.0%
1.7%
0.0%
0.9%
Corrected O2 %
2.3
Run Length
(Minutes) Uncorrected O2 %
60 2.3
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Page 4 of 5
Run 3
Crusoe Energy Systems, Inc.
Mullins Tap Facility
Duchesne County, Utah
Waukesha 9394 GSI Unit 2026-03 SN:1641331
Test Date: 3/28/2025
O2
21.2
10.71
0.0
10.3
0.0
10.5
0.0%
1.7%
0.0%
0.9%
Corrected O2 %
2.6
Run Length
(Minutes) Uncorrected O2 %
60 2.5
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Page 5 of 5
303 West 3rd Street ● Elk City, Oklahoma 73644 ● 580-225-0403

GAS Inc.
www.gasinc.us
April 29, 2025

Utah Department of Environmental Quality
State Office Building – Air Quality Division
195 North 1950 West
Salt Lake City, Utah 84114

RE: Crusoe Energy Systems, Inc.
40 CFR Part 60 Subpart JJJJ – Test Report SubmiVal

To Whom It May Concern,

Please find enclosed the performance tesXng reports for 40 CFR Subpart JJJJ/State Compliance
on behalf of Crusoe Energy Systems, Inc. Please see below for the informaXon perXnent to the
tesXng. Please see below for the informaXon perXnent to the enclosed reports. Test took place
the week of March 24, 2025.

Facility Unit # Serial # Loca1on
Mullins Tap Facility 1451 1658736 Duchesne County, Utah
Mullins Tap Facility 1351 1651147 Duchesne County, Utah
Mullins Tap Facility 1352 1651154 Duchesne County, Utah
Mullins Tap Facility 2026-03 1641331 Duchesne County, Utah
Mullins Tap Facility 2026-02 1641315 Duchesne County, Utah

For informaXon regarding the performance test, you can contact me by email at
[e-mail] or by phone at 580-225-0403. For informaXon regarding engine or
locaXon informaXon, please contact Kaitlin Meszaros by email at [e-mail] or
by phone at (631)-245-0308.

Regards,

Macie Holsapple
Client Services Supervisor
GAS Inc.
Performance Test Report
Test Type: Annual
Test Date: 3/25/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:07:52 AM 11:50 AM
Source:
Unit Number: 1351
Serial Number: 1651147
Engine Hours:11246
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.214 0.411 0.021
18.062 21.133 1.109
2.000 0.300 1.000 0.150 0.700 0.030
0.044 0.084 0.004
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
LYNN HUBER
3
Cody Hall
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 1351 with a serial number of 1651147 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 3/25/2025 by
Cody Hall with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were
within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2225 BHP and 1199 RPM which is 89.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1351 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1351Unit ID
Make Waukesha Site Elevation ft.5248
Model 9394 GSI Atmospheric Pressure psi.12.08
Serial Number 1651147 Stack Diameter in.18
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2225 2225 2225 2225
1200 1198 1199 1199
Percent Load %
Intake Manifold Pressure (hg)
89.00%89.00%89.00%89.00%
99.60 99.60 99.60 99.60
Intake Manifold Temperature (F)117.00 118.00 118.00 117.67
Ambient Conditions
Ambient Temperature Dry (F)34.00 55.00 69.00 52.67
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
164766.35 162947.58 160678.89 162797.61
4665.62 4614.12 4549.88 4609.87
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %18.38%18.41%18.46%18.42%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.08%0.11%0.16%0.11%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
07:52 AM 09:10 AM 10:29 AM 3/25/2025
State
NOx (mol wt) 46.01
0.916 0.840 0.960 0.905NMNEHC (ppmvw)
1.122 1.030 1.177 1.109NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
317.807 292.152 334.685 314.881 FailNMNEHC (ppbvd) @15% O2
0.004 0.004 0.004 0.0040.700 0.030 PassNMNEHC (g/hp-hr)
0.021 0.019 0.022 0.0210.170 PassNMNEHC (lbs/hr)
0.318 0.292 0.335 0.315 FailNMNEHC (ppmvd) @15% O2
0.0490.044CO (g/hp-hr)0.037 0.0442.000 0.300 Pass
CO (ppmvw)12.454 15.009 16.743 14.735
CO (ppmvd)15.258 18.395 20.533 18.062
CO (mol wt) 28.01
CO (ppmvd) @15% O2 4.323 5.220 5.840 5.128 Fail
CO (ppbvd) @15% O2 4323.106 5219.955 5840.163 5127.741 Fail
0.2400.218CO (lbs/hr)0.183 0.2141.650 Pass
NOx (g/hp-hr)0.082 0.083 0.086 0.0841.000 0.150 Pass
NOx (ppmvw)16.642 17.152 17.928 17.240
NOx (ppmvd)20.390 21.022 21.986 21.133
NOx (ppbvd) @15% O2 5776.928 5965.290 6253.505 5998.574 Fail
NOx (ppmvd) @15% O2 5.777 5.965 6.254 5.999 Fail
NOx (lbs/hr)0.401 0.409 0.422 0.4110.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
12.45
0.17
16.51 0.13 16.64
0.03%
0.06%
0.00%
18.38%
17.20 0.17 0.05%18.38%
33.17 1.73 0.06%16.75%
15.82 0.10 0.07%18.39%
0.00 0.00 0.00 0.12%0.02%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.91 0.00 0.00 0.00 0.12%0.02%
13.99 17.38 0.15 17.53 0.08%18.40%
60.73 27.96 3.85 31.81 0.04%16.82%
16.03 16.35 0.42 16.77 0.09%18.42%
0.92 0.00 0.00 0.00 0.12%0.02%
Avg. Wet 15.01 16.86 0.29 17.15 0.84 0.08%18.41%
NO2NO
0.18
0.83
22.61
0.85
0.24
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
17.87 17.96 0.35 18.31 0.14%18.46%
56.53 33.12 5.14 38.26 0.05%16.89%
15.62 17.20 0.35 17.55 0.11%18.46%
0.82 0.00 0.00 0.00 0.11%0.03%
0.92 0.00 0.00 0.00 0.24 0.12%0.02%
Avg. Wet 16.74 17.58 0.35 17.93 0.96 0.12%18.46%
NO2NO
0.39
1.00
22.49
0.92
NMNEHC
0.36
NO2
0.000.85
0.94
24.76
0.89
0.18
0.92
0.16
17.37
34.90
15.92
11.76
13.14
0.91
78.14
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =18 Inches or:1.5 feet or:1.77 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.67
Yes
18.00
11.00
17.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%18.38
29.96
0.57
Inches
3.01
9
14.99
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
12.24
0.05
0.00
1026.41
0.04
30.32
30.36
921.13
1380.80
493.96
27.76
81.79
144.52
201875.02
164766.35
Run 2
18.41
29.97
0.55
12.30
0.11
0.00
1026.41
0.04
30.32
30.36
936.13
1395.80
502.29
27.77
80.53
144.53
199717.58
162947.58
Run 3
18.46
29.98
0.58
12.32
0.16
0.00
1026.41
0.04
30.32
30.36
955.00
1414.67
512.78
27.77
83.40
144.53
197052.88
160678.89
18.42
29.97
0.57
12.29
0.11
0.00
1026.41
0.04
30.32
30.36
937.42
1397.09
503.01
27.77
81.91
144.53
199548.5
162797.61
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.54
Exhaust Temp F
921.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.62
0.66
0.63
921.00
921.00
922.00
0.60
0.53
0.61
922.00
922.00
920.00
0.70
0.74
0.63
920.00
920.00
921.00
0.52 921.00
0.59
0.50
0.47
921.00
922.00
922.00
0.39
0.36
0.57
922.00
920.00
921.13
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.53
Exhaust Temp F
955.00
0.59
0.63
0.66
955.00
955.00
954.00
0.66
0.61
0.57
954.00
954.00
956.00
0.55
0.52
0.49
956.00
956.00
955.00
0.45 955.00
0.51
0.57
0.59
955.00
954.00
954.00
0.66
0.67
954.00
958.00
955.000.58
Run 2
Δpstd (in) H2O
0.60
Exhaust Temp F
936.00
0.55
0.55
0.51
936.00
936.00
937.00
0.45
0.43
0.49
937.00
937.00
935.00
0.53
0.57
0.59
935.00
935.00
936.00
0.66 936.00
0.61
0.61
0.54
936.00
937.00
937.00
0.57
0.49
937.00
935.00
0.55 936.13
Pass
Strat Check
15.04Check 1
15.22Check 2
15.17Check 3
NoxGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(12.235)+ .32(.051)+ .28(87.712+.002) = 29.96 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.96(1 -.18382)+ 18.0(.18382) = 27.76 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.57*√(1380.8/(30.36*27.76)) = 81.79 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.18382)81.79*1.767((528*30.36)/ (1380.8*29.92)) = 164766.35 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 164766.354/35.315 = 4665.62 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 15.258*(20.9-15)/(20.9-.08%)) = 4.323 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(15.258*(1.164*10^-3)*4665.62*(Run Time/60))/2225 = .037 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .037*1/453.6*2225 = .183 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .183*4.38 = .802 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
15.26 = 12.4535*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.80%
21.23%
10.79%
10.80%
10.71%
10.71%
10.80%10.79%
10.80%
21.23%
10.71%
21.15%
10.71%
21.15%
10.71%21.15%
0.00%
10.71%
21.15%
0.09%
0.08%
0.44%
0.38%
10.71%
Span
Zero Offset 0.00%
21.15
0.00%
10.80%0.08%0.03%0.00%
0.08%
0.11%
0.16%
0.08%
0.11%
0.16%
9
GAS
0.0 0.0 0.0
0.0 0.0 0.0
1049.0 1049.0 1049.0
1071.0 1071.0 1071.0
0.7 0.7 .7
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
3/25/2025
5248
1351
Waukesha
Model
Serial Number
9394 GSI
1651147
Technician Cody Hall
Run Start Times 07:52 AM 09:10 AM 10:29 AM 11:50 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1198.0 1199.0 1199.0
Engine Hours 11243 11244 11245 11246
Intake Manifold Pressure (psi)61.0 61.0 61.0 61.0
Intake Manifold Temp °F 117.0 118.0 118.0 117.7
Engine Load (BHP)2225.0 2225.0 2225.0 2225.0
Ambient Temp °F 34.0 55.0 69.0 52.7
Humidity %74.0 74.0 77.0 75.0
Dew Point °F 27.0 30.0 18.0 25.0
Waukesha
N/A
N/A
Yes
N/A N/A N/A N/A
3 3 3 3# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1049.0
1071.0
0.7Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.13
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.04
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.04
Average:VOC 0.30
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 99.40
Tolerance 2.00%
Difference between measured and expected 0.60%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.71
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.35
Average:Oxygen 0.14
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 97.80
Tolerance 5.00%
Difference between measured and expected 2.20%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 247.66
Value:Spike Expected 251.20
System (Equilibration) Response Time Target (Spike)
89 secondsSystem Zero Response Time
89 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC524646 12/30/2027 104.20 10.71%
CC312964 10/17/2032 100.00
CC337712 5/1/2032 21.15%
Cylinder # CC230781 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 251.20 501.50 251.30 10.03
Analyzer System Response 247.66 498.14 249.65 9.90
Percent Difference 1.41%0.67%0.66%1.34%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.402 4.970
Spike Direct
Propane 249.162
Mechanical
Response Time
SF6 9.944
CO 500.661
NO 250.448
Ethylene 97.800 25 seconds
Analyzer
Response
Propane 247.658
SF6 9.896
CO 498.139
NO 249.648
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 248.846
CO 498.701
NO 248.223
42 seconds
89 seconds
8.95%
8.54%
8.51%
94.72%
93.99%
93.86%
9.915
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.006
50%9.000
83.3%14.994
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
18
11
17
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
162797.61
H2O%d @ Sampling Point:18.42
CO2%d @ Sampling Point:12.29
Pressure @ Sampling Point (Pg "H2O):0.57
Temperature @ Sampling Point (Deg F):937.42
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 100 99.4 4.97 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.402 4.970
Spike Direct
Propane 249.162
Mechanical
Response Time
SF6 9.944
CO 500.661
NO 250.448
Ethylene 97.800 25 seconds
Analyzer
Response
Propane 247.658
SF6 9.896
CO 498.139
NO 249.648
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 248.846
CO 498.701
NO 248.223
42 seconds
89 seconds
8.95%
8.54%
8.51%
94.72%
93.99%
93.86%
9.915
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
251.200
10.030
501.500
251.300
249.162
9.944
500.661
250.448
0.81%
0.86%
0.17%
0.34%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.002
Spike Average
21.295
0.890
Dilution Factor
8.950%
Expected
22.482
% Recovery
94.720%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.849
Dilution Factor
8.538%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.846
Dilution Factor
8.508%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 20.065 21.377 93.860%
0.011402
0.008894
0.006517
0.000 20.163 21.453 93.990%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass1.13%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-2.90650767 Pass
Line Position Difference:Resolution Difference to Reference 1.13%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
100.00
99.57
0.43%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1351; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
3/25/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
3/25/2025
Cody Hall
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 18S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Cody Hall
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1351
Make:Waukesha
Location:9394 GSIModel:
1651147Serial Number:
RAW Result Data
Stability
3/25/2025 05:55 0.3982.4130.104 0.000 0.1224.378 0.000 0.000 0.0000.0000.000 0.159 1.6570.057 0.398 849.02.560.000 0.000 2.81 0.51 181.0
Pre Test Baseline Direct
3/25/2025 06:05 0.0000.000-0.000 0.000 0.0000.176 0.029 0.000 0.0000.0009.257 0.924 0.0000.004 0.000 853.00.660.061 0.000 0.00 0.00 181.0
3/25/2025 06:07 0.0000.000-0.001 0.000 0.0000.122 0.011 0.000 0.0000.0001.151 0.152 0.0000.100 0.000 851.00.170.097 0.000 0.00 0.00 181.0
3/25/2025 06:08 0.0000.126-0.000 0.000 0.0000.102 0.015 0.000 0.0000.0001.355 0.015 0.0000.045 0.000 851.00.080.100 0.001 0.13 0.00 181.0
CTS Direct
3/25/2025 06:14 0.0000.1090.012 0.000 0.0000.140 0.042 0.175 0.0000.00010.475 99.874 0.0000.047 0.017 849.066.690.099 0.000 0.11 0.06 180.0
3/25/2025 06:15 0.0000.4800.010 0.000 0.0000.023 0.023 0.025 0.0000.0002.912 98.920 0.0000.037 0.003 847.066.040.124 0.000 0.48 0.06 180.0
3/25/2025 06:16 0.0000.4270.010 0.000 0.0000.045 0.025 0.197 0.0000.0002.956 99.412 0.0030.177 0.014 843.066.360.074 0.000 0.43 0.06 180.0
High O2 Direct
3/25/2025 06:26 0.0000.0000.002 0.028 0.0000.060 0.003 0.000 0.0000.0001.094 0.000 0.0000.112 0.000 847.00.110.158 0.000 0.00 21.24 180.0
3/25/2025 06:26 0.0000.0000.002 0.036 0.0000.050 0.006 0.050 0.0000.0001.187 0.000 0.0000.095 0.000 847.00.070.098 0.000 0.00 21.23 180.0
3/25/2025 06:27 0.0000.0000.001 0.037 0.1550.115 0.012 0.000 0.0000.0001.484 0.000 0.0000.018 0.008 847.00.040.035 0.000 0.00 21.22 180.0
NO2/Mid O2 Direct
3/25/2025 06:36 102.8870.285-0.000 0.000 0.2180.000 0.980 0.000 0.7620.0000.459 0.000 0.0000.000 0.000 847.00.000.000 0.000 103.17 10.81 180.0
3/25/2025 06:37 102.8580.225-0.001 0.000 0.4180.002 0.986 0.000 0.8550.0001.297 0.000 0.0000.000 0.000 847.00.000.000 0.000 103.08 10.80 180.0
3/25/2025 06:37 102.4150.319-0.001 0.000 0.3690.000 0.983 0.000 0.7450.0001.561 0.000 0.0000.000 0.000 847.00.000.000 0.000 102.73 10.80 180.0
Spike Direct
3/25/2025 06:46 0.000250.1010.002 4.962 1.784500.335 2.295 1.200 10.3000.2161.655 1.110 249.0490.000 0.000 847.0251.502.560 9.941 250.10 0.02 180.0
3/25/2025 06:47 0.000250.5360.002 4.977 1.758500.335 2.273 1.310 10.4310.2631.325 1.127 249.1310.000 0.000 847.0251.612.584 9.937 250.54 0.02 180.0
3/25/2025 06:47 0.000250.7060.004 4.975 1.700501.314 2.254 1.196 10.3720.2101.391 1.072 249.3070.000 0.000 847.0251.822.698 9.955 250.71 0.02 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
3/25/2025 06:53 0.0000.0000.030 0.088 0.0000.937 0.000 0.939 0.0000.0001.006 0.000 0.1700.000 0.118 847.00.410.000 0.000 0.00 0.15 180.0
3/25/2025 06:53 0.0000.0000.023 0.090 0.0000.658 0.000 0.771 0.0000.0001.317 0.000 0.0340.000 0.120 847.00.300.037 0.000 0.00 0.14 180.0
3/25/2025 06:53 0.0000.0000.019 0.081 0.0000.523 0.000 0.623 0.0000.0011.203 0.000 0.0330.000 0.095 847.00.330.161 0.000 0.00 0.13 180.0
CTS System with Response Time
3/25/2025 06:55 0.0000.0000.029 0.090 0.0000.477 0.000 0.482 0.0000.0000.000 97.721 0.0000.000 0.099 847.065.350.000 0.000 0.00 0.06 180.0
3/25/2025 06:55 0.0000.0000.029 0.096 0.0000.465 0.000 0.510 0.0000.0000.000 97.907 0.0000.000 0.077 847.065.450.032 0.000 0.00 0.06 180.0
3/25/2025 06:55 0.0000.0000.028 0.097 0.0000.480 0.000 0.496 0.0000.0000.000 97.771 0.0000.021 0.053 847.065.350.096 0.000 0.00 0.06 180.0
NO2/Mid O2 System with Response Time
3/25/2025 07:00 103.6471.5810.012 0.081 0.0000.563 0.969 0.243 0.0900.0000.851 0.000 0.0000.333 0.110 847.00.350.193 0.000 105.23 10.75 180.0
3/25/2025 07:01 104.2241.5440.011 0.067 0.0000.578 0.955 0.081 0.0950.0000.770 0.000 0.0000.227 0.095 847.00.390.305 0.000 105.77 10.84 180.0
3/25/2025 07:01 103.8781.2720.010 0.074 0.0000.561 0.965 0.354 0.0000.0000.778 0.000 0.0000.292 0.089 847.00.300.175 0.000 105.15 10.77 180.0
Spike System with Response Time
3/25/2025 07:03 0.000249.2790.016 4.926 1.060497.455 2.259 1.474 7.1940.0842.628 1.196 247.3420.000 0.000 847.0249.872.592 9.883 249.28 0.22 180.0
3/25/2025 07:03 0.000249.5060.017 4.939 1.122498.116 2.257 1.600 7.2760.1321.650 1.192 247.7520.186 0.000 847.0250.292.613 9.893 249.51 0.02 180.0
3/25/2025 07:03 0.000250.1580.016 4.962 0.476498.847 2.243 1.420 6.9300.1512.709 1.161 247.8790.000 0.000 847.0250.302.475 9.912 250.16 0.02 180.0
Baseline System with Response Time
3/25/2025 07:06 0.0000.2120.011 0.084 0.0000.982 0.000 0.368 0.0000.0041.162 0.289 0.2760.000 0.014 847.00.500.000 0.001 0.21 0.00 180.0
3/25/2025 07:06 0.0000.2030.009 0.087 0.0000.823 0.000 0.113 0.1480.0001.600 0.108 0.1860.013 0.018 847.00.340.075 0.000 0.20 0.11 180.0
3/25/2025 07:07 0.0000.0820.011 0.086 0.0000.747 0.000 0.140 0.0000.0001.567 0.000 0.1710.064 0.006 847.00.230.074 0.000 0.08 0.00 180.0
Run 1 - A 30minute/60min
3/25/2025 07:53 0.00015.47517.311 10.109 85.55612.082 0.375 0.789 1.4310.0001.617 0.000 0.0000.650 0.360 847.01.020.456 0.000 15.48 0.04 180.0
3/25/2025 07:54 0.13215.78018.145 10.002 77.15711.232 0.294 0.521 2.1530.0001.164 0.000 0.0000.871 0.254 847.00.750.356 0.000 15.91 0.06 180.0
3/25/2025 07:55 0.00015.51818.364 9.982 86.15511.600 0.069 0.721 1.6080.0001.389 0.000 0.0000.563 0.292 847.00.940.530 0.000 15.52 0.05 180.0
3/25/2025 07:56 0.27916.02118.164 9.957 78.53311.179 0.205 0.334 2.3450.0001.674 0.225 0.0000.898 0.218 847.00.800.326 0.000 16.30 0.06 180.0
3/25/2025 07:57 0.45415.74018.232 9.971 71.51912.199 0.000 0.341 1.7770.0001.350 0.000 0.0000.860 0.193 847.00.650.396 0.000 16.19 0.05 180.0
3/25/2025 07:58 0.16615.77418.337 9.982 76.21512.179 0.019 0.330 2.2220.0001.643 0.157 0.0000.861 0.179 847.00.740.415 0.000 15.94 0.05 180.0
3/25/2025 07:59 0.26415.99418.405 9.985 69.88111.761 0.000 0.261 1.6750.0001.467 0.000 0.0000.788 0.173 847.00.610.393 0.000 16.26 0.05 180.0
3/25/2025 08:00 0.00015.72918.486 10.001 89.22711.138 0.075 0.432 1.7130.0001.625 0.000 0.0000.709 0.259 847.00.880.537 0.000 15.73 0.05 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/25/2025 08:01 0.19216.02818.508 9.994 74.51811.768 0.450 0.793 2.2020.0000.494 0.000 0.0000.848 0.204 847.00.720.461 0.000 16.22 0.06 180.0
3/25/2025 08:02 0.05816.37718.588 10.034 79.19412.236 0.689 1.277 2.1370.0000.491 0.000 0.0001.003 0.204 847.00.710.461 0.000 16.44 0.05 180.0
3/25/2025 08:03 0.00016.14218.628 10.034 89.84211.676 0.385 1.033 1.6620.0000.605 0.000 0.0000.630 0.262 847.00.890.554 0.000 16.14 0.05 180.0
3/25/2025 08:04 0.00016.12418.656 10.043 89.53511.366 0.213 0.712 1.7130.0000.562 0.000 0.0000.678 0.243 847.00.830.509 0.000 16.12 0.06 180.0
3/25/2025 08:05 0.00016.10718.651 10.030 84.69911.378 0.413 0.683 1.4910.0000.705 0.045 0.0000.702 0.253 847.00.870.499 0.000 16.11 0.06 180.0
3/25/2025 08:06 0.05216.11318.621 10.024 88.35711.345 0.209 0.879 1.6650.0000.442 0.000 0.0000.700 0.261 847.00.910.577 0.000 16.16 0.06 180.0
3/25/2025 08:07 0.00015.92318.610 10.023 83.98611.371 0.331 0.777 1.4420.0000.545 0.046 0.0000.669 0.240 847.00.920.612 0.000 15.92 0.06 180.0
3/25/2025 08:08 0.00016.20318.570 10.011 92.44111.384 0.171 0.897 1.8240.0000.681 0.000 0.0000.699 0.259 847.00.930.614 0.000 16.20 0.05 180.0
3/25/2025 08:09 0.00016.23618.501 10.025 88.96011.304 0.175 0.768 1.6020.0000.799 0.000 0.0000.630 0.254 847.00.890.568 0.000 16.24 0.06 180.0
3/25/2025 08:10 0.19616.10118.406 10.018 83.84511.165 0.061 0.762 1.4190.0000.655 0.000 0.0000.805 0.234 847.00.840.556 0.000 16.30 0.06 180.0
3/25/2025 08:11 0.00015.93518.354 10.011 89.52211.819 0.173 0.919 1.7060.0000.295 0.032 0.0000.664 0.239 847.00.830.502 0.000 15.93 0.05 180.0
3/25/2025 08:13 0.00016.09118.348 10.014 89.16111.796 0.230 1.127 1.7690.0000.709 0.000 0.0000.648 0.232 847.00.830.542 0.000 16.09 0.06 180.0
3/25/2025 08:14 0.00015.60218.365 10.019 93.88412.108 0.127 1.171 1.8970.0000.808 0.000 0.0000.683 0.254 847.00.890.575 0.000 15.60 0.06 180.0
3/25/2025 08:15 0.08715.72118.359 10.026 83.72311.419 0.082 0.864 1.4090.0000.742 0.276 0.0000.477 0.228 847.01.030.592 0.000 15.81 0.06 180.0
3/25/2025 08:16 0.00015.59018.368 10.025 93.34411.577 0.104 0.839 1.8680.0000.848 0.155 0.0000.691 0.243 847.00.970.571 0.000 15.59 0.05 180.0
3/25/2025 08:17 0.00016.11218.343 10.025 90.87411.577 0.173 0.725 1.7660.0000.601 0.182 0.0000.640 0.232 847.00.960.562 0.000 16.11 0.06 180.0
3/25/2025 08:18 0.00015.89018.349 10.024 86.07911.924 0.269 1.103 1.5330.0000.598 0.000 0.0000.908 0.249 847.00.830.500 0.000 15.89 0.06 180.0
3/25/2025 08:19 0.09115.75118.337 9.727 87.10112.677 0.231 1.318 1.7640.0001.062 0.800 0.0000.754 0.243 847.01.410.586 0.003 15.84 0.06 180.0
3/25/2025 08:20 0.00016.01218.318 9.614 95.32412.684 0.270 1.317 2.0990.0006.543 0.924 0.0000.668 0.210 847.01.480.659 0.011 16.01 0.06 180.0
3/25/2025 08:21 0.51740.41318.317 9.639 70.36210.904 1.736 1.053 2.0590.0004.794 1.239 0.0000.782 0.134 847.01.500.615 0.009 40.93 0.06 180.0
3/25/2025 08:22 1.37930.13118.349 9.619 11.1557.850 0.327 0.479 0.0430.0003.341 0.964 0.0000.846 0.151 847.01.180.357 0.010 31.51 0.05 180.0
3/25/2025 08:23 1.20615.33118.361 9.622 14.34718.214 0.000 0.421 0.0810.0005.200 1.223 0.0000.834 0.157 847.01.410.413 0.012 16.54 0.01 180.0
0.16917.19918.378 9.953 79.81711.764 0.262 0.788 1.6690.0001.448 0.209 0.0000.739 0.230 847.000.9410.510 0.002 17.368 0.054 180.0Avg.
Spike 1
3/25/2025 08:29 1.73333.16916.754 9.116 87.12378.135 2.029 12.359 2.7860.0000.000 3.533 21.2950.518 0.309 847.024.760.731 0.890 34.90 0.06 180.0
Run 1 - B 30minute/60min
3/25/2025 08:32 0.23615.76718.363 9.860 77.58614.253 0.585 2.721 2.4490.0000.227 0.286 0.0000.714 0.238 848.00.930.398 0.004 16.00 0.06 179.0
3/25/2025 08:33 0.66615.81718.386 9.986 76.05513.355 0.472 2.617 2.3080.0000.266 0.162 0.0000.801 0.216 848.00.910.547 0.000 16.48 0.05 180.0
3/25/2025 08:34 0.00015.88618.396 9.996 88.16314.237 0.762 3.002 1.5760.0000.442 0.145 0.0000.691 0.278 848.00.980.484 0.000 15.89 0.05 180.0
3/25/2025 08:35 0.16116.12818.369 10.001 73.22314.191 0.787 4.326 1.8410.0000.000 0.000 0.0000.848 0.217 848.00.740.466 0.000 16.29 0.06 180.0
3/25/2025 08:36 0.00015.56518.395 10.018 92.07213.967 0.414 2.883 1.8540.0000.000 0.108 0.0000.577 0.267 848.00.940.506 0.000 15.56 0.05 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/25/2025 08:37 0.00015.95518.401 10.040 91.23113.005 0.483 2.020 1.7230.0000.000 0.073 0.0000.684 0.285 848.01.000.565 0.000 15.95 0.06 180.0
3/25/2025 08:38 0.00015.84318.388 10.031 90.78612.539 0.310 1.665 1.6740.0000.000 0.000 0.0000.631 0.266 848.00.860.500 0.000 15.84 0.06 180.0
3/25/2025 08:39 0.00015.61018.373 10.020 90.02011.997 0.267 1.303 1.6570.0000.000 0.041 0.0000.597 0.264 848.00.910.532 0.000 15.61 0.06 180.0
3/25/2025 08:40 0.00015.88718.379 10.024 82.95912.959 0.206 1.939 1.3900.0000.000 0.016 0.0000.849 0.252 848.00.860.513 0.000 15.89 0.06 180.0
3/25/2025 08:41 0.00015.68218.376 10.018 92.90513.594 0.369 1.967 1.9560.0000.000 0.000 0.0000.627 0.276 848.00.910.533 0.000 15.68 0.05 180.0
3/25/2025 08:42 0.00015.90718.385 10.034 91.88313.074 0.504 2.138 1.8070.0000.000 0.000 0.0000.753 0.261 848.00.880.537 0.000 15.91 0.06 180.0
3/25/2025 08:43 0.00015.98418.393 10.027 85.77212.635 0.200 1.640 1.5020.0000.000 0.000 0.0000.661 0.255 848.00.880.550 0.000 15.98 0.06 180.0
3/25/2025 08:44 0.27915.88418.396 10.029 65.99912.834 0.055 1.930 1.7960.0000.000 0.000 0.0000.767 0.216 848.00.790.540 0.000 16.16 0.06 180.0
3/25/2025 08:45 0.56815.69318.407 10.015 74.99414.376 0.237 2.785 2.3660.0000.000 0.000 0.0000.836 0.222 848.00.800.536 0.000 16.26 0.04 180.0
3/25/2025 08:46 0.03016.09218.390 10.003 66.60514.881 0.334 2.526 2.0940.0000.000 0.000 0.0000.721 0.207 848.00.800.586 0.000 16.12 0.05 180.0
3/25/2025 08:47 0.00015.57118.383 9.993 79.32115.832 0.401 3.309 2.3580.0000.000 0.000 0.0000.972 0.221 848.00.810.559 0.000 15.57 0.50 180.0
3/25/2025 08:48 0.00015.44718.401 9.995 87.32813.800 0.446 2.350 1.5390.0000.000 0.038 0.0000.556 0.266 848.00.900.520 0.000 15.45 0.05 180.0
3/25/2025 08:49 0.00015.50218.404 9.997 78.31813.123 0.432 2.244 2.2220.0000.000 0.055 0.0000.641 0.224 848.00.870.572 0.000 15.50 0.06 180.0
3/25/2025 08:51 0.42615.73918.392 10.000 76.36413.727 0.486 3.177 2.3930.0000.000 0.000 0.0000.762 0.232 848.00.800.499 0.000 16.17 0.05 180.0
3/25/2025 08:52 0.00015.55518.394 10.015 85.98813.713 0.371 2.807 1.5830.0000.000 0.120 0.0000.607 0.273 848.01.010.582 0.000 15.55 0.05 180.0
3/25/2025 08:53 0.00015.79718.375 10.021 88.74813.127 0.243 2.032 1.7130.0000.000 0.000 0.0000.704 0.283 848.00.930.547 0.000 15.80 0.06 180.0
3/25/2025 08:54 0.00015.65818.380 10.047 91.62113.675 0.348 2.175 1.7590.0000.000 0.000 0.0000.646 0.293 848.00.940.536 0.000 15.66 0.06 180.0
3/25/2025 08:55 0.00016.08718.392 10.057 83.39912.393 0.344 1.594 1.3880.0000.000 0.000 0.0000.538 0.262 848.00.950.637 0.000 16.09 0.06 180.0
3/25/2025 08:56 0.00015.65218.399 10.048 89.57312.111 0.089 1.308 1.6170.0000.000 0.000 0.0000.799 0.265 848.01.000.709 0.000 15.65 0.05 180.0
3/25/2025 08:57 0.00016.09518.384 10.049 87.09211.957 0.203 1.221 1.5220.0000.000 0.000 0.0000.798 0.255 848.00.970.691 0.000 16.09 0.06 180.0
3/25/2025 08:58 0.00016.11418.385 10.051 89.12511.967 0.254 0.933 1.5710.0000.000 0.000 0.0000.807 0.265 848.00.920.579 0.000 16.11 0.06 180.0
3/25/2025 08:59 0.00016.04718.385 10.053 83.91411.872 0.284 1.397 1.3710.0000.000 0.000 0.0000.765 0.261 848.00.910.590 0.000 16.05 0.06 180.0
3/25/2025 09:00 0.00015.85318.382 10.042 88.09411.808 0.184 1.201 1.6050.0000.000 0.005 0.0000.818 0.271 848.00.920.561 0.000 15.85 0.05 180.0
3/25/2025 09:01 0.00015.74018.380 10.048 85.47011.800 0.066 1.229 1.3890.0000.000 0.000 0.0000.805 0.268 848.00.900.551 0.000 15.74 0.06 180.0
3/25/2025 09:02 0.54416.00918.389 10.031 70.67711.500 0.444 1.335 1.8770.0000.000 0.000 0.0000.700 0.206 848.00.680.402 0.000 16.55 0.06 180.0
0.09715.81918.387 10.018 83.51013.143 0.353 2.126 1.7970.0000.031 0.035 0.0000.723 0.252 848.000.8900.544 0.000 15.915 0.071 180.0Avg.
0.13316.50918.383 9.986 81.66312.454 0.307 1.457 1.7330.0000.740 0.122 0.0000.731 0.241 847.500.9150.527 0.001 16.641 0.062 180.0Run 1 Avg:
Baseline 1
3/25/2025 09:07 0.0000.0000.018 0.067 0.0280.910 0.000 0.184 0.0510.0001.314 0.000 0.0000.000 0.078 848.00.180.042 0.000 0.00 0.12 180.0
Run 2 - A 30minute/60min
3/25/2025 09:10 0.00015.25618.220 9.913 78.35711.433 0.095 1.721 2.0080.0000.000 0.000 0.0000.768 0.222 848.00.760.477 0.000 15.26 0.02 180.0
3/25/2025 09:11 0.00015.31018.355 9.985 73.57713.012 0.000 1.226 2.0040.0000.000 0.000 0.0000.970 0.209 848.00.790.558 0.000 15.31 0.05 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/25/2025 09:12 0.18415.52918.387 10.001 57.79811.691 0.262 1.829 1.3280.0000.000 0.000 0.0000.677 0.221 848.00.700.392 0.000 15.71 0.05 180.0
3/25/2025 09:13 0.40315.62418.405 10.025 77.49713.913 0.000 1.864 2.1890.0000.000 0.000 0.0000.716 0.216 848.00.740.468 0.000 16.03 0.28 180.0
3/25/2025 09:14 0.00015.62418.424 10.042 84.72016.244 0.634 3.523 1.6410.0000.000 0.159 0.0000.660 0.283 848.01.010.506 0.000 15.62 0.48 180.0
3/25/2025 09:15 0.00015.63018.432 10.036 82.75013.964 0.352 2.896 1.2730.0000.000 0.000 0.0000.847 0.275 848.00.970.623 0.000 15.63 0.06 180.0
3/25/2025 09:16 0.00015.80618.404 10.023 85.96713.393 0.211 2.186 1.4320.0000.000 0.055 0.0000.850 0.281 848.01.070.706 0.000 15.81 0.05 180.0
3/25/2025 09:17 0.00015.88618.410 10.027 83.89813.237 0.275 2.018 1.4630.0000.000 0.000 0.0000.786 0.277 848.01.020.702 0.000 15.89 0.06 180.0
3/25/2025 09:18 0.57915.86418.413 10.039 74.31812.717 0.318 1.957 2.0200.0000.000 0.000 0.0000.941 0.232 848.00.770.454 0.000 16.44 0.05 180.0
3/25/2025 09:19 0.05415.97218.412 10.045 74.30212.353 0.222 2.019 1.7330.0000.000 0.000 0.0000.826 0.228 847.00.750.442 0.000 16.03 0.05 180.0
3/25/2025 09:20 0.00015.64918.394 10.024 86.15612.689 0.167 1.882 1.4500.0000.000 0.026 0.0000.768 0.299 848.01.050.658 0.000 15.65 0.05 180.0
3/25/2025 09:21 0.00015.91318.418 10.053 84.41512.175 0.259 1.556 1.3810.0000.000 0.027 0.0000.775 0.285 847.00.950.551 0.000 15.91 0.06 180.0
3/25/2025 09:22 0.16215.97418.416 10.049 70.47313.095 0.009 1.408 1.5760.0000.000 0.000 0.0000.898 0.220 847.00.800.534 0.000 16.14 0.06 180.0
3/25/2025 09:23 0.00015.98218.418 10.040 82.58812.092 0.311 1.727 1.2540.0000.000 0.000 0.0000.820 0.286 847.01.030.691 0.000 15.98 0.05 180.0
3/25/2025 09:24 0.00016.01918.402 10.039 83.12913.055 0.284 2.277 1.3320.0000.000 0.000 0.0000.876 0.277 847.00.930.572 0.000 16.02 0.05 180.0
3/25/2025 09:26 0.00015.27018.428 10.037 83.89813.545 0.327 2.477 1.2610.0000.000 0.000 0.0000.806 0.293 847.00.900.467 0.000 15.27 0.05 180.0
3/25/2025 09:27 0.20146.26118.406 10.022 79.09211.475 1.607 1.904 2.5860.0000.000 0.065 0.0000.754 0.222 847.00.820.505 0.000 46.46 0.05 180.0
3/25/2025 09:28 0.00037.59218.439 10.036 11.8817.547 0.345 0.946 0.2090.0000.000 0.000 0.0000.627 0.164 847.00.410.121 0.000 37.59 0.17 180.0
3/25/2025 09:29 0.33015.08018.424 10.041 13.66716.498 0.000 0.500 0.1850.0000.000 0.000 0.0000.632 0.173 847.00.500.231 0.000 15.41 0.01 180.0
3/25/2025 09:30 0.90314.90118.429 10.033 37.70930.814 0.000 0.972 0.5010.0000.000 0.000 0.0000.693 0.191 847.00.630.367 0.000 15.80 0.01 180.0
3/25/2025 09:31 0.12815.66618.402 10.040 61.78325.724 0.000 1.805 1.2890.0000.000 0.000 0.0000.699 0.222 847.00.760.477 0.000 15.79 0.14 180.0
3/25/2025 09:32 0.02915.71918.420 10.046 69.43517.287 0.314 1.795 1.8270.0000.000 0.000 0.0000.653 0.233 847.00.790.480 0.000 15.75 0.04 180.0
3/25/2025 09:33 0.39315.72518.399 10.046 74.06613.576 0.503 1.921 1.9030.0000.000 0.000 0.0000.733 0.244 847.00.790.448 0.000 16.12 0.32 180.0
3/25/2025 09:34 0.00015.62718.390 10.053 73.00213.433 0.322 1.928 1.8870.0000.000 0.000 0.0000.718 0.260 847.00.800.419 0.000 15.63 0.05 180.0
3/25/2025 09:35 0.00015.89018.397 10.065 90.76814.178 0.618 2.737 2.1340.0000.000 0.019 0.0050.468 0.313 847.01.000.532 0.000 15.89 0.05 180.0
3/25/2025 09:36 0.00015.77918.413 10.076 85.16113.367 0.257 2.023 1.7480.0000.000 0.000 0.0000.424 0.300 847.00.970.553 0.000 15.78 0.06 180.0
3/25/2025 09:37 0.00015.33218.423 10.062 83.01912.087 0.340 1.455 1.4360.0000.000 0.000 0.0000.689 0.293 847.00.890.452 0.000 15.33 0.06 180.0
3/25/2025 09:38 0.00015.65318.427 10.069 71.41211.299 0.069 1.297 1.9190.0000.000 0.000 0.0000.670 0.247 847.00.750.385 0.000 15.65 0.05 180.0
3/25/2025 09:39 0.70415.27918.406 10.051 73.20211.442 0.105 1.358 1.9790.0000.000 0.000 0.0000.684 0.257 847.00.770.379 0.000 15.98 0.05 180.0
3/25/2025 09:40 0.55615.47218.406 10.044 73.65612.262 0.309 2.015 2.1240.0000.000 0.000 0.0000.713 0.263 847.00.800.406 0.000 16.03 0.05 180.0
0.15417.37618.404 10.035 72.05713.987 0.284 1.841 1.5690.0000.000 0.012 0.0000.738 0.250 847.330.8310.485 0.000 17.530 0.086 180.0Avg.
Spike 2
3/25/2025 09:45 3.84727.96116.822 9.606 86.54960.732 0.395 3.247 3.2720.0000.000 2.345 20.1630.428 0.363 847.022.610.231 0.849 31.81 0.04 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
3/25/2025 09:50 0.24115.41418.403 10.057 65.95315.328 0.000 1.503 1.5920.0000.000 0.000 0.0000.634 0.262 847.00.850.491 0.000 15.66 0.04 180.0
3/25/2025 09:51 0.39115.25818.406 10.049 79.44420.786 0.174 4.846 2.4190.0000.000 0.000 0.0000.669 0.303 847.00.860.380 0.000 15.65 0.04 180.0
3/25/2025 09:52 0.29615.49318.394 10.054 61.36214.864 0.547 3.310 1.6320.0000.000 0.000 0.0000.601 0.279 847.00.810.378 0.000 15.79 0.05 180.0
3/25/2025 09:53 0.00015.37718.376 10.035 97.76060.024 0.817 35.927 2.9700.0000.000 0.000 0.2320.376 0.350 847.01.260.494 0.001 15.38 0.04 180.0
3/25/2025 09:54 0.00015.65118.371 10.051 93.93922.534 0.848 7.210 2.3940.0000.000 0.239 0.1690.442 0.368 847.01.500.652 0.000 15.65 0.20 180.0
3/25/2025 09:55 0.33515.35018.398 10.063 75.09814.230 0.527 2.868 1.9570.0000.000 0.000 0.0000.747 0.274 847.00.800.384 0.000 15.69 0.06 180.0
3/25/2025 09:56 0.42615.59718.395 10.049 73.90713.540 0.600 2.604 2.1110.0000.000 0.000 0.0000.710 0.269 847.00.820.429 0.000 16.02 0.33 180.0
3/25/2025 09:57 0.63915.25618.423 10.062 67.62012.037 0.159 1.992 1.4700.0000.000 0.000 0.0000.639 0.256 847.00.760.369 0.000 15.89 0.05 180.0
3/25/2025 09:58 0.51415.15418.432 10.066 79.04212.116 0.217 1.469 2.0280.0000.000 0.000 0.0000.795 0.264 847.00.810.425 0.000 15.67 0.04 180.0
3/25/2025 09:59 0.00015.50618.421 10.065 86.41212.083 0.370 1.918 1.4990.0000.000 0.000 0.0000.625 0.309 847.01.000.576 0.000 15.51 0.05 180.0
3/25/2025 10:01 0.73015.42818.408 10.056 69.19612.359 0.325 2.193 1.7700.0000.000 0.000 0.0000.692 0.247 848.00.770.406 0.000 16.16 0.06 180.0
3/25/2025 10:02 0.92845.60518.403 10.044 45.5929.339 2.272 1.537 0.9830.0000.000 0.000 0.0000.661 0.235 848.00.710.356 0.000 46.53 0.15 180.0
3/25/2025 10:03 0.51915.86918.434 10.057 7.1187.174 0.000 0.868 0.0700.0000.000 0.000 0.0000.607 0.198 847.00.520.190 0.000 16.39 0.03 180.0
3/25/2025 10:04 0.50715.07618.418 10.047 27.14126.248 0.000 0.938 0.2370.0000.000 0.000 0.0000.639 0.213 847.00.640.316 0.000 15.58 0.00 180.0
3/25/2025 10:05 0.10315.29918.428 10.047 55.55627.853 0.000 2.942 1.0630.0000.000 0.000 0.0000.631 0.241 847.00.790.456 0.000 15.40 0.02 180.0
3/25/2025 10:06 0.80715.61418.427 10.037 63.69723.217 0.145 4.878 1.4700.0000.000 0.000 0.0000.652 0.252 847.00.760.383 0.000 16.42 0.15 180.0
3/25/2025 10:07 0.00015.24218.411 10.024 84.35617.484 0.241 2.898 1.6900.0000.000 0.023 0.0000.374 0.315 847.01.020.569 0.000 15.24 0.04 180.0
3/25/2025 10:08 0.50115.48518.416 10.040 70.99613.096 0.487 1.945 1.9690.0000.000 0.000 0.0000.690 0.271 847.00.850.467 0.000 15.99 0.43 180.0
3/25/2025 10:09 0.00015.21418.430 10.037 85.71012.740 0.526 1.676 1.6130.0000.000 0.000 0.0000.367 0.302 847.01.020.624 0.000 15.21 0.05 180.0
3/25/2025 10:10 0.68715.11618.468 10.045 58.82411.072 0.624 1.697 1.2740.0000.000 0.000 0.0000.691 0.236 847.00.720.378 0.000 15.80 0.06 180.0
3/25/2025 10:11 0.66415.03418.436 10.045 66.45410.963 0.054 1.100 1.3870.0000.000 0.000 0.0000.678 0.247 847.00.790.446 0.000 15.70 0.04 180.0
3/25/2025 10:12 0.57614.95418.439 10.021 79.04415.162 0.782 4.420 2.2120.0000.000 0.000 0.0000.747 0.279 847.00.830.404 0.000 15.53 0.32 180.0
3/25/2025 10:13 0.54815.25518.441 10.030 66.89912.305 0.556 2.462 1.6130.0000.000 0.000 0.0000.607 0.260 847.00.800.419 0.000 15.80 0.05 180.0
3/25/2025 10:14 0.40315.31018.434 10.004 75.83812.287 0.508 2.414 2.2430.0000.000 0.000 0.0000.708 0.263 847.00.760.352 0.000 15.71 0.04 180.0
3/25/2025 10:15 0.79614.95118.444 10.027 72.59614.158 0.000 2.068 1.8310.0000.000 0.000 0.0000.709 0.243 847.00.780.435 0.000 15.75 0.17 180.0
3/25/2025 10:16 0.45815.20218.436 9.995 74.80311.735 0.256 1.578 1.9820.0000.000 0.000 0.0000.757 0.259 847.00.810.434 0.000 15.66 0.05 180.0
3/25/2025 10:17 0.00015.41918.420 10.025 84.78711.473 0.214 1.193 1.3370.0000.000 0.000 0.0000.829 0.292 847.01.020.651 0.000 15.42 0.05 180.0
3/25/2025 10:18 0.43115.28318.404 10.022 70.53712.863 0.039 1.432 1.6830.0000.000 0.000 0.0000.675 0.244 848.00.770.424 0.000 15.71 0.06 180.0
3/25/2025 10:19 0.59115.45618.430 10.007 74.18011.163 0.162 1.363 1.9910.0000.000 0.000 0.0000.707 0.251 848.00.770.398 0.000 16.05 0.05 180.0
3/25/2025 10:20 0.60315.63818.402 10.028 73.19010.654 0.229 0.896 1.8750.0000.000 0.080 0.0000.669 0.241 848.00.860.489 0.000 16.24 0.05 180.0
0.42316.35018.418 10.040 69.56816.030 0.389 3.472 1.6790.0000.000 0.011 0.0130.644 0.267 847.170.8490.439 0.000 16.773 0.092 180.0Avg.
0.28916.86318.411 10.038 70.81215.008 0.337 2.656 1.6240.0000.000 0.012 0.0070.691 0.258 847.250.8400.462 0.000 17.152 0.089 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
3/25/2025 10:24 0.0000.0000.024 0.060 0.0000.921 0.000 0.079 0.0000.0002.310 0.000 0.0000.000 0.118 847.00.240.000 0.000 0.00 0.12 180.0
Run 3 - A 30minute/60min
3/25/2025 10:30 0.00015.37118.418 10.009 81.51714.267 0.603 3.388 1.2400.0000.000 0.134 0.0000.841 0.349 847.01.150.547 0.000 15.37 0.45 180.0
3/25/2025 10:31 0.45827.68718.425 9.986 74.20452.918 2.954 26.523 2.3490.0000.000 0.000 0.0000.698 0.332 847.00.930.397 0.001 28.15 0.05 180.0
3/25/2025 10:32 1.04420.34218.441 10.044 13.47035.526 0.175 5.753 0.0280.0000.000 0.000 0.0000.722 0.225 847.00.720.404 0.000 21.39 0.05 180.0
3/25/2025 10:33 0.37215.32518.436 10.054 49.84758.893 0.000 5.718 0.7050.0000.000 0.000 0.0000.764 0.263 847.00.860.493 0.000 15.70 0.01 180.0
3/25/2025 10:34 0.12615.76718.455 10.046 68.33925.087 0.764 4.741 1.6020.0000.000 0.000 0.0000.688 0.270 847.00.800.389 0.000 15.89 0.18 180.0
3/25/2025 10:36 0.51715.28318.462 10.044 75.37015.812 0.233 2.989 2.0760.0000.000 0.000 0.0000.845 0.284 847.00.900.497 0.000 15.80 0.04 180.0
3/25/2025 10:37 0.63515.43018.473 10.051 78.37413.115 0.278 1.989 2.2830.0000.000 0.018 0.0000.802 0.300 847.00.930.470 0.000 16.06 0.18 180.0
3/25/2025 10:38 0.00015.63518.459 10.064 82.62712.427 0.686 2.029 1.3520.0000.000 0.000 0.0000.743 0.343 847.01.090.609 0.000 15.64 0.24 180.0
3/25/2025 10:39 0.05515.59018.461 10.057 71.28311.648 0.512 1.779 1.5370.0000.000 0.000 0.0000.844 0.303 847.00.880.409 0.000 15.65 0.05 180.0
3/25/2025 10:40 0.00028.50018.460 10.049 78.36311.210 1.062 1.714 2.1730.0000.000 0.000 0.0000.692 0.283 847.00.860.435 0.000 28.50 0.05 180.0
3/25/2025 10:41 1.02665.22018.458 10.050 18.2496.851 1.394 1.147 0.1070.0000.000 0.000 0.0000.769 0.242 847.00.700.318 0.000 66.25 0.05 180.0
3/25/2025 10:42 0.98214.95818.466 10.052 15.40513.368 0.000 0.770 0.0000.0000.000 0.000 0.0000.691 0.229 847.00.670.318 0.000 15.94 0.01 180.0
3/25/2025 10:43 0.57614.85718.450 10.035 48.60228.350 0.000 0.965 0.3620.0000.000 0.000 0.0000.834 0.268 847.00.820.430 0.000 15.43 0.01 180.0
3/25/2025 10:44 0.10314.88918.471 10.038 66.19819.109 0.260 1.700 1.6990.0000.000 0.000 0.0000.682 0.265 847.00.840.465 0.000 14.99 0.18 180.0
3/25/2025 10:45 0.02714.99018.462 10.032 72.83713.839 0.311 1.624 2.0720.0000.000 0.000 0.0000.583 0.285 847.00.930.537 0.000 15.02 0.04 180.0
3/25/2025 10:46 0.00015.03818.455 10.020 82.88715.562 0.862 3.618 1.5680.0000.000 0.046 0.0000.615 0.344 847.01.070.530 0.000 15.04 0.34 180.0
3/25/2025 10:47 0.00015.14218.445 10.007 85.93815.842 0.457 3.911 2.1340.0000.018 0.000 0.0000.442 0.352 847.01.120.617 0.000 15.14 0.05 180.0
3/25/2025 10:48 0.65717.03718.418 10.003 71.16014.746 0.105 2.570 2.3950.0000.000 0.000 0.0000.620 0.299 847.00.950.525 0.000 17.69 0.16 179.0
3/25/2025 10:49 0.78515.36618.466 10.037 56.55314.898 0.970 3.678 1.8630.0000.000 0.000 0.0000.678 0.324 847.00.890.361 0.000 16.15 0.44 180.0
3/25/2025 10:50 0.00014.94218.462 10.049 86.00513.512 0.185 2.481 1.5480.0000.000 0.000 0.0000.624 0.367 847.01.130.593 0.000 14.94 0.20 180.0
3/25/2025 10:51 0.54115.37318.446 10.053 62.17112.567 0.729 2.666 1.9800.0000.000 0.000 0.0000.697 0.309 847.00.870.385 0.000 15.91 0.06 180.0
3/25/2025 10:52 0.40914.46118.491 10.061 63.86913.218 0.129 2.439 1.3930.0000.000 0.000 0.0000.692 0.287 847.00.810.355 0.000 14.87 0.34 180.0
3/25/2025 10:53 0.86515.50918.489 10.067 62.47615.703 0.998 4.431 1.5520.0000.000 0.000 0.0000.673 0.298 847.00.870.417 0.000 16.37 0.23 180.0
3/25/2025 10:54 0.18215.17118.491 10.063 65.97212.987 0.798 2.892 1.7240.0000.000 0.000 0.0000.662 0.298 847.00.900.454 0.000 15.35 0.35 180.0
3/25/2025 10:55 0.21015.31218.467 10.048 74.82411.478 0.044 1.543 1.9540.0000.000 0.000 0.0000.652 0.308 847.00.920.447 0.000 15.52 0.04 180.0
3/25/2025 10:56 0.00015.21818.474 10.045 72.21613.054 0.602 3.028 2.0290.0000.000 0.000 0.0000.787 0.333 847.00.940.418 0.000 15.22 0.05 180.0
3/25/2025 10:57 0.77415.25218.491 10.053 77.15612.215 0.271 2.265 2.2490.0000.000 0.000 0.0000.677 0.313 847.00.950.485 0.000 16.03 0.05 180.0
3/25/2025 10:58 0.00014.91718.481 10.039 82.72811.846 0.402 2.063 1.3050.0000.000 0.000 0.0000.677 0.368 847.01.110.561 0.000 14.92 0.05 180.0
3/25/2025 10:59 0.00915.16418.464 10.045 67.36812.975 0.000 1.586 1.6280.0000.000 0.000 0.0000.622 0.298 847.00.920.486 0.000 15.17 0.05 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/25/2025 11:00 0.00015.11518.482 10.054 88.65512.968 0.382 2.146 1.6930.0000.000 0.000 0.0000.568 0.376 847.01.120.554 0.000 15.11 0.19 180.0
0.34517.96218.461 10.042 66.48917.866 0.539 3.472 1.5530.0000.001 0.007 0.0000.696 0.304 847.000.9220.464 0.000 18.307 0.140 180.0Avg.
Spike 3
3/25/2025 11:04 5.14033.12016.886 9.592 56.16156.528 0.284 2.022 2.0210.0000.155 2.189 20.0650.599 0.466 847.022.490.047 0.846 38.26 0.05 180.0
Run 3 - B 30minute/60min
3/25/2025 11:07 0.69614.65718.475 10.024 75.35911.101 0.086 1.414 2.0470.0000.000 0.000 0.0000.632 0.314 847.00.980.534 0.000 15.35 0.05 180.0
3/25/2025 11:08 0.24014.97718.469 10.039 68.98611.219 0.047 1.342 1.8120.0000.000 0.000 0.0000.659 0.322 847.00.980.500 0.000 15.22 0.05 180.0
3/25/2025 11:09 0.16115.14618.473 10.047 73.40311.437 0.536 1.835 2.0510.0000.000 0.000 0.0000.743 0.329 847.00.950.445 0.000 15.31 0.05 180.0
3/25/2025 11:11 0.96014.89818.484 10.069 68.31512.730 0.000 1.958 1.8710.0000.000 0.000 0.0000.638 0.298 847.00.960.545 0.000 15.86 0.38 180.0
3/25/2025 11:12 0.03115.05618.481 10.060 76.33313.166 0.578 2.888 2.2650.0000.000 0.000 0.0000.769 0.340 847.01.000.485 0.000 15.09 0.43 180.0
3/25/2025 11:13 0.06515.10618.436 10.056 83.42411.991 0.359 1.940 1.4520.0000.000 0.000 0.0000.680 0.376 847.01.150.604 0.000 15.17 0.05 180.0
3/25/2025 11:14 0.37314.87918.434 10.065 77.00111.781 0.457 1.819 2.1080.0000.000 0.035 0.0000.783 0.330 847.00.990.463 0.000 15.25 0.05 180.0
3/25/2025 11:15 0.24715.13418.437 10.062 72.16011.533 0.353 1.770 2.0500.0000.000 0.000 0.0000.714 0.317 847.00.990.537 0.000 15.38 0.05 180.0
3/25/2025 11:16 0.00014.38918.455 10.045 78.63942.635 0.000 17.703 2.4540.0000.000 0.000 0.0000.730 0.351 847.01.070.553 0.000 14.39 0.05 180.0
3/25/2025 11:17 0.73315.03918.490 10.073 76.44329.340 0.526 9.443 2.5190.0000.000 0.061 0.0000.795 0.362 847.01.080.469 0.001 15.77 0.05 181.0
3/25/2025 11:18 0.00015.21018.455 10.052 85.41122.668 1.029 7.007 2.0090.0000.000 0.000 0.0000.436 0.403 847.01.240.651 0.000 15.21 0.19 180.0
3/25/2025 11:19 0.15614.82818.487 10.047 76.79614.894 0.970 3.608 2.3400.0000.000 0.000 0.0000.646 0.334 847.01.000.491 0.000 14.98 0.06 180.0
3/25/2025 11:20 0.44816.41418.447 10.046 66.85316.071 0.040 2.762 1.8480.0000.000 0.051 0.0000.802 0.309 847.01.020.551 0.000 16.86 0.05 180.0
3/25/2025 11:21 0.14016.64118.454 10.039 74.93413.563 0.592 2.841 2.3120.0000.000 0.028 0.0000.801 0.317 847.00.980.486 0.000 16.78 0.16 180.0
3/25/2025 11:22 0.25214.82718.438 10.040 75.80712.910 0.497 2.377 2.2090.0000.000 0.000 0.0000.670 0.321 847.00.980.513 0.000 15.08 0.48 180.0
3/25/2025 11:23 1.08175.52118.446 10.026 25.8257.085 3.578 1.876 0.4580.0000.000 0.000 0.0000.651 0.259 847.00.740.336 0.000 76.60 0.05 180.0
3/25/2025 11:24 1.21216.64618.474 10.051 6.7496.637 0.000 0.735 0.0000.0000.000 0.000 0.0000.760 0.254 847.00.720.313 0.000 17.86 0.02 180.0
3/25/2025 11:25 1.03315.96918.475 10.042 32.44225.338 0.000 0.799 0.5540.0000.000 0.000 0.0000.596 0.262 847.00.790.405 0.000 17.00 0.00 180.0
3/25/2025 11:26 0.48416.32118.446 10.021 69.18835.004 0.000 3.496 1.4800.0000.000 0.000 0.0000.766 0.306 847.00.910.443 0.000 16.80 0.02 180.0
3/25/2025 11:27 0.00016.35218.452 10.022 83.12424.080 0.021 2.943 1.4690.0000.000 0.000 0.0000.578 0.361 847.01.150.639 0.000 16.35 0.05 180.0
3/25/2025 11:28 0.41716.96218.451 10.041 60.72414.055 0.487 2.106 1.5430.0000.000 0.000 0.0000.782 0.303 847.00.900.446 0.000 17.38 0.05 180.0
3/25/2025 11:29 0.47714.47318.446 10.066 66.42812.741 0.296 2.198 1.7790.0000.000 0.081 0.0000.704 0.307 847.01.000.494 0.000 14.95 0.17 180.0
3/25/2025 11:30 0.00014.47818.448 10.075 84.97914.380 0.600 3.013 1.8160.0000.000 0.009 0.0000.633 0.394 847.01.170.557 0.000 14.48 0.04 180.0
3/25/2025 11:31 0.00015.04218.445 10.091 83.95913.592 0.608 2.973 1.6850.0000.000 0.000 0.0000.654 0.387 847.01.190.618 0.000 15.04 0.26 180.0
3/25/2025 11:32 0.15814.61418.420 10.070 76.37911.500 0.068 1.551 2.1480.0000.000 0.000 0.0000.764 0.316 847.01.000.547 0.000 14.77 0.35 180.0
3/25/2025 11:33 0.29514.41618.436 10.059 66.39012.328 0.025 1.074 1.6950.0000.000 0.000 0.0000.729 0.308 847.00.960.520 0.000 14.71 0.05 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/25/2025 11:34 0.00014.22618.440 10.060 89.80911.330 0.000 1.191 1.8600.0000.000 0.000 0.0000.751 0.370 847.01.180.654 0.000 14.23 0.04 180.0
3/25/2025 11:35 0.16614.55618.445 10.063 76.27511.305 0.106 1.150 2.2120.0000.000 0.000 0.0000.771 0.327 847.00.990.499 0.000 14.72 0.18 180.0
3/25/2025 11:36 0.42314.49718.515 10.092 66.67210.543 0.099 1.184 1.6380.0000.000 0.000 0.0000.767 0.307 847.00.930.472 0.000 14.92 0.05 181.0
3/25/2025 11:37 0.26914.68518.449 10.048 68.06011.629 0.290 1.958 1.7310.0000.000 0.000 0.0000.734 0.304 847.00.900.443 0.000 14.95 0.04 180.0
0.35117.19918.457 10.053 69.56215.620 0.408 2.965 1.7810.0000.000 0.009 0.0000.705 0.326 847.000.9970.507 0.000 17.549 0.117 180.1Avg.
0.34817.58018.459 10.047 68.02616.743 0.474 3.218 1.6670.0000.000 0.008 0.0000.700 0.315 847.000.9590.485 0.000 17.928 0.129 180.0Run 3 Avg:
Baseline 3
3/25/2025 11:41 0.0000.0000.027 0.077 0.0000.822 0.000 0.220 0.0000.0001.411 0.000 0.0000.000 0.194 847.00.390.000 0.000 0.00 0.11 180.0
Post CTS
3/25/2025 11:43 0.0000.0000.031 0.071 0.0000.696 0.000 0.612 0.0000.0000.000 99.882 0.0000.000 0.240 847.067.180.156 0.000 0.00 0.07 180.0
3/25/2025 11:44 0.0000.0000.033 0.097 0.0000.797 0.000 0.331 0.0000.0000.000 99.918 0.0110.000 0.227 847.067.080.000 0.000 0.00 0.06 180.0
3/25/2025 11:44 0.0000.0000.030 0.059 0.0000.771 0.000 0.000 0.0000.0000.000 98.902 0.0000.000 0.245 847.066.470.065 0.000 0.00 0.06 180.0
Post NO2/Mid O2
3/25/2025 11:47 102.2870.0000.012 0.078 0.1700.899 0.837 0.005 0.5380.0000.496 0.000 0.0000.133 0.256 847.00.720.306 0.000 102.29 10.84 180.0
3/25/2025 11:47 102.6780.0000.016 0.089 0.0000.942 0.845 0.350 0.0000.0000.234 0.000 0.0000.451 0.177 847.00.540.274 0.000 102.68 10.76 180.0
3/25/2025 11:48 102.9720.0000.015 0.086 0.2770.992 0.834 0.286 0.3370.0000.000 0.000 0.0000.053 0.239 847.00.860.577 0.000 102.97 10.79 180.0
Post 5-Gas
3/25/2025 11:50 0.000248.7680.021 4.983 3.431497.905 2.150 1.306 7.2000.1681.765 1.190 248.5800.000 0.000 847.0251.102.590 9.918 248.77 0.02 180.0
3/25/2025 11:50 0.000247.4370.017 4.945 1.497497.750 2.105 1.245 7.2560.1321.013 1.068 248.7510.000 0.000 847.0251.252.678 9.937 247.44 0.02 180.0
3/25/2025 11:50 0.000248.6890.014 4.936 1.223500.101 2.139 2.177 9.9550.0632.712 1.270 249.3360.000 0.000 847.0251.902.578 9.875 248.69 0.02 180.0
3/25/2025 11:50 0.000247.9970.019 4.947 1.560499.049 2.116 1.706 7.2230.0361.959 1.078 248.7170.000 0.000 847.0251.112.519 9.929 248.00 0.02 180.0
End of Test Purge
3/25/2025 11:52 0.0000.0000.014 0.097 0.0002.564 0.000 0.502 0.0000.0101.404 0.000 0.6600.178 0.201 847.01.060.000 0.026 0.00 0.00 180.0
3/25/2025 11:52 0.0000.0000.014 0.099 0.0751.881 0.000 0.053 0.0000.0000.689 0.000 0.6600.000 0.144 847.00.960.024 0.016 0.00 0.11 180.0
3/25/2025 11:52 0.0000.0000.009 0.079 0.0001.569 0.000 0.183 0.0290.0000.822 0.042 0.5470.027 0.144 847.00.860.000 0.007 0.00 0.00 180.0
3/25/2025 11:52 0.0000.0000.018 0.092 0.0201.664 0.000 0.233 0.0000.0001.311 0.000 0.3200.000 0.209 847.00.740.000 0.004 0.00 0.00 180.0
3/25/2025 11:52 0.0000.0000.012 0.102 0.0651.357 0.000 0.000 0.3380.0201.533 0.000 0.3430.170 0.146 847.00.640.000 0.015 0.00 0.00 180.0
3/25/2025 11:52 0.0000.0000.016 0.082 0.0001.274 0.000 0.095 0.0000.0001.308 0.000 0.1340.000 0.219 847.00.570.000 0.008 0.00 0.00 180.0
3/25/2025 11:52 0.0000.0000.014 0.070 0.0001.220 0.000 0.194 0.0000.0000.415 0.000 0.0670.046 0.261 847.00.650.084 0.005 0.00 0.00 180.0
3/25/2025 11:52 0.0000.0000.010 0.074 0.0001.139 0.000 0.172 0.0040.0001.175 0.202 0.3570.000 0.156 847.00.800.000 0.000 0.00 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 3/26/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:07:27 AM 11:35 AM
Source:
Unit Number: 1352
Serial Number: 1651154
Engine Hours:11354
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.083 0.242 0.014
8.478 15.056 0.939
2.000 0.300 1.000 0.150 0.700 0.030
0.016 0.048 0.003
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
LYNN HUBER
3
Cody Hall
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
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Site Verification Photos
GAS
Unit 1352 with a serial number of 1651154 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 3/26/2025 by
Cody Hall with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were
within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2300 BHP and 1199 RPM which is 92.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1352 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1352Unit ID
Make Waukesha Site Elevation ft.5246
Model 9394 GSI Atmospheric Pressure psi.12.04
Serial Number 1651154 Stack Diameter in.18
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2300 2300 2300 2300
1199 1200 1199 1199
Percent Load %
Intake Manifold Pressure (hg)
92.00%92.00%92.00%92.00%
104.98 104.16 104.57 104.57
Intake Manifold Temperature (F)118.00 118.00 118.00 118.00
Ambient Conditions
Ambient Temperature Dry (F)36.00 42.00 53.00 43.67
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
136023.78 134890.00 133428.33 134780.70
3851.73 3819.62 3778.23 3816.53
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %18.30%18.33%18.36%18.33%
T
e
s
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S
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m
m
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mfg. rated rpm
Test RPM
0.19%0.15%0.16%0.17%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
07:27 AM 08:59 AM 10:14 AM 3/26/2025
State
NOx (mol wt) 46.01
0.770 0.742 0.789 0.767NMNEHC (ppmvw)
0.942 0.908 0.966 0.939NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
268.482 258.370 274.699 267.184 FailNMNEHC (ppbvd) @15% O2
0.003 0.003 0.003 0.0030.700 0.030 PassNMNEHC (g/hp-hr)
0.015 0.014 0.015 0.0140.170 PassNMNEHC (lbs/hr)
0.268 0.258 0.275 0.267 FailNMNEHC (ppmvd) @15% O2
0.0160.016CO (g/hp-hr)0.018 0.0162.000 0.300 Pass
CO (ppmvw)7.446 6.702 6.626 6.925
CO (ppmvd)9.113 8.206 8.116 8.478
CO (mol wt) 28.01
CO (ppmvd) @15% O2 2.596 2.334 2.308 2.413 Fail
CO (ppbvd) @15% O2 2596.260 2333.685 2308.206 2412.717 Fail
0.0790.080CO (lbs/hr)0.090 0.0831.650 Pass
NOx (g/hp-hr)0.049 0.047 0.047 0.0481.000 0.150 Pass
NOx (ppmvw)12.580 12.029 12.282 12.297
NOx (ppmvd)15.396 14.727 15.044 15.056
NOx (ppbvd) @15% O2 4386.201 4188.411 4278.656 4284.423 Fail
NOx (ppmvd) @15% O2 4.386 4.188 4.279 4.284 Fail
NOx (lbs/hr)0.250 0.237 0.240 0.2420.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
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6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
7.45
0.25
12.10 0.48 12.58
0.00%
0.15%
0.00%
18.30%
12.18 0.51 0.17%18.29%
32.64 5.07 0.03%16.63%
12.03 0.44 0.14%18.30%
0.00 0.00 0.00 0.00%0.03%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.87 0.00 0.00 0.00 0.00%0.03%
6.51 11.20 0.41 11.60 0.15%18.28%
53.53 21.68 11.53 33.21 0.14%16.67%
6.90 11.89 0.57 12.46 0.10%18.37%
0.58 0.00 0.00 0.00 0.00%0.04%
Avg. Wet 6.70 11.54 0.49 12.03 0.74 0.12%18.33%
NO2NO
0.27
0.76
23.45
0.72
0.26
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
6.52 11.65 0.44 12.09 0.12%18.38%
53.02 24.98 11.14 36.12 0.04%16.73%
6.73 11.84 0.64 12.48 0.13%18.34%
0.97 0.17 0.00 0.17 0.00%0.03%
0.58 0.00 0.00 0.00 0.26 0.00%0.04%
Avg. Wet 6.63 11.75 0.54 12.28 0.79 0.12%18.36%
NO2NO
0.39
0.79
23.36
0.78
NMNEHC
1.17
NO2
0.001.15
0.77
23.99
0.77
0.27
0.77
0.25
12.70
37.72
12.46
7.37
7.53
0.87
56.26
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =18 Inches or:1.5 feet or:1.77 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.44
Yes
18.00
14.00
12.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%18.30
29.95
0.40
Inches
3.01
9
14.99
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
12.14
0.13
0.00
1020.32
0.03
30.14
30.17
956.00
1415.67
513.33
27.76
69.59
122.97
166483.62
136023.78
Run 2
18.33
29.95
0.40
12.14
0.16
0.00
1019.98
0.03
30.13
30.16
967.00
1426.67
519.44
27.76
70.26
122.97
165154.58
134890.00
Run 3
18.36
29.95
0.40
12.15
0.16
0.00
1017.95
0.03
30.07
30.10
979.13
1438.80
526.18
27.76
69.86
122.97
163437.00
133428.33
18.33
29.95
0.40
12.14
0.15
0.00
1019.42
0.03
30.11
30.14
967.38
1427.05
519.65
27.76
69.91
122.97
165025.06
134780.7
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.35
Exhaust Temp F
956.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.31
0.33
0.39
956.00
956.00
957.00
0.42
0.45
0.47
957.00
957.00
955.00
0.40
0.33
0.33
955.00
955.00
956.00
0.38 956.00
0.45
0.42
0.44
956.00
955.00
955.00
0.44
0.42
0.40
955.00
959.00
956.00
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.38
Exhaust Temp F
979.00
0.33
0.39
0.44
979.00
979.00
980.00
0.44
0.41
0.46
980.00
980.00
978.00
0.44
0.40
0.35
978.00
978.00
979.00
0.37 979.00
0.38
0.33
0.36
979.00
980.00
980.00
0.41
0.44
980.00
978.00
979.130.40
Run 2
Δpstd (in) H2O
0.49
Exhaust Temp F
967.00
0.44
0.45
0.42
967.00
967.00
966.00
0.38
0.33
0.37
966.00
966.00
968.00
0.39
0.34
0.43
968.00
968.00
967.00
0.44 967.00
0.48
0.42
0.35
967.00
966.00
966.00
0.37
0.37
966.00
970.00
0.40 967.00
Pass
Strat Check
13.01Check 1
13.15Check 2
12.88Check 3
NoxGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(12.137)+ .32(.129)+ .28(87.733+.001) = 29.95 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.95(1 -.18296)+ 18.0(.18296) = 27.76 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.4*√(1415.67/(30.17*27.76)) = 69.59 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.18296)69.59*1.767((528*30.17)/ (1415.67*29.92)) = 136023.78 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 136023.777/35.315 = 3851.728 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 9.113*(20.9-15)/(20.9-.19%)) = 2.596 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(9.113*(1.164*10^-3)*3851.728*(Run Time/60))/2300 = .018 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .018*1/453.6*2300 = .09 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .09*4.38 = .394 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
9.11 = 7.446*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.89%
21.43%
10.87%
10.95%
10.71%
10.71%
10.95%10.87%
10.89%
21.43%
10.71%
21.15%
10.71%
21.15%
10.71%21.15%
0.00%
10.71%
21.15%
0.18%
0.28%
0.87%
1.31%
10.71%
Span
Zero Offset 0.00%
21.15
0.00%
10.89%0.11%0.27%0.00%
0.19%
0.16%
0.16%
0.19%
0.15%
0.16%
9
GAS
0.0 0.0 0.0
0.0 0.0 0.0
0.0
0.0
0.7 0.7 .7
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
3/26/2025
5246
1352
Waukesha
Model
Serial Number
9394 GSI
1651154
Technician Cody Hall
Run Start Times 07:27 AM 08:59 AM 10:14 AM 11:35 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1199.0 1200.0 1199.0 1199.3
Engine Hours 11351 11352 11353 11354
Intake Manifold Pressure (psi)63.6 63.2 63.4 63.4
Intake Manifold Temp °F 118.0 118.0 118.0 118.0
Engine Load (BHP)2300.0 2300.0 2300.0 2300.0
Ambient Temp °F 36.0 42.0 53.0 43.7
Humidity %72.0 60.0 37.0 56.3
Dew Point °F 27.0 29.0 27.0 27.7
Waukesha
N/A
N/A
Yes
N/A N/A N/A N/A
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
0.7Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.01
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.09
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 98.62
Tolerance 2.00%
Difference between measured and expected 1.38%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.83
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 1.16
Average:Oxygen 0.12
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 99.91
Tolerance 5.00%
Difference between measured and expected 0.09%
Pre-test System CTS & Mechanical Response Time
52 secondsEquilibration Response Time
Value:Spike Reported 249.66
Value:Spike Expected 251.20
System (Equilibration) Response Time Target (Spike)
86 secondsSystem Zero Response Time
86 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC524646 12/30/2027 104.20 10.71%
CC312964 10/17/2032 100.00
CC337712 5/1/2032 21.15%
Cylinder # CC230781 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 251.20 501.50 251.30 10.03
Analyzer System Response 249.66 496.39 248.37 9.93
Percent Difference 0.61%1.02%1.17%1.05%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.616 4.931
Spike Direct
Propane 252.029
Mechanical
Response Time
SF6 9.988
CO 501.768
NO 250.183
Ethylene 99.907 11 seconds
Analyzer
Response
Propane 249.663
SF6 9.925
CO 496.389
NO 248.366
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 249.863
CO 495.921
NO 249.003
52 seconds
86 seconds
9.00%
8.74%
8.62%
95.41%
94.86%
95.40%
9.904
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.006
50%9.000
83.3%14.994
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
18
14
12
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
134780.7
H2O%d @ Sampling Point:18.33
CO2%d @ Sampling Point:12.14
Pressure @ Sampling Point (Pg "H2O):0.4
Temperature @ Sampling Point (Deg F):967.38
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 100 98.62 4.931 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.616 4.931
Spike Direct
Propane 252.029
Mechanical
Response Time
SF6 9.988
CO 501.768
NO 250.183
Ethylene 99.907 11 seconds
Analyzer
Response
Propane 249.663
SF6 9.925
CO 496.389
NO 248.366
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 249.863
CO 495.921
NO 249.003
52 seconds
86 seconds
9.00%
8.74%
8.62%
95.41%
94.86%
95.40%
9.904
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
251.200
10.030
501.500
251.300
252.029
9.988
501.768
250.183
0.33%
0.42%
0.05%
0.44%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
21.570
0.899
Dilution Factor
9.001%
Expected
22.608
% Recovery
95.410%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.873
Dilution Factor
8.740%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.861
Dilution Factor
8.620%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 20.657 21.653 95.400%
0.000125
0.000143
0.000133
0.000 20.827 21.955 94.860%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass1.43%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-2.22141099 Pass
Line Position Difference:Resolution Difference to Reference 1.43%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
100.00
99.77
0.23%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1352; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
3/26/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
3/26/2025
Cody Hall
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 18S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Cody Hall
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1352
Make:Waukesha
Location:9394 GSIModel:
1651154Serial Number:
RAW Result Data
Stability
3/26/2025 06:12 0.0330.2030.001 0.084 0.0000.000 0.000 0.121 0.0170.0020.000 0.003 0.0100.000 0.017 847.00.040.000 0.000 0.24 0.15 181.0
Pre Test Baseline Direct
3/26/2025 06:23 0.0000.0040.001 0.014 0.0000.000 0.007 0.000 0.0000.0000.582 0.120 0.0000.000 0.000 847.00.100.036 0.000 0.00 0.00 180.0
3/26/2025 06:24 0.0000.0000.001 0.008 0.0220.038 0.004 0.000 0.0250.0000.723 0.028 0.0160.062 0.005 847.00.050.000 0.005 0.00 0.00 180.0
3/26/2025 06:24 0.0000.000-0.000 0.000 0.0000.001 0.000 0.025 0.0120.0000.657 0.164 0.0000.148 0.002 846.00.110.000 0.000 0.00 0.00 180.0
CTS Direct
3/26/2025 06:31 0.0000.3010.013 0.005 0.0000.000 0.001 0.194 0.0000.0570.000 98.608 0.0110.000 0.016 843.065.810.035 0.000 0.30 0.06 180.0
3/26/2025 06:32 0.0000.0000.013 0.008 0.0000.000 0.003 0.030 0.0010.0000.000 98.514 0.0040.075 0.015 843.065.710.000 0.000 0.00 0.06 180.0
3/26/2025 06:32 0.1270.0290.013 0.011 0.0000.000 0.008 0.076 0.0870.0000.000 98.726 0.0510.000 0.034 843.065.940.003 0.000 0.16 0.06 181.0
High O2 Direct
3/26/2025 06:38 0.0000.1250.003 0.000 0.0770.096 0.014 0.050 0.0270.0001.035 0.261 0.0190.015 0.008 843.00.220.018 0.000 0.13 21.42 180.0
3/26/2025 06:39 0.0000.2600.003 0.000 0.0490.104 0.015 0.000 0.0000.0761.021 0.190 0.0000.000 0.000 843.00.160.048 0.000 0.26 21.43 180.0
3/26/2025 06:39 0.0000.0000.003 0.000 0.1070.149 0.017 0.000 0.0000.0002.021 0.146 0.0000.007 0.000 843.00.120.038 0.000 0.00 21.43 180.0
NO2/Mid O2 Direct
3/26/2025 06:48 104.6920.4300.002 0.000 0.5500.000 0.972 0.000 1.5590.0000.530 0.000 0.0000.000 0.000 844.00.000.000 0.000 105.12 10.89 180.0
3/26/2025 06:48 102.8960.3890.002 0.000 0.3890.000 0.980 0.000 1.4250.0000.378 0.000 0.0000.086 0.000 844.00.000.000 0.000 103.29 10.90 180.0
3/26/2025 06:49 103.8750.5200.001 0.000 0.3060.000 0.967 0.000 1.3670.0000.385 0.000 0.0000.000 0.000 844.00.000.000 0.000 104.39 10.89 180.0
Spike Direct
3/26/2025 06:54 0.000250.0530.006 4.769 5.052502.072 2.259 0.976 10.2030.2383.725 1.061 252.0890.000 0.000 844.0254.522.593 9.990 250.05 0.02 180.0
3/26/2025 06:54 0.000250.3130.005 4.718 1.670501.690 2.278 1.102 10.4360.2934.790 1.091 251.9380.000 0.000 844.0254.432.645 9.986 250.31 0.02 180.0
3/26/2025 06:54 0.000250.1820.006 4.685 1.769501.543 2.261 1.162 10.2440.3785.632 1.078 252.0610.000 0.000 844.0254.542.638 9.987 250.18 0.02 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
3/26/2025 06:57 0.0000.0000.019 0.000 0.0130.863 0.004 0.000 0.0000.00014.686 1.318 0.0000.000 0.108 844.01.130.046 0.000 0.00 0.13 180.0
3/26/2025 06:58 0.0000.0000.018 0.000 0.0000.815 0.017 0.000 0.0000.00114.906 1.490 0.0000.000 0.104 844.01.230.036 0.000 0.00 0.12 180.0
3/26/2025 06:58 0.0000.0000.017 0.000 0.0000.807 0.020 0.021 0.0000.00015.148 1.318 0.0000.000 0.095 844.01.120.068 0.000 0.00 0.12 180.0
CTS System with Response Time
3/26/2025 07:00 0.0000.0000.029 0.000 0.0000.856 0.034 0.347 0.0000.00016.761 100.194 0.0000.000 0.101 844.067.010.010 0.000 0.00 0.06 180.0
3/26/2025 07:00 0.0000.0000.027 0.000 0.0000.871 0.042 0.299 0.0000.00016.701 99.740 0.0000.000 0.105 844.066.760.086 0.000 0.00 0.07 180.0
3/26/2025 07:01 0.0000.0000.028 0.000 0.0000.882 0.038 0.291 0.0000.00016.739 99.787 0.0000.000 0.101 844.066.760.046 0.000 0.00 0.07 180.0
NO2/Mid O2 System with Response Time
3/26/2025 07:02 100.0402.2690.015 0.000 0.0530.894 0.996 0.000 0.5580.0004.035 1.049 0.0000.000 0.163 844.01.140.172 0.000 102.31 10.85 180.0
3/26/2025 07:03 100.2012.1360.016 0.000 0.0000.811 0.997 0.000 0.5540.0003.705 1.112 0.0000.000 0.165 844.01.210.205 0.000 102.34 10.87 180.0
3/26/2025 07:03 100.8882.0240.015 0.000 0.0000.843 1.001 0.000 0.5440.0004.537 1.114 0.0000.019 0.158 844.01.160.160 0.000 102.91 10.89 180.0
Spike System with Response Time
3/26/2025 07:05 0.000247.8110.019 4.367 1.098495.844 2.228 1.376 7.4270.13612.070 1.205 249.4560.021 0.000 844.0252.162.854 9.927 247.81 0.02 180.0
3/26/2025 07:05 0.000248.3910.019 4.428 1.337496.186 2.263 1.482 7.2480.10810.755 1.264 249.6920.000 0.000 844.0252.222.526 9.917 248.39 0.02 180.0
3/26/2025 07:06 0.000248.8950.017 4.466 0.649497.138 2.241 1.439 7.1410.1359.987 1.212 249.8410.000 0.000 844.0252.462.713 9.930 248.90 0.15 180.0
Baseline System with Response Time
3/26/2025 07:09 0.0000.3560.012 0.000 0.0001.259 0.077 0.000 0.2740.00012.048 1.188 0.2510.000 0.107 844.01.380.187 0.007 0.36 0.00 180.0
3/26/2025 07:09 0.0000.3830.012 0.000 0.0111.164 0.056 0.000 0.0740.00012.121 0.896 0.2910.000 0.013 844.01.010.149 0.010 0.38 0.00 180.0
3/26/2025 07:09 0.0000.0000.011 0.000 0.0001.022 0.050 0.000 0.1510.00011.949 1.232 0.1970.000 0.016 844.01.130.126 0.002 0.00 0.00 180.0
Run 1 - A 30minute/60min
3/26/2025 07:28 0.65611.46818.164 9.780 47.9346.701 0.000 0.397 0.4200.0000.000 0.000 0.0000.917 0.249 844.00.770.404 0.000 12.12 0.22 180.0
3/26/2025 07:29 0.50313.25118.237 9.782 44.6816.392 0.000 0.228 0.8530.0000.000 0.000 0.0000.858 0.260 844.00.690.249 0.000 13.75 0.20 180.0
3/26/2025 07:30 0.6449.98318.276 9.778 50.3166.630 0.000 0.052 0.2610.0000.000 0.000 0.0000.928 0.180 844.00.600.360 0.000 10.63 0.18 179.0
3/26/2025 07:31 0.11011.37518.208 9.785 59.1526.995 0.000 0.000 0.6610.0000.000 0.000 0.0000.894 0.207 844.00.750.504 0.000 11.49 0.18 179.0
3/26/2025 07:32 0.40313.21918.234 9.846 52.6516.925 0.000 0.000 0.7130.0000.000 0.000 0.0000.876 0.226 844.00.750.441 0.000 13.62 0.19 180.0
3/26/2025 07:33 0.44012.70918.238 9.880 53.2007.004 0.000 0.000 0.5880.0000.000 0.000 0.0000.853 0.231 844.00.730.407 0.000 13.15 0.19 180.0
3/26/2025 07:34 0.64211.08218.243 9.891 52.9037.155 0.000 0.000 0.6240.0000.000 0.000 0.0000.716 0.232 844.00.700.359 0.000 11.72 0.19 180.0
3/26/2025 07:35 0.61911.22818.222 9.913 48.2117.080 0.000 0.000 0.6040.0000.000 0.000 0.0000.799 0.225 844.00.740.437 0.000 11.85 0.19 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/26/2025 07:36 0.66211.30118.324 9.971 55.7828.288 0.000 0.000 0.7200.0000.000 0.000 0.0000.957 0.253 843.00.700.288 0.000 11.96 0.17 181.0
3/26/2025 07:37 0.60511.37218.372 9.993 61.4308.595 0.000 0.000 0.9010.0000.000 0.000 0.0000.955 0.256 843.00.720.313 0.000 11.98 0.18 181.0
3/26/2025 07:38 0.74311.40218.368 9.985 50.8298.270 0.000 0.000 0.6460.0000.000 0.000 0.0000.857 0.228 843.00.790.502 0.000 12.14 0.18 181.0
3/26/2025 07:39 1.09913.41818.348 9.959 40.2947.015 0.000 0.000 0.3080.0000.000 0.000 0.0000.855 0.232 843.00.760.437 0.000 14.52 0.17 180.0
3/26/2025 07:40 0.61312.76418.381 9.975 55.8437.924 0.000 0.000 0.7560.0000.000 0.000 0.0000.708 0.234 843.00.820.535 0.000 13.38 0.16 181.0
3/26/2025 07:41 0.84713.29918.314 9.929 44.9847.706 0.000 0.096 0.6740.0000.000 0.000 0.0000.805 0.233 844.00.790.487 0.000 14.15 0.17 180.0
3/26/2025 07:42 0.62112.70618.327 9.907 59.7637.346 0.000 0.003 1.2060.0000.000 0.000 0.0000.728 0.238 844.00.860.580 0.000 13.33 0.16 180.0
3/26/2025 07:44 0.60412.21118.315 9.885 53.0217.186 0.000 0.000 0.8970.0000.000 0.000 0.0000.854 0.208 844.00.780.542 0.000 12.82 0.17 180.0
3/26/2025 07:45 0.77212.39118.329 9.876 45.7407.021 0.000 0.048 0.6570.0000.000 0.000 0.0000.850 0.219 844.00.760.484 0.000 13.16 0.15 180.0
3/26/2025 07:46 0.74212.28818.299 9.877 54.4407.096 0.000 0.000 1.0190.0000.000 0.000 0.0000.812 0.216 844.00.910.721 0.000 13.03 0.16 180.0
3/26/2025 07:47 0.26612.00818.301 9.864 51.5707.046 0.000 0.000 0.9210.0000.000 0.000 0.0000.809 0.216 844.00.800.551 0.000 12.27 0.15 180.0
3/26/2025 07:48 0.18112.05818.317 9.881 50.0707.031 0.000 0.041 0.8520.0000.000 0.000 0.0000.825 0.202 844.00.810.610 0.000 12.24 0.16 180.0
3/26/2025 07:49 0.67912.32918.316 9.882 49.4267.010 0.000 0.004 0.8400.0000.000 0.000 0.0000.885 0.210 844.00.780.539 0.000 13.01 0.16 180.0
3/26/2025 07:50 0.09012.34418.302 9.894 55.7417.156 0.000 0.134 0.6440.0000.000 0.000 0.0000.781 0.236 844.00.700.337 0.000 12.43 0.16 180.0
3/26/2025 07:51 0.72312.43018.302 9.895 49.1677.184 0.000 0.002 0.8560.0000.000 0.000 0.0000.797 0.222 844.00.850.602 0.000 13.15 0.17 180.0
3/26/2025 07:52 0.11212.32818.292 9.913 58.8847.415 0.000 0.008 1.2180.0000.000 0.000 0.0000.905 0.225 844.00.810.541 0.000 12.44 0.15 180.0
3/26/2025 07:53 0.68412.19518.301 9.923 61.7057.648 0.000 0.000 0.9470.0000.000 0.000 0.0000.808 0.227 844.00.820.549 0.000 12.88 0.16 180.0
3/26/2025 07:54 0.08312.69018.288 9.927 58.0858.983 0.000 0.164 1.2130.0000.000 0.000 0.0000.843 0.234 844.00.750.418 0.000 12.77 0.16 180.0
3/26/2025 07:55 0.05612.49618.296 9.924 51.7127.524 0.000 0.106 0.8500.0000.000 0.000 0.0000.921 0.241 844.00.790.467 0.000 12.55 0.17 180.0
3/26/2025 07:56 0.22612.47718.294 9.931 52.8617.491 0.000 0.201 0.5820.0000.000 0.000 0.0000.901 0.240 844.00.750.405 0.000 12.70 0.16 180.0
3/26/2025 07:57 0.76412.49218.296 9.929 53.4727.466 0.000 0.006 0.8800.0000.000 0.000 0.0000.906 0.232 844.00.760.452 0.000 13.26 0.15 180.0
3/26/2025 07:58 0.19512.15818.317 9.940 61.0937.727 0.000 0.000 1.1550.0000.000 0.000 0.0000.907 0.238 844.00.850.556 0.000 12.35 0.15 180.0
0.51312.18218.294 9.897 52.8327.367 0.000 0.050 0.7820.0000.000 0.000 0.0000.850 0.228 843.830.7700.469 0.000 12.695 0.170 180.1Avg.
Spike 1
3/26/2025 08:03 5.07332.64316.634 9.468 51.92256.264 0.529 0.268 2.0050.0000.000 2.465 21.5700.399 0.330 844.023.990.182 0.899 37.72 0.03 180.0
Run 1 - B 30minute/60min
3/26/2025 08:06 0.89512.15618.315 9.919 61.0037.895 0.000 0.073 1.3500.0000.000 0.000 0.0000.683 0.242 844.00.800.470 0.000 13.05 0.16 180.0
3/26/2025 08:07 0.81512.36218.309 9.931 56.1277.872 0.000 0.126 1.0780.0000.000 0.000 0.0000.739 0.223 844.00.730.421 0.000 13.18 0.16 180.0
3/26/2025 08:08 0.33012.18818.296 9.931 48.5297.734 0.000 0.067 0.8530.0000.000 0.000 0.0000.739 0.236 844.00.800.493 0.000 12.52 0.17 180.0
3/26/2025 08:09 0.25612.37318.303 9.939 47.3587.863 0.000 0.270 0.7660.0000.000 0.000 0.0000.675 0.239 844.00.750.407 0.000 12.63 0.03 180.0
3/26/2025 08:10 0.11312.38418.316 9.949 54.8248.190 0.000 0.118 1.2460.0000.000 0.026 0.0000.700 0.234 844.00.800.475 0.000 12.50 0.03 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/26/2025 08:11 0.21012.54818.308 9.951 50.8667.871 0.000 0.048 1.0960.0000.000 0.000 0.0000.696 0.225 844.00.750.454 0.000 12.76 0.14 180.0
3/26/2025 08:12 0.96312.36018.321 9.959 50.2007.697 0.000 0.195 0.8280.0000.000 0.000 0.0000.740 0.241 844.00.710.342 0.000 13.32 0.15 180.0
3/26/2025 08:13 0.77812.26418.310 9.949 50.3867.699 0.000 0.077 1.0150.0000.000 0.000 0.0000.673 0.220 844.00.750.459 0.000 13.04 0.15 180.0
3/26/2025 08:14 0.36612.15318.300 9.935 48.5607.616 0.000 0.108 0.7280.0000.000 0.000 0.0000.647 0.240 844.00.740.383 0.000 12.52 0.15 180.0
3/26/2025 08:15 0.89012.33118.313 9.944 51.2477.564 0.000 0.204 0.8250.0000.000 0.000 0.0000.635 0.233 844.00.710.367 0.000 13.22 0.15 180.0
3/26/2025 08:16 0.37912.29318.287 9.930 48.8837.516 0.000 0.114 0.9660.0000.000 0.000 0.0000.690 0.236 844.00.750.413 0.000 12.67 0.15 180.0
3/26/2025 08:17 0.37212.44018.286 9.920 52.3337.546 0.000 0.222 1.1260.0000.000 0.000 0.0000.642 0.226 844.00.730.412 0.000 12.81 0.15 180.0
3/26/2025 08:18 0.19111.91018.305 9.918 54.3817.623 0.000 0.066 1.0950.0000.000 0.000 0.0000.626 0.231 844.00.810.526 0.000 12.10 0.15 180.0
3/26/2025 08:19 0.90712.08618.306 9.920 51.5377.490 0.000 0.247 0.9540.0000.000 0.000 0.0000.648 0.238 844.00.790.474 0.000 12.99 0.15 180.0
3/26/2025 08:20 0.24611.80818.295 9.919 52.2857.439 0.000 0.193 0.9780.0000.000 0.006 0.0000.581 0.232 844.00.770.452 0.001 12.05 0.15 180.0
3/26/2025 08:21 0.23511.69718.295 9.916 51.4447.561 0.000 0.116 1.0920.0000.000 0.000 0.0000.659 0.211 844.00.770.526 0.000 11.93 0.16 180.0
3/26/2025 08:23 0.11211.59618.299 9.929 57.1247.590 0.000 0.158 1.2910.0000.000 0.000 0.0000.722 0.230 844.00.840.568 0.000 11.71 0.15 180.0
3/26/2025 08:24 0.24012.05918.282 9.926 53.8717.637 0.000 0.263 1.0970.0000.000 0.000 0.0000.652 0.239 844.00.740.387 0.000 12.30 0.16 180.0
3/26/2025 08:25 0.86911.70818.299 9.954 48.9697.378 0.000 0.291 0.9340.0000.000 0.000 0.0000.668 0.231 844.00.760.443 0.000 12.58 0.17 180.0
3/26/2025 08:26 0.29711.79418.282 9.938 48.7097.392 0.000 0.115 0.9940.0000.000 0.000 0.0000.605 0.240 844.00.800.487 0.000 12.09 0.15 180.0
3/26/2025 08:27 0.10111.78218.286 9.944 49.7747.511 0.000 0.319 0.9180.0000.000 0.000 0.0000.702 0.251 844.00.770.403 0.000 11.88 0.16 180.0
3/26/2025 08:28 0.11212.04918.300 9.970 54.9087.461 0.000 0.289 0.8680.0000.000 0.000 0.0000.648 0.256 844.00.770.387 0.000 12.16 0.15 180.0
3/26/2025 08:29 0.25611.94918.290 9.953 51.5847.465 0.000 0.098 1.0660.0000.000 0.000 0.0000.617 0.238 844.00.800.479 0.000 12.21 0.15 180.0
3/26/2025 08:30 0.24511.75018.284 9.954 53.3087.302 0.000 0.298 0.8320.0000.000 0.000 0.0000.854 0.254 844.00.770.396 0.000 12.00 0.15 180.0
3/26/2025 08:31 0.09911.71718.268 9.933 55.7037.409 0.000 0.061 1.0610.0000.000 0.000 0.0000.627 0.250 844.00.810.465 0.000 11.82 0.15 180.0
3/26/2025 08:32 0.05312.01218.278 9.926 49.7597.312 0.000 0.386 0.8500.0000.000 0.000 0.0000.614 0.251 844.00.720.330 0.000 12.06 0.14 180.0
3/26/2025 08:33 0.67211.92918.296 9.940 53.0587.289 0.000 0.141 0.9810.0000.000 0.000 0.0000.690 0.258 844.00.820.456 0.000 12.60 0.16 180.0
3/26/2025 08:34 0.26811.86518.301 9.932 38.9976.909 0.000 0.262 0.6180.0000.000 0.000 0.0000.572 0.246 844.00.750.386 0.000 12.13 0.18 180.0
3/26/2025 08:35 0.91911.53218.291 9.920 41.9286.944 0.000 0.159 0.7040.0000.000 0.000 0.0000.629 0.244 844.00.790.447 0.000 12.45 0.17 180.0
3/26/2025 08:36 0.90911.72418.329 9.926 41.4056.963 0.000 0.189 0.7940.0000.000 0.000 0.0000.537 0.232 844.00.790.493 0.000 12.63 0.15 180.0
0.43712.02718.298 9.936 50.9697.525 0.000 0.176 0.9670.0000.000 0.001 0.0000.664 0.238 844.000.7700.440 0.000 12.464 0.146 180.0Avg.
0.47512.10518.296 9.917 51.9007.446 0.000 0.113 0.8750.0000.000 0.001 0.0000.757 0.233 843.920.7700.455 0.000 12.579 0.158 180.0Run 1 Avg:
Baseline 1
3/26/2025 08:40 0.0000.0000.028 0.000 0.0000.865 0.019 0.069 0.0000.0000.400 0.000 0.0000.000 0.135 844.00.270.000 0.000 0.00 0.00 180.0
Run 2 - A 30minute/60min
3/26/2025 08:59 0.09611.40518.181 9.872 52.9557.112 0.000 0.489 0.8110.0000.000 0.000 0.0000.834 0.282 844.00.860.441 0.000 11.50 0.16 180.0
3/26/2025 09:00 0.15711.54718.177 9.896 51.5146.778 0.000 0.501 0.7750.0000.000 0.000 0.0000.815 0.275 844.00.730.261 0.000 11.70 0.18 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/26/2025 09:02 0.16611.71518.186 9.887 51.3296.607 0.000 0.337 0.7830.0000.000 0.000 0.0000.804 0.258 844.00.740.335 0.000 11.88 0.17 180.0
3/26/2025 09:03 1.00911.50118.248 9.919 53.7896.600 0.000 0.279 0.7850.0000.000 0.000 0.0000.667 0.258 844.00.760.371 0.000 12.51 0.16 181.0
3/26/2025 09:04 0.54711.36618.205 9.890 51.6136.545 0.000 0.142 0.7270.0000.000 0.000 0.0000.832 0.276 844.00.840.440 0.000 11.91 0.19 180.0
3/26/2025 09:05 0.89811.17618.225 9.890 50.4776.551 0.000 0.192 0.7120.0000.000 0.000 0.0000.820 0.255 844.00.730.329 0.000 12.07 0.17 180.0
3/26/2025 09:06 0.55511.24218.264 9.907 54.8856.512 0.000 0.336 0.8840.0000.000 0.000 0.0000.646 0.266 844.00.750.333 0.000 11.80 0.17 180.0
3/26/2025 09:07 0.60811.01918.271 9.910 51.8276.726 0.000 0.282 0.7600.0000.000 0.000 0.0000.619 0.253 844.00.770.389 0.000 11.63 0.15 180.0
3/26/2025 09:08 0.09511.12118.263 9.893 51.9706.585 0.000 0.163 0.7810.0000.000 0.000 0.0000.610 0.251 844.00.820.470 0.000 11.22 0.16 180.0
3/26/2025 09:09 0.66311.62518.297 9.922 45.6636.594 0.000 0.303 0.7630.0000.000 0.000 0.0000.593 0.250 844.00.760.385 0.000 12.29 0.19 180.0
3/26/2025 09:10 0.30511.40218.306 9.916 36.7046.274 0.000 0.317 0.4650.0000.000 0.026 0.0000.544 0.244 844.00.640.202 0.000 11.71 0.17 180.0
3/26/2025 09:11 0.77310.87718.276 9.877 51.7506.482 0.000 0.302 0.7520.0000.000 0.000 0.0000.582 0.261 844.00.780.392 0.000 11.65 0.18 180.0
3/26/2025 09:12 0.61010.90918.293 9.896 47.6816.372 0.000 0.227 0.7380.0000.000 0.000 0.0000.676 0.243 844.00.740.384 0.001 11.52 0.17 180.0
3/26/2025 09:13 0.79110.86618.314 9.903 42.7496.324 0.000 0.236 0.6070.0000.000 0.000 0.0000.768 0.230 844.00.740.418 0.000 11.66 0.16 180.0
3/26/2025 09:14 0.14210.67818.312 9.906 50.4976.411 0.000 0.391 0.6270.0000.000 0.000 0.0000.581 0.254 844.00.730.335 0.000 10.82 0.17 180.0
3/26/2025 09:15 0.00010.98718.290 9.891 45.5316.286 0.000 0.272 0.6870.0000.000 0.000 0.0000.580 0.267 844.00.790.385 0.000 10.99 0.17 180.0
3/26/2025 09:16 0.27310.78118.285 9.910 48.8526.323 0.000 0.228 0.6420.0000.000 0.000 0.0000.833 0.253 844.00.710.298 0.000 11.05 0.15 180.0
3/26/2025 09:17 0.02611.28118.303 9.917 55.2836.680 0.000 0.331 0.8720.0000.000 0.000 0.0000.672 0.277 844.00.770.321 0.000 11.31 0.17 180.0
3/26/2025 09:18 0.49211.27918.300 9.917 47.7496.562 0.000 0.240 0.6780.0000.000 0.000 0.0000.833 0.253 844.00.750.363 0.000 11.77 0.16 180.0
3/26/2025 09:19 0.61811.03118.323 9.938 54.1206.513 0.000 0.222 0.8290.0000.000 0.000 0.0000.749 0.264 844.00.740.320 0.000 11.65 0.17 180.0
3/26/2025 09:20 0.04311.55818.295 9.934 48.7236.428 0.000 0.269 0.6570.0000.000 0.000 0.0000.604 0.267 844.00.750.329 0.000 11.60 0.17 180.0
3/26/2025 09:21 0.59011.17418.309 9.939 52.6096.576 0.000 0.299 0.7780.0000.000 0.000 0.0000.883 0.259 844.00.780.396 0.000 11.76 0.16 180.0
3/26/2025 09:22 0.81510.94518.307 9.920 47.8046.384 0.000 0.224 0.5810.0000.000 0.000 0.0000.634 0.264 844.00.760.349 0.000 11.76 0.15 180.0
3/26/2025 09:23 0.25711.28218.307 9.930 39.0296.304 0.000 0.258 0.4090.0000.000 0.000 0.0000.551 0.277 844.00.730.258 0.000 11.54 0.16 180.0
3/26/2025 09:24 0.14711.46718.305 9.915 46.9756.415 0.000 0.242 0.6180.0000.000 0.000 0.0000.593 0.274 844.00.780.344 0.000 11.61 0.16 180.0
3/26/2025 09:25 1.01411.52118.306 9.921 41.3296.258 0.000 0.220 0.4660.0000.000 0.000 0.0000.654 0.283 844.00.800.346 0.000 12.54 0.16 180.0
3/26/2025 09:26 0.12011.28118.317 9.924 43.1066.511 0.000 0.268 0.5510.0000.000 0.000 0.0000.787 0.275 844.00.830.426 0.000 11.40 0.03 180.0
3/26/2025 09:27 0.00011.02118.324 9.921 56.3246.845 0.000 0.310 0.9000.0000.000 0.000 0.0000.619 0.267 844.00.760.339 0.000 11.02 0.03 180.0
3/26/2025 09:28 0.12911.09418.331 9.894 44.9986.419 0.000 0.264 0.5050.0000.000 0.000 0.0000.593 0.270 844.00.790.375 0.000 11.22 0.16 180.0
3/26/2025 09:29 0.19910.73618.313 9.883 43.8116.240 0.000 0.224 0.6010.0000.000 0.000 0.0000.616 0.241 844.00.680.293 0.000 10.94 0.16 180.0
0.40511.19618.281 9.908 48.7226.507 0.000 0.279 0.6910.0000.000 0.001 0.0000.686 0.262 844.000.7600.354 0.000 11.601 0.157 180.0Avg.
Spike 2
3/26/2025 09:33 11.53121.67616.671 9.467 50.30853.528 0.521 0.533 1.6650.0000.000 2.201 20.8270.529 0.427 844.023.450.458 0.873 33.21 0.14 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
3/26/2025 09:37 0.00011.60918.327 9.934 56.9396.833 0.000 0.262 0.9100.0000.000 0.000 0.0000.617 0.271 843.00.770.334 0.000 11.61 0.15 180.0
3/26/2025 09:39 0.62411.69118.333 9.935 54.7856.664 0.000 0.220 0.8530.0000.000 0.000 0.0000.683 0.262 843.00.750.346 0.000 12.32 0.04 180.0
3/26/2025 09:40 0.88911.82818.335 9.927 48.4266.574 0.000 0.223 0.6570.0000.000 0.000 0.0000.737 0.250 843.00.720.331 0.000 12.72 0.14 180.0
3/26/2025 09:41 0.16011.86018.343 9.921 47.8076.671 0.000 0.266 0.7060.0000.000 0.000 0.0000.599 0.253 843.00.760.388 0.001 12.02 0.03 180.0
3/26/2025 09:42 0.66311.73718.340 9.938 50.4026.604 0.000 0.161 0.7000.0000.000 0.000 0.0000.660 0.267 843.00.820.430 0.000 12.40 0.15 180.0
3/26/2025 09:43 0.33712.05118.356 9.941 33.0696.689 0.000 0.121 0.2850.0000.000 0.000 0.0000.742 0.249 843.00.750.385 0.000 12.39 0.03 180.0
3/26/2025 09:44 0.90211.94718.369 9.939 40.8678.023 0.000 0.358 0.4780.0000.000 0.000 0.0000.545 0.248 843.00.750.379 0.000 12.85 0.02 180.0
3/26/2025 09:45 0.58011.71518.376 9.924 45.9707.377 0.000 0.295 0.6610.0000.000 0.000 0.0000.773 0.231 843.00.700.356 0.000 12.30 0.03 180.0
3/26/2025 09:46 0.22211.88618.360 9.909 44.8786.895 0.000 0.317 0.6130.0000.000 0.000 0.0000.569 0.247 844.00.700.306 0.000 12.11 0.15 180.0
3/26/2025 09:47 0.01611.82418.347 9.885 47.0856.764 0.000 0.238 0.7260.0000.000 0.000 0.0000.471 0.222 844.00.750.458 0.000 11.84 0.15 180.0
3/26/2025 09:48 0.24811.51118.349 9.893 45.8976.662 0.000 0.187 0.3370.0000.000 0.000 0.0000.791 0.225 844.00.650.308 0.000 11.76 0.15 180.0
3/26/2025 09:49 0.71811.52818.373 9.902 55.5246.625 0.000 0.189 0.9660.0000.000 0.000 0.0000.553 0.228 843.00.700.371 0.002 12.25 0.15 180.0
3/26/2025 09:50 0.03411.64118.385 9.907 53.6416.562 0.000 0.167 0.8470.0000.000 0.000 0.0000.573 0.246 843.00.760.406 0.000 11.67 0.16 180.0
3/26/2025 09:51 0.27111.58618.360 9.903 37.9746.377 0.000 0.124 0.0000.0000.000 0.000 0.0000.773 0.251 843.00.740.352 0.000 11.86 0.15 180.0
3/26/2025 09:52 0.25311.79118.386 9.932 46.1076.612 0.000 0.194 0.6930.0000.000 0.000 0.0000.732 0.225 843.00.640.280 0.000 12.04 0.13 180.0
3/26/2025 09:53 0.80711.83418.392 9.936 43.6806.556 0.000 0.192 0.2800.0000.000 0.000 0.0000.784 0.236 843.00.750.422 0.000 12.64 0.14 180.0
3/26/2025 09:54 1.01212.13918.375 9.924 44.2756.307 0.000 0.111 0.2270.0000.000 0.000 0.0000.746 0.226 843.00.700.377 0.002 13.15 0.15 180.0
3/26/2025 09:55 0.78412.01018.394 9.933 39.8446.446 0.000 0.062 0.2200.0000.000 0.000 0.0000.651 0.219 843.00.760.477 0.000 12.79 0.15 180.0
3/26/2025 09:56 1.01411.96818.397 9.938 48.9866.657 0.000 0.143 0.4930.0000.000 0.000 0.0000.826 0.236 843.00.790.484 0.000 12.98 0.03 180.0
3/26/2025 09:57 0.70512.10618.423 9.933 45.3816.784 0.000 0.134 0.3930.0000.000 0.000 0.0000.723 0.222 843.00.700.391 0.000 12.81 0.03 180.0
3/26/2025 09:58 0.15512.01218.380 9.933 44.9076.956 0.000 0.193 0.3080.0000.000 0.000 0.0000.738 0.251 843.00.680.265 0.000 12.17 0.03 180.0
3/26/2025 09:59 0.16812.13318.375 9.943 52.2538.187 0.000 0.175 1.0310.0000.000 0.000 0.0000.809 0.233 843.00.720.381 0.000 12.30 0.15 180.0
3/26/2025 10:00 0.68711.93118.348 9.929 51.9357.322 0.000 0.298 0.8540.0000.000 0.000 0.0000.771 0.234 843.00.710.361 0.000 12.62 0.03 180.0
3/26/2025 10:01 0.97312.17218.356 9.934 41.2608.250 0.000 0.314 0.2740.0000.000 0.000 0.0000.837 0.236 843.00.730.385 0.000 13.14 0.14 180.0
3/26/2025 10:02 1.04212.21118.367 9.927 36.3446.543 0.000 0.223 0.0970.0000.000 0.000 0.0000.744 0.269 843.00.760.337 0.000 13.25 0.15 180.0
3/26/2025 10:03 0.94211.67618.374 9.918 57.1197.051 0.000 0.263 0.9500.0000.000 0.000 0.0000.700 0.239 843.00.680.298 0.000 12.62 0.02 180.0
3/26/2025 10:04 1.38212.47718.387 9.907 33.0166.562 0.000 0.306 0.3970.0000.000 0.000 0.0000.743 0.218 843.00.640.309 0.002 13.86 0.16 180.0
3/26/2025 10:05 0.34911.61518.388 9.909 47.9087.487 0.000 0.273 0.7090.0000.000 0.000 0.0000.688 0.216 843.00.730.446 0.000 11.96 0.02 180.0
3/26/2025 10:06 0.13812.03518.407 9.924 41.3937.287 0.000 0.466 0.5710.0000.000 0.000 0.0000.739 0.247 843.00.710.332 0.000 12.17 0.03 180.0
3/26/2025 10:07 0.97712.09718.369 9.897 37.4006.574 0.000 0.272 0.4590.0000.000 0.000 0.0000.708 0.226 843.00.700.371 0.000 13.07 0.14 180.0
0.56811.88718.369 9.923 45.8366.897 0.000 0.225 0.5570.0000.000 0.000 0.0000.701 0.239 843.100.7240.369 0.000 12.456 0.100 180.0Avg.
0.48711.54218.325 9.915 47.2796.702 0.000 0.252 0.6240.0000.000 0.000 0.0000.694 0.251 843.550.7420.362 0.000 12.028 0.129 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
3/26/2025 10:11 0.0000.0000.039 0.000 0.0000.583 0.079 0.000 0.0000.0040.709 0.000 0.0000.000 0.130 843.00.260.000 0.000 0.00 0.00 180.0
Run 3 - A 30minute/60min
3/26/2025 10:16 0.37811.95418.353 9.907 44.6416.454 0.000 0.348 0.6260.0000.000 0.000 0.0000.639 0.254 843.00.710.300 0.000 12.33 0.16 180.0
3/26/2025 10:17 0.10512.12918.350 9.914 48.9806.594 0.000 0.331 0.6560.0000.000 0.000 0.0000.807 0.256 843.00.690.262 0.000 12.23 0.15 180.0
3/26/2025 10:18 0.39211.91218.364 9.926 43.8636.480 0.000 0.194 0.6020.0000.000 0.000 0.0000.559 0.257 843.00.740.342 0.000 12.30 0.14 180.0
3/26/2025 10:19 0.28011.75418.382 9.930 47.1826.366 0.000 0.291 0.2740.0000.000 0.000 0.0000.774 0.259 843.00.760.358 0.000 12.03 0.15 180.0
3/26/2025 10:20 1.00311.63318.405 9.931 45.5166.284 0.000 0.280 0.6020.0000.000 0.000 0.0000.810 0.266 843.00.720.286 0.000 12.64 0.16 180.0
3/26/2025 10:21 0.12911.58918.383 9.912 54.7696.564 0.000 0.141 0.4160.0000.000 0.000 0.0000.795 0.283 843.00.870.461 0.000 11.72 0.15 180.0
3/26/2025 10:22 0.09011.56218.384 9.922 53.8876.484 0.000 0.315 0.7220.0000.000 0.000 0.0000.827 0.276 843.00.750.302 0.000 11.65 0.04 180.0
3/26/2025 10:23 0.07311.70818.386 9.910 50.3016.438 0.000 0.283 0.6350.0000.000 0.000 0.0000.619 0.275 843.00.820.407 0.000 11.78 0.15 180.0
3/26/2025 10:24 0.10611.57618.387 9.896 42.6716.179 0.000 0.285 0.4560.0000.000 0.000 0.0000.798 0.268 843.00.730.293 0.000 11.68 0.15 180.0
3/26/2025 10:25 0.15711.25718.411 9.905 54.6856.208 0.000 0.209 0.7490.0000.000 0.000 0.0000.508 0.271 843.00.820.423 0.000 11.41 0.03 180.0
3/26/2025 10:26 0.02711.40918.411 9.896 54.5836.134 0.000 0.254 0.7490.0000.000 0.000 0.0000.790 0.260 843.00.760.353 0.000 11.44 0.17 180.0
3/26/2025 10:27 0.71011.26318.413 9.880 40.8996.026 0.000 0.289 0.4950.0000.000 0.000 0.0000.545 0.254 843.00.760.374 0.002 11.97 0.17 180.0
3/26/2025 10:28 0.58911.17318.394 9.898 56.4036.546 0.000 0.139 0.8050.0000.000 0.000 0.0000.654 0.280 843.00.870.463 0.000 11.76 0.03 180.0
3/26/2025 10:29 0.33011.38018.391 9.909 50.3906.458 0.000 0.327 0.5970.0000.000 0.000 0.0000.527 0.278 843.00.800.363 0.000 11.71 0.17 180.0
3/26/2025 10:30 0.75211.66818.380 9.915 49.9856.479 0.000 0.291 0.6920.0000.000 0.000 0.0000.601 0.294 843.00.800.311 0.000 12.42 0.15 180.0
3/26/2025 10:31 0.73611.48018.343 9.909 51.6636.631 0.000 0.393 0.6850.0000.000 0.000 0.0000.621 0.289 843.00.780.308 0.000 12.22 0.15 180.0
3/26/2025 10:32 0.11011.73218.342 9.928 52.9466.653 0.000 0.420 0.6740.0000.000 0.000 0.0000.577 0.291 843.00.780.296 0.000 11.84 0.15 180.0
3/26/2025 10:33 0.25611.83918.363 9.929 46.2956.824 0.000 0.344 0.4280.0000.000 0.000 0.0000.646 0.312 843.00.820.289 0.000 12.09 0.03 180.0
3/26/2025 10:34 0.07611.42118.374 9.915 53.2886.940 0.000 0.350 0.8610.0000.000 0.000 0.0000.598 0.280 843.00.820.392 0.000 11.50 0.03 180.0
3/26/2025 10:35 0.74611.61318.353 9.918 53.1926.875 0.000 0.471 0.7760.0000.000 0.000 0.0000.672 0.281 843.00.780.326 0.000 12.36 0.15 180.0
3/26/2025 10:36 0.27011.65318.358 9.925 42.4486.696 0.000 0.301 0.3690.0000.000 0.000 0.0000.593 0.285 843.00.760.287 0.000 11.92 0.15 180.0
3/26/2025 10:37 1.09012.16818.370 9.938 36.9316.519 0.000 0.245 0.4270.0000.000 0.000 0.0000.610 0.272 843.00.720.265 0.000 13.26 0.15 180.0
3/26/2025 10:38 0.73711.73618.384 9.945 53.6757.229 0.000 0.414 0.7090.0000.000 0.000 0.0000.656 0.288 843.00.840.396 0.000 12.47 0.02 180.0
3/26/2025 10:39 0.47211.84918.385 9.925 40.6506.822 0.000 0.261 0.4070.0000.000 0.000 0.0000.621 0.294 843.00.750.238 0.000 12.32 0.15 180.0
3/26/2025 10:40 0.20211.63518.388 9.939 49.0796.639 0.000 0.110 0.5770.0000.000 0.000 0.0000.609 0.286 843.00.870.454 0.000 11.84 0.03 180.0
3/26/2025 10:41 0.37111.81118.368 9.920 40.6056.322 0.000 0.248 0.5110.0000.000 0.000 0.0000.521 0.259 843.00.730.316 0.000 12.18 0.16 180.0
3/26/2025 10:42 0.38111.77218.377 9.898 39.2406.255 0.000 0.045 0.5410.0000.000 0.000 0.0000.507 0.258 843.00.840.489 0.000 12.15 0.15 180.0
3/26/2025 10:43 0.92411.66818.388 9.919 45.6876.558 0.000 0.259 0.6100.0000.000 0.003 0.0000.483 0.270 843.00.780.352 0.000 12.59 0.14 180.0
3/26/2025 10:44 1.17611.55218.403 9.915 42.4786.440 0.000 0.308 0.4490.0000.000 0.000 0.0000.520 0.272 843.00.840.438 0.000 12.73 0.15 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/26/2025 10:45 0.61311.46518.357 9.887 48.1136.470 0.000 0.252 0.6150.0000.000 0.000 0.0000.628 0.266 843.00.770.350 0.000 12.08 0.03 179.0
0.44311.64518.378 9.915 47.8356.519 0.000 0.280 0.5910.0000.000 0.000 0.0000.637 0.274 843.000.7830.350 0.000 12.087 0.120 180.0Avg.
Spike 3
3/26/2025 10:50 11.14124.97616.731 9.489 27.09353.019 0.853 0.490 1.1750.0000.000 2.120 20.6570.405 0.472 843.023.360.511 0.861 36.12 0.04 180.0
Run 3 - B 30minute/60min
3/26/2025 10:53 1.12312.43818.325 9.918 40.7476.508 0.000 0.334 0.4380.0000.000 0.000 0.0000.543 0.296 843.00.830.358 0.002 13.56 0.16 180.0
3/26/2025 10:54 0.35011.86418.338 9.914 45.8346.585 0.000 0.279 0.5240.0000.000 0.000 0.0000.616 0.274 843.00.770.330 0.000 12.21 0.15 180.0
3/26/2025 10:55 1.14112.24418.352 9.933 41.4906.438 0.000 0.281 0.5750.0000.000 0.000 0.0000.533 0.262 843.00.780.381 0.000 13.38 0.15 180.0
3/26/2025 10:56 0.90312.08318.334 9.925 37.1146.360 0.000 0.252 0.4460.0000.000 0.000 0.0000.506 0.273 843.00.760.322 0.000 12.99 0.16 180.0
3/26/2025 10:57 0.95212.02218.348 9.928 43.1617.097 0.000 0.233 0.6030.0000.000 0.000 0.0000.597 0.258 843.00.720.301 0.001 12.97 0.14 180.0
3/26/2025 10:58 0.21412.10918.351 9.939 48.1876.913 0.000 0.338 0.6250.0000.000 0.000 0.0000.624 0.276 843.00.760.315 0.000 12.32 0.16 180.0
3/26/2025 10:59 1.04012.38518.356 9.943 29.7236.482 0.000 0.373 0.3090.0000.000 0.000 0.0000.524 0.278 843.00.720.251 0.000 13.43 0.16 180.0
3/26/2025 11:00 0.16311.79718.351 9.916 45.6827.341 0.000 0.468 0.6250.0000.000 0.000 0.0000.599 0.267 843.00.780.371 0.003 11.96 0.02 180.0
3/26/2025 11:01 0.28611.91018.338 9.907 45.1116.945 0.000 0.403 0.6060.0000.000 0.000 0.0000.591 0.290 843.00.800.322 0.000 12.20 0.16 180.0
3/26/2025 11:02 0.15911.44818.349 9.924 44.9656.910 0.000 0.343 0.6180.0000.000 0.000 0.0000.558 0.271 843.00.750.318 0.001 11.61 0.15 180.0
3/26/2025 11:03 0.15811.34918.345 9.909 46.2787.149 0.000 0.519 0.6230.0000.000 0.000 0.0000.488 0.266 843.00.770.363 0.002 11.51 0.03 180.0
3/26/2025 11:04 0.78711.49118.343 9.919 53.0357.071 0.000 0.457 0.7770.0000.000 0.000 0.0000.512 0.272 843.00.860.481 0.000 12.28 0.15 180.0
3/26/2025 11:05 1.14911.65018.335 9.911 35.8146.548 0.000 0.345 0.2960.0000.000 0.000 0.0000.597 0.278 843.00.740.271 0.000 12.80 0.16 180.0
3/26/2025 11:06 0.51112.05118.338 9.917 38.5006.446 0.000 0.326 0.3790.0000.000 0.000 0.0000.563 0.270 843.00.770.342 0.000 12.56 0.14 180.0
3/26/2025 11:07 0.99612.01418.319 9.910 42.2216.758 0.000 0.339 0.5140.0000.000 0.000 0.0000.595 0.283 843.00.760.288 0.000 13.01 0.15 180.0
3/26/2025 11:08 1.03511.85718.318 9.924 47.8406.740 0.000 0.347 0.6860.0000.000 0.000 0.0000.595 0.292 843.00.790.312 0.000 12.89 0.16 180.0
3/26/2025 11:09 0.96111.81318.357 9.948 38.6786.628 0.000 0.429 0.4280.0000.000 0.000 0.0000.606 0.276 843.00.760.304 0.000 12.77 0.18 180.0
3/26/2025 11:10 1.04811.79518.355 9.929 42.7196.579 0.000 0.328 0.4380.0000.000 0.000 0.0000.528 0.292 843.00.840.382 0.000 12.84 0.03 180.0
3/26/2025 11:11 0.07211.91618.338 9.919 47.1857.014 0.000 0.464 0.5960.0000.000 0.000 0.0000.515 0.306 843.00.910.454 0.000 11.99 0.17 180.0
3/26/2025 11:12 0.37811.85818.343 9.925 42.7606.825 0.000 0.403 0.4920.0000.000 0.000 0.0000.604 0.292 843.00.810.337 0.000 12.24 0.16 180.0
3/26/2025 11:13 0.88412.02818.356 9.912 34.7886.363 0.000 0.254 0.2860.0000.000 0.000 0.0000.539 0.302 843.00.840.352 0.001 12.91 0.17 180.0
3/26/2025 11:14 0.76211.75018.340 9.921 43.7286.649 0.000 0.450 0.4630.0000.000 0.000 0.0000.510 0.311 843.00.810.278 0.000 12.51 0.15 180.0
3/26/2025 11:15 0.67811.82718.353 9.932 44.0626.683 0.000 0.375 0.6020.0000.000 0.000 0.0000.625 0.297 843.00.820.343 0.000 12.51 0.16 180.0
3/26/2025 11:16 0.00011.65418.358 9.939 50.8666.882 0.000 0.390 0.7170.0000.000 0.000 0.0000.528 0.297 843.00.760.248 0.000 11.65 0.15 180.0
3/26/2025 11:17 0.20911.68918.357 9.925 44.1506.761 0.000 0.381 0.5590.0000.000 0.000 0.0000.583 0.291 843.00.790.311 0.000 11.90 0.15 180.0
3/26/2025 11:18 1.08112.09318.346 9.902 40.8706.586 0.000 0.423 0.4920.0000.000 0.000 0.0000.584 0.304 843.00.860.373 0.000 13.17 0.16 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/26/2025 11:19 0.87511.98518.346 9.900 35.0876.421 0.000 0.358 0.4730.0000.000 0.000 0.0000.503 0.297 843.00.760.245 0.000 12.86 0.17 180.0
3/26/2025 11:20 0.89511.50718.342 9.888 46.0456.391 0.000 0.331 0.6360.0000.000 0.000 0.0000.564 0.293 843.00.810.339 0.000 12.40 0.02 180.0
3/26/2025 11:21 0.17911.34518.347 9.898 53.2676.877 0.000 0.364 0.7480.0000.000 0.000 0.0000.517 0.301 843.00.870.405 0.000 11.52 0.15 180.0
3/26/2025 11:22 0.26911.06918.345 9.895 59.0067.006 0.000 0.350 0.9640.0000.000 0.000 0.0000.615 0.301 843.00.830.346 0.000 11.34 0.16 180.0
0.64211.83518.344 9.919 43.6306.732 0.000 0.365 0.5510.0000.000 0.000 0.0000.562 0.286 843.000.7940.335 0.000 12.476 0.139 180.0Avg.
0.54211.74018.361 9.917 45.7336.625 0.000 0.322 0.5710.0000.000 0.000 0.0000.600 0.280 843.000.7890.342 0.000 12.282 0.130 180.0Run 3 Avg:
Baseline 3
3/26/2025 11:27 0.0000.1660.028 0.000 0.0000.974 0.043 0.176 0.0000.0011.256 0.000 0.0000.000 0.193 843.00.390.000 0.000 0.17 0.00 180.0
Post CTS
3/26/2025 11:29 0.0000.0000.033 0.000 0.0001.072 0.033 0.403 0.0000.0000.000 100.237 0.0000.000 0.222 843.067.270.000 0.000 0.00 0.07 180.0
3/26/2025 11:29 0.0000.0000.037 0.002 0.0000.875 0.029 0.375 0.0000.0000.000 99.637 0.0000.000 0.182 843.066.800.008 0.000 0.00 0.07 180.0
3/26/2025 11:29 0.0000.0000.034 0.000 0.0000.892 0.029 0.524 0.0000.0000.098 100.135 0.0000.162 0.243 843.067.250.000 0.000 0.00 0.07 180.0
3/26/2025 11:29 0.0000.0000.034 0.000 0.0000.947 0.030 0.587 0.0000.0000.000 99.076 0.0000.000 0.217 843.066.490.000 0.000 0.00 0.07 180.0
Post NO2/Mid O2
3/26/2025 11:32 101.9033.8300.020 0.005 0.0801.157 0.914 0.318 0.2830.0000.000 0.000 0.0000.067 0.234 843.00.620.222 0.003 105.73 10.94 180.0
3/26/2025 11:33 102.7454.0850.022 0.000 0.2051.101 1.002 0.000 0.6300.0000.495 0.000 0.0000.427 0.183 843.00.440.110 0.000 106.83 10.96 180.0
3/26/2025 11:33 102.7153.5890.018 0.000 0.1851.044 0.983 0.095 0.1280.0000.000 0.000 0.0000.283 0.289 843.00.670.145 0.000 106.30 10.95 180.0
Post 5-Gas
3/26/2025 11:34 0.000247.8760.018 4.804 0.723494.619 2.223 1.429 7.1850.0730.000 1.212 248.9560.000 0.000 843.0251.372.407 9.892 247.88 0.02 180.0
3/26/2025 11:34 0.000249.1330.029 4.823 0.951494.965 2.231 1.089 6.9130.1670.631 1.240 249.9900.000 0.000 843.0252.602.677 9.863 249.13 0.02 180.0
3/26/2025 11:34 0.000248.9420.022 4.847 0.725496.655 2.198 1.327 7.1540.1161.100 1.169 249.9120.000 0.000 843.0252.422.589 9.909 248.94 0.02 180.0
3/26/2025 11:34 0.000249.0870.024 4.797 1.338496.235 2.204 1.355 7.0560.1890.295 1.143 250.1870.000 0.000 843.0252.572.432 9.905 249.09 0.02 180.0
3/26/2025 11:35 0.000249.9780.023 4.819 0.000497.131 2.210 1.526 6.7840.1170.962 1.100 250.2700.000 0.000 843.0252.532.288 9.950 249.98 0.02 180.0
End of Test Purge
3/26/2025 11:36 0.0000.3810.016 0.021 0.0342.383 0.000 0.286 0.0000.0001.224 0.056 0.6250.053 0.185 843.01.030.000 0.025 0.38 0.00 180.0
3/26/2025 11:36 0.0000.6280.018 0.026 0.4211.987 0.000 0.153 0.0000.0001.487 0.000 0.3340.000 0.219 843.00.770.000 0.020 0.63 0.00 180.0
3/26/2025 11:36 0.0001.5870.016 0.010 0.0001.704 0.000 0.419 0.0510.0001.072 0.000 0.3880.111 0.188 843.00.880.169 0.016 1.59 0.00 180.0
3/26/2025 11:37 0.0001.6270.018 0.014 0.0081.780 0.000 0.191 0.0000.0001.432 0.010 0.3310.156 0.192 843.00.720.000 0.017 1.63 0.00 180.0
3/26/2025 11:37 0.0001.7240.016 0.000 0.0001.728 0.070 0.140 0.0000.0001.806 0.000 0.1760.034 0.212 843.00.600.000 0.008 1.72 0.00 180.0
3/26/2025 11:37 0.0001.0270.020 0.000 0.0231.427 0.052 0.000 0.0000.0071.398 0.000 0.2860.203 0.186 843.00.720.097 0.004 1.03 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/26/2025 11:37 0.0001.0980.020 0.001 0.0001.506 0.065 0.094 0.0000.0281.444 0.000 0.1710.070 0.207 843.00.590.000 0.009 1.10 0.00 180.0
3/26/2025 11:37 0.0000.9110.016 0.000 0.0001.279 0.047 0.439 0.0000.0001.660 0.196 0.1450.000 0.205 843.00.790.161 0.013 0.91 0.00 180.0
3/26/2025 11:37 0.0000.7480.013 0.000 0.0001.281 0.046 0.370 0.5860.0002.102 0.000 0.4180.000 0.077 843.00.570.000 0.004 0.75 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 3/24/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:09:01 AM 01:54 PM
Source:
Unit Number: 1451
Serial Number: 1658736
Engine Hours:11299
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.023 0.384 0.024
1.665 17.002 1.088
2.000 0.300 1.000 0.150 0.700 0.030
0.005 0.077 0.005
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
LYNN HUBER
3
Cody Hall
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 1451 with a serial number of 1658736 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 3/24/2025 by
Cody Hall with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were
within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2250 BHP and 1198 RPM which is 90.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1451 is authorized to
operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 1451Unit ID
Make Waukesha Site Elevation ft.5249
Model 9394 GSI Atmospheric Pressure psi.12.08
Serial Number 1658736 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2250 2250 2250 2250
1199 1198 1198 1198
Percent Load %
Intake Manifold Pressure (hg)
90.00%90.00%90.00%90.00%
100.01 99.60 100.62 100.08
Intake Manifold Temperature (F)N/A N/A N/A N/A
Ambient Conditions
Ambient Temperature Dry (F)51.00 54.00 54.00 53.00
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
191113.10 188048.35 188235.45 189132.30
5411.67 5324.89 5330.18 5355.58
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %18.07%18.18%18.19%18.15%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.58%0.64%0.61%0.61%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
09:01 AM 10:44 AM 12:00 PM 3/24/2025
State
NOx (mol wt) 46.01
1.029 0.704 0.941 0.891NMNEHC (ppmvw)
1.255 0.860 1.150 1.088NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
364.567 250.557 334.276 316.467 FailNMNEHC (ppbvd) @15% O2
0.006 0.004 0.005 0.0050.700 0.030 PassNMNEHC (g/hp-hr)
0.027 0.019 0.025 0.0240.170 PassNMNEHC (lbs/hr)
0.365 0.251 0.334 0.316 FailNMNEHC (ppmvd) @15% O2
0.0040.005CO (g/hp-hr)0.005 0.0052.000 0.300 Pass
CO (ppmvw)1.389 1.462 1.238 1.363
CO (ppmvd)1.695 1.786 1.513 1.665
CO (mol wt) 28.01
CO (ppmvd) @15% O2 0.492 0.520 0.440 0.484 Fail
CO (ppbvd) @15% O2 492.174 520.155 440.015 484.115 Fail
0.0210.024CO (lbs/hr)0.024 0.0231.650 Pass
NOx (g/hp-hr)0.062 0.108 0.062 0.0771.000 0.150 Pass
NOx (ppmvw)11.028 19.457 11.261 13.915
NOx (ppmvd)13.460 23.781 13.764 17.002
NOx (ppbvd) @15% O2 3908.859 6924.841 4002.249 4945.317 Fail
NOx (ppmvd) @15% O2 3.909 6.925 4.002 4.945 Fail
NOx (lbs/hr)0.307 0.534 0.309 0.3840.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
1.39
0.17
10.35 0.68 11.03
0.03%
0.48%
0.00%
18.07%
9.10 0.66 0.41%18.04%
31.06 6.52 0.57%16.42%
11.60 0.70 0.55%18.11%
0.19 0.00 0.19 0.12%0.03%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.70 0.19 0.00 0.19 0.12%0.03%
1.71 22.85 0.93 23.78 0.53%18.13%
48.79 30.81 2.88 33.69 0.55%16.56%
1.21 14.25 0.89 15.14 0.51%18.23%
0.89 0.24 0.00 0.24 0.11%0.02%
Avg. Wet 1.46 18.55 0.91 19.46 0.70 0.52%18.18%
NO2NO
0.19
0.69
22.93
0.72
1.06
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
1.25 10.36 0.97 11.33 0.52%18.13%
48.29 27.64 6.09 33.74 0.43%16.65%
1.22 10.25 0.95 11.20 0.48%18.24%
0.69 0.58 0.00 0.58 0.12%0.02%
0.89 0.24 0.00 0.24 1.06 0.11%0.02%
Avg. Wet 1.24 10.31 0.96 11.26 0.94 0.50%18.19%
NO2NO
0.48
0.81
22.83
1.07
NMNEHC
0.29
NO2
0.000.69
1.35
23.98
0.71
0.19
1.03
0.17
9.76
37.58
12.29
1.98
0.80
0.70
49.87
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =20 Inches or:1.67 feet or:2.18 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.43
Yes
20.00
14.00
11.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%18.07
29.91
0.50
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.85
0.40
0.00
1025.40
0.04
30.29
30.33
922.19
1381.86
494.55
27.76
76.67
167.29
233272.43
191113.10
Run 2
18.18
29.94
0.46
11.95
0.64
0.00
1025.40
0.03
30.29
30.32
942.19
1401.86
505.66
27.77
74.37
167.27
229837.38
188048.35
Run 3
18.19
29.92
0.48
11.85
0.62
0.00
1025.40
0.04
30.29
30.33
941.19
1400.86
505.10
27.75
75.60
167.27
230077.31
188235.45
18.15
29.92
0.48
11.88
0.55
0.00
1025.40
0.04
30.29
30.33
935.19
1394.86
501.77
27.76
75.55
167.27
231062.37
189132.3
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.60
Exhaust Temp F
922.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.51
0.59
0.65
922.00
922.00
921.00
0.59
0.51
0.48
921.00
921.00
923.00
0.44
0.54
0.49
923.00
923.00
922.00
0.41 922.00
0.39
0.44
0.40
922.00
921.00
921.00
0.45
0.50
0.50
921.00
928.00
922.19
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.43
Exhaust Temp F
941.00
0.47
0.49
0.44
941.00
941.00
942.00
0.41
0.44
0.47
942.00
942.00
940.00
0.52
0.55
0.58
940.00
940.00
941.00
0.52 941.00
0.54
0.49
0.48
941.00
942.00
942.00
0.41
0.43
942.00
941.00
941.190.48
Run 2
Δpstd (in) H2O
0.44
Exhaust Temp F
942.00
0.44
0.48
0.49
942.00
942.00
943.00
0.55
0.52
0.55
943.00
943.00
941.00
0.57
0.50
0.49
941.00
941.00
942.00
0.46 942.00
0.44
0.41
0.39
942.00
943.00
943.00
0.33
0.36
943.00
942.00
0.46 942.19
Pass
Strat Check
13.01Check 1
12.87Check 2
13.11Check 3
NoxGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.851)+ .32(.395)+ .28(87.754+0) = 29.91 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.91(1 -.18073)+ 18.0(.18073) = 27.76 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.5*√(1381.86/(30.33*27.76)) = 76.67 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.18073)76.67*2.182((528*30.33)/ (1381.86*29.92)) = 191113.1 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 191113.104/35.315 = 5411.669 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 1.695*(20.9-15)/(20.9-.58%)) = .492 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(1.695*(1.164*10^-3)*5411.669*(Run Time/60))/2250 = .005 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .005*1/453.6*2250 = .024 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .024*4.38 = .105 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
1.69 = 1.3885*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.69%
21.12%
10.74%
10.89%
10.71%
10.71%
10.89%10.74%
10.69%
21.12%
10.71%
21.15%
10.71%
21.15%
10.71%21.15%
0.00%
10.71%
21.15%
0.02%
0.03%
0.11%
0.13%
10.71%
Span
Zero Offset 0.00%
21.15
0.00%
10.69%0.25%0.94%0.01%
0.59%
0.64%
0.62%
0.58%
0.64%
0.61%
9
GAS
0.0 0.0 0.0
0.0 0.0 0.0
1037.0 1036.0 1036.0
1073.0 1077.0 1073.7
6.0 6.0 6
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
3/24/2025
5249
1451
Waukesha
Model
Serial Number
9394 GSI
1658736
Technician Cody Hall
Run Start Times 09:01 AM 10:44 AM 12:00 PM 01:54 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1199.0 1198.0 1198.0 1198.3
Engine Hours 11296 11297 11298 11299
Intake Manifold Pressure (psi)61.2 61.0 61.5 61.2
Intake Manifold Temp °F N/A N/A N/A N/A
Engine Load (BHP)2250.0 2250.0 2250.0 2250.0
Ambient Temp °F 51.0 54.0 54.0 53.0
Humidity %43.0 39.0 39.0 40.3
Dew Point °F 29.0 29.0 29.0 29.0
Waukesha
N/A
N/A
Yes
N/A N/A N/A N/A
3 3 3 3# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1035.0
1071.0
6.0Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.09
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.05
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.05
Average:VOC 0.07
Average:Oxygen 0.04
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 100.91
Tolerance 2.00%
Difference between measured and expected 0.91%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 1.29
Average:Nitrogen monoxide NO 0.16
Average:Nitrogen dioxide NO2 0.04
Average:NOx 0.20
Average:VOC 0.28
Average:Oxygen 0.15
Pre-test System Zero Time:
Mechanical Response Time 5 seconds
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 100.06
Tolerance 5.00%
Difference between measured and expected 0.06%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 249.86
Value:Spike Expected 251.20
System (Equilibration) Response Time Target (Spike)
7 secondsSystem Zero Response Time
45 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC524646 12/30/2027 104.20 10.71%
CC312964 10/17/2032 100.00
CC337712 5/1/2032 21.15%
Cylinder # CC230781 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 251.20 501.50 251.30 10.03
Analyzer System Response 249.86 498.22 255.24 9.90
Percent Difference 0.53%0.65%1.57%1.26%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 100.905 5.045
Spike Direct
Propane 251.612
Mechanical
Response Time
SF6 9.963
CO 500.221
NO 255.830
Ethylene 100.065 5 seconds
Analyzer
Response
Propane 249.857
SF6 9.904
CO 498.217
NO 255.244
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 250.914
CO 502.619
NO 256.072
11 seconds
7 seconds
8.77%
8.71%
8.62%
92.96%
93.67%
93.79%
9.913
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
14
11
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
189132.3
H2O%d @ Sampling Point:18.15
CO2%d @ Sampling Point:11.88
Pressure @ Sampling Point (Pg "H2O):0.48
Temperature @ Sampling Point (Deg F):935.19
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 100 100.91 5.045 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 100.905 5.045
Spike Direct
Propane 251.612
Mechanical
Response Time
SF6 9.963
CO 500.221
NO 255.830
Ethylene 100.065 5 seconds
Analyzer
Response
Propane 249.857
SF6 9.904
CO 498.217
NO 255.244
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 250.914
CO 502.619
NO 256.072
11 seconds
7 seconds
8.77%
8.71%
8.62%
92.96%
93.67%
93.79%
9.913
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
251.200
10.030
501.500
251.300
251.612
9.963
500.221
255.830
0.16%
0.67%
0.26%
1.80%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.470
0.005
Spike Average
20.878
0.874
Dilution Factor
8.772%
Expected
22.459
% Recovery
92.960%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.868
Dilution Factor
8.712%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.001
Spike Average
0.859
Dilution Factor
8.622%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 20.309 21.653 93.790%
0.000212
0.000137
0.000207
0.000 20.495 21.880 93.670%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass1.47%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-.71986622 Pass
Line Position Difference:Resolution Difference to Reference 1.47%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
100.00
99.42
0.58%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 1451; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
3/24/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
3/24/2025
Cody Hall
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 18S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Cody Hall
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:1451
Make:Waukesha
Location:9394 GSIModel:
1658736Serial Number:
RAW Result Data
Stability
3/24/2025 05:57 0.2070.0000.031 0.000 0.0000.141 0.043 0.000 0.0000.0229.715 1.067 0.0840.067 0.039 848.00.870.000 0.001 0.21 0.24 181.0
Pre Test Baseline Direct
3/24/2025 07:42 0.0000.1450.009 0.000 0.0000.108 0.018 0.000 0.0120.0410.500 0.124 0.0000.000 0.000 845.00.080.000 0.001 0.14 0.12 180.0
3/24/2025 07:43 0.0040.0020.001 0.002 0.0000.075 0.009 0.027 0.0000.0000.109 0.000 0.0000.046 0.000 845.00.000.000 0.000 0.01 0.00 180.0
3/24/2025 07:43 0.0000.000-0.002 0.000 0.0600.089 0.007 0.045 0.0000.0000.000 0.141 0.0000.167 0.000 845.00.120.046 0.000 0.00 0.00 180.0
CTS Direct
3/24/2025 07:51 0.0090.5450.012 0.020 0.0000.000 0.000 0.068 0.0470.0000.000 101.034 0.0450.003 0.023 845.067.450.000 0.000 0.55 0.06 180.0
3/24/2025 07:51 0.1160.2530.011 0.012 0.0000.000 0.000 0.082 0.0640.0000.000 100.810 0.0370.098 0.017 845.067.280.000 0.000 0.37 0.06 180.0
3/24/2025 07:52 0.2000.2270.010 0.017 0.0000.000 0.000 0.213 0.0820.0030.000 100.871 0.0330.075 0.018 845.067.320.000 0.000 0.43 0.06 180.0
High O2 Direct
3/24/2025 07:57 0.0000.1390.002 0.000 0.0000.003 0.000 0.000 0.0170.0000.041 0.018 0.0080.000 0.001 845.00.020.000 0.003 0.14 21.12 180.0
3/24/2025 07:57 0.0000.0000.000 0.003 0.0990.000 0.000 0.000 0.0090.0430.000 0.126 0.0000.000 0.000 845.00.080.000 0.003 0.00 21.12 180.0
3/24/2025 07:58 0.1610.1410.002 0.000 0.1220.000 0.000 0.000 0.0520.0460.000 0.334 0.0060.000 0.011 845.00.250.000 0.002 0.30 21.13 180.0
NO2/Mid O2 Direct
3/24/2025 08:04 104.2540.7700.002 0.000 0.7060.000 0.947 0.000 1.7240.0000.159 0.000 0.0000.000 0.000 845.00.000.000 0.000 105.02 10.69 180.0
3/24/2025 08:05 105.4080.6860.001 0.000 0.6800.000 0.939 0.000 1.5810.0000.630 0.000 0.0000.000 0.000 845.00.000.000 0.000 106.09 10.69 179.0
3/24/2025 08:05 104.1250.2570.000 0.000 0.8030.000 0.942 0.000 1.6820.0000.788 0.000 0.0000.000 0.000 845.00.000.000 0.000 104.38 10.68 180.0
Spike Direct
3/24/2025 08:13 0.000255.5610.002 4.871 1.622499.890 2.315 1.146 10.4060.2660.210 1.000 251.6380.067 0.000 845.0253.962.478 9.978 255.56 0.02 180.0
3/24/2025 08:14 0.000256.1410.002 4.878 1.812500.686 2.295 1.631 10.4260.0940.233 1.050 251.6890.000 0.000 845.0254.052.485 9.962 256.14 0.02 180.0
3/24/2025 08:14 0.000255.7880.001 4.893 5.010500.086 2.314 1.623 10.6180.2250.460 1.105 251.5080.000 0.000 845.0253.852.408 9.948 255.79 0.02 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
3/24/2025 08:16 0.0000.0000.025 0.006 0.0001.430 0.000 0.696 0.0000.0010.000 0.000 0.1690.000 0.049 845.00.270.000 0.000 0.00 0.16 180.0
3/24/2025 08:16 0.0000.1870.022 0.012 0.0841.261 0.000 0.451 0.0000.0000.000 0.070 0.2350.000 0.041 845.00.360.000 0.000 0.19 0.15 180.0
3/24/2025 08:17 0.1210.2890.019 0.000 0.0561.175 0.004 0.616 0.0000.0000.000 0.048 0.1740.035 0.000 845.00.210.000 0.000 0.41 0.14 180.0
CTS System with Response Time
3/24/2025 08:19 0.0000.0000.031 0.019 0.0000.745 0.000 0.369 0.0000.0000.000 100.149 0.2120.000 0.025 845.067.030.000 0.000 0.00 0.06 180.0
3/24/2025 08:19 0.0000.0000.029 0.009 0.0000.726 0.000 0.497 0.0000.0000.000 100.142 0.2150.119 0.009 845.067.000.000 0.000 0.00 0.06 180.0
3/24/2025 08:20 0.0000.0000.030 0.015 0.0000.619 0.000 0.392 0.0000.0000.000 99.903 0.2070.000 0.000 845.066.810.000 0.000 0.00 0.06 180.0
NO2/Mid O2 System with Response Time
3/24/2025 08:22 101.1512.6140.016 0.008 0.0740.627 0.953 0.416 0.0330.0000.000 0.000 0.0000.080 0.139 845.00.380.147 0.000 103.77 10.75 180.0
3/24/2025 08:22 102.2312.4010.016 0.010 0.1880.658 0.958 0.425 0.3090.0000.000 0.000 0.0000.094 0.111 845.00.260.057 0.003 104.63 10.77 180.0
3/24/2025 08:22 103.8322.2300.014 0.004 0.0070.560 0.965 0.420 0.5720.0000.000 0.000 0.0000.182 0.067 845.00.200.101 0.000 106.06 10.70 180.0
Spike System with Response Time
3/24/2025 08:25 0.000255.5530.016 4.861 0.726498.914 2.304 1.539 7.0550.1390.992 1.186 250.1100.000 0.000 845.0252.522.431 9.912 255.55 0.02 180.0
3/24/2025 08:26 0.000255.1400.017 4.860 0.656498.038 2.274 1.643 7.1470.0981.014 1.200 249.8030.000 0.000 846.0252.302.545 9.904 255.14 0.02 180.0
3/24/2025 08:26 0.000255.0390.017 4.848 0.877497.700 2.296 1.593 7.1840.0980.861 1.193 249.6590.000 0.000 846.0252.202.619 9.897 255.04 0.02 180.0
Baseline System with Response Time
3/24/2025 08:29 0.0000.3410.012 0.006 0.0000.755 0.000 0.187 0.0000.0000.000 0.168 0.2410.059 0.000 846.00.360.011 0.001 0.34 0.00 180.0
3/24/2025 08:30 0.0000.0000.010 0.003 0.0000.660 0.000 0.245 0.0000.0000.000 0.000 0.1320.007 0.000 846.00.130.000 0.003 0.00 0.11 180.0
3/24/2025 08:30 0.0000.1650.012 0.000 0.0350.654 0.020 0.327 0.0000.0000.000 0.280 0.1910.000 0.000 846.00.380.000 0.001 0.16 0.00 180.0
Run 1 - A 30minute/60min
3/24/2025 09:02 4.05728.39711.622 7.725 57.21416.090 3.891 2.202 0.0000.1240.000 0.000 14.1101.090 2.832 846.019.770.000 0.140 32.45 0.58 180.0
3/24/2025 09:03 0.0008.56717.118 9.791 70.8891.822 4.243 0.000 1.5090.0000.841 0.000 0.0001.006 0.326 846.00.770.171 0.000 8.57 0.50 180.0
3/24/2025 09:04 0.2756.55718.068 9.728 71.0811.422 4.325 0.000 1.4940.0001.102 0.000 0.0001.079 0.255 846.00.670.235 0.000 6.83 0.46 180.0
3/24/2025 09:05 0.5727.58518.304 9.597 78.1591.151 4.324 0.000 2.0030.0000.752 0.097 0.0001.087 0.239 846.00.720.258 0.000 8.16 0.41 180.0
3/24/2025 09:06 0.1996.79818.145 9.523 81.7803.128 4.976 0.000 1.3160.0000.244 0.081 0.0000.870 0.286 846.00.840.320 0.000 7.00 0.45 180.0
3/24/2025 09:07 0.00010.94818.179 9.675 74.7211.791 5.153 0.000 2.0940.0000.043 0.000 0.0001.096 0.215 846.00.610.276 0.000 10.95 0.46 180.0
3/24/2025 09:08 0.6406.69418.247 9.713 72.5791.091 3.725 0.000 1.9970.0000.512 0.151 0.0001.058 0.215 846.00.870.503 0.000 7.33 0.42 180.0
3/24/2025 09:09 0.1267.46818.356 9.641 83.3861.287 5.192 0.000 1.3800.0001.117 0.000 0.0000.945 0.264 846.00.810.427 0.000 7.59 0.44 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/24/2025 09:10 0.3449.66618.449 9.723 73.7192.473 4.376 0.000 2.0220.0000.637 0.000 0.0000.964 0.219 846.00.670.345 0.000 10.01 0.42 180.0
3/24/2025 09:11 0.2855.95618.505 9.663 81.1281.212 4.265 0.018 1.2800.0001.328 0.000 0.0000.824 0.248 846.00.840.516 0.000 6.24 0.40 180.0
3/24/2025 09:12 0.68410.07718.536 9.711 72.1662.489 4.128 0.000 1.8830.0001.138 0.000 0.0001.032 0.194 846.00.630.361 0.000 10.76 0.36 180.0
3/24/2025 09:13 0.63713.63518.599 9.670 72.7062.649 4.319 0.106 1.9270.0001.166 0.000 0.0001.096 0.192 846.00.620.353 0.000 14.27 0.40 180.0
3/24/2025 09:14 0.44810.18918.592 9.665 73.7183.050 5.155 0.354 1.9930.0001.137 0.000 0.0000.927 0.204 846.00.720.465 0.000 10.64 0.42 180.0
3/24/2025 09:15 0.8597.61018.549 9.703 76.8011.046 3.988 0.343 2.0360.0001.272 0.000 0.0001.113 0.193 846.00.640.378 0.000 8.47 0.41 180.0
3/24/2025 09:16 0.5569.52418.485 9.675 71.0680.829 3.816 0.275 1.6620.0001.344 0.000 0.0000.963 0.187 846.00.600.342 0.000 10.08 0.37 180.0
3/24/2025 09:17 0.2335.43618.323 9.663 82.5541.295 4.783 0.244 1.4250.0001.773 0.004 0.0000.973 0.245 846.00.770.416 0.000 5.67 0.40 180.0
3/24/2025 09:18 0.9097.59018.242 9.670 73.5510.794 4.230 0.125 1.8050.0000.853 0.000 0.0001.085 0.195 846.00.680.431 0.000 8.50 0.41 180.0
3/24/2025 09:19 0.9649.23718.226 9.762 71.1021.270 3.566 0.000 1.7820.0000.521 0.000 0.0001.060 0.180 846.00.630.406 0.000 10.20 0.32 180.0
3/24/2025 09:20 0.8706.38718.230 9.781 78.6211.656 4.526 0.278 2.0990.0000.958 0.000 0.0001.223 0.208 846.00.710.442 0.000 7.26 0.39 180.0
3/24/2025 09:21 0.9236.53018.220 9.796 74.7910.880 4.073 0.138 1.8230.0000.902 0.000 0.0000.985 0.208 846.00.720.449 0.000 7.45 0.40 180.0
3/24/2025 09:22 0.9618.11518.220 9.806 70.6340.660 3.979 0.194 1.5570.0001.009 0.000 0.0000.990 0.195 846.00.670.424 0.000 9.08 0.38 180.0
3/24/2025 09:23 0.8727.62118.212 9.805 77.5960.903 4.227 0.157 2.0550.0000.984 0.000 0.0000.983 0.201 846.00.680.422 0.000 8.49 0.40 180.0
3/24/2025 09:24 0.7789.07118.201 9.814 72.9930.815 4.191 0.178 1.7970.0000.931 0.000 0.0000.973 0.192 846.00.690.460 0.000 9.85 0.39 180.0
3/24/2025 09:25 0.4839.81518.196 9.807 76.5281.092 4.507 0.353 1.9080.0001.042 0.000 0.0001.077 0.209 846.00.710.433 0.000 10.30 0.41 180.0
3/24/2025 09:26 0.87013.79218.194 9.805 73.9782.370 4.200 0.279 1.9000.0001.130 0.000 0.0001.051 0.234 846.00.750.419 0.000 14.66 0.41 180.0
3/24/2025 09:27 0.3328.22818.229 9.815 75.4441.785 4.302 0.442 1.9930.0001.195 0.000 0.0001.014 0.213 846.00.720.449 0.000 8.56 0.38 180.0
3/24/2025 09:28 0.1337.24018.212 9.801 81.2911.279 4.250 0.509 1.2630.0000.551 0.000 0.0001.023 0.279 846.00.840.425 0.000 7.37 0.38 180.0
3/24/2025 09:29 0.3517.77318.225 9.819 76.4311.274 4.335 0.398 2.0700.0001.201 0.000 0.0001.000 0.209 846.00.690.406 0.000 8.12 0.41 180.0
3/24/2025 09:30 0.8546.55018.207 9.812 76.2071.011 4.301 0.375 1.9570.0001.397 0.000 0.0001.084 0.234 845.00.710.359 0.000 7.40 0.41 180.0
3/24/2025 09:31 0.52910.05918.192 9.792 75.5500.744 4.271 0.413 2.0380.0001.460 0.000 0.0001.048 0.204 846.00.710.448 0.000 10.59 0.35 180.0
0.6589.10418.036 9.665 74.9461.979 4.321 0.246 1.7360.0040.951 0.011 0.4701.024 0.309 845.971.3490.378 0.005 9.762 0.411 180.0Avg.
Spike 1
3/24/2025 10:00 6.51931.06316.423 8.861 70.50049.870 5.064 0.104 2.8050.0000.000 3.636 20.8780.832 0.338 846.023.980.000 0.874 37.58 0.57 180.0
Run 1 - B 30minute/60min
3/24/2025 10:04 0.43212.54418.068 9.765 69.4681.354 4.299 0.164 1.6110.0000.957 0.000 0.0000.884 0.210 846.00.740.487 0.000 12.98 0.56 180.0
3/24/2025 10:05 0.76610.17318.089 9.771 68.6271.151 4.113 0.023 1.5910.0000.622 0.000 0.0000.882 0.214 846.00.720.440 0.000 10.94 0.56 180.0
3/24/2025 10:06 0.4969.51818.075 9.766 74.0360.912 4.341 0.114 1.8450.0000.850 0.000 0.0000.999 0.219 846.00.710.402 0.000 10.01 0.56 180.0
3/24/2025 10:07 0.49213.40418.072 9.747 65.5050.988 4.071 0.032 1.3770.0000.725 0.000 0.0000.945 0.222 846.00.710.405 0.000 13.90 0.56 180.0
3/24/2025 10:08 0.68810.99918.082 9.741 69.5780.926 4.289 0.046 1.6020.0000.756 0.000 0.0000.883 0.201 846.00.700.445 0.000 11.69 0.56 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/24/2025 10:09 0.6917.68918.092 9.724 67.2250.564 4.141 0.008 1.2830.0000.794 0.000 0.0000.970 0.201 846.00.680.415 0.000 8.38 0.56 180.0
3/24/2025 10:10 0.63612.22418.123 9.725 66.1480.664 4.654 0.007 1.4660.0000.877 0.000 0.0000.933 0.204 846.00.710.451 0.000 12.86 0.56 180.0
3/24/2025 10:11 0.78513.21818.106 9.737 62.1030.913 4.472 0.000 1.2890.0000.654 0.000 0.0000.862 0.198 846.00.650.386 0.000 14.00 0.56 180.0
3/24/2025 10:12 0.75911.82218.100 9.750 70.3410.686 4.386 0.000 1.7060.0001.012 0.000 0.0000.944 0.207 846.00.660.375 0.000 12.58 0.55 180.0
3/24/2025 10:13 0.58412.61418.103 9.752 65.7900.660 4.088 0.015 1.4070.0000.826 0.000 0.0000.921 0.206 846.00.700.436 0.000 13.20 0.56 180.0
3/24/2025 10:14 0.72110.19518.111 9.758 70.5221.030 4.880 0.000 1.6730.0001.091 0.000 0.0000.940 0.210 846.00.710.430 0.000 10.92 0.55 180.0
3/24/2025 10:15 0.63612.51818.089 9.756 66.1200.936 4.210 0.052 1.5440.0000.421 0.000 0.0000.994 0.199 846.00.660.391 0.000 13.15 0.56 180.0
3/24/2025 10:16 0.80312.69118.101 9.741 67.2571.176 4.469 0.000 1.6880.0001.095 0.020 0.0000.978 0.206 846.00.740.470 0.001 13.49 0.56 180.0
3/24/2025 10:17 0.7737.99518.084 9.741 69.2211.038 4.277 0.042 1.6450.0000.898 0.000 0.0000.893 0.212 846.00.750.489 0.000 8.77 0.55 180.0
3/24/2025 10:18 0.7699.55718.098 9.752 62.6210.559 4.534 0.000 1.1840.0000.694 0.000 0.0000.899 0.211 846.00.700.424 0.000 10.33 0.55 180.0
3/24/2025 10:19 0.7319.33618.140 9.781 63.6310.580 4.381 0.000 1.2210.0000.950 0.000 0.0000.910 0.200 846.00.680.421 0.000 10.07 0.55 180.0
3/24/2025 10:20 0.56911.84218.155 9.781 64.7520.560 4.578 0.013 1.2350.0000.854 0.000 0.0000.921 0.203 846.00.700.439 0.000 12.41 0.54 180.0
3/24/2025 10:21 0.7397.13118.130 9.781 68.7230.902 4.088 0.000 1.5470.0001.219 0.000 0.0000.934 0.213 846.00.730.459 0.000 7.87 0.56 180.0
3/24/2025 10:22 0.81613.66118.146 9.772 61.5410.452 4.968 0.000 1.3260.0000.775 0.073 0.0000.879 0.205 846.00.670.318 0.000 14.48 0.55 180.0
3/24/2025 10:23 0.51512.46318.127 9.761 64.5530.829 4.388 0.061 1.3460.0001.092 0.000 0.0000.933 0.208 846.00.680.393 0.000 12.98 0.55 180.0
3/24/2025 10:24 0.91111.68218.123 9.748 66.9940.779 4.281 0.051 1.4410.0000.958 0.000 0.0000.893 0.188 846.00.690.478 0.000 12.59 0.55 180.0
3/24/2025 10:25 0.9478.93718.064 9.708 69.5360.658 4.306 0.045 1.4540.0001.012 0.000 0.0000.947 0.205 846.00.730.473 0.000 9.88 0.56 180.0
3/24/2025 10:26 0.52212.45518.113 9.733 71.4800.620 4.573 0.027 1.6270.0001.489 0.000 0.0000.904 0.208 846.00.730.478 0.000 12.98 0.54 180.0
3/24/2025 10:27 0.5828.29918.137 9.735 71.5670.952 3.970 0.000 1.8350.0001.119 0.000 0.0000.929 0.189 846.00.720.518 0.000 8.88 0.55 180.0
3/24/2025 10:29 0.7478.76918.140 9.743 66.4830.496 4.010 0.058 1.5090.0001.125 0.000 0.0000.861 0.196 846.00.740.520 0.000 9.52 0.55 180.0
3/24/2025 10:30 0.62013.98718.140 9.764 67.7170.608 4.923 0.000 1.4780.0001.127 0.000 0.0000.893 0.206 846.00.700.430 0.000 14.61 0.54 180.0
3/24/2025 10:31 0.73716.08018.154 9.774 59.3820.558 4.417 0.000 1.2210.0001.020 0.090 0.0000.906 0.192 846.00.750.462 0.000 16.82 0.56 180.0
3/24/2025 10:32 0.83316.78218.099 9.751 62.3550.983 5.160 0.000 1.2230.0000.783 0.000 0.0000.951 0.208 846.00.710.443 0.000 17.62 0.54 180.0
3/24/2025 10:33 0.72311.71518.115 9.784 65.9630.934 4.465 0.000 1.4910.0000.633 0.000 0.0000.935 0.205 846.00.740.500 0.000 12.44 0.55 180.0
3/24/2025 10:34 0.91817.53518.124 9.768 61.1600.473 4.573 0.000 1.1150.0000.569 0.000 0.0000.925 0.210 846.00.720.455 0.000 18.45 0.56 180.0
0.69811.59518.110 9.754 66.6800.798 4.410 0.025 1.4660.0000.900 0.006 0.0000.922 0.205 846.000.7080.441 0.000 12.293 0.554 180.0Avg.
0.67810.34918.073 9.709 70.8131.388 4.365 0.136 1.6010.0020.926 0.009 0.2350.973 0.257 845.981.0280.410 0.002 11.027 0.483 180.0Run 1 Avg:
Baseline 1
3/24/2025 10:37 0.0000.1900.028 0.011 0.0000.702 0.011 0.000 0.0000.0000.000 0.029 0.0000.000 0.086 846.00.190.000 0.003 0.19 0.12 180.0
Run 2 - A 30minute/60min
3/24/2025 10:44 0.94616.55518.137 9.739 65.3370.655 5.012 0.032 1.5900.0001.343 0.000 0.0000.930 0.193 846.00.710.492 0.000 17.50 0.56 180.0
3/24/2025 10:45 0.7889.92818.156 9.751 72.4681.164 4.316 0.136 1.8690.0001.600 0.000 0.0000.886 0.213 846.00.740.470 0.000 10.72 0.55 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/24/2025 10:46 0.8509.69418.106 9.743 68.4110.435 4.565 0.082 1.5750.0001.594 0.000 0.0000.834 0.212 846.00.750.484 0.000 10.54 0.55 180.0
3/24/2025 10:47 0.91310.39618.129 9.753 67.4270.514 4.139 0.014 1.3790.0001.235 0.000 0.0000.818 0.215 846.00.750.486 0.000 11.31 0.55 180.0
3/24/2025 10:48 0.9726.60118.149 9.757 70.6951.088 4.152 0.077 1.6330.0001.533 0.000 0.0000.904 0.208 846.00.730.478 0.000 7.57 0.55 180.0
3/24/2025 10:49 0.8695.78718.133 9.761 73.1090.903 4.147 0.031 1.9070.0001.400 0.000 0.0000.841 0.211 846.00.720.446 0.000 6.66 0.56 180.0
3/24/2025 10:50 0.8298.53718.140 9.754 67.6530.722 4.458 0.053 1.5500.0001.227 0.000 0.0000.871 0.197 846.00.690.450 0.000 9.37 0.56 180.0
3/24/2025 10:51 0.86813.73018.118 9.765 64.3570.390 4.323 0.094 1.4490.0001.013 0.040 0.0000.921 0.212 846.00.710.393 0.000 14.60 0.55 180.0
3/24/2025 10:52 0.8116.75818.120 9.762 67.4710.680 4.060 0.017 1.5480.0001.280 0.000 0.0000.816 0.205 846.00.700.436 0.000 7.57 0.55 180.0
3/24/2025 10:53 0.67612.00318.128 9.766 67.2840.484 4.775 0.000 1.4840.0001.176 0.000 0.0000.895 0.208 846.00.650.357 0.000 12.68 0.54 180.0
3/24/2025 10:54 0.78213.28918.137 9.768 63.8041.968 4.100 0.049 1.4120.0001.007 0.000 0.0000.908 0.221 846.00.710.402 0.000 14.07 0.55 180.0
3/24/2025 10:55 0.8459.61618.129 9.773 66.1440.721 4.445 0.068 1.4870.0001.245 0.000 0.0000.905 0.200 846.00.650.377 0.000 10.46 0.54 180.0
3/24/2025 10:56 1.31417.84918.140 9.779 57.8580.332 4.505 0.060 1.1790.0000.971 0.000 0.0000.869 0.192 846.00.630.364 0.000 19.16 0.55 180.0
3/24/2025 10:57 0.8239.40618.126 9.774 66.6340.689 4.309 0.000 1.4460.0001.050 0.000 0.0000.883 0.197 846.00.680.427 0.000 10.23 0.53 180.0
3/24/2025 10:58 0.92912.77918.139 9.785 63.7820.522 4.086 0.000 1.4340.0001.132 0.000 0.0000.881 0.184 846.00.630.399 0.000 13.71 0.55 180.0
3/24/2025 10:59 0.97212.52618.114 9.780 66.9510.658 4.788 0.027 1.5590.0001.143 0.000 0.0000.894 0.203 846.00.710.462 0.000 13.50 0.54 180.0
3/24/2025 11:00 0.93611.82718.125 9.779 66.2592.121 3.811 0.041 1.5010.0001.163 0.000 0.0000.852 0.201 846.00.690.425 0.000 12.76 0.56 180.0
3/24/2025 11:01 0.6989.77418.133 9.755 75.1511.805 4.898 0.303 2.0440.0001.621 0.000 0.0001.032 0.222 846.00.710.402 0.000 10.47 0.54 180.0
3/24/2025 11:02 1.15113.52318.130 9.747 65.9930.368 4.211 0.234 1.2820.0001.606 0.000 0.0000.871 0.203 846.00.720.468 0.000 14.67 0.54 180.0
3/24/2025 11:03 0.80911.18118.140 9.744 70.0991.254 4.285 0.318 1.5650.0001.646 0.000 0.0000.895 0.207 846.00.720.466 0.000 11.99 0.55 180.0
3/24/2025 11:04 0.9239.28218.124 9.738 70.8660.416 4.064 0.083 1.6110.0001.742 0.000 0.0000.958 0.208 846.00.710.437 0.000 10.20 0.55 180.0
3/24/2025 11:06 0.97810.40518.143 9.761 64.6000.529 4.294 0.029 1.3110.0001.590 0.000 0.0000.834 0.191 846.00.670.428 0.000 11.38 0.54 180.0
3/24/2025 11:07 0.99115.33418.140 9.758 58.6590.042 4.289 0.036 0.9940.0001.382 0.000 0.0000.803 0.177 846.00.660.451 0.000 16.32 0.53 180.0
3/24/2025 11:08 0.94313.87218.126 9.754 62.7490.274 4.140 0.007 1.1810.0001.409 0.000 0.0000.882 0.201 846.00.650.379 0.000 14.81 0.53 180.0
3/24/2025 11:09 0.9476.62218.123 9.754 69.2290.576 4.142 0.046 1.5150.0001.446 0.000 0.0000.920 0.221 846.00.700.382 0.000 7.57 0.53 180.0
3/24/2025 11:10 1.09915.95818.130 9.786 56.6190.099 4.507 0.056 0.9020.0001.136 0.000 0.0000.894 0.207 846.00.670.383 0.000 17.06 0.54 180.0
3/24/2025 11:11 1.14718.59118.114 9.762 62.6464.757 5.217 0.370 1.3810.0001.118 0.000 0.0000.902 0.204 846.00.710.459 0.000 19.74 0.53 180.0
3/24/2025 11:12 0.82811.87118.129 9.793 64.0470.873 4.940 0.206 1.2360.0001.045 0.000 0.0000.969 0.229 846.00.660.308 0.000 12.70 0.53 180.0
3/24/2025 11:13 1.596326.99218.131 9.722 51.3110.025 11.846 0.075 0.7890.0000.713 0.000 0.0000.838 0.207 846.00.630.329 0.000 328.59 0.53 180.0
3/24/2025 11:14 0.62034.81118.245 9.740 68.42026.303 3.658 2.106 2.2970.0000.274 0.000 0.0000.873 0.273 846.00.710.249 0.000 35.43 0.40 180.0
0.92822.85018.134 9.760 65.8681.712 4.616 0.155 1.4700.0001.261 0.001 0.0000.886 0.207 846.000.6920.416 0.000 23.778 0.539 180.0Avg.
Spike 2
3/24/2025 11:21 2.87930.80816.563 9.349 59.29548.793 4.870 0.661 2.2300.0000.000 2.273 20.4950.882 0.385 846.022.930.222 0.868 33.69 0.55 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
3/24/2025 11:24 0.76315.65518.164 9.730 56.5840.424 4.164 0.304 0.9190.0001.070 0.000 0.0000.799 0.245 846.00.630.213 0.000 16.42 0.54 180.0
3/24/2025 11:25 0.7836.98118.179 9.761 68.1161.926 4.033 0.456 1.3530.0001.525 0.000 0.0000.905 0.241 846.00.630.217 0.000 7.76 0.54 180.0
3/24/2025 11:26 1.00216.28318.156 9.753 64.7490.626 4.590 0.482 1.2950.0000.176 0.000 0.0000.917 0.239 846.00.660.268 0.000 17.28 0.54 180.0
3/24/2025 11:27 0.79314.46518.155 9.754 59.5290.345 3.964 0.211 0.8630.0001.169 0.000 0.0000.915 0.238 846.00.780.455 0.000 15.26 0.55 180.0
3/24/2025 11:28 0.86711.05518.156 9.759 62.1580.468 4.025 0.161 1.1550.0001.088 0.000 0.0000.928 0.226 846.00.730.420 0.000 11.92 0.53 180.0
3/24/2025 11:29 0.8469.70118.152 9.777 60.8191.428 4.041 0.129 0.9940.0001.376 0.000 0.0000.916 0.229 846.00.700.360 0.000 10.55 0.53 180.0
3/24/2025 11:30 0.98112.53918.173 9.781 61.8341.788 4.236 0.274 1.1700.0000.814 0.000 0.0000.956 0.238 846.00.740.393 0.000 13.52 0.53 180.0
3/24/2025 11:31 0.7707.16718.148 9.793 76.4971.768 4.326 0.725 1.8840.0000.311 0.000 0.0000.857 0.258 846.00.670.226 0.000 7.94 0.53 180.0
3/24/2025 11:32 0.6966.95618.138 9.792 70.0831.881 4.273 0.586 1.4680.0000.449 0.000 0.0000.917 0.251 846.00.720.321 0.000 7.65 0.54 180.0
3/24/2025 11:33 0.93810.87718.141 9.793 60.7100.553 4.096 0.378 1.1090.0001.150 0.000 0.0000.987 0.221 846.00.730.427 0.000 11.82 0.54 180.0
3/24/2025 11:34 0.9207.85618.132 9.798 65.2284.257 4.005 0.333 1.2670.0001.158 0.000 0.0000.957 0.257 846.00.740.336 0.000 8.78 0.55 180.0
3/24/2025 11:35 0.88511.59018.119 9.803 60.9781.110 4.389 0.560 1.0220.0000.547 0.000 0.0000.824 0.249 846.00.680.274 0.001 12.48 0.55 180.0
3/24/2025 11:36 1.1067.35218.181 9.807 61.1990.521 4.181 0.204 1.1080.0000.867 0.000 0.0000.901 0.222 846.00.700.387 0.000 8.46 0.43 180.0
3/24/2025 11:37 1.74432.34718.252 9.846 44.2610.000 5.974 0.108 0.4170.0000.636 0.000 0.0000.690 0.221 846.00.710.396 0.000 34.09 0.43 180.0
3/24/2025 11:38 0.90910.88318.254 9.808 63.1801.392 3.959 0.082 1.1980.0001.266 0.000 0.0000.887 0.250 846.00.690.282 0.000 11.79 0.45 180.0
3/24/2025 11:39 0.86720.45018.257 9.817 61.7480.422 5.054 0.116 0.9860.0001.323 0.000 0.0000.989 0.233 846.00.680.320 0.000 21.32 0.51 180.0
3/24/2025 11:41 0.69955.31018.334 9.798 36.9140.000 6.390 0.007 0.2620.0000.603 0.000 0.0000.643 0.225 845.00.660.323 0.000 56.01 0.50 180.0
3/24/2025 11:42 1.17133.19618.335 9.786 47.6230.000 4.661 0.000 0.4440.0000.918 0.000 0.0000.877 0.213 845.00.710.420 0.000 34.37 0.51 180.0
3/24/2025 11:43 1.17726.69218.355 9.768 55.8920.214 4.263 0.053 0.8190.0001.042 0.000 0.0000.799 0.209 845.00.750.504 0.000 27.87 0.50 180.0
3/24/2025 11:44 0.84525.96818.357 9.761 58.8770.626 4.805 0.065 1.0300.0001.559 0.000 0.0000.692 0.224 845.00.700.381 0.000 26.81 0.49 180.0
3/24/2025 11:45 0.8076.40918.328 9.723 68.7950.798 4.046 0.088 1.1700.0001.623 0.000 0.0000.790 0.244 845.00.690.303 0.000 7.22 0.51 179.0
3/24/2025 11:46 1.04714.57718.375 9.767 65.3040.639 4.138 0.042 1.1880.0001.241 0.000 0.0000.813 0.215 845.00.730.451 0.000 15.62 0.49 180.0
3/24/2025 11:47 0.4335.83618.306 9.760 86.0756.928 4.540 0.414 1.1110.0001.962 0.000 0.0000.905 0.322 845.00.960.478 0.000 6.27 0.51 180.0
3/24/2025 11:48 0.7445.24118.298 9.809 74.9151.640 4.142 0.514 1.6230.0000.861 0.000 0.0000.762 0.263 845.00.730.311 0.000 5.99 0.55 180.0
3/24/2025 11:49 0.6485.35118.270 9.825 75.8141.590 3.796 0.370 1.8380.0001.692 0.000 0.0000.788 0.255 845.00.760.370 0.000 6.00 0.53 180.0
3/24/2025 11:50 0.4295.68218.253 9.823 74.4471.717 4.205 0.416 1.7730.0001.382 0.000 0.0000.731 0.259 845.00.810.441 0.000 6.11 0.54 180.0
3/24/2025 11:51 1.0919.06018.222 9.813 61.3790.738 3.815 0.272 1.0210.0001.218 0.000 0.0000.782 0.241 845.00.720.353 0.000 10.15 0.53 180.0
3/24/2025 11:52 0.7567.15318.227 9.837 68.6020.927 3.651 0.203 1.3020.0001.191 0.000 0.0000.752 0.251 845.00.720.333 0.000 7.91 0.52 180.0
3/24/2025 11:53 0.9528.86018.248 9.850 60.9440.736 3.832 0.134 0.9930.0000.976 0.000 0.0000.825 0.242 845.00.720.352 0.000 9.81 0.52 180.0
3/24/2025 11:54 0.90816.00418.238 9.828 57.1150.879 4.206 0.106 0.8630.0000.637 0.000 0.0000.953 0.239 845.00.640.242 0.000 16.91 0.49 180.0
0.88614.25018.230 9.791 63.0121.211 4.327 0.260 1.1220.0001.061 0.000 0.0000.849 0.241 845.530.7160.352 0.000 15.136 0.516 180.0Avg.
0.90718.55018.182 9.775 64.4401.462 4.471 0.207 1.2960.0001.161 0.001 0.0000.867 0.224 845.770.7040.384 0.000 19.457 0.528 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
3/24/2025 11:58 0.0000.2410.022 0.000 0.0000.888 0.075 0.000 0.0000.00013.838 1.119 0.0000.038 0.154 845.01.060.008 0.000 0.24 0.11 180.0
Run 3 - A 30minute/60min
3/24/2025 12:00 0.94813.90715.201 8.088 58.0490.009 3.942 0.982 0.8540.0000.000 1.086 0.0000.866 0.364 845.01.640.284 0.000 14.85 0.50 180.0
3/24/2025 12:01 1.20711.68818.221 9.419 58.7570.694 3.722 0.091 0.8500.0000.381 0.889 0.0000.814 0.246 845.01.300.322 0.001 12.89 0.52 180.0
3/24/2025 12:02 1.26919.61018.226 9.429 54.9390.571 4.228 0.000 0.6930.0005.983 0.927 0.0000.968 0.222 845.01.300.356 0.000 20.88 0.53 180.0
3/24/2025 12:03 1.2826.72218.232 9.388 63.3480.595 3.667 0.000 0.9000.0006.211 1.192 0.0000.945 0.235 845.01.490.342 0.000 8.00 0.53 180.0
3/24/2025 12:04 1.19310.09118.230 9.404 60.5770.858 4.204 0.000 0.8530.0006.550 0.962 0.0000.947 0.229 845.01.400.444 0.000 11.28 0.54 180.0
3/24/2025 12:05 1.0557.48018.208 9.358 64.1450.869 3.779 0.000 0.9900.0006.479 0.989 0.0000.896 0.239 845.01.460.489 0.000 8.53 0.53 180.0
3/24/2025 12:06 1.15011.06718.244 9.405 63.6931.519 4.189 0.000 1.0330.0006.620 1.046 0.0000.987 0.236 845.01.470.459 0.000 12.22 0.53 180.0
3/24/2025 12:07 1.12911.08118.215 9.412 61.6730.615 4.055 0.000 0.9140.0006.274 1.034 0.0000.928 0.212 845.01.410.446 0.000 12.21 0.55 180.0
3/24/2025 12:08 1.2006.50918.231 9.392 64.9330.792 3.666 0.000 1.1010.0006.299 1.166 0.0000.961 0.210 845.01.520.484 0.000 7.71 0.52 180.0
3/24/2025 12:09 0.9396.32818.240 9.422 67.8621.829 3.909 0.000 1.2680.0006.409 1.179 0.0001.029 0.215 845.01.530.474 0.000 7.27 0.51 180.0
3/24/2025 12:10 0.9856.98718.206 9.415 68.4832.089 4.231 0.000 1.2520.0006.627 1.000 0.0001.031 0.231 845.01.400.401 0.000 7.97 0.52 180.0
3/24/2025 12:11 1.1127.20918.226 9.441 69.6332.379 4.109 0.000 1.3160.0006.579 0.863 0.0000.983 0.223 845.01.340.476 0.000 8.32 0.53 180.0
3/24/2025 12:12 0.8855.95918.232 9.463 68.8381.734 3.672 0.143 1.2750.0000.486 0.873 0.0001.049 0.259 845.01.320.324 0.000 6.84 0.54 180.0
3/24/2025 12:13 0.9806.57818.236 9.607 77.4482.224 4.077 0.000 1.8480.0001.056 0.385 0.0001.029 0.264 845.01.000.330 0.000 7.56 0.55 180.0
3/24/2025 12:14 1.0428.71118.238 9.620 65.6511.022 3.700 0.353 1.1520.0000.503 0.494 0.0001.036 0.258 845.01.010.241 0.002 9.75 0.54 180.0
3/24/2025 12:15 1.01623.77118.214 9.643 56.7710.722 4.458 0.000 0.8950.0000.245 0.308 0.0000.827 0.250 845.00.880.264 0.001 24.79 0.50 180.0
3/24/2025 12:17 0.0008.36718.228 9.653 63.9711.890 4.074 0.208 1.1410.0000.939 0.175 0.0000.986 0.281 845.00.800.177 0.002 8.37 0.52 180.0
3/24/2025 12:18 0.9947.93318.235 9.646 63.5870.978 3.859 0.126 0.9470.0000.558 0.014 0.0001.040 0.261 845.00.740.321 0.009 8.93 0.54 180.0
3/24/2025 12:19 0.8657.68018.231 9.803 66.4133.221 3.991 0.387 1.2010.0001.138 0.000 0.0000.994 0.270 845.00.710.261 0.000 8.54 0.53 180.0
3/24/2025 12:20 0.7257.16718.223 9.803 73.3042.150 4.108 0.494 1.5560.0000.539 0.000 0.0000.983 0.282 845.00.790.344 0.000 7.89 0.52 180.0
3/24/2025 12:21 0.9566.73418.220 9.825 63.5621.919 3.482 0.334 1.0400.0001.248 0.000 0.0000.922 0.268 845.00.750.327 0.000 7.69 0.51 180.0
3/24/2025 12:22 0.9208.10918.235 9.817 65.4241.149 4.075 0.448 1.1080.0001.346 0.000 0.0000.967 0.261 845.00.750.344 0.000 9.03 0.52 180.0
3/24/2025 12:23 0.67711.94318.231 9.790 63.1560.666 4.435 0.241 1.1010.0001.339 0.000 0.0000.920 0.265 845.00.740.313 0.000 12.62 0.55 180.0
3/24/2025 12:24 1.09416.79718.230 9.783 62.4661.029 4.005 0.319 0.9960.0001.306 0.000 0.0000.836 0.277 845.00.790.360 0.000 17.89 0.53 180.0
3/24/2025 12:25 0.9107.91418.263 9.797 67.9121.258 3.702 0.196 1.3250.0001.602 0.000 0.0001.007 0.261 845.00.770.365 0.000 8.82 0.47 180.0
3/24/2025 12:26 1.01015.08318.235 9.789 67.6391.004 4.693 0.529 1.2500.0000.735 0.000 0.0000.799 0.275 845.00.770.321 0.000 16.09 0.49 180.0
3/24/2025 12:27 0.75817.73618.256 9.782 64.5841.114 4.132 0.354 1.1520.0001.357 0.000 0.0000.904 0.271 845.00.700.244 0.000 18.49 0.44 180.0
3/24/2025 12:28 0.8125.54418.247 9.779 70.9141.501 4.316 0.407 1.3780.0001.623 0.000 0.0000.871 0.274 845.00.790.362 0.000 6.36 0.51 180.0
3/24/2025 12:29 1.00111.52518.260 9.814 62.6600.555 3.922 0.291 1.0390.0001.266 0.000 0.0000.944 0.252 845.00.730.339 0.000 12.53 0.52 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/24/2025 12:30 0.94814.49418.257 9.800 59.0140.607 4.254 0.280 0.8550.0001.118 0.000 0.0000.889 0.264 845.00.740.318 0.000 15.44 0.51 180.0
0.96910.35718.132 9.560 64.6471.252 4.022 0.206 1.1090.0002.761 0.486 0.0000.945 0.255 845.001.0680.351 0.001 11.325 0.520 180.0Avg.
Spike 3
3/24/2025 12:34 6.09427.64116.650 9.415 60.73548.293 4.615 0.452 1.9410.0000.000 2.263 20.3090.645 0.505 845.022.830.000 0.859 33.74 0.43 180.0
Run 3 - B 30minute/60min
3/24/2025 12:37 0.6466.44118.217 9.831 67.3430.967 4.130 0.304 1.2390.0001.426 0.000 0.0000.996 0.297 845.00.810.322 0.000 7.09 0.52 180.0
3/24/2025 12:38 1.05323.30318.239 9.846 54.6390.310 5.079 0.220 0.6770.0001.331 0.000 0.0000.882 0.294 845.00.750.249 0.000 24.36 0.53 180.0
3/24/2025 12:39 0.8906.00018.261 9.836 71.0621.212 4.074 0.205 1.5140.0001.527 0.000 0.0001.004 0.299 845.00.780.278 0.000 6.89 0.50 180.0
3/24/2025 12:40 0.8636.45418.236 9.829 69.7690.812 4.082 0.230 1.3350.0001.707 0.000 0.0000.937 0.299 845.00.830.350 0.000 7.32 0.51 180.0
3/24/2025 12:41 1.05914.05518.232 9.822 56.0750.463 4.307 0.205 0.6290.0000.870 0.000 0.0000.910 0.292 845.00.790.306 0.000 15.11 0.48 180.0
3/24/2025 12:42 0.8265.80118.230 9.819 72.1631.394 4.524 0.226 1.4530.0001.847 0.000 0.0000.971 0.301 845.00.830.340 0.000 6.63 0.51 180.0
3/24/2025 12:43 0.8466.77218.216 9.824 64.1220.602 3.963 0.281 1.0970.0001.438 0.000 0.0000.853 0.289 845.00.780.301 0.000 7.62 0.43 180.0
3/24/2025 12:44 0.68812.64518.200 9.814 71.2431.458 4.955 0.367 1.6190.0001.585 0.000 0.0000.959 0.323 845.00.820.267 0.000 13.33 0.52 180.0
3/24/2025 12:45 0.9826.51918.232 9.829 64.8470.762 3.722 0.356 1.0090.0001.523 0.000 0.0000.942 0.307 845.00.840.344 0.000 7.50 0.53 180.0
3/24/2025 12:46 0.81112.51118.230 9.798 65.6371.974 4.056 0.389 1.1920.0001.686 0.000 0.0000.939 0.291 845.00.750.246 0.000 13.32 0.51 180.0
3/24/2025 12:47 0.7367.87318.241 9.793 71.6630.922 3.919 0.401 1.3800.0001.952 0.000 0.0000.832 0.326 845.00.810.238 0.000 8.61 0.48 180.0
3/24/2025 12:48 1.09714.17318.217 9.792 62.7491.031 4.794 0.280 0.9750.0001.688 0.000 0.0001.021 0.311 845.00.780.231 0.000 15.27 0.52 179.0
3/24/2025 12:49 0.7525.93418.280 9.835 68.3451.070 4.079 0.414 1.3010.0001.790 0.000 0.0000.909 0.306 845.00.790.270 0.000 6.69 0.50 180.0
3/24/2025 12:51 0.9377.86618.211 9.822 70.2912.103 4.348 0.562 1.3770.0000.902 0.000 0.0000.953 0.317 845.00.850.325 0.000 8.80 0.50 180.0
3/24/2025 12:52 1.16812.15018.241 9.823 61.1420.506 4.165 0.397 1.0120.0001.673 0.000 0.0000.957 0.284 845.00.730.251 0.000 13.32 0.46 180.0
3/24/2025 12:53 0.9035.90018.259 9.836 69.2511.093 3.805 0.265 1.3790.0001.652 0.000 0.0000.917 0.312 845.00.780.230 0.000 6.80 0.51 180.0
3/24/2025 12:54 1.0506.61918.235 9.814 65.3570.995 4.140 0.237 1.0670.0001.520 0.000 0.0000.908 0.324 845.00.870.338 0.000 7.67 0.52 180.0
3/24/2025 12:55 1.06214.63018.232 9.827 62.3430.822 4.352 0.328 0.9740.0001.366 0.000 0.0000.804 0.306 845.00.790.266 0.000 15.69 0.37 180.0
3/24/2025 12:56 0.9879.46518.240 9.856 71.9382.646 4.928 0.334 1.6720.0001.587 0.000 0.0000.832 0.310 845.00.790.251 0.000 10.45 0.51 180.0
3/24/2025 12:57 0.9579.32518.250 9.866 64.3541.426 3.746 0.364 1.1530.0001.442 0.000 0.0000.953 0.320 845.00.860.331 0.000 10.28 0.41 180.0
3/24/2025 12:58 0.8965.86518.251 9.842 73.5591.664 4.675 0.577 1.6740.0000.891 0.000 0.0000.931 0.323 845.00.810.250 0.000 6.76 0.47 180.0
3/24/2025 12:59 1.50616.79018.242 9.830 67.4460.751 5.433 0.555 1.3850.0000.617 0.000 0.0000.844 0.306 845.00.820.306 0.000 18.30 0.53 180.0
3/24/2025 13:00 1.03513.70418.250 9.857 63.5821.934 3.783 0.413 1.1150.0001.351 0.000 0.0000.878 0.337 845.00.840.248 0.000 14.74 0.49 180.0
3/24/2025 13:01 1.07311.12218.246 9.834 64.8160.684 4.694 0.424 1.1280.0001.298 0.000 0.0000.940 0.325 845.00.790.212 0.000 12.20 0.50 180.0
3/24/2025 13:02 0.9866.10318.237 9.855 71.7951.407 4.189 0.399 1.5210.0001.647 0.000 0.0000.975 0.336 845.00.860.284 0.000 7.09 0.44 180.0
3/24/2025 13:03 0.7897.10018.295 9.856 71.0951.819 4.793 0.464 1.4680.0000.638 0.000 0.0000.957 0.333 845.00.880.319 0.000 7.89 0.46 181.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/24/2025 13:04 0.97111.42418.240 9.860 65.5011.205 4.648 0.684 1.1510.0000.754 0.000 0.0000.953 0.342 845.00.860.265 0.000 12.40 0.47 180.0
3/24/2025 13:05 0.7556.74418.241 9.828 73.0832.391 4.895 0.720 1.5480.0000.635 0.000 0.0000.868 0.342 845.00.860.264 0.000 7.50 0.48 180.0
3/24/2025 13:06 0.80710.95918.253 9.837 70.5490.891 4.793 0.721 1.3680.0000.874 0.000 0.0001.001 0.338 845.00.820.216 0.000 11.77 0.51 180.0
3/24/2025 13:07 1.29723.19118.253 9.794 59.5911.405 4.399 0.573 0.9810.0000.576 0.000 0.0000.877 0.329 845.00.830.264 0.000 24.49 0.46 180.0
0.94810.24818.240 9.830 66.8451.224 4.382 0.397 1.2460.0001.326 0.000 0.0000.923 0.314 845.000.8130.279 0.000 11.196 0.488 180.0Avg.
0.95810.30318.186 9.695 65.7461.238 4.202 0.301 1.1780.0002.043 0.243 0.0000.934 0.285 845.000.9410.315 0.000 11.261 0.504 180.0Run 3 Avg:
Baseline 3
3/24/2025 13:12 0.0000.5820.022 0.000 0.0000.686 0.028 0.095 0.0250.0004.087 0.000 0.0000.004 0.241 844.00.480.000 0.000 0.58 0.12 180.0
Post CTS
3/24/2025 13:33 0.0000.0000.025 0.000 0.0000.572 0.000 0.332 0.0750.0001.681 99.763 0.0000.000 0.279 844.067.070.000 0.000 0.00 0.06 179.0
3/24/2025 13:33 0.0000.0000.028 0.000 0.0000.565 0.000 0.238 0.0000.0000.869 98.612 0.0000.000 0.260 844.066.270.009 0.000 0.00 0.06 179.0
3/24/2025 13:33 0.0000.0000.030 0.000 0.0000.677 0.007 0.426 0.0970.0000.609 99.946 0.0000.000 0.247 844.067.230.157 0.000 0.00 0.06 179.0
3/24/2025 13:33 0.0000.0000.030 0.010 0.0000.831 0.000 0.668 0.0000.0000.448 99.371 0.0000.112 0.242 844.066.740.000 0.000 0.00 0.06 179.0
Post NO2/Mid O2
3/24/2025 13:48 108.0172.0280.013 0.000 0.0000.706 0.985 0.223 0.5250.0003.046 0.000 0.0000.241 0.193 850.00.390.000 0.000 110.04 10.89 180.0
3/24/2025 13:49 108.1141.8130.016 0.001 0.4570.697 0.997 0.422 0.3820.0000.000 0.000 0.0000.583 0.186 849.00.530.230 0.000 109.93 10.90 180.0
3/24/2025 13:49 107.6192.2070.010 0.003 0.0000.675 0.953 0.358 0.0640.0002.511 0.000 0.0000.661 0.198 849.00.500.159 0.000 109.83 10.87 180.0
3/24/2025 13:49 108.2102.0420.018 0.000 0.0000.794 1.006 0.172 0.3330.0003.075 0.000 0.0000.299 0.198 849.00.400.000 0.000 110.25 10.86 180.0
3/24/2025 13:49 107.7981.8300.012 0.000 0.4430.626 1.011 0.288 0.6520.0071.470 0.000 0.0000.282 0.199 849.00.400.000 0.000 109.63 10.88 180.0
3/24/2025 13:49 108.4161.9260.010 0.000 0.0000.736 0.991 0.079 0.2580.0001.826 0.000 0.0000.527 0.182 849.00.610.367 0.005 110.34 10.91 180.0
Post 5-Gas
3/24/2025 13:54 0.000256.0290.020 4.829 0.140503.325 2.213 1.343 7.1220.1401.425 1.247 250.4670.000 0.000 849.0253.262.941 9.923 256.03 0.02 180.0
3/24/2025 13:54 0.000255.6620.018 4.807 1.072501.149 2.239 1.309 7.0570.0611.732 1.093 250.7010.000 0.000 849.0253.242.723 9.924 255.66 0.02 180.0
3/24/2025 13:54 0.000256.3700.022 4.870 0.000502.615 2.247 1.472 6.7230.1452.381 1.338 250.5900.000 0.000 849.0253.282.691 9.895 256.37 0.02 180.0
3/24/2025 13:54 0.000256.2270.014 4.832 0.565503.385 2.285 1.430 9.7730.1661.100 1.230 251.8990.000 0.000 848.0254.372.473 9.911 256.23 0.02 180.0
End of Test Purge
3/24/2025 14:01 0.0001.0350.012 0.000 0.2331.219 0.062 0.000 0.0000.0071.058 0.000 0.3540.000 0.075 849.00.510.000 0.018 1.04 0.00 180.0
3/24/2025 14:01 0.0000.6780.013 0.011 0.0001.173 0.000 0.042 0.0980.0000.389 0.572 0.1070.100 0.161 849.00.950.212 0.010 0.68 0.00 180.0
3/24/2025 14:01 0.0000.5370.011 0.000 0.0601.094 0.071 0.031 0.0000.0001.396 0.000 0.0970.000 0.098 849.00.290.000 0.008 0.54 0.00 180.0
3/24/2025 14:01 0.0000.3110.010 0.000 0.0001.276 0.077 0.466 0.0000.0000.589 0.896 0.2530.000 0.069 849.00.990.000 0.000 0.31 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/24/2025 14:01 0.0000.4040.011 0.000 0.0421.214 0.089 0.000 0.0000.0000.876 0.000 0.0680.136 0.117 849.00.300.000 0.000 0.40 0.00 180.0
3/24/2025 14:01 0.0000.5490.007 0.000 0.0001.182 0.069 0.140 0.0000.0001.543 0.197 0.1000.064 0.072 848.00.410.055 0.001 0.55 0.00 180.0
3/24/2025 14:01 0.0000.2300.014 0.000 0.0001.166 0.060 0.185 0.0000.0001.777 0.000 0.0930.000 0.089 848.00.410.211 0.003 0.23 0.00 180.0
3/24/2025 14:02 0.0000.5080.008 0.000 0.0001.041 0.067 0.326 0.0000.0001.290 0.882 0.0000.128 0.095 848.00.780.000 0.000 0.51 0.00 180.0
3/24/2025 14:02 0.0000.0010.011 0.008 0.0001.056 0.005 0.205 0.0000.0000.273 0.161 0.0000.000 0.090 848.00.380.133 0.000 0.00 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 3/28/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:07:41 AM 11:29 AM
Source:
Unit Number: 2026-02
Serial Number: 1641315
Engine Hours:11330
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.297 0.219 0.027
30.730 13.750 1.777
2.000 0.300 1.000 0.150 0.700 0.030
0.065 0.048 0.006
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
JD HERBERT
3
Cody Hall
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 2026-02 with a serial number of 1641315 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 3/28/2025 by
Cody Hall with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were
within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2075 BHP and 1199 RPM which is 83.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 2026-02 is authorized
to operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 2026-02Unit ID
Make Waukesha Site Elevation ft.5261
Model 9394 GSI Atmospheric Pressure psi.12.07
Serial Number 1641315 Stack Diameter in.18
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2075 2075 2075 2075
1199 1200 1199 1199
Percent Load %
Intake Manifold Pressure (hg)
83.00%83.00%83.00%83.00%
93.51 94.53 93.51 93.85
Intake Manifold Temperature (F)123.00 123.00 123.00 123.00
Ambient Conditions
Ambient Temperature Dry (F)53.00 52.00 52.00 52.33
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
134918.35 133286.59 131323.62 133176.19
3820.43 3774.22 3718.64 3771.09
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %17.85%17.77%17.84%17.82%
T
e
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t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.49%0.46%0.48%0.48%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
07:41 AM 08:53 AM 10:10 AM 3/28/2025
State
NOx (mol wt) 46.01
1.386 1.431 1.565 1.461NMNEHC (ppmvw)
1.687 1.740 1.905 1.777NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
487.643 502.270 550.387 513.433 FailNMNEHC (ppbvd) @15% O2
0.006 0.006 0.006 0.0060.700 0.030 PassNMNEHC (g/hp-hr)
0.026 0.027 0.029 0.0270.170 PassNMNEHC (lbs/hr)
0.488 0.502 0.550 0.513 FailNMNEHC (ppmvd) @15% O2
0.0710.066CO (g/hp-hr)0.059 0.0652.000 0.300 Pass
CO (ppmvw)22.460 25.450 27.852 25.254
CO (ppmvd)27.340 30.950 33.900 30.730
CO (mol wt) 28.01
CO (ppmvd) @15% O2 7.902 8.936 9.795 8.878 Fail
CO (ppbvd) @15% O2 7902.034 8935.707 9794.953 8877.564 Fail
0.3230.300CO (lbs/hr)0.268 0.2971.650 Pass
NOx (g/hp-hr)0.049 0.049 0.046 0.0481.000 0.150 Pass
NOx (ppmvw)11.330 11.530 11.039 11.300
NOx (ppmvd)13.792 14.022 13.436 13.750
NOx (ppbvd) @15% O2 3986.288 4048.359 3882.074 3972.240 Fail
NOx (ppmvd) @15% O2 3.986 4.048 3.882 3.972 Fail
NOx (lbs/hr)0.222 0.223 0.211 0.2190.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
22.46
0.66
11.33 0.00 11.33
0.00%
0.38%
0.00%
17.85%
11.25 0.00 0.39%17.86%
30.93 3.57 0.40%16.23%
11.40 0.01 0.38%17.84%
0.11 0.00 0.11 0.00%0.04%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
1.27 0.11 0.00 0.11 0.00%0.04%
22.23 11.69 0.00 11.69 0.34%17.68%
79.06 32.71 1.37 34.08 0.45%16.21%
28.67 11.29 0.08 11.37 0.39%17.86%
0.86 0.08 0.00 0.08 0.00%0.04%
Avg. Wet 25.45 11.49 0.04 11.53 1.43 0.37%17.77%
NO2NO
0.15
1.45
24.66
1.41
0.18
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
25.73 11.12 0.02 11.15 0.36%17.85%
72.01 31.08 2.92 34.00 0.36%16.20%
29.97 10.88 0.05 10.93 0.39%17.84%
0.98 0.12 0.00 0.12 0.00%0.04%
0.86 0.08 0.00 0.08 0.18 0.00%0.04%
Avg. Wet 27.85 11.00 0.03 11.04 1.57 0.38%17.84%
NO2NO
0.19
1.60
25.06
1.53
NMNEHC
0.42
NO2
0.001.06
1.30
24.59
1.47
0.15
1.39
0.66
11.25
34.49
11.41
21.72
23.20
1.27
63.60
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =18 Inches or:1.5 feet or:1.77 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.43
Yes
18.00
15.00
6.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%17.85
29.89
0.39
Inches
3.01
9
14.99
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
11.71
0.32
0.00
1017.95
0.03
30.07
30.10
955.19
1414.86
512.88
27.77
68.77
121.52
164234.14
134918.35
Run 2
17.77
29.88
0.39
11.64
0.45
0.00
1007.45
0.03
29.76
29.79
959.19
1418.86
515.10
27.77
69.61
121.52
162093.92
133286.59
Run 3
17.84
29.89
0.41
11.69
0.47
0.00
1007.45
0.03
29.76
29.79
979.19
1438.86
526.22
27.77
71.42
121.52
159840.83
131323.62
17.82
29.89
0.40
11.68
0.41
0.00
1010.95
0.03
29.86
29.89
964.52
1424.19
518.07
27.77
69.93
121.52
162056.29
133176.19
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.47
Exhaust Temp F
955.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.41
0.37
0.34
955.00
955.00
956.00
0.40
0.42
0.40
956.00
956.00
954.00
0.35
0.30
0.34
954.00
954.00
955.00
0.40 955.00
0.41
0.38
0.36
955.00
956.00
956.00
0.39
0.44
0.39
956.00
955.00
955.19
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.43
Exhaust Temp F
979.00
0.44
0.41
0.47
979.00
979.00
978.00
0.40
0.38
0.36
978.00
978.00
980.00
0.39
0.34
0.36
980.00
980.00
979.00
0.39 979.00
0.44
0.41
0.43
979.00
978.00
978.00
0.47
0.43
978.00
985.00
979.190.41
Run 2
Δpstd (in) H2O
0.39
Exhaust Temp F
959.00
0.44
0.42
0.44
959.00
959.00
960.00
0.40
0.35
0.37
960.00
960.00
958.00
0.33
0.33
0.38
958.00
958.00
959.00
0.36 959.00
0.35
0.40
0.46
959.00
960.00
960.00
0.42
0.47
960.00
959.00
0.39 959.19
Pass
Strat Check
11.29Check 1
11.52Check 2
11.31Check 3
NoxGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(11.705)+ .32(.318)+ .28(87.974+.003) = 29.89 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.89(1 -.1785)+ 18.0(.1785) = 27.77 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.39*√(1414.86/(30.1*27.77)) = 68.77 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.1785)68.77*1.767((528*30.1)/ (1414.86*29.92)) = 134918.35 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 134918.346/35.315 = 3820.426 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 27.34*(20.9-15)/(20.9-.49%)) = 7.902 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(27.34*(1.164*10^-3)*3820.426*(Run Time/60))/2075 = .059 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .059*1/453.6*2075 = .268 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .268*4.38 = 1.174 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
27.34 = 22.4595*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.81%
21.05%
10.26%
10.49%
10.71%
10.71%
10.49%10.26%
10.81%
21.05%
10.71%
21.15%
10.71%
21.15%
10.71%21.15%
0.00%
10.71%
21.15%
0.10%
0.10%
0.49%
0.47%
10.71%
Span
Zero Offset 0.00%
21.15
0.00%
10.81%2.61%1.53%0.01%
0.47%
0.45%
0.47%
0.49%
0.46%
0.48%
9
GAS
0.0 0.0 0.0
0.0 0.0 0.0
1009.0 1009.0 1009.0
1053.0 1053.0 1053.0
0.7 0.7 .7
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
3/28/2025
5261
2026-02
Waukesha
Model
Serial Number
9394 GSI
1641315
Technician Cody Hall
Run Start Times 07:41 AM 08:53 AM 10:10 AM 11:29 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1199.0 1200.0 1199.0 1199.3
Engine Hours 11327 11328 11329 11330
Intake Manifold Pressure (psi)58.0 58.5 58.0 58.2
Intake Manifold Temp °F 123.0 123.0 123.0 123.0
Engine Load (BHP)2075.0 2075.0 2075.0 2075.0
Ambient Temp °F 53.0 52.0 52.0 52.3
Humidity %37.0 40.0 40.0 39.0
Dew Point °F 27.0 28.0 28.0 27.7
N/A
N/A
N/A
Yes
N/A N/A N/A N/A
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
N/A N/A N/A
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1009.0
1053.0
0.7Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.11
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 99.90
Tolerance 2.00%
Difference between measured and expected 0.10%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.57
Average:Nitrogen monoxide NO 0.37
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.37
Average:VOC 0.33
Average:Oxygen 0.11
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 99.01
Tolerance 5.00%
Difference between measured and expected 0.99%
Pre-test System CTS & Mechanical Response Time
46 secondsEquilibration Response Time
Value:Spike Reported 253.30
Value:Spike Expected 251.20
System (Equilibration) Response Time Target (Spike)
52 secondsSystem Zero Response Time
52 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC524646 12/30/2027 104.20 10.71%
CC312964 10/17/2032 100.00
CC337712 5/1/2032 21.15%
Cylinder # CC230781 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 251.20 501.50 251.30 10.03
Analyzer System Response 253.30 492.06 247.02 10.01
Percent Difference 0.84%1.88%1.70%0.17%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.901 4.995
Spike Direct
Propane 254.371
Mechanical
Response Time
SF6 10.047
CO 493.452
NO 248.013
Ethylene 99.007 19 seconds
Analyzer
Response
Propane 253.303
SF6 10.013
CO 492.061
NO 247.017
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.547
CO 493.567
NO 246.901
46 seconds
52 seconds
9.19%
9.07%
9.06%
95.25%
95.85%
97.45%
9.981
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.006
50%9.000
83.3%14.994
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
18
15
6
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
133176.19
H2O%d @ Sampling Point:17.82
CO2%d @ Sampling Point:11.68
Pressure @ Sampling Point (Pg "H2O):0.4
Temperature @ Sampling Point (Deg F):964.52
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 100 99.9 4.995 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.901 4.995
Spike Direct
Propane 254.371
Mechanical
Response Time
SF6 10.047
CO 493.452
NO 248.013
Ethylene 99.007 19 seconds
Analyzer
Response
Propane 253.303
SF6 10.013
CO 492.061
NO 247.017
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.547
CO 493.567
NO 246.901
46 seconds
52 seconds
9.19%
9.07%
9.06%
95.25%
95.85%
97.45%
9.981
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
251.200
10.030
501.500
251.300
254.371
10.047
493.452
248.013
1.26%
0.17%
1.60%
1.31%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.048
0.002
Spike Average
22.029
0.923
Dilution Factor
9.187%
Expected
23.129
% Recovery
95.250%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.006
Spike Average
0.911
Dilution Factor
9.067%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.005
Spike Average
0.910
Dilution Factor
9.057%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.088 22.256 22.839 97.450%
0.001374
0.000761
0.000410
0.060 21.890 22.838 95.850%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass3.54%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-2.49055622 Pass
Line Position Difference:Resolution Difference to Reference 3.54%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
100.00
100.44
0.44%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 2026-02; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
3/28/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
3/28/2025
Cody Hall
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 18S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Cody Hall
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:2026-02
Make:Waukesha
Location:9394 GSIModel:
1641315Serial Number:
RAW Result Data
Stability
3/28/2025 06:19 0.0540.081-0.000 0.443 0.0000.028 0.000 0.273 0.0000.0320.000 0.000 0.0000.000 0.000 836.00.050.074 0.000 0.13 0.12 181.0
Pre Test Baseline Direct
3/28/2025 06:30 0.0000.0000.002 0.000 0.0310.000 0.000 0.000 0.1160.0130.677 0.160 0.0580.114 0.010 832.00.180.000 0.003 0.00 0.00 180.0
3/28/2025 06:31 0.0000.0000.000 0.000 0.0120.000 0.000 0.008 0.1000.0020.476 0.000 0.0410.030 0.007 832.00.050.000 0.003 0.00 0.00 180.0
3/28/2025 06:32 0.0000.0000.000 0.000 0.0470.000 0.000 0.098 0.0990.0000.314 0.038 0.0520.059 0.008 831.00.090.000 0.000 0.00 0.00 180.0
CTS Direct
3/28/2025 06:38 0.0000.0000.014 0.009 0.0000.000 0.000 0.000 0.1000.0000.000 100.286 0.0490.000 0.022 831.066.950.000 0.000 0.00 0.06 181.0
3/28/2025 06:38 0.0460.0000.010 0.000 0.0000.000 0.000 0.152 0.1900.0000.000 99.897 0.0000.000 0.012 831.066.630.000 0.000 0.05 0.06 181.0
3/28/2025 06:39 0.1030.3330.013 0.004 0.0000.000 0.000 0.024 0.0790.0000.000 99.519 0.0310.046 0.016 831.066.410.000 0.000 0.44 0.06 181.0
High O2 Direct
3/28/2025 06:44 0.0000.2310.004 0.000 0.0150.000 0.000 0.000 0.2450.0000.409 0.002 0.0030.000 0.000 831.00.000.000 0.001 0.23 21.05 180.0
3/28/2025 06:45 0.0000.1280.004 0.000 0.0000.000 0.000 0.000 0.2100.0120.575 0.121 0.0000.039 0.000 832.00.080.000 0.001 0.13 21.05 180.0
3/28/2025 06:45 0.0000.3610.005 0.000 0.0870.000 0.000 0.000 0.1170.0080.559 0.000 0.0550.090 0.003 832.00.060.000 0.000 0.36 21.05 180.0
NO2/Mid O2 Direct
3/28/2025 06:53 105.9350.0520.001 0.000 0.1090.000 0.999 0.000 0.7770.0030.280 0.000 0.0000.181 0.000 832.00.000.000 0.000 105.99 10.81 180.0
3/28/2025 06:54 105.7390.173-0.001 0.000 0.1980.000 0.993 0.000 0.7710.0000.000 0.000 0.0000.195 0.000 832.00.000.000 0.000 105.91 10.82 180.0
3/28/2025 06:55 106.7840.092-0.000 0.000 0.0970.000 0.985 0.000 0.9580.0000.088 0.000 0.0000.050 0.000 832.00.000.000 0.001 106.88 10.81 180.0
Spike Direct
3/28/2025 07:01 0.000248.0690.004 4.829 1.548493.591 2.258 1.202 10.0590.3110.000 1.165 254.2260.000 0.000 832.0256.692.534 10.041 248.07 0.02 180.0
3/28/2025 07:01 0.000247.7150.005 4.809 1.492493.358 2.253 1.259 10.0470.1360.000 1.156 254.3520.000 0.000 832.0256.872.626 10.049 247.72 0.02 180.0
3/28/2025 07:02 0.000248.2550.006 4.833 1.307493.406 2.247 1.318 9.9890.2330.000 1.143 254.5340.000 0.000 832.0257.042.616 10.051 248.25 0.02 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
3/28/2025 07:05 0.0000.6160.027 0.000 0.0000.601 0.000 0.653 0.0000.0000.149 0.000 0.0630.030 0.173 832.00.410.000 0.000 0.62 0.11 180.0
3/28/2025 07:05 0.0000.3030.025 0.000 0.0000.590 0.000 0.589 0.0000.0000.282 0.000 0.0240.000 0.147 832.00.320.000 0.000 0.30 0.11 180.0
3/28/2025 07:05 0.0000.1980.024 0.000 0.0000.512 0.000 0.598 0.0000.0000.368 0.000 0.0000.000 0.123 832.00.250.000 0.000 0.20 0.10 179.0
CTS System with Response Time
3/28/2025 07:07 0.0000.0000.033 0.000 0.0000.508 0.014 0.577 0.0530.0000.000 98.918 0.0000.000 0.126 832.066.200.000 0.000 0.00 0.06 180.0
3/28/2025 07:08 0.0000.0000.031 0.000 0.0000.524 0.009 0.480 0.0010.0000.000 99.040 0.0000.000 0.130 832.066.290.000 0.000 0.00 0.06 180.0
3/28/2025 07:08 0.0000.0000.031 0.000 0.0000.573 0.016 0.445 0.0010.0000.000 99.063 0.0000.000 0.105 832.066.260.000 0.000 0.00 0.06 180.0
NO2/Mid O2 System with Response Time
3/28/2025 07:17 100.2942.1300.013 0.000 0.1140.516 1.006 0.137 0.7390.0000.955 0.000 0.0000.221 0.120 832.00.270.050 0.000 102.42 10.25 180.0
3/28/2025 07:17 100.3202.1360.013 0.000 0.0000.516 0.997 0.208 0.7990.0000.979 0.000 0.0000.177 0.122 832.00.300.086 0.000 102.46 10.26 180.0
3/28/2025 07:18 100.4672.1570.014 0.000 0.2070.596 1.003 0.157 0.7490.0000.329 0.000 0.0000.192 0.057 832.00.180.103 0.000 102.62 10.27 180.0
Spike System with Response Time
3/28/2025 07:19 0.000246.7970.021 4.807 0.418491.342 2.230 1.560 6.8130.1440.929 1.258 252.9710.000 0.000 832.0255.602.679 9.994 246.80 0.02 180.0
3/28/2025 07:20 0.000246.9060.019 4.830 0.475491.776 2.211 1.318 6.7110.1151.195 1.199 253.3330.000 0.000 832.0255.972.751 10.024 246.91 0.02 180.0
3/28/2025 07:20 0.000247.3490.019 4.808 0.461493.065 2.223 1.344 6.5730.1381.072 1.173 253.6040.000 0.000 832.0256.242.779 10.020 247.35 0.02 180.0
Baseline System with Response Time
3/28/2025 07:22 0.0001.0290.016 0.000 0.0001.227 0.080 0.072 0.0760.0001.961 0.000 0.4120.006 0.056 832.00.520.000 0.003 1.03 0.00 180.0
3/28/2025 07:23 0.0000.3870.016 0.000 0.0000.984 0.053 0.022 0.0350.0032.492 0.000 0.2210.091 0.075 832.00.380.018 0.008 0.39 0.00 180.0
3/28/2025 07:23 0.0000.5610.015 0.000 0.1310.968 0.056 0.205 0.3900.0002.652 0.000 0.3690.000 0.000 832.00.370.000 0.000 0.56 0.00 180.0
Run 1 - A 30minute/60min
3/28/2025 07:42 0.00010.94517.846 9.521 86.68515.815 3.001 7.914 1.2670.0000.000 0.000 0.0000.851 0.360 832.01.100.574 0.000 10.94 0.40 180.0
3/28/2025 07:43 0.00010.33717.831 9.492 122.15326.546 2.307 18.784 4.4190.0000.000 0.168 0.2840.969 0.432 832.01.690.642 0.000 10.34 0.36 180.0
3/28/2025 07:44 0.00010.80017.812 9.515 121.39935.129 3.201 26.114 4.5210.0000.000 0.164 0.3810.901 0.452 832.01.820.641 0.007 10.80 0.46 180.0
3/28/2025 07:45 0.00011.14817.766 9.492 113.26130.806 4.344 26.004 3.7520.0000.000 0.000 0.1860.652 0.425 832.01.410.562 0.002 11.15 0.38 180.0
3/28/2025 07:46 0.00011.08917.796 9.584 100.18821.815 2.735 17.372 2.7140.0000.000 0.129 0.0000.677 0.405 832.01.220.490 0.000 11.09 0.40 180.0
3/28/2025 07:47 0.00011.71917.835 9.600 87.72423.989 2.730 16.403 1.9780.0000.000 0.329 0.0000.712 0.368 832.01.250.437 0.001 11.72 0.38 180.0
3/28/2025 07:48 0.00011.45017.850 9.629 93.44927.965 2.554 18.612 2.0630.0000.000 0.000 0.0000.731 0.359 832.01.030.464 0.000 11.45 0.41 180.0
3/28/2025 07:49 0.00011.51017.870 9.615 98.99027.652 3.111 30.234 2.3940.0000.000 0.000 0.0000.661 0.369 832.01.020.425 0.004 11.51 0.44 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 07:50 0.00011.82317.880 9.639 98.47924.272 3.775 25.215 2.4600.0000.000 0.076 0.0000.737 0.355 832.01.100.509 0.002 11.82 0.35 180.0
3/28/2025 07:51 0.00011.57317.909 9.655 110.36828.929 2.719 26.017 3.7890.0000.000 0.167 0.0740.604 0.424 832.01.360.486 0.003 11.57 0.45 180.0
3/28/2025 07:52 0.00011.58217.929 9.678 116.04522.533 3.649 13.993 4.2150.0000.000 0.139 0.1150.630 0.429 832.01.530.701 0.004 11.58 0.43 180.0
3/28/2025 07:53 0.00011.55417.922 9.679 107.98816.499 3.600 11.407 3.3770.0000.000 0.022 0.0000.648 0.371 832.01.130.553 0.001 11.55 0.41 180.0
3/28/2025 07:54 0.00011.41917.893 9.675 112.31614.789 3.399 10.058 3.8920.0000.000 0.151 0.0580.624 0.403 832.01.330.548 0.000 11.42 0.37 180.0
3/28/2025 07:55 0.00011.17517.883 9.658 111.66213.265 3.328 8.474 3.8110.0000.000 0.219 0.0330.626 0.382 832.01.310.545 0.001 11.18 0.37 180.0
3/28/2025 07:56 0.00010.96317.891 9.654 112.42913.344 3.045 10.825 3.7170.0000.000 0.350 0.0240.644 0.381 832.01.380.538 0.001 10.96 0.38 180.0
3/28/2025 07:57 0.00011.07617.861 9.627 115.05915.505 3.199 12.240 4.2130.0000.000 0.393 0.1020.630 0.416 832.01.710.766 0.002 11.08 0.34 180.0
3/28/2025 07:58 0.00011.09817.870 9.630 105.35015.146 3.437 15.857 3.0740.0000.000 0.303 0.0000.632 0.343 832.01.360.713 0.001 11.10 0.35 180.0
3/28/2025 07:59 0.00010.89317.855 9.623 103.38613.369 3.119 12.263 2.9250.0000.000 0.241 0.0000.601 0.333 832.01.240.618 0.003 10.89 0.36 180.0
3/28/2025 08:00 0.00010.67917.876 9.611 110.39617.984 2.722 21.575 3.6190.0000.000 0.013 0.0670.553 0.388 832.01.220.549 0.004 10.68 0.39 180.0
3/28/2025 08:01 0.00011.16617.884 9.625 100.26017.822 2.821 14.372 2.7910.0000.000 0.075 0.0000.677 0.339 832.01.090.549 0.004 11.17 0.40 180.0
3/28/2025 08:02 0.00010.92217.871 9.599 106.79126.574 3.064 26.153 3.4600.0000.000 0.000 0.0000.605 0.371 832.01.160.629 0.007 10.92 0.40 180.0
3/28/2025 08:03 0.00011.51617.846 9.620 97.57724.818 2.708 15.990 3.1020.0000.000 0.084 0.0330.580 0.385 832.01.260.601 0.003 11.52 0.39 180.0
3/28/2025 08:04 0.00011.31217.840 9.606 101.39525.412 2.930 22.107 2.7360.0000.000 0.194 0.0000.520 0.336 832.01.230.640 0.004 11.31 0.44 180.0
3/28/2025 08:05 0.00011.19517.859 9.637 110.23126.698 3.368 19.017 3.6870.0000.000 0.217 0.0000.566 0.390 832.01.360.650 0.000 11.20 0.42 180.0
3/28/2025 08:06 0.00011.85717.875 9.642 88.62423.797 2.925 17.292 2.4880.0000.000 0.198 0.0000.562 0.348 832.01.250.636 0.004 11.86 0.40 180.0
3/28/2025 08:07 0.00012.00717.846 9.637 94.05023.877 2.741 24.642 2.0490.0000.000 0.102 0.0000.590 0.332 832.01.140.607 0.004 12.01 0.45 180.0
3/28/2025 08:08 0.00011.51017.853 9.638 103.11323.661 3.146 26.567 2.9030.0000.000 0.126 0.0000.648 0.358 832.01.200.593 0.004 11.51 0.44 180.0
3/28/2025 08:09 0.00011.13017.881 9.651 115.35822.845 3.767 16.021 4.2290.0000.000 0.417 0.0710.593 0.411 832.01.540.556 0.001 11.13 0.36 180.0
3/28/2025 08:10 0.00011.06217.856 9.632 110.80015.531 3.405 10.401 3.3480.0000.000 0.190 0.0000.588 0.340 832.01.300.736 0.003 11.06 0.36 180.0
3/28/2025 08:11 0.00011.03217.855 9.635 110.53815.254 3.561 14.174 3.5480.0000.000 0.161 0.0000.580 0.357 832.01.190.556 0.003 11.03 0.36 180.0
0.00011.25117.861 9.617 105.53521.721 3.147 17.870 3.2180.0000.000 0.154 0.0480.653 0.379 832.001.2980.584 0.002 11.252 0.395 180.0Avg.
Spike 1
3/28/2025 08:15 3.56730.92516.230 9.199 101.67863.595 3.464 15.346 3.9820.0000.000 2.326 22.0290.618 0.364 832.024.590.419 0.923 34.49 0.40 180.0
Run 1 - B 30minute/60min
3/28/2025 08:19 0.00010.76117.841 9.611 116.18924.577 2.744 19.265 4.1550.0000.000 0.403 0.2660.502 0.396 832.01.830.750 0.007 10.76 0.43 180.0
3/28/2025 08:20 0.00010.84217.849 9.580 111.65726.277 4.214 23.474 3.9680.0000.000 0.198 0.1450.588 0.424 832.01.550.637 0.008 10.84 0.38 180.0
3/28/2025 08:21 0.00010.99817.832 9.610 106.32321.817 3.563 20.167 3.4370.0000.000 0.273 0.0000.487 0.365 832.01.320.606 0.008 11.00 0.37 179.0
3/28/2025 08:22 0.00011.45117.857 9.585 108.76820.974 4.450 22.777 3.5920.0000.000 0.284 0.0000.593 0.371 832.01.380.681 0.005 11.45 0.36 180.0
3/28/2025 08:23 0.00011.01517.868 9.633 115.71124.254 3.408 26.768 4.1780.0000.000 0.317 0.0770.523 0.420 832.01.550.630 0.010 11.01 0.39 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 08:24 0.00011.52617.864 9.610 113.79324.079 4.035 23.620 4.1150.0000.000 0.260 0.0690.480 0.408 832.01.460.608 0.005 11.53 0.38 180.0
3/28/2025 08:25 0.00011.25117.852 9.647 121.36625.821 3.662 19.117 5.0090.0000.000 0.283 0.2780.792 0.412 832.01.830.802 0.009 11.25 0.42 180.0
3/28/2025 08:26 0.00011.55317.824 9.605 119.77527.653 4.351 19.415 4.8370.0000.000 0.340 0.2510.516 0.411 832.01.760.686 0.005 11.55 0.38 180.0
3/28/2025 08:27 0.00011.68817.835 9.610 109.91824.983 4.570 27.890 3.7690.0000.000 0.173 0.0200.526 0.402 832.01.340.601 0.007 11.69 0.39 180.0
3/28/2025 08:28 0.00011.50517.856 9.649 114.12523.477 3.803 19.352 4.3950.0000.000 0.458 0.0340.584 0.405 832.01.580.652 0.002 11.50 0.38 180.0
3/28/2025 08:29 0.00011.38617.867 9.634 117.76025.183 3.820 22.851 4.5440.0000.000 0.289 0.1170.554 0.422 832.01.650.744 0.006 11.39 0.37 180.0
3/28/2025 08:30 0.00011.71317.859 9.614 110.51220.925 4.072 20.009 3.6610.0000.000 0.342 0.0000.600 0.352 832.01.400.703 0.003 11.71 0.36 180.0
3/28/2025 08:31 0.00011.37117.863 9.585 112.48928.575 4.015 36.963 4.0890.0000.000 0.113 0.0660.485 0.405 832.01.460.767 0.009 11.37 0.42 180.0
3/28/2025 08:32 0.00011.56917.872 9.597 116.55629.024 4.335 27.885 4.3350.0000.000 0.302 0.0810.533 0.428 832.01.510.563 0.006 11.57 0.43 180.0
3/28/2025 08:33 0.00011.30017.846 9.568 111.28629.161 5.008 34.578 3.8630.0000.000 0.071 0.0270.552 0.381 832.01.310.713 0.011 11.30 0.42 180.0
3/28/2025 08:34 0.00011.37017.852 9.567 105.25725.290 4.399 30.254 3.1980.0000.000 0.162 0.0000.543 0.333 832.01.200.645 0.009 11.37 0.39 180.0
3/28/2025 08:35 0.00010.93117.852 9.594 118.41629.003 3.899 26.977 4.5340.0000.000 0.454 0.1560.526 0.437 832.01.820.726 0.005 10.93 0.44 180.0
3/28/2025 08:36 0.00010.94417.841 9.565 111.16024.868 4.658 28.613 3.6620.0000.000 0.063 0.0000.508 0.381 832.01.220.621 0.010 10.94 0.38 180.0
3/28/2025 08:37 0.00011.02417.848 9.592 117.51823.371 4.230 20.248 4.5930.0000.000 0.348 0.2770.437 0.386 832.01.760.715 0.008 11.02 0.37 180.0
3/28/2025 08:38 0.00011.35517.838 9.601 112.14518.147 4.382 18.136 3.5980.0000.000 0.352 0.0000.553 0.349 832.01.420.731 0.006 11.35 0.35 180.0
3/28/2025 08:39 0.00011.18917.858 9.642 105.95816.861 3.257 16.113 3.5280.0000.000 0.271 0.0000.558 0.346 832.01.310.657 0.003 11.19 0.37 180.0
3/28/2025 08:40 0.00011.57217.851 9.656 105.73815.803 3.445 14.898 3.1460.0000.000 0.211 0.0000.587 0.329 832.01.260.689 0.004 11.57 0.34 180.0
3/28/2025 08:41 0.00011.70417.849 9.647 108.80321.104 3.829 27.466 3.5290.0000.000 0.155 0.0000.581 0.366 832.01.240.603 0.008 11.70 0.38 180.0
3/28/2025 08:42 0.00011.97217.799 9.607 105.03822.259 4.091 25.592 3.0590.0000.000 0.309 0.0000.517 0.364 832.01.330.590 0.003 11.97 0.39 180.0
3/28/2025 08:43 0.16211.64117.804 9.653 115.30624.602 3.424 20.981 4.5120.0000.000 0.266 0.1070.516 0.395 832.01.480.615 0.005 11.80 0.36 180.0
3/28/2025 08:44 0.00011.76017.801 9.614 109.41621.420 4.737 22.241 3.6580.0000.000 0.302 0.0000.565 0.376 832.01.400.669 0.009 11.76 0.36 180.0
3/28/2025 08:45 0.00011.77117.795 9.615 105.63918.213 4.439 23.057 3.0180.0000.000 0.153 0.0000.584 0.343 832.01.220.651 0.008 11.77 0.35 180.0
3/28/2025 08:46 0.00011.80317.811 9.659 117.20119.663 3.579 14.746 4.5750.0000.000 0.453 0.0970.486 0.422 832.01.670.643 0.007 11.80 0.35 180.0
3/28/2025 08:47 0.00011.66117.807 9.648 115.73820.248 3.892 16.702 4.2370.0000.000 0.400 0.0760.530 0.418 832.01.640.688 0.003 11.66 0.34 180.0
3/28/2025 08:48 0.00011.49117.818 9.617 110.45018.307 4.382 16.648 3.6100.0000.000 0.275 0.0000.495 0.378 832.01.320.572 0.005 11.49 0.34 180.0
0.00511.40417.840 9.614 112.33423.198 4.023 22.893 3.9470.0000.000 0.276 0.0710.543 0.388 832.001.4740.665 0.006 11.408 0.380 180.0Avg.
0.00311.32817.851 9.615 108.93522.460 3.585 20.382 3.5820.0000.000 0.215 0.0600.598 0.383 832.001.3860.625 0.004 11.330 0.387 180.0Run 1 Avg:
Baseline 1
3/28/2025 08:51 0.0000.1120.039 0.000 0.0001.265 0.149 0.565 0.0000.0001.074 0.000 0.0000.000 0.074 832.00.150.000 0.000 0.11 0.00 180.0
Run 2 - A 30minute/60min
3/28/2025 08:53 0.00017.10013.753 7.745 95.56720.854 3.066 22.514 3.4270.0030.000 0.344 0.2920.720 0.453 832.01.850.635 0.007 17.10 0.27 180.0
3/28/2025 08:54 0.00010.70817.719 9.535 109.72429.662 4.172 24.171 3.9450.0000.000 0.502 0.2210.470 0.398 832.01.830.713 0.004 10.71 0.36 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 08:55 0.00011.66117.769 9.588 111.33324.930 3.976 16.771 3.9860.0000.000 0.419 0.1260.514 0.428 832.01.810.820 0.006 11.66 0.33 180.0
3/28/2025 08:57 0.00011.63617.789 9.621 104.80920.021 3.835 22.815 3.1290.0000.000 0.305 0.0000.598 0.351 832.01.340.653 0.005 11.64 0.34 180.0
3/28/2025 08:58 0.00011.89317.798 9.603 104.47920.011 4.087 24.848 2.9670.0000.000 0.391 0.0000.483 0.328 832.01.360.661 0.004 11.89 0.34 180.0
3/28/2025 08:59 0.00011.72217.862 9.662 108.45224.080 3.812 23.018 3.7180.0000.000 0.206 0.0000.504 0.372 832.01.290.615 0.008 11.72 0.36 180.0
3/28/2025 09:00 0.00011.56417.855 9.620 107.97422.745 4.351 24.350 3.4030.0000.000 0.149 0.0000.547 0.362 832.01.240.631 0.003 11.56 0.35 180.0
3/28/2025 09:01 0.00011.76817.815 9.608 109.32019.615 4.585 21.612 3.4950.0000.000 0.395 0.0000.540 0.360 832.01.420.653 0.006 11.77 0.32 180.0
3/28/2025 09:02 0.00011.75917.792 9.630 112.26921.858 3.761 20.457 4.2010.0000.000 0.408 0.0720.502 0.411 832.01.560.590 0.006 11.76 0.32 180.0
3/28/2025 09:03 0.00011.79817.785 9.599 107.29118.901 4.525 19.990 3.3030.0000.000 0.081 0.0000.524 0.349 832.01.270.772 0.007 11.80 0.34 180.0
3/28/2025 09:04 0.00011.65617.803 9.627 112.64118.557 3.828 16.679 3.9420.0000.000 0.447 0.0140.579 0.384 832.01.510.641 0.004 11.66 0.32 180.0
3/28/2025 09:05 0.00011.73817.818 9.641 104.25515.413 3.749 13.694 2.9090.0000.000 0.084 0.0000.620 0.333 832.01.140.623 0.007 11.74 0.34 180.0
3/28/2025 09:06 0.00011.20617.832 9.632 109.57516.918 3.583 17.900 3.6300.0000.000 0.356 0.0250.453 0.332 832.01.410.722 0.004 11.21 0.31 180.0
3/28/2025 09:07 0.00011.27217.833 9.623 113.15920.569 3.741 21.267 4.0960.0000.000 0.272 0.0190.503 0.392 832.01.460.718 0.005 11.27 0.33 180.0
3/28/2025 09:08 0.00010.98217.832 9.611 117.47820.266 3.487 17.023 4.6810.0000.000 0.444 0.3000.433 0.391 832.01.830.683 0.006 10.98 0.36 180.0
3/28/2025 09:09 0.00011.35417.806 9.565 111.04022.216 4.576 20.881 3.8720.0000.000 0.363 0.0890.540 0.381 832.01.490.590 0.009 11.35 0.33 180.0
3/28/2025 09:10 0.00010.80817.817 9.584 106.86122.042 3.774 27.073 3.4470.0000.000 0.328 0.1290.465 0.325 832.01.460.697 0.007 10.81 0.35 180.0
3/28/2025 09:11 0.00010.76417.827 9.586 116.31826.189 3.658 27.797 4.2200.0000.000 0.273 0.0840.533 0.395 832.01.460.611 0.006 10.76 0.38 180.0
3/28/2025 09:12 0.00010.97417.847 9.600 117.18625.153 4.116 19.343 4.3470.0000.000 0.300 0.1650.545 0.422 832.01.650.665 0.007 10.97 0.38 180.0
3/28/2025 09:13 0.00011.52617.828 9.626 107.69021.910 3.737 20.015 3.4780.0000.000 0.297 0.0070.513 0.365 832.01.350.618 0.008 11.53 0.34 180.0
3/28/2025 09:14 0.00011.54017.812 9.583 112.57426.267 4.437 27.000 4.0550.0000.000 0.258 0.0460.552 0.398 832.01.470.676 0.006 11.54 0.37 180.0
3/28/2025 09:15 0.00011.53717.815 9.591 112.97027.260 4.286 28.140 4.0850.0000.000 0.415 0.0060.505 0.398 832.01.450.555 0.005 11.54 0.39 180.0
3/28/2025 09:16 0.00011.86117.823 9.605 107.99424.491 4.860 25.231 3.5050.0000.000 0.051 0.0000.613 0.374 832.01.210.640 0.009 11.86 0.38 180.0
3/28/2025 09:17 0.00011.64617.823 9.595 112.78427.223 3.970 26.790 4.1580.0000.000 0.351 0.0710.537 0.408 832.01.520.596 0.006 11.65 0.40 180.0
3/28/2025 09:18 0.00012.00617.827 9.598 110.40626.002 4.787 23.656 3.8820.0000.000 0.407 0.0510.510 0.397 832.01.480.546 0.005 12.01 0.38 180.0
3/28/2025 09:19 0.00011.54517.830 9.592 111.42225.970 4.362 30.159 3.8210.0000.000 0.061 0.0160.505 0.400 832.01.240.581 0.009 11.55 0.36 180.0
3/28/2025 09:20 0.00011.73317.850 9.613 113.61523.477 4.484 17.142 4.4210.0000.000 0.517 0.0690.497 0.422 832.01.680.627 0.003 11.73 0.34 180.0
3/28/2025 09:21 0.00011.39617.829 9.600 111.90518.042 4.240 19.231 3.6060.0000.000 0.281 0.0000.524 0.357 832.01.290.586 0.006 11.40 0.34 180.0
3/28/2025 09:22 0.00012.00217.825 9.607 109.76917.204 4.038 16.559 3.5280.0000.000 0.171 0.0000.529 0.349 832.01.210.604 0.008 12.00 0.31 180.0
3/28/2025 09:23 0.03711.45917.864 9.614 106.56619.020 3.442 21.184 3.1400.0000.000 0.125 0.0000.560 0.358 832.01.220.624 0.006 11.50 0.34 180.0
0.00111.68717.683 9.543 109.91422.229 4.044 21.910 3.7470.0000.000 0.300 0.0600.531 0.380 832.001.4500.645 0.006 11.689 0.346 180.0Avg.
Spike 2
3/28/2025 09:29 1.36832.70716.205 9.117 99.61279.056 4.664 33.237 3.6170.0000.000 2.395 21.8900.570 0.375 832.024.660.634 0.911 34.08 0.45 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
3/28/2025 09:33 0.00011.80717.861 9.602 113.62721.667 4.226 15.416 4.0590.0000.000 0.280 0.2260.526 0.380 832.01.620.670 0.012 11.81 0.35 180.0
3/28/2025 09:35 0.00011.44117.859 9.626 115.28724.006 3.787 18.598 4.3450.0000.000 0.223 0.1500.518 0.431 832.01.590.640 0.012 11.44 0.35 180.0
3/28/2025 09:36 0.00011.39317.869 9.631 118.35725.102 3.867 20.431 4.6760.0000.000 0.465 0.1930.514 0.450 832.01.830.641 0.007 11.39 0.35 180.0
3/28/2025 09:37 0.00011.87917.857 9.588 104.54622.380 4.524 20.759 3.3450.0000.000 0.330 0.0000.556 0.387 832.01.350.532 0.006 11.88 0.34 180.0
3/28/2025 09:38 0.00012.08717.865 9.611 110.34540.682 3.294 32.994 4.2730.0000.000 0.241 0.1740.551 0.444 832.01.670.674 0.010 12.09 0.43 180.0
3/28/2025 09:39 0.75512.61517.876 9.636 68.01726.589 1.540 17.953 1.9590.0000.000 0.013 0.0000.881 0.244 832.00.760.395 0.002 13.37 0.50 180.0
3/28/2025 09:40 0.03111.47817.848 9.625 105.32134.822 3.100 24.959 3.0950.0000.000 0.112 0.0000.513 0.354 832.01.120.498 0.009 11.51 0.46 180.0
3/28/2025 09:41 0.00011.00017.879 9.619 116.53432.412 3.491 26.245 4.3360.0000.000 0.296 0.1070.572 0.440 832.01.610.637 0.010 11.00 0.40 180.0
3/28/2025 09:42 0.00011.21717.877 9.593 108.12724.647 4.306 22.214 3.4840.0000.000 0.390 0.0000.546 0.346 832.01.320.552 0.009 11.22 0.36 180.0
3/28/2025 09:43 0.00011.30217.897 9.611 109.76726.381 3.796 25.404 3.7360.0000.000 0.485 0.0530.540 0.401 832.01.570.595 0.008 11.30 0.39 180.0
3/28/2025 09:44 0.00010.98917.901 9.603 115.60622.522 3.689 17.112 4.1750.0000.000 0.350 0.0810.540 0.418 832.01.560.610 0.008 10.99 0.38 180.0
3/28/2025 09:45 0.00010.77017.881 9.599 118.75119.669 3.539 14.252 4.5660.0000.000 0.456 0.1050.516 0.424 832.01.740.731 0.005 10.77 0.37 180.0
3/28/2025 09:46 0.00010.72617.868 9.591 113.41718.525 3.518 14.932 4.0640.0000.000 0.246 0.0180.517 0.399 833.01.390.615 0.008 10.73 0.33 180.0
3/28/2025 09:47 0.00010.98117.870 9.595 109.44418.230 3.677 16.389 3.7280.0000.000 0.350 0.0270.585 0.373 833.01.380.557 0.006 10.98 0.33 180.0
3/28/2025 09:48 0.00010.82917.867 9.602 116.70321.261 3.344 18.281 4.2880.0000.000 0.333 0.1090.526 0.420 833.01.600.646 0.007 10.83 0.34 180.0
3/28/2025 09:49 0.00010.89717.892 9.582 110.66420.814 4.136 23.027 3.6110.0000.000 0.376 0.0000.599 0.354 833.01.300.518 0.006 10.90 0.34 180.0
3/28/2025 09:50 0.00011.15317.897 9.586 110.38125.106 4.302 27.669 3.7160.0000.000 0.100 0.0190.499 0.376 833.01.160.489 0.006 11.15 0.33 180.0
3/28/2025 09:51 0.00011.04417.879 9.617 112.49730.338 3.627 26.480 4.0960.0000.000 0.261 0.0640.495 0.399 833.01.410.555 0.011 11.04 0.39 180.0
3/28/2025 09:52 0.00011.61917.847 9.604 105.78726.247 3.841 25.650 3.3970.0000.000 0.266 0.0000.534 0.359 833.01.260.548 0.008 11.62 0.39 180.0
3/28/2025 09:53 0.00011.22517.872 9.624 120.38032.892 3.327 17.768 4.9520.0000.000 0.354 0.3380.743 0.420 833.01.830.630 0.007 11.23 0.40 180.0
3/28/2025 09:54 0.00011.18317.852 9.617 115.05528.297 3.821 21.312 4.4110.0000.000 0.470 0.1440.513 0.433 833.01.740.625 0.006 11.18 0.39 180.0
3/28/2025 09:55 0.00011.36517.843 9.597 116.82456.959 3.772 39.854 4.6700.0000.000 0.139 0.3350.741 0.418 833.01.700.652 0.009 11.37 0.52 180.0
3/28/2025 09:56 0.87311.85917.841 9.639 62.92125.026 2.420 13.155 1.7770.0000.000 0.000 0.0000.774 0.243 833.00.740.377 0.000 12.73 0.41 180.0
3/28/2025 09:57 0.00011.13917.834 9.612 105.96438.668 2.448 20.739 2.9020.0000.000 0.186 0.0000.527 0.361 833.01.210.546 0.005 11.14 0.48 180.0
3/28/2025 09:58 0.00010.95717.815 9.601 119.32839.693 3.277 21.371 4.8730.0000.000 0.319 0.2190.525 0.473 833.01.810.642 0.009 10.96 0.47 180.0
3/28/2025 09:59 0.00010.96717.843 9.580 113.52026.552 3.975 19.497 4.1330.0000.000 0.420 0.0360.534 0.403 833.01.470.515 0.002 10.97 0.39 180.0
3/28/2025 10:00 0.00010.98217.841 9.571 110.95325.530 4.092 22.797 3.9180.0000.000 0.215 0.0630.588 0.388 833.01.380.603 0.005 10.98 0.35 180.0
3/28/2025 10:01 0.00010.66017.852 9.548 109.02528.132 3.994 28.472 3.4990.0000.000 0.162 0.0000.584 0.372 833.01.190.504 0.011 10.66 0.41 180.0
3/28/2025 10:02 0.00010.79017.826 9.543 105.78655.375 3.929 50.797 3.5520.0000.000 0.026 0.0000.502 0.398 833.01.160.526 0.012 10.79 0.47 180.0
3/28/2025 10:03 0.76412.34317.846 9.613 57.34521.566 1.906 11.910 1.4930.0000.000 0.144 0.0000.857 0.225 833.00.870.485 0.003 13.11 0.40 180.0
0.08111.29017.862 9.602 107.34328.670 3.552 22.548 3.7710.0000.000 0.267 0.0820.581 0.384 832.601.4110.574 0.007 11.371 0.394 180.0Avg.
0.04111.48917.772 9.573 108.62825.449 3.798 22.229 3.7590.0000.000 0.283 0.0710.556 0.382 832.301.4310.609 0.007 11.530 0.370 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
3/28/2025 10:07 0.0000.0840.041 0.000 0.0000.858 0.135 0.392 0.0930.0001.560 0.000 0.0000.000 0.090 833.00.180.000 0.000 0.08 0.00 180.0
Run 3 - A 30minute/60min
3/28/2025 10:10 0.00011.03517.615 9.499 107.00526.329 3.663 19.937 3.5950.0000.000 0.278 0.0000.543 0.436 833.01.410.534 0.004 11.03 0.29 180.0
3/28/2025 10:11 0.00011.53917.797 9.592 106.78822.603 3.361 17.789 3.3110.0000.000 0.160 0.0000.566 0.380 833.01.230.539 0.005 11.54 0.34 180.0
3/28/2025 10:13 0.00011.31317.820 9.610 110.24620.998 3.128 15.649 3.8810.0000.000 0.152 0.0000.543 0.397 833.01.320.630 0.001 11.31 0.33 180.0
3/28/2025 10:14 0.00011.52017.839 9.620 114.51724.329 3.295 14.947 4.3320.0000.000 0.411 0.1320.531 0.460 833.01.800.708 0.007 11.52 0.34 180.0
3/28/2025 10:15 0.00011.40117.871 9.636 112.49222.739 3.244 12.714 4.1910.0000.000 0.358 0.1090.537 0.441 833.01.690.693 0.005 11.40 0.34 180.0
3/28/2025 10:16 0.63411.99317.854 9.603 68.30124.778 2.866 27.692 2.2420.0000.000 0.000 0.0000.856 0.262 833.00.760.350 0.001 12.63 0.34 180.0
3/28/2025 10:17 0.00412.48517.845 9.626 86.97621.628 1.719 12.300 1.6690.0000.000 0.000 0.0000.716 0.308 833.00.990.566 0.005 12.49 0.35 180.0
3/28/2025 10:18 0.00010.88917.840 9.618 106.29928.378 2.539 20.591 3.1910.0000.000 0.296 0.0000.568 0.392 833.01.330.526 0.004 10.89 0.42 180.0
3/28/2025 10:19 0.00011.06517.845 9.597 114.92131.840 3.084 22.936 4.4330.0000.000 0.368 0.3650.450 0.439 833.01.930.656 0.005 11.06 0.45 180.0
3/28/2025 10:20 0.00011.08617.855 9.598 107.42928.310 3.692 22.913 3.6420.0000.000 0.099 0.0310.575 0.406 833.01.300.584 0.006 11.09 0.40 180.0
3/28/2025 10:21 0.00010.89617.877 9.597 107.35421.910 3.479 16.580 3.2300.0000.000 0.533 0.0000.583 0.404 833.01.500.509 0.000 10.90 0.35 180.0
3/28/2025 10:22 0.00011.16117.851 9.575 101.53719.240 3.323 20.309 2.7140.0000.000 0.174 0.0000.557 0.363 833.01.210.552 0.009 11.16 0.33 180.0
3/28/2025 10:23 0.00010.78617.873 9.589 109.37719.624 3.299 16.124 3.6280.0000.000 0.280 0.0000.488 0.409 833.01.410.605 0.005 10.79 0.34 180.0
3/28/2025 10:24 0.00010.50717.906 9.598 113.24619.816 2.841 13.945 3.9900.0000.000 0.334 0.1320.498 0.443 833.01.700.686 0.006 10.51 0.35 180.0
3/28/2025 10:25 0.00010.91917.861 9.583 106.13918.554 3.086 16.876 3.3070.0000.000 0.352 0.0000.574 0.379 833.01.390.591 0.007 10.92 0.34 180.0
3/28/2025 10:26 0.00010.90917.867 9.607 111.44921.131 2.923 14.293 3.9870.0000.000 0.299 0.0650.485 0.434 833.01.510.567 0.007 10.91 0.34 180.0
3/28/2025 10:27 0.00010.94117.854 9.607 108.96020.143 3.194 15.496 3.6770.0000.000 0.224 0.0000.583 0.401 833.01.340.581 0.004 10.94 0.32 180.0
3/28/2025 10:28 0.00010.74317.871 9.617 116.34224.413 2.763 15.421 4.6560.0000.000 0.418 0.2070.546 0.477 833.01.910.709 0.008 10.74 0.34 180.0
3/28/2025 10:29 0.00011.03417.869 9.634 115.27422.229 2.817 12.593 4.3340.0000.000 0.402 0.1480.558 0.471 833.01.760.600 0.005 11.03 0.37 180.0
3/28/2025 10:30 0.00011.08317.879 9.632 112.66525.654 3.110 19.439 4.1810.0000.000 0.483 0.0430.552 0.443 833.01.620.550 0.003 11.08 0.37 180.0
3/28/2025 10:31 0.00011.23417.847 9.599 116.90640.065 3.294 26.060 4.9410.0000.000 0.339 0.4000.432 0.488 833.02.110.771 0.012 11.23 0.46 180.0
3/28/2025 10:32 0.00011.36717.843 9.624 107.62929.796 3.445 20.285 3.5980.0000.000 0.225 0.0000.636 0.426 833.01.340.503 0.005 11.37 0.43 180.0
3/28/2025 10:33 0.00011.00617.850 9.622 108.21424.835 3.422 20.043 3.6480.0000.000 0.212 0.0000.570 0.418 833.01.340.548 0.007 11.01 0.34 180.0
3/28/2025 10:34 0.00011.21917.857 9.630 109.35818.756 2.945 10.699 3.4830.0000.000 0.140 0.0000.561 0.394 833.01.270.581 0.000 11.22 0.32 180.0
3/28/2025 10:35 0.00010.98717.861 9.617 116.54028.489 2.537 17.949 4.6720.0000.000 0.363 0.2900.778 0.438 833.01.850.664 0.006 10.99 0.40 180.0
3/28/2025 10:36 0.00011.30817.854 9.604 117.41638.654 3.092 24.820 4.6830.0000.000 0.679 0.3190.697 0.442 833.02.120.692 0.003 11.31 0.48 180.0
3/28/2025 10:37 0.00010.87717.836 9.566 109.59631.779 4.021 27.925 3.8550.0000.000 0.426 0.0110.577 0.436 833.01.550.576 0.010 10.88 0.37 180.0
3/28/2025 10:38 0.00010.70617.839 9.597 114.99628.413 3.266 18.345 4.3250.0000.000 0.489 0.2040.552 0.453 833.01.900.695 0.005 10.71 0.38 180.0
3/28/2025 10:39 0.00010.86917.863 9.587 112.78229.880 3.704 23.007 4.0360.0000.000 0.432 0.0770.511 0.442 833.01.690.668 0.008 10.87 0.36 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 10:40 0.00010.83617.829 9.561 111.68236.610 3.371 35.512 3.9400.0000.000 0.270 0.1130.580 0.441 833.01.640.697 0.008 10.84 0.45 180.0
0.02111.12417.846 9.602 108.74825.731 3.151 19.106 3.7790.0000.000 0.307 0.0880.573 0.417 833.001.5310.604 0.005 11.146 0.368 180.0Avg.
Spike 3
3/28/2025 10:44 2.91631.08116.204 9.176 106.38972.013 2.700 13.810 5.0540.0000.000 2.481 22.2560.429 0.372 832.025.060.603 0.910 34.00 0.36 180.0
Run 3 - B 30minute/60min
3/28/2025 10:47 0.16710.95017.835 9.627 113.15125.914 3.038 15.891 4.3090.0000.000 0.237 0.2040.505 0.425 832.01.680.699 0.010 11.12 0.36 180.0
3/28/2025 10:48 0.00011.46017.869 9.648 99.34622.751 3.523 23.344 2.5640.0000.000 0.237 0.0000.634 0.361 832.01.250.561 0.008 11.46 0.35 180.0
3/28/2025 10:49 0.00011.14817.862 9.646 107.76325.441 2.947 21.756 3.8220.0000.000 0.476 0.0540.604 0.417 832.01.580.556 0.007 11.15 0.39 180.0
3/28/2025 10:51 0.14711.24117.852 9.645 110.69630.044 3.046 20.136 4.2760.0000.000 0.598 0.3420.342 0.359 832.01.880.635 0.006 11.39 0.35 180.0
3/28/2025 10:52 0.02911.39117.864 9.640 111.60435.123 3.308 21.546 4.1360.0000.000 0.354 0.1610.563 0.443 832.01.730.665 0.006 11.42 0.45 180.0
3/28/2025 10:53 0.00011.07917.885 9.644 106.65528.965 3.335 21.691 3.5470.0000.000 0.312 0.1080.402 0.399 832.01.580.699 0.007 11.08 0.38 180.0
3/28/2025 10:54 0.00010.59417.884 9.620 113.79533.139 2.951 22.200 4.2050.0000.000 0.402 0.1450.532 0.460 832.01.780.664 0.009 10.59 0.43 180.0
3/28/2025 10:55 0.00010.93117.897 9.632 118.27846.066 2.879 24.103 4.9750.0000.000 0.601 0.3960.641 0.448 832.02.140.674 0.008 10.93 0.54 180.0
3/28/2025 10:56 0.00010.80117.868 9.592 104.40637.297 3.876 28.589 3.4960.0000.000 0.359 0.1740.397 0.387 833.01.650.692 0.012 10.80 0.47 180.0
3/28/2025 10:57 0.00010.67117.853 9.583 104.71728.166 3.341 24.269 3.1880.0000.000 0.591 0.0530.399 0.351 833.01.570.636 0.005 10.67 0.31 180.0
3/28/2025 10:58 0.00010.16517.796 9.551 113.05029.534 3.145 19.991 4.1900.0000.000 0.475 0.2580.420 0.425 833.01.930.762 0.005 10.16 0.37 180.0
3/28/2025 10:59 0.00010.66017.819 9.594 105.21919.361 2.831 10.625 3.5630.0000.000 0.389 0.1490.451 0.367 833.01.640.750 0.008 10.66 0.33 180.0
3/28/2025 11:00 0.00010.32317.823 9.593 110.90420.509 2.888 14.103 4.0450.0000.000 0.428 0.0780.547 0.393 833.01.590.661 0.006 10.32 0.31 180.0
3/28/2025 11:01 0.02910.50517.826 9.590 102.57117.158 3.132 15.910 2.8330.0000.000 0.286 0.0000.644 0.358 832.01.300.587 0.009 10.53 0.31 180.0
3/28/2025 11:02 0.00010.58617.816 9.594 109.20219.501 2.415 15.056 4.0710.0000.000 0.325 0.2310.409 0.386 833.01.670.675 0.008 10.59 0.31 180.0
3/28/2025 11:03 0.00910.88517.825 9.615 114.32536.413 2.474 23.618 4.4760.0000.000 0.388 0.2420.488 0.424 833.01.710.541 0.009 10.89 0.45 180.0
3/28/2025 11:04 0.00010.95617.845 9.633 106.03625.698 3.063 14.122 3.9420.0000.000 0.467 0.2230.421 0.402 832.01.770.642 0.006 10.96 0.34 180.0
3/28/2025 11:05 0.00011.02617.795 9.619 102.80219.079 2.597 13.983 2.9130.0000.000 0.175 0.0000.519 0.325 833.01.230.701 0.001 11.03 0.32 180.0
3/28/2025 11:06 0.04311.10917.789 9.627 101.77920.019 2.357 15.953 3.2030.0000.000 0.125 0.0490.458 0.354 833.01.270.650 0.007 11.15 0.32 180.0
3/28/2025 11:07 0.00010.76317.811 9.614 108.43723.922 2.673 16.649 3.9550.0000.000 0.161 0.2030.389 0.400 833.01.580.712 0.005 10.76 0.36 180.0
3/28/2025 11:08 0.00010.96917.792 9.602 112.68631.532 2.795 20.534 4.5760.0000.000 0.484 0.3460.392 0.433 833.02.020.722 0.010 10.97 0.40 180.0
3/28/2025 11:09 0.00010.69817.817 9.613 107.36628.190 2.526 16.303 3.8530.0000.000 0.319 0.1470.433 0.384 833.01.610.719 0.008 10.70 0.41 180.0
3/28/2025 11:10 0.00010.98717.821 9.604 107.44024.384 2.794 15.201 3.6140.0000.000 0.212 0.0000.478 0.400 833.01.340.602 0.010 10.99 0.35 180.0
3/28/2025 11:11 0.04110.82317.825 9.572 114.30560.716 2.551 34.401 4.5260.0000.000 0.563 0.3670.581 0.421 833.02.080.749 0.009 10.86 0.52 180.0
3/28/2025 11:12 0.00010.82117.817 9.569 115.11350.297 3.228 31.071 4.2350.0000.000 0.444 0.3710.392 0.371 833.01.860.679 0.007 10.82 0.52 180.0
3/28/2025 11:13 0.56211.33817.814 9.581 78.04226.743 3.143 14.809 3.4900.0000.000 0.094 0.0000.595 0.322 833.00.970.394 0.007 11.90 0.38 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 11:14 0.36011.63717.857 9.617 82.44926.897 0.999 13.920 1.7410.0000.000 0.313 0.0000.579 0.304 833.01.230.616 0.001 12.00 0.50 180.0
3/28/2025 11:15 0.00010.51517.859 9.591 106.42045.390 1.981 30.532 3.6990.0000.000 0.221 0.1890.356 0.375 833.01.550.697 0.008 10.52 0.49 180.0
3/28/2025 11:16 0.00010.62517.849 9.594 109.27332.636 3.051 20.323 3.8780.0000.000 0.281 0.1810.419 0.374 833.01.570.680 0.004 10.63 0.50 180.0
3/28/2025 11:17 0.01010.87417.815 9.578 101.68028.284 3.402 28.562 2.9850.0000.000 0.155 0.0000.430 0.366 833.01.210.561 0.011 10.88 0.38 180.0
0.04710.88417.836 9.608 106.65029.972 2.876 20.306 3.7440.0000.000 0.349 0.1560.481 0.388 832.671.5990.653 0.007 10.931 0.397 180.0Avg.
0.03411.00417.841 9.605 107.69927.852 3.014 19.706 3.7610.0000.000 0.328 0.1220.527 0.403 832.831.5650.629 0.006 11.038 0.382 180.0Run 3 Avg:
Baseline 3
3/28/2025 11:21 0.0000.1240.038 0.000 0.0000.977 0.140 0.459 0.0340.0000.482 0.000 0.0000.000 0.097 833.00.190.000 0.000 0.12 0.00 180.0
Post CTS
3/28/2025 11:23 0.0000.0000.041 0.000 0.0001.071 0.073 0.420 0.0000.0020.000 99.746 0.0000.147 0.143 833.066.810.036 0.000 0.00 0.06 180.0
3/28/2025 11:23 0.0000.0000.036 0.000 0.0001.033 0.073 0.281 0.0000.0000.000 100.637 0.0000.007 0.115 833.067.330.000 0.000 0.00 0.06 180.0
3/28/2025 11:23 0.0000.0000.037 0.000 0.0001.036 0.081 0.397 0.1310.0000.131 100.933 0.0000.000 0.116 833.067.630.164 0.000 0.00 0.06 180.0
Post NO2/Mid O2
3/28/2025 11:27 98.6153.5870.017 0.000 0.0000.975 1.051 0.359 0.0280.0000.000 0.133 0.0000.180 0.152 833.00.420.039 0.000 102.20 10.47 180.0
3/28/2025 11:27 99.2293.5170.020 0.000 0.2020.930 1.031 0.099 0.2870.0000.000 0.000 0.0000.000 0.143 833.00.350.091 0.004 102.75 10.51 180.0
3/28/2025 11:27 99.1673.0010.015 0.000 0.0000.974 1.048 0.251 0.5300.0000.000 0.000 0.0000.000 0.086 833.00.320.224 0.000 102.17 10.49 180.0
Post 5-Gas
3/28/2025 11:29 0.000245.9630.021 4.766 0.867492.709 2.244 1.499 6.9130.0990.000 1.299 251.8020.000 0.000 833.0254.512.764 9.967 245.96 0.02 180.0
3/28/2025 11:29 0.000247.0440.021 4.792 1.087491.998 2.231 1.691 7.2560.1140.548 1.330 252.4080.000 0.000 833.0255.102.703 9.978 247.04 0.13 180.0
3/28/2025 11:29 0.000247.0350.018 4.829 1.040495.034 2.260 1.405 6.8770.1450.374 1.275 252.8540.000 0.000 833.0255.612.854 10.007 247.04 0.02 180.0
3/28/2025 11:29 0.000247.5600.017 4.831 0.286494.526 2.196 1.830 6.7180.0821.869 1.335 253.1240.000 0.000 833.0255.932.871 9.973 247.56 0.02 180.0
End of Test Purge
3/28/2025 11:31 0.0000.2680.012 0.000 0.1441.439 0.087 0.161 0.3850.0001.055 0.840 0.5010.000 0.000 833.01.060.000 0.004 0.27 0.00 180.0
3/28/2025 11:31 0.0000.5150.016 0.000 0.1711.199 0.125 0.361 0.0130.0000.667 0.543 0.2390.000 0.108 833.00.890.114 0.005 0.52 0.00 180.0
3/28/2025 11:31 0.0000.7380.018 0.000 0.0001.315 0.118 0.165 0.0000.0001.013 0.000 0.1810.000 0.097 833.00.370.000 0.014 0.74 0.00 180.0
3/28/2025 11:32 0.0000.5560.016 0.000 0.0001.234 0.091 0.129 0.1000.0160.725 0.501 0.0620.171 0.167 832.00.760.046 0.008 0.56 0.00 180.0
3/28/2025 11:32 0.0000.0000.015 0.000 0.0001.151 0.072 0.000 0.1330.0001.424 0.430 0.2220.000 0.056 833.00.660.061 0.000 0.00 0.00 180.0
3/28/2025 11:32 0.0000.4140.015 0.000 0.1961.110 0.069 0.152 0.3890.0150.992 0.000 0.2630.016 0.020 833.00.300.000 0.013 0.41 0.00 180.0
3/28/2025 11:32 0.0000.2870.014 0.000 0.1291.167 0.070 0.006 0.6330.0000.901 0.163 0.2210.000 0.055 833.00.570.194 0.016 0.29 0.00 180.0
3/28/2025 11:32 0.0000.6030.015 0.001 0.0741.121 0.044 0.213 0.0000.0040.575 0.329 0.0000.282 0.122 832.00.480.027 0.003 0.60 0.00 180.0
GAS
Performance Test Report
Test Type: Annual
Test Date: 3/28/2025
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:12:03 PM 03:58 PM
Source:
Unit Number: 2026-03
Serial Number: 1641331
Engine Hours:11367
Permit #: #DAQE-AN161400001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
40 CFR Part 60 Subpart JJJJ
CO NOx NMNEHC
1.650 0.830 0.170
0.088 0.292 0.022
7.225 14.526 1.141
2.000 0.300 1.000 0.150 0.700 0.030
0.018 0.061 0.005
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results lb/hr
Results ppmvd
Permit lb/hr
Results g/hp-hr
Permit g/hp-hr
PASS ALL
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
JD HERBERT
3
Cody Hall
GAS
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
GAS
Unit 2026-03 with a serial number of 1641331 which is a Waukesha 9394 GSI engine located at Crusoe
Mullins Tap Facility and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 3/28/2025 by
Cody Hall with Great Plains Analytical Services, Inc. All quality assurance and quality control tests were
within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2175 BHP and 1200 RPM which is 87.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 2026-03 is authorized
to operate under permit #DAQE-AN161400001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Crusoe Mullins Tap FacilityLocation 2026-03Unit ID
Make Waukesha Site Elevation ft.53
Model 9394 GSI Atmospheric Pressure psi.14.67
Serial Number 1641331 Stack Diameter in.18
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2175 2175 2175 2175
1200 1199 1200 1200
Percent Load %
Intake Manifold Pressure (hg)
87.00%87.00%87.00%87.00%
92.29 92.29 92.29 92.29
Intake Manifold Temperature (F)123.00 123.00 123.00 123.00
Ambient Conditions
Ambient Temperature Dry (F)83.00 88.00 88.00 86.33
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
169355.74 167581.24 168362.02 168433.00
4795.58 4745.33 4767.44 4769.45
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.16 0.16 0.16
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %16.52%16.43%16.21%16.39%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
2.31%2.34%2.60%2.42%
Permitted Standards Results
5
Catalyst
Run 1 Run 2 Run 3 3 Run Average Pass Permits
12:03 PM 01:16 PM 02:28 PM 3/28/2025
State
NOx (mol wt) 46.01
1.073 0.982 0.806 0.954NMNEHC (ppmvw)
1.285 1.175 0.961 1.141NMNEHC (ppmvd)
NMNEHC (mol wt) 44.10
407.930 373.581 309.974 363.828 FailNMNEHC (ppbvd) @15% O2
0.005 0.005 0.004 0.0050.700 0.030 PassNMNEHC (g/hp-hr)
0.025 0.023 0.019 0.0220.170 PassNMNEHC (lbs/hr)
0.408 0.374 0.310 0.364 FailNMNEHC (ppmvd) @15% O2
0.0160.018CO (g/hp-hr)0.021 0.0182.000 0.300 Pass
CO (ppmvw)6.843 6.059 5.220 6.040
CO (ppmvd)8.196 7.250 6.229 7.225
CO (mol wt) 28.01
CO (ppmvd) @15% O2 2.601 2.305 2.009 2.305 Fail
CO (ppbvd) @15% O2 2601.362 2304.824 2008.579 2304.922 Fail
0.0760.088CO (lbs/hr)0.101 0.0881.650 Pass
NOx (g/hp-hr)0.062 0.064 0.056 0.0611.000 0.150 Pass
NOx (ppmvw)12.340 12.841 11.255 12.145
NOx (ppmvd)14.782 15.366 13.432 14.526
NOx (ppbvd) @15% O2 4691.386 4885.079 4330.981 4635.815 Fail
NOx (ppmvd) @15% O2 4.691 4.885 4.331 4.636 Fail
NOx (lbs/hr)0.299 0.307 0.270 0.2920.830 Pass
GAS
GAS
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
6.84
0.66
11.69 0.65 12.34
0.00%
1.86%
0.00%
16.52%
11.68 0.65 1.86%16.53%
28.34 3.38 1.74%15.00%
11.70 0.65 1.86%16.51%
0.00 0.00 0.00 0.00%0.03%
Avg. Wet
NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.51 0.00 0.00 0.00 0.00%0.03%
5.81 12.34 0.68 13.02 1.90%16.44%
58.03 31.41 5.51 36.91 1.82%14.88%
6.31 11.73 0.92 12.66 1.88%16.42%
0.17 0.17 0.00 0.17 0.00%0.03%
Avg. Wet 6.06 12.04 0.80 12.84 0.98 1.89%16.43%
NO2NO
0.13
1.01
25.30
0.96
0.21
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
5.71 10.58 0.86 11.44 2.07%16.24%
55.76 26.94 4.42 31.35 2.01%14.72%
4.73 10.25 0.83 11.07 2.14%16.18%
0.26 0.08 0.00 0.08 0.00%0.03%
0.17 0.17 0.00 0.17 0.21 0.00%0.03%
Avg. Wet 5.22 10.42 0.84 11.25 0.81 2.10%16.21%
NO2NO
0.15
0.82
24.70
0.79
NMNEHC
0.42
NO2
0.001.06
1.07
25.85
1.08
0.13
1.07
0.66
12.33
31.72
12.35
7.37
6.31
0.51
58.22
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Table 6.1. Data used for volumetric flow rate (Method 2)
Stack diameter =18 Inches or:1.5 feet or:1.77 Square feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.69
Yes
18.00
26.00
4.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
%d
%d
%d
%16.52
29.78
0.61
Inches
3.01
9
14.99
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
10.77
1.56
0.00
1021.34
0.05
30.17
30.22
993.19
1452.86
533.99
27.83
86.88
153.52
202862.55
169355.74
Run 2
16.43
29.81
0.68
10.73
2.27
0.00
1021.34
0.05
30.17
30.22
1010.19
1469.86
543.44
27.87
92.41
153.53
200527.99
167581.24
Run 3
16.21
29.79
0.66
10.56
2.52
0.00
1021.34
0.05
30.17
30.22
1007.19
1466.86
541.77
27.88
90.38
153.53
200938.11
168362.02
16.39
29.79
0.65
10.68
2.11
0.00
1021.34
0.05
30.17
30.22
1003.52
1463.19
539.73
27.86
89.91
153.53
201442.88
168433
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.69
Exhaust Temp F
993.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.57
0.52
0.48
993.00
993.00
992.00
0.55
0.59
0.67
992.00
992.00
994.00
0.60
0.53
0.50
994.00
994.00
993.00
0.58 993.00
0.66
0.69
0.77
993.00
992.00
992.00
0.70
0.66
0.61
992.00
999.00
993.19
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.56
Exhaust Temp F
1007.00
0.58
0.51
0.59
1007.00
1007.00
1008.00
0.63
0.66
0.69
1008.00
1008.00
1006.00
0.64
0.66
0.62
1006.00
1006.00
1007.00
0.69 1007.00
0.75
0.77
0.73
1007.00
1008.00
1008.00
0.71
0.69
1008.00
1007.00
1007.190.66
Run 2
Δpstd (in) H2O
0.63
Exhaust Temp F
1010.00
0.66
0.69
0.73
1010.00
1010.00
1011.00
0.77
0.71
0.70
1011.00
1011.00
1009.00
0.69
0.64
0.66
1009.00
1009.00
1010.00
0.62 1010.00
0.64
0.66
0.67
1010.00
1011.00
1011.00
0.69
0.77
1011.00
1010.00
0.68 1010.19
Pass
Strat Check
11.28Check 1
11.19Check 2
11.33Check 3
NoxGas Used
Pass/Fail
7
GAS
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(10.766)+ .32(1.558)+ .28(87.675+.001) = 29.78 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.78(1 -.16517)+ 18.0(.16517) = 27.83 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.61*√(1452.86/(30.22*27.83)) = 86.88 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.16517)86.88*1.767((528*30.22)/ (1452.86*29.92)) = 169355.74 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 169355.743/35.315 = 4795.575 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 8.196*(20.9-15)/(20.9-2.31%)) = 2.601 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(8.196*(1.164*10^-3)*4795.575*(Run Time/60))/2175 = .021 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .021*1/453.6*2175 = .101 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .101*4.38 = .442 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
8.2 = 6.8425*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
GAS
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.81%
21.05%
10.26%
10.46%
10.71%
10.71%
10.46%10.26%
10.81%
21.05%
10.71%
21.15%
10.71%
21.15%
10.71%21.15%
0.00%
10.71%
21.15%
0.10%
0.10%
0.49%
0.47%
10.71%
Span
Zero Offset 0.00%
21.15
0.00%
10.81%2.61%1.65%0.01%
2.24%
2.27%
2.52%
2.31%
2.34%
2.60%
9
GAS
0.0 0.0 0.0
0.0 0.0 0.0
1033.0 1033.0 1033.0
1069.0 1069.0 1069.0
0.7 0.7 .7
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Crusoe Mullins Tap Facility
3/28/2025
53
2026-03
Waukesha
Model
Serial Number
9394 GSI
1641331
Technician Cody Hall
Run Start Times 12:03 PM 01:16 PM 02:28 PM 03:58 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1199.0 1200.0 1199.7
Engine Hours 11364 11365 11366 11367
Intake Manifold Pressure (psi)60.0 60.0 60.0 60.0
Intake Manifold Temp °F 123.0 123.0 123.0 123.0
Engine Load (BHP)2175.0 2175.0 2175.0 2175.0
Ambient Temp °F 83.0 88.0 88.0 86.3
Humidity %41.0 41.0 41.0 41.0
Dew Point °F 25.0 25.0 25.0 25.0
Waukesha
N/A
N/A
Yes
N/A N/A N/A N/A
2 2 2 2# of Catalyst Installed
Catalyst Manufacturer
Catalyst (Yes or No)
AFR Setting (Target Left Bank)
AFR Setting (Target Right Bank)
AFR Manufacturer/Type
N/A N/A N/A
N/A N/A N/A
Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1033.0
1069.0
0.7Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
GAS
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.11
Average:Oxygen 0.00
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 99.90
Tolerance 2.00%
Difference between measured and expected 0.10%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.57
Average:Nitrogen monoxide NO 0.37
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.37
Average:VOC 0.33
Average:Oxygen 0.11
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 100.00
Value:CTS Compound Concentration Avg 99.01
Tolerance 5.00%
Difference between measured and expected 0.99%
Pre-test System CTS & Mechanical Response Time
46 secondsEquilibration Response Time
Value:Spike Reported 253.30
Value:Spike Expected 251.20
System (Equilibration) Response Time Target (Spike)
52 secondsSystem Zero Response Time
52 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC524646 12/30/2027 104.20 10.71%
CC312964 10/17/2032 100.00
CC337712 5/1/2032 21.15%
Cylinder # CC230781 Expiration: 10-18-2032
Propane CO NO SF6
Bottle Value 251.20 501.50 251.30 10.03
Analyzer System Response 253.30 492.06 247.02 10.01
Percent Difference 0.84%1.88%1.70%0.17%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.901 4.995
Spike Direct
Propane 254.371
Mechanical
Response Time
SF6 10.047
CO 493.452
NO 248.013
Ethylene 99.007 19 seconds
Analyzer
Response
Propane 253.303
SF6 10.013
CO 492.061
NO 247.017
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.425
CO 493.115
NO 247.181
46 seconds
52 seconds
9.62%
9.42%
9.31%
95.23%
96.13%
94.92%
10.015
12
GAS
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
GAS
Sampling Point Locations
in Inches
16.7%3.006
50%9.000
83.3%14.994
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
18
26
4
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
168433
H2O%d @ Sampling Point:16.39
CO2%d @ Sampling Point:10.68
Pressure @ Sampling Point (Pg "H2O):0.65
Temperature @ Sampling Point (Deg F):1003.52
GAS
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 100 99.9 4.995 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.901 4.995
Spike Direct
Propane 254.371
Mechanical
Response Time
SF6 10.047
CO 493.452
NO 248.013
Ethylene 99.007 19 seconds
Analyzer
Response
Propane 253.303
SF6 10.013
CO 492.061
NO 247.017
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.425
CO 493.115
NO 247.181
46 seconds
52 seconds
9.62%
9.42%
9.31%
95.23%
96.13%
94.92%
10.015
GAS
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
251.200
10.030
501.500
251.300
254.371
10.047
493.452
248.013
1.26%
0.17%
1.60%
1.31%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
23.012
0.967
Dilution Factor
9.625%
Expected
24.165
% Recovery
95.230%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.001
Spike Average
0.946
Dilution Factor
9.416%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.001
Spike Average
0.935
Dilution Factor
9.306%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 22.199 23.387 94.920%
0.001374
0.000761
0.000410
0.000 22.747 23.663 96.130%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass3.54%
16
GAS
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-2.49055622 Pass
Line Position Difference:Resolution Difference to Reference 3.54%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
100.00
99.24
0.77%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
GAS
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Crusoe Mullins Tap Facility; 2026-03; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
3/28/2025
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
3/28/2025
Cody Hall
GAS
Appendices
GAS
GAS
Spike (5 Gas)
GAS
9% O2/NO2
GAS
Ethylene Only
GAS
BIP
GAS
21% O2
Tri Probe Certification
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Probe size: 18S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Cody Hall
GAS
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Crusoe Mullins Tap Facility
Unit Number:2026-03
Make:Waukesha
Location:9394 GSIModel:
1641331Serial Number:
RAW Result Data
Stability
3/28/2025 06:19 0.0540.081-0.000 0.443 0.0000.028 0.000 0.273 0.0000.0320.000 0.000 0.0000.000 0.000 836.00.050.074 0.000 0.13 0.12 181.0
Pre Test Baseline Direct
3/28/2025 06:30 0.0000.0000.002 0.000 0.0310.000 0.000 0.000 0.1160.0130.677 0.160 0.0580.114 0.010 832.00.180.000 0.003 0.00 0.00 180.0
3/28/2025 06:31 0.0000.0000.000 0.000 0.0120.000 0.000 0.008 0.1000.0020.476 0.000 0.0410.030 0.007 832.00.050.000 0.003 0.00 0.00 180.0
3/28/2025 06:32 0.0000.0000.000 0.000 0.0470.000 0.000 0.098 0.0990.0000.314 0.038 0.0520.059 0.008 831.00.090.000 0.000 0.00 0.00 180.0
CTS Direct
3/28/2025 06:38 0.0000.0000.014 0.009 0.0000.000 0.000 0.000 0.1000.0000.000 100.286 0.0490.000 0.022 831.066.950.000 0.000 0.00 0.06 181.0
3/28/2025 06:38 0.0460.0000.010 0.000 0.0000.000 0.000 0.152 0.1900.0000.000 99.897 0.0000.000 0.012 831.066.630.000 0.000 0.05 0.06 181.0
3/28/2025 06:39 0.1030.3330.013 0.004 0.0000.000 0.000 0.024 0.0790.0000.000 99.519 0.0310.046 0.016 831.066.410.000 0.000 0.44 0.06 181.0
High O2 Direct
3/28/2025 06:44 0.0000.2310.004 0.000 0.0150.000 0.000 0.000 0.2450.0000.409 0.002 0.0030.000 0.000 831.00.000.000 0.001 0.23 21.05 180.0
3/28/2025 06:45 0.0000.1280.004 0.000 0.0000.000 0.000 0.000 0.2100.0120.575 0.121 0.0000.039 0.000 832.00.080.000 0.001 0.13 21.05 180.0
3/28/2025 06:45 0.0000.3610.005 0.000 0.0870.000 0.000 0.000 0.1170.0080.559 0.000 0.0550.090 0.003 832.00.060.000 0.000 0.36 21.05 180.0
NO2/Mid O2 Direct
3/28/2025 06:53 105.9350.0520.001 0.000 0.1090.000 0.999 0.000 0.7770.0030.280 0.000 0.0000.181 0.000 832.00.000.000 0.000 105.99 10.81 180.0
3/28/2025 06:54 105.7390.173-0.001 0.000 0.1980.000 0.993 0.000 0.7710.0000.000 0.000 0.0000.195 0.000 832.00.000.000 0.000 105.91 10.82 180.0
3/28/2025 06:55 106.7840.092-0.000 0.000 0.0970.000 0.985 0.000 0.9580.0000.088 0.000 0.0000.050 0.000 832.00.000.000 0.001 106.88 10.81 180.0
Spike Direct
3/28/2025 07:01 0.000248.0690.004 4.829 1.548493.591 2.258 1.202 10.0590.3110.000 1.165 254.2260.000 0.000 832.0256.692.534 10.041 248.07 0.02 180.0
3/28/2025 07:01 0.000247.7150.005 4.809 1.492493.358 2.253 1.259 10.0470.1360.000 1.156 254.3520.000 0.000 832.0256.872.626 10.049 247.72 0.02 180.0
3/28/2025 07:02 0.000248.2550.006 4.833 1.307493.406 2.247 1.318 9.9890.2330.000 1.143 254.5340.000 0.000 832.0257.042.616 10.051 248.25 0.02 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
3/28/2025 07:05 0.0000.6160.027 0.000 0.0000.601 0.000 0.653 0.0000.0000.149 0.000 0.0630.030 0.173 832.00.410.000 0.000 0.62 0.11 180.0
3/28/2025 07:05 0.0000.3030.025 0.000 0.0000.590 0.000 0.589 0.0000.0000.282 0.000 0.0240.000 0.147 832.00.320.000 0.000 0.30 0.11 180.0
3/28/2025 07:05 0.0000.1980.024 0.000 0.0000.512 0.000 0.598 0.0000.0000.368 0.000 0.0000.000 0.123 832.00.250.000 0.000 0.20 0.10 179.0
CTS System with Response Time
3/28/2025 07:07 0.0000.0000.033 0.000 0.0000.508 0.014 0.577 0.0530.0000.000 98.918 0.0000.000 0.126 832.066.200.000 0.000 0.00 0.06 180.0
3/28/2025 07:08 0.0000.0000.031 0.000 0.0000.524 0.009 0.480 0.0010.0000.000 99.040 0.0000.000 0.130 832.066.290.000 0.000 0.00 0.06 180.0
3/28/2025 07:08 0.0000.0000.031 0.000 0.0000.573 0.016 0.445 0.0010.0000.000 99.063 0.0000.000 0.105 832.066.260.000 0.000 0.00 0.06 180.0
NO2/Mid O2 System with Response Time
3/28/2025 07:17 100.2942.1300.013 0.000 0.1140.516 1.006 0.137 0.7390.0000.955 0.000 0.0000.221 0.120 832.00.270.050 0.000 102.42 10.25 180.0
3/28/2025 07:17 100.3202.1360.013 0.000 0.0000.516 0.997 0.208 0.7990.0000.979 0.000 0.0000.177 0.122 832.00.300.086 0.000 102.46 10.26 180.0
3/28/2025 07:18 100.4672.1570.014 0.000 0.2070.596 1.003 0.157 0.7490.0000.329 0.000 0.0000.192 0.057 832.00.180.103 0.000 102.62 10.27 180.0
Spike System with Response Time
3/28/2025 07:19 0.000246.7970.021 4.807 0.418491.342 2.230 1.560 6.8130.1440.929 1.258 252.9710.000 0.000 832.0255.602.679 9.994 246.80 0.02 180.0
3/28/2025 07:20 0.000246.9060.019 4.830 0.475491.776 2.211 1.318 6.7110.1151.195 1.199 253.3330.000 0.000 832.0255.972.751 10.024 246.91 0.02 180.0
3/28/2025 07:20 0.000247.3490.019 4.808 0.461493.065 2.223 1.344 6.5730.1381.072 1.173 253.6040.000 0.000 832.0256.242.779 10.020 247.35 0.02 180.0
Baseline System with Response Time
3/28/2025 07:22 0.0001.0290.016 0.000 0.0001.227 0.080 0.072 0.0760.0001.961 0.000 0.4120.006 0.056 832.00.520.000 0.003 1.03 0.00 180.0
3/28/2025 07:23 0.0000.3870.016 0.000 0.0000.984 0.053 0.022 0.0350.0032.492 0.000 0.2210.091 0.075 832.00.380.018 0.008 0.39 0.00 180.0
3/28/2025 07:23 0.0000.5610.015 0.000 0.1310.968 0.056 0.205 0.3900.0002.652 0.000 0.3690.000 0.000 832.00.370.000 0.000 0.56 0.00 180.0
Run 1 - A 30minute/60min
3/28/2025 12:04 0.86312.64816.445 8.904 70.1797.751 1.130 3.927 1.6150.0000.000 0.117 0.0000.774 0.309 832.01.000.460 0.000 13.51 1.96 180.0
3/28/2025 12:05 0.69512.49916.458 8.909 70.8657.838 1.067 5.192 1.6080.0000.000 0.279 0.0000.763 0.304 832.01.100.454 0.000 13.19 1.90 180.0
3/28/2025 12:06 0.77412.59916.485 8.924 75.5237.749 1.174 5.508 1.8030.0000.000 0.064 0.0000.905 0.302 832.00.980.504 0.000 13.37 1.88 180.0
3/28/2025 12:07 0.00012.18616.489 8.932 89.0447.838 1.120 4.599 1.2970.0000.000 0.172 0.0000.894 0.351 832.01.310.739 0.000 12.19 1.89 180.0
3/28/2025 12:08 0.00012.38916.506 8.935 89.0967.833 1.181 3.617 1.4320.0000.000 0.339 0.0000.855 0.334 832.01.410.770 0.000 12.39 1.85 180.0
3/28/2025 12:09 0.00012.12016.505 8.939 93.7737.538 0.888 2.294 1.7310.0000.000 0.067 0.0000.934 0.329 832.01.160.693 0.000 12.12 1.88 179.0
3/28/2025 12:10 0.00012.50316.537 8.971 84.5147.555 1.052 2.301 1.0850.0000.000 0.000 0.0000.758 0.317 832.01.090.682 0.000 12.50 1.85 180.0
3/28/2025 12:11 1.24012.82416.525 8.969 72.0057.342 1.089 2.663 1.6400.0000.000 0.222 0.0000.871 0.274 832.01.020.487 0.000 14.06 1.85 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 12:12 0.77110.77716.530 8.988 78.3308.083 1.526 5.943 2.0130.0000.000 0.232 0.0000.888 0.289 832.01.040.465 0.000 11.55 1.83 180.0
3/28/2025 12:13 0.00010.83416.556 8.994 91.2839.001 1.599 8.208 1.7120.0000.000 0.194 0.0000.856 0.348 832.01.290.702 0.003 10.83 1.87 180.0
3/28/2025 12:14 1.00311.34116.550 9.006 62.2377.979 1.340 4.769 1.1780.0000.000 0.180 0.0000.772 0.277 832.00.990.478 0.000 12.34 1.86 180.0
3/28/2025 12:15 1.06612.90916.537 9.007 77.2937.582 0.938 2.372 1.9360.0000.000 0.216 0.0000.903 0.296 832.01.030.440 0.000 13.98 1.89 180.0
3/28/2025 12:16 1.02010.98016.531 9.006 63.2257.340 0.908 2.265 1.2650.0000.000 0.089 0.0000.803 0.268 832.00.940.516 0.000 12.00 1.87 180.0
3/28/2025 12:17 0.89711.41916.527 9.009 61.5057.189 0.936 2.260 1.1300.0000.000 0.203 0.0000.834 0.276 832.00.980.436 0.000 12.32 1.88 180.0
3/28/2025 12:18 0.96411.01216.540 9.013 76.3657.218 0.916 2.219 2.0060.0000.000 0.000 0.0000.803 0.269 832.00.930.586 0.000 11.98 1.80 180.0
3/28/2025 12:19 0.82110.73016.553 9.016 76.5766.869 0.901 1.624 1.7910.0000.000 0.000 0.0000.832 0.283 832.00.950.571 0.000 11.55 1.89 180.0
3/28/2025 12:20 0.45310.73516.542 9.006 67.8966.855 0.738 1.008 1.3470.0000.000 0.000 0.0000.882 0.269 832.00.910.561 0.000 11.19 1.86 180.0
3/28/2025 12:21 0.76912.39316.532 8.974 77.2627.130 0.966 2.201 1.9550.0000.000 0.108 0.0000.756 0.272 832.01.000.582 0.000 13.16 1.84 180.0
3/28/2025 12:22 0.37512.67916.534 8.977 67.5007.206 1.084 3.043 1.4350.0000.000 0.032 0.0000.826 0.259 832.00.940.605 0.000 13.05 1.86 180.0
3/28/2025 12:23 0.80212.18216.526 8.967 74.9656.995 0.914 2.939 1.8110.0000.000 0.452 0.0000.782 0.274 832.01.260.611 0.001 12.98 1.85 180.0
3/28/2025 12:24 0.00012.09116.539 8.964 83.5187.394 1.050 2.845 1.2800.0000.000 0.129 0.0000.754 0.315 832.01.210.742 0.001 12.09 1.83 180.0
3/28/2025 12:25 0.90912.25416.535 8.964 77.9226.968 1.016 1.981 1.8940.0000.000 0.301 0.0000.775 0.268 832.01.180.657 0.000 13.16 1.85 180.0
3/28/2025 12:26 0.44112.60616.539 8.972 67.5026.891 0.984 1.898 1.4180.0000.000 0.187 0.0000.826 0.264 832.01.060.604 0.000 13.05 1.88 180.0
3/28/2025 12:27 0.82012.11516.531 8.988 77.0306.736 0.952 1.782 1.7780.0000.000 0.153 0.0000.789 0.269 832.00.940.452 0.002 12.93 1.85 180.0
3/28/2025 12:28 0.17010.67916.520 8.983 73.7887.006 1.222 2.028 1.6550.0000.000 0.161 0.0000.799 0.274 832.01.060.607 0.000 10.85 1.87 180.0
3/28/2025 12:29 0.88310.69016.534 9.001 80.4037.406 1.268 2.975 2.2170.0000.000 0.318 0.0000.874 0.281 832.01.190.627 0.000 11.57 1.84 180.0
3/28/2025 12:30 0.88910.91516.541 9.000 71.3047.179 1.167 3.143 1.6880.0000.000 0.313 0.0000.876 0.279 832.01.200.651 0.000 11.80 1.85 180.0
3/28/2025 12:31 0.98110.29516.530 8.999 77.7036.966 1.048 1.969 1.9840.0000.000 0.183 0.0000.824 0.259 832.01.050.613 0.001 11.28 1.84 180.0
3/28/2025 12:32 0.93010.25716.536 9.004 79.3016.850 0.869 1.491 2.0230.0000.000 0.000 0.0000.897 0.264 832.00.890.539 0.000 11.19 1.88 180.0
3/28/2025 12:33 0.99310.69116.559 9.017 76.1796.920 1.050 1.380 1.8490.0000.000 0.147 0.0000.841 0.279 832.01.020.550 0.002 11.68 1.84 180.0
0.65111.67816.526 8.978 76.1367.374 1.070 3.015 1.6530.0000.000 0.162 0.0000.832 0.288 832.001.0710.579 0.000 12.329 1.863 180.0Avg.
Spike 1
3/28/2025 12:39 3.38428.33614.999 8.560 65.24658.217 0.884 1.219 2.3830.0000.000 2.598 23.0120.644 0.345 832.025.850.616 0.967 31.72 1.74 180.0
Run 1 - B 30minute/60min
3/28/2025 12:41 0.92713.01816.496 8.951 77.4228.332 0.536 0.747 2.0090.0000.000 0.316 0.3980.817 0.398 832.01.780.571 0.041 13.95 1.84 180.0
3/28/2025 12:42 1.08012.03516.579 8.984 73.0066.274 0.583 0.697 1.6900.0000.000 0.314 0.0000.810 0.264 832.01.180.658 0.005 13.12 1.78 180.0
3/28/2025 12:43 1.12212.08516.558 8.978 72.3726.369 0.694 0.770 1.6070.0000.000 0.412 0.0000.841 0.271 832.01.230.619 0.001 13.21 1.81 180.0
3/28/2025 12:44 1.08412.26416.574 9.007 73.8546.347 0.645 0.669 1.7130.0000.000 0.282 0.0000.795 0.265 831.01.120.606 0.000 13.35 1.77 180.0
3/28/2025 12:45 0.94912.60116.567 9.015 68.6466.444 0.837 0.817 1.5240.0000.000 0.302 0.0000.806 0.262 832.01.100.555 0.001 13.55 1.86 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 12:46 0.31812.60316.530 9.004 61.0296.286 0.681 0.600 1.1820.0000.000 0.281 0.0000.757 0.254 832.01.080.574 0.002 12.92 1.84 180.0
3/28/2025 12:47 0.74212.81516.513 9.000 59.4916.151 0.657 0.536 1.0690.0000.000 0.085 0.0000.773 0.262 831.00.950.550 0.000 13.56 1.87 180.0
3/28/2025 12:48 0.65510.61816.486 8.990 61.5386.129 0.728 0.767 1.1280.0000.000 0.459 0.0000.840 0.260 831.01.190.550 0.000 11.27 1.91 180.0
3/28/2025 12:49 0.38410.15816.493 8.988 78.5036.121 0.626 0.720 1.8420.0000.000 0.376 0.0000.828 0.266 831.01.150.545 0.002 10.54 1.86 180.0
3/28/2025 12:50 0.50610.32916.509 9.016 68.4966.222 0.627 0.511 1.4420.0000.000 0.064 0.0000.803 0.257 831.00.890.504 0.000 10.83 1.91 180.0
3/28/2025 12:51 0.47910.71316.465 8.976 56.3665.965 0.632 0.483 0.8780.0000.000 0.117 0.0000.779 0.281 831.00.980.506 0.000 11.19 1.94 180.0
3/28/2025 12:52 0.53010.36216.503 8.983 61.7036.086 0.567 0.537 1.1160.0000.000 0.205 0.0000.797 0.270 831.01.050.564 0.001 10.89 1.91 180.0
3/28/2025 12:53 0.76212.36716.483 8.980 61.7036.187 0.607 0.727 1.1570.0000.000 0.162 0.0000.784 0.266 831.01.010.551 0.005 13.13 1.90 180.0
3/28/2025 12:54 0.48312.07116.506 8.993 70.7236.359 0.852 1.229 1.4770.0000.000 0.213 0.0000.826 0.262 831.01.020.531 0.003 12.55 1.84 180.0
3/28/2025 12:55 0.51312.44516.530 8.987 71.1306.936 1.227 3.121 1.7310.0000.000 0.148 0.0000.765 0.256 831.01.010.594 0.008 12.96 1.85 180.0
3/28/2025 12:56 0.36312.83516.534 8.998 59.5106.523 0.976 2.265 1.1780.0000.000 0.509 0.0000.711 0.260 831.01.250.590 0.000 13.20 1.84 180.0
3/28/2025 12:57 0.43112.15316.559 9.002 71.1956.686 0.920 1.920 1.5480.0000.000 0.048 0.0000.880 0.268 831.00.960.583 0.003 12.58 1.83 180.0
3/28/2025 12:58 0.44512.15616.545 9.012 77.5296.931 1.130 3.515 1.9900.0000.000 0.538 0.0000.866 0.271 831.01.270.554 0.002 12.60 1.83 180.0
3/28/2025 12:59 0.44312.52416.555 9.024 75.3546.873 1.049 1.821 2.3010.0000.000 0.105 0.0000.735 0.287 831.01.050.607 0.002 12.97 1.82 180.0
3/28/2025 13:00 0.91512.37216.519 9.017 58.6056.471 0.580 1.102 1.0480.0000.000 0.263 0.0000.805 0.269 831.01.040.492 0.003 13.29 1.91 180.0
3/28/2025 13:01 0.40810.24216.485 9.008 65.7496.336 0.745 0.810 1.4020.0000.000 0.154 0.0000.781 0.258 831.00.990.555 0.001 10.65 1.91 180.0
3/28/2025 13:02 0.59810.59716.484 9.004 67.0066.328 0.688 0.844 1.4090.0000.000 0.026 0.0000.754 0.253 831.00.860.503 0.000 11.20 1.87 180.0
3/28/2025 13:03 0.53711.01216.486 9.014 60.9236.179 0.869 0.790 1.1090.0000.000 0.189 0.0000.784 0.264 831.01.010.540 0.000 11.55 1.87 180.0
3/28/2025 13:04 0.55713.02616.472 9.009 56.5066.070 0.659 0.621 0.9390.0000.000 0.113 0.0000.741 0.255 831.00.960.564 0.004 13.58 1.90 180.0
3/28/2025 13:05 0.68110.40416.486 9.005 66.2076.089 0.754 0.496 1.3370.0000.000 0.234 0.0000.821 0.270 831.01.070.557 0.004 11.09 1.86 180.0
3/28/2025 13:06 1.19010.54216.483 9.004 66.6515.844 0.697 0.439 1.1840.0000.000 0.029 0.0000.918 0.277 831.00.930.535 0.000 11.73 1.92 180.0
3/28/2025 13:07 0.57810.90616.464 8.998 52.8185.761 0.683 0.520 0.8410.0000.000 0.212 0.0000.777 0.257 831.00.980.484 0.002 11.48 1.95 180.0
3/28/2025 13:08 0.45610.33316.464 8.984 59.9845.757 0.555 0.320 1.1570.0000.000 0.149 0.0000.734 0.248 831.00.980.576 0.004 10.79 1.90 180.0
3/28/2025 13:09 0.71412.93316.466 8.988 37.3825.528 0.522 0.525 0.3880.0000.000 0.283 0.0000.691 0.264 831.01.040.489 0.001 13.65 1.90 180.0
3/28/2025 13:10 0.74312.40916.482 8.980 60.1365.745 0.476 0.506 1.0680.0000.000 0.357 0.0000.777 0.250 831.01.130.586 0.000 13.15 1.88 180.0
0.65311.69816.509 8.997 65.0516.311 0.727 0.981 1.3490.0000.000 0.232 0.0130.793 0.268 831.171.0750.556 0.003 12.351 1.869 180.0Avg.
0.65211.68816.517 8.987 70.5946.842 0.898 1.998 1.5010.0000.000 0.197 0.0070.812 0.278 831.581.0730.568 0.002 12.340 1.866 180.0Run 1 Avg:
Baseline 1
3/28/2025 13:13 0.0000.0000.031 0.000 0.0000.514 0.121 0.110 0.0000.0001.328 0.000 0.0000.000 0.067 831.00.130.000 0.002 0.00 0.00 180.0
Run 2 - A 30minute/60min
3/28/2025 13:17 0.48512.66616.386 8.927 59.4865.722 0.586 0.683 0.9300.0000.000 0.214 0.0000.766 0.257 831.01.010.527 0.002 13.15 1.89 180.0
3/28/2025 13:18 0.68512.81716.451 8.968 66.6895.862 0.612 0.390 1.3640.0000.000 0.085 0.0000.754 0.265 831.00.940.522 0.001 13.50 1.87 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 13:19 1.18512.64716.477 8.984 68.6975.748 0.848 0.581 1.3380.0000.000 0.154 0.0000.815 0.266 831.01.000.548 0.000 13.83 1.85 180.0
3/28/2025 13:20 0.64412.71316.515 9.015 69.3415.795 0.636 0.498 1.3170.0000.000 0.154 0.0000.815 0.270 831.01.030.579 0.003 13.36 1.83 180.0
3/28/2025 13:21 0.67110.66916.505 8.997 61.5855.719 0.608 0.566 1.1580.0000.000 0.000 0.0000.778 0.253 831.00.820.477 0.000 11.34 1.86 180.0
3/28/2025 13:22 0.34010.95016.481 8.989 55.4455.749 0.546 0.178 0.7910.0000.000 0.040 0.0000.694 0.272 831.00.930.543 0.000 11.29 1.84 180.0
3/28/2025 13:23 0.54810.70616.457 8.996 72.6735.695 0.620 0.307 1.5850.0000.000 0.075 0.0000.813 0.273 831.00.960.550 0.000 11.25 1.90 180.0
3/28/2025 13:24 0.42212.77316.419 8.969 58.3155.648 0.695 0.435 1.0040.0000.000 0.178 0.0000.758 0.259 831.01.020.571 0.001 13.20 1.96 180.0
3/28/2025 13:25 0.07312.19916.457 8.977 82.8075.702 0.601 0.374 1.0570.0000.000 0.236 0.0000.640 0.310 831.01.280.754 0.003 12.27 1.85 180.0
3/28/2025 13:26 0.57412.12416.462 8.962 66.0935.553 0.516 0.326 1.2220.0000.000 0.318 0.0000.782 0.268 831.01.140.582 0.002 12.70 1.91 180.0
3/28/2025 13:27 0.40912.20516.478 8.955 69.2495.573 0.587 0.277 1.2800.0000.000 0.194 0.0000.768 0.266 831.01.030.559 0.001 12.61 1.89 180.0
3/28/2025 13:28 0.51712.50216.468 8.959 54.1475.448 0.582 0.459 0.7160.0000.000 0.261 0.0000.760 0.260 831.01.030.506 0.003 13.02 1.98 180.0
3/28/2025 13:29 0.70112.27216.437 8.953 57.3055.445 0.531 0.245 0.8360.0000.000 0.083 0.0000.797 0.255 831.00.940.558 0.002 12.97 1.88 180.0
3/28/2025 13:30 0.49712.39616.479 8.975 65.0585.279 0.547 0.260 1.1750.0000.000 0.230 0.0000.786 0.251 831.01.030.557 0.003 12.89 1.86 180.0
3/28/2025 13:31 0.71812.45616.461 8.976 57.9985.299 0.527 0.267 0.9410.0000.000 0.378 0.0000.813 0.256 831.01.110.525 0.001 13.17 1.96 180.0
3/28/2025 13:32 0.34212.83616.454 8.993 61.0795.676 0.749 0.517 1.0970.0000.000 0.242 0.0000.737 0.240 831.01.030.577 0.001 13.18 1.86 180.0
3/28/2025 13:33 0.64113.11816.436 8.989 54.4855.628 0.877 0.994 0.8410.0000.000 0.220 0.0000.803 0.269 831.01.020.500 0.001 13.76 1.96 180.0
3/28/2025 13:34 0.69812.75816.438 8.983 62.7635.656 0.783 0.682 1.1400.0000.000 0.048 0.0000.812 0.272 831.00.930.538 0.000 13.46 1.86 180.0
3/28/2025 13:35 0.58512.91216.440 8.993 53.0505.412 0.625 0.539 0.7700.0000.000 0.266 0.0000.759 0.256 831.01.050.544 0.003 13.50 1.91 180.0
3/28/2025 13:36 0.85812.71616.425 8.979 52.8865.532 0.431 0.319 0.8620.0000.000 0.302 0.0000.768 0.272 831.01.100.535 0.000 13.57 1.87 180.0
3/28/2025 13:37 1.11510.78116.461 9.001 62.7355.910 1.107 1.173 1.1470.0000.000 0.158 0.0000.890 0.266 831.01.000.546 0.000 11.90 1.87 180.0
3/28/2025 13:38 1.15912.58916.431 8.985 60.7646.460 0.712 2.005 1.1850.0000.000 0.039 0.0000.840 0.279 831.00.940.535 0.003 13.75 1.92 180.0
3/28/2025 13:39 0.95712.50216.430 8.977 77.6697.090 1.513 4.336 1.8820.0000.000 0.240 0.0000.841 0.289 831.01.150.623 0.000 13.46 1.89 180.0
3/28/2025 13:40 1.14013.16616.477 9.001 58.6826.755 1.183 3.419 1.1140.0000.000 0.310 0.0000.834 0.263 831.01.070.512 0.003 14.31 1.89 180.0
3/28/2025 13:41 1.05012.70216.403 8.966 64.1686.485 1.022 2.395 1.2610.0000.000 0.103 0.0000.788 0.277 831.01.010.578 0.002 13.75 1.99 180.0
3/28/2025 13:42 0.74012.40616.298 8.912 56.7025.952 0.643 1.395 0.9250.0000.000 0.090 0.0000.685 0.273 831.00.930.492 0.000 13.15 1.96 180.0
3/28/2025 13:43 0.32812.58016.361 8.926 64.3116.072 0.766 0.983 1.3180.0000.000 0.247 0.0000.767 0.259 831.01.050.545 0.004 12.91 2.00 180.0
3/28/2025 13:44 0.38412.15616.318 8.923 46.8985.559 0.547 0.620 0.4920.0000.000 0.012 0.0000.781 0.257 831.00.830.466 0.000 12.54 1.96 180.0
3/28/2025 13:45 0.93012.15416.434 8.957 64.3555.841 0.545 0.683 1.2640.0000.000 0.033 0.0000.870 0.276 831.00.940.544 0.000 13.08 1.88 180.0
3/28/2025 13:46 1.07612.76716.416 8.948 56.1725.897 0.891 1.198 0.9590.0000.000 0.047 0.0000.853 0.254 831.00.880.510 0.000 13.84 1.88 180.0
0.68212.34116.439 8.971 62.0545.805 0.715 0.903 1.0990.0000.000 0.165 0.0000.786 0.266 831.001.0070.547 0.001 13.024 1.901 180.0Avg.
Spike 2
3/28/2025 13:50 5.50531.40514.877 8.543 40.48158.033 0.680 2.841 1.3530.0000.000 2.477 22.7470.599 0.394 831.025.300.163 0.946 36.91 1.82 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
3/28/2025 13:52 1.11511.78116.315 8.938 55.9129.034 1.103 2.187 1.1290.0000.000 0.091 0.3630.848 0.394 831.01.460.380 0.037 12.90 1.91 180.0
3/28/2025 13:53 0.75612.98816.392 8.975 50.3746.745 0.859 1.064 0.8080.0000.000 0.000 0.0000.735 0.272 831.00.840.448 0.000 13.74 1.94 180.0
3/28/2025 13:55 1.03911.04916.378 8.962 39.6826.331 0.554 0.978 0.4330.0000.000 0.000 0.0000.814 0.259 831.00.820.455 0.000 12.09 1.90 180.0
3/28/2025 13:56 0.96013.10516.344 8.948 39.5796.168 0.686 0.795 0.5820.0000.000 0.168 0.0000.769 0.261 831.00.930.447 0.002 14.07 1.94 180.0
3/28/2025 13:57 0.86912.91716.406 8.971 47.9887.325 0.581 2.647 0.7460.0000.000 0.083 0.0000.703 0.263 831.00.910.499 0.000 13.79 1.87 180.0
3/28/2025 13:58 1.11212.73016.428 8.969 55.1697.234 0.836 2.413 0.8040.0000.000 0.112 0.0000.820 0.285 831.00.930.425 0.003 13.84 1.88 180.0
3/28/2025 13:59 0.63212.25416.438 8.966 67.4776.834 0.901 1.359 1.3410.0000.000 0.368 0.0000.693 0.265 831.01.080.458 0.000 12.89 1.87 180.0
3/28/2025 14:00 1.09812.34516.437 8.952 59.5836.517 0.892 1.213 1.0410.0000.000 0.245 0.0000.884 0.260 831.01.010.484 0.000 13.44 1.87 180.0
3/28/2025 14:01 1.06612.11516.451 8.946 66.2356.123 0.780 0.986 1.2370.0000.000 0.350 0.0000.796 0.271 831.01.180.607 0.001 13.18 1.85 180.0
3/28/2025 14:02 1.02012.34916.453 8.951 63.9155.845 0.827 0.913 1.1850.0000.000 0.195 0.0000.798 0.259 831.00.980.496 0.000 13.37 1.88 180.0
3/28/2025 14:03 0.58312.11116.465 8.945 57.4085.764 0.545 0.677 0.8590.0000.000 0.355 0.0000.726 0.264 831.01.130.540 0.002 12.69 1.88 180.0
3/28/2025 14:04 0.78712.20516.441 8.953 55.7545.613 0.530 0.303 0.8150.0000.000 0.197 0.0000.867 0.242 831.00.930.477 0.003 12.99 1.86 180.0
3/28/2025 14:05 1.10412.38116.446 8.954 64.4785.520 0.532 0.359 1.0610.0000.000 0.258 0.0000.785 0.273 831.01.110.580 0.000 13.49 1.85 180.0
3/28/2025 14:06 0.94710.57716.471 9.000 50.9885.679 0.543 0.433 0.7270.0000.000 0.180 0.0000.846 0.258 831.00.990.529 0.004 11.52 1.89 180.0
3/28/2025 14:07 0.98212.65716.439 8.966 65.0216.006 0.802 0.876 1.3310.0000.000 0.168 0.0000.780 0.268 831.00.950.445 0.000 13.64 1.84 180.0
3/28/2025 14:08 0.96010.43816.483 8.982 68.1046.806 1.103 3.290 1.4950.0000.000 0.126 0.0000.865 0.274 831.00.980.525 0.000 11.40 1.86 180.0
3/28/2025 14:09 0.78710.65916.442 8.976 52.9956.397 0.936 1.252 0.8220.0000.000 0.222 0.0000.830 0.261 831.00.980.465 0.003 11.45 1.86 180.0
3/28/2025 14:10 0.88510.41716.430 8.982 47.4995.976 0.659 0.808 0.5590.0000.000 0.063 0.0000.843 0.263 831.00.900.504 0.002 11.30 1.85 180.0
3/28/2025 14:11 1.23810.29916.441 8.974 64.1656.157 0.825 1.005 1.1930.0000.000 0.000 0.0000.876 0.266 831.00.820.430 0.000 11.54 1.87 180.0
3/28/2025 14:12 0.98311.02816.460 8.972 59.8896.188 1.018 1.585 1.1200.0000.000 0.199 0.0000.800 0.280 831.00.990.440 0.001 12.01 1.87 180.0
3/28/2025 14:13 0.91310.50516.441 8.986 55.2315.935 0.563 0.900 0.9320.0000.000 0.000 0.0000.773 0.273 831.00.830.430 0.000 11.42 1.87 180.0
3/28/2025 14:14 0.88710.20216.410 8.969 67.6605.832 0.754 0.525 1.3730.0000.000 0.244 0.0000.872 0.284 831.01.100.550 0.003 11.09 1.88 180.0
3/28/2025 14:15 1.14910.36316.437 8.969 59.6745.914 0.745 0.652 0.9870.0000.000 0.037 0.0000.958 0.254 831.00.860.492 0.000 11.51 1.85 180.0
3/28/2025 14:16 0.90912.32916.452 8.976 65.3425.898 1.104 1.262 1.2530.0000.000 0.036 0.0000.813 0.254 831.00.840.465 0.002 13.24 1.88 180.0
3/28/2025 14:17 0.63512.39616.422 8.939 59.5455.791 0.814 0.987 1.1080.0000.000 0.094 0.0000.781 0.250 831.00.900.511 0.000 13.03 1.90 180.0
3/28/2025 14:18 0.97912.26916.420 8.942 31.6725.802 0.588 0.975 0.3620.0000.000 0.000 0.0000.794 0.230 831.00.760.443 0.000 13.25 1.99 180.0
3/28/2025 14:19 0.67212.00516.355 8.895 49.5846.863 0.687 1.613 0.6590.0000.000 0.061 0.0000.819 0.245 831.00.830.449 0.000 12.68 1.94 180.0
3/28/2025 14:20 0.81811.82816.375 8.899 56.9026.452 0.840 1.670 0.9850.0000.000 0.254 0.0000.812 0.238 831.00.950.452 0.000 12.65 1.89 180.0
3/28/2025 14:21 0.96211.88316.392 8.911 67.6816.539 1.092 2.455 1.2450.0000.000 0.000 0.0000.804 0.265 831.00.820.436 0.000 12.85 1.92 180.0
3/28/2025 14:22 0.83711.83716.396 8.930 64.8366.081 0.960 1.371 1.1600.0000.000 0.159 0.0000.813 0.268 831.00.890.372 0.003 12.67 1.92 180.0
0.92311.73416.422 8.957 57.0116.312 0.789 1.252 0.9780.0000.000 0.142 0.0120.811 0.267 831.000.9570.474 0.002 12.658 1.886 180.0Avg.
0.80312.03816.430 8.964 59.5326.059 0.752 1.078 1.0390.0000.000 0.154 0.0060.798 0.266 831.000.9820.511 0.002 12.841 1.894 180.0Run 2 Avg:
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
3/28/2025 14:26 0.0000.1650.029 0.000 0.0000.173 0.086 0.000 0.0470.0001.023 0.000 0.0000.000 0.103 831.00.210.000 0.002 0.17 0.00 180.0
Run 3 - A 30minute/60min
3/28/2025 14:28 1.1619.83616.181 8.849 62.5206.248 0.833 0.919 1.2760.0000.000 0.212 0.0000.925 0.257 831.01.020.539 0.003 11.00 1.92 180.0
3/28/2025 14:29 0.94610.53016.344 8.925 35.2146.018 0.620 0.682 0.3470.0000.000 0.000 0.0000.820 0.245 831.00.720.351 0.000 11.48 1.95 180.0
3/28/2025 14:30 1.09310.33116.354 8.931 35.9675.944 0.516 0.957 0.3660.0000.000 0.101 0.0000.776 0.253 831.00.830.385 0.000 11.42 1.88 180.0
3/28/2025 14:32 0.66110.04216.378 8.934 63.6986.127 0.923 1.668 1.1250.0000.000 0.166 0.0000.814 0.273 831.00.930.414 0.000 10.70 1.88 180.0
3/28/2025 14:33 1.26810.43716.368 8.928 32.3085.674 0.744 1.018 0.1410.0000.000 0.000 0.0000.827 0.278 831.00.720.238 0.001 11.71 1.96 180.0
3/28/2025 14:34 0.7539.96216.359 8.914 48.4316.491 0.409 1.261 0.7860.0000.000 0.022 0.0000.801 0.239 831.00.770.416 0.000 10.71 1.96 180.0
3/28/2025 14:35 0.92110.01216.346 8.885 56.6686.602 1.047 1.620 0.6840.0000.000 0.037 0.0000.838 0.265 831.00.750.297 0.000 10.93 2.01 180.0
3/28/2025 14:36 0.90911.89716.357 8.894 42.0946.612 0.613 1.898 0.5610.0000.000 0.000 0.0000.803 0.237 830.00.710.354 0.000 12.81 1.99 180.0
3/28/2025 14:37 0.75811.92916.325 8.878 59.5346.594 0.990 2.633 0.7710.0000.000 0.000 0.0000.809 0.250 831.00.760.385 0.000 12.69 1.98 180.0
3/28/2025 14:38 0.66511.91616.304 8.874 52.3396.014 0.691 1.182 0.7280.0000.000 0.030 0.0000.768 0.254 830.00.790.400 0.000 12.58 2.00 180.0
3/28/2025 14:39 0.83511.30716.249 8.814 54.7865.548 0.455 0.744 0.4390.0000.000 0.000 0.0000.759 0.245 831.00.730.361 0.000 12.14 2.20 180.0
3/28/2025 14:40 0.76211.70316.175 8.802 54.0535.758 0.579 1.117 0.7510.0000.000 0.000 0.0000.710 0.247 830.00.750.378 0.000 12.46 2.16 180.0
3/28/2025 14:41 0.88611.97716.212 8.827 52.2655.936 0.869 1.979 0.6600.0000.000 0.000 0.0000.744 0.244 830.00.730.363 0.004 12.86 2.17 180.0
3/28/2025 14:42 0.5799.79416.189 8.839 61.2316.556 1.021 3.586 0.9170.0000.000 0.000 0.0000.801 0.251 830.00.760.384 0.000 10.37 2.14 180.0
3/28/2025 14:43 0.85210.24416.190 8.846 46.2696.300 1.032 2.820 0.5830.0000.000 0.198 0.0000.815 0.250 830.00.840.311 0.002 11.10 2.14 180.0
3/28/2025 14:44 0.87210.09616.188 8.846 55.0986.001 0.812 1.483 0.6460.0000.000 0.000 0.0000.817 0.257 830.00.710.287 0.000 10.97 2.15 180.0
3/28/2025 14:45 1.30210.35216.218 8.886 53.9025.990 0.810 1.559 0.5940.0000.000 0.199 0.0000.822 0.256 830.00.850.314 0.002 11.65 2.08 180.0
3/28/2025 14:46 0.70310.07316.175 8.865 58.2825.836 1.013 1.354 0.7440.0000.000 0.097 0.0000.721 0.251 830.00.790.334 0.002 10.78 2.17 180.0
3/28/2025 14:47 1.01110.38516.162 8.844 43.1865.581 0.591 0.718 0.2780.0000.000 0.000 0.0000.706 0.240 830.00.710.347 0.000 11.40 2.13 180.0
3/28/2025 14:48 0.74910.17316.193 8.863 61.9415.542 0.830 0.832 0.8360.0000.000 0.000 0.0000.799 0.251 830.00.770.410 0.000 10.92 2.14 180.0
3/28/2025 14:49 0.7239.95316.177 8.845 48.9965.141 0.800 0.687 0.4830.0000.000 0.000 0.0000.704 0.251 830.00.740.351 0.000 10.68 2.16 180.0
3/28/2025 14:50 1.15210.29116.198 8.857 33.5885.062 0.473 0.404 0.1520.0000.000 0.000 0.0000.792 0.239 830.00.730.379 0.000 11.44 2.08 180.0
3/28/2025 14:51 0.2299.54416.185 8.868 52.6235.093 0.523 0.304 0.5420.0000.000 0.000 0.0000.892 0.245 830.00.840.524 0.001 9.77 2.12 180.0
3/28/2025 14:52 0.98110.01216.157 8.827 40.8174.902 0.515 0.253 0.4140.0000.000 0.000 0.0000.735 0.236 830.00.780.467 0.000 10.99 2.18 180.0
3/28/2025 14:53 1.0089.97916.148 8.814 30.6454.905 0.358 0.184 0.0950.0000.000 0.000 0.0000.657 0.248 830.00.760.398 0.000 10.99 2.15 180.0
3/28/2025 14:54 0.8889.96216.148 8.814 43.8164.838 0.365 0.148 0.2580.0000.000 0.000 0.0000.707 0.231 830.00.770.467 0.000 10.85 2.13 180.0
3/28/2025 14:55 1.0779.88116.219 8.852 30.7674.714 0.330 0.147 0.2270.0000.000 0.117 0.0000.757 0.232 830.00.850.458 0.003 10.96 2.06 180.0
3/28/2025 14:56 0.52711.55116.242 8.846 49.8725.192 0.405 0.539 0.7280.0000.000 0.050 0.0000.738 0.241 830.00.800.418 0.001 12.08 2.06 180.0
3/28/2025 14:57 0.73211.61816.246 8.851 47.7865.128 0.579 0.464 0.6170.0000.000 0.237 0.0000.740 0.227 830.00.930.479 0.000 12.35 2.12 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 14:58 0.82611.46616.247 8.847 45.0505.058 0.513 0.371 0.4300.0000.000 0.045 0.0000.783 0.229 830.00.800.470 0.000 12.29 2.08 180.0
0.86110.57516.241 8.862 48.4585.714 0.675 1.118 0.5730.0000.000 0.050 0.0000.779 0.247 830.300.7880.389 0.001 11.436 2.072 180.0Avg.
Spike 3
3/28/2025 15:02 4.41526.93714.719 8.449 36.95655.763 0.722 0.669 1.8000.0000.000 2.393 22.1990.613 0.353 830.024.700.296 0.935 31.35 2.01 180.0
Run 3 - B 30minute/60min
3/28/2025 15:05 0.8049.96516.266 8.907 47.0215.164 0.416 0.172 0.4180.0000.000 0.000 0.0000.810 0.267 830.00.850.468 0.003 10.77 2.04 180.0
3/28/2025 15:06 0.96610.42516.209 8.856 43.5765.065 0.543 0.268 0.5710.0000.000 0.000 0.0000.858 0.246 830.00.830.501 0.000 11.39 2.08 180.0
3/28/2025 15:08 0.6609.73116.193 8.871 57.2244.836 0.500 0.000 0.8150.0000.000 0.200 0.0000.722 0.259 830.01.020.553 0.001 10.39 2.11 180.0
3/28/2025 15:09 0.84310.15616.206 8.868 34.1124.723 0.409 0.000 0.3340.0000.000 0.000 0.0000.760 0.236 830.00.760.427 0.000 11.00 2.20 180.0
3/28/2025 15:10 0.8189.87216.201 8.843 48.0894.829 0.515 0.171 0.3440.0000.000 0.000 0.0000.871 0.238 830.00.760.432 0.000 10.69 2.11 180.0
3/28/2025 15:11 1.15910.31116.240 8.867 29.3224.687 0.539 0.207 0.3120.0000.000 0.231 0.0000.775 0.231 830.00.860.369 0.003 11.47 2.11 180.0
3/28/2025 15:12 1.0599.54516.222 8.818 31.7565.108 0.317 0.283 0.0480.0000.000 0.000 0.0000.858 0.263 830.00.770.374 0.000 10.60 2.12 180.0
3/28/2025 15:13 0.8239.63416.212 8.830 45.1545.124 0.468 0.212 0.3910.0000.000 0.000 0.0000.767 0.229 830.00.740.418 0.000 10.46 2.15 180.0
3/28/2025 15:14 0.87111.41416.204 8.825 50.6864.872 0.474 0.303 0.6000.0000.000 0.286 0.0000.723 0.241 830.00.950.418 0.002 12.29 2.12 180.0
3/28/2025 15:15 0.82611.67516.227 8.830 46.2234.845 0.470 0.062 0.5640.0000.000 0.070 0.0000.779 0.219 830.00.830.516 0.000 12.50 2.10 180.0
3/28/2025 15:16 0.92911.36516.237 8.840 47.8764.752 0.433 0.105 0.5690.0000.000 0.215 0.0000.777 0.229 830.00.910.465 0.003 12.29 2.06 180.0
3/28/2025 15:17 0.63311.76516.239 8.870 56.2284.837 0.457 0.000 0.8290.0000.000 0.092 0.0000.795 0.229 830.00.880.540 0.000 12.40 2.07 180.0
3/28/2025 15:18 0.6699.84016.235 8.859 59.5024.812 0.669 0.077 0.6530.0000.000 0.000 0.0000.775 0.226 830.00.780.489 0.005 10.51 2.05 180.0
3/28/2025 15:19 0.75010.10716.246 8.875 51.6784.869 0.593 0.102 0.6130.0000.000 0.102 0.0000.725 0.238 830.00.800.381 0.000 10.86 2.05 180.0
3/28/2025 15:20 0.6949.78216.221 8.880 54.0114.865 0.653 0.047 0.6860.0000.000 0.043 0.0000.765 0.247 830.00.850.486 0.000 10.48 2.08 180.0
3/28/2025 15:21 0.77210.29316.228 8.878 53.9334.838 0.623 0.000 0.7470.0000.000 0.010 0.0000.701 0.229 830.00.820.528 0.000 11.07 2.06 180.0
3/28/2025 15:22 0.7669.89016.246 8.865 58.1034.799 0.726 0.079 0.6860.0000.000 0.000 0.0000.822 0.231 830.00.730.406 0.000 10.66 2.16 180.0
3/28/2025 15:23 0.8829.95816.213 8.850 53.3464.908 0.584 0.000 0.6800.0000.000 0.000 0.0000.784 0.248 830.00.810.477 0.000 10.84 2.14 180.0
3/28/2025 15:24 0.8229.88816.188 8.825 43.0604.711 0.449 0.204 0.4210.0000.000 0.069 0.0000.833 0.241 830.00.810.431 0.000 10.71 2.12 180.0
3/28/2025 15:25 0.6079.45716.144 8.812 52.7104.646 0.465 0.050 0.5350.0000.000 0.000 0.0000.679 0.236 830.00.780.456 0.000 10.06 2.23 180.0
3/28/2025 15:26 0.5839.71616.078 8.782 49.9504.532 0.654 0.000 0.6900.0000.000 0.095 0.0000.745 0.230 830.00.890.546 0.002 10.30 2.25 180.0
3/28/2025 15:27 1.0679.72516.055 8.765 41.2084.461 0.499 0.000 0.1380.0000.000 0.000 0.0000.675 0.277 830.00.790.359 0.000 10.79 2.26 180.0
3/28/2025 15:28 0.8509.89516.107 8.776 43.4194.596 0.463 0.000 0.4330.0000.000 0.114 0.0000.841 0.224 830.00.810.436 0.000 10.75 2.25 180.0
3/28/2025 15:29 1.1669.75116.131 8.769 33.7624.378 0.436 0.000 0.0880.0000.000 0.000 0.0000.810 0.255 830.00.670.240 0.000 10.92 2.25 180.0
3/28/2025 15:30 0.9499.38816.094 8.757 39.5594.404 0.427 0.001 0.2980.0000.000 0.000 0.0000.826 0.220 830.00.700.384 0.001 10.34 2.25 180.0
3/28/2025 15:31 0.7829.39716.098 8.761 43.3684.390 0.361 0.000 0.4690.0000.000 0.185 0.0000.741 0.214 830.00.870.484 0.002 10.18 2.17 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 15:32 0.84311.44116.114 8.777 38.1464.222 0.377 0.000 0.3780.0000.000 0.386 0.0000.775 0.226 830.00.990.416 0.003 12.28 2.25 180.0
3/28/2025 15:33 0.60511.23316.088 8.766 54.4924.405 0.390 0.000 0.7880.0000.000 0.150 0.0000.690 0.240 830.00.900.475 0.004 11.84 2.23 180.0
3/28/2025 15:34 0.75311.80716.154 8.798 38.6634.486 0.415 0.000 0.3770.0000.000 0.054 0.0000.805 0.229 830.00.800.452 0.000 12.56 2.17 180.0
3/28/2025 15:35 0.7989.99716.184 8.833 41.8464.592 0.411 0.000 0.1710.0000.000 0.000 0.0000.776 0.228 830.00.740.421 0.000 10.80 2.14 180.0
0.82510.24716.183 8.828 46.2674.725 0.491 0.078 0.4880.0000.000 0.077 0.0000.775 0.238 830.000.8230.445 0.001 11.073 2.146 180.0Avg.
0.84310.41116.212 8.845 47.3635.219 0.583 0.598 0.5300.0000.000 0.064 0.0000.777 0.242 830.150.8060.417 0.001 11.255 2.109 180.0Run 3 Avg:
Baseline 3
3/28/2025 15:41 0.0000.0780.025 0.000 0.0000.257 0.093 0.000 0.0920.0001.045 0.000 0.0000.000 0.077 830.00.150.000 0.001 0.08 0.00 180.0
Post CTS
3/28/2025 15:50 0.0000.0000.024 0.000 0.0000.342 0.044 0.334 0.0000.0000.000 99.233 0.0000.000 0.089 830.066.410.109 0.000 0.00 0.06 180.0
3/28/2025 15:50 0.0000.0000.022 0.000 0.0000.306 0.056 0.316 0.1440.0000.000 99.453 0.0000.111 0.081 830.066.600.207 0.000 0.00 0.06 180.0
3/28/2025 15:50 0.0000.0000.028 0.000 0.0000.291 0.066 0.000 0.0000.0030.000 99.028 0.0000.112 0.038 830.066.100.000 0.000 0.00 0.06 180.0
Post NO2/Mid O2
3/28/2025 15:56 99.5302.0630.008 0.000 0.0000.388 1.038 0.016 0.0860.0000.000 0.000 0.0000.374 0.136 830.00.390.181 0.005 101.59 10.48 180.0
3/28/2025 15:56 99.8672.4870.011 0.000 0.0000.375 1.035 0.387 0.4000.0000.000 0.000 0.0000.150 0.054 830.00.240.203 0.005 102.35 10.42 180.0
3/28/2025 15:56 99.5632.5780.010 0.000 0.0000.298 1.048 0.006 0.4880.0000.215 0.000 0.0000.022 0.137 830.00.280.008 0.000 102.14 10.49 180.0
Post 5-Gas
3/28/2025 15:57 0.000246.9210.017 4.789 2.160489.972 2.286 1.054 8.3820.1170.000 1.290 251.4160.737 0.000 831.0253.962.530 9.969 246.92 0.02 180.0
3/28/2025 15:58 0.000245.3240.017 4.754 4.089493.256 2.382 1.810 6.7990.0410.000 0.954 252.7790.000 0.000 831.0254.962.320 10.043 245.32 0.02 180.0
3/28/2025 15:58 0.000246.9980.016 4.802 2.235493.301 2.320 1.365 7.8880.1790.000 1.110 252.5640.000 0.000 831.0255.062.640 10.017 247.00 0.02 180.0
3/28/2025 15:58 0.000248.0450.016 4.815 3.903494.043 2.318 1.395 7.9380.1090.271 1.162 252.3300.000 0.000 831.0254.882.659 10.027 248.04 0.02 180.0
3/28/2025 15:58 0.000248.6150.015 4.825 0.896495.004 2.357 1.495 7.2650.1440.000 1.161 253.0350.000 0.000 831.0255.572.647 10.019 248.62 0.02 180.0
End of Test Purge
3/28/2025 16:01 0.0000.7210.014 0.000 0.0610.624 0.087 0.030 0.5650.0001.138 0.000 0.2030.121 0.045 827.00.420.188 0.007 0.72 0.00 180.0
3/28/2025 16:01 0.0000.7110.014 0.000 0.0000.637 0.104 0.000 0.6160.0000.687 0.000 0.4010.000 0.008 828.00.480.091 0.015 0.71 0.00 180.0
3/28/2025 16:01 0.0000.0110.011 0.000 0.0000.759 0.077 0.000 0.4200.0001.311 0.000 0.2750.000 0.026 829.00.420.144 0.007 0.01 0.00 180.0
3/28/2025 16:01 0.0000.0290.013 0.000 0.0000.793 0.092 0.106 0.5810.0000.796 0.000 0.3270.000 0.073 830.00.550.110 0.015 0.03 0.00 180.0
3/28/2025 16:01 0.0000.3110.013 0.000 0.0000.753 0.083 0.000 0.4110.0001.355 0.089 0.2620.000 0.018 830.00.370.025 0.016 0.31 0.00 180.0
3/28/2025 16:01 0.0000.0000.009 0.000 0.1070.595 0.067 0.000 0.3770.0000.861 0.000 0.2300.000 0.028 831.00.330.073 0.023 0.00 0.00 180.0
3/28/2025 16:01 0.0000.0380.011 0.000 0.3410.600 0.062 0.159 0.5560.0000.953 0.291 0.1400.000 0.000 831.00.510.270 0.000 0.04 0.00 180.0
GAS
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
3/28/2025 16:01 0.0000.1820.011 0.000 0.0370.359 0.079 0.152 0.2090.0102.000 0.197 0.1740.000 0.067 832.00.560.187 0.010 0.18 0.00 180.0
GAS