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HomeMy WebLinkAboutDDW-2025-004323May 06, 2025 Dear John Steffan: Please find enclosed the analytical results for the 4 sample(s) the laboratory received on 4/30/25 9:10 am and logged in under work order ID05362. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH25137RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID05362-01 Name: Sampled: Received: 04/30/25 09:10 04/24/25 08:40 WS003-COTTONWOOD WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH25137 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA05/02/25 16:36 MAB3U1.910.9 < 0.4 ng/L EPA 533PFMPA05/02/25 16:36 MAB3U1.910.4 < 0.5 ng/L EPA 533PFPeA05/02/25 16:36 MAB3U1.910.5 < 0.5 ng/L EPA 533PFBS05/02/25 16:36 MAB3U1.910.5 < 0.4 ng/L EPA 533PFMBA05/02/25 16:36 MAB3U1.910.4 < 0.5 ng/L EPA 533PFEESA05/02/25 16:36 MAB3U1.910.5 < 0.3 ng/L EPA 533HFPO-DA 05/02/25 16:36 MAB3U1.910.3 < 0.4 ng/L EPA 533NFDHA05/02/25 16:36 MAB3U1.910.4 < 0.3 ng/L EPA 5334:2 FTS 05/02/25 16:36 MAB3U1.910.3 < 0.4 ng/L EPA 533PFHxS05/02/25 16:36 MAB3U1.910.4 < 0.5 ng/L EPA 533PFHpA05/02/25 16:36 MAB3U1.910.5 < 1.0 ng/L EPA 533PFHxA05/02/25 16:36 MAB3U1.911.0 < 0.5 ng/L EPA 533ADONA05/02/25 16:36 MAB3U1.910.5 < 0.5 ng/L EPA 533PFPeS05/02/25 16:36 MAB3U1.910.5 < 0.5 ng/L EPA 5336:2 FTS 05/02/25 16:36 MAB3U1.910.5 < 0.7 ng/L EPA 533PFOA05/02/25 16:36 MAB3U1.910.7 < 0.6 ng/L EPA 533PFHpS05/02/25 16:36 MAB3U1.910.6 < 0.5 ng/L EPA 533PFOS05/02/25 16:36 MAB3U1.910.5 < 0.5 ng/L EPA 533PFNA05/02/25 16:36 MAB3U1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 05/02/25 16:36 MAB3U1.910.6 < 0.5 ng/L EPA 5338:2 FTS 05/02/25 16:36 MAB3U1.910.5 < 0.4 ng/L EPA 533PFDA05/02/25 16:36 MAB3U1.910.4 < 0.4 ng/L EPA 533PFUnA05/02/25 16:36 MAB3U1.910.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 05/02/25 16:36 MAB3U1.910.5 < 0.5 ng/L EPA 533PFDoA05/02/25 16:36 MAB3U1.910.5 Surrogate: 13C4-PFBA-SURR 92 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 86 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 93 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 76 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 91 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 112 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 95 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 94 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 77 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 90 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 98 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 92 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 79 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 95 %50-200 05/02/25 16:36 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 92 %50-200 05/02/25 16:36 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID05362-01 Name: Sampled: Received: 04/30/25 09:10 04/24/25 08:40 WS003-COTTONWOOD WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH25137 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 91 %50-200 05/02/25 16:36 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID05362-03 Name: Sampled: Received: 04/30/25 09:10 04/24/25 08:21 WS002-HARVEY WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH25137 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA05/02/25 17:24 MAB3U1.910.9 < 0.4 ng/L EPA 533PFMPA05/02/25 17:24 MAB3U1.910.4 < 0.5 ng/L EPA 533PFPeA05/02/25 17:24 MAB3U1.910.5 < 0.5 ng/L EPA 533PFBS05/02/25 17:24 MAB3U1.910.5 < 0.4 ng/L EPA 533PFMBA05/02/25 17:24 MAB3U1.910.4 < 0.5 ng/L EPA 533PFEESA05/02/25 17:24 MAB3U1.910.5 < 0.3 ng/L EPA 533HFPO-DA 05/02/25 17:24 MAB3U1.910.3 < 0.4 ng/L EPA 533NFDHA05/02/25 17:24 MAB3U1.910.4 < 0.3 ng/L EPA 5334:2 FTS 05/02/25 17:24 MAB3U1.910.3 < 0.4 ng/L EPA 533PFHxS05/02/25 17:24 MAB3U1.910.4 < 0.5 ng/L EPA 533PFHpA05/02/25 17:24 MAB3U1.910.5 < 1.0 ng/L EPA 533PFHxA05/02/25 17:24 MAB3U1.911.0 < 0.5 ng/L EPA 533ADONA05/02/25 17:24 MAB3U1.910.5 < 0.5 ng/L EPA 533PFPeS05/02/25 17:24 MAB3U1.910.5 < 0.5 ng/L EPA 5336:2 FTS 05/02/25 17:24 MAB3U1.910.5 < 0.7 ng/L EPA 533PFOA05/02/25 17:24 MAB3U1.910.7 < 0.6 ng/L EPA 533PFHpS05/02/25 17:24 MAB3U1.910.6 < 0.5 ng/L EPA 533PFOS05/02/25 17:24 MAB3U1.910.5 < 0.5 ng/L EPA 533PFNA05/02/25 17:24 MAB3U1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 05/02/25 17:24 MAB3U1.910.6 < 0.5 ng/L EPA 5338:2 FTS 05/02/25 17:24 MAB3U1.910.5 < 0.4 ng/L EPA 533PFDA05/02/25 17:24 MAB3U1.910.4 < 0.4 ng/L EPA 533PFUnA05/02/25 17:24 MAB3U1.910.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 05/02/25 17:24 MAB3U1.910.5 < 0.5 ng/L EPA 533PFDoA05/02/25 17:24 MAB3U1.910.5 Surrogate: 13C4-PFBA-SURR 90 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 85 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 93 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 76 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 89 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 109 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 93 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 94 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 78 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 88 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 97 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 93 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 80 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 92 %50-200 05/02/25 17:24 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 90 %50-200 05/02/25 17:24 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 6 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID05362-03 Name: Sampled: Received: 04/30/25 09:10 04/24/25 08:21 WS002-HARVEY WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH25137 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 90 %50-200 05/02/25 17:24 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 7 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B531576 - EPA 533 - EPA 533 Blank (B531576-BLK1)Prepared: 05/01/25 Analyzed: 05/02/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 1.0 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.6 ng/L U Surrogate: 13C4-PFBA-SURR 9.37 ug/L 10.00 94 50-200 Surrogate: 13C5-PFPeA-SURR 8.76 ug/L 10.00 88 50-200 Surrogate: 13C3-PFBS-SURR 9.16 ug/L 9.320 98 50-200 Surrogate: 13C2-4:2FTS-SURR 30.2 ug/L 37.60 80 50-200 Surrogate: 13C5-PFHxA-SURR 9.45 ug/L 10.00 94 50-200 Surrogate: 13C3-HFPOA-DA-SURR 11.3 ug/L 10.00 113 50-200 Surrogate: 13C4-PFHpA-SURR 9.77 ug/L 10.00 98 50-200 Surrogate: 13C3-PFHxS-SURR 9.61 ug/L 9.480 101 50-200 Surrogate: 13C2-6:2FTS-SURR 31.0 ug/L 38.00 82 50-200 Surrogate: 13C8-PFOA-SURR 9.24 ug/L 10.00 92 50-200 Surrogate: 13C9-PFNA-SURR 10.3 ug/L 10.00 103 50-200 Surrogate: 13C8-PFOS-SURR 9.61 ug/L 9.580 100 50-200 Surrogate: 13C2-8:2FTS-SURR 32.4 ug/L 38.40 84 50-200 Surrogate: 13C6-PFDA-SURR 9.82 ug/L 10.00 98 50-200 Surrogate: 13C7-PFUnA-SURR 9.71 ug/L 10.00 97 50-200 Surrogate: 13C2-PFDoA-SURR 9.81 ug/L 10.00 98 50-200 LCS (B531576-BS1)Prepared: 05/01/25 Analyzed: 05/02/25 PFBA 197 ng/L 200.0 98 70-130 PFMPA 214 ng/L 200.0 107 70-130 www.pacelabs.comCustomer #: 72-106174 Page 8 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B531576-BS1)Prepared: 05/01/25 Analyzed: 05/02/25 PFPeA 187 ng/L 200.0 93 70-130 PFBS 174 ng/L 200.0 87 70-130 PFMBA 169 ng/L 200.0 85 70-130 PFEESA 169 ng/L 200.0 85 70-130 HFPO-DA 171 ng/L 200.0 85 70-130 NFDHA 180 ng/L 200.0 90 70-130 PFHxS 181 ng/L 200.0 91 70-130 4:2 FTS 204 ng/L 200.0 102 70-130 PFHpA 172 ng/L 200.0 86 70-130 PFHxA 180 ng/L 200.0 90 70-130 ADONA 178 ng/L 200.0 89 70-130 PFPeS 186 ng/L 200.0 93 70-130 6:2 FTS 189 ng/L 200.0 95 70-130 PFOA 210 ng/L 200.0 105 70-130 PFHpS 185 ng/L 200.0 92 70-130 PFOS 169 ng/L 200.0 85 70-130 PFNA 191 ng/L 200.0 96 70-130 9Cl-PF3ONS 174 ng/L 200.0 87 70-130 8:2 FTS 201 ng/L 200.0 101 70-130 PFDA 170 ng/L 200.0 85 70-130 PFUnA 168 ng/L 200.0 84 70-130 11Cl-PF3OUdS 184 ng/L 200.0 92 70-130 PFDoA 168 ng/L 200.0 84 70-130 Surrogate: 13C4-PFBA-SURR 8.38 ug/L 10.00 84 50-200 Surrogate: 13C5-PFPeA-SURR 8.08 ug/L 10.00 81 50-200 Surrogate: 13C3-PFBS-SURR 8.68 ug/L 9.320 93 50-200 Surrogate: 13C2-4:2FTS-SURR 31.8 ug/L 37.60 85 50-200 Surrogate: 13C5-PFHxA-SURR 8.39 ug/L 10.00 84 50-200 Surrogate: 13C3-HFPOA-DA-SURR 10.0 ug/L 10.00 100 50-200 Surrogate: 13C4-PFHpA-SURR 8.73 ug/L 10.00 87 50-200 Surrogate: 13C3-PFHxS-SURR 9.02 ug/L 9.480 95 50-200 Surrogate: 13C2-6:2FTS-SURR 33.2 ug/L 38.00 87 50-200 Surrogate: 13C8-PFOA-SURR 8.30 ug/L 10.00 83 50-200 Surrogate: 13C9-PFNA-SURR 8.61 ug/L 10.00 86 50-200 Surrogate: 13C8-PFOS-SURR 8.61 ug/L 9.580 90 50-200 Surrogate: 13C2-8:2FTS-SURR 33.7 ug/L 38.40 88 50-200 Surrogate: 13C6-PFDA-SURR 7.26 ug/L 10.00 73 50-200 Surrogate: 13C7-PFUnA-SURR 7.15 ug/L 10.00 71 50-200 Surrogate: 13C2-PFDoA-SURR 7.92 ug/L 10.00 79 50-200 Duplicate (B531576-DUP1)Sample: ID04723-01 Prepared: 05/01/25 Analyzed: 05/02/25 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 9 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B531576-DUP1)Sample: ID04723-01 Prepared: 05/01/25 Analyzed: 05/02/25 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 1.0 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.6 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 9.60 ug/L 10.00 96 50-200 Surrogate: 13C5-PFPeA-SURR 10.9 ug/L 10.00 109 50-200 Surrogate: 13C3-PFBS-SURR 9.05 ug/L 9.320 97 50-200 Surrogate: 13C2-4:2FTS-SURR 29.6 ug/L 37.60 79 50-200 Surrogate: 13C5-PFHxA-SURR 9.45 ug/L 10.00 95 50-200 Surrogate: 13C3-HFPOA-DA-SURR 11.3 ug/L 10.00 113 50-200 Surrogate: 13C4-PFHpA-SURR 9.77 ug/L 10.00 98 50-200 Surrogate: 13C3-PFHxS-SURR 9.15 ug/L 9.480 97 50-200 Surrogate: 13C2-6:2FTS-SURR 30.8 ug/L 38.00 81 50-200 Surrogate: 13C8-PFOA-SURR 9.12 ug/L 10.00 91 50-200 Surrogate: 13C9-PFNA-SURR 9.86 ug/L 10.00 99 50-200 Surrogate: 13C8-PFOS-SURR 9.47 ug/L 9.580 99 50-200 Surrogate: 13C2-8:2FTS-SURR 31.9 ug/L 38.40 83 50-200 Surrogate: 13C6-PFDA-SURR 9.30 ug/L 10.00 93 50-200 Surrogate: 13C7-PFUnA-SURR 8.98 ug/L 10.00 90 50-200 Surrogate: 13C2-PFDoA-SURR 8.85 ug/L 10.00 88 50-200 Matrix Spike (B531576-MS1)Sample: ID05236-01 Prepared: 05/01/25 Analyzed: 05/02/25 PFBA 199 ng/L 193.9 14 95 70-130 PFMPA 274 ng/L 193.9 ND 141 70-130 PFPeA 173 ng/L 193.9 4 87 70-130 PFBS 168 ng/L 193.9 4 85 70-130 PFMBA 154 ng/L 193.9 ND 80 70-130 PFEESA 158 ng/L 193.9 ND 81 70-130 NFDHA 165 ng/L 193.9 ND 85 70-130 HFPO-DA 156 ng/L 193.9 ND 80 70-130 PFHxS 168 ng/L 193.9 6 84 70-130 4:2 FTS 186 ng/L 193.9 ND 96 70-130 PFHpA 160 ng/L 193.9 1 82 70-130 PFHxA 169 ng/L 193.9 2 86 70-130 www.pacelabs.comCustomer #: 72-106174 Page 10 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B531576-MS1)Sample: ID05236-01 Prepared: 05/01/25 Analyzed: 05/02/25 ADONA 163 ng/L 193.9 ND 84 70-130 PFPeS 172 ng/L 193.9 0.9 88 70-130 6:2 FTS 175 ng/L 193.9 ND 90 70-130 PFOA 200 ng/L 193.9 8 99 70-130 PFHpS 167 ng/L 193.9 ND 86 70-130 PFOS 155 ng/L 193.9 4 78 70-130 PFNA 176 ng/L 193.9 0.5 90 70-130 9Cl-PF3ONS 158 ng/L 193.9 ND 81 70-130 8:2 FTS 189 ng/L 193.9 ND 97 70-130 PFDA 154 ng/L 193.9 ND 79 70-130 PFUnA 152 ng/L 193.9 ND 78 70-130 11Cl-PF3OUdS 166 ng/L 193.9 ND 86 70-130 PFDoA 153 ng/L 193.9 ND 79 70-130 Surrogate: 13C4-PFBA-SURR 9.84 ug/L 10.00 98 50-200 Surrogate: 13C5-PFPeA-SURR 15.3 ug/L 10.00 153 50-200 Surrogate: 13C3-PFBS-SURR 9.78 ug/L 9.320 105 50-200 Surrogate: 13C2-4:2FTS-SURR 39.7 ug/L 37.60 106 50-200 Surrogate: 13C5-PFHxA-SURR 9.58 ug/L 10.00 96 50-200 Surrogate: 13C3-HFPOA-DA-SURR 11.8 ug/L 10.00 118 50-200 Surrogate: 13C4-PFHpA-SURR 9.74 ug/L 10.00 97 50-200 Surrogate: 13C3-PFHxS-SURR 10.3 ug/L 9.480 108 50-200 Surrogate: 13C2-6:2FTS-SURR 38.0 ug/L 38.00 100 50-200 Surrogate: 13C8-PFOA-SURR 9.04 ug/L 10.00 90 50-200 Surrogate: 13C9-PFNA-SURR 9.39 ug/L 10.00 94 50-200 Surrogate: 13C8-PFOS-SURR 9.62 ug/L 9.580 100 50-200 Surrogate: 13C2-8:2FTS-SURR 37.1 ug/L 38.40 97 50-200 Surrogate: 13C6-PFDA-SURR 9.01 ug/L 10.00 90 50-200 Surrogate: 13C7-PFUnA-SURR 8.99 ug/L 10.00 90 50-200 Surrogate: 13C2-PFDoA-SURR 8.89 ug/L 10.00 89 50-200 www.pacelabs.comCustomer #: 72-106174 Page 11 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 12 of 15 Page 13 of 15 Page 14 of 15 Page 15 of 15