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HomeMy WebLinkAboutDDW-2025-004266April 22, 2025 Dear John Steffan: Please find enclosed the analytical results for the 6 sample(s) the laboratory received on 4/16/25 9:30 am and logged in under work order ID03027. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH17005RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID03027-01 Name: Sampled: Received: 04/16/25 09:30 04/15/25 07:04 WS001-RANDOLPH SPRING Reg ID:Drinking Water - Regular SampleMatrix:UTAH17005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA04/18/25 21:52 MAB3U1.810.9 < 0.4 ng/L EPA 533PFMPA04/18/25 21:52 MAB3U1.810.4 < 0.5 ng/L EPA 533PFPeA04/18/25 21:52 MAB3U1.810.5 < 0.5 ng/L EPA 533PFBS04/18/25 21:52 MAB3U1.810.5 < 0.4 ng/L EPA 533PFMBA04/18/25 21:52 MAB3U1.810.4 < 0.5 ng/L EPA 533PFEESA04/18/25 21:52 MAB3U1.810.5 < 0.3 ng/L EPA 533HFPO-DA 04/18/25 21:52 MAB3U1.810.3 < 0.4 ng/L EPA 533NFDHA04/18/25 21:52 MAB3U1.810.4 < 0.3 ng/L EPA 5334:2 FTS 04/18/25 21:52 MAB3U1.810.3 < 0.4 ng/L EPA 533PFHxS04/18/25 21:52 MAB3U1.810.4 < 0.5 ng/L EPA 533PFHpA04/18/25 21:52 MAB3U1.810.5 < 0.4 ng/L EPA 533PFHxA04/18/25 21:52 MAB3U1.810.4 < 0.5 ng/L EPA 533ADONA04/18/25 21:52 MAB3U1.810.5 < 0.5 ng/L EPA 533PFPeS04/18/25 21:52 MAB3U1.810.5 < 0.5 ng/L EPA 5336:2 FTS 04/18/25 21:52 MAB3U1.810.5 < 0.7 ng/L EPA 533PFOA04/18/25 21:52 MAB3U1.810.7 < 0.5 ng/L EPA 533PFHpS04/18/25 21:52 MAB3U1.810.5 < 0.5 ng/L EPA 533PFOS04/18/25 21:52 MAB3U1.810.5 < 0.5 ng/L EPA 533PFNA04/18/25 21:52 MAB3U1.810.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 04/18/25 21:52 MAB3U1.810.6 < 0.5 ng/L EPA 5338:2 FTS 04/18/25 21:52 MAB3U1.810.5 < 0.4 ng/L EPA 533PFDA04/18/25 21:52 MAB3U1.810.4 < 0.4 ng/L EPA 533PFUnA04/18/25 21:52 MAB3U1.810.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 04/18/25 21:52 MAB3U1.810.5 < 0.5 ng/L EPA 533PFDoA04/18/25 21:52 MAB3U1.810.5 Surrogate: 13C4-PFBA-SURR 96 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 96 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 101 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 92 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 95 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 104 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 96 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 97 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 90 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 90 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 92 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 96 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 96 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 93 %50-200 04/18/25 21:52 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 88 %50-200 04/18/25 21:52 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID03027-01 Name: Sampled: Received: 04/16/25 09:30 04/15/25 07:04 WS001-RANDOLPH SPRING Reg ID:Drinking Water - Regular SampleMatrix:UTAH17005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 91 %50-200 04/18/25 21:52 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID03027-03 Name: Sampled: Received: 04/16/25 09:30 04/15/25 07:47 WS002-FIELD ST 1ST WEST WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH17005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 1.0 ng/L EPA 533PFBA04/18/25 22:15 MAB3U2.011.0 < 0.4 ng/L EPA 533PFMPA04/18/25 22:15 MAB3U2.010.4 < 0.5 ng/L EPA 533PFPeA04/18/25 22:15 MAB3U2.010.5 < 0.5 ng/L EPA 533PFBS04/18/25 22:15 MAB3U2.010.5 < 0.4 ng/L EPA 533PFMBA04/18/25 22:15 MAB3U2.010.4 < 0.5 ng/L EPA 533PFEESA04/18/25 22:15 MAB3U2.010.5 < 0.4 ng/L EPA 533HFPO-DA 04/18/25 22:15 MAB3U2.010.4 < 0.5 ng/L EPA 533NFDHA04/18/25 22:15 MAB3U2.010.5 < 0.4 ng/L EPA 5334:2 FTS 04/18/25 22:15 MAB3U2.010.4 < 0.4 ng/L EPA 533PFHxS04/18/25 22:15 MAB3U2.010.4 < 0.6 ng/L EPA 533PFHpA04/18/25 22:15 MAB3U2.010.6 < 0.5 ng/L EPA 533PFHxA04/18/25 22:15 MAB3U2.010.5 < 0.5 ng/L EPA 533ADONA04/18/25 22:15 MAB3U2.010.5 < 0.6 ng/L EPA 533PFPeS04/18/25 22:15 MAB3U2.010.6 < 0.5 ng/L EPA 5336:2 FTS 04/18/25 22:15 MAB3U2.010.5 < 0.7 ng/L EPA 533PFOA04/18/25 22:15 MAB3U2.010.7 < 0.6 ng/L EPA 533PFHpS04/18/25 22:15 MAB3U2.010.6 < 0.5 ng/L EPA 533PFOS04/18/25 22:15 MAB3U2.010.5 < 0.5 ng/L EPA 533PFNA04/18/25 22:15 MAB3U2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 04/18/25 22:15 MAB3U2.010.7 < 0.5 ng/L EPA 5338:2 FTS 04/18/25 22:15 MAB3U2.010.5 < 0.5 ng/L EPA 533PFDA04/18/25 22:15 MAB3U2.010.5 < 0.5 ng/L EPA 533PFUnA04/18/25 22:15 MAB3U2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 04/18/25 22:15 MAB3U2.010.6 < 0.5 ng/L EPA 533PFDoA04/18/25 22:15 MAB3U2.010.5 Surrogate: 13C4-PFBA-SURR 94 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 91 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 100 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 91 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 96 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 101 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 96 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 96 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 89 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 92 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 94 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 93 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 97 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 86 %50-200 04/18/25 22:15 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 78 %50-200 04/18/25 22:15 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 6 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID03027-03 Name: Sampled: Received: 04/16/25 09:30 04/15/25 07:47 WS002-FIELD ST 1ST WEST WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH17005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 87 %50-200 04/18/25 22:15 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 7 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID03027-05 Name: Sampled: Received: 04/16/25 09:30 04/15/25 08:03 WS003-PARK WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH17005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA04/18/25 22:39 MAB3U1.910.9 < 0.4 ng/L EPA 533PFMPA04/18/25 22:39 MAB3U1.910.4 < 0.5 ng/L EPA 533PFPeA04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 533PFBS04/18/25 22:39 MAB3U1.910.5 < 0.4 ng/L EPA 533PFMBA04/18/25 22:39 MAB3U1.910.4 < 0.5 ng/L EPA 533PFEESA04/18/25 22:39 MAB3U1.910.5 < 0.3 ng/L EPA 533HFPO-DA 04/18/25 22:39 MAB3U1.910.3 < 0.4 ng/L EPA 533NFDHA04/18/25 22:39 MAB3U1.910.4 < 0.4 ng/L EPA 5334:2 FTS 04/18/25 22:39 MAB3U1.910.4 < 0.4 ng/L EPA 533PFHxS04/18/25 22:39 MAB3U1.910.4 < 0.5 ng/L EPA 533PFHpA04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 533PFHxA04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 533ADONA04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 533PFPeS04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 5336:2 FTS 04/18/25 22:39 MAB3U1.910.5 < 0.7 ng/L EPA 533PFOA04/18/25 22:39 MAB3U1.910.7 < 0.6 ng/L EPA 533PFHpS04/18/25 22:39 MAB3U1.910.6 0.8 ng/L EPA 533PFOS04/18/25 22:39 MAB3J1.910.5 < 0.5 ng/L EPA 533PFNA04/18/25 22:39 MAB3U1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 04/18/25 22:39 MAB3U1.910.6 < 0.5 ng/L EPA 5338:2 FTS 04/18/25 22:39 MAB3U1.910.5 < 0.4 ng/L EPA 533PFDA04/18/25 22:39 MAB3U1.910.4 < 0.5 ng/L EPA 533PFUnA04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 53311Cl-PF3OUdS 04/18/25 22:39 MAB3U1.910.5 < 0.5 ng/L EPA 533PFDoA04/18/25 22:39 MAB3U1.910.5 Surrogate: 13C4-PFBA-SURR 95 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 93 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 99 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 91 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 97 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 103 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 97 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 95 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 88 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 91 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 88 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 96 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 96 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 78 %50-200 04/18/25 22:39 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 75 %50-200 04/18/25 22:39 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 8 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: ID03027-05 Name: Sampled: Received: 04/16/25 09:30 04/15/25 08:03 WS003-PARK WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH17005 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 84 %50-200 04/18/25 22:39 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 9 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B530363 - EPA 533 - EPA 533 Blank (B530363-BLK1)Prepared: 04/17/25 Analyzed: 04/18/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 0.5 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.5 ng/L U Surrogate: 13C4-PFBA-SURR 22.3 ng/L 40.00 56 50-200 Surrogate: 13C5-PFPeA-SURR 23.3 ng/L 40.00 58 50-200 Surrogate: 13C3-PFBS-SURR 40.7 ng/L 37.28 109 50-200 Surrogate: 13C2-4:2FTS-SURR 150 ng/L 150.4 100 50-200 Surrogate: 13C5-PFHxA-SURR 27.1 ng/L 40.00 68 50-200 Surrogate: 13C3-HFPOA-DA-SURR 25.6 ng/L 40.00 64 50-200 Surrogate: 13C4-PFHpA-SURR 30.2 ng/L 40.00 76 50-200 Surrogate: 13C3-PFHxS-SURR 40.4 ng/L 37.92 107 50-200 Surrogate: 13C2-6:2FTS-SURR 149 ng/L 152.0 98 50-200 Surrogate: 13C8-PFOA-SURR 32.2 ng/L 40.00 80 50-200 Surrogate: 13C9-PFNA-SURR 34.1 ng/L 40.00 85 50-200 Surrogate: 13C8-PFOS-SURR 40.7 ng/L 38.32 106 50-200 Surrogate: 13C2-8:2FTS-SURR 167 ng/L 153.6 109 50-200 Surrogate: 13C6-PFDA-SURR 32.7 ng/L 40.00 82 50-200 Surrogate: 13C7-PFUnA-SURR 31.9 ng/L 40.00 80 50-200 Surrogate: 13C2-PFDoA-SURR 36.0 ng/L 40.00 90 50-200 LCS (B530363-BS1)Prepared: 04/17/25 Analyzed: 04/18/25 PFBA 68 ng/L 80.00 85 70-130 PFMPA 67 ng/L 80.00 84 70-130 www.pacelabs.comCustomer #: 72-106174 Page 10 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B530363-BS1)Prepared: 04/17/25 Analyzed: 04/18/25 PFPeA 65 ng/L 80.00 81 70-130 PFBS 60 ng/L 80.00 75 70-130 PFMBA 58 ng/L 80.00 73 70-130 PFEESA 60 ng/L 80.00 74 70-130 HFPO-DA 59 ng/L 80.00 74 70-130 NFDHA 59 ng/L 80.00 74 70-130 PFHxS 61 ng/L 80.00 77 70-130 4:2 FTS 74 ng/L 80.00 92 70-130 PFHpA 58 ng/L 80.00 73 70-130 PFHxA 63 ng/L 80.00 78 70-130 ADONA 60 ng/L 80.00 75 70-130 PFPeS 66 ng/L 80.00 82 70-130 6:2 FTS 69 ng/L 80.00 86 70-130 PFOA 73 ng/L 80.00 91 70-130 PFHpS 64 ng/L 80.00 80 70-130 PFOS 56 ng/L 79.52 70 70-130 PFNA 68 ng/L 80.00 85 70-130 9Cl-PF3ONS 62 ng/L 80.00 77 70-130 8:2 FTS 74 ng/L 80.00 93 70-130 PFDA 59 ng/L 80.00 73 70-130 PFUnA 63 ng/L 80.00 79 70-130 11Cl-PF3OUdS 59 ng/L 80.00 74 70-130 PFDoA 60 ng/L 80.00 75 70-130 Surrogate: 13C4-PFBA-SURR 32.1 ng/L 40.00 80 50-200 Surrogate: 13C5-PFPeA-SURR 32.3 ng/L 40.00 81 50-200 Surrogate: 13C3-PFBS-SURR 37.3 ng/L 37.28 100 50-200 Surrogate: 13C2-4:2FTS-SURR 145 ng/L 150.4 96 50-200 Surrogate: 13C5-PFHxA-SURR 33.0 ng/L 40.00 82 50-200 Surrogate: 13C3-HFPOA-DA-SURR 35.1 ng/L 40.00 88 50-200 Surrogate: 13C4-PFHpA-SURR 34.3 ng/L 40.00 86 50-200 Surrogate: 13C3-PFHxS-SURR 37.4 ng/L 37.92 99 50-200 Surrogate: 13C2-6:2FTS-SURR 143 ng/L 152.0 94 50-200 Surrogate: 13C8-PFOA-SURR 34.2 ng/L 40.00 85 50-200 Surrogate: 13C9-PFNA-SURR 35.4 ng/L 40.00 88 50-200 Surrogate: 13C8-PFOS-SURR 37.2 ng/L 38.32 97 50-200 Surrogate: 13C2-8:2FTS-SURR 148 ng/L 153.6 97 50-200 Surrogate: 13C6-PFDA-SURR 34.1 ng/L 40.00 85 50-200 Surrogate: 13C7-PFUnA-SURR 32.1 ng/L 40.00 80 50-200 Surrogate: 13C2-PFDoA-SURR 32.1 ng/L 40.00 80 50-200 Duplicate (B530363-DUP1)Sample: ID03023-01 Prepared: 04/17/25 Analyzed: 04/18/25 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 11 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B530363-DUP1)Sample: ID03023-01 Prepared: 04/17/25 Analyzed: 04/18/25 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 0.5 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 36.8 ng/L 39.62 93 50-200 Surrogate: 13C5-PFPeA-SURR 40.0 ng/L 39.62 101 50-200 Surrogate: 13C3-PFBS-SURR 35.7 ng/L 36.93 97 50-200 Surrogate: 13C2-4:2FTS-SURR 132 ng/L 149.0 89 50-200 Surrogate: 13C5-PFHxA-SURR 37.9 ng/L 39.62 96 50-200 Surrogate: 13C3-HFPOA-DA-SURR 40.8 ng/L 39.62 103 50-200 Surrogate: 13C4-PFHpA-SURR 37.9 ng/L 39.62 96 50-200 Surrogate: 13C3-PFHxS-SURR 37.0 ng/L 37.56 99 50-200 Surrogate: 13C2-6:2FTS-SURR 134 ng/L 150.6 89 50-200 Surrogate: 13C8-PFOA-SURR 36.0 ng/L 39.62 91 50-200 Surrogate: 13C9-PFNA-SURR 36.2 ng/L 39.62 91 50-200 Surrogate: 13C8-PFOS-SURR 36.3 ng/L 37.96 96 50-200 Surrogate: 13C2-8:2FTS-SURR 150 ng/L 152.1 98 50-200 Surrogate: 13C6-PFDA-SURR 31.1 ng/L 39.62 78 50-200 Surrogate: 13C7-PFUnA-SURR 28.0 ng/L 39.62 71 50-200 Surrogate: 13C2-PFDoA-SURR 30.8 ng/L 39.62 78 50-200 Matrix Spike (B530363-MS1)Sample: ID03025-01 Prepared: 04/17/25 Analyzed: 04/18/25 PFBA 76 ng/L 80.94 ND 94 70-130 PFMPA 83 ng/L 80.94 ND 102 70-130 PFPeA 71 ng/L 80.94 ND 88 70-130 PFBS 67 ng/L 80.94 ND 83 70-130 PFMBA 66 ng/L 80.94 ND 82 70-130 PFEESA 66 ng/L 80.94 ND 82 70-130 NFDHA 69 ng/L 80.94 ND 86 70-130 HFPO-DA 66 ng/L 80.94 ND 82 70-130 PFHxS 68 ng/L 80.94 ND 84 70-130 4:2 FTS 81 ng/L 80.94 ND 100 70-130 PFHpA 66 ng/L 80.94 ND 81 70-130 PFHxA 72 ng/L 80.94 ND 88 70-130 www.pacelabs.comCustomer #: 72-106174 Page 12 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B530363-MS1)Sample: ID03025-01 Prepared: 04/17/25 Analyzed: 04/18/25 ADONA 69 ng/L 80.94 ND 85 70-130 PFPeS 73 ng/L 80.94 ND 90 70-130 6:2 FTS 76 ng/L 80.94 ND 94 70-130 PFOA 82 ng/L 80.94 ND 101 70-130 PFHpS 75 ng/L 80.94 ND 93 70-130 PFOS 64 ng/L 80.45 ND 79 70-130 PFNA 76 ng/L 80.94 ND 93 70-130 9Cl-PF3ONS 72 ng/L 80.94 ND 89 70-130 8:2 FTS 83 ng/L 80.94 ND 103 70-130 PFDA 65 ng/L 80.94 ND 81 70-130 PFUnA 70 ng/L 80.94 ND 87 70-130 11Cl-PF3OUdS 69 ng/L 80.94 ND 85 70-130 PFDoA 66 ng/L 80.94 ND 82 70-130 Surrogate: 13C4-PFBA-SURR 38.6 ng/L 40.47 95 50-200 Surrogate: 13C5-PFPeA-SURR 41.6 ng/L 40.47 103 50-200 Surrogate: 13C3-PFBS-SURR 38.1 ng/L 37.72 101 50-200 Surrogate: 13C2-4:2FTS-SURR 151 ng/L 152.2 99 50-200 Surrogate: 13C5-PFHxA-SURR 39.2 ng/L 40.47 97 50-200 Surrogate: 13C3-HFPOA-DA-SURR 42.5 ng/L 40.47 105 50-200 Surrogate: 13C4-PFHpA-SURR 39.2 ng/L 40.47 97 50-200 Surrogate: 13C3-PFHxS-SURR 38.4 ng/L 38.37 100 50-200 Surrogate: 13C2-6:2FTS-SURR 149 ng/L 153.8 97 50-200 Surrogate: 13C8-PFOA-SURR 37.4 ng/L 40.47 92 50-200 Surrogate: 13C9-PFNA-SURR 38.0 ng/L 40.47 94 50-200 Surrogate: 13C8-PFOS-SURR 37.0 ng/L 38.77 96 50-200 Surrogate: 13C2-8:2FTS-SURR 148 ng/L 155.4 95 50-200 Surrogate: 13C6-PFDA-SURR 32.4 ng/L 40.47 80 50-200 Surrogate: 13C7-PFUnA-SURR 29.5 ng/L 40.47 73 50-200 Surrogate: 13C2-PFDoA-SURR 31.6 ng/L 40.47 78 50-200 www.pacelabs.comCustomer #: 72-106174 Page 13 of 17 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 14 of 17 Page 15 of 17 Page 16 of 17 Page 17 of 17