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DAQ-2025-002076
1 DAQC-373-25 Site ID: 15938 (B4) MEMORANDUM TO: STACK TEST FILE – UINTA WAX OPERATING, LLC – North Randlett Compressor Station – Uintah County THROUGH: Rik Ombach, Minor Source Oil & Gas Section Manager FROM: Kyle Greenberg, Environmental Scientist DATE: April 14, 2025 SUBJECT: Sources: Compressor Engines: Unit #1 Caterpillar G3516B, SN: N6W/4EK00075; Unit #2 Caterpillar G3516B, SN: JEF01814; Unit #4 Caterpillar G3516B, SN: JEF01637; Unit #5 Caterpillar G3516B, SN: N6W/JEF01780 Contact: Karen Pratt: 720-990-9927 Location: Remote location in Uintah County, UT Test Contractor: Oasis Emissions Consultants, Inc. Permit/AO#: DAQE-AN159380002-23 dated December 11, 2023 Action Code: TR Subject: Review of Stack Test Reports dated July 2, 2024 On July 2, 2024, Utah Division of Air Quality (DAQ) received a test report for the above listed units. Testing was performed on June 19-20, 2024, to demonstrate compliance with the emission limits found in Condition II.B.2 of Approval Order DAQE-AN159380002-23 and 40 CFR Part 60 Subpart JJJJ. The DAQ calculated test results are: Source Test Date Test Method Pollutant Tester Results DAQ Results Limits Unit ID: #1 SN: N6W/4EK 00075 June 19, 2024 320 NOx 0.37 g/bhp-hr 0.66 lb/hr 39.33 ppmvd @15% O2 0.367 g/bhp-hr 0.654 lb/hr 39.326 ppmvd @15% O2 1.0 g/bhp-hr 1.52 lb/hr 41 ppmvd @15% O2 320 CO 0.03 g/bhp-hr 0.06 lb/hr 5.97 ppmvd @15% O2 0.034 g/bhp-hr 0.060 lb/hr 5.966 ppmvd @15% O2 2.0 g/bhp-hr 1.37 lb/hr 61 ppmvd @15% O2 320 VOC 0.32 g/bhp-hr 0.57 lb/hr 35.38 ppmvd @15% O2 0.316 g/bhp-hr 0.565 lb/hr 35.380 ppmvd @15% O2 0.7 g/bhp-hr 2.13 lb/hr 60 ppmvd @15% O2 Unit ID: #2 SN: JEF01814 June 19, 2024 320 NOx 0.47 g/bhp-hr 0.99 lb/hr 32.84 ppmvd @15% O2 0.466 g/bhp-hr 0.992 lb/hr 32.840 ppmvd @15% O2 1.0 g/bhp-hr 1.52 lb/hr 41 ppmvd @15% O2 320 CO 0.01 g/bhp-hr 0.03 lb/hr 1.50 ppmvd @15% O2 0.013 g/bhp-hr 0.028 lb/hr 1.497 ppmvd @15% O2 2.0 g/bhp-hr 1.37 lb/hr 61 ppmvd @15% O2 4 ' - ) - " 2 Source Test Date Test Method Pollutant Tester Results DAQ Results Limits Unit ID: #1 SN: N6W/4EK 00075 June 19, 2024 320 VOC 0.39 g/bhp-hr 0.83 lb/hr 28.56 ppmvd @15% O2 0.388 g/bhp-hr 0.827 lb/hr 28.556 ppmvd @15% O2 0.7 g/bhp-hr 2.13 lb/hr 60 ppmvd @15% O2 Unit ID: #4 SN: JEF01637 June 19, 2024 320 NOx 0.46 g/bhp-hr 0.99 lb/hr 28.81 ppmvd @15% O2 0.456 g/bhp-hr 0.985 lb/hr 28.809 ppmvd @15% O2 1.0 g/bhp-hr 1.52 lb/hr 41 ppmvd @15% O2 320 CO 0.08 g/bhp-hr 0.16 lb/hr 7.81 ppmvd @15% O2 0.075 g/bhp-hr 0.163 lb/hr 7.811 ppmvd @15% O2 2.0 g/bhp-hr 1.37 lb/hr 61 ppmvd @15% O2 320 VOC 0.36 g/bhp-hr 0.77 lb/hr 23.45 ppmvd @15% O2 0.356 g/bhp-hr 0.768 lb/hr 23.449 ppmvd @15% O2 0.7 g/bhp-hr 2.13 lb/hr 60 ppmvd @15% O2 Unit ID: #5 SN: N6W/JEF0 1780 June 20, 2024 320 NOx 0.37 g/bhp-hr 0.98 lb/hr 35.97 ppmvd @15% O2 0.371 g/bhp-hr 0.981 lb/hr 35.970 ppmvd @15% O2 1.0 g/bhp-hr 1.52 lb/hr 41 ppmvd @15% O2 320 CO 0.08 g/bhp-hr 0.22 lb/hr 13.29 ppmvd @15% O2 0.083 g/bhp-hr 0.221 lb/hr 13.288 ppmvd @15% O2 2.0 g/bhp-hr 1.37 lb/hr 61 ppmvd @15% O2 320 VOC 0.28 g/bhp-hr 0.73 lb/hr 28.07 ppmvd @15% O2 0.277 g/bhp-hr 0.733 lb/hr 28.073 ppmvd @15% O2 0.7 g/bhp-hr 2.13 lb/hr 60 ppmvd @15% O2 DEVIATIONS: None. CONCLUSION: The stack test report appears to be acceptable. RECOMMENDATION: It is recommended that the emissions from Units 1, 2, 4, and 5 be considered to have been in compliance with the emission limits of the AO and 40 CFR Part 60 subpart JJJJ during the time testing. HPV: N/A ATTACHMENTS: DAQ Stack Test Review Excel Spreadsheets, Uinta Wax Operating’s Stack Test Reports Emissions CH4-Finley Operating, LLC North Randlett Compressor Station Uintah County, Utah Compressor Engine E1 SN: N6W/4EK00075 Test Date: 6/19/2024 Run # 1 2 3 Average Start Time 16:49 17:50 18:52 Stop Time 17:48 18:50 19:51 Sample Duration (minutes) 60 60 60 BHP Engine Load - Actual (bhp) 800 800 828 810 DS Stack Diameter (inches) 10.0 10.0 10.0 10.0 PAVG Average (Delta P)½ (" H2O)½0.9910 0.9860 1.0130 0.9967 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 864 870 872 869 Pbar Barometric Pressure (" Hg) 23.01 23.01 23.01 23.01 Ps Stack Pressure ('' H2O)0.35 0.34 0.35 0.35 O2%vd O2 (%vd)5.6 6.0 6.1 5.9 CO2%vd CO2 (%vd)6.0 6.2 6.3 6.2 N2%vd N2 (%vd)88.4 87.8 87.6 87.9 dry NOX (ppmvd)94.2 101.0 104.6 99.9 dry CO (ppmvd) 14.8 15.2 15.5 15.2 wet NMNEOC (ppmvd as C3H8)94.8 88.4 86.7 90.0 Run # 1 2 3 Average Bws Measured Moisture Content (%/100) 0.109 0.110 0.111 0.110 Bws Saturated Moisture Content (%/100) 607.150 623.619 629.145 619.971 Bws Actual Moisture Content (%/100) 0.109 0.110 0.111 0.110 MD Molecular Weight Dry (lb/lb-mole) 29.18 29.23 29.25 29.22 MA Molecular Weight Wet (lb/lb-mole) 27.96 28.00 28.01 27.99 VS Gas Velocity (ft/sec)102.0 101.7 104.5 102.8 FACFM Gas Flow (acfm) 3339 3328 3421 3363 FDSCFM Gas Flow (dscfm) 912 905 928 915 FWSCFM Gas Flow (wscfm) 1025 1017 1044 1029 FKWSCFH Gas Flow (kwscfh) 61 61 63 62 FKWSCFM Gas Flow (kwscfm) 1111 lb/hr Gas Flow (lb/hr) 4463 4434 4552 4483 Fo Fo (unitless)2.550 2.403 2.349 2.434 wet O2 (%vw)5.0 5.3 5.4 5.3 wet CO2 (%vw)5.3 5.5 5.6 5.5 wet NOX (ppmvw)83.886 89.873 92.987 88.915 15 NOX (ppmvd @ 15% O2)36.318 39.981 41.679 39.326 41.0 lb/hr NOX (lb/hr)0.615 0.654 0.694 0.654 1.52 g/bhp-hr NOX (g/bhp-hr)0.349 0.371 0.380 0.367 1.0 wet CO (ppmvw) 13.200 13.521 13.759 13.493 15 CO (ppmvd @ 15% O2)5.715 6.015 6.167 5.966 61.0 lb/hr CO (lb/hr) 0.059 0.060 0.063 0.060 1.37 g/bhp-hr CO (g/bhp-hr) 0.033 0.034 0.034 0.034 2.0 dry NMEOC (ppmvd as C3H8)94.800 88.430 86.710 89.980 15 NMEOC (ppmvd as C3H8 @ 15% O2)36.557 35.016 34.567 35.380 60 lb/hr NMEOC (lb/hr as C3H8)0.593 0.549 0.552 0.565 2.13 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.336 0.311 0.302 0.316 0.7 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 1 Emissions CH4-Finley Operating, LLC North Randlett Compressor Station Uintah County, Utah Compressor Engine E2 SN: JEF01814 Test Date: 6/19/2024 Run # 1 2 3 Average Start Time 12:39 13:40 14:41 Stop Time 13:38 14:39 15:40 Sample Duration (minutes) 60 60 60 BHP Engine Load - Actual (bhp) 966 966 966 966 DS Stack Diameter (inches) 14.0 14.0 14.0 14.0 PAVG Average (Delta P)½ (" H2O)½0.9810 0.9590 0.9820 0.9740 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 1158 1161 1160 1160 Pbar Barometric Pressure (" Hg) 25.11 25.11 25.11 25.11 Ps Stack Pressure ('' H2O)0.29 0.30 0.30 0.30 O2%vd O2 (%vd)5.7 6.0 5.9 5.9 CO2%vd CO2 (%vd)6.9 7.0 7.0 7.0 N2%vd N2 (%vd)87.4 87.0 87.1 87.2 dry NOX (ppmvd)82.5 83.8 84.6 83.7 dry CO (ppmvd) 3.8 3.8 3.9 3.8 wet NMNEOC (ppmvd as C3H8)73.0 72.7 72.6 72.8 Run # 1 2 3 Average Bws Measured Moisture Content (%/100) 0.108 0.108 0.109 0.109 Bws Saturated Moisture Content (%/100) 1613.440 1627.598 1622.855 1621.298 Bws Actual Moisture Content (%/100) 0.108 0.108 0.109 0.109 MD Molecular Weight Dry (lb/lb-mole) 29.33 29.36 29.36 29.35 MA Molecular Weight Wet (lb/lb-mole) 28.11 28.13 28.12 28.12 VS Gas Velocity (ft/sec)106.6 104.3 106.8 105.9 FACFM Gas Flow (acfm) 6839 6689 6849 6793 FDSCFM Gas Flow (dscfm) 1671 1630 1669 1657 FWSCFM Gas Flow (wscfm) 1874 1830 1875 1860 FKWSCFH Gas Flow (kwscfh) 112 110 112 112 FKWSCFM Gas Flow (kwscfm) 2222 lb/hr Gas Flow (lb/hr) 8204 8015 8208 8143 Fo Fo (unitless)2.203 2.129 2.143 2.158 wet O2 (%vw)5.1 5.3 5.3 5.2 wet CO2 (%vw)6.2 6.2 6.2 6.2 wet NOX (ppmvw)73.608 74.752 75.389 74.583 15 NOX (ppmvd @ 15% O2)32.031 33.198 33.292 32.840 41.0 lb/hr NOX (lb/hr)0.987 0.979 1.011 0.992 1.52 g/bhp-hr NOX (g/bhp-hr)0.463 0.460 0.475 0.466 1.0 wet CO (ppmvw) 3.354 3.397 3.447 3.399 15 CO (ppmvd @ 15% O2)1.459 1.509 1.522 1.497 61.0 lb/hr CO (lb/hr) 0.027 0.027 0.028 0.028 1.37 g/bhp-hr CO (g/bhp-hr) 0.013 0.013 0.013 0.013 2.0 dry NMEOC (ppmvd as C3H8)72.960 72.680 72.630 72.757 15 NMEOC (ppmvd as C3H8 @ 15% O2)28.320 28.779 28.568 28.556 60 lb/hr NMEOC (lb/hr as C3H8)0.836 0.813 0.831 0.827 2.13 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.393 0.382 0.390 0.388 0.7 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 1 Emissions CH4-Finley Operating, LLC North Randlett Compressor Station Uintah County, Utah Compressor Engine E4 SN: JEF01637 Test Date: 6/19/2024 Run # 1 2 3 Average Start Time 7:37 8:38 9:39 Stop Time 8:36 9:37 10:39 Sample Duration (minutes) 60 60 60 BHP Engine Load - Actual (bhp) 979 979 979 979 DS Stack Diameter (inches) 16.0 16.0 16.0 16.0 PAVG Average (Delta P)½ (" H2O)½0.7270 0.7310 0.7320 0.7300 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 741 745 744 744 Pbar Barometric Pressure (" Hg) 25.13 25.13 25.13 25.13 Ps Stack Pressure ('' H2O)0.23 0.23 0.23 0.23 O2%vd O2 (%vd)5.7 5.9 6.1 5.9 CO2%vd CO2 (%vd)7.0 6.9 6.9 6.9 N2%vd N2 (%vd)87.3 87.2 87.0 87.2 dry NOX (ppmvd)73.5 73.1 73.1 73.2 dry CO (ppmvd) 20.0 19.8 19.7 19.9 wet NMNEOC (ppmvd as C3H8)59.7 59.4 59.7 59.6 Run # 1 2 3 Average Bws Measured Moisture Content (%/100) 0.113 0.109 0.109 0.110 Bws Saturated Moisture Content (%/100) 301.849 308.557 306.871 305.759 Bws Actual Moisture Content (%/100) 0.113 0.109 0.109 0.110 MD Molecular Weight Dry (lb/lb-mole) 29.35 29.34 29.35 29.35 MA Molecular Weight Wet (lb/lb-mole) 28.07 28.11 28.12 28.10 VS Gas Velocity (ft/sec) 68.1 68.6 68.6 68.4 FACFM Gas Flow (acfm) 5706 5743 5747 5732 FDSCFM Gas Flow (dscfm) 1868 1883 1887 1879 FWSCFM Gas Flow (wscfm) 2108 2114 2118 2113 FKWSCFH Gas Flow (kwscfh) 126 127 127 127 FKWSCFM Gas Flow (kwscfm) 2222 lb/hr Gas Flow (lb/hr) 9212 9254 9273 9246 Fo Fo (unitless)2.171 2.174 2.145 2.163 wet O2 (%vw)5.1 5.3 5.4 5.3 wet CO2 (%vw)6.2 6.1 6.2 6.2 wet NOX (ppmvw)65.189 65.113 65.195 65.166 15 NOX (ppmvd @ 15% O2)28.533 28.741 29.153 28.809 41.0 lb/hr NOX (lb/hr)0.983 0.985 0.988 0.985 1.52 g/bhp-hr NOX (g/bhp-hr)0.455 0.456 0.458 0.456 1.0 wet CO (ppmvw) 17.745 17.662 17.598 17.668 15 CO (ppmvd @ 15% O2)7.767 7.796 7.869 7.811 61.0 lb/hr CO (lb/hr) 0.163 0.163 0.162 0.163 1.37 g/bhp-hr CO (g/bhp-hr) 0.075 0.075 0.075 0.075 2.0 dry NMEOC (ppmvd as C3H8)59.730 59.400 59.700 59.610 15 NMEOC (ppmvd as C3H8 @ 15% O2)23.185 23.364 23.799 23.449 60 lb/hr NMEOC (lb/hr as C3H8)0.765 0.767 0.773 0.768 2.13 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.355 0.355 0.358 0.356 0.7 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 1 Emissions CH4-Finley Operating, LLC North Randlett Compressor Station Uintah County, Utah Compressor Engine E5 SN: N6W/JEF01780 Test Date: 6/20/2024 Run # 1 2 3 Average Start Time 7:51 8:52 9:53 Stop Time 8:50 9:51 10:52 Sample Duration (minutes) 60 60 60 BHP Engine Load - Actual (bhp) 1200 1200 1200 1200 DS Stack Diameter (inches) 13.5 13.5 13.5 13.5 PAVG Average (Delta P)½ (" H2O)½0.8140 0.8150 0.8300 0.8197 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 772 784 782 780 Pbar Barometric Pressure (" Hg) 25.17 25.17 25.17 25.17 Ps Stack Pressure ('' H2O)0.26 0.25 0.27 0.26 O2%vd O2 (%vd)5.5 5.9 5.9 5.8 CO2%vd CO2 (%vd)6.7 6.7 6.7 6.7 N2%vd N2 (%vd)87.8 87.4 87.4 87.5 dry NOX (ppmvd)90.9 91.4 94.4 92.2 dry CO (ppmvd) 34.0 33.9 34.4 34.1 wet NMNEOC (ppmvd as C3H8)71.8 71.4 72.8 72.0 Run # 1 2 3 Average Bws Measured Moisture Content (%/100) 0.110 0.107 0.108 0.108 Bws Saturated Moisture Content (%/100) 355.881 378.659 374.778 369.773 Bws Actual Moisture Content (%/100) 0.110 0.107 0.108 0.108 MD Molecular Weight Dry (lb/lb-mole) 29.29 29.31 29.31 29.30 MA Molecular Weight Wet (lb/lb-mole) 28.05 28.10 28.09 28.08 VS Gas Velocity (ft/sec) 77.2 77.6 79.0 77.9 FACFM Gas Flow (acfm) 4604 4628 4710 4648 FDSCFM Gas Flow (dscfm) 1477 1475 1502 1485 FWSCFM Gas Flow (wscfm) 1661 1653 1685 1666 FKWSCFH Gas Flow (kwscfh) 100 99 101 100 FKWSCFM Gas Flow (kwscfm) 2222 lb/hr Gas Flow (lb/hr) 7254 7234 7372 7287 Fo Fo (unitless)2.299 2.239 2.239 2.259 wet O2 (%vw)4.9 5.3 5.3 5.1 wet CO2 (%vw)6.0 6.0 6.0 6.0 wet NOX (ppmvw)80.919 81.584 84.232 82.245 15 NOX (ppmvd @ 15% O2)34.833 35.935 37.142 35.970 41.0 lb/hr NOX (lb/hr)0.961 0.965 1.016 0.981 1.52 g/bhp-hr NOX (g/bhp-hr)0.364 0.365 0.384 0.371 1.0 wet CO (ppmvw) 30.242 30.237 30.676 30.385 15 CO (ppmvd @ 15% O2)13.018 13.318 13.527 13.288 61.0 lb/hr CO (lb/hr) 0.219 0.218 0.225 0.221 1.37 g/bhp-hr CO (g/bhp-hr) 0.083 0.082 0.085 0.083 2.0 dry NMEOC (ppmvd as C3H8)71.750 71.440 72.790 71.993 15 NMEOC (ppmvd as C3H8 @ 15% O2)27.489 28.100 28.631 28.073 60 lb/hr NMEOC (lb/hr as C3H8)0.727 0.723 0.750 0.733 2.13 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.275 0.273 0.284 0.277 0.7 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 1 Source Test Report For Uinta Wax Operating, LLC North Randlett Compressor Station Uintah County, Utah Test Date: June 19, 2024 Report Date: July 2, 2024 UDEQ Permit: #DAQE-AN159380002-23 Engine: Caterpillar G3516B SN: N6W/4EK00075 Unit ID: #1 Prepared By: Oasis Emission Consultants, Inc. 2730 Commercial Way Rock Springs, WY 82901 July 2, 2024 Ms. Karen Pratt Uinta Wax Operating, LLC Dear Ms. Pratt: Re: Engine Emission Testing For Uinta Wax Operating, LLC, North Randlett Compressor Station, Unit #1, Permit #DAQE-AN159380002-23. An air emissions test program was conducted on a Caterpillar G3516B engine, operated by Uinta Wax Operating, LLC and designated as Unit #1, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC). Oasis Emission Consultants, Inc. conducted the testing on June 19, 2024. UDEQ Permit #DAQE-AN159380002-23 Emission Levels The average recorded levels were found to comply with emission levels stipulated in the permit, as shown in the attached report and summarized below. Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC ppm @ 15% O2 39.33 41 5.97 61 35.38 60 lbs/hr 0.66 1.52 0.06 1.37 0.57 2.13 *VOC levels reported as non-methane, non-ethane hydrocarbon on a propane basis (NMNEHC C3). EPA 40 CFR 60, Subpart JJJJ Emission Levels Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC g/bhp-hr 0.37 1.0 0.03 2.0 0.32 0.7 Catalyst Parameters (Averaged Over 3 Test Runs) Inlet Temp (deg F) DP (in H2O) 849 1.2 Engine Load (Averaged Over 3 Test Runs) Rated BHP Operating BHP % Load 1380 809.6 58.7 Testing Protocol The attached report was generated using an extractive FTIR system using methodologies as required by and in accordance with EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, as outlined in the submitted Source Test Protocol. Quality Assurance Oasis has performed a full review of the raw data and calculated results in this report. Any errors we have encountered have been listed in the body of this report. After performing the review, we are confident that this engine has met all requirements. If you have any questions or require further information, please contact the undersigned at (307) 382-3297. Yours truly, Oasis Emission Consultants, Inc. _________________________ _______________________ Charles A. Chapman Crystal Leonard Manager of Technical Services Senior EHS Specialist _________________________ Christopher N. Knott, P.Eng. Director, Engineering and Operations SOURCE EMISSION TEST REPORT UDEQ Permit #DAQE-AN159380002-23 Test Performed By: Oasis Emission Consultants, Inc. Test Company Contact: Chris Knott 2730 Commercial Way Rock Springs, WY 82901 307.382.3297 Owner/Operator: Uinta Wax Operating, LLC Owner/Operator Contact: Karen Pratt (720) 990-9927 Facility Name: North Randlett Compressor Station UTM Coordinates: 593,702 m Easting, 4,453,005 m Northing UTM Zone 12 Uintah County, Utah Emission Source: Caterpillar G3516B Unit #1 Date of Test: June 19, 2024 Date of Report: July 2, 2024 TABLE OF CONTENTS 1.1 Introduction .......................................................................................................................... 1 2.1 Stack Sampling Location ..................................................................................................... 2 3.1 Discussion of NOx, CO and VOC Test Results ................................................................... 3 3.1.1 Source Test 1 ............................................................................................................................................ 3 3.1.2 Source Test 2 ............................................................................................................................................ 3 3.1.3 Source Test 3 ............................................................................................................................................ 3 4.1 Stack Sampling Methods and Procedures ............................................................................ 4 4.2 Equipment Utilization .......................................................................................................... 5 4.3 Measurement of VOC (NMNEHC C3) ............................................................................... 6 4.4 Process Parameters............................................................................................................... 6 5.1 Quality Assurance ................................................................................................................ 7 List of Tables and Figures Figure 1 - Sample Port Location ............................................................................................................................. 2 Figure 2 - Sampling Train Schematic-Method 320 ................................................................................................ 5 Table 1 - Insertion Depths of Traverse Points for Stratification Test ..................................................................... 2 Table 2 - Test Matrix .............................................................................................................................................. 4 Table 3 - Concentrations and Interference .............................................................................................................. 5 APPENDIX A: NOx, CO and VOC Test Data APPENDIX B: Quality Assurance/Calibration Data APPENDIX C: Load Approximation APPENDIX D: Example Calculations and Summary APPENDIX E: Field Notes 1 1.1 Introduction An air emissions test program was conducted on a Caterpillar G3516B engine, operated by Uinta Wax Operating, LLC and designated as Unit #1, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC) defined as non-methane, non-ethane hydrocarbons, reported as propane (NMNEHC C3). The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Three one hour test runs were performed on June 19, 2024 to analyze NOx, CO and VOC emission levels. Test runs were performed according to methodologies outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320 as outlined in the submitted Source Test Protocol dated May 17, 2024. Each one hour test run consisted of 60 readings taken at one minute intervals. Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. The following key personnel were present during testing: David Martinez, OEC Kyle John 2 2.1 Stack Sampling Location The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Testing was conducted on the Caterpillar G3516B engine. The sampling port for moisture, NOx, CO and VOC measurements was approximately 3.2 pipe diameters (32”) downstream from the nearest flow disturbance (Distance B) and 9.6 pipe diameters (96”) upstream from the nearest disturbance (Distance A), as seen in Figure 1. The stack sampling location was placed at approximately 50% insertion depth based on an O2 stratification check which demonstrated a non-stratified flow regime. The stratification was conducted according to EPA 40 CFR 75(A), §6.5.6.1 using 3 traverse points determined according to Table 1 below. Figure 1 - Sample Port Location Table 1 - Insertion Depths of Traverse Points for Stratification Test Traverse Point Insertion Depth (Percent of Stack Diameter) 1 16.6 2 50.0 3 83.3 10" A B Oxidation Catalyst 3 3.1 Discussion of NOx, CO and VOC Test Results Three, one hour test runs were performed on June 19, 2024 to analyze exhaust NOx, CO and VOC (NMNEHC C3) emission levels to demonstrate annual compliance with the emissions limits contained in the WDEQ Permit #DAQE-AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ. Testing for NOx, CO and VOC were run concurrently with one another. Each test was performed at the maximum achievable load. Measured emissions were below permitted limits. Please refer to the Appendices for a listing of all raw data, calibration error response and calculations performed per EPA 40 CFR 60(A) requirements. 3.1.1 Source Test 1: Caterpillar G3516B, NOx, CO and VOC The first test was performed from 16:49 to 17:48 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 800.4 bhp, and the average NOx and CO levels were found to be 0.35 g/bhp-hr and 0.03 g/bhp-hr respectively, below limitations. The VOC level tested at 0.34 g/bhp- hr, which tested in compliance. 3.1.2 Source Test 2: Caterpillar G3516B, NOx, CO and VOC The second test was performed from 17:50 to 18:50 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 800.4 bhp, and the average NOx and CO levels were found to be 0.37 g/bhp-hr and 0.03 g/bhp-hr respectively, below limitations. The VOC level tested at 0.31 g/bhp- hr, which tested in compliance. 3.1.3 Source Test 3: Caterpillar G3516B, NOx, CO and VOC The third test was performed from 18:52 to 19:51 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 828.0 bhp, and the average NOx and CO levels were found to be 0.38 g/bhp-hr and 0.03 g/bhp-hr respectively, below limitations. The VOC level tested at 0.30 g/bhp- hr, which tested in compliance. Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 1 94.18 0.35 14.82 0.03 94.80 0.34 5.6 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 2 100.97 0.37 15.19 0.03 88.43 0.31 6.0 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 3 104.55 0.38 15.47 0.03 86.71 0.30 6.1 4 4.1 Stack Sampling Methods and Procedures Testing followed EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, with no exceptions. Table 2 - Test Matrix Method Title Parameter Reference EPA 40 CFR 60 Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources Sampling Point Determination https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_1_3.pdf EPA 40 CFR 60 Appendix A, Method 2 Determination of Stack Gas Velocity and Volumetric Flow Rate Exhaust Effluent Flow https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_2.pdf EPA 40 CFR 60 Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight O2, CO2, Dry Volumetric Flow Rate https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_3.pdf EPA 40 CFR 63 Appendix A, EPA Method 320 Vapor Phase Organic and Inorganic Emissions by Extractive FTIR Nitrogen Oxides, Carbon Monoxide, Non- Methane Non- Ethane Hydrocarbons on a Propane Basis https://www.epa.gov/ emc/method-320- vapor-phase-organic- and-inorganic- emissions-extractive- ftir United States. U.S. Environmental Protection Agency. “EMC Promulgated Test Methods.” Air Emission Measurement Center (EMC). 31 August 2023. Web. 2 July 2024. <https://www.epa.gov/emc/emc-promulgated-test-methods>. ASTM International. “Standards & Publications.” All Environment Standards. Web. 2 July 2024. <https://www.astm.org/Standards/D6348.htm>. 5 4.2 Equipment Utilization The following equipment was used during the tests performed at this facility in conjunction with procedures outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320. • (1) MKS MultiGas 2030 FTIR Continuous Gas Analyzer (0.210 L/min sample flow, 0.014 atmosphere sample pressure, 1 atmosphere cell pressure, 191°C cell temperature) • (1) Laptop Computer for the FTIR Analyzer using MKS MG2000 Software • (1) 75ft or 100ft Heated Teflon Line w/ Heated Sample Probe and Spike Bypass Line • S-Type Pitot Tube c/w 20 ft. Heated Sample Line (coefficient 0.84) • (1) Enerac 500 Portable O2/CO2 Analyzer • (1) Fyrite O2/CO2 Analyzer • (5) EPA Protocol G1 Calibration Gas (NOx, CO, C3H8, C2H4 and NO2) The MKS Multigas 2030 FTIR Analyzer operated with a spectral resolution of 0.5 cm-1 and a scan time of 30 seconds. The FTIR spectrometer utilizes a multi-pass gas cell with a 5.11 meter effective pathlength. Figure 2 - Sampling Train Schematic-Method 320 Table 3 - Concentrations and Interference 6 The MKS 2030 software provides a Natural Gas Method that is designed to minimize all expected interferences by removing the regions in the quant region where they are most absorbed (i.e. picket fence approach). So, for example, all the water peaks that are greater than about 0.1 abs are removed from the quant region. Since the spectral noise measured (sample spectrum) is in the range of 0.001 absorbance, it is desirable to have any error within this range. The MKS software will match the water calibration spectrum to the sample spectrum at any 1 point in the spectrum to about 1% precision. So, 1% of 0.1 absorbance is 0.001 abs. This is why any peaks greater than this for interfering compounds are usually excluded so they do not interfere. To summarize, the MKS software and the method are designed to minimize any interferences by removing their largest interfering absorptions. 4.3 Measurement of VOC (NMNEHC C3) The algorithm currently used for NMNEHC C3 and developed for natural gas fired applications by Dr. Spartz and MKS instruments in accordance with EPA standards, is the following: (2.4*c8/(1+exp((2-c8)/0.2))+1.9*c11/(1+exp((2-c11)/0.2))+6*c12/(1+exp((0.5-c12) /0.2))+2.85*c13/(1+exp((2-c13)/0.2))+3*c14/(1+exp((1-c14)/0.2)))/3 c8= acetylene c11= ethylene c12= hexane c13= propylene c14= propane Note: The constants in front of each of the compounds listed represents the FID response factor when calibrated with Propane. As with any CEMS analyzer, the FTIR may demonstrate a negative zero bias. The “exp” functions listed in the algorithm above are intended to mathematically filter out any negative biases and set them to approach zero. 4.4 Process Parameters Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. Results are provided in Appendix C. 7 5.1 Quality Assurance The MKS Multigas 2030 FTIR Analyzer was used to measure NOx, CO and VOC on a dry basis. A pre Direct and System calibration measurement was made on compounds of NOx, CO, C3H8 and C2H4. In addition, post System calibrations were made on compounds of NOx, CO, C3H8 and C2H4. Compounds of CO2 and C3H8 were measured for the quality assurance spiking requirements. Levels for calibrations and zeroes must be within +/- 5% of the certified calibration gas or response to zero gas, respectively. CTS procedures were followed according to EPA requirements for both pre and post testing. Similarly, QA spiking procedures were followed. Analysis of the CO2 exhaust effluent was used to determine the dilution factor. Steady levels of the CO2 were observed and a sufficient duration of time was allowed to elapse for a representative average. The calibration gas was spiked into the effluent stream using a bypass line at approximately 10% of the sampling rate. The dilution factor was obtained from observation of the stack CO2 behavior using the following equation: CO2AVG – CO2SPIKE DF = ------------------------ CO2 AVG Where: CO2AVG = The average undiluted CO2 stack gas concentration of spike measurements CO2SPIKE = The average diluted CO2 stack gas concentration when spiked The sample recovery was then obtained from the following equation: % REC = (Spike MEAS – Stack MEAS)* (1 – DF) --------------------------------------------------------- CS * DF Where: Spike MEAS = The average diluted stack gas concentration when spiked Stack MEAS = The average undiluted stack gas concentration DF = Dilution factor CS = Certified concentration of calibration standards The Sample Recovery average level for C3H8 was found to be 86.4%, which was within the allowable tolerance of Method 320 (70% to 130%). A summary of all spiking procedures/results can be found in Appendix B. APPENDIX A NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 58.203711 33.886391 92.090102 15.00558 98.872665 10.948117 16:49:51 06/19/2024 2 59.092532 34.192035 93.284567 15.016221 96.905169 11.147216 16:50:51 06/19/2024 3 58.230295 33.923078 92.153373 14.867625 96.510638 11.252185 16:51:52 06/19/2024 4 65.33858 37.675893 103.014473 15.640244 94.787878 11.184955 16:52:52 06/19/2024 5 58.414333 33.964256 92.378589 15.06903 99.364625 11.060062 16:53:52 06/19/2024 6 54.648315 31.876422 86.524737 14.642775 99.361735 10.910879 16:54:52 06/19/2024 7 60.246703 34.785177 95.03188 15.19635 96.048896 10.862486 16:55:52 06/19/2024 8 65.129901 37.607045 102.736946 15.600779 94.699146 10.857098 16:56:52 06/19/2024 9 57.083861 33.08973 90.173591 14.934839 98.451111 10.782596 16:57:52 06/19/2024 10 55.439748 32.031775 87.471523 14.719331 99.318065 10.785487 16:58:52 06/19/2024 11 53.946176 31.217547 85.163723 14.543009 100.291386 10.801745 16:59:52 06/19/2024 12 58.154123 33.7637 91.917823 14.743134 97.754973 10.827661 17:00:52 06/19/2024 13 57.782219 33.526285 91.308504 14.661494 98.461651 10.817633 17:01:52 06/19/2024 14 59.352138 34.247601 93.599739 14.758925 97.612402 10.869863 17:02:53 06/19/2024 15 59.157125 34.277713 93.434838 14.683456 97.707649 10.868137 17:03:53 06/19/2024 16 57.335751 33.454458 90.790209 14.561423 97.922034 10.859001 17:04:52 06/19/2024 17 59.302577 34.555475 93.858052 14.730103 95.496341 10.892814 17:05:53 06/19/2024 18 65.917023 38.253924 104.170947 15.299088 93.131859 10.957993 17:06:53 06/19/2024 19 59.442564 34.693403 94.135967 14.836382 96.383661 10.907822 17:07:53 06/19/2024 20 60.404674 35.204729 95.609403 14.999161 95.983626 10.929564 17:08:53 06/19/2024 21 59.445534 34.479747 93.925281 14.776178 96.655972 10.898002 17:09:53 06/19/2024 22 60.873105 35.303624 96.176729 14.966114 96.850202 10.919791 17:10:53 06/19/2024 23 60.458695 34.97974 95.438435 14.990597 96.357934 10.915137 17:11:53 06/19/2024 24 59.367548 34.439506 93.807054 15.173856 96.939595 10.925823 17:12:53 06/19/2024 25 56.727769 33.005475 89.733244 14.652504 97.116047 10.885877 17:13:54 06/19/2024 26 57.758689 33.405042 91.163731 14.91849 95.615000 10.92421 17:14:53 06/19/2024 27 63.801748 36.693136 100.494884 15.289123 92.581203 10.950152 17:15:53 06/19/2024 28 53.798848 31.066344 84.865192 14.391285 99.000160 10.842475 17:16:54 06/19/2024 29 60.768958 34.942292 95.71125 14.952597 96.078859 10.908137 17:17:54 06/19/2024 30 56.438121 32.600418 89.038539 14.462065 97.546019 10.87283 17:18:54 06/19/2024 31 60.631892 34.77503 95.406922 15.019507 96.529002 10.909496 17:19:54 06/19/2024 32 61.174194 35.141525 96.315719 14.977579 95.371600 10.917013 17:20:54 06/19/2024 33 61.225629 35.029289 96.254918 15.007926 95.608869 10.930247 17:21:54 06/19/2024 34 58.722665 33.84866 92.571325 14.709543 95.516160 10.911519 17:22:54 06/19/2024 35 60.540132 34.788797 95.328929 14.810659 96.020248 10.943152 17:23:54 06/19/2024 36 59.282944 34.028054 93.310998 14.76341 95.599946 10.914582 17:24:54 06/19/2024 37 58.849146 33.754969 92.604115 14.800092 95.391092 10.940181 17:25:55 06/19/2024 38 59.625227 34.191279 93.816506 15.024016 95.370901 10.912896 17:26:54 06/19/2024 39 59.141997 34.09768 93.239677 14.95516 93.750941 10.95285 17:27:54 06/19/2024 40 58.641142 33.734949 92.376091 15.019794 93.735360 10.960164 17:28:55 06/19/2024 41 58.613076 33.544087 92.157163 14.740234 93.773681 10.975983 17:29:55 06/19/2024 42 59.10689 33.718486 92.825376 14.716449 93.499205 10.952855 17:30:55 06/19/2024 43 59.365719 34.02432 93.390039 14.767508 92.659700 10.931932 17:31:55 06/19/2024 44 60.902527 34.84086 95.743387 14.738349 91.601431 10.965107 17:32:55 06/19/2024 45 60.276669 34.419041 94.69571 14.649924 91.808307 10.95325 17:33:55 06/19/2024 46 60.241949 34.258549 94.500498 14.590803 91.251549 10.944776 17:34:55 06/19/2024 47 60.194824 34.260046 94.45487 14.537196 91.416680 10.960541 17:35:55 06/19/2024 48 60.93484 34.563761 95.498601 14.595133 91.396438 10.927464 17:36:56 06/19/2024 49 60.573684 34.267383 94.841067 14.604054 91.291600 10.944807 17:37:55 06/19/2024 50 61.139802 34.687557 95.827359 14.550265 90.241072 10.937373 17:38:55 06/19/2024 51 61.464617 34.953289 96.417906 14.663956 91.094441 10.929474 17:39:56 06/19/2024 52 62.063767 35.083724 97.147491 14.638978 91.768647 10.951448 17:40:56 06/19/2024 53 61.495025 34.996829 96.491854 14.573745 91.290141 10.96484 17:41:56 06/19/2024 54 60.468233 34.370115 94.838348 14.526319 91.697316 10.932919 17:42:56 06/19/2024 55 61.605718 35.040419 96.646137 14.580338 91.295428 10.933167 17:43:56 06/19/2024 56 62.089112 35.127461 97.216573 14.574891 90.999452 10.958567 17:44:56 06/19/2024 57 62.220884 35.360792 97.581676 14.599067 89.748552 10.962413 17:45:56 06/19/2024 58 62.128006 35.307871 97.435877 14.825668 90.684467 10.956019 17:46:56 06/19/2024 59 60.734059 34.554607 95.288666 14.664169 88.924490 10.971901 17:47:56 06/19/2024 60 62.104213 35.209577 97.31379 14.852092 88.852276 10.962207 17:48:56 06/19/2024 AVG 59.79 0.00 94.18 14.82 94.80 10.93 ppm@15% O2 36.32 5.71 36.56 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.35 0.62 0.03 0.06 0.34 0.59 #1 FTIR Measurements Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 1 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 10 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.93 1323 0.35 0.964 Average O2 5.6 (% dry)A 2 1.05 0.95 0.975 Average CO2 6 (% dry)A 3 1.94 0.99 0.995 Average N2 + CO 88.4 (% dry)A 4 3.23 1.01 1.005 Dry Molecular Weight 29.18 lb/lbmol A 5 6.77 1.04 1.020 Wet Molecular Weight 27.96 lb/lbmol A 6 8.06 0.99 0.995 EPA REFERENCE METHOD 320 A 7 8.95 0.97 0.985 Barometric Pressure 23.01 in Hg A 8 9.50 0.94 0.970 Moisture Content 10.93 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 94.18 ppm A 11 Calculated NOx Mass Output 0.62 lbs/hr A 12 Calculated NOx Output 0.35 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 14.82 ppm A 15 Calculated CO Mass Output 0.06 lbs/hr A 16 Calculated CO Output 0.03 g/bhp-hr B 1 0.50 0.94 1323 0.35 0.970 EPA REFERENCE METHOD 320 B 2 1.05 0.97 0.985 Average Analyzer NMNEHC Level 94.80 ppm B 3 1.94 0.99 0.995 Calculated NMNEHC Mass Output 0.59 lbs/hr B 4 3.23 1.03 1.015 Calculated NMNEHC Output 0.34 g/bhp-hr B 5 6.77 1.06 1.030 LOAD APPROXIMATION B 6 8.06 1.00 1.000 Estimated Engine Load 800.4 BHP B 7 8.95 0.96 0.980 B 8 9.50 0.96 0.980 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 1.0 1323 0.4 0.991 Average Stack Gas Velocity 102.03 ft/sec Average Dry Flowrate 913.78 dscfm TEST RUN # 1 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 60.970978 34.374166 95.345144 14.916562 89.990847 10.92465 17:50:57 06/19/2024 2 62.398141 35.168022 97.566163 14.89559 90.398865 10.952503 17:51:57 06/19/2024 3 61.888632 34.949198 96.83783 14.936537 90.542173 10.955575 17:52:57 06/19/2024 4 61.969532 34.81331 96.782842 14.902534 91.551725 10.940858 17:53:57 06/19/2024 5 63.724479 35.812306 99.536785 14.88748 89.972163 10.958478 17:54:57 06/19/2024 6 63.666149 35.647983 99.314132 14.868564 89.495742 10.930412 17:55:57 06/19/2024 7 63.735585 35.619778 99.355363 14.722866 88.657410 10.947796 17:56:57 06/19/2024 8 64.214106 35.904495 100.118601 14.974925 89.746131 10.964181 17:57:57 06/19/2024 9 64.166615 35.933077 100.099692 14.886796 87.833835 10.952886 17:58:57 06/19/2024 10 64.528206 35.999008 100.527214 15.074317 88.915837 10.95223 17:59:57 06/19/2024 11 63.959143 35.813105 99.772248 15.037388 89.622633 10.960064 18:00:57 06/19/2024 12 65.062774 36.207373 101.270147 15.289281 87.763500 10.950528 18:01:57 06/19/2024 13 63.091857 35.282996 98.374853 15.057549 88.452566 10.932682 18:02:58 06/19/2024 14 62.203823 34.894157 97.09798 14.983838 88.132740 10.960887 18:03:58 06/19/2024 15 63.480488 35.427147 98.907635 15.038937 88.325183 10.970748 18:04:58 06/19/2024 16 62.187834 35.026771 97.214605 14.960088 88.890262 10.938314 18:05:58 06/19/2024 17 65.458321 36.639798 102.098119 15.247541 85.841444 10.986955 18:06:58 06/19/2024 18 64.953415 36.611434 101.564849 15.287654 86.241001 10.990078 18:07:58 06/19/2024 19 64.353049 36.102009 100.455058 15.234146 85.850579 10.992716 18:08:58 06/19/2024 20 64.767785 36.47122 101.239005 15.056593 86.022988 10.983254 18:09:58 06/19/2024 21 65.559144 37.08313 102.642274 15.095471 86.395841 10.993844 18:10:59 06/19/2024 22 64.714907 36.473381 101.188288 15.220958 86.289181 10.998178 18:11:58 06/19/2024 23 64.074497 36.324584 100.399081 15.255049 88.097710 10.982507 18:12:59 06/19/2024 24 64.214138 36.57265 100.786788 15.222749 86.712267 10.99252 18:13:59 06/19/2024 25 63.308182 36.165446 99.473628 15.20031 86.376034 11.012249 18:14:59 06/19/2024 26 62.925781 35.912574 98.838355 15.032072 87.657367 11.001499 18:15:59 06/19/2024 27 64.115957 36.44912 100.565077 15.188597 88.258296 10.994241 18:16:59 06/19/2024 28 63.207026 35.957436 99.164462 15.038829 89.859305 10.977918 18:17:59 06/19/2024 29 64.157015 36.605958 100.762973 15.274304 89.550621 11.007589 18:18:59 06/19/2024 30 64.938326 37.08944 102.027766 15.272718 88.179236 10.994952 18:19:59 06/19/2024 31 64.237716 36.737644 100.97536 15.238232 89.931624 11.012175 18:20:59 06/19/2024 32 66.196658 37.825826 104.022484 15.506928 87.126957 11.022228 18:21:59 06/19/2024 33 66.687988 37.937242 104.62523 15.441076 86.301333 11.03476 18:23:00 06/19/2024 34 65.284503 37.272098 102.556601 15.240454 88.059706 11.019362 18:23:59 06/19/2024 35 64.701676 36.942087 101.643763 15.311472 89.577580 11.011333 18:24:59 06/19/2024 36 65.693794 37.452611 103.146405 15.369285 88.615879 11.02127 18:26:00 06/19/2024 37 65.462639 37.305765 102.768404 15.645131 88.890002 11.018418 18:27:00 06/19/2024 38 62.598745 35.615412 98.214157 15.262858 89.888541 10.992 18:28:00 06/19/2024 39 63.608298 36.061285 99.669583 15.302191 88.039492 11.022459 18:29:00 06/19/2024 40 63.929886 36.321998 100.251884 15.394609 88.741207 11.022953 18:30:00 06/19/2024 41 66.736573 37.649067 104.38564 15.700494 87.343296 11.0284 18:31:00 06/19/2024 42 64.977561 36.714674 101.692235 15.302356 87.674232 11.004323 18:32:00 06/19/2024 43 66.298974 37.615215 103.914189 15.502869 87.669978 11.018649 18:33:00 06/19/2024 44 65.749295 37.128492 102.877787 15.356 87.055010 11.016695 18:34:00 06/19/2024 45 63.317898 35.98226 99.300158 15.107838 89.022319 10.995376 18:35:00 06/19/2024 46 65.489097 37.174839 102.663936 15.291237 88.830467 11.012466 18:36:00 06/19/2024 47 66.600152 37.538889 104.139041 15.372407 87.866163 11.02799 18:37:01 06/19/2024 48 66.579818 37.630517 104.210335 15.296239 87.637120 11.014958 18:38:01 06/19/2024 49 65.186841 36.92963 102.116471 15.217532 89.222858 11.010868 18:39:01 06/19/2024 50 65.128706 37.040209 102.168915 15.276323 90.418638 10.993288 18:40:01 06/19/2024 51 64.644192 36.873931 101.518123 15.298764 89.132294 11.010053 18:41:01 06/19/2024 52 63.621534 36.266234 99.887768 15.268379 90.413906 10.996761 18:42:01 06/19/2024 53 64.097785 36.427718 100.525503 15.01573 87.628126 10.995395 18:43:01 06/19/2024 54 68.363779 38.778611 107.14239 15.250318 87.109195 11.029001 18:44:01 06/19/2024 55 68.395026 38.64939 107.044416 15.29237 87.591064 11.0549 18:45:01 06/19/2024 56 66.507756 37.74896 104.256716 15.349243 88.698088 10.995328 18:46:02 06/19/2024 57 64.27264 36.550088 100.822728 15.285664 89.817733 11.003211 18:47:02 06/19/2024 58 64.775626 36.658653 101.434279 15.279784 89.529832 11.003027 18:48:02 06/19/2024 59 64.079758 36.250147 100.329905 15.213115 88.171635 11.009997 18:49:02 06/19/2024 60 64.452366 36.311831 100.764197 15.18046 90.054196 11.009395 18:50:02 06/19/2024 AVG 64.49 0.00 100.97 15.19 88.43 10.99 ppm@15% O2 39.98 6.02 35.02 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.37 0.65 0.03 0.06 0.31 0.55 Calculated Emission Levels Record Date Uinta Wax Operating, LLC North Randlett Compressor Station Run 2 #1 FTIR Measurements EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 10 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.91 1329 0.34 0.954 Average O2 6.0 (% dry)A 2 1.05 0.95 0.975 Average CO2 6.2 (% dry)A 3 1.94 0.97 0.985 Average N2 + CO 87.8 (% dry)A 4 3.23 1.02 1.010 Dry Molecular Weight 29.23 lb/lbmol A 5 6.77 1.08 1.039 Wet Molecular Weight 28.00 lb/lbmol A 6 8.06 1.02 1.010 EPA REFERENCE METHOD 320 A 7 8.95 0.98 0.990 Barometric Pressure 23.01 in Hg A 8 9.50 0.96 0.980 Moisture Content 10.99 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 100.97 ppm A 11 Calculated NOx Mass Output 0.65 lbs/hr A 12 Calculated NOx Output 0.37 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 15.19 ppm A 15 Calculated CO Mass Output 0.06 lbs/hr A 16 Calculated CO Output 0.03 g/bhp-hr B 1 0.50 0.89 1329 0.34 0.943 EPA REFERENCE METHOD 320 B 2 1.05 0.93 0.964 Average Analyzer NMNEHC Level 88.43 ppm B 3 1.94 0.96 0.980 Calculated NMNEHC Mass Output 0.55 lbs/hr B 4 3.23 0.99 0.995 Calculated NMNEHC Output 0.31 g/bhp-hr B 5 6.77 1.02 1.010 LOAD APPROXIMATION B 6 8.06 0.97 0.985 Estimated Engine Load 800.4 BHP B 7 8.95 0.97 0.985 B 8 9.50 0.95 0.975 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 1.0 1329 0.3 0.986 Average Stack Gas Velocity 101.67 ft/sec Average Dry Flowrate 905.77 dscfm TEST RUN # 2 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 63.952052 35.996397 99.948449 15.238025 90.838841 10.979418 18:52:02 06/19/2024 2 67.449168 37.700383 105.149551 15.541716 89.582107 11.003686 18:53:02 06/19/2024 3 67.665839 37.914203 105.580042 15.532344 88.655536 11.029321 18:54:02 06/19/2024 4 66.946189 37.541149 104.487338 15.425616 88.336879 11.019878 18:55:02 06/19/2024 5 69.636197 38.822841 108.459038 15.821741 87.579007 11.043874 18:56:02 06/19/2024 6 67.22227 37.635823 104.858093 15.484816 87.796985 11.027523 18:57:02 06/19/2024 7 66.625271 37.37967 104.004941 15.534932 88.281046 11.022206 18:58:02 06/19/2024 8 67.146522 37.614979 104.761501 15.578451 89.013006 11.017682 18:59:02 06/19/2024 9 68.327227 38.270707 106.597934 15.63381 87.983698 11.016286 19:00:03 06/19/2024 10 66.380948 37.396831 103.777779 15.472155 87.429594 11.044957 19:01:03 06/19/2024 11 65.102033 36.724374 101.826407 15.39171 86.245727 11.02044 19:02:03 06/19/2024 12 66.684847 37.467786 104.152633 15.646615 86.703867 11.021753 19:03:03 06/19/2024 13 65.765153 36.882995 102.648148 15.444608 86.554362 11.027421 19:04:03 06/19/2024 14 65.415647 36.768607 102.184254 15.609369 87.864903 11.021226 19:05:03 06/19/2024 15 66.730247 37.473753 104.204 15.667276 87.276995 11.042061 19:06:03 06/19/2024 16 68.82558 38.563091 107.388671 15.684169 85.821240 11.018286 19:07:03 06/19/2024 17 69.547355 38.936209 108.483564 15.70333 84.284678 11.060192 19:08:03 06/19/2024 18 68.45202 38.260032 106.712052 15.730705 86.484170 11.032069 19:09:03 06/19/2024 19 69.297306 38.884211 108.181517 15.669564 85.616121 11.028096 19:10:04 06/19/2024 20 67.583704 38.041732 105.625436 15.589586 86.842993 11.031823 19:11:04 06/19/2024 21 66.897662 37.711768 104.60943 15.61604 87.171402 11.024621 19:12:04 06/19/2024 22 67.544392 38.208814 105.753206 15.609412 87.047190 11.050094 19:13:04 06/19/2024 23 65.61899 37.014602 102.633592 15.477834 88.655135 11.050076 19:14:04 06/19/2024 24 65.552567 37.233497 102.786064 15.142389 86.833783 11.039953 19:15:04 06/19/2024 25 65.284528 37.174052 102.45858 15.162598 86.401473 11.042022 19:16:04 06/19/2024 26 64.058452 36.545603 100.604055 14.982457 85.743974 11.047196 19:17:04 06/19/2024 27 67.712324 38.578009 106.290333 15.333281 85.355091 11.078763 19:18:04 06/19/2024 28 64.9759 37.172502 102.148402 15.055588 86.791764 11.063994 19:19:05 06/19/2024 29 65.379111 37.410439 102.78955 15.29283 85.579810 11.055894 19:20:04 06/19/2024 30 64.531421 36.911918 101.443339 15.137246 85.896778 11.05548 19:21:04 06/19/2024 31 65.789645 37.400308 103.189953 15.305187 86.028198 11.08074 19:22:04 06/19/2024 32 65.840672 37.512768 103.35344 15.421363 86.059029 11.077071 19:23:05 06/19/2024 33 63.988144 36.430575 100.418719 15.285525 85.849246 11.059592 19:24:05 06/19/2024 34 64.701483 36.929567 101.63105 15.265201 86.425334 11.053469 19:25:05 06/19/2024 35 65.08748 36.993326 102.080806 15.253841 84.769260 11.073946 19:26:05 06/19/2024 36 64.465045 36.703554 101.168599 15.265777 84.769486 11.064766 19:27:05 06/19/2024 37 65.480961 37.314929 102.79589 15.338255 85.308678 11.060568 19:28:05 06/19/2024 38 64.673978 36.836699 101.510677 15.283295 86.019873 11.081648 19:29:05 06/19/2024 39 65.019378 37.055246 102.074624 15.110833 85.085364 11.072489 19:30:06 06/19/2024 40 64.51557 36.608823 101.124393 15.123602 86.420678 11.045955 19:31:05 06/19/2024 41 65.547492 37.151227 102.698719 15.361283 85.081073 11.044918 19:32:06 06/19/2024 42 64.215089 36.61357 100.828659 15.178599 86.686959 11.053507 19:33:06 06/19/2024 43 67.27562 38.110914 105.386534 15.564503 86.711145 11.080669 19:34:06 06/19/2024 44 64.857752 36.990873 101.848625 15.073 87.214338 11.045657 19:35:06 06/19/2024 45 68.035478 38.573053 106.608531 15.361924 86.874045 11.082999 19:36:06 06/19/2024 46 72.032003 40.429583 112.461586 15.600088 85.711995 11.098215 19:37:06 06/19/2024 47 66.667162 37.844322 104.511484 15.290876 86.981713 11.064706 19:38:06 06/19/2024 48 66.936417 37.830244 104.766661 15.357827 87.351056 11.074755 19:39:06 06/19/2024 49 68.404742 38.830813 107.235555 15.443263 85.583813 11.091133 19:40:06 06/19/2024 50 68.43638 38.849211 107.285591 15.617502 85.771864 11.10714 19:41:06 06/19/2024 51 67.795462 38.595845 106.391307 15.546531 85.964570 11.097828 19:42:06 06/19/2024 52 66.30405 37.801912 104.105962 15.644863 87.247830 11.079719 19:43:06 06/19/2024 53 66.354517 37.743708 104.098225 15.532751 87.652049 11.065025 19:44:06 06/19/2024 54 68.134436 38.849798 106.984234 15.764359 85.627328 11.090996 19:45:07 06/19/2024 55 69.382645 39.291788 108.674433 15.860579 86.805746 11.11015 19:46:07 06/19/2024 56 71.192035 40.341346 111.533381 16.083203 85.225756 11.103042 19:47:07 06/19/2024 57 69.050385 39.372518 108.422903 15.841923 86.651982 11.116753 19:48:07 06/19/2024 58 69.495643 39.603935 109.099578 15.930685 87.179524 11.091082 19:49:07 06/19/2024 59 65.524682 37.62587 103.150552 15.651775 88.690393 11.083851 19:50:07 06/19/2024 60 68.129759 39.009465 107.139224 15.781394 86.315281 11.084128 19:51:07 06/19/2024 AVG 66.76 0.00 104.55 15.47 86.71 11.06 ppm@15% O2 41.68 6.17 34.57 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.38 0.70 0.03 0.06 0.30 0.55 FTIR Measurements #1 Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 3 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 10 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.95 1331 0.35 0.975 Average O2 6.1 (% dry)A 2 1.05 0.99 0.995 Average CO2 6.3 (% dry)A 3 1.94 1.01 1.005 Average N2 + CO 87.6 (% dry)A 4 3.23 1.04 1.020 Dry Molecular Weight 29.25 lb/lbmol A 5 6.77 1.09 1.044 Wet Molecular Weight 28.01 lb/lbmol A 6 8.06 1.06 1.030 EPA REFERENCE METHOD 320 A 7 8.95 1.03 1.015 Barometric Pressure 23.01 in Hg A 8 9.50 1.02 1.010 Moisture Content 11.06 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 104.55 ppm A 11 Calculated NOx Mass Output 0.70 lbs/hr A 12 Calculated NOx Output 0.38 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 15.47 ppm A 15 Calculated CO Mass Output 0.06 lbs/hr A 16 Calculated CO Output 0.03 g/bhp-hr B 1 0.50 0.99 1331 0.35 0.995 EPA REFERENCE METHOD 320 B 2 1.05 0.99 0.995 Average Analyzer NMNEHC Level 86.71 ppm B 3 1.94 1.02 1.010 Calculated NMNEHC Mass Output 0.55 lbs/hr B 4 3.23 1.05 1.025 Calculated NMNEHC Output 0.30 g/bhp-hr B 5 6.77 1.08 1.039 LOAD APPROXIMATION B 6 8.06 1.06 1.030 Estimated Engine Load 828.0 BHP B 7 8.95 1.03 1.015 B 8 9.50 1.02 1.010 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 1.0 1331 0.4 1.013 Average Stack Gas Velocity 104.50 ft/sec Average Dry Flowrate 929.02 dscfm TEST RUN # 3 APPENDIX B Date Time NO 191C span NO2 191C span H2O% (high) 191C Formaldehyde 191C Ethylene 191C TE span Propane 191C span Acetaldehyde 191C span CO ppm 191C (1of2) span CO ppm Dry CO2% 191C NOx Wet NOx Dry NM NE HC C3 Temp ( C )Pressure (atm) 6/19/2024 16:28:06 -0.035552 -0.005362 0.00508 0.079918 -0.620334 1.456193 -0.521584 -0.137808 -0.137815 0.015291 -0.040915 -0.040917 1.316897 191.876404 1.017234 6/19/2024 16:28:13 0.040267 -0.010232 -0.008504 0.211962 -1.030779 -0.870157 0.835251 -0.012499 -0.012498 -0.014045 0.030035 0.030033 2.913897 191.871567 1.01949 6/19/2024 16:28:21 0.376617 -0.068138 -0.009253 -0.023375 -0.150541 -0.271051 0.786469 0.162244 0.162229 0.001243 0.308479 0.30845 0.04073 191.886093 1.02073 6/19/2024 16:28:28 0.024404 0.024234 0.007907 0.061342 -0.102266 -0.190364 0.709904 0.040773 0.040776 -0.005767 0.048638 0.048642 0.080134 191.842484 1.017563 6/19/2024 16:29:07 0 0 0 0 0 0 0 0 0 0 0 0 0 191.864075 0.999965 6/19/2024 16:29:21 -0.035107 0.083912 -0.002047 -0.093456 -0.166163 -0.288727 0.310535 -0.390109 -0.390101 0.009189 0.048805 0.048804 -0.007712 191.825531 0.995277 6/19/2024 16:29:29 0.099913 0.0008 -0.002363 -0.068939 1.003298 -0.119532 0.727881 -0.130873 -0.13087 0.008912 0.100713 0.100711 0.011255 191.769806 0.999936 6/19/2024 16:29:36 0.051793 0.091442 -0.001889 -0.115348 1.364412 -0.97743 0.987795 0.159975 0.159972 0.002306 0.143235 0.143233 0.057179 191.638992 0.999569 6/19/2024 16:29:44 0.011169 0.096451 -0.00052 -0.052472 1.427838 -1.280551 -0.206459 -0.235207 -0.235206 -0.00811 0.10762 0.107619 0.05683 191.595383 1.000395 6/19/2024 16:29:51 0.110188 0.058589 -0.007928 -0.063737 0.351025 -0.695395 -1.54357 -0.186874 -0.186859 0.001345 0.168778 0.168764 0.01014 191.508163 0.998972 6/19/2024 16:29:59 0.140038 0.088804 0.002374 0.044896 -0.540222 -0.839619 -0.39248 -0.017629 -0.017629 -0.009887 0.228842 0.228848 0.000004 191.464554 1.001726 6/19/2024 16:30:06 0.055284 0.058202 0.006704 -0.05505 0.2248 -0.802457 0.0591 -0.234951 -0.234967 -0.008601 0.113486 0.113493 0.004526 191.384613 1.000257 6/19/2024 16:30:14 -0.144046 0.129717 0.004445 0.000737 0.115254 -0.860524 -0.461643 0.219085 0.219095 0.010152 -0.014329 -0.01433 0.022289 191.348282 0.997136 6/19/2024 16:30:22 -0.192748 -0.021684 -0.012723 0.147506 1.442087 -0.716175 -0.693978 -0.066492 -0.066484 -0.00159 -0.214432 -0.214405 0.070468 191.362808 0.996998 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 16:31:11 520.540921 496.539617 499.497675 191.706818 0.988422 6/19/2024 16:34:53 98.920564 192.130783 0.990564 6/19/2024 16:31:19 519.654164 495.908983 494.618553 191.75528 0.989838 6/19/2024 16:35:01 97.76867 192.0896 0.993234 6/19/2024 16:31:27 518.486163 495.423514 492.837345 191.75528 0.991444 6/19/2024 16:35:08 99.437802 192.04599 0.990756 6/19/2024 16:31:34 520.427491 496.829937 497.856759 191.842484 0.98869 6/19/2024 16:35:16 98.708819 192.0896 0.991811 6/19/2024 16:31:42 519.44025 494.597677 496.167202 191.886093 0.993143 6/19/2024 16:35:23 98.012825 192.075058 0.992179 6/19/2024 16:31:49 523.204062 498.616515 498.889931 191.871567 0.98511 6/19/2024 16:35:31 98.768053 192.0896 0.992638 6/19/2024 16:31:57 522.663513 498.139762 497.248439 191.931519 0.986682 6/19/2024 16:35:38 97.746377 192.104126 0.993418 6/19/2024 16:32:04 521.771744 497.831515 500.537221 191.987854 0.989287 6/19/2024 16:35:46 99.151528 192.071426 0.987485 6/19/2024 16:32:12 520.280554 496.760541 496.207249 191.987854 0.990939 6/19/2024 16:35:53 100.236604 192.0896 0.989379 6/19/2024 16:32:19 521.269031 495.816655 491.347756 192.00238 0.993326 6/19/2024 16:36:01 97.945603 192.0896 0.990343 6/19/2024 16:36:08 98.687908 192.071426 0.985919 Date Time NO2 191C span Temp ( C )Pressure (atm) 6/19/2024 16:32:55 146.324949 192.027496 0.976831 6/19/2024 16:33:03 146.919218 192.071426 0.97881 6/19/2024 16:33:11 146.985895 192.0896 0.980244 6/19/2024 16:33:18 147.617443 192.0896 0.978362 6/19/2024 16:33:25 146.745059 192.0896 0.991077 6/19/2024 16:33:33 147.969215 192.04599 0.986992 6/19/2024 16:33:40 147.703324 192.058716 0.98857 6/19/2024 16:33:48 147.5461 192.118668 0.988966 6/19/2024 16:33:55 147.426251 192.220413 0.989884 6/19/2024 16:34:03 147.980428 192.176819 0.985569 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 16:36:41 494.821498 474.547535 475.819797 192.122299 0.962931 6/19/2024 16:38:44 98.2975 192.139267 0.958379 6/19/2024 16:36:49 509.774864 490.323709 495.607405 192.075058 0.957981 6/19/2024 16:38:52 98.730666 192.060532 0.972532 6/19/2024 16:36:56 507.698352 486.940918 488.188149 192.133209 0.980611 6/19/2024 16:38:59 98.737327 192.104126 0.987175 6/19/2024 16:37:04 521.011868 498.341592 494.892056 192.118668 0.999385 6/19/2024 16:39:06 99.146511 192.04599 0.987772 6/19/2024 16:37:11 521.437777 496.951362 497.575713 192.135025 1.000498 6/19/2024 16:39:14 98.671921 192.04599 0.989057 6/19/2024 16:37:19 520.079261 496.914866 496.24142 192.162277 1.001038 6/19/2024 16:39:22 100.342487 192.033264 0.989293 6/19/2024 16:37:26 521.561284 495.895225 495.626919 192.133209 1.002185 6/19/2024 16:39:29 97.772775 192.031448 0.994015 6/19/2024 16:37:34 523.83412 497.960607 499.435821 192.104126 0.998284 6/19/2024 16:39:37 96.937361 192.04599 0.996264 6/19/2024 16:37:41 521.469748 496.39953 493.989182 192.118668 1.001634 6/19/2024 16:39:44 98.004737 192.075058 0.995392 6/19/2024 16:37:49 521.332706 497.820806 499.427616 192.162277 1.000854 6/19/2024 16:39:52 98.917044 192.04599 0.995071 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 16:40:14 0.047753 -0.070763 -0.323077 0.857729 192.04599 1.003057 6/19/2024 16:40:22 -0.321965 0.184316 -1.27041 -0.124683 192.075058 1.005949 6/19/2024 16:40:29 0.011824 0.166468 0.229078 0.862305 192.04599 1.008015 6/19/2024 16:40:37 0.462014 0.00638 -0.419395 0.110248 192.118668 1.002415 6/19/2024 16:40:44 0.058952 0.200221 -1.007701 -0.067542 192.104126 1.010402 6/19/2024 16:40:52 -0.095457 -0.066977 0.153269 0.700708 192.133209 1.010907 6/19/2024 16:40:59 -0.006058 0.092397 -1.550356 0.196198 192.198608 1.010299 6/19/2024 16:41:07 0.179637 0.319123 -0.191053 0.386251 192.205887 1.011871 Raw Calibration Data BACKGROUND / PRE DIRECT ZERO PRE DIRECT CAL NO2 CAL PRE SYSTEM CAL PRE SYSTEM ZERO Date Time CO2% 191C Propane 191C span Temp ( C )Pressure (atm) 6/19/2024 16:44:56 6.385008 57.035265 192.257965 0.982237 6/19/2024 16:45:04 6.344377 57.933937 192.278564 0.984559 6/19/2024 16:45:11 6.356373 59.611333 192.278564 0.983595 6/19/2024 16:45:19 6.323521 59.85675 192.234955 0.985064 6/19/2024 16:45:26 6.281254 57.896892 192.249496 0.99553 6/19/2024 16:46:19 6.269489 62.166829 192.096863 0.999621 6/19/2024 16:46:27 6.264315 60.68006 192.029037 0.99774 6/19/2024 16:46:34 4.166005 43.328771 192.04599 1.003792 6/19/2024 16:46:41 3.494113 138.584934 192.058716 1.006162 6/19/2024 16:46:49 3.46834 240.609594 192.031448 1.002782 6/19/2024 16:46:56 3.471675 243.34325 192.00238 1.003654 6/19/2024 16:47:04 3.997462 201.63215 192.031448 1.008015 6/19/2024 16:47:12 5.697536 101.743514 192.020554 0.999816 6/19/2024 16:48:04 5.715926 98.979503 191.97554 1.001382 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 19:56:14 524.514401 496.860738 488.144041 192.291885 1.015279 6/19/2024 19:54:32 96.189358 192.181656 0.982906 6/19/2024 19:56:22 526.276079 498.755301 490.136406 192.307632 1.013799 6/19/2024 19:54:39 100.083519 192.234955 0.979647 6/19/2024 19:56:29 527.81868 501.098006 492.079222 192.278564 1.009346 6/19/2024 19:54:47 99.074611 192.162277 0.97749 6/19/2024 19:56:37 524.635818 497.387543 493.327448 192.264023 1.016186 6/19/2024 19:54:54 98.640516 192.220413 0.979142 6/19/2024 19:56:44 526.632002 499.146529 494.347304 192.220413 1.011641 6/19/2024 19:55:02 99.796458 192.220413 0.985431 6/19/2024 19:56:52 522.723726 496.749469 490.804035 192.191345 1.015818 6/19/2024 19:55:09 99.307363 192.278564 0.98892 6/19/2024 19:56:59 523.775541 497.045695 493.839564 192.249496 1.017127 6/19/2024 19:55:17 99.367543 192.278564 0.985156 6/19/2024 19:57:07 524.58249 498.545358 491.970394 192.264023 1.014717 6/19/2024 19:55:24 99.589134 192.274933 0.984312 6/19/2024 19:57:14 523.321409 497.456265 488.97963 192.278564 1.016553 6/19/2024 19:55:32 100.073068 192.278564 0.989516 6/19/2024 19:57:22 526.649937 499.819428 500.255816 192.234955 1.012789 6/19/2024 19:55:39 98.517749 192.264023 0.999982 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 19:54:47 -0.287479 0.174254 -1.225989 192.162277 0.97749 6/19/2024 19:58:11 -0.254316 192.3367 1.001359 6/19/2024 19:54:54 -0.492848 0.060661 -0.917033 192.220413 0.979142 6/19/2024 19:58:19 1.741042 192.293091 1.000625 6/19/2024 19:55:02 -0.55856 0.413771 -2.419934 192.220413 0.985431 6/19/2024 19:58:27 0.056311 192.249496 0.99596 6/19/2024 19:55:09 -0.421869 0.361699 -1.351614 192.278564 0.98892 6/19/2024 19:58:34 -1.092947 192.283401 0.99608 6/19/2024 19:55:17 -0.240079 0.259038 -1.684758 192.278564 0.985156 6/19/2024 19:58:41 -1.390485 192.31308 0.999575 6/19/2024 19:55:24 -0.410211 0.060733 -1.698643 192.274933 0.984312 6/19/2024 19:58:49 0.770161 192.322174 0.999523 6/19/2024 19:55:32 -0.644723 0.297571 -0.873306 192.278564 0.989516 6/19/2024 19:58:56 -0.146136 192.3367 0.999202 6/19/2024 19:55:39 -0.151063 0.220589 -2.094374 192.264023 0.999982 6/19/2024 19:59:04 -0.82134 192.322174 0.999523 SAMPLE SPIKE RECOVERY POST SYSTEM CAL POST SYSTEM ZERO PRE TEST 1 495.6 6.3 57.9 5.7 101.7 0.093 86.4% Sensor Analyzer Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Error (%)Error (%) NOx 495.8 493.4 0.1 0.49 0.02 CO 521.3 520.2 -0.1 0.21 -0.02 Propane 491.3 495.6 -0.7 -0.86 -0.15 Ethylene 99.4 101.9 0.5 -2.42 0.46 Sensor System Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%) NOx 497.8 493.4 0.1 0.90 0.01 CO 521.3 520.2 0.0 0.22 0.00 Propane 499.4 495.6 -0.6 0.77 -0.12 Ethylene*98.9 101.9 0.4 -2.93 0.36 Sensor System Cal Zero Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%)Drift Error (%)Drift Error (%) NOx 499.8 493.4 0.2 1.30 0.05 0.41 0.03 CO 526.6 520.2 -0.4 1.24 -0.08 1.02 0.09 Propane 500.3 495.6 -1.5 0.94 -0.29 0.17 0.17 Ethylene*98.5 101.9 -0.2 -3.32 -0.18 0.39 0.54 *CTS Scans are conducted with Ethylene through the sample line. Lf 5.11 Lr Cr Tr Pr Lr/Lf 5.31 99.4 192.0 1.0 1.04 Ls Cs Ts Ps Ls/Lf 5.32 98.9 192.0 1.0 1.04 % Recovery Propane PRE DIRECT CAL FTIR QA/QC SUMMARY SAMPLE RECOVERY CALCULATIONS Period Spike #Concentration of Propane Cylinder Stack CO2 Concentration Pathlength Stack Propane Concentration Stack + Spike CO2 Concentration Stack + Propane Concentration DF Calculated POST SYSTEM CAL PRE SYSTEM CAL CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number:E02NI99E15W0051 Reference Number:153-402577489-1 Cylinder Number:CC486070 Cylinder Volume:144.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG PGVP Number:B72022 Valve Outlet:660 Gas Code:NO2,BALN Certification Date:Nov 08, 2022 Expiration Date:Nov 08, 2025 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates NITROGEN DIOXIDE 150.0 PPM 146.6 PPM G1 +/- 2.0% NIST Traceable 11/01/2022, 11/08/2022 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 15340120215 CC511005 59.52 PPM NITROGEN DIOXIDE/NITROGEN 1.4%Dec 17, 2024 PRM 12397 D887665 74.2 PPM NITROGEN DIOXIDE/AIR 1.3%Feb 02, 2022 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration MKS FTIR NO2 018143349 FTIR Nov 01, 2022 Triad Data Available Upon Request PERMANENT NOTES:OXYGEN ADDED TO MAINTAIN STABILITY Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD Part Number:X02NI99P15AD524 Reference Number:153-402622613-1 Cylinder Number:CC173895 Cylinder Volume:140.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG Analysis Date:Dec 22, 2022 Valve Outlet:350 Lot Number:153-402622613-1 Expiration Date:Dec 22, 2025 Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. ANALYTICAL RESULTS Component Req Conc Actual Concentration Analytical (Mole %)Uncertainty ETHYLENE 100.0 PPM 101.9 PPM +/- 1% NITROGEN Balance Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 Finely – North Randlett 6-19-2024 Finely – North Randlett 6-19-2024 Finely – North Randlett 6-19-2024 Spectral Fit Run 1 Spectral Fit Run 2 Spectral Fit Run 3 Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000141.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000075.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000076.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 54.55 3.4 -0.24 0.33 4.63 4.63 -1.9 --0-2795 1.05 Good NO2 191C 33.51 0.51 -0.03 0.03 0.54 0.54 -0.67 --0-488 1.06 Good N2O 191C 0.4 0.36 0.57 0.03 0.03 0.41 0.41 0.69 0.69 0.12 0.19 0-200 -Close to DL NH3 TE 191C 7.98 40.98 9.25 4.14 7.06 69.94 69.94 10.4 36.83 1.15 3.08 0-2995 -Close to DL H2O% (HIGH) 191C10.95 0.26 -0.02 0.03 0.42 0.42 -0.22 --0-40 -Good FORMALDEHYDE 191C2.82 0.97 2.9 0.24 0.27 1.1 1.1 3.18 3.19 0.29 0.97 0-69 -Close to DL FORMIC ACID 191C TE3.7 15.38 4.82 1.56 1.83 18.01 18.01 6.04 13.77 1.23 1.61 0-466 -Close to DL CH4 2900 CM-1 191C1180.54 35.87 -1.69 2.46 66.46 66.46 -23.61 --0-3143 1 Good PROPANE 191C56.06 1.9 -0.22 0.27 2.29 2.29 -1.12 --0-4976 0.95 Good PROPYLENE 191C TE4.88 14.9 4.56 1.57 1.86 17.63 17.63 5.41 13.21 0.85 1.52 0-194 -Close to DL ETHANE 191C112.28 4.25 -0.55 0.85 6.62 6.62 -2.27 --0-1004 -Good ETHYLENE 191C TE16.16 24.61 17.04 2.07 2.55 29.63 29.63 19.34 22.12 2.3 5.68 0-900 -Close to DL CO PPM 191C (1OF2)13.07 0.99 -0.26 0.57 1.83 1.83 -0.43 --0-5010 1.05 Good CO2% 191C 6.27 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.38 2.56 1.66 0.64 0.82 3.29 3.29 1.96 1.96 0.3 0.55 0-186 1 Close to DL ACETYLENE 191C0.06 4.6 1.15 0.79 1.05 6.07 6.07 1.17 3.85 0.02 0.38 0-1016 -Close to DL SO2 191C 2.2 2.44 2.74 0.26 0.32 2.98 2.98 2.94 2.94 0.2 0.91 0-964 1.02 Close to DL HEXANE 191C 5.51 1.35 5.94 0.13 0.18 1.82 1.82 6.65 6.66 0.71 1.98 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000202.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000075.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000076.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 55.91 3.31 -0.24 0.33 4.5 4.5 -1.81 --0-2795 1.05 Good NO2 191C 34.62 0.52 -0.03 0.03 0.55 0.55 -0.69 --0-488 1.06 Good N2O 191C 0.42 0.34 0.57 0.03 0.03 0.39 0.39 0.69 0.69 0.12 0.19 0-200 -Close to DL NH3 TE 191C 7.22 38.99 9.25 4.14 7.06 66.55 66.55 10.4 34.86 1.15 3.08 0-2995 -Close to DL H2O% (HIGH) 191C11 0.26 -0.02 0.03 0.42 0.42 -0.22 --0-40 -Good FORMALDEHYDE 191C2.89 0.94 2.9 0.24 0.27 1.06 1.06 3.18 3.19 0.29 0.97 0-69 -Close to DL FORMIC ACID 191C TE2.35 15 4.82 1.56 1.83 17.56 17.56 6.04 13.43 1.23 1.61 0-466 -Close to DL CH4 2900 CM-1 191C1170.98 35.39 -1.69 2.46 65.56 65.56 -23.42 --0-3143 1 Good PROPANE 191C55.39 1.83 -0.22 0.27 2.2 2.2 -1.11 --0-4976 0.95 Good PROPYLENE 191C TE4.93 14.52 4.56 1.57 1.86 17.18 17.18 5.41 12.83 0.85 1.52 0-194 -Close to DL ETHANE 191C 112.3 4.15 -0.55 0.85 6.46 6.46 -2.26 --0-1004 -Good ETHYLENE 191C TE15.74 23.87 17.04 2.07 2.55 28.74 28.74 19.34 21.39 2.3 5.68 0-900 -Close to DL CO PPM 191C (1OF2)13.63 1.03 -0.26 0.57 1.91 1.91 -0.46 --0-5010 1.05 Good CO2% 191C 6.3 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.26 2.48 1.66 0.64 0.82 3.18 3.18 1.96 1.96 0.3 0.55 0-186 1 Close to DL ACETYLENE 191C0.13 4.41 1.15 0.79 1.05 5.83 5.83 1.17 3.66 0.02 0.38 0-1016 -Close to DL SO2 191C 2.71 2.58 2.74 0.26 0.32 3.15 3.15 2.94 2.94 0.2 0.91 0-964 1.02 Close to DL HEXANE 191C 5.32 1.31 5.94 0.13 0.18 1.78 1.78 6.65 6.66 0.71 1.98 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000263.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000075.LAB C:\OLT\Data\Finley Resources\Finley NR CS E1 6-19-24\FINLEY NR CS E1 6-19-24_000076.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 58.3 3.29 -0.24 0.33 4.47 4.47 -1.76 --0-2795 1.05 Good NO2 191C 36 0.53 -0.03 0.03 0.56 0.56 -0.72 --0-488 1.06 Good N2O 191C 0.45 0.34 0.57 0.03 0.03 0.4 0.4 0.69 0.69 0.12 0.19 0-200 -Close to DL NH3 TE 191C 7.98 38.51 9.25 4.14 7.06 65.72 65.72 10.4 34.36 1.15 3.08 0-2995 -Close to DL H2O% (HIGH) 191C11.09 0.26 -0.02 0.03 0.43 0.43 -0.22 --0-40 -Good FORMALDEHYDE 191C3.01 0.9 2.9 0.24 0.27 1.01 1.01 3.18 3.19 0.29 0.97 0-69 -Close to DL FORMIC ACID 191C TE2.33 14.6 4.82 1.56 1.83 17.09 17.09 6.04 13.03 1.23 1.61 0-466 -Close to DL CH4 2900 CM-1 191C1187.28 42.63 -1.69 2.46 78.97 78.97 -24.35 --0-3143 1 Good PROPANE 191C53.13 1.8 -0.22 0.27 2.16 2.16 -1.06 --0-4976 0.95 Good PROPYLENE 191C TE4.48 14.27 4.56 1.57 1.86 16.88 16.88 5.41 12.59 0.85 1.52 0-194 -Close to DL ETHANE 191C 109.3 4.01 -0.55 0.85 6.24 6.24 -2.2 --0-1004 -Good ETHYLENE 191C TE15.46 23.79 17.04 2.07 2.55 28.65 28.65 19.34 21.33 2.3 5.68 0-900 -Close to DL CO PPM 191C (1OF2)13.95 0.97 -0.26 0.57 1.79 1.79 -0.41 --0-5010 1.05 Good CO2% 191C 6.32 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.55 2.26 1.66 0.64 0.82 2.9 2.9 1.96 1.96 0.3 0.55 0-186 1 Close to DL ACETYLENE 191C0.13 4.55 1.15 0.79 1.05 6.01 6.01 1.17 3.8 0.02 0.38 0-1016 -Close to DL SO2 191C 1.74 2.28 2.74 0.26 0.32 2.78 2.78 2.94 2.94 0.2 0.91 0-964 1.02 Close to DL HEXANE 191C 5.15 1.29 5.94 0.13 0.18 1.75 1.75 6.65 6.66 0.71 1.98 0-1000 -Close to DL APPENDIX C Test Run Load %Site Rated Load, bhp Load Approx., bhp 1 58 1380 800.4 2 58 1380 800.4 3 60 1380 828.0 Engine Load Approximation based on Panel Levels APPENDIX D Test Run Flowrate dscfm Approx. BHP Avg O2 % NOx ppmvd NOx g/bhp-hr NOx lbs/hr CO ppmvd CO g/bhp-hr CO lbs/hr NMNEHC ppmvd NMNEHC g/bhp-hr NMNEHC lbs/hr Moisture Content % 1 913.78 800.4 5.6 94.18 0.35 0.62 14.82 0.03 0.06 94.80 0.34 0.59 10.93 2 905.77 800.4 6.0 100.97 0.37 0.65 15.19 0.03 0.06 88.43 0.31 0.55 10.99 3 929.02 828.0 6.1 104.55 0.38 0.70 15.47 0.03 0.06 86.71 0.30 0.55 11.06 809.6 5.9 99.90 0.37 0.66 15.16 0.03 0.06 89.98 0.32 0.57 10.99 Summary Average Levels Example Calculations: Uinta Wax Operating, LLC, North Randlett Compressor Station, #1 The following is a step-by-step calculation for the first test run conducted on the North Randlett Compressor Station #1. Test Parameters • Stack Diameter = 10 inches • Traverse Points = 16 • Ports = 2 • Barometric Pressure = 23.01 in Hg • Average O2 = 5.6% • Average CO2 = 6% • Load Approximation = 800.4 bhp • Moisture Content = 10.93% EPA 40 CFR 60(A) Methods 1-3: Determination of Stack Gas Velocity and Flow Rate Dry Molecular Weight (lb/lbmol) = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) Where: %CO2 – Carbon Dioxide Content Of The Gas = 6% %O2 – Oxygen Content Of The Gas = 5.6% %N2 – Nitrogen Content Of The Gas %CO – Carbon Monoxide Content Of The Gas (%N2 +%CO) = (100 - %O2 - %CO2) = (100 – 5.6 – 6) = 88.4% Dry = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) = (0.44 * 6) + (0.32 * 5.6) + (0.28 * 88.4) = 29.18 lb/lbmol Wet Molecular Weight (lb/lbmol) = MD * (1-BWS) + (18) * BWS Where: MD – Molecular Weight Of The Dry Gas (lb/lbmol) = 29.18 lb/lbmol BWS – Moisture Content Of The Gas (%/100) = 10.93% = MD * (1-BWS) + (18) * BWS = 29.18 * (1 – (10.93/ 100)) + (18 * (10.93/ 100)) = 27.96 lb/lbmol Average Stack Gas Velocity (ft/sec) = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) Where: CP – Pitot tube constant (unitless) = 0.84 ∆PAVG – Average square root of the stack gas pitot DP (inches water) = 0.991 in H2O TS – Average stack temperature (R) = 1323 R PB – Barometric pressure (in Hg) = 23.01 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.4 in H2O MA – Molecular weight of the wet gas (lb/lbmol) = 27.96 lb/lbmol = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) = 0.84 * (85.49) * 0.991 * ( 1323 / (((0.4/ 13.6) + 23.01) * 27.96)) = 102.03 ft/sec Average Dry Flowrate (dscfm) = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 Where: DS – Diameter of the stack (inches) = 10 inches BWS – Moisture content of the gas (%) = 10.93% TSTD – Standard temperature (528R) TS – Average stack temperature (R) = 1323 R PB – Barometric pressure (in Hg) = 23.01 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.4 in H2O VS– Average Stack gas velocity (ft/sec) = 102.03 ft/sec = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 = 60 * (1 - (10.93/ 100)) * 102.03 * * (((10 / 2) / 12))2) * 528 / 1323 * (23.01 + (0.4 / 13.6)) / 29.92 = 913.78 dscfm Conversion of Dry Flowrate to m3/hr = Q * 60 * 2.83168*10 -2 Where: Q – Volumetric Flowrate = 913.78 dscfm 2.83168*10 -2 – Conversion factor for cubic feet to cubic meter 60 – Minutes in an hour = Q * 60 * 2.83168*10 -2 = 913.78 *60 * 2.83168*10 -2 = 1552.52 m3/hr ASTM D 6348-03: Determination of NOx, CO and VOC Emissions From Stationary Sources NOx Emission Rate (g/Bhp-hr) = (Cd * 1.912*10 -3 * Q * T) / HP-hr Where: Cd – Measured NOx concentration in ppm = 94.18 ppm 1.92*10 -3 - Conversion constant for ppm to g/m3 NOx Q – Volumetric Flowrate = 1552.52 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 800.4 Bhp = (Cd * 1.912*10 -3 * Q * T) / HP-hr = (94.18 * 1.912*10 -3 * 1552.52 * 1) / 800.4 = 0.35 g/Bhp-hr NOx Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.35 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 800.4 Bhp = g/Bhp-hr / 454 * Bhp = 0.35 / 454 * 800.4 = 0.62 lbs/hr CO Emission Rate (g/Bhp-hr) = (Cd * 1.164*10 -3 * Q * T) / HP-hr Where: Cd – Measured CO concentration in ppm = 14.82 ppm 1.164*10 -3 - Conversion constant for ppm to g/m3 CO Q – Volumetric Flowrate = 1552.52 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 800.4 Bhp = (Cd * 1.164*10 -3 * Q * T) / HP-hr = (14.82 * 1.164*10 -3 * 1552.52 * 1) / 800.4 = 0.03 g/Bhp-hr CO Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.03 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 800.4 Bhp = g/Bhp-hr / 454 * Bhp = 0.03 / 454 * 800.4 = 0.06 lbs/hr VOC Emission Rate (g/Bhp-hr) = (Cd * 1.833*10 -3 * Q * T) / HP-hr Where: Cd – Measured VOC concentration in ppm = 94.80 ppm 1.833*10 -3 - Conversion constant for ppm to g/m3 VOC Q – Volumetric Flowrate = 1552.52 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 800.4 Bhp = (Cd * 1.833*10 -3 * Q * T) / HP-hr = (94.80 * 1.833*10 -3 * 1552.52 * 1) / 800.4 = 0.34 g/Bhp-hr VOC Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.34 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 800.4 Bhp = g/Bhp-hr / 454 * Bhp = 0.34 / 454 * 800.4 = 0.59 lbs/hr APPENDIX E FTIR Engine Test Sheet Company Name Location / Unit I.D. F\I\\e " #nr.A... Y.! a.A 6\c,.\-\L~ ~,1 Type of Test Completed 3x'lhr A/("v Field Technician (s) David Martinez Client Rep and/or State Rep K\lI,,1 3;l'hn Date h-Iq~).t.f Non-Resettable Run Time Hours -:)"l.\ YO Engine Make L-A T Engine Model (1\ ' ,~\~~ Engine SIN tVliJ ltV /'1t;,t,( () 00'1 S Port Distance A ~~ " Port Distance B StAt Exhaust Diameter (inches) -'0\\ Calibration Gas CYlinder # Concentration NO (ppm CC453965 493.4 CO (ppm) CC453965 520.2 Propane (ppm) CC453965 495.6 N02 (ppm) CC486070 146.6 Ethylene ppm CC173895 101.9 Methane (ppm CC453965 499.4 Acetalpehvde ppm) CC321163 196.7 Test 1 Test 2 Time of Reading Y:~I~ S:50 Atm Pressure in Hg) ~\,ol d..~,O\ Atm Temp CF ,ct 70( Engine RPM ~ ld.Y~ \~~), *Manifold Pres. Vae(") or Elc:f<>st(pSi) or Boost (psia) ~S il( Manifold Temp CF) -\?H \j, liS Psuction (psi) Stage 1 Pi \'1 Tsuction ('F) Stage 1 --Pdischar( e (psi) Stage 1 £4 it Psuction (psi) Stage 2 \ \ Tsuction 'F) Stage 2 I Pdischarc e (psi) Staae 2 CA.. 0 lS' ~~() Psuction (psi) Stage 3 Tsuction OF) Stage 3 Pdischar e (psi) StaQe 3 t, \ 6")\ Psuction (psi) Staae 4 \ \ Tsuction 'F) Stage 4 I Pdischarge (psi) Stage 4 \ Gas Throughput (mmef/d) or ( VY\ FF ) Lf,.Jj.,r J",\~ a..~ 1 Pre Cat Temp CF) 'k 1 Post Cat Temp CF) 5? ,2> Cat Differential Pres. (n of H2O) \, Humidity% \5 I'02% ~,t ~, 0 C02 % Dr _ ..., ,0 ].0 LOAD% Panel) or (Estimated) S~ S;:, Ignition Tir rrng-rF) ~ .\ ~\,' AFR SettinQ mV/~;[nk) ~G\.\ ~'l,l AFR Setting mV ank) ~'" Stack Diagram .'~y.,""",;"~x_,., ..,,,·,· ",.,-...",,,,,-.,~,,,,,,,,,,,. ;,.......:....'o/';,.:...~;;-~'" . .....".." Test 3 (P:~t ~~,o\ -1~' \~S ~S \?>g 1'1 - '70 , ri..lO \ \ f>' 0 \ \ I d-..~_~ 'ir~ I ~-I \'d, h.\ "7. I ,(,0 '~.:d. ,0 '~'t.)- \ COSo ~6Cf ,A 'T "<{.i","'" .. , '% ",.. l lI·····~~:~J•• 'A' t J. '8' '.' RevS • Some units show boost in inches of Hg. In this situation please indicate if it is positive (+) or negative(-). Eg: (+12") or (-5") 9/17/2019 Worksheet: O2 Stratification Client:Finley Location:North Randlett E1 Date:6/19/2024 PD:10 DD:32 YES Method 1 Criteria Met UD:96 YES Method 1 Criteria Met Port Point Insertion Depth Reading (inches)(%) A 1 1.66 5.60 A 2 5.00 6.00 A 3 8.33 6.10 A 4 A 5 A 6 A 7 A 8 A 9 A 10 A 11 A 12 Average 5.90 Notes: To demonstrate non-stratified flow and utilize one sampling location O2 may not deviate by more than +/- 0.3% of the average O2 concentration. EPA REFERENCE METHOD 3A (Determination Of Stratification) COMPANY NAME:Finley COMPANY LOCATION:North Randlett E1 DATE:6/19/2024 STACK DIAMETER (inches):10 TRAVERSE POINTS:16 2 TEST RUN #1 TEST RUN #2 TEST RUN #3 AVERAGE O2:5.6 AVERAGE O2:6 AVERAGE O2:6.1 AVERAGE CO2:6 AVERAGE CO2:6.2 AVERAGE CO2:6.3 BARO PRESSURE:23.01 BARO PRESSURE:23.01 BARO PRESSURE:23.01 Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O) 1 0.5 0.93 863 0.35 1 0.5 0.91 869 0.34 1 0.5 0.95 871 0.35 2 1.05 0.95 2 1.05 0.95 2 1.05 0.99 3 1.94 0.99 3 1.94 0.97 3 1.94 1.01 4 3.23 1.01 4 3.23 1.02 4 3.23 1.04 5 6.77 1.04 5 6.77 1.08 5 6.77 1.09 6 8.06 0.99 6 8.06 1.02 6 8.06 1.06 7 8.95 0.97 7 8.95 0.98 7 8.95 1.03 8 9.5 0.94 8 9.5 0.96 8 9.5 1.02 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 1 0.5 0.94 863 0.35 1 0.5 0.89 869 0.34 1 0.5 0.99 871 0.35 2 1.05 97 2 1.05 0.93 2 1.05 0.99 3 1.94 0.99 3 1.94 0.96 3 1.94 1.02 4 3.23 1.03 4 3.23 0.99 4 3.23 1.05 5 6.77 1.06 5 6.77 1.02 5 6.77 1.08 6 8.06 1 6 8.06 0.97 6 8.06 1.06 7 8.95 0.96 7 8.95 0.97 7 8.95 1.03 8 9.5 0.96 8 9.5 0.95 8 9.5 1.02 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 Source Test Report For Uinta Wax Operating, LLC North Randlett Compressor Station Uintah County, Utah Test Date: June 19, 2024 Report Date: July 2, 2024 UDEQ Permit: #DAQE-AN159380002-23 Engine: Caterpillar G3516B SN: JEF01814 Unit ID: #2 Prepared By: Oasis Emission Consultants, Inc. 2730 Commercial Way Rock Springs, WY 82901 July 2, 2024 Ms. Karen Pratt Uinta Wax Operating, LLC Dear Ms. Pratt: Re: Engine Emission Testing For Uinta Wax Operating, LLC, North Randlett Compressor Station, Unit #2, Permit #DAQE-AN159380002-23. An air emissions test program was conducted on a Caterpillar G3516B engine, operated by Uinta Wax Operating, LLC and designated as Unit #2, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC). Oasis Emission Consultants, Inc. conducted the testing on June 19, 2024. UDEQ Permit #DAQE-AN159380002-23 Emission Levels The average recorded levels were found to comply with emission levels stipulated in the permit, as shown in the attached report and summarized below. Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC ppm @ 15% O2 32.84 41 1.50 61 28.56 60 lbs/hr 0.99 1.52 0.03 1.37 0.83 2.13 *VOC levels reported as non-methane, non-ethane hydrocarbon on a propane basis (NMNEHC C3). EPA 40 CFR 60, Subpart JJJJ Emission Levels Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC g/bhp-hr 0.47 1.0 0.01 2.0 0.39 0.7 Catalyst Parameters (Averaged Over 3 Test Runs) Inlet Temp (deg F) DP (in H2O) 1126 4.9 Engine Load (Averaged Over 3 Test Runs) Rated BHP Operating BHP % Load 1380 966.0 70.0 Testing Protocol The attached report was generated using an extractive FTIR system using methodologies as required by and in accordance with EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, as outlined in the submitted Source Test Protocol. Quality Assurance Oasis has performed a full review of the raw data and calculated results in this report. Any errors we have encountered have been listed in the body of this report. After performing the review, we are confident that this engine has met all requirements. If you have any questions or require further information, please contact the undersigned at (307) 382-3297. Yours truly, Oasis Emission Consultants, Inc. _________________________ _______________________ Charles A. Chapman Crystal Leonard Manager of Technical Services Senior EHS Specialist _________________________ Christopher N. Knott, P.Eng. Director, Engineering and Operations SOURCE EMISSION TEST REPORT UDEQ Permit #DAQE-AN159380002-23 Test Performed By: Oasis Emission Consultants, Inc. Test Company Contact: Chris Knott 2730 Commercial Way Rock Springs, WY 82901 307.382.3297 Owner/Operator: Uinta Wax Operating, LLC Owner/Operator Contact: Karen Pratt (720) 990-9927 Facility Name: North Randlett Compressor Station UTM Coordinates: 593,702 m Easting, 4,453,005 m Northing UTM Zone 12 Uintah County, Utah Emission Source: Caterpillar G3516B Unit #2 Date of Test: June 19, 2024 Date of Report: July 2, 2024 TABLE OF CONTENTS 1.1 Introduction .......................................................................................................................... 1 2.1 Stack Sampling Location ..................................................................................................... 2 3.1 Discussion of NOx, CO and VOC Test Results ................................................................... 3 3.1.1 Source Test 1 ............................................................................................................................................ 3 3.1.2 Source Test 2 ............................................................................................................................................ 3 3.1.3 Source Test 3 ............................................................................................................................................ 3 4.1 Stack Sampling Methods and Procedures ............................................................................ 4 4.2 Equipment Utilization .......................................................................................................... 5 4.3 Measurement of VOC (NMNEHC C3) ............................................................................... 6 4.4 Process Parameters............................................................................................................... 6 5.1 Quality Assurance ................................................................................................................ 7 List of Tables and Figures Figure 1 - Sample Port Location ............................................................................................................................. 2 Figure 2 - Sampling Train Schematic-Method 320 ................................................................................................ 5 Table 1 - Insertion Depths of Traverse Points for Stratification Test ..................................................................... 2 Table 2 - Test Matrix .............................................................................................................................................. 4 Table 3 - Concentrations and Interference .............................................................................................................. 5 APPENDIX A: NOx, CO and VOC Test Data APPENDIX B: Quality Assurance/Calibration Data APPENDIX C: Load Approximation APPENDIX D: Example Calculations and Summary APPENDIX E: Field Notes 1 1.1 Introduction An air emissions test program was conducted on a Caterpillar G3516B engine, operated by Uinta Wax Operating, LLC and designated as Unit #2, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC) defined as non-methane, non-ethane hydrocarbons, reported as propane (NMNEHC C3). The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Three one hour test runs were performed on June 19, 2024 to analyze NOx, CO and VOC emission levels. Test runs were performed according to methodologies outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320 as outlined in the submitted Source Test Protocol dated May 17, 2024. Each one hour test run consisted of 60 readings taken at one minute intervals. Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. The following key personnel were present during testing: David Martinez, OEC Kyle John 2 2.1 Stack Sampling Location The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Testing was conducted on the Caterpillar G3516B engine. The sampling port for moisture, NOx, CO and VOC measurements was approximately 3.4 pipe diameters (48”) downstream from the nearest flow disturbance (Distance B) and 8.6 pipe diameters (120”) upstream from the nearest disturbance (Distance A), as seen in Figure 1. The stack sampling location was placed at approximately 50% insertion depth based on an O2 stratification check which demonstrated a non-stratified flow regime. The stratification was conducted according to EPA 40 CFR 75(A), §6.5.6.1 using 3 traverse points determined according to Table 1 below. Figure 1 - Sample Port Location Table 1 - Insertion Depths of Traverse Points for Stratification Test Traverse Point Insertion Depth (Percent of Stack Diameter) 1 16.6 2 50.0 3 83.3 14" A B Oxidation Catalyst 3 3.1 Discussion of NOx, CO and VOC Test Results Three, one hour test runs were performed on June 19, 2024 to analyze exhaust NOx, CO and VOC (NMNEHC C3) emission levels to demonstrate annual compliance with the emissions limits contained in the WDEQ Permit #DAQE-AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ. Testing for NOx, CO and VOC were run concurrently with one another. Each test was performed at the maximum achievable load. Measured emissions were below permitted limits. Please refer to the Appendices for a listing of all raw data, calibration error response and calculations performed per EPA 40 CFR 60(A) requirements. 3.1.1 Source Test 1: Caterpillar G3516B, NOx, CO and VOC The first test was performed from 12:39 to 13:38 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 966.0 bhp, and the average NOx and CO levels were found to be 0.46 g/bhp-hr and 0.01 g/bhp-hr respectively, below limitations. The VOC level tested at 0.39 g/bhp- hr, which tested in compliance. 3.1.2 Source Test 2: Caterpillar G3516B, NOx, CO and VOC The second test was performed from 13:40 to 14:39 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 966.0 bhp, and the average NOx and CO levels were found to be 0.46 g/bhp-hr and 0.01 g/bhp-hr respectively, below limitations. The VOC level tested at 0.38 g/bhp- hr, which tested in compliance. 3.1.3 Source Test 3: Caterpillar G3516B, NOx, CO and VOC The third test was performed from 14:41 to 15:40 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 966.0 bhp, and the average NOx and CO levels were found to be 0.48 g/bhp-hr and 0.01 g/bhp-hr respectively, below limitations. The VOC level tested at 0.39 g/bhp- hr, which tested in compliance. Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 1 82.52 0.46 3.76 0.01 72.96 0.39 5.7 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 2 83.84 0.46 3.81 0.01 72.68 0.38 6.0 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 3 84.64 0.48 3.87 0.01 72.63 0.39 5.9 4 4.1 Stack Sampling Methods and Procedures Testing followed EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, with no exceptions. Table 2 - Test Matrix Method Title Parameter Reference EPA 40 CFR 60 Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources Sampling Point Determination https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_1_3.pdf EPA 40 CFR 60 Appendix A, Method 2 Determination of Stack Gas Velocity and Volumetric Flow Rate Exhaust Effluent Flow https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_2.pdf EPA 40 CFR 60 Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight O2, CO2, Dry Volumetric Flow Rate https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_3.pdf EPA 40 CFR 63 Appendix A, EPA Method 320 Vapor Phase Organic and Inorganic Emissions by Extractive FTIR Nitrogen Oxides, Carbon Monoxide, Non- Methane Non- Ethane Hydrocarbons on a Propane Basis https://www.epa.gov/ emc/method-320- vapor-phase-organic- and-inorganic- emissions-extractive- ftir United States. U.S. Environmental Protection Agency. “EMC Promulgated Test Methods.” Air Emission Measurement Center (EMC). 31 August 2023. Web. 2 July 2024. <https://www.epa.gov/emc/emc-promulgated-test-methods>. ASTM International. “Standards & Publications.” All Environment Standards. Web. 2 July 2024. <https://www.astm.org/Standards/D6348.htm>. 5 4.2 Equipment Utilization The following equipment was used during the tests performed at this facility in conjunction with procedures outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320. • (1) MKS MultiGas 2030 FTIR Continuous Gas Analyzer (0.210 L/min sample flow, 0.014 atmosphere sample pressure, 1 atmosphere cell pressure, 191°C cell temperature) • (1) Laptop Computer for the FTIR Analyzer using MKS MG2000 Software • (1) 75ft or 100ft Heated Teflon Line w/ Heated Sample Probe and Spike Bypass Line • S-Type Pitot Tube c/w 20 ft. Heated Sample Line (coefficient 0.84) • (1) Enerac 500 Portable O2/CO2 Analyzer • (1) Fyrite O2/CO2 Analyzer • (5) EPA Protocol G1 Calibration Gas (NOx, CO, C3H8, C2H4 and NO2) The MKS Multigas 2030 FTIR Analyzer operated with a spectral resolution of 0.5 cm-1 and a scan time of 30 seconds. The FTIR spectrometer utilizes a multi-pass gas cell with a 5.11 meter effective pathlength. Figure 2 - Sampling Train Schematic-Method 320 Table 3 - Concentrations and Interference 6 The MKS 2030 software provides a Natural Gas Method that is designed to minimize all expected interferences by removing the regions in the quant region where they are most absorbed (i.e. picket fence approach). So, for example, all the water peaks that are greater than about 0.1 abs are removed from the quant region. Since the spectral noise measured (sample spectrum) is in the range of 0.001 absorbance, it is desirable to have any error within this range. The MKS software will match the water calibration spectrum to the sample spectrum at any 1 point in the spectrum to about 1% precision. So, 1% of 0.1 absorbance is 0.001 abs. This is why any peaks greater than this for interfering compounds are usually excluded so they do not interfere. To summarize, the MKS software and the method are designed to minimize any interferences by removing their largest interfering absorptions. 4.3 Measurement of VOC (NMNEHC C3) The algorithm currently used for NMNEHC C3 and developed for natural gas fired applications by Dr. Spartz and MKS instruments in accordance with EPA standards, is the following: (2.4*c8/(1+exp((2-c8)/0.2))+1.9*c11/(1+exp((2-c11)/0.2))+6*c12/(1+exp((0.5-c12) /0.2))+2.85*c13/(1+exp((2-c13)/0.2))+3*c14/(1+exp((1-c14)/0.2)))/3 c8= acetylene c11= ethylene c12= hexane c13= propylene c14= propane Note: The constants in front of each of the compounds listed represents the FID response factor when calibrated with Propane. As with any CEMS analyzer, the FTIR may demonstrate a negative zero bias. The “exp” functions listed in the algorithm above are intended to mathematically filter out any negative biases and set them to approach zero. 4.4 Process Parameters Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. Results are provided in Appendix C. 7 5.1 Quality Assurance The MKS Multigas 2030 FTIR Analyzer was used to measure NOx, CO and VOC on a dry basis. A pre Direct and System calibration measurement was made on compounds of NOx, CO, C3H8 and C2H4. In addition, post System calibrations were made on compounds of NOx, CO, C3H8 and C2H4. Compounds of CO2 and C3H8 were measured for the quality assurance spiking requirements. Levels for calibrations and zeroes must be within +/- 5% of the certified calibration gas or response to zero gas, respectively. CTS procedures were followed according to EPA requirements for both pre and post testing. Similarly, QA spiking procedures were followed. Analysis of the CO2 exhaust effluent was used to determine the dilution factor. Steady levels of the CO2 were observed and a sufficient duration of time was allowed to elapse for a representative average. The calibration gas was spiked into the effluent stream using a bypass line at approximately 10% of the sampling rate. The dilution factor was obtained from observation of the stack CO2 behavior using the following equation: CO2AVG – CO2SPIKE DF = ------------------------ CO2 AVG Where: CO2AVG = The average undiluted CO2 stack gas concentration of spike measurements CO2SPIKE = The average diluted CO2 stack gas concentration when spiked The sample recovery was then obtained from the following equation: % REC = (Spike MEAS – Stack MEAS)* (1 – DF) --------------------------------------------------------- CS * DF Where: Spike MEAS = The average diluted stack gas concentration when spiked Stack MEAS = The average undiluted stack gas concentration DF = Dilution factor CS = Certified concentration of calibration standards The Sample Recovery average level for C3H8 was found to be 75.9%, which was within the allowable tolerance of Method 320 (70% to 130%). A summary of all spiking procedures/results can be found in Appendix B. APPENDIX A NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 66.149613 16.218682 82.368295 3.93302 73.281276 10.791492 12:39:17 06/19/2024 2 64.410803 15.81963 80.230433 3.818567 74.628419 10.89553 12:40:17 06/19/2024 3 63.904925 15.79688 79.701805 3.84622 73.296221 10.722381 12:41:17 06/19/2024 4 59.511032 14.438725 73.949757 3.730878 74.883268 10.478952 12:42:17 06/19/2024 5 65.394816 16.099973 81.494789 3.840282 72.141553 10.511843 12:43:17 06/19/2024 6 65.831306 16.254582 82.085888 3.864942 73.278219 10.376493 12:44:18 06/19/2024 7 66.876604 16.576536 83.45314 3.869057 73.267594 10.420194 12:45:17 06/19/2024 8 65.364787 16.155894 81.520681 3.748082 72.806443 10.363438 12:46:18 06/19/2024 9 66.091221 16.306922 82.398143 3.767469 72.342123 10.837447 12:47:18 06/19/2024 10 66.017609 16.343745 82.361354 3.70952 72.230483 10.789981 12:48:18 06/19/2024 11 71.631223 17.748268 89.379491 3.776142 71.017191 10.873186 12:49:18 06/19/2024 12 68.517067 16.903154 85.420221 3.796537 72.599608 10.980746 12:50:18 06/19/2024 13 63.363641 15.51635 78.879991 3.595946 74.321747 11.162598 12:51:18 06/19/2024 14 62.075104 15.131057 77.206161 3.743394 74.306401 11.065243 12:52:18 06/19/2024 15 64.850344 15.948063 80.798407 3.760328 72.926994 10.799339 12:53:18 06/19/2024 16 67.250902 16.55399 83.804892 3.769032 72.575699 10.765297 12:54:19 06/19/2024 17 71.153769 17.584223 88.737992 3.773388 71.667843 10.7026 12:55:18 06/19/2024 18 69.29002 16.955547 86.245567 3.723582 72.721392 10.639341 12:56:18 06/19/2024 19 65.106505 15.951905 81.05841 3.741744 73.227911 10.614212 12:57:19 06/19/2024 20 59.761481 14.52757 74.289051 3.666228 74.023246 10.601211 12:58:19 06/19/2024 21 66.973703 16.509329 83.483032 3.779646 72.569374 10.717177 12:59:19 06/19/2024 22 72.57596 17.971422 90.547382 3.757293 71.240285 10.735712 13:00:19 06/19/2024 23 66.844591 16.350456 83.195047 3.735193 73.106157 10.738976 13:01:19 06/19/2024 24 64.967105 15.875967 80.843072 3.702479 74.183405 10.677639 13:02:19 06/19/2024 25 61.258169 14.826288 76.084457 3.761114 75.232416 10.702939 13:03:19 06/19/2024 26 64.20473 15.626642 79.831372 3.658377 73.799838 10.618905 13:04:19 06/19/2024 27 65.780085 16.059413 81.839498 3.686572 73.228581 10.625496 13:05:20 06/19/2024 28 66.252164 16.27814 82.530304 3.744407 73.850706 10.595273 13:06:20 06/19/2024 29 65.889446 16.162329 82.051775 3.726294 73.853273 10.574282 13:07:20 06/19/2024 30 66.288462 16.167983 82.456445 3.744279 73.107060 10.567809 13:08:19 06/19/2024 31 66.447916 16.300614 82.74853 3.74905 73.545792 10.688676 13:09:20 06/19/2024 32 65.458981 15.967899 81.42688 3.787837 73.870973 10.951438 13:10:20 06/19/2024 33 66.181145 16.155491 82.336636 3.694385 74.179838 11.043192 13:11:20 06/19/2024 34 67.195181 16.365812 83.560993 3.758013 73.574349 10.936825 13:12:20 06/19/2024 35 66.670494 16.338378 83.008872 3.777064 73.891471 10.944549 13:13:20 06/19/2024 36 66.622269 16.335219 82.957488 3.745556 73.739279 10.947471 13:14:20 06/19/2024 37 66.225157 16.143134 82.368291 3.733641 73.332715 10.829676 13:15:20 06/19/2024 38 66.212324 16.209691 82.422015 3.690226 74.089874 10.702716 13:16:20 06/19/2024 39 66.497554 16.303707 82.801261 3.810521 72.502137 10.689167 13:17:21 06/19/2024 40 66.509197 16.253779 82.762976 3.7435 72.195826 10.703567 13:18:21 06/19/2024 41 66.746421 16.409672 83.156093 3.78576 72.429878 10.626391 13:19:21 06/19/2024 42 67.719826 16.650473 84.370299 3.794704 71.922324 10.661616 13:20:21 06/19/2024 43 67.479692 16.50326 83.982952 3.725053 72.567907 10.984062 13:21:21 06/19/2024 44 66.435893 16.329796 82.765689 3.771295 72.544667 11.0666 13:22:21 06/19/2024 45 65.740913 16.085821 81.826734 3.747682 72.369654 10.992984 13:23:21 06/19/2024 46 67.154006 16.382019 83.536025 3.76921 72.429060 10.9482 13:24:21 06/19/2024 47 66.605618 16.335385 82.941003 3.71754 72.180302 10.89025 13:25:21 06/19/2024 48 65.945172 16.15225 82.097422 3.768254 72.231163 10.898236 13:26:21 06/19/2024 49 67.768651 16.628152 84.396803 3.748922 72.542485 10.876037 13:27:21 06/19/2024 50 67.755818 16.488547 84.244365 3.841786 72.330881 10.930601 13:28:22 06/19/2024 51 66.484139 16.147282 82.631421 3.799858 73.041033 11.037678 13:29:21 06/19/2024 52 67.93928 16.512137 84.451417 3.823639 71.849045 11.043347 13:30:22 06/19/2024 53 65.84279 15.935884 81.778674 3.726654 72.467827 11.011601 13:31:22 06/19/2024 54 68.109911 16.485139 84.59505 3.833609 72.156386 10.969414 13:32:22 06/19/2024 55 66.830342 16.22382 83.054162 3.815468 72.598890 10.983089 13:33:22 06/19/2024 56 66.90504 16.106129 83.011169 3.818293 72.936395 11.031118 13:34:22 06/19/2024 57 67.44742 16.144513 83.591933 3.76261 72.022715 10.982315 13:35:22 06/19/2024 58 67.026272 16.095774 83.122046 3.793143 72.018161 10.890407 13:36:22 06/19/2024 59 66.918859 16.197711 83.11657 3.821945 72.483541 10.854567 13:37:22 06/19/2024 60 67.38855 16.366947 83.755497 3.698468 71.828020 10.839611 13:38:22 06/19/2024 AVG 66.30 0.00 82.52 3.76 72.96 10.80 ppm@15% O2 32.03 1.46 28.32 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.46 0.99 0.01 0.03 0.39 0.84 #2 FTIR Measurements Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 1 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 14 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.91 1617 0.29 0.954 Average O2 5.7 (% dry)A 2 1.47 0.93 0.964 Average CO2 6.9 (% dry)A 3 2.72 0.95 0.975 Average N2 + CO 87.4 (% dry)A 4 4.52 0.99 0.995 Dry Molecular Weight 29.33 lb/lbmol A 5 9.48 1.04 1.020 Wet Molecular Weight 28.11 lb/lbmol A 6 11.28 0.96 0.980 EPA REFERENCE METHOD 320 A 7 12.53 0.94 0.970 Barometric Pressure 25.11 in Hg A 8 13.50 0.92 0.959 Moisture Content 10.80 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 82.52 ppm A 11 Calculated NOx Mass Output 0.99 lbs/hr A 12 Calculated NOx Output 0.46 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 3.76 ppm A 15 Calculated CO Mass Output 0.03 lbs/hr A 16 Calculated CO Output 0.01 g/bhp-hr B 1 0.50 0.93 1617 0.29 0.964 EPA REFERENCE METHOD 320 B 2 1.47 0.94 0.970 Average Analyzer NMNEHC Level 72.96 ppm B 3 2.72 0.97 0.985 Calculated NMNEHC Mass Output 0.84 lbs/hr B 4 4.52 0.99 0.995 Calculated NMNEHC Output 0.39 g/bhp-hr B 5 9.48 1.02 1.010 LOAD APPROXIMATION B 6 11.28 0.98 0.990 Estimated Engine Load 966.0 BHP B 7 12.53 1.00 1.000 B 8 13.50 0.94 0.970 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 1.0 1617 0.3 0.981 Average Stack Gas Velocity 106.61 ft/sec Average Dry Flowrate 1672.92 dscfm TEST RUN # 1 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 66.488986 16.219516 82.708502 3.763871 72.278126 10.76832 13:40:23 06/19/2024 2 67.80525 16.503511 84.308761 3.863107 71.883217 10.811432 13:41:22 06/19/2024 3 67.420661 16.427602 83.848263 3.827072 72.728998 10.832165 13:42:23 06/19/2024 4 66.800774 16.266959 83.067733 3.81711 72.267702 10.814847 13:43:23 06/19/2024 5 66.572402 16.210332 82.782734 3.821537 72.601126 10.803507 13:44:23 06/19/2024 6 67.638786 16.53254 84.171326 3.770709 71.187874 10.833883 13:45:23 06/19/2024 7 67.228005 16.376356 83.604361 3.88929 71.850056 10.845826 13:46:23 06/19/2024 8 67.450822 16.475104 83.925926 3.700525 73.083208 10.818089 13:47:23 06/19/2024 9 67.59997 16.542524 84.142494 3.71367 71.958159 10.809257 13:48:23 06/19/2024 10 66.58102 16.199103 82.780123 3.787845 72.386557 10.780573 13:49:23 06/19/2024 11 66.955708 16.369224 83.324932 3.812872 72.352276 10.841111 13:50:23 06/19/2024 12 67.572247 16.518724 84.090971 3.845781 72.318715 10.837859 13:51:23 06/19/2024 13 67.483246 16.506324 83.98957 3.872927 71.841198 10.820004 13:52:23 06/19/2024 14 67.353121 16.432364 83.785485 3.802544 72.401101 10.83803 13:53:24 06/19/2024 15 68.056839 16.61718 84.674019 3.836517 72.030453 10.841366 13:54:24 06/19/2024 16 66.926231 16.295879 83.22211 3.835913 72.615627 10.827012 13:55:24 06/19/2024 17 67.502077 16.467697 83.969774 3.810043 72.285389 10.861724 13:56:24 06/19/2024 18 67.480919 16.449099 83.930018 3.76742 72.010506 10.845559 13:57:24 06/19/2024 19 67.807872 16.524851 84.332723 3.86087 72.627450 10.82513 13:58:24 06/19/2024 20 66.763565 16.229073 82.992638 3.741837 72.921573 10.819328 13:59:24 06/19/2024 21 67.227327 16.391405 83.618732 3.853398 72.375174 10.820217 14:00:24 06/19/2024 22 68.122982 16.525326 84.648308 3.855437 71.620696 10.823267 14:01:24 06/19/2024 23 67.185608 16.264568 83.450176 3.89916 73.021792 10.82081 14:02:25 06/19/2024 24 67.362115 16.260741 83.622856 3.833359 72.671071 10.82693 14:03:24 06/19/2024 25 68.47202 16.644523 85.116543 3.794683 73.005405 10.85676 14:04:25 06/19/2024 26 67.500898 16.40736 83.908258 3.899489 72.571023 10.835487 14:05:25 06/19/2024 27 67.422389 16.239921 83.66231 3.832921 72.970885 10.814608 14:06:25 06/19/2024 28 67.362874 16.298152 83.661026 3.865821 73.007132 10.832543 14:07:25 06/19/2024 29 66.067753 15.96016 82.027913 3.788865 73.470364 10.802807 14:08:25 06/19/2024 30 67.334251 16.237459 83.57171 3.81332 72.217797 10.837376 14:09:25 06/19/2024 31 67.549899 16.346036 83.895935 3.786339 72.810576 10.827448 14:10:25 06/19/2024 32 67.297781 16.255128 83.552909 3.778037 73.251244 10.850359 14:11:25 06/19/2024 33 67.189936 16.258994 83.44893 3.819107 72.521779 10.864738 14:12:25 06/19/2024 34 66.851073 16.159501 83.010574 3.784289 72.585879 10.851972 14:13:25 06/19/2024 35 67.576266 16.277223 83.853489 3.8324 72.854400 10.857728 14:14:25 06/19/2024 36 68.570737 16.537687 85.108424 3.779588 72.920576 10.851058 14:15:26 06/19/2024 37 67.684598 16.322585 84.007183 3.781329 72.910723 10.842898 14:16:26 06/19/2024 38 67.366446 16.242469 83.608915 3.7762 72.924799 10.852037 14:17:26 06/19/2024 39 68.020235 16.379552 84.399787 3.730023 72.983176 10.875939 14:18:26 06/19/2024 40 68.226091 16.385718 84.611809 3.75021 72.918460 10.866546 14:19:26 06/19/2024 41 67.949236 16.357071 84.306307 3.837227 73.430786 10.875546 14:20:26 06/19/2024 42 67.559038 16.240543 83.799581 3.850908 72.920458 10.867121 14:21:26 06/19/2024 43 67.302276 16.20942 83.511696 3.755452 73.301297 10.85467 14:22:26 06/19/2024 44 67.857841 16.378755 84.236596 3.795156 72.483916 10.832639 14:23:26 06/19/2024 45 68.711508 16.655252 85.36676 3.79793 72.496322 10.853298 14:24:26 06/19/2024 46 67.186792 16.339625 83.526417 3.825851 72.813244 10.848453 14:25:26 06/19/2024 47 67.184399 16.291777 83.476176 3.878227 73.271954 10.852027 14:26:26 06/19/2024 48 66.906858 16.21071 83.117568 3.873437 72.478387 10.832586 14:27:27 06/19/2024 49 66.638547 16.118107 82.756654 3.787113 72.767061 10.848688 14:28:27 06/19/2024 50 68.118948 16.497838 84.616786 3.863948 72.871390 10.855345 14:29:27 06/19/2024 51 67.573335 16.333708 83.907043 3.706624 73.037806 10.857842 14:30:27 06/19/2024 52 67.499432 16.269564 83.768996 3.841915 73.194060 10.838814 14:31:27 06/19/2024 53 67.863278 16.435172 84.29845 3.847302 72.405574 10.841466 14:32:27 06/19/2024 54 67.370665 16.259636 83.630301 3.808169 73.144752 10.840736 14:33:27 06/19/2024 55 67.916316 16.320188 84.236504 3.82402 72.470172 10.818144 14:34:27 06/19/2024 56 69.262264 16.761637 86.023901 3.859115 72.861052 10.829851 14:35:27 06/19/2024 57 66.332868 15.88116 82.214028 3.816274 74.088575 10.860018 14:36:27 06/19/2024 58 67.614939 16.287685 83.902624 3.826024 73.366560 10.876476 14:37:27 06/19/2024 59 68.196799 16.4074 84.604199 3.803617 72.555167 10.861491 14:38:27 06/19/2024 60 68.114982 16.367984 84.482966 3.844098 73.628189 10.855592 14:39:28 06/19/2024 AVG 67.48 0.00 83.84 3.81 72.68 10.84 ppm@15% O2 33.20 1.51 28.78 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.46 0.98 0.01 0.03 0.38 0.81 Calculated Emission Levels Record Date Uinta Wax Operating, LLC North Randlett Compressor Station Run 2 #2 FTIR Measurements EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 14 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.82 1620 0.3 0.906 Average O2 6.0 (% dry)A 2 1.47 0.88 0.938 Average CO2 7 (% dry)A 3 2.72 0.92 0.959 Average N2 + CO 87.0 (% dry)A 4 4.52 0.95 0.975 Dry Molecular Weight 29.36 lb/lbmol A 5 9.48 0.99 0.995 Wet Molecular Weight 28.13 lb/lbmol A 6 11.28 0.96 0.980 EPA REFERENCE METHOD 320 A 7 12.53 0.93 0.964 Barometric Pressure 25.11 in Hg A 8 13.50 0.93 0.964 Moisture Content 10.84 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 83.84 ppm A 11 Calculated NOx Mass Output 0.98 lbs/hr A 12 Calculated NOx Output 0.46 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 3.81 ppm A 15 Calculated CO Mass Output 0.03 lbs/hr A 16 Calculated CO Output 0.01 g/bhp-hr B 1 0.50 0.85 1620 0.3 0.922 EPA REFERENCE METHOD 320 B 2 1.47 0.87 0.933 Average Analyzer NMNEHC Level 72.68 ppm B 3 2.72 0.90 0.949 Calculated NMNEHC Mass Output 0.81 lbs/hr B 4 4.52 0.93 0.964 Calculated NMNEHC Output 0.38 g/bhp-hr B 5 9.48 0.97 0.985 LOAD APPROXIMATION B 6 11.28 0.95 0.975 Estimated Engine Load 966.0 BHP B 7 12.53 0.94 0.970 B 8 13.50 0.92 0.959 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.9 1620 0.3 0.959 Average Stack Gas Velocity 104.20 ft/sec Average Dry Flowrate 1631.48 dscfm TEST RUN # 2 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 68.217758 16.250448 84.468206 3.856574 73.220193 10.890005 14:41:28 06/19/2024 2 68.125343 16.325055 84.450398 3.90645 73.735953 10.886983 14:42:28 06/19/2024 3 67.730108 16.316693 84.046801 3.854181 74.052539 10.902262 14:43:28 06/19/2024 4 66.355288 15.904889 82.260177 3.796942 74.171891 10.90381 14:44:28 06/19/2024 5 67.795434 16.372649 84.168083 3.834461 73.579727 10.882729 14:45:28 06/19/2024 6 67.444316 16.220216 83.664532 3.796536 74.198249 10.872858 14:46:29 06/19/2024 7 67.276056 16.232889 83.508945 3.856142 73.564574 10.845532 14:47:28 06/19/2024 8 67.411784 16.239856 83.65164 3.809439 73.317813 10.866626 14:48:29 06/19/2024 9 67.797254 16.460284 84.257538 3.95235 72.376979 10.883073 14:49:29 06/19/2024 10 67.749734 16.423444 84.173178 3.874295 72.524064 10.874033 14:50:29 06/19/2024 11 66.802368 16.144749 82.947117 3.759103 72.582913 10.883365 14:51:29 06/19/2024 12 67.854824 16.403447 84.258271 3.800274 73.050617 10.922925 14:52:29 06/19/2024 13 68.054883 16.429893 84.484776 3.83058 72.136456 10.904886 14:53:29 06/19/2024 14 67.942542 16.393183 84.335725 3.758989 72.477813 10.887383 14:54:29 06/19/2024 15 67.253323 16.23218 83.485503 3.898263 72.548464 10.924103 14:55:29 06/19/2024 16 68.50975 16.507994 85.017744 3.859474 72.691011 10.916808 14:56:29 06/19/2024 17 67.61228 16.250054 83.862334 3.853552 72.800119 10.885023 14:57:30 06/19/2024 18 68.160837 16.515037 84.675874 3.894863 73.026811 10.798701 14:58:29 06/19/2024 19 68.055086 16.526343 84.581429 3.951449 72.813672 10.725104 14:59:29 06/19/2024 20 66.87489 16.195005 83.069895 3.89522 73.064177 10.801455 15:00:29 06/19/2024 21 67.820814 16.483334 84.304148 3.949519 72.793351 10.844139 15:01:30 06/19/2024 22 67.234265 16.256238 83.490503 3.943649 73.227202 10.823488 15:02:30 06/19/2024 23 67.963737 16.458624 84.422361 3.916919 73.249996 10.801966 15:03:30 06/19/2024 24 67.493913 16.331832 83.825745 3.922049 73.198160 10.824797 15:04:30 06/19/2024 25 67.67523 16.331525 84.006755 3.861048 72.690034 10.855994 15:05:30 06/19/2024 26 67.613979 16.277272 83.891251 3.802211 72.262078 10.890368 15:06:30 06/19/2024 27 66.7696 16.043899 82.813499 3.898321 72.929169 10.89466 15:07:30 06/19/2024 28 68.193692 16.464862 84.658554 3.842226 71.712356 10.888284 15:08:30 06/19/2024 29 67.81604 16.357602 84.173642 3.896108 72.542446 10.841979 15:09:30 06/19/2024 30 68.278304 16.494129 84.772433 3.874616 71.650189 10.812634 15:10:30 06/19/2024 31 68.443333 16.554257 84.99759 3.893713 72.217356 10.819796 15:11:31 06/19/2024 32 67.89839 16.51411 84.4125 3.914134 71.869458 10.984038 15:12:31 06/19/2024 33 68.041843 16.409194 84.451037 3.885008 71.542928 11.143212 15:13:31 06/19/2024 34 68.523284 16.648788 85.172072 3.953864 71.422461 11.029565 15:14:31 06/19/2024 35 68.542435 16.63581 85.178245 3.920446 71.163279 10.905702 15:15:31 06/19/2024 36 67.906778 16.516537 84.423315 3.960641 71.954431 10.906556 15:16:31 06/19/2024 37 68.574597 16.761681 85.336278 3.923177 71.353687 11.093217 15:17:31 06/19/2024 38 68.573768 16.665394 85.239162 3.909948 71.085601 11.038248 15:18:31 06/19/2024 39 68.714732 16.721587 85.436319 3.958936 70.808044 11.076917 15:19:31 06/19/2024 40 69.396829 16.714981 86.11181 3.831232 70.760777 11.055305 15:20:32 06/19/2024 41 67.760214 16.417045 84.177259 3.789012 71.650591 11.018364 15:21:31 06/19/2024 42 68.933734 16.703002 85.636736 3.927606 72.552920 11.095776 15:22:31 06/19/2024 43 68.652214 16.551514 85.203728 3.940328 72.596740 11.04598 15:23:32 06/19/2024 44 68.603436 16.371695 84.975131 3.815853 72.654217 11.022483 15:24:32 06/19/2024 45 68.881625 16.523402 85.405027 3.793303 72.190615 11.004356 15:25:32 06/19/2024 46 68.270341 16.341439 84.61178 3.874737 72.671032 10.985661 15:26:32 06/19/2024 47 68.751858 16.386028 85.137886 3.871119 72.779200 10.996614 15:27:32 06/19/2024 48 68.630235 16.373704 85.003939 3.851588 73.470391 11.001836 15:28:32 06/19/2024 49 68.791626 16.40637 85.197996 3.807159 72.538689 11.017813 15:29:32 06/19/2024 50 70.154741 16.749125 86.903866 3.881817 72.464952 11.021225 15:30:32 06/19/2024 51 68.703318 16.46444 85.167758 3.884106 73.007169 10.997557 15:31:33 06/19/2024 52 68.44403 16.34418 84.78821 3.874492 72.475686 11.005323 15:32:32 06/19/2024 53 71.151317 16.960763 88.11208 3.940678 71.220905 11.024593 15:33:33 06/19/2024 54 67.283003 16.019211 83.302214 3.865215 73.136802 10.965662 15:34:33 06/19/2024 55 69.297585 16.572278 85.869863 3.820431 73.074281 10.967855 15:35:33 06/19/2024 56 70.0988 16.568387 86.667187 3.881419 73.147644 10.984564 15:36:33 06/19/2024 57 69.143696 16.44964 85.593336 3.873595 73.154323 10.986774 15:37:33 06/19/2024 58 68.732034 16.409497 85.141531 3.910714 73.402082 10.991745 15:38:33 06/19/2024 59 69.113013 16.45596 85.568973 3.882341 73.717416 10.98324 15:39:33 06/19/2024 60 68.985908 16.40127 85.387178 3.893285 73.587748 10.976308 15:40:33 06/19/2024 AVG 68.21 0.00 84.64 3.87 72.63 10.93 ppm@15% O2 33.29 1.52 28.57 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.48 1.01 0.01 0.03 0.39 0.83 FTIR Measurements #2 Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 3 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 14 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.89 1619 0.3 0.943 Average O2 5.9 (% dry)A 2 1.47 0.91 0.954 Average CO2 7 (% dry)A 3 2.72 0.94 0.970 Average N2 + CO 87.1 (% dry)A 4 4.52 0.99 0.995 Dry Molecular Weight 29.36 lb/lbmol A 5 9.48 1.02 1.010 Wet Molecular Weight 28.11 lb/lbmol A 6 11.28 0.98 0.990 EPA REFERENCE METHOD 320 A 7 12.53 0.98 0.990 Barometric Pressure 25.11 in Hg A 8 13.50 0.95 0.975 Moisture Content 10.93 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 84.64 ppm A 11 Calculated NOx Mass Output 1.01 lbs/hr A 12 Calculated NOx Output 0.48 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 3.87 ppm A 15 Calculated CO Mass Output 0.03 lbs/hr A 16 Calculated CO Output 0.01 g/bhp-hr B 1 0.50 0.91 1619 0.3 0.954 EPA REFERENCE METHOD 320 B 2 1.47 0.93 0.964 Average Analyzer NMNEHC Level 72.63 ppm B 3 2.72 0.97 0.985 Calculated NMNEHC Mass Output 0.83 lbs/hr B 4 4.52 1.03 1.015 Calculated NMNEHC Output 0.39 g/bhp-hr B 5 9.48 1.01 1.005 LOAD APPROXIMATION B 6 11.28 0.97 0.985 Estimated Engine Load 966.0 BHP B 7 12.53 0.98 0.990 B 8 13.50 0.96 0.980 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 1.0 1619 0.3 0.982 Average Stack Gas Velocity 106.69 ft/sec Average Dry Flowrate 1669.67 dscfm TEST RUN # 3 APPENDIX B Date Time NO 191C span NO2 191C span H2O% (high) 191C Formaldehyde 191C Ethylene 191C TE span Propane 191C span Acetaldehyde 191C span CO ppm 191C (1of2) span CO ppm Dry CO2% 191C NOx Wet NOx Dry NM NE HC C3 Temp ( C )Pressure (atm) 6/19/2024 12:16:08 -8.640084 -1.544026 -0.835586 -0.513861 -3.571717 -4.248064 -1.941719 -0.322705 -0.320031 -0.823399 -10.18411 -10.099718 -0.009371 192.020554 1.024651 6/19/2024 12:16:15 -8.824537 -1.48725 -0.83338 -0.534233 -3.220536 -4.288123 -0.398855 -0.278533 -0.276231 -0.823307 -10.311787 -10.22656 -0.007944 192.016922 1.022658 6/19/2024 12:16:22 -8.503543 -1.465926 -0.84389 -0.621526 -3.557335 -4.9077 -0.342537 0.014434 0.014313 -0.815972 -9.969469 -9.886042 -0.009739 192.031448 1.022933 6/19/2024 12:16:30 -8.777526 -1.448341 -0.835471 -0.585982 -3.585313 -4.583317 -0.739901 0.062245 0.061729 -0.819578 -10.225867 -10.14114 -0.011018 192.016922 1.022933 6/19/2024 12:17:07 0 0 0 0 0 0 0 0 0 0 0 0 0 192.039825 1.021698 6/19/2024 12:17:21 0.165856 0.039964 0.004905 0.049864 -1.040345 0.141529 1.492392 0.222613 0.222624 0.007495 0.20582 0.20583 0.021408 192.04599 1.017019 6/19/2024 12:17:28 -0.098067 -0.07931 0.005673 0.027544 -0.072307 -0.166523 -0.60438 0.097956 0.097961 0.009828 -0.177377 -0.177387 0.008048 192.00238 1.021418 6/19/2024 12:17:36 -0.003484 0.045121 0.007681 0.202319 0.296779 -0.124285 0.858677 0.149561 0.149572 0.001885 0.041636 0.04164 -0.006302 192.075058 1.026055 6/19/2024 12:17:43 -0.194083 0.001337 0.003989 0.091974 -0.204705 0.846708 0.520149 0.042469 0.042471 -0.002079 -0.192746 -0.192753 0.263279 192.016922 1.019399 6/19/2024 12:17:51 0.094989 -0.045403 -0.001133 0.105791 -0.497055 1.227168 0.039833 0.143005 0.143003 0.004475 0.049586 0.049585 0.919227 191.958771 1.003976 6/19/2024 12:17:58 0.285048 -0.094326 -0.001711 0.028853 0.413852 0.284152 0.237848 -0.051692 -0.051691 0.008089 0.190722 0.190719 0.000201 192.033264 1.00339 6/19/2024 12:18:06 -0.026474 -0.05786 0.008457 -0.156632 -0.369111 0.537992 0.435519 0.146754 0.146767 0.005862 -0.084334 -0.084341 0.061166 192.031448 1.000946 6/19/2024 12:18:13 -0.103253 -0.036804 -0.004281 -0.058943 -0.108662 -0.496108 -1.162717 -0.018249 -0.018248 -0.000705 -0.140057 -0.140051 0.00113 191.987854 0.997503 6/19/2024 12:18:21 0.189837 0.027328 0.00894 0.006498 -0.024076 -0.134288 0.47005 0.072021 0.072027 0.001758 0.217165 0.217184 0.014418 192.016922 0.995621 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 12:18:54 514.849898 491.680448 497.241146 192.088379 0.988181 6/19/2024 12:23:38 98.882185 192.283401 0.974472 6/19/2024 12:19:02 515.332918 491.984055 496.445899 192.104126 0.988139 6/19/2024 12:23:45 98.661826 192.264023 0.969549 6/19/2024 12:19:09 514.694803 491.210928 499.040106 192.0896 0.989149 6/19/2024 12:23:52 99.583063 192.234955 0.973588 6/19/2024 12:19:17 517.980256 494.977644 498.841325 192.104126 0.983274 6/19/2024 12:24:00 98.252696 192.264023 0.972532 6/19/2024 12:19:24 515.965987 492.395543 495.133256 192.075058 0.987726 6/19/2024 12:24:08 99.297042 192.234955 0.968355 6/19/2024 12:19:31 512.698541 490.730974 494.476684 192.060532 0.991306 6/19/2024 12:24:15 99.522372 192.249496 0.972825 6/19/2024 12:19:39 516.174932 493.104802 501.190558 192.060532 0.987083 6/19/2024 12:24:23 99.269347 192.249496 0.973772 6/19/2024 12:19:47 516.490634 493.44919 501.141979 192.096863 0.987124 6/19/2024 12:24:30 98.579618 192.234955 0.97065 6/19/2024 12:19:54 517.058538 493.573976 498.163546 192.060532 0.986028 6/19/2024 12:24:38 98.388561 192.234955 0.975608 6/19/2024 12:20:02 513.401407 489.523414 495.64683 192.104126 0.994841 6/19/2024 12:24:45 99.251879 192.220413 0.970834 Date Time NO2 191C span Temp ( C )Pressure (atm) 6/19/2024 12:21:56 145.393154 192.198608 0.973909 6/19/2024 12:22:03 145.767682 192.147736 0.973037 6/19/2024 12:22:11 146.291836 192.191345 0.974093 6/19/2024 12:22:18 145.583868 192.176819 0.976572 6/19/2024 12:22:26 146.409468 192.191345 0.97446 6/19/2024 12:22:33 145.953685 192.220413 0.976388 6/19/2024 12:22:41 146.028282 192.249496 0.976205 6/19/2024 12:22:49 146.947351 192.300369 0.971339 6/19/2024 12:22:56 146.980046 192.220413 0.971614 6/19/2024 12:23:03 146.821572 192.249496 0.973818 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 12:25:18 381.245092 340.507532 359.822626 192.249496 0.943331 6/19/2024 12:26:58 68.073059 192.266449 0.946598 6/19/2024 12:25:25 506.975652 486.404781 490.820784 192.278564 0.963995 6/19/2024 12:27:05 98.294442 192.249496 0.972257 6/19/2024 12:25:32 515.030965 493.469146 494.183516 192.264023 0.985982 6/19/2024 12:27:13 98.793678 192.220413 0.974093 6/19/2024 12:25:40 513.122416 490.900017 495.379724 192.234955 0.990939 6/19/2024 12:27:20 98.374879 192.249496 0.974323 6/19/2024 12:25:48 516.583205 492.306598 496.488569 192.249496 0.985477 6/19/2024 12:27:28 99.654531 192.220413 0.974231 6/19/2024 12:25:55 518.181067 493.740119 500.382872 192.198608 0.987646 6/19/2024 12:27:35 98.398439 192.278564 0.977628 6/19/2024 12:26:03 516.368934 493.354025 493.113099 192.234955 0.989746 6/19/2024 12:27:43 99.902677 192.274933 0.971821 6/19/2024 12:26:10 515.721222 493.068362 497.583569 192.249496 0.990893 6/19/2024 12:27:50 99.107203 192.249496 0.974598 6/19/2024 12:26:18 518.364156 494.431382 495.168969 192.249496 0.985615 6/19/2024 12:27:58 97.984084 192.234955 0.974598 6/19/2024 12:26:25 516.745157 493.031585 499.402787 192.278564 0.986946 6/19/2024 12:28:05 98.648517 192.220413 0.978178 6/19/2024 12:28:13 98.283418 192.205887 0.9757 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 12:28:28 0.19232 0.152253 0.446181 -0.66245 192.262207 0.998892 6/19/2024 12:28:35 0.111695 0.126964 -0.750152 0.01052 192.191345 1.001176 6/19/2024 12:28:43 0.102614 -0.182473 0.679635 -0.168246 192.234955 1.004205 6/19/2024 12:28:50 0.430109 0.053681 0.096142 -0.166869 192.220413 1.001038 6/19/2024 12:28:58 -0.056715 -0.29097 0.416146 0.481277 192.176819 0.997549 6/19/2024 12:29:05 -0.02275 -0.062322 0.084769 0.756563 192.205887 1.002094 6/19/2024 12:29:13 0.050098 0.190059 0.297428 -0.266657 192.118668 0.998605 6/19/2024 12:29:21 0.226669 0.037093 0.275441 -0.224224 192.135025 1.002547 Raw Calibration Data BACKGROUND / PRE DIRECT ZERO PRE DIRECT CAL NO2 CAL PRE SYSTEM CAL PRE SYSTEM ZERO Date Time CO2% 191C Propane 191C span Temp ( C )Pressure (atm) 6/19/2024 12:34:10 6.322335 44.290999 192.156219 1.006978 6/19/2024 12:34:17 6.310285 44.218388 192.191345 1.006867 6/19/2024 12:34:25 6.316794 43.581749 192.147736 1.005353 6/19/2024 12:34:33 6.298698 42.894177 192.104126 1.008245 6/19/2024 12:34:40 6.332465 44.232134 192.162277 1.00269 6/19/2024 12:35:48 6.284165 44.385543 192.11644 1.004271 6/19/2024 12:35:55 6.204994 49.010185 192.234955 1.006271 6/19/2024 12:36:02 4.516721 161.461139 192.264023 1.003654 6/19/2024 12:36:10 3.988237 196.001715 192.162277 1.008795 6/19/2024 12:36:18 4.094016 190.818945 192.191345 1.0037 6/19/2024 12:36:25 5.56832 95.996863 192.191345 1.000716 6/19/2024 12:36:33 5.715335 84.832993 192.236771 1.002306 6/19/2024 12:37:25 5.712776 83.086709 192.198608 1.002982 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 15:52:17 523.29707 496.054031 500.832464 191.884888 1.004622 6/19/2024 15:50:38 98.938884 192.075058 0.994474 6/19/2024 15:52:24 525.621118 497.988062 495.946925 191.769806 0.999156 6/19/2024 15:50:45 96.963045 192.133209 0.996723 6/19/2024 15:52:32 520.829231 495.085927 494.664098 191.75528 1.006959 6/19/2024 15:50:53 99.505368 192.075058 0.995392 6/19/2024 15:52:39 522.640259 496.324076 498.093296 191.740738 1.003471 6/19/2024 15:51:00 98.907832 192.075058 0.996218 6/19/2024 15:52:47 521.931014 496.160487 495.64519 191.798889 1.003746 6/19/2024 15:51:08 98.342656 192.04599 0.993556 6/19/2024 15:52:54 521.941197 497.278816 492.788837 191.769806 1.003517 6/19/2024 15:51:15 99.213064 192.075058 0.99149 6/19/2024 15:53:02 522.752214 497.914737 495.496218 191.753464 1.002346 6/19/2024 15:51:23 97.808523 192.071426 0.997205 6/19/2024 15:53:09 522.263575 496.113096 494.024005 191.784348 1.005307 6/19/2024 15:51:30 97.179633 192.075058 0.993464 6/19/2024 15:53:17 521.616917 494.782687 497.389881 191.769806 1.007143 6/19/2024 15:51:38 98.974743 192.0896 0.995025 6/19/2024 15:53:24 523.933519 498.538165 500.60845 191.784348 1.001038 6/19/2024 15:51:46 98.194075 192.04599 0.994749 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 15:50:53 -0.118776 0.141533 -0.067799 192.075058 0.995392 6/19/2024 15:54:13 -0.80503 191.857025 0.991628 6/19/2024 15:51:00 -0.309412 0.021388 0.419583 192.075058 0.996218 6/19/2024 15:54:20 0.02373 191.842484 0.993693 6/19/2024 15:51:08 -0.332288 0.356526 -0.44843 192.04599 0.993556 6/19/2024 15:54:28 -0.790109 191.827957 0.988323 6/19/2024 15:51:15 -0.371521 0.085878 1.131088 192.075058 0.99149 6/19/2024 15:54:35 -1.117634 191.813416 0.990067 6/19/2024 15:51:23 -0.14978 0.141641 -1.020729 192.071426 0.997205 6/19/2024 15:54:43 0.250636 191.900635 0.991857 6/19/2024 15:51:30 -0.400711 -0.032776 0.170205 192.075058 0.993464 6/19/2024 15:54:50 -1.007877 191.855209 0.993068 6/19/2024 15:51:38 -0.455828 -0.127766 -0.62871 192.0896 0.995025 6/19/2024 15:54:58 -0.40516 191.842484 0.993739 6/19/2024 15:51:46 -0.281512 -0.079998 0.418371 192.04599 0.994749 6/19/2024 15:55:05 -0.951174 191.842484 0.997044 SAMPLE SPIKE RECOVERY POST SYSTEM CAL POST SYSTEM ZERO PRE TEST 1 495.6 6.3 44.2 5.7 84.8 0.097 75.9% Sensor Analyzer Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Error (%)Error (%) NOx 489.5 493.4 0.0 -0.79 0.00 CO 513.4 520.2 0.1 -1.31 0.02 Propane 495.6 495.6 0.3 0.01 0.06 Ethylene 99.3 101.9 -0.2 -2.60 -0.19 Sensor System Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%) NOx 493.0 493.4 0.0 -0.07 0.00 CO 516.7 520.2 0.1 -0.66 0.02 Propane 499.4 495.6 0.2 0.77 0.04 Ethylene*98.3 101.9 0.0 -3.55 0.00 Sensor System Cal Zero Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%)Drift Error (%)Drift Error (%) NOx 498.5 493.4 0.1 1.04 0.02 1.12 0.02 CO 523.9 520.2 -0.3 0.72 -0.06 1.38 0.08 Propane 500.6 495.6 -0.1 1.01 -0.01 0.24 0.05 Ethylene*98.2 101.9 -0.5 -3.64 -0.48 0.09 0.48 *CTS Scans are conducted with Ethylene through the sample line. Lf 5.11 Lr Cr Tr Pr Lr/Lf 5.44 99.3 192.2 1.0 1.06 Ls Cs Ts Ps Ls/Lf 5.46 98.3 192.2 1.0 1.07 % Recovery Propane PRE DIRECT CAL FTIR QA/QC SUMMARY SAMPLE RECOVERY CALCULATIONS Period Spike #Concentration of Propane Cylinder Stack CO2 Concentration Pathlength Stack Propane Concentration Stack + Spike CO2 Concentration Stack + Propane Concentration DF Calculated POST SYSTEM CAL PRE SYSTEM CAL CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number:E02NI99E15W0051 Reference Number:153-402577489-1 Cylinder Number:CC486070 Cylinder Volume:144.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG PGVP Number:B72022 Valve Outlet:660 Gas Code:NO2,BALN Certification Date:Nov 08, 2022 Expiration Date:Nov 08, 2025 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates NITROGEN DIOXIDE 150.0 PPM 146.6 PPM G1 +/- 2.0% NIST Traceable 11/01/2022, 11/08/2022 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 15340120215 CC511005 59.52 PPM NITROGEN DIOXIDE/NITROGEN 1.4%Dec 17, 2024 PRM 12397 D887665 74.2 PPM NITROGEN DIOXIDE/AIR 1.3%Feb 02, 2022 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration MKS FTIR NO2 018143349 FTIR Nov 01, 2022 Triad Data Available Upon Request PERMANENT NOTES:OXYGEN ADDED TO MAINTAIN STABILITY Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD Part Number:X02NI99P15AD524 Reference Number:153-402622613-1 Cylinder Number:CC173895 Cylinder Volume:140.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG Analysis Date:Dec 22, 2022 Valve Outlet:350 Lot Number:153-402622613-1 Expiration Date:Dec 22, 2025 Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. ANALYTICAL RESULTS Component Req Conc Actual Concentration Analytical (Mole %)Uncertainty ETHYLENE 100.0 PPM 101.9 PPM +/- 1% NITROGEN Balance Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 Finley – North Randlett 6-19-2024 Finley – North Randlett 6-19-2024 Finley – North Randlett 6-19-2024 Spectral Fit Run 1 Spectral Fit Run 2 Spectral Fit Run 3 Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000139.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000068.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 59.74 3.76 -0.24 0.33 5.11 5.11 -2.12 --0-2795 1.05 Good NO2 191C 15.76 0.3 -0.03 0.03 0.32 0.32 -0.32 --0-488 1.06 Good N2O 191C -0.01 0.36 0.12 0.03 0.03 0.42 0.42 0.12 0.34 0 0.04 0-200 -Close to DL NH3 TE 191C 9.6 41.85 6.96 4.14 7.06 71.43 71.43 8.92 37.65 1.96 2.32 0-2995 -Close to DL H2O% (HIGH) 191C11.04 0.26 -0.02 0.03 0.43 0.43 -0.22 --0-40 -Good FORMALDEHYDE 191C6.72 0.92 6.13 0.24 0.27 1.04 1.04 6.88 6.88 0.75 2.04 0-69 -Close to DL FORMIC ACID 191C TE3.2 12.78 3.11 1.56 1.83 14.97 14.97 3.86 11.19 0.75 1.04 0-466 -Close to DL CH4 2900 CM-1 191C778.12 27.12 -1.69 2.46 52.27 52.27 -15.71 --0-3143 1 Good PROPANE 191C42.78 1.56 -0.22 0.27 1.87 1.87 -0.86 --0-4976 0.95 Good PROPYLENE 191C TE-1.01 12.91 2.27 1.57 1.86 15.27 15.27 2.43 11.33 0.16 0.76 0-194 -Close to DL ETHANE 191C 78.97 3.68 -0.55 0.85 5.73 5.73 -1.76 --0-1004 -Good ETHYLENE 191C TE20.51 21.68 21.93 2.07 2.55 26.1 26.1 24.58 24.58 2.64 7.31 0-900 -Close to DL CO PPM 191C (1OF2)3.45 1.24 3.95 0.26 0.57 2.68 2.68 4.53 4.53 0.58 1.32 0-5010 1.05 Close to DL CO2% 191C 6.25 0.16 -0.01 0.02 0.22 0.22 -0.12 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.67 2.5 1.6 0.64 0.82 3.21 3.21 1.91 1.91 0.32 0.53 0-186 1 Close to DL ACETYLENE 191C-0.1 4.83 0.77 0.79 1.05 6.38 6.38 0.8 4.08 0.04 0.26 0-1016 -Close to DL SO2 191C 1.65 2.04 1.72 0.26 0.32 2.48 2.48 1.98 1.98 0.26 0.57 0-964 1.02 Close to DL HEXANE 191C 4.16 1.13 4.68 0.13 0.18 1.53 1.53 5.19 5.19 0.51 1.56 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000200.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000068.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 59.49 3.61 -0.24 0.33 4.91 4.91 -2 --0-2795 1.05 Good NO2 191C 15.56 0.32 -0.03 0.03 0.34 0.34 -0.31 --0-488 1.06 Good N2O 191C -0.01 0.37 0.12 0.03 0.03 0.43 0.43 0.12 0.35 0 0.04 0-200 -Close to DL NH3 TE 191C 7.58 40.87 6.96 4.14 7.06 69.76 69.76 8.92 36.73 1.96 2.32 0-2995 -Close to DL H2O% (HIGH) 191C10.84 0.26 -0.02 0.03 0.42 0.42 -0.22 --0-40 -Good FORMALDEHYDE 191C6.71 0.9 6.13 0.24 0.27 1.01 1.01 6.88 6.88 0.75 2.04 0-69 -Close to DL FORMIC ACID 191C TE3.3 12.78 3.11 1.56 1.83 14.97 14.97 3.86 11.18 0.75 1.04 0-466 -Close to DL CH4 2900 CM-1 191C772.09 26.97 -1.69 2.46 51.98 51.98 -15.6 --0-3143 1 Good PROPANE 191C43.58 1.54 -0.22 0.27 1.85 1.85 -0.87 --0-4976 0.95 Good PROPYLENE 191C TE-0.57 12.83 2.27 1.57 1.86 15.17 15.17 2.43 11.26 0.16 0.76 0-194 -Close to DL ETHANE 191C 79.18 3.67 -0.55 0.85 5.72 5.72 -1.76 --0-1004 -Good ETHYLENE 191C TE20.65 21.43 21.93 2.07 2.55 25.8 25.8 24.58 24.58 2.64 7.31 0-900 -Close to DL CO PPM 191C (1OF2)3.47 1.19 3.95 0.26 0.57 2.57 2.57 4.53 4.53 0.58 1.32 0-5010 1.05 Close to DL CO2% 191C 6.28 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.89 2.44 1.6 0.64 0.82 3.14 3.14 1.91 1.91 0.32 0.53 0-186 1 Close to DL ACETYLENE 191C0.05 4.73 0.77 0.79 1.05 6.25 6.25 0.8 3.98 0.04 0.26 0-1016 -Close to DL SO2 191C 1.15 2.14 1.72 0.26 0.32 2.61 2.61 1.98 1.98 0.26 0.57 0-964 1.02 Close to DL HEXANE 191C 4.39 1.12 4.68 0.13 0.18 1.52 1.52 5.19 5.19 0.51 1.56 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000261.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000068.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\NR CS E2 6-19-24\FINLEY NR CS E2 6-19-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 60.22 3.63 -0.24 0.33 4.94 4.94 -2.01 --0-2795 1.05 Good NO2 191C 15.6 0.29 -0.03 0.03 0.31 0.31 -0.31 --0-488 1.06 Good N2O 191C 0 0.36 0.12 0.03 0.03 0.42 0.42 0.12 0.34 0 0.04 0-200 -Close to DL NH3 TE 191C 9.54 41.07 6.96 4.14 7.06 70.09 70.09 8.92 36.87 1.96 2.32 0-2995 -Close to DL H2O% (HIGH) 191C11.01 0.25 -0.02 0.03 0.41 0.41 -0.22 --0-40 -Good FORMALDEHYDE 191C6.62 0.97 6.13 0.24 0.27 1.1 1.1 6.88 6.88 0.75 2.04 0-69 -Close to DL FORMIC ACID 191C TE2.94 13.04 3.11 1.56 1.83 15.26 15.26 3.86 11.45 0.75 1.04 0-466 -Close to DL CH4 2900 CM-1 191C765.52 24.27 -1.69 2.46 46.78 46.78 -15.31 --0-3143 1 Good PROPANE 191C43.56 1.59 -0.22 0.27 1.91 1.91 -0.87 --0-4976 0.95 Good PROPYLENE 191C TE0.06 13.27 2.27 1.57 1.86 15.7 15.7 2.43 11.73 0.16 0.76 0-194 -Close to DL ETHANE 191C 78.36 3.77 -0.55 0.85 5.87 5.87 -1.8 --0-1004 -Good ETHYLENE 191C TE19.86 21.97 21.93 2.07 2.55 26.45 26.45 24.58 24.58 2.64 7.31 0-900 -Close to DL CO PPM 191C (1OF2)3.5 1.21 3.95 0.26 0.57 2.61 2.61 4.53 4.53 0.58 1.32 0-5010 1.05 Close to DL CO2% 191C 6.34 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.92 2.56 1.6 0.64 0.82 3.29 3.29 1.91 1.91 0.32 0.53 0-186 1 Close to DL ACETYLENE 191C-0.12 5.03 0.77 0.79 1.05 6.64 6.64 0.8 4.27 0.04 0.26 0-1016 -Close to DL SO2 191C 1.72 2.06 1.72 0.26 0.32 2.51 2.51 1.98 1.98 0.26 0.57 0-964 1.02 Close to DL HEXANE 191C 4.27 1.15 4.68 0.13 0.18 1.55 1.55 5.19 5.19 0.51 1.56 0-1000 -Close to DL APPENDIX C Test Run Load %Site Rated Load, bhp Load Approx., bhp 1 70 1380 966.0 2 70 1380 966.0 3 70 1380 966.0 Engine Load Approximation based on Panel Levels APPENDIX D Test Run Flowrate dscfm Approx. BHP Avg O2 % NOx ppmvd NOx g/bhp-hr NOx lbs/hr CO ppmvd CO g/bhp-hr CO lbs/hr NMNEHC ppmvd NMNEHC g/bhp-hr NMNEHC lbs/hr Moisture Content % 1 1672.92 966.0 5.7 82.52 0.46 0.99 3.76 0.01 0.03 72.96 0.39 0.84 10.80 2 1631.48 966.0 6.0 83.84 0.46 0.98 3.81 0.01 0.03 72.68 0.38 0.81 10.84 3 1669.67 966.0 5.9 84.64 0.48 1.01 3.87 0.01 0.03 72.63 0.39 0.83 10.93 966.0 5.9 83.66 0.47 0.99 3.82 0.01 0.03 72.76 0.39 0.83 10.86 Summary Average Levels Example Calculations: Uinta Wax Operating, LLC, North Randlett Compressor Station, #2 The following is a step-by-step calculation for the first test run conducted on the North Randlett Compressor Station #2. Test Parameters • Stack Diameter = 14 inches • Traverse Points = 16 • Ports = 2 • Barometric Pressure = 25.11 in Hg • Average O2 = 5.7% • Average CO2 = 6.9% • Load Approximation = 966.0 bhp • Moisture Content = 10.80% EPA 40 CFR 60(A) Methods 1-3: Determination of Stack Gas Velocity and Flow Rate Dry Molecular Weight (lb/lbmol) = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) Where: %CO2 – Carbon Dioxide Content Of The Gas = 6.9% %O2 – Oxygen Content Of The Gas = 5.7% %N2 – Nitrogen Content Of The Gas %CO – Carbon Monoxide Content Of The Gas (%N2 +%CO) = (100 - %O2 - %CO2) = (100 – 5.7 – 6.9) = 87.4% Dry = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) = (0.44 * 6.9) + (0.32 * 5.7) + (0.28 * 87.4) = 29.33 lb/lbmol Wet Molecular Weight (lb/lbmol) = MD * (1-BWS) + (18) * BWS Where: MD – Molecular Weight Of The Dry Gas (lb/lbmol) = 29.33 lb/lbmol BWS – Moisture Content Of The Gas (%/100) = 10.80% = MD * (1-BWS) + (18) * BWS = 29.33 * (1 – (10.80/ 100)) + (18 * (10.80/ 100)) = 28.11 lb/lbmol Average Stack Gas Velocity (ft/sec) = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) Where: CP – Pitot tube constant (unitless) = 0.84 ∆PAVG – Average square root of the stack gas pitot DP (inches water) = 0.981 in H2O TS – Average stack temperature (R) = 1617 R PB – Barometric pressure (in Hg) = 25.11 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O MA – Molecular weight of the wet gas (lb/lbmol) = 28.11 lb/lbmol = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) = 0.84 * (85.49) * 0.981 * ( 1617 / (((0.3/ 13.6) + 25.11) * 28.11)) = 106.61 ft/sec Average Dry Flowrate (dscfm) = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 Where: DS – Diameter of the stack (inches) = 14 inches BWS – Moisture content of the gas (%) = 10.80% TSTD – Standard temperature (528R) TS – Average stack temperature (R) = 1617 R PB – Barometric pressure (in Hg) = 25.11 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O VS– Average Stack gas velocity (ft/sec) = 106.61 ft/sec = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 = 60 * (1 - (10.80/ 100)) * 106.61 * * (((14 / 2) / 12))2) * 528 / 1617 * (25.11 + (0.3 / 13.6)) / 29.92 = 1672.92 dscfm Conversion of Dry Flowrate to m3/hr = Q * 60 * 2.83168*10 -2 Where: Q – Volumetric Flowrate = 1672.92 dscfm 2.83168*10 -2 – Conversion factor for cubic feet to cubic meter 60 – Minutes in an hour = Q * 60 * 2.83168*10 -2 = 1672.92 *60 * 2.83168*10 -2 = 2842.3 m3/hr ASTM D 6348-03: Determination of NOx, CO and VOC Emissions From Stationary Sources NOx Emission Rate (g/Bhp-hr) = (Cd * 1.912*10 -3 * Q * T) / HP-hr Where: Cd – Measured NOx concentration in ppm = 82.52 ppm 1.92*10 -3 - Conversion constant for ppm to g/m3 NOx Q – Volumetric Flowrate = 2842.3 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 966.0 Bhp = (Cd * 1.912*10 -3 * Q * T) / HP-hr = (82.52 * 1.912*10 -3 * 2842.3 * 1) / 966.0 = 0.46 g/Bhp-hr NOx Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.46 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 966.0 Bhp = g/Bhp-hr / 454 * Bhp = 0.46 / 454 * 966.0 = 0.99 lbs/hr CO Emission Rate (g/Bhp-hr) = (Cd * 1.164*10 -3 * Q * T) / HP-hr Where: Cd – Measured CO concentration in ppm = 3.76 ppm 1.164*10 -3 - Conversion constant for ppm to g/m3 CO Q – Volumetric Flowrate = 2842.3 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 966.0 Bhp = (Cd * 1.164*10 -3 * Q * T) / HP-hr = (3.76 * 1.164*10 -3 * 2842.3 * 1) / 966.0 = 0.01 g/Bhp-hr CO Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.01 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 966.0 Bhp = g/Bhp-hr / 454 * Bhp = 0.01 / 454 * 966.0 = 0.03 lbs/hr VOC Emission Rate (g/Bhp-hr) = (Cd * 1.833*10 -3 * Q * T) / HP-hr Where: Cd – Measured VOC concentration in ppm = 72.96 ppm 1.833*10 -3 - Conversion constant for ppm to g/m3 VOC Q – Volumetric Flowrate = 2842.3 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 966.0 Bhp = (Cd * 1.833*10 -3 * Q * T) / HP-hr = (72.96 * 1.833*10 -3 * 2842.3 * 1) / 966.0 = 0.39 g/Bhp-hr VOC Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.39 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 966.0 Bhp = g/Bhp-hr / 454 * Bhp = 0.39 / 454 * 966.0 = 0.84 lbs/hr APPENDIX E FTIR Engine Test Sheet Company Name F".\\e" Location / Unit 1.0. .Aff'.\l~ '(1..hof\AI~t+ 3x'lhr David Martinez V\"Ie.-J~;';;:';: l.. -'(.\ -~t\ c.~ t). Type of Test Completed Field Technician (5) Client Rep and/or State Reo Date Non-Resettable Run Time Hours EnQine Make EnQine Model Enaine SIN Port Distance A Port Distance B Exhaust Diameter (inches) Calibration Gas NO (ppm) CO (ppm) Propane (ppm) N02 (ppm) Ethylene (ppm Methane (ppm Acetaldehyde :ppm) (J4.T \1,\ \ Cvlinder# CC453965 CC453965 CC453965 CC486070 CC173895 CC453965 CC321163 Concentration 493.4 520.2 495.6 146.6 101.9 499.4 196.7 Stack Diagram Test 1 Test 2 Test 3 Time of Readina \'~;~'6 \;l.:>~ ~;l.fo Atm Pressure (in Ha) ~S,lf ~S,l/ )..5.11 Atm Temp CF) "60 '6:~ )s'-S Enaine RPM ~ \15 d.. ns ~ H&.I~ *Manifolp Pres. Vac(It) or BOoSt(p~) or Boost (psia) ().., ~~ '''0\ Manifold Temp (OF) :set' \t[7'J I" &' Psuction (psi) Stage 1 \1> H, \b Tsuction CF) Stage 1 _. Pdischarc e (psi) Staae 1 '7' "-:7~ I/~ Psuction (psi) StaQe 2 \ Tsuction OF) Stage 2 \ Pdischarc e (psi) Staae 2 ~\. I ~~G1 'd..110 Psuction :psi) Stage 3 \ I I Tsuction OF) Staae 3 I I Pdischar Je (psi) Staae 3 1ST1 ft16tt ~b7.., Psuction [psi) StaQe 4 \ ) Tsuction OF) Stage 4 I I Pdischarge (psi) Stage 4 Gas Throuahput (mmcf/d) or ( VY1 FF llTlkf' '), ~15 ~ ~CI ~Sl Pre Cat Temp CF) \ ~I \\ ~~ , \).'l Post Cat Temp CF) ~'l l hO \' ~c\ Cat Differential Pres. (It of H2O) '"1.lA u,~-Ii ,q Humidity% \'1 .1t.. \ \.7 02% 5·1 ~.o S.~ C02 % Dry ---c,er 1,0 /'0LOAD % (~n~or (Estimated) 70 -,C) 70 IQnition TimrrmTF) ~,1r ~Vl\c( ')..O.~· AFR Setting mV (I l!>'3:l ~f1K) ~'6',1 ~'€.T '),.~ \ \ AFR Settina mV ank) . -_. ' Rev 8 * Some units show boost in inches of Hg. In this situation please indicate if it is positive (+) or negative(-). Eg: (+12") or (-5") 9/17/2019 Worksheet: O2 Stratification Client:Finley Location:North Randlett E2 Date:6/19/2024 PD:14 DD:48 YES Method 1 Criteria Met UD:120 YES Method 1 Criteria Met Port Point Insertion Depth Reading (inches)(%) A 1 2.32 5.70 A 2 7.00 6.00 A 3 11.66 5.90 A 4 A 5 A 6 A 7 A 8 A 9 A 10 A 11 A 12 Average 5.87 Notes: To demonstrate non-stratified flow and utilize one sampling location O2 may not deviate by more than +/- 0.3% of the average O2 concentration. EPA REFERENCE METHOD 3A (Determination Of Stratification) COMPANY NAME:Finley COMPANY LOCATION:North Randlett E2 DATE:6/19/2024 STACK DIAMETER (inches):14 TRAVERSE POINTS:16 2 TEST RUN #1 TEST RUN #2 TEST RUN #3 AVERAGE O2:5.7 AVERAGE O2:6 AVERAGE O2:5.9 AVERAGE CO2:6.9 AVERAGE CO2:7 AVERAGE CO2:7 BARO PRESSURE:25.11 BARO PRESSURE:25.11 BARO PRESSURE:25.11 Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O) 1 0.5 0.91 1157 0.29 1 0.5 0.82 1160 0.3 1 0.5 0.89 1159 0.3 2 1.47 0.93 2 1.47 0.88 2 1.47 0.91 3 2.716 0.95 3 2.716 0.92 3 2.716 0.94 4 4.522 0.99 4 4.522 0.95 4 4.522 0.99 5 9.478 1.04 5 9.478 0.99 5 9.478 1.02 6 11.284 0.96 6 11.284 0.96 6 11.284 0.98 7 12.53 0.94 7 12.53 0.93 7 12.53 0.98 8 13.5 0.92 8 13.5 0.93 8 13.5 0.95 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 1 0.5 0.93 1157 0.29 1 0.5 0.85 1160 0.3 1 0.5 0.91 1159 0.3 2 1.47 0.94 2 1.47 0.87 2 1.47 0.93 3 2.716 0.97 3 2.716 0.9 3 2.716 0.97 4 4.522 0.99 4 4.522 0.93 4 4.522 1.03 5 9.478 1.02 5 9.478 0.97 5 9.478 1.01 6 11.284 0.98 6 11.284 0.95 6 11.284 0.97 7 12.53 1 7 12.53 0.94 7 12.53 0.98 8 13.5 0.94 8 13.5 0.92 8 13.5 0.96 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 Source Test Report For Uinta Wax Operating, LLC North Randlett Compressor Station Uintah County, Utah Test Date: June 19, 2024 Report Date: July 2, 2024 UDEQ Permit: #DAQE-AN159380002-23 Engine: Caterpillar G3516J SN: JEF01637 Unit ID: #4 Prepared By: Oasis Emission Consultants, Inc. 2730 Commercial Way Rock Springs, WY 82901 July 2, 2024 Ms. Karen Pratt Uinta Wax Operating, LLC Dear Ms. Pratt: Re: Engine Emission Testing For Uinta Wax Operating, LLC, North Randlett Compressor Station, Unit #4, Permit #DAQE-AN159380002-23. An air emissions test program was conducted on a Caterpillar G3516J engine, operated by Uinta Wax Operating, LLC and designated as Unit #4, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate source emission testing with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC). Oasis Emission Consultants, Inc. conducted the testing on June 19, 2024. UDEQ Permit #DAQE-AN159380002-23 Emission Levels The average recorded levels were found to comply with emission levels stipulated in the permit, as shown in the attached report and summarized below. Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC ppm @ 15% O2 28.81 41 7.81 61 23.45 60 lbs/hr 0.99 1.52 0.16 1.37 0.77 2.13 *VOC levels reported as non-methane, non-ethane hydrocarbon on a propane basis (NMNEHC C3). EPA 40 CFR 60, Subpart JJJJ Emission Levels Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC g/bhp-hr 0.46 1.0 0.08 2.0 0.36 0.7 Catalyst Parameters (Averaged Over 3 Test Runs) Inlet Temp (deg F) DP (in H2O) 736 6.2 Engine Load (Averaged Over 3 Test Runs) Rated BHP Operating BHP % Load 1379 979.1 71.0 Testing Protocol The attached report was generated using an extractive FTIR system using methodologies as required by and in accordance with EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, as outlined in the submitted Source Test Protocol. Quality Assurance Oasis has performed a full review of the raw data and calculated results in this report. Any errors we have encountered have been listed in the body of this report. After performing the review, we are confident that this engine has met all requirements. If you have any questions or require further information, please contact the undersigned at (307) 382-3297. Yours truly, Oasis Emission Consultants, Inc. _________________________ _______________________ Charles A. Chapman Crystal Leonard Manager of Technical Services Senior EHS Specialist _________________________ Christopher N. Knott, P.Eng. Director, Engineering and Operations SOURCE EMISSION TEST REPORT UDEQ Permit #DAQE-AN159380002-23 Test Performed By: Oasis Emission Consultants, Inc. Test Company Contact: Chris Knott 2730 Commercial Way Rock Springs, WY 82901 307.382.3297 Owner/Operator: Uinta Wax Operating, LLC Owner/Operator Contact: Karen Pratt (720) 990-9927 Facility Name: North Randlett Compressor Station UTM Coordinates: 593,702 m Easting, 4,453,005 m Northing UTM Zone 12 Uintah County, Utah Emission Source: Caterpillar G3516J Unit #4 Date of Test: June 19, 2024 Date of Report: July 2, 2024 TABLE OF CONTENTS 1.1 Introduction .......................................................................................................................... 1 2.1 Stack Sampling Location ..................................................................................................... 2 3.1 Discussion of NOx, CO and VOC Test Results ................................................................... 3 3.1.1 Source Test 1 ............................................................................................................................................ 3 3.1.2 Source Test 2 ............................................................................................................................................ 3 3.1.3 Source Test 3 ............................................................................................................................................ 3 4.1 Stack Sampling Methods and Procedures ............................................................................ 4 4.2 Equipment Utilization .......................................................................................................... 5 4.3 Measurement of VOC (NMNEHC C3) ............................................................................... 6 4.4 Process Parameters............................................................................................................... 6 5.1 Quality Assurance ................................................................................................................ 7 List of Tables and Figures Figure 1 - Sample Port Location ............................................................................................................................. 2 Figure 2 - Sampling Train Schematic-Method 320 ................................................................................................ 5 Table 1 - Insertion Depths of Traverse Points for Stratification Test ..................................................................... 2 Table 2 - Test Matrix .............................................................................................................................................. 4 Table 3 - Concentrations and Interference .............................................................................................................. 5 APPENDIX A: NOx, CO and VOC Test Data APPENDIX B: Quality Assurance/Calibration Data APPENDIX C: Load Approximation APPENDIX D: Example Calculations and Summary APPENDIX E: Field Notes 1 1.1 Introduction An air emissions test program was conducted on a Caterpillar G3516J engine, operated by Uinta Wax Operating, LLC and designated as Unit #4, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate source emission testing with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC) defined as non-methane, non-ethane hydrocarbons, reported as propane (NMNEHC C3). The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Three one hour test runs were performed on June 19, 2024 to analyze NOx, CO and VOC emission levels. Test runs were performed according to methodologies outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320 as outlined in the submitted Source Test Protocol dated May 17, 2024. Each one hour test run consisted of 60 readings taken at one minute intervals. Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. The following key personnel were present during testing: David Martinez, OEC Kyle 2 2.1 Stack Sampling Location The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Testing was conducted on the Caterpillar G3516J engine. The sampling port for moisture, NOx, CO and VOC measurements was approximately 2.5 pipe diameters (40”) downstream from the nearest flow disturbance (Distance B) and 0.5 pipe diameters (8”) upstream from the nearest disturbance (Distance A), as seen in Figure 1. The stack sampling location was placed at approximately 50% insertion depth based on an O2 stratification check which demonstrated a non-stratified flow regime. The stratification was conducted according to EPA 40 CFR 75(A), §6.5.6.1 using 3 traverse points determined according to Table 1 below. Figure 1 - Sample Port Location Table 1 - Insertion Depths of Traverse Points for Stratification Test Traverse Point Insertion Depth (Percent of Stack Diameter) 1 16.6 2 50.0 3 83.3 16" A B Oxidation Catalyst 3 3.1 Discussion of NOx, CO and VOC Test Results Three, one hour test runs were performed on June 19, 2024 to analyze exhaust NOx, CO and VOC (NMNEHC C3) emission levels to demonstrate source emission testing with the emissions limits contained in the WDEQ Permit #DAQE-AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ. Testing for NOx, CO and VOC were run concurrently with one another. Each test was performed at the maximum achievable load. Measured emissions were below permitted limits. Please refer to the Appendices for a listing of all raw data, calibration error response and calculations performed per EPA 40 CFR 60(A) requirements. 3.1.1 Source Test 1: Caterpillar G3516J, NOx, CO and VOC The first test was performed from 7:37 to 8:36 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 979.1 bhp, and the average NOx and CO levels were found to be 0.46 g/bhp-hr and 0.08 g/bhp-hr respectively, below limitations. The VOC level tested at 0.36 g/bhp- hr, which tested in compliance. 3.1.2 Source Test 2: Caterpillar G3516J, NOx, CO and VOC The second test was performed from 8:38 to 9:37 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 979.1 bhp, and the average NOx and CO levels were found to be 0.46 g/bhp-hr and 0.08 g/bhp-hr respectively, below limitations. The VOC level tested at 0.36 g/bhp- hr, which tested in compliance. 3.1.3 Source Test 3: Caterpillar G3516J, NOx, CO and VOC The third test was performed from 9:39 to 10:39 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 979.1 bhp, and the average NOx and CO levels were found to be 0.46 g/bhp-hr and 0.08 g/bhp-hr respectively, below limitations. The VOC level tested at 0.36 g/bhp- hr, which tested in compliance. Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 1 73.51 0.46 20.01 0.08 59.73 0.36 5.7 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 2 73.07 0.46 19.82 0.08 59.40 0.36 5.9 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 3 73.13 0.46 19.74 0.08 59.70 0.36 6.1 4 4.1 Stack Sampling Methods and Procedures Testing followed EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, with no exceptions. Table 2 - Test Matrix Method Title Parameter Reference EPA 40 CFR 60 Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources Sampling Point Determination https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_1_3.pdf EPA 40 CFR 60 Appendix A, Method 2 Determination of Stack Gas Velocity and Volumetric Flow Rate Exhaust Effluent Flow https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_2.pdf EPA 40 CFR 60 Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight O2, CO2, Dry Volumetric Flow Rate https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_3.pdf EPA 40 CFR 63 Appendix A, EPA Method 320 Vapor Phase Organic and Inorganic Emissions by Extractive FTIR Nitrogen Oxides, Carbon Monoxide, Non- Methane Non- Ethane Hydrocarbons on a Propane Basis https://www.epa.gov/ emc/method-320- vapor-phase-organic- and-inorganic- emissions-extractive- ftir United States. U.S. Environmental Protection Agency. “EMC Promulgated Test Methods.” Air Emission Measurement Center (EMC). 31 August 2023. Web. 2 July 2024. <https://www.epa.gov/emc/emc-promulgated-test-methods>. ASTM International. “Standards & Publications.” All Environment Standards. Web. 2 July 2024. <https://www.astm.org/Standards/D6348.htm>. 5 4.2 Equipment Utilization The following equipment was used during the tests performed at this facility in conjunction with procedures outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320. • (1) MKS MultiGas 2030 FTIR Continuous Gas Analyzer (0.210 L/min sample flow, 0.014 atmosphere sample pressure, 1 atmosphere cell pressure, 191°C cell temperature) • (1) Laptop Computer for the FTIR Analyzer using MKS MG2000 Software • (1) 75ft or 100ft Heated Teflon Line w/ Heated Sample Probe and Spike Bypass Line • S-Type Pitot Tube c/w 20 ft. Heated Sample Line (coefficient 0.84) • (1) Enerac 500 Portable O2/CO2 Analyzer • (1) Fyrite O2/CO2 Analyzer • (5) EPA Protocol G1 Calibration Gas (NOx, CO, C3H8, C2H4 and NO2) The MKS Multigas 2030 FTIR Analyzer operated with a spectral resolution of 0.5 cm-1 and a scan time of 30 seconds. The FTIR spectrometer utilizes a multi-pass gas cell with a 5.11 meter effective pathlength. Figure 2 - Sampling Train Schematic-Method 320 Table 3 - Concentrations and Interference 6 The MKS 2030 software provides a Natural Gas Method that is designed to minimize all expected interferences by removing the regions in the quant region where they are most absorbed (i.e. picket fence approach). So, for example, all the water peaks that are greater than about 0.1 abs are removed from the quant region. Since the spectral noise measured (sample spectrum) is in the range of 0.001 absorbance, it is desirable to have any error within this range. The MKS software will match the water calibration spectrum to the sample spectrum at any 1 point in the spectrum to about 1% precision. So, 1% of 0.1 absorbance is 0.001 abs. This is why any peaks greater than this for interfering compounds are usually excluded so they do not interfere. To summarize, the MKS software and the method are designed to minimize any interferences by removing their largest interfering absorptions. 4.3 Measurement of VOC (NMNEHC C3) The algorithm currently used for NMNEHC C3 and developed for natural gas fired applications by Dr. Spartz and MKS instruments in accordance with EPA standards, is the following: (2.4*c8/(1+exp((2-c8)/0.2))+1.9*c11/(1+exp((2-c11)/0.2))+6*c12/(1+exp((0.5-c12) /0.2))+2.85*c13/(1+exp((2-c13)/0.2))+3*c14/(1+exp((1-c14)/0.2)))/3 c8= acetylene c11= ethylene c12= hexane c13= propylene c14= propane Note: The constants in front of each of the compounds listed represents the FID response factor when calibrated with Propane. As with any CEMS analyzer, the FTIR may demonstrate a negative zero bias. The “exp” functions listed in the algorithm above are intended to mathematically filter out any negative biases and set them to approach zero. 4.4 Process Parameters Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. Results are provided in Appendix C. 7 5.1 Quality Assurance The MKS Multigas 2030 FTIR Analyzer was used to measure NOx, CO and VOC on a dry basis. A pre Direct and System calibration measurement was made on compounds of NOx, CO, C3H8 and C2H4. In addition, post System calibrations were made on compounds of NOx, CO, C3H8 and C2H4. Compounds of CO2 and C3H8 were measured for the quality assurance spiking requirements. Levels for calibrations and zeroes must be within +/- 5% of the certified calibration gas or response to zero gas, respectively. CTS procedures were followed according to EPA requirements for both pre and post testing. Similarly, QA spiking procedures were followed. Analysis of the CO2 exhaust effluent was used to determine the dilution factor. Steady levels of the CO2 were observed and a sufficient duration of time was allowed to elapse for a representative average. The calibration gas was spiked into the effluent stream using a bypass line at approximately 10% of the sampling rate. The dilution factor was obtained from observation of the stack CO2 behavior using the following equation: CO2AVG – CO2SPIKE DF = ------------------------ CO2 AVG Where: CO2AVG = The average undiluted CO2 stack gas concentration of spike measurements CO2SPIKE = The average diluted CO2 stack gas concentration when spiked The sample recovery was then obtained from the following equation: % REC = (Spike MEAS – Stack MEAS)* (1 – DF) --------------------------------------------------------- CS * DF Where: Spike MEAS = The average diluted stack gas concentration when spiked Stack MEAS = The average undiluted stack gas concentration DF = Dilution factor CS = Certified concentration of calibration standards The Sample Recovery average level for C3H8 was found to be 71.1%, which was within the allowable tolerance of Method 320 (70% to 130%). A summary of all spiking procedures/results can be found in Appendix B. APPENDIX A NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 51.508109 23.637873 75.145982 20.418257 61.106542 10.069884 7:37:44 06/19/2024 2 50.991215 23.476179 74.467394 20.276626 59.685252 10.383132 7:38:45 06/19/2024 3 50.372468 23.301441 73.673909 20.141155 60.190493 10.616884 7:39:45 06/19/2024 4 51.992897 24.003736 75.996633 20.330351 59.403077 10.9336 7:40:45 06/19/2024 5 50.92195 23.701099 74.623049 20.066938 60.449059 10.76939 7:41:45 06/19/2024 6 50.743018 23.627502 74.37052 20.18589 60.638118 10.767133 7:42:45 06/19/2024 7 49.906389 23.412407 73.318796 20.033249 59.332543 10.916007 7:43:45 06/19/2024 8 50.940933 23.887903 74.828836 20.171557 61.476228 11.151953 7:44:45 06/19/2024 9 50.458507 23.671369 74.129876 20.100451 58.990388 11.58885 7:45:45 06/19/2024 10 50.206675 23.417243 73.623918 20.19051 60.253982 12.012989 7:46:46 06/19/2024 11 50.37886 23.516773 73.895633 20.134042 60.157230 12.233986 7:47:46 06/19/2024 12 49.801594 22.991238 72.792832 19.986137 60.167785 12.458817 7:48:46 06/19/2024 13 50.873833 23.302568 74.176401 20.077345 59.245937 12.57691 7:49:46 06/19/2024 14 49.157312 22.582226 71.739538 19.994189 60.279627 12.670471 7:50:46 06/19/2024 15 50.429736 23.488015 73.917751 20.037597 59.794735 12.749179 7:51:46 06/19/2024 16 50.986987 23.88949 74.876477 20.020578 59.316819 12.775856 7:52:46 06/19/2024 17 51.340454 23.950993 75.291447 20.162759 59.598456 12.796023 7:53:46 06/19/2024 18 50.246901 23.460019 73.70692 20.177592 60.873211 12.754773 7:54:46 06/19/2024 19 48.961125 22.859221 71.820346 20.045631 60.297406 12.729646 7:55:46 06/19/2024 20 50.307818 23.429647 73.737465 19.969706 59.161719 12.598895 7:56:46 06/19/2024 21 50.719071 23.374747 74.093818 20.095449 59.532668 12.50788 7:57:47 06/19/2024 22 51.559624 23.628755 75.188379 19.921885 59.612994 12.211904 7:58:47 06/19/2024 23 49.545466 22.583625 72.129091 19.917792 60.590961 10.98096 7:59:47 06/19/2024 24 50.762081 23.342411 74.104492 20.034712 61.027842 10.77386 8:00:47 06/19/2024 25 51.375611 23.831046 75.206657 19.99252 59.931507 10.75422 8:01:47 06/19/2024 26 49.398272 22.842883 72.241155 19.919545 59.448408 10.823023 8:02:47 06/19/2024 27 49.500221 22.921824 72.422045 20.027841 60.046252 10.922487 8:03:47 06/19/2024 28 49.885958 23.036974 72.922932 20.023119 60.008401 10.995401 8:04:47 06/19/2024 29 50.523309 23.439198 73.962507 20.028477 59.891254 11.142533 8:05:47 06/19/2024 30 50.470245 23.449925 73.92017 20.031875 59.247800 11.238233 8:06:47 06/19/2024 31 49.566782 23.007933 72.574715 19.953819 59.904645 11.263288 8:07:47 06/19/2024 32 50.437882 23.352964 73.790846 19.94821 61.499686 11.260952 8:08:48 06/19/2024 33 51.30171 23.800967 75.102677 19.925673 59.368746 11.12016 8:09:47 06/19/2024 34 49.871043 23.083964 72.955007 20.03343 59.322793 11.069263 8:10:48 06/19/2024 35 49.717983 23.092457 72.81044 19.908833 60.914149 11.073411 8:11:48 06/19/2024 36 49.373574 22.960631 72.334205 19.849048 59.617367 11.116849 8:12:48 06/19/2024 37 49.848449 23.05735 72.905799 19.839708 60.164671 11.158258 8:13:48 06/19/2024 38 49.896838 23.044456 72.941294 19.938578 59.083753 11.216267 8:14:48 06/19/2024 39 50.3273 23.331876 73.659176 19.950155 58.148300 11.224169 8:15:48 06/19/2024 40 50.056612 23.279874 73.336486 19.931457 59.383854 11.155081 8:16:48 06/19/2024 41 50.249331 23.302576 73.551907 19.883526 59.687158 11.027999 8:17:48 06/19/2024 42 50.318669 23.372437 73.691106 19.894494 58.638738 11.04226 8:18:49 06/19/2024 43 49.126072 22.860323 71.986395 19.730168 60.131437 11.012811 8:19:48 06/19/2024 44 50.336605 23.505676 73.842281 19.868233 59.172010 11.051599 8:20:49 06/19/2024 45 49.46872 23.055314 72.524034 19.736415 59.838341 11.08972 8:21:49 06/19/2024 46 50.634116 23.486308 74.120424 19.941407 59.382776 11.11715 8:22:49 06/19/2024 47 49.627409 23.009174 72.636583 19.889683 59.044066 11.043101 8:23:49 06/19/2024 48 50.463877 23.276243 73.74012 20.018184 60.263471 10.98666 8:24:49 06/19/2024 49 50.426406 23.241094 73.6675 19.904395 59.163244 10.963168 8:25:49 06/19/2024 50 50.571521 23.262954 73.834475 19.94102 59.816107 10.977458 8:26:49 06/19/2024 51 50.109534 23.039519 73.149053 19.970145 59.096408 10.957317 8:27:49 06/19/2024 52 50.361161 22.966808 73.327969 20.143469 59.084642 10.947805 8:28:49 06/19/2024 53 50.652311 23.30541 73.957721 20.12054 57.939380 10.92681 8:29:49 06/19/2024 54 49.822626 22.680378 72.503004 20.01425 60.308905 10.938001 8:30:49 06/19/2024 55 50.195267 22.775589 72.970856 20.00952 59.097149 10.936901 8:31:50 06/19/2024 56 50.051335 22.682101 72.733436 19.995098 59.155816 10.936885 8:32:50 06/19/2024 57 49.988596 22.746316 72.734912 19.926919 59.264909 10.943347 8:33:50 06/19/2024 58 49.300554 22.533161 71.833715 19.834173 59.028963 10.938955 8:34:50 06/19/2024 59 49.458647 22.589205 72.047852 19.881956 59.492975 10.923476 8:35:50 06/19/2024 60 49.977809 22.839943 72.817752 19.947028 58.963314 10.941625 8:36:50 06/19/2024 AVG 50.26 0.00 73.51 20.01 59.73 11.32 ppm@15% O2 28.53 7.77 23.18 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.46 0.98 0.08 0.16 0.36 0.77 #4 FTIR Measurements Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 1 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 16 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.51 0.46 1200 0.23 0.678 Average O2 5.7 (% dry)A 2 1.68 0.50 0.707 Average CO2 7 (% dry)A 3 3.10 0.54 0.735 Average N2 + CO 87.3 (% dry)A 4 5.17 0.59 0.768 Dry Molecular Weight 29.35 lb/lbmol A 5 10.83 0.59 0.768 Wet Molecular Weight 28.06 lb/lbmol A 6 12.90 0.55 0.742 EPA REFERENCE METHOD 320 A 7 14.32 0.51 0.714 Barometric Pressure 25.13 in Hg A 8 15.49 0.48 0.693 Moisture Content 11.32 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 73.51 ppm A 11 Calculated NOx Mass Output 0.98 lbs/hr A 12 Calculated NOx Output 0.46 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 20.01 ppm A 15 Calculated CO Mass Output 0.16 lbs/hr A 16 Calculated CO Output 0.08 g/bhp-hr B 1 0.51 0.44 1200 0.23 0.663 EPA REFERENCE METHOD 320 B 2 1.68 0.48 0.693 Average Analyzer NMNEHC Level 59.73 ppm B 3 3.10 0.53 0.728 Calculated NMNEHC Mass Output 0.77 lbs/hr B 4 5.17 0.57 0.755 Calculated NMNEHC Output 0.36 g/bhp-hr B 5 10.83 0.60 0.775 LOAD APPROXIMATION B 6 12.90 0.56 0.748 Estimated Engine Load 979.1 BHP B 7 14.32 0.56 0.748 B 8 15.49 0.52 0.721 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.5 1200 0.2 0.727 Average Stack Gas Velocity 68.10 ft/sec Average Dry Flowrate 1871.07 dscfm TEST RUN # 1 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 50.084971 22.944562 73.029533 19.973203 59.267954 10.933974 8:38:50 06/19/2024 2 48.987651 22.43485 71.422501 19.76785 58.426234 10.921885 8:39:50 06/19/2024 3 51.847653 23.860434 75.708087 20.026917 59.119270 10.957768 8:40:51 06/19/2024 4 48.913546 22.479933 71.393479 19.817541 59.083101 10.925352 8:41:50 06/19/2024 5 49.337892 22.632902 71.970794 19.839278 59.388072 10.925598 8:42:50 06/19/2024 6 50.631899 23.119085 73.750984 19.912445 58.412070 10.948564 8:43:51 06/19/2024 7 49.993439 22.964938 72.958377 19.878047 58.828596 10.936775 8:44:51 06/19/2024 8 50.109533 23.004151 73.113684 19.903021 58.447589 10.925009 8:45:51 06/19/2024 9 49.993564 23.003203 72.996767 19.954549 58.620046 10.926567 8:46:51 06/19/2024 10 50.560373 23.085252 73.645625 19.870186 59.223544 10.92466 8:47:51 06/19/2024 11 50.386443 23.141761 73.528204 19.886571 59.085346 10.932722 8:48:51 06/19/2024 12 51.508615 23.876903 75.385518 19.96404 58.735297 10.906752 8:49:51 06/19/2024 13 49.144097 22.538828 71.682925 19.797719 59.306630 10.892442 8:50:52 06/19/2024 14 49.906812 22.723247 72.630059 19.77073 59.629105 10.91153 8:51:52 06/19/2024 15 50.113688 22.671843 72.785531 19.862528 59.369789 10.915136 8:52:52 06/19/2024 16 51.131893 23.318812 74.450705 19.95858 59.102530 10.903327 8:53:52 06/19/2024 17 47.763306 21.868077 69.631383 19.719348 59.773592 10.852074 8:54:52 06/19/2024 18 50.065873 22.783195 72.849068 19.800828 59.190640 10.903475 8:55:52 06/19/2024 19 50.838895 23.110256 73.949151 19.901974 59.543820 10.871933 8:56:52 06/19/2024 20 49.782632 22.712948 72.49558 19.833487 59.077603 10.878883 8:57:52 06/19/2024 21 50.361239 22.94341 73.304649 19.849924 58.307925 10.896057 8:58:52 06/19/2024 22 49.437358 22.392142 71.8295 19.810966 59.343589 10.8618 8:59:52 06/19/2024 23 50.882345 23.16023 74.042575 19.832515 59.099683 10.902959 9:00:52 06/19/2024 24 50.742666 23.247333 73.989999 19.886668 58.837136 10.884546 9:01:52 06/19/2024 25 50.232058 23.026126 73.258184 19.93447 58.744313 10.893768 9:02:53 06/19/2024 26 50.187812 22.901485 73.089297 19.838064 59.741831 10.881593 9:03:52 06/19/2024 27 51.333387 23.414612 74.747999 19.952659 59.145171 10.892591 9:04:53 06/19/2024 28 50.230992 22.967378 73.19837 19.823694 58.843453 10.885341 9:05:53 06/19/2024 29 50.559073 23.21515 73.774223 19.771838 59.209628 10.887558 9:06:53 06/19/2024 30 48.869279 22.269989 71.139268 19.699911 59.772029 10.87326 9:07:53 06/19/2024 31 49.691656 22.685569 72.377225 19.832591 59.272257 10.886542 9:08:53 06/19/2024 32 50.738154 23.165763 73.903917 19.865523 58.872080 10.888164 9:09:53 06/19/2024 33 50.322846 23.128753 73.451599 19.889561 59.021751 10.89916 9:10:53 06/19/2024 34 49.781719 22.843518 72.625237 19.753523 59.216746 10.857385 9:11:53 06/19/2024 35 49.630844 22.751194 72.382038 19.67501 59.512821 10.856203 9:12:53 06/19/2024 36 49.493099 22.769315 72.262414 19.587892 59.956418 10.864091 9:13:54 06/19/2024 37 50.261706 23.264083 73.525789 19.775039 59.409458 10.884168 9:14:54 06/19/2024 38 49.042103 22.542997 71.5851 19.619585 60.151671 10.866688 9:15:54 06/19/2024 39 49.588947 22.653538 72.242485 19.607845 59.764221 10.86439 9:16:54 06/19/2024 40 50.88158 23.271863 74.153443 19.756948 59.977845 10.85129 9:17:54 06/19/2024 41 49.532453 22.869136 72.401589 19.837096 60.263304 10.868303 9:18:54 06/19/2024 42 51.259005 23.773098 75.032103 19.910671 58.856449 10.880876 9:19:54 06/19/2024 43 50.904981 23.45309 74.358071 19.826812 60.326080 10.887668 9:20:54 06/19/2024 44 48.623035 22.245297 70.868332 19.784143 60.827110 10.83726 9:21:54 06/19/2024 45 49.829459 22.806672 72.636131 19.737838 59.936393 10.861224 9:22:55 06/19/2024 46 50.885707 23.42146 74.307167 19.93619 59.522734 10.869901 9:23:55 06/19/2024 47 51.236061 23.474385 74.710446 19.885916 59.192790 10.874794 9:24:55 06/19/2024 48 50.237629 22.887217 73.124846 19.842175 60.170328 10.869358 9:25:55 06/19/2024 49 48.991824 22.385459 71.377283 19.772216 60.695767 10.836777 9:26:55 06/19/2024 50 49.465819 22.483452 71.949271 19.792505 60.154416 10.859863 9:27:55 06/19/2024 51 50.567378 23.171636 73.739014 19.92782 59.296211 10.880677 9:28:55 06/19/2024 52 50.682285 23.018276 73.700561 19.8332 59.699775 10.869806 9:29:55 06/19/2024 53 51.43244 23.310779 74.743219 19.817645 59.405003 10.86946 9:30:55 06/19/2024 54 48.52588 21.858522 70.384402 19.580651 60.462755 10.837089 9:31:55 06/19/2024 55 51.10629 23.213982 74.320272 19.822948 59.308149 10.858389 9:32:55 06/19/2024 56 50.983095 23.299854 74.282949 19.81204 59.149629 10.878107 9:33:55 06/19/2024 57 49.849639 22.516426 72.366065 19.737709 59.918695 10.843674 9:34:55 06/19/2024 58 50.063771 22.524841 72.588612 19.634113 59.744322 10.849293 9:35:55 06/19/2024 59 50.789271 22.895586 73.684857 19.769733 59.633822 10.847783 9:36:55 06/19/2024 60 50.521339 22.986176 73.507515 19.712682 59.698338 10.858848 9:37:56 06/19/2024 AVG 50.15 0.00 73.07 19.82 59.40 10.89 ppm@15% O2 28.74 7.80 23.36 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.46 0.99 0.08 0.16 0.36 0.77 Calculated Emission Levels Record Date Uinta Wax Operating, LLC North Randlett Compressor Station Run 2 #4 FTIR Measurements EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 16 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.51 0.46 1204 0.23 0.678 Average O2 5.9 (% dry)A 2 1.68 0.49 0.700 Average CO2 6.9 (% dry)A 3 3.10 0.53 0.728 Average N2 + CO 87.2 (% dry)A 4 5.17 0.58 0.762 Dry Molecular Weight 29.34 lb/lbmol A 5 10.83 0.62 0.787 Wet Molecular Weight 28.11 lb/lbmol A 6 12.90 0.59 0.768 EPA REFERENCE METHOD 320 A 7 14.32 0.56 0.748 Barometric Pressure 25.13 in Hg A 8 15.49 0.52 0.721 Moisture Content 10.89 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 73.07 ppm A 11 Calculated NOx Mass Output 0.99 lbs/hr A 12 Calculated NOx Output 0.46 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 19.82 ppm A 15 Calculated CO Mass Output 0.16 lbs/hr A 16 Calculated CO Output 0.08 g/bhp-hr B 1 0.51 0.45 1204 0.23 0.671 EPA REFERENCE METHOD 320 B 2 1.68 0.48 0.693 Average Analyzer NMNEHC Level 59.40 ppm B 3 3.10 0.52 0.721 Calculated NMNEHC Mass Output 0.77 lbs/hr B 4 5.17 0.56 0.748 Calculated NMNEHC Output 0.36 g/bhp-hr B 5 10.83 0.59 0.768 LOAD APPROXIMATION B 6 12.90 0.58 0.762 Estimated Engine Load 979.1 BHP B 7 14.32 0.54 0.735 B 8 15.49 0.50 0.707 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.5 1204 0.2 0.731 Average Stack Gas Velocity 68.52 ft/sec Average Dry Flowrate 1885.56 dscfm TEST RUN # 2 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 51.665505 23.550002 75.215507 19.735623 59.262960 10.87498 9:39:56 06/19/2024 2 48.965431 22.219561 71.184992 19.552845 60.396716 10.824562 9:40:56 06/19/2024 3 50.644287 23.142633 73.78692 19.684367 60.102232 10.84233 9:41:56 06/19/2024 4 50.421721 22.999631 73.421352 19.730225 59.128493 10.826315 9:42:56 06/19/2024 5 49.708823 22.691953 72.400776 19.721538 60.194693 10.84572 9:43:56 06/19/2024 6 49.730438 22.768177 72.498615 19.658426 60.419498 10.852836 9:44:56 06/19/2024 7 50.42335 22.941026 73.364376 19.717532 59.717029 10.842796 9:45:57 06/19/2024 8 49.974407 22.861783 72.83619 19.735203 60.407228 10.835299 9:46:56 06/19/2024 9 50.992173 23.448597 74.44077 19.721918 58.993151 10.831033 9:47:56 06/19/2024 10 50.955736 23.373413 74.329149 19.810609 59.426330 10.848309 9:48:57 06/19/2024 11 49.042865 22.303021 71.345886 19.611755 60.567154 10.82713 9:49:57 06/19/2024 12 50.464599 23.064685 73.529284 19.705514 60.129266 10.824929 9:50:57 06/19/2024 13 50.286641 23.147831 73.434472 19.711149 60.215608 10.804152 9:51:57 06/19/2024 14 49.995347 23.123848 73.119195 19.922289 59.873756 10.715821 9:52:57 06/19/2024 15 51.447393 23.824208 75.271601 19.877835 59.584959 10.75037 9:53:57 06/19/2024 16 49.51615 22.700488 72.216638 19.690637 60.340276 10.862379 9:54:57 06/19/2024 17 50.132019 22.933814 73.065833 19.680922 60.537856 10.954498 9:55:57 06/19/2024 18 49.579643 22.489688 72.069331 19.645095 60.810319 10.866055 9:56:57 06/19/2024 19 50.256232 22.956889 73.213121 19.772908 60.531942 10.834197 9:57:57 06/19/2024 20 50.283958 22.882629 73.166587 19.818412 60.803850 10.8276 9:58:58 06/19/2024 21 49.675456 22.532528 72.207984 19.671911 61.041019 10.816391 9:59:58 06/19/2024 22 50.05501 22.613279 72.668289 19.779753 61.470154 10.85044 10:00:58 06/19/2024 23 49.032288 22.004652 71.03694 19.522452 61.460639 10.807076 10:01:58 06/19/2024 24 49.874444 22.618517 72.492961 19.630506 60.167515 10.819335 10:02:58 06/19/2024 25 49.29761 22.547387 71.844997 19.668453 59.412136 10.827439 10:03:58 06/19/2024 26 50.035643 22.974131 73.009774 19.720918 60.243010 10.838775 10:04:58 06/19/2024 27 50.120203 22.877392 72.997595 19.773376 60.080762 10.841649 10:05:58 06/19/2024 28 49.659965 22.6799 72.339865 19.619889 59.767584 10.833095 10:06:59 06/19/2024 29 49.740423 22.87163 72.612053 19.701684 59.885054 10.853278 10:07:58 06/19/2024 30 49.885265 22.768191 72.653456 19.635964 60.276593 10.843257 10:08:58 06/19/2024 31 49.997522 22.96775 72.965272 19.65719 59.069645 10.843105 10:09:58 06/19/2024 32 49.786292 22.916897 72.703189 19.693856 59.512854 10.848597 10:10:59 06/19/2024 33 49.531592 22.796322 72.327914 19.662834 59.343290 10.849671 10:11:59 06/19/2024 34 48.749696 22.530869 71.280565 19.626854 60.144925 10.839666 10:12:59 06/19/2024 35 50.509778 23.275226 73.785004 19.734005 59.815587 10.847564 10:13:59 06/19/2024 36 49.419294 22.745802 72.165096 19.618154 59.611966 10.827761 10:14:59 06/19/2024 37 50.330576 23.031964 73.36254 19.799251 59.904185 10.845448 10:15:59 06/19/2024 38 50.480211 23.373379 73.85359 19.789007 59.266332 10.839046 10:16:59 06/19/2024 39 50.27755 23.322668 73.600218 19.733916 58.621266 10.8572 10:17:59 06/19/2024 40 50.131793 23.302434 73.434227 19.771963 58.279889 10.862661 10:18:59 06/19/2024 41 49.936056 23.166843 73.102899 19.857056 58.842010 10.84477 10:19:59 06/19/2024 42 50.4462 23.276521 73.722721 19.761238 59.356243 10.829189 10:21:00 06/19/2024 43 51.057029 23.24214 74.299169 19.799439 58.935709 10.852948 10:22:00 06/19/2024 44 49.718217 22.677442 72.395659 19.72408 60.310746 10.867525 10:23:00 06/19/2024 45 50.172206 22.796054 72.96826 19.792785 60.167635 10.870557 10:24:00 06/19/2024 46 50.803009 23.256841 74.05985 19.764851 59.710186 10.88764 10:25:00 06/19/2024 47 48.886657 22.299567 71.186224 19.631738 59.809486 10.862524 10:26:00 06/19/2024 48 50.860527 23.319011 74.179538 19.896419 58.490006 10.884423 10:27:00 06/19/2024 49 49.269135 22.500674 71.769809 19.927777 59.146319 10.868744 10:28:00 06/19/2024 50 51.636904 23.635324 75.272228 20.000759 58.907095 10.888234 10:29:00 06/19/2024 51 49.970625 22.95403 72.924655 19.767409 59.285853 10.871434 10:30:00 06/19/2024 52 50.421791 23.14396 73.565751 19.950057 59.138598 10.88553 10:31:00 06/19/2024 53 50.323802 23.129106 73.452908 19.918078 59.674974 10.9066 10:32:01 06/19/2024 54 49.983876 22.954652 72.938528 19.747961 59.326046 10.900631 10:33:01 06/19/2024 55 50.068319 22.921516 72.989835 19.847082 59.176617 10.878677 10:34:01 06/19/2024 56 51.132804 23.467345 74.600149 19.76366 58.729829 10.872481 10:35:01 06/19/2024 57 50.894814 23.523107 74.417921 19.763964 58.214609 10.864957 10:36:01 06/19/2024 58 52.115683 23.902673 76.018356 19.85191 58.387402 10.868798 10:37:01 06/19/2024 59 49.30901 22.460566 71.769576 19.693534 59.017427 10.847958 10:38:01 06/19/2024 60 51.608992 23.541845 75.150837 19.851567 58.583403 10.883654 10:39:01 06/19/2024 AVG 50.16 0.00 73.13 19.74 59.70 10.85 ppm@15% O2 29.15 7.87 23.80 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.46 0.99 0.08 0.16 0.36 0.77 FTIR Measurements #4 Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 3 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 16 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.51 0.44 1203 0.23 0.663 Average O2 6.1 (% dry)A 2 1.68 0.48 0.693 Average CO2 6.9 (% dry)A 3 3.10 0.51 0.714 Average N2 + CO 87.0 (% dry)A 4 5.17 0.55 0.742 Dry Molecular Weight 29.35 lb/lbmol A 5 10.83 0.59 0.768 Wet Molecular Weight 28.12 lb/lbmol A 6 12.90 0.57 0.755 EPA REFERENCE METHOD 320 A 7 14.32 0.57 0.755 Barometric Pressure 25.13 in Hg A 8 15.49 0.54 0.735 Moisture Content 10.85 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 73.13 ppm A 11 Calculated NOx Mass Output 0.99 lbs/hr A 12 Calculated NOx Output 0.46 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 19.74 ppm A 15 Calculated CO Mass Output 0.16 lbs/hr A 16 Calculated CO Output 0.08 g/bhp-hr B 1 0.51 0.45 1203 0.23 0.671 EPA REFERENCE METHOD 320 B 2 1.68 0.49 0.700 Average Analyzer NMNEHC Level 59.70 ppm B 3 3.10 0.54 0.735 Calculated NMNEHC Mass Output 0.77 lbs/hr B 4 5.17 0.58 0.762 Calculated NMNEHC Output 0.36 g/bhp-hr B 5 10.83 0.62 0.787 LOAD APPROXIMATION B 6 12.90 0.57 0.755 Estimated Engine Load 979.1 BHP B 7 14.32 0.54 0.735 B 8 15.49 0.55 0.742 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.5 1203 0.2 0.732 Average Stack Gas Velocity 68.56 ft/sec Average Dry Flowrate 1888.91 dscfm TEST RUN # 3 APPENDIX B Date Time NO 191C span NO2 191C span H2O% (high) 191C Formaldehyde 191C Ethylene 191C TE span Propane 191C span Acetaldehyde 191C span CO ppm 191C (1of2) span CO ppm Dry CO2% 191C NOx Wet NOx Dry NM NE HC C3 Temp ( C )Pressure (atm) 6/19/2024 7:14:39 0.226792 0.062727 -0.002904 -0.099759 0.592607 0.178238 -0.015568 -0.146896 -0.146892 0.000624 0.289519 0.289511 0.808373 192.164703 0.99841 6/19/2024 7:14:46 0.062184 0.142539 -0.00325 -0.134844 0.401942 -0.163137 -0.602548 0.052511 0.052509 -0.00066 0.204722 0.204715 0.146275 192.162277 0.995667 6/19/2024 7:14:54 -0.022319 0.011476 -0.004351 -0.040615 0.711846 0.499291 -0.164076 -0.041042 -0.04104 -0.007668 -0.010843 -0.010842 0.037108 192.147736 1.001772 6/19/2024 7:15:01 0.112159 0.054753 -0.001553 0.021903 0.315365 -0.347671 0.172143 0.027159 0.027158 0.008948 0.166912 0.16691 -0.001132 192.118668 1.001038 6/19/2024 7:15:42 0 0 0 0 0 0 0 0 0 0 0 0 0 192.092239 0.999196 6/19/2024 7:15:56 0.128773 -0.037018 -0.002424 -0.037249 -0.456328 0.145411 0.668038 0.076756 0.076754 -0.002463 0.091756 0.091753 0.026497 192.088379 0.998169 6/19/2024 7:16:03 0.149404 -0.026211 0.001714 0.114832 -0.06006 -0.177915 0.012422 0.049226 0.049227 0.000115 0.123193 0.123195 3.240471 192.0896 0.997136 6/19/2024 7:16:10 0.297062 0.057412 -0.00455 -0.079293 0.47896 -1.04042 -0.826644 0.210582 0.210573 -0.014926 0.354474 0.354457 0.002889 192.118668 0.999707 6/19/2024 7:16:18 0.017685 -0.023667 0.001232 0.111476 0.47932 -0.091293 0.008861 -0.084155 -0.084156 0.001882 -0.005982 -0.005982 0.008897 192.118668 0.99888 6/19/2024 7:16:25 -0.097105 0.027359 -0.010106 0.071331 -0.324707 -0.781281 0.4628 -0.113539 -0.113528 -0.018827 -0.069746 -0.069739 2.288948 192.104126 0.997871 6/19/2024 7:16:33 0.094404 0.016646 0.004324 -0.152827 1.263133 -0.115972 0.055341 -0.275515 -0.275526 0.001248 0.11105 0.111055 0.048759 192.0896 0.997779 6/19/2024 7:16:41 0.235592 -0.032129 0.004067 -0.089221 0.441448 -0.914762 0.279541 -0.011518 -0.011518 -0.005951 0.203462 0.203471 0.001203 192.0896 0.999523 6/19/2024 7:16:48 0.170382 0.079511 -0.002801 0.057476 -0.296827 -0.160512 -0.645489 0.055829 0.055828 0.001389 0.249893 0.249886 -0.009284 192.109589 0.997366 6/19/2024 7:16:56 0.199693 -0.093658 -0.005892 0.260772 0.768205 -0.205463 0.765158 -0.085016 -0.085011 -0.005056 0.106035 0.106029 0.029382 192.0896 0.996815 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 7:17:36 517.862985 492.973425 494.142414 192.113831 1.011878 6/19/2024 7:21:18 98.743453 192.07991 1.007514 6/19/2024 7:17:44 513.605976 489.678834 494.864185 192.104126 1.017884 6/19/2024 7:21:26 99.039569 192.060532 1.008979 6/19/2024 7:17:51 516.19934 491.796823 498.067281 192.075058 1.013982 6/19/2024 7:21:33 99.05074 192.04599 1.006087 6/19/2024 7:17:59 515.160954 491.23914 493.553857 192.060532 1.017195 6/19/2024 7:21:41 98.695342 192.031448 1.01233 6/19/2024 7:18:06 517.18614 492.580119 495.973457 192.031448 1.016369 6/19/2024 7:21:48 97.971352 192.060532 1.010494 6/19/2024 7:18:14 518.165719 493.200159 499.075324 192.00238 1.015589 6/19/2024 7:21:56 98.217673 192.118668 1.007923 6/19/2024 7:18:21 517.552849 491.704997 497.066192 191.973312 1.017976 6/19/2024 7:22:03 98.931552 192.109589 1.011263 6/19/2024 7:18:29 516.647198 492.492009 497.025542 192.04599 1.019054 6/19/2024 7:22:11 98.247893 192.075058 0.991628 6/19/2024 7:18:37 518.410788 493.218925 498.414959 192.016922 1.015589 6/19/2024 7:22:18 98.386153 192.133209 0.983228 6/19/2024 7:18:44 516.679553 492.541772 496.813126 192.04599 1.018435 6/19/2024 7:22:26 98.78346 192.118668 0.978454 Date Time NO2 191C span Temp ( C )Pressure (atm) 6/19/2024 7:19:36 144.362711 192.054474 1.004595 6/19/2024 7:19:44 145.351506 192.075058 1.005261 6/19/2024 7:19:51 145.746178 192.060532 1.005261 6/19/2024 7:19:59 146.579066 192.075058 1.003057 6/19/2024 7:20:06 146.744273 192.031448 1.003562 6/19/2024 7:20:14 146.651195 192.104126 1.003746 6/19/2024 7:20:21 146.875253 192.031448 1.00393 6/19/2024 7:20:29 146.76966 192.071426 1.004153 6/19/2024 7:20:36 146.806322 192.104126 1.007785 6/19/2024 7:20:44 146.939027 192.104126 1.00673 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 7:22:59 412.348381 403.197184 383.609661 192.105347 0.947401 6/19/2024 7:24:45 71.575503 192.054474 0.945125 6/19/2024 7:23:06 498.177858 478.222661 486.533508 192.133209 0.970421 6/19/2024 7:24:52 100.365214 192.031448 0.940401 6/19/2024 7:23:14 511.868665 490.803167 497.714063 192.104126 0.985431 6/19/2024 7:24:59 98.545712 192.016922 0.951371 6/19/2024 7:23:21 511.728107 490.208356 498.973822 192.0896 0.98488 6/19/2024 7:25:07 99.076809 192.0896 0.978041 6/19/2024 7:23:29 510.75923 488.785838 493.698935 192.04599 0.990664 6/19/2024 7:25:14 98.584906 192.031448 0.976985 6/19/2024 7:23:36 513.192136 491.456613 498.984195 192.075058 0.98488 6/19/2024 7:25:22 98.332691 192.031448 0.976847 6/19/2024 7:23:44 510.615178 488.739197 495.163949 192.0896 0.990021 6/19/2024 7:25:30 99.73623 192.016922 0.973405 6/19/2024 7:23:51 512.100599 490.165954 496.908307 192.058716 0.985316 6/19/2024 7:25:37 100.330654 192.016922 0.973726 6/19/2024 7:23:59 512.48514 490.448828 497.855497 192.0896 0.984559 6/19/2024 7:25:44 99.009099 192.020554 0.979412 6/19/2024 7:24:06 512.061212 491.335 500.288625 192.04599 0.983824 6/19/2024 7:25:52 98.021447 192.029037 0.976159 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 7:26:15 0.115463 0.463137 0.014398 0.9213 191.973312 0.971247 6/19/2024 7:26:22 0.120532 0.132015 0.04325 -0.303243 191.944244 0.974047 6/19/2024 7:26:30 0.069509 0.117748 0.029066 0.667397 191.944244 0.974047 6/19/2024 7:26:37 -0.009312 0.120233 0.623768 -0.347446 191.973312 0.97951 6/19/2024 7:26:44 0.073634 0.022434 -0.376695 0.159928 191.958771 0.984697 6/19/2024 7:26:52 -0.106763 0.255023 -0.284181 1.097985 191.944244 0.989562 6/19/2024 7:27:00 0.23223 -0.093074 -0.189707 0.565505 191.915161 0.985247 6/19/2024 7:27:07 -0.221937 -0.121813 0.266158 0.211793 191.918808 1.003671 Raw Calibration Data BACKGROUND / PRE DIRECT ZERO PRE DIRECT CAL NO2 CAL PRE SYSTEM CAL PRE SYSTEM ZERO Date Time CO2% 191C Propane 191C span Temp ( C )Pressure (atm) 6/19/2024 7:32:14 6.519614 35.796143 191.995117 1.002533 6/19/2024 7:32:22 6.517024 36.68097 191.973312 1.003562 6/19/2024 7:32:30 6.447529 37.330455 191.944244 1.005674 6/19/2024 7:32:37 6.501242 36.910437 191.915161 1.004251 6/19/2024 7:32:44 6.488927 37.080679 191.929703 1.003195 6/19/2024 7:33:59 6.372486 37.849533 191.931335 1.004978 6/19/2024 7:34:07 6.32383 36.959771 191.893372 1.00343 6/19/2024 7:34:15 4.181181 26.636382 191.900635 1.001818 6/19/2024 7:34:22 3.625697 110.777045 191.900635 1.002323 6/19/2024 7:34:30 3.580531 218.323967 191.900635 1.002139 6/19/2024 7:34:37 3.593114 221.532644 191.944244 1.000441 6/19/2024 7:34:45 3.584542 222.150427 191.973312 1.004802 6/19/2024 7:34:52 5.179118 111.787623 192.00238 1.000395 6/19/2024 7:35:00 5.880462 71.456698 192.00238 1.004021 6/19/2024 7:35:53 5.881455 70.050807 191.97496 1.001373 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 10:47:02 517.559552 493.182428 491.92758 192.173172 1.004917 6/19/2024 10:45:20 99.31583 192.130783 0.99675 6/19/2024 10:47:10 516.812376 492.631235 493.63685 192.220413 1.007005 6/19/2024 10:45:27 98.139894 192.104126 0.998192 6/19/2024 10:47:17 516.498964 492.407897 490.978729 192.147736 1.007785 6/19/2024 10:45:35 97.881733 192.0896 0.996861 6/19/2024 10:47:25 518.327633 492.587202 487.074235 192.264023 1.008015 6/19/2024 10:45:42 99.103954 192.031448 0.995484 6/19/2024 10:47:32 519.173441 495.176611 496.383318 192.293091 1.005031 6/19/2024 10:45:50 99.5092 192.075058 0.993739 6/19/2024 10:47:40 517.115865 492.380438 492.301621 192.293091 1.011274 6/19/2024 10:45:57 99.42638 192.071426 0.997848 6/19/2024 10:47:47 516.629311 494.261007 492.054428 192.307632 1.008795 6/19/2024 10:46:05 99.733157 192.060532 0.996815 6/19/2024 10:47:55 518.502263 493.430801 489.458507 192.264023 1.009851 6/19/2024 10:46:12 99.095595 192.104126 0.997871 6/19/2024 10:48:02 519.189649 494.445807 490.687561 192.31308 1.007608 6/19/2024 10:46:20 99.914324 192.075058 0.995392 6/19/2024 10:48:10 518.900318 494.52181 493.276063 192.307632 1.009117 6/19/2024 10:46:27 98.421076 192.060532 0.997733 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/19/2024 10:45:35 -0.368082 0.087863 -0.673356 192.0896 0.996861 6/19/2024 10:49:05 -0.570845 192.3367 0.996218 6/19/2024 10:45:42 -0.451075 -0.11848 -1.595938 192.031448 0.995484 6/19/2024 10:49:12 0.307709 192.3367 0.992546 6/19/2024 10:45:50 -0.364913 0.300879 -1.240074 192.075058 0.993739 6/19/2024 10:49:20 0.051847 192.307632 0.991857 6/19/2024 10:45:57 -0.560571 -0.091316 -1.634276 192.071426 0.997848 6/19/2024 10:49:27 -0.084092 192.322174 0.997228 6/19/2024 10:46:05 -0.581523 0.057353 -1.490725 192.060532 0.996815 6/19/2024 10:49:35 0.503864 192.293091 0.993923 6/19/2024 10:46:12 -0.3652 0.266176 -1.464492 192.104126 0.997871 6/19/2024 10:49:42 -0.721271 192.322174 0.997641 6/19/2024 10:46:20 -0.220381 -0.020048 -1.264651 192.075058 0.995392 6/19/2024 10:49:50 0.353139 192.351242 0.991903 6/19/2024 10:46:27 -0.219612 0.075376 -1.771715 192.060532 0.997733 6/19/2024 10:49:57 0.614522 192.365784 0.990434 SAMPLE SPIKE RECOVERY POST SYSTEM CAL POST SYSTEM ZERO PRE TEST 1 495.6 6.4 37.1 5.9 70.8 0.087 71.1% Sensor Analyzer Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Error (%)Error (%) NOx 492.5 493.4 0.1 -0.17 0.03 CO 516.7 520.2 0.0 -0.68 0.00 Propane 496.8 495.6 -0.4 0.24 -0.08 Ethylene 99.1 101.9 0.2 -2.80 0.19 Sensor System Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%) NOx 491.3 493.4 0.1 -0.42 0.03 CO 512.1 520.2 0.1 -1.56 0.01 Propane 500.3 495.6 0.0 0.95 0.00 Ethylene*98.0 101.9 0.4 -3.81 0.39 Sensor System Cal Zero Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%)Drift Error (%)Drift Error (%) NOx 494.5 493.4 0.1 0.23 0.01 0.65 0.02 CO 518.9 520.2 -0.4 -0.25 -0.08 1.31 0.09 Propane 493.3 495.6 -1.3 -0.47 -0.27 1.41 0.27 Ethylene*98.4 101.9 0.0 -3.41 0.04 0.39 0.35 *CTS Scans are conducted with Ethylene through the sample line. Lf 5.11 Lr Cr Tr Pr Lr/Lf 5.25 99.1 192.0 1.0 1.03 Ls Cs Ts Ps Ls/Lf 5.47 98.0 192.0 1.0 1.07 Pathlength Stack Propane Concentration Stack + Spike CO2 Concentration Stack + Propane Concentration DF Calculated POST SYSTEM CAL PRE SYSTEM CAL % Recovery Propane PRE DIRECT CAL FTIR QA/QC SUMMARY SAMPLE RECOVERY CALCULATIONS Period Spike #Concentration of Propane Cylinder Stack CO2 Concentration CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number:E02NI99E15W0051 Reference Number:153-402577489-1 Cylinder Number:CC486070 Cylinder Volume:144.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG PGVP Number:B72022 Valve Outlet:660 Gas Code:NO2,BALN Certification Date:Nov 08, 2022 Expiration Date:Nov 08, 2025 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates NITROGEN DIOXIDE 150.0 PPM 146.6 PPM G1 +/- 2.0% NIST Traceable 11/01/2022, 11/08/2022 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 15340120215 CC511005 59.52 PPM NITROGEN DIOXIDE/NITROGEN 1.4%Dec 17, 2024 PRM 12397 D887665 74.2 PPM NITROGEN DIOXIDE/AIR 1.3%Feb 02, 2022 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration MKS FTIR NO2 018143349 FTIR Nov 01, 2022 Triad Data Available Upon Request PERMANENT NOTES:OXYGEN ADDED TO MAINTAIN STABILITY Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD Part Number:X02NI99P15AD524 Reference Number:153-402622613-1 Cylinder Number:CC173895 Cylinder Volume:140.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG Analysis Date:Dec 22, 2022 Valve Outlet:350 Lot Number:153-402622613-1 Expiration Date:Dec 22, 2025 Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. ANALYTICAL RESULTS Component Req Conc Actual Concentration Analytical (Mole %)Uncertainty ETHYLENE 100.0 PPM 101.9 PPM +/- 1% NITROGEN Balance Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 Finely – North Randlett 6-19-2024 Finely – North Randlett 6-19-2024 Finely – North Randlett 6-19-2024 Spectral Fit Run 1 Spectral Fit Run 2 Spectral Fit Run 3 Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000141.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000068.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 44.13 3.56 -0.24 0.33 4.85 4.85 -2.21 --0-2795 1.05 Good NO2 191C 21.64 0.38 -0.03 0.03 0.4 0.4 -0.43 --0-488 1.06 Good N2O 191C -0.01 0.37 0.06 0.03 0.03 0.42 0.42 0.08 0.35 0.02 0.02 0-200 -Close to DL NH3 TE 191C 7.76 45.57 6.6 4.14 7.06 77.78 77.78 6.66 41.43 0.06 2.2 0-2995 -Close to DL H2O% (HIGH) 191C10.95 0.27 -0.02 0.03 0.44 0.44 -0.22 --0-40 -Good FORMALDEHYDE 191C3.7 0.8 3.04 0.24 0.27 0.9 0.9 3.38 3.39 0.35 1.01 0-69 -Close to DL FORMIC ACID 191C TE1.53 10.63 3.71 1.56 1.83 12.45 12.45 3.87 9.09 0.16 1.24 0-466 -Close to DL CH4 2900 CM-1 191C742.56 28.52 -1.69 2.46 54.96 54.96 -15.55 --0-3143 1 Good PROPANE 191C 37.5 1.2 -0.22 0.27 1.44 1.44 -0.75 --0-4976 0.95 Good PROPYLENE 191C TE1.6 10.96 4.31 1.57 1.86 12.96 12.96 5.62 9.37 1.31 1.44 0-194 -Close to DL ETHANE 191C 77.18 2.93 -0.55 0.85 4.57 4.57 -1.55 --0-1004 -Good ETHYLENE 191C TE14.83 20.25 14.54 2.07 2.55 24.38 24.38 16.54 17.8 2 4.85 0-900 -Close to DL CO PPM 191C (1OF2)17.96 1.22 -0.26 0.57 2.52 2.52 -0.56 --0-5010 1.05 Good CO2% 191C 6.26 0.17 -0.01 0.02 0.24 0.24 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.25 2.12 1.65 0.64 0.82 2.73 2.73 1.7 1.7 0.05 0.55 0-186 1 Close to DL ACETYLENE 191C0.1 4.32 0.81 0.79 1.05 5.71 5.71 1.01 3.57 0.2 0.27 0-1016 -Close to DL SO2 191C 2.59 2.21 2.06 0.26 0.32 2.69 2.69 2.68 2.68 0.62 0.69 0-964 1.02 Close to DL HEXANE 191C 2.84 0.98 3.03 0.13 0.18 1.33 1.33 3.35 3.35 0.32 1.01 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000202.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000068.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 44.46 3.81 -0.24 0.33 5.19 5.19 -2.43 --0-2795 1.05 Good NO2 191C 21.71 0.37 -0.03 0.03 0.39 0.39 -0.43 --0-488 1.06 Good N2O 191C -0.05 0.38 0.06 0.03 0.03 0.43 0.43 0.08 0.35 0.02 0.02 0-200 -Close to DL NH3 TE 191C 10.61 46.78 6.6 4.14 7.06 79.83 79.83 6.66 42.54 0.06 2.2 0-2995 -Close to DL H2O% (HIGH) 191C10.87 0.28 -0.02 0.03 0.46 0.46 -0.22 --0-40 -Good FORMALDEHYDE 191C3.78 0.85 3.04 0.24 0.27 0.96 0.96 3.38 3.39 0.35 1.01 0-69 -Close to DL FORMIC ACID 191C TE1.6 10.84 3.71 1.56 1.83 12.69 12.69 3.87 9.29 0.16 1.24 0-466 -Close to DL CH4 2900 CM-1 191C740.08 28.42 -1.69 2.46 54.77 54.77 -15.5 --0-3143 1 Good PROPANE 191C38.02 1.26 -0.22 0.27 1.51 1.51 -0.76 --0-4976 0.95 Good PROPYLENE 191C TE-0.45 11.44 4.31 1.57 1.86 13.53 13.53 5.62 9.88 1.31 1.44 0-194 -Close to DL ETHANE 191C 76.37 3.02 -0.55 0.85 4.7 4.7 -1.54 --0-1004 -Good ETHYLENE 191C TE14.87 21.22 14.54 2.07 2.55 25.55 25.55 16.54 18.77 2 4.85 0-900 -Close to DL CO PPM 191C (1OF2)17.7 1.32 -0.26 0.57 2.73 2.73 -0.65 --0-5010 1.05 Good CO2% 191C 6.21 0.17 -0.01 0.02 0.24 0.24 -0.12 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C-0.28 2.22 1.65 0.64 0.82 2.84 2.84 1.7 1.7 0.05 0.55 0-186 1 Close to DL ACETYLENE 191C0.1 4.69 0.81 0.79 1.05 6.19 6.19 1.01 3.93 0.2 0.27 0-1016 -Close to DL SO2 191C 2.62 2.12 2.06 0.26 0.32 2.58 2.58 2.68 2.68 0.62 0.69 0-964 1.02 Close to DL HEXANE 191C 2.96 1.02 3.03 0.13 0.18 1.38 1.38 3.35 3.35 0.32 1.01 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000263.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000068.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000069.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000070.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000071.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000072.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000073.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000074.LAB C:\OLT\Data\Finley Resources\North Randlett CS E1 (E5) 6-19-24\FINLEY NORTH RANDLETT CS E4 6-19-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 44.22 3.66 -0.24 0.33 4.99 4.99 -2.3 --0-2795 1.05 Good NO2 191C 21.82 0.35 -0.03 0.03 0.37 0.37 -0.44 --0-488 1.06 Good N2O 191C -0.05 0.38 0.06 0.03 0.03 0.43 0.43 0.08 0.35 0.02 0.02 0-200 -Close to DL NH3 TE 191C 9.79 43.73 6.6 4.14 7.06 74.63 74.63 6.66 39.52 0.06 2.2 0-2995 -Close to DL H2O% (HIGH) 191C10.89 0.27 -0.02 0.03 0.44 0.44 -0.22 --0-40 -Good FORMALDEHYDE 191C3.74 0.88 3.04 0.24 0.27 0.99 0.99 3.38 3.39 0.35 1.01 0-69 -Close to DL FORMIC ACID 191C TE1 11.2 3.71 1.56 1.83 13.12 13.12 3.87 9.67 0.16 1.24 0-466 -Close to DL CH4 2900 CM-1 191C756.54 26.55 -1.69 2.46 51.18 51.18 -15.3 --0-3143 1 Good PROPANE 191C37.27 1.31 -0.22 0.27 1.57 1.57 -0.75 --0-4976 0.95 Good PROPYLENE 191C TE-0.48 11.75 4.31 1.57 1.86 13.89 13.89 5.62 10.18 1.31 1.44 0-194 -Close to DL ETHANE 191C 74.74 3.15 -0.55 0.85 4.9 4.9 -1.54 --0-1004 -Good ETHYLENE 191C TE14.8 21.17 14.54 2.07 2.55 25.49 25.49 16.54 18.72 2 4.85 0-900 -Close to DL CO PPM 191C (1OF2)17.8 1.28 -0.26 0.57 2.65 2.65 -0.61 --0-5010 1.05 Good CO2% 191C 6.23 0.17 -0.01 0.02 0.23 0.23 -0.12 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.64 2.32 1.65 0.64 0.82 2.98 2.98 1.7 1.7 0.05 0.55 0-186 1 Close to DL ACETYLENE 191C0.02 4.85 0.81 0.79 1.05 6.4 6.4 1.01 4.1 0.2 0.27 0-1016 -Close to DL SO2 191C 1.68 2.05 2.06 0.26 0.32 2.5 2.5 2.68 2.68 0.62 0.69 0-964 1.02 Close to DL HEXANE 191C 3.1 1.04 3.03 0.13 0.18 1.41 1.41 3.35 3.35 0.32 1.01 0-1000 -Close to DL APPENDIX C Test Run Load %Site Rated Load, bhp Load Approx., bhp 1 71 1379 979.1 2 71 1379 979.1 3 71 1379 979.1 Engine Load Approximation based on Panel Levels APPENDIX D Test Run Flowrate dscfm Approx. BHP Avg O2 % NOx ppmvd NOx g/bhp-hr NOx lbs/hr CO ppmvd CO g/bhp-hr CO lbs/hr NMNEHC ppmvd NMNEHC g/bhp-hr NMNEHC lbs/hr Moisture Content % 1 1871.07 979.1 5.7 73.51 0.46 0.98 20.01 0.08 0.16 59.73 0.36 0.77 11.32 2 1885.56 979.1 5.9 73.07 0.46 0.99 19.82 0.08 0.16 59.40 0.36 0.77 10.89 3 1888.91 979.1 6.1 73.13 0.46 0.99 19.74 0.08 0.16 59.70 0.36 0.77 10.85 979.1 5.9 73.24 0.46 0.99 19.86 0.08 0.16 59.61 0.36 0.77 11.02 Summary Average Levels Example Calculations: Uinta Wax Operating, LLC, North Randlett Compressor Station, #4 The following is a step-by-step calculation for the first test run conducted on the North Randlett Compressor Station #4. Test Parameters • Stack Diameter = 16 inches • Traverse Points = 16 • Ports = 2 • Barometric Pressure = 25.13 in Hg • Average O2 = 5.7% • Average CO2 = 7% • Load Approximation = 979.1 bhp • Moisture Content = 11.32% EPA 40 CFR 60(A) Methods 1-3: Determination of Stack Gas Velocity and Flow Rate Dry Molecular Weight (lb/lbmol) = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) Where: %CO2 – Carbon Dioxide Content Of The Gas = 7% %O2 – Oxygen Content Of The Gas = 5.7% %N2 – Nitrogen Content Of The Gas %CO – Carbon Monoxide Content Of The Gas (%N2 +%CO) = (100 - %O2 - %CO2) = (100 – 5.7 – 7) = 87.3% Dry = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) = (0.44 * 7) + (0.32 * 5.7) + (0.28 * 87.3) = 29.35 lb/lbmol Wet Molecular Weight (lb/lbmol) = MD * (1-BWS) + (18) * BWS Where: MD – Molecular Weight Of The Dry Gas (lb/lbmol) = 29.35 lb/lbmol BWS – Moisture Content Of The Gas (%/100) = 11.32% = MD * (1-BWS) + (18) * BWS = 29.35 * (1 – (11.32/ 100)) + (18 * (11.32/ 100)) = 28.06 lb/lbmol Average Stack Gas Velocity (ft/sec) = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) Where: CP – Pitot tube constant (unitless) = 0.84 ∆PAVG – Average square root of the stack gas pitot DP (inches water) = 0.727 in H2O TS – Average stack temperature (R) = 1200 R PB – Barometric pressure (in Hg) = 25.13 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.2 in H2O MA – Molecular weight of the wet gas (lb/lbmol) = 28.06 lb/lbmol = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) = 0.84 * (85.49) * 0.727 * ( 1200 / (((0.2/ 13.6) + 25.13) * 28.06)) = 68.10 ft/sec Average Dry Flowrate (dscfm) = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 Where: DS – Diameter of the stack (inches) = 16 inches BWS – Moisture content of the gas (%) = 11.32% TSTD – Standard temperature (528R) TS – Average stack temperature (R) = 1200 R PB – Barometric pressure (in Hg) = 25.13 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.2 in H2O VS– Average Stack gas velocity (ft/sec) = 68.10 ft/sec = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 = 60 * (1 - (11.32/ 100)) * 68.10 * * (((16 / 2) / 12))2) * 528 / 1200 * (25.13 + (0.2 / 13.6)) / 29.92 = 1871.07 dscfm Conversion of Dry Flowrate to m3/hr = Q * 60 * 2.83168*10 -2 Where: Q – Volumetric Flowrate = 1871.07 dscfm 2.83168*10 -2 – Conversion factor for cubic feet to cubic meter 60 – Minutes in an hour = Q * 60 * 2.83168*10 -2 = 1871.07 *60 * 2.83168*10 -2 = 3178.97 m3/hr ASTM D 6348-03: Determination of NOx, CO and VOC Emissions From Stationary Sources NOx Emission Rate (g/Bhp-hr) = (Cd * 1.912*10 -3 * Q * T) / HP-hr Where: Cd – Measured NOx concentration in ppm = 73.51 ppm 1.92*10 -3 - Conversion constant for ppm to g/m3 NOx Q – Volumetric Flowrate = 3178.97 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 979.1 Bhp = (Cd * 1.912*10 -3 * Q * T) / HP-hr = (73.51 * 1.912*10 -3 * 3178.97 * 1) / 979.1 = 0.46 g/Bhp-hr NOx Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.46 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 979.1 Bhp = g/Bhp-hr / 454 * Bhp = 0.46 / 454 * 979.1 = 0.98 lbs/hr CO Emission Rate (g/Bhp-hr) = (Cd * 1.164*10 -3 * Q * T) / HP-hr Where: Cd – Measured CO concentration in ppm = 20.01 ppm 1.164*10 -3 - Conversion constant for ppm to g/m3 CO Q – Volumetric Flowrate = 3178.97 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 979.1 Bhp = (Cd * 1.164*10 -3 * Q * T) / HP-hr = (20.01 * 1.164*10 -3 * 3178.97 * 1) / 979.1 = 0.08 g/Bhp-hr CO Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.08 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 979.1 Bhp = g/Bhp-hr / 454 * Bhp = 0.08 / 454 * 979.1 = 0.16 lbs/hr VOC Emission Rate (g/Bhp-hr) = (Cd * 1.833*10 -3 * Q * T) / HP-hr Where: Cd – Measured VOC concentration in ppm = 59.73 ppm 1.833*10 -3 - Conversion constant for ppm to g/m3 VOC Q – Volumetric Flowrate = 3178.97 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 979.1 Bhp = (Cd * 1.833*10 -3 * Q * T) / HP-hr = (59.73 * 1.833*10 -3 * 3178.97 * 1) / 979.1 = 0.36 g/Bhp-hr VOC Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.36 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 979.1 Bhp = g/Bhp-hr / 454 * Bhp = 0.36 / 454 * 979.1 = 0.77 lbs/hr APPENDIX E FTIR Engine Test Sheet Company Name f' Ilk " Location / Unit 1.0. A'()r!=-h ~~"d\~ ~t L~ t_1 IrG.~l 3x1hr ....v&VType of Test Completed Field Technician (s) David Martinez \(\lI~, b~'1 t,~a..\i' Client Rep and/or State Rep Date Non-Resettable Run Time Hours 'it ~"\ Engine Make f:,Al Engine Model f",'hS-1 "":\ Enaine SIN ~£fo\b<"1 Port Distance A ~II W"-'·" Port Distance B VI 1/" Exhaust Diameter (inches) \ bII Calibration Gas Cylinder # Concentration NO (ppm CC453965 493.4 CO(ppm CC453965 520.2 Propane ppm CC453965 495.6 N02 (ppm) CC486070 146.6 Ethylene (ppm CC173895 101.9 Methane (ppm CC453965 499.4 Acetaldehyde ppm) CC321163 196.7 Stack Diagram '*~"~"';""~":"",,".: ".~_'~"·~··"""'N_ '. "-, .........,"'..._~....... .. ....,.... ". ";~" . ' <' [, '~. iT '" "~",, T t A 1 8 Test1 Test 2 Test 3 Time of Reading Atm Pressure (in Hg) Atm Temp CF) EnQine RPM ...---. *Manifold Pres. Vac(") or atiost(pSi) or Boost (psia) \\Sr Manifold Temp CF) _ •.. \\~ \\ " \~,U Psuction (psi) Stage 1 \5 \~ Tsuction OF) Stage 1 Pdischar e (psi) Staqe 1 Psuction (psi) Stage 2 , \ Tsuction OF) Stage 2 l Pdischarae (osj) Staae 2 Psuction (psi) Stage 3 \ \ 1 Tsuction CF) Stage 3 I \ I Pdischar e (osj) Staae 3 Psuction (psi) Stage 4 \ Tsudion 'F) Stage 4 I I Pdischarge (psi) Stage 4 Gas Throuqhput (mmet/d) or ( tv) Ff ) I...e:./hr Pre Cat Temp CF) Post Cat Temp CF) Cat Differential Pres. (" of H20) Humidity % 02% C02 % Dry .....- LOAD % ((»ane!Yor (Estimated) Ignition Timil1i:r('F) AFR Setting mV (~nk) AFR Setting mV k) )'0 c:\, 7,(; "'-'---.-'. "71 n.1 I • Some units show boost in inches of Hg. In this situation please indicate if it is positive (+) or negative(-). Eg: (+12') or (-5') 911712019 Worksheet: O2 Stratification Client:Finley Location:North Randlett E4 Date:6/19/2024 PD:16 DD:40 YES Method 1 Criteria Met UD:8 YES Method 1 Criteria Met Port Point Insertion Depth Reading (inches)(%) A 1 2.66 5.70 A 2 8.00 5.90 A 3 13.33 6.10 A 4 A 5 A 6 A 7 A 8 A 9 A 10 A 11 A 12 Average 5.90 Notes: To demonstrate non-stratified flow and utilize one sampling location O2 may not deviate by more than +/- 0.3% of the average O2 concentration. EPA REFERENCE METHOD 3A (Determination Of Stratification) COMPANY NAME:Finley COMPANY LOCATION:North Randlett E4 DATE:6/19/2024 STACK DIAMETER (inches):16 TRAVERSE POINTS:16 2 TEST RUN #1 TEST RUN #2 TEST RUN #3 AVERAGE O2:5.7 AVERAGE O2:5.9 AVERAGE O2:6.1 AVERAGE CO2:7 AVERAGE CO2:6.9 AVERAGE CO2:6.9 BARO PRESSURE:25.13 BARO PRESSURE:25.13 BARO PRESSURE:25.13 Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O) 1 0.512 0.46 740 0.23 1 0.512 0.46 744 0.23 1 0.512 0.44 743 0.23 2 1.68 0.5 2 1.68 0.49 2 1.68 0.48 3 3.104 0.54 3 3.104 0.53 3 3.104 0.51 4 5.168 0.59 4 5.168 0.58 4 5.168 0.55 5 10.832 0.59 5 10.832 0.62 5 10.832 0.59 6 12.896 0.55 6 12.896 0.59 6 12.896 0.57 7 14.32 0.51 7 14.32 0.56 7 14.32 0.57 8 15.488 0.48 8 15.488 0.52 8 15.488 0.54 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 1 0.512 0.44 740 0.23 1 0.512 0.45 744 0.23 1 0.512 0.45 743 0.23 2 1.68 0.48 2 1.68 0.48 2 1.68 0.49 3 3.104 0.53 3 3.104 0.52 3 3.104 0.54 4 5.168 0.57 4 5.168 0.56 4 5.168 0.58 5 10.832 0.6 5 10.832 0.59 5 10.832 0.62 6 12.896 0.56 6 12.896 0.58 6 12.896 0.57 7 14.32 0.56 7 14.32 0.54 7 14.32 0.54 8 15.488 0.52 8 15.488 0.5 8 15.488 0.55 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 Source Test Report For Uinta Wax Operating, LLC North Randlett Compressor Station Uintah County, Utah Test Date: June 20, 2024 Report Date: July 3, 2024 UDEQ Permit: #DAQE-AN159380002-23 Engine: Caterpillar G3516J SN: N6W/JEF01780 Unit ID: #5 Prepared By: Oasis Emission Consultants, Inc. 2730 Commercial Way Rock Springs, WY 82901 July 3, 2024 Ms. Karen Pratt Uinta Wax Operating, LLC Dear Ms. Pratt: Re: Engine Emission Testing For Uinta Wax Operating, LLC, North Randlett Compressor Station, Unit #5, Permit #DAQE-AN159380002-23. An air emissions test program was conducted on a Caterpillar G3516J engine, operated by Uinta Wax Operating, LLC and designated as Unit #5, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC). Oasis Emission Consultants, Inc. conducted the testing on June 20, 2024. UDEQ Permit #DAQE-AN159380002-23 Emission Levels The average recorded levels were found to comply with emission levels stipulated in the permit, as shown in the attached report and summarized below. Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC ppm @ 15% O2 35.97 41 13.29 61 28.07 60 lbs/hr 0.98 1.52 0.22 1.37 0.73 2.13 *VOC levels reported as non-methane, non-ethane hydrocarbon on a propane basis (NMNEHC C3). EPA 40 CFR 60, Subpart JJJJ Emission Levels Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC g/bhp-hr 0.37 1.0 0.08 2.0 0.28 0.7 Catalyst Parameters (Averaged Over 3 Test Runs) Inlet Temp (deg F) DP (in H2O) 706 5.4 Engine Load (Averaged Over 3 Test Runs) Rated BHP Operating BHP % Load 1379 1199.7 87.0 Testing Protocol The attached report was generated using an extractive FTIR system using methodologies as required by and in accordance with EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, as outlined in the submitted Source Test Protocol. Quality Assurance Oasis has performed a full review of the raw data and calculated results in this report. Any errors we have encountered have been listed in the body of this report. After performing the review, we are confident that this engine has met all requirements. If you have any questions or require further information, please contact the undersigned at (307) 382-3297. Yours truly, Oasis Emission Consultants, Inc. _________________________ _______________________ Charles A. Chapman Crystal Leonard Manager of Technical Services Senior EHS Specialist _________________________ Christopher N. Knott, P.Eng. Director, Engineering and Operations SOURCE EMISSION TEST REPORT UDEQ Permit #DAQE-AN159380002-23 Test Performed By: Oasis Emission Consultants, Inc. Test Company Contact: Chris Knott 2730 Commercial Way Rock Springs, WY 82901 307.382.3297 Owner/Operator: Uinta Wax Operating, LLC Owner/Operator Contact: Karen Pratt (720) 990-9927 Facility Name: North Randlett Compressor Station UTM Coordinates: 593,702 m Easting, 4,453,005 m Northing UTM Zone 12 Uintah County, Utah Emission Source: Caterpillar G3516J Unit #5 Date of Test: June 20, 2024 Date of Report: July 3, 2024 TABLE OF CONTENTS 1.1 Introduction .......................................................................................................................... 1 2.1 Stack Sampling Location ..................................................................................................... 2 3.1 Discussion of NOx, CO and VOC Test Results ................................................................... 3 3.1.1 Source Test 1 ............................................................................................................................................ 3 3.1.2 Source Test 2 ............................................................................................................................................ 3 3.1.3 Source Test 3 ............................................................................................................................................ 3 4.1 Stack Sampling Methods and Procedures ............................................................................ 4 4.2 Equipment Utilization .......................................................................................................... 5 4.3 Measurement of VOC (NMNEHC C3) ............................................................................... 6 4.4 Process Parameters............................................................................................................... 6 5.1 Quality Assurance ................................................................................................................ 7 List of Tables and Figures Figure 1 - Sample Port Location ............................................................................................................................. 2 Figure 2 - Sampling Train Schematic-Method 320 ................................................................................................ 5 Table 1 - Insertion Depths of Traverse Points for Stratification Test ..................................................................... 2 Table 2 - Test Matrix .............................................................................................................................................. 4 Table 3 - Concentrations and Interference .............................................................................................................. 5 APPENDIX A: NOx, CO and VOC Test Data APPENDIX B: Quality Assurance/Calibration Data APPENDIX C: Load Approximation APPENDIX D: Example Calculations and Summary APPENDIX E: Field Notes 1 1.1 Introduction An air emissions test program was conducted on a Caterpillar G3516J engine, operated by Uinta Wax Operating, LLC and designated as Unit #5, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC) defined as non-methane, non-ethane hydrocarbons, reported as propane (NMNEHC C3). The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Three one hour test runs were performed on June 20, 2024 to analyze NOx, CO and VOC emission levels. Test runs were performed according to methodologies outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320 as outlined in the submitted Source Test Protocol dated May 17, 2024. Each one hour test run consisted of 60 readings taken at one minute intervals. Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. The following key personnel were present during testing: David Martinez, OEC Tyler Kyle 2 2.1 Stack Sampling Location The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Testing was conducted on the Caterpillar G3516J engine. The sampling port for moisture, NOx, CO and VOC measurements was approximately 2.7 pipe diameters (36”) downstream from the nearest flow disturbance (Distance B) and 1.4 pipe diameters (19”) upstream from the nearest disturbance (Distance A), as seen in Figure 1. The stack sampling location was placed at approximately 50% insertion depth based on an O2 stratification check which demonstrated a non-stratified flow regime. The stratification was conducted according to EPA 40 CFR 75(A), §6.5.6.1 using 3 traverse points determined according to Table 1 below. Figure 1 - Sample Port Location Table 1 - Insertion Depths of Traverse Points for Stratification Test Traverse Point Insertion Depth (Percent of Stack Diameter) 1 16.6 2 50.0 3 83.3 13.5" A B Oxidation Catalyst 3 3.1 Discussion of NOx, CO and VOC Test Results Three, one hour test runs were performed on June 20, 2024 to analyze exhaust NOx, CO and VOC (NMNEHC C3) emission levels to demonstrate annual compliance with the emissions limits contained in the WDEQ Permit #DAQE-AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ. Testing for NOx, CO and VOC were run concurrently with one another. Each test was performed at the maximum achievable load. Measured emissions were below permitted limits. Please refer to the Appendices for a listing of all raw data, calibration error response and calculations performed per EPA 40 CFR 60(A) requirements. 3.1.1 Source Test 1: Caterpillar G3516J, NOx, CO and VOC The first test was performed from 7:51 to 8:50 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 1199.7 bhp, and the average NOx and CO levels were found to be 0.36 g/bhp-hr and 0.08 g/bhp-hr respectively, below limitations. The VOC level tested at 0.28 g/bhp- hr, which tested in compliance. 3.1.2 Source Test 2: Caterpillar G3516J, NOx, CO and VOC The second test was performed from 8:52 to 9:51 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 1199.7 bhp, and the average NOx and CO levels were found to be 0.37 g/bhp-hr and 0.08 g/bhp-hr respectively, below limitations. The VOC level tested at 0.27 g/bhp- hr, which tested in compliance. 3.1.3 Source Test 3: Caterpillar G3516J, NOx, CO and VOC The third test was performed from 9:53 to 10:52 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 1199.7 bhp, and the average NOx and CO levels were found to be 0.38 g/bhp-hr and 0.09 g/bhp-hr respectively, below limitations. The VOC level tested at 0.28 g/bhp- hr, which tested in compliance. Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 1 90.92 0.36 33.98 0.08 71.75 0.28 5.5 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 2 91.36 0.37 33.86 0.08 71.44 0.27 5.9 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 3 94.43 0.38 34.39 0.09 72.79 0.28 5.9 4 4.1 Stack Sampling Methods and Procedures Testing followed EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, with no exceptions. Table 2 - Test Matrix Method Title Parameter Reference EPA 40 CFR 60 Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources Sampling Point Determination https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_1_3.pdf EPA 40 CFR 60 Appendix A, Method 2 Determination of Stack Gas Velocity and Volumetric Flow Rate Exhaust Effluent Flow https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_2.pdf EPA 40 CFR 60 Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight O2, CO2, Dry Volumetric Flow Rate https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_3.pdf EPA 40 CFR 63 Appendix A, EPA Method 320 Vapor Phase Organic and Inorganic Emissions by Extractive FTIR Nitrogen Oxides, Carbon Monoxide, Non- Methane Non- Ethane Hydrocarbons on a Propane Basis https://www.epa.gov/ emc/method-320- vapor-phase-organic- and-inorganic- emissions-extractive- ftir United States. U.S. Environmental Protection Agency. “EMC Promulgated Test Methods.” Air Emission Measurement Center (EMC). 31 August 2023. Web. 2 July 2024. <https://www.epa.gov/emc/emc-promulgated-test-methods>. ASTM International. “Standards & Publications.” All Environment Standards. Web. 2 July 2024. <https://www.astm.org/Standards/D6348.htm>. 5 4.2 Equipment Utilization The following equipment was used during the tests performed at this facility in conjunction with procedures outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320. • (1) MKS MultiGas 2030 FTIR Continuous Gas Analyzer (0.210 L/min sample flow, 0.014 atmosphere sample pressure, 1 atmosphere cell pressure, 191°C cell temperature) • (1) Laptop Computer for the FTIR Analyzer using MKS MG2000 Software • (1) 75ft or 100ft Heated Teflon Line w/ Heated Sample Probe and Spike Bypass Line • S-Type Pitot Tube c/w 20 ft. Heated Sample Line (coefficient 0.84) • (1) Enerac 500 Portable O2/CO2 Analyzer • (1) Fyrite O2/CO2 Analyzer • (5) EPA Protocol G1 Calibration Gas (NOx, CO, C3H8, C2H4 and NO2) The MKS Multigas 2030 FTIR Analyzer operated with a spectral resolution of 0.5 cm-1 and a scan time of 30 seconds. The FTIR spectrometer utilizes a multi-pass gas cell with a 5.11 meter effective pathlength. Figure 2 - Sampling Train Schematic-Method 320 Table 3 - Concentrations and Interference 6 The MKS 2030 software provides a Natural Gas Method that is designed to minimize all expected interferences by removing the regions in the quant region where they are most absorbed (i.e. picket fence approach). So, for example, all the water peaks that are greater than about 0.1 abs are removed from the quant region. Since the spectral noise measured (sample spectrum) is in the range of 0.001 absorbance, it is desirable to have any error within this range. The MKS software will match the water calibration spectrum to the sample spectrum at any 1 point in the spectrum to about 1% precision. So, 1% of 0.1 absorbance is 0.001 abs. This is why any peaks greater than this for interfering compounds are usually excluded so they do not interfere. To summarize, the MKS software and the method are designed to minimize any interferences by removing their largest interfering absorptions. 4.3 Measurement of VOC (NMNEHC C3) The algorithm currently used for NMNEHC C3 and developed for natural gas fired applications by Dr. Spartz and MKS instruments in accordance with EPA standards, is the following: (2.4*c8/(1+exp((2-c8)/0.2))+1.9*c11/(1+exp((2-c11)/0.2))+6*c12/(1+exp((0.5-c12) /0.2))+2.85*c13/(1+exp((2-c13)/0.2))+3*c14/(1+exp((1-c14)/0.2)))/3 c8= acetylene c11= ethylene c12= hexane c13= propylene c14= propane Note: The constants in front of each of the compounds listed represents the FID response factor when calibrated with Propane. As with any CEMS analyzer, the FTIR may demonstrate a negative zero bias. The “exp” functions listed in the algorithm above are intended to mathematically filter out any negative biases and set them to approach zero. 4.4 Process Parameters Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. Results are provided in Appendix C. 7 5.1 Quality Assurance The MKS Multigas 2030 FTIR Analyzer was used to measure NOx, CO and VOC on a dry basis. A pre Direct and System calibration measurement was made on compounds of NOx, CO, C3H8 and C2H4. In addition, post System calibrations were made on compounds of NOx, CO, C3H8 and C2H4. Compounds of CO2 and C3H8 were measured for the quality assurance spiking requirements. Levels for calibrations and zeroes must be within +/- 5% of the certified calibration gas or response to zero gas, respectively. CTS procedures were followed according to EPA requirements for both pre and post testing. Similarly, QA spiking procedures were followed. Analysis of the CO2 exhaust effluent was used to determine the dilution factor. Steady levels of the CO2 were observed and a sufficient duration of time was allowed to elapse for a representative average. The calibration gas was spiked into the effluent stream using a bypass line at approximately 10% of the sampling rate. The dilution factor was obtained from observation of the stack CO2 behavior using the following equation: CO2AVG – CO2SPIKE DF = ------------------------ CO2 AVG Where: CO2AVG = The average undiluted CO2 stack gas concentration of spike measurements CO2SPIKE = The average diluted CO2 stack gas concentration when spiked The sample recovery was then obtained from the following equation: % REC = (Spike MEAS – Stack MEAS)* (1 – DF) --------------------------------------------------------- CS * DF Where: Spike MEAS = The average diluted stack gas concentration when spiked Stack MEAS = The average undiluted stack gas concentration DF = Dilution factor CS = Certified concentration of calibration standards The Sample Recovery average level for C3H8 was found to be 70.9%, which was within the allowable tolerance of Method 320 (70% to 130%). A summary of all spiking procedures/results can be found in Appendix B. APPENDIX A NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 66.578706 22.995984 89.57469 34.141763 72.280328 10.480278 7:51:32 06/20/2024 2 66.539856 22.865903 89.405759 33.967144 70.248665 10.756217 7:52:32 06/20/2024 3 67.989985 23.35275 91.342735 34.029974 72.122076 10.978572 7:53:32 06/20/2024 4 68.013983 23.384017 91.398 34.116116 72.234453 11.173179 7:54:32 06/20/2024 5 70.582757 24.239744 94.822501 34.338542 68.988674 11.368729 7:55:32 06/20/2024 6 65.825846 22.551856 88.377702 34.06283 73.558290 11.489541 7:56:32 06/20/2024 7 67.489728 23.276576 90.766304 34.153525 72.297584 11.660226 7:57:32 06/20/2024 8 65.850035 22.778647 88.628682 33.907839 72.983360 11.851204 7:58:32 06/20/2024 9 68.223274 23.444627 91.667901 33.848916 72.030905 11.957466 7:59:32 06/20/2024 10 67.252863 22.962419 90.215282 33.948238 71.063900 12.018505 8:00:33 06/20/2024 11 66.350932 22.648027 88.998959 33.913368 71.454825 12.067117 8:01:33 06/20/2024 12 67.639099 23.281843 90.920942 34.069086 70.379654 12.024613 8:02:33 06/20/2024 13 67.742561 23.233166 90.975727 33.914383 70.354515 11.94656 8:03:33 06/20/2024 14 69.456651 23.465974 92.922625 33.839745 72.009453 11.708729 8:04:33 06/20/2024 15 64.548295 21.679488 86.227783 33.740615 73.035190 10.939501 8:05:33 06/20/2024 16 67.326808 22.783081 90.109889 33.959089 73.253741 10.629921 8:06:33 06/20/2024 17 66.347987 22.711449 89.059436 33.877721 73.555708 10.428969 8:07:33 06/20/2024 18 65.851752 22.526336 88.378088 33.905357 73.286558 10.528648 8:08:33 06/20/2024 19 65.950628 22.570307 88.520935 33.844772 71.647672 10.490992 8:09:33 06/20/2024 20 67.550357 23.073598 90.623955 33.848852 71.571936 10.489178 8:10:34 06/20/2024 21 67.064135 22.862195 89.92633 33.960383 72.619897 10.496663 8:11:34 06/20/2024 22 66.854132 22.908461 89.762593 33.865906 71.195415 10.422407 8:12:34 06/20/2024 23 68.459915 23.398569 91.858484 33.930434 71.923639 10.467695 8:13:34 06/20/2024 24 67.137217 22.825253 89.96247 33.893274 72.554807 10.51766 8:14:34 06/20/2024 25 67.027887 22.817766 89.845653 33.933304 70.876081 10.74548 8:15:34 06/20/2024 26 68.614465 23.393774 92.008239 33.987845 71.912381 10.707613 8:16:34 06/20/2024 27 67.242981 22.850205 90.093186 33.852505 70.528367 10.592215 8:17:34 06/20/2024 28 67.634602 22.805718 90.44032 33.86517 70.225921 10.679582 8:18:34 06/20/2024 29 69.289262 23.39491 92.684172 34.116314 71.406541 10.841096 8:19:34 06/20/2024 30 68.608738 23.147919 91.756657 34.075233 71.804026 11.120686 8:20:34 06/20/2024 31 67.158127 22.687932 89.846059 34.001101 73.100226 11.239809 8:21:34 06/20/2024 32 68.651855 23.184927 91.836782 34.088988 70.398840 11.17556 8:22:35 06/20/2024 33 68.39621 22.875265 91.271475 33.82797 72.668968 11.152061 8:23:35 06/20/2024 34 68.480473 22.828489 91.308962 33.863834 71.010233 11.097198 8:24:35 06/20/2024 35 68.483254 22.952682 91.435936 33.928206 71.148972 11.162496 8:25:35 06/20/2024 36 68.580206 23.054237 91.634443 33.952311 71.212792 11.164084 8:26:35 06/20/2024 37 68.326129 22.861595 91.187724 33.886819 71.080225 11.111997 8:27:35 06/20/2024 38 68.075561 22.666951 90.742512 33.934307 71.537215 11.056652 8:28:35 06/20/2024 39 68.858304 22.947907 91.806211 33.989808 70.898789 11.005897 8:29:35 06/20/2024 40 68.635722 22.897464 91.533186 33.846298 70.500184 10.949507 8:30:35 06/20/2024 41 68.578516 22.95376 91.532276 34.047363 71.441880 10.866733 8:31:35 06/20/2024 42 69.377677 23.321036 92.698713 34.126449 72.020475 10.876829 8:32:35 06/20/2024 43 67.837145 22.723683 90.560828 33.948134 73.203765 10.859913 8:33:36 06/20/2024 44 68.840143 22.942498 91.782641 33.966267 70.956054 10.869228 8:34:36 06/20/2024 45 68.764498 22.796683 91.561181 33.922165 72.624365 10.864047 8:35:36 06/20/2024 46 67.620338 22.487028 90.107366 33.717992 72.817621 10.849739 8:36:36 06/20/2024 47 69.311754 23.275229 92.586983 34.08071 72.033262 10.868317 8:37:36 06/20/2024 48 68.130426 22.88764 91.018066 33.963828 72.659001 10.843248 8:38:36 06/20/2024 49 67.269912 22.537961 89.807873 33.816913 71.274307 10.838523 8:39:36 06/20/2024 50 70.193372 23.671247 93.864619 34.226438 70.813787 10.886729 8:40:37 06/20/2024 51 69.23088 23.326121 92.557001 34.144384 71.703154 10.863451 8:41:36 06/20/2024 52 68.054653 22.969161 91.023814 34.090672 72.791459 10.843495 8:42:36 06/20/2024 53 67.747488 23.050762 90.79825 34.040243 73.762749 10.847151 8:43:36 06/20/2024 54 69.121389 23.528327 92.649716 34.157525 70.796315 10.854044 8:44:37 06/20/2024 55 69.335689 23.46128 92.796969 34.186314 71.253208 10.856317 8:45:37 06/20/2024 56 66.791767 22.429291 89.221058 33.944034 70.965892 10.837884 8:46:37 06/20/2024 57 68.548922 23.150315 91.699237 33.976868 72.664993 10.830496 8:47:37 06/20/2024 58 68.047416 22.94176 90.989176 33.966757 70.861754 10.823113 8:48:37 06/20/2024 59 68.713611 23.373571 92.087182 34.008227 72.798580 10.807543 8:49:37 06/20/2024 60 68.564009 23.202033 91.766042 34.05962 70.648957 10.820765 8:50:37 06/20/2024 AVG 67.91 0.00 90.92 33.98 71.75 11.00 ppm@15% O2 34.83 13.02 27.49 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.36 0.96 0.08 0.22 0.28 0.73 #5 FTIR Measurements Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 1 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.59 1231 0.26 0.768 Average O2 5.5 (% dry)A 2 1.42 0.62 0.787 Average CO2 6.7 (% dry)A 3 2.62 0.66 0.812 Average N2 + CO 87.8 (% dry)A 4 4.36 0.71 0.843 Dry Molecular Weight 29.29 lb/lbmol A 5 9.14 0.74 0.860 Wet Molecular Weight 28.05 lb/lbmol A 6 10.88 0.70 0.837 EPA REFERENCE METHOD 320 A 7 12.08 0.67 0.819 Barometric Pressure 25.17 in Hg A 8 13.00 0.63 0.794 Moisture Content 11.00 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 90.92 ppm A 11 Calculated NOx Mass Output 0.96 lbs/hr A 12 Calculated NOx Output 0.36 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 33.98 ppm A 15 Calculated CO Mass Output 0.22 lbs/hr A 16 Calculated CO Output 0.08 g/bhp-hr B 1 0.50 0.61 1231 0.26 0.781 EPA REFERENCE METHOD 320 B 2 1.42 0.64 0.800 Average Analyzer NMNEHC Level 71.75 ppm B 3 2.62 0.67 0.819 Calculated NMNEHC Mass Output 0.73 lbs/hr B 4 4.36 0.70 0.837 Calculated NMNEHC Output 0.28 g/bhp-hr B 5 9.14 0.69 0.831 LOAD APPROXIMATION B 6 10.88 0.71 0.843 Estimated Engine Load 1199.7 BHP B 7 12.08 0.66 0.812 B 8 13.00 0.62 0.787 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.7 1231 0.3 0.814 Average Stack Gas Velocity 77.19 ft/sec Average Dry Flowrate 1479.54 dscfm TEST RUN # 1 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 68.058618 22.735929 90.794547 33.841874 71.035151 10.808677 8:52:37 06/20/2024 2 68.013259 22.714179 90.727438 33.589767 71.992553 10.756471 8:53:37 06/20/2024 3 69.139439 23.237856 92.377295 33.969185 71.898633 10.727555 8:54:37 06/20/2024 4 67.809641 22.778445 90.588086 33.928437 71.140806 10.66888 8:55:38 06/20/2024 5 67.468971 22.681288 90.150259 33.862712 72.563443 10.59245 8:56:38 06/20/2024 6 69.080598 23.119777 92.200375 33.884708 70.160564 10.564197 8:57:38 06/20/2024 7 68.713656 22.919742 91.633398 33.877979 70.919290 10.501873 8:58:38 06/20/2024 8 69.209078 22.997633 92.206711 33.930711 70.909934 10.522283 8:59:38 06/20/2024 9 67.389565 22.393441 89.783006 33.858276 71.538479 10.532749 9:00:38 06/20/2024 10 69.343122 23.180148 92.52327 33.971127 71.294083 10.589613 9:01:38 06/20/2024 11 69.004613 23.134647 92.13926 33.740106 73.223011 10.664905 9:02:38 06/20/2024 12 68.913257 23.022378 91.935635 33.915304 71.155455 10.763926 9:03:39 06/20/2024 13 68.850515 22.902527 91.753042 33.909439 71.118634 11.001655 9:04:39 06/20/2024 14 68.404461 22.587573 90.992034 33.861905 71.870009 10.960899 9:05:38 06/20/2024 15 69.378359 22.895227 92.273586 33.798414 71.771107 10.853261 9:06:38 06/20/2024 16 68.045475 22.658342 90.703817 33.789291 72.008106 10.752973 9:07:39 06/20/2024 17 68.308125 22.779576 91.087701 33.828209 73.168438 10.717636 9:08:39 06/20/2024 18 67.95018 22.695019 90.645199 33.894191 72.681760 10.683604 9:09:39 06/20/2024 19 67.611116 22.517802 90.128918 33.871584 71.422103 10.697496 9:10:39 06/20/2024 20 67.633999 22.352695 89.986694 33.820378 71.692317 10.658951 9:11:39 06/20/2024 21 70.334669 23.39169 93.726359 34.025645 70.880671 10.668599 9:12:39 06/20/2024 22 69.408372 22.866421 92.274793 33.866602 71.509985 10.732089 9:13:39 06/20/2024 23 68.371422 22.743996 91.115418 33.997495 71.458157 10.798336 9:14:40 06/20/2024 24 66.610775 22.336307 88.947082 33.840133 73.562083 10.711593 9:15:40 06/20/2024 25 67.311075 22.371003 89.682078 33.861739 72.389479 10.701009 9:16:39 06/20/2024 26 69.09534 22.942698 92.038038 33.937806 72.953562 10.701615 9:17:40 06/20/2024 27 68.912217 22.866579 91.778796 34.003993 70.864565 10.705 9:18:40 06/20/2024 28 68.788737 22.813014 91.601751 33.891407 71.778151 10.699846 9:19:40 06/20/2024 29 68.734378 22.700016 91.434394 33.899709 71.938067 10.72737 9:20:40 06/20/2024 30 68.362576 22.635095 90.997671 33.944061 71.503847 10.718396 9:21:40 06/20/2024 31 67.98079 22.532761 90.513551 33.912783 72.007943 10.714987 9:22:40 06/20/2024 32 68.327758 22.670037 90.997795 33.905961 72.307292 10.70229 9:23:40 06/20/2024 33 70.417408 23.363175 93.780583 33.910613 70.169645 10.720572 9:24:40 06/20/2024 34 69.239879 22.92041 92.160289 33.789518 71.261411 10.702934 9:25:40 06/20/2024 35 68.658898 22.630321 91.289219 33.786564 70.934080 10.687711 9:26:40 06/20/2024 36 70.046137 22.851863 92.898 33.572721 70.883599 10.70204 9:27:40 06/20/2024 37 68.159868 22.430745 90.590613 33.645636 71.106412 10.719108 9:28:41 06/20/2024 38 68.662419 22.437499 91.099918 33.793754 70.189865 10.710593 9:29:41 06/20/2024 39 68.672029 22.532161 91.20419 33.888189 70.580295 10.704976 9:30:41 06/20/2024 40 69.043892 22.589459 91.633351 33.879979 70.930196 10.717237 9:31:41 06/20/2024 41 68.428019 22.385757 90.813776 33.823197 70.327680 10.696309 9:32:41 06/20/2024 42 69.880378 22.769817 92.650195 34.034019 71.032131 10.702067 9:33:41 06/20/2024 43 67.949436 22.126705 90.076141 33.717384 70.828755 10.686815 9:34:41 06/20/2024 44 68.566156 22.373396 90.939552 33.881306 71.544865 10.675746 9:35:41 06/20/2024 45 68.853377 22.453075 91.306452 33.973463 72.638685 10.675568 9:36:41 06/20/2024 46 68.780552 22.503496 91.284048 33.975385 71.760567 10.670493 9:37:41 06/20/2024 47 68.888094 22.530789 91.418883 33.933628 72.947569 10.660746 9:38:41 06/20/2024 48 68.922242 22.488334 91.410576 33.985636 72.544575 10.668439 9:39:42 06/20/2024 49 69.289134 22.4599 91.749034 33.829123 71.032948 10.657428 9:40:42 06/20/2024 50 69.773539 22.500883 92.274422 33.864196 71.188381 10.657737 9:41:42 06/20/2024 51 68.672879 22.191563 90.864442 33.725249 71.299654 10.652981 9:42:42 06/20/2024 52 69.317148 22.354068 91.671216 33.816732 70.422314 10.687376 9:43:42 06/20/2024 53 68.20481 22.140106 90.344916 33.727216 70.584949 10.72149 9:44:42 06/20/2024 54 68.653089 22.334591 90.98768 33.845756 71.197210 10.719068 9:45:42 06/20/2024 55 69.287478 22.52146 91.808938 33.610431 69.656497 10.724548 9:46:42 06/20/2024 56 68.621788 22.420202 91.04199 33.834301 70.273031 10.722529 9:47:42 06/20/2024 57 69.044476 22.580448 91.624924 33.850865 71.640831 10.744802 9:48:42 06/20/2024 58 68.383658 22.359353 90.743011 33.870845 70.603948 10.744509 9:49:43 06/20/2024 59 68.553875 22.346261 90.900136 33.889683 72.150563 10.750426 9:50:42 06/20/2024 60 70.263477 22.882801 93.146278 33.97056 70.207875 10.748919 9:51:43 06/20/2024 AVG 68.70 0.00 91.36 33.86 71.44 10.70 ppm@15% O2 35.93 13.32 28.10 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.37 0.97 0.08 0.22 0.27 0.72 Calculated Emission Levels Record Date Uinta Wax Operating, LLC North Randlett Compressor Station Run 2 #5 FTIR Measurements EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.60 1243 0.25 0.775 Average O2 5.9 (% dry)A 2 1.42 0.64 0.800 Average CO2 6.7 (% dry)A 3 2.62 0.68 0.825 Average N2 + CO 87.4 (% dry)A 4 4.36 0.72 0.849 Dry Molecular Weight 29.31 lb/lbmol A 5 9.14 0.75 0.866 Wet Molecular Weight 28.10 lb/lbmol A 6 10.88 0.69 0.831 EPA REFERENCE METHOD 320 A 7 12.08 0.69 0.831 Barometric Pressure 25.17 in Hg A 8 13.00 0.65 0.806 Moisture Content 10.70 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 91.36 ppm A 11 Calculated NOx Mass Output 0.97 lbs/hr A 12 Calculated NOx Output 0.37 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 33.86 ppm A 15 Calculated CO Mass Output 0.22 lbs/hr A 16 Calculated CO Output 0.08 g/bhp-hr B 1 0.50 0.58 1243 0.25 0.762 EPA REFERENCE METHOD 320 B 2 1.42 0.61 0.781 Average Analyzer NMNEHC Level 71.44 ppm B 3 2.62 0.65 0.806 Calculated NMNEHC Mass Output 0.72 lbs/hr B 4 4.36 0.69 0.831 Calculated NMNEHC Output 0.27 g/bhp-hr B 5 9.14 0.70 0.837 LOAD APPROXIMATION B 6 10.88 0.68 0.825 Estimated Engine Load 1199.7 BHP B 7 12.08 0.66 0.812 B 8 13.00 0.64 0.800 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.7 1243 0.3 0.815 Average Stack Gas Velocity 77.53 ft/sec Average Dry Flowrate 1476.55 dscfm TEST RUN # 2 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 70.003509 22.665175 92.668684 33.930509 71.202573 10.773325 9:53:43 06/20/2024 2 69.236348 22.48329 91.719638 33.92468 70.776239 10.756541 9:54:43 06/20/2024 3 68.56736 22.237535 90.804895 33.96422 71.867624 10.746681 9:55:43 06/20/2024 4 69.510562 22.574701 92.085263 33.924728 71.416174 10.757064 9:56:43 06/20/2024 5 70.343918 22.944834 93.288752 34.162268 70.734807 10.764432 9:57:43 06/20/2024 6 69.261987 22.553531 91.815518 33.955488 73.230406 10.750737 9:58:43 06/20/2024 7 70.385155 22.772376 93.157531 33.993037 70.672416 10.769906 9:59:43 06/20/2024 8 70.543144 22.801539 93.344683 34.027241 73.100416 10.749207 10:00:44 06/20/2024 9 70.5801 22.77278 93.35288 34.170237 72.709247 10.75638 10:01:43 06/20/2024 10 71.322401 22.988548 94.310949 34.005832 72.118944 10.752709 10:02:44 06/20/2024 11 69.307276 22.264219 91.571495 34.027993 73.720720 10.774331 10:03:44 06/20/2024 12 70.280943 22.59206 92.873003 34.080777 73.122069 10.752396 10:04:44 06/20/2024 13 70.179786 22.585212 92.764998 34.009636 73.894499 10.759877 10:05:44 06/20/2024 14 70.545948 22.608387 93.154335 34.141137 73.053626 10.773909 10:06:44 06/20/2024 15 70.603642 22.574135 93.177777 34.204309 73.937323 10.792613 10:07:44 06/20/2024 16 69.691528 22.571373 92.262901 34.101268 72.949379 10.768233 10:08:44 06/20/2024 17 69.576188 22.42994 92.006128 34.167129 73.150460 10.789995 10:09:44 06/20/2024 18 69.676374 22.495877 92.172251 34.103211 74.795067 10.752148 10:10:45 06/20/2024 19 69.724118 22.447148 92.171266 34.073035 75.195749 10.75092 10:11:44 06/20/2024 20 68.782016 22.205376 90.987392 33.892071 73.554871 10.740991 10:12:44 06/20/2024 21 69.534972 22.348752 91.883724 34.035014 72.362872 10.78372 10:13:45 06/20/2024 22 68.460502 21.981951 90.442453 34.039331 72.565988 10.804853 10:14:45 06/20/2024 23 68.716608 22.124944 90.841552 34.089452 72.340831 10.824047 10:15:45 06/20/2024 24 68.923696 22.18923 91.112926 34.174412 73.915527 10.784208 10:16:45 06/20/2024 25 70.789973 22.777719 93.567692 34.02437 73.302741 10.808919 10:17:45 06/20/2024 26 70.11674 22.584267 92.701007 34.19238 72.426846 10.811372 10:18:45 06/20/2024 27 70.086449 22.501658 92.588107 34.156888 71.937815 10.839678 10:19:45 06/20/2024 28 69.321899 22.348997 91.670896 34.114151 71.925176 10.810285 10:20:45 06/20/2024 29 69.910874 22.598016 92.50889 34.136914 72.167085 10.830448 10:21:45 06/20/2024 30 70.473739 22.690236 93.163975 34.273987 70.273185 10.83821 10:22:45 06/20/2024 31 71.194821 22.819511 94.014332 34.146496 72.655630 10.84244 10:23:46 06/20/2024 32 69.985111 22.36121 92.346321 34.034628 73.340940 10.820166 10:24:45 06/20/2024 33 69.114375 22.112093 91.226468 34.004544 71.593911 10.826268 10:25:46 06/20/2024 34 70.089834 22.438377 92.528211 34.188367 71.903488 10.828016 10:26:46 06/20/2024 35 70.714925 22.670331 93.385256 34.190379 72.262067 10.80727 10:27:46 06/20/2024 36 71.47496 22.864035 94.338995 34.316147 71.214476 10.755995 10:28:46 06/20/2024 37 65.379512 21.49125 86.870762 33.760838 73.921336 10.725251 10:29:46 06/20/2024 38 70.141507 23.041235 93.182742 34.251992 73.781951 10.755621 10:30:46 06/20/2024 39 71.717838 23.300696 95.018534 34.47919 71.716761 10.783706 10:31:46 06/20/2024 40 72.685908 23.415182 96.10109 34.441609 73.813525 10.758964 10:32:46 06/20/2024 41 71.19832 22.940964 94.139284 34.352997 72.698458 10.756916 10:33:46 06/20/2024 42 70.86506 22.838485 93.703545 34.321644 75.280303 10.767671 10:34:46 06/20/2024 43 70.088647 22.538603 92.62725 34.365083 74.681006 10.76647 10:35:46 06/20/2024 44 70.579014 22.700902 93.279916 34.317963 75.584568 10.758175 10:36:47 06/20/2024 45 69.909268 22.421772 92.33104 34.168851 73.752879 10.776995 10:37:47 06/20/2024 46 70.209762 22.586035 92.795797 34.422784 74.774493 10.788531 10:38:47 06/20/2024 47 69.913745 22.490155 92.4039 34.235653 73.622011 10.786499 10:39:47 06/20/2024 48 69.35766 22.255894 91.613554 34.330996 72.846626 10.783235 10:40:47 06/20/2024 49 69.676369 22.34635 92.022719 34.196977 72.360491 10.781017 10:41:47 06/20/2024 50 69.114191 22.128217 91.242408 34.091034 72.809195 10.746091 10:42:47 06/20/2024 51 69.0438 22.184727 91.228527 34.112046 72.854414 10.769202 10:43:47 06/20/2024 52 69.642492 22.422958 92.06545 34.002128 73.978333 10.755062 10:44:47 06/20/2024 53 70.048604 22.826485 92.875089 34.243149 73.978350 10.764979 10:45:47 06/20/2024 54 87.460174 32.459452 119.919626 36.203583 69.227956 10.946964 10:46:48 06/20/2024 55 83.543215 32.922318 116.465533 36.714817 69.517731 11.016254 10:47:48 06/20/2024 56 73.457029 29.491862 102.948891 36.097641 72.548341 10.965671 10:48:48 06/20/2024 57 76.092079 30.375674 106.467753 36.409573 73.723720 11.014965 10:49:48 06/20/2024 58 76.199832 30.551351 106.751183 36.284824 72.653903 11.008535 10:50:48 06/20/2024 59 74.294281 29.875055 104.169336 36.185487 73.700909 11.003257 10:51:48 06/20/2024 60 76.668084 30.843519 107.511603 36.577416 71.941753 11.03484 10:52:48 06/20/2024 AVG 70.91 23.52 94.43 34.39 72.79 10.80 ppm@15% O2 37.14 13.53 28.63 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.38 1.02 0.09 0.23 0.28 0.75 FTIR Measurements #5 Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 3 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.65 1241 0.27 0.806 Average O2 5.9 (% dry)A 2 1.42 0.67 0.819 Average CO2 6.7 (% dry)A 3 2.62 0.72 0.849 Average N2 + CO 87.4 (% dry)A 4 4.36 0.76 0.872 Dry Molecular Weight 29.31 lb/lbmol A 5 9.14 0.79 0.889 Wet Molecular Weight 28.09 lb/lbmol A 6 10.88 0.68 0.825 EPA REFERENCE METHOD 320 A 7 12.08 0.64 0.800 Barometric Pressure 25.17 in Hg A 8 13.00 0.60 0.775 Moisture Content 10.80 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 94.43 ppm A 11 Calculated NOx Mass Output 1.02 lbs/hr A 12 Calculated NOx Output 0.38 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 34.39 ppm A 15 Calculated CO Mass Output 0.23 lbs/hr A 16 Calculated CO Output 0.09 g/bhp-hr B 1 0.50 0.63 1241 0.27 0.794 EPA REFERENCE METHOD 320 B 2 1.42 0.66 0.812 Average Analyzer NMNEHC Level 72.79 ppm B 3 2.62 0.70 0.837 Calculated NMNEHC Mass Output 0.75 lbs/hr B 4 4.36 0.72 0.849 Calculated NMNEHC Output 0.28 g/bhp-hr B 5 9.14 0.75 0.866 LOAD APPROXIMATION B 6 10.88 0.71 0.843 Estimated Engine Load 1199.7 BHP B 7 12.08 0.67 0.819 B 8 13.00 0.68 0.825 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.7 1241 0.3 0.830 Average Stack Gas Velocity 78.92 ft/sec Average Dry Flowrate 1503.80 dscfm TEST RUN # 3 APPENDIX B Date Time NO 191C span NO2 191C span H2O% (high) 191C Formaldehyde 191C Ethylene 191C TE span Propane 191C span Acetaldehyde 191C span CO ppm 191C (1of2) spanCO ppm Dry CO2% 191C NOx Wet NOx Dry NM NE HC C3 Temp ( C )Pressure (atm)6/20/2024 7:28:45 -0.181153 -0.038142 0.009883 -0.134745 0.267542 -0.087151 -1.166035 0.027277 0.02728 0.006975 -0.219296 -0.219317 -0.003927 192.22406 1.0108346/20/2024 7:28:52 -0.052176 -0.064178 -0.0038 -0.059094 0.01971 0.062445 -1.551326 -0.212959 -0.212951 -0.018026 -0.116354 -0.11635 -0.01007 192.191345 1.0065466/20/2024 7:29:00 -0.283468 -0.004626 -0.000938 0.109496 0.363759 -0.340284 -0.96249 0.014845 0.014845 0.014032 -0.288094 -0.288092 -0.010791 192.278564 1.009117 6/20/2024 7:29:07 -0.094397 -0.072223 0.003545 0.169579 0.406995 -0.224465 0.03704 -0.052683 -0.052685 0.011253 -0.166619 -0.166625 -0.012127 192.220413 1.0086126/20/2024 7:29:44 0 0 0 0 0 0 0 0 0 0 0 0 0 192.292664 1.008378 6/20/2024 7:29:58 0.000066 -0.117515 0.001261 -0.021597 0.698156 -0.319776 -0.112155 0.066875 0.066876 -0.024629 -0.117449 -0.117451 0.018324 192.342758 1.0079426/20/2024 7:30:05 0.013208 -0.075128 0.0062 0.021157 -0.201931 -1.011696 -0.446033 -0.032166 -0.032168 -0.018172 -0.06192 -0.061924 -0.00217 192.394852 1.0034256/20/2024 7:30:13 -0.212345 0.063074 0.006482 0.029079 0.523412 -0.520301 0.062065 0.064604 0.064608 0.000159 -0.14927 -0.14928 0.009736 192.42392 1.0040676/20/2024 7:30:20 0.007408 -0.124242 0.002703 0.207217 -0.382077 -1.224483 0.289142 0.213709 0.213715 0.001542 -0.116833 -0.116836 -0.002606 192.365784 1.0097596/20/2024 7:30:28 -0.146927 -0.019042 -0.004443 0.031604 0.7708 -0.469643 -0.065742 -0.109082 -0.109077 0.010257 -0.16597 -0.165962 0.006347 192.409378 1.0018646/20/2024 7:30:35 0.020309 -0.023391 0.001542 0.033914 0.147682 -1.114965 0.099529 -0.003455 -0.003455 -0.011341 -0.003082 -0.003082 0.00008 192.351242 1.0073266/20/2024 7:30:43 0.152717 -0.019423 0.002538 0.22846 -0.417996 -0.542546 -0.598511 0.090733 0.090736 -0.006024 0.133295 0.133298 -0.009295 192.363953 1.004073 6/20/2024 7:30:50 0.223334 -0.02882 -0.002437 0.297429 0.086671 -0.502008 0.048703 0.061462 0.061461 0.001562 0.194514 0.194509 0.206114 192.42392 1.0056286/20/2024 7:30:58 -0.064296 -0.112075 0.001801 0.016748 0.160852 -1.089518 0.224837 -0.198024 -0.198028 -0.008941 -0.176371 -0.176374 0.026336 192.3367 1.006271 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm)6/20/2024 7:31:32 514.435461 490.545871 491.429607 192.342758 1.007755 6/20/2024 7:34:58 97.723085 192.274933 0.9997226/20/2024 7:31:39 514.409899 492.473535 496.748748 192.322174 1.006592 6/20/2024 7:35:05 97.486638 192.249496 0.999569 6/20/2024 7:31:47 515.727512 492.378613 494.430541 192.293091 1.006592 6/20/2024 7:35:13 97.267884 192.205887 1.0017726/20/2024 7:31:54 512.165998 488.848754 496.491317 192.365784 1.01389 6/20/2024 7:35:20 98.949088 192.205887 1.0002576/20/2024 7:32:02 516.393528 493.189853 500.326268 192.3367 1.004802 6/20/2024 7:35:28 98.521361 192.278564 1.0011766/20/2024 7:32:09 513.494094 490.913017 492.429712 192.264023 1.010999 6/20/2024 7:35:35 98.296444 192.220413 1.0019566/20/2024 7:32:17 513.317095 490.858367 494.681897 192.31308 1.010901 6/20/2024 7:35:43 98.381723 192.211334 1.0030296/20/2024 7:32:25 513.160638 489.382232 496.178299 192.322174 1.012651 6/20/2024 7:35:51 97.660325 192.176819 1.0002126/20/2024 7:32:32 512.708588 488.559609 491.331682 192.264023 1.014349 6/20/2024 7:35:58 98.027146 192.249496 0.998926 6/20/2024 7:32:39 513.709077 491.182568 497.894137 192.3367 1.011963 6/20/2024 7:36:05 98.071841 192.234955 0.999936 Date Time NO2 191C span Temp ( C )Pressure (atm)6/20/2024 7:33:15 143.581688 192.300369 0.9955186/20/2024 7:33:23 144.227378 192.307632 0.9957596/20/2024 7:33:30 144.872837 192.351242 0.99732 6/20/2024 7:33:38 144.857318 192.3367 0.998886/20/2024 7:33:45 144.828754 192.322174 1.0004416/20/2024 7:33:53 144.730044 192.307632 1.002926/20/2024 7:34:00 144.60986 192.351242 1.0001776/20/2024 7:34:08 144.830405 192.293091 1.0023236/20/2024 7:34:15 145.391101 192.293091 1.0023696/20/2024 7:34:23 146.004332 192.264023 0.99911 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm)6/20/2024 7:36:38 465.143412 445.428007 447.178022 192.207092 0.96435 6/20/2024 7:38:30 97.267017 192.191345 0.9847426/20/2024 7:36:45 502.837422 481.591757 487.663614 192.234955 0.995116 6/20/2024 7:38:37 98.670916 192.147736 0.9980086/20/2024 7:36:52 512.300308 489.736622 496.939764 192.278564 1.010631 6/20/2024 7:38:45 98.82138 192.147736 0.9988346/20/2024 7:37:00 513.66101 492.165798 494.476008 192.234955 1.005995 6/20/2024 7:38:52 98.362695 192.234955 0.994657 6/20/2024 7:37:08 514.354669 491.092316 494.759799 192.236771 1.007527 6/20/2024 7:39:00 99.157548 192.191345 0.999116/20/2024 7:37:15 514.149447 491.505312 496.47761 192.191345 1.006913 6/20/2024 7:39:07 99.132605 192.198608 0.999173 6/20/2024 7:37:23 515.169052 492.222649 496.265783 192.278564 1.007005 6/20/2024 7:39:15 98.597693 192.147736 0.9995696/20/2024 7:37:30 515.114046 491.554069 499.900208 192.278564 1.007051 6/20/2024 7:39:22 97.676654 192.133209 1.0010386/20/2024 7:37:37 515.36675 492.57509 498.095619 192.293091 1.006408 6/20/2024 7:39:30 99.06369 192.147736 1.0008086/20/2024 7:37:45 515.901464 491.236807 495.700961 192.307632 1.007694 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Ethylene 191C TE Temp ( C )Pressure (atm)6/20/2024 7:39:53 0.331911 0.12744 0.168967 0.746181 191.944244 1.0102586/20/2024 7:40:00 0.057252 -0.228419 -1.009888 -0.07605 191.987854 1.0059956/20/2024 7:40:08 0.083461 0.222458 0.110697 0.197319 191.973312 1.008526/20/2024 7:40:15 0.101047 0.031695 0.124941 0.851211 191.915161 1.0044356/20/2024 7:40:22 0.249417 0.035213 -0.263529 0.00279 191.886093 1.004526 6/20/2024 7:40:30 0.029099 0.040005 -0.52586 0.01417 191.857025 1.0031036/20/2024 7:40:38 0.390347 -0.049911 -0.025152 0.090415 191.880646 1.006764 6/20/2024 7:40:45 0.079181 -0.092888 -0.332606 0.469555 191.857025 1.00829 Raw Calibration Data BACKGROUND / PRE DIRECT ZERO PRE DIRECT CAL NO2 CAL PRE SYSTEM CAL PRE SYSTEM ZERO Date Time CO2% 191C Propane 191C span Temp ( C )Pressure (atm) 6/20/2024 7:44:01 6.252792 44.153878 191.791611 0.9661186/20/2024 7:44:09 6.25785 44.612414 191.75528 0.9669326/20/2024 7:44:16 6.249709 43.98512 191.784348 0.9679426/20/2024 7:44:24 6.21775 45.023125 191.798889 0.9704216/20/2024 7:44:31 6.240977 44.509635 191.769806 0.9649136/20/2024 7:45:16 6.202251 44.213381 191.796234 0.9658996/20/2024 7:45:24 6.179 42.983605 191.813416 0.969687 6/20/2024 7:45:31 4.92539 36.425219 191.813416 0.9740476/20/2024 7:45:39 3.79955 57.718379 191.857025 0.9765266/20/2024 7:45:46 3.713678 207.257903 191.842484 0.9762966/20/2024 7:45:54 3.709946 212.573931 191.842484 0.9755166/20/2024 7:46:02 3.728419 213.164983 191.813416 0.9734966/20/2024 7:46:09 4.035289 190.747121 191.7789 0.9751956/20/2024 7:46:16 5.373761 101.575858 191.71167 0.973634 6/20/2024 7:46:24 5.414054 97.57746 191.726212 0.9740476/20/2024 7:46:31 5.399467 95.793397 191.726212 0.983641 6/20/2024 7:46:39 5.415937 95.673926 191.75528 0.9885526/20/2024 7:46:47 5.711992 75.548199 191.677139 0.9882486/20/2024 7:46:54 5.965474 60.560226 191.757706 0.9843526/20/2024 7:47:01 5.950054 58.917861 191.740738 0.9876866/20/2024 7:47:09 5.947482 58.383059 191.75528 0.9874516/20/2024 7:47:17 5.964765 57.038242 191.784348 0.9881856/20/2024 7:47:24 5.911404 57.937095 191.784348 1.000579 6/20/2024 7:47:31 5.791874 69.456501 191.813416 0.9945666/20/2024 7:47:39 5.231528 106.638198 191.766174 0.9953986/20/2024 7:47:47 5.123433 112.299112 191.827957 1.0042516/20/2024 7:47:54 5.125188 114.558478 191.871567 1.0003956/20/2024 7:48:02 5.237525 103.764217 191.842484 1.0027366/20/2024 7:48:09 5.432898 90.735432 191.86792 1.0016636/20/2024 7:48:17 5.582844 84.158469 191.842484 0.994795 6/20/2024 7:48:24 5.755024 69.933461 191.871567 0.9975956/20/2024 7:48:32 5.809762 66.08089 191.86792 0.997486 6/20/2024 7:48:39 5.844296 65.298768 191.857025 0.9928216/20/2024 7:48:47 5.743584 69.676107 191.900635 1.0001666/20/2024 7:48:54 5.674544 72.73179 191.915161 0.9986516/20/2024 7:49:47 5.467754 87.211851 191.955765 0.998287 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm)6/20/2024 10:57:34 516.540112 491.38643 491.392783 192.054474 1.004809 6/20/2024 10:55:53 98.693652 192.113831 0.9964286/20/2024 10:57:41 516.205471 492.058059 491.247015 192.075058 1.004343 6/20/2024 10:56:00 98.165953 192.162277 0.994526/20/2024 10:57:49 518.281675 493.472078 494.949544 192.04599 1.002782 6/20/2024 10:56:08 99.285995 192.162277 0.9938316/20/2024 10:57:57 518.191649 493.638121 495.547499 192.060532 1.00292 6/20/2024 10:56:15 99.255789 192.104126 0.9941986/20/2024 10:58:04 514.216292 489.724426 488.187477 192.016922 1.011412 6/20/2024 10:56:23 98.795949 192.0896 0.994244 6/20/2024 10:58:12 518.577649 492.944762 490.576358 192.020554 1.006041 6/20/2024 10:56:30 98.240392 192.075058 0.9974576/20/2024 10:58:19 516.719651 492.709873 491.81018 192.00238 1.00673 6/20/2024 10:56:38 99.046232 192.033264 0.995036 6/20/2024 10:58:27 516.233733 492.389499 493.339052 191.973312 1.00751 6/20/2024 10:56:45 99.10651 192.060532 0.9939236/20/2024 10:58:34 519.434861 494.143862 492.388193 191.987854 1.003838 6/20/2024 10:56:53 98.008892 192.016922 0.9918576/20/2024 10:58:42 517.874098 493.544495 494.846447 191.900635 1.004985 6/20/2024 10:57:00 98.256721 192.031448 0.995897 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm)6/20/2024 10:56:08 -0.093842 -0.02652 -1.171856 192.162277 0.993831 6/20/2024 10:59:31 0.278125 191.827957 0.989241 6/20/2024 10:56:15 -0.495442 0.102534 -1.688019 192.104126 0.994198 6/20/2024 10:59:39 -0.006065 191.857025 0.9880936/20/2024 10:56:23 -0.391981 0.194067 -1.523244 192.0896 0.994244 6/20/2024 10:59:46 -0.447854 191.857025 0.9931436/20/2024 10:56:30 -0.46729 -0.153347 -1.007033 192.075058 0.997457 6/20/2024 10:59:53 -0.71073 191.842484 0.9867626/20/2024 10:56:38 -0.313392 0.408647 -1.970402 192.033264 0.995036 6/20/2024 11:00:01 0.283148 191.842484 0.9881286/20/2024 10:56:45 -0.23457 0.026576 -1.639213 192.060532 0.993923 6/20/2024 11:00:08 0.425952 191.842484 0.9851566/20/2024 10:56:53 -0.240628 0.034283 -1.07197 192.016922 0.991857 6/20/2024 11:00:16 0.732398 191.827957 0.9839626/20/2024 10:57:00 -0.12448 0.03501 -1.64256 192.031448 0.995897 6/20/2024 11:00:23 0.339787 191.886093 0.985798 SAMPLE SPIKE RECOVERY POST SYSTEM CAL POST SYSTEM ZERO PRE TEST 1 495.6 6.2 44.2 5.6 80.7 0.094 70.9% Sensor Analyzer Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Error (%)Error (%) NOx 491.2 493.4 0.0 -0.45 -0.01 CO 513.7 520.2 0.0 -1.25 0.01 Propane 497.9 495.6 -0.7 0.46 -0.14 Ethylene 98.1 101.9 0.2 -3.76 0.15 Sensor System Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%) NOx 491.2 493.4 0.0 -0.44 0.01 CO 515.9 520.2 0.2 -0.83 0.03 Propane 495.7 495.6 -0.2 0.02 -0.04 Ethylene*99.1 101.9 0.3 -2.78 0.26 Sensor System Cal Zero Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%)Drift Error (%)Drift Error (%) NOx 493.5 493.4 0.1 0.03 0.02 0.47 0.01 CO 517.9 520.2 -0.3 -0.45 -0.06 0.38 0.10 Propane 494.8 495.6 -1.4 -0.15 -0.29 0.17 0.25 Ethylene*98.3 101.9 -0.1 -3.58 -0.12 0.79 0.37 *CTS Scans are conducted with Ethylene through the sample line. Lf 5.11 Lr Cr Tr Pr Lr/Lf 5.34 98.1 192.2 1.0 1.05 Ls Cs Ts Ps Ls/Lf 5.28 99.1 192.1 1.0 1.03 % Recovery Propane PRE DIRECT CAL FTIR QA/QC SUMMARY SAMPLE RECOVERY CALCULATIONS Period Spike #Concentration of Propane Cylinder Stack CO2 Concentration Pathlength Stack Propane Concentration Stack + Spike CO2 Concentration Stack + Propane Concentration DF Calculated POST SYSTEM CAL PRE SYSTEM CAL CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number:E02NI99E15W0051 Reference Number:153-402577489-1 Cylinder Number:CC486070 Cylinder Volume:144.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG PGVP Number:B72022 Valve Outlet:660 Gas Code:NO2,BALN Certification Date:Nov 08, 2022 Expiration Date:Nov 08, 2025 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates NITROGEN DIOXIDE 150.0 PPM 146.6 PPM G1 +/- 2.0% NIST Traceable 11/01/2022, 11/08/2022 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 15340120215 CC511005 59.52 PPM NITROGEN DIOXIDE/NITROGEN 1.4%Dec 17, 2024 PRM 12397 D887665 74.2 PPM NITROGEN DIOXIDE/AIR 1.3%Feb 02, 2022 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration MKS FTIR NO2 018143349 FTIR Nov 01, 2022 Triad Data Available Upon Request PERMANENT NOTES:OXYGEN ADDED TO MAINTAIN STABILITY Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD Part Number:X02NI99P15AD524 Reference Number:153-402622613-1 Cylinder Number:CC173895 Cylinder Volume:140.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG Analysis Date:Dec 22, 2022 Valve Outlet:350 Lot Number:153-402622613-1 Expiration Date:Dec 22, 2025 Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. ANALYTICAL RESULTS Component Req Conc Actual Concentration Analytical (Mole %)Uncertainty ETHYLENE 100.0 PPM 101.9 PPM +/- 1% NITROGEN Balance Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 Finley – North Randlett 6-20-2024 Finley – North Randlett 6-20-2024 Finley – North Randlett 6-20-2024 Spectral Fit Run 1 Spectral Fit Run 2 Spectral Fit Run 3 Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000162.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000068.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000069.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000070.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000071.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000072.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000073.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000074.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 59.99 3.92 -0.24 0.33 5.34 5.34 -2.26 --0-2795 1.05 Good NO2 191C 21.97 0.38 -0.03 0.03 0.4 0.4 -0.44 --0-488 1.06 Good N2O 191C 0 0.37 0.11 0.03 0.03 0.42 0.42 0.14 0.34 0.02 0.04 0-200 -Close to DL NH3 TE 191C 10.83 44.6 9.19 4.14 7.06 76.11 76.11 10.34 40.36 1.15 3.06 0-2995 -Close to DL H2O% (HIGH) 191C10.84 0.28 -0.02 0.03 0.45 0.45 -0.22 --0-40 -Good FORMALDEHYDE 191C6.22 0.83 5.46 0.24 0.27 0.93 0.93 6.18 6.18 0.72 1.82 0-69 -Close to DL FORMIC ACID 191C TE2.69 12.45 3.01 1.56 1.83 14.57 14.57 3.31 10.87 0.3 1 0-466 -Close to DL CH4 2900 CM-1 191C807.55 27.6 -1.69 2.46 51.14 51.14 -16.25 --0-3143 1 Good PROPANE 191C44.42 1.5 -0.22 0.27 1.81 1.81 -0.89 --0-4976 0.95 Good PROPYLENE 191C TE2.22 12.61 3.72 1.57 1.86 14.91 14.91 3.93 11 0.21 1.24 0-194 -Close to DL ETHANE 191C 85.8 3.45 -0.55 0.85 5.38 5.38 -1.75 --0-1004 -Good ETHYLENE 191C TE18.02 22.5 16.19 2.07 2.55 27.09 27.09 18.32 19.96 2.13 5.4 0-900 -Close to DL CO PPM 191C (1OF2)30.36 1.41 -0.26 0.57 3 3 -0.66 --0-5010 1.05 Good CO2% 191C 6.05 0.17 -0.01 0.02 0.24 0.24 -0.12 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.47 2.13 1.12 0.64 0.82 2.73 2.73 1.21 1.49 0.09 0.37 0-186 1 Close to DL ACETYLENE 191C0.23 4.9 0.52 0.79 1.05 6.47 6.47 0.54 4.14 0.02 0.17 0-1016 -Close to DL SO2 191C 1.91 2.18 1.66 0.26 0.32 2.66 2.66 2 2 0.35 0.55 0-964 1.02 Close to DL HEXANE 191C 3.83 1.15 4.12 0.13 0.18 1.56 1.56 4.57 4.57 0.45 1.37 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000223.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000068.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000069.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000070.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000071.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000072.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000073.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000074.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 61.23 4 -0.24 0.33 5.44 5.44 -2.3 --0-2795 1.05 Good NO2 191C 21.41 0.38 -0.03 0.03 0.4 0.4 -0.43 --0-488 1.06 Good N2O 191C 0.01 0.37 0.11 0.03 0.03 0.42 0.42 0.14 0.35 0.02 0.04 0-200 -Close to DL NH3 TE 191C 12.26 43.34 9.19 4.14 7.06 73.96 73.96 10.34 39.06 1.15 3.06 0-2995 -Close to DL H2O% (HIGH) 191C10.69 0.28 -0.02 0.03 0.44 0.44 -0.21 --0-40 -Good FORMALDEHYDE 191C6.51 0.89 5.46 0.24 0.27 1.01 1.01 6.18 6.18 0.72 1.82 0-69 -Close to DL FORMIC ACID 191C TE2.52 12.86 3.01 1.56 1.83 15.05 15.05 3.31 11.28 0.3 1 0-466 -Close to DL CH4 2900 CM-1 191C810.02 27.13 -1.69 2.46 50.26 50.26 -16.25 --0-3143 1 Good PROPANE 191C43.91 1.54 -0.22 0.27 1.85 1.85 -0.88 --0-4976 0.95 Good PROPYLENE 191C TE0.98 13.16 3.72 1.57 1.86 15.57 15.57 3.93 11.59 0.21 1.24 0-194 -Close to DL ETHANE 191C 84.66 3.61 -0.55 0.85 5.62 5.62 -1.78 --0-1004 -Good ETHYLENE 191C TE17.37 23.01 16.19 2.07 2.55 27.7 27.7 18.32 20.48 2.13 5.4 0-900 -Close to DL CO PPM 191C (1OF2)30.17 1.4 -0.26 0.57 2.99 2.99 -0.65 --0-5010 1.05 Good CO2% 191C 6.03 0.17 -0.01 0.02 0.23 0.23 -0.12 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.51 2.22 1.12 0.64 0.82 2.85 2.85 1.21 1.58 0.09 0.37 0-186 1 Close to DL ACETYLENE 191C-0.01 5.03 0.52 0.79 1.05 6.64 6.64 0.54 4.28 0.02 0.17 0-1016 -Close to DL SO2 191C 1.9 2.01 1.66 0.26 0.32 2.45 2.45 2 2 0.35 0.55 0-964 1.02 Close to DL HEXANE 191C 4.07 1.2 4.12 0.13 0.18 1.62 1.62 4.57 4.57 0.45 1.37 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000284.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000068.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000069.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000070.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000071.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000072.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000073.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000074.LAB C:\OLT\Data\Finley Resources\Finley NR CS E3 6-20-24\FINLEY NR CS E3 6-20-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 61.47 3.65 -0.24 0.33 4.97 4.97 -2.01 --0-2795 1.05 Good NO2 191C 21.46 0.37 -0.03 0.03 0.39 0.39 -0.43 --0-488 1.06 Good N2O 191C 0.02 0.36 0.11 0.03 0.03 0.42 0.42 0.14 0.34 0.02 0.04 0-200 -Close to DL NH3 TE 191C 9.21 39.12 9.19 4.14 7.06 66.76 66.76 10.34 34.93 1.15 3.06 0-2995 -Close to DL H2O% (HIGH) 191C10.76 0.25 -0.02 0.03 0.41 0.41 -0.22 --0-40 -Good FORMALDEHYDE 191C6.55 0.88 5.46 0.24 0.27 0.99 0.99 6.18 6.18 0.72 1.82 0-69 -Close to DL FORMIC ACID 191C TE2.33 12.77 3.01 1.56 1.83 14.95 14.95 3.31 11.2 0.3 1 0-466 -Close to DL CH4 2900 CM-1 191C794.86 25.31 -1.69 2.46 46.89 46.89 -15.9 --0-3143 1 Good PROPANE 191C45.26 1.57 -0.22 0.27 1.88 1.88 -0.91 --0-4976 0.95 Good PROPYLENE 191C TE2.15 12.94 3.72 1.57 1.86 15.3 15.3 3.93 11.33 0.21 1.24 0-194 -Close to DL ETHANE 191C 84.05 3.57 -0.55 0.85 5.56 5.56 -1.76 --0-1004 -Good ETHYLENE 191C TE16.96 21.8 16.19 2.07 2.55 26.24 26.24 18.32 19.28 2.13 5.4 0-900 -Close to DL CO PPM 191C (1OF2)30.32 1.45 -0.26 0.57 3.09 3.09 -0.67 --0-5010 1.05 Good CO2% 191C 6.05 0.16 -0.01 0.02 0.22 0.22 -0.12 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.66 2.2 1.12 0.64 0.82 2.83 2.83 1.21 1.56 0.09 0.37 0-186 1 Close to DL ACETYLENE 191C-0.09 4.63 0.52 0.79 1.05 6.12 6.12 0.54 3.88 0.02 0.17 0-1016 -Close to DL SO2 191C 1.98 2.05 1.66 0.26 0.32 2.5 2.5 2 2 0.35 0.55 0-964 1.02 Close to DL HEXANE 191C 4.4 1.16 4.12 0.13 0.18 1.56 1.56 4.57 4.57 0.45 1.37 0-1000 -Close to DL APPENDIX C Test Run Load %Site Rated Load, bhp Load Approx., bhp 1 87 1379 1199.7 2 87 1379 1199.7 3 87 1379 1199.7 Engine Load Approximation based on Panel Levels APPENDIX D Test Run Flowrate dscfm Approx. BHP Avg O2 % NOx ppmvd NOx g/bhp-hr NOx lbs/hr CO ppmvd CO g/bhp-hr CO lbs/hr NMNEHC ppmvd NMNEHC g/bhp-hr NMNEHC lbs/hr Moisture Content % 1 1479.54 1199.7 5.5 90.92 0.36 0.96 33.98 0.08 0.22 71.75 0.28 0.73 11.00 2 1476.55 1199.7 5.9 91.36 0.37 0.97 33.86 0.08 0.22 71.44 0.27 0.72 10.70 3 1503.80 1199.7 5.9 94.43 0.38 1.02 34.39 0.09 0.23 72.79 0.28 0.75 10.80 1199.7 5.8 92.23 0.37 0.98 34.08 0.08 0.22 71.99 0.28 0.73 10.83 Summary Average Levels Example Calculations: Uinta Wax Operating, LLC, North Randlett Compressor Station, #5 The following is a step-by-step calculation for the first test run conducted on the North Randlett Compressor Station #5. Test Parameters • Stack Diameter = 13.5 inches • Traverse Points = 16 • Ports = 2 • Barometric Pressure = 25.17 in Hg • Average O2 = 5.5% • Average CO2 = 6.7% • Load Approximation = 1199.7 bhp • Moisture Content = 11.00% EPA 40 CFR 60(A) Methods 1-3: Determination of Stack Gas Velocity and Flow Rate Dry Molecular Weight (lb/lbmol) = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) Where: %CO2 – Carbon Dioxide Content Of The Gas = 6.7% %O2 – Oxygen Content Of The Gas = 5.5% %N2 – Nitrogen Content Of The Gas %CO – Carbon Monoxide Content Of The Gas (%N2 +%CO) = (100 - %O2 - %CO2) = (100 – 5.5 – 6.7) = 87.8% Dry = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) = (0.44 * 6.7) + (0.32 * 5.5) + (0.28 * 87.8) = 29.29 lb/lbmol Wet Molecular Weight (lb/lbmol) = MD * (1-BWS) + (18) * BWS Where: MD – Molecular Weight Of The Dry Gas (lb/lbmol) = 29.29 lb/lbmol BWS – Moisture Content Of The Gas (%/100) = 11.00% = MD * (1-BWS) + (18) * BWS = 29.29 * (1 – (11.00/ 100)) + (18 * (11.00/ 100)) = 28.05 lb/lbmol Average Stack Gas Velocity (ft/sec) = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) Where: CP – Pitot tube constant (unitless) = 0.84 ∆PAVG – Average square root of the stack gas pitot DP (inches water) = 0.814 in H2O TS – Average stack temperature (R) = 1231 R PB – Barometric pressure (in Hg) = 25.17 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O MA – Molecular weight of the wet gas (lb/lbmol) = 28.05 lb/lbmol = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) = 0.84 * (85.49) * 0.814 * ( 1231 / (((0.3/ 13.6) + 25.17) * 28.05)) = 77.19 ft/sec Average Dry Flowrate (dscfm) = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 Where: DS – Diameter of the stack (inches) = 13.5 inches BWS – Moisture content of the gas (%) = 11.00% TSTD – Standard temperature (528R) TS – Average stack temperature (R) = 1231 R PB – Barometric pressure (in Hg) = 25.17 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O VS– Average Stack gas velocity (ft/sec) = 77.19 ft/sec = 60 * (1-BWS) * VS * * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 = 60 * (1 - (11.00/ 100)) * 77.19 * * (((13.5 / 2) / 12))2) * 528 / 1231 * (25.17 + (0.3 / 13.6)) / 29.92 = 1479.54 dscfm Conversion of Dry Flowrate to m3/hr = Q * 60 * 2.83168*10 -2 Where: Q – Volumetric Flowrate = 1479.54 dscfm 2.83168*10 -2 – Conversion factor for cubic feet to cubic meter 60 – Minutes in an hour = Q * 60 * 2.83168*10 -2 = 1479.54 *60 * 2.83168*10 -2 = 2513.74 m3/hr ASTM D 6348-03: Determination of NOx, CO and VOC Emissions From Stationary Sources NOx Emission Rate (g/Bhp-hr) = (Cd * 1.912*10 -3 * Q * T) / HP-hr Where: Cd – Measured NOx concentration in ppm = 90.92 ppm 1.92*10 -3 - Conversion constant for ppm to g/m3 NOx Q – Volumetric Flowrate = 2513.74 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 1199.7 Bhp = (Cd * 1.912*10 -3 * Q * T) / HP-hr = (90.92 * 1.912*10 -3 * 2513.74 * 1) / 1199.7 = 0.36 g/Bhp-hr NOx Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.36 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 1199.7 Bhp = g/Bhp-hr / 454 * Bhp = 0.36 / 454 * 1199.7 = 0.96 lbs/hr CO Emission Rate (g/Bhp-hr) = (Cd * 1.164*10 -3 * Q * T) / HP-hr Where: Cd – Measured CO concentration in ppm = 33.98 ppm 1.164*10 -3 - Conversion constant for ppm to g/m3 CO Q – Volumetric Flowrate = 2513.74 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 1199.7 Bhp = (Cd * 1.164*10 -3 * Q * T) / HP-hr = (33.98 * 1.164*10 -3 * 2513.74 * 1) / 1199.7 = 0.08 g/Bhp-hr CO Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.08 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 1199.7 Bhp = g/Bhp-hr / 454 * Bhp = 0.08 / 454 * 1199.7 = 0.22 lbs/hr VOC Emission Rate (g/Bhp-hr) = (Cd * 1.833*10 -3 * Q * T) / HP-hr Where: Cd – Measured VOC concentration in ppm = 71.75 ppm 1.833*10 -3 - Conversion constant for ppm to g/m3 VOC Q – Volumetric Flowrate = 2513.74 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 1199.7 Bhp = (Cd * 1.833*10 -3 * Q * T) / HP-hr = (71.75 * 1.833*10 -3 * 2513.74 * 1) / 1199.7 = 0.28 g/Bhp-hr VOC Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.28 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 1199.7 Bhp = g/Bhp-hr / 454 * Bhp = 0.28 / 454 * 1199.7 = 0.73 lbs/hr APPENDIX E FTIR Engine Test Sheet Company Name f-~l\ k.f Location / Unit 1.0. NtJr>r~ ~{M\ 1\\,.,++ LS t:\..\ (~) 3x1hr /lIfrV David Martinez Type of Test Completed Field Technician (s) Client Rep and/or State Rep 'I viI''' II/-."Ic... Date I h~ "d..O-'?J.t.l LA,. ~Slb Stack Diagram 499.4 520.2 493.4 495.6 146.6 101.9 196.7 Concentration A/{,\Jl/l :St;~b\llfO \~ " Cvlinder# CC453965 CC453965 CC486070 CC453965 CC321163 CC453965 CC173895 Non-Resettable Run Time Hours Engine Model Enaine Make Port Distance 8 Enaine SIN Port Distance A Propane (ppm CO (ppm Methane (ppm Calibration Gas N02 (ppm) Exhaust Diameter (inches) Ethvlene (ppm Acetaldehvde (ppm) NO (ppm Test 1 Test 2 Test 3 Time of Reading 7!..5 I 8' .-S cl. q:S.3 Atm Pressure (in Hg) ":lS,\, ~S·\I -a.S.\l Atm Temp CF) 5, .5'( ~3 Engine RPM ~\ H,\q \)"O~ r~Of)l *Manifold Pres. Vae(") or 600st(psiVor Boost (psia) 3'"1 ~5 ~b Manifold TemD ('F) It1 r> J'10 \'1l Psuction (psi) Stage 1 tb \ -, ,... Tsuction 'F) Stage 1 ---.... r----.. - Pdischan e (psi) Staae 1 Cfl en to Psuction psi) Stage 2 \ ~ 1 Tsuction OF) Stage 2 I \ f Pdischan e (psi) Staae 2 ~6a. 0\. ]01 d-.'lO Psuction psi) Stage 3 \ , Tsuction OF) Staae 3 \ I Pdischar< e (psi) Staae 3 !i~l ~bO \0\ 1 Psuction psi) Stage 4 \ ~ Tsuction OF) Staae 4 L Pdischarae (psi) Stage 4 I I Gas Throuahput (mmef/dl or ( V'Y1 Fi= l \..\~J hr 331 ~!:J .~ ~t\~ Pre Cat Temp CF) f(!).S, 10/ 706 Post Cat Temp CF) ,-> \ 1'6~ '7 '¥I Cat Differential Pres. (" of H2O) .s. L.j S,"l S.'i Humidity% ~~ '~-5 ';)..3 02% 5. b 5."'1 s,q C02 % Dry hJ' J 6./ &,., LOAD % (Panel).-br (Estimated) fs'"7 fJ7 k~ Ignition Timing CF) )..""/, I ~'f., '0.,£-1. I AFR Settina mV ~,~L=SaHk\ ~7,£.{ Af'''{ ,,)"7.IiP! AFR Settina mV -. --'I<:) -r---....~.. -, Rev 8 • Some units show boost in inches of Hg. In this situation please indicate if it is positive (+) or negative(-). Eg: (+12'~ or (-5'~ 9/17/2019 Worksheet: O2 Stratification Client:Finley Location:North Randlett CS E4 (E3) Date:6/20/2024 PD:13.5 DD:36 YES Method 1 Criteria Met UD:19 YES Method 1 Criteria Met Port Point Insertion Depth Reading (inches)(%) A 1 2.24 5.50 A 2 6.75 5.90 A 3 11.25 5.90 A 4 A 5 A 6 A 7 A 8 A 9 A 10 A 11 A 12 Average 5.77 Notes: To demonstrate non-stratified flow and utilize one sampling location O2 may not deviate by more than +/- 0.3% of the average O2 concentration. EPA REFERENCE METHOD 3A (Determination Of Stratification) COMPANY NAME:Finley COMPANY LOCATION:North Randlett CS E4 (E3)DATE:6/20/2024 STACK DIAMETER (inches):13.5 TRAVERSE POINTS:16 2 TEST RUN #1 TEST RUN #2 TEST RUN #3 AVERAGE O2:5.5 AVERAGE O2:5.9 AVERAGE O2:5.9 AVERAGE CO2:6.7 AVERAGE CO2:6.7 AVERAGE CO2:6.7 BARO PRESSURE:25.17 BARO PRESSURE:25.17 BARO PRESSURE:25.17 Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O) 1 0.5 0.59 771 0.26 1 0.5 0.6 783 0.25 1 0.5 0.65 781 0.27 2 1.4175 0.62 2 1.4175 0.64 2 1.4175 0.67 3 2.619 0.66 3 2.619 0.68 3 2.619 0.72 4 4.3605 0.71 4 4.3605 0.72 4 4.3605 0.76 5 9.1395 0.74 5 9.1395 0.75 5 9.1395 0.79 6 10.881 0.7 6 10.881 0.69 6 10.881 0.68 7 12.0825 0.67 7 12.0825 0.69 7 12.0825 0.64 8 13 0.63 8 13 0.65 8 13 0.6 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 1 0.5 0.61 771 0.26 1 0.5 0.58 783 0.25 1 0.5 0.63 781 0.27 2 1.4175 0.64 2 1.4175 0.61 2 1.4175 0.66 3 2.619 0.67 3 2.619 0.65 3 2.619 0.7 4 4.3605 0.7 4 4.3605 0.69 4 4.3605 0.72 5 9.1395 0.69 5 9.1395 0.7 5 9.1395 0.75 6 10.881 0.71 6 10.881 0.68 6 10.881 0.71 7 12.0825 0.66 7 12.0825 0.66 7 12.0825 0.67 8 13 0.62 8 13 0.64 8 13 0.68 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16