DSHW-2023-204946 - 0901a06881216d40

Deq submit <[e-mail]>
Recycled Earth Results - Maintenance Building and Borehole Soil Samples
1 message
Rasmuson, Anna <[e-mail]>Mon, Jun 5, 2023 at 8:29 AM
To: "Wadman, Heather" <[e-mail]>, "[e-mail]" <[e-mail]>, "[e-mail]"
<[e-mail]>
Cc: "Wilson, DavidWilson" <[e-mail]>, "Cahoon, Tyler R." <[e-mail]>, "Cahoon, Brad R."
<[e-mail]>, David Rawson <[e-mail]>
Hello,
Attached are the detection summary tables for the maintenance building confirmation samples and subsurface borehole soil samples
collected from Recycled Earth on May 4 and 8, respectively. I have also included two maps showing the sample locations.
All detections were below the Industrial RSLs except for arsenic, which was below the established background concentration of 15
mg/kg for all samples.
Please let us know if you have any questions regarding these data.
Thanks,
Anna
Anna Rasmuson, Ph.D., P.G. | Geological Engineer
Pronouns: she, her, hers
Mobile + | [e-mail]
Tetra Tech | Leading with Science® | ECA
4750 W. 2100 S., Suite. 400. | Salt Lake City, UT 84120 | tetratech.com
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6 attachments
DSHW-2023-204946
Table 4 Maintenance Building Confirmatin Sample Results.pdf
119K
Table 5 Borehole Soil Results.pdf
121K
Maintenance Excavation Footprint and Sample Locations.pdf
1816K
GW Monitoring Well Locations.pdf
2046K
L1613187.pdf
5206K
L1614172.pdf
5073K
S1500W
U n i o n P a c ifi c
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U T A
Maxar, Microsoft, Esri Community Maps Contributors, Ogden City, Utah Geospatial
Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure X: Map Excavation Footprint and Excavation
Confirmation Sample Locations
Recycled Earth LLC
Date 05/22/2023
¯
0 0.01 0.02 0.03 0.040.01
Miles
Maxar, Microsoft, Esri Community Maps
Contributors, Ogden City, Utah
Geospatial Resource Center, ©
OpenStreetMap, Microsoft, Esri, HERE,
Garmin, SafeGraph, GeoTechnologies,
Inc, METI/NASA, USGS, Bureau of Land
Management, EPA, NPS, US Census
Bureau, USDA
CS-2
CS-4
CS-3
CS-1
CS-5
¯¯
Legend
ExcavationFootprint
Excavation Confirmation
Sample Location
0 2.5 5 7.5 101.25
Feet
Table 4: Maintenance Building Confirmation Sample Detections
CS‐1CS‐2CS‐3CS‐4CS‐5
Arsenic 3 3.2 3.4 5.4 10 6.3
Beryllium 2,300 0.33 0.27 0.38 0.31 0.40
Chromium 8.5 15 9.6 7.6 10
Copper 47000 8.0 14 9.5 16 8.5
Lead 800 3.3 4.1 4.1 26 5.4
Nickel 6.2 7.8 6.9 5.6 7.3
Zinc 25 23 29 44 31
Gasoline Range Organics 2,200 <4 <3.96 <4.78 <4.22 <4.13
Diesel Range Organics 440 <5.18 16 <5.73 <5.31 9.0
Oil Range Organics 30,000 <5.18 42 <5.73 14 26
TPH <14 58 <16 14 35
Acetone 1,100,000 <0.0799 <0.0793 <0.0957 0.089 <0.0826
Tetrachloroethene 100 <0.004 0.0088 <0.00478 <0.00422 0.0077
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
EPA = Environmental Protection Agency
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
mg/kg = milligram per kilogram
Bold values indicate exceedance of State and/or federal screening levels
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds 
EPA Industrial 
Screening Level 
(mg/kg)
Sample Results (mg/kg)
Metals
Analyte Group Analyte
Table 5: Subsurface Investigation Soil Sample Detections
MW‐1MW‐2MW‐3MW‐4MW‐5MW‐6
Arsenic 3 4.9 8.5 13 6.3 6.0 4.6
Beryllium 2,300 0.29 0.44 0.41 0.41 0.31 0.35
Chromium 7.7 13 10 11 8.0 14
Copper 47000 7.4 16 12 17 5.6 14
Lead 800 3.9 16 8.2 12 3.7 15
Nickel 5.9 9.9 7.7 7.4 5.2 7.3
Zinc 350 23 40 35 39 21 49
Gasoline Range Organics 2,200 <3.7 <3.94 <3.84 <4.04 <3.94 <3.64
Diesel Range Organics 440 <6.03 <5.11 <4.93 <5.17 <4.69 <467
Oil Range Organics 30,000 6.2 8.5 <4.93 5.9 <4.69 732
TPH 6.2 8.5 <13.7 5.9 <13.3 732
1,2,3‐Trimethylbenzene 340 <0.0074 <0.00788 <0.00768 <0.00808 <0.00789 0.042
1,3,5‐Trimethylbenzene 270 <0.0074 <0.00788 <0.00768 <0.00808 <0.00789 0.066
Acetone 1,100,000 <0.074 <0.0788 0.079 <0.0808 0.0801 <0.0727
Ethylbenzene 25 <0.0037 0.020 <0.00384 <0.00404 <0.00394 <0.00364
Tetrachloroethene 100 <0.0037 <0.00394 <0.00384 <0.00404 <0.00394 0.79
Trichloroethene 6 <0.00148 <0.00158 <0.00154 <0.00162 <0.00158 0.0097
Xylenes, Total 2,500 <0.00962 0.10 <0.00999 <0.0105 <0.0103 0.015
Anthracene 230,000 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.083
Benzo(a)anthracene 21 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.13
Benzo(a)pyrene 2.1 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.12
Benzo(b)fluoranthene 21 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.12
Benzo(g,h,i)perylene <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.12
Chrysene 2,100 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.17
Fluoranthene 3,000 <0.00735 <0.00766 <0.00739 0.011 <0.00703 0.27
Indeno(1,2,3‐cd)pyrene 21 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.074
Phenanthrene <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.28
Pyrene 23,000 <0.00735 <0.00766 <0.00739 0.0078 <0.00703 0.33
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
EPA = Environmental Protection Agency
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
mg/kg = milligram per kilogram
Bold values indicate exceedance of State and/or federal screening levels
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds 
(VOCs)
Semi‐Volatile 
Organic 
Compounds 
(VOCs)
EPA Industrial 
Screening Level 
(mg/kg)
Sample Results (mg/kg)
Metals
Analyte Group Analyte
S150
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U nio n P a cific
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MW-6
MW-4
MW-1
MW-2
MW-3
MW-5
Maxar, Microsoft, Esri Community Maps Contributors, Ogden City, Utah Geospatial
Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 9: Map with Groundwater Monitoring Well
Locations
Recycled Earth LLC
Date 05/17/2023
Legend
¯
Groundwater Monitoring Wells
0 0.02 0.04 0.06 0.080.01
Miles
ANALYTICAL REPORT
May 19, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1613187
Samples Received:05/05/2023
Project Number:
Description:
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
May 19, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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May 22, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
MW-3 L1613187-01 6
MW-6 L1613187-02 10
MW-4 L1613187-03 14
MW-1 L1613187-04 18
MW-2 L1613187-05 22
MW-5 L1613187-06 26
Qc: Quality Control Summary 30
Total Solids by Method 2540 G-2011 30
Wet Chemistry by Method 7199 32
Mercury by Method 7471A 34
Metals (ICP) by Method 6010B 35
Volatile Organic Compounds (GC) by Method 8015D/GRO 37
Volatile Organic Compounds (GC/MS) by Method 8260B 38
Semi-Volatile Organic Compounds (GC) by Method 8015 42
Polychlorinated Biphenyls (GC) by Method 8082 43
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 44
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 49
Gl: Glossary of Terms 51
Al: Accreditations & Locations 52
Sc: Sample Chain of Custody 53
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-3 L1613187-01 Solid Richie T.05/04/23 10:00 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:02 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:26 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:20 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 26.5 05/04/23 10:00 05/11/23 12:28 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1.06 05/04/23 10:00 05/11/23 12:10 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 00:42 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 17:30 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 17:41 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:03 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1613187-02 Solid Richie T.05/04/23 10:45 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:08 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:28 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:23 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 27.5 05/04/23 10:45 05/11/23 12:46 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1.1 05/04/23 10:45 05/11/23 12:29 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 100 05/13/23 15:08 05/14/23 19:23 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 17:42 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 10 05/12/23 04:57 05/15/23 21:59 AMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 10 05/11/23 16:50 05/12/23 07:58 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4 L1613187-03 Solid Richie T.05/04/23 11:30 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:18 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:30 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:26 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 25 05/04/23 11:30 05/11/23 13:05 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1 05/04/23 11:30 05/11/23 12:48 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 01:38 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 17:55 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 18:31 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:20 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 L1613187-04 Solid Richie T.05/04/23 12:20 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:54 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:36 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:29 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 25 05/04/23 12:20 05/11/23 13:24 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1 05/04/23 12:20 05/11/23 13:07 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1.23 05/13/23 15:08 05/14/23 01:25 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 18:08 NWH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1613187-04 Solid Richie T.05/04/23 12:20 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 17:15 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:37 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1613187-05 Solid Richie T.05/04/23 13:15 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:59 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:38 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:32 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 25 05/04/23 13:15 05/11/23 13:42 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1 05/04/23 13:15 05/11/23 13:26 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 02:31 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 18:20 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 18:55 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:55 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1613187-06 Solid Richie T.05/04/23 14:10 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055863 1 05/08/23 15:11 05/08/23 15:17 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 02:05 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:40 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:35 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 30 05/04/23 14:10 05/11/23 14:01 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1.2 05/04/23 14:10 05/11/23 13:45 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 00:03 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 18:33 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 16:26 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 04:12 AMM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.2 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.23 1 05/11/2023 01:02 WG2056423
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0493 1 05/12/2023 12:26 WG2056112
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.46 1 05/10/2023 18:20 WG2055559
Arsenic 13.0 2.46 1 05/10/2023 18:20 WG2055559
Beryllium 0.409 0.246 1 05/10/2023 18:20 WG2055559
Cadmium ND 0.616 1 05/10/2023 18:20 WG2055559
Chromium 10.1 1.23 1 05/10/2023 18:20 WG2055559
Copper 11.8 2.46 1 05/10/2023 18:20 WG2055559
Lead 8.23 0.616 1 05/10/2023 18:20 WG2055559
Nickel 7.73 2.46 1 05/10/2023 18:20 WG2055559
Selenium ND 2.46 1 05/10/2023 18:20 WG2055559
Silver ND 1.23 1 05/10/2023 18:20 WG2055559
Thallium ND 2.46 1 05/10/2023 18:20 WG2055559
Zinc 34.8 6.16 1 05/10/2023 18:20 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.84 26.5 05/11/2023 12:28 WG2057784
(S) a,a,a-Trifluorotoluene(FID)94.0 77.0-120 05/11/2023 12:28 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0790 0.0768 1.06 05/11/2023 12:10 WG2058136
Acrylonitrile ND 0.0193 1.06 05/11/2023 12:10 WG2058136
Benzene ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Bromobenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
Bromodichloromethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Bromoform ND 0.0384 1.06 05/11/2023 12:10 WG2058136
Bromomethane ND 0.0193 1.06 05/11/2023 12:10 WG2058136
n-Butylbenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
sec-Butylbenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
tert-Butylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Carbon tetrachloride ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Chlorobenzene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Chlorodibromomethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Chloroethane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Chloroform ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Chloromethane ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
4-Chlorotoluene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0384 1.06 05/11/2023 12:10 WG2058136
1,2-Dibromoethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Dibromomethane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2-Dichlorobenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,3-Dichlorobenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,4-Dichlorobenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Dichlorodifluoromethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1-Dichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,2-Dichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1-Dichloroethene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
cis-1,2-Dichloroethene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
trans-1,2-Dichloroethene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2-Dichloropropane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,1-Dichloropropene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,3-Dichloropropane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
cis-1,3-Dichloropropene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
trans-1,3-Dichloropropene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
2,2-Dichloropropane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Di-isopropyl ether ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Ethylbenzene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Hexachloro-1,3-butadiene ND 0.0384 1.06 05/11/2023 12:10 WG2058136
Isopropylbenzene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
p-Isopropyltoluene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
2-Butanone (MEK)ND 0.154 1.06 05/11/2023 12:10 WG2058136
Methylene Chloride ND 0.0384 1.06 05/11/2023 12:10 WG2058136
4-Methyl-2-pentanone (MIBK)ND 0.0384 1.06 05/11/2023 12:10 WG2058136
Methyl tert-butyl ether ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Naphthalene ND J4 0.0193 1.06 05/11/2023 12:10 WG2058136
n-Propylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Styrene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Tetrachloroethene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Toluene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0193 1.06 05/11/2023 12:10 WG2058136
1,2,4-Trichlorobenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1,1,1-Trichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1,2-Trichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Trichloroethene ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Trichlorofluoromethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,2,3-Trichloropropane ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1,2,4-Trimethylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2,3-Trimethylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,3,5-Trimethylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Vinyl chloride ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Xylenes, Total ND 0.00999 1.06 05/11/2023 12:10 WG2058136
(S) Toluene-d8 106 75.0-131 05/11/2023 12:10 WG2058136
(S) 4-Bromofluorobenzene 93.4 67.0-138 05/11/2023 12:10 WG2058136
(S) 1,2-Dichloroethane-d4 113 70.0-130 05/11/2023 12:10 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.93 1 05/14/2023 00:42 WG2059338
C28-C40 Oil Range ND 4.93 1 05/14/2023 00:42 WG2059338
(S) o-Terphenyl 21.3 18.0-148 05/14/2023 00:42 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1221 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1232 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1242 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1248 ND 0.0209 1 05/13/2023 17:30 WG2057922
PCB 1254 ND 0.0209 1 05/13/2023 17:30 WG2057922
PCB 1260 ND 0.0209 1 05/13/2023 17:30 WG2057922
(S) Decachlorobiphenyl 63.8 10.0-135 05/13/2023 17:30 WG2057922
(S) Tetrachloro-m-xylene 76.4 10.0-139 05/13/2023 17:30 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Acenaphthylene ND 0.0410 1 05/12/2023 17:41 WG2058400
Anthracene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzidine ND 2.06 1 05/12/2023 17:41 WG2058400
Benzo(a)anthracene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(b)fluoranthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(k)fluoranthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(g,h,i)perylene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(a)pyrene ND 0.0410 1 05/12/2023 17:41 WG2058400
Bis(2-chlorethoxy)methane ND 0.410 1 05/12/2023 17:41 WG2058400
Bis(2-chloroethyl)ether ND 0.410 1 05/12/2023 17:41 WG2058400
2,2-Oxybis(1-Chloropropane)ND 0.410 1 05/12/2023 17:41 WG2058400
4-Bromophenyl-phenylether ND 0.410 1 05/12/2023 17:41 WG2058400
2-Chloronaphthalene ND 0.0410 1 05/12/2023 17:41 WG2058400
4-Chlorophenyl-phenylether ND 0.410 1 05/12/2023 17:41 WG2058400
Chrysene ND 0.0410 1 05/12/2023 17:41 WG2058400
Dibenz(a,h)anthracene ND 0.0410 1 05/12/2023 17:41 WG2058400
3,3-Dichlorobenzidine ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dinitrotoluene ND 0.410 1 05/12/2023 17:41 WG2058400
2,6-Dinitrotoluene ND 0.410 1 05/12/2023 17:41 WG2058400
Fluoranthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Fluorene ND 0.0410 1 05/12/2023 17:41 WG2058400
Hexachlorobenzene ND 0.410 1 05/12/2023 17:41 WG2058400
Hexachloro-1,3-butadiene ND 0.410 1 05/12/2023 17:41 WG2058400
Hexachlorocyclopentadiene ND 0.410 1 05/12/2023 17:41 WG2058400
Hexachloroethane ND 0.410 1 05/12/2023 17:41 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0410 1 05/12/2023 17:41 WG2058400
Isophorone ND 0.410 1 05/12/2023 17:41 WG2058400
Naphthalene ND 0.0410 1 05/12/2023 17:41 WG2058400
Nitrobenzene ND 0.410 1 05/12/2023 17:41 WG2058400
n-Nitrosodimethylamine ND 0.410 1 05/12/2023 17:41 WG2058400
n-Nitrosodiphenylamine ND 0.410 1 05/12/2023 17:41 WG2058400
n-Nitrosodi-n-propylamine ND 0.410 1 05/12/2023 17:41 WG2058400
Phenanthrene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzylbutyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Di-n-butyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Diethyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Dimethyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Di-n-octyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Pyrene ND 0.0410 1 05/12/2023 17:41 WG2058400
1,2,4-Trichlorobenzene ND 0.410 1 05/12/2023 17:41 WG2058400
4-Chloro-3-methylphenol ND 0.410 1 05/12/2023 17:41 WG2058400
2-Chlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dichlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dimethylphenol ND 0.410 1 05/12/2023 17:41 WG2058400
4,6-Dinitro-2-methylphenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dinitrophenol ND 0.410 1 05/12/2023 17:41 WG2058400
2-Nitrophenol ND 0.410 1 05/12/2023 17:41 WG2058400
4-Nitrophenol ND 0.410 1 05/12/2023 17:41 WG2058400
Pentachlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
Phenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4,6-Trichlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
(S) Nitrobenzene-d5 57.6 10.0-122 05/12/2023 17:41 WG2058400
(S) 2-Fluorobiphenyl 50.2 15.0-120 05/12/2023 17:41 WG2058400
(S) p-Terphenyl-d14 51.1 10.0-120 05/12/2023 17:41 WG2058400
(S) Phenol-d5 53.1 10.0-120 05/12/2023 17:41 WG2058400
(S) 2-Fluorophenol 54.5 12.0-120 05/12/2023 17:41 WG2058400
(S) 2,4,6-Tribromophenol 35.2 10.0-127 05/12/2023 17:41 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00739 1 05/12/2023 03:03 WG2058011
Acenaphthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Acenaphthylene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(a)anthracene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(a)pyrene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(b)fluoranthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(g,h,i)perylene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(k)fluoranthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Chrysene ND 0.00739 1 05/12/2023 03:03 WG2058011
Dibenz(a,h)anthracene ND 0.00739 1 05/12/2023 03:03 WG2058011
Fluoranthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Fluorene ND 0.00739 1 05/12/2023 03:03 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00739 1 05/12/2023 03:03 WG2058011
Naphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
Phenanthrene ND 0.00739 1 05/12/2023 03:03 WG2058011
Pyrene ND 0.00739 1 05/12/2023 03:03 WG2058011
1-Methylnaphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
2-Methylnaphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
2-Chloronaphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
(S) p-Terphenyl-d14 86.7 23.0-120 05/12/2023 03:03 WG2058011
(S) Nitrobenzene-d5 97.6 14.0-149 05/12/2023 03:03 WG2058011
(S) 2-Fluorobiphenyl 88.8 34.0-125 05/12/2023 03:03 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.6 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.17 1 05/11/2023 01:08 WG2056423
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0467 1 05/12/2023 12:28 WG2056112
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.34 1 05/10/2023 18:23 WG2055559
Arsenic 4.55 2.34 1 05/10/2023 18:23 WG2055559
Beryllium 0.353 0.234 1 05/10/2023 18:23 WG2055559
Cadmium ND 0.584 1 05/10/2023 18:23 WG2055559
Chromium 13.6 1.17 1 05/10/2023 18:23 WG2055559
Copper 14.1 2.34 1 05/10/2023 18:23 WG2055559
Lead 14.8 0.584 1 05/10/2023 18:23 WG2055559
Nickel 7.33 2.34 1 05/10/2023 18:23 WG2055559
Selenium ND 2.34 1 05/10/2023 18:23 WG2055559
Silver ND 1.17 1 05/10/2023 18:23 WG2055559
Thallium ND 2.34 1 05/10/2023 18:23 WG2055559
Zinc 48.7 5.84 1 05/10/2023 18:23 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.64 27.5 05/11/2023 12:46 WG2057784
(S) a,a,a-Trifluorotoluene(FID)89.8 77.0-120 05/11/2023 12:46 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0727 1.1 05/11/2023 12:29 WG2058136
Acrylonitrile ND 0.0182 1.1 05/11/2023 12:29 WG2058136
Benzene ND 0.00145 1.1 05/11/2023 12:29 WG2058136
Bromobenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
Bromodichloromethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Bromoform ND 0.0364 1.1 05/11/2023 12:29 WG2058136
Bromomethane ND 0.0182 1.1 05/11/2023 12:29 WG2058136
n-Butylbenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
sec-Butylbenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
tert-Butylbenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Carbon tetrachloride ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Chlorobenzene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Chlorodibromomethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Chloroethane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Chloroform ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Chloromethane ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
4-Chlorotoluene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0364 1.1 05/11/2023 12:29 WG2058136
1,2-Dibromoethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Dibromomethane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2-Dichlorobenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,3-Dichlorobenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,4-Dichlorobenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Dichlorodifluoromethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1-Dichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,2-Dichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1-Dichloroethene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
cis-1,2-Dichloroethene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
trans-1,2-Dichloroethene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2-Dichloropropane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,1-Dichloropropene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,3-Dichloropropane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
cis-1,3-Dichloropropene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
trans-1,3-Dichloropropene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
2,2-Dichloropropane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Di-isopropyl ether ND 0.00145 1.1 05/11/2023 12:29 WG2058136
Ethylbenzene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Hexachloro-1,3-butadiene ND 0.0364 1.1 05/11/2023 12:29 WG2058136
Isopropylbenzene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
p-Isopropyltoluene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
2-Butanone (MEK)ND 0.145 1.1 05/11/2023 12:29 WG2058136
Methylene Chloride ND 0.0364 1.1 05/11/2023 12:29 WG2058136
4-Methyl-2-pentanone (MIBK)ND 0.0364 1.1 05/11/2023 12:29 WG2058136
Methyl tert-butyl ether ND 0.00145 1.1 05/11/2023 12:29 WG2058136
Naphthalene ND J4 0.0182 1.1 05/11/2023 12:29 WG2058136
n-Propylbenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Styrene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Tetrachloroethene 0.787 0.00364 1.1 05/11/2023 12:29 WG2058136
Toluene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0182 1.1 05/11/2023 12:29 WG2058136
1,2,4-Trichlorobenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1,1,1-Trichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1,2-Trichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Trichloroethene 0.00974 0.00145 1.1 05/11/2023 12:29 WG2058136
Trichlorofluoromethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,2,3-Trichloropropane ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1,2,4-Trimethylbenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2,3-Trimethylbenzene 0.0416 0.00727 1.1 05/11/2023 12:29 WG2058136
1,3,5-Trimethylbenzene 0.0664 0.00727 1.1 05/11/2023 12:29 WG2058136
Vinyl chloride ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Xylenes, Total 0.0148 0.00945 1.1 05/11/2023 12:29 WG2058136
(S) Toluene-d8 105 75.0-131 05/11/2023 12:29 WG2058136
(S) 4-Bromofluorobenzene 96.8 67.0-138 05/11/2023 12:29 WG2058136
(S) 1,2-Dichloroethane-d4 116 70.0-130 05/11/2023 12:29 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 467 100 05/14/2023 19:23 WG2059338
C28-C40 Oil Range 732 467 100 05/14/2023 19:23 WG2059338
(S) o-Terphenyl 39.6 J7 18.0-148 05/14/2023 19:23 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1221 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1232 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1242 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1248 ND 0.0199 1 05/13/2023 17:42 WG2057922
PCB 1254 ND 0.0199 1 05/13/2023 17:42 WG2057922
PCB 1260 ND 0.0199 1 05/13/2023 17:42 WG2057922
(S) Decachlorobiphenyl 81.8 10.0-135 05/13/2023 17:42 WG2057922
(S) Tetrachloro-m-xylene 90.0 10.0-139 05/13/2023 17:42 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.389 10 05/15/2023 21:59 WG2058400
Acenaphthylene ND 0.389 10 05/15/2023 21:59 WG2058400
Anthracene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzidine ND 19.5 10 05/15/2023 21:59 WG2058400
Benzo(a)anthracene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(b)fluoranthene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(k)fluoranthene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(g,h,i)perylene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(a)pyrene ND 0.389 10 05/15/2023 21:59 WG2058400
Bis(2-chlorethoxy)methane ND 3.89 10 05/15/2023 21:59 WG2058400
Bis(2-chloroethyl)ether ND 3.89 10 05/15/2023 21:59 WG2058400
2,2-Oxybis(1-Chloropropane)ND 3.89 10 05/15/2023 21:59 WG2058400
4-Bromophenyl-phenylether ND 3.89 10 05/15/2023 21:59 WG2058400
2-Chloronaphthalene ND 0.389 10 05/15/2023 21:59 WG2058400
4-Chlorophenyl-phenylether ND 3.89 10 05/15/2023 21:59 WG2058400
Chrysene ND 0.389 10 05/15/2023 21:59 WG2058400
Dibenz(a,h)anthracene ND 0.389 10 05/15/2023 21:59 WG2058400
3,3-Dichlorobenzidine ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dinitrotoluene ND 3.89 10 05/15/2023 21:59 WG2058400
2,6-Dinitrotoluene ND 3.89 10 05/15/2023 21:59 WG2058400
Fluoranthene ND 0.389 10 05/15/2023 21:59 WG2058400
Fluorene ND 0.389 10 05/15/2023 21:59 WG2058400
Hexachlorobenzene ND 3.89 10 05/15/2023 21:59 WG2058400
Hexachloro-1,3-butadiene ND 3.89 10 05/15/2023 21:59 WG2058400
Hexachlorocyclopentadiene ND 3.89 10 05/15/2023 21:59 WG2058400
Hexachloroethane ND 3.89 10 05/15/2023 21:59 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.389 10 05/15/2023 21:59 WG2058400
Isophorone ND 3.89 10 05/15/2023 21:59 WG2058400
Naphthalene ND 0.389 10 05/15/2023 21:59 WG2058400
Nitrobenzene ND 3.89 10 05/15/2023 21:59 WG2058400
n-Nitrosodimethylamine ND 3.89 10 05/15/2023 21:59 WG2058400
n-Nitrosodiphenylamine ND 3.89 10 05/15/2023 21:59 WG2058400
n-Nitrosodi-n-propylamine ND 3.89 10 05/15/2023 21:59 WG2058400
Phenanthrene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzylbutyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Di-n-butyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Diethyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Dimethyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Di-n-octyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Pyrene ND 0.389 10 05/15/2023 21:59 WG2058400
1,2,4-Trichlorobenzene ND 3.89 10 05/15/2023 21:59 WG2058400
4-Chloro-3-methylphenol ND 3.89 10 05/15/2023 21:59 WG2058400
2-Chlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dichlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dimethylphenol ND 3.89 10 05/15/2023 21:59 WG2058400
4,6-Dinitro-2-methylphenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dinitrophenol ND 3.89 10 05/15/2023 21:59 WG2058400
2-Nitrophenol ND 3.89 10 05/15/2023 21:59 WG2058400
4-Nitrophenol ND 3.89 10 05/15/2023 21:59 WG2058400
Pentachlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
Phenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4,6-Trichlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
(S) Nitrobenzene-d5 78.9 10.0-122 05/15/2023 21:59 WG2058400
(S) 2-Fluorobiphenyl 62.9 15.0-120 05/15/2023 21:59 WG2058400
(S) p-Terphenyl-d14 61.6 10.0-120 05/15/2023 21:59 WG2058400
(S) Phenol-d5 61.9 10.0-120 05/15/2023 21:59 WG2058400
(S) 2-Fluorophenol 43.4 12.0-120 05/15/2023 21:59 WG2058400
(S) 2,4,6-Tribromophenol 35.8 10.0-127 05/15/2023 21:59 WG2058400
Sample Narrative:
L1613187-02 WG2058400: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.0827 0.0701 10 05/12/2023 07:58 WG2058011
Acenaphthene ND 0.0701 10 05/12/2023 07:58 WG2058011
Acenaphthylene ND 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(a)anthracene 0.132 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(a)pyrene 0.118 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(b)fluoranthene 0.117 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(g,h,i)perylene 0.117 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(k)fluoranthene ND 0.0701 10 05/12/2023 07:58 WG2058011
Chrysene 0.172 0.0701 10 05/12/2023 07:58 WG2058011
Dibenz(a,h)anthracene ND 0.0701 10 05/12/2023 07:58 WG2058011
Fluoranthene 0.268 0.0701 10 05/12/2023 07:58 WG2058011
Fluorene ND 0.0701 10 05/12/2023 07:58 WG2058011
Indeno(1,2,3-cd)pyrene 0.0742 0.0701 10 05/12/2023 07:58 WG2058011
Naphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
Phenanthrene 0.282 0.0701 10 05/12/2023 07:58 WG2058011
Pyrene 0.325 0.0701 10 05/12/2023 07:58 WG2058011
1-Methylnaphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
2-Methylnaphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
2-Chloronaphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
(S) p-Terphenyl-d14 91.0 23.0-120 05/12/2023 07:58 WG2058011
(S) Nitrobenzene-d5 90.1 14.0-149 05/12/2023 07:58 WG2058011
(S) 2-Fluorobiphenyl 77.1 34.0-125 05/12/2023 07:58 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.4 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND J3 J6 1.29 1 05/11/2023 01:18 WG2056423
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0517 1 05/12/2023 12:30 WG2056112
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.59 1 05/10/2023 18:26 WG2055559
Arsenic 6.29 2.59 1 05/10/2023 18:26 WG2055559
Beryllium 0.406 0.259 1 05/10/2023 18:26 WG2055559
Cadmium ND 0.646 1 05/10/2023 18:26 WG2055559
Chromium 10.5 1.29 1 05/10/2023 18:26 WG2055559
Copper 17.0 2.59 1 05/10/2023 18:26 WG2055559
Lead 11.8 0.646 1 05/10/2023 18:26 WG2055559
Nickel 7.39 2.59 1 05/10/2023 18:26 WG2055559
Selenium ND 2.59 1 05/10/2023 18:26 WG2055559
Silver ND 1.29 1 05/10/2023 18:26 WG2055559
Thallium ND 2.59 1 05/10/2023 18:26 WG2055559
Zinc 39.0 6.46 1 05/10/2023 18:26 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.04 25 05/11/2023 13:05 WG2057784
(S) a,a,a-Trifluorotoluene(FID)92.0 77.0-120 05/11/2023 13:05 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0808 1 05/11/2023 12:48 WG2058136
Acrylonitrile ND 0.0202 1 05/11/2023 12:48 WG2058136
Benzene ND 0.00162 1 05/11/2023 12:48 WG2058136
Bromobenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
Bromodichloromethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Bromoform ND 0.0404 1 05/11/2023 12:48 WG2058136
Bromomethane ND 0.0202 1 05/11/2023 12:48 WG2058136
n-Butylbenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
sec-Butylbenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
tert-Butylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Carbon tetrachloride ND 0.00808 1 05/11/2023 12:48 WG2058136
Chlorobenzene ND 0.00404 1 05/11/2023 12:48 WG2058136
Chlorodibromomethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Chloroethane ND 0.00808 1 05/11/2023 12:48 WG2058136
Chloroform ND 0.00404 1 05/11/2023 12:48 WG2058136
Chloromethane ND 0.0202 1 05/11/2023 12:48 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00404 1 05/11/2023 12:48 WG2058136
4-Chlorotoluene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0404 1 05/11/2023 12:48 WG2058136
1,2-Dibromoethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Dibromomethane ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2-Dichlorobenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,3-Dichlorobenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,4-Dichlorobenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Dichlorodifluoromethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1-Dichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,2-Dichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1-Dichloroethene ND 0.00404 1 05/11/2023 12:48 WG2058136
cis-1,2-Dichloroethene ND 0.00404 1 05/11/2023 12:48 WG2058136
trans-1,2-Dichloroethene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2-Dichloropropane ND 0.00808 1 05/11/2023 12:48 WG2058136
1,1-Dichloropropene ND 0.00404 1 05/11/2023 12:48 WG2058136
1,3-Dichloropropane ND 0.00808 1 05/11/2023 12:48 WG2058136
cis-1,3-Dichloropropene ND 0.00404 1 05/11/2023 12:48 WG2058136
trans-1,3-Dichloropropene ND 0.00808 1 05/11/2023 12:48 WG2058136
2,2-Dichloropropane ND 0.00404 1 05/11/2023 12:48 WG2058136
Di-isopropyl ether ND 0.00162 1 05/11/2023 12:48 WG2058136
Ethylbenzene ND 0.00404 1 05/11/2023 12:48 WG2058136
Hexachloro-1,3-butadiene ND 0.0404 1 05/11/2023 12:48 WG2058136
Isopropylbenzene ND 0.00404 1 05/11/2023 12:48 WG2058136
p-Isopropyltoluene ND 0.00808 1 05/11/2023 12:48 WG2058136
2-Butanone (MEK)ND 0.162 1 05/11/2023 12:48 WG2058136
Methylene Chloride ND 0.0404 1 05/11/2023 12:48 WG2058136
4-Methyl-2-pentanone (MIBK)ND 0.0404 1 05/11/2023 12:48 WG2058136
Methyl tert-butyl ether ND 0.00162 1 05/11/2023 12:48 WG2058136
Naphthalene ND J4 0.0202 1 05/11/2023 12:48 WG2058136
n-Propylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Styrene ND 0.0202 1 05/11/2023 12:48 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Tetrachloroethene ND 0.00404 1 05/11/2023 12:48 WG2058136
Toluene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0202 1 05/11/2023 12:48 WG2058136
1,2,4-Trichlorobenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
1,1,1-Trichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1,2-Trichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Trichloroethene ND 0.00162 1 05/11/2023 12:48 WG2058136
Trichlorofluoromethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,2,3-Trichloropropane ND 0.0202 1 05/11/2023 12:48 WG2058136
1,2,4-Trimethylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2,3-Trimethylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,3,5-Trimethylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Vinyl chloride ND 0.00404 1 05/11/2023 12:48 WG2058136
Xylenes, Total ND 0.0105 1 05/11/2023 12:48 WG2058136
(S) Toluene-d8 107 75.0-131 05/11/2023 12:48 WG2058136
(S) 4-Bromofluorobenzene 97.7 67.0-138 05/11/2023 12:48 WG2058136
(S) 1,2-Dichloroethane-d4 117 70.0-130 05/11/2023 12:48 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.17 1 05/14/2023 01:38 WG2059338
C28-C40 Oil Range 5.88 5.17 1 05/14/2023 01:38 WG2059338
(S) o-Terphenyl 18.6 18.0-148 05/14/2023 01:38 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1221 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1232 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1242 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1248 ND 0.0220 1 05/13/2023 17:55 WG2057922
PCB 1254 ND 0.0220 1 05/13/2023 17:55 WG2057922
PCB 1260 ND 0.0220 1 05/13/2023 17:55 WG2057922
(S) Decachlorobiphenyl 41.4 10.0-135 05/13/2023 17:55 WG2057922
(S) Tetrachloro-m-xylene 67.0 10.0-139 05/13/2023 17:55 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Acenaphthylene ND 0.0430 1 05/12/2023 18:31 WG2058400
Anthracene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzidine ND 2.16 1 05/12/2023 18:31 WG2058400
Benzo(a)anthracene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(b)fluoranthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(k)fluoranthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(g,h,i)perylene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(a)pyrene ND 0.0430 1 05/12/2023 18:31 WG2058400
Bis(2-chlorethoxy)methane ND 0.430 1 05/12/2023 18:31 WG2058400
Bis(2-chloroethyl)ether ND 0.430 1 05/12/2023 18:31 WG2058400
2,2-Oxybis(1-Chloropropane)ND 0.430 1 05/12/2023 18:31 WG2058400
4-Bromophenyl-phenylether ND 0.430 1 05/12/2023 18:31 WG2058400
2-Chloronaphthalene ND 0.0430 1 05/12/2023 18:31 WG2058400
4-Chlorophenyl-phenylether ND 0.430 1 05/12/2023 18:31 WG2058400
Chrysene ND 0.0430 1 05/12/2023 18:31 WG2058400
Dibenz(a,h)anthracene ND 0.0430 1 05/12/2023 18:31 WG2058400
3,3-Dichlorobenzidine ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dinitrotoluene ND 0.430 1 05/12/2023 18:31 WG2058400
2,6-Dinitrotoluene ND 0.430 1 05/12/2023 18:31 WG2058400
Fluoranthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Fluorene ND 0.0430 1 05/12/2023 18:31 WG2058400
Hexachlorobenzene ND 0.430 1 05/12/2023 18:31 WG2058400
Hexachloro-1,3-butadiene ND 0.430 1 05/12/2023 18:31 WG2058400
Hexachlorocyclopentadiene ND 0.430 1 05/12/2023 18:31 WG2058400
Hexachloroethane ND 0.430 1 05/12/2023 18:31 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0430 1 05/12/2023 18:31 WG2058400
Isophorone ND 0.430 1 05/12/2023 18:31 WG2058400
Naphthalene ND 0.0430 1 05/12/2023 18:31 WG2058400
Nitrobenzene ND 0.430 1 05/12/2023 18:31 WG2058400
n-Nitrosodimethylamine ND 0.430 1 05/12/2023 18:31 WG2058400
n-Nitrosodiphenylamine ND 0.430 1 05/12/2023 18:31 WG2058400
n-Nitrosodi-n-propylamine ND 0.430 1 05/12/2023 18:31 WG2058400
Phenanthrene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzylbutyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Di-n-butyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Diethyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Dimethyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Di-n-octyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Pyrene ND 0.0430 1 05/12/2023 18:31 WG2058400
1,2,4-Trichlorobenzene ND 0.430 1 05/12/2023 18:31 WG2058400
4-Chloro-3-methylphenol ND 0.430 1 05/12/2023 18:31 WG2058400
2-Chlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dichlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dimethylphenol ND 0.430 1 05/12/2023 18:31 WG2058400
4,6-Dinitro-2-methylphenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dinitrophenol ND 0.430 1 05/12/2023 18:31 WG2058400
2-Nitrophenol ND 0.430 1 05/12/2023 18:31 WG2058400
4-Nitrophenol ND 0.430 1 05/12/2023 18:31 WG2058400
Pentachlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
Phenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4,6-Trichlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
(S) Nitrobenzene-d5 50.9 10.0-122 05/12/2023 18:31 WG2058400
(S) 2-Fluorobiphenyl 43.1 15.0-120 05/12/2023 18:31 WG2058400
(S) p-Terphenyl-d14 38.6 10.0-120 05/12/2023 18:31 WG2058400
(S) Phenol-d5 44.4 10.0-120 05/12/2023 18:31 WG2058400
(S) 2-Fluorophenol 50.2 12.0-120 05/12/2023 18:31 WG2058400
(S) 2,4,6-Tribromophenol 33.3 10.0-127 05/12/2023 18:31 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00776 1 05/12/2023 03:20 WG2058011
Acenaphthene ND 0.00776 1 05/12/2023 03:20 WG2058011
Acenaphthylene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(a)anthracene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(a)pyrene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(b)fluoranthene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(g,h,i)perylene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(k)fluoranthene ND 0.00776 1 05/12/2023 03:20 WG2058011
Chrysene ND 0.00776 1 05/12/2023 03:20 WG2058011
Dibenz(a,h)anthracene ND 0.00776 1 05/12/2023 03:20 WG2058011
Fluoranthene 0.0113 0.00776 1 05/12/2023 03:20 WG2058011
Fluorene ND 0.00776 1 05/12/2023 03:20 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00776 1 05/12/2023 03:20 WG2058011
Naphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
Phenanthrene ND 0.00776 1 05/12/2023 03:20 WG2058011
Pyrene 0.00777 0.00776 1 05/12/2023 03:20 WG2058011
1-Methylnaphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
2-Methylnaphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
2-Chloronaphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
(S) p-Terphenyl-d14 77.6 23.0-120 05/12/2023 03:20 WG2058011
(S) Nitrobenzene-d5 114 14.0-149 05/12/2023 03:20 WG2058011
(S) 2-Fluorobiphenyl 102 34.0-125 05/12/2023 03:20 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.7 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.22 1 05/11/2023 01:54 WG2056423
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0490 1 05/12/2023 12:36 WG2056112
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.45 1 05/10/2023 18:29 WG2055559
Arsenic 4.89 2.45 1 05/10/2023 18:29 WG2055559
Beryllium 0.288 0.245 1 05/10/2023 18:29 WG2055559
Cadmium ND 0.612 1 05/10/2023 18:29 WG2055559
Chromium 7.71 1.22 1 05/10/2023 18:29 WG2055559
Copper 7.43 2.45 1 05/10/2023 18:29 WG2055559
Lead 3.89 0.612 1 05/10/2023 18:29 WG2055559
Nickel 5.93 2.45 1 05/10/2023 18:29 WG2055559
Selenium ND 2.45 1 05/10/2023 18:29 WG2055559
Silver ND 1.22 1 05/10/2023 18:29 WG2055559
Thallium ND 2.45 1 05/10/2023 18:29 WG2055559
Zinc 23.3 6.12 1 05/10/2023 18:29 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.70 25 05/11/2023 13:24 WG2057784
(S) a,a,a-Trifluorotoluene(FID)91.0 77.0-120 05/11/2023 13:24 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0740 1 05/11/2023 13:07 WG2058136
Acrylonitrile ND 0.0185 1 05/11/2023 13:07 WG2058136
Benzene ND 0.00148 1 05/11/2023 13:07 WG2058136
Bromobenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
Bromodichloromethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Bromoform ND 0.0370 1 05/11/2023 13:07 WG2058136
Bromomethane ND 0.0185 1 05/11/2023 13:07 WG2058136
n-Butylbenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
sec-Butylbenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
tert-Butylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Carbon tetrachloride ND 0.00740 1 05/11/2023 13:07 WG2058136
Chlorobenzene ND 0.00370 1 05/11/2023 13:07 WG2058136
Chlorodibromomethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Chloroethane ND 0.00740 1 05/11/2023 13:07 WG2058136
Chloroform ND 0.00370 1 05/11/2023 13:07 WG2058136
Chloromethane ND 0.0185 1 05/11/2023 13:07 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00370 1 05/11/2023 13:07 WG2058136
4-Chlorotoluene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0370 1 05/11/2023 13:07 WG2058136
1,2-Dibromoethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Dibromomethane ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2-Dichlorobenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,3-Dichlorobenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,4-Dichlorobenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Dichlorodifluoromethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1-Dichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,2-Dichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1-Dichloroethene ND 0.00370 1 05/11/2023 13:07 WG2058136
cis-1,2-Dichloroethene ND 0.00370 1 05/11/2023 13:07 WG2058136
trans-1,2-Dichloroethene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2-Dichloropropane ND 0.00740 1 05/11/2023 13:07 WG2058136
1,1-Dichloropropene ND 0.00370 1 05/11/2023 13:07 WG2058136
1,3-Dichloropropane ND 0.00740 1 05/11/2023 13:07 WG2058136
cis-1,3-Dichloropropene ND 0.00370 1 05/11/2023 13:07 WG2058136
trans-1,3-Dichloropropene ND 0.00740 1 05/11/2023 13:07 WG2058136
2,2-Dichloropropane ND 0.00370 1 05/11/2023 13:07 WG2058136
Di-isopropyl ether ND 0.00148 1 05/11/2023 13:07 WG2058136
Ethylbenzene ND 0.00370 1 05/11/2023 13:07 WG2058136
Hexachloro-1,3-butadiene ND 0.0370 1 05/11/2023 13:07 WG2058136
Isopropylbenzene ND 0.00370 1 05/11/2023 13:07 WG2058136
p-Isopropyltoluene ND 0.00740 1 05/11/2023 13:07 WG2058136
2-Butanone (MEK)ND 0.148 1 05/11/2023 13:07 WG2058136
Methylene Chloride ND 0.0370 1 05/11/2023 13:07 WG2058136
4-Methyl-2-pentanone (MIBK)ND 0.0370 1 05/11/2023 13:07 WG2058136
Methyl tert-butyl ether ND 0.00148 1 05/11/2023 13:07 WG2058136
Naphthalene ND J4 0.0185 1 05/11/2023 13:07 WG2058136
n-Propylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Styrene ND 0.0185 1 05/11/2023 13:07 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Tetrachloroethene ND 0.00370 1 05/11/2023 13:07 WG2058136
Toluene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0185 1 05/11/2023 13:07 WG2058136
1,2,4-Trichlorobenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
1,1,1-Trichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1,2-Trichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Trichloroethene ND 0.00148 1 05/11/2023 13:07 WG2058136
Trichlorofluoromethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,2,3-Trichloropropane ND 0.0185 1 05/11/2023 13:07 WG2058136
1,2,4-Trimethylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2,3-Trimethylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,3,5-Trimethylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Vinyl chloride ND 0.00370 1 05/11/2023 13:07 WG2058136
Xylenes, Total ND 0.00962 1 05/11/2023 13:07 WG2058136
(S) Toluene-d8 103 75.0-131 05/11/2023 13:07 WG2058136
(S) 4-Bromofluorobenzene 102 67.0-138 05/11/2023 13:07 WG2058136
(S) 1,2-Dichloroethane-d4 119 70.0-130 05/11/2023 13:07 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 6.03 1.23 05/14/2023 01:25 WG2059338
C28-C40 Oil Range 6.18 6.03 1.23 05/14/2023 01:25 WG2059338
(S) o-Terphenyl 28.3 18.0-148 05/14/2023 01:25 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1221 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1232 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1242 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1248 ND 0.0208 1 05/13/2023 18:08 WG2057922
PCB 1254 ND 0.0208 1 05/13/2023 18:08 WG2057922
PCB 1260 ND 0.0208 1 05/13/2023 18:08 WG2057922
(S) Decachlorobiphenyl 52.4 10.0-135 05/13/2023 18:08 WG2057922
(S) Tetrachloro-m-xylene 73.4 10.0-139 05/13/2023 18:08 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Acenaphthylene ND 0.0408 1 05/12/2023 17:15 WG2058400
Anthracene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzidine ND 2.05 1 05/12/2023 17:15 WG2058400
Benzo(a)anthracene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(b)fluoranthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(k)fluoranthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(g,h,i)perylene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(a)pyrene ND 0.0408 1 05/12/2023 17:15 WG2058400
Bis(2-chlorethoxy)methane ND 0.408 1 05/12/2023 17:15 WG2058400
Bis(2-chloroethyl)ether ND 0.408 1 05/12/2023 17:15 WG2058400
2,2-Oxybis(1-Chloropropane)ND 0.408 1 05/12/2023 17:15 WG2058400
4-Bromophenyl-phenylether ND 0.408 1 05/12/2023 17:15 WG2058400
2-Chloronaphthalene ND 0.0408 1 05/12/2023 17:15 WG2058400
4-Chlorophenyl-phenylether ND 0.408 1 05/12/2023 17:15 WG2058400
Chrysene ND 0.0408 1 05/12/2023 17:15 WG2058400
Dibenz(a,h)anthracene ND 0.0408 1 05/12/2023 17:15 WG2058400
3,3-Dichlorobenzidine ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dinitrotoluene ND 0.408 1 05/12/2023 17:15 WG2058400
2,6-Dinitrotoluene ND 0.408 1 05/12/2023 17:15 WG2058400
Fluoranthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Fluorene ND 0.0408 1 05/12/2023 17:15 WG2058400
Hexachlorobenzene ND 0.408 1 05/12/2023 17:15 WG2058400
Hexachloro-1,3-butadiene ND 0.408 1 05/12/2023 17:15 WG2058400
Hexachlorocyclopentadiene ND 0.408 1 05/12/2023 17:15 WG2058400
Hexachloroethane ND 0.408 1 05/12/2023 17:15 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0408 1 05/12/2023 17:15 WG2058400
Isophorone ND 0.408 1 05/12/2023 17:15 WG2058400
Naphthalene ND 0.0408 1 05/12/2023 17:15 WG2058400
Nitrobenzene ND 0.408 1 05/12/2023 17:15 WG2058400
n-Nitrosodimethylamine ND 0.408 1 05/12/2023 17:15 WG2058400
n-Nitrosodiphenylamine ND 0.408 1 05/12/2023 17:15 WG2058400
n-Nitrosodi-n-propylamine ND 0.408 1 05/12/2023 17:15 WG2058400
Phenanthrene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzylbutyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Di-n-butyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Diethyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Dimethyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Di-n-octyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Pyrene ND 0.0408 1 05/12/2023 17:15 WG2058400
1,2,4-Trichlorobenzene ND 0.408 1 05/12/2023 17:15 WG2058400
4-Chloro-3-methylphenol ND 0.408 1 05/12/2023 17:15 WG2058400
2-Chlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dichlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dimethylphenol ND 0.408 1 05/12/2023 17:15 WG2058400
4,6-Dinitro-2-methylphenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dinitrophenol ND 0.408 1 05/12/2023 17:15 WG2058400
2-Nitrophenol ND 0.408 1 05/12/2023 17:15 WG2058400
4-Nitrophenol ND 0.408 1 05/12/2023 17:15 WG2058400
Pentachlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
Phenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4,6-Trichlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
(S) Nitrobenzene-d5 50.6 10.0-122 05/12/2023 17:15 WG2058400
(S) 2-Fluorobiphenyl 45.5 15.0-120 05/12/2023 17:15 WG2058400
(S) p-Terphenyl-d14 43.9 10.0-120 05/12/2023 17:15 WG2058400
(S) Phenol-d5 47.0 10.0-120 05/12/2023 17:15 WG2058400
(S) 2-Fluorophenol 51.2 12.0-120 05/12/2023 17:15 WG2058400
(S) 2,4,6-Tribromophenol 35.6 10.0-127 05/12/2023 17:15 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00735 1 05/12/2023 03:37 WG2058011
Acenaphthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Acenaphthylene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(a)anthracene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(a)pyrene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(b)fluoranthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(g,h,i)perylene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(k)fluoranthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Chrysene ND 0.00735 1 05/12/2023 03:37 WG2058011
Dibenz(a,h)anthracene ND 0.00735 1 05/12/2023 03:37 WG2058011
Fluoranthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Fluorene ND 0.00735 1 05/12/2023 03:37 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00735 1 05/12/2023 03:37 WG2058011
Naphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
Phenanthrene ND 0.00735 1 05/12/2023 03:37 WG2058011
Pyrene ND 0.00735 1 05/12/2023 03:37 WG2058011
1-Methylnaphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
2-Methylnaphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
2-Chloronaphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
(S) p-Terphenyl-d14 89.3 23.0-120 05/12/2023 03:37 WG2058011
(S) Nitrobenzene-d5 111 14.0-149 05/12/2023 03:37 WG2058011
(S) 2-Fluorobiphenyl 99.0 34.0-125 05/12/2023 03:37 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.3 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.28 1 05/11/2023 01:59 WG2056423
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0511 1 05/12/2023 12:38 WG2056112
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.55 1 05/10/2023 18:32 WG2055559
Arsenic 8.49 2.55 1 05/10/2023 18:32 WG2055559
Beryllium 0.443 0.255 1 05/10/2023 18:32 WG2055559
Cadmium ND 0.638 1 05/10/2023 18:32 WG2055559
Chromium 12.6 1.28 1 05/10/2023 18:32 WG2055559
Copper 16.3 2.55 1 05/10/2023 18:32 WG2055559
Lead 15.8 0.638 1 05/10/2023 18:32 WG2055559
Nickel 9.89 2.55 1 05/10/2023 18:32 WG2055559
Selenium ND 2.55 1 05/10/2023 18:32 WG2055559
Silver ND 1.28 1 05/10/2023 18:32 WG2055559
Thallium ND 2.55 1 05/10/2023 18:32 WG2055559
Zinc 39.7 6.38 1 05/10/2023 18:32 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.94 25 05/11/2023 13:42 WG2057784
(S) a,a,a-Trifluorotoluene(FID)90.4 77.0-120 05/11/2023 13:42 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0788 1 05/11/2023 13:26 WG2058136
Acrylonitrile ND 0.0197 1 05/11/2023 13:26 WG2058136
Benzene ND 0.00158 1 05/11/2023 13:26 WG2058136
Bromobenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
Bromodichloromethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Bromoform ND 0.0394 1 05/11/2023 13:26 WG2058136
Bromomethane ND 0.0197 1 05/11/2023 13:26 WG2058136
n-Butylbenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
sec-Butylbenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
tert-Butylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Carbon tetrachloride ND 0.00788 1 05/11/2023 13:26 WG2058136
Chlorobenzene ND 0.00394 1 05/11/2023 13:26 WG2058136
Chlorodibromomethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Chloroethane ND 0.00788 1 05/11/2023 13:26 WG2058136
Chloroform ND 0.00394 1 05/11/2023 13:26 WG2058136
Chloromethane ND 0.0197 1 05/11/2023 13:26 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00394 1 05/11/2023 13:26 WG2058136
4-Chlorotoluene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0394 1 05/11/2023 13:26 WG2058136
1,2-Dibromoethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Dibromomethane ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2-Dichlorobenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,3-Dichlorobenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,4-Dichlorobenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Dichlorodifluoromethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1-Dichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,2-Dichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1-Dichloroethene ND 0.00394 1 05/11/2023 13:26 WG2058136
cis-1,2-Dichloroethene ND 0.00394 1 05/11/2023 13:26 WG2058136
trans-1,2-Dichloroethene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2-Dichloropropane ND 0.00788 1 05/11/2023 13:26 WG2058136
1,1-Dichloropropene ND 0.00394 1 05/11/2023 13:26 WG2058136
1,3-Dichloropropane ND 0.00788 1 05/11/2023 13:26 WG2058136
cis-1,3-Dichloropropene ND 0.00394 1 05/11/2023 13:26 WG2058136
trans-1,3-Dichloropropene ND 0.00788 1 05/11/2023 13:26 WG2058136
2,2-Dichloropropane ND 0.00394 1 05/11/2023 13:26 WG2058136
Di-isopropyl ether ND 0.00158 1 05/11/2023 13:26 WG2058136
Ethylbenzene 0.0196 0.00394 1 05/11/2023 13:26 WG2058136
Hexachloro-1,3-butadiene ND 0.0394 1 05/11/2023 13:26 WG2058136
Isopropylbenzene ND 0.00394 1 05/11/2023 13:26 WG2058136
p-Isopropyltoluene ND 0.00788 1 05/11/2023 13:26 WG2058136
2-Butanone (MEK)ND 0.158 1 05/11/2023 13:26 WG2058136
Methylene Chloride ND 0.0394 1 05/11/2023 13:26 WG2058136
4-Methyl-2-pentanone (MIBK)ND 0.0394 1 05/11/2023 13:26 WG2058136
Methyl tert-butyl ether ND 0.00158 1 05/11/2023 13:26 WG2058136
Naphthalene ND J4 0.0197 1 05/11/2023 13:26 WG2058136
n-Propylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Styrene ND 0.0197 1 05/11/2023 13:26 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Tetrachloroethene ND 0.00394 1 05/11/2023 13:26 WG2058136
Toluene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0197 1 05/11/2023 13:26 WG2058136
1,2,4-Trichlorobenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
1,1,1-Trichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1,2-Trichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Trichloroethene ND 0.00158 1 05/11/2023 13:26 WG2058136
Trichlorofluoromethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,2,3-Trichloropropane ND 0.0197 1 05/11/2023 13:26 WG2058136
1,2,4-Trimethylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2,3-Trimethylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,3,5-Trimethylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Vinyl chloride ND 0.00394 1 05/11/2023 13:26 WG2058136
Xylenes, Total 0.102 0.0103 1 05/11/2023 13:26 WG2058136
(S) Toluene-d8 101 75.0-131 05/11/2023 13:26 WG2058136
(S) 4-Bromofluorobenzene 101 67.0-138 05/11/2023 13:26 WG2058136
(S) 1,2-Dichloroethane-d4 120 70.0-130 05/11/2023 13:26 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.11 1 05/14/2023 02:31 WG2059338
C28-C40 Oil Range 8.45 5.11 1 05/14/2023 02:31 WG2059338
(S) o-Terphenyl 31.9 18.0-148 05/14/2023 02:31 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1221 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1232 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1242 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1248 ND 0.0217 1 05/13/2023 18:20 WG2057922
PCB 1254 ND 0.0217 1 05/13/2023 18:20 WG2057922
PCB 1260 ND 0.0217 1 05/13/2023 18:20 WG2057922
(S) Decachlorobiphenyl 61.7 10.0-135 05/13/2023 18:20 WG2057922
(S) Tetrachloro-m-xylene 82.3 10.0-139 05/13/2023 18:20 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Acenaphthylene ND 0.0425 1 05/12/2023 18:55 WG2058400
Anthracene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzidine ND 2.13 1 05/12/2023 18:55 WG2058400
Benzo(a)anthracene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(b)fluoranthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(k)fluoranthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(g,h,i)perylene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(a)pyrene ND 0.0425 1 05/12/2023 18:55 WG2058400
Bis(2-chlorethoxy)methane ND 0.425 1 05/12/2023 18:55 WG2058400
Bis(2-chloroethyl)ether ND 0.425 1 05/12/2023 18:55 WG2058400
2,2-Oxybis(1-Chloropropane)ND 0.425 1 05/12/2023 18:55 WG2058400
4-Bromophenyl-phenylether ND 0.425 1 05/12/2023 18:55 WG2058400
2-Chloronaphthalene ND 0.0425 1 05/12/2023 18:55 WG2058400
4-Chlorophenyl-phenylether ND 0.425 1 05/12/2023 18:55 WG2058400
Chrysene ND 0.0425 1 05/12/2023 18:55 WG2058400
Dibenz(a,h)anthracene ND 0.0425 1 05/12/2023 18:55 WG2058400
3,3-Dichlorobenzidine ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dinitrotoluene ND 0.425 1 05/12/2023 18:55 WG2058400
2,6-Dinitrotoluene ND 0.425 1 05/12/2023 18:55 WG2058400
Fluoranthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Fluorene ND 0.0425 1 05/12/2023 18:55 WG2058400
Hexachlorobenzene ND 0.425 1 05/12/2023 18:55 WG2058400
Hexachloro-1,3-butadiene ND 0.425 1 05/12/2023 18:55 WG2058400
Hexachlorocyclopentadiene ND 0.425 1 05/12/2023 18:55 WG2058400
Hexachloroethane ND 0.425 1 05/12/2023 18:55 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0425 1 05/12/2023 18:55 WG2058400
Isophorone ND 0.425 1 05/12/2023 18:55 WG2058400
Naphthalene ND 0.0425 1 05/12/2023 18:55 WG2058400
Nitrobenzene ND 0.425 1 05/12/2023 18:55 WG2058400
n-Nitrosodimethylamine ND 0.425 1 05/12/2023 18:55 WG2058400
n-Nitrosodiphenylamine ND 0.425 1 05/12/2023 18:55 WG2058400
n-Nitrosodi-n-propylamine ND 0.425 1 05/12/2023 18:55 WG2058400
Phenanthrene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzylbutyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Di-n-butyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Diethyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Dimethyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Di-n-octyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Pyrene ND 0.0425 1 05/12/2023 18:55 WG2058400
1,2,4-Trichlorobenzene ND 0.425 1 05/12/2023 18:55 WG2058400
4-Chloro-3-methylphenol ND 0.425 1 05/12/2023 18:55 WG2058400
2-Chlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dichlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dimethylphenol ND 0.425 1 05/12/2023 18:55 WG2058400
4,6-Dinitro-2-methylphenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dinitrophenol ND 0.425 1 05/12/2023 18:55 WG2058400
2-Nitrophenol ND 0.425 1 05/12/2023 18:55 WG2058400
4-Nitrophenol ND 0.425 1 05/12/2023 18:55 WG2058400
Pentachlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
Phenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4,6-Trichlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
(S) Nitrobenzene-d5 59.6 10.0-122 05/12/2023 18:55 WG2058400
(S) 2-Fluorobiphenyl 51.7 15.0-120 05/12/2023 18:55 WG2058400
(S) p-Terphenyl-d14 55.8 10.0-120 05/12/2023 18:55 WG2058400
(S) Phenol-d5 51.1 10.0-120 05/12/2023 18:55 WG2058400
(S) 2-Fluorophenol 55.2 12.0-120 05/12/2023 18:55 WG2058400
(S) 2,4,6-Tribromophenol 37.1 10.0-127 05/12/2023 18:55 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00766 1 05/12/2023 03:55 WG2058011
Acenaphthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Acenaphthylene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(a)anthracene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(a)pyrene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(b)fluoranthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(g,h,i)perylene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(k)fluoranthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Chrysene ND 0.00766 1 05/12/2023 03:55 WG2058011
Dibenz(a,h)anthracene ND 0.00766 1 05/12/2023 03:55 WG2058011
Fluoranthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Fluorene ND 0.00766 1 05/12/2023 03:55 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00766 1 05/12/2023 03:55 WG2058011
Naphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
Phenanthrene ND 0.00766 1 05/12/2023 03:55 WG2058011
Pyrene ND 0.00766 1 05/12/2023 03:55 WG2058011
1-Methylnaphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
2-Methylnaphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
2-Chloronaphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
(S) p-Terphenyl-d14 94.5 23.0-120 05/12/2023 03:55 WG2058011
(S) Nitrobenzene-d5 105 14.0-149 05/12/2023 03:55 WG2058011
(S) 2-Fluorobiphenyl 91.5 34.0-125 05/12/2023 03:55 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.3 1 05/08/2023 15:17 WG2055863
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.17 1 05/11/2023 02:05 WG2056423
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0469 1 05/12/2023 12:40 WG2056112
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.34 1 05/10/2023 18:35 WG2055559
Arsenic 6.04 2.34 1 05/10/2023 18:35 WG2055559
Beryllium 0.310 0.234 1 05/10/2023 18:35 WG2055559
Cadmium ND 0.586 1 05/10/2023 18:35 WG2055559
Chromium 7.97 1.17 1 05/10/2023 18:35 WG2055559
Copper 5.59 2.34 1 05/10/2023 18:35 WG2055559
Lead 3.71 0.586 1 05/10/2023 18:35 WG2055559
Nickel 5.22 2.34 1 05/10/2023 18:35 WG2055559
Selenium ND 2.34 1 05/10/2023 18:35 WG2055559
Silver ND 1.17 1 05/10/2023 18:35 WG2055559
Thallium ND 2.34 1 05/10/2023 18:35 WG2055559
Zinc 20.7 5.86 1 05/10/2023 18:35 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.94 30 05/11/2023 14:01 WG2057784
(S) a,a,a-Trifluorotoluene(FID)91.5 77.0-120 05/11/2023 14:01 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0801 0.0789 1.2 05/11/2023 13:45 WG2058136
Acrylonitrile ND 0.0197 1.2 05/11/2023 13:45 WG2058136
Benzene ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Bromobenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
Bromodichloromethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Bromoform ND 0.0394 1.2 05/11/2023 13:45 WG2058136
Bromomethane ND 0.0197 1.2 05/11/2023 13:45 WG2058136
n-Butylbenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
sec-Butylbenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
tert-Butylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Carbon tetrachloride ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Chlorobenzene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Chlorodibromomethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Chloroethane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Chloroform ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Chloromethane ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
4-Chlorotoluene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0394 1.2 05/11/2023 13:45 WG2058136
1,2-Dibromoethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Dibromomethane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2-Dichlorobenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,3-Dichlorobenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,4-Dichlorobenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Dichlorodifluoromethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1-Dichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,2-Dichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1-Dichloroethene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
cis-1,2-Dichloroethene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
trans-1,2-Dichloroethene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2-Dichloropropane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,1-Dichloropropene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,3-Dichloropropane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
cis-1,3-Dichloropropene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
trans-1,3-Dichloropropene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
2,2-Dichloropropane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Di-isopropyl ether ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Ethylbenzene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Hexachloro-1,3-butadiene ND 0.0394 1.2 05/11/2023 13:45 WG2058136
Isopropylbenzene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
p-Isopropyltoluene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
2-Butanone (MEK)ND 0.158 1.2 05/11/2023 13:45 WG2058136
Methylene Chloride ND 0.0394 1.2 05/11/2023 13:45 WG2058136
4-Methyl-2-pentanone (MIBK)ND 0.0394 1.2 05/11/2023 13:45 WG2058136
Methyl tert-butyl ether ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Naphthalene ND J4 0.0197 1.2 05/11/2023 13:45 WG2058136
n-Propylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Styrene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Tetrachloroethene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Toluene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0197 1.2 05/11/2023 13:45 WG2058136
1,2,4-Trichlorobenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1,1,1-Trichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1,2-Trichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Trichloroethene ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Trichlorofluoromethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,2,3-Trichloropropane ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1,2,4-Trimethylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2,3-Trimethylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,3,5-Trimethylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Vinyl chloride ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Xylenes, Total ND 0.0103 1.2 05/11/2023 13:45 WG2058136
(S) Toluene-d8 102 75.0-131 05/11/2023 13:45 WG2058136
(S) 4-Bromofluorobenzene 101 67.0-138 05/11/2023 13:45 WG2058136
(S) 1,2-Dichloroethane-d4 121 70.0-130 05/11/2023 13:45 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.69 1 05/14/2023 00:03 WG2059338
C28-C40 Oil Range ND 4.69 1 05/14/2023 00:03 WG2059338
(S) o-Terphenyl 27.9 18.0-148 05/14/2023 00:03 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1221 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1232 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1242 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1248 ND 0.0199 1 05/13/2023 18:33 WG2057922
PCB 1254 ND 0.0199 1 05/13/2023 18:33 WG2057922
PCB 1260 ND 0.0199 1 05/13/2023 18:33 WG2057922
(S) Decachlorobiphenyl 53.3 10.0-135 05/13/2023 18:33 WG2057922
(S) Tetrachloro-m-xylene 72.9 10.0-139 05/13/2023 18:33 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Acenaphthylene ND 0.0390 1 05/12/2023 16:26 WG2058400
Anthracene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzidine ND 1.96 1 05/12/2023 16:26 WG2058400
Benzo(a)anthracene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(b)fluoranthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(k)fluoranthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(g,h,i)perylene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(a)pyrene ND 0.0390 1 05/12/2023 16:26 WG2058400
Bis(2-chlorethoxy)methane ND 0.390 1 05/12/2023 16:26 WG2058400
Bis(2-chloroethyl)ether ND 0.390 1 05/12/2023 16:26 WG2058400
2,2-Oxybis(1-Chloropropane)ND 0.390 1 05/12/2023 16:26 WG2058400
4-Bromophenyl-phenylether ND 0.390 1 05/12/2023 16:26 WG2058400
2-Chloronaphthalene ND 0.0390 1 05/12/2023 16:26 WG2058400
4-Chlorophenyl-phenylether ND 0.390 1 05/12/2023 16:26 WG2058400
Chrysene ND 0.0390 1 05/12/2023 16:26 WG2058400
Dibenz(a,h)anthracene ND 0.0390 1 05/12/2023 16:26 WG2058400
3,3-Dichlorobenzidine ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dinitrotoluene ND 0.390 1 05/12/2023 16:26 WG2058400
2,6-Dinitrotoluene ND 0.390 1 05/12/2023 16:26 WG2058400
Fluoranthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Fluorene ND 0.0390 1 05/12/2023 16:26 WG2058400
Hexachlorobenzene ND 0.390 1 05/12/2023 16:26 WG2058400
Hexachloro-1,3-butadiene ND 0.390 1 05/12/2023 16:26 WG2058400
Hexachlorocyclopentadiene ND 0.390 1 05/12/2023 16:26 WG2058400
Hexachloroethane ND 0.390 1 05/12/2023 16:26 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0390 1 05/12/2023 16:26 WG2058400
Isophorone ND 0.390 1 05/12/2023 16:26 WG2058400
Naphthalene ND 0.0390 1 05/12/2023 16:26 WG2058400
Nitrobenzene ND 0.390 1 05/12/2023 16:26 WG2058400
n-Nitrosodimethylamine ND 0.390 1 05/12/2023 16:26 WG2058400
n-Nitrosodiphenylamine ND 0.390 1 05/12/2023 16:26 WG2058400
n-Nitrosodi-n-propylamine ND 0.390 1 05/12/2023 16:26 WG2058400
Phenanthrene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzylbutyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Di-n-butyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Diethyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Dimethyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Di-n-octyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Pyrene ND 0.0390 1 05/12/2023 16:26 WG2058400
1,2,4-Trichlorobenzene ND 0.390 1 05/12/2023 16:26 WG2058400
4-Chloro-3-methylphenol ND 0.390 1 05/12/2023 16:26 WG2058400
2-Chlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dichlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dimethylphenol ND 0.390 1 05/12/2023 16:26 WG2058400
4,6-Dinitro-2-methylphenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dinitrophenol ND 0.390 1 05/12/2023 16:26 WG2058400
2-Nitrophenol ND 0.390 1 05/12/2023 16:26 WG2058400
4-Nitrophenol ND 0.390 1 05/12/2023 16:26 WG2058400
Pentachlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
Phenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4,6-Trichlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
(S) Nitrobenzene-d5 54.4 10.0-122 05/12/2023 16:26 WG2058400
(S) 2-Fluorobiphenyl 46.8 15.0-120 05/12/2023 16:26 WG2058400
(S) p-Terphenyl-d14 51.1 10.0-120 05/12/2023 16:26 WG2058400
(S) Phenol-d5 45.6 10.0-120 05/12/2023 16:26 WG2058400
(S) 2-Fluorophenol 53.2 12.0-120 05/12/2023 16:26 WG2058400
(S) 2,4,6-Tribromophenol 39.4 10.0-127 05/12/2023 16:26 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00703 1 05/12/2023 04:12 WG2058011
Acenaphthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Acenaphthylene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(a)anthracene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(a)pyrene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(b)fluoranthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(g,h,i)perylene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(k)fluoranthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Chrysene ND 0.00703 1 05/12/2023 04:12 WG2058011
Dibenz(a,h)anthracene ND 0.00703 1 05/12/2023 04:12 WG2058011
Fluoranthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Fluorene ND 0.00703 1 05/12/2023 04:12 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00703 1 05/12/2023 04:12 WG2058011
Naphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
Phenanthrene ND 0.00703 1 05/12/2023 04:12 WG2058011
Pyrene ND 0.00703 1 05/12/2023 04:12 WG2058011
1-Methylnaphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
2-Methylnaphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
2-Chloronaphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
(S) p-Terphenyl-d14 86.2 23.0-120 05/12/2023 04:12 WG2058011
(S) Nitrobenzene-d5 97.0 14.0-149 05/12/2023 04:12 WG2058011
(S) 2-Fluorobiphenyl 87.8 34.0-125 05/12/2023 04:12 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055430
Total Solids by Method 2540 G-2011 L1613187-01,02,03,04,05
Method Blank (MB)
(MB) R3922359-1 05/08/23 15:55
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1613174-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1613174-05 05/08/23 15:55 • (DUP) R3922359-3 05/08/23 15:55
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 86.3 85.9 1 0.432 10
Laboratory Control Sample (LCS)
(LCS) R3922359-2 05/08/23 15:55
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055863
Total Solids by Method 2540 G-2011 L1613187-06
Method Blank (MB)
(MB) R3922349-1 05/08/23 15:17
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1613207-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1613207-01 05/08/23 15:17 • (DUP) R3922349-3 05/08/23 15:17
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 79.5 79.9 1 0.495 10
Laboratory Control Sample (LCS)
(LCS) R3922349-2 05/08/23 15:17
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2056423
Wet Chemistry by Method 7199 L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3923385-1 05/11/23 00:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1613187-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1613187-02 05/11/23 01:08 • (DUP) R3923385-3 05/11/23 01:13
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.872 20
L1613243-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1613243-02 05/11/23 02:41 • (DUP) R3923385-8 05/11/23 03:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3923385-2 05/11/23 00:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 9.33 93.3 80.0-120
L1613187-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613187-03 05/11/23 01:18 • (MS) R3923385-5 05/11/23 01:28 • (MSD) R3923385-6 05/11/23 01:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 25.9 ND 9.11 16.0 35.2 61.8 1 75.0-125 J6 J3 J6 54.7 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2056423
Wet Chemistry by Method 7199 L1613187-01,02,03,04,05,06
L1613187-03 Original Sample (OS) • Matrix Spike (MS)
(OS) L1613187-03 05/11/23 01:18 • (MS) R3923385-7 05/11/23 01:39
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 825 ND 579 70.2 50 75.0-125 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2056112
Mercury by Method 7471A L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924090-1 05/12/23 11:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3924090-2 05/12/23 11:47
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.598 120 80.0-120
L1613337-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613337-01 05/12/23 11:49 • (MS) R3924090-3 05/12/23 11:51 • (MSD) R3924090-4 05/12/23 11:53
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.504 ND 0.566 0.598 112 119 1 75.0-125 5.43 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055559
Metals (ICP) by Method 6010B L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3923333-1 05/10/23 17:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3923333-2 05/10/23 17:37
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 99.9 99.9 80.0-120
Arsenic 100 97.2 97.2 80.0-120
Beryllium 100 98.1 98.1 80.0-120
Cadmium 100 97.4 97.4 80.0-120
Chromium 100 98.8 98.8 80.0-120
Copper 100 105 105 80.0-120
Lead 100 92.9 92.9 80.0-120
Nickel 100 94.9 94.9 80.0-120
Selenium 100 102 102 80.0-120
Silver 20.0 19.8 98.9 80.0-120
Thallium 100 96.3 96.3 80.0-120
Zinc 100 96.0 96.0 80.0-120
L1613201-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613201-01 05/10/23 17:40 • (MS) R3923333-5 05/10/23 17:48 • (MSD) R3923333-6 05/10/23 17:50
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Antimony 131 ND 51.0 50.8 38.8 38.7 1 75.0-125 J6 J6 0.263 20
Arsenic 131 ND 116 117 88.1 88.5 1 75.0-125 0.522 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055559
Metals (ICP) by Method 6010B L1613187-01,02,03,04,05,06
L1613201-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613201-01 05/10/23 17:40 • (MS) R3923333-5 05/10/23 17:48 • (MSD) R3923333-6 05/10/23 17:50
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Beryllium 131 0.371 124 123 93.9 93.5 1 75.0-125 0.422 20
Cadmium 131 ND 123 122 93.8 92.8 1 75.0-125 1.03 20
Chromium 131 4.77 132 130 96.8 95.2 1 75.0-125 1.65 20
Copper 131 3.83 140 138 104 102 1 75.0-125 1.58 20
Lead 131 4.96 125 125 91.6 91.3 1 75.0-125 0.387 20
Nickel 131 ND 127 126 95.3 94.5 1 75.0-125 0.831 20
Selenium 131 ND 122 122 92.7 92.8 1 75.0-125 0.121 20
Silver 26.3 ND 25.4 25.0 96.6 95.4 1 75.0-125 1.29 20
Thallium 131 ND 121 118 92.0 89.8 1 75.0-125 2.37 20
Zinc 131 14.3 145 143 99.3 97.8 1 75.0-125 1.40 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057784
Volatile Organic Compounds (GC) by Method 8015D/GRO L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924133-2 05/11/23 02:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)92.0 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3924133-1 05/11/23 01:19
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 4.61 83.8 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 97.2 77.0-120
L1613158-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613158-01 05/11/23 11:32 • (MS) R3924133-3 05/11/23 14:37 • (MSD) R3924133-4 05/11/23 14:56
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 163 ND 135 130 81.9 78.9 25 10.0-151 3.71 28
(S)
a,a,a-Trifluorotoluene(FID) 97.5 95.6 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924032-3 05/11/23 10:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924032-3 05/11/23 10:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.000875 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 91.4 67.0-138
(S) 1,2-Dichloroethane-d4 113 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3924032-1 05/11/23 08:53 • (LCSD) R3924032-2 05/11/23 09:12
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.868 0.874 139 140 10.0-160 0.689 31
Acrylonitrile 0.625 0.650 0.668 104 107 45.0-153 2.73 22
Benzene 0.125 0.118 0.120 94.4 96.0 70.0-123 1.68 20
Bromobenzene 0.125 0.108 0.115 86.4 92.0 73.0-121 6.28 20
Bromodichloromethane 0.125 0.121 0.127 96.8 102 73.0-121 4.84 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3924032-1 05/11/23 08:53 • (LCSD) R3924032-2 05/11/23 09:12
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.108 0.111 86.4 88.8 64.0-132 2.74 20
Bromomethane 0.125 0.123 0.125 98.4 100 56.0-147 1.61 20
n-Butylbenzene 0.125 0.130 0.138 104 110 68.0-135 5.97 20
sec-Butylbenzene 0.125 0.125 0.137 100 110 74.0-130 9.16 20
tert-Butylbenzene 0.125 0.116 0.125 92.8 100 75.0-127 7.47 20
Carbon tetrachloride 0.125 0.116 0.123 92.8 98.4 66.0-128 5.86 20
Chlorobenzene 0.125 0.109 0.114 87.2 91.2 76.0-128 4.48 20
Chlorodibromomethane 0.125 0.111 0.110 88.8 88.0 74.0-127 0.905 20
Chloroethane 0.125 0.128 0.127 102 102 61.0-134 0.784 20
Chloroform 0.125 0.122 0.123 97.6 98.4 72.0-123 0.816 20
Chloromethane 0.125 0.134 0.135 107 108 51.0-138 0.743 20
2-Chlorotoluene 0.125 0.121 0.131 96.8 105 75.0-124 7.94 20
4-Chlorotoluene 0.125 0.117 0.123 93.6 98.4 75.0-124 5.00 20
1,2-Dibromo-3-Chloropropane 0.125 0.0927 0.0934 74.2 74.7 59.0-130 0.752 20
1,2-Dibromoethane 0.125 0.106 0.109 84.8 87.2 74.0-128 2.79 20
Dibromomethane 0.125 0.120 0.123 96.0 98.4 75.0-122 2.47 20
1,2-Dichlorobenzene 0.125 0.117 0.120 93.6 96.0 76.0-124 2.53 20
1,3-Dichlorobenzene 0.125 0.120 0.122 96.0 97.6 76.0-125 1.65 20
1,4-Dichlorobenzene 0.125 0.118 0.121 94.4 96.8 77.0-121 2.51 20
Dichlorodifluoromethane 0.125 0.113 0.113 90.4 90.4 43.0-156 0.000 20
1,1-Dichloroethane 0.125 0.126 0.130 101 104 70.0-127 3.12 20
1,2-Dichloroethane 0.125 0.141 0.144 113 115 65.0-131 2.11 20
1,1-Dichloroethene 0.125 0.137 0.139 110 111 65.0-131 1.45 20
cis-1,2-Dichloroethene 0.125 0.115 0.119 92.0 95.2 73.0-125 3.42 20
trans-1,2-Dichloroethene 0.125 0.114 0.117 91.2 93.6 71.0-125 2.60 20
1,2-Dichloropropane 0.125 0.121 0.123 96.8 98.4 74.0-125 1.64 20
1,1-Dichloropropene 0.125 0.123 0.126 98.4 101 73.0-125 2.41 20
1,3-Dichloropropane 0.125 0.115 0.119 92.0 95.2 80.0-125 3.42 20
cis-1,3-Dichloropropene 0.125 0.118 0.126 94.4 101 76.0-127 6.56 20
trans-1,3-Dichloropropene 0.125 0.119 0.121 95.2 96.8 73.0-127 1.67 20
2,2-Dichloropropane 0.125 0.153 0.155 122 124 59.0-135 1.30 20
Di-isopropyl ether 0.125 0.132 0.140 106 112 60.0-136 5.88 20
Ethylbenzene 0.125 0.112 0.117 89.6 93.6 74.0-126 4.37 20
Hexachloro-1,3-butadiene 0.125 0.119 0.100 95.2 80.0 57.0-150 17.4 20
Isopropylbenzene 0.125 0.119 0.126 95.2 101 72.0-127 5.71 20
p-Isopropyltoluene 0.125 0.128 0.137 102 110 72.0-133 6.79 20
2-Butanone (MEK)0.625 0.795 0.820 127 131 30.0-160 3.10 24
Methylene Chloride 0.125 0.119 0.123 95.2 98.4 68.0-123 3.31 20
4-Methyl-2-pentanone (MIBK)0.625 0.689 0.707 110 113 56.0-143 2.58 20
Methyl tert-butyl ether 0.125 0.131 0.142 105 114 66.0-132 8.06 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3924032-1 05/11/23 08:53 • (LCSD) R3924032-2 05/11/23 09:12
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0788 0.0728 63.0 58.2 59.0-130 J4 7.92 20
n-Propylbenzene 0.125 0.122 0.130 97.6 104 74.0-126 6.35 20
Styrene 0.125 0.101 0.106 80.8 84.8 72.0-127 4.83 20
1,1,1,2-Tetrachloroethane 0.125 0.117 0.120 93.6 96.0 74.0-129 2.53 20
1,1,2,2-Tetrachloroethane 0.125 0.128 0.132 102 106 68.0-128 3.08 20
1,1,2-Trichlorotrifluoroethane 0.125 0.118 0.118 94.4 94.4 61.0-139 0.000 20
Tetrachloroethene 0.125 0.114 0.115 91.2 92.0 70.0-136 0.873 20
Toluene 0.125 0.107 0.111 85.6 88.8 75.0-121 3.67 20
1,2,3-Trichlorobenzene 0.125 0.0830 0.0709 66.4 56.7 59.0-139 J4 15.7 20
1,2,4-Trichlorobenzene 0.125 0.0970 0.0858 77.6 68.6 62.0-137 12.3 20
1,1,1-Trichloroethane 0.125 0.135 0.146 108 117 69.0-126 7.83 20
1,1,2-Trichloroethane 0.125 0.108 0.112 86.4 89.6 78.0-123 3.64 20
Trichloroethene 0.125 0.115 0.119 92.0 95.2 76.0-126 3.42 20
Trichlorofluoromethane 0.125 0.151 0.145 121 116 61.0-142 4.05 20
1,2,3-Trichloropropane 0.125 0.125 0.122 100 97.6 67.0-129 2.43 20
1,2,4-Trimethylbenzene 0.125 0.125 0.132 100 106 70.0-126 5.45 20
1,2,3-Trimethylbenzene 0.125 0.125 0.132 100 106 74.0-124 5.45 20
1,3,5-Trimethylbenzene 0.125 0.125 0.132 100 106 73.0-127 5.45 20
Vinyl chloride 0.125 0.136 0.138 109 110 63.0-134 1.46 20
Xylenes, Total 0.375 0.335 0.342 89.3 91.2 72.0-127 2.07 20
(S) Toluene-d8 99.1 101 75.0-131
(S) 4-Bromofluorobenzene 100 99.3 67.0-138
(S) 1,2-Dichloroethane-d4 125 126 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059338
Semi-Volatile Organic Compounds (GC) by Method 8015 L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924747-1 05/13/23 23:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 40.5 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3924747-2 05/13/23 23:36
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 31.7 63.4 50.0-150
(S) o-Terphenyl 69.1 18.0-148
L1613819-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613819-01 05/15/23 13:47 • (MS) R3924994-1 05/15/23 14:00 • (MSD) R3924994-2 05/15/23 14:13
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 50.0 417 268 627 0.000 423 5 50.0-150 V J3 V 80.2 20
(S) o-Terphenyl 58.4 43.2 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057922
Polychlorinated Biphenyls (GC) by Method 8082 L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3925516-1 05/13/23 17:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 113 10.0-135
(S) Tetrachloro-m-xylene 107 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3925516-2 05/13/23 17:17
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.134 80.2 36.0-141
PCB 1260 0.167 0.146 87.4 37.0-145
(S) Decachlorobiphenyl 88.9 10.0-135
(S) Tetrachloro-m-xylene 95.8 10.0-139
L1613023-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613023-21 05/14/23 22:25 • (MS) R3925569-1 05/14/23 22:57 • (MSD) R3925569-2 05/14/23 23:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.174 ND 0.184 0.174 105 100 1 10.0-160 5.25 37
PCB 1260 0.174 ND 0.201 0.210 116 120 1 10.0-160 4.06 38
(S) Decachlorobiphenyl 123 128 10.0-135
(S) Tetrachloro-m-xylene 115 118 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924305-2 05/12/23 14:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924305-2 05/12/23 14:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 64.6 10.0-122
(S) 2-Fluorobiphenyl 60.4 15.0-120
(S) p-Terphenyl-d14 61.3 10.0-120
(S) Phenol-d5 58.7 10.0-120
(S) 2-Fluorophenol 67.9 12.0-120
(S) 2,4,6-Tribromophenol 53.6 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3924305-1 05/12/23 14:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.420 63.1 38.0-120
Acenaphthylene 0.666 0.450 67.6 40.0-120
Anthracene 0.666 0.475 71.3 42.0-120
Benzidine 1.33 0.383 28.8 10.0-120
Benzo(a)anthracene 0.666 0.490 73.6 44.0-120
Benzo(b)fluoranthene 0.666 0.446 67.0 43.0-120
Benzo(k)fluoranthene 0.666 0.427 64.1 44.0-120
Benzo(g,h,i)perylene 0.666 0.465 69.8 43.0-120
Benzo(a)pyrene 0.666 0.504 75.7 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.358 53.8 20.0-120
Bis(2-chloroethyl)ether 0.666 0.414 62.2 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.360 54.1 23.0-120
4-Bromophenyl-phenylether 0.666 0.402 60.4 40.0-120
2-Chloronaphthalene 0.666 0.424 63.7 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3924305-1 05/12/23 14:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.420 63.1 40.0-120
Chrysene 0.666 0.450 67.6 43.0-120
Dibenz(a,h)anthracene 0.666 0.471 70.7 44.0-120
3,3-Dichlorobenzidine 1.33 0.895 67.3 28.0-120
2,4-Dinitrotoluene 0.666 0.509 76.4 45.0-120
2,6-Dinitrotoluene 0.666 0.439 65.9 42.0-120
Fluoranthene 0.666 0.456 68.5 44.0-120
Fluorene 0.666 0.427 64.1 41.0-120
Hexachlorobenzene 0.666 0.390 58.6 39.0-120
Hexachloro-1,3-butadiene 0.666 0.386 58.0 15.0-120
Hexachlorocyclopentadiene 0.666 0.456 68.5 15.0-120
Hexachloroethane 0.666 0.418 62.8 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.445 66.8 45.0-120
Isophorone 0.666 0.375 56.3 23.0-120
Naphthalene 0.666 0.354 53.2 18.0-120
Nitrobenzene 0.666 0.385 57.8 17.0-120
n-Nitrosodimethylamine 0.666 0.452 67.9 10.0-125
n-Nitrosodiphenylamine 0.666 0.445 66.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.400 60.1 26.0-120
Phenanthrene 0.666 0.449 67.4 42.0-120
Benzylbutyl phthalate 0.666 0.528 79.3 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.520 78.1 41.0-120
Di-n-butyl phthalate 0.666 0.522 78.4 43.0-120
Diethyl phthalate 0.666 0.521 78.2 43.0-120
Dimethyl phthalate 0.666 0.477 71.6 43.0-120
Di-n-octyl phthalate 0.666 0.512 76.9 40.0-120
Pyrene 0.666 0.421 63.2 41.0-120
1,2,4-Trichlorobenzene 0.666 0.353 53.0 17.0-120
4-Chloro-3-methylphenol 0.666 0.438 65.8 28.0-120
2-Chlorophenol 0.666 0.409 61.4 28.0-120
2,4-Dichlorophenol 0.666 0.394 59.2 25.0-120
2,4-Dimethylphenol 0.666 0.428 64.3 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.531 79.7 16.0-120
2,4-Dinitrophenol 0.666 0.381 57.2 10.0-120
2-Nitrophenol 0.666 0.411 61.7 20.0-120
4-Nitrophenol 0.666 0.343 51.5 27.0-120
Pentachlorophenol 0.666 0.474 71.2 29.0-120
Phenol 0.666 0.408 61.3 28.0-120
2,4,6-Trichlorophenol 0.666 0.429 64.4 37.0-120
(S) Nitrobenzene-d5 57.1 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3924305-1 05/12/23 14:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 64.3 15.0-120
(S) p-Terphenyl-d14 67.3 10.0-120
(S) Phenol-d5 64.7 10.0-120
(S) 2-Fluorophenol 72.5 12.0-120
(S) 2,4,6-Tribromophenol 62.9 10.0-127
L1613366-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613366-02 05/17/23 11:29 • (MS) R3926121-1 05/17/23 11:49 • (MSD) R3926121-2 05/17/23 12:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.659 ND 0.354 0.391 53.7 58.7 10 18.0-120 9.87 32
Acenaphthylene 0.659 ND ND ND 49.7 50.8 10 25.0-120 3.15 32
Anthracene 0.659 ND 0.375 0.461 56.8 69.2 10 22.0-120 20.6 29
Benzidine 1.32 ND ND ND 74.0 75.9 10 10.0-120 3.27 40
Benzo(a)anthracene 0.659 ND 0.413 0.595 62.6 89.4 10 25.0-120 J3 36.2 29
Benzo(b)fluoranthene 0.659 ND 0.377 0.572 57.2 86.0 10 19.0-122 J3 41.2 31
Benzo(k)fluoranthene 0.659 ND 0.351 0.463 53.2 69.6 10 23.0-120 27.6 30
Benzo(g,h,i)perylene 0.659 ND 0.406 0.478 61.6 71.8 10 10.0-120 16.2 33
Benzo(a)pyrene 0.659 ND 0.380 0.540 57.6 81.1 10 24.0-120 J3 34.7 30
Bis(2-chlorethoxy)methane 0.659 ND ND ND 44.9 52.1 10 10.0-120 15.7 34
Bis(2-chloroethyl)ether 0.659 ND ND ND 41.2 56.6 10 10.0-120 32.4 40
2,2-Oxybis(1-Chloropropane)0.659 ND ND ND 47.3 50.8 10 10.0-120 8.08 40
4-Bromophenyl-phenylether 0.659 ND ND ND 46.7 50.8 10 27.0-120 9.43 30
2-Chloronaphthalene 0.659 ND ND ND 50.5 50.0 10 20.0-120 0.000 32
4-Chlorophenyl-phenylether 0.659 ND ND ND 51.0 50.5 10 24.0-120 0.000 29
Chrysene 0.659 ND 0.413 0.589 62.6 88.5 10 21.0-120 J3 35.2 29
Dibenz(a,h)anthracene 0.659 ND 0.351 0.405 53.2 60.9 10 10.0-120 14.4 32
3,3-Dichlorobenzidine 1.32 ND ND ND 52.7 54.6 10 10.0-120 4.27 34
2,4-Dinitrotoluene 0.659 ND ND ND 49.5 52.5 10 30.0-120 6.83 31
2,6-Dinitrotoluene 0.659 ND ND ND 48.1 52.4 10 25.0-120 9.46 31
Fluoranthene 0.659 ND 0.395 0.819 59.9 123 10 18.0-126 J3 69.9 32
Fluorene 0.659 ND 0.350 0.390 53.0 58.5 10 25.0-120 10.8 30
Hexachlorobenzene 0.659 ND ND ND 47.6 48.4 10 27.0-120 2.64 28
Hexachloro-1,3-butadiene 0.659 ND ND ND 41.9 42.7 10 10.0-120 3.00 38
Hexachlorocyclopentadiene 0.659 ND ND ND 25.2 2.48 10 10.0-120 J3 J6 164 40
Hexachloroethane 0.659 ND ND ND 40.8 46.1 10 10.0-120 13.1 40
Indeno(1,2,3-cd)pyrene 0.659 ND 0.370 0.481 56.1 72.2 10 10.0-120 26.2 32
Isophorone 0.659 ND ND ND 41.7 44.6 10 13.0-120 7.71 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
L1613366-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613366-02 05/17/23 11:29 • (MS) R3926121-1 05/17/23 11:49 • (MSD) R3926121-2 05/17/23 12:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.659 ND ND 0.362 49.2 54.4 10 10.0-120 11.0 35
Nitrobenzene 0.659 ND ND ND 46.3 49.1 10 10.0-120 6.64 36
n-Nitrosodimethylamine 0.659 ND ND ND 0.000 0.000 10 10.0-127 J6 J6 0.000 40
n-Nitrosodiphenylamine 0.659 ND ND ND 57.5 55.8 10 17.0-120 1.96 29
n-Nitrosodi-n-propylamine 0.659 ND ND ND 44.1 44.0 10 10.0-120 0.719 37
Phenanthrene 0.659 ND 0.385 0.657 58.4 98.7 10 17.0-120 J3 52.2 31
Benzylbutyl phthalate 0.659 ND ND ND 65.6 67.2 10 23.0-120 3.34 30
Bis(2-ethylhexyl)phthalate 0.659 ND ND ND 68.6 72.4 10 17.0-126 6.29 30
Di-n-butyl phthalate 0.659 ND ND ND 54.9 55.4 10 30.0-120 1.72 29
Diethyl phthalate 0.659 ND ND ND 56.2 55.4 10 26.0-120 0.568 28
Dimethyl phthalate 0.628 ND ND ND 0.000 0.000 10 25.0-120 J6 J6 0.000 29
Di-n-octyl phthalate 0.659 ND ND ND 59.1 54.6 10 21.0-123 6.97 29
Pyrene 0.659 ND 0.425 0.728 64.5 109 10 16.0-121 J3 52.5 32
1,2,4-Trichlorobenzene 0.659 ND ND ND 45.9 45.4 10 12.0-120 0.000 37
4-Chloro-3-methylphenol 0.659 ND ND ND 52.4 56.5 10 15.0-120 8.44 30
2-Chlorophenol 0.659 ND ND ND 43.3 49.1 10 15.0-120 13.4 37
2,4-Dichlorophenol 0.659 ND ND ND 44.9 50.2 10 20.0-120 12.0 31
2,4-Dimethylphenol 0.659 ND ND ND 63.4 59.8 10 10.0-120 4.89 33
4,6-Dinitro-2-methylphenol 0.628 ND ND ND 172 166 10 10.0-120 J5 J5 2.82 39
2,4-Dinitrophenol 0.628 ND ND ND 0.000 0.000 10 10.0-121 J6 J6 0.000 40
2-Nitrophenol 0.659 ND ND ND 54.3 56.5 10 12.0-120 4.86 39
4-Nitrophenol 0.659 ND ND ND 42.8 43.5 10 10.0-137 2.57 32
Pentachlorophenol 0.659 ND ND ND 41.4 45.0 10 10.0-160 9.17 31
Phenol 0.659 ND ND ND 46.0 49.7 10 12.0-120 8.61 38
2,4,6-Trichlorophenol 0.659 ND ND ND 47.0 42.4 10 19.0-120 9.22 32
(S) Nitrobenzene-d5 47.8 50.2 10.0-122
(S) 2-Fluorobiphenyl 50.0 50.8 15.0-120
(S) p-Terphenyl-d14 58.6 59.0 10.0-120
(S) Phenol-d5 48.7 49.7 10.0-120
(S) 2-Fluorophenol 54.0 55.0 12.0-120
(S) 2,4,6-Tribromophenol 47.8 49.5 10.0-127
Sample Narrative:
OS: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058011
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924098-2 05/12/23 01:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 105 23.0-120
(S) Nitrobenzene-d5 81.1 14.0-149
(S) 2-Fluorobiphenyl 85.6 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3924098-1 05/12/23 01:19
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0760 95.0 50.0-126
Acenaphthene 0.0800 0.0663 82.9 50.0-120
Acenaphthylene 0.0800 0.0737 92.1 50.0-120
Benzo(a)anthracene 0.0800 0.0774 96.8 45.0-120
Benzo(a)pyrene 0.0800 0.0714 89.3 42.0-120
Benzo(b)fluoranthene 0.0800 0.0743 92.9 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0692 86.5 45.0-125
Benzo(k)fluoranthene 0.0800 0.0723 90.4 49.0-125
Chrysene 0.0800 0.0832 104 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0731 91.4 47.0-125
Fluoranthene 0.0800 0.0844 105 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058011
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3924098-1 05/12/23 01:19
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0791 98.9 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0812 102 46.0-125
Naphthalene 0.0800 0.0694 86.8 50.0-120
Phenanthrene 0.0800 0.0795 99.4 47.0-120
Pyrene 0.0800 0.0817 102 43.0-123
1-Methylnaphthalene 0.0800 0.0759 94.9 51.0-121
2-Methylnaphthalene 0.0800 0.0715 89.4 50.0-120
2-Chloronaphthalene 0.0800 0.0725 90.6 50.0-120
(S) p-Terphenyl-d14 112 23.0-120
(S) Nitrobenzene-d5 111 14.0-149
(S) 2-Fluorobiphenyl 106 34.0-125
L1613258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613258-01 05/12/23 05:39 • (MS) R3924098-3 05/12/23 05:56 • (MSD) R3924098-4 05/12/23 06:13
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0760 ND 0.0634 0.0613 83.4 80.2 1 10.0-145 3.37 30
Acenaphthene 0.0760 ND 0.0544 0.0535 71.6 70.0 1 14.0-127 1.67 27
Acenaphthylene 0.0760 ND 0.0595 0.0594 78.3 77.7 1 21.0-124 0.168 25
Benzo(a)anthracene 0.0760 ND 0.0652 0.0613 85.8 80.2 1 10.0-139 6.17 30
Benzo(a)pyrene 0.0760 ND 0.0646 0.0619 85.0 81.0 1 10.0-141 4.27 31
Benzo(b)fluoranthene 0.0760 ND 0.0620 0.0574 81.6 75.1 1 10.0-140 7.71 36
Benzo(g,h,i)perylene 0.0760 ND 0.0576 0.0543 75.8 71.1 1 10.0-140 5.90 33
Benzo(k)fluoranthene 0.0760 ND 0.0601 0.0582 79.1 76.2 1 10.0-137 3.21 31
Chrysene 0.0760 ND 0.0691 0.0692 90.9 90.6 1 10.0-145 0.145 30
Dibenz(a,h)anthracene 0.0760 ND 0.0614 0.0595 80.8 77.9 1 10.0-132 3.14 31
Fluoranthene 0.0760 ND 0.0699 0.0667 92.0 87.3 1 10.0-153 4.69 33
Fluorene 0.0760 ND 0.0671 0.0658 88.3 86.1 1 11.0-130 1.96 29
Indeno(1,2,3-cd)pyrene 0.0760 ND 0.0635 0.0596 83.6 78.0 1 10.0-137 6.34 32
Naphthalene 0.0760 ND 0.0536 0.0554 70.5 72.5 1 10.0-135 3.30 27
Phenanthrene 0.0760 ND 0.0672 0.0652 88.4 85.3 1 10.0-144 3.02 31
Pyrene 0.0760 ND 0.0691 0.0656 90.9 85.9 1 10.0-148 5.20 35
1-Methylnaphthalene 0.0760 ND 0.0597 0.0609 78.6 79.7 1 10.0-142 1.99 28
2-Methylnaphthalene 0.0760 ND 0.0576 0.0584 75.8 76.4 1 10.0-137 1.38 28
2-Chloronaphthalene 0.0760 ND 0.0602 0.0606 79.2 79.3 1 29.0-120 0.662 24
(S) p-Terphenyl-d14 97.0 89.2 23.0-120
(S) Nitrobenzene-d5 96.6 99.4 14.0-149
(S) 2-Fluorobiphenyl 91.9 88.8 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
May 20, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1614172
Samples Received:05/09/2023
Project Number:
Description:
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
May 20, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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May 22, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
CS-1 L1614172-01 6
CS-2 L1614172-02 10
CS-3 L1614172-03 14
CS-4 L1614172-04 18
CS-5 L1614172-05 22
Qc: Quality Control Summary 26
Total Solids by Method 2540 G-2011 26
Wet Chemistry by Method 7199 27
Mercury by Method 7471A 28
Metals (ICP) by Method 6010B 30
Volatile Organic Compounds (GC) by Method 8015D/GRO 32
Volatile Organic Compounds (GC/MS) by Method 8260B 34
Semi-Volatile Organic Compounds (GC) by Method 8015 44
Polychlorinated Biphenyls (GC) by Method 8082 45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 47
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 52
Gl: Glossary of Terms 58
Al: Accreditations & Locations 59
Sc: Sample Chain of Custody 60
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CS-1 L1614172-01 Solid RT 05/08/23 09:30 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 14:44 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:33 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:37 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2062511 25 05/08/23 09:30 05/18/23 18:10 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059471 1 05/08/23 09:30 05/13/23 20:10 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 20:46 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 02:07 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/14/23 00:24 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2062088 1 05/18/23 10:23 05/18/23 17:10 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-2 L1614172-02 Solid RT 05/08/23 09:35 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 14:49 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:35 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:40 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 28 05/08/23 09:35 05/14/23 05:06 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1.12 05/08/23 09:35 05/14/23 11:08 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 23:22 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 03:16 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/14/23 02:33 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059490 1 05/16/23 16:27 05/17/23 06:19 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-3 L1614172-03 Solid RT 05/08/23 09:40 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 14:55 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:37 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:43 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 25 05/08/23 09:40 05/14/23 05:26 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1 05/08/23 09:40 05/14/23 11:27 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 20:59 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 02:17 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/13/23 22:15 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059490 1 05/16/23 16:27 05/17/23 06:37 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-4 L1614172-04 Solid RT 05/08/23 09:45 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 15:00 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:39 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:46 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 25 05/08/23 09:45 05/14/23 05:47 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1 05/08/23 09:45 05/14/23 11:46 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/18/23 09:47 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 02:27 HMH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CS-4 L1614172-04 Solid RT 05/08/23 09:45 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/13/23 22:36 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059490 1 05/16/23 16:27 05/17/23 18:16 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-5 L1614172-05 Solid RT 05/08/23 09:50 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 15:05 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057613 1 05/15/23 11:04 05/18/23 16:56 AKB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:49 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 26 05/08/23 09:50 05/14/23 06:07 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1.04 05/08/23 09:50 05/14/23 12:04 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 22:56 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059034 1 05/14/23 16:44 05/15/23 01:50 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/14/23 00:45 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059491 1 05/15/23 09:10 05/15/23 19:10 AMG Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.2 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.30 1 05/13/2023 14:44 WG2057052
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0518 1 05/12/2023 11:33 WG2057615
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.59 1 05/11/2023 21:37 WG2057224
Arsenic 3.22 2.59 1 05/11/2023 21:37 WG2057224
Beryllium 0.334 0.259 1 05/11/2023 21:37 WG2057224
Cadmium ND 0.648 1 05/11/2023 21:37 WG2057224
Chromium 8.47 1.30 1 05/11/2023 21:37 WG2057224
Copper 7.97 2.59 1 05/11/2023 21:37 WG2057224
Lead 3.28 0.648 1 05/11/2023 21:37 WG2057224
Nickel 6.19 2.59 1 05/11/2023 21:37 WG2057224
Selenium ND 2.59 1 05/11/2023 21:37 WG2057224
Silver ND 1.30 1 05/11/2023 21:37 WG2057224
Thallium ND 2.59 1 05/11/2023 21:37 WG2057224
Zinc 24.6 6.48 1 05/11/2023 21:37 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.00 25 05/18/2023 18:10 WG2062511
(S) a,a,a-Trifluorotoluene(FID)92.8 77.0-120 05/18/2023 18:10 WG2062511
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0799 1 05/13/2023 20:10 WG2059471
Acrylonitrile ND 0.0200 1 05/13/2023 20:10 WG2059471
Benzene ND 0.00160 1 05/13/2023 20:10 WG2059471
Bromobenzene ND 0.0200 1 05/13/2023 20:10 WG2059471
Bromodichloromethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Bromoform ND 0.0400 1 05/13/2023 20:10 WG2059471
Bromomethane ND 0.0200 1 05/13/2023 20:10 WG2059471
n-Butylbenzene ND 0.0200 1 05/13/2023 20:10 WG2059471
sec-Butylbenzene ND 0.0200 1 05/13/2023 20:10 WG2059471
tert-Butylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Carbon tetrachloride ND 0.00799 1 05/13/2023 20:10 WG2059471
Chlorobenzene ND 0.00400 1 05/13/2023 20:10 WG2059471
Chlorodibromomethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Chloroethane ND 0.00799 1 05/13/2023 20:10 WG2059471
Chloroform ND 0.00400 1 05/13/2023 20:10 WG2059471
Chloromethane ND 0.0200 1 05/13/2023 20:10 WG2059471
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00400 1 05/13/2023 20:10 WG2059471
4-Chlorotoluene ND J4 0.00799 1 05/13/2023 20:10 WG2059471
1,2-Dibromo-3-Chloropropane ND 0.0400 1 05/13/2023 20:10 WG2059471
1,2-Dibromoethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Dibromomethane ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2-Dichlorobenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,3-Dichlorobenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,4-Dichlorobenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Dichlorodifluoromethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1-Dichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,2-Dichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1-Dichloroethene ND 0.00400 1 05/13/2023 20:10 WG2059471
cis-1,2-Dichloroethene ND 0.00400 1 05/13/2023 20:10 WG2059471
trans-1,2-Dichloroethene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2-Dichloropropane ND 0.00799 1 05/13/2023 20:10 WG2059471
1,1-Dichloropropene ND 0.00400 1 05/13/2023 20:10 WG2059471
1,3-Dichloropropane ND 0.00799 1 05/13/2023 20:10 WG2059471
cis-1,3-Dichloropropene ND 0.00400 1 05/13/2023 20:10 WG2059471
trans-1,3-Dichloropropene ND 0.00799 1 05/13/2023 20:10 WG2059471
2,2-Dichloropropane ND 0.00400 1 05/13/2023 20:10 WG2059471
Di-isopropyl ether ND 0.00160 1 05/13/2023 20:10 WG2059471
Ethylbenzene ND 0.00400 1 05/13/2023 20:10 WG2059471
Hexachloro-1,3-butadiene ND 0.0400 1 05/13/2023 20:10 WG2059471
Isopropylbenzene ND 0.00400 1 05/13/2023 20:10 WG2059471
p-Isopropyltoluene ND 0.00799 1 05/13/2023 20:10 WG2059471
2-Butanone (MEK)ND 0.160 1 05/13/2023 20:10 WG2059471
Methylene Chloride ND 0.0400 1 05/13/2023 20:10 WG2059471
4-Methyl-2-pentanone (MIBK)ND 0.0400 1 05/13/2023 20:10 WG2059471
Methyl tert-butyl ether ND 0.00160 1 05/13/2023 20:10 WG2059471
Naphthalene ND J3 0.0200 1 05/13/2023 20:10 WG2059471
n-Propylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Styrene ND 0.0200 1 05/13/2023 20:10 WG2059471
1,1,1,2-Tetrachloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1,2,2-Tetrachloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1,2-Trichlorotrifluoroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Tetrachloroethene ND 0.00400 1 05/13/2023 20:10 WG2059471
Toluene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2,3-Trichlorobenzene ND J3 0.0200 1 05/13/2023 20:10 WG2059471
1,2,4-Trichlorobenzene ND J3 0.0200 1 05/13/2023 20:10 WG2059471
1,1,1-Trichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1,2-Trichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Trichloroethene ND 0.00160 1 05/13/2023 20:10 WG2059471
Trichlorofluoromethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,2,3-Trichloropropane ND 0.0200 1 05/13/2023 20:10 WG2059471
1,2,4-Trimethylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2,3-Trimethylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,3,5-Trimethylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Vinyl chloride ND 0.00400 1 05/13/2023 20:10 WG2059471
Xylenes, Total ND 0.0104 1 05/13/2023 20:10 WG2059471
(S) Toluene-d8 107 75.0-131 05/13/2023 20:10 WG2059471
(S) 4-Bromofluorobenzene 95.3 67.0-138 05/13/2023 20:10 WG2059471
(S) 1,2-Dichloroethane-d4 96.7 70.0-130 05/13/2023 20:10 WG2059471
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.18 1 05/17/2023 20:46 WG2061264
C28-C40 Oil Range ND 5.18 1 05/17/2023 20:46 WG2061264
(S) o-Terphenyl 33.8 18.0-148 05/17/2023 20:46 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1221 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1232 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1242 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1248 ND 0.0220 1 05/15/2023 02:07 WG2059033
PCB 1254 ND 0.0220 1 05/15/2023 02:07 WG2059033
PCB 1260 ND 0.0220 1 05/15/2023 02:07 WG2059033
(S) Decachlorobiphenyl 70.1 10.0-135 05/15/2023 02:07 WG2059033
(S) Tetrachloro-m-xylene 64.0 10.0-139 05/15/2023 02:07 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Acenaphthylene ND 0.0431 1 05/14/2023 00:24 WG2059348
Anthracene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzidine ND 2.16 1 05/14/2023 00:24 WG2059348
Benzo(a)anthracene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(b)fluoranthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(k)fluoranthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(g,h,i)perylene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(a)pyrene ND 0.0431 1 05/14/2023 00:24 WG2059348
Bis(2-chlorethoxy)methane ND 0.431 1 05/14/2023 00:24 WG2059348
Bis(2-chloroethyl)ether ND 0.431 1 05/14/2023 00:24 WG2059348
2,2-Oxybis(1-Chloropropane)ND 0.431 1 05/14/2023 00:24 WG2059348
4-Bromophenyl-phenylether ND 0.431 1 05/14/2023 00:24 WG2059348
2-Chloronaphthalene ND 0.0431 1 05/14/2023 00:24 WG2059348
4-Chlorophenyl-phenylether ND 0.431 1 05/14/2023 00:24 WG2059348
Chrysene ND 0.0431 1 05/14/2023 00:24 WG2059348
Dibenz(a,h)anthracene ND 0.0431 1 05/14/2023 00:24 WG2059348
3,3-Dichlorobenzidine ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dinitrotoluene ND 0.431 1 05/14/2023 00:24 WG2059348
2,6-Dinitrotoluene ND 0.431 1 05/14/2023 00:24 WG2059348
Fluoranthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Fluorene ND 0.0431 1 05/14/2023 00:24 WG2059348
Hexachlorobenzene ND 0.431 1 05/14/2023 00:24 WG2059348
Hexachloro-1,3-butadiene ND 0.431 1 05/14/2023 00:24 WG2059348
Hexachlorocyclopentadiene ND 0.431 1 05/14/2023 00:24 WG2059348
Hexachloroethane ND 0.431 1 05/14/2023 00:24 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0431 1 05/14/2023 00:24 WG2059348
Isophorone ND 0.431 1 05/14/2023 00:24 WG2059348
Naphthalene ND 0.0431 1 05/14/2023 00:24 WG2059348
Nitrobenzene ND 0.431 1 05/14/2023 00:24 WG2059348
n-Nitrosodimethylamine ND 0.431 1 05/14/2023 00:24 WG2059348
n-Nitrosodiphenylamine ND 0.431 1 05/14/2023 00:24 WG2059348
n-Nitrosodi-n-propylamine ND 0.431 1 05/14/2023 00:24 WG2059348
Phenanthrene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzylbutyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Di-n-butyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Diethyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Dimethyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Di-n-octyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Pyrene ND 0.0431 1 05/14/2023 00:24 WG2059348
1,2,4-Trichlorobenzene ND 0.431 1 05/14/2023 00:24 WG2059348
4-Chloro-3-methylphenol ND 0.431 1 05/14/2023 00:24 WG2059348
2-Chlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dichlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dimethylphenol ND 0.431 1 05/14/2023 00:24 WG2059348
4,6-Dinitro-2-methylphenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dinitrophenol ND 0.431 1 05/14/2023 00:24 WG2059348
2-Nitrophenol ND 0.431 1 05/14/2023 00:24 WG2059348
4-Nitrophenol ND 0.431 1 05/14/2023 00:24 WG2059348
Pentachlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
Phenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4,6-Trichlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
(S) Nitrobenzene-d5 42.9 10.0-122 05/14/2023 00:24 WG2059348
(S) 2-Fluorobiphenyl 48.9 15.0-120 05/14/2023 00:24 WG2059348
(S) p-Terphenyl-d14 58.1 10.0-120 05/14/2023 00:24 WG2059348
(S) Phenol-d5 43.8 10.0-120 05/14/2023 00:24 WG2059348
(S) 2-Fluorophenol 49.5 12.0-120 05/14/2023 00:24 WG2059348
(S) 2,4,6-Tribromophenol 55.3 10.0-127 05/14/2023 00:24 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00777 1 05/18/2023 17:10 WG2062088
Acenaphthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Acenaphthylene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(a)anthracene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(a)pyrene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(b)fluoranthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(g,h,i)perylene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(k)fluoranthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Chrysene ND 0.00777 1 05/18/2023 17:10 WG2062088
Dibenz(a,h)anthracene ND 0.00777 1 05/18/2023 17:10 WG2062088
Fluoranthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Fluorene ND 0.00777 1 05/18/2023 17:10 WG2062088
Indeno(1,2,3-cd)pyrene ND 0.00777 1 05/18/2023 17:10 WG2062088
Naphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
Phenanthrene ND 0.00777 1 05/18/2023 17:10 WG2062088
Pyrene ND 0.00777 1 05/18/2023 17:10 WG2062088
1-Methylnaphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
2-Methylnaphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
2-Chloronaphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
(S) p-Terphenyl-d14 92.6 23.0-120 05/18/2023 17:10 WG2062088
(S) Nitrobenzene-d5 93.8 14.0-149 05/18/2023 17:10 WG2062088
(S) 2-Fluorobiphenyl 91.8 34.0-125 05/18/2023 17:10 WG2062088
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.0 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.22 1 05/13/2023 14:49 WG2057052
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0488 1 05/12/2023 11:35 WG2057615
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.44 1 05/11/2023 21:40 WG2057224
Arsenic 3.37 2.44 1 05/11/2023 21:40 WG2057224
Beryllium 0.266 0.244 1 05/11/2023 21:40 WG2057224
Cadmium ND 0.610 1 05/11/2023 21:40 WG2057224
Chromium 14.6 1.22 1 05/11/2023 21:40 WG2057224
Copper 13.9 2.44 1 05/11/2023 21:40 WG2057224
Lead 4.12 0.610 1 05/11/2023 21:40 WG2057224
Nickel 7.79 2.44 1 05/11/2023 21:40 WG2057224
Selenium ND 2.44 1 05/11/2023 21:40 WG2057224
Silver ND 1.22 1 05/11/2023 21:40 WG2057224
Thallium ND 2.44 1 05/11/2023 21:40 WG2057224
Zinc 22.6 6.10 1 05/11/2023 21:40 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.96 28 05/14/2023 05:06 WG2059653
(S) a,a,a-Trifluorotoluene(FID)93.6 77.0-120 05/14/2023 05:06 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0793 1.12 05/14/2023 11:08 WG2059688
Acrylonitrile ND 0.0198 1.12 05/14/2023 11:08 WG2059688
Benzene ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Bromobenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
Bromodichloromethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Bromoform ND 0.0396 1.12 05/14/2023 11:08 WG2059688
Bromomethane ND 0.0198 1.12 05/14/2023 11:08 WG2059688
n-Butylbenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
sec-Butylbenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
tert-Butylbenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Carbon tetrachloride ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Chlorobenzene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Chlorodibromomethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Chloroethane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Chloroform ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Chloromethane ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
4-Chlorotoluene ND J4 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0396 1.12 05/14/2023 11:08 WG2059688
1,2-Dibromoethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Dibromomethane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2-Dichlorobenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,3-Dichlorobenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,4-Dichlorobenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Dichlorodifluoromethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1-Dichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,2-Dichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1-Dichloroethene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
cis-1,2-Dichloroethene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
trans-1,2-Dichloroethene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2-Dichloropropane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,1-Dichloropropene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,3-Dichloropropane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
cis-1,3-Dichloropropene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
trans-1,3-Dichloropropene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
2,2-Dichloropropane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Di-isopropyl ether ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Ethylbenzene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Hexachloro-1,3-butadiene ND 0.0396 1.12 05/14/2023 11:08 WG2059688
Isopropylbenzene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
p-Isopropyltoluene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
2-Butanone (MEK)ND 0.159 1.12 05/14/2023 11:08 WG2059688
Methylene Chloride ND 0.0396 1.12 05/14/2023 11:08 WG2059688
4-Methyl-2-pentanone (MIBK)ND 0.0396 1.12 05/14/2023 11:08 WG2059688
Methyl tert-butyl ether ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Naphthalene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
n-Propylbenzene ND J4 0.00793 1.12 05/14/2023 11:08 WG2059688
Styrene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Tetrachloroethene 0.00883 0.00396 1.12 05/14/2023 11:08 WG2059688
Toluene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2,3-Trichlorobenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,2,4-Trichlorobenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,1,1-Trichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1,2-Trichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Trichloroethene ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Trichlorofluoromethane ND J4 0.00396 1.12 05/14/2023 11:08 WG2059688
1,2,3-Trichloropropane ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2,3-Trimethylbenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,3,5-Trimethylbenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Vinyl chloride ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Xylenes, Total ND 0.0103 1.12 05/14/2023 11:08 WG2059688
(S) Toluene-d8 107 75.0-131 05/14/2023 11:08 WG2059688
(S) 4-Bromofluorobenzene 102 67.0-138 05/14/2023 11:08 WG2059688
(S) 1,2-Dichloroethane-d4 101 70.0-130 05/14/2023 11:08 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 16.0 4.88 1 05/17/2023 23:22 WG2061264
C28-C40 Oil Range 41.5 4.88 1 05/17/2023 23:22 WG2061264
(S) o-Terphenyl 39.5 18.0-148 05/17/2023 23:22 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1221 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1232 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1242 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1248 ND 0.0207 1 05/15/2023 03:16 WG2059033
PCB 1254 ND 0.0207 1 05/15/2023 03:16 WG2059033
PCB 1260 ND 0.0207 1 05/15/2023 03:16 WG2059033
(S) Decachlorobiphenyl 57.0 10.0-135 05/15/2023 03:16 WG2059033
(S) Tetrachloro-m-xylene 51.9 10.0-139 05/15/2023 03:16 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Acenaphthylene ND 0.0406 1 05/14/2023 02:33 WG2059348
Anthracene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzidine ND 2.04 1 05/14/2023 02:33 WG2059348
Benzo(a)anthracene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(b)fluoranthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(k)fluoranthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(g,h,i)perylene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(a)pyrene ND 0.0406 1 05/14/2023 02:33 WG2059348
Bis(2-chlorethoxy)methane ND 0.406 1 05/14/2023 02:33 WG2059348
Bis(2-chloroethyl)ether ND 0.406 1 05/14/2023 02:33 WG2059348
2,2-Oxybis(1-Chloropropane)ND 0.406 1 05/14/2023 02:33 WG2059348
4-Bromophenyl-phenylether ND 0.406 1 05/14/2023 02:33 WG2059348
2-Chloronaphthalene ND 0.0406 1 05/14/2023 02:33 WG2059348
4-Chlorophenyl-phenylether ND 0.406 1 05/14/2023 02:33 WG2059348
Chrysene ND 0.0406 1 05/14/2023 02:33 WG2059348
Dibenz(a,h)anthracene ND 0.0406 1 05/14/2023 02:33 WG2059348
3,3-Dichlorobenzidine ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dinitrotoluene ND 0.406 1 05/14/2023 02:33 WG2059348
2,6-Dinitrotoluene ND 0.406 1 05/14/2023 02:33 WG2059348
Fluoranthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Fluorene ND 0.0406 1 05/14/2023 02:33 WG2059348
Hexachlorobenzene ND 0.406 1 05/14/2023 02:33 WG2059348
Hexachloro-1,3-butadiene ND 0.406 1 05/14/2023 02:33 WG2059348
Hexachlorocyclopentadiene ND 0.406 1 05/14/2023 02:33 WG2059348
Hexachloroethane ND 0.406 1 05/14/2023 02:33 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0406 1 05/14/2023 02:33 WG2059348
Isophorone ND 0.406 1 05/14/2023 02:33 WG2059348
Naphthalene ND 0.0406 1 05/14/2023 02:33 WG2059348
Nitrobenzene ND 0.406 1 05/14/2023 02:33 WG2059348
n-Nitrosodimethylamine ND 0.406 1 05/14/2023 02:33 WG2059348
n-Nitrosodiphenylamine ND 0.406 1 05/14/2023 02:33 WG2059348
n-Nitrosodi-n-propylamine ND 0.406 1 05/14/2023 02:33 WG2059348
Phenanthrene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzylbutyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Di-n-butyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Diethyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Dimethyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Di-n-octyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Pyrene ND 0.0406 1 05/14/2023 02:33 WG2059348
1,2,4-Trichlorobenzene ND 0.406 1 05/14/2023 02:33 WG2059348
4-Chloro-3-methylphenol ND 0.406 1 05/14/2023 02:33 WG2059348
2-Chlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dichlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dimethylphenol ND 0.406 1 05/14/2023 02:33 WG2059348
4,6-Dinitro-2-methylphenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dinitrophenol ND 0.406 1 05/14/2023 02:33 WG2059348
2-Nitrophenol ND 0.406 1 05/14/2023 02:33 WG2059348
4-Nitrophenol ND 0.406 1 05/14/2023 02:33 WG2059348
Pentachlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
Phenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4,6-Trichlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
(S) Nitrobenzene-d5 38.8 10.0-122 05/14/2023 02:33 WG2059348
(S) 2-Fluorobiphenyl 40.1 15.0-120 05/14/2023 02:33 WG2059348
(S) p-Terphenyl-d14 45.6 10.0-120 05/14/2023 02:33 WG2059348
(S) Phenol-d5 42.4 10.0-120 05/14/2023 02:33 WG2059348
(S) 2-Fluorophenol 46.0 12.0-120 05/14/2023 02:33 WG2059348
(S) 2,4,6-Tribromophenol 56.0 10.0-127 05/14/2023 02:33 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00732 1 05/17/2023 06:19 WG2059490
Acenaphthene ND 0.00732 1 05/17/2023 06:19 WG2059490
Acenaphthylene ND 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(a)anthracene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(a)pyrene ND 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(b)fluoranthene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(g,h,i)perylene ND 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(k)fluoranthene ND 0.00732 1 05/17/2023 06:19 WG2059490
Chrysene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Dibenz(a,h)anthracene ND 0.00732 1 05/17/2023 06:19 WG2059490
Fluoranthene ND 0.00732 1 05/17/2023 06:19 WG2059490
Fluorene ND 0.00732 1 05/17/2023 06:19 WG2059490
Indeno(1,2,3-cd)pyrene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Naphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
Phenanthrene ND 0.00732 1 05/17/2023 06:19 WG2059490
Pyrene ND 0.00732 1 05/17/2023 06:19 WG2059490
1-Methylnaphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
2-Methylnaphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
2-Chloronaphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
(S) p-Terphenyl-d14 105 23.0-120 05/17/2023 06:19 WG2059490
(S) Nitrobenzene-d5 68.7 14.0-149 05/17/2023 06:19 WG2059490
(S) 2-Fluorobiphenyl 72.7 34.0-125 05/17/2023 06:19 WG2059490
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 69.8 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.43 1 05/13/2023 14:55 WG2057052
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0573 1 05/12/2023 11:37 WG2057615
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.87 1 05/11/2023 21:43 WG2057224
Arsenic 5.44 2.87 1 05/11/2023 21:43 WG2057224
Beryllium 0.380 0.287 1 05/11/2023 21:43 WG2057224
Cadmium ND 0.717 1 05/11/2023 21:43 WG2057224
Chromium 9.56 1.43 1 05/11/2023 21:43 WG2057224
Copper 9.51 2.87 1 05/11/2023 21:43 WG2057224
Lead 4.07 0.717 1 05/11/2023 21:43 WG2057224
Nickel 6.94 2.87 1 05/11/2023 21:43 WG2057224
Selenium ND 2.87 1 05/11/2023 21:43 WG2057224
Silver ND 1.43 1 05/11/2023 21:43 WG2057224
Thallium ND 2.87 1 05/11/2023 21:43 WG2057224
Zinc 28.5 7.17 1 05/11/2023 21:43 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.78 25 05/14/2023 05:26 WG2059653
(S) a,a,a-Trifluorotoluene(FID)93.6 77.0-120 05/14/2023 05:26 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0957 1 05/14/2023 11:27 WG2059688
Acrylonitrile ND 0.0239 1 05/14/2023 11:27 WG2059688
Benzene ND 0.00191 1 05/14/2023 11:27 WG2059688
Bromobenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
Bromodichloromethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Bromoform ND 0.0478 1 05/14/2023 11:27 WG2059688
Bromomethane ND 0.0239 1 05/14/2023 11:27 WG2059688
n-Butylbenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
sec-Butylbenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
tert-Butylbenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
Carbon tetrachloride ND 0.00957 1 05/14/2023 11:27 WG2059688
Chlorobenzene ND 0.00478 1 05/14/2023 11:27 WG2059688
Chlorodibromomethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Chloroethane ND 0.00957 1 05/14/2023 11:27 WG2059688
Chloroform ND 0.00478 1 05/14/2023 11:27 WG2059688
Chloromethane ND 0.0239 1 05/14/2023 11:27 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00478 1 05/14/2023 11:27 WG2059688
4-Chlorotoluene ND J4 0.00957 1 05/14/2023 11:27 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0478 1 05/14/2023 11:27 WG2059688
1,2-Dibromoethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Dibromomethane ND 0.00957 1 05/14/2023 11:27 WG2059688
1,2-Dichlorobenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,3-Dichlorobenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,4-Dichlorobenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
Dichlorodifluoromethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1-Dichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,2-Dichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1-Dichloroethene ND 0.00478 1 05/14/2023 11:27 WG2059688
cis-1,2-Dichloroethene ND 0.00478 1 05/14/2023 11:27 WG2059688
trans-1,2-Dichloroethene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,2-Dichloropropane ND 0.00957 1 05/14/2023 11:27 WG2059688
1,1-Dichloropropene ND 0.00478 1 05/14/2023 11:27 WG2059688
1,3-Dichloropropane ND 0.00957 1 05/14/2023 11:27 WG2059688
cis-1,3-Dichloropropene ND 0.00478 1 05/14/2023 11:27 WG2059688
trans-1,3-Dichloropropene ND 0.00957 1 05/14/2023 11:27 WG2059688
2,2-Dichloropropane ND 0.00478 1 05/14/2023 11:27 WG2059688
Di-isopropyl ether ND 0.00191 1 05/14/2023 11:27 WG2059688
Ethylbenzene ND 0.00478 1 05/14/2023 11:27 WG2059688
Hexachloro-1,3-butadiene ND 0.0478 1 05/14/2023 11:27 WG2059688
Isopropylbenzene ND 0.00478 1 05/14/2023 11:27 WG2059688
p-Isopropyltoluene ND 0.00957 1 05/14/2023 11:27 WG2059688
2-Butanone (MEK)ND 0.191 1 05/14/2023 11:27 WG2059688
Methylene Chloride ND 0.0478 1 05/14/2023 11:27 WG2059688
4-Methyl-2-pentanone (MIBK)ND 0.0478 1 05/14/2023 11:27 WG2059688
Methyl tert-butyl ether ND 0.00191 1 05/14/2023 11:27 WG2059688
Naphthalene ND 0.0239 1 05/14/2023 11:27 WG2059688
n-Propylbenzene ND J4 0.00957 1 05/14/2023 11:27 WG2059688
Styrene ND 0.0239 1 05/14/2023 11:27 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Tetrachloroethene ND 0.00478 1 05/14/2023 11:27 WG2059688
Toluene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,2,3-Trichlorobenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
1,2,4-Trichlorobenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
1,1,1-Trichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1,2-Trichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Trichloroethene ND 0.00191 1 05/14/2023 11:27 WG2059688
Trichlorofluoromethane ND J4 0.00478 1 05/14/2023 11:27 WG2059688
1,2,3-Trichloropropane ND 0.0239 1 05/14/2023 11:27 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00957 1 05/14/2023 11:27 WG2059688
1,2,3-Trimethylbenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,3,5-Trimethylbenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
Vinyl chloride ND 0.00478 1 05/14/2023 11:27 WG2059688
Xylenes, Total ND 0.0124 1 05/14/2023 11:27 WG2059688
(S) Toluene-d8 108 75.0-131 05/14/2023 11:27 WG2059688
(S) 4-Bromofluorobenzene 98.3 67.0-138 05/14/2023 11:27 WG2059688
(S) 1,2-Dichloroethane-d4 91.8 70.0-130 05/14/2023 11:27 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.73 1 05/17/2023 20:59 WG2061264
C28-C40 Oil Range ND 5.73 1 05/17/2023 20:59 WG2061264
(S) o-Terphenyl 47.6 18.0-148 05/17/2023 20:59 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1221 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1232 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1242 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1248 ND 0.0244 1 05/15/2023 02:17 WG2059033
PCB 1254 ND 0.0244 1 05/15/2023 02:17 WG2059033
PCB 1260 ND 0.0244 1 05/15/2023 02:17 WG2059033
(S) Decachlorobiphenyl 72.4 10.0-135 05/15/2023 02:17 WG2059033
(S) Tetrachloro-m-xylene 65.2 10.0-139 05/15/2023 02:17 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Acenaphthylene ND 0.0477 1 05/13/2023 22:15 WG2059348
Anthracene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzidine ND 2.39 1 05/13/2023 22:15 WG2059348
Benzo(a)anthracene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(b)fluoranthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(k)fluoranthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(g,h,i)perylene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(a)pyrene ND 0.0477 1 05/13/2023 22:15 WG2059348
Bis(2-chlorethoxy)methane ND 0.477 1 05/13/2023 22:15 WG2059348
Bis(2-chloroethyl)ether ND 0.477 1 05/13/2023 22:15 WG2059348
2,2-Oxybis(1-Chloropropane)ND 0.477 1 05/13/2023 22:15 WG2059348
4-Bromophenyl-phenylether ND 0.477 1 05/13/2023 22:15 WG2059348
2-Chloronaphthalene ND 0.0477 1 05/13/2023 22:15 WG2059348
4-Chlorophenyl-phenylether ND 0.477 1 05/13/2023 22:15 WG2059348
Chrysene ND 0.0477 1 05/13/2023 22:15 WG2059348
Dibenz(a,h)anthracene ND 0.0477 1 05/13/2023 22:15 WG2059348
3,3-Dichlorobenzidine ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dinitrotoluene ND 0.477 1 05/13/2023 22:15 WG2059348
2,6-Dinitrotoluene ND 0.477 1 05/13/2023 22:15 WG2059348
Fluoranthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Fluorene ND 0.0477 1 05/13/2023 22:15 WG2059348
Hexachlorobenzene ND 0.477 1 05/13/2023 22:15 WG2059348
Hexachloro-1,3-butadiene ND 0.477 1 05/13/2023 22:15 WG2059348
Hexachlorocyclopentadiene ND 0.477 1 05/13/2023 22:15 WG2059348
Hexachloroethane ND 0.477 1 05/13/2023 22:15 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0477 1 05/13/2023 22:15 WG2059348
Isophorone ND 0.477 1 05/13/2023 22:15 WG2059348
Naphthalene ND 0.0477 1 05/13/2023 22:15 WG2059348
Nitrobenzene ND 0.477 1 05/13/2023 22:15 WG2059348
n-Nitrosodimethylamine ND 0.477 1 05/13/2023 22:15 WG2059348
n-Nitrosodiphenylamine ND 0.477 1 05/13/2023 22:15 WG2059348
n-Nitrosodi-n-propylamine ND 0.477 1 05/13/2023 22:15 WG2059348
Phenanthrene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzylbutyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Di-n-butyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Diethyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Dimethyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Di-n-octyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Pyrene ND 0.0477 1 05/13/2023 22:15 WG2059348
1,2,4-Trichlorobenzene ND 0.477 1 05/13/2023 22:15 WG2059348
4-Chloro-3-methylphenol ND 0.477 1 05/13/2023 22:15 WG2059348
2-Chlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dichlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dimethylphenol ND 0.477 1 05/13/2023 22:15 WG2059348
4,6-Dinitro-2-methylphenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dinitrophenol ND 0.477 1 05/13/2023 22:15 WG2059348
2-Nitrophenol ND 0.477 1 05/13/2023 22:15 WG2059348
4-Nitrophenol ND 0.477 1 05/13/2023 22:15 WG2059348
Pentachlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
Phenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4,6-Trichlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
(S) Nitrobenzene-d5 37.9 10.0-122 05/13/2023 22:15 WG2059348
(S) 2-Fluorobiphenyl 44.8 15.0-120 05/13/2023 22:15 WG2059348
(S) p-Terphenyl-d14 53.9 10.0-120 05/13/2023 22:15 WG2059348
(S) Phenol-d5 38.6 10.0-120 05/13/2023 22:15 WG2059348
(S) 2-Fluorophenol 45.9 12.0-120 05/13/2023 22:15 WG2059348
(S) 2,4,6-Tribromophenol 47.9 10.0-127 05/13/2023 22:15 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00860 1 05/17/2023 06:37 WG2059490
Acenaphthene ND 0.00860 1 05/17/2023 06:37 WG2059490
Acenaphthylene ND 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(a)anthracene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(a)pyrene ND 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(b)fluoranthene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(g,h,i)perylene ND 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(k)fluoranthene ND 0.00860 1 05/17/2023 06:37 WG2059490
Chrysene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Dibenz(a,h)anthracene ND 0.00860 1 05/17/2023 06:37 WG2059490
Fluoranthene ND 0.00860 1 05/17/2023 06:37 WG2059490
Fluorene ND 0.00860 1 05/17/2023 06:37 WG2059490
Indeno(1,2,3-cd)pyrene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Naphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
Phenanthrene ND 0.00860 1 05/17/2023 06:37 WG2059490
Pyrene ND 0.00860 1 05/17/2023 06:37 WG2059490
1-Methylnaphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
2-Methylnaphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
2-Chloronaphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
(S) p-Terphenyl-d14 98.5 23.0-120 05/17/2023 06:37 WG2059490
(S) Nitrobenzene-d5 46.7 14.0-149 05/17/2023 06:37 WG2059490
(S) 2-Fluorobiphenyl 55.7 34.0-125 05/17/2023 06:37 WG2059490
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.3 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.33 1 05/13/2023 15:00 WG2057052
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0531 1 05/12/2023 11:39 WG2057615
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.66 1 05/11/2023 21:46 WG2057224
Arsenic 10.1 2.66 1 05/11/2023 21:46 WG2057224
Beryllium 0.311 0.266 1 05/11/2023 21:46 WG2057224
Cadmium ND 0.664 1 05/11/2023 21:46 WG2057224
Chromium 7.57 1.33 1 05/11/2023 21:46 WG2057224
Copper 16.1 2.66 1 05/11/2023 21:46 WG2057224
Lead 25.6 0.664 1 05/11/2023 21:46 WG2057224
Nickel 5.63 2.66 1 05/11/2023 21:46 WG2057224
Selenium ND 2.66 1 05/11/2023 21:46 WG2057224
Silver ND 1.33 1 05/11/2023 21:46 WG2057224
Thallium ND 2.66 1 05/11/2023 21:46 WG2057224
Zinc 44.0 6.64 1 05/11/2023 21:46 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.22 25 05/14/2023 05:47 WG2059653
(S) a,a,a-Trifluorotoluene(FID)94.9 77.0-120 05/14/2023 05:47 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0889 0.0844 1 05/14/2023 11:46 WG2059688
Acrylonitrile ND 0.0211 1 05/14/2023 11:46 WG2059688
Benzene ND 0.00169 1 05/14/2023 11:46 WG2059688
Bromobenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
Bromodichloromethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Bromoform ND 0.0422 1 05/14/2023 11:46 WG2059688
Bromomethane ND 0.0211 1 05/14/2023 11:46 WG2059688
n-Butylbenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
sec-Butylbenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
tert-Butylbenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
Carbon tetrachloride ND 0.00844 1 05/14/2023 11:46 WG2059688
Chlorobenzene ND 0.00422 1 05/14/2023 11:46 WG2059688
Chlorodibromomethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Chloroethane ND 0.00844 1 05/14/2023 11:46 WG2059688
Chloroform ND 0.00422 1 05/14/2023 11:46 WG2059688
Chloromethane ND 0.0211 1 05/14/2023 11:46 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00422 1 05/14/2023 11:46 WG2059688
4-Chlorotoluene ND J4 0.00844 1 05/14/2023 11:46 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0422 1 05/14/2023 11:46 WG2059688
1,2-Dibromoethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Dibromomethane ND 0.00844 1 05/14/2023 11:46 WG2059688
1,2-Dichlorobenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,3-Dichlorobenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,4-Dichlorobenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
Dichlorodifluoromethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1-Dichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,2-Dichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1-Dichloroethene ND 0.00422 1 05/14/2023 11:46 WG2059688
cis-1,2-Dichloroethene ND 0.00422 1 05/14/2023 11:46 WG2059688
trans-1,2-Dichloroethene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,2-Dichloropropane ND 0.00844 1 05/14/2023 11:46 WG2059688
1,1-Dichloropropene ND 0.00422 1 05/14/2023 11:46 WG2059688
1,3-Dichloropropane ND 0.00844 1 05/14/2023 11:46 WG2059688
cis-1,3-Dichloropropene ND 0.00422 1 05/14/2023 11:46 WG2059688
trans-1,3-Dichloropropene ND 0.00844 1 05/14/2023 11:46 WG2059688
2,2-Dichloropropane ND 0.00422 1 05/14/2023 11:46 WG2059688
Di-isopropyl ether ND 0.00169 1 05/14/2023 11:46 WG2059688
Ethylbenzene ND 0.00422 1 05/14/2023 11:46 WG2059688
Hexachloro-1,3-butadiene ND 0.0422 1 05/14/2023 11:46 WG2059688
Isopropylbenzene ND 0.00422 1 05/14/2023 11:46 WG2059688
p-Isopropyltoluene ND 0.00844 1 05/14/2023 11:46 WG2059688
2-Butanone (MEK)ND 0.169 1 05/14/2023 11:46 WG2059688
Methylene Chloride ND 0.0422 1 05/14/2023 11:46 WG2059688
4-Methyl-2-pentanone (MIBK)ND 0.0422 1 05/14/2023 11:46 WG2059688
Methyl tert-butyl ether ND 0.00169 1 05/14/2023 11:46 WG2059688
Naphthalene ND 0.0211 1 05/14/2023 11:46 WG2059688
n-Propylbenzene ND J4 0.00844 1 05/14/2023 11:46 WG2059688
Styrene ND 0.0211 1 05/14/2023 11:46 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Tetrachloroethene ND 0.00422 1 05/14/2023 11:46 WG2059688
Toluene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,2,3-Trichlorobenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
1,2,4-Trichlorobenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
1,1,1-Trichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1,2-Trichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Trichloroethene ND 0.00169 1 05/14/2023 11:46 WG2059688
Trichlorofluoromethane ND J4 0.00422 1 05/14/2023 11:46 WG2059688
1,2,3-Trichloropropane ND 0.0211 1 05/14/2023 11:46 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00844 1 05/14/2023 11:46 WG2059688
1,2,3-Trimethylbenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,3,5-Trimethylbenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
Vinyl chloride ND 0.00422 1 05/14/2023 11:46 WG2059688
Xylenes, Total ND 0.0110 1 05/14/2023 11:46 WG2059688
(S) Toluene-d8 107 75.0-131 05/14/2023 11:46 WG2059688
(S) 4-Bromofluorobenzene 95.1 67.0-138 05/14/2023 11:46 WG2059688
(S) 1,2-Dichloroethane-d4 95.9 70.0-130 05/14/2023 11:46 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.31 1 05/18/2023 09:47 WG2061264
C28-C40 Oil Range 13.6 5.31 1 05/18/2023 09:47 WG2061264
(S) o-Terphenyl 69.8 18.0-148 05/18/2023 09:47 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1221 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1232 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1242 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1248 ND 0.0226 1 05/15/2023 02:27 WG2059033
PCB 1254 ND 0.0226 1 05/15/2023 02:27 WG2059033
PCB 1260 ND 0.0226 1 05/15/2023 02:27 WG2059033
(S) Decachlorobiphenyl 69.1 10.0-135 05/15/2023 02:27 WG2059033
(S) Tetrachloro-m-xylene 61.8 10.0-139 05/15/2023 02:27 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Acenaphthylene ND 0.0442 1 05/13/2023 22:36 WG2059348
Anthracene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzidine ND 2.22 1 05/13/2023 22:36 WG2059348
Benzo(a)anthracene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(b)fluoranthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(k)fluoranthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(g,h,i)perylene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(a)pyrene ND 0.0442 1 05/13/2023 22:36 WG2059348
Bis(2-chlorethoxy)methane ND 0.442 1 05/13/2023 22:36 WG2059348
Bis(2-chloroethyl)ether ND 0.442 1 05/13/2023 22:36 WG2059348
2,2-Oxybis(1-Chloropropane)ND 0.442 1 05/13/2023 22:36 WG2059348
4-Bromophenyl-phenylether ND 0.442 1 05/13/2023 22:36 WG2059348
2-Chloronaphthalene ND 0.0442 1 05/13/2023 22:36 WG2059348
4-Chlorophenyl-phenylether ND 0.442 1 05/13/2023 22:36 WG2059348
Chrysene ND 0.0442 1 05/13/2023 22:36 WG2059348
Dibenz(a,h)anthracene ND 0.0442 1 05/13/2023 22:36 WG2059348
3,3-Dichlorobenzidine ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dinitrotoluene ND 0.442 1 05/13/2023 22:36 WG2059348
2,6-Dinitrotoluene ND 0.442 1 05/13/2023 22:36 WG2059348
Fluoranthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Fluorene ND 0.0442 1 05/13/2023 22:36 WG2059348
Hexachlorobenzene ND 0.442 1 05/13/2023 22:36 WG2059348
Hexachloro-1,3-butadiene ND 0.442 1 05/13/2023 22:36 WG2059348
Hexachlorocyclopentadiene ND 0.442 1 05/13/2023 22:36 WG2059348
Hexachloroethane ND 0.442 1 05/13/2023 22:36 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0442 1 05/13/2023 22:36 WG2059348
Isophorone ND 0.442 1 05/13/2023 22:36 WG2059348
Naphthalene ND 0.0442 1 05/13/2023 22:36 WG2059348
Nitrobenzene ND 0.442 1 05/13/2023 22:36 WG2059348
n-Nitrosodimethylamine ND 0.442 1 05/13/2023 22:36 WG2059348
n-Nitrosodiphenylamine ND 0.442 1 05/13/2023 22:36 WG2059348
n-Nitrosodi-n-propylamine ND 0.442 1 05/13/2023 22:36 WG2059348
Phenanthrene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzylbutyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Di-n-butyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Diethyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Dimethyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Di-n-octyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Pyrene ND 0.0442 1 05/13/2023 22:36 WG2059348
1,2,4-Trichlorobenzene ND 0.442 1 05/13/2023 22:36 WG2059348
4-Chloro-3-methylphenol ND 0.442 1 05/13/2023 22:36 WG2059348
2-Chlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dichlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dimethylphenol ND 0.442 1 05/13/2023 22:36 WG2059348
4,6-Dinitro-2-methylphenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dinitrophenol ND 0.442 1 05/13/2023 22:36 WG2059348
2-Nitrophenol ND 0.442 1 05/13/2023 22:36 WG2059348
4-Nitrophenol ND 0.442 1 05/13/2023 22:36 WG2059348
Pentachlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
Phenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4,6-Trichlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
(S) Nitrobenzene-d5 36.8 10.0-122 05/13/2023 22:36 WG2059348
(S) 2-Fluorobiphenyl 43.2 15.0-120 05/13/2023 22:36 WG2059348
(S) p-Terphenyl-d14 55.3 10.0-120 05/13/2023 22:36 WG2059348
(S) Phenol-d5 38.9 10.0-120 05/13/2023 22:36 WG2059348
(S) 2-Fluorophenol 46.8 12.0-120 05/13/2023 22:36 WG2059348
(S) 2,4,6-Tribromophenol 52.6 10.0-127 05/13/2023 22:36 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00797 1 05/17/2023 18:16 WG2059490
Acenaphthene ND 0.00797 1 05/17/2023 18:16 WG2059490
Acenaphthylene ND 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(a)anthracene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(a)pyrene ND 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(b)fluoranthene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(g,h,i)perylene ND 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(k)fluoranthene ND 0.00797 1 05/17/2023 18:16 WG2059490
Chrysene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Dibenz(a,h)anthracene ND 0.00797 1 05/17/2023 18:16 WG2059490
Fluoranthene ND 0.00797 1 05/17/2023 18:16 WG2059490
Fluorene ND 0.00797 1 05/17/2023 18:16 WG2059490
Indeno(1,2,3-cd)pyrene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Naphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
Phenanthrene ND 0.00797 1 05/17/2023 18:16 WG2059490
Pyrene ND 0.00797 1 05/17/2023 18:16 WG2059490
1-Methylnaphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
2-Methylnaphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
2-Chloronaphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
(S) p-Terphenyl-d14 87.5 23.0-120 05/17/2023 18:16 WG2059490
(S) Nitrobenzene-d5 73.4 14.0-149 05/17/2023 18:16 WG2059490
(S) 2-Fluorobiphenyl 65.8 34.0-125 05/17/2023 18:16 WG2059490
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.0 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.30 1 05/13/2023 15:05 WG2057052
Mercury by Method 7471A
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0520 1 05/18/2023 16:56 WG2057613
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.60 1 05/11/2023 21:49 WG2057224
Arsenic 6.27 2.60 1 05/11/2023 21:49 WG2057224
Beryllium 0.399 0.260 1 05/11/2023 21:49 WG2057224
Cadmium ND 0.650 1 05/11/2023 21:49 WG2057224
Chromium 10.3 1.30 1 05/11/2023 21:49 WG2057224
Copper 8.52 2.60 1 05/11/2023 21:49 WG2057224
Lead 5.43 0.650 1 05/11/2023 21:49 WG2057224
Nickel 7.30 2.60 1 05/11/2023 21:49 WG2057224
Selenium ND 2.60 1 05/11/2023 21:49 WG2057224
Silver ND 1.30 1 05/11/2023 21:49 WG2057224
Thallium ND 2.60 1 05/11/2023 21:49 WG2057224
Zinc 30.9 6.50 1 05/11/2023 21:49 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.13 26 05/14/2023 06:07 WG2059653
(S) a,a,a-Trifluorotoluene(FID)90.0 77.0-120 05/14/2023 06:07 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0826 1.04 05/14/2023 12:04 WG2059688
Acrylonitrile ND 0.0206 1.04 05/14/2023 12:04 WG2059688
Benzene ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Bromobenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
Bromodichloromethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Bromoform ND 0.0413 1.04 05/14/2023 12:04 WG2059688
Bromomethane ND 0.0206 1.04 05/14/2023 12:04 WG2059688
n-Butylbenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
sec-Butylbenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
tert-Butylbenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Carbon tetrachloride ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Chlorobenzene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Chlorodibromomethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Chloroethane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Chloroform ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Chloromethane ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
4-Chlorotoluene ND J4 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0413 1.04 05/14/2023 12:04 WG2059688
1,2-Dibromoethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Dibromomethane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2-Dichlorobenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,3-Dichlorobenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,4-Dichlorobenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Dichlorodifluoromethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1-Dichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,2-Dichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1-Dichloroethene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
cis-1,2-Dichloroethene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
trans-1,2-Dichloroethene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2-Dichloropropane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,1-Dichloropropene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,3-Dichloropropane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
cis-1,3-Dichloropropene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
trans-1,3-Dichloropropene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
2,2-Dichloropropane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Di-isopropyl ether ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Ethylbenzene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Hexachloro-1,3-butadiene ND 0.0413 1.04 05/14/2023 12:04 WG2059688
Isopropylbenzene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
p-Isopropyltoluene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
2-Butanone (MEK)ND 0.165 1.04 05/14/2023 12:04 WG2059688
Methylene Chloride ND 0.0413 1.04 05/14/2023 12:04 WG2059688
4-Methyl-2-pentanone (MIBK)ND 0.0413 1.04 05/14/2023 12:04 WG2059688
Methyl tert-butyl ether ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Naphthalene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
n-Propylbenzene ND J4 0.00826 1.04 05/14/2023 12:04 WG2059688
Styrene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Tetrachloroethene 0.00772 0.00413 1.04 05/14/2023 12:04 WG2059688
Toluene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2,3-Trichlorobenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,2,4-Trichlorobenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,1,1-Trichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1,2-Trichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Trichloroethene ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Trichlorofluoromethane ND J4 0.00413 1.04 05/14/2023 12:04 WG2059688
1,2,3-Trichloropropane ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2,3-Trimethylbenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,3,5-Trimethylbenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Vinyl chloride ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Xylenes, Total ND 0.0107 1.04 05/14/2023 12:04 WG2059688
(S) Toluene-d8 110 75.0-131 05/14/2023 12:04 WG2059688
(S) 4-Bromofluorobenzene 103 67.0-138 05/14/2023 12:04 WG2059688
(S) 1,2-Dichloroethane-d4 95.3 70.0-130 05/14/2023 12:04 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 8.98 5.20 1 05/17/2023 22:56 WG2061264
C28-C40 Oil Range 26.1 5.20 1 05/17/2023 22:56 WG2061264
(S) o-Terphenyl 38.1 18.0-148 05/17/2023 22:56 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1221 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1232 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1242 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1248 ND 0.0221 1 05/15/2023 01:50 WG2059034
PCB 1254 ND 0.0221 1 05/15/2023 01:50 WG2059034
PCB 1260 ND 0.0221 1 05/15/2023 01:50 WG2059034
(S) Decachlorobiphenyl 36.5 10.0-135 05/15/2023 01:50 WG2059034
(S) Tetrachloro-m-xylene 41.8 10.0-139 05/15/2023 01:50 WG2059034
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Acenaphthylene ND 0.0433 1 05/14/2023 00:45 WG2059348
Anthracene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzidine ND J6 2.17 1 05/14/2023 00:45 WG2059348
Benzo(a)anthracene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(b)fluoranthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(k)fluoranthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(g,h,i)perylene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(a)pyrene ND 0.0433 1 05/14/2023 00:45 WG2059348
Bis(2-chlorethoxy)methane ND 0.433 1 05/14/2023 00:45 WG2059348
Bis(2-chloroethyl)ether ND 0.433 1 05/14/2023 00:45 WG2059348
2,2-Oxybis(1-Chloropropane)ND 0.433 1 05/14/2023 00:45 WG2059348
4-Bromophenyl-phenylether ND 0.433 1 05/14/2023 00:45 WG2059348
2-Chloronaphthalene ND 0.0433 1 05/14/2023 00:45 WG2059348
4-Chlorophenyl-phenylether ND 0.433 1 05/14/2023 00:45 WG2059348
Chrysene ND 0.0433 1 05/14/2023 00:45 WG2059348
Dibenz(a,h)anthracene ND 0.0433 1 05/14/2023 00:45 WG2059348
3,3-Dichlorobenzidine ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dinitrotoluene ND 0.433 1 05/14/2023 00:45 WG2059348
2,6-Dinitrotoluene ND 0.433 1 05/14/2023 00:45 WG2059348
Fluoranthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Fluorene ND 0.0433 1 05/14/2023 00:45 WG2059348
Hexachlorobenzene ND 0.433 1 05/14/2023 00:45 WG2059348
Hexachloro-1,3-butadiene ND 0.433 1 05/14/2023 00:45 WG2059348
Hexachlorocyclopentadiene ND 0.433 1 05/14/2023 00:45 WG2059348
Hexachloroethane ND 0.433 1 05/14/2023 00:45 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0433 1 05/14/2023 00:45 WG2059348
Isophorone ND 0.433 1 05/14/2023 00:45 WG2059348
Naphthalene ND 0.0433 1 05/14/2023 00:45 WG2059348
Nitrobenzene ND 0.433 1 05/14/2023 00:45 WG2059348
n-Nitrosodimethylamine ND 0.433 1 05/14/2023 00:45 WG2059348
n-Nitrosodiphenylamine ND 0.433 1 05/14/2023 00:45 WG2059348
n-Nitrosodi-n-propylamine ND 0.433 1 05/14/2023 00:45 WG2059348
Phenanthrene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzylbutyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Di-n-butyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Diethyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Dimethyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Di-n-octyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Pyrene ND 0.0433 1 05/14/2023 00:45 WG2059348
1,2,4-Trichlorobenzene ND 0.433 1 05/14/2023 00:45 WG2059348
4-Chloro-3-methylphenol ND 0.433 1 05/14/2023 00:45 WG2059348
2-Chlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dichlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dimethylphenol ND 0.433 1 05/14/2023 00:45 WG2059348
4,6-Dinitro-2-methylphenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dinitrophenol ND 0.433 1 05/14/2023 00:45 WG2059348
2-Nitrophenol ND 0.433 1 05/14/2023 00:45 WG2059348
4-Nitrophenol ND 0.433 1 05/14/2023 00:45 WG2059348
Pentachlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
Phenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4,6-Trichlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
(S) Nitrobenzene-d5 44.0 10.0-122 05/14/2023 00:45 WG2059348
(S) 2-Fluorobiphenyl 47.7 15.0-120 05/14/2023 00:45 WG2059348
(S) p-Terphenyl-d14 55.4 10.0-120 05/14/2023 00:45 WG2059348
(S) Phenol-d5 44.6 10.0-120 05/14/2023 00:45 WG2059348
(S) 2-Fluorophenol 48.6 12.0-120 05/14/2023 00:45 WG2059348
(S) 2,4,6-Tribromophenol 58.3 10.0-127 05/14/2023 00:45 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00780 1 05/15/2023 19:10 WG2059491
Acenaphthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Acenaphthylene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(a)anthracene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(a)pyrene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(b)fluoranthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(g,h,i)perylene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(k)fluoranthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Chrysene ND 0.00780 1 05/15/2023 19:10 WG2059491
Dibenz(a,h)anthracene ND 0.00780 1 05/15/2023 19:10 WG2059491
Fluoranthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Fluorene ND 0.00780 1 05/15/2023 19:10 WG2059491
Indeno(1,2,3-cd)pyrene ND 0.00780 1 05/15/2023 19:10 WG2059491
Naphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
Phenanthrene ND 0.00780 1 05/15/2023 19:10 WG2059491
Pyrene ND 0.00780 1 05/15/2023 19:10 WG2059491
1-Methylnaphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
2-Methylnaphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
2-Chloronaphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
(S) p-Terphenyl-d14 84.7 23.0-120 05/15/2023 19:10 WG2059491
(S) Nitrobenzene-d5 81.4 14.0-149 05/15/2023 19:10 WG2059491
(S) 2-Fluorobiphenyl 68.9 34.0-125 05/15/2023 19:10 WG2059491
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057261
Total Solids by Method 2540 G-2011 L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3923503-1 05/10/23 17:08
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1614172-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1614172-02 05/10/23 17:08 • (DUP) R3923503-3 05/10/23 17:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 82.0 80.9 1 1.33 10
Laboratory Control Sample (LCS)
(LCS) R3923503-2 05/10/23 17:08
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057052
Wet Chemistry by Method 7199 L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3924698-1 05/13/23 13:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1614576-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1614576-02 05/13/23 15:31 • (DUP) R3924698-7 05/13/23 15:36
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
L1613016-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1613016-02 05/13/23 16:02 • (DUP) R3924698-8 05/13/23 16:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium 1610 1370 100 16.2 20
Laboratory Control Sample (LCS)
(LCS) R3924698-2 05/13/23 13:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 10.5 105 80.0-120
L1613016-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613016-01 05/13/23 13:32 • (MS) R3924698-3 05/13/23 13:37 • (MSD) R3924698-4 05/13/23 13:42
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 4.93 26.6 26.2 108 106 1 75.0-125 1.53 20
L1613016-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1613016-01 05/13/23 13:32 • (MS) R3924698-5 05/13/23 13:47
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 646 4.93 776 120 50 75.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057613
Mercury by Method 7471A L1614172-05
Method Blank (MB)
(MB) R3926642-1 05/18/23 16:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3926642-2 05/18/23 16:42
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.547 109 80.0-120
L1614238-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-01 05/18/23 16:44 • (MS) R3926642-3 05/18/23 16:47 • (MSD) R3926642-4 05/18/23 16:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.580 ND 0.575 0.590 93.4 96.0 1 75.0-125 2.61 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057615
Mercury by Method 7471A L1614172-01,02,03,04
Method Blank (MB)
(MB) R3924101-1 05/12/23 10:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3924101-2 05/12/23 10:43
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.582 116 80.0-120
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/12/23 10:45 • (MS) R3924101-3 05/12/23 10:47 • (MSD) R3924101-4 05/12/23 10:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.547 ND 0.476 0.612 79.0 104 1 75.0-125 J3 25.1 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057224
Metals (ICP) by Method 6010B L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3923898-1 05/11/23 20:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper 0.532 J 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3923898-2 05/11/23 20:58
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 98.5 98.5 80.0-120
Arsenic 100 94.5 94.5 80.0-120
Beryllium 100 98.6 98.6 80.0-120
Cadmium 100 97.0 97.0 80.0-120
Chromium 100 98.3 98.3 80.0-120
Copper 100 99.5 99.5 80.0-120
Lead 100 95.7 95.7 80.0-120
Nickel 100 96.9 96.9 80.0-120
Selenium 100 98.9 98.9 80.0-120
Silver 20.0 19.3 96.7 80.0-120
Thallium 100 95.4 95.4 80.0-120
Zinc 100 94.8 94.8 80.0-120
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/11/23 21:01 • (MS) R3923898-5 05/11/23 21:09 • (MSD) R3923898-6 05/11/23 21:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 109 ND 73.5 80.3 65.9 72.0 1 75.0-125 J6 J6 8.74 20
Arsenic 109 2.27 110 116 98.6 104 1 75.0-125 4.79 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057224
Metals (ICP) by Method 6010B L1614172-01,02,03,04,05
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/11/23 21:01 • (MS) R3923898-5 05/11/23 21:09 • (MSD) R3923898-6 05/11/23 21:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 109 0.387 107 118 97.1 107 1 75.0-125 9.77 20
Cadmium 109 ND 107 118 97.9 108 1 75.0-125 9.75 20
Chromium 109 35.5 143 151 98.0 105 1 75.0-125 5.35 20
Copper 109 27.1 153 154 115 116 1 75.0-125 0.822 20
Lead 109 17.9 143 133 114 106 1 75.0-125 6.71 20
Nickel 109 33.6 149 156 105 112 1 75.0-125 4.79 20
Selenium 109 ND 109 117 99.9 106 1 75.0-125 6.34 20
Silver 21.9 ND 21.8 23.7 99.8 108 1 75.0-125 8.35 20
Thallium 109 ND 96.2 107 87.9 97.4 1 75.0-125 10.3 20
Zinc 109 53.6 157 172 94.4 108 1 75.0-125 9.02 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059653
Volatile Organic Compounds (GC) by Method 8015D/GRO L1614172-02,03,04,05
Method Blank (MB)
(MB) R3925948-2 05/14/23 01:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.728 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)92.9 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3925948-1 05/13/23 23:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 4.79 87.1 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 107 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062511
Volatile Organic Compounds (GC) by Method 8015D/GRO L1614172-01
Method Blank (MB)
(MB) R3926950-3 05/18/23 13:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)92.5 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3926950-2 05/18/23 12:47
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.47 99.5 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 97.5 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Method Blank (MB)
(MB) R3925455-3 05/13/23 13:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Method Blank (MB)
(MB) R3925455-3 05/13/23 13:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride 0.00695 J 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 109 75.0-131
(S) 4-Bromofluorobenzene 99.1 67.0-138
(S) 1,2-Dichloroethane-d4 86.4 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3925455-1 05/13/23 11:47 • (LCSD) R3925455-2 05/13/23 12:06
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.538 0.556 86.1 89.0 10.0-160 3.29 31
Acrylonitrile 0.625 0.727 0.830 116 133 45.0-153 13.2 22
Benzene 0.125 0.106 0.105 84.8 84.0 70.0-123 0.948 20
Bromobenzene 0.125 0.0990 0.0976 79.2 78.1 73.0-121 1.42 20
Bromodichloromethane 0.125 0.104 0.107 83.2 85.6 73.0-121 2.84 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3925455-1 05/13/23 11:47 • (LCSD) R3925455-2 05/13/23 12:06
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.117 0.121 93.6 96.8 64.0-132 3.36 20
Bromomethane 0.125 0.106 0.0983 84.8 78.6 56.0-147 7.54 20
n-Butylbenzene 0.125 0.0993 0.110 79.4 88.0 68.0-135 10.2 20
sec-Butylbenzene 0.125 0.103 0.107 82.4 85.6 74.0-130 3.81 20
tert-Butylbenzene 0.125 0.104 0.103 83.2 82.4 75.0-127 0.966 20
Carbon tetrachloride 0.125 0.118 0.118 94.4 94.4 66.0-128 0.000 20
Chlorobenzene 0.125 0.112 0.114 89.6 91.2 76.0-128 1.77 20
Chlorodibromomethane 0.125 0.110 0.113 88.0 90.4 74.0-127 2.69 20
Chloroethane 0.125 0.108 0.0961 86.4 76.9 61.0-134 11.7 20
Chloroform 0.125 0.106 0.104 84.8 83.2 72.0-123 1.90 20
Chloromethane 0.125 0.103 0.104 82.4 83.2 51.0-138 0.966 20
2-Chlorotoluene 0.125 0.106 0.107 84.8 85.6 75.0-124 0.939 20
4-Chlorotoluene 0.125 0.0851 0.0865 68.1 69.2 75.0-124 J4 J4 1.63 20
1,2-Dibromo-3-Chloropropane 0.125 0.137 0.151 110 121 59.0-130 9.72 20
1,2-Dibromoethane 0.125 0.112 0.117 89.6 93.6 74.0-128 4.37 20
Dibromomethane 0.125 0.112 0.111 89.6 88.8 75.0-122 0.897 20
1,2-Dichlorobenzene 0.125 0.0998 0.108 79.8 86.4 76.0-124 7.89 20
1,3-Dichlorobenzene 0.125 0.101 0.105 80.8 84.0 76.0-125 3.88 20
1,4-Dichlorobenzene 0.125 0.0985 0.106 78.8 84.8 77.0-121 7.33 20
Dichlorodifluoromethane 0.125 0.0864 0.0927 69.1 74.2 43.0-156 7.04 20
1,1-Dichloroethane 0.125 0.105 0.106 84.0 84.8 70.0-127 0.948 20
1,2-Dichloroethane 0.125 0.0926 0.0952 74.1 76.2 65.0-131 2.77 20
1,1-Dichloroethene 0.125 0.105 0.107 84.0 85.6 65.0-131 1.89 20
cis-1,2-Dichloroethene 0.125 0.114 0.110 91.2 88.0 73.0-125 3.57 20
trans-1,2-Dichloroethene 0.125 0.112 0.107 89.6 85.6 71.0-125 4.57 20
1,2-Dichloropropane 0.125 0.103 0.103 82.4 82.4 74.0-125 0.000 20
1,1-Dichloropropene 0.125 0.115 0.118 92.0 94.4 73.0-125 2.58 20
1,3-Dichloropropane 0.125 0.107 0.107 85.6 85.6 80.0-125 0.000 20
cis-1,3-Dichloropropene 0.125 0.100 0.0990 80.0 79.2 76.0-127 1.01 20
trans-1,3-Dichloropropene 0.125 0.0993 0.0968 79.4 77.4 73.0-127 2.55 20
2,2-Dichloropropane 0.125 0.101 0.101 80.8 80.8 59.0-135 0.000 20
Di-isopropyl ether 0.125 0.105 0.107 84.0 85.6 60.0-136 1.89 20
Ethylbenzene 0.125 0.117 0.121 93.6 96.8 74.0-126 3.36 20
Hexachloro-1,3-butadiene 0.125 0.0970 0.110 77.6 88.0 57.0-150 12.6 20
Isopropylbenzene 0.125 0.117 0.128 93.6 102 72.0-127 8.98 20
p-Isopropyltoluene 0.125 0.102 0.109 81.6 87.2 72.0-133 6.64 20
2-Butanone (MEK)0.625 0.669 0.662 107 106 30.0-160 1.05 24
Methylene Chloride 0.125 0.108 0.108 86.4 86.4 68.0-123 0.000 20
4-Methyl-2-pentanone (MIBK)0.625 0.725 0.725 116 116 56.0-143 0.000 20
Methyl tert-butyl ether 0.125 0.109 0.111 87.2 88.8 66.0-132 1.82 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3925455-1 05/13/23 11:47 • (LCSD) R3925455-2 05/13/23 12:06
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.120 0.161 96.0 129 59.0-130 J3 29.2 20
n-Propylbenzene 0.125 0.0941 0.0973 75.3 77.8 74.0-126 3.34 20
Styrene 0.125 0.110 0.113 88.0 90.4 72.0-127 2.69 20
1,1,1,2-Tetrachloroethane 0.125 0.114 0.117 91.2 93.6 74.0-129 2.60 20
1,1,2,2-Tetrachloroethane 0.125 0.119 0.115 95.2 92.0 68.0-128 3.42 20
1,1,2-Trichlorotrifluoroethane 0.125 0.119 0.122 95.2 97.6 61.0-139 2.49 20
Tetrachloroethene 0.125 0.116 0.118 92.8 94.4 70.0-136 1.71 20
Toluene 0.125 0.106 0.106 84.8 84.8 75.0-121 0.000 20
1,2,3-Trichlorobenzene 0.125 0.105 0.140 84.0 112 59.0-139 J3 28.6 20
1,2,4-Trichlorobenzene 0.125 0.0977 0.128 78.2 102 62.0-137 J3 26.8 20
1,1,1-Trichloroethane 0.125 0.116 0.114 92.8 91.2 69.0-126 1.74 20
1,1,2-Trichloroethane 0.125 0.114 0.109 91.2 87.2 78.0-123 4.48 20
Trichloroethene 0.125 0.112 0.111 89.6 88.8 76.0-126 0.897 20
Trichlorofluoromethane 0.125 0.115 0.117 92.0 93.6 61.0-142 1.72 20
1,2,3-Trichloropropane 0.125 0.126 0.115 101 92.0 67.0-129 9.13 20
1,2,4-Trimethylbenzene 0.125 0.101 0.105 80.8 84.0 70.0-126 3.88 20
1,2,3-Trimethylbenzene 0.125 0.101 0.106 80.8 84.8 74.0-124 4.83 20
1,3,5-Trimethylbenzene 0.125 0.104 0.104 83.2 83.2 73.0-127 0.000 20
Vinyl chloride 0.125 0.109 0.103 87.2 82.4 63.0-134 5.66 20
Xylenes, Total 0.375 0.337 0.346 89.9 92.3 72.0-127 2.64 20
(S) Toluene-d8 102 102 75.0-131
(S) 4-Bromofluorobenzene 103 107 67.0-138
(S) 1,2-Dichloroethane-d4 93.7 93.8 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Method Blank (MB)
(MB) R3925553-2 05/14/23 07:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Method Blank (MB)
(MB) R3925553-2 05/14/23 07:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 91.7 67.0-138
(S) 1,2-Dichloroethane-d4 95.1 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3925553-1 05/14/23 06:08
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.609 97.4 10.0-160
Acrylonitrile 0.625 0.748 120 45.0-153
Benzene 0.125 0.101 80.8 70.0-123
Bromobenzene 0.125 0.0959 76.7 73.0-121
Bromodichloromethane 0.125 0.110 88.0 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925553-1 05/14/23 06:08
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.146 117 64.0-132
Bromomethane 0.125 0.176 141 56.0-147
n-Butylbenzene 0.125 0.0940 75.2 68.0-135
sec-Butylbenzene 0.125 0.0983 78.6 74.0-130
tert-Butylbenzene 0.125 0.0947 75.8 75.0-127
Carbon tetrachloride 0.125 0.130 104 66.0-128
Chlorobenzene 0.125 0.109 87.2 76.0-128
Chlorodibromomethane 0.125 0.128 102 74.0-127
Chloroethane 0.125 0.143 114 61.0-134
Chloroform 0.125 0.109 87.2 72.0-123
Chloromethane 0.125 0.128 102 51.0-138
2-Chlorotoluene 0.125 0.106 84.8 75.0-124
4-Chlorotoluene 0.125 0.0876 70.1 75.0-124 J4
1,2-Dibromo-3-Chloropropane 0.125 0.137 110 59.0-130
1,2-Dibromoethane 0.125 0.117 93.6 74.0-128
Dibromomethane 0.125 0.119 95.2 75.0-122
1,2-Dichlorobenzene 0.125 0.0993 79.4 76.0-124
1,3-Dichlorobenzene 0.125 0.0974 77.9 76.0-125
1,4-Dichlorobenzene 0.125 0.0993 79.4 77.0-121
Dichlorodifluoromethane 0.125 0.0882 70.6 43.0-156
1,1-Dichloroethane 0.125 0.113 90.4 70.0-127
1,2-Dichloroethane 0.125 0.0982 78.6 65.0-131
1,1-Dichloroethene 0.125 0.119 95.2 65.0-131
cis-1,2-Dichloroethene 0.125 0.107 85.6 73.0-125
trans-1,2-Dichloroethene 0.125 0.121 96.8 71.0-125
1,2-Dichloropropane 0.125 0.101 80.8 74.0-125
1,1-Dichloropropene 0.125 0.110 88.0 73.0-125
1,3-Dichloropropane 0.125 0.108 86.4 80.0-125
cis-1,3-Dichloropropene 0.125 0.0984 78.7 76.0-127
trans-1,3-Dichloropropene 0.125 0.100 80.0 73.0-127
2,2-Dichloropropane 0.125 0.112 89.6 59.0-135
Di-isopropyl ether 0.125 0.105 84.0 60.0-136
Ethylbenzene 0.125 0.112 89.6 74.0-126
Hexachloro-1,3-butadiene 0.125 0.0867 69.4 57.0-150
Isopropylbenzene 0.125 0.109 87.2 72.0-127
p-Isopropyltoluene 0.125 0.0971 77.7 72.0-133
2-Butanone (MEK)0.625 0.649 104 30.0-160
Methylene Chloride 0.125 0.114 91.2 68.0-123
4-Methyl-2-pentanone (MIBK)0.625 0.765 122 56.0-143
Methyl tert-butyl ether 0.125 0.108 86.4 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925553-1 05/14/23 06:08
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.0969 77.5 59.0-130
n-Propylbenzene 0.125 0.0881 70.5 74.0-126 J4
Styrene 0.125 0.101 80.8 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.117 93.6 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.123 98.4 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.126 101 61.0-139
Tetrachloroethene 0.125 0.114 91.2 70.0-136
Toluene 0.125 0.103 82.4 75.0-121
1,2,3-Trichlorobenzene 0.125 0.0941 75.3 59.0-139
1,2,4-Trichlorobenzene 0.125 0.0916 73.3 62.0-137
1,1,1-Trichloroethane 0.125 0.117 93.6 69.0-126
1,1,2-Trichloroethane 0.125 0.119 95.2 78.0-123
Trichloroethene 0.125 0.106 84.8 76.0-126
Trichlorofluoromethane 0.125 0.189 151 61.0-142 J4
1,2,3-Trichloropropane 0.125 0.120 96.0 67.0-129
1,2,4-Trimethylbenzene 0.125 0.0874 69.9 70.0-126 J4
1,2,3-Trimethylbenzene 0.125 0.0971 77.7 74.0-124
1,3,5-Trimethylbenzene 0.125 0.0923 73.8 73.0-127
Vinyl chloride 0.125 0.141 113 63.0-134
Xylenes, Total 0.375 0.302 80.5 72.0-127
(S) Toluene-d8 105 75.0-131
(S) 4-Bromofluorobenzene 96.6 67.0-138
(S) 1,2-Dichloroethane-d4 99.2 70.0-130
L1614238-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-03 05/14/23 12:42 • (MS) R3925553-3 05/14/23 17:05 • (MSD) R3925553-4 05/14/23 17:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.968 ND 0.376 0.389 38.9 40.2 1 10.0-160 3.27 40
Acrylonitrile 0.968 ND 0.798 0.754 82.4 77.9 1 10.0-160 5.63 40
Benzene 0.194 ND 0.162 0.155 83.9 80.3 1 10.0-149 4.32 37
Bromobenzene 0.194 ND 0.142 0.154 73.4 79.8 1 10.0-156 8.32 38
Bromodichloromethane 0.194 ND 0.159 0.154 82.3 79.4 1 10.0-143 3.59 37
Bromoform 0.194 ND 0.186 0.181 96.0 93.5 1 10.0-146 2.55 36
Bromomethane 0.194 ND 0.124 0.151 64.0 78.0 1 10.0-149 19.6 38
n-Butylbenzene 0.194 ND 0.162 0.176 83.9 91.1 1 10.0-160 8.29 40
sec-Butylbenzene 0.194 ND 0.155 0.165 80.0 85.5 1 10.0-159 6.63 39
tert-Butylbenzene 0.194 ND 0.147 0.161 76.2 83.1 1 10.0-156 8.61 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
L1614238-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-03 05/14/23 12:42 • (MS) R3925553-3 05/14/23 17:05 • (MSD) R3925553-4 05/14/23 17:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.194 ND 0.203 0.197 105 102 1 10.0-145 3.12 37
Chlorobenzene 0.194 ND 0.167 0.165 86.3 85.5 1 10.0-152 0.939 39
Chlorodibromomethane 0.194 ND 0.183 0.176 94.4 91.1 1 10.0-146 3.48 37
Chloroethane 0.194 ND 0.137 0.118 70.7 60.9 1 10.0-146 15.0 40
Chloroform 0.194 ND 0.152 0.147 78.5 76.1 1 10.0-146 3.03 37
Chloromethane 0.194 ND 0.179 0.169 92.7 87.1 1 10.0-159 6.28 37
2-Chlorotoluene 0.194 ND 0.159 0.169 82.3 87.1 1 10.0-159 5.71 38
4-Chlorotoluene 0.194 ND 0.120 0.142 62.0 73.1 1 10.0-155 16.5 39
1,2-Dibromo-3-Chloropropane 0.194 ND 0.167 0.165 86.3 85.5 1 10.0-151 0.939 39
1,2-Dibromoethane 0.194 ND 0.170 0.167 87.9 86.3 1 10.0-148 1.85 34
Dibromomethane 0.194 ND 0.154 0.148 79.6 76.4 1 10.0-147 4.14 35
1,2-Dichlorobenzene 0.194 ND 0.146 0.159 75.5 82.3 1 10.0-155 8.59 37
1,3-Dichlorobenzene 0.194 ND 0.147 0.161 75.9 83.1 1 10.0-153 9.03 38
1,4-Dichlorobenzene 0.194 ND 0.146 0.161 75.6 83.1 1 10.0-151 9.46 38
Dichlorodifluoromethane 0.194 ND 0.173 0.156 89.5 80.6 1 10.0-160 10.4 35
1,1-Dichloroethane 0.194 ND 0.158 0.159 81.5 82.3 1 10.0-147 0.985 37
1,2-Dichloroethane 0.194 ND 0.130 0.123 67.2 63.8 1 10.0-148 5.17 35
1,1-Dichloroethene 0.194 ND 0.206 0.197 106 102 1 10.0-155 4.65 37
cis-1,2-Dichloroethene 0.194 ND 0.165 0.156 85.5 80.4 1 10.0-149 6.13 37
trans-1,2-Dichloroethene 0.194 ND 0.179 0.178 92.7 91.9 1 10.0-150 0.873 37
1,2-Dichloropropane 0.194 ND 0.149 0.144 76.9 74.4 1 10.0-148 3.31 37
1,1-Dichloropropene 0.194 ND 0.178 0.181 91.9 93.5 1 10.0-153 1.74 35
1,3-Dichloropropane 0.194 ND 0.158 0.161 81.5 83.1 1 10.0-154 1.96 35
cis-1,3-Dichloropropene 0.194 ND 0.146 0.141 75.6 73.1 1 10.0-151 3.36 37
trans-1,3-Dichloropropene 0.194 ND 0.158 0.158 81.5 81.5 1 10.0-148 0.000 37
2,2-Dichloropropane 0.194 ND 0.108 0.106 56.0 54.8 1 10.0-138 2.18 36
Di-isopropyl ether 0.194 ND 0.150 0.145 77.3 74.9 1 10.0-147 3.07 36
Ethylbenzene 0.194 0.00453 0.175 0.167 88.0 84.0 1 10.0-160 4.57 38
Hexachloro-1,3-butadiene 0.194 ND 0.214 0.200 110 103 1 10.0-160 6.79 40
Isopropylbenzene 0.194 ND 0.167 0.161 86.3 83.1 1 10.0-155 3.81 38
p-Isopropyltoluene 0.194 ND 0.152 0.170 78.8 87.9 1 10.0-160 10.9 40
2-Butanone (MEK)0.968 ND 0.660 0.631 68.2 65.2 1 10.0-160 4.59 40
Methylene Chloride 0.194 0.0420 0.201 0.214 82.3 88.8 1 10.0-141 6.02 37
4-Methyl-2-pentanone (MIBK)0.968 ND 0.910 0.862 94.0 89.0 1 10.0-160 5.46 35
Methyl tert-butyl ether 0.194 ND 0.141 0.138 72.8 71.2 1 11.0-147 2.24 35
Naphthalene 0.194 0.0258 0.143 0.164 60.4 71.4 1 10.0-160 13.8 36
n-Propylbenzene 0.194 ND 0.142 0.156 73.6 80.6 1 10.0-158 9.10 38
Styrene 0.194 0.0272 0.184 0.189 81.1 83.5 1 10.0-160 2.51 40
1,1,1,2-Tetrachloroethane 0.194 ND 0.176 0.164 91.1 84.7 1 10.0-149 7.34 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
L1614238-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-03 05/14/23 12:42 • (MS) R3925553-3 05/14/23 17:05 • (MSD) R3925553-4 05/14/23 17:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.194 ND 0.158 0.158 81.5 81.5 1 10.0-160 0.000 35
1,1,2-Trichlorotrifluoroethane 0.194 ND 0.248 0.248 128 128 1 10.0-160 0.000 36
Tetrachloroethene 0.194 ND 0.215 0.211 111 109 1 10.0-156 2.20 39
Toluene 0.194 ND 0.179 0.179 90.1 90.1 1 10.0-156 0.000 38
1,2,3-Trichlorobenzene 0.194 ND 0.167 0.200 86.3 103 1 10.0-160 17.9 40
1,2,4-Trichlorobenzene 0.194 ND 0.161 0.190 83.1 98.4 1 10.0-160 16.9 40
1,1,1-Trichloroethane 0.194 ND 0.181 0.178 93.5 91.9 1 10.0-144 1.74 35
1,1,2-Trichloroethane 0.194 ND 0.173 0.167 89.5 86.3 1 10.0-160 3.67 35
Trichloroethene 0.194 ND 0.169 0.173 87.1 89.5 1 10.0-156 2.74 38
Trichlorofluoromethane 0.194 ND 0.243 0.189 126 97.6 1 10.0-160 25.3 40
1,2,3-Trichloropropane 0.194 ND 0.153 0.170 79.2 87.9 1 10.0-156 10.4 35
1,2,4-Trimethylbenzene 0.194 ND 0.145 0.152 71.8 75.3 1 10.0-160 4.53 36
1,2,3-Trimethylbenzene 0.194 ND 0.144 0.155 72.1 77.5 1 10.0-160 7.11 36
1,3,5-Trimethylbenzene 0.194 0.0151 0.146 0.161 67.8 75.3 1 10.0-160 9.46 38
Vinyl chloride 0.194 ND 0.183 0.178 94.4 91.9 1 10.0-160 2.60 37
Xylenes, Total 0.581 ND 0.495 0.484 83.7 81.8 1 10.0-160 2.23 38
(S) Toluene-d8 107 110 75.0-131
(S) 4-Bromofluorobenzene 97.4 94.6 67.0-138
(S) 1,2-Dichloroethane-d4 90.4 89.6 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2061264
Semi-Volatile Organic Compounds (GC) by Method 8015 L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3926233-1 05/17/23 20:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 55.9 18.0-148
Method Blank (MB)
(MB) R3926425-1 05/18/23 09:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range 2.22 J 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 87.8 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3926233-2 05/17/23 20:20
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 28.7 57.4 50.0-150
(S) o-Terphenyl 68.0 18.0-148
L1614205-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614205-01 05/17/23 21:51 • (MS) R3926233-3 05/17/23 22:04 • (MSD) R3926233-4 05/17/23 22:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 57.4 ND 32.3 32.7 56.4 56.7 1 50.0-150 1.07 20
(S) o-Terphenyl 57.6 53.2 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059033
Polychlorinated Biphenyls (GC) by Method 8082 L1614172-01,02,03,04
Method Blank (MB)
(MB) R3924792-1 05/15/23 00:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 97.9 10.0-135
(S) Tetrachloro-m-xylene 74.3 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3924792-5 05/15/23 01:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.113 67.7 36.0-141 P
PCB 1260 0.167 0.122 73.1 37.0-145 P
(S) Decachlorobiphenyl 87.1 10.0-135
(S) Tetrachloro-m-xylene 78.2 10.0-139
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/15/23 04:34 • (MS) R3924792-6 05/15/23 05:03 • (MSD) R3924792-7 05/15/23 05:13
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.177 ND 0.112 0.100 63.0 57.1 1 10.0-160 P P 11.0 37
PCB 1260 0.177 ND 0.115 0.116 64.8 66.3 1 10.0-160 P P 0.948 38
(S) Decachlorobiphenyl 73.1 73.1 10.0-135
(S) Tetrachloro-m-xylene 72.1 70.7 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059034
Polychlorinated Biphenyls (GC) by Method 8082 L1614172-05
Method Blank (MB)
(MB) R3925344-1 05/15/23 01:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 0.000 J2 10.0-135
(S) Tetrachloro-m-xylene 0.000 J2 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3925344-5 05/15/23 01:42
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0690 41.3 36.0-141
PCB 1260 0.167 0.0777 46.5 37.0-145
(S) Decachlorobiphenyl 49.4 10.0-135
(S) Tetrachloro-m-xylene 44.0 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3925411-2 05/13/23 21:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3925411-2 05/13/23 21:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 44.4 10.0-122
(S) 2-Fluorobiphenyl 52.6 15.0-120
(S) p-Terphenyl-d14 64.3 10.0-120
(S) Phenol-d5 47.4 10.0-120
(S) 2-Fluorophenol 52.9 12.0-120
(S) 2,4,6-Tribromophenol 56.0 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3925411-1 05/13/23 20:49
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.412 61.9 38.0-120
Acenaphthylene 0.666 0.423 63.5 40.0-120
Anthracene 0.666 0.469 70.4 42.0-120
Benzidine 1.33 0.345 25.9 10.0-120
Benzo(a)anthracene 0.666 0.487 73.1 44.0-120
Benzo(b)fluoranthene 0.666 0.448 67.3 43.0-120
Benzo(k)fluoranthene 0.666 0.449 67.4 44.0-120
Benzo(g,h,i)perylene 0.666 0.465 69.8 43.0-120
Benzo(a)pyrene 0.666 0.490 73.6 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.346 52.0 20.0-120
Bis(2-chloroethyl)ether 0.666 0.402 60.4 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.394 59.2 23.0-120
4-Bromophenyl-phenylether 0.666 0.467 70.1 40.0-120
2-Chloronaphthalene 0.666 0.403 60.5 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925411-1 05/13/23 20:49
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.429 64.4 40.0-120
Chrysene 0.666 0.452 67.9 43.0-120
Dibenz(a,h)anthracene 0.666 0.469 70.4 44.0-120
3,3-Dichlorobenzidine 1.33 0.930 69.9 28.0-120
2,4-Dinitrotoluene 0.666 0.466 70.0 45.0-120
2,6-Dinitrotoluene 0.666 0.409 61.4 42.0-120
Fluoranthene 0.666 0.473 71.0 44.0-120
Fluorene 0.666 0.427 64.1 41.0-120
Hexachlorobenzene 0.666 0.492 73.9 39.0-120
Hexachloro-1,3-butadiene 0.666 0.372 55.9 15.0-120
Hexachlorocyclopentadiene 0.666 0.469 70.4 15.0-120
Hexachloroethane 0.666 0.376 56.5 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.441 66.2 45.0-120
Isophorone 0.666 0.333 50.0 23.0-120
Naphthalene 0.666 0.352 52.9 18.0-120
Nitrobenzene 0.666 0.311 46.7 17.0-120
n-Nitrosodimethylamine 0.666 0.314 47.1 10.0-125
n-Nitrosodiphenylamine 0.666 0.439 65.9 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.377 56.6 26.0-120
Phenanthrene 0.666 0.448 67.3 42.0-120
Benzylbutyl phthalate 0.666 0.470 70.6 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.448 67.3 41.0-120
Di-n-butyl phthalate 0.666 0.491 73.7 43.0-120
Diethyl phthalate 0.666 0.449 67.4 43.0-120
Dimethyl phthalate 0.666 0.448 67.3 43.0-120
Di-n-octyl phthalate 0.666 0.423 63.5 40.0-120
Pyrene 0.666 0.431 64.7 41.0-120
1,2,4-Trichlorobenzene 0.666 0.376 56.5 17.0-120
4-Chloro-3-methylphenol 0.666 0.361 54.2 28.0-120
2-Chlorophenol 0.666 0.408 61.3 28.0-120
2,4-Dichlorophenol 0.666 0.375 56.3 25.0-120
2,4-Dimethylphenol 0.666 0.358 53.8 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.347 52.1 16.0-120
2,4-Dinitrophenol 0.666 0.220 33.0 10.0-120
2-Nitrophenol 0.666 0.360 54.1 20.0-120
4-Nitrophenol 0.666 0.311 46.7 27.0-120
Pentachlorophenol 0.666 0.469 70.4 29.0-120
Phenol 0.666 0.353 53.0 28.0-120
2,4,6-Trichlorophenol 0.666 0.369 55.4 37.0-120
(S) Nitrobenzene-d5 48.0 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925411-1 05/13/23 20:49
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 63.4 15.0-120
(S) p-Terphenyl-d14 72.7 10.0-120
(S) Phenol-d5 57.7 10.0-120
(S) 2-Fluorophenol 67.7 12.0-120
(S) 2,4,6-Tribromophenol 83.5 10.0-127
L1614172-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614172-05 05/14/23 00:45 • (MS) R3925411-3 05/14/23 01:07 • (MSD) R3925411-4 05/14/23 01:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.852 ND 0.368 0.362 43.1 42.7 1 18.0-120 1.42 32
Acenaphthylene 0.852 ND 0.382 0.369 44.8 43.4 1 25.0-120 3.46 32
Anthracene 0.852 ND 0.426 0.399 50.0 46.9 1 22.0-120 6.61 29
Benzidine 1.70 ND ND ND 7.57 8.09 1 10.0-120 J6 J6 6.63 40
Benzo(a)anthracene 0.852 ND 0.450 0.414 52.7 48.8 1 25.0-120 8.12 29
Benzo(b)fluoranthene 0.852 ND 0.407 0.375 47.7 44.2 1 19.0-122 7.97 31
Benzo(k)fluoranthene 0.852 ND 0.390 0.361 45.7 42.5 1 23.0-120 7.61 30
Benzo(g,h,i)perylene 0.852 ND 0.408 0.357 47.9 42.0 1 10.0-120 13.2 33
Benzo(a)pyrene 0.852 ND 0.451 0.412 52.9 48.5 1 24.0-120 9.04 30
Bis(2-chlorethoxy)methane 0.852 ND ND ND 35.1 35.6 1 10.0-120 1.30 34
Bis(2-chloroethyl)ether 0.852 ND ND ND 38.4 38.8 1 10.0-120 0.791 40
2,2-Oxybis(1-Chloropropane)0.852 ND ND ND 37.2 38.7 1 10.0-120 3.62 40
4-Bromophenyl-phenylether 0.852 ND 0.438 ND 51.4 48.8 1 27.0-120 5.49 30
2-Chloronaphthalene 0.852 ND 0.360 0.357 42.2 42.0 1 20.0-120 0.725 32
4-Chlorophenyl-phenylether 0.852 ND ND ND 46.5 44.8 1 24.0-120 4.01 29
Chrysene 0.852 ND 0.409 0.379 48.0 44.6 1 21.0-120 7.58 29
Dibenz(a,h)anthracene 0.852 ND 0.427 0.381 50.2 44.8 1 10.0-120 11.6 32
3,3-Dichlorobenzidine 1.70 ND 0.648 0.676 38.1 39.7 1 10.0-120 4.12 34
2,4-Dinitrotoluene 0.852 ND ND ND 50.2 48.9 1 30.0-120 2.77 31
2,6-Dinitrotoluene 0.852 ND ND ND 46.2 46.2 1 25.0-120 0.331 31
Fluoranthene 0.852 ND 0.435 0.409 51.1 48.2 1 18.0-126 6.15 32
Fluorene 0.852 ND 0.390 0.375 45.7 44.2 1 25.0-120 3.74 30
Hexachlorobenzene 0.852 ND 0.448 ND 52.6 49.1 1 27.0-120 7.21 28
Hexachloro-1,3-butadiene 0.852 ND ND ND 37.0 37.9 1 10.0-120 2.04 38
Hexachlorocyclopentadiene 0.852 ND ND ND 23.5 21.6 1 10.0-120 8.81 40
Hexachloroethane 0.852 ND ND ND 33.5 35.0 1 10.0-120 4.01 40
Indeno(1,2,3-cd)pyrene 0.852 ND 0.422 0.383 49.5 45.1 1 10.0-120 9.68 32
Isophorone 0.852 ND ND ND 34.0 34.6 1 13.0-120 1.34 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
L1614172-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614172-05 05/14/23 00:45 • (MS) R3925411-3 05/14/23 01:07 • (MSD) R3925411-4 05/14/23 01:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.852 ND 0.305 0.309 35.8 36.4 1 10.0-120 1.27 35
Nitrobenzene 0.852 ND ND ND 31.6 32.3 1 10.0-120 1.91 36
n-Nitrosodimethylamine 0.852 ND ND ND 23.5 23.4 1 10.0-127 0.651 40
n-Nitrosodiphenylamine 0.852 ND ND ND 47.9 45.9 1 17.0-120 4.56 29
n-Nitrosodi-n-propylamine 0.852 ND ND ND 37.5 37.3 1 10.0-120 0.816 37
Phenanthrene 0.852 ND 0.408 0.383 47.9 45.1 1 17.0-120 6.24 31
Benzylbutyl phthalate 0.852 ND 0.477 0.443 55.9 52.1 1 23.0-120 7.34 30
Bis(2-ethylhexyl)phthalate 0.852 ND 0.438 ND 51.4 48.2 1 17.0-126 6.75 30
Di-n-butyl phthalate 0.852 ND 0.461 ND 54.1 50.3 1 30.0-120 7.60 29
Diethyl phthalate 0.852 ND ND ND 47.7 46.2 1 26.0-120 3.58 28
Dimethyl phthalate 0.852 ND ND ND 47.9 45.9 1 25.0-120 4.56 29
Di-n-octyl phthalate 0.852 ND 0.452 ND 53.0 50.6 1 21.0-123 5.01 29
Pyrene 0.852 ND 0.400 0.374 47.0 44.0 1 16.0-121 6.71 32
1,2,4-Trichlorobenzene 0.852 ND ND ND 38.7 40.1 1 12.0-120 3.10 37
4-Chloro-3-methylphenol 0.852 ND ND ND 39.0 38.1 1 15.0-120 2.77 30
2-Chlorophenol 0.852 ND ND ND 41.0 41.9 1 15.0-120 1.84 37
2,4-Dichlorophenol 0.852 ND ND ND 43.9 44.2 1 20.0-120 0.347 31
2,4-Dimethylphenol 0.852 ND ND ND 15.4 18.2 1 10.0-120 16.4 33
4,6-Dinitro-2-methylphenol 0.852 ND ND ND 32.2 27.4 1 10.0-120 16.4 39
2,4-Dinitrophenol 0.852 ND ND ND 22.1 20.2 1 10.0-121 9.39 40
2-Nitrophenol 0.852 ND ND ND 41.0 42.0 1 12.0-120 2.21 39
4-Nitrophenol 0.852 ND ND ND 11.5 15.4 1 10.0-137 29.0 32
Pentachlorophenol 0.852 ND 0.435 ND 51.1 43.4 1 10.0-160 16.5 31
Phenol 0.852 ND ND ND 23.8 26.0 1 12.0-120 8.59 38
2,4,6-Trichlorophenol 0.852 ND ND ND 40.1 37.8 1 19.0-120 6.27 32
(S) Nitrobenzene-d5 33.5 33.6 10.0-122
(S) 2-Fluorobiphenyl 43.9 43.4 15.0-120
(S) p-Terphenyl-d14 53.4 48.9 10.0-120
(S) Phenol-d5 35.2 36.2 10.0-120
(S) 2-Fluorophenol 42.7 42.7 12.0-120
(S) 2,4,6-Tribromophenol 58.5 59.2 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059490
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-02,03,04
Method Blank (MB)
(MB) R3925884-2 05/17/23 00:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 90.5 23.0-120
(S) Nitrobenzene-d5 68.9 14.0-149
(S) 2-Fluorobiphenyl 68.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3925884-1 05/17/23 00:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0885 111 50.0-126
Acenaphthene 0.0800 0.0833 104 50.0-120
Acenaphthylene 0.0800 0.0819 102 50.0-120
Benzo(a)anthracene 0.0800 0.112 140 45.0-120 J4
Benzo(a)pyrene 0.0800 0.0937 117 42.0-120
Benzo(b)fluoranthene 0.0800 0.105 131 42.0-121 J4
Benzo(g,h,i)perylene 0.0800 0.0906 113 45.0-125
Benzo(k)fluoranthene 0.0800 0.0932 117 49.0-125
Chrysene 0.0800 0.110 138 49.0-122 J4
Dibenz(a,h)anthracene 0.0800 0.0906 113 47.0-125
Fluoranthene 0.0800 0.0970 121 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059490
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3925884-1 05/17/23 00:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0874 109 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.102 128 46.0-125 J4
Naphthalene 0.0800 0.0771 96.4 50.0-120
Phenanthrene 0.0800 0.0865 108 47.0-120
Pyrene 0.0800 0.0931 116 43.0-123
1-Methylnaphthalene 0.0800 0.0788 98.5 51.0-121
2-Methylnaphthalene 0.0800 0.0836 105 50.0-120
2-Chloronaphthalene 0.0800 0.0801 100 50.0-120
(S) p-Terphenyl-d14 92.7 23.0-120
(S) Nitrobenzene-d5 105 14.0-149
(S) 2-Fluorobiphenyl 88.8 34.0-125
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/17/23 05:08 • (MS) R3925884-3 05/17/23 05:26 • (MSD) R3925884-4 05/17/23 05:44
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0876 ND 0.0904 0.0951 103 109 1 10.0-145 5.07 30
Acenaphthene 0.0876 ND 0.0821 0.0865 93.8 98.8 1 14.0-127 5.19 27
Acenaphthylene 0.0876 ND 0.0803 0.0851 91.6 97.1 1 21.0-124 5.83 25
Benzo(a)anthracene 0.0876 ND 0.0913 0.0974 104 111 1 10.0-139 6.50 30
Benzo(a)pyrene 0.0876 ND 0.0902 0.0958 103 109 1 10.0-141 6.00 31
Benzo(b)fluoranthene 0.0876 ND 0.0926 0.100 106 115 1 10.0-140 7.95 36
Benzo(g,h,i)perylene 0.0876 ND 0.0549 0.0530 62.6 60.5 1 10.0-140 3.45 33
Benzo(k)fluoranthene 0.0876 ND 0.0881 0.0943 101 108 1 10.0-137 6.72 31
Chrysene 0.0876 ND 0.0874 0.0937 99.8 107 1 10.0-145 7.01 30
Dibenz(a,h)anthracene 0.0876 ND 0.0554 0.0530 63.3 60.5 1 10.0-132 4.44 31
Fluoranthene 0.0876 ND 0.0926 0.0999 106 114 1 10.0-153 7.51 33
Fluorene 0.0876 ND 0.0896 0.0938 102 107 1 11.0-130 4.66 29
Indeno(1,2,3-cd)pyrene 0.0876 ND 0.0585 0.0564 66.8 64.4 1 10.0-137 3.62 32
Naphthalene 0.0876 ND 0.0693 0.0774 79.1 88.4 1 10.0-135 11.0 27
Phenanthrene 0.0876 ND 0.0859 0.0927 98.1 106 1 10.0-144 7.60 31
Pyrene 0.0876 ND 0.0877 0.0939 100 107 1 10.0-148 6.87 35
1-Methylnaphthalene 0.0876 ND 0.0746 0.0813 85.1 92.9 1 10.0-142 8.71 28
2-Methylnaphthalene 0.0876 ND 0.0789 0.0858 90.1 98.0 1 10.0-137 8.37 28
2-Chloronaphthalene 0.0876 ND 0.0764 0.0820 87.3 93.6 1 29.0-120 7.05 24
(S) p-Terphenyl-d14 92.2 94.4 23.0-120
(S) Nitrobenzene-d5 76.1 91.1 14.0-149
(S) 2-Fluorobiphenyl 71.3 78.9 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059491
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-05
Method Blank (MB)
(MB) R3924997-2 05/15/23 13:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 108 23.0-120
(S) Nitrobenzene-d5 94.8 14.0-149
(S) 2-Fluorobiphenyl 85.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3924997-1 05/15/23 13:23
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0761 95.1 50.0-126
Acenaphthene 0.0800 0.0727 90.9 50.0-120
Acenaphthylene 0.0800 0.0785 98.1 50.0-120
Benzo(a)anthracene 0.0800 0.0809 101 45.0-120
Benzo(a)pyrene 0.0800 0.0718 89.8 42.0-120
Benzo(b)fluoranthene 0.0800 0.0826 103 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0753 94.1 45.0-125
Benzo(k)fluoranthene 0.0800 0.0774 96.8 49.0-125
Chrysene 0.0800 0.0870 109 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0781 97.6 47.0-125
Fluoranthene 0.0800 0.0844 105 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059491
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-05
Laboratory Control Sample (LCS)
(LCS) R3924997-1 05/15/23 13:23
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0847 106 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0840 105 46.0-125
Naphthalene 0.0800 0.0784 98.0 50.0-120
Phenanthrene 0.0800 0.0835 104 47.0-120
Pyrene 0.0800 0.0875 109 43.0-123
1-Methylnaphthalene 0.0800 0.0837 105 51.0-121
2-Methylnaphthalene 0.0800 0.0791 98.9 50.0-120
2-Chloronaphthalene 0.0800 0.0799 99.9 50.0-120
(S) p-Terphenyl-d14 107 23.0-120
(S) Nitrobenzene-d5 110 14.0-149
(S) 2-Fluorobiphenyl 105 34.0-125
L1614496-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614496-02 05/15/23 14:32 • (MS) R3924997-3 05/15/23 14:50 • (MSD) R3924997-4 05/15/23 15:07
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.105 ND 0.0661 0.0901 62.8 88.1 1 10.0-145 J3 30.7 30
Acenaphthene 0.105 ND 0.0643 0.0842 61.0 82.3 1 14.0-127 26.8 27
Acenaphthylene 0.105 ND 0.0729 0.0918 69.1 89.8 1 21.0-124 23.0 25
Benzo(a)anthracene 0.105 ND 0.0697 0.0945 66.1 92.4 1 10.0-139 J3 30.2 30
Benzo(a)pyrene 0.105 ND 0.0718 0.0974 68.1 95.2 1 10.0-141 30.2 31
Benzo(b)fluoranthene 0.105 ND 0.0642 0.0934 60.9 91.4 1 10.0-140 J3 37.1 36
Benzo(g,h,i)perylene 0.105 ND 0.0661 0.0942 62.8 92.1 1 10.0-140 J3 35.0 33
Benzo(k)fluoranthene 0.105 ND 0.0718 0.0934 68.1 91.4 1 10.0-137 26.2 31
Chrysene 0.105 ND 0.0837 0.106 79.4 103 1 10.0-145 23.1 30
Dibenz(a,h)anthracene 0.105 ND 0.0810 0.102 76.9 100 1 10.0-132 23.4 31
Fluoranthene 0.105 ND 0.0655 0.101 62.1 99.1 1 10.0-153 J3 43.0 33
Fluorene 0.105 ND 0.0710 0.0960 67.4 93.9 1 11.0-130 J3 30.0 29
Indeno(1,2,3-cd)pyrene 0.105 ND 0.0693 0.0966 65.8 94.5 1 10.0-137 J3 32.9 32
Naphthalene 0.105 ND 0.0839 0.0937 79.6 91.6 1 10.0-135 11.0 27
Phenanthrene 0.105 ND 0.0672 0.102 63.8 99.5 1 10.0-144 J3 40.9 31
Pyrene 0.105 ND 0.0682 0.104 64.8 102 1 10.0-148 J3 41.6 35
1-Methylnaphthalene 0.105 ND 0.0802 0.0983 76.1 96.1 1 10.0-142 20.2 28
2-Methylnaphthalene 0.105 ND 0.0759 0.0910 72.0 89.0 1 10.0-137 18.2 28
2-Chloronaphthalene 0.105 ND 0.0746 0.0925 70.8 90.5 1 29.0-120 21.5 24
(S) p-Terphenyl-d14 64.9 85.8 23.0-120
(S) Nitrobenzene-d5 95.8 84.7 14.0-149
(S) 2-Fluorobiphenyl 63.4 70.2 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062088
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-01
Method Blank (MB)
(MB) R3926686-2 05/18/23 16:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 99.5 23.0-120
(S) Nitrobenzene-d5 68.0 14.0-149
(S) 2-Fluorobiphenyl 83.7 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3926686-1 05/18/23 16:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0762 95.3 50.0-126
Acenaphthene 0.0800 0.0813 102 50.0-120
Acenaphthylene 0.0800 0.0751 93.9 50.0-120
Benzo(a)anthracene 0.0800 0.0740 92.5 45.0-120
Benzo(a)pyrene 0.0800 0.0784 98.0 42.0-120
Benzo(b)fluoranthene 0.0800 0.0885 111 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0905 113 45.0-125
Benzo(k)fluoranthene 0.0800 0.0868 109 49.0-125
Chrysene 0.0800 0.0865 108 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0870 109 47.0-125
Fluoranthene 0.0800 0.0809 101 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062088
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-01
Laboratory Control Sample (LCS)
(LCS) R3926686-1 05/18/23 16:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0785 98.1 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0840 105 46.0-125
Naphthalene 0.0800 0.0819 102 50.0-120
Phenanthrene 0.0800 0.0816 102 47.0-120
Pyrene 0.0800 0.0827 103 43.0-123
1-Methylnaphthalene 0.0800 0.0796 99.5 51.0-121
2-Methylnaphthalene 0.0800 0.0817 102 50.0-120
2-Chloronaphthalene 0.0800 0.0819 102 50.0-120
(S) p-Terphenyl-d14 98.7 23.0-120
(S) Nitrobenzene-d5 75.8 14.0-149
(S) 2-Fluorobiphenyl 89.7 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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