DSHW-2023-211360 - 0901a068812b1ff4

11/6/23, 10:07 AM State of Utah Mail - Revised Recycled Earth Site Characterization Completion Report
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Revised Recycled Earth Site Characterization Completion Report
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Rasmuson, Anna <[e-mail]>Fri, Nov 3, 2023 at 4:30 PM
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Cc: "Wadman, Heather" <[e-mail]>, "Wilson, DavidWilson" <[e-mail]>,
"Cahoon, Tyler R." <[e-mail]>, "Cahoon, Brad R." <[e-mail]>, David Rawson
<[e-mail]>, Wade Hess <[e-mail]>, "Nielsen, Taylor" <[e-mail]>,
"Anderson, Justin" <[e-mail]>
Director Hansen,
Please see the revised Site Characterization Report and Recycled Earth’s responses to agency comments found here:
Revised Recycled Earth Site Characterization Report
Please let us know if you have any questions or if you encounter any issues accessing the report.
Regards,
Anna
Anna Rasmuson, Ph.D., P.G. | Geological Engineer
Pronouns: she, her, hers
Mobile [phone] | [e-mail]
Tetra Tech | Leading with Science® | ECA
4750 W. 2100 S., Suite. 400. | Salt Lake City, UT 84120 | tetratech.com
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DSHW-2023-211360
_6479224.2
RESPONSES TO COMMENTS (RTC) FROM UDEQ-DWMRC
Site Characterization Completion Report for Recycled Earth South Property

The comments provided by the Utah Department of Environmental Quality, Division of Waste Management
and Radiation Control (Division) dated October 5, 2023, are copied below, with responses to the comments
prepared by Tetra Tech on behalf of Recycled Earth provided in blue font. These responses are provided to
accompany the revised Site Characterization Completion Report for Recycled Earth South Property (Report)
to be concurrently re-submitted to the Division.

1. Section 1.0 Introduction
The first paragraph states that a singular discharge was received from one Recycled Earth customer. This
discharge is described as responsible for an odor, leading to Ogden City’s subsequent investigation, and
the Division’s request for investigation of any potential contamination from disposal of unauthorized
liquid wastes on the site. According to records provided to Ogden City and the Division by Recycled
Earth of historical releases at the site, there were several liquid waste loads accepted from multiple
customers between February and August 2022. Any one or several of these accepted liquid waste
disposals could have caused the purported contamination. Please update the report to reflect this
information.
Response: The indicated text has been revised in the Report as directed by DWMRC. However, the
Division’s assertion that the contamination could have come from customers other than Beck Sanitation
Inc. (BSI), is inaccurate. Recycled Earth has obtained evidence proving that BSI was the only customer
who offloaded wastewater at the South Property. Recycled Earth is litigating its claims against BSI in the
district court.

2. Section 1.2 Historical Releases
Again, throughout this section, a singular release has been identified as the cause of the odor and
subsequent investigations by Ogden City and the Division. Additionally, the third paragraph of this
section states that Ogden City and the Division identified an unauthorized release by the singular
customer as the cause in their respective Notice of Violation and Request. This is not correct; neither
Ogden City nor the Division have identified a singular disposal as the primary interest in this
investigation. It is the Division’s understanding that Recycled Earth LLC did not know the nature of
accepted liquid waste loads and that there were multiple loads from multiple customers. A responsible
party should not be named without sufficient records that characterize the waste received all parties
that disposed of liquid waste at Recycled Earth LLC. Please update the report to reflect this information.

Response: See Response No. 1. However, Section 1.2 has been revised to reflect the language presented
in the Site Characterization Plan that was originally approved by the Division and Ogden City.

3. Section 2.1.3 Catch Basin Cleanout, Section 2.1.4 Excavation Near Maintenance Building
Please provide waste manifests for the catch basin cleanout and the excavation near the maintenance
building.

_6479224.2
Response: Waste manifests for the catch basin cleanout and excavation near the maintenance building
have been added to Appendix A of the Report.

4. Section 3.3.1 French Drain Sample Results
In the Division’s December 5, 2022, letter (DSHW-2022-026972) that detailed comments on the site
characterization plan, the Division states “For future soil and water analysis, please note that the
Division does not recognize the use of the Division of Environmental Response and Remediation (DERR)
Initial Screening Levels (ISL) for soil and groundwater. In lieu of that, the acceptable screening standards
for all media of concern will be the US EPA Regional Screening Level, (EPA RSLs).” Please update the Site
Characterization Report to use EPA RSL’s for French drain groundwater sample results.

Response: Recycled Earth’s technical consultant Tetra Tech and legal counsel Dentons Durham Jones
Pinegar strongly oppose application of the Tap Water RSLs because there is no current or anticipated
future use of groundwater as tap water at the South Property and because shallow groundwater at the
south property and all other properties along the Wasatch Front is not a suitable for drinking water and
cannot be used for this purpose without extensive treatment to remove high concentrations of total
dissolved solids (TDS). The only water-related screening levels on the EPA RSLs are for drinking water,
i.e., Tap Water levels and Maximum Contaminant Levels (MCLs). However, Recycled Earth agrees to add
the MCLs to Table 6.

Recycled Earth recognizes that there is no MCL or Utah Groundwater Quality Standard for TPH-DRO. As
a conservative approach and at the direction of the DWMRC, EPA Tap Water RSLs were added to the
Report for screening purposes for indicator compounds specified in Table 5 of the Division’s Technical
Guide for Risk Assessments Section 5.2.7. The Guide states that risk from TPH should be evaluated by
assessing individual chemical constituents rather than relying on TPH fraction data. All french drain
groundwater detections were below the MCLs and Tap Water levels for the indicator compounds except
for arsenic. We have revised The Report text and Table 6 to reflect this comparison and the prior
references to the ISLs have been removed as directed. Background concentration for arsenic will be
further evaluated per the method to be presented in the forthcoming Site Management Plan.

5. Section 3.4.2 Groundwater Sample Results
In the Division’s December 5, 2022, letter (DSHW-2022-026972) that detailed comments on the site
characterization plan, the Division states: “For future soil and water analysis, please note that the
Division does not recognize the use of the Division of Environmental Response and Remediation
(DERR) Initial Screening Levels (ISL) for soil and groundwater. In lieu of that, the acceptable
screening standards for all media of concern will be the US EPA Regional Screening Level, (EPA
RSLs).” Please update the Site Characterization Report to use EPA RSL’s for groundwater sample
results.

Response: Recycled Earth’s response to this comment is the same as for Response No. 4. Table 11 has
been revised to include conservative comparisons of results to the MCLs and EPA Tap Water RSLs for
TPH indicator compounds. All groundwater detections were below the MCLs and Tap Water levels for
the indicator compounds except for arsenic and manganese. Background concentrations for arsenic and
_6479224.2
manganese will be further evaluated per the method to be presented in the forthcoming Site
Management Plan.

6. Section 3.6 Conceptual Site Model
According to Utah Administrative Code (UAC) R315-101-5 (d), the conceptual site model shall include a
determination as to whether or not any potential exposure pathways for subsurface soils are complete
under both current and anticipated future conditions. For any exposure pathways that have a
reasonable potential for being complete, associated risks shall be evaluated.

Section 2.3 of the report states that the French drain invert depth, where sample FD-1 was taken, is
approximately five feet below ground surface. Utah Administrative Code R315-101-5 (d)(3) describes
that the soil exposure interval applicable to the construction worker is defined as surface down to depth
of construction of ten feet below ground surface. Because the French drain soil depth is within surface
down to ten feet below ground surface, the exposure pathway has reasonable potential for being
complete. Therefore, to protect workers on any future construction activity at the site, please update
the Site Characterization Report to include evaluated risks associated with contaminant exposure depth
from surface to ten feet below ground surface.

Response: Based on this comment, Recycled Earth completed further remediation by excavating soils
from the area of french drain soil sample FD-1. This work was performed as described in email
correspondence sent by Tetra Tech to the Division on October 13, 2023. A description of this work and
the results from confirmation sampling after soil removal have been added to Section 3.3.1 of the
Report. Because the three confirmation sample results collected from the excavation floor and sidewalls
showed arsenic concentrations below the established background concentration of 15 mg/kg, there is
no remaining exposure pathway for subsurface soils and no further assessment or remediation is
required for this area.

7. Section 4.1 Summary of Findings
As detailed in Number 6 above, the conceptual site model should indicate the risks associated with
French drain sample FD-1 arsenic levels from ground surface to ten feet below ground surface. The
Summary of Findings section should be updated to detail any necessary remediation or additional
sampling needed for the mitigation of those risks, to occur before site closure.

Bullet three in Section 4.1 states that data suggests the elevated arsenic detections in groundwater at
the site are naturally occurring. Although this may be accurate, variations in groundwater arsenic levels
downstream from MW-1 indicate an increase in arsenic levels within the site. Arsenic groundwater
background concentration should be established, and further groundwater monitoring and analysis
must occur, to make this, or any other groundwater determination.

Arsenic groundwater background concentration should be established through upgradient groundwater
sampling and further on-site groundwater monitoring shall be used to establish constituent
concentration trends to determine if arsenic or other groundwater constituents are shown to be above
background concentration. For any on-site constituent concentrations shown to be above background,
_6479224.2
potential contamination of downstream resources (i.e., the site storm system if the French drain is
reconnected, the Hooper Water Improvement District, and any other potential contamination source
downstream from the site) should then be addressed.

A plan for future groundwater monitoring and analysis, including background constituent
determinations and monitoring objectives, should be included as an attachment in the upcoming Site
Management Plan.

Please note, for the proposed future groundwater monitoring, the constituent standards should be the
U.S. EPA Total Petroleum Hydrocarbons Diesel Range Organics (TPH DRO) RSL standard (ensuring that
the analytical method to be used is consistent with the U.S. EPA TPH DRO analytical Method for
applicability) or a semi-volatile organic compounds (SVOC) analysis to represent the TPH DRO should be
used. The standards for the SVOC constituents detected in groundwater are available in the EPA RSL
Table and are listed as the maximum contaminant level (MCL) values. If the MCL value is not available,
the default value shall be the Tap Water value. If both values are available, the greater of the two values
shall be the standard. See the Division’s Technical Guide for Risk Assessments Section 5.2.7. for further
instructions.

Response: Recycled Earth has revised Section 4.2 of the Report to include a plan for future groundwater
monitoring and background constituent determination for arsenic in the forthcoming SMP; and based
on conservative comparison of groundwater results to the EPA Tap Water RSLs for TPH indicator
compounds, manganese will require similar evaluation. Arsenic and manganese concentrations in the
south property groundwater will be further evaluated to develop site-specific background values per the
method to be presented in the forthcoming SMP.

8. Section 4.2 Recommendations
Recommendations should reflect the changes made in the Conceptual Site Model and Summary of
Findings sections. This may include, but is not limited to, further sampling and remediation of soil from
ground surface to ten feet at the French drain FD-1 sample area before site closure.

Response: Section 4.2 has been updated to reflect the further remediation through soil excavation and
removal at the FD-1 sample location. Confirmation samples results and supporting information about
this remediation work are provided in a new Appendix H in the Report.

9. Tables
Table 6 – French Drain Sample Detections and Table 11 – Groundwater Monitoring Well Sample
Detections should include EPA RSLs.

Response: Please Response No. 4. Tables 6 and 11 have been updated to include the TPH indicator
compounds listed in Table 5 of the Division’s Technical Guide for Risk Assessments Section 5.2.7.

10. Figures
Please verify the depth of monitoring well MW-1; the depth specified in Figure 10 may be a typo.
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Response: Please note that Figure 10 presents groundwater elevations, not depths. The legend has been
revised for clarity on this matter.
11. In addition, a reminder that an updated plan of operations for Recycled Earth South Property must be
submitted to the Division. Currently, construction and demolition (C&D) wastes are approved to be
received at the recycling facility, located on the north property of Recycled Earth, for recycling purposes
only. The management of C&D wastes on the southern campus, along with the unauthorized dumping of
liquid wastes, has not been reviewed or approved by the Division. The updated plan of operations does
not need to be included in the revised Site Characterization Report, but any changes to the facility’s
operation or construction resulting from the site investigation, characterization, and management plan
must be reflected in the updated plan of operations.

Response: An updated Plan of Operations will be prepared and provided to DWMRC by Recycled Earth;
it will be submitted separately from the Site Characterization Report.

RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
1 The NOV was issued by Ogden City Public
Services on September 30, 2022 for a
purported illicit discharge on the Site by
one of Recycled Earth’s customers to the
Ogden City Municipal Storm Sewer
System (MS4).
This phrase should be deleted. The NOV
made no reference to Beck SanitaƟon as
the illicit discharge source, as this sentence
implies.
The indicated text has been deleted from
the Site CharacterizaƟon Report (Report).
2 According to Recycled Earth, Recycled
Earth, no significant spills or releases
have occurred at the Site.
Add "prior to the August 2022 illicit
discharge."
The requested text has been added to the
Report.
3 Except for the purported release of
unauthorized liquid waste by Beck’s
SanitaƟon, Inc. idenƟfied by the City and
UDEQ in their respecƟve NOV and
Request as described previously and
described in the Ɵmeline below, Recycled
Earth is unaware of other significant
releases on or from the Site.
Delete this phrase as it implies that the
NOV idenƟfied Beck SanitaƟon as
responsible for the illicit discharge, which
the NOV does not do.
The indicated text has been deleted from
the Report.

It was not Recycled Earth’s intenƟon to
suggest that Beck SanitaƟon Inc. (BSI) was
idenƟfied in the NOV, but rather the original
language was to document which Recycled
Earth customer had discharged impacted
water to the south property and was
ulƟmately responsible for the
contaminaƟon. Recycled Earth has obtained
evidence proving that BSI was the only
customer who offloaded wastewater at the
South Property. Recycled Earth is liƟgaƟng its
claims against BSI in the district court.

4 August 24: 2022 - Ogden City terminated
Recycled Earth's access to the MS4 due to
the detecƟon of illicit discharge of
pollutants or water containing pollutants
to the MS4 by Beck’s SanitaƟon, Inc.
Revise to "suspended Recycled Earth's
access to the MS4 for 30 days. . ." Ogden
City has never terminated Recycled Earth's
access to the MS4. The City suspended
access for 30 days on 8/24 and the 9/30
NOV suspended access indefinitely, pending
compliance with the City's orders.
The indicated text has been revised in the
Report as requested.
RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
5 The released water flowed into Ogden
City’s off-Site detenƟon pond and
overflowed into the City’s MS4.
Revise to "Recycled Earth's detenƟon pond
on the north side of the Site ("SE-Pond").
During this incident, water flowed through
Recycled Earth's storm water system into
the SE-Pond which overflowed into the
City's MS4. As shown in the figures
aƩached to this report and in public
records, the SE-Pond is on Recycled Earth's
property. The City has an easement to
access the SE-Pond but does not own the
pond.
The text has been revised in the Report to
reflect Recycled Earth’s ownership of the
detenƟon pond.
6 Upon acceptance of these results set
forth in this Report, Tetra Tech
recommends that Ogden City remove the
plug and allow Recycled Earth to resume
at the Site storm water discharges to the
MS4
Ogden City will allow Recycled Earth to
resume storm water discharges to the MS4.
However, Recycled Earth will be required to
idenƟfy and test all liquid retained on Site
proposed to be discharged to confirm it
meets appropriate water quality standards
prior to reconnecƟon. Furthermore, upon
reconnecƟon, Recycled Earth will be
required to test the storm water discharge
at Ouƞall #1 (See Figure 2) at least
quarterly for 3 years. Only the previously
approved storm water system on Site may
be reconnected. The perforated pipe
systems were never approved by Ogden
City.
Recycled Earth submiƩed to Ogden City on
October 24, 2023, a “Request for
Reinstatement of Storm Water MS4
ConnecƟon,” and is working with Ogden City
to complete this process consistent with this
comment. No revisions are required for the
Report in connecƟon with his comment.
7 The released water flowed into Ogden
City’s off-Site detenƟon pond and
overflowed into the City’s MS4.
While there is an easement dedicated to
OC for this detenƟon basin, the basin is
owned and operated by RE.
See Response to Comment 5
8 Recycled Earth appealed the Second NOV,
and the appeal is currently pending
before the Ogden City Mayor.
A leƩer from the Ogden City Mayor is
coming soon.
Acknowledged.
RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
9 It is anƟcipated that upon acceptance of
the site characterizaƟon results and the
resumpƟon of discharges to the MS4 that
the french drain will be reconnected to
the storm water system in cooperaƟon
with Ogden City, and the temporary
detenƟon basin will be filled and
eliminated as a Site feature.
Ogden City has not permiƩed and will not
permit the french drain to be reconnected
for these reasons:
1. The original connecƟon of this french
drain was done without approval. Ogden
City does not have any site plan or
permiƫng records on file showing original
approval of the installaƟon of this french
drain and the City would not permit such a
connecƟon.
2. ReconnecƟng of the french drain would
result in discharge of Site groundwater into
Ogden MS4 and waters of the state.
Concern for groundwater contaminaƟon on
site is warranted based on the following
informaƟon:
•The established need to sample
groundwater again in December 2023 to re-
evaluate arsenic and TPH DRO
concentraƟons in the groundwater at the
Site.
•The established need to develop a Site
Management Plan which restricts use of,
and requires worker protecƟon and
management during work in, shallow
groundwater.
•Table 6: All water samples taken along the
french drain show exceedances against
UDEQ Groundwater Quality Standards for
the following analyte.
oFD-1: Arsenic
oFD-2: Arsenic
The french drain has been further excavated
in the vicinity of Sample FD-1 to remove the
arsenic affected soil. The Report has been
revised to present supplemental soil
confirmaƟon sample results following the
excavaƟon that show remaining arsenic
concentraƟons are below the established
background concentraƟon of 15 mg/kg.
AnalyƟcal results for the confirmaƟon
samples are provided in Appendix H.

Tetra Tech will include steps for establishing
a background concentraƟon for arsenic in
groundwater in the forthcoming Site
Management Plan.

The french drain will remain permanently
disconnected.

Recycled Earth would like to discuss an
approach for future development of a new
land drain at the south property when the
environmental concerns for shallow
groundwater are resolved. This maƩer will
be addressed outside of this Report; and
text revisions have been made to the Report
reflecƟng this revised approach.
RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
oFD-3: Arsenic
oFD-4: Arsenic and Oil & Grease
oFD-5: Arsenic
•Table 11: Four of six groundwater samples
show exceedances against UDEQ
Groundwater Quality Standards for the
following analyte.
oMW-1: Arsenic
oMW-2: Arsenic
oMW-3: Arsenic and TPH DRO
oMS-5: Arsenic
10 Sample detecƟons are provided on Table
1 and are compared to the UTG790000
Effluent LimitaƟons and Sector N
Benchmark LimitaƟons
Why not test samples in Table 1 for all
UTG790000 Effluent and Sector N
Benchmark limitaƟons when other surface
water samples (Table 5) taken on site have
shown exceedances in TSS, pH, Aluminum,
Copper, Iron, Zinc, and TPH DRO?
The indicated water samples were analyzed
for all parameters required per the approved
Site CharacterizaƟon Work Plan for surface
water samples. These surface water samples
were not analyzed for the addiƟonal
parameters in UTG790000 because this
water was not considered for discharge to
the MS4 (only the samples on Table 5 were
considered for MS4 discharge; and the final
decision was to not discharge any water to
the MS4).

11 The released water flowed into Ogden
City’s off-site detenƟon pond and
overflowed its banks entering a storm
water inlet along Midland Drive and the
City’s MS4.
Revise to "Recycled Earth's SE-Pond located
on the Site. . ."
The indicated text has been revised in the
Report as requested.
12 As described in SecƟon 2.1.1, Recycled
Earth constructed a temporary detenƟon
pond to contain and evaporate
groundwater on the southern porƟon of
What is the intent with the liquids in the
temporary detenƟon pond? Sample PW-1
in Table 1 shows that this liquid exceeds
UTG790000 Effluent LimitaƟons for Copper
The water detained in the temporary pond
will be held and evaporated unƟl condiƟons
allow discussion of a new land drain as
described in the Response to Comment 9.
RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
the Site at the locaƟon shown on Figure
4.
and Lead. Both PW-1 and STRENCHSW-1
exceed arsenic screening levels for Utah
Groundwater Monitoring Requirements
(R315-308-4) and EPA RSLs.
Table 1 has been updated to include the
UTG790000 effluent limitaƟon for copper.
There is no requirement for lead in this
general permit.
13 A conceptual site model has been
developed to evaluate potenƟal
connecƟons between sources and
receptors as shown on Figure 11. The
model idenƟfies the Beck’s SanitaƟon,
Inc. discharge as the source of
consƟtuents remaining in Site media (i.e.,
soil and groundwater) following the
preliminary remedial acƟons completed
as part of this work and described in this
Report.
Ogden City has never idenƟfied Beck
SanitaƟon as the source. This secƟon
should be revised to idenƟfy Recycled Earth
Site as the source of the discharge.
The indicated text has been revised in the
Report as requested.
14 Elevated arsenic was detected in soil at
french drain sample locaƟon FD-1;
however, there is no risk of direct
exposure because this sample was
collected several feet below ground
surface and has subsequently been
backfilled and covered with soil from
other areas of the Site determined to be
clean through sample collecƟon and
analysis.
Wouldn't there be risk of direct exposure if
the french drain was reconnected to the
Site storm system per the recommendaƟon
in this report?
The french drain area around sample FD-1
has been excavated to remove the affected
soil that originally showed an elevated
arsenic concentraƟon. Three soil
confirmaƟon sample results from the
excavaƟon floor and sidewalls showed
arsenic concentraƟons below the
established background concentraƟon of 15
mg/kg, eliminaƟng the concern for soil
exposure to arsenic above background
levels. The results from this supplemental
work have been added to the revised
Report.
RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
15 Further evaluaƟon of these potenƟal
groundwater exposure points is
unnecessary due to the small number of
downgradient well users.
A porƟon of the Hooper Water
Improvement District (System Facility ID
29006WS005) groundwater source
protecƟon zone is located less than a
quarter mile downgradient to the Site. This
system services a populaƟon of 19,524. Has
this been considered in the Site
CharacterisƟc Report?
Recycled Earth has considered all known
sources of water supply around Recycled
Earth. The Hooper Water Improvement
District’s Source ProtecƟon Zone 4 for
Supply Well 4 is located approximately ¼
mile from the Recycled Earth south property.

According to the UDEQ Guidelines for
Groundwater Source ProtecƟon, Zone 4 is
defined as an “area within a 15-year
groundwater travel Ɵme to a wellhead or
margin of the collecƟon area, the boundary
of the aquifer(s) which supplies water to the
groundwater source, or the groundwater
divide, whichever is closest.” Zone 4 is the
lowest threshold zone for groundwater
source protecƟon.

Because Recycled Earth is outside of the
Zone 4 Source ProtecƟon Zone, there are no
specific groundwater requirements that
must be met.

Furthermore, future groundwater sampling
will be performed to ascertain background
concentraƟons for arsenic and to establish
whether TPH-DRO concentraƟons are
decreasing at the south property.

RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
16 There are three downgradient wells used
for non-potable purposes within one mile
of the Site: one is approximately 0.25
miles to the north and the remaining two
are approximately one mile to the
northwest. All wells are used for
irrigaƟon/stock water and are not used as
potable drinking water sources.
Both Water Right 35-3315 and 3317 state
"domesƟc" as one of the Water Uses
idenƟfied at the boƩom of the water right
informaƟon. Is it confirmed that domesƟc
use is not occurring? See water right details
from links below:
hƩps://www.waterrights.utah.gov/asp_app
s/wrprint/wrprint.asp?wrnum=35-3317
hƩps://www.waterrights.utah.gov/asp_app
s/wrprint/wrprint.asp?wrnum=35-3315
Is a 1-mile evaluaƟon sufficient? There are
many addiƟonal wells down gradient that
show domesƟc use. See map here:
hƩps://maps.waterrights.utah.gov/EsriMap
/map.asp
Water Rights 35-3315 and 3317 correspond
to the two wells located one mile to the
northwest. Both water claims are from 1936
and the wells were installed in the 1940s.
Both wells are now located in the parking lot
of a current Burger King restaurant located
at 2450 S 1900 W, West Haven, Utah. The
wells appear to have been paved over based
on Google Street View imagery.

The Water Rights well records appear to be
out of date based on Recycled Earth’s
supplemental research regarding these wells
idenƟfied by Ogden City. The Report has
been revised to reflect this addiƟonal
informaƟon.

17 The Site characterizaƟon results showed
that the soil and water at the Site contain
no consƟtuent levels above regulatory
standards, background levels, or other
relevant standards except for the
following observaƟons:
This sentence is misleading since 82% of
the on-site water and 21% of the on-site
soil samples exceeded regulatory standards
or background levels idenƟfied in the
tables. This does not include confirmaƟon
samples. It also appears that some of the
tables do not show all parameters sampled
as indicated in the laboratory reports.
Further, it looks that there are some
parameters that should have been sampled
based on results of other samples.
Recycled Earth interprets the City’s
comment to refer to the results presentaƟon
format used by Tetra Tech to indicate that
most results saƟsfy applicable or relevant
standards or screening criteria, “except” for
certain condiƟons listed in the subsequent
bullets of SecƟon 4.1. This format is well
suited for the “Conclusion” secƟon because
if focuses on exceeding condiƟons while
acknowledging all the media samples and
laboratory analytes tested that were not
above the regulatory criteria (see all results
in Appendix G that are non-detect and/or
below regulatory criteria).

RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
Furthermore, the tables in the Report show
detecƟons only as is standard pracƟce to
pare down the laboratory reports (Appendix
G) to present a usable and interpretable
summary of results. Recycled Earth does not
believe changes to the language in this
secƟon is required.
18 Arsenic was detected in one soil sample
(FD-1) at a concentraƟon of 151 mg/kg
(Table 6). This soil exceeds the
established background level for arsenic
(15 mg/kg); however, there is no risk of
direct exposure because this sample was
collected several feet below ground
surface and has subsequently been
backfilled and covered with soil from
other areas of the Site determined to be
clean through sample collecƟon and
analysis. The potenƟal for arsenic
migraƟon from soil to groundwater has
been evaluated and may conƟnue to be
evaluated by monitoring shallow
groundwater at the Site.
See comment [14] above. This sample was
taken at the end of the french drain and
Tetra Tech is recommending to reconnect
the french drain and begin discharging
groundwater to the Ogden storm water
system.
The response to this comment is the same
as Responses to Comments 9 and 14; and
revisions to the Report have been made to
consistently describe the soil remediaƟon at
Sample FD-1 with confirmaƟon sample
results below the background level of 15
mg/kg.
19 Tetra Tech recommends no further
remedial acƟon on or off Site based on
the soil removal acƟons performed as
part of this work and the results of post-
remedial sampling and other sampling
conducted during the Site
characterizaƟon work
Ogden City will follow the
recommendaƟons of the DEQ related to
this comment.
Acknowledged.
RESPONSE TO COMMENTS (RTC) FROM OGDEN CITY
Site CharacterizaƟon Report for Recycled Earth South Property
_6479347.2
Comment
No.
Referenced Text from Report Comment Tetra Tech Response
20 Tetra Tech recommends that an
addiƟonal round of groundwater
sampling be performed in December
2023 to re-evaluate the presence of
arsenic and TPH DRO concentraƟons in
the groundwater.
Ogden agrees that further groundwater
sampling is necessary.
Acknowledged.
21 Recognizing that this is an industrial Site
and the characterizaƟon consƟtuent
concentraƟon levels were compared to
regulatory industrial standards, Tetra Tech
also recommends that a Site
Management Plan (SMP) be prepared
and implemented in accordance with UAC
R315-101-7…… The SMP is expected to
include the following elements in tandem
with an environmental covenant:
• Restrict land use of the Site to only
industrial or commercial uses;
• IdenƟfy the locaƟon of sample FD-1
that contains arsenic at a concentraƟon
above background levels and the
industrial RSL and require worker
protecƟon soil management at depth and
soil cover management; and
• Restrict use of, and require worker
protecƟon and management during work
in, shallow groundwater.
Ogden agrees that a SMP will be necessary.
The restricƟon of land use should not
preclude construcƟon of roadways through
the property. Any SMP developed for the
property must be submiƩed to and
approved by Ogden City before it can be
considered to be recorded.
The SMP will restrict land use to
commercial/industrial, without residenƟal
use. The SMP is not intended to specify
future land development plans and will not
specifically address construcƟon of roads or
other infrastructure. The DWMRC Director
will publish the SMP for public comment,
and Recycled Earth invites Ogden City to
comment during that process or coordinate
with DWMRC for prior review.
22 Table 6, Page 31. The filtered and total metals results for
water samples FD-1 through FD-5 are the
same. Checking laboratory report, it is the
filtered sample results which are not
reported on Table 6.
Table 6 has been revised to show both
unfiltered and filtered results correctly.

_6479884.2

Site Characterization Completion Report
for Recycled Earth South Property
Project No. 117-9187001
November 3, 2023

PREPARED FOR PRESENTED BY
Recycled Earth LLC
C/O Tyler R. Cahoon
Dentons Durham Jones Pinegar P.C.
111 S. Main St., Ste. 2400
Salt Lake City, UT 84111
[phone]
[e-mail]
Tetra Tech, Inc.
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
(801)-736-7451
Fax [phone]
tetratech.com

Prepared by:

David S. Wilson, P.E., P.G.
Principal Engineer & Project Manager
[e-mail]
11/03/2023

Anna Rasmuson, Ph.D., P.G.
Geological Engineer
[e-mail]
11/03/2023

_6479884.2

TABLE OF CONTENTS
1.0 INTRODUCTION ..................................................................................................................................................1
Site Description ..............................................................................................................................................1
Historical Releases ........................................................................................................................................2
Regulatory Actions .........................................................................................................................................3
2.0 SCOPE OF WORK ...............................................................................................................................................5
Preliminary Remedial Actions ........................................................................................................................5
2.1.1 French Drain Cutoff ..............................................................................................................................5
2.1.2 South Trench Cleanout .........................................................................................................................6
2.1.3 Catch Basin Cleanout ...........................................................................................................................6
2.1.4 Excavation Near Maintenance Building ................................................................................................7
Detained Water Characterization and Permitting ..........................................................................................7
Surface Media Characterization .....................................................................................................................8
Subsurface Characterization ..........................................................................................................................9
2.4.1 Subsurface Soil Sampling ................................................................................................................. 10
2.4.2 Groundwater Sampling ...................................................................................................................... 10
Quality Assurance ....................................................................................................................................... 11
3.0 RESULTS .......................................................................................................................................................... 12
Preliminary Remedial Action Verification Results ....................................................................................... 12
3.1.1 South Trench Excavation .................................................................................................................. 12
3.1.2 Catch Basin Sampling ....................................................................................................................... 12
3.1.3 Excavation Near Maintenance Building ............................................................................................. 12
Detained Water Characterization ................................................................................................................ 12
Surface Media Characterization Results ..................................................................................................... 13
3.3.1 French Drain Sample Results............................................................................................................ 13
3.3.2 Soil Sample Results .......................................................................................................................... 13
3.3.3 Surface Water Sample Results ......................................................................................................... 14
3.3.4 Concrete Sample Results .................................................................................................................. 14
Subsurface Characterization Results .......................................................................................................... 14
3.4.1 Subsurface Soil Sample Results ....................................................................................................... 15
3.4.2 Groundwater Sample Results............................................................................................................ 15

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Quality Assurance ....................................................................................................................................... 15
Conceptual Site ModeL ............................................................................................................................... 15
4.0 CONCLUSIONS AND RECOMMENDATIONS ................................................................................................ 17
Summary of Findings .................................................................................................................................. 17
Recommendations ...................................................................................................................................... 17
5.0 REFERENCES .................................................................................................................................................. 19

LIST OF TABLES
Table 1 South Trench and Retained Water Detections
Table 2 South Trench Excavation Characterization Detections
Table 3 Catch Basin Sample Detections
Table 4 Maintenance Building Excavation Confirmation Sample Detections
Table 5 Detained Water Sample Detections
Table 6 French Drain Sample Detections
Table 7 Surface Soil Sample Detections
Table 8 Surface Water Sample Detections
Table 9 Crushed Concrete Sample Detections
Table 10 Soil Boring Sample Detections
Table 11 Groundwater Monitoring Well Sample Detections
Table 12 Quality Assurance Sample Results

_6479884.2
LIST OF FIGURES
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Catch Basin Sample Locations
Figure 4 Detained Water Extent and Sample Locations
Figure 5 South Trench and Confirmation Sample Locations
Figure 6 Excavation Near Maintenance Building Confirmation Sample Locations
Figure 7 French Drain Sample Locations
Figure 8 Surface Media Characterization Sample Locations
Figure 9 On-Site Surface Media Characterization Sample Locations
Figure 10 Monitoring Well Locations and Groundwater Flow
Figure 11 Conceptual Site Model Exposure Pathways

APPENDICES
Appendix A Waste Manifests
Appendix B Standard Operating Procedures for Groundwater Monitoring Well Installation
Appendix C Subsurface Investigation Logs
Appendix D Daily Field Logs
Appendix E Photo Log
Appendix F Soil Sampling Logs
Appendix G Laboratory Reports
Appendix H French Drain Excavation
Appendix I Gas Chromatograph Logs

_6479884.2
LIST OF ACRONYMS/ABBREVIATIONS
Acronyms/Abbreviations Definition
BTV Background Threshold Value
DRO Diesel Range Organics
DWMRC Division of Waste Management and Radiation Control
EPA Environmental Protection Agency
GRO Gasoline Range Organics
MS4 Ogden City Municipal Storm Sewer System
NOV Notice of Violation
ORO Oil Range Organics
PAH Polycyclic Aromatic Hydrocarbons
PCB Polychlorinated Biphenyls
PID Photoionization Detector
PPL Priority Pollutant List
RPD Relative Percent Difference
RSL Regional Screening Level
SMP Site Management Plan
SOP Standard Operating Procedure
SVOC Semi-Volatile Organic Compound
TDS Total Dissolved Solids
TSS Total Suspended Solids
TPH Total Petroleum Hydrocarbons
UAC Utah Administrative Code
UDEQ Utah Department of Environmental Quality
UGPS Utah Groundwater Protection Standard
VOC Volatile Organic Compound
Site Characterization Report Recycled Earth
Ogden, Utah
1 November 3, 2023

_6479884.2
1.0 Introduction
On behalf of Recycled Earth LLC, Tetra Tech, Inc. (Tetra Tech) has prepared this Site Characterization Completion
Report (Report) for the Recycled Earth South Property located at 3025 South 1500 West in Ogden, Utah (Site) in
accordance with the Site Characterization Plan (Tetra Tech 2023). The Site Characterization Plan was prepared in
response to a Notice of Violation (NOV) and a Request for Voluntary Action (Request) issued to Recycled Earth.
The NOV was issued by Ogden City Public Services on September 30, 2022 for a purported illicit discharge from
the Site to the Ogden City Municipal Storm Sewer System (MS4). The Request was issued by the Utah Department
of Environmental Quality (UDEQ), Division of Waste Management and Radiation Control (DWMRC), on August 26,
2022, and pertained to the same illicit discharge. The Request requested that Recycled Earth investigate the
quantity, nature, and extent of potentially contaminated materials on the Site and potential contamination identified
in connection with the purported disposal of unauthorized liquid wastes. This Report presents the findings,
conclusions, and recommendations from completion of the Site characterization activities.
This Report is organized as follows:
 Section 1.0: Introduction – Provides the Report organization and background information, including a
Site description, history of releases, and regulatory actions driving this work.
 Section 2.0: Scope of Work – Describes preliminary remedial actions performed and the Site
characterization activities completed.
 Section 3.0: Results – Describes final sampling results from remedial activities and Site characterization
activities.
 Section 4.0: Conclusion – Provides a summary of results, conclusions, and recommendations based on
the completed work.
 Section 5.0: References – Provides a list of references included in this Report.

As set forth below, Tetra Tech recommends no further remedial action be undertaken based on the soil removal
actions and the results of post-remedial sampling and other sampling conducted during the Site characterization
work. Tetra Tech recommends that (i) an additional round of groundwater sampling be performed in December
2023 to re-evaluate arsenic and TPH DRO concentrations in the groundwater at the Site and (ii) a Site
Management Plan (SMP) be implemented at the Site in accordance with the requirements of Utah Administrative
Code (UAC) R315-101-7 and further described in Section 4 of this Report.
SITE DESCRIPTION
The Site is located at 3025 South 1500 West in Ogden, Utah as shown on Figure 1. The Site covers approximately
11 acres and includes vehicle maintenance, concrete crushing operations, and composting operations, as depicted
on the Figure 2 Site Map. Concrete washout operations were historically performed near the crushing operations,
but these operations are no longer performed on Site. Vehicle maintenance for Recycled Earth’s vehicles and
equipment is performed in the building located on the north end of the Site, and the concrete crushing and
composting operations occur on the south end of the Site.
The Site was constructed in 2015 by Recycled Earth and was developed over prior agricultural lands. The Site was
excavated two to four feet below the original land surface and earth berms were established around the perimeter
of the Site to obscure operations from Midland Drive per Ogden City requirements. During development at the Site,
shallow groundwater was encountered near the native soil surface. Groundwater levels were lowered by installing
a trench filled with gravel and a perforated pipe (land or french drain) to redirect shallow groundwater to the
Site Characterization Report Recycled Earth
Ogden, Utah
2 November 3, 2023

_6479884.2
stormwater system to lower the groundwater table in the southern portion of the Site. The french drain connects to
the southern-most inlet box that collects surface water from the operational areas on the north side of the Site, thus
connecting the groundwater dewatering system to the storm water drainage system that eventually discharges to
the MS4 with temporary storage in a detention basin located northwest of the Site along Midland Drive. Storm water
discharges from the Site are regulated under a Utah General Industrial Storm Water Permit (UTG790000) through
the MS4, which eventually discharges to the Weber River approximately two miles north of the Site.
HISTORICAL RELEASES
According to Recycled Earth, Recycled Earth, no significant spills or releases have occurred at the Site prior to the
August 2022 illicit discharge. Recycled Earth periodically excavates soils with visible minor hydrocarbon staining
from equipment leaks and properly disposes of them off Site at Intermountain Regional Landfill, which is a Class V
municipal waste facility. The soil is transported along with other municipal solid waste in 40-ton haul trucks.
Excavated areas are backfilled with clean gravel to the previous grade.
As part of Recycled Earth’s concrete recycling operation, Recycled Earth accepted concrete washout from a variety
of customers since beginning the operation. The concrete washout was received in various containers and was
typically a dry or slurry form when received. The concrete washout was dumped near the base of the concrete pile
located on the southern portion of the Site for subsequent crushing when fully cured. Recycled Earth stopped
receiving concrete washout in August 2022 when it was discovered the Recycled Earth’s customer, Beck’s
Sanitation, Inc., offloaded, without Recycled Earth’s knowledge or consent, liquid waste near the base of the
concrete pile located on the southern side of the Site.
Except for the purported releases identified by the City and UDEQ in their respective NOV and Request as described
previously and described in the timeline below, Recycled Earth is unaware of other significant releases on or from
the Site.
A summary of the timeline relating to the reported August 2022 release was provided by Recycled Earth and is
presented below, including the recent operational history, release history and preliminary mitigation measures:
 February 2022 – Recycled Earth began accepting from various customers liquids from trenchless
excavation and construction projects in Ogden. One of these customers was Beck Sanitation, Inc. Beck
Sanitation, Inc. that represented to Recycled Earth that it was offloading water that would be filtered through
a gravel filtration system before being offloaded at the Site. Recycled Earth used this water for dust control
at Recycled Earth’s concrete crushing operations.
 August 2022 – Recycled Earth began receiving liquids from Beck’s Sanitation, Inc. trucks at the southern
end of the Site near the south end of the Site (this area is referred to as the “South Trench”).
 August 17, 2022 – The last load of liquid from Beck’s Sanitation, Inc. was accepted in the morning of
August 17, 2022. Recycled Earth was notified mid-day about an odor coming from the MS4 conveyance
system downstream of the Site. Beck’s Sanitation, Inc. informed the Weber County Health Department that
it had disposed at the Site unfiltered wastewater from car wash sumps and other industrial operations,
which Beck’s Sanitation, Inc. did without the knowledge or consent of Recycled Earth. (See First Amended
Complaint, Recycled Earth, LLC v. Beck’s Sanitation, Inc., Case No. 220905020, 2nd Dist. Ct., Weber
County, Utah (alleging Beck’s Sanitation, Inc. dumped unfiltered wastewater onto the Site).
 August 18, 2022 – Ogden City plugged the stormwater culvert crossing located at 2550 South Street. A
Site visit was conducted by Ogden City and UDEQ to inspect the stormwater conveyance pathway from
the Site.
 August 19, 2022 – On behalf of Recycled Earth, Clean Harbors placed silt curtains and sorbent booms at
the 2550 South Street culvert and Wilson Creek crossing, and Recycled Earth placed oil absorbent booms
Site Characterization Report Recycled Earth
Ogden, Utah
3 November 3, 2023

_6479884.2
and pads at the Site (e.g., in catch basins and the outlet to the stormwater detention basin) and downstream
at the Wilson Canal crossing. Clean Harbors also collected preliminary soil and water samples at the Site
(results were included in the Site Characterization Plan). Ogden City removed the culvert plug at the 2550
South Street due to concerns for flooding.
 August 20, 2022 – Ogden City installed a mechanical plug to prevent water from the Site from entering the
MS4, and Recycled Earth began pumping the on-Site inlet box into a temporary pond to remove potentially
impacted groundwater.
 August 24: 2022 - Ogden City suspended Recycled Earth’s access to the MS4 for 30 days due to the
detection of illicit discharge of pollutants or water containing pollutants to the MS4; and subsequently
suspended access indefinitely on September 30 with the NOV, pending compliance with the City’s
requirements .
 September 12, 2022 – Recycled Earth stopped pumping water from the inlet box. The flow to the inlet box
slowed but ponding was still occurring on the Site.
 September 27, 2022 – DWMRC representatives inspecting the Site observed soil staining near the cement
pad on the south side of the maintenance building, and Recycled Earth immediately excavated visibly
affected soil and disposed of the soil off-site at Intermountain Regional Landfill along with other solid waste.
Verification samples were collected by Tetra Tech from the excavation on September 27, 2022; the results
showed residual hydrocarbon concentrations. This area was further excavated and resampled as part of
the preliminary remedial actions as described in Sections 2.1.4 and 3.1.3.
Recycled Earth retained Tetra Tech to assist in responding to the NOV and Request.
REGULATORY ACTIONS
Recycled Earth received a NOV from Ogden City on September 30, 2022 titled “Notice of Violation and Order of
Compliance with Municipal Code 9-7D at property address: 3025 S 1500 W Ogden 84401.” According to Ogden
City, the NOV was in response to complaints of odors leaving the Site and correspondence between the City and
Beck’s Sanitation, Inc. and Recycled Earth. Recycled Earth was ordered in the NOV to complete the following
actions:
1. Cease discharge to the City MS4 until further notice.
2. Submit an Industrial Storm Water Pollution Prevention Plan to the City.
3. Submit all records of liquid waste accepted by Recycled Earth to the City no later than 30 days after the
NOV.
4. Submit all existing and future soil and water sample data obtained by Recycled Earth or their contractors
to the City.
5. Collect and analyze the following soil and water samples in accordance with an approved sampling plan
submitted to the City:
o Minimum of five soil samples along the french drain
o Minimum of two water samples from the white storage tank
o All storm inlet boxes
o Minimum of 10 soil and five water samples along the storm water conveyance path from
Recycled Earth’s property to the Ogden City Limits
6. An environmental report assessing the situation and providing recommendations for site remediation.
Site Characterization Report Recycled Earth
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4 November 3, 2023

_6479884.2
These items in the NOV have been addressed previously or are addressed by this Report. Discharge to the MS4
was plugged immediately after receiving the NOV and remains plugged. Upon acceptance of these results set
forth in this Report, Tetra Tech recommends that Ogden City remove the plug and allow Recycled Earth to
resume at the Site storm water discharges to the MS4.
On August 26, 2022, DWMRC issued Recycled Earth the Request. The Request was not a notice of violation or
administrative order but was intended to provide Recycled Earth with a preliminary notice and an opportunity to
take the following actions voluntarily:
1. Cease accepting solid waste materials not approved in its plan of operation, including trenchless
excavation waste, liquids potentially containing greases or petroleum products, concrete washout water,
car wash sump wastes, and waste asphalt.
2. Submit an updated plan of operations and investigate the quantity, nature, and extent of any potentially
contaminated materials in the concrete piles on the southern campus of Recycled Earth and provide a
report to the Division on this issue.
3. Prepare and submit a plan to characterize the source(s), nature, and extent of potential contamination to
groundwater at the Site.
These items in the Request have been addressed previously or are addressed by this Report, except for item 2,
which is forthcoming and will be provided to DWMRC separately by Recycled Earth.
Recycled Earth received a second notice of violation (Second NOV) from Ogden City on January 19, 2023
alleging that Recycled Earth had reinstated access to the MS4 and illegally discharged pollutants therein,
following an event in which the pressure from the detained water on the Site blew out a temporary plug in one of
the on-Site catch basins. The released water flowed into Recycled Earth's detention pond on the north side of the
Site shown on Figure 2 and overflowed into the City’s MS4. Recycled Earth took immediate action to
repair/improve the plug and immediately contacted Ogden City. The Second NOV included a penalty of $1,000.
Recycled Earth appealed the Second NOV, and the appeal is currently pending before the Ogden City Mayor.
Site Characterization Report Recycled Earth
Ogden, Utah
5 November 3, 2023

_6479884.2
2.0 SCOPE OF WORK
The scope of work performed to meet the regulatory requirements in Ogden City’s NOV and DWMRC’s Request
were presented in the Site Characterization Plan, which was approved by Ogden City on January 23, 2023, and
by DWMRC on January 25, 2023. The work performed included preliminary remedial actions and sampling of
select areas on the Site to further characterize sources of hydrocarbons and other constituents in surface water,
soil, and groundwater based on the results from preliminary sampling and analyses presented in the Site
Characterization Work Plan. The following table presents a chronological timeline of activities performed at the
Site; the sequence varied from the anticipated order of activities due to heavy precipitation during early 2023,
which was detained over parts of the Site.

Remedial Action Activity Date
Detained Water Characterization January 18, 2023
Catch Basin Sampling and Cleanout February 2, June 9, 2023, and
August 16, 2023
Surface Characterization February 2, 3, 9, March 10, and
April 20, 2023
Subsurface Characterization May 4, 5, and 11, 2023
Excavation Near Maintenance Building May 8, 2023
French Drain Cutoff May 16, 2023
South Trench Cleanout June 29, 2023
French Drain Excavation October 19, 2023

PRELIMINARY REMEDIAL ACTIONS
This section describes the preliminary remedial actions performed at specific areas to address observed and
probable sources of petroleum hydrocarbon impacts at the Site. These actions were based on findings from
preliminary inspections and analysis of environmental samples described in the Site Characterization Plan. The
primary objective was to eliminate the sources of hydrocarbon impacts, thereby preventing potential migration to
surface water or groundwater and safeguarding environmental media.
2.1.1 French Drain Cutoff
The french subdrain system, running beneath the existing concrete pile from south to north, was disconnected
from the stormwater drainage system. Recycled Earth cut off and sealed the outlet from the french on May 16,
2023 by excavating and cutting off the pipe south of catch basin CB-8 shown on Figure 3. Both the terminated
pipe and the inlet to CB-8 were sealed with mechanical plugs to permanently disconnect the french drain from the
storm water collection system. A temporary groundwater detention basin (or sink) was developed at the north end
of the concrete pile concurrently with the french drain cutoff to provide an on-Site reservoir for storage and
evaporation of groundwater to minimize flooding of site operations. The location of this temporary basin is shown
on Figure 4.
Site Characterization Report Recycled Earth
Ogden, Utah
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_6479884.2
It is anticipated by Recycled Earth that upon resolution of remaining groundwater concerns described in this
report that a new land drain system may be discussed with Ogden City; and if (when) a new land drain system is
installed, the temporary ground water detention basin will be filled and eliminated as a Site feature.
2.1.2 South Trench Cleanout
Standing surface water in the South Trench was sampled and analyzed prior to trench cleanout for the same
parameters as the site characterization surface water samples. Sample detections are provided on Table 1 and
are compared to the UTG790000 Effluent Limitations and Sector N Benchmark Limitations; and all results were
below the effluent limitations. Based on these results, the standing water in the South Trench was pumped into
the temporary detention pond, described above in Section 2.1.1, prior to excavation.
The South Trench was cleaned out via excavation on June 29, 2023 by Recycled Earth with observation and
oversight provided by Tetra Tech. The excavation process was guided by visual observations and a handheld
photoionization detector (PID) instrument, which was used to screen for volatile organic compounds (VOCs). The
quantity of soil removed from the South Trench is estimated to be 60 cubic yards based on field dimensions.
A total of seven verification samples were collected, with samples being obtained approximately every 20 feet
along the trench excavation area at the locations shown on Figure 5. Based on the shape and extent of the
excavation, representative samples were collected at these locations because there were no distinct bottom and
sidewalls for the excavation. The samples were collected in accordance with the Standard Operating Procedures
(SOPs) provided in the Site Characterization Plan. The purpose for these samples was to verify that impacted
soils have been sufficiently removed to meet the applicable regulatory screening criteria and demonstrate removal
of as much source material containing hydrocarbon mass as possible in the immediate area of the trench.
Additionally, one soil sample was collected as a ten-point composite from the piles of excavated material to
characterize the excavated soil for landfill disposal requirements. All samples were sent to Pace Analytical
Laboratory (Pace) for analysis of the following parameters:
 VOCs to represent total petroleum hydrocarbons gasoline range organics (TPH GRO) using Method
8260B.
 Semi-volatile organic compounds (SVOCs) to represent total petroleum hydrocarbons diesel range
organics (TPH DRO) using Method 8270C.
 Polycyclic aromatic hydrocarbons (PAHs) using Method 8270-SIM.
The impacted soils removed from the trench were disposed of at Intermountain Regional Landfill after receiving
laboratory results for the confirmation sample that showed the material was non-hazardous and acceptable to the
landfill; a copy of the waste manifest is provided in Appendix A. The results for the verification samples are
presented in Section 3.1.
2.1.3 Catch Basin Cleanout
Prior to cleaning out the catch basins, soil samples were obtained from each catch basin. Catch basins CB-1, CB-
2, CB-3, and CB-4 were sampled on February 2, 2023. Notably, sample locations CB-5, CB-6, and CB-7 identified
in the Site Characterization Plan were empty and could not be sampled. Catch basins CB-8 and CB-9 were in the
flooded area of the Site and were therefore sampled later on June 9, 2023. The samples were collected as grab
samples in accordance with the applicable SOPs provided in the Site Characterization Plan. The samples were
sent to Pace for analysis of the following parameters:
 PPL Metals by Methods 6010B and 7471A
 VOCs to represent TPH GRO by Method 8260B
 SVOCs to represent TPH DRO by Methods 8270C
Site Characterization Report Recycled Earth
Ogden, Utah
7 November 3, 2023

_6479884.2
 PAHs by Method 8270-SIM
The locations of the catch basins are shown and numbered for identification purposes on Figure 3. The results for
the catch basin samples are presented in Section 3.1.
The on-site catch basins containing sediment were cleaned out by Recycled Earth at various times during the site
characterization activities with final cleanout and inspection on August 16, 2023, with verification by Tetra Tech.
The material from the catch basins was disposed of at Intermountain Regional Landfill after receiving sample
results confirming that the sediment in the catch basins is non-hazardous. Copies of waste manifests are provided
in Appendix A. The catch basin sediment traps were hand shoveled and pumped out to remove potentially
impacted media. The quantity of solids removed from the catch basins was relatively small and these materials
were disposed of with other solid wastes from the Site at the Intermountain Regional Landfill.
2.1.4 Excavation Near Maintenance Building
The excavation near the cement pad on the south side of the maintenance building on the Site was expanded to
remove additional residual petroleum hydrocarbon impacts. After the additional excavation was completed, five
confirmation samples were collected on May 8, 2023. Three samples were collected in the footprint of the
excavation, four on the sidewalls, and one on the floor at the locations shown on Figure 6. The samples were
obtained as grab samples in accordance with the relevant SOPs provided in the Site Characterization Plan. The
samples were sent to Pace for analysis of the following parameters:
 PPL Metals by Methods 6010B and 7471A
 VOCs to represent TPH GRO by Method 8260B
 SVOCs to represent TPH DRO by Methods 8270C
 PAHs by Method 8270-SIM
The earthwork associated with this remedial action was performed by Recycled Earth with observation and
oversight provided by Tetra Tech. It is estimated that six cubic yards of soil were excavated to complete this
remedial action. The excavated soil was disposed of at the Intermountain Regional Landfill and a copy of the
waste manifest is provided in Appendix A.
DETAINED WATER CHARACTERIZATION AND PERMITTING
The plug installed at Recycled Earth’s MS4 outlet led to a substantial volume of detained water held on the Site.
The detained water initially flooded the center of the Site where concrete crushing activities were previously
performed, as shown on Figure 4. During the highest water level, it was estimated that approximately 600,000
gallons of water were detained in this area. Excess water was attributed to unusually high precipitation early in
2023 and groundwater discharge from the french drain outlet (i.e., catch basin CB-8 shown on Figure 3).
Groundwater discharge was higher than normal during the spring of 2023 due to record snowmelt and related
runoff from the nearby Wasatch Mountains.
On January 13, 2023 the pressure from the detained water on the Site blew out the temporary plug installed over
catch basin CB-9 (Figure 4). The released water flowed into Recycled Earth's detention pond located on the Site
and overflowed its banks entering a storm water inlet along Midland Drive and the City’s MS4. Recycled Earth
took immediate action and installed an earthen plug over the catch basin to isolate the detained on-Site water
from the detention basin. The plug was constructed by packing a plastic tarp filled with road base material
secured with zip ties into the 12-inch pipe on the north side of the catch basin. A geosynthetic fabric was then
placed under the catch basin grate and an additional plastic tarp was placed over the grate. Approximately 200
tons of road base material was placed on top of the tarp until the plug extended one to two feet above the ponded
area. The earthen plug was later replaced by a mechanical plug that completely sealed off the french drain
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connection to the storm water system as described in Section 2.1.1. Recycled Earth and Tetra Tech immediately
contacted Ogden city about the temporary plug failure and its swift action to re-plug the detained water.
Tetra Tech collected four initial water samples from the detained water on January 18, 2023 from the locations
shown on Figure 4. The samples were analyzed for the following parameters:
 pH
 Chemical oxygen demand (COD)
 Total suspended solids (TSS)
 Total dissolved solids (TDS)
 Total recoverable lead
 Oil and grease
 Benzene, toluene, ethylene, and xylene (BTEX)
 Methyl tert-butyl ether (MTBE)
 Naphthalene
 Total toxic organics (TTO)
 TPH gasoline range organics (GRO)
 TPH Diesel range organics (DRO)
 Select metals, including:
o Total recoverable aluminum
o Arsenic
o Barium
o Beryllium
o Total recoverable cadmium
o Total recoverable chromium
o Total recoverable copper
o Total recoverable iron
o Total recoverable lead
o Mercury
o Selenium
o Total recoverable silver
o Total recoverable zinc
The results for these samples are presented in Section 3.2. Recycled Earth initially planned to treat and discharge
the detained water under a General Permit for Treated Groundwater and Surface Water (Permit Number
UTG790000); however, it was later decided to continue to hold the water on Site based on decreased
precipitation and increased evaporation during the summer months, which significantly reduced the volume of
water held on Site. Also, Recycled Earth’s attempts to retain a water treatment contractor proved to be cost-
prohibitive.
As described in Section 2.1.1, Recycled Earth constructed a temporary detention pond to contain and evaporate
groundwater on the southern portion of the Site at the location shown on Figure 4. Tetra Tech collected a water
sample from the temporary detention pond on July 14, 2023, in order to characterize the remaining water held on-
Site. The results for this detained groundwater sample are presented in Section 3.2.
SURFACE MEDIA CHARACTERIZATION
This section presents the scope of work for sampling and analysis required by DWMRC and Ogden City. This
work included sampling and analysis of surface soils and water at the locations shown on Figures 7 through 9. A
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brief description of the investigation methods is provided below, and complete SOPs developed by Tetra Tech for
these activities are in the Site Characterization Plan.
Per the NOV from Ogden City, the following samples were collected on- and off-Site:
1. Five water and five soil samples were collected at generally equal distances along the extent of the french
drain on April 20, 2023 (Figure 7). The samples were collected by excavating to the water table at each
location and collecting samples from the open excavations. Soil samples were collected just above the
soil-groundwater interface. The french drain invert depth is approximately five feet below ground surface
and is below the water table.
2. Seven soil samples were collected from the locations shown on Figure 8:
a. SS-1, SS-2, SS-3 and SS-4 samples were collected from below the broken concrete pile on the
southern end of the Site on April 20, 2023. Areas of the broken concrete pile required movement
to allow for soil sampling below the concrete.
b. Sample, SS-5, was collected on the east side of the concrete pad south of the maintenance
building on February 2, 2023.
c. Samples SS-6 and SS-7 were collected from the stormwater detention basin on February 2,
2023.
3. Three concrete samples were collected from the broken concrete materials on the southern side of the
Site; and one processed (crushed) concrete sample was collected from one of the piles in the center of
the Site on March 10, 2023 (Figure 8). Samples were collected from one to two foot depth below the
surface of the pile and were crushed to a fine powder using a sledgehammer prior to submittal to the
laboratory for analysis.
4. Five water samples and six soil samples were collected along the stormwater conveyance flow path from
the Site to the Ogden City Limits on February 3 and 9, 2023 (Figure 9). Each water sample had a
corresponding soil sample from the same location except for SW-4, which was in a deep stormwater
catch basin that could not be entered for safety reasons. Per direction from Ogden City, sample SS-12
was moved to a location along the Wilson Canal northeast of SW-5 and SS-13.
All samples were collected in accordance with the SOPs provided in the Site Characterization Plan.
The samples were sent to Pace for analysis of the following parameters:
 Priority pollutant list (PPL) Metals by Methods 6010B and 7471A
 Chromium (VI) by Methods 3060A/7199 and 3500 CR C-2011
 Total Solids by (water samples only) Method SM2540 D
 Oil and Grease (water samples only) by Method 1664A
 VOCs to represent GRO by Method 8260B
 SVOCs to represent DRO by Methods 8270C
 PAHs by Method 8270-SIM
 Total petroleum hydrocarbons oil range organics (TPH ORO) using Method 8015
 Polychlorinated Biphenyls (PCB) Congeners by Method 8082
Additionally, three confirmation samples were collected from an excavation near the french drain inlet. The
additional excavation was performed in response to the french drain soil sample results for this location, as
described in Section 3.3.1. The confirmation samples were analyzed by Pace for total arsenic.
SUBSURFACE CHARACTERIZATION
This section describes groundwater monitoring well locations, installation procedures, and groundwater
monitoring requirements.
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2.4.1 Subsurface Soil Sampling
Six monitoring wells were installed on May 4, 2023 at the locations shown on Figure 10 using direct push drilling
techniques operated by ET. Technologies with observation and oversight provided by Tetra Tech and in
accordance with the revised SOP provided in Appendix B. The revision to the SOP included using direct push
methods instead of hollow-stem-auger drilling and such method was approved by DWMRC on April 28, 2023.
Blue Stakes was notified prior to the well installations and a private utility locator came on Site and used ground
penetrating radar to mark the target well locations. The boreholes were performed sequentially with each
boreholes being two inches in diameter and extending to five feet below the water table. The soil lithologies were
logged during drilling and the dates and times of soil sample collection, along with the corresponding Quality
Control samples, are provided in the Soil Sample Logs provided in Appendix C.
One subsurface soil sample was collected from each borehole for laboratory analysis. The samples were
collected as grab samples using the collection methods described in the SOPs provided in the Site
Characterization Plan. Samples were collected from areas of visibly impacted soils, soils showing detection of
volatile organic vapors with the PID, or from a depth immediately above the water table if observations of potential
impacts were not observed. The samples were shipped to Pace for analysis of the following parameters:
 PPL Metals by Methods 6010B and 7471A
 Chromium (VI) by Methods 3060A/7199 and 3500 CR C-2011
 VOCs to represent GRO by Method 8260B
 SVOCs to represent DRO by Methods 8270C
 PAHs by Method 8270-SIM
 TPH ORO by Method 8015
 PCB Congeners by Method 8082
All sampling and excavation equipment were decontaminated between locations using potable water, and the
decontamination liquids and soil cuttings were removed from the Site for proper disposal.
The soil borings were completed as shallow groundwater monitoring wells in accordance with the SOPs provided
in the Site Characterization Plan. Protective well casings (vaults) were complete for the wells on May 5, 2023.
2.4.2 Groundwater Sampling
The monitoring wells were developed prior to sampling on May 8, 2023 using development techniques described
in the revised SOP 011 provided in Appendix B. The procedures and results of the well development process for
each monitoring well are presented in Appendix C.
Groundwater samples were collected on May 11, 2023 using the procedures described in the SOPs provided in
the Site Characterization Plan. Samples were collected after a minimum of three well volumes had been purged
from the well and field parameters (temperature, pH, specific conductivity, dissolved oxygen, and oxidation-
reduction potential) were within 10% of prior readings. Groundwater samples were analyzed for constituents listed
in UAC R315-308-4 as directed by the DWMRC:
 Inorganic Constituents:
o ammonia (as N) - 350.1
o carbonate/bicarbonate - 2320 B-2011
o calcium - 6010
o COD - 410.4
o chloride – 9056
o iron - 6010
o magnesium - 6010
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o manganese - 6010
o nitrate (as N) - 9056
o pH - 9045
o potassium - 6010
o sodium - 6010
o sulfate - 9056
o TDS - 2540 C-2011
o total organic carbon (TOC) - 9060A
 PPL Metals by Methods 6010B and 7471A
 VOCs by Method 8260B
 SVOCs by Method 8270C
In addition, TPH GRO (Method 8060) and TPH DRO (Method 8070) concentrations were obtained through the
VOC and SVOC analyses, given the nature of past releases and the preliminary laboratory results.
Groundwater elevations were surveyed for each well on May 17, 2023. Interpolated groundwater contours and the
interpreted direction of groundwater flow are presented on Figure 10.
QUALITY ASSURANCE
Duplicate samples were collected at a rate of one per every ten samples and Matrix Spike/Matrix Spike Duplicate
(MS/MSD) samples were collected at a rate of one per ten samples. The results from quality assurance sampling
and analysis are presented in Section 3.5.
The person collecting the samples was responsible for sample custody from the time of sample collection to
receipt by a laboratory or until samples were shipped. A sample is considered under custody if one of the
following conditions applies:
 The sample is in a person’s possession.
 The sample is in that person’s view after being in his or her possession.
 The sample was in that person’s possession and then placed in a secured location.
 The sample is in a designated secure area.
A Chain-of-Custody Record with its assigned sample numbers accompanied all samples to the laboratory. When
samples were shipped, custody seals were attached to each cooler to ensure that tampering with the samples did
not occur in transit, and the shipment air bill became part of the Chain-of-Custody documentation.

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3.0 RESULTS
This section presents the analytical results for confirmation samples and Site characterization work and compares
them to the regulatory limits, screening levels and/or background values as applicable and presented in the
approved Site Characterization Plan. This section also presents a conceptual site model developed based on the
site characterization findings.
Daily field forms describing field activities and are included in Appendix D. Representative photos capturing
project work are provided as a photo log in Appendix E. Soil sampling logs are provided in Appendix F and full
laboratory analytical reports organized in chronological order by sample collection date are provided in Appendix
G.
PRELIMINARY REMEDIAL ACTION VERIFICATION RESULTS
3.1.1 South Trench Excavation
The South Trench soil verification sample locations are shown on Figure 5, and the corresponding, detected
results are presented on Table 2. All detections for the verification samples were below the U.S. Environmental
Protection Agency (EPA) Industrial Regional Soil Screening Levels (RSLs), and the South Trench excavation is
complete having achieved the target remediation levels.
3.1.2 Catch Basin Sampling
Soil detections for the catch basin sediment samples are provided on Table 3. All samples exceeded the EPA
RSLs for arsenic, which is set at 3 mg/kg. The highest level detected was 53 mg/kg in sample CB-2. Sample CB-4
exceeded the EPA RSL for TPH DRO at a concentration of 3,600 mg/kg. This sample was located near the
maintenance building. All impacted sediment was removed from the catch basins, was properly landfilled off Site,
and does not pose a risk to the environment or future surface water discharged to the MS4.
3.1.3 Excavation Near Maintenance Building
Confirmation soil sample detections are provided on Table 4. All five confirmation samples exceeded the EPA RSL
for arsenic; all other detections were below the EPA RSLs. The arsenic concentrations are all below the background
threshold value (BTV) of 15 mg/kg established through correspondence between Recycled Earth and DWMRC
dated August 9, 2023 confirming that this “surrogate” BTV was obtained from the Ogden Business Exchange
Voluntary Cleanup Program documents, as described in the agency-approved Site Characterization Report
(Section 2.3.2), and as such this value is an acceptable BTV per the Technical Guide for Risk Assessment.
DETAINED WATER CHARACTERIZATION
Detections for the ponded water samples are provided on Table 5. The results were compared to the UTG790000
Effluent Limitations and Sector N Benchmark Limitation. Note that the benchmark limitations for copper, lead, and
zinc are based on the hardness of the Weber River. Tetra Tech obtained hardness data from the UDEQ, Division
of Water Quality. Hardness was calculated from Ca and Mg as CaCO3 equivalent and was equal to 360 mg/L. All
detections were below the effluent limitations with the following exceptions:
 Site-North exceeded the Sector N Benchmark Limitation for TSS and the UTG790000 limitation for zinc
 Site-North, SE-Pond, and Outfall #1 exceeded the UTG790000 effluent limitations for pH
 Site-South and Site-North exceeded the Sector N Benchmark Limitations for aluminum and iron
 All samples exceeded the effluent limitations for copper
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 Site-North and Outfall #1 exceeded the UTG790000 for TPH DRO

These results indicated that Recycled Earth could not discharge the detained water to the MS4 without prior
treatment. The water was detained at the Site until weather conditions changed and the water levels were
reduced.
Sample detections for the temporary groundwater detention pond are provided on Table 1 for comparison to the
results for the South Trench water sample. All results were below the UTG790000 Effluent Limitations and Sector
N Benchmark Limitations.
SURFACE MEDIA CHARACTERIZATION RESULTS
This section describes the results of the surface characterization samples collected on and off Site in accordance
with the Site Characterization Plan.
3.3.1 French Drain Sample Results
The french drain sample detections are presented on Table 6. Arsenic concentrations were above the EPA RSLs
for all soil samples but were below the established background concentration of 15 mg/kg except for sample FD-1
located near the former french drain inlet that had an arsenic concentration of 151 mg/kg.
Based on the elevated arsenic detected at FD-1 and direction from the DWMRC that remediation of this area
would be required for site closure, supplemental soil excavation was performed at this location on October 18,
2023. Recycled Earth informed the DWMRC and Ogden City of the planned excavation activities via email
correspondence issued by Tetra Tech dated October 13, 2023. Approximately 8 cubic yards of material was
removed and disposed of at Intermountain Regional Landfill; a copy of the waste manifest is provided in
Appendix A. Three confirmation soil samples were collected from the excavation floor and sidewalls and were
analyzed for total arsenic. All three samples were below the background concentration of 15 mg/kg for arsenic.
Confirmation sample locations, analytical results, and representative photographs of the excavation at this
location are provided in Appendix H.
All groundwater results were below the UDEQ Groundwater Quality Standards except for arsenic.
As directed by the DWMRC, the Division’s Technical Guide for Risk Assessments (Guide) was used to assess
risk associated with TPH. The TPH risk was evaluated by assessing individual chemical constituents identified in
the Guide rather than relying on TPH fraction data due to the limitations of TPH measurement techniques which
provide no specific information about individual detected hydrocarbons. EPA Tap Water RSLs were compared to
groundwater results for indicator compounds associated with common TPH mixtures. All french drain groundwater
results were below the EPA Tap Water levels for the indicator compounds except for arsenic.
3.3.2 Soil Sample Results
Surface soil sample detections are provided on Table 7. All detections were below the EPA RSLs except for the
following samples for the indicated parameters:
 All soil samples exceeded the EPA RSL for arsenic; however, only sample SS-13 at 87 mg/kg was above the
established background concentration of 15 mg/kg.
 Sample SS-13 exceeded the EPA RSL for silver and TPH-DRO.
The detection of elevated arsenic at sample SS-13 could be related to naturally occurring high arsenic although it
is significantly higher than the background level; and the elevated arsenic and TPH-DRO could come from other
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industrial operations along the channel between Recycled Earth and the Wilson Canal crossing where this sample
was collected. Other soil samples collected during this investigation from the channel between Recycled Earth
and the Wilson Canal crossing did not show arsenic or TPH-DRO above the background or RSL values,
respectively indicating that there are sections of channel between these locations that are not impacted above
regulatory or background levels.
Furthermore, Gas Chromatogram (GC) and Gas Chromatogram/Mass Spectrometry (GC/MS) charts were
obtained from the laboratory and used by Tetra Tech to compare on- and off-Site GC and GC/MS fingerprints for
petroleum hydrocarbon compounds. Based on the analysis of these data, the major naturally occurring peaks
present in off-Site samples were not identified in on-Site samples and major naturally occurring peaks in on-Site
samples were not identified in off-Site samples. Importantly, the highest peaks shown on the chromatograms are
internal standards and surrogates used by the laboratory for calibration purposes, and they do not reflect actual
constituents in the samples. Peaks for ethanol, isopropyl alcohol, and acetone were observed in several samples;
however, these are common laboratory contaminants and are not associated with the purported release at the
Site. These data support that the petroleum hydrocarbons identified downstream and off Site do not come from
the same source as the hydrocarbons identified on Site. Tetra Tech’s analysis of the GC and GC/MS charts is
included in Appendix I.
3.3.3 Surface Water Sample Results
Surface water sample detections are presented on Table 8. All surface water sample detections collected for the
Site Characterization were below the regulatory comparison criteria except for Sample SW-1 that exceeded the
UTG790000 Effluent Limitations for copper, zinc, and diesel range organics. This location is approximately 0.25
miles downgradient from the Site; therefore, it is unknown whether the source of these elevated results comes
from other industrial businesses and/or the historical railroad adjacent to the channel in this area. These
constituents were not elevated elsewhere along the stormwater conveyance system in surface water.
Gas Chromatogram (GC) and Gas Chromatogram/Mass Spectrometry (GC/MS) charts were also reviewed for the
water samples to compare on- and off-Site GC and GC/MS fingerprints for the petroleum hydrocarbon
compounds detected at Sample SW-1. Based on the analysis of these data, the petroleum hydrocarbons
identified downstream and off Site are not the same as those detected on Site and do not come from the same
source. Tetra Tech’s analysis of the GC and GC/MS charts is included in Appendix I.
3.3.4 Concrete Sample Results
The concrete sample detections are presented on Table 9. All detections were below the EPA RSLs and the
Toxicity Characteristic Leaching Procedure (TCLP) Rule of 20 except for sample CS-1, which exceeded the EPA
RSL with a concentration of 3.8 mg/kg arsenic, which is below the established background concentration of 15
mg/kg and not considered to pose a risk to the environment or potential users of the concrete product. In
accordance with the correspondence received by Recycled Earth from DWMRC dated April 5, 2023, and based
on the results from this evaluation, Recycled Earth has resumed production and sale of crushed concrete
products.
SUBSURFACE CHARACTERIZATION RESULTS
This section describes results for the subsurface characterization samples collected on Site. The locations of the
soil borings and monitoring wells are shown on Figure 10, and corresponding Borehole Logs detailing soil sample
depths, depth to water, lithology, PID readings, and well construction schematics are provided in Appendix C.
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3.4.1 Subsurface Soil Sample Results
During advancement of the soil borings, only the subsurface soils at location MW-6 showed a PID reading above
the background level, indicating a detection of volatile organic vapors at 1.2 parts per million (PPM) using the field
instrument. The soil sample detections from each soil boring are presented on Table 10. All sample results were
below EPA RSLs except for arsenic, but all results were below the established background concentration of 15
mg/kg.
3.4.2 Groundwater Sample Results
The groundwater sample detections for each monitoring well are presented on Table 11, and corresponding
groundwater sampling logs are provided in Appendix C. All detections were below the Utah Groundwater
Protection Standard (UGPS) except for arsenic at wells MW-1, MW-2, MW-3, and MW-5 for both filtered and
unfiltered samples. Notably, arsenic was detected in MW-1, which is upgradient from the historical release area
(i.e., the South Trench) and serves as a background well. The detections of arsenic in shallow groundwater are
likely due to elevated arsenic occurring naturally in the regional soils.
Sample MW-3 exhibited concentrations of TPH DRO at 1.8 mg/L.
As directed by the DWMRC, the Division’s Technical Guide for Risk Assessments (Guide) was used to assess
risk associated with TPH. The TPH risk was evaluated by assessing individual chemical constituents identified in
the Guide rather than relying on TPH fraction data due to the limitations of TPH measurement techniques which
provide no specific information about individual detected hydrocarbons. EPA Tap Water RSLs were compared to
groundwater results for indicator compounds associated with common TPH mixtures. All groundwater results
were below the EPA Tap Water levels for the indicator compounds except for arsenic and manganese.
The presence of TPH DRO at well MW-3 is believed to be related to the detention and ponding of surface water
on the west side of the property prior to installation of the well. The surface water in this area was also observed
to contain TPH DRO concentrations.
QUALITY ASSURANCE
Quality Assurance samples, sample locations, and sample times are listed in the sample logs in Appendix F.
Chain of Custody documents included with the full laboratory reports are provided in Appendix G.
Duplicate sample results and the relative percent difference (RPD) between duplicate and parent samples are
presented on Table 12. The RPD was not calculated for sample pairs where one or more of the samples were
non-detect. The RPD ranged from 0 to 157% and 85% of results had an RPD less than 35%. MS and MSDS
sample results are provided in the laboratory reports provided in Appendix G. Based on the quality assurance
sample results and evaluation of these data as described herein, the results obtained during these activities are
considered valid for their purposes of characterizing the Site.
CONCEPTUAL SITE MODEL
Due to the limited number of samples showing elevated levels of constituents above EPA RSLs (i.e., arsenic and
TPH DRO), established background concentrations, or other regulatory criteria, Tetra Tech does not recommend
performing a quantitative risk assessment to evaluate potential risks associated with the Site. However,
development of a conceptual site model is relevant for evaluation of the results in the context of potential
constituent migration and exposures to human and/or ecological receptors.
A conceptual site model has been developed to evaluate potential connections between sources and receptors as
shown on Figure 11. The model identifies the 2022 discharges to the Recycled Earth Site as the source of
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constituents remaining in Site media (i.e., soil and groundwater) following the preliminary remedial actions
completed as part of this work and described in this Report.
Potential soil exposure points and exposure routes are mitigated as described below for the few remaining
detections of constituents above regulatory levels in soils:
 Elevated arsenic and TPH-DRO detected in three catch basins do not pose a risk to human and/or
ecological receptors because the catch basins are cement lined and were cleaned out to remove the
sediment that contained these parameters.
 Elevated arsenic was originally detected in one soil sample from french drain sample location FD-1;
however, remediation was performed at the direction of DWMRC, soil from this location was removed
and disposed of off-Site, and confirmation samples from the excavation floor and sidewalls were below
the established background concentration of 15 mg/kg for arsenic. Based on these results, there is no
remaining exposure pathway for subsurface soils.
 The potential for arsenic to migrate from the soil at this location into groundwater can be directly
assessed by monitoring site groundwater, as has been done for this Site characterization.
Low detections of arsenic were detected in all groundwater samples at the Site and elevated TPH-DRO was
detected at one well (MW-3). Potential exposure points, exposure routes and receptors to groundwater impacts
are presented on Figure 11. Further evaluation of these potential groundwater exposure points is unnecessary
due to the small number of downgradient well users. Tetra Tech conducted a review of the interactive Utah
Division of Water Rights (DWR) well permit website to identify wells downgradient from the Site. There are no
municipal water supply wells within one mile downgradient from the Site A 1-mile radius is considered sufficient
for evaluation for shallow groundwater impacts, as this water is not utilized or suitable for water supply use due to
the presence of high dissolved solids concentrations typical of the regional shallow aquifer along the Wasatch
Front.
The Utah Division of Water Rights identifies three downgradient wells potentially used for non-potable purposes
within one mile of the Site. One well is located approximately 0.25 miles to the north (Water Right 35-4501), and
the remaining two wells are approximately one mile to the northwest (Water Rights 35-3315 and 35-3317) of the
Site. The claim for Water Right 35-4501 is from 1970 and was for irrigation/stock water, and not potable drinking
water; no public information was available on the depth of the well. The well currently is located in the parking lot
of Lansing Building Products and appears to have been paved over based on aerial imagery. The claims for
Water Rights 33-3315 and 35-3317 are from 1936. Both wells were installed in 1940 and were drilled to 302 feet
below ground surface. The wells were used for irrigation, stock watering and domestic use, according to the well
records with the Division of Water Rights. The locations of these wells are in the parking lot of a current Burger
King restaurant and appear to have been paved over based on aerial imagery and Google Street View imagery.
Based on the records for Water Rights 35-3315 and 35-3317 and their location in a paved parking lot, it is highly
unlikely that these wells currently exist and they are certainly not used for domestic purposes. Based on this
review, the arsenic and TPH-DRO concentrations that slightly exceed the regulatory levels in groundwater will not
pose a risk to groundwater users near the Site. However, additional groundwater monitoring is recommended in
Section 4.2 to observe Site groundwater conditions.

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4.0 CONCLUSIONS AND RECOMMENDATIONS
The following subsections present the summary of findings and recommendations for the Site.
SUMMARY OF FINDINGS
The Site characterization results showed that the soil and water at the Site contain no constituent levels above
regulatory standards, background levels, or other relevant standards except for the following observations:
 Catch basin samples CB-2 and CB-8 exceeded the established background concentration for arsenic (15
mg/kg) with concentrations of 53 and 18 mg/kg, respectively. Sample CB-4 exceeded the EPA RSL for total
petroleum hydrocarbon diesel range organics (TPH-DRO) with a concentration of 946 mg/kg (Table 3). The
catch basins were cleaned out by Recycled Earth with oversite by Tetra Tech, and the materials were
disposed of off Site at a commercial solid waste landfill. No further action is required for the catch basins.
 Arsenic was originally detected in one soil sample (FD-1) at a concentration of 151 mg/kg (Table 6). The soil
from this location was subsequently removed for off-Site disposal, and confirmation samples from the
excavation floor and sidewalls showed remaining soil to be below the established background concentration
of 15 mg/kg for arsenic. No further action is required for this location.
 Arsenic was detected in all groundwater samples collected along the french drain and from four of the six
monitoring wells with concentrations ranging from 0.015 to 0.63 mg/L (Tables 6 and 11). These levels exceed
the UGPS for arsenic set at 0.01 mg/L. Importantly, arsenic was detected in the background well at the Site
(MW-1) at a concentration of 0.018 mg/L, suggesting that arsenic detections above the UGPS in groundwater
are naturally occurring. No remedial action is recommended for this location, but additional groundwater
monitoring is recommended as described in the section below.
 Well MW-3 showed an elevated level of TPH-DRO in groundwater at 1.8 mg/L (Table 11). All groundwater
results were below the EPA Tap Water levels for the indicator compounds for TPH except for arsenic and
manganese. Tetra Tech recommends future groundwater sampling to monitor TPH-DRO concentrations at
this location, as described in the section below.
RECOMMENDATIONS
Tetra Tech recommends no further remedial action on or off Site based on the soil removal actions performed as
part of this work and the results of post-remedial sampling and other sampling conducted during the Site
characterization work. Tetra Tech recommends that an additional round of groundwater sampling be performed in
December 2023 to re-evaluate the presence of arsenic and TPH DRO concentrations in the groundwater.
Recognizing that this is an industrial site and the characterization constituent concentration levels were compared
to regulatory industrial standards, Tetra Tech also recommends that a Site Management Plan (SMP) be prepared
and implemented in accordance with UAC R315-101-7. The SMP will specify controls and conditions to manage
potential risks to human health and the environment to the acceptable levels considered for the current and
reasonably anticipated future industrial land use. The SMP is expected to include the following elements in
tandem with an environmental covenant:
 Restrict land use of the Site to only industrial or commercial uses;
 Present a plan for future groundwater monitoring and analysis, including further evaluation to determine
whether arsenic and manganese in groundwater at the levels detected is a background condition or
related to Site impacts.
Site Characterization Report Recycled Earth
Ogden, Utah
18 November 3, 2023

_6479884.2
 Restrict use of, and require worker protection and management during work in, shallow groundwater until
the TPH-DRO and arsenic issues are resolved to satisfy regulatory acceptable criteria.
The SMP will be submitted to DWMRC within 60 days of agency concurrence with this Report in accordance with
UAC R315-101-7.
Based on the results presented herein and upon concurrence by Ogden City, Recycled Earth will coordinate with
the City to reconnect the Site storm water conveyance systems to the MS4, and corresponding storm water
management will be performed under the existing Industrial Storm Water General Permit and Site-specific Storm
Water Pollution Prevention Plan.

Site Characterization Report Recycled Earth
Ogden, Utah
19 November 3, 2023

_6479884.2
5.0 REFERENCES
Amec Foster Wheeler Environment & Infrastructure, Inc. 2014. Ogden Business Exchange, Remedial Action
Work Plan, Voluntary Cleanup Program, Assistance ID No. C084, Ogden, Utah.
EPA. 2022. Regional Screening Level (RSL) Summary Table (TR=1E-06, HQ-1), May 2022

EPA. 2023. Title 40 - Protection of Environment, Chapter I - Environmental Protection Agency, Subchapter I - Solid
Wastes, Part 261 - Identification and Listing of Hazardous Waste, Subpart C - Characteristics of Hazardous
Waste, May 2023.

EPA. 2021. Multi-Sector General Permit for Stormwater Discharges Associated with Industrial Activity: Part 8 - Sector-
Specific Requirements. Retrieved from https://www.epa.gov/sites/default/files/2021-
01/documents/2021_msgp_-_permit_part_8_-_sector_specific_requirements.pdf

Utah Division of Water Rights Well Database, accessed by web 07/20/2023:
https://maps.waterrights.utah.gov/EsriMap/map.asp

Utah Department of Environmental Quality. 2016. Utah Pollutant Discharge Elimination System: General Permit for
Discharges of Storm Water Runoff Associated with Construction Activities (Permit No. UTG790000).
Retrieved from: https://documents.deq.utah.gov/legacy/permits/water-quality/utah-pollutant-discharge-
elimination-system/docs/utg7900002016.pdf

UDEQ Utah Ground Water Quality Protection Program, accessed by web 12/05/2022: https://deq.utah.gov/water-
quality/standards-utah-ground-water-quality-protection-program

Utah Department of Environmental Quality Division of Waste Management and Radiation Control. 2023. Technical
Guide for Risk Assessments: Utah Administrative Code R315-101 (RGRA).

Tables
Table 1. South Trench and retained Water Detections
STRENCHSW-1 PW-1
Arsenic 0.1 NS 0.072 0.016
Copper 0.003 0.028 <0.01 0.027
Hexavalent Chromium NS NS <0.0005 0.0015
Lead NS 0.164 <0.006 0.036
Selenium NS NS <0.01 0.017
Gasoline Range Organics 1 NS <0.1 <0.1
Diesel Range Organics 1 NS 0.16 <0.2
Oil Range Organics NS NS 0.15 0.54
TPH NS NS 0.31 0.54
Oil & Grease 10 NS <5.68 <6.58
Toluene 0.1 NS 0.0021 <0.001
Notes:
Results with a < symbol were not detected above the laboratory detection limit.
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
Bold values indicate exceedance of State and/or federal screening levels
Water Sample Results (mg/L)
Volatile Organic Compounds (VOCs)
Metals
Petroleum Hydrocarbons
Sector N Benchmark
Limitations (mg/L)Analyte Group Analyte UTG790000 Effluent
Limitations (mg/L)
Table 2: South Trench Excavation Confirmation Sample Results
ST‐CS‐1ST‐CS‐2ST‐CS‐3ST‐CS‐4ST‐CS‐5ST‐CS‐6ST‐CS‐7ST‐CS‐COMP
Gasoline Range Organics 2,200 0.88 <3.8 <4.05 1.5 1.9 <4.02 <4.22 1.6
Diesel Range Organics 440 1.3 1.3 5.3 52 56 1.4 1.8 59
TPH NS 2.2 1.3 5.3 53 58 1.4 1.8 60
1,2,3‐Trichlorobenzene NS <0.0193 <0.019 <0.0203 <0.0218 <0.0171 <0.0201 <0.0211 0.020
1,2,3‐Trimethylbenzene 340 <0.00772 <0.0076 <0.00811 <0.0087 <0.00685 <0.00804 <0.00844 0.026
1,2,4‐Trimethylbenzene 300 <0.00772 <0.0076 <0.00811 <0.0087 <0.00685 <0.00804 <0.00844 0.095
1,3,5‐Trimethylbenzene 270 <0.00772 <0.0076 <0.00811 <0.0087 <0.00685 <0.00804 <0.00844 0.031
4‐Methyl‐2‐pentanone (MIBK) 140,000 0.016 0.022 <0.0405 0.0045 <0.0343 <0.0402 <0.0422 0.011
Ethylbenzene 25 <0.00386 <0.0038 <0.00405 0.0020 <0.00343 <0.00402 <0.00422 <0.00398
Methylene Chloride NS <0.0386 <0.038 <0.0405 0.013 <0.0343 <0.0402 <0.0422 <0.0398
Naphthalene 8.6 <0.0193 <0.019 <0.0203 <0.0218 <0.0171 <0.0201 <0.0211 0.034
n‐Propylbenzene 24,000 <0.00772 <0.0076 <0.00811 <0.0087 <0.00685 <0.00804 <0.00844 0.012
Styrene 35,000 <0.0193 0.00067 <0.0203 <0.0218 <0.0171 <0.0201 <0.0211 <0.0199
Tetrachloroethene 100 <0.00386 <0.0038 <0.00405 <0.00435 <0.00343 <0.00402 <0.00422 0.0066
Toluene 4,900 <0.00772 0.012 0.11 0.017 0.0026 <0.00804 0.0080 0.027
Xylenes, Total 2,500 <0.01 0.0040 <0.0105 0.010 0.0016 <0.0105 0.0029 0.057
1‐Methylnaphthalene 73 <0.0249 <0.025 <0.0253 <0.0247 <0.0235 <0.0259 <0.0262 0.0093
2‐Methylnaphthalene 3,000 <0.0249 <0.025 <0.0253 <0.0247 0.0082 <0.0259 <0.0262 0.015
Acenaphthene 45,000 0.0044 <0.0416 <0.0422 <0.0822 <0.0784 <0.0431 <0.0437 0.003
Anthracene 230,000 0.026 0.0090 <0.0422 <0.0822 <0.0784 <0.0431 <0.0437 <0.21
Benzo(a)anthracene 21 0.26 0.086 0.0062 0.0042 <0.0784 0.057 0.0027 0.0064
Benzo(a)pyrene 2.1 0.22 0.076 0.0092 0.0090 <0.0784 0.070 0.0035 0.0064
Benzo(b)fluoranthene 21 0.29 0.10 0.014 0.017 0.020 0.097 0.0039 0.0059
Benzo(g,h,i)perylene NS <0.0414 0.046 0.0077 0.035 <0.0784 0.056 0.0048 0.0046
Benzo(k)fluoranthene 11 0.10 0.037 0.0050 <0.0822 <0.0784 0.035 <0.0437 <0.21
Chrysene 2,100 0.21 0.074 0.0097 0.012 <0.0784 0.075 <0.0437 0.0059
Dibenz(a,h)anthracene 2.1 0.029 0.010 <0.0422 0.012 <0.0784 0.010 <0.0437 <0.21
Fluoranthene 3,000 0.41 0.14 0.019 0.0058 <0.0784 0.14 0.0056 0.014
Fluorene 30,000 0.0040 <0.0416 <0.0422 <0.0822 <0.0784 <0.0431 <0.0437 <0.21
Indeno(1,2,3‐cd)pyrene 21 0.14 0.054 0.0086 0.0080 <0.0784 0.063 0.0030 0.0034
Naphthalene 8.6 <0.0193 <0.019 <0.0203 <0.0218 <0.0171 <0.0201 <0.0211 0.034
Phenanthrene NS 0.10 0.033 0.0049 0.0043 <0.0784 0.027 <0.0437 0.011
Pyrene 23,000 0.34 0.11 0.015 0.0092 <0.0784 0.12 0.0061 0.014
Notes:
Bold values indicate exceedance of State and/or federal screening levels
Results with a < symbol  were not detected above the laboratory detection limit. 
EPA = Environmental Protection Agency
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
NS = Not Specified
mg/kg = milligram per kilogram
Sample Results (mg/kg)
EPA Industrial 
Screening Level 
(mg/kg)
Analyte Group Analyte
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds 
(VOCs)
Semi‐Volatile 
Organic 
Compounds 
(VOCs)
Table 3: Catch Basin Sample Detections
CB-1 CB-2 CB-3 CB-4 CB-8 CB-9
Arsenic 3 9.6 53 4.2 9.5 18 9.3
Beryllium 2,300 <0.272 0.41 0.33 0.40 <0.281 <0.252
Cadmium 100 <0.679 <0.731 <0.652 0.86 <0.704 <0.629
Chromium NS 16 216 82 86 38.10 10.4
Copper 47000 17 30 65 183 43.30 16.4
Hexavalent Chromium 6.3 <1.36 <1.46 1.6 <1.54 NM NM
Lead 800 5.6 8.9 13 23 10.60 2.6
Nickel NS 9.1 14 27 152 19.60 5.5
Selenium 5,800 <2.72 3.5 <2.61 <3.08 <2.81 <2.52
Zinc NS 37 70 77 471 45.30 18.5
Diesel Range Organics 440 172 212 122 3,600 <113 <101
Oil Range Organics 30,000 585 543 314 9,080 184 303
TPH NS 757 755 436 12,680 <297 <404
1,2,3-Trimethylbenzene 340 <0.0111 <0.0114 <0.00911 0.04 <0.00922 <0.00779
1,2,4-Trimethylbenzene 300 0.012 0.013 <0.00911 0.07 <0.00922 0.016
1,3,5-Trimethylbenzene 270 <0.0111 <0.0114 <0.00911 0.02 <0.00922 <0.00779
2-Butanone (MEK)NS <0.222 0.31 <0.182 <0.277 <0.184 <0.156
4-Methyl-2-pentanone (MIBK)140,000 <0.0555 0.62 <0.0455 <0.0693 <0.0461 <0.039
Benzene 5 0.0026 <0.00228 <0.00182 0.01 0.0040 <0.00156
Ethylbenzene 25 0.0064 <0.00569 <0.00455 0.01 0.018 <0.0039
Naphthalene 8.6 <0.0277 <0.0284 <0.0228 0.06 <0.023 <0.0195
p-Isopropyltoluene NS 0.091 0.035 <0.00911 <0.0138 <0.00922 <0.00779
Styrene 35,000 <0.0277 <0.0284 <0.0228 0.90 <0.023 <0.0195
Tetrachloroethene 100 <0.00555 <0.00569 <0.00455 0.57 0.56 0.026
Toluene 4,900 0.13 0.064 <0.00911 0.030 <0.00922 0.76
Xylenes, Total 2,500 0.019 0.015 <0.0118 0.046 0.066 0.013
1-Methylnaphthalene 73 <0.0272 <0.0293 <0.13 0.20 <0.0281 <0.0252
Benzo(a)anthracene 21 0.0084 0.012 <0.039 0.022 0.0092 <0.419
Benzo(a)pyrene 2.1 <0.00815 0.010 <0.039 0.016 0.011 <0.419
Benzo(b)fluoranthene 21 0.011 0.013 0.043 0.031 0.0097 <0.419
Benzo(g,h,i)perylene NS 0.0097 <0.00878 <0.039 0.028 0.016 <0.419
Chrysene 2,100 0.011 0.013 <0.039 0.023 0.010 <0.419
Fluoranthene 3,000 0.018 0.028 0.055 0.060 <0.469 <0.419
Indeno(1,2,3-cd)pyrene 21 <0.00815 <0.00878 <0.039 0.016 <0.469 <0.419
Naphthalene 8.6 <0.0277 <0.0284 <0.0228 0.064 <0.023 <0.0195
Phenanthrene NS 0.016 0.027 <0.039 0.097 0.00887 <0.419
Pyrene 23,000 0.020 0.031 0.048 0.18
0.0211 0.00828
Notes:
Results with a < symbol were not detected above the laboratory detection limit.
Regional Industrial Soil Screening Levlels are from the United States Environmental Protection Agency (EPA) website:
https://www.epa.gov/risk/regional-screening-levels-rsls-generic-tables
TPH = Total Petroleum Hydrocarbons
mg/kg = milligram per kilogram
B = Same analyte is found in associated blank.
NM = Not Measured
Bold values indicate exceedance of State and/or federal screening levels
Sample Results (mg/kg)
Petroleum
Hydrocarbons
Volatile Organic
Compounds
(VOCs)
Semi-Volatile
Organic
Compounds
(VOCs)
EPA Industrial
Screening Level
(mg/kg)
Metals
Analyte Group Analyte
B
CS‐1CS‐2CS‐3CS‐4CS‐5
Arsenic 3 3.2 3.4 5.4 10 6.3
Beryllium 2,300 0.33 0.27 0.38 0.31 0.40
Chromium NS 8.5 15 9.6 7.6 10.3
Copper 47000 8.0 14 9.5 16 8.5
Lead 800 3.28 4.12 4.07 25.60 5.43
Nickel NS 6.2 7.8 6.9 5.6 7.3
Zinc NS 25 23 29 44 31
Gasoline Range Organics 2,200 <4 <3.96 <4.78 <4.22 <4.13
Diesel Range Organics 440 <5.18 16 <5.73 <5.31 9.0
Oil Range Organics 30,000 <5.18 42 <5.73 14 26
TPH NS <14.36 58 <16.24 14 35
Acetone 1,100,000 <0.0799 <0.0793 <0.0957 0.089 <0.0826
Tetrachloroethene 100 <0.004 0.0088 <0.00478 <0.00422 0.0077
Notes:
Bold values indicate exceedance of State and/or federal screening levels
Results with a < symbol  were not detected above the laboratory detection limit. 
EPA = Environmental Protection Agency
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
mg/kg = milligram per kilogram
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds 
Sample Results (mg/kg)
EPA Industrial 
Screening Level 
(mg/kg)
Metals
Analyte Group Analyte
Table 4: Maintenance Building Excavation Confirmation Sample Results
Site‐South Site‐ North SE‐POND OUTFALL #1
COD 120 39 51 71 55
TSS 70 100 50 266 8.7 21
TDS 1,200 657 637 772 576
pH1 6.5‐9.0 8.8 11 10 10
Aluminum 0.75 1.6 3.6 <0.2 <0.2
Arsenic 0.1 0.0267 0.011 0.0215 0.0134
Barium 1.0 0.121 0.17 0.1 0.0471
Beryllium 0.0004 <0.002 <0.002 <0.002 <0.002
Cadmium 0.26 <0.002 <0.002 <0.002 <0.002
Chromium 0.1 0.0132 0.026 <0.01 0.0129
Copper 0.003 0.032 0.024 0.034 0.023 0.033
Iron 1.0 1.0 2.9 6.7 0.3 0.24
Lead 0.10 0.262 <0.005 0.0071 <0.005 <0.005
Mercury 0.002 <0.0002 <0.0002 <0.0002 <0.0002
Selenium 0.050 <0.01 <0.01 <0.01 <0.01
Silver 0.050 <0.005 <0.006 <0.005 <0.005
Zinc 0.04 0.26 <0.05 0.061 <0.05 <0.05
Oil and Grease 10.0 < 5.62 < 5.63 < 5.62 < 5.62
Benzene 0.0 <.001 <.002 <.001 <.001
BTEX 0.1 <0.01 <0.02 <0.03 <0.03
MTBE 0.2 <.001 <.002 <.001 <.001
Napthalene 0.7 <0.001 <0.000 <0.001 <0.001
TTO2 2.0 <2.0 <2.0 0.004 0.011
TPH GRO 1.0 <0.1 <0.1 <0.1 <0.1
TPH DRO 1.0 0.87 3.1 0.80 1.2
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
mg/L = milligram per liter
TPH = Total Petroleum Hydrocarbons
TTO = Total Toxic Organics
Bold values indicate exceedance of State and/or federal screening levels
1: Units are standard pH units
2: Results for SITE‐SOUTH and SITE‐NORTH were non‐detect for all TTO compounds
Results (mg/L)Sector N 
Benchmark 
Limitations 
(mg/L)
UTG790000 
Effluent 
Limitations 
(mg/L)
Analyte
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Table 5: Detained Water Sample Detections
Table 6: French Drain Sample Results
FD-1 FD-2 FD-3 FD-4 FD-5 FD-1 FD-2 FD-3 FD-4 FD-5
Arsenic 0.01 0.000052 0.01 0.015 0.047 0.026 0.041 0.023 NS 3 151 14 8.1 6.5 6.2
Beryllium 0.004 0.25 0.004 <0.002 <0.002 <0.002 <0.002 <0.002 NS 2300 <0.264 <0.24 0.323 0.284 0.298
Chromium 0.1 NS 0.1 <0.01 <0.01 <0.01 0.018 0.020 NS NS 8.0 5.6 16 28 59
Copper 1.3 0.8 1.3 <0.01 <0.01 <0.01 0.019 0.038 NS 47 5.6 <2.4 26 35 75
Hexavalent Chromium NS 0.000035 NS <0.0005 <0.0005 <0.0005 0.001 0.001 NS 6.3 <1.32 <1.2 <1.18 <1.22 1.58
Lead 0.015 0.015 0.015 <0.006 <0.006 <0.006 0.006 <0.006 NS 8 4.4 0.88 13 7.6 14
Mercury 0.002 0.00063 0.002 0.00031 0.00045 <0.0002 <0.0002 0.00034 NS 46 <0.0528 <0.048 <0.0474 <0.0487 <0.051
Nickel 0.006 0.000047 0.2 0.013 0.012 <0.01 0.019 0.020 NS NS 7.7 3.3 12 14 30
Selenium 0.05 0.1 0.05 0.019 <0.01 <0.01 <0.01 <0.01 NS 58 <2.64 <2.4 <2.37 <2.44 <2.55
Zinc 5 0.6 NS <0.05 <0.05 <0.05 <0.05 <0.05 NS 350,000 18 10.0 46 42 55
Arsenic 0.01 0.000052 0.01 0.024 0.070 0.021 0.035 0.025 NS 3 NM NM NM NM NM
Hexavalent Chromium NS 0.000035 NS <0.0005 <0.0005 <0.0005 0.00059 0.00072 NS 0.3 NM NM NM NM NM
Nickel 0.006 0.000047 0.2 <0.01 0.017 <0.01 <0.01 <0.01 NS NS NM NM NM NM NM
Selenium 0.05 0.1 0.05 <0.01 <0.01 <0.01 0.013 <0.01 NS 58 NM NM NM NM NM
Gasoline Range Organics NS NS NS <0.1 <0.1 <0.1 <0.5 <0.1 150 3,500,000 <4.31 5.8 8.0 <3.73 <4.01
Diesel Range Organics NS NS NS <0.1 0.46 0.27 0.70 0.45 500 520 15 <4.8 59 39 12
Oil Range Organics NS NS NS <0.1 0.32 0.16 0.32 0.71 NS 2,200 64 <4.8 121 117 54
TPH NS NS NS <0.3 0.78 0.42 1.0 1.2 NS NS 79 5.8 188 156 66
Oil & Grease NS NS NS <6.76 <5.95 <6.41 10.800 <6.1 1000 NS NM NM NM NM NM
PCB 1254 NS NS NS <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 NS 0.94 <0.0224 <0.0204 <0.0201 <0.0207 0.0895
1,2,3-Trimethylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS 2,000 <0.00862 <0.00718 0.081 <0.00747 <0.00801
1,2,4-Trimethylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS 1,800 <0.00862 <0.00718 0.25 <0.00747 <0.00801
1,3,5-Trimethylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS 1,500 <0.00862 <0.00718 0.068 <0.00747 <0.00801
Ethylbenzene 0.7 0.0015 0.7 <0.001 <0.001 <0.001 <0.001 <0.001 5 25 <0.00431 <0.00359 0.016 <0.00373 <0.00401
Isopropylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS NS <0.00431 <0.00359 0.010 <0.00373 <0.00401
n-Butylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS 58,000 <0.0216 <0.0179 0.040 <0.0187 <0.02
n-Propylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS 24,000 <0.00862 <0.00718 0.034 <0.00747 <0.00801
Naphthalene NS 0.00012 NS <0.005 <0.005 <0.005 <0.005 <0.005 51 8.6 <0.0216 <0.0179 0.034 <0.0187 <0.02
p-Isopropyltoluene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS NS <0.00862 <0.00718 0.088 <0.00747 <0.00801
sec-Butylbenzene NS NS NS <0.001 <0.001 <0.001 <0.001 <0.001 NS 12 <0.0216 <0.0179 0.024 <0.0187 <0.02
Toluene 1 1.1 1 <0.001 0.0016 0.0033 <0.001 <0.001 9 47,000 <0.00862 <0.00718 0.22 <0.00747 <0.00801
Xylenes, Total 10 0.19 10 <0.003 <0.003 <0.003 <0.003 <0.003 142 2,500 <0.0112 <0.00933 0.11 <0.00971 <0.0104
Acenaphthene NS 0.53 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 45,000 0.010 <0.04 0.0078 <0.0406 <0.0425
Anthracene NS 1.8 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 23,000 0.011 <0.04 <0.0394 <0.0406 <0.0425
Benzo(a)anthracene NS NS NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 21 0.023 <0.04 0.019 0.044 0.010
Benzo(a)pyrene NS 0.000025 0.0002 <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 2.1 0.020 <0.04 0.016 0.033 0.013
Benzo(b)fluoranthene NS 0.00025 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 21 0.021 <0.04 0.017 0.051 0.012
Benzo(g,h,i)perylene NS NS NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS NS 0.015 <0.04 0.018 0.032 0.028
Benzo(k)fluoranthene NS NS NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 210 0.0093 <0.04 <0.0394 0.017 <0.0425
Chrysene NS 0.025 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 210 0.028 <0.04 0.022 0.045 0.012
Fluoranthene NS 0.8 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 30,000 0.072 <0.04 0.040 0.090 0.015
Indeno(1,2,3-cd)pyrene NS 0.00025 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 21 0.013 <0.04 0.011 0.027 0.012
Phenanthrene NS NS NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS NS 0.064 <0.04 0.058 0.027 0.018
Pyrene NS 0.12 NS <0.00105 <0.00105 <0.001 <0.001 <0.001 NS 23,000 0.069 <0.04 0.051 0.14 0.050
Notes:
1: EPA Tap Water Levels are listed for Indicator Compounds Associated with Common TPH Mixtures specified in Table 5 of the Division of Waste Management and Radiation Control Technical Guide for Risk Assessments, Section
5.2.7. Results with a < symbol were not detected above the laboratory detection limit.
EPA = Environmental Protection Agency
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
mg/kg = milligram per kilogram
Bold values indicate exceedance of State and/or federal screening levels
NM = Not Measured
NS = Not Specified
Petroleum Hydrocarbons
Polychlorinated biphenyls (PCBs)
Semi-Volatile Organic Compounds
(VOCs)
Filtered Metals
Soil Sample Results (mg/kg)UDEQ Groundwater
Quality Standards
(mg/L)
Water Sample Results (mg/L)
UDEQ Soil Initial
Screening Levels
(mg/kg)
EPA Industrial
Screening Level
(mg/kg)
EPA Maximum
Contaminate Level
(mg/L)
EPA Tapwater Level
for TPH Indicator
Compounds 1 (mg/L)
Volatile Organic Compounds (VOCs)
Analyte Group Analyte
Metals
Table 7: Surface Soil Sample Results
SS‐1
(On‐Site)
SS‐2
(On‐Site)
SS‐3
(On‐Site)
SS‐4
(On‐Site)
SS‐5
(On‐Site)
SS‐6
(On‐Site)
SS‐7
(On‐Site)
SS‐8 
(Off‐Site)
SS‐9 
(Off‐Site)
SS‐10
(Off‐Site)
SS‐11
(Off‐Site)
SS‐12
(Off‐Site)
SS‐13
(Off‐Site)
Arsenic 3 6.91 12.4 10.2 7.37 5.7 7.4 5.2 11 9.5 11 10 6.3 87
Beryllium 2,300 <0.24 1.02 0.368 0.39 0.43 0.34 <0.389 0.39 0.40 0.58 0.61 0.38 4.59
Cadmium 100 <0.6 <0.81 <0.593 <0.651 <0.557 <0.746 <0.972 <0.895 <0.868 <1.19 0.84 <0.68 <0.946
Chromium NS 7.9 21 18 20 30 8.8 48 9.2 5.9 17 38 21 33
Copper 47000 6.4 12 33 29 40 15 25 19 17 28 49 17 44
Lead 800 4.8 11 23 21 13 21 18 40 29 36 43 30 14
Mercury 46 <0.048 <0.0648 <0.0474 <0.0521 <0.0445 <0.0597 <0.0778 <0.0716 <0.0694 <0.0955 0.07 <0.0544 <0.0757
Nickel NS 5.6 12 12 12 19 6.8 13 7.4 5.7 11 19 7.0 29
Silver 5,800 <1.2 <1.62 <1.19 <1.3 <1.11 <1.49 <1.94 <1.79 <1.74 <2.39 <1.55 <1.36 2.6
Zinc NS 18 39 56 58 45 43 88 105 71 168 421 103 231
Gasoline Range Organics 2,200 <3.66 <5.77 5.4 <4.11 <3.21 <5.17 <7.7 <7.23 <7.62 32.70 <7.63 <4.77 <8.17
Diesel Range Organics 440 <4.8 <6.48 255 <26 <89.1 <5.97 24 15 <6.94 <9.55 <124 <54.4 946
Oil Range Organics 30,000 8.5 19 198 47 538 <5.97 176 16 <6.94 <9.55 261 <54.4 817
TPH NS 8.5 19 458 47 538 <17 200 31 <22 33 261 <115 1763
1,2,3‐Trimethylbenzene 340 <0.00733 <0.0115 0.024 <0.00821 <0.00641 <0.0103 <0.0308 <0.0144 <0.0152 <0.0207 <0.0152 <0.00876 <0.0163
1,2,4‐Trimethylbenzene 300 <0.00733 <0.0115 0.15 <0.00821 <0.00641 <0.0103 <0.0308 <0.0144 <0.0152 <0.0207 <0.0152 <0.00876 <0.0163
1,3,5‐Trimethylbenzene 270 <0.00733 <0.0115 0.053 <0.00821 <0.00641 <0.0103 <0.0308 <0.0144 <0.0152 <0.0207 <0.0152 <0.00876 <0.0163
Isopropylbenzene NS <0.00366 <0.00577 0.0060 <0.00411 <0.00321 <0.00517 <0.0154 <0.00723 <0.00762 <0.0104 <0.00763 <0.00438 <0.00817
n‐Propylbenzene NS <0.00733 <0.0115 0.033 <0.00821 <0.00641 <0.0103 <0.0308 <0.0144 <0.0152 <0.0207 <0.0152 <0.00876 <0.0163
p‐Isopropyltoluene NS <0.00733 <0.0115 0.45 <0.00821 <0.00641 <0.0103 <0.0308 <0.0144 <0.0152 <0.0207 <0.0152 <0.00876 <0.0163
Tetrachloroethene 100 <0.00366 <0.00577 <0.00347 <0.00411 0.0055 <0.00517 <0.0154 <0.00723 <0.00762 <0.0104 <0.00763 <0.00438 <0.00817
Toluene 4,900 <0.00733 <0.0115 0.13 0.0126 <0.00641 <0.0103 0.05 0.70 <0.0152 <0.0207 <0.0152 0.01 <0.0163
Xylenes, Total 2,500 <0.00952 <0.015 0.018 <0.0107 <0.00834 <0.0134 <0.04 <0.0187 <0.0198 <0.0269 <0.0199 <0.0114 <0.0212
1‐Methylnaphthalene 73 <0.024 <0.0324 0.36 <0.026 <0.0223 <0.0298 <0.0389 <0.0358 <0.0347 <0.0477 <0.031 <0.0272 <0.0378
2‐Methylnaphthalene 3,000 <0.024 <0.0324 0.38 <0.026 <0.0223 <0.0298 <0.0389 <0.0358 <0.0347 <0.0477 <0.031 <0.0272 <0.0378
Acenaphthene NS <0.04 <0.054 2.0 <0.0433 <0.00668 <0.0497 <0.0647 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Anthracene NS <0.04 <0.054 2.1 <0.0433 <0.00668 <0.0497 <0.0647 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Benzo(a)anthracene 21 <0.04 <0.054 <0.395 0.0083 0.019 <0.0497 0.012 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Benzo(a)pyrene 2.1 <0.04 <0.054 1.8 <0.0433 0.027 <0.0497 0.013 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Benzo(b)fluoranthene 21 <0.04 <0.054 1.8 0.010 0.027 <0.0497 0.018 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Benzo(g,h,i)perylene NS <0.04 <0.054 0.76 0.0082 0.045 <0.0497 0.020 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Benzo(k)fluoranthene 11 <0.04 <0.054 0.69 <0.0433 0.0089 <0.0497 <0.0647 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Chrysene 2,100 <0.04 <0.054 3.0 0.0093 0.019 <0.0497 0.014 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Dibenz(a,h)anthracene 2.1 <0.04 <0.054 0.25 <0.00781 0.0071 <0.0497 <0.0647 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Fluoranthene 3,000 <0.0072 0.013 6.6 0.017 0.027 <0.0497 0.026 <0.0596 <0.0578 <0.399 0.01 <0.0453 <0.316
Fluorene NS <0.04 <0.054 1.1 <0.00781 <0.00668 <0.0497 <0.0647 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Indeno(1,2,3‐cd)pyrene 21 <0.04 <0.054 1.0 <0.0433 0.019 <0.0497 0.012 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Phenanthrene NS <0.04 0.010 8.2 0.013 0.014 <0.0497 0.018 <0.0596 <0.0578 <0.399 <0.0516 <0.0453 <0.316
Pyrene 23,000 <0.0072 0.014 6.4 0.018 0.046 0.0093 0.022 <0.0596 <0.0578 <0.399 0.012 <0.0453 <0.316
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
Regional Industrial Soil Screening Levlels are from the United States Environmental Protection Agency (EPA) website: https://www.epa.gov/risk/regional‐screening‐levels‐rsls‐generic‐tables
TPH = Total Petroleum Hydrocarbons
mg/kg = milligram per kilogram
Bold values indicate exceedance of State and/or federal screening levels
Sample Results (mg/kg)
EPA Industrial 
Screening Level 
(mg/kg)
Metals
Analyte Group Analyte
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds 
(VOCs)
Semi‐Volatile 
Organic 
Compounds 
(VOCs)
Table 8: Surface Water Sample Detections
SW‐1SW‐2SW‐3SW‐4SW‐5
Arsenic 0.1 NS 0.047 0.028 0.028 0.065 0.052
Copper 0.003 0.032 0.022 <0.01 0.020 <0.01 <0.01
Hexavalent Chromium NS NS 0.001 0.00055 <0.0005 0.0027 <0.0005
Lead 0.1 0.262 0.018 <0.006 <0.006 <0.006 <0.006
Zinc 0.04 0.026 0.14 <0.05 <0.05 <0.05 <0.05
Diesel Range Organics 1.0 NS 67 0.16 0.13 <0.1 <0.1
TPH NS NS 67 0.16 0.13 <6.9 <6.2
cis‐1,2‐Dichloroethene NS NS <0.001 <0.001 <0.001 <0.001 0.0021
Trichloroethene NS NS <0.001 <0.001 <0.001 <0.001 0.0027
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
TPH = Total Petroleum Hydrocarbons
mg/L = milligram per liter
Bold values indicate exceedance of State and/or federal screening levels
Water Sample Results (mg/L)
Analyte Group Analyte
Petroleum Hydrocarbons 
Sector N 
Benchmark 
Limitations 
(mg/L)
Volatile Organic 
Compounds (VOCs)
Metals
UTG790000 
Effluent 
Limitations (mg/L)
Table 9: Crushed Concrete Sample Detections
CS‐1CS‐2CS‐3CS‐4
Arsenic 100 3 3.8 <2.19 2.4 <2.13
Beryllium NS 2,300 0.24 0.44 0.85 0.34
Chromium 100 NS 10 19 26 14
Copper NS 47,000 39 12 35 3.6
Hexavalent Chromium NS 6.3 2.1 <1.1 2.3 <1.07
Lead 100 800 2.8 11 19 13
Nickel NS NS 4.5 8.8 14 5.8
Zinc NS NS 23 33 57 22
Diesel Range Organics NS 440 70 <4.39 43 9.1
Oil Range Organics NS 30,000 363 <4.39 38 24
TPH NS NS 433 <11.85 81 33
1,2,3‐Trimethylbenzene NS 2,000 <0.00674 0.010 <0.00674 <0.00647
1,2,4‐Trimethylbenzene NS 1,800 <0.00674 0.011 <0.00674 <0.00647
1,3,5‐Trimethylbenzene NS 1,500 <0.00674 0.0079 <0.00674 <0.00647
Isopropylbenzene NS 9,900 0.0051 <0.00307 <0.00337 <0.00324
p‐Isopropyltoluene NS NS 0.033 <0.00613 <0.00674 <0.00647
Styrene NS 35,000 0.14 <0.0153 <0.0169 <0.0162
Tetrachloroethene 14 100 <0.00337 <0.00307 <0.00337 0.014
Toluene NS 47,000 0.0094 <0.00613 <0.00674 0.0091
Xylenes, Total NS 2,500 0.017 0.023 <0.00876 <0.00841
Benzo(a)anthracene NS NS 0.14 <0.0365 <0.187 0.016
Benzo(a)pyrene NS 2.1 0.11 <0.0365 <0.187 0.021
Benzo(b)fluoranthene NS 21 0.043 <0.0365 <0.187 0.030
Benzo(g,h,i)perylene NS NS 0.091 <0.0365 <0.187 0.016
Dibenz(a,h)anthracene NS 2.1 0.014 <0.0365 <0.187 <0.0355
Indeno(1,2,3‐cd)pyrene NS 21 0.030 <0.0365 <0.187 0.018
Phenanthrene NS NS 0.047 <0.0365 <0.187 0.014
Pyrene NS 23,000 0.33 <0.0365 <0.187 0.026
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
NS = Not Specified
EPA = Environmental Protection Agency
Toxicity Characteristic Leachate Procedure
TPH = Total Petroleum Hydrocarbons
mg/L = milligram per liter
mg/kg = milligram per kilogram
Bold values indicate exceedance of State and/or federal screening levels
Sample Results (mg/kg)
Metals
Analyte Group Analyte TCLP "Rule‐of‐20" Equivalent
(mg/L)
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds (VOCs)
Semi‐Volatile 
Organic 
Compounds (VOCs)
EPA Industrial 
Screening Level 
(mg/kg)
Table 10: Soil Boring Sample Detections
MW‐1MW‐2MW‐3MW‐4MW‐5MW‐6
Arsenic 3 4.9 8.5 13 6.3 6.0 4.6
Beryllium 2,300 0.29 0.44 0.41 0.41 0.31 0.35
Chromium NS 7.7 13 10 11 8.0 14
Copper 47000 7.4 16 12 17 5.6 14
Lead 800 3.9 16 8.2 12 3.7 15
Nickel NS 5.9 9.9 7.7 7.4 5.2 7.3
Zinc 350 23 40 35 39 21 49
Gasoline Range Organics 2,200 <3.7 <3.94 <3.84 <4.04 <3.94 <3.64
Diesel Range Organics 440 <6.03 <5.11 <4.93 <5.17 <4.69 <467
Oil Range Organics 30,000 6.2 8.5 <4.93 5.9 <4.69 732
TPH NS 6.2 8.5 <13.7 5.9 <13.3 732
1,2,3‐Trimethylbenzene 340 <0.0074 <0.00788 <0.00768 <0.00808 <0.00789 0.042
1,3,5‐Trimethylbenzene 270 <0.0074 <0.00788 <0.00768 <0.00808 <0.00789 0.066
Acetone 1,100,000 <0.074 <0.0788 0.079 <0.0808 0.0801 <0.0727
Ethylbenzene 25 <0.0037 0.020 <0.00384 <0.00404 <0.00394 <0.00364
Tetrachloroethene 100 <0.0037 <0.00394 <0.00384 <0.00404 <0.00394 0.79
Trichloroethene 6 <0.00148 <0.00158 <0.00154 <0.00162 <0.00158 0.0097
Xylenes, Total 2,500 <0.00962 0.10 <0.00999 <0.0105 <0.0103 0.015
Anthracene 230,000 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.083
Benzo(a)anthracene 21 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.13
Benzo(a)pyrene 2.1 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.12
Benzo(b)fluoranthene 21 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.12
Benzo(g,h,i)perylene NS <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.12
Chrysene 2,100 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.17
Fluoranthene 3,000 <0.00735 <0.00766 <0.00739 0.011 <0.00703 0.27
Indeno(1,2,3‐cd)pyrene 21 <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.074
Phenanthrene NS <0.00735 <0.00766 <0.00739 <0.00776 <0.00703 0.28
Pyrene 23,000 <0.00735 <0.00766 <0.00739 0.0078 <0.00703 0.33
Notes:
Results with a < symbol  were not detected above the laboratory detection limit. 
EPA = Environmental Protection Agency
TPH = Total Petroleum Hydrocarbons
UDEQ = Utah Departmetn of Environmental Quality
mg/L = milligram per liter
mg/kg = milligram per kilogram
NS =Not Specified
Bold values indicate exceedance of State and/or federal screening levels
Sample Results (mg/kg)
Petroleum 
Hydrocarbons 
Volatile Organic 
Compounds 
(VOCs)
Semi‐Volatile 
Organic 
Compounds 
(VOCs)
EPA Industrial 
Screening Level 
(mg/kg)
Metals
Analyte Group Analyte
Table 11: Groundwater Monitoring Well Sample Results
Diesel Range Organics NS NS NS
TPH NS NS NS
2-Butanone (MEK)0.17 5.6 NS
4-Methyl-2-pentanone (MIBK)3 NS NS
Acetone 4 NS NS
Toluene 1 1.1 1.0
Alkalinity,Bicarbonate NS NS NS
Ammonia Nitrogen NS NS NS
Calcium NS NS NS
Chloride NS NS NS
Chemical Oxygen Demand NS NS NS
Dissolved Solids NS NS NS
Nitrate as N NS 32 10
pH (Standard Units)NS NS NS
Potassium NS NS NS
Sodium NS NS NS
Sulfate NS NS NS
Total Organic Carbon NS NS NS
Unfiltered Filtered Unfiltered Filtered Unfiltered Filtered Unfiltered Filtered Unfiltered Filtered Unfiltered Filtered
Arsenic 0.01 0.000052 0.01 0.018 0.012 0.021 0.014 0.60 0.63 <0.01 <0.01 0.029 0.034 <0.01 <0.01
Iron NS 14 NS 3.6 NA 0.338 NA 6.0 NA 1.2 NA 0.12 NA 1.54 NA
Magnesium NS NS NS 45 NA 46 NA 67 NA 62 NA 40 NA 58 NA
Manganese NS 0.43 NS 0.14 NA 0.63 NA 0.73 NA 0.93 NA 0.41 NA 0.44 NA
Nickel 0.006 NS NS <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.011 0.011 <0.01 <0.01 <0.01 <0.01
EPA Maximum
Contaminate Level
(mg/L)
EPA Maximum
Contaminate Level
(mg/L)
<0.01
<0.05
<0.01
<0.05
<0.01
<0.05
0.19
0.10
830
97
371 347
0.70
238
21
<0.25
320
10
95
Metals
<0.01
<0.05
<0.01
<0.05
414
<0.25
430
<20
894
0.19
8.0
95
0.62
119
<20
635 10,600
<0.1
217
0.80
0.80
Groundwater Sample Results (mg/L)
<0.001
0.34
0.34
<0.001
1.8
0.0058 <0.001
22
207
<0.01 <0.01
1.8
MW-5
345
<0.25
41
MW-1 MW-2 MW-3
8.8
7.9
47
2.7
1,250
2.4
7.7
91
3.2 7.7
MW-6
5.2
7.7
78
5.6
26
73
MW-4
<20
468
2.6
8.1
26
3.0
197
6.5
30
7.4
Analyte Group Analyte
UDEQ Groundwater
Quality Standards
(mg/L)
51
10
110
8.0
252
Inorganic Constituents
461
1.3
271
7.7
12
Analyte Group
EPA Tapwater Level for
TPH Indicator
Compounds 1 (mg/L)
138 153 176 63 175
<0.1
<0.001
<0.1
<0.1
<0.001
<0.01 <0.01 0.13
Analyte
EPA Tapwater Level for
TPH Indicator
Compounds1 (mg/L)
Notes:
1: EPA Tap Water Levels are listed for Indicator Compounds Associated with Common TPH Mixtures specified in Table 5 of the Division of Waste Management and Radiation Control Technical Guide for Risk Assessments, Section
5.2.7. Results with a < symbol were not detected above the laboratory detection limit.
EPA = Environmental Protection Agency
MCL = Maximum Contaminant Level
RSL = Regional Screening Level
TPH = Total Petroleum Hydrocarbons
mg/L = milligram per liter
pH is reported in Standard Units; not mg/L
Bold values indicate exceedance of State and/or federal screening levels
NS = Not Specified
NA = Not Sampled
<0.01
Groundwater Sample Results (mg/L)
MW-6
Utah Groundwater
Protection Standards
Standards (mg/L)
Volatile Organic Compounds (VOCs)
Petroleum Hydrocarbons
MW-1 MW-2 MW-3 MW-4 MW-5
<0.1
<0.1
<0.1
Table 12: Quality Assurance Sample Results
SS‐9 (mg/kg) DUP‐1 (mg/kg) RPD (%) SS‐11 (mg/kg) DUP‐2 (mg/kg) RPD (%) CB‐9 (mg/kg) DUP‐5 (mg/kg) RPD (%)FD‐5 soil 
(mg/kg)
DUP soil 
(mg/kg)RPD (%)FD‐5 water 
(mg/L)
DUP water 
(mg/L)RPD (%)ST‐CS‐4 
(mg/kg)
ST‐CS‐DUPE 
(mg/kg)RPD (%)
Antimony <3.47 6.0 NA <3.1 <3.21 NA <2.52 <2.42 NA <2.55 <2.43 NA <0.01 <0.01 NA NM NM NM
Arsenic 9.5 10 8.9 10 12 12 9.3 12 29 6.2 6.0 4.1 0.023 0.024 3.4 NM NM NM
Beryllium 0.40 0.64 46 0.61 0.38 46 <0.252 <0.242 NA 0.30 <0.243 NA <0.002 <0.002 NA NM NM NM
Cadmium <0.868 <0.944 NA 0.84 <0.802 NA <0.629 <0.606 NA <0.638 <0.608 NA <0.002 <0.002 NA NM NM NM
Chromium 5.9 10 55 38 60 46 10 30 96 59 40 40 0.020 <0.01 NA NM NM NM
Copper 17 24 30 49 51 4.0 16 37 77 75 52 36 0.038 0.014 93 NM NM NM
Hexavalent Chromium <1.74 <1.89 NA <1.55 <1.6 NA NM NM NM 1.6 1.4 9.3 0.00067 0.0018 91 NM NM NM
Lead 29 42 38 43 44 1.4 2.6 6.5 87 14 11 29 <0.006 <0.006 NA NM NM NM
Mercury <0.0694 <0.0755 NA 0.069 0.080 14 NM NM NM <0.051 <0.0487 NA 0.00034 0.00027 21 NM NM NM
Nickel 5.7 8.6 40 19 19 0.52 5.5 14 88 30 21 34 0.020 0.012 50 NM NM NM
Zinc 71 98 33 421 416 1.2 19 37 68 55 43 25 NM NM NM NM NM NM
Gasoline Range Organics <7.62 <7.99 NA <7.63 <11.3 NA <3.9 <3.68 NA <4.01 <3.65 NA <0.1 NM NA 1.50 <3.81 NA
Diesel Range Organics <6.94 <7.55 NA <124 <63.9 NA <101 46.10 NA 12.10 <243 NA 0 0 8.6 52 9 138
Oil Range Organics <6.94 <7.55 NA 261 220 17 303 104 98 54 647 169 1 0 85 NM NM NM
TPH <21 <22 NA 261 220 17 303 150 67 66 <115 NA 1 NM NM NM NM NM
Polychlorinated biphenyls (PCBs)PCB 1254 <0.0295 <0.0321 NA <0.0264 <0.0542 NA NM NM NM 0.090 <0.0207 NA <0.0005 <0.0005 NA NM NM NM
1,2,4‐Trimethylbenzene <0.0152 <0.016 NA <0.0152 <0.0226 NA 0.02 <0.00736 NA <0.00801 <0.00729 NA <0.001 <0.001 NA <0.0087 <0.00762 NA
4‐Methyl‐2‐pentanone (MIBK)<0.0762 <0.0799 NA <0.0763 <0.113 NA <0.039 <0.0368 NA <0.0401 <0.0365 NA <0.01 <0.01 NA 0.0045 <0.0381 NA
Ethylbenzene <0.00762 <0.00799 NA <0.00763 <0.0113 NA <0.0039 <0.00368 NA <0.00401 <0.00365 NA <0.001 <0.001 NA 0.0020 <0.00381 NA
Methylene Chloride <0.0762 <0.0799 NA <0.0763 <0.113 NA <0.039 <0.0368 NA <0.0401 <0.0365 NA <0.005 <0.005 NA 0.013 <0.0381 NA
Styrene <0.038 <0.0401 NA <0.0381 <0.0565 NA <0.0195 <0.0184 NA <0.02 <0.0182 NA <0.001 NM NA <0.0218 0.00088 NA
tert‐Butylbenzene <0.0152 <0.016 NA <0.0152 <0.0226 NA <0.00779 <0.00736 NA <0.00801 <0.00729 NA <0.001 NM NA <0.0087 <0.00762 NA
Tetrachloroethene <0.00762 <0.00799 NA <0.00763 <0.0113 NA 0.026 0.0091 97 <0.00401 <0.00365 NA <0.001 NM NA <0.00435 <0.00381 NA
Toluene <0.0152 <0.016 NA <0.0152 <0.0226 NA 0.76 0.37 69 <0.00801 <0.00729 NA <0.001 NM NA 0.017 <0.00762 NA
Trichloroethene <0.00304 <0.0032 NA <0.00305 <0.00452 NA 0.0020 <0.00147 NA <0.0016 <0.00146 NA NM NM NM <0.00174 <0.00152 NA
Xylenes, Total <0.0198 <0.0208 NA <0.0199 <0.0295 NA 0.013 <0.00957 NA <0.0104 <0.00948 NA NM NM NM 0.010 0.0023 126
Benzo(a)anthracene <0.0578 <0.0629 NA <0.00931 0.025 NA <0.419 <0.0404 NA 0.010 0.013 26 <0.001 <0.001 NA 0.0042 0.018 125
Benzo(a)pyrene <0.0578 <0.0629 NA <0.00931 0.032 NA <0.419 <0.0404 NA 0.013 0.010 26 <0.001 <0.001 NA 0.0090 0.024 92
Benzo(b)fluoranthene <0.0578 <0.0629 NA 0.013 0.050 118 <0.419 <0.0404 NA 0.012 0.012 0 <0.001 <0.001 NA 0.017 0.037 72
Benzo(g,h,i)perylene <0.0578 <0.0629 NA 0.013 0.049 114 <0.419 <0.0404 NA 0.028 0.015 61 <0.001 <0.001 NA 0.035 0.020 54
Benzo(k)fluoranthene <0.0578 <0.0629 NA <0.0516 <0.107 NA <0.419 <0.0404 NA <0.0425 <0.203 NA <0.001 <0.001 NA <0.00741 0.012 NA
Chrysene <0.0578 <0.0629 NA <0.00931 0.037 NA <0.419 <0.0404 NA 0.012 0.020 52 <0.001 <0.001 NA 0.012 0.026 77
Dibenz(a,h)anthracene <0.0578 <0.0629 NA <0.0516 <0.107 NA <0.419 <0.0404 NA <0.0425 <0.203 NA <0.001 <0.001 NA 0.012 <0.0416 NA
Fluoranthene <0.0578 <0.0629 NA 0.014 0.059 123 <0.00755 0.0087 NA 0.015 0.020 31 <0.001 <0.001 NA 0.0058 0.048 157
Indeno(1,2,3‐cd)pyrene <0.0578 <0.0629 NA <0.0516 <0.107 NA <0.419 <0.0404 NA 0.012 <0.0073 NA <0.001 <0.001 NA 0.0080 0.023 95
Phenanthrene <0.0578 <0.0629 NA <0.00931 0.020 NA <0.00755 0.0077 NA 0.018 0.021 14 <0.001 <0.001 NA 0.0043 0.012 96
Pyrene <0.0578 <0.0629 NA 0.012 0.051 125 0.0083 0.0091 9.8 0.050 0.032 44 <0.001 <0.001 NA 0.0092 0.037 120
Notes:
Results with a < symbol  were not detected above the laboratory detection limit
TPH = Total Petroleum Hydrocarbons
mg/L = milligram per liter
mg/kg = milligram per kilogram
NA=Not Applicable; one or both of the results were non‐detect
NM = Not Measured
RPD = Relative Percent Difference
Sample Results 
Petroleum Hydrocarbons 
Volatile Organic Compounds (VOCs)
Semi‐Volatile Organic Compounds 
(VOCs)
Metals
Analyte Group Analyte
Figures
Figure 1: Site Location Map
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
Legend
Ogden
Maxar
k k
Recyled Earth Site Boundary
Ogden Municipality Boundary
0 0.12 0.23 0.35 0.460.06
Miles
0 0.71 1.42 2.13 2.840.35
Miles
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Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Date 8/11/2023
Retail
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Crusher and
Crushed Concrete
Piles
Compost Area
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Soil Pile
Uncrushed
Concrete Pile
(<5% asphalt)
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Outfall #1
Legend
SouthTrench
Storm Water Outfall
Catch Basins
Catch Basin Drainage
Pipes
French Drain
Detention Basin
Approximate Property
Boundary
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Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 3: Catch Basin Sample Locations
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
Retail
Sales
Crusher and
Crushed Concrete
Piles
Compost Area
CB3
Legend
Catch Basins
Catch Basin Drainage
Pipes
French Drain
Approximate Property
Boundary
Catch Basin Sample
Loaction
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Maxar, Microsoft, Esri Community Maps Contributors, Ogden City, Utah Geospatial
Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 4: Detained Water Extent and
Sample Location
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
Retail
Sales
Crusher and
Crushed Concrete
Piles
Compost Area
Rock Pile
Soil Pile
Uncrushed
Concrete Pile
(<5% asphalt)
CB2
CB9
CB8 CB6
CB3
CB4
CB5
CB7
CB1
Outfall #1
Legend
SouthTrench
Storm Water Outfall
Catch Basins
Catch Basin Drainage Pipes
French Drain
Northeast Detention
Approximate Property
Boundary
Original Extent of Held
Water
Temporary Detention
Basin
m 0 140 280 420 56070
Feet
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Maxar, Microsoft, Esri Community Maps Contributors, Ogden City, Utah Geospatial
Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 5: South Trench and Confirmation Sample
Locations
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
Legend
French Drain
Approximate Property
Boundary
Verification Sample
Location
Extent of South Trench
Excavation
±
ST-CS-1
ST-CS-2
ST-CS-3
ST-CS-4
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0 10 20 30 405
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Maxar, Microsoft, Esri Community Maps Contributors, Ogden City, Utah Geospatial
Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 6: Excavation Near Maintenance Building
Confirmation Sample Locations
Site Characterization Completion Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
Legend
Excavation Confirmation
Sample Location
Excavation Footprint
Maxar, Microsoft, Sources: Esri, HERE,
Garmin, FAO, NOAA, USGS, ©
OpenStreetMap contributors, and the GIS
User Community01.5 3 4.5 60.75
Feet
0 0.01 0.01 0.02 0.020
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Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 7: French Drain Sample locations
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
CB8
Legend
South Trench
Catch Basins
Catch Basin Drainage
Pipes
French Drain
Approximate Property
Boundary
Sample Location
m FD-5
FD-4
FD-3
FD-1
FD-2
CB6
CB7
CB5
CB4
Uncrushed
Concrete Pile
(<5% asphalt)
Soil Pile
Rock Pile
0 70 140 210 28035
Feet
Legend
-South Trench
-Catch Basins
_ Catch Basin Drainage
Pipes
--French Drain
_ Approximate Property
Boundary e Soil Sample Location 0 Concrete_Samples
Figure 8: On-Site Surface Media
Sample Locations
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
["Tl:] TETRA TECH
Date 8/11/2023
Legend
e Soil Sample Location
O Surface Water Sample
Location
Figure 9: Surface Media
Characterization Sample Locations
Along MS4
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
["Tl:] TETRA TECH
Date 8/11/2023
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Maxar, Microsoft, Esri Community Maps Contributors, Ogden City, Utah Geospatial
Resource Center, © OpenStreetMap, Microsoft, Esri, HERE, Garmin, SafeGraph,
GeoTechnologies, Inc, METI/NASA, USGS, Bureau of Land Management, EPA, NPS,
US Census Bureau, USDA
Figure 10: Monitoring Well Locations
and Groundwater Flow
Site Characterization Closeout Report
Recycled Earth LLC
3025 S 1500 W, Ogden, UT 84401
Date 8/11/2023
Legend
Groundwater Monitoring Wells
Grounwater Elevation Countour
0 0.02 0.04 0.06 0.080.01
Miles
Groundwater Flow Direction
4,183 ft
4,280 ft
4,279 ft4,275 ft
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Designed By:AR
Figure
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AUGUST 9, 2023
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Recycled Earth Completion Report
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Project No.: 117-9187001
Groundwater
Soil
BTS
Discharge Stock Wells
Municipal
Water Supply
Ingestion
Ingestion Residents
Cattle
Appendix A
Waste Manifests
CamScanner
Appendix B
Standard Operating Procedures for
Groundwater Monitoring Well Installation
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 1 of 12
Groundwater monitoring well installation
1. Purpose
The purpose of this Standard Operating Procedure (SOP) is to delineate the quality control
measures required to ensure the accurate installation of groundwater monitoring wells. The term
monitoring well is used to denote any environmental sampling well.
2. Procedure
2.1 FIELD PREPARATION
Notify client, property owner prior to sampling date in case there is any requirement to reach
property.
2.1.1 Forms
Gather proper field forms necessary for field sampling such as:
Daily Report Sheets
Field Service Request
Tailgate Health and Safety
Excavation Permits
Utility clearances
Borehole logging form
Well completion forms
Appropriate work plan
2.1.2 Drilling Equipment
Appropriately sized drill rig adequately equipped with sampling equipment, bits, drill stem, etc.
Steam cleaner and water obtained from an approved source for decontaminating
drilling equipment
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 2 of 12

Water level indicator
LEL-oxygen monitor
Steel drums for investigation derived waste (drill cuttings, contaminated PPE, decon
solution) (if necessary)
Source of approved water
Heavy plastic sheeting
Decontamination area

2.1.3 Well installation materials
The specifications for the following materials are included in the well construction:
Well screen
Riser pipe
Plugs/caps
Filter pack
Bentonite
Portland cement
Steel protective casing
Submersible pump
Surge block
Concrete

Decontamination equipment including:
Deionized or distilled water
Alconox
graduated cylinders
paper towel

2.1.4 Personal Equipment
Appropriate PPE (see HASP)
Munsell color chart
Hand lens
Folding rule
First aid kit
Fire extinguisher

2.2 WELL DRILLING PROCEDURE

2.2.1 Rationale
Sound groundwater sample integrity is dependent primarily on strict adherence to properly
conceived monitor well construction and development procedures. In addition, it is equally
important that boreholes (i.e., soil borings, wells, and piezometers) be abandoned properly, when
necessary, to preclude the possibility of cross-contamination of water-bearing zones. To ensure
that these goals are met, the following monitoring well drilling, and completion procedures will be
utilized.
2.2.2 Preliminary procedures
Never assume the rig will arrive on-site completely decontaminated from the previous job.
Always inspect it. Road dust can have elevated levels of organics and inorganics attached to it. It
is always a good idea to have the drillers lay out all the tools from their side tool panels and wash
both the tools and the storage compartments. Between holes and on-site locations, ensure that
dirty tools are decontaminated before being returned to these compartments

The following standard field procedures should be followed at each borehole location:
Check the location and number of the drilling location against a map and against the flag or stake.
A good rule of thumb is to measure twice, and drill once.
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 3 of 12
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 4 of 12

Make sure you have a utility clearance for that location.
Back the rig into position so you do not have to drive over the finished hole.
Set up the work area (and sample holding area) to be upwind of the rig exhaust. This
may require the work area to be moved several times during the day.
Check the condition of the driller’s downhole measuring device. Often these devices are missing
several inches, tenths of inches, or feet, and, if used, will result in contradictory hole and well
completion information.
Remove any electrical tape or materials from any devices that, if lost downhole, could result in
possible contamination of groundwater.
Ensure that the measuring device is decontaminated each time it is used.
Drilling is a team effort that includes personnel and the driller. Arrange with the driller before
activities begin to keep you informed of what he/she sees or believes is happening downhole.
For example, the driller can often tell you when the soil is getting harder or softer, or when
he/she is losing or gaining fluids (the hole is making water). These comments often may be
related later to lithologic and hydro stratigraphic changes and, therefore, may verify logs.

2.2.3 Direct Push Technology
Direct push methods use up to 40,000 pounds of hydraulic force to push a steel
instrumented cone or a sampling device into the ground. No material comes to the surface
unless soil or groundwater samples are being collected.
2.2.3.1 Advantages
This method is generally cleaner than other drilling techniques that require a water supply and
may result in the need to containerize drilling fluids (e.g., muds) as well as cuttings. No material
comes to the surface unless soil or groundwater samples are being collected. Because no drilling
muds introduced to the hole, soil and groundwater samples are considered more accurate and
representative. Sample moisture content is more likely to be representative of the formation.
Small-diameter monitoring wells can be installed quickly and efficiently.

2.2.4.2 Limitations
Limited in depth of penetration to approximately 100 feet depending on the materials encountered
and the size of the drill rig. Can smear a layer of fine-grained soil on the side of borehole that may
prevent groundwater from entering. The finer the matrix, the greater the chance for smearing the
side of the hole.
2.2.3.3 Procedures
Once the rig is in place, ensure that it is level by insisting that the driller use a
carpenter’s level on each rig. Unaided visual assessment of plumbness is not acceptable.
Using the direct push drill rig, advance a carbon steel core sampler containing a 2 or 3-
foot clear acetate sample tube to the desired depth into the soil. This is referred to as a sampling
interval. Carefully watch the progression of the core sampler while recording blow counts and
note irregularities in the penetration rate. Upon removal of the sampler from the borehole, the
acetate sample tube will be removed and the ends will be
capped to prevent volatilization from the sample. Sample tubes will be marked with the
depth interval and the sample orientation. Place acetate sample tubes on clean polyethylene
sheeting for inspection/sampling. Each sample tube will be inspected for the presence of
groundwater. The tube will be cut lengthwise using a decontaminated closed blade knife, and the
soil will be logged. These steps will be repeated until the desired boring depth is reached.
Record observations of:
- Sampler penetration rates.

- Characteristics of sample (i.e., moisture content, color, and texture),
including changes in the nature (behavior) of the sample. For example, if the soil
begins to form balls or rope, moisture in the soil has probably increased at that
depth.
- Gravel, boulders, and competent bedrock will make the rig bounce, or vibrate.
- Remember that the samples appear at the surface after a time lag, and that this lag
increases with the depth of the hole; therefore, it is not possible to correlate
cuttings with the exact depth being drilled.
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 5 of 12
Running, heaving, or flowing sands occur when the carbon steel core intercepts a saturated soil
unit whose fluid or formational pressure pushes its materials out into the boring and up the
augers.
Document all refusals,), rig gyrations, and physical conditions of samplers.

2.3 Well Construction

2.3.1 Casing/Screen
Typically, only polyvinyl chloride (PVC), Teflon (polytetrafluoroethylene or PTFE), and/or
stainless steel will be used.
All well screens will be commercially fabricated, slotted or continuously wound, and have an inside
diameter (ID) equal to or greater than the ID of the well casing. An exception may be needed in
the case of continuously wound screens because their supporting rods may reduce the full ID.
Stainless steel screens may be used with PVC or PTFE well casing. No fitting will restrict the ID
of the joined casing and/or screen. All screens, casings, and fittings will be new. Screens will have
the largest open area per unit length that is practical for the adjacent aquifer and available filter.

Couplings within the casing and between the casing and screen will be compatibly threaded.
Thermal or solvent welded couplings on plastic pipe will not be used. This also applies to
threaded or slip-joint couplings thermally welded to the casing by the manufacturer or in the
field.

Each cap will be constructed to preclude binding to the well casing due to tightness of fit,
unclean surface, or frost, and secure enough to preclude debris and insects from entering the
well. Caps and risers may be threaded; however, sufficient annular space will be allowed
between the well and protective casing to enable one to thaw any frosted shut caps. Preferably,
unfiltered vents will not be placed in these caps or in the well riser/stickup. Unfiltered vents may
compromise water sample integrity by allowing foreign materials to enter the well between
sampling events. Caps will be loose enough to allow equilibration between hydrostatic and
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 6 of 12
atmospheric pressures or have filtered vents. Special cap (and riser) designs will be provided for
wells in floodplains and those instances where the top of the well may be below grade, e.g., in
roadways and parking lots.

The use of well centralizers will be considered for wells deeper than 20 ft. When used, they will
be of PVC, PTFE, or stainless steel and attached to the casing at regular intervals by means of
stainless steel fasteners or strapping. Centralizers will not be attached to the well screen or to
that part of the well casing exposed to the granular filter or bentonite seal. Centralizers will be
oriented to allow for the unrestricted passage of the tremie pipe(s) used for filter pack and grout
placement.

2.3.2 Filter Pack
All granular filters will be approved prior to drilling and will be discussed in the work plans.
Discussions will include composition, source, placement, and gradation. If the actual gradation is
to be determined during drilling, then more than one filter pack gradation will be on hand so that
well installation will not be unnecessarily delayed.
Granular filter packs will be visually free of material that would pass through a No. 200 (75-
micrometer (µm)) sieve, inert, siliceous, composed of rounded grains, and of appropriate size for
the well screen and host environment. The filter material will be packaged in bags by the
supplier and therein delivered to the site.

2.3.2 Bentonite Seal
Bentonite is the only material that is allowed for sealing or as drilling mud under normal
circumstances. This includes any form of bentonite (powders, granules, or pellets) intended for
drilling mud, grout, seals, etc. Chips or pellets of an appropriate size depending on the annular
space available will be used to form the well seal. If chips are used, they should be sieved to
remove fine-grained material. Organic additives will not be used in drilling mud. An exception
might be made for some high yield bentonites, to which the manufacturer has added a small
quantity of polymer. The use of any bentonite will be discussed in the work plans. Bentonite will
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 7 of 12
only be used if absolutely necessary to ensure that the borehole will not collapse or to improve
cuttings removal.

2.3.3 Grout
Grout, when used in monitor well construction or borehole/well abandonment, will be composed
of Portland cement, bentonite (0-10% dry bentonite per 94-lb sack of dry cement), and a maximum
6 to 7 gallons of approved water per sack of cement. The amount of water per sack of cement
required for a pumpable mix will vary with the amount of bentonite used. The amount of water
used will be kept to a minimum. Neither additives nor borehole cuttings will be mixed with the
grout. All grout materials will be combined in an aboveground rigid container or mixer, and
mechanically (not manually) blended on-site to produce a thick, lump-free mixture throughout the
mixing vessel. The mixed grout will be recirculated through the grout pump prior to placement.
Grout will be placed using a grout pump and pipe/tremie. The grout pipe will be of rigid
construction for vertical control of pipe placement. Drill rods, rigid PVC, or metal pipes are
suggested stock for tremie pipes. If hoses or flexible plastics must be used, they may have to be
fitted with a length of steel pipe at the downhole end to keep the flexible material from curling and
embedding itself into the borehole wall. This is especially true in cold weather when the coiled
material resists straightening. Grout pipes will have side discharge. The side discharge will help
to maintain the integrity of the underlying material (especially the bentonite seal).
2.4 Water Source
To the extent practical, the use of drilling water will be held to a minimum. When water usage is
deemed necessary, the source of any water used in drilling, grouting, sealing, filter placement,
well installation, well decommissioning/abandonment, equipment washing, etc. will be approved
prior to arrival of the drilling equipment on-site and specified in the work plans. If a suitable
source exists on-site, that source will be used. The drilling subcontractor will have the
responsibility to procure, transport, and store the water required for project needs in a manner to
avoid the chemical contamination or degradation of the water once obtained. The drilling
subcontractor will also be responsible for any heating, thermal insulation, or agitation of the
water to maintain the water as a fluid for its intended uses.
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 8 of 12
2.5 Delivery, storage, and handling of materials
Materials will be delivered to the site and stored in a secure area. Subcontractors are generally
responsible for scheduling delivery and ordering those supplies pertaining to the installation of
wells. An inventory will be kept to track the materials. Perishable materials will be covered with
tarps and secured to prevent water damage. All materials will be handled in a safe manner and
in accordance with health and safety protocols
3. WELL INSTALLATION
3.1 Preparation
Every morning before entering the field, the field team and drilling subcontractor will meet to
discuss the location and construction criteria for the day’s activities. The field geologist will also
ensure that the drilling subcontractor obtains all necessary supplies for the day’s work (e.g.,
bentonite, Portland cement, and screen and riser), and has decontaminated all equipment and
manmade construction materials to be used downhole (e.g., PVC or stainless-steel screen and
riser). All available areal data (e.g., borehole logs) should be reviewed to determine expected
formation depths prior to the day’s drilling.

3.2 Documentation
During any activities pertaining to well construction, abandonment, or development, the field
geologist will note in the GEOLIS logbook the following information:
Length of time required to perform all drill rig activities (e.g., overdrilling, well construction,
abandonment/grouting, development times, and pumping rates).
All well construction/abandonment supplies used (e.g., bentonite, Portland cement, filter sand,
and screen/riser footage).
Any difficulties in well construction, development, or abandonment. This information may be
used to substantiate a change of scope or explain anomalous sampling data.
Exact measurements (using a tape measure) of screen, end cap trap, and riser lengths.
A completed well construction diagram.

TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 9 of 12
4. WELL COMPLETION
4.1 Background
Elements of well protection are intended to protect the monitoring well from physical damage, to
prevent erosion and/or ponding in the immediate vicinity of the monitoring well, and to enhance
the validity of the water samples. The potential for physical damage is lessened by the
installation of padlocked, protective iron/steel casing over the monitor well and iron/steel posts
around the well (when needed for protection). The casing and posts will be new. The protective
casing diameter or minimum dimension will be 2 in. greater than the nominal diameter of the
monitor well, and the nominal length will be 5 ft. The concrete/cement filled posts will be at least
3 in. in diameter and the top modified to preclude the entry of water. Nominal length of the posts
will be 6 ft. Special circumstances necessitating different materials will be addressed in the work
plan. Erosion and/or ponding in the immediate vicinity of the monitoring well may be prevented
by assuring that the ground surface slopes away from the monitor well protective casing by the
installation of a 2-ft by 2-ft coarse gravel blanket around the well. Wells will contain a locking
cover on the protective casing. The cover will be hinged or telescoped, but not threaded. All
locks on these covers should be opened by a single key, if possible.

4.2 Aboveground well completion
Aboveground wells will be completed as follows:
Extend the well casing 2 to 3 feet above ground surface.
Provide an end plug or casing cap for each well. Use a filtered vented cap or drill a small (0.125-
inch) hole into the PVC riser just below the PVC cap or into the PVC cap to allow air circulation
in the well.
Shield the extended well casing with a carbon steel protective casing that is set over the well
casing and cap and extends to a depth of 3 ft bgs.
Grout the annular space between the borehole and the protective casing with cement/bentonite
grout to a depth of 4 ft bgs.

TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 10 of 12
Fill the annular space between the well casing and the protective casing with pure sodium
bentonite slurry to protect the well casing from frost heave.
Construct a 2- by 2-foot by 4-inch coarse gravel blanket at the surface, sloped away from the
protective casing.
Drill a small diameter hole (0.25- to 0.375-inch) in the protective casing (weep hole) near the top
of the cement pad to allow for drainage and mark a survey location on the inner casing (mark
with an indelible marker or cut a small notch in the PVC on the side toward the hinge).
Install a lockable cap or lid on the protective casing.
Mark the well number clearly on the protective casing cap using impact lettering.
Install three 3-inch-diameter, concrete-filled steel guard posts, if directed to do so by the on-site
geologist.
The guard posts will be 6 feet in total length and installed radially from each well head.
Recess the guard posts approximately 2 feet into the ground outside of the cement pad and set
in concrete approximately 3 to 5 feet from the protective casing.
Fill each guard post with concrete.
All wells will be secured as soon as possible after drilling. Corrosion-resistant locks will be used
for both flush and aboveground well assemblies. The locks must have extended shanks.

4.3 Flush-mounted well completion
Groundwater monitoring wells will be completed aboveground at most locations. Where well
stickup is of concern, the well will be completed as a flush mount, level with the ground surface.
Flush-mounted wells will be completed as follows:
Cut the casing 2 to 3 in. bgs and install a protective locking lid consisting of a cast iron valve box
assembly or manhole cover.
Center the lid assembly in a 3-foot-diameter concrete pad sloped away from the valve box.
Provide a cap with a filtered vent for equilibrium and to prevent infiltration of surface water.
Maintain a minimum of 1 foot of clearance between the casing top and the bottom of the valve
box. Clearly mark the well number on the valve box lid and well casing using an impact-labeling
method, and mark a surveying point on the inner casing.
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 11 of 12

5. MAINTENCE
Wells need to be examined periodically (normally during sampling) to determine if they have
been damaged, vandalized, or otherwise compromised, and to check for evidence of
disintegration such as cracked casing, pads, or surface seals, and to check the security of the
well (locked cap).
TETRA TECH, INC.
Standard Operating Procedure
Revision Date: 4/21/2023
Created by: Anthony Camacho
Project name: Recycled Earth
Page 12 of 12

Appendix C
Subsurface Investigation Logs
Date:
0 12:15 100 0‐5'
12:20 100 5'‐10'
0
2.5
TOW
5.0
7.5
10.0
12.5
15.0
17.5
20.0
10' BGS
Soil Logging Sample Location
Sheet 1 of 1
DE
P
T
H
 (f
e
e
t
)
LI
T
H
O
L
O
G
Y
CLASIFICATION AND DESCRIPTION
SA
M
P
L
E

SY
M
B
O
L
TI
M
E

CO
L
L
E
C
T
E
D
PE
R
C
E
N
T

RE
C
O
V
E
R
Y
Monitoring Well/Boring NO.: MW‐1
Remarks: No PID readings above background levels. Sample taken from above capilary fringe.
PI
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(P
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Completed: 5/4/23 12:40
Project: Recycled Earth
Project NO: 117‐9187001‐07
Logged By: Richie Torney
WE
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CO
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N

SC
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A
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I
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WELL MATERIAL 
DESCRIPTION
RE
C
O
V
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Y

IN
T
E
R
V
A
L
RECOVERY
Location: Ogden, Utah
Drilling Contractor: E.T. Technologies
Drilling Method: Direct Push
Groundwater (ft): ~ 3
Hole Started: 5/4/23 12:15
TD @
EXPLORITORY BORING LOG
Laboratory Sample Location
SCH 40 PVC well 
casing.
Bentonite plug
SM
Rust Colored silty sand
TR gravel, 60% sand (50% medium, 50% fine), 40% silt, TR clay
Well sortedSM Backfill
Screen interval
0.01 slot PVC 2" 
diameter screen 
Pre‐Pack #2/16 
sand
Top of filter pack
#2/16 sand
4% organic brown soil, moist,
5% gravel, 30% fine sand, 60% silt, 5% clayML
Light Brown, wet, 
TR gravel, 70% sand(50% medium, 50% fine), 30% silt, TR clay
well sorted.
Date:
0 13:05 20% 0‐5'
TOW
2.5
5.0
7.5
10.0
12.5
15.0
17.5
20.0
7' BGS
Soil Logging Sample Location
Sheet 1 of 1
DE
P
T
H
 (f
e
e
t
)
LI
T
H
O
L
O
G
Y
CLASIFICATION AND DESCRIPTION
SA
M
P
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SY
M
B
O
L
TI
M
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CO
L
L
E
C
T
E
D
PE
R
C
E
N
T

RE
C
O
V
E
R
Y
Monitoring Well/Boring NO.: MW‐2
Remarks: No PID readings above background levels. Sample taken from above capilary fringe. Set 
screen from 2'‐7' BGS to allow 1' of filter pack and 1' of bentonite seal above screen.
PI
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(P
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Completed: 5/4/23 13:50
Project: Recycled Earth
Project NO: 117‐9187001‐07
Logged By: Richie Torney
WE
L
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CO
N
S
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U
C
T
I
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N

SC
H
E
M
A
T
I
C
WELL MATERIAL 
DESCRIPTION
RE
C
O
V
E
R
Y

IN
T
E
R
V
A
L
RECOVERY
Location: Ogden, Utah
Drilling Contractor: E.T. Technologies
Drilling Method: Direct Push
Groundwater (ft): ~ 1
Hole Started: 5/4/23 13:05
SCH 40 PVC casing.
Bentonite plug
TD @
EXPLORITORY BORING LOG
Laboratory Sample Location
light brown, moist,
TR gravel, 50% fine sand, 50% silt, TR claySP
Light brown, wet,
TR gravel, 70% sand (50% medium, 50% fine), 30% silt, TR clay, 
Well sorted
SW
Screen interval
0.01 slot PVC 2" 
diameter screen 
Pre‐Pack #2/16 
sand
Top of filter pack
#2/16 sand
Date:
0 9:35 100% 0‐5'
9:40 100% 5'‐10'
0
2.5
0
0
5.0 TOW
7.5
10.0
12.5
15.0
17.5
20.0
10' BGS
Soil Logging Sample Location
Sheet 1 of 1
DE
P
T
H
 (f
e
e
t
)
LI
T
H
O
L
O
G
Y
CLASIFICATION AND DESCRIPTION
SA
M
P
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SY
M
B
O
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TI
M
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CO
L
L
E
C
T
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D
PE
R
C
E
N
T

RE
C
O
V
E
R
Y
Monitoring Well/Boring NO.: MW‐3
Remarks: No PID readings above background levels. Sample taken from above capilary fringe. 
PI
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(P
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Completed: 5/4/23 9:55
Project: Recycled Earth
Project NO: 117‐9187001‐07
Logged By: Richie Torney
WE
L
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CO
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N

SC
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I
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WELL MATERIAL 
DESCRIPTION
RE
C
O
V
E
R
Y

IN
T
E
R
V
A
L
RECOVERY
Location: Ogden, Utah
Drilling Contractor: E.T. Technologies
Drilling Method: Direct Push
Groundwater (ft): ~ 5
Hole Started: 5/4/23 9:30
TD @
EXPLORITORY BORING LOG
Laboratory Sample Location
SM
ML
SM
Surface Gravel and Sand interbeded
20% gravel, 60% sand, 20% silt, 0% clay
Silt layer
0% gravel, 30% fine sand, 60% silt, 10% clay
capilary fringe area, light brown, moist,
TR gravel, 60% fine sand, 40% silt, TR clay Top of filter pack
#2/16 sand
Screen interval
0.01 slot PVC 2" 
diameter screen 
Pre‐Pack #2/16 
sand
SCH 40 PVC well 
casing.
Bentonite plug
light brown, wet,
TR gravel, 60% fine sand, 40% silt, TR claySM
SM Transition to dark greenish brown wet soil,
TR gravel, 60% fine sand, 40% silt, TR clay.
Date:
0 11:20 100% 0‐5'
11:25 100% 5'‐10'
0
2.5
0
0
5.0 0
0
TOW
7.5
10.0
12.5
15.0
17.5
20.0
12' BGS
Soil Logging Sample Location
Sheet 1 of 1
DE
P
T
H
 (f
e
e
t
)
LI
T
H
O
L
O
G
Y
CLASIFICATION AND DESCRIPTION
SA
M
P
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SY
M
B
O
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TI
M
E

CO
L
L
E
C
T
E
D
PE
R
C
E
N
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RE
C
O
V
E
R
Y
Monitoring Well/Boring NO.: MW‐4
Remarks: No PID readings above background levels. Sample taken from above capilary fringe. 
PI
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(P
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Completed: 5/4/23 11:45
Project: Recycled Earth
Project NO: 117‐9187001‐07
Logged By: Richie Torney
WE
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CO
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N

SC
H
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A
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I
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WELL MATERIAL 
DESCRIPTION
RE
C
O
V
E
R
Y

IN
T
E
R
V
A
L
RECOVERY
Location: Ogden, Utah
Drilling Contractor: E.T. Technologies
Drilling Method: Direct Push
Groundwater (ft): ~ 7
Hole Started: 5/4/23 11:20
TD @
EXPLORITORY BORING LOG
Laboratory Sample Location
Top of filter pack
#2/16 sand
gravel/sand fill dry
Screen interval
0.01 slot PVC 2" 
diameter screen 
Pre‐Pack #2/16 
sand
SCH 40 PVC well 
casing.
Bentonite plug
ML Organic dark brown soil, ~6% organics, moist,
TR gravel, 30% fine sand, 65% silt, 5% clay
SM Light brown, moist, 0% organic, capilary fringe area,
TR gravel, 50% sand(80% fine, 20% medium), 40% silt, 10% clay.
SM
Light brown, wet, saturated,
TR gravel, 60% sand(50% fine, 50% medium), 40% silt, TR clay.
Bottomed by dark organic layer.
Date:
0 13:55 100% 0‐5'
14:00 100% 5'‐10'
0
2.5
0
5. 0 TOW 0
7.5
10.0
12.5
15.0
17.5
20.0
10' BGS
Soil Logging Sample Location
Sheet 1 of 1
DE
P
T
H
 (f
e
e
t
)
LI
T
H
O
L
O
G
Y
CLASIFICATION AND DESCRIPTION
SA
M
P
L
E

SY
M
B
O
L
TI
M
E

CO
L
L
E
C
T
E
D
PE
R
C
E
N
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RE
C
O
V
E
R
Y
Monitoring Well/Boring NO.: MW‐5
Remarks: No PID readings above background levels. Sample taken from above capilary fringe. 
PI
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(P
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Completed: 5/4/23 14:30
Project: Recycled Earth
Project NO: 117‐9187001‐07
Logged By: Richie Torney
WE
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CO
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U
C
T
I
O
N

SC
H
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A
T
I
C
WELL MATERIAL 
DESCRIPTION
RE
C
O
V
E
R
Y

IN
T
E
R
V
A
L
RECOVERY
Location: Ogden, Utah
Drilling Contractor: E.T. Technologies
Drilling Method: Direct Push
Groundwater (ft): ~ 5
Hole Started: 5/4/23 13:55
TD @
EXPLORITORY BORING LOG
Laboratory Sample Location
SCH 40 PVC well 
casing.
Bentonite plug
Brown, moist,
TR gravel, 20% sand, 70%silt, 10% clay
10% organics
looks like landscaping fill
ML
light brown, wet,
TR gravel, 70% sand(50% medium, 50% fine ), 30% silt, TR claySM
Top of filter pack
#2/16 sand
Screen interval
0.01 slot PVC 2" 
diameter screen 
Pre‐Pack #2/16 
sand
Date:
10:40 100% 0‐5'
1 10:45 100% 5'‐10'
2.5 1.2
0.3
5.0
0.8
TOW
7.5
10.0
12.5
15.0
17.5
20.0
12' BGS
Soil Logging Sample Location Laboratory Sample Location
RECOVERY
Sheet 1 of 1
DE
P
T
H
 (f
e
e
t
)
LI
T
H
O
L
O
G
Y
CLASIFICATION AND DESCRIPTION
SA
M
P
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SY
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O
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TI
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CO
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C
T
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D
PE
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E
N
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RE
C
O
V
E
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Monitoring Well/Boring NO.: MW‐6
Remarks: Soil sample taken at the highest PID reading.
PI
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EXPLORITORY BORING LOG
Location: Ogden, Utah
Drilling Contractor: E.T. Technologies
Drilling Method: Direct Push
Groundwater (ft): ~ 7
Hole Started: 5/4/23 10:35
Completed: 5/4/23 11:00
Project: Recycled Earth
Project NO: 117‐9187001‐07
Logged By: Richie Torney
WE
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CO
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N

SC
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WELL MATERIAL 
DESCRIPTION
RE
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IN
T
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A
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Top of filter pack
#2/16 sand
TD @
Screen interval
0.01 slot PVC 2" 
diameter screen 
Pre‐Pack #2/16 
sand
SCH 40 PVC well 
casing.
Bentonite plug
SM brownish white, wet,
TR gravel, 70% sand(50% medium, 50% fine), 30% silt, TR clay
ML light brown, moist,
0% gravel, 40% sand, 50% silt, 10% clay
dark brown, moist,
15% gravel, 50% sand, 30% silt, 5% claySM
SM light brown, dry,
20% gravel, 50% sand, 30%silt, TR clay
SM brown, dry,
5% gravel, 50% sand, 40%silt, 5% clay
Measuring Point, MP (ft AGS) =TOC
Developer: R. Torney
Turbidimeter
Begin End Gal.
Casing
Volumes
14:16 14:16 8.21 0 -----
14:24 14:24 8.21 0.5 0.5952 12.5 7.75 153
14:27 14:27 8.21 1 1.1905 12.2 7.75 151.6
14:30 14:30 8.21 1.5 1.7857 12.7 7.76 150.2
AGS = Above Ground Surface dw = Inner Diameter of Well ORP = Oxidation/Reduction Potential TD = Well Total Depth
BGS = Below Ground Surface dh = Nominal Diameter of Borehole pH = measure of hydrogen ion concentration TOS = Top of Screen
BMP = Below Measuring Point Gal = Gallon uS/cm = Micro Siemens per Centimeter DO = Dissolved Oxygen
BOS = Bottom of Screen MP = Measuring Point NTU = Nephelometric Turbidity Units
WELL DEVELOPMENT COMPLETE WHEN A MINIMUM OF 3 CASING VOLUMES HAVE BEEN REMOVED AND 3 CONSECUTIVE READINGS OVER ONE CASING VOLUME
ARE WITHIN: ± 0.1 for pH; ± 10% for Cond and Temp ± 10% or <10 NTU Turbidity
Pump 0.5 568
Pump 0.5 575 pumped well dry
pH ORP
Surge 0
Surged well for 3 mins and began
pumping
Pump 0.5 560
Development Log Cumulative
Removed
Water Quality Parameters Other Parameters
(ORP, DO...) / Remarks (Flow Cell
… )Time Develop
Depth
(ft bgs)
Method
(surge, swab,
pump, bail, jet…)
Water
Removed
(gal.)
Temp
(°C)
Spec.
Conduct.
(uS/cm)
Water Quality YSI PRO PLUS 18M102255
Same as Water Quality Meter -
Other:
Equipment
Model Serial Number
Material: polyethelene Tubing metal/rubber
Dimension:1.5"
Pump Bailer Swabbing Where C = 0.163 (2-inch) or
C = 0.653 (4-inch)Type:Parastaltic plugged bailer
Contractor: Total Depth of Well, TD (ft BGS) =8.21
Casing Volume, V C, (gal) =
V C = [(TD+MP) - DTW ] * C=Development Methods (Describe):0.84
Borehole Diameter, d h (in) =4
Total Development
Time (Hours):0.5
Total Cumulative
Volume Removed:1.5
Depth to Top of Screen, TOS (ft BGS) =2.91
Depth to Bot of Screen, BOS (ft BGS) =7.91
Initial Depth to Water (ft BMP):2.94 Time:14:16 Date Installed =5/4/2023
Final Total Depth
of Well (feet bTOC):8.21
Final Turbidity
Achieved (NTU):NA
Well Inner Diameter, d w (in) =2
Date:05/08/23 Task Manager: D. Wilson Recorded by:R. Torney Well Construction Details:
WELL DEVELOPMENT LOG
Page _1__ of _1__
Ogden, Utah Project
Task Name:Recycled Earth Task 07 Task No.:117-9187001-07
Well ID: MW-1
Measuring Point, MP (ft AGS) =TOC
Developer: R. Torney
Turbidimeter
Begin End Gal.
Casing
Volumes
13:49 13:49 7.45 0 -----
13:56 13:56 7.45 0.5 0.4683 11 7.38 154.6
13:59 13:59 7.45 1 0.9366 11 7.33 153.7
14:02 14:02 7.45 1.5 1.405 10.5 7.35 150.2
14:05 14:05 7.45 2 1.8733 10.6 7.34 150.1
AGS = Above Ground Surface dw = Inner Diameter of Well ORP = Oxidation/Reduction Potential TD = Well Total Depth
BGS = Below Ground Surface dh = Nominal Diameter of Borehole pH = measure of hydrogen ion concentration TOS = Top of Screen
BMP = Below Measuring Point Gal = Gallon uS/cm = Micro Siemens per Centimeter DO = Dissolved Oxygen
BOS = Bottom of Screen MP = Measuring Point NTU = Nephelometric Turbidity Units
WELL DEVELOPMENT COMPLETE WHEN A MINIMUM OF 3 CASING VOLUMES HAVE BEEN REMOVED AND 3 CONSECUTIVE READINGS OVER ONE CASING VOLUME
ARE WITHIN: ± 0.1 for pH; ± 10% for Cond and Temp ± 10% or <10 NTU Turbidity
Pump 0.5 962 pumped well dry
Pump 0.5 931
Pump 0.5 958
pH ORP
Surge 0
Surged well for 3 mins and began
pumping
Pump 0.5 892
Development Log Cumulative
Removed
Water Quality Parameters Other Parameters
(ORP, DO...) / Remarks (Flow Cell
… )Time Develop
Depth
(ft bgs)
Method
(surge, swab,
pump, bail, jet…)
Water
Removed
(gal.)
Temp
(°C)
Spec.
Conduct.
(uS/cm)
Water Quality YSI PRO PLUS 18M102255
Same as Water Quality Meter -
Other:
Equipment
Model Serial Number
Material: polyethelene Tubing metal/rubber
Dimension:1.5"
Pump Bailer Swabbing Where C = 0.163 (2-inch) or
C = 0.653 (4-inch)Type:Parastaltic plugged bailer
Contractor: Total Depth of Well, TD (ft BGS) =7.45
Casing Volume, V C, (gal) =
V C = [(TD+MP) - DTW ] * C=Development Methods (Describe):1.07
Borehole Diameter, d h (in) =4
Total Development
Time (Hours):0.5
Total Cumulative
Volume Removed:2 gallons
Depth to Top of Screen, TOS (ft BGS) =2.15
Depth to Bot of Screen, BOS (ft BGS) =7.15
Initial Depth to Water (ft BMP):0.9 Time:13:49 Date Installed =5/4/2023
Final Total Depth
of Well (feet bTOC):7.45
Final Turbidity
Achieved (NTU):NA
Well Inner Diameter, d w (in) =2
Date:05/08/23 Task Manager: D. Wilson Recorded by:R. Torney Well Construction Details:
WELL DEVELOPMENT LOG
Page _1__ of _1__
Ogden, Utah Project
Task Name:Recycled Earth Task 07 Task No.:117-9187001-07
Well ID: MW-2
Measuring Point, MP (ft AGS) =TOC
Developer: R. Torney
Turbidimeter
Begin End Gal.
Casing
Volumes
12:44 12:44 10.3 0.5 0.2978 -----
12:49 12:49 10.3 1 0.5956 10.5 7.26 75.4
12:52 12:52 10.3 1.5 0.8934 10.3 7.29 37.9
12:55 12:55 10.3 2 1.1913 10.1 7.3 28.7
12:58 12:58 10.3 2.75 1.638 9.9 7.26 23.1
13:01 13:01 10.3 3.5 2.0847 9.9 7.3 13.5
13:04 13:04 10.3 4.25 2.5314 9.9 7.3 11.7
13:07 13:07 10.3 5 2.9781 10.4 7.32 13.5
AGS = Above Ground Surface dw = Inner Diameter of Well ORP = Oxidation/Reduction Potential TD = Well Total Depth
BGS = Below Ground Surface dh = Nominal Diameter of Borehole pH = measure of hydrogen ion concentration TOS = Top of Screen
BMP = Below Measuring Point Gal = Gallon uS/cm = Micro Siemens per Centimeter DO = Dissolved Oxygen
BOS = Bottom of Screen MP = Measuring Point NTU = Nephelometric Turbidity Units
WELL DEVELOPMENT COMPLETE WHEN A MINIMUM OF 3 CASING VOLUMES HAVE BEEN REMOVED AND 3 CONSECUTIVE READINGS OVER ONE CASING VOLUME
ARE WITHIN: ± 0.1 for pH; ± 10% for Cond and Temp ± 10% or <10 NTU Turbidity
Pump 0.75 1281
Pump 0.75 1313 pumped well dry
Pump 0.75 1379
Pump 0.75 1325
Pump 0.5 1427
Pump 0.5 1413
pH ORP
Surge 0.5
Surged well for 3 mins and began
pumping
Pump 0.5 1491
Development Log Cumulative
Removed
Water Quality Parameters Other Parameters
(ORP, DO...) / Remarks (Flow Cell
… )Time Develop
Depth
(ft bgs)
Method
(surge, swab,
pump, bail, jet…)
Water
Removed
(gal.)
Temp
(°C)
Spec.
Conduct.
(uS/cm)
Water Quality YSI PRO PLUS 18M102255
Same as Water Quality Meter -
Other:
Equipment
Model Serial Number
Material: polyethelene Tubing metal/rubber
Dimension:1.5"
Pump Bailer Swabbing Where C = 0.163 (2-inch) or
C = 0.653 (4-inch)Type:Parastaltic plugged bailer
Contractor: Total Depth of Well, TD (ft BGS) =10.3
Casing Volume, V C, (gal) =
V C = [(TD+MP) - DTW ] * C=Development Methods (Describe):1.68
Borehole Diameter, d h (in) =4
Total Development
Time (Hours):0.5
Total Cumulative
Volume Removed:5 gallons
Depth to Top of Screen, TOS (ft BGS) =5
Depth to Bot of Screen, BOS (ft BGS) =10
Initial Depth to Water (ft BMP):0 Time:12:44 Date Installed =5/4/2023
Final Total Depth
of Well (feet bTOC):10.3
Final Turbidity
Achieved (NTU):NA
Well Inner Diameter, d w (in) =2
Date:05/08/23 Task Manager: D. Wilson Recorded by:R. Torney Well Construction Details:
WELL DEVELOPMENT LOG
Page _1__ of _1__
Ogden, Utah Project
Task Name:Recycled Earth Task 07 Task No.:117-9187001-07
Well ID: MW-3
Measuring Point, MP (ft AGS) =TOC
Developer: R. Torney
Turbidimeter
Begin End Gal.
Casing
Volumes
13:16 13:16 11.81 0 0-----
13:24 13:24 11.81 0.25 0.2289 11.4 7.39 84
13:27 13:27 11.81 1 0.9157 10.4 7.37 36.3
13:30 13:30 11.81 1.5 1.3735 10.1 7.31 7.5
13:33 13:33 11.81 2.25 2.0603 9.9 7.22 -4.9
13:36 13:36 11.81 3 2.747 10 7.24 10.2
AGS = Above Ground Surface dw = Inner Diameter of Well ORP = Oxidation/Reduction Potential TD = Well Total Depth
BGS = Below Ground Surface dh = Nominal Diameter of Borehole pH = measure of hydrogen ion concentration TOS = Top of Screen
BMP = Below Measuring Point Gal = Gallon uS/cm = Micro Siemens per Centimeter DO = Dissolved Oxygen
BOS = Bottom of Screen MP = Measuring Point NTU = Nephelometric Turbidity Units
WELL DEVELOPMENT COMPLETE WHEN A MINIMUM OF 3 CASING VOLUMES HAVE BEEN REMOVED AND 3 CONSECUTIVE READINGS OVER ONE CASING VOLUME
ARE WITHIN: ± 0.1 for pH; ± 10% for Cond and Temp ± 10% or <10 NTU Turbidity
Pump 0.75 1839
Pump 0.75 1853 pumped well dry
Pump 0.75 1832
Pump 0.5 1827
pH ORP
Surge 0.25
Surged well for 3 mins and began
pumping
Pump 0.25 1832
Development Log Cumulative
Removed
Water Quality Parameters Other Parameters
(ORP, DO...) / Remarks (Flow Cell
… )Time Develop
Depth
(ft bgs)
Method
(surge, swab,
pump, bail, jet…)
Water
Removed
(gal.)
Temp
(°C)
Spec.
Conduct.
(uS/cm)
Water Quality YSI PRO PLUS 18M102255
Same as Water Quality Meter -
Other:
Equipment
Model Serial Number
Material: polyethelene Tubing metal/rubber
Dimension:1.5"
Pump Bailer Swabbing Where C = 0.163 (2-inch) or
C = 0.653 (4-inch)Type:Parastaltic plugged bailer
Contractor: Total Depth of Well, TD (ft BGS) =11.81
Casing Volume, V C, (gal) =
V C = [(TD+MP) - DTW ] * C=Development Methods (Describe):1.09
Borehole Diameter, d h (in) =4
Total Development
Time (Hours):0.5
Total Cumulative
Volume Removed:3 gallons
Depth to Top of Screen, TOS (ft BGS) =6.51
Depth to Bot of Screen, BOS (ft BGS) =11.51
Initial Depth to Water (ft BMP):5.11 Time:13:16 Date Installed =5/4/2023
Final Total Depth
of Well (feet bTOC):11.81
Final Turbidity
Achieved (NTU):NA
Well Inner Diameter, d w (in) =2
Date:05/08/23 Task Manager: D. Wilson Recorded by:R. Torney Well Construction Details:
WELL DEVELOPMENT LOG
Page _1__ of _1__
Ogden, Utah Project
Task Name:Recycled Earth Task 07 Task No.:117-9187001-07
Well ID: MW-4
Measuring Point, MP (ft AGS) =TOC
Developer: R. Torney
Turbidimeter
Begin End Gal.
Casing
Volumes
14:51 14:51 10.1 0 0-----
14:57 14:57 10.1 0.5 0.4606 9.8 7.86 117
15:00 15:00 10.1 0.75 0.6909 9.6 7.87 99.2
15:03 15:03 10.1 1.5 1.3817 9.3 7.89 93.8
15:06 15:06 10.1 2 1.8423 8.9 7.84 93.3
15:09 15:09 10.1 2.5 2.3029 8.8 7.9 98.7
15:12 15:12 10.1 3.25 2.9938 8.8 7.91 98
AGS = Above Ground Surface dw = Inner Diameter of Well ORP = Oxidation/Reduction Potential TD = Well Total Depth
BGS = Below Ground Surface dh = Nominal Diameter of Borehole pH = measure of hydrogen ion concentration TOS = Top of Screen
BMP = Below Measuring Point Gal = Gallon uS/cm = Micro Siemens per Centimeter DO = Dissolved Oxygen
BOS = Bottom of Screen MP = Measuring Point NTU = Nephelometric Turbidity Units
WELL DEVELOPMENT COMPLETE WHEN A MINIMUM OF 3 CASING VOLUMES HAVE BEEN REMOVED AND 3 CONSECUTIVE READINGS OVER ONE CASING VOLUME
ARE WITHIN: ± 0.1 for pH; ± 10% for Cond and Temp ± 10% or <10 NTU Turbidity
Pump 0.75 1242 pumped well dry
Pump 0.5 1248
Pump 0.5 1241
Pump 0.25 1252
Pump 0.75 1248
pH ORP
Surge 0.25
Surged well for 3 mins and began
pumping
Pump 0.5 1239
Development Log Cumulative
Removed
Water Quality Parameters Other Parameters
(ORP, DO...) / Remarks (Flow Cell
… )Time Develop
Depth
(ft bgs)
Method
(surge, swab,
pump, bail, jet…)
Water
Removed
(gal.)
Temp
(°C)
Spec.
Conduct.
(uS/cm)
Water Quality YSI PRO PLUS 18M102255
Same as Water Quality Meter -
Other:
Equipment
Model Serial Number
Material: polyethelene Tubing metal/rubber
Dimension:1.5"
Pump Bailer Swabbing Where C = 0.163 (2-inch) or
C = 0.653 (4-inch)Type:Parastaltic plugged bailer
Contractor: Total Depth of Well, TD (ft BGS) =10.1
Casing Volume, V C, (gal) =
V C = [(TD+MP) - DTW ] * C=Development Methods (Describe):1.09
Borehole Diameter, d h (in) =4
Total Development
Time (Hours):0.5
Total Cumulative
Volume Removed:3.25 gallons
Depth to Top of Screen, TOS (ft BGS) =4.8
Depth to Bot of Screen, BOS (ft BGS) =9.8
Initial Depth to Water (ft BMP):3.44 Time:14.51 Date Installed =5/4/2023
Final Total Depth
of Well (feet bTOC):10.1
Final Turbidity
Achieved (NTU):NA
Well Inner Diameter, d w (in) =2
Date:05/08/23 Task Manager: D. Wilson Recorded by:R. Torney Well Construction Details:
WELL DEVELOPMENT LOG
Page _1__ of _1__
Ogden, Utah Project
Task Name:Recycled Earth Task 07 Task No.:117-9187001-07
Well ID: MW-5
Measuring Point, MP (ft AGS) =TOC
Developer: R. Torney
Turbidimeter
Begin End Gal.
Casing
Volumes
11:36 11:36 12.11 0.25 0.2286 -----
11:50 11:50 12.11 0.75 0.6857 11 8.28 150.7
11:53 11:53 12.11 1.25 1.1429 11 7.67 143.9
11:56 11:56 12.11 1.75 1.6 10.9 7.53 121.7
11:59 11:59 12.11 2.25 2.0572 11.4 7.44 93.9
AGS = Above Ground Surface dw = Inner Diameter of Well ORP = Oxidation/Reduction Potential TD = Well Total Depth
BGS = Below Ground Surface dh = Nominal Diameter of Borehole pH = measure of hydrogen ion concentration TOS = Top of Screen
BMP = Below Measuring Point Gal = Gallon uS/cm = Micro Siemens per Centimeter DO = Dissolved Oxygen
BOS = Bottom of Screen MP = Measuring Point NTU = Nephelometric Turbidity Units
WELL DEVELOPMENT LOG
Page _1__ of _1__
Ogden, Utah Project
Task Name:Recycled Earth Task 07 Task No.:117-9187001-07
Well ID: MW-6
Initial Depth to Water (ft BMP):5.4 Time:11:36 Date Installed =5/4/2023
Final Total Depth
of Well (feet bTOC):12.11
Final Turbidity
Achieved (NTU):NA
Well Inner Diameter, d w (in) =2
Date:05/08/23 Task Manager: D. Wilson Recorded by:R. Torney Well Construction Details:
Borehole Diameter, d h (in) =4
Total Development
Time (Hours):0.5
Total Cumulative
Volume Removed:2.25 gallons
Depth to Top of Screen, TOS (ft BGS) =6.81
Depth to Bot of Screen, BOS (ft BGS) =11.81
Where C = 0.163 (2-inch) or
C = 0.653 (4-inch)Type: Parastaltic plugged bailer
Contractor: Total Depth of Well, TD (ft BGS) =12.11
Casing Volume, V C, (gal) =
V C = [(TD+MP) - DTW ] * C=Development Methods (Describe):1.09
Material: polyethelene Tubing metal/rubber
Dimension:1.5"
Pump Bailer Swabbing
Water Quality YSI PRO PLUS 18M102255
Same as Water Quality Meter -
Other:
Equipment
Model Serial Number
Development Log Cumulative
Removed
Water Quality Parameters Other Parameters
(ORP, DO...) / Remarks (Flow Cell
… )Time Develop
Depth
(ft bgs)
Method
(surge, swab,
pump, bail, jet…)
Water
Removed
(gal.)
Temp
(°C)
Spec.
Conduct.
(uS/cm)
Pump 0.5 1262
Pump 0.5 1193
pH ORP
Surge 0.25
Surged well for 4 mins and began
pumping
Pump 0.5 1272
Pump 0.5 1226 pumped well dry
WELL DEVELOPMENT COMPLETE WHEN A MINIMUM OF 3 CASING VOLUMES HAVE BEEN REMOVED AND 3 CONSECUTIVE READINGS OVER ONE CASING VOLUME
ARE WITHIN: ± 0.1 for pH; ± 10% for Cond and Temp ± 10% or <10 NTU Turbidity
GROUNDWATER SAMPLING DATA SHEET
TETRA TECH, INC.
Time
Volume 
(gallons)Temp (C) pH SC DO ORP
13:36 ‐16 7.43 633 3 176.7
13:39 0.25 13.7 7.56 572 1.81 193
13:42 0.5 13.7 7.56 570 1.58 198.6
13:45 0.75 14.3 7.62 599 1.48 201
13:48 1 14.3 7.65 618 1.4 199
Bottle Size (mL)
Project:  Recycled Earth Boring/Well Number: MW‐1
Project Info
Date: 05‐11‐23 Sample Time: 13:48 pm
Project Location:  Recycled Earth, Ogden, UT 84657 Sample Type: GW Grab
Sample ID: MW‐1Project Number:  117‐9187001‐07
WL ‐ Depth to Water (ft): 2.99 Type of Well: Surface Completion
Field Measurements
Personnel:  Richie Torney Site Conditions: clear
Weather: clear, 75 FTime: 13:31 am
Sampling Information
Max Purge Volume (TD‐WL)/25 x (CD)2 x 3: 2.5 gallons Recovery: 1.5
CD ‐ Casing Diameter (in): 2Sample Method: Parastaltic Pump
TD ‐ Total Well Depth (ft): 8.21 Purge Method: Parastaltic Pump
Parameters Preservative Sample Time
Remarks/Notes: 
See COC for sample parameters
Visual Observations:
none.
GROUNDWATER SAMPLING DATA SHEET
TETRA TECH, INC.
Time
Volume 
(gallons)Temp (C) pH SC DO ORP
12:46 ‐13.1 7.28 1014 1.8 197.73
12:49 0.5 12.4 7.32 912 0.51 200.3
12:52 1 12.8 7.29 951 0.46 200.2
12:55 1.25 12.8 7.29 947 0.46 199.6
Bottle Size (mL)
Project:  Recycled Earth Boring/Well Number: MW‐2
Project Info
Date: 05‐11‐23 Sample Time: 12:56 pm
Project Location:  Recycled Earth, Ogden, UT 84657 Sample Type: GW Grab
Sample ID: MW‐2Project Number:  117‐9187001‐07
WL ‐ Depth to Water (ft): 0.7 Type of Well: Surface Completion
Field Measurements
Personnel:  Richie Torney Site Conditions: clear
Weather: Sunny, 75 FTime: 12:42 pm
Sampling Information
Max Purge Volume (TD‐WL)/25 x (CD)2 x 3: 3.235 gallons Recovery: 1.5
CD ‐ Casing Diameter (in): 2Sample Method: Parastaltic Pump
TD ‐ Total Well Depth (ft): 7.44 Purge Method: Parastaltic Pump
Parameters Preservative Sample Time
Remarks/Notes: 
See COC for sample parameters
Visual Observations:
none.
GROUNDWATER SAMPLING DATA SHEET
TETRA TECH, INC.
Time
Volume 
(gallons)Temp (C) pH SC DO ORP
11:15 0.25 12.2 7.26 1537 0.64 98.4
11:18 0.5 12.4 7.25 1535 0.57 102.3
11:21 1 12.3 7.25 1520 0.51 100.9
Bottle Size (mL)
Project:  Recycled Earth Boring/Well Number: MW‐3
Project Info
Date: 05‐11‐23 Sample Time: 11:21 am
Project Location:  Recycled Earth, Ogden, UT 84657 Sample Type: GW Grab
Sample ID: MW‐3Project Number:  117‐9187001‐07
WL ‐ Depth to Water (ft): 0Type of Well: Surface Completion
Field Measurements
Personnel:  Richie Torney Site Conditions: clear
Weather: Sunny, 75 FTime: 12:15 am
Sampling Information
Max Purge Volume (TD‐WL)/25 x (CD)2 x 3: 4.8 gallons Recovery: 1.5
CD ‐ Casing Diameter (in): 2Sample Method: Parastaltic Pump
TD ‐ Total Well Depth (ft): 10.3 Purge Method: Parastaltic Pump
Parameters Preservative Sample Time
Remarks/Notes: 
See COC for sample parameters
Visual Observations:
none.
GROUNDWATER SAMPLING DATA SHEET
TETRA TECH, INC.
Time
Volume 
(gallons)Temp (C) pH SC DO ORP
11:54 ‐12.7 7.23 1948 1.65 105.8
11:57 0.3 11.4 7.29 1886 0.7 74.5
12:00 0.5 11.7 7.28 1911 0.59 40
12:03 0.75 11.6 7.27 1909 0.58 7.1
12:06 0.9 11.5 7.26 1925 0.56 ‐3.7
12:09 1.15 11.3 7.24 1950 0.54 ‐12.7
Bottle Size (mL)
Project:  Recycled Earth Boring/Well Number: MW‐4
Project Info
Date: 05‐11‐23 Sample Time: 12:10 pm
Project Location:  Recycled Earth, Ogden, UT 84657 Sample Type: GW Grab
Sample ID: MW‐4Project Number:  117‐9187001‐07
WL ‐ Depth to Water (ft): 5.28 Type of Well: Surface Completion
Field Measurements
Personnel:  Richie Torney Site Conditions: clear
Weather: Sunny, 75 FTime: 11:50 am
Sampling Information
Max Purge Volume (TD‐WL)/25 x (CD)2 x 3: 3.139 gallons Recovery: 1.5
CD ‐ Casing Diameter (in): 2Sample Method: Parastaltic Pump
TD ‐ Total Well Depth (ft): 11.82 Purge Method: Parastaltic Pump
Parameters Preservative Sample Time
Remarks/Notes: 
See COC for sample parameters
Visual Observations:
none.
GROUNDWATER SAMPLING DATA SHEET
TETRA TECH, INC.
Time
Volume 
(gallons)Temp (C) pH SC DO ORP
14:32 ‐12.1 7.37 1331 2.05 165.9
14:35 0.25 10.6 7.47 1302 0.93 169.1
14:38 0.5 10.7 7.61 1311 0.74 170.1
14:41 0.75 11.2 7.7 1326 0.62 173.5
14:44 1.1 10.9 7.74 1318 0.56 170.2
14:47 1.4 11 7.77 1322 0.54 166.9
14:50 1.75 10.8 7.78 1315 0.49 168.2
Bottle Size (mL)
Project:  Recycled Earth Boring/Well Number: MW‐5
Project Info
Date: 05‐11‐23 Sample Time: 14:50
Project Location:  Recycled Earth, Ogden, UT 84657 Sample Type: GW Grab
Sample ID: MW‐5Project Number:  117‐9187001‐07
WL ‐ Depth to Water (ft): 4.51 Type of Well: Surface Completion
Field Measurements
Personnel:  Richie Torney Site Conditions: clear
Weather: Sunny, 75 FTime: 14:28
Sampling Information
Max Purge Volume (TD‐WL)/25 x (CD)2 x 3: 2.69 gallons Recovery: 2
CD ‐ Casing Diameter (in): 2Sample Method: Parastaltic Pump
TD ‐ Total Well Depth (ft): 10.11 Purge Method: Parastaltic Pump
Parameters Preservative Sample Time
Remarks/Notes: 
See COC for sample parameters
Visual Observations:
none.
GROUNDWATER SAMPLING DATA SHEET
TETRA TECH, INC.
Time
Volume 
(gallons)Temp (C) pH SC DO ORP
10:30 0.5 10.9 7.27 1296 1.28 185.1
10:33 0.75 11.2 7.32 1299 0.99 173.5
10:36 0.85 11.3 7.31 1304 0.87 170.1
10:39 1 11.3 7.28 1300 0.8 168.6
Bottle Size (mL)
Project:  Recycled Earth Boring/Well Number: MW‐6
Project Info
Date: 05‐11‐23 Sample Time: 10:40
Project Location:  Recycled Earth, Ogden, UT 84657 Sample Type: GW Grab
Sample ID: MW‐6Project Number:  117‐9187001‐07
WL ‐ Depth to Water (ft): 4.64 Type of Well: Surface Completion
Field Measurements
Personnel:  Richie Torney Site Conditions: clear
Weather: Sunny, 75 FTime: 10:06
Sampling Information
Max Purge Volume (TD‐WL)/25 x (CD)2 x 3: 3.59 gallons Recovery: 1 gallon
CD ‐ Casing Diameter (in): 2Sample Method: Parastaltic Pump
TD ‐ Total Well Depth (ft): 12.11 Purge Method: Parastaltic Pump
Parameters Preservative Sample Time
Remarks/Notes: See COC for sample parameters
Visual Observations:
none.

Appendix D
Daily Field Logs
Weather Conditions: 5° F, partially cloudy, dry, snow on ground
FIELD INVESTIGATION DAILY LOG Page _1_ of _1_
Ogden, Utah
Task Name: Recycled Earth Task Manager: A. Rassmuson Date:02/02/2023
Field Personnel: R. Torney Task No:117-9187001-01
Location:Recycled earth south property Reported by: R. Torney
Matters of Safety: Cold, Sliping on Ice, working in cramped spaces, traffic areas.
Problems / Concerns and Corrective Actions Taken: most of the catch basins are cleaned out or frozen. Dificult/no possible to collect sample. Empty catch
basins wer noted and not sampled, frozen samples were chipped out as best as could be done.
Time Activities
8:00
Arrive on site and begin planning the day with the the client. The client wants other samples collected on the
north property as well and begins pumpin the catch basins that are full of water.
8:30 Begin sampling the south side catch basins.
9:00 Began sampling all the soil from CB-3 and there was very little soil in the bottom of the catch basin.
9:15 CB-5 is under water, samped CB-4. there was a black sludge in CB-4 and a Hydrocarbon smell.
9:30
CB-6 was completely cleaned out. The client is helping remove gravel from SS-5 with an excavator so it can be
Sampled.
9:45 SS-5 is sampled.
10:10 Sampled SS-7
10:25 Sampled SS-6. moving on to do north site sampled until CB-1 and 2 are pumped clean.
13:30 Returned to sample CB-1 and 2.
13:45 Sampled CB-1.
14:30 Sampled CB-2. driving to prep and deliver samples.
15:45 Delivered samples to fedex and back to home office to prepare for the next days sampling.
14:30 Sampled SW-4. moving on to SW-5 Location behing Rocky Mountain Power.
15:30 Sampled SW-5 and SS-13. on my way to deliver sampled to fedex.
16:55 Prepared sample coolers with Ice and Delivered Samples to Fedex for Overnight Delivery to Pace Laboratories.
12:45
Sampling was dificult due to frosen ground and iced over water. Sampled SS-11 + DUP-2 and MS/MSD-2.
Sampled SW-3. moving to SW-4.
13:30
SW-4 is in a deep stormwater box that cannot be entered without confined space training. Going to Tractor
Supply to buy a rope for the bailer I have been using for sampling.
14:10
Arrived back on site and began sampling SW-4. SS-12 can not be sampled from this location without confined
spae entry.
10:30
parked as close to the sample site as possible and followed the train tracks to the sample site. The sample site
needed to be moved to a place where the surface water is not being piped underground.
11:20 SS-10 and GW-2 sampled, movign to the next sample site
11:45 Arrived at SS-11 and GW-3. parked on the side of W 2550 S to sample the south side of the road.
8:30 Began sampling SS-8 and SW-1.
9:00 Began sampling SS-9, walked from first sample location
10:00 SS-9 sampled along with DUP-1 and MS/MSD-1. Moving to SW-2 and SS-10
Matters of Safety: Cold, Sliping on Ice, working in cramped spaces, traffic areas.
Problems / Concerns and Corrective Actions Taken: most of the catch basins are cleaned out or frozen. Dificult/no possible to collect sample. Empty catch
basins wer noted and not sampled, frozen samples were chipped out as best as could be done.
Time Activities
8:00
Arrive on site and begin planning the day with the the Ogden City Representative. Ogden City can grant me
access to property that is closer to sample locations.
Weather Conditions: 5° F, partially cloudy, dry, snow on ground
FIELD INVESTIGATION DAILY LOG Page _1_ of _1_
Ogden, Utah
Task Name: Recycled Earth Task Manager: A. Rassmuson Date:02/02/2023
Field Personnel: R. Torney Task No:117-9187001-01
Location:Recycled earth south property Reported by: R. Torney
12:05 cooler packed. on the way to fedex for shipment
11:35 sampled SS-7 from bottem of channel. deconing and samoling SS-6 next.
11:50 sampled SS-6. bottles from pace were slightly damaged. added tape for strength
11:55 Ogden City off site, began labeling and packing cooler.
10:45 removalizing to SS-10
11:00 arrived at SS-10, began sampling.
11:20 samoles labeled and decontated. remobalizing to Ss-6 and SS-7
10:00 Ogden city representative Arrives. both drive to sample location SS-12
10:15 arrive at ss-12
10:30 arrive back at vehicle to label and decon
Matters of Safety:ice, cold, bending twisting and stooping, use of tools.
Problems / Concerns and Corrective Actions Taken:
Time Activities
9:45 TT arrives on site and prepares for the morning
Weather Conditions: snow on ground, 16°F, cloudy, calm.
FIELD INVESTIGATION DAILY LOG Page _1_ of _1_
NERT, Henderson, NV
Task Name: Recycled Earth stormwater compliance Task Manager: A. Rassmuson Date:2/09/23
Field Personnel: R. Torney, Ogden City Task No:
Location: west Ogden Industrial Area Reported by: R. Torney

Appendix E
Photo Log

Recycled Earth Site Characterization

Page 1 of 21 PHOTO LOG

Number: 1 Date: February 2, 2023
Description: View of sample site CB-3.

Number: 2 Date: February 2, 2023
Description: View of sample site CB-4

Recycled Earth Site Characterization

Page 2 of 21 PHOTO LOG

Number: 3 Date: February 2, 2023
Description: View of attempted sample site CB-6.

Number: 4 Date: February 2, 2023
Description: View of sample location SS-5 collected from excavation dug down to native soil.

Recycled Earth Site Characterization

Page 3 of 21 PHOTO LOG

Number: 5 Date: February 2, 2023
Description: Picture of excavator used to scrape SS-5 to native soil.

Number: 6 Date: February 2, 2023
Description: Sample Site SS-7.

Date: February 3, 2023
Recycled Earth Site Characterization

Page 4 of 21 PHOTO LOG

Number: 7 Date: February 3, 2023
Description: View of updated sample site SW-2.

Date: February 3, 2023
Number: 8 Date: February 3, 2023
Description: View of sample site for SW-3 and SS-11.

Recycled Earth Site Characterization

Page 5 of 21 PHOTO LOG

Number: 9 Date: February 3, 2023
Description: Sample Site SW-4 manhole.

Number: 10 Date: February 3, 2023
Description: Sample Site SW-4 inside manhole.

Recycled Earth Site Characterization

Page 6 of 21 PHOTO LOG

Number: 11 Date: February 09, 2023
Description: view of the sample location for SS-10.

Number: 12 Date: February 09, 2023
Description: View of the detention basin along Midland Drive.

Recycled Earth Site Characterization

Page 7 of 21 PHOTO LOG

Number: 13 Date: May 04, 2023
Description: Direct Push drilling for MW-3.

Number: 14 Date: May 4, 2023
Description: View of geologist reviewing cores for borehole MW-1.

Recycled Earth Site Characterization

Page 8 of 21 PHOTO LOG

Number: 15 Date: May 4, 2023
Description: View of Photo Ionization Detector use on soil cores from MW-6

Number: 16 Date: May 17, 2023
Description: View of MW-1 well surface mount.

Recycled Earth Site Characterization

Page 9 of 21 PHOTO LOG

Number: 17 Date: May 17, 2023
Description: View of MW-2 surface mount.

Number: 18 Date: May 17, 2023
Description: View of MW-3 surface mount.

Recycled Earth Site Characterization

Page 10 of 21 PHOTO LOG

Number: 19 Date: May 17, 2023
Description: View of MW-4 surface mount.

Number: 20 Date: May 17, 2023
Description: view of MW-5 surface mount.

Recycled Earth Site Characterization

Page 11 of 21 PHOTO LOG

Number: 21 Date: May 17, 2023
Description: View of MW-6 surface mount.

Number: 22 Date: June 6, 2023
Description: Temporary retention pond constructed in June, 2023.

Recycled Earth Site Characterization

Page 12 of 21 PHOTO LOG

Number: 23 Date: June 6, 2023
Description: View of french drain cutoff.

Number: 24 Date: June 6, 2023
Description: View of CB-8 being pumped out.

Recycled Earth Site Characterization

Page 13 of 21 PHOTO LOG

Number: 25 Date: June 29, 2023
Description: View of the temporary water detention basin.

Number: 26 Date: June 29, 2023
Description: View of the southern portion of the south trench prior to excavation.

Recycled Earth Site Characterization

Page 14 of 21 PHOTO LOG

Number: 27 Date: June 29, 2023
Description: View of the pump used to remove water from the south trench prior to excavation.

Number: 28 Date: June 29, 2023
Description: South trench prior to excavation began.

Recycled Earth Site Characterization

Page 15 of 21 PHOTO LOG

Number: 29 Date: June 29, 2023
Description: View of field PID screening to guide the south trench excavtation.

Number: 30 Date: June 29, 2023
Description: PID screening of south trench excavation to guide excavation.

Recycled Earth Site Characterization

Page 16 of 21 PHOTO LOG

Number: 31 Date: June 29, 2023
Description: PID screening progress in the south trench

Number: 32 Date: June 29, 2023
Description: PID guided excavation progress of south trench.

Recycled Earth Site Characterization

Page 17 of 21 PHOTO LOG

Number: 33 Date: June 29, 2023
Description: Area of south trench with higher PID reading that required extra excation

Number: 34 Date: June 29, 2023
Description: PID excavation progress in south trench.

Recycled Earth Site Characterization

Page 18 of 21 PHOTO LOG

Number: 35 Date: June 29, 2023
Description: Final zone of excavation in south trench.

Number: 36 Date: June 29, 2023
Description: Excavation progress on the north end of the south trench.

Recycled Earth Site Characterization

Page 19 of 21 PHOTO LOG

Number: 37 Date: June 29, 2023
Description: Guiding excavation south trench excavation with PID.

Number: 38 Date: June 29, 2023
Description: Progressing south trench excavation.

Recycled Earth Site Characterization

Page 20 of 21 PHOTO LOG

Number: 39 Date: June 29, 2023
Description: Final PID confirmation readings show 0 PPM of hydrocarbons in south trench excavation.

Number: 40 Date: August 16, 2023
Description: Catch basin cleanout

Recycled Earth Site Characterization

Page 21 of 21 PHOTO LOG

Number: 41 Date: August 16, 2023
Description: Catch basin cleanout

Appendix F
Soil Sampling Logs

Page ___ of ___
NORTHING EASTING
Material Codes: AG=Amber Glass; CG=Clear Glass; PE=polyethylene; WM=wide mouth; O=Other (Specify): __________________________________
Signature(s): _________________________________
Volume Preserv.
Sample Container Specification
Intended Analysis
and/or Method
Remarks: (color, odor, sand & silt content, factors possibly affecting samples; condition of sampling apparatus, etc.)
No.
Material
Code
Sampling Initiated (hrs):Sampling Ended (hrs):COC No.:COC Time:** Sample Type: C = Composite; D = Duplicate; G = Grab; P =
Primary; other ______________________________
SOIL SAMPLING LOG
Sampling Method/ Equipment:Decontamination Method:\
Sample ID Date Time
Location (coordinates or
description)
Soil Description
(USCS Classification, texture, color, biota, debris, sheens, odor, moisture,
vertical changes, etc.)Sample
Type**
Project:
Sample Notes
Field Staff:Weather:Date:
Task:
Intended Analyses
CB-3 2/02/23 SIlty samnd with Gravel, frozen, no odor, light brown Grab Frozen
CB-4 2/02/23 Silty Sand, intersticial Black Sludge, Strong hydrocarbon odor.Grab
SS-5 2/02/23
SS-6
SS-7
CB-1
CB-2
2/02/23
2/02/23
2/02/23
2/02/23
silty sand, no odor, light brown.
silty sand, no odor, dark brown, moist/frozen
silty sand, no odor, dark brown, moist/frozen.
silty sand, hydrocarbon odor, dark brown/black, west
silty sand, hydrocarbon odor, dark brown/black. wet.
Grab
Grab
Grab
Grab
Grab
saturate
saturated
Recycled Earth 117-9187001
2/02/23R. Torney
Shovel and trowel Liqunox wipe and distilled rinse.
black hydrocarbon like sludge
Page ___ of ___
NORTHING EASTING
Material Codes: AG=Amber Glass; CG=Clear Glass; PE=polyethylene; WM=wide mouth; O=Other (Specify): __________________________________
Signature(s): _________________________________
Volume Preserv.
Sample Container Specification
Intended Analysis
and/or Method
Remarks: (color, odor, sand & silt content, factors possibly affecting samples; condition of sampling apparatus, etc.)
No.
Material
Code
Sampling Initiated (hrs):Sampling Ended (hrs):COC No.:COC Time:** Sample Type: C = Composite; D = Duplicate; G = Grab; P =
Primary; other ______________________________
SOIL SAMPLING LOG
Sampling Method/ Equipment:Decontamination Method:\
Sample ID Date Time
Location (coordinates or
description)
Soil Description
(USCS Classification, texture, color, biota, debris, sheens, odor, moisture,
vertical changes, etc.)Sample
Type**
Project:
Sample Notes
Field Staff:Weather:Date:
Task:
Intended Analyses
Ogden Trx Station Env Consult 117-9238001
R. Torney 2/02/23
Trowel and shovel Alconox rinse and wipe.
CBN-1 2/02/23 10:55 Silty Sand, hydrocarbon odor, light brown.Grab
CBN-2 2/02/23 11:05 SIlty Sand, Hydrocarbon Odor, Light Brown Grab
CBN-3 2/02/23 11:25 Sity Sand, Hydrocarbon Smell, Light Brown Grab
CBN-4 2/02/23 11:45 Silty Sand, Hydrocarbon Smell, Light Brown Grab
CBN-5 2/02/23 12:20 Silty Sand, Hydrocarbon SMell, Light Brown Grab
Saturated
saturated
saturated
saturated
saturate, debris from surface
10:30 12:30
Page ___ of ___
NORTHING EASTING
Material Codes: AG=Amber Glass; CG=Clear Glass; PE=polyethylene; WM=wide mouth; O=Other (Specify): __________________________________
Signature(s): _________________________________
Volume Preserv.
Sample Container Specification
Intended Analysis
and/or Method
Remarks: (color, odor, sand & silt content, factors possibly affecting samples; condition of sampling apparatus, etc.)
No.
Material
Code
Sampling Initiated (hrs):Sampling Ended (hrs):COC No.:COC Time:** Sample Type: C = Composite; D = Duplicate; G = Grab; P =
Primary; other ______________________________
SOIL SAMPLING LOG
Sampling Method/ Equipment:Decontamination Method:\
Sample ID Date Time
Location (coordinates or
description)
Soil Description
(USCS Classification, texture, color, biota, debris, sheens, odor, moisture,
vertical changes, etc.)Sample
Type**
Project:
Sample Notes
Field Staff:Weather:Date:
Task:
Intended Analyses
SS-8 2/03/23 SIlty samnd with Gravel, frozen, no odor, light brown Grab
SS-9 2/03/23
Silty Sand, dark brown, no odor, moist/frozen.
SS-10 2/03/23
SS-11
SS-13
2/03/23
2/03/23
silty sand, no odor, light brown, moist/frozen.
silty sand, no odor, dark brown, moist/frozen
silty sand, no odor, dark brown, moist/frozen.
Grab
Grab
Grab
Recycled Earth 117-9187001
2/03/23R. Torney
Shovel and trowel Liqunox wipe and distilled rinse.
Grab
8:00 16:00
Dup-1 2/03/23
2/03/23
2/03/23
2/03/23
Dup-2
MS/MSD-1
MS/MSD-2
From SS-9
From SS-11
From SS-9
From SS-11
Grab
Grab
Grab
Grab
Silty Sand, dark brown, no odor, moist/frozen.
Silty Sand, dark brown, no odor, moist/frozen.
silty sand, no odor, dark brown, moist/frozen
silty sand, no odor, dark brown, moist/frozen
9:00
10:00
11:20
12:45
15:30

Appendix G
Laboratory Reports

ANALYTICAL REPORT
January 30, 2023
Revised Report
Tetra Tech Inc. - UT
Sample Delivery Group:L1577056
Samples Received:01/18/2023
Project Number:RECYCLED EARTH
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
January 30, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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January 30, 2023
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SITE-SOUTH L1577056-01 5
SITE-NORTH L1577056-02 9
Qc: Quality Control Summary 13
Gravimetric Analysis by Method 2540 C-2011 13
Gravimetric Analysis by Method 2540 D-2015 14
Wet Chemistry by Method 1664A 15
Wet Chemistry by Method 410.4 16
Wet Chemistry by Method 4500H+ B-2011 17
Mercury by Method 245.1 18
Metals (ICP) by Method 200.7 19
Volatile Organic Compounds (GC) by Method 8015D/GRO 22
Volatile Organic Compounds (GC/MS) by Method 624.1 23
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 25
Pesticides (GC) by Method EPA 608.3 26
Polychlorinated Biphenyls (GC) by Method EPA-608.3 29
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 30
Gl: Glossary of Terms 35
Al: Accreditations & Locations 36
Sc: Sample Chain of Custody 37
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SITE-SOUTH L1577056-01 WW Anna Rasmuson 01/17/23 13:00 01/18/23 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1991110 1 01/19/23 09:10 01/19/23 10:25 AS Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015 WG1990901 1 01/18/23 16:38 01/18/23 18:56 AS Mt. Juliet, TN
Wet Chemistry by Method 1664A WG1992203 1 01/20/23 14:27 01/20/23 20:13 ICD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG1991163 1 01/19/23 14:18 01/19/23 16:43 NEF Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011 WG1991157 1 01/19/23 18:00 01/19/23 18:00 KAD Mt. Juliet, TN
Mercury by Method 245.1 WG1993212 1 01/23/23 11:18 01/23/23 17:01 SRT Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1991625 1 01/20/23 08:09 01/21/23 01:01 ZSA Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1995184 1 01/26/23 13:33 01/27/23 10:12 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1991047 1 01/19/23 04:57 01/19/23 04:57 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1992102 1 01/20/23 14:04 01/20/23 14:04 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG1991076 1 01/19/23 07:10 01/19/23 19:24 MAA Mt. Juliet, TN
Pesticides (GC) by Method EPA 608.3 WG1991021 1 01/19/23 22:58 01/20/23 12:58 AMM Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method EPA-608.3 WG1991021 1 01/19/23 22:58 01/20/23 12:58 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1994855 1 01/26/23 07:51 01/26/23 15:40 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SITE-NORTH L1577056-02 WW Anna Rasmuson 01/17/23 12:30 01/18/23 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1991110 1 01/19/23 09:10 01/19/23 10:25 AS Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015 WG1990901 1 01/18/23 16:38 01/18/23 18:56 AS Mt. Juliet, TN
Wet Chemistry by Method 1664A WG1992203 1 01/20/23 14:27 01/20/23 20:13 ICD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG1991163 1 01/19/23 14:18 01/19/23 16:44 NEF Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011 WG1991157 1 01/19/23 18:00 01/19/23 18:00 KAD Mt. Juliet, TN
Mercury by Method 245.1 WG1993212 1 01/23/23 11:18 01/23/23 17:03 SRT Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1991625 1 01/20/23 08:09 01/21/23 01:04 ZSA Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1995184 1 01/26/23 13:33 01/27/23 10:15 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1991047 1 01/19/23 05:19 01/19/23 05:19 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1992102 1 01/20/23 14:26 01/20/23 14:26 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG1991076 1 01/19/23 07:10 01/19/23 21:05 MAA Mt. Juliet, TN
Pesticides (GC) by Method EPA 608.3 WG1991021 1 01/19/23 22:58 01/20/23 13:06 AMM Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method EPA-608.3 WG1991021 1 01/19/23 22:58 01/20/23 13:06 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1994855 1 01/26/23 07:51 01/27/23 10:28 AMG Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 01/25/23 12:42
Project Narrative
Report reissued to add in additional compounds
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1577056
SITE-SOUTH
Collected date/time: 01/17/23 13:00
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 657 13.3 1 01/19/2023 10:25 WG1991110
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 49.6 5.00 1 01/18/2023 18:56 WG1990901
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.62 1 01/20/2023 20:13 WG1992203
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 39.3 20.0 1 01/19/2023 16:43 WG1991163
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 8.79 T8 1 01/19/2023 18:00 WG1991157
Sample Narrative:
L1577056-01 WG1991157: 8.79 at 18.5C
Mercury by Method 245.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 01/23/2023 17:01 WG1993212
Metals (ICP) by Method 200.7
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aluminum 1.61 0.200 1 01/21/2023 01:01 WG1991625
Arsenic 0.0267 0.0100 1 01/21/2023 01:01 WG1991625
Barium 0.121 0.00500 1 01/21/2023 01:01 WG1991625
Beryllium ND 0.00200 1 01/21/2023 01:01 WG1991625
Cadmium ND 0.00200 1 01/21/2023 01:01 WG1991625
Chromium 0.0132 0.0100 1 01/21/2023 01:01 WG1991625
Copper 0.0244 0.0100 1 01/21/2023 01:01 WG1991625
Iron 2.90 0.100 1 01/21/2023 01:01 WG1991625
Lead ND 0.00500 1 01/27/2023 10:12 WG1995184
Selenium ND 0.0100 1 01/21/2023 01:01 WG1991625
Silver ND 0.00500 1 01/21/2023 01:01 WG1991625
Zinc ND 0.0500 1 01/21/2023 01:01 WG1991625
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 01/19/2023 04:57 WG1991047
(S) a,a,a-Trifluorotoluene(FID) 101 78.0-120 01/19/2023 04:57 WG1991047
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1577056
SITE-SOUTH
Collected date/time: 01/17/23 13:00
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acrolein ND 0.0500 1 01/20/2023 14:04 WG1992102
Acrylonitrile ND 0.0100 1 01/20/2023 14:04 WG1992102
Benzene ND 0.00100 1 01/20/2023 14:04 WG1992102
Bromodichloromethane ND 0.00100 1 01/20/2023 14:04 WG1992102
Bromoform ND 0.00100 1 01/20/2023 14:04 WG1992102
Bromomethane ND 0.00500 1 01/20/2023 14:04 WG1992102
Carbon tetrachloride ND 0.00100 1 01/20/2023 14:04 WG1992102
Chlorobenzene ND 0.00100 1 01/20/2023 14:04 WG1992102
Chlorodibromomethane ND 0.00100 1 01/20/2023 14:04 WG1992102
Chloroethane ND 0.00500 1 01/20/2023 14:04 WG1992102
2-Chloroethyl vinyl ether ND 0.0500 1 01/20/2023 14:04 WG1992102
Chloroform ND 0.00500 1 01/20/2023 14:04 WG1992102
Chloromethane ND 0.00250 1 01/20/2023 14:04 WG1992102
1,2-Dichlorobenzene ND 0.00100 1 01/20/2023 14:04 WG1992102
1,3-Dichlorobenzene ND 0.00100 1 01/20/2023 14:04 WG1992102
1,4-Dichlorobenzene ND 0.00100 1 01/20/2023 14:04 WG1992102
Dichlorodifluoromethane ND 0.00500 1 01/20/2023 14:04 WG1992102
1,1-Dichloroethane ND 0.00100 1 01/20/2023 14:04 WG1992102
1,2-Dichloroethane ND 0.00100 1 01/20/2023 14:04 WG1992102
1,1-Dichloroethene ND 0.00100 1 01/20/2023 14:04 WG1992102
trans-1,2-Dichloroethene ND 0.00100 1 01/20/2023 14:04 WG1992102
1,2-Dichloropropane ND 0.00100 1 01/20/2023 14:04 WG1992102
cis-1,3-Dichloropropene ND 0.00100 1 01/20/2023 14:04 WG1992102
trans-1,3-Dichloropropene ND 0.00100 1 01/20/2023 14:04 WG1992102
Ethylbenzene ND 0.00100 1 01/20/2023 14:04 WG1992102
Methylene Chloride ND 0.00500 1 01/20/2023 14:04 WG1992102
Methyl tert-butyl ether ND 0.00100 1 01/20/2023 14:04 WG1992102
1,1,2,2-Tetrachloroethane ND 0.00100 1 01/20/2023 14:04 WG1992102
Tetrachloroethene ND 0.00100 1 01/20/2023 14:04 WG1992102
Toluene ND 0.00100 1 01/20/2023 14:04 WG1992102
1,1,1-Trichloroethane ND 0.00100 1 01/20/2023 14:04 WG1992102
1,1,2-Trichloroethane ND 0.00100 1 01/20/2023 14:04 WG1992102
Trichloroethene ND 0.00100 1 01/20/2023 14:04 WG1992102
Trichlorofluoromethane ND 0.00500 1 01/20/2023 14:04 WG1992102
Vinyl chloride ND 0.00100 1 01/20/2023 14:04 WG1992102
Total Xylenes ND 0.00300 1 01/20/2023 14:04 WG1992102
(S) Toluene-d8 96.9 80.0-120 01/20/2023 14:04 WG1992102
(S) 4-Bromofluorobenzene 98.8 80.0-120 01/20/2023 14:04 WG1992102
(S) 1,2-Dichloroethane-d4 117 70.0-130 01/20/2023 14:04 WG1992102
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 0.869 0.100 1 01/19/2023 19:24 WG1991076
(S) o-Terphenyl 83.7 31.0-160 01/19/2023 19:24 WG1991076
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aldrin ND 0.0000500 1 01/20/2023 12:58 WG1991021
Alpha BHC ND 0.0000500 1 01/20/2023 12:58 WG1991021
Beta BHC ND 0.0000500 1 01/20/2023 12:58 WG1991021
Delta BHC ND 0.0000500 1 01/20/2023 12:58 WG1991021
Gamma BHC ND 0.0000500 1 01/20/2023 12:58 WG1991021
Chlordane ND 0.00500 1 01/20/2023 12:58 WG1991021
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 11:15 6 of 38
SAMPLE RESULTS - 01
L1577056
SITE-SOUTH
Collected date/time: 01/17/23 13:00
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
4,4-DDD ND 0.0000500 1 01/20/2023 12:58 WG1991021
4,4-DDE ND 0.0000500 1 01/20/2023 12:58 WG1991021
4,4-DDT ND 0.0000500 1 01/20/2023 12:58 WG1991021
Dieldrin ND 0.0000500 1 01/20/2023 12:58 WG1991021
Endosulfan I ND 0.0000500 1 01/20/2023 12:58 WG1991021
Endosulfan II ND 0.0000500 1 01/20/2023 12:58 WG1991021
Endosulfan sulfate ND 0.0000500 1 01/20/2023 12:58 WG1991021
Endrin ND 0.0000500 1 01/20/2023 12:58 WG1991021
Endrin aldehyde ND 0.0000500 1 01/20/2023 12:58 WG1991021
Endrin ketone ND 0.0000500 1 01/20/2023 12:58 WG1991021
Heptachlor ND 0.0000500 1 01/20/2023 12:58 WG1991021
Heptachlor epoxide ND 0.0000500 1 01/20/2023 12:58 WG1991021
Hexachlorobenzene ND 0.0000500 1 01/20/2023 12:58 WG1991021
Methoxychlor ND 0.0000500 1 01/20/2023 12:58 WG1991021
Toxaphene ND 0.000500 1 01/20/2023 12:58 WG1991021
gamma-Chlordane ND 0.0000500 1 01/20/2023 12:58 WG1991021
alpha-Chlordane ND 0.0000500 1 01/20/2023 12:58 WG1991021
(S) Decachlorobiphenyl 37.1 10.0-144 01/20/2023 12:58 WG1991021
(S) Tetrachloro-m-xylene 67.0 10.0-135 01/20/2023 12:58 WG1991021
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 01/20/2023 12:58 WG1991021
PCB 1221 ND 0.000500 1 01/20/2023 12:58 WG1991021
PCB 1232 ND 0.000500 1 01/20/2023 12:58 WG1991021
PCB 1242 ND 0.000500 1 01/20/2023 12:58 WG1991021
PCB 1248 ND 0.000500 1 01/20/2023 12:58 WG1991021
PCB 1254 ND 0.000500 1 01/20/2023 12:58 WG1991021
PCB 1260 ND 0.000500 1 01/20/2023 12:58 WG1991021
Total PCBs ND 0.000500 1 01/20/2023 12:58 WG1991021
(S) Decachlorobiphenyl 43.1 10.0-144 01/20/2023 12:58 WG1991021
(S) Tetrachloro-m-xylene 73.7 10.0-135 01/20/2023 12:58 WG1991021
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Acenaphthylene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Anthracene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Benzidine ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Benzo(a)anthracene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Benzo(b)fluoranthene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Benzo(k)fluoranthene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Benzo(g,h,i)perylene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Benzo(a)pyrene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Bis(2-chlorethoxy)methane ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Bis(2-chloroethyl)ether ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2,2-Oxybis(1-Chloropropane) ND T8 0.0100 1 01/26/2023 15:40 WG1994855
4-Bromophenyl-phenylether ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2-Chloronaphthalene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
4-Chlorophenyl-phenylether ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Chrysene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Dibenz(a,h)anthracene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
3,3-Dichlorobenzidine ND T8 0.0100 1 01/26/2023 15:40 WG1994855
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 11:15 7 of 38
SAMPLE RESULTS - 01
L1577056
SITE-SOUTH
Collected date/time: 01/17/23 13:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
2,4-Dinitrotoluene ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2,6-Dinitrotoluene ND T8 0.0100 1 01/26/2023 15:40 WG1994855
1,2-Diphenylhydrazine ND N2 0.0100 1 01/26/2023 15:40 WG1994855
Fluoranthene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Fluorene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Hexachlorobenzene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Hexachloro-1,3-butadiene ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Hexachlorocyclopentadiene ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Hexachloroethane ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Indeno(1,2,3-cd)pyrene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Isophorone ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Naphthalene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Nitrobenzene ND T8 0.0100 1 01/26/2023 15:40 WG1994855
n-Nitrosodimethylamine ND T8 0.0100 1 01/26/2023 15:40 WG1994855
n-Nitrosodiphenylamine ND T8 0.0100 1 01/26/2023 15:40 WG1994855
n-Nitrosodi-n-propylamine ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Phenanthrene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
Benzylbutyl phthalate ND T8 0.00300 1 01/26/2023 15:40 WG1994855
Bis(2-ethylhexyl)phthalate ND T8 0.00300 1 01/26/2023 15:40 WG1994855
Di-n-butyl phthalate ND T8 0.00300 1 01/26/2023 15:40 WG1994855
Diethyl phthalate ND T8 0.00300 1 01/26/2023 15:40 WG1994855
Dimethyl phthalate ND T8 0.00300 1 01/26/2023 15:40 WG1994855
Di-n-octyl phthalate ND T8 0.00300 1 01/26/2023 15:40 WG1994855
Pyrene ND T8 0.00100 1 01/26/2023 15:40 WG1994855
1,2,4-Trichlorobenzene ND T8 0.0100 1 01/26/2023 15:40 WG1994855
4-Chloro-3-methylphenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2-Chlorophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2,4-Dichlorophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2,4-Dimethylphenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
4,6-Dinitro-2-methylphenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2,4-Dinitrophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2-Nitrophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
4-Nitrophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Pentachlorophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
Phenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
2,4,6-Trichlorophenol ND T8 0.0100 1 01/26/2023 15:40 WG1994855
(S) 2-Fluorophenol 31.9 10.0-120 01/26/2023 15:40 WG1994855
(S) Phenol-d5 19.9 8.00-424 01/26/2023 15:40 WG1994855
(S) Nitrobenzene-d5 53.5 15.0-314 01/26/2023 15:40 WG1994855
(S) 2-Fluorobiphenyl 66.7 22.0-127 01/26/2023 15:40 WG1994855
(S) 2,4,6-Tribromophenol 112 10.0-153 01/26/2023 15:40 WG1994855
(S) p-Terphenyl-d14 81.1 29.0-141 01/26/2023 15:40 WG1994855
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 11:15 8 of 38
SAMPLE RESULTS - 02
L1577056
SITE-NORTH
Collected date/time: 01/17/23 12:30
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 637 13.3 1 01/19/2023 10:25 WG1991110
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 266 J3 25.0 1 01/18/2023 18:56 WG1990901
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.56 1 01/20/2023 20:13 WG1992203
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 51.3 20.0 1 01/19/2023 16:44 WG1991163
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 10.6 T8 1 01/19/2023 18:00 WG1991157
Sample Narrative:
L1577056-02 WG1991157: 10.57 at 18.5C
Mercury by Method 245.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 01/23/2023 17:03 WG1993212
Metals (ICP) by Method 200.7
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aluminum 3.56 0.200 1 01/21/2023 01:04 WG1991625
Arsenic 0.0110 0.0100 1 01/21/2023 01:04 WG1991625
Barium 0.172 0.00500 1 01/21/2023 01:04 WG1991625
Beryllium ND 0.00200 1 01/21/2023 01:04 WG1991625
Cadmium ND 0.00200 1 01/21/2023 01:04 WG1991625
Chromium 0.0257 0.0100 1 01/21/2023 01:04 WG1991625
Copper 0.0339 0.0100 1 01/21/2023 01:04 WG1991625
Iron 6.69 0.100 1 01/21/2023 01:04 WG1991625
Lead 0.00711 0.00500 1 01/27/2023 10:15 WG1995184
Selenium ND 0.0100 1 01/21/2023 01:04 WG1991625
Silver ND 0.00500 1 01/21/2023 01:04 WG1991625
Zinc 0.0605 0.0500 1 01/21/2023 01:04 WG1991625
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 01/19/2023 05:19 WG1991047
(S) a,a,a-Trifluorotoluene(FID) 102 78.0-120 01/19/2023 05:19 WG1991047
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 10:45 9 of 38
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 11:15 9 of 38
SAMPLE RESULTS - 02
L1577056
SITE-NORTH
Collected date/time: 01/17/23 12:30
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acrolein ND 0.0500 1 01/20/2023 14:26 WG1992102
Acrylonitrile ND 0.0100 1 01/20/2023 14:26 WG1992102
Benzene ND 0.00100 1 01/20/2023 14:26 WG1992102
Bromodichloromethane ND 0.00100 1 01/20/2023 14:26 WG1992102
Bromoform ND 0.00100 1 01/20/2023 14:26 WG1992102
Bromomethane ND 0.00500 1 01/20/2023 14:26 WG1992102
Carbon tetrachloride ND 0.00100 1 01/20/2023 14:26 WG1992102
Chlorobenzene ND 0.00100 1 01/20/2023 14:26 WG1992102
Chlorodibromomethane ND 0.00100 1 01/20/2023 14:26 WG1992102
Chloroethane ND 0.00500 1 01/20/2023 14:26 WG1992102
2-Chloroethyl vinyl ether ND 0.0500 1 01/20/2023 14:26 WG1992102
Chloroform ND 0.00500 1 01/20/2023 14:26 WG1992102
Chloromethane ND 0.00250 1 01/20/2023 14:26 WG1992102
1,2-Dichlorobenzene ND 0.00100 1 01/20/2023 14:26 WG1992102
1,3-Dichlorobenzene ND 0.00100 1 01/20/2023 14:26 WG1992102
1,4-Dichlorobenzene ND 0.00100 1 01/20/2023 14:26 WG1992102
Dichlorodifluoromethane ND 0.00500 1 01/20/2023 14:26 WG1992102
1,1-Dichloroethane ND 0.00100 1 01/20/2023 14:26 WG1992102
1,2-Dichloroethane ND 0.00100 1 01/20/2023 14:26 WG1992102
1,1-Dichloroethene ND 0.00100 1 01/20/2023 14:26 WG1992102
trans-1,2-Dichloroethene ND 0.00100 1 01/20/2023 14:26 WG1992102
1,2-Dichloropropane ND 0.00100 1 01/20/2023 14:26 WG1992102
cis-1,3-Dichloropropene ND 0.00100 1 01/20/2023 14:26 WG1992102
trans-1,3-Dichloropropene ND 0.00100 1 01/20/2023 14:26 WG1992102
Ethylbenzene ND 0.00100 1 01/20/2023 14:26 WG1992102
Methylene Chloride ND 0.00500 1 01/20/2023 14:26 WG1992102
Methyl tert-butyl ether ND 0.00100 1 01/20/2023 14:26 WG1992102
1,1,2,2-Tetrachloroethane ND 0.00100 1 01/20/2023 14:26 WG1992102
Tetrachloroethene ND 0.00100 1 01/20/2023 14:26 WG1992102
Toluene ND 0.00100 1 01/20/2023 14:26 WG1992102
1,1,1-Trichloroethane ND 0.00100 1 01/20/2023 14:26 WG1992102
1,1,2-Trichloroethane ND 0.00100 1 01/20/2023 14:26 WG1992102
Trichloroethene ND 0.00100 1 01/20/2023 14:26 WG1992102
Trichlorofluoromethane ND 0.00500 1 01/20/2023 14:26 WG1992102
Vinyl chloride ND 0.00100 1 01/20/2023 14:26 WG1992102
Total Xylenes ND 0.00300 1 01/20/2023 14:26 WG1992102
(S) Toluene-d8 97.4 80.0-120 01/20/2023 14:26 WG1992102
(S) 4-Bromofluorobenzene 98.3 80.0-120 01/20/2023 14:26 WG1992102
(S) 1,2-Dichloroethane-d4 120 70.0-130 01/20/2023 14:26 WG1992102
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 3.13 0.100 1 01/19/2023 21:05 WG1991076
(S) o-Terphenyl 88.4 31.0-160 01/19/2023 21:05 WG1991076
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aldrin ND 0.0000500 1 01/20/2023 13:06 WG1991021
Alpha BHC ND 0.0000500 1 01/20/2023 13:06 WG1991021
Beta BHC ND 0.0000500 1 01/20/2023 13:06 WG1991021
Delta BHC ND 0.0000500 1 01/20/2023 13:06 WG1991021
Gamma BHC ND 0.0000500 1 01/20/2023 13:06 WG1991021
Chlordane ND 0.00500 1 01/20/2023 13:06 WG1991021
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 10:45 10 of 38
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 11:15 10 of 38
SAMPLE RESULTS - 02
L1577056
SITE-NORTH
Collected date/time: 01/17/23 12:30
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
4,4-DDD ND 0.0000500 1 01/20/2023 13:06 WG1991021
4,4-DDE ND 0.0000500 1 01/20/2023 13:06 WG1991021
4,4-DDT ND 0.0000500 1 01/20/2023 13:06 WG1991021
Dieldrin ND 0.0000500 1 01/20/2023 13:06 WG1991021
Endosulfan I ND 0.0000500 1 01/20/2023 13:06 WG1991021
Endosulfan II ND 0.0000500 1 01/20/2023 13:06 WG1991021
Endosulfan sulfate ND 0.0000500 1 01/20/2023 13:06 WG1991021
Endrin ND 0.0000500 1 01/20/2023 13:06 WG1991021
Endrin aldehyde ND 0.0000500 1 01/20/2023 13:06 WG1991021
Endrin ketone ND 0.0000500 1 01/20/2023 13:06 WG1991021
Heptachlor ND 0.0000500 1 01/20/2023 13:06 WG1991021
Heptachlor epoxide ND 0.0000500 1 01/20/2023 13:06 WG1991021
Hexachlorobenzene ND 0.0000500 1 01/20/2023 13:06 WG1991021
Methoxychlor ND 0.0000500 1 01/20/2023 13:06 WG1991021
Toxaphene ND 0.000500 1 01/20/2023 13:06 WG1991021
gamma-Chlordane ND 0.0000500 1 01/20/2023 13:06 WG1991021
alpha-Chlordane ND 0.0000500 1 01/20/2023 13:06 WG1991021
(S) Decachlorobiphenyl 15.0 10.0-144 01/20/2023 13:06 WG1991021
(S) Tetrachloro-m-xylene 57.0 10.0-135 01/20/2023 13:06 WG1991021
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 01/20/2023 13:06 WG1991021
PCB 1221 ND 0.000500 1 01/20/2023 13:06 WG1991021
PCB 1232 ND 0.000500 1 01/20/2023 13:06 WG1991021
PCB 1242 ND 0.000500 1 01/20/2023 13:06 WG1991021
PCB 1248 ND 0.000500 1 01/20/2023 13:06 WG1991021
PCB 1254 ND 0.000500 1 01/20/2023 13:06 WG1991021
PCB 1260 ND 0.000500 1 01/20/2023 13:06 WG1991021
Total PCBs ND 0.000500 1 01/20/2023 13:06 WG1991021
(S) Decachlorobiphenyl 18.4 10.0-144 01/20/2023 13:06 WG1991021
(S) Tetrachloro-m-xylene 66.2 10.0-135 01/20/2023 13:06 WG1991021
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Acenaphthylene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Anthracene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Benzidine ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Benzo(a)anthracene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Benzo(b)fluoranthene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Benzo(k)fluoranthene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Benzo(g,h,i)perylene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Benzo(a)pyrene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Bis(2-chlorethoxy)methane ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Bis(2-chloroethyl)ether ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2,2-Oxybis(1-Chloropropane) ND T8 0.0100 1 01/27/2023 10:28 WG1994855
4-Bromophenyl-phenylether ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2-Chloronaphthalene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
4-Chlorophenyl-phenylether ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Chrysene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Dibenz(a,h)anthracene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
3,3-Dichlorobenzidine ND T8 0.0100 1 01/27/2023 10:28 WG1994855
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1577056
SITE-NORTH
Collected date/time: 01/17/23 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
2,4-Dinitrotoluene ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2,6-Dinitrotoluene ND T8 0.0100 1 01/27/2023 10:28 WG1994855
1,2-Diphenylhydrazine ND N2 0.0100 1 01/27/2023 10:28 WG1994855
Fluoranthene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Fluorene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Hexachlorobenzene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Hexachloro-1,3-butadiene ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Hexachlorocyclopentadiene ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Hexachloroethane ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Indeno(1,2,3-cd)pyrene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Isophorone ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Naphthalene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Nitrobenzene ND T8 0.0100 1 01/27/2023 10:28 WG1994855
n-Nitrosodimethylamine ND T8 0.0100 1 01/27/2023 10:28 WG1994855
n-Nitrosodiphenylamine ND T8 0.0100 1 01/27/2023 10:28 WG1994855
n-Nitrosodi-n-propylamine ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Phenanthrene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
Benzylbutyl phthalate ND T8 0.00300 1 01/27/2023 10:28 WG1994855
Bis(2-ethylhexyl)phthalate ND T8 0.00300 1 01/27/2023 10:28 WG1994855
Di-n-butyl phthalate ND T8 0.00300 1 01/27/2023 10:28 WG1994855
Diethyl phthalate ND T8 0.00300 1 01/27/2023 10:28 WG1994855
Dimethyl phthalate ND T8 0.00300 1 01/27/2023 10:28 WG1994855
Di-n-octyl phthalate ND T8 0.00300 1 01/27/2023 10:28 WG1994855
Pyrene ND T8 0.00100 1 01/27/2023 10:28 WG1994855
1,2,4-Trichlorobenzene ND T8 0.0100 1 01/27/2023 10:28 WG1994855
4-Chloro-3-methylphenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2-Chlorophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2,4-Dichlorophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2,4-Dimethylphenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
4,6-Dinitro-2-methylphenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2,4-Dinitrophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2-Nitrophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
4-Nitrophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Pentachlorophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
Phenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
2,4,6-Trichlorophenol ND T8 0.0100 1 01/27/2023 10:28 WG1994855
(S) 2-Fluorophenol 26.0 10.0-120 01/27/2023 10:28 WG1994855
(S) Phenol-d5 17.8 8.00-424 01/27/2023 10:28 WG1994855
(S) Nitrobenzene-d5 52.0 15.0-314 01/27/2023 10:28 WG1994855
(S) 2-Fluorobiphenyl 74.6 22.0-127 01/27/2023 10:28 WG1994855
(S) 2,4,6-Tribromophenol 115 10.0-153 01/27/2023 10:28 WG1994855
(S) p-Terphenyl-d14 96.9 29.0-141 01/27/2023 10:28 WG1994855
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991110
Gravimetric Analysis by Method 2540 C-2011 L1577056-01,02
Method Blank (MB)
(MB) R3883116-1 01/19/23 10:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U 10.0 10.0
Laboratory Control Sample (LCS)
(LCS) R3883116-2 01/19/23 10:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Dissolved Solids 8800 7290 82.8 77.3-123
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1990901
Gravimetric Analysis by Method 2540 D-2015 L1577056-01,02
Method Blank (MB)
(MB) R3882351-1 01/18/23 18:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Suspended Solids U 2.50 2.50
L1576975-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1576975-01 01/18/23 18:56 • (DUP) R3882351-3 01/18/23 18:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Suspended Solids 46.8 53.6 1 13.5 J3 5
L1577056-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1577056-02 01/18/23 18:56 • (DUP) R3882351-4 01/18/23 18:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Suspended Solids 266 331 1 21.8 J3 5
Laboratory Control Sample (LCS)
(LCS) R3882351-2 01/18/23 18:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Suspended Solids 773 848 110 85.7-114
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1992203
Wet Chemistry by Method 1664A L1577056-01,02
Method Blank (MB)
(MB) R3883066-1 01/20/23 20:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3883066-2 01/20/23 20:13 • (LCSD) R3883066-3 01/20/23 20:13
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 32.3 31.3 80.8 78.3 78.0-114 3.14 20
L1577017-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1577017-02 01/20/23 20:13 • (MS) R3883066-4 01/20/23 20:13
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr) 40.0 ND 29.7 68.4 1 78.0-114 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991163
Wet Chemistry by Method 410.4 L1577056-01,02
Method Blank (MB)
(MB) R3882657-1 01/19/23 16:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
COD U 11.7 20.0
L1569484-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1569484-02 01/19/23 16:37 • (DUP) R3882657-3 01/19/23 16:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
COD 1470 1490 5 0.926 20
L1577001-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1577001-03 01/19/23 16:41 • (DUP) R3882657-6 01/19/23 16:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
COD 29.3 30.4 1 3.50 20
Laboratory Control Sample (LCS)
(LCS) R3882657-2 01/19/23 16:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
COD 500 481 96.2 90.0-110
L1576911-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576911-01 01/19/23 16:39 • (MS) R3882657-4 01/19/23 16:40 • (MSD) R3882657-5 01/19/23 16:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
COD 500 220 814 741 119 104 1 80.0-120 9.37 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991157
Wet Chemistry by Method 4500H+ B-2011 L1577056-01,02
L1576879-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1576879-01 01/19/23 18:00 • (DUP) R3882693-2 01/19/23 18:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 7.84 7.84 1 0.000 1
Sample Narrative:
OS: 7.84 at 19.6C
DUP: 7.84 at 19.6C
L1577209-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1577209-02 01/19/23 18:00 • (DUP) R3882693-3 01/19/23 18:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 9.23 9.24 1 0.108 1
Sample Narrative:
OS: 9.23 at 19.7C
DUP: 9.24 at 19.3C
Laboratory Control Sample (LCS)
(LCS) R3882693-1 01/19/23 18:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su %%
pH 10.0 9.90 99.0 99.0-101
Sample Narrative:
LCS: 9.9 at 20.5C
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1993212
Mercury by Method 245.1 L1577056-01,02
Method Blank (MB)
(MB) R3883591-1 01/23/23 16:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3883591-2 01/23/23 16:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00316 105 85.0-115
L1577227-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1577227-01 01/23/23 16:52 • (MS) R3883591-3 01/23/23 16:54 • (MSD) R3883591-4 01/23/23 16:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00351 0.00327 112 104 1 70.0-130 7.08 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991625
Metals (ICP) by Method 200.7 L1577056-01,02
Method Blank (MB)
(MB) R3883233-1 01/21/23 00:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Aluminum U 0.0592 0.200
Arsenic U 0.00645 0.0100
Barium U 0.000795 0.00500
Beryllium U 0.000401 0.00200
Cadmium U 0.000552 0.00200
Chromium U 0.00163 0.0100
Copper U 0.00226 0.0100
Iron U 0.0205 0.100
Selenium U 0.00616 0.0100
Silver U 0.00131 0.00500
Zinc U 0.00578 0.0500
Laboratory Control Sample (LCS)
(LCS) R3883233-2 01/21/23 00:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Aluminum 10.0 9.48 94.8 85.0-115
Arsenic 1.00 0.939 93.9 85.0-115
Barium 1.00 0.989 98.9 85.0-115
Beryllium 1.00 0.984 98.4 85.0-115
Cadmium 1.00 0.979 97.9 85.0-115
Chromium 1.00 0.956 95.6 85.0-115
Copper 1.00 0.934 93.4 85.0-115
Iron 10.0 9.86 98.6 85.0-115
Selenium 1.00 0.972 97.2 85.0-115
Silver 0.200 0.178 89.1 85.0-115
Zinc 1.00 0.959 95.9 85.0-115
L1576680-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576680-01 01/21/23 00:16 • (MS) R3883233-4 01/21/23 00:21 • (MSD) R3883233-5 01/21/23 00:24
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Aluminum 10.0 0.285 9.79 9.56 95.0 92.7 1 70.0-130 2.38 20
Arsenic 1.00 ND 0.978 0.948 97.0 94.0 1 70.0-130 3.11 20
Barium 1.00 0.00721 1.00 0.979 99.5 97.2 1 70.0-130 2.39 20
Beryllium 1.00 ND 0.991 0.965 99.1 96.5 1 70.0-130 2.70 20
Cadmium 1.00 ND 0.999 0.973 99.9 97.3 1 70.0-130 2.63 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991625
Metals (ICP) by Method 200.7 L1577056-01,02
L1576680-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576680-01 01/21/23 00:16 • (MS) R3883233-4 01/21/23 00:21 • (MSD) R3883233-5 01/21/23 00:24
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Chromium 1.00 ND 0.974 0.943 97.1 94.0 1 70.0-130 3.25 20
Copper 1.00 0.0179 0.972 0.955 95.5 93.7 1 70.0-130 1.86 20
Iron 10.0 1.33 11.1 10.8 98.0 94.5 1 70.0-130 3.17 20
Selenium 1.00 ND 1.00 0.983 100 98.3 1 70.0-130 2.02 20
Silver 0.200 ND 0.179 0.175 89.6 87.7 1 70.0-130 2.16 20
Zinc 1.00 ND 0.978 0.953 96.4 94.0 1 70.0-130 2.50 20
L1576685-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576685-01 01/21/23 00:26 • (MS) R3883233-6 01/21/23 00:29 • (MSD) R3883233-7 01/21/23 00:31
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Aluminum 10.0 1.47 11.6 11.7 101 102 1 70.0-130 0.999 20
Arsenic 1.00 ND 0.993 0.988 98.4 97.9 1 70.0-130 0.475 20
Barium 1.00 0.0181 1.03 1.03 102 101 1 70.0-130 0.422 20
Beryllium 1.00 ND 1.00 0.998 100 99.8 1 70.0-130 0.485 20
Cadmium 1.00 ND 1.03 1.03 103 103 1 70.0-130 0.338 20
Chromium 1.00 0.0124 1.00 0.998 98.8 98.6 1 70.0-130 0.252 20
Copper 1.00 0.0257 1.03 1.02 101 99.7 1 70.0-130 0.862 20
Iron 10.0 1.62 11.6 11.6 99.5 99.5 1 70.0-130 0.0370 20
Selenium 1.00 ND 1.03 1.02 103 102 1 70.0-130 0.817 20
Silver 0.200 ND 0.188 0.187 94.2 93.4 1 70.0-130 0.857 20
Zinc 1.00 0.241 1.23 1.22 98.9 98.3 1 70.0-130 0.490 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1995184
Metals (ICP) by Method 200.7 L1577056-01,02
Method Blank (MB)
(MB) R3885147-1 01/27/23 09:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Lead U 0.00227 0.00500
Laboratory Control Sample (LCS)
(LCS) R3885147-2 01/27/23 09:58
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Lead 1.00 0.930 93.0 85.0-115
L1579086-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1579086-01 01/27/23 10:01 • (MS) R3885147-4 01/27/23 10:06 • (MSD) R3885147-5 01/27/23 10:09
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Lead 1.00 ND 0.954 0.960 95.4 96.0 1 70.0-130 0.672 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991047
Volatile Organic Compounds (GC) by Method 8015D/GRO L1577056-01,02
Method Blank (MB)
(MB) R3882601-2 01/18/23 22:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 0.0408 J 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)101 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3882601-1 01/18/23 21:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.86 107 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 107 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1992102
Volatile Organic Compounds (GC/MS) by Method 624.1 L1577056-01,02
Method Blank (MB)
(MB) R3883913-2 01/20/23 09:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
2-Chloroethyl vinyl ether U 0.000575 0.0500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
Ethylbenzene U 0.000137 0.00100
Methylene Chloride U 0.000430 0.00500
Methyl tert-butyl ether U 0.000101 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 97.7 80.0-120
(S) 4-Bromofluorobenzene 101 80.0-120
(S) 1,2-Dichloroethane-d4 118 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1992102
Volatile Organic Compounds (GC/MS) by Method 624.1 L1577056-01,02
Laboratory Control Sample (LCS)
(LCS) R3883913-1 01/20/23 09:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acrolein 0.0250 0.0262 105 60.0-140
Acrylonitrile 0.0250 0.0344 138 60.0-140
Benzene 0.00500 0.00444 88.8 65.0-135
Bromodichloromethane 0.00500 0.00467 93.4 65.0-135
Bromoform 0.00500 0.00417 83.4 70.0-130
Bromomethane 0.00500 0.00236 47.2 15.0-185
Carbon tetrachloride 0.00500 0.00472 94.4 70.0-130
Chlorobenzene 0.00500 0.00416 83.2 65.0-135
Chlorodibromomethane 0.00500 0.00417 83.4 70.0-135
Chloroethane 0.00500 0.00607 121 40.0-160
2-Chloroethyl vinyl ether 0.0250 0.0389 156 0.100-225
Chloroform 0.00500 0.00459 91.8 70.0-135
Chloromethane 0.00500 0.00650 130 0.100-205
1,2-Dichlorobenzene 0.00500 0.00498 99.6 65.0-135
1,3-Dichlorobenzene 0.00500 0.00471 94.2 70.0-130
1,4-Dichlorobenzene 0.00500 0.00450 90.0 65.0-135
Dichlorodifluoromethane 0.00500 0.00410 82.0 49.0-155
1,1-Dichloroethane 0.00500 0.00534 107 70.0-130
1,2-Dichloroethane 0.00500 0.00530 106 70.0-130
1,1-Dichloroethene 0.00500 0.00463 92.6 50.0-150
trans-1,2-Dichloroethene 0.00500 0.00449 89.8 70.0-130
1,2-Dichloropropane 0.00500 0.00531 106 35.0-165
cis-1,3-Dichloropropene 0.00500 0.00449 89.8 25.0-175
trans-1,3-Dichloropropene 0.00500 0.00436 87.2 50.0-150
Ethylbenzene 0.00500 0.00430 86.0 60.0-140
Methylene Chloride 0.00500 0.00422 84.4 60.0-140
Methyl tert-butyl ether 0.00500 0.00500 100 64.0-123
1,1,2,2-Tetrachloroethane 0.00500 0.00459 91.8 60.0-140
Tetrachloroethene 0.00500 0.00433 86.6 70.0-130
Toluene 0.00500 0.00422 84.4 70.0-130
1,1,1-Trichloroethane 0.00500 0.00485 97.0 70.0-130
1,1,2-Trichloroethane 0.00500 0.00428 85.6 70.0-130
Trichloroethene 0.00500 0.00449 89.8 65.0-135
Trichlorofluoromethane 0.00500 0.00505 101 50.0-150
Vinyl chloride 0.00500 0.00595 119 5.00-195
Xylenes, Total 0.0150 0.0134 89.3 77.0-120
(S) Toluene-d8 96.9 80.0-120
(S) 4-Bromofluorobenzene 99.7 80.0-120
(S) 1,2-Dichloroethane-d4 116 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991076
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1577056-01,02
Method Blank (MB)
(MB) R3882764-1 01/19/23 12:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) High Fraction U 0.0247 0.100
(S) o-Terphenyl 100 31.0-160
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3882764-2 01/19/23 13:15 • (LCSD) R3882764-3 01/19/23 13:35
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.50 1.60 1.65 107 110 50.0-150 3.08 20
(S) o-Terphenyl 67.5 70.0 31.0-160
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Pesticides (GC) by Method EPA 608.3 L1577056-01,02
Method Blank (MB)
(MB) R3883380-1 01/20/23 12:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Aldrin U 0.0000198 0.0000500
Alpha BHC U 0.0000172 0.0000500
Beta BHC U 0.0000208 0.0000500
Delta BHC U 0.0000150 0.0000500
Gamma BHC U 0.0000209 0.0000500
Chlordane U 0.0000198 0.00500
4,4-DDD U 0.0000177 0.0000500
4,4-DDE U 0.0000154 0.0000500
4,4-DDT U 0.0000198 0.0000500
Dieldrin U 0.0000162 0.0000500
Endosulfan I U 0.0000160 0.0000500
Endosulfan II U 0.0000164 0.0000500
Endosulfan sulfate U 0.0000217 0.0000500
Endrin U 0.0000161 0.0000500
Endrin aldehyde U 0.0000237 0.0000500
Endrin ketone U 0.0000219 0.0000500
Heptachlor U 0.0000148 0.0000500
Heptachlor epoxide U 0.0000183 0.0000500
Hexachlorobenzene U 0.0000176 0.0000500
Methoxychlor U 0.0000193 0.0000500
Toxaphene U 0.000168 0.000500
gamma-Chlordane U 0.0000137 0.0000500
alpha-Chlordane U 0.0000149 0.0000500
(S) Decachlorobiphenyl 75.5 10.0-144
(S) Tetrachloro-m-xylene 55.0 10.0-135
Laboratory Control Sample (LCS)
(LCS) R3883380-2 01/20/23 12:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Aldrin 0.00100 0.000808 80.8 42.0-140
Alpha BHC 0.00100 0.000854 85.4 37.0-140
Beta BHC 0.00100 0.00100 100 17.0-147
Delta BHC 0.00100 0.000924 92.4 19.0-140
Gamma BHC 0.00100 0.000840 84.0 32.0-140
4,4-DDD 0.00100 0.00100 100 31.0-141
4,4-DDE 0.00100 0.00104 104 30.0-145
4,4-DDT 0.00100 0.00102 102 25.0-160
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Pesticides (GC) by Method EPA 608.3 L1577056-01,02
Laboratory Control Sample (LCS)
(LCS) R3883380-2 01/20/23 12:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Dieldrin 0.00100 0.000847 84.7 36.0-146
Endosulfan I 0.00100 0.000907 90.7 45.0-153
Endosulfan II 0.00100 0.000938 93.8 1.00-202
Endosulfan sulfate 0.00100 0.000940 94.0 26.0-144
Endrin 0.00100 0.000895 89.5 30.0-147
Endrin aldehyde 0.00100 0.000991 99.1 56.0-128
Endrin ketone 0.00100 0.000944 94.4 54.0-142
Heptachlor 0.00100 0.000800 80.0 34.0-140
Heptachlor epoxide 0.00100 0.000901 90.1 37.0-142
Hexachlorobenzene 0.00100 0.000914 91.4 35.0-120
Methoxychlor 0.00100 0.00108 108 44.0-160
gamma-Chlordane 0.00100 0.000991 99.1 45.0-140
alpha-Chlordane 0.00100 0.000876 87.6 45.0-140
(S) Decachlorobiphenyl 68.7 10.0-144
(S) Tetrachloro-m-xylene 55.4 10.0-135
L1576864-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576864-09 01/20/23 15:02 • (MS) R3883380-4 01/20/23 15:12 • (MSD) R3883380-5 01/20/23 15:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Aldrin 0.00100 ND 0.000691 0.000720 69.1 72.0 1 42.0-140 4.11 35
Alpha BHC 0.00100 ND 0.000724 0.000766 72.4 76.6 1 37.0-140 5.64 36
Beta BHC 0.00100 ND 0.000838 0.000889 83.8 88.9 1 17.0-147 5.91 44
Delta BHC 0.00100 ND 0.000823 0.000808 82.3 80.8 1 19.0-140 1.84 52
Gamma BHC 0.00100 ND 0.000706 0.000766 70.6 76.6 1 32.0-140 8.15 39
4,4-DDD 0.00100 ND 0.000826 0.000924 82.6 92.4 1 31.0-141 11.2 39
4,4-DDE 0.00100 ND 0.000728 0.000792 72.8 79.2 1 30.0-145 8.42 35
4,4-DDT 0.00100 ND 0.000478 0.000530 47.8 53.0 1 25.0-160 10.3 42
Dieldrin 0.00100 ND 0.000696 0.000737 69.6 73.7 1 36.0-146 5.72 49
Endosulfan I 0.00100 ND 0.000664 0.000736 66.4 73.6 1 45.0-153 10.3 28
Endosulfan II 0.00100 ND 0.000672 0.000704 67.2 70.4 1 1.00-202 4.65 53
Endosulfan sulfate 0.00100 ND 0.000609 0.000692 60.9 69.2 1 26.0-144 12.8 38
Endrin 0.00100 ND 0.000607 0.000678 60.7 67.8 1 30.0-147 11.1 48
Endrin aldehyde 0.00100 ND 0.000647 0.000737 64.7 73.7 1 56.0-128 13.0 20
Endrin ketone 0.00100 ND 0.000621 0.000688 62.1 68.8 1 54.0-142 10.2 20
Heptachlor 0.00100 ND 0.000605 0.000628 60.5 62.8 1 34.0-140 3.73 43
Heptachlor epoxide 0.00100 ND 0.000659 0.000718 65.9 71.8 1 37.0-142 8.57 26
Hexachlorobenzene 0.00100 ND 0.000689 0.000727 68.9 72.7 1 35.0-120 5.37 25
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Pesticides (GC) by Method EPA 608.3 L1577056-01,02
L1576864-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576864-09 01/20/23 15:02 • (MS) R3883380-4 01/20/23 15:12 • (MSD) R3883380-5 01/20/23 15:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Methoxychlor 0.00100 ND 0.000577 0.000629 57.7 62.9 1 44.0-160 8.62 22
gamma-Chlordane 0.00100 ND 0.000725 0.000784 72.5 78.4 1 45.0-140 7.82 35
alpha-Chlordane 0.00100 ND 0.000597 0.000622 59.7 62.2 1 45.0-140 4.10 35
(S) Decachlorobiphenyl 57.9 52.4 10.0-144
(S) Tetrachloro-m-xylene 37.7 38.9 10.0-135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Polychlorinated Biphenyls (GC) by Method EPA-608.3 L1577056-01,02
Method Blank (MB)
(MB) R3883380-1 01/20/23 12:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
Total PCBs U 0.000173 0.000500
(S) Decachlorobiphenyl 87.9 10.0-144
(S) Tetrachloro-m-xylene 71.1 10.0-135
Laboratory Control Sample (LCS)
(LCS) R3883380-3 01/20/23 12:38
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
PCB 1016 0.00250 0.00204 81.6 50.0-140
PCB 1260 0.00250 0.00233 93.2 8.00-140
(S) Decachlorobiphenyl 67.5 10.0-144
(S) Tetrachloro-m-xylene 69.8 10.0-135
L1576864-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576864-09 01/20/23 15:02 • (MS) R3883380-6 01/20/23 15:33 • (MSD) R3883380-7 01/20/23 15:43
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 ND 0.00157 0.00137 62.8 54.8 1 50.0-140 13.6 36
PCB 1260 0.00250 ND 0.00191 0.00190 76.4 76.0 1 8.00-140 0.525 38
(S) Decachlorobiphenyl 64.0 69.6 10.0-144
(S) Tetrachloro-m-xylene 57.1 55.6 10.0-135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1994855
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577056-01,02
Method Blank (MB)
(MB) R3884839-2 01/26/23 16:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-oxybis(1-chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
1,2-Diphenylhydrazine U N2 0.000105 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1994855
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577056-01,02
Method Blank (MB)
(MB) R3884839-2 01/26/23 16:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 58.0 10.0-120
(S) Phenol-d5 35.1 8.00-424
(S) Nitrobenzene-d5 93.2 15.0-314
(S) 2-Fluorobiphenyl 82.6 22.0-127
(S) 2,4,6-Tribromophenol 85.5 10.0-153
(S) p-Terphenyl-d14 83.2 29.0-141
Laboratory Control Sample (LCS)
(LCS) R3884839-1 01/26/23 15:51
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acenaphthene 0.0500 0.0448 89.6 47.0-145
Acenaphthylene 0.0500 0.0480 96.0 33.0-145
Anthracene 0.0500 0.0434 86.8 27.0-133
Benzidine 0.100 0.0282 28.2 1.00-120
Benzo(a)anthracene 0.0500 0.0499 99.8 33.0-143
Benzo(b)fluoranthene 0.0500 0.0456 91.2 24.0-159
Benzo(k)fluoranthene 0.0500 0.0421 84.2 11.0-162
Benzo(g,h,i)perylene 0.0500 0.0473 94.6 1.00-219
Benzo(a)pyrene 0.0500 0.0469 93.8 17.0-163
Bis(2-chlorethoxy)methane 0.0500 0.0404 80.8 1.00-219
Bis(2-chloroethyl)ether 0.0500 0.0412 82.4 33.0-185
2,2-oxybis(1-chloropropane) 0.0500 0.0420 84.0 36.0-166
4-Bromophenyl-phenylether 0.0500 0.0544 109 53.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1994855
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577056-01,02
Laboratory Control Sample (LCS)
(LCS) R3884839-1 01/26/23 15:51
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Chloronaphthalene 0.0500 0.0417 83.4 60.0-120
4-Chlorophenyl-phenylether 0.0500 0.0489 97.8 25.0-158
Chrysene 0.0500 0.0466 93.2 17.0-168
Dibenz(a,h)anthracene 0.0500 0.0501 100 1.00-227
3,3-Dichlorobenzidine 0.100 0.0874 87.4 1.00-262
2,4-Dinitrotoluene 0.0500 0.0528 106 39.0-139
2,6-Dinitrotoluene 0.0500 0.0503 101 50.0-158
1,2-Diphenylhydrazine 0.0500 0.0545 109 37.0-125 N2
Fluoranthene 0.0500 0.0517 103 26.0-137
Fluorene 0.0500 0.0474 94.8 59.0-121
Hexachlorobenzene 0.0500 0.0443 88.6 1.00-152
Hexachloro-1,3-butadiene 0.0500 0.0378 75.6 24.0-120
Hexachlorocyclopentadiene 0.0500 0.0256 51.2 10.0-120
Hexachloroethane 0.0500 0.0368 73.6 40.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0469 93.8 1.00-171
Isophorone 0.0500 0.0420 84.0 21.0-196
Naphthalene 0.0500 0.0345 69.0 21.0-133
Nitrobenzene 0.0500 0.0418 83.6 35.0-180
n-Nitrosodimethylamine 0.0500 0.0343 68.6 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0365 73.0 44.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0496 99.2 1.00-230
Phenanthrene 0.0500 0.0453 90.6 54.0-120
Benzylbutyl phthalate 0.0500 0.0464 92.8 1.00-152
Bis(2-ethylhexyl)phthalate 0.0500 0.0441 88.2 8.00-158
Di-n-butyl phthalate 0.0500 0.0521 104 1.00-120
Diethyl phthalate 0.0500 0.0534 107 1.00-120
Dimethyl phthalate 0.0500 0.0512 102 1.00-120
Di-n-octyl phthalate 0.0500 0.0517 103 4.00-146
Pyrene 0.0500 0.0449 89.8 52.0-120
1,2,4-Trichlorobenzene 0.0500 0.0347 69.4 44.0-142
4-Chloro-3-methylphenol 0.0500 0.0423 84.6 22.0-147
2-Chlorophenol 0.0500 0.0337 67.4 23.0-134
2,4-Dichlorophenol 0.0500 0.0384 76.8 39.0-135
2,4-Dimethylphenol 0.0500 0.0357 71.4 32.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0645 129 1.00-181
2,4-Dinitrophenol 0.0500 0.0667 133 1.00-191
2-Nitrophenol 0.0500 0.0392 78.4 29.0-182
4-Nitrophenol 0.0500 0.0241 48.2 1.00-132
Pentachlorophenol 0.0500 0.0462 92.4 14.0-176
Phenol 0.0500 0.0161 32.2 5.00-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1994855
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577056-01,02
Laboratory Control Sample (LCS)
(LCS) R3884839-1 01/26/23 15:51
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,4,6-Trichlorophenol 0.0500 0.0470 94.0 37.0-144
(S) 2-Fluorophenol 45.6 10.0-120
(S) Phenol-d5 32.0 8.00-424
(S) Nitrobenzene-d5 83.8 15.0-314
(S) 2-Fluorobiphenyl 79.3 22.0-127
(S) 2,4,6-Tribromophenol 93.0 10.0-153
(S) p-Terphenyl-d14 87.4 29.0-141
L1578856-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1578856-03 01/26/23 17:59 • (MS) R3884839-3 01/26/23 18:21 • (MSD) R3884839-4 01/26/23 18:42
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 ND 0.0294 0.0368 58.8 73.6 1 47.0-145 22.4 48
Acenaphthylene 0.0500 ND 0.0314 0.0393 62.8 78.6 1 33.0-145 22.3 74
Anthracene 0.0500 ND 0.0328 0.0407 65.6 81.4 1 27.0-133 21.5 66
Benzidine 0.100 ND 0.0334 0.0540 33.4 54.0 1 1.00-120 J3 47.1 40
Benzo(a)anthracene 0.0500 ND 0.0425 0.0481 85.0 96.2 1 33.0-143 12.4 53
Benzo(b)fluoranthene 0.0500 ND 0.0390 0.0442 78.0 88.4 1 24.0-159 12.5 71
Benzo(k)fluoranthene 0.0500 ND 0.0363 0.0409 72.6 81.8 1 11.0-162 11.9 63
Benzo(g,h,i)perylene 0.0500 ND 0.0404 0.0448 80.8 89.6 1 1.00-219 10.3 97
Benzo(a)pyrene 0.0500 ND 0.0394 0.0448 78.8 89.6 1 17.0-163 12.8 72
Bis(2-chlorethoxy)methane 0.0500 ND 0.0257 0.0310 51.4 62.0 1 33.0-184 18.7 54
Bis(2-chloroethyl)ether 0.0500 ND 0.0254 0.0316 50.8 63.2 1 12.0-158 21.8 108
2,2-oxybis(1-chloropropane) 0.0500 ND 0.0250 0.0303 50.0 60.6 1 36.0-166 19.2 76
4-Bromophenyl-phenylether 0.0500 ND 0.0400 0.0499 80.0 99.8 1 53.0-127 22.0 43
2-Chloronaphthalene 0.0500 ND 0.0267 0.0331 53.4 66.2 1 60.0-120 J6 21.4 24
4-Chlorophenyl-phenylether 0.0500 ND 0.0338 0.0420 67.6 84.0 1 25.0-158 21.6 61
Chrysene 0.0500 ND 0.0400 0.0452 80.0 90.4 1 17.0-168 12.2 87
Dibenz(a,h)anthracene 0.0500 ND 0.0429 0.0484 85.8 96.8 1 1.00-227 12.0 126
3,3-Dichlorobenzidine 0.100 ND 0.0695 0.0851 69.5 85.1 1 1.00-262 20.2 108
2,4-Dinitrotoluene 0.0500 ND 0.0399 0.0494 79.8 98.8 1 39.0-139 21.3 42
2,6-Dinitrotoluene 0.0500 ND 0.0354 0.0442 70.8 88.4 1 50.0-158 22.1 48
1,2-Diphenylhydrazine 0.0500 ND 0.0389 0.0475 77.8 95.0 1 18.0-156 N2 N2 19.9 34
Fluoranthene 0.0500 ND 0.0432 0.0513 86.4 103 1 26.0-137 17.1 66
Fluorene 0.0500 ND 0.0328 0.0414 65.6 82.8 1 59.0-121 23.2 38
Hexachlorobenzene 0.0500 ND 0.0338 0.0412 67.6 82.4 1 1.00-152 19.7 55
Hexachloro-1,3-butadiene 0.0500 ND 0.0239 0.0303 47.8 60.6 1 24.0-120 23.6 62
Hexachlorocyclopentadiene 0.0500 ND 0.0157 0.0207 31.4 41.4 1 10.0-146 27.5 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1994855
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577056-01,02
L1578856-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1578856-03 01/26/23 17:59 • (MS) R3884839-3 01/26/23 18:21 • (MSD) R3884839-4 01/26/23 18:42
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexachloroethane 0.0500 ND 0.0223 0.0280 44.6 56.0 1 40.0-120 22.7 52
Indeno(1,2,3-cd)pyrene 0.0500 ND 0.0402 0.0453 80.4 90.6 1 1.00-171 11.9 99
Isophorone 0.0500 ND 0.0269 0.0322 53.8 64.4 1 21.0-196 17.9 93
Naphthalene 0.0500 ND 0.0217 0.0271 43.4 54.2 1 21.0-133 22.1 65
Nitrobenzene 0.0500 ND 0.0266 0.0332 53.2 66.4 1 35.0-180 22.1 62
n-Nitrosodimethylamine 0.0500 ND 0.0248 0.0252 49.6 50.4 1 10.0-120 1.60 40
n-Nitrosodiphenylamine 0.0500 ND 0.0275 0.0350 55.0 70.0 1 16.0-160 24.0 28
n-Nitrosodi-n-propylamine 0.0500 ND 0.0302 0.0376 60.4 75.2 1 1.00-230 21.8 87
Phenanthrene 0.0500 ND 0.0344 0.0428 68.8 85.6 1 54.0-120 21.8 39
Benzylbutyl phthalate 0.0500 ND 0.0391 0.0452 78.2 90.4 1 1.00-152 14.5 60
Bis(2-ethylhexyl)phthalate 0.0500 ND 0.0379 0.0426 75.8 85.2 1 8.00-158 11.7 82
Di-n-butyl phthalate 0.0500 ND 0.0428 0.0506 85.6 101 1 1.00-120 16.7 47
Diethyl phthalate 0.0500 ND 0.0399 0.0495 79.8 99.0 1 1.00-120 21.5 100
Dimethyl phthalate 0.0500 ND 0.0367 0.0452 73.4 90.4 1 1.00-120 20.8 183
Di-n-octyl phthalate 0.0500 ND 0.0437 0.0487 87.4 97.4 1 4.00-146 10.8 69
Pyrene 0.0500 ND 0.0369 0.0425 73.8 85.0 1 52.0-120 14.1 49
1,2,4-Trichlorobenzene 0.0500 ND 0.0218 0.0275 43.6 55.0 1 44.0-142 J6 23.1 50
4-Chloro-3-methylphenol 0.0500 ND 0.0296 0.0363 59.2 72.6 1 22.0-147 20.3 73
2-Chlorophenol 0.0500 ND 0.0198 0.0251 39.6 50.2 1 23.0-134 23.6 61
2,4-Dichlorophenol 0.0500 ND 0.0242 0.0309 48.4 61.8 1 39.0-135 24.3 50
2,4-Dimethylphenol 0.0500 ND 0.0233 0.0284 46.6 56.8 1 32.0-120 19.7 58
4,6-Dinitro-2-methylphenol 0.0500 ND 0.0516 0.0615 103 123 1 1.00-181 17.5 203
2,4-Dinitrophenol 0.0500 ND 0.0521 0.0615 104 123 1 1.00-191 16.5 132
2-Nitrophenol 0.0500 ND 0.0255 0.0316 51.0 63.2 1 29.0-182 21.4 55
4-Nitrophenol 0.0500 ND 0.0184 0.0194 36.8 38.8 1 1.00-132 5.29 131
Pentachlorophenol 0.0500 ND 0.0368 0.0457 73.6 91.4 1 14.0-176 21.6 86
Phenol 0.0500 ND 0.0107 0.0121 21.4 24.2 1 5.00-120 12.3 64
2,4,6-Trichlorophenol 0.0500 ND 0.0315 0.0393 63.0 78.6 1 37.0-144 22.0 58
(S) 2-Fluorophenol 28.7 35.1 10.0-120
(S) Phenol-d5 20.2 22.9 8.00-424
(S) Nitrobenzene-d5 53.9 65.0 15.0-314
(S) 2-Fluorobiphenyl 49.2 60.8 22.0-127
(S) 2,4,6-Tribromophenol 72.5 84.0 10.0-153
(S) p-Terphenyl-d14 74.2 84.3 29.0-141
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
N2 Analyte reported using a calibration and validation based on Azobenzene (CAS 103-33-3). 1,2-Diphenylhydrazine
decomposes into Azobenzene during the analysis.
T8 Sample(s) received past/too close to holding time expiration.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577056 01/30/23 11:15 36 of 38
ANALYTICAL REPORT
January 26, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1577067
Samples Received:01/18/2023
Project Number:RECYCLED EARTH
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
January 26, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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January 26, 2023
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577067 01/26/23 16:57 1 of 21
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Gl: Glossary of Terms 5
Al: Accreditations & Locations 6
Sc: Sample Chain of Custody 7
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SITE-SOUTH L1577067-01 WW Anna Rasmuson 01/17/23 13:00 01/18/23 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Subcontracted Analyses WG1990821 1 01/26/23 00:00 01/26/23 00:00 -Minneapolis, MN
55414
Collected by Collected date/time Received date/time
SITE-NORTH L1577067-02 WW Anna Rasmuson 01/17/23 12:30 01/18/23 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Subcontracted Analyses WG1990821 1 01/26/23 00:00 01/26/23 00:00 -Minneapolis, MN
55414
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Project Narrative
L1577067 -01, -02 contains subout data that is included after the chain of custody.
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577067 01/26/23 16:57 4 of 21
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
SDG Sample Delivery Group.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577067 01/26/23 16:48 6 of 21
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577067 01/26/23 16:57 6 of 21
Thisreportshould notbe reproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamples included inthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,LLC.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
Client Services
Pace Analytical National
12065 Lebanon Rd
Mt. Juliet TN 37122
REPORT OF
LABORATORY
ANALYSIS FOR
TCDD
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
January 26, 2023
Pace Project #:10640332
Sample Receipt Date:01/19/2023
Client Project #:L1577067 WG1990821
Client Sub PO #:L1577067
The report provided has been invoiced as a Level 2
2,3,7,8-TCDD Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questions to Kongmeng Vang,your Pace
Project Manager.
State Cert #:N/A
Report Prepared for:
Page 1 of 14Report No.....10640332_SW8290TCDD_L2_dfr
January 26, 2023
Kongmeng Vang, Project Manager
[phone]
[phone] (fax)
[e-mail]
Pace Analytical Services,LLC.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
This report presents the results from the analyses performed on two samples submitted
by a representative of Pace Analytical National. The samples were analyzed for the
presence or absence of 2,3,7,8-tetrachlorodibenzo-p-dioxin (2,3,7,8-TCDD) using a
modified version of USEPA Method 8290. The reporting limits were set to correspond
to the lowest calibration point and a nominal 1-Liter sample amount, and the sensitivity
was verified by signal-to-noise measurements. The quantitation limits, adjusted for
sample extraction amount, may be somewhat higher or lower than the reporting limits
provided in this report.
The recoveries of the isotopically-labeled TCDD internal standard in the sample
extracts ranged from 40-64%. Except for one low value, which was flagged "R" on the
results table, the labeled internal standard recoveries obtained for this project were
within the 40-135% target range specified in Method 8290. Also, since the
quantification of the native TCDD was based on isotope dilution, the data were
automatically corrected for recovery and accurate values were obtained.
A laboratory method blank was prepared and analyzed with each sample batch as part
of our routine quality control procedures. The results show the blanks to be free of
2,3,7,8-TCDD at the reporting limit.
Laboratory spike samples were also prepared using clean reference matrix that had
been fortified with native standard material. The results show that the spiked native
TCDD was recovered at 104-111% with a relative percent difference of 6.5%. These
results were within the target ranges for the method. Matrix spikes were not prepared
with the sample batch.
DISCUSSION
Page 2 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Report No.....10640332
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 14Report No.....10640332_SW8290TCDD_L2_dfr
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14Report No.....10640332_SW8290TCDD_L2_dfr
Pa
g
e

5

o
f

1
4
Re
p
o
r
t

N
o
.
.
.
.
.
1
0
6
4
0
3
3
2
_
S
W
8
2
9
0
T
C
D
D
_
L
2
_
d
f
r
Page 6 of 14Report No.....10640332_SW8290TCDD_L2_dfr
1/19/23
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
A =

B =

C =

D =

E =

H2 =

I =

J =

L =

Nn =

P =

R =

S =

U =

V =

X =

Y =

* =
Reporting Limit based on signal to noise (EDL)

Less than 10x higher than method blank level

Result obtained from confirmation analysis

Result obtained from analysis of diluted sample

Exceeds calibration range

Extracted outside of holding time

Isotope ratio out of specification

Estimated value

Suppressive interference, analyte may be biased low

Value obtained from additional analysis

PCDE Interference

Recovery outside target range

Peak saturated

Analyte not detected

Result verified by confirmation analysis

%D Exceeds limits

Calculated using average of daily RFs

See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 14Report No.....10640332_SW8290TCDD_L2_dfr
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
% Moisture
Dry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID SITE-SOUTH
10640332001
U230124B_12
SMT
NA
1020 mL
NA
U221005
U230124A_16 & U230124B_16
BLANK-103673
Matrix
Dilution
Collected
Received
Extracted
Analyzed
Water
NA
01/17/2023 13:00
01/19/2023 08:50
01/20/2023 11:30
01/25/2023 08:57
Client - Pace Analytical National
Method 8290 Sample Analysis Results
NativeIsomers Conc
pg/L pg/L
InternalStandards Addedng's PercentRecoveryEMPC
pg/L
RL
2,3,7,8-TCDD ND 10 2,3,7,8-TCDD-13C 2.00 64-----
Recovery Standard1,2,3,4-TCDD-13C 2.00 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 76
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
R=Recovery outside target range
E=Exceeds calibration range
RL = Reporting Limit
Page 9 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
% Moisture
Dry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID SITE-NORTH
10640332002
U230124B_13
SMT
NA
1020 mL
NA
U221005
U230124A_16 & U230124B_16
BLANK-103673
Matrix
Dilution
Collected
Received
Extracted
Analyzed
Water
NA
01/17/2023 12:30
01/19/2023 08:50
01/20/2023 11:30
01/25/2023 09:44
Client - Pace Analytical National
Method 8290 Sample Analysis Results
NativeIsomers Conc
pg/L pg/L
InternalStandards Addedng's PercentRecoveryEMPC
pg/L
RL
2,3,7,8-TCDD ND 10 2,3,7,8-TCDD-13C 2.00 40-----
Recovery Standard1,2,3,4-TCDD-13C 2.00 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 48
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
R=Recovery outside target range
E=Exceeds calibration range
RL = Reporting Limit
Page 10 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL ID
CCal Filename(s)
BLANK-103673
U230124B_09
SMT
979 mL
U221005
U230124A_16 & U230124B_16
Matrix
Dilution
Extracted
Analyzed
Water
01/20/2023 11:30
01/25/2023 06:39
NA
Method 8290 Blank Analysis Results
Lab Sample Name DFBLKMT
NativeIsomers pg/L
Conc EMPC
pg/L pg/L
InternalStandards Addedng's PercentRecoveryRL
2,3,7,8-TCDD ND -----10 2,3,7,8-TCDD-13C 2.00 61
Recovery Standard1,2,3,4-TCDD-13C 2.00 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 75
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC =Estimated Maximum Possible Concentration
R =Recovery outside target range
E =Exceeds calibration range
RL =Reporting Limit
Page 11 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL ID
CCal Filename(s)
LCS-103674
L230125A_17
SMT
1010 mL
L220811
L230125A_01 & L230125A_19
Matrix
Dilution
Extracted
Analyzed
Water
01/20/2023 11:30
01/25/2023 21:09
NA
Method Blank ID BLANK-103673
Method 8290 Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDD 0.20 0.21 2,3,7,8-TCDD-13C 2.0 36104 R
Recovery Standard1,2,3,4-TCDD-13C 2.0 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 45
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressed as Percent)
R=Recovery outside of target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
* =See Discussion
Page 12 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL ID
CCal Filename(s)
LCSD-103675
L230125B_13
SMT
995 mL
L220811
L230125A_19 & L230125B_14
Matrix
Dilution
Extracted
Analyzed
Water
01/20/2023 11:30
01/26/2023 07:31
NA
Method Blank ID BLANK-103673
Method 8290 Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDD 0.20 0.22 2,3,7,8-TCDD-13C 2.0 48111
Recovery Standard1,2,3,4-TCDD-13C 2.0 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 56
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressed as Percent)
R=Recovery outside of target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
* =See Discussion
Page 13 of 14Report No.....10640332_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Client
Spike 1 ID
Spike 1 Filename L230125A_17
LCS-103674
Pace Analytical National
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 ID
Spike 2 Filename L230125B_13
LCSD-103675
Method 8290
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDD 104 111 6.5
%REC = Percent Recovered
RPD =The difference between the two values divided by the mean value
Page 14 of 14Report No.....10640332_SW8290TCDD_L2_dfr
ANALYTICAL REPORT
January 27, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1577038
Samples Received:01/18/2023
Project Number:RECYCLED EARTH
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
January 27, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 1 of 39
January 27, 2023
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 1 of 39
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SE-POND L1577038-01 5
OUTFALL #1 L1577038-02 9
Qc: Quality Control Summary 13
Gravimetric Analysis by Method 2540 C-2011 13
Gravimetric Analysis by Method 2540 D-2015 14
Wet Chemistry by Method 1664A 15
Wet Chemistry by Method 410.4 16
Wet Chemistry by Method 4500H+ B-2011 17
Mercury by Method 245.1 18
Metals (ICP) by Method 200.7 19
Volatile Organic Compounds (GC) by Method 8015D/GRO 22
Volatile Organic Compounds (GC/MS) by Method 624.1 23
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 25
Pesticides (GC) by Method EPA 608.3 26
Polychlorinated Biphenyls (GC) by Method EPA-608.3 29
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 30
Gl: Glossary of Terms 35
Al: Accreditations & Locations 36
Sc: Sample Chain of Custody 37
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 2 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 2 of 39
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SE-POND L1577038-01 WW Anna Rasmuson 01/17/23 11:45 01/18/23 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1991110 1 01/19/23 09:10 01/19/23 10:25 AS Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015 WG1990901 1 01/18/23 16:38 01/18/23 18:56 AS Mt. Juliet, TN
Wet Chemistry by Method 1664A WG1990838 1 01/19/23 00:03 01/19/23 14:59 WAW Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG1991163 1 01/19/23 14:18 01/19/23 16:43 NEF Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011 WG1991157 1 01/19/23 18:00 01/19/23 18:00 KAD Mt. Juliet, TN
Mercury by Method 245.1 WG1990811 1 01/18/23 18:45 01/19/23 09:06 SRT Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1990808 1 01/19/23 10:42 01/19/23 20:53 ABL Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1991929 1 01/20/23 12:24 01/23/23 12:53 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1991047 1 01/19/23 01:40 01/19/23 01:40 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1991291 5 01/19/23 14:21 01/19/23 14:21 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG1991076 2 01/19/23 07:10 01/19/23 18:23 MAA Mt. Juliet, TN
Pesticides (GC) by Method EPA 608.3 WG1991021 1 01/19/23 22:58 01/20/23 11:56 AMM Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method EPA-608.3 WG1991021 1 01/19/23 22:58 01/20/23 11:56 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1991022 1 01/20/23 13:37 01/23/23 12:22 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
OUTFALL #1 L1577038-02 WW Anna Rasmuson 01/17/23 13:20 01/18/23 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1991110 1 01/19/23 09:10 01/19/23 10:25 AS Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015 WG1990901 1 01/18/23 16:38 01/18/23 18:56 AS Mt. Juliet, TN
Wet Chemistry by Method 1664A WG1990838 1 01/19/23 00:03 01/19/23 14:59 WAW Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG1991163 1 01/19/23 14:18 01/19/23 16:43 NEF Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011 WG1991157 1 01/19/23 18:00 01/19/23 18:00 KAD Mt. Juliet, TN
Mercury by Method 245.1 WG1990811 1 01/18/23 18:45 01/19/23 09:08 SRT Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1990808 1 01/19/23 10:42 01/19/23 20:55 ABL Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG1991929 1 01/20/23 12:24 01/23/23 12:55 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1991047 1 01/19/23 02:01 01/19/23 02:01 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1991291 5 01/19/23 14:40 01/19/23 14:40 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG1991076 1 01/19/23 07:10 01/19/23 19:03 MAA Mt. Juliet, TN
Pesticides (GC) by Method EPA 608.3 WG1991021 1 01/19/23 22:58 01/20/23 12:05 AMM Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method EPA-608.3 WG1991021 1 01/19/23 22:58 01/20/23 12:05 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1991022 1 01/20/23 13:37 01/21/23 19:45 CCW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1991022 1 01/20/23 13:37 01/23/23 12:43 CCW Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 3 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 3 of 39
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 4 of 39
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 4 of 39
SAMPLE RESULTS - 01
L1577038
SE-POND
Collected date/time: 01/17/23 11:45
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 772 20.0 1 01/19/2023 10:25 WG1991110
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 8.70 2.50 1 01/18/2023 18:56 WG1990901
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.26 1 01/19/2023 14:59 WG1990838
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 71.3 20.0 1 01/19/2023 16:43 WG1991163
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 10.0 T8 1 01/19/2023 18:00 WG1991157
Sample Narrative:
L1577038-01 WG1991157: 10.02 at 18.9C
Mercury by Method 245.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 01/19/2023 09:06 WG1990811
Metals (ICP) by Method 200.7
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aluminum ND 0.200 1 01/23/2023 12:53 WG1991929
Arsenic 0.0215 0.0100 1 01/19/2023 20:53 WG1990808
Barium 0.100 0.00500 1 01/19/2023 20:53 WG1990808
Beryllium ND 0.00200 1 01/19/2023 20:53 WG1990808
Cadmium ND 0.00200 1 01/19/2023 20:53 WG1990808
Chromium ND 0.0100 1 01/23/2023 12:53 WG1991929
Copper 0.0233 0.0100 1 01/19/2023 20:53 WG1990808
Iron 0.300 0.100 1 01/19/2023 20:53 WG1990808
Lead ND 0.00500 1 01/19/2023 20:53 WG1990808
Selenium ND 0.0100 1 01/19/2023 20:53 WG1990808
Silver ND 0.00500 1 01/23/2023 12:53 WG1991929
Zinc ND 0.0500 1 01/23/2023 12:53 WG1991929
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 01/19/2023 01:40 WG1991047
(S) a,a,a-Trifluorotoluene(FID) 102 78.0-120 01/19/2023 01:40 WG1991047
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 5 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 5 of 39
SAMPLE RESULTS - 01
L1577038
SE-POND
Collected date/time: 01/17/23 11:45
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acrolein ND J3 0.250 5 01/19/2023 14:21 WG1991291
Acrylonitrile ND 0.0500 5 01/19/2023 14:21 WG1991291
Benzene ND 0.00500 5 01/19/2023 14:21 WG1991291
Bromodichloromethane ND 0.00500 5 01/19/2023 14:21 WG1991291
Bromoform ND 0.00500 5 01/19/2023 14:21 WG1991291
Bromomethane ND 0.0250 5 01/19/2023 14:21 WG1991291
Carbon tetrachloride ND 0.00500 5 01/19/2023 14:21 WG1991291
Chlorobenzene ND 0.00500 5 01/19/2023 14:21 WG1991291
Chlorodibromomethane ND 0.00500 5 01/19/2023 14:21 WG1991291
Chloroethane ND 0.0250 5 01/19/2023 14:21 WG1991291
2-Chloroethyl vinyl ether ND 0.250 5 01/19/2023 14:21 WG1991291
Chloroform ND 0.0250 5 01/19/2023 14:21 WG1991291
Chloromethane ND 0.0125 5 01/19/2023 14:21 WG1991291
1,2-Dichlorobenzene ND 0.00500 5 01/19/2023 14:21 WG1991291
1,3-Dichlorobenzene ND 0.00500 5 01/19/2023 14:21 WG1991291
1,4-Dichlorobenzene ND 0.00500 5 01/19/2023 14:21 WG1991291
Dichlorodifluoromethane ND 0.0250 5 01/19/2023 14:21 WG1991291
1,1-Dichloroethane ND 0.00500 5 01/19/2023 14:21 WG1991291
1,2-Dichloroethane ND 0.00500 5 01/19/2023 14:21 WG1991291
1,1-Dichloroethene ND 0.00500 5 01/19/2023 14:21 WG1991291
trans-1,2-Dichloroethene ND 0.00500 5 01/19/2023 14:21 WG1991291
1,2-Dichloropropane ND 0.00500 5 01/19/2023 14:21 WG1991291
cis-1,3-Dichloropropene ND 0.00500 5 01/19/2023 14:21 WG1991291
trans-1,3-Dichloropropene ND 0.00500 5 01/19/2023 14:21 WG1991291
Ethylbenzene ND 0.00500 5 01/19/2023 14:21 WG1991291
Methylene Chloride ND 0.0250 5 01/19/2023 14:21 WG1991291
Methyl tert-butyl ether ND 0.00500 5 01/19/2023 14:21 WG1991291
1,1,2,2-Tetrachloroethane ND 0.00500 5 01/19/2023 14:21 WG1991291
Tetrachloroethene ND 0.00500 5 01/19/2023 14:21 WG1991291
Toluene ND 0.00500 5 01/19/2023 14:21 WG1991291
1,1,1-Trichloroethane ND 0.00500 5 01/19/2023 14:21 WG1991291
1,1,2-Trichloroethane ND 0.00500 5 01/19/2023 14:21 WG1991291
Trichloroethene ND 0.00500 5 01/19/2023 14:21 WG1991291
Trichlorofluoromethane ND 0.0250 5 01/19/2023 14:21 WG1991291
Vinyl chloride ND 0.00500 5 01/19/2023 14:21 WG1991291
Total Xylenes ND 0.0150 5 01/19/2023 14:21 WG1991291
(S) Toluene-d8 106 80.0-120 01/19/2023 14:21 WG1991291
(S) 4-Bromofluorobenzene 106 80.0-120 01/19/2023 14:21 WG1991291
(S) 1,2-Dichloroethane-d4 107 70.0-130 01/19/2023 14:21 WG1991291
Sample Narrative:
L1577038-01 WG1991291: Lowest possible dilution due to sample foaming.
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 0.804 0.200 2 01/19/2023 18:23 WG1991076
(S) o-Terphenyl 93.5 31.0-160 01/19/2023 18:23 WG1991076
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 6 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 6 of 39
SAMPLE RESULTS - 01
L1577038
SE-POND
Collected date/time: 01/17/23 11:45
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aldrin ND 0.0000500 1 01/20/2023 11:56 WG1991021
Alpha BHC ND 0.0000500 1 01/20/2023 11:56 WG1991021
Beta BHC ND 0.0000500 1 01/20/2023 11:56 WG1991021
Delta BHC ND 0.0000500 1 01/20/2023 11:56 WG1991021
Gamma BHC ND 0.0000500 1 01/20/2023 11:56 WG1991021
Chlordane ND 0.00500 1 01/20/2023 11:56 WG1991021
4,4-DDD ND 0.0000500 1 01/20/2023 11:56 WG1991021
4,4-DDE ND 0.0000500 1 01/20/2023 11:56 WG1991021
4,4-DDT ND 0.0000500 1 01/20/2023 11:56 WG1991021
Dieldrin ND 0.0000500 1 01/20/2023 11:56 WG1991021
Endosulfan I ND 0.0000500 1 01/20/2023 11:56 WG1991021
Endosulfan II ND 0.0000500 1 01/20/2023 11:56 WG1991021
Endosulfan sulfate ND 0.0000500 1 01/20/2023 11:56 WG1991021
Endrin ND 0.0000500 1 01/20/2023 11:56 WG1991021
Endrin aldehyde ND 0.0000500 1 01/20/2023 11:56 WG1991021
Endrin ketone ND 0.0000500 1 01/20/2023 11:56 WG1991021
Heptachlor ND 0.0000500 1 01/20/2023 11:56 WG1991021
Heptachlor epoxide ND 0.0000500 1 01/20/2023 11:56 WG1991021
Hexachlorobenzene ND 0.0000500 1 01/20/2023 11:56 WG1991021
Methoxychlor ND 0.0000500 1 01/20/2023 11:56 WG1991021
Toxaphene ND 0.000500 1 01/20/2023 11:56 WG1991021
gamma-Chlordane ND 0.0000500 1 01/20/2023 11:56 WG1991021
alpha-Chlordane ND 0.0000500 1 01/20/2023 11:56 WG1991021
(S) Decachlorobiphenyl 49.7 10.0-144 01/20/2023 11:56 WG1991021
(S) Tetrachloro-m-xylene 52.8 10.0-135 01/20/2023 11:56 WG1991021
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 01/20/2023 11:56 WG1991021
PCB 1221 ND 0.000500 1 01/20/2023 11:56 WG1991021
PCB 1232 ND 0.000500 1 01/20/2023 11:56 WG1991021
PCB 1242 ND 0.000500 1 01/20/2023 11:56 WG1991021
PCB 1248 ND 0.000500 1 01/20/2023 11:56 WG1991021
PCB 1254 ND 0.000500 1 01/20/2023 11:56 WG1991021
PCB 1260 ND 0.000500 1 01/20/2023 11:56 WG1991021
Total PCBs ND 0.000500 1 01/20/2023 11:56 WG1991021
(S) Decachlorobiphenyl 59.8 10.0-144 01/20/2023 11:56 WG1991021
(S) Tetrachloro-m-xylene 59.6 10.0-135 01/20/2023 11:56 WG1991021
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 01/23/2023 12:22 WG1991022
Acenaphthylene ND 0.00100 1 01/23/2023 12:22 WG1991022
Anthracene ND 0.00100 1 01/23/2023 12:22 WG1991022
Benzidine ND 0.0100 1 01/23/2023 12:22 WG1991022
Benzo(a)anthracene ND 0.00100 1 01/23/2023 12:22 WG1991022
Benzo(b)fluoranthene ND 0.00100 1 01/23/2023 12:22 WG1991022
Benzo(k)fluoranthene ND 0.00100 1 01/23/2023 12:22 WG1991022
Benzo(g,h,i)perylene ND 0.00100 1 01/23/2023 12:22 WG1991022
Benzo(a)pyrene ND 0.00100 1 01/23/2023 12:22 WG1991022
Bis(2-chlorethoxy)methane ND 0.0100 1 01/23/2023 12:22 WG1991022
Bis(2-chloroethyl)ether ND 0.0100 1 01/23/2023 12:22 WG1991022
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 01/23/2023 12:22 WG1991022
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 7 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 7 of 39
SAMPLE RESULTS - 01
L1577038
SE-POND
Collected date/time: 01/17/23 11:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
4-Bromophenyl-phenylether ND 0.0100 1 01/23/2023 12:22 WG1991022
2-Chloronaphthalene ND 0.00100 1 01/23/2023 12:22 WG1991022
4-Chlorophenyl-phenylether ND 0.0100 1 01/23/2023 12:22 WG1991022
Chrysene ND 0.00100 1 01/23/2023 12:22 WG1991022
Dibenz(a,h)anthracene ND 0.00100 1 01/23/2023 12:22 WG1991022
3,3-Dichlorobenzidine ND 0.0100 1 01/23/2023 12:22 WG1991022
2,4-Dinitrotoluene ND 0.0100 1 01/23/2023 12:22 WG1991022
2,6-Dinitrotoluene ND 0.0100 1 01/23/2023 12:22 WG1991022
1,2-Diphenylhydrazine ND N2 0.0100 1 01/23/2023 12:22 WG1991022
Fluoranthene ND 0.00100 1 01/23/2023 12:22 WG1991022
Fluorene ND 0.00100 1 01/23/2023 12:22 WG1991022
Hexachlorobenzene ND 0.00100 1 01/23/2023 12:22 WG1991022
Hexachloro-1,3-butadiene ND 0.0100 1 01/23/2023 12:22 WG1991022
Hexachlorocyclopentadiene ND 0.0100 1 01/23/2023 12:22 WG1991022
Hexachloroethane ND 0.0100 1 01/23/2023 12:22 WG1991022
Indeno(1,2,3-cd)pyrene ND 0.00100 1 01/23/2023 12:22 WG1991022
Isophorone ND 0.0100 1 01/23/2023 12:22 WG1991022
Naphthalene ND 0.00100 1 01/23/2023 12:22 WG1991022
Nitrobenzene ND 0.0100 1 01/23/2023 12:22 WG1991022
n-Nitrosodimethylamine ND 0.0100 1 01/23/2023 12:22 WG1991022
n-Nitrosodiphenylamine ND 0.0100 1 01/23/2023 12:22 WG1991022
n-Nitrosodi-n-propylamine ND 0.0100 1 01/23/2023 12:22 WG1991022
Phenanthrene ND 0.00100 1 01/23/2023 12:22 WG1991022
Benzylbutyl phthalate ND 0.00300 1 01/23/2023 12:22 WG1991022
Bis(2-ethylhexyl)phthalate ND 0.00300 1 01/23/2023 12:22 WG1991022
Di-n-butyl phthalate 0.00400 0.00300 1 01/23/2023 12:22 WG1991022
Diethyl phthalate ND 0.00300 1 01/23/2023 12:22 WG1991022
Dimethyl phthalate ND 0.00300 1 01/23/2023 12:22 WG1991022
Di-n-octyl phthalate ND 0.00300 1 01/23/2023 12:22 WG1991022
Pyrene ND 0.00100 1 01/23/2023 12:22 WG1991022
1,2,4-Trichlorobenzene ND 0.0100 1 01/23/2023 12:22 WG1991022
4-Chloro-3-methylphenol ND 0.0100 1 01/23/2023 12:22 WG1991022
2-Chlorophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
2,4-Dichlorophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
2,4-Dimethylphenol ND 0.0100 1 01/23/2023 12:22 WG1991022
4,6-Dinitro-2-methylphenol ND 0.0100 1 01/23/2023 12:22 WG1991022
2,4-Dinitrophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
2-Nitrophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
4-Nitrophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
Pentachlorophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
Phenol ND 0.0100 1 01/23/2023 12:22 WG1991022
2,4,6-Trichlorophenol ND 0.0100 1 01/23/2023 12:22 WG1991022
(S) 2-Fluorophenol 41.5 10.0-120 01/23/2023 12:22 WG1991022
(S) Phenol-d5 26.6 8.00-424 01/23/2023 12:22 WG1991022
(S) Nitrobenzene-d5 60.9 15.0-314 01/23/2023 12:22 WG1991022
(S) 2-Fluorobiphenyl 78.6 22.0-127 01/23/2023 12:22 WG1991022
(S) 2,4,6-Tribromophenol 105 10.0-153 01/23/2023 12:22 WG1991022
(S) p-Terphenyl-d14 87.4 29.0-141 01/23/2023 12:22 WG1991022
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 8 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 8 of 39
SAMPLE RESULTS - 02
L1577038
OUTFALL #1
Collected date/time: 01/17/23 13:20
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 576 13.3 1 01/19/2023 10:25 WG1991110
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 21.4 2.50 1 01/18/2023 18:56 WG1990901
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.75 1 01/19/2023 14:59 WG1990838
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 55.3 20.0 1 01/19/2023 16:43 WG1991163
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 10.1 T8 1 01/19/2023 18:00 WG1991157
Sample Narrative:
L1577038-02 WG1991157: 10.08 at 18.6C
Mercury by Method 245.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 01/19/2023 09:08 WG1990811
Metals (ICP) by Method 200.7
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aluminum ND 0.200 1 01/23/2023 12:55 WG1991929
Arsenic 0.0134 0.0100 1 01/19/2023 20:55 WG1990808
Barium 0.0471 0.00500 1 01/19/2023 20:55 WG1990808
Beryllium ND 0.00200 1 01/19/2023 20:55 WG1990808
Cadmium ND 0.00200 1 01/19/2023 20:55 WG1990808
Chromium 0.0129 0.0100 1 01/23/2023 12:55 WG1991929
Copper 0.0334 0.0100 1 01/19/2023 20:55 WG1990808
Iron 0.240 0.100 1 01/19/2023 20:55 WG1990808
Lead ND 0.00500 1 01/19/2023 20:55 WG1990808
Selenium ND 0.0100 1 01/19/2023 20:55 WG1990808
Silver ND 0.00500 1 01/23/2023 12:55 WG1991929
Zinc ND 0.0500 1 01/23/2023 12:55 WG1991929
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 01/19/2023 02:01 WG1991047
(S) a,a,a-Trifluorotoluene(FID) 101 78.0-120 01/19/2023 02:01 WG1991047
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 9 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 9 of 39
SAMPLE RESULTS - 02
L1577038
OUTFALL #1
Collected date/time: 01/17/23 13:20
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acrolein ND J3 0.250 5 01/19/2023 14:40 WG1991291
Acrylonitrile ND 0.0500 5 01/19/2023 14:40 WG1991291
Benzene ND 0.00500 5 01/19/2023 14:40 WG1991291
Bromodichloromethane ND 0.00500 5 01/19/2023 14:40 WG1991291
Bromoform ND 0.00500 5 01/19/2023 14:40 WG1991291
Bromomethane ND 0.0250 5 01/19/2023 14:40 WG1991291
Carbon tetrachloride ND 0.00500 5 01/19/2023 14:40 WG1991291
Chlorobenzene ND 0.00500 5 01/19/2023 14:40 WG1991291
Chlorodibromomethane ND 0.00500 5 01/19/2023 14:40 WG1991291
Chloroethane ND 0.0250 5 01/19/2023 14:40 WG1991291
2-Chloroethyl vinyl ether ND 0.250 5 01/19/2023 14:40 WG1991291
Chloroform ND 0.0250 5 01/19/2023 14:40 WG1991291
Chloromethane ND 0.0125 5 01/19/2023 14:40 WG1991291
1,2-Dichlorobenzene ND 0.00500 5 01/19/2023 14:40 WG1991291
1,3-Dichlorobenzene ND 0.00500 5 01/19/2023 14:40 WG1991291
1,4-Dichlorobenzene ND 0.00500 5 01/19/2023 14:40 WG1991291
Dichlorodifluoromethane ND 0.0250 5 01/19/2023 14:40 WG1991291
1,1-Dichloroethane ND 0.00500 5 01/19/2023 14:40 WG1991291
1,2-Dichloroethane ND 0.00500 5 01/19/2023 14:40 WG1991291
1,1-Dichloroethene ND 0.00500 5 01/19/2023 14:40 WG1991291
trans-1,2-Dichloroethene ND 0.00500 5 01/19/2023 14:40 WG1991291
1,2-Dichloropropane ND 0.00500 5 01/19/2023 14:40 WG1991291
cis-1,3-Dichloropropene ND 0.00500 5 01/19/2023 14:40 WG1991291
trans-1,3-Dichloropropene ND 0.00500 5 01/19/2023 14:40 WG1991291
Ethylbenzene ND 0.00500 5 01/19/2023 14:40 WG1991291
Methylene Chloride ND 0.0250 5 01/19/2023 14:40 WG1991291
Methyl tert-butyl ether ND 0.00500 5 01/19/2023 14:40 WG1991291
1,1,2,2-Tetrachloroethane ND 0.00500 5 01/19/2023 14:40 WG1991291
Tetrachloroethene ND 0.00500 5 01/19/2023 14:40 WG1991291
Toluene ND 0.00500 5 01/19/2023 14:40 WG1991291
1,1,1-Trichloroethane ND 0.00500 5 01/19/2023 14:40 WG1991291
1,1,2-Trichloroethane ND 0.00500 5 01/19/2023 14:40 WG1991291
Trichloroethene ND 0.00500 5 01/19/2023 14:40 WG1991291
Trichlorofluoromethane ND 0.0250 5 01/19/2023 14:40 WG1991291
Vinyl chloride ND 0.00500 5 01/19/2023 14:40 WG1991291
Total Xylenes ND 0.0150 5 01/19/2023 14:40 WG1991291
(S) Toluene-d8 108 80.0-120 01/19/2023 14:40 WG1991291
(S) 4-Bromofluorobenzene 110 80.0-120 01/19/2023 14:40 WG1991291
(S) 1,2-Dichloroethane-d4 105 70.0-130 01/19/2023 14:40 WG1991291
Sample Narrative:
L1577038-02 WG1991291: Lowest possible dilution due to sample foaming.
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 1.16 0.100 1 01/19/2023 19:03 WG1991076
(S) o-Terphenyl 99.0 31.0-160 01/19/2023 19:03 WG1991076
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 10:56 10 of 39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 10 of 39
SAMPLE RESULTS - 02
L1577038
OUTFALL #1
Collected date/time: 01/17/23 13:20
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Aldrin ND 0.0000500 1 01/20/2023 12:05 WG1991021
Alpha BHC ND 0.0000500 1 01/20/2023 12:05 WG1991021
Beta BHC ND 0.0000500 1 01/20/2023 12:05 WG1991021
Delta BHC ND 0.0000500 1 01/20/2023 12:05 WG1991021
Gamma BHC ND 0.0000500 1 01/20/2023 12:05 WG1991021
Chlordane ND 0.00500 1 01/20/2023 12:05 WG1991021
4,4-DDD ND 0.0000500 1 01/20/2023 12:05 WG1991021
4,4-DDE ND 0.0000500 1 01/20/2023 12:05 WG1991021
4,4-DDT ND 0.0000500 1 01/20/2023 12:05 WG1991021
Dieldrin ND 0.0000500 1 01/20/2023 12:05 WG1991021
Endosulfan I ND 0.0000500 1 01/20/2023 12:05 WG1991021
Endosulfan II ND 0.0000500 1 01/20/2023 12:05 WG1991021
Endosulfan sulfate ND 0.0000500 1 01/20/2023 12:05 WG1991021
Endrin ND 0.0000500 1 01/20/2023 12:05 WG1991021
Endrin aldehyde ND 0.0000500 1 01/20/2023 12:05 WG1991021
Endrin ketone ND 0.0000500 1 01/20/2023 12:05 WG1991021
Heptachlor ND 0.0000500 1 01/20/2023 12:05 WG1991021
Heptachlor epoxide ND 0.0000500 1 01/20/2023 12:05 WG1991021
Hexachlorobenzene ND 0.0000500 1 01/20/2023 12:05 WG1991021
Methoxychlor ND 0.0000500 1 01/20/2023 12:05 WG1991021
Toxaphene ND 0.000500 1 01/20/2023 12:05 WG1991021
gamma-Chlordane ND 0.0000500 1 01/20/2023 12:05 WG1991021
alpha-Chlordane ND 0.0000500 1 01/20/2023 12:05 WG1991021
(S) Decachlorobiphenyl 56.6 10.0-144 01/20/2023 12:05 WG1991021
(S) Tetrachloro-m-xylene 66.7 10.0-135 01/20/2023 12:05 WG1991021
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 01/20/2023 12:05 WG1991021
PCB 1221 ND 0.000500 1 01/20/2023 12:05 WG1991021
PCB 1232 ND 0.000500 1 01/20/2023 12:05 WG1991021
PCB 1242 ND 0.000500 1 01/20/2023 12:05 WG1991021
PCB 1248 ND 0.000500 1 01/20/2023 12:05 WG1991021
PCB 1254 ND 0.000500 1 01/20/2023 12:05 WG1991021
PCB 1260 ND 0.000500 1 01/20/2023 12:05 WG1991021
Total PCBs ND 0.000500 1 01/20/2023 12:05 WG1991021
(S) Decachlorobiphenyl 67.4 10.0-144 01/20/2023 12:05 WG1991021
(S) Tetrachloro-m-xylene 76.0 10.0-135 01/20/2023 12:05 WG1991021
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 01/21/2023 19:45 WG1991022
Acenaphthylene ND 0.00100 1 01/21/2023 19:45 WG1991022
Anthracene ND 0.00100 1 01/21/2023 19:45 WG1991022
Benzidine ND 0.0100 1 01/21/2023 19:45 WG1991022
Benzo(a)anthracene ND 0.00100 1 01/21/2023 19:45 WG1991022
Benzo(b)fluoranthene ND 0.00100 1 01/21/2023 19:45 WG1991022
Benzo(k)fluoranthene ND 0.00100 1 01/21/2023 19:45 WG1991022
Benzo(g,h,i)perylene ND 0.00100 1 01/21/2023 19:45 WG1991022
Benzo(a)pyrene ND 0.00100 1 01/21/2023 19:45 WG1991022
Bis(2-chlorethoxy)methane ND 0.0100 1 01/21/2023 19:45 WG1991022
Bis(2-chloroethyl)ether ND 0.0100 1 01/21/2023 19:45 WG1991022
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 01/21/2023 19:45 WG1991022
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1577038
OUTFALL #1
Collected date/time: 01/17/23 13:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
4-Bromophenyl-phenylether ND 0.0100 1 01/21/2023 19:45 WG1991022
2-Chloronaphthalene ND 0.00100 1 01/21/2023 19:45 WG1991022
4-Chlorophenyl-phenylether ND 0.0100 1 01/21/2023 19:45 WG1991022
Chrysene ND 0.00100 1 01/21/2023 19:45 WG1991022
Dibenz(a,h)anthracene ND 0.00100 1 01/21/2023 19:45 WG1991022
3,3-Dichlorobenzidine ND 0.0100 1 01/21/2023 19:45 WG1991022
2,4-Dinitrotoluene ND 0.0100 1 01/21/2023 19:45 WG1991022
2,6-Dinitrotoluene ND 0.0100 1 01/21/2023 19:45 WG1991022
1,2-Diphenylhydrazine ND N2 0.0100 1 01/21/2023 19:45 WG1991022
Fluoranthene ND 0.00100 1 01/21/2023 19:45 WG1991022
Fluorene ND 0.00100 1 01/21/2023 19:45 WG1991022
Hexachlorobenzene ND 0.00100 1 01/21/2023 19:45 WG1991022
Hexachloro-1,3-butadiene ND 0.0100 1 01/21/2023 19:45 WG1991022
Hexachlorocyclopentadiene ND 0.0100 1 01/21/2023 19:45 WG1991022
Hexachloroethane ND 0.0100 1 01/21/2023 19:45 WG1991022
Indeno(1,2,3-cd)pyrene ND 0.00100 1 01/21/2023 19:45 WG1991022
Isophorone ND 0.0100 1 01/21/2023 19:45 WG1991022
Naphthalene ND 0.00100 1 01/21/2023 19:45 WG1991022
Nitrobenzene ND 0.0100 1 01/21/2023 19:45 WG1991022
n-Nitrosodimethylamine ND 0.0100 1 01/21/2023 19:45 WG1991022
n-Nitrosodiphenylamine ND 0.0100 1 01/21/2023 19:45 WG1991022
n-Nitrosodi-n-propylamine ND 0.0100 1 01/21/2023 19:45 WG1991022
Phenanthrene ND 0.00100 1 01/21/2023 19:45 WG1991022
Benzylbutyl phthalate ND 0.00300 1 01/21/2023 19:45 WG1991022
Bis(2-ethylhexyl)phthalate ND 0.00300 1 01/21/2023 19:45 WG1991022
Di-n-butyl phthalate 0.0107 0.00300 1 01/23/2023 12:43 WG1991022
Diethyl phthalate ND 0.00300 1 01/21/2023 19:45 WG1991022
Dimethyl phthalate ND 0.00300 1 01/21/2023 19:45 WG1991022
Di-n-octyl phthalate ND 0.00300 1 01/21/2023 19:45 WG1991022
Pyrene ND 0.00100 1 01/21/2023 19:45 WG1991022
1,2,4-Trichlorobenzene ND 0.0100 1 01/21/2023 19:45 WG1991022
4-Chloro-3-methylphenol ND 0.0100 1 01/21/2023 19:45 WG1991022
2-Chlorophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
2,4-Dichlorophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
2,4-Dimethylphenol ND 0.0100 1 01/21/2023 19:45 WG1991022
4,6-Dinitro-2-methylphenol ND 0.0100 1 01/21/2023 19:45 WG1991022
2,4-Dinitrophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
2-Nitrophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
4-Nitrophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
Pentachlorophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
Phenol ND 0.0100 1 01/21/2023 19:45 WG1991022
2,4,6-Trichlorophenol ND 0.0100 1 01/21/2023 19:45 WG1991022
(S) 2-Fluorophenol 43.8 10.0-120 01/23/2023 12:43 WG1991022
(S) 2-Fluorophenol 41.0 10.0-120 01/21/2023 19:45 WG1991022
(S) Phenol-d5 25.4 8.00-424 01/21/2023 19:45 WG1991022
(S) Phenol-d5 27.6 8.00-424 01/23/2023 12:43 WG1991022
(S) Nitrobenzene-d5 58.9 15.0-314 01/21/2023 19:45 WG1991022
(S) Nitrobenzene-d5 63.3 15.0-314 01/23/2023 12:43 WG1991022
(S) 2-Fluorobiphenyl 82.6 22.0-127 01/21/2023 19:45 WG1991022
(S) 2-Fluorobiphenyl 80.1 22.0-127 01/23/2023 12:43 WG1991022
(S) 2,4,6-Tribromophenol 114 10.0-153 01/23/2023 12:43 WG1991022
(S) 2,4,6-Tribromophenol 121 10.0-153 01/21/2023 19:45 WG1991022
(S) p-Terphenyl-d14 84.8 29.0-141 01/21/2023 19:45 WG1991022
(S) p-Terphenyl-d14 89.5 29.0-141 01/23/2023 12:43 WG1991022
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991110
Gravimetric Analysis by Method 2540 C-2011 L1577038-01,02
Method Blank (MB)
(MB) R3883116-1 01/19/23 10:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U 10.0 10.0
Laboratory Control Sample (LCS)
(LCS) R3883116-2 01/19/23 10:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Dissolved Solids 8800 7290 82.8 77.3-123
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1990901
Gravimetric Analysis by Method 2540 D-2015 L1577038-01,02
Method Blank (MB)
(MB) R3882351-1 01/18/23 18:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Suspended Solids U 2.50 2.50
L1576975-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1576975-01 01/18/23 18:56 • (DUP) R3882351-3 01/18/23 18:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Suspended Solids 46.8 53.6 1 13.5 J3 5
L1577056-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1577056-02 01/18/23 18:56 • (DUP) R3882351-4 01/18/23 18:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Suspended Solids 266 331 1 21.8 J3 5
Laboratory Control Sample (LCS)
(LCS) R3882351-2 01/18/23 18:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Suspended Solids 773 848 110 85.7-114
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1990838
Wet Chemistry by Method 1664A L1577038-01,02
Method Blank (MB)
(MB) R3882660-1 01/19/23 14:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3882660-2 01/19/23 14:59 • (LCSD) R3882660-3 01/19/23 14:59
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 32.8 32.2 82.0 80.5 78.0-114 1.85 20
L1576391-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1576391-02 01/19/23 14:59 • (MS) R3882660-4 01/19/23 14:59
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr) 40.0 ND 7.87 19.7 1 78.0-114 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991163
Wet Chemistry by Method 410.4 L1577038-01,02
Method Blank (MB)
(MB) R3882657-1 01/19/23 16:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
COD U 11.7 20.0
L1569484-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1569484-02 01/19/23 16:37 • (DUP) R3882657-3 01/19/23 16:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
COD 1470 1490 5 0.926 20
L1577001-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1577001-03 01/19/23 16:41 • (DUP) R3882657-6 01/19/23 16:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
COD 29.3 30.4 1 3.50 20
Laboratory Control Sample (LCS)
(LCS) R3882657-2 01/19/23 16:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
COD 500 481 96.2 90.0-110
L1576911-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576911-01 01/19/23 16:39 • (MS) R3882657-4 01/19/23 16:40 • (MSD) R3882657-5 01/19/23 16:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
COD 500 220 814 741 119 104 1 80.0-120 9.37 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991157
Wet Chemistry by Method 4500H+ B-2011 L1577038-01,02
L1576879-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1576879-01 01/19/23 18:00 • (DUP) R3882693-2 01/19/23 18:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 7.84 7.84 1 0.000 1
Sample Narrative:
OS: 7.84 at 19.6C
DUP: 7.84 at 19.6C
L1577209-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1577209-02 01/19/23 18:00 • (DUP) R3882693-3 01/19/23 18:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 9.23 9.24 1 0.108 1
Sample Narrative:
OS: 9.23 at 19.7C
DUP: 9.24 at 19.3C
Laboratory Control Sample (LCS)
(LCS) R3882693-1 01/19/23 18:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su %%
pH 10.0 9.90 99.0 99.0-101
Sample Narrative:
LCS: 9.9 at 20.5C
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1990811
Mercury by Method 245.1 L1577038-01,02
Method Blank (MB)
(MB) R3882466-1 01/19/23 08:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3882466-2 01/19/23 08:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00306 102 85.0-115
L1576846-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576846-01 01/19/23 08:49 • (MS) R3882466-3 01/19/23 08:51 • (MSD) R3882466-4 01/19/23 08:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00313 0.00322 104 107 1 70.0-130 2.84 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1990808
Metals (ICP) by Method 200.7 L1577038-01,02
Method Blank (MB)
(MB) R3882770-1 01/19/23 19:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Arsenic U 0.00645 0.0100
Barium U 0.000795 0.00500
Beryllium U 0.000401 0.00200
Cadmium U 0.000552 0.00200
Copper 0.00233 J 0.00226 0.0100
Iron U 0.0205 0.100
Lead U 0.00227 0.00500
Selenium U 0.00616 0.0100
Laboratory Control Sample (LCS)
(LCS) R3882770-2 01/19/23 19:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Arsenic 1.00 0.875 87.5 85.0-115
Barium 1.00 0.928 92.8 85.0-115
Beryllium 1.00 0.944 94.4 85.0-115
Cadmium 1.00 0.856 85.6 85.0-115
Copper 1.00 0.899 89.9 85.0-115
Iron 10.0 8.83 88.3 85.0-115
Lead 1.00 0.958 95.8 85.0-115
Selenium 1.00 0.949 94.9 85.0-115
L1576493-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576493-01 01/19/23 19:39 • (MS) R3882770-4 01/19/23 19:45 • (MSD) R3882770-5 01/19/23 19:47
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 ND 0.910 0.919 91.0 91.9 1 70.0-130 0.948 20
Barium 1.00 0.0155 0.972 0.976 95.6 96.0 1 70.0-130 0.365 20
Beryllium 1.00 ND 0.985 0.988 98.5 98.8 1 70.0-130 0.297 20
Cadmium 1.00 ND 0.900 0.904 90.0 90.4 1 70.0-130 0.364 20
Copper 1.00 ND 0.939 0.931 93.5 92.7 1 70.0-130 0.889 20
Iron 10.0 ND 9.18 9.21 91.5 91.7 1 70.0-130 0.276 20
Lead 1.00 ND 0.993 1.00 99.3 100 1 70.0-130 0.728 20
Selenium 1.00 ND 0.986 1.00 98.6 100 1 70.0-130 1.41 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1990808
Metals (ICP) by Method 200.7 L1577038-01,02
L1576892-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576892-01 01/19/23 19:50 • (MS) R3882770-6 01/19/23 19:52 • (MSD) R3882770-7 01/19/23 19:55
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 ND 0.886 0.916 88.6 91.6 1 70.0-130 3.28 20
Barium 1.00 0.00714 0.955 0.986 94.8 97.9 1 70.0-130 3.20 20
Beryllium 1.00 ND 0.974 1.00 97.4 100 1 70.0-130 2.91 20
Cadmium 1.00 ND 0.870 0.899 87.0 89.9 1 70.0-130 3.29 20
Copper 1.00 ND 0.915 0.950 90.8 94.2 1 70.0-130 3.73 20
Iron 10.0 ND 9.13 9.38 91.0 93.5 1 70.0-130 2.63 20
Lead 1.00 ND 0.987 1.00 98.7 100 1 70.0-130 1.67 20
Selenium 1.00 ND 0.956 0.990 95.6 99.0 1 70.0-130 3.52 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991929
Metals (ICP) by Method 200.7 L1577038-01,02
Method Blank (MB)
(MB) R3883537-1 01/23/23 11:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Aluminum U 0.0592 0.200
Chromium U 0.00163 0.0100
Silver U 0.00131 0.00500
Zinc U 0.00578 0.0500
Laboratory Control Sample (LCS)
(LCS) R3883537-2 01/23/23 11:38
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Aluminum 10.0 10.0 100 85.0-115
Chromium 1.00 0.989 98.9 85.0-115
Silver 0.200 0.197 98.3 85.0-115
Zinc 1.00 0.986 98.6 85.0-115
L1576901-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576901-01 01/23/23 11:40 • (MS) R3883537-4 01/23/23 11:46 • (MSD) R3883537-5 01/23/23 11:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Aluminum 10.0 ND 9.83 10.2 96.8 100 1 70.0-130 3.32 20
Chromium 1.00 ND 0.944 0.964 94.4 96.4 1 70.0-130 2.09 20
Silver 0.200 ND 0.197 0.203 98.3 101 1 70.0-130 2.97 20
Zinc 1.00 0.152 1.12 1.14 97.0 99.2 1 70.0-130 1.93 20
L1576905-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576905-01 01/23/23 11:51 • (MS) R3883537-6 01/23/23 11:54 • (MSD) R3883537-7 01/23/23 11:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Aluminum 10.0 ND 10.0 9.93 99.6 98.6 1 70.0-130 1.03 20
Chromium 1.00 ND 0.989 0.976 98.9 97.6 1 70.0-130 1.36 20
Silver 0.200 ND 0.196 0.195 98.2 97.5 1 70.0-130 0.714 20
Zinc 1.00 0.0558 1.03 1.02 97.2 96.0 1 70.0-130 1.20 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991047
Volatile Organic Compounds (GC) by Method 8015D/GRO L1577038-01,02
Method Blank (MB)
(MB) R3882601-2 01/18/23 22:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 0.0408 J 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)101 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3882601-1 01/18/23 21:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.86 107 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 107 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 22 of 39
QUALITY CONTROL SUMMARYWG1991291
Volatile Organic Compounds (GC/MS) by Method 624.1 L1577038-01,02
Method Blank (MB)
(MB) R3882579-3 01/19/23 09:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
2-Chloroethyl vinyl ether U 0.000575 0.0500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
Ethylbenzene U 0.000137 0.00100
Methylene Chloride U 0.000430 0.00500
Methyl tert-butyl ether U 0.000101 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 115 80.0-120
(S) 4-Bromofluorobenzene 111 80.0-120
(S) 1,2-Dichloroethane-d4 99.7 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991291
Volatile Organic Compounds (GC/MS) by Method 624.1 L1577038-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3882579-1 01/19/23 08:51 • (LCSD) R3882579-2 01/19/23 09:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acrolein 0.0250 0.0180 0.0227 72.0 90.8 60.0-140 J3 23.1 20
Acrylonitrile 0.0250 0.0244 0.0218 97.6 87.2 60.0-140 11.3 20
Benzene 0.00500 0.00492 0.00489 98.4 97.8 65.0-135 0.612 20
Bromodichloromethane 0.00500 0.00471 0.00470 94.2 94.0 65.0-135 0.213 20
Bromoform 0.00500 0.00582 0.00620 116 124 70.0-130 6.32 20
Bromomethane 0.00500 0.00503 0.00551 101 110 15.0-185 9.11 20
Carbon tetrachloride 0.00500 0.00555 0.00516 111 103 70.0-130 7.28 20
Chlorobenzene 0.00500 0.00571 0.00582 114 116 65.0-135 1.91 20
Chlorodibromomethane 0.00500 0.00555 0.00576 111 115 70.0-135 3.71 20
Chloroethane 0.00500 0.00555 0.00582 111 116 40.0-160 4.75 20
2-Chloroethyl vinyl ether 0.0250 0.0226 0.0215 90.4 86.0 0.100-225 4.99 20
Chloroform 0.00500 0.00477 0.00490 95.4 98.0 70.0-135 2.69 20
Chloromethane 0.00500 0.00401 0.00453 80.2 90.6 0.100-205 12.2 20
1,2-Dichlorobenzene 0.00500 0.00489 0.00495 97.8 99.0 65.0-135 1.22 20
1,3-Dichlorobenzene 0.00500 0.00510 0.00500 102 100 70.0-130 1.98 20
1,4-Dichlorobenzene 0.00500 0.00510 0.00487 102 97.4 65.0-135 4.61 20
Dichlorodifluoromethane 0.00500 0.00411 0.00434 82.2 86.8 49.0-155 5.44 20
1,1-Dichloroethane 0.00500 0.00454 0.00480 90.8 96.0 70.0-130 5.57 20
1,2-Dichloroethane 0.00500 0.00447 0.00454 89.4 90.8 70.0-130 1.55 20
1,1-Dichloroethene 0.00500 0.00517 0.00491 103 98.2 50.0-150 5.16 20
trans-1,2-Dichloroethene 0.00500 0.00514 0.00545 103 109 70.0-130 5.85 20
1,2-Dichloropropane 0.00500 0.00419 0.00390 83.8 78.0 35.0-165 7.17 20
cis-1,3-Dichloropropene 0.00500 0.00461 0.00444 92.2 88.8 25.0-175 3.76 20
trans-1,3-Dichloropropene 0.00500 0.00470 0.00483 94.0 96.6 50.0-150 2.73 20
Ethylbenzene 0.00500 0.00557 0.00564 111 113 60.0-140 1.25 20
Methylene Chloride 0.00500 0.00481 0.00466 96.2 93.2 60.0-140 3.17 20
Methyl tert-butyl ether 0.00500 0.00463 0.00488 92.6 97.6 64.0-123 5.26 20
1,1,2,2-Tetrachloroethane 0.00500 0.00478 0.00430 95.6 86.0 60.0-140 10.6 20
Tetrachloroethene 0.00500 0.00625 0.00634 125 127 70.0-130 1.43 20
Toluene 0.00500 0.00504 0.00534 101 107 70.0-130 5.78 20
1,1,1-Trichloroethane 0.00500 0.00510 0.00529 102 106 70.0-130 3.66 20
1,1,2-Trichloroethane 0.00500 0.00544 0.00521 109 104 70.0-130 4.32 20
Trichloroethene 0.00500 0.00602 0.00584 120 117 65.0-135 3.04 20
Trichlorofluoromethane 0.00500 0.00626 0.00626 125 125 50.0-150 0.000 20
Vinyl chloride 0.00500 0.00496 0.00552 99.2 110 5.00-195 10.7 20
Xylenes, Total 0.0150 0.0164 0.0171 109 114 77.0-120 4.18 20
(S) Toluene-d8 105 114 80.0-120
(S) 4-Bromofluorobenzene 104 108 80.0-120
(S) 1,2-Dichloroethane-d4 99.8 102 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991076
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1577038-01,02
Method Blank (MB)
(MB) R3882764-1 01/19/23 12:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) High Fraction U 0.0247 0.100
(S) o-Terphenyl 100 31.0-160
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3882764-2 01/19/23 13:15 • (LCSD) R3882764-3 01/19/23 13:35
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.50 1.60 1.65 107 110 50.0-150 3.08 20
(S) o-Terphenyl 67.5 70.0 31.0-160
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Pesticides (GC) by Method EPA 608.3 L1577038-01,02
Method Blank (MB)
(MB) R3883380-1 01/20/23 12:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Aldrin U 0.0000198 0.0000500
Alpha BHC U 0.0000172 0.0000500
Beta BHC U 0.0000208 0.0000500
Delta BHC U 0.0000150 0.0000500
Gamma BHC U 0.0000209 0.0000500
Chlordane U 0.0000198 0.00500
4,4-DDD U 0.0000177 0.0000500
4,4-DDE U 0.0000154 0.0000500
4,4-DDT U 0.0000198 0.0000500
Dieldrin U 0.0000162 0.0000500
Endosulfan I U 0.0000160 0.0000500
Endosulfan II U 0.0000164 0.0000500
Endosulfan sulfate U 0.0000217 0.0000500
Endrin U 0.0000161 0.0000500
Endrin aldehyde U 0.0000237 0.0000500
Endrin ketone U 0.0000219 0.0000500
Heptachlor U 0.0000148 0.0000500
Heptachlor epoxide U 0.0000183 0.0000500
Hexachlorobenzene U 0.0000176 0.0000500
Methoxychlor U 0.0000193 0.0000500
Toxaphene U 0.000168 0.000500
gamma-Chlordane U 0.0000137 0.0000500
alpha-Chlordane U 0.0000149 0.0000500
(S) Decachlorobiphenyl 75.5 10.0-144
(S) Tetrachloro-m-xylene 55.0 10.0-135
Laboratory Control Sample (LCS)
(LCS) R3883380-2 01/20/23 12:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Aldrin 0.00100 0.000808 80.8 42.0-140
Alpha BHC 0.00100 0.000854 85.4 37.0-140
Beta BHC 0.00100 0.00100 100 17.0-147
Delta BHC 0.00100 0.000924 92.4 19.0-140
Gamma BHC 0.00100 0.000840 84.0 32.0-140
4,4-DDD 0.00100 0.00100 100 31.0-141
4,4-DDE 0.00100 0.00104 104 30.0-145
4,4-DDT 0.00100 0.00102 102 25.0-160
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Pesticides (GC) by Method EPA 608.3 L1577038-01,02
Laboratory Control Sample (LCS)
(LCS) R3883380-2 01/20/23 12:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Dieldrin 0.00100 0.000847 84.7 36.0-146
Endosulfan I 0.00100 0.000907 90.7 45.0-153
Endosulfan II 0.00100 0.000938 93.8 1.00-202
Endosulfan sulfate 0.00100 0.000940 94.0 26.0-144
Endrin 0.00100 0.000895 89.5 30.0-147
Endrin aldehyde 0.00100 0.000991 99.1 56.0-128
Endrin ketone 0.00100 0.000944 94.4 54.0-142
Heptachlor 0.00100 0.000800 80.0 34.0-140
Heptachlor epoxide 0.00100 0.000901 90.1 37.0-142
Hexachlorobenzene 0.00100 0.000914 91.4 35.0-120
Methoxychlor 0.00100 0.00108 108 44.0-160
gamma-Chlordane 0.00100 0.000991 99.1 45.0-140
alpha-Chlordane 0.00100 0.000876 87.6 45.0-140
(S) Decachlorobiphenyl 68.7 10.0-144
(S) Tetrachloro-m-xylene 55.4 10.0-135
L1576864-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576864-09 01/20/23 15:02 • (MS) R3883380-4 01/20/23 15:12 • (MSD) R3883380-5 01/20/23 15:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Aldrin 0.00100 ND 0.000691 0.000720 69.1 72.0 1 42.0-140 4.11 35
Alpha BHC 0.00100 ND 0.000724 0.000766 72.4 76.6 1 37.0-140 5.64 36
Beta BHC 0.00100 ND 0.000838 0.000889 83.8 88.9 1 17.0-147 5.91 44
Delta BHC 0.00100 ND 0.000823 0.000808 82.3 80.8 1 19.0-140 1.84 52
Gamma BHC 0.00100 ND 0.000706 0.000766 70.6 76.6 1 32.0-140 8.15 39
4,4-DDD 0.00100 ND 0.000826 0.000924 82.6 92.4 1 31.0-141 11.2 39
4,4-DDE 0.00100 ND 0.000728 0.000792 72.8 79.2 1 30.0-145 8.42 35
4,4-DDT 0.00100 ND 0.000478 0.000530 47.8 53.0 1 25.0-160 10.3 42
Dieldrin 0.00100 ND 0.000696 0.000737 69.6 73.7 1 36.0-146 5.72 49
Endosulfan I 0.00100 ND 0.000664 0.000736 66.4 73.6 1 45.0-153 10.3 28
Endosulfan II 0.00100 ND 0.000672 0.000704 67.2 70.4 1 1.00-202 4.65 53
Endosulfan sulfate 0.00100 ND 0.000609 0.000692 60.9 69.2 1 26.0-144 12.8 38
Endrin 0.00100 ND 0.000607 0.000678 60.7 67.8 1 30.0-147 11.1 48
Endrin aldehyde 0.00100 ND 0.000647 0.000737 64.7 73.7 1 56.0-128 13.0 20
Endrin ketone 0.00100 ND 0.000621 0.000688 62.1 68.8 1 54.0-142 10.2 20
Heptachlor 0.00100 ND 0.000605 0.000628 60.5 62.8 1 34.0-140 3.73 43
Heptachlor epoxide 0.00100 ND 0.000659 0.000718 65.9 71.8 1 37.0-142 8.57 26
Hexachlorobenzene 0.00100 ND 0.000689 0.000727 68.9 72.7 1 35.0-120 5.37 25
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991021
Pesticides (GC) by Method EPA 608.3 L1577038-01,02
L1576864-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576864-09 01/20/23 15:02 • (MS) R3883380-4 01/20/23 15:12 • (MSD) R3883380-5 01/20/23 15:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Methoxychlor 0.00100 ND 0.000577 0.000629 57.7 62.9 1 44.0-160 8.62 22
gamma-Chlordane 0.00100 ND 0.000725 0.000784 72.5 78.4 1 45.0-140 7.82 35
alpha-Chlordane 0.00100 ND 0.000597 0.000622 59.7 62.2 1 45.0-140 4.10 35
(S) Decachlorobiphenyl 57.9 52.4 10.0-144
(S) Tetrachloro-m-xylene 37.7 38.9 10.0-135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Tetra Tech Inc. - UT RECYCLED EARTH L1577038 01/27/23 15:35 28 of 39
QUALITY CONTROL SUMMARYWG1991021
Polychlorinated Biphenyls (GC) by Method EPA-608.3 L1577038-01,02
Method Blank (MB)
(MB) R3883380-1 01/20/23 12:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
Total PCBs U 0.000173 0.000500
(S) Decachlorobiphenyl 87.9 10.0-144
(S) Tetrachloro-m-xylene 71.1 10.0-135
Laboratory Control Sample (LCS)
(LCS) R3883380-3 01/20/23 12:38
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
PCB 1016 0.00250 0.00204 81.6 50.0-140
PCB 1260 0.00250 0.00233 93.2 8.00-140
(S) Decachlorobiphenyl 67.5 10.0-144
(S) Tetrachloro-m-xylene 69.8 10.0-135
L1576864-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576864-09 01/20/23 15:02 • (MS) R3883380-6 01/20/23 15:33 • (MSD) R3883380-7 01/20/23 15:43
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 ND 0.00157 0.00137 62.8 54.8 1 50.0-140 13.6 36
PCB 1260 0.00250 ND 0.00191 0.00190 76.4 76.0 1 8.00-140 0.525 38
(S) Decachlorobiphenyl 64.0 69.6 10.0-144
(S) Tetrachloro-m-xylene 57.1 55.6 10.0-135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1991022
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577038-01,02
Method Blank (MB)
(MB) R3883396-2 01/21/23 15:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-oxybis(1-chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
1,2-Diphenylhydrazine U N2 0.000105 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1991022
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577038-01,02
Method Blank (MB)
(MB) R3883396-2 01/21/23 15:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 38.1 10.0-120
(S) Phenol-d5 22.3 8.00-424
(S) Nitrobenzene-d5 71.8 15.0-314
(S) 2-Fluorobiphenyl 77.7 22.0-127
(S) 2,4,6-Tribromophenol 72.5 10.0-153
(S) p-Terphenyl-d14 76.1 29.0-141
Laboratory Control Sample (LCS)
(LCS) R3883396-1 01/21/23 14:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acenaphthene 0.0500 0.0370 74.0 47.0-145
Acenaphthylene 0.0500 0.0396 79.2 33.0-145
Anthracene 0.0500 0.0359 71.8 27.0-133
Benzidine 0.100 0.0213 21.3 1.00-120
Benzo(a)anthracene 0.0500 0.0391 78.2 33.0-143
Benzo(b)fluoranthene 0.0500 0.0362 72.4 24.0-159
Benzo(k)fluoranthene 0.0500 0.0348 69.6 11.0-162
Benzo(g,h,i)perylene 0.0500 0.0371 74.2 1.00-219
Benzo(a)pyrene 0.0500 0.0391 78.2 17.0-163
Bis(2-chlorethoxy)methane 0.0500 0.0312 62.4 1.00-219
Bis(2-chloroethyl)ether 0.0500 0.0329 65.8 33.0-185
2,2-oxybis(1-chloropropane) 0.0500 0.0355 71.0 36.0-166
4-Bromophenyl-phenylether 0.0500 0.0469 93.8 53.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991022
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577038-01,02
Laboratory Control Sample (LCS)
(LCS) R3883396-1 01/21/23 14:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Chloronaphthalene 0.0500 0.0372 74.4 60.0-120
4-Chlorophenyl-phenylether 0.0500 0.0396 79.2 25.0-158
Chrysene 0.0500 0.0371 74.2 17.0-168
Dibenz(a,h)anthracene 0.0500 0.0391 78.2 1.00-227
3,3-Dichlorobenzidine 0.100 0.0715 71.5 1.00-262
2,4-Dinitrotoluene 0.0500 0.0428 85.6 39.0-139
2,6-Dinitrotoluene 0.0500 0.0398 79.6 50.0-158
1,2-Diphenylhydrazine 0.0500 0.0340 68.0 37.0-125 N2
Fluoranthene 0.0500 0.0457 91.4 26.0-137
Fluorene 0.0500 0.0388 77.6 59.0-121
Hexachlorobenzene 0.0500 0.0391 78.2 1.00-152
Hexachloro-1,3-butadiene 0.0500 0.0384 76.8 24.0-120
Hexachlorocyclopentadiene 0.0500 0.0340 68.0 10.0-120
Hexachloroethane 0.0500 0.0327 65.4 40.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0377 75.4 1.00-171
Isophorone 0.0500 0.0294 58.8 21.0-196
Naphthalene 0.0500 0.0341 68.2 21.0-133
Nitrobenzene 0.0500 0.0311 62.2 35.0-180
n-Nitrosodimethylamine 0.0500 0.0189 37.8 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0306 61.2 44.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0321 64.2 1.00-230
Phenanthrene 0.0500 0.0391 78.2 54.0-120
Benzylbutyl phthalate 0.0500 0.0333 66.6 1.00-152
Bis(2-ethylhexyl)phthalate 0.0500 0.0319 63.8 8.00-158
Di-n-butyl phthalate 0.0500 0.0408 81.6 1.00-120
Diethyl phthalate 0.0500 0.0406 81.2 1.00-120
Dimethyl phthalate 0.0500 0.0394 78.8 1.00-120
Di-n-octyl phthalate 0.0500 0.0368 73.6 4.00-146
Pyrene 0.0500 0.0337 67.4 52.0-120
1,2,4-Trichlorobenzene 0.0500 0.0350 70.0 44.0-142
4-Chloro-3-methylphenol 0.0500 0.0329 65.8 22.0-147
2-Chlorophenol 0.0500 0.0322 64.4 23.0-134
2,4-Dichlorophenol 0.0500 0.0343 68.6 39.0-135
2,4-Dimethylphenol 0.0500 0.0254 50.8 32.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0529 106 1.00-181
2,4-Dinitrophenol 0.0500 0.0532 106 1.00-191
2-Nitrophenol 0.0500 0.0361 72.2 29.0-182
4-Nitrophenol 0.0500 0.0172 34.4 1.00-132
Pentachlorophenol 0.0500 0.0362 72.4 14.0-176
Phenol 0.0500 0.0147 29.4 5.00-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991022
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577038-01,02
Laboratory Control Sample (LCS)
(LCS) R3883396-1 01/21/23 14:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,4,6-Trichlorophenol 0.0500 0.0388 77.6 37.0-144
(S) 2-Fluorophenol 46.4 10.0-120
(S) Phenol-d5 27.2 8.00-424
(S) Nitrobenzene-d5 63.0 15.0-314
(S) 2-Fluorobiphenyl 73.3 22.0-127
(S) 2,4,6-Tribromophenol 80.0 10.0-153
(S) p-Terphenyl-d14 68.1 29.0-141
L1577188-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1577188-01 01/23/23 19:03 • (MS) R3884084-1 01/23/23 19:24 • (MSD) R3884084-2 01/23/23 19:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 ND 0.0330 0.0321 66.0 64.2 1 47.0-145 2.76 48
Acenaphthylene 0.0500 ND 0.0351 0.0344 70.2 68.8 1 33.0-145 2.01 74
Anthracene 0.0500 ND 0.0356 0.0341 71.2 68.2 1 27.0-133 4.30 66
Benzidine 0.100 ND ND ND 0.000 0.000 1 1.00-120 J6 J6 0.000 40
Benzo(a)anthracene 0.0500 ND 0.0399 0.0398 79.8 79.6 1 33.0-143 0.251 53
Benzo(b)fluoranthene 0.0500 ND 0.0423 0.0428 84.6 85.6 1 24.0-159 1.18 71
Benzo(k)fluoranthene 0.0500 ND 0.0401 0.0401 80.2 80.2 1 11.0-162 0.000 63
Benzo(g,h,i)perylene 0.0500 ND 0.0395 0.0395 79.0 79.0 1 1.00-219 0.000 97
Benzo(a)pyrene 0.0500 ND 0.0440 0.0435 88.0 87.0 1 17.0-163 1.14 72
Bis(2-chlorethoxy)methane 0.0500 ND 0.0285 0.0274 57.0 54.8 1 33.0-184 3.94 54
Bis(2-chloroethyl)ether 0.0500 ND 0.0287 0.0285 57.4 57.0 1 12.0-158 0.699 108
2,2-oxybis(1-chloropropane) 0.0500 ND 0.0278 0.0263 55.6 52.6 1 36.0-166 5.55 76
4-Bromophenyl-phenylether 0.0500 ND 0.0387 0.0379 77.4 75.8 1 53.0-127 2.09 43
2-Chloronaphthalene 0.0500 ND 0.0326 0.0314 65.2 62.8 1 60.0-120 3.75 24
4-Chlorophenyl-phenylether 0.0500 ND 0.0350 0.0342 70.0 68.4 1 25.0-158 2.31 61
Chrysene 0.0500 ND 0.0397 0.0395 79.4 79.0 1 17.0-168 0.505 87
Dibenz(a,h)anthracene 0.0500 ND 0.0400 0.0401 80.0 80.2 1 1.00-227 0.250 126
3,3-Dichlorobenzidine 0.100 ND 0.0374 0.0355 37.4 35.5 1 1.00-262 5.21 108
2,4-Dinitrotoluene 0.0500 ND 0.0388 0.0388 77.6 77.6 1 39.0-139 0.000 42
2,6-Dinitrotoluene 0.0500 ND 0.0374 0.0367 74.8 73.4 1 50.0-158 1.89 48
1,2-Diphenylhydrazine 0.0500 ND 0.0400 0.0384 80.0 76.8 1 18.0-156 N2 N2 4.08 34
Fluoranthene 0.0500 ND 0.0410 0.0402 82.0 80.4 1 26.0-137 1.97 66
Fluorene 0.0500 ND 0.0356 0.0343 71.2 68.6 1 59.0-121 3.72 38
Hexachlorobenzene 0.0500 ND 0.0366 0.0354 73.2 70.8 1 1.00-152 3.33 55
Hexachloro-1,3-butadiene 0.0500 ND 0.0263 0.0254 52.6 50.8 1 24.0-120 3.48 62
Hexachlorocyclopentadiene 0.0500 ND 0.0257 0.0227 51.4 45.4 1 10.0-146 12.4 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG1991022
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1577038-01,02
L1577188-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1577188-01 01/23/23 19:03 • (MS) R3884084-1 01/23/23 19:24 • (MSD) R3884084-2 01/23/23 19:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexachloroethane 0.0500 ND 0.0273 0.0259 54.6 51.8 1 40.0-120 5.26 52
Indeno(1,2,3-cd)pyrene 0.0500 ND 0.0380 0.0381 76.0 76.2 1 1.00-171 0.263 99
Isophorone 0.0500 ND 0.0278 0.0269 55.6 53.8 1 21.0-196 3.29 93
Naphthalene 0.0500 ND 0.0265 0.0260 53.0 52.0 1 21.0-133 1.90 65
Nitrobenzene 0.0500 ND 0.0289 0.0284 57.8 56.8 1 35.0-180 1.75 62
n-Nitrosodimethylamine 0.0500 ND 0.0228 0.0234 45.6 46.8 1 10.0-120 2.60 40
n-Nitrosodiphenylamine 0.0500 ND 0.0349 0.0345 69.8 69.0 1 16.0-160 1.15 28
n-Nitrosodi-n-propylamine 0.0500 ND 0.0284 0.0269 56.8 53.8 1 1.00-230 5.42 87
Phenanthrene 0.0500 ND 0.0412 0.0405 82.4 81.0 1 54.0-120 1.71 39
Benzylbutyl phthalate 0.0500 ND 0.0470 0.0486 94.0 97.2 1 1.00-152 3.35 60
Bis(2-ethylhexyl)phthalate 0.0500 ND 0.0447 0.0460 87.3 89.9 1 8.00-158 2.87 82
Di-n-butyl phthalate 0.0500 ND 0.0440 0.0436 88.0 87.2 1 1.00-120 0.913 47
Diethyl phthalate 0.0500 ND 0.0369 0.0373 73.8 74.6 1 1.00-120 1.08 100
Dimethyl phthalate 0.0500 ND 0.0358 0.0349 71.6 69.8 1 1.00-120 2.55 183
Di-n-octyl phthalate 0.0500 ND 0.0475 0.0468 95.0 93.6 1 4.00-146 1.48 69
Pyrene 0.0500 ND 0.0444 0.0451 88.8 90.2 1 52.0-120 1.56 49
1,2,4-Trichlorobenzene 0.0500 ND 0.0272 0.0260 54.4 52.0 1 44.0-142 4.51 50
4-Chloro-3-methylphenol 0.0500 ND 0.0321 0.0318 64.2 63.6 1 22.0-147 0.939 73
2-Chlorophenol 0.0500 ND 0.0233 0.0222 46.6 44.4 1 23.0-134 4.84 61
2,4-Dichlorophenol 0.0500 ND 0.0274 0.0270 54.8 54.0 1 39.0-135 1.47 50
2,4-Dimethylphenol 0.0500 ND 0.0258 0.0237 51.6 47.4 1 32.0-120 8.48 58
4,6-Dinitro-2-methylphenol 0.0500 ND 0.0441 0.0454 88.2 90.8 1 1.00-181 2.91 203
2,4-Dinitrophenol 0.0500 ND 0.0405 0.0398 81.0 79.6 1 1.00-191 1.74 132
2-Nitrophenol 0.0500 ND 0.0270 0.0258 54.0 51.6 1 29.0-182 4.55 55
4-Nitrophenol 0.0500 ND 0.0169 0.0176 33.8 35.2 1 1.00-132 4.06 131
Pentachlorophenol 0.0500 ND 0.0401 0.0405 80.2 81.0 1 14.0-176 0.993 86
Phenol 0.0500 ND 0.0114 0.0111 22.8 22.2 1 5.00-120 2.67 64
2,4,6-Trichlorophenol 0.0500 ND 0.0356 0.0349 71.2 69.8 1 37.0-144 1.99 58
(S) 2-Fluorophenol 33.2 32.3 10.0-120
(S) Phenol-d5 21.9 20.8 8.00-424
(S) Nitrobenzene-d5 49.7 50.5 15.0-314
(S) 2-Fluorobiphenyl 65.6 63.8 22.0-127
(S) 2,4,6-Tribromophenol 79.5 80.0 10.0-153
(S) p-Terphenyl-d14 83.5 85.5 29.0-141
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
N2 Analyte reported using a calibration and validation based on Azobenzene (CAS 103-33-3). 1,2-Diphenylhydrazine
decomposes into Azobenzene during the analysis.
T8 Sample(s) received past/too close to holding time expiration.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
January 26, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1577040
Samples Received:01/18/2023
Project Number:RECYCLED EARTH
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
January 26, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
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January 26, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Gl: Glossary of Terms 5
Al: Accreditations & Locations 6
Sc: Sample Chain of Custody 7
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SE-POND L1577040-01 WW Anna Rasmuson 01/17/23 11:45 01/18/23 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Subcontracted Analyses WG1990791 1 01/26/23 00:00 01/26/23 00:00 -Minneapolis, MN
55414
Collected by Collected date/time Received date/time
OUTFALL #1 L1577040-02 WW Anna Rasmuson 01/17/23 13:20 01/18/23 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Subcontracted Analyses WG1990791 1 01/26/23 00:00 01/26/23 00:00 -Minneapolis, MN
55414
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:48 3 of 23
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:56 3 of 23
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Project Narrative
L1577040 -01, -02 contains subout data that is included after the chain of custody.
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:48 4 of 23
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:56 4 of 23
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
SDG Sample Delivery Group.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:48 5 of 23
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:56 5 of 23

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Gl
6 Al
7 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:48 6 of 23
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1577040 01/26/23 16:56 6 of 23
Thisreportshould notbe reproduced,exceptinfull,
withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlytothesamples included inthisreport.
Report of Laboratory Analysis
www.pacelabs.com
Pace Analytical Services,LLC.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
Client Services
Pace Analytical National
12065 Lebanon Rd
Mt. Juliet TN 37122
REPORT OF
LABORATORY
ANALYSIS FOR
TCDD
This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
January 26, 2023
Pace Project #:10640325
Sample Receipt Date:01/19/2023
Client Project #:L1577040 WG1990791
Client Sub PO #:L1577040
The report provided has been invoiced as a Level 2
2,3,7,8-TCDD Report. If an upgrade of this report
package is requested,an additional charge may be
applied.
Please review the attached invoice for accuracy and
forward any questions to Kongmeng Vang,your Pace
Project Manager.
State Cert #:N/A
Report Prepared for:
Page 1 of 14Report No.....10640325_SW8290TCDD_L2_dfr
January 26, 2023
Kongmeng Vang, Project Manager
[phone]
[phone] (fax)
[e-mail]
Pace Analytical Services,LLC.
1700 Elm Street
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
This report presents the results from the analyses performed on two samples submitted
by a representative of Pace Analytical National. The samples were analyzed for the
presence or absence of 2,3,7,8-tetrachlorodibenzo-p-dioxin (2,3,7,8-TCDD) using a
modified version of USEPA Method 8290. The reporting limits were set to correspond
to the lowest calibration point and a nominal 1-Liter sample amount, and the sensitivity
was verified by signal-to-noise measurements. The quantitation limits, adjusted for
sample extraction amount, may be somewhat higher or lower than the reporting limits
provided in this report.
The recoveries of the isotopically-labeled TCDD internal standard in the sample
extracts ranged from 53-69%. Except for one low value, which was flagged "R" on the
results table, the labeled internal standard recoveries obtained for this project were
within the 40-135% target range specified in Method 8290. Also, since the
quantification of the native TCDD was based on isotope dilution, the data were
automatically corrected for recovery and accurate values were obtained.
A laboratory method blank was prepared and analyzed with each sample batch as part
of our routine quality control procedures. The results show the blanks to be free of
2,3,7,8-TCDD at the reporting limit.
Laboratory spike samples were also prepared using clean reference matrix that had
been fortified with native standard material. The results show that the spiked native
TCDD was recovered at 104-111% with a relative percent difference of 6.5%. These
results were within the target ranges for the method. Matrix spikes were not prepared
with the sample batch.
DISCUSSION
Page 2 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Report No.....10640325
Minnesota Laboratory Certifications
Authority Certificate #Authority Certificate #
Missouri 10100
A2LA 2926.01 Montana CERT0092
Alabama 40770 Nebraska NE-OS-18-06
Alaska-DW MN00064 Nevada MN00064
Alaska-UST 17-009 New Hampshire 2081
Arizona AZ0014 New Jersey MN002
Arkansas - WW 88-0680 New York 11647
Arkansas-DW MN00064 North Carolina-27700
California 2929 North Carolina-530
Colorado MN00064 North Dakota R-036
Connecticut PH-0256 Ohio-DW 41244
Florida E87605 Ohio-VAP (170 CL101
Georgia 959 Ohio-VAP (180 CL110
Hawaii MN00064 Oklahoma 9507
Idaho MN00064 Oregon-Primary MN300001
Illinois 200011 Oregon-Second MN200001
Indiana C-MN-01 Pennsylvania 68-00563
Iowa 368 Puerto Rico MN00064
Kansas E-10167 South Carolina 74003
Kentucky-DW 90062 Tennessee TN02818
Kentucky-WW 90062 Texas T104704192
Louisiana-DEQ AI-84596 Utah MN00064
Louisiana-DW MN00064 Vermont VT-027053137
Maine MN00064 Virginia 460163
Maryland 322 Washington C486
Michigan 9909 West Virginia-D 382
Minnesota 027-053-137 West Virginia-D 9952C
Minnesota-Ag via MN 027-053 Wisconsin 999407970
Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Mississippi MN00064
Page 3 of 14Report No.....10640325_SW8290TCDD_L2_dfr
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix A
Sample Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14Report No.....10640325_SW8290TCDD_L2_dfr
Pa
g
e

5

o
f

1
4
Re
p
o
r
t

N
o
.
.
.
.
.
1
0
6
4
0
3
2
5
_
S
W
8
2
9
0
T
C
D
D
_
L
2
_
d
f
r
Page 6 of 14Report No.....10640325_SW8290TCDD_L2_dfr
1/19/23
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
A =

B =

C =

D =

E =

H2 =

I =

J =

L =

Nn =

P =

R =

S =

U =

V =

X =

Y =

* =
Reporting Limit based on signal to noise (EDL)

Less than 10x higher than method blank level

Result obtained from confirmation analysis

Result obtained from analysis of diluted sample

Exceeds calibration range

Extracted outside of holding time

Isotope ratio out of specification

Estimated value

Suppressive interference, analyte may be biased low

Value obtained from additional analysis

PCDE Interference

Recovery outside target range

Peak saturated

Analyte not detected

Result verified by confirmation analysis

%D Exceeds limits

Calculated using average of daily RFs

See Discussion
Reporting Flags
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 14Report No.....10640325_SW8290TCDD_L2_dfr
Pace Analytical Services, LLC
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Appendix B
Sample Analysis Summary
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
% Moisture
Dry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID SE-POND
10640325001
U230124B_10
SMT
NA
1040 mL
NA
U221005
U230124A_16 & U230124B_16
BLANK-103673
Matrix
Dilution
Collected
Received
Extracted
Analyzed
Water
NA
01/17/2023 11:45
01/19/2023 08:50
01/20/2023 11:30
01/25/2023 07:25
Client - Pace Analytical National
Method 8290 Sample Analysis Results
NativeIsomers Conc
pg/L pg/L
InternalStandards Addedng's PercentRecoveryEMPC
pg/L
RL
2,3,7,8-TCDD ND 10 2,3,7,8-TCDD-13C 2.00 69-----
Recovery Standard1,2,3,4-TCDD-13C 2.00 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 86
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
R=Recovery outside target range
E=Exceeds calibration range
RL = Reporting Limit
Page 9 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
% Moisture
Dry Weight Extracted
ICAL ID
CCal Filename(s)
Method Blank ID
Client's Sample ID OUTFALL #1
10640325002
U230124B_11
SMT
NA
1040 mL
NA
U221005
U230124A_16 & U230124B_16
BLANK-103673
Matrix
Dilution
Collected
Received
Extracted
Analyzed
Water
NA
01/17/2023 13:20
01/19/2023 08:50
01/20/2023 11:30
01/25/2023 08:11
Client - Pace Analytical National
Method 8290 Sample Analysis Results
NativeIsomers Conc
pg/L pg/L
InternalStandards Addedng's PercentRecoveryEMPC
pg/L
RL
2,3,7,8-TCDD ND 10 2,3,7,8-TCDD-13C 2.00 53-----
Recovery Standard1,2,3,4-TCDD-13C 2.00 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 63
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration
ND = Not Detected
NA = Not Applicable
NC = Not Calculated
R=Recovery outside target range
E=Exceeds calibration range
RL = Reporting Limit
Page 10 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL ID
CCal Filename(s)
BLANK-103673
U230124B_09
SMT
979 mL
U221005
U230124A_16 & U230124B_16
Matrix
Dilution
Extracted
Analyzed
Water
01/20/2023 11:30
01/25/2023 06:39
NA
Method 8290 Blank Analysis Results
Lab Sample Name DFBLKMT
NativeIsomers pg/L
Conc EMPC
pg/L pg/L
InternalStandards Addedng's PercentRecoveryRL
2,3,7,8-TCDD ND -----10 2,3,7,8-TCDD-13C 2.00 61
Recovery Standard1,2,3,4-TCDD-13C 2.00 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 75
Conc =Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC =Estimated Maximum Possible Concentration
R =Recovery outside target range
E =Exceeds calibration range
RL =Reporting Limit
Page 11 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL ID
CCal Filename(s)
LCS-103674
L230125A_17
SMT
1010 mL
L220811
L230125A_01 & L230125A_19
Matrix
Dilution
Extracted
Analyzed
Water
01/20/2023 11:30
01/25/2023 21:09
NA
Method Blank ID BLANK-103673
Method 8290 Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDD 0.20 0.21 2,3,7,8-TCDD-13C 2.0 36104 R
Recovery Standard1,2,3,4-TCDD-13C 2.0 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 45
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressed as Percent)
R=Recovery outside of target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
* =See Discussion
Page 12 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Lab Sample ID
Injected By
Filename
Total Amount Extracted
ICAL ID
CCal Filename(s)
LCSD-103675
L230125B_13
SMT
995 mL
L220811
L230125A_19 & L230125B_14
Matrix
Dilution
Extracted
Analyzed
Water
01/20/2023 11:30
01/26/2023 07:31
NA
Method Blank ID BLANK-103673
Method 8290 Laboratory Control Spike Results
Native Qs Qm Internal ng's PercentRecoveryIsomersStandardsAdded%
Rec.(ng) (ng)
2,3,7,8-TCDD 0.20 0.22 2,3,7,8-TCDD-13C 2.0 48111
Recovery Standard1,2,3,4-TCDD-13C 2.0 NA
Cleanup Standard2,3,7,8-TCDD-37Cl4 0.20 56
Qs = Quantity Spiked
Qm = Quantity Measured
Rec.=Recovery (Expressed as Percent)
R=Recovery outside of target range
Y =RF averaging used in calculations
Nn =Value obtained from additional analysis
NA = Not Applicable
* =See Discussion
Page 13 of 14Report No.....10640325_SW8290TCDD_L2_dfr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.
Pace Analytical Services,LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
Tel:[phone]
Fax:[phone]
Client
Spike 1 ID
Spike 1 Filename L230125A_17
LCS-103674
Pace Analytical National
Spike Recovery Relative Percent Difference (RPD) Results
Spike 2 ID
Spike 2 Filename L230125B_13
LCSD-103675
Method 8290
Spike 1 Spike 2Compound%REC %REC %RPD
2,3,7,8-TCDD 104 111 6.5
%REC = Percent Recovered
RPD =The difference between the two values divided by the mean value
Page 14 of 14Report No.....10640325_SW8290TCDD_L2_dfr
ANALYTICAL REPORT
February 20, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1586780
Samples Received:02/07/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
February 20, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1586780 02/20/23 13:42 1 of 21
February 20, 2023
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1586780 02/20/23 13:46 1 of 21
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
CD-3 L1586780-01 5
CB-4 L1586780-02 6
SS-5 L1586780-03 7
SS-6 L1586780-04 8
SS-7 L1586780-05 9
CB-1 L1586780-06 10
CB-2 L1586780-07 11
Qc: Quality Control Summary 12
Total Solids by Method 2540 G-2011 12
Volatile Organic Compounds (GC) by Method 8015D/GRO 15
Gl: Glossary of Terms 16
Al: Accreditations & Locations 17
Sc: Sample Chain of Custody 18
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1586780 02/20/23 13:42 2 of 21
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1586780 02/20/23 13:46 2 of 21
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CD-3 L1586780-01 Solid Richiz T 02/02/23 08:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 MAS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 25 02/02/23 08:50 02/17/23 23:40 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-4 L1586780-02 Solid Richiz T 02/02/23 09:20 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 MAS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 36.3 02/02/23 09:20 02/18/23 00:01 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-5 L1586780-03 Solid Richiz T 02/02/23 09:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 MAS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 26.3 02/02/23 09:50 02/18/23 00:21 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-6 L1586780-04 Solid Richiz T 02/02/23 10:25 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2008111 1 02/17/23 14:23 02/17/23 14:53 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 25.8 02/02/23 10:25 02/18/23 00:42 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-7 L1586780-05 Solid Richiz T 02/02/23 10:10 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2008112 1 02/18/23 09:51 02/18/23 10:25 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 28.7 02/02/23 10:10 02/18/23 01:02 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-1 L1586780-06 Solid Richiz T 02/02/23 14:30 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 MAS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 34.3 02/02/23 14:30 02/18/23 01:23 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-2 L1586780-07 Solid Richiz T 02/02/23 14:45 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 MAS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2008397 31 02/02/23 14:45 02/18/23 01:44 ADM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1586780
CD-3
Collected date/time: 02/02/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.7 1 02/08/2023 17:47 WG2002024
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 4.55 25 02/17/2023 23:40 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 96.7 77.0-120 02/17/2023 23:40 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1586780
CB-4
Collected date/time: 02/02/23 09:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 65.0 1 02/08/2023 17:47 WG2002024
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 6.93 36.3 02/18/2023 00:01 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 97.6 77.0-120 02/18/2023 00:01 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1586780
SS-5
Collected date/time: 02/02/23 09:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.8 1 02/08/2023 17:47 WG2002024
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 3.21 26.3 02/18/2023 00:21 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 96.4 77.0-120 02/18/2023 00:21 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1586780
SS-6
Collected date/time: 02/02/23 10:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 71.7 1 02/17/2023 14:53 WG2008111
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 4.58 25.8 02/18/2023 00:42 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 94.5 77.0-120 02/18/2023 00:42 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1586780
SS-7
Collected date/time: 02/02/23 10:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.2 1 02/18/2023 10:25 WG2008112
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 4.64 28.7 02/18/2023 01:02 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 96.3 77.0-120 02/18/2023 01:02 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1586780
CB-1
Collected date/time: 02/02/23 14:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.6 1 02/08/2023 17:47 WG2002024
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 5.55 34.3 02/18/2023 01:23 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 96.4 77.0-120 02/18/2023 01:23 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1586780
CB-2
Collected date/time: 02/02/23 14:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 68.4 1 02/08/2023 17:47 WG2002024
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND T8 5.69 31 02/18/2023 01:44 WG2008397
(S) a,a,a-Trifluorotoluene(FID) 96.7 77.0-120 02/18/2023 01:44 WG2008397
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002024
Total Solids by Method 2540 G-2011 L1586780-01,02,03,06,07
Method Blank (MB)
(MB) R3889031-1 02/08/23 17:47
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1582922-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1582922-04 02/08/23 17:47 • (DUP) R3889031-3 02/08/23 17:47
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 82.2 82.5 1 0.367 10
Laboratory Control Sample (LCS)
(LCS) R3889031-2 02/08/23 17:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2008111
Total Solids by Method 2540 G-2011 L1586780-04
Method Blank (MB)
(MB) R3892239-1 02/17/23 14:53
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1586725-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1586725-01 02/17/23 14:53 • (DUP) R3892239-3 02/17/23 14:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 80.5 81.2 1 0.806 10
Laboratory Control Sample (LCS)
(LCS) R3892239-2 02/17/23 14:53
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2008112
Total Solids by Method 2540 G-2011 L1586780-05
Method Blank (MB)
(MB) R3892559-1 02/18/23 10:25
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00400
L1586252-17 Original Sample (OS) • Duplicate (DUP)
(OS) L1586252-17 02/18/23 10:25 • (DUP) R3892559-3 02/18/23 10:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 82.5 83.4 1 1.14 10
Laboratory Control Sample (LCS)
(LCS) R3892559-2 02/18/23 10:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2008397
Volatile Organic Compounds (GC) by Method 8015D/GRO L1586780-01,02,03,04,05,06,07
Method Blank (MB)
(MB) R3892262-2 02/17/23 20:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.815 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)97.4 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3892262-1 02/17/23 18:59
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.85 106 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 113 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
T8 Sample(s) received past/too close to holding time expiration.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
February 16, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1582929
Samples Received:02/07/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
February 16, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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February 16, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
CD-3 L1582929-01 6
CB-4 L1582929-02 9
SS-5 L1582929-03 12
CB-1 L1582929-06 15
CB-2 L1582929-07 18
Qc: Quality Control Summary 21
Total Solids by Method 2540 G-2011 21
Wet Chemistry by Method 7199 22
Mercury by Method 7471A 23
Metals (ICP) by Method 6010B 24
Volatile Organic Compounds (GC/MS) by Method 8260B 26
Semi-Volatile Organic Compounds (GC) by Method 8015 38
Polychlorinated Biphenyls (GC) by Method 8082 39
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 42
Gl: Glossary of Terms 46
Al: Accreditations & Locations 47
Sc: Sample Chain of Custody 48
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CD-3 L1582929-01 Solid Richiz T 02/02/23 08:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2002122 1 02/08/23 13:05 02/09/23 11:20 ARD Mt. Juliet, TN
Mercury by Method 7471A WG2002055 1 02/08/23 07:16 02/08/23 11:49 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2002164 1 02/08/23 09:22 02/08/23 20:35 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2002807 1 02/02/23 08:50 02/09/23 04:23 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 5 02/08/23 15:38 02/09/23 02:23 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001937 5 02/08/23 06:18 02/08/23 17:30 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2002084 4.98 02/08/23 18:31 02/09/23 06:43 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-4 L1582929-02 Solid Richiz T 02/02/23 08:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2002122 1 02/08/23 13:05 02/09/23 11:25 ARD Mt. Juliet, TN
Mercury by Method 7471A WG2002055 1 02/08/23 07:16 02/08/23 11:52 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2002164 1 02/08/23 09:22 02/08/23 20:38 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2002811 1.45 02/02/23 08:50 02/09/23 03:39 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 10 02/08/23 15:38 02/09/23 02:48 KAP Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 100 02/08/23 15:38 02/09/23 10:20 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001937 1 02/08/23 06:18 02/08/23 17:39 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2002084 1 02/08/23 18:31 02/09/23 07:03 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-5 L1582929-03 Solid Richiz T 02/02/23 08:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2002122 1 02/08/23 13:05 02/09/23 11:31 ARD Mt. Juliet, TN
Mercury by Method 7471A WG2002055 1 02/08/23 07:16 02/08/23 11:54 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2002164 1 02/08/23 09:22 02/08/23 20:40 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2002811 1.05 02/02/23 08:50 02/09/23 03:58 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 20 02/08/23 15:38 02/09/23 02:11 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001943 1 02/08/23 11:09 02/09/23 09:39 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2002084 1 02/08/23 18:31 02/10/23 00:28 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-1 L1582929-06 Solid Richiz T 02/02/23 08:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2002122 1 02/08/23 13:05 02/09/23 12:02 ARD Mt. Juliet, TN
Mercury by Method 7471A WG2002055 1 02/08/23 07:16 02/08/23 11:59 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2002164 1 02/08/23 09:22 02/08/23 20:29 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2002811 1.37 02/02/23 08:50 02/09/23 04:18 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 1 02/08/23 15:38 02/09/23 02:11 KAP Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 10 02/08/23 15:38 02/09/23 10:20 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001943 1 02/08/23 11:09 02/09/23 23:50 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2002084 1 02/08/23 18:31 02/09/23 07:22 JRM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CB-2 L1582929-07 Solid Richiz T 02/02/23 08:50 02/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2002024 1 02/08/23 17:34 02/08/23 17:47 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2002122 1 02/08/23 13:05 02/09/23 12:07 ARD Mt. Juliet, TN
Mercury by Method 7471A WG2002055 1 02/08/23 07:16 02/08/23 12:02 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2002164 1 02/08/23 09:22 02/08/23 20:32 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2002811 1.24 02/02/23 08:50 02/09/23 04:37 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2002546 5 02/08/23 15:38 02/09/23 01:58 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2002078 1 02/10/23 06:11 02/11/23 00:48 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2002085 1 02/08/23 09:49 02/08/23 20:32 JCH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1582929
CD-3
Collected date/time: 02/02/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.7 1 02/08/2023 17:47 WG2002024
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium 1.60 1.30 1 02/09/2023 11:20 WG2002122
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0521 1 02/08/2023 11:49 WG2002055
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.61 1 02/08/2023 20:35 WG2002164
Arsenic 4.22 2.61 1 02/08/2023 20:35 WG2002164
Beryllium 0.328 0.261 1 02/08/2023 20:35 WG2002164
Cadmium ND 0.652 1 02/08/2023 20:35 WG2002164
Chromium 81.6 1.30 1 02/08/2023 20:35 WG2002164
Copper 64.7 2.61 1 02/08/2023 20:35 WG2002164
Lead 12.7 0.652 1 02/08/2023 20:35 WG2002164
Nickel 26.8 2.61 1 02/08/2023 20:35 WG2002164
Selenium ND 2.61 1 02/08/2023 20:35 WG2002164
Silver ND 1.30 1 02/08/2023 20:35 WG2002164
Thallium ND 2.61 1 02/08/2023 20:35 WG2002164
Zinc 76.7 6.52 1 02/08/2023 20:35 WG2002164
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0911 1 02/09/2023 04:23 WG2002807
Acrylonitrile ND 0.0228 1 02/09/2023 04:23 WG2002807
Benzene ND 0.00182 1 02/09/2023 04:23 WG2002807
Bromobenzene ND 0.0228 1 02/09/2023 04:23 WG2002807
Bromodichloromethane ND 0.00455 1 02/09/2023 04:23 WG2002807
Bromoform ND 0.0455 1 02/09/2023 04:23 WG2002807
Bromomethane ND 0.0228 1 02/09/2023 04:23 WG2002807
n-Butylbenzene ND 0.0228 1 02/09/2023 04:23 WG2002807
sec-Butylbenzene ND 0.0228 1 02/09/2023 04:23 WG2002807
tert-Butylbenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
Carbon tetrachloride ND 0.00911 1 02/09/2023 04:23 WG2002807
Chlorobenzene ND 0.00455 1 02/09/2023 04:23 WG2002807
Chlorodibromomethane ND 0.00455 1 02/09/2023 04:23 WG2002807
Chloroethane ND 0.00911 1 02/09/2023 04:23 WG2002807
Chloroform ND 0.00455 1 02/09/2023 04:23 WG2002807
Chloromethane ND 0.0228 1 02/09/2023 04:23 WG2002807
2-Chlorotoluene ND 0.00455 1 02/09/2023 04:23 WG2002807
4-Chlorotoluene ND 0.00911 1 02/09/2023 04:23 WG2002807
1,2-Dibromo-3-Chloropropane ND 0.0455 1 02/09/2023 04:23 WG2002807
1,2-Dibromoethane ND 0.00455 1 02/09/2023 04:23 WG2002807
Dibromomethane ND 0.00911 1 02/09/2023 04:23 WG2002807
1,2-Dichlorobenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
1,3-Dichlorobenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1582929
CD-3
Collected date/time: 02/02/23 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,4-Dichlorobenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
Dichlorodifluoromethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,1-Dichloroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,2-Dichloroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,1-Dichloroethene ND 0.00455 1 02/09/2023 04:23 WG2002807
cis-1,2-Dichloroethene ND 0.00455 1 02/09/2023 04:23 WG2002807
trans-1,2-Dichloroethene ND 0.00911 1 02/09/2023 04:23 WG2002807
1,2-Dichloropropane ND 0.00911 1 02/09/2023 04:23 WG2002807
1,1-Dichloropropene ND 0.00455 1 02/09/2023 04:23 WG2002807
1,3-Dichloropropane ND 0.00911 1 02/09/2023 04:23 WG2002807
cis-1,3-Dichloropropene ND 0.00455 1 02/09/2023 04:23 WG2002807
trans-1,3-Dichloropropene ND 0.00911 1 02/09/2023 04:23 WG2002807
2,2-Dichloropropane ND 0.00455 1 02/09/2023 04:23 WG2002807
Di-isopropyl ether ND 0.00182 1 02/09/2023 04:23 WG2002807
Ethylbenzene ND 0.00455 1 02/09/2023 04:23 WG2002807
Hexachloro-1,3-butadiene ND 0.0455 1 02/09/2023 04:23 WG2002807
Isopropylbenzene ND 0.00455 1 02/09/2023 04:23 WG2002807
p-Isopropyltoluene ND 0.00911 1 02/09/2023 04:23 WG2002807
2-Butanone (MEK)ND 0.182 1 02/09/2023 04:23 WG2002807
Methylene Chloride ND 0.0455 1 02/09/2023 04:23 WG2002807
4-Methyl-2-pentanone (MIBK) ND 0.0455 1 02/09/2023 04:23 WG2002807
Methyl tert-butyl ether ND 0.00182 1 02/09/2023 04:23 WG2002807
Naphthalene ND 0.0228 1 02/09/2023 04:23 WG2002807
n-Propylbenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
Styrene ND 0.0228 1 02/09/2023 04:23 WG2002807
1,1,1,2-Tetrachloroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,1,2,2-Tetrachloroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,1,2-Trichlorotrifluoroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
Tetrachloroethene ND 0.00455 1 02/09/2023 04:23 WG2002807
Toluene ND 0.00911 1 02/09/2023 04:23 WG2002807
1,2,3-Trichlorobenzene ND 0.0228 1 02/09/2023 04:23 WG2002807
1,2,4-Trichlorobenzene ND 0.0228 1 02/09/2023 04:23 WG2002807
1,1,1-Trichloroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,1,2-Trichloroethane ND 0.00455 1 02/09/2023 04:23 WG2002807
Trichloroethene ND 0.00182 1 02/09/2023 04:23 WG2002807
Trichlorofluoromethane ND 0.00455 1 02/09/2023 04:23 WG2002807
1,2,3-Trichloropropane ND 0.0228 1 02/09/2023 04:23 WG2002807
1,2,4-Trimethylbenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
1,2,3-Trimethylbenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
1,3,5-Trimethylbenzene ND 0.00911 1 02/09/2023 04:23 WG2002807
Vinyl chloride ND 0.00455 1 02/09/2023 04:23 WG2002807
Xylenes, Total ND 0.0118 1 02/09/2023 04:23 WG2002807
(S) Toluene-d8 110 75.0-131 02/09/2023 04:23 WG2002807
(S) 4-Bromofluorobenzene 88.4 67.0-138 02/09/2023 04:23 WG2002807
(S) 1,2-Dichloroethane-d4 86.4 70.0-130 02/09/2023 04:23 WG2002807
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 122 26.1 5 02/09/2023 02:23 WG2002546
C28-C40 Oil Range 314 26.1 5 02/09/2023 02:23 WG2002546
(S) o-Terphenyl 62.3 18.0-148 02/09/2023 02:23 WG2002546
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1582929
CD-3
Collected date/time: 02/02/23 08:50
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.222 5 02/08/2023 17:30 WG2001937
PCB 1221 ND 0.222 5 02/08/2023 17:30 WG2001937
PCB 1232 ND 0.222 5 02/08/2023 17:30 WG2001937
PCB 1242 ND 0.222 5 02/08/2023 17:30 WG2001937
PCB 1248 ND 0.111 5 02/08/2023 17:30 WG2001937
PCB 1254 ND 0.111 5 02/08/2023 17:30 WG2001937
PCB 1260 ND 0.111 5 02/08/2023 17:30 WG2001937
(S) Decachlorobiphenyl 78.4 10.0-135 02/08/2023 17:30 WG2001937
(S) Tetrachloro-m-xylene 72.1 10.0-139 02/08/2023 17:30 WG2001937
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Acenaphthene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Acenaphthylene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Benzo(a)anthracene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Benzo(a)pyrene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Benzo(b)fluoranthene 0.0429 0.0390 4.98 02/09/2023 06:43 WG2002084
Benzo(g,h,i)perylene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Benzo(k)fluoranthene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Chrysene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Dibenz(a,h)anthracene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Fluoranthene 0.0554 0.0390 4.98 02/09/2023 06:43 WG2002084
Fluorene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Indeno(1,2,3-cd)pyrene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Naphthalene ND 0.130 4.98 02/09/2023 06:43 WG2002084
Phenanthrene ND 0.0390 4.98 02/09/2023 06:43 WG2002084
Pyrene 0.0481 0.0390 4.98 02/09/2023 06:43 WG2002084
1-Methylnaphthalene ND 0.130 4.98 02/09/2023 06:43 WG2002084
2-Methylnaphthalene ND 0.130 4.98 02/09/2023 06:43 WG2002084
2-Chloronaphthalene ND 0.130 4.98 02/09/2023 06:43 WG2002084
(S) p-Terphenyl-d14 85.3 23.0-120 02/09/2023 06:43 WG2002084
(S) Nitrobenzene-d5 48.1 14.0-149 02/09/2023 06:43 WG2002084
(S) 2-Fluorobiphenyl 73.6 34.0-125 02/09/2023 06:43 WG2002084
Sample Narrative:
L1582929-01 WG2002084: Dilution due to matrix impact during extraction procedure
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1582929
CB-4
Collected date/time: 02/02/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 65.0 1 02/08/2023 17:47 WG2002024
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.54 1 02/09/2023 11:25 WG2002122
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0615 1 02/08/2023 11:52 WG2002055
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 3.08 1 02/08/2023 20:38 WG2002164
Arsenic 9.52 3.08 1 02/08/2023 20:38 WG2002164
Beryllium 0.401 0.308 1 02/08/2023 20:38 WG2002164
Cadmium 0.855 0.769 1 02/08/2023 20:38 WG2002164
Chromium 85.5 1.54 1 02/08/2023 20:38 WG2002164
Copper 183 3.08 1 02/08/2023 20:38 WG2002164
Lead 23.2 0.769 1 02/08/2023 20:38 WG2002164
Nickel 152 3.08 1 02/08/2023 20:38 WG2002164
Selenium ND 3.08 1 02/08/2023 20:38 WG2002164
Silver ND 1.54 1 02/08/2023 20:38 WG2002164
Thallium ND 3.08 1 02/08/2023 20:38 WG2002164
Zinc 471 7.69 1 02/08/2023 20:38 WG2002164
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.138 1.45 02/09/2023 03:39 WG2002811
Acrylonitrile ND 0.0346 1.45 02/09/2023 03:39 WG2002811
Benzene 0.00588 0.00277 1.45 02/09/2023 03:39 WG2002811
Bromobenzene ND 0.0346 1.45 02/09/2023 03:39 WG2002811
Bromodichloromethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Bromoform ND 0.0693 1.45 02/09/2023 03:39 WG2002811
Bromomethane ND 0.0346 1.45 02/09/2023 03:39 WG2002811
n-Butylbenzene ND 0.0346 1.45 02/09/2023 03:39 WG2002811
sec-Butylbenzene ND 0.0346 1.45 02/09/2023 03:39 WG2002811
tert-Butylbenzene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
Carbon tetrachloride ND 0.0138 1.45 02/09/2023 03:39 WG2002811
Chlorobenzene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Chlorodibromomethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Chloroethane ND 0.0138 1.45 02/09/2023 03:39 WG2002811
Chloroform ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Chloromethane ND 0.0346 1.45 02/09/2023 03:39 WG2002811
2-Chlorotoluene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
4-Chlorotoluene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
1,2-Dibromo-3-Chloropropane ND 0.0693 1.45 02/09/2023 03:39 WG2002811
1,2-Dibromoethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Dibromomethane ND 0.0138 1.45 02/09/2023 03:39 WG2002811
1,2-Dichlorobenzene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
1,3-Dichlorobenzene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1582929
CB-4
Collected date/time: 02/02/23 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,4-Dichlorobenzene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
Dichlorodifluoromethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,1-Dichloroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,2-Dichloroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,1-Dichloroethene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
cis-1,2-Dichloroethene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
trans-1,2-Dichloroethene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
1,2-Dichloropropane ND 0.0138 1.45 02/09/2023 03:39 WG2002811
1,1-Dichloropropene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,3-Dichloropropane ND 0.0138 1.45 02/09/2023 03:39 WG2002811
cis-1,3-Dichloropropene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
trans-1,3-Dichloropropene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
2,2-Dichloropropane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Di-isopropyl ether ND 0.00277 1.45 02/09/2023 03:39 WG2002811
Ethylbenzene 0.00747 0.00693 1.45 02/09/2023 03:39 WG2002811
Hexachloro-1,3-butadiene ND 0.0693 1.45 02/09/2023 03:39 WG2002811
Isopropylbenzene ND 0.00693 1.45 02/09/2023 03:39 WG2002811
p-Isopropyltoluene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
2-Butanone (MEK)ND 0.277 1.45 02/09/2023 03:39 WG2002811
Methylene Chloride ND 0.0693 1.45 02/09/2023 03:39 WG2002811
4-Methyl-2-pentanone (MIBK) ND 0.0693 1.45 02/09/2023 03:39 WG2002811
Methyl tert-butyl ether ND 0.00277 1.45 02/09/2023 03:39 WG2002811
Naphthalene 0.0602 0.0346 1.45 02/09/2023 03:39 WG2002811
n-Propylbenzene ND 0.0138 1.45 02/09/2023 03:39 WG2002811
Styrene 0.896 0.0346 1.45 02/09/2023 03:39 WG2002811
1,1,1,2-Tetrachloroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,1,2,2-Tetrachloroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,1,2-Trichlorotrifluoroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Tetrachloroethene 0.567 0.00693 1.45 02/09/2023 03:39 WG2002811
Toluene 0.0296 0.0138 1.45 02/09/2023 03:39 WG2002811
1,2,3-Trichlorobenzene ND 0.0346 1.45 02/09/2023 03:39 WG2002811
1,2,4-Trichlorobenzene ND 0.0346 1.45 02/09/2023 03:39 WG2002811
1,1,1-Trichloroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
1,1,2-Trichloroethane ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Trichloroethene ND 0.00277 1.45 02/09/2023 03:39 WG2002811
Trichlorofluoromethane 0.0920 0.00693 1.45 02/09/2023 03:39 WG2002811
1,2,3-Trichloropropane ND 0.0346 1.45 02/09/2023 03:39 WG2002811
1,2,4-Trimethylbenzene 0.0665 0.0138 1.45 02/09/2023 03:39 WG2002811
1,2,3-Trimethylbenzene 0.0430 0.0138 1.45 02/09/2023 03:39 WG2002811
1,3,5-Trimethylbenzene 0.0169 0.0138 1.45 02/09/2023 03:39 WG2002811
Vinyl chloride ND 0.00693 1.45 02/09/2023 03:39 WG2002811
Xylenes, Total 0.0458 0.0180 1.45 02/09/2023 03:39 WG2002811
(S) Toluene-d8 104 75.0-131 02/09/2023 03:39 WG2002811
(S) 4-Bromofluorobenzene 84.4 67.0-138 02/09/2023 03:39 WG2002811
(S) 1,2-Dichloroethane-d4 61.5 J2 70.0-130 02/09/2023 03:39 WG2002811
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 3600 61.5 10 02/09/2023 02:48 WG2002546
C28-C40 Oil Range 9080 615 100 02/09/2023 10:20 WG2002546
(S) o-Terphenyl 53.7 18.0-148 02/09/2023 02:48 WG2002546
(S) o-Terphenyl 0.000 J7 18.0-148 02/09/2023 10:20 WG2002546
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1582929
CB-4
Collected date/time: 02/02/23 08:50
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0523 1 02/08/2023 17:39 WG2001937
PCB 1221 ND 0.0523 1 02/08/2023 17:39 WG2001937
PCB 1232 ND 0.0523 1 02/08/2023 17:39 WG2001937
PCB 1242 ND 0.0523 1 02/08/2023 17:39 WG2001937
PCB 1248 ND 0.0262 1 02/08/2023 17:39 WG2001937
PCB 1254 ND 0.0262 1 02/08/2023 17:39 WG2001937
PCB 1260 ND 0.0262 1 02/08/2023 17:39 WG2001937
(S) Decachlorobiphenyl 60.8 10.0-135 02/08/2023 17:39 WG2001937
(S) Tetrachloro-m-xylene 51.9 10.0-139 02/08/2023 17:39 WG2001937
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00923 1 02/09/2023 07:03 WG2002084
Acenaphthene ND 0.00923 1 02/09/2023 07:03 WG2002084
Acenaphthylene ND 0.00923 1 02/09/2023 07:03 WG2002084
Benzo(a)anthracene 0.0220 0.00923 1 02/09/2023 07:03 WG2002084
Benzo(a)pyrene 0.0155 0.00923 1 02/09/2023 07:03 WG2002084
Benzo(b)fluoranthene 0.0311 0.00923 1 02/09/2023 07:03 WG2002084
Benzo(g,h,i)perylene 0.0278 0.00923 1 02/09/2023 07:03 WG2002084
Benzo(k)fluoranthene ND 0.00923 1 02/09/2023 07:03 WG2002084
Chrysene 0.0228 0.00923 1 02/09/2023 07:03 WG2002084
Dibenz(a,h)anthracene ND 0.00923 1 02/09/2023 07:03 WG2002084
Fluoranthene 0.0597 0.00923 1 02/09/2023 07:03 WG2002084
Fluorene ND 0.00923 1 02/09/2023 07:03 WG2002084
Indeno(1,2,3-cd)pyrene 0.0162 0.00923 1 02/09/2023 07:03 WG2002084
Naphthalene 0.0637 0.0308 1 02/09/2023 07:03 WG2002084
Phenanthrene 0.0965 0.00923 1 02/09/2023 07:03 WG2002084
Pyrene 0.178 0.00923 1 02/09/2023 07:03 WG2002084
1-Methylnaphthalene 0.195 0.0308 1 02/09/2023 07:03 WG2002084
2-Methylnaphthalene 0.248 0.0308 1 02/09/2023 07:03 WG2002084
2-Chloronaphthalene ND 0.0308 1 02/09/2023 07:03 WG2002084
(S) p-Terphenyl-d14 82.6 23.0-120 02/09/2023 07:03 WG2002084
(S) Nitrobenzene-d5 0.000 J2 14.0-149 02/09/2023 07:03 WG2002084
(S) 2-Fluorobiphenyl 66.2 34.0-125 02/09/2023 07:03 WG2002084
Sample Narrative:
L1582929-02 WG2002084: Surrogate failure due to matrix interference
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1582929
SS-5
Collected date/time: 02/02/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.8 1 02/08/2023 17:47 WG2002024
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.11 1 02/09/2023 11:31 WG2002122
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0445 1 02/08/2023 11:54 WG2002055
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.23 1 02/08/2023 20:40 WG2002164
Arsenic 5.68 2.23 1 02/08/2023 20:40 WG2002164
Beryllium 0.433 0.223 1 02/08/2023 20:40 WG2002164
Cadmium ND 0.557 1 02/08/2023 20:40 WG2002164
Chromium 30.3 1.11 1 02/08/2023 20:40 WG2002164
Copper 39.7 2.23 1 02/08/2023 20:40 WG2002164
Lead 12.9 0.557 1 02/08/2023 20:40 WG2002164
Nickel 18.9 2.23 1 02/08/2023 20:40 WG2002164
Selenium ND 2.23 1 02/08/2023 20:40 WG2002164
Silver ND 1.11 1 02/08/2023 20:40 WG2002164
Thallium ND 2.23 1 02/08/2023 20:40 WG2002164
Zinc 45.3 5.57 1 02/08/2023 20:40 WG2002164
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0641 1.05 02/09/2023 03:58 WG2002811
Acrylonitrile ND 0.0160 1.05 02/09/2023 03:58 WG2002811
Benzene ND 0.00128 1.05 02/09/2023 03:58 WG2002811
Bromobenzene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
Bromodichloromethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Bromoform ND 0.0321 1.05 02/09/2023 03:58 WG2002811
Bromomethane ND 0.0160 1.05 02/09/2023 03:58 WG2002811
n-Butylbenzene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
sec-Butylbenzene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
tert-Butylbenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
Carbon tetrachloride ND 0.00641 1.05 02/09/2023 03:58 WG2002811
Chlorobenzene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Chlorodibromomethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Chloroethane ND 0.00641 1.05 02/09/2023 03:58 WG2002811
Chloroform ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Chloromethane ND 0.0160 1.05 02/09/2023 03:58 WG2002811
2-Chlorotoluene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
4-Chlorotoluene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,2-Dibromo-3-Chloropropane ND 0.0321 1.05 02/09/2023 03:58 WG2002811
1,2-Dibromoethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Dibromomethane ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,2-Dichlorobenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,3-Dichlorobenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Tetra Tech Inc. - UT L1582929 02/16/23 16:33 12 of 49
SAMPLE RESULTS - 03
L1582929
SS-5
Collected date/time: 02/02/23 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,4-Dichlorobenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
Dichlorodifluoromethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,1-Dichloroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,2-Dichloroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,1-Dichloroethene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
cis-1,2-Dichloroethene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
trans-1,2-Dichloroethene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,2-Dichloropropane ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,1-Dichloropropene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,3-Dichloropropane ND 0.00641 1.05 02/09/2023 03:58 WG2002811
cis-1,3-Dichloropropene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
trans-1,3-Dichloropropene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
2,2-Dichloropropane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Di-isopropyl ether ND 0.00128 1.05 02/09/2023 03:58 WG2002811
Ethylbenzene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Hexachloro-1,3-butadiene ND 0.0321 1.05 02/09/2023 03:58 WG2002811
Isopropylbenzene ND 0.00321 1.05 02/09/2023 03:58 WG2002811
p-Isopropyltoluene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
2-Butanone (MEK)ND 0.128 1.05 02/09/2023 03:58 WG2002811
Methylene Chloride ND 0.0321 1.05 02/09/2023 03:58 WG2002811
4-Methyl-2-pentanone (MIBK) ND 0.0321 1.05 02/09/2023 03:58 WG2002811
Methyl tert-butyl ether ND 0.00128 1.05 02/09/2023 03:58 WG2002811
Naphthalene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
n-Propylbenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
Styrene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
1,1,1,2-Tetrachloroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,1,2,2-Tetrachloroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,1,2-Trichlorotrifluoroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Tetrachloroethene 0.00552 0.00321 1.05 02/09/2023 03:58 WG2002811
Toluene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,2,3-Trichlorobenzene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
1,2,4-Trichlorobenzene ND 0.0160 1.05 02/09/2023 03:58 WG2002811
1,1,1-Trichloroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,1,2-Trichloroethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Trichloroethene ND 0.00128 1.05 02/09/2023 03:58 WG2002811
Trichlorofluoromethane ND 0.00321 1.05 02/09/2023 03:58 WG2002811
1,2,3-Trichloropropane ND 0.0160 1.05 02/09/2023 03:58 WG2002811
1,2,4-Trimethylbenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,2,3-Trimethylbenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
1,3,5-Trimethylbenzene ND 0.00641 1.05 02/09/2023 03:58 WG2002811
Vinyl chloride ND 0.00321 1.05 02/09/2023 03:58 WG2002811
Xylenes, Total ND 0.00834 1.05 02/09/2023 03:58 WG2002811
(S) Toluene-d8 102 75.0-131 02/09/2023 03:58 WG2002811
(S) 4-Bromofluorobenzene 79.3 67.0-138 02/09/2023 03:58 WG2002811
(S) 1,2-Dichloroethane-d4 72.1 70.0-130 02/09/2023 03:58 WG2002811
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 89.1 20 02/09/2023 02:11 WG2002546
C28-C40 Oil Range 538 89.1 20 02/09/2023 02:11 WG2002546
(S) o-Terphenyl 77.7 J7 18.0-148 02/09/2023 02:11 WG2002546
Sample Narrative:
L1582929-03 WG2002546: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 03
L1582929
SS-5
Collected date/time: 02/02/23 08:50
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0378 1 02/09/2023 09:39 WG2001943
PCB 1221 ND 0.0378 1 02/09/2023 09:39 WG2001943
PCB 1232 ND 0.0378 1 02/09/2023 09:39 WG2001943
PCB 1242 ND 0.0378 1 02/09/2023 09:39 WG2001943
PCB 1248 ND 0.0189 1 02/09/2023 09:39 WG2001943
PCB 1254 ND 0.0189 1 02/09/2023 09:39 WG2001943
PCB 1260 ND 0.0189 1 02/09/2023 09:39 WG2001943
(S) Decachlorobiphenyl 83.0 10.0-135 02/09/2023 09:39 WG2001943
(S) Tetrachloro-m-xylene 59.6 10.0-139 02/09/2023 09:39 WG2001943
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00668 1 02/10/2023 00:28 WG2002084
Acenaphthene ND 0.00668 1 02/10/2023 00:28 WG2002084
Acenaphthylene ND 0.00668 1 02/10/2023 00:28 WG2002084
Benzo(a)anthracene 0.0186 0.00668 1 02/10/2023 00:28 WG2002084
Benzo(a)pyrene 0.0273 0.00668 1 02/10/2023 00:28 WG2002084
Benzo(b)fluoranthene 0.0274 0.00668 1 02/10/2023 00:28 WG2002084
Benzo(g,h,i)perylene 0.0452 0.00668 1 02/10/2023 00:28 WG2002084
Benzo(k)fluoranthene 0.00893 0.00668 1 02/10/2023 00:28 WG2002084
Chrysene 0.0194 0.00668 1 02/10/2023 00:28 WG2002084
Dibenz(a,h)anthracene 0.00709 0.00668 1 02/10/2023 00:28 WG2002084
Fluoranthene 0.0273 0.00668 1 02/10/2023 00:28 WG2002084
Fluorene ND 0.00668 1 02/10/2023 00:28 WG2002084
Indeno(1,2,3-cd)pyrene 0.0185 0.00668 1 02/10/2023 00:28 WG2002084
Naphthalene ND 0.0223 1 02/10/2023 00:28 WG2002084
Phenanthrene 0.0136 0.00668 1 02/10/2023 00:28 WG2002084
Pyrene 0.0460 0.00668 1 02/10/2023 00:28 WG2002084
1-Methylnaphthalene ND 0.0223 1 02/10/2023 00:28 WG2002084
2-Methylnaphthalene ND 0.0223 1 02/10/2023 00:28 WG2002084
2-Chloronaphthalene ND 0.0223 1 02/10/2023 00:28 WG2002084
(S) p-Terphenyl-d14 83.0 23.0-120 02/10/2023 00:28 WG2002084
(S) Nitrobenzene-d5 51.8 14.0-149 02/10/2023 00:28 WG2002084
(S) 2-Fluorobiphenyl 59.4 34.0-125 02/10/2023 00:28 WG2002084
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 06
L1582929
CB-1
Collected date/time: 02/02/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.6 1 02/08/2023 17:47 WG2002024
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.36 1 02/09/2023 12:02 WG2002122
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0543 1 02/08/2023 11:59 WG2002055
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.72 1 02/08/2023 20:29 WG2002164
Arsenic 9.55 2.72 1 02/08/2023 20:29 WG2002164
Beryllium ND 0.272 1 02/08/2023 20:29 WG2002164
Cadmium ND 0.679 1 02/08/2023 20:29 WG2002164
Chromium 16.2 1.36 1 02/08/2023 20:29 WG2002164
Copper 17.1 2.72 1 02/08/2023 20:29 WG2002164
Lead 5.63 0.679 1 02/08/2023 20:29 WG2002164
Nickel 9.10 2.72 1 02/08/2023 20:29 WG2002164
Selenium ND 2.72 1 02/08/2023 20:29 WG2002164
Silver ND 1.36 1 02/08/2023 20:29 WG2002164
Thallium ND 2.72 1 02/08/2023 20:29 WG2002164
Zinc 37.0 6.79 1 02/08/2023 20:29 WG2002164
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.111 1.37 02/09/2023 04:18 WG2002811
Acrylonitrile ND 0.0277 1.37 02/09/2023 04:18 WG2002811
Benzene 0.00256 0.00222 1.37 02/09/2023 04:18 WG2002811
Bromobenzene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
Bromodichloromethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Bromoform ND 0.0555 1.37 02/09/2023 04:18 WG2002811
Bromomethane ND 0.0277 1.37 02/09/2023 04:18 WG2002811
n-Butylbenzene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
sec-Butylbenzene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
tert-Butylbenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
Carbon tetrachloride ND 0.0111 1.37 02/09/2023 04:18 WG2002811
Chlorobenzene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Chlorodibromomethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Chloroethane ND 0.0111 1.37 02/09/2023 04:18 WG2002811
Chloroform ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Chloromethane ND 0.0277 1.37 02/09/2023 04:18 WG2002811
2-Chlorotoluene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
4-Chlorotoluene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1,2-Dibromo-3-Chloropropane ND 0.0555 1.37 02/09/2023 04:18 WG2002811
1,2-Dibromoethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Dibromomethane ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1,2-Dichlorobenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1,3-Dichlorobenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 06
L1582929
CB-1
Collected date/time: 02/02/23 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,4-Dichlorobenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
Dichlorodifluoromethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,1-Dichloroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,2-Dichloroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,1-Dichloroethene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
cis-1,2-Dichloroethene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
trans-1,2-Dichloroethene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1,2-Dichloropropane ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1,1-Dichloropropene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,3-Dichloropropane ND 0.0111 1.37 02/09/2023 04:18 WG2002811
cis-1,3-Dichloropropene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
trans-1,3-Dichloropropene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
2,2-Dichloropropane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Di-isopropyl ether ND 0.00222 1.37 02/09/2023 04:18 WG2002811
Ethylbenzene 0.00638 0.00555 1.37 02/09/2023 04:18 WG2002811
Hexachloro-1,3-butadiene ND 0.0555 1.37 02/09/2023 04:18 WG2002811
Isopropylbenzene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
p-Isopropyltoluene 0.0910 0.0111 1.37 02/09/2023 04:18 WG2002811
2-Butanone (MEK)ND 0.222 1.37 02/09/2023 04:18 WG2002811
Methylene Chloride ND 0.0555 1.37 02/09/2023 04:18 WG2002811
4-Methyl-2-pentanone (MIBK) ND 0.0555 1.37 02/09/2023 04:18 WG2002811
Methyl tert-butyl ether ND 0.00222 1.37 02/09/2023 04:18 WG2002811
Naphthalene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
n-Propylbenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
Styrene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
1,1,1,2-Tetrachloroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,1,2,2-Tetrachloroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,1,2-Trichlorotrifluoroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Tetrachloroethene ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Toluene 0.130 0.0111 1.37 02/09/2023 04:18 WG2002811
1,2,3-Trichlorobenzene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
1,2,4-Trichlorobenzene ND 0.0277 1.37 02/09/2023 04:18 WG2002811
1,1,1-Trichloroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,1,2-Trichloroethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Trichloroethene ND 0.00222 1.37 02/09/2023 04:18 WG2002811
Trichlorofluoromethane ND 0.00555 1.37 02/09/2023 04:18 WG2002811
1,2,3-Trichloropropane ND 0.0277 1.37 02/09/2023 04:18 WG2002811
1,2,4-Trimethylbenzene 0.0124 B 0.0111 1.37 02/09/2023 04:18 WG2002811
1,2,3-Trimethylbenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
1,3,5-Trimethylbenzene ND 0.0111 1.37 02/09/2023 04:18 WG2002811
Vinyl chloride ND 0.00555 1.37 02/09/2023 04:18 WG2002811
Xylenes, Total 0.0194 0.0144 1.37 02/09/2023 04:18 WG2002811
(S) Toluene-d8 98.4 75.0-131 02/09/2023 04:18 WG2002811
(S) 4-Bromofluorobenzene 79.8 67.0-138 02/09/2023 04:18 WG2002811
(S) 1,2-Dichloroethane-d4 77.9 70.0-130 02/09/2023 04:18 WG2002811
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 172 5.43 1 02/09/2023 02:11 WG2002546
C28-C40 Oil Range 585 54.3 10 02/09/2023 10:20 WG2002546
(S) o-Terphenyl 28.5 18.0-148 02/09/2023 10:20 WG2002546
(S) o-Terphenyl 38.0 18.0-148 02/09/2023 02:11 WG2002546
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 06
L1582929
CB-1
Collected date/time: 02/02/23 08:50
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0462 1 02/09/2023 23:50 WG2001943
PCB 1221 ND 0.0462 1 02/09/2023 23:50 WG2001943
PCB 1232 ND 0.0462 1 02/09/2023 23:50 WG2001943
PCB 1242 ND 0.0462 1 02/09/2023 23:50 WG2001943
PCB 1248 ND 0.0231 1 02/09/2023 23:50 WG2001943
PCB 1254 ND 0.0231 1 02/09/2023 23:50 WG2001943
PCB 1260 ND 0.0231 1 02/09/2023 23:50 WG2001943
(S) Decachlorobiphenyl 38.0 10.0-135 02/09/2023 23:50 WG2001943
(S) Tetrachloro-m-xylene 38.6 10.0-139 02/09/2023 23:50 WG2001943
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00815 1 02/09/2023 07:22 WG2002084
Acenaphthene ND 0.00815 1 02/09/2023 07:22 WG2002084
Acenaphthylene ND 0.00815 1 02/09/2023 07:22 WG2002084
Benzo(a)anthracene 0.00838 0.00815 1 02/09/2023 07:22 WG2002084
Benzo(a)pyrene ND 0.00815 1 02/09/2023 07:22 WG2002084
Benzo(b)fluoranthene 0.0105 0.00815 1 02/09/2023 07:22 WG2002084
Benzo(g,h,i)perylene 0.00970 0.00815 1 02/09/2023 07:22 WG2002084
Benzo(k)fluoranthene ND 0.00815 1 02/09/2023 07:22 WG2002084
Chrysene 0.0107 0.00815 1 02/09/2023 07:22 WG2002084
Dibenz(a,h)anthracene ND 0.00815 1 02/09/2023 07:22 WG2002084
Fluoranthene 0.0183 0.00815 1 02/09/2023 07:22 WG2002084
Fluorene ND 0.00815 1 02/09/2023 07:22 WG2002084
Indeno(1,2,3-cd)pyrene ND 0.00815 1 02/09/2023 07:22 WG2002084
Naphthalene ND 0.0272 1 02/09/2023 07:22 WG2002084
Phenanthrene 0.0163 0.00815 1 02/09/2023 07:22 WG2002084
Pyrene 0.0200 0.00815 1 02/09/2023 07:22 WG2002084
1-Methylnaphthalene ND 0.0272 1 02/09/2023 07:22 WG2002084
2-Methylnaphthalene ND 0.0272 1 02/09/2023 07:22 WG2002084
2-Chloronaphthalene ND 0.0272 1 02/09/2023 07:22 WG2002084
(S) p-Terphenyl-d14 67.5 23.0-120 02/09/2023 07:22 WG2002084
(S) Nitrobenzene-d5 42.8 14.0-149 02/09/2023 07:22 WG2002084
(S) 2-Fluorobiphenyl 53.0 34.0-125 02/09/2023 07:22 WG2002084
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1582929
CB-2
Collected date/time: 02/02/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 68.4 1 02/08/2023 17:47 WG2002024
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.46 1 02/09/2023 12:07 WG2002122
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0585 1 02/08/2023 12:02 WG2002055
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.93 1 02/08/2023 20:32 WG2002164
Arsenic 52.7 2.93 1 02/08/2023 20:32 WG2002164
Beryllium 0.405 0.293 1 02/08/2023 20:32 WG2002164
Cadmium ND 0.731 1 02/08/2023 20:32 WG2002164
Chromium 216 1.46 1 02/08/2023 20:32 WG2002164
Copper 29.6 2.93 1 02/08/2023 20:32 WG2002164
Lead 8.89 0.731 1 02/08/2023 20:32 WG2002164
Nickel 14.1 2.93 1 02/08/2023 20:32 WG2002164
Selenium 3.45 2.93 1 02/08/2023 20:32 WG2002164
Silver ND 1.46 1 02/08/2023 20:32 WG2002164
Thallium ND 2.93 1 02/08/2023 20:32 WG2002164
Zinc 69.6 7.31 1 02/08/2023 20:32 WG2002164
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.114 1.24 02/09/2023 04:37 WG2002811
Acrylonitrile ND 0.0284 1.24 02/09/2023 04:37 WG2002811
Benzene ND 0.00228 1.24 02/09/2023 04:37 WG2002811
Bromobenzene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
Bromodichloromethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Bromoform ND 0.0569 1.24 02/09/2023 04:37 WG2002811
Bromomethane ND 0.0284 1.24 02/09/2023 04:37 WG2002811
n-Butylbenzene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
sec-Butylbenzene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
tert-Butylbenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
Carbon tetrachloride ND 0.0114 1.24 02/09/2023 04:37 WG2002811
Chlorobenzene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Chlorodibromomethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Chloroethane ND 0.0114 1.24 02/09/2023 04:37 WG2002811
Chloroform ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Chloromethane ND 0.0284 1.24 02/09/2023 04:37 WG2002811
2-Chlorotoluene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
4-Chlorotoluene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1,2-Dibromo-3-Chloropropane ND 0.0569 1.24 02/09/2023 04:37 WG2002811
1,2-Dibromoethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Dibromomethane ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1,2-Dichlorobenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1,3-Dichlorobenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 07
L1582929
CB-2
Collected date/time: 02/02/23 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,4-Dichlorobenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
Dichlorodifluoromethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,1-Dichloroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,2-Dichloroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,1-Dichloroethene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
cis-1,2-Dichloroethene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
trans-1,2-Dichloroethene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1,2-Dichloropropane ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1,1-Dichloropropene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,3-Dichloropropane ND 0.0114 1.24 02/09/2023 04:37 WG2002811
cis-1,3-Dichloropropene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
trans-1,3-Dichloropropene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
2,2-Dichloropropane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Di-isopropyl ether ND 0.00228 1.24 02/09/2023 04:37 WG2002811
Ethylbenzene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Hexachloro-1,3-butadiene ND 0.0569 1.24 02/09/2023 04:37 WG2002811
Isopropylbenzene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
p-Isopropyltoluene 0.0347 0.0114 1.24 02/09/2023 04:37 WG2002811
2-Butanone (MEK)0.310 0.228 1.24 02/09/2023 04:37 WG2002811
Methylene Chloride ND 0.0569 1.24 02/09/2023 04:37 WG2002811
4-Methyl-2-pentanone (MIBK) 0.615 0.0569 1.24 02/09/2023 04:37 WG2002811
Methyl tert-butyl ether ND 0.00228 1.24 02/09/2023 04:37 WG2002811
Naphthalene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
n-Propylbenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
Styrene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
1,1,1,2-Tetrachloroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,1,2,2-Tetrachloroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,1,2-Trichlorotrifluoroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Tetrachloroethene ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Toluene 0.0637 0.0114 1.24 02/09/2023 04:37 WG2002811
1,2,3-Trichlorobenzene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
1,2,4-Trichlorobenzene ND 0.0284 1.24 02/09/2023 04:37 WG2002811
1,1,1-Trichloroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,1,2-Trichloroethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Trichloroethene ND 0.00228 1.24 02/09/2023 04:37 WG2002811
Trichlorofluoromethane ND 0.00569 1.24 02/09/2023 04:37 WG2002811
1,2,3-Trichloropropane ND 0.0284 1.24 02/09/2023 04:37 WG2002811
1,2,4-Trimethylbenzene 0.0134 B 0.0114 1.24 02/09/2023 04:37 WG2002811
1,2,3-Trimethylbenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
1,3,5-Trimethylbenzene ND 0.0114 1.24 02/09/2023 04:37 WG2002811
Vinyl chloride ND 0.00569 1.24 02/09/2023 04:37 WG2002811
Xylenes, Total 0.0153 0.0148 1.24 02/09/2023 04:37 WG2002811
(S) Toluene-d8 98.5 75.0-131 02/09/2023 04:37 WG2002811
(S) 4-Bromofluorobenzene 80.8 67.0-138 02/09/2023 04:37 WG2002811
(S) 1,2-Dichloroethane-d4 74.4 70.0-130 02/09/2023 04:37 WG2002811
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 212 29.3 5 02/09/2023 01:58 WG2002546
C28-C40 Oil Range 543 29.3 5 02/09/2023 01:58 WG2002546
(S) o-Terphenyl 33.3 18.0-148 02/09/2023 01:58 WG2002546
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 07
L1582929
CB-2
Collected date/time: 02/02/23 08:50
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0497 1 02/11/2023 00:48 WG2002078
PCB 1221 ND 0.0497 1 02/11/2023 00:48 WG2002078
PCB 1232 ND 0.0497 1 02/11/2023 00:48 WG2002078
PCB 1242 ND 0.0497 1 02/11/2023 00:48 WG2002078
PCB 1248 ND 0.0249 1 02/11/2023 00:48 WG2002078
PCB 1254 ND 0.0249 1 02/11/2023 00:48 WG2002078
PCB 1260 ND 0.0249 1 02/11/2023 00:48 WG2002078
(S) Decachlorobiphenyl 79.9 10.0-135 02/11/2023 00:48 WG2002078
(S) Tetrachloro-m-xylene 104 10.0-139 02/11/2023 00:48 WG2002078
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00878 1 02/08/2023 20:32 WG2002085
Acenaphthene ND 0.00878 1 02/08/2023 20:32 WG2002085
Acenaphthylene ND 0.00878 1 02/08/2023 20:32 WG2002085
Benzo(a)anthracene 0.0120 0.00878 1 02/08/2023 20:32 WG2002085
Benzo(a)pyrene 0.0103 0.00878 1 02/08/2023 20:32 WG2002085
Benzo(b)fluoranthene 0.0130 0.00878 1 02/08/2023 20:32 WG2002085
Benzo(g,h,i)perylene ND 0.00878 1 02/08/2023 20:32 WG2002085
Benzo(k)fluoranthene ND 0.00878 1 02/08/2023 20:32 WG2002085
Chrysene 0.0126 0.00878 1 02/08/2023 20:32 WG2002085
Dibenz(a,h)anthracene ND 0.00878 1 02/08/2023 20:32 WG2002085
Fluoranthene 0.0281 0.00878 1 02/08/2023 20:32 WG2002085
Fluorene ND 0.00878 1 02/08/2023 20:32 WG2002085
Indeno(1,2,3-cd)pyrene ND 0.00878 1 02/08/2023 20:32 WG2002085
Naphthalene ND 0.0293 1 02/08/2023 20:32 WG2002085
Phenanthrene 0.0269 0.00878 1 02/08/2023 20:32 WG2002085
Pyrene 0.0306 0.00878 1 02/08/2023 20:32 WG2002085
1-Methylnaphthalene ND 0.0293 1 02/08/2023 20:32 WG2002085
2-Methylnaphthalene ND 0.0293 1 02/08/2023 20:32 WG2002085
2-Chloronaphthalene ND 0.0293 1 02/08/2023 20:32 WG2002085
(S) p-Terphenyl-d14 40.6 23.0-120 02/08/2023 20:32 WG2002085
(S) Nitrobenzene-d5 44.1 14.0-149 02/08/2023 20:32 WG2002085
(S) 2-Fluorobiphenyl 40.8 34.0-125 02/08/2023 20:32 WG2002085
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002024
Total Solids by Method 2540 G-2011 L1582929-01,02,03,06,07
Method Blank (MB)
(MB) R3889031-1 02/08/23 17:47
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1582922-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1582922-04 02/08/23 17:47 • (DUP) R3889031-3 02/08/23 17:47
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 82.2 82.5 1 0.367 10
Laboratory Control Sample (LCS)
(LCS) R3889031-2 02/08/23 17:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002122
Wet Chemistry by Method 7199 L1582929-01,02,03,06,07
Method Blank (MB)
(MB) R3890711-1 02/09/23 10:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1582808-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1582808-01 02/09/23 10:34 • (DUP) R3890711-3 02/09/23 10:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 11.7 20
L1582929-07 Original Sample (OS) • Duplicate (DUP)
(OS) L1582929-07 02/09/23 12:07 • (DUP) R3890711-10 02/09/23 12:23
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3890711-2 02/09/23 10:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 10.1 101 80.0-120
L1582929-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582929-05 02/09/23 11:36 • (MS) R3890711-6 02/09/23 11:41 • (MSD) R3890711-7 02/09/23 11:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 ND 12.5 11.5 62.6 57.5 1 75.0-125 J6 J6 8.47 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002055
Mercury by Method 7471A L1582929-01,02,03,06,07
Method Blank (MB)
(MB) R3888672-1 02/08/23 11:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3888672-2 02/08/23 11:27
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.470 94.0 80.0-120
L1582850-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582850-01 02/08/23 11:29 • (MS) R3888672-3 02/08/23 11:32 • (MSD) R3888672-4 02/08/23 11:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 2.21 ND 2.13 1.91 92.6 82.6 1 75.0-125 11.0 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002164
Metals (ICP) by Method 6010B L1582929-01,02,03,06,07
Method Blank (MB)
(MB) R3888911-1 02/08/23 19:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead 0.231 J 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3888911-2 02/08/23 19:24
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 106 106 80.0-120
Arsenic 100 101 101 80.0-120
Beryllium 100 106 106 80.0-120
Cadmium 100 104 104 80.0-120
Chromium 100 104 104 80.0-120
Copper 100 106 106 80.0-120
Lead 100 101 101 80.0-120
Nickel 100 102 102 80.0-120
Selenium 100 105 105 80.0-120
Silver 20.0 20.4 102 80.0-120
Thallium 100 103 103 80.0-120
Zinc 100 101 101 80.0-120
L1582902-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582902-13 02/08/23 19:27 • (MS) R3888911-5 02/08/23 19:35 • (MSD) R3888911-6 02/08/23 19:37
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 113 ND 89.9 91.8 79.3 81.0 1 75.0-125 2.09 20
Arsenic 113 ND 112 114 98.7 101 1 75.0-125 1.89 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002164
Metals (ICP) by Method 6010B L1582929-01,02,03,06,07
L1582902-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582902-13 02/08/23 19:27 • (MS) R3888911-5 02/08/23 19:35 • (MSD) R3888911-6 02/08/23 19:37
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 113 ND 123 124 109 109 1 75.0-125 0.576 20
Cadmium 113 ND 117 119 104 105 1 75.0-125 1.22 20
Chromium 113 6.93 127 130 106 109 1 75.0-125 1.92 20
Copper 113 ND 127 128 111 112 1 75.0-125 0.966 20
Lead 113 3.52 122 123 105 105 1 75.0-125 0.599 20
Nickel 113 ND 120 120 105 105 1 75.0-125 0.304 20
Selenium 113 ND 115 116 102 102 1 75.0-125 0.924 20
Silver 22.7 ND 23.7 24.1 105 106 1 75.0-125 1.67 20
Thallium 113 ND 117 120 104 106 1 75.0-125 2.07 20
Zinc 113 ND 116 116 102 103 1 75.0-125 0.217 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002807
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-01
Method Blank (MB)
(MB) R3888935-2 02/08/23 20:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002807
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-01
Method Blank (MB)
(MB) R3888935-2 02/08/23 20:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 116 75.0-131
(S) 4-Bromofluorobenzene 89.1 67.0-138
(S) 1,2-Dichloroethane-d4 88.4 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3888935-1 02/08/23 19:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.718 115 10.0-160
Acrylonitrile 0.625 0.867 139 45.0-153
Benzene 0.125 0.141 113 70.0-123
Bromobenzene 0.125 0.142 114 73.0-121
Bromodichloromethane 0.125 0.149 119 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002807
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-01
Laboratory Control Sample (LCS)
(LCS) R3888935-1 02/08/23 19:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.154 123 64.0-132
Bromomethane 0.125 0.126 101 56.0-147
n-Butylbenzene 0.125 0.112 89.6 68.0-135
sec-Butylbenzene 0.125 0.123 98.4 74.0-130
tert-Butylbenzene 0.125 0.121 96.8 75.0-127
Carbon tetrachloride 0.125 0.144 115 66.0-128
Chlorobenzene 0.125 0.142 114 76.0-128
Chlorodibromomethane 0.125 0.156 125 74.0-127
Chloroethane 0.125 0.128 102 61.0-134
Chloroform 0.125 0.138 110 72.0-123
Chloromethane 0.125 0.135 108 51.0-138
2-Chlorotoluene 0.125 0.146 117 75.0-124
4-Chlorotoluene 0.125 0.124 99.2 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.134 107 59.0-130
1,2-Dibromoethane 0.125 0.136 109 74.0-128
Dibromomethane 0.125 0.136 109 75.0-122
1,2-Dichlorobenzene 0.125 0.142 114 76.0-124
1,3-Dichlorobenzene 0.125 0.140 112 76.0-125
1,4-Dichlorobenzene 0.125 0.141 113 77.0-121
Dichlorodifluoromethane 0.125 0.0982 78.6 43.0-156
1,1-Dichloroethane 0.125 0.140 112 70.0-127
1,2-Dichloroethane 0.125 0.125 100 65.0-131
1,1-Dichloroethene 0.125 0.137 110 65.0-131
cis-1,2-Dichloroethene 0.125 0.131 105 73.0-125
trans-1,2-Dichloroethene 0.125 0.139 111 71.0-125
1,2-Dichloropropane 0.125 0.142 114 74.0-125
1,1-Dichloropropene 0.125 0.126 101 73.0-125
1,3-Dichloropropane 0.125 0.143 114 80.0-125
cis-1,3-Dichloropropene 0.125 0.141 113 76.0-127
trans-1,3-Dichloropropene 0.125 0.132 106 73.0-127
2,2-Dichloropropane 0.125 0.137 110 59.0-135
Di-isopropyl ether 0.125 0.134 107 60.0-136
Ethylbenzene 0.125 0.143 114 74.0-126
Hexachloro-1,3-butadiene 0.125 0.122 97.6 57.0-150
Isopropylbenzene 0.125 0.123 98.4 72.0-127
p-Isopropyltoluene 0.125 0.123 98.4 72.0-133
2-Butanone (MEK)0.625 0.709 113 30.0-160
Methylene Chloride 0.125 0.137 110 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.716 115 56.0-143
Methyl tert-butyl ether 0.125 0.149 119 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002807
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-01
Laboratory Control Sample (LCS)
(LCS) R3888935-1 02/08/23 19:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.0874 69.9 59.0-130
n-Propylbenzene 0.125 0.131 105 74.0-126
Styrene 0.125 0.114 91.2 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.153 122 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.143 114 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.116 92.8 61.0-139
Tetrachloroethene 0.125 0.138 110 70.0-136
Toluene 0.125 0.136 109 75.0-121
1,2,3-Trichlorobenzene 0.125 0.100 80.0 59.0-139
1,2,4-Trichlorobenzene 0.125 0.122 97.6 62.0-137
1,1,1-Trichloroethane 0.125 0.144 115 69.0-126
1,1,2-Trichloroethane 0.125 0.151 121 78.0-123
Trichloroethene 0.125 0.141 113 76.0-126
Trichlorofluoromethane 0.125 0.0992 79.4 61.0-142
1,2,3-Trichloropropane 0.125 0.152 122 67.0-129
1,2,4-Trimethylbenzene 0.125 0.128 102 70.0-126
1,2,3-Trimethylbenzene 0.125 0.127 102 74.0-124
1,3,5-Trimethylbenzene 0.125 0.121 96.8 73.0-127
Vinyl chloride 0.125 0.141 113 63.0-134
Xylenes, Total 0.375 0.415 111 72.0-127
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 89.6 67.0-138
(S) 1,2-Dichloroethane-d4 103 70.0-130
L1582843-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582843-14 02/09/23 02:24 • (MS) R3888935-3 02/09/23 05:21 • (MSD) R3888935-4 02/09/23 05:41
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Acetone 0.813 ND 0.372 0.411 45.8 50.6 1 10.0-160 9.98 40
Acrylonitrile 0.813 ND 0.602 0.641 74.0 78.8 1 10.0-160 6.29 40
Benzene 0.163 1.33 1.55 1.59 136 164 1 10.0-149 V 2.99 37
Bromobenzene 0.163 ND 0.184 0.188 113 115 1 10.0-156 1.68 38
Bromodichloromethane 0.163 ND 0.151 0.164 93.0 101 1 10.0-143 8.23 37
Bromoform 0.163 ND 0.158 0.172 97.1 106 1 10.0-146 8.53 36
Bromomethane 0.163 ND 0.106 0.102 65.3 62.9 1 10.0-149 3.75 38
n-Butylbenzene 0.163 ND 0.153 0.154 93.9 94.8 1 10.0-160 0.917 40
sec-Butylbenzene 0.163 ND 0.166 0.166 102 102 1 10.0-159 0.000 39
tert-Butylbenzene 0.163 ND 0.166 0.166 102 102 1 10.0-156 0.000 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002807
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-01
L1582843-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582843-14 02/09/23 02:24 • (MS) R3888935-3 02/09/23 05:21 • (MSD) R3888935-4 02/09/23 05:41
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Carbon tetrachloride 0.163 ND 0.180 0.180 111 111 1 10.0-145 0.000 37
Chlorobenzene 0.163 ND 0.178 0.183 110 113 1 10.0-152 2.60 39
Chlorodibromomethane 0.163 ND 0.169 0.172 104 106 1 10.0-146 1.83 37
Chloroethane 0.163 ND 0.0655 0.0674 40.3 41.4 1 10.0-146 2.82 40
Chloroform 0.163 ND 0.148 0.164 91.2 101 1 10.0-146 10.2 37
Chloromethane 0.163 ND 0.149 0.149 91.4 91.9 1 10.0-159 0.524 37
2-Chlorotoluene 0.163 ND 0.174 0.188 107 115 1 10.0-159 7.79 38
4-Chlorotoluene 0.163 ND 0.174 0.195 107 120 1 10.0-155 11.9 39
1,2-Dibromo-3-Chloropropane 0.163 ND 0.132 0.133 81.3 82.0 1 10.0-151 0.942 39
1,2-Dibromoethane 0.163 ND 0.159 0.170 98.1 105 1 10.0-148 6.64 34
Dibromomethane 0.163 ND 0.132 0.148 81.4 91.2 1 10.0-147 11.3 35
1,2-Dichlorobenzene 0.163 ND 0.163 0.166 100 102 1 10.0-155 1.90 37
1,3-Dichlorobenzene 0.163 ND 0.170 0.177 105 109 1 10.0-153 3.60 38
1,4-Dichlorobenzene 0.163 ND 0.172 0.180 106 111 1 10.0-151 4.44 38
Dichlorodifluoromethane 0.163 ND 0.156 0.152 96.0 93.4 1 10.0-160 2.74 35
1,1-Dichloroethane 0.163 ND 0.154 0.166 94.6 102 1 10.0-147 7.44 37
1,2-Dichloroethane 0.163 ND 0.122 0.125 74.8 76.9 1 10.0-148 2.79 35
1,1-Dichloroethene 0.163 ND 0.177 0.172 109 106 1 10.0-155 2.69 37
cis-1,2-Dichloroethene 0.163 ND 0.155 0.159 95.6 98.1 1 10.0-149 2.58 37
trans-1,2-Dichloroethene 0.163 ND 0.163 0.169 100 104 1 10.0-150 3.77 37
1,2-Dichloropropane 0.163 ND 0.166 0.161 102 99.0 1 10.0-148 2.87 37
1,1-Dichloropropene 0.163 ND 0.167 0.174 103 107 1 10.0-153 3.67 35
1,3-Dichloropropane 0.163 ND 0.166 0.174 102 107 1 10.0-154 4.61 35
cis-1,3-Dichloropropene 0.163 ND 0.163 0.166 100 102 1 10.0-151 1.90 37
trans-1,3-Dichloropropene 0.163 ND 0.154 0.164 94.6 101 1 10.0-148 6.49 37
2,2-Dichloropropane 0.163 ND 0.126 0.116 77.4 71.2 1 10.0-138 8.41 36
Di-isopropyl ether 0.163 ND 0.148 0.155 91.3 95.4 1 10.0-147 4.43 36
Ethylbenzene 0.163 0.389 0.599 0.605 129 133 1 10.0-160 1.04 38
Hexachloro-1,3-butadiene 0.163 ND 0.150 0.136 92.5 83.6 1 10.0-160 10.2 40
Isopropylbenzene 0.163 0.0159 0.172 0.180 96.0 101 1 10.0-155 4.44 38
p-Isopropyltoluene 0.163 ND 0.161 0.167 99.0 103 1 10.0-160 3.81 40
2-Butanone (MEK)0.813 ND 0.546 0.458 67.1 56.3 1 10.0-160 17.4 40
Methylene Chloride 0.163 ND 0.151 0.146 92.7 89.8 1 10.0-141 3.16 37
4-Methyl-2-pentanone (MIBK) 0.813 ND 0.641 0.683 78.8 84.0 1 10.0-160 6.38 35
Methyl tert-butyl ether 0.163 ND 0.135 0.148 82.9 91.0 1 11.0-147 9.29 35
Naphthalene 0.163 0.0610 0.169 0.161 66.3 61.5 1 10.0-160 4.74 36
n-Propylbenzene 0.163 0.0370 0.217 0.225 111 116 1 10.0-158 3.53 38
Styrene 0.163 ND 0.154 0.152 95.0 93.4 1 10.0-160 1.74 40
1,1,1,2-Tetrachloroethane 0.163 ND 0.170 0.180 105 111 1 10.0-149 5.36 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002807
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-01
L1582843-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582843-14 02/09/23 02:24 • (MS) R3888935-3 02/09/23 05:21 • (MSD) R3888935-4 02/09/23 05:41
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.163 ND 0.156 0.166 96.2 102 1 10.0-160 5.83 35
1,1,2-Trichlorotrifluoroethane 0.163 ND 0.170 0.163 105 100 1 10.0-160 4.69 36
Tetrachloroethene 0.163 ND 0.181 0.181 112 112 1 10.0-156 0.000 39
Toluene 0.163 0.263 0.453 0.461 117 122 1 10.0-156 1.71 38
1,2,3-Trichlorobenzene 0.163 ND 0.111 0.112 68.6 69.0 1 10.0-160 0.699 40
1,2,4-Trichlorobenzene 0.163 ND 0.126 0.126 77.6 77.6 1 10.0-160 0.000 40
1,1,1-Trichloroethane 0.163 ND 0.177 0.172 109 106 1 10.0-144 2.69 35
1,1,2-Trichloroethane 0.163 ND 0.164 0.177 101 109 1 10.0-160 7.34 35
Trichloroethene 0.163 ND 0.161 0.177 99.0 109 1 10.0-156 9.26 38
Trichlorofluoromethane 0.163 ND 0.0721 0.0599 44.3 36.8 1 10.0-160 18.5 40
1,2,3-Trichloropropane 0.163 ND 0.167 0.166 103 102 1 10.0-156 0.939 35
1,2,4-Trimethylbenzene 0.163 0.336 0.503 0.502 103 102 1 10.0-160 0.311 36
1,2,3-Trimethylbenzene 0.163 0.128 0.289 0.285 98.9 96.1 1 10.0-160 1.63 36
1,3,5-Trimethylbenzene 0.163 0.0933 0.244 0.241 92.6 90.7 1 10.0-160 1.29 38
Vinyl chloride 0.163 ND 0.169 0.166 104 102 1 10.0-160 1.87 37
Xylenes, Total 0.488 1.83 2.53 2.58 144 154 1 10.0-160 1.83 38
(S) Toluene-d8 111 112 75.0-131
(S) 4-Bromofluorobenzene 90.8 91.6 67.0-138
(S) 1,2-Dichloroethane-d4 81.3 89.6 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002811
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-02,03,06,07
Method Blank (MB)
(MB) R3888963-2 02/08/23 19:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002811
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-02,03,06,07
Method Blank (MB)
(MB) R3888963-2 02/08/23 19:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene 0.00303 J 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 102 75.0-131
(S) 4-Bromofluorobenzene 85.7 67.0-138
(S) 1,2-Dichloroethane-d4 79.3 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3888963-1 02/08/23 19:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.752 120 10.0-160
Acrylonitrile 0.625 0.750 120 45.0-153
Benzene 0.125 0.109 87.2 70.0-123
Bromobenzene 0.125 0.119 95.2 73.0-121
Bromodichloromethane 0.125 0.103 82.4 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002811
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-02,03,06,07
Laboratory Control Sample (LCS)
(LCS) R3888963-1 02/08/23 19:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.128 102 64.0-132
Bromomethane 0.125 0.105 84.0 56.0-147
n-Butylbenzene 0.125 0.102 81.6 68.0-135
sec-Butylbenzene 0.125 0.102 81.6 74.0-130
tert-Butylbenzene 0.125 0.104 83.2 75.0-127
Carbon tetrachloride 0.125 0.110 88.0 66.0-128
Chlorobenzene 0.125 0.114 91.2 76.0-128
Chlorodibromomethane 0.125 0.112 89.6 74.0-127
Chloroethane 0.125 0.104 83.2 61.0-134
Chloroform 0.125 0.104 83.2 72.0-123
Chloromethane 0.125 0.0933 74.6 51.0-138
2-Chlorotoluene 0.125 0.109 87.2 75.0-124
4-Chlorotoluene 0.125 0.104 83.2 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.105 84.0 59.0-130
1,2-Dibromoethane 0.125 0.122 97.6 74.0-128
Dibromomethane 0.125 0.101 80.8 75.0-122
1,2-Dichlorobenzene 0.125 0.108 86.4 76.0-124
1,3-Dichlorobenzene 0.125 0.116 92.8 76.0-125
1,4-Dichlorobenzene 0.125 0.105 84.0 77.0-121
Dichlorodifluoromethane 0.125 0.105 84.0 43.0-156
1,1-Dichloroethane 0.125 0.100 80.0 70.0-127
1,2-Dichloroethane 0.125 0.0955 76.4 65.0-131
1,1-Dichloroethene 0.125 0.0970 77.6 65.0-131
cis-1,2-Dichloroethene 0.125 0.111 88.8 73.0-125
trans-1,2-Dichloroethene 0.125 0.102 81.6 71.0-125
1,2-Dichloropropane 0.125 0.0984 78.7 74.0-125
1,1-Dichloropropene 0.125 0.0997 79.8 73.0-125
1,3-Dichloropropane 0.125 0.116 92.8 80.0-125
cis-1,3-Dichloropropene 0.125 0.105 84.0 76.0-127
trans-1,3-Dichloropropene 0.125 0.0940 75.2 73.0-127
2,2-Dichloropropane 0.125 0.109 87.2 59.0-135
Di-isopropyl ether 0.125 0.0858 68.6 60.0-136
Ethylbenzene 0.125 0.117 93.6 74.0-126
Hexachloro-1,3-butadiene 0.125 0.0987 79.0 57.0-150
Isopropylbenzene 0.125 0.106 84.8 72.0-127
p-Isopropyltoluene 0.125 0.105 84.0 72.0-133
2-Butanone (MEK)0.625 0.513 82.1 30.0-160
Methylene Chloride 0.125 0.108 86.4 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.544 87.0 56.0-143
Methyl tert-butyl ether 0.125 0.122 97.6 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002811
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-02,03,06,07
Laboratory Control Sample (LCS)
(LCS) R3888963-1 02/08/23 19:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.112 89.6 59.0-130
n-Propylbenzene 0.125 0.105 84.0 74.0-126
Styrene 0.125 0.106 84.8 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.107 85.6 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.0976 78.1 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.105 84.0 61.0-139
Tetrachloroethene 0.125 0.122 97.6 70.0-136
Toluene 0.125 0.114 91.2 75.0-121
1,2,3-Trichlorobenzene 0.125 0.0965 77.2 59.0-139
1,2,4-Trichlorobenzene 0.125 0.101 80.8 62.0-137
1,1,1-Trichloroethane 0.125 0.105 84.0 69.0-126
1,1,2-Trichloroethane 0.125 0.113 90.4 78.0-123
Trichloroethene 0.125 0.125 100 76.0-126
Trichlorofluoromethane 0.125 0.110 88.0 61.0-142
1,2,3-Trichloropropane 0.125 0.113 90.4 67.0-129
1,2,4-Trimethylbenzene 0.125 0.119 95.2 70.0-126
1,2,3-Trimethylbenzene 0.125 0.103 82.4 74.0-124
1,3,5-Trimethylbenzene 0.125 0.0975 78.0 73.0-127
Vinyl chloride 0.125 0.0977 78.2 63.0-134
Xylenes, Total 0.375 0.336 89.6 72.0-127
(S) Toluene-d8 90.5 75.0-131
(S) 4-Bromofluorobenzene 85.1 67.0-138
(S) 1,2-Dichloroethane-d4 85.9 70.0-130
L1582929-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582929-07 02/09/23 04:37 • (MS) R3888963-3 02/09/23 05:16 • (MSD) R3888963-4 02/09/23 05:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 1.42 ND 1.02 1.09 71.9 76.5 1.24 10.0-160 6.26 40
Acrylonitrile 1.42 ND 1.44 1.21 101 85.3 1.24 10.0-160 16.9 40
Benzene 0.284 ND 0.266 0.266 93.1 93.1 1.24 10.0-149 0.000 37
Bromobenzene 0.284 ND 0.290 0.295 102 104 1.24 10.0-156 1.88 38
Bromodichloromethane 0.284 ND 0.224 0.237 78.7 83.2 1.24 10.0-143 5.58 37
Bromoform 0.284 ND 0.248 0.240 87.1 84.5 1.24 10.0-146 3.01 36
Bromomethane 0.284 ND 0.198 0.191 69.7 67.1 1.24 10.0-149 3.77 38
n-Butylbenzene 0.284 ND 0.284 0.261 100 91.6 1.24 10.0-160 8.75 40
sec-Butylbenzene 0.284 ND 0.277 0.250 97.4 87.7 1.24 10.0-159 10.5 39
tert-Butylbenzene 0.284 ND 0.284 0.272 100 95.5 1.24 10.0-156 4.62 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002811
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-02,03,06,07
L1582929-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582929-07 02/09/23 04:37 • (MS) R3888963-3 02/09/23 05:16 • (MSD) R3888963-4 02/09/23 05:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.284 ND 0.242 0.233 85.2 81.9 1.24 10.0-145 3.86 37
Chlorobenzene 0.284 ND 0.273 0.275 96.1 96.8 1.24 10.0-152 0.669 39
Chlorodibromomethane 0.284 ND 0.239 0.244 83.9 85.8 1.24 10.0-146 2.28 37
Chloroethane 0.284 ND 0.142 0.138 50.1 48.6 1.24 10.0-146 2.88 40
Chloroform 0.284 ND 0.228 0.229 79.1 79.7 1.24 10.0-146 0.803 37
Chloromethane 0.284 ND 0.226 0.213 79.4 74.8 1.24 10.0-159 5.86 37
2-Chlorotoluene 0.284 ND 0.261 0.275 91.6 96.8 1.24 10.0-159 5.48 38
4-Chlorotoluene 0.284 ND 0.288 0.283 101 99.4 1.24 10.0-155 1.93 39
1,2-Dibromo-3-Chloropropane 0.284 ND 0.196 0.182 69.0 64.1 1.24 10.0-151 7.36 39
1,2-Dibromoethane 0.284 ND 0.261 0.270 91.6 94.8 1.24 10.0-148 3.46 34
Dibromomethane 0.284 ND 0.217 0.220 76.1 77.4 1.24 10.0-147 1.68 35
1,2-Dichlorobenzene 0.284 ND 0.244 0.251 85.8 88.4 1.24 10.0-155 2.96 37
1,3-Dichlorobenzene 0.284 ND 0.272 0.283 95.5 99.4 1.24 10.0-153 3.97 38
1,4-Dichlorobenzene 0.284 ND 0.251 0.251 88.4 88.4 1.24 10.0-151 0.000 38
Dichlorodifluoromethane 0.284 ND 0.306 0.268 108 94.2 1.24 10.0-160 13.4 35
1,1-Dichloroethane 0.284 ND 0.226 0.228 79.4 80.0 1.24 10.0-147 0.810 37
1,2-Dichloroethane 0.284 ND 0.218 0.229 76.8 80.6 1.24 10.0-148 4.92 35
1,1-Dichloroethene 0.284 ND 0.273 0.257 96.1 90.3 1.24 10.0-155 6.23 37
cis-1,2-Dichloroethene 0.284 ND 0.237 0.250 83.2 87.7 1.24 10.0-149 5.28 37
trans-1,2-Dichloroethene 0.284 ND 0.228 0.248 80.0 87.1 1.24 10.0-150 8.49 37
1,2-Dichloropropane 0.284 ND 0.235 0.229 82.6 80.6 1.24 10.0-148 2.37 37
1,1-Dichloropropene 0.284 ND 0.270 0.262 94.8 92.3 1.24 10.0-153 2.76 35
1,3-Dichloropropane 0.284 ND 0.268 0.277 94.2 97.4 1.24 10.0-154 3.37 35
cis-1,3-Dichloropropene 0.284 ND 0.262 0.257 92.3 90.3 1.24 10.0-151 2.12 37
trans-1,3-Dichloropropene 0.284 ND 0.235 0.237 82.6 83.2 1.24 10.0-148 0.778 37
2,2-Dichloropropane 0.284 ND 0.204 0.180 71.6 63.3 1.24 10.0-138 12.3 36
Di-isopropyl ether 0.284 ND 0.187 0.207 65.8 72.9 1.24 10.0-147 10.2 36
Ethylbenzene 0.284 ND 0.286 0.277 98.9 95.7 1.24 10.0-160 3.26 38
Hexachloro-1,3-butadiene 0.284 ND 0.290 0.222 102 78.1 1.24 10.0-160 26.5 40
Isopropylbenzene 0.284 ND 0.248 0.229 86.6 80.2 1.24 10.0-155 7.69 38
p-Isopropyltoluene 0.284 0.0347 0.310 0.295 96.8 91.7 1.24 10.0-160 4.85 40
2-Butanone (MEK)1.42 0.310 1.21 1.28 63.5 67.9 1.24 10.0-160 5.01 40
Methylene Chloride 0.284 ND 0.259 0.268 91.0 94.2 1.24 10.0-141 3.48 37
4-Methyl-2-pentanone (MIBK) 1.42 0.615 1.66 1.71 73.4 77.2 1.24 10.0-160 3.16 35
Methyl tert-butyl ether 0.284 ND 0.206 0.228 72.3 80.0 1.24 11.0-147 10.2 35
Naphthalene 0.284 ND 0.213 0.200 74.8 70.3 1.24 10.0-160 6.22 36
n-Propylbenzene 0.284 ND 0.294 0.286 103 101 1.24 10.0-158 2.53 38
Styrene 0.284 ND 0.272 0.268 95.5 94.2 1.24 10.0-160 1.36 40
1,1,1,2-Tetrachloroethane 0.284 ND 0.215 0.211 75.5 74.2 1.24 10.0-149 1.72 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002811
Volatile Organic Compounds (GC/MS) by Method 8260B L1582929-02,03,06,07
L1582929-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582929-07 02/09/23 04:37 • (MS) R3888963-3 02/09/23 05:16 • (MSD) R3888963-4 02/09/23 05:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.284 ND 0.202 0.213 71.0 74.8 1.24 10.0-160 5.31 35
1,1,2-Trichlorotrifluoroethane 0.284 ND 0.327 0.286 115 101 1.24 10.0-160 13.2 36
Tetrachloroethene 0.284 ND 0.312 0.303 108 105 1.24 10.0-156 2.99 39
Toluene 0.284 0.0637 0.347 0.350 99.5 101 1.24 10.0-156 1.05 38
1,2,3-Trichlorobenzene 0.284 ND 0.211 0.196 74.2 69.0 1.24 10.0-160 7.21 40
1,2,4-Trichlorobenzene 0.284 ND 0.233 0.217 81.9 76.1 1.24 10.0-160 7.35 40
1,1,1-Trichloroethane 0.284 ND 0.240 0.237 84.5 83.2 1.24 10.0-144 1.54 35
1,1,2-Trichloroethane 0.284 ND 0.255 0.259 89.7 91.0 1.24 10.0-160 1.43 35
Trichloroethene 0.284 ND 0.297 0.299 105 105 1.24 10.0-156 0.615 38
Trichlorofluoromethane 0.284 ND 0.294 0.264 103 92.9 1.24 10.0-160 10.5 40
1,2,3-Trichloropropane 0.284 ND 0.224 0.251 78.7 88.4 1.24 10.0-156 11.6 35
1,2,4-Trimethylbenzene 0.284 0.0134 0.268 0.262 89.5 87.6 1.24 10.0-160 2.08 36
1,2,3-Trimethylbenzene 0.284 ND 0.240 0.229 83.2 79.3 1.24 10.0-160 4.69 36
1,3,5-Trimethylbenzene 0.284 ND 0.237 0.239 83.2 83.9 1.24 10.0-160 0.772 38
Vinyl chloride 0.284 ND 0.239 0.215 83.9 75.5 1.24 10.0-160 10.5 37
Xylenes, Total 0.853 0.0153 0.773 0.776 88.7 89.2 1.24 10.0-160 0.474 38
(S) Toluene-d8 94.4 94.7 75.0-131
(S) 4-Bromofluorobenzene 82.4 80.6 67.0-138
(S) 1,2-Dichloroethane-d4 76.6 82.6 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002546
Semi-Volatile Organic Compounds (GC) by Method 8015 L1582929-01,02,03,06,07
Method Blank (MB)
(MB) R3888902-2 02/09/23 00:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 95.6 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3888902-1 02/09/23 00:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 37.5 75.0 50.0-150
(S) o-Terphenyl 74.2 18.0-148
L1582929-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582929-03 02/09/23 02:11 • (MS) R3888902-3 02/09/23 02:23 • (MSD) R3888902-4 02/09/23 02:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 55.1 ND 104 116 56.8 76.9 20 50.0-150 10.3 20
(S) o-Terphenyl 71.7 71.0 18.0-148 J7 J7
Sample Narrative:
OS: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001937
Polychlorinated Biphenyls (GC) by Method 8082 L1582929-01,02
Method Blank (MB)
(MB) R3888729-1 02/08/23 10:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 54.1 10.0-135
(S) Tetrachloro-m-xylene 58.6 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3888729-2 02/08/23 11:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.120 71.9 36.0-141
PCB 1260 0.167 0.104 62.3 37.0-145
(S) Decachlorobiphenyl 54.4 10.0-135
(S) Tetrachloro-m-xylene 63.1 10.0-139
L1581058-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1581058-09 02/08/23 11:09 • (MS) R3888729-3 02/08/23 11:18 • (MSD) R3888729-4 02/08/23 11:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.205 ND 0.665 0.659 324 321 1 10.0-160 J5 P J5 P 0.934 37
PCB 1260 0.205 ND 0.616 0.671 300 327 1 10.0-160 J5 P J5 P 8.65 38
(S) Decachlorobiphenyl 61.5 50.7 10.0-135
(S) Tetrachloro-m-xylene 52.8 45.2 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001943
Polychlorinated Biphenyls (GC) by Method 8082 L1582929-03,06
Method Blank (MB)
(MB) R3889118-1 02/08/23 22:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 85.1 10.0-135
(S) Tetrachloro-m-xylene 66.2 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3889118-2 02/08/23 23:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0922 55.2 36.0-141
PCB 1260 0.167 0.134 80.2 37.0-145
(S) Decachlorobiphenyl 73.4 10.0-135
(S) Tetrachloro-m-xylene 61.4 10.0-139
L1581666-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1581666-10 02/08/23 23:35 • (MS) R3889118-3 02/08/23 23:46 • (MSD) R3889118-4 02/08/23 23:56
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 1.60 ND 0.789 1.03 49.2 72.0 9.62 10.0-160 P P 26.7 37
PCB 1260 1.60 ND 1.36 1.29 85.0 90.2 9.62 10.0-160 P P 5.28 38
(S) Decachlorobiphenyl 58.4 75.4 10.0-135
(S) Tetrachloro-m-xylene 34.4 47.8 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002078
Polychlorinated Biphenyls (GC) by Method 8082 L1582929-07
Method Blank (MB)
(MB) R3891527-1 02/10/23 22:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 111 10.0-135
(S) Tetrachloro-m-xylene 130 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3891527-2 02/10/23 22:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.214 128 36.0-141
PCB 1260 0.167 0.198 119 37.0-145
(S) Decachlorobiphenyl 109 10.0-135
(S) Tetrachloro-m-xylene 130 10.0-139
L1582929-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582929-07 02/11/23 00:48 • (MS) R3891527-3 02/11/23 01:00 • (MSD) R3891527-4 02/11/23 01:13
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.236 ND 0.309 0.225 131 97.5 1 10.0-160 P P 31.2 37
PCB 1260 0.236 ND 0.199 0.208 84.5 89.9 1 10.0-160 P P 4.32 38
(S) Decachlorobiphenyl 89.7 91.8 10.0-135
(S) Tetrachloro-m-xylene 108 110 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002084
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1582929-01,02,03,06
Method Blank (MB)
(MB) R3889446-2 02/09/23 00:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 83.1 23.0-120
(S) Nitrobenzene-d5 58.8 14.0-149
(S) 2-Fluorobiphenyl 84.1 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3889446-1 02/09/23 00:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0769 96.1 50.0-126
Acenaphthene 0.0800 0.0726 90.8 50.0-120
Acenaphthylene 0.0800 0.0748 93.5 50.0-120
Benzo(a)anthracene 0.0800 0.0796 99.5 45.0-120
Benzo(a)pyrene 0.0800 0.0687 85.9 42.0-120
Benzo(b)fluoranthene 0.0800 0.0707 88.4 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0713 89.1 45.0-125
Benzo(k)fluoranthene 0.0800 0.0713 89.1 49.0-125
Chrysene 0.0800 0.0770 96.3 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0737 92.1 47.0-125
Fluoranthene 0.0800 0.0871 109 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002084
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1582929-01,02,03,06
Laboratory Control Sample (LCS)
(LCS) R3889446-1 02/09/23 00:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0786 98.3 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0791 98.9 46.0-125
Naphthalene 0.0800 0.0738 92.3 50.0-120
Phenanthrene 0.0800 0.0772 96.5 47.0-120
Pyrene 0.0800 0.0699 87.4 43.0-123
1-Methylnaphthalene 0.0800 0.0820 103 51.0-121
2-Methylnaphthalene 0.0800 0.0843 105 50.0-120
2-Chloronaphthalene 0.0800 0.0745 93.1 50.0-120
(S) p-Terphenyl-d14 92.1 23.0-120
(S) Nitrobenzene-d5 60.0 14.0-149
(S) 2-Fluorobiphenyl 86.9 34.0-125
L1582902-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582902-16 02/09/23 00:49 • (MS) R3889446-3 02/09/23 01:09 • (MSD) R3889446-4 02/09/23 01:29
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0899 ND 0.0644 0.0668 71.6 74.7 1 10.0-145 3.73 30
Acenaphthene 0.0899 ND 0.0621 0.0655 69.0 73.3 1 14.0-127 5.47 27
Acenaphthylene 0.0899 ND 0.0643 0.0679 71.5 75.9 1 21.0-124 5.46 25
Benzo(a)anthracene 0.0899 ND 0.0654 0.0673 72.8 75.3 1 10.0-139 2.81 30
Benzo(a)pyrene 0.0899 ND 0.0661 0.0692 73.6 77.3 1 10.0-141 4.48 31
Benzo(b)fluoranthene 0.0899 ND 0.0603 0.0639 67.1 71.5 1 10.0-140 5.81 36
Benzo(g,h,i)perylene 0.0899 ND 0.0601 0.0643 66.8 71.9 1 10.0-140 6.74 33
Benzo(k)fluoranthene 0.0899 ND 0.0611 0.0645 68.0 72.1 1 10.0-137 5.38 31
Chrysene 0.0899 ND 0.0658 0.0687 73.2 76.8 1 10.0-145 4.33 30
Dibenz(a,h)anthracene 0.0899 ND 0.0612 0.0657 68.1 73.4 1 10.0-132 6.97 31
Fluoranthene 0.0899 ND 0.0715 0.0738 79.5 82.6 1 10.0-153 3.21 33
Fluorene 0.0899 ND 0.0686 0.0699 76.3 78.1 1 11.0-130 1.85 29
Indeno(1,2,3-cd)pyrene 0.0899 ND 0.0658 0.0685 73.2 76.6 1 10.0-137 3.99 32
Naphthalene 0.0899 ND 0.0711 0.0702 79.1 78.5 1 10.0-135 1.32 27
Phenanthrene 0.0899 ND 0.0667 0.0680 74.2 76.0 1 10.0-144 1.90 31
Pyrene 0.0899 ND 0.0595 0.0621 66.2 69.4 1 10.0-148 4.21 35
1-Methylnaphthalene 0.0899 ND 0.0715 0.0746 79.5 83.5 1 10.0-142 4.30 28
2-Methylnaphthalene 0.0899 ND 0.0756 0.0766 84.1 85.7 1 10.0-137 1.38 28
2-Chloronaphthalene 0.0899 ND 0.0653 0.0693 72.7 77.5 1 29.0-120 5.88 24
(S) p-Terphenyl-d14 60.2 51.6 23.0-120
(S) Nitrobenzene-d5 45.8 45.3 14.0-149
(S) 2-Fluorobiphenyl 60.2 55.6 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002085
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1582929-07
Method Blank (MB)
(MB) R3888888-2 02/08/23 14:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 62.7 23.0-120
(S) Nitrobenzene-d5 47.2 14.0-149
(S) 2-Fluorobiphenyl 67.1 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3888888-1 02/08/23 14:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0519 64.9 50.0-126
Acenaphthene 0.0800 0.0515 64.4 50.0-120
Acenaphthylene 0.0800 0.0512 64.0 50.0-120
Benzo(a)anthracene 0.0800 0.0524 65.5 45.0-120
Benzo(a)pyrene 0.0800 0.0491 61.4 42.0-120
Benzo(b)fluoranthene 0.0800 0.0545 68.1 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0490 61.3 45.0-125
Benzo(k)fluoranthene 0.0800 0.0536 67.0 49.0-125
Chrysene 0.0800 0.0535 66.9 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0502 62.8 47.0-125
Fluoranthene 0.0800 0.0577 72.1 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2002085
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1582929-07
Laboratory Control Sample (LCS)
(LCS) R3888888-1 02/08/23 14:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0543 67.9 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0516 64.5 46.0-125
Naphthalene 0.0800 0.0530 66.3 50.0-120
Phenanthrene 0.0800 0.0536 67.0 47.0-120
Pyrene 0.0800 0.0510 63.8 43.0-123
1-Methylnaphthalene 0.0800 0.0572 71.5 51.0-121
2-Methylnaphthalene 0.0800 0.0582 72.8 50.0-120
2-Chloronaphthalene 0.0800 0.0534 66.8 50.0-120
(S) p-Terphenyl-d14 68.0 23.0-120
(S) Nitrobenzene-d5 54.8 14.0-149
(S) 2-Fluorobiphenyl 73.4 34.0-125
L1583030-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1583030-01 02/08/23 15:38 • (MS) R3888888-3 02/08/23 15:57 • (MSD) R3888888-4 02/08/23 16:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.106 ND 0.0479 0.0572 45.2 53.9 1 10.0-145 17.6 30
Acenaphthene 0.106 ND 0.0511 0.0590 48.2 55.7 1 14.0-127 14.3 27
Acenaphthylene 0.106 ND 0.0511 0.0581 48.2 54.8 1 21.0-124 12.7 25
Benzo(a)anthracene 0.106 ND 0.0471 0.0568 44.4 53.5 1 10.0-139 18.6 30
Benzo(a)pyrene 0.106 ND 0.0498 0.0594 47.0 56.1 1 10.0-141 17.6 31
Benzo(b)fluoranthene 0.106 ND 0.0466 0.0592 43.9 55.8 1 10.0-140 23.8 36
Benzo(g,h,i)perylene 0.106 ND 0.0423 0.0499 39.9 47.1 1 10.0-140 16.5 33
Benzo(k)fluoranthene 0.106 ND 0.0501 0.0588 47.2 55.4 1 10.0-137 16.0 31
Chrysene 0.106 ND 0.0534 0.0611 50.4 57.6 1 10.0-145 13.3 30
Dibenz(a,h)anthracene 0.106 ND 0.0457 0.0517 43.1 48.7 1 10.0-132 12.4 31
Fluoranthene 0.106 ND 0.0495 0.0629 46.7 59.3 1 10.0-153 23.8 33
Fluorene 0.106 ND 0.0514 0.0621 48.5 58.6 1 11.0-130 18.9 29
Indeno(1,2,3-cd)pyrene 0.106 ND 0.0418 0.0495 39.4 46.7 1 10.0-137 17.0 32
Naphthalene 0.106 ND 0.0597 0.0619 56.3 58.3 1 10.0-135 3.52 27
Phenanthrene 0.106 ND 0.0501 0.0624 47.2 58.8 1 10.0-144 21.9 31
Pyrene 0.106 ND 0.0459 0.0574 43.3 54.2 1 10.0-148 22.3 35
1-Methylnaphthalene 0.106 ND 0.0607 0.0653 57.2 61.6 1 10.0-142 7.44 28
2-Methylnaphthalene 0.106 ND 0.0616 0.0673 58.1 63.5 1 10.0-137 8.93 28
2-Chloronaphthalene 0.106 ND 0.0557 0.0625 52.5 59.0 1 29.0-120 11.6 24
(S) p-Terphenyl-d14 50.1 46.6 23.0-120
(S) Nitrobenzene-d5 49.0 48.3 14.0-149
(S) 2-Fluorobiphenyl 60.2 51.3 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
P RPD between the primary and confirmatory analysis exceeded 40%.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
February 17, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1584351
Samples Received:02/10/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
February 17, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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February 20, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
SS-12 L1584351-01 6
SS-10 L1584351-02 10
SS-7 L1584351-03 14
SS-6 L1584351-04 18
Qc: Quality Control Summary 22
Total Solids by Method 2540 G-2011 22
Wet Chemistry by Method 7199 23
Mercury by Method 7471A 25
Metals (ICP) by Method 6010B 26
Volatile Organic Compounds (GC) by Method 8015D/GRO 30
Volatile Organic Compounds (GC/MS) by Method 8260B 32
Semi-Volatile Organic Compounds (GC) by Method 8015 48
Polychlorinated Biphenyls (GC) by Method 8082 50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 51
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 61
Gl: Glossary of Terms 63
Al: Accreditations & Locations 64
Sc: Sample Chain of Custody 65
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SS-12 L1584351-01 Solid Richie Torney 02/09/23 10:20 02/10/23 08:50
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2004469 1 02/14/23 11:54 02/14/23 12:09 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2004535 1 02/13/23 15:18 02/16/23 01:02 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2004804 1 02/13/23 10:29 02/13/23 20:42 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2005201 1 02/14/23 07:48 02/14/23 18:16 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2007003 28.5 02/09/23 10:20 02/16/23 12:04 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2004844 1 02/09/23 10:20 02/13/23 00:17 JBE Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2005423 10 02/15/23 17:25 02/16/23 10:04 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2004450 10 02/15/23 14:43 02/16/23 20:27 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2004703 1 02/15/23 06:08 02/15/23 15:20 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2007018 1 02/16/23 16:37 02/17/23 04:55 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-10 L1584351-02 Solid Richie Torney 02/09/23 11:00 02/10/23 08:50
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2004469 1 02/14/23 11:54 02/14/23 12:09 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2004535 10 02/13/23 15:18 02/16/23 01:38 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2004804 1 02/13/23 10:29 02/13/23 20:57 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2005201 1 02/14/23 07:48 02/14/23 19:24 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2006017 28.7 02/09/23 11:00 02/15/23 13:48 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2004751 1.15 02/09/23 11:00 02/12/23 12:35 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2005423 1 02/15/23 17:25 02/16/23 00:06 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2004450 1 02/15/23 14:43 02/15/23 22:10 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2004454 5 02/11/23 06:13 02/16/23 09:07 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2007018 1 02/16/23 16:37 02/17/23 04:15 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-7 L1584351-03 Solid Richie Torney 02/09/23 11:35 02/10/23 08:50
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2004469 1 02/14/23 11:54 02/14/23 12:09 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2004535 1 02/13/23 15:18 02/16/23 01:43 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2004804 1 02/13/23 10:29 02/13/23 21:00 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2005201 1 02/14/23 07:48 02/14/23 19:27 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2007003 27.5 02/09/23 11:35 02/16/23 12:24 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2006549 2.2 02/09/23 11:35 02/17/23 00:03 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2005842 2 02/14/23 19:30 02/15/23 05:44 KAP Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2005842 2 02/14/23 19:30 02/15/23 09:58 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2004450 1 02/15/23 14:43 02/16/23 00:38 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2004454 1 02/11/23 06:13 02/12/23 02:11 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2007018 1 02/16/23 16:37 02/17/23 05:15 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-6 L1584351-04 Solid Richie Torney 02/09/23 11:58 02/10/23 08:50
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2004469 1 02/14/23 11:54 02/14/23 12:09 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2004535 1 02/13/23 15:18 02/16/23 01:48 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2004804 1 02/13/23 10:29 02/13/23 21:07 SRT Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2005200 1 02/14/23 08:34 02/15/23 01:22 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2007003 25 02/09/23 11:58 02/16/23 12:45 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2004751 1 02/09/23 11:58 02/12/23 12:55 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2005842 1 02/14/23 19:30 02/15/23 05:31 KAP Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SS-6 L1584351-04 Solid Richie Torney 02/09/23 11:58 02/10/23 08:50
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Polychlorinated Biphenyls (GC) by Method 8082 WG2004450 1 02/15/23 14:43 02/15/23 22:22 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2004454 1 02/11/23 06:13 02/12/23 00:46 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2007018 1 02/16/23 16:37 02/17/23 02:36 AGW Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1584351
SS-12
Collected date/time: 02/09/23 10:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.6 1 02/14/2023 12:09 WG2004469
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND J3 J6 O1 1.36 1 02/16/2023 01:02 WG2004535
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND J3 J5 0.0544 1 02/13/2023 20:42 WG2004804
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.72 1 02/14/2023 18:16 WG2005201
Arsenic 6.26 2.72 1 02/14/2023 18:16 WG2005201
Beryllium 0.384 0.272 1 02/14/2023 18:16 WG2005201
Cadmium ND 0.680 1 02/14/2023 18:16 WG2005201
Chromium 20.6 O1 1.36 1 02/14/2023 18:16 WG2005201
Copper 17.0 2.72 1 02/14/2023 18:16 WG2005201
Lead 30.1 O1 0.680 1 02/14/2023 18:16 WG2005201
Nickel 7.03 2.72 1 02/14/2023 18:16 WG2005201
Selenium ND 2.72 1 02/14/2023 18:16 WG2005201
Silver ND 1.36 1 02/14/2023 18:16 WG2005201
Thallium ND 2.72 1 02/14/2023 18:16 WG2005201
Zinc 103 O1 6.80 1 02/14/2023 18:16 WG2005201
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.77 28.5 02/16/2023 12:04 WG2007003
(S) a,a,a-Trifluorotoluene(FID) 95.9 77.0-120 02/16/2023 12:04 WG2007003
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND J3 0.0876 1 02/13/2023 00:17 WG2004844
Acrylonitrile ND 0.0219 1 02/13/2023 00:17 WG2004844
Benzene ND 0.00175 1 02/13/2023 00:17 WG2004844
Bromobenzene ND 0.0219 1 02/13/2023 00:17 WG2004844
Bromodichloromethane ND 0.00438 1 02/13/2023 00:17 WG2004844
Bromoform ND 0.0438 1 02/13/2023 00:17 WG2004844
Bromomethane ND 0.0219 1 02/13/2023 00:17 WG2004844
n-Butylbenzene ND 0.0219 1 02/13/2023 00:17 WG2004844
sec-Butylbenzene ND 0.0219 1 02/13/2023 00:17 WG2004844
tert-Butylbenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
Carbon tetrachloride ND 0.00876 1 02/13/2023 00:17 WG2004844
Chlorobenzene ND 0.00438 1 02/13/2023 00:17 WG2004844
Chlorodibromomethane ND 0.00438 1 02/13/2023 00:17 WG2004844
Chloroethane ND 0.00876 1 02/13/2023 00:17 WG2004844
Chloroform ND 0.00438 1 02/13/2023 00:17 WG2004844
Chloromethane ND 0.0219 1 02/13/2023 00:17 WG2004844
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1584351
SS-12
Collected date/time: 02/09/23 10:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00438 1 02/13/2023 00:17 WG2004844
4-Chlorotoluene ND 0.00876 1 02/13/2023 00:17 WG2004844
1,2-Dibromo-3-Chloropropane ND 0.0438 1 02/13/2023 00:17 WG2004844
1,2-Dibromoethane ND 0.00438 1 02/13/2023 00:17 WG2004844
Dibromomethane ND 0.00876 1 02/13/2023 00:17 WG2004844
1,2-Dichlorobenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
1,3-Dichlorobenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
1,4-Dichlorobenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
Dichlorodifluoromethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,1-Dichloroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,2-Dichloroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,1-Dichloroethene ND 0.00438 1 02/13/2023 00:17 WG2004844
cis-1,2-Dichloroethene ND 0.00438 1 02/13/2023 00:17 WG2004844
trans-1,2-Dichloroethene ND 0.00876 1 02/13/2023 00:17 WG2004844
1,2-Dichloropropane ND 0.00876 1 02/13/2023 00:17 WG2004844
1,1-Dichloropropene ND 0.00438 1 02/13/2023 00:17 WG2004844
1,3-Dichloropropane ND 0.00876 1 02/13/2023 00:17 WG2004844
cis-1,3-Dichloropropene ND 0.00438 1 02/13/2023 00:17 WG2004844
trans-1,3-Dichloropropene ND 0.00876 1 02/13/2023 00:17 WG2004844
2,2-Dichloropropane ND 0.00438 1 02/13/2023 00:17 WG2004844
Di-isopropyl ether ND 0.00175 1 02/13/2023 00:17 WG2004844
Ethylbenzene ND 0.00438 1 02/13/2023 00:17 WG2004844
Hexachloro-1,3-butadiene ND 0.0438 1 02/13/2023 00:17 WG2004844
Isopropylbenzene ND 0.00438 1 02/13/2023 00:17 WG2004844
p-Isopropyltoluene ND 0.00876 1 02/13/2023 00:17 WG2004844
2-Butanone (MEK)ND 0.175 1 02/13/2023 00:17 WG2004844
Methylene Chloride ND 0.0438 1 02/13/2023 00:17 WG2004844
4-Methyl-2-pentanone (MIBK) ND 0.0438 1 02/13/2023 00:17 WG2004844
Methyl tert-butyl ether ND 0.00175 1 02/13/2023 00:17 WG2004844
Naphthalene ND 0.0219 1 02/13/2023 00:17 WG2004844
n-Propylbenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
Styrene ND 0.0219 1 02/13/2023 00:17 WG2004844
1,1,1,2-Tetrachloroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,1,2,2-Tetrachloroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,1,2-Trichlorotrifluoroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
Tetrachloroethene ND 0.00438 1 02/13/2023 00:17 WG2004844
Toluene 0.0141 0.00876 1 02/13/2023 00:17 WG2004844
1,2,3-Trichlorobenzene ND 0.0219 1 02/13/2023 00:17 WG2004844
1,2,4-Trichlorobenzene ND 0.0219 1 02/13/2023 00:17 WG2004844
1,1,1-Trichloroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,1,2-Trichloroethane ND 0.00438 1 02/13/2023 00:17 WG2004844
Trichloroethene ND 0.00175 1 02/13/2023 00:17 WG2004844
Trichlorofluoromethane ND 0.00438 1 02/13/2023 00:17 WG2004844
1,2,3-Trichloropropane ND 0.0219 1 02/13/2023 00:17 WG2004844
1,2,4-Trimethylbenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
1,2,3-Trimethylbenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
1,3,5-Trimethylbenzene ND 0.00876 1 02/13/2023 00:17 WG2004844
Vinyl chloride ND 0.00438 1 02/13/2023 00:17 WG2004844
Xylenes, Total ND 0.0114 1 02/13/2023 00:17 WG2004844
(S) Toluene-d8 115 75.0-131 02/13/2023 00:17 WG2004844
(S) 4-Bromofluorobenzene 101 67.0-138 02/13/2023 00:17 WG2004844
(S) 1,2-Dichloroethane-d4 95.3 70.0-130 02/13/2023 00:17 WG2004844
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1584351
SS-12
Collected date/time: 02/09/23 10:20
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND J3 J5 54.4 10 02/16/2023 10:04 WG2005423
C28-C40 Oil Range ND 54.4 10 02/16/2023 10:04 WG2005423
(S) o-Terphenyl 39.2 18.0-148 02/16/2023 10:04 WG2005423
Sample Narrative:
L1584351-01 WG2005423: Dilution due to matrix impact during extract concentration procedure
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND J6 0.462 10 02/16/2023 20:27 WG2004450
PCB 1221 ND 0.462 10 02/16/2023 20:27 WG2004450
PCB 1232 ND 0.462 10 02/16/2023 20:27 WG2004450
PCB 1242 ND 0.462 10 02/16/2023 20:27 WG2004450
PCB 1248 ND 0.231 10 02/16/2023 20:27 WG2004450
PCB 1254 ND 0.231 10 02/16/2023 20:27 WG2004450
PCB 1260 ND J6 0.231 10 02/16/2023 20:27 WG2004450
(S) Decachlorobiphenyl 1510 J1 10.0-135 02/16/2023 20:27 WG2004450
(S) Tetrachloro-m-xylene 23.9 10.0-139 02/16/2023 20:27 WG2004450
Sample Narrative:
L1584351-01 WG2004450: IS/SURR failed on lower dilution.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0453 1 02/15/2023 15:20 WG2004703
Acenaphthylene ND 0.0453 1 02/15/2023 15:20 WG2004703
Anthracene ND 0.0453 1 02/15/2023 15:20 WG2004703
Benzidine ND 2.27 1 02/15/2023 15:20 WG2004703
Benzo(a)anthracene ND 0.0453 1 02/15/2023 15:20 WG2004703
Benzo(b)fluoranthene ND 0.0453 1 02/15/2023 15:20 WG2004703
Benzo(k)fluoranthene ND 0.0453 1 02/15/2023 15:20 WG2004703
Benzo(g,h,i)perylene ND 0.0453 1 02/15/2023 15:20 WG2004703
Benzo(a)pyrene ND 0.0453 1 02/15/2023 15:20 WG2004703
Bis(2-chlorethoxy)methane ND 0.453 1 02/15/2023 15:20 WG2004703
Bis(2-chloroethyl)ether ND 0.453 1 02/15/2023 15:20 WG2004703
2,2-Oxybis(1-Chloropropane) ND 0.453 1 02/15/2023 15:20 WG2004703
4-Bromophenyl-phenylether ND 0.453 1 02/15/2023 15:20 WG2004703
2-Chloronaphthalene ND 0.0453 1 02/15/2023 15:20 WG2004703
4-Chlorophenyl-phenylether ND 0.453 1 02/15/2023 15:20 WG2004703
Chrysene ND 0.0453 1 02/15/2023 15:20 WG2004703
Dibenz(a,h)anthracene ND 0.0453 1 02/15/2023 15:20 WG2004703
3,3-Dichlorobenzidine ND 0.453 1 02/15/2023 15:20 WG2004703
2,4-Dinitrotoluene ND 0.453 1 02/15/2023 15:20 WG2004703
2,6-Dinitrotoluene ND 0.453 1 02/15/2023 15:20 WG2004703
Fluoranthene ND 0.0453 1 02/15/2023 15:20 WG2004703
Fluorene ND 0.0453 1 02/15/2023 15:20 WG2004703
Hexachlorobenzene ND 0.453 1 02/15/2023 15:20 WG2004703
Hexachloro-1,3-butadiene ND 0.453 1 02/15/2023 15:20 WG2004703
Hexachlorocyclopentadiene ND J6 0.453 1 02/15/2023 15:20 WG2004703
Hexachloroethane ND 0.453 1 02/15/2023 15:20 WG2004703
Indeno(1,2,3-cd)pyrene ND 0.0453 1 02/15/2023 15:20 WG2004703
Isophorone ND 0.453 1 02/15/2023 15:20 WG2004703
Naphthalene ND 0.0453 1 02/15/2023 15:20 WG2004703
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1584351
SS-12
Collected date/time: 02/09/23 10:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Nitrobenzene ND 0.453 1 02/15/2023 15:20 WG2004703
n-Nitrosodimethylamine ND 0.453 1 02/15/2023 15:20 WG2004703
n-Nitrosodiphenylamine ND 0.453 1 02/15/2023 15:20 WG2004703
n-Nitrosodi-n-propylamine ND 0.453 1 02/15/2023 15:20 WG2004703
Phenanthrene ND 0.0453 1 02/15/2023 15:20 WG2004703
Benzylbutyl phthalate ND 0.453 1 02/15/2023 15:20 WG2004703
Bis(2-ethylhexyl)phthalate ND 0.453 1 02/15/2023 15:20 WG2004703
Di-n-butyl phthalate ND 0.453 1 02/15/2023 15:20 WG2004703
Diethyl phthalate ND 0.453 1 02/15/2023 15:20 WG2004703
Dimethyl phthalate ND 0.453 1 02/15/2023 15:20 WG2004703
Di-n-octyl phthalate ND 0.453 1 02/15/2023 15:20 WG2004703
Pyrene ND 0.0453 1 02/15/2023 15:20 WG2004703
1,2,4-Trichlorobenzene ND 0.453 1 02/15/2023 15:20 WG2004703
4-Chloro-3-methylphenol ND 0.453 1 02/15/2023 15:20 WG2004703
2-Chlorophenol ND 0.453 1 02/15/2023 15:20 WG2004703
2,4-Dichlorophenol ND 0.453 1 02/15/2023 15:20 WG2004703
2,4-Dimethylphenol ND 0.453 1 02/15/2023 15:20 WG2004703
4,6-Dinitro-2-methylphenol ND 0.453 1 02/15/2023 15:20 WG2004703
2,4-Dinitrophenol ND 0.453 1 02/15/2023 15:20 WG2004703
2-Nitrophenol ND 0.453 1 02/15/2023 15:20 WG2004703
4-Nitrophenol ND 0.453 1 02/15/2023 15:20 WG2004703
Pentachlorophenol ND 0.453 1 02/15/2023 15:20 WG2004703
Phenol ND 0.453 1 02/15/2023 15:20 WG2004703
2,4,6-Trichlorophenol ND 0.453 1 02/15/2023 15:20 WG2004703
(S) Nitrobenzene-d5 42.8 10.0-122 02/15/2023 15:20 WG2004703
(S) 2-Fluorobiphenyl 51.4 15.0-120 02/15/2023 15:20 WG2004703
(S) p-Terphenyl-d14 58.7 10.0-120 02/15/2023 15:20 WG2004703
(S) Phenol-d5 49.5 10.0-120 02/15/2023 15:20 WG2004703
(S) 2-Fluorophenol 54.9 12.0-120 02/15/2023 15:20 WG2004703
(S) 2,4,6-Tribromophenol 72.0 10.0-127 02/15/2023 15:20 WG2004703
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00816 1 02/17/2023 04:55 WG2007018
Acenaphthene ND 0.00816 1 02/17/2023 04:55 WG2007018
Acenaphthylene ND 0.00816 1 02/17/2023 04:55 WG2007018
Benzo(a)anthracene ND 0.00816 1 02/17/2023 04:55 WG2007018
Benzo(a)pyrene ND 0.00816 1 02/17/2023 04:55 WG2007018
Benzo(b)fluoranthene ND 0.00816 1 02/17/2023 04:55 WG2007018
Benzo(g,h,i)perylene ND 0.00816 1 02/17/2023 04:55 WG2007018
Benzo(k)fluoranthene ND 0.00816 1 02/17/2023 04:55 WG2007018
Chrysene ND 0.00816 1 02/17/2023 04:55 WG2007018
Dibenz(a,h)anthracene ND 0.00816 1 02/17/2023 04:55 WG2007018
Fluoranthene ND J3 0.00816 1 02/17/2023 04:55 WG2007018
Fluorene ND 0.00816 1 02/17/2023 04:55 WG2007018
Indeno(1,2,3-cd)pyrene ND 0.00816 1 02/17/2023 04:55 WG2007018
Naphthalene ND 0.0272 1 02/17/2023 04:55 WG2007018
Phenanthrene ND 0.00816 1 02/17/2023 04:55 WG2007018
Pyrene ND J3 0.00816 1 02/17/2023 04:55 WG2007018
1-Methylnaphthalene ND 0.0272 1 02/17/2023 04:55 WG2007018
2-Methylnaphthalene ND 0.0272 1 02/17/2023 04:55 WG2007018
2-Chloronaphthalene ND 0.0272 1 02/17/2023 04:55 WG2007018
(S) p-Terphenyl-d14 61.8 23.0-120 02/17/2023 04:55 WG2007018
(S) Nitrobenzene-d5 47.6 14.0-149 02/17/2023 04:55 WG2007018
(S) 2-Fluorobiphenyl 59.1 34.0-125 02/17/2023 04:55 WG2007018
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1584351
SS-10
Collected date/time: 02/09/23 11:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 41.9 1 02/14/2023 12:09 WG2004469
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 23.9 10 02/16/2023 01:38 WG2004535
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0955 1 02/13/2023 20:57 WG2004804
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 4.77 1 02/14/2023 19:24 WG2005201
Arsenic 11.3 4.77 1 02/14/2023 19:24 WG2005201
Beryllium 0.584 0.477 1 02/14/2023 19:24 WG2005201
Cadmium ND 1.19 1 02/14/2023 19:24 WG2005201
Chromium 17.4 2.39 1 02/14/2023 19:24 WG2005201
Copper 27.7 4.77 1 02/14/2023 19:24 WG2005201
Lead 35.6 1.19 1 02/14/2023 19:24 WG2005201
Nickel 11.4 4.77 1 02/14/2023 19:24 WG2005201
Selenium ND 4.77 1 02/14/2023 19:24 WG2005201
Silver ND 2.39 1 02/14/2023 19:24 WG2005201
Thallium ND 4.77 1 02/14/2023 19:24 WG2005201
Zinc 168 11.9 1 02/14/2023 19:24 WG2005201
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 32.7 10.3 28.7 02/15/2023 13:48 WG2006017
(S) a,a,a-Trifluorotoluene(FID) 95.9 77.0-120 02/15/2023 13:48 WG2006017
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND J3 0.207 1.15 02/12/2023 12:35 WG2004751
Acrylonitrile ND J3 0.0518 1.15 02/12/2023 12:35 WG2004751
Benzene ND 0.00413 1.15 02/12/2023 12:35 WG2004751
Bromobenzene ND 0.0518 1.15 02/12/2023 12:35 WG2004751
Bromodichloromethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Bromoform ND J3 0.104 1.15 02/12/2023 12:35 WG2004751
Bromomethane ND 0.0518 1.15 02/12/2023 12:35 WG2004751
n-Butylbenzene ND 0.0518 1.15 02/12/2023 12:35 WG2004751
sec-Butylbenzene ND 0.0518 1.15 02/12/2023 12:35 WG2004751
tert-Butylbenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
Carbon tetrachloride ND 0.0207 1.15 02/12/2023 12:35 WG2004751
Chlorobenzene ND J3 0.0104 1.15 02/12/2023 12:35 WG2004751
Chlorodibromomethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Chloroethane ND 0.0207 1.15 02/12/2023 12:35 WG2004751
Chloroform ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Chloromethane ND 0.0518 1.15 02/12/2023 12:35 WG2004751
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1584351
SS-10
Collected date/time: 02/09/23 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
4-Chlorotoluene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,2-Dibromo-3-Chloropropane ND J3 0.104 1.15 02/12/2023 12:35 WG2004751
1,2-Dibromoethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Dibromomethane ND J3 0.0207 1.15 02/12/2023 12:35 WG2004751
1,2-Dichlorobenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,3-Dichlorobenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,4-Dichlorobenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
Dichlorodifluoromethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,1-Dichloroethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,2-Dichloroethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,1-Dichloroethene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
cis-1,2-Dichloroethene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
trans-1,2-Dichloroethene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,2-Dichloropropane ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,1-Dichloropropene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,3-Dichloropropane ND 0.0207 1.15 02/12/2023 12:35 WG2004751
cis-1,3-Dichloropropene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
trans-1,3-Dichloropropene ND J3 0.0207 1.15 02/12/2023 12:35 WG2004751
2,2-Dichloropropane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Di-isopropyl ether ND 0.00413 1.15 02/12/2023 12:35 WG2004751
Ethylbenzene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Hexachloro-1,3-butadiene ND 0.104 1.15 02/12/2023 12:35 WG2004751
Isopropylbenzene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
p-Isopropyltoluene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
2-Butanone (MEK)ND J3 0.413 1.15 02/12/2023 12:35 WG2004751
Methylene Chloride ND 0.104 1.15 02/12/2023 12:35 WG2004751
4-Methyl-2-pentanone (MIBK) ND J3 0.104 1.15 02/12/2023 12:35 WG2004751
Methyl tert-butyl ether ND 0.00413 1.15 02/12/2023 12:35 WG2004751
Naphthalene ND 0.0518 1.15 02/12/2023 12:35 WG2004751
n-Propylbenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
Styrene ND J3 0.0518 1.15 02/12/2023 12:35 WG2004751
1,1,1,2-Tetrachloroethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,1,2,2-Tetrachloroethane ND J3 0.0104 1.15 02/12/2023 12:35 WG2004751
1,1,2-Trichlorotrifluoroethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Tetrachloroethene ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Toluene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,2,3-Trichlorobenzene ND 0.0518 1.15 02/12/2023 12:35 WG2004751
1,2,4-Trichlorobenzene ND 0.0518 1.15 02/12/2023 12:35 WG2004751
1,1,1-Trichloroethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,1,2-Trichloroethane ND J3 0.0104 1.15 02/12/2023 12:35 WG2004751
Trichloroethene ND 0.00413 1.15 02/12/2023 12:35 WG2004751
Trichlorofluoromethane ND 0.0104 1.15 02/12/2023 12:35 WG2004751
1,2,3-Trichloropropane ND J3 J4 0.0518 1.15 02/12/2023 12:35 WG2004751
1,2,4-Trimethylbenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,2,3-Trimethylbenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
1,3,5-Trimethylbenzene ND 0.0207 1.15 02/12/2023 12:35 WG2004751
Vinyl chloride ND 0.0104 1.15 02/12/2023 12:35 WG2004751
Xylenes, Total ND 0.0269 1.15 02/12/2023 12:35 WG2004751
(S) Toluene-d8 109 75.0-131 02/12/2023 12:35 WG2004751
(S) 4-Bromofluorobenzene 78.3 67.0-138 02/12/2023 12:35 WG2004751
(S) 1,2-Dichloroethane-d4 81.4 70.0-130 02/12/2023 12:35 WG2004751
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1584351
SS-10
Collected date/time: 02/09/23 11:00
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 9.55 1 02/16/2023 00:06 WG2005423
C28-C40 Oil Range ND 9.55 1 02/16/2023 00:06 WG2005423
(S) o-Terphenyl 75.2 18.0-148 02/16/2023 00:06 WG2005423
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0812 1 02/15/2023 22:10 WG2004450
PCB 1221 ND 0.0812 1 02/15/2023 22:10 WG2004450
PCB 1232 ND 0.0812 1 02/15/2023 22:10 WG2004450
PCB 1242 ND 0.0812 1 02/15/2023 22:10 WG2004450
PCB 1248 ND 0.0406 1 02/15/2023 22:10 WG2004450
PCB 1254 ND 0.0406 1 02/15/2023 22:10 WG2004450
PCB 1260 ND 0.0406 1 02/15/2023 22:10 WG2004450
(S) Decachlorobiphenyl 75.1 10.0-135 02/15/2023 22:10 WG2004450
(S) Tetrachloro-m-xylene 97.2 10.0-139 02/15/2023 22:10 WG2004450
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.399 5 02/16/2023 09:07 WG2004454
Acenaphthylene ND 0.399 5 02/16/2023 09:07 WG2004454
Anthracene ND 0.399 5 02/16/2023 09:07 WG2004454
Benzidine ND 19.9 5 02/16/2023 09:07 WG2004454
Benzo(a)anthracene ND 0.399 5 02/16/2023 09:07 WG2004454
Benzo(b)fluoranthene ND 0.399 5 02/16/2023 09:07 WG2004454
Benzo(k)fluoranthene ND 0.399 5 02/16/2023 09:07 WG2004454
Benzo(g,h,i)perylene ND 0.399 5 02/16/2023 09:07 WG2004454
Benzo(a)pyrene ND 0.399 5 02/16/2023 09:07 WG2004454
Bis(2-chlorethoxy)methane ND 3.99 5 02/16/2023 09:07 WG2004454
Bis(2-chloroethyl)ether ND 3.99 5 02/16/2023 09:07 WG2004454
2,2-Oxybis(1-Chloropropane) ND 3.99 5 02/16/2023 09:07 WG2004454
4-Bromophenyl-phenylether ND 3.99 5 02/16/2023 09:07 WG2004454
2-Chloronaphthalene ND 0.399 5 02/16/2023 09:07 WG2004454
4-Chlorophenyl-phenylether ND 3.99 5 02/16/2023 09:07 WG2004454
Chrysene ND 0.399 5 02/16/2023 09:07 WG2004454
Dibenz(a,h)anthracene ND 0.399 5 02/16/2023 09:07 WG2004454
3,3-Dichlorobenzidine ND 3.99 5 02/16/2023 09:07 WG2004454
2,4-Dinitrotoluene ND 3.99 5 02/16/2023 09:07 WG2004454
2,6-Dinitrotoluene ND 3.99 5 02/16/2023 09:07 WG2004454
Fluoranthene ND 0.399 5 02/16/2023 09:07 WG2004454
Fluorene ND 0.399 5 02/16/2023 09:07 WG2004454
Hexachlorobenzene ND 3.99 5 02/16/2023 09:07 WG2004454
Hexachloro-1,3-butadiene ND 3.99 5 02/16/2023 09:07 WG2004454
Hexachlorocyclopentadiene ND 3.99 5 02/16/2023 09:07 WG2004454
Hexachloroethane ND 3.99 5 02/16/2023 09:07 WG2004454
Indeno(1,2,3-cd)pyrene ND 0.399 5 02/16/2023 09:07 WG2004454
Isophorone ND 3.99 5 02/16/2023 09:07 WG2004454
Naphthalene ND 0.399 5 02/16/2023 09:07 WG2004454
Nitrobenzene ND 3.99 5 02/16/2023 09:07 WG2004454
n-Nitrosodimethylamine ND 3.99 5 02/16/2023 09:07 WG2004454
n-Nitrosodiphenylamine ND 3.99 5 02/16/2023 09:07 WG2004454
n-Nitrosodi-n-propylamine ND 3.99 5 02/16/2023 09:07 WG2004454
Phenanthrene ND 0.399 5 02/16/2023 09:07 WG2004454
Benzylbutyl phthalate ND 3.99 5 02/16/2023 09:07 WG2004454
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1584351
SS-10
Collected date/time: 02/09/23 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 3.99 5 02/16/2023 09:07 WG2004454
Di-n-butyl phthalate ND 3.99 5 02/16/2023 09:07 WG2004454
Diethyl phthalate ND 3.99 5 02/16/2023 09:07 WG2004454
Dimethyl phthalate ND 3.99 5 02/16/2023 09:07 WG2004454
Di-n-octyl phthalate ND 3.99 5 02/16/2023 09:07 WG2004454
Pyrene ND 0.399 5 02/16/2023 09:07 WG2004454
1,2,4-Trichlorobenzene ND 3.99 5 02/16/2023 09:07 WG2004454
4-Chloro-3-methylphenol ND 3.99 5 02/16/2023 09:07 WG2004454
2-Chlorophenol ND 3.99 5 02/16/2023 09:07 WG2004454
2,4-Dichlorophenol ND 3.99 5 02/16/2023 09:07 WG2004454
2,4-Dimethylphenol ND 3.99 5 02/16/2023 09:07 WG2004454
4,6-Dinitro-2-methylphenol ND 3.99 5 02/16/2023 09:07 WG2004454
2,4-Dinitrophenol ND 3.99 5 02/16/2023 09:07 WG2004454
2-Nitrophenol ND 3.99 5 02/16/2023 09:07 WG2004454
4-Nitrophenol ND 3.99 5 02/16/2023 09:07 WG2004454
Pentachlorophenol ND 3.99 5 02/16/2023 09:07 WG2004454
Phenol ND 3.99 5 02/16/2023 09:07 WG2004454
2,4,6-Trichlorophenol ND 3.99 5 02/16/2023 09:07 WG2004454
(S) Nitrobenzene-d5 99.7 10.0-122 02/16/2023 09:07 WG2004454
(S) 2-Fluorobiphenyl 54.1 15.0-120 02/16/2023 09:07 WG2004454
(S) p-Terphenyl-d14 53.5 10.0-120 02/16/2023 09:07 WG2004454
(S) Phenol-d5 46.5 10.0-120 02/16/2023 09:07 WG2004454
(S) 2-Fluorophenol 53.2 12.0-120 02/16/2023 09:07 WG2004454
(S) 2,4,6-Tribromophenol 61.0 10.0-127 02/16/2023 09:07 WG2004454
Sample Narrative:
L1584351-02 WG2004454: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.0143 1 02/17/2023 04:15 WG2007018
Acenaphthene ND 0.0143 1 02/17/2023 04:15 WG2007018
Acenaphthylene ND 0.0143 1 02/17/2023 04:15 WG2007018
Benzo(a)anthracene ND 0.0143 1 02/17/2023 04:15 WG2007018
Benzo(a)pyrene ND 0.0143 1 02/17/2023 04:15 WG2007018
Benzo(b)fluoranthene ND 0.0143 1 02/17/2023 04:15 WG2007018
Benzo(g,h,i)perylene ND 0.0143 1 02/17/2023 04:15 WG2007018
Benzo(k)fluoranthene ND 0.0143 1 02/17/2023 04:15 WG2007018
Chrysene ND 0.0143 1 02/17/2023 04:15 WG2007018
Dibenz(a,h)anthracene ND 0.0143 1 02/17/2023 04:15 WG2007018
Fluoranthene ND 0.0143 1 02/17/2023 04:15 WG2007018
Fluorene ND 0.0143 1 02/17/2023 04:15 WG2007018
Indeno(1,2,3-cd)pyrene ND 0.0143 1 02/17/2023 04:15 WG2007018
Naphthalene ND 0.0477 1 02/17/2023 04:15 WG2007018
Phenanthrene ND 0.0143 1 02/17/2023 04:15 WG2007018
Pyrene ND 0.0143 1 02/17/2023 04:15 WG2007018
1-Methylnaphthalene ND 0.0477 1 02/17/2023 04:15 WG2007018
2-Methylnaphthalene ND 0.0477 1 02/17/2023 04:15 WG2007018
2-Chloronaphthalene ND 0.0477 1 02/17/2023 04:15 WG2007018
(S) p-Terphenyl-d14 67.7 23.0-120 02/17/2023 04:15 WG2007018
(S) Nitrobenzene-d5 46.2 14.0-149 02/17/2023 04:15 WG2007018
(S) 2-Fluorobiphenyl 58.6 34.0-125 02/17/2023 04:15 WG2007018
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1584351
SS-7
Collected date/time: 02/09/23 11:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 51.4 1 02/14/2023 12:09 WG2004469
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.94 1 02/16/2023 01:43 WG2004535
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0778 1 02/13/2023 21:00 WG2004804
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 3.89 1 02/14/2023 19:27 WG2005201
Arsenic 5.16 3.89 1 02/14/2023 19:27 WG2005201
Beryllium ND 0.389 1 02/14/2023 19:27 WG2005201
Cadmium ND 0.972 1 02/14/2023 19:27 WG2005201
Chromium 47.5 1.94 1 02/14/2023 19:27 WG2005201
Copper 24.8 3.89 1 02/14/2023 19:27 WG2005201
Lead 18.1 0.972 1 02/14/2023 19:27 WG2005201
Nickel 13.0 3.89 1 02/14/2023 19:27 WG2005201
Selenium ND 3.89 1 02/14/2023 19:27 WG2005201
Silver ND 1.94 1 02/14/2023 19:27 WG2005201
Thallium ND 3.89 1 02/14/2023 19:27 WG2005201
Zinc 88.0 9.72 1 02/14/2023 19:27 WG2005201
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 7.70 27.5 02/16/2023 12:24 WG2007003
(S) a,a,a-Trifluorotoluene(FID) 95.5 77.0-120 02/16/2023 12:24 WG2007003
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.308 2.2 02/17/2023 00:03 WG2006549
Acrylonitrile ND 0.0770 2.2 02/17/2023 00:03 WG2006549
Benzene ND 0.00616 2.2 02/17/2023 00:03 WG2006549
Bromobenzene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
Bromodichloromethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Bromoform ND 0.154 2.2 02/17/2023 00:03 WG2006549
Bromomethane ND 0.0770 2.2 02/17/2023 00:03 WG2006549
n-Butylbenzene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
sec-Butylbenzene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
tert-Butylbenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
Carbon tetrachloride ND 0.0308 2.2 02/17/2023 00:03 WG2006549
Chlorobenzene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Chlorodibromomethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Chloroethane ND 0.0308 2.2 02/17/2023 00:03 WG2006549
Chloroform ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Chloromethane ND 0.0770 2.2 02/17/2023 00:03 WG2006549
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1584351
SS-7
Collected date/time: 02/09/23 11:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
4-Chlorotoluene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,2-Dibromo-3-Chloropropane ND 0.154 2.2 02/17/2023 00:03 WG2006549
1,2-Dibromoethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Dibromomethane ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,2-Dichlorobenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,3-Dichlorobenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,4-Dichlorobenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
Dichlorodifluoromethane ND J4 0.0154 2.2 02/17/2023 00:03 WG2006549
1,1-Dichloroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,2-Dichloroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,1-Dichloroethene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
cis-1,2-Dichloroethene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
trans-1,2-Dichloroethene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,2-Dichloropropane ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,1-Dichloropropene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,3-Dichloropropane ND 0.0308 2.2 02/17/2023 00:03 WG2006549
cis-1,3-Dichloropropene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
trans-1,3-Dichloropropene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
2,2-Dichloropropane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Di-isopropyl ether ND 0.00616 2.2 02/17/2023 00:03 WG2006549
Ethylbenzene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Hexachloro-1,3-butadiene ND 0.154 2.2 02/17/2023 00:03 WG2006549
Isopropylbenzene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
p-Isopropyltoluene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
2-Butanone (MEK)ND 0.616 2.2 02/17/2023 00:03 WG2006549
Methylene Chloride ND 0.154 2.2 02/17/2023 00:03 WG2006549
4-Methyl-2-pentanone (MIBK) ND 0.154 2.2 02/17/2023 00:03 WG2006549
Methyl tert-butyl ether ND 0.00616 2.2 02/17/2023 00:03 WG2006549
Naphthalene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
n-Propylbenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
Styrene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
1,1,1,2-Tetrachloroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,1,2,2-Tetrachloroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,1,2-Trichlorotrifluoroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Tetrachloroethene ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Toluene 0.0470 0.0308 2.2 02/17/2023 00:03 WG2006549
1,2,3-Trichlorobenzene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
1,2,4-Trichlorobenzene ND 0.0770 2.2 02/17/2023 00:03 WG2006549
1,1,1-Trichloroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,1,2-Trichloroethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Trichloroethene ND 0.00616 2.2 02/17/2023 00:03 WG2006549
Trichlorofluoromethane ND 0.0154 2.2 02/17/2023 00:03 WG2006549
1,2,3-Trichloropropane ND 0.0770 2.2 02/17/2023 00:03 WG2006549
1,2,4-Trimethylbenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,2,3-Trimethylbenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
1,3,5-Trimethylbenzene ND 0.0308 2.2 02/17/2023 00:03 WG2006549
Vinyl chloride ND 0.0154 2.2 02/17/2023 00:03 WG2006549
Xylenes, Total ND 0.0400 2.2 02/17/2023 00:03 WG2006549
(S) Toluene-d8 99.0 75.0-131 02/17/2023 00:03 WG2006549
(S) 4-Bromofluorobenzene 104 67.0-138 02/17/2023 00:03 WG2006549
(S) 1,2-Dichloroethane-d4 90.1 70.0-130 02/17/2023 00:03 WG2006549
Sample Narrative:
L1584351-03 WG2006549: Lowest possible dilution due to sample foaming.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1584351
SS-7
Collected date/time: 02/09/23 11:35
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 23.7 15.6 2 02/15/2023 05:44 WG2005842
C28-C40 Oil Range 176 15.6 2 02/15/2023 09:58 WG2005842
(S) o-Terphenyl 59.3 18.0-148 02/15/2023 09:58 WG2005842
(S) o-Terphenyl 85.4 18.0-148 02/15/2023 05:44 WG2005842
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0661 1 02/16/2023 00:38 WG2004450
PCB 1221 ND 0.0661 1 02/16/2023 00:38 WG2004450
PCB 1232 ND 0.0661 1 02/16/2023 00:38 WG2004450
PCB 1242 ND 0.0661 1 02/16/2023 00:38 WG2004450
PCB 1248 ND 0.0331 1 02/16/2023 00:38 WG2004450
PCB 1254 ND 0.0331 1 02/16/2023 00:38 WG2004450
PCB 1260 ND 0.0331 1 02/16/2023 00:38 WG2004450
(S) Decachlorobiphenyl 61.7 10.0-135 02/16/2023 00:38 WG2004450
(S) Tetrachloro-m-xylene 74.2 10.0-139 02/16/2023 00:38 WG2004450
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0647 1 02/12/2023 02:11 WG2004454
Acenaphthylene ND 0.0647 1 02/12/2023 02:11 WG2004454
Anthracene ND 0.0647 1 02/12/2023 02:11 WG2004454
Benzidine ND 3.25 1 02/12/2023 02:11 WG2004454
Benzo(a)anthracene ND 0.0647 1 02/12/2023 02:11 WG2004454
Benzo(b)fluoranthene ND 0.0647 1 02/12/2023 02:11 WG2004454
Benzo(k)fluoranthene ND 0.0647 1 02/12/2023 02:11 WG2004454
Benzo(g,h,i)perylene ND 0.0647 1 02/12/2023 02:11 WG2004454
Benzo(a)pyrene ND 0.0647 1 02/12/2023 02:11 WG2004454
Bis(2-chlorethoxy)methane ND 0.647 1 02/12/2023 02:11 WG2004454
Bis(2-chloroethyl)ether ND 0.647 1 02/12/2023 02:11 WG2004454
2,2-Oxybis(1-Chloropropane) ND 0.647 1 02/12/2023 02:11 WG2004454
4-Bromophenyl-phenylether ND 0.647 1 02/12/2023 02:11 WG2004454
2-Chloronaphthalene ND 0.0647 1 02/12/2023 02:11 WG2004454
4-Chlorophenyl-phenylether ND 0.647 1 02/12/2023 02:11 WG2004454
Chrysene ND 0.0647 1 02/12/2023 02:11 WG2004454
Dibenz(a,h)anthracene ND 0.0647 1 02/12/2023 02:11 WG2004454
3,3-Dichlorobenzidine ND 0.647 1 02/12/2023 02:11 WG2004454
2,4-Dinitrotoluene ND 0.647 1 02/12/2023 02:11 WG2004454
2,6-Dinitrotoluene ND 0.647 1 02/12/2023 02:11 WG2004454
Fluoranthene ND 0.0647 1 02/12/2023 02:11 WG2004454
Fluorene ND 0.0647 1 02/12/2023 02:11 WG2004454
Hexachlorobenzene ND 0.647 1 02/12/2023 02:11 WG2004454
Hexachloro-1,3-butadiene ND 0.647 1 02/12/2023 02:11 WG2004454
Hexachlorocyclopentadiene ND 0.647 1 02/12/2023 02:11 WG2004454
Hexachloroethane ND 0.647 1 02/12/2023 02:11 WG2004454
Indeno(1,2,3-cd)pyrene ND 0.0647 1 02/12/2023 02:11 WG2004454
Isophorone ND 0.647 1 02/12/2023 02:11 WG2004454
Naphthalene ND 0.0647 1 02/12/2023 02:11 WG2004454
Nitrobenzene ND 0.647 1 02/12/2023 02:11 WG2004454
n-Nitrosodimethylamine ND 0.647 1 02/12/2023 02:11 WG2004454
n-Nitrosodiphenylamine ND 0.647 1 02/12/2023 02:11 WG2004454
n-Nitrosodi-n-propylamine ND 0.647 1 02/12/2023 02:11 WG2004454
Phenanthrene ND 0.0647 1 02/12/2023 02:11 WG2004454
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1584351
SS-7
Collected date/time: 02/09/23 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzylbutyl phthalate ND 0.647 1 02/12/2023 02:11 WG2004454
Bis(2-ethylhexyl)phthalate ND 0.647 1 02/12/2023 02:11 WG2004454
Di-n-butyl phthalate ND 0.647 1 02/12/2023 02:11 WG2004454
Diethyl phthalate ND 0.647 1 02/12/2023 02:11 WG2004454
Dimethyl phthalate ND 0.647 1 02/12/2023 02:11 WG2004454
Di-n-octyl phthalate ND 0.647 1 02/12/2023 02:11 WG2004454
Pyrene ND 0.0647 1 02/12/2023 02:11 WG2004454
1,2,4-Trichlorobenzene ND 0.647 1 02/12/2023 02:11 WG2004454
4-Chloro-3-methylphenol ND 0.647 1 02/12/2023 02:11 WG2004454
2-Chlorophenol ND 0.647 1 02/12/2023 02:11 WG2004454
2,4-Dichlorophenol ND 0.647 1 02/12/2023 02:11 WG2004454
2,4-Dimethylphenol ND 0.647 1 02/12/2023 02:11 WG2004454
4,6-Dinitro-2-methylphenol ND 0.647 1 02/12/2023 02:11 WG2004454
2,4-Dinitrophenol ND 0.647 1 02/12/2023 02:11 WG2004454
2-Nitrophenol ND 0.647 1 02/12/2023 02:11 WG2004454
4-Nitrophenol ND 0.647 1 02/12/2023 02:11 WG2004454
Pentachlorophenol ND 0.647 1 02/12/2023 02:11 WG2004454
Phenol ND 0.647 1 02/12/2023 02:11 WG2004454
2,4,6-Trichlorophenol ND 0.647 1 02/12/2023 02:11 WG2004454
(S) Nitrobenzene-d5 60.7 10.0-122 02/12/2023 02:11 WG2004454
(S) 2-Fluorobiphenyl 67.2 15.0-120 02/12/2023 02:11 WG2004454
(S) p-Terphenyl-d14 79.6 10.0-120 02/12/2023 02:11 WG2004454
(S) Phenol-d5 60.4 10.0-120 02/12/2023 02:11 WG2004454
(S) 2-Fluorophenol 69.5 12.0-120 02/12/2023 02:11 WG2004454
(S) 2,4,6-Tribromophenol 86.1 10.0-127 02/12/2023 02:11 WG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.0117 1 02/17/2023 05:15 WG2007018
Acenaphthene ND 0.0117 1 02/17/2023 05:15 WG2007018
Acenaphthylene ND 0.0117 1 02/17/2023 05:15 WG2007018
Benzo(a)anthracene 0.0119 0.0117 1 02/17/2023 05:15 WG2007018
Benzo(a)pyrene 0.0133 0.0117 1 02/17/2023 05:15 WG2007018
Benzo(b)fluoranthene 0.0183 0.0117 1 02/17/2023 05:15 WG2007018
Benzo(g,h,i)perylene 0.0200 0.0117 1 02/17/2023 05:15 WG2007018
Benzo(k)fluoranthene ND 0.0117 1 02/17/2023 05:15 WG2007018
Chrysene 0.0137 0.0117 1 02/17/2023 05:15 WG2007018
Dibenz(a,h)anthracene ND 0.0117 1 02/17/2023 05:15 WG2007018
Fluoranthene 0.0257 0.0117 1 02/17/2023 05:15 WG2007018
Fluorene ND 0.0117 1 02/17/2023 05:15 WG2007018
Indeno(1,2,3-cd)pyrene 0.0121 0.0117 1 02/17/2023 05:15 WG2007018
Naphthalene ND 0.0389 1 02/17/2023 05:15 WG2007018
Phenanthrene 0.0177 0.0117 1 02/17/2023 05:15 WG2007018
Pyrene 0.0220 0.0117 1 02/17/2023 05:15 WG2007018
1-Methylnaphthalene ND 0.0389 1 02/17/2023 05:15 WG2007018
2-Methylnaphthalene ND 0.0389 1 02/17/2023 05:15 WG2007018
2-Chloronaphthalene ND 0.0389 1 02/17/2023 05:15 WG2007018
(S) p-Terphenyl-d14 58.7 23.0-120 02/17/2023 05:15 WG2007018
(S) Nitrobenzene-d5 50.5 14.0-149 02/17/2023 05:15 WG2007018
(S) 2-Fluorobiphenyl 57.2 34.0-125 02/17/2023 05:15 WG2007018
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1584351
SS-6
Collected date/time: 02/09/23 11:58
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 67.0 1 02/14/2023 12:09 WG2004469
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.49 1 02/16/2023 01:48 WG2004535
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0597 1 02/13/2023 21:07 WG2004804
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.98 1 02/15/2023 01:22 WG2005200
Arsenic 7.43 2.98 1 02/15/2023 01:22 WG2005200
Beryllium 0.336 0.298 1 02/15/2023 01:22 WG2005200
Cadmium ND 0.746 1 02/15/2023 01:22 WG2005200
Chromium 8.78 1.49 1 02/15/2023 01:22 WG2005200
Copper 14.8 2.98 1 02/15/2023 01:22 WG2005200
Lead 21.1 0.746 1 02/15/2023 01:22 WG2005200
Nickel 6.78 2.98 1 02/15/2023 01:22 WG2005200
Selenium ND 2.98 1 02/15/2023 01:22 WG2005200
Silver ND 1.49 1 02/15/2023 01:22 WG2005200
Thallium ND 2.98 1 02/15/2023 01:22 WG2005200
Zinc 42.5 7.46 1 02/15/2023 01:22 WG2005200
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 5.17 25 02/16/2023 12:45 WG2007003
(S) a,a,a-Trifluorotoluene(FID) 96.4 77.0-120 02/16/2023 12:45 WG2007003
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND J3 0.103 1 02/12/2023 12:55 WG2004751
Acrylonitrile ND J3 0.0259 1 02/12/2023 12:55 WG2004751
Benzene ND 0.00207 1 02/12/2023 12:55 WG2004751
Bromobenzene ND 0.0259 1 02/12/2023 12:55 WG2004751
Bromodichloromethane ND 0.00517 1 02/12/2023 12:55 WG2004751
Bromoform ND J3 0.0517 1 02/12/2023 12:55 WG2004751
Bromomethane ND 0.0259 1 02/12/2023 12:55 WG2004751
n-Butylbenzene ND 0.0259 1 02/12/2023 12:55 WG2004751
sec-Butylbenzene ND 0.0259 1 02/12/2023 12:55 WG2004751
tert-Butylbenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
Carbon tetrachloride ND 0.0103 1 02/12/2023 12:55 WG2004751
Chlorobenzene ND J3 0.00517 1 02/12/2023 12:55 WG2004751
Chlorodibromomethane ND 0.00517 1 02/12/2023 12:55 WG2004751
Chloroethane ND 0.0103 1 02/12/2023 12:55 WG2004751
Chloroform ND 0.00517 1 02/12/2023 12:55 WG2004751
Chloromethane ND 0.0259 1 02/12/2023 12:55 WG2004751
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1584351
SS-6
Collected date/time: 02/09/23 11:58
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00517 1 02/12/2023 12:55 WG2004751
4-Chlorotoluene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,2-Dibromo-3-Chloropropane ND J3 0.0517 1 02/12/2023 12:55 WG2004751
1,2-Dibromoethane ND 0.00517 1 02/12/2023 12:55 WG2004751
Dibromomethane ND J3 0.0103 1 02/12/2023 12:55 WG2004751
1,2-Dichlorobenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,3-Dichlorobenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,4-Dichlorobenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
Dichlorodifluoromethane ND 0.00517 1 02/12/2023 12:55 WG2004751
1,1-Dichloroethane ND 0.00517 1 02/12/2023 12:55 WG2004751
1,2-Dichloroethane ND 0.00517 1 02/12/2023 12:55 WG2004751
1,1-Dichloroethene ND 0.00517 1 02/12/2023 12:55 WG2004751
cis-1,2-Dichloroethene ND 0.00517 1 02/12/2023 12:55 WG2004751
trans-1,2-Dichloroethene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,2-Dichloropropane ND 0.0103 1 02/12/2023 12:55 WG2004751
1,1-Dichloropropene ND 0.00517 1 02/12/2023 12:55 WG2004751
1,3-Dichloropropane ND 0.0103 1 02/12/2023 12:55 WG2004751
cis-1,3-Dichloropropene ND 0.00517 1 02/12/2023 12:55 WG2004751
trans-1,3-Dichloropropene ND J3 0.0103 1 02/12/2023 12:55 WG2004751
2,2-Dichloropropane ND 0.00517 1 02/12/2023 12:55 WG2004751
Di-isopropyl ether ND 0.00207 1 02/12/2023 12:55 WG2004751
Ethylbenzene ND 0.00517 1 02/12/2023 12:55 WG2004751
Hexachloro-1,3-butadiene ND 0.0517 1 02/12/2023 12:55 WG2004751
Isopropylbenzene ND 0.00517 1 02/12/2023 12:55 WG2004751
p-Isopropyltoluene ND 0.0103 1 02/12/2023 12:55 WG2004751
2-Butanone (MEK)ND J3 0.207 1 02/12/2023 12:55 WG2004751
Methylene Chloride ND 0.0517 1 02/12/2023 12:55 WG2004751
4-Methyl-2-pentanone (MIBK) ND J3 0.0517 1 02/12/2023 12:55 WG2004751
Methyl tert-butyl ether ND 0.00207 1 02/12/2023 12:55 WG2004751
Naphthalene ND 0.0259 1 02/12/2023 12:55 WG2004751
n-Propylbenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
Styrene ND J3 0.0259 1 02/12/2023 12:55 WG2004751
1,1,1,2-Tetrachloroethane ND 0.00517 1 02/12/2023 12:55 WG2004751
1,1,2,2-Tetrachloroethane ND J3 0.00517 1 02/12/2023 12:55 WG2004751
1,1,2-Trichlorotrifluoroethane ND 0.00517 1 02/12/2023 12:55 WG2004751
Tetrachloroethene ND 0.00517 1 02/12/2023 12:55 WG2004751
Toluene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,2,3-Trichlorobenzene ND 0.0259 1 02/12/2023 12:55 WG2004751
1,2,4-Trichlorobenzene ND 0.0259 1 02/12/2023 12:55 WG2004751
1,1,1-Trichloroethane ND 0.00517 1 02/12/2023 12:55 WG2004751
1,1,2-Trichloroethane ND J3 0.00517 1 02/12/2023 12:55 WG2004751
Trichloroethene ND 0.00207 1 02/12/2023 12:55 WG2004751
Trichlorofluoromethane ND 0.00517 1 02/12/2023 12:55 WG2004751
1,2,3-Trichloropropane ND J3 J4 0.0259 1 02/12/2023 12:55 WG2004751
1,2,4-Trimethylbenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,2,3-Trimethylbenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
1,3,5-Trimethylbenzene ND 0.0103 1 02/12/2023 12:55 WG2004751
Vinyl chloride ND 0.00517 1 02/12/2023 12:55 WG2004751
Xylenes, Total ND 0.0134 1 02/12/2023 12:55 WG2004751
(S) Toluene-d8 110 75.0-131 02/12/2023 12:55 WG2004751
(S) 4-Bromofluorobenzene 79.1 67.0-138 02/12/2023 12:55 WG2004751
(S) 1,2-Dichloroethane-d4 75.5 70.0-130 02/12/2023 12:55 WG2004751
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1584351
SS-6
Collected date/time: 02/09/23 11:58
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.97 1 02/15/2023 05:31 WG2005842
C28-C40 Oil Range ND 5.97 1 02/15/2023 05:31 WG2005842
(S) o-Terphenyl 71.0 18.0-148 02/15/2023 05:31 WG2005842
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0507 1 02/15/2023 22:22 WG2004450
PCB 1221 ND 0.0507 1 02/15/2023 22:22 WG2004450
PCB 1232 ND 0.0507 1 02/15/2023 22:22 WG2004450
PCB 1242 ND 0.0507 1 02/15/2023 22:22 WG2004450
PCB 1248 ND 0.0254 1 02/15/2023 22:22 WG2004450
PCB 1254 ND 0.0254 1 02/15/2023 22:22 WG2004450
PCB 1260 ND 0.0254 1 02/15/2023 22:22 WG2004450
(S) Decachlorobiphenyl 62.1 10.0-135 02/15/2023 22:22 WG2004450
(S) Tetrachloro-m-xylene 94.3 10.0-139 02/15/2023 22:22 WG2004450
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0497 1 02/12/2023 00:46 WG2004454
Acenaphthylene ND 0.0497 1 02/12/2023 00:46 WG2004454
Anthracene ND 0.0497 1 02/12/2023 00:46 WG2004454
Benzidine ND 2.49 1 02/12/2023 00:46 WG2004454
Benzo(a)anthracene ND 0.0497 1 02/12/2023 00:46 WG2004454
Benzo(b)fluoranthene ND 0.0497 1 02/12/2023 00:46 WG2004454
Benzo(k)fluoranthene ND 0.0497 1 02/12/2023 00:46 WG2004454
Benzo(g,h,i)perylene ND 0.0497 1 02/12/2023 00:46 WG2004454
Benzo(a)pyrene ND 0.0497 1 02/12/2023 00:46 WG2004454
Bis(2-chlorethoxy)methane ND 0.497 1 02/12/2023 00:46 WG2004454
Bis(2-chloroethyl)ether ND 0.497 1 02/12/2023 00:46 WG2004454
2,2-Oxybis(1-Chloropropane) ND 0.497 1 02/12/2023 00:46 WG2004454
4-Bromophenyl-phenylether ND 0.497 1 02/12/2023 00:46 WG2004454
2-Chloronaphthalene ND 0.0497 1 02/12/2023 00:46 WG2004454
4-Chlorophenyl-phenylether ND 0.497 1 02/12/2023 00:46 WG2004454
Chrysene ND 0.0497 1 02/12/2023 00:46 WG2004454
Dibenz(a,h)anthracene ND 0.0497 1 02/12/2023 00:46 WG2004454
3,3-Dichlorobenzidine ND 0.497 1 02/12/2023 00:46 WG2004454
2,4-Dinitrotoluene ND 0.497 1 02/12/2023 00:46 WG2004454
2,6-Dinitrotoluene ND 0.497 1 02/12/2023 00:46 WG2004454
Fluoranthene ND 0.0497 1 02/12/2023 00:46 WG2004454
Fluorene ND 0.0497 1 02/12/2023 00:46 WG2004454
Hexachlorobenzene ND 0.497 1 02/12/2023 00:46 WG2004454
Hexachloro-1,3-butadiene ND 0.497 1 02/12/2023 00:46 WG2004454
Hexachlorocyclopentadiene ND 0.497 1 02/12/2023 00:46 WG2004454
Hexachloroethane ND 0.497 1 02/12/2023 00:46 WG2004454
Indeno(1,2,3-cd)pyrene ND 0.0497 1 02/12/2023 00:46 WG2004454
Isophorone ND 0.497 1 02/12/2023 00:46 WG2004454
Naphthalene ND 0.0497 1 02/12/2023 00:46 WG2004454
Nitrobenzene ND 0.497 1 02/12/2023 00:46 WG2004454
n-Nitrosodimethylamine ND 0.497 1 02/12/2023 00:46 WG2004454
n-Nitrosodiphenylamine ND 0.497 1 02/12/2023 00:46 WG2004454
n-Nitrosodi-n-propylamine ND 0.497 1 02/12/2023 00:46 WG2004454
Phenanthrene ND 0.0497 1 02/12/2023 00:46 WG2004454
Benzylbutyl phthalate ND 0.497 1 02/12/2023 00:46 WG2004454
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1584351
SS-6
Collected date/time: 02/09/23 11:58
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.497 1 02/12/2023 00:46 WG2004454
Di-n-butyl phthalate ND 0.497 1 02/12/2023 00:46 WG2004454
Diethyl phthalate ND 0.497 1 02/12/2023 00:46 WG2004454
Dimethyl phthalate ND 0.497 1 02/12/2023 00:46 WG2004454
Di-n-octyl phthalate ND 0.497 1 02/12/2023 00:46 WG2004454
Pyrene ND 0.0497 1 02/12/2023 00:46 WG2004454
1,2,4-Trichlorobenzene ND 0.497 1 02/12/2023 00:46 WG2004454
4-Chloro-3-methylphenol ND 0.497 1 02/12/2023 00:46 WG2004454
2-Chlorophenol ND 0.497 1 02/12/2023 00:46 WG2004454
2,4-Dichlorophenol ND 0.497 1 02/12/2023 00:46 WG2004454
2,4-Dimethylphenol ND 0.497 1 02/12/2023 00:46 WG2004454
4,6-Dinitro-2-methylphenol ND 0.497 1 02/12/2023 00:46 WG2004454
2,4-Dinitrophenol ND 0.497 1 02/12/2023 00:46 WG2004454
2-Nitrophenol ND 0.497 1 02/12/2023 00:46 WG2004454
4-Nitrophenol ND 0.497 1 02/12/2023 00:46 WG2004454
Pentachlorophenol ND 0.497 1 02/12/2023 00:46 WG2004454
Phenol ND 0.497 1 02/12/2023 00:46 WG2004454
2,4,6-Trichlorophenol ND 0.497 1 02/12/2023 00:46 WG2004454
(S) Nitrobenzene-d5 60.3 10.0-122 02/12/2023 00:46 WG2004454
(S) 2-Fluorobiphenyl 68.6 15.0-120 02/12/2023 00:46 WG2004454
(S) p-Terphenyl-d14 75.6 10.0-120 02/12/2023 00:46 WG2004454
(S) Phenol-d5 61.4 10.0-120 02/12/2023 00:46 WG2004454
(S) 2-Fluorophenol 70.3 12.0-120 02/12/2023 00:46 WG2004454
(S) 2,4,6-Tribromophenol 88.7 10.0-127 02/12/2023 00:46 WG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00895 1 02/17/2023 02:36 WG2007018
Acenaphthene ND 0.00895 1 02/17/2023 02:36 WG2007018
Acenaphthylene ND 0.00895 1 02/17/2023 02:36 WG2007018
Benzo(a)anthracene ND 0.00895 1 02/17/2023 02:36 WG2007018
Benzo(a)pyrene ND 0.00895 1 02/17/2023 02:36 WG2007018
Benzo(b)fluoranthene ND 0.00895 1 02/17/2023 02:36 WG2007018
Benzo(g,h,i)perylene ND 0.00895 1 02/17/2023 02:36 WG2007018
Benzo(k)fluoranthene ND 0.00895 1 02/17/2023 02:36 WG2007018
Chrysene ND 0.00895 1 02/17/2023 02:36 WG2007018
Dibenz(a,h)anthracene ND 0.00895 1 02/17/2023 02:36 WG2007018
Fluoranthene ND 0.00895 1 02/17/2023 02:36 WG2007018
Fluorene ND 0.00895 1 02/17/2023 02:36 WG2007018
Indeno(1,2,3-cd)pyrene ND 0.00895 1 02/17/2023 02:36 WG2007018
Naphthalene ND 0.0298 1 02/17/2023 02:36 WG2007018
Phenanthrene ND 0.00895 1 02/17/2023 02:36 WG2007018
Pyrene 0.00925 0.00895 1 02/17/2023 02:36 WG2007018
1-Methylnaphthalene ND 0.0298 1 02/17/2023 02:36 WG2007018
2-Methylnaphthalene ND 0.0298 1 02/17/2023 02:36 WG2007018
2-Chloronaphthalene ND 0.0298 1 02/17/2023 02:36 WG2007018
(S) p-Terphenyl-d14 61.3 23.0-120 02/17/2023 02:36 WG2007018
(S) Nitrobenzene-d5 46.3 14.0-149 02/17/2023 02:36 WG2007018
(S) 2-Fluorobiphenyl 54.6 34.0-125 02/17/2023 02:36 WG2007018
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004469
Total Solids by Method 2540 G-2011 L1584351-01,02,03,04
Method Blank (MB)
(MB) R3890943-1 02/14/23 12:09
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00400
L1584340-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1584340-01 02/14/23 12:09 • (DUP) R3890943-3 02/14/23 12:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 97.5 97.3 1 0.272 10
Laboratory Control Sample (LCS)
(LCS) R3890943-2 02/14/23 12:09
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004535
Wet Chemistry by Method 7199 L1584351-01,02,03,04
Method Blank (MB)
(MB) R3891403-1 02/16/23 00:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1584585-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1584585-01 02/16/23 01:53 • (DUP) R3891403-7 02/16/23 01:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
L1584587-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1584587-03 02/16/23 02:51 • (DUP) R3891403-8 02/16/23 02:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3891403-2 02/16/23 00:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 11.4 114 80.0-120
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/16/23 01:02 • (MS) R3891403-3 02/16/23 01:07 • (MSD) R3891403-4 02/16/23 01:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 27.2 ND 3.38 ND 12.4 1.30 1 75.0-125 J6 J3 J6 162 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004535
Wet Chemistry by Method 7199 L1584351-01,02,03,04
L1584351-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1584351-01 02/16/23 01:02 • (MS) R3891403-5 02/16/23 01:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 858 ND 764 89.0 50 75.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004804
Mercury by Method 7471A L1584351-01,02,03,04
Method Blank (MB)
(MB) R3890332-1 02/13/23 20:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3890332-2 02/13/23 20:40
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.545 109 80.0-120
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/13/23 20:42 • (MS) R3890332-3 02/13/23 20:45 • (MSD) R3890332-4 02/13/23 20:47
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.680 ND 0.613 0.882 90.2 130 1 75.0-125 J3 J5 36.0 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2005200
Metals (ICP) by Method 6010B L1584351-04
Method Blank (MB)
(MB) R3890895-1 02/15/23 00:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper 0.412 J 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3890895-2 02/15/23 00:38
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 102 102 80.0-120
Arsenic 100 95.6 95.6 80.0-120
Beryllium 100 98.2 98.2 80.0-120
Cadmium 100 99.4 99.4 80.0-120
Chromium 100 103 103 80.0-120
Copper 100 102 102 80.0-120
Lead 100 101 101 80.0-120
Nickel 100 95.0 95.0 80.0-120
Selenium 100 101 101 80.0-120
Silver 20.0 19.9 99.3 80.0-120
Thallium 100 96.9 96.9 80.0-120
Zinc 100 98.2 98.2 80.0-120
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/15/23 00:41 • (MS) R3890895-5 02/15/23 00:49 • (MSD) R3890895-6 02/15/23 00:51
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 103 ND 74.3 75.3 72.5 73.4 1 75.0-125 J6 J6 1.22 20
Arsenic 103 ND 95.5 93.6 91.9 90.0 1 75.0-125 1.98 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2005200
Metals (ICP) by Method 6010B L1584351-04
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/15/23 00:41 • (MS) R3890895-5 02/15/23 00:49 • (MSD) R3890895-6 02/15/23 00:51
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 103 0.348 97.1 95.7 94.3 93.0 1 75.0-125 1.41 20
Cadmium 103 ND 99.5 98.3 97.0 95.8 1 75.0-125 1.29 20
Chromium 103 9.04 108 107 97.0 95.4 1 75.0-125 1.54 20
Copper 103 16.6 113 110 93.6 91.3 1 75.0-125 2.07 20
Lead 103 4.44 107 105 100 98.0 1 75.0-125 2.04 20
Nickel 103 9.95 105 105 93.1 92.5 1 75.0-125 0.554 20
Selenium 103 ND 101 99.4 98.2 97.0 1 75.0-125 1.26 20
Silver 20.5 ND 19.9 19.6 97.1 95.5 1 75.0-125 1.71 20
Thallium 103 ND 96.6 95.5 94.2 93.1 1 75.0-125 1.11 20
Zinc 103 29.1 125 123 93.5 91.6 1 75.0-125 1.62 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2005201
Metals (ICP) by Method 6010B L1584351-01,02,03
Method Blank (MB)
(MB) R3890832-1 02/14/23 18:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3890832-2 02/14/23 18:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 102 102 80.0-120
Arsenic 100 92.5 92.5 80.0-120
Beryllium 100 93.9 93.9 80.0-120
Cadmium 100 97.0 97.0 80.0-120
Chromium 100 102 102 80.0-120
Copper 100 97.4 97.4 80.0-120
Lead 100 98.5 98.5 80.0-120
Nickel 100 90.6 90.6 80.0-120
Selenium 100 100 100 80.0-120
Silver 20.0 19.5 97.7 80.0-120
Thallium 100 93.5 93.5 80.0-120
Zinc 100 94.3 94.3 80.0-120
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/14/23 18:16 • (MS) R3890832-5 02/14/23 18:24 • (MSD) R3890832-6 02/14/23 18:26
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 136 ND 106 110 78.1 80.9 1 75.0-125 3.50 20
Arsenic 136 6.26 126 136 88.2 95.5 1 75.0-125 7.59 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2005201
Metals (ICP) by Method 6010B L1584351-01,02,03
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/14/23 18:16 • (MS) R3890832-5 02/14/23 18:24 • (MSD) R3890832-6 02/14/23 18:26
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 136 0.384 119 126 87.1 92.5 1 75.0-125 6.01 20
Cadmium 136 ND 124 132 90.7 96.9 1 75.0-125 6.61 20
Chromium 136 20.6 143 150 89.8 94.9 1 75.0-125 4.76 20
Copper 136 17.0 144 151 93.5 98.7 1 75.0-125 4.76 20
Lead 136 30.1 135 143 77.3 83.1 1 75.0-125 5.71 20
Nickel 136 7.03 125 133 86.9 92.3 1 75.0-125 5.67 20
Selenium 136 ND 128 135 94.1 99.2 1 75.0-125 5.30 20
Silver 27.2 ND 25.2 27.0 92.5 99.1 1 75.0-125 6.91 20
Thallium 136 ND 117 126 86.0 92.8 1 75.0-125 7.62 20
Zinc 136 103 212 229 79.7 92.3 1 75.0-125 7.77 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2006017
Volatile Organic Compounds (GC) by Method 8015D/GRO L1584351-02
Method Blank (MB)
(MB) R3891231-2 02/15/23 12:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.543 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)101 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3891231-1 02/15/23 11:17
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.24 95.3 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 100 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2007003
Volatile Organic Compounds (GC) by Method 8015D/GRO L1584351-01,03,04
Method Blank (MB)
(MB) R3891785-3 02/16/23 11:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.968 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)95.5 77.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3891785-1 02/16/23 10:01 • (LCSD) R3891785-2 02/16/23 10:21
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.50 4.88 4.61 88.7 83.8 72.0-127 5.69 20
(S)
a,a,a-Trifluorotoluene(FID) 99.9 102 77.0-120
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/16/23 12:04 • (MS) R3891785-4 02/16/23 18:54 • (MSD) R3891785-5 02/16/23 19:15
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 263 ND 261 244 98.6 92.2 28.5 10.0-151 6.62 28
(S)
a,a,a-Trifluorotoluene(FID) 108 101 77.0-120
L1584896-26 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584896-26 02/16/23 16:51 • (MS) R3891785-6 02/16/23 19:35 • (MSD) R3891785-7 02/16/23 19:56
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 175 ND 190 184 107 104 30.3 10.0-151 3.37 28
(S)
a,a,a-Trifluorotoluene(FID) 112 111 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004751
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-02,04
Method Blank (MB)
(MB) R3890654-3 02/12/23 11:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004751
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-02,04
Method Blank (MB)
(MB) R3890654-3 02/12/23 11:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 110 75.0-131
(S) 4-Bromofluorobenzene 90.3 67.0-138
(S) 1,2-Dichloroethane-d4 83.4 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3890654-1 02/12/23 09:44 • (LCSD) R3890654-2 02/12/23 10:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.521 0.338 83.4 54.1 10.0-160 J3 42.6 31
Acrylonitrile 0.625 0.697 0.531 112 85.0 45.0-153 J3 27.0 22
Benzene 0.125 0.142 0.122 114 97.6 70.0-123 15.2 20
Bromobenzene 0.125 0.151 0.128 121 102 73.0-121 16.5 20
Bromodichloromethane 0.125 0.149 0.127 119 102 73.0-121 15.9 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004751
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-02,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3890654-1 02/12/23 09:44 • (LCSD) R3890654-2 02/12/23 10:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.162 0.129 130 103 64.0-132 J3 22.7 20
Bromomethane 0.125 0.129 0.111 103 88.8 56.0-147 15.0 20
n-Butylbenzene 0.125 0.123 0.108 98.4 86.4 68.0-135 13.0 20
sec-Butylbenzene 0.125 0.131 0.111 105 88.8 74.0-130 16.5 20
tert-Butylbenzene 0.125 0.128 0.111 102 88.8 75.0-127 14.2 20
Carbon tetrachloride 0.125 0.145 0.135 116 108 66.0-128 7.14 20
Chlorobenzene 0.125 0.153 0.125 122 100 76.0-128 J3 20.1 20
Chlorodibromomethane 0.125 0.158 0.131 126 105 74.0-127 18.7 20
Chloroethane 0.125 0.124 0.108 99.2 86.4 61.0-134 13.8 20
Chloroform 0.125 0.139 0.118 111 94.4 72.0-123 16.3 20
Chloromethane 0.125 0.123 0.111 98.4 88.8 51.0-138 10.3 20
2-Chlorotoluene 0.125 0.150 0.129 120 103 75.0-124 15.1 20
4-Chlorotoluene 0.125 0.138 0.117 110 93.6 75.0-124 16.5 20
1,2-Dibromo-3-Chloropropane 0.125 0.142 0.110 114 88.0 59.0-130 J3 25.4 20
1,2-Dibromoethane 0.125 0.139 0.116 111 92.8 74.0-128 18.0 20
Dibromomethane 0.125 0.136 0.107 109 85.6 75.0-122 J3 23.9 20
1,2-Dichlorobenzene 0.125 0.146 0.121 117 96.8 76.0-124 18.7 20
1,3-Dichlorobenzene 0.125 0.148 0.123 118 98.4 76.0-125 18.5 20
1,4-Dichlorobenzene 0.125 0.148 0.127 118 102 77.0-121 15.3 20
Dichlorodifluoromethane 0.125 0.117 0.114 93.6 91.2 43.0-156 2.60 20
1,1-Dichloroethane 0.125 0.138 0.124 110 99.2 70.0-127 10.7 20
1,2-Dichloroethane 0.125 0.127 0.105 102 84.0 65.0-131 19.0 20
1,1-Dichloroethene 0.125 0.143 0.126 114 101 65.0-131 12.6 20
cis-1,2-Dichloroethene 0.125 0.137 0.114 110 91.2 73.0-125 18.3 20
trans-1,2-Dichloroethene 0.125 0.141 0.126 113 101 71.0-125 11.2 20
1,2-Dichloropropane 0.125 0.143 0.117 114 93.6 74.0-125 20.0 20
1,1-Dichloropropene 0.125 0.136 0.121 109 96.8 73.0-125 11.7 20
1,3-Dichloropropane 0.125 0.140 0.120 112 96.0 80.0-125 15.4 20
cis-1,3-Dichloropropene 0.125 0.145 0.123 116 98.4 76.0-127 16.4 20
trans-1,3-Dichloropropene 0.125 0.140 0.111 112 88.8 73.0-127 J3 23.1 20
2,2-Dichloropropane 0.125 0.143 0.130 114 104 59.0-135 9.52 20
Di-isopropyl ether 0.125 0.131 0.112 105 89.6 60.0-136 15.6 20
Ethylbenzene 0.125 0.148 0.125 118 100 74.0-126 16.8 20
Hexachloro-1,3-butadiene 0.125 0.131 0.117 105 93.6 57.0-150 11.3 20
Isopropylbenzene 0.125 0.129 0.109 103 87.2 72.0-127 16.8 20
p-Isopropyltoluene 0.125 0.134 0.116 107 92.8 72.0-133 14.4 20
2-Butanone (MEK)0.625 0.574 0.361 91.8 57.8 30.0-160 J3 45.6 24
Methylene Chloride 0.125 0.135 0.118 108 94.4 68.0-123 13.4 20
4-Methyl-2-pentanone (MIBK) 0.625 0.671 0.510 107 81.6 56.0-143 J3 27.3 20
Methyl tert-butyl ether 0.125 0.144 0.119 115 95.2 66.0-132 19.0 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004751
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-02,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3890654-1 02/12/23 09:44 • (LCSD) R3890654-2 02/12/23 10:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0905 0.0767 72.4 61.4 59.0-130 16.5 20
n-Propylbenzene 0.125 0.142 0.118 114 94.4 74.0-126 18.5 20
Styrene 0.125 0.122 0.0973 97.6 77.8 72.0-127 J3 22.5 20
1,1,1,2-Tetrachloroethane 0.125 0.152 0.130 122 104 74.0-129 15.6 20
1,1,2,2-Tetrachloroethane 0.125 0.151 0.121 121 96.8 68.0-128 J3 22.1 20
1,1,2-Trichlorotrifluoroethane 0.125 0.120 0.123 96.0 98.4 61.0-139 2.47 20
Tetrachloroethene 0.125 0.143 0.119 114 95.2 70.0-136 18.3 20
Toluene 0.125 0.139 0.115 111 92.0 75.0-121 18.9 20
1,2,3-Trichlorobenzene 0.125 0.109 0.0989 87.2 79.1 59.0-139 9.72 20
1,2,4-Trichlorobenzene 0.125 0.123 0.109 98.4 87.2 62.0-137 12.1 20
1,1,1-Trichloroethane 0.125 0.146 0.132 117 106 69.0-126 10.1 20
1,1,2-Trichloroethane 0.125 0.150 0.120 120 96.0 78.0-123 J3 22.2 20
Trichloroethene 0.125 0.146 0.120 117 96.0 76.0-126 19.5 20
Trichlorofluoromethane 0.125 0.107 0.101 85.6 80.8 61.0-142 5.77 20
1,2,3-Trichloropropane 0.125 0.162 0.126 130 101 67.0-129 J4 J3 25.0 20
1,2,4-Trimethylbenzene 0.125 0.136 0.114 109 91.2 70.0-126 17.6 20
1,2,3-Trimethylbenzene 0.125 0.134 0.116 107 92.8 74.0-124 14.4 20
1,3,5-Trimethylbenzene 0.125 0.127 0.109 102 87.2 73.0-127 15.3 20
Vinyl chloride 0.125 0.125 0.125 100 100 63.0-134 0.000 20
Xylenes, Total 0.375 0.421 0.351 112 93.6 72.0-127 18.1 20
(S) Toluene-d8 105 103 75.0-131
(S) 4-Bromofluorobenzene 90.8 90.9 67.0-138
(S) 1,2-Dichloroethane-d4 89.9 91.1 70.0-130
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/12/23 12:16 • (MS) R3890654-4 02/12/23 18:29 • (MSD) R3890654-5 02/12/23 18:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.593 ND 0.195 0.196 32.9 33.0 1 10.0-160 0.539 40
Acrylonitrile 0.593 ND 0.407 0.369 68.6 62.2 1 10.0-160 9.78 40
Benzene 0.119 ND 0.124 0.126 104 106 1 10.0-149 1.68 37
Bromobenzene 0.119 ND 0.133 0.147 112 124 1 10.0-156 10.5 38
Bromodichloromethane 0.119 ND 0.109 0.118 91.2 99.1 1 10.0-143 8.37 37
Bromoform 0.119 ND 0.118 0.123 99.1 104 1 10.0-146 4.37 36
Bromomethane 0.119 ND 0.0805 0.0848 67.6 71.2 1 10.0-149 5.23 38
n-Butylbenzene 0.119 ND 0.100 0.109 84.0 91.2 1 10.0-160 8.19 40
sec-Butylbenzene 0.119 ND 0.113 0.125 94.7 105 1 10.0-159 10.6 39
tert-Butylbenzene 0.119 ND 0.116 0.127 97.3 107 1 10.0-156 9.52 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004751
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-02,04
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/12/23 12:16 • (MS) R3890654-4 02/12/23 18:29 • (MSD) R3890654-5 02/12/23 18:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.119 ND 0.130 0.152 109 127 1 10.0-145 15.7 37
Chlorobenzene 0.119 ND 0.125 0.138 105 116 1 10.0-152 9.60 39
Chlorodibromomethane 0.119 ND 0.121 0.133 102 112 1 10.0-146 9.13 37
Chloroethane 0.119 ND 0.0512 0.0514 43.0 43.2 1 10.0-146 0.411 40
Chloroform 0.119 ND 0.107 0.112 90.3 93.8 1 10.0-146 3.85 37
Chloromethane 0.119 ND 0.117 0.120 98.2 101 1 10.0-159 2.67 37
2-Chlorotoluene 0.119 ND 0.125 0.137 105 115 1 10.0-159 8.84 38
4-Chlorotoluene 0.119 ND 0.116 0.127 97.3 107 1 10.0-155 9.52 39
1,2-Dibromo-3-Chloropropane 0.119 ND 0.0917 0.0945 77.0 79.4 1 10.0-151 3.06 39
1,2-Dibromoethane 0.119 ND 0.117 0.123 98.2 104 1 10.0-148 5.26 34
Dibromomethane 0.119 ND 0.0924 0.0931 77.6 78.2 1 10.0-147 0.795 35
1,2-Dichlorobenzene 0.119 ND 0.110 0.121 92.0 102 1 10.0-155 10.0 37
1,3-Dichlorobenzene 0.119 ND 0.121 0.130 102 109 1 10.0-153 6.72 38
1,4-Dichlorobenzene 0.119 ND 0.105 0.130 88.5 109 1 10.0-151 20.6 38
Dichlorodifluoromethane 0.119 ND 0.129 0.140 108 118 1 10.0-160 8.63 35
1,1-Dichloroethane 0.119 ND 0.115 0.120 96.5 101 1 10.0-147 4.48 37
1,2-Dichloroethane 0.119 ND 0.0813 0.0966 68.3 81.2 1 10.0-148 17.2 35
1,1-Dichloroethene 0.119 ND 0.141 0.147 119 124 1 10.0-155 4.38 37
cis-1,2-Dichloroethene 0.119 ND 0.106 0.113 89.4 94.7 1 10.0-149 5.77 37
trans-1,2-Dichloroethene 0.119 ND 0.127 0.131 107 110 1 10.0-150 2.45 37
1,2-Dichloropropane 0.119 ND 0.107 0.123 90.3 104 1 10.0-148 13.7 37
1,1-Dichloropropene 0.119 ND 0.129 0.139 108 117 1 10.0-153 7.87 35
1,3-Dichloropropane 0.119 ND 0.120 0.133 101 112 1 10.0-154 10.0 35
cis-1,3-Dichloropropene 0.119 ND 0.122 0.129 103 108 1 10.0-151 5.04 37
trans-1,3-Dichloropropene 0.119 ND 0.110 0.122 92.0 103 1 10.0-148 10.9 37
2,2-Dichloropropane 0.119 ND 0.0811 0.0937 68.1 78.7 1 10.0-138 14.3 36
Di-isopropyl ether 0.119 ND 0.0974 0.104 81.9 87.0 1 10.0-147 6.08 36
Ethylbenzene 0.119 ND 0.125 0.137 105 115 1 10.0-160 8.84 38
Hexachloro-1,3-butadiene 0.119 ND 0.0982 0.117 82.5 98.2 1 10.0-160 17.4 40
Isopropylbenzene 0.119 ND 0.104 0.115 87.7 96.5 1 10.0-155 9.51 38
p-Isopropyltoluene 0.119 ND 0.111 0.120 92.9 101 1 10.0-160 8.22 40
2-Butanone (MEK)0.593 ND 0.252 0.260 0.000 0.000 1 10.0-160 0.000 40
Methylene Chloride 0.119 ND 0.121 0.124 102 104 1 10.0-141 2.58 37
4-Methyl-2-pentanone (MIBK) 0.593 ND 0.391 0.466 65.9 78.5 1 10.0-160 17.5 35
Methyl tert-butyl ether 0.119 ND 0.0925 0.0972 77.7 81.7 1 11.0-147 5.00 35
Naphthalene 0.119 ND 0.0728 0.0796 61.2 66.9 1 10.0-160 8.98 36
n-Propylbenzene 0.119 ND 0.123 0.135 104 113 1 10.0-158 8.98 38
Styrene 0.119 ND 0.100 0.111 84.1 92.9 1 10.0-160 10.0 40
1,1,1,2-Tetrachloroethane 0.119 ND 0.113 0.125 94.7 105 1 10.0-149 10.6 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004751
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-02,04
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/12/23 12:16 • (MS) R3890654-4 02/12/23 18:29 • (MSD) R3890654-5 02/12/23 18:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.119 ND 0.0967 0.0986 81.2 82.8 1 10.0-160 1.94 35
1,1,2-Trichlorotrifluoroethane 0.119 ND 0.141 0.142 119 119 1 10.0-160 0.743 36
Tetrachloroethene 0.119 ND 0.135 0.147 113 124 1 10.0-156 8.96 39
Toluene 0.119 ND 0.124 0.134 104 112 1 10.0-156 7.35 38
1,2,3-Trichlorobenzene 0.119 ND 0.0734 0.0937 61.7 78.7 1 10.0-160 24.2 40
1,2,4-Trichlorobenzene 0.119 ND 0.0920 0.109 77.3 91.2 1 10.0-160 16.5 40
1,1,1-Trichloroethane 0.119 ND 0.132 0.139 111 117 1 10.0-144 5.45 35
1,1,2-Trichloroethane 0.119 ND 0.122 0.124 103 104 1 10.0-160 1.71 35
Trichloroethene 0.119 ND 0.141 0.160 119 135 1 10.0-156 12.6 38
Trichlorofluoromethane 0.119 ND 0.0557 0.0602 46.8 50.5 1 10.0-160 7.64 40
1,2,3-Trichloropropane 0.119 ND 0.118 0.131 99.1 110 1 10.0-156 10.2 35
1,2,4-Trimethylbenzene 0.119 ND 0.106 0.120 89.4 101 1 10.0-160 12.1 36
1,2,3-Trimethylbenzene 0.119 ND 0.0976 0.111 81.9 92.9 1 10.0-160 12.6 36
1,3,5-Trimethylbenzene 0.119 ND 0.106 0.117 89.4 98.2 1 10.0-160 9.43 38
Vinyl chloride 0.119 ND 0.133 0.136 112 114 1 10.0-160 2.35 37
Xylenes, Total 0.355 ND 0.339 0.373 95.5 105 1 10.0-160 9.47 38
(S) Toluene-d8 109 111 75.0-131
(S) 4-Bromofluorobenzene 89.4 91.8 67.0-138
(S) 1,2-Dichloroethane-d4 77.8 77.8 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004844
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-01
Method Blank (MB)
(MB) R3891594-2 02/12/23 21:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004844
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-01
Method Blank (MB)
(MB) R3891594-2 02/12/23 21:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00107 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 119 75.0-131
(S) 4-Bromofluorobenzene 94.0 67.0-138
(S) 1,2-Dichloroethane-d4 93.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3891594-1 02/12/23 20:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.319 51.0 10.0-160
Acrylonitrile 0.625 0.528 84.5 45.0-153
Benzene 0.125 0.109 87.2 70.0-123
Bromobenzene 0.125 0.129 103 73.0-121
Bromodichloromethane 0.125 0.109 87.2 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004844
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-01
Laboratory Control Sample (LCS)
(LCS) R3891594-1 02/12/23 20:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.108 86.4 64.0-132
Bromomethane 0.125 0.0932 74.6 56.0-147
n-Butylbenzene 0.125 0.0927 74.2 68.0-135
sec-Butylbenzene 0.125 0.106 84.8 74.0-130
tert-Butylbenzene 0.125 0.112 89.6 75.0-127
Carbon tetrachloride 0.125 0.111 88.8 66.0-128
Chlorobenzene 0.125 0.123 98.4 76.0-128
Chlorodibromomethane 0.125 0.127 102 74.0-127
Chloroethane 0.125 0.117 93.6 61.0-134
Chloroform 0.125 0.104 83.2 72.0-123
Chloromethane 0.125 0.119 95.2 51.0-138
2-Chlorotoluene 0.125 0.129 103 75.0-124
4-Chlorotoluene 0.125 0.117 93.6 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.0963 77.0 59.0-130
1,2-Dibromoethane 0.125 0.123 98.4 74.0-128
Dibromomethane 0.125 0.104 83.2 75.0-122
1,2-Dichlorobenzene 0.125 0.104 83.2 76.0-124
1,3-Dichlorobenzene 0.125 0.115 92.0 76.0-125
1,4-Dichlorobenzene 0.125 0.104 83.2 77.0-121
Dichlorodifluoromethane 0.125 0.0996 79.7 43.0-156
1,1-Dichloroethane 0.125 0.119 95.2 70.0-127
1,2-Dichloroethane 0.125 0.103 82.4 65.0-131
1,1-Dichloroethene 0.125 0.121 96.8 65.0-131
cis-1,2-Dichloroethene 0.125 0.107 85.6 73.0-125
trans-1,2-Dichloroethene 0.125 0.105 84.0 71.0-125
1,2-Dichloropropane 0.125 0.124 99.2 74.0-125
1,1-Dichloropropene 0.125 0.115 92.0 73.0-125
1,3-Dichloropropane 0.125 0.132 106 80.0-125
cis-1,3-Dichloropropene 0.125 0.118 94.4 76.0-127
trans-1,3-Dichloropropene 0.125 0.134 107 73.0-127
2,2-Dichloropropane 0.125 0.104 83.2 59.0-135
Di-isopropyl ether 0.125 0.122 97.6 60.0-136
Ethylbenzene 0.125 0.112 89.6 74.0-126
Hexachloro-1,3-butadiene 0.125 0.0867 69.4 57.0-150
Isopropylbenzene 0.125 0.105 84.0 72.0-127
p-Isopropyltoluene 0.125 0.101 80.8 72.0-133
2-Butanone (MEK)0.625 0.548 87.7 30.0-160
Methylene Chloride 0.125 0.104 83.2 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.738 118 56.0-143
Methyl tert-butyl ether 0.125 0.0931 74.5 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004844
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-01
Laboratory Control Sample (LCS)
(LCS) R3891594-1 02/12/23 20:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.0764 61.1 59.0-130
n-Propylbenzene 0.125 0.120 96.0 74.0-126
Styrene 0.125 0.113 90.4 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.126 101 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.119 95.2 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.120 96.0 61.0-139
Tetrachloroethene 0.125 0.134 107 70.0-136
Toluene 0.125 0.131 105 75.0-121
1,2,3-Trichlorobenzene 0.125 0.0768 61.4 59.0-139
1,2,4-Trichlorobenzene 0.125 0.0778 62.2 62.0-137
1,1,1-Trichloroethane 0.125 0.101 80.8 69.0-126
1,1,2-Trichloroethane 0.125 0.109 87.2 78.0-123
Trichloroethene 0.125 0.123 98.4 76.0-126
Trichlorofluoromethane 0.125 0.108 86.4 61.0-142
1,2,3-Trichloropropane 0.125 0.128 102 67.0-129
1,2,4-Trimethylbenzene 0.125 0.105 84.0 70.0-126
1,2,3-Trimethylbenzene 0.125 0.105 84.0 74.0-124
1,3,5-Trimethylbenzene 0.125 0.115 92.0 73.0-127
Vinyl chloride 0.125 0.112 89.6 63.0-134
Xylenes, Total 0.375 0.339 90.4 72.0-127
(S) Toluene-d8 121 75.0-131
(S) 4-Bromofluorobenzene 94.1 67.0-138
(S) 1,2-Dichloroethane-d4 94.9 70.0-130
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/13/23 00:17 • (MS) R3891594-3 02/13/23 05:02 • (MSD) R3891594-4 02/13/23 05:20
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 1.01 ND 1.60 0.539 159 53.6 1 10.0-160 J3 99.1 40
Acrylonitrile 1.01 ND 1.27 1.01 126 100 1 10.0-160 23.2 40
Benzene 0.201 ND 0.200 0.207 99.1 103 1 10.0-149 3.45 37
Bromobenzene 0.201 ND 0.191 0.231 94.8 115 1 10.0-156 19.1 38
Bromodichloromethane 0.201 ND 0.184 0.187 91.3 93.0 1 10.0-143 1.89 37
Bromoform 0.201 ND 0.198 0.191 98.3 94.8 1 10.0-146 3.60 36
Bromomethane 0.201 ND 0.123 0.119 61.0 59.2 1 10.0-149 2.89 38
n-Butylbenzene 0.201 ND 0.179 0.198 88.7 98.3 1 10.0-160 10.2 40
sec-Butylbenzene 0.201 ND 0.175 0.226 87.0 112 1 10.0-159 25.3 39
tert-Butylbenzene 0.201 ND 0.173 0.219 86.1 109 1 10.0-156 23.2 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004844
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-01
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/13/23 00:17 • (MS) R3891594-3 02/13/23 05:02 • (MSD) R3891594-4 02/13/23 05:20
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.201 ND 0.207 0.229 103 114 1 10.0-145 10.4 37
Chlorobenzene 0.201 ND 0.207 0.214 103 106 1 10.0-152 3.33 39
Chlorodibromomethane 0.201 ND 0.207 0.219 103 109 1 10.0-146 5.76 37
Chloroethane 0.201 ND 0.151 0.156 74.8 77.3 1 10.0-146 3.32 40
Chloroform 0.201 ND 0.186 0.191 92.2 94.8 1 10.0-146 2.79 37
Chloromethane 0.201 ND 0.200 0.212 99.1 105 1 10.0-159 5.96 37
2-Chlorotoluene 0.201 ND 0.200 0.236 99.1 117 1 10.0-159 16.9 38
4-Chlorotoluene 0.201 ND 0.184 0.222 91.3 110 1 10.0-155 19.0 39
1,2-Dibromo-3-Chloropropane 0.201 ND 0.162 0.189 80.5 93.9 1 10.0-151 15.4 39
1,2-Dibromoethane 0.201 ND 0.210 0.221 104 110 1 10.0-148 4.88 34
Dibromomethane 0.201 ND 0.184 0.189 91.3 93.9 1 10.0-147 2.82 35
1,2-Dichlorobenzene 0.201 ND 0.191 0.196 94.8 97.4 1 10.0-155 2.71 37
1,3-Dichlorobenzene 0.201 ND 0.187 0.198 93.0 98.3 1 10.0-153 5.45 38
1,4-Dichlorobenzene 0.201 ND 0.182 0.193 90.4 95.7 1 10.0-151 5.61 38
Dichlorodifluoromethane 0.201 ND 0.210 0.207 104 103 1 10.0-160 1.68 35
1,1-Dichloroethane 0.201 ND 0.210 0.219 104 109 1 10.0-147 4.08 37
1,2-Dichloroethane 0.201 ND 0.182 0.184 90.4 91.3 1 10.0-148 0.957 35
1,1-Dichloroethene 0.201 ND 0.222 0.238 110 118 1 10.0-155 6.84 37
cis-1,2-Dichloroethene 0.201 ND 0.187 0.193 93.0 95.7 1 10.0-149 2.76 37
trans-1,2-Dichloroethene 0.201 ND 0.191 0.198 94.8 98.3 1 10.0-150 3.60 37
1,2-Dichloropropane 0.201 ND 0.224 0.235 111 117 1 10.0-148 4.58 37
1,1-Dichloropropene 0.201 ND 0.207 0.224 103 111 1 10.0-153 8.13 35
1,3-Dichloropropane 0.201 ND 0.226 0.238 112 118 1 10.0-154 5.28 35
cis-1,3-Dichloropropene 0.201 ND 0.205 0.215 102 107 1 10.0-151 5.00 37
trans-1,3-Dichloropropene 0.201 ND 0.219 0.238 109 118 1 10.0-148 8.43 37
2,2-Dichloropropane 0.201 ND 0.174 0.184 86.3 91.3 1 10.0-138 5.58 36
Di-isopropyl ether 0.201 ND 0.231 0.243 115 121 1 10.0-147 5.17 36
Ethylbenzene 0.201 ND 0.207 0.217 103 108 1 10.0-160 4.96 38
Hexachloro-1,3-butadiene 0.201 ND 0.198 0.193 98.3 95.7 1 10.0-160 2.69 40
Isopropylbenzene 0.201 ND 0.203 0.210 101 104 1 10.0-155 3.39 38
p-Isopropyltoluene 0.201 ND 0.168 0.214 83.3 106 1 10.0-160 24.1 40
2-Butanone (MEK)1.01 ND 1.22 0.986 121 97.9 1 10.0-160 21.1 40
Methylene Chloride 0.201 ND 0.177 0.193 87.8 95.7 1 10.0-141 8.53 37
4-Methyl-2-pentanone (MIBK) 1.01 ND 1.32 1.26 131 125 1 10.0-160 4.88 35
Methyl tert-butyl ether 0.201 ND 0.166 0.177 82.4 87.8 1 11.0-147 6.33 35
Naphthalene 0.201 ND 0.153 0.187 76.2 93.0 1 10.0-160 19.9 36
n-Propylbenzene 0.201 ND 0.191 0.236 94.8 117 1 10.0-158 21.3 38
Styrene 0.201 ND 0.210 0.215 104 107 1 10.0-160 2.47 40
1,1,1,2-Tetrachloroethane 0.201 ND 0.205 0.222 102 110 1 10.0-149 8.20 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004844
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-01
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/13/23 00:17 • (MS) R3891594-3 02/13/23 05:02 • (MSD) R3891594-4 02/13/23 05:20
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.201 ND 0.164 0.226 81.4 112 1 10.0-160 31.8 35
1,1,2-Trichlorotrifluoroethane 0.201 ND 0.235 0.249 117 123 1 10.0-160 5.80 36
Tetrachloroethene 0.201 ND 0.233 0.247 116 123 1 10.0-156 5.84 39
Toluene 0.201 0.0141 0.238 0.252 111 118 1 10.0-156 5.71 38
1,2,3-Trichlorobenzene 0.201 ND 0.153 0.200 75.8 99.1 1 10.0-160 26.6 40
1,2,4-Trichlorobenzene 0.201 ND 0.180 0.180 89.6 89.6 1 10.0-160 0.000 40
1,1,1-Trichloroethane 0.201 ND 0.194 0.205 96.5 102 1 10.0-144 5.26 35
1,1,2-Trichloroethane 0.201 ND 0.229 0.238 114 118 1 10.0-160 3.75 35
Trichloroethene 0.201 ND 0.219 0.212 109 105 1 10.0-156 3.25 38
Trichlorofluoromethane 0.201 ND 0.189 0.201 93.9 100 1 10.0-160 6.28 40
1,2,3-Trichloropropane 0.201 ND 0.191 0.217 94.8 108 1 10.0-156 12.9 35
1,2,4-Trimethylbenzene 0.201 ND 0.173 0.205 83.4 99.1 1 10.0-160 16.8 36
1,2,3-Trimethylbenzene 0.201 ND 0.172 0.205 83.3 99.7 1 10.0-160 17.6 36
1,3,5-Trimethylbenzene 0.201 ND 0.182 0.233 88.5 114 1 10.0-160 24.5 38
Vinyl chloride 0.201 ND 0.113 0.163 56.1 81.0 1 10.0-160 36.3 37
Xylenes, Total 0.604 ND 0.634 0.653 104 107 1 10.0-160 2.99 38
(S) Toluene-d8 114 117 75.0-131
(S) 4-Bromofluorobenzene 104 96.4 67.0-138
(S) 1,2-Dichloroethane-d4 96.4 95.7 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2006549
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-03
Method Blank (MB)
(MB) R3891891-3 02/16/23 20:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2006549
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-03
Method Blank (MB)
(MB) R3891891-3 02/16/23 20:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00115 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 101 75.0-131
(S) 4-Bromofluorobenzene 103 67.0-138
(S) 1,2-Dichloroethane-d4 88.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3891891-1 02/16/23 19:40 • (LCSD) R3891891-2 02/16/23 19:59
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.436 0.357 69.8 57.1 10.0-160 19.9 31
Acrylonitrile 0.625 0.480 0.528 76.8 84.5 45.0-153 9.52 22
Benzene 0.125 0.127 0.131 102 105 70.0-123 3.10 20
Bromobenzene 0.125 0.125 0.123 100 98.4 73.0-121 1.61 20
Bromodichloromethane 0.125 0.134 0.136 107 109 73.0-121 1.48 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2006549
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3891891-1 02/16/23 19:40 • (LCSD) R3891891-2 02/16/23 19:59
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.140 0.149 112 119 64.0-132 6.23 20
Bromomethane 0.125 0.124 0.131 99.2 105 56.0-147 5.49 20
n-Butylbenzene 0.125 0.108 0.112 86.4 89.6 68.0-135 3.64 20
sec-Butylbenzene 0.125 0.113 0.116 90.4 92.8 74.0-130 2.62 20
tert-Butylbenzene 0.125 0.111 0.113 88.8 90.4 75.0-127 1.79 20
Carbon tetrachloride 0.125 0.138 0.144 110 115 66.0-128 4.26 20
Chlorobenzene 0.125 0.126 0.128 101 102 76.0-128 1.57 20
Chlorodibromomethane 0.125 0.128 0.133 102 106 74.0-127 3.83 20
Chloroethane 0.125 0.113 0.115 90.4 92.0 61.0-134 1.75 20
Chloroform 0.125 0.128 0.130 102 104 72.0-123 1.55 20
Chloromethane 0.125 0.108 0.120 86.4 96.0 51.0-138 10.5 20
2-Chlorotoluene 0.125 0.115 0.115 92.0 92.0 75.0-124 0.000 20
4-Chlorotoluene 0.125 0.114 0.113 91.2 90.4 75.0-124 0.881 20
1,2-Dibromo-3-Chloropropane 0.125 0.121 0.121 96.8 96.8 59.0-130 0.000 20
1,2-Dibromoethane 0.125 0.132 0.131 106 105 74.0-128 0.760 20
Dibromomethane 0.125 0.134 0.132 107 106 75.0-122 1.50 20
1,2-Dichlorobenzene 0.125 0.130 0.126 104 101 76.0-124 3.12 20
1,3-Dichlorobenzene 0.125 0.123 0.126 98.4 101 76.0-125 2.41 20
1,4-Dichlorobenzene 0.125 0.123 0.120 98.4 96.0 77.0-121 2.47 20
Dichlorodifluoromethane 0.125 0.292 0.281 234 225 43.0-156 J4 J4 3.84 20
1,1-Dichloroethane 0.125 0.118 0.122 94.4 97.6 70.0-127 3.33 20
1,2-Dichloroethane 0.125 0.114 0.118 91.2 94.4 65.0-131 3.45 20
1,1-Dichloroethene 0.125 0.121 0.124 96.8 99.2 65.0-131 2.45 20
cis-1,2-Dichloroethene 0.125 0.121 0.128 96.8 102 73.0-125 5.62 20
trans-1,2-Dichloroethene 0.125 0.131 0.137 105 110 71.0-125 4.48 20
1,2-Dichloropropane 0.125 0.122 0.122 97.6 97.6 74.0-125 0.000 20
1,1-Dichloropropene 0.125 0.127 0.130 102 104 73.0-125 2.33 20
1,3-Dichloropropane 0.125 0.125 0.122 100 97.6 80.0-125 2.43 20
cis-1,3-Dichloropropene 0.125 0.136 0.138 109 110 76.0-127 1.46 20
trans-1,3-Dichloropropene 0.125 0.123 0.128 98.4 102 73.0-127 3.98 20
2,2-Dichloropropane 0.125 0.134 0.141 107 113 59.0-135 5.09 20
Di-isopropyl ether 0.125 0.111 0.112 88.8 89.6 60.0-136 0.897 20
Ethylbenzene 0.125 0.124 0.123 99.2 98.4 74.0-126 0.810 20
Hexachloro-1,3-butadiene 0.125 0.119 0.131 95.2 105 57.0-150 9.60 20
Isopropylbenzene 0.125 0.127 0.133 102 106 72.0-127 4.62 20
p-Isopropyltoluene 0.125 0.116 0.119 92.8 95.2 72.0-133 2.55 20
2-Butanone (MEK)0.625 0.514 0.498 82.2 79.7 30.0-160 3.16 24
Methylene Chloride 0.125 0.131 0.127 105 102 68.0-123 3.10 20
4-Methyl-2-pentanone (MIBK) 0.625 0.584 0.576 93.4 92.2 56.0-143 1.38 20
Methyl tert-butyl ether 0.125 0.130 0.139 104 111 66.0-132 6.69 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2006549
Volatile Organic Compounds (GC/MS) by Method 8260B L1584351-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3891891-1 02/16/23 19:40 • (LCSD) R3891891-2 02/16/23 19:59
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.109 0.118 87.2 94.4 59.0-130 7.93 20
n-Propylbenzene 0.125 0.110 0.111 88.0 88.8 74.0-126 0.905 20
Styrene 0.125 0.133 0.136 106 109 72.0-127 2.23 20
1,1,1,2-Tetrachloroethane 0.125 0.129 0.133 103 106 74.0-129 3.05 20
1,1,2,2-Tetrachloroethane 0.125 0.105 0.100 84.0 80.0 68.0-128 4.88 20
1,1,2-Trichlorotrifluoroethane 0.125 0.129 0.135 103 108 61.0-139 4.55 20
Tetrachloroethene 0.125 0.138 0.145 110 116 70.0-136 4.95 20
Toluene 0.125 0.120 0.125 96.0 100 75.0-121 4.08 20
1,2,3-Trichlorobenzene 0.125 0.120 0.131 96.0 105 59.0-139 8.76 20
1,2,4-Trichlorobenzene 0.125 0.144 0.143 115 114 62.0-137 0.697 20
1,1,1-Trichloroethane 0.125 0.138 0.145 110 116 69.0-126 4.95 20
1,1,2-Trichloroethane 0.125 0.127 0.127 102 102 78.0-123 0.000 20
Trichloroethene 0.125 0.147 0.149 118 119 76.0-126 1.35 20
Trichlorofluoromethane 0.125 0.113 0.122 90.4 97.6 61.0-142 7.66 20
1,2,3-Trichloropropane 0.125 0.118 0.111 94.4 88.8 67.0-129 6.11 20
1,2,4-Trimethylbenzene 0.125 0.115 0.114 92.0 91.2 70.0-126 0.873 20
1,2,3-Trimethylbenzene 0.125 0.115 0.117 92.0 93.6 74.0-124 1.72 20
1,3,5-Trimethylbenzene 0.125 0.113 0.116 90.4 92.8 73.0-127 2.62 20
Vinyl chloride 0.125 0.135 0.136 108 109 63.0-134 0.738 20
Xylenes, Total 0.375 0.370 0.390 98.7 104 72.0-127 5.26 20
(S) Toluene-d8 96.5 97.8 75.0-131
(S) 4-Bromofluorobenzene 105 106 67.0-138
(S) 1,2-Dichloroethane-d4 93.5 96.3 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2005423
Semi-Volatile Organic Compounds (GC) by Method 8015 L1584351-01,02
Method Blank (MB)
(MB) R3891446-2 02/15/23 23:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range 0.375 J 0.274 4.00
(S) o-Terphenyl 64.9 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3891446-1 02/15/23 23:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 33.2 66.4 50.0-150
(S) o-Terphenyl 65.3 18.0-148
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/16/23 10:04 • (MS) R3891548-1 02/16/23 10:16 • (MSD) R3891548-2 02/16/23 10:29
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 66.5 ND 189 239 284 356 10 50.0-150 J5 J3 J5 23.5 20
(S) o-Terphenyl 58.9 63.1 18.0-148
Sample Narrative:
OS: Dilution due to matrix impact during extract concentration procedure
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2005842
Semi-Volatile Organic Compounds (GC) by Method 8015 L1584351-03,04
Method Blank (MB)
(MB) R3890921-2 02/14/23 23:46
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 74.8 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3890921-1 02/14/23 23:15
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 38.8 77.6 50.0-150
(S) o-Terphenyl 87.8 18.0-148
L1585248-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1585248-01 02/15/23 11:47 • (MS) R3891134-1 02/15/23 12:01 • (MSD) R3891134-2 02/15/23 12:15
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 54.0 598 351 555 0.000 0.000 10 50.0-150 V J3 V 45.0 20
(S) o-Terphenyl 94.8 90.8 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004450
Polychlorinated Biphenyls (GC) by Method 8082 L1584351-01,02,03,04
Method Blank (MB)
(MB) R3891660-1 02/15/23 21:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 56.2 10.0-135
(S) Tetrachloro-m-xylene 70.4 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3891660-2 02/15/23 21:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0887 53.1 36.0-141
PCB 1260 0.167 0.0795 47.6 37.0-145
(S) Decachlorobiphenyl 64.6 10.0-135
(S) Tetrachloro-m-xylene 83.9 10.0-139
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/16/23 20:27 • (MS) R3892153-1 02/16/23 20:36 • (MSD) R3892153-2 02/16/23 20:45
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.227 ND ND ND 0.000 0.000 10 10.0-160 J6 J6 0.000 37
PCB 1260 0.227 ND ND ND 0.000 0.000 10 10.0-160 J6 J6 0.000 38
(S) Decachlorobiphenyl 0.435 35.3 10.0-135 J2
(S) Tetrachloro-m-xylene 27.6 55.7 10.0-139
Sample Narrative:
OS: IS/SURR failed on lower dilution.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-02,03,04
Method Blank (MB)
(MB) R3890035-2 02/11/23 22:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-02,03,04
Method Blank (MB)
(MB) R3890035-2 02/11/23 22:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 57.4 10.0-122
(S) 2-Fluorobiphenyl 67.6 15.0-120
(S) p-Terphenyl-d14 77.5 10.0-120
(S) Phenol-d5 55.7 10.0-120
(S) 2-Fluorophenol 62.3 12.0-120
(S) 2,4,6-Tribromophenol 50.0 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3890035-1 02/11/23 21:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.550 82.6 38.0-120
Acenaphthylene 0.666 0.592 88.9 40.0-120
Anthracene 0.666 0.605 90.8 42.0-120
Benzidine 1.33 0.356 26.8 10.0-120
Benzo(a)anthracene 0.666 0.703 106 44.0-120
Benzo(b)fluoranthene 0.666 0.685 103 43.0-120
Benzo(k)fluoranthene 0.666 0.627 94.1 44.0-120
Benzo(g,h,i)perylene 0.666 0.717 108 43.0-120
Benzo(a)pyrene 0.666 0.717 108 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.393 59.0 20.0-120
Bis(2-chloroethyl)ether 0.666 0.493 74.0 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.468 70.3 23.0-120
4-Bromophenyl-phenylether 0.666 0.652 97.9 40.0-120
2-Chloronaphthalene 0.666 0.535 80.3 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3890035-1 02/11/23 21:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.630 94.6 40.0-120
Chrysene 0.666 0.647 97.1 43.0-120
Dibenz(a,h)anthracene 0.666 0.705 106 44.0-120
3,3-Dichlorobenzidine 1.33 1.21 91.0 28.0-120
2,4-Dinitrotoluene 0.666 0.654 98.2 45.0-120
2,6-Dinitrotoluene 0.666 0.636 95.5 42.0-120
Fluoranthene 0.666 0.675 101 44.0-120
Fluorene 0.666 0.590 88.6 41.0-120
Hexachlorobenzene 0.666 0.651 97.7 39.0-120
Hexachloro-1,3-butadiene 0.666 0.498 74.8 15.0-120
Hexachlorocyclopentadiene 0.666 0.575 86.3 15.0-120
Hexachloroethane 0.666 0.423 63.5 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.689 103 45.0-120
Isophorone 0.666 0.414 62.2 23.0-120
Naphthalene 0.666 0.407 61.1 18.0-120
Nitrobenzene 0.666 0.394 59.2 17.0-120
n-Nitrosodimethylamine 0.666 0.370 55.6 10.0-125
n-Nitrosodiphenylamine 0.666 0.582 87.4 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.453 68.0 26.0-120
Phenanthrene 0.666 0.590 88.6 42.0-120
Benzylbutyl phthalate 0.666 0.614 92.2 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.604 90.7 41.0-120
Di-n-butyl phthalate 0.666 0.586 88.0 43.0-120
Diethyl phthalate 0.666 0.632 94.9 43.0-120
Dimethyl phthalate 0.666 0.630 94.6 43.0-120
Di-n-octyl phthalate 0.666 0.588 88.3 40.0-120
Pyrene 0.666 0.660 99.1 41.0-120
1,2,4-Trichlorobenzene 0.666 0.476 71.5 17.0-120
4-Chloro-3-methylphenol 0.666 0.484 72.7 28.0-120
2-Chlorophenol 0.666 0.507 76.1 28.0-120
2,4-Dichlorophenol 0.666 0.487 73.1 25.0-120
2,4-Dimethylphenol 0.666 0.448 67.3 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.533 80.0 16.0-120
2,4-Dinitrophenol 0.666 0.344 51.7 10.0-120
2-Nitrophenol 0.666 0.475 71.3 20.0-120
4-Nitrophenol 0.666 0.601 90.2 27.0-120
Pentachlorophenol 0.666 0.489 73.4 29.0-120
Phenol 0.666 0.498 74.8 28.0-120
2,4,6-Trichlorophenol 0.666 0.659 98.9 37.0-120
(S) Nitrobenzene-d5 61.6 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3890035-1 02/11/23 21:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 86.8 15.0-120
(S) p-Terphenyl-d14 100 10.0-120
(S) Phenol-d5 74.3 10.0-120
(S) 2-Fluorophenol 84.1 12.0-120
(S) 2,4,6-Tribromophenol 106 10.0-127
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/11/23 22:39 • (MS) R3890035-3 02/11/23 23:00 • (MSD) R3890035-4 02/11/23 23:21
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.683 ND 0.415 0.359 60.8 52.6 1 18.0-120 14.6 32
Acenaphthylene 0.683 ND 0.444 0.380 65.0 55.7 1 25.0-120 15.4 32
Anthracene 0.683 ND 0.457 0.386 67.0 56.5 1 22.0-120 17.0 29
Benzidine 1.36 ND ND ND 51.4 43.7 1 10.0-120 16.3 40
Benzo(a)anthracene 0.683 ND 0.518 0.447 75.8 65.5 1 25.0-120 14.7 29
Benzo(b)fluoranthene 0.683 ND 0.492 0.414 72.1 60.7 1 19.0-122 17.2 31
Benzo(k)fluoranthene 0.683 ND 0.472 0.403 69.1 59.0 1 23.0-120 15.7 30
Benzo(g,h,i)perylene 0.683 ND 0.532 0.449 77.9 65.8 1 10.0-120 16.9 33
Benzo(a)pyrene 0.683 ND 0.540 0.458 79.1 67.1 1 24.0-120 16.4 30
Bis(2-chlorethoxy)methane 0.683 ND ND ND 46.5 42.2 1 10.0-120 9.81 34
Bis(2-chloroethyl)ether 0.683 ND 0.368 ND 53.9 47.1 1 10.0-120 13.4 40
2,2-Oxybis(1-Chloropropane) 0.683 ND ND ND 49.8 45.9 1 10.0-120 8.15 40
4-Bromophenyl-phenylether 0.683 ND 0.493 0.430 72.2 62.9 1 27.0-120 13.8 30
2-Chloronaphthalene 0.683 ND 0.412 0.357 60.4 52.3 1 20.0-120 14.4 32
4-Chlorophenyl-phenylether 0.683 ND 0.473 0.401 69.2 58.7 1 24.0-120 16.4 29
Chrysene 0.683 ND 0.470 0.404 68.8 59.2 1 21.0-120 15.0 29
Dibenz(a,h)anthracene 0.683 ND 0.525 0.448 76.9 65.6 1 10.0-120 15.8 32
3,3-Dichlorobenzidine 1.36 ND 0.938 0.840 68.8 61.6 1 10.0-120 11.1 34
2,4-Dinitrotoluene 0.683 ND 0.497 0.419 72.8 61.4 1 30.0-120 17.0 31
2,6-Dinitrotoluene 0.683 ND 0.469 0.403 68.6 59.0 1 25.0-120 15.1 31
Fluoranthene 0.683 ND 0.507 0.432 74.2 63.2 1 18.0-126 16.0 32
Fluorene 0.683 ND 0.438 0.379 64.1 55.6 1 25.0-120 14.3 30
Hexachlorobenzene 0.683 ND 0.483 0.414 70.7 60.7 1 27.0-120 15.3 28
Hexachloro-1,3-butadiene 0.683 ND 0.404 0.356 59.2 52.1 1 10.0-120 12.7 38
Hexachlorocyclopentadiene 0.683 ND 0.440 0.350 64.4 51.2 1 10.0-120 22.9 40
Hexachloroethane 0.683 ND ND ND 47.9 43.4 1 10.0-120 9.87 40
Indeno(1,2,3-cd)pyrene 0.683 ND 0.518 0.438 75.8 64.1 1 10.0-120 16.7 32
Isophorone 0.683 ND ND ND 48.2 43.4 1 13.0-120 10.5 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004454
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-02,03,04
L1584340-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584340-01 02/11/23 22:39 • (MS) R3890035-3 02/11/23 23:00 • (MSD) R3890035-4 02/11/23 23:21
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.683 ND 0.327 0.293 47.9 42.9 1 10.0-120 10.9 35
Nitrobenzene 0.683 ND ND ND 47.7 42.6 1 10.0-120 11.3 36
n-Nitrosodimethylamine 0.683 ND ND ND 40.8 34.7 1 10.0-127 16.3 40
n-Nitrosodiphenylamine 0.683 ND 0.443 0.383 64.9 56.2 1 17.0-120 14.4 29
n-Nitrosodi-n-propylamine 0.683 ND ND ND 49.1 44.4 1 10.0-120 9.95 37
Phenanthrene 0.683 ND 0.442 0.374 64.7 54.8 1 17.0-120 16.6 31
Benzylbutyl phthalate 0.683 ND 0.469 0.404 68.6 59.2 1 23.0-120 14.8 30
Bis(2-ethylhexyl)phthalate 0.683 ND 0.470 0.409 68.8 59.9 1 17.0-126 13.8 30
Di-n-butyl phthalate 0.683 ND 0.450 0.380 65.9 55.7 1 30.0-120 16.8 29
Diethyl phthalate 0.683 ND 0.477 0.406 69.8 59.5 1 26.0-120 16.0 28
Dimethyl phthalate 0.683 ND 0.467 0.403 68.3 59.0 1 25.0-120 14.6 29
Di-n-octyl phthalate 0.683 ND 0.478 0.418 70.0 61.3 1 21.0-123 13.3 29
Pyrene 0.683 ND 0.476 0.412 69.7 60.4 1 16.0-121 14.3 32
1,2,4-Trichlorobenzene 0.683 ND 0.387 0.343 56.6 50.3 1 12.0-120 11.8 37
4-Chloro-3-methylphenol 0.683 ND 0.391 0.346 57.2 50.6 1 15.0-120 12.3 30
2-Chlorophenol 0.683 ND 0.390 ND 57.1 49.7 1 15.0-120 13.8 37
2,4-Dichlorophenol 0.683 ND 0.399 0.360 58.4 52.7 1 20.0-120 10.3 31
2,4-Dimethylphenol 0.683 ND 0.377 ND 55.3 48.5 1 10.0-120 13.0 33
4,6-Dinitro-2-methylphenol 0.683 ND 0.535 0.428 78.4 62.6 1 10.0-120 22.4 39
2,4-Dinitrophenol 0.683 ND 0.494 0.395 72.4 57.8 1 10.0-121 22.4 40
2-Nitrophenol 0.683 ND 0.424 0.379 62.2 55.6 1 12.0-120 11.2 39
4-Nitrophenol 0.683 ND 0.478 0.409 70.0 59.9 1 10.0-137 15.5 32
Pentachlorophenol 0.683 ND 0.457 0.371 67.0 54.4 1 10.0-160 20.8 31
Phenol 0.683 ND 0.370 ND 54.2 48.6 1 12.0-120 10.8 38
2,4,6-Trichlorophenol 0.683 ND 0.503 0.441 73.7 64.6 1 19.0-120 13.2 32
(S) Nitrobenzene-d5 48.9 47.1 10.0-122
(S) 2-Fluorobiphenyl 64.3 58.6 15.0-120
(S) p-Terphenyl-d14 74.5 67.9 10.0-120
(S) Phenol-d5 53.9 51.7 10.0-120
(S) 2-Fluorophenol 61.4 58.4 12.0-120
(S) 2,4,6-Tribromophenol 82.7 73.6 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004703
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-01
Method Blank (MB)
(MB) R3891334-2 02/15/23 11:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004703
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-01
Method Blank (MB)
(MB) R3891334-2 02/15/23 11:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 52.9 10.0-122
(S) 2-Fluorobiphenyl 71.2 15.0-120
(S) p-Terphenyl-d14 81.1 10.0-120
(S) Phenol-d5 64.9 10.0-120
(S) 2-Fluorophenol 72.5 12.0-120
(S) 2,4,6-Tribromophenol 82.0 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3891334-1 02/15/23 10:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.443 66.5 38.0-120
Acenaphthylene 0.666 0.476 71.5 40.0-120
Anthracene 0.666 0.477 71.6 42.0-120
Benzidine 1.33 0.503 37.8 10.0-120
Benzo(a)anthracene 0.666 0.494 74.2 44.0-120
Benzo(b)fluoranthene 0.666 0.472 70.9 43.0-120
Benzo(k)fluoranthene 0.666 0.500 75.1 44.0-120
Benzo(g,h,i)perylene 0.666 0.517 77.6 43.0-120
Benzo(a)pyrene 0.666 0.523 78.5 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.361 54.2 20.0-120
Bis(2-chloroethyl)ether 0.666 0.389 58.4 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.422 63.4 23.0-120
4-Bromophenyl-phenylether 0.666 0.502 75.4 40.0-120
2-Chloronaphthalene 0.666 0.449 67.4 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004703
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-01
Laboratory Control Sample (LCS)
(LCS) R3891334-1 02/15/23 10:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.499 74.9 40.0-120
Chrysene 0.666 0.499 74.9 43.0-120
Dibenz(a,h)anthracene 0.666 0.524 78.7 44.0-120
3,3-Dichlorobenzidine 1.33 1.03 77.4 28.0-120
2,4-Dinitrotoluene 0.666 0.529 79.4 45.0-120
2,6-Dinitrotoluene 0.666 0.483 72.5 42.0-120
Fluoranthene 0.666 0.489 73.4 44.0-120
Fluorene 0.666 0.466 70.0 41.0-120
Hexachlorobenzene 0.666 0.526 79.0 39.0-120
Hexachloro-1,3-butadiene 0.666 0.393 59.0 15.0-120
Hexachlorocyclopentadiene 0.666 0.484 72.7 15.0-120
Hexachloroethane 0.666 0.408 61.3 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.470 70.6 45.0-120
Isophorone 0.666 0.350 52.6 23.0-120
Naphthalene 0.666 0.344 51.7 18.0-120
Nitrobenzene 0.666 0.339 50.9 17.0-120
n-Nitrosodimethylamine 0.666 0.432 64.9 10.0-125
n-Nitrosodiphenylamine 0.666 0.461 69.2 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.398 59.8 26.0-120
Phenanthrene 0.666 0.444 66.7 42.0-120
Benzylbutyl phthalate 0.666 0.454 68.2 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.457 68.6 41.0-120
Di-n-butyl phthalate 0.666 0.470 70.6 43.0-120
Diethyl phthalate 0.666 0.470 70.6 43.0-120
Dimethyl phthalate 0.666 0.480 72.1 43.0-120
Di-n-octyl phthalate 0.666 0.482 72.4 40.0-120
Pyrene 0.666 0.476 71.5 41.0-120
1,2,4-Trichlorobenzene 0.666 0.393 59.0 17.0-120
4-Chloro-3-methylphenol 0.666 0.377 56.6 28.0-120
2-Chlorophenol 0.666 0.426 64.0 28.0-120
2,4-Dichlorophenol 0.666 0.397 59.6 25.0-120
2,4-Dimethylphenol 0.666 0.366 55.0 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.421 63.2 16.0-120
2,4-Dinitrophenol 0.666 0.292 43.8 10.0-120
2-Nitrophenol 0.666 0.430 64.6 20.0-120
4-Nitrophenol 0.666 0.473 71.0 27.0-120
Pentachlorophenol 0.666 0.410 61.6 29.0-120
Phenol 0.666 0.414 62.2 28.0-120
2,4,6-Trichlorophenol 0.666 0.439 65.9 37.0-120
(S) Nitrobenzene-d5 43.5 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004703
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-01
Laboratory Control Sample (LCS)
(LCS) R3891334-1 02/15/23 10:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 70.3 15.0-120
(S) p-Terphenyl-d14 75.7 10.0-120
(S) Phenol-d5 64.6 10.0-120
(S) 2-Fluorophenol 73.7 12.0-120
(S) 2,4,6-Tribromophenol 86.0 10.0-127
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/15/23 15:20 • (MS) R3891334-3 02/15/23 15:40 • (MSD) R3891334-4 02/15/23 16:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.905 ND 0.495 0.419 54.7 46.2 1 18.0-120 16.7 32
Acenaphthylene 0.905 ND 0.529 0.451 58.4 49.8 1 25.0-120 15.8 32
Anthracene 0.905 ND 0.559 0.462 61.7 51.1 1 22.0-120 18.9 29
Benzidine 1.81 ND ND ND 28.5 21.4 1 10.0-120 28.7 40
Benzo(a)anthracene 0.905 ND 0.581 0.472 64.1 52.1 1 25.0-120 20.7 29
Benzo(b)fluoranthene 0.905 ND 0.537 0.440 59.3 48.6 1 19.0-122 19.7 31
Benzo(k)fluoranthene 0.905 ND 0.536 0.434 59.2 47.9 1 23.0-120 21.0 30
Benzo(g,h,i)perylene 0.905 ND 0.553 0.450 61.1 49.7 1 10.0-120 20.6 33
Benzo(a)pyrene 0.905 ND 0.598 0.491 66.1 54.2 1 24.0-120 19.7 30
Bis(2-chlorethoxy)methane 0.905 ND ND ND 44.0 39.2 1 10.0-120 11.6 34
Bis(2-chloroethyl)ether 0.905 ND 0.551 ND 60.8 47.0 1 10.0-120 25.6 40
2,2-Oxybis(1-Chloropropane) 0.905 ND 0.462 ND 51.1 43.4 1 10.0-120 16.2 40
4-Bromophenyl-phenylether 0.905 ND 0.582 0.483 64.3 53.3 1 27.0-120 18.6 30
2-Chloronaphthalene 0.905 ND 0.491 0.420 54.2 46.4 1 20.0-120 15.5 32
4-Chlorophenyl-phenylether 0.905 ND 0.568 0.483 62.8 53.3 1 24.0-120 16.3 29
Chrysene 0.905 ND 0.576 0.465 63.7 51.4 1 21.0-120 21.4 29
Dibenz(a,h)anthracene 0.905 ND 0.576 0.474 63.7 52.4 1 10.0-120 19.4 32
3,3-Dichlorobenzidine 1.81 ND 1.28 0.980 70.8 54.2 1 10.0-120 26.5 34
2,4-Dinitrotoluene 0.905 ND 0.639 0.526 70.6 58.1 1 30.0-120 19.4 31
2,6-Dinitrotoluene 0.905 ND 0.571 0.487 63.1 53.8 1 25.0-120 15.9 31
Fluoranthene 0.905 ND 0.593 0.481 65.5 53.2 1 18.0-126 20.8 32
Fluorene 0.905 ND 0.537 0.453 59.3 50.0 1 25.0-120 17.0 30
Hexachlorobenzene 0.905 ND 0.593 0.502 65.5 55.4 1 27.0-120 16.6 28
Hexachloro-1,3-butadiene 0.905 ND ND ND 46.7 41.6 1 10.0-120 11.6 38
Hexachlorocyclopentadiene 0.905 ND ND ND 8.51 11.4 1 10.0-120 J6 29.2 40
Hexachloroethane 0.905 ND ND ND 43.5 38.0 1 10.0-120 13.6 40
Indeno(1,2,3-cd)pyrene 0.905 ND 0.533 0.439 58.9 48.5 1 10.0-120 19.3 32
Isophorone 0.905 ND ND ND 43.5 38.3 1 13.0-120 12.8 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2004703
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1584351-01
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/15/23 15:20 • (MS) R3891334-3 02/15/23 15:40 • (MSD) R3891334-4 02/15/23 16:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.905 ND 0.408 0.359 45.0 39.6 1 10.0-120 12.8 35
Nitrobenzene 0.905 ND ND ND 41.0 36.2 1 10.0-120 12.5 36
n-Nitrosodimethylamine 0.905 ND ND ND 45.3 36.6 1 10.0-127 21.2 40
n-Nitrosodiphenylamine 0.905 ND 0.549 ND 60.7 49.1 1 17.0-120 21.1 29
n-Nitrosodi-n-propylamine 0.905 ND ND ND 49.7 41.7 1 10.0-120 17.4 37
Phenanthrene 0.905 ND 0.523 0.434 57.8 47.9 1 17.0-120 18.7 31
Benzylbutyl phthalate 0.905 ND 0.578 0.460 63.8 50.8 1 23.0-120 22.8 30
Bis(2-ethylhexyl)phthalate 0.905 ND 0.589 0.481 65.0 53.2 1 17.0-126 20.1 30
Di-n-butyl phthalate 0.905 ND 0.568 0.461 62.8 50.9 1 30.0-120 20.9 29
Diethyl phthalate 0.905 ND 0.544 0.455 60.1 50.3 1 26.0-120 17.7 28
Dimethyl phthalate 0.905 ND 0.541 0.457 59.8 50.5 1 25.0-120 16.9 29
Di-n-octyl phthalate 0.905 ND 0.632 0.515 69.8 56.9 1 21.0-123 20.4 29
Pyrene 0.905 ND 0.559 0.446 61.7 49.2 1 16.0-121 22.5 32
1,2,4-Trichlorobenzene 0.905 ND ND ND 47.4 42.3 1 12.0-120 11.4 37
4-Chloro-3-methylphenol 0.905 ND 0.470 ND 52.0 44.1 1 15.0-120 16.2 30
2-Chlorophenol 0.905 ND 0.487 ND 53.8 46.8 1 15.0-120 13.7 37
2,4-Dichlorophenol 0.905 ND 0.468 ND 51.7 44.6 1 20.0-120 14.7 31
2,4-Dimethylphenol 0.905 ND ND ND 47.4 40.5 1 10.0-120 15.7 33
4,6-Dinitro-2-methylphenol 0.905 ND 0.474 ND 52.4 43.8 1 10.0-120 17.8 39
2,4-Dinitrophenol 0.905 ND ND ND 47.1 40.4 1 10.0-121 15.4 40
2-Nitrophenol 0.905 ND 0.503 ND 55.6 48.9 1 12.0-120 12.6 39
4-Nitrophenol 0.905 ND 0.610 0.506 67.4 55.9 1 10.0-137 18.8 32
Pentachlorophenol 0.905 ND 0.615 0.479 67.9 52.9 1 10.0-160 24.9 31
Phenol 0.905 ND 0.473 ND 52.3 43.2 1 12.0-120 18.9 38
2,4,6-Trichlorophenol 0.905 ND 0.523 ND 57.8 48.5 1 19.0-120 17.5 32
(S) Nitrobenzene-d5 39.9 35.7 10.0-122
(S) 2-Fluorobiphenyl 56.5 52.6 15.0-120
(S) p-Terphenyl-d14 67.3 58.9 10.0-120
(S) Phenol-d5 53.9 50.2 10.0-120
(S) 2-Fluorophenol 59.8 54.7 12.0-120
(S) 2,4,6-Tribromophenol 76.9 69.1 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2007018
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1584351-01,02,03,04
Method Blank (MB)
(MB) R3891958-2 02/16/23 22:38
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 73.0 23.0-120
(S) Nitrobenzene-d5 64.0 14.0-149
(S) 2-Fluorobiphenyl 71.0 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3891958-1 02/16/23 22:18
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0655 81.9 50.0-126
Acenaphthene 0.0800 0.0604 75.5 50.0-120
Acenaphthylene 0.0800 0.0643 80.4 50.0-120
Benzo(a)anthracene 0.0800 0.0657 82.1 45.0-120
Benzo(a)pyrene 0.0800 0.0589 73.6 42.0-120
Benzo(b)fluoranthene 0.0800 0.0598 74.8 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0595 74.4 45.0-125
Benzo(k)fluoranthene 0.0800 0.0589 73.6 49.0-125
Chrysene 0.0800 0.0642 80.3 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0599 74.9 47.0-125
Fluoranthene 0.0800 0.0652 81.5 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2007018
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1584351-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3891958-1 02/16/23 22:18
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0674 84.3 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0625 78.1 46.0-125
Naphthalene 0.0800 0.0597 74.6 50.0-120
Phenanthrene 0.0800 0.0616 77.0 47.0-120
Pyrene 0.0800 0.0634 79.3 43.0-123
1-Methylnaphthalene 0.0800 0.0603 75.4 51.0-121
2-Methylnaphthalene 0.0800 0.0635 79.4 50.0-120
2-Chloronaphthalene 0.0800 0.0619 77.4 50.0-120
(S) p-Terphenyl-d14 74.9 23.0-120
(S) Nitrobenzene-d5 71.9 14.0-149
(S) 2-Fluorobiphenyl 75.1 34.0-125
L1584351-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1584351-01 02/17/23 04:55 • (MS) R3891958-5 02/17/23 05:35 • (MSD) R3891958-6 02/17/23 05:55
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.109 ND 0.0672 0.0761 61.8 70.0 1 10.0-145 12.5 30
Acenaphthene 0.109 ND 0.0638 0.0680 58.6 62.5 1 14.0-127 6.40 27
Acenaphthylene 0.109 ND 0.0681 0.0730 62.6 67.1 1 21.0-124 6.94 25
Benzo(a)anthracene 0.109 ND 0.0782 0.0968 69.3 86.4 1 10.0-139 21.3 30
Chrysene 0.109 ND 0.0719 0.0964 66.1 88.6 1 10.0-145 29.1 30
Fluoranthene 0.109 ND 0.0814 0.121 70.7 107 1 10.0-153 J3 38.9 33
Fluorene 0.109 ND 0.0710 0.0779 65.3 71.6 1 11.0-130 9.32 29
Naphthalene 0.109 ND 0.0628 0.0663 57.8 61.0 1 10.0-135 5.47 27
Phenanthrene 0.109 ND 0.0684 0.0867 62.9 79.8 1 10.0-144 23.7 31
Pyrene 0.109 ND 0.0712 0.103 61.2 90.0 1 10.0-148 J3 36.1 35
1-Methylnaphthalene 0.109 ND 0.0651 0.0680 59.9 62.5 1 10.0-142 4.29 28
2-Methylnaphthalene 0.109 ND 0.0684 0.0726 62.9 66.8 1 10.0-137 5.98 28
2-Chloronaphthalene 0.109 ND 0.0634 0.0651 58.3 59.9 1 29.0-120 2.75 24
(S) p-Terphenyl-d14 57.1 58.3 23.0-120
(S) Nitrobenzene-d5 58.0 68.0 14.0-149
(S) 2-Fluorobiphenyl 61.4 62.9 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
February 13, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1582319
Samples Received:02/04/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
February 13, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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February 13, 2023
Jason Romer
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
SW-1 L1582319-01 6
SW-2 L1582319-02 11
SW-3 L1582319-03 16
SW-4 L1582319-04 21
SW-5 L1582319-05 26
Qc: Quality Control Summary 31
Gravimetric Analysis by Method 2540 D-2015 31
Wet Chemistry by Method 1664A 32
Wet Chemistry by Method 3500Cr C-2011 33
Mercury by Method 7470A 34
Metals (ICP) by Method 6010B 35
Volatile Organic Compounds (GC) by Method 8015D/GRO 39
Volatile Organic Compounds (GC/MS) by Method 8260B 40
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 44
Polychlorinated Biphenyls (GC) by Method 8082 45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 47
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 52
Gl: Glossary of Terms 54
Al: Accreditations & Locations 55
Sc: Sample Chain of Custody 56
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-1 L1582319-01 GW Richie T. 02/03/23 09:00 02/04/23 10:20
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 D-2015 WG2000336 1 02/04/23 21:28 02/04/23 22:57 DTM Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2003057 1 02/10/23 09:06 02/10/23 14:42 MCE Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2000530 1 02/06/23 04:25 02/06/23 04:25 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2001380 1 02/07/23 09:07 02/07/23 18:04 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2001114 1 02/07/23 01:14 02/07/23 10:53 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2003633 1 02/09/23 20:38 02/09/23 20:38 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2001134 1 02/07/23 02:03 02/07/23 02:03 ZME Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2000565 20 02/07/23 09:37 02/07/23 21:48 DMG Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2000361 1 02/06/23 06:29 02/06/23 17:01 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2000359 1 02/06/23 06:31 02/08/23 18:07 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2000383 1 02/06/23 08:40 02/06/23 23:03 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-2 L1582319-02 GW Richie T. 02/03/23 11:20 02/04/23 10:20
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 D-2015 WG2000336 1 02/04/23 21:28 02/04/23 22:57 DTM Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2003057 1 02/10/23 09:06 02/10/23 14:42 MCE Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2000530 1 02/06/23 04:33 02/06/23 04:33 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2001380 1 02/07/23 09:07 02/07/23 18:06 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2001114 1 02/07/23 01:14 02/07/23 10:56 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2003633 1 02/09/23 21:00 02/09/23 21:00 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2001134 1 02/07/23 02:24 02/07/23 02:24 ZME Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2000565 1 02/07/23 09:37 02/07/23 19:30 DMG Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2000361 1 02/06/23 06:29 02/06/23 17:12 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2000359 1 02/06/23 06:31 02/07/23 13:19 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2000383 1 02/06/23 08:40 02/06/23 23:21 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-3 L1582319-03 GW Richie T. 02/03/23 12:45 02/04/23 10:20
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 D-2015 WG2000336 1 02/04/23 21:28 02/04/23 22:57 DTM Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2003057 1 02/10/23 09:06 02/10/23 14:42 MCE Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2000530 1 02/06/23 05:12 02/06/23 05:12 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2001380 1 02/07/23 09:07 02/07/23 17:53 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2001114 1 02/07/23 01:14 02/07/23 11:04 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2003633 1 02/09/23 21:22 02/09/23 21:22 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2001134 1 02/07/23 02:47 02/07/23 02:47 ZME Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2000565 1 02/07/23 09:37 02/07/23 19:50 DMG Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001014 1 02/06/23 16:26 02/07/23 01:19 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2000359 1 02/06/23 06:31 02/07/23 13:40 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2000383 1 02/06/23 08:40 02/06/23 23:39 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-4 L1582319-04 GW Richie T. 02/03/23 14:30 02/04/23 10:20
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 D-2015 WG2000336 1 02/04/23 21:28 02/04/23 22:57 DTM Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2003057 1 02/10/23 09:06 02/10/23 14:42 MCE Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2000530 1 02/06/23 05:19 02/06/23 05:19 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2001380 1 02/07/23 09:07 02/07/23 18:09 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2001114 1 02/07/23 01:14 02/07/23 11:07 ABL Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-4 L1582319-04 GW Richie T. 02/03/23 14:30 02/04/23 10:20
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2003633 1 02/09/23 21:44 02/09/23 21:44 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2001134 1 02/07/23 03:08 02/07/23 03:08 ZME Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2000565 1 02/07/23 09:37 02/08/23 00:23 DMG Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001014 1 02/06/23 16:26 02/07/23 01:30 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2000359 1 02/06/23 06:31 02/07/23 14:02 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2000383 1 02/06/23 08:40 02/06/23 23:57 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-5 L1582319-05 GW Richie T. 02/03/23 15:30 02/04/23 10:20
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 D-2015 WG2000336 1 02/04/23 21:28 02/04/23 22:57 DTM Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2003057 1 02/10/23 09:06 02/10/23 14:42 MCE Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2000530 1 02/06/23 05:27 02/06/23 05:27 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2001380 1 02/07/23 09:07 02/07/23 18:11 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2001119 1 02/07/23 04:45 02/07/23 13:19 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2003633 1 02/09/23 22:06 02/09/23 22:06 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2001134 1 02/07/23 03:31 02/07/23 03:31 ZME Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2000565 1 02/07/23 09:37 02/07/23 20:30 DMG Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2001014 1 02/06/23 16:26 02/07/23 01:40 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2000359 1 02/06/23 06:31 02/07/23 14:23 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2000383 1 02/06/23 08:40 02/07/23 00:14 AGW Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1582319-01 SW-1 3500Cr C-2011
L1582319-05 SW-5 3500Cr C-2011
pH outside of method requirement.
Lab Sample ID Project Sample ID Method
L1582319-01 SW-1 3511/8015
L1582319-02 SW-2 3511/8015
L1582319-03 SW-3 3511/8015
L1582319-04 SW-4 3511/8015
L1582319-05 SW-5 3511/8015
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Jason Romer
Project Manager
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SAMPLE RESULTS - 01
L1582319
SW-1
Collected date/time: 02/03/23 09:00
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 3.00 J4 2.50 1 02/04/2023 22:57 WG2000336
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.25 1 02/10/2023 14:42 WG2003057
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.000909 0.000500 1 02/06/2023 04:25 WG2000530
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 02/07/2023 18:04 WG2001380
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 02/07/2023 10:53 WG2001114
Arsenic 0.0472 B 0.0100 1 02/07/2023 10:53 WG2001114
Beryllium ND 0.00200 1 02/07/2023 10:53 WG2001114
Cadmium ND 0.00200 1 02/07/2023 10:53 WG2001114
Chromium ND 0.0100 1 02/07/2023 10:53 WG2001114
Copper 0.0219 0.0100 1 02/07/2023 10:53 WG2001114
Lead 0.0177 0.00600 1 02/07/2023 10:53 WG2001114
Nickel ND 0.0100 1 02/07/2023 10:53 WG2001114
Selenium ND 0.0100 1 02/07/2023 10:53 WG2001114
Silver ND 0.00500 1 02/07/2023 10:53 WG2001114
Thallium ND 0.0100 1 02/07/2023 10:53 WG2001114
Zinc 0.137 0.0500 1 02/07/2023 10:53 WG2001114
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 02/09/2023 20:38 WG2003633
(S) a,a,a-Trifluorotoluene(FID) 101 78.0-120 02/09/2023 20:38 WG2003633
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 02/07/2023 02:03 WG2001134
Acrolein ND 0.0500 1 02/07/2023 02:03 WG2001134
Acrylonitrile ND 0.0100 1 02/07/2023 02:03 WG2001134
Benzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Bromobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Bromodichloromethane ND 0.00100 1 02/07/2023 02:03 WG2001134
Bromoform ND 0.00100 1 02/07/2023 02:03 WG2001134
Bromomethane ND 0.00500 1 02/07/2023 02:03 WG2001134
n-Butylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
sec-Butylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
tert-Butylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1582319
SW-1
Collected date/time: 02/03/23 09:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 02/07/2023 02:03 WG2001134
Chlorobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Chlorodibromomethane ND 0.00100 1 02/07/2023 02:03 WG2001134
Chloroethane ND 0.00500 1 02/07/2023 02:03 WG2001134
Chloroform ND 0.00500 1 02/07/2023 02:03 WG2001134
Chloromethane ND 0.00250 1 02/07/2023 02:03 WG2001134
2-Chlorotoluene ND 0.00100 1 02/07/2023 02:03 WG2001134
4-Chlorotoluene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2-Dibromo-3-Chloropropane ND 0.00500 1 02/07/2023 02:03 WG2001134
1,2-Dibromoethane ND 0.00100 1 02/07/2023 02:03 WG2001134
Dibromomethane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2-Dichlorobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,3-Dichlorobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,4-Dichlorobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Dichlorodifluoromethane ND 0.00500 1 02/07/2023 02:03 WG2001134
1,1-Dichloroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2-Dichloroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1-Dichloroethene ND 0.00100 1 02/07/2023 02:03 WG2001134
cis-1,2-Dichloroethene ND 0.00100 1 02/07/2023 02:03 WG2001134
trans-1,2-Dichloroethene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2-Dichloropropane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1-Dichloropropene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,3-Dichloropropane ND 0.00100 1 02/07/2023 02:03 WG2001134
cis-1,3-Dichloropropene ND 0.00100 1 02/07/2023 02:03 WG2001134
trans-1,3-Dichloropropene ND 0.00100 1 02/07/2023 02:03 WG2001134
2,2-Dichloropropane ND 0.00100 1 02/07/2023 02:03 WG2001134
Di-isopropyl ether ND 0.00100 1 02/07/2023 02:03 WG2001134
Ethylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Hexachloro-1,3-butadiene ND 0.00100 1 02/07/2023 02:03 WG2001134
Isopropylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
p-Isopropyltoluene ND 0.00100 1 02/07/2023 02:03 WG2001134
2-Butanone (MEK)ND 0.0100 1 02/07/2023 02:03 WG2001134
Methylene Chloride ND 0.00500 1 02/07/2023 02:03 WG2001134
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 02/07/2023 02:03 WG2001134
Methyl tert-butyl ether ND 0.00100 1 02/07/2023 02:03 WG2001134
Naphthalene ND 0.00500 1 02/07/2023 02:03 WG2001134
n-Propylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Styrene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
Tetrachloroethene ND J4 0.00100 1 02/07/2023 02:03 WG2001134
Toluene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2,3-Trichlorobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2,4-Trichlorobenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1,1-Trichloroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
1,1,2-Trichloroethane ND 0.00100 1 02/07/2023 02:03 WG2001134
Trichloroethene ND 0.00100 1 02/07/2023 02:03 WG2001134
Trichlorofluoromethane ND 0.00500 1 02/07/2023 02:03 WG2001134
1,2,3-Trichloropropane ND 0.00250 1 02/07/2023 02:03 WG2001134
1,2,4-Trimethylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,2,3-Trimethylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
1,3,5-Trimethylbenzene ND 0.00100 1 02/07/2023 02:03 WG2001134
Vinyl chloride ND 0.00100 1 02/07/2023 02:03 WG2001134
Xylenes, Total ND 0.00300 1 02/07/2023 02:03 WG2001134
(S) Toluene-d8 111 80.0-120 02/07/2023 02:03 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1582319
SW-1
Collected date/time: 02/03/23 09:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 88.3 77.0-126 02/07/2023 02:03 WG2001134
(S) 1,2-Dichloroethane-d4 100 70.0-130 02/07/2023 02:03 WG2001134
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 66.7 2.00 20 02/07/2023 21:48 WG2000565
(S) o-Terphenyl 0.000 J7 31.0-160 02/07/2023 21:48 WG2000565
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 02/06/2023 17:01 WG2000361
PCB 1221 ND 0.000500 1 02/06/2023 17:01 WG2000361
PCB 1232 ND 0.000500 1 02/06/2023 17:01 WG2000361
PCB 1242 ND 0.000500 1 02/06/2023 17:01 WG2000361
PCB 1248 ND 0.000500 1 02/06/2023 17:01 WG2000361
PCB 1254 ND 0.000500 1 02/06/2023 17:01 WG2000361
PCB 1260 ND 0.000500 1 02/06/2023 17:01 WG2000361
(S) Decachlorobiphenyl 55.6 10.0-128 02/06/2023 17:01 WG2000361
(S) Tetrachloro-m-xylene 36.9 10.0-127 02/06/2023 17:01 WG2000361
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 02/08/2023 18:07 WG2000359
Acenaphthylene ND 0.00100 1 02/08/2023 18:07 WG2000359
Anthracene ND 0.00100 1 02/08/2023 18:07 WG2000359
Benzidine ND J4 0.0100 1 02/08/2023 18:07 WG2000359
Benzo(a)anthracene ND 0.00100 1 02/08/2023 18:07 WG2000359
Benzo(b)fluoranthene ND 0.00100 1 02/08/2023 18:07 WG2000359
Benzo(k)fluoranthene ND 0.00100 1 02/08/2023 18:07 WG2000359
Benzo(g,h,i)perylene ND 0.00100 1 02/08/2023 18:07 WG2000359
Benzo(a)pyrene ND 0.00100 1 02/08/2023 18:07 WG2000359
Bis(2-chlorethoxy)methane ND 0.0100 1 02/08/2023 18:07 WG2000359
Bis(2-chloroethyl)ether ND 0.0100 1 02/08/2023 18:07 WG2000359
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 02/08/2023 18:07 WG2000359
4-Bromophenyl-phenylether ND 0.0100 1 02/08/2023 18:07 WG2000359
2-Chloronaphthalene ND 0.00100 1 02/08/2023 18:07 WG2000359
4-Chlorophenyl-phenylether ND 0.0100 1 02/08/2023 18:07 WG2000359
Chrysene ND 0.00100 1 02/08/2023 18:07 WG2000359
Dibenz(a,h)anthracene ND 0.00100 1 02/08/2023 18:07 WG2000359
1,2-Dichlorobenzene ND 0.0100 1 02/08/2023 18:07 WG2000359
1,3-Dichlorobenzene ND 0.0100 1 02/08/2023 18:07 WG2000359
1,4-Dichlorobenzene ND 0.0100 1 02/08/2023 18:07 WG2000359
3,3-Dichlorobenzidine ND 0.0100 1 02/08/2023 18:07 WG2000359
2,4-Dinitrotoluene ND 0.0100 1 02/08/2023 18:07 WG2000359
2,6-Dinitrotoluene ND 0.0100 1 02/08/2023 18:07 WG2000359
Fluoranthene ND 0.00100 1 02/08/2023 18:07 WG2000359
Fluorene ND 0.00100 1 02/08/2023 18:07 WG2000359
Hexachlorobenzene ND 0.00100 1 02/08/2023 18:07 WG2000359
Hexachloro-1,3-butadiene ND 0.0100 1 02/08/2023 18:07 WG2000359
Hexachlorocyclopentadiene ND 0.0100 1 02/08/2023 18:07 WG2000359
Hexachloroethane ND 0.0100 1 02/08/2023 18:07 WG2000359
Indeno(1,2,3-cd)pyrene ND 0.00100 1 02/08/2023 18:07 WG2000359
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1582319
SW-1
Collected date/time: 02/03/23 09:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Isophorone ND 0.0100 1 02/08/2023 18:07 WG2000359
Naphthalene ND 0.00100 1 02/08/2023 18:07 WG2000359
Nitrobenzene ND 0.0100 1 02/08/2023 18:07 WG2000359
n-Nitrosodimethylamine ND 0.0100 1 02/08/2023 18:07 WG2000359
n-Nitrosodiphenylamine ND 0.0100 1 02/08/2023 18:07 WG2000359
n-Nitrosodi-n-propylamine ND 0.0100 1 02/08/2023 18:07 WG2000359
Phenanthrene ND 0.00100 1 02/08/2023 18:07 WG2000359
Benzylbutyl phthalate ND 0.00300 1 02/08/2023 18:07 WG2000359
Bis(2-ethylhexyl)phthalate ND 0.00300 1 02/08/2023 18:07 WG2000359
Di-n-butyl phthalate ND 0.00300 1 02/08/2023 18:07 WG2000359
Diethyl phthalate ND 0.00300 1 02/08/2023 18:07 WG2000359
Dimethyl phthalate ND 0.00300 1 02/08/2023 18:07 WG2000359
Di-n-octyl phthalate ND 0.00300 1 02/08/2023 18:07 WG2000359
Pyrene ND 0.00100 1 02/08/2023 18:07 WG2000359
1,2,4-Trichlorobenzene ND 0.0100 1 02/08/2023 18:07 WG2000359
4-Chloro-3-methylphenol ND 0.0100 1 02/08/2023 18:07 WG2000359
2-Chlorophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
2,4-Dichlorophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
2,4-Dimethylphenol ND 0.0100 1 02/08/2023 18:07 WG2000359
4,6-Dinitro-2-methylphenol ND 0.0100 1 02/08/2023 18:07 WG2000359
2,4-Dinitrophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
2-Nitrophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
4-Nitrophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
Pentachlorophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
Phenol ND 0.0100 1 02/08/2023 18:07 WG2000359
2,4,6-Trichlorophenol ND 0.0100 1 02/08/2023 18:07 WG2000359
(S) 2-Fluorophenol 24.5 10.0-120 02/08/2023 18:07 WG2000359
(S) Phenol-d5 17.3 10.0-120 02/08/2023 18:07 WG2000359
(S) Nitrobenzene-d5 64.6 10.0-127 02/08/2023 18:07 WG2000359
(S) 2-Fluorobiphenyl 65.4 10.0-130 02/08/2023 18:07 WG2000359
(S) 2,4,6-Tribromophenol 61.0 10.0-155 02/08/2023 18:07 WG2000359
(S) p-Terphenyl-d14 59.9 10.0-128 02/08/2023 18:07 WG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Acenaphthene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Acenaphthylene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Benzo(a)anthracene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Benzo(a)pyrene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Benzo(b)fluoranthene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Benzo(g,h,i)perylene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Benzo(k)fluoranthene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Chrysene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Dibenz(a,h)anthracene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Fluoranthene ND 0.000100 1 02/06/2023 23:03 WG2000383
Fluorene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Naphthalene ND 0.000250 1 02/06/2023 23:03 WG2000383
Phenanthrene ND 0.0000500 1 02/06/2023 23:03 WG2000383
Pyrene ND 0.0000500 1 02/06/2023 23:03 WG2000383
1-Methylnaphthalene ND 0.000250 1 02/06/2023 23:03 WG2000383
2-Methylnaphthalene ND 0.000250 1 02/06/2023 23:03 WG2000383
2-Chloronaphthalene ND 0.000250 1 02/06/2023 23:03 WG2000383
(S) Nitrobenzene-d5 95.3 31.0-160 02/06/2023 23:03 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1582319
SW-1
Collected date/time: 02/03/23 09:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorobiphenyl 91.6 48.0-148 02/06/2023 23:03 WG2000383
(S) p-Terphenyl-d14 102 37.0-146 02/06/2023 23:03 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1582319
SW-2
Collected date/time: 02/03/23 11:20
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 26.3 J4 2.80 1 02/04/2023 22:57 WG2000336
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.56 1 02/10/2023 14:42 WG2003057
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.000554 0.000500 1 02/06/2023 04:33 WG2000530
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 02/07/2023 18:06 WG2001380
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 02/07/2023 10:56 WG2001114
Arsenic 0.0275 B 0.0100 1 02/07/2023 10:56 WG2001114
Beryllium ND 0.00200 1 02/07/2023 10:56 WG2001114
Cadmium ND 0.00200 1 02/07/2023 10:56 WG2001114
Chromium ND 0.0100 1 02/07/2023 10:56 WG2001114
Copper ND 0.0100 1 02/07/2023 10:56 WG2001114
Lead ND 0.00600 1 02/07/2023 10:56 WG2001114
Nickel ND 0.0100 1 02/07/2023 10:56 WG2001114
Selenium ND 0.0100 1 02/07/2023 10:56 WG2001114
Silver ND 0.00500 1 02/07/2023 10:56 WG2001114
Thallium ND 0.0100 1 02/07/2023 10:56 WG2001114
Zinc ND 0.0500 1 02/07/2023 10:56 WG2001114
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 02/09/2023 21:00 WG2003633
(S) a,a,a-Trifluorotoluene(FID) 102 78.0-120 02/09/2023 21:00 WG2003633
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 02/07/2023 02:24 WG2001134
Acrolein ND 0.0500 1 02/07/2023 02:24 WG2001134
Acrylonitrile ND 0.0100 1 02/07/2023 02:24 WG2001134
Benzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Bromobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Bromodichloromethane ND 0.00100 1 02/07/2023 02:24 WG2001134
Bromoform ND 0.00100 1 02/07/2023 02:24 WG2001134
Bromomethane ND 0.00500 1 02/07/2023 02:24 WG2001134
n-Butylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
sec-Butylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
tert-Butylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1582319
SW-2
Collected date/time: 02/03/23 11:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 02/07/2023 02:24 WG2001134
Chlorobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Chlorodibromomethane ND 0.00100 1 02/07/2023 02:24 WG2001134
Chloroethane ND 0.00500 1 02/07/2023 02:24 WG2001134
Chloroform ND 0.00500 1 02/07/2023 02:24 WG2001134
Chloromethane ND 0.00250 1 02/07/2023 02:24 WG2001134
2-Chlorotoluene ND 0.00100 1 02/07/2023 02:24 WG2001134
4-Chlorotoluene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2-Dibromo-3-Chloropropane ND 0.00500 1 02/07/2023 02:24 WG2001134
1,2-Dibromoethane ND 0.00100 1 02/07/2023 02:24 WG2001134
Dibromomethane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2-Dichlorobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,3-Dichlorobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,4-Dichlorobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Dichlorodifluoromethane ND 0.00500 1 02/07/2023 02:24 WG2001134
1,1-Dichloroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2-Dichloroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1-Dichloroethene ND 0.00100 1 02/07/2023 02:24 WG2001134
cis-1,2-Dichloroethene ND 0.00100 1 02/07/2023 02:24 WG2001134
trans-1,2-Dichloroethene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2-Dichloropropane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1-Dichloropropene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,3-Dichloropropane ND 0.00100 1 02/07/2023 02:24 WG2001134
cis-1,3-Dichloropropene ND 0.00100 1 02/07/2023 02:24 WG2001134
trans-1,3-Dichloropropene ND 0.00100 1 02/07/2023 02:24 WG2001134
2,2-Dichloropropane ND 0.00100 1 02/07/2023 02:24 WG2001134
Di-isopropyl ether ND 0.00100 1 02/07/2023 02:24 WG2001134
Ethylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Hexachloro-1,3-butadiene ND 0.00100 1 02/07/2023 02:24 WG2001134
Isopropylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
p-Isopropyltoluene ND 0.00100 1 02/07/2023 02:24 WG2001134
2-Butanone (MEK)ND 0.0100 1 02/07/2023 02:24 WG2001134
Methylene Chloride ND 0.00500 1 02/07/2023 02:24 WG2001134
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 02/07/2023 02:24 WG2001134
Methyl tert-butyl ether ND 0.00100 1 02/07/2023 02:24 WG2001134
Naphthalene ND 0.00500 1 02/07/2023 02:24 WG2001134
n-Propylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Styrene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
Tetrachloroethene ND J4 0.00100 1 02/07/2023 02:24 WG2001134
Toluene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2,3-Trichlorobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2,4-Trichlorobenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1,1-Trichloroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
1,1,2-Trichloroethane ND 0.00100 1 02/07/2023 02:24 WG2001134
Trichloroethene ND 0.00100 1 02/07/2023 02:24 WG2001134
Trichlorofluoromethane ND 0.00500 1 02/07/2023 02:24 WG2001134
1,2,3-Trichloropropane ND 0.00250 1 02/07/2023 02:24 WG2001134
1,2,4-Trimethylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,2,3-Trimethylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
1,3,5-Trimethylbenzene ND 0.00100 1 02/07/2023 02:24 WG2001134
Vinyl chloride ND 0.00100 1 02/07/2023 02:24 WG2001134
Xylenes, Total ND 0.00300 1 02/07/2023 02:24 WG2001134
(S) Toluene-d8 109 80.0-120 02/07/2023 02:24 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1582319
SW-2
Collected date/time: 02/03/23 11:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 106 77.0-126 02/07/2023 02:24 WG2001134
(S) 1,2-Dichloroethane-d4 92.9 70.0-130 02/07/2023 02:24 WG2001134
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 0.156 0.100 1 02/07/2023 19:30 WG2000565
(S) o-Terphenyl 107 31.0-160 02/07/2023 19:30 WG2000565
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 02/06/2023 17:12 WG2000361
PCB 1221 ND 0.000500 1 02/06/2023 17:12 WG2000361
PCB 1232 ND 0.000500 1 02/06/2023 17:12 WG2000361
PCB 1242 ND 0.000500 1 02/06/2023 17:12 WG2000361
PCB 1248 ND 0.000500 1 02/06/2023 17:12 WG2000361
PCB 1254 ND 0.000500 1 02/06/2023 17:12 WG2000361
PCB 1260 ND 0.000500 1 02/06/2023 17:12 WG2000361
(S) Decachlorobiphenyl 71.8 10.0-128 02/06/2023 17:12 WG2000361
(S) Tetrachloro-m-xylene 56.6 10.0-127 02/06/2023 17:12 WG2000361
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 02/07/2023 13:19 WG2000359
Acenaphthylene ND 0.00100 1 02/07/2023 13:19 WG2000359
Anthracene ND 0.00100 1 02/07/2023 13:19 WG2000359
Benzidine ND J4 0.0100 1 02/07/2023 13:19 WG2000359
Benzo(a)anthracene ND 0.00100 1 02/07/2023 13:19 WG2000359
Benzo(b)fluoranthene ND 0.00100 1 02/07/2023 13:19 WG2000359
Benzo(k)fluoranthene ND 0.00100 1 02/07/2023 13:19 WG2000359
Benzo(g,h,i)perylene ND 0.00100 1 02/07/2023 13:19 WG2000359
Benzo(a)pyrene ND 0.00100 1 02/07/2023 13:19 WG2000359
Bis(2-chlorethoxy)methane ND 0.0100 1 02/07/2023 13:19 WG2000359
Bis(2-chloroethyl)ether ND 0.0100 1 02/07/2023 13:19 WG2000359
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 02/07/2023 13:19 WG2000359
4-Bromophenyl-phenylether ND 0.0100 1 02/07/2023 13:19 WG2000359
2-Chloronaphthalene ND 0.00100 1 02/07/2023 13:19 WG2000359
4-Chlorophenyl-phenylether ND 0.0100 1 02/07/2023 13:19 WG2000359
Chrysene ND 0.00100 1 02/07/2023 13:19 WG2000359
Dibenz(a,h)anthracene ND 0.00100 1 02/07/2023 13:19 WG2000359
1,2-Dichlorobenzene ND 0.0100 1 02/07/2023 13:19 WG2000359
1,3-Dichlorobenzene ND 0.0100 1 02/07/2023 13:19 WG2000359
1,4-Dichlorobenzene ND 0.0100 1 02/07/2023 13:19 WG2000359
3,3-Dichlorobenzidine ND 0.0100 1 02/07/2023 13:19 WG2000359
2,4-Dinitrotoluene ND 0.0100 1 02/07/2023 13:19 WG2000359
2,6-Dinitrotoluene ND 0.0100 1 02/07/2023 13:19 WG2000359
Fluoranthene ND 0.00100 1 02/07/2023 13:19 WG2000359
Fluorene ND 0.00100 1 02/07/2023 13:19 WG2000359
Hexachlorobenzene ND 0.00100 1 02/07/2023 13:19 WG2000359
Hexachloro-1,3-butadiene ND 0.0100 1 02/07/2023 13:19 WG2000359
Hexachlorocyclopentadiene ND 0.0100 1 02/07/2023 13:19 WG2000359
Hexachloroethane ND 0.0100 1 02/07/2023 13:19 WG2000359
Indeno(1,2,3-cd)pyrene ND 0.00100 1 02/07/2023 13:19 WG2000359
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 13 of 56
SAMPLE RESULTS - 02
L1582319
SW-2
Collected date/time: 02/03/23 11:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Isophorone ND 0.0100 1 02/07/2023 13:19 WG2000359
Naphthalene ND 0.00100 1 02/07/2023 13:19 WG2000359
Nitrobenzene ND 0.0100 1 02/07/2023 13:19 WG2000359
n-Nitrosodimethylamine ND 0.0100 1 02/07/2023 13:19 WG2000359
n-Nitrosodiphenylamine ND 0.0100 1 02/07/2023 13:19 WG2000359
n-Nitrosodi-n-propylamine ND 0.0100 1 02/07/2023 13:19 WG2000359
Phenanthrene ND 0.00100 1 02/07/2023 13:19 WG2000359
Benzylbutyl phthalate ND 0.00300 1 02/07/2023 13:19 WG2000359
Bis(2-ethylhexyl)phthalate ND 0.00300 1 02/07/2023 13:19 WG2000359
Di-n-butyl phthalate ND 0.00300 1 02/07/2023 13:19 WG2000359
Diethyl phthalate ND 0.00300 1 02/07/2023 13:19 WG2000359
Dimethyl phthalate ND 0.00300 1 02/07/2023 13:19 WG2000359
Di-n-octyl phthalate ND 0.00300 1 02/07/2023 13:19 WG2000359
Pyrene ND 0.00100 1 02/07/2023 13:19 WG2000359
1,2,4-Trichlorobenzene ND 0.0100 1 02/07/2023 13:19 WG2000359
4-Chloro-3-methylphenol ND 0.0100 1 02/07/2023 13:19 WG2000359
2-Chlorophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
2,4-Dichlorophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
2,4-Dimethylphenol ND 0.0100 1 02/07/2023 13:19 WG2000359
4,6-Dinitro-2-methylphenol ND 0.0100 1 02/07/2023 13:19 WG2000359
2,4-Dinitrophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
2-Nitrophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
4-Nitrophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
Pentachlorophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
Phenol ND 0.0100 1 02/07/2023 13:19 WG2000359
2,4,6-Trichlorophenol ND 0.0100 1 02/07/2023 13:19 WG2000359
(S) 2-Fluorophenol 20.2 10.0-120 02/07/2023 13:19 WG2000359
(S) Phenol-d5 12.2 10.0-120 02/07/2023 13:19 WG2000359
(S) Nitrobenzene-d5 38.1 10.0-127 02/07/2023 13:19 WG2000359
(S) 2-Fluorobiphenyl 42.3 10.0-130 02/07/2023 13:19 WG2000359
(S) 2,4,6-Tribromophenol 40.2 10.0-155 02/07/2023 13:19 WG2000359
(S) p-Terphenyl-d14 49.3 10.0-128 02/07/2023 13:19 WG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Acenaphthene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Acenaphthylene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Benzo(a)anthracene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Benzo(a)pyrene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Benzo(b)fluoranthene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Benzo(g,h,i)perylene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Benzo(k)fluoranthene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Chrysene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Dibenz(a,h)anthracene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Fluoranthene ND 0.000100 1 02/06/2023 23:21 WG2000383
Fluorene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Naphthalene ND 0.000250 1 02/06/2023 23:21 WG2000383
Phenanthrene ND 0.0000500 1 02/06/2023 23:21 WG2000383
Pyrene ND 0.0000500 1 02/06/2023 23:21 WG2000383
1-Methylnaphthalene ND 0.000250 1 02/06/2023 23:21 WG2000383
2-Methylnaphthalene ND 0.000250 1 02/06/2023 23:21 WG2000383
2-Chloronaphthalene ND 0.000250 1 02/06/2023 23:21 WG2000383
(S) Nitrobenzene-d5 104 31.0-160 02/06/2023 23:21 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1582319
SW-2
Collected date/time: 02/03/23 11:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorobiphenyl 93.2 48.0-148 02/06/2023 23:21 WG2000383
(S) p-Terphenyl-d14 105 37.0-146 02/06/2023 23:21 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 15 of 56
SAMPLE RESULTS - 03
L1582319
SW-3
Collected date/time: 02/03/23 12:45
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 12.9 J4 2.50 1 02/04/2023 22:57 WG2000336
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.62 1 02/10/2023 14:42 WG2003057
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 02/06/2023 05:12 WG2000530
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 02/07/2023 17:53 WG2001380
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 02/07/2023 11:04 WG2001114
Arsenic 0.0279 B 0.0100 1 02/07/2023 11:04 WG2001114
Beryllium ND 0.00200 1 02/07/2023 11:04 WG2001114
Cadmium ND 0.00200 1 02/07/2023 11:04 WG2001114
Chromium ND 0.0100 1 02/07/2023 11:04 WG2001114
Copper 0.0195 0.0100 1 02/07/2023 11:04 WG2001114
Lead ND 0.00600 1 02/07/2023 11:04 WG2001114
Nickel ND 0.0100 1 02/07/2023 11:04 WG2001114
Selenium ND 0.0100 1 02/07/2023 11:04 WG2001114
Silver ND 0.00500 1 02/07/2023 11:04 WG2001114
Thallium ND 0.0100 1 02/07/2023 11:04 WG2001114
Zinc ND 0.0500 1 02/07/2023 11:04 WG2001114
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 02/09/2023 21:22 WG2003633
(S) a,a,a-Trifluorotoluene(FID) 101 78.0-120 02/09/2023 21:22 WG2003633
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 02/07/2023 02:47 WG2001134
Acrolein ND 0.0500 1 02/07/2023 02:47 WG2001134
Acrylonitrile ND 0.0100 1 02/07/2023 02:47 WG2001134
Benzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Bromobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Bromodichloromethane ND 0.00100 1 02/07/2023 02:47 WG2001134
Bromoform ND 0.00100 1 02/07/2023 02:47 WG2001134
Bromomethane ND 0.00500 1 02/07/2023 02:47 WG2001134
n-Butylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
sec-Butylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
tert-Butylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 16 of 56
SAMPLE RESULTS - 03
L1582319
SW-3
Collected date/time: 02/03/23 12:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 02/07/2023 02:47 WG2001134
Chlorobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Chlorodibromomethane ND 0.00100 1 02/07/2023 02:47 WG2001134
Chloroethane ND 0.00500 1 02/07/2023 02:47 WG2001134
Chloroform ND 0.00500 1 02/07/2023 02:47 WG2001134
Chloromethane ND 0.00250 1 02/07/2023 02:47 WG2001134
2-Chlorotoluene ND 0.00100 1 02/07/2023 02:47 WG2001134
4-Chlorotoluene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2-Dibromo-3-Chloropropane ND 0.00500 1 02/07/2023 02:47 WG2001134
1,2-Dibromoethane ND 0.00100 1 02/07/2023 02:47 WG2001134
Dibromomethane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2-Dichlorobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,3-Dichlorobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,4-Dichlorobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Dichlorodifluoromethane ND 0.00500 1 02/07/2023 02:47 WG2001134
1,1-Dichloroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2-Dichloroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1-Dichloroethene ND 0.00100 1 02/07/2023 02:47 WG2001134
cis-1,2-Dichloroethene ND 0.00100 1 02/07/2023 02:47 WG2001134
trans-1,2-Dichloroethene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2-Dichloropropane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1-Dichloropropene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,3-Dichloropropane ND 0.00100 1 02/07/2023 02:47 WG2001134
cis-1,3-Dichloropropene ND 0.00100 1 02/07/2023 02:47 WG2001134
trans-1,3-Dichloropropene ND 0.00100 1 02/07/2023 02:47 WG2001134
2,2-Dichloropropane ND 0.00100 1 02/07/2023 02:47 WG2001134
Di-isopropyl ether ND 0.00100 1 02/07/2023 02:47 WG2001134
Ethylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Hexachloro-1,3-butadiene ND 0.00100 1 02/07/2023 02:47 WG2001134
Isopropylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
p-Isopropyltoluene ND 0.00100 1 02/07/2023 02:47 WG2001134
2-Butanone (MEK)ND 0.0100 1 02/07/2023 02:47 WG2001134
Methylene Chloride ND 0.00500 1 02/07/2023 02:47 WG2001134
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 02/07/2023 02:47 WG2001134
Methyl tert-butyl ether ND 0.00100 1 02/07/2023 02:47 WG2001134
Naphthalene ND 0.00500 1 02/07/2023 02:47 WG2001134
n-Propylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Styrene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
Tetrachloroethene ND J4 0.00100 1 02/07/2023 02:47 WG2001134
Toluene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2,3-Trichlorobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2,4-Trichlorobenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1,1-Trichloroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
1,1,2-Trichloroethane ND 0.00100 1 02/07/2023 02:47 WG2001134
Trichloroethene ND 0.00100 1 02/07/2023 02:47 WG2001134
Trichlorofluoromethane ND 0.00500 1 02/07/2023 02:47 WG2001134
1,2,3-Trichloropropane ND 0.00250 1 02/07/2023 02:47 WG2001134
1,2,4-Trimethylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,2,3-Trimethylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
1,3,5-Trimethylbenzene ND 0.00100 1 02/07/2023 02:47 WG2001134
Vinyl chloride ND 0.00100 1 02/07/2023 02:47 WG2001134
Xylenes, Total ND 0.00300 1 02/07/2023 02:47 WG2001134
(S) Toluene-d8 109 80.0-120 02/07/2023 02:47 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 17 of 56
SAMPLE RESULTS - 03
L1582319
SW-3
Collected date/time: 02/03/23 12:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 104 77.0-126 02/07/2023 02:47 WG2001134
(S) 1,2-Dichloroethane-d4 98.3 70.0-130 02/07/2023 02:47 WG2001134
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 0.132 0.100 1 02/07/2023 19:50 WG2000565
(S) o-Terphenyl 112 31.0-160 02/07/2023 19:50 WG2000565
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 02/07/2023 01:19 WG2001014
PCB 1221 ND 0.000500 1 02/07/2023 01:19 WG2001014
PCB 1232 ND 0.000500 1 02/07/2023 01:19 WG2001014
PCB 1242 ND 0.000500 1 02/07/2023 01:19 WG2001014
PCB 1248 ND 0.000500 1 02/07/2023 01:19 WG2001014
PCB 1254 ND 0.000500 1 02/07/2023 01:19 WG2001014
PCB 1260 ND 0.000500 1 02/07/2023 01:19 WG2001014
(S) Decachlorobiphenyl 66.8 10.0-128 02/07/2023 01:19 WG2001014
(S) Tetrachloro-m-xylene 60.9 10.0-127 02/07/2023 01:19 WG2001014
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 02/07/2023 13:40 WG2000359
Acenaphthylene ND 0.00100 1 02/07/2023 13:40 WG2000359
Anthracene ND 0.00100 1 02/07/2023 13:40 WG2000359
Benzidine ND J4 0.0100 1 02/07/2023 13:40 WG2000359
Benzo(a)anthracene ND 0.00100 1 02/07/2023 13:40 WG2000359
Benzo(b)fluoranthene ND 0.00100 1 02/07/2023 13:40 WG2000359
Benzo(k)fluoranthene ND 0.00100 1 02/07/2023 13:40 WG2000359
Benzo(g,h,i)perylene ND 0.00100 1 02/07/2023 13:40 WG2000359
Benzo(a)pyrene ND 0.00100 1 02/07/2023 13:40 WG2000359
Bis(2-chlorethoxy)methane ND 0.0100 1 02/07/2023 13:40 WG2000359
Bis(2-chloroethyl)ether ND 0.0100 1 02/07/2023 13:40 WG2000359
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 02/07/2023 13:40 WG2000359
4-Bromophenyl-phenylether ND 0.0100 1 02/07/2023 13:40 WG2000359
2-Chloronaphthalene ND 0.00100 1 02/07/2023 13:40 WG2000359
4-Chlorophenyl-phenylether ND 0.0100 1 02/07/2023 13:40 WG2000359
Chrysene ND 0.00100 1 02/07/2023 13:40 WG2000359
Dibenz(a,h)anthracene ND 0.00100 1 02/07/2023 13:40 WG2000359
1,2-Dichlorobenzene ND 0.0100 1 02/07/2023 13:40 WG2000359
1,3-Dichlorobenzene ND 0.0100 1 02/07/2023 13:40 WG2000359
1,4-Dichlorobenzene ND 0.0100 1 02/07/2023 13:40 WG2000359
3,3-Dichlorobenzidine ND 0.0100 1 02/07/2023 13:40 WG2000359
2,4-Dinitrotoluene ND 0.0100 1 02/07/2023 13:40 WG2000359
2,6-Dinitrotoluene ND 0.0100 1 02/07/2023 13:40 WG2000359
Fluoranthene ND 0.00100 1 02/07/2023 13:40 WG2000359
Fluorene ND 0.00100 1 02/07/2023 13:40 WG2000359
Hexachlorobenzene ND 0.00100 1 02/07/2023 13:40 WG2000359
Hexachloro-1,3-butadiene ND 0.0100 1 02/07/2023 13:40 WG2000359
Hexachlorocyclopentadiene ND 0.0100 1 02/07/2023 13:40 WG2000359
Hexachloroethane ND 0.0100 1 02/07/2023 13:40 WG2000359
Indeno(1,2,3-cd)pyrene ND 0.00100 1 02/07/2023 13:40 WG2000359
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 18 of 56
SAMPLE RESULTS - 03
L1582319
SW-3
Collected date/time: 02/03/23 12:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Isophorone ND 0.0100 1 02/07/2023 13:40 WG2000359
Naphthalene ND 0.00100 1 02/07/2023 13:40 WG2000359
Nitrobenzene ND 0.0100 1 02/07/2023 13:40 WG2000359
n-Nitrosodimethylamine ND 0.0100 1 02/07/2023 13:40 WG2000359
n-Nitrosodiphenylamine ND 0.0100 1 02/07/2023 13:40 WG2000359
n-Nitrosodi-n-propylamine ND 0.0100 1 02/07/2023 13:40 WG2000359
Phenanthrene ND 0.00100 1 02/07/2023 13:40 WG2000359
Benzylbutyl phthalate ND 0.00300 1 02/07/2023 13:40 WG2000359
Bis(2-ethylhexyl)phthalate ND 0.00300 1 02/07/2023 13:40 WG2000359
Di-n-butyl phthalate ND 0.00300 1 02/07/2023 13:40 WG2000359
Diethyl phthalate ND 0.00300 1 02/07/2023 13:40 WG2000359
Dimethyl phthalate ND 0.00300 1 02/07/2023 13:40 WG2000359
Di-n-octyl phthalate ND 0.00300 1 02/07/2023 13:40 WG2000359
Pyrene ND 0.00100 1 02/07/2023 13:40 WG2000359
1,2,4-Trichlorobenzene ND 0.0100 1 02/07/2023 13:40 WG2000359
4-Chloro-3-methylphenol ND 0.0100 1 02/07/2023 13:40 WG2000359
2-Chlorophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
2,4-Dichlorophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
2,4-Dimethylphenol ND 0.0100 1 02/07/2023 13:40 WG2000359
4,6-Dinitro-2-methylphenol ND 0.0100 1 02/07/2023 13:40 WG2000359
2,4-Dinitrophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
2-Nitrophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
4-Nitrophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
Pentachlorophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
Phenol ND 0.0100 1 02/07/2023 13:40 WG2000359
2,4,6-Trichlorophenol ND 0.0100 1 02/07/2023 13:40 WG2000359
(S) 2-Fluorophenol 30.2 10.0-120 02/07/2023 13:40 WG2000359
(S) Phenol-d5 18.1 10.0-120 02/07/2023 13:40 WG2000359
(S) Nitrobenzene-d5 60.7 10.0-127 02/07/2023 13:40 WG2000359
(S) 2-Fluorobiphenyl 66.7 10.0-130 02/07/2023 13:40 WG2000359
(S) 2,4,6-Tribromophenol 60.4 10.0-155 02/07/2023 13:40 WG2000359
(S) p-Terphenyl-d14 74.7 10.0-128 02/07/2023 13:40 WG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Acenaphthene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Acenaphthylene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Benzo(a)anthracene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Benzo(a)pyrene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Benzo(b)fluoranthene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Benzo(g,h,i)perylene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Benzo(k)fluoranthene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Chrysene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Dibenz(a,h)anthracene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Fluoranthene ND 0.000100 1 02/06/2023 23:39 WG2000383
Fluorene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Naphthalene ND 0.000250 1 02/06/2023 23:39 WG2000383
Phenanthrene ND 0.0000500 1 02/06/2023 23:39 WG2000383
Pyrene ND 0.0000500 1 02/06/2023 23:39 WG2000383
1-Methylnaphthalene ND 0.000250 1 02/06/2023 23:39 WG2000383
2-Methylnaphthalene ND 0.000250 1 02/06/2023 23:39 WG2000383
2-Chloronaphthalene ND 0.000250 1 02/06/2023 23:39 WG2000383
(S) Nitrobenzene-d5 99.5 31.0-160 02/06/2023 23:39 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 19 of 56
SAMPLE RESULTS - 03
L1582319
SW-3
Collected date/time: 02/03/23 12:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorobiphenyl 94.2 48.0-148 02/06/2023 23:39 WG2000383
(S) p-Terphenyl-d14 103 37.0-146 02/06/2023 23:39 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT L1582319 02/13/23 16:56 20 of 56
SAMPLE RESULTS - 04
L1582319
SW-4
Collected date/time: 02/03/23 14:30
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids 32.0 J4 2.75 1 02/04/2023 22:57 WG2000336
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.67 1 02/10/2023 14:42 WG2003057
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.00269 0.000500 1 02/06/2023 05:19 WG2000530
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 02/07/2023 18:09 WG2001380
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 02/07/2023 11:07 WG2001114
Arsenic 0.0651 0.0100 1 02/07/2023 11:07 WG2001114
Beryllium ND 0.00200 1 02/07/2023 11:07 WG2001114
Cadmium ND 0.00200 1 02/07/2023 11:07 WG2001114
Chromium ND 0.0100 1 02/07/2023 11:07 WG2001114
Copper ND 0.0100 1 02/07/2023 11:07 WG2001114
Lead ND 0.00600 1 02/07/2023 11:07 WG2001114
Nickel ND 0.0100 1 02/07/2023 11:07 WG2001114
Selenium ND 0.0100 1 02/07/2023 11:07 WG2001114
Silver ND 0.00500 1 02/07/2023 11:07 WG2001114
Thallium ND 0.0100 1 02/07/2023 11:07 WG2001114
Zinc ND 0.0500 1 02/07/2023 11:07 WG2001114
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 02/09/2023 21:44 WG2003633
(S) a,a,a-Trifluorotoluene(FID) 102 78.0-120 02/09/2023 21:44 WG2003633
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 02/07/2023 03:08 WG2001134
Acrolein ND 0.0500 1 02/07/2023 03:08 WG2001134
Acrylonitrile ND 0.0100 1 02/07/2023 03:08 WG2001134
Benzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Bromobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Bromodichloromethane ND 0.00100 1 02/07/2023 03:08 WG2001134
Bromoform ND 0.00100 1 02/07/2023 03:08 WG2001134
Bromomethane ND 0.00500 1 02/07/2023 03:08 WG2001134
n-Butylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
sec-Butylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
tert-Butylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1582319
SW-4
Collected date/time: 02/03/23 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 02/07/2023 03:08 WG2001134
Chlorobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Chlorodibromomethane ND 0.00100 1 02/07/2023 03:08 WG2001134
Chloroethane ND 0.00500 1 02/07/2023 03:08 WG2001134
Chloroform ND 0.00500 1 02/07/2023 03:08 WG2001134
Chloromethane ND 0.00250 1 02/07/2023 03:08 WG2001134
2-Chlorotoluene ND 0.00100 1 02/07/2023 03:08 WG2001134
4-Chlorotoluene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2-Dibromo-3-Chloropropane ND 0.00500 1 02/07/2023 03:08 WG2001134
1,2-Dibromoethane ND 0.00100 1 02/07/2023 03:08 WG2001134
Dibromomethane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2-Dichlorobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,3-Dichlorobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,4-Dichlorobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Dichlorodifluoromethane ND 0.00500 1 02/07/2023 03:08 WG2001134
1,1-Dichloroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2-Dichloroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1-Dichloroethene ND 0.00100 1 02/07/2023 03:08 WG2001134
cis-1,2-Dichloroethene ND 0.00100 1 02/07/2023 03:08 WG2001134
trans-1,2-Dichloroethene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2-Dichloropropane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1-Dichloropropene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,3-Dichloropropane ND 0.00100 1 02/07/2023 03:08 WG2001134
cis-1,3-Dichloropropene ND 0.00100 1 02/07/2023 03:08 WG2001134
trans-1,3-Dichloropropene ND 0.00100 1 02/07/2023 03:08 WG2001134
2,2-Dichloropropane ND 0.00100 1 02/07/2023 03:08 WG2001134
Di-isopropyl ether ND 0.00100 1 02/07/2023 03:08 WG2001134
Ethylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Hexachloro-1,3-butadiene ND 0.00100 1 02/07/2023 03:08 WG2001134
Isopropylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
p-Isopropyltoluene ND 0.00100 1 02/07/2023 03:08 WG2001134
2-Butanone (MEK)ND 0.0100 1 02/07/2023 03:08 WG2001134
Methylene Chloride ND 0.00500 1 02/07/2023 03:08 WG2001134
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 02/07/2023 03:08 WG2001134
Methyl tert-butyl ether ND 0.00100 1 02/07/2023 03:08 WG2001134
Naphthalene ND 0.00500 1 02/07/2023 03:08 WG2001134
n-Propylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Styrene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
Tetrachloroethene ND J4 0.00100 1 02/07/2023 03:08 WG2001134
Toluene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2,3-Trichlorobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2,4-Trichlorobenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1,1-Trichloroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
1,1,2-Trichloroethane ND 0.00100 1 02/07/2023 03:08 WG2001134
Trichloroethene ND 0.00100 1 02/07/2023 03:08 WG2001134
Trichlorofluoromethane ND 0.00500 1 02/07/2023 03:08 WG2001134
1,2,3-Trichloropropane ND 0.00250 1 02/07/2023 03:08 WG2001134
1,2,4-Trimethylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,2,3-Trimethylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
1,3,5-Trimethylbenzene ND 0.00100 1 02/07/2023 03:08 WG2001134
Vinyl chloride ND 0.00100 1 02/07/2023 03:08 WG2001134
Xylenes, Total ND 0.00300 1 02/07/2023 03:08 WG2001134
(S) Toluene-d8 110 80.0-120 02/07/2023 03:08 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1582319
SW-4
Collected date/time: 02/03/23 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 88.1 77.0-126 02/07/2023 03:08 WG2001134
(S) 1,2-Dichloroethane-d4 95.8 70.0-130 02/07/2023 03:08 WG2001134
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction ND 0.100 1 02/08/2023 00:23 WG2000565
(S) o-Terphenyl 106 31.0-160 02/08/2023 00:23 WG2000565
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 02/07/2023 01:30 WG2001014
PCB 1221 ND 0.000500 1 02/07/2023 01:30 WG2001014
PCB 1232 ND 0.000500 1 02/07/2023 01:30 WG2001014
PCB 1242 ND 0.000500 1 02/07/2023 01:30 WG2001014
PCB 1248 ND 0.000500 1 02/07/2023 01:30 WG2001014
PCB 1254 ND 0.000500 1 02/07/2023 01:30 WG2001014
PCB 1260 ND 0.000500 1 02/07/2023 01:30 WG2001014
(S) Decachlorobiphenyl 68.0 10.0-128 02/07/2023 01:30 WG2001014
(S) Tetrachloro-m-xylene 68.3 10.0-127 02/07/2023 01:30 WG2001014
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 02/07/2023 14:02 WG2000359
Acenaphthylene ND 0.00100 1 02/07/2023 14:02 WG2000359
Anthracene ND 0.00100 1 02/07/2023 14:02 WG2000359
Benzidine ND J4 0.0100 1 02/07/2023 14:02 WG2000359
Benzo(a)anthracene ND 0.00100 1 02/07/2023 14:02 WG2000359
Benzo(b)fluoranthene ND 0.00100 1 02/07/2023 14:02 WG2000359
Benzo(k)fluoranthene ND 0.00100 1 02/07/2023 14:02 WG2000359
Benzo(g,h,i)perylene ND 0.00100 1 02/07/2023 14:02 WG2000359
Benzo(a)pyrene ND 0.00100 1 02/07/2023 14:02 WG2000359
Bis(2-chlorethoxy)methane ND 0.0100 1 02/07/2023 14:02 WG2000359
Bis(2-chloroethyl)ether ND 0.0100 1 02/07/2023 14:02 WG2000359
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 02/07/2023 14:02 WG2000359
4-Bromophenyl-phenylether ND 0.0100 1 02/07/2023 14:02 WG2000359
2-Chloronaphthalene ND 0.00100 1 02/07/2023 14:02 WG2000359
4-Chlorophenyl-phenylether ND 0.0100 1 02/07/2023 14:02 WG2000359
Chrysene ND 0.00100 1 02/07/2023 14:02 WG2000359
Dibenz(a,h)anthracene ND 0.00100 1 02/07/2023 14:02 WG2000359
1,2-Dichlorobenzene ND 0.0100 1 02/07/2023 14:02 WG2000359
1,3-Dichlorobenzene ND 0.0100 1 02/07/2023 14:02 WG2000359
1,4-Dichlorobenzene ND 0.0100 1 02/07/2023 14:02 WG2000359
3,3-Dichlorobenzidine ND 0.0100 1 02/07/2023 14:02 WG2000359
2,4-Dinitrotoluene ND 0.0100 1 02/07/2023 14:02 WG2000359
2,6-Dinitrotoluene ND 0.0100 1 02/07/2023 14:02 WG2000359
Fluoranthene ND 0.00100 1 02/07/2023 14:02 WG2000359
Fluorene ND 0.00100 1 02/07/2023 14:02 WG2000359
Hexachlorobenzene ND 0.00100 1 02/07/2023 14:02 WG2000359
Hexachloro-1,3-butadiene ND 0.0100 1 02/07/2023 14:02 WG2000359
Hexachlorocyclopentadiene ND 0.0100 1 02/07/2023 14:02 WG2000359
Hexachloroethane ND 0.0100 1 02/07/2023 14:02 WG2000359
Indeno(1,2,3-cd)pyrene ND 0.00100 1 02/07/2023 14:02 WG2000359
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1582319
SW-4
Collected date/time: 02/03/23 14:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Isophorone ND 0.0100 1 02/07/2023 14:02 WG2000359
Naphthalene ND 0.00100 1 02/07/2023 14:02 WG2000359
Nitrobenzene ND 0.0100 1 02/07/2023 14:02 WG2000359
n-Nitrosodimethylamine ND 0.0100 1 02/07/2023 14:02 WG2000359
n-Nitrosodiphenylamine ND 0.0100 1 02/07/2023 14:02 WG2000359
n-Nitrosodi-n-propylamine ND 0.0100 1 02/07/2023 14:02 WG2000359
Phenanthrene ND 0.00100 1 02/07/2023 14:02 WG2000359
Benzylbutyl phthalate ND 0.00300 1 02/07/2023 14:02 WG2000359
Bis(2-ethylhexyl)phthalate ND 0.00300 1 02/07/2023 14:02 WG2000359
Di-n-butyl phthalate ND 0.00300 1 02/07/2023 14:02 WG2000359
Diethyl phthalate ND 0.00300 1 02/07/2023 14:02 WG2000359
Dimethyl phthalate ND 0.00300 1 02/07/2023 14:02 WG2000359
Di-n-octyl phthalate ND 0.00300 1 02/07/2023 14:02 WG2000359
Pyrene ND 0.00100 1 02/07/2023 14:02 WG2000359
1,2,4-Trichlorobenzene ND 0.0100 1 02/07/2023 14:02 WG2000359
4-Chloro-3-methylphenol ND 0.0100 1 02/07/2023 14:02 WG2000359
2-Chlorophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
2,4-Dichlorophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
2,4-Dimethylphenol ND 0.0100 1 02/07/2023 14:02 WG2000359
4,6-Dinitro-2-methylphenol ND 0.0100 1 02/07/2023 14:02 WG2000359
2,4-Dinitrophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
2-Nitrophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
4-Nitrophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
Pentachlorophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
Phenol ND 0.0100 1 02/07/2023 14:02 WG2000359
2,4,6-Trichlorophenol ND 0.0100 1 02/07/2023 14:02 WG2000359
(S) 2-Fluorophenol 29.7 10.0-120 02/07/2023 14:02 WG2000359
(S) Phenol-d5 17.8 10.0-120 02/07/2023 14:02 WG2000359
(S) Nitrobenzene-d5 52.9 10.0-127 02/07/2023 14:02 WG2000359
(S) 2-Fluorobiphenyl 60.9 10.0-130 02/07/2023 14:02 WG2000359
(S) 2,4,6-Tribromophenol 58.5 10.0-155 02/07/2023 14:02 WG2000359
(S) p-Terphenyl-d14 70.6 10.0-128 02/07/2023 14:02 WG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Acenaphthene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Acenaphthylene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Benzo(a)anthracene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Benzo(a)pyrene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Benzo(b)fluoranthene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Benzo(g,h,i)perylene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Benzo(k)fluoranthene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Chrysene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Dibenz(a,h)anthracene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Fluoranthene ND 0.000100 1 02/06/2023 23:57 WG2000383
Fluorene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Naphthalene ND 0.000250 1 02/06/2023 23:57 WG2000383
Phenanthrene ND 0.0000500 1 02/06/2023 23:57 WG2000383
Pyrene ND 0.0000500 1 02/06/2023 23:57 WG2000383
1-Methylnaphthalene ND 0.000250 1 02/06/2023 23:57 WG2000383
2-Methylnaphthalene ND 0.000250 1 02/06/2023 23:57 WG2000383
2-Chloronaphthalene ND 0.000250 1 02/06/2023 23:57 WG2000383
(S) Nitrobenzene-d5 94.2 31.0-160 02/06/2023 23:57 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1582319
SW-4
Collected date/time: 02/03/23 14:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorobiphenyl 89.5 48.0-148 02/06/2023 23:57 WG2000383
(S) p-Terphenyl-d14 102 37.0-146 02/06/2023 23:57 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1582319
SW-5
Collected date/time: 02/03/23 15:30
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Suspended Solids ND J4 2.50 1 02/04/2023 22:57 WG2000336
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.02 1 02/10/2023 14:42 WG2003057
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 02/06/2023 05:27 WG2000530
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 02/07/2023 18:11 WG2001380
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 02/07/2023 13:19 WG2001119
Arsenic 0.0522 0.0100 1 02/07/2023 13:19 WG2001119
Beryllium ND 0.00200 1 02/07/2023 13:19 WG2001119
Cadmium ND 0.00200 1 02/07/2023 13:19 WG2001119
Chromium ND 0.0100 1 02/07/2023 13:19 WG2001119
Copper ND 0.0100 1 02/07/2023 13:19 WG2001119
Lead ND 0.00600 1 02/07/2023 13:19 WG2001119
Nickel ND 0.0100 1 02/07/2023 13:19 WG2001119
Selenium ND 0.0100 1 02/07/2023 13:19 WG2001119
Silver ND 0.00500 1 02/07/2023 13:19 WG2001119
Thallium ND 0.0100 1 02/07/2023 13:19 WG2001119
Zinc ND 0.0500 1 02/07/2023 13:19 WG2001119
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 02/09/2023 22:06 WG2003633
(S) a,a,a-Trifluorotoluene(FID) 102 78.0-120 02/09/2023 22:06 WG2003633
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 02/07/2023 03:31 WG2001134
Acrolein ND 0.0500 1 02/07/2023 03:31 WG2001134
Acrylonitrile ND 0.0100 1 02/07/2023 03:31 WG2001134
Benzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Bromobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Bromodichloromethane ND 0.00100 1 02/07/2023 03:31 WG2001134
Bromoform ND 0.00100 1 02/07/2023 03:31 WG2001134
Bromomethane ND 0.00500 1 02/07/2023 03:31 WG2001134
n-Butylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
sec-Butylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
tert-Butylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1582319
SW-5
Collected date/time: 02/03/23 15:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 02/07/2023 03:31 WG2001134
Chlorobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Chlorodibromomethane ND 0.00100 1 02/07/2023 03:31 WG2001134
Chloroethane ND 0.00500 1 02/07/2023 03:31 WG2001134
Chloroform ND 0.00500 1 02/07/2023 03:31 WG2001134
Chloromethane ND 0.00250 1 02/07/2023 03:31 WG2001134
2-Chlorotoluene ND 0.00100 1 02/07/2023 03:31 WG2001134
4-Chlorotoluene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2-Dibromo-3-Chloropropane ND 0.00500 1 02/07/2023 03:31 WG2001134
1,2-Dibromoethane ND 0.00100 1 02/07/2023 03:31 WG2001134
Dibromomethane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2-Dichlorobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,3-Dichlorobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,4-Dichlorobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Dichlorodifluoromethane ND 0.00500 1 02/07/2023 03:31 WG2001134
1,1-Dichloroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2-Dichloroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1-Dichloroethene ND 0.00100 1 02/07/2023 03:31 WG2001134
cis-1,2-Dichloroethene 0.00209 0.00100 1 02/07/2023 03:31 WG2001134
trans-1,2-Dichloroethene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2-Dichloropropane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1-Dichloropropene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,3-Dichloropropane ND 0.00100 1 02/07/2023 03:31 WG2001134
cis-1,3-Dichloropropene ND 0.00100 1 02/07/2023 03:31 WG2001134
trans-1,3-Dichloropropene ND 0.00100 1 02/07/2023 03:31 WG2001134
2,2-Dichloropropane ND 0.00100 1 02/07/2023 03:31 WG2001134
Di-isopropyl ether ND 0.00100 1 02/07/2023 03:31 WG2001134
Ethylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Hexachloro-1,3-butadiene ND 0.00100 1 02/07/2023 03:31 WG2001134
Isopropylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
p-Isopropyltoluene ND 0.00100 1 02/07/2023 03:31 WG2001134
2-Butanone (MEK)ND 0.0100 1 02/07/2023 03:31 WG2001134
Methylene Chloride ND 0.00500 1 02/07/2023 03:31 WG2001134
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 02/07/2023 03:31 WG2001134
Methyl tert-butyl ether ND 0.00100 1 02/07/2023 03:31 WG2001134
Naphthalene ND 0.00500 1 02/07/2023 03:31 WG2001134
n-Propylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Styrene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
Tetrachloroethene ND J4 0.00100 1 02/07/2023 03:31 WG2001134
Toluene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2,3-Trichlorobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2,4-Trichlorobenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1,1-Trichloroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
1,1,2-Trichloroethane ND 0.00100 1 02/07/2023 03:31 WG2001134
Trichloroethene 0.00268 0.00100 1 02/07/2023 03:31 WG2001134
Trichlorofluoromethane ND 0.00500 1 02/07/2023 03:31 WG2001134
1,2,3-Trichloropropane ND 0.00250 1 02/07/2023 03:31 WG2001134
1,2,4-Trimethylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,2,3-Trimethylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
1,3,5-Trimethylbenzene ND 0.00100 1 02/07/2023 03:31 WG2001134
Vinyl chloride ND 0.00100 1 02/07/2023 03:31 WG2001134
Xylenes, Total ND 0.00300 1 02/07/2023 03:31 WG2001134
(S) Toluene-d8 110 80.0-120 02/07/2023 03:31 WG2001134
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1582319
SW-5
Collected date/time: 02/03/23 15:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 88.5 77.0-126 02/07/2023 03:31 WG2001134
(S) 1,2-Dichloroethane-d4 97.7 70.0-130 02/07/2023 03:31 WG2001134
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction ND 0.100 1 02/07/2023 20:30 WG2000565
(S) o-Terphenyl 103 31.0-160 02/07/2023 20:30 WG2000565
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 02/07/2023 01:40 WG2001014
PCB 1221 ND 0.000500 1 02/07/2023 01:40 WG2001014
PCB 1232 ND 0.000500 1 02/07/2023 01:40 WG2001014
PCB 1242 ND 0.000500 1 02/07/2023 01:40 WG2001014
PCB 1248 ND 0.000500 1 02/07/2023 01:40 WG2001014
PCB 1254 ND 0.000500 1 02/07/2023 01:40 WG2001014
PCB 1260 ND 0.000500 1 02/07/2023 01:40 WG2001014
(S) Decachlorobiphenyl 74.0 10.0-128 02/07/2023 01:40 WG2001014
(S) Tetrachloro-m-xylene 65.4 10.0-127 02/07/2023 01:40 WG2001014
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 02/07/2023 14:23 WG2000359
Acenaphthylene ND 0.00100 1 02/07/2023 14:23 WG2000359
Anthracene ND 0.00100 1 02/07/2023 14:23 WG2000359
Benzidine ND J4 0.0100 1 02/07/2023 14:23 WG2000359
Benzo(a)anthracene ND 0.00100 1 02/07/2023 14:23 WG2000359
Benzo(b)fluoranthene ND 0.00100 1 02/07/2023 14:23 WG2000359
Benzo(k)fluoranthene ND 0.00100 1 02/07/2023 14:23 WG2000359
Benzo(g,h,i)perylene ND 0.00100 1 02/07/2023 14:23 WG2000359
Benzo(a)pyrene ND 0.00100 1 02/07/2023 14:23 WG2000359
Bis(2-chlorethoxy)methane ND 0.0100 1 02/07/2023 14:23 WG2000359
Bis(2-chloroethyl)ether ND 0.0100 1 02/07/2023 14:23 WG2000359
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 02/07/2023 14:23 WG2000359
4-Bromophenyl-phenylether ND 0.0100 1 02/07/2023 14:23 WG2000359
2-Chloronaphthalene ND 0.00100 1 02/07/2023 14:23 WG2000359
4-Chlorophenyl-phenylether ND 0.0100 1 02/07/2023 14:23 WG2000359
Chrysene ND 0.00100 1 02/07/2023 14:23 WG2000359
Dibenz(a,h)anthracene ND 0.00100 1 02/07/2023 14:23 WG2000359
1,2-Dichlorobenzene ND 0.0100 1 02/07/2023 14:23 WG2000359
1,3-Dichlorobenzene ND 0.0100 1 02/07/2023 14:23 WG2000359
1,4-Dichlorobenzene ND 0.0100 1 02/07/2023 14:23 WG2000359
3,3-Dichlorobenzidine ND 0.0100 1 02/07/2023 14:23 WG2000359
2,4-Dinitrotoluene ND 0.0100 1 02/07/2023 14:23 WG2000359
2,6-Dinitrotoluene ND 0.0100 1 02/07/2023 14:23 WG2000359
Fluoranthene ND 0.00100 1 02/07/2023 14:23 WG2000359
Fluorene ND 0.00100 1 02/07/2023 14:23 WG2000359
Hexachlorobenzene ND 0.00100 1 02/07/2023 14:23 WG2000359
Hexachloro-1,3-butadiene ND 0.0100 1 02/07/2023 14:23 WG2000359
Hexachlorocyclopentadiene ND 0.0100 1 02/07/2023 14:23 WG2000359
Hexachloroethane ND 0.0100 1 02/07/2023 14:23 WG2000359
Indeno(1,2,3-cd)pyrene ND 0.00100 1 02/07/2023 14:23 WG2000359
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1582319
SW-5
Collected date/time: 02/03/23 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Isophorone ND 0.0100 1 02/07/2023 14:23 WG2000359
Naphthalene ND 0.00100 1 02/07/2023 14:23 WG2000359
Nitrobenzene ND 0.0100 1 02/07/2023 14:23 WG2000359
n-Nitrosodimethylamine ND 0.0100 1 02/07/2023 14:23 WG2000359
n-Nitrosodiphenylamine ND 0.0100 1 02/07/2023 14:23 WG2000359
n-Nitrosodi-n-propylamine ND 0.0100 1 02/07/2023 14:23 WG2000359
Phenanthrene ND 0.00100 1 02/07/2023 14:23 WG2000359
Benzylbutyl phthalate ND 0.00300 1 02/07/2023 14:23 WG2000359
Bis(2-ethylhexyl)phthalate ND 0.00300 1 02/07/2023 14:23 WG2000359
Di-n-butyl phthalate ND 0.00300 1 02/07/2023 14:23 WG2000359
Diethyl phthalate ND 0.00300 1 02/07/2023 14:23 WG2000359
Dimethyl phthalate ND 0.00300 1 02/07/2023 14:23 WG2000359
Di-n-octyl phthalate ND 0.00300 1 02/07/2023 14:23 WG2000359
Pyrene ND 0.00100 1 02/07/2023 14:23 WG2000359
1,2,4-Trichlorobenzene ND 0.0100 1 02/07/2023 14:23 WG2000359
4-Chloro-3-methylphenol ND 0.0100 1 02/07/2023 14:23 WG2000359
2-Chlorophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
2,4-Dichlorophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
2,4-Dimethylphenol ND 0.0100 1 02/07/2023 14:23 WG2000359
4,6-Dinitro-2-methylphenol ND 0.0100 1 02/07/2023 14:23 WG2000359
2,4-Dinitrophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
2-Nitrophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
4-Nitrophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
Pentachlorophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
Phenol ND 0.0100 1 02/07/2023 14:23 WG2000359
2,4,6-Trichlorophenol ND 0.0100 1 02/07/2023 14:23 WG2000359
(S) 2-Fluorophenol 26.8 10.0-120 02/07/2023 14:23 WG2000359
(S) Phenol-d5 16.2 10.0-120 02/07/2023 14:23 WG2000359
(S) Nitrobenzene-d5 47.9 10.0-127 02/07/2023 14:23 WG2000359
(S) 2-Fluorobiphenyl 54.7 10.0-130 02/07/2023 14:23 WG2000359
(S) 2,4,6-Tribromophenol 52.0 10.0-155 02/07/2023 14:23 WG2000359
(S) p-Terphenyl-d14 63.0 10.0-128 02/07/2023 14:23 WG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Acenaphthene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Acenaphthylene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Benzo(a)anthracene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Benzo(a)pyrene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Benzo(b)fluoranthene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Benzo(g,h,i)perylene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Benzo(k)fluoranthene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Chrysene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Dibenz(a,h)anthracene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Fluoranthene ND 0.000100 1 02/07/2023 00:14 WG2000383
Fluorene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Naphthalene ND 0.000250 1 02/07/2023 00:14 WG2000383
Phenanthrene ND 0.0000500 1 02/07/2023 00:14 WG2000383
Pyrene ND 0.0000500 1 02/07/2023 00:14 WG2000383
1-Methylnaphthalene ND 0.000250 1 02/07/2023 00:14 WG2000383
2-Methylnaphthalene ND 0.000250 1 02/07/2023 00:14 WG2000383
2-Chloronaphthalene ND 0.000250 1 02/07/2023 00:14 WG2000383
(S) Nitrobenzene-d5 95.8 31.0-160 02/07/2023 00:14 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1582319
SW-5
Collected date/time: 02/03/23 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorobiphenyl 92.6 48.0-148 02/07/2023 00:14 WG2000383
(S) p-Terphenyl-d14 111 37.0-146 02/07/2023 00:14 WG2000383
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2000336
Gravimetric Analysis by Method 2540 D-2015 L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3887691-1 02/04/23 22:57
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Suspended Solids U 2.50 2.50
L1582242-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1582242-01 02/04/23 22:57 • (DUP) R3887691-3 02/04/23 22:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Suspended Solids 138 154 1 11.0 J3 5
L1582323-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1582323-01 02/04/23 22:57 • (DUP) R3887691-4 02/04/23 22:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Suspended Solids 49.2 48.8 1 0.816 5
Laboratory Control Sample (LCS)
(LCS) R3887691-2 02/04/23 22:57
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Suspended Solids 773 652 84.3 85.7-114 J4
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2003057
Wet Chemistry by Method 1664A L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3889629-1 02/10/23 14:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3889629-2 02/10/23 14:42 • (LCSD) R3889629-3 02/10/23 14:42
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 33.8 31.8 84.5 79.5 78.0-114 6.10 20
L1582226-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1582226-01 02/10/23 14:42 • (MS) R3889629-4 02/10/23 14:42
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr) 40.0 ND 48.4 111 1 78.0-114
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2000530
Wet Chemistry by Method 3500Cr C-2011 L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3887699-1 02/06/23 01:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Hexavalent Chromium U 0.000150 0.000500
L1580855-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1580855-01 02/06/23 02:13 • (DUP) R3887699-3 02/06/23 02:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND ND 1 0.000 20
L1582167-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1582167-01 02/06/23 04:10 • (DUP) R3887699-4 02/06/23 04:18
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3887699-2 02/06/23 02:02
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00200 0.00212 106 90.0-110
L1582319-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582319-02 02/06/23 04:33 • (MS) R3887699-5 02/06/23 04:41 • (MSD) R3887699-6 02/06/23 05:04
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexavalent Chromium 0.0500 0.000554 0.0508 0.0508 100 100 1 90.0-110 0.0162 20
L1580855-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1580855-02 02/06/23 02:30 • (MS) R3887699-7 02/06/23 06:47
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Hexavalent Chromium 0.0500 ND 0.0504 100 1 90.0-110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2001380
Mercury by Method 7470A L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888398-1 02/07/23 17:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3888398-2 02/07/23 17:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00285 95.0 80.0-120
L1582319-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582319-03 02/07/23 17:53 • (MS) R3888398-3 02/07/23 17:55 • (MSD) R3888398-4 02/07/23 17:58
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00276 0.00277 92.0 92.3 1 75.0-125 0.362 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2001114
Metals (ICP) by Method 6010B L1582319-01,02,03,04
Method Blank (MB)
(MB) R3888254-1 02/07/23 09:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic 0.00518 J 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3888254-2 02/07/23 10:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.951 95.1 80.0-120
Arsenic 1.00 0.923 92.3 80.0-120
Beryllium 1.00 0.966 96.6 80.0-120
Cadmium 1.00 0.953 95.3 80.0-120
Chromium 1.00 0.938 93.8 80.0-120
Copper 1.00 0.973 97.3 80.0-120
Lead 1.00 0.954 95.4 80.0-120
Nickel 1.00 0.954 95.4 80.0-120
Selenium 1.00 0.923 92.3 80.0-120
Silver 0.200 0.186 92.9 80.0-120
Thallium 1.00 0.953 95.3 80.0-120
Zinc 1.00 0.960 96.0 80.0-120
L1581929-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1581929-01 02/07/23 10:03 • (MS) R3888254-4 02/07/23 10:08 • (MSD) R3888254-5 02/07/23 10:11
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 0.994 0.968 99.4 96.8 1 75.0-125 2.72 20
Arsenic 1.00 0.256 1.22 1.19 96.3 93.8 1 75.0-125 2.07 20
Beryllium 1.00 ND 0.963 0.931 96.3 93.1 1 75.0-125 3.35 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001114
Metals (ICP) by Method 6010B L1582319-01,02,03,04
L1581929-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1581929-01 02/07/23 10:03 • (MS) R3888254-4 02/07/23 10:08 • (MSD) R3888254-5 02/07/23 10:11
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Cadmium 1.00 ND 0.987 0.962 98.7 96.2 1 75.0-125 2.52 20
Chromium 1.00 ND 0.937 0.907 93.6 90.5 1 75.0-125 3.31 20
Copper 1.00 0.0615 1.07 1.03 100 96.9 1 75.0-125 3.31 20
Lead 1.00 0.0148 0.988 0.957 97.4 94.2 1 75.0-125 3.27 20
Nickel 1.00 0.378 1.34 1.31 95.8 92.9 1 75.0-125 2.21 20
Selenium 1.00 ND 0.979 0.957 97.9 95.7 1 75.0-125 2.25 20
Silver 0.200 ND 0.192 0.186 96.1 93.2 1 75.0-125 3.10 20
Thallium 1.00 ND 0.969 0.933 96.9 93.3 1 75.0-125 3.78 20
Zinc 1.00 0.352 1.29 1.26 94.0 91.3 1 75.0-125 2.15 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001119
Metals (ICP) by Method 6010B L1582319-05
Method Blank (MB)
(MB) R3888297-1 02/07/23 13:03
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic U 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3888297-2 02/07/23 13:06
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.961 96.1 80.0-120
Arsenic 1.00 0.940 94.0 80.0-120
Beryllium 1.00 1.01 101 80.0-120
Cadmium 1.00 0.964 96.4 80.0-120
Chromium 1.00 0.953 95.3 80.0-120
Copper 1.00 0.968 96.8 80.0-120
Lead 1.00 0.950 95.0 80.0-120
Nickel 1.00 0.961 96.1 80.0-120
Selenium 1.00 0.950 95.0 80.0-120
Silver 0.200 0.187 93.3 80.0-120
Thallium 1.00 0.968 96.8 80.0-120
Zinc 1.00 0.911 91.1 80.0-120
L1582336-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582336-01 02/07/23 13:09 • (MS) R3888297-4 02/07/23 13:14 • (MSD) R3888297-5 02/07/23 13:16
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 0.965 0.973 96.5 97.3 1 75.0-125 0.865 20
Arsenic 1.00 ND 0.945 0.944 94.0 93.9 1 75.0-125 0.168 20
Beryllium 1.00 ND 1.00 0.993 100 99.3 1 75.0-125 0.728 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001119
Metals (ICP) by Method 6010B L1582319-05
L1582336-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582336-01 02/07/23 13:09 • (MS) R3888297-4 02/07/23 13:14 • (MSD) R3888297-5 02/07/23 13:16
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Cadmium 1.00 ND 0.965 0.965 96.5 96.5 1 75.0-125 0.0480 20
Chromium 1.00 ND 0.943 0.940 94.3 94.0 1 75.0-125 0.322 20
Copper 1.00 ND 0.966 0.962 96.0 95.6 1 75.0-125 0.443 20
Lead 1.00 ND 0.946 0.943 94.6 94.3 1 75.0-125 0.294 20
Nickel 1.00 ND 0.965 0.966 96.5 96.6 1 75.0-125 0.0355 20
Selenium 1.00 ND 0.962 0.965 96.2 96.5 1 75.0-125 0.294 20
Silver 0.200 ND 0.187 0.185 93.3 92.4 1 75.0-125 1.01 20
Thallium 1.00 ND 0.960 0.944 95.5 93.9 1 75.0-125 1.75 20
Zinc 1.00 ND 0.942 0.946 91.4 91.8 1 75.0-125 0.453 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2003633
Volatile Organic Compounds (GC) by Method 8015D/GRO L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3889743-3 02/09/23 11:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 0.0432 J 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)101 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3889743-2 02/09/23 10:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.52 100 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 105 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001134
Volatile Organic Compounds (GC/MS) by Method 8260B L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888119-2 02/06/23 17:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromobenzene U 0.000118 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-Butylbenzene U 0.000125 0.00100
tert-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
2-Chlorotoluene U 0.000106 0.00100
4-Chlorotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
cis-1,2-Dichloroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
1,1-Dichloropropene U 0.000142 0.00100
1,3-Dichloropropane U 0.000110 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
2,2-Dichloropropane U 0.000161 0.00100
Di-isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Hexachloro-1,3-butadiene U 0.000337 0.00100
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001134
Volatile Organic Compounds (GC/MS) by Method 8260B L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888119-2 02/06/23 17:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Isopropylbenzene U 0.000105 0.00100
p-Isopropyltoluene U 0.000120 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK) U 0.000478 0.0100
Methyl tert-butyl ether U 0.000101 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100
1,1,1,2-Tetrachloroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene U 0.000230 0.00100
1,2,4-Trichlorobenzene U 0.000481 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,2,3-Trichloropropane U 0.000237 0.00250
1,2,4-Trimethylbenzene U 0.000322 0.00100
1,2,3-Trimethylbenzene U 0.000104 0.00100
1,3,5-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 87.1 77.0-126
(S) 1,2-Dichloroethane-d4 95.1 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3888119-1 02/06/23 16:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acetone 0.0250 0.0230 92.0 19.0-160
Acrolein 0.0250 0.00934 37.4 10.0-160
Acrylonitrile 0.0250 0.0218 87.2 55.0-149
Benzene 0.00500 0.00525 105 70.0-123
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001134
Volatile Organic Compounds (GC/MS) by Method 8260B L1582319-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3888119-1 02/06/23 16:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Bromobenzene 0.00500 0.00413 82.6 73.0-121
Bromodichloromethane 0.00500 0.00482 96.4 75.0-120
Bromoform 0.00500 0.00584 117 68.0-132
Bromomethane 0.00500 0.00665 133 10.0-160
n-Butylbenzene 0.00500 0.00438 87.6 73.0-125
sec-Butylbenzene 0.00500 0.00437 87.4 75.0-125
tert-Butylbenzene 0.00500 0.00438 87.6 76.0-124
Carbon tetrachloride 0.00500 0.00565 113 68.0-126
Chlorobenzene 0.00500 0.00594 119 80.0-121
Chlorodibromomethane 0.00500 0.00627 125 77.0-125
Chloroethane 0.00500 0.00658 132 47.0-150
Chloroform 0.00500 0.00496 99.2 73.0-120
Chloromethane 0.00500 0.00496 99.2 41.0-142
2-Chlorotoluene 0.00500 0.00449 89.8 76.0-123
4-Chlorotoluene 0.00500 0.00418 83.6 75.0-122
1,2-Dibromo-3-Chloropropane 0.00500 0.00424 84.8 58.0-134
1,2-Dibromoethane 0.00500 0.00551 110 80.0-122
Dibromomethane 0.00500 0.00538 108 80.0-120
1,2-Dichlorobenzene 0.00500 0.00518 104 79.0-121
1,3-Dichlorobenzene 0.00500 0.00517 103 79.0-120
1,4-Dichlorobenzene 0.00500 0.00521 104 79.0-120
Dichlorodifluoromethane 0.00500 0.00574 115 51.0-149
1,1-Dichloroethane 0.00500 0.00490 98.0 70.0-126
1,2-Dichloroethane 0.00500 0.00470 94.0 70.0-128
1,1-Dichloroethene 0.00500 0.00477 95.4 71.0-124
cis-1,2-Dichloroethene 0.00500 0.00464 92.8 73.0-120
trans-1,2-Dichloroethene 0.00500 0.00522 104 73.0-120
1,2-Dichloropropane 0.00500 0.00483 96.6 77.0-125
1,1-Dichloropropene 0.00500 0.00524 105 74.0-126
1,3-Dichloropropane 0.00500 0.00546 109 80.0-120
cis-1,3-Dichloropropene 0.00500 0.00492 98.4 80.0-123
trans-1,3-Dichloropropene 0.00500 0.00534 107 78.0-124
2,2-Dichloropropane 0.00500 0.00537 107 58.0-130
Di-isopropyl ether 0.00500 0.00414 82.8 58.0-138
Ethylbenzene 0.00500 0.00534 107 79.0-123
Hexachloro-1,3-butadiene 0.00500 0.00476 95.2 54.0-138
Isopropylbenzene 0.00500 0.00516 103 76.0-127
p-Isopropyltoluene 0.00500 0.00446 89.2 76.0-125
2-Butanone (MEK)0.0250 0.0235 94.0 44.0-160
Methylene Chloride 0.00500 0.00497 99.4 67.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001134
Volatile Organic Compounds (GC/MS) by Method 8260B L1582319-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3888119-1 02/06/23 16:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
4-Methyl-2-pentanone (MIBK) 0.0250 0.0242 96.8 68.0-142
Methyl tert-butyl ether 0.00500 0.00483 96.6 68.0-125
Naphthalene 0.00500 0.00348 69.6 54.0-135
n-Propylbenzene 0.00500 0.00411 82.2 77.0-124
Styrene 0.00500 0.00521 104 73.0-130
1,1,1,2-Tetrachloroethane 0.00500 0.00587 117 75.0-125
1,1,2,2-Tetrachloroethane 0.00500 0.00434 86.8 65.0-130
1,1,2-Trichlorotrifluoroethane 0.00500 0.00591 118 69.0-132
Tetrachloroethene 0.00500 0.00690 138 72.0-132 J4
Toluene 0.00500 0.00538 108 79.0-120
1,2,3-Trichlorobenzene 0.00500 0.00465 93.0 50.0-138
1,2,4-Trichlorobenzene 0.00500 0.00455 91.0 57.0-137
1,1,1-Trichloroethane 0.00500 0.00531 106 73.0-124
1,1,2-Trichloroethane 0.00500 0.00595 119 80.0-120
Trichloroethene 0.00500 0.00610 122 78.0-124
Trichlorofluoromethane 0.00500 0.00719 144 59.0-147
1,2,3-Trichloropropane 0.00500 0.00454 90.8 73.0-130
1,2,4-Trimethylbenzene 0.00500 0.00405 81.0 76.0-121
1,2,3-Trimethylbenzene 0.00500 0.00415 83.0 77.0-120
1,3,5-Trimethylbenzene 0.00500 0.00427 85.4 76.0-122
Vinyl chloride 0.00500 0.00589 118 67.0-131
Xylenes, Total 0.0150 0.0166 111 79.0-123
(S) Toluene-d8 109 80.0-120
(S) 4-Bromofluorobenzene 93.9 77.0-126
(S) 1,2-Dichloroethane-d4 92.1 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000565
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888499-1 02/07/23 14:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) High Fraction U 0.0247 0.100
(S) o-Terphenyl 106 31.0-160
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3888499-2 02/07/23 15:04 • (LCSD) R3888499-3 02/07/23 15:24
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.50 1.82 1.81 121 121 50.0-150 0.551 20
(S) o-Terphenyl 111 112 31.0-160
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000361
Polychlorinated Biphenyls (GC) by Method 8082 L1582319-01,02
Method Blank (MB)
(MB) R3887885-1 02/06/23 13:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
(S) Decachlorobiphenyl 50.0 10.0-128
(S) Tetrachloro-m-xylene 80.4 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3887885-2 02/06/23 13:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
PCB 1016 0.00250 0.00221 88.4 36.0-135
PCB 1260 0.00250 0.00253 101 42.0-131
(S) Decachlorobiphenyl 42.7 10.0-128
(S) Tetrachloro-m-xylene 77.1 10.0-127
L1582014-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582014-09 02/06/23 14:05 • (MS) R3887885-6 02/06/23 14:36 • (MSD) R3887885-7 02/06/23 14:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 ND 0.00212 0.00271 84.8 108 1 11.0-160 24.4 38
PCB 1260 0.00250 ND 0.00107 0.00225 42.8 90.0 1 20.0-142 J3 71.1 27
(S) Decachlorobiphenyl 35.8 72.1 10.0-128
(S) Tetrachloro-m-xylene 47.2 70.8 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2001014
Polychlorinated Biphenyls (GC) by Method 8082 L1582319-03,04,05
Method Blank (MB)
(MB) R3888110-1 02/06/23 23:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
(S) Decachlorobiphenyl 76.5 10.0-128
(S) Tetrachloro-m-xylene 65.6 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3888110-5 02/06/23 23:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
PCB 1016 0.00250 0.00204 81.6 36.0-135
PCB 1260 0.00250 0.00198 79.2 42.0-131
(S) Decachlorobiphenyl 26.1 10.0-128
(S) Tetrachloro-m-xylene 66.4 10.0-127
L1582562-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582562-03 02/07/23 07:34 • (MS) R3888110-6 02/07/23 08:05 • (MSD) R3888110-7 02/07/23 08:15
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 ND 0.00230 0.00156 92.0 62.4 1 11.0-160 J3 38.3 38
PCB 1260 0.00250 ND 0.00135 0.00118 54.0 47.2 1 20.0-142 13.4 27
(S) Decachlorobiphenyl 38.1 34.1 10.0-128
(S) Tetrachloro-m-xylene 62.1 61.5 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888265-3 02/07/23 11:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-oxybis(1-chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888265-3 02/07/23 11:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 32.7 10.0-120
(S) Phenol-d5 20.7 10.0-120
(S) Nitrobenzene-d5 71.4 10.0-127
(S) 2-Fluorobiphenyl 77.6 10.0-130
(S) 2,4,6-Tribromophenol 62.0 10.0-155
(S) p-Terphenyl-d14 81.2 10.0-128
Laboratory Control Sample (LCS)
(LCS) R3888265-1 02/07/23 10:30
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acenaphthene 0.0500 0.0379 75.8 41.0-120
Acenaphthylene 0.0500 0.0405 81.0 43.0-120
Anthracene 0.0500 0.0372 74.4 45.0-120
Benzidine 0.100 0.00481 4.81 10.0-120 J4
Benzo(a)anthracene 0.0500 0.0392 78.4 47.0-120
Benzo(b)fluoranthene 0.0500 0.0395 79.0 46.0-120
Benzo(k)fluoranthene 0.0500 0.0391 78.2 46.0-120
Benzo(g,h,i)perylene 0.0500 0.0388 77.6 48.0-121
Benzo(a)pyrene 0.0500 0.0419 83.8 47.0-120
Bis(2-chlorethoxy)methane 0.0500 0.0339 67.8 33.0-120
Bis(2-chloroethyl)ether 0.0500 0.0350 70.0 23.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1582319-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3888265-1 02/07/23 10:30
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,2-oxybis(1-chloropropane) 0.0500 0.0349 69.8 28.0-120
4-Bromophenyl-phenylether 0.0500 0.0405 81.0 45.0-120
2-Chloronaphthalene 0.0500 0.0379 75.8 37.0-120
4-Chlorophenyl-phenylether 0.0500 0.0394 78.8 44.0-120
Chrysene 0.0500 0.0399 79.8 48.0-120
Dibenz(a,h)anthracene 0.0500 0.0389 77.8 47.0-120
1,2-Dichlorobenzene 0.0500 0.0343 68.6 20.0-120
1,3-Dichlorobenzene 0.0500 0.0332 66.4 17.0-120
1,4-Dichlorobenzene 0.0500 0.0339 67.8 18.0-120
3,3-Dichlorobenzidine 0.100 0.0674 67.4 44.0-120
2,4-Dinitrotoluene 0.0500 0.0406 81.2 49.0-124
2,6-Dinitrotoluene 0.0500 0.0404 80.8 46.0-120
Fluoranthene 0.0500 0.0401 80.2 51.0-120
Fluorene 0.0500 0.0395 79.0 47.0-120
Hexachlorobenzene 0.0500 0.0390 78.0 44.0-120
Hexachloro-1,3-butadiene 0.0500 0.0333 66.6 19.0-120
Hexachlorocyclopentadiene 0.0500 0.0320 64.0 15.0-120
Hexachloroethane 0.0500 0.0343 68.6 15.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0361 72.2 49.0-122
Isophorone 0.0500 0.0321 64.2 36.0-120
Naphthalene 0.0500 0.0326 65.2 27.0-120
Nitrobenzene 0.0500 0.0326 65.2 27.0-120
n-Nitrosodimethylamine 0.0500 0.0164 32.8 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0323 64.6 47.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0364 72.8 31.0-120
Phenanthrene 0.0500 0.0388 77.6 46.0-120
Benzylbutyl phthalate 0.0500 0.0401 80.2 43.0-121
Bis(2-ethylhexyl)phthalate 0.0500 0.0415 83.0 43.0-122
Di-n-butyl phthalate 0.0500 0.0406 81.2 49.0-121
Diethyl phthalate 0.0500 0.0398 79.6 48.0-122
Dimethyl phthalate 0.0500 0.0398 79.6 48.0-120
Di-n-octyl phthalate 0.0500 0.0359 71.8 42.0-125
Pyrene 0.0500 0.0393 78.6 47.0-120
1,2,4-Trichlorobenzene 0.0500 0.0326 65.2 24.0-120
4-Chloro-3-methylphenol 0.0500 0.0303 60.6 40.0-120
2-Chlorophenol 0.0500 0.0286 57.2 25.0-120
2,4-Dichlorophenol 0.0500 0.0323 64.6 36.0-120
2,4-Dimethylphenol 0.0500 0.0271 54.2 33.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0373 74.6 38.0-138
2,4-Dinitrophenol 0.0500 0.0318 63.6 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1582319-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3888265-1 02/07/23 10:30
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Nitrophenol 0.0500 0.0334 66.8 31.0-120
4-Nitrophenol 0.0500 0.0125 25.0 10.0-120
Pentachlorophenol 0.0500 0.0372 74.4 23.0-120
Phenol 0.0500 0.0110 22.0 10.0-120
2,4,6-Trichlorophenol 0.0500 0.0390 78.0 42.0-120
(S) 2-Fluorophenol 34.1 10.0-120
(S) Phenol-d5 20.3 10.0-120
(S) Nitrobenzene-d5 51.8 10.0-127
(S) 2-Fluorobiphenyl 74.2 10.0-130
(S) 2,4,6-Tribromophenol 75.5 10.0-155
(S) p-Terphenyl-d14 75.2 10.0-128
L1582316-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582316-01 02/07/23 12:16 • (MS) R3888265-4 02/07/23 12:37 • (MSD) R3888265-5 02/07/23 12:58
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 ND 0.0309 0.0314 61.8 62.8 1 28.0-120 1.61 25
Acenaphthylene 0.0500 ND 0.0322 0.0331 64.4 66.2 1 31.0-121 2.76 25
Anthracene 0.0500 ND 0.0334 0.0311 66.8 62.2 1 36.0-120 7.13 23
Benzidine 0.100 ND ND ND 0.000 3.80 1 10.0-120 J6 J3 J6 200 37
Benzo(a)anthracene 0.0500 ND 0.0363 0.0323 72.6 64.6 1 39.0-120 11.7 23
Benzo(b)fluoranthene 0.0500 ND 0.0370 0.0329 74.0 65.8 1 37.0-120 11.7 23
Benzo(k)fluoranthene 0.0500 ND 0.0364 0.0327 72.8 65.4 1 37.0-120 10.7 26
Benzo(g,h,i)perylene 0.0500 ND 0.0378 0.0321 75.6 64.2 1 37.0-123 16.3 25
Benzo(a)pyrene 0.0500 ND 0.0402 0.0351 80.4 70.2 1 37.0-120 13.5 24
Bis(2-chlorethoxy)methane 0.0500 ND 0.0256 0.0287 51.2 57.4 1 17.0-120 11.4 31
Bis(2-chloroethyl)ether 0.0500 ND 0.0251 0.0250 50.2 50.0 1 14.0-120 0.399 33
2,2-oxybis(1-chloropropane) 0.0500 ND 0.0249 0.0277 49.8 55.4 1 18.0-120 10.6 34
4-Bromophenyl-phenylether 0.0500 ND 0.0343 0.0347 68.6 69.4 1 37.0-120 1.16 24
2-Chloronaphthalene 0.0500 ND 0.0284 0.0308 56.8 61.6 1 29.0-120 8.11 28
4-Chlorophenyl-phenylether 0.0500 ND 0.0345 0.0326 69.0 65.2 1 36.0-120 5.66 23
Chrysene 0.0500 ND 0.0379 0.0332 75.8 66.4 1 38.0-120 13.2 23
Dibenz(a,h)anthracene 0.0500 ND 0.0370 0.0321 74.0 64.2 1 36.0-121 14.2 24
1,2-Dichlorobenzene 0.0500 ND 0.0230 0.0253 46.0 50.6 1 18.0-120 9.52 40
1,3-Dichlorobenzene 0.0500 ND 0.0219 0.0247 43.8 49.4 1 15.0-120 12.0 40
1,4-Dichlorobenzene 0.0500 ND 0.0220 0.0251 44.0 50.2 1 17.0-120 13.2 40
3,3-Dichlorobenzidine 0.100 ND 0.0384 0.0486 38.4 48.6 1 10.0-134 23.4 30
2,4-Dinitrotoluene 0.0500 ND 0.0388 0.0341 77.6 68.2 1 39.0-125 12.9 25
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000359
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1582319-01,02,03,04,05
L1582316-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582316-01 02/07/23 12:16 • (MS) R3888265-4 02/07/23 12:37 • (MSD) R3888265-5 02/07/23 12:58
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
2,6-Dinitrotoluene 0.0500 ND 0.0346 0.0334 69.2 66.8 1 36.0-120 3.53 27
Fluoranthene 0.0500 ND 0.0404 0.0339 80.8 67.8 1 41.0-121 17.5 22
Fluorene 0.0500 ND 0.0345 0.0330 69.0 66.0 1 37.0-120 4.44 24
Hexachlorobenzene 0.0500 ND 0.0337 0.0333 67.4 66.6 1 35.0-122 1.19 24
Hexachloro-1,3-butadiene 0.0500 ND 0.0233 0.0265 46.6 53.0 1 12.0-120 12.9 34
Hexachlorocyclopentadiene 0.0500 ND 0.0230 0.0275 46.0 55.0 1 10.0-120 17.8 33
Hexachloroethane 0.0500 ND 0.0219 0.0248 43.8 49.6 1 10.0-120 12.4 40
Indeno(1,2,3-cd)pyrene 0.0500 ND 0.0354 0.0303 70.8 60.6 1 38.0-125 15.5 24
Isophorone 0.0500 ND 0.0248 0.0268 49.6 53.6 1 21.0-120 7.75 27
Naphthalene 0.0500 ND 0.0243 0.0262 48.6 52.4 1 10.0-120 7.52 31
Nitrobenzene 0.0500 ND 0.0240 0.0268 48.0 53.6 1 12.0-120 11.0 30
n-Nitrosodimethylamine 0.0500 ND 0.0127 0.0142 25.4 28.4 1 10.0-120 11.2 40
n-Nitrosodiphenylamine 0.0500 ND 0.0282 0.0277 56.4 55.4 1 37.0-120 1.79 24
n-Nitrosodi-n-propylamine 0.0500 ND 0.0276 0.0286 55.2 57.2 1 16.0-120 3.56 30
Phenanthrene 0.0500 ND 0.0347 0.0325 69.4 65.0 1 33.0-120 6.55 22
Benzylbutyl phthalate 0.0500 ND 0.0392 0.0342 78.4 68.4 1 34.0-126 13.6 24
Bis(2-ethylhexyl)phthalate 0.0500 ND 0.0393 0.0351 78.6 70.2 1 33.0-126 11.3 25
Di-n-butyl phthalate 0.0500 ND 0.0396 0.0340 79.2 68.0 1 35.0-128 15.2 23
Diethyl phthalate 0.0500 ND 0.0369 0.0324 73.8 64.8 1 39.0-125 13.0 24
Dimethyl phthalate 0.0500 ND 0.0338 0.0328 67.6 65.6 1 37.0-120 3.00 24
Di-n-octyl phthalate 0.0500 ND 0.0364 0.0316 72.8 63.2 1 25.0-135 14.1 26
Pyrene 0.0500 ND 0.0356 0.0326 71.2 65.2 1 39.0-120 8.80 22
1,2,4-Trichlorobenzene 0.0500 ND 0.0230 0.0260 46.0 52.0 1 15.0-120 12.2 31
4-Chloro-3-methylphenol 0.0500 ND 0.0284 0.0268 56.8 53.6 1 26.0-120 5.80 27
2-Chlorophenol 0.0500 ND 0.0210 0.0233 42.0 46.6 1 18.0-120 10.4 34
2,4-Dichlorophenol 0.0500 ND 0.0251 0.0269 50.2 53.8 1 19.0-120 6.92 27
2,4-Dimethylphenol 0.0500 ND 0.0223 0.0244 44.6 48.8 1 15.0-120 8.99 28
4,6-Dinitro-2-methylphenol 0.0500 ND 0.0338 0.0318 67.6 63.6 1 10.0-144 6.10 39
2,4-Dinitrophenol 0.0500 ND 0.0348 0.0315 69.6 63.0 1 10.0-120 9.95 40
2-Nitrophenol 0.0500 ND 0.0242 0.0273 48.4 54.6 1 20.0-120 12.0 30
4-Nitrophenol 0.0500 ND 0.0137 0.0109 27.4 21.8 1 10.0-120 22.8 40
Pentachlorophenol 0.0500 ND 0.0386 0.0341 77.2 68.2 1 10.0-128 12.4 37
Phenol 0.0500 ND ND ND 17.3 18.2 1 10.0-120 5.06 40
2,4,6-Trichlorophenol 0.0500 ND 0.0310 0.0322 60.6 63.0 1 26.0-120 3.80 31
(S) 2-Fluorophenol 25.1 28.4 10.0-120
(S) Phenol-d5 16.4 17.1 10.0-120
(S) Nitrobenzene-d5 43.4 44.8 10.0-127
(S) 2-Fluorobiphenyl 55.4 61.7 10.0-130
(S) 2,4,6-Tribromophenol 68.5 66.5 10.0-155
(S) p-Terphenyl-d14 69.3 62.5 10.0-128
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000383
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1582319-01,02,03,04,05
Method Blank (MB)
(MB) R3888223-2 02/06/23 17:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Anthracene U 0.0000190 0.0000500
Acenaphthene U 0.0000190 0.0000500
Acenaphthylene U 0.0000171 0.0000500
Benzo(a)anthracene U 0.0000203 0.0000500
Benzo(a)pyrene U 0.0000184 0.0000500
Benzo(b)fluoranthene U 0.0000168 0.0000500
Benzo(g,h,i)perylene U 0.0000184 0.0000500
Benzo(k)fluoranthene U 0.0000202 0.0000500
Chrysene U 0.0000179 0.0000500
Dibenz(a,h)anthracene U 0.0000160 0.0000500
Fluoranthene U 0.0000270 0.000100
Fluorene U 0.0000169 0.0000500
Indeno(1,2,3-cd)pyrene U 0.0000158 0.0000500
Naphthalene U 0.0000917 0.000250
Phenanthrene U 0.0000180 0.0000500
Pyrene U 0.0000169 0.0000500
1-Methylnaphthalene U 0.0000687 0.000250
2-Methylnaphthalene U 0.0000674 0.000250
2-Chloronaphthalene U 0.0000682 0.000250
(S) Nitrobenzene-d5 97.5 31.0-160
(S) 2-Fluorobiphenyl 90.5 48.0-148
(S) p-Terphenyl-d14 102 37.0-146
Laboratory Control Sample (LCS)
(LCS) R3888223-1 02/06/23 17:24
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Anthracene 0.00200 0.00185 92.5 67.0-150
Acenaphthene 0.00200 0.00192 96.0 65.0-138
Acenaphthylene 0.00200 0.00196 98.0 66.0-140
Benzo(a)anthracene 0.00200 0.00200 100 61.0-140
Benzo(a)pyrene 0.00200 0.00215 107 60.0-143
Benzo(b)fluoranthene 0.00200 0.00197 98.5 58.0-141
Benzo(g,h,i)perylene 0.00200 0.00188 94.0 52.0-153
Benzo(k)fluoranthene 0.00200 0.00183 91.5 58.0-148
Chrysene 0.00200 0.00204 102 64.0-144
Dibenz(a,h)anthracene 0.00200 0.00171 85.5 52.0-155
Fluoranthene 0.00200 0.00209 104 69.0-153
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2000383
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1582319-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3888223-1 02/06/23 17:24
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Fluorene 0.00200 0.00192 96.0 64.0-136
Indeno(1,2,3-cd)pyrene 0.00200 0.00185 92.5 54.0-153
Naphthalene 0.00200 0.00187 93.5 61.0-137
Phenanthrene 0.00200 0.00187 93.5 62.0-137
Pyrene 0.00200 0.00228 114 60.0-142
1-Methylnaphthalene 0.00200 0.00201 100 66.0-142
2-Methylnaphthalene 0.00200 0.00201 100 62.0-136
2-Chloronaphthalene 0.00200 0.00178 89.0 64.0-140
(S) Nitrobenzene-d5 95.0 31.0-160
(S) 2-Fluorobiphenyl 94.0 48.0-148
(S) p-Terphenyl-d14 100 37.0-146
L1582219-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1582219-02 02/06/23 18:53 • (MS) R3888223-3 02/06/23 19:11 • (MSD) R3888223-4 02/06/23 19:29
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Anthracene 0.00190 ND 0.00185 0.00181 97.4 95.3 1 56.0-156 2.19 20
Acenaphthene 0.00190 ND 0.00183 0.00185 96.3 97.4 1 44.0-153 1.09 20
Acenaphthylene 0.00190 ND 0.00186 0.00184 97.9 96.8 1 53.0-150 1.08 20
Benzo(a)anthracene 0.00190 ND 0.00193 0.00194 102 102 1 47.0-151 0.517 20
Benzo(a)pyrene 0.00190 ND 0.00203 0.00201 107 106 1 45.0-146 0.990 20
Benzo(b)fluoranthene 0.00190 ND 0.00188 0.00191 98.9 101 1 43.0-142 1.58 20
Benzo(g,h,i)perylene 0.00190 ND 0.00171 0.00173 90.0 91.1 1 40.0-147 1.16 20
Benzo(k)fluoranthene 0.00190 ND 0.00171 0.00173 90.0 91.1 1 43.0-148 1.16 21
Chrysene 0.00190 ND 0.00195 0.00199 103 105 1 50.0-148 2.03 20
Dibenz(a,h)anthracene 0.00190 ND 0.00156 0.00159 82.1 83.7 1 37.0-151 1.90 20
Fluoranthene 0.00190 ND 0.00203 0.00201 107 106 1 56.0-157 0.990 20
Fluorene 0.00190 ND 0.00185 0.00188 97.4 98.9 1 48.0-148 1.61 20
Indeno(1,2,3-cd)pyrene 0.00190 ND 0.00165 0.00168 86.8 88.4 1 41.0-148 1.80 20
Naphthalene 0.00190 ND 0.00196 0.00204 96.7 101 1 10.0-160 4.00 20
Phenanthrene 0.00190 ND 0.00185 0.00181 97.4 95.3 1 47.0-147 2.19 20
Pyrene 0.00190 ND 0.00225 0.00221 117 115 1 51.0-148 1.79 20
1-Methylnaphthalene 0.00190 ND 0.00195 0.00195 103 103 1 21.0-160 0.000 20
2-Methylnaphthalene 0.00190 ND 0.00199 0.00205 105 108 1 31.0-160 2.97 20
2-Chloronaphthalene 0.00190 ND 0.00179 0.00179 94.2 94.2 1 52.0-148 0.000 20
(S) Nitrobenzene-d5 100 103 31.0-160
(S) 2-Fluorobiphenyl 93.2 95.3 48.0-148
(S) p-Terphenyl-d14 94.2 97.9 37.0-146
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
March 24, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1594238
Samples Received:03/11/2023
Project Number:
Description:Recycled Earth - South
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
March 24, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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March 24, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
CS-1 L1594238-01 6
CS-4 L1594238-02 10
CS-3 L1594238-03 14
CS-2 L1594238-04 18
Qc: Quality Control Summary 22
Total Solids by Method 2540 G-2011 22
Wet Chemistry by Method 7199 23
Mercury by Method 7471A 27
Metals (ICP) by Method 6010B 28
Volatile Organic Compounds (GC) by Method 8015D/GRO 30
Volatile Organic Compounds (GC/MS) by Method 8260B 31
Semi-Volatile Organic Compounds (GC) by Method 8015 35
Polychlorinated Biphenyls (GC) by Method 8082 36
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 37
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 42
Gl: Glossary of Terms 46
Al: Accreditations & Locations 47
Sc: Sample Chain of Custody 48
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CS-1 L1594238-01 Solid Richie Torney 03/10/23 08:50 03/11/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2023759 1 03/16/23 06:58 03/16/23 07:06 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2023705 1 03/15/23 11:44 03/16/23 13:03 SET Mt. Juliet, TN
Mercury by Method 7471A WG2023712 1 03/15/23 11:49 03/15/23 17:41 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2023650 1 03/15/23 11:49 03/16/23 13:19 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2023463 25 03/10/23 08:50 03/15/23 15:36 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2023837 1 03/10/23 08:50 03/15/23 15:18 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2026270 10 03/20/23 10:31 03/21/23 01:03 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2026234 1 03/20/23 22:06 03/21/23 13:47 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2026297 10 03/20/23 12:34 03/23/23 17:08 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2026014 1 03/20/23 08:29 03/20/23 23:39 DLH Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-4 L1594238-02 Solid Richie Torney 03/10/23 09:25 03/11/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2023759 1 03/16/23 06:58 03/16/23 07:06 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2023705 1 03/15/23 11:44 03/16/23 13:09 SET Mt. Juliet, TN
Mercury by Method 7471A WG2023712 1 03/15/23 11:49 03/15/23 17:43 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2023650 1 03/15/23 11:49 03/16/23 13:21 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2023463 28.7 03/10/23 09:25 03/15/23 15:56 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2023837 1.15 03/10/23 09:25 03/15/23 15:39 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2026270 1 03/20/23 10:31 03/21/23 00:24 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2026234 1 03/20/23 22:06 03/21/23 12:33 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2026297 1 03/20/23 12:34 03/21/23 22:19 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2026298 1 03/20/23 16:53 03/21/23 06:39 DLH Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-3 L1594238-03 Solid Richie Torney 03/10/23 09:55 03/11/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2023759 1 03/16/23 06:58 03/16/23 07:06 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2024335 1 03/16/23 13:07 03/17/23 09:45 NCK Mt. Juliet, TN
Mercury by Method 7471A WG2023712 1 03/15/23 11:49 03/15/23 17:51 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2023650 1 03/15/23 11:49 03/16/23 13:24 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2023463 27.5 03/10/23 09:55 03/15/23 16:17 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2023837 1.1 03/10/23 09:55 03/15/23 16:01 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2026270 1 03/20/23 10:31 03/20/23 22:53 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2026234 1 03/20/23 22:06 03/21/23 11:18 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2026297 5 03/20/23 12:34 03/21/23 23:23 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2026298 1 03/20/23 16:53 03/21/23 01:29 DLH Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-2 L1594238-04 Solid Richie Torney 03/10/23 10:15 03/11/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2023759 1 03/16/23 06:58 03/16/23 07:06 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2024335 1 03/16/23 13:07 03/17/23 09:50 NCK Mt. Juliet, TN
Mercury by Method 7471A WG2023712 1 03/15/23 11:49 03/15/23 17:53 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2023650 1 03/15/23 11:49 03/16/23 13:27 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2023463 25 03/10/23 10:15 03/15/23 16:37 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2023837 1 03/10/23 10:15 03/15/23 16:22 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2026270 1 03/20/23 10:31 03/21/23 09:03 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2026234 1 03/20/23 22:06 03/21/23 11:28 JMB Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CS-2 L1594238-04 Solid Richie Torney 03/10/23 10:15 03/11/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2026297 1 03/20/23 12:34 03/21/23 20:10 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2026298 1 03/20/23 16:53 03/21/23 01:46 DLH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1594238
CS-1
Collected date/time: 03/10/23 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.2 1 03/16/2023 07:06 WG2023759
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium 2.05 1.17 1 03/16/2023 13:03 WG2023705
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0470 1 03/15/2023 17:41 WG2023712
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.35 1 03/16/2023 13:19 WG2023650
Arsenic 3.79 2.35 1 03/16/2023 13:19 WG2023650
Beryllium 0.243 0.235 1 03/16/2023 13:19 WG2023650
Cadmium ND 0.587 1 03/16/2023 13:19 WG2023650
Chromium 10.3 1.17 1 03/16/2023 13:19 WG2023650
Copper 39.0 2.35 1 03/16/2023 13:19 WG2023650
Lead 2.79 0.587 1 03/16/2023 13:19 WG2023650
Nickel 4.52 2.35 1 03/16/2023 13:19 WG2023650
Selenium ND 2.35 1 03/16/2023 13:19 WG2023650
Silver ND 1.17 1 03/16/2023 13:19 WG2023650
Thallium ND 2.35 1 03/16/2023 13:19 WG2023650
Zinc 23.3 5.87 1 03/16/2023 13:19 WG2023650
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.37 25 03/15/2023 15:36 WG2023463
(S) a,a,a-Trifluorotoluene(FID) 95.6 77.0-120 03/15/2023 15:36 WG2023463
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0674 1 03/15/2023 15:18 WG2023837
Acrylonitrile ND 0.0169 1 03/15/2023 15:18 WG2023837
Benzene ND 0.00135 1 03/15/2023 15:18 WG2023837
Bromobenzene ND 0.0169 1 03/15/2023 15:18 WG2023837
Bromodichloromethane ND 0.00337 1 03/15/2023 15:18 WG2023837
Bromoform ND 0.0337 1 03/15/2023 15:18 WG2023837
Bromomethane ND 0.0169 1 03/15/2023 15:18 WG2023837
n-Butylbenzene ND 0.0169 1 03/15/2023 15:18 WG2023837
sec-Butylbenzene ND 0.0169 1 03/15/2023 15:18 WG2023837
tert-Butylbenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
Carbon tetrachloride ND 0.00674 1 03/15/2023 15:18 WG2023837
Chlorobenzene ND 0.00337 1 03/15/2023 15:18 WG2023837
Chlorodibromomethane ND 0.00337 1 03/15/2023 15:18 WG2023837
Chloroethane ND 0.00674 1 03/15/2023 15:18 WG2023837
Chloroform ND 0.00337 1 03/15/2023 15:18 WG2023837
Chloromethane ND 0.0169 1 03/15/2023 15:18 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1594238
CS-1
Collected date/time: 03/10/23 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00337 1 03/15/2023 15:18 WG2023837
4-Chlorotoluene ND 0.00674 1 03/15/2023 15:18 WG2023837
1,2-Dibromo-3-Chloropropane ND 0.0337 1 03/15/2023 15:18 WG2023837
1,2-Dibromoethane ND 0.00337 1 03/15/2023 15:18 WG2023837
Dibromomethane ND 0.00674 1 03/15/2023 15:18 WG2023837
1,2-Dichlorobenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
1,3-Dichlorobenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
1,4-Dichlorobenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
Dichlorodifluoromethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,1-Dichloroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,2-Dichloroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,1-Dichloroethene ND 0.00337 1 03/15/2023 15:18 WG2023837
cis-1,2-Dichloroethene ND 0.00337 1 03/15/2023 15:18 WG2023837
trans-1,2-Dichloroethene ND 0.00674 1 03/15/2023 15:18 WG2023837
1,2-Dichloropropane ND 0.00674 1 03/15/2023 15:18 WG2023837
1,1-Dichloropropene ND 0.00337 1 03/15/2023 15:18 WG2023837
1,3-Dichloropropane ND 0.00674 1 03/15/2023 15:18 WG2023837
cis-1,3-Dichloropropene ND 0.00337 1 03/15/2023 15:18 WG2023837
trans-1,3-Dichloropropene ND 0.00674 1 03/15/2023 15:18 WG2023837
2,2-Dichloropropane ND 0.00337 1 03/15/2023 15:18 WG2023837
Di-isopropyl ether ND 0.00135 1 03/15/2023 15:18 WG2023837
Ethylbenzene ND 0.00337 1 03/15/2023 15:18 WG2023837
Hexachloro-1,3-butadiene ND 0.0337 1 03/15/2023 15:18 WG2023837
Isopropylbenzene 0.00510 0.00337 1 03/15/2023 15:18 WG2023837
p-Isopropyltoluene 0.0326 0.00674 1 03/15/2023 15:18 WG2023837
2-Butanone (MEK)ND 0.135 1 03/15/2023 15:18 WG2023837
Methylene Chloride ND 0.0337 1 03/15/2023 15:18 WG2023837
4-Methyl-2-pentanone (MIBK) ND 0.0337 1 03/15/2023 15:18 WG2023837
Methyl tert-butyl ether ND 0.00135 1 03/15/2023 15:18 WG2023837
Naphthalene ND 0.0169 1 03/15/2023 15:18 WG2023837
n-Propylbenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
Styrene 0.139 0.0169 1 03/15/2023 15:18 WG2023837
1,1,1,2-Tetrachloroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,1,2,2-Tetrachloroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,1,2-Trichlorotrifluoroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
Tetrachloroethene ND 0.00337 1 03/15/2023 15:18 WG2023837
Toluene 0.00937 0.00674 1 03/15/2023 15:18 WG2023837
1,2,3-Trichlorobenzene ND 0.0169 1 03/15/2023 15:18 WG2023837
1,2,4-Trichlorobenzene ND 0.0169 1 03/15/2023 15:18 WG2023837
1,1,1-Trichloroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,1,2-Trichloroethane ND 0.00337 1 03/15/2023 15:18 WG2023837
Trichloroethene ND 0.00135 1 03/15/2023 15:18 WG2023837
Trichlorofluoromethane ND 0.00337 1 03/15/2023 15:18 WG2023837
1,2,3-Trichloropropane ND 0.0169 1 03/15/2023 15:18 WG2023837
1,2,4-Trimethylbenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
1,2,3-Trimethylbenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
1,3,5-Trimethylbenzene ND 0.00674 1 03/15/2023 15:18 WG2023837
Vinyl chloride ND 0.00337 1 03/15/2023 15:18 WG2023837
Xylenes, Total 0.0167 0.00876 1 03/15/2023 15:18 WG2023837
(S) Toluene-d8 111 75.0-131 03/15/2023 15:18 WG2023837
(S) 4-Bromofluorobenzene 117 67.0-138 03/15/2023 15:18 WG2023837
(S) 1,2-Dichloroethane-d4 86.9 70.0-130 03/15/2023 15:18 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1594238
CS-1
Collected date/time: 03/10/23 08:50
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 70.2 47.0 10 03/21/2023 01:03 WG2026270
C28-C40 Oil Range 363 47.0 10 03/21/2023 01:03 WG2026270
(S) o-Terphenyl 61.5 18.0-148 03/21/2023 01:03 WG2026270
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0399 1 03/21/2023 13:47 WG2026234
PCB 1221 ND 0.0399 1 03/21/2023 13:47 WG2026234
PCB 1232 ND 0.0399 1 03/21/2023 13:47 WG2026234
PCB 1242 ND 0.0399 1 03/21/2023 13:47 WG2026234
PCB 1248 ND 0.0200 1 03/21/2023 13:47 WG2026234
PCB 1254 ND 0.0200 1 03/21/2023 13:47 WG2026234
PCB 1260 ND 0.0200 1 03/21/2023 13:47 WG2026234
(S) Decachlorobiphenyl 32.1 10.0-135 03/21/2023 13:47 WG2026234
(S) Tetrachloro-m-xylene 42.7 10.0-139 03/21/2023 13:47 WG2026234
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.391 10 03/23/2023 17:08 WG2026297
Acenaphthylene ND 0.391 10 03/23/2023 17:08 WG2026297
Anthracene ND 0.391 10 03/23/2023 17:08 WG2026297
Benzidine ND 19.6 10 03/23/2023 17:08 WG2026297
Benzo(a)anthracene ND 0.391 10 03/23/2023 17:08 WG2026297
Benzo(b)fluoranthene ND 0.391 10 03/23/2023 17:08 WG2026297
Benzo(k)fluoranthene ND 0.391 10 03/23/2023 17:08 WG2026297
Benzo(g,h,i)perylene ND 0.391 10 03/23/2023 17:08 WG2026297
Benzo(a)pyrene ND 0.391 10 03/23/2023 17:08 WG2026297
Bis(2-chlorethoxy)methane ND 3.91 10 03/23/2023 17:08 WG2026297
Bis(2-chloroethyl)ether ND 3.91 10 03/23/2023 17:08 WG2026297
2,2-Oxybis(1-Chloropropane) ND 3.91 10 03/23/2023 17:08 WG2026297
4-Bromophenyl-phenylether ND 3.91 10 03/23/2023 17:08 WG2026297
2-Chloronaphthalene ND 0.391 10 03/23/2023 17:08 WG2026297
4-Chlorophenyl-phenylether ND 3.91 10 03/23/2023 17:08 WG2026297
Chrysene ND 0.391 10 03/23/2023 17:08 WG2026297
Dibenz(a,h)anthracene ND 0.391 10 03/23/2023 17:08 WG2026297
3,3-Dichlorobenzidine ND 3.91 10 03/23/2023 17:08 WG2026297
2,4-Dinitrotoluene ND 3.91 10 03/23/2023 17:08 WG2026297
2,6-Dinitrotoluene ND 3.91 10 03/23/2023 17:08 WG2026297
Fluoranthene ND 0.391 10 03/23/2023 17:08 WG2026297
Fluorene ND 0.391 10 03/23/2023 17:08 WG2026297
Hexachlorobenzene ND 3.91 10 03/23/2023 17:08 WG2026297
Hexachloro-1,3-butadiene ND 3.91 10 03/23/2023 17:08 WG2026297
Hexachlorocyclopentadiene ND 3.91 10 03/23/2023 17:08 WG2026297
Hexachloroethane ND 3.91 10 03/23/2023 17:08 WG2026297
Indeno(1,2,3-cd)pyrene ND 0.391 10 03/23/2023 17:08 WG2026297
Isophorone ND 3.91 10 03/23/2023 17:08 WG2026297
Naphthalene ND 0.391 10 03/23/2023 17:08 WG2026297
Nitrobenzene ND 3.91 10 03/23/2023 17:08 WG2026297
n-Nitrosodimethylamine ND 3.91 10 03/23/2023 17:08 WG2026297
n-Nitrosodiphenylamine ND 3.91 10 03/23/2023 17:08 WG2026297
n-Nitrosodi-n-propylamine ND 3.91 10 03/23/2023 17:08 WG2026297
Phenanthrene ND 0.391 10 03/23/2023 17:08 WG2026297
Benzylbutyl phthalate ND 3.91 10 03/23/2023 17:08 WG2026297
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1594238
CS-1
Collected date/time: 03/10/23 08:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 3.91 10 03/23/2023 17:08 WG2026297
Di-n-butyl phthalate ND 3.91 10 03/23/2023 17:08 WG2026297
Diethyl phthalate ND 3.91 10 03/23/2023 17:08 WG2026297
Dimethyl phthalate ND 3.91 10 03/23/2023 17:08 WG2026297
Di-n-octyl phthalate ND 3.91 10 03/23/2023 17:08 WG2026297
Pyrene ND 0.391 10 03/23/2023 17:08 WG2026297
1,2,4-Trichlorobenzene ND 3.91 10 03/23/2023 17:08 WG2026297
4-Chloro-3-methylphenol ND 3.91 10 03/23/2023 17:08 WG2026297
2-Chlorophenol ND 3.91 10 03/23/2023 17:08 WG2026297
2,4-Dichlorophenol ND 3.91 10 03/23/2023 17:08 WG2026297
2,4-Dimethylphenol ND 3.91 10 03/23/2023 17:08 WG2026297
4,6-Dinitro-2-methylphenol ND 3.91 10 03/23/2023 17:08 WG2026297
2,4-Dinitrophenol ND 3.91 10 03/23/2023 17:08 WG2026297
2-Nitrophenol ND 3.91 10 03/23/2023 17:08 WG2026297
4-Nitrophenol ND 3.91 10 03/23/2023 17:08 WG2026297
Pentachlorophenol ND 3.91 10 03/23/2023 17:08 WG2026297
Phenol ND 3.91 10 03/23/2023 17:08 WG2026297
2,4,6-Trichlorophenol ND 3.91 10 03/23/2023 17:08 WG2026297
(S) Nitrobenzene-d5 58.4 10.0-122 03/23/2023 17:08 WG2026297
(S) 2-Fluorobiphenyl 62.7 15.0-120 03/23/2023 17:08 WG2026297
(S) p-Terphenyl-d14 64.2 10.0-120 03/23/2023 17:08 WG2026297
(S) Phenol-d5 44.4 10.0-120 03/23/2023 17:08 WG2026297
(S) 2-Fluorophenol 31.5 12.0-120 03/23/2023 17:08 WG2026297
(S) 2,4,6-Tribromophenol 50.8 10.0-127 03/23/2023 17:08 WG2026297
Sample Narrative:
L1594238-01 WG2026297: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00704 1 03/20/2023 23:39 WG2026014
Acenaphthene ND 0.00704 1 03/20/2023 23:39 WG2026014
Acenaphthylene ND 0.00704 1 03/20/2023 23:39 WG2026014
Benzo(a)anthracene 0.144 J3 J5 J6 0.00704 1 03/20/2023 23:39 WG2026014
Benzo(a)pyrene 0.112 J3 J5 J6 0.00704 1 03/20/2023 23:39 WG2026014
Benzo(b)fluoranthene 0.0431 J3 0.00704 1 03/20/2023 23:39 WG2026014
Benzo(g,h,i)perylene 0.0906 J3 J5 0.00704 1 03/20/2023 23:39 WG2026014
Benzo(k)fluoranthene ND 0.00704 1 03/20/2023 23:39 WG2026014
Chrysene 0.131 J3 J5 J6 0.00704 1 03/20/2023 23:39 WG2026014
Dibenz(a,h)anthracene 0.0141 0.00704 1 03/20/2023 23:39 WG2026014
Fluoranthene 0.0370 J3 0.00704 1 03/20/2023 23:39 WG2026014
Fluorene ND 0.00704 1 03/20/2023 23:39 WG2026014
Indeno(1,2,3-cd)pyrene 0.0299 0.00704 1 03/20/2023 23:39 WG2026014
Naphthalene ND 0.0235 1 03/20/2023 23:39 WG2026014
Phenanthrene 0.0466 0.00704 1 03/20/2023 23:39 WG2026014
Pyrene 0.327 J3 J5 J6 0.00704 1 03/20/2023 23:39 WG2026014
1-Methylnaphthalene ND 0.0235 1 03/20/2023 23:39 WG2026014
2-Methylnaphthalene ND 0.0235 1 03/20/2023 23:39 WG2026014
2-Chloronaphthalene ND 0.0235 1 03/20/2023 23:39 WG2026014
(S) p-Terphenyl-d14 70.5 23.0-120 03/20/2023 23:39 WG2026014
(S) Nitrobenzene-d5 93.6 14.0-149 03/20/2023 23:39 WG2026014
(S) 2-Fluorobiphenyl 69.3 34.0-125 03/20/2023 23:39 WG2026014
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1594238
CS-4
Collected date/time: 03/10/23 09:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 93.8 1 03/16/2023 07:06 WG2023759
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.07 1 03/16/2023 13:09 WG2023705
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0427 1 03/15/2023 17:43 WG2023712
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.13 1 03/16/2023 13:21 WG2023650
Arsenic ND 2.13 1 03/16/2023 13:21 WG2023650
Beryllium 0.339 0.213 1 03/16/2023 13:21 WG2023650
Cadmium ND 0.533 1 03/16/2023 13:21 WG2023650
Chromium 13.8 1.07 1 03/16/2023 13:21 WG2023650
Copper 3.63 2.13 1 03/16/2023 13:21 WG2023650
Lead 12.5 0.533 1 03/16/2023 13:21 WG2023650
Nickel 5.80 2.13 1 03/16/2023 13:21 WG2023650
Selenium ND 2.13 1 03/16/2023 13:21 WG2023650
Silver ND 1.07 1 03/16/2023 13:21 WG2023650
Thallium ND 2.13 1 03/16/2023 13:21 WG2023650
Zinc 21.8 5.33 1 03/16/2023 13:21 WG2023650
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.23 28.7 03/15/2023 15:56 WG2023463
(S) a,a,a-Trifluorotoluene(FID) 96.3 77.0-120 03/15/2023 15:56 WG2023463
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0647 1.15 03/15/2023 15:39 WG2023837
Acrylonitrile ND 0.0162 1.15 03/15/2023 15:39 WG2023837
Benzene ND 0.00129 1.15 03/15/2023 15:39 WG2023837
Bromobenzene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
Bromodichloromethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Bromoform ND 0.0324 1.15 03/15/2023 15:39 WG2023837
Bromomethane ND 0.0162 1.15 03/15/2023 15:39 WG2023837
n-Butylbenzene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
sec-Butylbenzene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
tert-Butylbenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
Carbon tetrachloride ND 0.00647 1.15 03/15/2023 15:39 WG2023837
Chlorobenzene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Chlorodibromomethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Chloroethane ND 0.00647 1.15 03/15/2023 15:39 WG2023837
Chloroform ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Chloromethane ND 0.0162 1.15 03/15/2023 15:39 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1594238
CS-4
Collected date/time: 03/10/23 09:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
4-Chlorotoluene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,2-Dibromo-3-Chloropropane ND 0.0324 1.15 03/15/2023 15:39 WG2023837
1,2-Dibromoethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Dibromomethane ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,2-Dichlorobenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,3-Dichlorobenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,4-Dichlorobenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
Dichlorodifluoromethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,1-Dichloroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,2-Dichloroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,1-Dichloroethene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
cis-1,2-Dichloroethene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
trans-1,2-Dichloroethene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,2-Dichloropropane ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,1-Dichloropropene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,3-Dichloropropane ND 0.00647 1.15 03/15/2023 15:39 WG2023837
cis-1,3-Dichloropropene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
trans-1,3-Dichloropropene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
2,2-Dichloropropane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Di-isopropyl ether ND 0.00129 1.15 03/15/2023 15:39 WG2023837
Ethylbenzene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Hexachloro-1,3-butadiene ND 0.0324 1.15 03/15/2023 15:39 WG2023837
Isopropylbenzene ND 0.00324 1.15 03/15/2023 15:39 WG2023837
p-Isopropyltoluene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
2-Butanone (MEK)ND 0.129 1.15 03/15/2023 15:39 WG2023837
Methylene Chloride ND 0.0324 1.15 03/15/2023 15:39 WG2023837
4-Methyl-2-pentanone (MIBK) ND 0.0324 1.15 03/15/2023 15:39 WG2023837
Methyl tert-butyl ether ND 0.00129 1.15 03/15/2023 15:39 WG2023837
Naphthalene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
n-Propylbenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
Styrene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
1,1,1,2-Tetrachloroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,1,2,2-Tetrachloroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,1,2-Trichlorotrifluoroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Tetrachloroethene 0.0139 0.00324 1.15 03/15/2023 15:39 WG2023837
Toluene 0.00905 0.00647 1.15 03/15/2023 15:39 WG2023837
1,2,3-Trichlorobenzene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
1,2,4-Trichlorobenzene ND 0.0162 1.15 03/15/2023 15:39 WG2023837
1,1,1-Trichloroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,1,2-Trichloroethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Trichloroethene ND 0.00129 1.15 03/15/2023 15:39 WG2023837
Trichlorofluoromethane ND 0.00324 1.15 03/15/2023 15:39 WG2023837
1,2,3-Trichloropropane ND 0.0162 1.15 03/15/2023 15:39 WG2023837
1,2,4-Trimethylbenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,2,3-Trimethylbenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
1,3,5-Trimethylbenzene ND 0.00647 1.15 03/15/2023 15:39 WG2023837
Vinyl chloride ND 0.00324 1.15 03/15/2023 15:39 WG2023837
Xylenes, Total ND 0.00841 1.15 03/15/2023 15:39 WG2023837
(S) Toluene-d8 127 75.0-131 03/15/2023 15:39 WG2023837
(S) 4-Bromofluorobenzene 97.9 67.0-138 03/15/2023 15:39 WG2023837
(S) 1,2-Dichloroethane-d4 91.4 70.0-130 03/15/2023 15:39 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1594238
CS-4
Collected date/time: 03/10/23 09:25
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 9.07 4.27 1 03/21/2023 00:24 WG2026270
C28-C40 Oil Range 24.1 4.27 1 03/21/2023 00:24 WG2026270
(S) o-Terphenyl 60.7 18.0-148 03/21/2023 00:24 WG2026270
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0363 1 03/21/2023 12:33 WG2026234
PCB 1221 ND 0.0363 1 03/21/2023 12:33 WG2026234
PCB 1232 ND 0.0363 1 03/21/2023 12:33 WG2026234
PCB 1242 ND 0.0363 1 03/21/2023 12:33 WG2026234
PCB 1248 ND 0.0181 1 03/21/2023 12:33 WG2026234
PCB 1254 ND 0.0181 1 03/21/2023 12:33 WG2026234
PCB 1260 ND 0.0181 1 03/21/2023 12:33 WG2026234
(S) Decachlorobiphenyl 53.8 10.0-135 03/21/2023 12:33 WG2026234
(S) Tetrachloro-m-xylene 64.8 10.0-139 03/21/2023 12:33 WG2026234
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0355 1 03/21/2023 22:19 WG2026297
Acenaphthylene ND 0.0355 1 03/21/2023 22:19 WG2026297
Anthracene ND 0.0355 1 03/21/2023 22:19 WG2026297
Benzidine ND 1.78 1 03/21/2023 22:19 WG2026297
Benzo(a)anthracene ND 0.0355 1 03/21/2023 22:19 WG2026297
Benzo(b)fluoranthene ND 0.0355 1 03/21/2023 22:19 WG2026297
Benzo(k)fluoranthene ND 0.0355 1 03/21/2023 22:19 WG2026297
Benzo(g,h,i)perylene ND 0.0355 1 03/21/2023 22:19 WG2026297
Benzo(a)pyrene ND 0.0355 1 03/21/2023 22:19 WG2026297
Bis(2-chlorethoxy)methane ND 0.355 1 03/21/2023 22:19 WG2026297
Bis(2-chloroethyl)ether ND 0.355 1 03/21/2023 22:19 WG2026297
2,2-Oxybis(1-Chloropropane) ND 0.355 1 03/21/2023 22:19 WG2026297
4-Bromophenyl-phenylether ND 0.355 1 03/21/2023 22:19 WG2026297
2-Chloronaphthalene ND 0.0355 1 03/21/2023 22:19 WG2026297
4-Chlorophenyl-phenylether ND 0.355 1 03/21/2023 22:19 WG2026297
Chrysene ND 0.0355 1 03/21/2023 22:19 WG2026297
Dibenz(a,h)anthracene ND 0.0355 1 03/21/2023 22:19 WG2026297
3,3-Dichlorobenzidine ND 0.355 1 03/21/2023 22:19 WG2026297
2,4-Dinitrotoluene ND 0.355 1 03/21/2023 22:19 WG2026297
2,6-Dinitrotoluene ND 0.355 1 03/21/2023 22:19 WG2026297
Fluoranthene ND 0.0355 1 03/21/2023 22:19 WG2026297
Fluorene ND 0.0355 1 03/21/2023 22:19 WG2026297
Hexachlorobenzene ND 0.355 1 03/21/2023 22:19 WG2026297
Hexachloro-1,3-butadiene ND 0.355 1 03/21/2023 22:19 WG2026297
Hexachlorocyclopentadiene ND 0.355 1 03/21/2023 22:19 WG2026297
Hexachloroethane ND 0.355 1 03/21/2023 22:19 WG2026297
Indeno(1,2,3-cd)pyrene ND 0.0355 1 03/21/2023 22:19 WG2026297
Isophorone ND 0.355 1 03/21/2023 22:19 WG2026297
Naphthalene ND 0.0355 1 03/21/2023 22:19 WG2026297
Nitrobenzene ND 0.355 1 03/21/2023 22:19 WG2026297
n-Nitrosodimethylamine ND 0.355 1 03/21/2023 22:19 WG2026297
n-Nitrosodiphenylamine ND 0.355 1 03/21/2023 22:19 WG2026297
n-Nitrosodi-n-propylamine ND 0.355 1 03/21/2023 22:19 WG2026297
Phenanthrene ND 0.0355 1 03/21/2023 22:19 WG2026297
Benzylbutyl phthalate ND 0.355 1 03/21/2023 22:19 WG2026297
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1594238
CS-4
Collected date/time: 03/10/23 09:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.355 1 03/21/2023 22:19 WG2026297
Di-n-butyl phthalate ND 0.355 1 03/21/2023 22:19 WG2026297
Diethyl phthalate ND 0.355 1 03/21/2023 22:19 WG2026297
Dimethyl phthalate ND 0.355 1 03/21/2023 22:19 WG2026297
Di-n-octyl phthalate ND 0.355 1 03/21/2023 22:19 WG2026297
Pyrene ND 0.0355 1 03/21/2023 22:19 WG2026297
1,2,4-Trichlorobenzene ND 0.355 1 03/21/2023 22:19 WG2026297
4-Chloro-3-methylphenol ND 0.355 1 03/21/2023 22:19 WG2026297
2-Chlorophenol ND 0.355 1 03/21/2023 22:19 WG2026297
2,4-Dichlorophenol ND 0.355 1 03/21/2023 22:19 WG2026297
2,4-Dimethylphenol ND 0.355 1 03/21/2023 22:19 WG2026297
4,6-Dinitro-2-methylphenol ND 0.355 1 03/21/2023 22:19 WG2026297
2,4-Dinitrophenol ND 0.355 1 03/21/2023 22:19 WG2026297
2-Nitrophenol ND 0.355 1 03/21/2023 22:19 WG2026297
4-Nitrophenol ND 0.355 1 03/21/2023 22:19 WG2026297
Pentachlorophenol ND 0.355 1 03/21/2023 22:19 WG2026297
Phenol ND 0.355 1 03/21/2023 22:19 WG2026297
2,4,6-Trichlorophenol ND 0.355 1 03/21/2023 22:19 WG2026297
(S) Nitrobenzene-d5 53.9 10.0-122 03/21/2023 22:19 WG2026297
(S) 2-Fluorobiphenyl 59.1 15.0-120 03/21/2023 22:19 WG2026297
(S) p-Terphenyl-d14 63.0 10.0-120 03/21/2023 22:19 WG2026297
(S) Phenol-d5 46.2 10.0-120 03/21/2023 22:19 WG2026297
(S) 2-Fluorophenol 35.6 12.0-120 03/21/2023 22:19 WG2026297
(S) 2,4,6-Tribromophenol 51.7 10.0-127 03/21/2023 22:19 WG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00640 1 03/21/2023 06:39 WG2026298
Acenaphthene ND 0.00640 1 03/21/2023 06:39 WG2026298
Acenaphthylene ND 0.00640 1 03/21/2023 06:39 WG2026298
Benzo(a)anthracene 0.0164 0.00640 1 03/21/2023 06:39 WG2026298
Benzo(a)pyrene 0.0212 0.00640 1 03/21/2023 06:39 WG2026298
Benzo(b)fluoranthene 0.0302 0.00640 1 03/21/2023 06:39 WG2026298
Benzo(g,h,i)perylene 0.0162 0.00640 1 03/21/2023 06:39 WG2026298
Benzo(k)fluoranthene ND 0.00640 1 03/21/2023 06:39 WG2026298
Chrysene 0.0161 0.00640 1 03/21/2023 06:39 WG2026298
Dibenz(a,h)anthracene ND 0.00640 1 03/21/2023 06:39 WG2026298
Fluoranthene 0.0302 0.00640 1 03/21/2023 06:39 WG2026298
Fluorene ND 0.00640 1 03/21/2023 06:39 WG2026298
Indeno(1,2,3-cd)pyrene 0.0181 0.00640 1 03/21/2023 06:39 WG2026298
Naphthalene ND 0.0213 1 03/21/2023 06:39 WG2026298
Phenanthrene 0.0139 0.00640 1 03/21/2023 06:39 WG2026298
Pyrene 0.0259 0.00640 1 03/21/2023 06:39 WG2026298
1-Methylnaphthalene ND 0.0213 1 03/21/2023 06:39 WG2026298
2-Methylnaphthalene ND 0.0213 1 03/21/2023 06:39 WG2026298
2-Chloronaphthalene ND 0.0213 1 03/21/2023 06:39 WG2026298
(S) p-Terphenyl-d14 81.3 23.0-120 03/21/2023 06:39 WG2026298
(S) Nitrobenzene-d5 62.3 14.0-149 03/21/2023 06:39 WG2026298
(S) 2-Fluorobiphenyl 73.7 34.0-125 03/21/2023 06:39 WG2026298
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1594238
CS-3
Collected date/time: 03/10/23 09:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.5 1 03/16/2023 07:06 WG2023759
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium 2.34 1.12 1 03/17/2023 09:45 WG2024335
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0447 1 03/15/2023 17:51 WG2023712
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.24 1 03/16/2023 13:24 WG2023650
Arsenic 2.38 2.24 1 03/16/2023 13:24 WG2023650
Beryllium 0.845 0.224 1 03/16/2023 13:24 WG2023650
Cadmium ND 0.559 1 03/16/2023 13:24 WG2023650
Chromium 26.4 1.12 1 03/16/2023 13:24 WG2023650
Copper 34.8 2.24 1 03/16/2023 13:24 WG2023650
Lead 19.1 0.559 1 03/16/2023 13:24 WG2023650
Nickel 13.9 2.24 1 03/16/2023 13:24 WG2023650
Selenium ND 2.24 1 03/16/2023 13:24 WG2023650
Silver ND 1.12 1 03/16/2023 13:24 WG2023650
Thallium ND 2.24 1 03/16/2023 13:24 WG2023650
Zinc 57.3 5.59 1 03/16/2023 13:24 WG2023650
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.37 27.5 03/15/2023 16:17 WG2023463
(S) a,a,a-Trifluorotoluene(FID) 97.2 77.0-120 03/15/2023 16:17 WG2023463
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0674 1.1 03/15/2023 16:01 WG2023837
Acrylonitrile ND 0.0169 1.1 03/15/2023 16:01 WG2023837
Benzene ND 0.00135 1.1 03/15/2023 16:01 WG2023837
Bromobenzene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
Bromodichloromethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Bromoform ND 0.0337 1.1 03/15/2023 16:01 WG2023837
Bromomethane ND 0.0169 1.1 03/15/2023 16:01 WG2023837
n-Butylbenzene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
sec-Butylbenzene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
tert-Butylbenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
Carbon tetrachloride ND 0.00674 1.1 03/15/2023 16:01 WG2023837
Chlorobenzene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Chlorodibromomethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Chloroethane ND 0.00674 1.1 03/15/2023 16:01 WG2023837
Chloroform ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Chloromethane ND 0.0169 1.1 03/15/2023 16:01 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1594238
CS-3
Collected date/time: 03/10/23 09:55
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
4-Chlorotoluene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,2-Dibromo-3-Chloropropane ND 0.0337 1.1 03/15/2023 16:01 WG2023837
1,2-Dibromoethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Dibromomethane ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,2-Dichlorobenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,3-Dichlorobenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,4-Dichlorobenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
Dichlorodifluoromethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,1-Dichloroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,2-Dichloroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,1-Dichloroethene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
cis-1,2-Dichloroethene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
trans-1,2-Dichloroethene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,2-Dichloropropane ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,1-Dichloropropene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,3-Dichloropropane ND 0.00674 1.1 03/15/2023 16:01 WG2023837
cis-1,3-Dichloropropene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
trans-1,3-Dichloropropene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
2,2-Dichloropropane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Di-isopropyl ether ND 0.00135 1.1 03/15/2023 16:01 WG2023837
Ethylbenzene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Hexachloro-1,3-butadiene ND 0.0337 1.1 03/15/2023 16:01 WG2023837
Isopropylbenzene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
p-Isopropyltoluene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
2-Butanone (MEK)ND 0.135 1.1 03/15/2023 16:01 WG2023837
Methylene Chloride ND 0.0337 1.1 03/15/2023 16:01 WG2023837
4-Methyl-2-pentanone (MIBK) ND 0.0337 1.1 03/15/2023 16:01 WG2023837
Methyl tert-butyl ether ND 0.00135 1.1 03/15/2023 16:01 WG2023837
Naphthalene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
n-Propylbenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
Styrene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
1,1,1,2-Tetrachloroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,1,2,2-Tetrachloroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,1,2-Trichlorotrifluoroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Tetrachloroethene ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Toluene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,2,3-Trichlorobenzene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
1,2,4-Trichlorobenzene ND 0.0169 1.1 03/15/2023 16:01 WG2023837
1,1,1-Trichloroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,1,2-Trichloroethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Trichloroethene ND 0.00135 1.1 03/15/2023 16:01 WG2023837
Trichlorofluoromethane ND 0.00337 1.1 03/15/2023 16:01 WG2023837
1,2,3-Trichloropropane ND 0.0169 1.1 03/15/2023 16:01 WG2023837
1,2,4-Trimethylbenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,2,3-Trimethylbenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
1,3,5-Trimethylbenzene ND 0.00674 1.1 03/15/2023 16:01 WG2023837
Vinyl chloride ND 0.00337 1.1 03/15/2023 16:01 WG2023837
Xylenes, Total ND 0.00876 1.1 03/15/2023 16:01 WG2023837
(S) Toluene-d8 129 75.0-131 03/15/2023 16:01 WG2023837
(S) 4-Bromofluorobenzene 93.4 67.0-138 03/15/2023 16:01 WG2023837
(S) 1,2-Dichloroethane-d4 90.5 70.0-130 03/15/2023 16:01 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1594238
CS-3
Collected date/time: 03/10/23 09:55
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 43.4 4.47 1 03/20/2023 22:53 WG2026270
C28-C40 Oil Range 37.9 4.47 1 03/20/2023 22:53 WG2026270
(S) o-Terphenyl 58.9 18.0-148 03/20/2023 22:53 WG2026270
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0380 1 03/21/2023 11:18 WG2026234
PCB 1221 ND 0.0380 1 03/21/2023 11:18 WG2026234
PCB 1232 ND 0.0380 1 03/21/2023 11:18 WG2026234
PCB 1242 ND 0.0380 1 03/21/2023 11:18 WG2026234
PCB 1248 ND 0.0190 1 03/21/2023 11:18 WG2026234
PCB 1254 ND 0.0190 1 03/21/2023 11:18 WG2026234
PCB 1260 ND 0.0190 1 03/21/2023 11:18 WG2026234
(S) Decachlorobiphenyl 82.2 10.0-135 03/21/2023 11:18 WG2026234
(S) Tetrachloro-m-xylene 85.4 10.0-139 03/21/2023 11:18 WG2026234
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.187 5 03/21/2023 23:23 WG2026297
Acenaphthylene ND 0.187 5 03/21/2023 23:23 WG2026297
Anthracene ND 0.187 5 03/21/2023 23:23 WG2026297
Benzidine ND 9.33 5 03/21/2023 23:23 WG2026297
Benzo(a)anthracene ND 0.187 5 03/21/2023 23:23 WG2026297
Benzo(b)fluoranthene ND 0.187 5 03/21/2023 23:23 WG2026297
Benzo(k)fluoranthene ND 0.187 5 03/21/2023 23:23 WG2026297
Benzo(g,h,i)perylene ND 0.187 5 03/21/2023 23:23 WG2026297
Benzo(a)pyrene ND 0.187 5 03/21/2023 23:23 WG2026297
Bis(2-chlorethoxy)methane ND 1.87 5 03/21/2023 23:23 WG2026297
Bis(2-chloroethyl)ether ND 1.87 5 03/21/2023 23:23 WG2026297
2,2-Oxybis(1-Chloropropane) ND 1.87 5 03/21/2023 23:23 WG2026297
4-Bromophenyl-phenylether ND 1.87 5 03/21/2023 23:23 WG2026297
2-Chloronaphthalene ND 0.187 5 03/21/2023 23:23 WG2026297
4-Chlorophenyl-phenylether ND 1.87 5 03/21/2023 23:23 WG2026297
Chrysene ND 0.187 5 03/21/2023 23:23 WG2026297
Dibenz(a,h)anthracene ND 0.187 5 03/21/2023 23:23 WG2026297
3,3-Dichlorobenzidine ND 1.87 5 03/21/2023 23:23 WG2026297
2,4-Dinitrotoluene ND 1.87 5 03/21/2023 23:23 WG2026297
2,6-Dinitrotoluene ND 1.87 5 03/21/2023 23:23 WG2026297
Fluoranthene ND 0.187 5 03/21/2023 23:23 WG2026297
Fluorene ND 0.187 5 03/21/2023 23:23 WG2026297
Hexachlorobenzene ND 1.87 5 03/21/2023 23:23 WG2026297
Hexachloro-1,3-butadiene ND 1.87 5 03/21/2023 23:23 WG2026297
Hexachlorocyclopentadiene ND 1.87 5 03/21/2023 23:23 WG2026297
Hexachloroethane ND 1.87 5 03/21/2023 23:23 WG2026297
Indeno(1,2,3-cd)pyrene ND 0.187 5 03/21/2023 23:23 WG2026297
Isophorone ND 1.87 5 03/21/2023 23:23 WG2026297
Naphthalene ND 0.187 5 03/21/2023 23:23 WG2026297
Nitrobenzene ND 1.87 5 03/21/2023 23:23 WG2026297
n-Nitrosodimethylamine ND 1.87 5 03/21/2023 23:23 WG2026297
n-Nitrosodiphenylamine ND 1.87 5 03/21/2023 23:23 WG2026297
n-Nitrosodi-n-propylamine ND 1.87 5 03/21/2023 23:23 WG2026297
Phenanthrene ND 0.187 5 03/21/2023 23:23 WG2026297
Benzylbutyl phthalate ND 1.87 5 03/21/2023 23:23 WG2026297
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 03
L1594238
CS-3
Collected date/time: 03/10/23 09:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 1.87 5 03/21/2023 23:23 WG2026297
Di-n-butyl phthalate ND 1.87 5 03/21/2023 23:23 WG2026297
Diethyl phthalate ND 1.87 5 03/21/2023 23:23 WG2026297
Dimethyl phthalate ND 1.87 5 03/21/2023 23:23 WG2026297
Di-n-octyl phthalate ND 1.87 5 03/21/2023 23:23 WG2026297
Pyrene ND 0.187 5 03/21/2023 23:23 WG2026297
1,2,4-Trichlorobenzene ND 1.87 5 03/21/2023 23:23 WG2026297
4-Chloro-3-methylphenol ND 1.87 5 03/21/2023 23:23 WG2026297
2-Chlorophenol ND 1.87 5 03/21/2023 23:23 WG2026297
2,4-Dichlorophenol ND 1.87 5 03/21/2023 23:23 WG2026297
2,4-Dimethylphenol ND 1.87 5 03/21/2023 23:23 WG2026297
4,6-Dinitro-2-methylphenol ND 1.87 5 03/21/2023 23:23 WG2026297
2,4-Dinitrophenol ND 1.87 5 03/21/2023 23:23 WG2026297
2-Nitrophenol ND 1.87 5 03/21/2023 23:23 WG2026297
4-Nitrophenol ND 1.87 5 03/21/2023 23:23 WG2026297
Pentachlorophenol ND 1.87 5 03/21/2023 23:23 WG2026297
Phenol ND 1.87 5 03/21/2023 23:23 WG2026297
2,4,6-Trichlorophenol ND 1.87 5 03/21/2023 23:23 WG2026297
(S) Nitrobenzene-d5 43.2 10.0-122 03/21/2023 23:23 WG2026297
(S) 2-Fluorobiphenyl 49.2 15.0-120 03/21/2023 23:23 WG2026297
(S) p-Terphenyl-d14 48.0 10.0-120 03/21/2023 23:23 WG2026297
(S) Phenol-d5 39.8 10.0-120 03/21/2023 23:23 WG2026297
(S) 2-Fluorophenol 26.0 12.0-120 03/21/2023 23:23 WG2026297
(S) 2,4,6-Tribromophenol 16.8 10.0-127 03/21/2023 23:23 WG2026297
Sample Narrative:
L1594238-03 WG2026297: Dilution due to matrix impact during extract concentration procedure
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00671 1 03/21/2023 01:29 WG2026298
Acenaphthene ND 0.00671 1 03/21/2023 01:29 WG2026298
Acenaphthylene ND 0.00671 1 03/21/2023 01:29 WG2026298
Benzo(a)anthracene ND 0.00671 1 03/21/2023 01:29 WG2026298
Benzo(a)pyrene ND 0.00671 1 03/21/2023 01:29 WG2026298
Benzo(b)fluoranthene ND 0.00671 1 03/21/2023 01:29 WG2026298
Benzo(g,h,i)perylene ND 0.00671 1 03/21/2023 01:29 WG2026298
Benzo(k)fluoranthene ND 0.00671 1 03/21/2023 01:29 WG2026298
Chrysene ND 0.00671 1 03/21/2023 01:29 WG2026298
Dibenz(a,h)anthracene ND 0.00671 1 03/21/2023 01:29 WG2026298
Fluoranthene ND 0.00671 1 03/21/2023 01:29 WG2026298
Fluorene ND 0.00671 1 03/21/2023 01:29 WG2026298
Indeno(1,2,3-cd)pyrene ND 0.00671 1 03/21/2023 01:29 WG2026298
Naphthalene ND 0.0224 1 03/21/2023 01:29 WG2026298
Phenanthrene ND 0.00671 1 03/21/2023 01:29 WG2026298
Pyrene ND 0.00671 1 03/21/2023 01:29 WG2026298
1-Methylnaphthalene ND 0.0224 1 03/21/2023 01:29 WG2026298
2-Methylnaphthalene ND 0.0224 1 03/21/2023 01:29 WG2026298
2-Chloronaphthalene ND 0.0224 1 03/21/2023 01:29 WG2026298
(S) p-Terphenyl-d14 91.6 23.0-120 03/21/2023 01:29 WG2026298
(S) Nitrobenzene-d5 92.8 14.0-149 03/21/2023 01:29 WG2026298
(S) 2-Fluorobiphenyl 89.1 34.0-125 03/21/2023 01:29 WG2026298
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1594238
CS-2
Collected date/time: 03/10/23 10:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 91.1 1 03/16/2023 07:06 WG2023759
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.10 1 03/17/2023 09:50 WG2024335
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0439 1 03/15/2023 17:53 WG2023712
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.19 1 03/16/2023 13:27 WG2023650
Arsenic ND 2.19 1 03/16/2023 13:27 WG2023650
Beryllium 0.440 0.219 1 03/16/2023 13:27 WG2023650
Cadmium ND 0.549 1 03/16/2023 13:27 WG2023650
Chromium 19.0 1.10 1 03/16/2023 13:27 WG2023650
Copper 12.1 2.19 1 03/16/2023 13:27 WG2023650
Lead 10.6 0.549 1 03/16/2023 13:27 WG2023650
Nickel 8.75 2.19 1 03/16/2023 13:27 WG2023650
Selenium ND 2.19 1 03/16/2023 13:27 WG2023650
Silver ND 1.10 1 03/16/2023 13:27 WG2023650
Thallium ND 2.19 1 03/16/2023 13:27 WG2023650
Zinc 33.1 5.49 1 03/16/2023 13:27 WG2023650
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.07 25 03/15/2023 16:37 WG2023463
(S) a,a,a-Trifluorotoluene(FID) 98.3 77.0-120 03/15/2023 16:37 WG2023463
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0613 1 03/15/2023 16:22 WG2023837
Acrylonitrile ND 0.0153 1 03/15/2023 16:22 WG2023837
Benzene ND 0.00123 1 03/15/2023 16:22 WG2023837
Bromobenzene ND 0.0153 1 03/15/2023 16:22 WG2023837
Bromodichloromethane ND 0.00307 1 03/15/2023 16:22 WG2023837
Bromoform ND 0.0307 1 03/15/2023 16:22 WG2023837
Bromomethane ND 0.0153 1 03/15/2023 16:22 WG2023837
n-Butylbenzene ND 0.0153 1 03/15/2023 16:22 WG2023837
sec-Butylbenzene ND 0.0153 1 03/15/2023 16:22 WG2023837
tert-Butylbenzene ND 0.00613 1 03/15/2023 16:22 WG2023837
Carbon tetrachloride ND 0.00613 1 03/15/2023 16:22 WG2023837
Chlorobenzene ND 0.00307 1 03/15/2023 16:22 WG2023837
Chlorodibromomethane ND 0.00307 1 03/15/2023 16:22 WG2023837
Chloroethane ND 0.00613 1 03/15/2023 16:22 WG2023837
Chloroform ND 0.00307 1 03/15/2023 16:22 WG2023837
Chloromethane ND 0.0153 1 03/15/2023 16:22 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1594238
CS-2
Collected date/time: 03/10/23 10:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00307 1 03/15/2023 16:22 WG2023837
4-Chlorotoluene ND 0.00613 1 03/15/2023 16:22 WG2023837
1,2-Dibromo-3-Chloropropane ND 0.0307 1 03/15/2023 16:22 WG2023837
1,2-Dibromoethane ND 0.00307 1 03/15/2023 16:22 WG2023837
Dibromomethane ND 0.00613 1 03/15/2023 16:22 WG2023837
1,2-Dichlorobenzene ND 0.00613 1 03/15/2023 16:22 WG2023837
1,3-Dichlorobenzene ND 0.00613 1 03/15/2023 16:22 WG2023837
1,4-Dichlorobenzene ND 0.00613 1 03/15/2023 16:22 WG2023837
Dichlorodifluoromethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,1-Dichloroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,2-Dichloroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,1-Dichloroethene ND 0.00307 1 03/15/2023 16:22 WG2023837
cis-1,2-Dichloroethene ND 0.00307 1 03/15/2023 16:22 WG2023837
trans-1,2-Dichloroethene ND 0.00613 1 03/15/2023 16:22 WG2023837
1,2-Dichloropropane ND 0.00613 1 03/15/2023 16:22 WG2023837
1,1-Dichloropropene ND 0.00307 1 03/15/2023 16:22 WG2023837
1,3-Dichloropropane ND 0.00613 1 03/15/2023 16:22 WG2023837
cis-1,3-Dichloropropene ND 0.00307 1 03/15/2023 16:22 WG2023837
trans-1,3-Dichloropropene ND 0.00613 1 03/15/2023 16:22 WG2023837
2,2-Dichloropropane ND 0.00307 1 03/15/2023 16:22 WG2023837
Di-isopropyl ether ND 0.00123 1 03/15/2023 16:22 WG2023837
Ethylbenzene ND 0.00307 1 03/15/2023 16:22 WG2023837
Hexachloro-1,3-butadiene ND 0.0307 1 03/15/2023 16:22 WG2023837
Isopropylbenzene ND 0.00307 1 03/15/2023 16:22 WG2023837
p-Isopropyltoluene ND 0.00613 1 03/15/2023 16:22 WG2023837
2-Butanone (MEK)ND 0.123 1 03/15/2023 16:22 WG2023837
Methylene Chloride ND 0.0307 1 03/15/2023 16:22 WG2023837
4-Methyl-2-pentanone (MIBK) ND 0.0307 1 03/15/2023 16:22 WG2023837
Methyl tert-butyl ether ND 0.00123 1 03/15/2023 16:22 WG2023837
Naphthalene ND 0.0153 1 03/15/2023 16:22 WG2023837
n-Propylbenzene ND 0.00613 1 03/15/2023 16:22 WG2023837
Styrene ND 0.0153 1 03/15/2023 16:22 WG2023837
1,1,1,2-Tetrachloroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,1,2,2-Tetrachloroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,1,2-Trichlorotrifluoroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
Tetrachloroethene ND 0.00307 1 03/15/2023 16:22 WG2023837
Toluene ND 0.00613 1 03/15/2023 16:22 WG2023837
1,2,3-Trichlorobenzene ND 0.0153 1 03/15/2023 16:22 WG2023837
1,2,4-Trichlorobenzene ND 0.0153 1 03/15/2023 16:22 WG2023837
1,1,1-Trichloroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,1,2-Trichloroethane ND 0.00307 1 03/15/2023 16:22 WG2023837
Trichloroethene ND 0.00123 1 03/15/2023 16:22 WG2023837
Trichlorofluoromethane ND 0.00307 1 03/15/2023 16:22 WG2023837
1,2,3-Trichloropropane ND 0.0153 1 03/15/2023 16:22 WG2023837
1,2,4-Trimethylbenzene 0.0107 0.00613 1 03/15/2023 16:22 WG2023837
1,2,3-Trimethylbenzene 0.00996 0.00613 1 03/15/2023 16:22 WG2023837
1,3,5-Trimethylbenzene 0.00793 0.00613 1 03/15/2023 16:22 WG2023837
Vinyl chloride ND 0.00307 1 03/15/2023 16:22 WG2023837
Xylenes, Total 0.0227 0.00797 1 03/15/2023 16:22 WG2023837
(S) Toluene-d8 110 75.0-131 03/15/2023 16:22 WG2023837
(S) 4-Bromofluorobenzene 113 67.0-138 03/15/2023 16:22 WG2023837
(S) 1,2-Dichloroethane-d4 90.9 70.0-130 03/15/2023 16:22 WG2023837
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1594238
CS-2
Collected date/time: 03/10/23 10:15
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.39 1 03/21/2023 09:03 WG2026270
C28-C40 Oil Range ND 4.39 1 03/21/2023 09:03 WG2026270
(S) o-Terphenyl 61.1 18.0-148 03/21/2023 09:03 WG2026270
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0373 1 03/21/2023 11:28 WG2026234
PCB 1221 ND 0.0373 1 03/21/2023 11:28 WG2026234
PCB 1232 ND 0.0373 1 03/21/2023 11:28 WG2026234
PCB 1242 ND 0.0373 1 03/21/2023 11:28 WG2026234
PCB 1248 ND 0.0187 1 03/21/2023 11:28 WG2026234
PCB 1254 ND 0.0187 1 03/21/2023 11:28 WG2026234
PCB 1260 ND 0.0187 1 03/21/2023 11:28 WG2026234
(S) Decachlorobiphenyl 61.5 10.0-135 03/21/2023 11:28 WG2026234
(S) Tetrachloro-m-xylene 68.6 10.0-139 03/21/2023 11:28 WG2026234
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0365 1 03/21/2023 20:10 WG2026297
Acenaphthylene ND 0.0365 1 03/21/2023 20:10 WG2026297
Anthracene ND 0.0365 1 03/21/2023 20:10 WG2026297
Benzidine ND 1.83 1 03/21/2023 20:10 WG2026297
Benzo(a)anthracene ND 0.0365 1 03/21/2023 20:10 WG2026297
Benzo(b)fluoranthene ND 0.0365 1 03/21/2023 20:10 WG2026297
Benzo(k)fluoranthene ND 0.0365 1 03/21/2023 20:10 WG2026297
Benzo(g,h,i)perylene ND 0.0365 1 03/21/2023 20:10 WG2026297
Benzo(a)pyrene ND 0.0365 1 03/21/2023 20:10 WG2026297
Bis(2-chlorethoxy)methane ND 0.365 1 03/21/2023 20:10 WG2026297
Bis(2-chloroethyl)ether ND 0.365 1 03/21/2023 20:10 WG2026297
2,2-Oxybis(1-Chloropropane) ND 0.365 1 03/21/2023 20:10 WG2026297
4-Bromophenyl-phenylether ND 0.365 1 03/21/2023 20:10 WG2026297
2-Chloronaphthalene ND 0.0365 1 03/21/2023 20:10 WG2026297
4-Chlorophenyl-phenylether ND 0.365 1 03/21/2023 20:10 WG2026297
Chrysene ND 0.0365 1 03/21/2023 20:10 WG2026297
Dibenz(a,h)anthracene ND 0.0365 1 03/21/2023 20:10 WG2026297
3,3-Dichlorobenzidine ND 0.365 1 03/21/2023 20:10 WG2026297
2,4-Dinitrotoluene ND 0.365 1 03/21/2023 20:10 WG2026297
2,6-Dinitrotoluene ND 0.365 1 03/21/2023 20:10 WG2026297
Fluoranthene ND 0.0365 1 03/21/2023 20:10 WG2026297
Fluorene ND 0.0365 1 03/21/2023 20:10 WG2026297
Hexachlorobenzene ND 0.365 1 03/21/2023 20:10 WG2026297
Hexachloro-1,3-butadiene ND 0.365 1 03/21/2023 20:10 WG2026297
Hexachlorocyclopentadiene ND 0.365 1 03/21/2023 20:10 WG2026297
Hexachloroethane ND 0.365 1 03/21/2023 20:10 WG2026297
Indeno(1,2,3-cd)pyrene ND 0.0365 1 03/21/2023 20:10 WG2026297
Isophorone ND 0.365 1 03/21/2023 20:10 WG2026297
Naphthalene ND 0.0365 1 03/21/2023 20:10 WG2026297
Nitrobenzene ND 0.365 1 03/21/2023 20:10 WG2026297
n-Nitrosodimethylamine ND 0.365 1 03/21/2023 20:10 WG2026297
n-Nitrosodiphenylamine ND 0.365 1 03/21/2023 20:10 WG2026297
n-Nitrosodi-n-propylamine ND 0.365 1 03/21/2023 20:10 WG2026297
Phenanthrene ND 0.0365 1 03/21/2023 20:10 WG2026297
Benzylbutyl phthalate ND 0.365 1 03/21/2023 20:10 WG2026297
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1594238
CS-2
Collected date/time: 03/10/23 10:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.365 1 03/21/2023 20:10 WG2026297
Di-n-butyl phthalate ND 0.365 1 03/21/2023 20:10 WG2026297
Diethyl phthalate ND 0.365 1 03/21/2023 20:10 WG2026297
Dimethyl phthalate ND 0.365 1 03/21/2023 20:10 WG2026297
Di-n-octyl phthalate ND 0.365 1 03/21/2023 20:10 WG2026297
Pyrene ND 0.0365 1 03/21/2023 20:10 WG2026297
1,2,4-Trichlorobenzene ND 0.365 1 03/21/2023 20:10 WG2026297
4-Chloro-3-methylphenol ND 0.365 1 03/21/2023 20:10 WG2026297
2-Chlorophenol ND 0.365 1 03/21/2023 20:10 WG2026297
2,4-Dichlorophenol ND 0.365 1 03/21/2023 20:10 WG2026297
2,4-Dimethylphenol ND 0.365 1 03/21/2023 20:10 WG2026297
4,6-Dinitro-2-methylphenol ND 0.365 1 03/21/2023 20:10 WG2026297
2,4-Dinitrophenol ND J3 0.365 1 03/21/2023 20:10 WG2026297
2-Nitrophenol ND 0.365 1 03/21/2023 20:10 WG2026297
4-Nitrophenol ND 0.365 1 03/21/2023 20:10 WG2026297
Pentachlorophenol ND 0.365 1 03/21/2023 20:10 WG2026297
Phenol ND 0.365 1 03/21/2023 20:10 WG2026297
2,4,6-Trichlorophenol ND 0.365 1 03/21/2023 20:10 WG2026297
(S) Nitrobenzene-d5 59.9 10.0-122 03/21/2023 20:10 WG2026297
(S) 2-Fluorobiphenyl 65.3 15.0-120 03/21/2023 20:10 WG2026297
(S) p-Terphenyl-d14 67.5 10.0-120 03/21/2023 20:10 WG2026297
(S) Phenol-d5 54.7 10.0-120 03/21/2023 20:10 WG2026297
(S) 2-Fluorophenol 45.7 12.0-120 03/21/2023 20:10 WG2026297
(S) 2,4,6-Tribromophenol 38.8 10.0-127 03/21/2023 20:10 WG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00658 1 03/21/2023 01:46 WG2026298
Acenaphthene ND 0.00658 1 03/21/2023 01:46 WG2026298
Acenaphthylene ND 0.00658 1 03/21/2023 01:46 WG2026298
Benzo(a)anthracene ND 0.00658 1 03/21/2023 01:46 WG2026298
Benzo(a)pyrene ND 0.00658 1 03/21/2023 01:46 WG2026298
Benzo(b)fluoranthene ND 0.00658 1 03/21/2023 01:46 WG2026298
Benzo(g,h,i)perylene ND 0.00658 1 03/21/2023 01:46 WG2026298
Benzo(k)fluoranthene ND 0.00658 1 03/21/2023 01:46 WG2026298
Chrysene ND 0.00658 1 03/21/2023 01:46 WG2026298
Dibenz(a,h)anthracene ND 0.00658 1 03/21/2023 01:46 WG2026298
Fluoranthene ND 0.00658 1 03/21/2023 01:46 WG2026298
Fluorene ND 0.00658 1 03/21/2023 01:46 WG2026298
Indeno(1,2,3-cd)pyrene ND 0.00658 1 03/21/2023 01:46 WG2026298
Naphthalene ND 0.0219 1 03/21/2023 01:46 WG2026298
Phenanthrene ND 0.00658 1 03/21/2023 01:46 WG2026298
Pyrene ND 0.00658 1 03/21/2023 01:46 WG2026298
1-Methylnaphthalene ND 0.0219 1 03/21/2023 01:46 WG2026298
2-Methylnaphthalene ND 0.0219 1 03/21/2023 01:46 WG2026298
2-Chloronaphthalene ND 0.0219 1 03/21/2023 01:46 WG2026298
(S) p-Terphenyl-d14 77.1 23.0-120 03/21/2023 01:46 WG2026298
(S) Nitrobenzene-d5 62.9 14.0-149 03/21/2023 01:46 WG2026298
(S) 2-Fluorobiphenyl 76.0 34.0-125 03/21/2023 01:46 WG2026298
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2023759
Total Solids by Method 2540 G-2011 L1594238-01,02,03,04
Method Blank (MB)
(MB) R3902117-1 03/16/23 07:06
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1594182-21 Original Sample (OS) • Duplicate (DUP)
(OS) L1594182-21 03/16/23 07:06 • (DUP) R3902117-3 03/16/23 07:06
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 89.7 85.7 1 4.53 10
Laboratory Control Sample (LCS)
(LCS) R3902117-2 03/16/23 07:06
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023705
Wet Chemistry by Method 7199 L1594238-01,02
Method Blank (MB)
(MB) R3901876-1 03/16/23 10:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1594120-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1594120-02 03/16/23 11:09 • (DUP) R3901876-3 03/16/23 11:14
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%
Hexavalent Chromium ND ND 1 25.6 P1 20
L1594174-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1594174-03 03/16/23 12:43 • (DUP) R3901876-8 03/16/23 12:48
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3901876-2 03/16/23 10:38
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 9.96 99.6 80.0-120
L1594120-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594120-04 03/16/23 11:35 • (MS) R3901876-4 03/16/23 11:40 • (MSD) R3901876-5 03/16/23 11:45
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Hexavalent Chromium 24.2 ND 22.6 23.6 89.8 94.1 1 75.0-125 4.56 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023705
Wet Chemistry by Method 7199 L1594238-01,02
L1594120-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L1594120-04 03/16/23 11:35 • (MS) R3901876-6 03/16/23 11:51
Spike Amount
(dry)
Original Result
(dry)MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg %%
Hexavalent Chromium 769 ND 822 107 50 75.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2024335
Wet Chemistry by Method 7199 L1594238-03,04
Method Blank (MB)
(MB) R3902382-1 03/17/23 10:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1595209-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1595209-01 03/17/23 10:01 • (DUP) R3902382-3 03/17/23 10:49
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 15.4 20
L1595209-06 Original Sample (OS) • Duplicate (DUP)
(OS) L1595209-06 03/17/23 16:44 • (DUP) R3902382-9 03/17/23 16:49
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium 17.4 15.6 1 10.7 20
Laboratory Control Sample (LCS)
(LCS) R3902382-2 03/17/23 10:30
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 9.80 98.0 80.0-120
L1595209-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1595209-02 03/17/23 10:41 • (MS) R3902382-4 03/17/23 12:24 • (MSD) R3902382-5 03/17/23 12:07
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 24.3 ND 23.4 21.6 95.0 87.7 1 75.0-125 7.87 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2024335
Wet Chemistry by Method 7199 L1594238-03,04
L1595209-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1595209-02 03/17/23 10:41 • (MS) R3902382-6 03/17/23 12:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 782 ND 949 121 50 75.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023712
Mercury by Method 7471A L1594238-01,02,03,04
Method Blank (MB)
(MB) R3901536-1 03/15/23 16:51
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3901536-2 03/15/23 16:53
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.455 91.0 80.0-120
L1594160-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594160-01 03/15/23 16:55 • (MS) R3901536-3 03/15/23 16:58 • (MSD) R3901536-4 03/15/23 17:01
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.568 ND 0.612 0.628 108 111 1 75.0-125 2.55 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023650
Metals (ICP) by Method 6010B L1594238-01,02,03,04
Method Blank (MB)
(MB) R3901895-1 03/16/23 12:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3901895-2 03/16/23 12:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 106 106 80.0-120
Arsenic 100 102 102 80.0-120
Beryllium 100 107 107 80.0-120
Cadmium 100 107 107 80.0-120
Chromium 100 105 105 80.0-120
Copper 100 115 115 80.0-120
Lead 100 104 104 80.0-120
Nickel 100 105 105 80.0-120
Selenium 100 108 108 80.0-120
Silver 20.0 20.6 103 80.0-120
Thallium 100 106 106 80.0-120
Zinc 100 99.3 99.3 80.0-120
L1594160-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594160-01 03/16/23 12:38 • (MS) R3901895-5 03/16/23 12:46 • (MSD) R3901895-6 03/16/23 12:48
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 114 ND 86.6 79.8 76.3 70.3 1 75.0-125 J6 8.20 20
Arsenic 114 ND 120 112 106 98.9 1 75.0-125 6.82 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023650
Metals (ICP) by Method 6010B L1594238-01,02,03,04
L1594160-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594160-01 03/16/23 12:38 • (MS) R3901895-5 03/16/23 12:46 • (MSD) R3901895-6 03/16/23 12:48
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 114 0.378 120 112 105 98.0 1 75.0-125 7.06 20
Cadmium 114 ND 126 118 111 104 1 75.0-125 6.91 20
Chromium 114 13.6 130 121 103 94.8 1 75.0-125 7.17 20
Copper 114 24.1 162 152 122 113 1 75.0-125 6.37 20
Lead 114 4.82 126 118 106 100 1 75.0-125 5.85 20
Nickel 114 54.3 168 158 100 91.3 1 75.0-125 6.21 20
Selenium 114 ND 124 116 109 102 1 75.0-125 7.01 20
Silver 22.7 ND 24.1 22.6 106 99.6 1 75.0-125 6.46 20
Thallium 114 ND 123 115 109 101 1 75.0-125 7.16 20
Zinc 114 34.0 143 138 95.8 92.0 1 75.0-125 3.08 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023463
Volatile Organic Compounds (GC) by Method 8015D/GRO L1594238-01,02,03,04
Method Blank (MB)
(MB) R3902197-2 03/15/23 10:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.550 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)96.8 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3902197-1 03/15/23 09:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.36 97.5 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 101 77.0-120
L1594167-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594167-04 03/15/23 16:58 • (MS) R3902197-3 03/15/23 18:20 • (MSD) R3902197-4 03/15/23 18:40
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 702 219 780 795 80.0 82.1 100 10.0-151 1.87 28
(S)
a,a,a-Trifluorotoluene(FID) 103 104 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023837
Volatile Organic Compounds (GC/MS) by Method 8260B L1594238-01,02,03,04
Method Blank (MB)
(MB) R3901875-3 03/15/23 13:09
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023837
Volatile Organic Compounds (GC/MS) by Method 8260B L1594238-01,02,03,04
Method Blank (MB)
(MB) R3901875-3 03/15/23 13:09
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00640 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 121 75.0-131
(S) 4-Bromofluorobenzene 83.7 67.0-138
(S) 1,2-Dichloroethane-d4 92.6 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901875-1 03/15/23 11:22 • (LCSD) R3901875-2 03/15/23 11:44
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.494 0.496 79.0 79.4 10.0-160 0.404 31
Acrylonitrile 0.625 0.575 0.563 92.0 90.1 45.0-153 2.11 22
Benzene 0.125 0.109 0.108 87.2 86.4 70.0-123 0.922 20
Bromobenzene 0.125 0.105 0.115 84.0 92.0 73.0-121 9.09 20
Bromodichloromethane 0.125 0.113 0.111 90.4 88.8 73.0-121 1.79 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023837
Volatile Organic Compounds (GC/MS) by Method 8260B L1594238-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901875-1 03/15/23 11:22 • (LCSD) R3901875-2 03/15/23 11:44
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.138 0.136 110 109 64.0-132 1.46 20
Bromomethane 0.125 0.0855 0.0919 68.4 73.5 56.0-147 7.22 20
n-Butylbenzene 0.125 0.123 0.129 98.4 103 68.0-135 4.76 20
sec-Butylbenzene 0.125 0.116 0.114 92.8 91.2 74.0-130 1.74 20
tert-Butylbenzene 0.125 0.111 0.111 88.8 88.8 75.0-127 0.000 20
Carbon tetrachloride 0.125 0.113 0.115 90.4 92.0 66.0-128 1.75 20
Chlorobenzene 0.125 0.121 0.119 96.8 95.2 76.0-128 1.67 20
Chlorodibromomethane 0.125 0.134 0.133 107 106 74.0-127 0.749 20
Chloroethane 0.125 0.102 0.101 81.6 80.8 61.0-134 0.985 20
Chloroform 0.125 0.113 0.111 90.4 88.8 72.0-123 1.79 20
Chloromethane 0.125 0.102 0.0990 81.6 79.2 51.0-138 2.99 20
2-Chlorotoluene 0.125 0.118 0.119 94.4 95.2 75.0-124 0.844 20
4-Chlorotoluene 0.125 0.113 0.118 90.4 94.4 75.0-124 4.33 20
1,2-Dibromo-3-Chloropropane 0.125 0.139 0.135 111 108 59.0-130 2.92 20
1,2-Dibromoethane 0.125 0.125 0.121 100 96.8 74.0-128 3.25 20
Dibromomethane 0.125 0.111 0.114 88.8 91.2 75.0-122 2.67 20
1,2-Dichlorobenzene 0.125 0.127 0.134 102 107 76.0-124 5.36 20
1,3-Dichlorobenzene 0.125 0.128 0.125 102 100 76.0-125 2.37 20
1,4-Dichlorobenzene 0.125 0.128 0.134 102 107 77.0-121 4.58 20
Dichlorodifluoromethane 0.125 0.0944 0.0919 75.5 73.5 43.0-156 2.68 20
1,1-Dichloroethane 0.125 0.113 0.113 90.4 90.4 70.0-127 0.000 20
1,2-Dichloroethane 0.125 0.0983 0.0978 78.6 78.2 65.0-131 0.510 20
1,1-Dichloroethene 0.125 0.112 0.114 89.6 91.2 65.0-131 1.77 20
cis-1,2-Dichloroethene 0.125 0.113 0.114 90.4 91.2 73.0-125 0.881 20
trans-1,2-Dichloroethene 0.125 0.111 0.110 88.8 88.0 71.0-125 0.905 20
1,2-Dichloropropane 0.125 0.105 0.104 84.0 83.2 74.0-125 0.957 20
1,1-Dichloropropene 0.125 0.112 0.112 89.6 89.6 73.0-125 0.000 20
1,3-Dichloropropane 0.125 0.127 0.120 102 96.0 80.0-125 5.67 20
cis-1,3-Dichloropropene 0.125 0.115 0.109 92.0 87.2 76.0-127 5.36 20
trans-1,3-Dichloropropene 0.125 0.129 0.126 103 101 73.0-127 2.35 20
2,2-Dichloropropane 0.125 0.112 0.113 89.6 90.4 59.0-135 0.889 20
Di-isopropyl ether 0.125 0.102 0.104 81.6 83.2 60.0-136 1.94 20
Ethylbenzene 0.125 0.117 0.120 93.6 96.0 74.0-126 2.53 20
Hexachloro-1,3-butadiene 0.125 0.0945 0.112 75.6 89.6 57.0-150 16.9 20
Isopropylbenzene 0.125 0.132 0.134 106 107 72.0-127 1.50 20
p-Isopropyltoluene 0.125 0.118 0.120 94.4 96.0 72.0-133 1.68 20
2-Butanone (MEK)0.625 0.674 0.657 108 105 30.0-160 2.55 24
Methylene Chloride 0.125 0.116 0.121 92.8 96.8 68.0-123 4.22 20
4-Methyl-2-pentanone (MIBK) 0.625 0.579 0.583 92.6 93.3 56.0-143 0.688 20
Methyl tert-butyl ether 0.125 0.105 0.106 84.0 84.8 66.0-132 0.948 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2023837
Volatile Organic Compounds (GC/MS) by Method 8260B L1594238-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901875-1 03/15/23 11:22 • (LCSD) R3901875-2 03/15/23 11:44
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.121 0.131 96.8 105 59.0-130 7.94 20
n-Propylbenzene 0.125 0.115 0.121 92.0 96.8 74.0-126 5.08 20
Styrene 0.125 0.113 0.118 90.4 94.4 72.0-127 4.33 20
1,1,1,2-Tetrachloroethane 0.125 0.128 0.129 102 103 74.0-129 0.778 20
1,1,2,2-Tetrachloroethane 0.125 0.112 0.112 89.6 89.6 68.0-128 0.000 20
1,1,2-Trichlorotrifluoroethane 0.125 0.113 0.114 90.4 91.2 61.0-139 0.881 20
Tetrachloroethene 0.125 0.124 0.125 99.2 100 70.0-136 0.803 20
Toluene 0.125 0.127 0.128 102 102 75.0-121 0.784 20
1,2,3-Trichlorobenzene 0.125 0.115 0.125 92.0 100 59.0-139 8.33 20
1,2,4-Trichlorobenzene 0.125 0.121 0.133 96.8 106 62.0-137 9.45 20
1,1,1-Trichloroethane 0.125 0.114 0.114 91.2 91.2 69.0-126 0.000 20
1,1,2-Trichloroethane 0.125 0.120 0.123 96.0 98.4 78.0-123 2.47 20
Trichloroethene 0.125 0.115 0.118 92.0 94.4 76.0-126 2.58 20
Trichlorofluoromethane 0.125 0.101 0.115 80.8 92.0 61.0-142 13.0 20
1,2,3-Trichloropropane 0.125 0.117 0.117 93.6 93.6 67.0-129 0.000 20
1,2,4-Trimethylbenzene 0.125 0.117 0.117 93.6 93.6 70.0-126 0.000 20
1,2,3-Trimethylbenzene 0.125 0.117 0.121 93.6 96.8 74.0-124 3.36 20
1,3,5-Trimethylbenzene 0.125 0.116 0.117 92.8 93.6 73.0-127 0.858 20
Vinyl chloride 0.125 0.100 0.101 80.0 80.8 63.0-134 0.995 20
Xylenes, Total 0.375 0.370 0.367 98.7 97.9 72.0-127 0.814 20
(S) Toluene-d8 107 108 75.0-131
(S) 4-Bromofluorobenzene 96.8 99.9 67.0-138
(S) 1,2-Dichloroethane-d4 96.9 94.2 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026270
Semi-Volatile Organic Compounds (GC) by Method 8015 L1594238-01,02,03,04
Method Blank (MB)
(MB) R3903313-2 03/20/23 22:27
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 69.4 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3903313-1 03/20/23 22:14
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 32.5 65.0 50.0-150
(S) o-Terphenyl 75.7 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026234
Polychlorinated Biphenyls (GC) by Method 8082 L1594238-01,02,03,04
Method Blank (MB)
(MB) R3904224-1 03/21/23 10:51
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 64.1 10.0-135
(S) Tetrachloro-m-xylene 64.4 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3904224-2 03/21/23 11:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.148 88.6 36.0-141
PCB 1260 0.167 0.157 94.0 37.0-145
(S) Decachlorobiphenyl 68.2 10.0-135
(S) Tetrachloro-m-xylene 66.4 10.0-139
L1594973-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594973-01 03/21/23 11:56 • (MS) R3904224-3 03/21/23 12:05 • (MSD) R3904224-4 03/21/23 12:14
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.177 ND 0.135 0.160 76.6 90.4 1 10.0-160 16.5 37
PCB 1260 0.177 ND 0.143 0.174 80.8 98.8 1 10.0-160 20.0 38
(S) Decachlorobiphenyl 60.7 71.5 10.0-135
(S) Tetrachloro-m-xylene 61.0 73.7 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1594238-01,02,03,04
Method Blank (MB)
(MB) R3904062-2 03/21/23 17:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1594238-01,02,03,04
Method Blank (MB)
(MB) R3904062-2 03/21/23 17:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 59.8 10.0-122
(S) 2-Fluorobiphenyl 67.3 15.0-120
(S) p-Terphenyl-d14 73.0 10.0-120
(S) Phenol-d5 59.3 10.0-120
(S) 2-Fluorophenol 61.7 12.0-120
(S) 2,4,6-Tribromophenol 68.9 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3904062-1 03/21/23 16:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.481 72.2 38.0-120
Acenaphthylene 0.666 0.516 77.5 40.0-120
Anthracene 0.666 0.464 69.7 42.0-120
Benzidine 1.33 0.394 29.6 10.0-120
Benzo(a)anthracene 0.666 0.500 75.1 44.0-120
Benzo(b)fluoranthene 0.666 0.535 80.3 43.0-120
Benzo(k)fluoranthene 0.666 0.505 75.8 44.0-120
Benzo(g,h,i)perylene 0.666 0.515 77.3 43.0-120
Benzo(a)pyrene 0.666 0.567 85.1 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.381 57.2 20.0-120
Bis(2-chloroethyl)ether 0.666 0.494 74.2 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.427 64.1 23.0-120
4-Bromophenyl-phenylether 0.666 0.455 68.3 40.0-120
2-Chloronaphthalene 0.666 0.446 67.0 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1594238-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3904062-1 03/21/23 16:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.497 74.6 40.0-120
Chrysene 0.666 0.499 74.9 43.0-120
Dibenz(a,h)anthracene 0.666 0.515 77.3 44.0-120
3,3-Dichlorobenzidine 1.33 0.869 65.3 28.0-120
2,4-Dinitrotoluene 0.666 0.556 83.5 45.0-120
2,6-Dinitrotoluene 0.666 0.470 70.6 42.0-120
Fluoranthene 0.666 0.497 74.6 44.0-120
Fluorene 0.666 0.491 73.7 41.0-120
Hexachlorobenzene 0.666 0.506 76.0 39.0-120
Hexachloro-1,3-butadiene 0.666 0.370 55.6 15.0-120
Hexachlorocyclopentadiene 0.666 0.435 65.3 15.0-120
Hexachloroethane 0.666 0.415 62.3 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.479 71.9 45.0-120
Isophorone 0.666 0.368 55.3 23.0-120
Naphthalene 0.666 0.374 56.2 18.0-120
Nitrobenzene 0.666 0.370 55.6 17.0-120
n-Nitrosodimethylamine 0.666 0.442 66.4 10.0-125
n-Nitrosodiphenylamine 0.666 0.478 71.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.458 68.8 26.0-120
Phenanthrene 0.666 0.452 67.9 42.0-120
Benzylbutyl phthalate 0.666 0.510 76.6 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.515 77.3 41.0-120
Di-n-butyl phthalate 0.666 0.494 74.2 43.0-120
Diethyl phthalate 0.666 0.507 76.1 43.0-120
Dimethyl phthalate 0.666 0.479 71.9 43.0-120
Di-n-octyl phthalate 0.666 0.511 76.7 40.0-120
Pyrene 0.666 0.500 75.1 41.0-120
1,2,4-Trichlorobenzene 0.666 0.367 55.1 17.0-120
4-Chloro-3-methylphenol 0.666 0.382 57.4 28.0-120
2-Chlorophenol 0.666 0.458 68.8 28.0-120
2,4-Dichlorophenol 0.666 0.377 56.6 25.0-120
2,4-Dimethylphenol 0.666 0.379 56.9 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.444 66.7 16.0-120
2,4-Dinitrophenol 0.666 0.387 58.1 10.0-120
2-Nitrophenol 0.666 0.428 64.3 20.0-120
4-Nitrophenol 0.666 0.519 77.9 27.0-120
Pentachlorophenol 0.666 0.417 62.6 29.0-120
Phenol 0.666 0.426 64.0 28.0-120
2,4,6-Trichlorophenol 0.666 0.463 69.5 37.0-120
(S) Nitrobenzene-d5 58.6 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1594238-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3904062-1 03/21/23 16:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 75.7 15.0-120
(S) p-Terphenyl-d14 75.7 10.0-120
(S) Phenol-d5 70.0 10.0-120
(S) 2-Fluorophenol 73.1 12.0-120
(S) 2,4,6-Tribromophenol 92.0 10.0-127
L1594238-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594238-04 03/21/23 20:10 • (MS) R3904062-3 03/21/23 20:31 • (MSD) R3904062-4 03/21/23 20:53
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.696 ND 0.428 0.431 61.5 62.0 1 18.0-120 0.766 32
Acenaphthylene 0.696 ND 0.455 0.461 65.5 66.2 1 25.0-120 1.20 32
Anthracene 0.696 ND 0.397 0.406 57.1 58.4 1 22.0-120 2.19 29
Benzidine 1.39 ND ND ND 46.1 58.5 1 10.0-120 23.6 40
Benzo(a)anthracene 0.696 ND 0.440 0.438 63.2 62.9 1 25.0-120 0.500 29
Benzo(b)fluoranthene 0.696 ND 0.452 0.459 65.0 65.9 1 19.0-122 1.45 31
Benzo(k)fluoranthene 0.696 ND 0.453 0.443 65.1 63.7 1 23.0-120 2.20 30
Benzo(g,h,i)perylene 0.696 ND 0.452 0.460 65.0 66.1 1 10.0-120 1.68 33
Benzo(a)pyrene 0.696 ND 0.483 0.487 69.4 70.0 1 24.0-120 0.905 30
Bis(2-chlorethoxy)methane 0.696 ND ND ND 47.8 47.5 1 10.0-120 0.662 34
Bis(2-chloroethyl)ether 0.696 ND 0.442 0.438 63.6 62.9 1 10.0-120 0.998 40
2,2-Oxybis(1-Chloropropane) 0.696 ND 0.371 0.385 53.3 55.4 1 10.0-120 3.77 40
4-Bromophenyl-phenylether 0.696 ND 0.387 0.407 55.7 58.5 1 27.0-120 4.97 30
2-Chloronaphthalene 0.696 ND 0.393 0.393 56.5 56.5 1 20.0-120 0.000 32
4-Chlorophenyl-phenylether 0.696 ND 0.439 0.428 63.1 61.5 1 24.0-120 2.53 29
Chrysene 0.696 ND 0.447 0.433 64.2 62.3 1 21.0-120 2.99 29
Dibenz(a,h)anthracene 0.696 ND 0.452 0.449 65.0 64.5 1 10.0-120 0.731 32
3,3-Dichlorobenzidine 1.39 ND 0.819 0.842 58.7 60.4 1 10.0-120 2.78 34
2,4-Dinitrotoluene 0.696 ND 0.476 0.469 68.5 67.4 1 30.0-120 1.63 31
2,6-Dinitrotoluene 0.696 ND 0.411 0.418 59.1 60.1 1 25.0-120 1.59 31
Fluoranthene 0.696 ND 0.426 0.435 61.2 62.5 1 18.0-126 2.04 32
Fluorene 0.696 ND 0.429 0.435 61.7 62.5 1 25.0-120 1.27 30
Hexachlorobenzene 0.696 ND 0.435 0.443 62.5 63.7 1 27.0-120 2.00 28
Hexachloro-1,3-butadiene 0.696 ND ND ND 48.6 50.8 1 10.0-120 4.44 38
Hexachlorocyclopentadiene 0.696 ND ND ND 45.6 36.8 1 10.0-120 21.5 40
Hexachloroethane 0.696 ND ND 0.372 52.2 53.5 1 10.0-120 2.39 40
Indeno(1,2,3-cd)pyrene 0.696 ND 0.425 0.417 61.0 59.9 1 10.0-120 1.83 32
Isophorone 0.696 ND ND ND 46.7 48.4 1 13.0-120 3.65 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026297
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1594238-01,02,03,04
L1594238-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594238-04 03/21/23 20:10 • (MS) R3904062-3 03/21/23 20:31 • (MSD) R3904062-4 03/21/23 20:53
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.696 ND 0.342 0.343 49.2 49.4 1 10.0-120 0.320 35
Nitrobenzene 0.696 ND ND ND 47.0 48.4 1 10.0-120 2.98 36
n-Nitrosodimethylamine 0.696 ND 0.371 0.377 53.3 54.3 1 10.0-127 1.76 40
n-Nitrosodiphenylamine 0.696 ND 0.406 0.419 58.4 60.3 1 17.0-120 3.19 29
n-Nitrosodi-n-propylamine 0.696 ND 0.390 0.395 56.0 56.8 1 10.0-120 1.40 37
Phenanthrene 0.696 ND 0.390 0.392 56.0 56.3 1 17.0-120 0.562 31
Benzylbutyl phthalate 0.696 ND 0.436 0.436 62.6 62.6 1 23.0-120 0.000 30
Bis(2-ethylhexyl)phthalate 0.696 ND 0.464 0.454 66.7 65.3 1 17.0-126 2.15 30
Di-n-butyl phthalate 0.696 ND 0.416 0.424 59.8 60.9 1 30.0-120 1.83 29
Diethyl phthalate 0.696 ND 0.441 0.440 63.4 63.2 1 26.0-120 0.249 28
Dimethyl phthalate 0.696 ND 0.422 0.422 60.7 60.7 1 25.0-120 0.000 29
Di-n-octyl phthalate 0.696 ND 0.453 0.441 65.1 63.4 1 21.0-123 2.70 29
Pyrene 0.696 ND 0.447 0.437 64.2 62.8 1 16.0-121 2.24 32
1,2,4-Trichlorobenzene 0.696 ND ND ND 45.7 48.3 1 12.0-120 5.37 37
4-Chloro-3-methylphenol 0.696 ND ND ND 47.2 45.0 1 15.0-120 4.79 30
2-Chlorophenol 0.696 ND ND ND 42.1 41.5 1 15.0-120 1.51 37
2,4-Dichlorophenol 0.696 ND ND ND 31.9 29.8 1 20.0-120 6.65 31
2,4-Dimethylphenol 0.696 ND ND ND 48.9 50.0 1 10.0-120 2.23 33
4,6-Dinitro-2-methylphenol 0.696 ND ND ND 47.9 32.3 1 10.0-120 38.9 39
2,4-Dinitrophenol 0.696 ND 0.375 ND 53.9 28.9 1 10.0-121 J3 60.6 40
2-Nitrophenol 0.696 ND ND ND 30.3 30.4 1 12.0-120 0.519 39
4-Nitrophenol 0.696 ND ND ND 34.7 36.6 1 10.0-137 5.31 32
Pentachlorophenol 0.696 ND ND ND 35.0 35.8 1 10.0-160 2.23 31
Phenol 0.696 ND ND ND 49.8 50.8 1 12.0-120 1.88 38
2,4,6-Trichlorophenol 0.696 ND ND ND 29.7 32.5 1 19.0-120 9.14 32
(S) Nitrobenzene-d5 51.4 50.8 10.0-122
(S) 2-Fluorobiphenyl 67.5 66.9 15.0-120
(S) p-Terphenyl-d14 65.3 64.7 10.0-120
(S) Phenol-d5 55.8 55.8 10.0-120
(S) 2-Fluorophenol 44.6 44.5 12.0-120
(S) 2,4,6-Tribromophenol 49.1 48.7 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026014
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1594238-01
Method Blank (MB)
(MB) R3903465-2 03/20/23 17:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 106 23.0-120
(S) Nitrobenzene-d5 111 14.0-149
(S) 2-Fluorobiphenyl 100 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3903465-1 03/20/23 17:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0639 79.9 50.0-126
Acenaphthene 0.0800 0.0591 73.9 50.0-120
Acenaphthylene 0.0800 0.0616 77.0 50.0-120
Benzo(a)anthracene 0.0800 0.0697 87.1 45.0-120
Benzo(a)pyrene 0.0800 0.0551 68.9 42.0-120
Benzo(b)fluoranthene 0.0800 0.0586 73.3 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0571 71.4 45.0-125
Benzo(k)fluoranthene 0.0800 0.0568 71.0 49.0-125
Chrysene 0.0800 0.0640 80.0 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0614 76.8 47.0-125
Fluoranthene 0.0800 0.0643 80.4 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026014
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1594238-01
Laboratory Control Sample (LCS)
(LCS) R3903465-1 03/20/23 17:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0639 79.9 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0686 85.8 46.0-125
Naphthalene 0.0800 0.0572 71.5 50.0-120
Phenanthrene 0.0800 0.0600 75.0 47.0-120
Pyrene 0.0800 0.0610 76.3 43.0-123
1-Methylnaphthalene 0.0800 0.0584 73.0 51.0-121
2-Methylnaphthalene 0.0800 0.0606 75.8 50.0-120
2-Chloronaphthalene 0.0800 0.0571 71.4 50.0-120
(S) p-Terphenyl-d14 90.9 23.0-120
(S) Nitrobenzene-d5 109 14.0-149
(S) 2-Fluorobiphenyl 90.8 34.0-125
L1594238-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594238-01 03/20/23 23:39 • (MS) R3903465-3 03/20/23 23:58 • (MSD) R3903465-4 03/21/23 00:18
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0920 ND 0.0858 0.0865 86.3 87.1 1 10.0-145 0.817 30
Acenaphthene 0.0920 ND 0.0691 0.0771 75.1 83.8 1 14.0-127 10.9 27
Acenaphthylene 0.0920 ND 0.0728 0.0822 79.1 89.3 1 21.0-124 12.1 25
Benzo(a)anthracene 0.0920 0.144 0.338 0.114 210 0.000 1 10.0-139 J5 J3 J6 98.8 30
Benzo(a)pyrene 0.0920 0.112 0.282 0.102 185 0.000 1 10.0-141 J5 J3 J6 93.3 31
Benzo(b)fluoranthene 0.0920 0.0431 0.140 0.0844 105 44.9 1 10.0-140 J3 49.3 36
Benzo(g,h,i)perylene 0.0920 0.0906 0.236 0.113 158 24.4 1 10.0-140 J5 J3 70.4 33
Benzo(k)fluoranthene 0.0920 ND 0.0736 0.0700 73.0 69.1 1 10.0-137 5.07 31
Chrysene 0.0920 0.131 0.461 0.134 358 2.55 1 10.0-145 J5 J3 J6 110 30
Dibenz(a,h)anthracene 0.0920 0.0141 0.0912 0.0806 83.8 72.3 1 10.0-132 12.3 31
Fluoranthene 0.0920 0.0370 0.155 0.0975 128 65.8 1 10.0-153 J3 45.5 33
Fluorene 0.0920 ND 0.0757 0.0840 82.3 91.3 1 11.0-130 10.4 29
Indeno(1,2,3-cd)pyrene 0.0920 0.0299 0.126 0.0940 104 69.6 1 10.0-137 28.8 32
Naphthalene 0.0920 ND 0.0667 0.0757 72.4 82.3 1 10.0-135 12.7 27
Phenanthrene 0.0920 0.0466 0.142 0.116 104 75.6 1 10.0-144 20.0 31
Pyrene 0.0920 0.327 0.626 0.182 324 0.000 1 10.0-148 J5 J3 J6 110 35
1-Methylnaphthalene 0.0920 ND 0.0717 0.0797 77.9 86.6 1 10.0-142 10.5 28
2-Methylnaphthalene 0.0920 ND 0.0763 0.0853 82.9 92.7 1 10.0-137 11.2 28
2-Chloronaphthalene 0.0920 ND 0.0643 0.0721 69.9 78.3 1 29.0-120 11.4 24
(S) p-Terphenyl-d14 79.3 85.3 23.0-120
(S) Nitrobenzene-d5 98.7 113 14.0-149
(S) 2-Fluorobiphenyl 77.6 84.9 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026298
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1594238-02,03,04
Method Blank (MB)
(MB) R3903581-2 03/21/23 01:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 88.4 23.0-120
(S) Nitrobenzene-d5 68.3 14.0-149
(S) 2-Fluorobiphenyl 84.2 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3903581-1 03/21/23 00:54
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0653 81.6 50.0-126
Acenaphthene 0.0800 0.0690 86.3 50.0-120
Acenaphthylene 0.0800 0.0655 81.9 50.0-120
Benzo(a)anthracene 0.0800 0.0677 84.6 45.0-120
Benzo(a)pyrene 0.0800 0.0665 83.1 42.0-120
Benzo(b)fluoranthene 0.0800 0.0740 92.5 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0667 83.4 45.0-125
Benzo(k)fluoranthene 0.0800 0.0733 91.6 49.0-125
Chrysene 0.0800 0.0695 86.9 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0633 79.1 47.0-125
Fluoranthene 0.0800 0.0713 89.1 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2026298
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1594238-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3903581-1 03/21/23 00:54
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0721 90.1 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0713 89.1 46.0-125
Naphthalene 0.0800 0.0694 86.8 50.0-120
Phenanthrene 0.0800 0.0653 81.6 47.0-120
Pyrene 0.0800 0.0737 92.1 43.0-123
1-Methylnaphthalene 0.0800 0.0637 79.6 51.0-121
2-Methylnaphthalene 0.0800 0.0645 80.6 50.0-120
2-Chloronaphthalene 0.0800 0.0657 82.1 50.0-120
(S) p-Terphenyl-d14 88.2 23.0-120
(S) Nitrobenzene-d5 73.0 14.0-149
(S) 2-Fluorobiphenyl 78.2 34.0-125
L1594238-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1594238-04 03/21/23 01:46 • (MS) R3903581-3 03/21/23 02:03 • (MSD) R3903581-4 03/21/23 02:21
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0860 ND 0.0687 0.0701 79.8 79.9 1 10.0-145 2.06 30
Acenaphthene 0.0860 ND 0.0752 0.0751 87.4 85.5 1 14.0-127 0.146 27
Acenaphthylene 0.0860 ND 0.0776 0.0732 90.2 83.4 1 21.0-124 5.82 25
Benzo(a)anthracene 0.0860 ND 0.0722 0.0712 83.9 81.1 1 10.0-139 1.38 30
Benzo(a)pyrene 0.0860 ND 0.0827 0.0803 96.2 91.5 1 10.0-141 2.96 31
Benzo(b)fluoranthene 0.0860 ND 0.0779 0.0714 90.6 81.4 1 10.0-140 8.67 36
Benzo(g,h,i)perylene 0.0860 ND 0.0706 0.0658 82.0 75.0 1 10.0-140 6.92 33
Benzo(k)fluoranthene 0.0860 ND 0.0776 0.0714 90.2 81.4 1 10.0-137 8.25 31
Chrysene 0.0860 ND 0.0760 0.0736 88.4 83.9 1 10.0-145 3.23 30
Dibenz(a,h)anthracene 0.0860 ND 0.0695 0.0654 80.7 74.5 1 10.0-132 6.02 31
Fluoranthene 0.0860 ND 0.0843 0.0762 98.0 86.8 1 10.0-153 10.1 33
Fluorene 0.0860 ND 0.0785 0.0794 91.2 90.5 1 11.0-130 1.25 29
Indeno(1,2,3-cd)pyrene 0.0860 ND 0.0785 0.0746 91.2 85.0 1 10.0-137 5.02 32
Naphthalene 0.0860 ND 0.0741 0.0738 86.1 84.1 1 10.0-135 0.297 27
Phenanthrene 0.0860 ND 0.0708 0.0707 82.3 80.5 1 10.0-144 0.155 31
Pyrene 0.0860 ND 0.0767 0.0822 89.2 93.6 1 10.0-148 6.91 35
1-Methylnaphthalene 0.0860 ND 0.0767 0.0690 89.2 78.6 1 10.0-142 10.5 28
2-Methylnaphthalene 0.0860 ND 0.0748 0.0698 87.0 79.5 1 10.0-137 6.98 28
2-Chloronaphthalene 0.0860 ND 0.0796 0.0741 92.5 84.4 1 29.0-120 7.14 24
(S) p-Terphenyl-d14 93.9 98.6 23.0-120
(S) Nitrobenzene-d5 77.0 70.5 14.0-149
(S) 2-Fluorobiphenyl 89.6 83.1 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
May 11, 2023
Revised Report
Tetra Tech Inc. - UT
Sample Delivery Group:L1607939
Samples Received:04/21/2023
Project Number:
Description:
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
May 11, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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May 11, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTSTABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 4
Cn: Case Narrative 10
Sr: Sample Results 11
FD-5 L1607939-01 11
FD-4 L1607939-02 15
FD-3 L1607939-03 19
FD-2 L1607939-04 23
FD-1 L1607939-05 27
DUP-1 L1607939-06 31
SS-1 L1607939-07 35
SS-2 L1607939-08 39
SS-3 L1607939-09 43
SS-4 L1607939-10 47
FD-4 L1607939-11 51
FD-3 L1607939-12 56
FD-2 L1607939-13 61
FD-1 L1607939-14 66
FD-4 FILTERED L1607939-15 71
FD-3 FILTERED L1607939-16 72
FD-2 FILTERED L1607939-17 73
FD-1 FILTERED L1607939-18 74
FD-5 L1607939-19 75
DUP-1 L1607939-20 80
FD-5 FILTERED L1607939-21 85
DUP-1 L1607939-22 86
Qc: Quality Control Summary 87
Total Solids by Method 2540 B-2015 87
Total Solids by Method 2540 G-2011 88
Wet Chemistry by Method 1664A 90
Wet Chemistry by Method 3500Cr C-2011 92
Wet Chemistry by Method 7199 94
Mercury by Method 7470A 98
Mercury by Method 7471A 101
Metals (ICP) by Method 6010B 104
Volatile Organic Compounds (GC) by Method 8015D/GRO 115
Volatile Organic Compounds (GC/MS) by Method 8260B 121
Semi-Volatile Organic Compounds (GC) by Method 8015 145
Polychlorinated Biphenyls (GC) by Method 8082 150
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Semi Volatile Organic Compounds (GC/MS) by Method 8270C 155
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 186
Gl: Glossary of Terms 196
Al: Accreditations & Locations 198
Sc: Sample Chain of Custody 199
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FD-5 L1607939-01 Solid Richie T. 04/20/23 11:00 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2053502 1 05/03/23 15:49 05/03/23 15:57 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2052786 1 05/02/23 23:56 05/03/23 11:26 SET Mt. Juliet, TN
Mercury by Method 7471A WG2053230 1 05/03/23 22:23 05/04/23 09:24 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2054328 1 05/04/23 18:18 05/05/23 10:38 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2053393 26 04/20/23 11:00 05/03/23 14:54 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2052852 1.04 04/20/23 11:00 05/02/23 23:02 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2052920 25 05/04/23 07:04 05/04/23 12:11 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2054621 4.69 05/05/23 16:48 05/06/23 00:14 AMM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2052922 5 05/04/23 16:42 05/05/23 05:42 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2051665 1 05/04/23 10:44 05/04/23 22:23 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-4 L1607939-02 Solid Richie T. 04/20/23 13:06 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:26 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048765 1 04/27/23 14:52 04/28/23 16:42 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:13 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:02 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2048964 25 04/20/23 13:06 04/26/23 18:57 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048701 1 04/20/23 13:06 04/26/23 04:02 KSD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048624 2 04/26/23 18:03 04/27/23 09:10 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 22:50 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048869 1 04/26/23 18:31 04/27/23 20:02 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048849 1 04/26/23 08:18 04/26/23 20:50 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-3 L1607939-03 Solid Richie T. 04/20/23 15:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:31 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048765 1 04/27/23 14:52 04/28/23 16:44 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:16 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:05 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2048964 25 04/20/23 15:30 04/26/23 19:17 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048701 1 04/20/23 15:30 04/26/23 04:21 KSD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048624 10 04/26/23 18:03 04/27/23 06:30 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 23:00 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048869 1 04/26/23 18:31 04/27/23 20:22 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/27/23 01:39 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-2 L1607939-04 Solid Richie T. 04/20/23 16:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:36 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048768 1 04/27/23 15:06 04/28/23 12:09 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:24 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:08 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2048964 25 04/20/23 16:30 04/26/23 19:38 NCC Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FD-2 L1607939-04 Solid Richie T. 04/20/23 16:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048701 1 04/20/23 16:30 04/26/23 04:41 KSD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048624 1 04/26/23 18:03 04/27/23 02:19 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 23:10 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048869 1 04/26/23 18:31 04/27/23 01:07 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/26/23 19:46 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-1 L1607939-05 Solid Richie T. 04/20/23 14:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:42 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048768 1 04/27/23 15:06 04/28/23 12:55 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:27 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:17 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049437 25 04/20/23 14:30 04/27/23 14:10 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048701 1 04/20/23 14:30 04/26/23 05:00 KSD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048624 2 04/26/23 18:03 04/27/23 08:56 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 23:20 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048871 1 04/26/23 18:28 04/27/23 07:42 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/27/23 00:40 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
DUP-1 L1607939-06 Solid Richie T. 04/20/23 00:00 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:47 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048768 1 04/27/23 15:06 04/28/23 12:58 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:30 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:20 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049437 25 04/20/23 00:00 04/27/23 14:30 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048704 1 04/20/23 00:00 04/26/23 01:10 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048845 50 04/26/23 10:29 04/26/23 18:22 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 23:31 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048871 5 04/26/23 18:28 04/27/23 08:23 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/27/23 02:38 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-1 L1607939-07 Solid Richie T. 04/20/23 09:42 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:52 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048768 1 04/27/23 15:06 04/28/23 13:05 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:33 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:22 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049437 25 04/20/23 09:42 04/27/23 14:50 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048704 1 04/20/23 09:42 04/26/23 01:30 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048845 1 04/26/23 10:29 04/26/23 17:30 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 23:41 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048871 1 04/26/23 18:28 04/27/23 07:21 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/26/23 20:05 JRM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SS-2 L1607939-08 Solid Richie T. 04/20/23 10:00 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 15:57 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048768 1 04/27/23 15:06 04/28/23 13:07 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:36 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:25 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049437 26 04/20/23 10:00 04/27/23 15:11 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048704 1.04 04/20/23 10:00 04/26/23 01:49 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048845 1 04/26/23 10:29 04/26/23 17:43 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/26/23 23:51 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048871 1 04/26/23 18:28 04/27/23 07:00 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/26/23 20:25 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-3 L1607939-09 Solid Richie T. 04/20/23 09:06 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 16:13 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048768 1 04/27/23 15:06 04/28/23 13:10 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:39 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:28 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049437 25 04/20/23 09:06 04/27/23 15:31 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048704 1 04/20/23 09:06 04/26/23 02:08 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048845 10 04/26/23 10:29 04/27/23 08:42 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2050080 2 04/26/23 10:16 04/27/23 16:53 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048871 10 04/26/23 18:28 04/27/23 08:44 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/27/23 01:19 JRM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 10 04/26/23 08:21 04/28/23 16:46 JCH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-4 L1607939-10 Solid Richie T. 04/20/23 09:20 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2048861 1 04/26/23 10:22 04/26/23 10:37 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2048733 1 04/28/23 08:33 04/28/23 16:18 SET Mt. Juliet, TN
Mercury by Method 7471A WG2048765 1 04/27/23 14:52 04/28/23 16:47 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048870 1 04/26/23 07:52 04/27/23 17:41 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2050507 1 04/28/23 07:46 04/28/23 19:31 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049437 25 04/20/23 09:20 04/27/23 16:42 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048704 1 04/20/23 09:20 04/26/23 02:28 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2048845 5 04/26/23 10:29 04/26/23 18:09 KAP Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2048847 1 04/26/23 10:16 04/27/23 00:12 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048871 1 04/26/23 18:28 04/27/23 08:02 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048850 1 04/26/23 08:21 04/27/23 01:00 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-4 L1607939-11 GW Richie T. 04/20/23 11:00 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2048584 1 04/26/23 00:28 04/26/23 00:59 ARD Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2050781 1 04/28/23 13:31 04/28/23 22:12 ABP Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 12:10 04/28/23 12:10 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:22 NDL Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FD-4 L1607939-11 GW Richie T. 04/20/23 11:00 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/25/23 23:43 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2047755 5 04/26/23 02:17 04/26/23 02:17 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2047326 1 04/24/23 09:27 04/24/23 09:27 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2046978 1 04/22/23 15:26 04/23/23 05:40 ICD Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2047799 1 04/24/23 16:17 04/25/23 05:12 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2047405 1 04/24/23 16:25 04/26/23 04:29 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2047984 1 04/25/23 07:59 04/25/23 21:24 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-3 L1607939-12 GW Richie T. 04/20/23 13:05 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2048584 1 04/26/23 00:28 04/26/23 00:59 ARD Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2050781 1 04/28/23 13:31 04/28/23 22:12 ABP Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 12:43 04/28/23 12:43 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:24 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/25/23 23:46 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2047755 1 04/26/23 02:39 04/26/23 02:39 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2047326 1 04/24/23 09:48 04/24/23 09:48 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2046978 1 04/22/23 15:26 04/23/23 06:03 ICD Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2047799 1 04/24/23 16:17 04/25/23 03:32 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048000 1 04/27/23 11:24 04/27/23 20:05 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2047984 1 04/25/23 07:59 04/25/23 21:41 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-2 L1607939-13 GW Richie T. 04/20/23 15:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2048584 1 04/26/23 00:28 04/26/23 00:59 ARD Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2051086 1 04/30/23 09:35 04/30/23 16:09 RWT Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 12:54 04/28/23 12:54 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:30 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/25/23 23:55 ABL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/26/23 19:14 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2047755 1 04/26/23 06:25 04/26/23 06:25 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2047326 1 04/24/23 10:09 04/24/23 10:09 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2046978 1 04/22/23 15:26 04/23/23 06:26 ICD Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2047799 1 04/24/23 16:17 04/25/23 03:44 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048000 1.05 04/27/23 11:24 04/27/23 22:58 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2047984 1 04/25/23 07:59 04/25/23 21:59 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-1 L1607939-14 GW Richie T. 04/20/23 14:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2048584 1 04/26/23 00:28 04/26/23 00:59 ARD Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2051086 1 04/30/23 09:35 04/30/23 16:09 RWT Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 13:16 04/28/23 13:16 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2051471 1 04/30/23 19:01 04/30/23 22:33 AKB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/25/23 23:58 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2047755 1 04/26/23 06:46 04/26/23 06:46 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2047326 1 04/24/23 10:29 04/24/23 10:29 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2046978 1 04/22/23 15:26 04/23/23 06:49 ICD Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FD-1 L1607939-14 GW Richie T. 04/20/23 14:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Polychlorinated Biphenyls (GC) by Method 8082 WG2047799 1 04/24/23 16:17 04/25/23 03:57 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048000 1.05 04/27/23 11:24 04/27/23 20:26 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2047984 1 04/25/23 07:59 04/25/23 22:16 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-4 FILTERED L1607939-15 GW Richie T. 04/20/23 13:05 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 13:27 04/28/23 13:27 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:32 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/26/23 00:01 ABL Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-3 FILTERED L1607939-16 GW Richie T. 04/20/23 15:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 13:38 04/28/23 13:38 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:34 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048081 1 04/25/23 14:13 04/26/23 00:04 ABL Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-2 FILTERED L1607939-17 GW Richie T. 04/20/23 16:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 14:00 04/28/23 14:00 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:36 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048082 1 04/27/23 10:24 04/27/23 21:21 ABL Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-1 FILTERED L1607939-18 GW Richie T. 04/20/23 14:30 04/21/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 3500Cr C-2011 WG2048027 1 04/28/23 14:54 04/28/23 14:54 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2047887 1 04/27/23 13:40 04/28/23 12:38 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048082 1 04/27/23 10:24 04/27/23 21:24 ABL Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-5 L1607939-19 GW Richie T. 04/20/23 11:00 04/24/23 10:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2048584 1 04/26/23 00:28 04/26/23 00:59 ARD Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2051086 1 04/30/23 09:35 04/30/23 16:09 RWT Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2048715 1 04/27/23 01:43 04/27/23 01:43 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2048783 1 05/01/23 10:54 05/01/23 15:34 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048547 1 04/28/23 09:39 04/28/23 22:40 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049501 1 04/27/23 06:59 04/27/23 06:59 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048606 1 04/25/23 22:05 04/25/23 22:05 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2049589 1 04/27/23 13:40 04/28/23 18:04 MWS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2047970 1 04/25/23 16:31 04/26/23 01:25 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048428 1 04/25/23 15:47 04/26/23 10:58 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048874 1 04/26/23 19:57 04/27/23 00:58 DSH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
DUP-1 L1607939-20 GW Richie T. 04/20/23 00:00 04/24/23 10:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2048584 1 04/26/23 00:28 04/26/23 00:59 ARD Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2051086 1 04/30/23 09:35 04/30/23 16:09 RWT Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2048715 1 04/27/23 02:06 04/27/23 02:06 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2048783 1 05/01/23 10:54 05/01/23 16:19 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048547 1 04/28/23 09:39 04/28/23 22:50 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2049550 1 04/27/23 14:24 04/27/23 14:24 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2048606 1 04/25/23 22:26 04/25/23 22:26 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2049589 1 04/27/23 13:40 04/27/23 22:58 MWS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2047970 1 04/25/23 16:31 04/26/23 01:56 RDH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2048428 1 04/25/23 15:47 04/26/23 02:41 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2048874 1 04/26/23 19:57 04/27/23 01:50 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD-5 FILTERED L1607939-21 GW Richie T. 04/20/23 11:00 04/24/23 10:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 3500Cr C-2011 WG2048715 1 04/27/23 02:22 04/27/23 02:22 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2048783 1 05/01/23 10:54 05/01/23 16:26 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048547 1 04/28/23 09:39 04/28/23 22:53 SPL Mt. Juliet, TN
Collected by Collected date/time Received date/time
DUP-1 L1607939-22 GW Richie T. 04/20/23 00:00 04/24/23 10:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 3500Cr C-2011 WG2048715 1 04/27/23 02:29 04/27/23 02:29 VSS Mt. Juliet, TN
Mercury by Method 7470A WG2048783 1 05/01/23 10:54 05/01/23 16:28 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2048547 1 04/28/23 09:39 04/28/23 22:56 SPL Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 05/02/23 11:11
Project Narrative
Report reissued 5/11 for updated -01 with MS/MSD
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1607939-14 FD-1 1664A, 3500Cr C-2011
L1607939-21 FD-5 FILTERED 3500Cr C-2011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.5 1 05/03/2023 15:57 WG2053502
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium 2.04 1.21 1 05/03/2023 11:26 WG2052786
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0485 1 05/04/2023 09:24 WG2053230
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.42 1 05/05/2023 10:38 WG2054328
Arsenic 4.01 2.42 1 05/05/2023 10:38 WG2054328
Beryllium 0.265 0.242 1 05/05/2023 10:38 WG2054328
Cadmium ND 0.606 1 05/05/2023 10:38 WG2054328
Chromium 71.8 J6 O1 1.21 1 05/05/2023 10:38 WG2054328
Copper 86.4 J3 J6 2.42 1 05/05/2023 10:38 WG2054328
Lead 10.8 J3 J5 0.606 1 05/05/2023 10:38 WG2054328
Nickel 33.3 2.42 1 05/05/2023 10:38 WG2054328
Selenium ND 2.42 1 05/05/2023 10:38 WG2054328
Silver ND 1.21 1 05/05/2023 10:38 WG2054328
Thallium ND 2.42 1 05/05/2023 10:38 WG2054328
Zinc 35.6 J3 J5 6.06 1 05/05/2023 10:38 WG2054328
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.68 26 05/03/2023 14:54 WG2053393
(S) a,a,a-Trifluorotoluene(FID) 99.3 77.0-120 05/03/2023 14:54 WG2053393
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND J3 J5 0.0801 1.04 05/02/2023 23:02 WG2052852
Acrylonitrile ND 0.0200 1.04 05/02/2023 23:02 WG2052852
Benzene ND 0.00160 1.04 05/02/2023 23:02 WG2052852
Bromobenzene ND 0.0200 1.04 05/02/2023 23:02 WG2052852
Bromodichloromethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Bromoform ND 0.0401 1.04 05/02/2023 23:02 WG2052852
Bromomethane ND 0.0200 1.04 05/02/2023 23:02 WG2052852
n-Butylbenzene ND 0.0200 1.04 05/02/2023 23:02 WG2052852
sec-Butylbenzene ND 0.0200 1.04 05/02/2023 23:02 WG2052852
tert-Butylbenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
Carbon tetrachloride ND 0.00801 1.04 05/02/2023 23:02 WG2052852
Chlorobenzene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Chlorodibromomethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Chloroethane ND 0.00801 1.04 05/02/2023 23:02 WG2052852
Chloroform ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Chloromethane ND 0.0200 1.04 05/02/2023 23:02 WG2052852
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
4-Chlorotoluene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,2-Dibromo-3-Chloropropane ND 0.0401 1.04 05/02/2023 23:02 WG2052852
1,2-Dibromoethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Dibromomethane ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,2-Dichlorobenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,3-Dichlorobenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,4-Dichlorobenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
Dichlorodifluoromethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,1-Dichloroethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,2-Dichloroethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,1-Dichloroethene ND J3 0.00401 1.04 05/02/2023 23:02 WG2052852
cis-1,2-Dichloroethene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
trans-1,2-Dichloroethene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,2-Dichloropropane ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,1-Dichloropropene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,3-Dichloropropane ND 0.00801 1.04 05/02/2023 23:02 WG2052852
cis-1,3-Dichloropropene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
trans-1,3-Dichloropropene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
2,2-Dichloropropane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Di-isopropyl ether ND 0.00160 1.04 05/02/2023 23:02 WG2052852
Ethylbenzene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Hexachloro-1,3-butadiene ND J3 0.0401 1.04 05/02/2023 23:02 WG2052852
Isopropylbenzene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
p-Isopropyltoluene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
2-Butanone (MEK)ND 0.160 1.04 05/02/2023 23:02 WG2052852
Methylene Chloride ND 0.0401 1.04 05/02/2023 23:02 WG2052852
4-Methyl-2-pentanone (MIBK) ND 0.0401 1.04 05/02/2023 23:02 WG2052852
Methyl tert-butyl ether ND 0.00160 1.04 05/02/2023 23:02 WG2052852
Naphthalene ND J3 0.0200 1.04 05/02/2023 23:02 WG2052852
n-Propylbenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
Styrene ND 0.0200 1.04 05/02/2023 23:02 WG2052852
1,1,1,2-Tetrachloroethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,1,2,2-Tetrachloroethane ND J3 0.00401 1.04 05/02/2023 23:02 WG2052852
1,1,2-Trichlorotrifluoroethane ND J3 J4 0.00401 1.04 05/02/2023 23:02 WG2052852
Tetrachloroethene ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Toluene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,2,3-Trichlorobenzene ND J3 0.0200 1.04 05/02/2023 23:02 WG2052852
1,2,4-Trichlorobenzene ND 0.0200 1.04 05/02/2023 23:02 WG2052852
1,1,1-Trichloroethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,1,2-Trichloroethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
Trichloroethene ND 0.00160 1.04 05/02/2023 23:02 WG2052852
Trichlorofluoromethane ND 0.00401 1.04 05/02/2023 23:02 WG2052852
1,2,3-Trichloropropane ND 0.0200 1.04 05/02/2023 23:02 WG2052852
1,2,4-Trimethylbenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,2,3-Trimethylbenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
1,3,5-Trimethylbenzene ND 0.00801 1.04 05/02/2023 23:02 WG2052852
Vinyl chloride ND J5 0.00401 1.04 05/02/2023 23:02 WG2052852
Xylenes, Total ND 0.0104 1.04 05/02/2023 23:02 WG2052852
(S) Toluene-d8 107 75.0-131 05/02/2023 23:02 WG2052852
(S) 4-Bromofluorobenzene 91.2 67.0-138 05/02/2023 23:02 WG2052852
(S) 1,2-Dichloroethane-d4 114 70.0-130 05/02/2023 23:02 WG2052852
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND J3 J5 121 25 05/04/2023 12:11 WG2052920
C28-C40 Oil Range 245 121 25 05/04/2023 12:11 WG2052920
(S) o-Terphenyl 46.4 J7 18.0-148 05/04/2023 12:11 WG2052920
Sample Narrative:
L1607939-01 WG2052920: Cannot run at lower dilution due to viscosity of extract
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.203 4.69 05/06/2023 00:14 WG2054621
PCB 1221 ND 0.203 4.69 05/06/2023 00:14 WG2054621
PCB 1232 ND 0.203 4.69 05/06/2023 00:14 WG2054621
PCB 1242 ND 0.203 4.69 05/06/2023 00:14 WG2054621
PCB 1248 ND 0.102 4.69 05/06/2023 00:14 WG2054621
PCB 1254 ND 0.102 4.69 05/06/2023 00:14 WG2054621
PCB 1260 ND 0.102 4.69 05/06/2023 00:14 WG2054621
(S) Decachlorobiphenyl 93.6 10.0-135 05/06/2023 00:14 WG2054621
(S) Tetrachloro-m-xylene 76.6 10.0-139 05/06/2023 00:14 WG2054621
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.202 5 05/05/2023 05:42 WG2052922
Acenaphthylene ND 0.202 5 05/05/2023 05:42 WG2052922
Anthracene ND 0.202 5 05/05/2023 05:42 WG2052922
Benzidine ND 10.1 5 05/05/2023 05:42 WG2052922
Benzo(a)anthracene ND 0.202 5 05/05/2023 05:42 WG2052922
Benzo(b)fluoranthene ND 0.202 5 05/05/2023 05:42 WG2052922
Benzo(k)fluoranthene ND 0.202 5 05/05/2023 05:42 WG2052922
Benzo(g,h,i)perylene ND 0.202 5 05/05/2023 05:42 WG2052922
Benzo(a)pyrene ND 0.202 5 05/05/2023 05:42 WG2052922
Bis(2-chlorethoxy)methane ND 2.02 5 05/05/2023 05:42 WG2052922
Bis(2-chloroethyl)ether ND 2.02 5 05/05/2023 05:42 WG2052922
2,2-Oxybis(1-Chloropropane) ND 2.02 5 05/05/2023 05:42 WG2052922
4-Bromophenyl-phenylether ND 2.02 5 05/05/2023 05:42 WG2052922
2-Chloronaphthalene ND 0.202 5 05/05/2023 05:42 WG2052922
4-Chlorophenyl-phenylether ND 2.02 5 05/05/2023 05:42 WG2052922
Chrysene ND 0.202 5 05/05/2023 05:42 WG2052922
Dibenz(a,h)anthracene ND 0.202 5 05/05/2023 05:42 WG2052922
3,3-Dichlorobenzidine ND 2.02 5 05/05/2023 05:42 WG2052922
2,4-Dinitrotoluene ND 2.02 5 05/05/2023 05:42 WG2052922
2,6-Dinitrotoluene ND 2.02 5 05/05/2023 05:42 WG2052922
Fluoranthene ND 0.202 5 05/05/2023 05:42 WG2052922
Fluorene ND 0.202 5 05/05/2023 05:42 WG2052922
Hexachlorobenzene ND 2.02 5 05/05/2023 05:42 WG2052922
Hexachloro-1,3-butadiene ND 2.02 5 05/05/2023 05:42 WG2052922
Hexachlorocyclopentadiene ND J6 2.02 5 05/05/2023 05:42 WG2052922
Hexachloroethane ND 2.02 5 05/05/2023 05:42 WG2052922
Indeno(1,2,3-cd)pyrene ND 0.202 5 05/05/2023 05:42 WG2052922
Isophorone ND 2.02 5 05/05/2023 05:42 WG2052922
Naphthalene ND 0.202 5 05/05/2023 05:42 WG2052922
Nitrobenzene ND 2.02 5 05/05/2023 05:42 WG2052922
n-Nitrosodimethylamine ND 2.02 5 05/05/2023 05:42 WG2052922
n-Nitrosodiphenylamine ND 2.02 5 05/05/2023 05:42 WG2052922
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
n-Nitrosodi-n-propylamine ND 2.02 5 05/05/2023 05:42 WG2052922
Phenanthrene ND 0.202 5 05/05/2023 05:42 WG2052922
Benzylbutyl phthalate ND 2.02 5 05/05/2023 05:42 WG2052922
Bis(2-ethylhexyl)phthalate ND 2.02 5 05/05/2023 05:42 WG2052922
Di-n-butyl phthalate ND 2.02 5 05/05/2023 05:42 WG2052922
Diethyl phthalate ND 2.02 5 05/05/2023 05:42 WG2052922
Dimethyl phthalate ND J6 2.02 5 05/05/2023 05:42 WG2052922
Di-n-octyl phthalate ND 2.02 5 05/05/2023 05:42 WG2052922
Pyrene ND 0.202 5 05/05/2023 05:42 WG2052922
1,2,4-Trichlorobenzene ND 2.02 5 05/05/2023 05:42 WG2052922
4-Chloro-3-methylphenol ND 2.02 5 05/05/2023 05:42 WG2052922
2-Chlorophenol ND 2.02 5 05/05/2023 05:42 WG2052922
2,4-Dichlorophenol ND 2.02 5 05/05/2023 05:42 WG2052922
2,4-Dimethylphenol ND 2.02 5 05/05/2023 05:42 WG2052922
4,6-Dinitro-2-methylphenol ND J6 2.02 5 05/05/2023 05:42 WG2052922
2,4-Dinitrophenol ND J6 2.02 5 05/05/2023 05:42 WG2052922
2-Nitrophenol ND 2.02 5 05/05/2023 05:42 WG2052922
4-Nitrophenol ND J3 2.02 5 05/05/2023 05:42 WG2052922
Pentachlorophenol ND J3 2.02 5 05/05/2023 05:42 WG2052922
Phenol ND 2.02 5 05/05/2023 05:42 WG2052922
2,4,6-Trichlorophenol ND J3 2.02 5 05/05/2023 05:42 WG2052922
(S) Nitrobenzene-d5 54.4 10.0-122 05/05/2023 05:42 WG2052922
(S) 2-Fluorobiphenyl 49.2 15.0-120 05/05/2023 05:42 WG2052922
(S) p-Terphenyl-d14 53.8 10.0-120 05/05/2023 05:42 WG2052922
(S) Phenol-d5 44.6 10.0-120 05/05/2023 05:42 WG2052922
(S) 2-Fluorophenol 38.4 12.0-120 05/05/2023 05:42 WG2052922
(S) 2,4,6-Tribromophenol 47.1 10.0-127 05/05/2023 05:42 WG2052922
Sample Narrative:
L1607939-01 WG2052922: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND J3 0.00765 1 05/04/2023 22:23 WG2051665
Acenaphthene 0.00927 J3 0.00765 1 05/04/2023 22:23 WG2051665
Acenaphthylene ND J3 0.00765 1 05/04/2023 22:23 WG2051665
Benzo(a)anthracene 0.0236 J3 0.00765 1 05/04/2023 22:23 WG2051665
Benzo(a)pyrene 0.0249 J3 0.00765 1 05/04/2023 22:23 WG2051665
Benzo(b)fluoranthene 0.0191 J3 0.00765 1 05/04/2023 22:23 WG2051665
Benzo(g,h,i)perylene 0.0306 J3 J6 0.00765 1 05/04/2023 22:23 WG2051665
Benzo(k)fluoranthene ND J3 0.00765 1 05/04/2023 22:23 WG2051665
Chrysene 0.0219 0.00765 1 05/04/2023 22:23 WG2051665
Dibenz(a,h)anthracene ND 0.00765 1 05/04/2023 22:23 WG2051665
Fluoranthene 0.0235 J3 0.00765 1 05/04/2023 22:23 WG2051665
Fluorene ND J3 0.00765 1 05/04/2023 22:23 WG2051665
Indeno(1,2,3-cd)pyrene 0.0123 J3 0.00765 1 05/04/2023 22:23 WG2051665
Naphthalene ND J3 0.0255 1 05/04/2023 22:23 WG2051665
Phenanthrene 0.0368 J3 0.00765 1 05/04/2023 22:23 WG2051665
Pyrene 0.0509 J3 0.00765 1 05/04/2023 22:23 WG2051665
1-Methylnaphthalene ND J3 0.0255 1 05/04/2023 22:23 WG2051665
2-Methylnaphthalene ND J3 0.0255 1 05/04/2023 22:23 WG2051665
2-Chloronaphthalene ND J3 0.0255 1 05/04/2023 22:23 WG2051665
(S) p-Terphenyl-d14 60.3 23.0-120 05/04/2023 22:23 WG2051665
(S) Nitrobenzene-d5 82.2 14.0-149 05/04/2023 22:23 WG2051665
(S) 2-Fluorobiphenyl 53.5 34.0-125 05/04/2023 22:23 WG2051665
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1607939
FD-4
Collected date/time: 04/20/23 13:06
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.1 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.22 1 04/28/2023 15:26 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0487 1 04/28/2023 16:42 WG2048765
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.44 1 04/28/2023 19:02 WG2050507
Arsenic 6.45 2.44 1 04/27/2023 17:13 WG2048870
Beryllium 0.284 0.244 1 04/27/2023 17:13 WG2048870
Cadmium ND 0.609 1 04/27/2023 17:13 WG2048870
Chromium 27.6 1.22 1 04/27/2023 17:13 WG2048870
Copper 35.2 2.44 1 04/27/2023 17:13 WG2048870
Lead 7.60 0.609 1 04/27/2023 17:13 WG2048870
Nickel 14.0 2.44 1 04/27/2023 17:13 WG2048870
Selenium ND 2.44 1 04/27/2023 17:13 WG2048870
Silver ND 1.22 1 04/27/2023 17:13 WG2048870
Thallium ND 2.44 1 04/27/2023 17:13 WG2048870
Zinc 41.5 6.09 1 04/27/2023 17:13 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.73 25 04/26/2023 18:57 WG2048964
(S) a,a,a-Trifluorotoluene(FID) 97.2 77.0-120 04/26/2023 18:57 WG2048964
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0747 1 04/26/2023 04:02 WG2048701
Acrylonitrile ND 0.0187 1 04/26/2023 04:02 WG2048701
Benzene ND 0.00149 1 04/26/2023 04:02 WG2048701
Bromobenzene ND 0.0187 1 04/26/2023 04:02 WG2048701
Bromodichloromethane ND 0.00373 1 04/26/2023 04:02 WG2048701
Bromoform ND 0.0373 1 04/26/2023 04:02 WG2048701
Bromomethane ND 0.0187 1 04/26/2023 04:02 WG2048701
n-Butylbenzene ND 0.0187 1 04/26/2023 04:02 WG2048701
sec-Butylbenzene ND J3 0.0187 1 04/26/2023 04:02 WG2048701
tert-Butylbenzene ND J3 0.00747 1 04/26/2023 04:02 WG2048701
Carbon tetrachloride ND 0.00747 1 04/26/2023 04:02 WG2048701
Chlorobenzene ND 0.00373 1 04/26/2023 04:02 WG2048701
Chlorodibromomethane ND 0.00373 1 04/26/2023 04:02 WG2048701
Chloroethane ND 0.00747 1 04/26/2023 04:02 WG2048701
Chloroform ND 0.00373 1 04/26/2023 04:02 WG2048701
Chloromethane ND 0.0187 1 04/26/2023 04:02 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1607939
FD-4
Collected date/time: 04/20/23 13:06
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00373 1 04/26/2023 04:02 WG2048701
4-Chlorotoluene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,2-Dibromo-3-Chloropropane ND 0.0373 1 04/26/2023 04:02 WG2048701
1,2-Dibromoethane ND 0.00373 1 04/26/2023 04:02 WG2048701
Dibromomethane ND 0.00747 1 04/26/2023 04:02 WG2048701
1,2-Dichlorobenzene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,3-Dichlorobenzene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,4-Dichlorobenzene ND 0.00747 1 04/26/2023 04:02 WG2048701
Dichlorodifluoromethane ND 0.00373 1 04/26/2023 04:02 WG2048701
1,1-Dichloroethane ND J4 0.00373 1 04/26/2023 04:02 WG2048701
1,2-Dichloroethane ND 0.00373 1 04/26/2023 04:02 WG2048701
1,1-Dichloroethene ND 0.00373 1 04/26/2023 04:02 WG2048701
cis-1,2-Dichloroethene ND 0.00373 1 04/26/2023 04:02 WG2048701
trans-1,2-Dichloroethene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,2-Dichloropropane ND J4 0.00747 1 04/26/2023 04:02 WG2048701
1,1-Dichloropropene ND J4 0.00373 1 04/26/2023 04:02 WG2048701
1,3-Dichloropropane ND 0.00747 1 04/26/2023 04:02 WG2048701
cis-1,3-Dichloropropene ND 0.00373 1 04/26/2023 04:02 WG2048701
trans-1,3-Dichloropropene ND 0.00747 1 04/26/2023 04:02 WG2048701
2,2-Dichloropropane ND J3 0.00373 1 04/26/2023 04:02 WG2048701
Di-isopropyl ether ND J4 0.00149 1 04/26/2023 04:02 WG2048701
Ethylbenzene ND J3 0.00373 1 04/26/2023 04:02 WG2048701
Hexachloro-1,3-butadiene ND 0.0373 1 04/26/2023 04:02 WG2048701
Isopropylbenzene ND J3 0.00373 1 04/26/2023 04:02 WG2048701
p-Isopropyltoluene ND J3 0.00747 1 04/26/2023 04:02 WG2048701
2-Butanone (MEK)ND 0.149 1 04/26/2023 04:02 WG2048701
Methylene Chloride ND 0.0373 1 04/26/2023 04:02 WG2048701
4-Methyl-2-pentanone (MIBK) ND 0.0373 1 04/26/2023 04:02 WG2048701
Methyl tert-butyl ether ND 0.00149 1 04/26/2023 04:02 WG2048701
Naphthalene ND 0.0187 1 04/26/2023 04:02 WG2048701
n-Propylbenzene ND 0.00747 1 04/26/2023 04:02 WG2048701
Styrene ND 0.0187 1 04/26/2023 04:02 WG2048701
1,1,1,2-Tetrachloroethane ND 0.00373 1 04/26/2023 04:02 WG2048701
1,1,2,2-Tetrachloroethane ND 0.00373 1 04/26/2023 04:02 WG2048701
1,1,2-Trichlorotrifluoroethane ND 0.00373 1 04/26/2023 04:02 WG2048701
Tetrachloroethene ND 0.00373 1 04/26/2023 04:02 WG2048701
Toluene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,2,3-Trichlorobenzene ND J3 0.0187 1 04/26/2023 04:02 WG2048701
1,2,4-Trichlorobenzene ND J3 0.0187 1 04/26/2023 04:02 WG2048701
1,1,1-Trichloroethane ND 0.00373 1 04/26/2023 04:02 WG2048701
1,1,2-Trichloroethane ND 0.00373 1 04/26/2023 04:02 WG2048701
Trichloroethene ND 0.00149 1 04/26/2023 04:02 WG2048701
Trichlorofluoromethane ND 0.00373 1 04/26/2023 04:02 WG2048701
1,2,3-Trichloropropane ND 0.0187 1 04/26/2023 04:02 WG2048701
1,2,4-Trimethylbenzene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,2,3-Trimethylbenzene ND 0.00747 1 04/26/2023 04:02 WG2048701
1,3,5-Trimethylbenzene ND J3 0.00747 1 04/26/2023 04:02 WG2048701
Vinyl chloride ND 0.00373 1 04/26/2023 04:02 WG2048701
Xylenes, Total ND 0.00971 1 04/26/2023 04:02 WG2048701
(S) Toluene-d8 102 75.0-131 04/26/2023 04:02 WG2048701
(S) 4-Bromofluorobenzene 114 67.0-138 04/26/2023 04:02 WG2048701
(S) 1,2-Dichloroethane-d4 90.6 70.0-130 04/26/2023 04:02 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1607939
FD-4
Collected date/time: 04/20/23 13:06
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 38.9 9.75 2 04/27/2023 09:10 WG2048624
C28-C40 Oil Range 117 9.75 2 04/27/2023 09:10 WG2048624
(S) o-Terphenyl 92.6 18.0-148 04/27/2023 09:10 WG2048624
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0414 1 04/26/2023 22:50 WG2048847
PCB 1221 ND 0.0414 1 04/26/2023 22:50 WG2048847
PCB 1232 ND 0.0414 1 04/26/2023 22:50 WG2048847
PCB 1242 ND 0.0414 1 04/26/2023 22:50 WG2048847
PCB 1248 ND 0.0207 1 04/26/2023 22:50 WG2048847
PCB 1254 ND 0.0207 1 04/26/2023 22:50 WG2048847
PCB 1260 ND 0.0207 1 04/26/2023 22:50 WG2048847
(S) Decachlorobiphenyl 105 10.0-135 04/26/2023 22:50 WG2048847
(S) Tetrachloro-m-xylene 66.5 10.0-139 04/26/2023 22:50 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0406 1 04/27/2023 20:02 WG2048869
Acenaphthylene ND 0.0406 1 04/27/2023 20:02 WG2048869
Anthracene ND 0.0406 1 04/27/2023 20:02 WG2048869
Benzidine ND 2.03 1 04/27/2023 20:02 WG2048869
Benzo(a)anthracene ND 0.0406 1 04/27/2023 20:02 WG2048869
Benzo(b)fluoranthene ND 0.0406 1 04/27/2023 20:02 WG2048869
Benzo(k)fluoranthene ND 0.0406 1 04/27/2023 20:02 WG2048869
Benzo(g,h,i)perylene ND 0.0406 1 04/27/2023 20:02 WG2048869
Benzo(a)pyrene ND 0.0406 1 04/27/2023 20:02 WG2048869
Bis(2-chlorethoxy)methane ND 0.406 1 04/27/2023 20:02 WG2048869
Bis(2-chloroethyl)ether ND 0.406 1 04/27/2023 20:02 WG2048869
2,2-Oxybis(1-Chloropropane) ND 0.406 1 04/27/2023 20:02 WG2048869
4-Bromophenyl-phenylether ND 0.406 1 04/27/2023 20:02 WG2048869
2-Chloronaphthalene ND 0.0406 1 04/27/2023 20:02 WG2048869
4-Chlorophenyl-phenylether ND 0.406 1 04/27/2023 20:02 WG2048869
Chrysene ND 0.0406 1 04/27/2023 20:02 WG2048869
Dibenz(a,h)anthracene ND 0.0406 1 04/27/2023 20:02 WG2048869
3,3-Dichlorobenzidine ND 0.406 1 04/27/2023 20:02 WG2048869
2,4-Dinitrotoluene ND 0.406 1 04/27/2023 20:02 WG2048869
2,6-Dinitrotoluene ND 0.406 1 04/27/2023 20:02 WG2048869
Fluoranthene ND 0.0406 1 04/27/2023 20:02 WG2048869
Fluorene ND 0.0406 1 04/27/2023 20:02 WG2048869
Hexachlorobenzene ND 0.406 1 04/27/2023 20:02 WG2048869
Hexachloro-1,3-butadiene ND 0.406 1 04/27/2023 20:02 WG2048869
Hexachlorocyclopentadiene ND 0.406 1 04/27/2023 20:02 WG2048869
Hexachloroethane ND 0.406 1 04/27/2023 20:02 WG2048869
Indeno(1,2,3-cd)pyrene ND 0.0406 1 04/27/2023 20:02 WG2048869
Isophorone ND 0.406 1 04/27/2023 20:02 WG2048869
Naphthalene ND 0.0406 1 04/27/2023 20:02 WG2048869
Nitrobenzene ND 0.406 1 04/27/2023 20:02 WG2048869
n-Nitrosodimethylamine ND 0.406 1 04/27/2023 20:02 WG2048869
n-Nitrosodiphenylamine ND 0.406 1 04/27/2023 20:02 WG2048869
n-Nitrosodi-n-propylamine ND 0.406 1 04/27/2023 20:02 WG2048869
Phenanthrene ND 0.0406 1 04/27/2023 20:02 WG2048869
Benzylbutyl phthalate ND 0.406 1 04/27/2023 20:02 WG2048869
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1607939
FD-4
Collected date/time: 04/20/23 13:06
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.406 1 04/27/2023 20:02 WG2048869
Di-n-butyl phthalate ND 0.406 1 04/27/2023 20:02 WG2048869
Diethyl phthalate ND 0.406 1 04/27/2023 20:02 WG2048869
Dimethyl phthalate ND 0.406 1 04/27/2023 20:02 WG2048869
Di-n-octyl phthalate ND 0.406 1 04/27/2023 20:02 WG2048869
Pyrene ND 0.0406 1 04/27/2023 20:02 WG2048869
1,2,4-Trichlorobenzene ND 0.406 1 04/27/2023 20:02 WG2048869
4-Chloro-3-methylphenol ND 0.406 1 04/27/2023 20:02 WG2048869
2-Chlorophenol ND 0.406 1 04/27/2023 20:02 WG2048869
2,4-Dichlorophenol ND 0.406 1 04/27/2023 20:02 WG2048869
2,4-Dimethylphenol ND 0.406 1 04/27/2023 20:02 WG2048869
4,6-Dinitro-2-methylphenol ND 0.406 1 04/27/2023 20:02 WG2048869
2,4-Dinitrophenol ND 0.406 1 04/27/2023 20:02 WG2048869
2-Nitrophenol ND 0.406 1 04/27/2023 20:02 WG2048869
4-Nitrophenol ND 0.406 1 04/27/2023 20:02 WG2048869
Pentachlorophenol ND 0.406 1 04/27/2023 20:02 WG2048869
Phenol ND 0.406 1 04/27/2023 20:02 WG2048869
2,4,6-Trichlorophenol ND 0.406 1 04/27/2023 20:02 WG2048869
(S) Nitrobenzene-d5 40.2 10.0-122 04/27/2023 20:02 WG2048869
(S) 2-Fluorobiphenyl 36.6 15.0-120 04/27/2023 20:02 WG2048869
(S) p-Terphenyl-d14 39.0 10.0-120 04/27/2023 20:02 WG2048869
(S) Phenol-d5 36.2 10.0-120 04/27/2023 20:02 WG2048869
(S) 2-Fluorophenol 34.4 12.0-120 04/27/2023 20:02 WG2048869
(S) 2,4,6-Tribromophenol 39.8 10.0-127 04/27/2023 20:02 WG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00731 1 04/26/2023 20:50 WG2048849
Acenaphthene ND 0.00731 1 04/26/2023 20:50 WG2048849
Acenaphthylene ND 0.00731 1 04/26/2023 20:50 WG2048849
Benzo(a)anthracene 0.0441 0.00731 1 04/26/2023 20:50 WG2048849
Benzo(a)pyrene 0.0331 0.00731 1 04/26/2023 20:50 WG2048849
Benzo(b)fluoranthene 0.0509 0.00731 1 04/26/2023 20:50 WG2048849
Benzo(g,h,i)perylene 0.0323 0.00731 1 04/26/2023 20:50 WG2048849
Benzo(k)fluoranthene 0.0166 0.00731 1 04/26/2023 20:50 WG2048849
Chrysene 0.0453 0.00731 1 04/26/2023 20:50 WG2048849
Dibenz(a,h)anthracene ND 0.00731 1 04/26/2023 20:50 WG2048849
Fluoranthene 0.0897 0.00731 1 04/26/2023 20:50 WG2048849
Fluorene ND 0.00731 1 04/26/2023 20:50 WG2048849
Indeno(1,2,3-cd)pyrene 0.0274 0.00731 1 04/26/2023 20:50 WG2048849
Naphthalene ND 0.0244 1 04/26/2023 20:50 WG2048849
Phenanthrene 0.0274 0.00731 1 04/26/2023 20:50 WG2048849
Pyrene 0.140 0.00731 1 04/26/2023 20:50 WG2048849
1-Methylnaphthalene ND 0.0244 1 04/26/2023 20:50 WG2048849
2-Methylnaphthalene ND 0.0244 1 04/26/2023 20:50 WG2048849
2-Chloronaphthalene ND 0.0244 1 04/26/2023 20:50 WG2048849
(S) p-Terphenyl-d14 71.3 23.0-120 04/26/2023 20:50 WG2048849
(S) Nitrobenzene-d5 65.1 14.0-149 04/26/2023 20:50 WG2048849
(S) 2-Fluorobiphenyl 55.8 34.0-125 04/26/2023 20:50 WG2048849
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1607939
FD-3
Collected date/time: 04/20/23 15:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.4 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.18 1 04/28/2023 15:31 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0474 1 04/28/2023 16:44 WG2048765
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.37 1 04/28/2023 19:05 WG2050507
Arsenic 8.07 2.37 1 04/27/2023 17:16 WG2048870
Beryllium 0.323 0.237 1 04/27/2023 17:16 WG2048870
Cadmium ND 0.592 1 04/27/2023 17:16 WG2048870
Chromium 16.3 1.18 1 04/27/2023 17:16 WG2048870
Copper 26.1 2.37 1 04/27/2023 17:16 WG2048870
Lead 12.5 0.592 1 04/27/2023 17:16 WG2048870
Nickel 12.0 2.37 1 04/27/2023 17:16 WG2048870
Selenium ND 2.37 1 04/27/2023 17:16 WG2048870
Silver ND 1.18 1 04/27/2023 17:16 WG2048870
Thallium ND 2.37 1 04/27/2023 17:16 WG2048870
Zinc 46.4 5.92 1 04/27/2023 17:16 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 8.03 B 3.46 25 04/26/2023 19:17 WG2048964
(S) a,a,a-Trifluorotoluene(FID) 97.9 77.0-120 04/26/2023 19:17 WG2048964
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0692 1 04/26/2023 04:21 WG2048701
Acrylonitrile ND 0.0173 1 04/26/2023 04:21 WG2048701
Benzene ND 0.00138 1 04/26/2023 04:21 WG2048701
Bromobenzene ND 0.0173 1 04/26/2023 04:21 WG2048701
Bromodichloromethane ND 0.00346 1 04/26/2023 04:21 WG2048701
Bromoform ND 0.0346 1 04/26/2023 04:21 WG2048701
Bromomethane ND 0.0173 1 04/26/2023 04:21 WG2048701
n-Butylbenzene 0.0399 0.0173 1 04/26/2023 04:21 WG2048701
sec-Butylbenzene 0.0240 J3 0.0173 1 04/26/2023 04:21 WG2048701
tert-Butylbenzene ND J3 0.00692 1 04/26/2023 04:21 WG2048701
Carbon tetrachloride ND 0.00692 1 04/26/2023 04:21 WG2048701
Chlorobenzene ND 0.00346 1 04/26/2023 04:21 WG2048701
Chlorodibromomethane ND 0.00346 1 04/26/2023 04:21 WG2048701
Chloroethane ND 0.00692 1 04/26/2023 04:21 WG2048701
Chloroform ND 0.00346 1 04/26/2023 04:21 WG2048701
Chloromethane ND 0.0173 1 04/26/2023 04:21 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1607939
FD-3
Collected date/time: 04/20/23 15:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00346 1 04/26/2023 04:21 WG2048701
4-Chlorotoluene ND 0.00692 1 04/26/2023 04:21 WG2048701
1,2-Dibromo-3-Chloropropane ND 0.0346 1 04/26/2023 04:21 WG2048701
1,2-Dibromoethane ND 0.00346 1 04/26/2023 04:21 WG2048701
Dibromomethane ND 0.00692 1 04/26/2023 04:21 WG2048701
1,2-Dichlorobenzene ND 0.00692 1 04/26/2023 04:21 WG2048701
1,3-Dichlorobenzene ND 0.00692 1 04/26/2023 04:21 WG2048701
1,4-Dichlorobenzene ND 0.00692 1 04/26/2023 04:21 WG2048701
Dichlorodifluoromethane ND 0.00346 1 04/26/2023 04:21 WG2048701
1,1-Dichloroethane ND J4 0.00346 1 04/26/2023 04:21 WG2048701
1,2-Dichloroethane ND 0.00346 1 04/26/2023 04:21 WG2048701
1,1-Dichloroethene ND 0.00346 1 04/26/2023 04:21 WG2048701
cis-1,2-Dichloroethene ND 0.00346 1 04/26/2023 04:21 WG2048701
trans-1,2-Dichloroethene ND 0.00692 1 04/26/2023 04:21 WG2048701
1,2-Dichloropropane ND J4 0.00692 1 04/26/2023 04:21 WG2048701
1,1-Dichloropropene ND J4 0.00346 1 04/26/2023 04:21 WG2048701
1,3-Dichloropropane ND 0.00692 1 04/26/2023 04:21 WG2048701
cis-1,3-Dichloropropene ND 0.00346 1 04/26/2023 04:21 WG2048701
trans-1,3-Dichloropropene ND 0.00692 1 04/26/2023 04:21 WG2048701
2,2-Dichloropropane ND J3 0.00346 1 04/26/2023 04:21 WG2048701
Di-isopropyl ether ND J4 0.00138 1 04/26/2023 04:21 WG2048701
Ethylbenzene 0.0159 J3 0.00346 1 04/26/2023 04:21 WG2048701
Hexachloro-1,3-butadiene ND 0.0346 1 04/26/2023 04:21 WG2048701
Isopropylbenzene 0.00968 J3 0.00346 1 04/26/2023 04:21 WG2048701
p-Isopropyltoluene 0.0876 J3 0.00692 1 04/26/2023 04:21 WG2048701
2-Butanone (MEK)ND 0.138 1 04/26/2023 04:21 WG2048701
Methylene Chloride ND 0.0346 1 04/26/2023 04:21 WG2048701
4-Methyl-2-pentanone (MIBK) ND 0.0346 1 04/26/2023 04:21 WG2048701
Methyl tert-butyl ether ND 0.00138 1 04/26/2023 04:21 WG2048701
Naphthalene 0.0336 0.0173 1 04/26/2023 04:21 WG2048701
n-Propylbenzene 0.0336 0.00692 1 04/26/2023 04:21 WG2048701
Styrene ND 0.0173 1 04/26/2023 04:21 WG2048701
1,1,1,2-Tetrachloroethane ND 0.00346 1 04/26/2023 04:21 WG2048701
1,1,2,2-Tetrachloroethane ND 0.00346 1 04/26/2023 04:21 WG2048701
1,1,2-Trichlorotrifluoroethane ND 0.00346 1 04/26/2023 04:21 WG2048701
Tetrachloroethene ND 0.00346 1 04/26/2023 04:21 WG2048701
Toluene 0.220 0.00692 1 04/26/2023 04:21 WG2048701
1,2,3-Trichlorobenzene ND J3 0.0173 1 04/26/2023 04:21 WG2048701
1,2,4-Trichlorobenzene ND J3 0.0173 1 04/26/2023 04:21 WG2048701
1,1,1-Trichloroethane ND 0.00346 1 04/26/2023 04:21 WG2048701
1,1,2-Trichloroethane ND 0.00346 1 04/26/2023 04:21 WG2048701
Trichloroethene ND 0.00138 1 04/26/2023 04:21 WG2048701
Trichlorofluoromethane ND 0.00346 1 04/26/2023 04:21 WG2048701
1,2,3-Trichloropropane ND 0.0173 1 04/26/2023 04:21 WG2048701
1,2,4-Trimethylbenzene 0.245 0.00692 1 04/26/2023 04:21 WG2048701
1,2,3-Trimethylbenzene 0.0809 0.00692 1 04/26/2023 04:21 WG2048701
1,3,5-Trimethylbenzene 0.0683 J3 0.00692 1 04/26/2023 04:21 WG2048701
Vinyl chloride ND 0.00346 1 04/26/2023 04:21 WG2048701
Xylenes, Total 0.112 0.00900 1 04/26/2023 04:21 WG2048701
(S) Toluene-d8 100 75.0-131 04/26/2023 04:21 WG2048701
(S) 4-Bromofluorobenzene 109 67.0-138 04/26/2023 04:21 WG2048701
(S) 1,2-Dichloroethane-d4 84.9 70.0-130 04/26/2023 04:21 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1607939
FD-3
Collected date/time: 04/20/23 15:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 59.3 47.4 10 04/27/2023 06:30 WG2048624
C28-C40 Oil Range 121 47.4 10 04/27/2023 06:30 WG2048624
(S) o-Terphenyl 64.9 18.0-148 04/27/2023 06:30 WG2048624
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0403 1 04/26/2023 23:00 WG2048847
PCB 1221 ND 0.0403 1 04/26/2023 23:00 WG2048847
PCB 1232 ND 0.0403 1 04/26/2023 23:00 WG2048847
PCB 1242 ND 0.0403 1 04/26/2023 23:00 WG2048847
PCB 1248 ND 0.0201 1 04/26/2023 23:00 WG2048847
PCB 1254 ND 0.0201 1 04/26/2023 23:00 WG2048847
PCB 1260 ND 0.0201 1 04/26/2023 23:00 WG2048847
(S) Decachlorobiphenyl 84.3 10.0-135 04/26/2023 23:00 WG2048847
(S) Tetrachloro-m-xylene 68.8 10.0-139 04/26/2023 23:00 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0394 1 04/27/2023 20:22 WG2048869
Acenaphthylene ND 0.0394 1 04/27/2023 20:22 WG2048869
Anthracene ND 0.0394 1 04/27/2023 20:22 WG2048869
Benzidine ND 1.98 1 04/27/2023 20:22 WG2048869
Benzo(a)anthracene ND 0.0394 1 04/27/2023 20:22 WG2048869
Benzo(b)fluoranthene ND 0.0394 1 04/27/2023 20:22 WG2048869
Benzo(k)fluoranthene ND 0.0394 1 04/27/2023 20:22 WG2048869
Benzo(g,h,i)perylene ND 0.0394 1 04/27/2023 20:22 WG2048869
Benzo(a)pyrene ND 0.0394 1 04/27/2023 20:22 WG2048869
Bis(2-chlorethoxy)methane ND 0.394 1 04/27/2023 20:22 WG2048869
Bis(2-chloroethyl)ether ND 0.394 1 04/27/2023 20:22 WG2048869
2,2-Oxybis(1-Chloropropane) ND 0.394 1 04/27/2023 20:22 WG2048869
4-Bromophenyl-phenylether ND 0.394 1 04/27/2023 20:22 WG2048869
2-Chloronaphthalene ND 0.0394 1 04/27/2023 20:22 WG2048869
4-Chlorophenyl-phenylether ND 0.394 1 04/27/2023 20:22 WG2048869
Chrysene ND 0.0394 1 04/27/2023 20:22 WG2048869
Dibenz(a,h)anthracene ND 0.0394 1 04/27/2023 20:22 WG2048869
3,3-Dichlorobenzidine ND 0.394 1 04/27/2023 20:22 WG2048869
2,4-Dinitrotoluene ND 0.394 1 04/27/2023 20:22 WG2048869
2,6-Dinitrotoluene ND 0.394 1 04/27/2023 20:22 WG2048869
Fluoranthene ND 0.0394 1 04/27/2023 20:22 WG2048869
Fluorene ND 0.0394 1 04/27/2023 20:22 WG2048869
Hexachlorobenzene ND 0.394 1 04/27/2023 20:22 WG2048869
Hexachloro-1,3-butadiene ND 0.394 1 04/27/2023 20:22 WG2048869
Hexachlorocyclopentadiene ND 0.394 1 04/27/2023 20:22 WG2048869
Hexachloroethane ND 0.394 1 04/27/2023 20:22 WG2048869
Indeno(1,2,3-cd)pyrene ND 0.0394 1 04/27/2023 20:22 WG2048869
Isophorone ND 0.394 1 04/27/2023 20:22 WG2048869
Naphthalene ND 0.0394 1 04/27/2023 20:22 WG2048869
Nitrobenzene ND 0.394 1 04/27/2023 20:22 WG2048869
n-Nitrosodimethylamine ND 0.394 1 04/27/2023 20:22 WG2048869
n-Nitrosodiphenylamine ND 0.394 1 04/27/2023 20:22 WG2048869
n-Nitrosodi-n-propylamine ND 0.394 1 04/27/2023 20:22 WG2048869
Phenanthrene ND 0.0394 1 04/27/2023 20:22 WG2048869
Benzylbutyl phthalate ND 0.394 1 04/27/2023 20:22 WG2048869
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1607939
FD-3
Collected date/time: 04/20/23 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.394 1 04/27/2023 20:22 WG2048869
Di-n-butyl phthalate ND 0.394 1 04/27/2023 20:22 WG2048869
Diethyl phthalate ND 0.394 1 04/27/2023 20:22 WG2048869
Dimethyl phthalate ND 0.394 1 04/27/2023 20:22 WG2048869
Di-n-octyl phthalate ND 0.394 1 04/27/2023 20:22 WG2048869
Pyrene ND 0.0394 1 04/27/2023 20:22 WG2048869
1,2,4-Trichlorobenzene ND 0.394 1 04/27/2023 20:22 WG2048869
4-Chloro-3-methylphenol ND 0.394 1 04/27/2023 20:22 WG2048869
2-Chlorophenol ND 0.394 1 04/27/2023 20:22 WG2048869
2,4-Dichlorophenol ND 0.394 1 04/27/2023 20:22 WG2048869
2,4-Dimethylphenol ND 0.394 1 04/27/2023 20:22 WG2048869
4,6-Dinitro-2-methylphenol ND 0.394 1 04/27/2023 20:22 WG2048869
2,4-Dinitrophenol ND 0.394 1 04/27/2023 20:22 WG2048869
2-Nitrophenol ND 0.394 1 04/27/2023 20:22 WG2048869
4-Nitrophenol ND 0.394 1 04/27/2023 20:22 WG2048869
Pentachlorophenol ND 0.394 1 04/27/2023 20:22 WG2048869
Phenol ND 0.394 1 04/27/2023 20:22 WG2048869
2,4,6-Trichlorophenol ND 0.394 1 04/27/2023 20:22 WG2048869
(S) Nitrobenzene-d5 38.5 10.0-122 04/27/2023 20:22 WG2048869
(S) 2-Fluorobiphenyl 37.0 15.0-120 04/27/2023 20:22 WG2048869
(S) p-Terphenyl-d14 38.5 10.0-120 04/27/2023 20:22 WG2048869
(S) Phenol-d5 34.2 10.0-120 04/27/2023 20:22 WG2048869
(S) 2-Fluorophenol 38.0 12.0-120 04/27/2023 20:22 WG2048869
(S) 2,4,6-Tribromophenol 42.0 10.0-127 04/27/2023 20:22 WG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00711 1 04/27/2023 01:39 WG2048850
Acenaphthene 0.00784 0.00711 1 04/27/2023 01:39 WG2048850
Acenaphthylene ND 0.00711 1 04/27/2023 01:39 WG2048850
Benzo(a)anthracene 0.0193 0.00711 1 04/27/2023 01:39 WG2048850
Benzo(a)pyrene 0.0162 0.00711 1 04/27/2023 01:39 WG2048850
Benzo(b)fluoranthene 0.0168 0.00711 1 04/27/2023 01:39 WG2048850
Benzo(g,h,i)perylene 0.0182 0.00711 1 04/27/2023 01:39 WG2048850
Benzo(k)fluoranthene ND 0.00711 1 04/27/2023 01:39 WG2048850
Chrysene 0.0219 0.00711 1 04/27/2023 01:39 WG2048850
Dibenz(a,h)anthracene ND 0.00711 1 04/27/2023 01:39 WG2048850
Fluoranthene 0.0397 0.00711 1 04/27/2023 01:39 WG2048850
Fluorene 0.0147 0.00711 1 04/27/2023 01:39 WG2048850
Indeno(1,2,3-cd)pyrene 0.0109 0.00711 1 04/27/2023 01:39 WG2048850
Naphthalene ND 0.0237 1 04/27/2023 01:39 WG2048850
Phenanthrene 0.0584 0.00711 1 04/27/2023 01:39 WG2048850
Pyrene 0.0506 0.00711 1 04/27/2023 01:39 WG2048850
1-Methylnaphthalene ND 0.0237 1 04/27/2023 01:39 WG2048850
2-Methylnaphthalene 0.0267 0.0237 1 04/27/2023 01:39 WG2048850
2-Chloronaphthalene ND 0.0237 1 04/27/2023 01:39 WG2048850
(S) p-Terphenyl-d14 75.2 23.0-120 04/27/2023 01:39 WG2048850
(S) Nitrobenzene-d5 51.8 14.0-149 04/27/2023 01:39 WG2048850
(S) 2-Fluorobiphenyl 66.7 34.0-125 04/27/2023 01:39 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1607939
FD-2
Collected date/time: 04/20/23 16:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.3 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.20 1 04/28/2023 15:36 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0480 1 04/28/2023 12:09 WG2048768
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.40 1 04/28/2023 19:08 WG2050507
Arsenic 14.0 2.40 1 04/27/2023 17:24 WG2048870
Beryllium ND 0.240 1 04/27/2023 17:24 WG2048870
Cadmium ND 0.600 1 04/27/2023 17:24 WG2048870
Chromium 5.62 1.20 1 04/27/2023 17:24 WG2048870
Copper ND 2.40 1 04/27/2023 17:24 WG2048870
Lead 0.879 0.600 1 04/27/2023 17:24 WG2048870
Nickel 3.33 2.40 1 04/27/2023 17:24 WG2048870
Selenium ND 2.40 1 04/27/2023 17:24 WG2048870
Silver ND 1.20 1 04/27/2023 17:24 WG2048870
Thallium ND 2.40 1 04/27/2023 17:24 WG2048870
Zinc 9.99 6.00 1 04/27/2023 17:24 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 5.81 B 3.59 25 04/26/2023 19:38 WG2048964
(S) a,a,a-Trifluorotoluene(FID) 95.6 77.0-120 04/26/2023 19:38 WG2048964
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0718 1 04/26/2023 04:41 WG2048701
Acrylonitrile ND 0.0179 1 04/26/2023 04:41 WG2048701
Benzene ND 0.00144 1 04/26/2023 04:41 WG2048701
Bromobenzene ND 0.0179 1 04/26/2023 04:41 WG2048701
Bromodichloromethane ND 0.00359 1 04/26/2023 04:41 WG2048701
Bromoform ND 0.0359 1 04/26/2023 04:41 WG2048701
Bromomethane ND 0.0179 1 04/26/2023 04:41 WG2048701
n-Butylbenzene ND 0.0179 1 04/26/2023 04:41 WG2048701
sec-Butylbenzene ND J3 0.0179 1 04/26/2023 04:41 WG2048701
tert-Butylbenzene ND J3 0.00718 1 04/26/2023 04:41 WG2048701
Carbon tetrachloride ND 0.00718 1 04/26/2023 04:41 WG2048701
Chlorobenzene ND 0.00359 1 04/26/2023 04:41 WG2048701
Chlorodibromomethane ND 0.00359 1 04/26/2023 04:41 WG2048701
Chloroethane ND 0.00718 1 04/26/2023 04:41 WG2048701
Chloroform ND 0.00359 1 04/26/2023 04:41 WG2048701
Chloromethane ND 0.0179 1 04/26/2023 04:41 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1607939
FD-2
Collected date/time: 04/20/23 16:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00359 1 04/26/2023 04:41 WG2048701
4-Chlorotoluene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,2-Dibromo-3-Chloropropane ND 0.0359 1 04/26/2023 04:41 WG2048701
1,2-Dibromoethane ND 0.00359 1 04/26/2023 04:41 WG2048701
Dibromomethane ND 0.00718 1 04/26/2023 04:41 WG2048701
1,2-Dichlorobenzene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,3-Dichlorobenzene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,4-Dichlorobenzene ND 0.00718 1 04/26/2023 04:41 WG2048701
Dichlorodifluoromethane ND 0.00359 1 04/26/2023 04:41 WG2048701
1,1-Dichloroethane ND J4 0.00359 1 04/26/2023 04:41 WG2048701
1,2-Dichloroethane ND 0.00359 1 04/26/2023 04:41 WG2048701
1,1-Dichloroethene ND 0.00359 1 04/26/2023 04:41 WG2048701
cis-1,2-Dichloroethene ND 0.00359 1 04/26/2023 04:41 WG2048701
trans-1,2-Dichloroethene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,2-Dichloropropane ND J4 0.00718 1 04/26/2023 04:41 WG2048701
1,1-Dichloropropene ND J4 0.00359 1 04/26/2023 04:41 WG2048701
1,3-Dichloropropane ND 0.00718 1 04/26/2023 04:41 WG2048701
cis-1,3-Dichloropropene ND 0.00359 1 04/26/2023 04:41 WG2048701
trans-1,3-Dichloropropene ND 0.00718 1 04/26/2023 04:41 WG2048701
2,2-Dichloropropane ND J3 0.00359 1 04/26/2023 04:41 WG2048701
Di-isopropyl ether ND J4 0.00144 1 04/26/2023 04:41 WG2048701
Ethylbenzene ND J3 0.00359 1 04/26/2023 04:41 WG2048701
Hexachloro-1,3-butadiene ND 0.0359 1 04/26/2023 04:41 WG2048701
Isopropylbenzene ND J3 0.00359 1 04/26/2023 04:41 WG2048701
p-Isopropyltoluene ND J3 0.00718 1 04/26/2023 04:41 WG2048701
2-Butanone (MEK)ND 0.144 1 04/26/2023 04:41 WG2048701
Methylene Chloride ND 0.0359 1 04/26/2023 04:41 WG2048701
4-Methyl-2-pentanone (MIBK) ND 0.0359 1 04/26/2023 04:41 WG2048701
Methyl tert-butyl ether ND 0.00144 1 04/26/2023 04:41 WG2048701
Naphthalene ND 0.0179 1 04/26/2023 04:41 WG2048701
n-Propylbenzene ND 0.00718 1 04/26/2023 04:41 WG2048701
Styrene ND 0.0179 1 04/26/2023 04:41 WG2048701
1,1,1,2-Tetrachloroethane ND 0.00359 1 04/26/2023 04:41 WG2048701
1,1,2,2-Tetrachloroethane ND 0.00359 1 04/26/2023 04:41 WG2048701
1,1,2-Trichlorotrifluoroethane ND 0.00359 1 04/26/2023 04:41 WG2048701
Tetrachloroethene ND 0.00359 1 04/26/2023 04:41 WG2048701
Toluene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,2,3-Trichlorobenzene ND J3 0.0179 1 04/26/2023 04:41 WG2048701
1,2,4-Trichlorobenzene ND J3 0.0179 1 04/26/2023 04:41 WG2048701
1,1,1-Trichloroethane ND 0.00359 1 04/26/2023 04:41 WG2048701
1,1,2-Trichloroethane ND 0.00359 1 04/26/2023 04:41 WG2048701
Trichloroethene ND 0.00144 1 04/26/2023 04:41 WG2048701
Trichlorofluoromethane ND 0.00359 1 04/26/2023 04:41 WG2048701
1,2,3-Trichloropropane ND 0.0179 1 04/26/2023 04:41 WG2048701
1,2,4-Trimethylbenzene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,2,3-Trimethylbenzene ND 0.00718 1 04/26/2023 04:41 WG2048701
1,3,5-Trimethylbenzene ND J3 0.00718 1 04/26/2023 04:41 WG2048701
Vinyl chloride ND 0.00359 1 04/26/2023 04:41 WG2048701
Xylenes, Total ND 0.00933 1 04/26/2023 04:41 WG2048701
(S) Toluene-d8 98.9 75.0-131 04/26/2023 04:41 WG2048701
(S) 4-Bromofluorobenzene 108 67.0-138 04/26/2023 04:41 WG2048701
(S) 1,2-Dichloroethane-d4 77.5 70.0-130 04/26/2023 04:41 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1607939
FD-2
Collected date/time: 04/20/23 16:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.80 1 04/27/2023 02:19 WG2048624
C28-C40 Oil Range ND 4.80 1 04/27/2023 02:19 WG2048624
(S) o-Terphenyl 70.9 18.0-148 04/27/2023 02:19 WG2048624
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0408 1 04/26/2023 23:10 WG2048847
PCB 1221 ND 0.0408 1 04/26/2023 23:10 WG2048847
PCB 1232 ND 0.0408 1 04/26/2023 23:10 WG2048847
PCB 1242 ND 0.0408 1 04/26/2023 23:10 WG2048847
PCB 1248 ND 0.0204 1 04/26/2023 23:10 WG2048847
PCB 1254 ND 0.0204 1 04/26/2023 23:10 WG2048847
PCB 1260 ND 0.0204 1 04/26/2023 23:10 WG2048847
(S) Decachlorobiphenyl 72.2 10.0-135 04/26/2023 23:10 WG2048847
(S) Tetrachloro-m-xylene 66.3 10.0-139 04/26/2023 23:10 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0400 1 04/27/2023 01:07 WG2048869
Acenaphthylene ND 0.0400 1 04/27/2023 01:07 WG2048869
Anthracene ND 0.0400 1 04/27/2023 01:07 WG2048869
Benzidine ND 2.00 1 04/27/2023 01:07 WG2048869
Benzo(a)anthracene ND 0.0400 1 04/27/2023 01:07 WG2048869
Benzo(b)fluoranthene ND 0.0400 1 04/27/2023 01:07 WG2048869
Benzo(k)fluoranthene ND 0.0400 1 04/27/2023 01:07 WG2048869
Benzo(g,h,i)perylene ND 0.0400 1 04/27/2023 01:07 WG2048869
Benzo(a)pyrene ND 0.0400 1 04/27/2023 01:07 WG2048869
Bis(2-chlorethoxy)methane ND 0.400 1 04/27/2023 01:07 WG2048869
Bis(2-chloroethyl)ether ND 0.400 1 04/27/2023 01:07 WG2048869
2,2-Oxybis(1-Chloropropane) ND 0.400 1 04/27/2023 01:07 WG2048869
4-Bromophenyl-phenylether ND 0.400 1 04/27/2023 01:07 WG2048869
2-Chloronaphthalene ND 0.0400 1 04/27/2023 01:07 WG2048869
4-Chlorophenyl-phenylether ND 0.400 1 04/27/2023 01:07 WG2048869
Chrysene ND 0.0400 1 04/27/2023 01:07 WG2048869
Dibenz(a,h)anthracene ND 0.0400 1 04/27/2023 01:07 WG2048869
3,3-Dichlorobenzidine ND 0.400 1 04/27/2023 01:07 WG2048869
2,4-Dinitrotoluene ND 0.400 1 04/27/2023 01:07 WG2048869
2,6-Dinitrotoluene ND 0.400 1 04/27/2023 01:07 WG2048869
Fluoranthene ND 0.0400 1 04/27/2023 01:07 WG2048869
Fluorene ND 0.0400 1 04/27/2023 01:07 WG2048869
Hexachlorobenzene ND 0.400 1 04/27/2023 01:07 WG2048869
Hexachloro-1,3-butadiene ND 0.400 1 04/27/2023 01:07 WG2048869
Hexachlorocyclopentadiene ND 0.400 1 04/27/2023 01:07 WG2048869
Hexachloroethane ND 0.400 1 04/27/2023 01:07 WG2048869
Indeno(1,2,3-cd)pyrene ND 0.0400 1 04/27/2023 01:07 WG2048869
Isophorone ND 0.400 1 04/27/2023 01:07 WG2048869
Naphthalene ND 0.0400 1 04/27/2023 01:07 WG2048869
Nitrobenzene ND 0.400 1 04/27/2023 01:07 WG2048869
n-Nitrosodimethylamine ND 0.400 1 04/27/2023 01:07 WG2048869
n-Nitrosodiphenylamine ND 0.400 1 04/27/2023 01:07 WG2048869
n-Nitrosodi-n-propylamine ND 0.400 1 04/27/2023 01:07 WG2048869
Phenanthrene ND 0.0400 1 04/27/2023 01:07 WG2048869
Benzylbutyl phthalate ND 0.400 1 04/27/2023 01:07 WG2048869
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1607939
FD-2
Collected date/time: 04/20/23 16:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.400 1 04/27/2023 01:07 WG2048869
Di-n-butyl phthalate ND 0.400 1 04/27/2023 01:07 WG2048869
Diethyl phthalate ND 0.400 1 04/27/2023 01:07 WG2048869
Dimethyl phthalate ND 0.400 1 04/27/2023 01:07 WG2048869
Di-n-octyl phthalate ND 0.400 1 04/27/2023 01:07 WG2048869
Pyrene ND 0.0400 1 04/27/2023 01:07 WG2048869
1,2,4-Trichlorobenzene ND 0.400 1 04/27/2023 01:07 WG2048869
4-Chloro-3-methylphenol ND 0.400 1 04/27/2023 01:07 WG2048869
2-Chlorophenol ND 0.400 1 04/27/2023 01:07 WG2048869
2,4-Dichlorophenol ND 0.400 1 04/27/2023 01:07 WG2048869
2,4-Dimethylphenol ND 0.400 1 04/27/2023 01:07 WG2048869
4,6-Dinitro-2-methylphenol ND 0.400 1 04/27/2023 01:07 WG2048869
2,4-Dinitrophenol ND 0.400 1 04/27/2023 01:07 WG2048869
2-Nitrophenol ND 0.400 1 04/27/2023 01:07 WG2048869
4-Nitrophenol ND 0.400 1 04/27/2023 01:07 WG2048869
Pentachlorophenol ND 0.400 1 04/27/2023 01:07 WG2048869
Phenol ND 0.400 1 04/27/2023 01:07 WG2048869
2,4,6-Trichlorophenol ND 0.400 1 04/27/2023 01:07 WG2048869
(S) Nitrobenzene-d5 40.4 10.0-122 04/27/2023 01:07 WG2048869
(S) 2-Fluorobiphenyl 39.5 15.0-120 04/27/2023 01:07 WG2048869
(S) p-Terphenyl-d14 41.3 10.0-120 04/27/2023 01:07 WG2048869
(S) Phenol-d5 44.1 10.0-120 04/27/2023 01:07 WG2048869
(S) 2-Fluorophenol 50.2 12.0-120 04/27/2023 01:07 WG2048869
(S) 2,4,6-Tribromophenol 43.0 10.0-127 04/27/2023 01:07 WG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00720 1 04/26/2023 19:46 WG2048850
Acenaphthene ND 0.00720 1 04/26/2023 19:46 WG2048850
Acenaphthylene ND 0.00720 1 04/26/2023 19:46 WG2048850
Benzo(a)anthracene ND 0.00720 1 04/26/2023 19:46 WG2048850
Benzo(a)pyrene ND 0.00720 1 04/26/2023 19:46 WG2048850
Benzo(b)fluoranthene ND 0.00720 1 04/26/2023 19:46 WG2048850
Benzo(g,h,i)perylene ND 0.00720 1 04/26/2023 19:46 WG2048850
Benzo(k)fluoranthene ND 0.00720 1 04/26/2023 19:46 WG2048850
Chrysene ND 0.00720 1 04/26/2023 19:46 WG2048850
Dibenz(a,h)anthracene ND 0.00720 1 04/26/2023 19:46 WG2048850
Fluoranthene ND 0.00720 1 04/26/2023 19:46 WG2048850
Fluorene ND 0.00720 1 04/26/2023 19:46 WG2048850
Indeno(1,2,3-cd)pyrene ND 0.00720 1 04/26/2023 19:46 WG2048850
Naphthalene ND 0.0240 1 04/26/2023 19:46 WG2048850
Phenanthrene ND 0.00720 1 04/26/2023 19:46 WG2048850
Pyrene ND 0.00720 1 04/26/2023 19:46 WG2048850
1-Methylnaphthalene ND 0.0240 1 04/26/2023 19:46 WG2048850
2-Methylnaphthalene ND 0.0240 1 04/26/2023 19:46 WG2048850
2-Chloronaphthalene ND 0.0240 1 04/26/2023 19:46 WG2048850
(S) p-Terphenyl-d14 76.6 23.0-120 04/26/2023 19:46 WG2048850
(S) Nitrobenzene-d5 55.5 14.0-149 04/26/2023 19:46 WG2048850
(S) 2-Fluorobiphenyl 79.1 34.0-125 04/26/2023 19:46 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.8 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.32 1 04/28/2023 15:42 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0528 1 04/28/2023 12:55 WG2048768
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.64 1 04/28/2023 19:17 WG2050507
Arsenic 151 2.64 1 04/27/2023 17:27 WG2048870
Beryllium ND 0.264 1 04/27/2023 17:27 WG2048870
Cadmium ND 0.660 1 04/27/2023 17:27 WG2048870
Chromium 7.96 1.32 1 04/27/2023 17:27 WG2048870
Copper 5.62 2.64 1 04/27/2023 17:27 WG2048870
Lead 4.35 0.660 1 04/27/2023 17:27 WG2048870
Nickel 7.72 2.64 1 04/27/2023 17:27 WG2048870
Selenium ND 2.64 1 04/27/2023 17:27 WG2048870
Silver ND 1.32 1 04/27/2023 17:27 WG2048870
Thallium ND 2.64 1 04/27/2023 17:27 WG2048870
Zinc 18.3 6.60 1 04/27/2023 17:27 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.31 25 04/27/2023 14:10 WG2049437
(S) a,a,a-Trifluorotoluene(FID) 98.2 77.0-120 04/27/2023 14:10 WG2049437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0862 1 04/26/2023 05:00 WG2048701
Acrylonitrile ND 0.0216 1 04/26/2023 05:00 WG2048701
Benzene ND 0.00172 1 04/26/2023 05:00 WG2048701
Bromobenzene ND 0.0216 1 04/26/2023 05:00 WG2048701
Bromodichloromethane ND 0.00431 1 04/26/2023 05:00 WG2048701
Bromoform ND 0.0431 1 04/26/2023 05:00 WG2048701
Bromomethane ND 0.0216 1 04/26/2023 05:00 WG2048701
n-Butylbenzene ND 0.0216 1 04/26/2023 05:00 WG2048701
sec-Butylbenzene ND J3 0.0216 1 04/26/2023 05:00 WG2048701
tert-Butylbenzene ND J3 0.00862 1 04/26/2023 05:00 WG2048701
Carbon tetrachloride ND 0.00862 1 04/26/2023 05:00 WG2048701
Chlorobenzene ND 0.00431 1 04/26/2023 05:00 WG2048701
Chlorodibromomethane ND 0.00431 1 04/26/2023 05:00 WG2048701
Chloroethane ND 0.00862 1 04/26/2023 05:00 WG2048701
Chloroform ND 0.00431 1 04/26/2023 05:00 WG2048701
Chloromethane ND 0.0216 1 04/26/2023 05:00 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00431 1 04/26/2023 05:00 WG2048701
4-Chlorotoluene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,2-Dibromo-3-Chloropropane ND 0.0431 1 04/26/2023 05:00 WG2048701
1,2-Dibromoethane ND 0.00431 1 04/26/2023 05:00 WG2048701
Dibromomethane ND 0.00862 1 04/26/2023 05:00 WG2048701
1,2-Dichlorobenzene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,3-Dichlorobenzene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,4-Dichlorobenzene ND 0.00862 1 04/26/2023 05:00 WG2048701
Dichlorodifluoromethane ND 0.00431 1 04/26/2023 05:00 WG2048701
1,1-Dichloroethane ND J4 0.00431 1 04/26/2023 05:00 WG2048701
1,2-Dichloroethane ND 0.00431 1 04/26/2023 05:00 WG2048701
1,1-Dichloroethene ND 0.00431 1 04/26/2023 05:00 WG2048701
cis-1,2-Dichloroethene ND 0.00431 1 04/26/2023 05:00 WG2048701
trans-1,2-Dichloroethene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,2-Dichloropropane ND J4 0.00862 1 04/26/2023 05:00 WG2048701
1,1-Dichloropropene ND J4 0.00431 1 04/26/2023 05:00 WG2048701
1,3-Dichloropropane ND 0.00862 1 04/26/2023 05:00 WG2048701
cis-1,3-Dichloropropene ND 0.00431 1 04/26/2023 05:00 WG2048701
trans-1,3-Dichloropropene ND 0.00862 1 04/26/2023 05:00 WG2048701
2,2-Dichloropropane ND J3 0.00431 1 04/26/2023 05:00 WG2048701
Di-isopropyl ether ND J4 0.00172 1 04/26/2023 05:00 WG2048701
Ethylbenzene ND J3 0.00431 1 04/26/2023 05:00 WG2048701
Hexachloro-1,3-butadiene ND 0.0431 1 04/26/2023 05:00 WG2048701
Isopropylbenzene ND J3 0.00431 1 04/26/2023 05:00 WG2048701
p-Isopropyltoluene ND J3 0.00862 1 04/26/2023 05:00 WG2048701
2-Butanone (MEK)ND 0.172 1 04/26/2023 05:00 WG2048701
Methylene Chloride ND 0.0431 1 04/26/2023 05:00 WG2048701
4-Methyl-2-pentanone (MIBK) ND 0.0431 1 04/26/2023 05:00 WG2048701
Methyl tert-butyl ether ND 0.00172 1 04/26/2023 05:00 WG2048701
Naphthalene ND 0.0216 1 04/26/2023 05:00 WG2048701
n-Propylbenzene ND 0.00862 1 04/26/2023 05:00 WG2048701
Styrene ND 0.0216 1 04/26/2023 05:00 WG2048701
1,1,1,2-Tetrachloroethane ND 0.00431 1 04/26/2023 05:00 WG2048701
1,1,2,2-Tetrachloroethane ND 0.00431 1 04/26/2023 05:00 WG2048701
1,1,2-Trichlorotrifluoroethane ND 0.00431 1 04/26/2023 05:00 WG2048701
Tetrachloroethene ND 0.00431 1 04/26/2023 05:00 WG2048701
Toluene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,2,3-Trichlorobenzene ND J3 0.0216 1 04/26/2023 05:00 WG2048701
1,2,4-Trichlorobenzene ND J3 0.0216 1 04/26/2023 05:00 WG2048701
1,1,1-Trichloroethane ND 0.00431 1 04/26/2023 05:00 WG2048701
1,1,2-Trichloroethane ND 0.00431 1 04/26/2023 05:00 WG2048701
Trichloroethene ND 0.00172 1 04/26/2023 05:00 WG2048701
Trichlorofluoromethane ND 0.00431 1 04/26/2023 05:00 WG2048701
1,2,3-Trichloropropane ND 0.0216 1 04/26/2023 05:00 WG2048701
1,2,4-Trimethylbenzene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,2,3-Trimethylbenzene ND 0.00862 1 04/26/2023 05:00 WG2048701
1,3,5-Trimethylbenzene ND J3 0.00862 1 04/26/2023 05:00 WG2048701
Vinyl chloride ND 0.00431 1 04/26/2023 05:00 WG2048701
Xylenes, Total ND 0.0112 1 04/26/2023 05:00 WG2048701
(S) Toluene-d8 98.4 75.0-131 04/26/2023 05:00 WG2048701
(S) 4-Bromofluorobenzene 111 67.0-138 04/26/2023 05:00 WG2048701
(S) 1,2-Dichloroethane-d4 85.2 70.0-130 04/26/2023 05:00 WG2048701
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 14.9 10.6 2 04/27/2023 08:56 WG2048624
C28-C40 Oil Range 64.0 10.6 2 04/27/2023 08:56 WG2048624
(S) o-Terphenyl 69.4 18.0-148 04/27/2023 08:56 WG2048624
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0449 1 04/26/2023 23:20 WG2048847
PCB 1221 ND 0.0449 1 04/26/2023 23:20 WG2048847
PCB 1232 ND 0.0449 1 04/26/2023 23:20 WG2048847
PCB 1242 ND 0.0449 1 04/26/2023 23:20 WG2048847
PCB 1248 ND 0.0224 1 04/26/2023 23:20 WG2048847
PCB 1254 ND 0.0224 1 04/26/2023 23:20 WG2048847
PCB 1260 ND 0.0224 1 04/26/2023 23:20 WG2048847
(S) Decachlorobiphenyl 70.9 10.0-135 04/26/2023 23:20 WG2048847
(S) Tetrachloro-m-xylene 66.9 10.0-139 04/26/2023 23:20 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0440 1 04/27/2023 07:42 WG2048871
Acenaphthylene ND 0.0440 1 04/27/2023 07:42 WG2048871
Anthracene ND 0.0440 1 04/27/2023 07:42 WG2048871
Benzidine ND 2.20 1 04/27/2023 07:42 WG2048871
Benzo(a)anthracene ND 0.0440 1 04/27/2023 07:42 WG2048871
Benzo(b)fluoranthene ND 0.0440 1 04/27/2023 07:42 WG2048871
Benzo(k)fluoranthene ND 0.0440 1 04/27/2023 07:42 WG2048871
Benzo(g,h,i)perylene ND 0.0440 1 04/27/2023 07:42 WG2048871
Benzo(a)pyrene ND 0.0440 1 04/27/2023 07:42 WG2048871
Bis(2-chlorethoxy)methane ND 0.440 1 04/27/2023 07:42 WG2048871
Bis(2-chloroethyl)ether ND 0.440 1 04/27/2023 07:42 WG2048871
2,2-Oxybis(1-Chloropropane) ND 0.440 1 04/27/2023 07:42 WG2048871
4-Bromophenyl-phenylether ND 0.440 1 04/27/2023 07:42 WG2048871
2-Chloronaphthalene ND 0.0440 1 04/27/2023 07:42 WG2048871
4-Chlorophenyl-phenylether ND 0.440 1 04/27/2023 07:42 WG2048871
Chrysene ND 0.0440 1 04/27/2023 07:42 WG2048871
Dibenz(a,h)anthracene ND 0.0440 1 04/27/2023 07:42 WG2048871
3,3-Dichlorobenzidine ND 0.440 1 04/27/2023 07:42 WG2048871
2,4-Dinitrotoluene ND 0.440 1 04/27/2023 07:42 WG2048871
2,6-Dinitrotoluene ND 0.440 1 04/27/2023 07:42 WG2048871
Fluoranthene 0.0723 0.0440 1 04/27/2023 07:42 WG2048871
Fluorene ND 0.0440 1 04/27/2023 07:42 WG2048871
Hexachlorobenzene ND 0.440 1 04/27/2023 07:42 WG2048871
Hexachloro-1,3-butadiene ND 0.440 1 04/27/2023 07:42 WG2048871
Hexachlorocyclopentadiene ND 0.440 1 04/27/2023 07:42 WG2048871
Hexachloroethane ND 0.440 1 04/27/2023 07:42 WG2048871
Indeno(1,2,3-cd)pyrene ND 0.0440 1 04/27/2023 07:42 WG2048871
Isophorone ND 0.440 1 04/27/2023 07:42 WG2048871
Naphthalene ND 0.0440 1 04/27/2023 07:42 WG2048871
Nitrobenzene ND 0.440 1 04/27/2023 07:42 WG2048871
n-Nitrosodimethylamine ND 0.440 1 04/27/2023 07:42 WG2048871
n-Nitrosodiphenylamine ND 0.440 1 04/27/2023 07:42 WG2048871
n-Nitrosodi-n-propylamine ND 0.440 1 04/27/2023 07:42 WG2048871
Phenanthrene 0.0644 0.0440 1 04/27/2023 07:42 WG2048871
Benzylbutyl phthalate ND 0.440 1 04/27/2023 07:42 WG2048871
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.440 1 04/27/2023 07:42 WG2048871
Di-n-butyl phthalate ND 0.440 1 04/27/2023 07:42 WG2048871
Diethyl phthalate ND 0.440 1 04/27/2023 07:42 WG2048871
Dimethyl phthalate ND 0.440 1 04/27/2023 07:42 WG2048871
Di-n-octyl phthalate ND 0.440 1 04/27/2023 07:42 WG2048871
Pyrene 0.0689 0.0440 1 04/27/2023 07:42 WG2048871
1,2,4-Trichlorobenzene ND 0.440 1 04/27/2023 07:42 WG2048871
4-Chloro-3-methylphenol ND 0.440 1 04/27/2023 07:42 WG2048871
2-Chlorophenol ND 0.440 1 04/27/2023 07:42 WG2048871
2,4-Dichlorophenol ND 0.440 1 04/27/2023 07:42 WG2048871
2,4-Dimethylphenol ND 0.440 1 04/27/2023 07:42 WG2048871
4,6-Dinitro-2-methylphenol ND 0.440 1 04/27/2023 07:42 WG2048871
2,4-Dinitrophenol ND 0.440 1 04/27/2023 07:42 WG2048871
2-Nitrophenol ND 0.440 1 04/27/2023 07:42 WG2048871
4-Nitrophenol ND 0.440 1 04/27/2023 07:42 WG2048871
Pentachlorophenol ND 0.440 1 04/27/2023 07:42 WG2048871
Phenol ND 0.440 1 04/27/2023 07:42 WG2048871
2,4,6-Trichlorophenol ND 0.440 1 04/27/2023 07:42 WG2048871
(S) Nitrobenzene-d5 40.5 10.0-122 04/27/2023 07:42 WG2048871
(S) 2-Fluorobiphenyl 47.7 15.0-120 04/27/2023 07:42 WG2048871
(S) p-Terphenyl-d14 53.5 10.0-120 04/27/2023 07:42 WG2048871
(S) Phenol-d5 43.8 10.0-120 04/27/2023 07:42 WG2048871
(S) 2-Fluorophenol 49.5 12.0-120 04/27/2023 07:42 WG2048871
(S) 2,4,6-Tribromophenol 59.0 10.0-127 04/27/2023 07:42 WG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.0111 0.00792 1 04/27/2023 00:40 WG2048850
Acenaphthene 0.00954 0.00792 1 04/27/2023 00:40 WG2048850
Acenaphthylene ND 0.00792 1 04/27/2023 00:40 WG2048850
Benzo(a)anthracene 0.0226 0.00792 1 04/27/2023 00:40 WG2048850
Benzo(a)pyrene 0.0203 0.00792 1 04/27/2023 00:40 WG2048850
Benzo(b)fluoranthene 0.0214 0.00792 1 04/27/2023 00:40 WG2048850
Benzo(g,h,i)perylene 0.0152 0.00792 1 04/27/2023 00:40 WG2048850
Benzo(k)fluoranthene 0.00931 0.00792 1 04/27/2023 00:40 WG2048850
Chrysene 0.0279 0.00792 1 04/27/2023 00:40 WG2048850
Dibenz(a,h)anthracene ND 0.00792 1 04/27/2023 00:40 WG2048850
Fluoranthene 0.0516 0.00792 1 04/27/2023 00:40 WG2048850
Fluorene ND 0.00792 1 04/27/2023 00:40 WG2048850
Indeno(1,2,3-cd)pyrene 0.0129 0.00792 1 04/27/2023 00:40 WG2048850
Naphthalene ND 0.0264 1 04/27/2023 00:40 WG2048850
Phenanthrene 0.0448 0.00792 1 04/27/2023 00:40 WG2048850
Pyrene 0.0531 0.00792 1 04/27/2023 00:40 WG2048850
1-Methylnaphthalene ND 0.0264 1 04/27/2023 00:40 WG2048850
2-Methylnaphthalene ND 0.0264 1 04/27/2023 00:40 WG2048850
2-Chloronaphthalene ND 0.0264 1 04/27/2023 00:40 WG2048850
(S) p-Terphenyl-d14 59.3 23.0-120 04/27/2023 00:40 WG2048850
(S) Nitrobenzene-d5 45.8 14.0-149 04/27/2023 00:40 WG2048850
(S) 2-Fluorobiphenyl 60.9 34.0-125 04/27/2023 00:40 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.2 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium 1.44 1.22 1 04/28/2023 15:47 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0487 1 04/28/2023 12:58 WG2048768
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.43 1 04/28/2023 19:20 WG2050507
Arsenic 5.97 2.43 1 04/27/2023 17:30 WG2048870
Beryllium ND 0.243 1 04/27/2023 17:30 WG2048870
Cadmium ND 0.608 1 04/27/2023 17:30 WG2048870
Chromium 39.6 1.22 1 04/27/2023 17:30 WG2048870
Copper 52.1 2.43 1 04/27/2023 17:30 WG2048870
Lead 10.7 0.608 1 04/27/2023 17:30 WG2048870
Nickel 21.4 2.43 1 04/27/2023 17:30 WG2048870
Selenium ND 2.43 1 04/27/2023 17:30 WG2048870
Silver ND 1.22 1 04/27/2023 17:30 WG2048870
Thallium ND 2.43 1 04/27/2023 17:30 WG2048870
Zinc 42.8 6.08 1 04/27/2023 17:30 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.65 25 04/27/2023 14:30 WG2049437
(S) a,a,a-Trifluorotoluene(FID) 97.6 77.0-120 04/27/2023 14:30 WG2049437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0729 1 04/26/2023 01:10 WG2048704
Acrylonitrile ND 0.0182 1 04/26/2023 01:10 WG2048704
Benzene ND 0.00146 1 04/26/2023 01:10 WG2048704
Bromobenzene ND 0.0182 1 04/26/2023 01:10 WG2048704
Bromodichloromethane ND 0.00365 1 04/26/2023 01:10 WG2048704
Bromoform ND 0.0365 1 04/26/2023 01:10 WG2048704
Bromomethane ND 0.0182 1 04/26/2023 01:10 WG2048704
n-Butylbenzene ND 0.0182 1 04/26/2023 01:10 WG2048704
sec-Butylbenzene ND 0.0182 1 04/26/2023 01:10 WG2048704
tert-Butylbenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
Carbon tetrachloride ND 0.00729 1 04/26/2023 01:10 WG2048704
Chlorobenzene ND 0.00365 1 04/26/2023 01:10 WG2048704
Chlorodibromomethane ND 0.00365 1 04/26/2023 01:10 WG2048704
Chloroethane ND 0.00729 1 04/26/2023 01:10 WG2048704
Chloroform ND 0.00365 1 04/26/2023 01:10 WG2048704
Chloromethane ND 0.0182 1 04/26/2023 01:10 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00365 1 04/26/2023 01:10 WG2048704
4-Chlorotoluene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,2-Dibromo-3-Chloropropane ND 0.0365 1 04/26/2023 01:10 WG2048704
1,2-Dibromoethane ND 0.00365 1 04/26/2023 01:10 WG2048704
Dibromomethane ND 0.00729 1 04/26/2023 01:10 WG2048704
1,2-Dichlorobenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,3-Dichlorobenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,4-Dichlorobenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
Dichlorodifluoromethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,1-Dichloroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,2-Dichloroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,1-Dichloroethene ND 0.00365 1 04/26/2023 01:10 WG2048704
cis-1,2-Dichloroethene ND 0.00365 1 04/26/2023 01:10 WG2048704
trans-1,2-Dichloroethene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,2-Dichloropropane ND 0.00729 1 04/26/2023 01:10 WG2048704
1,1-Dichloropropene ND 0.00365 1 04/26/2023 01:10 WG2048704
1,3-Dichloropropane ND 0.00729 1 04/26/2023 01:10 WG2048704
cis-1,3-Dichloropropene ND 0.00365 1 04/26/2023 01:10 WG2048704
trans-1,3-Dichloropropene ND 0.00729 1 04/26/2023 01:10 WG2048704
2,2-Dichloropropane ND 0.00365 1 04/26/2023 01:10 WG2048704
Di-isopropyl ether ND 0.00146 1 04/26/2023 01:10 WG2048704
Ethylbenzene ND 0.00365 1 04/26/2023 01:10 WG2048704
Hexachloro-1,3-butadiene ND 0.0365 1 04/26/2023 01:10 WG2048704
Isopropylbenzene ND 0.00365 1 04/26/2023 01:10 WG2048704
p-Isopropyltoluene ND 0.00729 1 04/26/2023 01:10 WG2048704
2-Butanone (MEK)ND 0.146 1 04/26/2023 01:10 WG2048704
Methylene Chloride ND 0.0365 1 04/26/2023 01:10 WG2048704
4-Methyl-2-pentanone (MIBK) ND 0.0365 1 04/26/2023 01:10 WG2048704
Methyl tert-butyl ether ND 0.00146 1 04/26/2023 01:10 WG2048704
Naphthalene ND 0.0182 1 04/26/2023 01:10 WG2048704
n-Propylbenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
Styrene ND 0.0182 1 04/26/2023 01:10 WG2048704
1,1,1,2-Tetrachloroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,1,2,2-Tetrachloroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,1,2-Trichlorotrifluoroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
Tetrachloroethene ND 0.00365 1 04/26/2023 01:10 WG2048704
Toluene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,2,3-Trichlorobenzene ND 0.0182 1 04/26/2023 01:10 WG2048704
1,2,4-Trichlorobenzene ND 0.0182 1 04/26/2023 01:10 WG2048704
1,1,1-Trichloroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,1,2-Trichloroethane ND 0.00365 1 04/26/2023 01:10 WG2048704
Trichloroethene ND 0.00146 1 04/26/2023 01:10 WG2048704
Trichlorofluoromethane ND 0.00365 1 04/26/2023 01:10 WG2048704
1,2,3-Trichloropropane ND 0.0182 1 04/26/2023 01:10 WG2048704
1,2,4-Trimethylbenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,2,3-Trimethylbenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
1,3,5-Trimethylbenzene ND 0.00729 1 04/26/2023 01:10 WG2048704
Vinyl chloride ND 0.00365 1 04/26/2023 01:10 WG2048704
Xylenes, Total ND 0.00948 1 04/26/2023 01:10 WG2048704
(S) Toluene-d8 102 75.0-131 04/26/2023 01:10 WG2048704
(S) 4-Bromofluorobenzene 88.7 67.0-138 04/26/2023 01:10 WG2048704
(S) 1,2-Dichloroethane-d4 112 70.0-130 04/26/2023 01:10 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 243 50 04/26/2023 18:22 WG2048845
C28-C40 Oil Range 647 243 50 04/26/2023 18:22 WG2048845
(S) o-Terphenyl 53.2 J7 18.0-148 04/26/2023 18:22 WG2048845
Sample Narrative:
L1607939-06 WG2048845: Cannot run at lower dilution due to viscosity of extract
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0414 1 04/26/2023 23:31 WG2048847
PCB 1221 ND 0.0414 1 04/26/2023 23:31 WG2048847
PCB 1232 ND 0.0414 1 04/26/2023 23:31 WG2048847
PCB 1242 ND 0.0414 1 04/26/2023 23:31 WG2048847
PCB 1248 ND 0.0207 1 04/26/2023 23:31 WG2048847
PCB 1254 ND 0.0207 1 04/26/2023 23:31 WG2048847
PCB 1260 ND 0.0207 1 04/26/2023 23:31 WG2048847
(S) Decachlorobiphenyl 87.0 10.0-135 04/26/2023 23:31 WG2048847
(S) Tetrachloro-m-xylene 74.6 10.0-139 04/26/2023 23:31 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.203 5 04/27/2023 08:23 WG2048871
Acenaphthylene ND 0.203 5 04/27/2023 08:23 WG2048871
Anthracene ND 0.203 5 04/27/2023 08:23 WG2048871
Benzidine ND 10.2 5 04/27/2023 08:23 WG2048871
Benzo(a)anthracene ND 0.203 5 04/27/2023 08:23 WG2048871
Benzo(b)fluoranthene ND 0.203 5 04/27/2023 08:23 WG2048871
Benzo(k)fluoranthene ND 0.203 5 04/27/2023 08:23 WG2048871
Benzo(g,h,i)perylene ND 0.203 5 04/27/2023 08:23 WG2048871
Benzo(a)pyrene ND 0.203 5 04/27/2023 08:23 WG2048871
Bis(2-chlorethoxy)methane ND 2.03 5 04/27/2023 08:23 WG2048871
Bis(2-chloroethyl)ether ND 2.03 5 04/27/2023 08:23 WG2048871
2,2-Oxybis(1-Chloropropane) ND 2.03 5 04/27/2023 08:23 WG2048871
4-Bromophenyl-phenylether ND 2.03 5 04/27/2023 08:23 WG2048871
2-Chloronaphthalene ND 0.203 5 04/27/2023 08:23 WG2048871
4-Chlorophenyl-phenylether ND 2.03 5 04/27/2023 08:23 WG2048871
Chrysene ND 0.203 5 04/27/2023 08:23 WG2048871
Dibenz(a,h)anthracene ND 0.203 5 04/27/2023 08:23 WG2048871
3,3-Dichlorobenzidine ND 2.03 5 04/27/2023 08:23 WG2048871
2,4-Dinitrotoluene ND 2.03 5 04/27/2023 08:23 WG2048871
2,6-Dinitrotoluene ND 2.03 5 04/27/2023 08:23 WG2048871
Fluoranthene ND 0.203 5 04/27/2023 08:23 WG2048871
Fluorene ND 0.203 5 04/27/2023 08:23 WG2048871
Hexachlorobenzene ND 2.03 5 04/27/2023 08:23 WG2048871
Hexachloro-1,3-butadiene ND 2.03 5 04/27/2023 08:23 WG2048871
Hexachlorocyclopentadiene ND 2.03 5 04/27/2023 08:23 WG2048871
Hexachloroethane ND 2.03 5 04/27/2023 08:23 WG2048871
Indeno(1,2,3-cd)pyrene ND 0.203 5 04/27/2023 08:23 WG2048871
Isophorone ND 2.03 5 04/27/2023 08:23 WG2048871
Naphthalene ND 0.203 5 04/27/2023 08:23 WG2048871
Nitrobenzene ND 2.03 5 04/27/2023 08:23 WG2048871
n-Nitrosodimethylamine ND 2.03 5 04/27/2023 08:23 WG2048871
n-Nitrosodiphenylamine ND 2.03 5 04/27/2023 08:23 WG2048871
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
n-Nitrosodi-n-propylamine ND 2.03 5 04/27/2023 08:23 WG2048871
Phenanthrene ND 0.203 5 04/27/2023 08:23 WG2048871
Benzylbutyl phthalate ND 2.03 5 04/27/2023 08:23 WG2048871
Bis(2-ethylhexyl)phthalate ND 2.03 5 04/27/2023 08:23 WG2048871
Di-n-butyl phthalate ND 2.03 5 04/27/2023 08:23 WG2048871
Diethyl phthalate ND 2.03 5 04/27/2023 08:23 WG2048871
Dimethyl phthalate ND 2.03 5 04/27/2023 08:23 WG2048871
Di-n-octyl phthalate ND 2.03 5 04/27/2023 08:23 WG2048871
Pyrene ND 0.203 5 04/27/2023 08:23 WG2048871
1,2,4-Trichlorobenzene ND 2.03 5 04/27/2023 08:23 WG2048871
4-Chloro-3-methylphenol ND 2.03 5 04/27/2023 08:23 WG2048871
2-Chlorophenol ND 2.03 5 04/27/2023 08:23 WG2048871
2,4-Dichlorophenol ND 2.03 5 04/27/2023 08:23 WG2048871
2,4-Dimethylphenol ND 2.03 5 04/27/2023 08:23 WG2048871
4,6-Dinitro-2-methylphenol ND 2.03 5 04/27/2023 08:23 WG2048871
2,4-Dinitrophenol ND 2.03 5 04/27/2023 08:23 WG2048871
2-Nitrophenol ND 2.03 5 04/27/2023 08:23 WG2048871
4-Nitrophenol ND 2.03 5 04/27/2023 08:23 WG2048871
Pentachlorophenol ND 2.03 5 04/27/2023 08:23 WG2048871
Phenol ND 2.03 5 04/27/2023 08:23 WG2048871
2,4,6-Trichlorophenol ND 2.03 5 04/27/2023 08:23 WG2048871
(S) Nitrobenzene-d5 37.9 10.0-122 04/27/2023 08:23 WG2048871
(S) 2-Fluorobiphenyl 46.4 15.0-120 04/27/2023 08:23 WG2048871
(S) p-Terphenyl-d14 53.0 10.0-120 04/27/2023 08:23 WG2048871
(S) Phenol-d5 46.2 10.0-120 04/27/2023 08:23 WG2048871
(S) 2-Fluorophenol 41.2 12.0-120 04/27/2023 08:23 WG2048871
(S) 2,4,6-Tribromophenol 50.9 10.0-127 04/27/2023 08:23 WG2048871
Sample Narrative:
L1607939-06 WG2048871: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00730 1 04/27/2023 02:38 WG2048850
Acenaphthene ND 0.00730 1 04/27/2023 02:38 WG2048850
Acenaphthylene ND 0.00730 1 04/27/2023 02:38 WG2048850
Benzo(a)anthracene 0.0128 0.00730 1 04/27/2023 02:38 WG2048850
Benzo(a)pyrene 0.00968 0.00730 1 04/27/2023 02:38 WG2048850
Benzo(b)fluoranthene 0.0122 0.00730 1 04/27/2023 02:38 WG2048850
Benzo(g,h,i)perylene 0.0147 0.00730 1 04/27/2023 02:38 WG2048850
Benzo(k)fluoranthene ND 0.00730 1 04/27/2023 02:38 WG2048850
Chrysene 0.0201 0.00730 1 04/27/2023 02:38 WG2048850
Dibenz(a,h)anthracene ND 0.00730 1 04/27/2023 02:38 WG2048850
Fluoranthene 0.0198 0.00730 1 04/27/2023 02:38 WG2048850
Fluorene ND 0.00730 1 04/27/2023 02:38 WG2048850
Indeno(1,2,3-cd)pyrene ND 0.00730 1 04/27/2023 02:38 WG2048850
Naphthalene ND 0.0243 1 04/27/2023 02:38 WG2048850
Phenanthrene 0.0207 0.00730 1 04/27/2023 02:38 WG2048850
Pyrene 0.0319 0.00730 1 04/27/2023 02:38 WG2048850
1-Methylnaphthalene ND 0.0243 1 04/27/2023 02:38 WG2048850
2-Methylnaphthalene ND 0.0243 1 04/27/2023 02:38 WG2048850
2-Chloronaphthalene ND 0.0243 1 04/27/2023 02:38 WG2048850
(S) p-Terphenyl-d14 74.6 23.0-120 04/27/2023 02:38 WG2048850
(S) Nitrobenzene-d5 63.7 14.0-149 04/27/2023 02:38 WG2048850
(S) 2-Fluorobiphenyl 77.8 34.0-125 04/27/2023 02:38 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1607939
SS-1
Collected date/time: 04/20/23 09:42
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.3 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.20 1 04/28/2023 15:52 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0480 1 04/28/2023 13:05 WG2048768
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.40 1 04/28/2023 19:22 WG2050507
Arsenic 6.91 2.40 1 04/27/2023 17:33 WG2048870
Beryllium ND 0.240 1 04/27/2023 17:33 WG2048870
Cadmium ND 0.600 1 04/27/2023 17:33 WG2048870
Chromium 7.86 1.20 1 04/27/2023 17:33 WG2048870
Copper 6.44 2.40 1 04/27/2023 17:33 WG2048870
Lead 4.75 0.600 1 04/27/2023 17:33 WG2048870
Nickel 5.58 2.40 1 04/27/2023 17:33 WG2048870
Selenium ND 2.40 1 04/27/2023 17:33 WG2048870
Silver ND 1.20 1 04/27/2023 17:33 WG2048870
Thallium ND 2.40 1 04/27/2023 17:33 WG2048870
Zinc 17.8 6.00 1 04/27/2023 17:33 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.66 25 04/27/2023 14:50 WG2049437
(S) a,a,a-Trifluorotoluene(FID) 96.0 77.0-120 04/27/2023 14:50 WG2049437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0733 1 04/26/2023 01:30 WG2048704
Acrylonitrile ND 0.0183 1 04/26/2023 01:30 WG2048704
Benzene ND 0.00147 1 04/26/2023 01:30 WG2048704
Bromobenzene ND 0.0183 1 04/26/2023 01:30 WG2048704
Bromodichloromethane ND 0.00366 1 04/26/2023 01:30 WG2048704
Bromoform ND 0.0366 1 04/26/2023 01:30 WG2048704
Bromomethane ND 0.0183 1 04/26/2023 01:30 WG2048704
n-Butylbenzene ND 0.0183 1 04/26/2023 01:30 WG2048704
sec-Butylbenzene ND 0.0183 1 04/26/2023 01:30 WG2048704
tert-Butylbenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
Carbon tetrachloride ND 0.00733 1 04/26/2023 01:30 WG2048704
Chlorobenzene ND 0.00366 1 04/26/2023 01:30 WG2048704
Chlorodibromomethane ND 0.00366 1 04/26/2023 01:30 WG2048704
Chloroethane ND 0.00733 1 04/26/2023 01:30 WG2048704
Chloroform ND 0.00366 1 04/26/2023 01:30 WG2048704
Chloromethane ND 0.0183 1 04/26/2023 01:30 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1607939
SS-1
Collected date/time: 04/20/23 09:42
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00366 1 04/26/2023 01:30 WG2048704
4-Chlorotoluene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,2-Dibromo-3-Chloropropane ND 0.0366 1 04/26/2023 01:30 WG2048704
1,2-Dibromoethane ND 0.00366 1 04/26/2023 01:30 WG2048704
Dibromomethane ND 0.00733 1 04/26/2023 01:30 WG2048704
1,2-Dichlorobenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,3-Dichlorobenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,4-Dichlorobenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
Dichlorodifluoromethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,1-Dichloroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,2-Dichloroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,1-Dichloroethene ND 0.00366 1 04/26/2023 01:30 WG2048704
cis-1,2-Dichloroethene ND 0.00366 1 04/26/2023 01:30 WG2048704
trans-1,2-Dichloroethene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,2-Dichloropropane ND 0.00733 1 04/26/2023 01:30 WG2048704
1,1-Dichloropropene ND 0.00366 1 04/26/2023 01:30 WG2048704
1,3-Dichloropropane ND 0.00733 1 04/26/2023 01:30 WG2048704
cis-1,3-Dichloropropene ND 0.00366 1 04/26/2023 01:30 WG2048704
trans-1,3-Dichloropropene ND 0.00733 1 04/26/2023 01:30 WG2048704
2,2-Dichloropropane ND 0.00366 1 04/26/2023 01:30 WG2048704
Di-isopropyl ether ND 0.00147 1 04/26/2023 01:30 WG2048704
Ethylbenzene ND 0.00366 1 04/26/2023 01:30 WG2048704
Hexachloro-1,3-butadiene ND 0.0366 1 04/26/2023 01:30 WG2048704
Isopropylbenzene ND 0.00366 1 04/26/2023 01:30 WG2048704
p-Isopropyltoluene ND 0.00733 1 04/26/2023 01:30 WG2048704
2-Butanone (MEK)ND 0.147 1 04/26/2023 01:30 WG2048704
Methylene Chloride ND 0.0366 1 04/26/2023 01:30 WG2048704
4-Methyl-2-pentanone (MIBK) ND 0.0366 1 04/26/2023 01:30 WG2048704
Methyl tert-butyl ether ND 0.00147 1 04/26/2023 01:30 WG2048704
Naphthalene ND 0.0183 1 04/26/2023 01:30 WG2048704
n-Propylbenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
Styrene ND 0.0183 1 04/26/2023 01:30 WG2048704
1,1,1,2-Tetrachloroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,1,2,2-Tetrachloroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,1,2-Trichlorotrifluoroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
Tetrachloroethene ND 0.00366 1 04/26/2023 01:30 WG2048704
Toluene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,2,3-Trichlorobenzene ND 0.0183 1 04/26/2023 01:30 WG2048704
1,2,4-Trichlorobenzene ND 0.0183 1 04/26/2023 01:30 WG2048704
1,1,1-Trichloroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,1,2-Trichloroethane ND 0.00366 1 04/26/2023 01:30 WG2048704
Trichloroethene ND 0.00147 1 04/26/2023 01:30 WG2048704
Trichlorofluoromethane ND 0.00366 1 04/26/2023 01:30 WG2048704
1,2,3-Trichloropropane ND 0.0183 1 04/26/2023 01:30 WG2048704
1,2,4-Trimethylbenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,2,3-Trimethylbenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
1,3,5-Trimethylbenzene ND 0.00733 1 04/26/2023 01:30 WG2048704
Vinyl chloride ND 0.00366 1 04/26/2023 01:30 WG2048704
Xylenes, Total ND 0.00952 1 04/26/2023 01:30 WG2048704
(S) Toluene-d8 106 75.0-131 04/26/2023 01:30 WG2048704
(S) 4-Bromofluorobenzene 88.6 67.0-138 04/26/2023 01:30 WG2048704
(S) 1,2-Dichloroethane-d4 108 70.0-130 04/26/2023 01:30 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1607939
SS-1
Collected date/time: 04/20/23 09:42
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.80 1 04/26/2023 17:30 WG2048845
C28-C40 Oil Range 8.48 4.80 1 04/26/2023 17:30 WG2048845
(S) o-Terphenyl 59.0 18.0-148 04/26/2023 17:30 WG2048845
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0408 1 04/26/2023 23:41 WG2048847
PCB 1221 ND 0.0408 1 04/26/2023 23:41 WG2048847
PCB 1232 ND 0.0408 1 04/26/2023 23:41 WG2048847
PCB 1242 ND 0.0408 1 04/26/2023 23:41 WG2048847
PCB 1248 ND 0.0204 1 04/26/2023 23:41 WG2048847
PCB 1254 ND 0.0204 1 04/26/2023 23:41 WG2048847
PCB 1260 ND 0.0204 1 04/26/2023 23:41 WG2048847
(S) Decachlorobiphenyl 78.4 10.0-135 04/26/2023 23:41 WG2048847
(S) Tetrachloro-m-xylene 70.1 10.0-139 04/26/2023 23:41 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0400 1 04/27/2023 07:21 WG2048871
Acenaphthylene ND 0.0400 1 04/27/2023 07:21 WG2048871
Anthracene ND 0.0400 1 04/27/2023 07:21 WG2048871
Benzidine ND 2.01 1 04/27/2023 07:21 WG2048871
Benzo(a)anthracene ND 0.0400 1 04/27/2023 07:21 WG2048871
Benzo(b)fluoranthene ND 0.0400 1 04/27/2023 07:21 WG2048871
Benzo(k)fluoranthene ND 0.0400 1 04/27/2023 07:21 WG2048871
Benzo(g,h,i)perylene ND 0.0400 1 04/27/2023 07:21 WG2048871
Benzo(a)pyrene ND 0.0400 1 04/27/2023 07:21 WG2048871
Bis(2-chlorethoxy)methane ND 0.400 1 04/27/2023 07:21 WG2048871
Bis(2-chloroethyl)ether ND 0.400 1 04/27/2023 07:21 WG2048871
2,2-Oxybis(1-Chloropropane) ND 0.400 1 04/27/2023 07:21 WG2048871
4-Bromophenyl-phenylether ND 0.400 1 04/27/2023 07:21 WG2048871
2-Chloronaphthalene ND 0.0400 1 04/27/2023 07:21 WG2048871
4-Chlorophenyl-phenylether ND 0.400 1 04/27/2023 07:21 WG2048871
Chrysene ND 0.0400 1 04/27/2023 07:21 WG2048871
Dibenz(a,h)anthracene ND 0.0400 1 04/27/2023 07:21 WG2048871
3,3-Dichlorobenzidine ND 0.400 1 04/27/2023 07:21 WG2048871
2,4-Dinitrotoluene ND 0.400 1 04/27/2023 07:21 WG2048871
2,6-Dinitrotoluene ND 0.400 1 04/27/2023 07:21 WG2048871
Fluoranthene ND 0.0400 1 04/27/2023 07:21 WG2048871
Fluorene ND 0.0400 1 04/27/2023 07:21 WG2048871
Hexachlorobenzene ND 0.400 1 04/27/2023 07:21 WG2048871
Hexachloro-1,3-butadiene ND 0.400 1 04/27/2023 07:21 WG2048871
Hexachlorocyclopentadiene ND 0.400 1 04/27/2023 07:21 WG2048871
Hexachloroethane ND 0.400 1 04/27/2023 07:21 WG2048871
Indeno(1,2,3-cd)pyrene ND 0.0400 1 04/27/2023 07:21 WG2048871
Isophorone ND 0.400 1 04/27/2023 07:21 WG2048871
Naphthalene ND 0.0400 1 04/27/2023 07:21 WG2048871
Nitrobenzene ND 0.400 1 04/27/2023 07:21 WG2048871
n-Nitrosodimethylamine ND 0.400 1 04/27/2023 07:21 WG2048871
n-Nitrosodiphenylamine ND 0.400 1 04/27/2023 07:21 WG2048871
n-Nitrosodi-n-propylamine ND 0.400 1 04/27/2023 07:21 WG2048871
Phenanthrene ND 0.0400 1 04/27/2023 07:21 WG2048871
Benzylbutyl phthalate ND 0.400 1 04/27/2023 07:21 WG2048871
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1607939
SS-1
Collected date/time: 04/20/23 09:42
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.400 1 04/27/2023 07:21 WG2048871
Di-n-butyl phthalate ND 0.400 1 04/27/2023 07:21 WG2048871
Diethyl phthalate ND 0.400 1 04/27/2023 07:21 WG2048871
Dimethyl phthalate ND 0.400 1 04/27/2023 07:21 WG2048871
Di-n-octyl phthalate ND 0.400 1 04/27/2023 07:21 WG2048871
Pyrene ND 0.0400 1 04/27/2023 07:21 WG2048871
1,2,4-Trichlorobenzene ND 0.400 1 04/27/2023 07:21 WG2048871
4-Chloro-3-methylphenol ND 0.400 1 04/27/2023 07:21 WG2048871
2-Chlorophenol ND 0.400 1 04/27/2023 07:21 WG2048871
2,4-Dichlorophenol ND 0.400 1 04/27/2023 07:21 WG2048871
2,4-Dimethylphenol ND 0.400 1 04/27/2023 07:21 WG2048871
4,6-Dinitro-2-methylphenol ND 0.400 1 04/27/2023 07:21 WG2048871
2,4-Dinitrophenol ND 0.400 1 04/27/2023 07:21 WG2048871
2-Nitrophenol ND 0.400 1 04/27/2023 07:21 WG2048871
4-Nitrophenol ND 0.400 1 04/27/2023 07:21 WG2048871
Pentachlorophenol ND 0.400 1 04/27/2023 07:21 WG2048871
Phenol ND 0.400 1 04/27/2023 07:21 WG2048871
2,4,6-Trichlorophenol ND 0.400 1 04/27/2023 07:21 WG2048871
(S) Nitrobenzene-d5 43.4 10.0-122 04/27/2023 07:21 WG2048871
(S) 2-Fluorobiphenyl 52.7 15.0-120 04/27/2023 07:21 WG2048871
(S) p-Terphenyl-d14 59.6 10.0-120 04/27/2023 07:21 WG2048871
(S) Phenol-d5 48.8 10.0-120 04/27/2023 07:21 WG2048871
(S) 2-Fluorophenol 54.1 12.0-120 04/27/2023 07:21 WG2048871
(S) 2,4,6-Tribromophenol 61.4 10.0-127 04/27/2023 07:21 WG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00720 1 04/26/2023 20:05 WG2048850
Acenaphthene ND 0.00720 1 04/26/2023 20:05 WG2048850
Acenaphthylene ND 0.00720 1 04/26/2023 20:05 WG2048850
Benzo(a)anthracene ND 0.00720 1 04/26/2023 20:05 WG2048850
Benzo(a)pyrene ND 0.00720 1 04/26/2023 20:05 WG2048850
Benzo(b)fluoranthene ND 0.00720 1 04/26/2023 20:05 WG2048850
Benzo(g,h,i)perylene ND 0.00720 1 04/26/2023 20:05 WG2048850
Benzo(k)fluoranthene ND 0.00720 1 04/26/2023 20:05 WG2048850
Chrysene ND 0.00720 1 04/26/2023 20:05 WG2048850
Dibenz(a,h)anthracene ND 0.00720 1 04/26/2023 20:05 WG2048850
Fluoranthene ND 0.00720 1 04/26/2023 20:05 WG2048850
Fluorene ND 0.00720 1 04/26/2023 20:05 WG2048850
Indeno(1,2,3-cd)pyrene ND 0.00720 1 04/26/2023 20:05 WG2048850
Naphthalene ND 0.0240 1 04/26/2023 20:05 WG2048850
Phenanthrene ND 0.00720 1 04/26/2023 20:05 WG2048850
Pyrene ND 0.00720 1 04/26/2023 20:05 WG2048850
1-Methylnaphthalene ND 0.0240 1 04/26/2023 20:05 WG2048850
2-Methylnaphthalene ND 0.0240 1 04/26/2023 20:05 WG2048850
2-Chloronaphthalene ND 0.0240 1 04/26/2023 20:05 WG2048850
(S) p-Terphenyl-d14 60.8 23.0-120 04/26/2023 20:05 WG2048850
(S) Nitrobenzene-d5 49.1 14.0-149 04/26/2023 20:05 WG2048850
(S) 2-Fluorobiphenyl 67.8 34.0-125 04/26/2023 20:05 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1607939
SS-2
Collected date/time: 04/20/23 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 61.7 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.62 1 04/28/2023 15:57 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0648 1 04/28/2023 13:07 WG2048768
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 3.24 1 04/28/2023 19:25 WG2050507
Arsenic 12.4 3.24 1 04/27/2023 17:36 WG2048870
Beryllium 1.02 0.324 1 04/27/2023 17:36 WG2048870
Cadmium ND 0.810 1 04/27/2023 17:36 WG2048870
Chromium 21.2 1.62 1 04/27/2023 17:36 WG2048870
Copper 11.9 3.24 1 04/27/2023 17:36 WG2048870
Lead 11.4 0.810 1 04/27/2023 17:36 WG2048870
Nickel 11.6 3.24 1 04/27/2023 17:36 WG2048870
Selenium ND 3.24 1 04/27/2023 17:36 WG2048870
Silver ND 1.62 1 04/27/2023 17:36 WG2048870
Thallium ND 3.24 1 04/27/2023 17:36 WG2048870
Zinc 38.8 8.10 1 04/27/2023 17:36 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 5.77 26 04/27/2023 15:11 WG2049437
(S) a,a,a-Trifluorotoluene(FID) 95.6 77.0-120 04/27/2023 15:11 WG2049437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.115 1.04 04/26/2023 01:49 WG2048704
Acrylonitrile ND 0.0288 1.04 04/26/2023 01:49 WG2048704
Benzene ND 0.00231 1.04 04/26/2023 01:49 WG2048704
Bromobenzene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
Bromodichloromethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Bromoform ND 0.0577 1.04 04/26/2023 01:49 WG2048704
Bromomethane ND 0.0288 1.04 04/26/2023 01:49 WG2048704
n-Butylbenzene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
sec-Butylbenzene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
tert-Butylbenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
Carbon tetrachloride ND 0.0115 1.04 04/26/2023 01:49 WG2048704
Chlorobenzene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Chlorodibromomethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Chloroethane ND 0.0115 1.04 04/26/2023 01:49 WG2048704
Chloroform ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Chloromethane ND 0.0288 1.04 04/26/2023 01:49 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1607939
SS-2
Collected date/time: 04/20/23 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
4-Chlorotoluene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,2-Dibromo-3-Chloropropane ND 0.0577 1.04 04/26/2023 01:49 WG2048704
1,2-Dibromoethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Dibromomethane ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,2-Dichlorobenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,3-Dichlorobenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,4-Dichlorobenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
Dichlorodifluoromethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,1-Dichloroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,2-Dichloroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,1-Dichloroethene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
cis-1,2-Dichloroethene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
trans-1,2-Dichloroethene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,2-Dichloropropane ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,1-Dichloropropene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,3-Dichloropropane ND 0.0115 1.04 04/26/2023 01:49 WG2048704
cis-1,3-Dichloropropene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
trans-1,3-Dichloropropene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
2,2-Dichloropropane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Di-isopropyl ether ND 0.00231 1.04 04/26/2023 01:49 WG2048704
Ethylbenzene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Hexachloro-1,3-butadiene ND 0.0577 1.04 04/26/2023 01:49 WG2048704
Isopropylbenzene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
p-Isopropyltoluene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
2-Butanone (MEK)ND 0.231 1.04 04/26/2023 01:49 WG2048704
Methylene Chloride ND 0.0577 1.04 04/26/2023 01:49 WG2048704
4-Methyl-2-pentanone (MIBK) ND 0.0577 1.04 04/26/2023 01:49 WG2048704
Methyl tert-butyl ether ND 0.00231 1.04 04/26/2023 01:49 WG2048704
Naphthalene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
n-Propylbenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
Styrene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
1,1,1,2-Tetrachloroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,1,2,2-Tetrachloroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,1,2-Trichlorotrifluoroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Tetrachloroethene ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Toluene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,2,3-Trichlorobenzene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
1,2,4-Trichlorobenzene ND 0.0288 1.04 04/26/2023 01:49 WG2048704
1,1,1-Trichloroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,1,2-Trichloroethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Trichloroethene ND 0.00231 1.04 04/26/2023 01:49 WG2048704
Trichlorofluoromethane ND 0.00577 1.04 04/26/2023 01:49 WG2048704
1,2,3-Trichloropropane ND 0.0288 1.04 04/26/2023 01:49 WG2048704
1,2,4-Trimethylbenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,2,3-Trimethylbenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
1,3,5-Trimethylbenzene ND 0.0115 1.04 04/26/2023 01:49 WG2048704
Vinyl chloride ND 0.00577 1.04 04/26/2023 01:49 WG2048704
Xylenes, Total ND 0.0150 1.04 04/26/2023 01:49 WG2048704
(S) Toluene-d8 104 75.0-131 04/26/2023 01:49 WG2048704
(S) 4-Bromofluorobenzene 86.9 67.0-138 04/26/2023 01:49 WG2048704
(S) 1,2-Dichloroethane-d4 108 70.0-130 04/26/2023 01:49 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1607939
SS-2
Collected date/time: 04/20/23 10:00
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 6.48 1 04/26/2023 17:43 WG2048845
C28-C40 Oil Range 19.3 6.48 1 04/26/2023 17:43 WG2048845
(S) o-Terphenyl 42.4 18.0-148 04/26/2023 17:43 WG2048845
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0551 1 04/26/2023 23:51 WG2048847
PCB 1221 ND 0.0551 1 04/26/2023 23:51 WG2048847
PCB 1232 ND 0.0551 1 04/26/2023 23:51 WG2048847
PCB 1242 ND 0.0551 1 04/26/2023 23:51 WG2048847
PCB 1248 ND 0.0275 1 04/26/2023 23:51 WG2048847
PCB 1254 ND 0.0275 1 04/26/2023 23:51 WG2048847
PCB 1260 ND 0.0275 1 04/26/2023 23:51 WG2048847
(S) Decachlorobiphenyl 86.4 10.0-135 04/26/2023 23:51 WG2048847
(S) Tetrachloro-m-xylene 75.3 10.0-139 04/26/2023 23:51 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0540 1 04/27/2023 07:00 WG2048871
Acenaphthylene ND 0.0540 1 04/27/2023 07:00 WG2048871
Anthracene ND 0.0540 1 04/27/2023 07:00 WG2048871
Benzidine ND 2.71 1 04/27/2023 07:00 WG2048871
Benzo(a)anthracene ND 0.0540 1 04/27/2023 07:00 WG2048871
Benzo(b)fluoranthene ND 0.0540 1 04/27/2023 07:00 WG2048871
Benzo(k)fluoranthene ND 0.0540 1 04/27/2023 07:00 WG2048871
Benzo(g,h,i)perylene ND 0.0540 1 04/27/2023 07:00 WG2048871
Benzo(a)pyrene ND 0.0540 1 04/27/2023 07:00 WG2048871
Bis(2-chlorethoxy)methane ND 0.540 1 04/27/2023 07:00 WG2048871
Bis(2-chloroethyl)ether ND 0.540 1 04/27/2023 07:00 WG2048871
2,2-Oxybis(1-Chloropropane) ND 0.540 1 04/27/2023 07:00 WG2048871
4-Bromophenyl-phenylether ND 0.540 1 04/27/2023 07:00 WG2048871
2-Chloronaphthalene ND 0.0540 1 04/27/2023 07:00 WG2048871
4-Chlorophenyl-phenylether ND 0.540 1 04/27/2023 07:00 WG2048871
Chrysene ND 0.0540 1 04/27/2023 07:00 WG2048871
Dibenz(a,h)anthracene ND 0.0540 1 04/27/2023 07:00 WG2048871
3,3-Dichlorobenzidine ND 0.540 1 04/27/2023 07:00 WG2048871
2,4-Dinitrotoluene ND 0.540 1 04/27/2023 07:00 WG2048871
2,6-Dinitrotoluene ND 0.540 1 04/27/2023 07:00 WG2048871
Fluoranthene ND 0.0540 1 04/27/2023 07:00 WG2048871
Fluorene ND 0.0540 1 04/27/2023 07:00 WG2048871
Hexachlorobenzene ND 0.540 1 04/27/2023 07:00 WG2048871
Hexachloro-1,3-butadiene ND 0.540 1 04/27/2023 07:00 WG2048871
Hexachlorocyclopentadiene ND 0.540 1 04/27/2023 07:00 WG2048871
Hexachloroethane ND 0.540 1 04/27/2023 07:00 WG2048871
Indeno(1,2,3-cd)pyrene ND 0.0540 1 04/27/2023 07:00 WG2048871
Isophorone ND 0.540 1 04/27/2023 07:00 WG2048871
Naphthalene ND 0.0540 1 04/27/2023 07:00 WG2048871
Nitrobenzene ND 0.540 1 04/27/2023 07:00 WG2048871
n-Nitrosodimethylamine ND 0.540 1 04/27/2023 07:00 WG2048871
n-Nitrosodiphenylamine ND 0.540 1 04/27/2023 07:00 WG2048871
n-Nitrosodi-n-propylamine ND 0.540 1 04/27/2023 07:00 WG2048871
Phenanthrene ND 0.0540 1 04/27/2023 07:00 WG2048871
Benzylbutyl phthalate ND 0.540 1 04/27/2023 07:00 WG2048871
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1607939
SS-2
Collected date/time: 04/20/23 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.540 1 04/27/2023 07:00 WG2048871
Di-n-butyl phthalate ND 0.540 1 04/27/2023 07:00 WG2048871
Diethyl phthalate ND 0.540 1 04/27/2023 07:00 WG2048871
Dimethyl phthalate ND 0.540 1 04/27/2023 07:00 WG2048871
Di-n-octyl phthalate ND 0.540 1 04/27/2023 07:00 WG2048871
Pyrene ND 0.0540 1 04/27/2023 07:00 WG2048871
1,2,4-Trichlorobenzene ND 0.540 1 04/27/2023 07:00 WG2048871
4-Chloro-3-methylphenol ND 0.540 1 04/27/2023 07:00 WG2048871
2-Chlorophenol ND 0.540 1 04/27/2023 07:00 WG2048871
2,4-Dichlorophenol ND 0.540 1 04/27/2023 07:00 WG2048871
2,4-Dimethylphenol ND 0.540 1 04/27/2023 07:00 WG2048871
4,6-Dinitro-2-methylphenol ND 0.540 1 04/27/2023 07:00 WG2048871
2,4-Dinitrophenol ND 0.540 1 04/27/2023 07:00 WG2048871
2-Nitrophenol ND 0.540 1 04/27/2023 07:00 WG2048871
4-Nitrophenol ND 0.540 1 04/27/2023 07:00 WG2048871
Pentachlorophenol ND 0.540 1 04/27/2023 07:00 WG2048871
Phenol ND 0.540 1 04/27/2023 07:00 WG2048871
2,4,6-Trichlorophenol ND 0.540 1 04/27/2023 07:00 WG2048871
(S) Nitrobenzene-d5 43.2 10.0-122 04/27/2023 07:00 WG2048871
(S) 2-Fluorobiphenyl 51.7 15.0-120 04/27/2023 07:00 WG2048871
(S) p-Terphenyl-d14 58.3 10.0-120 04/27/2023 07:00 WG2048871
(S) Phenol-d5 41.8 10.0-120 04/27/2023 07:00 WG2048871
(S) 2-Fluorophenol 54.4 12.0-120 04/27/2023 07:00 WG2048871
(S) 2,4,6-Tribromophenol 58.8 10.0-127 04/27/2023 07:00 WG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00972 1 04/26/2023 20:25 WG2048850
Acenaphthene ND 0.00972 1 04/26/2023 20:25 WG2048850
Acenaphthylene ND 0.00972 1 04/26/2023 20:25 WG2048850
Benzo(a)anthracene ND 0.00972 1 04/26/2023 20:25 WG2048850
Benzo(a)pyrene ND 0.00972 1 04/26/2023 20:25 WG2048850
Benzo(b)fluoranthene ND 0.00972 1 04/26/2023 20:25 WG2048850
Benzo(g,h,i)perylene ND 0.00972 1 04/26/2023 20:25 WG2048850
Benzo(k)fluoranthene ND 0.00972 1 04/26/2023 20:25 WG2048850
Chrysene ND 0.00972 1 04/26/2023 20:25 WG2048850
Dibenz(a,h)anthracene ND 0.00972 1 04/26/2023 20:25 WG2048850
Fluoranthene 0.0133 0.00972 1 04/26/2023 20:25 WG2048850
Fluorene ND 0.00972 1 04/26/2023 20:25 WG2048850
Indeno(1,2,3-cd)pyrene ND 0.00972 1 04/26/2023 20:25 WG2048850
Naphthalene ND 0.0324 1 04/26/2023 20:25 WG2048850
Phenanthrene 0.0102 0.00972 1 04/26/2023 20:25 WG2048850
Pyrene 0.0137 0.00972 1 04/26/2023 20:25 WG2048850
1-Methylnaphthalene ND 0.0324 1 04/26/2023 20:25 WG2048850
2-Methylnaphthalene ND 0.0324 1 04/26/2023 20:25 WG2048850
2-Chloronaphthalene ND 0.0324 1 04/26/2023 20:25 WG2048850
(S) p-Terphenyl-d14 63.0 23.0-120 04/26/2023 20:25 WG2048850
(S) Nitrobenzene-d5 54.0 14.0-149 04/26/2023 20:25 WG2048850
(S) 2-Fluorobiphenyl 70.9 34.0-125 04/26/2023 20:25 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1607939
SS-3
Collected date/time: 04/20/23 09:06
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.3 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.19 1 04/28/2023 16:13 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0474 1 04/28/2023 13:10 WG2048768
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.37 1 04/28/2023 19:28 WG2050507
Arsenic 10.2 2.37 1 04/27/2023 17:39 WG2048870
Beryllium 0.368 0.237 1 04/27/2023 17:39 WG2048870
Cadmium ND 0.593 1 04/27/2023 17:39 WG2048870
Chromium 18.0 1.19 1 04/27/2023 17:39 WG2048870
Copper 32.6 2.37 1 04/27/2023 17:39 WG2048870
Lead 22.7 0.593 1 04/27/2023 17:39 WG2048870
Nickel 12.4 2.37 1 04/27/2023 17:39 WG2048870
Selenium ND 2.37 1 04/27/2023 17:39 WG2048870
Silver ND 1.19 1 04/27/2023 17:39 WG2048870
Thallium ND 2.37 1 04/27/2023 17:39 WG2048870
Zinc 56.4 5.93 1 04/27/2023 17:39 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 5.40 B 3.47 25 04/27/2023 15:31 WG2049437
(S) a,a,a-Trifluorotoluene(FID) 98.3 77.0-120 04/27/2023 15:31 WG2049437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0694 1 04/26/2023 02:08 WG2048704
Acrylonitrile ND 0.0174 1 04/26/2023 02:08 WG2048704
Benzene ND 0.00139 1 04/26/2023 02:08 WG2048704
Bromobenzene ND 0.0174 1 04/26/2023 02:08 WG2048704
Bromodichloromethane ND 0.00347 1 04/26/2023 02:08 WG2048704
Bromoform ND 0.0347 1 04/26/2023 02:08 WG2048704
Bromomethane ND 0.0174 1 04/26/2023 02:08 WG2048704
n-Butylbenzene ND 0.0174 1 04/26/2023 02:08 WG2048704
sec-Butylbenzene ND 0.0174 1 04/26/2023 02:08 WG2048704
tert-Butylbenzene ND 0.00694 1 04/26/2023 02:08 WG2048704
Carbon tetrachloride ND 0.00694 1 04/26/2023 02:08 WG2048704
Chlorobenzene ND 0.00347 1 04/26/2023 02:08 WG2048704
Chlorodibromomethane ND 0.00347 1 04/26/2023 02:08 WG2048704
Chloroethane ND 0.00694 1 04/26/2023 02:08 WG2048704
Chloroform ND 0.00347 1 04/26/2023 02:08 WG2048704
Chloromethane ND 0.0174 1 04/26/2023 02:08 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1607939
SS-3
Collected date/time: 04/20/23 09:06
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00347 1 04/26/2023 02:08 WG2048704
4-Chlorotoluene ND 0.00694 1 04/26/2023 02:08 WG2048704
1,2-Dibromo-3-Chloropropane ND 0.0347 1 04/26/2023 02:08 WG2048704
1,2-Dibromoethane ND 0.00347 1 04/26/2023 02:08 WG2048704
Dibromomethane ND 0.00694 1 04/26/2023 02:08 WG2048704
1,2-Dichlorobenzene ND 0.00694 1 04/26/2023 02:08 WG2048704
1,3-Dichlorobenzene ND 0.00694 1 04/26/2023 02:08 WG2048704
1,4-Dichlorobenzene ND 0.00694 1 04/26/2023 02:08 WG2048704
Dichlorodifluoromethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,1-Dichloroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,2-Dichloroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,1-Dichloroethene ND 0.00347 1 04/26/2023 02:08 WG2048704
cis-1,2-Dichloroethene ND 0.00347 1 04/26/2023 02:08 WG2048704
trans-1,2-Dichloroethene ND 0.00694 1 04/26/2023 02:08 WG2048704
1,2-Dichloropropane ND 0.00694 1 04/26/2023 02:08 WG2048704
1,1-Dichloropropene ND 0.00347 1 04/26/2023 02:08 WG2048704
1,3-Dichloropropane ND 0.00694 1 04/26/2023 02:08 WG2048704
cis-1,3-Dichloropropene ND 0.00347 1 04/26/2023 02:08 WG2048704
trans-1,3-Dichloropropene ND 0.00694 1 04/26/2023 02:08 WG2048704
2,2-Dichloropropane ND 0.00347 1 04/26/2023 02:08 WG2048704
Di-isopropyl ether ND 0.00139 1 04/26/2023 02:08 WG2048704
Ethylbenzene ND 0.00347 1 04/26/2023 02:08 WG2048704
Hexachloro-1,3-butadiene ND 0.0347 1 04/26/2023 02:08 WG2048704
Isopropylbenzene 0.00597 0.00347 1 04/26/2023 02:08 WG2048704
p-Isopropyltoluene 0.450 0.00694 1 04/26/2023 02:08 WG2048704
2-Butanone (MEK)ND 0.139 1 04/26/2023 02:08 WG2048704
Methylene Chloride ND 0.0347 1 04/26/2023 02:08 WG2048704
4-Methyl-2-pentanone (MIBK) ND 0.0347 1 04/26/2023 02:08 WG2048704
Methyl tert-butyl ether ND 0.00139 1 04/26/2023 02:08 WG2048704
Naphthalene ND 0.0174 1 04/26/2023 02:08 WG2048704
n-Propylbenzene 0.0325 0.00694 1 04/26/2023 02:08 WG2048704
Styrene ND 0.0174 1 04/26/2023 02:08 WG2048704
1,1,1,2-Tetrachloroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,1,2,2-Tetrachloroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,1,2-Trichlorotrifluoroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
Tetrachloroethene ND 0.00347 1 04/26/2023 02:08 WG2048704
Toluene 0.133 0.00694 1 04/26/2023 02:08 WG2048704
1,2,3-Trichlorobenzene ND 0.0174 1 04/26/2023 02:08 WG2048704
1,2,4-Trichlorobenzene ND 0.0174 1 04/26/2023 02:08 WG2048704
1,1,1-Trichloroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,1,2-Trichloroethane ND 0.00347 1 04/26/2023 02:08 WG2048704
Trichloroethene ND 0.00139 1 04/26/2023 02:08 WG2048704
Trichlorofluoromethane ND 0.00347 1 04/26/2023 02:08 WG2048704
1,2,3-Trichloropropane ND 0.0174 1 04/26/2023 02:08 WG2048704
1,2,4-Trimethylbenzene 0.149 0.00694 1 04/26/2023 02:08 WG2048704
1,2,3-Trimethylbenzene 0.0240 0.00694 1 04/26/2023 02:08 WG2048704
1,3,5-Trimethylbenzene 0.0527 0.00694 1 04/26/2023 02:08 WG2048704
Vinyl chloride ND 0.00347 1 04/26/2023 02:08 WG2048704
Xylenes, Total 0.0182 0.00902 1 04/26/2023 02:08 WG2048704
(S) Toluene-d8 109 75.0-131 04/26/2023 02:08 WG2048704
(S) 4-Bromofluorobenzene 83.8 67.0-138 04/26/2023 02:08 WG2048704
(S) 1,2-Dichloroethane-d4 107 70.0-130 04/26/2023 02:08 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1607939
SS-3
Collected date/time: 04/20/23 09:06
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 255 47.4 10 04/27/2023 08:42 WG2048845
C28-C40 Oil Range 198 47.4 10 04/27/2023 08:42 WG2048845
(S) o-Terphenyl 98.9 18.0-148 04/27/2023 08:42 WG2048845
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0806 2 04/27/2023 16:53 WG2050080
PCB 1221 ND 0.0806 2 04/27/2023 16:53 WG2050080
PCB 1232 ND 0.0806 2 04/27/2023 16:53 WG2050080
PCB 1242 ND 0.0806 2 04/27/2023 16:53 WG2050080
PCB 1248 ND 0.0403 2 04/27/2023 16:53 WG2050080
PCB 1254 ND 0.0403 2 04/27/2023 16:53 WG2050080
PCB 1260 ND 0.0403 2 04/27/2023 16:53 WG2050080
(S) Decachlorobiphenyl 70.0 10.0-135 04/27/2023 16:53 WG2050080
(S) Tetrachloro-m-xylene 72.8 10.0-139 04/27/2023 16:53 WG2050080
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.395 10 04/27/2023 08:44 WG2048871
Acenaphthylene ND 0.395 10 04/27/2023 08:44 WG2048871
Anthracene ND 0.395 10 04/27/2023 08:44 WG2048871
Benzidine ND 19.8 10 04/27/2023 08:44 WG2048871
Benzo(a)anthracene ND 0.395 10 04/27/2023 08:44 WG2048871
Benzo(b)fluoranthene ND 0.395 10 04/27/2023 08:44 WG2048871
Benzo(k)fluoranthene ND 0.395 10 04/27/2023 08:44 WG2048871
Benzo(g,h,i)perylene ND 0.395 10 04/27/2023 08:44 WG2048871
Benzo(a)pyrene ND 0.395 10 04/27/2023 08:44 WG2048871
Bis(2-chlorethoxy)methane ND 3.95 10 04/27/2023 08:44 WG2048871
Bis(2-chloroethyl)ether ND 3.95 10 04/27/2023 08:44 WG2048871
2,2-Oxybis(1-Chloropropane) ND 3.95 10 04/27/2023 08:44 WG2048871
4-Bromophenyl-phenylether ND 3.95 10 04/27/2023 08:44 WG2048871
2-Chloronaphthalene ND 0.395 10 04/27/2023 08:44 WG2048871
4-Chlorophenyl-phenylether ND 3.95 10 04/27/2023 08:44 WG2048871
Chrysene ND 0.395 10 04/27/2023 08:44 WG2048871
Dibenz(a,h)anthracene ND 0.395 10 04/27/2023 08:44 WG2048871
3,3-Dichlorobenzidine ND 3.95 10 04/27/2023 08:44 WG2048871
2,4-Dinitrotoluene ND 3.95 10 04/27/2023 08:44 WG2048871
2,6-Dinitrotoluene ND 3.95 10 04/27/2023 08:44 WG2048871
Fluoranthene ND 0.395 10 04/27/2023 08:44 WG2048871
Fluorene ND 0.395 10 04/27/2023 08:44 WG2048871
Hexachlorobenzene ND 3.95 10 04/27/2023 08:44 WG2048871
Hexachloro-1,3-butadiene ND 3.95 10 04/27/2023 08:44 WG2048871
Hexachlorocyclopentadiene ND 3.95 10 04/27/2023 08:44 WG2048871
Hexachloroethane ND 3.95 10 04/27/2023 08:44 WG2048871
Indeno(1,2,3-cd)pyrene ND 0.395 10 04/27/2023 08:44 WG2048871
Isophorone ND 3.95 10 04/27/2023 08:44 WG2048871
Naphthalene ND 0.395 10 04/27/2023 08:44 WG2048871
Nitrobenzene ND 3.95 10 04/27/2023 08:44 WG2048871
n-Nitrosodimethylamine ND 3.95 10 04/27/2023 08:44 WG2048871
n-Nitrosodiphenylamine ND 3.95 10 04/27/2023 08:44 WG2048871
n-Nitrosodi-n-propylamine ND 3.95 10 04/27/2023 08:44 WG2048871
Phenanthrene ND 0.395 10 04/27/2023 08:44 WG2048871
Benzylbutyl phthalate ND 3.95 10 04/27/2023 08:44 WG2048871
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1607939
SS-3
Collected date/time: 04/20/23 09:06
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 3.95 10 04/27/2023 08:44 WG2048871
Di-n-butyl phthalate ND 3.95 10 04/27/2023 08:44 WG2048871
Diethyl phthalate ND 3.95 10 04/27/2023 08:44 WG2048871
Dimethyl phthalate ND 3.95 10 04/27/2023 08:44 WG2048871
Di-n-octyl phthalate ND 3.95 10 04/27/2023 08:44 WG2048871
Pyrene ND 0.395 10 04/27/2023 08:44 WG2048871
1,2,4-Trichlorobenzene ND 3.95 10 04/27/2023 08:44 WG2048871
4-Chloro-3-methylphenol ND 3.95 10 04/27/2023 08:44 WG2048871
2-Chlorophenol ND 3.95 10 04/27/2023 08:44 WG2048871
2,4-Dichlorophenol ND 3.95 10 04/27/2023 08:44 WG2048871
2,4-Dimethylphenol ND 3.95 10 04/27/2023 08:44 WG2048871
4,6-Dinitro-2-methylphenol ND 3.95 10 04/27/2023 08:44 WG2048871
2,4-Dinitrophenol ND 3.95 10 04/27/2023 08:44 WG2048871
2-Nitrophenol ND 3.95 10 04/27/2023 08:44 WG2048871
4-Nitrophenol ND 3.95 10 04/27/2023 08:44 WG2048871
Pentachlorophenol ND 3.95 10 04/27/2023 08:44 WG2048871
Phenol ND 3.95 10 04/27/2023 08:44 WG2048871
2,4,6-Trichlorophenol ND 3.95 10 04/27/2023 08:44 WG2048871
(S) Nitrobenzene-d5 44.7 10.0-122 04/27/2023 08:44 WG2048871
(S) 2-Fluorobiphenyl 56.0 15.0-120 04/27/2023 08:44 WG2048871
(S) p-Terphenyl-d14 63.5 10.0-120 04/27/2023 08:44 WG2048871
(S) Phenol-d5 48.1 10.0-120 04/27/2023 08:44 WG2048871
(S) 2-Fluorophenol 56.8 12.0-120 04/27/2023 08:44 WG2048871
(S) 2,4,6-Tribromophenol 59.1 10.0-127 04/27/2023 08:44 WG2048871
Sample Narrative:
L1607939-09 WG2048871: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 2.10 0.00712 1 04/27/2023 01:19 WG2048850
Acenaphthene 1.99 0.00712 1 04/27/2023 01:19 WG2048850
Acenaphthylene ND 0.00712 1 04/27/2023 01:19 WG2048850
Benzo(a)anthracene 2.70 0.00712 1 04/27/2023 01:19 WG2048850
Benzo(a)pyrene 1.84 0.00712 1 04/27/2023 01:19 WG2048850
Benzo(b)fluoranthene 1.77 0.00712 1 04/27/2023 01:19 WG2048850
Benzo(g,h,i)perylene 0.763 0.00712 1 04/27/2023 01:19 WG2048850
Benzo(k)fluoranthene 0.685 0.00712 1 04/27/2023 01:19 WG2048850
Chrysene 3.01 0.00712 1 04/27/2023 01:19 WG2048850
Dibenz(a,h)anthracene 0.253 0.00712 1 04/27/2023 01:19 WG2048850
Fluoranthene 6.56 0.0712 10 04/28/2023 16:46 WG2048850
Fluorene 1.11 0.00712 1 04/27/2023 01:19 WG2048850
Indeno(1,2,3-cd)pyrene 1.01 0.00712 1 04/27/2023 01:19 WG2048850
Naphthalene 0.500 0.0237 1 04/27/2023 01:19 WG2048850
Phenanthrene 8.19 0.0712 10 04/28/2023 16:46 WG2048850
Pyrene 6.43 0.0712 10 04/28/2023 16:46 WG2048850
1-Methylnaphthalene 0.356 0.0237 1 04/27/2023 01:19 WG2048850
2-Methylnaphthalene 0.378 0.0237 1 04/27/2023 01:19 WG2048850
2-Chloronaphthalene ND 0.0237 1 04/27/2023 01:19 WG2048850
(S) p-Terphenyl-d14 72.8 23.0-120 04/27/2023 01:19 WG2048850
(S) p-Terphenyl-d14 84.2 23.0-120 04/28/2023 16:46 WG2048850
(S) Nitrobenzene-d5 65.1 14.0-149 04/27/2023 01:19 WG2048850
(S) Nitrobenzene-d5 114 14.0-149 04/28/2023 16:46 WG2048850
(S) 2-Fluorobiphenyl 72.1 34.0-125 04/27/2023 01:19 WG2048850
(S) 2-Fluorobiphenyl 86.5 34.0-125 04/28/2023 16:46 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 10
L1607939
SS-4
Collected date/time: 04/20/23 09:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.8 1 04/26/2023 10:37 WG2048861
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.30 1 04/28/2023 16:18 WG2048733
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0521 1 04/28/2023 16:47 WG2048765
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.60 1 04/28/2023 19:31 WG2050507
Arsenic 7.37 2.60 1 04/27/2023 17:41 WG2048870
Beryllium 0.390 0.260 1 04/27/2023 17:41 WG2048870
Cadmium ND 0.651 1 04/27/2023 17:41 WG2048870
Chromium 19.9 1.30 1 04/27/2023 17:41 WG2048870
Copper 28.8 2.60 1 04/27/2023 17:41 WG2048870
Lead 20.7 0.651 1 04/27/2023 17:41 WG2048870
Nickel 11.9 2.60 1 04/27/2023 17:41 WG2048870
Selenium ND 2.60 1 04/27/2023 17:41 WG2048870
Silver ND 1.30 1 04/27/2023 17:41 WG2048870
Thallium ND 2.60 1 04/27/2023 17:41 WG2048870
Zinc 57.9 6.51 1 04/27/2023 17:41 WG2048870
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.11 25 04/27/2023 16:42 WG2049437
(S) a,a,a-Trifluorotoluene(FID) 97.6 77.0-120 04/27/2023 16:42 WG2049437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0821 1 04/26/2023 02:28 WG2048704
Acrylonitrile ND 0.0205 1 04/26/2023 02:28 WG2048704
Benzene ND 0.00164 1 04/26/2023 02:28 WG2048704
Bromobenzene ND 0.0205 1 04/26/2023 02:28 WG2048704
Bromodichloromethane ND 0.00411 1 04/26/2023 02:28 WG2048704
Bromoform ND 0.0411 1 04/26/2023 02:28 WG2048704
Bromomethane ND 0.0205 1 04/26/2023 02:28 WG2048704
n-Butylbenzene ND 0.0205 1 04/26/2023 02:28 WG2048704
sec-Butylbenzene ND 0.0205 1 04/26/2023 02:28 WG2048704
tert-Butylbenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
Carbon tetrachloride ND 0.00821 1 04/26/2023 02:28 WG2048704
Chlorobenzene ND 0.00411 1 04/26/2023 02:28 WG2048704
Chlorodibromomethane ND 0.00411 1 04/26/2023 02:28 WG2048704
Chloroethane ND 0.00821 1 04/26/2023 02:28 WG2048704
Chloroform ND 0.00411 1 04/26/2023 02:28 WG2048704
Chloromethane ND 0.0205 1 04/26/2023 02:28 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 10
L1607939
SS-4
Collected date/time: 04/20/23 09:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00411 1 04/26/2023 02:28 WG2048704
4-Chlorotoluene ND 0.00821 1 04/26/2023 02:28 WG2048704
1,2-Dibromo-3-Chloropropane ND 0.0411 1 04/26/2023 02:28 WG2048704
1,2-Dibromoethane ND 0.00411 1 04/26/2023 02:28 WG2048704
Dibromomethane ND 0.00821 1 04/26/2023 02:28 WG2048704
1,2-Dichlorobenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
1,3-Dichlorobenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
1,4-Dichlorobenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
Dichlorodifluoromethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,1-Dichloroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,2-Dichloroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,1-Dichloroethene ND 0.00411 1 04/26/2023 02:28 WG2048704
cis-1,2-Dichloroethene ND 0.00411 1 04/26/2023 02:28 WG2048704
trans-1,2-Dichloroethene ND 0.00821 1 04/26/2023 02:28 WG2048704
1,2-Dichloropropane ND 0.00821 1 04/26/2023 02:28 WG2048704
1,1-Dichloropropene ND 0.00411 1 04/26/2023 02:28 WG2048704
1,3-Dichloropropane ND 0.00821 1 04/26/2023 02:28 WG2048704
cis-1,3-Dichloropropene ND 0.00411 1 04/26/2023 02:28 WG2048704
trans-1,3-Dichloropropene ND 0.00821 1 04/26/2023 02:28 WG2048704
2,2-Dichloropropane ND 0.00411 1 04/26/2023 02:28 WG2048704
Di-isopropyl ether ND 0.00164 1 04/26/2023 02:28 WG2048704
Ethylbenzene ND 0.00411 1 04/26/2023 02:28 WG2048704
Hexachloro-1,3-butadiene ND 0.0411 1 04/26/2023 02:28 WG2048704
Isopropylbenzene ND 0.00411 1 04/26/2023 02:28 WG2048704
p-Isopropyltoluene ND 0.00821 1 04/26/2023 02:28 WG2048704
2-Butanone (MEK)ND 0.164 1 04/26/2023 02:28 WG2048704
Methylene Chloride ND 0.0411 1 04/26/2023 02:28 WG2048704
4-Methyl-2-pentanone (MIBK) ND 0.0411 1 04/26/2023 02:28 WG2048704
Methyl tert-butyl ether ND 0.00164 1 04/26/2023 02:28 WG2048704
Naphthalene ND 0.0205 1 04/26/2023 02:28 WG2048704
n-Propylbenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
Styrene ND 0.0205 1 04/26/2023 02:28 WG2048704
1,1,1,2-Tetrachloroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,1,2,2-Tetrachloroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,1,2-Trichlorotrifluoroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
Tetrachloroethene ND 0.00411 1 04/26/2023 02:28 WG2048704
Toluene 0.0126 0.00821 1 04/26/2023 02:28 WG2048704
1,2,3-Trichlorobenzene ND 0.0205 1 04/26/2023 02:28 WG2048704
1,2,4-Trichlorobenzene ND 0.0205 1 04/26/2023 02:28 WG2048704
1,1,1-Trichloroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,1,2-Trichloroethane ND 0.00411 1 04/26/2023 02:28 WG2048704
Trichloroethene ND 0.00164 1 04/26/2023 02:28 WG2048704
Trichlorofluoromethane ND 0.00411 1 04/26/2023 02:28 WG2048704
1,2,3-Trichloropropane ND 0.0205 1 04/26/2023 02:28 WG2048704
1,2,4-Trimethylbenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
1,2,3-Trimethylbenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
1,3,5-Trimethylbenzene ND 0.00821 1 04/26/2023 02:28 WG2048704
Vinyl chloride ND 0.00411 1 04/26/2023 02:28 WG2048704
Xylenes, Total ND 0.0107 1 04/26/2023 02:28 WG2048704
(S) Toluene-d8 107 75.0-131 04/26/2023 02:28 WG2048704
(S) 4-Bromofluorobenzene 86.6 67.0-138 04/26/2023 02:28 WG2048704
(S) 1,2-Dichloroethane-d4 107 70.0-130 04/26/2023 02:28 WG2048704
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 10
L1607939
SS-4
Collected date/time: 04/20/23 09:20
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 26.0 5 04/26/2023 18:09 WG2048845
C28-C40 Oil Range 47.4 26.0 5 04/26/2023 18:09 WG2048845
(S) o-Terphenyl 39.3 18.0-148 04/26/2023 18:09 WG2048845
Sample Narrative:
L1607939-10 WG2048845: Cannot run at lower dilution due to viscosity of extract
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0442 1 04/27/2023 00:12 WG2048847
PCB 1221 ND 0.0442 1 04/27/2023 00:12 WG2048847
PCB 1232 ND 0.0442 1 04/27/2023 00:12 WG2048847
PCB 1242 ND 0.0442 1 04/27/2023 00:12 WG2048847
PCB 1248 ND 0.0221 1 04/27/2023 00:12 WG2048847
PCB 1254 ND 0.0221 1 04/27/2023 00:12 WG2048847
PCB 1260 ND 0.0221 1 04/27/2023 00:12 WG2048847
(S) Decachlorobiphenyl 80.7 10.0-135 04/27/2023 00:12 WG2048847
(S) Tetrachloro-m-xylene 71.8 10.0-139 04/27/2023 00:12 WG2048847
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0433 1 04/27/2023 08:02 WG2048871
Acenaphthylene ND 0.0433 1 04/27/2023 08:02 WG2048871
Anthracene ND 0.0433 1 04/27/2023 08:02 WG2048871
Benzidine ND 2.17 1 04/27/2023 08:02 WG2048871
Benzo(a)anthracene ND 0.0433 1 04/27/2023 08:02 WG2048871
Benzo(b)fluoranthene ND 0.0433 1 04/27/2023 08:02 WG2048871
Benzo(k)fluoranthene ND 0.0433 1 04/27/2023 08:02 WG2048871
Benzo(g,h,i)perylene ND 0.0433 1 04/27/2023 08:02 WG2048871
Benzo(a)pyrene ND 0.0433 1 04/27/2023 08:02 WG2048871
Bis(2-chlorethoxy)methane ND 0.433 1 04/27/2023 08:02 WG2048871
Bis(2-chloroethyl)ether ND 0.433 1 04/27/2023 08:02 WG2048871
2,2-Oxybis(1-Chloropropane) ND 0.433 1 04/27/2023 08:02 WG2048871
4-Bromophenyl-phenylether ND 0.433 1 04/27/2023 08:02 WG2048871
2-Chloronaphthalene ND 0.0433 1 04/27/2023 08:02 WG2048871
4-Chlorophenyl-phenylether ND 0.433 1 04/27/2023 08:02 WG2048871
Chrysene ND 0.0433 1 04/27/2023 08:02 WG2048871
Dibenz(a,h)anthracene ND 0.0433 1 04/27/2023 08:02 WG2048871
3,3-Dichlorobenzidine ND 0.433 1 04/27/2023 08:02 WG2048871
2,4-Dinitrotoluene ND 0.433 1 04/27/2023 08:02 WG2048871
2,6-Dinitrotoluene ND 0.433 1 04/27/2023 08:02 WG2048871
Fluoranthene ND 0.0433 1 04/27/2023 08:02 WG2048871
Fluorene ND 0.0433 1 04/27/2023 08:02 WG2048871
Hexachlorobenzene ND 0.433 1 04/27/2023 08:02 WG2048871
Hexachloro-1,3-butadiene ND 0.433 1 04/27/2023 08:02 WG2048871
Hexachlorocyclopentadiene ND 0.433 1 04/27/2023 08:02 WG2048871
Hexachloroethane ND 0.433 1 04/27/2023 08:02 WG2048871
Indeno(1,2,3-cd)pyrene ND 0.0433 1 04/27/2023 08:02 WG2048871
Isophorone ND 0.433 1 04/27/2023 08:02 WG2048871
Naphthalene ND 0.0433 1 04/27/2023 08:02 WG2048871
Nitrobenzene ND 0.433 1 04/27/2023 08:02 WG2048871
n-Nitrosodimethylamine ND 0.433 1 04/27/2023 08:02 WG2048871
n-Nitrosodiphenylamine ND 0.433 1 04/27/2023 08:02 WG2048871
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 10
L1607939
SS-4
Collected date/time: 04/20/23 09:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
n-Nitrosodi-n-propylamine ND 0.433 1 04/27/2023 08:02 WG2048871
Phenanthrene ND 0.0433 1 04/27/2023 08:02 WG2048871
Benzylbutyl phthalate ND 0.433 1 04/27/2023 08:02 WG2048871
Bis(2-ethylhexyl)phthalate ND 0.433 1 04/27/2023 08:02 WG2048871
Di-n-butyl phthalate ND 0.433 1 04/27/2023 08:02 WG2048871
Diethyl phthalate ND 0.433 1 04/27/2023 08:02 WG2048871
Dimethyl phthalate ND 0.433 1 04/27/2023 08:02 WG2048871
Di-n-octyl phthalate ND 0.433 1 04/27/2023 08:02 WG2048871
Pyrene ND 0.0433 1 04/27/2023 08:02 WG2048871
1,2,4-Trichlorobenzene ND 0.433 1 04/27/2023 08:02 WG2048871
4-Chloro-3-methylphenol ND 0.433 1 04/27/2023 08:02 WG2048871
2-Chlorophenol ND 0.433 1 04/27/2023 08:02 WG2048871
2,4-Dichlorophenol ND 0.433 1 04/27/2023 08:02 WG2048871
2,4-Dimethylphenol ND 0.433 1 04/27/2023 08:02 WG2048871
4,6-Dinitro-2-methylphenol ND 0.433 1 04/27/2023 08:02 WG2048871
2,4-Dinitrophenol ND 0.433 1 04/27/2023 08:02 WG2048871
2-Nitrophenol ND 0.433 1 04/27/2023 08:02 WG2048871
4-Nitrophenol ND 0.433 1 04/27/2023 08:02 WG2048871
Pentachlorophenol ND 0.433 1 04/27/2023 08:02 WG2048871
Phenol ND 0.433 1 04/27/2023 08:02 WG2048871
2,4,6-Trichlorophenol ND 0.433 1 04/27/2023 08:02 WG2048871
(S) Nitrobenzene-d5 42.7 10.0-122 04/27/2023 08:02 WG2048871
(S) 2-Fluorobiphenyl 50.6 15.0-120 04/27/2023 08:02 WG2048871
(S) p-Terphenyl-d14 59.7 10.0-120 04/27/2023 08:02 WG2048871
(S) Phenol-d5 48.5 10.0-120 04/27/2023 08:02 WG2048871
(S) 2-Fluorophenol 53.6 12.0-120 04/27/2023 08:02 WG2048871
(S) 2,4,6-Tribromophenol 60.3 10.0-127 04/27/2023 08:02 WG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00781 1 04/27/2023 01:00 WG2048850
Acenaphthene ND 0.00781 1 04/27/2023 01:00 WG2048850
Acenaphthylene ND 0.00781 1 04/27/2023 01:00 WG2048850
Benzo(a)anthracene 0.00826 0.00781 1 04/27/2023 01:00 WG2048850
Benzo(a)pyrene ND 0.00781 1 04/27/2023 01:00 WG2048850
Benzo(b)fluoranthene 0.00976 0.00781 1 04/27/2023 01:00 WG2048850
Benzo(g,h,i)perylene 0.00819 0.00781 1 04/27/2023 01:00 WG2048850
Benzo(k)fluoranthene ND 0.00781 1 04/27/2023 01:00 WG2048850
Chrysene 0.00928 0.00781 1 04/27/2023 01:00 WG2048850
Dibenz(a,h)anthracene ND 0.00781 1 04/27/2023 01:00 WG2048850
Fluoranthene 0.0173 0.00781 1 04/27/2023 01:00 WG2048850
Fluorene ND 0.00781 1 04/27/2023 01:00 WG2048850
Indeno(1,2,3-cd)pyrene ND 0.00781 1 04/27/2023 01:00 WG2048850
Naphthalene 0.0260 0.0260 1 04/27/2023 01:00 WG2048850
Phenanthrene 0.0130 0.00781 1 04/27/2023 01:00 WG2048850
Pyrene 0.0182 0.00781 1 04/27/2023 01:00 WG2048850
1-Methylnaphthalene ND 0.0260 1 04/27/2023 01:00 WG2048850
2-Methylnaphthalene ND 0.0260 1 04/27/2023 01:00 WG2048850
2-Chloronaphthalene ND 0.0260 1 04/27/2023 01:00 WG2048850
(S) p-Terphenyl-d14 69.0 23.0-120 04/27/2023 01:00 WG2048850
(S) Nitrobenzene-d5 51.1 14.0-149 04/27/2023 01:00 WG2048850
(S) 2-Fluorobiphenyl 69.1 34.0-125 04/27/2023 01:00 WG2048850
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 11
L1607939
FD-4
Collected date/time: 04/20/23 11:00
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 968 1 04/26/2023 00:59 WG2048584
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)10.8 6.02 1 04/28/2023 22:12 WG2050781
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.00102 0.000500 1 04/28/2023 12:10 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 04/28/2023 12:22 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/25/2023 23:43 WG2048081
Arsenic 0.0406 0.0100 1 04/25/2023 23:43 WG2048081
Beryllium ND 0.00200 1 04/25/2023 23:43 WG2048081
Cadmium ND 0.00200 1 04/25/2023 23:43 WG2048081
Chromium 0.0180 0.0100 1 04/25/2023 23:43 WG2048081
Copper 0.0191 0.0100 1 04/25/2023 23:43 WG2048081
Lead 0.00645 0.00600 1 04/25/2023 23:43 WG2048081
Nickel 0.0187 0.0100 1 04/25/2023 23:43 WG2048081
Selenium ND 0.0100 1 04/25/2023 23:43 WG2048081
Silver ND 0.00500 1 04/25/2023 23:43 WG2048081
Thallium ND 0.0100 1 04/25/2023 23:43 WG2048081
Zinc ND 0.0500 1 04/25/2023 23:43 WG2048081
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.500 5 04/26/2023 02:17 WG2047755
(S) a,a,a-Trifluorotoluene(FID) 113 78.0-120 04/26/2023 02:17 WG2047755
Sample Narrative:
L1607939-11 WG2047755: Lowest possible dilution due to sample foaming.
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 04/24/2023 09:27 WG2047326
Acrolein ND 0.0500 1 04/24/2023 09:27 WG2047326
Acrylonitrile ND 0.0100 1 04/24/2023 09:27 WG2047326
Benzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Bromobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Bromodichloromethane ND 0.00100 1 04/24/2023 09:27 WG2047326
Bromoform ND 0.00100 1 04/24/2023 09:27 WG2047326
Bromomethane ND 0.00500 1 04/24/2023 09:27 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 11
L1607939
FD-4
Collected date/time: 04/20/23 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
n-Butylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
sec-Butylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
tert-Butylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Carbon tetrachloride ND 0.00100 1 04/24/2023 09:27 WG2047326
Chlorobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Chlorodibromomethane ND 0.00100 1 04/24/2023 09:27 WG2047326
Chloroethane ND 0.00500 1 04/24/2023 09:27 WG2047326
Chloroform ND 0.00500 1 04/24/2023 09:27 WG2047326
Chloromethane ND 0.00250 1 04/24/2023 09:27 WG2047326
2-Chlorotoluene ND 0.00100 1 04/24/2023 09:27 WG2047326
4-Chlorotoluene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2-Dibromo-3-Chloropropane ND 0.00500 1 04/24/2023 09:27 WG2047326
1,2-Dibromoethane ND 0.00100 1 04/24/2023 09:27 WG2047326
Dibromomethane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2-Dichlorobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,3-Dichlorobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,4-Dichlorobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Dichlorodifluoromethane ND 0.00500 1 04/24/2023 09:27 WG2047326
1,1-Dichloroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2-Dichloroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1-Dichloroethene ND 0.00100 1 04/24/2023 09:27 WG2047326
cis-1,2-Dichloroethene ND 0.00100 1 04/24/2023 09:27 WG2047326
trans-1,2-Dichloroethene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2-Dichloropropane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1-Dichloropropene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,3-Dichloropropane ND 0.00100 1 04/24/2023 09:27 WG2047326
cis-1,3-Dichloropropene ND 0.00100 1 04/24/2023 09:27 WG2047326
trans-1,3-Dichloropropene ND 0.00100 1 04/24/2023 09:27 WG2047326
2,2-Dichloropropane ND 0.00100 1 04/24/2023 09:27 WG2047326
Di-isopropyl ether ND 0.00100 1 04/24/2023 09:27 WG2047326
Ethylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Hexachloro-1,3-butadiene ND 0.00100 1 04/24/2023 09:27 WG2047326
Isopropylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
p-Isopropyltoluene ND 0.00100 1 04/24/2023 09:27 WG2047326
2-Butanone (MEK)ND 0.0100 1 04/24/2023 09:27 WG2047326
Methylene Chloride ND 0.00500 1 04/24/2023 09:27 WG2047326
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 04/24/2023 09:27 WG2047326
Methyl tert-butyl ether ND 0.00100 1 04/24/2023 09:27 WG2047326
Naphthalene ND 0.00500 1 04/24/2023 09:27 WG2047326
n-Propylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
Styrene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1,1,2-Tetrachloroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1,2,2-Tetrachloroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
Tetrachloroethene ND 0.00100 1 04/24/2023 09:27 WG2047326
Toluene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2,3-Trichlorobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2,4-Trichlorobenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1,1-Trichloroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
1,1,2-Trichloroethane ND 0.00100 1 04/24/2023 09:27 WG2047326
Trichloroethene ND 0.00100 1 04/24/2023 09:27 WG2047326
Trichlorofluoromethane ND 0.00500 1 04/24/2023 09:27 WG2047326
1,2,3-Trichloropropane ND 0.00250 1 04/24/2023 09:27 WG2047326
1,2,4-Trimethylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,2,3-Trimethylbenzene ND 0.00100 1 04/24/2023 09:27 WG2047326
1,3,5-Trimethylbenzene ND J4 0.00100 1 04/24/2023 09:27 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 11
L1607939
FD-4
Collected date/time: 04/20/23 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Vinyl chloride ND 0.00100 1 04/24/2023 09:27 WG2047326
Xylenes, Total ND 0.00300 1 04/24/2023 09:27 WG2047326
(S) Toluene-d8 106 80.0-120 04/24/2023 09:27 WG2047326
(S) 4-Bromofluorobenzene 99.1 77.0-126 04/24/2023 09:27 WG2047326
(S) 1,2-Dichloroethane-d4 104 70.0-130 04/24/2023 09:27 WG2047326
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range 0.697 0.100 1 04/23/2023 05:40 WG2046978
C28-C40 Oil Range 0.324 0.100 1 04/23/2023 05:40 WG2046978
(S) o-Terphenyl 106 52.0-156 04/23/2023 05:40 WG2046978
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 04/25/2023 05:12 WG2047799
PCB 1221 ND 0.000500 1 04/25/2023 05:12 WG2047799
PCB 1232 ND 0.000500 1 04/25/2023 05:12 WG2047799
PCB 1242 ND 0.000500 1 04/25/2023 05:12 WG2047799
PCB 1248 ND 0.000500 1 04/25/2023 05:12 WG2047799
PCB 1254 ND 0.000500 1 04/25/2023 05:12 WG2047799
PCB 1260 ND 0.000500 1 04/25/2023 05:12 WG2047799
(S) Decachlorobiphenyl 39.0 10.0-128 04/25/2023 05:12 WG2047799
(S) Tetrachloro-m-xylene 70.5 10.0-127 04/25/2023 05:12 WG2047799
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 04/26/2023 04:29 WG2047405
Acenaphthylene ND 0.00100 1 04/26/2023 04:29 WG2047405
Anthracene ND 0.00100 1 04/26/2023 04:29 WG2047405
Benzidine ND J4 0.0100 1 04/26/2023 04:29 WG2047405
Benzo(a)anthracene ND 0.00100 1 04/26/2023 04:29 WG2047405
Benzo(b)fluoranthene ND 0.00100 1 04/26/2023 04:29 WG2047405
Benzo(k)fluoranthene ND 0.00100 1 04/26/2023 04:29 WG2047405
Benzo(g,h,i)perylene ND 0.00100 1 04/26/2023 04:29 WG2047405
Benzo(a)pyrene ND 0.00100 1 04/26/2023 04:29 WG2047405
Bis(2-chlorethoxy)methane ND 0.0100 1 04/26/2023 04:29 WG2047405
Bis(2-chloroethyl)ether ND 0.0100 1 04/26/2023 04:29 WG2047405
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 04/26/2023 04:29 WG2047405
4-Bromophenyl-phenylether ND 0.0100 1 04/26/2023 04:29 WG2047405
2-Chloronaphthalene ND 0.00100 1 04/26/2023 04:29 WG2047405
4-Chlorophenyl-phenylether ND 0.0100 1 04/26/2023 04:29 WG2047405
Chrysene ND 0.00100 1 04/26/2023 04:29 WG2047405
Dibenz(a,h)anthracene ND 0.00100 1 04/26/2023 04:29 WG2047405
1,2-Dichlorobenzene ND 0.0100 1 04/26/2023 04:29 WG2047405
1,3-Dichlorobenzene ND 0.0100 1 04/26/2023 04:29 WG2047405
1,4-Dichlorobenzene ND 0.0100 1 04/26/2023 04:29 WG2047405
3,3-Dichlorobenzidine ND 0.0100 1 04/26/2023 04:29 WG2047405
2,4-Dinitrotoluene ND 0.0100 1 04/26/2023 04:29 WG2047405
2,6-Dinitrotoluene ND 0.0100 1 04/26/2023 04:29 WG2047405
Fluoranthene ND 0.00100 1 04/26/2023 04:29 WG2047405
Fluorene ND 0.00100 1 04/26/2023 04:29 WG2047405
Hexachlorobenzene ND 0.00100 1 04/26/2023 04:29 WG2047405
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 11
L1607939
FD-4
Collected date/time: 04/20/23 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexachloro-1,3-butadiene ND 0.0100 1 04/26/2023 04:29 WG2047405
Hexachlorocyclopentadiene ND 0.0100 1 04/26/2023 04:29 WG2047405
Hexachloroethane ND 0.0100 1 04/26/2023 04:29 WG2047405
Indeno(1,2,3-cd)pyrene ND 0.00100 1 04/26/2023 04:29 WG2047405
Isophorone ND 0.0100 1 04/26/2023 04:29 WG2047405
Naphthalene ND 0.00100 1 04/26/2023 04:29 WG2047405
Nitrobenzene ND 0.0100 1 04/26/2023 04:29 WG2047405
n-Nitrosodimethylamine ND 0.0100 1 04/26/2023 04:29 WG2047405
n-Nitrosodiphenylamine ND 0.0100 1 04/26/2023 04:29 WG2047405
n-Nitrosodi-n-propylamine ND 0.0100 1 04/26/2023 04:29 WG2047405
Phenanthrene ND 0.00100 1 04/26/2023 04:29 WG2047405
Benzylbutyl phthalate ND 0.00300 1 04/26/2023 04:29 WG2047405
Bis(2-ethylhexyl)phthalate ND 0.00300 1 04/26/2023 04:29 WG2047405
Di-n-butyl phthalate ND 0.00300 1 04/26/2023 04:29 WG2047405
Diethyl phthalate ND 0.00300 1 04/26/2023 04:29 WG2047405
Dimethyl phthalate ND 0.00300 1 04/26/2023 04:29 WG2047405
Di-n-octyl phthalate ND 0.00300 1 04/26/2023 04:29 WG2047405
Pyrene ND 0.00100 1 04/26/2023 04:29 WG2047405
1,2,4-Trichlorobenzene ND 0.0100 1 04/26/2023 04:29 WG2047405
4-Chloro-3-methylphenol ND 0.0100 1 04/26/2023 04:29 WG2047405
2-Chlorophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
2,4-Dichlorophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
2,4-Dimethylphenol ND 0.0100 1 04/26/2023 04:29 WG2047405
4,6-Dinitro-2-methylphenol ND 0.0100 1 04/26/2023 04:29 WG2047405
2,4-Dinitrophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
2-Nitrophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
4-Nitrophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
Pentachlorophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
Phenol ND 0.0100 1 04/26/2023 04:29 WG2047405
2,4,6-Trichlorophenol ND 0.0100 1 04/26/2023 04:29 WG2047405
(S) 2-Fluorophenol 20.2 10.0-120 04/26/2023 04:29 WG2047405
(S) Phenol-d5 16.2 10.0-120 04/26/2023 04:29 WG2047405
(S) Nitrobenzene-d5 54.4 10.0-127 04/26/2023 04:29 WG2047405
(S) 2-Fluorobiphenyl 55.9 10.0-130 04/26/2023 04:29 WG2047405
(S) 2,4,6-Tribromophenol 33.8 10.0-155 04/26/2023 04:29 WG2047405
(S) p-Terphenyl-d14 42.5 10.0-128 04/26/2023 04:29 WG2047405
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Acenaphthene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Acenaphthylene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Benzo(a)anthracene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Benzo(a)pyrene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Benzo(b)fluoranthene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Benzo(g,h,i)perylene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Benzo(k)fluoranthene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Chrysene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Dibenz(a,h)anthracene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Fluoranthene ND 0.000100 1 04/25/2023 21:24 WG2047984
Fluorene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Naphthalene ND 0.000250 1 04/25/2023 21:24 WG2047984
Phenanthrene ND 0.0000500 1 04/25/2023 21:24 WG2047984
Pyrene ND 0.0000500 1 04/25/2023 21:24 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 11
L1607939
FD-4
Collected date/time: 04/20/23 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1-Methylnaphthalene ND 0.000250 1 04/25/2023 21:24 WG2047984
2-Methylnaphthalene ND 0.000250 1 04/25/2023 21:24 WG2047984
2-Chloronaphthalene ND 0.000250 1 04/25/2023 21:24 WG2047984
(S) Nitrobenzene-d5 92.6 31.0-160 04/25/2023 21:24 WG2047984
(S) 2-Fluorobiphenyl 109 48.0-148 04/25/2023 21:24 WG2047984
(S) p-Terphenyl-d14 102 37.0-146 04/25/2023 21:24 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 12
L1607939
FD-3
Collected date/time: 04/20/23 13:05
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 681 1 04/26/2023 00:59 WG2048584
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.41 1 04/28/2023 22:12 WG2050781
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 04/28/2023 12:43 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 04/28/2023 12:24 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/25/2023 23:46 WG2048081
Arsenic 0.0255 0.0100 1 04/25/2023 23:46 WG2048081
Beryllium ND 0.00200 1 04/25/2023 23:46 WG2048081
Cadmium ND 0.00200 1 04/25/2023 23:46 WG2048081
Chromium ND 0.0100 1 04/25/2023 23:46 WG2048081
Copper ND 0.0100 1 04/25/2023 23:46 WG2048081
Lead ND 0.00600 1 04/25/2023 23:46 WG2048081
Nickel ND 0.0100 1 04/25/2023 23:46 WG2048081
Selenium ND 0.0100 1 04/25/2023 23:46 WG2048081
Silver ND 0.00500 1 04/25/2023 23:46 WG2048081
Thallium ND 0.0100 1 04/25/2023 23:46 WG2048081
Zinc ND 0.0500 1 04/25/2023 23:46 WG2048081
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 04/26/2023 02:39 WG2047755
(S) a,a,a-Trifluorotoluene(FID) 114 78.0-120 04/26/2023 02:39 WG2047755
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 04/24/2023 09:48 WG2047326
Acrolein ND 0.0500 1 04/24/2023 09:48 WG2047326
Acrylonitrile ND 0.0100 1 04/24/2023 09:48 WG2047326
Benzene ND 0.00100 1 04/24/2023 09:48 WG2047326
Bromobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
Bromodichloromethane ND 0.00100 1 04/24/2023 09:48 WG2047326
Bromoform ND 0.00100 1 04/24/2023 09:48 WG2047326
Bromomethane ND 0.00500 1 04/24/2023 09:48 WG2047326
n-Butylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
sec-Butylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
tert-Butylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 12
L1607939
FD-3
Collected date/time: 04/20/23 13:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 04/24/2023 09:48 WG2047326
Chlorobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
Chlorodibromomethane ND 0.00100 1 04/24/2023 09:48 WG2047326
Chloroethane ND 0.00500 1 04/24/2023 09:48 WG2047326
Chloroform ND 0.00500 1 04/24/2023 09:48 WG2047326
Chloromethane ND 0.00250 1 04/24/2023 09:48 WG2047326
2-Chlorotoluene ND 0.00100 1 04/24/2023 09:48 WG2047326
4-Chlorotoluene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,2-Dibromo-3-Chloropropane ND 0.00500 1 04/24/2023 09:48 WG2047326
1,2-Dibromoethane ND 0.00100 1 04/24/2023 09:48 WG2047326
Dibromomethane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,2-Dichlorobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,3-Dichlorobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,4-Dichlorobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
Dichlorodifluoromethane ND 0.00500 1 04/24/2023 09:48 WG2047326
1,1-Dichloroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,2-Dichloroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1-Dichloroethene ND 0.00100 1 04/24/2023 09:48 WG2047326
cis-1,2-Dichloroethene ND 0.00100 1 04/24/2023 09:48 WG2047326
trans-1,2-Dichloroethene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,2-Dichloropropane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1-Dichloropropene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,3-Dichloropropane ND 0.00100 1 04/24/2023 09:48 WG2047326
cis-1,3-Dichloropropene ND 0.00100 1 04/24/2023 09:48 WG2047326
trans-1,3-Dichloropropene ND 0.00100 1 04/24/2023 09:48 WG2047326
2,2-Dichloropropane ND 0.00100 1 04/24/2023 09:48 WG2047326
Di-isopropyl ether ND 0.00100 1 04/24/2023 09:48 WG2047326
Ethylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
Hexachloro-1,3-butadiene ND 0.00100 1 04/24/2023 09:48 WG2047326
Isopropylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
p-Isopropyltoluene ND 0.00100 1 04/24/2023 09:48 WG2047326
2-Butanone (MEK)ND 0.0100 1 04/24/2023 09:48 WG2047326
Methylene Chloride ND 0.00500 1 04/24/2023 09:48 WG2047326
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 04/24/2023 09:48 WG2047326
Methyl tert-butyl ether ND 0.00100 1 04/24/2023 09:48 WG2047326
Naphthalene ND 0.00500 1 04/24/2023 09:48 WG2047326
n-Propylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
Styrene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1,1,2-Tetrachloroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1,2,2-Tetrachloroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
Tetrachloroethene ND 0.00100 1 04/24/2023 09:48 WG2047326
Toluene 0.00330 0.00100 1 04/24/2023 09:48 WG2047326
1,2,3-Trichlorobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,2,4-Trichlorobenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1,1-Trichloroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
1,1,2-Trichloroethane ND 0.00100 1 04/24/2023 09:48 WG2047326
Trichloroethene ND 0.00100 1 04/24/2023 09:48 WG2047326
Trichlorofluoromethane ND 0.00500 1 04/24/2023 09:48 WG2047326
1,2,3-Trichloropropane ND 0.00250 1 04/24/2023 09:48 WG2047326
1,2,4-Trimethylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,2,3-Trimethylbenzene ND 0.00100 1 04/24/2023 09:48 WG2047326
1,3,5-Trimethylbenzene ND J4 0.00100 1 04/24/2023 09:48 WG2047326
Vinyl chloride ND 0.00100 1 04/24/2023 09:48 WG2047326
Xylenes, Total ND 0.00300 1 04/24/2023 09:48 WG2047326
(S) Toluene-d8 110 80.0-120 04/24/2023 09:48 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 12
L1607939
FD-3
Collected date/time: 04/20/23 13:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 101 77.0-126 04/24/2023 09:48 WG2047326
(S) 1,2-Dichloroethane-d4 103 70.0-130 04/24/2023 09:48 WG2047326
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range 0.268 B 0.100 1 04/23/2023 06:03 WG2046978
C28-C40 Oil Range 0.155 0.100 1 04/23/2023 06:03 WG2046978
(S) o-Terphenyl 104 52.0-156 04/23/2023 06:03 WG2046978
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 04/25/2023 03:32 WG2047799
PCB 1221 ND 0.000500 1 04/25/2023 03:32 WG2047799
PCB 1232 ND 0.000500 1 04/25/2023 03:32 WG2047799
PCB 1242 ND 0.000500 1 04/25/2023 03:32 WG2047799
PCB 1248 ND 0.000500 1 04/25/2023 03:32 WG2047799
PCB 1254 ND 0.000500 1 04/25/2023 03:32 WG2047799
PCB 1260 ND 0.000500 1 04/25/2023 03:32 WG2047799
(S) Decachlorobiphenyl 66.2 10.0-128 04/25/2023 03:32 WG2047799
(S) Tetrachloro-m-xylene 88.5 10.0-127 04/25/2023 03:32 WG2047799
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 04/27/2023 20:05 WG2048000
Acenaphthylene ND 0.00100 1 04/27/2023 20:05 WG2048000
Anthracene ND 0.00100 1 04/27/2023 20:05 WG2048000
Benzidine ND J4 0.0100 1 04/27/2023 20:05 WG2048000
Benzo(a)anthracene ND 0.00100 1 04/27/2023 20:05 WG2048000
Benzo(b)fluoranthene ND 0.00100 1 04/27/2023 20:05 WG2048000
Benzo(k)fluoranthene ND 0.00100 1 04/27/2023 20:05 WG2048000
Benzo(g,h,i)perylene ND 0.00100 1 04/27/2023 20:05 WG2048000
Benzo(a)pyrene ND 0.00100 1 04/27/2023 20:05 WG2048000
Bis(2-chlorethoxy)methane ND 0.0100 1 04/27/2023 20:05 WG2048000
Bis(2-chloroethyl)ether ND 0.0100 1 04/27/2023 20:05 WG2048000
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 04/27/2023 20:05 WG2048000
4-Bromophenyl-phenylether ND 0.0100 1 04/27/2023 20:05 WG2048000
2-Chloronaphthalene ND 0.00100 1 04/27/2023 20:05 WG2048000
4-Chlorophenyl-phenylether ND 0.0100 1 04/27/2023 20:05 WG2048000
Chrysene ND 0.00100 1 04/27/2023 20:05 WG2048000
Dibenz(a,h)anthracene ND 0.00100 1 04/27/2023 20:05 WG2048000
1,2-Dichlorobenzene ND 0.0100 1 04/27/2023 20:05 WG2048000
1,3-Dichlorobenzene ND 0.0100 1 04/27/2023 20:05 WG2048000
1,4-Dichlorobenzene ND 0.0100 1 04/27/2023 20:05 WG2048000
3,3-Dichlorobenzidine ND 0.0100 1 04/27/2023 20:05 WG2048000
2,4-Dinitrotoluene ND 0.0100 1 04/27/2023 20:05 WG2048000
2,6-Dinitrotoluene ND 0.0100 1 04/27/2023 20:05 WG2048000
Fluoranthene ND 0.00100 1 04/27/2023 20:05 WG2048000
Fluorene ND 0.00100 1 04/27/2023 20:05 WG2048000
Hexachlorobenzene ND 0.00100 1 04/27/2023 20:05 WG2048000
Hexachloro-1,3-butadiene ND 0.0100 1 04/27/2023 20:05 WG2048000
Hexachlorocyclopentadiene ND 0.0100 1 04/27/2023 20:05 WG2048000
Hexachloroethane ND 0.0100 1 04/27/2023 20:05 WG2048000
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 12
L1607939
FD-3
Collected date/time: 04/20/23 13:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Indeno(1,2,3-cd)pyrene ND 0.00100 1 04/27/2023 20:05 WG2048000
Isophorone ND 0.0100 1 04/27/2023 20:05 WG2048000
Naphthalene ND 0.00100 1 04/27/2023 20:05 WG2048000
Nitrobenzene ND 0.0100 1 04/27/2023 20:05 WG2048000
n-Nitrosodimethylamine ND 0.0100 1 04/27/2023 20:05 WG2048000
n-Nitrosodiphenylamine ND 0.0100 1 04/27/2023 20:05 WG2048000
n-Nitrosodi-n-propylamine ND 0.0100 1 04/27/2023 20:05 WG2048000
Phenanthrene ND 0.00100 1 04/27/2023 20:05 WG2048000
Benzylbutyl phthalate ND 0.00300 1 04/27/2023 20:05 WG2048000
Bis(2-ethylhexyl)phthalate ND 0.00300 1 04/27/2023 20:05 WG2048000
Di-n-butyl phthalate ND 0.00300 1 04/27/2023 20:05 WG2048000
Diethyl phthalate ND 0.00300 1 04/27/2023 20:05 WG2048000
Dimethyl phthalate ND 0.00300 1 04/27/2023 20:05 WG2048000
Di-n-octyl phthalate ND 0.00300 1 04/27/2023 20:05 WG2048000
Pyrene ND 0.00100 1 04/27/2023 20:05 WG2048000
1,2,4-Trichlorobenzene ND 0.0100 1 04/27/2023 20:05 WG2048000
4-Chloro-3-methylphenol ND 0.0100 1 04/27/2023 20:05 WG2048000
2-Chlorophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
2,4-Dichlorophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
2,4-Dimethylphenol ND 0.0100 1 04/27/2023 20:05 WG2048000
4,6-Dinitro-2-methylphenol ND 0.0100 1 04/27/2023 20:05 WG2048000
2,4-Dinitrophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
2-Nitrophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
4-Nitrophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
Pentachlorophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
Phenol ND 0.0100 1 04/27/2023 20:05 WG2048000
2,4,6-Trichlorophenol ND 0.0100 1 04/27/2023 20:05 WG2048000
(S) 2-Fluorophenol 36.2 10.0-120 04/27/2023 20:05 WG2048000
(S) Phenol-d5 23.9 10.0-120 04/27/2023 20:05 WG2048000
(S) Nitrobenzene-d5 64.8 10.0-127 04/27/2023 20:05 WG2048000
(S) 2-Fluorobiphenyl 73.6 10.0-130 04/27/2023 20:05 WG2048000
(S) 2,4,6-Tribromophenol 69.0 10.0-155 04/27/2023 20:05 WG2048000
(S) p-Terphenyl-d14 87.8 10.0-128 04/27/2023 20:05 WG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Acenaphthene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Acenaphthylene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Benzo(a)anthracene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Benzo(a)pyrene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Benzo(b)fluoranthene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Benzo(g,h,i)perylene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Benzo(k)fluoranthene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Chrysene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Dibenz(a,h)anthracene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Fluoranthene ND 0.000100 1 04/25/2023 21:41 WG2047984
Fluorene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Naphthalene ND 0.000250 1 04/25/2023 21:41 WG2047984
Phenanthrene ND 0.0000500 1 04/25/2023 21:41 WG2047984
Pyrene ND 0.0000500 1 04/25/2023 21:41 WG2047984
1-Methylnaphthalene ND 0.000250 1 04/25/2023 21:41 WG2047984
2-Methylnaphthalene ND 0.000250 1 04/25/2023 21:41 WG2047984
2-Chloronaphthalene ND 0.000250 1 04/25/2023 21:41 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 12
L1607939
FD-3
Collected date/time: 04/20/23 13:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Nitrobenzene-d5 92.6 31.0-160 04/25/2023 21:41 WG2047984
(S) 2-Fluorobiphenyl 105 48.0-148 04/25/2023 21:41 WG2047984
(S) p-Terphenyl-d14 99.5 37.0-146 04/25/2023 21:41 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 13
L1607939
FD-2
Collected date/time: 04/20/23 15:30
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 791 1 04/26/2023 00:59 WG2048584
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.95 1 04/30/2023 16:09 WG2051086
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 04/28/2023 12:54 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury 0.000454 0.000200 1 04/28/2023 12:30 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/25/2023 23:55 WG2048081
Arsenic 0.0471 0.0100 1 04/26/2023 19:14 WG2048081
Beryllium ND 0.00200 1 04/25/2023 23:55 WG2048081
Cadmium ND 0.00200 1 04/25/2023 23:55 WG2048081
Chromium ND 0.0100 1 04/25/2023 23:55 WG2048081
Copper ND 0.0100 1 04/25/2023 23:55 WG2048081
Lead ND 0.00600 1 04/25/2023 23:55 WG2048081
Nickel 0.0115 0.0100 1 04/25/2023 23:55 WG2048081
Selenium ND 0.0100 1 04/25/2023 23:55 WG2048081
Silver ND 0.00500 1 04/25/2023 23:55 WG2048081
Thallium ND 0.0100 1 04/25/2023 23:55 WG2048081
Zinc ND 0.0500 1 04/25/2023 23:55 WG2048081
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 04/26/2023 06:25 WG2047755
(S) a,a,a-Trifluorotoluene(FID) 107 78.0-120 04/26/2023 06:25 WG2047755
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 04/24/2023 10:09 WG2047326
Acrolein ND 0.0500 1 04/24/2023 10:09 WG2047326
Acrylonitrile ND 0.0100 1 04/24/2023 10:09 WG2047326
Benzene ND 0.00100 1 04/24/2023 10:09 WG2047326
Bromobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
Bromodichloromethane ND 0.00100 1 04/24/2023 10:09 WG2047326
Bromoform ND 0.00100 1 04/24/2023 10:09 WG2047326
Bromomethane ND 0.00500 1 04/24/2023 10:09 WG2047326
n-Butylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
sec-Butylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
tert-Butylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 13
L1607939
FD-2
Collected date/time: 04/20/23 15:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 04/24/2023 10:09 WG2047326
Chlorobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
Chlorodibromomethane ND 0.00100 1 04/24/2023 10:09 WG2047326
Chloroethane ND 0.00500 1 04/24/2023 10:09 WG2047326
Chloroform ND 0.00500 1 04/24/2023 10:09 WG2047326
Chloromethane ND 0.00250 1 04/24/2023 10:09 WG2047326
2-Chlorotoluene ND 0.00100 1 04/24/2023 10:09 WG2047326
4-Chlorotoluene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,2-Dibromo-3-Chloropropane ND 0.00500 1 04/24/2023 10:09 WG2047326
1,2-Dibromoethane ND 0.00100 1 04/24/2023 10:09 WG2047326
Dibromomethane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,2-Dichlorobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,3-Dichlorobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,4-Dichlorobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
Dichlorodifluoromethane ND 0.00500 1 04/24/2023 10:09 WG2047326
1,1-Dichloroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,2-Dichloroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1-Dichloroethene ND 0.00100 1 04/24/2023 10:09 WG2047326
cis-1,2-Dichloroethene ND 0.00100 1 04/24/2023 10:09 WG2047326
trans-1,2-Dichloroethene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,2-Dichloropropane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1-Dichloropropene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,3-Dichloropropane ND 0.00100 1 04/24/2023 10:09 WG2047326
cis-1,3-Dichloropropene ND 0.00100 1 04/24/2023 10:09 WG2047326
trans-1,3-Dichloropropene ND 0.00100 1 04/24/2023 10:09 WG2047326
2,2-Dichloropropane ND 0.00100 1 04/24/2023 10:09 WG2047326
Di-isopropyl ether ND 0.00100 1 04/24/2023 10:09 WG2047326
Ethylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
Hexachloro-1,3-butadiene ND 0.00100 1 04/24/2023 10:09 WG2047326
Isopropylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
p-Isopropyltoluene ND 0.00100 1 04/24/2023 10:09 WG2047326
2-Butanone (MEK)ND 0.0100 1 04/24/2023 10:09 WG2047326
Methylene Chloride ND 0.00500 1 04/24/2023 10:09 WG2047326
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 04/24/2023 10:09 WG2047326
Methyl tert-butyl ether ND 0.00100 1 04/24/2023 10:09 WG2047326
Naphthalene ND 0.00500 1 04/24/2023 10:09 WG2047326
n-Propylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
Styrene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1,1,2-Tetrachloroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1,2,2-Tetrachloroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
Tetrachloroethene ND 0.00100 1 04/24/2023 10:09 WG2047326
Toluene 0.00158 0.00100 1 04/24/2023 10:09 WG2047326
1,2,3-Trichlorobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,2,4-Trichlorobenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1,1-Trichloroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
1,1,2-Trichloroethane ND 0.00100 1 04/24/2023 10:09 WG2047326
Trichloroethene ND 0.00100 1 04/24/2023 10:09 WG2047326
Trichlorofluoromethane ND 0.00500 1 04/24/2023 10:09 WG2047326
1,2,3-Trichloropropane ND 0.00250 1 04/24/2023 10:09 WG2047326
1,2,4-Trimethylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,2,3-Trimethylbenzene ND 0.00100 1 04/24/2023 10:09 WG2047326
1,3,5-Trimethylbenzene ND J4 0.00100 1 04/24/2023 10:09 WG2047326
Vinyl chloride ND 0.00100 1 04/24/2023 10:09 WG2047326
Xylenes, Total ND 0.00300 1 04/24/2023 10:09 WG2047326
(S) Toluene-d8 109 80.0-120 04/24/2023 10:09 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 13
L1607939
FD-2
Collected date/time: 04/20/23 15:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 98.7 77.0-126 04/24/2023 10:09 WG2047326
(S) 1,2-Dichloroethane-d4 102 70.0-130 04/24/2023 10:09 WG2047326
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range 0.461 B 0.100 1 04/23/2023 06:26 WG2046978
C28-C40 Oil Range 0.319 0.100 1 04/23/2023 06:26 WG2046978
(S) o-Terphenyl 103 52.0-156 04/23/2023 06:26 WG2046978
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 04/25/2023 03:44 WG2047799
PCB 1221 ND 0.000500 1 04/25/2023 03:44 WG2047799
PCB 1232 ND 0.000500 1 04/25/2023 03:44 WG2047799
PCB 1242 ND 0.000500 1 04/25/2023 03:44 WG2047799
PCB 1248 ND 0.000500 1 04/25/2023 03:44 WG2047799
PCB 1254 ND 0.000500 1 04/25/2023 03:44 WG2047799
PCB 1260 ND 0.000500 1 04/25/2023 03:44 WG2047799
(S) Decachlorobiphenyl 25.1 10.0-128 04/25/2023 03:44 WG2047799
(S) Tetrachloro-m-xylene 62.0 10.0-127 04/25/2023 03:44 WG2047799
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Acenaphthylene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Anthracene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Benzidine ND J4 0.0105 1.05 04/27/2023 22:58 WG2048000
Benzo(a)anthracene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Benzo(b)fluoranthene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Benzo(k)fluoranthene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Benzo(g,h,i)perylene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Benzo(a)pyrene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Bis(2-chlorethoxy)methane ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Bis(2-chloroethyl)ether ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 04/27/2023 22:58 WG2048000
4-Bromophenyl-phenylether ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2-Chloronaphthalene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
4-Chlorophenyl-phenylether ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Chrysene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Dibenz(a,h)anthracene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
1,2-Dichlorobenzene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
1,3-Dichlorobenzene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
1,4-Dichlorobenzene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
3,3-Dichlorobenzidine ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,4-Dinitrotoluene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,6-Dinitrotoluene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Fluoranthene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Fluorene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Hexachlorobenzene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Hexachloro-1,3-butadiene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Hexachlorocyclopentadiene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Hexachloroethane ND 0.0105 1.05 04/27/2023 22:58 WG2048000
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 13
L1607939
FD-2
Collected date/time: 04/20/23 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Isophorone ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Naphthalene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Nitrobenzene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
n-Nitrosodimethylamine ND 0.0105 1.05 04/27/2023 22:58 WG2048000
n-Nitrosodiphenylamine ND 0.0105 1.05 04/27/2023 22:58 WG2048000
n-Nitrosodi-n-propylamine ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Phenanthrene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
Benzylbutyl phthalate ND 0.00315 1.05 04/27/2023 22:58 WG2048000
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 04/27/2023 22:58 WG2048000
Di-n-butyl phthalate ND 0.00315 1.05 04/27/2023 22:58 WG2048000
Diethyl phthalate ND 0.00315 1.05 04/27/2023 22:58 WG2048000
Dimethyl phthalate ND 0.00315 1.05 04/27/2023 22:58 WG2048000
Di-n-octyl phthalate ND 0.00315 1.05 04/27/2023 22:58 WG2048000
Pyrene ND 0.00105 1.05 04/27/2023 22:58 WG2048000
1,2,4-Trichlorobenzene ND 0.0105 1.05 04/27/2023 22:58 WG2048000
4-Chloro-3-methylphenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2-Chlorophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,4-Dichlorophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,4-Dimethylphenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,4-Dinitrophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2-Nitrophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
4-Nitrophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Pentachlorophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
Phenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
2,4,6-Trichlorophenol ND 0.0105 1.05 04/27/2023 22:58 WG2048000
(S) 2-Fluorophenol 34.7 10.0-120 04/27/2023 22:58 WG2048000
(S) Phenol-d5 22.0 10.0-120 04/27/2023 22:58 WG2048000
(S) Nitrobenzene-d5 59.9 10.0-127 04/27/2023 22:58 WG2048000
(S) 2-Fluorobiphenyl 67.8 10.0-130 04/27/2023 22:58 WG2048000
(S) 2,4,6-Tribromophenol 64.3 10.0-155 04/27/2023 22:58 WG2048000
(S) p-Terphenyl-d14 85.6 10.0-128 04/27/2023 22:58 WG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Acenaphthene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Acenaphthylene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Benzo(a)anthracene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Benzo(a)pyrene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Benzo(b)fluoranthene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Benzo(g,h,i)perylene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Benzo(k)fluoranthene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Chrysene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Dibenz(a,h)anthracene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Fluoranthene ND 0.000100 1 04/25/2023 21:59 WG2047984
Fluorene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Naphthalene ND 0.000250 1 04/25/2023 21:59 WG2047984
Phenanthrene ND 0.0000500 1 04/25/2023 21:59 WG2047984
Pyrene ND 0.0000500 1 04/25/2023 21:59 WG2047984
1-Methylnaphthalene ND 0.000250 1 04/25/2023 21:59 WG2047984
2-Methylnaphthalene ND 0.000250 1 04/25/2023 21:59 WG2047984
2-Chloronaphthalene ND 0.000250 1 04/25/2023 21:59 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 13
L1607939
FD-2
Collected date/time: 04/20/23 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Nitrobenzene-d5 88.4 31.0-160 04/25/2023 21:59 WG2047984
(S) 2-Fluorobiphenyl 101 48.0-148 04/25/2023 21:59 WG2047984
(S) p-Terphenyl-d14 92.6 37.0-146 04/25/2023 21:59 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 14
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 3810 1 04/26/2023 00:59 WG2048584
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.76 1 04/30/2023 16:09 WG2051086
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 04/28/2023 13:16 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury 0.000306 0.000200 1 04/30/2023 22:33 WG2051471
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/25/2023 23:58 WG2048081
Arsenic 0.0151 0.0100 1 04/25/2023 23:58 WG2048081
Beryllium ND 0.00200 1 04/25/2023 23:58 WG2048081
Cadmium ND 0.00200 1 04/25/2023 23:58 WG2048081
Chromium ND 0.0100 1 04/25/2023 23:58 WG2048081
Copper ND 0.0100 1 04/25/2023 23:58 WG2048081
Lead ND 0.00600 1 04/25/2023 23:58 WG2048081
Nickel 0.0129 0.0100 1 04/25/2023 23:58 WG2048081
Selenium 0.0189 0.0100 1 04/25/2023 23:58 WG2048081
Silver ND 0.00500 1 04/25/2023 23:58 WG2048081
Thallium ND 0.0100 1 04/25/2023 23:58 WG2048081
Zinc ND 0.0500 1 04/25/2023 23:58 WG2048081
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 04/26/2023 06:46 WG2047755
(S) a,a,a-Trifluorotoluene(FID) 112 78.0-120 04/26/2023 06:46 WG2047755
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 04/24/2023 10:29 WG2047326
Acrolein ND 0.0500 1 04/24/2023 10:29 WG2047326
Acrylonitrile ND 0.0100 1 04/24/2023 10:29 WG2047326
Benzene ND 0.00100 1 04/24/2023 10:29 WG2047326
Bromobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
Bromodichloromethane ND 0.00100 1 04/24/2023 10:29 WG2047326
Bromoform ND 0.00100 1 04/24/2023 10:29 WG2047326
Bromomethane ND 0.00500 1 04/24/2023 10:29 WG2047326
n-Butylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
sec-Butylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
tert-Butylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 14
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 04/24/2023 10:29 WG2047326
Chlorobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
Chlorodibromomethane ND 0.00100 1 04/24/2023 10:29 WG2047326
Chloroethane ND 0.00500 1 04/24/2023 10:29 WG2047326
Chloroform ND 0.00500 1 04/24/2023 10:29 WG2047326
Chloromethane ND 0.00250 1 04/24/2023 10:29 WG2047326
2-Chlorotoluene ND 0.00100 1 04/24/2023 10:29 WG2047326
4-Chlorotoluene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2-Dibromo-3-Chloropropane ND 0.00500 1 04/24/2023 10:29 WG2047326
1,2-Dibromoethane ND 0.00100 1 04/24/2023 10:29 WG2047326
Dibromomethane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2-Dichlorobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,3-Dichlorobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,4-Dichlorobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
Dichlorodifluoromethane ND 0.00500 1 04/24/2023 10:29 WG2047326
1,1-Dichloroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2-Dichloroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1-Dichloroethene ND 0.00100 1 04/24/2023 10:29 WG2047326
cis-1,2-Dichloroethene ND 0.00100 1 04/24/2023 10:29 WG2047326
trans-1,2-Dichloroethene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2-Dichloropropane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1-Dichloropropene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,3-Dichloropropane ND 0.00100 1 04/24/2023 10:29 WG2047326
cis-1,3-Dichloropropene ND 0.00100 1 04/24/2023 10:29 WG2047326
trans-1,3-Dichloropropene ND 0.00100 1 04/24/2023 10:29 WG2047326
2,2-Dichloropropane ND 0.00100 1 04/24/2023 10:29 WG2047326
Di-isopropyl ether ND 0.00100 1 04/24/2023 10:29 WG2047326
Ethylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
Hexachloro-1,3-butadiene ND 0.00100 1 04/24/2023 10:29 WG2047326
Isopropylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
p-Isopropyltoluene ND 0.00100 1 04/24/2023 10:29 WG2047326
2-Butanone (MEK)ND 0.0100 1 04/24/2023 10:29 WG2047326
Methylene Chloride ND 0.00500 1 04/24/2023 10:29 WG2047326
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 04/24/2023 10:29 WG2047326
Methyl tert-butyl ether ND 0.00100 1 04/24/2023 10:29 WG2047326
Naphthalene ND 0.00500 1 04/24/2023 10:29 WG2047326
n-Propylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
Styrene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1,1,2-Tetrachloroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1,2,2-Tetrachloroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
Tetrachloroethene ND 0.00100 1 04/24/2023 10:29 WG2047326
Toluene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2,3-Trichlorobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2,4-Trichlorobenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1,1-Trichloroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
1,1,2-Trichloroethane ND 0.00100 1 04/24/2023 10:29 WG2047326
Trichloroethene ND 0.00100 1 04/24/2023 10:29 WG2047326
Trichlorofluoromethane ND 0.00500 1 04/24/2023 10:29 WG2047326
1,2,3-Trichloropropane ND 0.00250 1 04/24/2023 10:29 WG2047326
1,2,4-Trimethylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,2,3-Trimethylbenzene ND 0.00100 1 04/24/2023 10:29 WG2047326
1,3,5-Trimethylbenzene ND J4 0.00100 1 04/24/2023 10:29 WG2047326
Vinyl chloride ND 0.00100 1 04/24/2023 10:29 WG2047326
Xylenes, Total ND 0.00300 1 04/24/2023 10:29 WG2047326
(S) Toluene-d8 104 80.0-120 04/24/2023 10:29 WG2047326
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 14
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 97.7 77.0-126 04/24/2023 10:29 WG2047326
(S) 1,2-Dichloroethane-d4 105 70.0-130 04/24/2023 10:29 WG2047326
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range ND 0.100 1 04/23/2023 06:49 WG2046978
C28-C40 Oil Range ND 0.100 1 04/23/2023 06:49 WG2046978
(S) o-Terphenyl 91.1 52.0-156 04/23/2023 06:49 WG2046978
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 04/25/2023 03:57 WG2047799
PCB 1221 ND 0.000500 1 04/25/2023 03:57 WG2047799
PCB 1232 ND 0.000500 1 04/25/2023 03:57 WG2047799
PCB 1242 ND 0.000500 1 04/25/2023 03:57 WG2047799
PCB 1248 ND 0.000500 1 04/25/2023 03:57 WG2047799
PCB 1254 ND 0.000500 1 04/25/2023 03:57 WG2047799
PCB 1260 ND 0.000500 1 04/25/2023 03:57 WG2047799
(S) Decachlorobiphenyl 32.7 10.0-128 04/25/2023 03:57 WG2047799
(S) Tetrachloro-m-xylene 91.8 10.0-127 04/25/2023 03:57 WG2047799
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Acenaphthylene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Anthracene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Benzidine ND J4 0.0105 1.05 04/27/2023 20:26 WG2048000
Benzo(a)anthracene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Benzo(b)fluoranthene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Benzo(k)fluoranthene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Benzo(g,h,i)perylene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Benzo(a)pyrene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Bis(2-chlorethoxy)methane ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Bis(2-chloroethyl)ether ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 04/27/2023 20:26 WG2048000
4-Bromophenyl-phenylether ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2-Chloronaphthalene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
4-Chlorophenyl-phenylether ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Chrysene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Dibenz(a,h)anthracene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
1,2-Dichlorobenzene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
1,3-Dichlorobenzene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
1,4-Dichlorobenzene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
3,3-Dichlorobenzidine ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,4-Dinitrotoluene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,6-Dinitrotoluene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Fluoranthene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Fluorene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Hexachlorobenzene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Hexachloro-1,3-butadiene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Hexachlorocyclopentadiene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Hexachloroethane ND 0.0105 1.05 04/27/2023 20:26 WG2048000
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 14
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Isophorone ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Naphthalene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Nitrobenzene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
n-Nitrosodimethylamine ND 0.0105 1.05 04/27/2023 20:26 WG2048000
n-Nitrosodiphenylamine ND 0.0105 1.05 04/27/2023 20:26 WG2048000
n-Nitrosodi-n-propylamine ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Phenanthrene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
Benzylbutyl phthalate ND 0.00315 1.05 04/27/2023 20:26 WG2048000
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 04/27/2023 20:26 WG2048000
Di-n-butyl phthalate ND 0.00315 1.05 04/27/2023 20:26 WG2048000
Diethyl phthalate ND 0.00315 1.05 04/27/2023 20:26 WG2048000
Dimethyl phthalate ND 0.00315 1.05 04/27/2023 20:26 WG2048000
Di-n-octyl phthalate ND 0.00315 1.05 04/27/2023 20:26 WG2048000
Pyrene ND 0.00105 1.05 04/27/2023 20:26 WG2048000
1,2,4-Trichlorobenzene ND 0.0105 1.05 04/27/2023 20:26 WG2048000
4-Chloro-3-methylphenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2-Chlorophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,4-Dichlorophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,4-Dimethylphenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,4-Dinitrophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2-Nitrophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
4-Nitrophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Pentachlorophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
Phenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
2,4,6-Trichlorophenol ND 0.0105 1.05 04/27/2023 20:26 WG2048000
(S) 2-Fluorophenol 33.4 10.0-120 04/27/2023 20:26 WG2048000
(S) Phenol-d5 22.0 10.0-120 04/27/2023 20:26 WG2048000
(S) Nitrobenzene-d5 53.3 10.0-127 04/27/2023 20:26 WG2048000
(S) 2-Fluorobiphenyl 62.6 10.0-130 04/27/2023 20:26 WG2048000
(S) 2,4,6-Tribromophenol 56.2 10.0-155 04/27/2023 20:26 WG2048000
(S) p-Terphenyl-d14 77.6 10.0-128 04/27/2023 20:26 WG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Acenaphthene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Acenaphthylene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Benzo(a)anthracene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Benzo(a)pyrene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Benzo(b)fluoranthene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Benzo(g,h,i)perylene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Benzo(k)fluoranthene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Chrysene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Dibenz(a,h)anthracene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Fluoranthene ND 0.000100 1 04/25/2023 22:16 WG2047984
Fluorene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Naphthalene ND 0.000250 1 04/25/2023 22:16 WG2047984
Phenanthrene ND 0.0000500 1 04/25/2023 22:16 WG2047984
Pyrene ND 0.0000500 1 04/25/2023 22:16 WG2047984
1-Methylnaphthalene ND 0.000250 1 04/25/2023 22:16 WG2047984
2-Methylnaphthalene ND 0.000250 1 04/25/2023 22:16 WG2047984
2-Chloronaphthalene ND 0.000250 1 04/25/2023 22:16 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 14
L1607939
FD-1
Collected date/time: 04/20/23 14:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Nitrobenzene-d5 97.4 31.0-160 04/25/2023 22:16 WG2047984
(S) 2-Fluorobiphenyl 112 48.0-148 04/25/2023 22:16 WG2047984
(S) p-Terphenyl-d14 108 37.0-146 04/25/2023 22:16 WG2047984
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 15
L1607939
FD-4 FILTERED
Collected date/time: 04/20/23 13:05
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.000591 0.000500 1 04/28/2023 13:27 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 04/28/2023 12:32 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/26/2023 00:01 WG2048081
Arsenic 0.0348 0.0100 1 04/26/2023 00:01 WG2048081
Beryllium ND 0.00200 1 04/26/2023 00:01 WG2048081
Cadmium ND 0.00200 1 04/26/2023 00:01 WG2048081
Chromium ND 0.0100 1 04/26/2023 00:01 WG2048081
Copper ND 0.0100 1 04/26/2023 00:01 WG2048081
Lead ND 0.00600 1 04/26/2023 00:01 WG2048081
Nickel ND 0.0100 1 04/26/2023 00:01 WG2048081
Selenium 0.0130 0.0100 1 04/26/2023 00:01 WG2048081
Silver ND 0.00500 1 04/26/2023 00:01 WG2048081
Thallium ND 0.0100 1 04/26/2023 00:01 WG2048081
Zinc ND 0.0500 1 04/26/2023 00:01 WG2048081
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 16
L1607939
FD-3 FILTERED
Collected date/time: 04/20/23 15:30
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 04/28/2023 13:38 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 04/28/2023 12:34 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/26/2023 00:04 WG2048081
Arsenic 0.0206 0.0100 1 04/26/2023 00:04 WG2048081
Beryllium ND 0.00200 1 04/26/2023 00:04 WG2048081
Cadmium ND 0.00200 1 04/26/2023 00:04 WG2048081
Chromium ND 0.0100 1 04/26/2023 00:04 WG2048081
Copper ND 0.0100 1 04/26/2023 00:04 WG2048081
Lead ND 0.00600 1 04/26/2023 00:04 WG2048081
Nickel ND 0.0100 1 04/26/2023 00:04 WG2048081
Selenium ND 0.0100 1 04/26/2023 00:04 WG2048081
Silver ND 0.00500 1 04/26/2023 00:04 WG2048081
Thallium ND 0.0100 1 04/26/2023 00:04 WG2048081
Zinc ND 0.0500 1 04/26/2023 00:04 WG2048081
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 17
L1607939
FD-2 FILTERED
Collected date/time: 04/20/23 16:30
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 04/28/2023 14:00 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 04/28/2023 12:36 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/27/2023 21:21 WG2048082
Arsenic 0.0700 0.0100 1 04/27/2023 21:21 WG2048082
Beryllium ND 0.00200 1 04/27/2023 21:21 WG2048082
Cadmium ND 0.00200 1 04/27/2023 21:21 WG2048082
Chromium ND 0.0100 1 04/27/2023 21:21 WG2048082
Copper ND 0.0100 1 04/27/2023 21:21 WG2048082
Lead ND 0.00600 1 04/27/2023 21:21 WG2048082
Nickel 0.0170 0.0100 1 04/27/2023 21:21 WG2048082
Selenium ND 0.0100 1 04/27/2023 21:21 WG2048082
Silver ND 0.00500 1 04/27/2023 21:21 WG2048082
Thallium ND 0.0100 1 04/27/2023 21:21 WG2048082
Zinc ND 0.0500 1 04/27/2023 21:21 WG2048082
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 18
L1607939
FD-1 FILTERED
Collected date/time: 04/20/23 14:30
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 04/28/2023 14:54 WG2048027
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 04/28/2023 12:38 WG2047887
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/27/2023 21:24 WG2048082
Arsenic 0.0242 B 0.0100 1 04/27/2023 21:24 WG2048082
Beryllium ND 0.00200 1 04/27/2023 21:24 WG2048082
Cadmium ND 0.00200 1 04/27/2023 21:24 WG2048082
Chromium ND 0.0100 1 04/27/2023 21:24 WG2048082
Copper ND 0.0100 1 04/27/2023 21:24 WG2048082
Lead ND 0.00600 1 04/27/2023 21:24 WG2048082
Nickel ND 0.0100 1 04/27/2023 21:24 WG2048082
Selenium ND 0.0100 1 04/27/2023 21:24 WG2048082
Silver ND 0.00500 1 04/27/2023 21:24 WG2048082
Thallium ND 0.0100 1 04/27/2023 21:24 WG2048082
Zinc ND 0.0500 1 04/27/2023 21:24 WG2048082
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 19
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 1030 1 04/26/2023 00:59 WG2048584
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND J3 J6 6.10 1 04/30/2023 16:09 WG2051086
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.000674 0.000500 1 04/27/2023 01:43 WG2048715
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury 0.000336 0.000200 1 05/01/2023 15:34 WG2048783
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/28/2023 22:40 WG2048547
Arsenic 0.0233 0.0100 1 04/28/2023 22:40 WG2048547
Beryllium ND 0.00200 1 04/28/2023 22:40 WG2048547
Cadmium ND 0.00200 1 04/28/2023 22:40 WG2048547
Chromium 0.0204 0.0100 1 04/28/2023 22:40 WG2048547
Copper 0.0383 0.0100 1 04/28/2023 22:40 WG2048547
Lead ND 0.00600 1 04/28/2023 22:40 WG2048547
Nickel 0.0197 0.0100 1 04/28/2023 22:40 WG2048547
Selenium ND 0.0100 1 04/28/2023 22:40 WG2048547
Silver ND 0.00500 1 04/28/2023 22:40 WG2048547
Thallium ND 0.0100 1 04/28/2023 22:40 WG2048547
Zinc ND 0.0500 1 04/28/2023 22:40 WG2048547
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 04/27/2023 06:59 WG2049501
(S) a,a,a-Trifluorotoluene(FID) 109 78.0-120 04/27/2023 06:59 WG2049501
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 04/25/2023 22:05 WG2048606
Acrolein ND 0.0500 1 04/25/2023 22:05 WG2048606
Acrylonitrile ND 0.0100 1 04/25/2023 22:05 WG2048606
Benzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Bromobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Bromodichloromethane ND 0.00100 1 04/25/2023 22:05 WG2048606
Bromoform ND 0.00100 1 04/25/2023 22:05 WG2048606
Bromomethane ND 0.00500 1 04/25/2023 22:05 WG2048606
n-Butylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
sec-Butylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
tert-Butylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 19
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 04/25/2023 22:05 WG2048606
Chlorobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Chlorodibromomethane ND 0.00100 1 04/25/2023 22:05 WG2048606
Chloroethane ND 0.00500 1 04/25/2023 22:05 WG2048606
Chloroform ND 0.00500 1 04/25/2023 22:05 WG2048606
Chloromethane ND 0.00250 1 04/25/2023 22:05 WG2048606
2-Chlorotoluene ND 0.00100 1 04/25/2023 22:05 WG2048606
4-Chlorotoluene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2-Dibromo-3-Chloropropane ND 0.00500 1 04/25/2023 22:05 WG2048606
1,2-Dibromoethane ND 0.00100 1 04/25/2023 22:05 WG2048606
Dibromomethane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2-Dichlorobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,3-Dichlorobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,4-Dichlorobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Dichlorodifluoromethane ND 0.00500 1 04/25/2023 22:05 WG2048606
1,1-Dichloroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2-Dichloroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1-Dichloroethene ND 0.00100 1 04/25/2023 22:05 WG2048606
cis-1,2-Dichloroethene ND 0.00100 1 04/25/2023 22:05 WG2048606
trans-1,2-Dichloroethene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2-Dichloropropane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1-Dichloropropene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,3-Dichloropropane ND 0.00100 1 04/25/2023 22:05 WG2048606
cis-1,3-Dichloropropene ND 0.00100 1 04/25/2023 22:05 WG2048606
trans-1,3-Dichloropropene ND 0.00100 1 04/25/2023 22:05 WG2048606
2,2-Dichloropropane ND 0.00100 1 04/25/2023 22:05 WG2048606
Di-isopropyl ether ND 0.00100 1 04/25/2023 22:05 WG2048606
Ethylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Hexachloro-1,3-butadiene ND 0.00100 1 04/25/2023 22:05 WG2048606
Isopropylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
p-Isopropyltoluene ND 0.00100 1 04/25/2023 22:05 WG2048606
2-Butanone (MEK)ND 0.0100 1 04/25/2023 22:05 WG2048606
Methylene Chloride ND 0.00500 1 04/25/2023 22:05 WG2048606
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 04/25/2023 22:05 WG2048606
Methyl tert-butyl ether ND 0.00100 1 04/25/2023 22:05 WG2048606
Naphthalene ND 0.00500 1 04/25/2023 22:05 WG2048606
n-Propylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Styrene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1,1,2-Tetrachloroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1,2,2-Tetrachloroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
Tetrachloroethene ND 0.00100 1 04/25/2023 22:05 WG2048606
Toluene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2,3-Trichlorobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2,4-Trichlorobenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1,1-Trichloroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
1,1,2-Trichloroethane ND 0.00100 1 04/25/2023 22:05 WG2048606
Trichloroethene ND 0.00100 1 04/25/2023 22:05 WG2048606
Trichlorofluoromethane ND 0.00500 1 04/25/2023 22:05 WG2048606
1,2,3-Trichloropropane ND 0.00250 1 04/25/2023 22:05 WG2048606
1,2,4-Trimethylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,2,3-Trimethylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
1,3,5-Trimethylbenzene ND 0.00100 1 04/25/2023 22:05 WG2048606
Vinyl chloride ND 0.00100 1 04/25/2023 22:05 WG2048606
Xylenes, Total ND 0.00300 1 04/25/2023 22:05 WG2048606
(S) Toluene-d8 111 80.0-120 04/25/2023 22:05 WG2048606
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 19
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 102 77.0-126 04/25/2023 22:05 WG2048606
(S) 1,2-Dichloroethane-d4 108 70.0-130 04/25/2023 22:05 WG2048606
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range 0.449 0.100 1 04/28/2023 18:04 WG2049589
C28-C40 Oil Range 0.708 0.100 1 04/28/2023 18:04 WG2049589
(S) o-Terphenyl 120 52.0-156 04/28/2023 18:04 WG2049589
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 04/26/2023 01:25 WG2047970
PCB 1221 ND 0.000500 1 04/26/2023 01:25 WG2047970
PCB 1232 ND 0.000500 1 04/26/2023 01:25 WG2047970
PCB 1242 ND 0.000500 1 04/26/2023 01:25 WG2047970
PCB 1248 ND 0.000500 1 04/26/2023 01:25 WG2047970
PCB 1254 ND 0.000500 1 04/26/2023 01:25 WG2047970
PCB 1260 ND J3 0.000500 1 04/26/2023 01:25 WG2047970
(S) Decachlorobiphenyl 17.3 10.0-128 04/26/2023 01:25 WG2047970
(S) Tetrachloro-m-xylene 42.5 10.0-127 04/26/2023 01:25 WG2047970
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 04/26/2023 10:58 WG2048428
Acenaphthylene ND 0.00100 1 04/26/2023 10:58 WG2048428
Anthracene ND J3 0.00100 1 04/26/2023 10:58 WG2048428
Benzidine ND J4 J6 0.0100 1 04/26/2023 10:58 WG2048428
Benzo(a)anthracene ND J3 J6 0.00100 1 04/26/2023 10:58 WG2048428
Benzo(b)fluoranthene ND 0.00100 1 04/26/2023 10:58 WG2048428
Benzo(k)fluoranthene ND J6 0.00100 1 04/26/2023 10:58 WG2048428
Benzo(g,h,i)perylene ND 0.00100 1 04/26/2023 10:58 WG2048428
Benzo(a)pyrene ND J3 J6 0.00100 1 04/26/2023 10:58 WG2048428
Bis(2-chlorethoxy)methane ND 0.0100 1 04/26/2023 10:58 WG2048428
Bis(2-chloroethyl)ether ND 0.0100 1 04/26/2023 10:58 WG2048428
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 04/26/2023 10:58 WG2048428
4-Bromophenyl-phenylether ND 0.0100 1 04/26/2023 10:58 WG2048428
2-Chloronaphthalene ND 0.00100 1 04/26/2023 10:58 WG2048428
4-Chlorophenyl-phenylether ND 0.0100 1 04/26/2023 10:58 WG2048428
Chrysene ND 0.00100 1 04/26/2023 10:58 WG2048428
Dibenz(a,h)anthracene ND 0.00100 1 04/26/2023 10:58 WG2048428
1,2-Dichlorobenzene ND 0.0100 1 04/26/2023 10:58 WG2048428
1,3-Dichlorobenzene ND 0.0100 1 04/26/2023 10:58 WG2048428
1,4-Dichlorobenzene ND 0.0100 1 04/26/2023 10:58 WG2048428
3,3-Dichlorobenzidine ND J6 0.0100 1 04/26/2023 10:58 WG2048428
2,4-Dinitrotoluene ND 0.0100 1 04/26/2023 10:58 WG2048428
2,6-Dinitrotoluene ND 0.0100 1 04/26/2023 10:58 WG2048428
Fluoranthene ND 0.00100 1 04/26/2023 10:58 WG2048428
Fluorene ND 0.00100 1 04/26/2023 10:58 WG2048428
Hexachlorobenzene ND J3 J6 0.00100 1 04/26/2023 10:58 WG2048428
Hexachloro-1,3-butadiene ND 0.0100 1 04/26/2023 10:58 WG2048428
Hexachlorocyclopentadiene ND 0.0100 1 04/26/2023 10:58 WG2048428
Hexachloroethane ND 0.0100 1 04/26/2023 10:58 WG2048428
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 19
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Indeno(1,2,3-cd)pyrene ND J6 0.00100 1 04/26/2023 10:58 WG2048428
Isophorone ND 0.0100 1 04/26/2023 10:58 WG2048428
Naphthalene ND 0.00100 1 04/26/2023 10:58 WG2048428
Nitrobenzene ND 0.0100 1 04/26/2023 10:58 WG2048428
n-Nitrosodimethylamine ND 0.0100 1 04/26/2023 10:58 WG2048428
n-Nitrosodiphenylamine ND 0.0100 1 04/26/2023 10:58 WG2048428
n-Nitrosodi-n-propylamine ND 0.0100 1 04/26/2023 10:58 WG2048428
Phenanthrene ND 0.00100 1 04/26/2023 10:58 WG2048428
Benzylbutyl phthalate ND 0.00300 1 04/26/2023 10:58 WG2048428
Bis(2-ethylhexyl)phthalate ND J3 0.00300 1 04/26/2023 10:58 WG2048428
Di-n-butyl phthalate ND 0.00300 1 04/26/2023 10:58 WG2048428
Diethyl phthalate ND 0.00300 1 04/26/2023 10:58 WG2048428
Dimethyl phthalate ND 0.00300 1 04/26/2023 10:58 WG2048428
Di-n-octyl phthalate ND J3 0.00300 1 04/26/2023 10:58 WG2048428
Pyrene ND 0.00100 1 04/26/2023 10:58 WG2048428
1,2,4-Trichlorobenzene ND 0.0100 1 04/26/2023 10:58 WG2048428
4-Chloro-3-methylphenol ND 0.0100 1 04/26/2023 10:58 WG2048428
2-Chlorophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
2,4-Dichlorophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
2,4-Dimethylphenol ND J3 J6 0.0100 1 04/26/2023 10:58 WG2048428
4,6-Dinitro-2-methylphenol ND 0.0100 1 04/26/2023 10:58 WG2048428
2,4-Dinitrophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
2-Nitrophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
4-Nitrophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
Pentachlorophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
Phenol ND 0.0100 1 04/26/2023 10:58 WG2048428
2,4,6-Trichlorophenol ND 0.0100 1 04/26/2023 10:58 WG2048428
(S) 2-Fluorophenol 24.9 10.0-120 04/26/2023 10:58 WG2048428
(S) Phenol-d5 17.4 10.0-120 04/26/2023 10:58 WG2048428
(S) Nitrobenzene-d5 51.6 10.0-127 04/26/2023 10:58 WG2048428
(S) 2-Fluorobiphenyl 57.8 10.0-130 04/26/2023 10:58 WG2048428
(S) 2,4,6-Tribromophenol 55.0 10.0-155 04/26/2023 10:58 WG2048428
(S) p-Terphenyl-d14 64.1 10.0-128 04/26/2023 10:58 WG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Acenaphthene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Acenaphthylene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Benzo(a)anthracene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Benzo(a)pyrene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Benzo(b)fluoranthene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Benzo(g,h,i)perylene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Benzo(k)fluoranthene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Chrysene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Dibenz(a,h)anthracene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Fluoranthene ND J3 0.000100 1 04/27/2023 00:58 WG2048874
Fluorene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Indeno(1,2,3-cd)pyrene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Naphthalene ND J3 0.000250 1 04/27/2023 00:58 WG2048874
Phenanthrene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
Pyrene ND J3 0.0000500 1 04/27/2023 00:58 WG2048874
1-Methylnaphthalene ND J3 0.000250 1 04/27/2023 00:58 WG2048874
2-Methylnaphthalene ND J3 0.000250 1 04/27/2023 00:58 WG2048874
2-Chloronaphthalene ND J3 0.000250 1 04/27/2023 00:58 WG2048874
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 19
L1607939
FD-5
Collected date/time: 04/20/23 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Nitrobenzene-d5 117 31.0-160 04/27/2023 00:58 WG2048874
(S) 2-Fluorobiphenyl 96.5 48.0-148 04/27/2023 00:58 WG2048874
(S) p-Terphenyl-d14 96.0 37.0-146 04/27/2023 00:58 WG2048874
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 20
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 1080 1 04/26/2023 00:59 WG2048584
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.58 1 04/30/2023 16:09 WG2051086
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.00181 0.000500 1 04/27/2023 02:06 WG2048715
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury 0.000271 0.000200 1 05/01/2023 16:19 WG2048783
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/28/2023 22:50 WG2048547
Arsenic 0.0241 0.0100 1 04/28/2023 22:50 WG2048547
Beryllium ND 0.00200 1 04/28/2023 22:50 WG2048547
Cadmium ND 0.00200 1 04/28/2023 22:50 WG2048547
Chromium ND 0.0100 1 04/28/2023 22:50 WG2048547
Copper 0.0139 0.0100 1 04/28/2023 22:50 WG2048547
Lead ND 0.00600 1 04/28/2023 22:50 WG2048547
Nickel 0.0118 0.0100 1 04/28/2023 22:50 WG2048547
Selenium ND 0.0100 1 04/28/2023 22:50 WG2048547
Silver ND 0.00500 1 04/28/2023 22:50 WG2048547
Thallium ND 0.0100 1 04/28/2023 22:50 WG2048547
Zinc ND 0.0500 1 04/28/2023 22:50 WG2048547
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 04/27/2023 14:24 WG2049550
(S) a,a,a-Trifluorotoluene(FID) 107 78.0-120 04/27/2023 14:24 WG2049550
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 04/25/2023 22:26 WG2048606
Acrolein ND 0.0500 1 04/25/2023 22:26 WG2048606
Acrylonitrile ND 0.0100 1 04/25/2023 22:26 WG2048606
Benzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Bromobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Bromodichloromethane ND 0.00100 1 04/25/2023 22:26 WG2048606
Bromoform ND 0.00100 1 04/25/2023 22:26 WG2048606
Bromomethane ND 0.00500 1 04/25/2023 22:26 WG2048606
n-Butylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
sec-Butylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
tert-Butylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 20
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 04/25/2023 22:26 WG2048606
Chlorobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Chlorodibromomethane ND 0.00100 1 04/25/2023 22:26 WG2048606
Chloroethane ND 0.00500 1 04/25/2023 22:26 WG2048606
Chloroform ND 0.00500 1 04/25/2023 22:26 WG2048606
Chloromethane ND 0.00250 1 04/25/2023 22:26 WG2048606
2-Chlorotoluene ND 0.00100 1 04/25/2023 22:26 WG2048606
4-Chlorotoluene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2-Dibromo-3-Chloropropane ND 0.00500 1 04/25/2023 22:26 WG2048606
1,2-Dibromoethane ND 0.00100 1 04/25/2023 22:26 WG2048606
Dibromomethane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2-Dichlorobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,3-Dichlorobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,4-Dichlorobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Dichlorodifluoromethane ND 0.00500 1 04/25/2023 22:26 WG2048606
1,1-Dichloroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2-Dichloroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1-Dichloroethene ND 0.00100 1 04/25/2023 22:26 WG2048606
cis-1,2-Dichloroethene ND 0.00100 1 04/25/2023 22:26 WG2048606
trans-1,2-Dichloroethene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2-Dichloropropane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1-Dichloropropene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,3-Dichloropropane ND 0.00100 1 04/25/2023 22:26 WG2048606
cis-1,3-Dichloropropene ND 0.00100 1 04/25/2023 22:26 WG2048606
trans-1,3-Dichloropropene ND 0.00100 1 04/25/2023 22:26 WG2048606
2,2-Dichloropropane ND 0.00100 1 04/25/2023 22:26 WG2048606
Di-isopropyl ether ND 0.00100 1 04/25/2023 22:26 WG2048606
Ethylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Hexachloro-1,3-butadiene ND 0.00100 1 04/25/2023 22:26 WG2048606
Isopropylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
p-Isopropyltoluene ND 0.00100 1 04/25/2023 22:26 WG2048606
2-Butanone (MEK)ND 0.0100 1 04/25/2023 22:26 WG2048606
Methylene Chloride ND 0.00500 1 04/25/2023 22:26 WG2048606
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 04/25/2023 22:26 WG2048606
Methyl tert-butyl ether ND 0.00100 1 04/25/2023 22:26 WG2048606
Naphthalene ND 0.00500 1 04/25/2023 22:26 WG2048606
n-Propylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Styrene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1,1,2-Tetrachloroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1,2,2-Tetrachloroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
Tetrachloroethene ND 0.00100 1 04/25/2023 22:26 WG2048606
Toluene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2,3-Trichlorobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2,4-Trichlorobenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1,1-Trichloroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
1,1,2-Trichloroethane ND 0.00100 1 04/25/2023 22:26 WG2048606
Trichloroethene ND 0.00100 1 04/25/2023 22:26 WG2048606
Trichlorofluoromethane ND 0.00500 1 04/25/2023 22:26 WG2048606
1,2,3-Trichloropropane ND 0.00250 1 04/25/2023 22:26 WG2048606
1,2,4-Trimethylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,2,3-Trimethylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
1,3,5-Trimethylbenzene ND 0.00100 1 04/25/2023 22:26 WG2048606
Vinyl chloride ND 0.00100 1 04/25/2023 22:26 WG2048606
Xylenes, Total ND 0.00300 1 04/25/2023 22:26 WG2048606
(S) Toluene-d8 110 80.0-120 04/25/2023 22:26 WG2048606
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 20
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 103 77.0-126 04/25/2023 22:26 WG2048606
(S) 1,2-Dichloroethane-d4 110 70.0-130 04/25/2023 22:26 WG2048606
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range 0.412 0.100 1 04/27/2023 22:58 WG2049589
C28-C40 Oil Range 0.286 B 0.100 1 04/27/2023 22:58 WG2049589
(S) o-Terphenyl 117 52.0-156 04/27/2023 22:58 WG2049589
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 04/26/2023 01:56 WG2047970
PCB 1221 ND 0.000500 1 04/26/2023 01:56 WG2047970
PCB 1232 ND 0.000500 1 04/26/2023 01:56 WG2047970
PCB 1242 ND 0.000500 1 04/26/2023 01:56 WG2047970
PCB 1248 ND 0.000500 1 04/26/2023 01:56 WG2047970
PCB 1254 ND 0.000500 1 04/26/2023 01:56 WG2047970
PCB 1260 ND 0.000500 1 04/26/2023 01:56 WG2047970
(S) Decachlorobiphenyl 11.0 10.0-128 04/26/2023 01:56 WG2047970
(S) Tetrachloro-m-xylene 37.6 10.0-127 04/26/2023 01:56 WG2047970
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 04/26/2023 02:41 WG2048428
Acenaphthylene ND 0.00100 1 04/26/2023 02:41 WG2048428
Anthracene ND 0.00100 1 04/26/2023 02:41 WG2048428
Benzidine ND J4 0.0100 1 04/26/2023 02:41 WG2048428
Benzo(a)anthracene ND 0.00100 1 04/26/2023 02:41 WG2048428
Benzo(b)fluoranthene ND 0.00100 1 04/26/2023 02:41 WG2048428
Benzo(k)fluoranthene ND 0.00100 1 04/26/2023 02:41 WG2048428
Benzo(g,h,i)perylene ND 0.00100 1 04/26/2023 02:41 WG2048428
Benzo(a)pyrene ND 0.00100 1 04/26/2023 02:41 WG2048428
Bis(2-chlorethoxy)methane ND 0.0100 1 04/26/2023 02:41 WG2048428
Bis(2-chloroethyl)ether ND 0.0100 1 04/26/2023 02:41 WG2048428
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 04/26/2023 02:41 WG2048428
4-Bromophenyl-phenylether ND 0.0100 1 04/26/2023 02:41 WG2048428
2-Chloronaphthalene ND 0.00100 1 04/26/2023 02:41 WG2048428
4-Chlorophenyl-phenylether ND 0.0100 1 04/26/2023 02:41 WG2048428
Chrysene ND 0.00100 1 04/26/2023 02:41 WG2048428
Dibenz(a,h)anthracene ND 0.00100 1 04/26/2023 02:41 WG2048428
1,2-Dichlorobenzene ND 0.0100 1 04/26/2023 02:41 WG2048428
1,3-Dichlorobenzene ND 0.0100 1 04/26/2023 02:41 WG2048428
1,4-Dichlorobenzene ND 0.0100 1 04/26/2023 02:41 WG2048428
3,3-Dichlorobenzidine ND 0.0100 1 04/26/2023 02:41 WG2048428
2,4-Dinitrotoluene ND 0.0100 1 04/26/2023 02:41 WG2048428
2,6-Dinitrotoluene ND 0.0100 1 04/26/2023 02:41 WG2048428
Fluoranthene ND 0.00100 1 04/26/2023 02:41 WG2048428
Fluorene ND 0.00100 1 04/26/2023 02:41 WG2048428
Hexachlorobenzene ND 0.00100 1 04/26/2023 02:41 WG2048428
Hexachloro-1,3-butadiene ND 0.0100 1 04/26/2023 02:41 WG2048428
Hexachlorocyclopentadiene ND 0.0100 1 04/26/2023 02:41 WG2048428
Hexachloroethane ND 0.0100 1 04/26/2023 02:41 WG2048428
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 20
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Indeno(1,2,3-cd)pyrene ND 0.00100 1 04/26/2023 02:41 WG2048428
Isophorone ND 0.0100 1 04/26/2023 02:41 WG2048428
Naphthalene ND 0.00100 1 04/26/2023 02:41 WG2048428
Nitrobenzene ND 0.0100 1 04/26/2023 02:41 WG2048428
n-Nitrosodimethylamine ND 0.0100 1 04/26/2023 02:41 WG2048428
n-Nitrosodiphenylamine ND 0.0100 1 04/26/2023 02:41 WG2048428
n-Nitrosodi-n-propylamine ND 0.0100 1 04/26/2023 02:41 WG2048428
Phenanthrene ND 0.00100 1 04/26/2023 02:41 WG2048428
Benzylbutyl phthalate ND 0.00300 1 04/26/2023 02:41 WG2048428
Bis(2-ethylhexyl)phthalate ND 0.00300 1 04/26/2023 02:41 WG2048428
Di-n-butyl phthalate ND 0.00300 1 04/26/2023 02:41 WG2048428
Diethyl phthalate ND 0.00300 1 04/26/2023 02:41 WG2048428
Dimethyl phthalate ND 0.00300 1 04/26/2023 02:41 WG2048428
Di-n-octyl phthalate ND 0.00300 1 04/26/2023 02:41 WG2048428
Pyrene ND 0.00100 1 04/26/2023 02:41 WG2048428
1,2,4-Trichlorobenzene ND 0.0100 1 04/26/2023 02:41 WG2048428
4-Chloro-3-methylphenol ND 0.0100 1 04/26/2023 02:41 WG2048428
2-Chlorophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
2,4-Dichlorophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
2,4-Dimethylphenol ND 0.0100 1 04/26/2023 02:41 WG2048428
4,6-Dinitro-2-methylphenol ND 0.0100 1 04/26/2023 02:41 WG2048428
2,4-Dinitrophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
2-Nitrophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
4-Nitrophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
Pentachlorophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
Phenol ND 0.0100 1 04/26/2023 02:41 WG2048428
2,4,6-Trichlorophenol ND 0.0100 1 04/26/2023 02:41 WG2048428
(S) 2-Fluorophenol 22.1 10.0-120 04/26/2023 02:41 WG2048428
(S) Phenol-d5 15.4 10.0-120 04/26/2023 02:41 WG2048428
(S) Nitrobenzene-d5 47.7 10.0-127 04/26/2023 02:41 WG2048428
(S) 2-Fluorobiphenyl 54.5 10.0-130 04/26/2023 02:41 WG2048428
(S) 2,4,6-Tribromophenol 44.1 10.0-155 04/26/2023 02:41 WG2048428
(S) p-Terphenyl-d14 49.1 10.0-128 04/26/2023 02:41 WG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Acenaphthene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Acenaphthylene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Benzo(a)anthracene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Benzo(a)pyrene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Benzo(b)fluoranthene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Benzo(g,h,i)perylene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Benzo(k)fluoranthene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Chrysene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Dibenz(a,h)anthracene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Fluoranthene ND 0.000100 1 04/27/2023 01:50 WG2048874
Fluorene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Naphthalene ND 0.000250 1 04/27/2023 01:50 WG2048874
Phenanthrene ND 0.0000500 1 04/27/2023 01:50 WG2048874
Pyrene ND 0.0000500 1 04/27/2023 01:50 WG2048874
1-Methylnaphthalene ND 0.000250 1 04/27/2023 01:50 WG2048874
2-Methylnaphthalene ND 0.000250 1 04/27/2023 01:50 WG2048874
2-Chloronaphthalene ND 0.000250 1 04/27/2023 01:50 WG2048874
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 20
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Nitrobenzene-d5 123 31.0-160 04/27/2023 01:50 WG2048874
(S) 2-Fluorobiphenyl 103 48.0-148 04/27/2023 01:50 WG2048874
(S) p-Terphenyl-d14 99.5 37.0-146 04/27/2023 01:50 WG2048874
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 21
L1607939
FD-5 FILTERED
Collected date/time: 04/20/23 11:00
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.000716 0.000500 1 04/27/2023 02:22 WG2048715
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 05/01/2023 16:26 WG2048783
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/28/2023 22:53 WG2048547
Arsenic 0.0253 0.0100 1 04/28/2023 22:53 WG2048547
Beryllium ND 0.00200 1 04/28/2023 22:53 WG2048547
Cadmium ND 0.00200 1 04/28/2023 22:53 WG2048547
Chromium ND 0.0100 1 04/28/2023 22:53 WG2048547
Copper ND 0.0100 1 04/28/2023 22:53 WG2048547
Lead ND 0.00600 1 04/28/2023 22:53 WG2048547
Nickel ND 0.0100 1 04/28/2023 22:53 WG2048547
Selenium ND 0.0100 1 04/28/2023 22:53 WG2048547
Silver ND 0.00500 1 04/28/2023 22:53 WG2048547
Thallium ND 0.0100 1 04/28/2023 22:53 WG2048547
Zinc ND 0.0500 1 04/28/2023 22:53 WG2048547
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 22
L1607939
DUP-1
Collected date/time: 04/20/23 00:00
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.000932 0.000500 1 04/27/2023 02:29 WG2048715
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 05/01/2023 16:28 WG2048783
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 04/28/2023 22:56 WG2048547
Arsenic 0.0218 0.0100 1 04/28/2023 22:56 WG2048547
Beryllium ND 0.00200 1 04/28/2023 22:56 WG2048547
Cadmium ND 0.00200 1 04/28/2023 22:56 WG2048547
Chromium ND 0.0100 1 04/28/2023 22:56 WG2048547
Copper ND 0.0100 1 04/28/2023 22:56 WG2048547
Lead ND 0.00600 1 04/28/2023 22:56 WG2048547
Nickel ND 0.0100 1 04/28/2023 22:56 WG2048547
Selenium ND 0.0100 1 04/28/2023 22:56 WG2048547
Silver ND 0.00500 1 04/28/2023 22:56 WG2048547
Thallium ND 0.0100 1 04/28/2023 22:56 WG2048547
Zinc ND 0.0500 1 04/28/2023 22:56 WG2048547
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048584
Total Solids by Method 2540 B-2015 L1607939-11,12,13,14,19,20
Method Blank (MB)
(MB) R3917862-1 04/26/23 00:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Total Solids 1.00
L1607092-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1607092-01 04/26/23 00:59 • (DUP) R3917862-3 04/26/23 00:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Total Solids 246 259 1 5.15 J3 5
Laboratory Control Sample (LCS)
(LCS) R3917862-2 04/26/23 00:59
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Total Solids 9500 9440 99.4 92.5-108
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048861
Total Solids by Method 2540 G-2011 L1607939-02,03,04,05,06,07,08,09,10
Method Blank (MB)
(MB) R3917916-1 04/26/23 10:37
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1607939-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1607939-04 04/26/23 10:37 • (DUP) R3917916-3 04/26/23 10:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 83.3 82.8 1 0.648 10
Laboratory Control Sample (LCS)
(LCS) R3917916-2 04/26/23 10:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2053502
Total Solids by Method 2540 G-2011 L1607939-01
Method Blank (MB)
(MB) R3920780-1 05/03/23 15:57
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1607939-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1607939-01 05/03/23 15:57 • (DUP) R3920780-3 05/03/23 15:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 82.5 85.7 1 3.75 10
Laboratory Control Sample (LCS)
(LCS) R3920780-2 05/03/23 15:57
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2050781
Wet Chemistry by Method 1664A L1607939-11,12
Method Blank (MB)
(MB) R3918937-1 04/28/23 22:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3918937-2 04/28/23 22:12 • (LCSD) R3918937-3 04/28/23 22:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 35.1 37.4 87.8 93.5 78.0-114 6.34 20
L1606865-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1606865-01 04/28/23 22:12 • (MS) R3918937-4 04/28/23 22:12
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr) 40.0 ND 31.4 75.5 1 78.0-114 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2051086
Wet Chemistry by Method 1664A L1607939-13,14,19,20
Method Blank (MB)
(MB) R3919193-1 04/30/23 16:09
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3919193-2 04/30/23 16:09 • (LCSD) R3919193-3 04/30/23 16:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 35.2 35.7 88.0 89.3 78.0-114 1.41 20
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/30/23 16:09 • (MS) R3919193-4 04/30/23 16:09 • (MSD) R3919193-5 04/30/23 16:09
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 ND 16.0 32.5 39.9 81.2 1 78.0-114 J6 J3 68.1 18
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048027
Wet Chemistry by Method 3500Cr C-2011 L1607939-11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R3918905-1 04/28/23 10:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Hexavalent Chromium U 0.000150 0.000500
L1607742-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1607742-01 04/28/23 10:54 • (DUP) R3918905-3 04/28/23 11:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND 0.000785 1 200 P1 20
L1607939-16 Original Sample (OS) • Duplicate (DUP)
(OS) L1607939-16 04/28/23 13:38 • (DUP) R3918905-5 04/28/23 13:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3918905-2 04/28/23 10:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00200 0.00192 96.0 90.0-110
L1607939-13 Original Sample (OS) • Matrix Spike (MS)
(OS) L1607939-13 04/28/23 12:54 • (MS) R3918905-4 04/28/23 13:05
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Hexavalent Chromium 0.0500 ND 0.0487 96.7 1 90.0-110
L1607939-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-17 04/28/23 14:00 • (MS) R3918905-6 04/28/23 14:11 • (MSD) R3918905-7 04/28/23 14:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexavalent Chromium 0.0500 ND 0.0510 0.0504 102 101 1 90.0-110 1.31 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048715
Wet Chemistry by Method 3500Cr C-2011 L1607939-19,20,21,22
Method Blank (MB)
(MB) R3917870-1 04/27/23 01:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Hexavalent Chromium U 0.000150 0.000500
L1607939-20 Original Sample (OS) • Duplicate (DUP)
(OS) L1607939-20 04/27/23 02:06 • (DUP) R3917870-5 04/27/23 02:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00181 0.00182 1 0.247 20
L1608357-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1608357-01 04/27/23 04:02 • (DUP) R3917870-6 04/27/23 04:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3917870-2 04/27/23 01:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00200 0.00201 100 90.0-110
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/27/23 01:43 • (MS) R3917870-3 04/27/23 01:51 • (MSD) R3917870-4 04/27/23 01:59
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexavalent Chromium 0.0500 0.000674 0.0493 0.0499 97.2 98.5 1 90.0-110 1.29 20
L1609174-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1609174-01 04/27/23 05:12 • (MS) R3917870-7 04/27/23 05:19
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Hexavalent Chromium 0.0500 ND 0.0489 97.7 1 90.0-110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048733
Wet Chemistry by Method 7199 L1607939-02,03,04,05,06,07,08,09,10
Method Blank (MB)
(MB) R3918910-1 04/28/23 15:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1607994-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1607994-01 04/28/23 16:28 • (DUP) R3918910-3 04/28/23 16:33
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
L1608097-47 Original Sample (OS) • Duplicate (DUP)
(OS) L1608097-47 04/28/23 16:54 • (DUP) R3918910-4 04/28/23 16:59
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3918910-2 04/28/23 15:16
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 8.61 86.1 80.0-120
L1608097-48 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608097-48 04/28/23 17:15 • (MS) R3918910-5 04/28/23 17:20 • (MSD) R3918910-6 04/28/23 17:25
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 23.8 ND 21.5 23.2 90.2 97.7 1 75.0-125 7.92 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048733
Wet Chemistry by Method 7199 L1607939-02,03,04,05,06,07,08,09,10
L1608097-48 Original Sample (OS) • Matrix Spike (MS)
(OS) L1608097-48 04/28/23 17:15 • (MS) R3918910-8 04/28/23 17:31
Spike Amount
(dry)
Original Result
(dry)MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 774 ND 1340 174 50 75.0-125 J5
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052786
Wet Chemistry by Method 7199 L1607939-01
Method Blank (MB)
(MB) R3920469-1 05/03/23 11:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1610752-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1610752-01 05/03/23 12:59 • (DUP) R3920469-7 05/03/23 13:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
L1610752-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1610752-03 05/03/23 13:25 • (DUP) R3920469-8 05/03/23 13:31
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3920469-2 05/03/23 11:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 10.5 105 80.0-120
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/03/23 11:26 • (MS) R3920469-3 05/03/23 11:31 • (MSD) R3920469-4 05/03/23 11:36
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 25.5 2.04 24.7 26.7 88.4 96.4 1 75.0-125 7.93 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052786
Wet Chemistry by Method 7199 L1607939-01
L1607939-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1607939-01 05/03/23 11:26 • (MS) R3920469-5 05/03/23 11:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 824 2.04 812 98.6 50 75.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047887
Mercury by Method 7470A L1607939-11,12,13,15,16,17,18
Method Blank (MB)
(MB) R3918721-1 04/28/23 12:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3918721-2 04/28/23 12:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00265 88.3 80.0-120
L1607895-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607895-01 04/28/23 12:09 • (MS) R3918721-3 04/28/23 12:11 • (MSD) R3918721-4 04/28/23 12:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00273 0.00260 91.2 86.7 1 75.0-125 4.98 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048783
Mercury by Method 7470A L1607939-19,20,21,22
Method Blank (MB)
(MB) R3919622-3 05/01/23 16:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3919622-4 05/01/23 16:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00336 112 80.0-120
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 05/01/23 15:34 • (MS) R3919622-1 05/01/23 15:37 • (MSD) R3919622-2 05/01/23 15:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 0.000336 0.00337 0.00341 101 102 1 75.0-125 1.17 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2051471
Mercury by Method 7470A L1607939-14
Method Blank (MB)
(MB) R3919244-1 04/30/23 22:19
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3919244-2 04/30/23 22:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00339 113 80.0-120
L1608480-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608480-02 04/30/23 22:23 • (MS) R3919244-3 04/30/23 22:25 • (MSD) R3919244-4 04/30/23 22:27
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00348 0.00341 116 114 1 75.0-125 2.26 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048765
Mercury by Method 7471A L1607939-02,03,10
Method Blank (MB)
(MB) R3918889-1 04/28/23 15:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3918889-2 04/28/23 15:51
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.474 94.7 80.0-120
L1607518-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607518-01 04/28/23 15:53 • (MS) R3918889-3 04/28/23 15:56 • (MSD) R3918889-4 04/28/23 15:58
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 ND 0.555 0.542 106 104 1 75.0-125 2.28 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048768
Mercury by Method 7471A L1607939-04,05,06,07,08,09
Method Blank (MB)
(MB) R3918728-1 04/28/23 12:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3918728-2 04/28/23 12:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.469 93.8 80.0-120
L1607939-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-04 04/28/23 12:09 • (MS) R3918728-3 04/28/23 12:12 • (MSD) R3918728-4 04/28/23 12:14
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.600 ND 0.550 0.616 91.6 103 1 75.0-125 11.4 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2053230
Mercury by Method 7471A L1607939-01
Method Blank (MB)
(MB) R3920809-1 05/04/23 09:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3920809-2 05/04/23 09:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.511 102 80.0-120
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/04/23 09:24 • (MS) R3920809-3 05/04/23 09:26 • (MSD) R3920809-4 05/04/23 09:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.606 ND 0.622 0.529 97.6 83.0 1 75.0-125 16.1 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048081
Metals (ICP) by Method 6010B L1607939-11,12,13,14,15,16
Method Blank (MB)
(MB) R3917347-1 04/25/23 22:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic U 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3917347-2 04/25/23 22:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.993 99.3 80.0-120
Arsenic 1.00 0.964 96.4 80.0-120
Beryllium 1.00 1.03 103 80.0-120
Cadmium 1.00 1.02 102 80.0-120
Chromium 1.00 1.02 102 80.0-120
Copper 1.00 0.961 96.1 80.0-120
Lead 1.00 1.02 102 80.0-120
Nickel 1.00 1.02 102 80.0-120
Selenium 1.00 0.996 99.6 80.0-120
Silver 0.200 0.180 90.1 80.0-120
Thallium 1.00 1.02 102 80.0-120
Zinc 1.00 1.02 102 80.0-120
L1607764-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607764-05 04/25/23 22:46 • (MS) R3917347-4 04/25/23 22:53 • (MSD) R3917347-5 04/25/23 22:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 0.926 1.01 86.0 94.7 10 75.0-125 8.97 20
Arsenic 1.00 ND 0.719 0.666 71.9 66.6 10 75.0-125 J6 J6 7.69 20
Beryllium 1.00 0.367 1.19 1.18 82.6 81.0 10 75.0-125 1.29 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048081
Metals (ICP) by Method 6010B L1607939-11,12,13,14,15,16
L1607764-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607764-05 04/25/23 22:46 • (MS) R3917347-4 04/25/23 22:53 • (MSD) R3917347-5 04/25/23 22:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Cadmium 1.00 2.97 3.89 3.89 92.2 92.8 10 75.0-125 0.150 20
Chromium 1.00 0.183 0.940 0.922 75.7 73.8 10 75.0-125 J6 1.95 20
Copper 1.00 65.6 67.9 67.9 232 226 10 75.0-125 V V 0.0748 20
Lead 1.00 180 184 184 324 344 10 75.0-125 V V 0.108 20
Nickel 1.00 6.21 7.29 7.32 108 111 10 75.0-125 0.447 20
Selenium 1.00 ND 0.889 0.734 88.9 73.4 10 75.0-125 J6 19.1 20
Silver 0.200 6.25 6.52 6.51 135 130 10 75.0-125 V V 0.159 20
Thallium 1.00 ND 0.176 0.156 17.6 15.6 10 75.0-125 J6 J6 11.8 20
Zinc 1.00 197 199 200 286 354 10 75.0-125 V E V 0.338 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048082
Metals (ICP) by Method 6010B L1607939-17,18
Method Blank (MB)
(MB) R3918462-1 04/27/23 21:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic 0.00445 J 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3918462-2 04/27/23 21:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.993 99.3 80.0-120
Arsenic 1.00 0.965 96.5 80.0-120
Beryllium 1.00 0.976 97.6 80.0-120
Cadmium 1.00 0.994 99.4 80.0-120
Chromium 1.00 0.980 98.0 80.0-120
Copper 1.00 0.980 98.0 80.0-120
Lead 1.00 0.988 98.8 80.0-120
Nickel 1.00 0.985 98.5 80.0-120
Selenium 1.00 0.998 99.8 80.0-120
Silver 0.200 0.196 98.2 80.0-120
Thallium 1.00 0.990 99.0 80.0-120
Zinc 1.00 0.993 99.3 80.0-120
L1607977-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607977-07 04/27/23 21:11 • (MS) R3918462-4 04/27/23 21:16 • (MSD) R3918462-5 04/27/23 21:18
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 1.00 1.03 1.04 103 104 1 75.0-125 0.347 20
Arsenic 1.00 1.00 1.01 100 101 1 75.0-125 0.189 20
Beryllium 1.00 ND 0.990 0.992 98.9 99.2 1 75.0-125 0.299 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048082
Metals (ICP) by Method 6010B L1607939-17,18
L1607977-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607977-07 04/27/23 21:11 • (MS) R3918462-4 04/27/23 21:16 • (MSD) R3918462-5 04/27/23 21:18
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Cadmium 1.00 1.02 1.03 102 103 1 75.0-125 0.328 20
Chromium 1.00 ND 0.976 0.988 97.6 98.8 1 75.0-125 1.24 20
Copper 1.00 1.01 1.03 100 102 1 75.0-125 1.40 20
Lead 1.00 ND 0.973 0.986 97.3 98.6 1 75.0-125 1.31 20
Nickel 1.00 0.996 0.997 99.6 99.7 1 75.0-125 0.107 20
Selenium 1.00 1.04 1.05 104 105 1 75.0-125 0.880 20
Silver 0.200 ND 0.201 0.204 101 102 1 75.0-125 1.29 20
Thallium 1.00 0.992 1.00 99.2 100 1 75.0-125 0.900 20
Zinc 1.00 1.02 1.03 97.9 98.4 1 75.0-125 0.454 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048547
Metals (ICP) by Method 6010B L1607939-19,20,21,22
Method Blank (MB)
(MB) R3919071-1 04/28/23 22:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic U 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3919071-2 04/28/23 22:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.981 98.1 80.0-120
Arsenic 1.00 0.940 94.0 80.0-120
Beryllium 1.00 0.962 96.2 80.0-120
Cadmium 1.00 0.976 97.6 80.0-120
Chromium 1.00 0.961 96.1 80.0-120
Copper 1.00 0.974 97.4 80.0-120
Lead 1.00 0.959 95.9 80.0-120
Nickel 1.00 0.962 96.2 80.0-120
Selenium 1.00 0.969 96.9 80.0-120
Silver 0.200 0.193 96.5 80.0-120
Thallium 1.00 0.968 96.8 80.0-120
Zinc 1.00 0.962 96.2 80.0-120
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/28/23 22:40 • (MS) R3919071-4 04/28/23 22:45 • (MSD) R3919071-5 04/28/23 22:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 1.01 1.02 101 102 1 75.0-125 0.775 20
Arsenic 1.00 0.0233 1.01 1.04 98.3 102 1 75.0-125 3.69 20
Beryllium 1.00 ND 0.954 0.974 95.4 97.4 1 75.0-125 2.03 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048547
Metals (ICP) by Method 6010B L1607939-19,20,21,22
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/28/23 22:40 • (MS) R3919071-4 04/28/23 22:45 • (MSD) R3919071-5 04/28/23 22:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Cadmium 1.00 ND 1.00 1.03 100 103 1 75.0-125 2.94 20
Chromium 1.00 0.0204 0.961 0.984 94.0 96.3 1 75.0-125 2.39 20
Copper 1.00 0.0383 1.03 1.06 99.0 102 1 75.0-125 2.91 20
Lead 1.00 ND 0.968 0.989 96.8 98.9 1 75.0-125 2.13 20
Nickel 1.00 0.0197 0.988 1.01 96.8 99.4 1 75.0-125 2.59 20
Selenium 1.00 ND 0.999 1.04 99.9 104 1 75.0-125 4.14 20
Silver 0.200 ND 0.201 0.207 100 103 1 75.0-125 2.82 20
Thallium 1.00 ND 0.960 0.981 96.0 98.1 1 75.0-125 2.10 20
Zinc 1.00 ND 0.972 0.997 94.4 96.8 1 75.0-125 2.50 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048870
Metals (ICP) by Method 6010B L1607939-02,03,04,05,06,07,08,09,10
Method Blank (MB)
(MB) R3918368-1 04/27/23 16:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3918368-2 04/27/23 16:55
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Arsenic 100 104 104 80.0-120
Beryllium 100 95.3 95.3 80.0-120
Cadmium 100 98.8 98.8 80.0-120
Chromium 100 94.1 94.1 80.0-120
Copper 100 97.6 97.6 80.0-120
Lead 100 95.7 95.7 80.0-120
Nickel 100 96.0 96.0 80.0-120
Selenium 100 103 103 80.0-120
Silver 20.0 19.2 95.8 80.0-120
Thallium 100 97.5 97.5 80.0-120
Zinc 100 97.7 97.7 80.0-120
L1608007-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608007-11 04/27/23 16:57 • (MS) R3918368-5 04/27/23 17:05 • (MSD) R3918368-6 04/27/23 17:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 100 5.59 109 112 104 106 1 75.0-125 2.31 20
Beryllium 100 0.473 93.8 96.6 93.3 96.2 1 75.0-125 2.96 20
Cadmium 100 ND 98.6 100 98.6 100 1 75.0-125 1.37 20
Chromium 100 9.24 105 106 95.4 97.1 1 75.0-125 1.58 20
Copper 100 6.82 106 108 99.0 101 1 75.0-125 2.20 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048870
Metals (ICP) by Method 6010B L1607939-02,03,04,05,06,07,08,09,10
L1608007-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608007-11 04/27/23 16:57 • (MS) R3918368-5 04/27/23 17:05 • (MSD) R3918368-6 04/27/23 17:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Lead 100 7.97 104 106 96.4 98.5 1 75.0-125 1.97 20
Nickel 100 9.56 109 111 99.4 102 1 75.0-125 2.23 20
Selenium 100 ND 102 104 102 104 1 75.0-125 1.82 20
Silver 20.0 ND 19.2 19.5 96.1 97.5 1 75.0-125 1.45 20
Thallium 100 ND 97.0 98.9 97.0 98.9 1 75.0-125 1.95 20
Zinc 100 25.4 121 126 96.1 101 1 75.0-125 3.86 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2050507
Metals (ICP) by Method 6010B L1607939-02,03,04,05,06,07,08,09,10
Method Blank (MB)
(MB) R3918927-1 04/28/23 18:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Laboratory Control Sample (LCS)
(LCS) R3918927-2 04/28/23 18:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 100 100 80.0-120
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 04/28/23 18:48 • (MS) R3918927-5 04/28/23 18:56 • (MSD) R3918927-6 04/28/23 18:59
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 128 ND 124 107 101 87.1 1 75.0-125 14.8 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2054328
Metals (ICP) by Method 6010B L1607939-01
Method Blank (MB)
(MB) R3921364-1 05/05/23 10:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3921364-2 05/05/23 10:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 98.6 98.6 80.0-120
Arsenic 100 94.1 94.1 80.0-120
Beryllium 100 96.9 96.9 80.0-120
Cadmium 100 97.2 97.2 80.0-120
Chromium 100 96.0 96.0 80.0-120
Copper 100 95.8 95.8 80.0-120
Lead 100 95.1 95.1 80.0-120
Nickel 100 97.2 97.2 80.0-120
Selenium 100 97.8 97.8 80.0-120
Silver 20.0 18.6 93.1 80.0-120
Thallium 100 96.1 96.1 80.0-120
Zinc 100 95.4 95.4 80.0-120
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/05/23 10:38 • (MS) R3921364-5 05/05/23 10:46 • (MSD) R3921364-6 05/05/23 10:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 121 ND 131 115 101 89.2 1 75.0-125 12.6 20
Arsenic 121 4.01 137 124 104 94.0 1 75.0-125 9.65 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2054328
Metals (ICP) by Method 6010B L1607939-01
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/05/23 10:38 • (MS) R3921364-5 05/05/23 10:46 • (MSD) R3921364-6 05/05/23 10:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 121 0.265 129 115 101 89.8 1 75.0-125 11.4 20
Cadmium 121 ND 136 122 107 95.7 1 75.0-125 11.0 20
Chromium 121 71.8 172 143 75.6 52.7 1 75.0-125 J6 18.6 20
Copper 121 86.4 205 163 89.3 56.9 1 75.0-125 J3 J6 22.5 20
Lead 121 10.8 190 126 140 89.7 1 75.0-125 J5 J3 40.7 20
Nickel 121 33.3 155 134 94.1 77.3 1 75.0-125 14.8 20
Selenium 121 ND 135 121 106 95.1 1 75.0-125 10.8 20
Silver 24.2 ND 26.3 23.5 103 92.3 1 75.0-125 11.1 20
Thallium 121 ND 122 111 95.9 86.8 1 75.0-125 9.94 20
Zinc 121 35.6 241 149 160 87.3 1 75.0-125 J5 J3 47.3 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047755
Volatile Organic Compounds (GC) by Method 8015D/GRO L1607939-11,12,13,14
Method Blank (MB)
(MB) R3917591-2 04/25/23 22:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)111 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3917591-1 04/25/23 21:09
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.32 96.7 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 109 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2049501
Volatile Organic Compounds (GC) by Method 8015D/GRO L1607939-19
Method Blank (MB)
(MB) R3917994-2 04/27/23 00:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)110 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3917994-1 04/26/23 23:52
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.06 92.0 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 106 78.0-120
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/27/23 06:59 • (MS) R3917994-3 04/27/23 09:55 • (MSD) R3917994-4 04/27/23 10:17
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.50 ND 4.99 5.42 90.7 98.5 1 10.0-160 8.26 22
(S)
a,a,a-Trifluorotoluene(FID) 103 103 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2049550
Volatile Organic Compounds (GC) by Method 8015D/GRO L1607939-20
Method Blank (MB)
(MB) R3918622-2 04/27/23 12:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)109 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3918622-1 04/27/23 11:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.64 103 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 108 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048964
Volatile Organic Compounds (GC) by Method 8015D/GRO L1607939-02,03,04
Method Blank (MB)
(MB) R3917609-2 04/26/23 12:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.743 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)95.0 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3917609-1 04/26/23 11:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 4.80 87.3 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 108 77.0-120
L1607565-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607565-02 04/26/23 16:11 • (MS) R3917609-3 04/26/23 20:05 • (MSD) R3917609-4 04/26/23 20:25
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
TPH (GC/FID) Low Fraction 165 8.11 145 139 82.9 79.6 25 10.0-151 3.77 28
(S)
a,a,a-Trifluorotoluene(FID) 103 99.3 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2049437
Volatile Organic Compounds (GC) by Method 8015D/GRO L1607939-05,06,07,08,09,10
Method Blank (MB)
(MB) R3918436-2 04/27/23 11:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 1.31 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)97.4 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3918436-1 04/27/23 10:27
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.32 96.7 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 101 77.0-120
L1607641-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607641-02 04/27/23 19:14 • (MS) R3918436-3 04/27/23 20:15 • (MSD) R3918436-4 04/27/23 20:36
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 831 55.4 752 743 83.8 82.8 100 10.0-151 1.15 28
(S)
a,a,a-Trifluorotoluene(FID) 110 109 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2053393
Volatile Organic Compounds (GC) by Method 8015D/GRO L1607939-01
Method Blank (MB)
(MB) R3920921-2 05/03/23 13:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.865 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)95.0 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3920921-1 05/03/23 12:11
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 6.10 111 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 101 77.0-120
L1609953-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1609953-04 05/04/23 08:12 • (MS) R3920921-5 05/04/23 12:10 • (MSD) R3920921-6 05/04/23 12:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 239 ND 212 235 87.4 97.0 43.5 10.0-151 10.3 28
(S)
a,a,a-Trifluorotoluene(FID) 101 102 77.0-120
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/03/23 14:54 • (MS) R3920921-3 05/04/23 11:21 • (MSD) R3920921-4 05/04/23 11:46
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 202 ND 216 188 97.1 84.5 26 10.0-151 13.7 28
(S)
a,a,a-Trifluorotoluene(FID) 103 103 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047326
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-11,12,13,14
Method Blank (MB)
(MB) R3917291-2 04/23/23 23:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromobenzene U 0.000118 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-Butylbenzene U 0.000125 0.00100
tert-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
2-Chlorotoluene U 0.000106 0.00100
4-Chlorotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
cis-1,2-Dichloroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
1,1-Dichloropropene U 0.000142 0.00100
1,3-Dichloropropane U 0.000110 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
2,2-Dichloropropane U 0.000161 0.00100
Di-isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Hexachloro-1,3-butadiene U 0.000337 0.00100
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047326
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-11,12,13,14
Method Blank (MB)
(MB) R3917291-2 04/23/23 23:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Isopropylbenzene U 0.000105 0.00100
p-Isopropyltoluene U 0.000120 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK) U 0.000478 0.0100
Methyl tert-butyl ether U 0.000101 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100
1,1,1,2-Tetrachloroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene U 0.000230 0.00100
1,2,4-Trichlorobenzene U 0.000481 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,2,3-Trichloropropane U 0.000237 0.00250
1,2,4-Trimethylbenzene U 0.000322 0.00100
1,2,3-Trimethylbenzene U 0.000104 0.00100
1,3,5-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 107 80.0-120
(S) 4-Bromofluorobenzene 97.6 77.0-126
(S) 1,2-Dichloroethane-d4 105 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3917291-1 04/23/23 22:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acetone 0.0250 0.0244 97.6 19.0-160
Acrolein 0.0250 0.0371 148 10.0-160
Acrylonitrile 0.0250 0.0218 87.2 55.0-149
Benzene 0.00500 0.00419 83.8 70.0-123
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047326
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-11,12,13,14
Laboratory Control Sample (LCS)
(LCS) R3917291-1 04/23/23 22:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Bromobenzene 0.00500 0.00397 79.4 73.0-121
Bromodichloromethane 0.00500 0.00415 83.0 75.0-120
Bromoform 0.00500 0.00397 79.4 68.0-132
Bromomethane 0.00500 0.00436 87.2 10.0-160
n-Butylbenzene 0.00500 0.00389 77.8 73.0-125
sec-Butylbenzene 0.00500 0.00386 77.2 75.0-125
tert-Butylbenzene 0.00500 0.00395 79.0 76.0-124
Carbon tetrachloride 0.00500 0.00425 85.0 68.0-126
Chlorobenzene 0.00500 0.00435 87.0 80.0-121
Chlorodibromomethane 0.00500 0.00430 86.0 77.0-125
Chloroethane 0.00500 0.00473 94.6 47.0-150
Chloroform 0.00500 0.00441 88.2 73.0-120
Chloromethane 0.00500 0.00400 80.0 41.0-142
2-Chlorotoluene 0.00500 0.00400 80.0 76.0-123
4-Chlorotoluene 0.00500 0.00390 78.0 75.0-122
1,2-Dibromo-3-Chloropropane 0.00500 0.00407 81.4 58.0-134
1,2-Dibromoethane 0.00500 0.00424 84.8 80.0-122
Dibromomethane 0.00500 0.00437 87.4 80.0-120
1,2-Dichlorobenzene 0.00500 0.00421 84.2 79.0-121
1,3-Dichlorobenzene 0.00500 0.00419 83.8 79.0-120
1,4-Dichlorobenzene 0.00500 0.00413 82.6 79.0-120
Dichlorodifluoromethane 0.00500 0.00464 92.8 51.0-149
1,1-Dichloroethane 0.00500 0.00473 94.6 70.0-126
1,2-Dichloroethane 0.00500 0.00447 89.4 70.0-128
1,1-Dichloroethene 0.00500 0.00519 104 71.0-124
cis-1,2-Dichloroethene 0.00500 0.00435 87.0 73.0-120
trans-1,2-Dichloroethene 0.00500 0.00432 86.4 73.0-120
1,2-Dichloropropane 0.00500 0.00447 89.4 77.0-125
1,1-Dichloropropene 0.00500 0.00413 82.6 74.0-126
1,3-Dichloropropane 0.00500 0.00423 84.6 80.0-120
cis-1,3-Dichloropropene 0.00500 0.00425 85.0 80.0-123
trans-1,3-Dichloropropene 0.00500 0.00423 84.6 78.0-124
2,2-Dichloropropane 0.00500 0.00451 90.2 58.0-130
Di-isopropyl ether 0.00500 0.00396 79.2 58.0-138
Ethylbenzene 0.00500 0.00419 83.8 79.0-123
Hexachloro-1,3-butadiene 0.00500 0.00414 82.8 54.0-138
Isopropylbenzene 0.00500 0.00415 83.0 76.0-127
p-Isopropyltoluene 0.00500 0.00395 79.0 76.0-125
2-Butanone (MEK)0.0250 0.0205 82.0 44.0-160
Methylene Chloride 0.00500 0.00492 98.4 67.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047326
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-11,12,13,14
Laboratory Control Sample (LCS)
(LCS) R3917291-1 04/23/23 22:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
4-Methyl-2-pentanone (MIBK) 0.0250 0.0198 79.2 68.0-142
Methyl tert-butyl ether 0.00500 0.00472 94.4 68.0-125
Naphthalene 0.00500 0.00388 77.6 54.0-135
n-Propylbenzene 0.00500 0.00391 78.2 77.0-124
Styrene 0.00500 0.00417 83.4 73.0-130
1,1,1,2-Tetrachloroethane 0.00500 0.00423 84.6 75.0-125
1,1,2,2-Tetrachloroethane 0.00500 0.00420 84.0 65.0-130
1,1,2-Trichlorotrifluoroethane 0.00500 0.00552 110 69.0-132
Tetrachloroethene 0.00500 0.00404 80.8 72.0-132
Toluene 0.00500 0.00418 83.6 79.0-120
1,2,3-Trichlorobenzene 0.00500 0.00429 85.8 50.0-138
1,2,4-Trichlorobenzene 0.00500 0.00423 84.6 57.0-137
1,1,1-Trichloroethane 0.00500 0.00415 83.0 73.0-124
1,1,2-Trichloroethane 0.00500 0.00426 85.2 80.0-120
Trichloroethene 0.00500 0.00415 83.0 78.0-124
Trichlorofluoromethane 0.00500 0.00421 84.2 59.0-147
1,2,3-Trichloropropane 0.00500 0.00398 79.6 73.0-130
1,2,4-Trimethylbenzene 0.00500 0.00400 80.0 76.0-121
1,2,3-Trimethylbenzene 0.00500 0.00400 80.0 77.0-120
1,3,5-Trimethylbenzene 0.00500 0.00375 75.0 76.0-122 J4
Vinyl chloride 0.00500 0.00462 92.4 67.0-131
Xylenes, Total 0.0150 0.0127 84.7 79.0-123
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 99.8 77.0-126
(S) 1,2-Dichloroethane-d4 106 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048606
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-19,20
Method Blank (MB)
(MB) R3917469-2 04/25/23 16:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromobenzene U 0.000118 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-Butylbenzene U 0.000125 0.00100
tert-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
2-Chlorotoluene U 0.000106 0.00100
4-Chlorotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
cis-1,2-Dichloroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
1,1-Dichloropropene U 0.000142 0.00100
1,3-Dichloropropane U 0.000110 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
2,2-Dichloropropane U 0.000161 0.00100
Di-isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Hexachloro-1,3-butadiene U 0.000337 0.00100
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048606
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-19,20
Method Blank (MB)
(MB) R3917469-2 04/25/23 16:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Isopropylbenzene U 0.000105 0.00100
p-Isopropyltoluene U 0.000120 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK) U 0.000478 0.0100
Methyl tert-butyl ether U 0.000101 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100
1,1,1,2-Tetrachloroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene 0.000296 J 0.000230 0.00100
1,2,4-Trichlorobenzene U 0.000481 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,2,3-Trichloropropane U 0.000237 0.00250
1,2,4-Trimethylbenzene U 0.000322 0.00100
1,2,3-Trimethylbenzene U 0.000104 0.00100
1,3,5-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 110 80.0-120
(S) 4-Bromofluorobenzene 107 77.0-126
(S) 1,2-Dichloroethane-d4 106 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3917469-1 04/25/23 15:28 • (LCSD) R3917469-3 04/25/23 17:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0228 0.0232 91.2 92.8 19.0-160 1.74 27
Acrolein 0.0250 0.0243 0.0243 97.2 97.2 10.0-160 0.000 26
Acrylonitrile 0.0250 0.0249 0.0259 99.6 104 55.0-149 3.94 20
Benzene 0.00500 0.00508 0.00505 102 101 70.0-123 0.592 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048606
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3917469-1 04/25/23 15:28 • (LCSD) R3917469-3 04/25/23 17:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Bromobenzene 0.00500 0.00505 0.00497 101 99.4 73.0-121 1.60 20
Bromodichloromethane 0.00500 0.00461 0.00518 92.2 104 75.0-120 11.6 20
Bromoform 0.00500 0.00367 0.00368 73.4 73.6 68.0-132 0.272 20
Bromomethane 0.00500 0.00262 0.00266 52.4 53.2 10.0-160 1.52 25
n-Butylbenzene 0.00500 0.00492 0.00512 98.4 102 73.0-125 3.98 20
sec-Butylbenzene 0.00500 0.00506 0.00483 101 96.6 75.0-125 4.65 20
tert-Butylbenzene 0.00500 0.00494 0.00474 98.8 94.8 76.0-124 4.13 20
Carbon tetrachloride 0.00500 0.00491 0.00465 98.2 93.0 68.0-126 5.44 20
Chlorobenzene 0.00500 0.00474 0.00459 94.8 91.8 80.0-121 3.22 20
Chlorodibromomethane 0.00500 0.00421 0.00413 84.2 82.6 77.0-125 1.92 20
Chloroethane 0.00500 0.00416 0.00433 83.2 86.6 47.0-150 4.00 20
Chloroform 0.00500 0.00482 0.00524 96.4 105 73.0-120 8.35 20
Chloromethane 0.00500 0.00464 0.00433 92.8 86.6 41.0-142 6.91 20
2-Chlorotoluene 0.00500 0.00513 0.00514 103 103 76.0-123 0.195 20
4-Chlorotoluene 0.00500 0.00516 0.00536 103 107 75.0-122 3.80 20
1,2-Dibromo-3-Chloropropane 0.00500 0.00373 0.00371 74.6 74.2 58.0-134 0.538 20
1,2-Dibromoethane 0.00500 0.00426 0.00412 85.2 82.4 80.0-122 3.34 20
Dibromomethane 0.00500 0.00444 0.00462 88.8 92.4 80.0-120 3.97 20
1,2-Dichlorobenzene 0.00500 0.00466 0.00450 93.2 90.0 79.0-121 3.49 20
1,3-Dichlorobenzene 0.00500 0.00468 0.00453 93.6 90.6 79.0-120 3.26 20
1,4-Dichlorobenzene 0.00500 0.00445 0.00480 89.0 96.0 79.0-120 7.57 20
Dichlorodifluoromethane 0.00500 0.00377 0.00346 75.4 69.2 51.0-149 8.58 20
1,1-Dichloroethane 0.00500 0.00518 0.00549 104 110 70.0-126 5.81 20
1,2-Dichloroethane 0.00500 0.00494 0.00535 98.8 107 70.0-128 7.97 20
1,1-Dichloroethene 0.00500 0.00498 0.00453 99.6 90.6 71.0-124 9.46 20
cis-1,2-Dichloroethene 0.00500 0.00447 0.00499 89.4 99.8 73.0-120 11.0 20
trans-1,2-Dichloroethene 0.00500 0.00477 0.00506 95.4 101 73.0-120 5.90 20
1,2-Dichloropropane 0.00500 0.00537 0.00532 107 106 77.0-125 0.935 20
1,1-Dichloropropene 0.00500 0.00519 0.00499 104 99.8 74.0-126 3.93 20
1,3-Dichloropropane 0.00500 0.00464 0.00464 92.8 92.8 80.0-120 0.000 20
cis-1,3-Dichloropropene 0.00500 0.00457 0.00492 91.4 98.4 80.0-123 7.38 20
trans-1,3-Dichloropropene 0.00500 0.00458 0.00451 91.6 90.2 78.0-124 1.54 20
2,2-Dichloropropane 0.00500 0.00527 0.00513 105 103 58.0-130 2.69 20
Di-isopropyl ether 0.00500 0.00555 0.00583 111 117 58.0-138 4.92 20
Ethylbenzene 0.00500 0.00459 0.00469 91.8 93.8 79.0-123 2.16 20
Hexachloro-1,3-butadiene 0.00500 0.00481 0.00520 96.2 104 54.0-138 7.79 20
Isopropylbenzene 0.00500 0.00468 0.00439 93.6 87.8 76.0-127 6.39 20
p-Isopropyltoluene 0.00500 0.00486 0.00470 97.2 94.0 76.0-125 3.35 20
2-Butanone (MEK)0.0250 0.0245 0.0242 98.0 96.8 44.0-160 1.23 20
Methylene Chloride 0.00500 0.00536 0.00551 107 110 67.0-120 2.76 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048606
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3917469-1 04/25/23 15:28 • (LCSD) R3917469-3 04/25/23 17:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
4-Methyl-2-pentanone (MIBK) 0.0250 0.0238 0.0239 95.2 95.6 68.0-142 0.419 20
Methyl tert-butyl ether 0.00500 0.00451 0.00463 90.2 92.6 68.0-125 2.63 20
Naphthalene 0.00500 0.00346 0.00337 69.2 67.4 54.0-135 2.64 20
n-Propylbenzene 0.00500 0.00515 0.00492 103 98.4 77.0-124 4.57 20
Styrene 0.00500 0.00442 0.00436 88.4 87.2 73.0-130 1.37 20
1,1,1,2-Tetrachloroethane 0.00500 0.00447 0.00452 89.4 90.4 75.0-125 1.11 20
1,1,2,2-Tetrachloroethane 0.00500 0.00467 0.00518 93.4 104 65.0-130 10.4 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00475 0.00462 95.0 92.4 69.0-132 2.77 20
Tetrachloroethene 0.00500 0.00455 0.00418 91.0 83.6 72.0-132 8.48 20
Toluene 0.00500 0.00486 0.00472 97.2 94.4 79.0-120 2.92 20
1,2,3-Trichlorobenzene 0.00500 0.00401 0.00430 80.2 86.0 50.0-138 6.98 20
1,2,4-Trichlorobenzene 0.00500 0.00442 0.00418 88.4 83.6 57.0-137 5.58 20
1,1,1-Trichloroethane 0.00500 0.00480 0.00483 96.0 96.6 73.0-124 0.623 20
1,1,2-Trichloroethane 0.00500 0.00452 0.00442 90.4 88.4 80.0-120 2.24 20
Trichloroethene 0.00500 0.00502 0.00494 100 98.8 78.0-124 1.61 20
Trichlorofluoromethane 0.00500 0.00399 0.00372 79.8 74.4 59.0-147 7.00 20
1,2,3-Trichloropropane 0.00500 0.00449 0.00468 89.8 93.6 73.0-130 4.14 20
1,2,4-Trimethylbenzene 0.00500 0.00485 0.00486 97.0 97.2 76.0-121 0.206 20
1,2,3-Trimethylbenzene 0.00500 0.00465 0.00478 93.0 95.6 77.0-120 2.76 20
1,3,5-Trimethylbenzene 0.00500 0.00497 0.00488 99.4 97.6 76.0-122 1.83 20
Vinyl chloride 0.00500 0.00432 0.00411 86.4 82.2 67.0-131 4.98 20
Xylenes, Total 0.0150 0.0138 0.0134 92.0 89.3 79.0-123 2.94 20
(S) Toluene-d8 112 107 80.0-120
(S) 4-Bromofluorobenzene 105 102 77.0-126
(S) 1,2-Dichloroethane-d4 104 111 70.0-130
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/25/23 22:05 • (MS) R3917469-4 04/26/23 03:10 • (MSD) R3917469-5 04/26/23 03:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acetone 0.0250 ND ND ND 100 95.2 1 10.0-160 5.32 35
Acrolein 0.0250 ND ND ND 104 96.8 1 10.0-160 7.55 39
Acrylonitrile 0.0250 ND 0.0267 0.0254 107 102 1 21.0-160 4.99 32
Benzene 0.00500 ND 0.00585 0.00550 117 110 1 17.0-158 6.17 27
Bromobenzene 0.00500 ND 0.00563 0.00548 113 110 1 30.0-149 2.70 28
Bromodichloromethane 0.00500 ND 0.00533 0.00511 107 102 1 31.0-150 4.21 27
Bromoform 0.00500 ND 0.00401 0.00364 80.2 72.8 1 29.0-150 9.67 29
Bromomethane 0.00500 ND ND ND 66.6 67.8 1 10.0-160 1.79 38
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048606
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-19,20
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/25/23 22:05 • (MS) R3917469-4 04/26/23 03:10 • (MSD) R3917469-5 04/26/23 03:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
n-Butylbenzene 0.00500 ND 0.00582 0.00559 116 112 1 31.0-150 4.03 30
sec-Butylbenzene 0.00500 ND 0.00601 0.00570 120 114 1 33.0-155 5.29 29
tert-Butylbenzene 0.00500 ND 0.00558 0.00546 112 109 1 34.0-153 2.17 28
Carbon tetrachloride 0.00500 ND 0.00602 0.00588 120 118 1 23.0-159 2.35 28
Chlorobenzene 0.00500 ND 0.00520 0.00509 104 102 1 33.0-152 2.14 27
Chlorodibromomethane 0.00500 ND 0.00479 0.00430 95.8 86.0 1 37.0-149 10.8 27
Chloroethane 0.00500 ND 0.00525 ND 105 93.4 1 10.0-160 11.7 30
Chloroform 0.00500 ND 0.00584 0.00545 117 109 1 29.0-154 6.91 28
Chloromethane 0.00500 ND 0.00541 0.00531 108 106 1 10.0-160 1.87 29
2-Chlorotoluene 0.00500 ND 0.00575 0.00550 115 110 1 32.0-153 4.44 28
4-Chlorotoluene 0.00500 ND 0.00595 0.00563 119 113 1 32.0-150 5.53 28
1,2-Dibromo-3-Chloropropane 0.00500 ND ND ND 76.8 68.2 1 22.0-151 11.9 34
1,2-Dibromoethane 0.00500 ND 0.00458 0.00441 91.6 88.2 1 34.0-147 3.78 27
Dibromomethane 0.00500 ND 0.00484 0.00459 96.8 91.8 1 30.0-151 5.30 27
1,2-Dichlorobenzene 0.00500 ND 0.00492 0.00469 98.4 93.8 1 34.0-149 4.79 28
1,3-Dichlorobenzene 0.00500 ND 0.00530 0.00504 106 101 1 36.0-146 5.03 27
1,4-Dichlorobenzene 0.00500 ND 0.00515 0.00482 103 96.4 1 35.0-142 6.62 27
Dichlorodifluoromethane 0.00500 ND ND ND 98.2 93.0 1 10.0-160 5.44 29
1,1-Dichloroethane 0.00500 ND 0.00602 0.00580 120 116 1 25.0-158 3.72 27
1,2-Dichloroethane 0.00500 ND 0.00578 0.00536 116 107 1 29.0-151 7.54 27
1,1-Dichloroethene 0.00500 ND 0.00599 0.00558 120 112 1 11.0-160 7.09 29
cis-1,2-Dichloroethene 0.00500 ND 0.00532 0.00527 106 105 1 10.0-160 0.944 27
trans-1,2-Dichloroethene 0.00500 ND 0.00586 0.00556 117 111 1 17.0-153 5.25 27
1,2-Dichloropropane 0.00500 ND 0.00598 0.00603 120 121 1 30.0-156 0.833 27
1,1-Dichloropropene 0.00500 ND 0.00620 0.00623 124 125 1 25.0-158 0.483 27
1,3-Dichloropropane 0.00500 ND 0.00527 0.00478 105 95.6 1 38.0-147 9.75 27
cis-1,3-Dichloropropene 0.00500 ND 0.00513 0.00493 103 98.6 1 34.0-149 3.98 28
trans-1,3-Dichloropropene 0.00500 ND 0.00469 0.00445 93.8 89.0 1 32.0-149 5.25 28
2,2-Dichloropropane 0.00500 ND 0.00591 0.00547 118 109 1 24.0-152 7.73 29
Di-isopropyl ether 0.00500 ND 0.00618 0.00586 124 117 1 21.0-160 5.32 28
Ethylbenzene 0.00500 ND 0.00548 0.00499 110 99.8 1 30.0-155 9.36 27
Hexachloro-1,3-butadiene 0.00500 ND 0.00539 0.00559 108 112 1 20.0-154 3.64 34
Isopropylbenzene 0.00500 ND 0.00527 0.00504 105 101 1 28.0-157 4.46 27
p-Isopropyltoluene 0.00500 ND 0.00547 0.00523 109 105 1 30.0-154 4.49 29
2-Butanone (MEK)0.0250 ND 0.0262 0.0232 105 92.8 1 10.0-160 12.1 32
Methylene Chloride 0.00500 ND 0.00575 0.00549 115 110 1 23.0-144 4.63 28
4-Methyl-2-pentanone (MIBK) 0.0250 ND 0.0247 0.0232 98.8 92.8 1 29.0-160 6.26 29
Methyl tert-butyl ether 0.00500 ND 0.00501 0.00477 100 95.4 1 28.0-150 4.91 29
Naphthalene 0.00500 ND ND ND 70.8 69.2 1 12.0-156 2.29 35
n-Propylbenzene 0.00500 ND 0.00598 0.00561 120 112 1 31.0-154 6.38 28
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048606
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-19,20
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/25/23 22:05 • (MS) R3917469-4 04/26/23 03:10 • (MSD) R3917469-5 04/26/23 03:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Styrene 0.00500 ND 0.00450 0.00462 90.0 92.4 1 33.0-155 2.63 28
1,1,1,2-Tetrachloroethane 0.00500 ND 0.00507 0.00454 101 90.8 1 36.0-151 11.0 29
1,1,2,2-Tetrachloroethane 0.00500 ND 0.00519 0.00458 104 91.6 1 33.0-150 12.5 28
1,1,2-Trichlorotrifluoroethane 0.00500 ND 0.00594 0.00576 119 115 1 23.0-160 3.08 30
Tetrachloroethene 0.00500 ND 0.00596 0.00554 105 97.0 1 10.0-160 7.30 27
Toluene 0.00500 ND 0.00584 0.00556 117 111 1 26.0-154 4.91 28
1,2,3-Trichlorobenzene 0.00500 ND 0.00394 0.00437 78.8 87.4 1 17.0-150 10.3 36
1,2,4-Trichlorobenzene 0.00500 ND 0.00423 0.00450 84.6 90.0 1 24.0-150 6.19 33
1,1,1-Trichloroethane 0.00500 ND 0.00584 0.00563 117 113 1 23.0-160 3.66 28
1,1,2-Trichloroethane 0.00500 ND 0.00487 0.00456 97.4 91.2 1 35.0-147 6.57 27
Trichloroethene 0.00500 ND 0.00553 0.00520 111 104 1 10.0-160 6.15 25
Trichlorofluoromethane 0.00500 ND 0.00542 0.00515 108 103 1 17.0-160 5.11 31
1,2,3-Trichloropropane 0.00500 ND 0.00502 0.00423 100 84.6 1 34.0-151 17.1 29
1,2,4-Trimethylbenzene 0.00500 ND 0.00566 0.00526 113 105 1 26.0-154 7.33 27
1,2,3-Trimethylbenzene 0.00500 ND 0.00550 0.00511 110 102 1 32.0-149 7.35 28
1,3,5-Trimethylbenzene 0.00500 ND 0.00561 0.00520 112 104 1 28.0-153 7.59 27
Vinyl chloride 0.00500 ND 0.00537 0.00518 107 104 1 10.0-160 3.60 27
Xylenes, Total 0.0150 ND 0.0159 0.0147 106 98.0 1 29.0-154 7.84 28
(S) Toluene-d8 109 108 80.0-120
(S) 4-Bromofluorobenzene 102 101 77.0-126
(S) 1,2-Dichloroethane-d4 110 110 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048701
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-02,03,04,05
Method Blank (MB)
(MB) R3918099-3 04/25/23 22:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048701
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-02,03,04,05
Method Blank (MB)
(MB) R3918099-3 04/25/23 22:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 95.9 75.0-131
(S) 4-Bromofluorobenzene 112 67.0-138
(S) 1,2-Dichloroethane-d4 90.0 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3918099-1 04/25/23 20:38 • (LCSD) R3918099-2 04/25/23 20:57
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.667 0.861 107 138 10.0-160 25.4 31
Acrylonitrile 0.625 0.812 0.959 130 153 45.0-153 16.6 22
Benzene 0.125 0.129 0.151 103 121 70.0-123 15.7 20
Bromobenzene 0.125 0.118 0.136 94.4 109 73.0-121 14.2 20
Bromodichloromethane 0.125 0.124 0.141 99.2 113 73.0-121 12.8 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048701
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3918099-1 04/25/23 20:38 • (LCSD) R3918099-2 04/25/23 20:57
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.127 0.140 102 112 64.0-132 9.74 20
Bromomethane 0.125 0.0813 0.0979 65.0 78.3 56.0-147 18.5 20
n-Butylbenzene 0.125 0.0896 0.108 71.7 86.4 68.0-135 18.6 20
sec-Butylbenzene 0.125 0.102 0.125 81.6 100 74.0-130 J3 20.3 20
tert-Butylbenzene 0.125 0.107 0.132 85.6 106 75.0-127 J3 20.9 20
Carbon tetrachloride 0.125 0.123 0.149 98.4 119 66.0-128 19.1 20
Chlorobenzene 0.125 0.116 0.137 92.8 110 76.0-128 16.6 20
Chlorodibromomethane 0.125 0.118 0.134 94.4 107 74.0-127 12.7 20
Chloroethane 0.125 0.0931 0.109 74.5 87.2 61.0-134 15.7 20
Chloroform 0.125 0.118 0.140 94.4 112 72.0-123 17.1 20
Chloromethane 0.125 0.106 0.129 84.8 103 51.0-138 19.6 20
2-Chlorotoluene 0.125 0.110 0.133 88.0 106 75.0-124 18.9 20
4-Chlorotoluene 0.125 0.106 0.123 84.8 98.4 75.0-124 14.8 20
1,2-Dibromo-3-Chloropropane 0.125 0.116 0.135 92.8 108 59.0-130 15.1 20
1,2-Dibromoethane 0.125 0.117 0.132 93.6 106 74.0-128 12.0 20
Dibromomethane 0.125 0.119 0.143 95.2 114 75.0-122 18.3 20
1,2-Dichlorobenzene 0.125 0.116 0.131 92.8 105 76.0-124 12.1 20
1,3-Dichlorobenzene 0.125 0.119 0.135 95.2 108 76.0-125 12.6 20
1,4-Dichlorobenzene 0.125 0.102 0.115 81.6 92.0 77.0-121 12.0 20
Dichlorodifluoromethane 0.125 0.103 0.114 82.4 91.2 43.0-156 10.1 20
1,1-Dichloroethane 0.125 0.141 0.168 113 134 70.0-127 J4 17.5 20
1,2-Dichloroethane 0.125 0.115 0.133 92.0 106 65.0-131 14.5 20
1,1-Dichloroethene 0.125 0.135 0.159 108 127 65.0-131 16.3 20
cis-1,2-Dichloroethene 0.125 0.136 0.154 109 123 73.0-125 12.4 20
trans-1,2-Dichloroethene 0.125 0.129 0.156 103 125 71.0-125 18.9 20
1,2-Dichloropropane 0.125 0.144 0.166 115 133 74.0-125 J4 14.2 20
1,1-Dichloropropene 0.125 0.135 0.161 108 129 73.0-125 J4 17.6 20
1,3-Dichloropropane 0.125 0.124 0.137 99.2 110 80.0-125 9.96 20
cis-1,3-Dichloropropene 0.125 0.121 0.133 96.8 106 76.0-127 9.45 20
trans-1,3-Dichloropropene 0.125 0.109 0.116 87.2 92.8 73.0-127 6.22 20
2,2-Dichloropropane 0.125 0.133 0.165 106 132 59.0-135 J3 21.5 20
Di-isopropyl ether 0.125 0.156 0.173 125 138 60.0-136 J4 10.3 20
Ethylbenzene 0.125 0.117 0.144 93.6 115 74.0-126 J3 20.7 20
Hexachloro-1,3-butadiene 0.125 0.114 0.137 91.2 110 57.0-150 18.3 20
Isopropylbenzene 0.125 0.0996 0.122 79.7 97.6 72.0-127 J3 20.2 20
p-Isopropyltoluene 0.125 0.0900 0.111 72.0 88.8 72.0-133 J3 20.9 20
2-Butanone (MEK)0.625 0.640 0.765 102 122 30.0-160 17.8 24
Methylene Chloride 0.125 0.131 0.150 105 120 68.0-123 13.5 20
4-Methyl-2-pentanone (MIBK) 0.625 0.599 0.690 95.8 110 56.0-143 14.1 20
Methyl tert-butyl ether 0.125 0.142 0.155 114 124 66.0-132 8.75 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048701
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3918099-1 04/25/23 20:38 • (LCSD) R3918099-2 04/25/23 20:57
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0767 0.0920 61.4 73.6 59.0-130 18.1 20
n-Propylbenzene 0.125 0.106 0.129 84.8 103 74.0-126 19.6 20
Styrene 0.125 0.101 0.119 80.8 95.2 72.0-127 16.4 20
1,1,1,2-Tetrachloroethane 0.125 0.120 0.136 96.0 109 74.0-129 12.5 20
1,1,2,2-Tetrachloroethane 0.125 0.115 0.126 92.0 101 68.0-128 9.13 20
1,1,2-Trichlorotrifluoroethane 0.125 0.121 0.140 96.8 112 61.0-139 14.6 20
Tetrachloroethene 0.125 0.121 0.143 96.8 114 70.0-136 16.7 20
Toluene 0.125 0.114 0.138 91.2 110 75.0-121 19.0 20
1,2,3-Trichlorobenzene 0.125 0.0836 0.106 66.9 84.8 59.0-139 J3 23.6 20
1,2,4-Trichlorobenzene 0.125 0.0978 0.121 78.2 96.8 62.0-137 J3 21.2 20
1,1,1-Trichloroethane 0.125 0.121 0.144 96.8 115 69.0-126 17.4 20
1,1,2-Trichloroethane 0.125 0.119 0.134 95.2 107 78.0-123 11.9 20
Trichloroethene 0.125 0.126 0.152 101 122 76.0-126 18.7 20
Trichlorofluoromethane 0.125 0.0834 0.0962 66.7 77.0 61.0-142 14.3 20
1,2,3-Trichloropropane 0.125 0.119 0.133 95.2 106 67.0-129 11.1 20
1,2,4-Trimethylbenzene 0.125 0.0997 0.115 79.8 92.0 70.0-126 14.3 20
1,2,3-Trimethylbenzene 0.125 0.107 0.124 85.6 99.2 74.0-124 14.7 20
1,3,5-Trimethylbenzene 0.125 0.0965 0.120 77.2 96.0 73.0-127 J3 21.7 20
Vinyl chloride 0.125 0.103 0.125 82.4 100 63.0-134 19.3 20
Xylenes, Total 0.375 0.315 0.380 84.0 101 72.0-127 18.7 20
(S) Toluene-d8 95.8 97.2 75.0-131
(S) 4-Bromofluorobenzene 114 115 67.0-138
(S) 1,2-Dichloroethane-d4 94.9 91.3 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048704
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-06,07,08,09,10
Method Blank (MB)
(MB) R3918600-2 04/26/23 00:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048704
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-06,07,08,09,10
Method Blank (MB)
(MB) R3918600-2 04/26/23 00:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00220 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 89.6 67.0-138
(S) 1,2-Dichloroethane-d4 110 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3918600-1 04/25/23 23:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.694 111 10.0-160
Acrylonitrile 0.625 0.662 106 45.0-153
Benzene 0.125 0.123 98.4 70.0-123
Bromobenzene 0.125 0.123 98.4 73.0-121
Bromodichloromethane 0.125 0.130 104 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048704
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-06,07,08,09,10
Laboratory Control Sample (LCS)
(LCS) R3918600-1 04/25/23 23:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.108 86.4 64.0-132
Bromomethane 0.125 0.118 94.4 56.0-147
n-Butylbenzene 0.125 0.120 96.0 68.0-135
sec-Butylbenzene 0.125 0.125 100 74.0-130
tert-Butylbenzene 0.125 0.124 99.2 75.0-127
Carbon tetrachloride 0.125 0.122 97.6 66.0-128
Chlorobenzene 0.125 0.117 93.6 76.0-128
Chlorodibromomethane 0.125 0.114 91.2 74.0-127
Chloroethane 0.125 0.130 104 61.0-134
Chloroform 0.125 0.123 98.4 72.0-123
Chloromethane 0.125 0.139 111 51.0-138
2-Chlorotoluene 0.125 0.114 91.2 75.0-124
4-Chlorotoluene 0.125 0.128 102 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.128 102 59.0-130
1,2-Dibromoethane 0.125 0.117 93.6 74.0-128
Dibromomethane 0.125 0.122 97.6 75.0-122
1,2-Dichlorobenzene 0.125 0.117 93.6 76.0-124
1,3-Dichlorobenzene 0.125 0.112 89.6 76.0-125
1,4-Dichlorobenzene 0.125 0.117 93.6 77.0-121
Dichlorodifluoromethane 0.125 0.121 96.8 43.0-156
1,1-Dichloroethane 0.125 0.123 98.4 70.0-127
1,2-Dichloroethane 0.125 0.143 114 65.0-131
1,1-Dichloroethene 0.125 0.127 102 65.0-131
cis-1,2-Dichloroethene 0.125 0.118 94.4 73.0-125
trans-1,2-Dichloroethene 0.125 0.107 85.6 71.0-125
1,2-Dichloropropane 0.125 0.128 102 74.0-125
1,1-Dichloropropene 0.125 0.130 104 73.0-125
1,3-Dichloropropane 0.125 0.121 96.8 80.0-125
cis-1,3-Dichloropropene 0.125 0.131 105 76.0-127
trans-1,3-Dichloropropene 0.125 0.120 96.0 73.0-127
2,2-Dichloropropane 0.125 0.119 95.2 59.0-135
Di-isopropyl ether 0.125 0.134 107 60.0-136
Ethylbenzene 0.125 0.107 85.6 74.0-126
Hexachloro-1,3-butadiene 0.125 0.140 112 57.0-150
Isopropylbenzene 0.125 0.113 90.4 72.0-127
p-Isopropyltoluene 0.125 0.122 97.6 72.0-133
2-Butanone (MEK)0.625 0.882 141 30.0-160
Methylene Chloride 0.125 0.118 94.4 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.775 124 56.0-143
Methyl tert-butyl ether 0.125 0.110 88.0 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048704
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-06,07,08,09,10
Laboratory Control Sample (LCS)
(LCS) R3918600-1 04/25/23 23:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.126 101 59.0-130
n-Propylbenzene 0.125 0.129 103 74.0-126
Styrene 0.125 0.109 87.2 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.108 86.4 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.120 96.0 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.122 97.6 61.0-139
Tetrachloroethene 0.125 0.115 92.0 70.0-136
Toluene 0.125 0.115 92.0 75.0-121
1,2,3-Trichlorobenzene 0.125 0.127 102 59.0-139
1,2,4-Trichlorobenzene 0.125 0.128 102 62.0-137
1,1,1-Trichloroethane 0.125 0.121 96.8 69.0-126
1,1,2-Trichloroethane 0.125 0.112 89.6 78.0-123
Trichloroethene 0.125 0.130 104 76.0-126
Trichlorofluoromethane 0.125 0.142 114 61.0-142
1,2,3-Trichloropropane 0.125 0.132 106 67.0-129
1,2,4-Trimethylbenzene 0.125 0.114 91.2 70.0-126
1,2,3-Trimethylbenzene 0.125 0.120 96.0 74.0-124
1,3,5-Trimethylbenzene 0.125 0.122 97.6 73.0-127
Vinyl chloride 0.125 0.137 110 63.0-134
Xylenes, Total 0.375 0.336 89.6 72.0-127
(S) Toluene-d8 101 75.0-131
(S) 4-Bromofluorobenzene 92.4 67.0-138
(S) 1,2-Dichloroethane-d4 114 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052852
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-01
Method Blank (MB)
(MB) R3920204-3 05/02/23 22:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052852
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-01
Method Blank (MB)
(MB) R3920204-3 05/02/23 22:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00120 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 112 75.0-131
(S) 4-Bromofluorobenzene 83.4 67.0-138
(S) 1,2-Dichloroethane-d4 111 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3920204-1 05/02/23 20:42 • (LCSD) R3920204-2 05/02/23 21:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.775 0.694 124 111 10.0-160 11.0 31
Acrylonitrile 0.625 0.638 0.596 102 95.4 45.0-153 6.81 22
Benzene 0.125 0.116 0.113 92.8 90.4 70.0-123 2.62 20
Bromobenzene 0.125 0.132 0.126 106 101 73.0-121 4.65 20
Bromodichloromethane 0.125 0.122 0.121 97.6 96.8 73.0-121 0.823 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052852
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3920204-1 05/02/23 20:42 • (LCSD) R3920204-2 05/02/23 21:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.111 0.102 88.8 81.6 64.0-132 8.45 20
Bromomethane 0.125 0.113 0.116 90.4 92.8 56.0-147 2.62 20
n-Butylbenzene 0.125 0.128 0.132 102 106 68.0-135 3.08 20
sec-Butylbenzene 0.125 0.130 0.127 104 102 74.0-130 2.33 20
tert-Butylbenzene 0.125 0.132 0.135 106 108 75.0-127 2.25 20
Carbon tetrachloride 0.125 0.115 0.106 92.0 84.8 66.0-128 8.14 20
Chlorobenzene 0.125 0.119 0.117 95.2 93.6 76.0-128 1.69 20
Chlorodibromomethane 0.125 0.118 0.115 94.4 92.0 74.0-127 2.58 20
Chloroethane 0.125 0.105 0.109 84.0 87.2 61.0-134 3.74 20
Chloroform 0.125 0.118 0.114 94.4 91.2 72.0-123 3.45 20
Chloromethane 0.125 0.125 0.128 100 102 51.0-138 2.37 20
2-Chlorotoluene 0.125 0.130 0.124 104 99.2 75.0-124 4.72 20
4-Chlorotoluene 0.125 0.138 0.133 110 106 75.0-124 3.69 20
1,2-Dibromo-3-Chloropropane 0.125 0.129 0.130 103 104 59.0-130 0.772 20
1,2-Dibromoethane 0.125 0.121 0.115 96.8 92.0 74.0-128 5.08 20
Dibromomethane 0.125 0.124 0.121 99.2 96.8 75.0-122 2.45 20
1,2-Dichlorobenzene 0.125 0.122 0.120 97.6 96.0 76.0-124 1.65 20
1,3-Dichlorobenzene 0.125 0.118 0.116 94.4 92.8 76.0-125 1.71 20
1,4-Dichlorobenzene 0.125 0.125 0.121 100 96.8 77.0-121 3.25 20
Dichlorodifluoromethane 0.125 0.131 0.126 105 101 43.0-156 3.89 20
1,1-Dichloroethane 0.125 0.119 0.117 95.2 93.6 70.0-127 1.69 20
1,2-Dichloroethane 0.125 0.143 0.138 114 110 65.0-131 3.56 20
1,1-Dichloroethene 0.125 0.105 0.110 84.0 88.0 65.0-131 4.65 20
cis-1,2-Dichloroethene 0.125 0.104 0.106 83.2 84.8 73.0-125 1.90 20
trans-1,2-Dichloroethene 0.125 0.100 0.0985 80.0 78.8 71.0-125 1.51 20
1,2-Dichloropropane 0.125 0.125 0.121 100 96.8 74.0-125 3.25 20
1,1-Dichloropropene 0.125 0.126 0.123 101 98.4 73.0-125 2.41 20
1,3-Dichloropropane 0.125 0.127 0.123 102 98.4 80.0-125 3.20 20
cis-1,3-Dichloropropene 0.125 0.132 0.127 106 102 76.0-127 3.86 20
trans-1,3-Dichloropropene 0.125 0.130 0.123 104 98.4 73.0-127 5.53 20
2,2-Dichloropropane 0.125 0.110 0.108 88.0 86.4 59.0-135 1.83 20
Di-isopropyl ether 0.125 0.132 0.127 106 102 60.0-136 3.86 20
Ethylbenzene 0.125 0.109 0.110 87.2 88.0 74.0-126 0.913 20
Hexachloro-1,3-butadiene 0.125 0.130 0.123 104 98.4 57.0-150 5.53 20
Isopropylbenzene 0.125 0.114 0.114 91.2 91.2 72.0-127 0.000 20
p-Isopropyltoluene 0.125 0.129 0.127 103 102 72.0-133 1.56 20
2-Butanone (MEK)0.625 0.897 0.819 144 131 30.0-160 9.09 24
Methylene Chloride 0.125 0.106 0.100 84.8 80.0 68.0-123 5.83 20
4-Methyl-2-pentanone (MIBK) 0.625 0.855 0.801 137 128 56.0-143 6.52 20
Methyl tert-butyl ether 0.125 0.108 0.0978 86.4 78.2 66.0-132 9.91 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052852
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3920204-1 05/02/23 20:42 • (LCSD) R3920204-2 05/02/23 21:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.134 0.131 107 105 59.0-130 2.26 20
n-Propylbenzene 0.125 0.138 0.139 110 111 74.0-126 0.722 20
Styrene 0.125 0.114 0.111 91.2 88.8 72.0-127 2.67 20
1,1,1,2-Tetrachloroethane 0.125 0.113 0.110 90.4 88.0 74.0-129 2.69 20
1,1,2,2-Tetrachloroethane 0.125 0.139 0.129 111 103 68.0-128 7.46 20
1,1,2-Trichlorotrifluoroethane 0.125 0.0722 0.0719 57.8 57.5 61.0-139 J4 J4 0.416 20
Tetrachloroethene 0.125 0.115 0.113 92.0 90.4 70.0-136 1.75 20
Toluene 0.125 0.117 0.115 93.6 92.0 75.0-121 1.72 20
1,2,3-Trichlorobenzene 0.125 0.130 0.126 104 101 59.0-139 3.12 20
1,2,4-Trichlorobenzene 0.125 0.128 0.126 102 101 62.0-137 1.57 20
1,1,1-Trichloroethane 0.125 0.108 0.107 86.4 85.6 69.0-126 0.930 20
1,1,2-Trichloroethane 0.125 0.116 0.110 92.8 88.0 78.0-123 5.31 20
Trichloroethene 0.125 0.115 0.116 92.0 92.8 76.0-126 0.866 20
Trichlorofluoromethane 0.125 0.126 0.118 101 94.4 61.0-142 6.56 20
1,2,3-Trichloropropane 0.125 0.145 0.130 116 104 67.0-129 10.9 20
1,2,4-Trimethylbenzene 0.125 0.130 0.125 104 100 70.0-126 3.92 20
1,2,3-Trimethylbenzene 0.125 0.128 0.127 102 102 74.0-124 0.784 20
1,3,5-Trimethylbenzene 0.125 0.131 0.130 105 104 73.0-127 0.766 20
Vinyl chloride 0.125 0.140 0.139 112 111 63.0-134 0.717 20
Xylenes, Total 0.375 0.338 0.334 90.1 89.1 72.0-127 1.19 20
(S) Toluene-d8 105 104 75.0-131
(S) 4-Bromofluorobenzene 90.6 89.9 67.0-138
(S) 1,2-Dichloroethane-d4 116 116 70.0-130
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/02/23 23:02 • (MS) R3920204-4 05/03/23 06:58 • (MSD) R3920204-5 05/03/23 07:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 1.00 ND 0.205 3.94 20.5 394 1.04 10.0-160 J3 J5 180 40
Acrylonitrile 1.00 ND 0.920 0.887 91.8 88.6 1.04 10.0-160 3.58 40
Benzene 0.200 ND 0.200 0.242 100 121 1.04 10.0-149 18.8 37
Bromobenzene 0.200 ND 0.220 0.280 110 140 1.04 10.0-156 24.0 38
Bromodichloromethane 0.200 ND 0.193 0.234 96.2 117 1.04 10.0-143 19.5 37
Bromoform 0.200 ND 0.150 0.174 74.8 86.9 1.04 10.0-146 15.0 36
Bromomethane 0.200 ND 0.177 0.231 88.5 115 1.04 10.0-149 26.4 38
n-Butylbenzene 0.200 ND 0.223 0.276 112 138 1.04 10.0-160 21.0 40
sec-Butylbenzene 0.200 ND 0.236 0.294 118 147 1.04 10.0-159 22.1 39
tert-Butylbenzene 0.200 ND 0.236 0.305 118 152 1.04 10.0-156 25.6 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052852
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-01
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/02/23 23:02 • (MS) R3920204-4 05/03/23 06:58 • (MSD) R3920204-5 05/03/23 07:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.200 ND 0.186 0.230 93.1 115 1.04 10.0-145 20.7 37
Chlorobenzene 0.200 ND 0.185 0.230 92.3 115 1.04 10.0-152 21.6 39
Chlorodibromomethane 0.200 ND 0.174 0.216 86.9 108 1.04 10.0-146 21.3 37
Chloroethane 0.200 ND 0.131 0.196 65.4 97.7 1.04 10.0-146 39.6 40
Chloroform 0.200 ND 0.193 0.228 96.2 114 1.04 10.0-146 16.8 37
Chloromethane 0.200 ND 0.220 0.285 110 142 1.04 10.0-159 25.6 37
2-Chlorotoluene 0.200 ND 0.197 0.271 98.5 135 1.04 10.0-159 31.6 38
4-Chlorotoluene 0.200 ND 0.240 0.302 120 151 1.04 10.0-155 22.7 39
1,2-Dibromo-3-Chloropropane 0.200 ND 0.166 0.197 83.1 98.5 1.04 10.0-151 16.9 39
1,2-Dibromoethane 0.200 ND 0.183 0.226 91.5 113 1.04 10.0-148 21.1 34
Dibromomethane 0.200 ND 0.191 0.203 95.4 102 1.04 10.0-147 6.25 35
1,2-Dichlorobenzene 0.200 ND 0.182 0.223 90.8 112 1.04 10.0-155 20.5 37
1,3-Dichlorobenzene 0.200 ND 0.194 0.240 96.9 120 1.04 10.0-153 21.3 38
1,4-Dichlorobenzene 0.200 ND 0.193 0.245 96.2 122 1.04 10.0-151 23.9 38
Dichlorodifluoromethane 0.200 ND 0.253 0.302 126 151 1.04 10.0-160 17.8 35
1,1-Dichloroethane 0.200 ND 0.197 0.243 98.5 122 1.04 10.0-147 21.0 37
1,2-Dichloroethane 0.200 ND 0.228 0.267 114 133 1.04 10.0-148 15.6 35
1,1-Dichloroethene 0.200 ND 0.168 0.247 83.8 123 1.04 10.0-155 J3 37.9 37
cis-1,2-Dichloroethene 0.200 ND 0.180 0.213 90.0 106 1.04 10.0-149 16.5 37
trans-1,2-Dichloroethene 0.200 ND 0.176 0.206 87.7 103 1.04 10.0-150 16.1 37
1,2-Dichloropropane 0.200 ND 0.210 0.250 105 125 1.04 10.0-148 17.4 37
1,1-Dichloropropene 0.200 ND 0.223 0.271 112 135 1.04 10.0-153 19.3 35
1,3-Dichloropropane 0.200 ND 0.199 0.251 99.2 125 1.04 10.0-154 23.3 35
cis-1,3-Dichloropropene 0.200 ND 0.211 0.253 105 126 1.04 10.0-151 17.9 37
trans-1,3-Dichloropropene 0.200 ND 0.197 0.260 98.5 130 1.04 10.0-148 27.6 37
2,2-Dichloropropane 0.200 ND 0.150 0.197 74.7 98.5 1.04 10.0-138 27.5 36
Di-isopropyl ether 0.200 ND 0.220 0.259 110 129 1.04 10.0-147 16.1 36
Ethylbenzene 0.200 ND 0.180 0.223 89.4 111 1.04 10.0-160 21.4 38
Hexachloro-1,3-butadiene 0.200 ND 0.194 0.297 96.9 148 1.04 10.0-160 J3 42.0 40
Isopropylbenzene 0.200 ND 0.183 0.220 91.1 110 1.04 10.0-155 18.3 38
p-Isopropyltoluene 0.200 ND 0.231 0.274 115 137 1.04 10.0-160 17.1 40
2-Butanone (MEK)1.00 ND 1.31 1.49 131 149 1.04 10.0-160 13.0 40
Methylene Chloride 0.200 ND 0.165 0.206 82.3 103 1.04 10.0-141 22.4 37
4-Methyl-2-pentanone (MIBK) 1.00 ND 1.23 1.48 122 148 1.04 10.0-160 18.6 35
Methyl tert-butyl ether 0.200 ND 0.151 0.179 75.5 89.2 1.04 11.0-147 16.7 35
Naphthalene 0.200 ND 0.162 0.247 80.8 123 1.04 10.0-160 J3 41.5 36
n-Propylbenzene 0.200 ND 0.257 0.317 128 158 1.04 10.0-158 20.9 38
Styrene 0.200 ND 0.177 0.217 86.2 106 1.04 10.0-160 20.3 40
1,1,1,2-Tetrachloroethane 0.200 ND 0.169 0.203 84.6 102 1.04 10.0-149 18.2 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052852
Volatile Organic Compounds (GC/MS) by Method 8260B L1607939-01
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/02/23 23:02 • (MS) R3920204-4 05/03/23 06:58 • (MSD) R3920204-5 05/03/23 07:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.200 ND 0.0692 0.154 34.5 76.9 1.04 10.0-160 J3 76.1 35
1,1,2-Trichlorotrifluoroethane 0.200 ND 0.0659 0.102 32.9 50.7 1.04 10.0-160 J3 42.5 36
Tetrachloroethene 0.200 ND 0.190 0.245 94.6 122 1.04 10.0-156 25.5 39
Toluene 0.200 ND 0.197 0.251 96.5 123 1.04 10.0-156 24.1 38
1,2,3-Trichlorobenzene 0.200 ND 0.162 0.268 80.8 134 1.04 10.0-160 J3 49.5 40
1,2,4-Trichlorobenzene 0.200 ND 0.163 0.243 81.5 122 1.04 10.0-160 39.4 40
1,1,1-Trichloroethane 0.200 ND 0.179 0.247 89.2 123 1.04 10.0-144 31.9 35
1,1,2-Trichloroethane 0.200 ND 0.176 0.216 87.7 108 1.04 10.0-160 20.5 35
Trichloroethene 0.200 ND 0.294 0.308 147 154 1.04 10.0-156 4.60 38
Trichlorofluoromethane 0.200 ND 0.173 0.231 86.2 115 1.04 10.0-160 29.0 40
1,2,3-Trichloropropane 0.200 ND 0.214 0.263 107 132 1.04 10.0-156 20.6 35
1,2,4-Trimethylbenzene 0.200 ND 0.222 0.273 109 135 1.04 10.0-160 20.6 36
1,2,3-Trimethylbenzene 0.200 ND 0.213 0.262 106 131 1.04 10.0-160 20.8 36
1,3,5-Trimethylbenzene 0.200 ND 0.230 0.287 115 143 1.04 10.0-160 22.1 38
Vinyl chloride 0.200 ND 0.263 0.327 132 163 1.04 10.0-160 J5 21.4 37
Xylenes, Total 0.601 ND 0.544 0.661 89.8 109 1.04 10.0-160 19.4 38
(S) Toluene-d8 104 108 75.0-131
(S) 4-Bromofluorobenzene 86.6 82.2 67.0-138
(S) 1,2-Dichloroethane-d4 118 111 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2046978
Semi-Volatile Organic Compounds (GC) by Method 8015 L1607939-11,12,13,14
Method Blank (MB)
(MB) R3916576-1 04/22/23 22:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
C10-C28 Diesel Range 0.0549 J 0.0222 0.100
C28-C40 Oil Range U 0.0118 0.100
(S) o-Terphenyl 86.5 52.0-156
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3916576-2 04/22/23 23:04 • (LCSD) R3916576-3 04/22/23 23:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
C10-C28 Diesel Range 1.50 1.57 1.65 105 110 50.0-150 4.97 20
(S) o-Terphenyl 110 103 52.0-156
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2049589
Semi-Volatile Organic Compounds (GC) by Method 8015 L1607939-19,20
Method Blank (MB)
(MB) R3918400-1 04/27/23 18:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
C10-C28 Diesel Range U 0.0222 0.100
C28-C40 Oil Range 0.0357 J 0.0118 0.100
(S) o-Terphenyl 101 52.0-156
Laboratory Control Sample (LCS)
(LCS) R3918400-2 04/27/23 18:39
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
C10-C28 Diesel Range 1.50 1.54 103 50.0-150
(S) o-Terphenyl 117 52.0-156
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/28/23 18:04 • (MS) R3919021-1 04/28/23 18:24 • (MSD) R3919021-2 04/28/23 18:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
C10-C28 Diesel Range 1.43 0.449 1.98 2.07 107 113 1 50.0-150 4.44 20
(S) o-Terphenyl 121 126 52.0-156
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048624
Semi-Volatile Organic Compounds (GC) by Method 8015 L1607939-02,03,04,05
Method Blank (MB)
(MB) R3917888-2 04/27/23 01:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 63.5 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3917888-1 04/27/23 01:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 37.0 74.0 50.0-150
(S) o-Terphenyl 83.9 18.0-148
L1607968-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607968-01 04/27/23 03:43 • (MS) R3917888-3 04/27/23 03:57 • (MSD) R3917888-4 04/27/23 04:11
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
C10-C28 Diesel Range 55.9 8.99 35.9 35.2 48.1 47.0 1 50.0-150 J6 J6 1.94 20
(S) o-Terphenyl 46.8 43.3 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048845
Semi-Volatile Organic Compounds (GC) by Method 8015 L1607939-06,07,08,09,10
Method Blank (MB)
(MB) R3917854-1 04/26/23 15:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 73.0 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3917854-2 04/26/23 15:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 37.6 75.2 50.0-150
(S) o-Terphenyl 84.8 18.0-148
L1608058-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608058-03 04/26/23 15:33 • (MS) R3917854-3 04/26/23 15:47 • (MSD) R3917854-4 04/26/23 16:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 70.0 ND 38.4 50.1 54.9 70.7 1 50.0-150 J3 26.4 20
(S) o-Terphenyl 58.2 76.4 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052920
Semi-Volatile Organic Compounds (GC) by Method 8015 L1607939-01
Method Blank (MB)
(MB) R3920931-1 05/04/23 10:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 95.8 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3920931-2 05/04/23 11:09
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 39.3 78.6 50.0-150
(S) o-Terphenyl 81.2 18.0-148
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/04/23 12:11 • (MS) R3920931-3 05/04/23 12:23 • (MSD) R3920931-4 05/04/23 12:41
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 63.5 ND 405 ND 639 177 25 50.0-150 J5 J3 J5 113 20
(S) o-Terphenyl 63.9 50.0 18.0-148 J7 J7
Sample Narrative:
OS: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047799
Polychlorinated Biphenyls (GC) by Method 8082 L1607939-11,12,13,14
Method Blank (MB)
(MB) R3917426-1 04/25/23 00:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
(S) Decachlorobiphenyl 48.3 10.0-128
(S) Tetrachloro-m-xylene 72.2 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3917426-4 04/25/23 01:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
PCB 1016 0.00250 0.00168 67.2 36.0-135
PCB 1260 0.00250 0.00156 62.4 42.0-131
(S) Decachlorobiphenyl 35.2 10.0-128
(S) Tetrachloro-m-xylene 79.1 10.0-127
L1607700-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607700-03 04/25/23 01:26 • (MS) R3917426-5 04/25/23 01:39 • (MSD) R3917426-6 04/25/23 01:51
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 ND 0.00166 0.00193 66.4 77.2 1 11.0-160 15.0 38
PCB 1260 0.00250 ND 0.00154 0.00164 61.6 65.6 1 20.0-142 P 6.29 27
(S) Decachlorobiphenyl 46.2 47.1 10.0-128
(S) Tetrachloro-m-xylene 72.7 79.7 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047970
Polychlorinated Biphenyls (GC) by Method 8082 L1607939-19,20
Method Blank (MB)
(MB) R3917400-1 04/26/23 00:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
(S) Decachlorobiphenyl 48.7 10.0-128
(S) Tetrachloro-m-xylene 49.2 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3917400-4 04/26/23 00:55
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
PCB 1016 0.00250 0.00230 92.0 36.0-135
PCB 1260 0.00250 0.00202 80.8 42.0-131
(S) Decachlorobiphenyl 27.8 10.0-128
(S) Tetrachloro-m-xylene 65.1 10.0-127
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/26/23 01:25 • (MS) R3917400-5 04/26/23 01:36 • (MSD) R3917400-6 04/26/23 01:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 ND 0.00107 0.00155 42.8 62.0 1 11.0-160 36.6 38
PCB 1260 0.00250 ND 0.000576 0.00126 23.0 50.4 1 20.0-142 J3 74.5 27
(S) Decachlorobiphenyl 12.6 33.9 10.0-128
(S) Tetrachloro-m-xylene 35.1 52.2 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048847
Polychlorinated Biphenyls (GC) by Method 8082 L1607939-02,03,04,05,06,07,08,10
Method Blank (MB)
(MB) R3918161-1 04/26/23 22:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 85.1 10.0-135
(S) Tetrachloro-m-xylene 73.6 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3918161-2 04/26/23 22:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0809 48.4 36.0-141
PCB 1260 0.167 0.102 61.1 37.0-145
(S) Decachlorobiphenyl 79.1 10.0-135
(S) Tetrachloro-m-xylene 68.2 10.0-139
L1608043-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608043-03 04/27/23 00:43 • (MS) R3918161-3 04/27/23 00:53 • (MSD) R3918161-4 04/27/23 01:03
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.186 ND 0.0940 0.101 50.5 54.2 1 10.0-160 7.15 37
PCB 1260 0.186 ND 0.0980 0.111 52.6 59.8 1 10.0-160 12.8 38
(S) Decachlorobiphenyl 68.0 75.5 10.0-135
(S) Tetrachloro-m-xylene 61.4 68.0 10.0-139
Sample Narrative:
OS: spike recovery within historical limits.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2050080
Polychlorinated Biphenyls (GC) by Method 8082 L1607939-09
Method Blank (MB)
(MB) R3918551-1 04/27/23 15:51
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0236 0.0680
PCB 1221 U 0.0236 0.0680
PCB 1232 U 0.0236 0.0680
PCB 1242 U 0.0236 0.0680
PCB 1248 U 0.0148 0.0340
PCB 1254 U 0.0148 0.0340
PCB 1260 U 0.0148 0.0340
(S) Decachlorobiphenyl 92.8 10.0-135
(S) Tetrachloro-m-xylene 84.5 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3918551-2 04/27/23 16:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0979 58.6 36.0-141
PCB 1260 0.167 0.106 63.5 37.0-145
(S) Decachlorobiphenyl 91.3 10.0-135
(S) Tetrachloro-m-xylene 82.4 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2054621
Polychlorinated Biphenyls (GC) by Method 8082 L1607939-01
Method Blank (MB)
(MB) R3921701-1 05/05/23 23:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 52.3 10.0-135
(S) Tetrachloro-m-xylene 59.2 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3921701-4 05/05/23 23:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0867 51.9 36.0-141
PCB 1260 0.167 0.0987 59.1 37.0-145
(S) Decachlorobiphenyl 47.0 10.0-135
(S) Tetrachloro-m-xylene 48.3 10.0-139
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/06/23 00:14 • (MS) R3921701-5 05/06/23 00:24 • (MSD) R3921701-6 05/06/23 00:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 1.06 ND 0.621 0.685 58.5 58.6 5 10.0-160 9.77 37
PCB 1260 1.06 ND 0.546 0.722 51.4 61.8 5 10.0-160 P 27.8 38
(S) Decachlorobiphenyl 69.4 76.5 10.0-135
(S) Tetrachloro-m-xylene 82.9 84.2 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047405
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-11
Method Blank (MB)
(MB) R3916909-2 04/24/23 21:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047405
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-11
Method Blank (MB)
(MB) R3916909-2 04/24/23 21:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 27.2 10.0-120
(S) Phenol-d5 18.5 10.0-120
(S) Nitrobenzene-d5 57.8 10.0-127
(S) 2-Fluorobiphenyl 66.4 10.0-130
(S) 2,4,6-Tribromophenol 65.0 10.0-155
(S) p-Terphenyl-d14 87.7 10.0-128
Laboratory Control Sample (LCS)
(LCS) R3916909-1 04/24/23 21:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acenaphthene 0.0500 0.0291 58.2 41.0-120
Acenaphthylene 0.0500 0.0306 61.2 43.0-120
Anthracene 0.0500 0.0353 70.6 45.0-120
Benzidine 0.100 0.00581 5.81 10.0-120 J4
Benzo(a)anthracene 0.0500 0.0400 80.0 47.0-120
Benzo(b)fluoranthene 0.0500 0.0405 81.0 46.0-120
Benzo(k)fluoranthene 0.0500 0.0393 78.6 46.0-120
Benzo(g,h,i)perylene 0.0500 0.0352 70.4 48.0-121
Benzo(a)pyrene 0.0500 0.0396 79.2 47.0-120
Bis(2-chlorethoxy)methane 0.0500 0.0254 50.8 33.0-120
Bis(2-chloroethyl)ether 0.0500 0.0237 47.4 23.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047405
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-11
Laboratory Control Sample (LCS)
(LCS) R3916909-1 04/24/23 21:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,2-Oxybis(1-Chloropropane) 0.0500 0.0238 47.6 28.0-120
4-Bromophenyl-phenylether 0.0500 0.0363 72.6 45.0-120
2-Chloronaphthalene 0.0500 0.0280 56.0 37.0-120
4-Chlorophenyl-phenylether 0.0500 0.0334 66.8 44.0-120
Chrysene 0.0500 0.0386 77.2 48.0-120
Dibenz(a,h)anthracene 0.0500 0.0360 72.0 47.0-120
1,2-Dichlorobenzene 0.0500 0.0236 47.2 20.0-120
1,3-Dichlorobenzene 0.0500 0.0230 46.0 17.0-120
1,4-Dichlorobenzene 0.0500 0.0235 47.0 18.0-120
3,3-Dichlorobenzidine 0.100 0.0460 46.0 44.0-120
2,4-Dinitrotoluene 0.0500 0.0398 79.6 49.0-124
2,6-Dinitrotoluene 0.0500 0.0352 70.4 46.0-120
Fluoranthene 0.0500 0.0379 75.8 51.0-120
Fluorene 0.0500 0.0327 65.4 47.0-120
Hexachlorobenzene 0.0500 0.0356 71.2 44.0-120
Hexachloro-1,3-butadiene 0.0500 0.0242 48.4 19.0-120
Hexachlorocyclopentadiene 0.0500 0.0154 30.8 15.0-120
Hexachloroethane 0.0500 0.0210 42.0 15.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0325 65.0 49.0-122
Isophorone 0.0500 0.0242 48.4 36.0-120
Naphthalene 0.0500 0.0235 47.0 27.0-120
Nitrobenzene 0.0500 0.0218 43.6 27.0-120
n-Nitrosodimethylamine 0.0500 0.0129 25.8 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0333 66.6 47.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0244 48.8 31.0-120
Phenanthrene 0.0500 0.0353 70.6 46.0-120
Benzylbutyl phthalate 0.0500 0.0386 77.2 43.0-121
Bis(2-ethylhexyl)phthalate 0.0500 0.0371 74.2 43.0-122
Di-n-butyl phthalate 0.0500 0.0378 75.6 49.0-121
Diethyl phthalate 0.0500 0.0352 70.4 48.0-122
Dimethyl phthalate 0.0500 0.0337 67.4 48.0-120
Di-n-octyl phthalate 0.0500 0.0346 69.2 42.0-125
Pyrene 0.0500 0.0403 80.6 47.0-120
1,2,4-Trichlorobenzene 0.0500 0.0247 49.4 24.0-120
4-Chloro-3-methylphenol 0.0500 0.0207 41.4 40.0-120
2-Chlorophenol 0.0500 0.0165 33.0 25.0-120
2,4-Dichlorophenol 0.0500 0.0225 45.0 36.0-120
2,4-Dimethylphenol 0.0500 0.0183 36.6 33.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0472 94.4 38.0-138
2,4-Dinitrophenol 0.0500 0.0403 80.6 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047405
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-11
Laboratory Control Sample (LCS)
(LCS) R3916909-1 04/24/23 21:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Nitrophenol 0.0500 0.0244 48.8 31.0-120
4-Nitrophenol 0.0500 0.0136 27.2 10.0-120
Pentachlorophenol 0.0500 0.0298 59.6 23.0-120
Phenol 0.0500 0.00827 16.5 10.0-120
2,4,6-Trichlorophenol 0.0500 0.0309 61.8 42.0-120
(S) 2-Fluorophenol 21.9 10.0-120
(S) Phenol-d5 15.6 10.0-120
(S) Nitrobenzene-d5 43.8 10.0-127
(S) 2-Fluorobiphenyl 59.1 10.0-130
(S) 2,4,6-Tribromophenol 69.0 10.0-155
(S) p-Terphenyl-d14 83.9 10.0-128
L1608452-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608452-01 04/25/23 01:30 • (MS) R3916909-3 04/25/23 01:52 • (MSD) R3916909-4 04/25/23 02:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acenaphthene 0.0476 ND 0.0371 0.0379 77.9 75.8 1 28.0-120 2.13 25
Acenaphthylene 0.0476 ND 0.0385 0.0389 80.9 77.8 1 31.0-121 1.03 25
Anthracene 0.0476 ND 0.0393 0.0417 82.6 83.4 1 36.0-120 5.93 23
Benzidine 0.0952 ND ND ND 5.81 6.16 1 10.0-120 J6 J6 10.8 37
Benzo(a)anthracene 0.0476 ND 0.0422 0.0446 88.7 89.2 1 39.0-120 5.53 23
Benzo(b)fluoranthene 0.0476 ND 0.0423 0.0449 88.9 89.8 1 37.0-120 5.96 23
Benzo(k)fluoranthene 0.0476 ND 0.0413 0.0431 86.8 86.2 1 37.0-120 4.27 26
Benzo(g,h,i)perylene 0.0476 ND 0.0380 0.0416 79.8 83.2 1 37.0-123 9.05 25
Benzo(a)pyrene 0.0476 ND 0.0421 0.0446 88.4 89.2 1 37.0-120 5.77 24
Bis(2-chlorethoxy)methane 0.0476 ND 0.0331 0.0342 69.5 68.4 1 17.0-120 3.27 31
Bis(2-chloroethyl)ether 0.0476 ND 0.0329 0.0341 69.1 68.2 1 14.0-120 3.58 33
2,2-Oxybis(1-Chloropropane) 0.0476 ND 0.0337 0.0346 70.8 69.2 1 18.0-120 2.64 34
4-Bromophenyl-phenylether 0.0476 ND 0.0429 0.0436 90.1 87.2 1 37.0-120 1.62 24
2-Chloronaphthalene 0.0476 ND 0.0362 0.0366 76.1 73.2 1 29.0-120 1.10 28
4-Chlorophenyl-phenylether 0.0476 ND 0.0414 0.0434 87.0 86.8 1 36.0-120 4.72 23
Chrysene 0.0476 ND 0.0416 0.0433 87.4 86.6 1 38.0-120 4.00 23
Dibenz(a,h)anthracene 0.0476 ND 0.0386 0.0419 81.1 83.8 1 36.0-121 8.20 24
1,2-Dichlorobenzene 0.0476 ND 0.0323 0.0331 67.9 66.2 1 18.0-120 2.45 40
1,3-Dichlorobenzene 0.0476 ND 0.0315 0.0322 66.2 64.4 1 15.0-120 2.20 40
1,4-Dichlorobenzene 0.0476 ND 0.0318 0.0327 66.8 65.4 1 17.0-120 2.79 40
3,3-Dichlorobenzidine 0.0952 ND 0.0469 0.0536 49.3 53.6 1 10.0-134 13.3 30
2,4-Dinitrotoluene 0.0476 ND 0.0461 0.0488 96.8 97.6 1 39.0-125 5.69 25
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047405
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-11
L1608452-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608452-01 04/25/23 01:30 • (MS) R3916909-3 04/25/23 01:52 • (MSD) R3916909-4 04/25/23 02:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
2,6-Dinitrotoluene 0.0476 ND 0.0437 0.0442 91.8 88.4 1 36.0-120 1.14 27
Fluoranthene 0.0476 ND 0.0410 0.0442 86.1 88.4 1 41.0-121 7.51 22
Fluorene 0.0476 ND 0.0401 0.0416 84.2 83.2 1 37.0-120 3.67 24
Hexachlorobenzene 0.0476 ND 0.0413 0.0425 86.8 85.0 1 35.0-122 2.86 24
Hexachloro-1,3-butadiene 0.0476 ND 0.0320 0.0329 67.2 65.8 1 12.0-120 2.77 34
Hexachlorocyclopentadiene 0.0476 ND 0.0248 0.0271 52.1 54.2 1 10.0-120 8.86 33
Hexachloroethane 0.0476 ND 0.0291 0.0298 61.1 59.6 1 10.0-120 2.38 40
Indeno(1,2,3-cd)pyrene 0.0476 ND 0.0354 0.0382 74.4 76.4 1 38.0-125 7.61 24
Isophorone 0.0476 ND 0.0320 0.0329 67.2 65.8 1 21.0-120 2.77 27
Naphthalene 0.0476 ND 0.0304 0.0307 63.9 61.4 1 10.0-120 0.982 31
Nitrobenzene 0.0476 ND 0.0280 0.0286 58.8 57.2 1 12.0-120 2.12 30
n-Nitrosodimethylamine 0.0476 ND 0.0175 0.0200 36.8 40.0 1 10.0-120 13.3 40
n-Nitrosodiphenylamine 0.0476 ND 0.0373 0.0382 78.4 76.4 1 37.0-120 2.38 24
n-Nitrosodi-n-propylamine 0.0476 ND 0.0359 0.0365 75.4 73.0 1 16.0-120 1.66 30
Phenanthrene 0.0476 ND 0.0395 0.0410 83.0 82.0 1 33.0-120 3.73 22
Benzylbutyl phthalate 0.0476 ND 0.0422 0.0437 88.7 87.4 1 34.0-126 3.49 24
Bis(2-ethylhexyl)phthalate 0.0476 ND 0.0398 0.0418 83.6 83.6 1 33.0-126 4.90 25
Di-n-butyl phthalate 0.0476 ND 0.0425 0.0442 85.2 84.5 1 35.0-128 3.92 23
Diethyl phthalate 0.0476 ND 0.0418 0.0436 87.8 87.2 1 39.0-125 4.22 24
Dimethyl phthalate 0.0476 ND 0.0415 0.0422 87.2 84.4 1 37.0-120 1.67 24
Di-n-octyl phthalate 0.0476 ND 0.0370 0.0398 77.7 79.6 1 25.0-135 7.29 26
Pyrene 0.0476 ND 0.0439 0.0449 92.2 89.8 1 39.0-120 2.25 22
1,2,4-Trichlorobenzene 0.0476 ND 0.0316 0.0325 66.4 65.0 1 15.0-120 2.81 31
4-Chloro-3-methylphenol 0.0476 ND 0.0267 0.0323 56.1 64.6 1 26.0-120 19.0 27
2-Chlorophenol 0.0476 ND 0.0238 0.0289 50.0 57.8 1 18.0-120 19.4 34
2,4-Dichlorophenol 0.0476 ND 0.0291 0.0344 61.1 68.8 1 19.0-120 16.7 27
2,4-Dimethylphenol 0.0476 ND 0.0242 0.0282 50.8 56.4 1 15.0-120 15.3 28
4,6-Dinitro-2-methylphenol 0.0476 ND 0.0527 0.0551 111 110 1 10.0-144 4.45 39
2,4-Dinitrophenol 0.0476 ND 0.0519 0.0554 109 111 1 10.0-120 6.52 40
2-Nitrophenol 0.0476 ND 0.0324 0.0353 68.1 70.6 1 20.0-120 8.57 30
4-Nitrophenol 0.0476 ND 0.0156 0.0196 32.8 39.2 1 10.0-120 22.7 40
Pentachlorophenol 0.0476 ND 0.0385 0.0379 80.9 75.8 1 10.0-128 1.57 37
Phenol 0.0476 ND 0.0116 0.0138 24.4 27.6 1 10.0-120 17.3 40
2,4,6-Trichlorophenol 0.0476 ND 0.0392 0.0413 82.4 82.6 1 26.0-120 5.22 31
(S) 2-Fluorophenol 30.8 36.7 10.0-120
(S) Phenol-d5 22.7 25.3 10.0-120
(S) Nitrobenzene-d5 57.9 56.2 10.0-127
(S) 2-Fluorobiphenyl 76.5 74.3 10.0-130
(S) 2,4,6-Tribromophenol 80.5 79.5 10.0-155
(S) p-Terphenyl-d14 91.5 91.2 10.0-128
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-12,13,14
Method Blank (MB)
(MB) R3918420-2 04/27/23 17:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-12,13,14
Method Blank (MB)
(MB) R3918420-2 04/27/23 17:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 20.2 10.0-120
(S) Phenol-d5 14.4 10.0-120
(S) Nitrobenzene-d5 43.8 10.0-127
(S) 2-Fluorobiphenyl 50.6 10.0-130
(S) 2,4,6-Tribromophenol 51.5 10.0-155
(S) p-Terphenyl-d14 80.0 10.0-128
Laboratory Control Sample (LCS)
(LCS) R3918420-1 04/27/23 17:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acenaphthene 0.0500 0.0325 65.0 41.0-120
Acenaphthylene 0.0500 0.0344 68.8 43.0-120
Anthracene 0.0500 0.0365 73.0 45.0-120
Benzidine 0.100 0.00570 5.70 10.0-120 J4
Benzo(a)anthracene 0.0500 0.0407 81.4 47.0-120
Benzo(b)fluoranthene 0.0500 0.0438 87.6 46.0-120
Benzo(k)fluoranthene 0.0500 0.0416 83.2 46.0-120
Benzo(g,h,i)perylene 0.0500 0.0348 69.6 48.0-121
Benzo(a)pyrene 0.0500 0.0408 81.6 47.0-120
Bis(2-chlorethoxy)methane 0.0500 0.0293 58.6 33.0-120
Bis(2-chloroethyl)ether 0.0500 0.0289 57.8 23.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-12,13,14
Laboratory Control Sample (LCS)
(LCS) R3918420-1 04/27/23 17:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,2-Oxybis(1-Chloropropane) 0.0500 0.0278 55.6 28.0-120
4-Bromophenyl-phenylether 0.0500 0.0387 77.4 45.0-120
2-Chloronaphthalene 0.0500 0.0318 63.6 37.0-120
4-Chlorophenyl-phenylether 0.0500 0.0351 70.2 44.0-120
Chrysene 0.0500 0.0396 79.2 48.0-120
Dibenz(a,h)anthracene 0.0500 0.0357 71.4 47.0-120
1,2-Dichlorobenzene 0.0500 0.0265 53.0 20.0-120
1,3-Dichlorobenzene 0.0500 0.0253 50.6 17.0-120
1,4-Dichlorobenzene 0.0500 0.0259 51.8 18.0-120
3,3-Dichlorobenzidine 0.100 0.0581 58.1 44.0-120
2,4-Dinitrotoluene 0.0500 0.0402 80.4 49.0-124
2,6-Dinitrotoluene 0.0500 0.0382 76.4 46.0-120
Fluoranthene 0.0500 0.0353 70.6 51.0-120
Fluorene 0.0500 0.0345 69.0 47.0-120
Hexachlorobenzene 0.0500 0.0381 76.2 44.0-120
Hexachloro-1,3-butadiene 0.0500 0.0250 50.0 19.0-120
Hexachlorocyclopentadiene 0.0500 0.0141 28.2 15.0-120
Hexachloroethane 0.0500 0.0216 43.2 15.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0320 64.0 49.0-122
Isophorone 0.0500 0.0271 54.2 36.0-120
Naphthalene 0.0500 0.0267 53.4 27.0-120
Nitrobenzene 0.0500 0.0257 51.4 27.0-120
n-Nitrosodimethylamine 0.0500 0.0173 34.6 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0369 73.8 47.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0282 56.4 31.0-120
Phenanthrene 0.0500 0.0366 73.2 46.0-120
Benzylbutyl phthalate 0.0500 0.0403 80.6 43.0-121
Bis(2-ethylhexyl)phthalate 0.0500 0.0361 72.2 43.0-122
Di-n-butyl phthalate 0.0500 0.0353 70.6 49.0-121
Diethyl phthalate 0.0500 0.0359 71.8 48.0-122
Dimethyl phthalate 0.0500 0.0356 71.2 48.0-120
Di-n-octyl phthalate 0.0500 0.0313 62.6 42.0-125
Pyrene 0.0500 0.0483 96.6 47.0-120
1,2,4-Trichlorobenzene 0.0500 0.0271 54.2 24.0-120
4-Chloro-3-methylphenol 0.0500 0.0230 46.0 40.0-120
2-Chlorophenol 0.0500 0.0212 42.4 25.0-120
2,4-Dichlorophenol 0.0500 0.0274 54.8 36.0-120
2,4-Dimethylphenol 0.0500 0.0201 40.2 33.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0471 94.2 38.0-138
2,4-Dinitrophenol 0.0500 0.0369 73.8 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-12,13,14
Laboratory Control Sample (LCS)
(LCS) R3918420-1 04/27/23 17:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Nitrophenol 0.0500 0.0295 59.0 31.0-120
4-Nitrophenol 0.0500 0.0117 23.4 10.0-120
Pentachlorophenol 0.0500 0.0266 53.2 23.0-120
Phenol 0.0500 0.0111 22.2 10.0-120
2,4,6-Trichlorophenol 0.0500 0.0359 71.8 42.0-120
(S) 2-Fluorophenol 32.9 10.0-120
(S) Phenol-d5 24.5 10.0-120
(S) Nitrobenzene-d5 57.5 10.0-127
(S) 2-Fluorobiphenyl 74.8 10.0-130
(S) 2,4,6-Tribromophenol 82.5 10.0-155
(S) p-Terphenyl-d14 110 10.0-128
L1608100-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608100-05 04/28/23 00:24 • (MS) R3918420-3 04/28/23 00:46 • (MSD) R3918420-4 04/28/23 01:08
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acenaphthene 0.500 ND ND ND 85.4 78.4 4000 28.0-120 8.55 25
Acenaphthylene 0.500 ND ND ND 0.000 0.000 4000 31.0-121 J6 J6 0.000 25
Anthracene 0.500 ND ND ND 108 0.000 4000 36.0-120 J3 J6 200 23
Benzidine 1.00 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 37
Benzo(a)anthracene 0.500 ND ND ND 0.000 0.000 4000 39.0-120 J6 J6 0.000 23
Benzo(b)fluoranthene 0.500 ND ND ND 141 108 4000 37.0-120 J5 J3 26.8 23
Benzo(k)fluoranthene 0.500 ND ND ND 128 0.000 4000 37.0-120 J5 J3 J6 200 26
Benzo(g,h,i)perylene 0.500 ND ND ND 0.000 0.000 4000 37.0-123 J6 J6 0.000 25
Benzo(a)pyrene 0.500 ND ND ND 107 92.8 4000 37.0-120 14.6 24
Bis(2-chlorethoxy)methane 0.500 ND ND ND 0.000 0.000 4000 17.0-120 J6 J6 0.000 31
Bis(2-chloroethyl)ether 0.500 ND ND ND 0.000 0.000 4000 14.0-120 J6 J6 0.000 33
2,2-Oxybis(1-Chloropropane) 0.500 ND ND ND 0.000 0.000 4000 18.0-120 J6 J6 0.000 34
4-Bromophenyl-phenylether 0.500 ND ND ND 0.000 0.000 4000 37.0-120 J6 J6 0.000 24
2-Chloronaphthalene 0.500 ND ND ND 71.8 54.6 4000 29.0-120 27.2 28
4-Chlorophenyl-phenylether 0.500 ND ND ND 0.000 0.000 4000 36.0-120 J6 J6 0.000 23
Chrysene 0.500 ND ND ND 0.000 0.000 4000 38.0-120 J6 J6 0.000 23
Dibenz(a,h)anthracene 0.500 ND ND ND 65.4 52.6 4000 36.0-121 21.7 24
1,2-Dichlorobenzene 0.500 ND ND ND 0.000 0.000 4000 18.0-120 J6 J6 0.000 40
1,3-Dichlorobenzene 0.500 ND ND ND 0.000 0.000 4000 15.0-120 J6 J6 0.000 40
1,4-Dichlorobenzene 0.500 ND ND ND 0.000 0.000 4000 17.0-120 J6 J6 0.000 40
3,3-Dichlorobenzidine 1.00 ND ND ND 0.000 0.000 4000 10.0-134 J6 J6 0.000 30
2,4-Dinitrotoluene 0.500 ND ND ND 0.000 0.000 4000 39.0-125 J6 J6 0.000 25
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-12,13,14
L1608100-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608100-05 04/28/23 00:24 • (MS) R3918420-3 04/28/23 00:46 • (MSD) R3918420-4 04/28/23 01:08
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
2,6-Dinitrotoluene 0.500 ND ND ND 0.000 0.000 4000 36.0-120 J6 J6 0.000 27
Fluoranthene 0.500 ND ND ND 92.8 0.000 4000 41.0-121 J3 J6 200 22
Fluorene 0.500 ND ND ND 100 101 4000 37.0-120 0.993 24
Hexachlorobenzene 0.500 ND ND ND 0.000 0.000 4000 35.0-122 J6 J6 0.000 24
Hexachloro-1,3-butadiene 0.500 ND ND ND 0.000 0.000 4000 12.0-120 J6 J6 0.000 34
Hexachlorocyclopentadiene 0.500 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 33
Hexachloroethane 0.500 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 40
Indeno(1,2,3-cd)pyrene 0.500 ND ND ND 0.000 0.000 4000 38.0-125 J6 J6 0.000 24
Isophorone 0.500 ND ND ND 0.000 0.000 4000 21.0-120 J6 J6 0.000 27
Naphthalene 0.500 ND ND ND 81.8 15.8 4000 10.0-120 26.9 31
Nitrobenzene 0.500 ND ND ND 0.000 0.000 4000 12.0-120 J6 J6 0.000 30
n-Nitrosodimethylamine 0.500 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 40
n-Nitrosodiphenylamine 0.500 ND ND ND 0.000 0.000 4000 37.0-120 J6 J6 0.000 24
n-Nitrosodi-n-propylamine 0.500 ND ND ND 0.000 0.000 4000 16.0-120 J6 J6 0.000 30
Phenanthrene 0.500 ND ND ND 141 93.4 4000 33.0-120 J5 J3 40.3 22
Benzylbutyl phthalate 0.500 ND ND ND 0.000 0.000 4000 34.0-126 J6 J6 0.000 24
Bis(2-ethylhexyl)phthalate 0.500 ND ND ND 0.000 0.000 4000 33.0-126 J6 J6 0.000 25
Di-n-butyl phthalate 0.500 ND ND ND 0.000 0.000 4000 35.0-128 J6 J6 0.000 23
Diethyl phthalate 0.500 ND ND ND 0.000 0.000 4000 39.0-125 J6 J6 0.000 24
Dimethyl phthalate 0.500 ND ND ND 0.000 0.000 4000 37.0-120 J6 J6 0.000 24
Di-n-octyl phthalate 0.500 ND ND ND 0.000 0.000 4000 25.0-135 J6 J6 0.000 26
Pyrene 0.500 ND ND ND 142 115 4000 39.0-120 J5 20.8 22
1,2,4-Trichlorobenzene 0.500 ND ND ND 0.000 0.000 4000 15.0-120 J6 J6 0.000 31
4-Chloro-3-methylphenol 0.500 ND ND ND 0.000 0.000 4000 26.0-120 J6 J6 0.000 27
2-Chlorophenol 0.500 ND ND ND 0.000 0.000 4000 18.0-120 J6 J6 0.000 34
2,4-Dichlorophenol 0.500 ND ND ND 0.000 0.000 4000 19.0-120 J6 J6 0.000 27
2,4-Dimethylphenol 0.500 ND ND ND 0.000 0.000 4000 15.0-120 J6 J6 0.000 28
4,6-Dinitro-2-methylphenol 0.500 ND ND ND 0.000 0.000 4000 10.0-144 J6 J6 0.000 39
2,4-Dinitrophenol 0.500 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 40
2-Nitrophenol 0.500 ND ND ND 0.000 0.000 4000 20.0-120 J6 J6 0.000 30
4-Nitrophenol 0.500 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 40
Pentachlorophenol 0.500 ND ND ND 0.000 0.000 4000 10.0-128 J6 J6 0.000 37
Phenol 0.500 ND ND ND 0.000 0.000 4000 10.0-120 J6 J6 0.000 40
2,4,6-Trichlorophenol 0.500 ND ND ND 0.000 0.000 4000 26.0-120 J6 J6 0.000 31
(S) 2-Fluorophenol 0.000 0.000 10.0-120 J7 J7
(S) Phenol-d5 0.000 0.000 10.0-120 J7 J7
(S) Nitrobenzene-d5 0.000 0.000 10.0-127 J7 J7
(S) 2-Fluorobiphenyl 0.000 0.000 10.0-130 J7 J7
(S) 2,4,6-Tribromophenol 0.000 0.000 10.0-155 J7 J7
(S) p-Terphenyl-d14 0.000 0.000 10.0-128 J7 J7
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048000
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-12,13,14
L1608100-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608100-05 04/28/23 00:24 • (MS) R3918420-3 04/28/23 00:46 • (MSD) R3918420-4 04/28/23 01:08
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Sample Narrative:
OS: Dilution and surrogate failure due to matrix interference.
MS: Dilution and surrogate failure due to matrix interference.
MSD: Dilution and surrogate failure due to matrix interference.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-19,20
Method Blank (MB)
(MB) R3917390-2 04/25/23 21:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-19,20
Method Blank (MB)
(MB) R3917390-2 04/25/23 21:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 36.6 10.0-120
(S) Phenol-d5 22.9 10.0-120
(S) Nitrobenzene-d5 64.7 10.0-127
(S) 2-Fluorobiphenyl 70.4 10.0-130
(S) 2,4,6-Tribromophenol 57.0 10.0-155
(S) p-Terphenyl-d14 76.8 10.0-128
Laboratory Control Sample (LCS)
(LCS) R3917390-1 04/25/23 21:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acenaphthene 0.0500 0.0422 84.4 41.0-120
Acenaphthylene 0.0500 0.0451 90.2 43.0-120
Anthracene 0.0500 0.0441 88.2 45.0-120
Benzidine 0.100 0.00547 5.47 10.0-120 J4
Benzo(a)anthracene 0.0500 0.0478 95.6 47.0-120
Benzo(b)fluoranthene 0.0500 0.0440 88.0 46.0-120
Benzo(k)fluoranthene 0.0500 0.0441 88.2 46.0-120
Benzo(g,h,i)perylene 0.0500 0.0492 98.4 48.0-121
Benzo(a)pyrene 0.0500 0.0479 95.8 47.0-120
Bis(2-chlorethoxy)methane 0.0500 0.0362 72.4 33.0-120
Bis(2-chloroethyl)ether 0.0500 0.0409 81.8 23.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-19,20
Laboratory Control Sample (LCS)
(LCS) R3917390-1 04/25/23 21:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,2-Oxybis(1-Chloropropane) 0.0500 0.0388 77.6 28.0-120
4-Bromophenyl-phenylether 0.0500 0.0398 79.6 45.0-120
2-Chloronaphthalene 0.0500 0.0412 82.4 37.0-120
4-Chlorophenyl-phenylether 0.0500 0.0380 76.0 44.0-120
Chrysene 0.0500 0.0474 94.8 48.0-120
Dibenz(a,h)anthracene 0.0500 0.0500 100 47.0-120
1,2-Dichlorobenzene 0.0500 0.0387 77.4 20.0-120
1,3-Dichlorobenzene 0.0500 0.0385 77.0 17.0-120
1,4-Dichlorobenzene 0.0500 0.0385 77.0 18.0-120
3,3-Dichlorobenzidine 0.100 0.0654 65.4 44.0-120
2,4-Dinitrotoluene 0.0500 0.0457 91.4 49.0-124
2,6-Dinitrotoluene 0.0500 0.0437 87.4 46.0-120
Fluoranthene 0.0500 0.0452 90.4 51.0-120
Fluorene 0.0500 0.0416 83.2 47.0-120
Hexachlorobenzene 0.0500 0.0389 77.8 44.0-120
Hexachloro-1,3-butadiene 0.0500 0.0299 59.8 19.0-120
Hexachlorocyclopentadiene 0.0500 0.0234 46.8 15.0-120
Hexachloroethane 0.0500 0.0374 74.8 15.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0451 90.2 49.0-122
Isophorone 0.0500 0.0347 69.4 36.0-120
Naphthalene 0.0500 0.0354 70.8 27.0-120
Nitrobenzene 0.0500 0.0361 72.2 27.0-120
n-Nitrosodimethylamine 0.0500 0.0247 49.4 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0425 85.0 47.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0374 74.8 31.0-120
Phenanthrene 0.0500 0.0434 86.8 46.0-120
Benzylbutyl phthalate 0.0500 0.0523 105 43.0-121
Bis(2-ethylhexyl)phthalate 0.0500 0.0534 107 43.0-122
Di-n-butyl phthalate 0.0500 0.0506 101 49.0-121
Diethyl phthalate 0.0500 0.0431 86.2 48.0-122
Dimethyl phthalate 0.0500 0.0416 83.2 48.0-120
Di-n-octyl phthalate 0.0500 0.0525 105 42.0-125
Pyrene 0.0500 0.0453 90.6 47.0-120
1,2,4-Trichlorobenzene 0.0500 0.0322 64.4 24.0-120
4-Chloro-3-methylphenol 0.0500 0.0317 63.4 40.0-120
2-Chlorophenol 0.0500 0.0344 68.8 25.0-120
2,4-Dichlorophenol 0.0500 0.0336 67.2 36.0-120
2,4-Dimethylphenol 0.0500 0.0305 61.0 33.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0539 108 38.0-138
2,4-Dinitrophenol 0.0500 0.0508 102 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-19,20
Laboratory Control Sample (LCS)
(LCS) R3917390-1 04/25/23 21:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Nitrophenol 0.0500 0.0399 79.8 31.0-120
4-Nitrophenol 0.0500 0.0180 36.0 10.0-120
Pentachlorophenol 0.0500 0.0343 68.6 23.0-120
Phenol 0.0500 0.0155 31.0 10.0-120
2,4,6-Trichlorophenol 0.0500 0.0400 80.0 42.0-120
(S) 2-Fluorophenol 46.0 10.0-120
(S) Phenol-d5 29.3 10.0-120
(S) Nitrobenzene-d5 68.8 10.0-127
(S) 2-Fluorobiphenyl 87.1 10.0-130
(S) 2,4,6-Tribromophenol 79.0 10.0-155
(S) p-Terphenyl-d14 86.7 10.0-128
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/26/23 10:58 • (MS) R3918070-1 04/26/23 11:19 • (MSD) R3918070-2 04/26/23 11:41
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acenaphthene 0.0455 ND 0.0263 0.0229 57.8 50.3 1 28.0-120 13.8 25
Acenaphthylene 0.0455 ND 0.0281 0.0238 61.8 52.3 1 31.0-121 16.6 25
Anthracene 0.0455 ND 0.0228 0.0175 50.1 38.5 1 36.0-120 J3 26.3 23
Benzidine 0.0910 ND ND ND 0.000 0.000 1 10.0-120 J6 J6 0.000 37
Benzo(a)anthracene 0.0455 ND 0.0218 0.0172 47.9 37.8 1 39.0-120 J3 J6 23.6 23
Benzo(b)fluoranthene 0.0455 ND 0.0215 0.0173 47.3 38.0 1 37.0-120 21.6 23
Benzo(k)fluoranthene 0.0455 ND 0.0207 0.0168 45.5 36.9 1 37.0-120 J6 20.8 26
Benzo(g,h,i)perylene 0.0455 ND 0.0224 0.0178 49.2 39.1 1 37.0-123 22.9 25
Benzo(a)pyrene 0.0455 ND 0.0205 0.0139 45.1 30.5 1 37.0-120 J3 J6 38.4 24
Bis(2-chlorethoxy)methane 0.0455 ND 0.0263 0.0247 57.8 54.3 1 17.0-120 6.27 31
Bis(2-chloroethyl)ether 0.0455 ND 0.0301 0.0281 66.2 61.8 1 14.0-120 6.87 33
2,2-Oxybis(1-Chloropropane) 0.0455 ND 0.0277 0.0263 60.9 57.8 1 18.0-120 5.19 34
4-Bromophenyl-phenylether 0.0455 ND 0.0225 0.0187 49.5 41.1 1 37.0-120 18.4 24
2-Chloronaphthalene 0.0455 ND 0.0252 0.0217 55.4 47.7 1 29.0-120 14.9 28
4-Chlorophenyl-phenylether 0.0455 ND 0.0235 0.0191 51.6 42.0 1 36.0-120 20.7 23
Chrysene 0.0455 ND 0.0225 0.0179 49.5 39.3 1 38.0-120 22.8 23
Dibenz(a,h)anthracene 0.0455 ND 0.0231 0.0186 50.8 40.9 1 36.0-121 21.6 24
1,2-Dichlorobenzene 0.0455 ND 0.0253 0.0238 55.6 52.3 1 18.0-120 6.11 40
1,3-Dichlorobenzene 0.0455 ND 0.0248 0.0229 54.5 50.3 1 15.0-120 7.97 40
1,4-Dichlorobenzene 0.0455 ND 0.0255 0.0233 56.0 51.2 1 17.0-120 9.02 40
3,3-Dichlorobenzidine 0.0910 ND ND ND 0.000 0.000 1 10.0-134 J6 J6 0.000 30
2,4-Dinitrotoluene 0.0455 ND 0.0329 0.0290 72.3 63.7 1 39.0-125 12.6 25
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048428
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-19,20
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/26/23 10:58 • (MS) R3918070-1 04/26/23 11:19 • (MSD) R3918070-2 04/26/23 11:41
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
2,6-Dinitrotoluene 0.0455 ND 0.0307 0.0282 67.5 62.0 1 36.0-120 8.49 27
Fluoranthene 0.0455 ND 0.0244 0.0207 53.6 45.5 1 41.0-121 16.4 22
Fluorene 0.0455 ND 0.0267 0.0218 58.7 47.9 1 37.0-120 20.2 24
Hexachlorobenzene 0.0455 ND 0.0200 0.0154 44.0 33.8 1 35.0-122 J3 J6 26.0 24
Hexachloro-1,3-butadiene 0.0455 ND 0.0180 0.0152 39.6 33.4 1 12.0-120 16.9 34
Hexachlorocyclopentadiene 0.0455 ND 0.0131 0.0107 28.8 23.5 1 10.0-120 20.2 33
Hexachloroethane 0.0455 ND 0.0247 0.0224 54.3 49.2 1 10.0-120 9.77 40
Indeno(1,2,3-cd)pyrene 0.0455 ND 0.0204 0.0161 44.8 35.4 1 38.0-125 J6 23.6 24
Isophorone 0.0455 ND 0.0258 0.0241 56.7 53.0 1 21.0-120 6.81 27
Naphthalene 0.0455 ND 0.0237 0.0217 52.1 47.7 1 10.0-120 8.81 31
Nitrobenzene 0.0455 ND 0.0287 0.0303 63.1 66.6 1 12.0-120 5.42 30
n-Nitrosodimethylamine 0.0455 ND 0.0175 0.0174 38.5 38.2 1 10.0-120 0.573 40
n-Nitrosodiphenylamine 0.0455 ND 0.0265 0.0222 58.2 48.8 1 37.0-120 17.7 24
n-Nitrosodi-n-propylamine 0.0455 ND 0.0290 0.0272 63.7 59.8 1 16.0-120 6.41 30
Phenanthrene 0.0455 ND 0.0258 0.0223 56.7 49.0 1 33.0-120 14.6 22
Benzylbutyl phthalate 0.0455 ND 0.0304 0.0256 66.8 56.3 1 34.0-126 17.1 24
Bis(2-ethylhexyl)phthalate 0.0455 ND 0.0247 0.0192 54.3 42.2 1 33.0-126 J3 25.1 25
Di-n-butyl phthalate 0.0455 ND 0.0300 0.0255 65.9 56.0 1 35.0-128 16.2 23
Diethyl phthalate 0.0455 ND 0.0306 0.0263 67.3 57.8 1 39.0-125 15.1 24
Dimethyl phthalate 0.0455 ND 0.0289 0.0258 63.5 56.7 1 37.0-120 11.3 24
Di-n-octyl phthalate 0.0455 ND 0.0253 0.0192 55.6 42.2 1 25.0-135 J3 27.4 26
Pyrene 0.0455 ND 0.0251 0.0209 55.2 45.9 1 39.0-120 18.3 22
1,2,4-Trichlorobenzene 0.0455 ND 0.0212 0.0192 46.6 42.2 1 15.0-120 9.90 31
4-Chloro-3-methylphenol 0.0455 ND 0.0182 0.0154 40.0 33.8 1 26.0-120 16.7 27
2-Chlorophenol 0.0455 ND 0.0171 0.0149 37.6 32.7 1 18.0-120 13.8 34
2,4-Dichlorophenol 0.0455 ND 0.0173 0.0143 38.0 31.4 1 19.0-120 19.0 27
2,4-Dimethylphenol 0.0455 ND ND ND 20.4 8.68 1 15.0-120 J3 J6 80.5 28
4,6-Dinitro-2-methylphenol 0.0455 ND 0.0302 0.0231 66.4 50.8 1 10.0-144 26.6 39
2,4-Dinitrophenol 0.0455 ND 0.0304 0.0253 66.8 55.6 1 10.0-120 18.3 40
2-Nitrophenol 0.0455 ND 0.0226 0.0192 49.7 42.2 1 20.0-120 16.3 30
4-Nitrophenol 0.0455 ND 0.0111 0.0106 24.4 23.3 1 10.0-120 4.61 40
Pentachlorophenol 0.0455 ND 0.0212 0.0153 46.6 33.6 1 10.0-128 32.3 37
Phenol 0.0455 ND ND ND 19.6 21.9 1 10.0-120 11.3 40
2,4,6-Trichlorophenol 0.0455 ND 0.0200 0.0160 44.0 35.2 1 26.0-120 22.2 31
(S) 2-Fluorophenol 24.0 22.5 10.0-120
(S) Phenol-d5 18.4 17.3 10.0-120
(S) Nitrobenzene-d5 53.4 49.3 10.0-127
(S) 2-Fluorobiphenyl 54.3 47.4 10.0-130
(S) 2,4,6-Tribromophenol 45.9 32.8 10.0-155
(S) p-Terphenyl-d14 44.8 35.3 10.0-128
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-02,03,04
Method Blank (MB)
(MB) R3918154-2 04/27/23 00:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-02,03,04
Method Blank (MB)
(MB) R3918154-2 04/27/23 00:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 45.9 10.0-122
(S) 2-Fluorobiphenyl 47.1 15.0-120
(S) p-Terphenyl-d14 51.4 10.0-120
(S) Phenol-d5 47.7 10.0-120
(S) 2-Fluorophenol 53.5 12.0-120
(S) 2,4,6-Tribromophenol 42.9 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3918154-1 04/26/23 23:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.354 53.2 38.0-120
Acenaphthylene 0.666 0.358 53.8 40.0-120
Anthracene 0.666 0.372 55.9 42.0-120
Benzidine 1.33 0.331 24.9 10.0-120
Benzo(a)anthracene 0.666 0.389 58.4 44.0-120
Benzo(b)fluoranthene 0.666 0.365 54.8 43.0-120
Benzo(k)fluoranthene 0.666 0.365 54.8 44.0-120
Benzo(g,h,i)perylene 0.666 0.357 53.6 43.0-120
Benzo(a)pyrene 0.666 0.392 58.9 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.296 44.4 20.0-120
Bis(2-chloroethyl)ether 0.666 0.354 53.2 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.345 51.8 23.0-120
4-Bromophenyl-phenylether 0.666 0.336 50.5 40.0-120
2-Chloronaphthalene 0.666 0.347 52.1 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3918154-1 04/26/23 23:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.343 51.5 40.0-120
Chrysene 0.666 0.380 57.1 43.0-120
Dibenz(a,h)anthracene 0.666 0.362 54.4 44.0-120
3,3-Dichlorobenzidine 1.33 0.715 53.8 28.0-120
2,4-Dinitrotoluene 0.666 0.420 63.1 45.0-120
2,6-Dinitrotoluene 0.666 0.369 55.4 42.0-120
Fluoranthene 0.666 0.356 53.5 44.0-120
Fluorene 0.666 0.351 52.7 41.0-120
Hexachlorobenzene 0.666 0.314 47.1 39.0-120
Hexachloro-1,3-butadiene 0.666 0.258 38.7 15.0-120
Hexachlorocyclopentadiene 0.666 0.396 59.5 15.0-120
Hexachloroethane 0.666 0.318 47.7 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.336 50.5 45.0-120
Isophorone 0.666 0.286 42.9 23.0-120
Naphthalene 0.666 0.287 43.1 18.0-120
Nitrobenzene 0.666 0.280 42.0 17.0-120
n-Nitrosodimethylamine 0.666 0.240 36.0 10.0-125
n-Nitrosodiphenylamine 0.666 0.363 54.5 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.343 51.5 26.0-120
Phenanthrene 0.666 0.360 54.1 42.0-120
Benzylbutyl phthalate 0.666 0.433 65.0 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.442 66.4 41.0-120
Di-n-butyl phthalate 0.666 0.382 57.4 43.0-120
Diethyl phthalate 0.666 0.371 55.7 43.0-120
Dimethyl phthalate 0.666 0.365 54.8 43.0-120
Di-n-octyl phthalate 0.666 0.452 67.9 40.0-120
Pyrene 0.666 0.380 57.1 41.0-120
1,2,4-Trichlorobenzene 0.666 0.274 41.1 17.0-120
4-Chloro-3-methylphenol 0.666 0.307 46.1 28.0-120
2-Chlorophenol 0.666 0.360 54.1 28.0-120
2,4-Dichlorophenol 0.666 0.307 46.1 25.0-120
2,4-Dimethylphenol 0.666 0.350 52.6 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.458 68.8 16.0-120
2,4-Dinitrophenol 0.666 0.459 68.9 10.0-120
2-Nitrophenol 0.666 0.344 51.7 20.0-120
4-Nitrophenol 0.666 0.479 71.9 27.0-120
Pentachlorophenol 0.666 0.398 59.8 29.0-120
Phenol 0.666 0.344 51.7 28.0-120
2,4,6-Trichlorophenol 0.666 0.349 52.4 37.0-120
(S) Nitrobenzene-d5 42.6 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3918154-1 04/26/23 23:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 50.5 15.0-120
(S) p-Terphenyl-d14 55.3 10.0-120
(S) Phenol-d5 52.6 10.0-120
(S) 2-Fluorophenol 58.3 12.0-120
(S) 2,4,6-Tribromophenol 52.0 10.0-127
L1607518-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607518-08 04/27/23 04:51 • (MS) R3918154-3 04/27/23 05:11 • (MSD) R3918154-4 04/27/23 05:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.666 ND 0.293 0.256 44.0 38.4 1 18.0-120 13.5 32
Acenaphthylene 0.666 ND 0.294 0.260 44.1 39.0 1 25.0-120 12.3 32
Anthracene 0.666 ND 0.314 0.271 47.1 40.7 1 22.0-120 14.7 29
Benzidine 1.33 ND ND ND 7.08 7.20 1 10.0-120 J6 J6 1.58 40
Benzo(a)anthracene 0.666 ND 0.334 0.299 50.2 44.9 1 25.0-120 11.1 29
Benzo(b)fluoranthene 0.666 ND 0.321 0.296 46.7 42.9 1 19.0-122 8.10 31
Benzo(k)fluoranthene 0.666 ND 0.306 0.273 45.9 41.0 1 23.0-120 11.4 30
Benzo(g,h,i)perylene 0.666 ND 0.294 0.273 44.1 41.0 1 10.0-120 7.41 33
Benzo(a)pyrene 0.666 ND 0.341 0.308 50.2 45.3 1 24.0-120 10.2 30
Bis(2-chlorethoxy)methane 0.666 ND ND ND 38.7 33.8 1 10.0-120 13.7 34
Bis(2-chloroethyl)ether 0.666 ND ND ND 43.7 38.0 1 10.0-120 14.0 40
2,2-Oxybis(1-Chloropropane) 0.666 ND ND ND 44.9 38.4 1 10.0-120 15.5 40
4-Bromophenyl-phenylether 0.666 ND ND ND 43.2 36.9 1 27.0-120 15.7 30
2-Chloronaphthalene 0.666 ND 0.284 0.252 42.6 37.8 1 20.0-120 11.9 32
4-Chlorophenyl-phenylether 0.666 ND ND ND 43.1 37.7 1 24.0-120 13.4 29
Chrysene 0.666 ND 0.326 0.293 47.9 42.9 1 21.0-120 10.7 29
Dibenz(a,h)anthracene 0.666 ND 0.297 0.267 44.6 40.1 1 10.0-120 10.6 32
3,3-Dichlorobenzidine 1.33 ND 0.557 0.480 41.9 36.1 1 10.0-120 14.9 34
2,4-Dinitrotoluene 0.666 ND 0.356 ND 53.5 46.2 1 30.0-120 14.5 31
2,6-Dinitrotoluene 0.666 ND ND ND 48.3 42.6 1 25.0-120 12.5 31
Fluoranthene 0.666 ND 0.317 0.298 45.3 42.4 1 18.0-126 6.18 32
Fluorene 0.666 ND 0.293 0.258 44.0 38.7 1 25.0-120 12.7 30
Hexachlorobenzene 0.666 ND ND ND 40.2 35.4 1 27.0-120 12.7 28
Hexachloro-1,3-butadiene 0.666 ND ND ND 34.5 31.1 1 10.0-120 10.5 38
Hexachlorocyclopentadiene 0.666 ND ND ND 43.8 37.4 1 10.0-120 15.9 40
Hexachloroethane 0.666 ND ND ND 39.2 34.4 1 10.0-120 13.1 40
Indeno(1,2,3-cd)pyrene 0.666 ND 0.289 0.264 43.4 39.6 1 10.0-120 9.04 32
Isophorone 0.666 ND ND ND 36.3 32.4 1 13.0-120 11.4 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048869
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-02,03,04
L1607518-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607518-08 04/27/23 04:51 • (MS) R3918154-3 04/27/23 05:11 • (MSD) R3918154-4 04/27/23 05:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.666 ND 0.246 0.219 36.9 32.9 1 10.0-120 11.6 35
Nitrobenzene 0.666 ND ND ND 36.0 32.0 1 10.0-120 11.9 36
n-Nitrosodimethylamine 0.666 ND ND ND 33.3 27.3 1 10.0-127 19.8 40
n-Nitrosodiphenylamine 0.666 ND ND ND 43.7 37.8 1 17.0-120 14.4 29
n-Nitrosodi-n-propylamine 0.666 ND ND ND 42.3 36.6 1 10.0-120 14.4 37
Phenanthrene 0.666 ND 0.304 0.281 44.5 41.1 1 17.0-120 7.86 31
Benzylbutyl phthalate 0.666 ND 0.364 ND 54.7 47.7 1 23.0-120 13.5 30
Bis(2-ethylhexyl)phthalate 0.666 ND 0.367 ND 55.1 48.2 1 17.0-126 13.4 30
Di-n-butyl phthalate 0.666 ND ND ND 48.6 42.3 1 30.0-120 13.9 29
Diethyl phthalate 0.666 ND ND ND 45.9 40.1 1 26.0-120 13.6 28
Dimethyl phthalate 0.666 ND ND ND 45.8 39.6 1 25.0-120 14.4 29
Di-n-octyl phthalate 0.666 ND 0.386 0.339 58.0 50.9 1 21.0-123 13.0 29
Pyrene 0.666 ND 0.326 0.300 47.0 43.1 1 16.0-121 8.31 32
1,2,4-Trichlorobenzene 0.666 ND ND ND 36.3 32.1 1 12.0-120 12.3 37
4-Chloro-3-methylphenol 0.666 ND ND ND 40.5 34.8 1 15.0-120 15.1 30
2-Chlorophenol 0.666 ND ND ND 44.4 38.9 1 15.0-120 13.3 37
2,4-Dichlorophenol 0.666 ND ND ND 40.1 34.7 1 20.0-120 14.5 31
2,4-Dimethylphenol 0.666 ND ND ND 44.9 39.5 1 10.0-120 12.8 33
4,6-Dinitro-2-methylphenol 0.666 ND 0.410 0.368 61.6 55.3 1 10.0-120 10.8 39
2,4-Dinitrophenol 0.666 ND 0.460 0.408 69.1 61.3 1 10.0-121 12.0 40
2-Nitrophenol 0.666 ND ND ND 45.0 41.6 1 12.0-120 7.97 39
4-Nitrophenol 0.666 ND 0.382 ND 57.4 47.3 1 10.0-137 19.2 32
Pentachlorophenol 0.666 ND 0.354 ND 53.2 42.9 1 10.0-160 21.2 31
Phenol 0.666 ND ND ND 41.6 36.0 1 12.0-120 14.3 38
2,4,6-Trichlorophenol 0.666 ND ND ND 42.0 36.5 1 19.0-120 14.1 32
(S) Nitrobenzene-d5 36.6 34.2 10.0-122
(S) 2-Fluorobiphenyl 42.0 38.1 15.0-120
(S) p-Terphenyl-d14 45.3 41.4 10.0-120
(S) Phenol-d5 43.1 38.1 10.0-120
(S) 2-Fluorophenol 48.8 42.9 12.0-120
(S) 2,4,6-Tribromophenol 45.0 39.9 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-05,06,07,08,09,10
Method Blank (MB)
(MB) R3918190-2 04/27/23 01:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-05,06,07,08,09,10
Method Blank (MB)
(MB) R3918190-2 04/27/23 01:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 43.2 10.0-122
(S) 2-Fluorobiphenyl 55.0 15.0-120
(S) p-Terphenyl-d14 65.5 10.0-120
(S) Phenol-d5 51.4 10.0-120
(S) 2-Fluorophenol 57.5 12.0-120
(S) 2,4,6-Tribromophenol 58.6 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3918190-1 04/27/23 00:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.396 59.5 38.0-120
Acenaphthylene 0.666 0.426 64.0 40.0-120
Anthracene 0.666 0.430 64.6 42.0-120
Benzidine 1.33 0.278 20.9 10.0-120
Benzo(a)anthracene 0.666 0.447 67.1 44.0-120
Benzo(b)fluoranthene 0.666 0.424 63.7 43.0-120
Benzo(k)fluoranthene 0.666 0.417 62.6 44.0-120
Benzo(g,h,i)perylene 0.666 0.435 65.3 43.0-120
Benzo(a)pyrene 0.666 0.458 68.8 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.303 45.5 20.0-120
Bis(2-chloroethyl)ether 0.666 0.345 51.8 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.363 54.5 23.0-120
4-Bromophenyl-phenylether 0.666 0.462 69.4 40.0-120
2-Chloronaphthalene 0.666 0.394 59.2 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-05,06,07,08,09,10
Laboratory Control Sample (LCS)
(LCS) R3918190-1 04/27/23 00:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.436 65.5 40.0-120
Chrysene 0.666 0.433 65.0 43.0-120
Dibenz(a,h)anthracene 0.666 0.435 65.3 44.0-120
3,3-Dichlorobenzidine 1.33 0.686 51.6 28.0-120
2,4-Dinitrotoluene 0.666 0.445 66.8 45.0-120
2,6-Dinitrotoluene 0.666 0.429 64.4 42.0-120
Fluoranthene 0.666 0.448 67.3 44.0-120
Fluorene 0.666 0.408 61.3 41.0-120
Hexachlorobenzene 0.666 0.463 69.5 39.0-120
Hexachloro-1,3-butadiene 0.666 0.362 54.4 15.0-120
Hexachlorocyclopentadiene 0.666 0.396 59.5 15.0-120
Hexachloroethane 0.666 0.324 48.6 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.409 61.4 45.0-120
Isophorone 0.666 0.289 43.4 23.0-120
Naphthalene 0.666 0.321 48.2 18.0-120
Nitrobenzene 0.666 0.279 41.9 17.0-120
n-Nitrosodimethylamine 0.666 0.283 42.5 10.0-125
n-Nitrosodiphenylamine 0.666 0.410 61.6 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.333 50.0 26.0-120
Phenanthrene 0.666 0.408 61.3 42.0-120
Benzylbutyl phthalate 0.666 0.416 62.5 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.424 63.7 41.0-120
Di-n-butyl phthalate 0.666 0.418 62.8 43.0-120
Diethyl phthalate 0.666 0.411 61.7 43.0-120
Dimethyl phthalate 0.666 0.432 64.9 43.0-120
Di-n-octyl phthalate 0.666 0.422 63.4 40.0-120
Pyrene 0.666 0.419 62.9 41.0-120
1,2,4-Trichlorobenzene 0.666 0.347 52.1 17.0-120
4-Chloro-3-methylphenol 0.666 0.342 51.4 28.0-120
2-Chlorophenol 0.666 0.396 59.5 28.0-120
2,4-Dichlorophenol 0.666 0.380 57.1 25.0-120
2,4-Dimethylphenol 0.666 0.330 49.5 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.421 63.2 16.0-120
2,4-Dinitrophenol 0.666 0.314 47.1 10.0-120
2-Nitrophenol 0.666 0.364 54.7 20.0-120
4-Nitrophenol 0.666 0.409 61.4 27.0-120
Pentachlorophenol 0.666 0.453 68.0 29.0-120
Phenol 0.666 0.358 53.8 28.0-120
2,4,6-Trichlorophenol 0.666 0.427 64.1 37.0-120
(S) Nitrobenzene-d5 41.1 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-05,06,07,08,09,10
Laboratory Control Sample (LCS)
(LCS) R3918190-1 04/27/23 00:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 60.1 15.0-120
(S) p-Terphenyl-d14 67.3 10.0-120
(S) Phenol-d5 55.4 10.0-120
(S) 2-Fluorophenol 61.7 12.0-120
(S) 2,4,6-Tribromophenol 74.5 10.0-127
L1608027-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608027-02 04/27/23 04:56 • (MS) R3918190-3 04/27/23 05:17 • (MSD) R3918190-4 04/27/23 05:38
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.666 ND 0.334 0.346 50.2 52.0 1 18.0-120 3.53 32
Acenaphthylene 0.666 ND 0.360 0.373 54.1 56.0 1 25.0-120 3.55 32
Anthracene 0.666 ND 0.353 0.359 53.0 53.9 1 22.0-120 1.69 29
Benzidine 1.33 ND ND ND 31.9 37.7 1 10.0-120 16.6 40
Benzo(a)anthracene 0.666 ND 0.383 0.389 57.5 58.4 1 25.0-120 1.55 29
Benzo(b)fluoranthene 0.666 ND 0.353 0.368 53.0 55.3 1 19.0-122 4.16 31
Benzo(k)fluoranthene 0.666 ND 0.340 0.357 51.1 53.6 1 23.0-120 4.88 30
Benzo(g,h,i)perylene 0.666 ND 0.359 0.377 53.9 56.6 1 10.0-120 4.89 33
Benzo(a)pyrene 0.666 ND 0.386 0.405 58.0 60.8 1 24.0-120 4.80 30
Bis(2-chlorethoxy)methane 0.666 ND ND ND 39.0 40.1 1 10.0-120 2.66 34
Bis(2-chloroethyl)ether 0.666 ND ND ND 46.4 49.1 1 10.0-120 5.66 40
2,2-Oxybis(1-Chloropropane) 0.666 ND ND ND 46.8 47.9 1 10.0-120 2.22 40
4-Bromophenyl-phenylether 0.666 ND 0.391 0.396 58.7 59.5 1 27.0-120 1.27 30
2-Chloronaphthalene 0.666 ND 0.327 0.339 49.1 50.9 1 20.0-120 3.60 32
4-Chlorophenyl-phenylether 0.666 ND 0.375 0.383 56.3 57.5 1 24.0-120 2.11 29
Chrysene 0.666 ND 0.370 0.375 55.6 56.3 1 21.0-120 1.34 29
Dibenz(a,h)anthracene 0.666 ND 0.360 0.374 54.1 56.2 1 10.0-120 3.81 32
3,3-Dichlorobenzidine 1.33 ND 0.601 0.645 45.2 48.5 1 10.0-120 7.06 34
2,4-Dinitrotoluene 0.666 ND 0.381 0.397 57.2 59.6 1 30.0-120 4.11 31
2,6-Dinitrotoluene 0.666 ND 0.366 0.376 55.0 56.5 1 25.0-120 2.70 31
Fluoranthene 0.666 ND 0.380 0.387 57.1 58.1 1 18.0-126 1.83 32
Fluorene 0.666 ND 0.348 0.356 52.3 53.5 1 25.0-120 2.27 30
Hexachlorobenzene 0.666 ND 0.394 0.392 59.2 58.9 1 27.0-120 0.509 28
Hexachloro-1,3-butadiene 0.666 ND ND ND 46.8 48.0 1 10.0-120 2.53 38
Hexachlorocyclopentadiene 0.666 ND ND ND 18.9 21.6 1 10.0-120 13.3 40
Hexachloroethane 0.666 ND ND ND 41.4 42.3 1 10.0-120 2.15 40
Indeno(1,2,3-cd)pyrene 0.666 ND 0.343 0.360 51.5 54.1 1 10.0-120 4.84 32
Isophorone 0.666 ND ND ND 36.6 38.9 1 13.0-120 5.96 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048871
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-05,06,07,08,09,10
L1608027-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608027-02 04/27/23 04:56 • (MS) R3918190-3 04/27/23 05:17 • (MSD) R3918190-4 04/27/23 05:38
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.666 ND 0.285 0.296 41.3 42.9 1 10.0-120 3.79 35
Nitrobenzene 0.666 ND ND ND 36.0 37.5 1 10.0-120 4.08 36
n-Nitrosodimethylamine 0.666 ND ND ND 32.6 34.8 1 10.0-127 6.68 40
n-Nitrosodiphenylamine 0.666 ND 0.352 0.358 52.9 53.8 1 17.0-120 1.69 29
n-Nitrosodi-n-propylamine 0.666 ND ND ND 42.3 44.3 1 10.0-120 4.51 37
Phenanthrene 0.666 ND 0.362 0.366 51.4 52.0 1 17.0-120 1.10 31
Benzylbutyl phthalate 0.666 ND 0.360 0.374 54.1 56.2 1 23.0-120 3.81 30
Bis(2-ethylhexyl)phthalate 0.666 ND 0.360 0.365 54.1 54.8 1 17.0-126 1.38 30
Di-n-butyl phthalate 0.666 ND 0.351 0.364 52.7 54.7 1 30.0-120 3.64 29
Diethyl phthalate 0.666 ND 0.344 0.361 51.7 54.2 1 26.0-120 4.82 28
Dimethyl phthalate 0.666 ND 0.366 0.376 55.0 56.5 1 25.0-120 2.70 29
Di-n-octyl phthalate 0.666 ND 0.367 0.377 55.1 56.6 1 21.0-123 2.69 29
Pyrene 0.666 ND 0.357 0.360 53.6 54.1 1 16.0-121 0.837 32
1,2,4-Trichlorobenzene 0.666 ND ND ND 45.6 47.1 1 12.0-120 3.24 37
4-Chloro-3-methylphenol 0.666 ND ND ND 43.5 45.6 1 15.0-120 4.71 30
2-Chlorophenol 0.666 ND ND 0.341 49.5 51.2 1 15.0-120 3.28 37
2,4-Dichlorophenol 0.666 ND ND 0.334 47.3 50.2 1 20.0-120 5.86 31
2,4-Dimethylphenol 0.666 ND ND ND 42.0 45.8 1 10.0-120 8.55 33
4,6-Dinitro-2-methylphenol 0.666 ND 0.363 0.380 54.5 57.1 1 10.0-120 4.58 39
2,4-Dinitrophenol 0.666 ND ND 0.338 46.7 50.8 1 10.0-121 8.32 40
2-Nitrophenol 0.666 ND ND 0.337 46.5 50.6 1 12.0-120 8.35 39
4-Nitrophenol 0.666 ND ND ND 45.2 47.1 1 10.0-137 4.23 32
Pentachlorophenol 0.666 ND ND ND 47.7 49.7 1 10.0-160 4.01 31
Phenol 0.666 ND ND ND 42.3 44.1 1 12.0-120 4.17 38
2,4,6-Trichlorophenol 0.666 ND ND 0.336 48.9 50.5 1 19.0-120 3.02 32
(S) Nitrobenzene-d5 38.4 40.2 10.0-122
(S) 2-Fluorobiphenyl 53.2 56.5 15.0-120
(S) p-Terphenyl-d14 61.3 62.2 10.0-120
(S) Phenol-d5 50.0 51.2 10.0-120
(S) 2-Fluorophenol 56.5 58.7 12.0-120
(S) 2,4,6-Tribromophenol 61.3 66.5 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-01
Method Blank (MB)
(MB) R3921464-2 05/04/23 23:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-01
Method Blank (MB)
(MB) R3921464-2 05/04/23 23:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 62.5 10.0-122
(S) 2-Fluorobiphenyl 58.9 15.0-120
(S) p-Terphenyl-d14 63.7 10.0-120
(S) Phenol-d5 55.6 10.0-120
(S) 2-Fluorophenol 60.7 12.0-120
(S) 2,4,6-Tribromophenol 53.3 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3921464-1 05/04/23 23:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.314 47.1 38.0-120
Acenaphthylene 0.666 0.320 48.0 40.0-120
Anthracene 0.666 0.336 50.5 42.0-120
Benzidine 1.33 0.221 16.6 10.0-120
Benzo(a)anthracene 0.666 0.336 50.5 44.0-120
Benzo(b)fluoranthene 0.666 0.318 47.7 43.0-120
Benzo(k)fluoranthene 0.666 0.332 49.8 44.0-120
Benzo(g,h,i)perylene 0.666 0.364 54.7 43.0-120
Benzo(a)pyrene 0.666 0.346 52.0 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.291 43.7 20.0-120
Bis(2-chloroethyl)ether 0.666 0.361 54.2 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.299 44.9 23.0-120
4-Bromophenyl-phenylether 0.666 0.307 46.1 40.0-120
2-Chloronaphthalene 0.666 0.312 46.8 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-01
Laboratory Control Sample (LCS)
(LCS) R3921464-1 05/04/23 23:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.302 45.3 40.0-120
Chrysene 0.666 0.328 49.2 43.0-120
Dibenz(a,h)anthracene 0.666 0.341 51.2 44.0-120
3,3-Dichlorobenzidine 1.33 0.585 44.0 28.0-120
2,4-Dinitrotoluene 0.666 0.378 56.8 45.0-120
2,6-Dinitrotoluene 0.666 0.338 50.8 42.0-120
Fluoranthene 0.666 0.332 49.8 44.0-120
Fluorene 0.666 0.317 47.6 41.0-120
Hexachlorobenzene 0.666 0.323 48.5 39.0-120
Hexachloro-1,3-butadiene 0.666 0.262 39.3 15.0-120
Hexachlorocyclopentadiene 0.666 0.335 50.3 15.0-120
Hexachloroethane 0.666 0.288 43.2 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.318 47.7 45.0-120
Isophorone 0.666 0.308 46.2 23.0-120
Naphthalene 0.666 0.287 43.1 18.0-120
Nitrobenzene 0.666 0.291 43.7 17.0-120
n-Nitrosodimethylamine 0.666 0.317 47.6 10.0-125
n-Nitrosodiphenylamine 0.666 0.331 49.7 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.318 47.7 26.0-120
Phenanthrene 0.666 0.331 49.7 42.0-120
Benzylbutyl phthalate 0.666 0.354 53.2 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.358 53.8 41.0-120
Di-n-butyl phthalate 0.666 0.339 50.9 43.0-120
Diethyl phthalate 0.666 0.337 50.6 43.0-120
Dimethyl phthalate 0.666 0.326 48.9 43.0-120
Di-n-octyl phthalate 0.666 0.354 53.2 40.0-120
Pyrene 0.666 0.342 51.4 41.0-120
1,2,4-Trichlorobenzene 0.666 0.267 40.1 17.0-120
4-Chloro-3-methylphenol 0.666 0.280 42.0 28.0-120
2-Chlorophenol 0.666 0.316 47.4 28.0-120
2,4-Dichlorophenol 0.666 0.280 42.0 25.0-120
2,4-Dimethylphenol 0.666 0.321 48.2 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.392 58.9 16.0-120
2,4-Dinitrophenol 0.666 0.247 37.1 10.0-120
2-Nitrophenol 0.666 0.328 49.2 20.0-120
4-Nitrophenol 0.666 0.299 44.9 27.0-120
Pentachlorophenol 0.666 0.277 41.6 29.0-120
Phenol 0.666 0.307 46.1 28.0-120
2,4,6-Trichlorophenol 0.666 0.290 43.5 37.0-120
(S) Nitrobenzene-d5 46.2 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-01
Laboratory Control Sample (LCS)
(LCS) R3921464-1 05/04/23 23:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 51.1 15.0-120
(S) p-Terphenyl-d14 51.4 10.0-120
(S) Phenol-d5 48.5 10.0-120
(S) 2-Fluorophenol 51.8 12.0-120
(S) 2,4,6-Tribromophenol 53.9 10.0-127
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/05/23 05:42 • (MS) R3921464-3 05/05/23 06:03 • (MSD) R3921464-4 05/05/23 06:24
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.778 ND 0.417 0.418 50.9 50.3 5 18.0-120 0.305 32
Acenaphthylene 0.778 ND 0.408 0.413 49.8 49.7 5 25.0-120 1.24 32
Anthracene 0.778 ND 0.468 0.513 57.2 61.7 5 22.0-120 9.10 29
Benzidine 1.55 ND ND ND 50.2 55.5 5 10.0-120 11.4 40
Benzo(a)anthracene 0.778 ND 0.499 0.543 60.9 65.3 5 25.0-120 8.57 29
Benzo(b)fluoranthene 0.778 ND 0.570 0.603 69.6 72.5 5 19.0-122 5.65 31
Benzo(k)fluoranthene 0.778 ND 0.528 0.581 64.5 69.9 5 23.0-120 9.66 30
Benzo(g,h,i)perylene 0.778 ND 0.214 0.241 26.2 29.0 5 10.0-120 11.8 33
Benzo(a)pyrene 0.778 ND 0.529 0.579 64.6 69.6 5 24.0-120 8.98 30
Bis(2-chlorethoxy)methane 0.778 ND ND ND 44.2 44.5 5 10.0-120 2.09 34
Bis(2-chloroethyl)ether 0.778 ND ND ND 42.5 44.5 5 10.0-120 6.04 40
2,2-Oxybis(1-Chloropropane) 0.778 ND ND ND 41.3 40.3 5 10.0-120 0.758 40
4-Bromophenyl-phenylether 0.778 ND ND ND 50.6 53.8 5 27.0-120 7.69 30
2-Chloronaphthalene 0.778 ND 0.379 0.393 46.3 47.2 5 20.0-120 3.64 32
4-Chlorophenyl-phenylether 0.778 ND ND ND 50.0 53.4 5 24.0-120 8.07 29
Chrysene 0.778 ND 0.491 0.525 60.0 63.2 5 21.0-120 6.78 29
Dibenz(a,h)anthracene 0.778 ND 0.245 0.292 29.9 35.1 5 10.0-120 17.6 32
3,3-Dichlorobenzidine 1.55 ND ND ND 54.7 58.8 5 10.0-120 8.87 34
2,4-Dinitrotoluene 0.778 ND ND ND 57.8 57.2 5 30.0-120 0.538 31
2,6-Dinitrotoluene 0.778 ND ND ND 50.3 53.2 5 25.0-120 7.16 31
Fluoranthene 0.778 ND 0.500 0.525 61.1 63.2 5 18.0-126 4.98 32
Fluorene 0.778 ND 0.435 0.469 53.1 56.4 5 25.0-120 7.62 30
Hexachlorobenzene 0.778 ND ND ND 51.2 56.4 5 27.0-120 11.2 28
Hexachloro-1,3-butadiene 0.778 ND ND ND 39.1 38.2 5 10.0-120 0.800 38
Hexachlorocyclopentadiene 0.778 ND ND ND 0.000 0.000 5 10.0-120 J6 J6 0.000 40
Hexachloroethane 0.778 ND ND ND 39.1 35.1 5 10.0-120 9.17 40
Indeno(1,2,3-cd)pyrene 0.778 ND 0.232 0.269 28.3 32.4 5 10.0-120 14.8 32
Isophorone 0.778 ND ND ND 46.9 48.5 5 13.0-120 4.86 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2052922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1607939-01
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/05/23 05:42 • (MS) R3921464-3 05/05/23 06:03 • (MSD) R3921464-4 05/05/23 06:24
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.778 ND 0.365 0.371 44.5 44.6 5 10.0-120 1.73 35
Nitrobenzene 0.778 ND ND ND 44.1 46.3 5 10.0-120 6.50 36
n-Nitrosodimethylamine 0.778 ND ND ND 43.8 45.9 5 10.0-127 6.21 40
n-Nitrosodiphenylamine 0.778 ND ND ND 56.1 60.6 5 17.0-120 9.27 29
n-Nitrosodi-n-propylamine 0.778 ND ND ND 44.7 48.3 5 10.0-120 9.30 37
Phenanthrene 0.778 ND 0.481 0.514 58.7 61.8 5 17.0-120 6.67 31
Benzylbutyl phthalate 0.778 ND ND ND 68.2 70.9 5 23.0-120 5.33 30
Bis(2-ethylhexyl)phthalate 0.778 ND ND ND 67.6 73.2 5 17.0-126 9.44 30
Di-n-butyl phthalate 0.778 ND ND ND 58.7 65.2 5 30.0-120 12.0 29
Diethyl phthalate 0.778 ND ND ND 54.2 54.8 5 26.0-120 2.55 28
Dimethyl phthalate 0.778 ND ND ND 0.000 0.000 5 25.0-120 J6 J6 0.000 29
Di-n-octyl phthalate 0.778 ND ND ND 69.2 74.5 5 21.0-123 9.03 29
Pyrene 0.778 ND 0.530 0.571 64.8 68.7 5 16.0-121 7.41 32
1,2,4-Trichlorobenzene 0.778 ND ND ND 40.8 39.7 5 12.0-120 1.15 37
4-Chloro-3-methylphenol 0.778 ND ND ND 57.3 58.7 5 15.0-120 3.99 30
2-Chlorophenol 0.778 ND ND ND 37.4 34.5 5 15.0-120 6.45 37
2,4-Dichlorophenol 0.778 ND ND ND 40.8 38.3 5 20.0-120 4.69 31
2,4-Dimethylphenol 0.778 ND ND ND 57.3 58.0 5 10.0-120 2.68 33
4,6-Dinitro-2-methylphenol 0.778 ND ND ND 0.000 0.000 5 10.0-120 J6 J6 0.000 39
2,4-Dinitrophenol 0.778 ND ND ND 0.000 0.000 5 10.0-121 J6 J6 0.000 40
2-Nitrophenol 0.778 ND ND ND 27.9 22.5 5 12.0-120 19.6 39
4-Nitrophenol 0.778 ND ND ND 45.2 23.9 5 10.0-137 J3 60.1 32
Pentachlorophenol 0.778 ND ND ND 41.3 25.9 5 10.0-160 J3 44.2 31
Phenol 0.778 ND ND ND 46.3 43.7 5 12.0-120 4.12 38
2,4,6-Trichlorophenol 0.778 ND ND ND 36.1 23.0 5 19.0-120 J3 42.9 32
(S) Nitrobenzene-d5 46.7 49.1 10.0-122
(S) 2-Fluorobiphenyl 49.8 48.2 15.0-120
(S) p-Terphenyl-d14 61.4 64.7 10.0-120
(S) Phenol-d5 46.0 44.3 10.0-120
(S) 2-Fluorophenol 35.0 33.1 12.0-120
(S) 2,4,6-Tribromophenol 47.8 36.3 10.0-127
Sample Narrative:
OS: Dilution due to matrix.
MS: Dilution due to matrix.
MSD: Dilution due to matrix.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047984
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-11,12,13,14
Method Blank (MB)
(MB) R3917715-3 04/25/23 17:38
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Anthracene U 0.0000190 0.0000500
Acenaphthene U 0.0000190 0.0000500
Acenaphthylene U 0.0000171 0.0000500
Benzo(a)anthracene U 0.0000203 0.0000500
Benzo(a)pyrene U 0.0000184 0.0000500
Benzo(b)fluoranthene U 0.0000168 0.0000500
Benzo(g,h,i)perylene U 0.0000184 0.0000500
Benzo(k)fluoranthene U 0.0000202 0.0000500
Chrysene U 0.0000179 0.0000500
Dibenz(a,h)anthracene U 0.0000160 0.0000500
Fluoranthene U 0.0000270 0.000100
Fluorene U 0.0000169 0.0000500
Indeno(1,2,3-cd)pyrene U 0.0000158 0.0000500
Naphthalene U 0.0000917 0.000250
Phenanthrene U 0.0000180 0.0000500
Pyrene U 0.0000169 0.0000500
1-Methylnaphthalene U 0.0000687 0.000250
2-Methylnaphthalene U 0.0000674 0.000250
2-Chloronaphthalene U 0.0000682 0.000250
(S) Nitrobenzene-d5 96.0 31.0-160
(S) 2-Fluorobiphenyl 106 48.0-148
(S) p-Terphenyl-d14 102 37.0-146
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3917715-1 04/25/23 14:37 • (LCSD) R3917715-2 04/25/23 17:21
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Anthracene 0.00200 0.00201 0.00202 100 101 67.0-150 0.496 20
Acenaphthene 0.00200 0.00191 0.00184 95.5 92.0 65.0-138 3.73 20
Acenaphthylene 0.00200 0.00211 0.00204 105 102 66.0-140 3.37 20
Benzo(a)anthracene 0.00200 0.00219 0.00216 109 108 61.0-140 1.38 20
Benzo(a)pyrene 0.00200 0.00229 0.00227 115 114 60.0-143 0.877 20
Benzo(b)fluoranthene 0.00200 0.00213 0.00215 106 107 58.0-141 0.935 20
Benzo(g,h,i)perylene 0.00200 0.00208 0.00208 104 104 52.0-153 0.000 20
Benzo(k)fluoranthene 0.00200 0.00217 0.00214 108 107 58.0-148 1.39 20
Chrysene 0.00200 0.00220 0.00218 110 109 64.0-144 0.913 20
Dibenz(a,h)anthracene 0.00200 0.00213 0.00207 106 104 52.0-155 2.86 20
Fluoranthene 0.00200 0.00230 0.00233 115 117 69.0-153 1.30 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2047984
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-11,12,13,14
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3917715-1 04/25/23 14:37 • (LCSD) R3917715-2 04/25/23 17:21
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Fluorene 0.00200 0.00219 0.00215 109 107 64.0-136 1.84 20
Indeno(1,2,3-cd)pyrene 0.00200 0.00235 0.00233 117 117 54.0-153 0.855 20
Naphthalene 0.00200 0.00219 0.00209 109 104 61.0-137 4.67 20
Phenanthrene 0.00200 0.00212 0.00213 106 106 62.0-137 0.471 20
Pyrene 0.00200 0.00209 0.00210 104 105 60.0-142 0.477 20
1-Methylnaphthalene 0.00200 0.00224 0.00222 112 111 66.0-142 0.897 20
2-Methylnaphthalene 0.00200 0.00215 0.00211 107 105 62.0-136 1.88 20
2-Chloronaphthalene 0.00200 0.00209 0.00206 104 103 64.0-140 1.45 20
(S) Nitrobenzene-d5 95.5 92.5 31.0-160
(S) 2-Fluorobiphenyl 108 104 48.0-148
(S) p-Terphenyl-d14 103 102 37.0-146
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048874
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-19,20
Method Blank (MB)
(MB) R3918765-2 04/27/23 00:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Anthracene U 0.0000190 0.0000500
Acenaphthene U 0.0000190 0.0000500
Acenaphthylene U 0.0000171 0.0000500
Benzo(a)anthracene U 0.0000203 0.0000500
Benzo(a)pyrene U 0.0000184 0.0000500
Benzo(b)fluoranthene U 0.0000168 0.0000500
Benzo(g,h,i)perylene U 0.0000184 0.0000500
Benzo(k)fluoranthene U 0.0000202 0.0000500
Chrysene U 0.0000179 0.0000500
Dibenz(a,h)anthracene U 0.0000160 0.0000500
Fluoranthene U 0.0000270 0.000100
Fluorene U 0.0000169 0.0000500
Indeno(1,2,3-cd)pyrene U 0.0000158 0.0000500
Naphthalene U 0.0000917 0.000250
Phenanthrene U 0.0000180 0.0000500
Pyrene U 0.0000169 0.0000500
1-Methylnaphthalene U 0.0000687 0.000250
2-Methylnaphthalene U 0.0000674 0.000250
2-Chloronaphthalene U 0.0000682 0.000250
(S) Nitrobenzene-d5 122 31.0-160
(S) 2-Fluorobiphenyl 120 48.0-148
(S) p-Terphenyl-d14 123 37.0-146
Laboratory Control Sample (LCS)
(LCS) R3918765-1 04/26/23 23:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Anthracene 0.00200 0.00238 119 67.0-150
Acenaphthene 0.00200 0.00240 120 65.0-138
Acenaphthylene 0.00200 0.00238 119 66.0-140
Benzo(a)anthracene 0.00200 0.00258 129 61.0-140
Benzo(a)pyrene 0.00200 0.00267 133 60.0-143
Benzo(b)fluoranthene 0.00200 0.00251 126 58.0-141
Benzo(g,h,i)perylene 0.00200 0.00239 119 52.0-153
Benzo(k)fluoranthene 0.00200 0.00245 122 58.0-148
Chrysene 0.00200 0.00260 130 64.0-144
Dibenz(a,h)anthracene 0.00200 0.00235 117 52.0-155
Fluoranthene 0.00200 0.00248 124 69.0-153
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048874
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-19,20
Laboratory Control Sample (LCS)
(LCS) R3918765-1 04/26/23 23:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Fluorene 0.00200 0.00241 120 64.0-136
Indeno(1,2,3-cd)pyrene 0.00200 0.00240 120 54.0-153
Naphthalene 0.00200 0.00236 118 61.0-137
Phenanthrene 0.00200 0.00241 120 62.0-137
Pyrene 0.00200 0.00263 132 60.0-142
1-Methylnaphthalene 0.00200 0.00232 116 66.0-142
2-Methylnaphthalene 0.00200 0.00238 119 62.0-136
2-Chloronaphthalene 0.00200 0.00227 114 64.0-140
(S) Nitrobenzene-d5 133 31.0-160
(S) 2-Fluorobiphenyl 108 48.0-148
(S) p-Terphenyl-d14 113 37.0-146
L1607939-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-19 04/27/23 00:58 • (MS) R3918765-3 04/27/23 01:15 • (MSD) R3918765-4 04/27/23 01:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Anthracene 0.00200 ND 0.00187 0.00241 93.5 120 1 56.0-156 J3 25.2 20
Acenaphthene 0.00200 ND 0.00192 0.00247 96.0 123 1 44.0-153 J3 25.1 20
Acenaphthylene 0.00200 ND 0.00186 0.00241 93.0 120 1 53.0-150 J3 25.8 20
Benzo(a)anthracene 0.00200 ND 0.00184 0.00251 92.0 126 1 47.0-151 J3 30.8 20
Benzo(a)pyrene 0.00200 ND 0.00185 0.00257 92.5 129 1 45.0-146 J3 32.6 20
Benzo(b)fluoranthene 0.00200 ND 0.00177 0.00246 88.5 123 1 43.0-142 J3 32.6 20
Benzo(g,h,i)perylene 0.00200 ND 0.00167 0.00236 83.5 118 1 40.0-147 J3 34.2 20
Benzo(k)fluoranthene 0.00200 ND 0.00173 0.00240 86.5 120 1 43.0-148 J3 32.4 21
Chrysene 0.00200 ND 0.00187 0.00259 93.5 130 1 50.0-148 J3 32.3 20
Dibenz(a,h)anthracene 0.00200 ND 0.00158 0.00223 79.0 111 1 37.0-151 J3 34.1 20
Fluoranthene 0.00200 ND 0.00194 0.00251 97.0 126 1 56.0-157 J3 25.6 20
Fluorene 0.00200 ND 0.00190 0.00246 95.0 123 1 48.0-148 J3 25.7 20
Indeno(1,2,3-cd)pyrene 0.00200 ND 0.00159 0.00226 79.5 113 1 41.0-148 J3 34.8 20
Naphthalene 0.00200 ND 0.00189 0.00247 94.5 123 1 10.0-160 J3 26.6 20
Phenanthrene 0.00200 ND 0.00193 0.00247 96.5 123 1 47.0-147 J3 24.5 20
Pyrene 0.00200 ND 0.00201 0.00273 100 137 1 51.0-148 J3 30.4 20
1-Methylnaphthalene 0.00200 ND 0.00183 0.00240 91.5 120 1 21.0-160 J3 27.0 20
2-Methylnaphthalene 0.00200 ND 0.00189 0.00247 94.5 123 1 31.0-160 J3 26.6 20
2-Chloronaphthalene 0.00200 ND 0.00185 0.00239 92.5 119 1 52.0-148 J3 25.5 20
(S) Nitrobenzene-d5 107 131 31.0-160
(S) 2-Fluorobiphenyl 86.0 112 48.0-148
(S) p-Terphenyl-d14 81.0 111 37.0-146
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048849
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-02
Method Blank (MB)
(MB) R3918160-2 04/26/23 12:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 84.3 23.0-120
(S) Nitrobenzene-d5 70.7 14.0-149
(S) 2-Fluorobiphenyl 70.1 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3918160-1 04/26/23 12:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0705 88.1 50.0-126
Acenaphthene 0.0800 0.0709 88.6 50.0-120
Acenaphthylene 0.0800 0.0695 86.9 50.0-120
Benzo(a)anthracene 0.0800 0.0745 93.1 45.0-120
Benzo(a)pyrene 0.0800 0.0714 89.3 42.0-120
Benzo(b)fluoranthene 0.0800 0.0777 97.1 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0781 97.6 45.0-125
Benzo(k)fluoranthene 0.0800 0.0766 95.8 49.0-125
Chrysene 0.0800 0.0752 94.0 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0795 99.4 47.0-125
Fluoranthene 0.0800 0.0763 95.4 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048849
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-02
Laboratory Control Sample (LCS)
(LCS) R3918160-1 04/26/23 12:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0713 89.1 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0865 108 46.0-125
Naphthalene 0.0800 0.0693 86.6 50.0-120
Phenanthrene 0.0800 0.0696 87.0 47.0-120
Pyrene 0.0800 0.0743 92.9 43.0-123
1-Methylnaphthalene 0.0800 0.0743 92.9 51.0-121
2-Methylnaphthalene 0.0800 0.0721 90.1 50.0-120
2-Chloronaphthalene 0.0800 0.0616 77.0 50.0-120
(S) p-Terphenyl-d14 87.5 23.0-120
(S) Nitrobenzene-d5 86.9 14.0-149
(S) 2-Fluorobiphenyl 78.3 34.0-125
L1608036-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608036-10 04/26/23 14:36 • (MS) R3918160-3 04/26/23 14:56 • (MSD) R3918160-4 04/26/23 15:15
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0960 ND 0.0737 0.0768 76.8 80.0 1 10.0-145 4.07 30
Acenaphthene 0.0960 ND 0.0608 0.0686 63.3 71.4 1 14.0-127 12.1 27
Acenaphthylene 0.0960 ND 0.0606 0.0664 63.1 69.1 1 21.0-124 9.06 25
Benzo(a)anthracene 0.0960 ND 0.0837 0.0838 87.1 87.2 1 10.0-139 0.146 30
Benzo(a)pyrene 0.0960 ND 0.0952 0.0942 99.1 98.1 1 10.0-141 1.03 31
Benzo(b)fluoranthene 0.0960 ND 0.0772 0.0779 80.4 81.1 1 10.0-140 0.948 36
Benzo(g,h,i)perylene 0.0960 ND 0.0818 0.0823 85.2 85.7 1 10.0-140 0.597 33
Benzo(k)fluoranthene 0.0960 ND 0.0859 0.0846 89.4 88.1 1 10.0-137 1.44 31
Chrysene 0.0960 ND 0.0856 0.0853 89.2 88.8 1 10.0-145 0.430 30
Dibenz(a,h)anthracene 0.0960 ND 0.0881 0.0862 91.7 89.8 1 10.0-132 2.11 31
Fluoranthene 0.0960 ND 0.0771 0.0811 80.2 84.4 1 10.0-153 5.11 33
Fluorene 0.0960 ND 0.0643 0.0709 67.0 73.9 1 11.0-130 9.78 29
Indeno(1,2,3-cd)pyrene 0.0960 ND 0.0903 0.0906 94.0 94.4 1 10.0-137 0.406 32
Naphthalene 0.0960 ND 0.0637 0.0686 66.3 71.4 1 10.0-135 7.41 27
Phenanthrene 0.0960 ND 0.0666 0.0718 69.4 74.7 1 10.0-144 7.43 31
Pyrene 0.0960 ND 0.0730 0.0759 76.0 79.1 1 10.0-148 3.95 35
1-Methylnaphthalene 0.0960 ND 0.0649 0.0719 66.4 73.7 1 10.0-142 10.2 28
2-Methylnaphthalene 0.0960 ND 0.0638 0.0708 65.1 72.3 1 10.0-137 10.4 28
2-Chloronaphthalene 0.0960 ND 0.0545 0.0597 56.7 62.1 1 29.0-120 9.01 24
(S) p-Terphenyl-d14 60.3 76.3 23.0-120
(S) Nitrobenzene-d5 84.7 84.7 14.0-149
(S) 2-Fluorobiphenyl 43.6 60.0 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048850
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-03,04,05,06,07,08,09,10
Method Blank (MB)
(MB) R3918433-2 04/26/23 19:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 88.7 23.0-120
(S) Nitrobenzene-d5 66.1 14.0-149
(S) 2-Fluorobiphenyl 95.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3918433-1 04/26/23 19:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0795 99.4 50.0-126
Acenaphthene 0.0800 0.0793 99.1 50.0-120
Acenaphthylene 0.0800 0.0728 91.0 50.0-120
Benzo(a)anthracene 0.0800 0.0796 99.5 45.0-120
Benzo(a)pyrene 0.0800 0.0629 78.6 42.0-120
Benzo(b)fluoranthene 0.0800 0.0747 93.4 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0765 95.6 45.0-125
Benzo(k)fluoranthene 0.0800 0.0750 93.8 49.0-125
Chrysene 0.0800 0.0864 108 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0803 100 47.0-125
Fluoranthene 0.0800 0.0855 107 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2048850
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-03,04,05,06,07,08,09,10
Laboratory Control Sample (LCS)
(LCS) R3918433-1 04/26/23 19:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0830 104 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0799 99.9 46.0-125
Naphthalene 0.0800 0.0651 81.4 50.0-120
Phenanthrene 0.0800 0.0833 104 47.0-120
Pyrene 0.0800 0.0803 100 43.0-123
1-Methylnaphthalene 0.0800 0.0680 85.0 51.0-121
2-Methylnaphthalene 0.0800 0.0690 86.3 50.0-120
2-Chloronaphthalene 0.0800 0.0836 105 50.0-120
(S) p-Terphenyl-d14 83.6 23.0-120
(S) Nitrobenzene-d5 64.1 14.0-149
(S) 2-Fluorobiphenyl 91.7 34.0-125
L1607994-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607994-03 04/26/23 21:24 • (MS) R3918433-3 04/26/23 21:44 • (MSD) R3918433-4 04/26/23 22:03
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Anthracene 0.0818 ND 0.0826 0.0787 101 96.2 1 10.0-145 4.74 30
Acenaphthene 0.0818 ND 0.0846 0.0801 103 97.9 1 14.0-127 5.52 27
Acenaphthylene 0.0818 ND 0.0772 0.0729 94.3 89.0 1 21.0-124 5.79 25
Benzo(a)anthracene 0.0818 ND 0.0829 0.0780 101 95.3 1 10.0-139 6.04 30
Benzo(a)pyrene 0.0818 ND 0.0818 0.0777 100 94.9 1 10.0-141 5.18 31
Benzo(b)fluoranthene 0.0818 ND 0.0798 0.0757 97.5 92.6 1 10.0-140 5.18 36
Benzo(g,h,i)perylene 0.0818 ND 0.0822 0.0758 100 92.7 1 10.0-140 7.98 33
Benzo(k)fluoranthene 0.0818 ND 0.0787 0.0744 96.2 90.9 1 10.0-137 5.67 31
Chrysene 0.0818 ND 0.0899 0.0850 110 104 1 10.0-145 5.55 30
Dibenz(a,h)anthracene 0.0818 ND 0.0841 0.0786 103 96.1 1 10.0-132 6.73 31
Fluoranthene 0.0818 ND 0.0893 0.0842 109 103 1 10.0-153 5.84 33
Fluorene 0.0818 ND 0.0874 0.0827 107 101 1 11.0-130 5.59 29
Indeno(1,2,3-cd)pyrene 0.0818 ND 0.0836 0.0775 102 94.7 1 10.0-137 7.57 32
Naphthalene 0.0818 ND 0.0704 0.0658 86.0 80.4 1 10.0-135 6.68 27
Phenanthrene 0.0818 ND 0.0864 0.0817 106 99.9 1 10.0-144 5.53 31
Pyrene 0.0818 ND 0.0849 0.0802 104 98.0 1 10.0-148 5.76 35
1-Methylnaphthalene 0.0818 ND 0.0724 0.0685 88.5 83.7 1 10.0-142 5.57 28
2-Methylnaphthalene 0.0818 ND 0.0736 0.0699 89.9 85.4 1 10.0-137 5.19 28
2-Chloronaphthalene 0.0818 ND 0.0889 0.0839 109 103 1 29.0-120 5.74 24
(S) p-Terphenyl-d14 87.0 84.4 23.0-120
(S) Nitrobenzene-d5 68.3 63.3 14.0-149
(S) 2-Fluorobiphenyl 97.1 89.1 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2051665
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-01
Method Blank (MB)
(MB) R3921751-2 05/04/23 17:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 72.1 23.0-120
(S) Nitrobenzene-d5 63.9 14.0-149
(S) 2-Fluorobiphenyl 70.1 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3921751-1 05/04/23 16:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0525 65.6 50.0-126
Acenaphthene 0.0800 0.0548 68.5 50.0-120
Acenaphthylene 0.0800 0.0583 72.9 50.0-120
Benzo(a)anthracene 0.0800 0.0569 71.1 45.0-120
Benzo(a)pyrene 0.0800 0.0572 71.5 42.0-120
Benzo(b)fluoranthene 0.0800 0.0596 74.5 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0592 74.0 45.0-125
Benzo(k)fluoranthene 0.0800 0.0575 71.9 49.0-125
Chrysene 0.0800 0.0639 79.9 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0599 74.9 47.0-125
Fluoranthene 0.0800 0.0593 74.1 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2051665
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1607939-01
Laboratory Control Sample (LCS)
(LCS) R3921751-1 05/04/23 16:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0613 76.6 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0644 80.5 46.0-125
Naphthalene 0.0800 0.0579 72.4 50.0-120
Phenanthrene 0.0800 0.0612 76.5 47.0-120
Pyrene 0.0800 0.0668 83.5 43.0-123
1-Methylnaphthalene 0.0800 0.0603 75.4 51.0-121
2-Methylnaphthalene 0.0800 0.0573 71.6 50.0-120
2-Chloronaphthalene 0.0800 0.0595 74.4 50.0-120
(S) p-Terphenyl-d14 82.0 23.0-120
(S) Nitrobenzene-d5 75.5 14.0-149
(S) 2-Fluorobiphenyl 80.0 34.0-125
L1607939-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607939-01 05/04/23 22:23 • (MS) R3921751-3 05/04/23 22:42 • (MSD) R3921751-4 05/04/23 23:02
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0960 ND 0.0695 0.0476 63.4 41.7 1 10.0-145 J3 37.5 30
Acenaphthene 0.0960 0.00881 0.0631 0.0453 53.3 35.6 1 14.0-127 J3 32.9 27
Acenaphthylene 0.0960 ND 0.0760 0.0541 75.3 53.5 1 21.0-124 J3 33.7 25
Benzo(a)anthracene 0.0960 0.0224 0.0945 0.0609 70.2 37.0 1 10.0-139 J3 43.2 30
Benzo(a)pyrene 0.0960 0.0236 0.0812 0.0553 55.8 30.2 1 10.0-141 J3 37.9 31
Benzo(b)fluoranthene 0.0960 0.0182 0.0616 0.0426 42.0 23.2 1 10.0-140 J3 36.5 36
Benzo(g,h,i)perylene 0.0960 0.0291 0.0565 0.0399 25.6 9.22 1 10.0-140 J3 J6 34.4 33
Benzo(k)fluoranthene 0.0960 ND 0.0595 0.0425 54.4 37.5 1 10.0-137 J3 33.5 31
Chrysene 0.0960 0.0208 0.104 0.0785 81.3 56.1 1 10.0-145 27.9 30
Dibenz(a,h)anthracene 0.0960 ND 0.0620 0.0460 55.4 39.6 1 10.0-132 29.5 31
Fluoranthene 0.0960 0.0223 0.0780 0.0520 54.0 28.3 1 10.0-153 J3 40.0 33
Fluorene 0.0960 ND 0.0714 0.0499 64.4 43.1 1 11.0-130 J3 35.5 29
Indeno(1,2,3-cd)pyrene 0.0960 0.0117 0.0655 0.0458 52.7 33.2 1 10.0-137 J3 35.5 32
Naphthalene 0.0960 ND 0.0719 0.0544 71.2 53.9 1 10.0-135 J3 27.6 27
Phenanthrene 0.0960 0.0350 0.0788 0.0569 41.5 19.8 1 10.0-144 J3 32.3 31
Pyrene 0.0960 0.0483 0.0992 0.0639 47.9 12.9 1 10.0-148 J3 43.3 35
1-Methylnaphthalene 0.0960 ND 0.0755 0.0547 74.7 54.2 1 10.0-142 J3 31.9 28
2-Methylnaphthalene 0.0960 ND 0.0743 0.0538 65.9 45.6 1 10.0-137 J3 32.0 28
2-Chloronaphthalene 0.0960 ND 0.0632 0.0451 62.6 44.7 1 29.0-120 J3 33.4 24
(S) p-Terphenyl-d14 52.1 48.2 23.0-120
(S) Nitrobenzene-d5 92.7 86.7 14.0-149
(S) 2-Fluorobiphenyl 54.2 46.5 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Qualifier Description
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.
P RPD between the primary and confirmatory analysis exceeded 40%.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
May 19, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1613187
Samples Received:05/05/2023
Project Number:
Description:
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
May 19, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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May 22, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
MW-3 L1613187-01 6
MW-6 L1613187-02 10
MW-4 L1613187-03 14
MW-1 L1613187-04 18
MW-2 L1613187-05 22
MW-5 L1613187-06 26
Qc: Quality Control Summary 30
Total Solids by Method 2540 G-2011 30
Wet Chemistry by Method 7199 32
Mercury by Method 7471A 34
Metals (ICP) by Method 6010B 35
Volatile Organic Compounds (GC) by Method 8015D/GRO 37
Volatile Organic Compounds (GC/MS) by Method 8260B 38
Semi-Volatile Organic Compounds (GC) by Method 8015 42
Polychlorinated Biphenyls (GC) by Method 8082 43
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 44
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 49
Gl: Glossary of Terms 51
Al: Accreditations & Locations 52
Sc: Sample Chain of Custody 53
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-3 L1613187-01 Solid Richie T. 05/04/23 10:00 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:02 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:26 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:20 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 26.5 05/04/23 10:00 05/11/23 12:28 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1.06 05/04/23 10:00 05/11/23 12:10 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 00:42 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 17:30 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 17:41 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:03 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1613187-02 Solid Richie T. 05/04/23 10:45 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:08 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:28 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:23 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 27.5 05/04/23 10:45 05/11/23 12:46 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1.1 05/04/23 10:45 05/11/23 12:29 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 100 05/13/23 15:08 05/14/23 19:23 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 17:42 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 10 05/12/23 04:57 05/15/23 21:59 AMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 10 05/11/23 16:50 05/12/23 07:58 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4 L1613187-03 Solid Richie T. 05/04/23 11:30 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:18 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:30 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:26 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 25 05/04/23 11:30 05/11/23 13:05 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1 05/04/23 11:30 05/11/23 12:48 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 01:38 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 17:55 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 18:31 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:20 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 L1613187-04 Solid Richie T. 05/04/23 12:20 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:54 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:36 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:29 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 25 05/04/23 12:20 05/11/23 13:24 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1 05/04/23 12:20 05/11/23 13:07 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1.23 05/13/23 15:08 05/14/23 01:25 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 18:08 NWH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1613187-04 Solid Richie T. 05/04/23 12:20 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 17:15 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:37 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1613187-05 Solid Richie T. 05/04/23 13:15 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055430 1 05/08/23 15:47 05/08/23 15:55 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 01:59 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:38 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:32 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 25 05/04/23 13:15 05/11/23 13:42 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1 05/04/23 13:15 05/11/23 13:26 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 02:31 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 18:20 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 18:55 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 03:55 AMM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1613187-06 Solid Richie T. 05/04/23 14:10 05/05/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2055863 1 05/08/23 15:11 05/08/23 15:17 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2056423 1 05/10/23 07:29 05/11/23 02:05 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2056112 1 05/10/23 21:58 05/12/23 12:40 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2055559 1 05/06/23 23:41 05/10/23 18:35 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2057784 30 05/04/23 14:10 05/11/23 14:01 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2058136 1.2 05/04/23 14:10 05/11/23 13:45 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2059338 1 05/13/23 15:08 05/14/23 00:03 NH Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2057922 1 05/12/23 10:39 05/13/23 18:33 NWH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2058400 1 05/12/23 04:57 05/12/23 16:26 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2058011 1 05/11/23 16:50 05/12/23 04:12 AMM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.2 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.23 1 05/11/2023 01:02 WG2056423
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0493 1 05/12/2023 12:26 WG2056112
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.46 1 05/10/2023 18:20 WG2055559
Arsenic 13.0 2.46 1 05/10/2023 18:20 WG2055559
Beryllium 0.409 0.246 1 05/10/2023 18:20 WG2055559
Cadmium ND 0.616 1 05/10/2023 18:20 WG2055559
Chromium 10.1 1.23 1 05/10/2023 18:20 WG2055559
Copper 11.8 2.46 1 05/10/2023 18:20 WG2055559
Lead 8.23 0.616 1 05/10/2023 18:20 WG2055559
Nickel 7.73 2.46 1 05/10/2023 18:20 WG2055559
Selenium ND 2.46 1 05/10/2023 18:20 WG2055559
Silver ND 1.23 1 05/10/2023 18:20 WG2055559
Thallium ND 2.46 1 05/10/2023 18:20 WG2055559
Zinc 34.8 6.16 1 05/10/2023 18:20 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.84 26.5 05/11/2023 12:28 WG2057784
(S) a,a,a-Trifluorotoluene(FID) 94.0 77.0-120 05/11/2023 12:28 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0790 0.0768 1.06 05/11/2023 12:10 WG2058136
Acrylonitrile ND 0.0193 1.06 05/11/2023 12:10 WG2058136
Benzene ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Bromobenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
Bromodichloromethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Bromoform ND 0.0384 1.06 05/11/2023 12:10 WG2058136
Bromomethane ND 0.0193 1.06 05/11/2023 12:10 WG2058136
n-Butylbenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
sec-Butylbenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
tert-Butylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Carbon tetrachloride ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Chlorobenzene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Chlorodibromomethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Chloroethane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Chloroform ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Chloromethane ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
4-Chlorotoluene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0384 1.06 05/11/2023 12:10 WG2058136
1,2-Dibromoethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Dibromomethane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2-Dichlorobenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,3-Dichlorobenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,4-Dichlorobenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Dichlorodifluoromethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1-Dichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,2-Dichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1-Dichloroethene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
cis-1,2-Dichloroethene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
trans-1,2-Dichloroethene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2-Dichloropropane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,1-Dichloropropene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,3-Dichloropropane ND 0.00768 1.06 05/11/2023 12:10 WG2058136
cis-1,3-Dichloropropene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
trans-1,3-Dichloropropene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
2,2-Dichloropropane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Di-isopropyl ether ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Ethylbenzene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Hexachloro-1,3-butadiene ND 0.0384 1.06 05/11/2023 12:10 WG2058136
Isopropylbenzene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
p-Isopropyltoluene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
2-Butanone (MEK)ND 0.154 1.06 05/11/2023 12:10 WG2058136
Methylene Chloride ND 0.0384 1.06 05/11/2023 12:10 WG2058136
4-Methyl-2-pentanone (MIBK) ND 0.0384 1.06 05/11/2023 12:10 WG2058136
Methyl tert-butyl ether ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Naphthalene ND J4 0.0193 1.06 05/11/2023 12:10 WG2058136
n-Propylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Styrene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Tetrachloroethene ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Toluene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0193 1.06 05/11/2023 12:10 WG2058136
1,2,4-Trichlorobenzene ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1,1,1-Trichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,1,2-Trichloroethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Trichloroethene ND 0.00154 1.06 05/11/2023 12:10 WG2058136
Trichlorofluoromethane ND 0.00384 1.06 05/11/2023 12:10 WG2058136
1,2,3-Trichloropropane ND 0.0193 1.06 05/11/2023 12:10 WG2058136
1,2,4-Trimethylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,2,3-Trimethylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
1,3,5-Trimethylbenzene ND 0.00768 1.06 05/11/2023 12:10 WG2058136
Vinyl chloride ND 0.00384 1.06 05/11/2023 12:10 WG2058136
Xylenes, Total ND 0.00999 1.06 05/11/2023 12:10 WG2058136
(S) Toluene-d8 106 75.0-131 05/11/2023 12:10 WG2058136
(S) 4-Bromofluorobenzene 93.4 67.0-138 05/11/2023 12:10 WG2058136
(S) 1,2-Dichloroethane-d4 113 70.0-130 05/11/2023 12:10 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.93 1 05/14/2023 00:42 WG2059338
C28-C40 Oil Range ND 4.93 1 05/14/2023 00:42 WG2059338
(S) o-Terphenyl 21.3 18.0-148 05/14/2023 00:42 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1221 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1232 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1242 ND 0.0419 1 05/13/2023 17:30 WG2057922
PCB 1248 ND 0.0209 1 05/13/2023 17:30 WG2057922
PCB 1254 ND 0.0209 1 05/13/2023 17:30 WG2057922
PCB 1260 ND 0.0209 1 05/13/2023 17:30 WG2057922
(S) Decachlorobiphenyl 63.8 10.0-135 05/13/2023 17:30 WG2057922
(S) Tetrachloro-m-xylene 76.4 10.0-139 05/13/2023 17:30 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Acenaphthylene ND 0.0410 1 05/12/2023 17:41 WG2058400
Anthracene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzidine ND 2.06 1 05/12/2023 17:41 WG2058400
Benzo(a)anthracene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(b)fluoranthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(k)fluoranthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(g,h,i)perylene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzo(a)pyrene ND 0.0410 1 05/12/2023 17:41 WG2058400
Bis(2-chlorethoxy)methane ND 0.410 1 05/12/2023 17:41 WG2058400
Bis(2-chloroethyl)ether ND 0.410 1 05/12/2023 17:41 WG2058400
2,2-Oxybis(1-Chloropropane) ND 0.410 1 05/12/2023 17:41 WG2058400
4-Bromophenyl-phenylether ND 0.410 1 05/12/2023 17:41 WG2058400
2-Chloronaphthalene ND 0.0410 1 05/12/2023 17:41 WG2058400
4-Chlorophenyl-phenylether ND 0.410 1 05/12/2023 17:41 WG2058400
Chrysene ND 0.0410 1 05/12/2023 17:41 WG2058400
Dibenz(a,h)anthracene ND 0.0410 1 05/12/2023 17:41 WG2058400
3,3-Dichlorobenzidine ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dinitrotoluene ND 0.410 1 05/12/2023 17:41 WG2058400
2,6-Dinitrotoluene ND 0.410 1 05/12/2023 17:41 WG2058400
Fluoranthene ND 0.0410 1 05/12/2023 17:41 WG2058400
Fluorene ND 0.0410 1 05/12/2023 17:41 WG2058400
Hexachlorobenzene ND 0.410 1 05/12/2023 17:41 WG2058400
Hexachloro-1,3-butadiene ND 0.410 1 05/12/2023 17:41 WG2058400
Hexachlorocyclopentadiene ND 0.410 1 05/12/2023 17:41 WG2058400
Hexachloroethane ND 0.410 1 05/12/2023 17:41 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0410 1 05/12/2023 17:41 WG2058400
Isophorone ND 0.410 1 05/12/2023 17:41 WG2058400
Naphthalene ND 0.0410 1 05/12/2023 17:41 WG2058400
Nitrobenzene ND 0.410 1 05/12/2023 17:41 WG2058400
n-Nitrosodimethylamine ND 0.410 1 05/12/2023 17:41 WG2058400
n-Nitrosodiphenylamine ND 0.410 1 05/12/2023 17:41 WG2058400
n-Nitrosodi-n-propylamine ND 0.410 1 05/12/2023 17:41 WG2058400
Phenanthrene ND 0.0410 1 05/12/2023 17:41 WG2058400
Benzylbutyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1613187
MW-3
Collected date/time: 05/04/23 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Di-n-butyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Diethyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Dimethyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Di-n-octyl phthalate ND 0.410 1 05/12/2023 17:41 WG2058400
Pyrene ND 0.0410 1 05/12/2023 17:41 WG2058400
1,2,4-Trichlorobenzene ND 0.410 1 05/12/2023 17:41 WG2058400
4-Chloro-3-methylphenol ND 0.410 1 05/12/2023 17:41 WG2058400
2-Chlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dichlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dimethylphenol ND 0.410 1 05/12/2023 17:41 WG2058400
4,6-Dinitro-2-methylphenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4-Dinitrophenol ND 0.410 1 05/12/2023 17:41 WG2058400
2-Nitrophenol ND 0.410 1 05/12/2023 17:41 WG2058400
4-Nitrophenol ND 0.410 1 05/12/2023 17:41 WG2058400
Pentachlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
Phenol ND 0.410 1 05/12/2023 17:41 WG2058400
2,4,6-Trichlorophenol ND 0.410 1 05/12/2023 17:41 WG2058400
(S) Nitrobenzene-d5 57.6 10.0-122 05/12/2023 17:41 WG2058400
(S) 2-Fluorobiphenyl 50.2 15.0-120 05/12/2023 17:41 WG2058400
(S) p-Terphenyl-d14 51.1 10.0-120 05/12/2023 17:41 WG2058400
(S) Phenol-d5 53.1 10.0-120 05/12/2023 17:41 WG2058400
(S) 2-Fluorophenol 54.5 12.0-120 05/12/2023 17:41 WG2058400
(S) 2,4,6-Tribromophenol 35.2 10.0-127 05/12/2023 17:41 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00739 1 05/12/2023 03:03 WG2058011
Acenaphthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Acenaphthylene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(a)anthracene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(a)pyrene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(b)fluoranthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(g,h,i)perylene ND 0.00739 1 05/12/2023 03:03 WG2058011
Benzo(k)fluoranthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Chrysene ND 0.00739 1 05/12/2023 03:03 WG2058011
Dibenz(a,h)anthracene ND 0.00739 1 05/12/2023 03:03 WG2058011
Fluoranthene ND 0.00739 1 05/12/2023 03:03 WG2058011
Fluorene ND 0.00739 1 05/12/2023 03:03 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00739 1 05/12/2023 03:03 WG2058011
Naphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
Phenanthrene ND 0.00739 1 05/12/2023 03:03 WG2058011
Pyrene ND 0.00739 1 05/12/2023 03:03 WG2058011
1-Methylnaphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
2-Methylnaphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
2-Chloronaphthalene ND 0.0246 1 05/12/2023 03:03 WG2058011
(S) p-Terphenyl-d14 86.7 23.0-120 05/12/2023 03:03 WG2058011
(S) Nitrobenzene-d5 97.6 14.0-149 05/12/2023 03:03 WG2058011
(S) 2-Fluorobiphenyl 88.8 34.0-125 05/12/2023 03:03 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.6 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.17 1 05/11/2023 01:08 WG2056423
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0467 1 05/12/2023 12:28 WG2056112
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.34 1 05/10/2023 18:23 WG2055559
Arsenic 4.55 2.34 1 05/10/2023 18:23 WG2055559
Beryllium 0.353 0.234 1 05/10/2023 18:23 WG2055559
Cadmium ND 0.584 1 05/10/2023 18:23 WG2055559
Chromium 13.6 1.17 1 05/10/2023 18:23 WG2055559
Copper 14.1 2.34 1 05/10/2023 18:23 WG2055559
Lead 14.8 0.584 1 05/10/2023 18:23 WG2055559
Nickel 7.33 2.34 1 05/10/2023 18:23 WG2055559
Selenium ND 2.34 1 05/10/2023 18:23 WG2055559
Silver ND 1.17 1 05/10/2023 18:23 WG2055559
Thallium ND 2.34 1 05/10/2023 18:23 WG2055559
Zinc 48.7 5.84 1 05/10/2023 18:23 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.64 27.5 05/11/2023 12:46 WG2057784
(S) a,a,a-Trifluorotoluene(FID) 89.8 77.0-120 05/11/2023 12:46 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0727 1.1 05/11/2023 12:29 WG2058136
Acrylonitrile ND 0.0182 1.1 05/11/2023 12:29 WG2058136
Benzene ND 0.00145 1.1 05/11/2023 12:29 WG2058136
Bromobenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
Bromodichloromethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Bromoform ND 0.0364 1.1 05/11/2023 12:29 WG2058136
Bromomethane ND 0.0182 1.1 05/11/2023 12:29 WG2058136
n-Butylbenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
sec-Butylbenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
tert-Butylbenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Carbon tetrachloride ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Chlorobenzene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Chlorodibromomethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Chloroethane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Chloroform ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Chloromethane ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
4-Chlorotoluene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0364 1.1 05/11/2023 12:29 WG2058136
1,2-Dibromoethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Dibromomethane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2-Dichlorobenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,3-Dichlorobenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,4-Dichlorobenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Dichlorodifluoromethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1-Dichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,2-Dichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1-Dichloroethene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
cis-1,2-Dichloroethene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
trans-1,2-Dichloroethene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2-Dichloropropane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,1-Dichloropropene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,3-Dichloropropane ND 0.00727 1.1 05/11/2023 12:29 WG2058136
cis-1,3-Dichloropropene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
trans-1,3-Dichloropropene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
2,2-Dichloropropane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Di-isopropyl ether ND 0.00145 1.1 05/11/2023 12:29 WG2058136
Ethylbenzene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Hexachloro-1,3-butadiene ND 0.0364 1.1 05/11/2023 12:29 WG2058136
Isopropylbenzene ND 0.00364 1.1 05/11/2023 12:29 WG2058136
p-Isopropyltoluene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
2-Butanone (MEK)ND 0.145 1.1 05/11/2023 12:29 WG2058136
Methylene Chloride ND 0.0364 1.1 05/11/2023 12:29 WG2058136
4-Methyl-2-pentanone (MIBK) ND 0.0364 1.1 05/11/2023 12:29 WG2058136
Methyl tert-butyl ether ND 0.00145 1.1 05/11/2023 12:29 WG2058136
Naphthalene ND J4 0.0182 1.1 05/11/2023 12:29 WG2058136
n-Propylbenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
Styrene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Tetrachloroethene 0.787 0.00364 1.1 05/11/2023 12:29 WG2058136
Toluene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0182 1.1 05/11/2023 12:29 WG2058136
1,2,4-Trichlorobenzene ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1,1,1-Trichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,1,2-Trichloroethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Trichloroethene 0.00974 0.00145 1.1 05/11/2023 12:29 WG2058136
Trichlorofluoromethane ND 0.00364 1.1 05/11/2023 12:29 WG2058136
1,2,3-Trichloropropane ND 0.0182 1.1 05/11/2023 12:29 WG2058136
1,2,4-Trimethylbenzene ND 0.00727 1.1 05/11/2023 12:29 WG2058136
1,2,3-Trimethylbenzene 0.0416 0.00727 1.1 05/11/2023 12:29 WG2058136
1,3,5-Trimethylbenzene 0.0664 0.00727 1.1 05/11/2023 12:29 WG2058136
Vinyl chloride ND 0.00364 1.1 05/11/2023 12:29 WG2058136
Xylenes, Total 0.0148 0.00945 1.1 05/11/2023 12:29 WG2058136
(S) Toluene-d8 105 75.0-131 05/11/2023 12:29 WG2058136
(S) 4-Bromofluorobenzene 96.8 67.0-138 05/11/2023 12:29 WG2058136
(S) 1,2-Dichloroethane-d4 116 70.0-130 05/11/2023 12:29 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 467 100 05/14/2023 19:23 WG2059338
C28-C40 Oil Range 732 467 100 05/14/2023 19:23 WG2059338
(S) o-Terphenyl 39.6 J7 18.0-148 05/14/2023 19:23 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1221 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1232 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1242 ND 0.0397 1 05/13/2023 17:42 WG2057922
PCB 1248 ND 0.0199 1 05/13/2023 17:42 WG2057922
PCB 1254 ND 0.0199 1 05/13/2023 17:42 WG2057922
PCB 1260 ND 0.0199 1 05/13/2023 17:42 WG2057922
(S) Decachlorobiphenyl 81.8 10.0-135 05/13/2023 17:42 WG2057922
(S) Tetrachloro-m-xylene 90.0 10.0-139 05/13/2023 17:42 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.389 10 05/15/2023 21:59 WG2058400
Acenaphthylene ND 0.389 10 05/15/2023 21:59 WG2058400
Anthracene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzidine ND 19.5 10 05/15/2023 21:59 WG2058400
Benzo(a)anthracene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(b)fluoranthene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(k)fluoranthene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(g,h,i)perylene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzo(a)pyrene ND 0.389 10 05/15/2023 21:59 WG2058400
Bis(2-chlorethoxy)methane ND 3.89 10 05/15/2023 21:59 WG2058400
Bis(2-chloroethyl)ether ND 3.89 10 05/15/2023 21:59 WG2058400
2,2-Oxybis(1-Chloropropane) ND 3.89 10 05/15/2023 21:59 WG2058400
4-Bromophenyl-phenylether ND 3.89 10 05/15/2023 21:59 WG2058400
2-Chloronaphthalene ND 0.389 10 05/15/2023 21:59 WG2058400
4-Chlorophenyl-phenylether ND 3.89 10 05/15/2023 21:59 WG2058400
Chrysene ND 0.389 10 05/15/2023 21:59 WG2058400
Dibenz(a,h)anthracene ND 0.389 10 05/15/2023 21:59 WG2058400
3,3-Dichlorobenzidine ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dinitrotoluene ND 3.89 10 05/15/2023 21:59 WG2058400
2,6-Dinitrotoluene ND 3.89 10 05/15/2023 21:59 WG2058400
Fluoranthene ND 0.389 10 05/15/2023 21:59 WG2058400
Fluorene ND 0.389 10 05/15/2023 21:59 WG2058400
Hexachlorobenzene ND 3.89 10 05/15/2023 21:59 WG2058400
Hexachloro-1,3-butadiene ND 3.89 10 05/15/2023 21:59 WG2058400
Hexachlorocyclopentadiene ND 3.89 10 05/15/2023 21:59 WG2058400
Hexachloroethane ND 3.89 10 05/15/2023 21:59 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.389 10 05/15/2023 21:59 WG2058400
Isophorone ND 3.89 10 05/15/2023 21:59 WG2058400
Naphthalene ND 0.389 10 05/15/2023 21:59 WG2058400
Nitrobenzene ND 3.89 10 05/15/2023 21:59 WG2058400
n-Nitrosodimethylamine ND 3.89 10 05/15/2023 21:59 WG2058400
n-Nitrosodiphenylamine ND 3.89 10 05/15/2023 21:59 WG2058400
n-Nitrosodi-n-propylamine ND 3.89 10 05/15/2023 21:59 WG2058400
Phenanthrene ND 0.389 10 05/15/2023 21:59 WG2058400
Benzylbutyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1613187
MW-6
Collected date/time: 05/04/23 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Di-n-butyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Diethyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Dimethyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Di-n-octyl phthalate ND 3.89 10 05/15/2023 21:59 WG2058400
Pyrene ND 0.389 10 05/15/2023 21:59 WG2058400
1,2,4-Trichlorobenzene ND 3.89 10 05/15/2023 21:59 WG2058400
4-Chloro-3-methylphenol ND 3.89 10 05/15/2023 21:59 WG2058400
2-Chlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dichlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dimethylphenol ND 3.89 10 05/15/2023 21:59 WG2058400
4,6-Dinitro-2-methylphenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4-Dinitrophenol ND 3.89 10 05/15/2023 21:59 WG2058400
2-Nitrophenol ND 3.89 10 05/15/2023 21:59 WG2058400
4-Nitrophenol ND 3.89 10 05/15/2023 21:59 WG2058400
Pentachlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
Phenol ND 3.89 10 05/15/2023 21:59 WG2058400
2,4,6-Trichlorophenol ND 3.89 10 05/15/2023 21:59 WG2058400
(S) Nitrobenzene-d5 78.9 10.0-122 05/15/2023 21:59 WG2058400
(S) 2-Fluorobiphenyl 62.9 15.0-120 05/15/2023 21:59 WG2058400
(S) p-Terphenyl-d14 61.6 10.0-120 05/15/2023 21:59 WG2058400
(S) Phenol-d5 61.9 10.0-120 05/15/2023 21:59 WG2058400
(S) 2-Fluorophenol 43.4 12.0-120 05/15/2023 21:59 WG2058400
(S) 2,4,6-Tribromophenol 35.8 10.0-127 05/15/2023 21:59 WG2058400
Sample Narrative:
L1613187-02 WG2058400: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.0827 0.0701 10 05/12/2023 07:58 WG2058011
Acenaphthene ND 0.0701 10 05/12/2023 07:58 WG2058011
Acenaphthylene ND 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(a)anthracene 0.132 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(a)pyrene 0.118 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(b)fluoranthene 0.117 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(g,h,i)perylene 0.117 0.0701 10 05/12/2023 07:58 WG2058011
Benzo(k)fluoranthene ND 0.0701 10 05/12/2023 07:58 WG2058011
Chrysene 0.172 0.0701 10 05/12/2023 07:58 WG2058011
Dibenz(a,h)anthracene ND 0.0701 10 05/12/2023 07:58 WG2058011
Fluoranthene 0.268 0.0701 10 05/12/2023 07:58 WG2058011
Fluorene ND 0.0701 10 05/12/2023 07:58 WG2058011
Indeno(1,2,3-cd)pyrene 0.0742 0.0701 10 05/12/2023 07:58 WG2058011
Naphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
Phenanthrene 0.282 0.0701 10 05/12/2023 07:58 WG2058011
Pyrene 0.325 0.0701 10 05/12/2023 07:58 WG2058011
1-Methylnaphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
2-Methylnaphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
2-Chloronaphthalene ND 0.234 10 05/12/2023 07:58 WG2058011
(S) p-Terphenyl-d14 91.0 23.0-120 05/12/2023 07:58 WG2058011
(S) Nitrobenzene-d5 90.1 14.0-149 05/12/2023 07:58 WG2058011
(S) 2-Fluorobiphenyl 77.1 34.0-125 05/12/2023 07:58 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.4 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND J3 J6 1.29 1 05/11/2023 01:18 WG2056423
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0517 1 05/12/2023 12:30 WG2056112
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.59 1 05/10/2023 18:26 WG2055559
Arsenic 6.29 2.59 1 05/10/2023 18:26 WG2055559
Beryllium 0.406 0.259 1 05/10/2023 18:26 WG2055559
Cadmium ND 0.646 1 05/10/2023 18:26 WG2055559
Chromium 10.5 1.29 1 05/10/2023 18:26 WG2055559
Copper 17.0 2.59 1 05/10/2023 18:26 WG2055559
Lead 11.8 0.646 1 05/10/2023 18:26 WG2055559
Nickel 7.39 2.59 1 05/10/2023 18:26 WG2055559
Selenium ND 2.59 1 05/10/2023 18:26 WG2055559
Silver ND 1.29 1 05/10/2023 18:26 WG2055559
Thallium ND 2.59 1 05/10/2023 18:26 WG2055559
Zinc 39.0 6.46 1 05/10/2023 18:26 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.04 25 05/11/2023 13:05 WG2057784
(S) a,a,a-Trifluorotoluene(FID) 92.0 77.0-120 05/11/2023 13:05 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0808 1 05/11/2023 12:48 WG2058136
Acrylonitrile ND 0.0202 1 05/11/2023 12:48 WG2058136
Benzene ND 0.00162 1 05/11/2023 12:48 WG2058136
Bromobenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
Bromodichloromethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Bromoform ND 0.0404 1 05/11/2023 12:48 WG2058136
Bromomethane ND 0.0202 1 05/11/2023 12:48 WG2058136
n-Butylbenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
sec-Butylbenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
tert-Butylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Carbon tetrachloride ND 0.00808 1 05/11/2023 12:48 WG2058136
Chlorobenzene ND 0.00404 1 05/11/2023 12:48 WG2058136
Chlorodibromomethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Chloroethane ND 0.00808 1 05/11/2023 12:48 WG2058136
Chloroform ND 0.00404 1 05/11/2023 12:48 WG2058136
Chloromethane ND 0.0202 1 05/11/2023 12:48 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00404 1 05/11/2023 12:48 WG2058136
4-Chlorotoluene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0404 1 05/11/2023 12:48 WG2058136
1,2-Dibromoethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Dibromomethane ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2-Dichlorobenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,3-Dichlorobenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,4-Dichlorobenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Dichlorodifluoromethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1-Dichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,2-Dichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1-Dichloroethene ND 0.00404 1 05/11/2023 12:48 WG2058136
cis-1,2-Dichloroethene ND 0.00404 1 05/11/2023 12:48 WG2058136
trans-1,2-Dichloroethene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2-Dichloropropane ND 0.00808 1 05/11/2023 12:48 WG2058136
1,1-Dichloropropene ND 0.00404 1 05/11/2023 12:48 WG2058136
1,3-Dichloropropane ND 0.00808 1 05/11/2023 12:48 WG2058136
cis-1,3-Dichloropropene ND 0.00404 1 05/11/2023 12:48 WG2058136
trans-1,3-Dichloropropene ND 0.00808 1 05/11/2023 12:48 WG2058136
2,2-Dichloropropane ND 0.00404 1 05/11/2023 12:48 WG2058136
Di-isopropyl ether ND 0.00162 1 05/11/2023 12:48 WG2058136
Ethylbenzene ND 0.00404 1 05/11/2023 12:48 WG2058136
Hexachloro-1,3-butadiene ND 0.0404 1 05/11/2023 12:48 WG2058136
Isopropylbenzene ND 0.00404 1 05/11/2023 12:48 WG2058136
p-Isopropyltoluene ND 0.00808 1 05/11/2023 12:48 WG2058136
2-Butanone (MEK)ND 0.162 1 05/11/2023 12:48 WG2058136
Methylene Chloride ND 0.0404 1 05/11/2023 12:48 WG2058136
4-Methyl-2-pentanone (MIBK) ND 0.0404 1 05/11/2023 12:48 WG2058136
Methyl tert-butyl ether ND 0.00162 1 05/11/2023 12:48 WG2058136
Naphthalene ND J4 0.0202 1 05/11/2023 12:48 WG2058136
n-Propylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Styrene ND 0.0202 1 05/11/2023 12:48 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Tetrachloroethene ND 0.00404 1 05/11/2023 12:48 WG2058136
Toluene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0202 1 05/11/2023 12:48 WG2058136
1,2,4-Trichlorobenzene ND 0.0202 1 05/11/2023 12:48 WG2058136
1,1,1-Trichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,1,2-Trichloroethane ND 0.00404 1 05/11/2023 12:48 WG2058136
Trichloroethene ND 0.00162 1 05/11/2023 12:48 WG2058136
Trichlorofluoromethane ND 0.00404 1 05/11/2023 12:48 WG2058136
1,2,3-Trichloropropane ND 0.0202 1 05/11/2023 12:48 WG2058136
1,2,4-Trimethylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,2,3-Trimethylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
1,3,5-Trimethylbenzene ND 0.00808 1 05/11/2023 12:48 WG2058136
Vinyl chloride ND 0.00404 1 05/11/2023 12:48 WG2058136
Xylenes, Total ND 0.0105 1 05/11/2023 12:48 WG2058136
(S) Toluene-d8 107 75.0-131 05/11/2023 12:48 WG2058136
(S) 4-Bromofluorobenzene 97.7 67.0-138 05/11/2023 12:48 WG2058136
(S) 1,2-Dichloroethane-d4 117 70.0-130 05/11/2023 12:48 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.17 1 05/14/2023 01:38 WG2059338
C28-C40 Oil Range 5.88 5.17 1 05/14/2023 01:38 WG2059338
(S) o-Terphenyl 18.6 18.0-148 05/14/2023 01:38 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1221 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1232 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1242 ND 0.0439 1 05/13/2023 17:55 WG2057922
PCB 1248 ND 0.0220 1 05/13/2023 17:55 WG2057922
PCB 1254 ND 0.0220 1 05/13/2023 17:55 WG2057922
PCB 1260 ND 0.0220 1 05/13/2023 17:55 WG2057922
(S) Decachlorobiphenyl 41.4 10.0-135 05/13/2023 17:55 WG2057922
(S) Tetrachloro-m-xylene 67.0 10.0-139 05/13/2023 17:55 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Acenaphthylene ND 0.0430 1 05/12/2023 18:31 WG2058400
Anthracene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzidine ND 2.16 1 05/12/2023 18:31 WG2058400
Benzo(a)anthracene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(b)fluoranthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(k)fluoranthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(g,h,i)perylene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzo(a)pyrene ND 0.0430 1 05/12/2023 18:31 WG2058400
Bis(2-chlorethoxy)methane ND 0.430 1 05/12/2023 18:31 WG2058400
Bis(2-chloroethyl)ether ND 0.430 1 05/12/2023 18:31 WG2058400
2,2-Oxybis(1-Chloropropane) ND 0.430 1 05/12/2023 18:31 WG2058400
4-Bromophenyl-phenylether ND 0.430 1 05/12/2023 18:31 WG2058400
2-Chloronaphthalene ND 0.0430 1 05/12/2023 18:31 WG2058400
4-Chlorophenyl-phenylether ND 0.430 1 05/12/2023 18:31 WG2058400
Chrysene ND 0.0430 1 05/12/2023 18:31 WG2058400
Dibenz(a,h)anthracene ND 0.0430 1 05/12/2023 18:31 WG2058400
3,3-Dichlorobenzidine ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dinitrotoluene ND 0.430 1 05/12/2023 18:31 WG2058400
2,6-Dinitrotoluene ND 0.430 1 05/12/2023 18:31 WG2058400
Fluoranthene ND 0.0430 1 05/12/2023 18:31 WG2058400
Fluorene ND 0.0430 1 05/12/2023 18:31 WG2058400
Hexachlorobenzene ND 0.430 1 05/12/2023 18:31 WG2058400
Hexachloro-1,3-butadiene ND 0.430 1 05/12/2023 18:31 WG2058400
Hexachlorocyclopentadiene ND 0.430 1 05/12/2023 18:31 WG2058400
Hexachloroethane ND 0.430 1 05/12/2023 18:31 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0430 1 05/12/2023 18:31 WG2058400
Isophorone ND 0.430 1 05/12/2023 18:31 WG2058400
Naphthalene ND 0.0430 1 05/12/2023 18:31 WG2058400
Nitrobenzene ND 0.430 1 05/12/2023 18:31 WG2058400
n-Nitrosodimethylamine ND 0.430 1 05/12/2023 18:31 WG2058400
n-Nitrosodiphenylamine ND 0.430 1 05/12/2023 18:31 WG2058400
n-Nitrosodi-n-propylamine ND 0.430 1 05/12/2023 18:31 WG2058400
Phenanthrene ND 0.0430 1 05/12/2023 18:31 WG2058400
Benzylbutyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1613187
MW-4
Collected date/time: 05/04/23 11:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Di-n-butyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Diethyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Dimethyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Di-n-octyl phthalate ND 0.430 1 05/12/2023 18:31 WG2058400
Pyrene ND 0.0430 1 05/12/2023 18:31 WG2058400
1,2,4-Trichlorobenzene ND 0.430 1 05/12/2023 18:31 WG2058400
4-Chloro-3-methylphenol ND 0.430 1 05/12/2023 18:31 WG2058400
2-Chlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dichlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dimethylphenol ND 0.430 1 05/12/2023 18:31 WG2058400
4,6-Dinitro-2-methylphenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4-Dinitrophenol ND 0.430 1 05/12/2023 18:31 WG2058400
2-Nitrophenol ND 0.430 1 05/12/2023 18:31 WG2058400
4-Nitrophenol ND 0.430 1 05/12/2023 18:31 WG2058400
Pentachlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
Phenol ND 0.430 1 05/12/2023 18:31 WG2058400
2,4,6-Trichlorophenol ND 0.430 1 05/12/2023 18:31 WG2058400
(S) Nitrobenzene-d5 50.9 10.0-122 05/12/2023 18:31 WG2058400
(S) 2-Fluorobiphenyl 43.1 15.0-120 05/12/2023 18:31 WG2058400
(S) p-Terphenyl-d14 38.6 10.0-120 05/12/2023 18:31 WG2058400
(S) Phenol-d5 44.4 10.0-120 05/12/2023 18:31 WG2058400
(S) 2-Fluorophenol 50.2 12.0-120 05/12/2023 18:31 WG2058400
(S) 2,4,6-Tribromophenol 33.3 10.0-127 05/12/2023 18:31 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00776 1 05/12/2023 03:20 WG2058011
Acenaphthene ND 0.00776 1 05/12/2023 03:20 WG2058011
Acenaphthylene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(a)anthracene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(a)pyrene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(b)fluoranthene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(g,h,i)perylene ND 0.00776 1 05/12/2023 03:20 WG2058011
Benzo(k)fluoranthene ND 0.00776 1 05/12/2023 03:20 WG2058011
Chrysene ND 0.00776 1 05/12/2023 03:20 WG2058011
Dibenz(a,h)anthracene ND 0.00776 1 05/12/2023 03:20 WG2058011
Fluoranthene 0.0113 0.00776 1 05/12/2023 03:20 WG2058011
Fluorene ND 0.00776 1 05/12/2023 03:20 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00776 1 05/12/2023 03:20 WG2058011
Naphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
Phenanthrene ND 0.00776 1 05/12/2023 03:20 WG2058011
Pyrene 0.00777 0.00776 1 05/12/2023 03:20 WG2058011
1-Methylnaphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
2-Methylnaphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
2-Chloronaphthalene ND 0.0259 1 05/12/2023 03:20 WG2058011
(S) p-Terphenyl-d14 77.6 23.0-120 05/12/2023 03:20 WG2058011
(S) Nitrobenzene-d5 114 14.0-149 05/12/2023 03:20 WG2058011
(S) 2-Fluorobiphenyl 102 34.0-125 05/12/2023 03:20 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.7 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.22 1 05/11/2023 01:54 WG2056423
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0490 1 05/12/2023 12:36 WG2056112
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.45 1 05/10/2023 18:29 WG2055559
Arsenic 4.89 2.45 1 05/10/2023 18:29 WG2055559
Beryllium 0.288 0.245 1 05/10/2023 18:29 WG2055559
Cadmium ND 0.612 1 05/10/2023 18:29 WG2055559
Chromium 7.71 1.22 1 05/10/2023 18:29 WG2055559
Copper 7.43 2.45 1 05/10/2023 18:29 WG2055559
Lead 3.89 0.612 1 05/10/2023 18:29 WG2055559
Nickel 5.93 2.45 1 05/10/2023 18:29 WG2055559
Selenium ND 2.45 1 05/10/2023 18:29 WG2055559
Silver ND 1.22 1 05/10/2023 18:29 WG2055559
Thallium ND 2.45 1 05/10/2023 18:29 WG2055559
Zinc 23.3 6.12 1 05/10/2023 18:29 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.70 25 05/11/2023 13:24 WG2057784
(S) a,a,a-Trifluorotoluene(FID) 91.0 77.0-120 05/11/2023 13:24 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0740 1 05/11/2023 13:07 WG2058136
Acrylonitrile ND 0.0185 1 05/11/2023 13:07 WG2058136
Benzene ND 0.00148 1 05/11/2023 13:07 WG2058136
Bromobenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
Bromodichloromethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Bromoform ND 0.0370 1 05/11/2023 13:07 WG2058136
Bromomethane ND 0.0185 1 05/11/2023 13:07 WG2058136
n-Butylbenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
sec-Butylbenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
tert-Butylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Carbon tetrachloride ND 0.00740 1 05/11/2023 13:07 WG2058136
Chlorobenzene ND 0.00370 1 05/11/2023 13:07 WG2058136
Chlorodibromomethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Chloroethane ND 0.00740 1 05/11/2023 13:07 WG2058136
Chloroform ND 0.00370 1 05/11/2023 13:07 WG2058136
Chloromethane ND 0.0185 1 05/11/2023 13:07 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00370 1 05/11/2023 13:07 WG2058136
4-Chlorotoluene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0370 1 05/11/2023 13:07 WG2058136
1,2-Dibromoethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Dibromomethane ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2-Dichlorobenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,3-Dichlorobenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,4-Dichlorobenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Dichlorodifluoromethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1-Dichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,2-Dichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1-Dichloroethene ND 0.00370 1 05/11/2023 13:07 WG2058136
cis-1,2-Dichloroethene ND 0.00370 1 05/11/2023 13:07 WG2058136
trans-1,2-Dichloroethene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2-Dichloropropane ND 0.00740 1 05/11/2023 13:07 WG2058136
1,1-Dichloropropene ND 0.00370 1 05/11/2023 13:07 WG2058136
1,3-Dichloropropane ND 0.00740 1 05/11/2023 13:07 WG2058136
cis-1,3-Dichloropropene ND 0.00370 1 05/11/2023 13:07 WG2058136
trans-1,3-Dichloropropene ND 0.00740 1 05/11/2023 13:07 WG2058136
2,2-Dichloropropane ND 0.00370 1 05/11/2023 13:07 WG2058136
Di-isopropyl ether ND 0.00148 1 05/11/2023 13:07 WG2058136
Ethylbenzene ND 0.00370 1 05/11/2023 13:07 WG2058136
Hexachloro-1,3-butadiene ND 0.0370 1 05/11/2023 13:07 WG2058136
Isopropylbenzene ND 0.00370 1 05/11/2023 13:07 WG2058136
p-Isopropyltoluene ND 0.00740 1 05/11/2023 13:07 WG2058136
2-Butanone (MEK)ND 0.148 1 05/11/2023 13:07 WG2058136
Methylene Chloride ND 0.0370 1 05/11/2023 13:07 WG2058136
4-Methyl-2-pentanone (MIBK) ND 0.0370 1 05/11/2023 13:07 WG2058136
Methyl tert-butyl ether ND 0.00148 1 05/11/2023 13:07 WG2058136
Naphthalene ND J4 0.0185 1 05/11/2023 13:07 WG2058136
n-Propylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Styrene ND 0.0185 1 05/11/2023 13:07 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Tetrachloroethene ND 0.00370 1 05/11/2023 13:07 WG2058136
Toluene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0185 1 05/11/2023 13:07 WG2058136
1,2,4-Trichlorobenzene ND 0.0185 1 05/11/2023 13:07 WG2058136
1,1,1-Trichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,1,2-Trichloroethane ND 0.00370 1 05/11/2023 13:07 WG2058136
Trichloroethene ND 0.00148 1 05/11/2023 13:07 WG2058136
Trichlorofluoromethane ND 0.00370 1 05/11/2023 13:07 WG2058136
1,2,3-Trichloropropane ND 0.0185 1 05/11/2023 13:07 WG2058136
1,2,4-Trimethylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,2,3-Trimethylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
1,3,5-Trimethylbenzene ND 0.00740 1 05/11/2023 13:07 WG2058136
Vinyl chloride ND 0.00370 1 05/11/2023 13:07 WG2058136
Xylenes, Total ND 0.00962 1 05/11/2023 13:07 WG2058136
(S) Toluene-d8 103 75.0-131 05/11/2023 13:07 WG2058136
(S) 4-Bromofluorobenzene 102 67.0-138 05/11/2023 13:07 WG2058136
(S) 1,2-Dichloroethane-d4 119 70.0-130 05/11/2023 13:07 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 6.03 1.23 05/14/2023 01:25 WG2059338
C28-C40 Oil Range 6.18 6.03 1.23 05/14/2023 01:25 WG2059338
(S) o-Terphenyl 28.3 18.0-148 05/14/2023 01:25 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1221 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1232 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1242 ND 0.0416 1 05/13/2023 18:08 WG2057922
PCB 1248 ND 0.0208 1 05/13/2023 18:08 WG2057922
PCB 1254 ND 0.0208 1 05/13/2023 18:08 WG2057922
PCB 1260 ND 0.0208 1 05/13/2023 18:08 WG2057922
(S) Decachlorobiphenyl 52.4 10.0-135 05/13/2023 18:08 WG2057922
(S) Tetrachloro-m-xylene 73.4 10.0-139 05/13/2023 18:08 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Acenaphthylene ND 0.0408 1 05/12/2023 17:15 WG2058400
Anthracene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzidine ND 2.05 1 05/12/2023 17:15 WG2058400
Benzo(a)anthracene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(b)fluoranthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(k)fluoranthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(g,h,i)perylene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzo(a)pyrene ND 0.0408 1 05/12/2023 17:15 WG2058400
Bis(2-chlorethoxy)methane ND 0.408 1 05/12/2023 17:15 WG2058400
Bis(2-chloroethyl)ether ND 0.408 1 05/12/2023 17:15 WG2058400
2,2-Oxybis(1-Chloropropane) ND 0.408 1 05/12/2023 17:15 WG2058400
4-Bromophenyl-phenylether ND 0.408 1 05/12/2023 17:15 WG2058400
2-Chloronaphthalene ND 0.0408 1 05/12/2023 17:15 WG2058400
4-Chlorophenyl-phenylether ND 0.408 1 05/12/2023 17:15 WG2058400
Chrysene ND 0.0408 1 05/12/2023 17:15 WG2058400
Dibenz(a,h)anthracene ND 0.0408 1 05/12/2023 17:15 WG2058400
3,3-Dichlorobenzidine ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dinitrotoluene ND 0.408 1 05/12/2023 17:15 WG2058400
2,6-Dinitrotoluene ND 0.408 1 05/12/2023 17:15 WG2058400
Fluoranthene ND 0.0408 1 05/12/2023 17:15 WG2058400
Fluorene ND 0.0408 1 05/12/2023 17:15 WG2058400
Hexachlorobenzene ND 0.408 1 05/12/2023 17:15 WG2058400
Hexachloro-1,3-butadiene ND 0.408 1 05/12/2023 17:15 WG2058400
Hexachlorocyclopentadiene ND 0.408 1 05/12/2023 17:15 WG2058400
Hexachloroethane ND 0.408 1 05/12/2023 17:15 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0408 1 05/12/2023 17:15 WG2058400
Isophorone ND 0.408 1 05/12/2023 17:15 WG2058400
Naphthalene ND 0.0408 1 05/12/2023 17:15 WG2058400
Nitrobenzene ND 0.408 1 05/12/2023 17:15 WG2058400
n-Nitrosodimethylamine ND 0.408 1 05/12/2023 17:15 WG2058400
n-Nitrosodiphenylamine ND 0.408 1 05/12/2023 17:15 WG2058400
n-Nitrosodi-n-propylamine ND 0.408 1 05/12/2023 17:15 WG2058400
Phenanthrene ND 0.0408 1 05/12/2023 17:15 WG2058400
Benzylbutyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1613187
MW-1
Collected date/time: 05/04/23 12:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Di-n-butyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Diethyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Dimethyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Di-n-octyl phthalate ND 0.408 1 05/12/2023 17:15 WG2058400
Pyrene ND 0.0408 1 05/12/2023 17:15 WG2058400
1,2,4-Trichlorobenzene ND 0.408 1 05/12/2023 17:15 WG2058400
4-Chloro-3-methylphenol ND 0.408 1 05/12/2023 17:15 WG2058400
2-Chlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dichlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dimethylphenol ND 0.408 1 05/12/2023 17:15 WG2058400
4,6-Dinitro-2-methylphenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4-Dinitrophenol ND 0.408 1 05/12/2023 17:15 WG2058400
2-Nitrophenol ND 0.408 1 05/12/2023 17:15 WG2058400
4-Nitrophenol ND 0.408 1 05/12/2023 17:15 WG2058400
Pentachlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
Phenol ND 0.408 1 05/12/2023 17:15 WG2058400
2,4,6-Trichlorophenol ND 0.408 1 05/12/2023 17:15 WG2058400
(S) Nitrobenzene-d5 50.6 10.0-122 05/12/2023 17:15 WG2058400
(S) 2-Fluorobiphenyl 45.5 15.0-120 05/12/2023 17:15 WG2058400
(S) p-Terphenyl-d14 43.9 10.0-120 05/12/2023 17:15 WG2058400
(S) Phenol-d5 47.0 10.0-120 05/12/2023 17:15 WG2058400
(S) 2-Fluorophenol 51.2 12.0-120 05/12/2023 17:15 WG2058400
(S) 2,4,6-Tribromophenol 35.6 10.0-127 05/12/2023 17:15 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00735 1 05/12/2023 03:37 WG2058011
Acenaphthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Acenaphthylene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(a)anthracene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(a)pyrene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(b)fluoranthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(g,h,i)perylene ND 0.00735 1 05/12/2023 03:37 WG2058011
Benzo(k)fluoranthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Chrysene ND 0.00735 1 05/12/2023 03:37 WG2058011
Dibenz(a,h)anthracene ND 0.00735 1 05/12/2023 03:37 WG2058011
Fluoranthene ND 0.00735 1 05/12/2023 03:37 WG2058011
Fluorene ND 0.00735 1 05/12/2023 03:37 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00735 1 05/12/2023 03:37 WG2058011
Naphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
Phenanthrene ND 0.00735 1 05/12/2023 03:37 WG2058011
Pyrene ND 0.00735 1 05/12/2023 03:37 WG2058011
1-Methylnaphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
2-Methylnaphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
2-Chloronaphthalene ND 0.0245 1 05/12/2023 03:37 WG2058011
(S) p-Terphenyl-d14 89.3 23.0-120 05/12/2023 03:37 WG2058011
(S) Nitrobenzene-d5 111 14.0-149 05/12/2023 03:37 WG2058011
(S) 2-Fluorobiphenyl 99.0 34.0-125 05/12/2023 03:37 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.3 1 05/08/2023 15:55 WG2055430
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.28 1 05/11/2023 01:59 WG2056423
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0511 1 05/12/2023 12:38 WG2056112
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.55 1 05/10/2023 18:32 WG2055559
Arsenic 8.49 2.55 1 05/10/2023 18:32 WG2055559
Beryllium 0.443 0.255 1 05/10/2023 18:32 WG2055559
Cadmium ND 0.638 1 05/10/2023 18:32 WG2055559
Chromium 12.6 1.28 1 05/10/2023 18:32 WG2055559
Copper 16.3 2.55 1 05/10/2023 18:32 WG2055559
Lead 15.8 0.638 1 05/10/2023 18:32 WG2055559
Nickel 9.89 2.55 1 05/10/2023 18:32 WG2055559
Selenium ND 2.55 1 05/10/2023 18:32 WG2055559
Silver ND 1.28 1 05/10/2023 18:32 WG2055559
Thallium ND 2.55 1 05/10/2023 18:32 WG2055559
Zinc 39.7 6.38 1 05/10/2023 18:32 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.94 25 05/11/2023 13:42 WG2057784
(S) a,a,a-Trifluorotoluene(FID) 90.4 77.0-120 05/11/2023 13:42 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0788 1 05/11/2023 13:26 WG2058136
Acrylonitrile ND 0.0197 1 05/11/2023 13:26 WG2058136
Benzene ND 0.00158 1 05/11/2023 13:26 WG2058136
Bromobenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
Bromodichloromethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Bromoform ND 0.0394 1 05/11/2023 13:26 WG2058136
Bromomethane ND 0.0197 1 05/11/2023 13:26 WG2058136
n-Butylbenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
sec-Butylbenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
tert-Butylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Carbon tetrachloride ND 0.00788 1 05/11/2023 13:26 WG2058136
Chlorobenzene ND 0.00394 1 05/11/2023 13:26 WG2058136
Chlorodibromomethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Chloroethane ND 0.00788 1 05/11/2023 13:26 WG2058136
Chloroform ND 0.00394 1 05/11/2023 13:26 WG2058136
Chloromethane ND 0.0197 1 05/11/2023 13:26 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00394 1 05/11/2023 13:26 WG2058136
4-Chlorotoluene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0394 1 05/11/2023 13:26 WG2058136
1,2-Dibromoethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Dibromomethane ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2-Dichlorobenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,3-Dichlorobenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,4-Dichlorobenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Dichlorodifluoromethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1-Dichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,2-Dichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1-Dichloroethene ND 0.00394 1 05/11/2023 13:26 WG2058136
cis-1,2-Dichloroethene ND 0.00394 1 05/11/2023 13:26 WG2058136
trans-1,2-Dichloroethene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2-Dichloropropane ND 0.00788 1 05/11/2023 13:26 WG2058136
1,1-Dichloropropene ND 0.00394 1 05/11/2023 13:26 WG2058136
1,3-Dichloropropane ND 0.00788 1 05/11/2023 13:26 WG2058136
cis-1,3-Dichloropropene ND 0.00394 1 05/11/2023 13:26 WG2058136
trans-1,3-Dichloropropene ND 0.00788 1 05/11/2023 13:26 WG2058136
2,2-Dichloropropane ND 0.00394 1 05/11/2023 13:26 WG2058136
Di-isopropyl ether ND 0.00158 1 05/11/2023 13:26 WG2058136
Ethylbenzene 0.0196 0.00394 1 05/11/2023 13:26 WG2058136
Hexachloro-1,3-butadiene ND 0.0394 1 05/11/2023 13:26 WG2058136
Isopropylbenzene ND 0.00394 1 05/11/2023 13:26 WG2058136
p-Isopropyltoluene ND 0.00788 1 05/11/2023 13:26 WG2058136
2-Butanone (MEK)ND 0.158 1 05/11/2023 13:26 WG2058136
Methylene Chloride ND 0.0394 1 05/11/2023 13:26 WG2058136
4-Methyl-2-pentanone (MIBK) ND 0.0394 1 05/11/2023 13:26 WG2058136
Methyl tert-butyl ether ND 0.00158 1 05/11/2023 13:26 WG2058136
Naphthalene ND J4 0.0197 1 05/11/2023 13:26 WG2058136
n-Propylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Styrene ND 0.0197 1 05/11/2023 13:26 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Tetrachloroethene ND 0.00394 1 05/11/2023 13:26 WG2058136
Toluene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0197 1 05/11/2023 13:26 WG2058136
1,2,4-Trichlorobenzene ND 0.0197 1 05/11/2023 13:26 WG2058136
1,1,1-Trichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,1,2-Trichloroethane ND 0.00394 1 05/11/2023 13:26 WG2058136
Trichloroethene ND 0.00158 1 05/11/2023 13:26 WG2058136
Trichlorofluoromethane ND 0.00394 1 05/11/2023 13:26 WG2058136
1,2,3-Trichloropropane ND 0.0197 1 05/11/2023 13:26 WG2058136
1,2,4-Trimethylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,2,3-Trimethylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
1,3,5-Trimethylbenzene ND 0.00788 1 05/11/2023 13:26 WG2058136
Vinyl chloride ND 0.00394 1 05/11/2023 13:26 WG2058136
Xylenes, Total 0.102 0.0103 1 05/11/2023 13:26 WG2058136
(S) Toluene-d8 101 75.0-131 05/11/2023 13:26 WG2058136
(S) 4-Bromofluorobenzene 101 67.0-138 05/11/2023 13:26 WG2058136
(S) 1,2-Dichloroethane-d4 120 70.0-130 05/11/2023 13:26 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.11 1 05/14/2023 02:31 WG2059338
C28-C40 Oil Range 8.45 5.11 1 05/14/2023 02:31 WG2059338
(S) o-Terphenyl 31.9 18.0-148 05/14/2023 02:31 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1221 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1232 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1242 ND 0.0434 1 05/13/2023 18:20 WG2057922
PCB 1248 ND 0.0217 1 05/13/2023 18:20 WG2057922
PCB 1254 ND 0.0217 1 05/13/2023 18:20 WG2057922
PCB 1260 ND 0.0217 1 05/13/2023 18:20 WG2057922
(S) Decachlorobiphenyl 61.7 10.0-135 05/13/2023 18:20 WG2057922
(S) Tetrachloro-m-xylene 82.3 10.0-139 05/13/2023 18:20 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Acenaphthylene ND 0.0425 1 05/12/2023 18:55 WG2058400
Anthracene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzidine ND 2.13 1 05/12/2023 18:55 WG2058400
Benzo(a)anthracene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(b)fluoranthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(k)fluoranthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(g,h,i)perylene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzo(a)pyrene ND 0.0425 1 05/12/2023 18:55 WG2058400
Bis(2-chlorethoxy)methane ND 0.425 1 05/12/2023 18:55 WG2058400
Bis(2-chloroethyl)ether ND 0.425 1 05/12/2023 18:55 WG2058400
2,2-Oxybis(1-Chloropropane) ND 0.425 1 05/12/2023 18:55 WG2058400
4-Bromophenyl-phenylether ND 0.425 1 05/12/2023 18:55 WG2058400
2-Chloronaphthalene ND 0.0425 1 05/12/2023 18:55 WG2058400
4-Chlorophenyl-phenylether ND 0.425 1 05/12/2023 18:55 WG2058400
Chrysene ND 0.0425 1 05/12/2023 18:55 WG2058400
Dibenz(a,h)anthracene ND 0.0425 1 05/12/2023 18:55 WG2058400
3,3-Dichlorobenzidine ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dinitrotoluene ND 0.425 1 05/12/2023 18:55 WG2058400
2,6-Dinitrotoluene ND 0.425 1 05/12/2023 18:55 WG2058400
Fluoranthene ND 0.0425 1 05/12/2023 18:55 WG2058400
Fluorene ND 0.0425 1 05/12/2023 18:55 WG2058400
Hexachlorobenzene ND 0.425 1 05/12/2023 18:55 WG2058400
Hexachloro-1,3-butadiene ND 0.425 1 05/12/2023 18:55 WG2058400
Hexachlorocyclopentadiene ND 0.425 1 05/12/2023 18:55 WG2058400
Hexachloroethane ND 0.425 1 05/12/2023 18:55 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0425 1 05/12/2023 18:55 WG2058400
Isophorone ND 0.425 1 05/12/2023 18:55 WG2058400
Naphthalene ND 0.0425 1 05/12/2023 18:55 WG2058400
Nitrobenzene ND 0.425 1 05/12/2023 18:55 WG2058400
n-Nitrosodimethylamine ND 0.425 1 05/12/2023 18:55 WG2058400
n-Nitrosodiphenylamine ND 0.425 1 05/12/2023 18:55 WG2058400
n-Nitrosodi-n-propylamine ND 0.425 1 05/12/2023 18:55 WG2058400
Phenanthrene ND 0.0425 1 05/12/2023 18:55 WG2058400
Benzylbutyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1613187
MW-2
Collected date/time: 05/04/23 13:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Di-n-butyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Diethyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Dimethyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Di-n-octyl phthalate ND 0.425 1 05/12/2023 18:55 WG2058400
Pyrene ND 0.0425 1 05/12/2023 18:55 WG2058400
1,2,4-Trichlorobenzene ND 0.425 1 05/12/2023 18:55 WG2058400
4-Chloro-3-methylphenol ND 0.425 1 05/12/2023 18:55 WG2058400
2-Chlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dichlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dimethylphenol ND 0.425 1 05/12/2023 18:55 WG2058400
4,6-Dinitro-2-methylphenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4-Dinitrophenol ND 0.425 1 05/12/2023 18:55 WG2058400
2-Nitrophenol ND 0.425 1 05/12/2023 18:55 WG2058400
4-Nitrophenol ND 0.425 1 05/12/2023 18:55 WG2058400
Pentachlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
Phenol ND 0.425 1 05/12/2023 18:55 WG2058400
2,4,6-Trichlorophenol ND 0.425 1 05/12/2023 18:55 WG2058400
(S) Nitrobenzene-d5 59.6 10.0-122 05/12/2023 18:55 WG2058400
(S) 2-Fluorobiphenyl 51.7 15.0-120 05/12/2023 18:55 WG2058400
(S) p-Terphenyl-d14 55.8 10.0-120 05/12/2023 18:55 WG2058400
(S) Phenol-d5 51.1 10.0-120 05/12/2023 18:55 WG2058400
(S) 2-Fluorophenol 55.2 12.0-120 05/12/2023 18:55 WG2058400
(S) 2,4,6-Tribromophenol 37.1 10.0-127 05/12/2023 18:55 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00766 1 05/12/2023 03:55 WG2058011
Acenaphthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Acenaphthylene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(a)anthracene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(a)pyrene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(b)fluoranthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(g,h,i)perylene ND 0.00766 1 05/12/2023 03:55 WG2058011
Benzo(k)fluoranthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Chrysene ND 0.00766 1 05/12/2023 03:55 WG2058011
Dibenz(a,h)anthracene ND 0.00766 1 05/12/2023 03:55 WG2058011
Fluoranthene ND 0.00766 1 05/12/2023 03:55 WG2058011
Fluorene ND 0.00766 1 05/12/2023 03:55 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00766 1 05/12/2023 03:55 WG2058011
Naphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
Phenanthrene ND 0.00766 1 05/12/2023 03:55 WG2058011
Pyrene ND 0.00766 1 05/12/2023 03:55 WG2058011
1-Methylnaphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
2-Methylnaphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
2-Chloronaphthalene ND 0.0255 1 05/12/2023 03:55 WG2058011
(S) p-Terphenyl-d14 94.5 23.0-120 05/12/2023 03:55 WG2058011
(S) Nitrobenzene-d5 105 14.0-149 05/12/2023 03:55 WG2058011
(S) 2-Fluorobiphenyl 91.5 34.0-125 05/12/2023 03:55 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.3 1 05/08/2023 15:17 WG2055863
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.17 1 05/11/2023 02:05 WG2056423
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0469 1 05/12/2023 12:40 WG2056112
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.34 1 05/10/2023 18:35 WG2055559
Arsenic 6.04 2.34 1 05/10/2023 18:35 WG2055559
Beryllium 0.310 0.234 1 05/10/2023 18:35 WG2055559
Cadmium ND 0.586 1 05/10/2023 18:35 WG2055559
Chromium 7.97 1.17 1 05/10/2023 18:35 WG2055559
Copper 5.59 2.34 1 05/10/2023 18:35 WG2055559
Lead 3.71 0.586 1 05/10/2023 18:35 WG2055559
Nickel 5.22 2.34 1 05/10/2023 18:35 WG2055559
Selenium ND 2.34 1 05/10/2023 18:35 WG2055559
Silver ND 1.17 1 05/10/2023 18:35 WG2055559
Thallium ND 2.34 1 05/10/2023 18:35 WG2055559
Zinc 20.7 5.86 1 05/10/2023 18:35 WG2055559
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.94 30 05/11/2023 14:01 WG2057784
(S) a,a,a-Trifluorotoluene(FID) 91.5 77.0-120 05/11/2023 14:01 WG2057784
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0801 0.0789 1.2 05/11/2023 13:45 WG2058136
Acrylonitrile ND 0.0197 1.2 05/11/2023 13:45 WG2058136
Benzene ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Bromobenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
Bromodichloromethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Bromoform ND 0.0394 1.2 05/11/2023 13:45 WG2058136
Bromomethane ND 0.0197 1.2 05/11/2023 13:45 WG2058136
n-Butylbenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
sec-Butylbenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
tert-Butylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Carbon tetrachloride ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Chlorobenzene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Chlorodibromomethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Chloroethane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Chloroform ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Chloromethane ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
4-Chlorotoluene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2-Dibromo-3-Chloropropane ND 0.0394 1.2 05/11/2023 13:45 WG2058136
1,2-Dibromoethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Dibromomethane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2-Dichlorobenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,3-Dichlorobenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,4-Dichlorobenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Dichlorodifluoromethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1-Dichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,2-Dichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1-Dichloroethene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
cis-1,2-Dichloroethene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
trans-1,2-Dichloroethene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2-Dichloropropane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,1-Dichloropropene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,3-Dichloropropane ND 0.00789 1.2 05/11/2023 13:45 WG2058136
cis-1,3-Dichloropropene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
trans-1,3-Dichloropropene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
2,2-Dichloropropane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Di-isopropyl ether ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Ethylbenzene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Hexachloro-1,3-butadiene ND 0.0394 1.2 05/11/2023 13:45 WG2058136
Isopropylbenzene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
p-Isopropyltoluene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
2-Butanone (MEK)ND 0.158 1.2 05/11/2023 13:45 WG2058136
Methylene Chloride ND 0.0394 1.2 05/11/2023 13:45 WG2058136
4-Methyl-2-pentanone (MIBK) ND 0.0394 1.2 05/11/2023 13:45 WG2058136
Methyl tert-butyl ether ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Naphthalene ND J4 0.0197 1.2 05/11/2023 13:45 WG2058136
n-Propylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Styrene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1,1,1,2-Tetrachloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1,2,2-Tetrachloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1,2-Trichlorotrifluoroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Tetrachloroethene ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Toluene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2,3-Trichlorobenzene ND J4 0.0197 1.2 05/11/2023 13:45 WG2058136
1,2,4-Trichlorobenzene ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1,1,1-Trichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,1,2-Trichloroethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Trichloroethene ND 0.00158 1.2 05/11/2023 13:45 WG2058136
Trichlorofluoromethane ND 0.00394 1.2 05/11/2023 13:45 WG2058136
1,2,3-Trichloropropane ND 0.0197 1.2 05/11/2023 13:45 WG2058136
1,2,4-Trimethylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,2,3-Trimethylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
1,3,5-Trimethylbenzene ND 0.00789 1.2 05/11/2023 13:45 WG2058136
Vinyl chloride ND 0.00394 1.2 05/11/2023 13:45 WG2058136
Xylenes, Total ND 0.0103 1.2 05/11/2023 13:45 WG2058136
(S) Toluene-d8 102 75.0-131 05/11/2023 13:45 WG2058136
(S) 4-Bromofluorobenzene 101 67.0-138 05/11/2023 13:45 WG2058136
(S) 1,2-Dichloroethane-d4 121 70.0-130 05/11/2023 13:45 WG2058136
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 4.69 1 05/14/2023 00:03 WG2059338
C28-C40 Oil Range ND 4.69 1 05/14/2023 00:03 WG2059338
(S) o-Terphenyl 27.9 18.0-148 05/14/2023 00:03 WG2059338
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1221 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1232 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1242 ND 0.0398 1 05/13/2023 18:33 WG2057922
PCB 1248 ND 0.0199 1 05/13/2023 18:33 WG2057922
PCB 1254 ND 0.0199 1 05/13/2023 18:33 WG2057922
PCB 1260 ND 0.0199 1 05/13/2023 18:33 WG2057922
(S) Decachlorobiphenyl 53.3 10.0-135 05/13/2023 18:33 WG2057922
(S) Tetrachloro-m-xylene 72.9 10.0-139 05/13/2023 18:33 WG2057922
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Acenaphthylene ND 0.0390 1 05/12/2023 16:26 WG2058400
Anthracene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzidine ND 1.96 1 05/12/2023 16:26 WG2058400
Benzo(a)anthracene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(b)fluoranthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(k)fluoranthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(g,h,i)perylene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzo(a)pyrene ND 0.0390 1 05/12/2023 16:26 WG2058400
Bis(2-chlorethoxy)methane ND 0.390 1 05/12/2023 16:26 WG2058400
Bis(2-chloroethyl)ether ND 0.390 1 05/12/2023 16:26 WG2058400
2,2-Oxybis(1-Chloropropane) ND 0.390 1 05/12/2023 16:26 WG2058400
4-Bromophenyl-phenylether ND 0.390 1 05/12/2023 16:26 WG2058400
2-Chloronaphthalene ND 0.0390 1 05/12/2023 16:26 WG2058400
4-Chlorophenyl-phenylether ND 0.390 1 05/12/2023 16:26 WG2058400
Chrysene ND 0.0390 1 05/12/2023 16:26 WG2058400
Dibenz(a,h)anthracene ND 0.0390 1 05/12/2023 16:26 WG2058400
3,3-Dichlorobenzidine ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dinitrotoluene ND 0.390 1 05/12/2023 16:26 WG2058400
2,6-Dinitrotoluene ND 0.390 1 05/12/2023 16:26 WG2058400
Fluoranthene ND 0.0390 1 05/12/2023 16:26 WG2058400
Fluorene ND 0.0390 1 05/12/2023 16:26 WG2058400
Hexachlorobenzene ND 0.390 1 05/12/2023 16:26 WG2058400
Hexachloro-1,3-butadiene ND 0.390 1 05/12/2023 16:26 WG2058400
Hexachlorocyclopentadiene ND 0.390 1 05/12/2023 16:26 WG2058400
Hexachloroethane ND 0.390 1 05/12/2023 16:26 WG2058400
Indeno(1,2,3-cd)pyrene ND 0.0390 1 05/12/2023 16:26 WG2058400
Isophorone ND 0.390 1 05/12/2023 16:26 WG2058400
Naphthalene ND 0.0390 1 05/12/2023 16:26 WG2058400
Nitrobenzene ND 0.390 1 05/12/2023 16:26 WG2058400
n-Nitrosodimethylamine ND 0.390 1 05/12/2023 16:26 WG2058400
n-Nitrosodiphenylamine ND 0.390 1 05/12/2023 16:26 WG2058400
n-Nitrosodi-n-propylamine ND 0.390 1 05/12/2023 16:26 WG2058400
Phenanthrene ND 0.0390 1 05/12/2023 16:26 WG2058400
Benzylbutyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1613187
MW-5
Collected date/time: 05/04/23 14:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Di-n-butyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Diethyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Dimethyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Di-n-octyl phthalate ND 0.390 1 05/12/2023 16:26 WG2058400
Pyrene ND 0.0390 1 05/12/2023 16:26 WG2058400
1,2,4-Trichlorobenzene ND 0.390 1 05/12/2023 16:26 WG2058400
4-Chloro-3-methylphenol ND 0.390 1 05/12/2023 16:26 WG2058400
2-Chlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dichlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dimethylphenol ND 0.390 1 05/12/2023 16:26 WG2058400
4,6-Dinitro-2-methylphenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4-Dinitrophenol ND 0.390 1 05/12/2023 16:26 WG2058400
2-Nitrophenol ND 0.390 1 05/12/2023 16:26 WG2058400
4-Nitrophenol ND 0.390 1 05/12/2023 16:26 WG2058400
Pentachlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
Phenol ND 0.390 1 05/12/2023 16:26 WG2058400
2,4,6-Trichlorophenol ND 0.390 1 05/12/2023 16:26 WG2058400
(S) Nitrobenzene-d5 54.4 10.0-122 05/12/2023 16:26 WG2058400
(S) 2-Fluorobiphenyl 46.8 15.0-120 05/12/2023 16:26 WG2058400
(S) p-Terphenyl-d14 51.1 10.0-120 05/12/2023 16:26 WG2058400
(S) Phenol-d5 45.6 10.0-120 05/12/2023 16:26 WG2058400
(S) 2-Fluorophenol 53.2 12.0-120 05/12/2023 16:26 WG2058400
(S) 2,4,6-Tribromophenol 39.4 10.0-127 05/12/2023 16:26 WG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00703 1 05/12/2023 04:12 WG2058011
Acenaphthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Acenaphthylene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(a)anthracene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(a)pyrene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(b)fluoranthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(g,h,i)perylene ND 0.00703 1 05/12/2023 04:12 WG2058011
Benzo(k)fluoranthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Chrysene ND 0.00703 1 05/12/2023 04:12 WG2058011
Dibenz(a,h)anthracene ND 0.00703 1 05/12/2023 04:12 WG2058011
Fluoranthene ND 0.00703 1 05/12/2023 04:12 WG2058011
Fluorene ND 0.00703 1 05/12/2023 04:12 WG2058011
Indeno(1,2,3-cd)pyrene ND 0.00703 1 05/12/2023 04:12 WG2058011
Naphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
Phenanthrene ND 0.00703 1 05/12/2023 04:12 WG2058011
Pyrene ND 0.00703 1 05/12/2023 04:12 WG2058011
1-Methylnaphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
2-Methylnaphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
2-Chloronaphthalene ND 0.0234 1 05/12/2023 04:12 WG2058011
(S) p-Terphenyl-d14 86.2 23.0-120 05/12/2023 04:12 WG2058011
(S) Nitrobenzene-d5 97.0 14.0-149 05/12/2023 04:12 WG2058011
(S) 2-Fluorobiphenyl 87.8 34.0-125 05/12/2023 04:12 WG2058011
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055430
Total Solids by Method 2540 G-2011 L1613187-01,02,03,04,05
Method Blank (MB)
(MB) R3922359-1 05/08/23 15:55
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1613174-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1613174-05 05/08/23 15:55 • (DUP) R3922359-3 05/08/23 15:55
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 86.3 85.9 1 0.432 10
Laboratory Control Sample (LCS)
(LCS) R3922359-2 05/08/23 15:55
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2055863
Total Solids by Method 2540 G-2011 L1613187-06
Method Blank (MB)
(MB) R3922349-1 05/08/23 15:17
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1613207-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1613207-01 05/08/23 15:17 • (DUP) R3922349-3 05/08/23 15:17
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 79.5 79.9 1 0.495 10
Laboratory Control Sample (LCS)
(LCS) R3922349-2 05/08/23 15:17
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2056423
Wet Chemistry by Method 7199 L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3923385-1 05/11/23 00:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1613187-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1613187-02 05/11/23 01:08 • (DUP) R3923385-3 05/11/23 01:13
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.872 20
L1613243-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1613243-02 05/11/23 02:41 • (DUP) R3923385-8 05/11/23 03:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3923385-2 05/11/23 00:57
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 9.33 93.3 80.0-120
L1613187-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613187-03 05/11/23 01:18 • (MS) R3923385-5 05/11/23 01:28 • (MSD) R3923385-6 05/11/23 01:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 25.9 ND 9.11 16.0 35.2 61.8 1 75.0-125 J6 J3 J6 54.7 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2056423
Wet Chemistry by Method 7199 L1613187-01,02,03,04,05,06
L1613187-03 Original Sample (OS) • Matrix Spike (MS)
(OS) L1613187-03 05/11/23 01:18 • (MS) R3923385-7 05/11/23 01:39
Spike Amount
(dry)
Original Result
(dry)MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 825 ND 579 70.2 50 75.0-125 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2056112
Mercury by Method 7471A L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924090-1 05/12/23 11:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3924090-2 05/12/23 11:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.598 120 80.0-120
L1613337-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613337-01 05/12/23 11:49 • (MS) R3924090-3 05/12/23 11:51 • (MSD) R3924090-4 05/12/23 11:53
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.504 ND 0.566 0.598 112 119 1 75.0-125 5.43 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055559
Metals (ICP) by Method 6010B L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3923333-1 05/10/23 17:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3923333-2 05/10/23 17:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 99.9 99.9 80.0-120
Arsenic 100 97.2 97.2 80.0-120
Beryllium 100 98.1 98.1 80.0-120
Cadmium 100 97.4 97.4 80.0-120
Chromium 100 98.8 98.8 80.0-120
Copper 100 105 105 80.0-120
Lead 100 92.9 92.9 80.0-120
Nickel 100 94.9 94.9 80.0-120
Selenium 100 102 102 80.0-120
Silver 20.0 19.8 98.9 80.0-120
Thallium 100 96.3 96.3 80.0-120
Zinc 100 96.0 96.0 80.0-120
L1613201-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613201-01 05/10/23 17:40 • (MS) R3923333-5 05/10/23 17:48 • (MSD) R3923333-6 05/10/23 17:50
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Antimony 131 ND 51.0 50.8 38.8 38.7 1 75.0-125 J6 J6 0.263 20
Arsenic 131 ND 116 117 88.1 88.5 1 75.0-125 0.522 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2055559
Metals (ICP) by Method 6010B L1613187-01,02,03,04,05,06
L1613201-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613201-01 05/10/23 17:40 • (MS) R3923333-5 05/10/23 17:48 • (MSD) R3923333-6 05/10/23 17:50
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Beryllium 131 0.371 124 123 93.9 93.5 1 75.0-125 0.422 20
Cadmium 131 ND 123 122 93.8 92.8 1 75.0-125 1.03 20
Chromium 131 4.77 132 130 96.8 95.2 1 75.0-125 1.65 20
Copper 131 3.83 140 138 104 102 1 75.0-125 1.58 20
Lead 131 4.96 125 125 91.6 91.3 1 75.0-125 0.387 20
Nickel 131 ND 127 126 95.3 94.5 1 75.0-125 0.831 20
Selenium 131 ND 122 122 92.7 92.8 1 75.0-125 0.121 20
Silver 26.3 ND 25.4 25.0 96.6 95.4 1 75.0-125 1.29 20
Thallium 131 ND 121 118 92.0 89.8 1 75.0-125 2.37 20
Zinc 131 14.3 145 143 99.3 97.8 1 75.0-125 1.40 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057784
Volatile Organic Compounds (GC) by Method 8015D/GRO L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924133-2 05/11/23 02:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)92.0 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3924133-1 05/11/23 01:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 4.61 83.8 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 97.2 77.0-120
L1613158-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613158-01 05/11/23 11:32 • (MS) R3924133-3 05/11/23 14:37 • (MSD) R3924133-4 05/11/23 14:56
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 163 ND 135 130 81.9 78.9 25 10.0-151 3.71 28
(S)
a,a,a-Trifluorotoluene(FID) 97.5 95.6 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924032-3 05/11/23 10:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924032-3 05/11/23 10:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.000875 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 91.4 67.0-138
(S) 1,2-Dichloroethane-d4 113 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3924032-1 05/11/23 08:53 • (LCSD) R3924032-2 05/11/23 09:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.868 0.874 139 140 10.0-160 0.689 31
Acrylonitrile 0.625 0.650 0.668 104 107 45.0-153 2.73 22
Benzene 0.125 0.118 0.120 94.4 96.0 70.0-123 1.68 20
Bromobenzene 0.125 0.108 0.115 86.4 92.0 73.0-121 6.28 20
Bromodichloromethane 0.125 0.121 0.127 96.8 102 73.0-121 4.84 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3924032-1 05/11/23 08:53 • (LCSD) R3924032-2 05/11/23 09:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.108 0.111 86.4 88.8 64.0-132 2.74 20
Bromomethane 0.125 0.123 0.125 98.4 100 56.0-147 1.61 20
n-Butylbenzene 0.125 0.130 0.138 104 110 68.0-135 5.97 20
sec-Butylbenzene 0.125 0.125 0.137 100 110 74.0-130 9.16 20
tert-Butylbenzene 0.125 0.116 0.125 92.8 100 75.0-127 7.47 20
Carbon tetrachloride 0.125 0.116 0.123 92.8 98.4 66.0-128 5.86 20
Chlorobenzene 0.125 0.109 0.114 87.2 91.2 76.0-128 4.48 20
Chlorodibromomethane 0.125 0.111 0.110 88.8 88.0 74.0-127 0.905 20
Chloroethane 0.125 0.128 0.127 102 102 61.0-134 0.784 20
Chloroform 0.125 0.122 0.123 97.6 98.4 72.0-123 0.816 20
Chloromethane 0.125 0.134 0.135 107 108 51.0-138 0.743 20
2-Chlorotoluene 0.125 0.121 0.131 96.8 105 75.0-124 7.94 20
4-Chlorotoluene 0.125 0.117 0.123 93.6 98.4 75.0-124 5.00 20
1,2-Dibromo-3-Chloropropane 0.125 0.0927 0.0934 74.2 74.7 59.0-130 0.752 20
1,2-Dibromoethane 0.125 0.106 0.109 84.8 87.2 74.0-128 2.79 20
Dibromomethane 0.125 0.120 0.123 96.0 98.4 75.0-122 2.47 20
1,2-Dichlorobenzene 0.125 0.117 0.120 93.6 96.0 76.0-124 2.53 20
1,3-Dichlorobenzene 0.125 0.120 0.122 96.0 97.6 76.0-125 1.65 20
1,4-Dichlorobenzene 0.125 0.118 0.121 94.4 96.8 77.0-121 2.51 20
Dichlorodifluoromethane 0.125 0.113 0.113 90.4 90.4 43.0-156 0.000 20
1,1-Dichloroethane 0.125 0.126 0.130 101 104 70.0-127 3.12 20
1,2-Dichloroethane 0.125 0.141 0.144 113 115 65.0-131 2.11 20
1,1-Dichloroethene 0.125 0.137 0.139 110 111 65.0-131 1.45 20
cis-1,2-Dichloroethene 0.125 0.115 0.119 92.0 95.2 73.0-125 3.42 20
trans-1,2-Dichloroethene 0.125 0.114 0.117 91.2 93.6 71.0-125 2.60 20
1,2-Dichloropropane 0.125 0.121 0.123 96.8 98.4 74.0-125 1.64 20
1,1-Dichloropropene 0.125 0.123 0.126 98.4 101 73.0-125 2.41 20
1,3-Dichloropropane 0.125 0.115 0.119 92.0 95.2 80.0-125 3.42 20
cis-1,3-Dichloropropene 0.125 0.118 0.126 94.4 101 76.0-127 6.56 20
trans-1,3-Dichloropropene 0.125 0.119 0.121 95.2 96.8 73.0-127 1.67 20
2,2-Dichloropropane 0.125 0.153 0.155 122 124 59.0-135 1.30 20
Di-isopropyl ether 0.125 0.132 0.140 106 112 60.0-136 5.88 20
Ethylbenzene 0.125 0.112 0.117 89.6 93.6 74.0-126 4.37 20
Hexachloro-1,3-butadiene 0.125 0.119 0.100 95.2 80.0 57.0-150 17.4 20
Isopropylbenzene 0.125 0.119 0.126 95.2 101 72.0-127 5.71 20
p-Isopropyltoluene 0.125 0.128 0.137 102 110 72.0-133 6.79 20
2-Butanone (MEK)0.625 0.795 0.820 127 131 30.0-160 3.10 24
Methylene Chloride 0.125 0.119 0.123 95.2 98.4 68.0-123 3.31 20
4-Methyl-2-pentanone (MIBK) 0.625 0.689 0.707 110 113 56.0-143 2.58 20
Methyl tert-butyl ether 0.125 0.131 0.142 105 114 66.0-132 8.06 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058136
Volatile Organic Compounds (GC/MS) by Method 8260B L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3924032-1 05/11/23 08:53 • (LCSD) R3924032-2 05/11/23 09:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0788 0.0728 63.0 58.2 59.0-130 J4 7.92 20
n-Propylbenzene 0.125 0.122 0.130 97.6 104 74.0-126 6.35 20
Styrene 0.125 0.101 0.106 80.8 84.8 72.0-127 4.83 20
1,1,1,2-Tetrachloroethane 0.125 0.117 0.120 93.6 96.0 74.0-129 2.53 20
1,1,2,2-Tetrachloroethane 0.125 0.128 0.132 102 106 68.0-128 3.08 20
1,1,2-Trichlorotrifluoroethane 0.125 0.118 0.118 94.4 94.4 61.0-139 0.000 20
Tetrachloroethene 0.125 0.114 0.115 91.2 92.0 70.0-136 0.873 20
Toluene 0.125 0.107 0.111 85.6 88.8 75.0-121 3.67 20
1,2,3-Trichlorobenzene 0.125 0.0830 0.0709 66.4 56.7 59.0-139 J4 15.7 20
1,2,4-Trichlorobenzene 0.125 0.0970 0.0858 77.6 68.6 62.0-137 12.3 20
1,1,1-Trichloroethane 0.125 0.135 0.146 108 117 69.0-126 7.83 20
1,1,2-Trichloroethane 0.125 0.108 0.112 86.4 89.6 78.0-123 3.64 20
Trichloroethene 0.125 0.115 0.119 92.0 95.2 76.0-126 3.42 20
Trichlorofluoromethane 0.125 0.151 0.145 121 116 61.0-142 4.05 20
1,2,3-Trichloropropane 0.125 0.125 0.122 100 97.6 67.0-129 2.43 20
1,2,4-Trimethylbenzene 0.125 0.125 0.132 100 106 70.0-126 5.45 20
1,2,3-Trimethylbenzene 0.125 0.125 0.132 100 106 74.0-124 5.45 20
1,3,5-Trimethylbenzene 0.125 0.125 0.132 100 106 73.0-127 5.45 20
Vinyl chloride 0.125 0.136 0.138 109 110 63.0-134 1.46 20
Xylenes, Total 0.375 0.335 0.342 89.3 91.2 72.0-127 2.07 20
(S) Toluene-d8 99.1 101 75.0-131
(S) 4-Bromofluorobenzene 100 99.3 67.0-138
(S) 1,2-Dichloroethane-d4 125 126 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059338
Semi-Volatile Organic Compounds (GC) by Method 8015 L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924747-1 05/13/23 23:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 40.5 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3924747-2 05/13/23 23:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 31.7 63.4 50.0-150
(S) o-Terphenyl 69.1 18.0-148
L1613819-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613819-01 05/15/23 13:47 • (MS) R3924994-1 05/15/23 14:00 • (MSD) R3924994-2 05/15/23 14:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 50.0 417 268 627 0.000 423 5 50.0-150 V J3 V 80.2 20
(S) o-Terphenyl 58.4 43.2 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057922
Polychlorinated Biphenyls (GC) by Method 8082 L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3925516-1 05/13/23 17:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 113 10.0-135
(S) Tetrachloro-m-xylene 107 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3925516-2 05/13/23 17:17
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.134 80.2 36.0-141
PCB 1260 0.167 0.146 87.4 37.0-145
(S) Decachlorobiphenyl 88.9 10.0-135
(S) Tetrachloro-m-xylene 95.8 10.0-139
L1613023-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613023-21 05/14/23 22:25 • (MS) R3925569-1 05/14/23 22:57 • (MSD) R3925569-2 05/14/23 23:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.174 ND 0.184 0.174 105 100 1 10.0-160 5.25 37
PCB 1260 0.174 ND 0.201 0.210 116 120 1 10.0-160 4.06 38
(S) Decachlorobiphenyl 123 128 10.0-135
(S) Tetrachloro-m-xylene 115 118 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924305-2 05/12/23 14:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924305-2 05/12/23 14:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 64.6 10.0-122
(S) 2-Fluorobiphenyl 60.4 15.0-120
(S) p-Terphenyl-d14 61.3 10.0-120
(S) Phenol-d5 58.7 10.0-120
(S) 2-Fluorophenol 67.9 12.0-120
(S) 2,4,6-Tribromophenol 53.6 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3924305-1 05/12/23 14:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.420 63.1 38.0-120
Acenaphthylene 0.666 0.450 67.6 40.0-120
Anthracene 0.666 0.475 71.3 42.0-120
Benzidine 1.33 0.383 28.8 10.0-120
Benzo(a)anthracene 0.666 0.490 73.6 44.0-120
Benzo(b)fluoranthene 0.666 0.446 67.0 43.0-120
Benzo(k)fluoranthene 0.666 0.427 64.1 44.0-120
Benzo(g,h,i)perylene 0.666 0.465 69.8 43.0-120
Benzo(a)pyrene 0.666 0.504 75.7 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.358 53.8 20.0-120
Bis(2-chloroethyl)ether 0.666 0.414 62.2 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.360 54.1 23.0-120
4-Bromophenyl-phenylether 0.666 0.402 60.4 40.0-120
2-Chloronaphthalene 0.666 0.424 63.7 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3924305-1 05/12/23 14:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.420 63.1 40.0-120
Chrysene 0.666 0.450 67.6 43.0-120
Dibenz(a,h)anthracene 0.666 0.471 70.7 44.0-120
3,3-Dichlorobenzidine 1.33 0.895 67.3 28.0-120
2,4-Dinitrotoluene 0.666 0.509 76.4 45.0-120
2,6-Dinitrotoluene 0.666 0.439 65.9 42.0-120
Fluoranthene 0.666 0.456 68.5 44.0-120
Fluorene 0.666 0.427 64.1 41.0-120
Hexachlorobenzene 0.666 0.390 58.6 39.0-120
Hexachloro-1,3-butadiene 0.666 0.386 58.0 15.0-120
Hexachlorocyclopentadiene 0.666 0.456 68.5 15.0-120
Hexachloroethane 0.666 0.418 62.8 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.445 66.8 45.0-120
Isophorone 0.666 0.375 56.3 23.0-120
Naphthalene 0.666 0.354 53.2 18.0-120
Nitrobenzene 0.666 0.385 57.8 17.0-120
n-Nitrosodimethylamine 0.666 0.452 67.9 10.0-125
n-Nitrosodiphenylamine 0.666 0.445 66.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.400 60.1 26.0-120
Phenanthrene 0.666 0.449 67.4 42.0-120
Benzylbutyl phthalate 0.666 0.528 79.3 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.520 78.1 41.0-120
Di-n-butyl phthalate 0.666 0.522 78.4 43.0-120
Diethyl phthalate 0.666 0.521 78.2 43.0-120
Dimethyl phthalate 0.666 0.477 71.6 43.0-120
Di-n-octyl phthalate 0.666 0.512 76.9 40.0-120
Pyrene 0.666 0.421 63.2 41.0-120
1,2,4-Trichlorobenzene 0.666 0.353 53.0 17.0-120
4-Chloro-3-methylphenol 0.666 0.438 65.8 28.0-120
2-Chlorophenol 0.666 0.409 61.4 28.0-120
2,4-Dichlorophenol 0.666 0.394 59.2 25.0-120
2,4-Dimethylphenol 0.666 0.428 64.3 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.531 79.7 16.0-120
2,4-Dinitrophenol 0.666 0.381 57.2 10.0-120
2-Nitrophenol 0.666 0.411 61.7 20.0-120
4-Nitrophenol 0.666 0.343 51.5 27.0-120
Pentachlorophenol 0.666 0.474 71.2 29.0-120
Phenol 0.666 0.408 61.3 28.0-120
2,4,6-Trichlorophenol 0.666 0.429 64.4 37.0-120
(S) Nitrobenzene-d5 57.1 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3924305-1 05/12/23 14:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 64.3 15.0-120
(S) p-Terphenyl-d14 67.3 10.0-120
(S) Phenol-d5 64.7 10.0-120
(S) 2-Fluorophenol 72.5 12.0-120
(S) 2,4,6-Tribromophenol 62.9 10.0-127
L1613366-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613366-02 05/17/23 11:29 • (MS) R3926121-1 05/17/23 11:49 • (MSD) R3926121-2 05/17/23 12:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.659 ND 0.354 0.391 53.7 58.7 10 18.0-120 9.87 32
Acenaphthylene 0.659 ND ND ND 49.7 50.8 10 25.0-120 3.15 32
Anthracene 0.659 ND 0.375 0.461 56.8 69.2 10 22.0-120 20.6 29
Benzidine 1.32 ND ND ND 74.0 75.9 10 10.0-120 3.27 40
Benzo(a)anthracene 0.659 ND 0.413 0.595 62.6 89.4 10 25.0-120 J3 36.2 29
Benzo(b)fluoranthene 0.659 ND 0.377 0.572 57.2 86.0 10 19.0-122 J3 41.2 31
Benzo(k)fluoranthene 0.659 ND 0.351 0.463 53.2 69.6 10 23.0-120 27.6 30
Benzo(g,h,i)perylene 0.659 ND 0.406 0.478 61.6 71.8 10 10.0-120 16.2 33
Benzo(a)pyrene 0.659 ND 0.380 0.540 57.6 81.1 10 24.0-120 J3 34.7 30
Bis(2-chlorethoxy)methane 0.659 ND ND ND 44.9 52.1 10 10.0-120 15.7 34
Bis(2-chloroethyl)ether 0.659 ND ND ND 41.2 56.6 10 10.0-120 32.4 40
2,2-Oxybis(1-Chloropropane) 0.659 ND ND ND 47.3 50.8 10 10.0-120 8.08 40
4-Bromophenyl-phenylether 0.659 ND ND ND 46.7 50.8 10 27.0-120 9.43 30
2-Chloronaphthalene 0.659 ND ND ND 50.5 50.0 10 20.0-120 0.000 32
4-Chlorophenyl-phenylether 0.659 ND ND ND 51.0 50.5 10 24.0-120 0.000 29
Chrysene 0.659 ND 0.413 0.589 62.6 88.5 10 21.0-120 J3 35.2 29
Dibenz(a,h)anthracene 0.659 ND 0.351 0.405 53.2 60.9 10 10.0-120 14.4 32
3,3-Dichlorobenzidine 1.32 ND ND ND 52.7 54.6 10 10.0-120 4.27 34
2,4-Dinitrotoluene 0.659 ND ND ND 49.5 52.5 10 30.0-120 6.83 31
2,6-Dinitrotoluene 0.659 ND ND ND 48.1 52.4 10 25.0-120 9.46 31
Fluoranthene 0.659 ND 0.395 0.819 59.9 123 10 18.0-126 J3 69.9 32
Fluorene 0.659 ND 0.350 0.390 53.0 58.5 10 25.0-120 10.8 30
Hexachlorobenzene 0.659 ND ND ND 47.6 48.4 10 27.0-120 2.64 28
Hexachloro-1,3-butadiene 0.659 ND ND ND 41.9 42.7 10 10.0-120 3.00 38
Hexachlorocyclopentadiene 0.659 ND ND ND 25.2 2.48 10 10.0-120 J3 J6 164 40
Hexachloroethane 0.659 ND ND ND 40.8 46.1 10 10.0-120 13.1 40
Indeno(1,2,3-cd)pyrene 0.659 ND 0.370 0.481 56.1 72.2 10 10.0-120 26.2 32
Isophorone 0.659 ND ND ND 41.7 44.6 10 13.0-120 7.71 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058400
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1613187-01,02,03,04,05,06
L1613366-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613366-02 05/17/23 11:29 • (MS) R3926121-1 05/17/23 11:49 • (MSD) R3926121-2 05/17/23 12:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.659 ND ND 0.362 49.2 54.4 10 10.0-120 11.0 35
Nitrobenzene 0.659 ND ND ND 46.3 49.1 10 10.0-120 6.64 36
n-Nitrosodimethylamine 0.659 ND ND ND 0.000 0.000 10 10.0-127 J6 J6 0.000 40
n-Nitrosodiphenylamine 0.659 ND ND ND 57.5 55.8 10 17.0-120 1.96 29
n-Nitrosodi-n-propylamine 0.659 ND ND ND 44.1 44.0 10 10.0-120 0.719 37
Phenanthrene 0.659 ND 0.385 0.657 58.4 98.7 10 17.0-120 J3 52.2 31
Benzylbutyl phthalate 0.659 ND ND ND 65.6 67.2 10 23.0-120 3.34 30
Bis(2-ethylhexyl)phthalate 0.659 ND ND ND 68.6 72.4 10 17.0-126 6.29 30
Di-n-butyl phthalate 0.659 ND ND ND 54.9 55.4 10 30.0-120 1.72 29
Diethyl phthalate 0.659 ND ND ND 56.2 55.4 10 26.0-120 0.568 28
Dimethyl phthalate 0.628 ND ND ND 0.000 0.000 10 25.0-120 J6 J6 0.000 29
Di-n-octyl phthalate 0.659 ND ND ND 59.1 54.6 10 21.0-123 6.97 29
Pyrene 0.659 ND 0.425 0.728 64.5 109 10 16.0-121 J3 52.5 32
1,2,4-Trichlorobenzene 0.659 ND ND ND 45.9 45.4 10 12.0-120 0.000 37
4-Chloro-3-methylphenol 0.659 ND ND ND 52.4 56.5 10 15.0-120 8.44 30
2-Chlorophenol 0.659 ND ND ND 43.3 49.1 10 15.0-120 13.4 37
2,4-Dichlorophenol 0.659 ND ND ND 44.9 50.2 10 20.0-120 12.0 31
2,4-Dimethylphenol 0.659 ND ND ND 63.4 59.8 10 10.0-120 4.89 33
4,6-Dinitro-2-methylphenol 0.628 ND ND ND 172 166 10 10.0-120 J5 J5 2.82 39
2,4-Dinitrophenol 0.628 ND ND ND 0.000 0.000 10 10.0-121 J6 J6 0.000 40
2-Nitrophenol 0.659 ND ND ND 54.3 56.5 10 12.0-120 4.86 39
4-Nitrophenol 0.659 ND ND ND 42.8 43.5 10 10.0-137 2.57 32
Pentachlorophenol 0.659 ND ND ND 41.4 45.0 10 10.0-160 9.17 31
Phenol 0.659 ND ND ND 46.0 49.7 10 12.0-120 8.61 38
2,4,6-Trichlorophenol 0.659 ND ND ND 47.0 42.4 10 19.0-120 9.22 32
(S) Nitrobenzene-d5 47.8 50.2 10.0-122
(S) 2-Fluorobiphenyl 50.0 50.8 15.0-120
(S) p-Terphenyl-d14 58.6 59.0 10.0-120
(S) Phenol-d5 48.7 49.7 10.0-120
(S) 2-Fluorophenol 54.0 55.0 12.0-120
(S) 2,4,6-Tribromophenol 47.8 49.5 10.0-127
Sample Narrative:
OS: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058011
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1613187-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924098-2 05/12/23 01:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 105 23.0-120
(S) Nitrobenzene-d5 81.1 14.0-149
(S) 2-Fluorobiphenyl 85.6 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3924098-1 05/12/23 01:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0760 95.0 50.0-126
Acenaphthene 0.0800 0.0663 82.9 50.0-120
Acenaphthylene 0.0800 0.0737 92.1 50.0-120
Benzo(a)anthracene 0.0800 0.0774 96.8 45.0-120
Benzo(a)pyrene 0.0800 0.0714 89.3 42.0-120
Benzo(b)fluoranthene 0.0800 0.0743 92.9 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0692 86.5 45.0-125
Benzo(k)fluoranthene 0.0800 0.0723 90.4 49.0-125
Chrysene 0.0800 0.0832 104 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0731 91.4 47.0-125
Fluoranthene 0.0800 0.0844 105 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2058011
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1613187-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3924098-1 05/12/23 01:19
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0791 98.9 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0812 102 46.0-125
Naphthalene 0.0800 0.0694 86.8 50.0-120
Phenanthrene 0.0800 0.0795 99.4 47.0-120
Pyrene 0.0800 0.0817 102 43.0-123
1-Methylnaphthalene 0.0800 0.0759 94.9 51.0-121
2-Methylnaphthalene 0.0800 0.0715 89.4 50.0-120
2-Chloronaphthalene 0.0800 0.0725 90.6 50.0-120
(S) p-Terphenyl-d14 112 23.0-120
(S) Nitrobenzene-d5 111 14.0-149
(S) 2-Fluorobiphenyl 106 34.0-125
L1613258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613258-01 05/12/23 05:39 • (MS) R3924098-3 05/12/23 05:56 • (MSD) R3924098-4 05/12/23 06:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0760 ND 0.0634 0.0613 83.4 80.2 1 10.0-145 3.37 30
Acenaphthene 0.0760 ND 0.0544 0.0535 71.6 70.0 1 14.0-127 1.67 27
Acenaphthylene 0.0760 ND 0.0595 0.0594 78.3 77.7 1 21.0-124 0.168 25
Benzo(a)anthracene 0.0760 ND 0.0652 0.0613 85.8 80.2 1 10.0-139 6.17 30
Benzo(a)pyrene 0.0760 ND 0.0646 0.0619 85.0 81.0 1 10.0-141 4.27 31
Benzo(b)fluoranthene 0.0760 ND 0.0620 0.0574 81.6 75.1 1 10.0-140 7.71 36
Benzo(g,h,i)perylene 0.0760 ND 0.0576 0.0543 75.8 71.1 1 10.0-140 5.90 33
Benzo(k)fluoranthene 0.0760 ND 0.0601 0.0582 79.1 76.2 1 10.0-137 3.21 31
Chrysene 0.0760 ND 0.0691 0.0692 90.9 90.6 1 10.0-145 0.145 30
Dibenz(a,h)anthracene 0.0760 ND 0.0614 0.0595 80.8 77.9 1 10.0-132 3.14 31
Fluoranthene 0.0760 ND 0.0699 0.0667 92.0 87.3 1 10.0-153 4.69 33
Fluorene 0.0760 ND 0.0671 0.0658 88.3 86.1 1 11.0-130 1.96 29
Indeno(1,2,3-cd)pyrene 0.0760 ND 0.0635 0.0596 83.6 78.0 1 10.0-137 6.34 32
Naphthalene 0.0760 ND 0.0536 0.0554 70.5 72.5 1 10.0-135 3.30 27
Phenanthrene 0.0760 ND 0.0672 0.0652 88.4 85.3 1 10.0-144 3.02 31
Pyrene 0.0760 ND 0.0691 0.0656 90.9 85.9 1 10.0-148 5.20 35
1-Methylnaphthalene 0.0760 ND 0.0597 0.0609 78.6 79.7 1 10.0-142 1.99 28
2-Methylnaphthalene 0.0760 ND 0.0576 0.0584 75.8 76.4 1 10.0-137 1.38 28
2-Chloronaphthalene 0.0760 ND 0.0602 0.0606 79.2 79.3 1 29.0-120 0.662 24
(S) p-Terphenyl-d14 97.0 89.2 23.0-120
(S) Nitrobenzene-d5 96.6 99.4 14.0-149
(S) 2-Fluorobiphenyl 91.9 88.8 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
May 20, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1614172
Samples Received:05/09/2023
Project Number:
Description:
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
May 20, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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May 22, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
CS-1 L1614172-01 6
CS-2 L1614172-02 10
CS-3 L1614172-03 14
CS-4 L1614172-04 18
CS-5 L1614172-05 22
Qc: Quality Control Summary 26
Total Solids by Method 2540 G-2011 26
Wet Chemistry by Method 7199 27
Mercury by Method 7471A 28
Metals (ICP) by Method 6010B 30
Volatile Organic Compounds (GC) by Method 8015D/GRO 32
Volatile Organic Compounds (GC/MS) by Method 8260B 34
Semi-Volatile Organic Compounds (GC) by Method 8015 44
Polychlorinated Biphenyls (GC) by Method 8082 45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 47
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 52
Gl: Glossary of Terms 58
Al: Accreditations & Locations 59
Sc: Sample Chain of Custody 60
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CS-1 L1614172-01 Solid RT 05/08/23 09:30 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 14:44 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:33 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:37 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2062511 25 05/08/23 09:30 05/18/23 18:10 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059471 1 05/08/23 09:30 05/13/23 20:10 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 20:46 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 02:07 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/14/23 00:24 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2062088 1 05/18/23 10:23 05/18/23 17:10 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-2 L1614172-02 Solid RT 05/08/23 09:35 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 14:49 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:35 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:40 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 28 05/08/23 09:35 05/14/23 05:06 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1.12 05/08/23 09:35 05/14/23 11:08 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 23:22 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 03:16 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/14/23 02:33 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059490 1 05/16/23 16:27 05/17/23 06:19 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-3 L1614172-03 Solid RT 05/08/23 09:40 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 14:55 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:37 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:43 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 25 05/08/23 09:40 05/14/23 05:26 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1 05/08/23 09:40 05/14/23 11:27 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 20:59 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 02:17 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/13/23 22:15 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059490 1 05/16/23 16:27 05/17/23 06:37 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-4 L1614172-04 Solid RT 05/08/23 09:45 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 15:00 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057615 1 05/10/23 22:08 05/12/23 11:39 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:46 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 25 05/08/23 09:45 05/14/23 05:47 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1 05/08/23 09:45 05/14/23 11:46 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/18/23 09:47 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059033 1 05/14/23 16:34 05/15/23 02:27 HMH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CS-4 L1614172-04 Solid RT 05/08/23 09:45 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/13/23 22:36 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059490 1 05/16/23 16:27 05/17/23 18:16 CCW Mt. Juliet, TN
Collected by Collected date/time Received date/time
CS-5 L1614172-05 Solid RT 05/08/23 09:50 05/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2057261 1 05/10/23 16:48 05/10/23 17:08 CMK Mt. Juliet, TN
Wet Chemistry by Method 7199 WG2057052 1 05/11/23 08:06 05/13/23 15:05 VSS Mt. Juliet, TN
Mercury by Method 7471A WG2057613 1 05/15/23 11:04 05/18/23 16:56 AKB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2057224 1 05/10/23 23:21 05/11/23 21:49 ABL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2059653 26 05/08/23 09:50 05/14/23 06:07 KSD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2059688 1.04 05/08/23 09:50 05/14/23 12:04 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2061264 1 05/17/23 10:07 05/17/23 22:56 JAS Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2059034 1 05/14/23 16:44 05/15/23 01:50 HMH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2059348 1 05/13/23 15:24 05/14/23 00:45 AGW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2059491 1 05/15/23 09:10 05/15/23 19:10 AMG Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.2 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.30 1 05/13/2023 14:44 WG2057052
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0518 1 05/12/2023 11:33 WG2057615
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.59 1 05/11/2023 21:37 WG2057224
Arsenic 3.22 2.59 1 05/11/2023 21:37 WG2057224
Beryllium 0.334 0.259 1 05/11/2023 21:37 WG2057224
Cadmium ND 0.648 1 05/11/2023 21:37 WG2057224
Chromium 8.47 1.30 1 05/11/2023 21:37 WG2057224
Copper 7.97 2.59 1 05/11/2023 21:37 WG2057224
Lead 3.28 0.648 1 05/11/2023 21:37 WG2057224
Nickel 6.19 2.59 1 05/11/2023 21:37 WG2057224
Selenium ND 2.59 1 05/11/2023 21:37 WG2057224
Silver ND 1.30 1 05/11/2023 21:37 WG2057224
Thallium ND 2.59 1 05/11/2023 21:37 WG2057224
Zinc 24.6 6.48 1 05/11/2023 21:37 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.00 25 05/18/2023 18:10 WG2062511
(S) a,a,a-Trifluorotoluene(FID) 92.8 77.0-120 05/18/2023 18:10 WG2062511
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0799 1 05/13/2023 20:10 WG2059471
Acrylonitrile ND 0.0200 1 05/13/2023 20:10 WG2059471
Benzene ND 0.00160 1 05/13/2023 20:10 WG2059471
Bromobenzene ND 0.0200 1 05/13/2023 20:10 WG2059471
Bromodichloromethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Bromoform ND 0.0400 1 05/13/2023 20:10 WG2059471
Bromomethane ND 0.0200 1 05/13/2023 20:10 WG2059471
n-Butylbenzene ND 0.0200 1 05/13/2023 20:10 WG2059471
sec-Butylbenzene ND 0.0200 1 05/13/2023 20:10 WG2059471
tert-Butylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Carbon tetrachloride ND 0.00799 1 05/13/2023 20:10 WG2059471
Chlorobenzene ND 0.00400 1 05/13/2023 20:10 WG2059471
Chlorodibromomethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Chloroethane ND 0.00799 1 05/13/2023 20:10 WG2059471
Chloroform ND 0.00400 1 05/13/2023 20:10 WG2059471
Chloromethane ND 0.0200 1 05/13/2023 20:10 WG2059471
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00400 1 05/13/2023 20:10 WG2059471
4-Chlorotoluene ND J4 0.00799 1 05/13/2023 20:10 WG2059471
1,2-Dibromo-3-Chloropropane ND 0.0400 1 05/13/2023 20:10 WG2059471
1,2-Dibromoethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Dibromomethane ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2-Dichlorobenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,3-Dichlorobenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,4-Dichlorobenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Dichlorodifluoromethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1-Dichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,2-Dichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1-Dichloroethene ND 0.00400 1 05/13/2023 20:10 WG2059471
cis-1,2-Dichloroethene ND 0.00400 1 05/13/2023 20:10 WG2059471
trans-1,2-Dichloroethene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2-Dichloropropane ND 0.00799 1 05/13/2023 20:10 WG2059471
1,1-Dichloropropene ND 0.00400 1 05/13/2023 20:10 WG2059471
1,3-Dichloropropane ND 0.00799 1 05/13/2023 20:10 WG2059471
cis-1,3-Dichloropropene ND 0.00400 1 05/13/2023 20:10 WG2059471
trans-1,3-Dichloropropene ND 0.00799 1 05/13/2023 20:10 WG2059471
2,2-Dichloropropane ND 0.00400 1 05/13/2023 20:10 WG2059471
Di-isopropyl ether ND 0.00160 1 05/13/2023 20:10 WG2059471
Ethylbenzene ND 0.00400 1 05/13/2023 20:10 WG2059471
Hexachloro-1,3-butadiene ND 0.0400 1 05/13/2023 20:10 WG2059471
Isopropylbenzene ND 0.00400 1 05/13/2023 20:10 WG2059471
p-Isopropyltoluene ND 0.00799 1 05/13/2023 20:10 WG2059471
2-Butanone (MEK)ND 0.160 1 05/13/2023 20:10 WG2059471
Methylene Chloride ND 0.0400 1 05/13/2023 20:10 WG2059471
4-Methyl-2-pentanone (MIBK) ND 0.0400 1 05/13/2023 20:10 WG2059471
Methyl tert-butyl ether ND 0.00160 1 05/13/2023 20:10 WG2059471
Naphthalene ND J3 0.0200 1 05/13/2023 20:10 WG2059471
n-Propylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Styrene ND 0.0200 1 05/13/2023 20:10 WG2059471
1,1,1,2-Tetrachloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1,2,2-Tetrachloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1,2-Trichlorotrifluoroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Tetrachloroethene ND 0.00400 1 05/13/2023 20:10 WG2059471
Toluene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2,3-Trichlorobenzene ND J3 0.0200 1 05/13/2023 20:10 WG2059471
1,2,4-Trichlorobenzene ND J3 0.0200 1 05/13/2023 20:10 WG2059471
1,1,1-Trichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,1,2-Trichloroethane ND 0.00400 1 05/13/2023 20:10 WG2059471
Trichloroethene ND 0.00160 1 05/13/2023 20:10 WG2059471
Trichlorofluoromethane ND 0.00400 1 05/13/2023 20:10 WG2059471
1,2,3-Trichloropropane ND 0.0200 1 05/13/2023 20:10 WG2059471
1,2,4-Trimethylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,2,3-Trimethylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
1,3,5-Trimethylbenzene ND 0.00799 1 05/13/2023 20:10 WG2059471
Vinyl chloride ND 0.00400 1 05/13/2023 20:10 WG2059471
Xylenes, Total ND 0.0104 1 05/13/2023 20:10 WG2059471
(S) Toluene-d8 107 75.0-131 05/13/2023 20:10 WG2059471
(S) 4-Bromofluorobenzene 95.3 67.0-138 05/13/2023 20:10 WG2059471
(S) 1,2-Dichloroethane-d4 96.7 70.0-130 05/13/2023 20:10 WG2059471
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.18 1 05/17/2023 20:46 WG2061264
C28-C40 Oil Range ND 5.18 1 05/17/2023 20:46 WG2061264
(S) o-Terphenyl 33.8 18.0-148 05/17/2023 20:46 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1221 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1232 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1242 ND 0.0440 1 05/15/2023 02:07 WG2059033
PCB 1248 ND 0.0220 1 05/15/2023 02:07 WG2059033
PCB 1254 ND 0.0220 1 05/15/2023 02:07 WG2059033
PCB 1260 ND 0.0220 1 05/15/2023 02:07 WG2059033
(S) Decachlorobiphenyl 70.1 10.0-135 05/15/2023 02:07 WG2059033
(S) Tetrachloro-m-xylene 64.0 10.0-139 05/15/2023 02:07 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Acenaphthylene ND 0.0431 1 05/14/2023 00:24 WG2059348
Anthracene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzidine ND 2.16 1 05/14/2023 00:24 WG2059348
Benzo(a)anthracene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(b)fluoranthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(k)fluoranthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(g,h,i)perylene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzo(a)pyrene ND 0.0431 1 05/14/2023 00:24 WG2059348
Bis(2-chlorethoxy)methane ND 0.431 1 05/14/2023 00:24 WG2059348
Bis(2-chloroethyl)ether ND 0.431 1 05/14/2023 00:24 WG2059348
2,2-Oxybis(1-Chloropropane) ND 0.431 1 05/14/2023 00:24 WG2059348
4-Bromophenyl-phenylether ND 0.431 1 05/14/2023 00:24 WG2059348
2-Chloronaphthalene ND 0.0431 1 05/14/2023 00:24 WG2059348
4-Chlorophenyl-phenylether ND 0.431 1 05/14/2023 00:24 WG2059348
Chrysene ND 0.0431 1 05/14/2023 00:24 WG2059348
Dibenz(a,h)anthracene ND 0.0431 1 05/14/2023 00:24 WG2059348
3,3-Dichlorobenzidine ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dinitrotoluene ND 0.431 1 05/14/2023 00:24 WG2059348
2,6-Dinitrotoluene ND 0.431 1 05/14/2023 00:24 WG2059348
Fluoranthene ND 0.0431 1 05/14/2023 00:24 WG2059348
Fluorene ND 0.0431 1 05/14/2023 00:24 WG2059348
Hexachlorobenzene ND 0.431 1 05/14/2023 00:24 WG2059348
Hexachloro-1,3-butadiene ND 0.431 1 05/14/2023 00:24 WG2059348
Hexachlorocyclopentadiene ND 0.431 1 05/14/2023 00:24 WG2059348
Hexachloroethane ND 0.431 1 05/14/2023 00:24 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0431 1 05/14/2023 00:24 WG2059348
Isophorone ND 0.431 1 05/14/2023 00:24 WG2059348
Naphthalene ND 0.0431 1 05/14/2023 00:24 WG2059348
Nitrobenzene ND 0.431 1 05/14/2023 00:24 WG2059348
n-Nitrosodimethylamine ND 0.431 1 05/14/2023 00:24 WG2059348
n-Nitrosodiphenylamine ND 0.431 1 05/14/2023 00:24 WG2059348
n-Nitrosodi-n-propylamine ND 0.431 1 05/14/2023 00:24 WG2059348
Phenanthrene ND 0.0431 1 05/14/2023 00:24 WG2059348
Benzylbutyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1614172
CS-1
Collected date/time: 05/08/23 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Di-n-butyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Diethyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Dimethyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Di-n-octyl phthalate ND 0.431 1 05/14/2023 00:24 WG2059348
Pyrene ND 0.0431 1 05/14/2023 00:24 WG2059348
1,2,4-Trichlorobenzene ND 0.431 1 05/14/2023 00:24 WG2059348
4-Chloro-3-methylphenol ND 0.431 1 05/14/2023 00:24 WG2059348
2-Chlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dichlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dimethylphenol ND 0.431 1 05/14/2023 00:24 WG2059348
4,6-Dinitro-2-methylphenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4-Dinitrophenol ND 0.431 1 05/14/2023 00:24 WG2059348
2-Nitrophenol ND 0.431 1 05/14/2023 00:24 WG2059348
4-Nitrophenol ND 0.431 1 05/14/2023 00:24 WG2059348
Pentachlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
Phenol ND 0.431 1 05/14/2023 00:24 WG2059348
2,4,6-Trichlorophenol ND 0.431 1 05/14/2023 00:24 WG2059348
(S) Nitrobenzene-d5 42.9 10.0-122 05/14/2023 00:24 WG2059348
(S) 2-Fluorobiphenyl 48.9 15.0-120 05/14/2023 00:24 WG2059348
(S) p-Terphenyl-d14 58.1 10.0-120 05/14/2023 00:24 WG2059348
(S) Phenol-d5 43.8 10.0-120 05/14/2023 00:24 WG2059348
(S) 2-Fluorophenol 49.5 12.0-120 05/14/2023 00:24 WG2059348
(S) 2,4,6-Tribromophenol 55.3 10.0-127 05/14/2023 00:24 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00777 1 05/18/2023 17:10 WG2062088
Acenaphthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Acenaphthylene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(a)anthracene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(a)pyrene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(b)fluoranthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(g,h,i)perylene ND 0.00777 1 05/18/2023 17:10 WG2062088
Benzo(k)fluoranthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Chrysene ND 0.00777 1 05/18/2023 17:10 WG2062088
Dibenz(a,h)anthracene ND 0.00777 1 05/18/2023 17:10 WG2062088
Fluoranthene ND 0.00777 1 05/18/2023 17:10 WG2062088
Fluorene ND 0.00777 1 05/18/2023 17:10 WG2062088
Indeno(1,2,3-cd)pyrene ND 0.00777 1 05/18/2023 17:10 WG2062088
Naphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
Phenanthrene ND 0.00777 1 05/18/2023 17:10 WG2062088
Pyrene ND 0.00777 1 05/18/2023 17:10 WG2062088
1-Methylnaphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
2-Methylnaphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
2-Chloronaphthalene ND 0.0259 1 05/18/2023 17:10 WG2062088
(S) p-Terphenyl-d14 92.6 23.0-120 05/18/2023 17:10 WG2062088
(S) Nitrobenzene-d5 93.8 14.0-149 05/18/2023 17:10 WG2062088
(S) 2-Fluorobiphenyl 91.8 34.0-125 05/18/2023 17:10 WG2062088
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.0 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.22 1 05/13/2023 14:49 WG2057052
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0488 1 05/12/2023 11:35 WG2057615
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.44 1 05/11/2023 21:40 WG2057224
Arsenic 3.37 2.44 1 05/11/2023 21:40 WG2057224
Beryllium 0.266 0.244 1 05/11/2023 21:40 WG2057224
Cadmium ND 0.610 1 05/11/2023 21:40 WG2057224
Chromium 14.6 1.22 1 05/11/2023 21:40 WG2057224
Copper 13.9 2.44 1 05/11/2023 21:40 WG2057224
Lead 4.12 0.610 1 05/11/2023 21:40 WG2057224
Nickel 7.79 2.44 1 05/11/2023 21:40 WG2057224
Selenium ND 2.44 1 05/11/2023 21:40 WG2057224
Silver ND 1.22 1 05/11/2023 21:40 WG2057224
Thallium ND 2.44 1 05/11/2023 21:40 WG2057224
Zinc 22.6 6.10 1 05/11/2023 21:40 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.96 28 05/14/2023 05:06 WG2059653
(S) a,a,a-Trifluorotoluene(FID) 93.6 77.0-120 05/14/2023 05:06 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0793 1.12 05/14/2023 11:08 WG2059688
Acrylonitrile ND 0.0198 1.12 05/14/2023 11:08 WG2059688
Benzene ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Bromobenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
Bromodichloromethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Bromoform ND 0.0396 1.12 05/14/2023 11:08 WG2059688
Bromomethane ND 0.0198 1.12 05/14/2023 11:08 WG2059688
n-Butylbenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
sec-Butylbenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
tert-Butylbenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Carbon tetrachloride ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Chlorobenzene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Chlorodibromomethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Chloroethane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Chloroform ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Chloromethane ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
4-Chlorotoluene ND J4 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0396 1.12 05/14/2023 11:08 WG2059688
1,2-Dibromoethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Dibromomethane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2-Dichlorobenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,3-Dichlorobenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,4-Dichlorobenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Dichlorodifluoromethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1-Dichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,2-Dichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1-Dichloroethene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
cis-1,2-Dichloroethene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
trans-1,2-Dichloroethene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2-Dichloropropane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,1-Dichloropropene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,3-Dichloropropane ND 0.00793 1.12 05/14/2023 11:08 WG2059688
cis-1,3-Dichloropropene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
trans-1,3-Dichloropropene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
2,2-Dichloropropane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Di-isopropyl ether ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Ethylbenzene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Hexachloro-1,3-butadiene ND 0.0396 1.12 05/14/2023 11:08 WG2059688
Isopropylbenzene ND 0.00396 1.12 05/14/2023 11:08 WG2059688
p-Isopropyltoluene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
2-Butanone (MEK)ND 0.159 1.12 05/14/2023 11:08 WG2059688
Methylene Chloride ND 0.0396 1.12 05/14/2023 11:08 WG2059688
4-Methyl-2-pentanone (MIBK) ND 0.0396 1.12 05/14/2023 11:08 WG2059688
Methyl tert-butyl ether ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Naphthalene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
n-Propylbenzene ND J4 0.00793 1.12 05/14/2023 11:08 WG2059688
Styrene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Tetrachloroethene 0.00883 0.00396 1.12 05/14/2023 11:08 WG2059688
Toluene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2,3-Trichlorobenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,2,4-Trichlorobenzene ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,1,1-Trichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
1,1,2-Trichloroethane ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Trichloroethene ND 0.00159 1.12 05/14/2023 11:08 WG2059688
Trichlorofluoromethane ND J4 0.00396 1.12 05/14/2023 11:08 WG2059688
1,2,3-Trichloropropane ND 0.0198 1.12 05/14/2023 11:08 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00793 1.12 05/14/2023 11:08 WG2059688
1,2,3-Trimethylbenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
1,3,5-Trimethylbenzene ND 0.00793 1.12 05/14/2023 11:08 WG2059688
Vinyl chloride ND 0.00396 1.12 05/14/2023 11:08 WG2059688
Xylenes, Total ND 0.0103 1.12 05/14/2023 11:08 WG2059688
(S) Toluene-d8 107 75.0-131 05/14/2023 11:08 WG2059688
(S) 4-Bromofluorobenzene 102 67.0-138 05/14/2023 11:08 WG2059688
(S) 1,2-Dichloroethane-d4 101 70.0-130 05/14/2023 11:08 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 16.0 4.88 1 05/17/2023 23:22 WG2061264
C28-C40 Oil Range 41.5 4.88 1 05/17/2023 23:22 WG2061264
(S) o-Terphenyl 39.5 18.0-148 05/17/2023 23:22 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1221 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1232 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1242 ND 0.0415 1 05/15/2023 03:16 WG2059033
PCB 1248 ND 0.0207 1 05/15/2023 03:16 WG2059033
PCB 1254 ND 0.0207 1 05/15/2023 03:16 WG2059033
PCB 1260 ND 0.0207 1 05/15/2023 03:16 WG2059033
(S) Decachlorobiphenyl 57.0 10.0-135 05/15/2023 03:16 WG2059033
(S) Tetrachloro-m-xylene 51.9 10.0-139 05/15/2023 03:16 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Acenaphthylene ND 0.0406 1 05/14/2023 02:33 WG2059348
Anthracene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzidine ND 2.04 1 05/14/2023 02:33 WG2059348
Benzo(a)anthracene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(b)fluoranthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(k)fluoranthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(g,h,i)perylene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzo(a)pyrene ND 0.0406 1 05/14/2023 02:33 WG2059348
Bis(2-chlorethoxy)methane ND 0.406 1 05/14/2023 02:33 WG2059348
Bis(2-chloroethyl)ether ND 0.406 1 05/14/2023 02:33 WG2059348
2,2-Oxybis(1-Chloropropane) ND 0.406 1 05/14/2023 02:33 WG2059348
4-Bromophenyl-phenylether ND 0.406 1 05/14/2023 02:33 WG2059348
2-Chloronaphthalene ND 0.0406 1 05/14/2023 02:33 WG2059348
4-Chlorophenyl-phenylether ND 0.406 1 05/14/2023 02:33 WG2059348
Chrysene ND 0.0406 1 05/14/2023 02:33 WG2059348
Dibenz(a,h)anthracene ND 0.0406 1 05/14/2023 02:33 WG2059348
3,3-Dichlorobenzidine ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dinitrotoluene ND 0.406 1 05/14/2023 02:33 WG2059348
2,6-Dinitrotoluene ND 0.406 1 05/14/2023 02:33 WG2059348
Fluoranthene ND 0.0406 1 05/14/2023 02:33 WG2059348
Fluorene ND 0.0406 1 05/14/2023 02:33 WG2059348
Hexachlorobenzene ND 0.406 1 05/14/2023 02:33 WG2059348
Hexachloro-1,3-butadiene ND 0.406 1 05/14/2023 02:33 WG2059348
Hexachlorocyclopentadiene ND 0.406 1 05/14/2023 02:33 WG2059348
Hexachloroethane ND 0.406 1 05/14/2023 02:33 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0406 1 05/14/2023 02:33 WG2059348
Isophorone ND 0.406 1 05/14/2023 02:33 WG2059348
Naphthalene ND 0.0406 1 05/14/2023 02:33 WG2059348
Nitrobenzene ND 0.406 1 05/14/2023 02:33 WG2059348
n-Nitrosodimethylamine ND 0.406 1 05/14/2023 02:33 WG2059348
n-Nitrosodiphenylamine ND 0.406 1 05/14/2023 02:33 WG2059348
n-Nitrosodi-n-propylamine ND 0.406 1 05/14/2023 02:33 WG2059348
Phenanthrene ND 0.0406 1 05/14/2023 02:33 WG2059348
Benzylbutyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1614172
CS-2
Collected date/time: 05/08/23 09:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Di-n-butyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Diethyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Dimethyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Di-n-octyl phthalate ND 0.406 1 05/14/2023 02:33 WG2059348
Pyrene ND 0.0406 1 05/14/2023 02:33 WG2059348
1,2,4-Trichlorobenzene ND 0.406 1 05/14/2023 02:33 WG2059348
4-Chloro-3-methylphenol ND 0.406 1 05/14/2023 02:33 WG2059348
2-Chlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dichlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dimethylphenol ND 0.406 1 05/14/2023 02:33 WG2059348
4,6-Dinitro-2-methylphenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4-Dinitrophenol ND 0.406 1 05/14/2023 02:33 WG2059348
2-Nitrophenol ND 0.406 1 05/14/2023 02:33 WG2059348
4-Nitrophenol ND 0.406 1 05/14/2023 02:33 WG2059348
Pentachlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
Phenol ND 0.406 1 05/14/2023 02:33 WG2059348
2,4,6-Trichlorophenol ND 0.406 1 05/14/2023 02:33 WG2059348
(S) Nitrobenzene-d5 38.8 10.0-122 05/14/2023 02:33 WG2059348
(S) 2-Fluorobiphenyl 40.1 15.0-120 05/14/2023 02:33 WG2059348
(S) p-Terphenyl-d14 45.6 10.0-120 05/14/2023 02:33 WG2059348
(S) Phenol-d5 42.4 10.0-120 05/14/2023 02:33 WG2059348
(S) 2-Fluorophenol 46.0 12.0-120 05/14/2023 02:33 WG2059348
(S) 2,4,6-Tribromophenol 56.0 10.0-127 05/14/2023 02:33 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00732 1 05/17/2023 06:19 WG2059490
Acenaphthene ND 0.00732 1 05/17/2023 06:19 WG2059490
Acenaphthylene ND 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(a)anthracene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(a)pyrene ND 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(b)fluoranthene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(g,h,i)perylene ND 0.00732 1 05/17/2023 06:19 WG2059490
Benzo(k)fluoranthene ND 0.00732 1 05/17/2023 06:19 WG2059490
Chrysene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Dibenz(a,h)anthracene ND 0.00732 1 05/17/2023 06:19 WG2059490
Fluoranthene ND 0.00732 1 05/17/2023 06:19 WG2059490
Fluorene ND 0.00732 1 05/17/2023 06:19 WG2059490
Indeno(1,2,3-cd)pyrene ND J4 0.00732 1 05/17/2023 06:19 WG2059490
Naphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
Phenanthrene ND 0.00732 1 05/17/2023 06:19 WG2059490
Pyrene ND 0.00732 1 05/17/2023 06:19 WG2059490
1-Methylnaphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
2-Methylnaphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
2-Chloronaphthalene ND 0.0244 1 05/17/2023 06:19 WG2059490
(S) p-Terphenyl-d14 105 23.0-120 05/17/2023 06:19 WG2059490
(S) Nitrobenzene-d5 68.7 14.0-149 05/17/2023 06:19 WG2059490
(S) 2-Fluorobiphenyl 72.7 34.0-125 05/17/2023 06:19 WG2059490
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 69.8 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.43 1 05/13/2023 14:55 WG2057052
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0573 1 05/12/2023 11:37 WG2057615
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.87 1 05/11/2023 21:43 WG2057224
Arsenic 5.44 2.87 1 05/11/2023 21:43 WG2057224
Beryllium 0.380 0.287 1 05/11/2023 21:43 WG2057224
Cadmium ND 0.717 1 05/11/2023 21:43 WG2057224
Chromium 9.56 1.43 1 05/11/2023 21:43 WG2057224
Copper 9.51 2.87 1 05/11/2023 21:43 WG2057224
Lead 4.07 0.717 1 05/11/2023 21:43 WG2057224
Nickel 6.94 2.87 1 05/11/2023 21:43 WG2057224
Selenium ND 2.87 1 05/11/2023 21:43 WG2057224
Silver ND 1.43 1 05/11/2023 21:43 WG2057224
Thallium ND 2.87 1 05/11/2023 21:43 WG2057224
Zinc 28.5 7.17 1 05/11/2023 21:43 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.78 25 05/14/2023 05:26 WG2059653
(S) a,a,a-Trifluorotoluene(FID) 93.6 77.0-120 05/14/2023 05:26 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0957 1 05/14/2023 11:27 WG2059688
Acrylonitrile ND 0.0239 1 05/14/2023 11:27 WG2059688
Benzene ND 0.00191 1 05/14/2023 11:27 WG2059688
Bromobenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
Bromodichloromethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Bromoform ND 0.0478 1 05/14/2023 11:27 WG2059688
Bromomethane ND 0.0239 1 05/14/2023 11:27 WG2059688
n-Butylbenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
sec-Butylbenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
tert-Butylbenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
Carbon tetrachloride ND 0.00957 1 05/14/2023 11:27 WG2059688
Chlorobenzene ND 0.00478 1 05/14/2023 11:27 WG2059688
Chlorodibromomethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Chloroethane ND 0.00957 1 05/14/2023 11:27 WG2059688
Chloroform ND 0.00478 1 05/14/2023 11:27 WG2059688
Chloromethane ND 0.0239 1 05/14/2023 11:27 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00478 1 05/14/2023 11:27 WG2059688
4-Chlorotoluene ND J4 0.00957 1 05/14/2023 11:27 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0478 1 05/14/2023 11:27 WG2059688
1,2-Dibromoethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Dibromomethane ND 0.00957 1 05/14/2023 11:27 WG2059688
1,2-Dichlorobenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,3-Dichlorobenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,4-Dichlorobenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
Dichlorodifluoromethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1-Dichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,2-Dichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1-Dichloroethene ND 0.00478 1 05/14/2023 11:27 WG2059688
cis-1,2-Dichloroethene ND 0.00478 1 05/14/2023 11:27 WG2059688
trans-1,2-Dichloroethene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,2-Dichloropropane ND 0.00957 1 05/14/2023 11:27 WG2059688
1,1-Dichloropropene ND 0.00478 1 05/14/2023 11:27 WG2059688
1,3-Dichloropropane ND 0.00957 1 05/14/2023 11:27 WG2059688
cis-1,3-Dichloropropene ND 0.00478 1 05/14/2023 11:27 WG2059688
trans-1,3-Dichloropropene ND 0.00957 1 05/14/2023 11:27 WG2059688
2,2-Dichloropropane ND 0.00478 1 05/14/2023 11:27 WG2059688
Di-isopropyl ether ND 0.00191 1 05/14/2023 11:27 WG2059688
Ethylbenzene ND 0.00478 1 05/14/2023 11:27 WG2059688
Hexachloro-1,3-butadiene ND 0.0478 1 05/14/2023 11:27 WG2059688
Isopropylbenzene ND 0.00478 1 05/14/2023 11:27 WG2059688
p-Isopropyltoluene ND 0.00957 1 05/14/2023 11:27 WG2059688
2-Butanone (MEK)ND 0.191 1 05/14/2023 11:27 WG2059688
Methylene Chloride ND 0.0478 1 05/14/2023 11:27 WG2059688
4-Methyl-2-pentanone (MIBK) ND 0.0478 1 05/14/2023 11:27 WG2059688
Methyl tert-butyl ether ND 0.00191 1 05/14/2023 11:27 WG2059688
Naphthalene ND 0.0239 1 05/14/2023 11:27 WG2059688
n-Propylbenzene ND J4 0.00957 1 05/14/2023 11:27 WG2059688
Styrene ND 0.0239 1 05/14/2023 11:27 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Tetrachloroethene ND 0.00478 1 05/14/2023 11:27 WG2059688
Toluene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,2,3-Trichlorobenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
1,2,4-Trichlorobenzene ND 0.0239 1 05/14/2023 11:27 WG2059688
1,1,1-Trichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
1,1,2-Trichloroethane ND 0.00478 1 05/14/2023 11:27 WG2059688
Trichloroethene ND 0.00191 1 05/14/2023 11:27 WG2059688
Trichlorofluoromethane ND J4 0.00478 1 05/14/2023 11:27 WG2059688
1,2,3-Trichloropropane ND 0.0239 1 05/14/2023 11:27 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00957 1 05/14/2023 11:27 WG2059688
1,2,3-Trimethylbenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
1,3,5-Trimethylbenzene ND 0.00957 1 05/14/2023 11:27 WG2059688
Vinyl chloride ND 0.00478 1 05/14/2023 11:27 WG2059688
Xylenes, Total ND 0.0124 1 05/14/2023 11:27 WG2059688
(S) Toluene-d8 108 75.0-131 05/14/2023 11:27 WG2059688
(S) 4-Bromofluorobenzene 98.3 67.0-138 05/14/2023 11:27 WG2059688
(S) 1,2-Dichloroethane-d4 91.8 70.0-130 05/14/2023 11:27 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.73 1 05/17/2023 20:59 WG2061264
C28-C40 Oil Range ND 5.73 1 05/17/2023 20:59 WG2061264
(S) o-Terphenyl 47.6 18.0-148 05/17/2023 20:59 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1221 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1232 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1242 ND 0.0487 1 05/15/2023 02:17 WG2059033
PCB 1248 ND 0.0244 1 05/15/2023 02:17 WG2059033
PCB 1254 ND 0.0244 1 05/15/2023 02:17 WG2059033
PCB 1260 ND 0.0244 1 05/15/2023 02:17 WG2059033
(S) Decachlorobiphenyl 72.4 10.0-135 05/15/2023 02:17 WG2059033
(S) Tetrachloro-m-xylene 65.2 10.0-139 05/15/2023 02:17 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Acenaphthylene ND 0.0477 1 05/13/2023 22:15 WG2059348
Anthracene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzidine ND 2.39 1 05/13/2023 22:15 WG2059348
Benzo(a)anthracene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(b)fluoranthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(k)fluoranthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(g,h,i)perylene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzo(a)pyrene ND 0.0477 1 05/13/2023 22:15 WG2059348
Bis(2-chlorethoxy)methane ND 0.477 1 05/13/2023 22:15 WG2059348
Bis(2-chloroethyl)ether ND 0.477 1 05/13/2023 22:15 WG2059348
2,2-Oxybis(1-Chloropropane) ND 0.477 1 05/13/2023 22:15 WG2059348
4-Bromophenyl-phenylether ND 0.477 1 05/13/2023 22:15 WG2059348
2-Chloronaphthalene ND 0.0477 1 05/13/2023 22:15 WG2059348
4-Chlorophenyl-phenylether ND 0.477 1 05/13/2023 22:15 WG2059348
Chrysene ND 0.0477 1 05/13/2023 22:15 WG2059348
Dibenz(a,h)anthracene ND 0.0477 1 05/13/2023 22:15 WG2059348
3,3-Dichlorobenzidine ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dinitrotoluene ND 0.477 1 05/13/2023 22:15 WG2059348
2,6-Dinitrotoluene ND 0.477 1 05/13/2023 22:15 WG2059348
Fluoranthene ND 0.0477 1 05/13/2023 22:15 WG2059348
Fluorene ND 0.0477 1 05/13/2023 22:15 WG2059348
Hexachlorobenzene ND 0.477 1 05/13/2023 22:15 WG2059348
Hexachloro-1,3-butadiene ND 0.477 1 05/13/2023 22:15 WG2059348
Hexachlorocyclopentadiene ND 0.477 1 05/13/2023 22:15 WG2059348
Hexachloroethane ND 0.477 1 05/13/2023 22:15 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0477 1 05/13/2023 22:15 WG2059348
Isophorone ND 0.477 1 05/13/2023 22:15 WG2059348
Naphthalene ND 0.0477 1 05/13/2023 22:15 WG2059348
Nitrobenzene ND 0.477 1 05/13/2023 22:15 WG2059348
n-Nitrosodimethylamine ND 0.477 1 05/13/2023 22:15 WG2059348
n-Nitrosodiphenylamine ND 0.477 1 05/13/2023 22:15 WG2059348
n-Nitrosodi-n-propylamine ND 0.477 1 05/13/2023 22:15 WG2059348
Phenanthrene ND 0.0477 1 05/13/2023 22:15 WG2059348
Benzylbutyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1614172
CS-3
Collected date/time: 05/08/23 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Di-n-butyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Diethyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Dimethyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Di-n-octyl phthalate ND 0.477 1 05/13/2023 22:15 WG2059348
Pyrene ND 0.0477 1 05/13/2023 22:15 WG2059348
1,2,4-Trichlorobenzene ND 0.477 1 05/13/2023 22:15 WG2059348
4-Chloro-3-methylphenol ND 0.477 1 05/13/2023 22:15 WG2059348
2-Chlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dichlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dimethylphenol ND 0.477 1 05/13/2023 22:15 WG2059348
4,6-Dinitro-2-methylphenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4-Dinitrophenol ND 0.477 1 05/13/2023 22:15 WG2059348
2-Nitrophenol ND 0.477 1 05/13/2023 22:15 WG2059348
4-Nitrophenol ND 0.477 1 05/13/2023 22:15 WG2059348
Pentachlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
Phenol ND 0.477 1 05/13/2023 22:15 WG2059348
2,4,6-Trichlorophenol ND 0.477 1 05/13/2023 22:15 WG2059348
(S) Nitrobenzene-d5 37.9 10.0-122 05/13/2023 22:15 WG2059348
(S) 2-Fluorobiphenyl 44.8 15.0-120 05/13/2023 22:15 WG2059348
(S) p-Terphenyl-d14 53.9 10.0-120 05/13/2023 22:15 WG2059348
(S) Phenol-d5 38.6 10.0-120 05/13/2023 22:15 WG2059348
(S) 2-Fluorophenol 45.9 12.0-120 05/13/2023 22:15 WG2059348
(S) 2,4,6-Tribromophenol 47.9 10.0-127 05/13/2023 22:15 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00860 1 05/17/2023 06:37 WG2059490
Acenaphthene ND 0.00860 1 05/17/2023 06:37 WG2059490
Acenaphthylene ND 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(a)anthracene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(a)pyrene ND 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(b)fluoranthene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(g,h,i)perylene ND 0.00860 1 05/17/2023 06:37 WG2059490
Benzo(k)fluoranthene ND 0.00860 1 05/17/2023 06:37 WG2059490
Chrysene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Dibenz(a,h)anthracene ND 0.00860 1 05/17/2023 06:37 WG2059490
Fluoranthene ND 0.00860 1 05/17/2023 06:37 WG2059490
Fluorene ND 0.00860 1 05/17/2023 06:37 WG2059490
Indeno(1,2,3-cd)pyrene ND J4 0.00860 1 05/17/2023 06:37 WG2059490
Naphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
Phenanthrene ND 0.00860 1 05/17/2023 06:37 WG2059490
Pyrene ND 0.00860 1 05/17/2023 06:37 WG2059490
1-Methylnaphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
2-Methylnaphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
2-Chloronaphthalene ND 0.0287 1 05/17/2023 06:37 WG2059490
(S) p-Terphenyl-d14 98.5 23.0-120 05/17/2023 06:37 WG2059490
(S) Nitrobenzene-d5 46.7 14.0-149 05/17/2023 06:37 WG2059490
(S) 2-Fluorobiphenyl 55.7 34.0-125 05/17/2023 06:37 WG2059490
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.3 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.33 1 05/13/2023 15:00 WG2057052
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0531 1 05/12/2023 11:39 WG2057615
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.66 1 05/11/2023 21:46 WG2057224
Arsenic 10.1 2.66 1 05/11/2023 21:46 WG2057224
Beryllium 0.311 0.266 1 05/11/2023 21:46 WG2057224
Cadmium ND 0.664 1 05/11/2023 21:46 WG2057224
Chromium 7.57 1.33 1 05/11/2023 21:46 WG2057224
Copper 16.1 2.66 1 05/11/2023 21:46 WG2057224
Lead 25.6 0.664 1 05/11/2023 21:46 WG2057224
Nickel 5.63 2.66 1 05/11/2023 21:46 WG2057224
Selenium ND 2.66 1 05/11/2023 21:46 WG2057224
Silver ND 1.33 1 05/11/2023 21:46 WG2057224
Thallium ND 2.66 1 05/11/2023 21:46 WG2057224
Zinc 44.0 6.64 1 05/11/2023 21:46 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.22 25 05/14/2023 05:47 WG2059653
(S) a,a,a-Trifluorotoluene(FID) 94.9 77.0-120 05/14/2023 05:47 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0889 0.0844 1 05/14/2023 11:46 WG2059688
Acrylonitrile ND 0.0211 1 05/14/2023 11:46 WG2059688
Benzene ND 0.00169 1 05/14/2023 11:46 WG2059688
Bromobenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
Bromodichloromethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Bromoform ND 0.0422 1 05/14/2023 11:46 WG2059688
Bromomethane ND 0.0211 1 05/14/2023 11:46 WG2059688
n-Butylbenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
sec-Butylbenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
tert-Butylbenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
Carbon tetrachloride ND 0.00844 1 05/14/2023 11:46 WG2059688
Chlorobenzene ND 0.00422 1 05/14/2023 11:46 WG2059688
Chlorodibromomethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Chloroethane ND 0.00844 1 05/14/2023 11:46 WG2059688
Chloroform ND 0.00422 1 05/14/2023 11:46 WG2059688
Chloromethane ND 0.0211 1 05/14/2023 11:46 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00422 1 05/14/2023 11:46 WG2059688
4-Chlorotoluene ND J4 0.00844 1 05/14/2023 11:46 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0422 1 05/14/2023 11:46 WG2059688
1,2-Dibromoethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Dibromomethane ND 0.00844 1 05/14/2023 11:46 WG2059688
1,2-Dichlorobenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,3-Dichlorobenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,4-Dichlorobenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
Dichlorodifluoromethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1-Dichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,2-Dichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1-Dichloroethene ND 0.00422 1 05/14/2023 11:46 WG2059688
cis-1,2-Dichloroethene ND 0.00422 1 05/14/2023 11:46 WG2059688
trans-1,2-Dichloroethene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,2-Dichloropropane ND 0.00844 1 05/14/2023 11:46 WG2059688
1,1-Dichloropropene ND 0.00422 1 05/14/2023 11:46 WG2059688
1,3-Dichloropropane ND 0.00844 1 05/14/2023 11:46 WG2059688
cis-1,3-Dichloropropene ND 0.00422 1 05/14/2023 11:46 WG2059688
trans-1,3-Dichloropropene ND 0.00844 1 05/14/2023 11:46 WG2059688
2,2-Dichloropropane ND 0.00422 1 05/14/2023 11:46 WG2059688
Di-isopropyl ether ND 0.00169 1 05/14/2023 11:46 WG2059688
Ethylbenzene ND 0.00422 1 05/14/2023 11:46 WG2059688
Hexachloro-1,3-butadiene ND 0.0422 1 05/14/2023 11:46 WG2059688
Isopropylbenzene ND 0.00422 1 05/14/2023 11:46 WG2059688
p-Isopropyltoluene ND 0.00844 1 05/14/2023 11:46 WG2059688
2-Butanone (MEK)ND 0.169 1 05/14/2023 11:46 WG2059688
Methylene Chloride ND 0.0422 1 05/14/2023 11:46 WG2059688
4-Methyl-2-pentanone (MIBK) ND 0.0422 1 05/14/2023 11:46 WG2059688
Methyl tert-butyl ether ND 0.00169 1 05/14/2023 11:46 WG2059688
Naphthalene ND 0.0211 1 05/14/2023 11:46 WG2059688
n-Propylbenzene ND J4 0.00844 1 05/14/2023 11:46 WG2059688
Styrene ND 0.0211 1 05/14/2023 11:46 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Tetrachloroethene ND 0.00422 1 05/14/2023 11:46 WG2059688
Toluene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,2,3-Trichlorobenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
1,2,4-Trichlorobenzene ND 0.0211 1 05/14/2023 11:46 WG2059688
1,1,1-Trichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
1,1,2-Trichloroethane ND 0.00422 1 05/14/2023 11:46 WG2059688
Trichloroethene ND 0.00169 1 05/14/2023 11:46 WG2059688
Trichlorofluoromethane ND J4 0.00422 1 05/14/2023 11:46 WG2059688
1,2,3-Trichloropropane ND 0.0211 1 05/14/2023 11:46 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00844 1 05/14/2023 11:46 WG2059688
1,2,3-Trimethylbenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
1,3,5-Trimethylbenzene ND 0.00844 1 05/14/2023 11:46 WG2059688
Vinyl chloride ND 0.00422 1 05/14/2023 11:46 WG2059688
Xylenes, Total ND 0.0110 1 05/14/2023 11:46 WG2059688
(S) Toluene-d8 107 75.0-131 05/14/2023 11:46 WG2059688
(S) 4-Bromofluorobenzene 95.1 67.0-138 05/14/2023 11:46 WG2059688
(S) 1,2-Dichloroethane-d4 95.9 70.0-130 05/14/2023 11:46 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 5.31 1 05/18/2023 09:47 WG2061264
C28-C40 Oil Range 13.6 5.31 1 05/18/2023 09:47 WG2061264
(S) o-Terphenyl 69.8 18.0-148 05/18/2023 09:47 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1221 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1232 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1242 ND 0.0452 1 05/15/2023 02:27 WG2059033
PCB 1248 ND 0.0226 1 05/15/2023 02:27 WG2059033
PCB 1254 ND 0.0226 1 05/15/2023 02:27 WG2059033
PCB 1260 ND 0.0226 1 05/15/2023 02:27 WG2059033
(S) Decachlorobiphenyl 69.1 10.0-135 05/15/2023 02:27 WG2059033
(S) Tetrachloro-m-xylene 61.8 10.0-139 05/15/2023 02:27 WG2059033
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Acenaphthylene ND 0.0442 1 05/13/2023 22:36 WG2059348
Anthracene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzidine ND 2.22 1 05/13/2023 22:36 WG2059348
Benzo(a)anthracene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(b)fluoranthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(k)fluoranthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(g,h,i)perylene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzo(a)pyrene ND 0.0442 1 05/13/2023 22:36 WG2059348
Bis(2-chlorethoxy)methane ND 0.442 1 05/13/2023 22:36 WG2059348
Bis(2-chloroethyl)ether ND 0.442 1 05/13/2023 22:36 WG2059348
2,2-Oxybis(1-Chloropropane) ND 0.442 1 05/13/2023 22:36 WG2059348
4-Bromophenyl-phenylether ND 0.442 1 05/13/2023 22:36 WG2059348
2-Chloronaphthalene ND 0.0442 1 05/13/2023 22:36 WG2059348
4-Chlorophenyl-phenylether ND 0.442 1 05/13/2023 22:36 WG2059348
Chrysene ND 0.0442 1 05/13/2023 22:36 WG2059348
Dibenz(a,h)anthracene ND 0.0442 1 05/13/2023 22:36 WG2059348
3,3-Dichlorobenzidine ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dinitrotoluene ND 0.442 1 05/13/2023 22:36 WG2059348
2,6-Dinitrotoluene ND 0.442 1 05/13/2023 22:36 WG2059348
Fluoranthene ND 0.0442 1 05/13/2023 22:36 WG2059348
Fluorene ND 0.0442 1 05/13/2023 22:36 WG2059348
Hexachlorobenzene ND 0.442 1 05/13/2023 22:36 WG2059348
Hexachloro-1,3-butadiene ND 0.442 1 05/13/2023 22:36 WG2059348
Hexachlorocyclopentadiene ND 0.442 1 05/13/2023 22:36 WG2059348
Hexachloroethane ND 0.442 1 05/13/2023 22:36 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0442 1 05/13/2023 22:36 WG2059348
Isophorone ND 0.442 1 05/13/2023 22:36 WG2059348
Naphthalene ND 0.0442 1 05/13/2023 22:36 WG2059348
Nitrobenzene ND 0.442 1 05/13/2023 22:36 WG2059348
n-Nitrosodimethylamine ND 0.442 1 05/13/2023 22:36 WG2059348
n-Nitrosodiphenylamine ND 0.442 1 05/13/2023 22:36 WG2059348
n-Nitrosodi-n-propylamine ND 0.442 1 05/13/2023 22:36 WG2059348
Phenanthrene ND 0.0442 1 05/13/2023 22:36 WG2059348
Benzylbutyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1614172
CS-4
Collected date/time: 05/08/23 09:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Di-n-butyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Diethyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Dimethyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Di-n-octyl phthalate ND 0.442 1 05/13/2023 22:36 WG2059348
Pyrene ND 0.0442 1 05/13/2023 22:36 WG2059348
1,2,4-Trichlorobenzene ND 0.442 1 05/13/2023 22:36 WG2059348
4-Chloro-3-methylphenol ND 0.442 1 05/13/2023 22:36 WG2059348
2-Chlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dichlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dimethylphenol ND 0.442 1 05/13/2023 22:36 WG2059348
4,6-Dinitro-2-methylphenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4-Dinitrophenol ND 0.442 1 05/13/2023 22:36 WG2059348
2-Nitrophenol ND 0.442 1 05/13/2023 22:36 WG2059348
4-Nitrophenol ND 0.442 1 05/13/2023 22:36 WG2059348
Pentachlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
Phenol ND 0.442 1 05/13/2023 22:36 WG2059348
2,4,6-Trichlorophenol ND 0.442 1 05/13/2023 22:36 WG2059348
(S) Nitrobenzene-d5 36.8 10.0-122 05/13/2023 22:36 WG2059348
(S) 2-Fluorobiphenyl 43.2 15.0-120 05/13/2023 22:36 WG2059348
(S) p-Terphenyl-d14 55.3 10.0-120 05/13/2023 22:36 WG2059348
(S) Phenol-d5 38.9 10.0-120 05/13/2023 22:36 WG2059348
(S) 2-Fluorophenol 46.8 12.0-120 05/13/2023 22:36 WG2059348
(S) 2,4,6-Tribromophenol 52.6 10.0-127 05/13/2023 22:36 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00797 1 05/17/2023 18:16 WG2059490
Acenaphthene ND 0.00797 1 05/17/2023 18:16 WG2059490
Acenaphthylene ND 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(a)anthracene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(a)pyrene ND 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(b)fluoranthene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(g,h,i)perylene ND 0.00797 1 05/17/2023 18:16 WG2059490
Benzo(k)fluoranthene ND 0.00797 1 05/17/2023 18:16 WG2059490
Chrysene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Dibenz(a,h)anthracene ND 0.00797 1 05/17/2023 18:16 WG2059490
Fluoranthene ND 0.00797 1 05/17/2023 18:16 WG2059490
Fluorene ND 0.00797 1 05/17/2023 18:16 WG2059490
Indeno(1,2,3-cd)pyrene ND J4 0.00797 1 05/17/2023 18:16 WG2059490
Naphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
Phenanthrene ND 0.00797 1 05/17/2023 18:16 WG2059490
Pyrene ND 0.00797 1 05/17/2023 18:16 WG2059490
1-Methylnaphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
2-Methylnaphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
2-Chloronaphthalene ND 0.0266 1 05/17/2023 18:16 WG2059490
(S) p-Terphenyl-d14 87.5 23.0-120 05/17/2023 18:16 WG2059490
(S) Nitrobenzene-d5 73.4 14.0-149 05/17/2023 18:16 WG2059490
(S) 2-Fluorobiphenyl 65.8 34.0-125 05/17/2023 18:16 WG2059490
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.0 1 05/10/2023 17:08 WG2057261
Wet Chemistry by Method 7199
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.30 1 05/13/2023 15:05 WG2057052
Mercury by Method 7471A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0520 1 05/18/2023 16:56 WG2057613
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.60 1 05/11/2023 21:49 WG2057224
Arsenic 6.27 2.60 1 05/11/2023 21:49 WG2057224
Beryllium 0.399 0.260 1 05/11/2023 21:49 WG2057224
Cadmium ND 0.650 1 05/11/2023 21:49 WG2057224
Chromium 10.3 1.30 1 05/11/2023 21:49 WG2057224
Copper 8.52 2.60 1 05/11/2023 21:49 WG2057224
Lead 5.43 0.650 1 05/11/2023 21:49 WG2057224
Nickel 7.30 2.60 1 05/11/2023 21:49 WG2057224
Selenium ND 2.60 1 05/11/2023 21:49 WG2057224
Silver ND 1.30 1 05/11/2023 21:49 WG2057224
Thallium ND 2.60 1 05/11/2023 21:49 WG2057224
Zinc 30.9 6.50 1 05/11/2023 21:49 WG2057224
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.13 26 05/14/2023 06:07 WG2059653
(S) a,a,a-Trifluorotoluene(FID) 90.0 77.0-120 05/14/2023 06:07 WG2059653
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0826 1.04 05/14/2023 12:04 WG2059688
Acrylonitrile ND 0.0206 1.04 05/14/2023 12:04 WG2059688
Benzene ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Bromobenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
Bromodichloromethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Bromoform ND 0.0413 1.04 05/14/2023 12:04 WG2059688
Bromomethane ND 0.0206 1.04 05/14/2023 12:04 WG2059688
n-Butylbenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
sec-Butylbenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
tert-Butylbenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Carbon tetrachloride ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Chlorobenzene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Chlorodibromomethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Chloroethane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Chloroform ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Chloromethane ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2-Chlorotoluene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
4-Chlorotoluene ND J4 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2-Dibromo-3-Chloropropane ND 0.0413 1.04 05/14/2023 12:04 WG2059688
1,2-Dibromoethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Dibromomethane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2-Dichlorobenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,3-Dichlorobenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,4-Dichlorobenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Dichlorodifluoromethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1-Dichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,2-Dichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1-Dichloroethene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
cis-1,2-Dichloroethene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
trans-1,2-Dichloroethene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2-Dichloropropane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,1-Dichloropropene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,3-Dichloropropane ND 0.00826 1.04 05/14/2023 12:04 WG2059688
cis-1,3-Dichloropropene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
trans-1,3-Dichloropropene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
2,2-Dichloropropane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Di-isopropyl ether ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Ethylbenzene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Hexachloro-1,3-butadiene ND 0.0413 1.04 05/14/2023 12:04 WG2059688
Isopropylbenzene ND 0.00413 1.04 05/14/2023 12:04 WG2059688
p-Isopropyltoluene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
2-Butanone (MEK)ND 0.165 1.04 05/14/2023 12:04 WG2059688
Methylene Chloride ND 0.0413 1.04 05/14/2023 12:04 WG2059688
4-Methyl-2-pentanone (MIBK) ND 0.0413 1.04 05/14/2023 12:04 WG2059688
Methyl tert-butyl ether ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Naphthalene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
n-Propylbenzene ND J4 0.00826 1.04 05/14/2023 12:04 WG2059688
Styrene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,1,1,2-Tetrachloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1,2,2-Tetrachloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1,2-Trichlorotrifluoroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Tetrachloroethene 0.00772 0.00413 1.04 05/14/2023 12:04 WG2059688
Toluene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2,3-Trichlorobenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,2,4-Trichlorobenzene ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,1,1-Trichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
1,1,2-Trichloroethane ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Trichloroethene ND 0.00165 1.04 05/14/2023 12:04 WG2059688
Trichlorofluoromethane ND J4 0.00413 1.04 05/14/2023 12:04 WG2059688
1,2,3-Trichloropropane ND 0.0206 1.04 05/14/2023 12:04 WG2059688
1,2,4-Trimethylbenzene ND J4 0.00826 1.04 05/14/2023 12:04 WG2059688
1,2,3-Trimethylbenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
1,3,5-Trimethylbenzene ND 0.00826 1.04 05/14/2023 12:04 WG2059688
Vinyl chloride ND 0.00413 1.04 05/14/2023 12:04 WG2059688
Xylenes, Total ND 0.0107 1.04 05/14/2023 12:04 WG2059688
(S) Toluene-d8 110 75.0-131 05/14/2023 12:04 WG2059688
(S) 4-Bromofluorobenzene 103 67.0-138 05/14/2023 12:04 WG2059688
(S) 1,2-Dichloroethane-d4 95.3 70.0-130 05/14/2023 12:04 WG2059688
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 8.98 5.20 1 05/17/2023 22:56 WG2061264
C28-C40 Oil Range 26.1 5.20 1 05/17/2023 22:56 WG2061264
(S) o-Terphenyl 38.1 18.0-148 05/17/2023 22:56 WG2061264
Polychlorinated Biphenyls (GC) by Method 8082
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
PCB 1016 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1221 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1232 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1242 ND 0.0442 1 05/15/2023 01:50 WG2059034
PCB 1248 ND 0.0221 1 05/15/2023 01:50 WG2059034
PCB 1254 ND 0.0221 1 05/15/2023 01:50 WG2059034
PCB 1260 ND 0.0221 1 05/15/2023 01:50 WG2059034
(S) Decachlorobiphenyl 36.5 10.0-135 05/15/2023 01:50 WG2059034
(S) Tetrachloro-m-xylene 41.8 10.0-139 05/15/2023 01:50 WG2059034
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Acenaphthylene ND 0.0433 1 05/14/2023 00:45 WG2059348
Anthracene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzidine ND J6 2.17 1 05/14/2023 00:45 WG2059348
Benzo(a)anthracene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(b)fluoranthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(k)fluoranthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(g,h,i)perylene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzo(a)pyrene ND 0.0433 1 05/14/2023 00:45 WG2059348
Bis(2-chlorethoxy)methane ND 0.433 1 05/14/2023 00:45 WG2059348
Bis(2-chloroethyl)ether ND 0.433 1 05/14/2023 00:45 WG2059348
2,2-Oxybis(1-Chloropropane) ND 0.433 1 05/14/2023 00:45 WG2059348
4-Bromophenyl-phenylether ND 0.433 1 05/14/2023 00:45 WG2059348
2-Chloronaphthalene ND 0.0433 1 05/14/2023 00:45 WG2059348
4-Chlorophenyl-phenylether ND 0.433 1 05/14/2023 00:45 WG2059348
Chrysene ND 0.0433 1 05/14/2023 00:45 WG2059348
Dibenz(a,h)anthracene ND 0.0433 1 05/14/2023 00:45 WG2059348
3,3-Dichlorobenzidine ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dinitrotoluene ND 0.433 1 05/14/2023 00:45 WG2059348
2,6-Dinitrotoluene ND 0.433 1 05/14/2023 00:45 WG2059348
Fluoranthene ND 0.0433 1 05/14/2023 00:45 WG2059348
Fluorene ND 0.0433 1 05/14/2023 00:45 WG2059348
Hexachlorobenzene ND 0.433 1 05/14/2023 00:45 WG2059348
Hexachloro-1,3-butadiene ND 0.433 1 05/14/2023 00:45 WG2059348
Hexachlorocyclopentadiene ND 0.433 1 05/14/2023 00:45 WG2059348
Hexachloroethane ND 0.433 1 05/14/2023 00:45 WG2059348
Indeno(1,2,3-cd)pyrene ND 0.0433 1 05/14/2023 00:45 WG2059348
Isophorone ND 0.433 1 05/14/2023 00:45 WG2059348
Naphthalene ND 0.0433 1 05/14/2023 00:45 WG2059348
Nitrobenzene ND 0.433 1 05/14/2023 00:45 WG2059348
n-Nitrosodimethylamine ND 0.433 1 05/14/2023 00:45 WG2059348
n-Nitrosodiphenylamine ND 0.433 1 05/14/2023 00:45 WG2059348
n-Nitrosodi-n-propylamine ND 0.433 1 05/14/2023 00:45 WG2059348
Phenanthrene ND 0.0433 1 05/14/2023 00:45 WG2059348
Benzylbutyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1614172
CS-5
Collected date/time: 05/08/23 09:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Bis(2-ethylhexyl)phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Di-n-butyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Diethyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Dimethyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Di-n-octyl phthalate ND 0.433 1 05/14/2023 00:45 WG2059348
Pyrene ND 0.0433 1 05/14/2023 00:45 WG2059348
1,2,4-Trichlorobenzene ND 0.433 1 05/14/2023 00:45 WG2059348
4-Chloro-3-methylphenol ND 0.433 1 05/14/2023 00:45 WG2059348
2-Chlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dichlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dimethylphenol ND 0.433 1 05/14/2023 00:45 WG2059348
4,6-Dinitro-2-methylphenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4-Dinitrophenol ND 0.433 1 05/14/2023 00:45 WG2059348
2-Nitrophenol ND 0.433 1 05/14/2023 00:45 WG2059348
4-Nitrophenol ND 0.433 1 05/14/2023 00:45 WG2059348
Pentachlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
Phenol ND 0.433 1 05/14/2023 00:45 WG2059348
2,4,6-Trichlorophenol ND 0.433 1 05/14/2023 00:45 WG2059348
(S) Nitrobenzene-d5 44.0 10.0-122 05/14/2023 00:45 WG2059348
(S) 2-Fluorobiphenyl 47.7 15.0-120 05/14/2023 00:45 WG2059348
(S) p-Terphenyl-d14 55.4 10.0-120 05/14/2023 00:45 WG2059348
(S) Phenol-d5 44.6 10.0-120 05/14/2023 00:45 WG2059348
(S) 2-Fluorophenol 48.6 12.0-120 05/14/2023 00:45 WG2059348
(S) 2,4,6-Tribromophenol 58.3 10.0-127 05/14/2023 00:45 WG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00780 1 05/15/2023 19:10 WG2059491
Acenaphthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Acenaphthylene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(a)anthracene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(a)pyrene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(b)fluoranthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(g,h,i)perylene ND 0.00780 1 05/15/2023 19:10 WG2059491
Benzo(k)fluoranthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Chrysene ND 0.00780 1 05/15/2023 19:10 WG2059491
Dibenz(a,h)anthracene ND 0.00780 1 05/15/2023 19:10 WG2059491
Fluoranthene ND 0.00780 1 05/15/2023 19:10 WG2059491
Fluorene ND 0.00780 1 05/15/2023 19:10 WG2059491
Indeno(1,2,3-cd)pyrene ND 0.00780 1 05/15/2023 19:10 WG2059491
Naphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
Phenanthrene ND 0.00780 1 05/15/2023 19:10 WG2059491
Pyrene ND 0.00780 1 05/15/2023 19:10 WG2059491
1-Methylnaphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
2-Methylnaphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
2-Chloronaphthalene ND 0.0260 1 05/15/2023 19:10 WG2059491
(S) p-Terphenyl-d14 84.7 23.0-120 05/15/2023 19:10 WG2059491
(S) Nitrobenzene-d5 81.4 14.0-149 05/15/2023 19:10 WG2059491
(S) 2-Fluorobiphenyl 68.9 34.0-125 05/15/2023 19:10 WG2059491
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057261
Total Solids by Method 2540 G-2011 L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3923503-1 05/10/23 17:08
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1614172-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1614172-02 05/10/23 17:08 • (DUP) R3923503-3 05/10/23 17:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 82.0 80.9 1 1.33 10
Laboratory Control Sample (LCS)
(LCS) R3923503-2 05/10/23 17:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057052
Wet Chemistry by Method 7199 L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3924698-1 05/13/23 13:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1614576-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1614576-02 05/13/23 15:31 • (DUP) R3924698-7 05/13/23 15:36
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
L1613016-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1613016-02 05/13/23 16:02 • (DUP) R3924698-8 05/13/23 16:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium 1610 1370 100 16.2 20
Laboratory Control Sample (LCS)
(LCS) R3924698-2 05/13/23 13:26
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 10.5 105 80.0-120
L1613016-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1613016-01 05/13/23 13:32 • (MS) R3924698-3 05/13/23 13:37 • (MSD) R3924698-4 05/13/23 13:42
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 4.93 26.6 26.2 108 106 1 75.0-125 1.53 20
L1613016-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1613016-01 05/13/23 13:32 • (MS) R3924698-5 05/13/23 13:47
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 646 4.93 776 120 50 75.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057613
Mercury by Method 7471A L1614172-05
Method Blank (MB)
(MB) R3926642-1 05/18/23 16:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3926642-2 05/18/23 16:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.547 109 80.0-120
L1614238-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-01 05/18/23 16:44 • (MS) R3926642-3 05/18/23 16:47 • (MSD) R3926642-4 05/18/23 16:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.580 ND 0.575 0.590 93.4 96.0 1 75.0-125 2.61 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057615
Mercury by Method 7471A L1614172-01,02,03,04
Method Blank (MB)
(MB) R3924101-1 05/12/23 10:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3924101-2 05/12/23 10:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.582 116 80.0-120
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/12/23 10:45 • (MS) R3924101-3 05/12/23 10:47 • (MSD) R3924101-4 05/12/23 10:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.547 ND 0.476 0.612 79.0 104 1 75.0-125 J3 25.1 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057224
Metals (ICP) by Method 6010B L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3923898-1 05/11/23 20:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic U 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper 0.532 J 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3923898-2 05/11/23 20:58
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 98.5 98.5 80.0-120
Arsenic 100 94.5 94.5 80.0-120
Beryllium 100 98.6 98.6 80.0-120
Cadmium 100 97.0 97.0 80.0-120
Chromium 100 98.3 98.3 80.0-120
Copper 100 99.5 99.5 80.0-120
Lead 100 95.7 95.7 80.0-120
Nickel 100 96.9 96.9 80.0-120
Selenium 100 98.9 98.9 80.0-120
Silver 20.0 19.3 96.7 80.0-120
Thallium 100 95.4 95.4 80.0-120
Zinc 100 94.8 94.8 80.0-120
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/11/23 21:01 • (MS) R3923898-5 05/11/23 21:09 • (MSD) R3923898-6 05/11/23 21:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 109 ND 73.5 80.3 65.9 72.0 1 75.0-125 J6 J6 8.74 20
Arsenic 109 2.27 110 116 98.6 104 1 75.0-125 4.79 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2057224
Metals (ICP) by Method 6010B L1614172-01,02,03,04,05
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/11/23 21:01 • (MS) R3923898-5 05/11/23 21:09 • (MSD) R3923898-6 05/11/23 21:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 109 0.387 107 118 97.1 107 1 75.0-125 9.77 20
Cadmium 109 ND 107 118 97.9 108 1 75.0-125 9.75 20
Chromium 109 35.5 143 151 98.0 105 1 75.0-125 5.35 20
Copper 109 27.1 153 154 115 116 1 75.0-125 0.822 20
Lead 109 17.9 143 133 114 106 1 75.0-125 6.71 20
Nickel 109 33.6 149 156 105 112 1 75.0-125 4.79 20
Selenium 109 ND 109 117 99.9 106 1 75.0-125 6.34 20
Silver 21.9 ND 21.8 23.7 99.8 108 1 75.0-125 8.35 20
Thallium 109 ND 96.2 107 87.9 97.4 1 75.0-125 10.3 20
Zinc 109 53.6 157 172 94.4 108 1 75.0-125 9.02 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059653
Volatile Organic Compounds (GC) by Method 8015D/GRO L1614172-02,03,04,05
Method Blank (MB)
(MB) R3925948-2 05/14/23 01:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.728 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)92.9 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3925948-1 05/13/23 23:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 4.79 87.1 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 107 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062511
Volatile Organic Compounds (GC) by Method 8015D/GRO L1614172-01
Method Blank (MB)
(MB) R3926950-3 05/18/23 13:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)92.5 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3926950-2 05/18/23 12:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.47 99.5 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 97.5 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Method Blank (MB)
(MB) R3925455-3 05/13/23 13:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Method Blank (MB)
(MB) R3925455-3 05/13/23 13:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride 0.00695 J 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 109 75.0-131
(S) 4-Bromofluorobenzene 99.1 67.0-138
(S) 1,2-Dichloroethane-d4 86.4 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3925455-1 05/13/23 11:47 • (LCSD) R3925455-2 05/13/23 12:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.538 0.556 86.1 89.0 10.0-160 3.29 31
Acrylonitrile 0.625 0.727 0.830 116 133 45.0-153 13.2 22
Benzene 0.125 0.106 0.105 84.8 84.0 70.0-123 0.948 20
Bromobenzene 0.125 0.0990 0.0976 79.2 78.1 73.0-121 1.42 20
Bromodichloromethane 0.125 0.104 0.107 83.2 85.6 73.0-121 2.84 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3925455-1 05/13/23 11:47 • (LCSD) R3925455-2 05/13/23 12:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.117 0.121 93.6 96.8 64.0-132 3.36 20
Bromomethane 0.125 0.106 0.0983 84.8 78.6 56.0-147 7.54 20
n-Butylbenzene 0.125 0.0993 0.110 79.4 88.0 68.0-135 10.2 20
sec-Butylbenzene 0.125 0.103 0.107 82.4 85.6 74.0-130 3.81 20
tert-Butylbenzene 0.125 0.104 0.103 83.2 82.4 75.0-127 0.966 20
Carbon tetrachloride 0.125 0.118 0.118 94.4 94.4 66.0-128 0.000 20
Chlorobenzene 0.125 0.112 0.114 89.6 91.2 76.0-128 1.77 20
Chlorodibromomethane 0.125 0.110 0.113 88.0 90.4 74.0-127 2.69 20
Chloroethane 0.125 0.108 0.0961 86.4 76.9 61.0-134 11.7 20
Chloroform 0.125 0.106 0.104 84.8 83.2 72.0-123 1.90 20
Chloromethane 0.125 0.103 0.104 82.4 83.2 51.0-138 0.966 20
2-Chlorotoluene 0.125 0.106 0.107 84.8 85.6 75.0-124 0.939 20
4-Chlorotoluene 0.125 0.0851 0.0865 68.1 69.2 75.0-124 J4 J4 1.63 20
1,2-Dibromo-3-Chloropropane 0.125 0.137 0.151 110 121 59.0-130 9.72 20
1,2-Dibromoethane 0.125 0.112 0.117 89.6 93.6 74.0-128 4.37 20
Dibromomethane 0.125 0.112 0.111 89.6 88.8 75.0-122 0.897 20
1,2-Dichlorobenzene 0.125 0.0998 0.108 79.8 86.4 76.0-124 7.89 20
1,3-Dichlorobenzene 0.125 0.101 0.105 80.8 84.0 76.0-125 3.88 20
1,4-Dichlorobenzene 0.125 0.0985 0.106 78.8 84.8 77.0-121 7.33 20
Dichlorodifluoromethane 0.125 0.0864 0.0927 69.1 74.2 43.0-156 7.04 20
1,1-Dichloroethane 0.125 0.105 0.106 84.0 84.8 70.0-127 0.948 20
1,2-Dichloroethane 0.125 0.0926 0.0952 74.1 76.2 65.0-131 2.77 20
1,1-Dichloroethene 0.125 0.105 0.107 84.0 85.6 65.0-131 1.89 20
cis-1,2-Dichloroethene 0.125 0.114 0.110 91.2 88.0 73.0-125 3.57 20
trans-1,2-Dichloroethene 0.125 0.112 0.107 89.6 85.6 71.0-125 4.57 20
1,2-Dichloropropane 0.125 0.103 0.103 82.4 82.4 74.0-125 0.000 20
1,1-Dichloropropene 0.125 0.115 0.118 92.0 94.4 73.0-125 2.58 20
1,3-Dichloropropane 0.125 0.107 0.107 85.6 85.6 80.0-125 0.000 20
cis-1,3-Dichloropropene 0.125 0.100 0.0990 80.0 79.2 76.0-127 1.01 20
trans-1,3-Dichloropropene 0.125 0.0993 0.0968 79.4 77.4 73.0-127 2.55 20
2,2-Dichloropropane 0.125 0.101 0.101 80.8 80.8 59.0-135 0.000 20
Di-isopropyl ether 0.125 0.105 0.107 84.0 85.6 60.0-136 1.89 20
Ethylbenzene 0.125 0.117 0.121 93.6 96.8 74.0-126 3.36 20
Hexachloro-1,3-butadiene 0.125 0.0970 0.110 77.6 88.0 57.0-150 12.6 20
Isopropylbenzene 0.125 0.117 0.128 93.6 102 72.0-127 8.98 20
p-Isopropyltoluene 0.125 0.102 0.109 81.6 87.2 72.0-133 6.64 20
2-Butanone (MEK)0.625 0.669 0.662 107 106 30.0-160 1.05 24
Methylene Chloride 0.125 0.108 0.108 86.4 86.4 68.0-123 0.000 20
4-Methyl-2-pentanone (MIBK) 0.625 0.725 0.725 116 116 56.0-143 0.000 20
Methyl tert-butyl ether 0.125 0.109 0.111 87.2 88.8 66.0-132 1.82 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059471
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3925455-1 05/13/23 11:47 • (LCSD) R3925455-2 05/13/23 12:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.120 0.161 96.0 129 59.0-130 J3 29.2 20
n-Propylbenzene 0.125 0.0941 0.0973 75.3 77.8 74.0-126 3.34 20
Styrene 0.125 0.110 0.113 88.0 90.4 72.0-127 2.69 20
1,1,1,2-Tetrachloroethane 0.125 0.114 0.117 91.2 93.6 74.0-129 2.60 20
1,1,2,2-Tetrachloroethane 0.125 0.119 0.115 95.2 92.0 68.0-128 3.42 20
1,1,2-Trichlorotrifluoroethane 0.125 0.119 0.122 95.2 97.6 61.0-139 2.49 20
Tetrachloroethene 0.125 0.116 0.118 92.8 94.4 70.0-136 1.71 20
Toluene 0.125 0.106 0.106 84.8 84.8 75.0-121 0.000 20
1,2,3-Trichlorobenzene 0.125 0.105 0.140 84.0 112 59.0-139 J3 28.6 20
1,2,4-Trichlorobenzene 0.125 0.0977 0.128 78.2 102 62.0-137 J3 26.8 20
1,1,1-Trichloroethane 0.125 0.116 0.114 92.8 91.2 69.0-126 1.74 20
1,1,2-Trichloroethane 0.125 0.114 0.109 91.2 87.2 78.0-123 4.48 20
Trichloroethene 0.125 0.112 0.111 89.6 88.8 76.0-126 0.897 20
Trichlorofluoromethane 0.125 0.115 0.117 92.0 93.6 61.0-142 1.72 20
1,2,3-Trichloropropane 0.125 0.126 0.115 101 92.0 67.0-129 9.13 20
1,2,4-Trimethylbenzene 0.125 0.101 0.105 80.8 84.0 70.0-126 3.88 20
1,2,3-Trimethylbenzene 0.125 0.101 0.106 80.8 84.8 74.0-124 4.83 20
1,3,5-Trimethylbenzene 0.125 0.104 0.104 83.2 83.2 73.0-127 0.000 20
Vinyl chloride 0.125 0.109 0.103 87.2 82.4 63.0-134 5.66 20
Xylenes, Total 0.375 0.337 0.346 89.9 92.3 72.0-127 2.64 20
(S) Toluene-d8 102 102 75.0-131
(S) 4-Bromofluorobenzene 103 107 67.0-138
(S) 1,2-Dichloroethane-d4 93.7 93.8 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Method Blank (MB)
(MB) R3925553-2 05/14/23 07:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Method Blank (MB)
(MB) R3925553-2 05/14/23 07:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 91.7 67.0-138
(S) 1,2-Dichloroethane-d4 95.1 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3925553-1 05/14/23 06:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.609 97.4 10.0-160
Acrylonitrile 0.625 0.748 120 45.0-153
Benzene 0.125 0.101 80.8 70.0-123
Bromobenzene 0.125 0.0959 76.7 73.0-121
Bromodichloromethane 0.125 0.110 88.0 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925553-1 05/14/23 06:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.146 117 64.0-132
Bromomethane 0.125 0.176 141 56.0-147
n-Butylbenzene 0.125 0.0940 75.2 68.0-135
sec-Butylbenzene 0.125 0.0983 78.6 74.0-130
tert-Butylbenzene 0.125 0.0947 75.8 75.0-127
Carbon tetrachloride 0.125 0.130 104 66.0-128
Chlorobenzene 0.125 0.109 87.2 76.0-128
Chlorodibromomethane 0.125 0.128 102 74.0-127
Chloroethane 0.125 0.143 114 61.0-134
Chloroform 0.125 0.109 87.2 72.0-123
Chloromethane 0.125 0.128 102 51.0-138
2-Chlorotoluene 0.125 0.106 84.8 75.0-124
4-Chlorotoluene 0.125 0.0876 70.1 75.0-124 J4
1,2-Dibromo-3-Chloropropane 0.125 0.137 110 59.0-130
1,2-Dibromoethane 0.125 0.117 93.6 74.0-128
Dibromomethane 0.125 0.119 95.2 75.0-122
1,2-Dichlorobenzene 0.125 0.0993 79.4 76.0-124
1,3-Dichlorobenzene 0.125 0.0974 77.9 76.0-125
1,4-Dichlorobenzene 0.125 0.0993 79.4 77.0-121
Dichlorodifluoromethane 0.125 0.0882 70.6 43.0-156
1,1-Dichloroethane 0.125 0.113 90.4 70.0-127
1,2-Dichloroethane 0.125 0.0982 78.6 65.0-131
1,1-Dichloroethene 0.125 0.119 95.2 65.0-131
cis-1,2-Dichloroethene 0.125 0.107 85.6 73.0-125
trans-1,2-Dichloroethene 0.125 0.121 96.8 71.0-125
1,2-Dichloropropane 0.125 0.101 80.8 74.0-125
1,1-Dichloropropene 0.125 0.110 88.0 73.0-125
1,3-Dichloropropane 0.125 0.108 86.4 80.0-125
cis-1,3-Dichloropropene 0.125 0.0984 78.7 76.0-127
trans-1,3-Dichloropropene 0.125 0.100 80.0 73.0-127
2,2-Dichloropropane 0.125 0.112 89.6 59.0-135
Di-isopropyl ether 0.125 0.105 84.0 60.0-136
Ethylbenzene 0.125 0.112 89.6 74.0-126
Hexachloro-1,3-butadiene 0.125 0.0867 69.4 57.0-150
Isopropylbenzene 0.125 0.109 87.2 72.0-127
p-Isopropyltoluene 0.125 0.0971 77.7 72.0-133
2-Butanone (MEK)0.625 0.649 104 30.0-160
Methylene Chloride 0.125 0.114 91.2 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.765 122 56.0-143
Methyl tert-butyl ether 0.125 0.108 86.4 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925553-1 05/14/23 06:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.0969 77.5 59.0-130
n-Propylbenzene 0.125 0.0881 70.5 74.0-126 J4
Styrene 0.125 0.101 80.8 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.117 93.6 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.123 98.4 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.126 101 61.0-139
Tetrachloroethene 0.125 0.114 91.2 70.0-136
Toluene 0.125 0.103 82.4 75.0-121
1,2,3-Trichlorobenzene 0.125 0.0941 75.3 59.0-139
1,2,4-Trichlorobenzene 0.125 0.0916 73.3 62.0-137
1,1,1-Trichloroethane 0.125 0.117 93.6 69.0-126
1,1,2-Trichloroethane 0.125 0.119 95.2 78.0-123
Trichloroethene 0.125 0.106 84.8 76.0-126
Trichlorofluoromethane 0.125 0.189 151 61.0-142 J4
1,2,3-Trichloropropane 0.125 0.120 96.0 67.0-129
1,2,4-Trimethylbenzene 0.125 0.0874 69.9 70.0-126 J4
1,2,3-Trimethylbenzene 0.125 0.0971 77.7 74.0-124
1,3,5-Trimethylbenzene 0.125 0.0923 73.8 73.0-127
Vinyl chloride 0.125 0.141 113 63.0-134
Xylenes, Total 0.375 0.302 80.5 72.0-127
(S) Toluene-d8 105 75.0-131
(S) 4-Bromofluorobenzene 96.6 67.0-138
(S) 1,2-Dichloroethane-d4 99.2 70.0-130
L1614238-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-03 05/14/23 12:42 • (MS) R3925553-3 05/14/23 17:05 • (MSD) R3925553-4 05/14/23 17:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.968 ND 0.376 0.389 38.9 40.2 1 10.0-160 3.27 40
Acrylonitrile 0.968 ND 0.798 0.754 82.4 77.9 1 10.0-160 5.63 40
Benzene 0.194 ND 0.162 0.155 83.9 80.3 1 10.0-149 4.32 37
Bromobenzene 0.194 ND 0.142 0.154 73.4 79.8 1 10.0-156 8.32 38
Bromodichloromethane 0.194 ND 0.159 0.154 82.3 79.4 1 10.0-143 3.59 37
Bromoform 0.194 ND 0.186 0.181 96.0 93.5 1 10.0-146 2.55 36
Bromomethane 0.194 ND 0.124 0.151 64.0 78.0 1 10.0-149 19.6 38
n-Butylbenzene 0.194 ND 0.162 0.176 83.9 91.1 1 10.0-160 8.29 40
sec-Butylbenzene 0.194 ND 0.155 0.165 80.0 85.5 1 10.0-159 6.63 39
tert-Butylbenzene 0.194 ND 0.147 0.161 76.2 83.1 1 10.0-156 8.61 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
L1614238-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-03 05/14/23 12:42 • (MS) R3925553-3 05/14/23 17:05 • (MSD) R3925553-4 05/14/23 17:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.194 ND 0.203 0.197 105 102 1 10.0-145 3.12 37
Chlorobenzene 0.194 ND 0.167 0.165 86.3 85.5 1 10.0-152 0.939 39
Chlorodibromomethane 0.194 ND 0.183 0.176 94.4 91.1 1 10.0-146 3.48 37
Chloroethane 0.194 ND 0.137 0.118 70.7 60.9 1 10.0-146 15.0 40
Chloroform 0.194 ND 0.152 0.147 78.5 76.1 1 10.0-146 3.03 37
Chloromethane 0.194 ND 0.179 0.169 92.7 87.1 1 10.0-159 6.28 37
2-Chlorotoluene 0.194 ND 0.159 0.169 82.3 87.1 1 10.0-159 5.71 38
4-Chlorotoluene 0.194 ND 0.120 0.142 62.0 73.1 1 10.0-155 16.5 39
1,2-Dibromo-3-Chloropropane 0.194 ND 0.167 0.165 86.3 85.5 1 10.0-151 0.939 39
1,2-Dibromoethane 0.194 ND 0.170 0.167 87.9 86.3 1 10.0-148 1.85 34
Dibromomethane 0.194 ND 0.154 0.148 79.6 76.4 1 10.0-147 4.14 35
1,2-Dichlorobenzene 0.194 ND 0.146 0.159 75.5 82.3 1 10.0-155 8.59 37
1,3-Dichlorobenzene 0.194 ND 0.147 0.161 75.9 83.1 1 10.0-153 9.03 38
1,4-Dichlorobenzene 0.194 ND 0.146 0.161 75.6 83.1 1 10.0-151 9.46 38
Dichlorodifluoromethane 0.194 ND 0.173 0.156 89.5 80.6 1 10.0-160 10.4 35
1,1-Dichloroethane 0.194 ND 0.158 0.159 81.5 82.3 1 10.0-147 0.985 37
1,2-Dichloroethane 0.194 ND 0.130 0.123 67.2 63.8 1 10.0-148 5.17 35
1,1-Dichloroethene 0.194 ND 0.206 0.197 106 102 1 10.0-155 4.65 37
cis-1,2-Dichloroethene 0.194 ND 0.165 0.156 85.5 80.4 1 10.0-149 6.13 37
trans-1,2-Dichloroethene 0.194 ND 0.179 0.178 92.7 91.9 1 10.0-150 0.873 37
1,2-Dichloropropane 0.194 ND 0.149 0.144 76.9 74.4 1 10.0-148 3.31 37
1,1-Dichloropropene 0.194 ND 0.178 0.181 91.9 93.5 1 10.0-153 1.74 35
1,3-Dichloropropane 0.194 ND 0.158 0.161 81.5 83.1 1 10.0-154 1.96 35
cis-1,3-Dichloropropene 0.194 ND 0.146 0.141 75.6 73.1 1 10.0-151 3.36 37
trans-1,3-Dichloropropene 0.194 ND 0.158 0.158 81.5 81.5 1 10.0-148 0.000 37
2,2-Dichloropropane 0.194 ND 0.108 0.106 56.0 54.8 1 10.0-138 2.18 36
Di-isopropyl ether 0.194 ND 0.150 0.145 77.3 74.9 1 10.0-147 3.07 36
Ethylbenzene 0.194 0.00453 0.175 0.167 88.0 84.0 1 10.0-160 4.57 38
Hexachloro-1,3-butadiene 0.194 ND 0.214 0.200 110 103 1 10.0-160 6.79 40
Isopropylbenzene 0.194 ND 0.167 0.161 86.3 83.1 1 10.0-155 3.81 38
p-Isopropyltoluene 0.194 ND 0.152 0.170 78.8 87.9 1 10.0-160 10.9 40
2-Butanone (MEK)0.968 ND 0.660 0.631 68.2 65.2 1 10.0-160 4.59 40
Methylene Chloride 0.194 0.0420 0.201 0.214 82.3 88.8 1 10.0-141 6.02 37
4-Methyl-2-pentanone (MIBK) 0.968 ND 0.910 0.862 94.0 89.0 1 10.0-160 5.46 35
Methyl tert-butyl ether 0.194 ND 0.141 0.138 72.8 71.2 1 11.0-147 2.24 35
Naphthalene 0.194 0.0258 0.143 0.164 60.4 71.4 1 10.0-160 13.8 36
n-Propylbenzene 0.194 ND 0.142 0.156 73.6 80.6 1 10.0-158 9.10 38
Styrene 0.194 0.0272 0.184 0.189 81.1 83.5 1 10.0-160 2.51 40
1,1,1,2-Tetrachloroethane 0.194 ND 0.176 0.164 91.1 84.7 1 10.0-149 7.34 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059688
Volatile Organic Compounds (GC/MS) by Method 8260B L1614172-02,03,04,05
L1614238-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614238-03 05/14/23 12:42 • (MS) R3925553-3 05/14/23 17:05 • (MSD) R3925553-4 05/14/23 17:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.194 ND 0.158 0.158 81.5 81.5 1 10.0-160 0.000 35
1,1,2-Trichlorotrifluoroethane 0.194 ND 0.248 0.248 128 128 1 10.0-160 0.000 36
Tetrachloroethene 0.194 ND 0.215 0.211 111 109 1 10.0-156 2.20 39
Toluene 0.194 ND 0.179 0.179 90.1 90.1 1 10.0-156 0.000 38
1,2,3-Trichlorobenzene 0.194 ND 0.167 0.200 86.3 103 1 10.0-160 17.9 40
1,2,4-Trichlorobenzene 0.194 ND 0.161 0.190 83.1 98.4 1 10.0-160 16.9 40
1,1,1-Trichloroethane 0.194 ND 0.181 0.178 93.5 91.9 1 10.0-144 1.74 35
1,1,2-Trichloroethane 0.194 ND 0.173 0.167 89.5 86.3 1 10.0-160 3.67 35
Trichloroethene 0.194 ND 0.169 0.173 87.1 89.5 1 10.0-156 2.74 38
Trichlorofluoromethane 0.194 ND 0.243 0.189 126 97.6 1 10.0-160 25.3 40
1,2,3-Trichloropropane 0.194 ND 0.153 0.170 79.2 87.9 1 10.0-156 10.4 35
1,2,4-Trimethylbenzene 0.194 ND 0.145 0.152 71.8 75.3 1 10.0-160 4.53 36
1,2,3-Trimethylbenzene 0.194 ND 0.144 0.155 72.1 77.5 1 10.0-160 7.11 36
1,3,5-Trimethylbenzene 0.194 0.0151 0.146 0.161 67.8 75.3 1 10.0-160 9.46 38
Vinyl chloride 0.194 ND 0.183 0.178 94.4 91.9 1 10.0-160 2.60 37
Xylenes, Total 0.581 ND 0.495 0.484 83.7 81.8 1 10.0-160 2.23 38
(S) Toluene-d8 107 110 75.0-131
(S) 4-Bromofluorobenzene 97.4 94.6 67.0-138
(S) 1,2-Dichloroethane-d4 90.4 89.6 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2061264
Semi-Volatile Organic Compounds (GC) by Method 8015 L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3926233-1 05/17/23 20:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 55.9 18.0-148
Method Blank (MB)
(MB) R3926425-1 05/18/23 09:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range 2.22 J 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 87.8 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3926233-2 05/17/23 20:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 28.7 57.4 50.0-150
(S) o-Terphenyl 68.0 18.0-148
L1614205-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614205-01 05/17/23 21:51 • (MS) R3926233-3 05/17/23 22:04 • (MSD) R3926233-4 05/17/23 22:17
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 57.4 ND 32.3 32.7 56.4 56.7 1 50.0-150 1.07 20
(S) o-Terphenyl 57.6 53.2 18.0-148
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059033
Polychlorinated Biphenyls (GC) by Method 8082 L1614172-01,02,03,04
Method Blank (MB)
(MB) R3924792-1 05/15/23 00:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 97.9 10.0-135
(S) Tetrachloro-m-xylene 74.3 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3924792-5 05/15/23 01:18
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.113 67.7 36.0-141 P
PCB 1260 0.167 0.122 73.1 37.0-145 P
(S) Decachlorobiphenyl 87.1 10.0-135
(S) Tetrachloro-m-xylene 78.2 10.0-139
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/15/23 04:34 • (MS) R3924792-6 05/15/23 05:03 • (MSD) R3924792-7 05/15/23 05:13
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
PCB 1016 0.177 ND 0.112 0.100 63.0 57.1 1 10.0-160 P P 11.0 37
PCB 1260 0.177 ND 0.115 0.116 64.8 66.3 1 10.0-160 P P 0.948 38
(S) Decachlorobiphenyl 73.1 73.1 10.0-135
(S) Tetrachloro-m-xylene 72.1 70.7 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059034
Polychlorinated Biphenyls (GC) by Method 8082 L1614172-05
Method Blank (MB)
(MB) R3925344-1 05/15/23 01:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
PCB 1016 U 0.0118 0.0340
PCB 1221 U 0.0118 0.0340
PCB 1232 U 0.0118 0.0340
PCB 1242 U 0.0118 0.0340
PCB 1248 U 0.00738 0.0170
PCB 1254 U 0.00738 0.0170
PCB 1260 U 0.00738 0.0170
(S) Decachlorobiphenyl 0.000 J2 10.0-135
(S) Tetrachloro-m-xylene 0.000 J2 10.0-139
Laboratory Control Sample (LCS)
(LCS) R3925344-5 05/15/23 01:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
PCB 1016 0.167 0.0690 41.3 36.0-141
PCB 1260 0.167 0.0777 46.5 37.0-145
(S) Decachlorobiphenyl 49.4 10.0-135
(S) Tetrachloro-m-xylene 44.0 10.0-139
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3925411-2 05/13/23 21:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Method Blank (MB)
(MB) R3925411-2 05/13/23 21:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 44.4 10.0-122
(S) 2-Fluorobiphenyl 52.6 15.0-120
(S) p-Terphenyl-d14 64.3 10.0-120
(S) Phenol-d5 47.4 10.0-120
(S) 2-Fluorophenol 52.9 12.0-120
(S) 2,4,6-Tribromophenol 56.0 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3925411-1 05/13/23 20:49
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.412 61.9 38.0-120
Acenaphthylene 0.666 0.423 63.5 40.0-120
Anthracene 0.666 0.469 70.4 42.0-120
Benzidine 1.33 0.345 25.9 10.0-120
Benzo(a)anthracene 0.666 0.487 73.1 44.0-120
Benzo(b)fluoranthene 0.666 0.448 67.3 43.0-120
Benzo(k)fluoranthene 0.666 0.449 67.4 44.0-120
Benzo(g,h,i)perylene 0.666 0.465 69.8 43.0-120
Benzo(a)pyrene 0.666 0.490 73.6 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.346 52.0 20.0-120
Bis(2-chloroethyl)ether 0.666 0.402 60.4 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.394 59.2 23.0-120
4-Bromophenyl-phenylether 0.666 0.467 70.1 40.0-120
2-Chloronaphthalene 0.666 0.403 60.5 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925411-1 05/13/23 20:49
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.429 64.4 40.0-120
Chrysene 0.666 0.452 67.9 43.0-120
Dibenz(a,h)anthracene 0.666 0.469 70.4 44.0-120
3,3-Dichlorobenzidine 1.33 0.930 69.9 28.0-120
2,4-Dinitrotoluene 0.666 0.466 70.0 45.0-120
2,6-Dinitrotoluene 0.666 0.409 61.4 42.0-120
Fluoranthene 0.666 0.473 71.0 44.0-120
Fluorene 0.666 0.427 64.1 41.0-120
Hexachlorobenzene 0.666 0.492 73.9 39.0-120
Hexachloro-1,3-butadiene 0.666 0.372 55.9 15.0-120
Hexachlorocyclopentadiene 0.666 0.469 70.4 15.0-120
Hexachloroethane 0.666 0.376 56.5 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.441 66.2 45.0-120
Isophorone 0.666 0.333 50.0 23.0-120
Naphthalene 0.666 0.352 52.9 18.0-120
Nitrobenzene 0.666 0.311 46.7 17.0-120
n-Nitrosodimethylamine 0.666 0.314 47.1 10.0-125
n-Nitrosodiphenylamine 0.666 0.439 65.9 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.377 56.6 26.0-120
Phenanthrene 0.666 0.448 67.3 42.0-120
Benzylbutyl phthalate 0.666 0.470 70.6 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.448 67.3 41.0-120
Di-n-butyl phthalate 0.666 0.491 73.7 43.0-120
Diethyl phthalate 0.666 0.449 67.4 43.0-120
Dimethyl phthalate 0.666 0.448 67.3 43.0-120
Di-n-octyl phthalate 0.666 0.423 63.5 40.0-120
Pyrene 0.666 0.431 64.7 41.0-120
1,2,4-Trichlorobenzene 0.666 0.376 56.5 17.0-120
4-Chloro-3-methylphenol 0.666 0.361 54.2 28.0-120
2-Chlorophenol 0.666 0.408 61.3 28.0-120
2,4-Dichlorophenol 0.666 0.375 56.3 25.0-120
2,4-Dimethylphenol 0.666 0.358 53.8 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.347 52.1 16.0-120
2,4-Dinitrophenol 0.666 0.220 33.0 10.0-120
2-Nitrophenol 0.666 0.360 54.1 20.0-120
4-Nitrophenol 0.666 0.311 46.7 27.0-120
Pentachlorophenol 0.666 0.469 70.4 29.0-120
Phenol 0.666 0.353 53.0 28.0-120
2,4,6-Trichlorophenol 0.666 0.369 55.4 37.0-120
(S) Nitrobenzene-d5 48.0 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3925411-1 05/13/23 20:49
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 63.4 15.0-120
(S) p-Terphenyl-d14 72.7 10.0-120
(S) Phenol-d5 57.7 10.0-120
(S) 2-Fluorophenol 67.7 12.0-120
(S) 2,4,6-Tribromophenol 83.5 10.0-127
L1614172-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614172-05 05/14/23 00:45 • (MS) R3925411-3 05/14/23 01:07 • (MSD) R3925411-4 05/14/23 01:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.852 ND 0.368 0.362 43.1 42.7 1 18.0-120 1.42 32
Acenaphthylene 0.852 ND 0.382 0.369 44.8 43.4 1 25.0-120 3.46 32
Anthracene 0.852 ND 0.426 0.399 50.0 46.9 1 22.0-120 6.61 29
Benzidine 1.70 ND ND ND 7.57 8.09 1 10.0-120 J6 J6 6.63 40
Benzo(a)anthracene 0.852 ND 0.450 0.414 52.7 48.8 1 25.0-120 8.12 29
Benzo(b)fluoranthene 0.852 ND 0.407 0.375 47.7 44.2 1 19.0-122 7.97 31
Benzo(k)fluoranthene 0.852 ND 0.390 0.361 45.7 42.5 1 23.0-120 7.61 30
Benzo(g,h,i)perylene 0.852 ND 0.408 0.357 47.9 42.0 1 10.0-120 13.2 33
Benzo(a)pyrene 0.852 ND 0.451 0.412 52.9 48.5 1 24.0-120 9.04 30
Bis(2-chlorethoxy)methane 0.852 ND ND ND 35.1 35.6 1 10.0-120 1.30 34
Bis(2-chloroethyl)ether 0.852 ND ND ND 38.4 38.8 1 10.0-120 0.791 40
2,2-Oxybis(1-Chloropropane) 0.852 ND ND ND 37.2 38.7 1 10.0-120 3.62 40
4-Bromophenyl-phenylether 0.852 ND 0.438 ND 51.4 48.8 1 27.0-120 5.49 30
2-Chloronaphthalene 0.852 ND 0.360 0.357 42.2 42.0 1 20.0-120 0.725 32
4-Chlorophenyl-phenylether 0.852 ND ND ND 46.5 44.8 1 24.0-120 4.01 29
Chrysene 0.852 ND 0.409 0.379 48.0 44.6 1 21.0-120 7.58 29
Dibenz(a,h)anthracene 0.852 ND 0.427 0.381 50.2 44.8 1 10.0-120 11.6 32
3,3-Dichlorobenzidine 1.70 ND 0.648 0.676 38.1 39.7 1 10.0-120 4.12 34
2,4-Dinitrotoluene 0.852 ND ND ND 50.2 48.9 1 30.0-120 2.77 31
2,6-Dinitrotoluene 0.852 ND ND ND 46.2 46.2 1 25.0-120 0.331 31
Fluoranthene 0.852 ND 0.435 0.409 51.1 48.2 1 18.0-126 6.15 32
Fluorene 0.852 ND 0.390 0.375 45.7 44.2 1 25.0-120 3.74 30
Hexachlorobenzene 0.852 ND 0.448 ND 52.6 49.1 1 27.0-120 7.21 28
Hexachloro-1,3-butadiene 0.852 ND ND ND 37.0 37.9 1 10.0-120 2.04 38
Hexachlorocyclopentadiene 0.852 ND ND ND 23.5 21.6 1 10.0-120 8.81 40
Hexachloroethane 0.852 ND ND ND 33.5 35.0 1 10.0-120 4.01 40
Indeno(1,2,3-cd)pyrene 0.852 ND 0.422 0.383 49.5 45.1 1 10.0-120 9.68 32
Isophorone 0.852 ND ND ND 34.0 34.6 1 13.0-120 1.34 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059348
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1614172-01,02,03,04,05
L1614172-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614172-05 05/14/23 00:45 • (MS) R3925411-3 05/14/23 01:07 • (MSD) R3925411-4 05/14/23 01:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.852 ND 0.305 0.309 35.8 36.4 1 10.0-120 1.27 35
Nitrobenzene 0.852 ND ND ND 31.6 32.3 1 10.0-120 1.91 36
n-Nitrosodimethylamine 0.852 ND ND ND 23.5 23.4 1 10.0-127 0.651 40
n-Nitrosodiphenylamine 0.852 ND ND ND 47.9 45.9 1 17.0-120 4.56 29
n-Nitrosodi-n-propylamine 0.852 ND ND ND 37.5 37.3 1 10.0-120 0.816 37
Phenanthrene 0.852 ND 0.408 0.383 47.9 45.1 1 17.0-120 6.24 31
Benzylbutyl phthalate 0.852 ND 0.477 0.443 55.9 52.1 1 23.0-120 7.34 30
Bis(2-ethylhexyl)phthalate 0.852 ND 0.438 ND 51.4 48.2 1 17.0-126 6.75 30
Di-n-butyl phthalate 0.852 ND 0.461 ND 54.1 50.3 1 30.0-120 7.60 29
Diethyl phthalate 0.852 ND ND ND 47.7 46.2 1 26.0-120 3.58 28
Dimethyl phthalate 0.852 ND ND ND 47.9 45.9 1 25.0-120 4.56 29
Di-n-octyl phthalate 0.852 ND 0.452 ND 53.0 50.6 1 21.0-123 5.01 29
Pyrene 0.852 ND 0.400 0.374 47.0 44.0 1 16.0-121 6.71 32
1,2,4-Trichlorobenzene 0.852 ND ND ND 38.7 40.1 1 12.0-120 3.10 37
4-Chloro-3-methylphenol 0.852 ND ND ND 39.0 38.1 1 15.0-120 2.77 30
2-Chlorophenol 0.852 ND ND ND 41.0 41.9 1 15.0-120 1.84 37
2,4-Dichlorophenol 0.852 ND ND ND 43.9 44.2 1 20.0-120 0.347 31
2,4-Dimethylphenol 0.852 ND ND ND 15.4 18.2 1 10.0-120 16.4 33
4,6-Dinitro-2-methylphenol 0.852 ND ND ND 32.2 27.4 1 10.0-120 16.4 39
2,4-Dinitrophenol 0.852 ND ND ND 22.1 20.2 1 10.0-121 9.39 40
2-Nitrophenol 0.852 ND ND ND 41.0 42.0 1 12.0-120 2.21 39
4-Nitrophenol 0.852 ND ND ND 11.5 15.4 1 10.0-137 29.0 32
Pentachlorophenol 0.852 ND 0.435 ND 51.1 43.4 1 10.0-160 16.5 31
Phenol 0.852 ND ND ND 23.8 26.0 1 12.0-120 8.59 38
2,4,6-Trichlorophenol 0.852 ND ND ND 40.1 37.8 1 19.0-120 6.27 32
(S) Nitrobenzene-d5 33.5 33.6 10.0-122
(S) 2-Fluorobiphenyl 43.9 43.4 15.0-120
(S) p-Terphenyl-d14 53.4 48.9 10.0-120
(S) Phenol-d5 35.2 36.2 10.0-120
(S) 2-Fluorophenol 42.7 42.7 12.0-120
(S) 2,4,6-Tribromophenol 58.5 59.2 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059490
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-02,03,04
Method Blank (MB)
(MB) R3925884-2 05/17/23 00:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 90.5 23.0-120
(S) Nitrobenzene-d5 68.9 14.0-149
(S) 2-Fluorobiphenyl 68.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3925884-1 05/17/23 00:41
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0885 111 50.0-126
Acenaphthene 0.0800 0.0833 104 50.0-120
Acenaphthylene 0.0800 0.0819 102 50.0-120
Benzo(a)anthracene 0.0800 0.112 140 45.0-120 J4
Benzo(a)pyrene 0.0800 0.0937 117 42.0-120
Benzo(b)fluoranthene 0.0800 0.105 131 42.0-121 J4
Benzo(g,h,i)perylene 0.0800 0.0906 113 45.0-125
Benzo(k)fluoranthene 0.0800 0.0932 117 49.0-125
Chrysene 0.0800 0.110 138 49.0-122 J4
Dibenz(a,h)anthracene 0.0800 0.0906 113 47.0-125
Fluoranthene 0.0800 0.0970 121 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059490
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3925884-1 05/17/23 00:41
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0874 109 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.102 128 46.0-125 J4
Naphthalene 0.0800 0.0771 96.4 50.0-120
Phenanthrene 0.0800 0.0865 108 47.0-120
Pyrene 0.0800 0.0931 116 43.0-123
1-Methylnaphthalene 0.0800 0.0788 98.5 51.0-121
2-Methylnaphthalene 0.0800 0.0836 105 50.0-120
2-Chloronaphthalene 0.0800 0.0801 100 50.0-120
(S) p-Terphenyl-d14 92.7 23.0-120
(S) Nitrobenzene-d5 105 14.0-149
(S) 2-Fluorobiphenyl 88.8 34.0-125
L1614157-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614157-01 05/17/23 05:08 • (MS) R3925884-3 05/17/23 05:26 • (MSD) R3925884-4 05/17/23 05:44
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0876 ND 0.0904 0.0951 103 109 1 10.0-145 5.07 30
Acenaphthene 0.0876 ND 0.0821 0.0865 93.8 98.8 1 14.0-127 5.19 27
Acenaphthylene 0.0876 ND 0.0803 0.0851 91.6 97.1 1 21.0-124 5.83 25
Benzo(a)anthracene 0.0876 ND 0.0913 0.0974 104 111 1 10.0-139 6.50 30
Benzo(a)pyrene 0.0876 ND 0.0902 0.0958 103 109 1 10.0-141 6.00 31
Benzo(b)fluoranthene 0.0876 ND 0.0926 0.100 106 115 1 10.0-140 7.95 36
Benzo(g,h,i)perylene 0.0876 ND 0.0549 0.0530 62.6 60.5 1 10.0-140 3.45 33
Benzo(k)fluoranthene 0.0876 ND 0.0881 0.0943 101 108 1 10.0-137 6.72 31
Chrysene 0.0876 ND 0.0874 0.0937 99.8 107 1 10.0-145 7.01 30
Dibenz(a,h)anthracene 0.0876 ND 0.0554 0.0530 63.3 60.5 1 10.0-132 4.44 31
Fluoranthene 0.0876 ND 0.0926 0.0999 106 114 1 10.0-153 7.51 33
Fluorene 0.0876 ND 0.0896 0.0938 102 107 1 11.0-130 4.66 29
Indeno(1,2,3-cd)pyrene 0.0876 ND 0.0585 0.0564 66.8 64.4 1 10.0-137 3.62 32
Naphthalene 0.0876 ND 0.0693 0.0774 79.1 88.4 1 10.0-135 11.0 27
Phenanthrene 0.0876 ND 0.0859 0.0927 98.1 106 1 10.0-144 7.60 31
Pyrene 0.0876 ND 0.0877 0.0939 100 107 1 10.0-148 6.87 35
1-Methylnaphthalene 0.0876 ND 0.0746 0.0813 85.1 92.9 1 10.0-142 8.71 28
2-Methylnaphthalene 0.0876 ND 0.0789 0.0858 90.1 98.0 1 10.0-137 8.37 28
2-Chloronaphthalene 0.0876 ND 0.0764 0.0820 87.3 93.6 1 29.0-120 7.05 24
(S) p-Terphenyl-d14 92.2 94.4 23.0-120
(S) Nitrobenzene-d5 76.1 91.1 14.0-149
(S) 2-Fluorobiphenyl 71.3 78.9 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059491
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-05
Method Blank (MB)
(MB) R3924997-2 05/15/23 13:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 108 23.0-120
(S) Nitrobenzene-d5 94.8 14.0-149
(S) 2-Fluorobiphenyl 85.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3924997-1 05/15/23 13:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0761 95.1 50.0-126
Acenaphthene 0.0800 0.0727 90.9 50.0-120
Acenaphthylene 0.0800 0.0785 98.1 50.0-120
Benzo(a)anthracene 0.0800 0.0809 101 45.0-120
Benzo(a)pyrene 0.0800 0.0718 89.8 42.0-120
Benzo(b)fluoranthene 0.0800 0.0826 103 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0753 94.1 45.0-125
Benzo(k)fluoranthene 0.0800 0.0774 96.8 49.0-125
Chrysene 0.0800 0.0870 109 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0781 97.6 47.0-125
Fluoranthene 0.0800 0.0844 105 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059491
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-05
Laboratory Control Sample (LCS)
(LCS) R3924997-1 05/15/23 13:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0847 106 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0840 105 46.0-125
Naphthalene 0.0800 0.0784 98.0 50.0-120
Phenanthrene 0.0800 0.0835 104 47.0-120
Pyrene 0.0800 0.0875 109 43.0-123
1-Methylnaphthalene 0.0800 0.0837 105 51.0-121
2-Methylnaphthalene 0.0800 0.0791 98.9 50.0-120
2-Chloronaphthalene 0.0800 0.0799 99.9 50.0-120
(S) p-Terphenyl-d14 107 23.0-120
(S) Nitrobenzene-d5 110 14.0-149
(S) 2-Fluorobiphenyl 105 34.0-125
L1614496-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1614496-02 05/15/23 14:32 • (MS) R3924997-3 05/15/23 14:50 • (MSD) R3924997-4 05/15/23 15:07
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.105 ND 0.0661 0.0901 62.8 88.1 1 10.0-145 J3 30.7 30
Acenaphthene 0.105 ND 0.0643 0.0842 61.0 82.3 1 14.0-127 26.8 27
Acenaphthylene 0.105 ND 0.0729 0.0918 69.1 89.8 1 21.0-124 23.0 25
Benzo(a)anthracene 0.105 ND 0.0697 0.0945 66.1 92.4 1 10.0-139 J3 30.2 30
Benzo(a)pyrene 0.105 ND 0.0718 0.0974 68.1 95.2 1 10.0-141 30.2 31
Benzo(b)fluoranthene 0.105 ND 0.0642 0.0934 60.9 91.4 1 10.0-140 J3 37.1 36
Benzo(g,h,i)perylene 0.105 ND 0.0661 0.0942 62.8 92.1 1 10.0-140 J3 35.0 33
Benzo(k)fluoranthene 0.105 ND 0.0718 0.0934 68.1 91.4 1 10.0-137 26.2 31
Chrysene 0.105 ND 0.0837 0.106 79.4 103 1 10.0-145 23.1 30
Dibenz(a,h)anthracene 0.105 ND 0.0810 0.102 76.9 100 1 10.0-132 23.4 31
Fluoranthene 0.105 ND 0.0655 0.101 62.1 99.1 1 10.0-153 J3 43.0 33
Fluorene 0.105 ND 0.0710 0.0960 67.4 93.9 1 11.0-130 J3 30.0 29
Indeno(1,2,3-cd)pyrene 0.105 ND 0.0693 0.0966 65.8 94.5 1 10.0-137 J3 32.9 32
Naphthalene 0.105 ND 0.0839 0.0937 79.6 91.6 1 10.0-135 11.0 27
Phenanthrene 0.105 ND 0.0672 0.102 63.8 99.5 1 10.0-144 J3 40.9 31
Pyrene 0.105 ND 0.0682 0.104 64.8 102 1 10.0-148 J3 41.6 35
1-Methylnaphthalene 0.105 ND 0.0802 0.0983 76.1 96.1 1 10.0-142 20.2 28
2-Methylnaphthalene 0.105 ND 0.0759 0.0910 72.0 89.0 1 10.0-137 18.2 28
2-Chloronaphthalene 0.105 ND 0.0746 0.0925 70.8 90.5 1 29.0-120 21.5 24
(S) p-Terphenyl-d14 64.9 85.8 23.0-120
(S) Nitrobenzene-d5 95.8 84.7 14.0-149
(S) 2-Fluorobiphenyl 63.4 70.2 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062088
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-01
Method Blank (MB)
(MB) R3926686-2 05/18/23 16:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 99.5 23.0-120
(S) Nitrobenzene-d5 68.0 14.0-149
(S) 2-Fluorobiphenyl 83.7 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3926686-1 05/18/23 16:34
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0762 95.3 50.0-126
Acenaphthene 0.0800 0.0813 102 50.0-120
Acenaphthylene 0.0800 0.0751 93.9 50.0-120
Benzo(a)anthracene 0.0800 0.0740 92.5 45.0-120
Benzo(a)pyrene 0.0800 0.0784 98.0 42.0-120
Benzo(b)fluoranthene 0.0800 0.0885 111 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0905 113 45.0-125
Benzo(k)fluoranthene 0.0800 0.0868 109 49.0-125
Chrysene 0.0800 0.0865 108 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0870 109 47.0-125
Fluoranthene 0.0800 0.0809 101 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062088
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1614172-01
Laboratory Control Sample (LCS)
(LCS) R3926686-1 05/18/23 16:34
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0785 98.1 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0840 105 46.0-125
Naphthalene 0.0800 0.0819 102 50.0-120
Phenanthrene 0.0800 0.0816 102 47.0-120
Pyrene 0.0800 0.0827 103 43.0-123
1-Methylnaphthalene 0.0800 0.0796 99.5 51.0-121
2-Methylnaphthalene 0.0800 0.0817 102 50.0-120
2-Chloronaphthalene 0.0800 0.0819 102 50.0-120
(S) p-Terphenyl-d14 98.7 23.0-120
(S) Nitrobenzene-d5 75.8 14.0-149
(S) 2-Fluorobiphenyl 89.7 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
June 05, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1615666
Samples Received:05/12/2023
Project Number:
Description:
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
June 05, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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June 05, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
MW-1 L1615666-01 7
MW-2 L1615666-02 12
MW-3 L1615666-03 17
MW-4 L1615666-04 22
MW-5 L1615666-05 27
MW-6 L1615666-06 32
MW-1 FILTERED L1615666-07 37
MW-2 FILTERED L1615666-08 38
MW-3 FILTERED L1615666-09 39
MW-4 FILTERED L1615666-10 40
MW-5 FILTERED L1615666-11 41
MW-6 FILTERED L1615666-12 42
Qc: Quality Control Summary 43
Gravimetric Analysis by Method 2540 C-2011 43
Wet Chemistry by Method 2320 B-2011 44
Wet Chemistry by Method 350.1 47
Wet Chemistry by Method 410.4 48
Wet Chemistry by Method 9040C 49
Wet Chemistry by Method 9056A 50
Wet Chemistry by Method 9060A 52
Mercury by Method 7470A 54
Metals (ICP) by Method 6010B 56
Volatile Organic Compounds (GC) by Method 8015D/GRO 58
Volatile Organic Compounds (GC/MS) by Method 8260B 61
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 65
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 66
Gl: Glossary of Terms 70
Al: Accreditations & Locations 71
Sc: Sample Chain of Custody 72
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1615666-01 GW 05/11/23 13:48 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG2061054 1 05/17/23 08:19 05/17/23 09:52 AS Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG2060591 1 05/16/23 11:06 05/16/23 11:06 ARD Mt. Juliet, TN
Wet Chemistry by Method 350.1 WG2060350 1 05/16/23 09:42 05/16/23 09:42 BMD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG2059721 1 05/14/23 13:40 05/14/23 16:07 RTW Mt. Juliet, TN
Wet Chemistry by Method 9040C WG2061250 1 05/18/23 09:04 05/18/23 09:04 EPW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 1 05/13/23 21:51 05/13/23 21:51 LBR Mt. Juliet, TN
Wet Chemistry by Method 9060A WG2060200 1 05/15/23 15:07 05/15/23 15:07 LOH Mt. Juliet, TN
Mercury by Method 7470A WG2059827 1 06/01/23 18:07 06/05/23 11:50 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 21:42 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2062721 1 05/19/23 01:44 05/19/23 01:44 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2063135 1 05/19/23 23:10 05/19/23 23:10 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2061651 1 05/18/23 07:14 05/19/23 09:49 MWS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2060551 1.05 05/17/23 07:20 05/17/23 13:16 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1615666-02 GW 05/11/23 12:56 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG2061054 1 05/17/23 08:19 05/17/23 09:52 AS Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG2060591 1 05/16/23 11:24 05/16/23 11:24 ARD Mt. Juliet, TN
Wet Chemistry by Method 350.1 WG2060350 1 05/16/23 09:46 05/16/23 09:46 BMD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG2059721 1 05/14/23 13:40 05/14/23 16:07 RTW Mt. Juliet, TN
Wet Chemistry by Method 9040C WG2061250 1 05/18/23 09:04 05/18/23 09:04 EPW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 1 05/13/23 22:29 05/13/23 22:29 LBR Mt. Juliet, TN
Wet Chemistry by Method 9060A WG2060649 1 05/17/23 07:16 05/17/23 07:16 SJF Mt. Juliet, TN
Mercury by Method 7470A WG2059827 1 06/01/23 18:07 06/05/23 11:52 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 21:45 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/22/23 15:22 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2062721 1 05/19/23 02:07 05/19/23 02:07 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2063135 1 05/19/23 23:30 05/19/23 23:30 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2061651 1 05/18/23 07:14 05/19/23 10:10 MWS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2060551 1.05 05/17/23 07:20 05/17/23 13:37 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1615666-03 GW 05/11/23 11:21 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG2061054 1 05/17/23 08:19 05/17/23 09:52 AS Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG2062879 1 05/19/23 09:42 05/19/23 09:42 ARD Mt. Juliet, TN
Wet Chemistry by Method 350.1 WG2060350 1 05/16/23 09:49 05/16/23 09:49 BMD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG2059721 1 05/14/23 13:40 05/14/23 16:08 RTW Mt. Juliet, TN
Wet Chemistry by Method 9040C WG2061250 1 05/18/23 09:04 05/18/23 09:04 EPW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 1 05/13/23 22:42 05/13/23 22:42 LBR Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 10 05/14/23 03:24 05/14/23 03:24 LBR Mt. Juliet, TN
Wet Chemistry by Method 9060A WG2060649 1 05/17/23 07:34 05/17/23 07:34 SJF Mt. Juliet, TN
Mercury by Method 7470A WG2059827 1 06/01/23 18:07 06/05/23 11:55 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 21:31 ZSA Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/22/23 15:25 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2063582 10 05/21/23 15:52 05/21/23 15:52 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2063135 1 05/19/23 23:50 05/19/23 23:50 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2061651 1 05/18/23 07:14 05/19/23 17:44 HLJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2060551 1.05 05/17/23 07:20 05/17/23 13:59 AMG Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-4 L1615666-04 GW 05/11/23 12:10 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG2061054 1 05/17/23 08:19 05/17/23 09:52 AS Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG2062106 1 05/18/23 12:24 05/18/23 12:24 ARD Mt. Juliet, TN
Wet Chemistry by Method 350.1 WG2060350 1 05/16/23 09:51 05/16/23 09:51 BMD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG2059721 1 05/14/23 13:40 05/14/23 16:08 RTW Mt. Juliet, TN
Wet Chemistry by Method 9040C WG2061250 1 05/18/23 09:04 05/18/23 09:04 EPW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 1 05/13/23 22:55 05/13/23 22:55 LBR Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 10 05/14/23 03:37 05/14/23 03:37 LBR Mt. Juliet, TN
Wet Chemistry by Method 9060A WG2060649 1 05/17/23 07:52 05/17/23 07:52 SJF Mt. Juliet, TN
Mercury by Method 7470A WG2059827 1 06/01/23 18:07 06/05/23 11:57 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 21:47 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2062721 1 05/19/23 02:29 05/19/23 02:29 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2063135 1 05/20/23 00:09 05/20/23 00:09 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2061651 1 05/18/23 07:14 05/19/23 18:05 HLJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2060551 1.05 05/17/23 07:20 05/17/23 14:20 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1615666-05 GW 05/11/23 14:50 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG2061054 1 05/17/23 08:19 05/17/23 09:52 AS Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG2062879 1 05/19/23 09:47 05/19/23 09:47 ARD Mt. Juliet, TN
Wet Chemistry by Method 350.1 WG2060350 1 05/16/23 09:52 05/16/23 09:52 BMD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG2059721 1 05/14/23 13:40 05/14/23 16:08 RTW Mt. Juliet, TN
Wet Chemistry by Method 9040C WG2061250 1 05/18/23 09:04 05/18/23 09:04 EPW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 1 05/13/23 23:08 05/13/23 23:08 LBR Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 10 05/14/23 03:50 05/14/23 03:50 LBR Mt. Juliet, TN
Wet Chemistry by Method 9060A WG2060649 1 05/17/23 08:51 05/17/23 08:51 SJF Mt. Juliet, TN
Mercury by Method 7470A WG2059827 1 06/01/23 18:07 06/05/23 11:59 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 21:50 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2063048 5 05/19/23 17:43 05/19/23 17:43 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2063135 1 05/20/23 00:29 05/20/23 00:29 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2061651 1 05/18/23 07:14 05/19/23 10:30 MWS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2060551 1.05 05/17/23 07:20 05/17/23 15:24 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1615666-06 GW 05/11/23 10:40 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG2061054 1 05/17/23 08:19 05/17/23 09:52 AS Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG2062879 1 05/19/23 09:50 05/19/23 09:50 ARD Mt. Juliet, TN
Wet Chemistry by Method 350.1 WG2060350 1 05/16/23 09:58 05/16/23 09:58 BMD Mt. Juliet, TN
Wet Chemistry by Method 410.4 WG2059721 1 05/14/23 13:40 05/14/23 16:09 RTW Mt. Juliet, TN
Wet Chemistry by Method 9040C WG2061250 1 05/18/23 09:04 05/18/23 09:04 EPW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 1 05/13/23 23:21 05/13/23 23:21 LBR Mt. Juliet, TN
Wet Chemistry by Method 9056A WG2059136 10 05/14/23 04:03 05/14/23 04:03 LBR Mt. Juliet, TN
Wet Chemistry by Method 9060A WG2060649 1 05/17/23 09:26 05/17/23 09:26 SJF Mt. Juliet, TN
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:14 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 21:58 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2063048 5 05/19/23 18:01 05/19/23 18:01 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2063135 1 05/20/23 00:49 05/20/23 00:49 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2061651 1 05/18/23 07:14 05/19/23 10:51 MWS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2060551 1 05/17/23 07:20 05/17/23 15:45 AMG Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 FILTERED L1615666-07 GW 05/11/23 13:48 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:17 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 22:01 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 FILTERED L1615666-08 GW 05/11/23 12:56 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:24 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 22:04 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 FILTERED L1615666-09 GW 05/11/23 11:21 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:26 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 22:07 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4 FILTERED L1615666-10 GW 05/11/23 12:10 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:29 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 22:10 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 FILTERED L1615666-11 GW 05/11/23 14:50 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:31 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 22:12 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 FILTERED L1615666-12 GW 05/11/23 10:40 05/12/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG2059828 1 06/01/23 10:54 06/04/23 19:34 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2060110 1 05/17/23 15:23 05/18/23 22:15 ZSA Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Sample Delivery Group (SDG) Narrative
pH outside of method requirement.
Lab Sample ID Project Sample ID Method
L1615666-01 MW-1 8260B
L1615666-03 MW-3 8260B
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1615666
MW-1
Collected date/time: 05/11/23 13:48
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 468 10.0 1 05/17/2023 09:52 WG2061054
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity,Bicarbonate 345 20.0 1 05/16/2023 11:06 WG2060591
Alkalinity,Carbonate ND 20.0 1 05/16/2023 11:06 WG2060591
Sample Narrative:
L1615666-01 WG2060591: Endpoint pH 4.5 Headspace
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ammonia Nitrogen ND 0.250 1 05/16/2023 09:42 WG2060350
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD ND 20.0 1 05/14/2023 16:07 WG2059721
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 8.09 T8 1 05/18/2023 09:04 WG2061250
Sample Narrative:
L1615666-01 WG2061250: 8.09 at 19.8C
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 40.7 1.00 1 05/13/2023 21:51 WG2059136
Nitrate as (N)2.63 Q 0.100 1 05/13/2023 21:51 WG2059136
Sulfate 26.3 5.00 1 05/13/2023 21:51 WG2059136
Sample Narrative:
L1615666-01 WG2059136: Anions rerun 1 day outside hold for Nitrate due to unreportable in-hold run
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TOC (Total Organic Carbon)2.97 B 1.00 1 05/15/2023 15:07 WG2060200
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/05/2023 11:50 WG2059827
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1615666
MW-1
Collected date/time: 05/11/23 13:48
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 21:42 WG2060110
Arsenic 0.0184 B 0.0100 1 05/18/2023 21:42 WG2060110
Beryllium ND 0.00200 1 05/18/2023 21:42 WG2060110
Cadmium ND 0.00200 1 05/18/2023 21:42 WG2060110
Calcium 97.0 1.00 1 05/18/2023 21:42 WG2060110
Chromium ND 0.0100 1 05/18/2023 21:42 WG2060110
Copper ND 0.0100 1 05/18/2023 21:42 WG2060110
Iron 3.60 0.100 1 05/18/2023 21:42 WG2060110
Lead ND 0.00600 1 05/18/2023 21:42 WG2060110
Magnesium 44.8 1.00 1 05/18/2023 21:42 WG2060110
Manganese 0.138 0.0100 1 05/18/2023 21:42 WG2060110
Nickel ND 0.0100 1 05/18/2023 21:42 WG2060110
Potassium 6.47 2.00 1 05/18/2023 21:42 WG2060110
Selenium ND 0.0100 1 05/18/2023 21:42 WG2060110
Silver ND 0.00500 1 05/18/2023 21:42 WG2060110
Sodium 30.0 3.00 1 05/18/2023 21:42 WG2060110
Thallium ND 0.0100 1 05/18/2023 21:42 WG2060110
Zinc ND 0.0500 1 05/18/2023 21:42 WG2060110
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 05/19/2023 01:44 WG2062721
(S) a,a,a-Trifluorotoluene(FID) 94.7 78.0-120 05/19/2023 01:44 WG2062721
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 05/19/2023 23:10 WG2063135
Acrolein ND 0.0500 1 05/19/2023 23:10 WG2063135
Acrylonitrile ND 0.0100 1 05/19/2023 23:10 WG2063135
Benzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Bromobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Bromodichloromethane ND 0.00100 1 05/19/2023 23:10 WG2063135
Bromoform ND 0.00100 1 05/19/2023 23:10 WG2063135
Bromomethane ND 0.00500 1 05/19/2023 23:10 WG2063135
n-Butylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
sec-Butylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
tert-Butylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Carbon tetrachloride ND 0.00100 1 05/19/2023 23:10 WG2063135
Chlorobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Chlorodibromomethane ND 0.00100 1 05/19/2023 23:10 WG2063135
Chloroethane ND 0.00500 1 05/19/2023 23:10 WG2063135
Chloroform ND 0.00500 1 05/19/2023 23:10 WG2063135
Chloromethane ND 0.00250 1 05/19/2023 23:10 WG2063135
2-Chlorotoluene ND 0.00100 1 05/19/2023 23:10 WG2063135
4-Chlorotoluene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,2-Dibromo-3-Chloropropane ND 0.00500 1 05/19/2023 23:10 WG2063135
1,2-Dibromoethane ND 0.00100 1 05/19/2023 23:10 WG2063135
Dibromomethane ND 0.00100 1 05/19/2023 23:10 WG2063135
1,2-Dichlorobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,3-Dichlorobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,4-Dichlorobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Dichlorodifluoromethane ND 0.00500 1 05/19/2023 23:10 WG2063135
1,1-Dichloroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1615666
MW-1
Collected date/time: 05/11/23 13:48
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1,2-Dichloroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1-Dichloroethene ND 0.00100 1 05/19/2023 23:10 WG2063135
cis-1,2-Dichloroethene ND 0.00100 1 05/19/2023 23:10 WG2063135
trans-1,2-Dichloroethene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,2-Dichloropropane ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1-Dichloropropene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,3-Dichloropropane ND 0.00100 1 05/19/2023 23:10 WG2063135
cis-1,3-Dichloropropene ND 0.00100 1 05/19/2023 23:10 WG2063135
trans-1,3-Dichloropropene ND 0.00100 1 05/19/2023 23:10 WG2063135
2,2-Dichloropropane ND 0.00100 1 05/19/2023 23:10 WG2063135
Di-isopropyl ether ND 0.00100 1 05/19/2023 23:10 WG2063135
Ethylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Hexachloro-1,3-butadiene ND 0.00100 1 05/19/2023 23:10 WG2063135
Isopropylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
p-Isopropyltoluene ND 0.00100 1 05/19/2023 23:10 WG2063135
2-Butanone (MEK)ND 0.0100 1 05/19/2023 23:10 WG2063135
Methylene Chloride ND 0.00500 1 05/19/2023 23:10 WG2063135
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 05/19/2023 23:10 WG2063135
Methyl tert-butyl ether ND 0.00100 1 05/19/2023 23:10 WG2063135
Naphthalene ND 0.00500 1 05/19/2023 23:10 WG2063135
n-Propylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Styrene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1,1,2-Tetrachloroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
Tetrachloroethene ND 0.00100 1 05/19/2023 23:10 WG2063135
Toluene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,2,3-Trichlorobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,2,4-Trichlorobenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1,1-Trichloroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
1,1,2-Trichloroethane ND 0.00100 1 05/19/2023 23:10 WG2063135
Trichloroethene ND 0.00100 1 05/19/2023 23:10 WG2063135
Trichlorofluoromethane ND 0.00500 1 05/19/2023 23:10 WG2063135
1,2,3-Trichloropropane ND 0.00250 1 05/19/2023 23:10 WG2063135
1,2,4-Trimethylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,2,3-Trimethylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
1,3,5-Trimethylbenzene ND 0.00100 1 05/19/2023 23:10 WG2063135
Vinyl chloride ND 0.00100 1 05/19/2023 23:10 WG2063135
Xylenes, Total ND 0.00300 1 05/19/2023 23:10 WG2063135
(S) Toluene-d8 97.4 80.0-120 05/19/2023 23:10 WG2063135
(S) 4-Bromofluorobenzene 93.5 77.0-126 05/19/2023 23:10 WG2063135
(S) 1,2-Dichloroethane-d4 98.3 70.0-130 05/19/2023 23:10 WG2063135
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction ND 0.100 1 05/19/2023 09:49 WG2061651
(S) o-Terphenyl 107 31.0-160 05/19/2023 09:49 WG2061651
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1615666
MW-1
Collected date/time: 05/11/23 13:48
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Acenaphthylene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Anthracene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Benzidine ND J4 0.0105 1.05 05/17/2023 13:16 WG2060551
Benzo(a)anthracene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Benzo(b)fluoranthene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Benzo(k)fluoranthene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Benzo(g,h,i)perylene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Benzo(a)pyrene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Bis(2-chlorethoxy)methane ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Bis(2-chloroethyl)ether ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 05/17/2023 13:16 WG2060551
4-Bromophenyl-phenylether ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2-Chloronaphthalene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
4-Chlorophenyl-phenylether ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Chrysene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Dibenz(a,h)anthracene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
1,2-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
1,3-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
1,4-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
3,3-Dichlorobenzidine ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,4-Dinitrotoluene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,6-Dinitrotoluene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Fluoranthene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Fluorene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Hexachlorobenzene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Hexachloro-1,3-butadiene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Hexachlorocyclopentadiene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Hexachloroethane ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Isophorone ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Naphthalene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Nitrobenzene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
n-Nitrosodimethylamine ND 0.0105 1.05 05/17/2023 13:16 WG2060551
n-Nitrosodiphenylamine ND 0.0105 1.05 05/17/2023 13:16 WG2060551
n-Nitrosodi-n-propylamine ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Phenanthrene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
Benzylbutyl phthalate ND 0.00315 1.05 05/17/2023 13:16 WG2060551
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 05/17/2023 13:16 WG2060551
Di-n-butyl phthalate ND 0.00315 1.05 05/17/2023 13:16 WG2060551
Diethyl phthalate ND 0.00315 1.05 05/17/2023 13:16 WG2060551
Dimethyl phthalate ND 0.00315 1.05 05/17/2023 13:16 WG2060551
Di-n-octyl phthalate ND 0.00315 1.05 05/17/2023 13:16 WG2060551
Pyrene ND 0.00105 1.05 05/17/2023 13:16 WG2060551
1,2,4-Trichlorobenzene ND 0.0105 1.05 05/17/2023 13:16 WG2060551
4-Chloro-3-methylphenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2-Chlorophenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,4-Dichlorophenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,4-Dimethylphenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,4-Dinitrophenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2-Nitrophenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
4-Nitrophenol ND J4 0.0105 1.05 05/17/2023 13:16 WG2060551
Pentachlorophenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
Phenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
2,4,6-Trichlorophenol ND 0.0105 1.05 05/17/2023 13:16 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1615666
MW-1
Collected date/time: 05/11/23 13:48
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorophenol 35.4 10.0-120 05/17/2023 13:16 WG2060551
(S) Phenol-d5 26.2 10.0-120 05/17/2023 13:16 WG2060551
(S) Nitrobenzene-d5 88.0 10.0-127 05/17/2023 13:16 WG2060551
(S) 2-Fluorobiphenyl 64.1 10.0-130 05/17/2023 13:16 WG2060551
(S) 2,4,6-Tribromophenol 62.9 10.0-155 05/17/2023 13:16 WG2060551
(S) p-Terphenyl-d14 60.0 10.0-128 05/17/2023 13:16 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1615666
MW-2
Collected date/time: 05/11/23 12:56
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 635 J3 13.3 1 05/17/2023 09:52 WG2061054
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity,Bicarbonate 371 20.0 1 05/16/2023 11:24 WG2060591
Alkalinity,Carbonate ND 20.0 1 05/16/2023 11:24 WG2060591
Sample Narrative:
L1615666-02 WG2060591: Endpoint pH 4.5 Headspace
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ammonia Nitrogen 0.619 0.250 1 05/16/2023 09:46 WG2060350
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD ND 20.0 1 05/14/2023 16:07 WG2059721
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.93 T8 1 05/18/2023 09:04 WG2061250
Sample Narrative:
L1615666-02 WG2061250: 7.93 at 19.9C
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 119 1.00 1 05/13/2023 22:29 WG2059136
Nitrate as (N)8.82 Q 0.100 1 05/13/2023 22:29 WG2059136
Sulfate 46.9 5.00 1 05/13/2023 22:29 WG2059136
Sample Narrative:
L1615666-02 WG2059136: Anions rerun 1 day outside hold for Nitrate due to unreportable in-hold run
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TOC (Total Organic Carbon)2.74 B 1.00 1 05/17/2023 07:16 WG2060649
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/05/2023 11:52 WG2059827
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1615666
MW-2
Collected date/time: 05/11/23 12:56
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 21:45 WG2060110
Arsenic 0.0210 B 0.0100 1 05/18/2023 21:45 WG2060110
Beryllium ND 0.00200 1 05/18/2023 21:45 WG2060110
Cadmium ND 0.00200 1 05/18/2023 21:45 WG2060110
Calcium 138 1.00 1 05/18/2023 21:45 WG2060110
Chromium ND 0.0100 1 05/18/2023 21:45 WG2060110
Copper ND 0.0100 1 05/18/2023 21:45 WG2060110
Iron 0.338 0.100 1 05/18/2023 21:45 WG2060110
Lead ND 0.00600 1 05/18/2023 21:45 WG2060110
Magnesium 45.5 1.00 1 05/18/2023 21:45 WG2060110
Manganese 0.632 0.0100 1 05/18/2023 21:45 WG2060110
Nickel ND 0.0100 1 05/18/2023 21:45 WG2060110
Potassium 7.36 2.00 1 05/18/2023 21:45 WG2060110
Selenium ND 0.0100 1 05/18/2023 21:45 WG2060110
Silver ND 0.00500 1 05/18/2023 21:45 WG2060110
Sodium 50.6 3.00 1 05/18/2023 21:45 WG2060110
Thallium ND 0.0100 1 05/22/2023 15:22 WG2060110
Zinc ND 0.0500 1 05/18/2023 21:45 WG2060110
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 05/19/2023 02:07 WG2062721
(S) a,a,a-Trifluorotoluene(FID) 92.1 78.0-120 05/19/2023 02:07 WG2062721
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 05/19/2023 23:30 WG2063135
Acrolein ND 0.0500 1 05/19/2023 23:30 WG2063135
Acrylonitrile ND 0.0100 1 05/19/2023 23:30 WG2063135
Benzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Bromobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Bromodichloromethane ND 0.00100 1 05/19/2023 23:30 WG2063135
Bromoform ND 0.00100 1 05/19/2023 23:30 WG2063135
Bromomethane ND 0.00500 1 05/19/2023 23:30 WG2063135
n-Butylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
sec-Butylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
tert-Butylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Carbon tetrachloride ND 0.00100 1 05/19/2023 23:30 WG2063135
Chlorobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Chlorodibromomethane ND 0.00100 1 05/19/2023 23:30 WG2063135
Chloroethane ND 0.00500 1 05/19/2023 23:30 WG2063135
Chloroform ND 0.00500 1 05/19/2023 23:30 WG2063135
Chloromethane ND 0.00250 1 05/19/2023 23:30 WG2063135
2-Chlorotoluene ND 0.00100 1 05/19/2023 23:30 WG2063135
4-Chlorotoluene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,2-Dibromo-3-Chloropropane ND 0.00500 1 05/19/2023 23:30 WG2063135
1,2-Dibromoethane ND 0.00100 1 05/19/2023 23:30 WG2063135
Dibromomethane ND 0.00100 1 05/19/2023 23:30 WG2063135
1,2-Dichlorobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,3-Dichlorobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,4-Dichlorobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Dichlorodifluoromethane ND 0.00500 1 05/19/2023 23:30 WG2063135
1,1-Dichloroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1615666
MW-2
Collected date/time: 05/11/23 12:56
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1,2-Dichloroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1-Dichloroethene ND 0.00100 1 05/19/2023 23:30 WG2063135
cis-1,2-Dichloroethene ND 0.00100 1 05/19/2023 23:30 WG2063135
trans-1,2-Dichloroethene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,2-Dichloropropane ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1-Dichloropropene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,3-Dichloropropane ND 0.00100 1 05/19/2023 23:30 WG2063135
cis-1,3-Dichloropropene ND 0.00100 1 05/19/2023 23:30 WG2063135
trans-1,3-Dichloropropene ND 0.00100 1 05/19/2023 23:30 WG2063135
2,2-Dichloropropane ND 0.00100 1 05/19/2023 23:30 WG2063135
Di-isopropyl ether ND 0.00100 1 05/19/2023 23:30 WG2063135
Ethylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Hexachloro-1,3-butadiene ND 0.00100 1 05/19/2023 23:30 WG2063135
Isopropylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
p-Isopropyltoluene ND 0.00100 1 05/19/2023 23:30 WG2063135
2-Butanone (MEK)ND 0.0100 1 05/19/2023 23:30 WG2063135
Methylene Chloride ND 0.00500 1 05/19/2023 23:30 WG2063135
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 05/19/2023 23:30 WG2063135
Methyl tert-butyl ether ND 0.00100 1 05/19/2023 23:30 WG2063135
Naphthalene ND 0.00500 1 05/19/2023 23:30 WG2063135
n-Propylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Styrene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1,1,2-Tetrachloroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
Tetrachloroethene ND 0.00100 1 05/19/2023 23:30 WG2063135
Toluene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,2,3-Trichlorobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,2,4-Trichlorobenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1,1-Trichloroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
1,1,2-Trichloroethane ND 0.00100 1 05/19/2023 23:30 WG2063135
Trichloroethene ND 0.00100 1 05/19/2023 23:30 WG2063135
Trichlorofluoromethane ND 0.00500 1 05/19/2023 23:30 WG2063135
1,2,3-Trichloropropane ND 0.00250 1 05/19/2023 23:30 WG2063135
1,2,4-Trimethylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,2,3-Trimethylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
1,3,5-Trimethylbenzene ND 0.00100 1 05/19/2023 23:30 WG2063135
Vinyl chloride ND 0.00100 1 05/19/2023 23:30 WG2063135
Xylenes, Total ND 0.00300 1 05/19/2023 23:30 WG2063135
(S) Toluene-d8 99.2 80.0-120 05/19/2023 23:30 WG2063135
(S) 4-Bromofluorobenzene 89.2 77.0-126 05/19/2023 23:30 WG2063135
(S) 1,2-Dichloroethane-d4 100 70.0-130 05/19/2023 23:30 WG2063135
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction ND 0.100 1 05/19/2023 10:10 WG2061651
(S) o-Terphenyl 104 31.0-160 05/19/2023 10:10 WG2061651
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1615666
MW-2
Collected date/time: 05/11/23 12:56
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Acenaphthylene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Anthracene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Benzidine ND J4 0.0105 1.05 05/17/2023 13:37 WG2060551
Benzo(a)anthracene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Benzo(b)fluoranthene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Benzo(k)fluoranthene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Benzo(g,h,i)perylene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Benzo(a)pyrene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Bis(2-chlorethoxy)methane ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Bis(2-chloroethyl)ether ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 05/17/2023 13:37 WG2060551
4-Bromophenyl-phenylether ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2-Chloronaphthalene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
4-Chlorophenyl-phenylether ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Chrysene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Dibenz(a,h)anthracene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
1,2-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
1,3-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
1,4-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
3,3-Dichlorobenzidine ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,4-Dinitrotoluene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,6-Dinitrotoluene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Fluoranthene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Fluorene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Hexachlorobenzene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Hexachloro-1,3-butadiene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Hexachlorocyclopentadiene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Hexachloroethane ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Isophorone ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Naphthalene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Nitrobenzene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
n-Nitrosodimethylamine ND 0.0105 1.05 05/17/2023 13:37 WG2060551
n-Nitrosodiphenylamine ND 0.0105 1.05 05/17/2023 13:37 WG2060551
n-Nitrosodi-n-propylamine ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Phenanthrene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
Benzylbutyl phthalate ND 0.00315 1.05 05/17/2023 13:37 WG2060551
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 05/17/2023 13:37 WG2060551
Di-n-butyl phthalate ND 0.00315 1.05 05/17/2023 13:37 WG2060551
Diethyl phthalate ND 0.00315 1.05 05/17/2023 13:37 WG2060551
Dimethyl phthalate ND 0.00315 1.05 05/17/2023 13:37 WG2060551
Di-n-octyl phthalate ND 0.00315 1.05 05/17/2023 13:37 WG2060551
Pyrene ND 0.00105 1.05 05/17/2023 13:37 WG2060551
1,2,4-Trichlorobenzene ND 0.0105 1.05 05/17/2023 13:37 WG2060551
4-Chloro-3-methylphenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2-Chlorophenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,4-Dichlorophenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,4-Dimethylphenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,4-Dinitrophenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2-Nitrophenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
4-Nitrophenol ND J4 0.0105 1.05 05/17/2023 13:37 WG2060551
Pentachlorophenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
Phenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
2,4,6-Trichlorophenol ND 0.0105 1.05 05/17/2023 13:37 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1615666
MW-2
Collected date/time: 05/11/23 12:56
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorophenol 38.7 10.0-120 05/17/2023 13:37 WG2060551
(S) Phenol-d5 28.7 10.0-120 05/17/2023 13:37 WG2060551
(S) Nitrobenzene-d5 100 10.0-127 05/17/2023 13:37 WG2060551
(S) 2-Fluorobiphenyl 69.7 10.0-130 05/17/2023 13:37 WG2060551
(S) 2,4,6-Tribromophenol 64.8 10.0-155 05/17/2023 13:37 WG2060551
(S) p-Terphenyl-d14 64.4 10.0-128 05/17/2023 13:37 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1615666
MW-3
Collected date/time: 05/11/23 11:21
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 10600 200 1 05/17/2023 09:52 WG2061054
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity,Bicarbonate 461 20.0 1 05/19/2023 09:42 WG2062879
Alkalinity,Carbonate ND 20.0 1 05/19/2023 09:42 WG2062879
Sample Narrative:
L1615666-03 WG2062879: Endpoint pH 4.5 Headspace
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ammonia Nitrogen 1.27 0.250 1 05/16/2023 09:49 WG2060350
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 197 20.0 1 05/14/2023 16:08 WG2059721
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.65 T8 1 05/18/2023 09:04 WG2061250
Sample Narrative:
L1615666-03 WG2061250: 7.65 at 19.7C
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 271 10.0 10 05/14/2023 03:24 WG2059136
Nitrate as (N)ND Q 0.100 1 05/13/2023 22:42 WG2059136
Sulfate 11.9 5.00 1 05/13/2023 22:42 WG2059136
Sample Narrative:
L1615666-03 WG2059136: Anions rerun 1 day outside hold for Nitrate due to unreportable in-hold run
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TOC (Total Organic Carbon)73.3 1.00 1 05/17/2023 07:34 WG2060649
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/05/2023 11:55 WG2059827
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1615666
MW-3
Collected date/time: 05/11/23 11:21
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 21:31 WG2060110
Arsenic 0.596 O1 0.0100 1 05/18/2023 21:31 WG2060110
Beryllium ND 0.00200 1 05/18/2023 21:31 WG2060110
Cadmium ND 0.00200 1 05/18/2023 21:31 WG2060110
Calcium 153 V 1.00 1 05/18/2023 21:31 WG2060110
Chromium ND 0.0100 1 05/18/2023 21:31 WG2060110
Copper ND 0.0100 1 05/18/2023 21:31 WG2060110
Iron 5.97 0.100 1 05/18/2023 21:31 WG2060110
Lead ND 0.00600 1 05/18/2023 21:31 WG2060110
Magnesium 67.4 1.00 1 05/18/2023 21:31 WG2060110
Manganese 0.728 0.0100 1 05/18/2023 21:31 WG2060110
Nickel ND 0.0100 1 05/18/2023 21:31 WG2060110
Potassium 10.1 2.00 1 05/18/2023 21:31 WG2060110
Selenium ND 0.0100 1 05/18/2023 21:31 WG2060110
Silver ND 0.00500 1 05/18/2023 21:31 WG2060110
Sodium 110 3.00 1 05/18/2023 21:31 WG2060110
Thallium ND 0.0100 1 05/22/2023 15:25 WG2060110
Zinc ND 0.0500 1 05/18/2023 21:31 WG2060110
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 1.00 10 05/21/2023 15:52 WG2063582
(S) a,a,a-Trifluorotoluene(FID) 92.8 78.0-120 05/21/2023 15:52 WG2063582
Sample Narrative:
L1615666-03 WG2063582: Lowest possible dilution due to sample foaming.
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone 0.102 0.0500 1 05/19/2023 23:50 WG2063135
Acrolein ND 0.0500 1 05/19/2023 23:50 WG2063135
Acrylonitrile ND 0.0100 1 05/19/2023 23:50 WG2063135
Benzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Bromobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Bromodichloromethane ND 0.00100 1 05/19/2023 23:50 WG2063135
Bromoform ND 0.00100 1 05/19/2023 23:50 WG2063135
Bromomethane ND 0.00500 1 05/19/2023 23:50 WG2063135
n-Butylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
sec-Butylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
tert-Butylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Carbon tetrachloride ND 0.00100 1 05/19/2023 23:50 WG2063135
Chlorobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Chlorodibromomethane ND 0.00100 1 05/19/2023 23:50 WG2063135
Chloroethane ND 0.00500 1 05/19/2023 23:50 WG2063135
Chloroform ND 0.00500 1 05/19/2023 23:50 WG2063135
Chloromethane ND 0.00250 1 05/19/2023 23:50 WG2063135
2-Chlorotoluene ND 0.00100 1 05/19/2023 23:50 WG2063135
4-Chlorotoluene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,2-Dibromo-3-Chloropropane ND 0.00500 1 05/19/2023 23:50 WG2063135
1,2-Dibromoethane ND 0.00100 1 05/19/2023 23:50 WG2063135
Dibromomethane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,2-Dichlorobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,3-Dichlorobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1615666
MW-3
Collected date/time: 05/11/23 11:21
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1,4-Dichlorobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Dichlorodifluoromethane ND 0.00500 1 05/19/2023 23:50 WG2063135
1,1-Dichloroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,2-Dichloroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1-Dichloroethene ND 0.00100 1 05/19/2023 23:50 WG2063135
cis-1,2-Dichloroethene ND 0.00100 1 05/19/2023 23:50 WG2063135
trans-1,2-Dichloroethene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,2-Dichloropropane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1-Dichloropropene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,3-Dichloropropane ND 0.00100 1 05/19/2023 23:50 WG2063135
cis-1,3-Dichloropropene ND 0.00100 1 05/19/2023 23:50 WG2063135
trans-1,3-Dichloropropene ND 0.00100 1 05/19/2023 23:50 WG2063135
2,2-Dichloropropane ND 0.00100 1 05/19/2023 23:50 WG2063135
Di-isopropyl ether ND 0.00100 1 05/19/2023 23:50 WG2063135
Ethylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Hexachloro-1,3-butadiene ND 0.00100 1 05/19/2023 23:50 WG2063135
Isopropylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
p-Isopropyltoluene ND 0.00100 1 05/19/2023 23:50 WG2063135
2-Butanone (MEK)0.128 0.0100 1 05/19/2023 23:50 WG2063135
Methylene Chloride ND 0.00500 1 05/19/2023 23:50 WG2063135
4-Methyl-2-pentanone (MIBK) 0.192 0.0100 1 05/19/2023 23:50 WG2063135
Methyl tert-butyl ether ND 0.00100 1 05/19/2023 23:50 WG2063135
Naphthalene ND 0.00500 1 05/19/2023 23:50 WG2063135
n-Propylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Styrene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1,1,2-Tetrachloroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
Tetrachloroethene ND 0.00100 1 05/19/2023 23:50 WG2063135
Toluene 0.00584 0.00100 1 05/19/2023 23:50 WG2063135
1,2,3-Trichlorobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,2,4-Trichlorobenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1,1-Trichloroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
1,1,2-Trichloroethane ND 0.00100 1 05/19/2023 23:50 WG2063135
Trichloroethene ND 0.00100 1 05/19/2023 23:50 WG2063135
Trichlorofluoromethane ND 0.00500 1 05/19/2023 23:50 WG2063135
1,2,3-Trichloropropane ND 0.00250 1 05/19/2023 23:50 WG2063135
1,2,4-Trimethylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,2,3-Trimethylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
1,3,5-Trimethylbenzene ND 0.00100 1 05/19/2023 23:50 WG2063135
Vinyl chloride ND 0.00100 1 05/19/2023 23:50 WG2063135
Xylenes, Total ND 0.00300 1 05/19/2023 23:50 WG2063135
(S) Toluene-d8 99.7 80.0-120 05/19/2023 23:50 WG2063135
(S) 4-Bromofluorobenzene 91.6 77.0-126 05/19/2023 23:50 WG2063135
(S) 1,2-Dichloroethane-d4 99.3 70.0-130 05/19/2023 23:50 WG2063135
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 1.80 0.100 1 05/19/2023 17:44 WG2061651
(S) o-Terphenyl 125 31.0-160 05/19/2023 17:44 WG2061651
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1615666
MW-3
Collected date/time: 05/11/23 11:21
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Acenaphthylene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Anthracene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Benzidine ND J4 0.0105 1.05 05/17/2023 13:59 WG2060551
Benzo(a)anthracene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Benzo(b)fluoranthene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Benzo(k)fluoranthene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Benzo(g,h,i)perylene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Benzo(a)pyrene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Bis(2-chlorethoxy)methane ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Bis(2-chloroethyl)ether ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 05/17/2023 13:59 WG2060551
4-Bromophenyl-phenylether ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2-Chloronaphthalene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
4-Chlorophenyl-phenylether ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Chrysene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Dibenz(a,h)anthracene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
1,2-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
1,3-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
1,4-Dichlorobenzene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
3,3-Dichlorobenzidine ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2,4-Dinitrotoluene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2,6-Dinitrotoluene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Fluoranthene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Fluorene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Hexachlorobenzene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Hexachloro-1,3-butadiene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Hexachlorocyclopentadiene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Hexachloroethane ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Isophorone ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Naphthalene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Nitrobenzene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
n-Nitrosodimethylamine ND 0.0105 1.05 05/17/2023 13:59 WG2060551
n-Nitrosodiphenylamine ND 0.0105 1.05 05/17/2023 13:59 WG2060551
n-Nitrosodi-n-propylamine ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Phenanthrene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
Benzylbutyl phthalate ND 0.00315 1.05 05/17/2023 13:59 WG2060551
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 05/17/2023 13:59 WG2060551
Di-n-butyl phthalate ND 0.00315 1.05 05/17/2023 13:59 WG2060551
Diethyl phthalate ND 0.00315 1.05 05/17/2023 13:59 WG2060551
Dimethyl phthalate ND 0.00315 1.05 05/17/2023 13:59 WG2060551
Di-n-octyl phthalate ND 0.00315 1.05 05/17/2023 13:59 WG2060551
Pyrene ND 0.00105 1.05 05/17/2023 13:59 WG2060551
1,2,4-Trichlorobenzene ND 0.0105 1.05 05/17/2023 13:59 WG2060551
4-Chloro-3-methylphenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2-Chlorophenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2,4-Dichlorophenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2,4-Dimethylphenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2,4-Dinitrophenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
2-Nitrophenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
4-Nitrophenol ND J4 0.0105 1.05 05/17/2023 13:59 WG2060551
Pentachlorophenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
Phenol 0.0253 0.0105 1.05 05/17/2023 13:59 WG2060551
2,4,6-Trichlorophenol ND 0.0105 1.05 05/17/2023 13:59 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1615666
MW-3
Collected date/time: 05/11/23 11:21
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorophenol 33.4 10.0-120 05/17/2023 13:59 WG2060551
(S) Phenol-d5 28.8 10.0-120 05/17/2023 13:59 WG2060551
(S) Nitrobenzene-d5 88.4 10.0-127 05/17/2023 13:59 WG2060551
(S) 2-Fluorobiphenyl 62.6 10.0-130 05/17/2023 13:59 WG2060551
(S) 2,4,6-Tribromophenol 71.0 10.0-155 05/17/2023 13:59 WG2060551
(S) p-Terphenyl-d14 62.3 10.0-128 05/17/2023 13:59 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1615666
MW-4
Collected date/time: 05/11/23 12:10
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 1250 25.0 1 05/17/2023 09:52 WG2061054
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity,Bicarbonate 414 20.0 1 05/18/2023 12:24 WG2062106
Alkalinity,Carbonate ND 20.0 1 05/18/2023 12:24 WG2062106
Sample Narrative:
L1615666-04 WG2062106: Endpoint pH 4.5 Headspace
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ammonia Nitrogen ND 0.250 1 05/16/2023 09:51 WG2060350
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD ND 20.0 1 05/14/2023 16:08 WG2059721
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.66 T8 1 05/18/2023 09:04 WG2061250
Sample Narrative:
L1615666-04 WG2061250: 7.66 at 19.9C
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 430 10.0 10 05/14/2023 03:37 WG2059136
Nitrate as (N)2.42 Q 0.100 1 05/13/2023 22:55 WG2059136
Sulfate 90.7 5.00 1 05/13/2023 22:55 WG2059136
Sample Narrative:
L1615666-04 WG2059136: Anions rerun 1 day outside hold for Nitrate due to unreportable in-hold run
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TOC (Total Organic Carbon)3.16 B 1.00 1 05/17/2023 07:52 WG2060649
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/05/2023 11:57 WG2059827
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1615666
MW-4
Collected date/time: 05/11/23 12:10
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 21:47 WG2060110
Arsenic ND 0.0100 1 05/18/2023 21:47 WG2060110
Beryllium ND 0.00200 1 05/18/2023 21:47 WG2060110
Cadmium ND 0.00200 1 05/18/2023 21:47 WG2060110
Calcium 176 1.00 1 05/18/2023 21:47 WG2060110
Chromium ND 0.0100 1 05/18/2023 21:47 WG2060110
Copper ND 0.0100 1 05/18/2023 21:47 WG2060110
Iron 1.15 0.100 1 05/18/2023 21:47 WG2060110
Lead ND 0.00600 1 05/18/2023 21:47 WG2060110
Magnesium 61.7 1.00 1 05/18/2023 21:47 WG2060110
Manganese 0.933 0.0100 1 05/18/2023 21:47 WG2060110
Nickel 0.0110 B 0.0100 1 05/18/2023 21:47 WG2060110
Potassium 8.03 2.00 1 05/18/2023 21:47 WG2060110
Selenium ND 0.0100 1 05/18/2023 21:47 WG2060110
Silver ND 0.00500 1 05/18/2023 21:47 WG2060110
Sodium 252 3.00 1 05/18/2023 21:47 WG2060110
Thallium ND 0.0100 1 05/18/2023 21:47 WG2060110
Zinc ND 0.0500 1 05/18/2023 21:47 WG2060110
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 05/19/2023 02:29 WG2062721
(S) a,a,a-Trifluorotoluene(FID) 92.2 78.0-120 05/19/2023 02:29 WG2062721
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 05/20/2023 00:09 WG2063135
Acrolein ND 0.0500 1 05/20/2023 00:09 WG2063135
Acrylonitrile ND 0.0100 1 05/20/2023 00:09 WG2063135
Benzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Bromobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Bromodichloromethane ND 0.00100 1 05/20/2023 00:09 WG2063135
Bromoform ND 0.00100 1 05/20/2023 00:09 WG2063135
Bromomethane ND 0.00500 1 05/20/2023 00:09 WG2063135
n-Butylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
sec-Butylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
tert-Butylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Carbon tetrachloride ND 0.00100 1 05/20/2023 00:09 WG2063135
Chlorobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Chlorodibromomethane ND 0.00100 1 05/20/2023 00:09 WG2063135
Chloroethane ND 0.00500 1 05/20/2023 00:09 WG2063135
Chloroform ND 0.00500 1 05/20/2023 00:09 WG2063135
Chloromethane ND 0.00250 1 05/20/2023 00:09 WG2063135
2-Chlorotoluene ND 0.00100 1 05/20/2023 00:09 WG2063135
4-Chlorotoluene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,2-Dibromo-3-Chloropropane ND 0.00500 1 05/20/2023 00:09 WG2063135
1,2-Dibromoethane ND 0.00100 1 05/20/2023 00:09 WG2063135
Dibromomethane ND 0.00100 1 05/20/2023 00:09 WG2063135
1,2-Dichlorobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,3-Dichlorobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,4-Dichlorobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Dichlorodifluoromethane ND 0.00500 1 05/20/2023 00:09 WG2063135
1,1-Dichloroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1615666
MW-4
Collected date/time: 05/11/23 12:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1,2-Dichloroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1-Dichloroethene ND 0.00100 1 05/20/2023 00:09 WG2063135
cis-1,2-Dichloroethene ND 0.00100 1 05/20/2023 00:09 WG2063135
trans-1,2-Dichloroethene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,2-Dichloropropane ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1-Dichloropropene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,3-Dichloropropane ND 0.00100 1 05/20/2023 00:09 WG2063135
cis-1,3-Dichloropropene ND 0.00100 1 05/20/2023 00:09 WG2063135
trans-1,3-Dichloropropene ND 0.00100 1 05/20/2023 00:09 WG2063135
2,2-Dichloropropane ND 0.00100 1 05/20/2023 00:09 WG2063135
Di-isopropyl ether ND 0.00100 1 05/20/2023 00:09 WG2063135
Ethylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Hexachloro-1,3-butadiene ND 0.00100 1 05/20/2023 00:09 WG2063135
Isopropylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
p-Isopropyltoluene ND 0.00100 1 05/20/2023 00:09 WG2063135
2-Butanone (MEK)ND 0.0100 1 05/20/2023 00:09 WG2063135
Methylene Chloride ND 0.00500 1 05/20/2023 00:09 WG2063135
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 05/20/2023 00:09 WG2063135
Methyl tert-butyl ether ND 0.00100 1 05/20/2023 00:09 WG2063135
Naphthalene ND 0.00500 1 05/20/2023 00:09 WG2063135
n-Propylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Styrene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1,1,2-Tetrachloroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
Tetrachloroethene ND 0.00100 1 05/20/2023 00:09 WG2063135
Toluene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,2,3-Trichlorobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,2,4-Trichlorobenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1,1-Trichloroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
1,1,2-Trichloroethane ND 0.00100 1 05/20/2023 00:09 WG2063135
Trichloroethene ND 0.00100 1 05/20/2023 00:09 WG2063135
Trichlorofluoromethane ND 0.00500 1 05/20/2023 00:09 WG2063135
1,2,3-Trichloropropane ND 0.00250 1 05/20/2023 00:09 WG2063135
1,2,4-Trimethylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,2,3-Trimethylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
1,3,5-Trimethylbenzene ND 0.00100 1 05/20/2023 00:09 WG2063135
Vinyl chloride ND 0.00100 1 05/20/2023 00:09 WG2063135
Xylenes, Total ND 0.00300 1 05/20/2023 00:09 WG2063135
(S) Toluene-d8 97.4 80.0-120 05/20/2023 00:09 WG2063135
(S) 4-Bromofluorobenzene 94.2 77.0-126 05/20/2023 00:09 WG2063135
(S) 1,2-Dichloroethane-d4 102 70.0-130 05/20/2023 00:09 WG2063135
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction ND 0.100 1 05/19/2023 18:05 WG2061651
(S) o-Terphenyl 107 31.0-160 05/19/2023 18:05 WG2061651
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1615666
MW-4
Collected date/time: 05/11/23 12:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Acenaphthylene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Anthracene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Benzidine ND J4 0.0105 1.05 05/17/2023 14:20 WG2060551
Benzo(a)anthracene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Benzo(b)fluoranthene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Benzo(k)fluoranthene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Benzo(g,h,i)perylene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Benzo(a)pyrene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Bis(2-chlorethoxy)methane ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Bis(2-chloroethyl)ether ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 05/17/2023 14:20 WG2060551
4-Bromophenyl-phenylether ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2-Chloronaphthalene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
4-Chlorophenyl-phenylether ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Chrysene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Dibenz(a,h)anthracene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
1,2-Dichlorobenzene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
1,3-Dichlorobenzene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
1,4-Dichlorobenzene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
3,3-Dichlorobenzidine ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,4-Dinitrotoluene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,6-Dinitrotoluene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Fluoranthene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Fluorene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Hexachlorobenzene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Hexachloro-1,3-butadiene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Hexachlorocyclopentadiene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Hexachloroethane ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Isophorone ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Naphthalene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Nitrobenzene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
n-Nitrosodimethylamine ND 0.0105 1.05 05/17/2023 14:20 WG2060551
n-Nitrosodiphenylamine ND 0.0105 1.05 05/17/2023 14:20 WG2060551
n-Nitrosodi-n-propylamine ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Phenanthrene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
Benzylbutyl phthalate ND 0.00315 1.05 05/17/2023 14:20 WG2060551
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 05/17/2023 14:20 WG2060551
Di-n-butyl phthalate ND 0.00315 1.05 05/17/2023 14:20 WG2060551
Diethyl phthalate ND 0.00315 1.05 05/17/2023 14:20 WG2060551
Dimethyl phthalate ND 0.00315 1.05 05/17/2023 14:20 WG2060551
Di-n-octyl phthalate ND 0.00315 1.05 05/17/2023 14:20 WG2060551
Pyrene ND 0.00105 1.05 05/17/2023 14:20 WG2060551
1,2,4-Trichlorobenzene ND 0.0105 1.05 05/17/2023 14:20 WG2060551
4-Chloro-3-methylphenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2-Chlorophenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,4-Dichlorophenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,4-Dimethylphenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,4-Dinitrophenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2-Nitrophenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
4-Nitrophenol ND J4 0.0105 1.05 05/17/2023 14:20 WG2060551
Pentachlorophenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
Phenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
2,4,6-Trichlorophenol ND 0.0105 1.05 05/17/2023 14:20 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1615666
MW-4
Collected date/time: 05/11/23 12:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorophenol 26.0 10.0-120 05/17/2023 14:20 WG2060551
(S) Phenol-d5 20.4 10.0-120 05/17/2023 14:20 WG2060551
(S) Nitrobenzene-d5 74.0 10.0-127 05/17/2023 14:20 WG2060551
(S) 2-Fluorobiphenyl 53.7 10.0-130 05/17/2023 14:20 WG2060551
(S) 2,4,6-Tribromophenol 49.0 10.0-155 05/17/2023 14:20 WG2060551
(S) p-Terphenyl-d14 55.3 10.0-128 05/17/2023 14:20 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1615666
MW-5
Collected date/time: 05/11/23 14:50
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 894 20.0 1 05/17/2023 09:52 WG2061054
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity,Bicarbonate 217 20.0 1 05/19/2023 09:47 WG2062879
Alkalinity,Carbonate ND 20.0 1 05/19/2023 09:47 WG2062879
Sample Narrative:
L1615666-05 WG2062879: Endpoint pH 4.5 Headspace
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ammonia Nitrogen ND 0.250 1 05/16/2023 09:52 WG2060350
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 25.7 20.0 1 05/14/2023 16:08 WG2059721
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.99 T8 1 05/18/2023 09:04 WG2061250
Sample Narrative:
L1615666-05 WG2061250: 7.99 at 19.9C
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 320 10.0 10 05/14/2023 03:50 WG2059136
Nitrate as (N)0.192 Q 0.100 1 05/13/2023 23:08 WG2059136
Sulfate 95.2 5.00 1 05/13/2023 23:08 WG2059136
Sample Narrative:
L1615666-05 WG2059136: Anions rerun 1 day outside hold for Nitrate due to unreportable in-hold run
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TOC (Total Organic Carbon)7.73 1.00 1 05/17/2023 08:51 WG2060649
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/05/2023 11:59 WG2059827
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1615666
MW-5
Collected date/time: 05/11/23 14:50
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 21:50 WG2060110
Arsenic 0.0293 B 0.0100 1 05/18/2023 21:50 WG2060110
Beryllium ND 0.00200 1 05/18/2023 21:50 WG2060110
Cadmium ND 0.00200 1 05/18/2023 21:50 WG2060110
Calcium 63.0 1.00 1 05/18/2023 21:50 WG2060110
Chromium ND 0.0100 1 05/18/2023 21:50 WG2060110
Copper ND 0.0100 1 05/18/2023 21:50 WG2060110
Iron 0.115 0.100 1 05/18/2023 21:50 WG2060110
Lead ND 0.00600 1 05/18/2023 21:50 WG2060110
Magnesium 40.0 1.00 1 05/18/2023 21:50 WG2060110
Manganese 0.405 0.0100 1 05/18/2023 21:50 WG2060110
Nickel ND 0.0100 1 05/18/2023 21:50 WG2060110
Potassium 21.5 2.00 1 05/18/2023 21:50 WG2060110
Selenium ND 0.0100 1 05/18/2023 21:50 WG2060110
Silver ND 0.00500 1 05/18/2023 21:50 WG2060110
Sodium 207 3.00 1 05/18/2023 21:50 WG2060110
Thallium ND 0.0100 1 05/18/2023 21:50 WG2060110
Zinc ND 0.0500 1 05/18/2023 21:50 WG2060110
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.500 5 05/19/2023 17:43 WG2063048
(S) a,a,a-Trifluorotoluene(FID) 93.8 78.0-120 05/19/2023 17:43 WG2063048
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 05/20/2023 00:29 WG2063135
Acrolein ND 0.0500 1 05/20/2023 00:29 WG2063135
Acrylonitrile ND 0.0100 1 05/20/2023 00:29 WG2063135
Benzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Bromobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Bromodichloromethane ND 0.00100 1 05/20/2023 00:29 WG2063135
Bromoform ND 0.00100 1 05/20/2023 00:29 WG2063135
Bromomethane ND 0.00500 1 05/20/2023 00:29 WG2063135
n-Butylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
sec-Butylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
tert-Butylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Carbon tetrachloride ND 0.00100 1 05/20/2023 00:29 WG2063135
Chlorobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Chlorodibromomethane ND 0.00100 1 05/20/2023 00:29 WG2063135
Chloroethane ND 0.00500 1 05/20/2023 00:29 WG2063135
Chloroform ND 0.00500 1 05/20/2023 00:29 WG2063135
Chloromethane ND 0.00250 1 05/20/2023 00:29 WG2063135
2-Chlorotoluene ND 0.00100 1 05/20/2023 00:29 WG2063135
4-Chlorotoluene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,2-Dibromo-3-Chloropropane ND 0.00500 1 05/20/2023 00:29 WG2063135
1,2-Dibromoethane ND 0.00100 1 05/20/2023 00:29 WG2063135
Dibromomethane ND 0.00100 1 05/20/2023 00:29 WG2063135
1,2-Dichlorobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,3-Dichlorobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,4-Dichlorobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Dichlorodifluoromethane ND 0.00500 1 05/20/2023 00:29 WG2063135
1,1-Dichloroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1615666
MW-5
Collected date/time: 05/11/23 14:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1,2-Dichloroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1-Dichloroethene ND 0.00100 1 05/20/2023 00:29 WG2063135
cis-1,2-Dichloroethene ND 0.00100 1 05/20/2023 00:29 WG2063135
trans-1,2-Dichloroethene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,2-Dichloropropane ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1-Dichloropropene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,3-Dichloropropane ND 0.00100 1 05/20/2023 00:29 WG2063135
cis-1,3-Dichloropropene ND 0.00100 1 05/20/2023 00:29 WG2063135
trans-1,3-Dichloropropene ND 0.00100 1 05/20/2023 00:29 WG2063135
2,2-Dichloropropane ND 0.00100 1 05/20/2023 00:29 WG2063135
Di-isopropyl ether ND 0.00100 1 05/20/2023 00:29 WG2063135
Ethylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Hexachloro-1,3-butadiene ND 0.00100 1 05/20/2023 00:29 WG2063135
Isopropylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
p-Isopropyltoluene ND 0.00100 1 05/20/2023 00:29 WG2063135
2-Butanone (MEK)ND 0.0100 1 05/20/2023 00:29 WG2063135
Methylene Chloride ND 0.00500 1 05/20/2023 00:29 WG2063135
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 05/20/2023 00:29 WG2063135
Methyl tert-butyl ether ND 0.00100 1 05/20/2023 00:29 WG2063135
Naphthalene ND 0.00500 1 05/20/2023 00:29 WG2063135
n-Propylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Styrene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1,1,2-Tetrachloroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
Tetrachloroethene ND 0.00100 1 05/20/2023 00:29 WG2063135
Toluene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,2,3-Trichlorobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,2,4-Trichlorobenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1,1-Trichloroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
1,1,2-Trichloroethane ND 0.00100 1 05/20/2023 00:29 WG2063135
Trichloroethene ND 0.00100 1 05/20/2023 00:29 WG2063135
Trichlorofluoromethane ND 0.00500 1 05/20/2023 00:29 WG2063135
1,2,3-Trichloropropane ND 0.00250 1 05/20/2023 00:29 WG2063135
1,2,4-Trimethylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,2,3-Trimethylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
1,3,5-Trimethylbenzene ND 0.00100 1 05/20/2023 00:29 WG2063135
Vinyl chloride ND 0.00100 1 05/20/2023 00:29 WG2063135
Xylenes, Total ND 0.00300 1 05/20/2023 00:29 WG2063135
(S) Toluene-d8 99.1 80.0-120 05/20/2023 00:29 WG2063135
(S) 4-Bromofluorobenzene 92.9 77.0-126 05/20/2023 00:29 WG2063135
(S) 1,2-Dichloroethane-d4 99.6 70.0-130 05/20/2023 00:29 WG2063135
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 0.338 0.100 1 05/19/2023 10:30 WG2061651
(S) o-Terphenyl 121 31.0-160 05/19/2023 10:30 WG2061651
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1615666
MW-5
Collected date/time: 05/11/23 14:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Acenaphthylene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Anthracene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Benzidine ND J4 0.0105 1.05 05/17/2023 15:24 WG2060551
Benzo(a)anthracene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Benzo(b)fluoranthene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Benzo(k)fluoranthene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Benzo(g,h,i)perylene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Benzo(a)pyrene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Bis(2-chlorethoxy)methane ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Bis(2-chloroethyl)ether ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,2-Oxybis(1-Chloropropane) ND 0.0105 1.05 05/17/2023 15:24 WG2060551
4-Bromophenyl-phenylether ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2-Chloronaphthalene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
4-Chlorophenyl-phenylether ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Chrysene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Dibenz(a,h)anthracene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
1,2-Dichlorobenzene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
1,3-Dichlorobenzene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
1,4-Dichlorobenzene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
3,3-Dichlorobenzidine ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,4-Dinitrotoluene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,6-Dinitrotoluene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Fluoranthene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Fluorene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Hexachlorobenzene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Hexachloro-1,3-butadiene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Hexachlorocyclopentadiene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Hexachloroethane ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Indeno(1,2,3-cd)pyrene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Isophorone ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Naphthalene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Nitrobenzene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
n-Nitrosodimethylamine ND 0.0105 1.05 05/17/2023 15:24 WG2060551
n-Nitrosodiphenylamine ND 0.0105 1.05 05/17/2023 15:24 WG2060551
n-Nitrosodi-n-propylamine ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Phenanthrene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
Benzylbutyl phthalate ND 0.00315 1.05 05/17/2023 15:24 WG2060551
Bis(2-ethylhexyl)phthalate ND 0.00315 1.05 05/17/2023 15:24 WG2060551
Di-n-butyl phthalate ND 0.00315 1.05 05/17/2023 15:24 WG2060551
Diethyl phthalate ND 0.00315 1.05 05/17/2023 15:24 WG2060551
Dimethyl phthalate ND 0.00315 1.05 05/17/2023 15:24 WG2060551
Di-n-octyl phthalate ND 0.00315 1.05 05/17/2023 15:24 WG2060551
Pyrene ND 0.00105 1.05 05/17/2023 15:24 WG2060551
1,2,4-Trichlorobenzene ND 0.0105 1.05 05/17/2023 15:24 WG2060551
4-Chloro-3-methylphenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2-Chlorophenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,4-Dichlorophenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,4-Dimethylphenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
4,6-Dinitro-2-methylphenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,4-Dinitrophenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2-Nitrophenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
4-Nitrophenol ND J4 0.0105 1.05 05/17/2023 15:24 WG2060551
Pentachlorophenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
Phenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
2,4,6-Trichlorophenol ND 0.0105 1.05 05/17/2023 15:24 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1615666
MW-5
Collected date/time: 05/11/23 14:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorophenol 36.4 10.0-120 05/17/2023 15:24 WG2060551
(S) Phenol-d5 28.4 10.0-120 05/17/2023 15:24 WG2060551
(S) Nitrobenzene-d5 90.2 10.0-127 05/17/2023 15:24 WG2060551
(S) 2-Fluorobiphenyl 65.9 10.0-130 05/17/2023 15:24 WG2060551
(S) 2,4,6-Tribromophenol 66.2 10.0-155 05/17/2023 15:24 WG2060551
(S) p-Terphenyl-d14 63.6 10.0-128 05/17/2023 15:24 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1615666
MW-6
Collected date/time: 05/11/23 10:40
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 830 20.0 1 05/17/2023 09:52 WG2061054
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity,Bicarbonate 347 20.0 1 05/19/2023 09:50 WG2062879
Alkalinity,Carbonate ND 20.0 1 05/19/2023 09:50 WG2062879
Sample Narrative:
L1615666-06 WG2062879: Endpoint pH 4.5 Headspace
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ammonia Nitrogen 0.701 0.250 1 05/16/2023 09:58 WG2060350
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 20.8 20.0 1 05/14/2023 16:09 WG2059721
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.65 T8 1 05/18/2023 09:04 WG2061250
Sample Narrative:
L1615666-06 WG2061250: 7.65 at 19.8C
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 238 10.0 10 05/14/2023 04:03 WG2059136
Nitrate as (N)5.19 Q 0.100 1 05/13/2023 23:21 WG2059136
Sulfate 77.6 5.00 1 05/13/2023 23:21 WG2059136
Sample Narrative:
L1615666-06 WG2059136: Anions rerun 1 day outside hold for Nitrate due to unreportable in-hold run
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TOC (Total Organic Carbon)5.59 1.00 1 05/17/2023 09:26 WG2060649
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:14 WG2059828
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1615666
MW-6
Collected date/time: 05/11/23 10:40
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 21:58 WG2060110
Arsenic ND 0.0100 1 05/18/2023 21:58 WG2060110
Beryllium ND 0.00200 1 05/18/2023 21:58 WG2060110
Cadmium ND 0.00200 1 05/18/2023 21:58 WG2060110
Calcium 175 1.00 1 05/18/2023 21:58 WG2060110
Chromium ND 0.0100 1 05/18/2023 21:58 WG2060110
Copper ND 0.0100 1 05/18/2023 21:58 WG2060110
Iron 1.54 0.100 1 05/18/2023 21:58 WG2060110
Lead ND 0.00600 1 05/18/2023 21:58 WG2060110
Magnesium 58.0 1.00 1 05/18/2023 21:58 WG2060110
Manganese 0.440 0.0100 1 05/18/2023 21:58 WG2060110
Nickel ND 0.0100 1 05/18/2023 21:58 WG2060110
Potassium 10.3 2.00 1 05/18/2023 21:58 WG2060110
Selenium ND 0.0100 1 05/18/2023 21:58 WG2060110
Silver ND 0.00500 1 05/18/2023 21:58 WG2060110
Sodium 94.5 3.00 1 05/18/2023 21:58 WG2060110
Thallium ND 0.0100 1 05/18/2023 21:58 WG2060110
Zinc ND 0.0500 1 05/18/2023 21:58 WG2060110
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.500 5 05/19/2023 18:01 WG2063048
(S) a,a,a-Trifluorotoluene(FID) 96.4 78.0-120 05/19/2023 18:01 WG2063048
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 05/20/2023 00:49 WG2063135
Acrolein ND 0.0500 1 05/20/2023 00:49 WG2063135
Acrylonitrile ND 0.0100 1 05/20/2023 00:49 WG2063135
Benzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Bromobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Bromodichloromethane ND 0.00100 1 05/20/2023 00:49 WG2063135
Bromoform ND 0.00100 1 05/20/2023 00:49 WG2063135
Bromomethane ND 0.00500 1 05/20/2023 00:49 WG2063135
n-Butylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
sec-Butylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
tert-Butylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Carbon tetrachloride ND 0.00100 1 05/20/2023 00:49 WG2063135
Chlorobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Chlorodibromomethane ND 0.00100 1 05/20/2023 00:49 WG2063135
Chloroethane ND 0.00500 1 05/20/2023 00:49 WG2063135
Chloroform ND 0.00500 1 05/20/2023 00:49 WG2063135
Chloromethane ND 0.00250 1 05/20/2023 00:49 WG2063135
2-Chlorotoluene ND 0.00100 1 05/20/2023 00:49 WG2063135
4-Chlorotoluene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,2-Dibromo-3-Chloropropane ND 0.00500 1 05/20/2023 00:49 WG2063135
1,2-Dibromoethane ND 0.00100 1 05/20/2023 00:49 WG2063135
Dibromomethane ND 0.00100 1 05/20/2023 00:49 WG2063135
1,2-Dichlorobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,3-Dichlorobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,4-Dichlorobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Dichlorodifluoromethane ND 0.00500 1 05/20/2023 00:49 WG2063135
1,1-Dichloroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1615666
MW-6
Collected date/time: 05/11/23 10:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1,2-Dichloroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1-Dichloroethene ND 0.00100 1 05/20/2023 00:49 WG2063135
cis-1,2-Dichloroethene ND 0.00100 1 05/20/2023 00:49 WG2063135
trans-1,2-Dichloroethene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,2-Dichloropropane ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1-Dichloropropene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,3-Dichloropropane ND 0.00100 1 05/20/2023 00:49 WG2063135
cis-1,3-Dichloropropene ND 0.00100 1 05/20/2023 00:49 WG2063135
trans-1,3-Dichloropropene ND 0.00100 1 05/20/2023 00:49 WG2063135
2,2-Dichloropropane ND 0.00100 1 05/20/2023 00:49 WG2063135
Di-isopropyl ether ND 0.00100 1 05/20/2023 00:49 WG2063135
Ethylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Hexachloro-1,3-butadiene ND 0.00100 1 05/20/2023 00:49 WG2063135
Isopropylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
p-Isopropyltoluene ND 0.00100 1 05/20/2023 00:49 WG2063135
2-Butanone (MEK)ND 0.0100 1 05/20/2023 00:49 WG2063135
Methylene Chloride ND 0.00500 1 05/20/2023 00:49 WG2063135
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 05/20/2023 00:49 WG2063135
Methyl tert-butyl ether ND 0.00100 1 05/20/2023 00:49 WG2063135
Naphthalene ND 0.00500 1 05/20/2023 00:49 WG2063135
n-Propylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Styrene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1,1,2-Tetrachloroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
Tetrachloroethene ND 0.00100 1 05/20/2023 00:49 WG2063135
Toluene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,2,3-Trichlorobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,2,4-Trichlorobenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1,1-Trichloroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
1,1,2-Trichloroethane ND 0.00100 1 05/20/2023 00:49 WG2063135
Trichloroethene ND 0.00100 1 05/20/2023 00:49 WG2063135
Trichlorofluoromethane ND 0.00500 1 05/20/2023 00:49 WG2063135
1,2,3-Trichloropropane ND 0.00250 1 05/20/2023 00:49 WG2063135
1,2,4-Trimethylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,2,3-Trimethylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
1,3,5-Trimethylbenzene ND 0.00100 1 05/20/2023 00:49 WG2063135
Vinyl chloride ND 0.00100 1 05/20/2023 00:49 WG2063135
Xylenes, Total ND 0.00300 1 05/20/2023 00:49 WG2063135
(S) Toluene-d8 100 80.0-120 05/20/2023 00:49 WG2063135
(S) 4-Bromofluorobenzene 97.2 77.0-126 05/20/2023 00:49 WG2063135
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 05/20/2023 00:49 WG2063135
Semi-Volatile Organic Compounds (GC) by Method 3511/8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) High Fraction 0.797 0.100 1 05/19/2023 10:51 WG2061651
(S) o-Terphenyl 127 31.0-160 05/19/2023 10:51 WG2061651
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1615666
MW-6
Collected date/time: 05/11/23 10:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 05/17/2023 15:45 WG2060551
Acenaphthylene ND 0.00100 1 05/17/2023 15:45 WG2060551
Anthracene ND 0.00100 1 05/17/2023 15:45 WG2060551
Benzidine ND J4 0.0100 1 05/17/2023 15:45 WG2060551
Benzo(a)anthracene ND 0.00100 1 05/17/2023 15:45 WG2060551
Benzo(b)fluoranthene ND 0.00100 1 05/17/2023 15:45 WG2060551
Benzo(k)fluoranthene ND 0.00100 1 05/17/2023 15:45 WG2060551
Benzo(g,h,i)perylene ND 0.00100 1 05/17/2023 15:45 WG2060551
Benzo(a)pyrene ND 0.00100 1 05/17/2023 15:45 WG2060551
Bis(2-chlorethoxy)methane ND 0.0100 1 05/17/2023 15:45 WG2060551
Bis(2-chloroethyl)ether ND 0.0100 1 05/17/2023 15:45 WG2060551
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 05/17/2023 15:45 WG2060551
4-Bromophenyl-phenylether ND 0.0100 1 05/17/2023 15:45 WG2060551
2-Chloronaphthalene ND 0.00100 1 05/17/2023 15:45 WG2060551
4-Chlorophenyl-phenylether ND 0.0100 1 05/17/2023 15:45 WG2060551
Chrysene ND 0.00100 1 05/17/2023 15:45 WG2060551
Dibenz(a,h)anthracene ND 0.00100 1 05/17/2023 15:45 WG2060551
1,2-Dichlorobenzene ND 0.0100 1 05/17/2023 15:45 WG2060551
1,3-Dichlorobenzene ND 0.0100 1 05/17/2023 15:45 WG2060551
1,4-Dichlorobenzene ND 0.0100 1 05/17/2023 15:45 WG2060551
3,3-Dichlorobenzidine ND 0.0100 1 05/17/2023 15:45 WG2060551
2,4-Dinitrotoluene ND 0.0100 1 05/17/2023 15:45 WG2060551
2,6-Dinitrotoluene ND 0.0100 1 05/17/2023 15:45 WG2060551
Fluoranthene ND 0.00100 1 05/17/2023 15:45 WG2060551
Fluorene ND 0.00100 1 05/17/2023 15:45 WG2060551
Hexachlorobenzene ND 0.00100 1 05/17/2023 15:45 WG2060551
Hexachloro-1,3-butadiene ND 0.0100 1 05/17/2023 15:45 WG2060551
Hexachlorocyclopentadiene ND 0.0100 1 05/17/2023 15:45 WG2060551
Hexachloroethane ND 0.0100 1 05/17/2023 15:45 WG2060551
Indeno(1,2,3-cd)pyrene ND 0.00100 1 05/17/2023 15:45 WG2060551
Isophorone ND 0.0100 1 05/17/2023 15:45 WG2060551
Naphthalene ND 0.00100 1 05/17/2023 15:45 WG2060551
Nitrobenzene ND 0.0100 1 05/17/2023 15:45 WG2060551
n-Nitrosodimethylamine ND 0.0100 1 05/17/2023 15:45 WG2060551
n-Nitrosodiphenylamine ND 0.0100 1 05/17/2023 15:45 WG2060551
n-Nitrosodi-n-propylamine ND 0.0100 1 05/17/2023 15:45 WG2060551
Phenanthrene ND 0.00100 1 05/17/2023 15:45 WG2060551
Benzylbutyl phthalate ND 0.00300 1 05/17/2023 15:45 WG2060551
Bis(2-ethylhexyl)phthalate ND 0.00300 1 05/17/2023 15:45 WG2060551
Di-n-butyl phthalate ND 0.00300 1 05/17/2023 15:45 WG2060551
Diethyl phthalate ND 0.00300 1 05/17/2023 15:45 WG2060551
Dimethyl phthalate ND 0.00300 1 05/17/2023 15:45 WG2060551
Di-n-octyl phthalate ND 0.00300 1 05/17/2023 15:45 WG2060551
Pyrene ND 0.00100 1 05/17/2023 15:45 WG2060551
1,2,4-Trichlorobenzene ND 0.0100 1 05/17/2023 15:45 WG2060551
4-Chloro-3-methylphenol ND 0.0100 1 05/17/2023 15:45 WG2060551
2-Chlorophenol ND 0.0100 1 05/17/2023 15:45 WG2060551
2,4-Dichlorophenol ND 0.0100 1 05/17/2023 15:45 WG2060551
2,4-Dimethylphenol ND 0.0100 1 05/17/2023 15:45 WG2060551
4,6-Dinitro-2-methylphenol ND 0.0100 1 05/17/2023 15:45 WG2060551
2,4-Dinitrophenol ND 0.0100 1 05/17/2023 15:45 WG2060551
2-Nitrophenol ND 0.0100 1 05/17/2023 15:45 WG2060551
4-Nitrophenol ND J4 0.0100 1 05/17/2023 15:45 WG2060551
Pentachlorophenol ND 0.0100 1 05/17/2023 15:45 WG2060551
Phenol ND 0.0100 1 05/17/2023 15:45 WG2060551
2,4,6-Trichlorophenol ND 0.0100 1 05/17/2023 15:45 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1615666
MW-6
Collected date/time: 05/11/23 10:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 2-Fluorophenol 22.7 10.0-120 05/17/2023 15:45 WG2060551
(S) Phenol-d5 19.4 10.0-120 05/17/2023 15:45 WG2060551
(S) Nitrobenzene-d5 81.6 10.0-127 05/17/2023 15:45 WG2060551
(S) 2-Fluorobiphenyl 57.3 10.0-130 05/17/2023 15:45 WG2060551
(S) 2,4,6-Tribromophenol 42.3 10.0-155 05/17/2023 15:45 WG2060551
(S) p-Terphenyl-d14 46.1 10.0-128 05/17/2023 15:45 WG2060551
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1615666
MW-1 FILTERED
Collected date/time: 05/11/23 13:48
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:17 WG2059828
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 22:01 WG2060110
Arsenic 0.0123 B 0.0100 1 05/18/2023 22:01 WG2060110
Beryllium ND 0.00200 1 05/18/2023 22:01 WG2060110
Cadmium ND 0.00200 1 05/18/2023 22:01 WG2060110
Chromium ND 0.0100 1 05/18/2023 22:01 WG2060110
Copper ND 0.0100 1 05/18/2023 22:01 WG2060110
Lead ND 0.00600 1 05/18/2023 22:01 WG2060110
Nickel ND 0.0100 1 05/18/2023 22:01 WG2060110
Selenium ND 0.0100 1 05/18/2023 22:01 WG2060110
Silver ND 0.00500 1 05/18/2023 22:01 WG2060110
Thallium ND 0.0100 1 05/18/2023 22:01 WG2060110
Zinc ND 0.0500 1 05/18/2023 22:01 WG2060110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1615666
MW-2 FILTERED
Collected date/time: 05/11/23 12:56
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:24 WG2059828
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 22:04 WG2060110
Arsenic 0.0142 B 0.0100 1 05/18/2023 22:04 WG2060110
Beryllium ND 0.00200 1 05/18/2023 22:04 WG2060110
Cadmium ND 0.00200 1 05/18/2023 22:04 WG2060110
Chromium ND 0.0100 1 05/18/2023 22:04 WG2060110
Copper ND 0.0100 1 05/18/2023 22:04 WG2060110
Lead ND 0.00600 1 05/18/2023 22:04 WG2060110
Nickel ND 0.0100 1 05/18/2023 22:04 WG2060110
Selenium ND 0.0100 1 05/18/2023 22:04 WG2060110
Silver ND 0.00500 1 05/18/2023 22:04 WG2060110
Thallium ND 0.0100 1 05/18/2023 22:04 WG2060110
Zinc ND 0.0500 1 05/18/2023 22:04 WG2060110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1615666
MW-3 FILTERED
Collected date/time: 05/11/23 11:21
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:26 WG2059828
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 22:07 WG2060110
Arsenic 0.630 0.0100 1 05/18/2023 22:07 WG2060110
Beryllium ND 0.00200 1 05/18/2023 22:07 WG2060110
Cadmium ND 0.00200 1 05/18/2023 22:07 WG2060110
Chromium ND 0.0100 1 05/18/2023 22:07 WG2060110
Copper ND 0.0100 1 05/18/2023 22:07 WG2060110
Lead ND 0.00600 1 05/18/2023 22:07 WG2060110
Nickel ND 0.0100 1 05/18/2023 22:07 WG2060110
Selenium ND 0.0100 1 05/18/2023 22:07 WG2060110
Silver ND 0.00500 1 05/18/2023 22:07 WG2060110
Thallium ND 0.0100 1 05/18/2023 22:07 WG2060110
Zinc ND 0.0500 1 05/18/2023 22:07 WG2060110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 10
L1615666
MW-4 FILTERED
Collected date/time: 05/11/23 12:10
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:29 WG2059828
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 22:10 WG2060110
Arsenic ND 0.0100 1 05/18/2023 22:10 WG2060110
Beryllium ND 0.00200 1 05/18/2023 22:10 WG2060110
Cadmium ND 0.00200 1 05/18/2023 22:10 WG2060110
Chromium ND 0.0100 1 05/18/2023 22:10 WG2060110
Copper ND 0.0100 1 05/18/2023 22:10 WG2060110
Lead ND 0.00600 1 05/18/2023 22:10 WG2060110
Nickel 0.0111 B 0.0100 1 05/18/2023 22:10 WG2060110
Selenium ND 0.0100 1 05/18/2023 22:10 WG2060110
Silver ND 0.00500 1 05/18/2023 22:10 WG2060110
Thallium ND 0.0100 1 05/18/2023 22:10 WG2060110
Zinc ND 0.0500 1 05/18/2023 22:10 WG2060110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 11
L1615666
MW-5 FILTERED
Collected date/time: 05/11/23 14:50
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:31 WG2059828
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 22:12 WG2060110
Arsenic 0.0336 B 0.0100 1 05/18/2023 22:12 WG2060110
Beryllium ND 0.00200 1 05/18/2023 22:12 WG2060110
Cadmium ND 0.00200 1 05/18/2023 22:12 WG2060110
Chromium ND 0.0100 1 05/18/2023 22:12 WG2060110
Copper ND 0.0100 1 05/18/2023 22:12 WG2060110
Lead ND 0.00600 1 05/18/2023 22:12 WG2060110
Nickel ND 0.0100 1 05/18/2023 22:12 WG2060110
Selenium ND 0.0100 1 05/18/2023 22:12 WG2060110
Silver ND 0.00500 1 05/18/2023 22:12 WG2060110
Thallium ND 0.0100 1 05/18/2023 22:12 WG2060110
Zinc ND 0.0500 1 05/18/2023 22:12 WG2060110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 12
L1615666
MW-6 FILTERED
Collected date/time: 05/11/23 10:40
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/04/2023 19:34 WG2059828
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 05/18/2023 22:15 WG2060110
Arsenic ND 0.0100 1 05/18/2023 22:15 WG2060110
Beryllium ND 0.00200 1 05/18/2023 22:15 WG2060110
Cadmium ND 0.00200 1 05/18/2023 22:15 WG2060110
Chromium ND 0.0100 1 05/18/2023 22:15 WG2060110
Copper ND 0.0100 1 05/18/2023 22:15 WG2060110
Lead ND 0.00600 1 05/18/2023 22:15 WG2060110
Nickel ND 0.0100 1 05/18/2023 22:15 WG2060110
Selenium ND 0.0100 1 05/18/2023 22:15 WG2060110
Silver ND 0.00500 1 05/18/2023 22:15 WG2060110
Thallium ND 0.0100 1 05/18/2023 22:15 WG2060110
Zinc ND 0.0500 1 05/18/2023 22:15 WG2060110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2061054
Gravimetric Analysis by Method 2540 C-2011 L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3926805-1 05/17/23 09:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U J 10.0 10.0
L1615665-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1615665-01 05/17/23 09:52 • (DUP) R3926805-3 05/17/23 09:52
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Dissolved Solids 687 712 1 3.62 5
L1615666-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1615666-02 05/17/23 09:52 • (DUP) R3926805-4 05/17/23 09:52
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Dissolved Solids 635 669 1 5.32 J3 5
Laboratory Control Sample (LCS)
(LCS) R3926805-2 05/17/23 09:52
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Dissolved Solids 8800 7550 85.8 77.3-123
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060591
Wet Chemistry by Method 2320 B-2011 L1615666-01,02
Method Blank (MB)
(MB) R3925362-2 05/16/23 09:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Alkalinity,Bicarbonate U 8.45 20.0
Alkalinity,Carbonate U 8.45 20.0
Sample Narrative:
BLANK: Endpoint pH 4.5
L1614187-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1614187-05 05/16/23 09:57 • (DUP) R3925362-3 05/16/23 10:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Alkalinity,Bicarbonate 236 236 1 0.356 20
Alkalinity,Carbonate 33.6 29.8 1 11.9 20
Sample Narrative:
OS: Endpoint pH 4.5 Headspace
DUP: Endpoint pH 4.5
L1615503-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1615503-01 05/16/23 10:54 • (DUP) R3925362-4 05/16/23 11:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Alkalinity,Bicarbonate 179 183 1 2.28 20
Alkalinity,Carbonate ND ND 1 0.000 20
Sample Narrative:
OS: Endpoint pH 4.5 Headspace
DUP: Endpoint pH 4.5
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062106
Wet Chemistry by Method 2320 B-2011 L1615666-04
Method Blank (MB)
(MB) R3926451-2 05/18/23 10:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Alkalinity,Bicarbonate U 8.45 20.0
Alkalinity,Carbonate U 8.45 20.0
Sample Narrative:
BLANK: Endpoint pH 4.5
L1614778-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1614778-01 05/18/23 11:09 • (DUP) R3926451-4 05/18/23 11:15
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Alkalinity,Bicarbonate 482 473 1 1.89 20
Alkalinity,Carbonate ND ND 1 0.000 20
Sample Narrative:
OS: Endpoint pH 4.5 Headspace
DUP: Endpoint pH 4.5
L1615666-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1615666-04 05/18/23 12:24 • (DUP) R3926451-6 05/18/23 12:29
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Alkalinity,Bicarbonate 414 417 1 0.746 20
Alkalinity,Carbonate ND ND 1 0.000 20
Sample Narrative:
OS: Endpoint pH 4.5 Headspace
DUP: Endpoint pH 4.5
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062879
Wet Chemistry by Method 2320 B-2011 L1615666-03,05,06
Method Blank (MB)
(MB) R3926900-2 05/19/23 09:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Alkalinity,Bicarbonate U 8.45 20.0
Alkalinity,Carbonate U 8.45 20.0
Sample Narrative:
BLANK: Endpoint pH 4.5
L1615553-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1615553-01 05/19/23 09:33 • (DUP) R3926900-3 05/19/23 09:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Alkalinity,Bicarbonate 604 605 1 0.176 20
Alkalinity,Carbonate ND ND 1 0.000 20
Sample Narrative:
OS: Endpoint pH 4.5 Headspace
DUP: Endpoint pH 4.5
L1615682-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1615682-03 05/19/23 10:28 • (DUP) R3926900-4 05/19/23 10:31
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Alkalinity,Bicarbonate 418 420 1 0.375 20
Alkalinity,Carbonate ND ND 1 0.000 20
Sample Narrative:
OS: Endpoint pH 4.5 Headspace
DUP: Endpoint pH 4.5
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060350
Wet Chemistry by Method 350.1 L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3925284-1 05/16/23 09:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Ammonia Nitrogen U 0.117 0.250
L1615666-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1615666-02 05/16/23 09:46 • (DUP) R3925284-5 05/16/23 09:48
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Ammonia Nitrogen 0.619 0.621 1 0.323 10
L1615682-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1615682-05 05/16/23 10:07 • (DUP) R3925284-7 05/16/23 10:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Ammonia Nitrogen ND ND 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3925284-2 05/16/23 09:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Ammonia Nitrogen 7.50 7.55 101 90.0-110
L1615666-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615666-01 05/16/23 09:42 • (MS) R3925284-3 05/16/23 09:43 • (MSD) R3925284-4 05/16/23 09:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Ammonia Nitrogen 5.00 ND 5.05 5.15 101 103 1 90.0-110 1.90 10
L1615682-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L1615682-04 05/16/23 10:04 • (MS) R3925284-6 05/16/23 10:06
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Ammonia Nitrogen 5.00 ND 5.07 101 1 90.0-110
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059721
Wet Chemistry by Method 410.4 L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3924641-1 05/14/23 16:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
COD U 11.7 20.0
L1615666-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1615666-02 05/14/23 16:07 • (DUP) R3924641-5 05/14/23 16:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
COD ND ND 1 0.000 20
L1615666-06 Original Sample (OS) • Duplicate (DUP)
(OS) L1615666-06 05/14/23 16:09 • (DUP) R3924641-6 05/14/23 16:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
COD 20.8 21.1 1 1.40 20
Laboratory Control Sample (LCS)
(LCS) R3924641-2 05/14/23 16:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
COD 500 516 103 90.0-110
L1615633-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615633-03 05/14/23 16:05 • (MS) R3924641-3 05/14/23 16:06 • (MSD) R3924641-4 05/14/23 16:06
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
COD 500 64.8 525 543 92.0 95.6 1 80.0-120 3.31 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2061250
Wet Chemistry by Method 9040C L1615666-01,02,03,04,05,06
L1615570-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1615570-01 05/18/23 09:04 • (DUP) R3926330-2 05/18/23 09:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 7.44 7.45 1 0.134 1
Sample Narrative:
OS: 7.44 at 20.1C
DUP: 7.45 at 20C
L1616774-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1616774-01 05/18/23 09:04 • (DUP) R3926330-3 05/18/23 09:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 9.31 9.32 1 0.107 1
Sample Narrative:
OS: 9.31 at 19.6C
DUP: 9.32 at 19.6C
Laboratory Control Sample (LCS)
(LCS) R3926330-1 05/18/23 09:04
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su %%
pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS: 10 at 20.3C
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059136
Wet Chemistry by Method 9056A L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3930048-1 05/13/23 19:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Chloride U 0.379 1.00
Nitrate as (N)U 0.0480 0.100
Sulfate U 0.594 5.00
L1615640-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1615640-02 05/13/23 20:34 • (DUP) R3930048-3 05/14/23 01:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Chloride 31.8 34.1 1 6.92 15
Nitrate as (N)0.741 0.913 1 20.8 J3 15
Sulfate ND ND 1 14.8 15
L1615640-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1615640-05 05/13/23 21:12 • (DUP) R3930048-6 05/14/23 02:20
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Chloride 1.88 2.18 1 14.6 15
Nitrate as (N)0.167 0.293 1 55.0 P1 15
Sulfate ND ND 1 33.2 P1 15
Laboratory Control Sample (LCS)
(LCS) R3930048-2 05/13/23 20:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Chloride 40.0 38.1 95.2 80.0-120
Nitrate as (N)8.00 8.09 101 80.0-120
Sulfate 40.0 40.5 101 80.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059136
Wet Chemistry by Method 9056A L1615666-01,02,03,04,05,06
L1615640-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615640-02 05/13/23 20:34 • (MS) R3930048-4 05/14/23 01:55 • (MSD) R3930048-5 05/14/23 02:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Chloride 50.0 31.8 80.1 80.9 96.5 98.0 1 80.0-120 0.930 15
Nitrate as (N)5.00 0.741 5.59 5.88 96.9 103 1 80.0-120 5.04 15
Sulfate 50.0 ND 52.8 52.9 101 101 1 80.0-120 0.253 15
L1615640-05 Original Sample (OS) • Matrix Spike (MS)
(OS) L1615640-05 05/13/23 21:12 • (MS) R3930048-7 05/14/23 02:33
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Chloride 50.0 1.88 47.6 91.4 1 80.0-120
Nitrate as (N)5.00 0.167 4.62 89.1 1 80.0-120
Sulfate 50.0 ND 53.7 100 1 80.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060200
Wet Chemistry by Method 9060A L1615666-01
Method Blank (MB)
(MB) R3925088-2 05/15/23 13:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TOC (Total Organic Carbon) 0.525 J 0.102 1.00
L1615661-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1615661-02 05/15/23 14:29 • (DUP) R3925088-3 05/15/23 14:51
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
TOC (Total Organic Carbon) 71.6 74.2 1 3.58 20
Laboratory Control Sample (LCS)
(LCS) R3925088-1 05/15/23 13:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TOC (Total Organic Carbon) 75.0 74.3 99.1 85.0-115
L1615666-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615666-01 05/15/23 15:07 • (MS) R3925088-4 05/15/23 15:28 • (MSD) R3925088-5 05/15/23 15:49
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
TOC (Total Organic Carbon) 50.0 2.97 52.0 52.3 98.1 98.7 1 80.0-120 0.652 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060649
Wet Chemistry by Method 9060A L1615666-02,03,04,05,06
Method Blank (MB)
(MB) R3925980-2 05/17/23 03:46
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TOC (Total Organic Carbon) 0.393 J 0.102 1.00
L1615666-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1615666-05 05/17/23 08:51 • (DUP) R3925980-5 05/17/23 09:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
TOC (Total Organic Carbon) 7.73 7.38 1 4.60 20
L1615671-11 Original Sample (OS) • Duplicate (DUP)
(OS) L1615671-11 05/17/23 11:55 • (DUP) R3925980-8 05/17/23 12:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
TOC (Total Organic Carbon) ND ND 1 3.76 20
Laboratory Control Sample (LCS)
(LCS) R3925980-1 05/17/23 02:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TOC (Total Organic Carbon) 75.0 74.4 99.2 85.0-115
L1615666-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615666-04 05/17/23 07:52 • (MS) R3925980-3 05/17/23 08:13 • (MSD) R3925980-4 05/17/23 08:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
TOC (Total Organic Carbon) 50.0 3.16 50.5 53.6 94.6 101 1 80.0-120 6.07 20
L1615671-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615671-06 05/17/23 10:53 • (MS) R3925980-6 05/17/23 11:14 • (MSD) R3925980-7 05/17/23 11:36
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
TOC (Total Organic Carbon) 50.0 1.12 52.1 52.3 102 102 1 80.0-120 0.556 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059827
Mercury by Method 7470A L1615666-01,02,03,04,05
Method Blank (MB)
(MB) R3932821-1 06/05/23 10:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3932821-2 06/05/23 10:52
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00316 105 80.0-120
L1615280-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615280-02 06/05/23 10:55 • (MS) R3932821-3 06/05/23 10:57 • (MSD) R3932821-4 06/05/23 11:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00229 0.00233 76.4 77.6 1 75.0-125 1.61 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2059828
Mercury by Method 7470A L1615666-06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3932654-1 06/04/23 19:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3932654-2 06/04/23 19:04
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00269 89.7 80.0-120
L1615671-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615671-06 06/04/23 19:06 • (MS) R3932654-3 06/04/23 19:09 • (MSD) R3932654-4 06/04/23 19:12
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00312 0.00312 104 104 1 75.0-125 0.107 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060110
Metals (ICP) by Method 6010B L1615666-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3927760-1 05/18/23 21:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic 0.00661 J 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Calcium U 0.0793 1.00
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Iron U 0.0180 0.100
Lead U 0.00299 0.00600
Magnesium U 0.0853 1.00
Manganese U 0.000934 0.0100
Nickel 0.00258 J 0.00161 0.0100
Potassium U 0.261 2.00
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Sodium U 0.504 3.00
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3927760-2 05/18/23 21:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.994 99.4 80.0-120
Arsenic 1.00 0.952 95.2 80.0-120
Beryllium 1.00 0.986 98.6 80.0-120
Cadmium 1.00 0.976 97.6 80.0-120
Calcium 10.0 10.1 101 80.0-120
Chromium 1.00 0.984 98.4 80.0-120
Copper 1.00 0.991 99.1 80.0-120
Iron 10.0 9.68 96.8 80.0-120
Lead 1.00 0.950 95.0 80.0-120
Magnesium 10.0 9.77 97.7 80.0-120
Manganese 1.00 0.938 93.8 80.0-120
Nickel 1.00 0.972 97.2 80.0-120
Potassium 10.0 9.64 96.4 80.0-120
Selenium 1.00 0.964 96.4 80.0-120
Silver 0.200 0.190 95.1 80.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060110
Metals (ICP) by Method 6010B L1615666-01,02,03,04,05,06,07,08,09,10,11,12
Laboratory Control Sample (LCS)
(LCS) R3927760-2 05/18/23 21:28
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Sodium 10.0 10.0 100 80.0-120
Thallium 1.00 0.950 95.0 80.0-120
Zinc 1.00 0.948 94.8 80.0-120
L1615666-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615666-03 05/18/23 21:31 • (MS) R3927760-4 05/18/23 21:36 • (MSD) R3927760-5 05/18/23 21:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 1.00 1.01 100 100 1 75.0-125 0.102 20
Arsenic 1.00 0.596 1.58 1.57 97.9 97.0 1 75.0-125 0.602 20
Beryllium 1.00 ND 0.980 0.973 98.0 97.3 1 75.0-125 0.759 20
Cadmium 1.00 ND 1.00 0.990 100 98.9 1 75.0-125 1.07 20
Calcium 10.0 153 160 161 68.8 76.6 1 75.0-125 V 0.487 20
Chromium 1.00 ND 0.977 0.968 97.7 96.8 1 75.0-125 1.02 20
Copper 1.00 ND 1.01 1.00 101 100 1 75.0-125 0.964 20
Iron 10.0 5.97 15.2 15.1 92.3 91.7 1 75.0-125 0.412 20
Lead 1.00 ND 0.955 0.937 95.5 93.7 1 75.0-125 1.85 20
Magnesium 10.0 67.4 75.8 75.9 84.3 85.8 1 75.0-125 0.203 20
Manganese 1.00 0.728 1.63 1.61 89.9 88.5 1 75.0-125 0.842 20
Nickel 1.00 ND 0.981 0.970 97.3 96.2 1 75.0-125 1.19 20
Potassium 10.0 10.1 19.6 19.6 94.7 94.8 1 75.0-125 0.00862 20
Selenium 1.00 ND 0.996 0.988 99.6 98.8 1 75.0-125 0.735 20
Silver 0.200 ND 0.195 0.193 97.3 96.4 1 75.0-125 1.00 20
Sodium 10.0 110 118 118 82.9 85.1 1 75.0-125 0.184 20
Thallium 1.00 0.0116 0.935 0.927 92.4 91.5 1 75.0-125 0.934 20
Zinc 1.00 ND 0.923 0.911 92.3 91.1 1 75.0-125 1.34 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2062721
Volatile Organic Compounds (GC) by Method 8015D/GRO L1615666-01,02,04
Method Blank (MB)
(MB) R3926797-1 05/18/23 22:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)92.5 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3926797-2 05/18/23 22:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 4.87 88.5 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 98.6 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2063048
Volatile Organic Compounds (GC) by Method 8015D/GRO L1615666-05,06
Method Blank (MB)
(MB) R3927241-2 05/19/23 12:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)96.9 78.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3927241-1 05/19/23 12:09 • (LCSD) R3927241-3 05/19/23 13:07
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.50 4.96 4.78 90.2 86.9 72.0-127 3.70 20
(S)
a,a,a-Trifluorotoluene(FID) 102 101 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2063582
Volatile Organic Compounds (GC) by Method 8015D/GRO L1615666-03
Method Blank (MB)
(MB) R3927559-3 05/21/23 10:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)93.1 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3927559-2 05/21/23 10:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.93 108 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 100 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2063135
Volatile Organic Compounds (GC/MS) by Method 8260B L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3928287-3 05/19/23 21:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromobenzene U 0.000118 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-Butylbenzene U 0.000125 0.00100
tert-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
2-Chlorotoluene U 0.000106 0.00100
4-Chlorotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
cis-1,2-Dichloroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
1,1-Dichloropropene U 0.000142 0.00100
1,3-Dichloropropane U 0.000110 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
2,2-Dichloropropane U 0.000161 0.00100
Di-isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Hexachloro-1,3-butadiene U 0.000337 0.00100
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2063135
Volatile Organic Compounds (GC/MS) by Method 8260B L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3928287-3 05/19/23 21:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Isopropylbenzene U 0.000105 0.00100
p-Isopropyltoluene U 0.000120 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK) U 0.000478 0.0100
Methyl tert-butyl ether U 0.000101 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100
1,1,1,2-Tetrachloroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene U 0.000230 0.00100
1,2,4-Trichlorobenzene U 0.000481 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,2,3-Trichloropropane U 0.000237 0.00250
1,2,4-Trimethylbenzene U 0.000322 0.00100
1,2,3-Trimethylbenzene U 0.000104 0.00100
1,3,5-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 98.7 80.0-120
(S) 4-Bromofluorobenzene 89.9 77.0-126
(S) 1,2-Dichloroethane-d4 97.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3928287-1 05/19/23 20:13 • (LCSD) R3928287-2 05/19/23 20:33
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0278 0.0328 111 131 19.0-160 16.5 27
Acrolein 0.0250 0.0272 0.0250 109 100 10.0-160 8.43 26
Acrylonitrile 0.0250 0.0240 0.0259 96.0 104 55.0-149 7.62 20
Benzene 0.00500 0.00462 0.00463 92.4 92.6 70.0-123 0.216 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2063135
Volatile Organic Compounds (GC/MS) by Method 8260B L1615666-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3928287-1 05/19/23 20:13 • (LCSD) R3928287-2 05/19/23 20:33
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Bromobenzene 0.00500 0.00471 0.00457 94.2 91.4 73.0-121 3.02 20
Bromodichloromethane 0.00500 0.00517 0.00515 103 103 75.0-120 0.388 20
Bromoform 0.00500 0.00432 0.00444 86.4 88.8 68.0-132 2.74 20
Bromomethane 0.00500 0.00480 0.00407 96.0 81.4 10.0-160 16.5 25
n-Butylbenzene 0.00500 0.00410 0.00419 82.0 83.8 73.0-125 2.17 20
sec-Butylbenzene 0.00500 0.00453 0.00453 90.6 90.6 75.0-125 0.000 20
tert-Butylbenzene 0.00500 0.00438 0.00421 87.6 84.2 76.0-124 3.96 20
Carbon tetrachloride 0.00500 0.00475 0.00475 95.0 95.0 68.0-126 0.000 20
Chlorobenzene 0.00500 0.00479 0.00462 95.8 92.4 80.0-121 3.61 20
Chlorodibromomethane 0.00500 0.00485 0.00449 97.0 89.8 77.0-125 7.71 20
Chloroethane 0.00500 0.00483 0.00457 96.6 91.4 47.0-150 5.53 20
Chloroform 0.00500 0.00442 0.00450 88.4 90.0 73.0-120 1.79 20
Chloromethane 0.00500 0.00556 0.00499 111 99.8 41.0-142 10.8 20
2-Chlorotoluene 0.00500 0.00472 0.00468 94.4 93.6 76.0-123 0.851 20
4-Chlorotoluene 0.00500 0.00475 0.00455 95.0 91.0 75.0-122 4.30 20
1,2-Dibromo-3-Chloropropane 0.00500 0.00410 0.00367 82.0 73.4 58.0-134 11.1 20
1,2-Dibromoethane 0.00500 0.00472 0.00461 94.4 92.2 80.0-122 2.36 20
Dibromomethane 0.00500 0.00525 0.00497 105 99.4 80.0-120 5.48 20
1,2-Dichlorobenzene 0.00500 0.00450 0.00447 90.0 89.4 79.0-121 0.669 20
1,3-Dichlorobenzene 0.00500 0.00451 0.00450 90.2 90.0 79.0-120 0.222 20
1,4-Dichlorobenzene 0.00500 0.00443 0.00442 88.6 88.4 79.0-120 0.226 20
Dichlorodifluoromethane 0.00500 0.00581 0.00495 116 99.0 51.0-149 16.0 20
1,1-Dichloroethane 0.00500 0.00469 0.00477 93.8 95.4 70.0-126 1.69 20
1,2-Dichloroethane 0.00500 0.00468 0.00506 93.6 101 70.0-128 7.80 20
1,1-Dichloroethene 0.00500 0.00446 0.00494 89.2 98.8 71.0-124 10.2 20
cis-1,2-Dichloroethene 0.00500 0.00428 0.00424 85.6 84.8 73.0-120 0.939 20
trans-1,2-Dichloroethene 0.00500 0.00440 0.00443 88.0 88.6 73.0-120 0.680 20
1,2-Dichloropropane 0.00500 0.00498 0.00487 99.6 97.4 77.0-125 2.23 20
1,1-Dichloropropene 0.00500 0.00483 0.00479 96.6 95.8 74.0-126 0.832 20
1,3-Dichloropropane 0.00500 0.00484 0.00460 96.8 92.0 80.0-120 5.08 20
cis-1,3-Dichloropropene 0.00500 0.00481 0.00440 96.2 88.0 80.0-123 8.90 20
trans-1,3-Dichloropropene 0.00500 0.00475 0.00441 95.0 88.2 78.0-124 7.42 20
2,2-Dichloropropane 0.00500 0.00475 0.00432 95.0 86.4 58.0-130 9.48 20
Di-isopropyl ether 0.00500 0.00471 0.00511 94.2 102 58.0-138 8.15 20
Ethylbenzene 0.00500 0.00450 0.00433 90.0 86.6 79.0-123 3.85 20
Hexachloro-1,3-butadiene 0.00500 0.00424 0.00460 84.8 92.0 54.0-138 8.14 20
Isopropylbenzene 0.00500 0.00437 0.00420 87.4 84.0 76.0-127 3.97 20
p-Isopropyltoluene 0.00500 0.00415 0.00417 83.0 83.4 76.0-125 0.481 20
2-Butanone (MEK)0.0250 0.0249 0.0268 99.6 107 44.0-160 7.35 20
Methylene Chloride 0.00500 0.00477 0.00430 95.4 86.0 67.0-120 10.4 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2063135
Volatile Organic Compounds (GC/MS) by Method 8260B L1615666-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3928287-1 05/19/23 20:13 • (LCSD) R3928287-2 05/19/23 20:33
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
4-Methyl-2-pentanone (MIBK) 0.0250 0.0235 0.0224 94.0 89.6 68.0-142 4.79 20
Methyl tert-butyl ether 0.00500 0.00449 0.00471 89.8 94.2 68.0-125 4.78 20
Naphthalene 0.00500 0.00322 0.00347 64.4 69.4 54.0-135 7.47 20
n-Propylbenzene 0.00500 0.00456 0.00447 91.2 89.4 77.0-124 1.99 20
Styrene 0.00500 0.00420 0.00398 84.0 79.6 73.0-130 5.38 20
1,1,1,2-Tetrachloroethane 0.00500 0.00434 0.00431 86.8 86.2 75.0-125 0.694 20
1,1,2,2-Tetrachloroethane 0.00500 0.00480 0.00420 96.0 84.0 65.0-130 13.3 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00431 0.00457 86.2 91.4 69.0-132 5.86 20
Tetrachloroethene 0.00500 0.00461 0.00454 92.2 90.8 72.0-132 1.53 20
Toluene 0.00500 0.00455 0.00426 91.0 85.2 79.0-120 6.58 20
1,2,3-Trichlorobenzene 0.00500 0.00340 0.00401 68.0 80.2 50.0-138 16.5 20
1,2,4-Trichlorobenzene 0.00500 0.00394 0.00443 78.8 88.6 57.0-137 11.7 20
1,1,1-Trichloroethane 0.00500 0.00474 0.00495 94.8 99.0 73.0-124 4.33 20
1,1,2-Trichloroethane 0.00500 0.00491 0.00493 98.2 98.6 80.0-120 0.406 20
Trichloroethene 0.00500 0.00479 0.00493 95.8 98.6 78.0-124 2.88 20
Trichlorofluoromethane 0.00500 0.00542 0.00554 108 111 59.0-147 2.19 20
1,2,3-Trichloropropane 0.00500 0.00475 0.00453 95.0 90.6 73.0-130 4.74 20
1,2,4-Trimethylbenzene 0.00500 0.00405 0.00421 81.0 84.2 76.0-121 3.87 20
1,2,3-Trimethylbenzene 0.00500 0.00427 0.00415 85.4 83.0 77.0-120 2.85 20
1,3,5-Trimethylbenzene 0.00500 0.00467 0.00450 93.4 90.0 76.0-122 3.71 20
Vinyl chloride 0.00500 0.00535 0.00452 107 90.4 67.0-131 16.8 20
Xylenes, Total 0.0150 0.0131 0.0128 87.3 85.3 79.0-123 2.32 20
(S) Toluene-d8 97.4 97.9 80.0-120
(S) 4-Bromofluorobenzene 93.4 93.1 77.0-126
(S) 1,2-Dichloroethane-d4 102 110 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2061651
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3927104-1 05/19/23 08:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) High Fraction U 0.0247 0.100
(S) o-Terphenyl 115 31.0-160
Laboratory Control Sample (LCS)
(LCS) R3927104-2 05/19/23 08:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) High Fraction 1.50 1.77 118 50.0-150
(S) o-Terphenyl 141 31.0-160
L1615746-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615746-03 05/19/23 12:13 • (MS) R3927104-3 05/19/23 12:34 • (MSD) R3927104-4 05/19/23 12:54
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.43 2.71 4.43 5.23 120 176 1 50.0-150 J5 16.6 20
(S) o-Terphenyl 113 123 31.0-160
Sample Narrative:
OS: Surrogate failure due to matrix interference
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060551
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3926002-3 05/17/23 12:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060551
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1615666-01,02,03,04,05,06
Method Blank (MB)
(MB) R3926002-3 05/17/23 12:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 27.8 10.0-120
(S) Phenol-d5 23.1 10.0-120
(S) Nitrobenzene-d5 84.4 10.0-127
(S) 2-Fluorobiphenyl 60.9 10.0-130
(S) 2,4,6-Tribromophenol 60.0 10.0-155
(S) p-Terphenyl-d14 64.4 10.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3926002-1 05/17/23 11:29 • (LCSD) R3926002-2 05/17/23 11:51
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 0.0319 0.0323 63.8 64.6 41.0-120 1.25 22
Acenaphthylene 0.0500 0.0360 0.0338 72.0 67.6 43.0-120 6.30 22
Anthracene 0.0500 0.0345 0.0338 69.0 67.6 45.0-120 2.05 20
Benzidine 0.100 0.00112 0.000953 0.000 0.000 10.0-120 J4 J4 0.000 36
Benzo(a)anthracene 0.0500 0.0347 0.0349 69.4 69.8 47.0-120 0.575 20
Benzo(b)fluoranthene 0.0500 0.0337 0.0353 67.4 70.6 46.0-120 4.64 20
Benzo(k)fluoranthene 0.0500 0.0317 0.0302 63.4 60.4 46.0-120 4.85 21
Benzo(g,h,i)perylene 0.0500 0.0308 0.0302 61.6 60.4 48.0-121 1.97 20
Benzo(a)pyrene 0.0500 0.0354 0.0357 70.8 71.4 47.0-120 0.844 20
Bis(2-chlorethoxy)methane 0.0500 0.0426 0.0438 85.2 87.6 33.0-120 2.78 24
Bis(2-chloroethyl)ether 0.0500 0.0338 0.0388 67.6 77.6 23.0-120 13.8 33
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060551
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1615666-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3926002-1 05/17/23 11:29 • (LCSD) R3926002-2 05/17/23 11:51
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
2,2-Oxybis(1-Chloropropane) 0.0500 0.0305 0.0340 61.0 68.0 28.0-120 10.9 31
4-Bromophenyl-phenylether 0.0500 0.0365 0.0367 73.0 73.4 45.0-120 0.546 20
2-Chloronaphthalene 0.0500 0.0297 0.0290 59.4 58.0 37.0-120 2.39 25
4-Chlorophenyl-phenylether 0.0500 0.0378 0.0379 75.6 75.8 44.0-120 0.264 20
Chrysene 0.0500 0.0349 0.0348 69.8 69.6 48.0-120 0.287 20
Dibenz(a,h)anthracene 0.0500 0.0311 0.0308 62.2 61.6 47.0-120 0.969 20
1,2-Dichlorobenzene 0.0500 0.0286 0.0317 57.2 63.4 20.0-120 10.3 34
1,3-Dichlorobenzene 0.0500 0.0288 0.0315 57.6 63.0 17.0-120 8.96 35
1,4-Dichlorobenzene 0.0500 0.0293 0.0277 58.6 55.4 18.0-120 5.61 34
3,3-Dichlorobenzidine 0.100 0.0709 0.0764 70.9 76.4 44.0-120 7.47 20
2,4-Dinitrotoluene 0.0500 0.0445 0.0423 89.0 84.6 49.0-124 5.07 20
2,6-Dinitrotoluene 0.0500 0.0376 0.0387 75.2 77.4 46.0-120 2.88 21
Fluoranthene 0.0500 0.0392 0.0422 78.4 84.4 51.0-120 7.37 20
Fluorene 0.0500 0.0317 0.0327 63.4 65.4 47.0-120 3.11 20
Hexachlorobenzene 0.0500 0.0358 0.0356 71.6 71.2 44.0-120 0.560 20
Hexachloro-1,3-butadiene 0.0500 0.0448 0.0447 89.6 89.4 19.0-120 0.223 32
Hexachlorocyclopentadiene 0.0500 0.0205 0.0176 41.0 35.2 15.0-120 15.2 31
Hexachloroethane 0.0500 0.0324 0.0337 64.8 67.4 15.0-120 3.93 37
Indeno(1,2,3-cd)pyrene 0.0500 0.0291 0.0289 58.2 57.8 49.0-122 0.690 20
Isophorone 0.0500 0.0483 0.0507 96.6 101 36.0-120 4.85 23
Naphthalene 0.0500 0.0295 0.0295 59.0 59.0 27.0-120 0.000 27
Nitrobenzene 0.0500 0.0474 0.0480 94.8 96.0 27.0-120 1.26 29
n-Nitrosodimethylamine 0.0500 0.0234 0.0308 46.8 61.6 10.0-120 27.3 40
n-Nitrosodiphenylamine 0.0500 0.0303 0.0320 60.6 64.0 47.0-120 5.46 20
n-Nitrosodi-n-propylamine 0.0500 0.0367 0.0398 73.4 79.6 31.0-120 8.10 28
Phenanthrene 0.0500 0.0329 0.0328 65.8 65.6 46.0-120 0.304 20
Benzylbutyl phthalate 0.0500 0.0356 0.0366 71.2 73.2 43.0-121 2.77 20
Bis(2-ethylhexyl)phthalate 0.0500 0.0342 0.0342 68.4 68.4 43.0-122 0.000 20
Di-n-butyl phthalate 0.0500 0.0402 0.0389 80.4 77.8 49.0-121 3.29 20
Diethyl phthalate 0.0500 0.0437 0.0434 87.4 86.8 48.0-122 0.689 20
Dimethyl phthalate 0.0500 0.0394 0.0398 78.8 79.6 48.0-120 1.01 20
Di-n-octyl phthalate 0.0500 0.0319 0.0330 63.8 66.0 42.0-125 3.39 20
Pyrene 0.0500 0.0312 0.0312 62.4 62.4 47.0-120 0.000 20
1,2,4-Trichlorobenzene 0.0500 0.0371 0.0357 74.2 71.4 24.0-120 3.85 29
4-Chloro-3-methylphenol 0.0500 0.0321 0.0339 64.2 67.8 40.0-120 5.45 21
2-Chlorophenol 0.0500 0.0200 0.0216 40.0 43.2 25.0-120 7.69 35
2,4-Dichlorophenol 0.0500 0.0287 0.0288 57.4 57.6 36.0-120 0.348 26
2,4-Dimethylphenol 0.0500 0.0325 0.0341 65.0 68.2 33.0-120 4.80 26
4,6-Dinitro-2-methylphenol 0.0500 0.0342 0.0345 68.4 69.0 38.0-138 0.873 25
2,4-Dinitrophenol 0.0500 0.0316 0.0320 63.2 64.0 10.0-120 1.26 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2060551
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1615666-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3926002-1 05/17/23 11:29 • (LCSD) R3926002-2 05/17/23 11:51
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
2-Nitrophenol 0.0500 0.0316 0.0302 63.2 60.4 31.0-120 4.53 29
4-Nitrophenol 0.0500 0.100 0.0969 200 194 10.0-120 J4 J4 3.15 33
Pentachlorophenol 0.0500 0.0315 0.0330 63.0 66.0 23.0-120 4.65 25
Phenol 0.0500 0.0139 0.0162 27.8 32.4 10.0-120 15.3 36
2,4,6-Trichlorophenol 0.0500 0.0322 0.0318 64.4 63.6 42.0-120 1.25 23
(S) 2-Fluorophenol 30.4 32.8 10.0-120
(S) Phenol-d5 22.9 27.0 10.0-120
(S) Nitrobenzene-d5 91.7 94.2 10.0-127
(S) 2-Fluorobiphenyl 67.7 65.8 10.0-130
(S) 2,4,6-Tribromophenol 62.0 63.5 10.0-155
(S) p-Terphenyl-d14 63.3 65.7 10.0-128
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
T8 Sample(s) received past/too close to holding time expiration.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
June 20, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1623675
Samples Received:06/07/2023
Project Number:RECYCLED EARTH
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
June 20, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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June 20, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
STRENCHSW-1 L1623675-01 5
Qc: Quality Control Summary 10
Total Solids by Method 2540 B-2015 10
Wet Chemistry by Method 1664A 11
Wet Chemistry by Method 3500Cr C-2011 12
Mercury by Method 7470A 13
Metals (ICP) by Method 6010B 14
Volatile Organic Compounds (GC) by Method 8015D/GRO 16
Volatile Organic Compounds (GC/MS) by Method 8260B 17
Semi-Volatile Organic Compounds (GC) by Method 8015 21
Polychlorinated Biphenyls (GC) by Method 8082 22
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 23
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 27
Gl: Glossary of Terms 30
Al: Accreditations & Locations 31
Sc: Sample Chain of Custody 32
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
STRENCHSW-1 L1623675-01 GW Richie T. 06/06/23 08:30 06/07/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2076380 1 06/13/23 07:58 06/13/23 08:43 AS Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2073813 1 06/08/23 14:50 06/08/23 21:00 MCE Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2074741 1 06/12/23 10:23 06/12/23 10:23 SET Mt. Juliet, TN
Mercury by Method 7470A WG2075594 1 06/19/23 13:22 06/20/23 13:08 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2073614 1 06/08/23 14:39 06/14/23 12:58 SPL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2076271 1 06/13/23 06:07 06/13/23 06:07 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2075215 1 06/10/23 17:31 06/10/23 17:31 KSD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2073742 1 06/10/23 03:38 06/15/23 14:57 ICD Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2074397 1.05 06/09/23 06:32 06/10/23 14:24 LTB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2074753 1.11 06/09/23 16:51 06/10/23 03:37 JCH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2073722 1 06/09/23 21:30 06/10/23 06:24 DSH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1623675
STRENCHSW-1
Collected date/time: 06/06/23 08:30
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 596 1 06/13/2023 08:43 WG2076380
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 5.68 1 06/08/2023 21:00 WG2073813
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium ND 0.000500 1 06/12/2023 10:23 WG2074741
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 06/20/2023 13:08 WG2075594
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 06/14/2023 12:58 WG2073614
Arsenic 0.0723 0.0100 1 06/14/2023 12:58 WG2073614
Beryllium ND 0.00200 1 06/14/2023 12:58 WG2073614
Cadmium ND 0.00200 1 06/14/2023 12:58 WG2073614
Chromium ND 0.0100 1 06/14/2023 12:58 WG2073614
Copper ND 0.0100 1 06/14/2023 12:58 WG2073614
Lead ND 0.00600 1 06/14/2023 12:58 WG2073614
Nickel ND 0.0100 1 06/14/2023 12:58 WG2073614
Selenium ND 0.0100 1 06/14/2023 12:58 WG2073614
Silver ND 0.00500 1 06/14/2023 12:58 WG2073614
Thallium ND 0.0100 1 06/14/2023 12:58 WG2073614
Zinc ND 0.0500 1 06/14/2023 12:58 WG2073614
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 06/13/2023 06:07 WG2076271
(S) a,a,a-Trifluorotoluene(FID) 102 78.0-120 06/13/2023 06:07 WG2076271
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 06/10/2023 17:31 WG2075215
Acrolein ND 0.0500 1 06/10/2023 17:31 WG2075215
Acrylonitrile ND 0.0100 1 06/10/2023 17:31 WG2075215
Benzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Bromobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Bromodichloromethane ND 0.00100 1 06/10/2023 17:31 WG2075215
Bromoform ND 0.00100 1 06/10/2023 17:31 WG2075215
Bromomethane ND 0.00500 1 06/10/2023 17:31 WG2075215
n-Butylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
sec-Butylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
tert-Butylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1623675
STRENCHSW-1
Collected date/time: 06/06/23 08:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 06/10/2023 17:31 WG2075215
Chlorobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Chlorodibromomethane ND 0.00100 1 06/10/2023 17:31 WG2075215
Chloroethane ND 0.00500 1 06/10/2023 17:31 WG2075215
Chloroform ND 0.00500 1 06/10/2023 17:31 WG2075215
Chloromethane ND 0.00250 1 06/10/2023 17:31 WG2075215
2-Chlorotoluene ND 0.00100 1 06/10/2023 17:31 WG2075215
4-Chlorotoluene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,2-Dibromo-3-Chloropropane ND 0.00500 1 06/10/2023 17:31 WG2075215
1,2-Dibromoethane ND 0.00100 1 06/10/2023 17:31 WG2075215
Dibromomethane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,2-Dichlorobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,3-Dichlorobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,4-Dichlorobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Dichlorodifluoromethane ND 0.00500 1 06/10/2023 17:31 WG2075215
1,1-Dichloroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,2-Dichloroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1-Dichloroethene ND 0.00100 1 06/10/2023 17:31 WG2075215
cis-1,2-Dichloroethene ND 0.00100 1 06/10/2023 17:31 WG2075215
trans-1,2-Dichloroethene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,2-Dichloropropane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1-Dichloropropene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,3-Dichloropropane ND 0.00100 1 06/10/2023 17:31 WG2075215
cis-1,3-Dichloropropene ND 0.00100 1 06/10/2023 17:31 WG2075215
trans-1,3-Dichloropropene ND 0.00100 1 06/10/2023 17:31 WG2075215
2,2-Dichloropropane ND 0.00100 1 06/10/2023 17:31 WG2075215
Di-isopropyl ether ND 0.00100 1 06/10/2023 17:31 WG2075215
Ethylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Hexachloro-1,3-butadiene ND 0.00100 1 06/10/2023 17:31 WG2075215
Isopropylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
p-Isopropyltoluene ND 0.00100 1 06/10/2023 17:31 WG2075215
2-Butanone (MEK)ND 0.0100 1 06/10/2023 17:31 WG2075215
Methylene Chloride ND 0.00500 1 06/10/2023 17:31 WG2075215
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 06/10/2023 17:31 WG2075215
Methyl tert-butyl ether ND 0.00100 1 06/10/2023 17:31 WG2075215
Naphthalene ND 0.00500 1 06/10/2023 17:31 WG2075215
n-Propylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Styrene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1,1,2-Tetrachloroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1,2,2-Tetrachloroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
Tetrachloroethene ND 0.00100 1 06/10/2023 17:31 WG2075215
Toluene 0.00214 0.00100 1 06/10/2023 17:31 WG2075215
1,2,3-Trichlorobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,2,4-Trichlorobenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1,1-Trichloroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
1,1,2-Trichloroethane ND 0.00100 1 06/10/2023 17:31 WG2075215
Trichloroethene ND 0.00100 1 06/10/2023 17:31 WG2075215
Trichlorofluoromethane ND 0.00500 1 06/10/2023 17:31 WG2075215
1,2,3-Trichloropropane ND 0.00250 1 06/10/2023 17:31 WG2075215
1,2,4-Trimethylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,2,3-Trimethylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
1,3,5-Trimethylbenzene ND 0.00100 1 06/10/2023 17:31 WG2075215
Vinyl chloride ND 0.00100 1 06/10/2023 17:31 WG2075215
Xylenes, Total ND 0.00300 1 06/10/2023 17:31 WG2075215
(S) Toluene-d8 110 80.0-120 06/10/2023 17:31 WG2075215
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1623675
STRENCHSW-1
Collected date/time: 06/06/23 08:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) 4-Bromofluorobenzene 97.4 77.0-126 06/10/2023 17:31 WG2075215
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 06/10/2023 17:31 WG2075215
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range 0.159 0.100 1 06/15/2023 14:57 WG2073742
C28-C40 Oil Range 0.146 0.100 1 06/15/2023 14:57 WG2073742
(S) o-Terphenyl 85.3 52.0-156 06/15/2023 14:57 WG2073742
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
PCB 1221 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
PCB 1232 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
PCB 1242 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
PCB 1248 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
PCB 1254 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
PCB 1260 ND 0.000525 1.05 06/10/2023 14:24 WG2074397
(S) Decachlorobiphenyl 42.6 10.0-128 06/10/2023 14:24 WG2074397
(S) Tetrachloro-m-xylene 43.8 10.0-127 06/10/2023 14:24 WG2074397
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND J3 0.00111 1.11 06/10/2023 03:37 WG2074753
Acenaphthylene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Anthracene ND J3 0.00111 1.11 06/10/2023 03:37 WG2074753
Benzidine ND J3 J4 0.0111 1.11 06/10/2023 03:37 WG2074753
Benzo(a)anthracene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Benzo(b)fluoranthene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Benzo(k)fluoranthene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Benzo(g,h,i)perylene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Benzo(a)pyrene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Bis(2-chlorethoxy)methane ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Bis(2-chloroethyl)ether ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2,2-Oxybis(1-Chloropropane) ND 0.0111 1.11 06/10/2023 03:37 WG2074753
4-Bromophenyl-phenylether ND J3 0.0111 1.11 06/10/2023 03:37 WG2074753
2-Chloronaphthalene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
4-Chlorophenyl-phenylether ND J3 0.0111 1.11 06/10/2023 03:37 WG2074753
Chrysene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Dibenz(a,h)anthracene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
1,2-Dichlorobenzene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
1,3-Dichlorobenzene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
1,4-Dichlorobenzene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
3,3-Dichlorobenzidine ND J3 0.0111 1.11 06/10/2023 03:37 WG2074753
2,4-Dinitrotoluene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2,6-Dinitrotoluene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Fluoranthene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Fluorene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Hexachlorobenzene ND J3 0.00111 1.11 06/10/2023 03:37 WG2074753
Hexachloro-1,3-butadiene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Hexachlorocyclopentadiene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Hexachloroethane ND 0.0111 1.11 06/10/2023 03:37 WG2074753
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1623675
STRENCHSW-1
Collected date/time: 06/06/23 08:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Indeno(1,2,3-cd)pyrene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Isophorone ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Naphthalene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Nitrobenzene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
n-Nitrosodimethylamine ND 0.0111 1.11 06/10/2023 03:37 WG2074753
n-Nitrosodiphenylamine ND 0.0111 1.11 06/10/2023 03:37 WG2074753
n-Nitrosodi-n-propylamine ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Phenanthrene ND 0.00111 1.11 06/10/2023 03:37 WG2074753
Benzylbutyl phthalate ND 0.00333 1.11 06/10/2023 03:37 WG2074753
Bis(2-ethylhexyl)phthalate ND 0.00333 1.11 06/10/2023 03:37 WG2074753
Di-n-butyl phthalate ND 0.00333 1.11 06/10/2023 03:37 WG2074753
Diethyl phthalate ND 0.00333 1.11 06/10/2023 03:37 WG2074753
Dimethyl phthalate ND 0.00333 1.11 06/10/2023 03:37 WG2074753
Di-n-octyl phthalate ND 0.00333 1.11 06/10/2023 03:37 WG2074753
Pyrene ND J3 0.00111 1.11 06/10/2023 03:37 WG2074753
1,2,4-Trichlorobenzene ND 0.0111 1.11 06/10/2023 03:37 WG2074753
4-Chloro-3-methylphenol ND J4 0.0111 1.11 06/10/2023 03:37 WG2074753
2-Chlorophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2,4-Dichlorophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2,4-Dimethylphenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
4,6-Dinitro-2-methylphenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2,4-Dinitrophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2-Nitrophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
4-Nitrophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Pentachlorophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
Phenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
2,4,6-Trichlorophenol ND 0.0111 1.11 06/10/2023 03:37 WG2074753
(S) 2-Fluorophenol 37.0 10.0-120 06/10/2023 03:37 WG2074753
(S) Phenol-d5 20.3 10.0-120 06/10/2023 03:37 WG2074753
(S) Nitrobenzene-d5 55.2 10.0-127 06/10/2023 03:37 WG2074753
(S) 2-Fluorobiphenyl 54.4 10.0-130 06/10/2023 03:37 WG2074753
(S) 2,4,6-Tribromophenol 59.5 10.0-155 06/10/2023 03:37 WG2074753
(S) p-Terphenyl-d14 62.4 10.0-128 06/10/2023 03:37 WG2074753
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Acenaphthene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Acenaphthylene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Benzo(a)anthracene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Benzo(a)pyrene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Benzo(b)fluoranthene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Benzo(g,h,i)perylene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Benzo(k)fluoranthene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Chrysene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Dibenz(a,h)anthracene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Fluoranthene ND 0.000100 1 06/10/2023 06:24 WG2073722
Fluorene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Naphthalene ND 0.000250 1 06/10/2023 06:24 WG2073722
Phenanthrene ND 0.0000500 1 06/10/2023 06:24 WG2073722
Pyrene ND 0.0000500 1 06/10/2023 06:24 WG2073722
1-Methylnaphthalene ND 0.000250 1 06/10/2023 06:24 WG2073722
2-Methylnaphthalene ND 0.000250 1 06/10/2023 06:24 WG2073722
2-Chloronaphthalene ND 0.000250 1 06/10/2023 06:24 WG2073722
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Tetra Tech Inc. - UT RECYCLED EARTH L1623675 06/20/23 14:44 8 of 32
SAMPLE RESULTS - 01
L1623675
STRENCHSW-1
Collected date/time: 06/06/23 08:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Nitrobenzene-d5 87.9 31.0-160 06/10/2023 06:24 WG2073722
(S) 2-Fluorobiphenyl 75.3 48.0-148 06/10/2023 06:24 WG2073722
(S) p-Terphenyl-d14 76.8 37.0-146 06/10/2023 06:24 WG2073722
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1623675 06/20/23 13:53 9 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Tetra Tech Inc. - UT RECYCLED EARTH L1623675 06/20/23 14:44 9 of 32
QUALITY CONTROL SUMMARYWG2076380
Total Solids by Method 2540 B-2015 L1623675-01
Method Blank (MB)
(MB) R3936415-1 06/13/23 08:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Total Solids 0.000
L1623675-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1623675-01 06/13/23 08:43 • (DUP) R3936415-3 06/13/23 08:43
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Total Solids 596 595 1 0.168 5
Laboratory Control Sample (LCS)
(LCS) R3936415-2 06/13/23 08:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Total Solids 9500 9800 103 92.5-108
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2073813
Wet Chemistry by Method 1664A L1623675-01
Method Blank (MB)
(MB) R3934610-1 06/08/23 21:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3934610-2 06/08/23 21:00 • (LCSD) R3934610-3 06/08/23 21:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 38.6 35.2 96.5 88.0 78.0-114 9.21 20
L1623451-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1623451-02 06/08/23 21:00 • (MS) R3934610-4 06/08/23 21:00
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr) 40.0 7.37 26.0 46.5 1 78.0-114 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2074741
Wet Chemistry by Method 3500Cr C-2011 L1623675-01
Method Blank (MB)
(MB) R3935728-1 06/12/23 07:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Hexavalent Chromium U 0.000150 0.000500
L1623404-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1623404-01 06/12/23 09:17 • (DUP) R3935728-5 06/12/23 09:28
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND ND 1 0.000 20
L1624325-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1624325-01 06/12/23 11:28 • (DUP) R3935728-6 06/12/23 11:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3935728-2 06/12/23 08:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00200 0.00181 90.5 90.0-110
L1623295-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623295-10 06/12/23 08:44 • (MS) R3935728-3 06/12/23 08:55 • (MSD) R3935728-4 06/12/23 09:06
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexavalent Chromium 0.0500 0.000732 0.0492 0.0494 96.9 97.3 1 90.0-110 0.421 20
L1624325-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1624325-02 06/12/23 11:50 • (MS) R3935728-7 06/12/23 12:23
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Hexavalent Chromium 0.0500 2.06 1.99 0.000 1 90.0-110 V
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2075594
Mercury by Method 7470A L1623675-01
Method Blank (MB)
(MB) R3938818-1 06/20/23 12:14
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3938818-2 06/20/23 12:16
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00294 98.0 80.0-120
L1623477-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623477-01 06/20/23 12:18 • (MS) R3938818-3 06/20/23 12:20 • (MSD) R3938818-4 06/20/23 12:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00252 0.00240 84.0 80.0 1 75.0-125 4.88 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2073614
Metals (ICP) by Method 6010B L1623675-01
Method Blank (MB)
(MB) R3936940-1 06/14/23 12:09
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic U 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium U 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3936940-2 06/14/23 12:11
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 1.00 100 80.0-120
Arsenic 1.00 1.01 101 80.0-120
Beryllium 1.00 0.985 98.5 80.0-120
Cadmium 1.00 0.984 98.4 80.0-120
Chromium 1.00 0.977 97.7 80.0-120
Copper 1.00 0.986 98.6 80.0-120
Lead 1.00 0.966 96.6 80.0-120
Nickel 1.00 0.993 99.3 80.0-120
Selenium 1.00 0.996 99.6 80.0-120
Silver 0.200 0.192 96.0 80.0-120
Thallium 1.00 0.968 96.8 80.0-120
Zinc 1.00 0.968 96.8 80.0-120
L1623627-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623627-01 06/14/23 12:14 • (MS) R3936940-4 06/14/23 12:20 • (MSD) R3936940-5 06/14/23 12:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 1.04 1.02 104 102 1 75.0-125 1.72 20
Arsenic 1.00 ND 1.04 1.01 104 101 1 75.0-125 2.04 20
Beryllium 1.00 ND 1.02 0.999 102 99.9 1 75.0-125 2.40 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2073614
Metals (ICP) by Method 6010B L1623675-01
L1623627-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623627-01 06/14/23 12:14 • (MS) R3936940-4 06/14/23 12:20 • (MSD) R3936940-5 06/14/23 12:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Cadmium 1.00 ND 1.02 0.996 102 99.6 1 75.0-125 2.06 20
Chromium 1.00 ND 1.00 0.987 100 98.7 1 75.0-125 1.30 20
Lead 1.00 ND 1.00 0.980 100 98.0 1 75.0-125 2.08 20
Nickel 1.00 ND 1.02 1.00 102 100 1 75.0-125 1.91 20
Selenium 1.00 ND 1.02 1.01 101 100 1 75.0-125 0.695 20
Silver 0.200 ND 0.197 0.195 98.7 97.3 1 75.0-125 1.43 20
Thallium 1.00 ND 0.998 0.974 99.8 97.4 1 75.0-125 2.47 20
Zinc 1.00 ND 1.00 0.982 100 98.2 1 75.0-125 2.19 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2076271
Volatile Organic Compounds (GC) by Method 8015D/GRO L1623675-01
Method Blank (MB)
(MB) R3936841-2 06/13/23 04:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 0.0341 J 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)103 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3936841-1 06/13/23 03:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.72 104 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 109 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075215
Volatile Organic Compounds (GC/MS) by Method 8260B L1623675-01
Method Blank (MB)
(MB) R3936098-2 06/10/23 12:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromobenzene U 0.000118 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-Butylbenzene U 0.000125 0.00100
tert-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
2-Chlorotoluene U 0.000106 0.00100
4-Chlorotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
cis-1,2-Dichloroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
1,1-Dichloropropene U 0.000142 0.00100
1,3-Dichloropropane U 0.000110 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
2,2-Dichloropropane U 0.000161 0.00100
Di-isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Hexachloro-1,3-butadiene U 0.000337 0.00100
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075215
Volatile Organic Compounds (GC/MS) by Method 8260B L1623675-01
Method Blank (MB)
(MB) R3936098-2 06/10/23 12:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Isopropylbenzene U 0.000105 0.00100
p-Isopropyltoluene U 0.000120 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK) U 0.000478 0.0100
Methyl tert-butyl ether U 0.000101 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100
1,1,1,2-Tetrachloroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene U 0.000230 0.00100
1,2,4-Trichlorobenzene U 0.000481 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,2,3-Trichloropropane U 0.000237 0.00250
1,2,4-Trimethylbenzene U 0.000322 0.00100
1,2,3-Trimethylbenzene U 0.000104 0.00100
1,3,5-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 112 80.0-120
(S) 4-Bromofluorobenzene 98.8 77.0-126
(S) 1,2-Dichloroethane-d4 95.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3936098-1 06/10/23 11:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Acetone 0.0250 0.0164 65.6 19.0-160
Acrolein 0.0250 0.0160 64.0 10.0-160
Acrylonitrile 0.0250 0.0192 76.8 55.0-149
Benzene 0.00500 0.00484 96.8 70.0-123
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075215
Volatile Organic Compounds (GC/MS) by Method 8260B L1623675-01
Laboratory Control Sample (LCS)
(LCS) R3936098-1 06/10/23 11:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Bromobenzene 0.00500 0.00572 114 73.0-121
Bromodichloromethane 0.00500 0.00498 99.6 75.0-120
Bromoform 0.00500 0.00496 99.2 68.0-132
Bromomethane 0.00500 0.00602 120 10.0-160
n-Butylbenzene 0.00500 0.00585 117 73.0-125
sec-Butylbenzene 0.00500 0.00573 115 75.0-125
tert-Butylbenzene 0.00500 0.00575 115 76.0-124
Carbon tetrachloride 0.00500 0.00521 104 68.0-126
Chlorobenzene 0.00500 0.00589 118 80.0-121
Chlorodibromomethane 0.00500 0.00526 105 77.0-125
Chloroethane 0.00500 0.00475 95.0 47.0-150
Chloroform 0.00500 0.00515 103 73.0-120
Chloromethane 0.00500 0.00493 98.6 41.0-142
2-Chlorotoluene 0.00500 0.00542 108 76.0-123
4-Chlorotoluene 0.00500 0.00514 103 75.0-122
1,2-Dibromo-3-Chloropropane 0.00500 0.00422 84.4 58.0-134
1,2-Dibromoethane 0.00500 0.00510 102 80.0-122
Dibromomethane 0.00500 0.00525 105 80.0-120
1,2-Dichlorobenzene 0.00500 0.00527 105 79.0-121
1,3-Dichlorobenzene 0.00500 0.00555 111 79.0-120
1,4-Dichlorobenzene 0.00500 0.00531 106 79.0-120
Dichlorodifluoromethane 0.00500 0.00486 97.2 51.0-149
1,1-Dichloroethane 0.00500 0.00461 92.2 70.0-126
1,2-Dichloroethane 0.00500 0.00465 93.0 70.0-128
1,1-Dichloroethene 0.00500 0.00430 86.0 71.0-124
cis-1,2-Dichloroethene 0.00500 0.00523 105 73.0-120
trans-1,2-Dichloroethene 0.00500 0.00535 107 73.0-120
1,2-Dichloropropane 0.00500 0.00489 97.8 77.0-125
1,1-Dichloropropene 0.00500 0.00479 95.8 74.0-126
1,3-Dichloropropane 0.00500 0.00475 95.0 80.0-120
cis-1,3-Dichloropropene 0.00500 0.00503 101 80.0-123
trans-1,3-Dichloropropene 0.00500 0.00471 94.2 78.0-124
2,2-Dichloropropane 0.00500 0.00519 104 58.0-130
Di-isopropyl ether 0.00500 0.00387 77.4 58.0-138
Ethylbenzene 0.00500 0.00571 114 79.0-123
Hexachloro-1,3-butadiene 0.00500 0.00618 124 54.0-138
Isopropylbenzene 0.00500 0.00571 114 76.0-127
p-Isopropyltoluene 0.00500 0.00562 112 76.0-125
2-Butanone (MEK)0.0250 0.0196 78.4 44.0-160
Methylene Chloride 0.00500 0.00553 111 67.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075215
Volatile Organic Compounds (GC/MS) by Method 8260B L1623675-01
Laboratory Control Sample (LCS)
(LCS) R3936098-1 06/10/23 11:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
4-Methyl-2-pentanone (MIBK) 0.0250 0.0178 71.2 68.0-142
Methyl tert-butyl ether 0.00500 0.00495 99.0 68.0-125
Naphthalene 0.00500 0.00445 89.0 54.0-135
n-Propylbenzene 0.00500 0.00522 104 77.0-124
Styrene 0.00500 0.00567 113 73.0-130
1,1,1,2-Tetrachloroethane 0.00500 0.00514 103 75.0-125
1,1,2,2-Tetrachloroethane 0.00500 0.00384 76.8 65.0-130
1,1,2-Trichlorotrifluoroethane 0.00500 0.00521 104 69.0-132
Tetrachloroethene 0.00500 0.00575 115 72.0-132
Toluene 0.00500 0.00496 99.2 79.0-120
1,2,3-Trichlorobenzene 0.00500 0.00460 92.0 50.0-138
1,2,4-Trichlorobenzene 0.00500 0.00465 93.0 57.0-137
1,1,1-Trichloroethane 0.00500 0.00480 96.0 73.0-124
1,1,2-Trichloroethane 0.00500 0.00509 102 80.0-120
Trichloroethene 0.00500 0.00585 117 78.0-124
Trichlorofluoromethane 0.00500 0.00473 94.6 59.0-147
1,2,3-Trichloropropane 0.00500 0.00455 91.0 73.0-130
1,2,4-Trimethylbenzene 0.00500 0.00512 102 76.0-121
1,2,3-Trimethylbenzene 0.00500 0.00504 101 77.0-120
1,3,5-Trimethylbenzene 0.00500 0.00529 106 76.0-122
Vinyl chloride 0.00500 0.00546 109 67.0-131
Xylenes, Total 0.0150 0.0169 113 79.0-123
(S) Toluene-d8 105 80.0-120
(S) 4-Bromofluorobenzene 99.7 77.0-126
(S) 1,2-Dichloroethane-d4 103 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2073742
Semi-Volatile Organic Compounds (GC) by Method 8015 L1623675-01
Method Blank (MB)
(MB) R3935795-1 06/12/23 11:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
C10-C28 Diesel Range U 0.0222 0.100
C28-C40 Oil Range U 0.0118 0.100
(S) o-Terphenyl 115 52.0-156
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935795-2 06/12/23 11:43 • (LCSD) R3935795-3 06/12/23 12:04
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
C10-C28 Diesel Range 1.50 1.54 1.60 103 107 50.0-150 3.82 20
(S) o-Terphenyl 123 124 52.0-156
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2074397
Polychlorinated Biphenyls (GC) by Method 8082 L1623675-01
Method Blank (MB)
(MB) R3935429-1 06/10/23 13:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
(S) Decachlorobiphenyl 53.8 10.0-128
(S) Tetrachloro-m-xylene 69.6 10.0-127
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935429-4 06/10/23 13:48 • (LCSD) R3935429-5 06/10/23 13:57
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 0.00182 0.00186 72.8 74.4 36.0-135 2.17 29
PCB 1260 0.00250 0.00165 0.00148 66.0 59.2 42.0-131 10.9 25
(S) Decachlorobiphenyl 32.3 33.5 10.0-128
(S) Tetrachloro-m-xylene 67.8 75.5 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2074753
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1623675-01
Method Blank (MB)
(MB) R3935552-3 06/09/23 23:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate 0.00106 J 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2074753
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1623675-01
Method Blank (MB)
(MB) R3935552-3 06/09/23 23:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol U 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 23.5 10.0-120
(S) Phenol-d5 14.4 10.0-120
(S) Nitrobenzene-d5 45.9 10.0-127
(S) 2-Fluorobiphenyl 43.9 10.0-130
(S) 2,4,6-Tribromophenol 56.0 10.0-155
(S) p-Terphenyl-d14 67.3 10.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935552-1 06/09/23 23:15 • (LCSD) R3935552-2 06/09/23 23:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 0.0246 0.0310 49.2 62.0 41.0-120 J3 23.0 22
Acenaphthylene 0.0500 0.0258 0.0314 51.6 62.8 43.0-120 19.6 22
Anthracene 0.0500 0.0277 0.0344 55.4 68.8 45.0-120 J3 21.6 20
Benzidine 0.100 0.00597 0.0168 5.97 16.8 10.0-120 J4 J3 95.1 36
Benzo(a)anthracene 0.0500 0.0342 0.0417 68.4 83.4 47.0-120 19.8 20
Benzo(b)fluoranthene 0.0500 0.0328 0.0377 65.6 75.4 46.0-120 13.9 20
Benzo(k)fluoranthene 0.0500 0.0313 0.0364 62.6 72.8 46.0-120 15.1 21
Benzo(g,h,i)perylene 0.0500 0.0283 0.0336 56.6 67.2 48.0-121 17.1 20
Benzo(a)pyrene 0.0500 0.0314 0.0358 62.8 71.6 47.0-120 13.1 20
Bis(2-chlorethoxy)methane 0.0500 0.0225 0.0276 45.0 55.2 33.0-120 20.4 24
Bis(2-chloroethyl)ether 0.0500 0.0222 0.0272 44.4 54.4 23.0-120 20.2 33
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2074753
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1623675-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935552-1 06/09/23 23:15 • (LCSD) R3935552-2 06/09/23 23:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
2,2-Oxybis(1-Chloropropane) 0.0500 0.0225 0.0264 45.0 52.8 28.0-120 16.0 31
4-Bromophenyl-phenylether 0.0500 0.0283 0.0349 56.6 69.8 45.0-120 J3 20.9 20
2-Chloronaphthalene 0.0500 0.0238 0.0297 47.6 59.4 37.0-120 22.1 25
4-Chlorophenyl-phenylether 0.0500 0.0268 0.0330 53.6 66.0 44.0-120 J3 20.7 20
Chrysene 0.0500 0.0309 0.0364 61.8 72.8 48.0-120 16.3 20
Dibenz(a,h)anthracene 0.0500 0.0295 0.0351 59.0 70.2 47.0-120 17.3 20
1,2-Dichlorobenzene 0.0500 0.0197 0.0248 39.4 49.6 20.0-120 22.9 34
1,3-Dichlorobenzene 0.0500 0.0197 0.0242 39.4 48.4 17.0-120 20.5 35
1,4-Dichlorobenzene 0.0500 0.0203 0.0254 40.6 50.8 18.0-120 22.3 34
3,3-Dichlorobenzidine 0.100 0.0624 0.0810 62.4 81.0 44.0-120 J3 25.9 20
2,4-Dinitrotoluene 0.0500 0.0328 0.0379 65.6 75.8 49.0-124 14.4 20
2,6-Dinitrotoluene 0.0500 0.0276 0.0317 55.2 63.4 46.0-120 13.8 21
Fluoranthene 0.0500 0.0304 0.0347 60.8 69.4 51.0-120 13.2 20
Fluorene 0.0500 0.0268 0.0326 53.6 65.2 47.0-120 19.5 20
Hexachlorobenzene 0.0500 0.0284 0.0351 56.8 70.2 44.0-120 J3 21.1 20
Hexachloro-1,3-butadiene 0.0500 0.0205 0.0267 41.0 53.4 19.0-120 26.3 32
Hexachlorocyclopentadiene 0.0500 0.0148 0.0168 29.6 33.6 15.0-120 12.7 31
Hexachloroethane 0.0500 0.0198 0.0237 39.6 47.4 15.0-120 17.9 37
Indeno(1,2,3-cd)pyrene 0.0500 0.0255 0.0291 51.0 58.2 49.0-122 13.2 20
Isophorone 0.0500 0.0223 0.0271 44.6 54.2 36.0-120 19.4 23
Naphthalene 0.0500 0.0221 0.0267 44.2 53.4 27.0-120 18.9 27
Nitrobenzene 0.0500 0.0203 0.0250 40.6 50.0 27.0-120 20.8 29
n-Nitrosodimethylamine 0.0500 0.0315 0.0323 63.0 64.6 10.0-120 2.51 40
n-Nitrosodiphenylamine 0.0500 0.0264 0.0316 52.8 63.2 47.0-120 17.9 20
n-Nitrosodi-n-propylamine 0.0500 0.0231 0.0286 46.2 57.2 31.0-120 21.3 28
Phenanthrene 0.0500 0.0291 0.0346 58.2 69.2 46.0-120 17.3 20
Benzylbutyl phthalate 0.0500 0.0327 0.0399 65.4 79.8 43.0-121 19.8 20
Bis(2-ethylhexyl)phthalate 0.0500 0.0325 0.0384 65.0 76.8 43.0-122 16.6 20
Di-n-butyl phthalate 0.0500 0.0338 0.0402 67.6 80.4 49.0-121 17.3 20
Diethyl phthalate 0.0500 0.0318 0.0359 63.6 71.8 48.0-122 12.1 20
Dimethyl phthalate 0.0500 0.0283 0.0332 56.6 66.4 48.0-120 15.9 20
Di-n-octyl phthalate 0.0500 0.0311 0.0367 62.2 73.4 42.0-125 16.5 20
Pyrene 0.0500 0.0307 0.0377 61.4 75.4 47.0-120 J3 20.5 20
1,2,4-Trichlorobenzene 0.0500 0.0195 0.0253 39.0 50.6 24.0-120 25.9 29
4-Chloro-3-methylphenol 0.0500 0.0197 0.0218 39.4 43.6 40.0-120 J4 10.1 21
2-Chlorophenol 0.0500 0.0177 0.0191 35.4 38.2 25.0-120 7.61 35
2,4-Dichlorophenol 0.0500 0.0186 0.0210 37.2 42.0 36.0-120 12.1 26
2,4-Dimethylphenol 0.0500 0.0209 0.0222 41.8 44.4 33.0-120 6.03 26
4,6-Dinitro-2-methylphenol 0.0500 0.0367 0.0390 73.4 78.0 38.0-138 6.08 25
2,4-Dinitrophenol 0.0500 0.0355 0.0353 71.0 70.6 10.0-120 0.565 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2074753
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1623675-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935552-1 06/09/23 23:15 • (LCSD) R3935552-2 06/09/23 23:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
2-Nitrophenol 0.0500 0.0218 0.0244 43.6 48.8 31.0-120 11.3 29
4-Nitrophenol 0.0500 0.0102 0.0109 20.4 21.8 10.0-120 6.64 33
Pentachlorophenol 0.0500 0.0292 0.0309 58.4 61.8 23.0-120 5.66 25
Phenol 0.0500 0.00996 0.0102 19.9 20.4 10.0-120 2.38 36
2,4,6-Trichlorophenol 0.0500 0.0260 0.0291 52.0 58.2 42.0-120 11.3 23
(S) 2-Fluorophenol 26.4 29.8 10.0-120
(S) Phenol-d5 17.5 18.6 10.0-120
(S) Nitrobenzene-d5 42.4 50.1 10.0-127
(S) 2-Fluorobiphenyl 47.2 57.4 10.0-130
(S) 2,4,6-Tribromophenol 58.5 68.0 10.0-155
(S) p-Terphenyl-d14 63.3 76.4 10.0-128
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2073722
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1623675-01
Method Blank (MB)
(MB) R3935388-2 06/10/23 01:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Anthracene U 0.0000190 0.0000500
Acenaphthene U 0.0000190 0.0000500
Acenaphthylene U 0.0000171 0.0000500
Benzo(a)anthracene U 0.0000203 0.0000500
Benzo(a)pyrene U 0.0000184 0.0000500
Benzo(b)fluoranthene U 0.0000168 0.0000500
Benzo(g,h,i)perylene U 0.0000184 0.0000500
Benzo(k)fluoranthene U 0.0000202 0.0000500
Chrysene U 0.0000179 0.0000500
Dibenz(a,h)anthracene U 0.0000160 0.0000500
Fluoranthene U 0.0000270 0.000100
Fluorene U 0.0000169 0.0000500
Indeno(1,2,3-cd)pyrene U 0.0000158 0.0000500
Naphthalene U 0.0000917 0.000250
Phenanthrene U 0.0000180 0.0000500
Pyrene U 0.0000169 0.0000500
1-Methylnaphthalene U 0.0000687 0.000250
2-Methylnaphthalene U 0.0000674 0.000250
2-Chloronaphthalene U 0.0000682 0.000250
(S) Nitrobenzene-d5 113 31.0-160
(S) 2-Fluorobiphenyl 86.5 48.0-148
(S) p-Terphenyl-d14 95.0 37.0-146
Laboratory Control Sample (LCS)
(LCS) R3935388-1 06/10/23 01:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Anthracene 0.00200 0.00174 87.0 67.0-150
Acenaphthene 0.00200 0.00177 88.5 65.0-138
Acenaphthylene 0.00200 0.00186 93.0 66.0-140
Benzo(a)anthracene 0.00200 0.00185 92.5 61.0-140
Benzo(a)pyrene 0.00200 0.00189 94.5 60.0-143
Benzo(b)fluoranthene 0.00200 0.00191 95.5 58.0-141
Benzo(g,h,i)perylene 0.00200 0.00177 88.5 52.0-153
Benzo(k)fluoranthene 0.00200 0.00179 89.5 58.0-148
Chrysene 0.00200 0.00196 98.0 64.0-144
Dibenz(a,h)anthracene 0.00200 0.00165 82.5 52.0-155
Fluoranthene 0.00200 0.00190 95.0 69.0-153
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2073722
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1623675-01
Laboratory Control Sample (LCS)
(LCS) R3935388-1 06/10/23 01:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Fluorene 0.00200 0.00184 92.0 64.0-136
Indeno(1,2,3-cd)pyrene 0.00200 0.00178 89.0 54.0-153
Naphthalene 0.00200 0.00196 98.0 61.0-137
Phenanthrene 0.00200 0.00192 96.0 62.0-137
Pyrene 0.00200 0.00216 108 60.0-142
1-Methylnaphthalene 0.00200 0.00197 98.5 66.0-142
2-Methylnaphthalene 0.00200 0.00186 93.0 62.0-136
2-Chloronaphthalene 0.00200 0.00191 95.5 64.0-140
(S) Nitrobenzene-d5 113 31.0-160
(S) 2-Fluorobiphenyl 87.0 48.0-148
(S) p-Terphenyl-d14 93.5 37.0-146
L1623598-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623598-06 06/10/23 03:48 • (MS) R3935388-3 06/10/23 04:05 • (MSD) R3935388-4 06/10/23 04:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Anthracene 0.00190 ND 0.00168 0.00167 88.4 87.9 1 56.0-156 0.597 20
Acenaphthene 0.00190 ND 0.00170 0.00169 89.5 88.9 1 44.0-153 0.590 20
Acenaphthylene 0.00190 ND 0.00178 0.00177 93.7 93.2 1 53.0-150 0.563 20
Benzo(a)anthracene 0.00190 ND 0.00170 0.00174 89.5 91.6 1 47.0-151 2.33 20
Benzo(a)pyrene 0.00190 ND 0.00178 0.00184 93.7 96.8 1 45.0-146 3.31 20
Benzo(b)fluoranthene 0.00190 ND 0.00180 0.00184 94.7 96.8 1 43.0-142 2.20 20
Benzo(g,h,i)perylene 0.00190 ND 0.00165 0.00173 86.8 91.1 1 40.0-147 4.73 20
Benzo(k)fluoranthene 0.00190 ND 0.00167 0.00173 87.9 91.1 1 43.0-148 3.53 21
Chrysene 0.00190 ND 0.00188 0.00191 98.9 101 1 50.0-148 1.58 20
Dibenz(a,h)anthracene 0.00190 ND 0.00152 0.00155 80.0 81.6 1 37.0-151 1.95 20
Fluoranthene 0.00190 ND 0.00182 0.00185 95.8 97.4 1 56.0-157 1.63 20
Fluorene 0.00190 ND 0.00177 0.00175 93.2 92.1 1 48.0-148 1.14 20
Indeno(1,2,3-cd)pyrene 0.00190 ND 0.00162 0.00168 85.3 88.4 1 41.0-148 3.64 20
Naphthalene 0.00190 ND 0.00189 0.00192 99.5 101 1 10.0-160 1.57 20
Phenanthrene 0.00190 ND 0.00181 0.00187 95.3 98.4 1 47.0-147 3.26 20
Pyrene 0.00190 ND 0.00207 0.00210 109 111 1 51.0-148 1.44 20
1-Methylnaphthalene 0.00190 ND 0.00191 0.00192 101 101 1 21.0-160 0.522 20
2-Methylnaphthalene 0.00190 ND 0.00176 0.00177 92.6 93.2 1 31.0-160 0.567 20
2-Chloronaphthalene 0.00190 ND 0.00183 0.00183 96.3 96.3 1 52.0-148 0.000 20
(S) Nitrobenzene-d5 111 109 31.0-160
(S) 2-Fluorobiphenyl 89.5 93.2 48.0-148
(S) p-Terphenyl-d14 93.2 93.7 37.0-146
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2073722
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1623675-01
L1623694-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623694-01 06/10/23 07:51 • (MS) R3935388-5 06/10/23 08:08 • (MSD) R3935388-6 06/10/23 08:25
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Anthracene 0.00190 ND 0.00168 0.00164 87.2 85.1 1 56.0-156 2.41 20
Acenaphthene 0.00190 ND 0.00172 0.00167 90.5 87.9 1 44.0-153 2.95 20
Acenaphthylene 0.00190 ND 0.00178 0.00173 93.7 91.1 1 53.0-150 2.85 20
Benzo(a)anthracene 0.00190 0.0000813 0.00175 0.00170 87.8 85.2 1 47.0-151 2.90 20
Benzo(a)pyrene 0.00190 0.000144 0.00182 0.00176 88.2 85.1 1 45.0-146 3.35 20
Benzo(b)fluoranthene 0.00190 0.0000515 0.00185 0.00181 94.7 92.6 1 43.0-142 2.19 20
Benzo(g,h,i)perylene 0.00190 0.000133 0.00166 0.00162 80.4 78.3 1 40.0-147 2.44 20
Benzo(k)fluoranthene 0.00190 ND 0.00172 0.00167 90.5 87.9 1 43.0-148 2.95 21
Chrysene 0.00190 0.0000848 0.00194 0.00185 97.6 92.9 1 50.0-148 4.75 20
Dibenz(a,h)anthracene 0.00190 ND 0.00147 0.00143 75.1 73.0 1 37.0-151 2.76 20
Fluoranthene 0.00190 ND 0.00185 0.00177 97.4 93.2 1 56.0-157 4.42 20
Fluorene 0.00190 ND 0.00182 0.00178 95.8 93.7 1 48.0-148 2.22 20
Indeno(1,2,3-cd)pyrene 0.00190 ND 0.00167 0.00162 86.3 83.7 1 41.0-148 3.04 20
Naphthalene 0.00190 ND 0.00190 0.00185 100 97.4 1 10.0-160 2.67 20
Phenanthrene 0.00190 ND 0.00186 0.00179 95.7 92.0 1 47.0-147 3.84 20
Pyrene 0.00190 0.0000766 0.00215 0.00209 109 106 1 51.0-148 2.83 20
1-Methylnaphthalene 0.00190 ND 0.00190 0.00186 100 97.9 1 21.0-160 2.13 20
2-Methylnaphthalene 0.00190 ND 0.00182 0.00176 95.8 92.6 1 31.0-160 3.35 20
2-Chloronaphthalene 0.00190 ND 0.00184 0.00178 96.8 93.7 1 52.0-148 3.31 20
(S) Nitrobenzene-d5 112 108 31.0-160
(S) 2-Fluorobiphenyl 91.1 88.4 48.0-148
(S) p-Terphenyl-d14 96.3 92.6 37.0-146
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
July 03, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1629899
Samples Received:06/10/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
July 03, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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July 03, 2023
Chris Ward
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
CB-8 L1629899-01 5
CB-9 L1629899-02 6
DUP-5 L1629899-03 7
Qc: Quality Control Summary 8
Total Solids by Method 2540 G-2011 8
Metals (ICP) by Method 6010B 9
Gl: Glossary of Terms 11
Al: Accreditations & Locations 12
Sc: Sample Chain of Custody 13
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CB-8 L1629899-01 Solid RT 06/09/23 13:50 06/10/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2075981 1 06/13/23 11:22 06/13/23 11:32 JAV Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2087695 1 06/30/23 16:58 07/03/23 08:50 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-9 L1629899-02 Solid RT 06/09/23 13:15 06/10/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2075981 1 06/13/23 11:22 06/13/23 11:32 JAV Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2087695 1 06/30/23 16:58 07/03/23 08:53 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
DUP-5 L1629899-03 Solid RT 06/09/23 00:00 06/10/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2075981 1 06/13/23 11:22 06/13/23 11:32 JAV Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2087695 1 06/30/23 16:58 07/03/23 09:02 ZSA Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1629899
CB-8
Collected date/time: 06/09/23 13:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 71.1 1 06/13/2023 11:32 WG2075981
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.81 1 07/03/2023 08:50 WG2087695
Arsenic 17.5 2.81 1 07/03/2023 08:50 WG2087695
Beryllium ND 0.281 1 07/03/2023 08:50 WG2087695
Cadmium ND 0.704 1 07/03/2023 08:50 WG2087695
Chromium 38.1 1.41 1 07/03/2023 08:50 WG2087695
Copper 43.3 2.81 1 07/03/2023 08:50 WG2087695
Lead 10.6 0.704 1 07/03/2023 08:50 WG2087695
Nickel 19.6 2.81 1 07/03/2023 08:50 WG2087695
Selenium ND 2.81 1 07/03/2023 08:50 WG2087695
Silver ND 1.41 1 07/03/2023 08:50 WG2087695
Thallium ND 2.81 1 07/03/2023 08:50 WG2087695
Zinc 45.3 7.04 1 07/03/2023 08:50 WG2087695
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1629899
CB-9
Collected date/time: 06/09/23 13:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.4 1 06/13/2023 11:32 WG2075981
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.52 1 07/03/2023 08:53 WG2087695
Arsenic 9.28 B 2.52 1 07/03/2023 08:53 WG2087695
Beryllium ND 0.252 1 07/03/2023 08:53 WG2087695
Cadmium ND 0.629 1 07/03/2023 08:53 WG2087695
Chromium 10.4 1.26 1 07/03/2023 08:53 WG2087695
Copper 16.4 2.52 1 07/03/2023 08:53 WG2087695
Lead 2.59 0.629 1 07/03/2023 08:53 WG2087695
Nickel 5.49 2.52 1 07/03/2023 08:53 WG2087695
Selenium ND 2.52 1 07/03/2023 08:53 WG2087695
Silver ND 1.26 1 07/03/2023 08:53 WG2087695
Thallium ND 2.52 1 07/03/2023 08:53 WG2087695
Zinc 18.5 6.29 1 07/03/2023 08:53 WG2087695
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1629899
DUP-5
Collected date/time: 06/09/23 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.5 1 06/13/2023 11:32 WG2075981
Metals (ICP) by Method 6010B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.42 1 07/03/2023 09:02 WG2087695
Arsenic 12.4 2.42 1 07/03/2023 09:02 WG2087695
Beryllium ND 0.242 1 07/03/2023 09:02 WG2087695
Cadmium ND 0.606 1 07/03/2023 09:02 WG2087695
Chromium 29.7 1.21 1 07/03/2023 09:02 WG2087695
Copper 36.9 2.42 1 07/03/2023 09:02 WG2087695
Lead 6.54 0.606 1 07/03/2023 09:02 WG2087695
Nickel 14.1 2.42 1 07/03/2023 09:02 WG2087695
Selenium ND 2.42 1 07/03/2023 09:02 WG2087695
Silver ND 1.21 1 07/03/2023 09:02 WG2087695
Thallium ND 2.42 1 07/03/2023 09:02 WG2087695
Zinc 37.4 6.06 1 07/03/2023 09:02 WG2087695
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075981
Total Solids by Method 2540 G-2011 L1629899-01,02,03
Method Blank (MB)
(MB) R3936404-1 06/13/23 11:32
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1624935-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1624935-01 06/13/23 11:32 • (DUP) R3936404-3 06/13/23 11:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 71.1 70.6 1 0.635 10
Laboratory Control Sample (LCS)
(LCS) R3936404-2 06/13/23 11:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.2 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2087695
Metals (ICP) by Method 6010B L1629899-01,02,03
Method Blank (MB)
(MB) R3944158-1 07/03/23 08:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.544 2.00
Arsenic 0.939 J 0.518 2.00
Beryllium U 0.0315 0.200
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Copper U 0.400 2.00
Lead U 0.208 0.500
Nickel U 0.132 2.00
Selenium U 0.764 2.00
Silver U 0.127 1.00
Thallium U 0.394 2.00
Zinc U 0.832 5.00
Laboratory Control Sample (LCS)
(LCS) R3944158-2 07/03/23 08:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Antimony 100 96.7 96.7 80.0-120
Arsenic 100 97.0 97.0 80.0-120
Beryllium 100 96.5 96.5 80.0-120
Cadmium 100 95.1 95.1 80.0-120
Chromium 100 94.6 94.6 80.0-120
Copper 100 95.5 95.5 80.0-120
Lead 100 94.4 94.4 80.0-120
Nickel 100 95.1 95.1 80.0-120
Selenium 100 94.3 94.3 80.0-120
Silver 20.0 18.5 92.5 80.0-120
Thallium 100 95.0 95.0 80.0-120
Zinc 100 93.1 93.1 80.0-120
L1631045-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631045-07 07/03/23 08:34 • (MS) R3944158-5 07/03/23 08:42 • (MSD) R3944158-6 07/03/23 08:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 100 ND 43.3 47.6 43.3 47.6 1 75.0-125 J6 J6 9.45 20
Arsenic 100 11.1 112 118 101 107 1 75.0-125 5.52 20
Beryllium 100 0.670 95.2 99.7 94.5 99.0 1 75.0-125 4.63 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2087695
Metals (ICP) by Method 6010B L1629899-01,02,03
L1631045-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631045-07 07/03/23 08:34 • (MS) R3944158-5 07/03/23 08:42 • (MSD) R3944158-6 07/03/23 08:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Cadmium 100 ND 100 107 99.9 107 1 75.0-125 6.50 20
Chromium 100 18.8 112 115 92.7 95.8 1 75.0-125 2.75 20
Copper 100 17.3 119 122 102 104 1 75.0-125 2.39 20
Lead 100 6.47 103 108 96.8 102 1 75.0-125 4.53 20
Nickel 100 17.1 115 117 97.7 99.7 1 75.0-125 1.75 20
Selenium 100 ND 98.6 104 98.6 104 1 75.0-125 5.10 20
Silver 20.0 ND 19.7 21.1 98.6 105 1 75.0-125 6.59 20
Thallium 100 ND 94.9 99.8 94.9 99.8 1 75.0-125 5.07 20
Zinc 100 34.2 123 122 89.2 88.1 1 75.0-125 0.852 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
June 22, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1624935
Samples Received:06/10/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
June 22, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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June 22, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
CB-8 L1624935-01 5
CB-9 L1624935-02 9
DUP-5 L1624935-03 13
Qc: Quality Control Summary 17
Total Solids by Method 2540 G-2011 17
Volatile Organic Compounds (GC) by Method 8015D/GRO 18
Volatile Organic Compounds (GC/MS) by Method 8260B 19
Semi-Volatile Organic Compounds (GC) by Method 8015 24
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 25
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 30
Gl: Glossary of Terms 35
Al: Accreditations & Locations 36
Sc: Sample Chain of Custody 37
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
CB-8 L1624935-01 Solid RT 06/09/23 13:50 06/10/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2075981 1 06/13/23 11:22 06/13/23 11:32 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2078791 25 06/09/23 13:50 06/16/23 03:50 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2078708 1 06/09/23 13:50 06/16/23 01:54 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2079280 1 06/09/23 13:50 06/18/23 17:39 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2077992 20 06/16/23 08:00 06/16/23 15:49 HLJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2075724 10 06/14/23 08:56 06/15/23 18:33 AED Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2078829 1 06/16/23 08:08 06/16/23 18:27 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
CB-9 L1624935-02 Solid RT 06/09/23 13:15 06/10/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2075981 1 06/13/23 11:22 06/13/23 11:32 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2078791 25 06/09/23 13:15 06/16/23 04:15 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2078708 1 06/09/23 13:15 06/16/23 02:13 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2079280 1 06/09/23 13:15 06/18/23 18:00 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2077992 20 06/16/23 08:00 06/16/23 16:29 HLJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2075724 10 06/14/23 08:56 06/15/23 01:30 KLZ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2077933 1 06/15/23 12:41 06/15/23 23:19 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
DUP-5 L1624935-03 Solid RT 06/09/23 00:00 06/10/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2075981 1 06/13/23 11:22 06/13/23 11:32 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2078791 25 06/09/23 00:00 06/16/23 04:39 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2078708 1 06/09/23 00:00 06/16/23 02:33 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2079280 1 06/09/23 00:00 06/18/23 18:21 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2077992 4 06/16/23 08:00 06/17/23 09:12 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2075724 1 06/14/23 08:56 06/14/23 21:20 KLZ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2077933 1 06/15/23 12:41 06/15/23 23:00 DSH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1624935
CB-8
Collected date/time: 06/09/23 13:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 71.1 1 06/13/2023 11:32 WG2075981
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 4.67 25 06/16/2023 03:50 WG2078791
(S) a,a,a-Trifluorotoluene(FID) 101 77.0-120 06/16/2023 03:50 WG2078791
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0922 1 06/16/2023 01:54 WG2078708
Acrylonitrile ND 0.0230 1 06/16/2023 01:54 WG2078708
Benzene 0.00398 0.00184 1 06/16/2023 01:54 WG2078708
Bromobenzene ND 0.0230 1 06/16/2023 01:54 WG2078708
Bromodichloromethane ND 0.00461 1 06/16/2023 01:54 WG2078708
Bromoform ND 0.0461 1 06/16/2023 01:54 WG2078708
Bromomethane ND 0.0230 1 06/16/2023 01:54 WG2078708
n-Butylbenzene ND 0.0230 1 06/16/2023 01:54 WG2078708
sec-Butylbenzene ND 0.0230 1 06/16/2023 01:54 WG2078708
tert-Butylbenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
Carbon tetrachloride ND 0.00922 1 06/16/2023 01:54 WG2078708
Chlorobenzene ND 0.00461 1 06/16/2023 01:54 WG2078708
Chlorodibromomethane ND 0.00461 1 06/16/2023 01:54 WG2078708
Chloroethane ND 0.00922 1 06/16/2023 01:54 WG2078708
Chloroform ND 0.00461 1 06/16/2023 01:54 WG2078708
Chloromethane ND 0.0230 1 06/16/2023 01:54 WG2078708
2-Chlorotoluene ND 0.00461 1 06/16/2023 01:54 WG2078708
4-Chlorotoluene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,2-Dibromo-3-Chloropropane ND 0.0461 1 06/16/2023 01:54 WG2078708
1,2-Dibromoethane ND 0.00461 1 06/16/2023 01:54 WG2078708
Dibromomethane ND 0.00922 1 06/16/2023 01:54 WG2078708
1,2-Dichlorobenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,3-Dichlorobenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,4-Dichlorobenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
Dichlorodifluoromethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,1-Dichloroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,2-Dichloroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,1-Dichloroethene ND 0.00461 1 06/16/2023 01:54 WG2078708
cis-1,2-Dichloroethene ND 0.00461 1 06/16/2023 01:54 WG2078708
trans-1,2-Dichloroethene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,2-Dichloropropane ND 0.00922 1 06/16/2023 01:54 WG2078708
1,1-Dichloropropene ND 0.00461 1 06/16/2023 01:54 WG2078708
1,3-Dichloropropane ND 0.00922 1 06/16/2023 01:54 WG2078708
cis-1,3-Dichloropropene ND 0.00461 1 06/16/2023 01:54 WG2078708
trans-1,3-Dichloropropene ND 0.00922 1 06/16/2023 01:54 WG2078708
2,2-Dichloropropane ND 0.00461 1 06/16/2023 01:54 WG2078708
Di-isopropyl ether ND 0.00184 1 06/16/2023 01:54 WG2078708
Ethylbenzene 0.0184 0.00461 1 06/16/2023 01:54 WG2078708
Hexachloro-1,3-butadiene ND 0.0461 1 06/16/2023 01:54 WG2078708
Isopropylbenzene 0.00934 0.00461 1 06/16/2023 01:54 WG2078708
p-Isopropyltoluene ND 0.00922 1 06/16/2023 01:54 WG2078708
2-Butanone (MEK)ND 0.184 1 06/16/2023 01:54 WG2078708
Methylene Chloride ND 0.0461 1 06/16/2023 01:54 WG2078708
4-Methyl-2-pentanone (MIBK) ND 0.0461 1 06/16/2023 01:54 WG2078708
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1624935
CB-8
Collected date/time: 06/09/23 13:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Methyl tert-butyl ether ND 0.00187 1 06/18/2023 17:39 WG2079280
Naphthalene ND 0.0230 1 06/16/2023 01:54 WG2078708
n-Propylbenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
Styrene ND 0.0230 1 06/16/2023 01:54 WG2078708
1,1,1,2-Tetrachloroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,1,2,2-Tetrachloroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,1,2-Trichlorotrifluoroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
Tetrachloroethene 0.558 0.00461 1 06/16/2023 01:54 WG2078708
Toluene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,2,3-Trichlorobenzene ND 0.0230 1 06/16/2023 01:54 WG2078708
1,2,4-Trichlorobenzene ND 0.0230 1 06/16/2023 01:54 WG2078708
1,1,1-Trichloroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,1,2-Trichloroethane ND 0.00461 1 06/16/2023 01:54 WG2078708
Trichloroethene 0.0129 0.00184 1 06/16/2023 01:54 WG2078708
Trichlorofluoromethane ND 0.00461 1 06/16/2023 01:54 WG2078708
1,2,3-Trichloropropane ND 0.0230 1 06/16/2023 01:54 WG2078708
1,2,4-Trimethylbenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,2,3-Trimethylbenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
1,3,5-Trimethylbenzene ND 0.00922 1 06/16/2023 01:54 WG2078708
Vinyl chloride ND 0.00461 1 06/16/2023 01:54 WG2078708
Xylenes, Total 0.0662 0.0120 1 06/16/2023 01:54 WG2078708
(S) Toluene-d8 105 75.0-131 06/16/2023 01:54 WG2078708
(S) Toluene-d8 110 75.0-131 06/18/2023 17:39 WG2079280
(S) 4-Bromofluorobenzene 105 67.0-138 06/16/2023 01:54 WG2078708
(S) 4-Bromofluorobenzene 95.8 67.0-138 06/18/2023 17:39 WG2079280
(S) 1,2-Dichloroethane-d4 81.9 70.0-130 06/16/2023 01:54 WG2078708
(S) 1,2-Dichloroethane-d4 86.9 70.0-130 06/18/2023 17:39 WG2079280
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND J6 113 20 06/16/2023 15:49 WG2077992
C28-C40 Oil Range 184 113 20 06/16/2023 15:49 WG2077992
(S) o-Terphenyl 83.5 J7 18.0-148 06/16/2023 15:49 WG2077992
Sample Narrative:
L1624935-01 WG2077992: Cannot run at lower dilution due to viscosity of extract
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.469 10 06/15/2023 18:33 WG2075724
Acenaphthylene ND 0.469 10 06/15/2023 18:33 WG2075724
Anthracene ND 0.469 10 06/15/2023 18:33 WG2075724
Benzidine ND J5 23.5 10 06/15/2023 18:33 WG2075724
Benzo(a)anthracene ND 0.469 10 06/15/2023 18:33 WG2075724
Benzo(b)fluoranthene ND 0.469 10 06/15/2023 18:33 WG2075724
Benzo(k)fluoranthene ND 0.469 10 06/15/2023 18:33 WG2075724
Benzo(g,h,i)perylene ND 0.469 10 06/15/2023 18:33 WG2075724
Benzo(a)pyrene ND 0.469 10 06/15/2023 18:33 WG2075724
Bis(2-chlorethoxy)methane ND 4.69 10 06/15/2023 18:33 WG2075724
Bis(2-chloroethyl)ether ND 4.69 10 06/15/2023 18:33 WG2075724
2,2-Oxybis(1-Chloropropane) ND 4.69 10 06/15/2023 18:33 WG2075724
4-Bromophenyl-phenylether ND 4.69 10 06/15/2023 18:33 WG2075724
2-Chloronaphthalene ND 0.469 10 06/15/2023 18:33 WG2075724
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1624935
CB-8
Collected date/time: 06/09/23 13:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Chlorophenyl-phenylether ND 4.69 10 06/15/2023 18:33 WG2075724
Chrysene ND 0.469 10 06/15/2023 18:33 WG2075724
Dibenz(a,h)anthracene ND 0.469 10 06/15/2023 18:33 WG2075724
3,3-Dichlorobenzidine ND 4.69 10 06/15/2023 18:33 WG2075724
2,4-Dinitrotoluene ND 4.69 10 06/15/2023 18:33 WG2075724
2,6-Dinitrotoluene ND 4.69 10 06/15/2023 18:33 WG2075724
Fluoranthene ND 0.469 10 06/15/2023 18:33 WG2075724
Fluorene ND 0.469 10 06/15/2023 18:33 WG2075724
Hexachlorobenzene ND 4.69 10 06/15/2023 18:33 WG2075724
Hexachloro-1,3-butadiene ND 4.69 10 06/15/2023 18:33 WG2075724
Hexachlorocyclopentadiene ND J6 4.69 10 06/15/2023 18:33 WG2075724
Hexachloroethane ND 4.69 10 06/15/2023 18:33 WG2075724
Indeno(1,2,3-cd)pyrene ND 0.469 10 06/15/2023 18:33 WG2075724
Isophorone ND 4.69 10 06/15/2023 18:33 WG2075724
Naphthalene ND 0.469 10 06/15/2023 18:33 WG2075724
Nitrobenzene ND 4.69 10 06/15/2023 18:33 WG2075724
n-Nitrosodimethylamine ND J6 4.69 10 06/15/2023 18:33 WG2075724
n-Nitrosodiphenylamine ND 4.69 10 06/15/2023 18:33 WG2075724
n-Nitrosodi-n-propylamine ND 4.69 10 06/15/2023 18:33 WG2075724
Phenanthrene ND 0.469 10 06/15/2023 18:33 WG2075724
Benzylbutyl phthalate ND 4.69 10 06/15/2023 18:33 WG2075724
Bis(2-ethylhexyl)phthalate ND 4.69 10 06/15/2023 18:33 WG2075724
Di-n-butyl phthalate ND J4 4.69 10 06/15/2023 18:33 WG2075724
Diethyl phthalate ND 4.69 10 06/15/2023 18:33 WG2075724
Dimethyl phthalate ND J6 4.69 10 06/15/2023 18:33 WG2075724
Di-n-octyl phthalate ND 4.69 10 06/15/2023 18:33 WG2075724
Pyrene ND 0.469 10 06/15/2023 18:33 WG2075724
1,2,4-Trichlorobenzene ND 4.69 10 06/15/2023 18:33 WG2075724
4-Chloro-3-methylphenol ND 4.69 10 06/15/2023 18:33 WG2075724
2-Chlorophenol ND 4.69 10 06/15/2023 18:33 WG2075724
2,4-Dichlorophenol ND 4.69 10 06/15/2023 18:33 WG2075724
2,4-Dimethylphenol ND 4.69 10 06/15/2023 18:33 WG2075724
4,6-Dinitro-2-methylphenol ND J6 4.69 10 06/15/2023 18:33 WG2075724
2,4-Dinitrophenol ND J6 4.69 10 06/15/2023 18:33 WG2075724
2-Nitrophenol ND 4.69 10 06/15/2023 18:33 WG2075724
4-Nitrophenol ND 4.69 10 06/15/2023 18:33 WG2075724
Pentachlorophenol ND 4.69 10 06/15/2023 18:33 WG2075724
Phenol ND 4.69 10 06/15/2023 18:33 WG2075724
2,4,6-Trichlorophenol ND 4.69 10 06/15/2023 18:33 WG2075724
(S) Nitrobenzene-d5 43.8 10.0-122 06/15/2023 18:33 WG2075724
(S) 2-Fluorobiphenyl 54.6 15.0-120 06/15/2023 18:33 WG2075724
(S) p-Terphenyl-d14 55.2 10.0-120 06/15/2023 18:33 WG2075724
(S) Phenol-d5 51.7 10.0-120 06/15/2023 18:33 WG2075724
(S) 2-Fluorophenol 55.7 12.0-120 06/15/2023 18:33 WG2075724
(S) 2,4,6-Tribromophenol 48.0 10.0-127 06/15/2023 18:33 WG2075724
Sample Narrative:
L1624935-01 WG2075724: Dilution due to matrix impact during extraction procedure
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND J3 0.00844 1 06/16/2023 18:27 WG2078829
Acenaphthene ND J3 0.00844 1 06/16/2023 18:27 WG2078829
Acenaphthylene ND 0.00844 1 06/16/2023 18:27 WG2078829
Benzo(a)anthracene 0.00922 J5 0.00844 1 06/16/2023 18:27 WG2078829
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1624935
CB-8
Collected date/time: 06/09/23 13:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzo(a)pyrene 0.0109 J3 J5 0.00844 1 06/16/2023 18:27 WG2078829
Benzo(b)fluoranthene 0.00967 J3 J5 0.00844 1 06/16/2023 18:27 WG2078829
Benzo(g,h,i)perylene 0.0163 J3 0.00844 1 06/16/2023 18:27 WG2078829
Benzo(k)fluoranthene ND J3 J5 0.00844 1 06/16/2023 18:27 WG2078829
Chrysene 0.0102 J5 0.00844 1 06/16/2023 18:27 WG2078829
Dibenz(a,h)anthracene ND 0.00844 1 06/16/2023 18:27 WG2078829
Fluoranthene 0.0111 J5 0.00844 1 06/16/2023 18:27 WG2078829
Fluorene ND 0.00844 1 06/16/2023 18:27 WG2078829
Indeno(1,2,3-cd)pyrene ND J3 J5 0.00844 1 06/16/2023 18:27 WG2078829
Naphthalene ND 0.0281 1 06/16/2023 18:27 WG2078829
Phenanthrene 0.00887 J3 J5 0.00844 1 06/16/2023 18:27 WG2078829
Pyrene 0.0211 J5 0.00844 1 06/16/2023 18:27 WG2078829
1-Methylnaphthalene ND 0.0281 1 06/16/2023 18:27 WG2078829
2-Methylnaphthalene ND 0.0281 1 06/16/2023 18:27 WG2078829
2-Chloronaphthalene ND 0.0281 1 06/16/2023 18:27 WG2078829
(S) p-Terphenyl-d14 82.7 23.0-120 06/16/2023 18:27 WG2078829
(S) Nitrobenzene-d5 116 14.0-149 06/16/2023 18:27 WG2078829
(S) 2-Fluorobiphenyl 90.9 34.0-125 06/16/2023 18:27 WG2078829
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1624935
CB-9
Collected date/time: 06/09/23 13:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.4 1 06/13/2023 11:32 WG2075981
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.90 25 06/16/2023 04:15 WG2078791
(S) a,a,a-Trifluorotoluene(FID) 101 77.0-120 06/16/2023 04:15 WG2078791
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0779 1 06/16/2023 02:13 WG2078708
Acrylonitrile ND 0.0195 1 06/16/2023 02:13 WG2078708
Benzene ND 0.00156 1 06/16/2023 02:13 WG2078708
Bromobenzene ND 0.0195 1 06/16/2023 02:13 WG2078708
Bromodichloromethane ND 0.00390 1 06/16/2023 02:13 WG2078708
Bromoform ND 0.0390 1 06/16/2023 02:13 WG2078708
Bromomethane ND 0.0195 1 06/16/2023 02:13 WG2078708
n-Butylbenzene ND 0.0195 1 06/16/2023 02:13 WG2078708
sec-Butylbenzene ND 0.0195 1 06/16/2023 02:13 WG2078708
tert-Butylbenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
Carbon tetrachloride ND 0.00779 1 06/16/2023 02:13 WG2078708
Chlorobenzene ND 0.00390 1 06/16/2023 02:13 WG2078708
Chlorodibromomethane ND 0.00390 1 06/16/2023 02:13 WG2078708
Chloroethane ND 0.00779 1 06/16/2023 02:13 WG2078708
Chloroform ND 0.00390 1 06/16/2023 02:13 WG2078708
Chloromethane ND 0.0195 1 06/16/2023 02:13 WG2078708
2-Chlorotoluene ND 0.00390 1 06/16/2023 02:13 WG2078708
4-Chlorotoluene ND 0.00779 1 06/16/2023 02:13 WG2078708
1,2-Dibromo-3-Chloropropane ND 0.0390 1 06/16/2023 02:13 WG2078708
1,2-Dibromoethane ND 0.00390 1 06/16/2023 02:13 WG2078708
Dibromomethane ND 0.00779 1 06/16/2023 02:13 WG2078708
1,2-Dichlorobenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
1,3-Dichlorobenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
1,4-Dichlorobenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
Dichlorodifluoromethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,1-Dichloroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,2-Dichloroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,1-Dichloroethene ND 0.00390 1 06/16/2023 02:13 WG2078708
cis-1,2-Dichloroethene ND 0.00390 1 06/16/2023 02:13 WG2078708
trans-1,2-Dichloroethene ND 0.00779 1 06/16/2023 02:13 WG2078708
1,2-Dichloropropane ND 0.00779 1 06/16/2023 02:13 WG2078708
1,1-Dichloropropene ND 0.00390 1 06/16/2023 02:13 WG2078708
1,3-Dichloropropane ND 0.00779 1 06/16/2023 02:13 WG2078708
cis-1,3-Dichloropropene ND 0.00390 1 06/16/2023 02:13 WG2078708
trans-1,3-Dichloropropene ND 0.00779 1 06/16/2023 02:13 WG2078708
2,2-Dichloropropane ND 0.00390 1 06/16/2023 02:13 WG2078708
Di-isopropyl ether ND 0.00156 1 06/16/2023 02:13 WG2078708
Ethylbenzene ND 0.00390 1 06/16/2023 02:13 WG2078708
Hexachloro-1,3-butadiene ND 0.0390 1 06/16/2023 02:13 WG2078708
Isopropylbenzene ND 0.00390 1 06/16/2023 02:13 WG2078708
p-Isopropyltoluene ND 0.00779 1 06/16/2023 02:13 WG2078708
2-Butanone (MEK)ND 0.156 1 06/16/2023 02:13 WG2078708
Methylene Chloride ND 0.0390 1 06/16/2023 02:13 WG2078708
4-Methyl-2-pentanone (MIBK) ND 0.0390 1 06/16/2023 02:13 WG2078708
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1624935
CB-9
Collected date/time: 06/09/23 13:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Methyl tert-butyl ether ND 0.00156 1 06/18/2023 18:00 WG2079280
Naphthalene ND 0.0195 1 06/16/2023 02:13 WG2078708
n-Propylbenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
Styrene ND 0.0195 1 06/16/2023 02:13 WG2078708
1,1,1,2-Tetrachloroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,1,2,2-Tetrachloroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,1,2-Trichlorotrifluoroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
Tetrachloroethene 0.0263 0.00390 1 06/16/2023 02:13 WG2078708
Toluene 0.756 0.00779 1 06/16/2023 02:13 WG2078708
1,2,3-Trichlorobenzene ND 0.0195 1 06/16/2023 02:13 WG2078708
1,2,4-Trichlorobenzene ND 0.0195 1 06/16/2023 02:13 WG2078708
1,1,1-Trichloroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,1,2-Trichloroethane ND 0.00390 1 06/16/2023 02:13 WG2078708
Trichloroethene 0.00195 0.00156 1 06/16/2023 02:13 WG2078708
Trichlorofluoromethane ND 0.00390 1 06/16/2023 02:13 WG2078708
1,2,3-Trichloropropane ND 0.0195 1 06/16/2023 02:13 WG2078708
1,2,4-Trimethylbenzene 0.0161 0.00779 1 06/16/2023 02:13 WG2078708
1,2,3-Trimethylbenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
1,3,5-Trimethylbenzene ND 0.00779 1 06/16/2023 02:13 WG2078708
Vinyl chloride ND 0.00390 1 06/16/2023 02:13 WG2078708
Xylenes, Total 0.0126 0.0101 1 06/16/2023 02:13 WG2078708
(S) Toluene-d8 104 75.0-131 06/16/2023 02:13 WG2078708
(S) Toluene-d8 111 75.0-131 06/18/2023 18:00 WG2079280
(S) 4-Bromofluorobenzene 105 67.0-138 06/16/2023 02:13 WG2078708
(S) 4-Bromofluorobenzene 93.4 67.0-138 06/18/2023 18:00 WG2079280
(S) 1,2-Dichloroethane-d4 81.2 70.0-130 06/16/2023 02:13 WG2078708
(S) 1,2-Dichloroethane-d4 94.3 70.0-130 06/18/2023 18:00 WG2079280
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range ND 101 20 06/16/2023 16:29 WG2077992
C28-C40 Oil Range 303 101 20 06/16/2023 16:29 WG2077992
(S) o-Terphenyl 73.1 J7 18.0-148 06/16/2023 16:29 WG2077992
Sample Narrative:
L1624935-02 WG2077992: Cannot run at lower dilution due to viscosity of extract
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.419 10 06/15/2023 01:30 WG2075724
Acenaphthylene ND 0.419 10 06/15/2023 01:30 WG2075724
Anthracene ND 0.419 10 06/15/2023 01:30 WG2075724
Benzidine ND 21.0 10 06/15/2023 01:30 WG2075724
Benzo(a)anthracene ND 0.419 10 06/15/2023 01:30 WG2075724
Benzo(b)fluoranthene ND 0.419 10 06/15/2023 01:30 WG2075724
Benzo(k)fluoranthene ND 0.419 10 06/15/2023 01:30 WG2075724
Benzo(g,h,i)perylene ND 0.419 10 06/15/2023 01:30 WG2075724
Benzo(a)pyrene ND 0.419 10 06/15/2023 01:30 WG2075724
Bis(2-chlorethoxy)methane ND 4.19 10 06/15/2023 01:30 WG2075724
Bis(2-chloroethyl)ether ND 4.19 10 06/15/2023 01:30 WG2075724
2,2-Oxybis(1-Chloropropane) ND 4.19 10 06/15/2023 01:30 WG2075724
4-Bromophenyl-phenylether ND 4.19 10 06/15/2023 01:30 WG2075724
2-Chloronaphthalene ND 0.419 10 06/15/2023 01:30 WG2075724
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1624935
CB-9
Collected date/time: 06/09/23 13:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Chlorophenyl-phenylether ND 4.19 10 06/15/2023 01:30 WG2075724
Chrysene ND 0.419 10 06/15/2023 01:30 WG2075724
Dibenz(a,h)anthracene ND 0.419 10 06/15/2023 01:30 WG2075724
3,3-Dichlorobenzidine ND 4.19 10 06/15/2023 01:30 WG2075724
2,4-Dinitrotoluene ND 4.19 10 06/15/2023 01:30 WG2075724
2,6-Dinitrotoluene ND 4.19 10 06/15/2023 01:30 WG2075724
Fluoranthene ND 0.419 10 06/15/2023 01:30 WG2075724
Fluorene ND 0.419 10 06/15/2023 01:30 WG2075724
Hexachlorobenzene ND 4.19 10 06/15/2023 01:30 WG2075724
Hexachloro-1,3-butadiene ND 4.19 10 06/15/2023 01:30 WG2075724
Hexachlorocyclopentadiene ND 4.19 10 06/15/2023 01:30 WG2075724
Hexachloroethane ND 4.19 10 06/15/2023 01:30 WG2075724
Indeno(1,2,3-cd)pyrene ND 0.419 10 06/15/2023 01:30 WG2075724
Isophorone ND 4.19 10 06/15/2023 01:30 WG2075724
Naphthalene ND 0.419 10 06/15/2023 01:30 WG2075724
Nitrobenzene ND 4.19 10 06/15/2023 01:30 WG2075724
n-Nitrosodimethylamine ND 4.19 10 06/15/2023 01:30 WG2075724
n-Nitrosodiphenylamine ND 4.19 10 06/15/2023 01:30 WG2075724
n-Nitrosodi-n-propylamine ND 4.19 10 06/15/2023 01:30 WG2075724
Phenanthrene ND 0.419 10 06/15/2023 01:30 WG2075724
Benzylbutyl phthalate ND 4.19 10 06/15/2023 01:30 WG2075724
Bis(2-ethylhexyl)phthalate ND 4.19 10 06/15/2023 01:30 WG2075724
Di-n-butyl phthalate ND J4 4.19 10 06/15/2023 01:30 WG2075724
Diethyl phthalate ND 4.19 10 06/15/2023 01:30 WG2075724
Dimethyl phthalate ND 4.19 10 06/15/2023 01:30 WG2075724
Di-n-octyl phthalate ND 4.19 10 06/15/2023 01:30 WG2075724
Pyrene ND 0.419 10 06/15/2023 01:30 WG2075724
1,2,4-Trichlorobenzene ND 4.19 10 06/15/2023 01:30 WG2075724
4-Chloro-3-methylphenol ND 4.19 10 06/15/2023 01:30 WG2075724
2-Chlorophenol ND 4.19 10 06/15/2023 01:30 WG2075724
2,4-Dichlorophenol ND 4.19 10 06/15/2023 01:30 WG2075724
2,4-Dimethylphenol ND 4.19 10 06/15/2023 01:30 WG2075724
4,6-Dinitro-2-methylphenol ND 4.19 10 06/15/2023 01:30 WG2075724
2,4-Dinitrophenol ND 4.19 10 06/15/2023 01:30 WG2075724
2-Nitrophenol ND 4.19 10 06/15/2023 01:30 WG2075724
4-Nitrophenol ND 4.19 10 06/15/2023 01:30 WG2075724
Pentachlorophenol ND 4.19 10 06/15/2023 01:30 WG2075724
Phenol ND 4.19 10 06/15/2023 01:30 WG2075724
2,4,6-Trichlorophenol ND 4.19 10 06/15/2023 01:30 WG2075724
(S) Nitrobenzene-d5 38.5 10.0-122 06/15/2023 01:30 WG2075724
(S) 2-Fluorobiphenyl 44.6 15.0-120 06/15/2023 01:30 WG2075724
(S) p-Terphenyl-d14 52.9 10.0-120 06/15/2023 01:30 WG2075724
(S) Phenol-d5 45.0 10.0-120 06/15/2023 01:30 WG2075724
(S) 2-Fluorophenol 55.4 12.0-120 06/15/2023 01:30 WG2075724
(S) 2,4,6-Tribromophenol 49.1 10.0-127 06/15/2023 01:30 WG2075724
Sample Narrative:
L1624935-02 WG2075724: Dilution due to matrix impact during extract concentration procedure
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00755 1 06/15/2023 23:19 WG2077933
Acenaphthene ND 0.00755 1 06/15/2023 23:19 WG2077933
Acenaphthylene ND 0.00755 1 06/15/2023 23:19 WG2077933
Benzo(a)anthracene ND 0.00755 1 06/15/2023 23:19 WG2077933
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1624935
CB-9
Collected date/time: 06/09/23 13:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzo(a)pyrene ND 0.00755 1 06/15/2023 23:19 WG2077933
Benzo(b)fluoranthene ND 0.00755 1 06/15/2023 23:19 WG2077933
Benzo(g,h,i)perylene ND 0.00755 1 06/15/2023 23:19 WG2077933
Benzo(k)fluoranthene ND 0.00755 1 06/15/2023 23:19 WG2077933
Chrysene ND 0.00755 1 06/15/2023 23:19 WG2077933
Dibenz(a,h)anthracene ND 0.00755 1 06/15/2023 23:19 WG2077933
Fluoranthene ND 0.00755 1 06/15/2023 23:19 WG2077933
Fluorene ND 0.00755 1 06/15/2023 23:19 WG2077933
Indeno(1,2,3-cd)pyrene ND 0.00755 1 06/15/2023 23:19 WG2077933
Naphthalene ND 0.0252 1 06/15/2023 23:19 WG2077933
Phenanthrene ND 0.00755 1 06/15/2023 23:19 WG2077933
Pyrene 0.00828 0.00755 1 06/15/2023 23:19 WG2077933
1-Methylnaphthalene ND 0.0252 1 06/15/2023 23:19 WG2077933
2-Methylnaphthalene ND 0.0252 1 06/15/2023 23:19 WG2077933
2-Chloronaphthalene ND 0.0252 1 06/15/2023 23:19 WG2077933
(S) p-Terphenyl-d14 86.3 23.0-120 06/15/2023 23:19 WG2077933
(S) Nitrobenzene-d5 69.3 14.0-149 06/15/2023 23:19 WG2077933
(S) 2-Fluorobiphenyl 81.2 34.0-125 06/15/2023 23:19 WG2077933
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1624935
DUP-5
Collected date/time: 06/09/23 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.5 1 06/13/2023 11:32 WG2075981
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.68 25 06/16/2023 04:39 WG2078791
(S) a,a,a-Trifluorotoluene(FID) 99.0 77.0-120 06/16/2023 04:39 WG2078791
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0736 1 06/16/2023 02:33 WG2078708
Acrylonitrile ND 0.0184 1 06/16/2023 02:33 WG2078708
Benzene ND 0.00147 1 06/16/2023 02:33 WG2078708
Bromobenzene ND 0.0184 1 06/16/2023 02:33 WG2078708
Bromodichloromethane ND 0.00368 1 06/16/2023 02:33 WG2078708
Bromoform ND 0.0368 1 06/16/2023 02:33 WG2078708
Bromomethane ND 0.0184 1 06/16/2023 02:33 WG2078708
n-Butylbenzene ND 0.0184 1 06/16/2023 02:33 WG2078708
sec-Butylbenzene ND 0.0184 1 06/16/2023 02:33 WG2078708
tert-Butylbenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
Carbon tetrachloride ND 0.00736 1 06/16/2023 02:33 WG2078708
Chlorobenzene ND 0.00368 1 06/16/2023 02:33 WG2078708
Chlorodibromomethane ND 0.00368 1 06/16/2023 02:33 WG2078708
Chloroethane ND 0.00736 1 06/16/2023 02:33 WG2078708
Chloroform ND 0.00368 1 06/16/2023 02:33 WG2078708
Chloromethane ND 0.0184 1 06/16/2023 02:33 WG2078708
2-Chlorotoluene ND 0.00368 1 06/16/2023 02:33 WG2078708
4-Chlorotoluene ND 0.00736 1 06/16/2023 02:33 WG2078708
1,2-Dibromo-3-Chloropropane ND 0.0368 1 06/16/2023 02:33 WG2078708
1,2-Dibromoethane ND 0.00368 1 06/16/2023 02:33 WG2078708
Dibromomethane ND 0.00736 1 06/16/2023 02:33 WG2078708
1,2-Dichlorobenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
1,3-Dichlorobenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
1,4-Dichlorobenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
Dichlorodifluoromethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,1-Dichloroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,2-Dichloroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,1-Dichloroethene ND 0.00368 1 06/16/2023 02:33 WG2078708
cis-1,2-Dichloroethene ND 0.00368 1 06/16/2023 02:33 WG2078708
trans-1,2-Dichloroethene ND 0.00736 1 06/16/2023 02:33 WG2078708
1,2-Dichloropropane ND 0.00736 1 06/16/2023 02:33 WG2078708
1,1-Dichloropropene ND 0.00368 1 06/16/2023 02:33 WG2078708
1,3-Dichloropropane ND 0.00736 1 06/16/2023 02:33 WG2078708
cis-1,3-Dichloropropene ND 0.00368 1 06/16/2023 02:33 WG2078708
trans-1,3-Dichloropropene ND 0.00736 1 06/16/2023 02:33 WG2078708
2,2-Dichloropropane ND 0.00368 1 06/16/2023 02:33 WG2078708
Di-isopropyl ether ND 0.00147 1 06/16/2023 02:33 WG2078708
Ethylbenzene ND 0.00368 1 06/16/2023 02:33 WG2078708
Hexachloro-1,3-butadiene ND 0.0368 1 06/16/2023 02:33 WG2078708
Isopropylbenzene ND 0.00368 1 06/16/2023 02:33 WG2078708
p-Isopropyltoluene ND 0.00736 1 06/16/2023 02:33 WG2078708
2-Butanone (MEK)ND 0.147 1 06/16/2023 02:33 WG2078708
Methylene Chloride ND 0.0368 1 06/16/2023 02:33 WG2078708
4-Methyl-2-pentanone (MIBK) ND 0.0368 1 06/16/2023 02:33 WG2078708
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1624935
DUP-5
Collected date/time: 06/09/23 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Methyl tert-butyl ether ND 0.00147 1 06/18/2023 18:21 WG2079280
Naphthalene ND 0.0184 1 06/16/2023 02:33 WG2078708
n-Propylbenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
Styrene ND 0.0184 1 06/16/2023 02:33 WG2078708
1,1,1,2-Tetrachloroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,1,2,2-Tetrachloroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,1,2-Trichlorotrifluoroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
Tetrachloroethene 0.00910 0.00368 1 06/16/2023 02:33 WG2078708
Toluene 0.368 0.00736 1 06/16/2023 02:33 WG2078708
1,2,3-Trichlorobenzene ND 0.0184 1 06/16/2023 02:33 WG2078708
1,2,4-Trichlorobenzene ND 0.0184 1 06/16/2023 02:33 WG2078708
1,1,1-Trichloroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,1,2-Trichloroethane ND 0.00368 1 06/16/2023 02:33 WG2078708
Trichloroethene ND 0.00147 1 06/16/2023 02:33 WG2078708
Trichlorofluoromethane ND 0.00368 1 06/16/2023 02:33 WG2078708
1,2,3-Trichloropropane ND 0.0184 1 06/16/2023 02:33 WG2078708
1,2,4-Trimethylbenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
1,2,3-Trimethylbenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
1,3,5-Trimethylbenzene ND 0.00736 1 06/16/2023 02:33 WG2078708
Vinyl chloride ND 0.00368 1 06/16/2023 02:33 WG2078708
Xylenes, Total ND 0.00957 1 06/16/2023 02:33 WG2078708
(S) Toluene-d8 106 75.0-131 06/16/2023 02:33 WG2078708
(S) Toluene-d8 111 75.0-131 06/18/2023 18:21 WG2079280
(S) 4-Bromofluorobenzene 105 67.0-138 06/16/2023 02:33 WG2078708
(S) 4-Bromofluorobenzene 93.0 67.0-138 06/18/2023 18:21 WG2079280
(S) 1,2-Dichloroethane-d4 72.9 70.0-130 06/16/2023 02:33 WG2078708
(S) 1,2-Dichloroethane-d4 93.2 70.0-130 06/18/2023 18:21 WG2079280
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
C10-C28 Diesel Range 46.1 19.4 4 06/17/2023 09:12 WG2077992
C28-C40 Oil Range 104 19.4 4 06/17/2023 09:12 WG2077992
(S) o-Terphenyl 82.0 18.0-148 06/17/2023 09:12 WG2077992
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0404 1 06/14/2023 21:20 WG2075724
Acenaphthylene ND 0.0404 1 06/14/2023 21:20 WG2075724
Anthracene ND 0.0404 1 06/14/2023 21:20 WG2075724
Benzidine ND 2.02 1 06/14/2023 21:20 WG2075724
Benzo(a)anthracene ND 0.0404 1 06/14/2023 21:20 WG2075724
Benzo(b)fluoranthene ND 0.0404 1 06/14/2023 21:20 WG2075724
Benzo(k)fluoranthene ND 0.0404 1 06/14/2023 21:20 WG2075724
Benzo(g,h,i)perylene ND 0.0404 1 06/14/2023 21:20 WG2075724
Benzo(a)pyrene ND 0.0404 1 06/14/2023 21:20 WG2075724
Bis(2-chlorethoxy)methane ND 0.404 1 06/14/2023 21:20 WG2075724
Bis(2-chloroethyl)ether ND 0.404 1 06/14/2023 21:20 WG2075724
2,2-Oxybis(1-Chloropropane) ND 0.404 1 06/14/2023 21:20 WG2075724
4-Bromophenyl-phenylether ND 0.404 1 06/14/2023 21:20 WG2075724
2-Chloronaphthalene ND 0.0404 1 06/14/2023 21:20 WG2075724
4-Chlorophenyl-phenylether ND 0.404 1 06/14/2023 21:20 WG2075724
Chrysene ND 0.0404 1 06/14/2023 21:20 WG2075724
Dibenz(a,h)anthracene ND 0.0404 1 06/14/2023 21:20 WG2075724
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1624935
DUP-5
Collected date/time: 06/09/23 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
3,3-Dichlorobenzidine ND 0.404 1 06/14/2023 21:20 WG2075724
2,4-Dinitrotoluene ND 0.404 1 06/14/2023 21:20 WG2075724
2,6-Dinitrotoluene ND 0.404 1 06/14/2023 21:20 WG2075724
Fluoranthene ND 0.0404 1 06/14/2023 21:20 WG2075724
Fluorene ND 0.0404 1 06/14/2023 21:20 WG2075724
Hexachlorobenzene ND 0.404 1 06/14/2023 21:20 WG2075724
Hexachloro-1,3-butadiene ND 0.404 1 06/14/2023 21:20 WG2075724
Hexachlorocyclopentadiene ND 0.404 1 06/14/2023 21:20 WG2075724
Hexachloroethane ND 0.404 1 06/14/2023 21:20 WG2075724
Indeno(1,2,3-cd)pyrene ND 0.0404 1 06/14/2023 21:20 WG2075724
Isophorone ND 0.404 1 06/14/2023 21:20 WG2075724
Naphthalene ND 0.0404 1 06/14/2023 21:20 WG2075724
Nitrobenzene ND 0.404 1 06/14/2023 21:20 WG2075724
n-Nitrosodimethylamine ND 0.404 1 06/14/2023 21:20 WG2075724
n-Nitrosodiphenylamine ND 0.404 1 06/14/2023 21:20 WG2075724
n-Nitrosodi-n-propylamine ND 0.404 1 06/14/2023 21:20 WG2075724
Phenanthrene ND 0.0404 1 06/14/2023 21:20 WG2075724
Benzylbutyl phthalate ND 0.404 1 06/14/2023 21:20 WG2075724
Bis(2-ethylhexyl)phthalate ND 0.404 1 06/14/2023 21:20 WG2075724
Di-n-butyl phthalate ND J4 0.404 1 06/14/2023 21:20 WG2075724
Diethyl phthalate ND 0.404 1 06/14/2023 21:20 WG2075724
Dimethyl phthalate ND 0.404 1 06/14/2023 21:20 WG2075724
Di-n-octyl phthalate ND 0.404 1 06/14/2023 21:20 WG2075724
Pyrene ND 0.0404 1 06/14/2023 21:20 WG2075724
1,2,4-Trichlorobenzene ND 0.404 1 06/14/2023 21:20 WG2075724
4-Chloro-3-methylphenol ND 0.404 1 06/14/2023 21:20 WG2075724
2-Chlorophenol ND 0.404 1 06/14/2023 21:20 WG2075724
2,4-Dichlorophenol ND 0.404 1 06/14/2023 21:20 WG2075724
2,4-Dimethylphenol ND 0.404 1 06/14/2023 21:20 WG2075724
4,6-Dinitro-2-methylphenol ND 0.404 1 06/14/2023 21:20 WG2075724
2,4-Dinitrophenol ND 0.404 1 06/14/2023 21:20 WG2075724
2-Nitrophenol ND 0.404 1 06/14/2023 21:20 WG2075724
4-Nitrophenol ND 0.404 1 06/14/2023 21:20 WG2075724
Pentachlorophenol ND 0.404 1 06/14/2023 21:20 WG2075724
Phenol ND 0.404 1 06/14/2023 21:20 WG2075724
2,4,6-Trichlorophenol ND 0.404 1 06/14/2023 21:20 WG2075724
(S) Nitrobenzene-d5 36.3 10.0-122 06/14/2023 21:20 WG2075724
(S) 2-Fluorobiphenyl 40.1 15.0-120 06/14/2023 21:20 WG2075724
(S) p-Terphenyl-d14 49.8 10.0-120 06/14/2023 21:20 WG2075724
(S) Phenol-d5 40.7 10.0-120 06/14/2023 21:20 WG2075724
(S) 2-Fluorophenol 39.6 12.0-120 06/14/2023 21:20 WG2075724
(S) 2,4,6-Tribromophenol 40.1 10.0-127 06/14/2023 21:20 WG2075724
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00727 1 06/15/2023 23:00 WG2077933
Acenaphthene ND 0.00727 1 06/15/2023 23:00 WG2077933
Acenaphthylene ND 0.00727 1 06/15/2023 23:00 WG2077933
Benzo(a)anthracene ND 0.00727 1 06/15/2023 23:00 WG2077933
Benzo(a)pyrene ND 0.00727 1 06/15/2023 23:00 WG2077933
Benzo(b)fluoranthene ND 0.00727 1 06/15/2023 23:00 WG2077933
Benzo(g,h,i)perylene ND 0.00727 1 06/15/2023 23:00 WG2077933
Benzo(k)fluoranthene ND 0.00727 1 06/15/2023 23:00 WG2077933
Chrysene ND 0.00727 1 06/15/2023 23:00 WG2077933
Dibenz(a,h)anthracene ND 0.00727 1 06/15/2023 23:00 WG2077933
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1624935
DUP-5
Collected date/time: 06/09/23 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluoranthene 0.00871 0.00727 1 06/15/2023 23:00 WG2077933
Fluorene ND 0.00727 1 06/15/2023 23:00 WG2077933
Indeno(1,2,3-cd)pyrene ND 0.00727 1 06/15/2023 23:00 WG2077933
Naphthalene ND 0.0242 1 06/15/2023 23:00 WG2077933
Phenanthrene 0.00774 0.00727 1 06/15/2023 23:00 WG2077933
Pyrene 0.00913 0.00727 1 06/15/2023 23:00 WG2077933
1-Methylnaphthalene ND 0.0242 1 06/15/2023 23:00 WG2077933
2-Methylnaphthalene ND 0.0242 1 06/15/2023 23:00 WG2077933
2-Chloronaphthalene ND 0.0242 1 06/15/2023 23:00 WG2077933
(S) p-Terphenyl-d14 80.1 23.0-120 06/15/2023 23:00 WG2077933
(S) Nitrobenzene-d5 70.5 14.0-149 06/15/2023 23:00 WG2077933
(S) 2-Fluorobiphenyl 77.0 34.0-125 06/15/2023 23:00 WG2077933
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075981
Total Solids by Method 2540 G-2011 L1624935-01,02,03
Method Blank (MB)
(MB) R3936404-1 06/13/23 11:32
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1624935-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1624935-01 06/13/23 11:32 • (DUP) R3936404-3 06/13/23 11:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 71.1 70.6 1 0.635 10
Laboratory Control Sample (LCS)
(LCS) R3936404-2 06/13/23 11:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.2 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078791
Volatile Organic Compounds (GC) by Method 8015D/GRO L1624935-01,02,03
Method Blank (MB)
(MB) R3938223-2 06/16/23 00:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 1.44 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)98.1 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3938223-1 06/15/23 18:18
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.71 104 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 103 77.0-120
L1624935-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624935-01 06/16/23 03:50 • (MS) R3938223-3 06/16/23 07:30 • (MSD) R3938223-4 06/16/23 07:54
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 226 ND 269 262 118 115 25 10.0-151 2.82 28
(S)
a,a,a-Trifluorotoluene(FID) 103 103 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078708
Volatile Organic Compounds (GC/MS) by Method 8260B L1624935-01,02,03
Method Blank (MB)
(MB) R3937743-3 06/15/23 19:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078708
Volatile Organic Compounds (GC/MS) by Method 8260B L1624935-01,02,03
Method Blank (MB)
(MB) R3937743-3 06/15/23 19:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00335 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 91.3 67.0-138
(S) 1,2-Dichloroethane-d4 84.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3937743-1 06/15/23 18:06 • (LCSD) R3937743-2 06/15/23 18:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.362 0.344 57.9 55.0 10.0-160 5.10 31
Acrylonitrile 0.625 0.569 0.544 91.0 87.0 45.0-153 4.49 22
Benzene 0.125 0.123 0.123 98.4 98.4 70.0-123 0.000 20
Bromobenzene 0.125 0.147 0.151 118 121 73.0-121 2.68 20
Bromodichloromethane 0.125 0.124 0.130 99.2 104 73.0-121 4.72 20
Bromoform 0.125 0.135 0.137 108 110 64.0-132 1.47 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078708
Volatile Organic Compounds (GC/MS) by Method 8260B L1624935-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3937743-1 06/15/23 18:06 • (LCSD) R3937743-2 06/15/23 18:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromomethane 0.125 0.110 0.111 88.0 88.8 56.0-147 0.905 20
n-Butylbenzene 0.125 0.117 0.121 93.6 96.8 68.0-135 3.36 20
sec-Butylbenzene 0.125 0.116 0.122 92.8 97.6 74.0-130 5.04 20
tert-Butylbenzene 0.125 0.117 0.122 93.6 97.6 75.0-127 4.18 20
Carbon tetrachloride 0.125 0.132 0.132 106 106 66.0-128 0.000 20
Chlorobenzene 0.125 0.148 0.150 118 120 76.0-128 1.34 20
Chlorodibromomethane 0.125 0.146 0.143 117 114 74.0-127 2.08 20
Chloroethane 0.125 0.118 0.125 94.4 100 61.0-134 5.76 20
Chloroform 0.125 0.114 0.114 91.2 91.2 72.0-123 0.000 20
Chloromethane 0.125 0.104 0.108 83.2 86.4 51.0-138 3.77 20
2-Chlorotoluene 0.125 0.138 0.150 110 120 75.0-124 8.33 20
4-Chlorotoluene 0.125 0.141 0.138 113 110 75.0-124 2.15 20
1,2-Dibromo-3-Chloropropane 0.125 0.116 0.111 92.8 88.8 59.0-130 4.41 20
1,2-Dibromoethane 0.125 0.142 0.143 114 114 74.0-128 0.702 20
Dibromomethane 0.125 0.124 0.130 99.2 104 75.0-122 4.72 20
1,2-Dichlorobenzene 0.125 0.135 0.138 108 110 76.0-124 2.20 20
1,3-Dichlorobenzene 0.125 0.137 0.142 110 114 76.0-125 3.58 20
1,4-Dichlorobenzene 0.125 0.135 0.138 108 110 77.0-121 2.20 20
Dichlorodifluoromethane 0.125 0.110 0.113 88.0 90.4 43.0-156 2.69 20
1,1-Dichloroethane 0.125 0.124 0.124 99.2 99.2 70.0-127 0.000 20
1,2-Dichloroethane 0.125 0.114 0.113 91.2 90.4 65.0-131 0.881 20
1,1-Dichloroethene 0.125 0.138 0.138 110 110 65.0-131 0.000 20
cis-1,2-Dichloroethene 0.125 0.120 0.123 96.0 98.4 73.0-125 2.47 20
trans-1,2-Dichloroethene 0.125 0.125 0.123 100 98.4 71.0-125 1.61 20
1,2-Dichloropropane 0.125 0.133 0.128 106 102 74.0-125 3.83 20
1,1-Dichloropropene 0.125 0.131 0.130 105 104 73.0-125 0.766 20
1,3-Dichloropropane 0.125 0.146 0.147 117 118 80.0-125 0.683 20
cis-1,3-Dichloropropene 0.125 0.112 0.111 89.6 88.8 76.0-127 0.897 20
trans-1,3-Dichloropropene 0.125 0.140 0.145 112 116 73.0-127 3.51 20
2,2-Dichloropropane 0.125 0.109 0.106 87.2 84.8 59.0-135 2.79 20
Di-isopropyl ether 0.125 0.107 0.107 85.6 85.6 60.0-136 0.000 20
Ethylbenzene 0.125 0.141 0.136 113 109 74.0-126 3.61 20
Hexachloro-1,3-butadiene 0.125 0.133 0.135 106 108 57.0-150 1.49 20
Isopropylbenzene 0.125 0.113 0.113 90.4 90.4 72.0-127 0.000 20
p-Isopropyltoluene 0.125 0.109 0.114 87.2 91.2 72.0-133 4.48 20
2-Butanone (MEK)0.625 0.545 0.531 87.2 85.0 30.0-160 2.60 24
Methylene Chloride 0.125 0.120 0.116 96.0 92.8 68.0-123 3.39 20
4-Methyl-2-pentanone (MIBK) 0.625 0.602 0.612 96.3 97.9 56.0-143 1.65 20
Naphthalene 0.125 0.0824 0.0899 65.9 71.9 59.0-130 8.71 20
n-Propylbenzene 0.125 0.135 0.139 108 111 74.0-126 2.92 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078708
Volatile Organic Compounds (GC/MS) by Method 8260B L1624935-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3937743-1 06/15/23 18:06 • (LCSD) R3937743-2 06/15/23 18:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Styrene 0.125 0.119 0.119 95.2 95.2 72.0-127 0.000 20
1,1,1,2-Tetrachloroethane 0.125 0.141 0.144 113 115 74.0-129 2.11 20
1,1,2,2-Tetrachloroethane 0.125 0.137 0.142 110 114 68.0-128 3.58 20
1,1,2-Trichlorotrifluoroethane 0.125 0.123 0.119 98.4 95.2 61.0-139 3.31 20
Tetrachloroethene 0.125 0.143 0.139 114 111 70.0-136 2.84 20
Toluene 0.125 0.139 0.138 111 110 75.0-121 0.722 20
1,2,3-Trichlorobenzene 0.125 0.0902 0.108 72.2 86.4 59.0-139 18.0 20
1,2,4-Trichlorobenzene 0.125 0.0961 0.104 76.9 83.2 62.0-137 7.90 20
1,1,1-Trichloroethane 0.125 0.127 0.127 102 102 69.0-126 0.000 20
1,1,2-Trichloroethane 0.125 0.145 0.149 116 119 78.0-123 2.72 20
Trichloroethene 0.125 0.119 0.122 95.2 97.6 76.0-126 2.49 20
Trichlorofluoromethane 0.125 0.113 0.113 90.4 90.4 61.0-142 0.000 20
1,2,3-Trichloropropane 0.125 0.136 0.136 109 109 67.0-129 0.000 20
1,2,4-Trimethylbenzene 0.125 0.109 0.115 87.2 92.0 70.0-126 5.36 20
1,2,3-Trimethylbenzene 0.125 0.121 0.128 96.8 102 74.0-124 5.62 20
1,3,5-Trimethylbenzene 0.125 0.130 0.134 104 107 73.0-127 3.03 20
Vinyl chloride 0.125 0.126 0.126 101 101 63.0-134 0.000 20
Xylenes, Total 0.375 0.402 0.403 107 107 72.0-127 0.248 20
(S) Toluene-d8 104 103 75.0-131
(S) 4-Bromofluorobenzene 93.9 90.6 67.0-138
(S) 1,2-Dichloroethane-d4 92.1 88.7 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2079280
Volatile Organic Compounds (GC/MS) by Method 8260B L1624935-01,02,03
Method Blank (MB)
(MB) R3938183-3 06/18/23 11:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Methyl tert-butyl ether U 0.000350 0.00100
(S) Toluene-d8 106 75.0-131
(S) 4-Bromofluorobenzene 96.6 67.0-138
(S) 1,2-Dichloroethane-d4 97.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3938183-1 06/18/23 10:32 • (LCSD) R3938183-2 06/18/23 10:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.125 0.102 0.0973 81.6 77.8 66.0-132 4.72 20
(S) Toluene-d8 105 104 75.0-131
(S) 4-Bromofluorobenzene 101 96.0 67.0-138
(S) 1,2-Dichloroethane-d4 102 101 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2077992
Semi-Volatile Organic Compounds (GC) by Method 8015 L1624935-01,02,03
Method Blank (MB)
(MB) R3937867-1 06/16/23 13:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
C10-C28 Diesel Range U 1.61 4.00
C28-C40 Oil Range U 0.274 4.00
(S) o-Terphenyl 91.0 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3937867-2 06/16/23 13:34
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
C10-C28 Diesel Range 50.0 38.1 76.2 50.0-150
(S) o-Terphenyl 91.6 18.0-148
L1624935-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624935-01 06/16/23 15:49 • (MS) R3937867-3 06/16/23 16:02 • (MSD) R3937867-4 06/16/23 16:16
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
C10-C28 Diesel Range 67.8 ND ND ND 0.000 0.000 20 50.0-150 J6 J6 0.000 20
(S) o-Terphenyl 91.0 80.7 18.0-148 J7 J7
Sample Narrative:
OS: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075724
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1624935-01,02,03
Method Blank (MB)
(MB) R3937023-2 06/14/23 19:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate 0.112 J 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075724
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1624935-01,02,03
Method Blank (MB)
(MB) R3937023-2 06/14/23 19:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 34.8 10.0-122
(S) 2-Fluorobiphenyl 41.1 15.0-120
(S) p-Terphenyl-d14 50.2 10.0-120
(S) Phenol-d5 40.2 10.0-120
(S) 2-Fluorophenol 44.4 12.0-120
(S) 2,4,6-Tribromophenol 40.8 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3937023-1 06/14/23 19:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.336 50.5 38.0-120
Acenaphthylene 0.666 0.362 54.4 40.0-120
Anthracene 0.666 0.417 62.6 42.0-120
Benzidine 1.33 0.517 38.9 10.0-120
Benzo(a)anthracene 0.666 0.488 73.3 44.0-120
Benzo(b)fluoranthene 0.666 0.462 69.4 43.0-120
Benzo(k)fluoranthene 0.666 0.402 60.4 44.0-120
Benzo(g,h,i)perylene 0.666 0.591 88.7 43.0-120
Benzo(a)pyrene 0.666 0.499 74.9 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.259 38.9 20.0-120
Bis(2-chloroethyl)ether 0.666 0.304 45.6 16.0-120
2,2-Oxybis(1-Chloropropane) 0.666 0.312 46.8 23.0-120
4-Bromophenyl-phenylether 0.666 0.374 56.2 40.0-120
2-Chloronaphthalene 0.666 0.332 49.8 35.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075724
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1624935-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3937023-1 06/14/23 19:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.350 52.6 40.0-120
Chrysene 0.666 0.571 85.7 43.0-120
Dibenz(a,h)anthracene 0.666 0.606 91.0 44.0-120
3,3-Dichlorobenzidine 1.33 1.12 84.2 28.0-120
2,4-Dinitrotoluene 0.666 0.424 63.7 45.0-120
2,6-Dinitrotoluene 0.666 0.382 57.4 42.0-120
Fluoranthene 0.666 0.310 46.5 44.0-120
Fluorene 0.666 0.363 54.5 41.0-120
Hexachlorobenzene 0.666 0.409 61.4 39.0-120
Hexachloro-1,3-butadiene 0.666 0.289 43.4 15.0-120
Hexachlorocyclopentadiene 0.666 0.271 40.7 15.0-120
Hexachloroethane 0.666 0.295 44.3 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.573 86.0 45.0-120
Isophorone 0.666 0.268 40.2 23.0-120
Naphthalene 0.666 0.282 42.3 18.0-120
Nitrobenzene 0.666 0.243 36.5 17.0-120
n-Nitrosodimethylamine 0.666 0.256 38.4 10.0-125
n-Nitrosodiphenylamine 0.666 0.349 52.4 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.284 42.6 26.0-120
Phenanthrene 0.666 0.380 57.1 42.0-120
Benzylbutyl phthalate 0.666 0.482 72.4 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.552 82.9 41.0-120
Di-n-butyl phthalate 0.666 0.269 40.4 43.0-120 J4
Diethyl phthalate 0.666 0.527 79.1 43.0-120
Dimethyl phthalate 0.666 0.363 54.5 43.0-120
Di-n-octyl phthalate 0.666 0.559 83.9 40.0-120
Pyrene 0.666 0.461 69.2 41.0-120
1,2,4-Trichlorobenzene 0.666 0.293 44.0 17.0-120
4-Chloro-3-methylphenol 0.666 0.297 44.6 28.0-120
2-Chlorophenol 0.666 0.340 51.1 28.0-120
2,4-Dichlorophenol 0.666 0.309 46.4 25.0-120
2,4-Dimethylphenol 0.666 0.283 42.5 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.375 56.3 16.0-120
2,4-Dinitrophenol 0.666 0.291 43.7 10.0-120
2-Nitrophenol 0.666 0.328 49.2 20.0-120
4-Nitrophenol 0.666 0.376 56.5 27.0-120
Pentachlorophenol 0.666 0.383 57.5 29.0-120
Phenol 0.666 0.324 48.6 28.0-120
2,4,6-Trichlorophenol 0.666 0.369 55.4 37.0-120
(S) Nitrobenzene-d5 33.9 10.0-122
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075724
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1624935-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3937023-1 06/14/23 19:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 50.8 15.0-120
(S) p-Terphenyl-d14 71.5 10.0-120
(S) Phenol-d5 47.4 10.0-120
(S) 2-Fluorophenol 52.9 12.0-120
(S) 2,4,6-Tribromophenol 60.8 10.0-127
L1624935-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624935-01 06/15/23 18:33 • (MS) R3937963-1 06/15/23 18:54 • (MSD) R3937963-2 06/15/23 19:15
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.909 ND 0.729 0.639 80.2 69.8 10 18.0-120 13.2 32
Acenaphthylene 0.909 ND 0.726 0.663 79.9 72.5 10 25.0-120 9.12 32
Anthracene 0.909 ND 0.657 0.632 72.3 69.1 10 22.0-120 3.93 29
Benzidine 1.82 ND ND ND 130 140 10 10.0-120 J5 J5 8.00 40
Benzo(a)anthracene 0.909 ND 0.722 0.751 79.4 82.2 10 25.0-120 4.01 29
Benzo(b)fluoranthene 0.909 ND 0.809 0.768 89.0 84.0 10 19.0-122 5.17 31
Benzo(k)fluoranthene 0.909 ND 0.768 0.704 84.5 76.9 10 23.0-120 8.80 30
Benzo(g,h,i)perylene 0.909 ND 0.837 0.849 92.1 92.8 10 10.0-120 1.34 33
Benzo(a)pyrene 0.909 ND 0.895 0.854 98.5 93.4 10 24.0-120 4.67 30
Bis(2-chlorethoxy)methane 0.909 ND ND ND 61.3 58.6 10 10.0-120 3.86 34
Bis(2-chloroethyl)ether 0.909 ND ND ND 61.1 58.8 10 10.0-120 3.35 40
2,2-Oxybis(1-Chloropropane) 0.909 ND ND ND 69.7 59.7 10 10.0-120 14.8 40
4-Bromophenyl-phenylether 0.909 ND ND ND 71.7 69.1 10 27.0-120 3.07 30
2-Chloronaphthalene 0.909 ND 0.681 0.601 74.9 65.7 10 20.0-120 12.5 32
4-Chlorophenyl-phenylether 0.909 ND ND ND 80.2 70.6 10 24.0-120 12.1 29
Chrysene 0.909 ND 0.782 0.735 86.1 80.3 10 21.0-120 6.31 29
Dibenz(a,h)anthracene 0.909 ND 0.809 0.735 89.0 80.3 10 10.0-120 9.66 32
3,3-Dichlorobenzidine 1.82 ND ND ND 79.8 77.7 10 10.0-120 1.96 34
2,4-Dinitrotoluene 0.909 ND ND ND 81.1 71.8 10 30.0-120 11.5 31
2,6-Dinitrotoluene 0.909 ND ND ND 85.6 78.9 10 25.0-120 7.50 31
Fluoranthene 0.909 ND 0.747 0.653 82.2 71.4 10 18.0-126 13.5 32
Fluorene 0.909 ND 0.695 0.656 76.5 71.7 10 25.0-120 5.83 30
Hexachlorobenzene 0.909 ND ND ND 78.8 69.5 10 27.0-120 11.9 28
Hexachloro-1,3-butadiene 0.909 ND ND ND 69.0 63.2 10 10.0-120 8.17 38
Hexachlorocyclopentadiene 0.909 ND ND ND 0.000 0.000 10 10.0-120 J6 J6 0.000 40
Hexachloroethane 0.909 ND ND ND 53.3 45.1 10 10.0-120 16.0 40
Indeno(1,2,3-cd)pyrene 0.909 ND 0.878 0.766 96.6 83.7 10 10.0-120 13.7 32
Isophorone 0.909 ND ND ND 57.7 58.0 10 13.0-120 1.07 34
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2075724
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1624935-01,02,03
L1624935-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624935-01 06/15/23 18:33 • (MS) R3937963-1 06/15/23 18:54 • (MSD) R3937963-2 06/15/23 19:15
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.909 ND 0.667 0.643 73.4 70.3 10 10.0-120 3.65 35
Nitrobenzene 0.909 ND ND ND 57.7 58.9 10 10.0-120 2.65 36
n-Nitrosodimethylamine 0.909 ND ND ND 0.000 0.000 10 10.0-127 J6 J6 0.000 40
n-Nitrosodiphenylamine 0.909 ND ND ND 66.7 61.2 10 17.0-120 7.96 29
n-Nitrosodi-n-propylamine 0.909 ND ND ND 57.9 56.5 10 10.0-120 1.89 37
Phenanthrene 0.909 ND 0.721 0.677 79.3 74.0 10 17.0-120 6.24 31
Benzylbutyl phthalate 0.909 ND ND ND 95.4 93.4 10 23.0-120 1.47 30
Bis(2-ethylhexyl)phthalate 0.909 ND ND ND 84.7 82.9 10 17.0-126 1.47 30
Di-n-butyl phthalate 0.909 ND ND ND 74.0 71.2 10 30.0-120 3.19 29
Diethyl phthalate 0.909 ND ND ND 78.3 71.7 10 26.0-120 8.23 28
Dimethyl phthalate 0.646 ND ND ND 0.000 0.000 10 25.0-120 J6 J6 0.000 29
Di-n-octyl phthalate 0.909 ND ND ND 88.9 79.1 10 21.0-123 11.0 29
Pyrene 0.909 ND 0.781 0.711 85.9 77.7 10 16.0-121 9.43 32
1,2,4-Trichlorobenzene 0.909 ND ND ND 68.6 65.4 10 12.0-120 4.15 37
4-Chloro-3-methylphenol 0.909 ND ND ND 67.0 68.2 10 15.0-120 2.28 30
2-Chlorophenol 0.909 ND ND ND 67.8 64.0 10 15.0-120 5.15 37
2,4-Dichlorophenol 0.909 ND ND ND 72.9 68.6 10 20.0-120 5.45 31
2,4-Dimethylphenol 0.909 ND ND ND 61.3 62.3 10 10.0-120 2.25 33
4,6-Dinitro-2-methylphenol 0.646 ND ND ND 0.000 0.000 10 10.0-120 J6 J6 0.000 39
2,4-Dinitrophenol 0.646 ND ND ND 0.000 0.000 10 10.0-121 J6 J6 0.000 40
2-Nitrophenol 0.909 ND ND ND 61.6 60.2 10 12.0-120 1.77 39
4-Nitrophenol 0.909 ND ND ND 86.5 73.2 10 10.0-137 16.0 32
Pentachlorophenol 0.909 ND ND ND 66.1 56.2 10 10.0-160 15.7 31
Phenol 0.909 ND ND ND 61.0 59.1 10 12.0-120 2.57 38
2,4,6-Trichlorophenol 0.909 ND ND ND 82.0 78.0 10 19.0-120 4.44 32
(S) Nitrobenzene-d5 52.0 44.9 10.0-122
(S) 2-Fluorobiphenyl 73.7 63.4 15.0-120
(S) p-Terphenyl-d14 74.9 68.0 10.0-120
(S) Phenol-d5 63.5 57.2 10.0-120
(S) 2-Fluorophenol 68.0 61.5 12.0-120
(S) 2,4,6-Tribromophenol 70.1 62.6 10.0-127
Sample Narrative:
OS: Dilution due to matrix impact during extraction procedure
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2077933
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1624935-02,03
Method Blank (MB)
(MB) R3938197-2 06/15/23 16:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 93.5 23.0-120
(S) Nitrobenzene-d5 73.7 14.0-149
(S) 2-Fluorobiphenyl 83.0 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3938197-1 06/15/23 16:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0783 97.9 50.0-126
Acenaphthene 0.0800 0.0775 96.9 50.0-120
Acenaphthylene 0.0800 0.0775 96.9 50.0-120
Benzo(a)anthracene 0.0800 0.0712 89.0 45.0-120
Benzo(a)pyrene 0.0800 0.0756 94.5 42.0-120
Benzo(b)fluoranthene 0.0800 0.0730 91.3 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0787 98.4 45.0-125
Benzo(k)fluoranthene 0.0800 0.0796 99.5 49.0-125
Chrysene 0.0800 0.0793 99.1 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0780 97.5 47.0-125
Fluoranthene 0.0800 0.0839 105 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2077933
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1624935-02,03
Laboratory Control Sample (LCS)
(LCS) R3938197-1 06/15/23 16:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0842 105 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0752 94.0 46.0-125
Naphthalene 0.0800 0.0768 96.0 50.0-120
Phenanthrene 0.0800 0.0763 95.4 47.0-120
Pyrene 0.0800 0.0806 101 43.0-123
1-Methylnaphthalene 0.0800 0.0798 99.8 51.0-121
2-Methylnaphthalene 0.0800 0.0823 103 50.0-120
2-Chloronaphthalene 0.0800 0.0744 93.0 50.0-120
(S) p-Terphenyl-d14 98.1 23.0-120
(S) Nitrobenzene-d5 90.3 14.0-149
(S) 2-Fluorobiphenyl 95.3 34.0-125
L1624933-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624933-04 06/15/23 20:42 • (MS) R3938197-3 06/15/23 21:01 • (MSD) R3938197-4 06/15/23 21:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0764 ND 0.0573 0.0578 75.0 75.3 1 10.0-145 0.869 30
Acenaphthene 0.0764 0.0462 0.0840 0.0911 49.5 58.5 1 14.0-127 8.11 27
Acenaphthylene 0.0764 ND 0.0682 0.0677 89.3 88.2 1 21.0-124 0.736 25
Benzo(a)anthracene 0.0764 ND 0.0652 0.0795 82.8 101 1 10.0-139 19.8 30
Benzo(a)pyrene 0.0764 ND 0.0691 0.0768 90.4 100 1 10.0-141 10.6 31
Benzo(b)fluoranthene 0.0764 ND 0.0672 0.0727 83.3 90.1 1 10.0-140 7.86 36
Benzo(g,h,i)perylene 0.0764 ND 0.0662 0.0682 83.4 85.5 1 10.0-140 2.98 33
Benzo(k)fluoranthene 0.0764 ND 0.0693 0.0659 90.7 85.8 1 10.0-137 5.03 31
Chrysene 0.0764 ND 0.0711 0.0815 93.1 106 1 10.0-145 13.6 30
Dibenz(a,h)anthracene 0.0764 ND 0.0633 0.0615 82.9 80.1 1 10.0-132 2.88 31
Fluoranthene 0.0764 0.00936 0.0792 0.113 91.4 135 1 10.0-153 J3 35.2 33
Fluorene 0.0764 ND 0.106 0.118 139 154 1 11.0-130 J5 J5 10.7 29
Indeno(1,2,3-cd)pyrene 0.0764 ND 0.0629 0.0687 82.3 89.5 1 10.0-137 8.81 32
Naphthalene 0.0764 0.121 0.286 0.390 216 350 1 10.0-135 J5 J3 J5 30.8 27
Phenanthrene 0.0764 0.0834 0.120 0.185 47.9 132 1 10.0-144 J3 42.6 31
Pyrene 0.0764 0.00936 0.0769 0.102 88.4 121 1 10.0-148 28.1 35
1-Methylnaphthalene 0.0764 1.43 1.01 1.50 0.000 91.1 1 10.0-142 V J3 39.0 28
2-Methylnaphthalene 0.0764 ND 0.0727 0.0663 95.2 86.3 1 10.0-137 9.21 28
2-Chloronaphthalene 0.0764 ND 0.0622 0.0640 81.4 83.3 1 29.0-120 2.85 24
(S) p-Terphenyl-d14 87.3 85.8 23.0-120
(S) Nitrobenzene-d5 0.000 0.000 14.0-149 J2 J2
(S) 2-Fluorobiphenyl 63.8 54.7 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2077933
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1624935-02,03
L1624933-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624933-04 06/15/23 20:42 • (MS) R3938197-3 06/15/23 21:01 • (MSD) R3938197-4 06/15/23 21:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Sample Narrative:
OS: Surrogate failure due to matrix interference
MS: Surrogate failure due to matrix interference
MSD: Surrogate failure due to matrix interference
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078829
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1624935-01
Method Blank (MB)
(MB) R3937768-2 06/16/23 11:46
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 76.6 23.0-120
(S) Nitrobenzene-d5 81.3 14.0-149
(S) 2-Fluorobiphenyl 71.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3937768-1 06/16/23 11:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0646 80.7 50.0-126
Acenaphthene 0.0800 0.0701 87.6 50.0-120
Acenaphthylene 0.0800 0.0648 81.0 50.0-120
Benzo(a)anthracene 0.0800 0.0681 85.1 45.0-120
Benzo(a)pyrene 0.0800 0.0716 89.5 42.0-120
Benzo(b)fluoranthene 0.0800 0.0732 91.5 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0717 89.6 45.0-125
Benzo(k)fluoranthene 0.0800 0.0721 90.1 49.0-125
Chrysene 0.0800 0.0736 92.0 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0641 80.1 47.0-125
Fluoranthene 0.0800 0.0690 86.3 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2078829
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1624935-01
Laboratory Control Sample (LCS)
(LCS) R3937768-1 06/16/23 11:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0708 88.5 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0653 81.6 46.0-125
Naphthalene 0.0800 0.0708 88.5 50.0-120
Phenanthrene 0.0800 0.0688 86.0 47.0-120
Pyrene 0.0800 0.0798 99.8 43.0-123
1-Methylnaphthalene 0.0800 0.0672 84.0 51.0-121
2-Methylnaphthalene 0.0800 0.0685 85.6 50.0-120
2-Chloronaphthalene 0.0800 0.0696 87.0 50.0-120
(S) p-Terphenyl-d14 79.1 23.0-120
(S) Nitrobenzene-d5 89.1 14.0-149
(S) 2-Fluorobiphenyl 76.5 34.0-125
L1624935-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624935-01 06/16/23 18:27 • (MS) R3937768-3 06/16/23 18:44 • (MSD) R3937768-4 06/16/23 19:02
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.112 ND 0.0913 0.126 81.5 112 1 10.0-145 J3 31.8 30
Acenaphthene 0.112 ND 0.0922 0.134 82.3 120 1 14.0-127 J3 37.2 27
Acenaphthylene 0.112 ND 0.0943 0.102 84.2 91.5 1 21.0-124 8.30 25
Benzo(a)anthracene 0.112 0.00922 0.173 0.142 146 119 1 10.0-139 J5 19.6 30
Benzo(a)pyrene 0.112 0.0109 0.298 0.144 257 118 1 10.0-141 J5 J3 70.1 31
Benzo(b)fluoranthene 0.112 0.00967 0.318 0.126 275 104 1 10.0-140 J5 J3 86.6 36
Benzo(g,h,i)perylene 0.112 0.0163 0.172 0.122 139 94.1 1 10.0-140 J3 34.1 33
Benzo(k)fluoranthene 0.112 ND 0.163 0.107 146 95.1 1 10.0-137 J5 J3 42.0 31
Chrysene 0.112 0.0102 0.212 0.172 181 144 1 10.0-145 J5 21.2 30
Dibenz(a,h)anthracene 0.112 ND 0.105 0.0988 93.8 88.2 1 10.0-132 6.21 31
Fluoranthene 0.112 0.0111 0.140 0.186 115 156 1 10.0-153 J5 28.2 33
Fluorene 0.112 ND 0.0910 0.116 81.3 104 1 11.0-130 24.3 29
Indeno(1,2,3-cd)pyrene 0.112 ND 0.182 0.118 156 99.3 1 10.0-137 J5 J3 42.8 32
Naphthalene 0.112 ND 0.101 0.117 90.2 105 1 10.0-135 14.9 27
Phenanthrene 0.112 0.00887 0.103 0.191 84.4 163 1 10.0-144 J3 J5 59.7 31
Pyrene 0.112 0.0211 0.184 0.203 146 162 1 10.0-148 J5 9.45 35
1-Methylnaphthalene 0.112 ND 0.0926 0.109 82.7 97.4 1 10.0-142 16.3 28
2-Methylnaphthalene 0.112 ND 0.0984 0.116 87.8 104 1 10.0-137 16.7 28
2-Chloronaphthalene 0.112 ND 0.0889 0.0985 79.4 87.9 1 29.0-120 10.2 24
(S) p-Terphenyl-d14 85.7 86.7 23.0-120
(S) Nitrobenzene-d5 114 114 14.0-149
(S) 2-Fluorobiphenyl 85.7 86.9 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
July 13, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1631472
Samples Received:06/30/2023
Project Number:117-9187001
Description:Recycled Earth 117-9187001
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
July 13, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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July 13, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
ST-CS-1 L1631472-01 6
ST-CS-2 L1631472-02 10
ST-CS-3 L1631472-03 14
ST-CS-4 L1631472-04 18
ST-CS-DUPE L1631472-05 22
ST-CS-5 L1631472-06 26
ST-CS-6 L1631472-07 30
ST-CS-7 L1631472-08 34
ST-CS-COMP L1631472-09 38
Qc: Quality Control Summary 42
Total Solids by Method 2540 G-2011 42
Volatile Organic Compounds (GC) by Method 8015D/GRO 43
Volatile Organic Compounds (GC/MS) by Method 8260B 46
Semi-Volatile Organic Compounds (GC) by Method 8015 54
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 55
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 67
Gl: Glossary of Terms 73
Al: Accreditations & Locations 74
Sc: Sample Chain of Custody 75
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
ST-CS-1 L1631472-01 Solid Richie Torney 06/29/23 10:45 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25 06/29/23 10:45 07/07/23 18:33 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1 06/29/23 10:45 07/07/23 00:29 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/11/23 19:43 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089916 1 07/06/23 08:21 07/06/23 17:40 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091376 1 07/11/23 10:15 07/12/23 00:38 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-2 L1631472-02 Solid Richie Torney 06/29/23 10:50 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25 06/29/23 10:50 07/07/23 19:12 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1 06/29/23 10:50 07/07/23 00:48 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/11/23 10:35 KAP Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 1 07/07/23 22:26 07/08/23 15:41 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091376 1 07/11/23 10:15 07/12/23 00:56 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-3 L1631472-03 Solid Richie Torney 06/29/23 10:55 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25 06/29/23 10:55 07/07/23 20:18 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1 06/29/23 10:55 07/07/23 01:07 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/11/23 19:56 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 1 07/07/23 22:26 07/08/23 18:36 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091376 1 07/11/23 10:15 07/12/23 01:13 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-4 L1631472-04 Solid Richie Torney 06/29/23 11:03 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2093889 25 06/29/23 11:03 07/13/23 11:26 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2091079 1.22 06/29/23 11:03 07/08/23 12:59 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 20 07/10/23 19:52 07/12/23 03:35 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 2 07/07/23 22:26 07/10/23 20:12 MBE Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091375 1 07/10/23 17:08 07/11/23 06:00 MBE Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-DUPE L1631472-05 Solid Richie Torney 06/29/23 11:03 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25.5 06/29/23 11:03 07/07/23 20:41 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1.02 06/29/23 11:03 07/07/23 01:27 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/11/23 11:02 KAP Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 1 07/07/23 22:26 07/10/23 19:28 MBE Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091376 1 07/11/23 10:15 07/12/23 01:32 AED Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
ST-CS-5 L1631472-06 Solid Richie Torney 06/29/23 11:15 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2093590 25 06/29/23 11:15 07/12/23 21:18 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2091079 1 06/29/23 11:15 07/08/23 12:41 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 20 07/10/23 19:52 07/12/23 04:39 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 2 07/07/23 22:26 07/10/23 21:17 MBE Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091376 1 07/11/23 10:15 07/12/23 01:50 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-6 L1631472-07 Solid Richie Torney 06/29/23 11:22 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25 06/29/23 11:22 07/07/23 21:04 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1 06/29/23 11:22 07/07/23 01:46 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/11/23 10:22 KAP Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 1 07/07/23 22:26 07/08/23 16:03 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091376 1 07/11/23 10:15 07/12/23 02:08 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-7 L1631472-08 Solid Richie Torney 06/29/23 11:30 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25 06/29/23 11:30 07/07/23 21:26 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1 06/29/23 11:30 07/07/23 02:05 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/11/23 10:49 KAP Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 1 07/07/23 22:26 07/08/23 18:14 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091526 1 07/10/23 08:46 07/10/23 20:23 AED Mt. Juliet, TN
Collected by Collected date/time Received date/time
ST-CS-COMP L1631472-09 Solid Richie Torney 06/29/23 11:35 06/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2089245 1 07/05/23 10:52 07/05/23 11:15 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2090723 25 06/29/23 11:35 07/07/23 21:49 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2090578 1 06/29/23 11:35 07/07/23 02:24 BAM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2091569 1 07/10/23 19:52 07/12/23 03:00 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2089936 5 07/07/23 22:26 07/08/23 20:03 DSH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2091526 1 07/10/23 08:46 07/10/23 20:41 AED Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1631472
ST-CS-1
Collected date/time: 06/29/23 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.4 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.880 J 0.838 3.86 25 07/07/2023 18:33 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)96.4 77.0-120 07/07/2023 18:33 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0563 0.0772 1 07/07/2023 00:29 WG2090578
Acrylonitrile U 0.00557 0.0193 1 07/07/2023 00:29 WG2090578
Benzene U 0.000721 0.00154 1 07/07/2023 00:29 WG2090578
Bromobenzene U 0.00139 0.0193 1 07/07/2023 00:29 WG2090578
Bromodichloromethane U 0.00112 0.00386 1 07/07/2023 00:29 WG2090578
Bromoform U 0.00181 0.0386 1 07/07/2023 00:29 WG2090578
Bromomethane U 0.00304 0.0193 1 07/07/2023 00:29 WG2090578
n-Butylbenzene U 0.00810 0.0193 1 07/07/2023 00:29 WG2090578
sec-Butylbenzene U 0.00444 0.0193 1 07/07/2023 00:29 WG2090578
tert-Butylbenzene U 0.00301 0.00772 1 07/07/2023 00:29 WG2090578
Carbon tetrachloride U 0.00139 0.00772 1 07/07/2023 00:29 WG2090578
Chlorobenzene U 0.000324 0.00386 1 07/07/2023 00:29 WG2090578
Chlorodibromomethane U 0.000944 0.00386 1 07/07/2023 00:29 WG2090578
Chloroethane U 0.00262 0.00772 1 07/07/2023 00:29 WG2090578
Chloroform U 0.00159 0.00386 1 07/07/2023 00:29 WG2090578
Chloromethane U 0.00671 0.0193 1 07/07/2023 00:29 WG2090578
2-Chlorotoluene U 0.00133 0.00386 1 07/07/2023 00:29 WG2090578
4-Chlorotoluene U 0.000694 0.00772 1 07/07/2023 00:29 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00602 0.0386 1 07/07/2023 00:29 WG2090578
1,2-Dibromoethane U 0.00100 0.00386 1 07/07/2023 00:29 WG2090578
Dibromomethane U 0.00116 0.00772 1 07/07/2023 00:29 WG2090578
1,2-Dichlorobenzene U 0.000656 0.00772 1 07/07/2023 00:29 WG2090578
1,3-Dichlorobenzene U 0.000926 0.00772 1 07/07/2023 00:29 WG2090578
1,4-Dichlorobenzene U 0.00108 0.00772 1 07/07/2023 00:29 WG2090578
Dichlorodifluoromethane U 0.00248 0.00386 1 07/07/2023 00:29 WG2090578
1,1-Dichloroethane U 0.000758 0.00386 1 07/07/2023 00:29 WG2090578
1,2-Dichloroethane U 0.00100 0.00386 1 07/07/2023 00:29 WG2090578
1,1-Dichloroethene U 0.000935 0.00386 1 07/07/2023 00:29 WG2090578
cis-1,2-Dichloroethene U 0.00113 0.00386 1 07/07/2023 00:29 WG2090578
trans-1,2-Dichloroethene U 0.00161 0.00772 1 07/07/2023 00:29 WG2090578
1,2-Dichloropropane U 0.00219 0.00772 1 07/07/2023 00:29 WG2090578
1,1-Dichloropropene U 0.00125 0.00386 1 07/07/2023 00:29 WG2090578
1,3-Dichloropropane U 0.000773 0.00772 1 07/07/2023 00:29 WG2090578
cis-1,3-Dichloropropene U 0.00117 0.00386 1 07/07/2023 00:29 WG2090578
trans-1,3-Dichloropropene U 0.00176 0.00772 1 07/07/2023 00:29 WG2090578
2,2-Dichloropropane U 0.00213 0.00386 1 07/07/2023 00:29 WG2090578
Di-isopropyl ether U 0.000633 0.00154 1 07/07/2023 00:29 WG2090578
Ethylbenzene U 0.00114 0.00386 1 07/07/2023 00:29 WG2090578
Hexachloro-1,3-butadiene U 0.00926 0.0386 1 07/07/2023 00:29 WG2090578
Isopropylbenzene U 0.000656 0.00386 1 07/07/2023 00:29 WG2090578
p-Isopropyltoluene U 0.00394 0.00772 1 07/07/2023 00:29 WG2090578
2-Butanone (MEK)U 0.0980 0.154 1 07/07/2023 00:29 WG2090578
Methylene Chloride U 0.0102 0.0386 1 07/07/2023 00:29 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1631472
ST-CS-1
Collected date/time: 06/29/23 10:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) 0.0156 J 0.00352 0.0386 1 07/07/2023 00:29 WG2090578
Methyl tert-butyl ether U 0.000540 0.00154 1 07/07/2023 00:29 WG2090578
Naphthalene U J4 0.00753 0.0193 1 07/07/2023 00:29 WG2090578
n-Propylbenzene U 0.00147 0.00772 1 07/07/2023 00:29 WG2090578
Styrene U 0.000353 0.0193 1 07/07/2023 00:29 WG2090578
1,1,1,2-Tetrachloroethane U 0.00146 0.00386 1 07/07/2023 00:29 WG2090578
1,1,2,2-Tetrachloroethane U 0.00107 0.00386 1 07/07/2023 00:29 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00116 0.00386 1 07/07/2023 00:29 WG2090578
Tetrachloroethene U 0.00138 0.00386 1 07/07/2023 00:29 WG2090578
Toluene U 0.00201 0.00772 1 07/07/2023 00:29 WG2090578
1,2,3-Trichlorobenzene U 0.0113 0.0193 1 07/07/2023 00:29 WG2090578
1,2,4-Trichlorobenzene U 0.00679 0.0193 1 07/07/2023 00:29 WG2090578
1,1,1-Trichloroethane U 0.00142 0.00386 1 07/07/2023 00:29 WG2090578
1,1,2-Trichloroethane U 0.000921 0.00386 1 07/07/2023 00:29 WG2090578
Trichloroethene U 0.000901 0.00154 1 07/07/2023 00:29 WG2090578
Trichlorofluoromethane U 0.00128 0.00386 1 07/07/2023 00:29 WG2090578
1,2,3-Trichloropropane U 0.00250 0.0193 1 07/07/2023 00:29 WG2090578
1,2,4-Trimethylbenzene U 0.00244 0.00772 1 07/07/2023 00:29 WG2090578
1,2,3-Trimethylbenzene U 0.00244 0.00772 1 07/07/2023 00:29 WG2090578
1,3,5-Trimethylbenzene U 0.00309 0.00772 1 07/07/2023 00:29 WG2090578
Vinyl chloride U 0.00179 0.00386 1 07/07/2023 00:29 WG2090578
Xylenes, Total U 0.00136 0.0100 1 07/07/2023 00:29 WG2090578
(S) Toluene-d8 111 75.0-131 07/07/2023 00:29 WG2090578
(S) 4-Bromofluorobenzene 102 67.0-138 07/07/2023 00:29 WG2090578
(S) 1,2-Dichloroethane-d4 95.8 70.0-130 07/07/2023 00:29 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.28 J 0.957 4.98 1 07/11/2023 19:43 WG2091569
(S) o-Terphenyl 57.8 18.0-148 07/11/2023 19:43 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00671 0.0414 1 07/06/2023 17:40 WG2089916
Acenaphthylene U 0.00583 0.0414 1 07/06/2023 17:40 WG2089916
Anthracene U 0.00738 0.0414 1 07/06/2023 17:40 WG2089916
Benzidine U 0.0779 2.08 1 07/06/2023 17:40 WG2089916
Benzo(a)anthracene U 0.00730 0.0414 1 07/06/2023 17:40 WG2089916
Benzo(b)fluoranthene U 0.00773 0.0414 1 07/06/2023 17:40 WG2089916
Benzo(k)fluoranthene U 0.00736 0.0414 1 07/06/2023 17:40 WG2089916
Benzo(g,h,i)perylene U 0.00758 0.0414 1 07/06/2023 17:40 WG2089916
Benzo(a)pyrene U 0.00770 0.0414 1 07/06/2023 17:40 WG2089916
Bis(2-chlorethoxy)methane U 0.0124 0.414 1 07/06/2023 17:40 WG2089916
Bis(2-chloroethyl)ether U 0.0137 0.414 1 07/06/2023 17:40 WG2089916
2,2-Oxybis(1-Chloropropane) U 0.0179 0.414 1 07/06/2023 17:40 WG2089916
4-Bromophenyl-phenylether U 0.0146 0.414 1 07/06/2023 17:40 WG2089916
2-Chloronaphthalene U 0.00728 0.0414 1 07/06/2023 17:40 WG2089916
4-Chlorophenyl-phenylether U 0.0144 0.414 1 07/06/2023 17:40 WG2089916
Chrysene U 0.00824 0.0414 1 07/06/2023 17:40 WG2089916
Dibenz(a,h)anthracene U 0.0115 0.0414 1 07/06/2023 17:40 WG2089916
1,2-Dichlorobenzene U 0.0123 0.414 1 07/06/2023 17:40 WG2089916
1,3-Dichlorobenzene U 0.0126 0.414 1 07/06/2023 17:40 WG2089916
1,4-Dichlorobenzene U 0.0123 0.414 1 07/06/2023 17:40 WG2089916
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1631472
ST-CS-1
Collected date/time: 06/29/23 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0153 0.414 1 07/06/2023 17:40 WG2089916
2,4-Dinitrotoluene U 0.0119 0.414 1 07/06/2023 17:40 WG2089916
2,6-Dinitrotoluene U 0.0136 0.414 1 07/06/2023 17:40 WG2089916
Fluoranthene U 0.00748 0.0414 1 07/06/2023 17:40 WG2089916
Fluorene U 0.00674 0.0414 1 07/06/2023 17:40 WG2089916
Hexachlorobenzene U 0.0147 0.414 1 07/06/2023 17:40 WG2089916
Hexachloro-1,3-butadiene U 0.0139 0.414 1 07/06/2023 17:40 WG2089916
Hexachlorocyclopentadiene U 0.0218 0.414 1 07/06/2023 17:40 WG2089916
Hexachloroethane U 0.0163 0.414 1 07/06/2023 17:40 WG2089916
Indeno(1,2,3-cd)pyrene U 0.0117 0.0414 1 07/06/2023 17:40 WG2089916
Isophorone U 0.0127 0.414 1 07/06/2023 17:40 WG2089916
Naphthalene U 0.0104 0.0414 1 07/06/2023 17:40 WG2089916
Nitrobenzene U 0.0144 0.414 1 07/06/2023 17:40 WG2089916
n-Nitrosodimethylamine U 0.0615 0.414 1 07/06/2023 17:40 WG2089916
n-Nitrosodiphenylamine U 0.0314 0.414 1 07/06/2023 17:40 WG2089916
n-Nitrosodi-n-propylamine U 0.0138 0.414 1 07/06/2023 17:40 WG2089916
Phenanthrene U 0.00822 0.0414 1 07/06/2023 17:40 WG2089916
Benzylbutyl phthalate U 0.0129 0.414 1 07/06/2023 17:40 WG2089916
Bis(2-ethylhexyl)phthalate U 0.0525 0.414 1 07/06/2023 17:40 WG2089916
Di-n-butyl phthalate U 0.0142 0.414 1 07/06/2023 17:40 WG2089916
Diethyl phthalate U 0.0137 0.414 1 07/06/2023 17:40 WG2089916
Dimethyl phthalate U 0.0878 0.414 1 07/06/2023 17:40 WG2089916
Di-n-octyl phthalate U 0.0280 0.414 1 07/06/2023 17:40 WG2089916
Pyrene U 0.00806 0.0414 1 07/06/2023 17:40 WG2089916
1,2,4-Trichlorobenzene U 0.0129 0.414 1 07/06/2023 17:40 WG2089916
4-Chloro-3-methylphenol U 0.0134 0.414 1 07/06/2023 17:40 WG2089916
2-Chlorophenol U 0.0137 0.414 1 07/06/2023 17:40 WG2089916
2,4-Dichlorophenol U 0.0121 0.414 1 07/06/2023 17:40 WG2089916
2,4-Dimethylphenol U 0.0108 0.414 1 07/06/2023 17:40 WG2089916
4,6-Dinitro-2-methylphenol U 0.0939 0.414 1 07/06/2023 17:40 WG2089916
2,4-Dinitrophenol U 0.0969 0.414 1 07/06/2023 17:40 WG2089916
2-Nitrophenol U 0.0148 0.414 1 07/06/2023 17:40 WG2089916
4-Nitrophenol U 0.0129 0.414 1 07/06/2023 17:40 WG2089916
Pentachlorophenol U 0.0111 0.414 1 07/06/2023 17:40 WG2089916
Phenol U 0.0167 0.414 1 07/06/2023 17:40 WG2089916
2,4,6-Trichlorophenol U 0.0133 0.414 1 07/06/2023 17:40 WG2089916
(S) 2-Fluorophenol 44.3 12.0-120 07/06/2023 17:40 WG2089916
(S) Phenol-d5 41.2 10.0-120 07/06/2023 17:40 WG2089916
(S) Nitrobenzene-d5 37.7 10.0-122 07/06/2023 17:40 WG2089916
(S) 2-Fluorobiphenyl 37.7 15.0-120 07/06/2023 17:40 WG2089916
(S) 2,4,6-Tribromophenol 51.2 10.0-127 07/06/2023 17:40 WG2089916
(S) p-Terphenyl-d14 55.9 10.0-120 07/06/2023 17:40 WG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene 0.0260 0.00286 0.00746 1 07/12/2023 00:38 WG2091376
Acenaphthene 0.00439 J 0.00260 0.00746 1 07/12/2023 00:38 WG2091376
Acenaphthylene U 0.00269 0.00746 1 07/12/2023 00:38 WG2091376
Benzo(a)anthracene 0.260 0.00215 0.00746 1 07/12/2023 00:38 WG2091376
Benzo(a)pyrene 0.216 0.00223 0.00746 1 07/12/2023 00:38 WG2091376
Benzo(b)fluoranthene 0.294 0.00190 0.00746 1 07/12/2023 00:38 WG2091376
Benzo(g,h,i)perylene 0.112 0.00220 0.00746 1 07/12/2023 00:38 WG2091376
Benzo(k)fluoranthene 0.0950 0.00267 0.00746 1 07/12/2023 00:38 WG2091376
Chrysene 0.214 0.00289 0.00746 1 07/12/2023 00:38 WG2091376
Dibenz(a,h)anthracene 0.0285 0.00214 0.00746 1 07/12/2023 00:38 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1631472
ST-CS-1
Collected date/time: 06/29/23 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluoranthene 0.412 0.00282 0.00746 1 07/12/2023 00:38 WG2091376
Fluorene 0.00401 J 0.00255 0.00746 1 07/12/2023 00:38 WG2091376
Indeno(1,2,3-cd)pyrene 0.144 0.00225 0.00746 1 07/12/2023 00:38 WG2091376
Naphthalene U 0.00508 0.0249 1 07/12/2023 00:38 WG2091376
Phenanthrene 0.0972 0.00287 0.00746 1 07/12/2023 00:38 WG2091376
Pyrene 0.340 0.00249 0.00746 1 07/12/2023 00:38 WG2091376
1-Methylnaphthalene U 0.00559 0.0249 1 07/12/2023 00:38 WG2091376
2-Methylnaphthalene U 0.00531 0.0249 1 07/12/2023 00:38 WG2091376
2-Chloronaphthalene U 0.00580 0.0249 1 07/12/2023 00:38 WG2091376
(S) p-Terphenyl-d14 82.9 23.0-120 07/12/2023 00:38 WG2091376
(S) Nitrobenzene-d5 98.7 14.0-149 07/12/2023 00:38 WG2091376
(S) 2-Fluorobiphenyl 77.8 34.0-125 07/12/2023 00:38 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1631472
ST-CS-2
Collected date/time: 06/29/23 10:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.0 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U 0.826 3.80 25 07/07/2023 19:12 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)96.6 77.0-120 07/07/2023 19:12 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0555 0.0760 1 07/07/2023 00:48 WG2090578
Acrylonitrile U 0.00549 0.0190 1 07/07/2023 00:48 WG2090578
Benzene U 0.000710 0.00152 1 07/07/2023 00:48 WG2090578
Bromobenzene U 0.00137 0.0190 1 07/07/2023 00:48 WG2090578
Bromodichloromethane U 0.00110 0.00380 1 07/07/2023 00:48 WG2090578
Bromoform U 0.00178 0.0380 1 07/07/2023 00:48 WG2090578
Bromomethane U 0.00300 0.0190 1 07/07/2023 00:48 WG2090578
n-Butylbenzene U 0.00799 0.0190 1 07/07/2023 00:48 WG2090578
sec-Butylbenzene U 0.00438 0.0190 1 07/07/2023 00:48 WG2090578
tert-Butylbenzene U 0.00297 0.00760 1 07/07/2023 00:48 WG2090578
Carbon tetrachloride U 0.00137 0.00760 1 07/07/2023 00:48 WG2090578
Chlorobenzene U 0.000319 0.00380 1 07/07/2023 00:48 WG2090578
Chlorodibromomethane U 0.000931 0.00380 1 07/07/2023 00:48 WG2090578
Chloroethane U 0.00259 0.00760 1 07/07/2023 00:48 WG2090578
Chloroform U 0.00157 0.00380 1 07/07/2023 00:48 WG2090578
Chloromethane U 0.00662 0.0190 1 07/07/2023 00:48 WG2090578
2-Chlorotoluene U 0.00132 0.00380 1 07/07/2023 00:48 WG2090578
4-Chlorotoluene U 0.000684 0.00760 1 07/07/2023 00:48 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00593 0.0380 1 07/07/2023 00:48 WG2090578
1,2-Dibromoethane U 0.000986 0.00380 1 07/07/2023 00:48 WG2090578
Dibromomethane U 0.00114 0.00760 1 07/07/2023 00:48 WG2090578
1,2-Dichlorobenzene U 0.000646 0.00760 1 07/07/2023 00:48 WG2090578
1,3-Dichlorobenzene U 0.000913 0.00760 1 07/07/2023 00:48 WG2090578
1,4-Dichlorobenzene U 0.00106 0.00760 1 07/07/2023 00:48 WG2090578
Dichlorodifluoromethane U 0.00245 0.00380 1 07/07/2023 00:48 WG2090578
1,1-Dichloroethane U 0.000747 0.00380 1 07/07/2023 00:48 WG2090578
1,2-Dichloroethane U 0.000987 0.00380 1 07/07/2023 00:48 WG2090578
1,1-Dichloroethene U 0.000922 0.00380 1 07/07/2023 00:48 WG2090578
cis-1,2-Dichloroethene U 0.00112 0.00380 1 07/07/2023 00:48 WG2090578
trans-1,2-Dichloroethene U 0.00158 0.00760 1 07/07/2023 00:48 WG2090578
1,2-Dichloropropane U 0.00216 0.00760 1 07/07/2023 00:48 WG2090578
1,1-Dichloropropene U 0.00123 0.00380 1 07/07/2023 00:48 WG2090578
1,3-Dichloropropane U 0.000762 0.00760 1 07/07/2023 00:48 WG2090578
cis-1,3-Dichloropropene U 0.00115 0.00380 1 07/07/2023 00:48 WG2090578
trans-1,3-Dichloropropene U 0.00173 0.00760 1 07/07/2023 00:48 WG2090578
2,2-Dichloropropane U 0.00210 0.00380 1 07/07/2023 00:48 WG2090578
Di-isopropyl ether U 0.000624 0.00152 1 07/07/2023 00:48 WG2090578
Ethylbenzene U 0.00112 0.00380 1 07/07/2023 00:48 WG2090578
Hexachloro-1,3-butadiene U 0.00913 0.0380 1 07/07/2023 00:48 WG2090578
Isopropylbenzene U 0.000646 0.00380 1 07/07/2023 00:48 WG2090578
p-Isopropyltoluene U 0.00388 0.00760 1 07/07/2023 00:48 WG2090578
2-Butanone (MEK)U 0.0966 0.152 1 07/07/2023 00:48 WG2090578
Methylene Chloride U 0.0101 0.0380 1 07/07/2023 00:48 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1631472
ST-CS-2
Collected date/time: 06/29/23 10:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) 0.0219 J 0.00347 0.0380 1 07/07/2023 00:48 WG2090578
Methyl tert-butyl ether U 0.000532 0.00152 1 07/07/2023 00:48 WG2090578
Naphthalene U J4 0.00742 0.0190 1 07/07/2023 00:48 WG2090578
n-Propylbenzene U 0.00144 0.00760 1 07/07/2023 00:48 WG2090578
Styrene 0.000665 J 0.000348 0.0190 1 07/07/2023 00:48 WG2090578
1,1,1,2-Tetrachloroethane U 0.00144 0.00380 1 07/07/2023 00:48 WG2090578
1,1,2,2-Tetrachloroethane U 0.00106 0.00380 1 07/07/2023 00:48 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00115 0.00380 1 07/07/2023 00:48 WG2090578
Tetrachloroethene U 0.00136 0.00380 1 07/07/2023 00:48 WG2090578
Toluene 0.0123 0.00198 0.00760 1 07/07/2023 00:48 WG2090578
1,2,3-Trichlorobenzene U 0.0111 0.0190 1 07/07/2023 00:48 WG2090578
1,2,4-Trichlorobenzene U 0.00669 0.0190 1 07/07/2023 00:48 WG2090578
1,1,1-Trichloroethane U 0.00140 0.00380 1 07/07/2023 00:48 WG2090578
1,1,2-Trichloroethane U 0.000908 0.00380 1 07/07/2023 00:48 WG2090578
Trichloroethene U 0.000888 0.00152 1 07/07/2023 00:48 WG2090578
Trichlorofluoromethane U 0.00126 0.00380 1 07/07/2023 00:48 WG2090578
1,2,3-Trichloropropane U 0.00246 0.0190 1 07/07/2023 00:48 WG2090578
1,2,4-Trimethylbenzene U 0.00240 0.00760 1 07/07/2023 00:48 WG2090578
1,2,3-Trimethylbenzene U 0.00240 0.00760 1 07/07/2023 00:48 WG2090578
1,3,5-Trimethylbenzene U 0.00304 0.00760 1 07/07/2023 00:48 WG2090578
Vinyl chloride U 0.00176 0.00380 1 07/07/2023 00:48 WG2090578
Xylenes, Total 0.00395 J 0.00134 0.00989 1 07/07/2023 00:48 WG2090578
(S) Toluene-d8 112 75.0-131 07/07/2023 00:48 WG2090578
(S) 4-Bromofluorobenzene 99.7 67.0-138 07/07/2023 00:48 WG2090578
(S) 1,2-Dichloroethane-d4 92.8 70.0-130 07/07/2023 00:48 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.34 J 0.961 5.00 1 07/11/2023 10:35 WG2091569
(S) o-Terphenyl 62.8 18.0-148 07/11/2023 10:35 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00674 0.0416 1 07/08/2023 15:41 WG2089936
Acenaphthylene U 0.00586 0.0416 1 07/08/2023 15:41 WG2089936
Anthracene U 0.00741 0.0416 1 07/08/2023 15:41 WG2089936
Benzidine U 0.0782 2.09 1 07/08/2023 15:41 WG2089936
Benzo(a)anthracene U 0.00734 0.0416 1 07/08/2023 15:41 WG2089936
Benzo(b)fluoranthene U 0.00776 0.0416 1 07/08/2023 15:41 WG2089936
Benzo(k)fluoranthene U 0.00740 0.0416 1 07/08/2023 15:41 WG2089936
Benzo(g,h,i)perylene U 0.00761 0.0416 1 07/08/2023 15:41 WG2089936
Benzo(a)pyrene U 0.00774 0.0416 1 07/08/2023 15:41 WG2089936
Bis(2-chlorethoxy)methane U 0.0125 0.416 1 07/08/2023 15:41 WG2089936
Bis(2-chloroethyl)ether U 0.0137 0.416 1 07/08/2023 15:41 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0180 0.416 1 07/08/2023 15:41 WG2089936
4-Bromophenyl-phenylether U 0.0146 0.416 1 07/08/2023 15:41 WG2089936
2-Chloronaphthalene U 0.00731 0.0416 1 07/08/2023 15:41 WG2089936
4-Chlorophenyl-phenylether U 0.0145 0.416 1 07/08/2023 15:41 WG2089936
Chrysene U 0.00827 0.0416 1 07/08/2023 15:41 WG2089936
Dibenz(a,h)anthracene U 0.0115 0.0416 1 07/08/2023 15:41 WG2089936
1,2-Dichlorobenzene U 0.0123 0.416 1 07/08/2023 15:41 WG2089936
1,3-Dichlorobenzene U 0.0126 0.416 1 07/08/2023 15:41 WG2089936
1,4-Dichlorobenzene U 0.0124 0.416 1 07/08/2023 15:41 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1631472
ST-CS-2
Collected date/time: 06/29/23 10:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0154 0.416 1 07/08/2023 15:41 WG2089936
2,4-Dinitrotoluene U 0.0119 0.416 1 07/08/2023 15:41 WG2089936
2,6-Dinitrotoluene U 0.0136 0.416 1 07/08/2023 15:41 WG2089936
Fluoranthene U 0.00751 0.0416 1 07/08/2023 15:41 WG2089936
Fluorene U 0.00677 0.0416 1 07/08/2023 15:41 WG2089936
Hexachlorobenzene U 0.0147 0.416 1 07/08/2023 15:41 WG2089936
Hexachloro-1,3-butadiene U 0.0140 0.416 1 07/08/2023 15:41 WG2089936
Hexachlorocyclopentadiene U 0.0219 0.416 1 07/08/2023 15:41 WG2089936
Hexachloroethane U 0.0164 0.416 1 07/08/2023 15:41 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0118 0.0416 1 07/08/2023 15:41 WG2089936
Isophorone U 0.0127 0.416 1 07/08/2023 15:41 WG2089936
Naphthalene U 0.0104 0.0416 1 07/08/2023 15:41 WG2089936
Nitrobenzene U 0.0145 0.416 1 07/08/2023 15:41 WG2089936
n-Nitrosodimethylamine U 0.0617 0.416 1 07/08/2023 15:41 WG2089936
n-Nitrosodiphenylamine U 0.0315 0.416 1 07/08/2023 15:41 WG2089936
n-Nitrosodi-n-propylamine U 0.0139 0.416 1 07/08/2023 15:41 WG2089936
Phenanthrene U 0.00826 0.0416 1 07/08/2023 15:41 WG2089936
Benzylbutyl phthalate U 0.0130 0.416 1 07/08/2023 15:41 WG2089936
Bis(2-ethylhexyl)phthalate U 0.0527 0.416 1 07/08/2023 15:41 WG2089936
Di-n-butyl phthalate U 0.0142 0.416 1 07/08/2023 15:41 WG2089936
Diethyl phthalate U 0.0137 0.416 1 07/08/2023 15:41 WG2089936
Dimethyl phthalate U 0.0882 0.416 1 07/08/2023 15:41 WG2089936
Di-n-octyl phthalate U 0.0281 0.416 1 07/08/2023 15:41 WG2089936
Pyrene U 0.00810 0.0416 1 07/08/2023 15:41 WG2089936
1,2,4-Trichlorobenzene U 0.0130 0.416 1 07/08/2023 15:41 WG2089936
4-Chloro-3-methylphenol U 0.0135 0.416 1 07/08/2023 15:41 WG2089936
2-Chlorophenol U 0.0137 0.416 1 07/08/2023 15:41 WG2089936
2,4-Dichlorophenol U 0.0121 0.416 1 07/08/2023 15:41 WG2089936
2,4-Dimethylphenol U 0.0109 0.416 1 07/08/2023 15:41 WG2089936
4,6-Dinitro-2-methylphenol U 0.0944 0.416 1 07/08/2023 15:41 WG2089936
2,4-Dinitrophenol U 0.0974 0.416 1 07/08/2023 15:41 WG2089936
2-Nitrophenol U 0.0149 0.416 1 07/08/2023 15:41 WG2089936
4-Nitrophenol U 0.0130 0.416 1 07/08/2023 15:41 WG2089936
Pentachlorophenol U 0.0112 0.416 1 07/08/2023 15:41 WG2089936
Phenol U 0.0167 0.416 1 07/08/2023 15:41 WG2089936
2,4,6-Trichlorophenol U 0.0134 0.416 1 07/08/2023 15:41 WG2089936
(S) 2-Fluorophenol 52.6 12.0-120 07/08/2023 15:41 WG2089936
(S) Phenol-d5 17.6 10.0-120 07/08/2023 15:41 WG2089936
(S) Nitrobenzene-d5 48.6 10.0-122 07/08/2023 15:41 WG2089936
(S) 2-Fluorobiphenyl 49.5 15.0-120 07/08/2023 15:41 WG2089936
(S) 2,4,6-Tribromophenol 67.1 10.0-127 07/08/2023 15:41 WG2089936
(S) p-Terphenyl-d14 59.0 10.0-120 07/08/2023 15:41 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene 0.00902 0.00287 0.00750 1 07/12/2023 00:56 WG2091376
Acenaphthene U 0.00261 0.00750 1 07/12/2023 00:56 WG2091376
Acenaphthylene U 0.00270 0.00750 1 07/12/2023 00:56 WG2091376
Benzo(a)anthracene 0.0856 0.00216 0.00750 1 07/12/2023 00:56 WG2091376
Benzo(a)pyrene 0.0762 0.00224 0.00750 1 07/12/2023 00:56 WG2091376
Benzo(b)fluoranthene 0.101 0.00191 0.00750 1 07/12/2023 00:56 WG2091376
Benzo(g,h,i)perylene 0.0456 0.00221 0.00750 1 07/12/2023 00:56 WG2091376
Benzo(k)fluoranthene 0.0366 0.00269 0.00750 1 07/12/2023 00:56 WG2091376
Chrysene 0.0739 0.00290 0.00750 1 07/12/2023 00:56 WG2091376
Dibenz(a,h)anthracene 0.0103 0.00215 0.00750 1 07/12/2023 00:56 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1631472
ST-CS-2
Collected date/time: 06/29/23 10:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluoranthene 0.136 0.00284 0.00750 1 07/12/2023 00:56 WG2091376
Fluorene U 0.00256 0.00750 1 07/12/2023 00:56 WG2091376
Indeno(1,2,3-cd)pyrene 0.0536 0.00226 0.00750 1 07/12/2023 00:56 WG2091376
Naphthalene U 0.00510 0.0250 1 07/12/2023 00:56 WG2091376
Phenanthrene 0.0326 0.00289 0.00750 1 07/12/2023 00:56 WG2091376
Pyrene 0.113 0.00250 0.00750 1 07/12/2023 00:56 WG2091376
1-Methylnaphthalene U 0.00561 0.0250 1 07/12/2023 00:56 WG2091376
2-Methylnaphthalene U 0.00534 0.0250 1 07/12/2023 00:56 WG2091376
2-Chloronaphthalene U 0.00582 0.0250 1 07/12/2023 00:56 WG2091376
(S) p-Terphenyl-d14 70.8 23.0-120 07/12/2023 00:56 WG2091376
(S) Nitrobenzene-d5 72.8 14.0-149 07/12/2023 00:56 WG2091376
(S) 2-Fluorobiphenyl 65.3 34.0-125 07/12/2023 00:56 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1631472
ST-CS-3
Collected date/time: 06/29/23 10:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.0 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U 0.881 4.05 25 07/07/2023 20:18 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)96.5 77.0-120 07/07/2023 20:18 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0592 0.0811 1 07/07/2023 01:07 WG2090578
Acrylonitrile U 0.00586 0.0203 1 07/07/2023 01:07 WG2090578
Benzene U 0.000757 0.00162 1 07/07/2023 01:07 WG2090578
Bromobenzene U 0.00146 0.0203 1 07/07/2023 01:07 WG2090578
Bromodichloromethane U 0.00118 0.00405 1 07/07/2023 01:07 WG2090578
Bromoform U 0.00190 0.0405 1 07/07/2023 01:07 WG2090578
Bromomethane U 0.00320 0.0203 1 07/07/2023 01:07 WG2090578
n-Butylbenzene U 0.00852 0.0203 1 07/07/2023 01:07 WG2090578
sec-Butylbenzene U 0.00467 0.0203 1 07/07/2023 01:07 WG2090578
tert-Butylbenzene U 0.00316 0.00811 1 07/07/2023 01:07 WG2090578
Carbon tetrachloride U 0.00146 0.00811 1 07/07/2023 01:07 WG2090578
Chlorobenzene U 0.000341 0.00405 1 07/07/2023 01:07 WG2090578
Chlorodibromomethane U 0.000993 0.00405 1 07/07/2023 01:07 WG2090578
Chloroethane U 0.00276 0.00811 1 07/07/2023 01:07 WG2090578
Chloroform U 0.00167 0.00405 1 07/07/2023 01:07 WG2090578
Chloromethane U 0.00706 0.0203 1 07/07/2023 01:07 WG2090578
2-Chlorotoluene U 0.00140 0.00405 1 07/07/2023 01:07 WG2090578
4-Chlorotoluene U 0.000730 0.00811 1 07/07/2023 01:07 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00633 0.0405 1 07/07/2023 01:07 WG2090578
1,2-Dibromoethane U 0.00105 0.00405 1 07/07/2023 01:07 WG2090578
Dibromomethane U 0.00122 0.00811 1 07/07/2023 01:07 WG2090578
1,2-Dichlorobenzene U 0.000689 0.00811 1 07/07/2023 01:07 WG2090578
1,3-Dichlorobenzene U 0.000973 0.00811 1 07/07/2023 01:07 WG2090578
1,4-Dichlorobenzene U 0.00114 0.00811 1 07/07/2023 01:07 WG2090578
Dichlorodifluoromethane U 0.00261 0.00405 1 07/07/2023 01:07 WG2090578
1,1-Dichloroethane U 0.000796 0.00405 1 07/07/2023 01:07 WG2090578
1,2-Dichloroethane U 0.00105 0.00405 1 07/07/2023 01:07 WG2090578
1,1-Dichloroethene U 0.000983 0.00405 1 07/07/2023 01:07 WG2090578
cis-1,2-Dichloroethene U 0.00119 0.00405 1 07/07/2023 01:07 WG2090578
trans-1,2-Dichloroethene U 0.00169 0.00811 1 07/07/2023 01:07 WG2090578
1,2-Dichloropropane U 0.00230 0.00811 1 07/07/2023 01:07 WG2090578
1,1-Dichloropropene U 0.00131 0.00405 1 07/07/2023 01:07 WG2090578
1,3-Dichloropropane U 0.000813 0.00811 1 07/07/2023 01:07 WG2090578
cis-1,3-Dichloropropene U 0.00123 0.00405 1 07/07/2023 01:07 WG2090578
trans-1,3-Dichloropropene U 0.00185 0.00811 1 07/07/2023 01:07 WG2090578
2,2-Dichloropropane U 0.00224 0.00405 1 07/07/2023 01:07 WG2090578
Di-isopropyl ether U 0.000665 0.00162 1 07/07/2023 01:07 WG2090578
Ethylbenzene U 0.00120 0.00405 1 07/07/2023 01:07 WG2090578
Hexachloro-1,3-butadiene U 0.00973 0.0405 1 07/07/2023 01:07 WG2090578
Isopropylbenzene U 0.000689 0.00405 1 07/07/2023 01:07 WG2090578
p-Isopropyltoluene U 0.00414 0.00811 1 07/07/2023 01:07 WG2090578
2-Butanone (MEK)U 0.103 0.162 1 07/07/2023 01:07 WG2090578
Methylene Chloride U 0.0108 0.0405 1 07/07/2023 01:07 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1631472
ST-CS-3
Collected date/time: 06/29/23 10:55
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) U 0.00370 0.0405 1 07/07/2023 01:07 WG2090578
Methyl tert-butyl ether U 0.000568 0.00162 1 07/07/2023 01:07 WG2090578
Naphthalene U J4 0.00792 0.0203 1 07/07/2023 01:07 WG2090578
n-Propylbenzene U 0.00154 0.00811 1 07/07/2023 01:07 WG2090578
Styrene U 0.000371 0.0203 1 07/07/2023 01:07 WG2090578
1,1,1,2-Tetrachloroethane U 0.00154 0.00405 1 07/07/2023 01:07 WG2090578
1,1,2,2-Tetrachloroethane U 0.00113 0.00405 1 07/07/2023 01:07 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00122 0.00405 1 07/07/2023 01:07 WG2090578
Tetrachloroethene U 0.00145 0.00405 1 07/07/2023 01:07 WG2090578
Toluene 0.106 0.00211 0.00811 1 07/07/2023 01:07 WG2090578
1,2,3-Trichlorobenzene U 0.0119 0.0203 1 07/07/2023 01:07 WG2090578
1,2,4-Trichlorobenzene U 0.00714 0.0203 1 07/07/2023 01:07 WG2090578
1,1,1-Trichloroethane U 0.00150 0.00405 1 07/07/2023 01:07 WG2090578
1,1,2-Trichloroethane U 0.000968 0.00405 1 07/07/2023 01:07 WG2090578
Trichloroethene U 0.000947 0.00162 1 07/07/2023 01:07 WG2090578
Trichlorofluoromethane U 0.00134 0.00405 1 07/07/2023 01:07 WG2090578
1,2,3-Trichloropropane U 0.00263 0.0203 1 07/07/2023 01:07 WG2090578
1,2,4-Trimethylbenzene U 0.00256 0.00811 1 07/07/2023 01:07 WG2090578
1,2,3-Trimethylbenzene U 0.00256 0.00811 1 07/07/2023 01:07 WG2090578
1,3,5-Trimethylbenzene U 0.00324 0.00811 1 07/07/2023 01:07 WG2090578
Vinyl chloride U 0.00188 0.00405 1 07/07/2023 01:07 WG2090578
Xylenes, Total U 0.00143 0.0105 1 07/07/2023 01:07 WG2090578
(S) Toluene-d8 112 75.0-131 07/07/2023 01:07 WG2090578
(S) 4-Bromofluorobenzene 102 67.0-138 07/07/2023 01:07 WG2090578
(S) 1,2-Dichloroethane-d4 84.1 70.0-130 07/07/2023 01:07 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 5.31 0.974 5.07 1 07/11/2023 19:56 WG2091569
(S) o-Terphenyl 60.2 18.0-148 07/11/2023 19:56 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00683 0.0422 1 07/08/2023 18:36 WG2089936
Acenaphthylene U 0.00594 0.0422 1 07/08/2023 18:36 WG2089936
Anthracene U 0.00751 0.0422 1 07/08/2023 18:36 WG2089936
Benzidine U 0.0793 2.12 1 07/08/2023 18:36 WG2089936
Benzo(a)anthracene U 0.00743 0.0422 1 07/08/2023 18:36 WG2089936
Benzo(b)fluoranthene U 0.00787 0.0422 1 07/08/2023 18:36 WG2089936
Benzo(k)fluoranthene U 0.00750 0.0422 1 07/08/2023 18:36 WG2089936
Benzo(g,h,i)perylene U 0.00771 0.0422 1 07/08/2023 18:36 WG2089936
Benzo(a)pyrene U 0.00784 0.0422 1 07/08/2023 18:36 WG2089936
Bis(2-chlorethoxy)methane U 0.0127 0.422 1 07/08/2023 18:36 WG2089936
Bis(2-chloroethyl)ether U 0.0139 0.422 1 07/08/2023 18:36 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0182 0.422 1 07/08/2023 18:36 WG2089936
4-Bromophenyl-phenylether U 0.0148 0.422 1 07/08/2023 18:36 WG2089936
2-Chloronaphthalene U 0.00741 0.0422 1 07/08/2023 18:36 WG2089936
4-Chlorophenyl-phenylether U 0.0147 0.422 1 07/08/2023 18:36 WG2089936
Chrysene U 0.00838 0.0422 1 07/08/2023 18:36 WG2089936
Dibenz(a,h)anthracene U 0.0117 0.0422 1 07/08/2023 18:36 WG2089936
1,2-Dichlorobenzene U 0.0125 0.422 1 07/08/2023 18:36 WG2089936
1,3-Dichlorobenzene U 0.0128 0.422 1 07/08/2023 18:36 WG2089936
1,4-Dichlorobenzene U 0.0126 0.422 1 07/08/2023 18:36 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1631472
ST-CS-3
Collected date/time: 06/29/23 10:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0156 0.422 1 07/08/2023 18:36 WG2089936
2,4-Dinitrotoluene U 0.0121 0.422 1 07/08/2023 18:36 WG2089936
2,6-Dinitrotoluene U 0.0138 0.422 1 07/08/2023 18:36 WG2089936
Fluoranthene U 0.00761 0.0422 1 07/08/2023 18:36 WG2089936
Fluorene U 0.00686 0.0422 1 07/08/2023 18:36 WG2089936
Hexachlorobenzene U 0.0149 0.422 1 07/08/2023 18:36 WG2089936
Hexachloro-1,3-butadiene U 0.0142 0.422 1 07/08/2023 18:36 WG2089936
Hexachlorocyclopentadiene U 0.0222 0.422 1 07/08/2023 18:36 WG2089936
Hexachloroethane U 0.0166 0.422 1 07/08/2023 18:36 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0119 0.0422 1 07/08/2023 18:36 WG2089936
Isophorone U 0.0129 0.422 1 07/08/2023 18:36 WG2089936
Naphthalene U 0.0106 0.0422 1 07/08/2023 18:36 WG2089936
Nitrobenzene U 0.0147 0.422 1 07/08/2023 18:36 WG2089936
n-Nitrosodimethylamine U 0.0626 0.422 1 07/08/2023 18:36 WG2089936
n-Nitrosodiphenylamine U 0.0319 0.422 1 07/08/2023 18:36 WG2089936
n-Nitrosodi-n-propylamine U 0.0141 0.422 1 07/08/2023 18:36 WG2089936
Phenanthrene U 0.00837 0.0422 1 07/08/2023 18:36 WG2089936
Benzylbutyl phthalate U 0.0132 0.422 1 07/08/2023 18:36 WG2089936
Bis(2-ethylhexyl)phthalate U 0.0535 0.422 1 07/08/2023 18:36 WG2089936
Di-n-butyl phthalate U 0.0144 0.422 1 07/08/2023 18:36 WG2089936
Diethyl phthalate U 0.0139 0.422 1 07/08/2023 18:36 WG2089936
Dimethyl phthalate U 0.0894 0.422 1 07/08/2023 18:36 WG2089936
Di-n-octyl phthalate U 0.0285 0.422 1 07/08/2023 18:36 WG2089936
Pyrene U 0.00821 0.0422 1 07/08/2023 18:36 WG2089936
1,2,4-Trichlorobenzene U 0.0132 0.422 1 07/08/2023 18:36 WG2089936
4-Chloro-3-methylphenol U 0.0137 0.422 1 07/08/2023 18:36 WG2089936
2-Chlorophenol U 0.0139 0.422 1 07/08/2023 18:36 WG2089936
2,4-Dichlorophenol U 0.0123 0.422 1 07/08/2023 18:36 WG2089936
2,4-Dimethylphenol U 0.0110 0.422 1 07/08/2023 18:36 WG2089936
4,6-Dinitro-2-methylphenol U 0.0956 0.422 1 07/08/2023 18:36 WG2089936
2,4-Dinitrophenol U 0.0987 0.422 1 07/08/2023 18:36 WG2089936
2-Nitrophenol U 0.0151 0.422 1 07/08/2023 18:36 WG2089936
4-Nitrophenol U 0.0132 0.422 1 07/08/2023 18:36 WG2089936
Pentachlorophenol U 0.0113 0.422 1 07/08/2023 18:36 WG2089936
Phenol U 0.0170 0.422 1 07/08/2023 18:36 WG2089936
2,4,6-Trichlorophenol U 0.0136 0.422 1 07/08/2023 18:36 WG2089936
(S) 2-Fluorophenol 63.8 12.0-120 07/08/2023 18:36 WG2089936
(S) Phenol-d5 55.0 10.0-120 07/08/2023 18:36 WG2089936
(S) Nitrobenzene-d5 57.1 10.0-122 07/08/2023 18:36 WG2089936
(S) 2-Fluorobiphenyl 58.3 15.0-120 07/08/2023 18:36 WG2089936
(S) 2,4,6-Tribromophenol 78.5 10.0-127 07/08/2023 18:36 WG2089936
(S) p-Terphenyl-d14 66.5 10.0-120 07/08/2023 18:36 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U 0.00291 0.00760 1 07/12/2023 01:13 WG2091376
Acenaphthene U 0.00265 0.00760 1 07/12/2023 01:13 WG2091376
Acenaphthylene U 0.00274 0.00760 1 07/12/2023 01:13 WG2091376
Benzo(a)anthracene 0.00621 J 0.00219 0.00760 1 07/12/2023 01:13 WG2091376
Benzo(a)pyrene 0.00922 0.00227 0.00760 1 07/12/2023 01:13 WG2091376
Benzo(b)fluoranthene 0.0138 0.00194 0.00760 1 07/12/2023 01:13 WG2091376
Benzo(g,h,i)perylene 0.00770 0.00224 0.00760 1 07/12/2023 01:13 WG2091376
Benzo(k)fluoranthene 0.00495 J 0.00272 0.00760 1 07/12/2023 01:13 WG2091376
Chrysene 0.00974 0.00294 0.00760 1 07/12/2023 01:13 WG2091376
Dibenz(a,h)anthracene U 0.00218 0.00760 1 07/12/2023 01:13 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1631472
ST-CS-3
Collected date/time: 06/29/23 10:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluoranthene 0.0185 0.00288 0.00760 1 07/12/2023 01:13 WG2091376
Fluorene U 0.00260 0.00760 1 07/12/2023 01:13 WG2091376
Indeno(1,2,3-cd)pyrene 0.00859 0.00229 0.00760 1 07/12/2023 01:13 WG2091376
Naphthalene U 0.00517 0.0253 1 07/12/2023 01:13 WG2091376
Phenanthrene 0.00491 J 0.00293 0.00760 1 07/12/2023 01:13 WG2091376
Pyrene 0.0146 0.00253 0.00760 1 07/12/2023 01:13 WG2091376
1-Methylnaphthalene U 0.00569 0.0253 1 07/12/2023 01:13 WG2091376
2-Methylnaphthalene U 0.00541 0.0253 1 07/12/2023 01:13 WG2091376
2-Chloronaphthalene U 0.00590 0.0253 1 07/12/2023 01:13 WG2091376
(S) p-Terphenyl-d14 81.4 23.0-120 07/12/2023 01:13 WG2091376
(S) Nitrobenzene-d5 87.5 14.0-149 07/12/2023 01:13 WG2091376
(S) 2-Fluorobiphenyl 73.8 34.0-125 07/12/2023 01:13 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1631472
ST-CS-4
Collected date/time: 06/29/23 11:03
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.0 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.50 B J 0.825 3.80 25 07/13/2023 11:26 WG2093889
(S)
a,a,a-Trifluorotoluene(FID)93.9 77.0-120 07/13/2023 11:26 WG2093889
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0635 0.0870 1.22 07/08/2023 12:59 WG2091079
Acrylonitrile U 0.00628 0.0218 1.22 07/08/2023 12:59 WG2091079
Benzene U 0.000813 0.00174 1.22 07/08/2023 12:59 WG2091079
Bromobenzene U 0.00157 0.0218 1.22 07/08/2023 12:59 WG2091079
Bromodichloromethane U 0.00126 0.00435 1.22 07/08/2023 12:59 WG2091079
Bromoform U 0.00204 0.0435 1.22 07/08/2023 12:59 WG2091079
Bromomethane U 0.00342 0.0218 1.22 07/08/2023 12:59 WG2091079
n-Butylbenzene U 0.00913 0.0218 1.22 07/08/2023 12:59 WG2091079
sec-Butylbenzene U 0.00501 0.0218 1.22 07/08/2023 12:59 WG2091079
tert-Butylbenzene U 0.00340 0.00870 1.22 07/08/2023 12:59 WG2091079
Carbon tetrachloride U 0.00157 0.00870 1.22 07/08/2023 12:59 WG2091079
Chlorobenzene U 0.000365 0.00435 1.22 07/08/2023 12:59 WG2091079
Chlorodibromomethane U 0.00107 0.00435 1.22 07/08/2023 12:59 WG2091079
Chloroethane U 0.00295 0.00870 1.22 07/08/2023 12:59 WG2091079
Chloroform U 0.00180 0.00435 1.22 07/08/2023 12:59 WG2091079
Chloromethane U 0.00758 0.0218 1.22 07/08/2023 12:59 WG2091079
2-Chlorotoluene U 0.00151 0.00435 1.22 07/08/2023 12:59 WG2091079
4-Chlorotoluene U 0.000783 0.00870 1.22 07/08/2023 12:59 WG2091079
1,2-Dibromo-3-Chloropropane U 0.00679 0.0435 1.22 07/08/2023 12:59 WG2091079
1,2-Dibromoethane U 0.00113 0.00435 1.22 07/08/2023 12:59 WG2091079
Dibromomethane U 0.00131 0.00870 1.22 07/08/2023 12:59 WG2091079
1,2-Dichlorobenzene U 0.000740 0.00870 1.22 07/08/2023 12:59 WG2091079
1,3-Dichlorobenzene U 0.00104 0.00870 1.22 07/08/2023 12:59 WG2091079
1,4-Dichlorobenzene U 0.00122 0.00870 1.22 07/08/2023 12:59 WG2091079
Dichlorodifluoromethane U 0.00280 0.00435 1.22 07/08/2023 12:59 WG2091079
1,1-Dichloroethane U 0.000855 0.00435 1.22 07/08/2023 12:59 WG2091079
1,2-Dichloroethane U 0.00113 0.00435 1.22 07/08/2023 12:59 WG2091079
1,1-Dichloroethene U 0.00105 0.00435 1.22 07/08/2023 12:59 WG2091079
cis-1,2-Dichloroethene U 0.00128 0.00435 1.22 07/08/2023 12:59 WG2091079
trans-1,2-Dichloroethene U 0.00181 0.00870 1.22 07/08/2023 12:59 WG2091079
1,2-Dichloropropane U 0.00247 0.00870 1.22 07/08/2023 12:59 WG2091079
1,1-Dichloropropene U 0.00141 0.00435 1.22 07/08/2023 12:59 WG2091079
1,3-Dichloropropane U 0.000872 0.00870 1.22 07/08/2023 12:59 WG2091079
cis-1,3-Dichloropropene U 0.00132 0.00435 1.22 07/08/2023 12:59 WG2091079
trans-1,3-Dichloropropene U 0.00198 0.00870 1.22 07/08/2023 12:59 WG2091079
2,2-Dichloropropane U 0.00240 0.00435 1.22 07/08/2023 12:59 WG2091079
Di-isopropyl ether U 0.000713 0.00174 1.22 07/08/2023 12:59 WG2091079
Ethylbenzene 0.00204 J 0.00128 0.00435 1.22 07/08/2023 12:59 WG2091079
Hexachloro-1,3-butadiene U 0.0104 0.0435 1.22 07/08/2023 12:59 WG2091079
Isopropylbenzene U 0.000740 0.00435 1.22 07/08/2023 12:59 WG2091079
p-Isopropyltoluene U 0.00444 0.00870 1.22 07/08/2023 12:59 WG2091079
2-Butanone (MEK)U 0.111 0.174 1.22 07/08/2023 12:59 WG2091079
Methylene Chloride 0.0133 J 0.0116 0.0435 1.22 07/08/2023 12:59 WG2091079
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1631472
ST-CS-4
Collected date/time: 06/29/23 11:03
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) 0.00448 J 0.00397 0.0435 1.22 07/08/2023 12:59 WG2091079
Methyl tert-butyl ether U 0.000609 0.00174 1.22 07/08/2023 12:59 WG2091079
Naphthalene U 0.00849 0.0218 1.22 07/08/2023 12:59 WG2091079
n-Propylbenzene U 0.00165 0.00870 1.22 07/08/2023 12:59 WG2091079
Styrene U 0.000398 0.0218 1.22 07/08/2023 12:59 WG2091079
1,1,1,2-Tetrachloroethane U 0.00165 0.00435 1.22 07/08/2023 12:59 WG2091079
1,1,2,2-Tetrachloroethane U 0.00121 0.00435 1.22 07/08/2023 12:59 WG2091079
1,1,2-Trichlorotrifluoroethane U 0.00131 0.00435 1.22 07/08/2023 12:59 WG2091079
Tetrachloroethene U 0.00156 0.00435 1.22 07/08/2023 12:59 WG2091079
Toluene 0.0167 0.00227 0.00870 1.22 07/08/2023 12:59 WG2091079
1,2,3-Trichlorobenzene U 0.0128 0.0218 1.22 07/08/2023 12:59 WG2091079
1,2,4-Trichlorobenzene U 0.00766 0.0218 1.22 07/08/2023 12:59 WG2091079
1,1,1-Trichloroethane U 0.00161 0.00435 1.22 07/08/2023 12:59 WG2091079
1,1,2-Trichloroethane U 0.00104 0.00435 1.22 07/08/2023 12:59 WG2091079
Trichloroethene U 0.00102 0.00174 1.22 07/08/2023 12:59 WG2091079
Trichlorofluoromethane U 0.00144 0.00435 1.22 07/08/2023 12:59 WG2091079
1,2,3-Trichloropropane U 0.00282 0.0218 1.22 07/08/2023 12:59 WG2091079
1,2,4-Trimethylbenzene U 0.00275 0.00870 1.22 07/08/2023 12:59 WG2091079
1,2,3-Trimethylbenzene U 0.00275 0.00870 1.22 07/08/2023 12:59 WG2091079
1,3,5-Trimethylbenzene U 0.00348 0.00870 1.22 07/08/2023 12:59 WG2091079
Vinyl chloride U 0.00203 0.00435 1.22 07/08/2023 12:59 WG2091079
Xylenes, Total 0.0102 J 0.00153 0.0113 1.22 07/08/2023 12:59 WG2091079
(S) Toluene-d8 104 75.0-131 07/08/2023 12:59 WG2091079
(S) 4-Bromofluorobenzene 95.6 67.0-138 07/08/2023 12:59 WG2091079
(S) 1,2-Dichloroethane-d4 94.5 70.0-130 07/08/2023 12:59 WG2091079
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 51.9 J J5 19.0 98.8 20 07/12/2023 03:35 WG2091569
(S) o-Terphenyl 92.7 J7 18.0-148 07/12/2023 03:35 WG2091569
Sample Narrative:
L1631472-04 WG2091569: Cannot run at lower dilution due to viscosity of extract
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.0133 0.0822 2 07/10/2023 20:12 WG2089936
Acenaphthylene U 0.0116 0.0822 2 07/10/2023 20:12 WG2089936
Anthracene U 0.0147 0.0822 2 07/10/2023 20:12 WG2089936
Benzidine U J3 J6 0.154 4.12 2 07/10/2023 20:12 WG2089936
Benzo(a)anthracene U 0.0144 0.0822 2 07/10/2023 20:12 WG2089936
Benzo(b)fluoranthene U 0.0153 0.0822 2 07/10/2023 20:12 WG2089936
Benzo(k)fluoranthene U 0.0146 0.0822 2 07/10/2023 20:12 WG2089936
Benzo(g,h,i)perylene U 0.0151 0.0822 2 07/10/2023 20:12 WG2089936
Benzo(a)pyrene U 0.0153 0.0822 2 07/10/2023 20:12 WG2089936
Bis(2-chlorethoxy)methane U 0.0247 0.822 2 07/10/2023 20:12 WG2089936
Bis(2-chloroethyl)ether U 0.0272 0.822 2 07/10/2023 20:12 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0356 0.822 2 07/10/2023 20:12 WG2089936
4-Bromophenyl-phenylether U 0.0289 0.822 2 07/10/2023 20:12 WG2089936
2-Chloronaphthalene U 0.0144 0.0822 2 07/10/2023 20:12 WG2089936
4-Chlorophenyl-phenylether U 0.0286 0.822 2 07/10/2023 20:12 WG2089936
Chrysene U 0.0163 0.0822 2 07/10/2023 20:12 WG2089936
Dibenz(a,h)anthracene U 0.0228 0.0822 2 07/10/2023 20:12 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1631472
ST-CS-4
Collected date/time: 06/29/23 11:03
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichlorobenzene U 0.0243 0.822 2 07/10/2023 20:12 WG2089936
1,3-Dichlorobenzene U 0.0249 0.822 2 07/10/2023 20:12 WG2089936
1,4-Dichlorobenzene U 0.0244 0.822 2 07/10/2023 20:12 WG2089936
3,3-Dichlorobenzidine U J3 0.0304 0.822 2 07/10/2023 20:12 WG2089936
2,4-Dinitrotoluene U 0.0236 0.822 2 07/10/2023 20:12 WG2089936
2,6-Dinitrotoluene U 0.0269 0.822 2 07/10/2023 20:12 WG2089936
Fluoranthene U 0.0148 0.0822 2 07/10/2023 20:12 WG2089936
Fluorene U 0.0133 0.0822 2 07/10/2023 20:12 WG2089936
Hexachlorobenzene U 0.0291 0.822 2 07/10/2023 20:12 WG2089936
Hexachloro-1,3-butadiene U 0.0277 0.822 2 07/10/2023 20:12 WG2089936
Hexachlorocyclopentadiene U J6 0.0432 0.822 2 07/10/2023 20:12 WG2089936
Hexachloroethane U 0.0323 0.822 2 07/10/2023 20:12 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0232 0.0822 2 07/10/2023 20:12 WG2089936
Isophorone U 0.0252 0.822 2 07/10/2023 20:12 WG2089936
Naphthalene U 0.0206 0.0822 2 07/10/2023 20:12 WG2089936
Nitrobenzene U 0.0286 0.822 2 07/10/2023 20:12 WG2089936
n-Nitrosodimethylamine U 0.122 0.822 2 07/10/2023 20:12 WG2089936
n-Nitrosodiphenylamine U 0.0622 0.822 2 07/10/2023 20:12 WG2089936
n-Nitrosodi-n-propylamine U 0.0274 0.822 2 07/10/2023 20:12 WG2089936
Phenanthrene U 0.0163 0.0822 2 07/10/2023 20:12 WG2089936
Benzylbutyl phthalate U 0.0257 0.822 2 07/10/2023 20:12 WG2089936
Bis(2-ethylhexyl)phthalate U 0.104 0.822 2 07/10/2023 20:12 WG2089936
Di-n-butyl phthalate U 0.0282 0.822 2 07/10/2023 20:12 WG2089936
Diethyl phthalate U 0.0272 0.822 2 07/10/2023 20:12 WG2089936
Dimethyl phthalate U 0.174 0.822 2 07/10/2023 20:12 WG2089936
Di-n-octyl phthalate U 0.0556 0.822 2 07/10/2023 20:12 WG2089936
Pyrene U 0.0161 0.0822 2 07/10/2023 20:12 WG2089936
1,2,4-Trichlorobenzene U 0.0257 0.822 2 07/10/2023 20:12 WG2089936
4-Chloro-3-methylphenol U 0.0267 0.822 2 07/10/2023 20:12 WG2089936
2-Chlorophenol U 0.0272 0.822 2 07/10/2023 20:12 WG2089936
2,4-Dichlorophenol U 0.0240 0.822 2 07/10/2023 20:12 WG2089936
2,4-Dimethylphenol U 0.0215 0.822 2 07/10/2023 20:12 WG2089936
4,6-Dinitro-2-methylphenol U 0.186 0.822 2 07/10/2023 20:12 WG2089936
2,4-Dinitrophenol U J6 0.193 0.822 2 07/10/2023 20:12 WG2089936
2-Nitrophenol U 0.0294 0.822 2 07/10/2023 20:12 WG2089936
4-Nitrophenol U 0.0257 0.822 2 07/10/2023 20:12 WG2089936
Pentachlorophenol U 0.0221 0.822 2 07/10/2023 20:12 WG2089936
Phenol U 0.0331 0.822 2 07/10/2023 20:12 WG2089936
2,4,6-Trichlorophenol U 0.0264 0.822 2 07/10/2023 20:12 WG2089936
(S) 2-Fluorophenol 56.0 12.0-120 07/10/2023 20:12 WG2089936
(S) Phenol-d5 51.3 10.0-120 07/10/2023 20:12 WG2089936
(S) Nitrobenzene-d5 51.5 10.0-122 07/10/2023 20:12 WG2089936
(S) 2-Fluorobiphenyl 54.8 15.0-120 07/10/2023 20:12 WG2089936
(S) 2,4,6-Tribromophenol 81.5 10.0-127 07/10/2023 20:12 WG2089936
(S) p-Terphenyl-d14 75.8 10.0-120 07/10/2023 20:12 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U J3 0.00284 0.00741 1 07/11/2023 06:00 WG2091375
Acenaphthene U J3 0.00258 0.00741 1 07/11/2023 06:00 WG2091375
Acenaphthylene U J3 0.00267 0.00741 1 07/11/2023 06:00 WG2091375
Benzo(a)anthracene 0.00420 J J3 0.00214 0.00741 1 07/11/2023 06:00 WG2091375
Benzo(a)pyrene 0.00904 J3 0.00221 0.00741 1 07/11/2023 06:00 WG2091375
Benzo(b)fluoranthene 0.0172 0.00189 0.00741 1 07/11/2023 06:00 WG2091375
Benzo(g,h,i)perylene 0.0352 J3 0.00219 0.00741 1 07/11/2023 06:00 WG2091375
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 04
L1631472
ST-CS-4
Collected date/time: 06/29/23 11:03
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Benzo(k)fluoranthene U J3 0.00265 0.00741 1 07/11/2023 06:00 WG2091375
Chrysene 0.0117 J3 0.00286 0.00741 1 07/11/2023 06:00 WG2091375
Dibenz(a,h)anthracene 0.0117 J3 0.00212 0.00741 1 07/11/2023 06:00 WG2091375
Fluoranthene 0.00578 J J3 0.00280 0.00741 1 07/11/2023 06:00 WG2091375
Fluorene U J3 0.00253 0.00741 1 07/11/2023 06:00 WG2091375
Indeno(1,2,3-cd)pyrene 0.00803 J3 0.00223 0.00741 1 07/11/2023 06:00 WG2091375
Naphthalene U J3 0.00504 0.0247 1 07/11/2023 06:00 WG2091375
Phenanthrene 0.00431 J J3 0.00285 0.00741 1 07/11/2023 06:00 WG2091375
Pyrene 0.00922 J3 0.00247 0.00741 1 07/11/2023 06:00 WG2091375
1-Methylnaphthalene U J3 0.00554 0.0247 1 07/11/2023 06:00 WG2091375
2-Methylnaphthalene U J3 0.00527 0.0247 1 07/11/2023 06:00 WG2091375
2-Chloronaphthalene U J3 0.00575 0.0247 1 07/11/2023 06:00 WG2091375
(S) p-Terphenyl-d14 63.9 23.0-120 07/11/2023 06:00 WG2091375
(S) Nitrobenzene-d5 117 14.0-149 07/11/2023 06:00 WG2091375
(S) 2-Fluorobiphenyl 63.3 34.0-125 07/11/2023 06:00 WG2091375
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1631472
ST-CS-DUPE
Collected date/time: 06/29/23 11:03
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.1 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U 0.826 3.81 25.5 07/07/2023 20:41 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)95.8 77.0-120 07/07/2023 20:41 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0556 0.0762 1.02 07/07/2023 01:27 WG2090578
Acrylonitrile U 0.00550 0.0191 1.02 07/07/2023 01:27 WG2090578
Benzene U 0.000711 0.00152 1.02 07/07/2023 01:27 WG2090578
Bromobenzene U 0.00137 0.0191 1.02 07/07/2023 01:27 WG2090578
Bromodichloromethane U 0.00110 0.00381 1.02 07/07/2023 01:27 WG2090578
Bromoform U 0.00178 0.0381 1.02 07/07/2023 01:27 WG2090578
Bromomethane U 0.00300 0.0191 1.02 07/07/2023 01:27 WG2090578
n-Butylbenzene U 0.00799 0.0191 1.02 07/07/2023 01:27 WG2090578
sec-Butylbenzene U 0.00439 0.0191 1.02 07/07/2023 01:27 WG2090578
tert-Butylbenzene U 0.00297 0.00762 1.02 07/07/2023 01:27 WG2090578
Carbon tetrachloride U 0.00137 0.00762 1.02 07/07/2023 01:27 WG2090578
Chlorobenzene U 0.000320 0.00381 1.02 07/07/2023 01:27 WG2090578
Chlorodibromomethane U 0.000932 0.00381 1.02 07/07/2023 01:27 WG2090578
Chloroethane U 0.00258 0.00762 1.02 07/07/2023 01:27 WG2090578
Chloroform U 0.00157 0.00381 1.02 07/07/2023 01:27 WG2090578
Chloromethane U 0.00663 0.0191 1.02 07/07/2023 01:27 WG2090578
2-Chlorotoluene U 0.00132 0.00381 1.02 07/07/2023 01:27 WG2090578
4-Chlorotoluene U 0.000686 0.00762 1.02 07/07/2023 01:27 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00594 0.0381 1.02 07/07/2023 01:27 WG2090578
1,2-Dibromoethane U 0.000987 0.00381 1.02 07/07/2023 01:27 WG2090578
Dibromomethane U 0.00114 0.00762 1.02 07/07/2023 01:27 WG2090578
1,2-Dichlorobenzene U 0.000647 0.00762 1.02 07/07/2023 01:27 WG2090578
1,3-Dichlorobenzene U 0.000914 0.00762 1.02 07/07/2023 01:27 WG2090578
1,4-Dichlorobenzene U 0.00107 0.00762 1.02 07/07/2023 01:27 WG2090578
Dichlorodifluoromethane U 0.00245 0.00381 1.02 07/07/2023 01:27 WG2090578
1,1-Dichloroethane U 0.000748 0.00381 1.02 07/07/2023 01:27 WG2090578
1,2-Dichloroethane U 0.000989 0.00381 1.02 07/07/2023 01:27 WG2090578
1,1-Dichloroethene U 0.000923 0.00381 1.02 07/07/2023 01:27 WG2090578
cis-1,2-Dichloroethene U 0.00112 0.00381 1.02 07/07/2023 01:27 WG2090578
trans-1,2-Dichloroethene U 0.00158 0.00762 1.02 07/07/2023 01:27 WG2090578
1,2-Dichloropropane U 0.00217 0.00762 1.02 07/07/2023 01:27 WG2090578
1,1-Dichloropropene U 0.00123 0.00381 1.02 07/07/2023 01:27 WG2090578
1,3-Dichloropropane U 0.000763 0.00762 1.02 07/07/2023 01:27 WG2090578
cis-1,3-Dichloropropene U 0.00115 0.00381 1.02 07/07/2023 01:27 WG2090578
trans-1,3-Dichloropropene U 0.00173 0.00762 1.02 07/07/2023 01:27 WG2090578
2,2-Dichloropropane U 0.00211 0.00381 1.02 07/07/2023 01:27 WG2090578
Di-isopropyl ether U 0.000624 0.00152 1.02 07/07/2023 01:27 WG2090578
Ethylbenzene U 0.00112 0.00381 1.02 07/07/2023 01:27 WG2090578
Hexachloro-1,3-butadiene U 0.00914 0.0381 1.02 07/07/2023 01:27 WG2090578
Isopropylbenzene U 0.000647 0.00381 1.02 07/07/2023 01:27 WG2090578
p-Isopropyltoluene U 0.00388 0.00762 1.02 07/07/2023 01:27 WG2090578
2-Butanone (MEK)U 0.0968 0.152 1.02 07/07/2023 01:27 WG2090578
Methylene Chloride U 0.0101 0.0381 1.02 07/07/2023 01:27 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1631472
ST-CS-DUPE
Collected date/time: 06/29/23 11:03
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) U 0.00348 0.0381 1.02 07/07/2023 01:27 WG2090578
Methyl tert-butyl ether U 0.000533 0.00152 1.02 07/07/2023 01:27 WG2090578
Naphthalene U J4 0.00744 0.0191 1.02 07/07/2023 01:27 WG2090578
n-Propylbenzene U 0.00145 0.00762 1.02 07/07/2023 01:27 WG2090578
Styrene 0.000877 J 0.000349 0.0191 1.02 07/07/2023 01:27 WG2090578
1,1,1,2-Tetrachloroethane U 0.00144 0.00381 1.02 07/07/2023 01:27 WG2090578
1,1,2,2-Tetrachloroethane U 0.00106 0.00381 1.02 07/07/2023 01:27 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00115 0.00381 1.02 07/07/2023 01:27 WG2090578
Tetrachloroethene U 0.00137 0.00381 1.02 07/07/2023 01:27 WG2090578
Toluene U 0.00199 0.00762 1.02 07/07/2023 01:27 WG2090578
1,2,3-Trichlorobenzene U 0.0112 0.0191 1.02 07/07/2023 01:27 WG2090578
1,2,4-Trichlorobenzene U 0.00671 0.0191 1.02 07/07/2023 01:27 WG2090578
1,1,1-Trichloroethane U 0.00141 0.00381 1.02 07/07/2023 01:27 WG2090578
1,1,2-Trichloroethane U 0.000910 0.00381 1.02 07/07/2023 01:27 WG2090578
Trichloroethene U 0.000890 0.00152 1.02 07/07/2023 01:27 WG2090578
Trichlorofluoromethane U 0.00126 0.00381 1.02 07/07/2023 01:27 WG2090578
1,2,3-Trichloropropane U 0.00246 0.0191 1.02 07/07/2023 01:27 WG2090578
1,2,4-Trimethylbenzene U 0.00240 0.00762 1.02 07/07/2023 01:27 WG2090578
1,2,3-Trimethylbenzene U 0.00240 0.00762 1.02 07/07/2023 01:27 WG2090578
1,3,5-Trimethylbenzene U 0.00305 0.00762 1.02 07/07/2023 01:27 WG2090578
Vinyl chloride U 0.00176 0.00381 1.02 07/07/2023 01:27 WG2090578
Xylenes, Total 0.00233 J 0.00134 0.00990 1.02 07/07/2023 01:27 WG2090578
(S) Toluene-d8 112 75.0-131 07/07/2023 01:27 WG2090578
(S) 4-Bromofluorobenzene 110 67.0-138 07/07/2023 01:27 WG2090578
(S) 1,2-Dichloroethane-d4 92.9 70.0-130 07/07/2023 01:27 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 9.47 0.960 5.00 1 07/11/2023 11:02 WG2091569
(S) o-Terphenyl 61.2 18.0-148 07/11/2023 11:02 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00673 0.0416 1 07/10/2023 19:28 WG2089936
Acenaphthylene U 0.00586 0.0416 1 07/10/2023 19:28 WG2089936
Anthracene U 0.00741 0.0416 1 07/10/2023 19:28 WG2089936
Benzidine U 0.0782 2.09 1 07/10/2023 19:28 WG2089936
Benzo(a)anthracene U 0.00733 0.0416 1 07/10/2023 19:28 WG2089936
Benzo(b)fluoranthene U 0.00776 0.0416 1 07/10/2023 19:28 WG2089936
Benzo(k)fluoranthene U 0.00739 0.0416 1 07/10/2023 19:28 WG2089936
Benzo(g,h,i)perylene U 0.00761 0.0416 1 07/10/2023 19:28 WG2089936
Benzo(a)pyrene U 0.00773 0.0416 1 07/10/2023 19:28 WG2089936
Bis(2-chlorethoxy)methane U 0.0125 0.416 1 07/10/2023 19:28 WG2089936
Bis(2-chloroethyl)ether U 0.0137 0.416 1 07/10/2023 19:28 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0180 0.416 1 07/10/2023 19:28 WG2089936
4-Bromophenyl-phenylether U 0.0146 0.416 1 07/10/2023 19:28 WG2089936
2-Chloronaphthalene U 0.00731 0.0416 1 07/10/2023 19:28 WG2089936
4-Chlorophenyl-phenylether U 0.0145 0.416 1 07/10/2023 19:28 WG2089936
Chrysene U 0.00827 0.0416 1 07/10/2023 19:28 WG2089936
Dibenz(a,h)anthracene U 0.0115 0.0416 1 07/10/2023 19:28 WG2089936
1,2-Dichlorobenzene U 0.0123 0.416 1 07/10/2023 19:28 WG2089936
1,3-Dichlorobenzene U 0.0126 0.416 1 07/10/2023 19:28 WG2089936
1,4-Dichlorobenzene U 0.0124 0.416 1 07/10/2023 19:28 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1631472
ST-CS-DUPE
Collected date/time: 06/29/23 11:03
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0154 0.416 1 07/10/2023 19:28 WG2089936
2,4-Dinitrotoluene U 0.0119 0.416 1 07/10/2023 19:28 WG2089936
2,6-Dinitrotoluene U 0.0136 0.416 1 07/10/2023 19:28 WG2089936
Fluoranthene U 0.00751 0.0416 1 07/10/2023 19:28 WG2089936
Fluorene U 0.00677 0.0416 1 07/10/2023 19:28 WG2089936
Hexachlorobenzene U 0.0147 0.416 1 07/10/2023 19:28 WG2089936
Hexachloro-1,3-butadiene U 0.0140 0.416 1 07/10/2023 19:28 WG2089936
Hexachlorocyclopentadiene U 0.0219 0.416 1 07/10/2023 19:28 WG2089936
Hexachloroethane U 0.0164 0.416 1 07/10/2023 19:28 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0118 0.0416 1 07/10/2023 19:28 WG2089936
Isophorone U 0.0127 0.416 1 07/10/2023 19:28 WG2089936
Naphthalene U 0.0104 0.0416 1 07/10/2023 19:28 WG2089936
Nitrobenzene U 0.0145 0.416 1 07/10/2023 19:28 WG2089936
n-Nitrosodimethylamine U 0.0617 0.416 1 07/10/2023 19:28 WG2089936
n-Nitrosodiphenylamine U 0.0315 0.416 1 07/10/2023 19:28 WG2089936
n-Nitrosodi-n-propylamine U 0.0139 0.416 1 07/10/2023 19:28 WG2089936
Phenanthrene U 0.00826 0.0416 1 07/10/2023 19:28 WG2089936
Benzylbutyl phthalate U 0.0130 0.416 1 07/10/2023 19:28 WG2089936
Bis(2-ethylhexyl)phthalate U 0.0527 0.416 1 07/10/2023 19:28 WG2089936
Di-n-butyl phthalate U 0.0142 0.416 1 07/10/2023 19:28 WG2089936
Diethyl phthalate U 0.0137 0.416 1 07/10/2023 19:28 WG2089936
Dimethyl phthalate U 0.0882 0.416 1 07/10/2023 19:28 WG2089936
Di-n-octyl phthalate U 0.0281 0.416 1 07/10/2023 19:28 WG2089936
Pyrene U 0.00809 0.0416 1 07/10/2023 19:28 WG2089936
1,2,4-Trichlorobenzene U 0.0130 0.416 1 07/10/2023 19:28 WG2089936
4-Chloro-3-methylphenol U 0.0135 0.416 1 07/10/2023 19:28 WG2089936
2-Chlorophenol U 0.0137 0.416 1 07/10/2023 19:28 WG2089936
2,4-Dichlorophenol U 0.0121 0.416 1 07/10/2023 19:28 WG2089936
2,4-Dimethylphenol U 0.0109 0.416 1 07/10/2023 19:28 WG2089936
4,6-Dinitro-2-methylphenol U 0.0943 0.416 1 07/10/2023 19:28 WG2089936
2,4-Dinitrophenol U 0.0973 0.416 1 07/10/2023 19:28 WG2089936
2-Nitrophenol U 0.0149 0.416 1 07/10/2023 19:28 WG2089936
4-Nitrophenol U 0.0130 0.416 1 07/10/2023 19:28 WG2089936
Pentachlorophenol U 0.0112 0.416 1 07/10/2023 19:28 WG2089936
Phenol U 0.0167 0.416 1 07/10/2023 19:28 WG2089936
2,4,6-Trichlorophenol U 0.0134 0.416 1 07/10/2023 19:28 WG2089936
(S) 2-Fluorophenol 43.1 12.0-120 07/10/2023 19:28 WG2089936
(S) Phenol-d5 38.6 10.0-120 07/10/2023 19:28 WG2089936
(S) Nitrobenzene-d5 38.4 10.0-122 07/10/2023 19:28 WG2089936
(S) 2-Fluorobiphenyl 44.5 15.0-120 07/10/2023 19:28 WG2089936
(S) 2,4,6-Tribromophenol 64.9 10.0-127 07/10/2023 19:28 WG2089936
(S) p-Terphenyl-d14 60.7 10.0-120 07/10/2023 19:28 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U 0.00287 0.00749 1 07/12/2023 01:32 WG2091376
Acenaphthene U 0.00261 0.00749 1 07/12/2023 01:32 WG2091376
Acenaphthylene U 0.00270 0.00749 1 07/12/2023 01:32 WG2091376
Benzo(a)anthracene 0.0181 0.00216 0.00749 1 07/12/2023 01:32 WG2091376
Benzo(a)pyrene 0.0244 0.00224 0.00749 1 07/12/2023 01:32 WG2091376
Benzo(b)fluoranthene 0.0366 0.00191 0.00749 1 07/12/2023 01:32 WG2091376
Benzo(g,h,i)perylene 0.0202 0.00221 0.00749 1 07/12/2023 01:32 WG2091376
Benzo(k)fluoranthene 0.0121 0.00269 0.00749 1 07/12/2023 01:32 WG2091376
Chrysene 0.0264 0.00290 0.00749 1 07/12/2023 01:32 WG2091376
Dibenz(a,h)anthracene U 0.00215 0.00749 1 07/12/2023 01:32 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 05
L1631472
ST-CS-DUPE
Collected date/time: 06/29/23 11:03
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluoranthene 0.0478 0.00284 0.00749 1 07/12/2023 01:32 WG2091376
Fluorene U 0.00256 0.00749 1 07/12/2023 01:32 WG2091376
Indeno(1,2,3-cd)pyrene 0.0227 0.00226 0.00749 1 07/12/2023 01:32 WG2091376
Naphthalene U 0.00510 0.0250 1 07/12/2023 01:32 WG2091376
Phenanthrene 0.0123 0.00289 0.00749 1 07/12/2023 01:32 WG2091376
Pyrene 0.0371 0.00250 0.00749 1 07/12/2023 01:32 WG2091376
1-Methylnaphthalene U 0.00561 0.0250 1 07/12/2023 01:32 WG2091376
2-Methylnaphthalene U 0.00533 0.0250 1 07/12/2023 01:32 WG2091376
2-Chloronaphthalene U 0.00582 0.0250 1 07/12/2023 01:32 WG2091376
(S) p-Terphenyl-d14 84.5 23.0-120 07/12/2023 01:32 WG2091376
(S) Nitrobenzene-d5 79.9 14.0-149 07/12/2023 01:32 WG2091376
(S) 2-Fluorobiphenyl 71.7 34.0-125 07/12/2023 01:32 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1631472
ST-CS-5
Collected date/time: 06/29/23 11:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.0 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.88 B J 0.744 3.43 25 07/12/2023 21:18 WG2093590
(S)
a,a,a-Trifluorotoluene(FID)96.4 77.0-120 07/12/2023 21:18 WG2093590
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0500 0.0685 1 07/08/2023 12:41 WG2091079
Acrylonitrile U 0.00495 0.0171 1 07/08/2023 12:41 WG2091079
Benzene U 0.000640 0.00137 1 07/08/2023 12:41 WG2091079
Bromobenzene U 0.00123 0.0171 1 07/08/2023 12:41 WG2091079
Bromodichloromethane U 0.000994 0.00343 1 07/08/2023 12:41 WG2091079
Bromoform U 0.00160 0.0343 1 07/08/2023 12:41 WG2091079
Bromomethane U 0.00270 0.0171 1 07/08/2023 12:41 WG2091079
n-Butylbenzene U 0.00720 0.0171 1 07/08/2023 12:41 WG2091079
sec-Butylbenzene U 0.00395 0.0171 1 07/08/2023 12:41 WG2091079
tert-Butylbenzene U 0.00267 0.00685 1 07/08/2023 12:41 WG2091079
Carbon tetrachloride U 0.00123 0.00685 1 07/08/2023 12:41 WG2091079
Chlorobenzene U 0.000288 0.00343 1 07/08/2023 12:41 WG2091079
Chlorodibromomethane U 0.000839 0.00343 1 07/08/2023 12:41 WG2091079
Chloroethane U 0.00233 0.00685 1 07/08/2023 12:41 WG2091079
Chloroform U 0.00141 0.00343 1 07/08/2023 12:41 WG2091079
Chloromethane U 0.00596 0.0171 1 07/08/2023 12:41 WG2091079
2-Chlorotoluene U 0.00119 0.00343 1 07/08/2023 12:41 WG2091079
4-Chlorotoluene U 0.000617 0.00685 1 07/08/2023 12:41 WG2091079
1,2-Dibromo-3-Chloropropane U 0.00535 0.0343 1 07/08/2023 12:41 WG2091079
1,2-Dibromoethane U 0.000888 0.00343 1 07/08/2023 12:41 WG2091079
Dibromomethane U 0.00103 0.00685 1 07/08/2023 12:41 WG2091079
1,2-Dichlorobenzene U 0.000583 0.00685 1 07/08/2023 12:41 WG2091079
1,3-Dichlorobenzene U 0.000822 0.00685 1 07/08/2023 12:41 WG2091079
1,4-Dichlorobenzene U 0.000959 0.00685 1 07/08/2023 12:41 WG2091079
Dichlorodifluoromethane U 0.00221 0.00343 1 07/08/2023 12:41 WG2091079
1,1-Dichloroethane U 0.000673 0.00343 1 07/08/2023 12:41 WG2091079
1,2-Dichloroethane U 0.000890 0.00343 1 07/08/2023 12:41 WG2091079
1,1-Dichloroethene U 0.000831 0.00343 1 07/08/2023 12:41 WG2091079
cis-1,2-Dichloroethene U 0.00101 0.00343 1 07/08/2023 12:41 WG2091079
trans-1,2-Dichloroethene U 0.00143 0.00685 1 07/08/2023 12:41 WG2091079
1,2-Dichloropropane U 0.00195 0.00685 1 07/08/2023 12:41 WG2091079
1,1-Dichloropropene U 0.00111 0.00343 1 07/08/2023 12:41 WG2091079
1,3-Dichloropropane U 0.000687 0.00685 1 07/08/2023 12:41 WG2091079
cis-1,3-Dichloropropene U 0.00104 0.00343 1 07/08/2023 12:41 WG2091079
trans-1,3-Dichloropropene U 0.00156 0.00685 1 07/08/2023 12:41 WG2091079
2,2-Dichloropropane U 0.00189 0.00343 1 07/08/2023 12:41 WG2091079
Di-isopropyl ether U 0.000562 0.00137 1 07/08/2023 12:41 WG2091079
Ethylbenzene U 0.00101 0.00343 1 07/08/2023 12:41 WG2091079
Hexachloro-1,3-butadiene U 0.00822 0.0343 1 07/08/2023 12:41 WG2091079
Isopropylbenzene U 0.000583 0.00343 1 07/08/2023 12:41 WG2091079
p-Isopropyltoluene U 0.00350 0.00685 1 07/08/2023 12:41 WG2091079
2-Butanone (MEK)U 0.0870 0.137 1 07/08/2023 12:41 WG2091079
Methylene Chloride U 0.00910 0.0343 1 07/08/2023 12:41 WG2091079
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1631472
ST-CS-5
Collected date/time: 06/29/23 11:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) U 0.00313 0.0343 1 07/08/2023 12:41 WG2091079
Methyl tert-butyl ether U 0.000480 0.00137 1 07/08/2023 12:41 WG2091079
Naphthalene U 0.00669 0.0171 1 07/08/2023 12:41 WG2091079
n-Propylbenzene U 0.00130 0.00685 1 07/08/2023 12:41 WG2091079
Styrene U 0.000314 0.0171 1 07/08/2023 12:41 WG2091079
1,1,1,2-Tetrachloroethane U 0.00130 0.00343 1 07/08/2023 12:41 WG2091079
1,1,2,2-Tetrachloroethane U 0.000953 0.00343 1 07/08/2023 12:41 WG2091079
1,1,2-Trichlorotrifluoroethane U 0.00103 0.00343 1 07/08/2023 12:41 WG2091079
Tetrachloroethene U 0.00123 0.00343 1 07/08/2023 12:41 WG2091079
Toluene 0.00256 J 0.00178 0.00685 1 07/08/2023 12:41 WG2091079
1,2,3-Trichlorobenzene U 0.0100 0.0171 1 07/08/2023 12:41 WG2091079
1,2,4-Trichlorobenzene U 0.00603 0.0171 1 07/08/2023 12:41 WG2091079
1,1,1-Trichloroethane U 0.00127 0.00343 1 07/08/2023 12:41 WG2091079
1,1,2-Trichloroethane U 0.000818 0.00343 1 07/08/2023 12:41 WG2091079
Trichloroethene U 0.000800 0.00137 1 07/08/2023 12:41 WG2091079
Trichlorofluoromethane U 0.00113 0.00343 1 07/08/2023 12:41 WG2091079
1,2,3-Trichloropropane U 0.00222 0.0171 1 07/08/2023 12:41 WG2091079
1,2,4-Trimethylbenzene U 0.00217 0.00685 1 07/08/2023 12:41 WG2091079
1,2,3-Trimethylbenzene U 0.00217 0.00685 1 07/08/2023 12:41 WG2091079
1,3,5-Trimethylbenzene U 0.00274 0.00685 1 07/08/2023 12:41 WG2091079
Vinyl chloride U 0.00159 0.00343 1 07/08/2023 12:41 WG2091079
Xylenes, Total 0.00156 J 0.00121 0.00891 1 07/08/2023 12:41 WG2091079
(S) Toluene-d8 109 75.0-131 07/08/2023 12:41 WG2091079
(S) 4-Bromofluorobenzene 92.8 67.0-138 07/08/2023 12:41 WG2091079
(S) 1,2-Dichloroethane-d4 97.2 70.0-130 07/08/2023 12:41 WG2091079
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 55.8 J 18.1 94.2 20 07/12/2023 04:39 WG2091569
(S) o-Terphenyl 93.1 J7 18.0-148 07/12/2023 04:39 WG2091569
Sample Narrative:
L1631472-06 WG2091569: Cannot run at lower dilution due to viscosity of extract
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.0127 0.0784 2 07/10/2023 21:17 WG2089936
Acenaphthylene U 0.0110 0.0784 2 07/10/2023 21:17 WG2089936
Anthracene U 0.0140 0.0784 2 07/10/2023 21:17 WG2089936
Benzidine U 0.147 3.93 2 07/10/2023 21:17 WG2089936
Benzo(a)anthracene U 0.0138 0.0784 2 07/10/2023 21:17 WG2089936
Benzo(b)fluoranthene 0.0199 J 0.0146 0.0784 2 07/10/2023 21:17 WG2089936
Benzo(k)fluoranthene U 0.0139 0.0784 2 07/10/2023 21:17 WG2089936
Benzo(g,h,i)perylene U 0.0144 0.0784 2 07/10/2023 21:17 WG2089936
Benzo(a)pyrene U 0.0146 0.0784 2 07/10/2023 21:17 WG2089936
Bis(2-chlorethoxy)methane U 0.0235 0.784 2 07/10/2023 21:17 WG2089936
Bis(2-chloroethyl)ether U 0.0259 0.784 2 07/10/2023 21:17 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0339 0.784 2 07/10/2023 21:17 WG2089936
4-Bromophenyl-phenylether U 0.0275 0.784 2 07/10/2023 21:17 WG2089936
2-Chloronaphthalene U 0.0138 0.0784 2 07/10/2023 21:17 WG2089936
4-Chlorophenyl-phenylether U 0.0273 0.784 2 07/10/2023 21:17 WG2089936
Chrysene U 0.0155 0.0784 2 07/10/2023 21:17 WG2089936
Dibenz(a,h)anthracene U 0.0218 0.0784 2 07/10/2023 21:17 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1631472
ST-CS-5
Collected date/time: 06/29/23 11:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichlorobenzene U 0.0232 0.784 2 07/10/2023 21:17 WG2089936
1,3-Dichlorobenzene U 0.0238 0.784 2 07/10/2023 21:17 WG2089936
1,4-Dichlorobenzene U 0.0233 0.784 2 07/10/2023 21:17 WG2089936
3,3-Dichlorobenzidine U 0.0290 0.784 2 07/10/2023 21:17 WG2089936
2,4-Dinitrotoluene U 0.0225 0.784 2 07/10/2023 21:17 WG2089936
2,6-Dinitrotoluene U 0.0257 0.784 2 07/10/2023 21:17 WG2089936
Fluoranthene U 0.0141 0.0784 2 07/10/2023 21:17 WG2089936
Fluorene U 0.0127 0.0784 2 07/10/2023 21:17 WG2089936
Hexachlorobenzene U 0.0278 0.784 2 07/10/2023 21:17 WG2089936
Hexachloro-1,3-butadiene U 0.0264 0.784 2 07/10/2023 21:17 WG2089936
Hexachlorocyclopentadiene U 0.0412 0.784 2 07/10/2023 21:17 WG2089936
Hexachloroethane U 0.0308 0.784 2 07/10/2023 21:17 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0221 0.0784 2 07/10/2023 21:17 WG2089936
Isophorone U 0.0240 0.784 2 07/10/2023 21:17 WG2089936
Naphthalene U 0.0197 0.0784 2 07/10/2023 21:17 WG2089936
Nitrobenzene U 0.0273 0.784 2 07/10/2023 21:17 WG2089936
n-Nitrosodimethylamine U 0.116 0.784 2 07/10/2023 21:17 WG2089936
n-Nitrosodiphenylamine U 0.0593 0.784 2 07/10/2023 21:17 WG2089936
n-Nitrosodi-n-propylamine U 0.0261 0.784 2 07/10/2023 21:17 WG2089936
Phenanthrene U 0.0155 0.0784 2 07/10/2023 21:17 WG2089936
Benzylbutyl phthalate U 0.0245 0.784 2 07/10/2023 21:17 WG2089936
Bis(2-ethylhexyl)phthalate U 0.0993 0.784 2 07/10/2023 21:17 WG2089936
Di-n-butyl phthalate U 0.0268 0.784 2 07/10/2023 21:17 WG2089936
Diethyl phthalate U 0.0259 0.784 2 07/10/2023 21:17 WG2089936
Dimethyl phthalate U 0.166 0.784 2 07/10/2023 21:17 WG2089936
Di-n-octyl phthalate U 0.0530 0.784 2 07/10/2023 21:17 WG2089936
Pyrene U 0.0153 0.0784 2 07/10/2023 21:17 WG2089936
1,2,4-Trichlorobenzene U 0.0245 0.784 2 07/10/2023 21:17 WG2089936
4-Chloro-3-methylphenol U 0.0254 0.784 2 07/10/2023 21:17 WG2089936
2-Chlorophenol U 0.0259 0.784 2 07/10/2023 21:17 WG2089936
2,4-Dichlorophenol U 0.0228 0.784 2 07/10/2023 21:17 WG2089936
2,4-Dimethylphenol U 0.0205 0.784 2 07/10/2023 21:17 WG2089936
4,6-Dinitro-2-methylphenol U 0.178 0.784 2 07/10/2023 21:17 WG2089936
2,4-Dinitrophenol U 0.184 0.784 2 07/10/2023 21:17 WG2089936
2-Nitrophenol U 0.0280 0.784 2 07/10/2023 21:17 WG2089936
4-Nitrophenol U 0.0245 0.784 2 07/10/2023 21:17 WG2089936
Pentachlorophenol U 0.0211 0.784 2 07/10/2023 21:17 WG2089936
Phenol U 0.0315 0.784 2 07/10/2023 21:17 WG2089936
2,4,6-Trichlorophenol U 0.0252 0.784 2 07/10/2023 21:17 WG2089936
(S) 2-Fluorophenol 55.5 12.0-120 07/10/2023 21:17 WG2089936
(S) Phenol-d5 54.0 10.0-120 07/10/2023 21:17 WG2089936
(S) Nitrobenzene-d5 54.1 10.0-122 07/10/2023 21:17 WG2089936
(S) 2-Fluorobiphenyl 57.4 15.0-120 07/10/2023 21:17 WG2089936
(S) 2,4,6-Tribromophenol 85.4 10.0-127 07/10/2023 21:17 WG2089936
(S) p-Terphenyl-d14 75.1 10.0-120 07/10/2023 21:17 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U 0.00271 0.00706 1 07/12/2023 01:50 WG2091376
Acenaphthene U 0.00246 0.00706 1 07/12/2023 01:50 WG2091376
Acenaphthylene U 0.00254 0.00706 1 07/12/2023 01:50 WG2091376
Benzo(a)anthracene U 0.00204 0.00706 1 07/12/2023 01:50 WG2091376
Benzo(a)pyrene U 0.00211 0.00706 1 07/12/2023 01:50 WG2091376
Benzo(b)fluoranthene U 0.00180 0.00706 1 07/12/2023 01:50 WG2091376
Benzo(g,h,i)perylene U 0.00208 0.00706 1 07/12/2023 01:50 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 06
L1631472
ST-CS-5
Collected date/time: 06/29/23 11:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Benzo(k)fluoranthene U 0.00253 0.00706 1 07/12/2023 01:50 WG2091376
Chrysene U 0.00273 0.00706 1 07/12/2023 01:50 WG2091376
Dibenz(a,h)anthracene U 0.00202 0.00706 1 07/12/2023 01:50 WG2091376
Fluoranthene U 0.00267 0.00706 1 07/12/2023 01:50 WG2091376
Fluorene U 0.00241 0.00706 1 07/12/2023 01:50 WG2091376
Indeno(1,2,3-cd)pyrene U 0.00213 0.00706 1 07/12/2023 01:50 WG2091376
Naphthalene U 0.00480 0.0235 1 07/12/2023 01:50 WG2091376
Phenanthrene U 0.00272 0.00706 1 07/12/2023 01:50 WG2091376
Pyrene U 0.00235 0.00706 1 07/12/2023 01:50 WG2091376
1-Methylnaphthalene U 0.00529 0.0235 1 07/12/2023 01:50 WG2091376
2-Methylnaphthalene 0.00823 J 0.00503 0.0235 1 07/12/2023 01:50 WG2091376
2-Chloronaphthalene U 0.00549 0.0235 1 07/12/2023 01:50 WG2091376
(S) p-Terphenyl-d14 66.9 23.0-120 07/12/2023 01:50 WG2091376
(S) Nitrobenzene-d5 63.8 14.0-149 07/12/2023 01:50 WG2091376
(S) 2-Fluorobiphenyl 61.0 34.0-125 07/12/2023 01:50 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1631472
ST-CS-6
Collected date/time: 06/29/23 11:22
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.4 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U 0.873 4.02 25 07/07/2023 21:04 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)97.2 77.0-120 07/07/2023 21:04 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0587 0.0804 1 07/07/2023 01:46 WG2090578
Acrylonitrile U 0.00581 0.0201 1 07/07/2023 01:46 WG2090578
Benzene U 0.000751 0.00161 1 07/07/2023 01:46 WG2090578
Bromobenzene U 0.00145 0.0201 1 07/07/2023 01:46 WG2090578
Bromodichloromethane U 0.00117 0.00402 1 07/07/2023 01:46 WG2090578
Bromoform U 0.00188 0.0402 1 07/07/2023 01:46 WG2090578
Bromomethane U 0.00317 0.0201 1 07/07/2023 01:46 WG2090578
n-Butylbenzene U 0.00844 0.0201 1 07/07/2023 01:46 WG2090578
sec-Butylbenzene U 0.00463 0.0201 1 07/07/2023 01:46 WG2090578
tert-Butylbenzene U 0.00314 0.00804 1 07/07/2023 01:46 WG2090578
Carbon tetrachloride U 0.00144 0.00804 1 07/07/2023 01:46 WG2090578
Chlorobenzene U 0.000338 0.00402 1 07/07/2023 01:46 WG2090578
Chlorodibromomethane U 0.000984 0.00402 1 07/07/2023 01:46 WG2090578
Chloroethane U 0.00273 0.00804 1 07/07/2023 01:46 WG2090578
Chloroform U 0.00166 0.00402 1 07/07/2023 01:46 WG2090578
Chloromethane U 0.00700 0.0201 1 07/07/2023 01:46 WG2090578
2-Chlorotoluene U 0.00139 0.00402 1 07/07/2023 01:46 WG2090578
4-Chlorotoluene U 0.000724 0.00804 1 07/07/2023 01:46 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00627 0.0402 1 07/07/2023 01:46 WG2090578
1,2-Dibromoethane U 0.00104 0.00402 1 07/07/2023 01:46 WG2090578
Dibromomethane U 0.00121 0.00804 1 07/07/2023 01:46 WG2090578
1,2-Dichlorobenzene U 0.000684 0.00804 1 07/07/2023 01:46 WG2090578
1,3-Dichlorobenzene U 0.000965 0.00804 1 07/07/2023 01:46 WG2090578
1,4-Dichlorobenzene U 0.00113 0.00804 1 07/07/2023 01:46 WG2090578
Dichlorodifluoromethane U 0.00259 0.00402 1 07/07/2023 01:46 WG2090578
1,1-Dichloroethane U 0.000790 0.00402 1 07/07/2023 01:46 WG2090578
1,2-Dichloroethane U 0.00104 0.00402 1 07/07/2023 01:46 WG2090578
1,1-Dichloroethene U 0.000975 0.00402 1 07/07/2023 01:46 WG2090578
cis-1,2-Dichloroethene U 0.00118 0.00402 1 07/07/2023 01:46 WG2090578
trans-1,2-Dichloroethene U 0.00167 0.00804 1 07/07/2023 01:46 WG2090578
1,2-Dichloropropane U 0.00228 0.00804 1 07/07/2023 01:46 WG2090578
1,1-Dichloropropene U 0.00130 0.00402 1 07/07/2023 01:46 WG2090578
1,3-Dichloropropane U 0.000806 0.00804 1 07/07/2023 01:46 WG2090578
cis-1,3-Dichloropropene U 0.00122 0.00402 1 07/07/2023 01:46 WG2090578
trans-1,3-Dichloropropene U 0.00183 0.00804 1 07/07/2023 01:46 WG2090578
2,2-Dichloropropane U 0.00222 0.00402 1 07/07/2023 01:46 WG2090578
Di-isopropyl ether U 0.000659 0.00161 1 07/07/2023 01:46 WG2090578
Ethylbenzene U 0.00119 0.00402 1 07/07/2023 01:46 WG2090578
Hexachloro-1,3-butadiene U 0.00965 0.0402 1 07/07/2023 01:46 WG2090578
Isopropylbenzene U 0.000684 0.00402 1 07/07/2023 01:46 WG2090578
p-Isopropyltoluene U 0.00410 0.00804 1 07/07/2023 01:46 WG2090578
2-Butanone (MEK)U 0.102 0.161 1 07/07/2023 01:46 WG2090578
Methylene Chloride U 0.0107 0.0402 1 07/07/2023 01:46 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1631472
ST-CS-6
Collected date/time: 06/29/23 11:22
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) U 0.00367 0.0402 1 07/07/2023 01:46 WG2090578
Methyl tert-butyl ether U 0.000563 0.00161 1 07/07/2023 01:46 WG2090578
Naphthalene U J4 0.00785 0.0201 1 07/07/2023 01:46 WG2090578
n-Propylbenzene U 0.00153 0.00804 1 07/07/2023 01:46 WG2090578
Styrene U 0.000368 0.0201 1 07/07/2023 01:46 WG2090578
1,1,1,2-Tetrachloroethane U 0.00152 0.00402 1 07/07/2023 01:46 WG2090578
1,1,2,2-Tetrachloroethane U 0.00112 0.00402 1 07/07/2023 01:46 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00121 0.00402 1 07/07/2023 01:46 WG2090578
Tetrachloroethene U 0.00144 0.00402 1 07/07/2023 01:46 WG2090578
Toluene U 0.00209 0.00804 1 07/07/2023 01:46 WG2090578
1,2,3-Trichlorobenzene U 0.0118 0.0201 1 07/07/2023 01:46 WG2090578
1,2,4-Trichlorobenzene U 0.00708 0.0201 1 07/07/2023 01:46 WG2090578
1,1,1-Trichloroethane U 0.00148 0.00402 1 07/07/2023 01:46 WG2090578
1,1,2-Trichloroethane U 0.000960 0.00402 1 07/07/2023 01:46 WG2090578
Trichloroethene U 0.000939 0.00161 1 07/07/2023 01:46 WG2090578
Trichlorofluoromethane U 0.00133 0.00402 1 07/07/2023 01:46 WG2090578
1,2,3-Trichloropropane U 0.00261 0.0201 1 07/07/2023 01:46 WG2090578
1,2,4-Trimethylbenzene U 0.00254 0.00804 1 07/07/2023 01:46 WG2090578
1,2,3-Trimethylbenzene U 0.00254 0.00804 1 07/07/2023 01:46 WG2090578
1,3,5-Trimethylbenzene U 0.00322 0.00804 1 07/07/2023 01:46 WG2090578
Vinyl chloride U 0.00187 0.00402 1 07/07/2023 01:46 WG2090578
Xylenes, Total U 0.00142 0.0105 1 07/07/2023 01:46 WG2090578
(S) Toluene-d8 112 75.0-131 07/07/2023 01:46 WG2090578
(S) 4-Bromofluorobenzene 97.4 67.0-138 07/07/2023 01:46 WG2090578
(S) 1,2-Dichloroethane-d4 91.1 70.0-130 07/07/2023 01:46 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.40 J 0.994 5.17 1 07/11/2023 10:22 WG2091569
(S) o-Terphenyl 71.1 18.0-148 07/11/2023 10:22 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00697 0.0431 1 07/08/2023 16:03 WG2089936
Acenaphthylene U 0.00606 0.0431 1 07/08/2023 16:03 WG2089936
Anthracene U 0.00767 0.0431 1 07/08/2023 16:03 WG2089936
Benzidine U 0.0809 2.16 1 07/08/2023 16:03 WG2089936
Benzo(a)anthracene U 0.00759 0.0431 1 07/08/2023 16:03 WG2089936
Benzo(b)fluoranthene U 0.00803 0.0431 1 07/08/2023 16:03 WG2089936
Benzo(k)fluoranthene U 0.00765 0.0431 1 07/08/2023 16:03 WG2089936
Benzo(g,h,i)perylene U 0.00787 0.0431 1 07/08/2023 16:03 WG2089936
Benzo(a)pyrene U 0.00800 0.0431 1 07/08/2023 16:03 WG2089936
Bis(2-chlorethoxy)methane U 0.0129 0.431 1 07/08/2023 16:03 WG2089936
Bis(2-chloroethyl)ether U 0.0142 0.431 1 07/08/2023 16:03 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0186 0.431 1 07/08/2023 16:03 WG2089936
4-Bromophenyl-phenylether U 0.0151 0.431 1 07/08/2023 16:03 WG2089936
2-Chloronaphthalene U 0.00756 0.0431 1 07/08/2023 16:03 WG2089936
4-Chlorophenyl-phenylether U 0.0150 0.431 1 07/08/2023 16:03 WG2089936
Chrysene U 0.00856 0.0431 1 07/08/2023 16:03 WG2089936
Dibenz(a,h)anthracene U 0.0119 0.0431 1 07/08/2023 16:03 WG2089936
1,2-Dichlorobenzene U 0.0128 0.431 1 07/08/2023 16:03 WG2089936
1,3-Dichlorobenzene U 0.0131 0.431 1 07/08/2023 16:03 WG2089936
1,4-Dichlorobenzene U 0.0128 0.431 1 07/08/2023 16:03 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1631472
ST-CS-6
Collected date/time: 06/29/23 11:22
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0159 0.431 1 07/08/2023 16:03 WG2089936
2,4-Dinitrotoluene U 0.0123 0.431 1 07/08/2023 16:03 WG2089936
2,6-Dinitrotoluene U 0.0141 0.431 1 07/08/2023 16:03 WG2089936
Fluoranthene U 0.00777 0.0431 1 07/08/2023 16:03 WG2089936
Fluorene U 0.00701 0.0431 1 07/08/2023 16:03 WG2089936
Hexachlorobenzene U 0.0153 0.431 1 07/08/2023 16:03 WG2089936
Hexachloro-1,3-butadiene U 0.0145 0.431 1 07/08/2023 16:03 WG2089936
Hexachlorocyclopentadiene U 0.0226 0.431 1 07/08/2023 16:03 WG2089936
Hexachloroethane U 0.0169 0.431 1 07/08/2023 16:03 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0122 0.0431 1 07/08/2023 16:03 WG2089936
Isophorone U 0.0132 0.431 1 07/08/2023 16:03 WG2089936
Naphthalene U 0.0108 0.0431 1 07/08/2023 16:03 WG2089936
Nitrobenzene U 0.0150 0.431 1 07/08/2023 16:03 WG2089936
n-Nitrosodimethylamine U 0.0639 0.431 1 07/08/2023 16:03 WG2089936
n-Nitrosodiphenylamine U 0.0326 0.431 1 07/08/2023 16:03 WG2089936
n-Nitrosodi-n-propylamine U 0.0144 0.431 1 07/08/2023 16:03 WG2089936
Phenanthrene U 0.00855 0.0431 1 07/08/2023 16:03 WG2089936
Benzylbutyl phthalate U 0.0134 0.431 1 07/08/2023 16:03 WG2089936
Bis(2-ethylhexyl)phthalate U 0.0546 0.431 1 07/08/2023 16:03 WG2089936
Di-n-butyl phthalate U 0.0147 0.431 1 07/08/2023 16:03 WG2089936
Diethyl phthalate U 0.0142 0.431 1 07/08/2023 16:03 WG2089936
Dimethyl phthalate U 0.0913 0.431 1 07/08/2023 16:03 WG2089936
Di-n-octyl phthalate U 0.0291 0.431 1 07/08/2023 16:03 WG2089936
Pyrene U 0.00838 0.0431 1 07/08/2023 16:03 WG2089936
1,2,4-Trichlorobenzene U 0.0134 0.431 1 07/08/2023 16:03 WG2089936
4-Chloro-3-methylphenol U 0.0140 0.431 1 07/08/2023 16:03 WG2089936
2-Chlorophenol U 0.0142 0.431 1 07/08/2023 16:03 WG2089936
2,4-Dichlorophenol U 0.0125 0.431 1 07/08/2023 16:03 WG2089936
2,4-Dimethylphenol U 0.0112 0.431 1 07/08/2023 16:03 WG2089936
4,6-Dinitro-2-methylphenol U 0.0976 0.431 1 07/08/2023 16:03 WG2089936
2,4-Dinitrophenol U 0.101 0.431 1 07/08/2023 16:03 WG2089936
2-Nitrophenol U 0.0154 0.431 1 07/08/2023 16:03 WG2089936
4-Nitrophenol U 0.0134 0.431 1 07/08/2023 16:03 WG2089936
Pentachlorophenol U 0.0116 0.431 1 07/08/2023 16:03 WG2089936
Phenol U 0.0173 0.431 1 07/08/2023 16:03 WG2089936
2,4,6-Trichlorophenol U 0.0138 0.431 1 07/08/2023 16:03 WG2089936
(S) 2-Fluorophenol 47.5 12.0-120 07/08/2023 16:03 WG2089936
(S) Phenol-d5 41.3 10.0-120 07/08/2023 16:03 WG2089936
(S) Nitrobenzene-d5 41.3 10.0-122 07/08/2023 16:03 WG2089936
(S) 2-Fluorobiphenyl 43.2 15.0-120 07/08/2023 16:03 WG2089936
(S) 2,4,6-Tribromophenol 54.5 10.0-127 07/08/2023 16:03 WG2089936
(S) p-Terphenyl-d14 55.9 10.0-120 07/08/2023 16:03 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U 0.00297 0.00776 1 07/12/2023 02:08 WG2091376
Acenaphthene U 0.00270 0.00776 1 07/12/2023 02:08 WG2091376
Acenaphthylene U 0.00279 0.00776 1 07/12/2023 02:08 WG2091376
Benzo(a)anthracene 0.0569 0.00224 0.00776 1 07/12/2023 02:08 WG2091376
Benzo(a)pyrene 0.0697 0.00231 0.00776 1 07/12/2023 02:08 WG2091376
Benzo(b)fluoranthene 0.0967 0.00198 0.00776 1 07/12/2023 02:08 WG2091376
Benzo(g,h,i)perylene 0.0558 0.00229 0.00776 1 07/12/2023 02:08 WG2091376
Benzo(k)fluoranthene 0.0349 0.00278 0.00776 1 07/12/2023 02:08 WG2091376
Chrysene 0.0747 0.00300 0.00776 1 07/12/2023 02:08 WG2091376
Dibenz(a,h)anthracene 0.00968 0.00222 0.00776 1 07/12/2023 02:08 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 07
L1631472
ST-CS-6
Collected date/time: 06/29/23 11:22
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluoranthene 0.142 0.00293 0.00776 1 07/12/2023 02:08 WG2091376
Fluorene U 0.00265 0.00776 1 07/12/2023 02:08 WG2091376
Indeno(1,2,3-cd)pyrene 0.0633 0.00234 0.00776 1 07/12/2023 02:08 WG2091376
Naphthalene U 0.00527 0.0259 1 07/12/2023 02:08 WG2091376
Phenanthrene 0.0273 0.00299 0.00776 1 07/12/2023 02:08 WG2091376
Pyrene 0.115 0.00259 0.00776 1 07/12/2023 02:08 WG2091376
1-Methylnaphthalene U 0.00580 0.0259 1 07/12/2023 02:08 WG2091376
2-Methylnaphthalene U 0.00552 0.0259 1 07/12/2023 02:08 WG2091376
2-Chloronaphthalene U 0.00602 0.0259 1 07/12/2023 02:08 WG2091376
(S) p-Terphenyl-d14 70.9 23.0-120 07/12/2023 02:08 WG2091376
(S) Nitrobenzene-d5 74.5 14.0-149 07/12/2023 02:08 WG2091376
(S) 2-Fluorobiphenyl 65.2 34.0-125 07/12/2023 02:08 WG2091376
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1631472
ST-CS-7
Collected date/time: 06/29/23 11:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.2 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U J3 0.917 4.22 25 07/07/2023 21:26 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)96.7 77.0-120 07/07/2023 21:26 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0616 0.0844 1 07/07/2023 02:05 WG2090578
Acrylonitrile U 0.00610 0.0211 1 07/07/2023 02:05 WG2090578
Benzene U 0.000789 0.00169 1 07/07/2023 02:05 WG2090578
Bromobenzene U 0.00152 0.0211 1 07/07/2023 02:05 WG2090578
Bromodichloromethane U 0.00122 0.00422 1 07/07/2023 02:05 WG2090578
Bromoform U 0.00198 0.0422 1 07/07/2023 02:05 WG2090578
Bromomethane U 0.00333 0.0211 1 07/07/2023 02:05 WG2090578
n-Butylbenzene U 0.00887 0.0211 1 07/07/2023 02:05 WG2090578
sec-Butylbenzene U 0.00486 0.0211 1 07/07/2023 02:05 WG2090578
tert-Butylbenzene U 0.00329 0.00844 1 07/07/2023 02:05 WG2090578
Carbon tetrachloride U 0.00152 0.00844 1 07/07/2023 02:05 WG2090578
Chlorobenzene U 0.000355 0.00422 1 07/07/2023 02:05 WG2090578
Chlorodibromomethane U 0.00103 0.00422 1 07/07/2023 02:05 WG2090578
Chloroethane U 0.00287 0.00844 1 07/07/2023 02:05 WG2090578
Chloroform U 0.00174 0.00422 1 07/07/2023 02:05 WG2090578
Chloromethane U 0.00735 0.0211 1 07/07/2023 02:05 WG2090578
2-Chlorotoluene U 0.00146 0.00422 1 07/07/2023 02:05 WG2090578
4-Chlorotoluene U 0.000760 0.00844 1 07/07/2023 02:05 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00659 0.0422 1 07/07/2023 02:05 WG2090578
1,2-Dibromoethane U 0.00109 0.00422 1 07/07/2023 02:05 WG2090578
Dibromomethane U 0.00127 0.00844 1 07/07/2023 02:05 WG2090578
1,2-Dichlorobenzene U 0.000718 0.00844 1 07/07/2023 02:05 WG2090578
1,3-Dichlorobenzene U 0.00101 0.00844 1 07/07/2023 02:05 WG2090578
1,4-Dichlorobenzene U 0.00118 0.00844 1 07/07/2023 02:05 WG2090578
Dichlorodifluoromethane U 0.00272 0.00422 1 07/07/2023 02:05 WG2090578
1,1-Dichloroethane U 0.000829 0.00422 1 07/07/2023 02:05 WG2090578
1,2-Dichloroethane U 0.00110 0.00422 1 07/07/2023 02:05 WG2090578
1,1-Dichloroethene U 0.00102 0.00422 1 07/07/2023 02:05 WG2090578
cis-1,2-Dichloroethene U 0.00124 0.00422 1 07/07/2023 02:05 WG2090578
trans-1,2-Dichloroethene U 0.00176 0.00844 1 07/07/2023 02:05 WG2090578
1,2-Dichloropropane U 0.00240 0.00844 1 07/07/2023 02:05 WG2090578
1,1-Dichloropropene U 0.00137 0.00422 1 07/07/2023 02:05 WG2090578
1,3-Dichloropropane U 0.000846 0.00844 1 07/07/2023 02:05 WG2090578
cis-1,3-Dichloropropene U 0.00128 0.00422 1 07/07/2023 02:05 WG2090578
trans-1,3-Dichloropropene U 0.00193 0.00844 1 07/07/2023 02:05 WG2090578
2,2-Dichloropropane U 0.00233 0.00422 1 07/07/2023 02:05 WG2090578
Di-isopropyl ether U 0.000692 0.00169 1 07/07/2023 02:05 WG2090578
Ethylbenzene U 0.00124 0.00422 1 07/07/2023 02:05 WG2090578
Hexachloro-1,3-butadiene U 0.0101 0.0422 1 07/07/2023 02:05 WG2090578
Isopropylbenzene U 0.000718 0.00422 1 07/07/2023 02:05 WG2090578
p-Isopropyltoluene U 0.00431 0.00844 1 07/07/2023 02:05 WG2090578
2-Butanone (MEK)U 0.107 0.169 1 07/07/2023 02:05 WG2090578
Methylene Chloride U 0.0112 0.0422 1 07/07/2023 02:05 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1631472
ST-CS-7
Collected date/time: 06/29/23 11:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) U 0.00385 0.0422 1 07/07/2023 02:05 WG2090578
Methyl tert-butyl ether U 0.000591 0.00169 1 07/07/2023 02:05 WG2090578
Naphthalene U J4 0.00824 0.0211 1 07/07/2023 02:05 WG2090578
n-Propylbenzene U 0.00160 0.00844 1 07/07/2023 02:05 WG2090578
Styrene U 0.000387 0.0211 1 07/07/2023 02:05 WG2090578
1,1,1,2-Tetrachloroethane U 0.00160 0.00422 1 07/07/2023 02:05 WG2090578
1,1,2,2-Tetrachloroethane U 0.00117 0.00422 1 07/07/2023 02:05 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00127 0.00422 1 07/07/2023 02:05 WG2090578
Tetrachloroethene U 0.00151 0.00422 1 07/07/2023 02:05 WG2090578
Toluene 0.00802 J 0.00220 0.00844 1 07/07/2023 02:05 WG2090578
1,2,3-Trichlorobenzene U 0.0124 0.0211 1 07/07/2023 02:05 WG2090578
1,2,4-Trichlorobenzene U 0.00743 0.0211 1 07/07/2023 02:05 WG2090578
1,1,1-Trichloroethane U 0.00156 0.00422 1 07/07/2023 02:05 WG2090578
1,1,2-Trichloroethane U 0.00101 0.00422 1 07/07/2023 02:05 WG2090578
Trichloroethene U 0.000986 0.00169 1 07/07/2023 02:05 WG2090578
Trichlorofluoromethane U 0.00140 0.00422 1 07/07/2023 02:05 WG2090578
1,2,3-Trichloropropane U 0.00274 0.0211 1 07/07/2023 02:05 WG2090578
1,2,4-Trimethylbenzene U 0.00267 0.00844 1 07/07/2023 02:05 WG2090578
1,2,3-Trimethylbenzene U 0.00267 0.00844 1 07/07/2023 02:05 WG2090578
1,3,5-Trimethylbenzene U 0.00338 0.00844 1 07/07/2023 02:05 WG2090578
Vinyl chloride U 0.00196 0.00422 1 07/07/2023 02:05 WG2090578
Xylenes, Total 0.00290 J 0.00149 0.0110 1 07/07/2023 02:05 WG2090578
(S) Toluene-d8 110 75.0-131 07/07/2023 02:05 WG2090578
(S) 4-Bromofluorobenzene 108 67.0-138 07/07/2023 02:05 WG2090578
(S) 1,2-Dichloroethane-d4 97.2 70.0-130 07/07/2023 02:05 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.80 J 1.01 5.25 1 07/11/2023 10:49 WG2091569
(S) o-Terphenyl 62.2 18.0-148 07/11/2023 10:49 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00707 0.0437 1 07/08/2023 18:14 WG2089936
Acenaphthylene U 0.00615 0.0437 1 07/08/2023 18:14 WG2089936
Anthracene U 0.00778 0.0437 1 07/08/2023 18:14 WG2089936
Benzidine U 0.0821 2.19 1 07/08/2023 18:14 WG2089936
Benzo(a)anthracene U 0.00770 0.0437 1 07/08/2023 18:14 WG2089936
Benzo(b)fluoranthene U 0.00815 0.0437 1 07/08/2023 18:14 WG2089936
Benzo(k)fluoranthene U 0.00777 0.0437 1 07/08/2023 18:14 WG2089936
Benzo(g,h,i)perylene U 0.00799 0.0437 1 07/08/2023 18:14 WG2089936
Benzo(a)pyrene U 0.00812 0.0437 1 07/08/2023 18:14 WG2089936
Bis(2-chlorethoxy)methane U 0.0131 0.437 1 07/08/2023 18:14 WG2089936
Bis(2-chloroethyl)ether U 0.0144 0.437 1 07/08/2023 18:14 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0189 0.437 1 07/08/2023 18:14 WG2089936
4-Bromophenyl-phenylether U 0.0154 0.437 1 07/08/2023 18:14 WG2089936
2-Chloronaphthalene U 0.00768 0.0437 1 07/08/2023 18:14 WG2089936
4-Chlorophenyl-phenylether U 0.0152 0.437 1 07/08/2023 18:14 WG2089936
Chrysene U 0.00869 0.0437 1 07/08/2023 18:14 WG2089936
Dibenz(a,h)anthracene U 0.0121 0.0437 1 07/08/2023 18:14 WG2089936
1,2-Dichlorobenzene U 0.0130 0.437 1 07/08/2023 18:14 WG2089936
1,3-Dichlorobenzene U 0.0133 0.437 1 07/08/2023 18:14 WG2089936
1,4-Dichlorobenzene U 0.0130 0.437 1 07/08/2023 18:14 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1631472
ST-CS-7
Collected date/time: 06/29/23 11:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0161 0.437 1 07/08/2023 18:14 WG2089936
2,4-Dinitrotoluene U 0.0125 0.437 1 07/08/2023 18:14 WG2089936
2,6-Dinitrotoluene U 0.0143 0.437 1 07/08/2023 18:14 WG2089936
Fluoranthene U 0.00789 0.0437 1 07/08/2023 18:14 WG2089936
Fluorene U 0.00711 0.0437 1 07/08/2023 18:14 WG2089936
Hexachlorobenzene U 0.0155 0.437 1 07/08/2023 18:14 WG2089936
Hexachloro-1,3-butadiene U 0.0147 0.437 1 07/08/2023 18:14 WG2089936
Hexachlorocyclopentadiene U 0.0230 0.437 1 07/08/2023 18:14 WG2089936
Hexachloroethane U 0.0172 0.437 1 07/08/2023 18:14 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0123 0.0437 1 07/08/2023 18:14 WG2089936
Isophorone U 0.0134 0.437 1 07/08/2023 18:14 WG2089936
Naphthalene U 0.0110 0.0437 1 07/08/2023 18:14 WG2089936
Nitrobenzene U 0.0152 0.437 1 07/08/2023 18:14 WG2089936
n-Nitrosodimethylamine U 0.0648 0.437 1 07/08/2023 18:14 WG2089936
n-Nitrosodiphenylamine U 0.0331 0.437 1 07/08/2023 18:14 WG2089936
n-Nitrosodi-n-propylamine U 0.0146 0.437 1 07/08/2023 18:14 WG2089936
Phenanthrene U 0.00867 0.0437 1 07/08/2023 18:14 WG2089936
Benzylbutyl phthalate U 0.0136 0.437 1 07/08/2023 18:14 WG2089936
Bis(2-ethylhexyl)phthalate U 0.0554 0.437 1 07/08/2023 18:14 WG2089936
Di-n-butyl phthalate U 0.0150 0.437 1 07/08/2023 18:14 WG2089936
Diethyl phthalate U 0.0144 0.437 1 07/08/2023 18:14 WG2089936
Dimethyl phthalate U 0.0926 0.437 1 07/08/2023 18:14 WG2089936
Di-n-octyl phthalate U 0.0295 0.437 1 07/08/2023 18:14 WG2089936
Pyrene U 0.00850 0.0437 1 07/08/2023 18:14 WG2089936
1,2,4-Trichlorobenzene U 0.0136 0.437 1 07/08/2023 18:14 WG2089936
4-Chloro-3-methylphenol U 0.0142 0.437 1 07/08/2023 18:14 WG2089936
2-Chlorophenol U 0.0144 0.437 1 07/08/2023 18:14 WG2089936
2,4-Dichlorophenol U 0.0127 0.437 1 07/08/2023 18:14 WG2089936
2,4-Dimethylphenol U 0.0114 0.437 1 07/08/2023 18:14 WG2089936
4,6-Dinitro-2-methylphenol U 0.0991 0.437 1 07/08/2023 18:14 WG2089936
2,4-Dinitrophenol U 0.102 0.437 1 07/08/2023 18:14 WG2089936
2-Nitrophenol U 0.0156 0.437 1 07/08/2023 18:14 WG2089936
4-Nitrophenol U 0.0136 0.437 1 07/08/2023 18:14 WG2089936
Pentachlorophenol U 0.0118 0.437 1 07/08/2023 18:14 WG2089936
Phenol U 0.0176 0.437 1 07/08/2023 18:14 WG2089936
2,4,6-Trichlorophenol U 0.0140 0.437 1 07/08/2023 18:14 WG2089936
(S) 2-Fluorophenol 50.9 12.0-120 07/08/2023 18:14 WG2089936
(S) Phenol-d5 39.6 10.0-120 07/08/2023 18:14 WG2089936
(S) Nitrobenzene-d5 46.6 10.0-122 07/08/2023 18:14 WG2089936
(S) 2-Fluorobiphenyl 47.9 15.0-120 07/08/2023 18:14 WG2089936
(S) 2,4,6-Tribromophenol 54.7 10.0-127 07/08/2023 18:14 WG2089936
(S) p-Terphenyl-d14 47.6 10.0-120 07/08/2023 18:14 WG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U 0.00302 0.00787 1 07/10/2023 20:23 WG2091526
Acenaphthene U 0.00274 0.00787 1 07/10/2023 20:23 WG2091526
Acenaphthylene U 0.00283 0.00787 1 07/10/2023 20:23 WG2091526
Benzo(a)anthracene 0.00266 J 0.00227 0.00787 1 07/10/2023 20:23 WG2091526
Benzo(a)pyrene 0.00353 J 0.00235 0.00787 1 07/10/2023 20:23 WG2091526
Benzo(b)fluoranthene 0.00388 J 0.00201 0.00787 1 07/10/2023 20:23 WG2091526
Benzo(g,h,i)perylene 0.00479 J 0.00232 0.00787 1 07/10/2023 20:23 WG2091526
Benzo(k)fluoranthene U 0.00282 0.00787 1 07/10/2023 20:23 WG2091526
Chrysene U 0.00304 0.00787 1 07/10/2023 20:23 WG2091526
Dibenz(a,h)anthracene U 0.00226 0.00787 1 07/10/2023 20:23 WG2091526
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 08
L1631472
ST-CS-7
Collected date/time: 06/29/23 11:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluoranthene 0.00556 J 0.00298 0.00787 1 07/10/2023 20:23 WG2091526
Fluorene U 0.00269 0.00787 1 07/10/2023 20:23 WG2091526
Indeno(1,2,3-cd)pyrene 0.00303 J 0.00237 0.00787 1 07/10/2023 20:23 WG2091526
Naphthalene U 0.00535 0.0262 1 07/10/2023 20:23 WG2091526
Phenanthrene U 0.00303 0.00787 1 07/10/2023 20:23 WG2091526
Pyrene 0.00609 J 0.00262 0.00787 1 07/10/2023 20:23 WG2091526
1-Methylnaphthalene U 0.00589 0.0262 1 07/10/2023 20:23 WG2091526
2-Methylnaphthalene U 0.00560 0.0262 1 07/10/2023 20:23 WG2091526
2-Chloronaphthalene U 0.00611 0.0262 1 07/10/2023 20:23 WG2091526
(S) p-Terphenyl-d14 61.9 23.0-120 07/10/2023 20:23 WG2091526
(S) Nitrobenzene-d5 68.7 14.0-149 07/10/2023 20:23 WG2091526
(S) 2-Fluorobiphenyl 60.7 34.0-125 07/10/2023 20:23 WG2091526
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1631472
ST-CS-COMP
Collected date/time: 06/29/23 11:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.4 1 07/05/2023 11:15 WG2089245
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.57 J 0.864 3.98 25 07/07/2023 21:49 WG2090723
(S)
a,a,a-Trifluorotoluene(FID)97.9 77.0-120 07/07/2023 21:49 WG2090723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0581 0.0796 1 07/07/2023 02:24 WG2090578
Acrylonitrile U 0.00574 0.0199 1 07/07/2023 02:24 WG2090578
Benzene U 0.000743 0.00159 1 07/07/2023 02:24 WG2090578
Bromobenzene U 0.00143 0.0199 1 07/07/2023 02:24 WG2090578
Bromodichloromethane U 0.00115 0.00398 1 07/07/2023 02:24 WG2090578
Bromoform U 0.00186 0.0398 1 07/07/2023 02:24 WG2090578
Bromomethane U 0.00313 0.0199 1 07/07/2023 02:24 WG2090578
n-Butylbenzene U 0.00835 0.0199 1 07/07/2023 02:24 WG2090578
sec-Butylbenzene U 0.00458 0.0199 1 07/07/2023 02:24 WG2090578
tert-Butylbenzene U 0.00310 0.00796 1 07/07/2023 02:24 WG2090578
Carbon tetrachloride U 0.00143 0.00796 1 07/07/2023 02:24 WG2090578
Chlorobenzene U 0.000334 0.00398 1 07/07/2023 02:24 WG2090578
Chlorodibromomethane U 0.000974 0.00398 1 07/07/2023 02:24 WG2090578
Chloroethane U 0.00270 0.00796 1 07/07/2023 02:24 WG2090578
Chloroform U 0.00164 0.00398 1 07/07/2023 02:24 WG2090578
Chloromethane U 0.00692 0.0199 1 07/07/2023 02:24 WG2090578
2-Chlorotoluene U 0.00138 0.00398 1 07/07/2023 02:24 WG2090578
4-Chlorotoluene U 0.000716 0.00796 1 07/07/2023 02:24 WG2090578
1,2-Dibromo-3-Chloropropane U 0.00621 0.0398 1 07/07/2023 02:24 WG2090578
1,2-Dibromoethane U 0.00103 0.00398 1 07/07/2023 02:24 WG2090578
Dibromomethane U 0.00119 0.00796 1 07/07/2023 02:24 WG2090578
1,2-Dichlorobenzene U 0.000676 0.00796 1 07/07/2023 02:24 WG2090578
1,3-Dichlorobenzene U 0.000955 0.00796 1 07/07/2023 02:24 WG2090578
1,4-Dichlorobenzene U 0.00111 0.00796 1 07/07/2023 02:24 WG2090578
Dichlorodifluoromethane U 0.00256 0.00398 1 07/07/2023 02:24 WG2090578
1,1-Dichloroethane U 0.000781 0.00398 1 07/07/2023 02:24 WG2090578
1,2-Dichloroethane U 0.00103 0.00398 1 07/07/2023 02:24 WG2090578
1,1-Dichloroethene U 0.000964 0.00398 1 07/07/2023 02:24 WG2090578
cis-1,2-Dichloroethene U 0.00117 0.00398 1 07/07/2023 02:24 WG2090578
trans-1,2-Dichloroethene U 0.00165 0.00796 1 07/07/2023 02:24 WG2090578
1,2-Dichloropropane U 0.00226 0.00796 1 07/07/2023 02:24 WG2090578
1,1-Dichloropropene U 0.00129 0.00398 1 07/07/2023 02:24 WG2090578
1,3-Dichloropropane U 0.000797 0.00796 1 07/07/2023 02:24 WG2090578
cis-1,3-Dichloropropene U 0.00120 0.00398 1 07/07/2023 02:24 WG2090578
trans-1,3-Dichloropropene U 0.00181 0.00796 1 07/07/2023 02:24 WG2090578
2,2-Dichloropropane U 0.00220 0.00398 1 07/07/2023 02:24 WG2090578
Di-isopropyl ether U 0.000652 0.00159 1 07/07/2023 02:24 WG2090578
Ethylbenzene U 0.00117 0.00398 1 07/07/2023 02:24 WG2090578
Hexachloro-1,3-butadiene U 0.00955 0.0398 1 07/07/2023 02:24 WG2090578
Isopropylbenzene U 0.000676 0.00398 1 07/07/2023 02:24 WG2090578
p-Isopropyltoluene U 0.00406 0.00796 1 07/07/2023 02:24 WG2090578
2-Butanone (MEK)U 0.101 0.159 1 07/07/2023 02:24 WG2090578
Methylene Chloride U 0.0106 0.0398 1 07/07/2023 02:24 WG2090578
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1631472
ST-CS-COMP
Collected date/time: 06/29/23 11:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) 0.0109 J 0.00363 0.0398 1 07/07/2023 02:24 WG2090578
Methyl tert-butyl ether U 0.000557 0.00159 1 07/07/2023 02:24 WG2090578
Naphthalene 0.0337 J4 0.00776 0.0199 1 07/07/2023 02:24 WG2090578
n-Propylbenzene 0.0116 0.00151 0.00796 1 07/07/2023 02:24 WG2090578
Styrene U 0.000364 0.0199 1 07/07/2023 02:24 WG2090578
1,1,1,2-Tetrachloroethane U 0.00151 0.00398 1 07/07/2023 02:24 WG2090578
1,1,2,2-Tetrachloroethane U 0.00111 0.00398 1 07/07/2023 02:24 WG2090578
1,1,2-Trichlorotrifluoroethane U 0.00120 0.00398 1 07/07/2023 02:24 WG2090578
Tetrachloroethene 0.00657 0.00143 0.00398 1 07/07/2023 02:24 WG2090578
Toluene 0.0267 0.00207 0.00796 1 07/07/2023 02:24 WG2090578
1,2,3-Trichlorobenzene 0.0197 J 0.0117 0.0199 1 07/07/2023 02:24 WG2090578
1,2,4-Trichlorobenzene U 0.00700 0.0199 1 07/07/2023 02:24 WG2090578
1,1,1-Trichloroethane U 0.00147 0.00398 1 07/07/2023 02:24 WG2090578
1,1,2-Trichloroethane U 0.000950 0.00398 1 07/07/2023 02:24 WG2090578
Trichloroethene U 0.000929 0.00159 1 07/07/2023 02:24 WG2090578
Trichlorofluoromethane U 0.00132 0.00398 1 07/07/2023 02:24 WG2090578
1,2,3-Trichloropropane U 0.00258 0.0199 1 07/07/2023 02:24 WG2090578
1,2,4-Trimethylbenzene 0.0948 0.00251 0.00796 1 07/07/2023 02:24 WG2090578
1,2,3-Trimethylbenzene 0.0259 0.00251 0.00796 1 07/07/2023 02:24 WG2090578
1,3,5-Trimethylbenzene 0.0312 0.00318 0.00796 1 07/07/2023 02:24 WG2090578
Vinyl chloride U 0.00185 0.00398 1 07/07/2023 02:24 WG2090578
Xylenes, Total 0.0565 0.00140 0.0103 1 07/07/2023 02:24 WG2090578
(S) Toluene-d8 111 75.0-131 07/07/2023 02:24 WG2090578
(S) 4-Bromofluorobenzene 104 67.0-138 07/07/2023 02:24 WG2090578
(S) 1,2-Dichloroethane-d4 80.7 70.0-130 07/07/2023 02:24 WG2090578
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 58.7 0.969 5.04 1 07/12/2023 03:00 WG2091569
(S) o-Terphenyl 50.3 18.0-148 07/12/2023 03:00 WG2091569
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.0339 0.210 5 07/08/2023 20:03 WG2089936
Acenaphthylene U 0.0295 0.210 5 07/08/2023 20:03 WG2089936
Anthracene U 0.0374 0.210 5 07/08/2023 20:03 WG2089936
Benzidine U 0.394 10.5 5 07/08/2023 20:03 WG2089936
Benzo(a)anthracene U 0.0369 0.210 5 07/08/2023 20:03 WG2089936
Benzo(b)fluoranthene U 0.0392 0.210 5 07/08/2023 20:03 WG2089936
Benzo(k)fluoranthene U 0.0373 0.210 5 07/08/2023 20:03 WG2089936
Benzo(g,h,i)perylene U 0.0384 0.210 5 07/08/2023 20:03 WG2089936
Benzo(a)pyrene U 0.0389 0.210 5 07/08/2023 20:03 WG2089936
Bis(2-chlorethoxy)methane U 0.0630 2.10 5 07/08/2023 20:03 WG2089936
Bis(2-chloroethyl)ether U 0.0693 2.10 5 07/08/2023 20:03 WG2089936
2,2-Oxybis(1-Chloropropane) U 0.0907 2.10 5 07/08/2023 20:03 WG2089936
4-Bromophenyl-phenylether U 0.0737 2.10 5 07/08/2023 20:03 WG2089936
2-Chloronaphthalene U 0.0369 0.210 5 07/08/2023 20:03 WG2089936
4-Chlorophenyl-phenylether U 0.0731 2.10 5 07/08/2023 20:03 WG2089936
Chrysene U 0.0417 0.210 5 07/08/2023 20:03 WG2089936
Dibenz(a,h)anthracene U 0.0582 0.210 5 07/08/2023 20:03 WG2089936
1,2-Dichlorobenzene U 0.0623 2.10 5 07/08/2023 20:03 WG2089936
1,3-Dichlorobenzene U 0.0636 2.10 5 07/08/2023 20:03 WG2089936
1,4-Dichlorobenzene U 0.0625 2.10 5 07/08/2023 20:03 WG2089936
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1631472
ST-CS-COMP
Collected date/time: 06/29/23 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
3,3-Dichlorobenzidine U 0.0775 2.10 5 07/08/2023 20:03 WG2089936
2,4-Dinitrotoluene U 0.0602 2.10 5 07/08/2023 20:03 WG2089936
2,6-Dinitrotoluene U 0.0687 2.10 5 07/08/2023 20:03 WG2089936
Fluoranthene U 0.0379 0.210 5 07/08/2023 20:03 WG2089936
Fluorene U 0.0342 0.210 5 07/08/2023 20:03 WG2089936
Hexachlorobenzene U 0.0744 2.10 5 07/08/2023 20:03 WG2089936
Hexachloro-1,3-butadiene U 0.0706 2.10 5 07/08/2023 20:03 WG2089936
Hexachlorocyclopentadiene U 0.110 2.10 5 07/08/2023 20:03 WG2089936
Hexachloroethane U 0.0825 2.10 5 07/08/2023 20:03 WG2089936
Indeno(1,2,3-cd)pyrene U 0.0594 0.210 5 07/08/2023 20:03 WG2089936
Isophorone U 0.0643 2.10 5 07/08/2023 20:03 WG2089936
Naphthalene U 0.0527 0.210 5 07/08/2023 20:03 WG2089936
Nitrobenzene U 0.0731 2.10 5 07/08/2023 20:03 WG2089936
n-Nitrosodimethylamine U 0.311 2.10 5 07/08/2023 20:03 WG2089936
n-Nitrosodiphenylamine U 0.159 2.10 5 07/08/2023 20:03 WG2089936
n-Nitrosodi-n-propylamine U 0.0699 2.10 5 07/08/2023 20:03 WG2089936
Phenanthrene U 0.0417 0.210 5 07/08/2023 20:03 WG2089936
Benzylbutyl phthalate U 0.0655 2.10 5 07/08/2023 20:03 WG2089936
Bis(2-ethylhexyl)phthalate U 0.266 2.10 5 07/08/2023 20:03 WG2089936
Di-n-butyl phthalate U 0.0718 2.10 5 07/08/2023 20:03 WG2089936
Diethyl phthalate U 0.0693 2.10 5 07/08/2023 20:03 WG2089936
Dimethyl phthalate U 0.445 2.10 5 07/08/2023 20:03 WG2089936
Di-n-octyl phthalate U 0.142 2.10 5 07/08/2023 20:03 WG2089936
Pyrene U 0.0408 0.210 5 07/08/2023 20:03 WG2089936
1,2,4-Trichlorobenzene U 0.0655 2.10 5 07/08/2023 20:03 WG2089936
4-Chloro-3-methylphenol U 0.0680 2.10 5 07/08/2023 20:03 WG2089936
2-Chlorophenol U 0.0693 2.10 5 07/08/2023 20:03 WG2089936
2,4-Dichlorophenol U 0.0611 2.10 5 07/08/2023 20:03 WG2089936
2,4-Dimethylphenol U 0.0548 2.10 5 07/08/2023 20:03 WG2089936
4,6-Dinitro-2-methylphenol U 0.476 2.10 5 07/08/2023 20:03 WG2089936
2,4-Dinitrophenol U 0.490 2.10 5 07/08/2023 20:03 WG2089936
2-Nitrophenol U 0.0750 2.10 5 07/08/2023 20:03 WG2089936
4-Nitrophenol U 0.0655 2.10 5 07/08/2023 20:03 WG2089936
Pentachlorophenol U 0.0565 2.10 5 07/08/2023 20:03 WG2089936
Phenol U 0.0844 2.10 5 07/08/2023 20:03 WG2089936
2,4,6-Trichlorophenol U 0.0674 2.10 5 07/08/2023 20:03 WG2089936
(S) 2-Fluorophenol 57.3 12.0-120 07/08/2023 20:03 WG2089936
(S) Phenol-d5 52.6 10.0-120 07/08/2023 20:03 WG2089936
(S) Nitrobenzene-d5 53.3 10.0-122 07/08/2023 20:03 WG2089936
(S) 2-Fluorobiphenyl 55.5 15.0-120 07/08/2023 20:03 WG2089936
(S) 2,4,6-Tribromophenol 68.2 10.0-127 07/08/2023 20:03 WG2089936
(S) p-Terphenyl-d14 63.6 10.0-120 07/08/2023 20:03 WG2089936
Sample Narrative:
L1631472-09 WG2089936: Dilution due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Anthracene U 0.00290 0.00756 1 07/10/2023 20:41 WG2091526
Acenaphthene 0.00316 J 0.00263 0.00756 1 07/10/2023 20:41 WG2091526
Acenaphthylene U 0.00272 0.00756 1 07/10/2023 20:41 WG2091526
Benzo(a)anthracene 0.00635 J 0.00218 0.00756 1 07/10/2023 20:41 WG2091526
Benzo(a)pyrene 0.00644 J 0.00226 0.00756 1 07/10/2023 20:41 WG2091526
Benzo(b)fluoranthene 0.00590 J 0.00193 0.00756 1 07/10/2023 20:41 WG2091526
Benzo(g,h,i)perylene 0.00459 J 0.00223 0.00756 1 07/10/2023 20:41 WG2091526
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 09
L1631472
ST-CS-COMP
Collected date/time: 06/29/23 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Benzo(k)fluoranthene U 0.00271 0.00756 1 07/10/2023 20:41 WG2091526
Chrysene 0.00591 J 0.00292 0.00756 1 07/10/2023 20:41 WG2091526
Dibenz(a,h)anthracene U 0.00217 0.00756 1 07/10/2023 20:41 WG2091526
Fluoranthene 0.0141 0.00286 0.00756 1 07/10/2023 20:41 WG2091526
Fluorene U 0.00258 0.00756 1 07/10/2023 20:41 WG2091526
Indeno(1,2,3-cd)pyrene 0.00340 J 0.00228 0.00756 1 07/10/2023 20:41 WG2091526
Naphthalene U 0.00514 0.0252 1 07/10/2023 20:41 WG2091526
Phenanthrene 0.0110 0.00291 0.00756 1 07/10/2023 20:41 WG2091526
Pyrene 0.0141 0.00252 0.00756 1 07/10/2023 20:41 WG2091526
1-Methylnaphthalene 0.00929 J 0.00566 0.0252 1 07/10/2023 20:41 WG2091526
2-Methylnaphthalene 0.0152 J 0.00538 0.0252 1 07/10/2023 20:41 WG2091526
2-Chloronaphthalene U 0.00587 0.0252 1 07/10/2023 20:41 WG2091526
(S) p-Terphenyl-d14 68.7 23.0-120 07/10/2023 20:41 WG2091526
(S) Nitrobenzene-d5 78.3 14.0-149 07/10/2023 20:41 WG2091526
(S) 2-Fluorobiphenyl 68.5 34.0-125 07/10/2023 20:41 WG2091526
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089245
Total Solids by Method 2540 G-2011 L1631472-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3945190-1 07/05/23 11:15
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1631439-30 Original Sample (OS) • Duplicate (DUP)
(OS) L1631439-30 07/05/23 11:15 • (DUP) R3945190-3 07/05/23 11:15
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 92.6 91.0 1 1.80 10
Laboratory Control Sample (LCS)
(LCS) R3945190-2 07/05/23 11:15
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2090723
Volatile Organic Compounds (GC) by Method 8015D/GRO L1631472-01,02,03,05,07,08,09
Method Blank (MB)
(MB) R3947676-2 07/07/23 12:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)96.8 77.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3947676-1 07/07/23 11:05 • (LCSD) R3947676-3 07/07/23 14:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.50 4.46 4.73 81.1 86.0 72.0-127 5.88 20
(S)
a,a,a-Trifluorotoluene(FID) 106 108 77.0-120
L1631472-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-08 07/07/23 21:26 • (MS) R3947676-4 07/08/23 01:13 • (MSD) R3947676-5 07/08/23 01:41
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 193 U 110 158 57.3 81.9 25 10.0-151 J3 35.4 28
(S)
a,a,a-Trifluorotoluene(FID) 103 107 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2093590
Volatile Organic Compounds (GC) by Method 8015D/GRO L1631472-06
Method Blank (MB)
(MB) R3947958-2 07/12/23 15:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 1.65 J 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)90.8 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3947958-1 07/12/23 13:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 6.09 111 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 97.7 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2093889
Volatile Organic Compounds (GC) by Method 8015D/GRO L1631472-04
Method Blank (MB)
(MB) R3948336-3 07/13/23 03:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.0428 J 0.0217 0.100
(S)
a,a,a-Trifluorotoluene(FID)91.0 77.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3948336-1 07/13/23 01:23 • (LCSD) R3948336-2 07/13/23 01:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.50 6.41 6.29 117 114 72.0-127 1.89 20
(S)
a,a,a-Trifluorotoluene(FID) 96.1 96.9 77.0-120
L1631472-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-04 07/13/23 11:26 • (MS) R3948336-4 07/13/23 11:51 • (MSD) R3948336-5 07/13/23 12:16
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 173 1.50 191 185 110 106 25 10.0-151 3.23 28
(S)
a,a,a-Trifluorotoluene(FID) 95.2 94.1 77.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2090578
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-01,02,03,05,07,08,09
Method Blank (MB)
(MB) R3946116-2 07/06/23 22:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2090578
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-01,02,03,05,07,08,09
Method Blank (MB)
(MB) R3946116-2 07/06/23 22:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 112 75.0-131
(S) 4-Bromofluorobenzene 81.8 67.0-138
(S) 1,2-Dichloroethane-d4 88.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3946116-1 07/06/23 21:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.740 118 10.0-160
Acrylonitrile 0.625 0.612 97.9 45.0-153
Benzene 0.125 0.118 94.4 70.0-123
Bromobenzene 0.125 0.111 88.8 73.0-121
Bromodichloromethane 0.125 0.116 92.8 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2090578
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-01,02,03,05,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3946116-1 07/06/23 21:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.113 90.4 64.0-132
Bromomethane 0.125 0.152 122 56.0-147
n-Butylbenzene 0.125 0.103 82.4 68.0-135
sec-Butylbenzene 0.125 0.105 84.0 74.0-130
tert-Butylbenzene 0.125 0.125 100 75.0-127
Carbon tetrachloride 0.125 0.113 90.4 66.0-128
Chlorobenzene 0.125 0.106 84.8 76.0-128
Chlorodibromomethane 0.125 0.107 85.6 74.0-127
Chloroethane 0.125 0.137 110 61.0-134
Chloroform 0.125 0.111 88.8 72.0-123
Chloromethane 0.125 0.103 82.4 51.0-138
2-Chlorotoluene 0.125 0.107 85.6 75.0-124
4-Chlorotoluene 0.125 0.109 87.2 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.0877 70.2 59.0-130
1,2-Dibromoethane 0.125 0.103 82.4 74.0-128
Dibromomethane 0.125 0.118 94.4 75.0-122
1,2-Dichlorobenzene 0.125 0.106 84.8 76.0-124
1,3-Dichlorobenzene 0.125 0.112 89.6 76.0-125
1,4-Dichlorobenzene 0.125 0.106 84.8 77.0-121
Dichlorodifluoromethane 0.125 0.101 80.8 43.0-156
1,1-Dichloroethane 0.125 0.116 92.8 70.0-127
1,2-Dichloroethane 0.125 0.121 96.8 65.0-131
1,1-Dichloroethene 0.125 0.116 92.8 65.0-131
cis-1,2-Dichloroethene 0.125 0.104 83.2 73.0-125
trans-1,2-Dichloroethene 0.125 0.107 85.6 71.0-125
1,2-Dichloropropane 0.125 0.119 95.2 74.0-125
1,1-Dichloropropene 0.125 0.116 92.8 73.0-125
1,3-Dichloropropane 0.125 0.109 87.2 80.0-125
cis-1,3-Dichloropropene 0.125 0.121 96.8 76.0-127
trans-1,3-Dichloropropene 0.125 0.117 93.6 73.0-127
2,2-Dichloropropane 0.125 0.130 104 59.0-135
Di-isopropyl ether 0.125 0.123 98.4 60.0-136
Ethylbenzene 0.125 0.104 83.2 74.0-126
Hexachloro-1,3-butadiene 0.125 0.109 87.2 57.0-150
Isopropylbenzene 0.125 0.103 82.4 72.0-127
p-Isopropyltoluene 0.125 0.105 84.0 72.0-133
2-Butanone (MEK)0.625 0.639 102 30.0-160
Methylene Chloride 0.125 0.105 84.0 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.601 96.2 56.0-143
Methyl tert-butyl ether 0.125 0.107 85.6 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2090578
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-01,02,03,05,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3946116-1 07/06/23 21:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.0691 55.3 59.0-130 J4
n-Propylbenzene 0.125 0.105 84.0 74.0-126
Styrene 0.125 0.102 81.6 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.107 85.6 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.107 85.6 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.111 88.8 61.0-139
Tetrachloroethene 0.125 0.117 93.6 70.0-136
Toluene 0.125 0.118 94.4 75.0-121
1,2,3-Trichlorobenzene 0.125 0.0760 60.8 59.0-139
1,2,4-Trichlorobenzene 0.125 0.0861 68.9 62.0-137
1,1,1-Trichloroethane 0.125 0.109 87.2 69.0-126
1,1,2-Trichloroethane 0.125 0.114 91.2 78.0-123
Trichloroethene 0.125 0.104 83.2 76.0-126
Trichlorofluoromethane 0.125 0.148 118 61.0-142
1,2,3-Trichloropropane 0.125 0.116 92.8 67.0-129
1,2,4-Trimethylbenzene 0.125 0.102 81.6 70.0-126
1,2,3-Trimethylbenzene 0.125 0.104 83.2 74.0-124
1,3,5-Trimethylbenzene 0.125 0.110 88.0 73.0-127
Vinyl chloride 0.125 0.133 106 63.0-134
Xylenes, Total 0.375 0.303 80.8 72.0-127
(S) Toluene-d8 98.4 75.0-131
(S) 4-Bromofluorobenzene 91.5 67.0-138
(S) 1,2-Dichloroethane-d4 104 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091079
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-04,06
Method Blank (MB)
(MB) R3946707-2 07/08/23 09:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091079
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-04,06
Method Blank (MB)
(MB) R3946707-2 07/08/23 09:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 105 75.0-131
(S) 4-Bromofluorobenzene 95.3 67.0-138
(S) 1,2-Dichloroethane-d4 97.9 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3946707-1 07/08/23 08:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.618 98.9 10.0-160
Acrylonitrile 0.625 0.550 88.0 45.0-153
Benzene 0.125 0.106 84.8 70.0-123
Bromobenzene 0.125 0.112 89.6 73.0-121
Bromodichloromethane 0.125 0.102 81.6 73.0-121
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091079
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-04,06
Laboratory Control Sample (LCS)
(LCS) R3946707-1 07/08/23 08:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.103 82.4 64.0-132
Bromomethane 0.125 0.0877 70.2 56.0-147
n-Butylbenzene 0.125 0.110 88.0 68.0-135
sec-Butylbenzene 0.125 0.118 94.4 74.0-130
tert-Butylbenzene 0.125 0.118 94.4 75.0-127
Carbon tetrachloride 0.125 0.107 85.6 66.0-128
Chlorobenzene 0.125 0.103 82.4 76.0-128
Chlorodibromomethane 0.125 0.108 86.4 74.0-127
Chloroethane 0.125 0.103 82.4 61.0-134
Chloroform 0.125 0.103 82.4 72.0-123
Chloromethane 0.125 0.0929 74.3 51.0-138
2-Chlorotoluene 0.125 0.112 89.6 75.0-124
4-Chlorotoluene 0.125 0.121 96.8 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.107 85.6 59.0-130
1,2-Dibromoethane 0.125 0.107 85.6 74.0-128
Dibromomethane 0.125 0.104 83.2 75.0-122
1,2-Dichlorobenzene 0.125 0.110 88.0 76.0-124
1,3-Dichlorobenzene 0.125 0.110 88.0 76.0-125
1,4-Dichlorobenzene 0.125 0.114 91.2 77.0-121
Dichlorodifluoromethane 0.125 0.107 85.6 43.0-156
1,1-Dichloroethane 0.125 0.107 85.6 70.0-127
1,2-Dichloroethane 0.125 0.118 94.4 65.0-131
1,1-Dichloroethene 0.125 0.105 84.0 65.0-131
cis-1,2-Dichloroethene 0.125 0.0967 77.4 73.0-125
trans-1,2-Dichloroethene 0.125 0.0995 79.6 71.0-125
1,2-Dichloropropane 0.125 0.0957 76.6 74.0-125
1,1-Dichloropropene 0.125 0.106 84.8 73.0-125
1,3-Dichloropropane 0.125 0.114 91.2 80.0-125
cis-1,3-Dichloropropene 0.125 0.102 81.6 76.0-127
trans-1,3-Dichloropropene 0.125 0.108 86.4 73.0-127
2,2-Dichloropropane 0.125 0.102 81.6 59.0-135
Di-isopropyl ether 0.125 0.105 84.0 60.0-136
Ethylbenzene 0.125 0.108 86.4 74.0-126
Hexachloro-1,3-butadiene 0.125 0.119 95.2 57.0-150
Isopropylbenzene 0.125 0.108 86.4 72.0-127
p-Isopropyltoluene 0.125 0.111 88.8 72.0-133
2-Butanone (MEK)0.625 0.556 89.0 30.0-160
Methylene Chloride 0.125 0.105 84.0 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.594 95.0 56.0-143
Methyl tert-butyl ether 0.125 0.105 84.0 66.0-132
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091079
Volatile Organic Compounds (GC/MS) by Method 8260B L1631472-04,06
Laboratory Control Sample (LCS)
(LCS) R3946707-1 07/08/23 08:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.104 83.2 59.0-130
n-Propylbenzene 0.125 0.122 97.6 74.0-126
Styrene 0.125 0.107 85.6 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.103 82.4 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.126 101 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.115 92.0 61.0-139
Tetrachloroethene 0.125 0.107 85.6 70.0-136
Toluene 0.125 0.105 84.0 75.0-121
1,2,3-Trichlorobenzene 0.125 0.0987 79.0 59.0-139
1,2,4-Trichlorobenzene 0.125 0.110 88.0 62.0-137
1,1,1-Trichloroethane 0.125 0.104 83.2 69.0-126
1,1,2-Trichloroethane 0.125 0.104 83.2 78.0-123
Trichloroethene 0.125 0.102 81.6 76.0-126
Trichlorofluoromethane 0.125 0.113 90.4 61.0-142
1,2,3-Trichloropropane 0.125 0.121 96.8 67.0-129
1,2,4-Trimethylbenzene 0.125 0.113 90.4 70.0-126
1,2,3-Trimethylbenzene 0.125 0.116 92.8 74.0-124
1,3,5-Trimethylbenzene 0.125 0.115 92.0 73.0-127
Vinyl chloride 0.125 0.104 83.2 63.0-134
Xylenes, Total 0.375 0.305 81.3 72.0-127
(S) Toluene-d8 102 75.0-131
(S) 4-Bromofluorobenzene 99.7 67.0-138
(S) 1,2-Dichloroethane-d4 103 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091569
Semi-Volatile Organic Compounds (GC) by Method 8015 L1631472-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3947185-1 07/11/23 09:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 75.7 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3947185-2 07/11/23 09:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) High Fraction 50.0 34.5 69.0 50.0-150
(S) o-Terphenyl 72.2 18.0-148
L1631472-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-04 07/12/23 03:35 • (MS) R3947185-3 07/12/23 03:51 • (MSD) R3947185-4 07/12/23 04:07
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 61.0 51.9 151 143 162 151 20 50.0-150 J5 J5 5.04 20
(S) o-Terphenyl 72.6 100 18.0-148 J7 J7
Sample Narrative:
OS: Cannot run at lower dilution due to viscosity of extract
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-01
Method Blank (MB)
(MB) R3945687-2 07/06/23 15:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
1,2-Dichlorobenzene U 0.00987 0.333
1,3-Dichlorobenzene U 0.0101 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-01
Method Blank (MB)
(MB) R3945687-2 07/06/23 15:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 59.9 12.0-120
(S) Phenol-d5 55.1 10.0-120
(S) Nitrobenzene-d5 51.1 10.0-122
(S) 2-Fluorobiphenyl 52.6 15.0-120
(S) 2,4,6-Tribromophenol 55.9 10.0-127
(S) p-Terphenyl-d14 75.7 10.0-120
Laboratory Control Sample (LCS)
(LCS) R3945687-1 07/06/23 15:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.313 47.0 38.0-120
Acenaphthylene 0.666 0.310 46.5 40.0-120
Anthracene 0.666 0.413 62.0 42.0-120
Benzidine 1.33 0.262 19.7 10.0-120
Benzo(a)anthracene 0.666 0.446 67.0 44.0-120
Benzo(b)fluoranthene 0.666 0.388 58.3 43.0-120
Benzo(k)fluoranthene 0.666 0.404 60.7 44.0-120
Benzo(g,h,i)perylene 0.666 0.410 61.6 43.0-120
Benzo(a)pyrene 0.666 0.434 65.2 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.255 38.3 20.0-120
Bis(2-chloroethyl)ether 0.666 0.279 41.9 16.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-01
Laboratory Control Sample (LCS)
(LCS) R3945687-1 07/06/23 15:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2,2-Oxybis(1-Chloropropane) 0.666 0.295 44.3 23.0-120
4-Bromophenyl-phenylether 0.666 0.403 60.5 40.0-120
2-Chloronaphthalene 0.666 0.295 44.3 35.0-120
4-Chlorophenyl-phenylether 0.666 0.344 51.7 40.0-120
Chrysene 0.666 0.425 63.8 43.0-120
Dibenz(a,h)anthracene 0.666 0.416 62.5 44.0-120
1,2-Dichlorobenzene 0.666 0.292 43.8 32.0-120
1,3-Dichlorobenzene 0.666 0.279 41.9 30.0-120
1,4-Dichlorobenzene 0.666 0.286 42.9 31.0-120
3,3-Dichlorobenzidine 1.33 0.851 64.0 28.0-120
2,4-Dinitrotoluene 0.666 0.408 61.3 45.0-120
2,6-Dinitrotoluene 0.666 0.356 53.5 42.0-120
Fluoranthene 0.666 0.428 64.3 44.0-120
Fluorene 0.666 0.337 50.6 41.0-120
Hexachlorobenzene 0.666 0.393 59.0 39.0-120
Hexachloro-1,3-butadiene 0.666 0.257 38.6 15.0-120
Hexachlorocyclopentadiene 0.666 0.299 44.9 15.0-120
Hexachloroethane 0.666 0.264 39.6 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.402 60.4 45.0-120
Isophorone 0.666 0.253 38.0 23.0-120
Naphthalene 0.666 0.251 37.7 18.0-120
Nitrobenzene 0.666 0.242 36.3 17.0-120
n-Nitrosodimethylamine 0.666 0.264 39.6 10.0-125
n-Nitrosodiphenylamine 0.666 0.385 57.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.283 42.5 26.0-120
Phenanthrene 0.666 0.393 59.0 42.0-120
Benzylbutyl phthalate 0.666 0.415 62.3 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.439 65.9 41.0-120
Di-n-butyl phthalate 0.666 0.415 62.3 43.0-120
Diethyl phthalate 0.666 0.343 51.5 43.0-120
Dimethyl phthalate 0.666 0.350 52.6 43.0-120
Di-n-octyl phthalate 0.666 0.402 60.4 40.0-120
Pyrene 0.666 0.403 60.5 41.0-120
1,2,4-Trichlorobenzene 0.666 0.255 38.3 17.0-120
4-Chloro-3-methylphenol 0.666 0.295 44.3 28.0-120
2-Chlorophenol 0.666 0.308 46.2 28.0-120
2,4-Dichlorophenol 0.666 0.283 42.5 25.0-120
2,4-Dimethylphenol 0.666 0.345 51.8 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.392 58.9 16.0-120
2,4-Dinitrophenol 0.666 0.247 37.1 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-01
Laboratory Control Sample (LCS)
(LCS) R3945687-1 07/06/23 15:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2-Nitrophenol 0.666 0.273 41.0 20.0-120
4-Nitrophenol 0.666 0.394 59.2 27.0-120
Pentachlorophenol 0.666 0.404 60.7 29.0-120
Phenol 0.666 0.310 46.5 28.0-120
2,4,6-Trichlorophenol 0.666 0.315 47.3 37.0-120
(S) 2-Fluorophenol 49.5 12.0-120
(S) Phenol-d5 45.8 10.0-120
(S) Nitrobenzene-d5 36.9 10.0-122
(S) 2-Fluorobiphenyl 44.4 15.0-120
(S) 2,4,6-Tribromophenol 64.1 10.0-127
(S) p-Terphenyl-d14 64.0 10.0-120
L1630311-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1630311-09 07/06/23 22:39 • (MS) R3945687-3 07/06/23 23:03 • (MSD) R3945687-4 07/06/23 23:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.765 U 0.198 0.292 25.9 35.7 1 18.0-120 J3 38.4 32
Acenaphthylene 0.765 U 0.201 0.291 26.3 35.5 1 25.0-120 J3 36.3 32
Anthracene 0.765 0.00738 0.265 0.386 33.7 46.3 1 22.0-120 J3 37.0 29
Benzidine 1.53 U 0.179 0.203 11.7 12.4 1 10.0-120 12.7 40
Benzo(a)anthracene 0.765 U 0.294 0.439 38.5 53.7 1 25.0-120 J3 39.5 29
Benzo(b)fluoranthene 0.765 U 0.250 0.373 32.6 45.6 1 19.0-122 J3 39.5 31
Benzo(k)fluoranthene 0.765 U 0.246 0.368 32.2 45.0 1 23.0-120 J3 39.7 30
Benzo(g,h,i)perylene 0.765 U 0.253 0.378 33.1 46.2 1 10.0-120 J3 39.4 33
Benzo(a)pyrene 0.765 U 0.280 0.419 36.6 51.2 1 24.0-120 J3 39.7 30
Bis(2-chlorethoxy)methane 0.765 U 0.188 0.265 24.6 32.4 1 10.0-120 34.0 34
Bis(2-chloroethyl)ether 0.765 U 0.194 0.286 25.4 35.0 1 10.0-120 38.2 40
2,2-Oxybis(1-Chloropropane) 0.765 U 0.194 0.296 25.4 36.1 1 10.0-120 J3 41.4 40
4-Bromophenyl-phenylether 0.765 U 0.251 0.365 32.8 44.7 1 27.0-120 J3 37.2 30
2-Chloronaphthalene 0.765 U 0.193 0.275 25.2 33.6 1 20.0-120 J3 35.1 32
4-Chlorophenyl-phenylether 0.765 U 0.212 0.312 27.8 38.2 1 24.0-120 J3 38.2 29
Chrysene 0.765 U 0.276 0.413 36.1 50.4 1 21.0-120 J3 39.6 29
Dibenz(a,h)anthracene 0.765 U 0.262 0.390 34.2 47.6 1 10.0-120 J3 39.3 32
1,2-Dichlorobenzene 0.765 U 0.189 0.277 24.8 33.9 1 10.0-120 37.7 38
1,3-Dichlorobenzene 0.765 U 0.177 0.268 23.2 32.7 1 10.0-120 J3 40.7 40
1,4-Dichlorobenzene 0.765 U 0.183 0.270 24.0 33.0 1 10.0-120 38.3 39
3,3-Dichlorobenzidine 1.53 U 0.516 0.765 33.7 46.6 1 10.0-120 J3 38.8 34
2,4-Dinitrotoluene 0.765 U 0.258 0.382 33.8 46.8 1 30.0-120 J3 38.8 31
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-01
L1630311-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1630311-09 07/06/23 22:39 • (MS) R3945687-3 07/06/23 23:03 • (MSD) R3945687-4 07/06/23 23:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
2,6-Dinitrotoluene 0.765 U 0.220 0.329 28.7 40.3 1 25.0-120 J3 40.0 31
Fluoranthene 0.765 U 0.282 0.413 36.9 50.4 1 18.0-126 J3 37.5 32
Fluorene 0.765 U 0.210 0.310 27.4 37.9 1 25.0-120 J3 38.5 30
Hexachlorobenzene 0.765 U 0.244 0.356 31.9 43.5 1 27.0-120 J3 37.4 28
Hexachloro-1,3-butadiene 0.765 U 0.174 0.251 22.7 30.7 1 10.0-120 36.4 38
Hexachlorocyclopentadiene 0.765 U 0.0764 0.130 9.98 15.9 1 10.0-120 J6 J3 52.2 40
Hexachloroethane 0.765 U 0.157 0.230 20.5 28.2 1 10.0-120 38.0 40
Indeno(1,2,3-cd)pyrene 0.765 U 0.255 0.376 33.3 46.0 1 10.0-120 J3 38.6 32
Isophorone 0.765 U 0.186 0.269 24.3 32.9 1 13.0-120 J3 36.6 34
Naphthalene 0.765 U 0.180 0.257 23.5 31.4 1 10.0-120 J3 35.4 35
Nitrobenzene 0.765 U 0.174 0.246 22.7 30.1 1 10.0-120 34.5 36
n-Nitrosodimethylamine 0.765 U 0.158 0.229 20.7 28.0 1 10.0-127 36.8 40
n-Nitrosodiphenylamine 0.765 U 0.218 0.317 28.5 38.8 1 17.0-120 J3 36.9 29
n-Nitrosodi-n-propylamine 0.765 U 0.201 0.297 26.3 36.3 1 10.0-120 J3 38.3 37
Phenanthrene 0.765 U 0.256 0.374 33.4 45.7 1 17.0-120 J3 37.5 31
Benzylbutyl phthalate 0.765 U 0.298 0.443 39.0 54.1 1 23.0-120 J3 39.1 30
Bis(2-ethylhexyl)phthalate 0.765 U 0.300 0.464 39.3 56.8 1 17.0-126 J3 42.9 30
Di-n-butyl phthalate 0.765 U 0.275 0.402 36.0 49.1 1 30.0-120 J3 37.4 29
Diethyl phthalate 0.765 U 0.205 0.309 26.8 37.8 1 26.0-120 J3 40.4 28
Dimethyl phthalate 0.765 U 0.211 0.317 27.6 38.8 1 25.0-120 J3 40.2 29
Di-n-octyl phthalate 0.765 U 0.305 0.463 39.9 56.6 1 21.0-123 J3 41.1 29
Pyrene 0.765 U 0.267 0.402 34.9 49.1 1 16.0-121 J3 40.4 32
1,2,4-Trichlorobenzene 0.765 U 0.180 0.258 23.5 31.6 1 12.0-120 35.8 37
4-Chloro-3-methylphenol 0.765 U 0.204 0.292 26.7 35.7 1 15.0-120 J3 35.5 30
2-Chlorophenol 0.765 U 0.218 0.323 28.5 39.5 1 15.0-120 J3 38.8 37
2,4-Dichlorophenol 0.765 U 0.205 0.287 26.8 35.1 1 20.0-120 J3 33.3 31
2,4-Dimethylphenol 0.765 U 0.210 0.304 27.4 37.2 1 10.0-120 J3 36.6 33
4,6-Dinitro-2-methylphenol 0.765 U 0.289 0.399 37.9 48.8 1 10.0-120 31.9 39
2,4-Dinitrophenol 0.765 U 0.215 0.277 28.1 33.9 1 10.0-121 25.5 40
2-Nitrophenol 0.765 U 0.216 0.312 28.2 38.2 1 12.0-120 36.5 39
4-Nitrophenol 0.765 U 0.267 0.423 34.9 51.8 1 10.0-137 J3 45.5 32
Pentachlorophenol 0.765 U 0.281 0.414 36.8 50.6 1 10.0-160 J3 38.2 31
Phenol 0.765 U 0.220 0.324 28.7 39.7 1 12.0-120 J3 38.6 38
2,4,6-Trichlorophenol 0.765 U 0.205 0.298 26.8 36.4 1 19.0-120 J3 36.9 32
(S) 2-Fluorophenol 30.8 42.0 12.0-120
(S) Phenol-d5 29.0 39.5 10.0-120
(S) Nitrobenzene-d5 23.9 31.9 10.0-122
(S) 2-Fluorobiphenyl 25.4 35.1 15.0-120
(S) 2,4,6-Tribromophenol 36.6 49.9 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089916
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-01
L1630311-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1630311-09 07/06/23 22:39 • (MS) R3945687-3 07/06/23 23:03 • (MSD) R3945687-4 07/06/23 23:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
(S) p-Terphenyl-d14 36.9 51.0 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3946720-2 07/08/23 14:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane) U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
1,2-Dichlorobenzene U 0.00987 0.333
1,3-Dichlorobenzene U 0.0101 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene 0.00844 J 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3946720-2 07/08/23 14:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 72.4 12.0-120
(S) Phenol-d5 64.7 10.0-120
(S) Nitrobenzene-d5 65.5 10.0-122
(S) 2-Fluorobiphenyl 70.6 15.0-120
(S) 2,4,6-Tribromophenol 82.6 10.0-127
(S) p-Terphenyl-d14 88.9 10.0-120
Laboratory Control Sample (LCS)
(LCS) R3946720-1 07/08/23 13:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.443 66.5 38.0-120
Acenaphthylene 0.666 0.440 66.1 40.0-120
Anthracene 0.666 0.471 70.7 42.0-120
Benzidine 1.33 0.491 36.9 10.0-120
Benzo(a)anthracene 0.666 0.507 76.1 44.0-120
Benzo(b)fluoranthene 0.666 0.525 78.8 43.0-120
Benzo(k)fluoranthene 0.666 0.509 76.4 44.0-120
Benzo(g,h,i)perylene 0.666 0.545 81.8 43.0-120
Benzo(a)pyrene 0.666 0.557 83.6 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.316 47.4 20.0-120
Bis(2-chloroethyl)ether 0.666 0.367 55.1 16.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3946720-1 07/08/23 13:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2,2-Oxybis(1-Chloropropane) 0.666 0.372 55.9 23.0-120
4-Bromophenyl-phenylether 0.666 0.438 65.8 40.0-120
2-Chloronaphthalene 0.666 0.387 58.1 35.0-120
4-Chlorophenyl-phenylether 0.666 0.444 66.7 40.0-120
Chrysene 0.666 0.498 74.8 43.0-120
Dibenz(a,h)anthracene 0.666 0.539 80.9 44.0-120
1,2-Dichlorobenzene 0.666 0.364 54.7 32.0-120
1,3-Dichlorobenzene 0.666 0.353 53.0 30.0-120
1,4-Dichlorobenzene 0.666 0.363 54.5 31.0-120
3,3-Dichlorobenzidine 1.33 1.12 84.2 28.0-120
2,4-Dinitrotoluene 0.666 0.549 82.4 45.0-120
2,6-Dinitrotoluene 0.666 0.497 74.6 42.0-120
Fluoranthene 0.666 0.487 73.1 44.0-120
Fluorene 0.666 0.459 68.9 41.0-120
Hexachlorobenzene 0.666 0.432 64.9 39.0-120
Hexachloro-1,3-butadiene 0.666 0.314 47.1 15.0-120
Hexachlorocyclopentadiene 0.666 0.269 40.4 15.0-120
Hexachloroethane 0.666 0.357 53.6 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.510 76.6 45.0-120
Isophorone 0.666 0.323 48.5 23.0-120
Naphthalene 0.666 0.313 47.0 18.0-120
Nitrobenzene 0.666 0.323 48.5 17.0-120
n-Nitrosodimethylamine 0.666 0.388 58.3 10.0-125
n-Nitrosodiphenylamine 0.666 0.464 69.7 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.364 54.7 26.0-120
Phenanthrene 0.666 0.455 68.3 42.0-120
Benzylbutyl phthalate 0.666 0.563 84.5 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.591 88.7 41.0-120
Di-n-butyl phthalate 0.666 0.506 76.0 43.0-120
Diethyl phthalate 0.666 0.470 70.6 43.0-120
Dimethyl phthalate 0.666 0.468 70.3 43.0-120
Di-n-octyl phthalate 0.666 0.603 90.5 40.0-120
Pyrene 0.666 0.486 73.0 41.0-120
1,2,4-Trichlorobenzene 0.666 0.315 47.3 17.0-120
4-Chloro-3-methylphenol 0.666 0.356 53.5 28.0-120
2-Chlorophenol 0.666 0.389 58.4 28.0-120
2,4-Dichlorophenol 0.666 0.338 50.8 25.0-120
2,4-Dimethylphenol 0.666 0.363 54.5 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.528 79.3 16.0-120
2,4-Dinitrophenol 0.666 0.483 72.5 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3946720-1 07/08/23 13:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2-Nitrophenol 0.666 0.391 58.7 20.0-120
4-Nitrophenol 0.666 0.539 80.9 27.0-120
Pentachlorophenol 0.666 0.467 70.1 29.0-120
Phenol 0.666 0.357 53.6 28.0-120
2,4,6-Trichlorophenol 0.666 0.430 64.6 37.0-120
(S) 2-Fluorophenol 61.9 12.0-120
(S) Phenol-d5 53.6 10.0-120
(S) Nitrobenzene-d5 48.3 10.0-122
(S) 2-Fluorobiphenyl 60.7 15.0-120
(S) 2,4,6-Tribromophenol 81.5 10.0-127
(S) p-Terphenyl-d14 72.7 10.0-120
L1631472-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-04 07/10/23 20:12 • (MS) R3947002-1 07/10/23 20:34 • (MSD) R3947002-2 07/10/23 20:55
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.810 U 0.520 0.519 64.2 63.4 2 18.0-120 0.238 32
Acenaphthylene 0.810 U 0.522 0.510 64.5 62.4 2 25.0-120 2.39 32
Anthracene 0.810 U 0.540 0.580 66.6 71.0 2 22.0-120 7.28 29
Benzidine 1.62 U U 0.431 0.000 26.4 2 10.0-120 J6 J3 200 40
Benzo(a)anthracene 0.810 U 0.585 0.615 72.3 75.2 2 25.0-120 4.94 29
Benzo(b)fluoranthene 0.810 U 0.735 0.742 90.7 90.8 2 19.0-122 1.00 31
Benzo(k)fluoranthene 0.810 U 0.668 0.690 82.5 84.4 2 23.0-120 3.27 30
Benzo(g,h,i)perylene 0.810 U 0.244 0.247 30.2 30.2 2 10.0-120 1.01 33
Benzo(a)pyrene 0.810 U 0.647 0.665 79.9 81.4 2 24.0-120 2.82 30
Bis(2-chlorethoxy)methane 0.810 U 0.349 0.388 43.1 47.4 2 10.0-120 10.4 34
Bis(2-chloroethyl)ether 0.810 U 0.353 0.322 43.6 39.4 2 10.0-120 9.14 40
2,2-Oxybis(1-Chloropropane) 0.810 U 0.378 0.426 46.6 52.1 2 10.0-120 12.0 40
4-Bromophenyl-phenylether 0.810 U 0.512 0.537 63.3 65.7 2 27.0-120 4.71 30
2-Chloronaphthalene 0.810 U 0.444 0.438 54.9 53.6 2 20.0-120 1.40 32
4-Chlorophenyl-phenylether 0.810 U 0.511 0.532 63.1 65.1 2 24.0-120 4.02 29
Chrysene 0.810 U 0.667 0.600 82.3 73.4 2 21.0-120 10.5 29
Dibenz(a,h)anthracene 0.810 U 0.331 0.336 40.9 41.1 2 10.0-120 1.48 32
1,2-Dichlorobenzene 0.810 U 0.341 0.386 42.1 47.3 2 10.0-120 12.6 38
1,3-Dichlorobenzene 0.810 U 0.314 0.370 38.7 45.3 2 10.0-120 16.6 40
1,4-Dichlorobenzene 0.810 U 0.325 0.370 40.1 45.3 2 10.0-120 13.1 39
3,3-Dichlorobenzidine 1.62 U 0.693 1.33 42.8 81.8 2 10.0-120 J3 63.3 34
2,4-Dinitrotoluene 0.810 U 0.595 0.659 73.5 80.7 2 30.0-120 10.2 31
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-02,03,04,05,06,07,08,09
L1631472-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-04 07/10/23 20:12 • (MS) R3947002-1 07/10/23 20:34 • (MSD) R3947002-2 07/10/23 20:55
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
2,6-Dinitrotoluene 0.810 U 0.551 0.582 68.0 71.1 2 25.0-120 5.45 31
Fluoranthene 0.810 U 0.564 0.603 69.7 73.7 2 18.0-126 6.56 32
Fluorene 0.810 U 0.535 0.542 66.0 66.3 2 25.0-120 1.38 30
Hexachlorobenzene 0.810 U 0.484 0.533 59.8 65.3 2 27.0-120 9.71 28
Hexachloro-1,3-butadiene 0.810 U 0.358 0.370 44.2 45.3 2 10.0-120 3.39 38
Hexachlorocyclopentadiene 0.810 U U U 1.40 1.34 2 10.0-120 J6 J6 3.32 40
Hexachloroethane 0.810 U 0.274 0.252 33.8 30.8 2 10.0-120 8.45 40
Indeno(1,2,3-cd)pyrene 0.810 U 0.267 0.299 32.9 36.6 2 10.0-120 11.4 32
Isophorone 0.810 U 0.363 0.390 44.8 47.7 2 13.0-120 7.21 34
Naphthalene 0.810 U 0.344 0.375 42.5 45.9 2 10.0-120 8.58 35
Nitrobenzene 0.810 U 0.349 0.396 43.1 48.5 2 10.0-120 12.6 36
n-Nitrosodimethylamine 0.810 U 0.389 0.464 48.0 56.8 2 10.0-127 17.7 40
n-Nitrosodiphenylamine 0.810 U 0.527 0.573 65.1 70.1 2 17.0-120 8.31 29
n-Nitrosodi-n-propylamine 0.810 U 0.404 0.428 49.8 52.4 2 10.0-120 5.93 37
Phenanthrene 0.810 U 0.535 0.563 66.0 68.9 2 17.0-120 5.17 31
Benzylbutyl phthalate 0.810 U 0.782 0.785 96.5 96.1 2 23.0-120 0.473 30
Bis(2-ethylhexyl)phthalate 0.810 U 0.777 0.793 95.9 97.0 2 17.0-126 2.05 30
Di-n-butyl phthalate 0.810 U 0.585 0.635 72.3 77.6 2 30.0-120 8.10 29
Diethyl phthalate 0.810 U 0.543 0.568 67.1 69.5 2 26.0-120 4.44 28
Dimethyl phthalate 0.810 U 0.520 0.526 64.2 64.4 2 25.0-120 1.18 29
Di-n-octyl phthalate 0.810 U 0.815 0.863 101 106 2 21.0-123 5.74 29
Pyrene 0.810 U 0.631 0.642 77.9 78.5 2 16.0-121 1.75 32
1,2,4-Trichlorobenzene 0.810 U 0.342 0.367 42.2 44.9 2 12.0-120 6.97 37
4-Chloro-3-methylphenol 0.810 U 0.500 0.522 61.7 63.9 2 15.0-120 4.35 30
2-Chlorophenol 0.810 U 0.437 0.478 54.0 58.5 2 15.0-120 8.91 37
2,4-Dichlorophenol 0.810 U 0.453 0.462 55.9 56.5 2 20.0-120 1.89 31
2,4-Dimethylphenol 0.810 U 0.478 0.468 59.0 57.3 2 10.0-120 2.09 33
4,6-Dinitro-2-methylphenol 0.810 U 0.319 0.309 39.3 37.8 2 10.0-120 3.15 39
2,4-Dinitrophenol 0.810 U U U 0.000 0.000 2 10.0-121 J6 J6 0.000 40
2-Nitrophenol 0.810 U 0.443 0.500 54.7 61.2 2 12.0-120 12.0 39
4-Nitrophenol 0.810 U 0.668 0.728 82.5 89.1 2 10.0-137 8.66 32
Pentachlorophenol 0.810 U 0.595 0.674 73.5 82.5 2 10.0-160 12.5 31
Phenol 0.810 U 0.416 0.440 51.4 53.8 2 12.0-120 5.48 38
2,4,6-Trichlorophenol 0.810 U 0.575 0.588 71.0 71.9 2 19.0-120 2.12 32
(S) 2-Fluorophenol 54.0 56.9 12.0-120
(S) Phenol-d5 50.4 51.4 10.0-120
(S) Nitrobenzene-d5 44.8 48.6 10.0-122
(S) 2-Fluorobiphenyl 54.9 50.2 15.0-120
(S) 2,4,6-Tribromophenol 77.5 78.7 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2089936
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1631472-02,03,04,05,06,07,08,09
L1631472-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-04 07/10/23 20:12 • (MS) R3947002-1 07/10/23 20:34 • (MSD) R3947002-2 07/10/23 20:55
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
(S) p-Terphenyl-d14 77.1 71.3 10.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091375
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1631472-04
Method Blank (MB)
(MB) R3947160-2 07/10/23 23:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 86.9 23.0-120
(S) Nitrobenzene-d5 86.9 14.0-149
(S) 2-Fluorobiphenyl 69.7 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3947160-1 07/10/23 23:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0790 98.8 50.0-126
Acenaphthene 0.0800 0.0733 91.6 50.0-120
Acenaphthylene 0.0800 0.0791 98.9 50.0-120
Benzo(a)anthracene 0.0800 0.0884 111 45.0-120
Benzo(a)pyrene 0.0800 0.0765 95.6 42.0-120
Benzo(b)fluoranthene 0.0800 0.0747 93.4 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0686 85.8 45.0-125
Benzo(k)fluoranthene 0.0800 0.0695 86.9 49.0-125
Chrysene 0.0800 0.0780 97.5 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0782 97.8 47.0-125
Fluoranthene 0.0800 0.0782 97.8 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091375
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1631472-04
Laboratory Control Sample (LCS)
(LCS) R3947160-1 07/10/23 23:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0763 95.4 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0895 112 46.0-125
Naphthalene 0.0800 0.0735 91.9 50.0-120
Phenanthrene 0.0800 0.0740 92.5 47.0-120
Pyrene 0.0800 0.0764 95.5 43.0-123
1-Methylnaphthalene 0.0800 0.0721 90.1 51.0-121
2-Methylnaphthalene 0.0800 0.0750 93.8 50.0-120
2-Chloronaphthalene 0.0800 0.0718 89.8 50.0-120
(S) p-Terphenyl-d14 106 23.0-120
(S) Nitrobenzene-d5 149 14.0-149
(S) 2-Fluorobiphenyl 97.6 34.0-125
L1631472-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631472-04 07/11/23 06:00 • (MS) R3947160-3 07/11/23 06:20 • (MSD) R3947160-4 07/11/23 06:40
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0963 U 0.0510 0.0757 52.9 77.8 1 10.0-145 J3 39.0 30
Acenaphthene 0.0963 U 0.0483 0.0707 50.1 72.7 1 14.0-127 J3 37.8 27
Acenaphthylene 0.0963 U 0.0528 0.0774 54.9 79.6 1 21.0-124 J3 37.7 25
Benzo(a)anthracene 0.0963 0.00420 0.0604 0.0904 58.3 88.6 1 10.0-139 J3 39.8 30
Benzo(a)pyrene 0.0963 0.00904 0.0567 0.0824 49.5 75.4 1 10.0-141 J3 36.9 31
Benzo(b)fluoranthene 0.0963 0.0172 0.0512 0.0737 35.4 58.1 1 10.0-140 36.0 36
Benzo(g,h,i)perylene 0.0963 0.0352 0.0475 0.0707 12.8 36.5 1 10.0-140 J3 39.2 33
Benzo(k)fluoranthene 0.0963 U 0.0456 0.0673 47.3 69.2 1 10.0-137 J3 38.5 31
Chrysene 0.0963 0.0117 0.0562 0.0898 46.2 80.3 1 10.0-145 J3 46.0 30
Dibenz(a,h)anthracene 0.0963 0.0117 0.0514 0.0757 41.1 65.7 1 10.0-132 J3 38.3 31
Fluoranthene 0.0963 0.00578 0.0531 0.0785 49.1 74.8 1 10.0-153 J3 38.6 33
Fluorene 0.0963 U 0.0526 0.0764 54.6 78.6 1 11.0-130 J3 36.9 29
Indeno(1,2,3-cd)pyrene 0.0963 0.00803 0.0593 0.0868 53.2 81.0 1 10.0-137 J3 37.7 32
Naphthalene 0.0963 U 0.0504 0.0700 52.3 72.0 1 10.0-135 J3 32.6 27
Phenanthrene 0.0963 0.00431 0.0486 0.0725 46.0 70.1 1 10.0-144 J3 39.3 31
Pyrene 0.0963 0.00922 0.0520 0.0761 44.4 68.7 1 10.0-148 J3 37.6 35
1-Methylnaphthalene 0.0963 U 0.0490 0.0701 50.9 72.1 1 10.0-142 J3 35.4 28
2-Methylnaphthalene 0.0963 U 0.0512 0.0727 53.2 74.7 1 10.0-137 J3 34.7 28
2-Chloronaphthalene 0.0963 U 0.0474 0.0693 49.2 71.2 1 29.0-120 J3 37.5 24
(S) p-Terphenyl-d14 67.2 81.6 23.0-120
(S) Nitrobenzene-d5 97.9 111 14.0-149
(S) 2-Fluorobiphenyl 62.2 73.2 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091376
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1631472-01,02,03,05,06,07
Method Blank (MB)
(MB) R3947455-2 07/11/23 20:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 58.0 23.0-120
(S) Nitrobenzene-d5 50.0 14.0-149
(S) 2-Fluorobiphenyl 51.3 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3947455-1 07/11/23 20:11
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0624 78.0 50.0-126
Acenaphthene 0.0800 0.0611 76.4 50.0-120
Acenaphthylene 0.0800 0.0633 79.1 50.0-120
Benzo(a)anthracene 0.0800 0.0697 87.1 45.0-120
Benzo(a)pyrene 0.0800 0.0657 82.1 42.0-120
Benzo(b)fluoranthene 0.0800 0.0648 81.0 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0620 77.5 45.0-125
Benzo(k)fluoranthene 0.0800 0.0628 78.5 49.0-125
Chrysene 0.0800 0.0648 81.0 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0632 79.0 47.0-125
Fluoranthene 0.0800 0.0655 81.9 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091376
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1631472-01,02,03,05,06,07
Laboratory Control Sample (LCS)
(LCS) R3947455-1 07/11/23 20:11
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0652 81.5 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0694 86.8 46.0-125
Naphthalene 0.0800 0.0586 73.3 50.0-120
Phenanthrene 0.0800 0.0601 75.1 47.0-120
Pyrene 0.0800 0.0638 79.8 43.0-123
1-Methylnaphthalene 0.0800 0.0611 76.4 51.0-121
2-Methylnaphthalene 0.0800 0.0627 78.4 50.0-120
2-Chloronaphthalene 0.0800 0.0578 72.3 50.0-120
(S) p-Terphenyl-d14 82.5 23.0-120
(S) Nitrobenzene-d5 70.5 14.0-149
(S) 2-Fluorobiphenyl 68.6 34.0-125
L1631443-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1631443-02 07/11/23 21:58 • (MS) R3947455-3 07/11/23 22:15 • (MSD) R3947455-4 07/11/23 22:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0792 U 0.0564 0.0652 71.2 81.9 1 10.0-145 14.5 30
Acenaphthene 0.0792 U 0.0570 0.0657 72.0 82.5 1 14.0-127 14.2 27
Acenaphthylene 0.0792 U 0.0589 0.0671 74.4 84.3 1 21.0-124 13.0 25
Benzo(a)anthracene 0.0792 U 0.0663 0.0770 83.7 96.7 1 10.0-139 14.9 30
Benzo(a)pyrene 0.0792 U 0.0709 0.0772 89.5 97.0 1 10.0-141 8.51 31
Benzo(b)fluoranthene 0.0792 U 0.0772 0.0800 97.5 101 1 10.0-140 3.56 36
Benzo(g,h,i)perylene 0.0792 U 0.0944 0.104 119 131 1 10.0-140 9.68 33
Benzo(k)fluoranthene 0.0792 U 0.0736 0.0773 92.9 97.1 1 10.0-137 4.90 31
Chrysene 0.0792 U 0.0618 0.0696 78.0 87.4 1 10.0-145 11.9 30
Dibenz(a,h)anthracene 0.0792 U 0.0785 0.0859 99.1 108 1 10.0-132 9.00 31
Fluoranthene 0.0792 U 0.0669 0.0817 84.5 103 1 10.0-153 19.9 33
Fluorene 0.0792 U 0.0640 0.0711 80.8 89.3 1 11.0-130 10.5 29
Indeno(1,2,3-cd)pyrene 0.0792 U 0.0788 0.0818 99.5 103 1 10.0-137 3.74 32
Naphthalene 0.0792 U 0.0552 0.0657 69.7 82.5 1 10.0-135 17.4 27
Phenanthrene 0.0792 U 0.0621 0.0670 78.4 84.2 1 10.0-144 7.59 31
Pyrene 0.0792 U 0.0608 0.0713 76.8 89.6 1 10.0-148 15.9 35
1-Methylnaphthalene 0.0792 U 0.0585 0.0680 73.9 85.4 1 10.0-142 15.0 28
2-Methylnaphthalene 0.0792 U 0.0625 0.0721 78.9 90.6 1 10.0-137 14.3 28
2-Chloronaphthalene 0.0792 U 0.0532 0.0618 67.2 77.6 1 29.0-120 15.0 24
(S) p-Terphenyl-d14 83.7 88.4 23.0-120
(S) Nitrobenzene-d5 93.7 105 14.0-149
(S) 2-Fluorobiphenyl 71.3 80.0 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091526
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1631472-08,09
Method Blank (MB)
(MB) R3947071-2 07/10/23 16:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 95.1 23.0-120
(S) Nitrobenzene-d5 70.0 14.0-149
(S) 2-Fluorobiphenyl 73.5 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3947071-1 07/10/23 16:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0617 77.1 50.0-126
Acenaphthene 0.0800 0.0634 79.3 50.0-120
Acenaphthylene 0.0800 0.0639 79.9 50.0-120
Benzo(a)anthracene 0.0800 0.0679 84.9 45.0-120
Benzo(a)pyrene 0.0800 0.0643 80.4 42.0-120
Benzo(b)fluoranthene 0.0800 0.0667 83.4 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0670 83.8 45.0-125
Benzo(k)fluoranthene 0.0800 0.0635 79.4 49.0-125
Chrysene 0.0800 0.0651 81.4 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0654 81.8 47.0-125
Fluoranthene 0.0800 0.0674 84.3 49.0-129
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2091526
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1631472-08,09
Laboratory Control Sample (LCS)
(LCS) R3947071-1 07/10/23 16:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0635 79.4 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0683 85.4 46.0-125
Naphthalene 0.0800 0.0596 74.5 50.0-120
Phenanthrene 0.0800 0.0600 75.0 47.0-120
Pyrene 0.0800 0.0694 86.8 43.0-123
1-Methylnaphthalene 0.0800 0.0624 78.0 51.0-121
2-Methylnaphthalene 0.0800 0.0643 80.4 50.0-120
2-Chloronaphthalene 0.0800 0.0582 72.8 50.0-120
(S) p-Terphenyl-d14 93.4 23.0-120
(S) Nitrobenzene-d5 75.4 14.0-149
(S) 2-Fluorobiphenyl 75.2 34.0-125
L1632819-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1632819-05 07/10/23 17:25 • (MS) R3947071-3 07/10/23 17:43 • (MSD) R3947071-4 07/10/23 18:01
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0893 U 0.0592 0.0535 66.3 59.6 1 10.0-145 10.1 30
Acenaphthene 0.0893 U 0.0635 0.0563 71.1 62.8 1 14.0-127 12.0 27
Acenaphthylene 0.0893 U 0.0630 0.0563 70.6 62.8 1 21.0-124 11.3 25
Benzo(a)anthracene 0.0893 U 0.0665 0.0591 74.5 65.9 1 10.0-139 11.8 30
Benzo(a)pyrene 0.0893 U 0.0677 0.0601 75.9 67.0 1 10.0-141 11.9 31
Benzo(b)fluoranthene 0.0893 U 0.0637 0.0560 71.4 62.4 1 10.0-140 12.9 36
Benzo(g,h,i)perylene 0.0893 U 0.0674 0.0566 75.5 63.1 1 10.0-140 17.4 33
Benzo(k)fluoranthene 0.0893 U 0.0610 0.0534 68.3 59.5 1 10.0-137 13.3 31
Chrysene 0.0893 U 0.0635 0.0564 71.1 62.9 1 10.0-145 11.8 30
Dibenz(a,h)anthracene 0.0893 U 0.0648 0.0557 72.6 62.1 1 10.0-132 15.1 31
Fluoranthene 0.0893 U 0.0652 0.0592 73.0 66.0 1 10.0-153 9.56 33
Fluorene 0.0893 U 0.0636 0.0563 71.2 62.8 1 11.0-130 12.2 29
Indeno(1,2,3-cd)pyrene 0.0893 U 0.0658 0.0576 73.7 64.3 1 10.0-137 13.3 32
Naphthalene 0.0893 U 0.0589 0.0523 66.0 58.3 1 10.0-135 11.9 27
Phenanthrene 0.0893 U 0.0598 0.0547 67.0 61.0 1 10.0-144 8.81 31
Pyrene 0.0893 U 0.0693 0.0611 77.6 68.1 1 10.0-148 12.6 35
1-Methylnaphthalene 0.0893 U 0.0622 0.0564 69.7 62.9 1 10.0-142 9.83 28
2-Methylnaphthalene 0.0893 U 0.0634 0.0572 71.0 63.8 1 10.0-137 10.2 28
2-Chloronaphthalene 0.0893 U 0.0585 0.0516 65.6 57.5 1 29.0-120 12.6 24
(S) p-Terphenyl-d14 77.5 71.3 23.0-120
(S) Nitrobenzene-d5 65.4 64.6 14.0-149
(S) 2-Fluorobiphenyl 65.4 61.4 34.0-125
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ANALYTICAL REPORT
July 24, 2023
Tetra Tech Inc. - UT
Sample Delivery Group:L1635984
Samples Received:07/15/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
July 24, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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July 25, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
PW-1 L1635984-01 5
Qc: Quality Control Summary 10
Total Solids by Method 2540 B-2015 10
Wet Chemistry by Method 1664A 11
Wet Chemistry by Method 3500Cr C-2011 12
Mercury by Method 7470A 13
Metals (ICP) by Method 6010B 14
Volatile Organic Compounds (GC) by Method 8015D/GRO 16
Volatile Organic Compounds (GC/MS) by Method 8260B 17
Semi-Volatile Organic Compounds (GC) by Method 8015 22
Polychlorinated Biphenyls (GC) by Method 8082 23
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 24
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 28
Gl: Glossary of Terms 30
Al: Accreditations & Locations 31
Sc: Sample Chain of Custody 32
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
PW-1 L1635984-01 GW Richie Torney 07/14/23 08:30 07/15/23 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 B-2015 WG2095809 1 07/17/23 10:19 07/17/23 11:21 MMF Mt. Juliet, TN
Wet Chemistry by Method 1664A WG2097611 1 07/19/23 15:01 07/20/23 02:04 WAW Mt. Juliet, TN
Wet Chemistry by Method 3500Cr C-2011 WG2095928 1 07/20/23 14:57 07/20/23 14:57 SJC Mt. Juliet, TN
Mercury by Method 7470A WG2098129 1 07/21/23 07:44 07/22/23 11:01 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2096555 1 07/18/23 10:02 07/23/23 00:21 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2097817 1 07/19/23 17:49 07/19/23 17:49 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2096768 1 07/18/23 13:35 07/18/23 13:35 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2097882 1 07/20/23 01:55 07/20/23 01:55 KSD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2098975 2 07/21/23 06:48 07/22/23 18:06 MAA Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method 8082 WG2097512 1 07/19/23 16:04 07/20/23 02:03 LTB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG2098169 1 07/20/23 07:08 07/20/23 22:41 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG2098168 1 07/20/23 12:36 07/20/23 21:41 AMM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1635984
PW-1
Collected date/time: 07/14/23 08:30
Total Solids by Method 2540 B-2015
Result Qualifier Dilution Analysis Batch
Analyte mg/l date / time
Total Solids 1210 1 07/17/2023 11:21 WG2095809
Wet Chemistry by Method 1664A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)ND 6.58 1 07/20/2023 02:04 WG2097611
Wet Chemistry by Method 3500Cr C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexavalent Chromium 0.00154 0.000500 1 07/20/2023 14:57 WG2095928
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 07/22/2023 11:01 WG2098129
Metals (ICP) by Method 6010B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 1 07/23/2023 00:21 WG2096555
Arsenic 0.0161 0.0100 1 07/23/2023 00:21 WG2096555
Beryllium ND 0.00200 1 07/23/2023 00:21 WG2096555
Cadmium ND 0.00200 1 07/23/2023 00:21 WG2096555
Chromium ND 0.0100 1 07/23/2023 00:21 WG2096555
Copper 0.0270 0.0100 1 07/23/2023 00:21 WG2096555
Lead 0.0355 0.00600 1 07/23/2023 00:21 WG2096555
Nickel ND 0.0100 1 07/23/2023 00:21 WG2096555
Selenium 0.0168 B 0.0100 1 07/23/2023 00:21 WG2096555
Silver ND 0.00500 1 07/23/2023 00:21 WG2096555
Thallium ND 0.0100 1 07/23/2023 00:21 WG2096555
Zinc ND 0.0500 1 07/23/2023 00:21 WG2096555
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
TPH (GC/FID) Low Fraction ND 0.100 1 07/19/2023 17:49 WG2097817
(S) a,a,a-Trifluorotoluene(FID) 106 78.0-120 07/19/2023 17:49 WG2097817
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 07/18/2023 13:35 WG2096768
Acrolein ND 0.0500 1 07/18/2023 13:35 WG2096768
Acrylonitrile ND 0.0100 1 07/18/2023 13:35 WG2096768
Benzene ND 0.00100 1 07/18/2023 13:35 WG2096768
Bromobenzene ND J3 0.00100 1 07/18/2023 13:35 WG2096768
Bromodichloromethane ND 0.00100 1 07/18/2023 13:35 WG2096768
Bromoform ND 0.00100 1 07/18/2023 13:35 WG2096768
Bromomethane ND 0.00500 1 07/18/2023 13:35 WG2096768
n-Butylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
sec-Butylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
tert-Butylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1635984
PW-1
Collected date/time: 07/14/23 08:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Carbon tetrachloride ND 0.00100 1 07/18/2023 13:35 WG2096768
Chlorobenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
Chlorodibromomethane ND 0.00100 1 07/18/2023 13:35 WG2096768
Chloroethane ND J4 0.00500 1 07/18/2023 13:35 WG2096768
Chloroform ND 0.00500 1 07/18/2023 13:35 WG2096768
Chloromethane ND 0.00250 1 07/18/2023 13:35 WG2096768
2-Chlorotoluene ND 0.00100 1 07/18/2023 13:35 WG2096768
4-Chlorotoluene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2-Dibromo-3-Chloropropane ND J3 0.00500 1 07/18/2023 13:35 WG2096768
1,2-Dibromoethane ND 0.00100 1 07/18/2023 13:35 WG2096768
Dibromomethane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2-Dichlorobenzene ND J3 0.00100 1 07/18/2023 13:35 WG2096768
1,3-Dichlorobenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,4-Dichlorobenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
Dichlorodifluoromethane ND 0.00500 1 07/18/2023 13:35 WG2096768
1,1-Dichloroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2-Dichloroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1-Dichloroethene ND 0.00100 1 07/18/2023 13:35 WG2096768
cis-1,2-Dichloroethene ND 0.00100 1 07/18/2023 13:35 WG2096768
trans-1,2-Dichloroethene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2-Dichloropropane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1-Dichloropropene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,3-Dichloropropane ND 0.00100 1 07/18/2023 13:35 WG2096768
cis-1,3-Dichloropropene ND 0.00100 1 07/18/2023 13:35 WG2096768
trans-1,3-Dichloropropene ND 0.00100 1 07/18/2023 13:35 WG2096768
2,2-Dichloropropane ND 0.00100 1 07/18/2023 13:35 WG2096768
Di-isopropyl ether ND 0.00100 1 07/18/2023 13:35 WG2096768
Ethylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
Hexachloro-1,3-butadiene ND 0.00100 1 07/18/2023 13:35 WG2096768
Isopropylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
p-Isopropyltoluene ND 0.00100 1 07/18/2023 13:35 WG2096768
2-Butanone (MEK)ND 0.0100 1 07/18/2023 13:35 WG2096768
Methylene Chloride ND 0.00500 1 07/18/2023 13:35 WG2096768
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 07/18/2023 13:35 WG2096768
Methyl tert-butyl ether ND 0.00100 1 07/20/2023 01:55 WG2097882
Naphthalene ND 0.00500 1 07/18/2023 13:35 WG2096768
n-Propylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
Styrene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1,1,2-Tetrachloroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1,2,2-Tetrachloroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
Tetrachloroethene ND 0.00100 1 07/18/2023 13:35 WG2096768
Toluene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2,3-Trichlorobenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2,4-Trichlorobenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1,1-Trichloroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
1,1,2-Trichloroethane ND 0.00100 1 07/18/2023 13:35 WG2096768
Trichloroethene ND 0.00100 1 07/18/2023 13:35 WG2096768
Trichlorofluoromethane ND J4 0.00500 1 07/18/2023 13:35 WG2096768
1,2,3-Trichloropropane ND J3 0.00250 1 07/18/2023 13:35 WG2096768
1,2,4-Trimethylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,2,3-Trimethylbenzene ND 0.00100 1 07/18/2023 13:35 WG2096768
1,3,5-Trimethylbenzene ND J3 0.00100 1 07/18/2023 13:35 WG2096768
Vinyl chloride ND 0.00100 1 07/18/2023 13:35 WG2096768
Xylenes, Total ND 0.00300 1 07/18/2023 13:35 WG2096768
(S) Toluene-d8 103 80.0-120 07/18/2023 13:35 WG2096768
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1635984
PW-1
Collected date/time: 07/14/23 08:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
(S) Toluene-d8 101 80.0-120 07/20/2023 01:55 WG2097882
(S) 4-Bromofluorobenzene 102 77.0-126 07/18/2023 13:35 WG2096768
(S) 4-Bromofluorobenzene 97.6 77.0-126 07/20/2023 01:55 WG2097882
(S) 1,2-Dichloroethane-d4 109 70.0-130 07/18/2023 13:35 WG2096768
(S) 1,2-Dichloroethane-d4 117 70.0-130 07/20/2023 01:55 WG2097882
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
C10-C28 Diesel Range ND 0.200 2 07/22/2023 18:06 WG2098975
C28-C40 Oil Range 0.543 0.200 2 07/22/2023 18:06 WG2098975
(S) o-Terphenyl 77.4 52.0-156 07/22/2023 18:06 WG2098975
Polychlorinated Biphenyls (GC) by Method 8082
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
PCB 1016 ND 0.000500 1 07/20/2023 02:03 WG2097512
PCB 1221 ND 0.000500 1 07/20/2023 02:03 WG2097512
PCB 1232 ND 0.000500 1 07/20/2023 02:03 WG2097512
PCB 1242 ND 0.000500 1 07/20/2023 02:03 WG2097512
PCB 1248 ND 0.000500 1 07/20/2023 02:03 WG2097512
PCB 1254 ND 0.000500 1 07/20/2023 02:03 WG2097512
PCB 1260 ND 0.000500 1 07/20/2023 02:03 WG2097512
(S) Decachlorobiphenyl 42.4 10.0-128 07/20/2023 02:03 WG2097512
(S) Tetrachloro-m-xylene 65.3 10.0-127 07/20/2023 02:03 WG2097512
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 07/20/2023 22:41 WG2098169
Acenaphthylene ND 0.00100 1 07/20/2023 22:41 WG2098169
Anthracene ND 0.00100 1 07/20/2023 22:41 WG2098169
Benzidine ND J4 0.0100 1 07/20/2023 22:41 WG2098169
Benzo(a)anthracene ND 0.00100 1 07/20/2023 22:41 WG2098169
Benzo(b)fluoranthene ND 0.00100 1 07/20/2023 22:41 WG2098169
Benzo(k)fluoranthene ND 0.00100 1 07/20/2023 22:41 WG2098169
Benzo(g,h,i)perylene ND 0.00100 1 07/20/2023 22:41 WG2098169
Benzo(a)pyrene ND 0.00100 1 07/20/2023 22:41 WG2098169
Bis(2-chlorethoxy)methane ND 0.0100 1 07/20/2023 22:41 WG2098169
Bis(2-chloroethyl)ether ND 0.0100 1 07/20/2023 22:41 WG2098169
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 07/20/2023 22:41 WG2098169
4-Bromophenyl-phenylether ND 0.0100 1 07/20/2023 22:41 WG2098169
2-Chloronaphthalene ND 0.00100 1 07/20/2023 22:41 WG2098169
4-Chlorophenyl-phenylether ND 0.0100 1 07/20/2023 22:41 WG2098169
Chrysene ND 0.00100 1 07/20/2023 22:41 WG2098169
Dibenz(a,h)anthracene ND 0.00100 1 07/20/2023 22:41 WG2098169
1,2-Dichlorobenzene ND 0.0100 1 07/20/2023 22:41 WG2098169
1,3-Dichlorobenzene ND 0.0100 1 07/20/2023 22:41 WG2098169
1,4-Dichlorobenzene ND 0.0100 1 07/20/2023 22:41 WG2098169
3,3-Dichlorobenzidine ND 0.0100 1 07/20/2023 22:41 WG2098169
2,4-Dinitrotoluene ND 0.0100 1 07/20/2023 22:41 WG2098169
2,6-Dinitrotoluene ND 0.0100 1 07/20/2023 22:41 WG2098169
Fluoranthene ND 0.00100 1 07/20/2023 22:41 WG2098169
Fluorene ND 0.00100 1 07/20/2023 22:41 WG2098169
Hexachlorobenzene ND 0.00100 1 07/20/2023 22:41 WG2098169
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1635984
PW-1
Collected date/time: 07/14/23 08:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Hexachloro-1,3-butadiene ND 0.0100 1 07/20/2023 22:41 WG2098169
Hexachlorocyclopentadiene ND 0.0100 1 07/20/2023 22:41 WG2098169
Hexachloroethane ND 0.0100 1 07/20/2023 22:41 WG2098169
Indeno(1,2,3-cd)pyrene ND 0.00100 1 07/20/2023 22:41 WG2098169
Isophorone ND 0.0100 1 07/20/2023 22:41 WG2098169
Naphthalene ND 0.00100 1 07/20/2023 22:41 WG2098169
Nitrobenzene ND 0.0100 1 07/20/2023 22:41 WG2098169
n-Nitrosodimethylamine ND 0.0100 1 07/20/2023 22:41 WG2098169
n-Nitrosodiphenylamine ND 0.0100 1 07/20/2023 22:41 WG2098169
n-Nitrosodi-n-propylamine ND 0.0100 1 07/20/2023 22:41 WG2098169
Phenanthrene ND 0.00100 1 07/20/2023 22:41 WG2098169
Benzylbutyl phthalate ND 0.00300 1 07/20/2023 22:41 WG2098169
Bis(2-ethylhexyl)phthalate ND 0.00300 1 07/20/2023 22:41 WG2098169
Di-n-butyl phthalate ND 0.00300 1 07/20/2023 22:41 WG2098169
Diethyl phthalate ND 0.00300 1 07/20/2023 22:41 WG2098169
Dimethyl phthalate ND 0.00300 1 07/20/2023 22:41 WG2098169
Di-n-octyl phthalate ND 0.00300 1 07/20/2023 22:41 WG2098169
Pyrene ND 0.00100 1 07/20/2023 22:41 WG2098169
1,2,4-Trichlorobenzene ND 0.0100 1 07/20/2023 22:41 WG2098169
4-Chloro-3-methylphenol ND 0.0100 1 07/20/2023 22:41 WG2098169
2-Chlorophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
2,4-Dichlorophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
2,4-Dimethylphenol ND 0.0100 1 07/20/2023 22:41 WG2098169
4,6-Dinitro-2-methylphenol ND 0.0100 1 07/20/2023 22:41 WG2098169
2,4-Dinitrophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
2-Nitrophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
4-Nitrophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
Pentachlorophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
Phenol ND 0.0100 1 07/20/2023 22:41 WG2098169
2,4,6-Trichlorophenol ND 0.0100 1 07/20/2023 22:41 WG2098169
(S) 2-Fluorophenol 17.5 10.0-120 07/20/2023 22:41 WG2098169
(S) Phenol-d5 10.9 10.0-120 07/20/2023 22:41 WG2098169
(S) Nitrobenzene-d5 48.2 10.0-127 07/20/2023 22:41 WG2098169
(S) 2-Fluorobiphenyl 46.2 10.0-130 07/20/2023 22:41 WG2098169
(S) 2,4,6-Tribromophenol 56.6 10.0-155 07/20/2023 22:41 WG2098169
(S) p-Terphenyl-d14 56.4 10.0-128 07/20/2023 22:41 WG2098169
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Anthracene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Acenaphthene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Acenaphthylene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Benzo(a)anthracene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Benzo(a)pyrene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Benzo(b)fluoranthene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Benzo(g,h,i)perylene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Benzo(k)fluoranthene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Chrysene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Dibenz(a,h)anthracene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Fluoranthene ND 0.000100 1 07/20/2023 21:41 WG2098168
Fluorene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Indeno(1,2,3-cd)pyrene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Naphthalene ND 0.000250 1 07/20/2023 21:41 WG2098168
Phenanthrene ND 0.0000500 1 07/20/2023 21:41 WG2098168
Pyrene ND 0.0000500 1 07/20/2023 21:41 WG2098168
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1635984
PW-1
Collected date/time: 07/14/23 08:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
1-Methylnaphthalene ND 0.000250 1 07/20/2023 21:41 WG2098168
2-Methylnaphthalene ND 0.000250 1 07/20/2023 21:41 WG2098168
2-Chloronaphthalene ND 0.000250 1 07/20/2023 21:41 WG2098168
(S) Nitrobenzene-d5 105 31.0-160 07/20/2023 21:41 WG2098168
(S) 2-Fluorobiphenyl 97.4 48.0-148 07/20/2023 21:41 WG2098168
(S) p-Terphenyl-d14 99.5 37.0-146 07/20/2023 21:41 WG2098168
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2095809
Total Solids by Method 2540 B-2015 L1635984-01
Method Blank (MB)
(MB) R3950300-1 07/17/23 11:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Total Solids 0.000
L1632829-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1632829-02 07/17/23 11:21 • (DUP) R3950300-3 07/17/23 11:21
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Total Solids 18200 18100 1 0.414 5
L1633529-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1633529-01 07/17/23 11:21 • (DUP) R3950300-4 07/17/23 11:21
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Total Solids 327 323 1 1.23 5
Laboratory Control Sample (LCS)
(LCS) R3950300-2 07/17/23 11:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Total Solids 9500 9560 101 92.5-108
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2097611
Wet Chemistry by Method 1664A L1635984-01
Method Blank (MB)
(MB) R3950639-1 07/20/23 02:04
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr) U 1.16 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3950639-2 07/20/23 02:04 • (LCSD) R3950639-3 07/20/23 02:04
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr) 40.0 38.2 39.7 95.5 99.3 78.0-114 3.85 20
L1636305-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1636305-01 07/20/23 02:04 • (MS) R3950639-4 07/20/23 02:04
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr) 40.0 ND 44.4 111 1 78.0-114
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2095928
Wet Chemistry by Method 3500Cr C-2011 L1635984-01
Method Blank (MB)
(MB) R3950885-1 07/20/23 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Hexavalent Chromium U 0.000150 0.000500
L1636007-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1636007-01 07/20/23 15:29 • (DUP) R3950885-5 07/20/23 15:40
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00403 0.00404 1 0.246 20
Laboratory Control Sample (LCS)
(LCS) R3950885-2 07/20/23 14:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Hexavalent Chromium 0.00200 0.00200 99.8 90.0-110
L1635984-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1635984-01 07/20/23 14:57 • (MS) R3950885-3 07/20/23 15:07 • (MSD) R3950885-4 07/20/23 15:18
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Hexavalent Chromium 0.0500 0.00154 0.0505 0.0503 97.9 97.5 1 90.0-110 0.374 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098129
Mercury by Method 7470A L1635984-01
Method Blank (MB)
(MB) R3951567-1 07/22/23 10:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3951567-2 07/22/23 10:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00308 103 80.0-120
L1636747-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1636747-04 07/22/23 10:46 • (MS) R3951567-3 07/22/23 10:48 • (MSD) R3951567-4 07/22/23 10:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00283 0.00280 94.2 93.5 1 75.0-125 0.840 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2096555
Metals (ICP) by Method 6010B L1635984-01
Method Blank (MB)
(MB) R3951660-1 07/22/23 23:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00430 0.0100
Arsenic U 0.00440 0.0100
Beryllium U 0.000330 0.00200
Cadmium U 0.000479 0.00200
Chromium U 0.00140 0.0100
Copper U 0.00368 0.0100
Lead U 0.00299 0.00600
Nickel U 0.00161 0.0100
Selenium 0.00813 J 0.00735 0.0100
Silver U 0.00154 0.00500
Thallium U 0.00431 0.0100
Zinc U 0.00652 0.0500
Laboratory Control Sample (LCS)
(LCS) R3951660-2 07/22/23 23:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Antimony 1.00 0.990 99.0 80.0-120
Arsenic 1.00 0.961 96.1 80.0-120
Beryllium 1.00 0.990 99.0 80.0-120
Cadmium 1.00 0.968 96.8 80.0-120
Chromium 1.00 0.985 98.5 80.0-120
Copper 1.00 0.985 98.5 80.0-120
Lead 1.00 0.951 95.1 80.0-120
Nickel 1.00 0.986 98.6 80.0-120
Selenium 1.00 0.962 96.2 80.0-120
Silver 0.200 0.191 95.4 80.0-120
Thallium 1.00 0.954 95.4 80.0-120
Zinc 1.00 0.956 95.6 80.0-120
L1635990-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1635990-05 07/22/23 23:49 • (MS) R3951660-4 07/22/23 23:54 • (MSD) R3951660-5 07/22/23 23:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 1.00 ND 0.992 1.01 99.2 101 1 75.0-125 2.05 20
Arsenic 1.00 ND 0.982 1.01 98.2 101 1 75.0-125 2.78 20
Beryllium 1.00 ND 0.994 1.01 99.4 101 1 75.0-125 1.90 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2096555
Metals (ICP) by Method 6010B L1635984-01
L1635990-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1635990-05 07/22/23 23:49 • (MS) R3951660-4 07/22/23 23:54 • (MSD) R3951660-5 07/22/23 23:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Cadmium 1.00 ND 0.966 0.990 96.6 99.0 1 75.0-125 2.39 20
Chromium 1.00 ND 0.964 0.991 96.4 99.1 1 75.0-125 2.77 20
Copper 1.00 ND 0.990 1.01 99.0 101 1 75.0-125 2.24 20
Lead 1.00 ND 0.950 0.976 94.7 97.3 1 75.0-125 2.64 20
Nickel 1.00 ND 0.982 1.00 97.9 99.8 1 75.0-125 1.94 20
Selenium 1.00 ND 0.964 0.971 96.4 97.1 1 75.0-125 0.661 20
Silver 0.200 ND 0.191 0.196 95.5 98.0 1 75.0-125 2.51 20
Thallium 1.00 ND 0.943 0.964 94.3 96.4 1 75.0-125 2.28 20
Zinc 1.00 ND 0.942 0.960 94.2 96.0 1 75.0-125 1.90 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2097817
Volatile Organic Compounds (GC) by Method 8015D/GRO L1635984-01
Method Blank (MB)
(MB) R3952010-2 07/19/23 16:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
TPH (GC/FID) Low Fraction U 0.0314 0.100
(S)
a,a,a-Trifluorotoluene(FID)107 78.0-120
Laboratory Control Sample (LCS)
(LCS) R3952010-1 07/19/23 15:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
TPH (GC/FID) Low Fraction 5.50 5.12 93.1 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 105 78.0-120
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2096768
Volatile Organic Compounds (GC/MS) by Method 8260B L1635984-01
Method Blank (MB)
(MB) R3950239-4 07/18/23 09:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500
Acrylonitrile U 0.000671 0.0100
Benzene U 0.0000941 0.00100
Bromobenzene U 0.000118 0.00100
Bromodichloromethane U 0.000136 0.00100
Bromoform U 0.000129 0.00100
Bromomethane U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-Butylbenzene U 0.000125 0.00100
tert-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chlorodibromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500
Chloromethane U 0.000960 0.00250
2-Chlorotoluene U 0.000106 0.00100
4-Chlorotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100
1,4-Dichlorobenzene U 0.000120 0.00100
Dichlorodifluoromethane U 0.000374 0.00500
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
cis-1,2-Dichloroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
1,1-Dichloropropene U 0.000142 0.00100
1,3-Dichloropropane U 0.000110 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
2,2-Dichloropropane U 0.000161 0.00100
Di-isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Hexachloro-1,3-butadiene U 0.000337 0.00100
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2096768
Volatile Organic Compounds (GC/MS) by Method 8260B L1635984-01
Method Blank (MB)
(MB) R3950239-4 07/18/23 09:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Isopropylbenzene U 0.000105 0.00100
p-Isopropyltoluene U 0.000120 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK) U 0.000478 0.0100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100
1,1,1,2-Tetrachloroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene U 0.000230 0.00100
1,2,4-Trichlorobenzene U 0.000481 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,2,3-Trichloropropane U 0.000237 0.00250
1,2,4-Trimethylbenzene U 0.000322 0.00100
1,2,3-Trimethylbenzene U 0.000104 0.00100
1,3,5-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
Xylenes, Total U 0.000174 0.00300
(S) Toluene-d8 83.9 80.0-120
(S) 4-Bromofluorobenzene 117 77.0-126
(S) 1,2-Dichloroethane-d4 112 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3950239-1 07/18/23 08:25 • (LCSD) R3950239-2 07/18/23 08:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0268 0.0262 107 105 19.0-160 2.26 27
Acrolein 0.0250 0.0218 0.0224 87.2 89.6 10.0-160 2.71 26
Acrylonitrile 0.0250 0.0257 0.0256 103 102 55.0-149 0.390 20
Benzene 0.00500 0.00518 0.00519 104 104 70.0-123 0.193 20
Bromobenzene 0.00500 0.00488 0.00399 97.6 79.8 73.0-121 J3 20.1 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2096768
Volatile Organic Compounds (GC/MS) by Method 8260B L1635984-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3950239-1 07/18/23 08:25 • (LCSD) R3950239-2 07/18/23 08:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Bromodichloromethane 0.00500 0.00591 0.00531 118 106 75.0-120 10.7 20
Bromoform 0.00500 0.00537 0.00487 107 97.4 68.0-132 9.77 20
Bromomethane 0.00500 0.00757 0.00765 151 153 10.0-160 1.05 25
n-Butylbenzene 0.00500 0.00505 0.00518 101 104 73.0-125 2.54 20
sec-Butylbenzene 0.00500 0.00510 0.00496 102 99.2 75.0-125 2.78 20
tert-Butylbenzene 0.00500 0.00534 0.00479 107 95.8 76.0-124 10.9 20
Carbon tetrachloride 0.00500 0.00581 0.00590 116 118 68.0-126 1.54 20
Chlorobenzene 0.00500 0.00535 0.00551 107 110 80.0-121 2.95 20
Chlorodibromomethane 0.00500 0.00528 0.00557 106 111 77.0-125 5.35 20
Chloroethane 0.00500 0.0101 0.0105 202 210 47.0-150 J4 J4 3.88 20
Chloroform 0.00500 0.00560 0.00542 112 108 73.0-120 3.27 20
Chloromethane 0.00500 0.00424 0.00421 84.8 84.2 41.0-142 0.710 20
2-Chlorotoluene 0.00500 0.00578 0.00476 116 95.2 76.0-123 19.4 20
4-Chlorotoluene 0.00500 0.00495 0.00431 99.0 86.2 75.0-122 13.8 20
1,2-Dibromo-3-Chloropropane 0.00500 0.00449 0.00344 89.8 68.8 58.0-134 J3 26.5 20
1,2-Dibromoethane 0.00500 0.00570 0.00530 114 106 80.0-122 7.27 20
Dibromomethane 0.00500 0.00572 0.00560 114 112 80.0-120 2.12 20
1,2-Dichlorobenzene 0.00500 0.00575 0.00442 115 88.4 79.0-121 J3 26.2 20
1,3-Dichlorobenzene 0.00500 0.00514 0.00572 103 114 79.0-120 10.7 20
1,4-Dichlorobenzene 0.00500 0.00554 0.00538 111 108 79.0-120 2.93 20
Dichlorodifluoromethane 0.00500 0.00576 0.00557 115 111 51.0-149 3.35 20
1,1-Dichloroethane 0.00500 0.00528 0.00524 106 105 70.0-126 0.760 20
1,2-Dichloroethane 0.00500 0.00554 0.00538 111 108 70.0-128 2.93 20
1,1-Dichloroethene 0.00500 0.00519 0.00500 104 100 71.0-124 3.73 20
cis-1,2-Dichloroethene 0.00500 0.00519 0.00528 104 106 73.0-120 1.72 20
trans-1,2-Dichloroethene 0.00500 0.00523 0.00512 105 102 73.0-120 2.13 20
1,2-Dichloropropane 0.00500 0.00569 0.00525 114 105 77.0-125 8.04 20
1,1-Dichloropropene 0.00500 0.00550 0.00546 110 109 74.0-126 0.730 20
1,3-Dichloropropane 0.00500 0.00524 0.00506 105 101 80.0-120 3.50 20
cis-1,3-Dichloropropene 0.00500 0.00546 0.00578 109 116 80.0-123 5.69 20
trans-1,3-Dichloropropene 0.00500 0.00549 0.00521 110 104 78.0-124 5.23 20
2,2-Dichloropropane 0.00500 0.00529 0.00573 106 115 58.0-130 7.99 20
Di-isopropyl ether 0.00500 0.00485 0.00480 97.0 96.0 58.0-138 1.04 20
Ethylbenzene 0.00500 0.00522 0.00536 104 107 79.0-123 2.65 20
Hexachloro-1,3-butadiene 0.00500 0.00355 0.00341 71.0 68.2 54.0-138 4.02 20
Isopropylbenzene 0.00500 0.00582 0.00601 116 120 76.0-127 3.21 20
p-Isopropyltoluene 0.00500 0.00533 0.00593 107 119 76.0-125 10.7 20
2-Butanone (MEK)0.0250 0.0253 0.0250 101 100 44.0-160 1.19 20
Methylene Chloride 0.00500 0.00526 0.00507 105 101 67.0-120 3.68 20
4-Methyl-2-pentanone (MIBK) 0.0250 0.0258 0.0251 103 100 68.0-142 2.75 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2096768
Volatile Organic Compounds (GC/MS) by Method 8260B L1635984-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3950239-1 07/18/23 08:25 • (LCSD) R3950239-2 07/18/23 08:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Naphthalene 0.00500 0.00356 0.00336 71.2 67.2 54.0-135 5.78 20
n-Propylbenzene 0.00500 0.00506 0.00434 101 86.8 77.0-124 15.3 20
Styrene 0.00500 0.00534 0.00525 107 105 73.0-130 1.70 20
1,1,1,2-Tetrachloroethane 0.00500 0.00540 0.00540 108 108 75.0-125 0.000 20
1,1,2,2-Tetrachloroethane 0.00500 0.00466 0.00424 93.2 84.8 65.0-130 9.44 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00579 0.00592 116 118 69.0-132 2.22 20
Tetrachloroethene 0.00500 0.00551 0.00536 110 107 72.0-132 2.76 20
Toluene 0.00500 0.00486 0.00489 97.2 97.8 79.0-120 0.615 20
1,2,3-Trichlorobenzene 0.00500 0.00373 0.00366 74.6 73.2 50.0-138 1.89 20
1,2,4-Trichlorobenzene 0.00500 0.00407 0.00370 81.4 74.0 57.0-137 9.52 20
1,1,1-Trichloroethane 0.00500 0.00569 0.00569 114 114 73.0-124 0.000 20
1,1,2-Trichloroethane 0.00500 0.00511 0.00511 102 102 80.0-120 0.000 20
Trichloroethene 0.00500 0.00619 0.00584 124 117 78.0-124 5.82 20
Trichlorofluoromethane 0.00500 0.00801 0.00692 160 138 59.0-147 J4 14.6 20
1,2,3-Trichloropropane 0.00500 0.00610 0.00483 122 96.6 73.0-130 J3 23.2 20
1,2,4-Trimethylbenzene 0.00500 0.00518 0.00470 104 94.0 76.0-121 9.72 20
1,2,3-Trimethylbenzene 0.00500 0.00552 0.00513 110 103 77.0-120 7.32 20
1,3,5-Trimethylbenzene 0.00500 0.00576 0.00471 115 94.2 76.0-122 J3 20.1 20
Vinyl chloride 0.00500 0.00543 0.00532 109 106 67.0-131 2.05 20
Xylenes, Total 0.0150 0.0159 0.0159 106 106 79.0-123 0.000 20
(S) Toluene-d8 99.3 100 80.0-120
(S) 4-Bromofluorobenzene 126 116 77.0-126
(S) 1,2-Dichloroethane-d4 111 110 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2097882
Volatile Organic Compounds (GC/MS) by Method 8260B L1635984-01
Method Blank (MB)
(MB) R3950703-3 07/19/23 20:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Methyl tert-butyl ether U 0.000101 0.00100
(S) Toluene-d8 104 80.0-120
(S) 4-Bromofluorobenzene 104 77.0-126
(S) 1,2-Dichloroethane-d4 115 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3950703-1 07/19/23 19:11
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Methyl tert-butyl ether 0.00500 0.00538 108 68.0-125
(S) Toluene-d8 98.9 80.0-120
(S) 4-Bromofluorobenzene 98.9 77.0-126
(S) 1,2-Dichloroethane-d4 114 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098975
Semi-Volatile Organic Compounds (GC) by Method 8015 L1635984-01
Method Blank (MB)
(MB) R3951596-1 07/21/23 23:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
C10-C28 Diesel Range U 0.0222 0.100
C28-C40 Oil Range U 0.0118 0.100
(S) o-Terphenyl 76.0 52.0-156
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3951596-2 07/21/23 23:57 • (LCSD) R3951596-3 07/22/23 00:17
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
C10-C28 Diesel Range 1.50 1.26 1.29 84.0 86.0 50.0-150 2.35 20
(S) o-Terphenyl 88.0 89.5 52.0-156
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2097512
Polychlorinated Biphenyls (GC) by Method 8082 L1635984-01
Method Blank (MB)
(MB) R3951909-1 07/19/23 23:14
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
PCB 1016 U 0.000270 0.000500
PCB 1221 U 0.000270 0.000500
PCB 1232 U 0.000270 0.000500
PCB 1242 U 0.000270 0.000500
PCB 1248 U 0.000173 0.000500
PCB 1254 U 0.000173 0.000500
PCB 1260 U 0.000173 0.000500
(S) Decachlorobiphenyl 52.3 10.0-128
(S) Tetrachloro-m-xylene 66.2 10.0-127
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3951909-4 07/19/23 23:41 • (LCSD) R3951909-5 07/19/23 23:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
PCB 1016 0.00250 0.00149 0.00149 59.6 59.6 36.0-135 0.000 29
PCB 1260 0.00250 0.00163 0.00159 65.2 63.6 42.0-131 2.48 25
(S) Decachlorobiphenyl 54.0 46.9 10.0-128
(S) Tetrachloro-m-xylene 63.2 62.4 10.0-127
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098169
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1635984-01
Method Blank (MB)
(MB) R3952019-3 07/20/23 21:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.0000886 0.00100
Acenaphthylene U 0.0000921 0.00100
Anthracene U 0.0000804 0.00100
Benzidine U 0.00374 0.0100
Benzo(a)anthracene U 0.000199 0.00100
Benzo(b)fluoranthene U 0.000130 0.00100
Benzo(k)fluoranthene U 0.000120 0.00100
Benzo(g,h,i)perylene U 0.000121 0.00100
Benzo(a)pyrene U 0.0000381 0.00100
Bis(2-chlorethoxy)methane U 0.000116 0.0100
Bis(2-chloroethyl)ether U 0.000137 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100
4-Bromophenyl-phenylether U 0.0000877 0.0100
2-Chloronaphthalene U 0.0000648 0.00100
4-Chlorophenyl-phenylether U 0.0000926 0.0100
Chrysene U 0.000130 0.00100
Dibenz(a,h)anthracene U 0.0000644 0.00100
1,2-Dichlorobenzene U 0.0000713 0.0100
1,3-Dichlorobenzene U 0.000132 0.0100
1,4-Dichlorobenzene U 0.0000942 0.0100
3,3-Dichlorobenzidine U 0.000212 0.0100
2,4-Dinitrotoluene U 0.0000983 0.0100
2,6-Dinitrotoluene U 0.000250 0.0100
Fluoranthene U 0.000102 0.00100
Fluorene U 0.0000844 0.00100
Hexachlorobenzene U 0.0000755 0.00100
Hexachloro-1,3-butadiene U 0.0000968 0.0100
Hexachlorocyclopentadiene U 0.0000598 0.0100
Hexachloroethane U 0.000127 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000143 0.0100
Naphthalene U 0.000159 0.00100
Nitrobenzene U 0.000297 0.0100
n-Nitrosodimethylamine U 0.000998 0.0100
n-Nitrosodiphenylamine U 0.00237 0.0100
n-Nitrosodi-n-propylamine U 0.000261 0.0100
Phenanthrene U 0.000112 0.00100
Benzylbutyl phthalate U 0.000765 0.00300
Bis(2-ethylhexyl)phthalate U 0.000895 0.00300
Di-n-butyl phthalate U 0.000453 0.00300
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098169
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1635984-01
Method Blank (MB)
(MB) R3952019-3 07/20/23 21:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Diethyl phthalate U 0.000287 0.00300
Dimethyl phthalate U 0.000260 0.00300
Di-n-octyl phthalate U 0.000932 0.00300
Pyrene U 0.000107 0.00100
1,2,4-Trichlorobenzene U 0.0000698 0.0100
4-Chloro-3-methylphenol U 0.000131 0.0100
2-Chlorophenol U 0.000133 0.0100
2,4-Dichlorophenol U 0.000102 0.0100
2,4-Dimethylphenol 0.000323 J 0.0000636 0.0100
4,6-Dinitro-2-methylphenol U 0.00112 0.0100
2,4-Dinitrophenol U 0.00593 0.0100
2-Nitrophenol U 0.000117 0.0100
4-Nitrophenol U 0.000143 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.00433 0.0100
2,4,6-Trichlorophenol U 0.000100 0.0100
(S) 2-Fluorophenol 21.1 10.0-120
(S) Phenol-d5 13.1 10.0-120
(S) Nitrobenzene-d5 55.4 10.0-127
(S) 2-Fluorobiphenyl 48.4 10.0-130
(S) 2,4,6-Tribromophenol 63.5 10.0-155
(S) p-Terphenyl-d14 62.3 10.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3952019-1 07/20/23 21:14 • (LCSD) R3952019-2 07/20/23 21:36
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 0.0314 0.0308 62.8 61.6 41.0-120 1.93 22
Acenaphthylene 0.0500 0.0361 0.0340 72.2 68.0 43.0-120 5.99 22
Anthracene 0.0500 0.0359 0.0352 71.8 70.4 45.0-120 1.97 20
Benzidine 0.100 0.00683 0.00915 6.83 9.15 10.0-120 J4 J4 29.0 36
Benzo(a)anthracene 0.0500 0.0388 0.0397 77.6 79.4 47.0-120 2.29 20
Benzo(b)fluoranthene 0.0500 0.0385 0.0397 77.0 79.4 46.0-120 3.07 20
Benzo(k)fluoranthene 0.0500 0.0364 0.0364 72.8 72.8 46.0-120 0.000 21
Benzo(g,h,i)perylene 0.0500 0.0375 0.0380 75.0 76.0 48.0-121 1.32 20
Benzo(a)pyrene 0.0500 0.0403 0.0408 80.6 81.6 47.0-120 1.23 20
Bis(2-chlorethoxy)methane 0.0500 0.0305 0.0277 61.0 55.4 33.0-120 9.62 24
Bis(2-chloroethyl)ether 0.0500 0.0294 0.0251 58.8 50.2 23.0-120 15.8 33
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098169
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1635984-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3952019-1 07/20/23 21:14 • (LCSD) R3952019-2 07/20/23 21:36
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
2,2-Oxybis(1-Chloropropane) 0.0500 0.0273 0.0246 54.6 49.2 28.0-120 10.4 31
4-Bromophenyl-phenylether 0.0500 0.0374 0.0357 74.8 71.4 45.0-120 4.65 20
2-Chloronaphthalene 0.0500 0.0327 0.0307 65.4 61.4 37.0-120 6.31 25
4-Chlorophenyl-phenylether 0.0500 0.0349 0.0327 69.8 65.4 44.0-120 6.51 20
Chrysene 0.0500 0.0381 0.0388 76.2 77.6 48.0-120 1.82 20
Dibenz(a,h)anthracene 0.0500 0.0393 0.0398 78.6 79.6 47.0-120 1.26 20
1,2-Dichlorobenzene 0.0500 0.0271 0.0240 54.2 48.0 20.0-120 12.1 34
1,3-Dichlorobenzene 0.0500 0.0262 0.0231 52.4 46.2 17.0-120 12.6 35
1,4-Dichlorobenzene 0.0500 0.0267 0.0237 53.4 47.4 18.0-120 11.9 34
3,3-Dichlorobenzidine 0.100 0.0795 0.0825 79.5 82.5 44.0-120 3.70 20
2,4-Dinitrotoluene 0.0500 0.0389 0.0396 77.8 79.2 49.0-124 1.78 20
2,6-Dinitrotoluene 0.0500 0.0367 0.0353 73.4 70.6 46.0-120 3.89 21
Fluoranthene 0.0500 0.0415 0.0402 83.0 80.4 51.0-120 3.18 20
Fluorene 0.0500 0.0336 0.0330 67.2 66.0 47.0-120 1.80 20
Hexachlorobenzene 0.0500 0.0375 0.0366 75.0 73.2 44.0-120 2.43 20
Hexachloro-1,3-butadiene 0.0500 0.0326 0.0286 65.2 57.2 19.0-120 13.1 32
Hexachlorocyclopentadiene 0.0500 0.0119 0.0101 23.8 20.2 15.0-120 16.4 31
Hexachloroethane 0.0500 0.0270 0.0236 54.0 47.2 15.0-120 13.4 37
Indeno(1,2,3-cd)pyrene 0.0500 0.0310 0.0321 62.0 64.2 49.0-122 3.49 20
Isophorone 0.0500 0.0326 0.0308 65.2 61.6 36.0-120 5.68 23
Naphthalene 0.0500 0.0277 0.0254 55.4 50.8 27.0-120 8.66 27
Nitrobenzene 0.0500 0.0327 0.0295 65.4 59.0 27.0-120 10.3 29
n-Nitrosodimethylamine 0.0500 0.0201 0.0187 40.2 37.4 10.0-120 7.22 40
n-Nitrosodiphenylamine 0.0500 0.0347 0.0342 69.4 68.4 47.0-120 1.45 20
n-Nitrosodi-n-propylamine 0.0500 0.0304 0.0279 60.8 55.8 31.0-120 8.58 28
Phenanthrene 0.0500 0.0346 0.0338 69.2 67.6 46.0-120 2.34 20
Benzylbutyl phthalate 0.0500 0.0375 0.0384 75.0 76.8 43.0-121 2.37 20
Bis(2-ethylhexyl)phthalate 0.0500 0.0365 0.0381 73.0 76.2 43.0-122 4.29 20
Di-n-butyl phthalate 0.0500 0.0437 0.0439 87.4 87.8 49.0-121 0.457 20
Diethyl phthalate 0.0500 0.0382 0.0379 76.4 75.8 48.0-122 0.788 20
Dimethyl phthalate 0.0500 0.0362 0.0354 72.4 70.8 48.0-120 2.23 20
Di-n-octyl phthalate 0.0500 0.0404 0.0423 80.8 84.6 42.0-125 4.59 20
Pyrene 0.0500 0.0365 0.0371 73.0 74.2 47.0-120 1.63 20
1,2,4-Trichlorobenzene 0.0500 0.0302 0.0267 60.4 53.4 24.0-120 12.3 29
4-Chloro-3-methylphenol 0.0500 0.0344 0.0324 68.8 64.8 40.0-120 5.99 21
2-Chlorophenol 0.0500 0.0278 0.0238 55.6 47.6 25.0-120 15.5 35
2,4-Dichlorophenol 0.0500 0.0323 0.0293 64.6 58.6 36.0-120 9.74 26
2,4-Dimethylphenol 0.0500 0.0335 0.0313 67.0 62.6 33.0-120 6.79 26
4,6-Dinitro-2-methylphenol 0.0500 0.0403 0.0396 80.6 79.2 38.0-138 1.75 25
2,4-Dinitrophenol 0.0500 0.0392 0.0384 78.4 76.8 10.0-120 2.06 39
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098169
Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1635984-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3952019-1 07/20/23 21:14 • (LCSD) R3952019-2 07/20/23 21:36
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
2-Nitrophenol 0.0500 0.0330 0.0314 66.0 62.8 31.0-120 4.97 29
4-Nitrophenol 0.0500 0.0132 0.0127 26.4 25.4 10.0-120 3.86 33
Pentachlorophenol 0.0500 0.0399 0.0400 79.8 80.0 23.0-120 0.250 25
Phenol 0.0500 0.0128 0.0107 25.6 21.4 10.0-120 17.9 36
2,4,6-Trichlorophenol 0.0500 0.0397 0.0377 79.4 75.4 42.0-120 5.17 23
(S) 2-Fluorophenol 38.0 31.3 10.0-120
(S) Phenol-d5 24.4 20.3 10.0-120
(S) Nitrobenzene-d5 63.5 59.9 10.0-127
(S) 2-Fluorobiphenyl 67.1 61.7 10.0-130
(S) 2,4,6-Tribromophenol 83.0 82.0 10.0-155
(S) p-Terphenyl-d14 77.4 77.2 10.0-128
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098168
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1635984-01
Method Blank (MB)
(MB) R3951971-3 07/20/23 17:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Anthracene U 0.0000190 0.0000500
Acenaphthene U 0.0000190 0.0000500
Acenaphthylene U 0.0000171 0.0000500
Benzo(a)anthracene U 0.0000203 0.0000500
Benzo(a)pyrene U 0.0000184 0.0000500
Benzo(b)fluoranthene U 0.0000168 0.0000500
Benzo(g,h,i)perylene U 0.0000184 0.0000500
Benzo(k)fluoranthene U 0.0000202 0.0000500
Chrysene U 0.0000179 0.0000500
Dibenz(a,h)anthracene U 0.0000160 0.0000500
Fluoranthene U 0.0000270 0.000100
Fluorene U 0.0000169 0.0000500
Indeno(1,2,3-cd)pyrene U 0.0000158 0.0000500
Naphthalene U 0.0000917 0.000250
Phenanthrene U 0.0000180 0.0000500
Pyrene U 0.0000169 0.0000500
1-Methylnaphthalene U 0.0000687 0.000250
2-Methylnaphthalene U 0.0000674 0.000250
2-Chloronaphthalene U 0.0000682 0.000250
(S) Nitrobenzene-d5 98.5 31.0-160
(S) 2-Fluorobiphenyl 100 48.0-148
(S) p-Terphenyl-d14 105 37.0-146
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3951971-1 07/20/23 16:46 • (LCSD) R3951971-2 07/20/23 17:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Anthracene 0.00200 0.00172 0.00171 86.0 85.5 67.0-150 0.583 20
Acenaphthene 0.00200 0.00172 0.00171 86.0 85.5 65.0-138 0.583 20
Acenaphthylene 0.00200 0.00178 0.00181 89.0 90.5 66.0-140 1.67 20
Benzo(a)anthracene 0.00200 0.00177 0.00168 88.5 84.0 61.0-140 5.22 20
Benzo(a)pyrene 0.00200 0.00183 0.00164 91.5 82.0 60.0-143 11.0 20
Benzo(b)fluoranthene 0.00200 0.00188 0.00167 94.0 83.5 58.0-141 11.8 20
Benzo(g,h,i)perylene 0.00200 0.00157 0.00137 78.5 68.5 52.0-153 13.6 20
Benzo(k)fluoranthene 0.00200 0.00171 0.00155 85.5 77.5 58.0-148 9.82 20
Chrysene 0.00200 0.00187 0.00181 93.5 90.5 64.0-144 3.26 20
Dibenz(a,h)anthracene 0.00200 0.00148 0.00125 74.0 62.5 52.0-155 16.8 20
Fluoranthene 0.00200 0.00183 0.00181 91.5 90.5 69.0-153 1.10 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2098168
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1635984-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3951971-1 07/20/23 16:46 • (LCSD) R3951971-2 07/20/23 17:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Fluorene 0.00200 0.00185 0.00189 92.5 94.5 64.0-136 2.14 20
Indeno(1,2,3-cd)pyrene 0.00200 0.00166 0.00141 83.0 70.5 54.0-153 16.3 20
Naphthalene 0.00200 0.00182 0.00183 91.0 91.5 61.0-137 0.548 20
Phenanthrene 0.00200 0.00189 0.00189 94.5 94.5 62.0-137 0.000 20
Pyrene 0.00200 0.00209 0.00209 104 104 60.0-142 0.000 20
1-Methylnaphthalene 0.00200 0.00184 0.00184 92.0 92.0 66.0-142 0.000 20
2-Methylnaphthalene 0.00200 0.00176 0.00177 88.0 88.5 62.0-136 0.567 20
2-Chloronaphthalene 0.00200 0.00185 0.00188 92.5 94.0 64.0-140 1.61 20
(S) Nitrobenzene-d5 94.0 93.5 31.0-160
(S) 2-Fluorobiphenyl 91.5 92.0 48.0-148
(S) p-Terphenyl-d14 88.0 82.0 37.0-146
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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_6479884.1

Appendix H
French Drain Excavation

Table H‐1: French Drain Arsenic Confirmation Samples Results
Sample name
Sample 
Detection
(mg/kg)
FD1‐CS1 3.0
FD1‐CS2 6.8
FD1‐CS3 7.2
Notes:
mg/kg = milligram per kilogram
Background threshold value is equal to 15 mg/kg for arsenic.
Recycled Earth Site Characterization Report

Page 1 of 3 PHOTO LOG

Number: 1 Date: October 18, 2023
Description: View of the french drain inlet excavation.

Number: 2 Date: October 18, 2023
Description: View of the french drain inlet excavation.

Recycled Earth Site Characterization Report

Page 2 of 3 PHOTO LOG

Number: 3 Date: October 18, 2023
Description: View of the french drain inlet excavation.

Number: 4 Date: October 18, 2023
Description: View of soil stockpile removed from the french drain inlet excavation

Recycled Earth Site Characterization Report

Page 3 of 3 PHOTO LOG

Number: 5 Date: October 18, 2023
Description: View of french drain inlet excavation.

CamScanner
ANALYTICAL REPORT
October 24, 2023
Revised Report
Tetra Tech Inc. - UT
Sample Delivery Group:L1668348
Samples Received:10/19/2023
Project Number:
Description:Recycled Earth
Report To:Anna Rasmuson
4750 West 2100 South
Suite 400
Salt Lake City, UT 84120
Entire Report Reviewed By:
October 24, 2023
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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October 24, 2023
Chris Ward
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
FD1-CS1 L1668348-01 5
FD1-CS2 L1668348-02 6
FD1-CS3 L1668348-03 7
Qc: Quality Control Summary 8
Total Solids by Method 2540 G-2011 8
Metals (ICP) by Method 6010B 9
Gl: Glossary of Terms 10
Al: Accreditations & Locations 11
Sc: Sample Chain of Custody 12
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FD1-CS1 L1668348-01 Solid Richie T 10/18/23 09:00 10/19/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2154987 1 10/20/23 08:59 10/20/23 09:03 CMK Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2155216 1 10/21/23 01:26 10/22/23 10:17 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD1-CS2 L1668348-02 Solid Richie T 10/18/23 09:10 10/19/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2154987 1 10/20/23 08:59 10/20/23 09:03 CMK Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2155216 1 10/21/23 01:26 10/22/23 10:20 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
FD1-CS3 L1668348-03 Solid Richie T 10/18/23 09:15 10/19/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2154987 1 10/20/23 08:59 10/20/23 09:03 CMK Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2155216 1 10/21/23 01:26 10/22/23 10:23 ZSA Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 10/23/23 15:52
Project Narrative
Report revised to reflect updated sample Id's for samples L1668348-02 (FD1-CS2) and L1668348-03 (FD1-CS3)
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Chris Ward
Project Manager
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SAMPLE RESULTS - 01
L1668348
FD1-CS1
Collected date/time: 10/18/23 09:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.6 1 10/20/2023 09:03 WG2154987
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Arsenic 3.00 2.36 1 10/22/2023 10:17 WG2155216
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1668348
FD1-CS2
Collected date/time: 10/18/23 09:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.5 1 10/20/2023 09:03 WG2154987
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Arsenic 6.83 2.40 1 10/22/2023 10:20 WG2155216
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 03
L1668348
FD1-CS3
Collected date/time: 10/18/23 09:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.5 1 10/20/2023 09:03 WG2154987
Metals (ICP) by Method 6010B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Arsenic 7.22 2.48 1 10/22/2023 10:23 WG2155216
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2154987
Total Solids by Method 2540 G-2011 L1668348-01,02,03
Method Blank (MB)
(MB) R3989059-1 10/20/23 09:03
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1668348-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1668348-01 10/20/23 09:03 • (DUP) R3989059-3 10/20/23 09:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 84.6 84.7 1 0.0954 10
Laboratory Control Sample (LCS)
(LCS) R3989059-2 10/20/23 09:03
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 99.9 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2155216
Metals (ICP) by Method 6010B L1668348-01,02,03
Method Blank (MB)
(MB) R3989510-1 10/22/23 09:04
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.518 2.00
Laboratory Control Sample (LCS)
(LCS) R3989510-2 10/22/23 09:06
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Arsenic 100 104 104 80.0-120
L1668030-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1668030-01 10/22/23 09:09 • (MS) R3989510-5 10/22/23 09:17 • (MSD) R3989510-6 10/22/23 09:20
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 100 ND 108 110 108 110 1 75.0-125 1.57 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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_6479884.1

Appendix I
Gas Chromatograph Logs

Lab ID Matrix Sample ID Location Match SVOC GC 
All NA General 
Comments 
NA NA Peaks include surrogates (S), 
internal standards (I), and 
minor unlabelled peaks 
Major peaks include 
solvent peak and 
surrogate peak (o‐
terphenyl) 
L1584351‐
01 
Soil SS‐12 off‐site No PAHs, and hydrocarbon 
peak pattern at 2‐4 minutes, 
UCMR at 7‐12 minutes and 
at 13 minutes‐end. No 
match. 
No discernable peaks. 
No match.  
L1584351‐
02 
Soil SS‐10 off‐site No Unlabelled peak at 4.4 
minutes. No match. 
Minor peaks and UCMR 
in motor oil or late 
diesel range at 3‐5.5 
minutes. No match. 
L1584351‐
03 
Soil SS‐7 on‐site NA PAHs, unlabelled peaks 
throughout, UCMR at 6‐7 
minutes and at 13 minutes‐
end 
Minor peaks and UCMR 
in motor oil or late 
diesel range at 3‐5.5 
minutes 
L1584351‐
04 
Soil SS‐6 on‐site NA PAHs, unlabelled peaks 
throughout, UCMR at 6‐7 
minutes and at 13 minutes‐
end 
Minor peaks and UCMR 
in motor oil or late 
diesel range at 3‐5.5 
minutes 
L1582319‐
01 
Aq SW‐1 on‐site NA No labelled peaks, 
significant unlabelled peaks 
at 2‐2.4 minute and minor 
peaks throughout 
chromatogram especially 
from 6 minutes to end 
Typical hydrocarbon 
mixture pattern, 
quantified as TPH High 
Fraction. Hydrocarbon 
mixture not identified. 
L1582319‐
02 
Aq SW‐2 off‐site No Phthalates, and minor 
unlabelled peaks, no match 
No significant 
hydrocarbon pattern. No 
match. 
L1582319‐
03 
Aq SW‐3 off‐site No Phthalates, UCMR at 7 to 8 
minute, no match 
No significant 
hydrocarbon pattern. No 
match. 
L1582319‐
04 
Aq SW‐4 off‐site No Phthalates, low levels of 
PAHs, and unlabelled peaks, 
no match 
No significant 
hydrocarbon pattern. No 
match. 
L1582319‐
05 
Aq SW‐5 off‐site No Unlabelled peaks, no match No significant 
hydrocarbon pattern. No 
match. 
Lab ID Matrix Sample ID Location Match SVOC GC 
L1607939‐
07 
Soil SS‐1 on‐site NA PAHs, and unlabelled peaks 
at 2‐6.5 minutes 
Minor peaks before the 
diesel range, UCMR in 
the oil range 
L1607939‐
08 
Soil SS‐2 on‐site NA PAHs, and unlabelled peaks 
at 2‐5 minutes 
Minor peaks before the 
diesel range, UCMR in 
the oil range 
L1607939‐
09 
Soil SS‐3 on‐site NA PAHs, and unlabelled peaks 
at 4‐8 minutes 
Typical hydrocarbon 
mixture pattern in the 
diesel range, UCMR in 
the oil range 
L1607939‐
10 
Soil SS‐4 on‐site NA PAHs, and unlabelled peaks 
at 2‐7.5 minutes 
UCMR in the oil range 

Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_031.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 9:48 pm
Operator : 614
Sample : L1582319-01 20X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 27 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 08 07:04:17 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
20) S o-terphenyl 0.00 0 N.D. ppm d
Spiked Amount 0.4000 Range 70 - 130 Recovery = 0.00%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 6.17 926981858 70.0921641 ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h,m C10-C28 Diesel Range 0.00 0 N.D. ppm
9) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
10) h,m C28-C40 Oil Range 0.00 0 N.D. ppm
11) h,t,m C10-C24 Hydrocarbons 0.00 0 N.D. ppm
12) t,m,h C13-C22 Hydrocarbons 0.00 0 N.D. ppm
13) t,h,m DRO C13-22 0.00 0 N.D. ppm
14) h,m Diesel 0.00 0 N.D. ppm
15) h,m Motor Oil 0.00 0 N.D. ppm
16) h Mineral Spirits 0.00 0 N.D. ppm
17) h Kerosene 0.00 0 N.D. ppm
18) h #6 Fuel Oil 0.00 0 N.D. ppm
19) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM31A30W.M Wed Feb 08 07:04:19 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_031.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 9:48 pm
Operator : 614
Sample : L1582319-01 20X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 27 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 08 07:04:17 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
Time
Response_Signal: 0207_031.d\FID1A.ch
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DM31A30W.M Wed Feb 08 07:04:20 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_024.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 7:30 pm
Operator : 614
Sample : L1582319-02 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 20 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 07 20:09:28 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
20) S o-terphenyl 7.97 6675659 0.4254583 ppm
Spiked Amount 0.4000 Range 70 - 130 Recovery = 106.36%
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 6.17 55187920 3.2872671 ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h,m C10-C28 Diesel Range 0.00 0 N.D. ppm
9) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
10) h,m C28-C40 Oil Range 0.00 0 N.D. ppm
11) h,t,m C10-C24 Hydrocarbons 0.00 0 N.D. ppm
12) t,m,h C13-C22 Hydrocarbons 0.00 0 N.D. ppm
13) t,h,m DRO C13-22 0.00 0 N.D. ppm
14) h,m Diesel 0.00 0 N.D. ppm
15) h,m Motor Oil 0.00 0 N.D. ppm
16) h Mineral Spirits 0.00 0 N.D. ppm
17) h Kerosene 0.00 0 N.D. ppm
18) h #6 Fuel Oil 0.00 0 N.D. ppm
19) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM31A30W.M Tue Feb 07 20:09:30 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_024.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 7:30 pm
Operator : 614
Sample : L1582319-02 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 20 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 07 20:09:28 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
Time
Response_Signal: 0207_024.d\FID1A.ch
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DM31A30W.M Tue Feb 07 20:09:30 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_025.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 7:50 pm
Operator : 614
Sample : L1582319-03 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 21 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 07 20:09:47 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
20) S o-terphenyl 7.97 6972581 0.4443820 ppm
Spiked Amount 0.4000 Range 70 - 130 Recovery = 111.10%
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 6.17 48390805 2.7664095 ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h,m C10-C28 Diesel Range 0.00 0 N.D. ppm
9) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
10) h,m C28-C40 Oil Range 0.00 0 N.D. ppm
11) h,t,m C10-C24 Hydrocarbons 0.00 0 N.D. ppm
12) t,m,h C13-C22 Hydrocarbons 0.00 0 N.D. ppm
13) t,h,m DRO C13-22 0.00 0 N.D. ppm
14) h,m Diesel 0.00 0 N.D. ppm
15) h,m Motor Oil 0.00 0 N.D. ppm
16) h Mineral Spirits 0.00 0 N.D. ppm
17) h Kerosene 0.00 0 N.D. ppm
18) h #6 Fuel Oil 0.00 0 N.D. ppm
19) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM31A30W.M Tue Feb 07 20:09:49 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_025.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 7:50 pm
Operator : 614
Sample : L1582319-03 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 21 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 07 20:09:47 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
Time
Response_Signal: 0207_025.d\FID1A.ch
o-
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DM31A30W.M Tue Feb 07 20:09:49 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_038.d
Signal(s) : FID1A.ch
Acq On : 8 Feb 2023 12:23 am
Operator : 614
Sample : L1582319-04 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 22 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 08 07:06:45 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
20) S o-terphenyl 7.97 6675491 0.4254476 ppm
Spiked Amount 0.4000 Range 70 - 130 Recovery = 106.36%
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 6.17 39587321 2.0918053 ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h,m C10-C28 Diesel Range 0.00 0 N.D. ppm
9) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
10) h,m C28-C40 Oil Range 0.00 0 N.D. ppm
11) h,t,m C10-C24 Hydrocarbons 0.00 0 N.D. ppm
12) t,m,h C13-C22 Hydrocarbons 0.00 0 N.D. ppm
13) t,h,m DRO C13-22 0.00 0 N.D. ppm
14) h,m Diesel 0.00 0 N.D. ppm
15) h,m Motor Oil 0.00 0 N.D. ppm
16) h Mineral Spirits 0.00 0 N.D. ppm
17) h Kerosene 0.00 0 N.D. ppm
18) h #6 Fuel Oil 0.00 0 N.D. ppm
19) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM31A30W.M Wed Feb 08 07:06:49 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_038.d
Signal(s) : FID1A.ch
Acq On : 8 Feb 2023 12:23 am
Operator : 614
Sample : L1582319-04 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 22 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 08 07:06:45 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
Time
Response_Signal: 0207_038.d\FID1A.ch
o-
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DM31A30W.M Wed Feb 08 07:06:49 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_027.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 8:30 pm
Operator : 614
Sample : L1582319-05 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 23 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 07 21:40:11 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
20) S o-terphenyl 7.97 6465651 0.4120739 ppm
Spiked Amount 0.4000 Range 70 - 130 Recovery = 103.02%
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 6.17 34370267 1.6920264 ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h,m C10-C28 Diesel Range 0.00 0 N.D. ppm
9) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
10) h,m C28-C40 Oil Range 0.00 0 N.D. ppm
11) h,t,m C10-C24 Hydrocarbons 0.00 0 N.D. ppm
12) t,m,h C13-C22 Hydrocarbons 0.00 0 N.D. ppm
13) t,h,m DRO C13-22 0.00 0 N.D. ppm
14) h,m Diesel 0.00 0 N.D. ppm
15) h,m Motor Oil 0.00 0 N.D. ppm
16) h Mineral Spirits 0.00 0 N.D. ppm
17) h Kerosene 0.00 0 N.D. ppm
18) h #6 Fuel Oil 0.00 0 N.D. ppm
19) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM31A30W.M Tue Feb 07 21:44:52 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_027.d
Signal(s) : FID1A.ch
Acq On : 7 Feb 2023 8:30 pm
Operator : 614
Sample : L1582319-05 1X WG2000565
Misc : M.I.s on ranges are corrections
ALS Vial : 23 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 07 21:40:11 2023
Quant Method : C:\msdchem\1\methods\DM31A30W.M
Quant Title :
QLast Update : Mon Jan 30 10:21:43 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
Time
Response_Signal: 0207_027.d\FID1A.ch
o-
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DM31A30W.M Tue Feb 07 21:44:53 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\GCMS\1\data\020823\
Data File : 0208_27.D
Acq On : 08 Feb 2023 06:07 pm
Operator : 917
Sample : L1582319-01 1x WG2000359
Misc : WATER ISTD 23A31573 exp 07/31/23
ALS Vial : 25 Sample Multiplier: 1
Quant Time: Feb 08 20:33:34 2023
Quant Method : C:\GCMS\1\methods\S832A25W.M
Quant Title : 8270 BNA
QLast Update : Wed Jan 25 10:16:00 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.122 152 495922 8000.0000000 ppb -0.04
23) Naphthalene-d8 3.864 136 1919049 8000.0000000 ppb -0.04
46) Acenaphthene-d10 5.028 164 1144613 8000.0000000 ppb -0.04
70) Phenanthrene-d10 6.152 188 2141944 8000.0000000 ppb -0.03
84) Chrysene-d12 8.822 240 1783878 8000.0000000 ppb -0.04
94) Perylene-d12 11.387 264 1672185 8000.0000000 ppb -0.05
System Monitoring Compounds
4) 2-Fluorophenol 2.464 112 77757 979.6472551 ppb -0.03
Spiked Amount 4000.000 Range 10 - 120 Recovery = 24.49%
7) Phenol-d5 2.928 99 70995 691.0219004 ppb -0.03
Spiked Amount 4000.000 Range 10 - 120 Recovery = 17.28%
24) Nitrobenzene-d5 3.434 82 114383 1291.6901151 ppb -0.04
Spiked Amount 2000.000 Range 10 - 126 Recovery = 64.58%
50) 2-Fluorobiphenyl 4.552 172 225493 1308.2853591 ppb -0.03
Spiked Amount 2000.000 Range 22 - 127 Recovery = 65.41%
73) 2,4,6-Tribromophenol 5.611 330 65769 2445.3268507 ppb -0.03
Spiked Amount 4000.000 Range 10 - 153 Recovery = 61.13%
87) p-Terphenyl-d14 7.510 244 283575 1196.5942466 ppb -0.03
Spiked Amount 2000.000 Range 29 - 141 Recovery = 59.83%
Target Compounds Qvalue
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S832A25W.M Thu Feb 09 09:58:58 2023 Pag 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\GCMS\1\data\020823\
Data File : 0208_27.D
Acq On : 08 Feb 2023 06:07 pm
Operator : 917
Sample : L1582319-01 1x WG2000359
Misc : WATER ISTD 23A31573 exp 07/31/23
ALS Vial : 25 Sample Multiplier: 1
Quant Time: Feb 08 20:33:34 2023
Quant Method : C:\GCMS\1\methods\S832A25W.M
Quant Title : 8270 BNA
QLast Update : Wed Jan 25 10:16:00 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
5000000
5500000
6000000
6500000
7000000
7500000
8000000
8500000
9000000
Time-->
Abundance TIC: 0208_27.D\data.ms
Pe
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S832A25W.M Thu Feb 09 09:58:58 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_16.D
Acq On : 7 Feb 2023 1:19 pm
Operator : 3545
Sample : L1582319-02 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 16 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:51:19 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.404 152 215234 8000.0000000 ppb 0.00
23) Naphthalene-d8 4.151 136 809001 8000.0000000 ppb 0.00
46) Acenaphthene-d10 5.328 164 411505 8000.0000000 ppb 0.00
70) Phenanthrene-d10 6.445 188 738022 8000.0000000 ppb 0.00
84) Chrysene-d12 9.298 240 663245 8000.0000000 ppb 0.00
94) Perylene-d12 12.039 264 710220 8000.0000000 ppb 0.00
System Monitoring Compounds
4) 2-Fluorophenol 2.722 112 27501 807.6497436 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 20.19%
7) Phenol-d5 3.163 99 20902 488.6775020 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 12.22%
24) Nitrobenzene-d5 3.710 82 28056 762.6229425 ppb 0.00
Spiked Amount 2000.000 Range 10 - 126 Recovery = 38.13%
50) 2-Fluorobiphenyl 4.840 172 62418 845.1276180 ppb 0.00
Spiked Amount 2000.000 Range 22 - 127 Recovery = 42.26%
73) 2,4,6-Tribromophenol 5.904 330 18468 1606.3217334 ppb 0.00
Spiked Amount 4000.000 Range 10 - 153 Recovery = 40.16%
87) p-Terphenyl-d14 7.863 244 87237 986.6495702 ppb 0.00
Spiked Amount 2000.000 Range 29 - 141 Recovery = 49.33%
Target Compounds Qvalue
66) Diethyl phthalate 5.610 149 620 8.9138593 ppb 73
81) Di-n-butyl phthalate 6.881 149 1346m 12.4334954 ppb
92) bis(2-Ethylhexyl)phtha... 9.351 149 1881 26.8647295 ppb 96
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S826B01W.M Wed Feb 08 07:51:20 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_16.D
Acq On : 7 Feb 2023 1:19 pm
Operator : 3545
Sample : L1582319-02 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 16 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:51:19 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
100000
200000
300000
400000
500000
600000
700000
800000
900000
1000000
1100000
1200000
1300000
1400000
1500000
1600000
1700000
1800000
1900000
2000000
2100000
2200000
2300000
2400000
2500000
2600000
Time-->
Abundance TIC: 0207_16.D\data.ms
Pe
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S826B01W.M Wed Feb 08 07:51:21 2023 Page: 2
#66
Diethyl phthalate
Concen: 8.9138593 ppb
RT: 5.610 min Scan# 633
Delta R.T. -0.006 min
Lab File: 0207_16.D
Acq: 7 Feb 2023 1:19 pm
Tgt Ion:149 Resp: 620
Ion Ratio Lower Upper
149 100
177 33.6 1.1 41.1
150 0.0 0.0 32.3
176 0.0 0.0 28.3
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 634 (5.616 min): 0201_08.D\data.ms (-627) (-)
149
177761055012191 13563 222164 19337
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 633 (5.610 min): 0207_16.D\data.ms
43 14957
8471 207177
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 633 (5.610 min): 0207_16.D\data.ms (-617) (-)
149
57 7143 177
85
207
5.58 5.60 5.62 5.64
0
200
400
600
800
Time-->
Abundance
5.610
#81
Di-n-butyl phthalate
Concen: 12.4334954 ppb m
RT: 6.881 min Scan# 849
Delta R.T. -0.006 min
Lab File: 0207_16.D
Acq: 7 Feb 2023 1:19 pm
Tgt Ion:149 Resp: 1346
Ion Ratio Lower Upper
149 100
150 11.0 0.0 28.8
104 0.0 0.0 24.6
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 850 (6.886 min): 0201_08.D\data.ms (-843) (-)
149
41 104 2237657205121166 249 278
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 849 (6.881 min): 0207_16.D\data.ms
149
43 73 207
22695
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 849 (6.881 min): 0207_16.D\data.ms (-833) (-)
149
71 226539536207
6.85 6.90
0
500
1000
1500
Time-->
Abundance
6.881
0207_16.D S826B01W.M Wed Feb 08 07:51:21 2023 Page 3
#92
bis(2-Ethylhexyl)phthalate
Concen: 26.8647295 ppb
RT: 9.351 min Scan# 1269
Delta R.T. -0.006 min
Lab File: 0207_16.D
Acq: 7 Feb 2023 1:19 pm
Tgt Ion:149 Resp: 1881
Ion Ratio Lower Upper
149 100
167 25.7 7.1 47.1
279 0.0 0.0 25.1
150 10.7 0.0 31.3
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 1270 (9.357 min): 0201_08.D\data.ms (-1262) (-)
149
57 167 2284111383 279132200261
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 1269 (9.351 min): 0207_16.D\data.ms
149
240
5741 207
16784 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 1269 (9.351 min): 0207_16.D\data.ms (-1244) (-)
149
240
57 1674197 281207
9.30 9.32 9.34 9.36 9.38
0
500
1000
Time-->
Abundance
9.351
0207_16.D S826B01W.M Wed Feb 08 07:51:21 2023 Page 4
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_17.D
Acq On : 7 Feb 2023 1:40 pm
Operator : 3545
Sample : L1582319-03 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 17 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:52:38 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.404 152 197309 8000.0000000 ppb 0.00
23) Naphthalene-d8 4.151 136 746586 8000.0000000 ppb 0.00
46) Acenaphthene-d10 5.322 164 378307 8000.0000000 ppb 0.00
70) Phenanthrene-d10 6.445 188 677437 8000.0000000 ppb 0.00
84) Chrysene-d12 9.298 240 603316 8000.0000000 ppb 0.00
94) Perylene-d12 12.039 264 623462 8000.0000000 ppb 0.00
System Monitoring Compounds
4) 2-Fluorophenol 2.722 112 37684 1207.2453741 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 30.18%
7) Phenol-d5 3.163 99 28435 725.1898480 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 18.13%
24) Nitrobenzene-d5 3.710 82 41207 1213.7362633 ppb 0.00
Spiked Amount 2000.000 Range 10 - 126 Recovery = 60.69%
50) 2-Fluorobiphenyl 4.840 172 90510 1333.0294661 ppb 0.00
Spiked Amount 2000.000 Range 22 - 127 Recovery = 66.65%
73) 2,4,6-Tribromophenol 5.904 330 25619 2427.5894318 ppb 0.00
Spiked Amount 4000.000 Range 10 - 153 Recovery = 60.69%
87) p-Terphenyl-d14 7.863 244 120146 1493.8282460 ppb 0.00
Spiked Amount 2000.000 Range 29 - 141 Recovery = 74.69%
Target Compounds Qvalue
8) Phenol 3.169 94 1053 25.8332570 ppb # 30
31) Benzoic Acid 3.922 105 1669m 94.9054319 ppb
34) Naphthalene 4.163 128 716 7.0780788 ppb 83
66) Diethyl phthalate 5.610 149 635 9.9306700 ppb 84
81) Di-n-butyl phthalate 6.881 149 988 9.9427271 ppb 82
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S826B01W.M Wed Feb 08 07:52:39 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_17.D
Acq On : 7 Feb 2023 1:40 pm
Operator : 3545
Sample : L1582319-03 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 17 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:52:38 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
100000
200000
300000
400000
500000
600000
700000
800000
900000
1000000
1100000
1200000
1300000
1400000
1500000
1600000
1700000
1800000
1900000
2000000
2100000
2200000
2300000
2400000
Time-->
Abundance TIC: 0207_17.D\data.ms
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8
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S826B01W.M Wed Feb 08 07:52:39 2023 Page: 2
#8
Phenol
Concen: 25.8332570 ppb
RT: 3.169 min Scan# 218
Delta R.T. -0.005 min
Lab File: 0207_17.D
Acq: 7 Feb 2023 1:40 pm
Tgt Ion: 94 Resp: 1053
Ion Ratio Lower Upper
94 100
66 100.9 15.5 55.5#
65 51.7 8.4 48.4#
39 45.7 5.4 45.4#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 219 (3.175 min): 0201_08.D\data.ms (-214) (-)
94
6639
113
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 218 (3.169 min): 0207_17.D\data.ms
99
49 71
207147 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 218 (3.169 min): 0207_17.D\data.ms (-193) (-)
99
7142
147 207 281
3.14 3.16 3.18 3.20
0
500
1000
1500
2000
Time-->
Abundance
3.169
#31
Benzoic Acid
Concen: 94.9054319 ppb m
RT: 3.922 min Scan# 346
Delta R.T. -0.053 min
Lab File: 0207_17.D
Acq: 7 Feb 2023 1:40 pm
Tgt Ion:105 Resp: 1669
Ion Ratio Lower Upper
105 100
77 6.7 55.3 95.3#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 351 (3.951 min): 0116_16.D\data.ms (-347) (-)
105 12277
51
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 346 (3.922 min): 0207_17.D\data.ms
49
84
105 122 207147 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 346 (3.922 min): 0207_17.D\data.ms (-338) (-)
10577 122
51
3.88 3.90 3.92 3.94 3.96
0
500
1000
Time-->
Abundance
3.922
0207_17.D S826B01W.M Wed Feb 08 07:52:39 2023 Page 3
#34
Naphthalene
Concen: 7.0780788 ppb
RT: 4.163 min Scan# 387
Delta R.T. -0.006 min
Lab File: 0207_17.D
Acq: 7 Feb 2023 1:40 pm
Tgt Ion:128 Resp: 716
Ion Ratio Lower Upper
128 100
129 0.0 0.0 31.3
127 16.9 0.0 34.9
102 0.0 0.0 28.1
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 388 (4.169 min): 0201_08.D\data.ms (-381) (-)
128
51 10274 221 281193
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 387 (4.163 min): 0207_17.D\data.ms
136
49 84
108 20768
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 387 (4.163 min): 0207_17.D\data.ms (-371) (-)
136
54 1087637 207
4.12 4.14 4.16 4.18
0
1000
2000
3000
Time-->
Abundance
4.163
#66
Diethyl phthalate
Concen: 9.9306700 ppb
RT: 5.610 min Scan# 633
Delta R.T. -0.006 min
Lab File: 0207_17.D
Acq: 7 Feb 2023 1:40 pm
Tgt Ion:149 Resp: 635
Ion Ratio Lower Upper
149 100
177 23.4 1.1 41.1
150 0.0 0.0 32.3
176 0.0 0.0 28.3
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 634 (5.616 min): 0201_08.D\data.ms (-627) (-)
149
177761055012191 13563 222164 19337
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 633 (5.610 min): 0207_17.D\data.ms
64
192
49 84 128 14998 20736177
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 633 (5.610 min): 0207_17.D\data.ms (-617) (-)
64
192
128 14996 17750 7736
5.58 5.60 5.62 5.64
0
200
400
600
800
1000
Time-->
Abundance
5.610
0207_17.D S826B01W.M Wed Feb 08 07:52:39 2023 Page 4
#81
Di-n-butyl phthalate
Concen: 9.9427271 ppb
RT: 6.881 min Scan# 849
Delta R.T. -0.006 min
Lab File: 0207_17.D
Acq: 7 Feb 2023 1:40 pm
Tgt Ion:149 Resp: 988
Ion Ratio Lower Upper
149 100
150 16.3 0.0 28.8
104 0.0 0.0 24.6
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 850 (6.886 min): 0201_08.D\data.ms (-843) (-)
149
41 104 2237657205121166 249 278
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 849 (6.881 min): 0207_17.D\data.ms
66
49 98 149 207128175
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 849 (6.881 min): 0207_17.D\data.ms (-833) (-)
66
149
12998 20541175
6.85 6.90
0
200
400
600
800
Time-->
Abundance
6.881
0207_17.D S826B01W.M Wed Feb 08 07:52:40 2023 Page 5
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_18.D
Acq On : 7 Feb 2023 2:02 pm
Operator : 3545
Sample : L1582319-04 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 18 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:54:21 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.398 152 282660 8000.0000000 ppb 0.00
23) Naphthalene-d8 4.151 136 1048421 8000.0000000 ppb 0.00
46) Acenaphthene-d10 5.328 164 520365 8000.0000000 ppb 0.00
70) Phenanthrene-d10 6.451 188 898507 8000.0000000 ppb 0.00
84) Chrysene-d12 9.298 240 737802 8000.0000000 ppb 0.00
94) Perylene-d12 12.045 264 740411 8000.0000000 ppb 0.00
System Monitoring Compounds
4) 2-Fluorophenol 2.722 112 53143 1188.4123683 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 29.71%
7) Phenol-d5 3.163 99 40003 712.1534560 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 17.80%
24) Nitrobenzene-d5 3.710 82 50422 1057.5904697 ppb 0.00
Spiked Amount 2000.000 Range 10 - 126 Recovery = 52.88%
50) 2-Fluorobiphenyl 4.840 172 113780 1218.2752274 ppb 0.00
Spiked Amount 2000.000 Range 22 - 127 Recovery = 60.91%
73) 2,4,6-Tribromophenol 5.904 330 32888 2349.6218729 ppb 0.00
Spiked Amount 4000.000 Range 10 - 153 Recovery = 58.74%
87) p-Terphenyl-d14 7.863 244 138837 1411.5672907 ppb 0.00
Spiked Amount 2000.000 Range 29 - 141 Recovery = 70.58%
Target Compounds Qvalue
8) Phenol 3.169 94 984 16.8511068 ppb # 68
31) Benzoic Acid 3.922 105 815 33.0017122 ppb 93
33) alpha-terpineol 4.151 59 1722 46.7670945 ppb 89
34) Naphthalene 4.163 128 877 6.1737082 ppb 88
41) 2-Methylnaphthalene 4.604 142 1632m 19.0500979 ppb
42) 1-Methylnaphthalene 4.669 142 1107 13.6718137 ppb 98
51) Biphenyl 4.910 154 844 8.0642368 ppb 94
58) Acenaphthene 5.345 153 780 9.0394622 ppb 90
66) Diethyl phthalate 5.610 149 936 10.6418460 ppb 91
78) Phenanthrene 6.469 178 2206m 17.2783501 ppb
81) Di-n-butyl phthalate 6.886 149 1652 12.5344726 ppb 90
83) Fluoranthene 7.481 202 435 3.5647476 ppb # 62
86) Pyrene 7.710 202 769 6.2963819 ppb # 58
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S826B01W.M Wed Feb 08 07:54:23 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_18.D
Acq On : 7 Feb 2023 2:02 pm
Operator : 3545
Sample : L1582319-04 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 18 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:54:21 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
200000
400000
600000
800000
1000000
1200000
1400000
1600000
1800000
2000000
2200000
2400000
2600000
2800000
3000000
3200000
Time-->
Abundance TIC: 0207_18.D\data.ms
Pe
r
y
l
e
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-
d
1
2
,
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Ch
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y
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S826B01W.M Wed Feb 08 07:54:23 2023 Page: 2
#8
Phenol
Concen: 16.8511068 ppb
RT: 3.169 min Scan# 218
Delta R.T. -0.005 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion: 94 Resp: 984
Ion Ratio Lower Upper
94 100
66 70.6 15.5 55.5#
65 36.0 8.4 48.4
39 31.7 5.4 45.4
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 219 (3.175 min): 0201_08.D\data.ms (-214) (-)
94
6639
113
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 218 (3.169 min): 0207_18.D\data.ms
99
7149
207147 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 218 (3.169 min): 0207_18.D\data.ms (-193) (-)
99
7142
207147
3.14 3.16 3.18
0
500
1000
1500
2000
2500
Time-->
Abundance
3.169
#31
Benzoic Acid
Concen: 33.0017122 ppb
RT: 3.922 min Scan# 346
Delta R.T. -0.053 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:105 Resp: 815
Ion Ratio Lower Upper
105 100
77 69.3 55.3 95.3
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 351 (3.951 min): 0116_16.D\data.ms (-347) (-)
105
77
51
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 346 (3.922 min): 0207_18.D\data.ms
49
84 207
122147 281 341 415
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 346 (3.922 min): 0207_18.D\data.ms (-338) (-)
10577
51
147 207 415
281
3.90 3.95
0
200
400
Time-->
Abundance
3.922
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 3
#33
alpha-terpineol
Concen: 46.7670945 ppb
RT: 4.151 min Scan# 385
Delta R.T. 0.000 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion: 59 Resp: 1722
Ion Ratio Lower Upper
59 100
93 57.1 29.9 69.9
121 32.2 19.4 59.4
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 387 (4.163 min): 0116_16.D\data.ms (-383) (-)
136
59 934377 118
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 385 (4.151 min): 0207_18.D\data.ms
136
54 10876 193 28138221
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 385 (4.151 min): 0207_18.D\data.ms (-368) (-)
136
1085482 208 28138
4.10 4.12 4.14 4.16 4.18
0
500
1000
1500
Time-->
Abundance
4.151
#34
Naphthalene
Concen: 6.1737082 ppb
RT: 4.163 min Scan# 387
Delta R.T. -0.006 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:128 Resp: 877
Ion Ratio Lower Upper
128 100
129 16.3 0.0 31.3
127 16.9 0.0 34.9
102 0.0 0.0 28.1
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 388 (4.169 min): 0201_08.D\data.ms (-381) (-)
128
51 10274 221 281193
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 387 (4.163 min): 0207_18.D\data.ms
136
49 84 10868 207
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 387 (4.163 min): 0207_18.D\data.ms (-371) (-)
136
1085478 20736
4.12 4.14 4.16 4.18
0
1000
2000
3000
4000
Time-->
Abundance
4.163
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 4
#41
2-Methylnaphthalene
Concen: 19.0500979 ppb m
RT: 4.604 min Scan# 462
Delta R.T. 0.000 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:142 Resp: 1632
Ion Ratio Lower Upper
142 100
141 63.8 70.8 106.2#
115 21.6 25.2 37.8#
139 8.0 8.6 13.0#
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 462 (4.604 min): 0201_08.D\data.ms (-456) (-)
142
115
6339 89 207 371 399
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 462 (4.604 min): 0207_18.D\data.ms
14249
84
115 207
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 462 (4.604 min): 0207_18.D\data.ms (-445) (-)
142
43 115
91
4.56 4.58 4.60 4.62 4.64
0
500
1000
1500
Time-->
Abundance
4.604
#42
1-Methylnaphthalene
Concen: 13.6718137 ppb
RT: 4.669 min Scan# 473
Delta R.T. -0.006 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:142 Resp: 1107
Ion Ratio Lower Upper
142 100
141 93.9 73.9 110.9
115 31.8 26.3 39.5
139 11.8 9.2 13.8
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 474 (4.675 min): 0201_08.D\data.ms (-468) (-)
142
115
63 8939 10276 128 193 207
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 473 (4.669 min): 0207_18.D\data.ms
14249
84
115 2076936 221
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 473 (4.669 min): 0207_18.D\data.ms (-457) (-)
142
1156945 22183
4.64 4.66 4.68 4.70
0
500
1000
1500
Time-->
Abundance
4.669
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 5
#51
Biphenyl
Concen: 8.0642368 ppb
RT: 4.910 min Scan# 514
Delta R.T. 0.000 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:154 Resp: 844
Ion Ratio Lower Upper
154 100
153 44.7 32.8 49.2
152 29.9 21.7 32.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 514 (4.910 min): 0201_08.D\data.ms (-508) (-)
154
7651 128115102648938 141 198 216
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 514 (4.910 min): 0207_18.D\data.ms
15449
84
2071356936107
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 514 (4.910 min): 0207_18.D\data.ms (-497) (-)
154
1357736 107
4.88 4.90 4.92 4.94
0
500
1000
Time-->
Abundance
4.910
#58
Acenaphthene
Concen: 9.0394622 ppb
RT: 5.345 min Scan# 588
Delta R.T. -0.006 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:153 Resp: 780
Ion Ratio Lower Upper
153 100
154 78.9 72.3 112.3
152 45.7 24.9 64.9
151 22.9 0.0 37.0
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 589 (5.351 min): 0201_08.D\data.ms (-582) (-)
153
7663 184519110712638139167 196
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 588 (5.345 min): 0207_18.D\data.ms
16249
84
2076919336
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 588 (5.345 min): 0207_18.D\data.ms (-572) (-)
162
764059 95 193
5.30 5.32 5.34 5.36 5.38
0
500
1000
1500
2000
Time-->
Abundance
5.345
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 6
#66
Diethyl phthalate
Concen: 10.6418460 ppb
RT: 5.610 min Scan# 633
Delta R.T. -0.006 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:149 Resp: 936
Ion Ratio Lower Upper
149 100
177 24.9 1.1 41.1
150 11.5 0.0 32.3
176 0.0 0.0 28.3
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 634 (5.616 min): 0201_08.D\data.ms (-627) (-)
149
177761055012191 13563 222164 19337
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 633 (5.610 min): 0207_18.D\data.ms
14943 57
71 84
207177105193
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 633 (5.610 min): 0207_18.D\data.ms (-617) (-)
1495771
43
85 177105
207
5.58 5.60 5.62 5.64
0
500
1000
Time-->
Abundance
5.610
#78
Phenanthrene
Concen: 17.2783501 ppb m
RT: 6.469 min Scan# 779
Delta R.T. 0.000 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:178 Resp: 2206
Ion Ratio Lower Upper
178 100
179 15.4 0.0 35.1
152 11.4 0.0 29.8
89 11.1 0.0 29.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 779 (6.469 min): 0201_08.D\data.ms (-772) (-)
178
15276896350126139111 16537 221
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 779 (6.469 min): 0207_18.D\data.ms
188
43 84 2075715271105 137
40 60 80 100 120 140 160 180 200 220
0
50
m/z-->
Abundance Scan 779 (6.469 min): 0207_18.D\data.ms (-762) (-)
188
948043 15266137 207
6.44 6.46 6.48
0
1000
2000
Time-->
Abundance
6.469
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 7
#81
Di-n-butyl phthalate
Concen: 12.5344726 ppb
RT: 6.886 min Scan# 850
Delta R.T. 0.000 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:149 Resp: 1652
Ion Ratio Lower Upper
149 100
150 11.6 0.0 28.8
104 0.0 0.0 24.6
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 850 (6.886 min): 0201_08.D\data.ms (-843) (-)
149
41 104 2237657205121166 249 278
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 850 (6.886 min): 0207_18.D\data.ms
149 207
41
73
97 125 190 231 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 850 (6.886 min): 0207_18.D\data.ms (-833) (-)
149 205
41 70 125105 233188 281
6.84 6.86 6.88 6.90 6.92
0
500
1000
1500
Time-->
Abundance
6.886
#83
Fluoranthene
Concen: 3.5647476 ppb
RT: 7.481 min Scan# 951
Delta R.T. 0.000 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:202 Resp: 435
Ion Ratio Lower Upper
202 100
203 30.5 0.0 37.0
201 0.0 0.0 35.3
200 0.0 0.7 40.7#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 951 (7.481 min): 0201_08.D\data.ms (-941) (-)
202
101 174741503912255
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 951 (7.481 min): 0207_18.D\data.ms
59
43 11784 207147 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 951 (7.481 min): 0207_18.D\data.ms (-934) (-)
59
117 2024197 14777
7.46 7.48 7.50
0
100
200
300
400
Time-->
Abundance
7.481
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 8
#86
Pyrene
Concen: 6.2963819 ppb
RT: 7.710 min Scan# 990
Delta R.T. -0.006 min
Lab File: 0207_18.D
Acq: 7 Feb 2023 2:02 pm
Tgt Ion:202 Resp: 769
Ion Ratio Lower Upper
202 100
203 0.0 0.0 37.4
201 0.0 0.0 37.9
200 0.0 1.4 41.4#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 991 (7.716 min): 0201_08.D\data.ms (-982) (-)
202
10188 174150746212250138 162 18737
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 990 (7.710 min): 0207_18.D\data.ms
20249
84
147976736 135
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 990 (7.710 min): 0207_18.D\data.ms (-974) (-)
202
135 14749
7.68 7.70 7.72 7.74
0
200
400
600
800
Time-->
Abundance
7.710
0207_18.D S826B01W.M Wed Feb 08 07:54:23 2023 Page 9
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_19.D
Acq On : 7 Feb 2023 2:23 pm
Operator : 3545
Sample : L1582319-05 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 19 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:55:21 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.405 152 223919 8000.0000000 ppb 0.00
23) Naphthalene-d8 4.152 136 856157 8000.0000000 ppb 0.00
46) Acenaphthene-d10 5.328 164 434530 8000.0000000 ppb 0.00
70) Phenanthrene-d10 6.451 188 790256 8000.0000000 ppb 0.00
84) Chrysene-d12 9.298 240 701068 8000.0000000 ppb 0.00
94) Perylene-d12 12.045 264 721517 8000.0000000 ppb 0.00
System Monitoring Compounds
4) 2-Fluorophenol 2.722 112 37890 1069.5943734 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 26.74%
7) Phenol-d5 3.163 99 28845 648.2238053 ppb 0.00
Spiked Amount 4000.000 Range 10 - 120 Recovery = 16.21%
24) Nitrobenzene-d5 3.710 82 37326 958.7187293 ppb 0.00
Spiked Amount 2000.000 Range 10 - 126 Recovery = 47.94%
50) 2-Fluorobiphenyl 4.840 172 85338 1094.2341303 ppb 0.00
Spiked Amount 2000.000 Range 22 - 127 Recovery = 54.71%
73) 2,4,6-Tribromophenol 5.904 330 25564 2076.5528300 ppb 0.00
Spiked Amount 4000.000 Range 10 - 153 Recovery = 51.91%
87) p-Terphenyl-d14 7.863 244 117676 1259.1107932 ppb 0.00
Spiked Amount 2000.000 Range 29 - 141 Recovery = 62.96%
Target Compounds Qvalue
8) Phenol 3.169 94 1979 42.7811581 ppb # 65
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S826B01W.M Wed Feb 08 07:55:22 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\020723\
Data File : 0207_19.D
Acq On : 7 Feb 2023 2:23 pm
Operator : 3545
Sample : L1582319-05 1x WG2000359
Misc : WATER ISTD 23A31573 exp 06/31/23
ALS Vial : 19 Sample Multiplier: 1
InstName : BNAMS26
Quant Time: Feb 08 07:55:21 2023
Quant Method : C:\msdchem\1\methods\S826B01W.M
Quant Title : 8270 BNA
QLast Update : Thu Feb 02 09:55:30 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
100000
200000
300000
400000
500000
600000
700000
800000
900000
1000000
1100000
1200000
1300000
1400000
1500000
1600000
1700000
1800000
1900000
2000000
2100000
2200000
2300000
2400000
2500000
2600000
2700000
2800000
Time-->
Abundance TIC: 0207_19.D\data.ms
Pe
r
y
l
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n
e
-
d
1
2
,
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S826B01W.M Wed Feb 08 07:55:22 2023 Page: 2
#8
Phenol
Concen: 42.7811581 ppb
RT: 3.169 min Scan# 218
Delta R.T. -0.005 min
Lab File: 0207_19.D
Acq: 7 Feb 2023 2:23 pm
Tgt Ion: 94 Resp: 1979
Ion Ratio Lower Upper
94 100
66 69.0 15.5 55.5#
65 37.7 8.4 48.4
39 37.6 5.4 45.4
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 219 (3.175 min): 0201_08.D\data.ms (-214) (-)
94
6639
113
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 218 (3.169 min): 0207_19.D\data.ms
99
7149
207147 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 218 (3.169 min): 0207_19.D\data.ms (-193) (-)
99
7142
193 221147 281
3.14 3.16 3.18 3.20
0
500
1000
1500
2000
Time-->
Abundance
3.169
0207_19.D S826B01W.M Wed Feb 08 07:55:22 2023 Page 3
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021523\
Data File : 0215_18.D
Acq On : 15 Feb 2023 3:20 pm
Operator : 3895
Sample : L1584351-01 1x WG2004703
Misc : SOIL ISTD 23B06326 exp 08/06/23
ALS Vial : 33 Sample Multiplier: 1
InstName : BNAMS11
Quant Time: Feb 16 11:40:56 2023
Quant Method : C:\msdchem\1\methods\S811B14W.M
Quant Title : 8270 BNA
QLast Update : Tue Feb 14 16:17:59 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.286 152 80939 8000.0000000 ppb 0.00
23) Naphthalene-d8 4.008 136 317392 8000.0000000 ppb 0.00
46) Acenaphthene-d10 5.160 164 178808 8000.0000000 ppb 0.00
70) Phenanthrene-d10 6.270 188 335855 8000.0000000 ppb 0.00
84) Chrysene-d12 8.967 240 320336 8000.0000000 ppb 0.00
94) Perylene-d12 11.570 264 345164 8000.0000000 ppb 0.00
System Monitoring Compounds
4) 2-Fluorophenol 2.633 112 141587 10985.1161404 ppb 0.02
Spiked Amount 20000.000 Range 20 - 120 Recovery = 54.93%
7) Phenol-d5 3.068 99 163546 9909.9343906 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 49.55%
24) Nitrobenzene-d5 3.585 82 64520m 4291.9304567 ppb 0.00
Spiked Amount 10000.000 Range 18 - 125 Recovery = 42.92%
50) 2-Fluorobiphenyl 4.684 172 154882 5125.0179176 ppb 0.00
Spiked Amount 10000.000 Range 28 - 120 Recovery = 51.25%
73) 2,4,6-Tribromophenol 5.736 330 55147 14409.7294012 ppb 0.00
Spiked Amount 20000.000 Range 17 - 137 Recovery = 72.05%
87) p-Terphenyl-d14 7.634 244 243625 5876.5801929 ppb 0.00
Spiked Amount 10000.000 Range 13 - 131 Recovery = 58.77%
Target Compounds Qvalue
22) Acetophenone 3.485 105 21127 1096.9778597 ppb # 43
83) Fluoranthene 7.263 202 8657 181.7745970 ppb 97
86) Pyrene 7.481 202 15354 298.0992427 ppb 96
90) Benzo(a)anthracene 8.950 228 9572 193.4570120 ppb 90
91) Chrysene 9.003 228 9947m 208.5131318 ppb
92) bis(2-Ethylhexyl)phtha... 9.032 149 57310 1722.3971604 ppb 97
95) Benzo(b)fluoranthene 10.818 252 13641 263.5665666 ppb 82
97) Benzo(a)pyrene 11.447 252 8648 191.5279104 ppb 88
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S811B14W.M Thu Feb 16 11:41:09 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021523\
Data File : 0215_18.D
Acq On : 15 Feb 2023 3:20 pm
Operator : 3895
Sample : L1584351-01 1x WG2004703
Misc : SOIL ISTD 23B06326 exp 08/06/23
ALS Vial : 33 Sample Multiplier: 1
InstName : BNAMS11
Quant Time: Feb 16 11:40:56 2023
Quant Method : C:\msdchem\1\methods\S811B14W.M
Quant Title : 8270 BNA
QLast Update : Tue Feb 14 16:17:59 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
200000
400000
600000
800000
1000000
1200000
1400000
1600000
1800000
2000000
2200000
2400000
2600000
2800000
3000000
3200000
3400000
3600000
Time-->
Abundance TIC: 0215_18.D\data.ms
Pe
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-
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1
2
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(
a
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p
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S811B14W.M Thu Feb 16 11:41:09 2023 Page: 2
#22
Acetophenone
Concen: 1096.9778597 ppb
RT: 3.485 min Scan# 273
Delta R.T. -0.012 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:105 Resp: 21127
Ion Ratio Lower Upper
105 100
77 23.3 65.2 97.8#
51 11.0 26.7 40.1#
120 0.0 23.0 34.4#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260
0
50
m/z-->
Abundance Scan 275 (3.497 min): 0214A_03.D\data.ms (-271) (-)
10577
51
121 207 267
40 60 80 100 120 140 160 180 200 220 240 260
0
50
m/z-->
Abundance Scan 273 (3.485 min): 0215_18.D\data.ms
105
6941
134
85 154 207
40 60 80 100 120 140 160 180 200 220 240 260
0
50
m/z-->
Abundance Scan 273 (3.485 min): 0215_18.D\data.ms (-147) (-)
105
134
67 83 154
3.46 3.48 3.50 3.52
0
5000
10000
15000
20000
25000
Time-->
Abundance
3.485
#83
Fluoranthene
Concen: 181.7745970 ppb
RT: 7.263 min Scan# 916
Delta R.T. 0.000 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:202 Resp: 8657
Ion Ratio Lower Upper
202 100
203 18.7 0.0 37.3
201 12.6 0.0 34.8
200 20.9 0.3 40.3
Ref
Raw
Sub
40 60 80 100120140160180200220240260280300
0
50
m/z-->
Abundance Scan 916 (7.263 min): 0214A_02.D\data.ms (-907) (-)
202
101 1747415012250 228
40 60 80 100120140160180200220240260280300
0
50
m/z-->
Abundance Scan 916 (7.263 min): 0215_18.D\data.ms
55
97
202
123 14977 179 221 250 272 304
40 60 80 100120140160180200220240260280300
0
50
m/z-->
Abundance Scan 916 (7.263 min): 0215_18.D\data.ms (-865) (-)
57 202
83 111
139 165 250221 272 30438
7.25 7.30
0
2000
4000
6000
8000
10000
Time-->
Abundance
7.263
0215_18.D S811B14W.M Thu Feb 16 11:41:09 2023 Page 3
#86
Pyrene
Concen: 298.0992427 ppb
RT: 7.481 min Scan# 953
Delta R.T. 0.000 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:202 Resp: 15354
Ion Ratio Lower Upper
202 100
203 20.6 0.0 36.5
201 17.4 0.0 37.2
200 19.8 0.5 40.5
Ref
Raw
Sub
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 953 (7.481 min): 0214A_02.D\data.ms (-948) (-)
202
101
17475 15012250
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 953 (7.481 min): 0215_18.D\data.ms
55
83
202111
149 177 223 273243 302 323
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 953 (7.481 min): 0215_18.D\data.ms (-902) (-)
2028355
111
139 284163226259 305 328
7.45 7.50 7.55
0
5000
10000
Time-->
Abundance
7.481
#90
Benzo(a)anthracene
Concen: 193.4570120 ppb
RT: 8.950 min Scan# 1203
Delta R.T. -0.006 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:228 Resp: 9572
Ion Ratio Lower Upper
228 100
226 31.2 6.2 46.2
114 19.4 0.0 33.2
113 14.0 0.0 32.0
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1204 (8.956 min): 0214A_02.D\data.ms (-1196) (-)
228
114 2008817415139 63
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1203 (8.950 min): 0215_18.D\data.ms
57 240
97
125 151 179 208 315263287338361 390
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1203 (8.950 min): 0215_18.D\data.ms (-1178) (-)
240
120 2129218067152 277 338 36540305
8.90 8.95
0
2000
4000
6000
Time-->
Abundance
8.950
0215_18.D S811B14W.M Thu Feb 16 11:41:09 2023 Page 4
#91
Chrysene
Concen: 208.5131318 ppb m
RT: 9.003 min Scan# 1212
Delta R.T. -0.006 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:228 Resp: 9947
Ion Ratio Lower Upper
228 100
226 32.0 8.3 48.3
229 35.7 0.0 39.4
113 81.1 0.0 32.7#
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1213 (9.008 min): 0214A_02.D\data.ms (-1208) (-)
228
113 2008817550149
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1212 (9.003 min): 0215_18.D\data.ms
57
97
125 228151179203251 302326349372274
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1212 (9.003 min): 0215_18.D\data.ms (-1187) (-)
228
113 13781 175 202 343259 36831350282
8.98 9.00 9.02 9.04 9.06
0
2000
4000
6000
Time-->
Abundance
9.003
#92
bis(2-Ethylhexyl)phthalate
Concen: 1722.3971604 ppb
RT: 9.032 min Scan# 1217
Delta R.T. 0.000 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:149 Resp: 57310
Ion Ratio Lower Upper
149 100
167 28.8 9.8 49.8
279 7.5 0.0 26.4
150 12.3 0.0 30.3
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1217 (9.032 min): 0214A_02.D\data.ms (-1209) (-)
149
57
113 27983174 221
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1217 (9.032 min): 0215_18.D\data.ms
57
149
97
125
179 279207240302326350374
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1217 (9.032 min): 0215_18.D\data.ms (-1166) (-)
149
57
97 279240122 324 390209353186
8.95 9.00 9.05 9.10
0
10000
20000
30000
40000
Time-->
Abundance
9.032
0215_18.D S811B14W.M Thu Feb 16 11:41:09 2023 Page 5
#95
Benzo(b)fluoranthene
Concen: 263.5665666 ppb
RT: 10.818 min Scan# 1521
Delta R.T. 0.000 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:252 Resp: 13641
Ion Ratio Lower Upper
252 100
253 22.4 1.4 41.4
126 1.1 0.0 36.4
113 0.0 0.0 28.0
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1521 (10.818 min): 0214A_02.D\data.ms (-1512) (-)
252
126 2241007519917439
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1521 (10.818 min): 0215_18.D\data.ms
57
97
123 252149179 207 289 315 357382 412
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1521 (10.818 min): 0215_18.D\data.ms (-1504) (-)
252
58 125 163 292193 386225347 41832086
10.75 10.80 10.85
0
2000
4000
6000
Time-->
Abundance
10.818
#97
Benzo(a)pyrene
Concen: 191.5279104 ppb
RT: 11.447 min Scan# 1628
Delta R.T. -0.006 min
Lab File: 0215_18.D
Acq: 15 Feb 2023 3:20 pm
Tgt Ion:252 Resp: 8648
Ion Ratio Lower Upper
252 100
253 18.4 0.3 40.3
126 20.9 0.0 36.6
113 21.0 0.0 29.8
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1629 (11.453 min): 0214A_02.D\data.ms (-1619) (-)
252
126 22410074198 28115839
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1628 (11.447 min): 0215_18.D\data.ms
57
83
111
149 252207179 281 309 341 372400426
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1628 (11.447 min): 0215_18.D\data.ms (-1578) (-)
252
54
82
126 294168 396346225197 428
11.40 11.45 11.50 11.55
0
5000
10000
Time-->
Abundance
11.447
0215_18.D S811B14W.M Thu Feb 16 11:41:09 2023 Page 6
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021523B\
Data File : 0215B_28.D
Acq On : 16 Feb 2023 9:07 am
Operator : 3895
Sample : L1584351-02 5X WG2004454
Misc : SOIL ISTD 23A27189 exp 07/11/23
ALS Vial : 29 Sample Multiplier: 1
InstName : BNAMS2
Quant Time: Feb 16 15:05:47 2023
Quant Method : C:\msdchem\1\methods\S802A28W.M
Quant Title : 8270 BNA
QLast Update : Sat Jan 28 11:40:58 2023
Response via : Initial Calibration
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 3.433 152 181895 8000.0000000 ppb 0.00
23) Naphthalene-d8 4.167 136 683437 8000.0000000 ppb 0.00
46) Acenaphthene-d10 5.342 164 330834 8000.0000000 ppb 0.00
70) Phenanthrene-d10 6.464 188 679975 8000.0000000 ppb 0.00
84) Chrysene-d12 9.326 240 655396 8000.0000000 ppb 0.00
94) Perylene-d12 12.081 264 696924 8000.0000000 ppb 0.00
System Monitoring Compounds
4) 2-Fluorophenol 2.775 112 62729 2123.5573472 ppb 0.01
Spiked Amount 20000.000 Range 20 - 120 Recovery = 10.62%#
7) Phenol-d5 3.209 99 66170 1860.5460289 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 9.30%#
24) Nitrobenzene-d5 3.738 82 55866 1994.7168220 ppb 0.00
Spiked Amount 10000.000 Range 18 - 125 Recovery = 19.95%
50) 2-Fluorobiphenyl 4.855 172 60754 1083.9852118 ppb 0.00
Spiked Amount 10000.000 Range 28 - 120 Recovery = 10.84%#
73) 2,4,6-Tribromophenol 5.924 330 23049 2439.6670553 ppb 0.00
Spiked Amount 20000.000 Range 17 - 137 Recovery = 12.20%#
87) p-Terphenyl-d14 7.886 244 99769 1067.7124528 ppb 0.00
Spiked Amount 10000.000 Range 13 - 131 Recovery = 10.68%#
Target Compounds Qvalue
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S802A28W.M Thu Feb 16 15:05:50 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021523B\
Data File : 0215B_28.D
Acq On : 16 Feb 2023 9:07 am
Operator : 3895
Sample : L1584351-02 5X WG2004454
Misc : SOIL ISTD 23A27189 exp 07/11/23
ALS Vial : 29 Sample Multiplier: 1
InstName : BNAMS2
Quant Time: Feb 16 15:05:47 2023
Quant Method : C:\msdchem\1\methods\S802A28W.M
Quant Title : 8270 BNA
QLast Update : Sat Jan 28 11:40:58 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
2000000
4000000
6000000
8000000
1e+07
1.2e+07
1.4e+07
1.6e+07
1.8e+07
2e+07
2.2e+07
2.4e+07
2.6e+07
2.8e+07
3e+07
3.2e+07
Time-->
Abundance TIC: 0215B_28.D\data.ms
Pe
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y
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-
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1
2
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S802A28W.M Thu Feb 16 15:05:50 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021123A\
Data File : 0211A_20.D
Acq On : 12 Feb 2023 2:11 am
Operator : 3895
Sample : L1584351-03 1X WG2004454
Misc : SOIL ISTD 23A31573 exp 07/31/23
ALS Vial : 76 Sample Multiplier: 1
Quant Time: Feb 13 10:45:06 2023
Quant Method : C:\msdchem\1\methods\S823B10W.M
Quant Title : 8270 BNA
QLast Update : Fri Feb 10 16:31:46 2023
Response via : Initial Calibration
DataAcq Meth:BNA23PS.M
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 2.984 152 49725 8000.0000000 ppb -0.02
23) Naphthalene-d8 3.702 136 196824 8000.0000000 ppb -0.02
46) Acenaphthene-d10 4.825 164 109296 8000.0000000 ppb -0.02
70) Phenanthrene-d10 5.913 188 194195 8000.0000000 ppb -0.02
84) Chrysene-d12 8.378 240 168515 8000.0000000 ppb -0.04
94) Perylene-d12 10.713 264 177821 8000.0000000 ppb -0.06
System Monitoring Compounds
4) 2-Fluorophenol 2.337 112 105729 13900.6742471 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 69.50%
7) Phenol-d5 2.778 99 115552 12073.9871649 ppb -0.01
Spiked Amount 20000.000 Range 20 - 120 Recovery = 60.37%
24) Nitrobenzene-d5 3.290 82 49151 6075.8794580 ppb -0.02
Spiked Amount 10000.000 Range 18 - 125 Recovery = 60.76%
50) 2-Fluorobiphenyl 4.366 172 121469 6716.7087385 ppb -0.02
Spiked Amount 10000.000 Range 28 - 120 Recovery = 67.17%
73) 2,4,6-Tribromophenol 5.390 330 36523 17216.4896461 ppb -0.02
Spiked Amount 20000.000 Range 17 - 137 Recovery = 86.08%
87) p-Terphenyl-d14 7.213 244 170671 7959.9145768 ppb -0.03
Spiked Amount 10000.000 Range 13 - 131 Recovery = 79.60%
Target Compounds Qvalue
9) Benzaldehyde 2.755 105 2475m 1510.0462310 ppb
21) 3&4-Methyl phenol 3.190 107 7848 952.0822250 ppb 94
37) Hydroquinone 3.931 110 1562 311.6046662 ppb 91
78) Phenanthrene 5.931 178 12092 459.5413621 ppb 96
83) Fluoranthene 6.866 202 15716 614.3017286 ppb 94
86) Pyrene 7.060 202 14299 525.2693656 ppb 97
90) Benzo(a)anthracene 8.366 228 6980 292.5948502 ppb 94
91) Chrysene 8.413 228 6575m 264.8590293 ppb
95) Benzo(b)fluoranthene 10.031 252 9535 366.7017810 ppb 90
97) Benzo(a)pyrene 10.607 252 7145 320.8067327 ppb 91
100) Benzo(g,h,i)perylene 13.207 276 6920 292.0106499 ppb 95
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S823B10W.M Mon Feb 13 10:45:12 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021123A\
Data File : 0211A_20.D
Acq On : 12 Feb 2023 2:11 am
Operator : 3895
Sample : L1584351-03 1X WG2004454
Misc : SOIL ISTD 23A31573 exp 07/31/23
ALS Vial : 76 Sample Multiplier: 1
Quant Time: Feb 13 10:45:06 2023
Quant Method : C:\msdchem\1\methods\S823B10W.M
Quant Title : 8270 BNA
QLast Update : Fri Feb 10 16:31:46 2023
Response via : Initial Calibration
DataAcq Meth:BNA23PS.M
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
50000
100000
150000
200000
250000
300000
350000
400000
450000
500000
550000
600000
650000
700000
750000
800000
850000
900000
Time-->
Abundance TIC: 0211A_20.D\data.ms
Be
n
z
o
(
g
,
h
,
i
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p
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y
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S823B10W.M Mon Feb 13 10:45:12 2023 Page: 2
#9
Benzaldehyde
Concen: 1510.0462310 ppb m
RT: 2.755 min Scan# 190
Delta R.T. -0.023 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:105 Resp: 2475
Ion Ratio Lower Upper
105 100
106 66.5 81.5 122.3#
77 100.2 79.4 119.0
51 0.0 42.2 63.4#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 177 (2.778 min): 0210_04.D\data.ms (-174) (-)
10677
51
193 281135
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 190 (2.755 min): 0211A_20.D\data.ms
281
19343 24913310573221163
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 190 (2.755 min): 0211A_20.D\data.ms (-66) (-)
281
193 2491057713350165221
2.74 2.76 2.78 2.80
0
500
1000
1500
Time-->
Abundance
2.755
#21
3&4-Methyl phenol
Concen: 952.0822250 ppb
RT: 3.190 min Scan# 264
Delta R.T. -0.018 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:107 Resp: 7848
Ion Ratio Lower Upper
107 100
108 84.9 70.0 110.0
79 22.7 7.7 47.7
77 27.4 10.7 50.7
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 250 (3.207 min): 0210_03.D\data.ms (-245) (-)
107
77
43 13059 207 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 264 (3.190 min): 0211A_20.D\data.ms
107
77
43
61 124 207
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 264 (3.190 min): 0211A_20.D\data.ms (-216) (-)
107
77
53 12437 207
3.16 3.18 3.20 3.22
0
5000
10000
Time-->
Abundance
3.190
0211A_20.D S823B10W.M Mon Feb 13 10:45:12 2023 Page 3
#37
Hydroquinone
Concen: 311.6046662 ppb
RT: 3.931 min Scan# 390
Delta R.T. -0.023 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:110 Resp: 1562
Ion Ratio Lower Upper
110 100
81 23.8 11.1 51.1
53 26.2 4.5 44.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 377 (3.954 min): 0210_04.D\data.ms (-373) (-)
110
8153
39 65 95 193 207
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 390 (3.931 min): 0211A_20.D\data.ms
11043
55
69 81
97 207137
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 390 (3.931 min): 0211A_20.D\data.ms (-360) (-)
110
8269 97 1375541
3.92 3.94 3.96
0
500
1000
Time-->
Abundance
3.931
#78
Phenanthrene
Concen: 459.5413621 ppb
RT: 5.931 min Scan# 730
Delta R.T. -0.023 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:178 Resp: 12092
Ion Ratio Lower Upper
178 100
179 16.8 0.0 35.6
152 12.7 0.0 30.1
89 9.8 0.0 28.8
Ref
Raw
Sub
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 717 (5.954 min): 0210_03.D\data.ms (-713) (-)
178
152761269850
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 730 (5.931 min): 0211A_20.D\data.ms
178
151436489129108 224199 327
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 730 (5.931 min): 0211A_20.D\data.ms (-683) (-)
178
151765712698 224199 32738
5.88 5.90 5.92 5.94 5.96
0
5000
10000
15000
Time-->
Abundance
5.931
0211A_20.D S823B10W.M Mon Feb 13 10:45:12 2023 Page 4
#83
Fluoranthene
Concen: 614.3017286 ppb
RT: 6.866 min Scan# 889
Delta R.T. -0.029 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:202 Resp: 15716
Ion Ratio Lower Upper
202 100
203 21.2 0.0 36.7
201 17.9 0.0 34.4
200 20.2 0.0 40.0
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 877 (6.895 min): 0210_03.D\data.ms (-869) (-)
202
101 1741507512350 221
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 889 (6.866 min): 0211A_20.D\data.ms
64
202
1609612841 224 256176 28180
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 889 (6.866 min): 0211A_20.D\data.ms (-843) (-)
20264
101 160128 25622417681 28143
6.85 6.90
0
5000
10000
15000
Time-->
Abundance
6.866
#86
Pyrene
Concen: 525.2693656 ppb
RT: 7.060 min Scan# 922
Delta R.T. -0.029 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:202 Resp: 14299
Ion Ratio Lower Upper
202 100
203 16.7 0.0 37.9
201 20.0 0.0 37.2
200 20.7 0.5 40.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 910 (7.089 min): 0210_03.D\data.ms (-903) (-)
202
101 1747415012250 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 922 (7.060 min): 0211A_20.D\data.ms
202
64 1004381 123 151 175 218 281241 259
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 922 (7.060 min): 0211A_20.D\data.ms (-876) (-)
202
100 1756941 218151129 237 281259
7.00 7.05 7.10
0
5000
10000
15000
Time-->
Abundance
7.060
0211A_20.D S823B10W.M Mon Feb 13 10:45:12 2023 Page 5
#90
Benzo(a)anthracene
Concen: 292.5948502 ppb
RT: 8.366 min Scan# 1144
Delta R.T. -0.041 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:228 Resp: 6980
Ion Ratio Lower Upper
228 100
226 28.6 6.8 46.8
114 20.7 0.0 36.0
113 12.1 0.0 34.4
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 1134 (8.407 min): 0210_03.D\data.ms (-1127) (-)
228
114 20088150 17439 62 281132
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 1144 (8.366 min): 0211A_20.D\data.ms
240
12055 20892156 18071137 28139262
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 1144 (8.366 min): 0211A_20.D\data.ms (-1125) (-)
240
120
2129266 156 19442 262 281173138
8.30 8.35 8.40
0
1000
2000
3000
4000
5000
Time-->
Abundance
8.366
#91
Chrysene
Concen: 264.8590293 ppb m
RT: 8.413 min Scan# 1152
Delta R.T. -0.041 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:228 Resp: 6575
Ion Ratio Lower Upper
228 100
226 30.4 9.3 49.3
229 24.8 0.0 39.1
113 15.2 0.0 35.7
Ref
Raw
Sub
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 1142 (8.454 min): 0210_03.D\data.ms (-1138) (-)
228
113 2008717515039 63 281
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 1152 (8.413 min): 0211A_20.D\data.ms
228
55
97
123 20715117977 281249 329
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 1152 (8.413 min): 0211A_20.D\data.ms (-1133) (-)
228
114 202181 281159932493974 329134
8.40 8.45
0
1000
2000
3000
4000
5000
Time-->
Abundance
8.413
0211A_20.D S823B10W.M Mon Feb 13 10:45:12 2023 Page 6
#95
Benzo(b)fluoranthene
Concen: 366.7017810 ppb
RT: 10.031 min Scan# 1427
Delta R.T. -0.059 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:252 Resp: 9535
Ion Ratio Lower Upper
252 100
253 20.8 1.4 41.4
126 10.8 0.0 38.7
113 13.8 0.0 28.5
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1420 (10.089 min): 0210_03.D\data.ms (-1411) (-)
252
126 224991986317415039 281
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1427 (10.031 min): 0211A_20.D\data.ms
252
6943
95
125 207149 281178229 341
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1427 (10.031 min): 0211A_20.D\data.ms (-1420) (-)
252
125 22415581197 281103 34360
10.00 10.05
0
1000
2000
3000
4000
Time-->
Abundance
10.031
#97
Benzo(a)pyrene
Concen: 320.8067327 ppb
RT: 10.607 min Scan# 1525
Delta R.T. -0.059 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:252 Resp: 7145
Ion Ratio Lower Upper
252 100
253 17.4 1.1 41.1
126 17.1 2.2 42.2
113 15.6 0.0 32.6
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1518 (10.666 min): 0210_03.D\data.ms (-1509) (-)
252
126
224997120017443147
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1525 (10.607 min): 0211A_20.D\data.ms
57
252
95
207125163 281231185 355
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1525 (10.607 min): 0211A_20.D\data.ms (-1484) (-)
252
57
85 126 207 273229161 298185
10.55 10.60 10.65
0
1000
2000
3000
Time-->
Abundance
10.607
0211A_20.D S823B10W.M Mon Feb 13 10:45:12 2023 Page 7
#100
Benzo(g,h,i)perylene
Concen: 292.0106499 ppb
RT: 13.207 min Scan# 1967
Delta R.T. -0.053 min
Lab File: 0211A_20.D
Acq: 12 Feb 2023 2:11 am
Tgt Ion:276 Resp: 6920
Ion Ratio Lower Upper
276 100
138 28.2 9.0 49.0
137 28.2 4.1 44.1
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1959 (13.260 min): 0210_03.D\data.ms (-1949) (-)
276
138
91 22324959 341170197
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1967 (13.207 min): 0211A_20.D\data.ms
55
27681207
137109
163 245 343 412304374
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1967 (13.207 min): 0211A_20.D\data.ms (-1921) (-)
276
13755 20781
107 174 251 412313374345
13.15 13.20 13.25
0
1000
2000
3000
Time-->
Abundance
13.207
0211A_20.D S823B10W.M Mon Feb 13 10:45:12 2023 Page 8
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021123A\
Data File : 0211A_16.D
Acq On : 12 Feb 2023 12:46 am
Operator : 3895
Sample : L1584351-04 1X WG2004454
Misc : SOIL ISTD 23A31573 exp 07/31/23
ALS Vial : 72 Sample Multiplier: 1
Quant Time: Feb 13 10:39:53 2023
Quant Method : C:\msdchem\1\methods\S823B10W.M
Quant Title : 8270 BNA
QLast Update : Fri Feb 10 16:31:46 2023
Response via : Initial Calibration
DataAcq Meth:BNA23PS.M
Compound R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------
Internal Standards
1) 1,4-Dichlorobenzene-d4 2.984 152 49664 8000.0000000 ppb -0.02
23) Naphthalene-d8 3.701 136 199075 8000.0000000 ppb -0.02
46) Acenaphthene-d10 4.825 164 108964 8000.0000000 ppb -0.02
70) Phenanthrene-d10 5.913 188 201280 8000.0000000 ppb -0.02
84) Chrysene-d12 8.378 240 171990 8000.0000000 ppb -0.04
94) Perylene-d12 10.713 264 183012 8000.0000000 ppb -0.06
System Monitoring Compounds
4) 2-Fluorophenol 2.343 112 106868 14067.6812636 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 70.34%
7) Phenol-d5 2.778 99 117345 12276.3971285 ppb -0.01
Spiked Amount 20000.000 Range 20 - 120 Recovery = 61.38%
24) Nitrobenzene-d5 3.290 82 49251 6019.3995720 ppb -0.02
Spiked Amount 10000.000 Range 18 - 125 Recovery = 60.19%
50) 2-Fluorobiphenyl 4.366 172 123838 6868.5682794 ppb -0.02
Spiked Amount 10000.000 Range 28 - 120 Recovery = 68.69%
73) 2,4,6-Tribromophenol 5.390 330 38996 17735.1817793 ppb -0.02
Spiked Amount 20000.000 Range 17 - 137 Recovery = 88.68%
87) p-Terphenyl-d14 7.213 244 165179 7548.1213686 ppb -0.03
Spiked Amount 10000.000 Range 13 - 131 Recovery = 75.48%
Target Compounds Qvalue
9) Benzaldehyde 2.760 105 1830m 1117.8904002 ppb
21) 3&4-Methyl phenol 3.190 107 3587 435.6923514 ppb 96
37) Hydroquinone 3.937 110 1327 261.7310064 ppb 85
83) Fluoranthene 6.872 202 14973 564.6586193 ppb 99
86) Pyrene 7.060 202 11393 410.0623275 ppb 96
90) Benzo(a)anthracene 8.366 228 6552 269.1042226 ppb 92
91) Chrysene 8.413 228 6108m 241.0756923 ppb
92) bis(2-Ethylhexyl)phtha... 8.489 149 2387m 1866.0409993 ppb
95) Benzo(b)fluoranthene 10.036 252 7169 267.8886930 ppb 90
--------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration (+) = signals summed
S823B10W.M Mon Feb 13 10:39:55 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021123A\
Data File : 0211A_16.D
Acq On : 12 Feb 2023 12:46 am
Operator : 3895
Sample : L1584351-04 1X WG2004454
Misc : SOIL ISTD 23A31573 exp 07/31/23
ALS Vial : 72 Sample Multiplier: 1
Quant Time: Feb 13 10:39:53 2023
Quant Method : C:\msdchem\1\methods\S823B10W.M
Quant Title : 8270 BNA
QLast Update : Fri Feb 10 16:31:46 2023
Response via : Initial Calibration
DataAcq Meth:BNA23PS.M
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
200000
400000
600000
800000
1000000
1200000
1400000
1600000
1800000
2000000
2200000
2400000
2600000
2800000
3000000
3200000
3400000
3600000
3800000
4000000
4200000
Time-->
Abundance TIC: 0211A_16.D\data.ms
Pe
r
y
l
e
n
e
-
d
1
2
,
I
Be
n
z
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(
b
)
f
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a
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M
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bi
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(
2
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t
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p
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a
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Ch
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1
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Fl
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a
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C
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2,
4
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F
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p
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8
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S
S823B10W.M Mon Feb 13 10:39:55 2023 Page: 2
#9
Benzaldehyde
Concen: 1117.8904002 ppb m
RT: 2.760 min Scan# 191
Delta R.T. -0.018 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:105 Resp: 1830
Ion Ratio Lower Upper
105 100
106 74.7 81.5 122.3#
77 99.7 79.4 119.0
51 108.6 42.2 63.4#
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 177 (2.778 min): 0210_04.D\data.ms (-174) (-)
10677
51
193 281135
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 191 (2.760 min): 0211A_16.D\data.ms
281
43
77 105 193133 24922160
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 191 (2.760 min): 0211A_16.D\data.ms (-66) (-)
281
10577 24951193133221
2.74 2.76 2.78 2.80
0
500
1000
Time-->
Abundance
2.760
#21
3&4-Methyl phenol
Concen: 435.6923514 ppb
RT: 3.190 min Scan# 264
Delta R.T. -0.018 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:107 Resp: 3587
Ion Ratio Lower Upper
107 100
108 93.6 70.0 110.0
79 22.7 7.7 47.7
77 31.3 10.7 50.7
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 250 (3.207 min): 0210_03.D\data.ms (-245) (-)
107
77
43 13059 207 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 264 (3.190 min): 0211A_16.D\data.ms
107
43 77
20761
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 264 (3.190 min): 0211A_16.D\data.ms (-216) (-)
107
77
51 207
3.16 3.18 3.20 3.22
0
2000
4000
Time-->
Abundance
3.190
0211A_16.D S823B10W.M Mon Feb 13 10:39:55 2023 Page 3
#37
Hydroquinone
Concen: 261.7310064 ppb
RT: 3.937 min Scan# 391
Delta R.T. -0.018 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:110 Resp: 1327
Ion Ratio Lower Upper
110 100
81 23.2 11.1 51.1
53 16.8 4.5 44.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 377 (3.954 min): 0210_04.D\data.ms (-373) (-)
110
8153
39 65 95 193 207
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 391 (3.937 min): 0211A_16.D\data.ms
43 110
55
81 2076713595
40 60 80 100 120 140 160 180 200
0
50
m/z-->
Abundance Scan 391 (3.937 min): 0211A_16.D\data.ms (-360) (-)
110
2076981421355597
3.92 3.94 3.96
0
500
1000
Time-->
Abundance
3.937
#83
Fluoranthene
Concen: 564.6586193 ppb
RT: 6.872 min Scan# 890
Delta R.T. -0.023 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:202 Resp: 14973
Ion Ratio Lower Upper
202 100
203 17.4 0.0 36.7
201 14.4 0.0 34.4
200 19.8 0.0 40.0
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 877 (6.895 min): 0210_03.D\data.ms (-869) (-)
202
101 1741507512350 221
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 890 (6.872 min): 0211A_16.D\data.ms
64
202
1609612843 224 256185 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 890 (6.872 min): 0211A_16.D\data.ms (-843) (-)
64
202
160128 25622496182 281
6.84 6.86 6.88 6.90 6.92
0
5000
10000
15000
Time-->
Abundance
6.872
0211A_16.D S823B10W.M Mon Feb 13 10:39:55 2023 Page 4
#86
Pyrene
Concen: 410.0623275 ppb
RT: 7.060 min Scan# 922
Delta R.T. -0.029 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:202 Resp: 11393
Ion Ratio Lower Upper
202 100
203 18.5 0.0 37.9
201 14.6 0.0 37.2
200 18.7 0.5 40.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 910 (7.089 min): 0210_03.D\data.ms (-903) (-)
202
101 1747415012250 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 922 (7.060 min): 0211A_16.D\data.ms
202
43 64 10981 137 177159 235 259 281
40 60 80 100 120 140 160 180 200 220 240 260 280
0
50
m/z-->
Abundance Scan 922 (7.060 min): 0211A_16.D\data.ms (-876) (-)
202
10181 121 177 2592356113815843 290
7.02 7.04 7.06 7.08 7.10
0
5000
10000
Time-->
Abundance
7.060
#90
Benzo(a)anthracene
Concen: 269.1042226 ppb
RT: 8.366 min Scan# 1144
Delta R.T. -0.041 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:228 Resp: 6552
Ion Ratio Lower Upper
228 100
226 28.1 6.8 46.8
114 20.5 0.0 36.0
113 7.3 0.0 34.4
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1134 (8.407 min): 0210_03.D\data.ms (-1127) (-)
228
114 20088150 17439 62 281132
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1144 (8.366 min): 0211A_16.D\data.ms
240
120
43 92 20866184141 163 285263
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1144 (8.366 min): 0211A_16.D\data.ms (-1125) (-)
240
120
2129266156178138 26342 281 302
8.30 8.35 8.40
0
1000
2000
3000
4000
5000
Time-->
Abundance
8.366
0211A_16.D S823B10W.M Mon Feb 13 10:39:55 2023 Page 5
#91
Chrysene
Concen: 241.0756923 ppb m
RT: 8.413 min Scan# 1152
Delta R.T. -0.041 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:228 Resp: 6108
Ion Ratio Lower Upper
228 100
226 31.6 9.3 49.3
229 27.1 0.0 39.1
113 15.1 0.0 35.7
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1142 (8.454 min): 0210_03.D\data.ms (-1138) (-)
228
113 2008717515039 63 281
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1152 (8.413 min): 0211A_16.D\data.ms
228
43 91 30213169109259157207185281
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1152 (8.413 min): 0211A_16.D\data.ms (-1133) (-)
228
302
13691 2591142001571764567 282
8.40 8.45
0
1000
2000
3000
4000
5000
Time-->
Abundance
8.413
#92
bis(2-Ethylhexyl)phthalate
Concen: 1866.0409993 ppb m
RT: 8.489 min Scan# 1165
Delta R.T. -0.035 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:149 Resp: 2387
Ion Ratio Lower Upper
149 100
167 63.6 8.8 48.8#
279 0.0 0.0 25.4
150 20.7 0.0 30.9
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1154 (8.525 min): 0210_03.D\data.ms (-1148) (-)
149
16757
113 2798339193 221 261
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1165 (8.489 min): 0211A_16.D\data.ms
43
149
69 91 167 239109207131 285185259
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1165 (8.489 min): 0211A_16.D\data.ms (-1120) (-)
149
71
96 167 191 267 30221324942122
8.45 8.50
0
500
1000
1500
2000
Time-->
Abundance
8.489
0211A_16.D S823B10W.M Mon Feb 13 10:39:55 2023 Page 6
#95
Benzo(b)fluoranthene
Concen: 267.8886930 ppb
RT: 10.036 min Scan# 1428
Delta R.T. -0.053 min
Lab File: 0211A_16.D
Acq: 12 Feb 2023 12:46 am
Tgt Ion:252 Resp: 7169
Ion Ratio Lower Upper
252 100
253 13.9 1.4 41.4
126 16.0 0.0 38.7
113 7.9 0.0 28.5
Ref
Raw
Sub
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1420 (10.089 min): 0210_03.D\data.ms (-1411) (-)
252
126 224991986317415039 281
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1428 (10.036 min): 0211A_16.D\data.ms
252
43 69
95 207126147 281 300177226
40 60 80 100 120 140 160 180 200 220 240 260 280 300
0
50
m/z-->
Abundance Scan 1428 (10.036 min): 0211A_16.D\data.ms (-1420) (-)
252
1264169 169 211187 30192 146 271
10.00 10.05
0
1000
2000
3000
Time-->
Abundance
10.036
0211A_16.D S823B10W.M Mon Feb 13 10:39:55 2023 Page 7
Quantitation Report (QT Reviewed)
Data Path : C:\GCMS\1\data\021623\
Data File : 0216_006.D
Signal(s) : FID1A.ch
Acq On : 16 Feb 2023 10:04 am
Operator : 3726
Sample : L1584351-01 1x WG2005423
Misc : MIs on ranges are corrections
ALS Vial : 16 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 16 10:28:19 2023
Quant Method : C:\GCMS\1\methods\DM50A10W.M
Quant Title :
QLast Update : Tue Jan 10 12:38:25 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
---------------------------------------------------------------------------
System Monitoring Compounds
21) S o-terphenyl 3.28 2469521 0.7827173 ppm m
Spiked Amount 0.0200 Range 50 - 150 Recovery = 3913.59%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 2.14 28104789 24.7101180 ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 1.70 115137100 49.7582443 ppm
3) h,t DRO W/ SGT 1.70 115137100 49.7582443 ppm
4) h,m DRO C8-C28 1.08 120876680 50.2177290 ppm
5) h,m (WY) Diesel Range Org... 1.70 177324056 67.6431800 ppm
6) h,m Diesel Range Organics 2.14 52381524 33.8833426 ppm
7) h,m Residual Range Organics 3.90 284748389 96.1054188 ppm
8) h Gasoline (C7-C12)0.91 8117495 3.1946360 ppm
9) h,m Diesel (C12-C24)2.14 52381524 33.8833426 ppm
10) h,m Motor Oil (C24-C30) 3.90 91717520 57.4971407 ppm
11) h,m C10-C28 Diesel Range 1.70 115137100 49.7582443 ppm
12) h,m C28-C40 Oil Range 4.32 222667677 127.8388418 ppm
13) h,m C28-C36 Motor Oil Range 4.32 132540676 92.9457480 ppm
14) h Gasoline 0.83 13101439 N.D. ppm
15) h,m Diesel 1.34 110188406 47.2489210 ppm
16) h,m Motor Oil 3.18 347530422 84.0510488 ppm
17) h Mineral Spirits 0.00 2605613492 NoCal ppm
18) h Kerosene 0.00 2605613492 NoCal ppm
19) h #6 Fuel Oil 0.00 2605613492 NoCal ppm
20) h Hydraulic Fluid 0.00 2605613492 NoCal ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM50A10W.M Thu Feb 16 10:28:48 2023 GC50 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\GCMS\1\data\021623\
Data File : 0216_006.D
Signal(s) : FID1A.ch
Acq On : 16 Feb 2023 10:04 am
Operator : 3726
Sample : L1584351-01 1x WG2005423
Misc : MIs on ranges are corrections
ALS Vial : 16 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 16 10:28:19 2023
Quant Method : C:\GCMS\1\methods\DM50A10W.M
Quant Title :
QLast Update : Tue Jan 10 12:38:25 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
0
5000000
1e+07
1.5e+07
2e+07
2.5e+07
3e+07
3.5e+07
4e+07
4.5e+07
Time
Response_Signal: 0216_006.D\FID1A.ch
C2
8
-
C
3
6

M
o
C2
8
-
C
4
0

O
i
Mo
t
o
r

O
i
l

R
e
s
i
d
u
a
l

R
o-
t
e
r
p
h
e
n
y
Mo
t
o
r

O
i
l
Di
e
s
e
l

R
a
n
C
1
2
-
C
2
2

H
y
Di
e
s
e
l

(
C
1
DR
O

W
/

S
G
T
(W
Y
)

D
i
e
s
e
C1
0
-
C
2
8

D
i
Di
e
s
e
l
DR
O

C
8
-
C
2
8
Ga
s
o
l
i
n
e

(
TP
H

(
G
C
/
F
I
DM50A10W.M Thu Feb 16 10:28:48 2023 GC50 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021523\
Data File : 0215_048.d
Signal(s) : FID1A.CH
Acq On : 16 Feb 2023 0:06 am
Operator : 3726
Sample : L1584351-02 1x WG2005423
Misc : M.I.'s on ranges are corrections
ALS Vial : 34 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 16 09:30:30 2023
Quant Method : C:\msdchem\1\methods\DM16B10W.M
Quant Title :
QLast Update : Fri Feb 10 09:54:43 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
21) S O-TERPHENYL 3.27 12335240 15.0632679 ppm
Spiked Amount 20.0000 Range 50 - 150 Recovery = 75.32%
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.71 62530655 72.4855525 ppm
12) h,m C28-C40 Oil Range 4.31 52646759 130.6052418 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h Gasoline 0.00 0 N.D. ppm
15) h,m Diesel 0.00 0 N.D. ppm
16) h,m Motor Oil 0.00 0 N.D. ppm
17) h Mineral Spirits 0.00 0 N.D. ppm
18) h Kerosene 0.00 0 N.D. ppm
19) h #6 Fuel Oil 0.00 0 N.D. ppm
20) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM16B10W.M Thu Feb 16 09:30:33 2023 Page: 1
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021523\
Data File : 0215_048.d
Signal(s) : FID1A.CH
Acq On : 16 Feb 2023 0:06 am
Operator : 3726
Sample : L1584351-02 1x WG2005423
Misc : M.I.'s on ranges are corrections
ALS Vial : 34 Sample Multiplier: 1
Integration File: events.e
Quant Time: Feb 16 09:30:30 2023
Quant Method : C:\msdchem\1\methods\DM16B10W.M
Quant Title :
QLast Update : Fri Feb 10 09:54:43 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
-500000
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
5000000
5500000
6000000
6500000
7000000
7500000
8000000
8500000
9000000
9500000
Time
Response_Signal: 0215_048.d\FID1A.CH
C2
8
-
C
4
0

O
i
O-
T
E
R
P
H
E
N
Y
C1
0
-
C
2
8

D
i
DM16B10W.M Thu Feb 16 09:30:33 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\GCMS\1\data\021523R\
Data File : 0215_014R.D
Signal(s) : FID2B.ch
Acq On : 15 Feb 2023 09:58 am
Operator : 3932
Sample : L1584351-03 1X WG2005842
Misc : MIs on ranges are corrections
ALS Vial : 23 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 15 10:15:02 2023
Quant Method : C:\GCMS\1\methods\DM50A07WR.M
Quant Title :
QLast Update : Sat Jan 07 13:36:42 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
---------------------------------------------------------------------------
System Monitoring Compounds
21) S o-terphenyl 3.30 18396752 5.9279327 ppm
Spiked Amount 0.0200 Range 50 - 150 Recovery = 29639.66%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm d
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm d
3) h,t DRO W/ SGT 0.00 0 N.D. ppm d
4) h,m DRO C8-C28 0.00 0 N.D. ppm d
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm d
6) h,m Diesel Range Organics 0.00 0 N.D. ppm d
7) h,m Residual Range Organics 0.00 0 N.D. ppm d
8) h Gasoline (C7-C12)0.00 0 N.D. ppm d
9) h,m Diesel (C12-C24)0.00 0 N.D. ppm d
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm d
11) h,m C10-C28 Diesel Range 1.71 690170430 237.4924526 ppm
12) h,m C28-C40 Oil Range 4.32 1892350352 1387.8042494 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm d
14) h Gasoline 0.00 0 N.D. ppm d
15) h,m Diesel 0.00 0 N.D. ppm d
16) h,m Motor Oil 0.00 0 N.D. ppm d
17) h Mineral Spirits 0.00 0 N.D. ppm d
18) h Kerosene 0.00 0 N.D. ppm d
19) h #6 Fuel Oil 0.00 0 N.D. ppm d
20) h Hydraulic Fluid 0.00 0 N.D. ppm d
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM50A07WR.M Wed Feb 15 14:29:11 2023 GC50 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\GCMS\1\data\021523R\
Data File : 0215_014R.D
Signal(s) : FID2B.ch
Acq On : 15 Feb 2023 09:58 am
Operator : 3932
Sample : L1584351-03 1X WG2005842
Misc : MIs on ranges are corrections
ALS Vial : 23 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 15 10:15:02 2023
Quant Method : C:\GCMS\1\methods\DM50A07WR.M
Quant Title :
QLast Update : Sat Jan 07 13:36:42 2023
Response via : Initial Calibration
Integrator: ChemStation
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-2000000
0
2000000
4000000
6000000
8000000
1e+07
1.2e+07
1.4e+07
1.6e+07
1.8e+07
2e+07
2.2e+07
2.4e+07
2.6e+07
Time
Response_Signal: 0215_014R.D\FID2B.ch
C2
8
-
C
4
0

O
i
o-
t
e
r
p
h
e
n
y
C1
0
-
C
2
8

D
i
DM50A07WR.M Wed Feb 15 14:29:11 2023 GC50 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021423\
Data File : 0214_062.d
Signal(s) : FID1A.CH
Acq On : 15 Feb 2023 5:44 am
Operator : 3726
Sample : L1584351-03 1X WG2005842
Misc : M.I.s on ranges are corrections
ALS Vial : 29 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 15 08:44:56 2023
Quant Method : C:\msdchem\1\methods\DM07B13W.M
Quant Title :
QLast Update : Mon Feb 13 15:28:38 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
21) S o-terphenyl 3.61 11512911 8.5397124 ppm
Spiked Amount 0.0200 Range 50 - 150 Recovery = 42698.56%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.98 307915872 262.8153058 ppm
12) h,m C28-C40 Oil Range 4.76 924147334 1477.8434870 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h Gasoline 0.00 0 N.D. ppm
15) h,m Diesel 0.00 0 N.D. ppm
16) h,m Motor Oil 0.00 0 N.D. ppm
17) h Mineral Spirits 0.00 0 N.D. ppm
18) h Kerosene 0.00 0 N.D. ppm
19) h #6 Fuel Oil 0.00 0 N.D. ppm
20) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM07B13W.M Wed Feb 15 08:45:00 2023 Page: 1
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021423\
Data File : 0214_062.d
Signal(s) : FID1A.CH
Acq On : 15 Feb 2023 5:44 am
Operator : 3726
Sample : L1584351-03 1X WG2005842
Misc : M.I.s on ranges are corrections
ALS Vial : 29 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 15 08:44:56 2023
Quant Method : C:\msdchem\1\methods\DM07B13W.M
Quant Title :
QLast Update : Mon Feb 13 15:28:38 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
Time
Response_Signal: 0214_062.d\FID1A.CH
C2
8
-
C
4
0

O
i
o-
t
e
r
p
h
e
n
y
C1
0
-
C
2
8

D
i
DM07B13W.M Wed Feb 15 08:45:00 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021423\
Data File : 0214_061.d
Signal(s) : FID1A.CH
Acq On : 15 Feb 2023 5:31 am
Operator : 3726
Sample : L1584351-04 1X WG2005842
Misc : M.I.s on ranges are corrections
ALS Vial : 28 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 15 08:44:36 2023
Quant Method : C:\msdchem\1\methods\DM07B13W.M
Quant Title :
QLast Update : Mon Feb 13 15:28:38 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
21) S o-terphenyl 3.61 19158672 14.2109624 ppm
Spiked Amount 0.0200 Range 50 - 150 Recovery = 71054.81%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.98 168510133 158.4238029 ppm
12) h,m C28-C40 Oil Range 4.76 439971603 606.0006038 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h Gasoline 0.00 0 N.D. ppm
15) h,m Diesel 0.00 0 N.D. ppm
16) h,m Motor Oil 0.00 0 N.D. ppm
17) h Mineral Spirits 0.00 0 N.D. ppm
18) h Kerosene 0.00 0 N.D. ppm
19) h #6 Fuel Oil 0.00 0 N.D. ppm
20) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM07B13W.M Wed Feb 15 08:44:40 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\021423\
Data File : 0214_061.d
Signal(s) : FID1A.CH
Acq On : 15 Feb 2023 5:31 am
Operator : 3726
Sample : L1584351-04 1X WG2005842
Misc : M.I.s on ranges are corrections
ALS Vial : 28 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Feb 15 08:44:36 2023
Quant Method : C:\msdchem\1\methods\DM07B13W.M
Quant Title :
QLast Update : Mon Feb 13 15:28:38 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
Time
Response_Signal: 0214_061.d\FID1A.CH
C2
8
-
C
4
0

O
i
o-
t
e
r
p
h
e
n
y
C1
0
-
C
2
8

D
i
DM07B13W.M Wed Feb 15 08:44:40 2023 Page: 2
OFF-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_016.d
Signal(s) : FID1A.CH
Acq On : 26 Apr 2023 17:30 pm
Operator : 3726
Sample : L1607939-07 1X WG2048845
Misc : M.I.s on ranges are corrections
ALS Vial : 23 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Apr 27 06:55:49 2023
Quant Method : C:\msdchem\1\methods\DM07D26W.M
Quant Title :
QLast Update : Wed Apr 26 15:51:04 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
22) S o-terphenyl 3.59 12995180 11.7986008 ppm m
Spiked Amount 0.0200 Range 50 - 150 Recovery = 58993.00%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.98 89158877 107.7320341 ppm
12) h,m C28-C40 Oil Range 4.70 195751858 263.7538985 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h,m DRO C13-22 0.00 0 N.D. ppm
15) h Gasoline 0.00 0 N.D. ppm
16) h,m Diesel 0.00 0 N.D. ppm
17) h,m Motor Oil 0.00 0 N.D. ppm
18) h Mineral Spirits 0.00 0 N.D. ppm
19) h Kerosene 0.00 0 N.D. ppm
20) h #6 Fuel Oil 0.00 0 N.D. ppm
21) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM07D26W.M Thu Apr 27 06:56:00 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_016.d
Signal(s) : FID1A.CH
Acq On : 26 Apr 2023 17:30 pm
Operator : 3726
Sample : L1607939-07 1X WG2048845
Misc : M.I.s on ranges are corrections
ALS Vial : 23 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Apr 27 06:55:49 2023
Quant Method : C:\msdchem\1\methods\DM07D26W.M
Quant Title :
QLast Update : Wed Apr 26 15:51:04 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
Time
Response_Signal: 0426_016.d\FID1A.CH
C2
8
-
C
4
0

O
i
o-
t
e
r
p
h
e
n
y
C1
0
-
C
2
8

D
i
DM07D26W.M Thu Apr 27 06:56:00 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_017.d
Signal(s) : FID1A.CH
Acq On : 26 Apr 2023 17:43 pm
Operator : 3726
Sample : L1607939-08 1X WG2048845
Misc : M.I.s on ranges are corrections
ALS Vial : 24 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Apr 27 06:56:16 2023
Quant Method : C:\msdchem\1\methods\DM07D26W.M
Quant Title :
QLast Update : Wed Apr 26 15:51:04 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
22) S o-terphenyl 3.58 9349359 8.4884828 ppm
Spiked Amount 0.0200 Range 50 - 150 Recovery = 42442.41%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.98 63438145 84.8110201 ppm
12) h,m C28-C40 Oil Range 4.70 266742739 409.5703245 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h,m DRO C13-22 0.00 0 N.D. ppm
15) h Gasoline 0.00 0 N.D. ppm
16) h,m Diesel 0.00 0 N.D. ppm
17) h,m Motor Oil 0.00 0 N.D. ppm
18) h Mineral Spirits 0.00 0 N.D. ppm
19) h Kerosene 0.00 0 N.D. ppm
20) h #6 Fuel Oil 0.00 0 N.D. ppm
21) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM07D26W.M Thu Apr 27 06:56:21 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_017.d
Signal(s) : FID1A.CH
Acq On : 26 Apr 2023 17:43 pm
Operator : 3726
Sample : L1607939-08 1X WG2048845
Misc : M.I.s on ranges are corrections
ALS Vial : 24 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Apr 27 06:56:16 2023
Quant Method : C:\msdchem\1\methods\DM07D26W.M
Quant Title :
QLast Update : Wed Apr 26 15:51:04 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
Time
Response_Signal: 0426_017.d\FID1A.CH
C2
8
-
C
4
0

O
i
o-
t
e
r
p
h
e
n
y
C1
0
-
C
2
8

D
i
DM07D26W.M Thu Apr 27 06:56:21 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_043.d
Signal(s) : FID1A.CH
Acq On : 27 Apr 2023 8:42 am
Operator : 473
Sample : L1607939-09 1x WG2048845
Misc : M.I.'s on ranges are corrections
ALS Vial : 36 Sample Multiplier: 1
Integration File: events.e
Quant Time: Apr 27 09:48:35 2023
Quant Method : C:\msdchem\1\methods\DM16D25W.M
Quant Title :
QLast Update : Tue Apr 25 11:20:09 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
22) S O-TERPHENYL 3.20 1311452 1.9785818 ppm m
Spiked Amount 20.0000 Range 50 - 150 Recovery = 9.89%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.63 443161463 669.5382873 ppm
12) h,m C28-C40 Oil Range 4.19 150083501 526.1178111 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h,m DRO C13-22 0.00 0 N.D. ppm
15) h Gasoline 0.00 0 N.D. ppm
16) h,m Diesel 0.00 0 N.D. ppm
17) h,m Motor Oil 0.00 0 N.D. ppm
18) h Mineral Spirits 0.00 0 N.D. ppm
19) h Kerosene 0.00 0 N.D. ppm
20) h #6 Fuel Oil 0.00 0 N.D. ppm
21) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM16D25W.M Thu Apr 27 09:48:44 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_043.d
Signal(s) : FID1A.CH
Acq On : 27 Apr 2023 8:42 am
Operator : 473
Sample : L1607939-09 1x WG2048845
Misc : M.I.'s on ranges are corrections
ALS Vial : 36 Sample Multiplier: 1
Integration File: events.e
Quant Time: Apr 27 09:48:35 2023
Quant Method : C:\msdchem\1\methods\DM16D25W.M
Quant Title :
QLast Update : Tue Apr 25 11:20:09 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
-500000
0
500000
1000000
1500000
2000000
2500000
3000000
3500000
4000000
4500000
5000000
5500000
6000000
6500000
7000000
7500000
8000000
8500000
9000000
9500000
Time
Response_Signal: 0426_043.d\FID1A.CH
C2
8
-
C
4
0

O
i
O-
T
E
R
P
H
E
N
Y
C1
0
-
C
2
8

D
i
DM16D25W.M Thu Apr 27 09:48:44 2023 Page: 2
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_019.d
Signal(s) : FID1A.CH
Acq On : 26 Apr 2023 18:09 pm
Operator : 3726
Sample : L1607939-10 5X WG2048845
Misc : M.I.s on ranges are corrections
ALS Vial : 26 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Apr 27 06:57:07 2023
Quant Method : C:\msdchem\1\methods\DM07D26W.M
Quant Title :
QLast Update : Wed Apr 26 15:51:04 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
Compound R.T. Response Conc Units
--------------------------------------------------------------------------------
System Monitoring Compounds
22) S o-terphenyl 3.58 1733176 1.5735876 ppm m
Spiked Amount 0.0200 Range 50 - 150 Recovery = 7867.94%#
Target Compounds
1) t,m,h C12-C22 Hydrocarbons 0.00 0 N.D. ppm
2) t,m,h TPH (GC/FID) HIGH FRA... 0.00 0 N.D. ppm
3) h,t DRO W/ SGT 0.00 0 N.D. ppm
4) h,m DRO C8-C28 0.00 0 N.D. ppm
5) h,m (WY) Diesel Range Org... 0.00 0 N.D. ppm
6) h,m Diesel Range Organics 0.00 0 N.D. ppm
7) h,m Residual Range Organics 0.00 0 N.D. ppm
8) h Gasoline (C7-C12) 0.00 0 N.D. ppm
9) h,m Diesel (C12-C24) 0.00 0 N.D. ppm
10) h,m Motor Oil (C24-C30) 0.00 0 N.D. ppm
11) h,m C10-C28 Diesel Range 1.98 65402543 86.5615927 ppm
12) h,m C28-C40 Oil Range 4.70 202533350 277.6831937 ppm
13) h,m C28-C36 Motor Oil Range 0.00 0 N.D. ppm
14) h,m DRO C13-22 0.00 0 N.D. ppm
15) h Gasoline 0.00 0 N.D. ppm
16) h,m Diesel 0.00 0 N.D. ppm
17) h,m Motor Oil 0.00 0 N.D. ppm
18) h Mineral Spirits 0.00 0 N.D. ppm
19) h Kerosene 0.00 0 N.D. ppm
20) h #6 Fuel Oil 0.00 0 N.D. ppm
21) h Hydraulic Fluid 0.00 0 N.D. ppm
---------------------------------------------------------------------------
(f)=RT Delta > 1/2 Window (m)=manual int.
DM07D26W.M Thu Apr 27 06:57:18 2023 Page: 1
ON-SITE
Quantitation Report (QT Reviewed)
Data Path : C:\msdchem\1\data\042623\
Data File : 0426_019.d
Signal(s) : FID1A.CH
Acq On : 26 Apr 2023 18:09 pm
Operator : 3726
Sample : L1607939-10 5X WG2048845
Misc : M.I.s on ranges are corrections
ALS Vial : 26 Sample Multiplier: 1
Integration File: EVENTS.E
Quant Time: Apr 27 06:57:07 2023
Quant Method : C:\msdchem\1\methods\DM07D26W.M
Quant Title :
QLast Update : Wed Apr 26 15:51:04 2023
Response via : Initial Calibration
Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped
Volume Inj. :
Signal Phase :
Signal Info :
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
-1000000
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
Time
Response_Signal: 0426_019.d\FID1A.CH
C2
8
-
C
4
0

O
i
o-
t
e
r
p
h
e
n
y
C1
0
-
C
2
8

D
i
DM07D26W.M Thu Apr 27 06:57:18 2023 Page: 2
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_24.D Vial: 24
Acq On : 27 Apr 2023 7:21 am Operator: 3545
Sample : L1607939-07 1X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:34 2023 Quant Results File: S804D05W.RES
Quant Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
DataAcq Meth : BNA4PS
Internal Standards R.T. QIon Response Conc Units Dev(Min)
-------------------------------------------------------------------------
1) 1,4-Dichlorobenzene-d4 3.17 152 66462 8000.00 ppb -0.03
23) Naphthalene-d8 3.90 136 254474 8000.00 ppb -0.03
46) Acenaphthene-d10 5.05 164 138685 8000.00 ppb -0.03
70) Phenanthrene-d10 6.16 188 268252 8000.00 ppb -0.04
84) Chrysene-d12 8.81 240 276898 8000.00 ppb -0.05
94) Perylene-d12 11.38 264 306623 8000.00 ppb -0.07
System Monitoring Compounds
4) 2-Fluorophenol 2.52 112 112482 10818.0178739 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 54.09%
7) Phenol-d5 2.95 99 129510 9770.8250712 ppb -0.02
Spiked Amount 20000.000 Range 20 - 120 Recovery = 48.85%
24) Nitrobenzene-d5 3.48 82 49655 4337.1064629 ppb -0.03
Spiked Amount 10000.000 Range 18 - 125 Recovery = 43.37%
50) 2-Fluorobiphenyl 4.58 172 136993 5262.4150206 ppb -0.03
Spiked Amount 10000.000 Range 28 - 120 Recovery = 52.62%
73) 2,4,6-Tribromophenol 5.63 330 52586 12289.4515030 ppb -0.03
Spiked Amount 20000.000 Range 17 - 137 Recovery = 61.45%
87) p-Terphenyl-d14 7.52 244 226787 5951.6483478 ppb -0.04
Spiked Amount 10000.000 Range 13 - 131 Recovery = 59.52%
Target Compounds Qvalue
100) Benzo(g,h,i)perylene 13.80 276 9877 207.4746630 ppb 99
-------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration
0426B_24.D S804D05W.M Thu Apr 27 14:34:10 2023 Page 1
ON-SITE
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_24.D Vial: 24
Acq On : 27 Apr 2023 7:21 am Operator: 3545
Sample : L1607939-07 1X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:34 2023 Quant Results File: S804D05W.RES
Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
1.5e+07
1.6e+07
1.7e+07
1.8e+07
1.9e+07
2e+07
2.1e+07
Time-->
Abundance TIC: 0426B_24.D
Be
n
z
o
(
g
,
h
,
i
)
p
e
r
y
l
e
n
e
,
M
T
Pe
r
y
l
e
n
e
-
d
1
2
,
I
Ch
r
y
s
e
n
e
-
d
1
2
,
I
p-
T
e
r
p
h
e
n
y
l
-
d
1
4

,
S
Ph
e
n
a
n
t
h
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-
d
1
0
,
I
2,
4
,
6
-
T
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i
b
r
o
m
o
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e
n
o
l

,
S
Ac
e
n
a
p
h
t
h
e
n
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-
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1
0
,
I
2-
F
l
u
o
r
o
b
i
p
h
e
n
y
l

,
S
Na
p
h
t
h
a
l
e
n
e
-
d
8
,
I
Ni
t
r
o
b
e
n
z
e
n
e
-
d
5

,
S
1,
4
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e
-
d
4
,
I
Ph
e
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o
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-
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5

,
S
2-
F
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o
l

,
S
0426B_24.D S804D05W.M Thu Apr 27 14:34:11 2023 Page 2
#100
Benzo(g,h,i)perylene
Concen: 207.4746630 ppb
RT: 13.80 min Scan# 1989
Delta R.T. -0.06 min
Lab File: 0426B_24.D
Acq: 27 Apr 2023 7:21 am
Tgt Ion:276 Resp: 9877
Ion Ratio Lower Upper
276 100
138 22.3 2.6 42.6
137 20.8 0.0 39.8
Ref
Raw
Sub
0 50 100 150 200 250 300 350 400 450
0
50
m/z-->
Abundance Scan 1950 (13.856 min): 0405_03.D (-1942) (-)
276
138
22491 343 42957 171 48917
0 50 100 150 200 250 300 350 400 450
0
50
m/z-->
Abundance Scan 1989 (13.795 min): 0426B_24.D
276
28
207
73 138
355310239 401172 489105
0 50 100 150 200 250 300 350 400 450
0
50
m/z-->
Abundance Scan 1989 (13.795 min): 0426B_24.D (-1946) (-)
276
138
20773 357308 48939 172 239 401
13.75 13.80 13.85
0
2000
4000
6000
8000
Time-->
Abundance Ion 276.00 (275.30 to 276.70):
13.80
Ion 138.00 (137.30 to 138.70):
Ion 137.00 (136.30 to 137.70):
L1607939-07 0426B_24.D S804D05W.M Thu Apr 27 14:34:11 2023 Page 3
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_23.D Vial: 23
Acq On : 27 Apr 2023 7:00 am Operator: 3545
Sample : L1607939-08 1X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:33 2023 Quant Results File: S804D05W.RES
Quant Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
DataAcq Meth : BNA4PS
Internal Standards R.T. QIon Response Conc Units Dev(Min)
-------------------------------------------------------------------------
1) 1,4-Dichlorobenzene-d4 3.17 152 66036 8000.00 ppb -0.03
23) Naphthalene-d8 3.90 136 250889 8000.00 ppb -0.03
46) Acenaphthene-d10 5.05 164 138930 8000.00 ppb -0.03
70) Phenanthrene-d10 6.16 188 266553 8000.00 ppb -0.04
84) Chrysene-d12 8.81 240 270016 8000.00 ppb -0.05
94) Perylene-d12 11.38 264 298007 8000.00 ppb -0.07
System Monitoring Compounds
4) 2-Fluorophenol 2.52 112 112524 10891.8706272 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 54.46%
7) Phenol-d5 2.96 99 110302 8375.3693654 ppb -0.01
Spiked Amount 20000.000 Range 20 - 120 Recovery = 41.88%
24) Nitrobenzene-d5 3.48 82 48921 4334.0530062 ppb -0.03
Spiked Amount 10000.000 Range 18 - 125 Recovery = 43.34%
50) 2-Fluorobiphenyl 4.58 172 134347 5151.6713265 ppb -0.03
Spiked Amount 10000.000 Range 28 - 120 Recovery = 51.52%
73) 2,4,6-Tribromophenol 5.63 330 49989 11756.9915450 ppb -0.03
Spiked Amount 20000.000 Range 17 - 137 Recovery = 58.78%
87) p-Terphenyl-d14 7.52 244 216645 5830.3965884 ppb -0.04
Spiked Amount 10000.000 Range 13 - 131 Recovery = 58.30%
Target Compounds Qvalue
-------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration
0426B_23.D S804D05W.M Thu Apr 27 14:33:41 2023 Page 1
ON-SITE
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_23.D Vial: 23
Acq On : 27 Apr 2023 7:00 am Operator: 3545
Sample : L1607939-08 1X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:33 2023 Quant Results File: S804D05W.RES
Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
1.5e+07
1.6e+07
1.7e+07
1.8e+07
1.9e+07
2e+07
2.1e+07
Time-->
Abundance TIC: 0426B_23.D
Pe
r
y
l
e
n
e
-
d
1
2
,
I
Ch
r
y
s
e
n
e
-
d
1
2
,
I
p-
T
e
r
p
h
e
n
y
l
-
d
1
4

,
S
Ph
e
n
a
n
t
h
r
e
n
e
-
d
1
0
,
I
2,
4
,
6
-
T
r
i
b
r
o
m
o
p
h
e
n
o
l

,
S
Ac
e
n
a
p
h
t
h
e
n
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-
d
1
0
,
I
2-
F
l
u
o
r
o
b
i
p
h
e
n
y
l

,
S
Na
p
h
t
h
a
l
e
n
e
-
d
8
,
I
Ni
t
r
o
b
e
n
z
e
n
e
-
d
5

,
S
1,
4
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e
-
d
4
,
I
Ph
e
n
o
l
-
d
5

,
S
2-
F
l
u
o
r
o
p
h
e
n
o
l

,
S
0426B_23.D S804D05W.M Thu Apr 27 14:33:41 2023 Page 2
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_28.D Vial: 28
Acq On : 27 Apr 2023 8:44 am Operator: 3545
Sample : L1607939-09 10X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:42 2023 Quant Results File: S804D05W.RES
Quant Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
DataAcq Meth : BNA4PS
Internal Standards R.T. QIon Response Conc Units Dev(Min)
-------------------------------------------------------------------------
1) 1,4-Dichlorobenzene-d4 3.17 152 65209 8000.00 ppb -0.03
23) Naphthalene-d8 3.90 136 246435 8000.00 ppb -0.03
46) Acenaphthene-d10 5.05 164 135170 8000.00 ppb -0.03
70) Phenanthrene-d10 6.16 188 262032 8000.00 ppb -0.04
84) Chrysene-d12 8.81 240 273052 8000.00 ppb -0.05
94) Perylene-d12 11.38 264 288286 8000.00 ppb -0.07
System Monitoring Compounds
4) 2-Fluorophenol 2.51 112 11588 1135.8971694 ppb -0.02
Spiked Amount 20000.000 Range 20 - 120 Recovery = 5.68%#
7) Phenol-d5 2.95 99 12519 962.6389723 ppb -0.02
Spiked Amount 20000.000 Range 20 - 120 Recovery = 4.81%#
24) Nitrobenzene-d5 3.48 82 4964 447.7235073 ppb -0.03
Spiked Amount 10000.000 Range 18 - 125 Recovery = 4.48%#
50) 2-Fluorobiphenyl 4.58 172 14197 559.5417268 ppb -0.03
Spiked Amount 10000.000 Range 28 - 120 Recovery = 5.60%#
73) 2,4,6-Tribromophenol 5.63 330 4945 1183.0886716 ppb -0.03
Spiked Amount 20000.000 Range 17 - 137 Recovery = 5.92%#
87) p-Terphenyl-d14 7.52 244 23881 635.5446579 ppb -0.04
Spiked Amount 10000.000 Range 13 - 131 Recovery = 6.36%#
Target Compounds Qvalue
-------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration
0426B_28.D S804D05W.M Thu Apr 27 14:42:36 2023 Page 1
ON-SITE
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_28.D Vial: 28
Acq On : 27 Apr 2023 8:44 am Operator: 3545
Sample : L1607939-09 10X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:42 2023 Quant Results File: S804D05W.RES
Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
1.5e+07
1.6e+07
1.7e+07
1.8e+07
1.9e+07
2e+07
2.1e+07
2.2e+07
2.3e+07
2.4e+07
2.5e+07
Time-->
Abundance TIC: 0426B_28.D
Pe
r
y
l
e
n
e
-
d
1
2
,
I
Ch
r
y
s
e
n
e
-
d
1
2
,
I
p-
T
e
r
p
h
e
n
y
l
-
d
1
4

,
S
Ph
e
n
a
n
t
h
r
e
n
e
-
d
1
0
,
I
2,
4
,
6
-
T
r
i
b
r
o
m
o
p
h
e
n
o
l

,
S
Ac
e
n
a
p
h
t
h
e
n
e
-
d
1
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0426B_28.D S804D05W.M Thu Apr 27 14:42:36 2023 Page 2
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_26.D Vial: 26
Acq On : 27 Apr 2023 8:02 am Operator: 3545
Sample : L1607939-10 1X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:37 2023 Quant Results File: S804D05W.RES
Quant Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
DataAcq Meth : BNA4PS
Internal Standards R.T. QIon Response Conc Units Dev(Min)
-------------------------------------------------------------------------
1) 1,4-Dichlorobenzene-d4 3.17 152 64686 8000.00 ppb -0.03
23) Naphthalene-d8 3.90 136 250066 8000.00 ppb -0.03
46) Acenaphthene-d10 5.05 164 139780 8000.00 ppb -0.03
70) Phenanthrene-d10 6.16 188 268877 8000.00 ppb -0.04
84) Chrysene-d12 8.81 240 273206 8000.00 ppb -0.05
94) Perylene-d12 11.38 264 289371 8000.00 ppb -0.07
System Monitoring Compounds
4) 2-Fluorophenol 2.52 112 108666 10737.9519317 ppb 0.00
Spiked Amount 20000.000 Range 20 - 120 Recovery = 53.69%
7) Phenol-d5 2.95 99 124987 9688.4853841 ppb -0.02
Spiked Amount 20000.000 Range 20 - 120 Recovery = 48.44%
24) Nitrobenzene-d5 3.48 82 48119 4277.0316016 ppb -0.03
Spiked Amount 10000.000 Range 18 - 125 Recovery = 42.77%
50) 2-Fluorobiphenyl 4.58 172 132826 5062.3744823 ppb -0.03
Spiked Amount 10000.000 Range 28 - 120 Recovery = 50.62%
73) 2,4,6-Tribromophenol 5.63 330 51764 12069.2284081 ppb -0.03
Spiked Amount 20000.000 Range 17 - 137 Recovery = 60.35%
87) p-Terphenyl-d14 7.52 244 224332 5966.7785704 ppb -0.04
Spiked Amount 10000.000 Range 13 - 131 Recovery = 59.67%
Target Compounds Qvalue
78) Phenanthrene 6.18 178 16405m 429.2121974 ppb
83) Fluoranthene 7.15 202 18751 466.7803453 ppb 96
86) Pyrene 7.36 202 23777 546.2221613 ppb 99
88) Benzylbutyl phthalate 8.08 149 25424 1551.9546716 ppb 93
90) Benzo(a)anthracene 8.80 228 10673 257.9684575 ppb 92
91) Chrysene 8.85 228 12357m 304.6520330 ppb
95) Benzo(b)fluoranthene 10.64 252 11663m 260.6980168 ppb
97) Benzo(a)pyrene 11.26 252 9910 258.0911914 ppb 87
-------------------------------------------------------------------------
(#) = qualifier out of range (m) = manual integration
0426B_26.D S804D05W.M Thu Apr 27 14:37:31 2023 Page 1
ON-SITE
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\042623B\0426B_26.D Vial: 26
Acq On : 27 Apr 2023 8:02 am Operator: 3545
Sample : L1607939-10 1X WG2048871 Inst : BNAMS4
Misc : SOIL ISTD 23D27147 exp 10/27/23 Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Apr 27 14:37 2023 Quant Results File: S804D05W.RES
Method : C:\MSDCHEM\1\METHODS\S804D05W.M (RTE Integrator)
Title : 8270 BNA
Last Update : Wed Apr 05 14:20:16 2023
Response via : Initial Calibration
2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00
0
1000000
2000000
3000000
4000000
5000000
6000000
7000000
8000000
9000000
1e+07
1.1e+07
1.2e+07
1.3e+07
1.4e+07
1.5e+07
1.6e+07
1.7e+07
1.8e+07
1.9e+07
2e+07
2.1e+07
2.2e+07
Time-->
Abundance TIC: 0426B_26.D
Pe
r
y
l
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n
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-
d
1
2
,
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Be
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(
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0426B_26.D S804D05W.M Thu Apr 27 14:37:31 2023 Page 2
#78
Phenanthrene
Concen: 429.2121974 ppb m
RT: 6.18 min Scan# 749
Delta R.T. -0.04 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:178 Resp: 16405
Ion Ratio Lower Upper
178 100
179 15.6 0.0 35.4
152 9.9 0.0 29.2
89 6.2 0.0 28.0
Ref
Raw
Sub
20 40 60 80 100 120 140 160180 200 220 240260 280
0
50
m/z-->
Abundance Scan 706 (6.215 min): 0405_03.D (-701) (-)
178
89 1526311039128 28118221
20 40 60 80 100 120 140 160180 200 220 240260 280
0
50
m/z-->
Abundance Scan 749 (6.179 min): 0426B_26.D
178
28
15255 76 97 125 207 232 261281
20 40 60 80 100 120 140 160180 200 220 240260 280
0
50
m/z-->
Abundance Scan 749 (6.179 min): 0426B_26.D (-706) (-)
178
76 15250 197 231 26194 12317 281
6.10 6.15 6.20
0
10000
20000
30000
Time-->
Abundance Ion 178.00 (177.30 to 178.70):
6.18
Ion 179.00 (178.30 to 179.70):
Ion 152.00 (151.30 to 152.70):
Ion 89.00 (88.30 to 89.70): 042
#83
Fluoranthene
Concen: 466.7803453 ppb
RT: 7.15 min Scan# 907
Delta R.T. -0.04 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:202 Resp: 18751
Ion Ratio Lower Upper
202 100
203 18.8 0.0 36.8
201 18.1 0.0 35.7
200 20.2 0.9 40.9
Ref
Raw
Sub
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 864 (7.186 min): 0405_03.D (-856) (-)
202
101
17475 1501225028 281
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 907 (7.150 min): 0426B_26.D
202
5528 97 125 149 17977 258222 279 303
50 100 150 200 250 300
0
50
m/z-->
Abundance Scan 907 (7.150 min): 0426B_26.D (-864) (-)
202
1016943 174125 150 258 279 30623017
7.10 7.15 7.20
0
10000
20000
30000
Time-->
Abundance Ion 202.00 (201.30 to 202.70):
7.15
Ion 203.00 (202.30 to 203.70):
Ion 201.00 (200.30 to 201.70):
Ion 200.00 (199.30 to 200.70):
L1607939-10 0426B_26.D S804D05W.M Thu Apr 27 14:37:32 2023 Page 3
#86
Pyrene
Concen: 546.2221613 ppb
RT: 7.36 min Scan# 941
Delta R.T. -0.04 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:202 Resp: 23777
Ion Ratio Lower Upper
202 100
203 17.5 0.0 37.7
201 18.2 0.0 38.1
200 20.0 1.2 41.2
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 899 (7.401 min): 0405_03.D (-893) (-)
202
101
1746213316 281 355 429
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 941 (7.359 min): 0426B_26.D
202
55 97
12518 281165 355 429230 327
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 941 (7.359 min): 0426B_26.D (-899) (-)
202
10157 35514729281 429231 327
7.30 7.35 7.40
0
10000
20000
30000
40000
Time-->
Abundance Ion 202.00 (201.30 to 202.70):
7.36
Ion 203.00 (202.30 to 203.70):
Ion 201.00 (200.30 to 201.70):
Ion 200.00 (199.30 to 200.70):
#88
Benzylbutyl phthalate
Concen: 1551.9546716 ppb
RT: 8.08 min Scan# 1059
Delta R.T. -0.05 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:149 Resp: 25424
Ion Ratio Lower Upper
149 100
91 59.1 45.7 85.7
206 25.3 2.6 42.6
150 11.7 0.0 31.7
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1018 (8.132 min): 0405_03.D (-1013) (-)
149
91
206
65 12341 178 23817 283 312 341
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1059 (8.083 min): 0426B_26.D
149
9155
20612328
177 238 291316 342261
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1059 (8.083 min): 0426B_26.D (-1018) (-)
149
91
206
55 12329 238178 312269 336
8.00 8.05 8.10
0
10000
20000
30000
40000
Time-->
Abundance Ion 149.00 (148.30 to 149.70):
8.08
Ion 91.00 (90.30 to 91.70): 042
Ion 206.00 (205.30 to 206.70):
Ion 150.00 (149.30 to 150.70):
L1607939-10 0426B_26.D S804D05W.M Thu Apr 27 14:37:32 2023 Page 4
#90
Benzo(a)anthracene
Concen: 257.9684575 ppb
RT: 8.80 min Scan# 1176
Delta R.T. -0.05 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:228 Resp: 10673
Ion Ratio Lower Upper
228 100
226 28.2 6.3 46.3
114 18.9 0.0 31.8
113 8.2 0.0 31.1
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1136 (8.856 min): 0405_03.D (-1129) (-)
228
113 2008839 15063 17514
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1176 (8.802 min): 0426B_26.D
240
57 97
12528 151 208179 303 362329277
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1176 (8.802 min): 0426B_26.D (-1160) (-)
240
120
2089254 18014530 265290317 347372
8.75 8.80
0
5000
10000
Time-->
Abundance Ion 228.00 (227.30 to 228.70):
8.80
Ion 226.00 (225.30 to 226.70):
Ion 114.00 (113.30 to 114.70):
Ion 113.00 (112.30 to 113.70):
#91
Chrysene
Concen: 304.6520330 ppb m
RT: 8.85 min Scan# 1184
Delta R.T. -0.06 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:228 Resp: 12357
Ion Ratio Lower Upper
228 100
226 34.1 10.2 50.2
229 30.9 0.0 39.2
113 32.3 0.0 32.9
Ref
Raw
Sub
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1145 (8.912 min): 0405_03.D (-1140) (-)
228
113 200881746314738 355282
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1184 (8.851 min): 0426B_26.D
55
97
228
12528
151 179 261 331303 372
50 100 150 200 250 300 350
0
50
m/z-->
Abundance Scan 1184 (8.851 min): 0426B_26.D (-1169) (-)
228
114 16579 200 30753 35017 256 390281
8.80 8.85 8.90
0
5000
10000
15000
Time-->
Abundance Ion 228.00 (227.30 to 228.70):
8.85
Ion 226.00 (225.30 to 226.70):
Ion 229.00 (228.30 to 229.70):
Ion 113.00 (112.30 to 113.70):
L1607939-10 0426B_26.D S804D05W.M Thu Apr 27 14:37:33 2023 Page 5
#95
Benzo(b)fluoranthene
Concen: 260.6980168 ppb m
RT: 10.64 min Scan# 1475
Delta R.T. -0.07 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:252 Resp: 11663
Ion Ratio Lower Upper
252 100
253 32.8 2.3 42.3
126 36.7 0.0 33.7#
113 42.9 0.0 26.6#
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1437 (10.705 min): 0405_03.D (-1429) (-)
252
126
224996317416 281 355
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1475 (10.638 min): 0426B_26.D
57
97
125 25228
165 193 221 360281317 389416
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1475 (10.638 min): 0426B_26.D (-1470) (-)
252
69 123 193 291 38432422116039354 416
10.60 10.65
0
2000
4000
6000
8000
Time-->
Abundance Ion 252.00 (251.30 to 252.70):
10.64
Ion 253.00 (252.30 to 253.70):
Ion 126.00 (125.30 to 126.70):
Ion 113.00 (112.30 to 113.70):
#97
Benzo(a)pyrene
Concen: 258.0911914 ppb
RT: 11.26 min Scan# 1577
Delta R.T. -0.07 min
Lab File: 0426B_26.D
Acq: 27 Apr 2023 8:02 am
Tgt Ion:252 Resp: 9910
Ion Ratio Lower Upper
252 100
253 28.7 1.9 41.9
126 13.9 0.0 34.8
113 18.5 0.0 28.3
Ref
Raw
Sub
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1540 (11.338 min): 0405_03.D (-1531) (-)
252
126
2248716319327 57 282 355
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1577 (11.265 min): 0426B_26.D
57
97
125 25228
165 207 281 343371400315 430
50 100 150 200 250 300 350 400
0
50
m/z-->
Abundance Scan 1577 (11.265 min): 0426B_26.D (-1540) (-)
25257
85
155113 40019530522428357 430
11.20 11.25 11.30
0
2000
4000
6000
8000
Time-->
Abundance Ion 252.00 (251.30 to 252.70):
11.26
Ion 253.00 (252.30 to 253.70):
Ion 126.00 (125.30 to 126.70):
Ion 113.00 (112.30 to 113.70):
L1607939-10 0426B_26.D S804D05W.M Thu Apr 27 14:37:33 2023 Page 6