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HomeMy WebLinkAboutDWQ-2011-020017 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Utah Div. of Water Quality Jim Harris Dear Jim Harris: Red Butte Lab Set ID:1107094 PO Box 144870 SLC, UT 84114 RE: American West Analytical Laboratories received 1 sample(s) on 7/6/2011 for the analyses presented in the following report. All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise. American West Analytical Laboratories is certified by The NELAC Institute in Utah and Texas; and is state certified in Colorado, Idaho, and Missouri. Certification document is available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: _____________________________ Laboratory Director or designee Report Date: 7/20/2011 Page 1 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Client:Utah Div. of Water Quality ORGANIC ANALYTICAL REPORT Contact:Jim Harris Project:Red Butte Lab Sample ID:1107094-001A Client Sample ID:Vought Property Collection Date:7/6/2011 Received Date:7/6/2011 Method:SW8270D Analytical Results SVOA SIM List by GC/MS Method 8270D/3545A 1500h 1700h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:7/19/2011 2100h 7/7/2011 0927hExtracted: 1-Methylnaphthalene 14.2 < 14.290-12-0 2-Methylnaphthalene 14.2 < 14.291-57-6 Acenaphthene 14.2 < 14.283-32-9 Acenaphthylene 14.2 < 14.2208-96-8 Anthracene 14.2 < 14.2120-12-7 Benz(a)anthracene 14.2 71.956-55-3 Benzo(a)pyrene 14.2 35.050-32-8 Benzo(b)fluoranthene 14.2 53.9205-99-2 Benzo(g,h,i)perylene 14.2 < 14.2191-24-2 Benzo(k)fluoranthene 14.2 < 14.2207-08-9 Chrysene 14.2 132218-01-9 Dibenz(a,h)anthracene 14.2 < 14.253-70-3 Fluoranthene 14.2 56.8206-44-0 Fluorene 14.2 < 14.286-73-7 Indene 14.2 < 14.295-13-6 Indeno(1,2,3-cd)pyrene 14.2 29.3193-39-5 Naphthalene 14.2 < 14.291-20-3 Phenanthrene 14.2 74.885-01-8 Pyrene 14.2 80.4129-00-0 Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 7/20/2011 Page 2 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Client:Utah Div. of Water Quality ORGANIC ANALYTICAL REPORT Contact:Jim Harris Project:Red Butte Lab Sample ID:1107094-001A Client Sample ID:Vought Property Collection Date:7/6/2011 Received Date:7/6/2011 Method:SW8270D Analytical Results SVOA Fractionation by GC/MS Method 8270D/3546 1500h 1700h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:7/8/2011 2130h 7/7/2011 0927hExtracted: Acenaphthene 483 < 48383-32-9 Acenaphthylene 483 < 483208-96-8 Anthracene 483 < 483120-12-7 Benz(a)anthracene 483 < 48356-55-3 Benzo(a)pyrene 483 < 48350-32-8 Benzo(b)fluoranthene 483 < 483205-99-2 Benzo(g,h,i)perylene 483 < 483191-24-2 Benzo(k)fluoranthene 483 < 483207-08-9 Chrysene 483 < 483218-01-9 Dibenz(a,h)anthracene 483 < 48353-70-3 Fluoranthene 483 < 483206-44-0 Fluorene 483 < 48386-73-7 Indeno(1,2,3-cd)pyrene 483 < 483193-39-5 Phenanthrene 483 < 48385-01-8 Pyrene 483 < 483 ¹@129-00-0 C11-C12 Aliphatic hydrocarbons 483 12,000 C13-C16 Aliphatic hydrocarbons 483 64,600 C17-C21 Aliphatic hydrocarbons 483 26,400 C22-C35 Aliphatic hydrocarbons 483 160,000 C11-C13 Alkyl Naphthalenes 483 < 483 Total C12-C22 PAH**483 < 483 Surr: Terphenyl-d14 10-265 1011718-51-0 ¹ - Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. @ - High RPD due to suspected sample non-homogeneity or matrix interference. ** - This value is a summation of the PAH compounds listed above. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 7/20/2011 Page 3 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Client:Utah Div. of Water Quality ORGANIC ANALYTICAL REPORT Contact:Jim Harris Project:Red Butte Lab Sample ID:1107094-001A Client Sample ID:Vought Property Collection Date:7/6/2011 Received Date:7/6/2011 Method:SW8260C Analytical Results VOAs by GC/MS Method 8260C 1500h 1700h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:10 CAS Number Qual Analyzed:7/7/2011 1345h 1,1,1,2-Tetrachloroethane 28.4 < 28.4630-20-6 1,1,1-Trichloroethane 28.4 < 28.471-55-6 1,1,2,2-Tetrachloroethane 28.4 < 28.479-34-5 1,1,2-Trichloro-1,2,2-trifluoroethane 28.4 < 28.476-13-1 1,1,2-Trichloroethane 28.4 < 28.479-00-5 1,1-Dichloropropene 28.4 < 28.4563-58-6 1,1-Dichloroethane 28.4 < 28.475-34-3 1,1-Dichloroethene 28.4 < 28.475-35-4 1,2,3-Trichlorobenzene 28.4 < 28.487-61-6 1,2,3-Trichloropropane 28.4 < 28.496-18-4 1,2,3-Trimethylbenzene 28.4 < 28.4526-73-8 1,2,4-Trichlorobenzene 28.4 < 28.4120-82-1 1,2,4-Trimethylbenzene 28.4 < 28.495-63-6 1,2-Dibromo-3-chloropropane 71.0 < 71.096-12-8 1,2-Dibromoethane 28.4 < 28.4106-93-4 1,2-Dichlorobenzene 28.4 < 28.495-50-1 1,2-Dichloroethane 28.4 < 28.4107-06-2 1,2-Dichloropropane 28.4 < 28.478-87-5 1,3,5-Trimethylbenzene 28.4 < 28.4108-67-8 1,3-Dichlorobenzene 28.4 < 28.4541-73-1 1,3-Dichloropropane 28.4 < 28.4142-28-9 1,4-Dichlorobenzene 28.4 < 28.4106-46-7 1,4-Dioxane 710 < 710123-91-1 2,2-Dichloropropane 28.4 < 28.4594-20-7 2-Butanone 142 < 14278-93-3 2-Chloroethyl vinyl ether 71.0 < 71.0110-75-8 2-Chlorotoluene 28.4 < 28.495-49-8 2-Hexanone 71.0 < 71.0591-78-6 2-Nitropropane 71.0 < 71.079-46-9 4-Chlorotoluene 28.4 < 28.4106-43-4 Report Date: 7/20/2011 Page 4 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1107094-001A Client Sample ID:Vought Property Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:10 CAS Number Qual Analyzed:7/7/2011 1345h 4-Isopropyltoluene 28.4 < 28.499-87-6 4-Methyl-2-pentanone 71.0 < 71.0108-10-1 Acetone 142 < 14267-64-1 Acetonitrile 71.0 < 71.075-05-8 Acrolein 71.0 < 71.0107-02-8 Acrylonitrile 142 < 142107-13-1 Allyl chloride 71.0 < 71.0107-05-1 Benzene 28.4 < 28.471-43-2 Benzyl chloride 71.0 < 71.0100-44-7 Bis(2-chloroisopropyl) ether 71.0 < 71.0108-60-1 Bromobenzene 28.4 < 28.4108-86-1 Bromochloromethane 28.4 < 28.474-97-5 Bromodichloromethane 28.4 < 28.475-27-4 Bromoform 28.4 < 28.475-25-2 Bromomethane 71.0 < 71.074-83-9 Butyl acetate 142 < 142123-86-4 Carbon disulfide 28.4 < 28.475-15-0 Carbon tetrachloride 28.4 < 28.456-23-5 Chlorobenzene 28.4 < 28.4108-90-7 Chloroethane 28.4 < 28.475-00-3 Chloroform 28.4 < 28.467-66-3 Chloromethane 71.0 < 71.074-87-3 Chloroprene 28.4 < 28.4126-99-8 cis-1,2-Dichloroethene 28.4 < 28.4156-59-2 cis-1,3-Dichloropropene 28.4 < 28.410061-01-5 Cyclohexane 28.4 < 28.4110-82-7 Cyclohexanone 710 < 710108-94-1 Dibromochloromethane 28.4 < 28.4124-48-1 Dibromomethane 28.4 < 28.474-95-3 Dichlorodifluoromethane 28.4 < 28.475-71-8 Ethyl acetate 142 < 142141-78-6 Ethyl ether 142 < 14260-29-7 Ethyl methacrylate 28.4 < 28.497-63-2 Ethylbenzene 28.4 < 28.4100-41-4 Hexachlorobutadiene 28.4 < 28.487-68-3 Iodomethane 71.0 < 71.074-88-4 Isobutyl alcohol 1,420 < 1,42078-83-1 Report Date: 7/20/2011 Page 5 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1107094-001A Client Sample ID:Vought Property Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:10 CAS Number Qual Analyzed:7/7/2011 1345h Isopropyl acetate 142 < 142108-21-4 Isopropyl alcohol 568 < 56867-63-0 Isopropylbenzene 28.4 < 28.498-82-8 Isopropyltoluene 28.4 < 28.499-87-6 m,p-Xylene 28.4 < 28.4179601-23-1 Methacrylonitrile 71.0 < 71.0126-98-7 Methyl Acetate 71.0 < 71.079-20-9 Methyl methacrylate 71.0 < 71.080-62-6 Methyl tert-butyl ether 28.4 < 28.41634-04-4 Methylcyclohexane 28.4 < 28.4108-87-2 Methylene chloride 71.0 < 71.075-09-2 n-Amyl acetate 142 < 142628-63-7 n-Butyl alcohol 1,420 < 1,42071-36-3 n-Butylbenzene 28.4 < 28.4104-51-8 n-Hexane 28.4 < 28.4110-54-3 n-Octane 28.4 < 28.4111-65-9 n-Propylbenzene 28.4 < 28.4103-65-1 Naphthalene 28.4 < 28.491-20-3 o-Xylene 28.4 < 28.495-47-6 Pentachloroethane 28.4 < 28.476-01-7 Propionitrile 355 < 355107-12-0 Propyl acetate 142 < 142109-60-4 sec-Butylbenzene 28.4 < 28.4135-98-8 Styrene 28.4 < 28.4100-42-5 tert-Butyl alcohol 284 < 28476-65-0 tert-Butylbenzene 28.4 < 28.498-06-6 Tetrachloroethene 28.4 < 28.4127-18-4 Tetrahydrofuran 28.4 < 28.4109-99-9 Toluene 28.4 < 28.4108-88-3 trans-1,2-Dichloroethene 28.4 < 28.4156-60-5 trans-1,3-Dichloropropene 28.4 < 28.410061-02-6 trans-1,4-Dichloro-2-butene 28.4 < 28.4110-57-6 Trichloroethene 28.4 < 28.479-01-6 Trichlorofluoromethane 28.4 < 28.475-69-4 Vinyl acetate 142 < 142108-05-4 Vinyl chloride 14.2 < 14.275-01-4 Xylenes, Total 28.4 < 28.41330-20-7 Report Date: 7/20/2011 Page 6 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1107094-001A Client Sample ID:Vought Property Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:10 CAS Number Qual Analyzed:7/7/2011 1345h TPH C6-C10 (GRO)284 5,230 Surr: 1,2-Dichloroethane-d4 68-147 98.717060-07-0 Surr: 4-Bromofluorobenzene 71-144 105460-00-4 Surr: Dibromofluoromethane 71-129 97.81868-53-7 Surr: Toluene-d8 72-129 1052037-26-5 The reporting limits were raised due to high analyte concentrations. Sampling and analytical preparation performed by method 5030C. Report Date: 7/20/2011 Page 7 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSSV QC Type:LCS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Acenaphthene5,33380.110-15004,270µg/kg7/8/2011LCS-13165 SW8270D 2104h Benzo(a)pyrene5,33374.038-19403,950µg/kg7/8/2011LCS-13165 SW8270D 2104h Pyrene5,33376.622-16704,080µg/kg7/8/2011LCS-13165 SW8270D 2104h Surr: 2,4,6-Tribromophenol5,33391.810-1574,900%REC7/8/2011LCS-13165 SW8270D 2104h Surr: 2-Fluorobiphenyl2,66778.522-1282,090%REC7/8/2011LCS-13165 SW8270D 2104h Surr: 2-Fluorophenol5,33371.710-1353,820%REC7/8/2011LCS-13165 SW8270D 2104h Surr: Nitrobenzene-d52,66791.110-1452,430%REC7/8/2011LCS-13165 SW8270D 2104h Surr: Phenol-d65,33380.010-1574,270%REC7/8/2011LCS-13165 SW8270D 2104h Surr: Terphenyl-d142,66785.422-1672,280%REC7/8/2011LCS-13165 SW8270D 2104h Acenaphthene5,33374.810-15003,990µg/kg7/19/2011LCS-13165 SW8270D 2034h Benzo(a)pyrene5,33353.038-19402,830µg/kg7/19/2011LCS-13165 SW8270D 2034h Pyrene5,33372.822-16703,880µg/kg7/19/2011LCS-13165 SW8270D 2034h Surr: 2,4,6-Tribromophenol-0%REC7/19/2011LCS-13165 SW8270D 2034h Surr: 2-Fluorobiphenyl-0%REC7/19/2011LCS-13165 SW8270D 2034h Surr: 2-Fluorophenol-0%REC7/19/2011LCS-13165 SW8270D 2034h Surr: Nitrobenzene-d5-0%REC7/19/2011LCS-13165 SW8270D 2034h Surr: Phenol-d6-0%REC7/19/2011LCS-13165 SW8270D 2034h Surr: Terphenyl-d14-0%REC7/19/2011LCS-13165 SW8270D 2034h Report Date: 7/20/2011 Page 8 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1-Methylnaphthalene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h 2-Methylnaphthalene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Acenaphthene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Acenaphthylene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Anthracene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Benz(a)anthracene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Benzo(a)pyrene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Benzo(b)fluoranthene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Benzo(g,h,i)perylene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Benzo(k)fluoranthene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h C11-C12 Aliphatic hydrocarbons-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h C11-C13 Alkyl Naphthalenes-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h C13-C16 Aliphatic hydrocarbons-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h C17-C21 Aliphatic hydrocarbons-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h C22-C35 Aliphatic hydrocarbons-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Chrysene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Dibenz(a,h)anthracene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Fluoranthene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Fluorene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Indene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Indeno(1,2,3-cd)pyrene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Naphthalene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Phenanthrene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Report Date: 7/20/2011 Page 9 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Pyrene-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Total C12-C22 PAH**-< 340µg/kg7/8/2011MB-13165 SW8270D 2037h Surr: 2,4,6-Tribromophenol5,33366.710-1573,560%REC7/8/2011MB-13165 SW8270D 2037h Surr: 2-Fluorobiphenyl2,66772.922-1281,940%REC7/8/2011MB-13165 SW8270D 2037h Surr: 2-Fluorophenol5,33363.110-1113,360%REC7/8/2011MB-13165 SW8270D 2037h Surr: Nitrobenzene-d52,66783.610-1452,230%REC7/8/2011MB-13165 SW8270D 2037h Surr: Phenol-d65,33371.010-1573,790%REC7/8/2011MB-13165 SW8270D 2037h Surr: Terphenyl-d142,66777.922-1672,080%REC7/8/2011MB-13165 SW8270D 2037h 1-Methylnaphthalene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h 2-Methylnaphthalene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Acenaphthene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Acenaphthylene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Anthracene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Benz(a)anthracene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Benzo(a)pyrene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Benzo(b)fluoranthene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Benzo(g,h,i)perylene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Benzo(k)fluoranthene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Chrysene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Dibenz(a,h)anthracene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Fluoranthene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Fluorene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Indene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Report Date: 7/20/2011 Page 10 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Indeno(1,2,3-cd)pyrene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Naphthalene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Phenanthrene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Pyrene-< 10.0µg/kg7/19/2011MB-13165 SW8270D 2008h Surr: 2,4,6-Tribromophenol-0%REC7/19/2011MB-13165 SW8270D 2008h Surr: 2-Fluorobiphenyl-0%REC7/19/2011MB-13165 SW8270D 2008h Surr: 2-Fluorophenol-0%REC7/19/2011MB-13165 SW8270D 2008h Surr: Nitrobenzene-d5-0%REC7/19/2011MB-13165 SW8270D 2008h Surr: Phenol-d6-0%REC7/19/2011MB-13165 SW8270D 2008h Surr: Terphenyl-d14-0%REC7/19/2011MB-13165 SW8270D 2008h Report Date: 7/20/2011 Page 11 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSSV QC Type:MS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Acenaphthene7,57068.431-11305,180µg/kg-dry7/8/20111107094-001AMS SW8270D 2156h Benzo(a)pyrene7,57074.338-16905,620µg/kg-dry7/8/20111107094-001AMS SW8270D 2156h Pyrene7,5709.3631-150 ¹0709µg/kg-dry7/8/20111107094-001AMS SW8270D 2156h Surr: 2,4,6-Tribromophenol7,57070.710-2375,350%REC7/8/20111107094-001AMS SW8270D 2156h Surr: 2-Fluorobiphenyl3,78671.317-1792,700%REC7/8/20111107094-001AMS SW8270D 2156h Surr: 2-Fluorophenol7,57071.410-1865,400%REC7/8/20111107094-001AMS SW8270D 2156h Surr: Nitrobenzene-d53,78691.010-1663,450%REC7/8/20111107094-001AMS SW8270D 2156h Surr: Phenol-d67,57078.610-1945,950%REC7/8/20111107094-001AMS SW8270D 2156h Surr: Terphenyl-d143,78691.510-2653,460%REC7/8/20111107094-001AMS SW8270D 2156h Acenaphthene7,57076.031-11305,750µg/kg-dry7/19/20111107094-001AMS SW8270D 2126h Benzo(a)pyrene7,57051.538-16935.013,940µg/kg-dry7/19/20111107094-001AMS SW8270D 2126h Pyrene7,57072.931-15080.445,600µg/kg-dry7/19/20111107094-001AMS SW8270D 2126h Surr: 2,4,6-Tribromophenol0010-2370%REC7/19/20111107094-001AMS SW8270D 2126h Surr: 2-Fluorobiphenyl0017-1790%REC7/19/20111107094-001AMS SW8270D 2126h Surr: 2-Fluorophenol0010-1860%REC7/19/20111107094-001AMS SW8270D 2126h Surr: Nitrobenzene-d50010-1660%REC7/19/20111107094-001AMS SW8270D 2126h Surr: Phenol-d60010-1940%REC7/19/20111107094-001AMS SW8270D 2126h Surr: Terphenyl-d140010-2650%REC7/19/20111107094-001AMS SW8270D 2126h ¹ - Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/20/2011 Page 12 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSSV QC Type:MSD AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Acenaphthene7,57073.831-113 3507.655,590µg/kg-dry7/8/20111107094-001AMSD SW8270D 2222h Benzo(a)pyrene7,57072.538-169 3502.355,490µg/kg-dry7/8/20111107094-001AMSD SW8270D 2222h Pyrene7,57081.731-150 35@01596,180µg/kg-dry7/8/20111107094-001AMSD SW8270D 2222h Surr: 2,4,6-Tribromophenol7,57072.210-237 05,470%REC7/8/20111107094-001AMSD SW8270D 2222h Surr: 2-Fluorobiphenyl3,78672.517-179 02,740%REC7/8/20111107094-001AMSD SW8270D 2222h Surr: 2-Fluorophenol7,57068.510-186 05,180%REC7/8/20111107094-001AMSD SW8270D 2222h Surr: Nitrobenzene-d53,78684.810-166 03,210%REC7/8/20111107094-001AMSD SW8270D 2222h Surr: Phenol-d67,57074.510-194 05,640%REC7/8/20111107094-001AMSD SW8270D 2222h Surr: Terphenyl-d143,78687.110-265 03,300%REC7/8/20111107094-001AMSD SW8270D 2222h Acenaphthene7,57073.531-113 3503.345,560µg/kg-dry7/19/20111107094-001AMSD SW8270D 2152h Benzo(a)pyrene7,57053.038-169 3535.01 2.844,050µg/kg-dry7/19/20111107094-001AMSD SW8270D 2152h Pyrene7,57073.431-150 3580.44 0.6735,640µg/kg-dry7/19/20111107094-001AMSD SW8270D 2152h Surr: 2,4,6-Tribromophenol0010-237 00%REC7/19/20111107094-001AMSD SW8270D 2152h Surr: 2-Fluorobiphenyl0017-179 00%REC7/19/20111107094-001AMSD SW8270D 2152h Surr: 2-Fluorophenol0010-186 00%REC7/19/20111107094-001AMSD SW8270D 2152h Surr: Nitrobenzene-d50010-166 00%REC7/19/20111107094-001AMSD SW8270D 2152h Surr: Phenol-d60010-194 00%REC7/19/20111107094-001AMSD SW8270D 2152h Surr: Terphenyl-d140010-265 00%REC7/19/20111107094-001AMSD SW8270D 2152h @ - High RPD due to suspected sample non-homogeneity or matrix interference. Report Date: 7/20/2011 Page 13 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:LCS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1-Trichloroethane20.0012452-144024.7µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h 1,1-Dichloroethene20.0010036-184020.0µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h 1,2-Dichlorobenzene20.0010770-134021.4µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h 1,2-Dichloroethane20.0011155-146022.3µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h 1,2-Dichloropropane20.0091.456-133018.3µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Benzene20.0096.760-130019.3µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Chlorobenzene20.0010375-130020.6µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Chloroform20.0011061-130022.0µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Ethylbenzene20.0010669-147021.2µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Isopropylbenzene20.0011065-147022.0µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Methyl tert-butyl ether20.0097.033.1-139019.4µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Methylene chloride20.0010439-164020.8µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Naphthalene20.0082.240-131016.4µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Tetrahydrofuran20.0090.243-146018.0µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Toluene20.0010161-140020.2µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Trichloroethene20.0011151-154022.1µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Xylenes, Total60.0010472-147062.5µg/kg7/7/2011LCS VOC 070711A SW8260C 0917h Surr: 1,2-Dichloroethane-d450.0011873-13258.8%REC7/7/2011LCS VOC 070711A SW8260C 0917h Surr: 4-Bromofluorobenzene50.0010285-11550.9%REC7/7/2011LCS VOC 070711A SW8260C 0917h Surr: Dibromofluoromethane50.0010784-12153.3%REC7/7/2011LCS VOC 070711A SW8260C 0917h Surr: Toluene-d850.0099.185-11549.5%REC7/7/2011LCS VOC 070711A SW8260C 0917h Report Date: 7/20/2011 Page 14 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1,2-Tetrachloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1,1-Trichloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1,2,2-Tetrachloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1,2-Trichloro-1,2,2- trifluoroethane -< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1,2-Trichloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1-Dichloropropene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1-Dichloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,1-Dichloroethene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2,3-Trichlorobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2,3-Trichloropropane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2,3-Trimethylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2,4-Trichlorobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2,4-Trimethylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2-Dibromo-3-chloropropane-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2-Dibromoethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2-Dichlorobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2-Dichloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,2-Dichloropropane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,3,5-Trimethylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,3-Dichlorobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,3-Dichloropropane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 1,4-Dichlorobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Report Date: 7/20/2011 Page 15 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,4-Dioxane-< 50.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 2,2-Dichloropropane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 2-Butanone-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 2-Chloroethyl vinyl ether-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 2-Chlorotoluene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 2-Hexanone-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 2-Nitropropane-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 4-Chlorotoluene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 4-Isopropyltoluene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h 4-Methyl-2-pentanone-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Acetone-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Acetonitrile-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Acrolein-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Acrylonitrile-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Allyl chloride-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Benzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Benzyl chloride-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Bis(2-chloroisopropyl) ether-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Bromobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Bromochloromethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Bromodichloromethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Bromoform-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Bromomethane-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Report Date: 7/20/2011 Page 16 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Butyl acetate-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Carbon disulfide-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Carbon tetrachloride-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Chlorobenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Chloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Chloroform-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Chloromethane-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Chloroprene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h cis-1,2-Dichloroethene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h cis-1,3-Dichloropropene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Cyclohexane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Cyclohexanone-< 50.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Dibromochloromethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Dibromomethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Dichlorodifluoromethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Ethyl acetate-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Ethyl ether-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Ethyl methacrylate-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Ethylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Hexachlorobutadiene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Iodomethane-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Isobutyl alcohol-< 100µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Isopropyl acetate-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Report Date: 7/20/2011 Page 17 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Isopropyl alcohol-< 40.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Isopropylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Isopropyltoluene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h m,p-Xylene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Methacrylonitrile-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Methyl Acetate-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Methyl methacrylate-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Methyl tert-butyl ether-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Methylcyclohexane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Methylene chloride-< 5.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h n-Amyl acetate-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Naphthalene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h n-Butyl alcohol-< 100µg/kg7/7/2011MB VOC 070711A SW8260C 1002h n-Butylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h n-Hexane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h n-Octane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h n-Propylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h o-Xylene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Pentachloroethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Propionitrile-< 25.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Propyl acetate-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h sec-Butylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Styrene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Report Date: 7/20/2011 Page 18 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris tert-Butyl alcohol-< 20.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h tert-Butylbenzene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Tetrachloroethene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Tetrahydrofuran-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Toluene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h TPH C6-C10 (GRO)-< 20.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h trans-1,2-Dichloroethene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h trans-1,3-Dichloropropene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h trans-1,4-Dichloro-2-butene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Trichloroethene-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Trichlorofluoromethane-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Vinyl acetate-< 10.0µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Vinyl chloride-< 1.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Xylenes, Total-< 2.00µg/kg7/7/2011MB VOC 070711A SW8260C 1002h Surr: 1,2-Dichloroethane-d450.0012873-13263.8%REC7/7/2011MB VOC 070711A SW8260C 1002h Surr: 4-Bromofluorobenzene50.0010285-11550.8%REC7/7/2011MB VOC 070711A SW8260C 1002h Surr: Dibromofluoromethane50.0011184-12155.3%REC7/7/2011MB VOC 070711A SW8260C 1002h Surr: Toluene-d850.0097.785-11548.8%REC7/7/2011MB VOC 070711A SW8260C 1002h Report Date: 7/20/2011 Page 19 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1-Trichloroethane283.910520-1440298µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h 1,1-Dichloroethene283.910124-1740288µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h 1,2-Dichlorobenzene283.910410-1480295µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h 1,2-Dichloroethane283.997.054-1330276µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h 1,2-Dichloropropane283.995.528-1400271µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Benzene283.997.817-1380278µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Chlorobenzene283.910513-1500298µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Chloroform283.996.621-1470274µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Ethylbenzene283.910510-1640299µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Isopropylbenzene283.910126-1460288µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Methyl tert-butyl ether283.994.028-1370267µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Methylene chloride283.911210-2170319µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Naphthalene283.912113-1560343µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Tetrahydrofuran283.913310-1360377µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Toluene283.910423-1680295µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Trichloroethene283.910514-1610299µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Xylenes, Total851.710210-1600871µg/kg-dry7/7/20111107094-001AMS SW8260C 1300h Surr: 1,2-Dichloroethane-d4709.710268-147722%REC7/7/20111107094-001AMS SW8260C 1300h Surr: 4-Bromofluorobenzene709.710571-144744%REC7/7/20111107094-001AMS SW8260C 1300h Surr: Dibromofluoromethane709.799.071-129702%REC7/7/20111107094-001AMS SW8260C 1300h Surr: Toluene-d8709.710272-129726%REC7/7/20111107094-001AMS SW8260C 1300h Report Date: 7/20/2011 Page 20 of 21 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Client:Utah Div. of Water Quality Lab Set ID:1107094 QC SUMMARY REPORT Dept:MSVOA QC Type:MSD AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1-Trichloroethane283.910420-144 3501.1295µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h 1,1-Dichloroethene283.998.524-174 3502.9280µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h 1,2-Dichlorobenzene283.910510-148 3501.34299µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h 1,2-Dichloroethane283.998.754-133 3501.74280µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h 1,2-Dichloropropane283.995.628-140 3500.0523271µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Benzene283.997.617-138 3500.153277µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Chlorobenzene283.910413-150 3500.573297µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Chloroform283.998.321-147 3501.74279µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Ethylbenzene283.910410-164 3501.53295µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Isopropylbenzene283.910226-146 3500.933290µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Methyl tert-butyl ether283.997.728-137 3503.91278µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Methylene chloride283.911210-217 3500.848317µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Naphthalene283.911513-156 3504.66327µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Tetrahydrofuran283.913310-136 3500.526379µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Toluene283.910323-168 3501.11291µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Trichloroethene283.910614-161 3500.569300µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Xylenes, Total851.710310-160 3500.52876µg/kg-dry7/7/20111107094-001AMSD SW8260C 1322h Surr: 1,2-Dichloroethane-d4709.710368-147 0733%REC7/7/20111107094-001AMSD SW8260C 1322h Surr: 4-Bromofluorobenzene709.710371-144 0734%REC7/7/20111107094-001AMSD SW8260C 1322h Surr: Dibromofluoromethane709.710071-129 0713%REC7/7/20111107094-001AMSD SW8260C 1322h Surr: Toluene-d8709.710272-129 0721%REC7/7/20111107094-001AMSD SW8260C 1322h Report Date: 7/20/2011 Page 21 of 21