Loading...
HomeMy WebLinkAboutDWQ-2011-020002 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Utah DEQ DERR Jim Harris Dear Jim Harris: Red Butte Creek - Hayes Property Lab Set ID:1101433 TEL:(801) 536-4145 168 N. 1950 W., 1st Floor Salt Lake City, Ut 84116 RE: American West Analytical Laboratories received 1 sample(s) on 1/27/2011 for the analyses presented in the following report. All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise. American West Analytical Laboratories is certified by The NELAC Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification document is available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitaion limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: _____________________________ Laboratory Director or designee Report Date: 2/8/2011 Page 1 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Client:Utah DEQ DERR ORGANIC ANALYTICAL REPORT Contact:Jim Harris Project:Red Butte Creek - Hayes Property Lab Sample ID:1101433-001B Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8260C Analytical Results VOAs by GC/MS Method 8260C 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:50 CAS Number Qual Analyzed:1/28/2011 1539h 1,1,1,2-Tetrachloroethane 127 < 127630-20-6 1,1,1-Trichloroethane 127 < 12771-55-6 1,1,2,2-Tetrachloroethane 127 < 12779-34-5 1,1,2-Trichloro-1,2,2-trifluoroethane 127 < 12776-13-1 1,1,2-Trichloroethane 127 < 12779-00-5 1,1-Dichloropropene 127 < 127563-58-6 1,1-Dichloroethane 127 < 12775-34-3 1,1-Dichloroethene 127 < 12775-35-4 1,2,3-Trichlorobenzene 127 < 12787-61-6 1,2,3-Trichloropropane 127 < 12796-18-4 1,2,3-Trimethylbenzene 127 203526-73-8 1,2,4-Trichlorobenzene 127 < 127120-82-1 1,2,4-Trimethylbenzene 127 47395-63-6 1,2-Dibromo-3-chloropropane 318 < 31896-12-8 1,2-Dibromoethane 127 < 127106-93-4 1,2-Dichlorobenzene 127 < 12795-50-1 1,2-Dichloroethane 127 < 127107-06-2 1,2-Dichloropropane 127 < 127 @78-87-5 1,3,5-Trimethylbenzene 127 235108-67-8 1,3-Dichlorobenzene 127 < 127541-73-1 1,3-Dichloropropane 127 < 127142-28-9 1,4-Dichlorobenzene 127 < 127106-46-7 1,4-Dioxane 3,180 < 3,180123-91-1 2,2-Dichloropropane 127 < 127594-20-7 2-Butanone 636 < 63678-93-3 2-Chloroethyl vinyl ether 318 < 318110-75-8 2-Chlorotoluene 127 < 12795-49-8 2-Hexanone 318 < 318591-78-6 2-Nitropropane 318 < 31879-46-9 4-Chlorotoluene 127 < 127106-43-4 Report Date: 2/8/2011 Page 2 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001B Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8260C Analytical Results VOAs by GC/MS Method 8260C 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:50 CAS Number Qual Analyzed:1/28/2011 1539h 4-Isopropyltoluene 127 31799-87-6 4-Methyl-2-pentanone 318 < 318108-10-1 Acetone 636 < 63667-64-1 Acetonitrile 318 < 31875-05-8 Acrolein 318 < 318107-02-8 Acrylonitrile 636 < 636107-13-1 Allyl chloride 318 < 318107-05-1 Benzene 127 < 12771-43-2 Benzyl chloride 318 < 318100-44-7 Bis(2-chloroisopropyl) ether 318 < 318108-60-1 Bromobenzene 127 < 127108-86-1 Bromochloromethane 127 < 12774-97-5 Bromodichloromethane 127 < 12775-27-4 Bromoform 127 < 12775-25-2 Bromomethane 318 < 31874-83-9 Butyl acetate 636 < 636123-86-4 Carbon disulfide 127 < 12775-15-0 Carbon tetrachloride 127 < 12756-23-5 Chlorobenzene 127 < 127108-90-7 Chloroethane 127 < 12775-00-3 Chloroform 127 < 12767-66-3 Chloromethane 318 < 31874-87-3 Chloroprene 127 < 127126-99-8 cis-1,2-Dichloroethene 127 < 127156-59-2 cis-1,3-Dichloropropene 127 < 12710061-01-5 Cyclohexane 127 < 127110-82-7 Cyclohexanone 3,180 < 3,180108-94-1 Dibromochloromethane 127 < 127124-48-1 Dibromomethane 127 < 12774-95-3 Dichlorodifluoromethane 127 < 12775-71-8 Ethyl acetate 636 < 636141-78-6 Ethyl ether 636 < 63660-29-7 Ethyl methacrylate 127 < 12797-63-2 Report Date: 2/8/2011 Page 3 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001B Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8260C Analytical Results VOAs by GC/MS Method 8260C 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:50 CAS Number Qual Analyzed:1/28/2011 1539h Ethylbenzene 127 < 127100-41-4 Hexachlorobutadiene 127 < 12787-68-3 Iodomethane 318 < 31874-88-4 Isobutyl alcohol 6,360 < 6,36078-83-1 Isopropyl acetate 636 < 636108-21-4 Isopropyl alcohol 2,540 < 2,54067-63-0 Isopropylbenzene 127 < 12798-82-8 Isopropyltoluene 127 31799-87-6 m,p-Xylene 127 < 127179601-23-1 Methacrylonitrile 318 < 318126-98-7 Methyl Acetate 318 < 31879-20-9 Methyl methacrylate 318 < 31880-62-6 Methyl tert-butyl ether 127 < 127 @1634-04-4 Methylcyclohexane 127 200108-87-2 Methylene chloride 318 < 31875-09-2 n-Amyl acetate 636 < 636628-63-7 n-Butyl alcohol 6,360 < 6,36071-36-3 n-Butylbenzene 127 < 127104-51-8 n-Hexane 127 < 127110-54-3 n-Octane 127 2,120111-65-9 n-Propylbenzene 127 < 127103-65-1 Naphthalene 127 < 12791-20-3 o-Xylene 127 < 12795-47-6 Pentachloroethane 127 < 12776-01-7 Propionitrile 1,590 < 1,590107-12-0 Propyl acetate 636 < 636109-60-4 sec-Butylbenzene 127 < 127135-98-8 Styrene 127 < 127100-42-5 tert-Butyl alcohol 1,270 < 1,27076-65-0 tert-Butylbenzene 127 < 12798-06-6 Tetrachloroethene 127 < 127127-18-4 Tetrahydrofuran 127 < 127109-99-9 Toluene 127 < 127108-88-3 Report Date: 2/8/2011 Page 4 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001B Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8260C Analytical Results VOAs by GC/MS Method 8260C 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:50 CAS Number Qual Analyzed:1/28/2011 1539h trans-1,2-Dichloroethene 127 < 127156-60-5 trans-1,3-Dichloropropene 127 < 12710061-02-6 trans-1,4-Dichloro-2-butene 127 < 127110-57-6 Trichloroethene 127 < 12779-01-6 Trichlorofluoromethane 127 < 12775-69-4 Vinyl acetate 636 < 636108-05-4 Vinyl chloride 63.6 < 63.675-01-4 Xylenes, Total 127 < 1271330-20-7 C11&C12 Aliphatic hydrocarbons 1,270 80,600 C6 Aliphatic hydrocarbons 1,270 < 1,270 C7&C8 Aliphatic hydrocarbons 1,270 5,020 C9&C10 Aliphatic hydrocarbons 1,270 37,000 C9&C10 Alkyl Benzenes 1,270 3,140 Total Purgable Petroleum Hydrocarbons (C6-C15)1,270 126,000 TPH C11-C15 (DRO)1,270 80,600 TPH C6-C10 (GRO)1,270 45,100 Surr: 1,2-Dichloroethane-d4 68-147 10617060-07-0 Surr: 4-Bromofluorobenzene 71-144 99.0460-00-4 Surr: Dibromofluoromethane 71-129 1061868-53-7 Surr: Toluene-d8 72-129 97.52037-26-5 @ - High RPD due to suspected sample non-homogeneity or matrix interference. The sample was received with headspace. The reporting limits were raised due to high analyte concentrations. Sampling and analytical preparation performed by method 5030C. Report Date: 2/8/2011 Page 5 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Client:Utah DEQ DERR ORGANIC ANALYTICAL REPORT Contact:Jim Harris Project:Red Butte Creek - Hayes Property Lab Sample ID:1101433-001A Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8270D Analytical Results SVOA List by GC/MS Method 8270D/3545A 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/1/2011 1521h 1/27/2011 1700hExtracted: 1-Methylnaphthalene 12.7 143 $90-12-0 2-Methylnaphthalene 12.7 56.8 $91-57-6 Acenaphthene 12.7 19.5 $¹83-32-9 Acenaphthylene 12.7 < 12.7 $208-96-8 Anthracene 12.7 108 $120-12-7 Benz(a)anthracene 12.7 130 $56-55-3 Benzo(a)pyrene 12.7 102 $50-32-8 Benzo(b)fluoranthene 12.7 73.8 $205-99-2 Benzo(g,h,i)perylene 12.7 73.0 $191-24-2 Benzo(k)fluoranthene 12.7 56.8 $207-08-9 Chrysene 12.7 127 $218-01-9 Dibenz(a,h)anthracene 12.7 64.5 $53-70-3 Fluoranthene 12.7 95.9 $206-44-0 Fluorene 12.7 32.2 $86-73-7 Indene 12.7 16.1 $95-13-6 Indeno(1,2,3-cd)pyrene 12.7 20.4 $193-39-5 Naphthalene 12.7 25.4 $91-20-3 Phenanthrene 12.7 112 $85-01-8 Pyrene 12.7 107 $129-00-0 $ - Samples utilized SIM analysis to achieve required PQLs. ¹ - Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/2/2011 1359h 1/27/2011 1700hExtracted: 1,1´-Biphenyl 433 < 43392-52-4 1,2,4,5-Tetrachlorobenzene 433 < 43395-94-3 1,2,4-Trichlorobenzene 433 < 433120-82-1 1,2-Dichlorobenzene 433 < 43395-50-1 Report Date: 2/8/2011 Page 6 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001A Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8270D Analytical Results SVOA List by GC/MS Method 8270D/3545A 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/2/2011 1359h 1/27/2011 1700hExtracted: 1,3,5-Trinitrobenzene 433 < 43399-35-4 1,4-Naphthoquinone 853 < 853130-15-4 1,3-Dichlorobenzene 433 < 433541-73-1 1,3-Dinitrobenzene 433 < 43399-65-0 1,4-Dichlorobenzene 433 < 433 ¹106-46-7 1,4-Phenylenediamine 433 < 433106-50-3 1-Chloronaphthalene 433 < 43390-13-1 1-Methylnaphthalene 433 < 43390-12-0 1-Naphthylamine 853 < 853134-32-7 2,3,4,6-Tetrachlorophenol 433 < 43358-90-2 2,4,5-Trichlorophenol 433 < 43395-95-4 2,4,6-Trichlorophenol 433 < 433 ¹88-06-2 2,4-Dichlorophenol 433 < 433120-83-2 2,4-Dimethylphenol 433 < 433105-67-9 2,4-Dinitrophenol 853 < 85351-28-5 2,4-Dinitrotoluene 433 < 433121-14-2 2,6-Dichlorophenol 433 < 43387-65-0 2,6-Dinitrotoluene 433 < 433606-20-2 2-Acetylaminofluorene 433 < 43353-96-3 2-Chloronaphthalene 433 < 43391-58-7 2-Chlorophenol 433 < 433 ¹95-57-8 2-Methylnaphthalene 433 < 43391-57-6 2-Methylphenol 433 < 43395-48-7 2-Naphthylamine 853 < 85391-59-8 2-Nitroaniline 433 < 43388-74-4 2-Nitrophenol 433 < 43388-75-5 2-Picoline 433 < 433109-06-8 3&4-Methylphenol 433 < 433 3,3´-Dichlorobenzidine 433 < 43391-94-1 3,3´-Dimethylbenzidine 853 < 853119-93-7 3-Methylcholanthrene 433 < 43356-49-5 3-Nitroaniline 1,270 < 1,27099-09-2 4,6-Dinitro-2-methylphenol 853 < 853 @534-52-1 Report Date: 2/8/2011 Page 7 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001A Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8270D Analytical Results SVOA List by GC/MS Method 8270D/3545A 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/2/2011 1359h 1/27/2011 1700hExtracted: 4-Aminobiphenyl 433 < 43392-67-1 4-Bromophenyl phenyl ether 433 < 433101-55-3 4-Chloro-3-methylphenol 433 < 43359-50-7 4-Chloroaniline 433 < 433106-47-8 4-Chlorophenyl phenyl ether 433 < 4337005-72-3 4-Nitroaniline 1,270 < 1,270100-01-6 4-Nitrophenol 853 < 853100-02-7 5-Nitro-o-toluidine 433 < 43399-55-8 7,12-Dimethylbenz(a)anthracene 433 < 43357-97-6 a,a-Dimethylphenethylamine 853 2,250122-09-8 Acenaphthene 433 < 433 ¹83-32-9 Acenaphthylene 433 < 433208-96-8 Acetophenone 433 < 43398-86-2 alpha-Terpineol 433 < 43398-55-5 Aniline 853 < 85362-53-3 Anthracene 433 < 433120-12-7 Aramite 853 < 853140-57-8 Azobenzene 433 < 433103-33-3 Benz(a)anthracene 433 < 43356-55-3 Benzidine 1,710 < 1,71092-87-5 Benzo(a)pyrene 433 < 43350-32-8 Benzo(b)fluoranthene 433 < 433205-99-2 Benzo(g,h,i)perylene 433 < 433191-24-2 Benzo(k)fluoranthene 433 < 433207-08-9 Benzoic acid 1,270 2,98065-85-0 Benzyl alcohol 433 < 433100-51-6 Bis(2-chloroethoxy)methane 433 < 433111-91-1 Bis(2-chloroethyl) ether 433 < 433111-44-4 Bis(2-chloroisopropyl) ether 433 < 433108-60-1 Bis(2-ethylhexyl) phthalate 433 < 433117-81-7 bis(2-ethylhexyl)adipate 853 2,690103-23-1 Butyl benzyl phthalate 433 < 43385-68-7 Carbazole 433 < 43386-74-8 Report Date: 2/8/2011 Page 8 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001A Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8270D Analytical Results SVOA List by GC/MS Method 8270D/3545A 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/2/2011 1359h 1/27/2011 1700hExtracted: Chlorobenzilate 433 < 433510-15-6 Chrysene 433 < 433218-01-9 Di-n-butyl phthalate 433 < 43384-74-2 Di-n-octyl phthalate 433 < 433117-84-0 Diallate (cis or trans)433 < 4332303-16-4 Dibenz(a,h)anthracene 433 < 43353-70-3 Dibenzofuran 433 < 433132-64-9 Diethyl phthalate 433 < 43384-66-2 Dimethoate 433 < 43360-51-5 Dimethyl phthalate 433 < 433131-11-3 Dimethylaminoazobenzene 433 < 43360-11-7 Dinoseb 853 < 85388-85-7 Diphenylamine 433 < 433122-39-4 Disulfoton 433 < 433298-04-4 Ethyl methanesulfonate 433 < 43362-50-0 Famphur 433 < 43352-85-7 Fluoranthene 433 < 433206-44-0 Fluorene 433 < 43386-73-7 Hexachlorobenzene 433 < 433118-74-1 Hexachlorobutadiene 433 < 43387-68-3 Hexachlorocyclopentadiene 433 < 43377-47-4 Hexachloroethane 433 < 43367-72-1 Hexachlorophene 433 < 43370-30-4 Hexachloropropene 433 < 4331888-71-7 Indene 433 < 43395-13-6 Indeno(1,2,3-cd)pyrene 433 < 433193-39-5 Isodrin 433 < 433465-73-6 Isophorone 433 < 43378-59-1 Isosafrole 433 < 433120-58-1 Kepone 433 < 433143-50-0 Methapyrilene 853 98791-80-5 Methyl methanesulfonate 433 < 43366-27-3 n-Decane 433 1,000124-18-5 Report Date: 2/8/2011 Page 9 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001A Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8270D Analytical Results SVOA List by GC/MS Method 8270D/3545A 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/2/2011 1359h 1/27/2011 1700hExtracted: N-Nitrosodi-n-butylamine 433 < 433924-16-3 N-Nitrosodiethylamine 433 < 43355-18-5 N-Nitrosodimethylamine 853 < 85362-75-9 N-Nitrosodiphenylamine 433 < 43386-30-6 N-Nitrosodi-n-propylamine 433 < 433621-64-7 N-Nitrosomethylethylamine 433 < 43310595-95-6 N-Nitrosomorpholine 433 < 43359-89-2 N-Nitrosopiperidine 433 < 433100-75-4 N-Nitrosopyrrolidine 433 < 433930-55-2 n-Octadecane 433 1,920593-45-3 Naphthalene 433 < 43391-20-3 Nitrobenzene 433 < 43398-95-3 Nitroquinoline-1-oxide 853 < 85356-57-5 O,O,O-Triethyl phosphorothioate 433 < 433126-68-1 o-Toluidine 433 < 43395-53-4 Parathion 433 < 43356-38-2 Methyl parathion 433 < 433298-00-0 Pentachlorobenzene 433 < 433608-93-5 Pentachloronitrobenzene 433 < 43382-68-8 Pentachlorophenol 433 < 43387-86-5 Phenacetin 433 < 43362-44-2 Phenanthrene 433 < 43385-01-8 Phenol 433 < 433 ¹108-95-2 Phorate 433 < 433298-02-2 Pronamide 433 < 43323950-58-5 Pyrene 433 < 433129-00-0 Pyridine 853 < 853110-86-1 Quinoline 433 < 43391-22-5 Safrole 433 < 43394-59-7 Tetraethyl dithiopyrophosphate 433 < 4333689-24-5 Thionazin 433 < 433297-97-2 C11-C12 Aliphatic hydrocarbons 433 8,620 C13-C16 Aliphatic hydrocarbons 433 11,000 Report Date: 2/8/2011 Page 10 of 34 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Lab Sample ID:1101433-001A Client Sample ID:Soil Test Collection Date:1/27/2011 Received Date:1/27/2011 Method:SW8270D Analytical Results SVOA List by GC/MS Method 8270D/3545A 1440h 1632h Analytical ResultCompound Reporting Limit Units:µg/kg-dry Dilution Factor:1 CAS Number Qual Analyzed:2/2/2011 1359h 1/27/2011 1700hExtracted: C17-C21 Aliphatic hydrocarbons 433 24,500 C22-C35 Aliphatic hydrocarbons 433 36,100 C11-C13 Alkyl Naphthalenes 433 < 433 Total C12-C22 PAH**433 < 433 Surr: 2,4,6-Tribromophenol 10-237 121118-79-6 Surr: 2-Fluorobiphenyl 17-179 120321-60-8 Surr: 2-Fluorophenol 10-186 122367-12-4 Surr: Nitrobenzene-d5 10-166 1454165-60-0 Surr: Phenol-d6 10-194 12613127-88-3 Surr: Terphenyl-d14 10-265 1491718-51-0 ¹ - Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. @ - High RPD due to suspected sample non-homogeneity or matrix interference. ** - This value is a summation of the PAH compounds listed above. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 2/8/2011 Page 11 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:LCS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,2,4-Trichlorobenzene5,33397.510-12905,200µg/kg2/2/2011LCS-10514SW8270D1332h 1,4-Dichlorobenzene5,33311010-12905,850µg/kg2/2/2011LCS-10514SW8270D1332h 2,4,6-Trichlorophenol5,33310811-12605,760µg/kg2/2/2011LCS-10514SW8270D1332h 2,4-Dimethylphenol5,33311629-13106,170µg/kg2/2/2011LCS-10514SW8270D1332h 2,4-Dinitrotoluene5,33313210-16907,020µg/kg2/2/2011LCS-10514SW8270D1332h 2-Chloronaphthalene5,33397.023-12605,170µg/kg2/2/2011LCS-10514SW8270D1332h 2-Chlorophenol5,33311310-14106,040µg/kg2/2/2011LCS-10514SW8270D1332h 4,6-Dinitro-2-methylphenol5,33327.610-15301,470µg/kg2/2/2011LCS-10514SW8270D1332h 4-Chloro-3-methylphenol5,33312014-14806,400µg/kg2/2/2011LCS-10514SW8270D1332h 4-Nitrophenol5,33381.810-11404,360µg/kg2/2/2011LCS-10514SW8270D1332h Acenaphthene5,33311210-15005,950µg/kg2/2/2011LCS-10514SW8270D1332h Acenaphthene266.610.310-150 $027.3µg/kg2/1/2011LCS-10514SW8270D0051h Benzo(a)pyrene266.690.038-194 $0240µg/kg2/1/2011LCS-10514SW8270D0051h Benzo(a)pyrene5,33399.638-19405,310µg/kg2/2/2011LCS-10514SW8270D1332h N-Nitrosodi-n-propylamine5,33311725-14806,250µg/kg2/2/2011LCS-10514SW8270D1332h Pentachlorophenol5,33365.110-11203,470µg/kg2/2/2011LCS-10514SW8270D1332h Phenol5,33312910-14706,900µg/kg2/2/2011LCS-10514SW8270D1332h Pyrene5,33311022-16705,850µg/kg2/2/2011LCS-10514SW8270D1332h Pyrene266.679.822-167 $0213µg/kg2/1/2011LCS-10514SW8270D0051h Surr: 2,4,6-Tribromophenol5,33312810-1576,840%REC2/2/2011LCS-10514SW8270D1332h Surr: 2-Fluorobiphenyl2,66711422-1283,040%REC2/2/2011LCS-10514SW8270D1332h Surr: 2-Fluorophenol5,33312710-1356,770%REC2/2/2011LCS-10514SW8270D1332h Surr: Nitrobenzene-d52,66712210-1453,260%REC2/2/2011LCS-10514SW8270D1332h Report Date: 2/8/2011 Page 12 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:LCS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Surr: Phenol-d65,33313810-1577,340%REC2/2/2011LCS-10514SW8270D1332h Surr: Terphenyl-d142,66714022-1673,730%REC2/2/2011LCS-10514SW8270D1332h $ - Samples utilized SIM analysis to achieve required PQLs. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 2/8/2011 Page 13 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1´-Biphenyl-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,2,4,5-Tetrachlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,2,4-Trichlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,2-Dichlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,3,5-Trinitrobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,3-Dichlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,3-Dinitrobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,4-Dichlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1,4-Naphthoquinone-< 670µg/kg2/2/2011MB-10514SW8270D1029h 1,4-Phenylenediamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1-Chloronaphthalene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1-Methylnaphthalene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 1-Methylnaphthalene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h 1-Naphthylamine-< 670µg/kg2/2/2011MB-10514SW8270D1029h 2,3,4,6-Tetrachlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,4,5-Trichlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,4,6-Trichlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,4-Dichlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,4-Dimethylphenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,4-Dinitrophenol-< 670µg/kg2/2/2011MB-10514SW8270D1029h 2,4-Dinitrotoluene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,6-Dichlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2,6-Dinitrotoluene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 14 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 2-Acetylaminofluorene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Chloronaphthalene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Chlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Methylnaphthalene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Methylnaphthalene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h 2-Methylphenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Naphthylamine-< 670µg/kg2/2/2011MB-10514SW8270D1029h 2-Nitroaniline-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Nitrophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 2-Picoline-< 340µg/kg2/2/2011MB-10514SW8270D1029h 3&4-Methylphenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 3,3´-Dichlorobenzidine-< 340µg/kg2/2/2011MB-10514SW8270D1029h 3,3´-Dimethylbenzidine-< 670µg/kg2/2/2011MB-10514SW8270D1029h 3-Methylcholanthrene-< 340µg/kg2/2/2011MB-10514SW8270D1029h 3-Nitroaniline-< 1,000µg/kg2/2/2011MB-10514SW8270D1029h 4,6-Dinitro-2-methylphenol-< 670µg/kg2/2/2011MB-10514SW8270D1029h 4-Aminobiphenyl-< 340µg/kg2/2/2011MB-10514SW8270D1029h 4-Bromophenyl phenyl ether-< 340µg/kg2/2/2011MB-10514SW8270D1029h 4-Chloro-3-methylphenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h 4-Chloroaniline-< 340µg/kg2/2/2011MB-10514SW8270D1029h 4-Chlorophenyl phenyl ether-< 340µg/kg2/2/2011MB-10514SW8270D1029h 4-Nitroaniline-< 1,000µg/kg2/2/2011MB-10514SW8270D1029h 4-Nitrophenol-< 670µg/kg2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 15 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 5-Nitro-o-toluidine-< 340µg/kg2/2/2011MB-10514SW8270D1029h 7,12-Dimethylbenz(a)anthracene-< 340µg/kg2/2/2011MB-10514SW8270D1029h a,a-Dimethylphenethylamine-< 670µg/kg2/2/2011MB-10514SW8270D1029h Acenaphthene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Acenaphthene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Acenaphthylene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Acenaphthylene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Acetophenone-< 340µg/kg2/2/2011MB-10514SW8270D1029h alpha-Terpineol-< 340µg/kg2/2/2011MB-10514SW8270D1029h Aniline-< 670µg/kg2/2/2011MB-10514SW8270D1029h Anthracene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Anthracene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Aramite-< 670µg/kg2/2/2011MB-10514SW8270D1029h Azobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Benz(a)anthracene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Benz(a)anthracene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Benzidine-< 1,340µg/kg2/2/2011MB-10514SW8270D1029h Benzo(a)pyrene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Benzo(a)pyrene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Benzo(b)fluoranthene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Benzo(b)fluoranthene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Benzo(g,h,i)perylene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Benzo(g,h,i)perylene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 16 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Benzo(k)fluoranthene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Benzo(k)fluoranthene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Benzoic acid-< 1,000µg/kg2/2/2011MB-10514SW8270D1029h Benzyl alcohol-< 340µg/kg2/2/2011MB-10514SW8270D1029h Bis(2-chloroethoxy)methane-< 340µg/kg2/2/2011MB-10514SW8270D1029h Bis(2-chloroethyl) ether-< 340µg/kg2/2/2011MB-10514SW8270D1029h Bis(2-chloroisopropyl) ether-< 340µg/kg2/2/2011MB-10514SW8270D1029h Bis(2-ethylhexyl) phthalate-< 340µg/kg2/2/2011MB-10514SW8270D1029h bis(2-ethylhexyl)adipate-< 670µg/kg2/2/2011MB-10514SW8270D1029h Butyl benzyl phthalate-< 340µg/kg2/2/2011MB-10514SW8270D1029h C11-C12 Aliphatic hydrocarbons-< 340µg/kg2/2/2011MB-10514SW8270D1029h C11-C13 Alkyl Naphthalenes-< 340µg/kg2/2/2011MB-10514SW8270D1029h C13-C16 Aliphatic hydrocarbons-< 340µg/kg2/2/2011MB-10514SW8270D1029h C17-C21 Aliphatic hydrocarbons-< 340µg/kg2/2/2011MB-10514SW8270D1029h C22-C35 Aliphatic hydrocarbons-< 340µg/kg2/2/2011MB-10514SW8270D1029h Carbazole-< 340µg/kg2/2/2011MB-10514SW8270D1029h Chlorobenzilate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Chrysene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Chrysene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Diallate (cis or trans)-< 340µg/kg2/2/2011MB-10514SW8270D1029h Dibenz(a,h)anthracene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Dibenz(a,h)anthracene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Dibenzofuran-< 340µg/kg2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 17 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Diethyl phthalate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Dimethoate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Dimethyl phthalate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Dimethylaminoazobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Di-n-butyl phthalate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Di-n-octyl phthalate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Dinoseb-< 670µg/kg2/2/2011MB-10514SW8270D1029h Diphenylamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h Disulfoton-< 340µg/kg2/2/2011MB-10514SW8270D1029h Ethyl methanesulfonate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Famphur-< 340µg/kg2/2/2011MB-10514SW8270D1029h Fluoranthene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Fluoranthene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Fluorene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Fluorene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Hexachlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Hexachlorobutadiene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Hexachlorocyclopentadiene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Hexachloroethane-< 340µg/kg2/2/2011MB-10514SW8270D1029h Hexachlorophene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Hexachloropropene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Indene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Indene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 18 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Indeno(1,2,3-cd)pyrene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Indeno(1,2,3-cd)pyrene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Isodrin-< 340µg/kg2/2/2011MB-10514SW8270D1029h Isophorone-< 340µg/kg2/2/2011MB-10514SW8270D1029h Isosafrole-< 340µg/kg2/2/2011MB-10514SW8270D1029h Kepone-< 340µg/kg2/2/2011MB-10514SW8270D1029h Methapyrilene-< 670µg/kg2/2/2011MB-10514SW8270D1029h Methyl methanesulfonate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Naphthalene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Naphthalene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h n-Decane-< 340µg/kg2/2/2011MB-10514SW8270D1029h Nitrobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Nitroquinoline-1-oxide-< 670µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosodiethylamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosodimethylamine-< 670µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosodi-n-butylamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosodiphenylamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosodi-n-propylamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosomethylethylamine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosomorpholine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosopiperidine-< 340µg/kg2/2/2011MB-10514SW8270D1029h N-Nitrosopyrrolidine-< 340µg/kg2/2/2011MB-10514SW8270D1029h n-Octadecane-< 340µg/kg2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 19 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris O,O,O-Triethyl phosphorothioate-< 340µg/kg2/2/2011MB-10514SW8270D1029h o-Toluidine-< 340µg/kg2/2/2011MB-10514SW8270D1029h Parathion-< 340µg/kg2/2/2011MB-10514SW8270D1029h Methyl parathion-< 340µg/kg2/2/2011MB-10514SW8270D1029h Pentachlorobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Pentachloronitrobenzene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Pentachlorophenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h Phenacetin-< 340µg/kg2/2/2011MB-10514SW8270D1029h Phenanthrene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Phenanthrene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Phenol-< 340µg/kg2/2/2011MB-10514SW8270D1029h Phorate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Pronamide-< 340µg/kg2/2/2011MB-10514SW8270D1029h Pyrene-$< 10.0µg/kg2/1/2011MB-10514SW8270D1428h Pyrene-< 340µg/kg2/2/2011MB-10514SW8270D1029h Pyridine-< 670µg/kg2/2/2011MB-10514SW8270D1029h Quinoline-< 340µg/kg2/2/2011MB-10514SW8270D1029h Safrole-< 340µg/kg2/2/2011MB-10514SW8270D1029h Tetraethyl dithiopyrophosphate-< 340µg/kg2/2/2011MB-10514SW8270D1029h Thionazin-< 340µg/kg2/2/2011MB-10514SW8270D1029h Total C12-C22 PAH**-< 340µg/kg2/2/2011MB-10514SW8270D1029h Surr: 2,4,6-Tribromophenol5,33395.610-1185,100%REC2/2/2011MB-10514SW8270D1029h Surr: 2-Fluorobiphenyl2,66710522-1282,800%REC2/2/2011MB-10514SW8270D1029h Report Date: 2/8/2011 Page 20 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Surr: 2-Fluorophenol5,33310910-1115,820%REC2/2/2011MB-10514SW8270D1029h Surr: Nitrobenzene-d52,66712810-1453,410%REC2/2/2011MB-10514SW8270D1029h Surr: Phenol-d65,33311110-1575,930%REC2/2/2011MB-10514SW8270D1029h Surr: Terphenyl-d142,66713522-1673,590%REC2/2/2011MB-10514SW8270D1029h $ - Samples utilized SIM analysis to achieve required PQLs. ** - This value is a summation of the PAH compounds listed above. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 2/8/2011 Page 21 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,2,4-Trichlorobenzene6,78694.710-10706,420µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 1,4-Dichlorobenzene6,78610410-90 ¹07,070µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 2,4,6-Trichlorophenol6,78612626-12808,580µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 2,4-Dimethylphenol6,78611810-17607,990µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 2,4-Dinitrotoluene6,78613010-19108,840µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 2-Chloronaphthalene6,78612310-13208,340µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 2-Chlorophenol6,78611310-107 ¹07,690µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 4,6-Dinitro-2-methylphenol6,78657.210-25003,880µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 4-Chloro-3-methylphenol6,78612610-13608,560µg/kg-dry2/2/20111101433-001AMSSW8270D1426h 4-Nitrophenol6,78611810-13508,010µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Acenaphthene6,78611931-113 ¹19.518,110µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Acenaphthene339.33.2531-113 $¹19.5130.5µg/kg-dry2/1/20111101433-001AMSSW8270D0143h Benzo(a)pyrene6,78687.938-169101.86,060µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Benzo(a)pyrene339.372.838-169 $101.8349µg/kg-dry2/1/20111101433-001AMSSW8270D0143h N-Nitrosodi-n-propylamine6,78612010-13308,150µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Pentachlorophenol6,78683.720-13105,680µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Phenol6,78613210-71 ¹08,960µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Pyrene339.356.531-150 $106.9299µg/kg-dry2/1/20111101433-001AMSSW8270D0143h Pyrene6,78611731-150106.98,070µg/kg-dry2/2/20111101433-001AMSSW8270D1426h Surr: 2,4,6-Tribromophenol6,78613510-2379,140%REC2/2/20111101433-001AMSSW8270D1426h Surr: 2-Fluorobiphenyl3,39411317-1793,830%REC2/2/20111101433-001AMSSW8270D1426h Surr: 2-Fluorophenol6,78612410-1868,390%REC2/2/20111101433-001AMSSW8270D1426h Surr: Nitrobenzene-d53,39411310-1663,840%REC2/2/20111101433-001AMSSW8270D1426h Report Date: 2/8/2011 Page 22 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Surr: Phenol-d66,78613210-1948,930%REC2/2/20111101433-001AMSSW8270D1426h Surr: Terphenyl-d143,39415010-2655,080%REC2/2/20111101433-001AMSSW8270D1426h $ - Samples utilized SIM analysis to achieve required PQLs. ¹ - Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 2/8/2011 Page 23 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MSD AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,2,4-Trichlorobenzene6,78695.910-107 3501.336,510µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 1,4-Dichlorobenzene6,78610910-90 35¹0 4.137,360µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 2,4,6-Trichlorophenol6,78613026-128 35¹0 2.938,830µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 2,4-Dimethylphenol6,78611810-176 3500.6358,040µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 2,4-Dinitrotoluene6,78613710-191 3504.989,290µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 2-Chloronaphthalene6,78612610-132 3502.398,540µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 2-Chlorophenol6,78611610-107 35¹0 2.147,860µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 4,6-Dinitro-2-methylphenol6,78636.710-250 35@043.52,490µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 4-Chloro-3-methylphenol6,78612610-136 3500.1398,550µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h 4-Nitrophenol6,78611710-135 3501.327,910µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Acenaphthene339.34.2531-113 35$¹19.51 10.533.9µg/kg-dry2/1/20111101433-001AMSDSW8270D0210h Acenaphthene6,78611931-113 35¹19.51 0.2098,130µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Benzo(a)pyrene6,78691.038-169 35101.8 3.496,280µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Benzo(a)pyrene339.383.038-169 35$101.8 9.50383µg/kg-dry2/1/20111101433-001AMSDSW8270D0210h N-Nitrosodi-n-propylamine6,78612410-133 3503.398,430µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Pentachlorophenol6,78686.120-131 3502.835,840µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Phenol6,78613610-71 35¹0 2.559,200µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Pyrene339.367.531-150 35$106.9 11.8336µg/kg-dry2/1/20111101433-001AMSDSW8270D0210h Pyrene6,78611831-150 35106.9 0.8588,140µg/kg-dry2/2/20111101433-001AMSDSW8270D1522h Surr: 2,4,6-Tribromophenol6,78613210-237 08,940%REC2/2/20111101433-001AMSDSW8270D1522h Surr: 2-Fluorobiphenyl3,39411417-179 03,870%REC2/2/20111101433-001AMSDSW8270D1522h Surr: 2-Fluorophenol6,78612710-186 08,650%REC2/2/20111101433-001AMSDSW8270D1522h Surr: Nitrobenzene-d53,39411710-166 03,950%REC2/2/20111101433-001AMSDSW8270D1522h Report Date: 2/8/2011 Page 24 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSSV QC Type:MSD AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Surr: Phenol-d66,78613210-194 08,950%REC2/2/20111101433-001AMSDSW8270D1522h Surr: Terphenyl-d143,39415010-265 05,090%REC2/2/20111101433-001AMSDSW8270D1522h $ - Samples utilized SIM analysis to achieve required PQLs. @ - High RPD due to suspected sample non-homogeneity or matrix interference. ¹ - Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample. Report Date: 2/8/2011 Page 25 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:LCS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1-Trichloroethane1,00087.064-1440870µg/kg1/28/2011LCS-10536SW8260C1623h 1,1-Dichloroethene1,00061.936-1840618µg/kg1/28/2011LCS-10536SW8260C1623h 1,2-Dichlorobenzene1,00097.670-1340976µg/kg1/28/2011LCS-10536SW8260C1623h 1,2-Dichloroethane1,00085.455-1460854µg/kg1/28/2011LCS-10536SW8260C1623h 1,2-Dichloropropane1,00073.956-1330738µg/kg1/28/2011LCS-10536SW8260C1623h Benzene1,00083.160-1300831µg/kg1/28/2011LCS-10536SW8260C1623h Chlorobenzene1,00096.075-1300960µg/kg1/28/2011LCS-10536SW8260C1623h Chloroform1,00087.961-1300879µg/kg1/28/2011LCS-10536SW8260C1623h Ethylbenzene1,00090.769-1470906µg/kg1/28/2011LCS-10536SW8260C1623h Isopropylbenzene1,00091.265-1470912µg/kg1/28/2011LCS-10536SW8260C1623h Methyl tert-butyl ether1,00064.233.1-1390642µg/kg1/28/2011LCS-10536SW8260C1623h Methylene chloride1,00011739-16401,170µg/kg1/28/2011LCS-10536SW8260C1623h Naphthalene1,00076.240-1310762µg/kg1/28/2011LCS-10536SW8260C1623h Tetrahydrofuran1,00054.843-1460548µg/kg1/28/2011LCS-10536SW8260C1623h Toluene1,00087.161-1400870µg/kg1/28/2011LCS-10536SW8260C1623h Trichloroethene1,00081.651-1540816µg/kg1/28/2011LCS-10536SW8260C1623h Xylenes, Total3,00089.672-14702,690µg/kg1/28/2011LCS-10536SW8260C1623h Surr: 1,2-Dichloroethane-d42,50010073-1322,510%REC1/28/2011LCS-10536SW8260C1623h Surr: 4-Bromofluorobenzene2,50096.185-1152,400%REC1/28/2011LCS-10536SW8260C1623h Surr: Dibromofluoromethane2,50010584-1212,640%REC1/28/2011LCS-10536SW8260C1623h Surr: Toluene-d82,50097.385-1152,430%REC1/28/2011LCS-10536SW8260C1623h Report Date: 2/8/2011 Page 26 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1,2-Tetrachloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1,1-Trichloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1,2,2-Tetrachloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1,2-Trichloro-1,2,2- trifluoroethane -< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1,2-Trichloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1-Dichloropropene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1-Dichloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,1-Dichloroethene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2,3-Trichlorobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2,3-Trichloropropane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2,3-Trimethylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2,4-Trichlorobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2,4-Trimethylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2-Dibromo-3-chloropropane-< 250µg/kg1/28/2011MB-10536SW8260C1645h 1,2-Dibromoethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2-Dichlorobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2-Dichloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,2-Dichloropropane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,3,5-Trimethylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,3-Dichlorobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,3-Dichloropropane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 1,4-Dichlorobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Report Date: 2/8/2011 Page 27 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,4-Dioxane-< 2,500µg/kg1/28/2011MB-10536SW8260C1645h 2,2-Dichloropropane-< 100µg/kg1/28/2011MB-10536SW8260C1645h 2-Butanone-< 500µg/kg1/28/2011MB-10536SW8260C1645h 2-Chloroethyl vinyl ether-< 250µg/kg1/28/2011MB-10536SW8260C1645h 2-Chlorotoluene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 2-Hexanone-< 250µg/kg1/28/2011MB-10536SW8260C1645h 2-Nitropropane-< 250µg/kg1/28/2011MB-10536SW8260C1645h 4-Chlorotoluene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 4-Isopropyltoluene-< 100µg/kg1/28/2011MB-10536SW8260C1645h 4-Methyl-2-pentanone-< 250µg/kg1/28/2011MB-10536SW8260C1645h Acetone-< 500µg/kg1/28/2011MB-10536SW8260C1645h Acetonitrile-< 250µg/kg1/28/2011MB-10536SW8260C1645h Acrolein-< 250µg/kg1/28/2011MB-10536SW8260C1645h Acrylonitrile-< 500µg/kg1/28/2011MB-10536SW8260C1645h Allyl chloride-< 250µg/kg1/28/2011MB-10536SW8260C1645h Benzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Benzyl chloride-< 250µg/kg1/28/2011MB-10536SW8260C1645h Bis(2-chloroisopropyl) ether-< 250µg/kg1/28/2011MB-10536SW8260C1645h Bromobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Bromochloromethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Bromodichloromethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Bromoform-< 100µg/kg1/28/2011MB-10536SW8260C1645h Bromomethane-< 250µg/kg1/28/2011MB-10536SW8260C1645h Report Date: 2/8/2011 Page 28 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Butyl acetate-< 500µg/kg1/28/2011MB-10536SW8260C1645h C11&C12 Aliphatic hydrocarbons-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h C6 Aliphatic hydrocarbons-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h C7&C8 Aliphatic hydrocarbons-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h C9&C10 Aliphatic hydrocarbons-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h C9&C10 Alkyl Benzenes-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h Carbon disulfide-< 100µg/kg1/28/2011MB-10536SW8260C1645h Carbon tetrachloride-< 100µg/kg1/28/2011MB-10536SW8260C1645h Chlorobenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Chloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Chloroform-< 100µg/kg1/28/2011MB-10536SW8260C1645h Chloromethane-< 250µg/kg1/28/2011MB-10536SW8260C1645h Chloroprene-< 100µg/kg1/28/2011MB-10536SW8260C1645h cis-1,2-Dichloroethene-< 100µg/kg1/28/2011MB-10536SW8260C1645h cis-1,3-Dichloropropene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Cyclohexane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Cyclohexanone-< 2,500µg/kg1/28/2011MB-10536SW8260C1645h Dibromochloromethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Dibromomethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Dichlorodifluoromethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Ethyl acetate-< 500µg/kg1/28/2011MB-10536SW8260C1645h Ethyl ether-< 500µg/kg1/28/2011MB-10536SW8260C1645h Ethyl methacrylate-< 100µg/kg1/28/2011MB-10536SW8260C1645h Report Date: 2/8/2011 Page 29 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Ethylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Hexachlorobutadiene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Iodomethane-< 250µg/kg1/28/2011MB-10536SW8260C1645h Isobutyl alcohol-< 5,000µg/kg1/28/2011MB-10536SW8260C1645h Isopropyl acetate-< 500µg/kg1/28/2011MB-10536SW8260C1645h Isopropyl alcohol-< 2,000µg/kg1/28/2011MB-10536SW8260C1645h Isopropylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Isopropyltoluene-< 100µg/kg1/28/2011MB-10536SW8260C1645h m,p-Xylene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Methacrylonitrile-< 250µg/kg1/28/2011MB-10536SW8260C1645h Methyl Acetate-< 250µg/kg1/28/2011MB-10536SW8260C1645h Methyl methacrylate-< 250µg/kg1/28/2011MB-10536SW8260C1645h Methyl tert-butyl ether-< 100µg/kg1/28/2011MB-10536SW8260C1645h Methylcyclohexane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Methylene chloride-< 250µg/kg1/28/2011MB-10536SW8260C1645h n-Amyl acetate-< 500µg/kg1/28/2011MB-10536SW8260C1645h Naphthalene-< 100µg/kg1/28/2011MB-10536SW8260C1645h n-Butyl alcohol-< 5,000µg/kg1/28/2011MB-10536SW8260C1645h n-Butylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h n-Hexane-< 100µg/kg1/28/2011MB-10536SW8260C1645h n-Octane-< 100µg/kg1/28/2011MB-10536SW8260C1645h n-Propylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h o-Xylene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Report Date: 2/8/2011 Page 30 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Pentachloroethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Propionitrile-< 1,250µg/kg1/28/2011MB-10536SW8260C1645h Propyl acetate-< 500µg/kg1/28/2011MB-10536SW8260C1645h sec-Butylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Styrene-< 100µg/kg1/28/2011MB-10536SW8260C1645h tert-Butyl alcohol-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h tert-Butylbenzene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Tetrachloroethene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Tetrahydrofuran-< 100µg/kg1/28/2011MB-10536SW8260C1645h Toluene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Total Purgable Petroleum Hydrocarbons (C6-C15) -< 1,000µg/kg1/28/2011MB-10536SW8260C1645h TPH C11-C15 (DRO)-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h TPH C6-C10 (GRO)-< 1,000µg/kg1/28/2011MB-10536SW8260C1645h trans-1,2-Dichloroethene-< 100µg/kg1/28/2011MB-10536SW8260C1645h trans-1,3-Dichloropropene-< 100µg/kg1/28/2011MB-10536SW8260C1645h trans-1,4-Dichloro-2-butene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Trichloroethene-< 100µg/kg1/28/2011MB-10536SW8260C1645h Trichlorofluoromethane-< 100µg/kg1/28/2011MB-10536SW8260C1645h Vinyl acetate-< 500µg/kg1/28/2011MB-10536SW8260C1645h Vinyl chloride-< 50.0µg/kg1/28/2011MB-10536SW8260C1645h Xylenes, Total-< 100µg/kg1/28/2011MB-10536SW8260C1645h Surr: 1,2-Dichloroethane-d42,50011173-1322,780%REC1/28/2011MB-10536SW8260C1645h Report Date: 2/8/2011 Page 31 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MBLK AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris Surr: 4-Bromofluorobenzene2,50096.185-1152,400%REC1/28/2011MB-10536SW8260C1645h Surr: Dibromofluoromethane2,50011384-1212,830%REC1/28/2011MB-10536SW8260C1645h Surr: Toluene-d82,50098.585-1152,460%REC1/28/2011MB-10536SW8260C1645h Report Date: 2/8/2011 Page 32 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MS AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1-Trichloroethane1,27271.720-1440912µg/kg-dry1/28/20111101433-001BMSSW8260C1941h 1,1-Dichloroethene1,27260.024-1740763µg/kg-dry1/28/20111101433-001BMSSW8260C1941h 1,2-Dichlorobenzene1,27288.910-14801,130µg/kg-dry1/28/20111101433-001BMSSW8260C1941h 1,2-Dichloroethane1,27282.354-13301,050µg/kg-dry1/28/20111101433-001BMSSW8260C1941h 1,2-Dichloropropane1,27248.428-1400616µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Benzene1,27269.917-1380889µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Chlorobenzene1,27284.313-15001,070µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Chloroform1,27286.421-14701,100µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Ethylbenzene1,27279.510-16401,010µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Isopropylbenzene1,27281.426-14601,040µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Methyl tert-butyl ether1,27235.528-1370452µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Methylene chloride1,27286.710-21701,100µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Naphthalene1,27211713-15601,490µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Tetrahydrofuran1,27243.410-1360552µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Toluene1,27274.623-1680949µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Trichloroethene1,27259.014-1610751µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Xylenes, Total3,81778.010-16002,980µg/kg-dry1/28/20111101433-001BMSSW8260C1941h Surr: 1,2-Dichloroethane-d43,18110168-1473,200%REC1/28/20111101433-001BMSSW8260C1941h Surr: 4-Bromofluorobenzene3,18195.971-1443,050%REC1/28/20111101433-001BMSSW8260C1941h Surr: Dibromofluoromethane3,18111571-1293,660%REC1/28/20111101433-001BMSSW8260C1941h Surr: Toluene-d83,18196.572-1293,070%REC1/28/20111101433-001BMSSW8260C1941h Report Date: 2/8/2011 Page 33 of 34 463 West 3600 South AMERICAN WEST ANALYTICAL LABORATORIES Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QA Officer Jose Rocha Kyle F. Gross Laboratory Director All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science. Project:Red Butte Creek - Hayes Property Client:Utah DEQ DERR Lab Set ID:1101433 QC SUMMARY REPORT Dept:MSVOA QC Type:MSD AnalyteResult Amount Spiked Original Amount %REC%RPDLimits RPD Limit QualUnitsDate AnalyzedSample IDMethod Contact:Jim Harris 1,1,1-Trichloroethane1,27276.920-144 3506.93978µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h 1,1-Dichloroethene1,27252.224-174 35013.9664µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h 1,2-Dichlorobenzene1,27287.110-148 3502.051,110µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h 1,2-Dichloroethane1,27280.054-133 3502.901,020µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h 1,2-Dichloropropane1,27275.628-140 35@043.9962µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Benzene1,27275.317-138 3507.51958µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Chlorobenzene1,27283.213-150 3501.311,060µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Chloroform1,27276.821-147 35011.8977µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Ethylbenzene1,27277.810-164 3502.10990µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Isopropylbenzene1,27280.226-146 3501.491,020µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Methyl tert-butyl ether1,27261.228-137 35@053.2779µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Methylene chloride1,27278.510-217 3509.99998µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Naphthalene1,27211313-156 3503.551,440µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Tetrahydrofuran1,27248.810-136 35011.7621µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Toluene1,27274.823-168 3500.268952µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Trichloroethene1,27272.714-161 35020.7924µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Xylenes, Total3,81776.210-160 3502.272,910µg/kg-dry1/28/20111101433-001BMSDSW8260C2003h Surr: 1,2-Dichloroethane-d43,18198.168-147 03,120%REC1/28/20111101433-001BMSDSW8260C2003h Surr: 4-Bromofluorobenzene3,18197.371-144 03,090%REC1/28/20111101433-001BMSDSW8260C2003h Surr: Dibromofluoromethane3,18110271-129 03,230%REC1/28/20111101433-001BMSDSW8260C2003h Surr: Toluene-d83,18198.072-129 03,120%REC1/28/20111101433-001BMSDSW8260C2003h @ - High RPD due to suspected sample non-homogeneity or matrix interference. Report Date: 2/8/2011 Page 34 of 34