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HomeMy WebLinkAboutDDW-2025-001903February 20, 2025 Dear John Steffan: Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 2/12/25 9:10 am and logged in under work order IB02031. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH06021RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 2 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 3 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IB02031-01 Name: Sampled: Received: 02/12/25 09:10 02/11/25 10:16 TP001-GAC TREATENT - 04, 05 06 Reg ID:Drinking Water - Regular SampleMatrix:UTAH06021 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 1.0 ng/L EPA 533PFBA02/17/25 17:04 PSBU2.011.0 < 0.4 ng/L EPA 533PFMPA02/17/25 17:04 PSBU2.010.4 < 0.5 ng/L EPA 533PFPeA02/17/25 17:04 PSBU2.010.5 < 0.5 ng/L EPA 533PFBS02/17/25 17:04 PSBU2.010.5 < 0.4 ng/L EPA 533PFMBA02/17/25 17:04 PSBU2.010.4 < 0.5 ng/L EPA 533PFEESA02/17/25 17:04 PSBU2.010.5 < 0.4 ng/L EPA 533HFPO-DA 02/17/25 17:04 PSBU2.010.4 < 0.5 ng/L EPA 533NFDHA02/17/25 17:04 PSBU2.010.5 < 0.4 ng/L EPA 5334:2 FTS 02/17/25 17:04 PSBU2.010.4 0.9 ng/L EPA 533PFHxS02/17/25 17:04 PSBJ2.010.4 < 0.6 ng/L EPA 533PFHpA02/17/25 17:04 PSBU2.010.6 < 0.5 ng/L EPA 533PFHxA02/17/25 17:04 PSBU2.010.5 < 0.5 ng/L EPA 533ADONA02/17/25 17:04 PSBU2.010.5 < 0.6 ng/L EPA 533PFPeS02/17/25 17:04 PSBU2.010.6 < 0.5 ng/L EPA 5336:2 FTS 02/17/25 17:04 PSBU2.010.5 < 0.7 ng/L EPA 533PFOA02/17/25 17:04 PSBU2.010.7 < 0.6 ng/L EPA 533PFHpS02/17/25 17:04 PSBU2.010.6 < 0.5 ng/L EPA 533PFOS02/17/25 17:04 PSBU2.010.5 < 0.5 ng/L EPA 533PFNA02/17/25 17:04 PSBU2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 02/17/25 17:04 PSBU2.010.7 < 0.5 ng/L EPA 5338:2 FTS 02/17/25 17:04 PSBU2.010.5 < 0.5 ng/L EPA 533PFDA02/17/25 17:04 PSBU2.010.5 < 0.5 ng/L EPA 533PFUnA02/17/25 17:04 PSBU2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 02/17/25 17:04 PSBU2.010.6 < 0.5 ng/L EPA 533PFDoA02/17/25 17:04 PSBU2.010.5 Surrogate: 13C4-PFBA-SURR 89 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C5-PFPeA-SURR 99 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C3-PFBS-SURR 94 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C2-4:2FTS-SURR 90 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C5-PFHxA-SURR 96 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 93 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C4-PFHpA-SURR 95 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C3-PFHxS-SURR 91 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C2-6:2FTS-SURR 87 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C8-PFOA-SURR 90 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C9-PFNA-SURR 89 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C8-PFOS-SURR 89 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C2-8:2FTS-SURR 95 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C6-PFDA-SURR 88 %50-200 02/17/25 17:04 PSB EPA 533 Surrogate: 13C7-PFUnA-SURR 87 %50-200 02/17/25 17:04 PSB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 4 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: IB02031-01 Name: Sampled: Received: 02/12/25 09:10 02/11/25 10:16 TP001-GAC TREATENT - 04, 05 06 Reg ID:Drinking Water - Regular SampleMatrix:UTAH06021 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 89 %50-200 02/17/25 17:04 PSB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B524965 - EPA 533 - EPA 533 Blank (B524965-BLK1)Prepared: 02/13/25 Analyzed: 02/17/25 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA 0.4 ng/L J NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 0.5 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.5 ng/L U Surrogate: 13C4-PFBA-SURR 29.4 ng/L 40.00 74 50-200 Surrogate: 13C5-PFPeA-SURR 30.5 ng/L 40.00 76 50-200 Surrogate: 13C3-PFBS-SURR 33.6 ng/L 37.28 90 50-200 Surrogate: 13C2-4:2FTS-SURR 132 ng/L 150.4 88 50-200 Surrogate: 13C5-PFHxA-SURR 29.4 ng/L 40.00 73 50-200 Surrogate: 13C3-HFPOA-DA-SURR 27.7 ng/L 40.00 69 50-200 Surrogate: 13C4-PFHpA-SURR 29.4 ng/L 40.00 73 50-200 Surrogate: 13C3-PFHxS-SURR 33.5 ng/L 37.92 88 50-200 Surrogate: 13C2-6:2FTS-SURR 129 ng/L 152.0 85 50-200 Surrogate: 13C8-PFOA-SURR 29.9 ng/L 40.00 75 50-200 Surrogate: 13C9-PFNA-SURR 30.2 ng/L 40.00 76 50-200 Surrogate: 13C8-PFOS-SURR 34.4 ng/L 38.32 90 50-200 Surrogate: 13C2-8:2FTS-SURR 142 ng/L 153.6 93 50-200 Surrogate: 13C6-PFDA-SURR 29.0 ng/L 40.00 72 50-200 Surrogate: 13C7-PFUnA-SURR 26.1 ng/L 40.00 65 50-200 Surrogate: 13C2-PFDoA-SURR 30.1 ng/L 40.00 75 50-200 LCS (B524965-BS1)Prepared: 02/13/25 Analyzed: 02/17/25 PFBA 83 ng/L 80.00 104 70-130 PFMPA 86 ng/L 80.00 108 70-130 www.pacelabs.comCustomer #: 72-106174 Page 6 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B524965-BS1)Prepared: 02/13/25 Analyzed: 02/17/25 PFPeA 77 ng/L 80.00 96 70-130 PFBS 78 ng/L 80.00 98 70-130 PFMBA 76 ng/L 80.00 95 70-130 PFEESA 77 ng/L 80.00 96 70-130 HFPO-DA 72 ng/L 80.00 90 70-130 NFDHA 70 ng/L 80.00 87 70-130 PFHxS 60 ng/L 80.00 75 70-130 4:2 FTS 87 ng/L 80.00 109 70-130 PFHpA 74 ng/L 80.00 93 70-130 PFHxA 76 ng/L 80.00 95 70-130 ADONA 77 ng/L 80.00 96 70-130 PFPeS 82 ng/L 80.00 103 70-130 6:2 FTS 84 ng/L 80.00 105 70-130 PFOA 89 ng/L 80.00 111 70-130 PFHpS 86 ng/L 80.00 107 70-130 PFOS 75 ng/L 80.00 94 70-130 PFNA 87 ng/L 80.00 109 70-130 9Cl-PF3ONS 84 ng/L 80.00 105 70-130 8:2 FTS 86 ng/L 80.00 108 70-130 PFDA 72 ng/L 80.00 90 70-130 PFUnA 77 ng/L 80.00 97 70-130 11Cl-PF3OUdS 85 ng/L 80.00 107 70-130 PFDoA 70 ng/L 80.00 88 70-130 Surrogate: 13C4-PFBA-SURR 32.5 ng/L 40.00 81 50-200 Surrogate: 13C5-PFPeA-SURR 34.7 ng/L 40.00 87 50-200 Surrogate: 13C3-PFBS-SURR 33.9 ng/L 37.28 91 50-200 Surrogate: 13C2-4:2FTS-SURR 142 ng/L 150.4 95 50-200 Surrogate: 13C5-PFHxA-SURR 33.1 ng/L 40.00 83 50-200 Surrogate: 13C3-HFPOA-DA-SURR 32.7 ng/L 40.00 82 50-200 Surrogate: 13C4-PFHpA-SURR 32.7 ng/L 40.00 82 50-200 Surrogate: 13C3-PFHxS-SURR 35.5 ng/L 37.92 94 50-200 Surrogate: 13C2-6:2FTS-SURR 138 ng/L 152.0 91 50-200 Surrogate: 13C8-PFOA-SURR 31.3 ng/L 40.00 78 50-200 Surrogate: 13C9-PFNA-SURR 29.9 ng/L 40.00 75 50-200 Surrogate: 13C8-PFOS-SURR 33.7 ng/L 38.32 88 50-200 Surrogate: 13C2-8:2FTS-SURR 141 ng/L 153.6 92 50-200 Surrogate: 13C6-PFDA-SURR 27.5 ng/L 40.00 69 50-200 Surrogate: 13C7-PFUnA-SURR 26.0 ng/L 40.00 65 50-200 Surrogate: 13C2-PFDoA-SURR 28.3 ng/L 40.00 71 50-200 Duplicate (B524965-DUP1)Sample: IB02030-01 Prepared: 02/13/25 Analyzed: 02/17/25 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L 0.8 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 7 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B524965-DUP1)Sample: IB02030-01 Prepared: 02/13/25 Analyzed: 02/17/25 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L 0.6 30U PFHxA < 0.5 ng/L 0.7 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA 0.8 ng/L 1 47 30J PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L 0.9 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L 0.5 30U PFUnA < 0.5 ng/L 0.5 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 31.7 ng/L 40.05 79 50-200 Surrogate: 13C5-PFPeA-SURR 33.2 ng/L 40.05 83 50-200 Surrogate: 13C3-PFBS-SURR 34.0 ng/L 37.32 91 50-200 Surrogate: 13C2-4:2FTS-SURR 134 ng/L 150.6 89 50-200 Surrogate: 13C5-PFHxA-SURR 33.4 ng/L 40.05 83 50-200 Surrogate: 13C3-HFPOA-DA-SURR 32.6 ng/L 40.05 81 50-200 Surrogate: 13C4-PFHpA-SURR 34.2 ng/L 40.05 85 50-200 Surrogate: 13C3-PFHxS-SURR 34.3 ng/L 37.97 90 50-200 Surrogate: 13C2-6:2FTS-SURR 130 ng/L 152.2 85 50-200 Surrogate: 13C8-PFOA-SURR 33.9 ng/L 40.05 85 50-200 Surrogate: 13C9-PFNA-SURR 33.6 ng/L 40.05 84 50-200 Surrogate: 13C8-PFOS-SURR 34.1 ng/L 38.37 89 50-200 Surrogate: 13C2-8:2FTS-SURR 143 ng/L 153.8 93 50-200 Surrogate: 13C6-PFDA-SURR 33.4 ng/L 40.05 83 50-200 Surrogate: 13C7-PFUnA-SURR 31.5 ng/L 40.05 79 50-200 Surrogate: 13C2-PFDoA-SURR 34.6 ng/L 40.05 87 50-200 Matrix Spike (B524965-MS1)Sample: IB02030-02 Prepared: 02/13/25 Analyzed: 02/17/25 PFBA 105 ng/L 100.4 ND 104 70-130 PFMPA 107 ng/L 100.4 ND 107 70-130 PFPeA 97 ng/L 100.4 ND 96 70-130 PFBS 99 ng/L 100.4 ND 98 70-130 PFMBA 95 ng/L 100.4 ND 94 70-130 PFEESA 97 ng/L 100.4 ND 97 70-130 NFDHA 86 ng/L 100.4 ND 86 70-130 HFPO-DA 91 ng/L 100.4 0.9 90 70-130 PFHxS 80 ng/L 100.4 ND 80 70-130 4:2 FTS 112 ng/L 100.4 ND 112 70-130 PFHpA 95 ng/L 100.4 ND 94 70-130 PFHxA 97 ng/L 100.4 ND 97 70-130 www.pacelabs.comCustomer #: 72-106174 Page 8 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B524965-MS1)Sample: IB02030-02 Prepared: 02/13/25 Analyzed: 02/17/25 ADONA 92 ng/L 100.4 ND 92 70-130 PFPeS 105 ng/L 100.4 ND 104 70-130 6:2 FTS 103 ng/L 100.4 ND 103 70-130 PFOA 114 ng/L 100.4 ND 113 70-130 PFHpS 111 ng/L 100.4 ND 110 70-130 PFOS 96 ng/L 100.4 ND 96 70-130 PFNA 111 ng/L 100.4 ND 111 70-130 9Cl-PF3ONS 107 ng/L 100.4 ND 107 70-130 8:2 FTS 111 ng/L 100.4 ND 111 70-130 PFDA 90 ng/L 100.4 ND 90 70-130 PFUnA 95 ng/L 100.4 ND 94 70-130 11Cl-PF3OUdS 107 ng/L 100.4 ND 106 70-130 PFDoA 89 ng/L 100.4 ND 89 70-130 Surrogate: 13C4-PFBA-SURR 38.5 ng/L 50.20 77 50-200 Surrogate: 13C5-PFPeA-SURR 41.2 ng/L 50.20 82 50-200 Surrogate: 13C3-PFBS-SURR 43.0 ng/L 46.79 92 50-200 Surrogate: 13C2-4:2FTS-SURR 178 ng/L 188.8 94 50-200 Surrogate: 13C5-PFHxA-SURR 39.9 ng/L 50.20 79 50-200 Surrogate: 13C3-HFPOA-DA-SURR 39.5 ng/L 50.20 79 50-200 Surrogate: 13C4-PFHpA-SURR 39.8 ng/L 50.20 79 50-200 Surrogate: 13C3-PFHxS-SURR 44.3 ng/L 47.59 93 50-200 Surrogate: 13C2-6:2FTS-SURR 175 ng/L 190.8 92 50-200 Surrogate: 13C8-PFOA-SURR 37.2 ng/L 50.20 74 50-200 Surrogate: 13C9-PFNA-SURR 37.2 ng/L 50.20 74 50-200 Surrogate: 13C8-PFOS-SURR 42.1 ng/L 48.09 87 50-200 Surrogate: 13C2-8:2FTS-SURR 173 ng/L 192.8 90 50-200 Surrogate: 13C6-PFDA-SURR 35.9 ng/L 50.20 72 50-200 Surrogate: 13C7-PFUnA-SURR 36.3 ng/L 50.20 72 50-200 Surrogate: 13C2-PFDoA-SURR 40.0 ng/L 50.20 80 50-200 www.pacelabs.comCustomer #: 72-106174 Page 9 of 13 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 10 of 13 Page 11 of 13 Page 12 of 13 Page 13 of 13