DERR-2025-001090

SITE CHARACTIZATION REPORT
Paxton Development
203 to 225 West Paxton Avenue
Salt Lake City, Utah
Voluntary Cleanup Site #C-129
Prepared for
Paxton Project, LLC
2630 Canyon Road
Springville, Utah
Prepared by
Geosyntec Consultants, Inc.
215 South State Street
Salt Lake City, Utah 84111
Project SLC1091
December 2024 (updated January 30, 2025)

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TABLE OF CONTENTS
ACRONYMS AND ABBREVIATIONS ...................................................................................III
1. INTRODUCTION .................................................................................................................1
1.1 Site Location and Description ......................................................................................1
1.2 Site Background ...........................................................................................................1
1.3 Previous Investigations Summary ................................................................................1
1.4 Environmental Setting ..................................................................................................3
1.5 Geology and Hydrogeology .........................................................................................3
1.6 Investigation Objectives, Scope and Rational ..............................................................4
2. SAMPLING COLLETION PROCEDURES ........................................................................5
2.1 Soil Sampling ...............................................................................................................5
2.2 Groundwater Sampling .................................................................................................5
2.3 Soil Gas Sampling ........................................................................................................5
2.4 Laboratory Analytical Methods ....................................................................................6
2.5 Quality Control Sampling ............................................................................................6
2.6 Sample Handling and Custody .....................................................................................6
2.6.2 Sample Packaging ............................................................................................7
2.6.3 Chain of Custody ..............................................................................................7
2.7 Decontamination ..........................................................................................................7
2.8 Investigation Derived Waste Management ..................................................................7
2.9 Screening Levels ..........................................................................................................7
3. INVESTIGATION FINDINGS .............................................................................................8
3.1 Soil Sample Results ......................................................................................................8
3.1.1 Metals ...............................................................................................................8
3.1.2 Petroleum Constituents .....................................................................................8
3.1.3 VOCs ................................................................................................................8
3.2 Groundwater .................................................................................................................9
3.2.1 Petroleum Constituents .....................................................................................9
3.2.2 VOCs ................................................................................................................9
3.3 Soil Gas ........................................................................................................................9
3.4 Water Level Measurements ........................................................................................10
4. DATA VALIDATION ........................................................................................................11
5. FINDINGS AND CONCLUSIONS ....................................................................................12
6. REFERENCES ....................................................................................................................14

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LIST OF TABLES
Table 1: Soil Sample Analytical Summary
Table 2: Groundwater Analytical Summary
Table 3: Soil Gas Analytical Summary
Table 4: Depth to Groundwater Summary

LIST OF FIGURES
Figure 1: Site Location Map
Figure 2: Site Layout Map
Figure 3: Previous Investigation Sample Locations
Figure 4: Soil Sample Locations
Figure 4a: Estimated Extent of Soil Exceedances - Petroleum Hydrocarbons
Figure 5: Groundwater Sample Locations
Figure 5a: Estimated Extent of Groundwater Exceedances – Petroleum Hydrocarbons
Figure 5b: Estimated Extent of Groundwater Exceedances - VOCs
Figure 6: Soil Gas Sample Locations
Figure 7: Groundwater Contour Map

LIST OF APPENDICES
Appendix A: Previous Sample Results
Appendix B: Field Forms
Appendix C: Laboratory Analytical Reports
Appendix D: Data Validation Report

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ACRONYMS AND ABBREVIATIONS
SCR Site Characterization Report
SCWP Site Characterization Work Plan
UDEQ Utah Department of Environmental Quality
DERR Division of Environmental Response and Remediation
VCP Voluntary Cleanup Program
ESA Environmental Site Assessment
REC Recognized Environmental Condition
EPA United States Environmental Protection Agency
TPH-DRO Total petroleum hydrocarbons - diesel range organics
TPH-GRO Total petroleum hydrocarbons - gasoline range organics
VOC Volatile organic compound
RCRA Resource Conservation and Recovery Metals
PCB Polychlorinated Biphenyls
RSL Regional Screening Level
RAP Remedial Action Plan
RBCA Risk Based Corrective Action
QAPP Quality Assurance Project Plan
bgs Below Ground Surface
CoC Chain-of-Custody
ISL Initial Screening Level
IDW Investigation Derived Waste
MCL Maximum Containment Level
PPE Personnel Protective Equipment
MS/MSD Matrix Spike/Matrix Spike Duplicate
QA/QC Quality Assurance/Quality Control
UGWQS Utah Groundwater Quality Standard
VISL Vapor Intrusion Screening Level

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1. INTRODUCTION
On behalf of Paxton Project, LLC (Paxton), Geosyntec Consultants (Geosyntec) has prepared this
Site Characterization Report (SCR) for the planned Paxton residential development project
located at 203 to 225 West Paxton Avenue in Salt Lake City, Utah (Site). This SCR presents
results of the soil, soil gas, and groundwater characterization samples that were collected in
accordance with the Site Characterization Work Plan (SCWP) and SCWP Addendum prepared
for the project (Geosyntec 2024a and 20204b). The above samples were collected to support the
preparation of a Remedial Action Plan (RAP) to address identified impacts and facilitate the
planned development of the Site. The characterization and remediation of the Site are being
conducted under the Utah Department of Environmental Quality (UDEQ), Division of
Environmental Response and Remediation’s (DERR) Voluntary Cleanup Program (VCP),
Voluntary Cleanup Site #C-129.
1.1 Site Location and Description
The Site is approximately 0.71 acres in size and was previously occupied by a towing/auto repair
business (Tucker Towing) and two residential dwellings. The location and boundaries of the Site
are presented on Figure 1. The general layout of the Site and key features are presented on Figure
2.
It is noted that the Site buildings and structures have been demolished down to the foundations,
but were present when the site characterization activities were conducted. Prior to the demolition,
required asbestos and lead based paint surveys were conducted and abatement was performed
where required. Additionally, small quantities of miscellaneous fuels and chemicals left by the
previous owner were removed and removed and managed off-site. Records regarding the
demolition and waste management activities were provided to the DERR on November 11, 2024.
1.2 Site Background
Based on historical records, the Site was used for residential purposes dating back to at least 1898.
Towing and/or auto repair operations began at the Site in the 1940s and continued until June 2024.
Paxton is planning to redevelop the property with a multi-unit residential/commercial development
and has entered into the DERR VCP to address the impacts that have been observed at the Site
(see Section 1.3) as part of the planned development. The Site was accepted into the VCP program
on April 1, 2024.
1.3 Previous Investigations Summary
Prior to implementation of the characterization activities described herein, previous investigations
conducted at the Site included a Phase I Environmental Site Assessment (ESA) and two limited
subsurface sampling investigations (Atlas 2023, AGEC 2023a and AGEC 2023b). These previous
investigations were conducted in 2023 as part of Paxton’s planned acquisition of the Site.
The Phase I ESA identified Recognized Environmental Conditions (RECs) associated with the
historic towing/automotive repair activities on the Site including the presence of two former in-

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ground hydraulic lifts (the former hydraulic lift located in the southwestern portion of the Site was
identified in the Phase I ESA as an “underground vault”). The Phase I ESA also identified the
potential for chlorinated solvent impacts from an adjacent RETEP property, which is located to
the north of the Site at 216 West Paxton Avenue, as shown on Figure 2 as a REC. The RETEP
property is listed on EPA’s Comprehensive Environmental Response, Compensation and Liability
Information System (CERCLIS) and has undergone investigation by the EPA and DERR related
to chlorinated solvent impacts to soil and groundwater (Atlas 2023).
The limited subsurface investigations were conducted to determine if the historic auto repair and
towing operations and the adjacent RETEP property had adversely impacted the Site. The initial
investigation was conducted in September 2023 and included the completion of five borings to
collect soil and groundwater samples at potential areas of concern. The subsequent investigation
was conducted in October 2023 and included the installation of 10 monitoring wells at
representative areas around the Site and the collection of two surface soil samples from areas of
surface staining in the storage yard in the center of the Site. All samples were analyzed for oil and
grease, total petroleum hydrocarbon diesel and gasoline range organics (TPH-DRO and TPH-
GRO), and volatile organic compounds (VOCs). Select samples were also analyzed for Resource
Conservation and Recovery Metals (RCRA) metals and polychlorinated biphenyls (PCBs). The
previous sample locations are presented on Figure 3. A tabular summary of the previous analytical
results is provided in Appendix A (AGEC 2023a and AGEC 2023b). The prior investigation
results were screened against. EPA residential and industrial Regional Screening Levels (RSLs),
DERR Initial Screening Levels (ISLs), DERR Risk Based Corrective Action (RBCA) Tier 1
Screening Levels and EPA Maximum Contaminant Levels (MCLs) as relevant and appropriate
based on media type.
Based on the analytical results from the previous investigations, the following key findings were
identified:
 Petroleum related constituents (oil and grease and/or TPH-DRO) were detected above
screening levels in soil samples from three locations. These include boring GP-5
(completed next to the former hydraulic lift in the shop building), monitoring well MW-3
(completed in the northeast corner of the Site), and SS-1 (collected from a stained area in
the storage yard). No other exceedances for petroleum related constituents were observed
in any of the other soil samples that were collected.
 Petroleum related constituents (TPH-DRO/GRO and/or benzene) were detected above
screening levels in groundwater at three locations. These include boring GP-1 (completed
in the north-central portion of the Site), boring GP-5 (completed next to the former
hydraulic lift in the shop building), and MW-7 (completed in the central portion of the
Site). No other exceedances for petroleum related constituents were observed in any of the
other groundwater samples collected from the borings and monitoring wells.
 Chlorinated VOC concentrations did not exceed screening levels in any soil samples, with
the exception of the soil sample that was collected in boring GP-4 from 6 to 7 feet below

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ground surface (bgs). Trichloroethene was detected in this sample at a concentration
exceeding the residential RSL, but below the industrial RSL. This sample appears to have
been collected from below the ground water table and the result is likely influenced by
impacted groundwater.
 One or more chlorinated VOC were detected above screening levels in groundwater in four
of the five boring locations and seven of the ten monitoring well locations. Observed
exceedances included 1,1-dichloroethane, 1,1-dichloroethene, cis-dichloroethene, trans-
dichloroethene, tetrachloroethene, trichloroethene and vinyl chloride. No petroleum or
chlorinated VOCs were detected above screening levels in the deep monitoring wells
(MW-9 and MW-10) that were installed in western portion of the Site.
 RCRA metals were analyzed in the surface soil samples collected from the storage yard
(SS-1 and SS-2), the subsurface soil sample collected from location MW-3 and the
groundwater sample collected from boring GP-1 (installed in the north central portion of
the Site). With the exception arsenic in soil, no exceedances of the screening levels were
identified in the soil or groundwater samples. The reported arsenic concentrations in the
soil samples ranged from 5.64 to 8.35 mg/kg. While the observed concentrations exceed
the screening levels, the investigation report notes that the concentrations are consistent
with background levels of arsenic in soils for the Salt Lake Valley (AGEC 2023b).
 PCBs were analyzed in the soil samples collected from the boring locations (GP-1 through
GP-5). All results were either non-detect or below screening levels.
The overall previous investigation results indicated the presence of limited petroleum related
impacts to soil and groundwater in select areas. Potential sources were noted to include incidental
spills and releases in the storage yard, the historic hydraulic lift in the shop building and a potential
unknown source in the northeast corner of the Site (MW-3). Additionally, the detection of
chlorinated VOCs in groundwater across the Site were indicated to potentially be related to the
RETEP property given their widespread prevalence and the close proximity of that property to the
Site.
1.4 Environmental Setting
The Site is located approximately 1.5 miles southwest of downtown Salt Lake City, Utah. Land
use in the surrounding area is comprised of a mixture of residential, commercial and light industrial
properties. The general topography of the surrounding area is flat with a slight slope to the west.
1.5 Geology and Hydrogeology
The Site is located within the Salt Lake Valley, which is part of the Great Basin physiographic
province of the western United States. It is bordered on the east and northeast by the Wasatch
Range, to the northwest by the Great Salt Lake, on the west by the Oquirrh Mountains, and to the
south by the Traverse Mountains. The valley is filled with unconsolidated to semi-consolidated
sediments with thicknesses reaching up to 4,000 feet in certain areas. The basin fill mainly consists

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of fluvial and lacustrine deposits eroded from the surrounding mountains that intermingle with
alluvial-fan deposits and, to a lesser degree, deltaic and landslide deposits along the valley margins.
Surface deposits in the center of the valley primarily consist of offshore lacustrine silt and clay,
which were deposited during the Pleistocene Bonneville lake cycle approximately 12,000 to
29,000 years ago.
Based on subsurface borings from the previous site investigations, surface soils are primarily
composed of fill from approximately 0 to 2 feet bgs. Surface fill is underlain by predominately by
clays with minor silty sand and clayey sand zones up to depth of 45 feet bgs (maximum depth of
previous investigation conducted at the Site) (AGEC 2023b).
Groundwater has been observed to be present at depths ranging from approximately 4 to 6 feet
below ground surface (bgs) with a relatively flat gradient across the Site (AGEC 2023b). Regional
groundwater flow is estimated to be towards the west, based on topography. The nearest surface
water body to the Site is the Jordan River, which is located approximately one mile west of the
Site. Water level measurements collected from the wells as part of the site characterization
activities are discussed in Section 3.4.
1.6 Investigation Objectives, Scope and Rational
The following site characterization activities were completed in accordance with the SCWP and
SCWP Addendum to further characterize the Site and provided data to support the development
of the RAP:
 Soil sampling – Shallow surface and subsurface soil samples were collected from
representative areas within the Site to further characterize potential impacts from the
storage of vehicles, equipment and potential incidental spills/or leaks of petroleum
products. Samples were initially focused in the areas where exposed soil is present, but
were expanded to include samples beneath paved surfaces along the northern portion of the
Site and beneath the concrete slabs for the shop building and storage building.
 Soil gas sampling – Soil gas samples were collected at two locations in the central portion
of the Site where elevated groundwater concentrations are present. Samples were collected
to determine potential soil gas concentrations and evaluate the need for vapor mitigation
as part of the planned development.
 Groundwater sampling – Groundwater samples were collected from the existing
monitoring wells to confirm prior groundwater concentrations from the previous
investigations and collect additional groundwater elevation measurements to confirm the
groundwater flow direction. In conjunction with the monitoring activities, the wells were
also resurveyed to establish casing elevations relative to NAVD88 elevation datum. The
Site wells were previously surveyed relative to an on-site benchmark.

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2. SAMPLING COLLETION PROCEDURES
The following section present the sample collection procedures that were used for the surface soil,
soil gas and groundwater sampling activities conducted under the SCWP and SCWP Addendum.
All sampling and analytical testing was done in accordance with the Quality Assurance Project
Plan (QAPP) prepared for the Site (Geosyntec 2024c).
2.1 Soil Sampling
Shallow soil samples were collected using a stainless-steel hand auger from 16 representative
locations within the Site in accordance with the sampling procedures presented in the QAPP (SOP-
002). Samples were collected 0-6 inches below ground surface (bgs) with additional samples
collected at approximately 6-12 inches and 12-18 inches bgs at select locations to aid in vertical
delineation. Completed site characterization soil sample locations are shown on Figure 4, along
with the sample intervals completed at each location. At locations where asphalt or concrete
surfaces were present the samples were collected directly below the engineered surfaces. All
samples from 0-6 inches and 6-12 inches bgs were analyzed for RCRA metals, TPH-DRO/GRO,
oil and grease and VOCs using the analytical methods specified in Section 2.4. Deeper samples
collected from 12-18 inches were only analyzed for the above parameters that were observed to
exceed one more screening level based on the initial results from the shallower samples.
2.2 Groundwater Sampling
Groundwater samples were collected from 9 of the 10 monitoring wells within the Site. One well
(MW-6) could not be located during the sampling and was not sampled. The monitoring well
locations are shown on Figure 5. All wells were sampled using a peristaltic pump in accordance
with the low-flow sampling procedures presented in the QAPP (SOP-008). The samples were
collected at the approximate midpoint of the saturated screen interval. Prior to sampling, fluid level
measurements were collected from all wells in accordance with SOP-7 in the QAPP. All
groundwater samples were analyzed for TPH-DRO/GRO, oil and grease and VOCs using the
analytical methods specified in Section 2.4. Completed well sampling logs are included in
Appendix B.
2.3 Soil Gas Sampling
Soil gas samples were collected from temporary soil gas probes installed adjacent to wells MW-5
and MW-7. These wells are located in the central portion of the Site where the highest groundwater
concentration have generally been observed. The location of the soil gas probes is shown on Figure
6. The soil gas probes were installed within the vadose zone at a depth ranging from approximately
3.5 to 4.5 feet bgs (approximately 1.5 feet above the measured groundwater level at the time of the
probe installation) using a direct push drill rig. After installation, soil gas samples were collected
from the probes for VOCs analysis via evacuated stainless-steel summa canisters using the
analytical methods specified in Section 2.4. The soil gas probe installation and soil gas sampling
were performed in accordance with the methods and procedures presented in the QAPP (SOP-009

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and SOP-010). Prior to sampling, the following leak checks were performed to ensure that
representative samples were obtained:
 Summa check;
 Vacuum shut-in leak test; and
 Purging, field screening, and helium shroud leak test.
All samples were collected at a flow rate of approximately 200 milliliters per min (mL/min) using
a laboratory supplied flow controller. Completed soil gas probe construction and sampling logs
are included in Appendix B.
2.4 Laboratory Analytical Methods
All samples were submitted to Pace Analytical Laboratory, a National Environmental Laboratory
Accreditation Conference accredited and Utah certified analytical laboratory. Analyses were
completed using the EPA approved methods presented below, as applicable:
Soil/Groundwater Samples
 RCRA metals by Methods 6010B/7470A/7471A
 TPH -DRO/GRO by Method 8015
 Oil and Grease by Method 1664A/9071
 VOCs by Method 8260B
Soil Gas Samples
 VOCs by Method TO-15
All analyses were performed in accordance with method specific requirements specified in the
QAPP using standard analytical turnaround times. All reports were completed as Level III reports.
Completed laboratory reports are provided in Appendix C.
2.5 Quality Control Sampling
Quality control samples included field duplicate, matrix spike/matrix spike duplicate and
equipment blank and trip blank samples (VOCs only). Quality control samples were collected at
the frequency specified in the QAPP. Data validation is discussed in Section 4.0.
2.6 Sample Handling and Custody
2.6.1 Sample Containers and Labeling
Upon collection, all samples were placed into laboratory-supplied sample containers and labeled
with a unique identification. Clean, disposable, nitrile gloves were worn during sample handling
to prevent cross-contamination between samples.

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2.6.2 Sample Packaging
After labeling, each sample was placed in a cooler containing wet ice to reduce the sample
temperature to approximately 4 (±2) °C during storage and transport to the laboratory. The samples
were packaged and shipped in general accordance with laboratory specified procedures.
2.6.3 Chain of Custody
A Chain of Custody (CoC) form was completed to track sample control and possession from the
time of collection through laboratory analysis. The analyses to be performed were designated on
the CoC form, including the quantity and types of containers that comprised each sample and other
pertinent sample information. One CoC form accompanied each sample shipment.
2.7 Decontamination
All non-disposable sampling equipment was decontaminated prior to use and in-between sample
locations in accordance with the decontamination procedures specified in the QAPP (SOP-12).
Non-disposable sampling equipment was limited to the stainless-steel hand auger used during the
soil sampling activities. Equipment blank samples were collected during soil sampling to evaluate
the effectiveness of the decontamination procedures. Results of the equipment blank samples were
evaluated as part of the data validation (see Section 4.0). No significant detections were reported
in the equipment blank samples indicating that the decontamination procedures were generally
effective at limiting potential cross contamination.
2.8 Investigation Derived Waste Management
Generated investigation derived waste (IDW) consisted of consumable field supplies (paper
towels, miscellaneous paper products, etc.), disposable PPE items (nitrile gloves), purge water and
decontamination water. Consumable field supplies and PPE were collected and disposed of as non-
hazardous solid waste. Purge water and decontamination water were collected containerized in 55-
gallon drum, labeled, and temporarily staged at the Site for future disposal pending
characterization. Approximately 25 gallons of purge/decon water was generated during the site
characterization activities.
2.9 Screening Levels
Screening levels applied to the site characterization data include the most recent EPA residential
RSLs, EPA MCLs, EPA residential Vapor Intrusion Screening Levels (VISLs), and/or DERR
ISLs, as relevant and appropriate based on media type.

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3. INVESTIGATION FINDINGS
The following section present the analytical results for soil, groundwater and soil gas samples
collected as part of the site characterization activities, which are summarized on Tables 1, 2 and 3,
respectively.
3.1 Soil Sample Results
Soil sample locations and depths are indicated on Figure 4. Exceedances of site screening levels
(both sample locations and depths) are described below.
3.1.1 Metals
Exceedances for arsenic, lead and/or cadmium were observed above the EPA residential RSLs in
all of the soil samples. The maximum detected arsenic, cadmium and lead concentrations were
reported at 34.6 mg/kg, 8.79 mg/kg and 714 mg/kg, respectively. Cadmium exceedances were
identified at one sample location (S-4) from 0 to 6 inches bgs. Lead exceedances were observed in
seven sample locations (S-1, S-3, S-4, S-6, S-7, S-15, and SS-1) at depths of 0 to 6 inches and/or
6 to 12 inches bgs. No lead exceedances were observed at deeper depths, with the exception of one
sample (S-6) from 12 to 18 inches bgs. Arsenic concentrations exceeded the screening levels at all
of the sample locations. Arsenic concentrations were generally observed to decrease with depth. It
is noted that naturally occurring concentrations of arsenic are regularly observed exceeding the
screening levels in Salt Lake Valley.
3.1.2 Petroleum Constituents
Exceedances for oil and grease were detected above the DERR ISL of 1,000 mg/kg at seven of the
16 sample locations (S-4, S-5, S-6, S-7, S-11, S-12 and SS-1), with reported concentrations ranging
from 1,250 mg/kg to 11,500 mg/kg. Additionally, TPH-DRO was also detected above the DERR
ISL of 500 mg/kg at sample locations S-5 and S-7 (TPH-DRO concentrations of 542 mg/kg and
1,180 mg/kg, respectively). No exceedances for TPH-GRO were detected in any of the sample
locations. All of the exceedances were observed in the samples collected from 0-6 inches, except
for location SS-1 where the exceedance was observed in the 6-12 inch bgs interval. Deeper samples
(from 6-12 inches or 12-18 inches) were collected from all of the locations where exceedances
were observed, except for locations S-5 and S-11 (deeper samples were not proposed for these
locations). No DERR ISL exceedances were identified in the deeper samples. Similar to the
observed detections of metals, the data suggests that while detections of oil and grease and TPH-
DRO in soil are present in select areas, the impacts do not appear to extend below 12 inches in
depth and in most cases are only present in the upper 6 inches. Figure 4a depicts the estimated
extent of screening level exceedances in soil for petroleum hydrocarbons (e.g., oil and grease,
TPH-DRO, and/or TPG-GRO).
3.1.3 VOCs
Trace detections of one or more VOCs were detected at all 16 sample locations. However, all of
the reported detections were below EPA residential RSLs for soil indicating that significant

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concentrations of VOCs are not present in shallow soil. This is consistent with the samples
collected during the initial investigations, which also did not identify significant VOCs in soil.
3.2 Groundwater
Groundwater sample locations are indicated on Figure 5. Exceedances of site screening levels are
described below.
3.2.1 Petroleum Constituents
TPH-DRO and TPH-GRO were detected in wells MW-2 and MW-7, respectively, at
concentrations that exceed the DERR ISLs of 1 mg/L for these parameters. The reported TPH-
DRO concentration in MW-2 was 1.08 mg/L. The reported TPH-GRO concentration at MW-7 was
3.28 mg/L. At all other locations, the TPH-DRO and TPH-GRO concentrations were either non-
detect or below the DERR ISLs. Figure 5a depicts the estimated extent of screening level
exceedances in groundwater for petroleum hydrocarbons (e.g., TPH-DRO and/or TPG-GRO).
Oil and grease was detected in one well location (MW-1) at a reported concentration of 1.68 mg/L.
The reported concentration is significantly below the DERR ISL for this parameter of 10 mg/L.
No other detections for oil and grease were reported in the samples.
3.2.2 VOCs
Samples from wells MW-2, MW-3, MW-4, MW-5, MW-7 and MW-8 showed detections for one
or more VOCs above the EPA MCLs or RSLs (the RSLs were only applied if an MCL has not
been established for a detected compound). VOCs detected above the MCLs/RSLs include 1,1-
dichloroethane, 1,1-dichloroethene, cis-1,2-dichloroethene, 1,2-dichloropane, and vinyl chloride.
The VOCs that were observed to exceed the MCLs/RSLs and the range of concentrations that were
detected are generally similar to the previous groundwater sample data collected as part of the
initial investigation activities (AGEC 2023a and AGEC 2023b). VOCs observed exceeding the
MCL/RSLs were also observed to exceed the EPA groundwater VISLs in one or more locations,
indicating a potential for vapor intrusion from groundwater to soil gas.
Samples collected from wells MW-9 and MW-10, which are screened at deeper intervals than the
other Site wells, did not show any exceedances of relevant screening levels. The only reported
detection in these wells was for cis-1,2-dichloroethene, which was observed at concentrations
several orders of magnitude below the MCL and VISL for this compound. Figure 5b depicts the
estimated extent of screening level exceedances in groundwater for VOCs.
3.3 Soil Gas
The samples collected from the soil gas probes showed reported detections for benzene,
chloroform, 1,1-dichloroethane, cis-1,2-dichloroethene, tetrachloroethene, trichloroethene and
vinyl chloride at one or both locations above the EPA VISLs for sub-slab and near source soil gas.
Total VOC concentrations ranged from approximately 6,017 μg/m3 in SV-1 to 9,996 μg/m3 in SV-
2, with the highest concentrations generally observed for 1,1-dichloroethane, cis-1,2-
dichloroethene, tetrachloroethene and trichloroethene in both samples. The results indicate that

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elevated levels of soil gas are present that would potentially require mitigation for the development
of residential structures on the Site.
3.4 Water Level Measurements
In conjunction with the groundwater sampling activities water level measurements were made at
the existing well locations. The water level measurements are summarized on Table 4. A
groundwater contour map developed from the water level measurements is provided as Figure 7.
Groundwater was observed to range from approximately 4.5 to 6.0 feet below ground surface
across the Site during the groundwater sampling activities. As shown on Figure 7, the groundwater
gradient is very flat with approximately 0.3 feet of change across the site or 0.0013 ft/ft. The
groundwater flow direction also varies but is generally west to northwest depending on location
with a localized area of flow to the north in the southwest corner of the Site. The overall
groundwater flow direction is generally consistent with the expected regional groundwater flow
direction, which also assumed to be to the west based on topography. Given the shallow depth and
the flat gradient it is likely that shallow groundwater is influenced significantly by surface
precipitation and infiltration and the groundwater depth and flow direction may fluctuate
periodically with these changes.

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4. DATA VALIDATION
All laboratory data were validated by Geosyntec’s internal data validation team in accordance with
the procedures and methods specified in the QAPP. The data validation reports are included in
Appendix D.
The data validation included a review of project specific and laboratory quality control samples
and each analytical test to verify the rests and confirm that no systematic laboratory issues were
occurring for the required analyses. The data were qualified, where necessary, in accordance with
criteria established in the QAPP. Based on the results of the validation, all of the data, as qualified,
were determined to be usable for supporting project objectives and decision-making purposes,
except as noted below.
The non-detect VOC results from the groundwater sample collected from well MW-10 were
qualified as “rejected” due to a holding time issue. MW-10 is a deep well screened from 28 to 33
feet bgs. Sample MW-10 did not meet the method criteria of a pH ≤ 2 (the pH was not determined
until the sample was analyzed by the lab in accordance with standard laboratory procedure).
Therefore, the sample was considered unpreserved. The holding times for the VOCs analysis of
preserved water samples is 14 days from sample collection to analysis. The holding times for the
VOCs analysis of unpreserved water samples is 7 days from sample collection to analysis. Due to
this issue, the sample was analyzed approximately one day outside of the hold time (approximately
8 days after collection).
The only reported analyte in the sample from MW-10 was a trace detection of cis-1,2-
dichloroethene (0.000166 J mg/L), which was detected at a level below the reporting limit (note,
the reported detection was not rejected). While non-detect results in the sample from MW-10, were
rejected it is noted that a comparison of the previous sample collected from this location during
the initial investigation by AGEC (AGEC 2023b) is consistent with the current result, showing
primarily non-detect results. Further, previous data and the current results from the other deep well
on the Site (MW-9) have not indicated that there are elevated levels of VOCs in deeper
groundwater at the Site consistent with the current result from MW-10. Based on this, while the
non-detect results are qualified as “rejected,” they are not considered to significantly hinder the
overall usability of the data or affect the overall conclusions of the SCR report and therefore
additional action to address this issue is not recommended.

Paxton SCR
12
5. FINDINGS AND CONCLUSIONS
Based on the completed Site characterization activities the following key findings and conclusions
are noted:
 Metals (arsenic, lead and/or cadmium) and/or petroleum constituents (oil and grease and/or
TPH-DRO) were observed at all of the 16 soil sample locations (above relevant screening
levels.. With the exception of arsenic, observed exceedances were generally confined
within the upper 12 inches of soil, with only one location (S-6) showing potential elevated
levels of lead from the deeper sample collected from 12-18 inches bgs. Naturally occurring
concentrations of arsenic that exceed the screening levels are regularly observed in the Salt
Lake City Valley. No VOCs were detected in any of the soil samples above relevant
screening levels.
 VOCs and/or petroleum constituents (TPH-GRO/DRO) were detected above screening
levels in the groundwater samples collected from monitoring wells MW-2, MW-3, MW-4,
MW-5, MW-7 and MW-8. Additionally, the VOCs that were observed exceeding the
MCL/RSLs were also observed to exceed the EPA VISLs for groundwater in one or more
locations indicating a potential for vapor intrusion. All of the groundwater exceedances
were observed in the uppermost saturated groundwater zone. No exceedances of relevant
screening levels were detected in the two wells that are screened at deeper intervals within
the Site (wells MW-9 and MW-10), which is consistent with previous investigation data.
Soil data collected from the Site has shown trace detections of VOCs, but has not identified
a significant on-site source for the observed detections in groundwater. No significant on-
site potential sources of VOCs were identified during this or previous investigations and
the available data suggests that the observed detections are potentially related to the
adjacent RETEP site or another off-site source.
 Both soil gas samples collected from the Site showed VOCs levels above the EPA VISLs
for near source sub-slab and near source soil gas. The detection of elevated levels of soil
gas is consistent with observed groundwater concentrations which also exceed the VISLs.
 Groundwater elevation data collected during the groundwater monitoring activities
indicates that a relatively flat gradient exists at the Site and that the overall groundwater
flow direction is generally to the west-northwest, which is consistent with the expected
regional groundwater flow direction and previous Site data. Groundwater is present at
depths ranging from approximately 4.5 to 6.0 feet bgs. Given the shallow depth and the flat
gradient, it is likely that shallow groundwater is influenced significantly by surface
precipitation and infiltration and the groundwater flow direction and depth may fluctuate
with these changes.
Paxton will prepare a remedial action plan (RAP) to address the identified impacts from the Site
characterization activities and the previous assessments. In addition to addressing the identified
impacts, the RAP will also describe the removal of the hydraulic lifts and building foundations

Paxton SCR
13
that are present within the Site. The RAP will be submitted to the DERR for review, public
comment, and approval prior to initiation of work.

Paxton SCR
14
6. REFERENCES
AGEC. 2023a. Limited Subsurface Sampling Investigation, Tucker Towing, 203 to 225 West
Paxton Avenue, Salt Lake City, Utah. September 2023.
AGEC. 2023b. Limited Subsurface Sampling Investigation No. 2, Tucker Towing, 203 to 225 West
Paxton Avenue, Salt Lake City, Utah. October 2023
EPA. 2020. US EPA Contract Laboratory Program National Functional Guidelines for Organic
Superfund Methods Data Review, November 2020 (EPA 540-R-20-005)
ATLAS. 2023. Phase I Environmental Assessment, Tucker Towing, 215 West Paxton Avenue, Salt
Lake City, Utah. December 2023.
Geosyntec. 2024a. Site Characterization Work Plan, 203 to 225 West Paxton Avenue, Salt Lake
City, Utah. June 2024
Geosyntec. 2024b. Site Characterization Work Plan Addendum, 203 to 225 West Paxton Avenue,
Salt Lake City, Utah. September 2024
Geosyntec. 2024c. Quality Assurance Project Plan, Paxton Development, 203 to 225 West Paxton
Avenue, Salt Lake City, Utah. June 2024.

Paxton SCR
TABLES
TABLE 1
SOIL SAMPLE SUMMARY
PAXTON DEVELOPMENT
SALT LAKE CITY, UTAH
SAMPLE LOCATION
DATE COLLECTED
DEPTH (INCHES)
ANALYTE EPA RSL1 UTAH ISL2 Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier
ARSENIC 0.68 - 10.4 12.8 6.92 7.52 15.6 10.7 J 25.9 J 14.3 23.6 34.6 8.48 6.5 4.48 NA 23.3 13.8 11.3
BARIUM 15000 - 203 217 NA 111 107 118 J 213 J NA 260 268 NA 75 52.5 NA 374 145 NA
CADMIUM 7.1 - 1.94 2.2 NA 0.891 J+ 2.49 1.28 J 2.37 J NA 8.79 7.95 1.65 0.609 J+ 0.681 J+ NA 3.1 1.16 NA
CHROMIUM5 85000 - 18.8 15.5 NA 11.4 14.4 10.6 16.7 NA 54.2 68.4 NA 9.93 15.1 NA 20.6 11.8 NA
LEAD 200 - 190 221 53.4 58.9 130 125 J 316 J 224 605 565 186 73.8 385 482 714 270 96.7
SELENIUM 390 - 1.75 J 1.28 J NA 2.47 1.91 J 0.831 U 0.824 U NA 6.34 J 13.2 J NA 0.774 U 0.778 U NA 2.04 J 0.814 U NA
SILVER 390 - 0.136 U 0.140 U NA 0.134 U 0.129 U 0.138 U 0.137 U NA 0.131 U 0.653 U NA 0.653 U 0.129 U NA 1.06 U 1.07 U NA
MERCURY 11 - 0.238 0.318 NA 0.074 0.0548 0.175 0.174 NA 0.173 0.214 NA 0.0474 0.0733 NA 0.638 0.674 NA
TPH-DRO (GC/FID) HIGH FRACTION - 500 58.3 J 62 NA 123 52.5 39 48.5 NA 207 J 233 J NA 542 98.9 J NA 1180 118 NA
TPH-GRO (GC/FID) LOW FRACTION - 150 6.95 J+ 3.38 U NA 9.85 2.82 U 3.08 U J 3.36 J+ NA 2.37 J 1.81 J NA 0.629 J 1.1 J NA 7.03 3.67 J+ NA
OIL & GREASE (HEXANE EXTR) - 1000 852 785 NA 512 251 J 162 150 NA 8270 J 11500 J 345 1440 2070 495 5380 646 NA
BENZENE 1.2 - 0.00713 0.0242 NA 0.0162 0.00169 0.00329 0.00235 NA 0.0163 J 0.00413 J NA 0.00101 J 0.000745 J NA 0.0398 0.0115 NA
N-BUTYLBENZENE 3900 - 0.00726 U 0.00739 U NA 0.00612 U 0.00594 U 0.00645 U 0.00665 U NA 0.00631 U 0.00668 U NA 0.00539 U 0.00545 U NA 0.0083 J 0.00711 U NA
SEC-BUTYLBENZENE 7800 - 0.00398 U 0.00406 U NA 0.00335 U 0.00326 U 0.00353 U 0.00365 U NA 0.00345 U 0.00366 U NA 0.00296 U 0.00299 U NA 0.0048 J 0.00390 U NA
CARBON TETRACHLORIDE 0.65 - 0.00125 U 0.00127 U NA 0.00105 U 0.00101 U 0.00110 U 0.00114 U NA 0.00168 J 0.00165 J NA 0.000923 U 0.000932 U NA 0.00137 U 0.00122 U NA
CHLOROFORM 0.32 - 0.00143 U 0.00145 U NA 0.00120 U 0.00116 U 0.00126 U 0.00130 U NA 0.00123 U 0.00132 U NA 0.00106 U 0.00107 U NA 0.00157 U 0.00278 J NA
1,1-DICHLOROETHANE 3.6 - 0.000680 U 0.00479 NA 0.00685 0.000555 U 0.000604 U 0.000621 U NA 0.000590 U 0.000826 U NA 0.000505 U 0.000510 U NA 0.000747 U 0.000665 U NA
CIS-1,2-DICHLOROETHENE 63 - 0.00198 J 0.0294 NA 0.0285 0.000829 U 0.000902 U 0.000928 U NA 0.000881 U 0.000934 U NA 0.000754 U 0.000822 J NA 0.00144 J 0.0127 NA
TRANS-1,2-DICHLOROETHENE 70 - 0.00144 U 0.00246 J NA 0.00338 J 0.00117 U 0.00128 U 0.00131 U NA 0.00125 U 0.00145 U NA 0.00107 U 0.00108U NA 0.00158 U 0.00141 U NA
ETHYLBENZENE 5.8 - 0.00537 0.0104 NA 0.0186 0.000833 U 0.00786 J 0.00332 J NA 0.0112 J 0.00649 J NA 0.00176 J 0.00208 J NA 0.0267 0.00867 NA
ISOPROPYLBENZENE 1900 - 0.00221 J 0.00342 J NA 0.00775 0.000481 U 0.00427 J 0.00186 J NA 0.000511 U 0.00299 J NA 0.00058 J 0.000874 J NA 0.0117 0.00407 NA
P-ISOPROPYLTOLUENE - - 0.0131 0.0114 NA 0.00871 0.00289 U 0.0367 J 0.0111 J NA 0.0131 0.0123 NA 0.00262 U 0.0046 J NA 0.07 0.0189 NA
METHYLENE CHLORIDE 57 - 0.00919 U 0.00934 U NA 0.00774 U 0.00797 J 0.00816 U 0.00840 U NA 0.00797 U 0.0119 J NA 0.00693 J 0.0085 J NA 0.0101 U 0.00900 U NA
4-METHYL-2-PENTANONE (MIBK) 33000 - 0.00316 U 0.00320 U NA 0.00266 U <0.00258 0.0224 J 0.0114 J NA 0.00274 U 0.00290 U NA 0.00234 U 0.00237 U NA 0.00347 U 0.0175 J NA
METHYL TERT-BUTYL ETHER - 0.000485 U 0.000493 U NA 0.000408 U 0.000395 U 0.000431 U 0.000443 U NA 0.000420 U 0.000445 U NA 0.000360 U 0.000363 U NA 0.000533 U 0.000474 U NA
NAPHTHALENE 2 - 0.0453 J+ 0.0477 J+ NA 0.0382 0.0113 J 0.0302 0.0183 NA 0.0531 0.0459 NA 0.00957 J 0.017 NA 0.104 0.0499 NA
N-PROPYLBENZENE 3800 - 0.00294 J 0.00355 J NA 0.00636 0.00108 U 0.00504 J 0.00199 J NA 0.00393 J 0.00280 J NA 0.000976 U 0.00108 J NA 0.0113 0.00492 J NA
STYRENE 6000 - 0.000317 U 0.000323 U NA 0.000267 U 0.000259 U 0.000281 U 0.000290 U NA 0.0574 0.0369 NA 0.000235 U 0.000238 U NA 0.000349 U 0.000310 U NA
TETRACHLOROETHENE 24 - 0.0157 0.0492 NA 0.0246 0.00101 U 0.00110 U 0.00113 U NA 0.0148 0.0122 NA 0.00144 J 0.00501 NA 0.0195 0.0164 NA
TOLUENE 4900 - 0.0403 0.0893 NA 0.0921 0.00316 J 0.039 J 0.0153 J NA 0.0718 J 0.0240 J NA 0.00693 0.00568 NA 0.168 0.0534 NA
1,1,1-TRICHLOROETHANE 8100 - 0.00128 U 0.00130 U NA 0.00108 U 0.00105 U 0.00113 U 0.00117 U NA 0.00111 U 0.00118 U NA 0.000948 U 0.000958 U NA 0.00140 U 0.00125 U NA
TRICHLOROETHENE 0.94 - 0.015 0.101 NA 0.0477 0.000659 U 0.000717 U 0.000738 U NA 0.00957 0.00850 NA 0.00201 0.0166 NA 0.0205 0.0485 NA
1,2,4-TRIMETHYLBENZENE 300 - 0.0348 0.0408 NA 0.0784 0.00426 J 0.0536 J 0.0213 J NA 0.0496 0.0312 NA 0.00689 0.0144 NA 0.172 0.0642 NA
1,2,3-TRIMETHYLBENZENE 340 - 0.0252 0.0287 NA 0.0438 0.00319 J 0.0344 J 0.0173 J NA 0.0313 0.0214 NA 0.00503 J 0.0106 NA 0.12 0.0365 NA
1,3,5-TRIMETHYLBENZENE 270 - 0.0107 0.011 NA 0.043 0.00226 U 0.0233 J 0.0104 J NA 0.0173 0.0120 NA 0.00325 J 0.00455 J NA 0.0502 0.0243 NA
XYLENES, TOTAL 580 - 0.0721 0.13 NA 0.22 0.00886 0.0836 J 0.046 J NA 0.12 J 0.0641 J NA 0.0174 0.0244 NA 0.374 0.147 NA
Notes:
All results units are reported as mg/kg
U = Analyte not detected above laboratory method detection limit.
TPH-DRO = Total Petroluem Hydrocarbons - Diesel Range Organics
TPH-GRO = Total Petroluem Hydrocarbons - Gasoline Range Organics
NA = Not Analyzed
Gray highlighted concentrations indicate analyte was detected above laboratory method detection limit
Orange highlighted concentrations exceed either residentail soil RSLs or Utah ISLs
2Utah Initial Screening Level (ISL) for Leaking Underground Storage Tank Sites
5RSL for chromium based on trivalent chromium
*Blind duplicate sample labeled S-30 (6-12)
**Blind duplicate sample labeled S-31 (0-6)
***Blind suplicate sample labeled S-32 (0-6)
Qualifiers (based on final data validation qualification):
UJ: The analyte was not detected above the reported sample quantitation limit. However, the reported quantitation limit is approximate and may or may not represent the actual limit of quantitation necessary to accurately and precisely measure the analyte in the sample.
S-5 (0-6)
6-12 0-6 0-6
07/16/2024 07/16/2024 07/16/202407/16/2024
S-4 (0-6)**S-1 (0-6)
07/16/2024
S-1 (6-12)
07/16/2024
0-6 6-12
U: The analyte was analyzed for, but was not detected above the reported sample quantitation limit.
J: The analyte was positively identified; the associated numerical value is the approximate concentration of the analyte in the sample.
J+: The analyte was positively identified; however, the associated numerical value is likely to be higher than the concentration of the analyte in the sample due to positive bias of associated QC or calibration data or attributable to matrix interference.
07/16/2024 07/16/2024
S-6 (12-18)
09/27/2024
12-18
07/16/2024
0-6
S-3 (0-6)
07/16/2024
0-6
S-6 (0-6)
07/16/2024
0-6
S-7 (12-18)
09/27/2024
12-180-6 6-12
S-7 (0-6) S-7 (6-12)
12-18
09/27/2024
S-1 (12-18)
12-18
09/27/2024
S-4 (12-18)S-3 (12-18)
09/27/2024
12-18
S-3 (6-12)*
07/16/2024
6-12
S-2 (0-6) S-3 (6-12) S-4 (0-6)
0-6
1EPA Regional Screening Level (RSL) for Residential Soil, November 2024. RSLs
based on cancer risk of 10-6 and hazard quotient of one.
Page 1 of 2
TABLE 1
SOIL SAMPLE SUMMARY
PAXTON DEVELOPMENT
SALT LAKE CITY, UTAH
SAMPLE LOCATION
DATE COLLECTED
DEPTH (INCHES)
ANALYTE EPA RSL1 UTAH ISL2
ARSENIC 0.68 -
BARIUM 15000 -
CADMIUM 7.1 -
CHROMIUM5 85000 -
LEAD 200 -
SELENIUM 390 -
SILVER 390 -
MERCURY 11 -
TPH-DRO (GC/FID) HIGH FRACTION - 500
TPH-GRO (GC/FID) LOW FRACTION - 150
OIL & GREASE (HEXANE EXTR) - 1000
BENZENE 1.2 -
N-BUTYLBENZENE 3900 -
SEC-BUTYLBENZENE 7800 -
CARBON TETRACHLORIDE 0.65 -
CHLOROFORM 0.32 -
1,1-DICHLOROETHANE 3.6 -
CIS-1,2-DICHLOROETHENE 63 -
TRANS-1,2-DICHLOROETHENE 70 -
ETHYLBENZENE 5.8 -
ISOPROPYLBENZENE 1900 -
P-ISOPROPYLTOLUENE - -
METHYLENE CHLORIDE 57 -
4-METHYL-2-PENTANONE (MIBK) 33000 -
METHYL TERT-BUTYL ETHER -
NAPHTHALENE 2 -
N-PROPYLBENZENE 3800 -
STYRENE 6000 -
TETRACHLOROETHENE 24 -
TOLUENE 4900 -
1,1,1-TRICHLOROETHANE 8100 -
TRICHLOROETHENE 0.94 -
1,2,4-TRIMETHYLBENZENE 300 -
1,2,3-TRIMETHYLBENZENE 340 -
1,3,5-TRIMETHYLBENZENE 270 -
XYLENES, TOTAL 580 -
Notes:
All results units are reported as mg/kg
U = Analyte not detected above laboratory method detection limit.
TPH-DRO = Total Petroluem Hydrocarbons - Diesel Range Organics
TPH-GRO = Total Petroluem Hydrocarbons - Gasoline Range Organics
NA = Not Analyzed
Gray highlighted concentrations indicate analyte was detected above laboratory method
Orange highlighted concentrations exceed either residentail soil RSLs or Utah ISLs
2Utah Initial Screening Level (ISL) for Leaking Underground Storage Tank Sites
5RSL for chromium based on trivalent chromium
*Blind duplicate sample labeled S-30 (6-12)
**Blind duplicate sample labeled S-31 (0-6)
***Blind suplicate sample labeled S-32 (0-6)
Qualifiers (based on final data validation qualification):
UJ: The analyte was not detected above the reported sample quantitation limit. However
U: The analyte was analyzed for, but was not detected above the reported sample quanti
J: The analyte was positively identified; the associated numerical value is the approxima
J+: The analyte was positively identified; however, the associated numerical value is lik
1EPA Regional Screening Level (RSL) for Residential Soil, November 2024. RSLs
based on cancer risk of 10-6 and hazard quotient of one.
Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier
6.5 14.8 15.5 9.25 9.3 12.1 13.6 4.4 4.03 10.9 3.13 26.5 12.4 6.44
70.7 76.3 170 J 88.8 34 103 144 92.2 81.2 137 89.2 251 262 NA
0.909 J+ 1.35 1.98 0.375 J 0.173 J 1.13 1.38 0.249 J 0.413 J 0.613 0.137 J 1.99 2.5 NA
16.7 11.5 8.16 3.49 67 6.69 8.49 5.65 4.5 7.68 5.2 10.6 17 NA
146 178 183 26.1 6.06 136 190 26.2 27.1 121 12.8 309 414 19.1
0.778 U 1.09 J 0.816 U 0.798 U 0.785 U 0.845 U 0.893 U 0.910 U 0.921 U 0.903 U 0.885 U 0.877 U 1.57 J NA
0.129 U 0.130 U 1.07 U 1.04 U 1.03 U 1.11 U 1.17 U 1.19 U 1.21 U 1.18 U 1.16 U 1.15 U 0.286 J NA
0.0529 0.0848 0.128 0.032 J 0.0212 U 0.195 0.208 0.226 J 0.487 J 0.56 0.0243 J 0.947 0.552 NA
60.4 60 49.8 J 41.6 J 114 39.6 J 126 J 6.92 J 3.17 J 29.7 2.26 J 72.1 143 NA
2.59 U 1.51 J 4.59 J+ 3.04 U 2.64 U 3.04 U 3.37 U 3.51 U 3.56 U 3.7 U 3.58 U 4.76 J+ 3.36 U NA
362 445 785 J 646 2280 1250 979 116 J 120 J- 128 38.2 U 184 1220 151
0.00713 0.00169 0.035 0.000911 J 0.000493 U 0.00153 0.0155 0.000655 U 0.000666 U 0.00671 0.000670 U 0.0184 0.000911 J NA
0.00544 U <0.00565 0.00669 U 0.00638 U 0.00555 U 0.00639 U 0.00708 U 0.00736 U 0.00748 U 0.00779 U 0.00753 U 0.00728 U 0.00705 U NA
0.00298 U 0.0042 J 0.00367 U 0.00350 U 0.00304 U 0.00351 U 0.00389 U 0.00404 U 0.00411 U 0.00427 U 0.00413 U 0.00399 U 0.00387 U NA
0.000930 U 0.000966 U 0.00114 U 0.00110 U 0.000949 U 0.00109 U 0.00121 U 0.00126 U 0.00128 U 0.00174 J 0.00129 U 0.00125 U 0.00121 U NA
0.00107 U 0.00111 U 0.00131 U 0.00125 U 0.00109 U 0.00125 U 0.00139 U 0.00144 U 0.00147 U 0.00152 U 0.00147 U 0.00143 U 0.00138 U NA
0.000509 U 0.000529 U 0.0106 0.000596 U 0.000519 U 0.0033 0.00951 0.000689 U 0.000700 U 0.0023 J 0.000704 U 0.000681 U 0.00297 J NA
0.000760 U 0.000790 U 0.165 0.0101 0.000775 U 0.0321 0.0606 0.00103 U 0.00105 U 0.0114 0.00105 U 0.00102 U 0.0106 NA
0.00108 U 0.00112 U 0.00733 0.00126 U 0.00110 U 0.00477 J 0.0066 J 0.00146 U 0.00148 U 0.00167 J 0.00149 U 0.00144 U 0.00185 J NA
0.00521 0.00312 0.00988 0.000894 U 0.000778 U 0.00196 J 0.00704 0.00103 U 0.00143 J 0.00341 J 0.00172 J 0.0289 0.00277 J NA
0.00195 J 0.00199 J 0.00277 J 0.000516 U 0.000449 U 0.00122 J 0.00152 J 0.000596 U 0.000606 U 0.000630 U 0.000610 U 0.00434 0.00215 J NA
0.01 0.0132 0.0132 0.00310 U 0.00269 U 0.00679 0.00761 0.00358 U 0.00405 J 0.00508 J 0.00366 U 0.0203 0.00765 NA
0.00688 U 0.00828 J 0.0319 U 0.0304 U 0.00701 U 0.0304 U 0.0337 U 0.00931 U 0.0356 U 0.00983 U 0.00951 U 0.0347 U 0.00891 U NA
0.0172 J 0.00734 J 0.0133 J 0.00276 U 0.00241 U 0.00309 J 0.00308 U 0.00320 U 0.00325 U 0.00338 U 0.00327 U 0.00946 J 0.00306 U NA
0.000363 U 0.000377U 0.000447 U 0.000425 U 0.00086 J 0.000426 U 0.000472 U 0.000491 U 0.000499 U 0.000519 U 0.000502 U 0.00125 J 0.000470 U NA
0.0248 0.0118 J 0.0451 0.00593 U 0.00879 J 0.0192 0.0225 0.00685 U 0.00696 U 0.0143 J 0.00700 U 0.0203 0.0315 J+ NA
0.00215 J 0.00328 J 0.00293 J 0.00115 U 0.00100 U 0.00136 J 0.00219 J 0.00133 U 0.00135 U 0.00141 U 0.00137 U 0.00981 0.00189 J NA
0.000237 U 0.000246 U 0.000292 U 0.000278 U 0.000242 U 0.000279 U 0.000309 U 0.000321 U 0.000326 U 0.000339 U 0.000328 U 0.000317 U 0.000307 U NA
0.000928 U 0.000964 U 0.0461 0.00388 0.000946 U 0.00425 0.0112 0.00243 J 0.0017 J 0.119 0.0128 1.71 0.209 NA
0.0352 0.0168 0.169 J 0.00459 J 0.00137 U 0.0115 0.0781 0.00182 U 0.00185 U 0.0264 0.00186 U 0.176 0.00976 NA
0.000956 U 0.000993 U 0.00564 0.00112 U 0.000975 U 0.00145 J 0.00125 U 0.00129 U 0.00132 U 0.016 0.00133 U 0.00604 0.0148 NA
0.000605 U 0.000629 U 0.0625 0.0031 0.000617 U 0.0106 0.0258 0.000819 U 0.000832 U 0.244 0.0159 0.0103 0.176 NA
0.031 0.175 0.0529 0.00276 J 0.00167 U 0.019 0.02 0.00222 U 0.00225 U 0.00455 J 0.00227 U 0.119 0.0273 NA
0.0223 0.159 0.0379 0.00236 J 0.00167 U 0.0109 0.00954 0.00222 U 0.00225 U 0.00319 J 0.00227 U 0.0462 0.0165 NA
0.00951 0.0402 0.0132 0.00243 U 0.00211 U 0.00772 0.00609 J 0.00281 U 0.00285 U 0.00296 U 0.00287 U 0.0533 0.0104 NA
0.0805 0.053 0.142 0.00571 J 0.000930 U 0.0311 0.0793 0.00123 U 0.00235 J 0.0214 0.00244 J 0.326 0.0456 NA
S-14 (6-12)S-8 (0-6) S-9 (0-6) S-10 (0-6) S-10 (6-12) S-11 (0-6)
07/16/2024 07/16/2024 09/27/2024 09/27/2024 09/30/2024
0-6 0-6
S-12 (6-12) S-13 (0-6) S-13 (0-6)*** S-14 (0-6)
09/27/2024 09/27/2024 09/30/2024 09/30/2024 09/30/2024
SS-1 (12-18)
09/30/2024
12-18
S-15 (0-6) SS-1 (6-12)
0-6 0-6 6-12 0-6
09/30/2024 09/27/2024 07/16/2024
S-12 (0-6)
6-12 0-6 6-120-6 6-12 0-6 0-6
Page 2 of 2
TABLE 2
GROUNDWATER SAMPLE SUMMARY
PAXTON DEVELOPMENT
SALT LAKE CITY, UT
SAMPLE LOCATION
DATE COLLECTED
Analyte EPA MCLs EPA RSL DERR ISL EPA VISLs Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier
OIL & GREASE (HEXANE EXTR) - - 10 - 1.29 U J 1.68 J 1.22 U 1.38 U 1.36 U 1.36 U 1.22 U 1.38 U 1.36 U 1.36 U
TPH-DRO (GC/FID) HIGH FRACTION - - 1 - 0.107 0.0391 J 1.08 0.134 0.133 0.145 0.13 0.189 0.164 J- 0.216
TPH-GRO (GC/FID) LOW FRACTION - - 1 - 0.1 U 0.1 U 0.139 J 0.1 U 0.254 J+ 0.570 3.28 0.583 0.1 U 0.1 U
BENZENE 0.005 - - 0.00159 0.0000941 U 0.0000941 U 0.000232 J 0.0014 0.000247 J 0.000343 J 0.00141 0.000292 J 0.0000941 U 0.0000941 U R
1,1-DICHLOROETHANE - 0.0028 - 0.00764 0.000100 U 0.000100 U 0.00965 0.00405 0.0437 0.0829 0.707 0.138 0.000100 U 0.000100 U R
1,2-DICHLOROETHANE 0.005 - - 0.00224 0.0000819 U 0.0000819 U 0.0000819 U 0.0000819 U 0.0000819 U 0.0000819 U 0.00114 0.0000819 U 0.0000819 U 0.0000819 U R
1,1-DICHLOROETHENE 0.007 - - 0.00387 0.000188 U 0.000188 U 0.00284 0.000683 J 0.00647 0.0233 0.141 0.0416 0.000188 U 0.000188 U R
CIS-1,2-DICHLOROETHENE 0.07 - - 0.250 0.000126 U 0.000126 U 0.146 0.0527 0.247 0.672 4.19 0.726 0.000309 J 0.000166 J
TRANS-1,2-DICHLOROETHENE 0.1 - - 0.109 0.000149 U 0.000149 U 0.00346 0.00162 0.00881 0.0195 0.0901 0.0127 0.000149 U 0.000149 U R
1,2-DICHLOROPROPANE 0.005 - - 0.00658 0.000149 U 0.000149 U 0.000149 U 0.000149 U 0.000149 U 0.000255 J 0.00695 0.000149 U 0.000149 U 0.000149 U R
ETHYLBENZENE 0.7 - - 0.00349 0.000137 U 0.000137 U 0.000137 U 0.000175 J 0.000137 U 0.000137 U 0.000137 U 0.000137 U 0.000137 U 0.000137 U R
TETRACHLOROETHENE 0.005 - - 0.0149 0.000300 U 0.000300 U 0.000300 U 0.000401 J 0.000300 U 0.000300 U 0.000300 U 0.000300 U 0.000300 U 0.000300 UR
TOLUENE 1 - - 19.2 0.000278 U 0.000278 U 0.000278 U 0.00123 0.000278 U 0.000278 U 0.000278 U 0.000278 U 0.000278 U 0.000278 U R
1,1,1-TRICHLOROETHANE 0.2 - - 7.420 0.000149 U 0.000149 U 0.000149 U 0.000163 J 0.000149 U 0.000149 U 0.000149 U 0.000149 U 0.000149 U 0.000149 U R
TRICHLOROETHENE 0.005 - - 0.0019 0.000190 U 0.000190 U 0.00034 J 0.00162 0.00112 0.00115 0.00141 0.000632 J 0.000190 U 0.000190 U R
VINYL CHLORIDE 0.002 - - 0.000147 0.000234 U 0.000234 U 0.00191 0.000865 J 0.0434 0.00767 0.28 0.0105 0.000234 U 0.000234 U R
XYLENES, TOTAL 10 - - 0.385 0.000174 U 0.000174 U 0.000174 U 0.000433 J 0.000174 U 0.000174 U 0.000174 U 0.000174 U 0.000174 U 0.000174 U R
Notes:
All results units are reported as mg/l
U = Analyte not detected above laboratory method detection limit.
Gray highlighted concentrations indicate analyte was detected above laboratory method detection limit
Orange highlighted concentrations exceed EPA MCLs, RSLs or DERR ISLs. RSLs only applied if MCL does not exist for a parameter
Underlined and bold concentrations exceed EPA VISLs
U = Analyte not detected. Value shown is the method detection limit.
TPH-DRO = Total Petroluem Hydrocarbons - Diesel Range Organics
TPH-GRO = Total Petroluem Hydrocarbons - Gasoline Range Organics
EPA MCL = EPA Maximum Containment Level (MCL) for drinking water
EPA RSL = EPA Regional Screening Level (RSL) for Tap Water, November 2024. RSLs based on residential exposure using cancer risk of 10-6 and hazard quotient of one.
EPA VISL = EPA Vapor Intrusion Screening Level (VISL). VISL based on residential exposure using cancer risk of 10-6 and hazard quotient of one.
DERR ISL = Division of Environmental Response and Remediation Initial Screening Levels
*Blind duplicate sample labeled MW-25
Qualifiers (based on final data validation qualification):
R-: The sample results are rejected due to deficiencies in the ability to analyze the sample and meet quality control criteria. The presence or absence of the analyte cannot be verified.
07/17/2024 07/17/2024 07/18/2024 07/18/202407/17/2024
Petroleum Hydrocarbons
Volatile Orgainic Compounds
J+: The analyte was positively identified; however, the associated numerical value is likely to be higher than the concentration of the analyte in the sample due to positive bias of associated QC or calibration data or attributable to matrix interference.
J: The analyte was positively identified; the associated numerical value is the approximate concentration of the analyte in the sample.
UJ: The analyte was not detected above the reported sample quantitation limit. However, the reported quantitation limit is approximate and may or may not represent the actual limit of quantitation necessary to accurately and precisely measure the analyte in the sample.
MW-2
07/17/2024
MW-1 MW-10MW-4 MW-7MW-3 MW-9
07/18/2024
MW-1*
07/17/2024 07/17/2024
MW-5
07/18/2024
MW-8
1
TABLE 3
SOIL GAS SAMPLE SUMMARY
PAXTON DEVELOPMENT
SALT LAKE CITY, UTAH
ANALYTE EPA VISL Result Qualifier Result Qualifier Result Qualifier
ACETONE - 9.48 13.5 J 6.94 J
BENZENE 12 20.1 4.92 4.95
CARBON DISULFIDE 24000 1.95 1.39 J 0.317 U J
CHLOROFORM 4.07 5.35 15.9 16.4
1,1-DICHLOROETHANE 58.5 1580 1040 J 1480 J
1,1-DICHLOROETHENE 6950 57.1 80.8 84.4
CIS-1,2-DICHLOROETHENE 1390 1260 3920 J 5630 J
TRANS-1,2-DICHLOROETHENE 1390 68.6 227 J 325 J
1,2-DICHLOROPROPANE 25.3 3.75 2.54 2.39
ETHANOL - 11.1 9.14 J 5.45 J
ETHYLBENZENE 37.4 14.3 4.18 4.19
4-ETHYLTOLUENE - 6.58 0.384 U 0.384 U
TRICHLOROFLUOROMETHANE - 0.460 U 1.42 1.4
DICHLORODIFLUOROMETHANE 3480 1.24 2.2 2.84
HEPTANE 13900 5.4 3.61 3.2
N-HEXANE 24300 3.7 2.37 J 0.726 U J
ISOPROPYLBENZENE - 2.09 0.382 U 0.382 U
METHYLENE CHLORIDE 3380 2.26 2.7 J 1.23 J
METHYL TERT-BUTYL ETHER 360 4.9 0.233 U 0.233 U
TETRACHLOROETHENE 360 1100 733 J 1070 J
TETRAHYDROFURAN 69500 2.21 1.93 1.87
TOLUENE 174000 67.4 24.9 26.3
1,1,1-TRICHLOROETHANE 174000 60.4 54.9 57.1
TRICHLOROETHENE 15.9 1610 836 J 1250 J
1,2,4-TRIMETHYLBENZENE 2090 33.8 2.46 J 1.81 J
1,3,5-TRIMETHYLBENZENE 2090 10.4 0.382 U 0.382 U
2,2,4-TRIMETHYLPENTANE - 5.93 5.00 5.14
VINYL CHLORIDE 5.59 4.01 0.243 U 0.243 U
M&P-XYLENE 3480 46.8 10.6 11.4
O-XYLENE 3480 18.3 3.93 4.38
TPH (GC/MS) LOW FRACTION 13900 2910 2960 2210
TOTAL VOCS - 6017.15 7004.39 9996.39
Notes:
Table shows detected compounds only
All results units are reported as μg/m3
U = Analyte not detected above laboratory method detection limit.
Gray highlighted concentrations indicate analyte was detected above laboratory method detection limit
Orange highlighted concentrations exceed VISL
EPA VISL = EPA Residential Vapor Intrusion Screening Level (VISL) for sub-slab and near source soil gas. VISL based on cancer risk of 10-6 and hazard quoteint of one.
VOCs = Volatile Organic Compounds
Total VOC calculated as the sum of detected VOCs
*Blind duplicate sample labeled SV-20
Qualifiers (based on final data validation qualification):
DATE COLLECTED
SAMPLE LOCATION
J: The analyte was positively identified; the associated numerical value is the approximate concentration of the analyte in the sample.
SV-1 SV-2 SV-2*
09/30/2024 09/30/2024 09/30/2024
TABLE 4
DEPTH TO GROUNDWATER SUMMARY (JULY 2024)
PAXTON DEVELOPMENT
SALT LAKE CITY, UTAH
Well Top of Casing Elevation (ft) Depth To Groundwater (ft) Groundwater Elevation (ft)
MW-1 4230.634 5.90 4224.73
MW-2 4230.996 6.20 4224.80
MW-3 4230.549 5.75 4224.80
MW-4 4229.354 4.62 4224.73
MW-5 4230.419 5.55 4224.87
MW-7 4230.741 5.98 4224.76
MW-8 4229.362 4.79 4224.57
MW-9 4230.340 6.02 4224.32
MW-10 4230.256 5.21 4225.05
Notes:
All groundwater measurments performed on July 24, 2024
Top of casing elevations based on survey conducted on survey conducted by Ensign Engineering on September 1, 2024.
All elevations based on NAVD88 datum
Paxton SCR
FIGURES
J.

W
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Legend Figure
1
Site Location
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT November 2024
Client LogoPaxton
DevelopmentApproximate Site Boundary
Site
J.

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c
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Legend
Figure
2
Site Location
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT November 2024
Client LogoPaxton
DevelopmentApproximate Site Boundary
Site
Paxton Ave.
W Lucy Ave.
Paxton Place
Apartments
RETEP site
Private Residence
Shop Building
Storage BuildingResidences
Storage
Building
In-ground Lift
Storage Yard
J.

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Legend
Figure
3
Previous Investigation Sample Locations
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT November 2024
Client LogoPaxton
Development
Approximate Site Boundary
Groundwater Sample Location
Soil Boring Sample Location
GP-2
MW-8 MW-4
GP-1
GP-4
MW-7 SS-2
SS-1
MW-2
MW-3
GP-5
MW-6
GP-3
MW-1
MW-10
MW-9
MW-5
Surface Soil Sample Location
J.

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Legend
Figure
4
Soil Sample Locations
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT November 2024
Client LogoPaxton
Development
Approximate Site Boundary
Impervious Surfaces
Soil Sample Location (Sample Depths Shown in
Parenthesis)
SS-1 (6-12”,
12-18”)
S-1 (0-6”, 6-
12”, 12-18”)
S-2 (0-6”)
S-4 (0-6”,
12-18”)S-5 (0-6”)
S-6 (0-6”,
12-18”)
S-7 (0-6”`, 6-
12”, 12-18”)S-8 (0-6”)
S-3 (0-6”, 6-
12”, 12-18”)
S-9 (0-6”)
S-10 (0-6”,
6-12”)
S-14
(0-6”,
6-12”)
S-11 (0-6”)S-12 (0-6”,
6-12”)
S-13 (0-6”)
S-15 (0-6”)
J.

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Legend
Figure
4a
Estimated Extent of Soil Exceedances – Petroleum
Hydrocarbons
203 to 225 West, Salt Lake City, Utah
Salt Lake City, UT January 2025
Client LogoPaxton
Development
Approximate Site Boundary
Impervious Surfaces
Soil Sample Location (Sample Depths Shown in
Parenthesis)
SS-1 (6-12”,
12-18”)
S-1 (0-6”, 6-
12”, 12-18”)
S-2 (0-6”)
S-4 (0-6”,
12-18”)S-5 (0-6”)
S-6 (0-6”,
12-18”)
S-7 (0-6”, 6-
12”, 12-18”)S-8 (0-6”)
S-3 (0-6”, 6-
12”, 12-18”)
S-9 (0-6”)
S-10 (0-6”,
6-12”)
S-14
(0-6”,
6-12”)
S-11 (0-6”)S-12 (0-6”,
6-12”)
S-13 (0-6”)
S-15 (0-6”)
Soil Sample Location with Petroleum Hydrocarbon
Exceedance (Sample Depths Shown in
Parenthesis with Exceedances Highlighted)
Approximate Extent of Petroleum Hydrocarbon
Exceedance
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Legend
Figure
5
Groundwater Sample Locations
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT November 2024
Client LogoPaxton
Development
Approximate Site Boundary
Existing Groundwater Monitoring Well
MW-8 MW-4
MW-7
MW-2
MW-3
MW-6*
MW-1
MW-10
MW-9
MW-5
J.

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Legend
Figure
5a
Estimated Extent of Groundwater Exceedances –
Petroleum Hydrocarbons
203 to 225 West, Salt Lake City, Utah
Salt Lake City, UT January 2025
Client LogoPaxton
Development
Approximate Site Boundary
Existing Groundwater Monitoring Well
MW-8 MW-4
MW-7
MW-2
MW-3
MW-6
MW-1
MW-10
MW-9
MW-5
Existing Groundwater Monitoring Well with
Petroleum Hydrocarbon Exceedance
Approximate Extent of Petroleum
Hydrocarbon Screening Level Exceedances
in Groundwater
J.

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Legend
Figure
5b
Estimated Extent of Groundwater Exceedances -
VOCs
203 to 225 West, Salt Lake City, Utah
Salt Lake City, UT January 2025
Client LogoPaxton
Development
Approximate Site Boundary
Existing Groundwater Monitoring Well
MW-8 MW-4
MW-7
MW-2
MW-3
MW-6*
MW-1
MW-10
MW-9
MW-5
*MW -6 could not be located and was not
sampled, but previously had exceedances.
Existing Groundwater Monitoring Well with
VOC Exceedance
Approximate Extent of VOC Exceedance
in Groundwater
J.

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Legend
Figure
6
Soil Gas Sample Locations
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT November 2024
Client LogoPaxton
Development
Approximate Site Boundary
Groundwater Monitoring Well
MW-8 MW-4
MW-7
MW-2
MW-3
MW-6
MW-1
MW-10
MW-9
MW-5
Soil Gas Vapor Probe
SV-1SV-2
J.

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Legend
Figure
7
Groundwater Contour Map (July 24, 2024)
203 to 225 West.
Salt Lake City, Utah
Salt Lake City, UT October 2024
Client LogoPaxton
Development
Approximate Site Boundary
Groundwater Monitoring Well
MW-8 MW-4
MW-7
MW-2
MW-3
MW-6
MW-1
MW-5
4224.57
4224.73
4224.80
4224.80
4224.73
4224.87
4224.60
MW-9
MW-10 4224.76
Groundwater Contour Line
Groundwater Flow Direction

Paxton SCR

APPENDIX A
Previous Sample Results
Table 1A - Soil Analytical Results
Tucker Towing, 203-225 West Paxton Avenue, Salt Lake City, Utah
Sample Depth Sample PI
D
PC
B
s
*
O
&

G
*
*
TP
H
-
D
R
O
TP
H
-
G
R
O
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-
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1,
1
-
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s

1
,
2
-
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P
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o
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z
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PC
E
*
*
*
To
l
u
e
n
e
1,
1
,
1
-
T
r
i
c
h
l
o
r
o
e
t
h
a
n
e
TC
E
*
*
*
*
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
2
,
3
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
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n
z
e
n
e
Xy
l
e
n
e
s
ID (feet) Date (ppm) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)
GP-1 6 to 7 8/12/2023 0.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
GP-2 6 to 7 8/12/2023 0.2 ND ND ND ND ND ND ND 0.0210 0.178 ND ND ND ND ND ND 0.00588 0.00462 ND ND ND ND ND ND
GP-3 7 to 8 8/12/2023 0.1 ND ND ND ND ND ND ND 0.0193 0.175 ND ND ND ND ND ND 0.00987 ND ND 0.0103 ND ND ND ND
GP-4 0 to 1 8/12/2023 0.3 ND 654 36 ND ND ND ND 0.0145 0.102 ND ND ND ND ND ND 0.0117 ND ND 0.00492 ND ND ND ND
GP-4 6 to 7 8/12/2023 0 0.0827 ND ND 5.17 0.542 0.00883 0.0149 0.0712 0.339 0.0236 0.00592 ND 0.0118 ND ND 1.64 0.0437 0.109 2.21 0.0388 0.0234 0.0132 0.0823
GP-5 0 to 1 8/12/2023 0 ND 185 71.4 8.89 ND 0.0274 ND ND ND ND 0.0334 0.0157 0.0165 0.0445 0.0134 1.99 0.233 ND ND 0.0962 0.0920 0.0836 0.308
GP-5 7 to 8 8/12/2023 0 ND 1,360 228 ND ND ND ND ND ND ND ND ND ND ND ND 0.0240 ND ND 0.00318 ND ND ND ND
SS-1 0 to 1/2 10/5/2023 756 NA 18,600 9,380 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.00573 ND 0.00118 0.00783 ND ND 0.0111
SS-2 0 to 1/2 10/6/2023 122 NA 405 60.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-1 7 10/6/2023 0 NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-2 7 10/5/2023 0.6 NA 169 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.0167 ND ND 0.00697 ND ND ND ND
MW-3 1 to 2 10/5/2023 68 NA 1,220 5.30 ND ND ND ND ND ND 0.00329 ND ND ND ND ND 0.00807 ND 0.00381 0.0210 0.00594 ND ND 0.00984
MW-4 7 10/6/2023 398 NA ND ND ND ND ND ND 0.00972 ND 0.0991 ND ND ND ND ND 0.00660 ND ND 0.0147 ND ND ND ND
MW-5 7 10/6/2023 394 NA ND ND ND ND ND ND 0.00646 ND 0.0419 ND ND ND ND ND 0.0228 ND ND 0.0147 ND ND ND ND
MW-6 7 10/6/2023 0 NA 179 ND ND ND ND ND ND ND 0.00588 ND ND ND ND ND 0.00568 ND ND 0.00527 ND ND ND ND
MW-7 7 10/6/2023 399 NA ND ND ND ND ND ND 0.0147 ND 0.109 ND ND ND ND ND 0.0710 ND ND 0.0551 ND ND ND ND
MW-8 7 10/5/2023 0 NA 245 ND ND ND ND ND 0.0129 ND 0.260 ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-9 7 10/5/2023 1.5 NA 157 ND ND ND ND ND ND ND 0.0303 ND ND ND ND ND 0.0295 ND ND 0.0174 ND ND ND ND
MW-10 7 10/5/2023 0 NA ND ND ND ND ND ND 0.00511 ND 0.0413 ND ND ND ND ND 0.0350 ND ND 0.0210 ND ND ND ND
Utah ISL 1,000 500 150 0.2 5 51 9 142
10,000 5,000 1,500 0.9 23 51 25 142
0.24 NS NS NS 70,000 1.2 0.65 3.6 230 63 5.8 1,900 NS 2 380 24 4,900 8,100 0.94 300 340 270 580
November 2023 EPA Industrial RSL 0.99 NS NS NS 1,100,000 5.1 2.9 16 1,000 370 25 9,900 NS 8.6 2,400 100 47,000 36,000 6 1,800 2,000 1,500 2,500
NA = Not analyzed
ND = Non Detect
NS = No Utah or EPA Standard
* = PCB 1260
** = TPH Oil and Grease
*** = PCE expressed as tetrachloroethylene in laboratory results
**** = TCE expressed as trichloroethylene in laboratory results
Bold = Concentrations above Utah Initial Screening Level (ISL)
Bold Shaded = Concentrations above RBCA Tier 1 SL
EPA Residential and Industrial RSLs based on Hazard Index of one and cancer risk of 10-6.
Utah RBCA Tier 1 SL
November 2023 EPA Residential RSL
Table modified from Table 1A presented in the Limited Subsurface Sampling Investigation No. 2, Tucker Towing, 203 to 225 West Paxton Avenue, Salt Lake City, Utah (AGEC 2023).
Table 1B - Soil Anaytical Results - RCRA 8 Metals
Tucker Towing, 203-225 West Paxton Avenue, Salt Lake City, Utah
Sample Depth Sample Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver
ID (feet) Date (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)
SS-1 0 to 1/2 10/5/2023 0.0771 6.15 176 1.26 16.6 123 ND ND
SS-2 0 to 1/2 10/6/2023 ND 8.35 174 ND 16.1 43.5 ND ND
MW-3 1 to 2 10/5/2023 0.0441 5.64 50.8 ND 4.64 62.9 ND 1.38
November 2023 EPA Residential RSL 11 0.68 15,000 7.1 NS 400 390 390
November 2023 EPA Industrial RSL 46 3 220,000 100 NS 800 5,800 5,800
NS = No EPA standard for total chromium
ND = Non Detect
Bold = Concentrations above EPA Residential SL
EPA Residential and Industrial RSLs based on a Hazard Index of one and cancer risk of 10-6.
Table modified from Table 1B presented in the Limited Subsurface Sampling Investigation No. 2, Tucker Towing, 203 to 225 West
Paxton Avenue, Salt Lake City, Utah (AGEC 2023).
Table 2 - Groundwater Analytical Results
Tucker Towing, 203-225 West Paxton Avenue, Salt Lake City, Utah
Sample Sample Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver O & G*TPH-DRO TPH-GRO C10-C28 (Diesel)C28-C40 (Oil)Benzene 1,1-Dichloroethane 1,1-Dichloroethene cis 1,2-Dichloroethene Trans-1,2-Dichloroethene 1,2-Dichloropropane PCE Toluene TCE Vinyl Chloride
ID Date (mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)
GP-1 8/12/2023 ND ND 0.296 ND ND ND ND ND ND 0.402 0.134 NA NA 0.00747 0.0169 0.00231 0.0687 0.00174 ND ND 0.00520 ND 0.0309
GP-2 8/12/2023 NA NA NA NA NA NA NA NA ND ND 0.650 NA NA 0.00468 0.0777 0.0244 0.904 0.0230 ND ND 0.00520 ND 0.0135
GP-3 8/12/2023 NA NA NA NA NA NA NA NA ND ND 0.557 NA NA 0.00174 0.118 0.0511 0.750 0.0106 ND ND 0.00163 ND 0.0104
GP-4 8/12/2023 NA NA NA NA NA NA NA NA ND ND 0.320 NA NA ND 0.0807 0.0247 0.292 0.00675 ND ND ND ND 0.00526
GP-5 8/12/2023 NA NA NA NA NA NA NA NA ND 1.19 ND NA NA 0.00501 ND ND 0.00744 ND ND 0.00235 0.00637 ND ND
MW-1 10/11/2023 NA NA NA NA NA NA NA NA ND NA ND 0.100 0.363 ND ND ND ND ND ND ND ND ND ND
MW-2 10/11/2023 NA NA NA NA NA NA NA NA ND NA 0.166 ND 0.356 ND 0.0107 0.00390 0.176 0.00472 ND ND ND ND 0.00255
MW-3 10/11/2023 NA NA NA NA NA NA NA NA ND NA 0.218 0.137 0.395 ND 0.0350 0.0151 0.488 0.0105 ND ND ND ND 0.00620
MW-4 10/11/2023 NA NA NA NA NA NA NA NA ND NA 0.275 0.215 0.534 0.00146 0.0311 0.00611 0.254 0.00989 ND ND 0.00157 0.00227 0.0378
MW-5 10/12/2023 NA NA NA NA NA NA NA NA ND NA 0.482 0.0140 0.445 ND 0.0755 0.0294 0.732 0.0203 ND ND ND 0.00109 0.00702
MW-5A-Dup 10/12/2023 NA NA NA NA NA NA NA NA ND NA 0.554 0.123 0.447 ND 0.0802 0.0323 0.737 0.0201 ND ND ND 0.00103 0.00726
MW-6 10/12/2023 NA NA NA NA NA NA NA NA ND NA 0.107 0.177 0.485 ND 0.0102 0.00224 0.136 0.00473 ND ND ND 0.00118 0.00197
MW-7 10/11/2023 NA NA NA NA NA NA NA NA ND NA 2.36 0.150 0.415 0.00161 0.373 0.0995 2.47 0.0572 0.00424 ND ND 0.00134 0.163
MW-8 10/11/2023 NA NA NA NA NA NA NA NA ND NA 0.537 0.256 0.499 ND 0.0737 0.0248 0.536 0.0111 ND ND ND ND 0.00633
MW-9 10/12/2023 NA NA NA NA NA NA NA NA ND NA ND 0.344 0.369 ND ND ND 0.00357 ND ND ND ND ND ND
MW-10 10/12/2023 NA NA NA NA NA NA NA NA ND NA ND 0.143 0.295 ND ND ND 0.00118 ND ND ND ND ND ND
Trip Blank 8/12/2023 NA NA NA NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND ND ND ND ND
Trip Blank 10/6/2023 NA NA NA NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND ND ND ND ND
Trip Blank 10/12/2023 NA NA NA NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND ND ND ND ND
Utah ISL 10 1 1 1 10 0.005 1
Utah RBCA Tier 1 SL 10 10 10 10 10 0.3 3
May 2023 EPA MCL 0.002 0.010 2 0.005 100 0.015 0.050 NS NS NS NS NS NS 0.005 NS 0.007 0.07 0.07 0.005 0.005 1 0.005 0.002
May 2023 EPA Tapwater 0.00063 0.000052 0.380 0.00018 NS 0.015 0.010 0.0094 NS NS NS NS NS 0.00046 0.0028 0.28 0.025 0.068 0.00085 0.011 1.10 0.00049 0.000019
* = TPH Oil and Grease HEM
Bold = Concentrations above Utah Initial Screening Level (ISL) and/or MCL
NA = Not Analyzed
NS = No Standard

Paxton SCR

APPENDIX B
Field Forms

Paxton SCR

APPENDIX C
Laboratory Reports
ANALYTICAL REPORT
November 22, 2024
Revised Report
Geosyntec Consultants - UT
Sample Delivery Group:L1757957
Samples Received:07/18/2024
Project Number:
Description:
Report To:Brian Smith
215 South State Street
Suite 500
Salt Lake City, UT 84111
Entire Report Reviewed By:
November 22, 2024
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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November 22, 2024
Chris Ward
Project Manager
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TABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 16
Cn: Case Narrative 20
Su: Summary Results 21
1664A Wet Chemistry 21
Sample Result Inorganic Analysis Data Sheet 22
L1757957-16 07/26/24 12:55 OGBAL1 22
BLANK(R4098874-1) WG2330367 07/26/24 12:55 OGBAL1 23
LCS(R4098874-2) WG2330367 07/26/24 12:55 OGBAL1 24
LCSD(R4098874-3) WG2330367 07/26/24 12:55 OGBAL1 25
MS(R4098874-4) WG2330367 07/26/24 12:55 OGBAL1 26
Blank 27
OGBAL1 WG2330367 27
Matrix Spike / Duplicate 28
WG2330367 MS(R4098874-4) 28
Laboratory Control Sample / Duplicate 29
WG2330367 LCS(R4098874-2) LCSD(R4098874-3) 29
Detection Limit Summary 30
1664A - GW 30
Analysis Log 31
OGBAL1 WG2330367 31
2540 G-2011 Total Solids 32
Sample Result Inorganic Analysis Data Sheet 33
L1757957-01 07/19/24 10:21 LOGBAL1 33
L1757957-02 07/19/24 10:21 LOGBAL1 34
L1757957-03 07/19/24 10:21 LOGBAL1 35
L1757957-04 07/19/24 10:05 LOGBAL1 36
L1757957-05 07/19/24 10:05 LOGBAL1 37
L1757957-06 07/19/24 10:05 LOGBAL1 38
L1757957-07 07/19/24 10:05 LOGBAL1 39
L1757957-08 07/19/24 10:05 LOGBAL1 40
L1757957-09 07/19/24 10:05 LOGBAL1 41
L1757957-10 07/19/24 10:05 LOGBAL1 42
L1757957-11 07/19/24 10:05 LOGBAL1 43
L1757957-12 07/19/24 10:05 LOGBAL1 44
L1757957-13 07/19/24 10:05 LOGBAL1 45
L1757957-14 07/19/24 09:45 LOGBAL1 46
L1757957-15 07/19/24 09:45 LOGBAL1 47
BLANK(R4096284-1) WG2326128 07/19/24 09:45 LOGBAL1 48
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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BLANK(R4096285-1) WG2326127 07/19/24 10:05 LOGBAL1 49
BLANK(R4096286-1) WG2326126 07/19/24 10:21 LOGBAL1 50
DUP(R4096284-3) WG2326128 07/19/24 09:45 LOGBAL1 51
DUP(R4096285-3) WG2326127 07/19/24 10:05 LOGBAL1 52
LCS(R4096284-2) WG2326128 07/19/24 09:45 LOGBAL1 53
LCS(R4096285-2) WG2326127 07/19/24 10:05 LOGBAL1 54
LCS(R4096286-2) WG2326126 07/19/24 10:21 LOGBAL1 55
DUP(R4096286-3) WG2326126 07/19/24 10:21 LOGBAL1 56
Blank 57
LOGBAL1 WG2326128 57
LOGBAL1 WG2326127 58
LOGBAL1 WG2326126 59
Laboratory Duplicate 60
WG2326128 DUP(R4096284-3) 60
WG2326127 DUP(R4096285-3) 61
WG2326126 DUP(R4096286-3) 62
Laboratory Control Sample / Duplicate 63
WG2326128 LCS(R4096284-2) 63
WG2326127 LCS(R4096285-2) 64
WG2326126 LCS(R4096286-2) 65
Detection Limit Summary 66
2540 G-2011 - Solid 66
Analysis Log 67
LOGBAL1 WG2326128 67
LOGBAL1 WG2326127 68
LOGBAL1 WG2326126 69
3511/8015 Semi-Volatile Organic Compounds (GC) 70
Surrogate Recovery 71
GW Surrogate Summary 71
Laboratory Control Sample / Duplicate 72
WG2330427 LCS(R4099988-2) LCSD(R4099988-3) 72
Method Blank 73
WG2330427 R4099988-1 SVGC27 07/29/24 16:07 73
Sample Result Summary Organic Analysis Data Sheet 74
L1757957-16 07/29/24 22:14 SVGC27 74
Retention Time of Single Component Analytes 75
SVGC27 05/30/24 02:22 75
Calibration Factor of Single Component Analytes 76
SVGC27 05/30/24 02:22 76
Calibration Verification Single Component Analytes 78
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SVGC27 05/30/24 05:28 78
SVGC27 07/30/24 00:16 79
Analytical Sequence 80
SVGC27 05/30/24 02:22 80
Detection Limit Summary 81
3511/8015 - GW 81
QC Result Summary Organic Analysis Data Sheet 82
BLANK(R4099988-1) WG2330427 07/29/24 16:07 SVGC27 82
LCS(R4099988-2) WG2330427 07/29/24 16:27 SVGC27 83
LCSD(R4099988-3) WG2330427 07/29/24 16:48 SVGC27 84
6010B Metals (ICP) 85
Sample Result Inorganic Analysis Data Sheet 86
L1757957-01 07/24/24 09:36 ICP17 86
L1757957-02 07/23/24 09:24 ICP17 87
L1757957-03 07/23/24 09:26 ICP17 88
L1757957-04 07/23/24 09:28 ICP17 89
L1757957-05 07/23/24 09:29 ICP17 90
L1757957-06 07/23/24 09:31 ICP17 91
L1757957-07 07/23/24 09:33 ICP17 92
L1757957-08 07/23/24 10:08 ICP17 93
L1757957-09 07/24/24 09:54 ICP17 94
L1757957-10 07/24/24 09:56 ICP17 95
L1757957-11 07/24/24 14:53 ICP17 96
L1757957-12 07/24/24 09:59 ICP17 97
L1757957-13 07/24/24 10:01 ICP17 98
L1757957-14 07/24/24 10:02 ICP17 99
L1757957-15 07/24/24 10:04 ICP17 100
L1757957-16 07/29/24 00:46 ICP16 101
BLANK(R4097314-1) WG2326410 07/23/24 08:43 ICP17 102
BLANK(R4097913-1) WG2326543 07/24/24 09:33 ICP17 103
BLANK(R4099537-1) WG2327640 07/29/24 00:17 ICP16 104
LCS(R4097314-2) WG2326410 07/23/24 08:44 ICP17 105
LCS(R4097913-2) WG2326543 07/24/24 09:34 ICP17 106
LCS(R4099537-2) WG2327640 07/29/24 00:19 ICP16 107
MS(R4097314-5) WG2326410 07/23/24 08:51 ICP17 108
MS(R4097913-5) WG2326543 07/24/24 09:41 ICP17 109
MS(R4099537-4) WG2327640 07/29/24 00:24 ICP16 110
MSD(R4097314-6) WG2326410 07/23/24 08:53 ICP17 111
MSD(R4097913-6) WG2326543 07/24/24 09:43 ICP17 112
MSD(R4099537-5) WG2327640 07/29/24 00:25 ICP16 113
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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PS(R4097314-4) WG2326410 07/23/24 08:49 ICP17 114
PS(R4097314-7) WG2326410 07/23/24 14:40 ICP17 115
PS(R4097913-4) WG2326543 07/24/24 09:39 ICP17 116
SD(R4097314-3) WG2326410 07/23/24 08:48 ICP17 117
SD(R4097913-3) WG2326543 07/24/24 09:38 ICP17 118
SD(R4099537-3) WG2327640 07/29/24 00:22 ICP16 119
Calibration Verification 120
ICP16 072824ICP16 120
ICP17 072324ICP17 122
ICP17 072424ICP17 125
Blank 127
ICP16 072824ICP16 127
ICP17 072324ICP17 129
ICP17 072424ICP17 132
ICP Interference Check Sample 134
ICP16 07/28/24 17:44 134
ICP16 07/28/24 22:22 135
ICP16 07/29/24 01:23 136
ICP17 07/23/24 07:58 137
ICP17 07/23/24 13:39 138
ICP17 07/23/24 15:26 139
ICP17 07/24/24 06:56 140
ICP17 07/24/24 13:58 141
ICP17 07/24/24 20:34 142
Matrix Spike / Duplicate 143
WG2326410 MS(R4097314-5) MSD(R4097314-6) 143
WG2326543 MS(R4097913-5) MSD(R4097913-6) 144
WG2327640 MS(R4099537-4) MSD(R4099537-5) 145
Post Digestion Spike 146
WG2326410 PS(R4097314-4) 146
WG2326410 PS(R4097314-7) 147
WG2326543 PS(R4097913-4) 148
Laboratory Control Sample / Duplicate 149
WG2326410 LCS(R4097314-2) 149
WG2326543 LCS(R4097913-2) 150
WG2327640 LCS(R4099537-2) 151
Serial Dilution 152
WG2326410 SD(R4097314-3) 152
WG2326543 SD(R4097913-3) 153
WG2327640 SD(R4099537-3) 154
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Detection Limit Summary 155
6010B - GW 155
6010B - Solid 156
Linear Dynamic Range 157
ICP16 01/25/24 15:25 157
ICP17 06/09/24 17:06 158
Analysis Log 159
ICP16 072824ICP16 07/28/24 17:05 159
ICP17 072324ICP17 07/23/24 07:38 160
ICP17 072424ICP17 07/24/24 06:36 162
Initial Calibration Recovery 163
ICP16 072824ICP16 07/28/24 17:05 163
ICP17 072324ICP17 07/23/24 07:38 166
ICP17 072424ICP17 07/24/24 06:36 169
Initial Calibration 172
ICP16 072824ICP16 07/28/24 17:05 172
ICP17 072324ICP17 07/23/24 07:38 173
ICP17 072424ICP17 07/24/24 06:36 174
7470A Mercury 175
Sample Result Inorganic Analysis Data Sheet 176
L1757957-16 07/20/24 23:52 CVAA9 176
BLANK(R4096472-1) WG2325902 07/20/24 22:52 CVAA9 177
LCS(R4096472-2) WG2325902 07/20/24 23:00 CVAA9 178
MS(R4096472-4) WG2325902 07/20/24 23:07 CVAA9 179
MSD(R4096472-5) WG2325902 07/20/24 23:10 CVAA9 180
SD(R4096472-3) WG2325902 07/20/24 23:05 CVAA9 181
Calibration Verification 182
CVAA9 072024CVAA9 WB 182
Blank 184
CVAA9 072024CVAA9 WB 184
Matrix Spike / Duplicate 186
WG2325902 MS(R4096472-4) MSD(R4096472-5) 186
Laboratory Control Sample / Duplicate 187
WG2325902 LCS(R4096472-2) 187
Serial Dilution 188
WG2325902 SD(R4096472-3) 188
Detection Limit Summary 189
7470A - GW 189
Linear Dynamic Range 190
CVAA9 07/10/23 14:11 190
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Analysis Log 191
CVAA9 072024CVAA9 WB 07/20/24 18:56 191
Initial Calibration Recovery 192
CVAA9 072024CVAA9 WB 07/20/24 18:56 192
Initial Calibration 195
CVAA9 072024CVAA9 WB 07/20/24 18:56 195
7471A Mercury 196
Sample Result Inorganic Analysis Data Sheet 197
L1757957-01 07/23/24 14:32 CVAA10 197
L1757957-02 07/21/24 18:50 CVAA7 198
L1757957-03 07/23/24 14:47 CVAA10 199
L1757957-04 07/23/24 14:55 CVAA10 200
L1757957-05 07/23/24 14:58 CVAA10 201
L1757957-06 07/23/24 15:00 CVAA10 202
L1757957-07 07/23/24 15:03 CVAA10 203
L1757957-08 07/23/24 15:06 CVAA10 204
L1757957-09 07/23/24 15:08 CVAA10 205
L1757957-10 07/23/24 15:16 CVAA10 206
L1757957-11 07/23/24 15:18 CVAA10 207
L1757957-12 07/23/24 15:21 CVAA10 208
L1757957-13 07/23/24 15:23 CVAA10 209
L1757957-14 07/23/24 15:26 CVAA10 210
L1757957-15 07/23/24 15:29 CVAA10 211
BLANK(R4096524-1) WG2326415 07/21/24 17:30 CVAA7 212
BLANK(R4097489-1) WG2326412 07/23/24 14:27 CVAA10 213
LCS(R4096524-2) WG2326415 07/21/24 17:32 CVAA7 214
LCS(R4097489-2) WG2326412 07/23/24 14:29 CVAA10 215
MS(R4096524-4) WG2326415 07/21/24 17:40 CVAA7 216
MS(R4097489-4) WG2326412 07/23/24 14:37 CVAA10 217
MSD(R4096524-5) WG2326415 07/21/24 17:47 CVAA7 218
MSD(R4097489-5) WG2326412 07/23/24 14:45 CVAA10 219
SD(R4096524-3) WG2326415 07/21/24 17:37 CVAA7 220
SD(R4097489-3) WG2326412 07/23/24 14:35 CVAA10 221
Calibration Verification 222
CVAA7 072124CVAA7 S 222
CVAA10 072324CVAA10 SB 225
Blank 227
CVAA7 072124CVAA7 S 227
CVAA10 072324CVAA10 SB 229
Matrix Spike / Duplicate 231
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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WG2326415 MS(R4096524-4) MSD(R4096524-5) 231
WG2326412 MS(R4097489-4) MSD(R4097489-5) 232
Laboratory Control Sample / Duplicate 233
WG2326415 LCS(R4096524-2) 233
WG2326412 LCS(R4097489-2) 234
Serial Dilution 235
WG2326415 SD(R4096524-3) 235
WG2326412 SD(R4097489-3) 236
Detection Limit Summary 237
7471A - Solid 237
Linear Dynamic Range 238
CVAA7 06/27/19 15:34 238
Analysis Log 239
CVAA7 072124CVAA7 S 07/21/24 15:16 239
CVAA10 072324CVAA10 SB 07/23/24 13:46 240
Initial Calibration Recovery 241
CVAA7 072124CVAA7 S 07/21/24 15:16 241
CVAA10 072324CVAA10 SB 07/23/24 13:46 244
Initial Calibration 247
CVAA7 072124CVAA7 S 07/21/24 15:16 247
CVAA10 072324CVAA10 SB 07/23/24 13:46 248
8015 Semi-Volatile Organic Compounds (GC) 249
Surrogate Recovery 250
Solid Surrogate Summary 250
Matrix Spike / Duplicate 251
WG2331405 MS(R4100074-3) MSD(R4100074-4) 251
Laboratory Control Sample / Duplicate 252
WG2331405 LCS(R4100074-2) 252
Method Blank 253
WG2331405 R4100074-1 SVGC50 07/29/24 09:29 253
Sample Result Summary Organic Analysis Data Sheet 254
L1757957-01 07/29/24 11:46 SVGC50 254
L1757957-02 07/29/24 11:21 SVGC50 255
L1757957-03 07/29/24 10:56 SVGC50 256
L1757957-04 07/29/24 13:00 SVGC50 257
L1757957-05 07/29/24 12:23 SVGC50 258
L1757957-06 07/29/24 14:28 SVGC50 259
L1757957-07 07/29/24 12:36 SVGC50 260
L1757957-08 07/29/24 13:13 SVGC50 261
L1757957-09 07/29/24 13:38 SVGC50 262
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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L1757957-10 07/29/24 14:03 SVGC50 263
L1757957-11 07/29/24 14:15 SVGC50 264
L1757957-12 07/29/24 13:50 SVGC50 265
L1757957-13 07/30/24 12:01 SVGC50 266
L1757957-14 07/29/24 12:48 SVGC50 267
L1757957-15 07/29/24 11:09 SVGC50 268
Retention Time of Single Component Analytes 269
SVGC50 03/21/24 10:00 269
SVGC50 03/21/24 10:00 270
Calibration Factor of Single Component Analytes 271
SVGC50 03/21/24 10:00 271
SVGC50 03/21/24 10:00 273
Calibration Verification Single Component Analytes 275
SVGC50 03/21/24 14:43 275
SVGC50 07/29/24 08:55 276
SVGC50 07/29/24 15:17 277
SVGC50 07/29/24 22:40 278
SVGC50 07/30/24 10:18 279
SVGC50 07/30/24 16:34 280
Analytical Sequence 281
SVGC50 03/21/24 10:00 281
SVGC50 03/21/24 10:00 282
Detection Limit Summary 283
8015 - Solid 283
QC Result Summary Organic Analysis Data Sheet 284
BLANK(R4100074-1) WG2331405 07/29/24 09:29 SVGC50 284
LCS(R4100074-2) WG2331405 07/29/24 09:42 SVGC50 285
MS(R4100074-3) WG2331405 07/29/24 11:58 SVGC50 286
MSD(R4100074-4) WG2331405 07/29/24 12:11 SVGC50 287
8015D/GRO Volatile Organic Compounds (GC) 288
Surrogate Recovery 289
GW Surrogate Summary 289
Solid Surrogate Summary 290
Matrix Spike / Duplicate 291
WG2327971 MS(R4098551-3) MSD(R4098551-4) 291
WG2330774 MS(R4100115-3) MSD(R4100115-4) 292
Laboratory Control Sample / Duplicate 293
WG2329459 LCS(R4098253-1) 293
WG2329941 LCS(R4098321-1) LCSD(R4098321-2) 294
WG2329829 LCS(R4098479-1) LCSD(R4098479-2) 295
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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WG2327971 LCS(R4098551-1) 296
WG2328825 LCS(R4098862-1) 297
WG2330767 LCS(R4100114-1) 298
WG2330774 LCS(R4100115-1) 299
Method Blank 300
WG2327971 R4098551-2 VOCGC10 07/23/24 12:49 300
WG2328825 R4098862-2 VOCGC10 07/24/24 10:54 301
WG2329829 R4098479-3 VOCGC10 07/25/24 12:59 302
WG2329459 R4098253-2 VOCGC15 07/24/24 18:25 303
WG2330767 R4100114-2 VOCGC15 07/28/24 11:14 304
WG2330774 R4100115-2 VOCGC15 07/28/24 11:14 305
WG2329941 R4098321-3 VOCGC17 07/25/24 11:56 306
Internal Standard & Retention Time 307
VOCGC10 07/23/24 12:03 307
VOCGC10 07/24/24 10:08 308
VOCGC10 07/25/24 11:50 309
VOCGC15 07/24/24 16:45 310
VOCGC15 07/28/24 09:39 311
VOCGC17 07/25/24 10:04 312
Sample Result Summary Organic Analysis Data Sheet 313
L1757957-01 07/28/24 17:12 VOCGC15 313
L1757957-02 07/28/24 14:51 VOCGC15 314
L1757957-03 07/24/24 13:40 VOCGC10 315
L1757957-04 07/25/24 13:02 VOCGC17 316
L1757957-05 07/24/24 23:45 VOCGC15 317
L1757957-06 07/25/24 13:21 VOCGC17 318
L1757957-07 07/25/24 00:08 VOCGC15 319
L1757957-08 07/25/24 13:40 VOCGC17 320
L1757957-09 07/25/24 14:00 VOCGC17 321
L1757957-10 07/25/24 14:19 VOCGC17 322
L1757957-11 07/25/24 14:39 VOCGC17 323
L1757957-12 07/25/24 14:52 VOCGC10 324
L1757957-13 07/25/24 15:15 VOCGC10 325
L1757957-14 07/25/24 15:38 VOCGC10 326
L1757957-15 07/25/24 16:01 VOCGC10 327
L1757957-16 07/23/24 17:16 VOCGC10 328
Retention Time of Single Component Analytes 329
VOCGC10 06/04/24 17:40 329
VOCGC15 06/26/24 14:42 330
VOCGC17 01/30/24 00:30 331
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Calibration Factor of Single Component Analytes 332
VOCGC10 06/04/24 17:40 332
VOCGC15 06/26/24 14:42 334
VOCGC17 01/30/24 00:30 336
Calibration Verification Single Component Analytes 338
VOCGC10 06/05/24 02:00 338
VOCGC10 07/23/24 12:03 339
VOCGC10 07/24/24 10:08 340
VOCGC10 07/25/24 11:50 341
VOCGC15 06/26/24 22:05 342
VOCGC15 07/24/24 16:45 343
VOCGC15 07/28/24 09:39 344
VOCGC17 01/30/24 03:23 345
VOCGC17 07/25/24 10:04 346
Analytical Sequence 347
VOCGC10 06/04/24 17:40 347
VOCGC15 06/26/24 14:42 349
VOCGC17 01/30/24 00:30 350
Detection Limit Summary 351
8015D/GRO - GW 351
8015D/GRO - Solid 352
QC Result Summary Organic Analysis Data Sheet 353
BLANK(R4098253-2) WG2329459 07/24/24 18:25 VOCGC15 353
BLANK(R4098321-3) WG2329941 07/25/24 11:56 VOCGC17 354
BLANK(R4098479-3) WG2329829 07/25/24 12:59 VOCGC10 355
BLANK(R4098551-2) WG2327971 07/23/24 12:49 VOCGC10 356
BLANK(R4098862-2) WG2328825 07/24/24 10:54 VOCGC10 357
BLANK(R4100114-2) WG2330767 07/28/24 11:14 VOCGC15 358
BLANK(R4100115-2) WG2330774 07/28/24 11:14 VOCGC15 359
LCS(R4098253-1) WG2329459 07/24/24 17:08 VOCGC15 360
LCS(R4098321-1) WG2329941 07/25/24 10:23 VOCGC17 361
LCS(R4098479-1) WG2329829 07/25/24 11:50 VOCGC10 362
LCS(R4098551-1) WG2327971 07/23/24 12:03 VOCGC10 363
LCS(R4098862-1) WG2328825 07/24/24 10:08 VOCGC10 364
LCS(R4100114-1) WG2330767 07/28/24 10:03 VOCGC15 365
LCS(R4100115-1) WG2330774 07/28/24 10:03 VOCGC15 366
LCSD(R4098321-2) WG2329941 07/25/24 10:43 VOCGC17 367
LCSD(R4098479-2) WG2329829 07/25/24 12:13 VOCGC10 368
MS(R4098551-3) WG2327971 07/24/24 00:06 VOCGC10 369
MS(R4100115-3) WG2330774 07/28/24 17:35 VOCGC15 370
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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MSD(R4098551-4) WG2327971 07/24/24 00:28 VOCGC10 371
MSD(R4100115-4) WG2330774 07/28/24 17:59 VOCGC15 372
8260B Volatile Organic Compounds (GC/MS) 373
Surrogate Recovery 374
GW Surrogate Summary 374
Solid Surrogate Summary 375
Matrix Spike / Duplicate 376
WG2329486 MS(R4098455-4) MSD(R4098455-5) 376
Laboratory Control Sample / Duplicate 378
WG2327390 LCS(R4097932-1) LCSD(R4097932-2) 378
WG2329566 LCS(R4098226-1) 380
WG2329486 LCS(R4098455-1) LCSD(R4098455-2) 382
WG2329510 LCS(R4098753-1) 384
Method Blank 386
WG2327390 R4097932-3 VOCMS21 07/21/24 23:25 386
WG2329566 R4098226-2 VOCMS56 07/24/24 21:48 387
WG2329510 R4098753-2 VOCMS56 07/25/24 08:44 388
WG2329486 R4098455-3 VOCMS58 07/25/24 10:05 389
GC/MS Performance Check 390
VOCMS21 071024 07/10/24 10:50 390
VOCMS21 071024A 07/10/24 10:50 391
VOCMS21 072124 07/21/24 21:27 392
VOCMS56 070824 07/08/24 19:11 393
VOCMS56 072424A 07/24/24 19:54 394
VOCMS56 072524 07/25/24 06:49 395
VOCMS58 071824 07/19/24 03:22 396
VOCMS58 072524 07/25/24 08:11 397
Internal Standard & Retention Time 398
VOCMS21 07/21/24 21:51 398
VOCMS56 07/24/24 20:32 399
VOCMS56 07/25/24 07:27 400
VOCMS58 07/25/24 08:30 401
Sample Result Summary Organic Analysis Data Sheet 402
L1757957-01 07/25/24 15:51 VOCMS58 402
L1757957-02 07/25/24 12:21 VOCMS58 404
L1757957-03 07/25/24 12:40 VOCMS58 406
L1757957-04 07/25/24 16:10 VOCMS58 408
L1757957-05 07/25/24 12:59 VOCMS58 410
L1757957-06 07/25/24 16:29 VOCMS58 412
L1757957-07 07/25/24 13:18 VOCMS58 414
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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L1757957-08 07/25/24 16:48 VOCMS58 416
L1757957-09 07/25/24 15:58 VOCMS56 418
L1757957-10 07/25/24 16:17 VOCMS56 420
L1757957-11 07/25/24 16:36 VOCMS56 422
L1757957-12 07/25/24 14:34 VOCMS56 424
L1757957-13 07/25/24 00:48 VOCMS56 426
L1757957-14 07/25/24 01:07 VOCMS56 428
L1757957-15 07/25/24 01:26 VOCMS56 430
L1757957-16 07/22/24 01:20 VOCMS21 432
L1757957-17 07/22/24 00:33 VOCMS21 434
GC/MS Initial Calibration 436
VOCMS21 07/10/24 11:59 436
VOCMS56 07/08/24 19:30 440
VOCMS58 07/19/24 04:01 444
GC/MS Calibration Verification 448
VOCMS21 07/10/24 16:17 448
VOCMS21 07/10/24 17:04 450
VOCMS21 07/21/24 21:51 451
VOCMS56 07/08/24 23:37 453
VOCMS56 07/08/24 23:56 455
VOCMS56 07/24/24 20:32 456
VOCMS56 07/25/24 07:27 458
VOCMS58 07/19/24 08:27 460
VOCMS58 07/19/24 09:05 462
VOCMS58 07/25/24 08:30 463
Analytical Sequence 465
VOCMS21 07/10/24 11:59 465
VOCMS56 07/08/24 19:30 466
VOCMS58 07/19/24 04:01 468
Detection Limit Summary 469
8260B - GW 469
8260B - Solid 471
QC Result Summary Organic Analysis Data Sheet 473
BLANK(R4097932-3) WG2327390 07/21/24 23:25 VOCMS21 473
BLANK(R4098226-2) WG2329566 07/24/24 21:48 VOCMS56 475
BLANK(R4098455-3) WG2329486 07/25/24 10:05 VOCMS58 477
BLANK(R4098753-2) WG2329510 07/25/24 08:44 VOCMS56 479
LCS(R4097932-1) WG2327390 07/21/24 21:51 VOCMS21 481
LCS(R4098226-1) WG2329566 07/24/24 20:32 VOCMS56 483
LCS(R4098455-1) WG2329486 07/25/24 08:30 VOCMS58 485
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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LCS(R4098753-1) WG2329510 07/25/24 07:27 VOCMS56 487
LCSD(R4097932-2) WG2327390 07/21/24 22:14 VOCMS21 489
LCSD(R4098455-2) WG2329486 07/25/24 08:49 VOCMS58 491
MS(R4098455-4) WG2329486 07/25/24 17:45 VOCMS58 493
MSD(R4098455-5) WG2329486 07/25/24 18:04 VOCMS58 495
9071B Wet Chemistry 497
Sample Result Inorganic Analysis Data Sheet 498
L1757957-01 07/25/24 23:08 OGBAL1 498
L1757957-02 07/25/24 23:08 OGBAL1 499
L1757957-03 07/25/24 23:08 OGBAL1 500
L1757957-04 07/25/24 23:08 OGBAL1 501
L1757957-05 07/25/24 23:08 OGBAL1 502
L1757957-06 07/25/24 23:08 OGBAL1 503
L1757957-07 07/25/24 23:08 OGBAL1 504
L1757957-08 07/25/24 23:08 OGBAL1 505
L1757957-09 07/25/24 23:08 OGBAL1 506
L1757957-10 07/25/24 23:08 OGBAL1 507
L1757957-11 07/25/24 23:08 OGBAL1 508
L1757957-12 07/25/24 23:08 OGBAL1 509
L1757957-13 07/25/24 23:08 OGBAL1 510
L1757957-14 07/25/24 23:08 OGBAL1 511
L1757957-15 07/25/24 23:08 OGBAL1 512
BLANK(R4098647-1) WG2330146 07/25/24 23:08 OGBAL1 513
LCS(R4098647-2) WG2330146 07/25/24 23:08 OGBAL1 514
DUP(R4098647-4) WG2330146 07/25/24 23:08 OGBAL1 515
LCSD(R4098647-3) WG2330146 07/25/24 23:08 OGBAL1 516
MS(R4098647-5) WG2330146 07/25/24 23:08 OGBAL1 517
MSD(R4098647-6) WG2330146 07/25/24 23:08 OGBAL1 518
Blank 519
OGBAL1 WG2330146 519
Matrix Spike / Duplicate 520
WG2330146 MS(R4098647-5) MSD(R4098647-6) 520
Laboratory Duplicate 521
WG2330146 DUP(R4098647-4) 521
Laboratory Control Sample / Duplicate 522
WG2330146 LCS(R4098647-2) LCSD(R4098647-3) 522
Detection Limit Summary 523
9071B - Solid 523
Analysis Log 524
OGBAL1 WG2330146 524
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Gl: Glossary of Terms 525
Al: Accreditations & Locations 527
Sc: Sample Chain of Custody 528
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-3 (0-6) L1757957-01 Solid Jessica Welch 07/16/24 09:30 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326126 1 07/19/24 10:08 07/19/24 10:21 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 14:32 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 09:36 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2330774 27.5 07/16/24 09:30 07/28/24 17:12 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1.1 07/16/24 09:30 07/25/24 15:51 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 10 07/28/24 08:04 07/29/24 11:46 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-3 (6-12) L1757957-02 Solid Jessica Welch 07/16/24 10:00 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326126 1 07/19/24 10:08 07/19/24 10:21 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326415 1 07/20/24 15:03 07/21/24 18:50 SDG Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 09:24 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2330767 26.3 07/16/24 10:00 07/28/24 14:51 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1.05 07/16/24 10:00 07/25/24 12:21 JBE Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 1 07/28/24 08:04 07/29/24 11:21 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-30 (6-12) L1757957-03 Solid Jessica Welch 07/16/24 13:30 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326126 1 07/19/24 10:08 07/19/24 10:21 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 14:47 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 09:26 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2328825 27.5 07/16/24 13:30 07/24/24 13:40 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1.1 07/16/24 13:30 07/25/24 12:40 JBE Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 2 07/28/24 08:04 07/29/24 10:56 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-9 (0-6) L1757957-04 Solid Jessica Welch 07/16/24 10:34 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 14:55 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 09:28 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329941 25.8 07/16/24 10:34 07/25/24 13:02 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1.03 07/16/24 10:34 07/25/24 16:10 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 10 07/28/24 08:04 07/29/24 13:00 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-8 (0-6) L1757957-05 Solid Jessica Welch 07/16/24 10:58 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 14:58 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 09:29 DJS Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 16 of 530
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Geosyntec Consultants - UT L1757957 11/22/24 14:34 16 of 530
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-8 (0-6) L1757957-05 Solid Jessica Welch 07/16/24 10:58 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329459 25 07/16/24 10:58 07/24/24 23:45 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1 07/16/24 10:58 07/25/24 12:59 JBE Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 10 07/28/24 08:04 07/29/24 12:23 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-7 (0-6) L1757957-06 Solid Jessica Welch 07/16/24 11:20 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:00 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 09:31 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329941 34.3 07/16/24 11:20 07/25/24 13:21 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1.37 07/16/24 11:20 07/25/24 16:29 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 250 07/28/24 08:04 07/29/24 14:28 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-7 (6-12) L1757957-07 Solid Jessica Welch 07/16/24 11:35 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:03 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 09:33 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329459 30.3 07/16/24 11:35 07/25/24 00:08 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1.21 07/16/24 11:35 07/25/24 13:18 JBE Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 10 07/28/24 08:04 07/29/24 12:36 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-6 (0-6) L1757957-08 Solid Jessica Welch 07/16/24 11:55 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:06 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326410 1 07/22/24 06:40 07/23/24 10:08 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329941 25 07/16/24 11:55 07/25/24 13:40 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329486 1 07/16/24 11:55 07/25/24 16:48 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 50 07/28/24 08:04 07/29/24 13:13 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-5 (0-6) L1757957-09 Solid Jessica Welch 07/16/24 13:15 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:08 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 09:54 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329941 25 07/16/24 13:15 07/25/24 14:00 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329510 1 07/16/24 13:15 07/25/24 15:58 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 50 07/28/24 08:04 07/29/24 13:38 KKS Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 17 of 530
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Geosyntec Consultants - UT L1757957 11/22/24 14:34 17 of 530
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-4 (0-6) L1757957-10 Solid Jessica Welch 07/16/24 13:30 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:16 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 09:56 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329941 28.5 07/16/24 13:30 07/25/24 14:19 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329510 1.14 07/16/24 13:30 07/25/24 16:17 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 250 07/28/24 08:04 07/29/24 14:03 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-31 (0-6) L1757957-11 Solid Jessica Welch 07/16/24 14:40 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:18 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 5 07/23/24 22:02 07/24/24 14:53 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329941 30.3 07/16/24 14:40 07/25/24 14:39 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329510 1.21 07/16/24 14:40 07/25/24 16:36 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 250 07/28/24 08:04 07/29/24 14:15 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-2 (0-6) L1757957-12 Solid Jessica Welch 07/16/24 13:55 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:21 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 09:59 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329829 26.8 07/16/24 13:55 07/25/24 14:52 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329510 1.06 07/16/24 13:55 07/25/24 14:34 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 25 07/28/24 08:04 07/29/24 13:50 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-1 (0-6) L1757957-13 Solid Jessica Welch 07/16/24 14:10 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326127 1 07/19/24 09:50 07/19/24 10:05 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:23 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 10:01 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329829 28.5 07/16/24 14:10 07/25/24 15:15 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329566 1.22 07/16/24 14:10 07/25/24 00:48 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 20 07/28/24 08:04 07/30/24 12:01 JAS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-1 (6-12) L1757957-14 Solid Jessica Welch 07/16/24 14:25 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326128 1 07/19/24 09:34 07/19/24 09:45 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:26 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 10:02 DJS Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-1 (6-12) L1757957-14 Solid Jessica Welch 07/16/24 14:25 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329829 28.5 07/16/24 14:25 07/25/24 15:38 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329566 1.19 07/16/24 14:25 07/25/24 01:07 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 10 07/28/24 08:04 07/29/24 12:48 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-1 (6-12) L1757957-15 Solid Jessica Welch 07/16/24 14:41 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2326128 1 07/19/24 09:34 07/19/24 09:45 KDW Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2330146 1 07/25/24 16:30 07/25/24 23:08 DAL Mt. Juliet, TN
Mercury by Method 7471A WG2326412 1 07/21/24 21:10 07/23/24 15:29 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2326543 1 07/23/24 22:02 07/24/24 10:04 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329829 25 07/16/24 14:41 07/25/24 16:01 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2329566 1 07/16/24 14:41 07/25/24 01:26 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2331405 2 07/28/24 08:04 07/29/24 11:09 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
EB-1-071624 L1757957-16 GW Jessica Welch 07/16/24 15:00 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2330367 1 07/26/24 03:49 07/26/24 12:55 MAB Mt. Juliet, TN
Mercury by Method 7470A WG2325902 1 07/19/24 18:14 07/20/24 23:52 AKB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2327640 1 07/27/24 10:37 07/29/24 00:46 DJS Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2327971 1 07/23/24 17:16 07/23/24 17:16 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2327390 1 07/22/24 01:20 07/22/24 01:20 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2330427 1 07/26/24 09:07 07/29/24 22:14 TJD Mt. Juliet, TN
Collected by Collected date/time Received date/time
TRIP BLANK L1757957-17 GW Jessica Welch 07/16/24 00:00 07/18/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG2327390 1 07/22/24 00:33 07/22/24 00:33 JAH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 08/01/24 11:52
Level III Report - Version 2: 08/01/24 13:14
Level II Report - Version 3: 11/22/24 14:27
Project Narrative
Report reissued 11/22 for updated sample depth on -10
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Chris Ward
Project Manager
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1664A Wet Chemistry
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:20 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/26/24 03:49
Analytical Batch:WG2330367 Analysis Date/Time:07/26/24 12:55
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:880 ml
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.32 5.68
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098874-1
Lab Sample ID:R4098874-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/26/24 03:48
Analytical Batch:WG2330367 Analysis Date/Time:07/26/24 12:55
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098874-2
Lab Sample ID:R4098874-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:04 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/26/24 03:48
Analytical Batch:WG2330367 Analysis Date/Time:07/26/24 12:55
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)35.2 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098874-3
Lab Sample ID:R4098874-3 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:05 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/26/24 03:48
Analytical Batch:WG2330367 Analysis Date/Time:07/26/24 12:55
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)36.8 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098874-4
Lab Sample ID:R4098874-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 15:00
Lab File ID:06 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/26/24 03:49
Analytical Batch:WG2330367 Analysis Date/Time:07/26/24 12:55
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:820 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)41.3 1.16 5.00
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:_______________
Instrument ID:OGBAL1 Calibration (end) date/time:_______________
Analytical Method:1664A Analytical Run:WG2330367
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte mg/l
OIL & GREASE
(HEXANE EXTR)U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4098874-4
L1757957-16 _______________
MS Sample / File ID:R4098874-4 / 06 SDG:L1757957
MSD Sample / File ID:_______________Analytical Batch:WG2330367
OS Sample / File ID:L1757957-16 / 20 Matrix:GW
Instrument ID:OGBAL1
Analytical Method:1664A
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 U 41.3 103 1 78.0 - 114
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098874-2
RECOVERY R4098874-3
L1757957-16
LCS Sample / File ID:R4098874-2 / 04 SDG:L1757957
LCSD Sample / File ID:R4098874-3 / 05 Analytical Batch:WG2330367
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:1664A Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 35.2 36.8 88.0 92.0 78.0 - 114 4.44 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16 Analytical Method:1664A
Matrix:GW Prep Method:1664A
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Oil & Grease (Hexane Extr)1.32 5.68
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:1664A
Instrument ID:OGBAL1 Calibration Start Date:_______________
Analytical Run:WG2330367 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4098874-1 01 07/26/24 12:55 1 WG2330367
LCS R4098874-2 04 07/26/24 12:55 1 WG2330367
LCSD R4098874-3 05 07/26/24 12:55 1 WG2330367
MS R4098874-4 06 07/26/24 12:55 1 WG2330367
EB-1-071624 L1757957-16 20 07/26/24 12:55 1 WG2330367
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2540 G-2011 Total Solids
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:11 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 10:08
Analytical Batch:WG2326126 Analysis Date/Time:07/19/24 10:21
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.452 g
Total Solids (%):98.6 Final Wt/Vol:11.31 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 98.6
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:12 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 10:08
Analytical Batch:WG2326126 Analysis Date/Time:07/19/24 10:21
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.393 g
Total Solids (%):92.0 Final Wt/Vol:8.744 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 92.0
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:13 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 10:08
Analytical Batch:WG2326126 Analysis Date/Time:07/19/24 10:21
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.158 g
Total Solids (%):92.7 Final Wt/Vol:9.512 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 92.7
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:04 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.75 g
Total Solids (%):97.8 Final Wt/Vol:9.564 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 97.8
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:05 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.305 g
Total Solids (%):98.2 Final Wt/Vol:11.129 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 98.2
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:06 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.56 g
Total Solids (%):94.0 Final Wt/Vol:9.065 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 94.0
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:07 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.578 g
Total Solids (%):93.8 Final Wt/Vol:9.067 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 93.8
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:08 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.41 g
Total Solids (%):98.1 Final Wt/Vol:10.241 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 98.1
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:09 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.657 g
Total Solids (%):98.7 Final Wt/Vol:11.518 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 98.7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:10 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:12.042 g
Total Solids (%):97.3 Final Wt/Vol:11.748 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 97.3
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:11 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.073 g
Total Solids (%):97.2 Final Wt/Vol:10.802 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 97.2
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:12 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.409 g
Total Solids (%):95.1 Final Wt/Vol:9.964 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 95.1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:13 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:50
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.758 g
Total Solids (%):93.1 Final Wt/Vol:10.106 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 93.1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:04 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:34
Analytical Batch:WG2326128 Analysis Date/Time:07/19/24 09:45
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.556 g
Total Solids (%):91.0 Final Wt/Vol:9.72 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 91.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:05 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:34
Analytical Batch:WG2326128 Analysis Date/Time:07/19/24 09:45
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.999 g
Total Solids (%):85.6 Final Wt/Vol:8.745 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 85.6
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096284-1
Lab Sample ID:R4096284-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:32
Analytical Batch:WG2326128 Analysis Date/Time:07/19/24 09:45
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.313 g
Total Solids (%):_______________Final Wt/Vol:1.314 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096285-1
Lab Sample ID:R4096285-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:48
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.321 g
Total Solids (%):_______________Final Wt/Vol:1.321 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.000
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096286-1
Lab Sample ID:R4096286-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 10:05
Analytical Batch:WG2326126 Analysis Date/Time:07/19/24 10:21
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.306 g
Total Solids (%):_______________Final Wt/Vol:1.307 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096284-3
Lab Sample ID:R4096284-3 SDG:L1757957
Client Sample ID:DUP Collected Date/Time:07/16/24 10:50
Lab File ID:02 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:32
Analytical Batch:WG2326128 Analysis Date/Time:07/19/24 09:45
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.315 g
Total Solids (%):79.6 Final Wt/Vol:6.911 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 80.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096285-3
Lab Sample ID:R4096285-3 SDG:L1757957
Client Sample ID:DUP Collected Date/Time:07/16/24 14:40
Lab File ID:02 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:48
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.309 g
Total Solids (%):97.2 Final Wt/Vol:10.073 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 97.4
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096284-2
Lab Sample ID:R4096284-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:32
Analytical Batch:WG2326128 Analysis Date/Time:07/19/24 09:45
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.311 g
Total Solids (%):_______________Final Wt/Vol:6.311 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096285-2
Lab Sample ID:R4096285-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 09:48
Analytical Batch:WG2326127 Analysis Date/Time:07/19/24 10:05
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.316 g
Total Solids (%):_______________Final Wt/Vol:6.315 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096286-2
Lab Sample ID:R4096286-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 10:05
Analytical Batch:WG2326126 Analysis Date/Time:07/19/24 10:21
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.314 g
Total Solids (%):_______________Final Wt/Vol:6.314 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096286-3
Lab Sample ID:R4096286-3 SDG:L1757957
Client Sample ID:DUP Collected Date/Time:07/16/24 09:30
Lab File ID:02 Received Date/Time:07/18/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:07/19/24 10:05
Analytical Batch:WG2326126 Analysis Date/Time:07/19/24 10:21
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:6.931 g
Total Solids (%):98.6 Final Wt/Vol:6.842 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 98.4
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2326128
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2326127
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.000
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2326126
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6-IN DUPLICATES SAMPLE NO.:
L1757957-14,15 R4096284-3
DUP Sample / File ID:R4096284-3 / 02 SDG:L1757957
OS Sample / File ID:L1757964-04 / 10 Analytical Batch:WG2326128
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 79.6 80.0 0.415 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6-IN DUPLICATES SAMPLE NO.:
L1757957-04,05,06,07,08,09,10,11,12,13 R4096285-3
DUP Sample / File ID:R4096285-3 / 02 SDG:L1757957
OS Sample / File ID:L1757957-11 / 11 Analytical Batch:WG2326127
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 97.2 97.4 0.151 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6-IN DUPLICATES SAMPLE NO.:
L1757957-01,02,03 R4096286-3
DUP Sample / File ID:R4096286-3 / 02 SDG:L1757957
OS Sample / File ID:L1757957-01 / 11 Analytical Batch:WG2326126
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 98.6 98.4 0.184 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4096284-2
RECOVERY _______________
L1757957-14,15
LCS Sample / File ID:R4096284-2 / 03 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326128
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.0 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4096285-2
RECOVERY _______________
L1757957-04,05,06,07,08,09,10,11,12,13
LCS Sample / File ID:R4096285-2 / 03 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326127
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.0 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4096286-2
RECOVERY _______________
L1757957-01,02,03
LCS Sample / File ID:R4096286-2 / 03 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326126
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.0 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:2540 G-2011
Matrix:Solid Prep Method:SM 2540 G
Analyte CAS Wavelength Mass MDL RDL
%%
Total Solids TSOLIDS
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2326128 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4096284-1 01 07/19/24 09:45 1 WG2326128
DUP R4096284-3 02 07/19/24 09:45 1 WG2326128
LCS R4096284-2 03 07/19/24 09:45 1 WG2326128
OS L1757964-04 10 07/19/24 09:45
SS-1 (6-12)L1757957-15 05 07/19/24 09:45 1 WG2326128
S-1 (6-12)L1757957-14 04 07/19/24 09:45 1 WG2326128
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2326127 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4096285-1 01 07/19/24 10:05 1 WG2326127
DUP R4096285-3 02 07/19/24 10:05 1 WG2326127
LCS R4096285-2 03 07/19/24 10:05 1 WG2326127
S-6 (0-6)L1757957-08 08 07/19/24 10:05 1 WG2326127
S-9 (0-6)L1757957-04 04 07/19/24 10:05 1 WG2326127
S-5 (0-6)L1757957-09 09 07/19/24 10:05 1 WG2326127
S-4 (0-6)L1757957-10 10 07/19/24 10:05 1 WG2326127
S-2 (0-6)L1757957-12 12 07/19/24 10:05 1 WG2326127
S-1 (0-6)L1757957-13 13 07/19/24 10:05 1 WG2326127
S-31 (0-6)L1757957-11 11 07/19/24 10:05 1 WG2326127
S-8 (0-6)L1757957-05 05 07/19/24 10:05 1 WG2326127
S-7 (0-6)L1757957-06 06 07/19/24 10:05 1 WG2326127
S-7 (6-12)L1757957-07 07 07/19/24 10:05 1 WG2326127
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2326126 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4096286-1 01 07/19/24 10:21 1 WG2326126
DUP R4096286-3 02 07/19/24 10:21 1 WG2326126
LCS R4096286-2 03 07/19/24 10:21 1 WG2326126
S-3 (0-6)L1757957-01 11 07/19/24 10:21 1 WG2326126
S-30 (6-12)L1757957-03 13 07/19/24 10:21 1 WG2326126
S-3 (6-12)L1757957-02 12 07/19/24 10:21 1 WG2326126
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3511/8015 Semi-Volatile Organic Compounds (GC)
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2A-OR SURROGATE RECOVERY
Analytical Method:3511/8015 SDG:L1757957
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
EB-1-071624 L1757957-16 SVGC27 0729_040 90.5 0
BLANK R4099988-1 SVGC27 0729_022 96.0 0
LCS R4099988-2 SVGC27 0729_023 96.5 0
LCSD R4099988-3 SVGC27 0729_024 103 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 o-Terphenyl 52.0 - 156
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4099988-2
RECOVERY R4099988-3
L1757957-16
LCS Sample / File ID:R4099988-2 / 0729_023 SDG:L1757957
LCSD Sample / File ID:R4099988-3 / 0729_024 Analytical Batch:WG2330427
Instrument ID:SVGC27 Dilution Factor:1
Analytical Method:3511/8015 Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.50 1.27 1.31 84.7 87.3 50.0 - 150 3.10 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4099988-1
Lab Sample ID:R4099988-1 SDG:L1757957
Lab File ID:0729_022 Preparation Date/Time:07/26/24 09:06
Instrument ID:SVGC27 Analysis Date/Time:07/29/24 16:07
Analytical Batch:WG2330427 Dilution Factor:1
Analytical Method:3511/8015 Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4099988-2 SVGC27 0729_023 07/29/24 16:27
LCSD R4099988-3 SVGC27 0729_024 07/29/24 16:48
EB-1-071624 L1757957-16 SVGC27 0729_040 07/29/24 22:14
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:0729_040 Received Date/Time:07/18/24 09:00
Instrument ID:SVGC27 Preparation Date/Time:07/26/24 09:07
Analytical Batch:WG2330427 Analysis Date/Time:07/29/24 22:14
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6.12 0.0688 B J 0.0247 0.100
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200 CS: 2M
TPH (GC/FID) HIGH FRACTION 5.79 5.79 5.79 5.79 5.79 5.79 5.79 5.79 0
O-TERPHENYL 7.71 7.73 7.72 7.71 7.71 7.71 7.71
File ID:0530_004 0530_005 0530_006 0530_007 0530_008 0530_009 0530_010 0530_011 0729_007
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 20960000 17370000 14610000 13340000 13690000 14100000 14530000 14590000
O-TERPHENYL 15420000 9640000 13450000 15220000 13400000 13920000 14380000
File ID:0530_004 0530_005 0530_006 0530_007 0530_008 0530_009 0530_010 0530_011
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Analytical Method:3511/8015
Analyte RRF: 2M RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 14250000 15270560 15.84 0.998
O-TERPHENYL 13631050 14.17
File ID:0729_007
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Lab File ID:0530_013-1 Analysis date/time:05/30/24 05:28
Analytical Method:3511/8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 15270560 13015600 14.80 60 54.13 90.20 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Lab File ID:0729_046-1 Analysis date/time:07/30/24 00:16
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 15270560 14412440 5.62 60 60.05 100 85 - 115
O-TERPHENYL 13631050 13256450 2.75 0.40 0.3890 97.30 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:3511/8015
Instrument ID:SVGC27 Calibration Start Date:05/30/24 02:22
Calibration End Date:07/29/24 11:16
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2 0530_004 05/30/24 02:22
CAL 4 0530_005 05/30/24 02:43
CAL 10 0530_006 05/30/24 03:03
CAL 20 0530_007 05/30/24 03:24
CAL 40 0530_008 05/30/24 03:45
CAL 60 0530_009 05/30/24 04:06
CAL 100 0530_010 05/30/24 04:26
CAL 200 0530_011 05/30/24 04:47
SSCV SVGC270530240530_013-1741929 0530_013-1 05/30/24 05:28
CAL 2M 0729_007 07/29/24 09:13
CAL 4M 0729_008 07/29/24 09:33
CAL 10M 0729_009 07/29/24 09:54
CAL 20M 0729_010 07/29/24 10:14
CAL 40M 0729_011 07/29/24 10:35
CAL 50M 0729_012 07/29/24 10:55
CAL 100M 0729_013 07/29/24 11:16
CCV SVGC270729240729_020-1741929 0729_020-1 07/29/24 15:23
BLANK R4099988-1 0729_022 07/29/24 16:07 1 WG2330427
LCS R4099988-2 0729_023 07/29/24 16:27 1 WG2330427
LCSD R4099988-3 0729_024 07/29/24 16:48 1 WG2330427
L1757627-02 L1757627-02 0729_025 07/29/24 17:08 1 WG2330427
L1757924-03 L1757924-03 0729_028 07/29/24 18:10 1 WG2330427
L1757924-04 L1757924-04 0729_029 07/29/24 18:30 1 WG2330427
L1757924-06 L1757924-06 0729_031 07/29/24 19:11 1 WG2330427
L1757924-07 L1757924-07 0729_032 07/29/24 19:31 1 WG2330427
L1757924-08 L1757924-08 0729_033 07/29/24 19:51 1 WG2330427
L1757924-09 L1757924-09 0729_034 07/29/24 20:12 1 WG2330427
L1757924-10 L1757924-10 0729_035 07/29/24 20:32 1 WG2330427
L1757924-11 L1757924-11 0729_036 07/29/24 20:53 1 WG2330427
L1757924-12 L1757924-12 0729_037 07/29/24 21:13 1 WG2330427
L1757924-13 L1757924-13 0729_038 07/29/24 21:33 1 WG2330427
L1757924-14 L1757924-14 0729_039 07/29/24 21:54 1 WG2330427
EB-1-071624 L1757957-16 0729_040 07/29/24 22:14 1 WG2330427
L1757924-02 L1757924-02 0729_044 07/29/24 23:35 10 WG2330427
CCV SVGC270729240729_046-1741929 0729_046-1 07/30/24 00:16
CCV SVGC270729240729_047-1741929 0729_047-1 07/30/24 00:36
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16 Analytical Method:3511/8015
Matrix:GW Prep Method:3511/8015
Analyte CAS MDL RDL
mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 0.0247 0.10
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099988-1
Lab Sample ID:R4099988-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0729_022 Received Date/Time:_______________
Instrument ID:SVGC27 Preparation Date/Time:07/26/24 09:06
Analytical Batch:WG2330427 Analysis Date/Time:07/29/24 16:07
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6.12 0.0252 J 0.0247 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099988-2
Lab Sample ID:R4099988-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0729_023 Received Date/Time:_______________
Instrument ID:SVGC27 Preparation Date/Time:07/26/24 09:06
Analytical Batch:WG2330427 Analysis Date/Time:07/29/24 16:27
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6.12 1.27 0.0247 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099988-3
Lab Sample ID:R4099988-3 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0729_024 Received Date/Time:_______________
Instrument ID:SVGC27 Preparation Date/Time:07/26/24 09:06
Analytical Batch:WG2330427 Analysis Date/Time:07/29/24 16:48
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6.12 1.31 0.0247 0.100
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6010B Metals (ICP)
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:20240724093622 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:36
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 15.6 0.525 2.03
Barium 7440-39-3 107 0.0864 0.507
Cadmium 7440-43-9 2.49 0.0478 0.507
Chromium 7440-47-3 14.4 0.135 1.01
Lead 7439-92-1 130 0.211 0.507
Selenium 7782-49-2 1.91 J 0.775 2.03
Silver 7440-22-4 U 0.129 1.01
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:20240723092446 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 09:24
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):92.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 10.7 0.563 2.17
Barium 7440-39-3 118 0.0926 0.544
Cadmium 7440-43-9 1.28 0.0512 0.544
Chromium 7440-47-3 10.6 0.145 1.09
Lead 7439-92-1 125 0.226 0.544
Selenium 7782-49-2 U 0.831 2.17
Silver 7440-22-4 U 0.138 1.09
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:20240723092626 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 09:26
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):92.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 25.9 0.559 2.16
Barium 7440-39-3 213 0.0919 0.539
Cadmium 7440-43-9 2.37 0.0508 0.539
Chromium 7440-47-3 16.7 0.143 1.08
Lead 7439-92-1 316 0.224 0.539
Selenium 7782-49-2 U 0.824 2.16
Silver 7440-22-4 U 0.137 1.08
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:20240723092805 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 09:28
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):97.8 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 14.8 0.530 2.05
Barium 7440-39-3 76.3 0.0871 0.511
Cadmium 7440-43-9 1.35 0.0482 0.511
Chromium 7440-47-3 11.5 0.136 1.02
Lead 7439-92-1 178 0.213 0.511
Selenium 7782-49-2 1.09 J 0.781 2.05
Silver 7440-22-4 U 0.130 1.02
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:20240723092944 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 09:29
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):98.2 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 6.50 0.527 2.04
Barium 7440-39-3 70.7 0.0867 0.509
Cadmium 7440-43-9 0.909 0.0479 0.509
Chromium 7440-47-3 16.7 0.135 1.02
Lead 7439-92-1 146 0.212 0.509
Selenium 7782-49-2 U 0.778 2.04
Silver 7440-22-4 U 0.129 1.02
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:20240723093123 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 09:31
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):94.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 23.3 0.551 2.13
Barium 7440-39-3 374 0.0906 0.532
Cadmium 7440-43-9 3.10 0.0501 0.532
Chromium 7440-47-3 20.6 0.141 1.06
Lead 7439-92-1 714 0.221 0.532
Selenium 7782-49-2 2.04 J 0.813 2.13
Silver 7440-22-4 0.242 B J 0.135 1.06
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:20240723093303 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 09:33
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):93.8 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 13.8 0.552 2.13
Barium 7440-39-3 145 0.0908 0.533
Cadmium 7440-43-9 1.16 0.0502 0.533
Chromium 7440-47-3 11.8 0.142 1.07
Lead 7439-92-1 270 0.222 0.533
Selenium 7782-49-2 U 0.814 2.13
Silver 7440-22-4 0.229 B J 0.135 1.07
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:20240723100819 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 10:08
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):98.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 4.48 0.528 2.04
Barium 7440-39-3 52.5 0.0868 0.509
Cadmium 7440-43-9 0.681 0.0480 0.509
Chromium 7440-47-3 15.1 0.136 1.02
Lead 7439-92-1 385 0.212 0.509
Selenium 7782-49-2 U 0.778 2.04
Silver 7440-22-4 U 0.129 1.02
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:20240724095440 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:54
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):98.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 6.50 0.525 2.03
Barium 7440-39-3 75.0 0.0864 0.507
Cadmium 7440-43-9 0.609 0.0477 0.507
Chromium 7440-47-3 9.93 0.135 1.01
Lead 7439-92-1 73.8 0.211 0.507
Selenium 7782-49-2 U 0.774 2.03
Silver 7440-22-4 U 0.129 1.01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:20240724095620 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:56
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):97.3 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 23.6 0.533 2.06
Barium 7440-39-3 260 0.0876 0.514
Cadmium 7440-43-9 8.79 0.0484 0.514
Chromium 7440-47-3 54.2 0.137 1.03
Lead 7439-92-1 605 0.214 0.514
Selenium 7782-49-2 6.34 0.786 2.06
Silver 7440-22-4 U 0.131 1.03
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:20240724145342 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 14:53
Dilution Factor:5 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):97.2 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 34.6 2.66 10.3
Barium 7440-39-3 268 0.438 2.57
Cadmium 7440-43-9 7.95 0.243 2.57
Chromium 7440-47-3 68.4 0.684 5.14
Lead 7439-92-1 565 1.07 2.57
Selenium 7782-49-2 13.2 3.93 10.3
Silver 7440-22-4 U 0.653 5.14
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 96 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:20240724095939 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:59
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.49 g
Total Solids (%):95.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 7.52 0.545 2.10
Barium 7440-39-3 111 0.0896 0.526
Cadmium 7440-43-9 0.891 0.0495 0.526
Chromium 7440-47-3 11.4 0.140 1.05
Lead 7439-92-1 58.9 0.219 0.526
Selenium 7782-49-2 2.47 0.803 2.10
Silver 7440-22-4 U 0.134 1.05
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 97 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:20240724100118 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 10:01
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):93.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 10.4 0.556 2.15
Barium 7440-39-3 203 0.0915 0.537
Cadmium 7440-43-9 1.94 0.0506 0.537
Chromium 7440-47-3 18.8 0.143 1.07
Lead 7439-92-1 190 0.223 0.537
Selenium 7782-49-2 1.75 J 0.821 2.15
Silver 7440-22-4 U 0.136 1.07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 98 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:20240724100258 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 10:02
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):91.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 12.8 0.569 2.20
Barium 7440-39-3 217 0.0937 0.550
Cadmium 7440-43-9 2.20 0.0518 0.550
Chromium 7440-47-3 15.5 0.146 1.10
Lead 7439-92-1 221 0.229 0.550
Selenium 7782-49-2 1.28 J 0.840 2.20
Silver 7440-22-4 U 0.140 1.10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 99 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:20240724100438 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 10:04
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):85.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 12.4 0.605 2.34
Barium 7440-39-3 262 0.0996 0.584
Cadmium 7440-43-9 2.50 0.0550 0.584
Chromium 7440-47-3 17.0 0.155 1.17
Lead 7439-92-1 414 0.243 0.584
Selenium 7782-49-2 1.57 J 0.893 2.34
Silver 7440-22-4 0.286 J 0.148 1.17
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 100 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:20240729004607 Received Date/Time:07/18/24 09:00
Instrument ID:ICP16 Preparation Date/Time:07/27/24 10:37
Analytical Batch:WG2327640 Analysis Date/Time:07/29/24 00:46
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 U 0.00440 0.0100
Barium 7440-39-3 U 0.000736 0.00500
Cadmium 7440-43-9 0.00106 J 0.000479 0.00200
Chromium 7440-47-3 0.00159 B J 0.00140 0.0100
Lead 7439-92-1 U 0.00299 0.00600
Selenium 7782-49-2 U 0.00735 0.0100
Silver 7440-22-4 U 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 101 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-1
Lab Sample ID:R4097314-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20240723084305 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:07/19/24 12:31
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 08:43
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 U 0.518 2.00
Barium 7440-39-3 U 0.0852 0.500
Cadmium 7440-43-9 U 0.0471 0.500
Chromium 7440-47-3 U 0.133 1.00
Lead 7439-92-1 U 0.208 0.500
Selenium 7782-49-2 U 0.764 2.00
Silver 7440-22-4 0.766 J 0.127 1.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 102 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097913-1
Lab Sample ID:R4097913-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20240724093303 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:07/19/24 15:15
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:33
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 U 0.518 2.00
Barium 7440-39-3 U 0.0852 0.500
Cadmium 7440-43-9 U 0.0471 0.500
Chromium 7440-47-3 U 0.133 1.00
Lead 7439-92-1 U 0.208 0.500
Selenium 7782-49-2 U 0.764 2.00
Silver 7440-22-4 U 0.127 1.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 103 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099537-1
Lab Sample ID:R4099537-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20240729001726 Received Date/Time:_______________
Instrument ID:ICP16 Preparation Date/Time:07/27/24 10:37
Analytical Batch:WG2327640 Analysis Date/Time:07/29/24 00:17
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 U 0.00440 0.0100
Barium 7440-39-3 U 0.000736 0.00500
Cadmium 7440-43-9 U 0.000479 0.00200
Chromium 7440-47-3 0.00143 J 0.00140 0.0100
Lead 7439-92-1 U 0.00299 0.00600
Selenium 7782-49-2 U 0.00735 0.0100
Silver 7440-22-4 U 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-2
Lab Sample ID:R4097314-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20240723084446 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:07/19/24 12:31
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 08:44
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 94.6 0.518 2.00
Barium 7440-39-3 102 0.0852 0.500
Cadmium 7440-43-9 102 0.0471 0.500
Chromium 7440-47-3 101 0.133 1.00
Lead 7439-92-1 98.2 0.208 0.500
Selenium 7782-49-2 96.4 0.764 2.00
Silver 7440-22-4 18.0 0.127 1.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 105 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097913-2
Lab Sample ID:R4097913-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20240724093443 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:07/19/24 15:15
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:34
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.49 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 107 0.518 2.00
Barium 7440-39-3 107 0.0852 0.500
Cadmium 7440-43-9 104 0.0471 0.500
Chromium 7440-47-3 105 0.133 1.00
Lead 7439-92-1 104 0.208 0.500
Selenium 7782-49-2 100 0.764 2.00
Silver 7440-22-4 18.8 0.127 1.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 106 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099537-2
Lab Sample ID:R4099537-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20240729001907 Received Date/Time:_______________
Instrument ID:ICP16 Preparation Date/Time:07/27/24 10:37
Analytical Batch:WG2327640 Analysis Date/Time:07/29/24 00:19
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 0.932 0.00440 0.0100
Barium 7440-39-3 0.974 0.000763 0.00500
Cadmium 7440-43-9 0.930 0.000479 0.00200
Chromium 7440-47-3 0.943 0.00140 0.0100
Lead 7439-92-1 0.899 0.00299 0.00600
Selenium 7782-49-2 0.904 0.00735 0.0100
Silver 7440-22-4 0.190 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-5
Lab Sample ID:R4097314-5 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/15/24 17:40
Lab File ID:20240723085128 Received Date/Time:07/17/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/19/24 12:31
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 08:51
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 114 0.618 2.38
Barium 7440-39-3 239 0.102 0.596
Cadmium 7440-43-9 115 0.0562 0.596
Chromium 7440-47-3 121 0.159 1.19
Lead 7439-92-1 121 0.248 0.596
Selenium 7782-49-2 115 0.911 2.38
Silver 7440-22-4 20.8 0.151 1.19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097913-5
Lab Sample ID:R4097913-5 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:20240724094121 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:41
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 120 0.525 2.03
Barium 7440-39-3 216 0.0864 0.507
Cadmium 7440-43-9 106 0.0478 0.507
Chromium 7440-47-3 113 0.135 1.01
Selenium 7782-49-2 110 0.775 2.03
Silver 7440-22-4 19.3 0.129 1.01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099537-4
Lab Sample ID:R4099537-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 08:02
Lab File ID:20240729002410 Received Date/Time:07/18/24 09:00
Instrument ID:ICP16 Preparation Date/Time:07/27/24 10:37
Analytical Batch:WG2327640 Analysis Date/Time:07/29/24 00:24
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 0.964 0.00440 0.0100
Barium 7440-39-3 1.04 0.000736 0.00500
Cadmium 7440-43-9 0.948 0.000479 0.00200
Chromium 7440-47-3 0.952 0.00140 0.0100
Lead 7439-92-1 0.924 0.00299 0.00600
Selenium 7782-49-2 0.970 0.00735 0.0100
Silver 7440-22-4 0.194 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-6
Lab Sample ID:R4097314-6 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/15/24 17:40
Lab File ID:20240723085308 Received Date/Time:07/17/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/19/24 12:31
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 08:53
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 108 0.618 2.38
Barium 7440-39-3 243 0.102 0.596
Cadmium 7440-43-9 108 0.0562 0.596
Chromium 7440-47-3 115 0.159 1.19
Lead 7439-92-1 113 0.248 0.596
Selenium 7782-49-2 109 0.911 2.38
Silver 7440-22-4 19.4 0.151 1.19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097913-6
Lab Sample ID:R4097913-6 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:20240724094301 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:43
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 117 0.525 2.03
Barium 7440-39-3 206 0.0864 0.507
Cadmium 7440-43-9 100 0.0478 0.507
Chromium 7440-47-3 109 0.135 1.01
Selenium 7782-49-2 106 0.775 2.03
Silver 7440-22-4 18.3 0.129 1.01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 112 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099537-5
Lab Sample ID:R4099537-5 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 08:02
Lab File ID:20240729002551 Received Date/Time:07/18/24 09:00
Instrument ID:ICP16 Preparation Date/Time:07/27/24 10:37
Analytical Batch:WG2327640 Analysis Date/Time:07/29/24 00:25
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 0.973 0.00440 0.0100
Barium 7440-39-3 1.04 0.000736 0.00500
Cadmium 7440-43-9 0.952 0.000479 0.00200
Chromium 7440-47-3 0.957 0.00140 0.0100
Lead 7439-92-1 0.925 0.00299 0.00600
Selenium 7782-49-2 0.969 0.00735 0.0100
Silver 7440-22-4 0.196 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-4
Lab Sample ID:R4097314-4 SDG:L1757957
Client Sample ID:PS Collected Date/Time:07/15/24 17:40
Lab File ID:20240723084948 Received Date/Time:07/17/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 08:49
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 69.4 O1 0.618 2.38
Barium 7440-39-3 151 O1 0.102 0.596
Cadmium 7440-43-9 68.2 O1 0.0562 0.596
Chromium 7440-47-3 73.5 O1 0.159 1.19
Lead 7439-92-1 71.6 O1 0.248 0.596
Selenium 7782-49-2 67.1 O1 0.911 2.38
Silver 7440-22-4 12.5 O1 0.151 1.19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-7
Lab Sample ID:R4097314-7 SDG:L1757957
Client Sample ID:PS Collected Date/Time:07/15/24 17:40
Lab File ID:20240723144045 Received Date/Time:07/17/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 14:40
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 114 0.618 2.38
Barium 7440-39-3 237 0.102 0.596
Cadmium 7440-43-9 116 0.0562 0.596
Chromium 7440-47-3 121 0.159 1.19
Lead 7439-92-1 120 0.248 0.596
Selenium 7782-49-2 116 0.911 2.38
Silver 7440-22-4 20.4 0.151 1.19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 115 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097913-4
Lab Sample ID:R4097913-4 SDG:L1757957
Client Sample ID:PS Collected Date/Time:07/16/24 09:30
Lab File ID:20240724093942 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:39
Dilution Factor:1 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 117 0.525 2.03
Barium 7440-39-3 199 0.0864 0.507
Cadmium 7440-43-9 99.8 0.0478 0.507
Chromium 7440-47-3 108 0.135 1.01
Selenium 7782-49-2 107 0.775 2.03
Silver 7440-22-4 18.1 0.129 1.01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097314-3
Lab Sample ID:R4097314-3 SDG:L1757957
Client Sample ID:SD Collected Date/Time:07/15/24 17:40
Lab File ID:20240723084807 Received Date/Time:07/17/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/22/24 06:40
Analytical Batch:WG2326410 Analysis Date/Time:07/23/24 08:48
Dilution Factor:5 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 13.4 3.09 11.9
Barium 7440-39-3 90.7 O1 0.508 2.98
Cadmium 7440-43-9 12.2 0.281 2.98
Chromium 7440-47-3 16.5 0.793 5.96
Lead 7439-92-1 14.6 1.24 2.98
Selenium 7782-49-2 15.3 4.55 11.9
Silver 7440-22-4 1.93 0.757 5.96
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097913-3
Lab Sample ID:R4097913-3 SDG:L1757957
Client Sample ID:SD Collected Date/Time:07/16/24 09:30
Lab File ID:20240724093802 Received Date/Time:07/18/24 09:00
Instrument ID:ICP17 Preparation Date/Time:07/23/24 22:02
Analytical Batch:WG2326543 Analysis Date/Time:07/24/24 09:38
Dilution Factor:5 Prep Method:3050B
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 12.3 2.63 10.1
Barium 7440-39-3 105 0.432 2.54
Cadmium 7440-43-9 2.36 0.239 2.54
Chromium 7440-47-3 14.4 0.674 5.07
Lead 7439-92-1 120 1.05 2.54
Selenium 7782-49-2 U 3.87 10.1
Silver 7440-22-4 U 0.644 5.07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099537-3
Lab Sample ID:R4099537-3 SDG:L1757957
Client Sample ID:SD Collected Date/Time:07/16/24 08:02
Lab File ID:20240729002229 Received Date/Time:07/18/24 09:00
Instrument ID:ICP16 Preparation Date/Time:07/27/24 10:37
Analytical Batch:WG2327640 Analysis Date/Time:07/29/24 00:22
Dilution Factor:5 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 U 0.0220 0.0500
Barium 7440-39-3 0.0550 0.00368 0.0250
Cadmium 7440-43-9 U 0.00240 0.0100
Chromium 7440-47-3 U 0.00700 0.0500
Lead 7439-92-1 U 0.0150 0.0300
Selenium 7782-49-2 U 0.0368 0.0500
Silver 7440-22-4 U 0.00770 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Concentration Units:mg/l
ICV ICVLL CCV
Sample ID:ICP160728241717 ICP160728241742 ICP160729240014
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.9794422 97.9
0 0.897000 0.01 0.01184958 118 27.100000 1 0.9473552 94.7
0 0.546000
BARIUM 1 1.006561 101 0.287000 0.0050 0.005071986 101 4.240000 0.50 1.006191 201 0.440000
CADMIUM 1 0.9755388 97.6
0 0.308000 0.0020 0.001609497 80.5
0 23.900000 0.50 0.9524702 190 0.410000
CHROMIUM 1 0.982977 98.3
0 0.423000 0.01 0.009681465 96.8
0 6.880000 1 0.9716283 97.2
0 0.583000
LEAD 1 0.9528121 95.3
0 0.340000 0.0050 0.00548321 110 21.700000 0.50 0.9244014 185 0.249000
SELENIUM 1 0.9505527 95.10 1.250000 0.01 0.008476041 84.8
0 66.100000 1 0.9207665 92.10 0.208000
SILVER 1 0.9565937 95.7
0 0.451000 0.0050 0.004807537 96.2
0 11.900000 0.50 0.5243941 105 0.533000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Concentration Units:mg/l
CCV CCV
Sample ID:ICP160729240034 ICP160729240054-2
Analyte True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.9391141 93.9
0 0.702000 1 0.9364211 93.6
0 0.387000
BARIUM 0.50 0.9983504 200 0.500000 0.50 0.9923347 198 0.142000
CADMIUM 0.50 0.9452982 189 1.010000 0.50 0.9464534 189 0.099200
CHROMIUM 1 0.9630321 96.3
0 0.922000 1 0.9582428 95.8
0 0.199000
LEAD 0.50 0.9154758 183 0.924000 0.50 0.919583 184 0.617000
SELENIUM 1 0.9120092 91.20 1.490000 1 0.9250776 92.5
0 0.683000
SILVER 0.50 0.5166225 103 0.648000 0.50 0.520228 104 0.542000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Concentration Units:mg/l
ICV CCV ICVLL
Sample ID:ICP170723240749 ICP170723240753 ICP170723240756
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.9541931 95.4
0 0.496000 1 0.9548903 95.5
0 0.347000 0.01 0.00894866 89.5
0 50.400000
BARIUM 1 1.028188 103 0.071900 0.50 1.044939 209 0.141000 0.0050 0.00531814 106 2.390000
CADMIUM 1 1.014968 101 0.418000 0.50 1.023581 205 0.293000 0.0020 0.00234351 117 9.100000
CHROMIUM 1 1.021166 102 0.384000 1 1.023314 102 0.384000 0.01 0.01099421 110 1.260000
LEAD 1 0.9827086 98.3
0 0.447000 0.50 0.9912179 198 0.150000 0.0050 0.00522526
6 105 39.500000
SELENIUM 1 0.9593698 95.9
0 1.490000 1 0.9560572 95.6
0 1.500000 0.01 0.01198765 120 13.500000
SILVER 1 0.9614327 96.10 0.246000 0.50 0.5021598 100 0.366000 0.0050 0.004674543 93.5
0 8.870000
ICV Limits:90 - 110 CCV Limits:90 - 110 ICVLL Limits:50 - 150 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Concentration Units:mg/l
CCV CCV CCV
Sample ID:ICP170723240859 ICP170723240934 ICP170723240954
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.98264 98.3
0 0.482000 1 0.9821919 98.2
0 0.285000 1 0.9931187 99.3
0 0.486000
BARIUM 0.50 1.059888 212 0.416000 0.50 1.054307 211 0.125000 0.50 1.069516 214 0.302000
CADMIUM 0.50 1.071064 214 0.583000 0.50 1.073949 215 0.318000 0.50 1.089575 218 0.790000
CHROMIUM 1 1.036522 104 0.489000 1 1.034341 103 0.511000 1 1.050366 105 0.774000
LEAD 0.50 1.01087 202 0.587000 0.50 1.013575 203 0.611000 0.50 1.02882 206 0.359000
SELENIUM 1 0.9965831 99.7
0 0.465000 1 1.004598 100 1.740000 1 1.016322 102 0.188000
SILVER 0.50 0.517427 103 0.412000 0.50 0.5227283 105 0.513000 0.50 0.5225192 105 0.183000
ICV Limits:90 - 110 CCV Limits:90 - 110 ICVLL Limits:50 - 150 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Concentration Units:mg/l
CCV CCVLL
Sample ID:ICP170723241010 ICP170723241337
Analyte True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.9689807 96.9
0 0.809000 0.01 0.01148304 115 25.100000
BARIUM 0.50 1.059698 212 0.594000 0.0050 0.004921753 98.4
0 4.080000
CADMIUM 0.50 1.070472 214 0.465000 0.0020 0.001930288 96.5
0 3.910000
CHROMIUM 1 1.030341 103 0.602000 0.01 0.01122629 112 2.800000
LEAD 0.50 1.017939 204 0.230000 0.0050 0.00385499
6 77.10 11.500000
SELENIUM 1 0.9930231 99.3
0 1.290000 0.01 0.012988 130 69.800000
SILVER 0.50 0.5179228 104 0.114000 0.0050 0.005820144 116 7.940000
ICV Limits:90 - 110 CCV Limits:90 - 110 ICVLL Limits:50 - 150 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Concentration Units:mg/l
ICV ICVLL CCV
Sample ID:ICP170724240648-2 ICP170724240654-2 ICP170724240929-2
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 1.030435 103 0.672000 0.01 0.008857584 88.6
0 10.100000 1 1.031751 103 0.181000
BARIUM 1 1.014686 101 0.334000 0.0050 0.00539893
9 108 3.450000 0.50 1.039841 208 0.217000
CADMIUM 1 0.9971579 99.7
0 0.320000 0.0020 0.002095617 105 6.010000 0.50 1.013874 203 0.687000
CHROMIUM 1 1.009112 101 0.473000 0.01 0.01066089 107 2.550000 1 1.024338 102 1.010000
LEAD 1 0.9907688 99.10 0.326000 0.0050 0.005297137 106 34.000000 0.50 0.997948 200 0.612000
SELENIUM 1 0.9589313 95.9
0 1.290000 0.01 0.008421565 84.2
0 78.600000 1 0.9783302 97.8
0 0.454000
SILVER 1 0.9568668 95.7
0 0.590000 0.0050 0.00535932
9 107 9.070000 0.50 0.5001186 100 0.565000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Concentration Units:mg/l
CCV CCV
Sample ID:ICP170724240949-2 ICP170724241007
Analyte True Found %R %RSD True Found %R %RSD
ARSENIC 1 1.026165 103 1.340000 1 1.025883 103 0.416000
BARIUM 0.50 1.033436 207 0.068400 0.50 1.037828 208 0.145000
CADMIUM 0.50 1.002075 200 0.595000 0.50 1.009058 202 0.694000
CHROMIUM 1 1.016734 102 0.335000 1 1.019879 102 0.602000
LEAD 0.50 0.9925521 199 0.675000 0.50 1.003118 201 0.465000
SELENIUM 1 0.961896 96.2
0 1.150000 1 0.9678371 96.8
0 0.411000
SILVER 0.50 0.4983131 99.7
0 0.394000 0.50 0.4991119 99.8
0 0.115000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Sample ID:ICB Result ICB Qual ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual
File ID:20240728171855 20240728173744 20240729001542 20240729001726
Analyte mg/l mg/l mg/l mg/l
ARSENIC 0.004282035 U 0.003326882 U 0.001071475 U U
BARIUM 0.0002091881 U -0.0000769494
9 U 0.00007395571 U U
CADMIUM 0.0004957856 U 0.0001334708 U 0.0005219358 U U
CHROMIUM 0.000667832 U 0.0002623314 U 0.001286895 U 0.00143 J
LEAD 0.00001666993 U 0.001305131 U -0.000280963 U U
SELENIUM 0.001442136 U -0.001956624 U 0.005369911 U U
SILVER 0.01490916 -0.0004267012 U -0.001500243 U U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Sample ID:CCB Result CCB Qual CCB Result CCB Qual
File ID:20240729003559 20240729005616-2
Analyte mg/l mg/l
ARSENIC 0.001304417 U 0.002125147 U
BARIUM 0.0001038767 U 0.0000939608
6 U
CADMIUM 0.00106588 U 0.0009858219 U
CHROMIUM 0.0009097377 U 0.000615369 U
LEAD 0.001059222 U 0.001533288 U
SELENIUM 0.0004213811 U 0.0009749606 U
SILVER -0.00123377 U -0.0007751066 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20240723075138 20240723075501 20240723084305 20240723090124
Analyte mg/l mg/l mg/kg mg/l
ARSENIC -0.0009151036 U 0.001142486 U U 0.003586524 U
BARIUM 0.0001600245 U 0.00006709741 U U -0.0000582600
8 U
CADMIUM 0.0002629077 U -0.0002013137 U U 0.00006930275 U
CHROMIUM 0.0004587515 U 0.0006152251 U U 0.0004676812 U
LEAD 0.0007366537 U 0.0004523676 U U -0.002349163 U
SELENIUM 0.006042863 U 0.004574391 U U 0.0008128039 U
SILVER 0.003402531 U -0.00005451375 U 0.766 J 0.0001779437 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Sample ID:CCB Result CCB Qual CCB Result CCB Qual CCB Result CCB Qual CCB Result CCB Qual
File ID:20240723093631 20240723095634 20240723101207 20240723143356-2
Analyte mg/l mg/l mg/l mg/l
ARSENIC -0.001662196 U 0.003220882 U 0.006468245 U 0.004616221 U
BARIUM -0.0000795853
8 U -0.0000636993
1 U -0.00001757598 U -0.0001547097 U
CADMIUM 0.0001531304 U 0.0002180546 U 0.000271005 U -0.00002370172 U
CHROMIUM 0.0002812071 U 0.0003344088 U -0.0000428192 U 0.0002464563 U
LEAD -0.001744124 U -0.001026729 U -0.001104922 U -0.0004957657 U
SELENIUM 0.0003981617 U 0.002925328 U -0.0000227292
8 U 0.001481738 U
SILVER 0.0001356362 U 0.0002763592 U -0.0002532289 U 0.0009552222 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Sample ID:CCB Result CCB Qual
File ID:20240723144552-2
Analyte mg/l
ARSENIC 0.003626238 U
BARIUM -0.0001566003 U
CADMIUM 0.0000208350
8 U
CHROMIUM 0.0001588234 U
LEAD -0.002805395 U
SELENIUM -0.00176951 U
SILVER 0.0005098437 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20240724064946-2 20240724093120-2 20240724093303 20240724095120-2
Analyte mg/l mg/l mg/kg mg/l
ARSENIC -0.004611237 U -0.0005854955 U U -0.006594523 U
BARIUM 0.00003830232 U 0.0000784308 U U 0.000212557 U
CADMIUM 0.0003060168 U 0.0002462632 U U 0.0001464805 U
CHROMIUM 0.0003475957 U 0.0002374276 U U 0.0000007045
06 U
LEAD 0.0009850762 U -0.001060454 U U -0.001161023 U
SELENIUM -0.004565535 U 0.004109865 U U 0.0003180232 U
SILVER 0.003113186 U 0.0001172023 U U 0.0001935297 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Sample ID:CCB Result CCB Qual CCB Result CCB Qual CCB Result CCB Qual
File ID:20240724100937 20240724145015-2 20240724151059-2
Analyte mg/l mg/l mg/l
ARSENIC -0.002515842 U -0.0001548446 U 0.0006671415 U
BARIUM 0.0001564748 U 0.00007453134 U 0.0003635251 U
CADMIUM 0.0002231926 U -0.00003015581 U -0.0002275602 U
CHROMIUM 0.0003297926 U 0.000370263 U -0.0001265448 U
LEAD -0.0009136607 U 0.0008089302 U 0.001948857 U
SELENIUM 0.003099077 U -0.002505828 U -0.0000738239
7 U
SILVER 0.00032356 U 0.0002560098 U 0.0003375871 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP16 Date:07/28/24 17:44
Instrument Run:072824ICP16
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 496.68 99.30 500 496.1699 99.20
ANTIMONY 0 -0.00421866 0.50 0.4926935 98.50
ARSENIC 0 0.0004391966 0.50 0.4916697 98.30
BARIUM 0 0.001962434 0.50 0.4934952 98.70
BERYLLIUM 0 0.000302902 0.50 0.4931907 98.60
BORON 0 -0.02401114 1 0.9419397 94.20
CADMIUM 0 0.00004574783 1 1.008427 101
CALCIUM 500 499.655 99.90 500 505.0792 101
CERIUM 0 0.09153216 0 0.07041015
CHROMIUM 0 -0.003362664 0.50 0.4774614 95.50
COBALT 0 0.00240203 0.50 0.4862682 97.30
COPPER 0 0.0001937122 0.50 0.5019632 100
IRON 200 200.7651 100 200 200.1619 100
LANTHANUM 0 -0.005675969 0 -0.008553484
LEAD 0 -0.002883262 1 0.95843 95.80
LITHIUM 0 0.003587866 0 0.001922575
MAGNESIUM 500 509.0172 102 500 507.0744 101
MANGANESE 0 -0.003778775 0.50 0.4784587 95.70
MOLYBDENUM 0 -0.001180414 0.50 0.477041 95.40
NICKEL 0 0.001019149 1 0.9572119 95.70
PHOSPHORUS 0 0.003955052 0 0.01396033
POTASSIUM 0 -0.008337506 0 0.02805844
SELENIUM 0 -0.0005674592 0.50 0.515026 103
SILICON 0 -0.03184845 1 1.284886 128
SILVER 0 -0.001167687 1 0.9505818 95.10
SODIUM 0 -0.02183743 0 0.01038057
STRONTIUM 0 0.004020475 0 0.004200873
SULFUR 0 -0.02532272 0 -0.01142502
THALLIUM 0 -0.0008390556 0.50 0.4749659 95
TIN 0 0.0003385258 0.50 0.4747941 95
TITANIUM 0 -0.004701036 0.50 0.4727499 94.50
VANADIUM 0 0.008369841 0.50 0.4827045 96.50
ZINC 0 0.007704126 1 0.935444 93.50
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 134 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP16 Date:07/28/24 22:22
Instrument Run:072824ICP16
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 493.0517 98.60 500 499.2369 99.80
ANTIMONY 0 -0.01114957 0.50 0.4706199 94.10
ARSENIC 0 -0.003821763 0.50 0.4755729 95.10
BARIUM 0 0.002169592 0.50 0.4817743 96.40
BERYLLIUM 0 0.0002662894 0.50 0.4947604 99
BORON 0 -0.02471691 1 0.9516071 95.20
CADMIUM 0 0.0001726751 1 0.9914212 99.10
CALCIUM 500 502.5257 101 500 516.0312 103
CERIUM 0 0.05805027 0 0.05109558
CHROMIUM 0 -0.001980105 0.50 0.4678323 93.60
COBALT 0 0.001844195 0.50 0.4788576 95.80
COPPER 0 0.00242816 0.50 0.4991894 99.80
IRON 200 197.3505 98.70 200 201.3845 101
LANTHANUM 0 -0.001928584 0 -0.009138459
LEAD 0 -0.001515908 1 0.9383772 93.80
LITHIUM 0 -0.0009365436 0 0.000235271
MAGNESIUM 500 499.9764 100 500 505.4734 101
MANGANESE 0 -0.003383538 0.50 0.4700625 94
MOLYBDENUM 0 -0.001246728 0.50 0.4643263 92.90
NICKEL 0 0.0004470574 1 0.9301583 93
PHOSPHORUS 0 0.001858337 0 0.006463541
POTASSIUM 0 0.007749364 0 -0.0008817085
SELENIUM 0 -0.003581805 0.50 0.5182663 104
SILICON 0 -0.03305315 1 1.25123 125
SILVER 0 -0.0009292462 1 0.9378972 93.80
SODIUM 0 0.03672769 0 0.06770268
STRONTIUM 0 0.004327866 0 0.00422719
SULFUR 0 -0.03024604 0 -0.02252997
THALLIUM 0 -0.0002814685 0.50 0.4559847 91.20
TIN 0 -0.001385745 0.50 0.4607712 92.20
TITANIUM 0 -0.004623823 0.50 0.4751089 95
VANADIUM 0 0.007681537 0.50 0.4831668 96.60
ZINC 0 0.007691529 1 0.9068779 90.70
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 135 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP16 Date:07/29/24 01:23
Instrument Run:072824ICP16
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 495.7611 99.20 500 498.0066 99.60
ANTIMONY 0 -0.009313657 0.50 0.4973459 99.50
ARSENIC 0 -0.003957026 0.50 0.4864615 97.30
BARIUM 0 0.00211463 0.50 0.4990686 99.80
BERYLLIUM 0 0.0003221068 0.50 0.4895232 97.90
BORON 0 -0.02638724 1 0.9448782 94.50
CADMIUM 0 0.0007185298 1 1.019362 102
CALCIUM 500 506.7083 101 500 512.1681 102
CERIUM 0 0.05274248 0 0.0289551
CHROMIUM 0 -0.002357391 0.50 0.4847703 97
COBALT 0 0.002002669 0.50 0.4956998 99.10
COPPER 0 0.001964013 0.50 0.5181233 104
IRON 200 197.5913 98.80 200 196.3753 98.20
LANTHANUM 0 -0.007152529 0 -0.007415454
LEAD 0 -0.002980778 1 0.9707482 97.10
LITHIUM 0 0.0005505064 0 0.002249344
MAGNESIUM 500 500.3171 100 500 496.2983 99.30
MANGANESE 0 -0.0034244 0.50 0.4868217 97.40
MOLYBDENUM 0 -0.0007006883 0.50 0.4814122 96.30
NICKEL 0 0.001775412 1 0.9627654 96.30
PHOSPHORUS 0 0.01495303 0 0.01374512
POTASSIUM 0 0.1011543 0 0.1004027
SELENIUM 0 0.008365678 0.50 0.5224535 104
SILICON 0 -0.0275809 1 1.303437 130
SILVER 0 -0.001500795 1 0.9591825 95.90
SODIUM 0 0.3185929 0 0.2686728
STRONTIUM 0 0.004206089 0 0.004179158
SULFUR 0 -0.01317824 0 0.01738397
THALLIUM 0 -0.001391121 0.50 0.4742734 94.90
TIN 0 -0.0002483354 0.50 0.4767608 95.40
TITANIUM 0 -0.003847992 0.50 0.4657449 93.10
VANADIUM 0 0.005866655 0.50 0.4759115 95.20
ZINC 0 0.008182843 1 0.933504 93.40
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 136 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:07/23/24 07:58
Instrument Run:072324ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 495.0137 99 500 493.6939 98.70
ANTIMONY 0 -0.003760356 0.50 0.5233511 105
ARSENIC 0 0.008842344 0.50 0.508459 102
BARIUM 0 0.002513597 0.50 0.5014559 100
BERYLLIUM 0 0.0003307021 0.50 0.4913536 98.30
BORON 0 -0.03040233 1 0.9614367 96.10
CADMIUM 0 0.00004171456 1 1.007485 101
CALCIUM 500 501.6195 100 500 498.4698 99.70
CERIUM 0 0.04164563 0 0.0560998
CHROMIUM 0 0.0009190967 0.50 0.4792533 95.90
COBALT 0 -0.00004165408 0.50 0.4822739 96.50
COPPER 0 -0.001855356 0.50 0.5155221 103
IRON 200 199.2651 99.60 200 198.1423 99.10
LANTHANUM 0 -0.001820486 0 -0.006309096
LEAD 0 0.002017827 1 0.9727627 97.30
LITHIUM 0 0.001846446 0 0.002146135
MAGNESIUM 500 503.7251 101 500 499.076 99.80
MANGANESE 0 -0.0006954371 0.50 0.4851268 97
MOLYBDENUM 0 -0.000148945 0.50 0.4758884 95.20
NICKEL 0 0.002069055 1 0.9674636 96.70
PHOSPHORUS 0 0.009404001 0 0.01078615
POTASSIUM 0 0.054075 0 0.04194892
SELENIUM 0 0.006689237 0.50 0.5081598 102
SILICON 0 -0.03808797 1 1.260445 126
SILVER 0 -0.002561479 1 0.9350195 93.50
SODIUM 0 0.05875576 0 0.02745563
STRONTIUM 0 0.004134877 0 0.00426416
SULFUR 0 -0.02460256 0 -0.005419502
THALLIUM 0 0.002089902 0.50 0.4998161 100
TIN 0 -0.003044393 0.50 0.4759424 95.20
TITANIUM 0 -0.004054905 0.50 0.4774885 95.50
VANADIUM 0 0.001858483 0.50 0.4731672 94.60
ZINC 0 0.007712361 1 0.9565027 95.70
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 137 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:07/23/24 13:39
Instrument Run:072324ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 493.6466 98.70 500 501.1413 100
ANTIMONY 0 -0.001050192 0.50 0.5261275 105
ARSENIC 0 0.008480984 0.50 0.5187617 104
BARIUM 0 0.001837947 0.50 0.5056382 101
BERYLLIUM 0 0.0002349011 0.50 0.5034153 101
BORON 0 -0.02649777 1 0.994218 99.40
CADMIUM 0 0.0008021756 1 1.077757 108
CALCIUM 500 499.9956 100 500 504.3697 101
CERIUM 0 0.05947807 0 0.07323085
CHROMIUM 0 0.0007830269 0.50 0.4955963 99.10
COBALT 0 0.00005284802 0.50 0.5174186 103
COPPER 0 -0.0003821452 0.50 0.5222981 104
IRON 200 195.6688 97.80 200 198.4678 99.20
LANTHANUM 0 -0.001913683 0 -0.007553073
LEAD 0 -0.003987908 1 1.002778 100
LITHIUM 0 0.00170821 0 0.002203425
MAGNESIUM 500 508.6375 102 500 515.3715 103
MANGANESE 0 -0.0009150349 0.50 0.4998455 100
MOLYBDENUM 0 0.0001429101 0.50 0.4985249 99.70
NICKEL 0 0.001470572 1 1.013542 101
PHOSPHORUS 0 0.01054522 0 0.0117023
POTASSIUM 0 0.07834413 0 0.0977485
SELENIUM 0 0.005795048 0.50 0.560865 112
SILICON 0 -0.04724472 1 1.200311 120
SILVER 0 -0.003251031 1 0.8453391 84.50
SODIUM 0 0.1560287 0 0.1464338
STRONTIUM 0 0.004174351 0 0.004232727
SULFUR 0 -0.00864274 0 -0.008902089
THALLIUM 0 0.005744111 0.50 0.5203406 104
TIN 0 -0.002020123 0.50 0.5149036 103
TITANIUM 0 -0.00426407 0.50 0.4798756 96
VANADIUM 0 0.004280422 0.50 0.4944024 98.90
ZINC 0 0.007694674 1 0.9765602 97.70
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 138 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:07/23/24 15:26
Instrument Run:072324ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 490.8228 98.20 500 493.2437 98.60
ANTIMONY 0 -0.007274277 0.50 0.5280532 106
ARSENIC 0 0.006812393 0.50 0.5154486 103
BARIUM 0 0.001920015 0.50 0.504029 101
BERYLLIUM 0 0.0002067883 0.50 0.5017276 100
BORON 0 -0.02772254 1 0.9753032 97.50
CADMIUM 0 0.0003292845 1 1.062422 106
CALCIUM 500 496.6005 99.30 500 500.9868 100
CERIUM 0 0.05574862 0 0.07162025
CHROMIUM 0 0.0005695873 0.50 0.4944214 98.90
COBALT 0 -0.00004195449 0.50 0.5095532 102
COPPER 0 -0.001062314 0.50 0.5238895 105
IRON 200 195.3197 97.70 200 195.7867 97.90
LANTHANUM 0 -0.00156907 0 -0.00588298
LEAD 0 0.000139298 1 0.9936318 99.40
LITHIUM 0 0.0009445523 0 0.001031153
MAGNESIUM 500 506.9383 101 500 506.4386 101
MANGANESE 0 -0.0009058173 0.50 0.4985434 99.70
MOLYBDENUM 0 0.001786108 0.50 0.4980456 99.60
NICKEL 0 0.001324678 1 1.004653 100
PHOSPHORUS 0 0.004728663 0 0.01402623
POTASSIUM 0 0.02620455 0 0.04309516
SELENIUM 0 0.001170922 0.50 0.5392923 108
SILICON 0 -0.04481442 1 1.155882 116
SILVER 0 -0.002911481 1 0.9400248 94
SODIUM 0 0.0310046 0 0.03552502
STRONTIUM 0 0.004223782 0 0.004181806
SULFUR 0 -0.01254285 0 -0.005147099
THALLIUM 0 0.002615307 0.50 0.5109913 102
TIN 0 0.0004631096 0.50 0.5074746 101
TITANIUM 0 -0.004204874 0.50 0.4755921 95.10
VANADIUM 0 0.004201848 0.50 0.4905609 98.10
ZINC 0 0.008005796 1 0.9778074 97.80
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 139 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:07/24/24 06:56
Instrument Run:072424ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 489.6059 97.90 500 494.2248 98.80
ANTIMONY 0 -0.01114549 0.50 0.5091164 102
ARSENIC 0 0.003494374 0.50 0.5114674 102
BARIUM 0 0.002184899 0.50 0.5001953 100
BERYLLIUM 0 0.0003501915 0.50 0.4934392 98.70
BORON 0 -0.02976743 1 0.9496853 95
CADMIUM 0 0.0006450021 1 1.020727 102
CALCIUM 500 497.9691 99.60 500 503.0035 101
CERIUM 0 0.04329031 0 0.07165468
CHROMIUM 0 0.000353801 0.50 0.487645 97.50
COBALT 0 0.0004366505 0.50 0.4904747 98.10
COPPER 0 -0.0018276 0.50 0.5159365 103
IRON 200 197.5113 98.80 200 198.7357 99.40
LANTHANUM 0 -0.003141219 0 -0.006108175
LEAD 0 -0.00137326 1 0.9730044 97.30
LITHIUM 0 -0.000568196 0 0.0018244
MAGNESIUM 500 501.1284 100 500 505.778 101
MANGANESE 0 -0.000615489 0.50 0.4913859 98.30
MOLYBDENUM 0 0.001738151 0.50 0.4852619 97.10
NICKEL 0 0.002361134 1 0.9744883 97.40
PHOSPHORUS 0 0.01073627 0 0.005312449
POTASSIUM 0 0.09914129 0 0.07593751
SELENIUM 0 0.004047866 0.50 0.5342454 107
SILICON 0 -0.04087322 1 1.19549 120
SILVER 0 -0.00383878 1 0.9087615 90.90
SODIUM 0 0.09121744 0 0.08387868
STRONTIUM 0 0.004115844 0 0.004039654
SULFUR 0 -0.006059994 0 0.005866368
THALLIUM 0 -0.003158089 0.50 0.4713872 94.30
TIN 0 -0.00110305 0.50 0.4849462 97
TITANIUM 0 -0.004228194 0.50 0.4779903 95.60
VANADIUM 0 0.002805441 0.50 0.4803588 96.10
ZINC 0 0.01053699 1 0.9663592 96.60
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 140 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:07/24/24 13:58
Instrument Run:072424ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 492.8447 98.60 500 498.2676 99.70
ANTIMONY 0 -0.01090618 0.50 0.5087204 102
ARSENIC 0 0.005363675 0.50 0.5268847 105
BARIUM 0 0.002262428 0.50 0.4985288 99.70
BERYLLIUM 0 0.0003391037 0.50 0.498843 99.80
BORON 0 -0.02537099 1 0.9580579 95.80
CADMIUM 0 0.000536783 1 1.026407 103
CALCIUM 500 503.7503 101 500 510.1357 102
CERIUM 0 0.06519308 0 0.07289372
CHROMIUM 0 0.0007917265 0.50 0.489938 98
COBALT 0 0.0006817978 0.50 0.4965773 99.30
COPPER 0 -0.001257493 0.50 0.5211195 104
IRON 200 197.7838 98.90 200 200.392 100
LANTHANUM 0 -0.00198148 0 -0.005428143
LEAD 0 -0.003286616 1 0.9875241 98.80
LITHIUM 0 0.002729052 0 0.003653806
MAGNESIUM 500 507.3436 101 500 512.7269 103
MANGANESE 0 -0.000725843 0.50 0.4907914 98.20
MOLYBDENUM 0 0.00126838 0.50 0.4912437 98.20
NICKEL 0 0.002478298 1 0.9846671 98.50
PHOSPHORUS 0 0.005486459 0 0.01407766
POTASSIUM 0 0.2687972 0 0.2521414
SELENIUM 0 0.02399692 0.50 0.5362337 107
SILICON 0 -0.0396754 1 1.210234 121
SILVER 0 -0.003598268 1 0.9205094 92.10
SODIUM 0 0.1670177 0 0.161861
STRONTIUM 0 0.004123465 0 0.004119104
SULFUR 0 0.01244696 0 0.004423887
THALLIUM 0 -0.0007217954 0.50 0.4928824 98.60
TIN 0 -0.005521109 0.50 0.4924892 98.50
TITANIUM 0 -0.004873295 0.50 0.4773989 95.50
VANADIUM 0 0.003524743 0.50 0.4882868 97.70
ZINC 0 0.01105995 1 0.9790123 97.90
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 141 of 530
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:07/24/24 20:34
Instrument Run:072424ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 493.9168 98.80 500 496.3146 99.30
ANTIMONY 0 0.001947559 0.50 0.5263034 105
ARSENIC 0 0.01271171 0.50 0.5414363 108
BARIUM 0 0.002203868 0.50 0.5060757 101
BERYLLIUM 0 0.0003653985 0.50 0.4981 99.60
BORON 0 -0.0240301 1 0.9519126 95.20
CADMIUM 0 0.0002428658 1 1.034245 103
CALCIUM 500 500.4952 100 500 504.4163 101
CERIUM 0 0.08545482 0 0.08181107
CHROMIUM 0 0.001279328 0.50 0.4940924 98.80
COBALT 0 0.00107581 0.50 0.4981979 99.60
COPPER 0 -0.001092472 0.50 0.5223236 104
IRON 200 198.0042 99 200 198.404 99.20
LANTHANUM 0 -0.003165035 0 -0.007768464
LEAD 0 0.001993708 1 1.004132 100
LITHIUM 0 0.001489239 0 0.00231021
MAGNESIUM 500 505.8463 101 500 508.2389 102
MANGANESE 0 -0.0007187374 0.50 0.4958614 99.20
MOLYBDENUM 0 0.0009438618 0.50 0.4881104 97.60
NICKEL 0 0.002377954 1 0.9930369 99.30
PHOSPHORUS 0 0.006460869 0 0.008547958
POTASSIUM 0 0.3608503 0 0.3386958
SELENIUM 0 0.008479727 0.50 0.5417382 108
SILICON 0 -0.03351688 1 1.193472 119
SILVER 0 -0.002955556 1 0.9275141 92.80
SODIUM 0 0.07577273 0 0.06152054
STRONTIUM 0 0.004279498 0 0.004323726
SULFUR 0 -0.003945643 0 -0.0132109
THALLIUM 0 0.001618016 0.50 0.495162 99
TIN 0 -0.004652038 0.50 0.4951054 99
TITANIUM 0 -0.002541398 0.50 0.4741621 94.80
VANADIUM 0 0.002753311 0.50 0.4837316 96.70
ZINC 0 0.009859552 1 0.9827521 98.30
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 142 of 530
5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4097314-5
L1757957-02,03,04,05,06,07,08 R4097314-6
MS Sample / File ID:R4097314-5 / 20240723085128 SDG:L1757957
MSD Sample / File ID:R4097314-6 / 20240723085308 Analytical Batch:WG2326410
OS Sample / File ID:L1757594-01 / 20240723084627 Matrix:Solid
Instrument ID:ICP17
Analytical Method:6010B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 119 1.66 114 108 94.5 89.3 1 75.0 - 125 5.50 20
Barium 119 123 239 243 97.9 101 1 75.0 - 125 1.33 20
Cadmium 119 0.609 115 108 96.3 89.9 1 75.0 - 125 6.81 20
Chromium 119 7.10 121 115 95.8 90.5 1 75.0 - 125 5.29 20
Lead 119 4.45 121 113 97.4 90.8 1 75.0 - 125 6.82 20
Selenium 119 U 115 109 96.5 91.1 1 75.0 - 125 5.83 20
Silver 23.8 U 20.8 19.4 87.3 81.4 1 75.0 - 125 7.06 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 143 of 530
5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4097913-5
L1757957-01,09,10,11,12,13,14,15 R4097913-6
MS Sample / File ID:R4097913-5 / 20240724094121 SDG:L1757957
MSD Sample / File ID:R4097913-6 / 20240724094301 Analytical Batch:WG2326543
OS Sample / File ID:L1757957-01 / 20240724093622 Matrix:Solid
Instrument ID:ICP17
Analytical Method:6010B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 101 15.6 120 117 103 100 1 75.0 - 125 2.35 20
Barium 101 107 216 206 107 97.0 1 75.0 - 125 4.83 20
Cadmium 101 2.49 106 100 102 96.4 1 75.0 - 125 5.50 20
Chromium 101 14.4 113 109 97.4 93.7 1 75.0 - 125 3.35 20
Selenium 101 1.91 110 106 107 103 1 75.0 - 125 3.88 20
Silver 20.3 U 19.3 18.3 94.9 90.3 1 75.0 - 125 4.94 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 144 of 530
5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4099537-4
L1757957-16 R4099537-5
MS Sample / File ID:R4099537-4 / 20240729002410 SDG:L1757957
MSD Sample / File ID:R4099537-5 / 20240729002551 Analytical Batch:WG2327640
OS Sample / File ID:L1758018-06 / 20240729002048 Matrix:GW
Instrument ID:ICP16
Analytical Method:6010B
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 U 0.964 0.973 96.4 97.3 1 75.0 - 125 0.927 20
Barium 1.00 0.0597 1.04 1.04 97.6 98.1 1 75.0 - 125 0.471 20
Cadmium 1.00 0.00104 0.948 0.952 94.7 95.1 1 75.0 - 125 0.412 20
Chromium 1.00 0.00275 0.952 0.957 94.9 95.4 1 75.0 - 125 0.493 20
Lead 1.00 U 0.924 0.925 92.4 92.5 1 75.0 - 125 0.150 20
Selenium 1.00 U 0.970 0.969 97.0 96.9 1 75.0 - 125 0.0879 20
Silver 0.200 U 0.194 0.196 96.8 97.9 1 75.0 - 125 1.11 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4097314-4
L1757957-02,03,04,05,06,07,08
PS Sample / File ID:R4097314-4 / 20240723084948 SDG:L1757957
OS Sample / File ID:L1757594-01 / 20240723084627 Analytical Batch:WG2326410
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
PD
Result
(dry)
DS
Result
(dry)
PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/kg mg/kg mg/kg %%%mg/kg mg/kg
Arsenic 119 1.66 69.4 56.8*1 80.0 -
120 *
Barium 119 123 151 23.5*1 80.0 -
120 *
Cadmium 119 0.609 68.2 56.7*1 80.0 -
120 *
Chromium 119 7.10 73.5 55.7*1 80.0 -
120 *
Lead 119 4.45 71.6 56.4*1 80.0 -
120 *
Selenium 119 U 67.1 56.2*1 80.0 -
120 *
Silver 23.8 U 12.5 52.6*1 80.0 -
120 *
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4097314-7
L1757957-02,03,04,05,06,07,08
PS Sample / File ID:R4097314-7 / 20240723144045 SDG:L1757957
OS Sample / File ID:L1757594-01 / 20240723084627 Analytical Batch:WG2326410
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
PD
Result
(dry)
DS
Result
(dry)
PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/kg mg/kg mg/kg %%%mg/kg mg/kg
Arsenic 119 1.66 114 94.6 1 80.0 -
120
Barium 119 123 237 95.7 1 80.0 -
120
Cadmium 119 0.609 116 96.8 1 80.0 -
120
Chromium 119 7.10 121 95.7 1 80.0 -
120
Lead 119 4.45 120 96.8 1 80.0 -
120
Selenium 119 U 116 97.6 1 80.0 -
120
Silver 23.8 U 20.4 85.6 1 80.0 -
120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4097913-4
L1757957-01,09,10,11,12,13,14,15
PS Sample / File ID:R4097913-4 / 20240724093942 SDG:L1757957
OS Sample / File ID:L1757957-01 / 20240724093622 Analytical Batch:WG2326543
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
PD
Result
(dry)
DS
Result
(dry)
PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/kg mg/kg mg/kg %%%mg/kg mg/kg
Arsenic 101 15.6 117 100 1 80.0 -
120
Barium 101 107 199 90.9 1 80.0 -
120
Cadmium 101 2.49 99.8 95.9 1 80.0 -
120
Chromium 101 14.4 108 92.7 1 80.0 -
120
Selenium 101 1.91 107 103 1 80.0 -
120
Silver 20.3 U 18.1 89.0 1 80.0 -
120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4097314-2
RECOVERY _______________
L1757957-02,03,04,05,06,07,08
LCS Sample / File ID:R4097314-2 / 20240723084446 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326410
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Arsenic 100 94.6 94.6 80.0 - 120
Barium 100 102 102 80.0 - 120
Cadmium 100 102 102 80.0 - 120
Chromium 100 101 101 80.0 - 120
Lead 100 98.2 98.2 80.0 - 120
Selenium 100 96.4 96.4 80.0 - 120
Silver 20.0 18.0 90.2 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4097913-2
RECOVERY _______________
L1757957-01,09,10,11,12,13,14,15
LCS Sample / File ID:R4097913-2 / 20240724093443 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326543
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Arsenic 100 107 107 80.0 - 120
Barium 100 107 107 80.0 - 120
Cadmium 100 104 104 80.0 - 120
Chromium 100 105 105 80.0 - 120
Lead 100 104 104 80.0 - 120
Selenium 100 100 100 80.0 - 120
Silver 20.0 18.8 94.0 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 150 of 530
7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4099537-2
RECOVERY _______________
L1757957-16
LCS Sample / File ID:R4099537-2 / 20240729001907 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2327640
Instrument ID:ICP16 Dilution Factor:1
Analytical Method:6010B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l %%%%%
Arsenic 1.00 0.932 93.2 80.0 - 120
Barium 1.00 0.974 97.4 80.0 - 120
Cadmium 1.00 0.930 93.0 80.0 - 120
Chromium 1.00 0.943 94.3 80.0 - 120
Lead 1.00 0.899 89.9 80.0 - 120
Selenium 1.00 0.904 90.4 80.0 - 120
Silver 0.200 0.190 95.1 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4097314-3
L1757957-02,03,04,05,06,07,08
SD Sample / File ID:R4097314-3 / 20240723084807 SDG:L1757957
OS Sample / File ID:L1757594-01 / 20240723084627 Analytical Batch:WG2326410
Lab File ID:20240723084807 Dilution Factor:5
Instrument ID:ICP17 Matrix:Solid
Analytical Method:6010B
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Arsenic 1.66 13.4 0.000 10
Barium 123 90.7 26.0*10
Cadmium 0.609 12.2 1900 10
Chromium 7.10 16.5 133 10
Lead 4.45 14.6 229 10
Selenium U 15.3 0.000 10
Silver U 1.93 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4097913-3
L1757957-01,09,10,11,12,13,14,15
SD Sample / File ID:R4097913-3 / 20240724093802 SDG:L1757957
OS Sample / File ID:L1757957-01 / 20240724093622 Analytical Batch:WG2326543
Lab File ID:20240724093802 Dilution Factor:5
Instrument ID:ICP17 Matrix:Solid
Analytical Method:6010B
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Arsenic 15.6 12.3 21.5 10
Barium 107 105 2.15 10
Cadmium 2.49 2.36 5.13 10
Chromium 14.4 14.4 0.243 10
Lead 130 120 7.50 10
Selenium 1.91 U 0.000 10
Silver U U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 153 of 530
8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4099537-3
L1757957-16
SD Sample / File ID:R4099537-3 / 20240729002229 SDG:L1757957
OS Sample / File ID:L1758018-06 / 20240729002048 Analytical Batch:WG2327640
Lab File ID:20240729002229 Dilution Factor:5
Instrument ID:ICP16 Matrix:GW
Analytical Method:6010B
Analyte OS
Result
SD
Result RPD RPD
Limits
mg/l mg/l %%
Arsenic U U 0.000 10
Barium 0.0597 0.0550 7.84 10
Cadmium 0.00104 U 0.000 10
Chromium 0.00275 U 0.000 10
Lead U U 0.000 10
Selenium U U 0.000 10
Silver U U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16 Analytical Method:6010B
Matrix:GW Prep Method:3015
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Cadmium 7440-43-9 228.8020 0.000479 0.0020
Chromium 7440-47-3 267.7160 0.0014 0.01
Lead 7439-92-1 220.3530 0.002990 0.0060
Selenium 7782-49-2 196.09 0.007350 0.01
Silver 7440-22-4 328.0680 0.001540 0.0050
Arsenic 7440-38-2 189.0420 0.0044 0.01
Barium 7440-39-3 233.5270 0.000736 0.0050
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:6010B
Matrix:Solid Prep Method:3050B
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Lead 7439-92-1 220.3530 0.2080 0.50
Selenium 7782-49-2 196.09 0.7640 2
Silver 7440-22-4 328.0680 0.1270 1
Arsenic 7440-38-2 189.0420 0.5180 2
Barium 7440-39-3 233.5270 0.0852 0.50
Cadmium 7440-43-9 228.8020 0.0471 0.50
Chromium 7440-47-3 267.7160 0.1330 1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 156 of 530
10C-IN LINEAR DYNAMIC RANGE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP16 Date:01/25/24 15:25
Analyte LDR
ppm
ALUMINUM 500
ANTIMONY 10
ARSENIC 50
BARIUM 50
BERYLLIUM 10
BORON 50
CADMIUM 10
CALCIUM 1000
CHROMIUM 50
COBALT 50
COPPER 50
IRON 500
LEAD 100
LITHIUM 10
MAGNESIUM 1000
MANGANESE 20
MOLYBDENUM 20
NICKEL 50
PHOSPHORUS 200
POTASSIUM 500
SELENIUM 10
SILICON 100
SILVER 10
SODIUM 1000
STRONTIUM 20
SULFUR 200
THALLIUM 10
TIN 50
TITANIUM 50
VANADIUM 20
ZINC 20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 157 of 530
10C-IN LINEAR DYNAMIC RANGE
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Date:06/09/24 17:06
Analyte LDR
ppm
ALUMINUM 500
ANTIMONY 10
ARSENIC 50
BARIUM 50
BERYLLIUM 10
BORON 50
CADMIUM 10
CALCIUM 1000
CHROMIUM 50
COBALT 50
COPPER 50
IRON 500
LEAD 100
LITHIUM 10
MAGNESIUM 1000
MANGANESE 20
MOLYBDENUM 20
NICKEL 50
PHOSPHORUS 200
POTASSIUM 500
SELENIUM 10
SILICON 100
SILVER 10
SODIUM 1000
STRONTIUM 20
SULFUR 200
THALLIUM 10
TIN 50
TITANIUM 50
VANADIUM 20
ZINC 20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 158 of 530
12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP16 Calibration Start Date:07/28/24 17:05
Analytical Run:072824ICP16 Calibration End Date:07/28/24 17:15
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP160728241703 20240728170354 07/28/24 17:03
CAL STD1 20240728170534 07/28/24 17:05
CAL STD2 20240728170713 07/28/24 17:07
CAL STD3 20240728170852 07/28/24 17:08
CAL STD4 20240728171032 07/28/24 17:10
CAL STD5 20240728171211 07/28/24 17:12
CAL STD6 20240728171350 07/28/24 17:13
CAL STD7 20240728171528 07/28/24 17:15
ICV ICP160728241717 20240728171717 07/28/24 17:17
ICB ICP160728241718 20240728171855 07/28/24 17:18
ICB ICP160728241737 20240728173744 07/28/24 17:37
ICVLL ICP160728241742 20240728174239 07/28/24 17:42
ICSA ICP160728241744 20240728174419 07/28/24 17:44
ICSAB ICP160728241745 20240728174558 07/28/24 17:45
ICSA ICP160728242222 20240728222208 07/28/24 22:22
ICSAB ICP160728242223 20240728222348 07/28/24 22:23
CCV ICP160729240014 20240729001401 07/29/24 00:14
CCB ICP160729240015 20240729001542 07/29/24 00:15
BLANK R4099537-1 20240729001726 07/29/24 00:17 1 WG2327640
LCS R4099537-2 20240729001907 07/29/24 00:19 1 WG2327640
OS L1758018-06 20240729002048 07/29/24 00:20
SD R4099537-3 20240729002229 07/29/24 00:22 5 WG2327640
MS R4099537-4 20240729002410 07/29/24 00:24 1 WG2327640
MSD R4099537-5 20240729002551 07/29/24 00:25 1 WG2327640
L1757930-14 L1757930-14 20240729002733 07/29/24 00:27 1 WG2327640
L1757930-15 L1757930-15 20240729002914 07/29/24 00:29 1 WG2327640
L1757930-16 L1757930-16 20240729003055 07/29/24 00:30 1 WG2327640
CCV ICP160729240034 20240729003418 07/29/24 00:34
CCB ICP160729240035 20240729003559 07/29/24 00:35
EB-1-071624 L1757957-16 20240729004607 07/29/24 00:46 1 WG2327640
CCV ICP160729240054-2 20240729005434-2 07/29/24 00:54
CCB ICP160729240056-2 20240729005616-2 07/29/24 00:56
ICSA ICP160729240123 20240729012326 07/29/24 01:23
ICSAB ICP160729240125 20240729012508 07/29/24 01:25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 159 of 530
12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Calibration Start Date:07/23/24 07:38
Analytical Run:072324ICP17 Calibration End Date:07/23/24 07:48
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP170723240736 20240723073630 07/23/24 07:36
CAL STD1 20240723073810 07/23/24 07:38
CAL STD2 20240723073950 07/23/24 07:39
CAL STD3 20240723074130 07/23/24 07:41
CAL STD4 20240723074310 07/23/24 07:43
CAL STD5 20240723074451 07/23/24 07:44
CAL STD6 20240723074630 07/23/24 07:46
ICV ICP170723240749 20240723074959 07/23/24 07:49
ICB ICP170723240751 20240723075138 07/23/24 07:51
CCV ICP170723240753 20240723075322 07/23/24 07:53
CCB ICP170723240755 20240723075501 07/23/24 07:55
ICVLL ICP170723240756 20240723075640 07/23/24 07:56
ICSA ICP170723240758 20240723075820 07/23/24 07:58
ICSAB ICP170723240800 20240723080000 07/23/24 08:00
BLANK R4097314-1 20240723084305 07/23/24 08:43 1 WG2326410
LCS R4097314-2 20240723084446 07/23/24 08:44 1 WG2326410
OS L1757594-01 20240723084627 07/23/24 08:46
L1757594-01 L1757594-01 20240723084627 07/23/24 08:46 1 WG2326410
SD R4097314-3 20240723084807 07/23/24 08:48 5 WG2326410
PS R4097314-4 20240723084948 07/23/24 08:49 1 WG2326410
MS R4097314-5 20240723085128 07/23/24 08:51 1 WG2326410
MSD R4097314-6 20240723085308 07/23/24 08:53 1 WG2326410
L1757594-02 L1757594-02 20240723085806 07/23/24 08:58 1 WG2326410
CCV ICP170723240859 20240723085945 07/23/24 08:59
CCB ICP170723240901 20240723090124 07/23/24 09:01
L1757594-03 L1757594-03 20240723091757 07/23/24 09:17 1 WG2326410
L1757594-04 L1757594-04 20240723091940 07/23/24 09:19 1 WG2326410
L1757594-05 L1757594-05 20240723092125 07/23/24 09:21 1 WG2326410
L1757594-13 L1757594-13 20240723092307 07/23/24 09:23 1 WG2326410
S-3 (6-12)L1757957-02 20240723092446 07/23/24 09:24 1 WG2326410
S-30 (6-12)L1757957-03 20240723092626 07/23/24 09:26 1 WG2326410
S-9 (0-6)L1757957-04 20240723092805 07/23/24 09:28 1 WG2326410
S-8 (0-6)L1757957-05 20240723092944 07/23/24 09:29 1 WG2326410
S-7 (0-6)L1757957-06 20240723093123 07/23/24 09:31 1 WG2326410
S-7 (6-12)L1757957-07 20240723093303 07/23/24 09:33 1 WG2326410
CCV ICP170723240934 20240723093448 07/23/24 09:34
CCB ICP170723240936 20240723093631 07/23/24 09:36
CCV ICP170723240954 20240723095455 07/23/24 09:54
CCB ICP170723240956 20240723095634 07/23/24 09:56
L1754608-01 L1754608-01 20240723095815 07/23/24 09:58 1 WG2325773
L1756171-01 L1756171-01 20240723095957 07/23/24 09:59 .1 WG2325773
L1756180-11 L1756180-11 20240723100136 07/23/24 10:01 1 WG2325773
L1756226-01 L1756226-01 20240723100316 07/23/24 10:03 1 WG2325773
L1756298-08 L1756298-08 20240723100637 07/23/24 10:06 1 WG2327279
S-6 (0-6)L1757957-08 20240723100819 07/23/24 10:08 1 WG2326410
CCV ICP170723241010 20240723101004 07/23/24 10:10
CCB ICP170723241012 20240723101207 07/23/24 10:12
CCVLL ICP170723241337 20240723133759 07/23/24 13:37
ICSA ICP170723241339 20240723133940 07/23/24 13:39
ICSAB ICP170723241341 20240723134121 07/23/24 13:41
CCB ICP170723241433-2 20240723143356-2 07/23/24 14:33
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 160 of 530
12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Calibration Start Date:07/23/24 07:38
Analytical Run:072324ICP17 Calibration End Date:07/23/24 07:48
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
PS R4097314-7 20240723144045 07/23/24 14:40 1 WG2326410
CCB ICP170723241445-2 20240723144552-2 07/23/24 14:45
ICSA ICP170723241526-2 20240723152636-2 07/23/24 15:26
ICSAB ICP170723241528-2 20240723152817-2 07/23/24 15:28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 161 of 530
12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:6010B
Instrument ID:ICP17 Calibration Start Date:07/24/24 06:36
Analytical Run:072424ICP17 Calibration End Date:07/24/24 06:46
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP170724240634 20240724063444 07/24/24 06:34
CAL STD1 20240724063622 07/24/24 06:36
CAL STD2 20240724063800 07/24/24 06:38
CAL STD3 20240724063940 07/24/24 06:39
CAL STD4 20240724064120 07/24/24 06:41
CAL STD5 20240724064300 07/24/24 06:43
CAL STD6 20240724064439 07/24/24 06:44
ICV ICP170724240648-2 20240724064807-2 07/24/24 06:48
ICB ICP170724240649-2 20240724064946-2 07/24/24 06:49
ICVLL ICP170724240654-2 20240724065455-2 07/24/24 06:54
ICSA ICP170724240656-2 20240724065635-2 07/24/24 06:56
ICSAB ICP170724240658-2 20240724065815-2 07/24/24 06:58
CCV ICP170724240929-2 20240724092941-2 07/24/24 09:29
CCB ICP170724240931-2 20240724093120-2 07/24/24 09:31
BLANK R4097913-1 20240724093303 07/24/24 09:33 1 WG2326543
LCS R4097913-2 20240724093443 07/24/24 09:34 1 WG2326543
S-3 (0-6)L1757957-01 20240724093622 07/24/24 09:36 1 WG2326543
SD R4097913-3 20240724093802 07/24/24 09:38 5 WG2326543
PS R4097913-4 20240724093942 07/24/24 09:39 1 WG2326543
MS R4097913-5 20240724094121 07/24/24 09:41 1 WG2326543
MSD R4097913-6 20240724094301 07/24/24 09:43 1 WG2326543
L1757151-02 L1757151-02 20240724094441 07/24/24 09:44 1 WG2326543
L1757597-09 L1757597-09 20240724094621 07/24/24 09:46 1 WG2326543
L1757597-10 L1757597-10 20240724094801 07/24/24 09:48 1 WG2326543
CCV ICP170724240949-2 20240724094941-2 07/24/24 09:49
CCB ICP170724240951-2 20240724095120-2 07/24/24 09:51
L1757687-02 L1757687-02 20240724095300 07/24/24 09:53 1 WG2326543
S-5 (0-6)L1757957-09 20240724095440 07/24/24 09:54 1 WG2326543
S-4 (0-6)L1757957-10 20240724095620 07/24/24 09:56 1 WG2326543
S-2 (0-6)L1757957-12 20240724095939 07/24/24 09:59 1 WG2326543
S-1 (0-6)L1757957-13 20240724100118 07/24/24 10:01 1 WG2326543
S-1 (6-12)L1757957-14 20240724100258 07/24/24 10:02 1 WG2326543
SS-1 (6-12)L1757957-15 20240724100438 07/24/24 10:04 1 WG2326543
CCV ICP170724241007 20240724100757 07/24/24 10:07
CCB ICP170724241009 20240724100937 07/24/24 10:09
ICSA ICP170724241358-2 20240724135816-2 07/24/24 13:58
ICSAB ICP170724241359-2 20240724135958-2 07/24/24 13:59
CCB ICP170724241450-2 20240724145015-2 07/24/24 14:50
S-31 (0-6)L1757957-11 20240724145342 07/24/24 14:53 5 WG2326543
CCB ICP170724241510-2 20240724151059-2 07/24/24 15:10
ICSA ICP170724242034-2 20240724203456-2 07/24/24 20:34
ICSAB ICP170724242036-2 20240724203641-2 07/24/24 20:36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 162 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.01 .00969597 97 0.25 .24598 98.40
BARIUM 0.0050 .005203384 104 0.25 .2620982 105
CADMIUM 0.0020 .002121984 106 0.05 .04990672 99.80
CHROMIUM 0.01 .01038001 104 0.25 .2529953 101
LEAD 0.0050 .005747298 115 0.50 .4786379 95.70
SELENIUM 0.01 .01027092 103 0.05 .04242848 84.90
SILVER 0.0050 .004739972 94.80 0.05 .05244649 105
File ID: 20240728170534 20240728170713
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.50 .4739409 94.80 1 .9905375 99.10
BARIUM 0.50 .503004 101 1 1.027051 103
CADMIUM 0.10 .09504619 95 0.20 .197085 98.50
CHROMIUM 0.50 .4827895 96.60 1 1.004623 100
LEAD 1 .9284019 92.80 2 1.943804 97.20
SELENIUM 0.10 .09396459 94 0.20 .1888848 94.40
SILVER 0.10 .1006736 101 0.20 .2068945 103
File ID: 20240728170852 20240728171032
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 164 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 2.50 2.52454 101 5 4.99243 99.80
BARIUM 2.50 2.545351 102 5 4.971009 99.40
CADMIUM 0.50 .5061493 101 1 .9980081 99.80
CHROMIUM 2.50 2.557077 102 5 4.972107 99.40
LEAD 5 5.034535 101 10 10.0022 100
SELENIUM 0.50 .5012184 100 1 1.002593 100
SILVER 0.50 .5072748 101 1 .9947953 99.50
File ID: 20240728171211 20240728171350
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 165 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.01 .01081694 108 0.25 .2419299 96.80
BARIUM 0.0050 .005276156 106 0.25 .2625818 105
CADMIUM 0.0020 .001904555 95.20 0.05 .05097391 102
CHROMIUM 0.01 .01063682 106 0.25 .2585457 103
LEAD 0.0050 .004656517 93.10 0.50 .498119 99.60
SELENIUM 0.01 .009658243 96.60 0.05 .04935572 98.70
SILVER 0.0050 .004621082 92.40 0.05 .05013787 100
File ID: 20240723073810 20240723073950
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 166 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.50 .4810824 96.20 1 .9495334 95
BARIUM 0.50 .5237228 105 1 1.024142 102
CADMIUM 0.10 .1023379 102 0.20 .2021633 101
CHROMIUM 0.50 .5168869 103 1 1.020071 102
LEAD 1 1.001446 100 2 1.978245 98.90
SELENIUM 0.10 .09354052 93.50 0.20 .1925015 96.30
SILVER 0.10 .1001903 100 0.20 .1988789 99.40
File ID: 20240723074130 20240723074310
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 167 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 2.50 2.473369 98.90 5 5.025702 101
BARIUM 2.50 2.535759 101 5 4.97429 99.50
CADMIUM 0.50 .5000246 100 1 .9992728 99.90
CHROMIUM 2.50 2.531567 101 5 4.978085 99.60
LEAD 5 5.009126 100 10 9.999738 100
SELENIUM 0.50 .4995672 99.90 1 1.002398 100
SILVER 0.50 .5025888 101 1 .9989058 99.90
File ID: 20240723074451 20240723074630
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.01 .008449537 84.50 0.25 .2539184 102
BARIUM 0.0050 .005465071 109 0.25 .2572933 103
CADMIUM 0.0020 .002021316 101 0.05 .04958779 99.20
CHROMIUM 0.01 .01026609 103 0.25 .2543759 102
LEAD 0.0050 .005159292 103 0.50 .4961796 99.20
SELENIUM 0.01 .008206512 82.10 0.05 .04646984 92.90
SILVER 0.0050 .004932559 98.70 0.05 .0497224 99.40
File ID: 20240724063622 20240724063800
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 169 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.50 .5176699 104 1 1.029716 103
BARIUM 0.50 .5155824 103 1 1.028267 103
CADMIUM 0.10 .0990662 99.10 0.20 .199967 100
CHROMIUM 0.50 .5078332 102 1 1.023878 102
LEAD 1 1.002511 100 2 2.014325 101
SELENIUM 0.10 .09993797 99.90 0.20 .1926102 96.30
SILVER 0.10 .09964153 99.60 0.20 .1999583 100
File ID: 20240724063940 20240724064120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 170 of 530
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 2.50 2.49791 99.90 5 4.993142 99.90
BARIUM 2.50 2.507092 100 5 4.988877 99.80
CADMIUM 0.50 .4937777 98.80 1 1.003232 100
CHROMIUM 2.50 2.505226 100 5 4.991609 99.80
LEAD 5 4.966633 99.30 10 10.01376 100
SELENIUM 0.50 .4805008 96.10 1 1.011428 101
SILVER 0.50 .4931855 98.60 1 1.003466 100
File ID: 20240724064300 20240724064439
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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16A-IN INITIAL
CALIBRATION
SDG:L1757957 Calibration (begin) date/time:07/28/24 17:05
Instrument ID:ICP16 Calibration (end) date/time:07/28/24 17:15
Analytical Method:6010B Analytical Run:072824ICP16
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
ARSENIC 189.042 8 5 0.999965 190.594 -0.679692
BARIUM 233.527 8 5 0.999906 7737.806 -1.131318
CADMIUM 228.802 8 5 0.999954 2078.961 1.389613
CHROMIUM 267.716 8 5 0.999892 3120.744 -5.137234
LEAD 220.353 8 5 0.999939 464.6032 -0.190903
SELENIUM 196.09 8 5 0.999862 109.0383 0.529
SILVER 328.068 8 5 0.999917 4940.834 11.27011
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 172 of 530
16A-IN INITIAL
CALIBRATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 07:38
Instrument ID:ICP17 Calibration (end) date/time:07/23/24 07:48
Analytical Method:6010B Analytical Run:072324ICP17
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
ARSENIC 189.042 8 5 0.999894 134.3466 -1.061082
BARIUM 233.527 8 5 0.99992 8067.508 -1.080119
CADMIUM 228.802 8 5 0.999993 3752.136 1.66757
CHROMIUM 267.716 8 5 0.999945 2807.386 -9.046812
LEAD 220.353 8 5 0.999997 606.6619 1.078479
SELENIUM 196.09 8 5 0.999936 75.52792 -0.380616
SILVER 328.068 8 5 0.999994 5482.323 -5.823416
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 173 of 530
16A-IN INITIAL
CALIBRATION
SDG:L1757957 Calibration (begin) date/time:07/24/24 06:36
Instrument ID:ICP17 Calibration (end) date/time:07/24/24 06:46
Analytical Method:6010B Analytical Run:072424ICP17
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
ARSENIC 189.042 8 5 0.999969 127.3698 -0.425797
BARIUM 233.527 8 5 0.999969 8316.901 -3.338691
CADMIUM 228.802 8 5 0.999969 3968.073 1.054535
CHROMIUM 267.716 8 5 0.999982 2904.532 -9.766368
LEAD 220.353 8 5 0.999991 583.8614 0.806646
SELENIUM 196.09 8 5 0.999646 75.60863 -0.306098
SILVER 328.068 8 5 0.999964 5875.574 -6.20754
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7470A Mercury
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 175 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:20240720235238 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA9 Preparation Date/Time:07/19/24 18:14
Analytical Batch:WG2325902 Analysis Date/Time:07/20/24 23:52
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 U 0.000100 0.000200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 176 of 530
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096472-1
Lab Sample ID:R4096472-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20240720225247 Received Date/Time:_______________
Instrument ID:CVAA9 Preparation Date/Time:07/19/24 18:14
Analytical Batch:WG2325902 Analysis Date/Time:07/20/24 22:52
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 U 0.000100 0.000200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096472-2
Lab Sample ID:R4096472-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20240720230012 Received Date/Time:_______________
Instrument ID:CVAA9 Preparation Date/Time:07/19/24 18:14
Analytical Batch:WG2325902 Analysis Date/Time:07/20/24 23:00
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00296 0.000100 0.000200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096472-4
Lab Sample ID:R4096472-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/17/24 11:40
Lab File ID:20240720230732 Received Date/Time:07/17/24 17:00
Instrument ID:CVAA9 Preparation Date/Time:07/19/24 18:14
Analytical Batch:WG2325902 Analysis Date/Time:07/20/24 23:07
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00308 0.000100 0.000200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096472-5
Lab Sample ID:R4096472-5 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/17/24 11:40
Lab File ID:20240720231003 Received Date/Time:07/17/24 17:00
Instrument ID:CVAA9 Preparation Date/Time:07/19/24 18:14
Analytical Batch:WG2325902 Analysis Date/Time:07/20/24 23:10
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00300 0.000100 0.000200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096472-3
Lab Sample ID:R4096472-3 SDG:L1757957
Client Sample ID:SD Collected Date/Time:07/17/24 11:40
Lab File ID:20240720230513 Received Date/Time:07/17/24 17:00
Instrument ID:CVAA9 Preparation Date/Time:07/19/24 18:14
Analytical Batch:WG2325902 Analysis Date/Time:07/20/24 23:05
Dilution Factor:5 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 U 0.000500 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Concentration Units:mg/L
ICV ICVLL CCV
Sample ID:CVAA90720241918 CVAA90720241928 CVAA90720242225-2
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.005147694 103 1.830000 0.0002 0.000194409
7
97.2
0 2.250000 0.0050 0.004973853 99.5
0 1.490000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Concentration Units:mg/L
CCV CCV CCV
Sample ID:CVAA90720242255-2 CVAA90720242325 CVAA90720242355
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.004931054 98.6
0 1.900000 0.0050 0.004938811 98.8
0 1.950000 0.0050 0.004852142 97 1.850000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20240720192104 20240720222751-2 20240720225247 20240720225745-2
Analyte mg/L mg/L mg/l mg/L
MERCURY 0.00000676337
5 U 0.00000972998 U U 0.000007416017 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Sample ID:CCB Result CCB Qual CCB Result CCB Qual
File ID:20240720232734 20240720235736
Analyte mg/L mg/L
MERCURY 0.00001032023 U 0.00001065755 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4096472-4
L1757957-16 R4096472-5
MS Sample / File ID:R4096472-4 / 20240720230732 SDG:L1757957
MSD Sample / File ID:R4096472-5 / 20240720231003 Analytical Batch:WG2325902
OS Sample / File ID:L1757658-03 / 20240720230242 Matrix:GW
Instrument ID:CVAA9
Analytical Method:7470A
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 U 0.00308 0.00300 103 100 1 75.0 - 125 2.64 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4096472-2
RECOVERY _______________
L1757957-16
LCS Sample / File ID:R4096472-2 / 20240720230012 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2325902
Instrument ID:CVAA9 Dilution Factor:1
Analytical Method:7470A Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l %%%%%
Mercury 0.00300 0.00296 98.7 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4096472-3
L1757957-16
SD Sample / File ID:R4096472-3 / 20240720230513 SDG:L1757957
OS Sample / File ID:L1757658-03 / 20240720230242 Analytical Batch:WG2325902
Lab File ID:20240720230513 Dilution Factor:5
Instrument ID:CVAA9 Matrix:GW
Analytical Method:7470A
Analyte OS
Result
SD
Result RPD RPD
Limits
mg/l mg/l %%
Mercury U U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16 Analytical Method:7470A
Matrix:GW Prep Method:7470A
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Mercury 7439-97-6 253.70 0.0001 0.0002
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10C-IN LINEAR DYNAMIC RANGE
SDG:L1757957 Analytical Method:7470A
Instrument ID:CVAA9 Date:07/10/23 14:11
Analyte LDR
ppm
MERCURY 0.01
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:7470A
Instrument ID:CVAA9 Calibration Start Date:07/20/24 18:56
Analytical Run:072024CVAA9 WB Calibration End Date:07/20/24 19:08
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK CVAA90720241853 20240720185338 07/20/24 18:53
CAL STD 0.2 20240720185604 07/20/24 18:56
CAL STD 0.4 20240720185832 07/20/24 18:58
CAL STD 1.0 20240720190100 07/20/24 19:01
CAL STD 2.0 20240720190329 07/20/24 19:03
CAL STD 5.0 20240720190558 07/20/24 19:05
CAL STD 10.0 20240720190825 07/20/24 19:08
ICV CVAA90720241918 20240720191835 07/20/24 19:18
ICB CVAA90720241921 20240720192104 07/20/24 19:21
ICVLL CVAA90720241928 20240720192825 07/20/24 19:28
CCV CVAA90720242225-2 20240720222523-2 07/20/24 22:25
CCB CVAA90720242227-2 20240720222751-2 07/20/24 22:27
BLANK R4096472-1 20240720225247 07/20/24 22:52 1 WG2325902
CCV CVAA90720242255-2 20240720225518-2 07/20/24 22:55
CCB CVAA90720242257-2 20240720225745-2 07/20/24 22:57
LCS R4096472-2 20240720230012 07/20/24 23:00 1 WG2325902
OS L1757658-03 20240720230242 07/20/24 23:02
L1757658-03 L1757658-03 20240720230242 07/20/24 23:02 1 WG2325902
SD R4096472-3 20240720230513 07/20/24 23:05 5 WG2325902
MS R4096472-4 20240720230732 07/20/24 23:07 1 WG2325902
MSD R4096472-5 20240720231003 07/20/24 23:10 1 WG2325902
L1757594-06 L1757594-06 20240720231233 07/20/24 23:12 1 WG2325902
L1757594-07 L1757594-07 20240720231503 07/20/24 23:15 1 WG2325902
L1757594-08 L1757594-08 20240720231734 07/20/24 23:17 1 WG2325902
L1757594-09 L1757594-09 20240720232004 07/20/24 23:20 1 WG2325902
L1757594-10 L1757594-10 20240720232235 07/20/24 23:22 1 WG2325902
CCV CVAA90720242325 20240720232506 07/20/24 23:25
CCB CVAA90720242327 20240720232734 07/20/24 23:27
L1757658-01 L1757658-01 20240720233000 07/20/24 23:30 1 WG2325902
L1757658-02 L1757658-02 20240720233230 07/20/24 23:32 1 WG2325902
L1757658-04 L1757658-04 20240720233501 07/20/24 23:35 1 WG2325902
L1757658-05 L1757658-05 20240720233731 07/20/24 23:37 1 WG2325902
L1757658-06 L1757658-06 20240720234002 07/20/24 23:40 1 WG2325902
L1757660-01 L1757660-01 20240720234233 07/20/24 23:42 1 WG2325902
L1757660-02 L1757660-02 20240720234504 07/20/24 23:45 1 WG2325902
L1757660-03 L1757660-03 20240720234735 07/20/24 23:47 1 WG2325902
L1757928-01 L1757928-01 20240720235006 07/20/24 23:50 1 WG2325902
EB-1-071624 L1757957-16 20240720235238 07/20/24 23:52 1 WG2325902
CCV CVAA90720242355 20240720235509 07/20/24 23:55
CCB CVAA90720242357 20240720235736 07/20/24 23:57
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/L mg/L %mg/L mg/L %
MERCURY 0.0002 .0001645362 82.30 0.0004 .0003962955 99.10
File ID: 20240720185604 20240720185832
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/L mg/L %mg/L mg/L %
MERCURY 0.0010 .001010582 101 0.0020 .001981997 99.10
File ID: 20240720190100 20240720190329
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/L mg/L %mg/L mg/L %
MERCURY 0.0050 .005145581 103 0.01 .00993061 99.30
File ID: 20240720190558 20240720190825
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16A-IN INITIAL
CALIBRATION
SDG:L1757957 Calibration (begin) date/time:07/20/24 18:56
Instrument ID:CVAA9 Calibration (end) date/time:07/20/24 19:08
Analytical Method:7470A Analytical Run:072024CVAA9 WB
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
MERCURY 253.7 0 5 0.999779 9.562877 0.000283
Calibration Type
0 = Linear Regression
Weightage
5 = None
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7471A Mercury
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:20240723143229 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:32
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0548 0.0183 0.0406
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:20240721185047 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA7 Preparation Date/Time:07/20/24 15:03
Analytical Batch:WG2326415 Analysis Date/Time:07/21/24 18:50
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):92.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.175 0.0196 0.0435
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:20240723144751 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:47
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.29 g
Total Solids (%):92.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.174 0.0194 0.0431
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:20240723145531 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:55
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):97.8 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0848 0.0184 0.0409
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:20240723145808 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:58
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):98.2 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0529 0.0183 0.0407
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:20240723150046 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:00
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):94.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.638 0.0191 0.0426
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:20240723150324 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:03
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.29 g
Total Solids (%):93.8 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.674 0.0192 0.0426
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:20240723150601 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:06
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.29 g
Total Solids (%):98.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0733 0.0183 0.0408
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:20240723150839 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:08
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):98.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0474 0.0182 0.0405
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:20240723151606 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:16
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):97.3 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.173 0.0185 0.0411
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:20240723151844 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:18
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.29 g
Total Solids (%):97.2 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.214 0.0185 0.0411
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:20240723152121 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:21
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):95.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0740 0.0189 0.0421
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:20240723152358 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:23
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):93.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.238 0.0193 0.0430
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:20240723152636 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:26
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.33 g
Total Solids (%):91.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.318 0.0198 0.0440
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:20240723152915 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 15:29
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.35 g
Total Solids (%):85.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.552 0.0210 0.0467
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096524-1
Lab Sample ID:R4096524-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20240721173016 Received Date/Time:_______________
Instrument ID:CVAA7 Preparation Date/Time:07/20/24 15:00
Analytical Batch:WG2326415 Analysis Date/Time:07/21/24 17:30
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 U 0.0180 0.0400
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097489-1
Lab Sample ID:R4097489-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20240723142717 Received Date/Time:_______________
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 19:46
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:27
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 U 0.0180 0.0400
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096524-2
Lab Sample ID:R4096524-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20240721173235 Received Date/Time:_______________
Instrument ID:CVAA7 Preparation Date/Time:07/20/24 15:00
Analytical Batch:WG2326415 Analysis Date/Time:07/21/24 17:32
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.501 0.0180 0.0400
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097489-2
Lab Sample ID:R4097489-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20240723142953 Received Date/Time:_______________
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 19:46
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:29
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.474 0.0180 0.0400
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096524-4
Lab Sample ID:R4096524-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/15/24 10:00
Lab File ID:20240721174008 Received Date/Time:07/17/24 09:00
Instrument ID:CVAA7 Preparation Date/Time:07/20/24 15:00
Analytical Batch:WG2326415 Analysis Date/Time:07/21/24 17:40
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.536 0.0180 0.0400
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097489-4
Lab Sample ID:R4097489-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:20240723143743 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 19:46
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:37
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.530 0.0183 0.0406
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096524-5
Lab Sample ID:R4096524-5 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/15/24 10:00
Lab File ID:20240721174737 Received Date/Time:07/17/24 09:00
Instrument ID:CVAA7 Preparation Date/Time:07/20/24 15:00
Analytical Batch:WG2326415 Analysis Date/Time:07/21/24 17:47
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.517 0.0180 0.0400
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097489-5
Lab Sample ID:R4097489-5 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:20240723144513 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 19:46
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:45
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.33 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.498 0.0183 0.0406
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4096524-3
Lab Sample ID:R4096524-3 SDG:L1757957
Client Sample ID:SD Collected Date/Time:07/15/24 10:00
Lab File ID:20240721173737 Received Date/Time:07/17/24 09:00
Instrument ID:CVAA7 Preparation Date/Time:07/20/24 15:03
Analytical Batch:WG2326415 Analysis Date/Time:07/21/24 17:37
Dilution Factor:5 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.33 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 U 0.0900 0.200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4097489-3
Lab Sample ID:R4097489-3 SDG:L1757957
Client Sample ID:SD Collected Date/Time:07/16/24 09:30
Lab File ID:20240723143506 Received Date/Time:07/18/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:07/21/24 21:10
Analytical Batch:WG2326412 Analysis Date/Time:07/23/24 14:35
Dilution Factor:5 Prep Method:7471A
Analytical Method:7471A Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):98.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 U 0.0913 0.203
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Concentration Units:mg/kg
ICV ICVLL CCV
Sample ID:CVAA70721241540 CVAA70721241550 CVAA70721241712-2
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.005074854 101 6.210000 0.0002 0.000234381
9 117 6.630000 0.0050 0.005093323 102 3.880000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Concentration Units:mg/kg
CCV CCV CCV
Sample ID:CVAA70721241742-2 CVAA70721241812 CVAA70721241843
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.005070738 101 4.550000 0.0050 0.005040214 101 4.360000 0.0050 0.004979943 99.6
0 4.100000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Concentration Units:mg/kg
CCV
Sample ID:CVAA70721241916
Analyte True Found %R %RSD
MERCURY 0.0050 0.00489528
2
97.9
0 3.440000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Concentration Units:mg/kg
ICV CCV ICVLL
Sample ID:CVAA100723241401 CVAA100723241406 CVAA100723241411
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.00507042
6 101 1.890000 0.0050 0.00502235
5 100 1.690000 0.0002 0.00022265
07 111 1.880000
ICV Limits:90 - 110 CCV Limits:90 - 110 ICVLL Limits:70 - 130
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Concentration Units:mg/kg
CCV CCV CCV
Sample ID:CVAA100723241440 CVAA100723241511 CVAA100723241542
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.00500592
3 100 2.290000 0.0050 0.004903476 98.10 2.450000 0.0050 0.004842582 96.9
0 2.630000
ICV Limits:90 - 110 CCV Limits:90 - 110 ICVLL Limits:70 - 130
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20240721154301 20240721171511-2 20240721173016 20240721174508-2
Analyte mg/kg mg/kg mg/kg mg/kg
MERCURY 0.0000092220
5 U 0.00000994791
7 U U 0.00000703896
6 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Sample ID:CCB Result CCB Qual CCB Result CCB Qual CCB Result CCB Qual
File ID:20240721181520 20240721184626 20240721191831
Analyte mg/kg mg/kg mg/kg
MERCURY 0.00000256730
4 U 0.00000583103
7 U 0.00001123977 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20240723140433 20240723140923 20240723142717 20240723144258
Analyte mg/kg mg/kg mg/kg mg/kg
MERCURY -0.0000052447
62 U -0.00000410109
9 U U -0.0000042883
77 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Sample ID:CCB Result CCB Qual CCB Result CCB Qual
File ID:20240723151353 20240723154503
Analyte mg/kg mg/kg
MERCURY -0.0000043855
05 U -0.0000050027
18 U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4096524-4
L1757957-02 R4096524-5
MS Sample / File ID:R4096524-4 / 20240721174008 SDG:L1757957
MSD Sample / File ID:R4096524-5 / 20240721174737 Analytical Batch:WG2326415
OS Sample / File ID:L1757487-26 / 20240721173507 Matrix:Solid
Instrument ID:CVAA7
Analytical Method:7471A
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 0.0353 0.536 0.517 100 96.4 1 75.0 - 125 3.61 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4097489-4
L1757957-01,03,04,05,06,07,08,09,10,11,12,13,14,15 R4097489-5
MS Sample / File ID:R4097489-4 / 20240723143743 SDG:L1757957
MSD Sample / File ID:R4097489-5 / 20240723144513 Analytical Batch:WG2326412
OS Sample / File ID:L1757957-01 / 20240723143229 Matrix:Solid
Instrument ID:CVAA10
Analytical Method:7471A
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.507 0.0548 0.530 0.498 93.8 87.3 1 75.0 - 125 6.39 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4096524-2
RECOVERY _______________
L1757957-02
LCS Sample / File ID:R4096524-2 / 20240721173235 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326415
Instrument ID:CVAA7 Dilution Factor:1
Analytical Method:7471A Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Mercury 0.500 0.501 100 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4097489-2
RECOVERY _______________
L1757957-01,03,04,05,06,07,08,09,10,11,12,13,14,15
LCS Sample / File ID:R4097489-2 / 20240723142953 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2326412
Instrument ID:CVAA10 Dilution Factor:1
Analytical Method:7471A Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Mercury 0.500 0.474 94.9 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4096524-3
L1757957-02
SD Sample / File ID:R4096524-3 / 20240721173737 SDG:L1757957
OS Sample / File ID:L1757487-26 / 20240721173507 Analytical Batch:WG2326415
Lab File ID:20240721173737 Dilution Factor:5
Instrument ID:CVAA7 Matrix:Solid
Analytical Method:7471A
Analyte OS
Result
SD
Result RPD RPD
Limits
mg/kg mg/kg %%
Mercury 0.0353 U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4097489-3
L1757957-01,03,04,05,06,07,08,09,10,11,12,13,14,15
SD Sample / File ID:R4097489-3 / 20240723143506 SDG:L1757957
OS Sample / File ID:L1757957-01 / 20240723143229 Analytical Batch:WG2326412
Lab File ID:20240723143506 Dilution Factor:5
Instrument ID:CVAA10 Matrix:Solid
Analytical Method:7471A
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Mercury 0.0548 U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:7471A
Matrix:Solid Prep Method:7471A
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Mercury 7439-97-6 253.70 0.0180 0.04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10C-IN LINEAR DYNAMIC RANGE
SDG:L1757957 Analytical Method:7471A
Instrument ID:CVAA7 Date:06/27/19 15:34
Analyte LDR
ppm
MERCURY 0.01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:7471A
Instrument ID:CVAA7 Calibration Start Date:07/21/24 15:16
Analytical Run:072124CVAA7 S Calibration End Date:07/21/24 15:26
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK CVAA70721241514 20240721151427 07/21/24 15:14
CAL STD 0.2 20240721151654 07/21/24 15:16
CAL STD 0.4 20240721151925 07/21/24 15:19
CAL STD 1.0 20240721152155 07/21/24 15:21
CAL STD 2.0 20240721152425 07/21/24 15:24
CAL STD 5.0 20240721152657 07/21/24 15:26
ICV CVAA70721241540 20240721154028 07/21/24 15:40
ICB CVAA70721241543 20240721154301 07/21/24 15:43
ICVLL CVAA70721241550 20240721155028 07/21/24 15:50
CCV CVAA70721241712-2 20240721171242-2 07/21/24 17:12
CCB CVAA70721241715-2 20240721171511-2 07/21/24 17:15
L1757597-09 L1757597-09 20240721172513 07/21/24 17:25 1 WG2325860
L1757597-10 L1757597-10 20240721172745 07/21/24 17:27 1 WG2325860
BLANK R4096524-1 20240721173016 07/21/24 17:30 1 WG2326415
LCS R4096524-2 20240721173235 07/21/24 17:32 1 WG2326415
OS L1757487-26 20240721173507 07/21/24 17:35
SD R4096524-3 20240721173737 07/21/24 17:37 5 WG2326415
MS R4096524-4 20240721174008 07/21/24 17:40 1 WG2326415
CCV CVAA70721241742-2 20240721174239-2 07/21/24 17:42
CCB CVAA70721241745-2 20240721174508-2 07/21/24 17:45
MSD R4096524-5 20240721174737 07/21/24 17:47 1 WG2326415
L1757594-01 L1757594-01 20240721175741 07/21/24 17:57 1 WG2326415
L1757594-02 L1757594-02 20240721180012 07/21/24 18:00 1 WG2326415
L1757594-03 L1757594-03 20240721180244 07/21/24 18:02 1 WG2326415
L1757594-04 L1757594-04 20240721180516 07/21/24 18:05 1 WG2326415
L1757594-05 L1757594-05 20240721180747 07/21/24 18:07 1 WG2326415
L1757618-01 L1757618-01 20240721181019 07/21/24 18:10 1 WG2326415
CCV CVAA70721241812 20240721181250 07/21/24 18:12
CCB CVAA70721241815 20240721181520 07/21/24 18:15
CCV CVAA70721241843 20240721184356 07/21/24 18:43
CCB CVAA70721241846 20240721184626 07/21/24 18:46
S-3 (6-12)L1757957-02 20240721185047 07/21/24 18:50 1 WG2326415
BLANK R4096528-1 20240721185319 07/21/24 18:53 1 WG2327092
LCS R4096528-2 20240721185550 07/21/24 18:55 1 WG2327092
OS L1758747-04 20240721185822 07/21/24 18:58
L1758747-04 L1758747-04 20240721185822 07/21/24 18:58 1 WG2327092
SD R4096528-3 20240721190053 07/21/24 19:00 5 WG2327092
MS R4096528-4 20240721190325 07/21/24 19:03 1 WG2327092
MSD R4096528-5 20240721190556 07/21/24 19:05 1 WG2327092
L1758747-01 L1758747-01 20240721190828 07/21/24 19:08 1 WG2327092
L1758747-02 L1758747-02 20240721191100 07/21/24 19:11 1 WG2327092
L1758747-03 L1758747-03 20240721191331 07/21/24 19:13 1 WG2327092
CCV CVAA70721241916 20240721191603 07/21/24 19:16
CCB CVAA70721241918 20240721191831 07/21/24 19:18
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:7471A
Instrument ID:CVAA10 Calibration Start Date:07/23/24 13:46
Analytical Run:072324CVAA10 SB Calibration End Date:07/23/24 13:59
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK CVAA100723241343 20240723134336 07/23/24 13:43
CAL STD 0.2 20240723134611 07/23/24 13:46
CAL STD 0.4 20240723134848 07/23/24 13:48
CAL STD 1.0 20240723135125 07/23/24 13:51
CAL STD 2.0 20240723135402 07/23/24 13:54
CAL STD 5.0 20240723135639 07/23/24 13:56
CAL STD 10.0 20240723135915 07/23/24 13:59
ICV CVAA100723241401 20240723140156 07/23/24 14:01
ICB CVAA100723241404 20240723140433 07/23/24 14:04
CCV CVAA100723241406 20240723140646 07/23/24 14:06
CCB CVAA100723241409 20240723140923 07/23/24 14:09
ICVLL CVAA100723241411 20240723141137 07/23/24 14:11
L1758898-16 L1758898-16 20240723141413 07/23/24 14:14 1 WG2327969
L1758898-17 L1758898-17 20240723141649 07/23/24 14:16 1 WG2327969
L1758982-02 L1758982-02 20240723141926 07/23/24 14:19 20 WG2327969
L1758982-03 L1758982-03 20240723142204 07/23/24 14:22 100 WG2327969
BLANK R4097489-1 20240723142717 07/23/24 14:27 1 WG2326412
LCS R4097489-2 20240723142953 07/23/24 14:29 1 WG2326412
S-3 (0-6)L1757957-01 20240723143229 07/23/24 14:32 1 WG2326412
SD R4097489-3 20240723143506 07/23/24 14:35 5 WG2326412
MS R4097489-4 20240723143743 07/23/24 14:37 1 WG2326412
CCV CVAA100723241440 20240723144021 07/23/24 14:40
CCB CVAA100723241442 20240723144258 07/23/24 14:42
MSD R4097489-5 20240723144513 07/23/24 14:45 1 WG2326412
S-30 (6-12)L1757957-03 20240723144751 07/23/24 14:47 1 WG2326412
L1758982-04 L1758982-04 20240723145252 07/23/24 14:52 1 WG2327969
S-9 (0-6)L1757957-04 20240723145531 07/23/24 14:55 1 WG2326412
S-8 (0-6)L1757957-05 20240723145808 07/23/24 14:58 1 WG2326412
S-7 (0-6)L1757957-06 20240723150046 07/23/24 15:00 1 WG2326412
S-7 (6-12)L1757957-07 20240723150324 07/23/24 15:03 1 WG2326412
S-6 (0-6)L1757957-08 20240723150601 07/23/24 15:06 1 WG2326412
S-5 (0-6)L1757957-09 20240723150839 07/23/24 15:08 1 WG2326412
CCV CVAA100723241511 20240723151117 07/23/24 15:11
CCB CVAA100723241513 20240723151353 07/23/24 15:13
S-4 (0-6)L1757957-10 20240723151606 07/23/24 15:16 1 WG2326412
S-31 (0-6)L1757957-11 20240723151844 07/23/24 15:18 1 WG2326412
S-2 (0-6)L1757957-12 20240723152121 07/23/24 15:21 1 WG2326412
S-1 (0-6)L1757957-13 20240723152358 07/23/24 15:23 1 WG2326412
S-1 (6-12)L1757957-14 20240723152636 07/23/24 15:26 1 WG2326412
SS-1 (6-12)L1757957-15 20240723152915 07/23/24 15:29 1 WG2326412
L1758046-19 L1758046-19 20240723153153 07/23/24 15:31 1 WG2326412
L1758046-20 L1758046-20 20240723153431 07/23/24 15:34 1 WG2326412
L1758046-21 L1758046-21 20240723153709 07/23/24 15:37 1 WG2326412
L1758046-22 L1758046-22 20240723153947 07/23/24 15:39 1 WG2326412
CCV CVAA100723241542 20240723154225 07/23/24 15:42
CCB CVAA100723241545 20240723154503 07/23/24 15:45
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0002 .0001865398 93.30 0.0004 .0004060432 102
File ID: 20240721151654 20240721151925
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0010 .0009471948 94.70 0.0020 .00203136 102
File ID: 20240721152155 20240721152425
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Analyte Std Conc Result Rec.
mg/kg mg/kg %
MERCURY 0.0050 .005136311 103
File ID: 20240721152657
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0002 .0001812609 90.60 0.0004 .0003788205 94.70
File ID: 20240723134611 20240723134848
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0010 .0009984262 99.80 0.0020 .002062494 103
File ID: 20240723135125 20240723135402
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0050 .005070298 101 0.01 .009953731 99.50
File ID: 20240723135639 20240723135915
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16A-IN INITIAL
CALIBRATION
SDG:L1757957 Calibration (begin) date/time:07/21/24 15:16
Instrument ID:CVAA7 Calibration (end) date/time:07/21/24 15:26
Analytical Method:7471A Analytical Run:072124CVAA7 S
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
MERCURY 253.7 0 5 0.99976 18.60902 0.000713
Calibration Type
0 = Linear Regression
Weightage
5 = None
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16A-IN INITIAL
CALIBRATION
SDG:L1757957 Calibration (begin) date/time:07/23/24 13:46
Instrument ID:CVAA10 Calibration (end) date/time:07/23/24 13:59
Analytical Method:7471A Analytical Run:072324CVAA10 SB
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
MERCURY 253.7 0 5 0.999846 15.43312 0.000695
Calibration Type
0 = Linear Regression
Weightage
5 = None
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8015 Semi-Volatile Organic Compounds (GC)
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2A-OR SURROGATE RECOVERY
Analytical Method:8015 SDG:L1757957
Matrix:Solid
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
S-3 (0-6)L1757957-01 SVGC50 0729_016R 51.4 0
S-3 (6-12)L1757957-02 SVGC50 0729_014R 54.0 0
S-30 (6-12)L1757957-03 SVGC50 0729_012R 50.7 0
S-9 (0-6)L1757957-04 SVGC50 0729_022R 51.2 0
S-8 (0-6)L1757957-05 SVGC50 0729_019R 58.1 0
S-7 (0-6)L1757957-06 SVGC50 0729_029R 93.1D 1
S-7 (6-12)L1757957-07 SVGC50 0729_020R 48.7 0
S-6 (0-6)L1757957-08 SVGC50 0729_023R 65.6D 1
S-5 (0-6)L1757957-09 SVGC50 0729_025R 85.8D 1
S-4 (0-6)L1757957-10 SVGC50 0729_027R 48.1D 1
S-31 (0-6)L1757957-11 SVGC50 0729_028R 54.3D 1
S-2 (0-6)L1757957-12 SVGC50 0729_026R 46.0D 1
S-1 (0-6)L1757957-13 SVGC50 0730_009R 53.1D 1
S-1 (6-12)L1757957-14 SVGC50 0729_021R 47.6 0
SS-1 (6-12)L1757957-15 SVGC50 0729_013R 50.8 0
MS R4100074-3 SVGC50 0729_017R 55.8 0
MSD R4100074-4 SVGC50 0729_018R 52.3 0
BLANK R4100074-1 SVGC50 0729_006R 47.9 0
LCS R4100074-2 SVGC50 0729_007R 56.0 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 o-Terphenyl 18.0 - 148
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4100074-3
L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 R4100074-4
MS Sample / File ID:R4100074-3 / 0729_017R SDG:L1757957
MSD Sample / File ID:R4100074-4 / 0729_018R Analytical Batch:WG2331405
OS Sample / File ID:L1757957-01 / 0729_016R Matrix:Solid
Instrument ID:SVGC50
Analytical Method:8015
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 49.0 52.5 101 89.8 98.8 76.0 10 50.0 - 150 11.7 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4100074-2
RECOVERY _______________
L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
LCS Sample / File ID:R4100074-2 / 0729_007R SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2331405
Instrument ID:SVGC50 Dilution Factor:1
Analytical Method:8015 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 50.0 37.5 75.0 50.0 - 150
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4100074-1
Lab Sample ID:R4100074-1 SDG:L1757957
Lab File ID:0729_006R Preparation Date/Time:07/28/24 08:02
Instrument ID:SVGC50 Analysis Date/Time:07/29/24 09:29
Analytical Batch:WG2331405 Dilution Factor:1
Analytical Method:8015 Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4100074-2 SVGC50 0729_007R 07/29/24 09:42
S-30 (6-12)L1757957-03 SVGC50 0729_012R 07/29/24 10:56
SS-1 (6-12)L1757957-15 SVGC50 0729_013R 07/29/24 11:09
S-3 (6-12)L1757957-02 SVGC50 0729_014R 07/29/24 11:21
S-3 (0-6)L1757957-01 SVGC50 0729_016R 07/29/24 11:46
MS R4100074-3 SVGC50 0729_017R 07/29/24 11:58
MSD R4100074-4 SVGC50 0729_018R 07/29/24 12:11
S-8 (0-6)L1757957-05 SVGC50 0729_019R 07/29/24 12:23
S-7 (6-12)L1757957-07 SVGC50 0729_020R 07/29/24 12:36
S-1 (6-12)L1757957-14 SVGC50 0729_021R 07/29/24 12:48
S-9 (0-6)L1757957-04 SVGC50 0729_022R 07/29/24 13:00
S-6 (0-6)L1757957-08 SVGC50 0729_023R 07/29/24 13:13
S-5 (0-6)L1757957-09 SVGC50 0729_025R 07/29/24 13:38
S-2 (0-6)L1757957-12 SVGC50 0729_026R 07/29/24 13:50
S-4 (0-6)L1757957-10 SVGC50 0729_027R 07/29/24 14:03
S-31 (0-6)L1757957-11 SVGC50 0729_028R 07/29/24 14:15
S-7 (0-6)L1757957-06 SVGC50 0729_029R 07/29/24 14:28
S-1 (0-6)L1757957-13 SVGC50 0730_009R 07/30/24 12:01

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:0729_016R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 11:46
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.63 g
Total Solids (%):98.6 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 52.5 7.80 40.6
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:0729_014R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 11:21
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.26 g
Total Solids (%):92.0 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 39.0 0.836 4.35
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:0729_012R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 10:56
Dilution Factor:2 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.18 g
Total Solids (%):92.7 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 48.5 1.66 8.63
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:0729_022R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 13:00
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.39 g
Total Solids (%):97.8 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 60.0 7.86 40.9
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:0729_019R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 12:23
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.17 g
Total Solids (%):98.2 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 60.4 7.83 40.7
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:0729_029R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 14:28
Dilution Factor:250 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.41 g
Total Solids (%):94.0 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 1180 204 1060
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:0729_020R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 12:36
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.98 g
Total Solids (%):93.8 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 118 8.20 42.6
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:0729_023R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 13:13
Dilution Factor:50 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.09 g
Total Solids (%):98.1 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 98.9 J 39.2 204

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:0729_025R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 13:38
Dilution Factor:50 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.83 g
Total Solids (%):98.7 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 542 39.0 203
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:0729_027R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 14:03
Dilution Factor:250 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.45 g
Total Solids (%):97.3 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 207 J 197 1030

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:0729_028R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 14:15
Dilution Factor:250 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.49 g
Total Solids (%):97.2 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 233 J 197 1030

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:0729_026R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 13:50
Dilution Factor:25 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.80 g
Total Solids (%):95.1 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 123 20.2 105
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:0730_009R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/30/24 12:01
Dilution Factor:20 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.40 g
Total Solids (%):93.1 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 58.3 J 16.5 85.9

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:0729_021R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 12:48
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.42 g
Total Solids (%):91.0 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 62.0 8.45 44.0
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:0729_013R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:04
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 11:09
Dilution Factor:2 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.31 g
Total Solids (%):85.6 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 143 1.80 9.35
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Analytical Method:8015
Analyte CS: 100 CS: 200 CS: 500 CS: 1000 CS: 2000 CS: 3000 CS: 5000 CS: 10000
TPH (GC/FID) HIGH FRACTION 1.78 1.78 1.78 1.78 1.78 1.78 1.78 1.78
O-TERPHENYL 3.38 3.38 3.38 3.39 3.39 3.39 3.40
File ID:0321_010R 0321_011R 0321_012R 0321_013R 0321_014R 0321_015R 0321_016R 0321_017R
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Analytical Method:8015
Analyte CS: 100 CS: 200 CS: 500 CS: 1000 CS: 2000 CS: 3000 CS: 5000 CS: 10000
TPH (GC/FID) HIGH FRACTION 1.78 1.78 1.78 1.78 1.78 1.78 1.78 1.78
O-TERPHENYL 3.38 3.38 3.38 3.39 3.39 3.39 3.40
File ID:0321_010R 0321_011R 0321_012R 0321_013R 0321_014R 0321_015R 0321_016R 0321_017R
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Analytical Method:8015
Analyte RRF: 100 RRF: 200 RRF: 500 RRF: 1000 RRF: 2000 RRF: 3000 RRF: 5000 RRF: 10000
TPH (GC/FID) HIGH FRACTION 2356000 2322000 2267000 2464000 2347000 2376000 2393000 2361000
O-TERPHENYL 2667000 2627000 2575000 2666000 2414000 2319000 2207000
File ID:0321_010R 0321_011R 0321_012R 0321_013R 0321_014R 0321_015R 0321_016R 0321_017R
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Analytical Method:8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 2360778 2.4 1
O-TERPHENYL 2496545 7.37
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Analytical Method:8015
Analyte RRF: 100 RRF: 200 RRF: 500 RRF: 1000 RRF: 2000 RRF: 3000 RRF: 5000 RRF: 10000
TPH (GC/FID) HIGH FRACTION 2356000 2322000 2267000 2464000 2347000 2376000 2393000 2361000
O-TERPHENYL 2667000 2627000 2575000 2666000 2414000 2319000 2207000
File ID:0321_010R 0321_011R 0321_012R 0321_013R 0321_014R 0321_015R 0321_016R 0321_017R
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Analytical Method:8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 2360778 2.4 1
O-TERPHENYL 2496545 7.37
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Lab File ID:0321_027R Analysis date/time:03/21/24 14:43
Analytical Method:8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2360778 2194116 7.06 1500 1389 92.60 80 - 120
TPH (GC/FID) HIGH FRACTION 2360778 2194116 7.06 1500 1389 92.60 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Lab File ID:0729_004R Analysis date/time:07/29/24 08:55
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2360778 2227762 5.63 3000 2818 93.90 85 - 115
O-TERPHENYL 2496545 2182950 12.60 20 17.49 87.40 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Lab File ID:0729_033R Analysis date/time:07/29/24 15:17
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2360778 2276740 3.56 3000 2880 96 85 - 115
O-TERPHENYL 2496545 2159736 13.50 20 17.30 86.50 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Lab File ID:0729_038R Analysis date/time:07/29/24 22:40
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2360778 2444943 3.57 3000 3093 103 85 - 115
O-TERPHENYL 2496545 2257585 9.57 20 18.09 90.40 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Lab File ID:0730_004R Analysis date/time:07/30/24 10:18
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2360778 2230522 5.52 3000 2822 94.10 85 - 115
O-TERPHENYL 2496545 2096119 16 20 16.79 84 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:03/21/24 10:00
Instrument ID:SVGC50 Calibration (end) date/time:06/06/24 10:32
Lab File ID:0730_028R Analysis date/time:07/30/24 16:34
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2360778 2269515 3.87 3000 2871 95.70 85 - 115
O-TERPHENYL 2496545 2086424 16.40 20 16.71 83.50 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8015
Instrument ID:SVGC50 Calibration Start Date:03/21/24 10:00
Calibration End Date:06/06/24 10:32
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 100A 0321_004R 03/21/24 10:00
CAL 400A 0321_005R 03/21/24 10:13
CAL 1KA 0321_006R 03/21/24 10:25
CAL 2500 0321_007R 03/21/24 10:37
CAL 5KA 0321_008R 03/21/24 10:50
CAL 100 0321_010R 03/21/24 11:14
CAL 200 0321_011R 03/21/24 11:26
CAL 500 0321_012R 03/21/24 11:39
CAL 1000 0321_013R 03/21/24 11:51
CAL 2000 0321_014R 03/21/24 12:03
CAL 3000 0321_015R 03/21/24 12:15
CAL 5000 0321_016R 03/21/24 12:28
CAL 10000 0321_017R 03/21/24 12:40
SSCV SVGC50032124R0321_027R742098 0321_027R 03/21/24 14:43
CAL 100M 0606_006R 06/06/24 09:17
CAL 200M 0606_007R 06/06/24 09:30
CAL 500M 0606_008R 06/06/24 09:42
CAL 1KM 0606_009R 06/06/24 09:54
CAL 2KM 0606_010R 06/06/24 10:07
CAL 2.5000 0606_011R 06/06/24 10:19
CAL 5KM 0606_012R 06/06/24 10:32
CCV SVGC50072924R0729_003R742098 0729_003R 07/29/24 08:42
CCV SVGC50072924R0729_004R742098 0729_004R 07/29/24 08:55
BLANK R4100074-1 0729_006R 07/29/24 09:29 1 WG2331405
LCS R4100074-2 0729_007R 07/29/24 09:42 1 WG2331405
S-30 (6-12)L1757957-03 0729_012R 07/29/24 10:56 2 WG2331405
SS-1 (6-12)L1757957-15 0729_013R 07/29/24 11:09 2 WG2331405
S-3 (6-12)L1757957-02 0729_014R 07/29/24 11:21 1 WG2331405
S-3 (0-6)L1757957-01 0729_016R 07/29/24 11:46 10 WG2331405
MS R4100074-3 0729_017R 07/29/24 11:58 10 WG2331405
MSD R4100074-4 0729_018R 07/29/24 12:11 10 WG2331405
S-8 (0-6)L1757957-05 0729_019R 07/29/24 12:23 10 WG2331405
S-7 (6-12)L1757957-07 0729_020R 07/29/24 12:36 10 WG2331405
S-1 (6-12)L1757957-14 0729_021R 07/29/24 12:48 10 WG2331405
S-9 (0-6)L1757957-04 0729_022R 07/29/24 13:00 10 WG2331405
S-6 (0-6)L1757957-08 0729_023R 07/29/24 13:13 50 WG2331405
S-5 (0-6)L1757957-09 0729_025R 07/29/24 13:38 50 WG2331405
S-2 (0-6)L1757957-12 0729_026R 07/29/24 13:50 25 WG2331405
S-4 (0-6)L1757957-10 0729_027R 07/29/24 14:03 250 WG2331405
S-31 (0-6)L1757957-11 0729_028R 07/29/24 14:15 250 WG2331405
S-7 (0-6)L1757957-06 0729_029R 07/29/24 14:28 250 WG2331405
CCV SVGC50072924R0729_033R742098 0729_033R 07/29/24 15:17
CCV SVGC50072924R0729_035R742098 0729_035R 07/29/24 15:42
CCV SVGC50072924R0729_037R742098 0729_037R 07/29/24 22:28
CCV SVGC50072924R0729_038R742098 0729_038R 07/29/24 22:40
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8015
Instrument ID:SVGC50 Calibration Start Date:03/21/24 10:00
Calibration End Date:06/06/24 10:32
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 100A 0321_004R 03/21/24 10:00
CAL 400A 0321_005R 03/21/24 10:13
CAL 1KA 0321_006R 03/21/24 10:25
CAL 2500 0321_007R 03/21/24 10:37
CAL 5KA 0321_008R 03/21/24 10:50
CAL 100 0321_010R 03/21/24 11:14
CAL 200 0321_011R 03/21/24 11:26
CAL 500 0321_012R 03/21/24 11:39
CAL 1000 0321_013R 03/21/24 11:51
CAL 2000 0321_014R 03/21/24 12:03
CAL 3000 0321_015R 03/21/24 12:15
CAL 5000 0321_016R 03/21/24 12:28
CAL 10000 0321_017R 03/21/24 12:40
SSCV SVGC50032124R0321_027R742208 0321_027R 03/21/24 14:43
CAL 100M 0606_006R 06/06/24 09:17
CAL 200M 0606_007R 06/06/24 09:30
CAL 500M 0606_008R 06/06/24 09:42
CAL 1KM 0606_009R 06/06/24 09:54
CAL 2KM 0606_010R 06/06/24 10:07
CAL 2.5000 0606_011R 06/06/24 10:19
CAL 5KM 0606_012R 06/06/24 10:32
CCV SVGC50073024R0730_003R742208 0730_003R 07/30/24 10:05
CCV SVGC50073024R0730_004R742208 0730_004R 07/30/24 10:18
S-1 (0-6)L1757957-13 0730_009R 07/30/24 12:01 20 WG2331405
L1757621-01 L1757621-01 0730_025R 07/30/24 15:34 20 WG2331404
CCV SVGC50073024R0730_027R742208 0730_027R 07/30/24 16:21
CCV SVGC50073024R0730_028R742208 0730_028R 07/30/24 16:34
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:8015
Matrix:Solid Prep Method:3546
Analyte CAS MDL RDL
mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 0.7690 4
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100074-1
Lab Sample ID:R4100074-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0729_006R Received Date/Time:_______________
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:02
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 09:29
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 U 0.769 4.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100074-2
Lab Sample ID:R4100074-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0729_007R Received Date/Time:_______________
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:02
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 09:42
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 37.5 1.33 4.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100074-3
Lab Sample ID:R4100074-3 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:0729_017R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:02
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 11:58
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.55 g
Total Solids (%):98.6 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 101 7.80 40.6
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100074-4
Lab Sample ID:R4100074-4 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:0729_018R Received Date/Time:07/18/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:07/28/24 08:02
Analytical Batch:WG2331405 Analysis Date/Time:07/29/24 12:11
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.56 g
Total Solids (%):98.6 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.69 89.8 7.80 40.6
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8015D/GRO Volatile Organic Compounds (GC)
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2A-OR SURROGATE RECOVERY
Analytical Method:8015D/GRO SDG:L1757957
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
EB-1-071624 L1757957-16 VOCGC10 0723_14 104 0
MS R4098551-3 VOCGC10 0723_32 105 0
MSD R4098551-4 VOCGC10 0723_33 109 0
BLANK R4098551-2 VOCGC10 0723_05 102 0
LCS R4098551-1 VOCGC10 0723_03U 106 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 a,a,a-Trifluorotoluene(FID)78.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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2A-OR SURROGATE RECOVERY
Analytical Method:8015D/GRO SDG:L1757957
Matrix:Solid
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
S-3 (0-6)L1757957-01 VOCGC15 0728_20 100 0
S-3 (6-12)L1757957-02 VOCGC15 0728_14 99.8 0
S-30 (6-12)L1757957-03 VOCGC10 0724_11 102 0
S-9 (0-6)L1757957-04 VOCGC17 0725_11 97.0 0
S-8 (0-6)L1757957-05 VOCGC15 0724_20 98.4 0
S-7 (0-6)L1757957-06 VOCGC17 0725_12 97.8 0
S-7 (6-12)L1757957-07 VOCGC15 0724_21 100 0
S-6 (0-6)L1757957-08 VOCGC17 0725_13 96.6 0
S-5 (0-6)L1757957-09 VOCGC17 0725_14 97.1 0
S-4 (0-6)L1757957-10 VOCGC17 0725_15 97.7 0
S-31 (0-6)L1757957-11 VOCGC17 0725_16 97.9 0
S-2 (0-6)L1757957-12 VOCGC10 0725_15 102 0
S-1 (0-6)L1757957-13 VOCGC10 0725_16 103 0
S-1 (6-12)L1757957-14 VOCGC10 0725_17 103 0
SS-1 (6-12)L1757957-15 VOCGC10 0725_18 103 0
MS R4100115-3 VOCGC15 0728_21 103 0
MSD R4100115-4 VOCGC15 0728_22 101 0
BLANK R4098862-2 VOCGC10 0724_05 105 0
BLANK R4098479-3 VOCGC10 0725_10 106 0
BLANK R4098253-2 VOCGC15 0724_07 97.9 0
BLANK R4100114-2 VOCGC15 0728_06 99.6 0
BLANK R4100115-2 VOCGC15 0728_06C 99.6 0
BLANK R4098321-3 VOCGC17 0725_08 96.3 0
LCS R4098862-1 VOCGC10 0724_03U 107 0
LCS R4098479-1 VOCGC10 0725_07u 105 0
LCS R4098253-1 VOCGC15 0724_04 106 0
LCS R4100114-1 VOCGC15 0728_03 101 0
LCS R4100115-1 VOCGC15 0728_03C 101 0
LCS R4098321-1 VOCGC17 0725_04 105 0
LCSD R4098479-2 VOCGC10 0725_08 111 0
LCSD R4098321-2 VOCGC17 0725_05 105 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 a,a,a-Trifluorotoluene(FID)77.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4098551-3
L1757957-16 R4098551-4
MS Sample / File ID:R4098551-3 / 0723_32 SDG:L1757957
MSD Sample / File ID:R4098551-4 / 0723_33 Analytical Batch:WG2327971
OS Sample / File ID:L1757954-05 / 0723_18 Matrix:GW
Instrument ID:VOCGC10
Analytical Method:8015D/GRO
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.00 U 4.47 5.92 89.4 118 1 10.0 - 160 27.9*22
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4100115-3
L1757957-01 R4100115-4
MS Sample / File ID:R4100115-3 / 0728_21 SDG:L1757957
MSD Sample / File ID:R4100115-4 / 0728_22 Analytical Batch:WG2330774
OS Sample / File ID:L1757957-01 / 0728_20 Matrix:Solid
Instrument ID:VOCGC15
Analytical Method:8015D/GRO
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 142 2.32 112 128 77.3 88.9 27.5 10.0 - 151 13.7 28
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098253-1
RECOVERY _______________
L1757957-05,07
LCS Sample / File ID:R4098253-1 / 0724_04 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2329459
Instrument ID:VOCGC15 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 5.16 103 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098321-1
RECOVERY R4098321-2
L1757957-04,06,08,09,10,11
LCS Sample / File ID:R4098321-1 / 0725_04 SDG:L1757957
LCSD Sample / File ID:R4098321-2 / 0725_05 Analytical Batch:WG2329941
Instrument ID:VOCGC17 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 4.94 4.99 98.8 99.8 72.0 - 127 1.01 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098479-1
RECOVERY R4098479-2
L1757957-12,13,14,15
LCS Sample / File ID:R4098479-1 / 0725_07u SDG:L1757957
LCSD Sample / File ID:R4098479-2 / 0725_08 Analytical Batch:WG2329829
Instrument ID:VOCGC10 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 4.65 5.66 93.0 113 72.0 - 127 19.6 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098551-1
RECOVERY _______________
L1757957-16
LCS Sample / File ID:R4098551-1 / 0723_03U SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2327971
Instrument ID:VOCGC10 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.00 4.52 90.4 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098862-1
RECOVERY _______________
L1757957-03
LCS Sample / File ID:R4098862-1 / 0724_03U SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2328825
Instrument ID:VOCGC10 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 4.72 94.4 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4100114-1
RECOVERY _______________
L1757957-02
LCS Sample / File ID:R4100114-1 / 0728_03 SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2330767
Instrument ID:VOCGC15 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 5.54 111 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4100115-1
RECOVERY _______________
L1757957-01
LCS Sample / File ID:R4100115-1 / 0728_03C SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2330774
Instrument ID:VOCGC15 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 5.54 111 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4098551-2
Lab Sample ID:R4098551-2 SDG:L1757957
Lab File ID:0723_05 Preparation Date/Time:07/23/24 12:49
Instrument ID:VOCGC10 Analysis Date/Time:07/23/24 12:49
Analytical Batch:WG2327971 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098551-1 VOCGC10 0723_03U 07/23/24 12:03
EB-1-071624 L1757957-16 VOCGC10 0723_14 07/23/24 17:16
OS L1757954-05 VOCGC10 0723_18 07/23/24 18:47
MS R4098551-3 VOCGC10 0723_32 07/24/24 00:06
MSD R4098551-4 VOCGC10 0723_33 07/24/24 00:28
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4A-OR METHOD BLANK SAMPLE NO.:
R4098862-2
Lab Sample ID:R4098862-2 SDG:L1757957
Lab File ID:0724_05 Preparation Date/Time:07/24/24 10:54
Instrument ID:VOCGC10 Analysis Date/Time:07/24/24 10:54
Analytical Batch:WG2328825 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098862-1 VOCGC10 0724_03U 07/24/24 10:08
S-30 (6-12)L1757957-03 VOCGC10 0724_11 07/24/24 13:40
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4A-OR METHOD BLANK SAMPLE NO.:
R4098479-3
Lab Sample ID:R4098479-3 SDG:L1757957
Lab File ID:0725_10 Preparation Date/Time:07/25/24 12:59
Instrument ID:VOCGC10 Analysis Date/Time:07/25/24 12:59
Analytical Batch:WG2329829 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098479-1 VOCGC10 0725_07u 07/25/24 11:50
LCSD R4098479-2 VOCGC10 0725_08 07/25/24 12:13
S-2 (0-6)L1757957-12 VOCGC10 0725_15 07/25/24 14:52
S-1 (0-6)L1757957-13 VOCGC10 0725_16 07/25/24 15:15
S-1 (6-12)L1757957-14 VOCGC10 0725_17 07/25/24 15:38
SS-1 (6-12)L1757957-15 VOCGC10 0725_18 07/25/24 16:01
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4A-OR METHOD BLANK SAMPLE NO.:
R4098253-2
Lab Sample ID:R4098253-2 SDG:L1757957
Lab File ID:0724_07 Preparation Date/Time:07/24/24 18:25
Instrument ID:VOCGC15 Analysis Date/Time:07/24/24 18:25
Analytical Batch:WG2329459 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098253-1 VOCGC15 0724_04 07/24/24 17:08
S-8 (0-6)L1757957-05 VOCGC15 0724_20 07/24/24 23:45
S-7 (6-12)L1757957-07 VOCGC15 0724_21 07/25/24 00:08
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4A-OR METHOD BLANK SAMPLE NO.:
R4100114-2
Lab Sample ID:R4100114-2 SDG:L1757957
Lab File ID:0728_06 Preparation Date/Time:07/28/24 11:14
Instrument ID:VOCGC15 Analysis Date/Time:07/28/24 11:14
Analytical Batch:WG2330767 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4100114-1 VOCGC15 0728_03 07/28/24 10:03
S-3 (6-12)L1757957-02 VOCGC15 0728_14 07/28/24 14:51
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4A-OR METHOD BLANK SAMPLE NO.:
R4100115-2
Lab Sample ID:R4100115-2 SDG:L1757957
Lab File ID:0728_06C Preparation Date/Time:07/28/24 11:14
Instrument ID:VOCGC15 Analysis Date/Time:07/28/24 11:14
Analytical Batch:WG2330774 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4100115-1 VOCGC15 0728_03C 07/28/24 10:03
S-3 (0-6)L1757957-01 VOCGC15 0728_20 07/28/24 17:12
MS R4100115-3 VOCGC15 0728_21 07/28/24 17:35
MSD R4100115-4 VOCGC15 0728_22 07/28/24 17:59
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4A-OR METHOD BLANK SAMPLE NO.:
R4098321-3
Lab Sample ID:R4098321-3 SDG:L1757957
Lab File ID:0725_08 Preparation Date/Time:07/25/24 11:56
Instrument ID:VOCGC17 Analysis Date/Time:07/25/24 11:56
Analytical Batch:WG2329941 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098321-1 VOCGC17 0725_04 07/25/24 10:23
LCSD R4098321-2 VOCGC17 0725_05 07/25/24 10:43
S-9 (0-6)L1757957-04 VOCGC17 0725_11 07/25/24 13:02
S-7 (0-6)L1757957-06 VOCGC17 0725_12 07/25/24 13:21
S-6 (0-6)L1757957-08 VOCGC17 0725_13 07/25/24 13:40
S-5 (0-6)L1757957-09 VOCGC17 0725_14 07/25/24 14:00
S-4 (0-6)L1757957-10 VOCGC17 0725_15 07/25/24 14:19
S-31 (0-6)L1757957-11 VOCGC17 0725_16 07/25/24 14:39
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC10 Calibration Start Date:06/04/24 17:40
Std File: 0723_03 Calibration End Date:06/05/24 00:52
Std Analysis Date:07/23/24 12:03
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 308394700 7.82 4485202000 7.81
UPPER LIMIT 616789400 8970404000
LOWER LIMIT 154197300 2242601000
LCS R4098551-1
WG2327971 1x 0723_03U 308394700 7.82 4485202000 7.81
BLANK R4098551-2
WG2327971 1x 0723_05 345473800 7.82 5098882000 7.81
L1757957-16 WG2327971
1x 0723_14 271897400 7.82 4183700000 7.81
OS L1757954-05
WG2327971 1x 0723_18 322737700 7.82 4876488000 7.81
MS R4098551-3
WG2327971 1x 0723_32 363255900 7.82 5204767000 7.82
MSD R4098551-4
WG2327971 1x 0723_33 287146600 7.82 4137160000 7.82
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC10 Calibration Start Date:06/04/24 17:40
Std File: 0724_03 Calibration End Date:06/05/24 00:52
Std Analysis Date:07/24/24 10:08
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 336128100 7.82 4897133000 7.82
UPPER LIMIT 672256200 9794266000
LOWER LIMIT 168064000 2448567000
LCS R4098862-1
WG2328825 1x 0724_03U 336128100 7.82 4897133000 7.82
BLANK R4098862-2
WG2328825 25x 0724_05 299273600 7.82 4577920000 7.81
L1757957-03 WG2328825
27.5x 0724_11 251354700 7.81 3917292000 7.81
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC10 Calibration Start Date:06/04/24 17:40
Std File: 0725_07 Calibration End Date:06/05/24 00:52
Std Analysis Date:07/25/24 11:50
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 312116300 7.81 4707109000 7.81
UPPER LIMIT 624232600 9414218000
LOWER LIMIT 156058100 2353554000
LCS R4098479-1
WG2329829 1x 0725_07u 312116300 7.81 4707109000 7.81
LCSD R4098479-2
WG2329829 1x 0725_08 260453600 7.81 3777693000 7.81
BLANK R4098479-3
WG2329829 25x 0725_10 261378700 7.81 4079024000 7.81
L1757957-12 WG2329829
26.8x 0725_15 256329000 7.81 3976424000 7.81
L1757957-13 WG2329829
28.5x 0725_16 251374100 7.81 3949206000 7.81
L1757957-14 WG2329829
28.5x 0725_17 244858000 7.81 3872152000 7.81
L1757957-15 WG2329829
25x 0725_18 226612700 7.81 3624739000 7.81
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC15 Calibration Start Date:06/26/24 14:42
Std File: 0724_03 Calibration End Date:06/26/24 19:34
Std Analysis Date:07/24/24 16:45
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 381796000 7.40 0 0
UPPER LIMIT 763592000 0
LOWER LIMIT 190898000 0
LCS R4098253-1
WG2329459 1x 0724_04 387377800 7.40 0 0
BLANK R4098253-2
WG2329459 25x 0724_07 389499100 7.40 0 0
L1757957-05 WG2329459
25x 0724_20 372285900 7.40 0 0
L1757957-07 WG2329459
30.3x 0724_21 359208700 7.40 0 0
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC15 Calibration Start Date:06/26/24 14:42
Std File: 0728_02 Calibration End Date:06/26/24 19:34
Std Analysis Date:07/28/24 09:39
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 370540300 7.40 0 0
UPPER LIMIT 741080600 0
LOWER LIMIT 185270100 0
LCS R4100115-1
WG2330774 1x 0728_03C 377512100 7.40 0 0
LCS R4100114-1
WG2330767 1x 0728_03 377512100 7.40 0 0
BLANK R4100115-2
WG2330774 25x 0728_06C 341527700 7.40 0 0
BLANK R4100114-2
WG2330767 25x 0728_06 341527700 7.40 0 0
L1757957-02 WG2330767
26.3x 0728_14 372737700 7.40 0 0
OS L1757957-01
WG2330774 27.5x 0728_20 370635900 7.40 0 0
L1757957-01 WG2330774
27.5x 0728_20 370635900 7.40 0 0
MS R4100115-3
WG2330774 27.5x 0728_21 416426600 7.40 0 0
MSD R4100115-4
WG2330774 27.5x 0728_22 369882800 7.40 0 0
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC17 Calibration Start Date:01/30/24 00:30
Std File: 0725_03 Calibration End Date:01/30/24 02:26
Std Analysis Date:07/25/24 10:04
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 180261600 5.06 180261600 5.06
UPPER LIMIT 360523200 360523200
LOWER LIMIT 90130800 90130800
LCS R4098321-1
WG2329941 1x 0725_04 186827100 5.06 186827100 5.06
LCSD R4098321-2
WG2329941 1x 0725_05 184175700 5.06 184175700 5.06
BLANK R4098321-3
WG2329941 25x 0725_08 171909200 5.06 171909200 5.06
L1757957-04 WG2329941
25.8x 0725_11 176465300 5.06 176465300 5.06
L1757957-06 WG2329941
34.3x 0725_12 149559800 5.05 149559800 5.05
L1757957-08 WG2329941
25x 0725_13 168254500 5.05 168254500 5.05
L1757957-09 WG2329941
25x 0725_14 176168900 5.06 176168900 5.06
L1757957-10 WG2329941
28.5x 0725_15 159941800 5.05 159941800 5.05
L1757957-11 WG2329941
30.3x 0725_16 159497000 5.06 159497000 5.06
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:0728_20 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2330774 Analysis Date/Time:07/28/24 17:12
Dilution Factor:27.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 2.32 B J 0.613 2.82
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:0728_14 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:07/16/24 10:00
Analytical Batch:WG2330767 Analysis Date/Time:07/28/24 14:51
Dilution Factor:26.3 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.52 g
Total Solids (%):92.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 2.91 B J 0.668 3.08
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:0724_11 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/16/24 13:30
Analytical Batch:WG2328825 Analysis Date/Time:07/24/24 13:40
Dilution Factor:27.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.08 g
Total Solids (%):92.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 3.36 B 0.687 3.16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:0725_11 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:07/16/24 10:34
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 13:02
Dilution Factor:25.8 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.71 g
Total Solids (%):97.8 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 1.51 J 0.585 2.69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:0724_20 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:07/16/24 10:58
Analytical Batch:WG2329459 Analysis Date/Time:07/24/24 23:45
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.02 g
Total Solids (%):98.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 1.40 B J 0.563 2.59
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:0725_12 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:07/16/24 11:20
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 13:21
Dilution Factor:34.3 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.32 g
Total Solids (%):94.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 7.03 0.826 3.81
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:0724_21 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:07/16/24 11:35
Analytical Batch:WG2329459 Analysis Date/Time:07/25/24 00:08
Dilution Factor:30.3 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.26 g
Total Solids (%):93.8 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 3.67 B 0.737 3.39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:0725_13 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:07/16/24 11:55
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 13:40
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.06 g
Total Solids (%):98.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 1.10 J 0.564 2.59
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:0725_14 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:07/16/24 13:15
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 14:00
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.23 g
Total Solids (%):98.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 0.629 J 0.558 2.57
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:0725_15 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:07/16/24 13:30
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 14:19
Dilution Factor:28.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.81 g
Total Solids (%):97.3 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 2.37 J 0.651 3.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:0725_16 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:07/16/24 14:40
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 14:39
Dilution Factor:30.3 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.28 g
Total Solids (%):97.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 1.81 J 0.692 3.19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:0725_15 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/16/24 13:55
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 14:52
Dilution Factor:26.8 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.34 g
Total Solids (%):95.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 9.85 0.640 2.95
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:0725_16 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/16/24 14:10
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 15:15
Dilution Factor:28.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.81 g
Total Solids (%):93.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 6.95 B 0.704 3.25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:0725_17 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/16/24 14:25
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 15:38
Dilution Factor:28.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.78 g
Total Solids (%):91.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 2.93 B J 0.733 3.38
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:0725_18 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/16/24 14:41
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 16:01
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.3 g
Total Solids (%):85.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 3.14 B J 0.729 3.36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:0723_14 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/23/24 17:16
Analytical Batch:WG2327971 Analysis Date/Time:07/23/24 17:16
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 U 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Analytical Method:8015D/GRO
Analyte CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G
TPH (GC/FID) LOW FRACTION 8 8 8 8 8 8
A,A,A-TRIFLUOROTOLUENE(FID)8.26 8.26 8.26 8.26 8.26 8.26
File ID:0604_19 0604_20 0604_21 0604_22 0604_23 0604_24
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Analytical Method:8015D/GRO
Analyte CS: .05G CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G
TPH (GC/FID) LOW FRACTION 8 8 8 8 8 8 8
A,A,A-TRIFLUOROTOLUENE(FID)7.85 7.85 7.85 7.85 7.85 7.85 7.85
File ID:0626_05 0626_06 0626_07 0626_08 0626_09 0626_10 0626_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:01/30/24 00:30
Instrument ID:VOCGC17 Calibration (end) date/time:01/30/24 02:26
Analytical Method:8015D/GRO
Analyte CS: .05G CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G
TPH (GC/FID) LOW FRACTION 6 6 6 6 6 6 6
A,A,A-TRIFLUOROTOLUENE(FID)5.33 5.33 5.33 5.33 5.33 5.36 5.33
File ID:0129_36 0129_37 0129_38 0129_39 0129_40 0129_41 0129_42
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Analytical Method:8015D/GRO
Analyte RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G
TPH (GC/FID) LOW FRACTION 299.20 187.30 253.10 313.30 320.90 294.70
A,A,A-TRIFLUOROTOLUENE(FID)0.6740 0.6610 0.6670 0.68 0.6980 0.7290
File ID:0604_19 0604_20 0604_21 0604_22 0604_23 0604_24
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 278.1044 18.1
A,A,A-TRIFLUOROTOLUENE(FID)0.684749 3.66
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Analytical Method:8015D/GRO
Analyte RRF: .05G RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G
TPH (GC/FID) LOW FRACTION 896.70 868.5001 829.90 748.60 774.80 699.10 709.80
A,A,A-TRIFLUOROTOLUENE(FID)0.7190 0.7140 0.7140 0.70 0.7470 0.7620 0.8380
File ID:0626_05 0626_06 0626_07 0626_08 0626_09 0626_10 0626_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 789.6191 9.78
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 6.39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 335 of 530
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:01/30/24 00:30
Instrument ID:VOCGC17 Calibration (end) date/time:01/30/24 02:26
Analytical Method:8015D/GRO
Analyte RRF: .05G RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G
TPH (GC/FID) LOW FRACTION 709.50 787.20 808.60 862.60 859.90 818.40 741
A,A,A-TRIFLUOROTOLUENE(FID)0.7470 0.7330 0.7550 0.7710 0.7740 0.8190 0.8920
File ID:0129_36 0129_37 0129_38 0129_39 0129_40 0129_41 0129_42
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 336 of 530
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:01/30/24 00:30
Instrument ID:VOCGC17 Calibration (end) date/time:01/30/24 02:26
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 798.17 7.18
A,A,A-TRIFLUOROTOLUENE(FID)0.784443 6.98
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 337 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Lab File ID:0604_27 Analysis date/time:06/05/24 02:00
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 278.1044 0.31927570 99.90 5 5.740 115 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.684749 0.69868240 2.03 0.20 0.2041 102 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 338 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Lab File ID:0723_03 Analysis date/time:07/23/24 12:03
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 278.1044 0.25118840 99.90 5 4.516 90.30 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.684749 0.72844180 6.38 0.20 0.2128 106 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 339 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Lab File ID:0724_03 Analysis date/time:07/24/24 10:08
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 278.1044 0.26277830 99.90 5 4.724 94.50 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.684749 0.73145060 6.82 0.20 0.2136 107 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 340 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/04/24 17:40
Instrument ID:VOCGC10 Calibration (end) date/time:06/05/24 00:52
Lab File ID:0725_07 Analysis date/time:07/25/24 11:50
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 278.1044 0.25850160 99.90 5 4.648 93 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.684749 0.71759150 4.80 0.20 0.2096 105 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 341 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Lab File ID:0626_14 Analysis date/time:06/26/24 22:05
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 789.6191 0.63304530 99.90 5 4.009 80.20 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 0.73361710 1.14 0.20 0.1977 98.80 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 342 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Lab File ID:0724_03 Analysis date/time:07/24/24 16:45
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 789.6191 0.75129020 99.90 5 4.757 95.10 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 0.78900830 6.33 0.20 0.2127 106 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 343 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Lab File ID:0728_02 Analysis date/time:07/28/24 09:39
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 789.6191 0.79563150 99.90 5 5.038 101 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 0.75786440 2.13 0.20 0.2043 102 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 344 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:01/30/24 00:30
Instrument ID:VOCGC17 Calibration (end) date/time:01/30/24 02:26
Lab File ID:0129_45 Analysis date/time:01/30/24 03:23
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 798.17 0.64011140 99.90 5 4.010 80.20 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.784443 0.77147590 1.65 0.20 0.1967 98.30 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 345 of 530
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1757957 Calibration (begin) date/time:01/30/24 00:30
Instrument ID:VOCGC17 Calibration (end) date/time:01/30/24 02:26
Lab File ID:0725_03 Analysis date/time:07/25/24 10:04
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 798.17 0.80918840 99.90 5 5.069 101 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.784443 0.82107340 4.67 0.20 0.2093 105 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 346 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC10 Calibration Start Date:06/04/24 17:40
Calibration End Date:06/05/24 00:52
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 0.5 0604_05 06/04/24 17:40
CAL 1 0604_06 06/04/24 18:03
CAL 5 0604_07 06/04/24 18:25
CAL 25 0604_08 06/04/24 18:48
CAL 50 0604_09 06/04/24 19:11
CAL 150 0604_10 06/04/24 19:34
CAL 250 0604_11 06/04/24 19:57
SSCV VOCGC100604240604_14729187 0604_14 06/04/24 21:05
CAL .1G 0604_19 06/04/24 22:59
CAL .5G 0604_20 06/04/24 23:21
CAL 1G 0604_21 06/04/24 23:44
CAL 2.5G 0604_22 06/05/24 00:07
CAL 5G 0604_23 06/05/24 00:29
CAL 10G 0604_24 06/05/24 00:52
SSCV VOCGC100604240604_27729187 0604_27 06/05/24 02:00
ICV VOCGC100723240723_03729187 0723_03 07/23/24 12:03
LCS R4098551-1 0723_03U 07/23/24 12:03 1 WG2327971
LCS R4098552-1 0723_03UA 07/23/24 12:03 1 WG2328320
BLANK R4098551-2 0723_05 07/23/24 12:49 1 WG2327971
BLANK R4098552-2 0723_05A 07/23/24 12:49 1 WG2328320
L1757076-01 L1757076-01 0723_06 07/23/24 14:14 1 WG2328320
L1757076-03 L1757076-03 0723_07 07/23/24 14:37 1 WG2328320
OS L1757076-12 0723_08 07/23/24 15:00
L1757076-12 L1757076-12 0723_08 07/23/24 15:00 1 WG2328320
MS R4098552-3 0723_09 07/23/24 15:23 1 WG2328320
MSD R4098552-4 0723_10 07/23/24 15:46 1 WG2328320
L1757954-09 L1757954-09 0723_12 07/23/24 16:31 1 WG2327971
L1757954-08 L1757954-08 0723_13 07/23/24 16:54 1 WG2327971
EB-1-071624 L1757957-16 0723_14 07/23/24 17:16 1 WG2327971
L1757954-02 L1757954-02 0723_15 07/23/24 17:39 1 WG2327971
L1757954-03 L1757954-03 0723_16 07/23/24 18:01 1 WG2327971
L1757954-04 L1757954-04 0723_17 07/23/24 18:24 1 WG2327971
OS L1757954-05 0723_18 07/23/24 18:47
L1757954-05 L1757954-05 0723_18 07/23/24 18:47 1 WG2327971
L1757954-06 L1757954-06 0723_19 07/23/24 19:10 1 WG2327971
L1757974-01 L1757974-01 0723_20 07/23/24 19:32 1 WG2327971
L1757974-02 L1757974-02 0723_21 07/23/24 19:55 1 WG2327971
L1757974-03 L1757974-03 0723_22 07/23/24 20:18 1 WG2327971
L1757974-04 L1757974-04 0723_23 07/23/24 20:41 1 WG2327971
L1757974-05 L1757974-05 0723_24 07/23/24 21:03 1 WG2327971
L1757974-06 L1757974-06 0723_25 07/23/24 21:26 1 WG2327971
L1757974-07 L1757974-07 0723_26 07/23/24 21:50 1 WG2327971
L1757974-08 L1757974-08 0723_27 07/23/24 22:12 1 WG2327971
L1757926-12 L1757926-12 0723_28 07/23/24 22:35 5 WG2327971
L1757954-01 L1757954-01 0723_29 07/23/24 22:58 10 WG2327971
L1757954-07 L1757954-07 0723_30 07/23/24 23:20 10 WG2327971
L1757972-01 L1757972-01 0723_31 07/23/24 23:43 50 WG2327971
MS R4098551-3 0723_32 07/24/24 00:06 1 WG2327971
MSD R4098551-4 0723_33 07/24/24 00:28 1 WG2327971
ICV VOCGC100724240724_03729187 0724_03 07/24/24 10:08
LCS R4098862-1 0724_03U 07/24/24 10:08 1 WG2328825
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 347 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC10 Calibration Start Date:06/04/24 17:40
Calibration End Date:06/05/24 00:52
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4098862-2 0724_05 07/24/24 10:54 25 WG2328825
S-30 (6-12)L1757957-03 0724_11 07/24/24 13:40 27.5 WG2328825
L1757232-01 L1757232-01 0724_12 07/24/24 14:03 2000 WG2328825
L1757232-02 L1757232-02 0724_13 07/24/24 14:26 1000 WG2328825
L1757555-13 L1757555-13 0724_15 07/24/24 15:12 100 WG2328825
L1757555-14 L1757555-14 0724_16 07/24/24 15:35 100 WG2328825
L1757588-12 L1757588-12 0724_17 07/24/24 15:57 1000 WG2328825
L1757588-13 L1757588-13 0724_18 07/24/24 16:20 1000 WG2328825
L1757588-14 L1757588-14 0724_19 07/24/24 16:43 1000 WG2328825
L1757588-15 L1757588-15 0724_20 07/24/24 17:06 1000 WG2328825
L1757588-16 L1757588-16 0724_21 07/24/24 17:29 1000 WG2328825
ICV VOCGC100725240725_07729187 0725_07 07/25/24 11:50
LCS R4098479-1 0725_07u 07/25/24 11:50 1 WG2329829
LCSD R4098479-2 0725_08 07/25/24 12:13 1 WG2329829
BLANK R4098479-3 0725_10 07/25/24 12:59 25 WG2329829
L1758052-11 L1758052-11 0725_11 07/25/24 13:21 25 WG2329829
L1758052-12 L1758052-12 0725_12 07/25/24 13:44 25 WG2329829
L1758093-01 L1758093-01 0725_13 07/25/24 14:07 27.3 WG2329829
L1758093-02 L1758093-02 0725_14 07/25/24 14:30 25 WG2329829
S-2 (0-6)L1757957-12 0725_15 07/25/24 14:52 26.8 WG2329829
S-1 (0-6)L1757957-13 0725_16 07/25/24 15:15 28.5 WG2329829
S-1 (6-12)L1757957-14 0725_17 07/25/24 15:38 28.5 WG2329829
SS-1 (6-12)L1757957-15 0725_18 07/25/24 16:01 25 WG2329829
L1757963-01 L1757963-01 0725_19 07/25/24 16:23 25 WG2329829
L1757963-02 L1757963-02 0725_20 07/25/24 16:46 25 WG2329829
L1758007-15 L1758007-15 0725_21 07/25/24 17:09 25 WG2329829
L1758007-17 L1758007-17 0725_22 07/25/24 17:32 34.8 WG2329829
L1758094-01 L1758094-01 0725_23 07/25/24 17:54 25 WG2329829
L1758094-02 L1758094-02 0725_24 07/25/24 18:17 25 WG2329829
L1758094-03 L1758094-03 0725_25 07/25/24 18:40 25 WG2329829
L1758101-01 L1758101-01 0725_26 07/25/24 19:02 25 WG2329829
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 348 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC15 Calibration Start Date:06/26/24 14:42
Calibration End Date:06/26/24 19:34
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL .05G 0626_05 06/26/24 14:42
CAL .1G 0626_06 06/26/24 15:29
CAL .5G 0626_07 06/26/24 15:57
CAL 1G 0626_08 06/26/24 17:00
CAL 2.5G 0626_09 06/26/24 18:19
CAL 5G 0626_10 06/26/24 19:11
CAL 10G 0626_11 06/26/24 19:34
SSCV VOCGC150626240626_14734485 0626_14 06/26/24 22:05
ICV VOCGC150724240724_03734485 0724_03 07/24/24 16:45
LCS R4098253-1 0724_04 07/24/24 17:08 1 WG2329459
BLANK R4098253-2 0724_07 07/24/24 18:25 25 WG2329459
L1759553-01 L1759553-01 0724_08 07/24/24 19:05 25 WG2329459
L1758945-07 L1758945-07 0724_09 07/24/24 19:28 25 WG2329459
L1758945-05 L1758945-05 0724_10 07/24/24 19:52 149 WG2329459
L1758945-06 L1758945-06 0724_11 07/24/24 20:15 100 WG2329459
L1758945-08 L1758945-08 0724_12 07/24/24 20:39 100 WG2329459
L1758945-09 L1758945-09 0724_13 07/24/24 21:02 147 WG2329459
L1758945-10 L1758945-10 0724_14 07/24/24 21:25 100 WG2329459
L1758945-11 L1758945-11 0724_15 07/24/24 21:49 100 WG2329459
L1758945-12 L1758945-12 0724_16 07/24/24 22:12 100 WG2329459
L1758945-13 L1758945-13 0724_17 07/24/24 22:35 100 WG2329459
S-8 (0-6)L1757957-05 0724_20 07/24/24 23:45 25 WG2329459
S-7 (6-12)L1757957-07 0724_21 07/25/24 00:08 30.3 WG2329459
ICV VOCGC150728240728_02734485 0728_02 07/28/24 09:39
LCS R4100113-1 0728_03B 07/28/24 10:03 1 WG2329999
LCS R4100114-1 0728_03 07/28/24 10:03 1 WG2330767
LCS R4100115-1 0728_03C 07/28/24 10:03 1 WG2330774
LCS R4100116-1 0728_03A 07/28/24 10:03 1 WG2330897
BLANK R4100113-2 0728_06B 07/28/24 11:14 25 WG2329999
BLANK R4100114-2 0728_06 07/28/24 11:14 25 WG2330767
BLANK R4100115-2 0728_06C 07/28/24 11:14 25 WG2330774
BLANK R4100116-2 0728_06A 07/28/24 11:14 25 WG2330897
L1757555-11 L1757555-11 0728_07 07/28/24 12:05 25 WG2330767
L1757588-18 L1757588-18 0728_08 07/28/24 12:28 25 WG2330767
L1757588-19 L1757588-19 0728_09 07/28/24 12:51 25 WG2330767
L1757588-20 L1757588-20 0728_10 07/28/24 13:15 25 WG2330767
L1757621-03 L1757621-03 0728_11 07/28/24 13:39 25 WG2330767
L1757626-01 L1757626-01 0728_12 07/28/24 14:04 25 WG2330767
L1757626-02 L1757626-02 0728_13 07/28/24 14:28 25 WG2330767
S-3 (6-12)L1757957-02 0728_14 07/28/24 14:51 26.3 WG2330767
L1757588-17 L1757588-17 0728_15 07/28/24 15:15 50 WG2330767
L1757594-13 L1757594-13 0728_16 07/28/24 15:39 250 WG2330767
L1758648-04 L1758648-04 0728_17 07/28/24 16:02 202 WG2330897
L1758648-05 L1758648-05 0728_18 07/28/24 16:25 100 WG2330897
L1757555-12 L1757555-12 0728_19 07/28/24 16:49 50 WG2329999
S-3 (0-6)L1757957-01 0728_20 07/28/24 17:12 27.5 WG2330774
MS R4100115-3 0728_21 07/28/24 17:35 27.5 WG2330774
MSD R4100115-4 0728_22 07/28/24 17:59 27.5 WG2330774
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 349 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8015D/GRO
Instrument ID:VOCGC17 Calibration Start Date:01/30/24 00:30
Calibration End Date:01/30/24 02:26
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL .05G 0129_36 01/30/24 00:30
CAL .1G 0129_37 01/30/24 00:49
CAL .5G 0129_38 01/30/24 01:08
CAL 1G 0129_39 01/30/24 01:28
CAL 2.5G 0129_40 01/30/24 01:47
CAL 5G 0129_41 01/30/24 02:06
CAL 10G 0129_42 01/30/24 02:26
SSCV VOCGC17012924A0129_45740290 0129_45 01/30/24 03:23
ICV VOCGC170725240725_03740290 0725_03 07/25/24 10:04
LCS R4098870-1 0725_04A 07/25/24 10:23 1 WG2329597
LCS R4098321-1 0725_04 07/25/24 10:23 1 WG2329941
LCSD R4098870-2 0725_05A 07/25/24 10:43 1 WG2329597
LCSD R4098321-2 0725_05 07/25/24 10:43 1 WG2329941
BLANK R4098870-3 0725_07 07/25/24 11:36 1 WG2329597
BLANK R4098321-3 0725_08 07/25/24 11:56 25 WG2329941
L1758945-14 L1758945-14 0725_09 07/25/24 12:23 32.5 WG2329941
S-9 (0-6)L1757957-04 0725_11 07/25/24 13:02 25.8 WG2329941
S-7 (0-6)L1757957-06 0725_12 07/25/24 13:21 34.3 WG2329941
S-6 (0-6)L1757957-08 0725_13 07/25/24 13:40 25 WG2329941
S-5 (0-6)L1757957-09 0725_14 07/25/24 14:00 25 WG2329941
S-4 (0-6)L1757957-10 0725_15 07/25/24 14:19 28.5 WG2329941
S-31 (0-6)L1757957-11 0725_16 07/25/24 14:39 30.3 WG2329941
L1757983-10 L1757983-10 0725_20 07/25/24 15:56 1 WG2329597
L1757983-11 L1757983-11 0725_21 07/25/24 16:16 1 WG2329597
L1757983-12 L1757983-12 0725_22 07/25/24 16:35 1 WG2329597
L1757983-13 L1757983-13 0725_23 07/25/24 16:55 1 WG2329597
L1758079-01 L1758079-01 0725_24 07/25/24 17:14 1 WG2329597
L1758079-03 L1758079-03 0725_25 07/25/24 17:33 1 WG2329597
L1757987-01 L1757987-01 0725_26 07/25/24 17:52 1 WG2329597
L1757987-02 L1757987-02 0725_27 07/25/24 18:12 1 WG2329597
L1757987-03 L1757987-03 0725_28 07/25/24 18:31 1.01 WG2329597
L1757987-04 L1757987-04 0725_29 07/25/24 18:51 1 WG2329597
L1757987-05 L1757987-05 0725_30 07/25/24 19:10 1 WG2329597
L1757987-06 L1757987-06 0725_31 07/25/24 19:29 1 WG2329597
L1757987-07 L1757987-07 0725_32 07/25/24 19:48 1 WG2329597
L1757987-08 L1757987-08 0725_33 07/25/24 20:08 1 WG2329597
L1757987-09 L1757987-09 0725_34 07/25/24 20:27 1 WG2329597
L1757987-10 L1757987-10 0725_35 07/25/24 20:46 1 WG2329597
L1757987-11 L1757987-11 0725_36 07/25/24 21:08 1 WG2329597
L1757987-12 L1757987-12 0725_37 07/25/24 21:28 1 WG2329597
L1757987-22 L1757987-22 0725_38 07/25/24 21:47 1 WG2329597
L1757987-23 L1757987-23 0725_39 07/25/24 22:07 1 WG2329597
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16 Analytical Method:8015D/GRO
Matrix:GW Prep Method:8015D/GRO
Analyte CAS MDL RDL
mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 0.0314 0.10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:8015D/GRO
Matrix:Solid Prep Method:8015D/GRO
Analyte CAS MDL RDL
mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 0.0217 0.10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098253-2
Lab Sample ID:R4098253-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0724_07 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:07/24/24 18:25
Analytical Batch:WG2329459 Analysis Date/Time:07/24/24 18:25
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 1.06 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098321-3
Lab Sample ID:R4098321-3 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_08 Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:07/25/24 11:56
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 11:56
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 U 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098479-3
Lab Sample ID:R4098479-3 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_10 Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/25/24 12:59
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 12:59
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 0.738 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098551-2
Lab Sample ID:R4098551-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0723_05 Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/23/24 12:49
Analytical Batch:WG2327971 Analysis Date/Time:07/23/24 12:49
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 U 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098862-2
Lab Sample ID:R4098862-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0724_05 Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/24/24 10:54
Analytical Batch:WG2328825 Analysis Date/Time:07/24/24 10:54
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 0.657 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100114-2
Lab Sample ID:R4100114-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0728_06 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:07/28/24 11:14
Analytical Batch:WG2330767 Analysis Date/Time:07/28/24 11:14
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 2.01 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100115-2
Lab Sample ID:R4100115-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0728_06C Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:07/28/24 11:14
Analytical Batch:WG2330774 Analysis Date/Time:07/28/24 11:14
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 2.01 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098253-1
Lab Sample ID:R4098253-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0724_04 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:07/24/24 17:08
Analytical Batch:WG2329459 Analysis Date/Time:07/24/24 17:08
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 5.16 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098321-1
Lab Sample ID:R4098321-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_04 Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:07/25/24 10:23
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 10:23
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 4.94 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098479-1
Lab Sample ID:R4098479-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_07u Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/25/24 11:50
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 11:50
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 4.65 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098551-1
Lab Sample ID:R4098551-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0723_03U Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/23/24 12:03
Analytical Batch:WG2327971 Analysis Date/Time:07/23/24 12:03
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 4.52 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098862-1
Lab Sample ID:R4098862-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0724_03U Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/24/24 10:08
Analytical Batch:WG2328825 Analysis Date/Time:07/24/24 10:08
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 4.72 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100114-1
Lab Sample ID:R4100114-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0728_03 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:07/28/24 10:03
Analytical Batch:WG2330767 Analysis Date/Time:07/28/24 10:03
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 5.54 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100115-1
Lab Sample ID:R4100115-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0728_03C Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:07/28/24 10:03
Analytical Batch:WG2330774 Analysis Date/Time:07/28/24 10:03
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 5.54 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098321-2
Lab Sample ID:R4098321-2 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0725_05 Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:07/25/24 10:43
Analytical Batch:WG2329941 Analysis Date/Time:07/25/24 10:43
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 4.99 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098479-2
Lab Sample ID:R4098479-2 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0725_08 Received Date/Time:_______________
Instrument ID:VOCGC10 Preparation Date/Time:07/25/24 12:13
Analytical Batch:WG2329829 Analysis Date/Time:07/25/24 12:13
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 5.66 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098551-3
Lab Sample ID:R4098551-3 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 10:45
Lab File ID:0723_32 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/24/24 00:06
Analytical Batch:WG2327971 Analysis Date/Time:07/24/24 00:06
Dilution Factor:1 Prep Method:8015/NWTPHGX
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 4.47 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100115-3
Lab Sample ID:R4100115-3 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:0728_21 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2330774 Analysis Date/Time:07/28/24 17:35
Dilution Factor:27.5 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 112 0.613 2.82
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098551-4
Lab Sample ID:R4098551-4 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 10:45
Lab File ID:0723_33 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC10 Preparation Date/Time:07/24/24 00:28
Analytical Batch:WG2327971 Analysis Date/Time:07/24/24 00:28
Dilution Factor:1 Prep Method:8015/NWTPHGX
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 5.92 J3 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100115-4
Lab Sample ID:R4100115-4 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:0728_22 Received Date/Time:07/18/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2330774 Analysis Date/Time:07/28/24 17:59
Dilution Factor:27.5 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 128 0.613 2.82
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8260B Volatile Organic Compounds (GC/MS)
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2A-OR SURROGATE RECOVERY
Analytical Method:8260B SDG:L1757957
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 DMC-2 DMC-3 TOT Out
% Rec.% Rec.% Rec.
EB-1-071624 L1757957-16 VOCMS21 0721_35 101 110 111 0
TRIP BLANK L1757957-17 VOCMS21 0721_33 103 110 107 0
BLANK R4097932-3 VOCMS21 0721_32 102 109 109 0
LCS R4097932-1 VOCMS21 0721_28LCS 102 110 109 0
LCSD R4097932-2 VOCMS21 0721_29 101 110 109 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 Toluene-d8 80.0 - 120
DMC-2 4-Bromofluorobenzene 77.0 - 126
DMC-3 1,2-Dichloroethane-d4 70.0 - 130
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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2A-OR SURROGATE RECOVERY
Analytical Method:8260B SDG:L1757957
Matrix:Solid
Sample ID Lab Sample ID Instrument File ID DMC-1 DMC-2 DMC-3 TOT Out
% Rec.% Rec.% Rec.
S-3 (0-6)L1757957-01 VOCMS58 0725_53 103 105 92.3 0
S-3 (6-12)L1757957-02 VOCMS58 0725_41 103 105 89.1 0
S-30 (6-12)L1757957-03 VOCMS58 0725_42 103 104 87.4 0
S-9 (0-6)L1757957-04 VOCMS58 0725_54 106 105 90.4 0
S-8 (0-6)L1757957-05 VOCMS58 0725_43 104 105 88.7 0
S-7 (0-6)L1757957-06 VOCMS58 0725_55 103 107 88.5 0
S-7 (6-12)L1757957-07 VOCMS58 0725_44 105 105 87.6 0
S-6 (0-6)L1757957-08 VOCMS58 0725_56 104 102 87.8 0
S-5 (0-6)L1757957-09 VOCMS56 0725_28 95.4 104 106 0
S-4 (0-6)L1757957-10 VOCMS56 0725_29 96.8 101 107 0
S-31 (0-6)L1757957-11 VOCMS56 0725_30 96.1 102 106 0
S-2 (0-6)L1757957-12 VOCMS56 0725_24 94.4 104 111 0
S-1 (0-6)L1757957-13 VOCMS56 0724A_16 102 104 89.4 0
S-1 (6-12)L1757957-14 VOCMS56 0724A_17 99.5 104 93.3 0
SS-1 (6-12)L1757957-15 VOCMS56 0724A_18 100 106 92.8 0
MS R4098455-4 VOCMS58 0725_59 103 105 84.6 0
MSD R4098455-5 VOCMS58 0725_60 102 105 92.0 0
BLANK R4098226-2 VOCMS56 0724A_07 98.8 103 94.4 0
BLANK R4098753-2 VOCMS56 0725_07 118 105 96.5 0
BLANK R4098455-3 VOCMS58 0725_34 105 101 88.3 0
LCS R4098226-1 VOCMS56 0724A_03LCS 97.9 103 101 0
LCS R4098753-1 VOCMS56 0725_03LCS 98.9 102 98.4 0
LCS R4098455-1 VOCMS58 0725_29LCS 103 104 97.8 0
LCSD R4098455-2 VOCMS58 0725_30 102 103 95.8 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 Toluene-d8 75.0 - 131
DMC-2 4-Bromofluorobenzene 67.0 - 138
DMC-3 1,2-Dichloroethane-d4 70.0 - 130
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4098455-4
L1757957-01,02,03,04,05,06,07,08 R4098455-5
MS Sample / File ID:R4098455-4 / 0725_59 SDG:L1757957
MSD Sample / File ID:R4098455-5 / 0725_60 Analytical Batch:WG2329486
OS Sample / File ID:L1757957-01 / 0725_53 Matrix:Solid
Instrument ID:VOCMS58
Analytical Method:8260B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.707 U 0.282 0.109 40.0 15.4 1.1 10.0 - 160 88.7*40
Acrylonitrile 0.707 U 0.485 0.507 68.6 71.8 1.1 10.0 - 160 4.55 40
Benzene 0.142 0.00169 0.128 0.127 89.4 88.7 1.1 10.0 - 149 0.803 37
Bromobenzene 0.142 U 0.126 0.127 89.1 89.9 1.1 10.0 - 156 0.810 38
Bromodichloromethane 0.142 U 0.122 0.128 86.2 90.6 1.1 10.0 - 143 4.92 37
Bromoform 0.142 U 0.112 0.112 79.0 79.0 1.1 10.0 - 146 0.000 36
Bromomethane 0.142 U 0.0731 0.0704 51.6 49.6 1.1 10.0 - 149 3.87 38
n-Butylbenzene 0.142 U 0.159 0.162 112 114 1.1 10.0 - 160 1.92 40
sec-Butylbenzene 0.142 U 0.151 0.154 107 109 1.1 10.0 - 159 2.02 39
tert-Butylbenzene 0.142 U 0.139 0.146 97.8 103 1.1 10.0 - 156 5.05 39
Carbon tetrachloride 0.142 U 0.130 0.124 92.0 87.7 1.1 10.0 - 145 4.84 37
Chlorobenzene 0.142 U 0.134 0.131 94.2 92.8 1.1 10.0 - 152 1.55 39
Chlorodibromomethane 0.142 U 0.123 0.125 87.0 88.4 1.1 10.0 - 146 1.65 37
Chloroethane 0.142 U 0.0558 0.0660 39.3 46.6 1.1 10.0 - 146 16.9 40
Chloroform 0.142 U 0.132 0.128 93.5 90.6 1.1 10.0 - 146 3.15 37
Chloromethane 0.142 U 0.114 0.109 80.4 76.8 1.1 10.0 - 159 4.61 37
2-Chlorotoluene 0.142 U 0.134 0.138 94.2 97.1 1.1 10.0 - 159 3.03 38
4-Chlorotoluene 0.142 U 0.136 0.136 95.7 95.7 1.1 10.0 - 155 0.000 39
1,2-Dibromo-3-Chloropropane 0.142 U 0.0863 0.0974 60.9 68.7 1.1 10.0 - 151 12.1 39
1,2-Dibromoethane 0.142 U 0.127 0.130 89.9 92.0 1.1 10.0 - 148 2.39 34
Dibromomethane 0.142 U 0.115 0.119 81.2 84.1 1.1 10.0 - 147 3.51 35
1,2-Dichlorobenzene 0.142 U 0.131 0.139 92.8 97.8 1.1 10.0 - 155 5.32 37
1,3-Dichlorobenzene 0.142 U 0.134 0.136 94.2 95.7 1.1 10.0 - 153 1.53 38
1,4-Dichlorobenzene 0.142 U 0.131 0.132 92.8 93.5 1.1 10.0 - 151 0.778 38
Dichlorodifluoromethane 0.142 U 0.139 0.126 97.8 89.1 1.1 10.0 - 160 9.30 35
1,1-Dichloroethane 0.142 U 0.129 0.127 91.3 89.9 1.1 10.0 - 147 1.60 37
1,2-Dichloroethane 0.142 U 0.111 0.112 78.3 79.0 1.1 10.0 - 148 0.922 35
1,1-Dichloroethene 0.142 U 0.129 0.123 91.3 87.0 1.1 10.0 - 155 4.88 37
cis-1,2-Dichloroethene 0.142 U 0.132 0.135 93.5 94.9 1.1 10.0 - 149 1.54 37
trans-1,2-Dichloroethene 0.142 U 0.128 0.123 90.6 87.0 1.1 10.0 - 150 4.08 37
1,2-Dichloropropane 0.142 U 0.128 0.131 90.6 92.8 1.1 10.0 - 148 2.37 37
1,1-Dichloropropene 0.142 U 0.134 0.126 94.2 89.1 1.1 10.0 - 153 5.53 35
1,3-Dichloropropane 0.142 U 0.134 0.132 94.2 93.5 1.1 10.0 - 154 0.772 35
cis-1,3-Dichloropropene 0.142 U 0.135 0.135 94.9 94.9 1.1 10.0 - 151 0.000 37
trans-1,3-Dichloropropene 0.142 U 0.138 0.139 97.1 97.8 1.1 10.0 - 148 0.743 37
2,2-Dichloropropane 0.142 U 0.110 0.108 77.5 76.1 1.1 10.0 - 138 1.89 36
Di-isopropyl ether 0.142 U 0.134 0.131 94.2 92.8 1.1 10.0 - 147 1.55 36
Ethylbenzene 0.142 U 0.139 0.136 97.8 95.7 1.1 10.0 - 160 2.25 38
Hexachloro-1,3-butadiene 0.142 U 0.183 0.197 129 139 1.1 10.0 - 160 7.57 40
Isopropylbenzene 0.142 U 0.150 0.149 106 105 1.1 10.0 - 155 0.687 38
p-Isopropyltoluene 0.142 U 0.153 0.158 108 112 1.1 10.0 - 160 3.30 40
2-Butanone (MEK)0.707 U 0.420 0.447 59.4 63.2 1.1 10.0 - 160 6.16 40
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4098455-4
L1757957-01,02,03,04,05,06,07,08 R4098455-5
MS Sample / File ID:R4098455-4 / 0725_59 SDG:L1757957
MSD Sample / File ID:R4098455-5 / 0725_60 Analytical Batch:WG2329486
OS Sample / File ID:L1757957-01 / 0725_53 Matrix:Solid
Instrument ID:VOCMS58
Analytical Method:8260B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
Methylene Chloride 0.142 0.00797 0.130 0.126 86.4 83.5 1.1 10.0 - 141 3.20 37
4-Methyl-2-pentanone (MIBK)0.707 U 0.575 0.592 81.4 83.7 1.1 10.0 - 160 2.82 35
Methyl tert-butyl ether 0.142 U 0.119 0.125 84.1 88.4 1.1 11.0 - 147 5.04 35
Naphthalene 0.142 0.0113 0.108 0.121 68.1 77.5 1.1 10.0 - 160 11.7 36
n-Propylbenzene 0.142 U 0.132 0.137 93.5 96.4 1.1 10.0 - 158 3.05 38
Styrene 0.142 U 0.146 0.142 103 100 1.1 10.0 - 160 2.86 40
1,1,1,2-Tetrachloroethane 0.142 U 0.134 0.130 94.2 92.0 1.1 10.0 - 149 2.33 39
1,1,2,2-Tetrachloroethane 0.142 U 0.111 0.110 78.3 77.5 1.1 10.0 - 160 0.930 35
1,1,2-Trichlorotrifluoroethane 0.142 U 0.147 0.140 104 98.6 1.1 10.0 - 160 5.02 36
Tetrachloroethene 0.142 U 0.136 0.134 95.7 94.2 1.1 10.0 - 156 1.53 39
Toluene 0.142 0.00316 0.131 0.129 90.5 89.1 1.1 10.0 - 156 1.57 38
1,2,3-Trichlorobenzene 0.142 U 0.163 0.161 115 114 1.1 10.0 - 160 1.27 40
1,2,4-Trichlorobenzene 0.142 U 0.164 0.166 116 117 1.1 10.0 - 160 1.24 40
1,1,1-Trichloroethane 0.142 U 0.136 0.134 95.7 94.2 1.1 10.0 - 144 1.53 35
1,1,2-Trichloroethane 0.142 U 0.137 0.135 96.4 94.9 1.1 10.0 - 160 1.52 35
Trichloroethene 0.142 U 0.131 0.138 92.8 97.1 1.1 10.0 - 156 4.58 38
Trichlorofluoromethane 0.142 U 0.0615 0.0719 43.4 50.7 1.1 10.0 - 160 15.6 40
1,2,3-Trichloropropane 0.142 U 0.115 0.121 81.2 85.5 1.1 10.0 - 156 5.22 35
1,2,4-Trimethylbenzene 0.142 0.00426 0.146 0.148 99.9 101 1.1 10.0 - 160 1.40 36
1,2,3-Trimethylbenzene 0.142 0.00319 0.128 0.136 88.3 93.4 1.1 10.0 - 160 5.45 36
1,3,5-Trimethylbenzene 0.142 U 0.143 0.145 101 102 1.1 10.0 - 160 1.43 38
Vinyl chloride 0.142 U 0.129 0.123 91.3 87.0 1.1 10.0 - 160 4.88 37
Xylenes, Total 0.424 0.00886 0.425 0.424 98.2 97.9 1.1 10.0 - 160 0.242 38
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4097932-1
RECOVERY R4097932-2
L1757957-16,17
LCS Sample / File ID:R4097932-1 / 0721_28LCS SDG:L1757957
LCSD Sample / File ID:R4097932-2 / 0721_29 Analytical Batch:WG2327390
Instrument ID:VOCMS21 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0233 0.0234 93.2 93.6 19.0 - 160 0.428 27
Acrolein 0.0250 0.0261 0.0289 104 116 10.0 - 160 10.2 26
Acrylonitrile 0.0250 0.0245 0.0266 98.0 106 55.0 - 149 8.22 20
Benzene 0.00500 0.00530 0.00570 106 114 70.0 - 123 7.27 20
Bromobenzene 0.00500 0.00498 0.00527 99.6 105 73.0 - 121 5.66 20
Bromodichloromethane 0.00500 0.00482 0.00522 96.4 104 75.0 - 120 7.97 20
Bromoform 0.00500 0.00360 0.00382 72.0 76.4 68.0 - 132 5.93 20
Bromomethane 0.00500 0.00195 0.00236 39.0 47.2 10.0 - 160 19.0 25
n-Butylbenzene 0.00500 0.00470 0.00498 94.0 99.6 73.0 - 125 5.79 20
sec-Butylbenzene 0.00500 0.00483 0.00512 96.6 102 75.0 - 125 5.83 20
tert-Butylbenzene 0.00500 0.00485 0.00511 97.0 102 76.0 - 124 5.22 20
Carbon tetrachloride 0.00500 0.00462 0.00504 92.4 101 68.0 - 126 8.70 20
Chlorobenzene 0.00500 0.00438 0.00457 87.6 91.4 80.0 - 121 4.25 20
Chlorodibromomethane 0.00500 0.00413 0.00433 82.6 86.6 77.0 - 125 4.73 20
Chloroethane 0.00500 0.0112 0.0104 224*208*47.0 - 150 7.41 20
Chloroform 0.00500 0.00492 0.00499 98.4 99.8 73.0 - 120 1.41 20
Chloromethane 0.00500 0.00446 0.00498 89.2 99.6 41.0 - 142 11.0 20
2-Chlorotoluene 0.00500 0.00500 0.00536 100 107 76.0 - 123 6.95 20
4-Chlorotoluene 0.00500 0.00476 0.00514 95.2 103 75.0 - 122 7.68 20
1,2-Dibromo-3-Chloropropane 0.00500 0.00362 0.00398 72.4 79.6 58.0 - 134 9.47 20
1,2-Dibromoethane 0.00500 0.00434 0.00450 86.8 90.0 80.0 - 122 3.62 20
Dibromomethane 0.00500 0.00485 0.00519 97.0 104 80.0 - 120 6.77 20
1,2-Dichlorobenzene 0.00500 0.00425 0.00460 85.0 92.0 79.0 - 121 7.91 20
1,3-Dichlorobenzene 0.00500 0.00442 0.00455 88.4 91.0 79.0 - 120 2.90 20
1,4-Dichlorobenzene 0.00500 0.00431 0.00464 86.2 92.8 79.0 - 120 7.37 20
Dichlorodifluoromethane 0.00500 0.00424 0.00497 84.8 99.4 51.0 - 149 15.9 20
1,1-Dichloroethane 0.00500 0.00504 0.00553 101 111 70.0 - 126 9.27 20
1,2-Dichloroethane 0.00500 0.00505 0.00538 101 108 70.0 - 128 6.33 20
1,1-Dichloroethene 0.00500 0.00498 0.00561 99.6 112 71.0 - 124 11.9 20
cis-1,2-Dichloroethene 0.00500 0.00479 0.00542 95.8 108 73.0 - 120 12.3 20
trans-1,2-Dichloroethene 0.00500 0.00512 0.00517 102 103 73.0 - 120 0.972 20
1,2-Dichloropropane 0.00500 0.00525 0.00556 105 111 77.0 - 125 5.74 20
1,1-Dichloropropene 0.00500 0.00495 0.00545 99.0 109 74.0 - 126 9.62 20
1,3-Dichloropropane 0.00500 0.00470 0.00495 94.0 99.0 80.0 - 120 5.18 20
cis-1,3-Dichloropropene 0.00500 0.00499 0.00526 99.8 105 80.0 - 123 5.27 20
trans-1,3-Dichloropropene 0.00500 0.00465 0.00485 93.0 97.0 78.0 - 124 4.21 20
2,2-Dichloropropane 0.00500 0.00482 0.00512 96.4 102 58.0 - 130 6.04 20
Di-isopropyl ether 0.00500 0.00551 0.00587 110 117 58.0 - 138 6.33 20
Ethylbenzene 0.00500 0.00451 0.00469 90.2 93.8 79.0 - 123 3.91 20
Hexachloro-1,3-butadiene 0.00500 0.00362 0.00373 72.4 74.6 54.0 - 138 2.99 20
Isopropylbenzene 0.00500 0.00449 0.00481 89.8 96.2 76.0 - 127 6.88 20
p-Isopropyltoluene 0.00500 0.00471 0.00511 94.2 102 76.0 - 125 8.15 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4097932-1
RECOVERY R4097932-2
L1757957-16,17
LCS Sample / File ID:R4097932-1 / 0721_28LCS SDG:L1757957
LCSD Sample / File ID:R4097932-2 / 0721_29 Analytical Batch:WG2327390
Instrument ID:VOCMS21 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
2-Butanone (MEK)0.0250 0.0238 0.0258 95.2 103 44.0 - 160 8.06 20
Methylene Chloride 0.00500 0.00490 0.00572 98.0 114 67.0 - 120 15.4 20
4-Methyl-2-pentanone (MIBK)0.0250 0.0248 0.0265 99.2 106 68.0 - 142 6.63 20
Methyl tert-butyl ether 0.00500 0.00518 0.00555 104 111 68.0 - 125 6.90 20
Naphthalene 0.00500 0.00451 0.00445 90.2 89.0 54.0 - 135 1.34 20
n-Propylbenzene 0.00500 0.00518 0.00551 104 110 77.0 - 124 6.17 20
Styrene 0.00500 0.00409 0.00430 81.8 86.0 73.0 - 130 5.01 20
1,1,1,2-Tetrachloroethane 0.00500 0.00409 0.00441 81.8 88.2 75.0 - 125 7.53 20
1,1,2,2-Tetrachloroethane 0.00500 0.00476 0.00525 95.2 105 65.0 - 130 9.79 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00489 0.00533 97.8 107 69.0 - 132 8.61 20
Tetrachloroethene 0.00500 0.00381 0.00407 76.2 81.4 72.0 - 132 6.60 20
Toluene 0.00500 0.00464 0.00484 92.8 96.8 79.0 - 120 4.22 20
1,2,3-Trichlorobenzene 0.00500 0.00365 0.00385 73.0 77.0 50.0 - 138 5.33 20
1,2,4-Trichlorobenzene 0.00500 0.00359 0.00383 71.8 76.6 57.0 - 137 6.47 20
1,1,1-Trichloroethane 0.00500 0.00475 0.00524 95.0 105 73.0 - 124 9.81 20
1,1,2-Trichloroethane 0.00500 0.00439 0.00467 87.8 93.4 80.0 - 120 6.18 20
Trichloroethene 0.00500 0.00465 0.00491 93.0 98.2 78.0 - 124 5.44 20
Trichlorofluoromethane 0.00500 0.00474 0.00532 94.8 106 59.0 - 147 11.5 20
1,2,3-Trichloropropane 0.00500 0.00455 0.00488 91.0 97.6 73.0 - 130 7.00 20
1,2,4-Trimethylbenzene 0.00500 0.00506 0.00523 101 105 76.0 - 121 3.30 20
1,2,3-Trimethylbenzene 0.00500 0.00501 0.00526 100 105 77.0 - 120 4.87 20
1,3,5-Trimethylbenzene 0.00500 0.00501 0.00523 100 105 76.0 - 122 4.30 20
Vinyl chloride 0.00500 0.00530 0.00590 106 118 67.0 - 131 10.7 20
Xylenes, Total 0.0150 0.0136 0.0140 90.7 93.3 79.0 - 123 2.90 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098226-1
RECOVERY _______________
L1757957-13,14,15
LCS Sample / File ID:R4098226-1 / 0724A_03LCS SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2329566
Instrument ID:VOCMS56 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
Acetone 0.625 0.531 85.0 10.0 - 160
Acrylonitrile 0.625 0.857 137 45.0 - 153
Benzene 0.125 0.116 92.8 70.0 - 123
Bromobenzene 0.125 0.125 100 73.0 - 121
Bromodichloromethane 0.125 0.139 111 73.0 - 121
Bromoform 0.125 0.160 128 64.0 - 132
Bromomethane 0.125 0.141 113 56.0 - 147
n-Butylbenzene 0.125 0.102 81.6 68.0 - 135
sec-Butylbenzene 0.125 0.104 83.2 74.0 - 130
tert-Butylbenzene 0.125 0.112 89.6 75.0 - 127
Carbon tetrachloride 0.125 0.139 111 66.0 - 128
Chlorobenzene 0.125 0.119 95.2 76.0 - 128
Chlorodibromomethane 0.125 0.132 106 74.0 - 127
Chloroethane 0.125 0.170 136*61.0 - 134
Chloroform 0.125 0.117 93.6 72.0 - 123
Chloromethane 0.125 0.112 89.6 51.0 - 138
2-Chlorotoluene 0.125 0.114 91.2 75.0 - 124
4-Chlorotoluene 0.125 0.118 94.4 75.0 - 124
1,2-Dibromo-3-Chloropropane 0.125 0.155 124 59.0 - 130
1,2-Dibromoethane 0.125 0.127 102 74.0 - 128
Dibromomethane 0.125 0.130 104 75.0 - 122
1,2-Dichlorobenzene 0.125 0.130 104 76.0 - 124
1,3-Dichlorobenzene 0.125 0.121 96.8 76.0 - 125
1,4-Dichlorobenzene 0.125 0.117 93.6 77.0 - 121
Dichlorodifluoromethane 0.125 0.128 102 43.0 - 156
1,1-Dichloroethane 0.125 0.124 99.2 70.0 - 127
1,2-Dichloroethane 0.125 0.124 99.2 65.0 - 131
1,1-Dichloroethene 0.125 0.113 90.4 65.0 - 131
cis-1,2-Dichloroethene 0.125 0.123 98.4 73.0 - 125
trans-1,2-Dichloroethene 0.125 0.127 102 71.0 - 125
1,2-Dichloropropane 0.125 0.126 101 74.0 - 125
1,1-Dichloropropene 0.125 0.124 99.2 73.0 - 125
1,3-Dichloropropane 0.125 0.122 97.6 80.0 - 125
cis-1,3-Dichloropropene 0.125 0.135 108 76.0 - 127
trans-1,3-Dichloropropene 0.125 0.128 102 73.0 - 127
2,2-Dichloropropane 0.125 0.110 88.0 59.0 - 135
Di-isopropyl ether 0.125 0.145 116 60.0 - 136
Ethylbenzene 0.125 0.118 94.4 74.0 - 126
Hexachloro-1,3-butadiene 0.125 0.131 105 57.0 - 150
Isopropylbenzene 0.125 0.124 99.2 72.0 - 127
p-Isopropyltoluene 0.125 0.109 87.2 72.0 - 133
2-Butanone (MEK)0.625 0.644 103 30.0 - 160
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098226-1
RECOVERY _______________
L1757957-13,14,15
LCS Sample / File ID:R4098226-1 / 0724A_03LCS SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2329566
Instrument ID:VOCMS56 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
Methylene Chloride 0.125 0.111 88.8 68.0 - 123
4-Methyl-2-pentanone (MIBK)0.625 0.743 119 56.0 - 143
Methyl tert-butyl ether 0.125 0.148 118 66.0 - 132
Naphthalene 0.125 0.128 102 59.0 - 130
n-Propylbenzene 0.125 0.113 90.4 74.0 - 126
Styrene 0.125 0.118 94.4 72.0 - 127
1,1,1,2-Tetrachloroethane 0.125 0.143 114 74.0 - 129
1,1,2,2-Tetrachloroethane 0.125 0.128 102 68.0 - 128
1,1,2-Trichlorotrifluoroethane 0.125 0.106 84.8 61.0 - 139
Tetrachloroethene 0.125 0.130 104 70.0 - 136
Toluene 0.125 0.118 94.4 75.0 - 121
1,2,3-Trichlorobenzene 0.125 0.161 129 59.0 - 139
1,2,4-Trichlorobenzene 0.125 0.136 109 62.0 - 137
1,1,1-Trichloroethane 0.125 0.141 113 69.0 - 126
1,1,2-Trichloroethane 0.125 0.128 102 78.0 - 123
Trichloroethene 0.125 0.129 103 76.0 - 126
Trichlorofluoromethane 0.125 0.109 87.2 61.0 - 142
1,2,3-Trichloropropane 0.125 0.115 92.0 67.0 - 129
1,2,4-Trimethylbenzene 0.125 0.114 91.2 70.0 - 126
1,2,3-Trimethylbenzene 0.125 0.110 88.0 74.0 - 124
1,3,5-Trimethylbenzene 0.125 0.116 92.8 73.0 - 127
Vinyl chloride 0.125 0.102 81.6 63.0 - 134
Xylenes, Total 0.375 0.357 95.2 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098455-1
RECOVERY R4098455-2
L1757957-01,02,03,04,05,06,07,08
LCS Sample / File ID:R4098455-1 / 0725_29LCS SDG:L1757957
LCSD Sample / File ID:R4098455-2 / 0725_30 Analytical Batch:WG2329486
Instrument ID:VOCMS58 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.630 0.610 101 97.6 10.0 - 160 3.23 31
Acrylonitrile 0.625 0.675 0.656 108 105 45.0 - 153 2.85 22
Benzene 0.125 0.121 0.122 96.8 97.6 70.0 - 123 0.823 20
Bromobenzene 0.125 0.116 0.117 92.8 93.6 73.0 - 121 0.858 20
Bromodichloromethane 0.125 0.119 0.119 95.2 95.2 73.0 - 121 0.000 20
Bromoform 0.125 0.114 0.114 91.2 91.2 64.0 - 132 0.000 20
Bromomethane 0.125 0.105 0.110 84.0 88.0 56.0 - 147 4.65 20
n-Butylbenzene 0.125 0.119 0.121 95.2 96.8 68.0 - 135 1.67 20
sec-Butylbenzene 0.125 0.119 0.124 95.2 99.2 74.0 - 130 4.12 20
tert-Butylbenzene 0.125 0.118 0.120 94.4 96.0 75.0 - 127 1.68 20
Carbon tetrachloride 0.125 0.117 0.119 93.6 95.2 66.0 - 128 1.69 20
Chlorobenzene 0.125 0.120 0.119 96.0 95.2 76.0 - 128 0.837 20
Chlorodibromomethane 0.125 0.119 0.121 95.2 96.8 74.0 - 127 1.67 20
Chloroethane 0.125 0.116 0.115 92.8 92.0 61.0 - 134 0.866 20
Chloroform 0.125 0.120 0.119 96.0 95.2 72.0 - 123 0.837 20
Chloromethane 0.125 0.105 0.133 84.0 106 51.0 - 138 23.5*20
2-Chlorotoluene 0.125 0.120 0.120 96.0 96.0 75.0 - 124 0.000 20
4-Chlorotoluene 0.125 0.116 0.119 92.8 95.2 75.0 - 124 2.55 20
1,2-Dibromo-3-Chloropropane 0.125 0.113 0.115 90.4 92.0 59.0 - 130 1.75 20
1,2-Dibromoethane 0.125 0.124 0.122 99.2 97.6 74.0 - 128 1.63 20
Dibromomethane 0.125 0.120 0.119 96.0 95.2 75.0 - 122 0.837 20
1,2-Dichlorobenzene 0.125 0.119 0.120 95.2 96.0 76.0 - 124 0.837 20
1,3-Dichlorobenzene 0.125 0.119 0.119 95.2 95.2 76.0 - 125 0.000 20
1,4-Dichlorobenzene 0.125 0.113 0.117 90.4 93.6 77.0 - 121 3.48 20
Dichlorodifluoromethane 0.125 0.100 0.101 80.0 80.8 43.0 - 156 0.995 20
1,1-Dichloroethane 0.125 0.120 0.122 96.0 97.6 70.0 - 127 1.65 20
1,2-Dichloroethane 0.125 0.109 0.108 87.2 86.4 65.0 - 131 0.922 20
1,1-Dichloroethene 0.125 0.118 0.120 94.4 96.0 65.0 - 131 1.68 20
cis-1,2-Dichloroethene 0.125 0.123 0.128 98.4 102 73.0 - 125 3.98 20
trans-1,2-Dichloroethene 0.125 0.123 0.123 98.4 98.4 71.0 - 125 0.000 20
1,2-Dichloropropane 0.125 0.122 0.120 97.6 96.0 74.0 - 125 1.65 20
1,1-Dichloropropene 0.125 0.121 0.121 96.8 96.8 73.0 - 125 0.000 20
1,3-Dichloropropane 0.125 0.126 0.121 101 96.8 80.0 - 125 4.05 20
cis-1,3-Dichloropropene 0.125 0.120 0.121 96.0 96.8 76.0 - 127 0.830 20
trans-1,3-Dichloropropene 0.125 0.125 0.126 100 101 73.0 - 127 0.797 20
2,2-Dichloropropane 0.125 0.114 0.113 91.2 90.4 59.0 - 135 0.881 20
Di-isopropyl ether 0.125 0.122 0.123 97.6 98.4 60.0 - 136 0.816 20
Ethylbenzene 0.125 0.121 0.123 96.8 98.4 74.0 - 126 1.64 20
Hexachloro-1,3-butadiene 0.125 0.117 0.121 93.6 96.8 57.0 - 150 3.36 20
Isopropylbenzene 0.125 0.127 0.129 102 103 72.0 - 127 1.56 20
p-Isopropyltoluene 0.125 0.124 0.127 99.2 102 72.0 - 133 2.39 20
2-Butanone (MEK)0.625 0.645 0.627 103 100 30.0 - 160 2.83 24
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098455-1
RECOVERY R4098455-2
L1757957-01,02,03,04,05,06,07,08
LCS Sample / File ID:R4098455-1 / 0725_29LCS SDG:L1757957
LCSD Sample / File ID:R4098455-2 / 0725_30 Analytical Batch:WG2329486
Instrument ID:VOCMS58 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
Methylene Chloride 0.125 0.116 0.116 92.8 92.8 68.0 - 123 0.000 20
4-Methyl-2-pentanone (MIBK)0.625 0.654 0.646 105 103 56.0 - 143 1.23 20
Methyl tert-butyl ether 0.125 0.130 0.126 104 101 66.0 - 132 3.12 20
Naphthalene 0.125 0.109 0.112 87.2 89.6 59.0 - 130 2.71 20
n-Propylbenzene 0.125 0.116 0.118 92.8 94.4 74.0 - 126 1.71 20
Styrene 0.125 0.129 0.129 103 103 72.0 - 127 0.000 20
1,1,1,2-Tetrachloroethane 0.125 0.125 0.124 100 99.2 74.0 - 129 0.803 20
1,1,2,2-Tetrachloroethane 0.125 0.122 0.121 97.6 96.8 68.0 - 128 0.823 20
1,1,2-Trichlorotrifluoroethane 0.125 0.119 0.122 95.2 97.6 61.0 - 139 2.49 20
Tetrachloroethene 0.125 0.122 0.124 97.6 99.2 70.0 - 136 1.63 20
Toluene 0.125 0.117 0.117 93.6 93.6 75.0 - 121 0.000 20
1,2,3-Trichlorobenzene 0.125 0.133 0.134 106 107 59.0 - 139 0.749 20
1,2,4-Trichlorobenzene 0.125 0.130 0.133 104 106 62.0 - 137 2.28 20
1,1,1-Trichloroethane 0.125 0.123 0.126 98.4 101 69.0 - 126 2.41 20
1,1,2-Trichloroethane 0.125 0.125 0.127 100 102 78.0 - 123 1.59 20
Trichloroethene 0.125 0.120 0.121 96.0 96.8 76.0 - 126 0.830 20
Trichlorofluoromethane 0.125 0.115 0.119 92.0 95.2 61.0 - 142 3.42 20
1,2,3-Trichloropropane 0.125 0.122 0.122 97.6 97.6 67.0 - 129 0.000 20
1,2,4-Trimethylbenzene 0.125 0.120 0.123 96.0 98.4 70.0 - 126 2.47 20
1,2,3-Trimethylbenzene 0.125 0.117 0.119 93.6 95.2 74.0 - 124 1.69 20
1,3,5-Trimethylbenzene 0.125 0.121 0.127 96.8 102 73.0 - 127 4.84 20
Vinyl chloride 0.125 0.116 0.117 92.8 93.6 63.0 - 134 0.858 20
Xylenes, Total 0.375 0.375 0.377 100 101 72.0 - 127 0.532 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098753-1
RECOVERY _______________
L1757957-09,10,11,12
LCS Sample / File ID:R4098753-1 / 0725_03LCS SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2329510
Instrument ID:VOCMS56 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
Acetone 0.625 0.593 94.9 10.0 - 160
Acrylonitrile 0.625 0.856 137 45.0 - 153
Benzene 0.125 0.114 91.2 70.0 - 123
Bromobenzene 0.125 0.121 96.8 73.0 - 121
Bromodichloromethane 0.125 0.132 106 73.0 - 121
Bromoform 0.125 0.145 116 64.0 - 132
Bromomethane 0.125 0.120 96.0 56.0 - 147
n-Butylbenzene 0.125 0.0975 78.0 68.0 - 135
sec-Butylbenzene 0.125 0.101 80.8 74.0 - 130
tert-Butylbenzene 0.125 0.108 86.4 75.0 - 127
Carbon tetrachloride 0.125 0.128 102 66.0 - 128
Chlorobenzene 0.125 0.115 92.0 76.0 - 128
Chlorodibromomethane 0.125 0.121 96.8 74.0 - 127
Chloroethane 0.125 0.145 116 61.0 - 134
Chloroform 0.125 0.112 89.6 72.0 - 123
Chloromethane 0.125 0.0919 73.5 51.0 - 138
2-Chlorotoluene 0.125 0.112 89.6 75.0 - 124
4-Chlorotoluene 0.125 0.108 86.4 75.0 - 124
1,2-Dibromo-3-Chloropropane 0.125 0.134 107 59.0 - 130
1,2-Dibromoethane 0.125 0.120 96.0 74.0 - 128
Dibromomethane 0.125 0.130 104 75.0 - 122
1,2-Dichlorobenzene 0.125 0.113 90.4 76.0 - 124
1,3-Dichlorobenzene 0.125 0.115 92.0 76.0 - 125
1,4-Dichlorobenzene 0.125 0.114 91.2 77.0 - 121
Dichlorodifluoromethane 0.125 0.102 81.6 43.0 - 156
1,1-Dichloroethane 0.125 0.120 96.0 70.0 - 127
1,2-Dichloroethane 0.125 0.120 96.0 65.0 - 131
1,1-Dichloroethene 0.125 0.114 91.2 65.0 - 131
cis-1,2-Dichloroethene 0.125 0.120 96.0 73.0 - 125
trans-1,2-Dichloroethene 0.125 0.123 98.4 71.0 - 125
1,2-Dichloropropane 0.125 0.124 99.2 74.0 - 125
1,1-Dichloropropene 0.125 0.117 93.6 73.0 - 125
1,3-Dichloropropane 0.125 0.120 96.0 80.0 - 125
cis-1,3-Dichloropropene 0.125 0.130 104 76.0 - 127
trans-1,3-Dichloropropene 0.125 0.125 100 73.0 - 127
2,2-Dichloropropane 0.125 0.117 93.6 59.0 - 135
Di-isopropyl ether 0.125 0.151 121 60.0 - 136
Ethylbenzene 0.125 0.115 92.0 74.0 - 126
Hexachloro-1,3-butadiene 0.125 0.110 88.0 57.0 - 150
Isopropylbenzene 0.125 0.117 93.6 72.0 - 127
p-Isopropyltoluene 0.125 0.106 84.8 72.0 - 133
2-Butanone (MEK)0.625 0.861 138 30.0 - 160
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098753-1
RECOVERY _______________
L1757957-09,10,11,12
LCS Sample / File ID:R4098753-1 / 0725_03LCS SDG:L1757957
LCSD Sample / File ID:_______________Analytical Batch:WG2329510
Instrument ID:VOCMS56 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
Methylene Chloride 0.125 0.107 85.6 68.0 - 123
4-Methyl-2-pentanone (MIBK)0.625 0.756 121 56.0 - 143
Methyl tert-butyl ether 0.125 0.136 109 66.0 - 132
Naphthalene 0.125 0.104 83.2 59.0 - 130
n-Propylbenzene 0.125 0.116 92.8 74.0 - 126
Styrene 0.125 0.112 89.6 72.0 - 127
1,1,1,2-Tetrachloroethane 0.125 0.134 107 74.0 - 129
1,1,2,2-Tetrachloroethane 0.125 0.125 100 68.0 - 128
1,1,2-Trichlorotrifluoroethane 0.125 0.117 93.6 61.0 - 139
Tetrachloroethene 0.125 0.126 101 70.0 - 136
Toluene 0.125 0.114 91.2 75.0 - 121
1,2,3-Trichlorobenzene 0.125 0.120 96.0 59.0 - 139
1,2,4-Trichlorobenzene 0.125 0.117 93.6 62.0 - 137
1,1,1-Trichloroethane 0.125 0.138 110 69.0 - 126
1,1,2-Trichloroethane 0.125 0.125 100 78.0 - 123
Trichloroethene 0.125 0.126 101 76.0 - 126
Trichlorofluoromethane 0.125 0.115 92.0 61.0 - 142
1,2,3-Trichloropropane 0.125 0.111 88.8 67.0 - 129
1,2,4-Trimethylbenzene 0.125 0.112 89.6 70.0 - 126
1,2,3-Trimethylbenzene 0.125 0.105 84.0 74.0 - 124
1,3,5-Trimethylbenzene 0.125 0.112 89.6 73.0 - 127
Vinyl chloride 0.125 0.125 100 63.0 - 134
Xylenes, Total 0.375 0.343 91.5 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4097932-3
Lab Sample ID:R4097932-3 SDG:L1757957
Lab File ID:0721_32 Preparation Date/Time:07/21/24 23:25
Instrument ID:VOCMS21 Analysis Date/Time:07/21/24 23:25
Analytical Batch:WG2327390 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4097932-1 VOCMS21 0721_28LCS 07/21/24 21:51
LCSD R4097932-2 VOCMS21 0721_29 07/21/24 22:14
TRIP BLANK L1757957-17 VOCMS21 0721_33 07/22/24 00:33
EB-1-071624 L1757957-16 VOCMS21 0721_35 07/22/24 01:20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4098226-2
Lab Sample ID:R4098226-2 SDG:L1757957
Lab File ID:0724A_07 Preparation Date/Time:07/24/24 21:48
Instrument ID:VOCMS56 Analysis Date/Time:07/24/24 21:48
Analytical Batch:WG2329566 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098226-1 VOCMS56 0724A_03LCS 07/24/24 20:32
S-1 (0-6)L1757957-13 VOCMS56 0724A_16 07/25/24 00:48
S-1 (6-12)L1757957-14 VOCMS56 0724A_17 07/25/24 01:07
SS-1 (6-12)L1757957-15 VOCMS56 0724A_18 07/25/24 01:26
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4098753-2
Lab Sample ID:R4098753-2 SDG:L1757957
Lab File ID:0725_07 Preparation Date/Time:07/25/24 08:44
Instrument ID:VOCMS56 Analysis Date/Time:07/25/24 08:44
Analytical Batch:WG2329510 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098753-1 VOCMS56 0725_03LCS 07/25/24 07:27
S-2 (0-6)L1757957-12 VOCMS56 0725_24 07/25/24 14:34
S-5 (0-6)L1757957-09 VOCMS56 0725_28 07/25/24 15:58
S-4 (0-6)L1757957-10 VOCMS56 0725_29 07/25/24 16:17
S-31 (0-6)L1757957-11 VOCMS56 0725_30 07/25/24 16:36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4098455-3
Lab Sample ID:R4098455-3 SDG:L1757957
Lab File ID:0725_34 Preparation Date/Time:07/25/24 10:05
Instrument ID:VOCMS58 Analysis Date/Time:07/25/24 10:05
Analytical Batch:WG2329486 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098455-1 VOCMS58 0725_29LCS 07/25/24 08:30
LCSD R4098455-2 VOCMS58 0725_30 07/25/24 08:49
S-3 (6-12)L1757957-02 VOCMS58 0725_41 07/25/24 12:21
S-30 (6-12)L1757957-03 VOCMS58 0725_42 07/25/24 12:40
S-8 (0-6)L1757957-05 VOCMS58 0725_43 07/25/24 12:59
S-7 (6-12)L1757957-07 VOCMS58 0725_44 07/25/24 13:18
S-3 (0-6)L1757957-01 VOCMS58 0725_53 07/25/24 15:51
S-9 (0-6)L1757957-04 VOCMS58 0725_54 07/25/24 16:10
S-7 (0-6)L1757957-06 VOCMS58 0725_55 07/25/24 16:29
S-6 (0-6)L1757957-08 VOCMS58 0725_56 07/25/24 16:48
MS R4098455-4 VOCMS58 0725_59 07/25/24 17:45
MSD R4098455-5 VOCMS58 0725_60 07/25/24 18:04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0710_01 SDG:L1757957
Instrument ID:VOCMS21 Analytical Method:8260B
Analysis Date/Time:07/10/24 10:50
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 112
96 95 5 9 7
173 174 0 2 1
174 95 50 200 90
175 174 5 9 8
176 174 95 105 99
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.5 0.5 0710_04 07/10/24 11:59
STD-1 1 0710_05 07/10/24 12:23
STD-2 2 0710_06 07/10/24 12:46
STD-5.0 5.0 0710_07 07/10/24 13:10
STD-25 25 0710_08 07/10/24 13:33
STD-75 75 0710_09 07/10/24 13:57
STD-100 100 0710_10 07/10/24 14:20
STD-200 200 0710_11 07/10/24 14:44
SSCV VOCMS210710240710_15740563 0710_15 07/10/24 16:17
SSCV VOCMS210710240710_17740563 0710_17 07/10/24 17:04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0710_01A SDG:L1757957
Instrument ID:VOCMS21 Analytical Method:8260B
Analysis Date/Time:07/10/24 10:50
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 112
96 95 5 9 7
173 174 0 2 1
174 95 50 200 90
175 174 5 9 8
176 174 95 105 99
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-1A 1A 0710_20A 07/10/24 18:15
STD-5A 5A 0710_21A 07/10/24 18:38
STD-10A 10A 0710_22A 07/10/24 19:02
STD-15A 15A 0710_23A 07/10/24 19:25
STD-20A 20A 0710_24A 07/10/24 19:49
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0721_27T SDG:L1757957
Instrument ID:VOCMS21 Analytical Method:8260B
Analysis Date/Time:07/21/24 21:27
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 127
96 95 5 9 7
173 174 0 2 1
174 95 50 200 79
175 174 5 9 7
176 174 95 105 100
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS210721240721_28740563 0721_28 07/21/24 21:51
LCS R4097932-1 0721_28LCS 07/21/24 21:51
LCSD R4097932-2 0721_29 07/21/24 22:14
BLANK R4097932-3 0721_32 07/21/24 23:25
TRIP BLANK L1757957-17 0721_33 07/22/24 00:33
EB-1-071624 L1757957-16 0721_35 07/22/24 01:20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0708_08 SDG:L1757957
Instrument ID:VOCMS56 Analytical Method:8260B
Analysis Date/Time:07/08/24 19:11
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 134
96 95 5 9 7
173 174 0 2 0
174 95 50 200 74
175 174 5 9 8
176 174 95 105 97
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.04 0.04 0708_09 07/08/24 19:30
STD-0.1 0.1 0708_10 07/08/24 19:49
STD-0.2 0.2 0708_11 07/08/24 20:08
STD-0.5 0.5 0708_12 07/08/24 20:27
STD-1 1 0708_13 07/08/24 20:46
STD-2 2 0708_14 07/08/24 21:05
STD-5.0 5.0 0708_15 07/08/24 21:24
STD-25 25 0708_16 07/08/24 21:43
STD-75 75 0708_17 07/08/24 22:02
STD-100 100 0708_18 07/08/24 22:21
SSCV VOCMS560708240708_22737277 0708_22 07/08/24 23:37
SSCV VOCMS560708240708_23737277 0708_23 07/08/24 23:56
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0724A_01T SDG:L1757957
Instrument ID:VOCMS56 Analytical Method:8260B
Analysis Date/Time:07/24/24 19:54
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 116
96 95 5 9 7
173 174 0 2 1
174 95 50 200 86
175 174 5 9 8
176 174 95 105 98
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS56072424A0724A_03737277 0724A_03 07/24/24 20:32
LCS R4098226-1 0724A_03LCS 07/24/24 20:32
BLANK R4098226-2 0724A_07 07/24/24 21:48
S-1 (0-6)L1757957-13 0724A_16 07/25/24 00:48
S-1 (6-12)L1757957-14 0724A_17 07/25/24 01:07
SS-1 (6-12)L1757957-15 0724A_18 07/25/24 01:26
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0725_01T SDG:L1757957
Instrument ID:VOCMS56 Analytical Method:8260B
Analysis Date/Time:07/25/24 06:49
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 124
96 95 5 9 7
173 174 0 2 1
174 95 50 200 81
175 174 5 9 7
176 174 95 105 98
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS560725240725_03737277 0725_03 07/25/24 07:27
LCS R4098753-1 0725_03LCS 07/25/24 07:27
BLANK R4098753-2 0725_07 07/25/24 08:44
S-2 (0-6)L1757957-12 0725_24 07/25/24 14:34
S-5 (0-6)L1757957-09 0725_28 07/25/24 15:58
S-4 (0-6)L1757957-10 0725_29 07/25/24 16:17
S-31 (0-6)L1757957-11 0725_30 07/25/24 16:36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 395 of 530
5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0718_05 SDG:L1757957
Instrument ID:VOCMS58 Analytical Method:8260B
Analysis Date/Time:07/19/24 03:22
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 114
96 95 5 9 6
173 174 0 2 1
174 95 50 200 87
175 174 5 9 7
176 174 95 105 97
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.04 0.04 0718_07 07/19/24 04:01
STD-0.1 0.1 0718_08 07/19/24 04:20
STD-0.2 0.2 0718_09 07/19/24 04:39
STD-0.5 0.5 0718_10 07/19/24 04:58
STD-1 1 0718_11 07/19/24 05:17
STD-2 2 0718_12 07/19/24 05:36
STD-5.0 5.0 0718_13 07/19/24 05:55
STD-25 25 0718_14 07/19/24 06:14
STD-75 75 0718_15 07/19/24 06:33
STD-100 100 0718_16 07/19/24 06:52
SSCV VOCMS580718240718_21740383 0718_21 07/19/24 08:27
SSCV VOCMS580718240718_23740383 0718_23 07/19/24 09:05
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 396 of 530
5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0725_28T SDG:L1757957
Instrument ID:VOCMS58 Analytical Method:8260B
Analysis Date/Time:07/25/24 08:11
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 115
96 95 5 9 7
173 174 0 2 1
174 95 50 200 87
175 174 5 9 7
176 174 95 105 96
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
CCV VOCMS580725240725_29740383 0725_29 07/25/24 08:30
LCS R4098455-1 0725_29LCS 07/25/24 08:30
LCSD R4098455-2 0725_30 07/25/24 08:49
BLANK R4098455-3 0725_34 07/25/24 10:05
S-3 (6-12)L1757957-02 0725_41 07/25/24 12:21
S-30 (6-12)L1757957-03 0725_42 07/25/24 12:40
S-8 (0-6)L1757957-05 0725_43 07/25/24 12:59
S-7 (6-12)L1757957-07 0725_44 07/25/24 13:18
OS L1757957-01 0725_53 07/25/24 15:51
S-3 (0-6)L1757957-01 0725_53 07/25/24 15:51
S-9 (0-6)L1757957-04 0725_54 07/25/24 16:10
S-7 (0-6)L1757957-06 0725_55 07/25/24 16:29
S-6 (0-6)L1757957-08 0725_56 07/25/24 16:48
MS R4098455-4 0725_59 07/25/24 17:45
MSD R4098455-5 0725_60 07/25/24 18:04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 397 of 530
8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS21 Calibration Start Date:07/10/24 11:59
Std File: 0721_28 Calibration End Date:07/10/24 19:49
Std Analysis Date:07/21/24 21:51
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 293539 7.81 309541 6.10 512048 4.17
UPPER LIMIT 587078 619082 1024096
LOWER LIMIT 146770 154771 256024
LCS R4097932-1
WG2327390 1x
0721_28LC
S 293539 7.81 309541 6.10 512048 4.17
LCSD R4097932-2
WG2327390 1x 0721_29 288198 7.81 305975 6.10 497208 4.17
BLANK R4097932-3
WG2327390 1x 0721_32 274531 7.81 291810 6.10 483897 4.17
L1757957-17 WG2327390
1x 0721_33 269887 7.81 283379 6.10 473602 4.17
L1757957-16 WG2327390
1x 0721_35 268254 7.81 285405 6.10 468015 4.17
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 398 of 530
8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56 Calibration Start Date:07/08/24 19:30
Std File: 0724A_03 Calibration End Date:07/08/24 22:21
Std Analysis Date:07/24/24 20:32
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 273226 8.26 358636.20 6.57 813101.10 4.63
UPPER LIMIT 546452 717272 1626202
LOWER LIMIT 136613 179318 406551
LCS R4098226-1
WG2329566 1x
0724A_03L
CS 273226 8.26 358636.20 6.57 813101.10 4.63
BLANK R4098226-2
WG2329566 1x 0724A_07 333113.10 8.26 345374.80 6.57 805376.20 4.62
L1757957-13 WG2329566
1.22x 0724A_16 276477.60 8.26 373888.40 6.57 906222.80 4.62
L1757957-14 WG2329566
1.19x 0724A_17 312312.70 8.26 401609.70 6.57 957972 4.62
L1757957-15 WG2329566
1x 0724A_18 328217 8.26 413500.60 6.57 970643.70 4.62
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 399 of 530
8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56 Calibration Start Date:07/08/24 19:30
Std File: 0725_03 Calibration End Date:07/08/24 22:21
Std Analysis Date:07/25/24 07:27
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 315089.10 8.26 433201 6.57 999742.60 4.63
UPPER LIMIT 630178 866402 1999485
LOWER LIMIT 157545 216601 499871
LCS R4098753-1
WG2329510 1x
0725_03LC
S 315089.10 8.26 433201 6.57 999742.60 4.63
BLANK R4098753-2
WG2329510 1x 0725_07 310067 8.26 387219.30 6.57 885068.40 4.62
L1757957-12 WG2329510
1.06x 0725_24 369924.20 8.26 497186.90 6.57 1104184 4.62
L1757957-09 WG2329510
1x 0725_28 354727 8.26 465886.80 6.57 1071203 4.62
L1757957-10 WG2329510
1.14x 0725_29 345651.50 8.26 490329.20 6.57 1126378 4.62
L1757957-11 WG2329510
1.21x 0725_30 342913.60 8.26 481760.20 6.57 1097412 4.62
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 400 of 530
8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS58 Calibration Start Date:07/19/24 04:01
Std File: 0725_29 Calibration End Date:07/19/24 06:52
Std Analysis Date:07/25/24 08:30
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 431674.40 8.27 454689.50 6.57 959251.40 4.62
UPPER LIMIT 815277 885169 1895017
LOWER LIMIT 203819 221292 473754
LCS R4098455-1
WG2329486 1x
0725_29LC
S 431674.40 8.27 454689.50 6.57 959251.40 4.62
LCSD R4098455-2
WG2329486 1x 0725_30 431536.30 8.27 458161.40 6.57 969672.10 4.62
BLANK R4098455-3
WG2329486 1x 0725_34 398258.20 8.27 438623.20 6.57 960059.80 4.61
L1757957-02 WG2329486
1.05x 0725_41 426768.90 8.27 457067.10 6.57 985567.70 4.61
L1757957-03 WG2329486
1.1x 0725_42 419553.80 8.27 464713.90 6.57 996723.20 4.61
L1757957-05 WG2329486
1x 0725_43 421252 8.27 462601.90 6.57 999590.90 4.61
L1757957-07 WG2329486
1.21x 0725_44 427576.40 8.27 465195.10 6.57 1011202 4.61
L1757957-01 WG2329486
1.1x 0725_53 445282.60 8.27 464959 6.57 1015042 4.61
OS L1757957-01
WG2329486 1.1x 0725_53 445282.60 8.27 464959 6.57 1015042 4.61
L1757957-04 WG2329486
1.03x 0725_54 443148.30 8.27 468404.20 6.57 1019654 4.61
L1757957-06 WG2329486
1.37x 0725_55 451673.20 8.27 486461.90 6.57 1046794 4.61
L1757957-08 WG2329486
1x 0725_56 426550.50 8.27 472005.20 6.57 1025721 4.61
MS R4098455-4
WG2329486 1.1x 0725_59 451148.20 8.27 477252.70 6.57 1001613 4.61
MSD R4098455-5
WG2329486 1.1x 0725_60 466411.20 8.27 497444.80 6.57 1056976 4.61
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 401 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:0725_53 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 15:51
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U J3 0.0412 0.0565
Acrylonitrile 107-13-1 0 U 0.00408 0.0142
Benzene 71-43-2 4.38 0.00169 0.000528 0.00113
Bromobenzene 108-86-1 0 U 0.00102 0.0142
Bromodichloromethane 75-27-4 0 U 0.000819 0.00282
Bromoform 75-25-2 0 U 0.00132 0.0282
Bromomethane 74-83-9 2.27 U 0.00223 0.0142
n-Butylbenzene 104-51-8 0 U 0.00594 0.0142
sec-Butylbenzene 135-98-8 8.03 U 0.00326 0.0142
tert-Butylbenzene 98-06-6 7.94 U 0.00221 0.00565
Carbon tetrachloride 56-23-5 4.14 U 0.00101 0.00565
Chlorobenzene 108-90-7 0 U 0.000237 0.00282
Chlorodibromomethane 124-48-1 0 U 0.000691 0.00282
Chloroethane 75-00-3 2.38 U 0.00192 0.00565
Chloroform 67-66-3 0 U 0.00116 0.00282
Chloromethane 74-87-3 0 U J3 0.00492 0.0142
2-Chlorotoluene 95-49-8 0 U 0.000978 0.00282
4-Chlorotoluene 106-43-4 7.80 U 0.000508 0.00565
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00441 0.0282
1,2-Dibromoethane 106-93-4 0 U 0.000732 0.00282
Dibromomethane 74-95-3 0 U 0.000847 0.00565
1,2-Dichlorobenzene 95-50-1 0 U 0.000481 0.00565
1,3-Dichlorobenzene 541-73-1 8.28 U 0.000678 0.00565
1,4-Dichlorobenzene 106-46-7 8.28 U 0.000791 0.00565
Dichlorodifluoromethane 75-71-8 0 U 0.00182 0.00565
1,1-Dichloroethane 75-34-3 0 U 0.000555 0.00282
1,2-Dichloroethane 107-06-2 4.49 U 0.000733 0.00282
1,1-Dichloroethene 75-35-4 0 U 0.000685 0.00282
cis-1,2-Dichloroethene 156-59-2 0 U 0.000829 0.00282
trans-1,2-Dichloroethene 156-60-5 0 U 0.00117 0.00565
1,2-Dichloropropane 78-87-5 0 U 0.00160 0.00565
1,1-Dichloropropene 563-58-6 0 U 0.000914 0.00282
1,3-Dichloropropane 142-28-9 0 U 0.000566 0.00565
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000856 0.00282
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00128 0.00565
2,2-Dichloropropane 594-20-7 0 U 0.00156 0.00282
Di-isopropyl ether 108-20-3 3.44 U 0.000463 0.00113
Ethylbenzene 100-41-4 6.58 U 0.000833 0.00282
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00678 0.0282
Isopropylbenzene 98-82-8 7.20 U 0.000481 0.00282
p-Isopropyltoluene 99-87-6 8.13 U 0.00289 0.00565
2-Butanone (MEK)78-93-3 4.20 U 0.0718 0.113
Methylene Chloride 75-09-2 3.16 0.00797 J 0.00750 0.0282
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:0725_53 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 15:51
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.77 U 0.00258 0.0282
Methyl tert-butyl ether 1634-04-4 3.28 U 0.000395 0.00113
Naphthalene 91-20-3 10.09 0.0113 J 0.00552 0.0142
n-Propylbenzene 103-65-1 7.50 U 0.00108 0.00565
Styrene 100-42-5 7.02 U 0.000259 0.0142
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00107 0.00282
1,1,2,2-Tetrachloroethane 79-34-5 7.58 U 0.000786 0.00282
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000851 0.00282
Tetrachloroethene 127-18-4 0 U 0.00101 0.00282
Toluene 108-88-3 5.58 0.00316 J 0.00147 0.00565
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00828 0.0142
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00497 0.0142
1,1,1-Trichloroethane 71-55-6 0 U 0.00105 0.00282
1,1,2-Trichloroethane 79-00-5 0 U 0.000675 0.00282
Trichloroethene 79-01-6 0 U 0.000659 0.00113
Trichlorofluoromethane 75-69-4 2.43 U 0.000935 0.00282
1,2,3-Trichloropropane 96-18-4 0 U 0.00183 0.0142
1,2,4-Trimethylbenzene 95-63-6 7.94 0.00426 J 0.00179 0.00565
1,2,3-Trimethylbenzene 526-73-8 8.28 0.00319 J 0.00179 0.00565
1,3,5-Trimethylbenzene 108-67-8 7.64 U 0.00226 0.00565
Vinyl chloride 75-01-4 0 U 0.00131 0.00282
Xylenes, Total 1330-20-7 6.98 0.00886 0.000994 0.00734
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:0725_41 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 10:00
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 12:21
Dilution Factor:1.05 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.52 g
Total Solids (%):92.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.15 U 0.0448 0.0614
Acrylonitrile 107-13-1 3.64 U 0.00444 0.0153
Benzene 71-43-2 4.38 0.00329 0.000573 0.00123
Bromobenzene 108-86-1 0 U 0.00111 0.0153
Bromodichloromethane 75-27-4 4.98 U 0.000891 0.00308
Bromoform 75-25-2 7.06 U 0.00144 0.0308
Bromomethane 74-83-9 2.25 U 0.00242 0.0153
n-Butylbenzene 104-51-8 8.46 U 0.00645 0.0153
sec-Butylbenzene 135-98-8 8.03 U 0.00353 0.0153
tert-Butylbenzene 98-06-6 7.94 U 0.00240 0.00614
Carbon tetrachloride 56-23-5 0 U 0.00110 0.00614
Chlorobenzene 108-90-7 0 U 0.000259 0.00308
Chlorodibromomethane 124-48-1 0 U 0.000753 0.00308
Chloroethane 75-00-3 2.40 U 0.00209 0.00614
Chloroform 67-66-3 4.03 U 0.00126 0.00308
Chloromethane 74-87-3 1.86 U J3 0.00535 0.0153
2-Chlorotoluene 95-49-8 0 U 0.00106 0.00308
4-Chlorotoluene 106-43-4 7.81 U 0.000554 0.00614
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00479 0.0308
1,2-Dibromoethane 106-93-4 0 U 0.000796 0.00308
Dibromomethane 74-95-3 0 U 0.000922 0.00614
1,2-Dichlorobenzene 95-50-1 8.72 U 0.000522 0.00614
1,3-Dichlorobenzene 541-73-1 8.27 U 0.000737 0.00614
1,4-Dichlorobenzene 106-46-7 8.27 U 0.000860 0.00614
Dichlorodifluoromethane 75-71-8 0 U 0.00198 0.00614
1,1-Dichloroethane 75-34-3 0 U 0.000604 0.00308
1,2-Dichloroethane 107-06-2 4.51 U 0.000797 0.00308
1,1-Dichloroethene 75-35-4 0 U 0.000744 0.00308
cis-1,2-Dichloroethene 156-59-2 0 U 0.000902 0.00308
trans-1,2-Dichloroethene 156-60-5 0 U 0.00128 0.00614
1,2-Dichloropropane 78-87-5 0 U 0.00174 0.00614
1,1-Dichloropropene 563-58-6 0 U 0.000994 0.00308
1,3-Dichloropropane 142-28-9 0 U 0.000616 0.00614
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000930 0.00308
trans-1,3-Dichloropropene 10061-02-6 5.89 U 0.00140 0.00614
2,2-Dichloropropane 594-20-7 3.92 U 0.00170 0.00308
Di-isopropyl ether 108-20-3 0 U 0.000504 0.00123
Ethylbenzene 100-41-4 6.58 0.00786 0.000906 0.00308
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00737 0.0308
Isopropylbenzene 98-82-8 7.20 0.00427 0.000522 0.00308
p-Isopropyltoluene 99-87-6 8.13 0.0367 0.00314 0.00614
2-Butanone (MEK)78-93-3 0 U 0.0781 0.123
Methylene Chloride 75-09-2 3.16 U 0.00816 0.0308
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:0725_41 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 10:00
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 12:21
Dilution Factor:1.05 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.52 g
Total Solids (%):92.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.77 0.0224 J 0.00280 0.0308
Methyl tert-butyl ether 1634-04-4 0 U 0.000431 0.00123
Naphthalene 91-20-3 10.09 0.0302 0.00599 0.0153
n-Propylbenzene 103-65-1 7.50 0.00504 J 0.00117 0.00614
Styrene 100-42-5 6.99 U 0.000281 0.0153
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00116 0.00308
1,1,2,2-Tetrachloroethane 79-34-5 7.58 U 0.000854 0.00308
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000927 0.00308
Tetrachloroethene 127-18-4 5.83 U 0.00110 0.00308
Toluene 108-88-3 5.58 0.0390 0.00159 0.00614
1,2,3-Trichlorobenzene 87-61-6 10.32 U 0.00901 0.0153
1,2,4-Trichlorobenzene 120-82-1 9.86 U 0.00541 0.0153
1,1,1-Trichloroethane 71-55-6 0 U 0.00113 0.00308
1,1,2-Trichloroethane 79-00-5 5.86 U 0.000734 0.00308
Trichloroethene 79-01-6 0 U 0.000717 0.00123
Trichlorofluoromethane 75-69-4 0 U 0.00102 0.00308
1,2,3-Trichloropropane 96-18-4 7.73 U 0.00199 0.0153
1,2,4-Trimethylbenzene 95-63-6 7.94 0.0536 0.00194 0.00614
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0344 0.00194 0.00614
1,3,5-Trimethylbenzene 108-67-8 7.64 0.0233 0.00246 0.00614
Vinyl chloride 75-01-4 0 U 0.00143 0.00308
Xylenes, Total 1330-20-7 6.98 0.0836 0.00108 0.00799
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 405 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:0725_42 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 13:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 12:40
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.08 g
Total Solids (%):92.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U 0.0461 0.0633
Acrylonitrile 107-13-1 3.65 U 0.00457 0.0159
Benzene 71-43-2 4.39 0.00235 0.000591 0.00127
Bromobenzene 108-86-1 0 U 0.00114 0.0159
Bromodichloromethane 75-27-4 4.98 U 0.000917 0.00316
Bromoform 75-25-2 0 U 0.00148 0.0316
Bromomethane 74-83-9 2.32 U 0.00250 0.0159
n-Butylbenzene 104-51-8 8.43 U 0.00665 0.0159
sec-Butylbenzene 135-98-8 8.03 U 0.00365 0.0159
tert-Butylbenzene 98-06-6 7.95 U 0.00247 0.00633
Carbon tetrachloride 56-23-5 0 U 0.00114 0.00633
Chlorobenzene 108-90-7 0 U 0.000266 0.00316
Chlorodibromomethane 124-48-1 0 U 0.000774 0.00316
Chloroethane 75-00-3 2.41 U 0.00215 0.00633
Chloroform 67-66-3 4.04 U 0.00130 0.00316
Chloromethane 74-87-3 0 U J3 0.00551 0.0159
2-Chlorotoluene 95-49-8 0 U 0.00109 0.00316
4-Chlorotoluene 106-43-4 7.81 U 0.000569 0.00633
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00493 0.0316
1,2-Dibromoethane 106-93-4 0 U 0.000820 0.00316
Dibromomethane 74-95-3 0 U 0.000949 0.00633
1,2-Dichlorobenzene 95-50-1 8.71 U 0.000538 0.00633
1,3-Dichlorobenzene 541-73-1 0 U 0.000759 0.00633
1,4-Dichlorobenzene 106-46-7 0 U 0.000886 0.00633
Dichlorodifluoromethane 75-71-8 0 U 0.00204 0.00633
1,1-Dichloroethane 75-34-3 0 U 0.000621 0.00316
1,2-Dichloroethane 107-06-2 4.49 U 0.000821 0.00316
1,1-Dichloroethene 75-35-4 0 U 0.000767 0.00316
cis-1,2-Dichloroethene 156-59-2 3.97 U 0.000928 0.00316
trans-1,2-Dichloroethene 156-60-5 0 U 0.00131 0.00633
1,2-Dichloropropane 78-87-5 0 U 0.00179 0.00633
1,1-Dichloropropene 563-58-6 4.23 U 0.00102 0.00316
1,3-Dichloropropane 142-28-9 0 U 0.000634 0.00633
cis-1,3-Dichloropropene 10061-01-5 5.46 U 0.000958 0.00316
trans-1,3-Dichloropropene 10061-02-6 5.83 U 0.00144 0.00633
2,2-Dichloropropane 594-20-7 3.99 U 0.00175 0.00316
Di-isopropyl ether 108-20-3 0 U 0.000519 0.00127
Ethylbenzene 100-41-4 6.58 0.00332 0.000933 0.00316
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00759 0.0316
Isopropylbenzene 98-82-8 7.20 0.00186 J 0.000538 0.00316
p-Isopropyltoluene 99-87-6 8.13 0.0111 0.00323 0.00633
2-Butanone (MEK)78-93-3 4.19 U 0.0804 0.127
Methylene Chloride 75-09-2 3.17 U 0.00840 0.0316
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:0725_42 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 13:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 12:40
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.08 g
Total Solids (%):92.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.0114 J 0.00289 0.0316
Methyl tert-butyl ether 1634-04-4 3.34 U 0.000443 0.00127
Naphthalene 91-20-3 10.09 0.0183 0.00618 0.0159
n-Propylbenzene 103-65-1 7.50 0.00199 J 0.00121 0.00633
Styrene 100-42-5 6.99 U 0.000290 0.0159
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00120 0.00316
1,1,2,2-Tetrachloroethane 79-34-5 7.54 U 0.000880 0.00316
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000953 0.00316
Tetrachloroethene 127-18-4 5.84 U 0.00113 0.00316
Toluene 108-88-3 5.58 0.0153 0.00164 0.00633
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00927 0.0159
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00557 0.0159
1,1,1-Trichloroethane 71-55-6 0 U 0.00117 0.00316
1,1,2-Trichloroethane 79-00-5 5.96 U 0.000756 0.00316
Trichloroethene 79-01-6 0 U 0.000738 0.00127
Trichlorofluoromethane 75-69-4 0 U 0.00105 0.00316
1,2,3-Trichloropropane 96-18-4 0 U 0.00205 0.0159
1,2,4-Trimethylbenzene 95-63-6 7.94 0.0213 0.00200 0.00633
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0173 0.00200 0.00633
1,3,5-Trimethylbenzene 108-67-8 7.64 0.0104 0.00253 0.00633
Vinyl chloride 75-01-4 0 U 0.00147 0.00316
Xylenes, Total 1330-20-7 6.99 0.0460 0.00111 0.00822
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:0725_54 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 10:34
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 16:10
Dilution Factor:1.03 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.71 g
Total Solids (%):97.8 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U 0.0393 0.0538
Acrylonitrile 107-13-1 0 U 0.00389 0.0135
Benzene 71-43-2 4.39 0.00169 0.000502 0.00108
Bromobenzene 108-86-1 0 U 0.000968 0.0135
Bromodichloromethane 75-27-4 0 U 0.000780 0.00269
Bromoform 75-25-2 0 U 0.00126 0.0269
Bromomethane 74-83-9 2.30 U 0.00212 0.0135
n-Butylbenzene 104-51-8 8.46 U 0.00565 0.0135
sec-Butylbenzene 135-98-8 8.03 0.00420 J 0.00310 0.0135
tert-Butylbenzene 98-06-6 7.94 U 0.00210 0.00538
Carbon tetrachloride 56-23-5 0 U 0.000966 0.00538
Chlorobenzene 108-90-7 0 U 0.000226 0.00269
Chlorodibromomethane 124-48-1 0 U 0.000658 0.00269
Chloroethane 75-00-3 2.37 U 0.00183 0.00538
Chloroform 67-66-3 0 U 0.00111 0.00269
Chloromethane 74-87-3 0 U J3 0.00468 0.0135
2-Chlorotoluene 95-49-8 0 U 0.000931 0.00269
4-Chlorotoluene 106-43-4 7.81 U 0.000485 0.00538
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00420 0.0269
1,2-Dibromoethane 106-93-4 0 U 0.000697 0.00269
Dibromomethane 74-95-3 0 U 0.000807 0.00538
1,2-Dichlorobenzene 95-50-1 0 U 0.000457 0.00538
1,3-Dichlorobenzene 541-73-1 0 U 0.000645 0.00538
1,4-Dichlorobenzene 106-46-7 0 U 0.000753 0.00538
Dichlorodifluoromethane 75-71-8 0 U 0.00173 0.00538
1,1-Dichloroethane 75-34-3 0 U 0.000529 0.00269
1,2-Dichloroethane 107-06-2 4.50 U 0.000698 0.00269
1,1-Dichloroethene 75-35-4 0 U 0.000652 0.00269
cis-1,2-Dichloroethene 156-59-2 3.97 U 0.000790 0.00269
trans-1,2-Dichloroethene 156-60-5 0 U 0.00112 0.00538
1,2-Dichloropropane 78-87-5 0 U 0.00152 0.00538
1,1-Dichloropropene 563-58-6 4.20 U 0.000870 0.00269
1,3-Dichloropropane 142-28-9 0 U 0.000539 0.00538
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000815 0.00269
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00122 0.00538
2,2-Dichloropropane 594-20-7 0 U 0.00148 0.00269
Di-isopropyl ether 108-20-3 3.44 U 0.000441 0.00108
Ethylbenzene 100-41-4 6.58 0.00312 0.000793 0.00269
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00645 0.0269
Isopropylbenzene 98-82-8 7.20 0.00199 J 0.000457 0.00269
p-Isopropyltoluene 99-87-6 8.10 0.0132 0.00275 0.00538
2-Butanone (MEK)78-93-3 4.20 U 0.0683 0.108
Methylene Chloride 75-09-2 3.18 0.00828 J 0.00714 0.0269
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 408 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:0725_54 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 10:34
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 16:10
Dilution Factor:1.03 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.71 g
Total Solids (%):97.8 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.00734 J 0.00245 0.0269
Methyl tert-butyl ether 1634-04-4 3.31 U 0.000377 0.00108
Naphthalene 91-20-3 10.09 0.0118 J 0.00525 0.0135
n-Propylbenzene 103-65-1 7.50 0.00328 J 0.00102 0.00538
Styrene 100-42-5 6.98 U 0.000246 0.0135
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00102 0.00269
1,1,2,2-Tetrachloroethane 79-34-5 7.56 U 0.000748 0.00269
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000812 0.00269
Tetrachloroethene 127-18-4 0 U 0.000964 0.00269
Toluene 108-88-3 5.58 0.0168 0.00140 0.00538
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00789 0.0135
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00473 0.0135
1,1,1-Trichloroethane 71-55-6 0 U 0.000993 0.00269
1,1,2-Trichloroethane 79-00-5 6 U 0.000642 0.00269
Trichloroethene 79-01-6 0 U 0.000629 0.00108
Trichlorofluoromethane 75-69-4 2.45 U 0.000890 0.00269
1,2,3-Trichloropropane 96-18-4 0 U 0.00174 0.0135
1,2,4-Trimethylbenzene 95-63-6 7.94 0.175 0.00170 0.00538
1,2,3-Trimethylbenzene 526-73-8 8.28 0.159 0.00170 0.00538
1,3,5-Trimethylbenzene 108-67-8 7.64 0.0402 0.00215 0.00538
Vinyl chloride 75-01-4 0 U 0.00124 0.00269
Xylenes, Total 1330-20-7 6.98 0.0530 0.000946 0.00700
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 409 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:0725_43 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 10:58
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 12:59
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.02 g
Total Solids (%):98.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U 0.0378 0.0518
Acrylonitrile 107-13-1 3.65 U 0.00374 0.0129
Benzene 71-43-2 4.39 0.00713 0.000484 0.00104
Bromobenzene 108-86-1 0 U 0.000932 0.0129
Bromodichloromethane 75-27-4 4.98 U 0.000751 0.00259
Bromoform 75-25-2 0 U 0.00121 0.0259
Bromomethane 74-83-9 2.37 U 0.00204 0.0129
n-Butylbenzene 104-51-8 8.46 U 0.00544 0.0129
sec-Butylbenzene 135-98-8 8.03 U 0.00298 0.0129
tert-Butylbenzene 98-06-6 7.94 U 0.00202 0.00518
Carbon tetrachloride 56-23-5 0 U 0.000930 0.00518
Chlorobenzene 108-90-7 0 U 0.000218 0.00259
Chlorodibromomethane 124-48-1 0 U 0.000634 0.00259
Chloroethane 75-00-3 2.38 U 0.00176 0.00518
Chloroform 67-66-3 4.04 U 0.00107 0.00259
Chloromethane 74-87-3 0 U J3 0.00451 0.0129
2-Chlorotoluene 95-49-8 0 U 0.000896 0.00259
4-Chlorotoluene 106-43-4 7.81 U 0.000466 0.00518
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00404 0.0259
1,2-Dibromoethane 106-93-4 0 U 0.000671 0.00259
Dibromomethane 74-95-3 0 U 0.000777 0.00518
1,2-Dichlorobenzene 95-50-1 8.71 U 0.000440 0.00518
1,3-Dichlorobenzene 541-73-1 8.28 U 0.000622 0.00518
1,4-Dichlorobenzene 106-46-7 8.28 U 0.000725 0.00518
Dichlorodifluoromethane 75-71-8 0 U 0.00167 0.00518
1,1-Dichloroethane 75-34-3 3.65 U 0.000509 0.00259
1,2-Dichloroethane 107-06-2 4.49 U 0.000672 0.00259
1,1-Dichloroethene 75-35-4 0 U 0.000628 0.00259
cis-1,2-Dichloroethene 156-59-2 3.98 U 0.000760 0.00259
trans-1,2-Dichloroethene 156-60-5 0 U 0.00108 0.00518
1,2-Dichloropropane 78-87-5 0 U 0.00147 0.00518
1,1-Dichloropropene 563-58-6 0 U 0.000838 0.00259
1,3-Dichloropropane 142-28-9 0 U 0.000519 0.00518
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000784 0.00259
trans-1,3-Dichloropropene 10061-02-6 5.81 U 0.00118 0.00518
2,2-Dichloropropane 594-20-7 3.92 U 0.00143 0.00259
Di-isopropyl ether 108-20-3 0 U 0.000425 0.00104
Ethylbenzene 100-41-4 6.58 0.00521 0.000763 0.00259
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00622 0.0259
Isopropylbenzene 98-82-8 7.20 0.00195 J 0.000440 0.00259
p-Isopropyltoluene 99-87-6 8.13 0.0100 0.00264 0.00518
2-Butanone (MEK)78-93-3 4.19 U 0.0658 0.104
Methylene Chloride 75-09-2 3.17 U 0.00688 0.0259
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:0725_43 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 10:58
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 12:59
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.02 g
Total Solids (%):98.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.0172 J 0.00236 0.0259
Methyl tert-butyl ether 1634-04-4 3.28 U 0.000363 0.00104
Naphthalene 91-20-3 10.09 0.0248 0.00506 0.0129
n-Propylbenzene 103-65-1 7.50 0.00215 J 0.000984 0.00518
Styrene 100-42-5 6.99 U 0.000237 0.0129
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000982 0.00259
1,1,2,2-Tetrachloroethane 79-34-5 7.54 U 0.000720 0.00259
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000781 0.00259
Tetrachloroethene 127-18-4 0 U 0.000928 0.00259
Toluene 108-88-3 5.58 0.0352 0.00135 0.00518
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00759 0.0129
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00456 0.0129
1,1,1-Trichloroethane 71-55-6 0 U 0.000956 0.00259
1,1,2-Trichloroethane 79-00-5 5.95 U 0.000618 0.00259
Trichloroethene 79-01-6 0 U 0.000605 0.00104
Trichlorofluoromethane 75-69-4 2.45 U 0.000857 0.00259
1,2,3-Trichloropropane 96-18-4 7.68 U 0.00168 0.0129
1,2,4-Trimethylbenzene 95-63-6 7.94 0.0310 0.00164 0.00518
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0223 0.00164 0.00518
1,3,5-Trimethylbenzene 108-67-8 7.64 0.00951 0.00207 0.00518
Vinyl chloride 75-01-4 0 U 0.00120 0.00259
Xylenes, Total 1330-20-7 6.98 0.0805 0.000912 0.00673
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:0725_55 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 11:20
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 16:29
Dilution Factor:1.37 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.32 g
Total Solids (%):94.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U 0.0555 0.0761
Acrylonitrile 107-13-1 3.66 U 0.00550 0.0190
Benzene 71-43-2 4.39 0.0398 0.000711 0.00152
Bromobenzene 108-86-1 0 U 0.00137 0.0190
Bromodichloromethane 75-27-4 4.98 U 0.00110 0.00381
Bromoform 75-25-2 7.06 U 0.00178 0.0381
Bromomethane 74-83-9 2.32 U 0.00300 0.0190
n-Butylbenzene 104-51-8 8.46 0.00830 J 0.00799 0.0190
sec-Butylbenzene 135-98-8 8.03 0.00480 J 0.00439 0.0190
tert-Butylbenzene 98-06-6 7.94 U 0.00297 0.00761
Carbon tetrachloride 56-23-5 0 U 0.00137 0.00761
Chlorobenzene 108-90-7 6.58 U 0.000320 0.00381
Chlorodibromomethane 124-48-1 0 U 0.000931 0.00381
Chloroethane 75-00-3 0 U 0.00259 0.00761
Chloroform 67-66-3 4.04 U 0.00157 0.00381
Chloromethane 74-87-3 1.95 U J3 0.00662 0.0190
2-Chlorotoluene 95-49-8 7.70 U 0.00132 0.00381
4-Chlorotoluene 106-43-4 7.81 U 0.000685 0.00761
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00593 0.0381
1,2-Dibromoethane 106-93-4 0 U 0.000986 0.00381
Dibromomethane 74-95-3 0 U 0.00114 0.00761
1,2-Dichlorobenzene 95-50-1 0 U 0.000646 0.00761
1,3-Dichlorobenzene 541-73-1 8.28 U 0.000913 0.00761
1,4-Dichlorobenzene 106-46-7 8.28 U 0.00107 0.00761
Dichlorodifluoromethane 75-71-8 0 U 0.00245 0.00761
1,1-Dichloroethane 75-34-3 3.59 U 0.000747 0.00381
1,2-Dichloroethane 107-06-2 4.50 U 0.000987 0.00381
1,1-Dichloroethene 75-35-4 0 U 0.000922 0.00381
cis-1,2-Dichloroethene 156-59-2 3.90 0.00144 J 0.00112 0.00381
trans-1,2-Dichloroethene 156-60-5 0 U 0.00158 0.00761
1,2-Dichloropropane 78-87-5 0 U 0.00217 0.00761
1,1-Dichloropropene 563-58-6 0 U 0.00123 0.00381
1,3-Dichloropropane 142-28-9 0 U 0.000762 0.00761
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00116 0.00381
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00173 0.00761
2,2-Dichloropropane 594-20-7 4.04 U 0.00210 0.00381
Di-isopropyl ether 108-20-3 3.41 U 0.000624 0.00152
Ethylbenzene 100-41-4 6.58 0.0267 0.00112 0.00381
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00913 0.0381
Isopropylbenzene 98-82-8 7.20 0.0117 0.000646 0.00381
p-Isopropyltoluene 99-87-6 8.13 0.0700 0.00388 0.00761
2-Butanone (MEK)78-93-3 4.19 U 0.0966 0.152
Methylene Chloride 75-09-2 3.17 U 0.0101 0.0381
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:0725_55 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 11:20
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 16:29
Dilution Factor:1.37 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.32 g
Total Solids (%):94.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.77 U 0.00347 0.0381
Methyl tert-butyl ether 1634-04-4 3.22 U 0.000533 0.00152
Naphthalene 91-20-3 10.08 0.104 0.00743 0.0190
n-Propylbenzene 103-65-1 7.50 0.0113 0.00144 0.00761
Styrene 100-42-5 6.98 U 0.000349 0.0190
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00144 0.00381
1,1,2,2-Tetrachloroethane 79-34-5 7.55 U 0.00106 0.00381
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00114 0.00381
Tetrachloroethene 127-18-4 5.84 0.0195 0.00137 0.00381
Toluene 108-88-3 5.58 0.168 0.00198 0.00761
1,2,3-Trichlorobenzene 87-61-6 10.25 U 0.0111 0.0190
1,2,4-Trichlorobenzene 120-82-1 9.82 U 0.00670 0.0190
1,1,1-Trichloroethane 71-55-6 4.18 U 0.00140 0.00381
1,1,2-Trichloroethane 79-00-5 5.95 U 0.000908 0.00381
Trichloroethene 79-01-6 4.72 0.0205 0.000888 0.00152
Trichlorofluoromethane 75-69-4 0 U 0.00126 0.00381
1,2,3-Trichloropropane 96-18-4 7.73 U 0.00247 0.0190
1,2,4-Trimethylbenzene 95-63-6 7.94 0.172 0.00240 0.00761
1,2,3-Trimethylbenzene 526-73-8 8.28 0.120 0.00240 0.00761
1,3,5-Trimethylbenzene 108-67-8 7.64 0.0502 0.00304 0.00761
Vinyl chloride 75-01-4 0 U 0.00177 0.00381
Xylenes, Total 1330-20-7 6.98 0.374 0.00134 0.00988
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:0725_44 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 11:35
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 13:18
Dilution Factor:1.21 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.26 g
Total Solids (%):93.8 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.15 U 0.0495 0.0678
Acrylonitrile 107-13-1 3.65 U 0.00490 0.0169
Benzene 71-43-2 4.39 0.0115 0.000633 0.00136
Bromobenzene 108-86-1 0 U 0.00122 0.0169
Bromodichloromethane 75-27-4 4.98 U 0.000983 0.00339
Bromoform 75-25-2 0 U 0.00159 0.0339
Bromomethane 74-83-9 2.28 U 0.00267 0.0169
n-Butylbenzene 104-51-8 8.46 U 0.00711 0.0169
sec-Butylbenzene 135-98-8 8.03 U 0.00390 0.0169
tert-Butylbenzene 98-06-6 7.94 U 0.00264 0.00678
Carbon tetrachloride 56-23-5 0 U 0.00122 0.00678
Chlorobenzene 108-90-7 0 U 0.000285 0.00339
Chlorodibromomethane 124-48-1 0 U 0.000830 0.00339
Chloroethane 75-00-3 2.41 U 0.00231 0.00678
Chloroform 67-66-3 4.04 0.00278 J 0.00140 0.00339
Chloromethane 74-87-3 1.95 U J3 0.00589 0.0169
2-Chlorotoluene 95-49-8 0 U 0.00118 0.00339
4-Chlorotoluene 106-43-4 7.81 U 0.000609 0.00678
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00529 0.0339
1,2-Dibromoethane 106-93-4 0 U 0.000878 0.00339
Dibromomethane 74-95-3 0 U 0.00102 0.00678
1,2-Dichlorobenzene 95-50-1 0 U 0.000576 0.00678
1,3-Dichlorobenzene 541-73-1 0 U 0.000813 0.00678
1,4-Dichlorobenzene 106-46-7 0 U 0.000949 0.00678
Dichlorodifluoromethane 75-71-8 0 U 0.00218 0.00678
1,1-Dichloroethane 75-34-3 3.59 U 0.000665 0.00339
1,2-Dichloroethane 107-06-2 4.49 U 0.000879 0.00339
1,1-Dichloroethene 75-35-4 0 U 0.000821 0.00339
cis-1,2-Dichloroethene 156-59-2 3.90 0.0127 0.000995 0.00339
trans-1,2-Dichloroethene 156-60-5 3.23 U 0.00141 0.00678
1,2-Dichloropropane 78-87-5 0 U 0.00193 0.00678
1,1-Dichloropropene 563-58-6 4.21 U 0.00110 0.00339
1,3-Dichloropropane 142-28-9 0 U 0.000679 0.00678
cis-1,3-Dichloropropene 10061-01-5 5.48 U 0.00103 0.00339
trans-1,3-Dichloropropene 10061-02-6 5.81 U 0.00155 0.00678
2,2-Dichloropropane 594-20-7 3.92 U 0.00187 0.00339
Di-isopropyl ether 108-20-3 0 U 0.000556 0.00136
Ethylbenzene 100-41-4 6.58 0.00867 0.000999 0.00339
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00813 0.0339
Isopropylbenzene 98-82-8 7.20 0.00407 0.000576 0.00339
p-Isopropyltoluene 99-87-6 8.13 0.0189 0.00346 0.00678
2-Butanone (MEK)78-93-3 4.09 U 0.0860 0.136
Methylene Chloride 75-09-2 3.17 U 0.00900 0.0339
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:0725_44 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 11:35
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 13:18
Dilution Factor:1.21 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.26 g
Total Solids (%):93.8 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.77 0.0175 J 0.00309 0.0339
Methyl tert-butyl ether 1634-04-4 3.23 U 0.000474 0.00136
Naphthalene 91-20-3 10.09 0.0499 0.00661 0.0169
n-Propylbenzene 103-65-1 7.50 0.00492 J 0.00129 0.00678
Styrene 100-42-5 6.98 U 0.000310 0.0169
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00129 0.00339
1,1,2,2-Tetrachloroethane 79-34-5 7.54 U 0.000942 0.00339
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00102 0.00339
Tetrachloroethene 127-18-4 5.84 0.0164 0.00121 0.00339
Toluene 108-88-3 5.58 0.0534 0.00176 0.00678
1,2,3-Trichlorobenzene 87-61-6 10.26 U 0.00994 0.0169
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00596 0.0169
1,1,1-Trichloroethane 71-55-6 4.18 U 0.00125 0.00339
1,1,2-Trichloroethane 79-00-5 5.96 U 0.000809 0.00339
Trichloroethene 79-01-6 4.72 0.0485 0.000792 0.00136
Trichlorofluoromethane 75-69-4 0 U 0.00112 0.00339
1,2,3-Trichloropropane 96-18-4 7.68 U 0.00220 0.0169
1,2,4-Trimethylbenzene 95-63-6 7.94 0.0642 0.00214 0.00678
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0365 0.00214 0.00678
1,3,5-Trimethylbenzene 108-67-8 7.64 0.0243 0.00271 0.00678
Vinyl chloride 75-01-4 0 U 0.00157 0.00339
Xylenes, Total 1330-20-7 6.98 0.147 0.00119 0.00881
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:0725_56 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 11:55
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 16:48
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.06 g
Total Solids (%):98.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U 0.0379 0.0519
Acrylonitrile 107-13-1 3.65 U 0.00375 0.0130
Benzene 71-43-2 4.39 0.000745 J 0.000485 0.00104
Bromobenzene 108-86-1 0 U 0.000934 0.0130
Bromodichloromethane 75-27-4 4.98 U 0.000753 0.00259
Bromoform 75-25-2 7.06 U 0.00121 0.0259
Bromomethane 74-83-9 2.33 U 0.00204 0.0130
n-Butylbenzene 104-51-8 8.46 U 0.00545 0.0130
sec-Butylbenzene 135-98-8 8.03 U 0.00299 0.0130
tert-Butylbenzene 98-06-6 7.94 U 0.00202 0.00519
Carbon tetrachloride 56-23-5 4.18 U 0.000932 0.00519
Chlorobenzene 108-90-7 0 U 0.000218 0.00259
Chlorodibromomethane 124-48-1 0 U 0.000635 0.00259
Chloroethane 75-00-3 2.29 U 0.00176 0.00519
Chloroform 67-66-3 4.04 U 0.00107 0.00259
Chloromethane 74-87-3 0 U J3 0.00452 0.0130
2-Chlorotoluene 95-49-8 0 U 0.000898 0.00259
4-Chlorotoluene 106-43-4 7.81 U 0.000467 0.00519
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00405 0.0259
1,2-Dibromoethane 106-93-4 0 U 0.000673 0.00259
Dibromomethane 74-95-3 0 U 0.000778 0.00519
1,2-Dichlorobenzene 95-50-1 0 U 0.000441 0.00519
1,3-Dichlorobenzene 541-73-1 0 U 0.000623 0.00519
1,4-Dichlorobenzene 106-46-7 0 U 0.000727 0.00519
Dichlorodifluoromethane 75-71-8 0 U 0.00167 0.00519
1,1-Dichloroethane 75-34-3 3.59 U 0.000510 0.00259
1,2-Dichloroethane 107-06-2 4.49 U 0.000674 0.00259
1,1-Dichloroethene 75-35-4 0 U 0.000629 0.00259
cis-1,2-Dichloroethene 156-59-2 3.90 0.000822 J 0.000762 0.00259
trans-1,2-Dichloroethene 156-60-5 0 U 0.00108 0.00519
1,2-Dichloropropane 78-87-5 0 U 0.00147 0.00519
1,1-Dichloropropene 563-58-6 0 U 0.000840 0.00259
1,3-Dichloropropane 142-28-9 0 U 0.000520 0.00519
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000786 0.00259
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00118 0.00519
2,2-Dichloropropane 594-20-7 0 U 0.00143 0.00259
Di-isopropyl ether 108-20-3 3.41 U 0.000426 0.00104
Ethylbenzene 100-41-4 6.58 0.00208 J 0.000765 0.00259
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00623 0.0259
Isopropylbenzene 98-82-8 7.20 0.000874 J 0.000441 0.00259
p-Isopropyltoluene 99-87-6 8.13 0.00460 J 0.00265 0.00519
2-Butanone (MEK)78-93-3 4.19 U 0.0659 0.104
Methylene Chloride 75-09-2 3.17 0.00850 J 0.00689 0.0259
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:0725_56 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 11:55
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 16:48
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.06 g
Total Solids (%):98.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 U 0.00237 0.0259
Methyl tert-butyl ether 1634-04-4 3.30 U 0.000363 0.00104
Naphthalene 91-20-3 10.09 0.0170 0.00507 0.0130
n-Propylbenzene 103-65-1 7.50 0.00108 J 0.000986 0.00519
Styrene 100-42-5 7.02 U 0.000238 0.0130
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000984 0.00259
1,1,2,2-Tetrachloroethane 79-34-5 7.56 U 0.000721 0.00259
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000783 0.00259
Tetrachloroethene 127-18-4 5.84 0.00501 0.000930 0.00259
Toluene 108-88-3 5.58 0.00568 0.00135 0.00519
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00761 0.0130
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00457 0.0130
1,1,1-Trichloroethane 71-55-6 4.19 U 0.000958 0.00259
1,1,2-Trichloroethane 79-00-5 5.94 U 0.000620 0.00259
Trichloroethene 79-01-6 4.72 0.0166 0.000606 0.00104
Trichlorofluoromethane 75-69-4 0 U 0.000858 0.00259
1,2,3-Trichloropropane 96-18-4 7.73 U 0.00168 0.0130
1,2,4-Trimethylbenzene 95-63-6 7.94 0.0144 0.00164 0.00519
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0106 0.00164 0.00519
1,3,5-Trimethylbenzene 108-67-8 7.64 0.00455 J 0.00208 0.00519
Vinyl chloride 75-01-4 0 U 0.00120 0.00259
Xylenes, Total 1330-20-7 6.98 0.0244 0.000913 0.00675
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:0725_28 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 13:15
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 15:58
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.23 g
Total Solids (%):98.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 U 0.0375 0.0514
Acrylonitrile 107-13-1 3.69 U 0.00371 0.0128
Benzene 71-43-2 4.40 0.00101 J 0.000480 0.00103
Bromobenzene 108-86-1 0 U 0.000925 0.0128
Bromodichloromethane 75-27-4 0 U 0.000745 0.00257
Bromoform 75-25-2 0 U 0.00120 0.0257
Bromomethane 74-83-9 2.42 U 0.00202 0.0128
n-Butylbenzene 104-51-8 8.45 U 0.00539 0.0128
sec-Butylbenzene 135-98-8 8.01 U 0.00296 0.0128
tert-Butylbenzene 98-06-6 7.93 U 0.00200 0.00514
Carbon tetrachloride 56-23-5 0 U 0.000923 0.00514
Chlorobenzene 108-90-7 6.57 U 0.000216 0.00257
Chlorodibromomethane 124-48-1 0 U 0.000629 0.00257
Chloroethane 75-00-3 2.45 U 0.00175 0.00514
Chloroform 67-66-3 0 U 0.00106 0.00257
Chloromethane 74-87-3 0 U 0.00447 0.0128
2-Chlorotoluene 95-49-8 0 U 0.000889 0.00257
4-Chlorotoluene 106-43-4 7.75 U 0.000462 0.00514
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00401 0.0257
1,2-Dibromoethane 106-93-4 0 U 0.000666 0.00257
Dibromomethane 74-95-3 0 U 0.000771 0.00514
1,2-Dichlorobenzene 95-50-1 0 U 0.000437 0.00514
1,3-Dichlorobenzene 541-73-1 0 U 0.000617 0.00514
1,4-Dichlorobenzene 106-46-7 0 U 0.000719 0.00514
Dichlorodifluoromethane 75-71-8 0 U 0.00165 0.00514
1,1-Dichloroethane 75-34-3 0 U 0.000505 0.00257
1,2-Dichloroethane 107-06-2 4.51 U 0.000667 0.00257
1,1-Dichloroethene 75-35-4 0 U 0.000623 0.00257
cis-1,2-Dichloroethene 156-59-2 3.98 U 0.000754 0.00257
trans-1,2-Dichloroethene 156-60-5 0 U 0.00107 0.00514
1,2-Dichloropropane 78-87-5 0 U 0.00146 0.00514
1,1-Dichloropropene 563-58-6 0 U 0.000831 0.00257
1,3-Dichloropropane 142-28-9 0 U 0.000515 0.00514
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000778 0.00257
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00117 0.00514
2,2-Dichloropropane 594-20-7 0 U 0.00142 0.00257
Di-isopropyl ether 108-20-3 3.47 U 0.000421 0.00103
Ethylbenzene 100-41-4 6.58 0.00176 J 0.000757 0.00257
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00617 0.0257
Isopropylbenzene 98-82-8 7.20 0.000580 J 0.000437 0.00257
p-Isopropyltoluene 99-87-6 8.11 U 0.00262 0.00514
2-Butanone (MEK)78-93-3 4.24 U 0.0652 0.103
Methylene Chloride 75-09-2 3.20 0.00693 J 0.00682 0.0257
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:0725_28 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 13:15
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 15:58
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.23 g
Total Solids (%):98.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.76 U 0.00234 0.0257
Methyl tert-butyl ether 1634-04-4 3.30 U 0.000360 0.00103
Naphthalene 91-20-3 10.09 0.00957 J 0.00501 0.0128
n-Propylbenzene 103-65-1 7.50 U 0.000976 0.00514
Styrene 100-42-5 7.04 U 0.000235 0.0128
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000974 0.00257
1,1,2,2-Tetrachloroethane 79-34-5 7.51 U 0.000714 0.00257
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000775 0.00257
Tetrachloroethene 127-18-4 5.83 0.00144 J 0.000921 0.00257
Toluene 108-88-3 5.58 0.00693 0.00134 0.00514
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00753 0.0128
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00452 0.0128
1,1,1-Trichloroethane 71-55-6 0 U 0.000948 0.00257
1,1,2-Trichloroethane 79-00-5 0 U 0.000613 0.00257
Trichloroethene 79-01-6 4.72 0.00201 0.000600 0.00103
Trichlorofluoromethane 75-69-4 0 U 0.000850 0.00257
1,2,3-Trichloropropane 96-18-4 0 U 0.00166 0.0128
1,2,4-Trimethylbenzene 95-63-6 7.93 0.00689 0.00162 0.00514
1,2,3-Trimethylbenzene 526-73-8 8.28 0.00503 J 0.00162 0.00514
1,3,5-Trimethylbenzene 108-67-8 7.63 0.00325 J 0.00206 0.00514
Vinyl chloride 75-01-4 0 U 0.00119 0.00257
Xylenes, Total 1330-20-7 6.98 0.0174 0.000904 0.00668
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:0725_29 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 13:30
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 16:17
Dilution Factor:1.14 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.81 g
Total Solids (%):97.3 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 0 U 0.0438 0.0600
Acrylonitrile 107-13-1 3.67 U 0.00434 0.0151
Benzene 71-43-2 4.40 0.0163 0.000560 0.00120
Bromobenzene 108-86-1 0 U 0.00108 0.0151
Bromodichloromethane 75-27-4 0 U 0.000871 0.00300
Bromoform 75-25-2 0 U 0.00140 0.0300
Bromomethane 74-83-9 2.37 U 0.00237 0.0151
n-Butylbenzene 104-51-8 8.45 U 0.00631 0.0151
sec-Butylbenzene 135-98-8 8.01 U 0.00345 0.0151
tert-Butylbenzene 98-06-6 7.93 U 0.00234 0.00600
Carbon tetrachloride 56-23-5 4.16 0.00168 J 0.00107 0.00600
Chlorobenzene 108-90-7 6.57 U 0.000252 0.00300
Chlorodibromomethane 124-48-1 0 U 0.000735 0.00300
Chloroethane 75-00-3 2.45 U 0.00204 0.00600
Chloroform 67-66-3 4.07 U 0.00123 0.00300
Chloromethane 74-87-3 0 U 0.00522 0.0151
2-Chlorotoluene 95-49-8 0 U 0.00104 0.00300
4-Chlorotoluene 106-43-4 0 U 0.000540 0.00600
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00469 0.0300
1,2-Dibromoethane 106-93-4 0 U 0.000778 0.00300
Dibromomethane 74-95-3 0 U 0.000900 0.00600
1,2-Dichlorobenzene 95-50-1 0 U 0.000511 0.00600
1,3-Dichlorobenzene 541-73-1 8.27 U 0.000720 0.00600
1,4-Dichlorobenzene 106-46-7 8.27 U 0.000840 0.00600
Dichlorodifluoromethane 75-71-8 0 U 0.00194 0.00600
1,1-Dichloroethane 75-34-3 0 U 0.000590 0.00300
1,2-Dichloroethane 107-06-2 4.51 U 0.000779 0.00300
1,1-Dichloroethene 75-35-4 0 U 0.000728 0.00300
cis-1,2-Dichloroethene 156-59-2 0 U 0.000881 0.00300
trans-1,2-Dichloroethene 156-60-5 0 U 0.00125 0.00600
1,2-Dichloropropane 78-87-5 0 U 0.00171 0.00600
1,1-Dichloropropene 563-58-6 0 U 0.000971 0.00300
1,3-Dichloropropane 142-28-9 0 U 0.000601 0.00600
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000909 0.00300
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00137 0.00600
2,2-Dichloropropane 594-20-7 3.99 U 0.00165 0.00300
Di-isopropyl ether 108-20-3 0 U 0.000492 0.00120
Ethylbenzene 100-41-4 6.58 0.0112 0.000885 0.00300
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00720 0.0300
Isopropylbenzene 98-82-8 7.22 U 0.000511 0.00300
p-Isopropyltoluene 99-87-6 8.11 0.0131 0.00306 0.00600
2-Butanone (MEK)78-93-3 4.24 U 0.0762 0.120
Methylene Chloride 75-09-2 3.21 U 0.00797 0.0300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:0725_29 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 13:30
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 16:17
Dilution Factor:1.14 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.81 g
Total Solids (%):97.3 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.76 U 0.00274 0.0300
Methyl tert-butyl ether 1634-04-4 3.33 U 0.000420 0.00120
Naphthalene 91-20-3 10.08 0.0531 0.00585 0.0151
n-Propylbenzene 103-65-1 7.50 0.00393 J 0.00114 0.00600
Styrene 100-42-5 7.02 0.0574 0.000275 0.0151
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00114 0.00300
1,1,2,2-Tetrachloroethane 79-34-5 7.54 U 0.000834 0.00300
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000906 0.00300
Tetrachloroethene 127-18-4 5.83 0.0148 0.00107 0.00300
Toluene 108-88-3 5.58 0.0718 0.00156 0.00600
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00880 0.0151
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00529 0.0151
1,1,1-Trichloroethane 71-55-6 4.21 U 0.00111 0.00300
1,1,2-Trichloroethane 79-00-5 0 U 0.000717 0.00300
Trichloroethene 79-01-6 4.72 0.00957 0.000701 0.00120
Trichlorofluoromethane 75-69-4 0 U 0.000993 0.00300
1,2,3-Trichloropropane 96-18-4 7.65 U 0.00195 0.0151
1,2,4-Trimethylbenzene 95-63-6 7.93 0.0496 0.00190 0.00600
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0313 0.00190 0.00600
1,3,5-Trimethylbenzene 108-67-8 7.63 0.0173 0.00240 0.00600
Vinyl chloride 75-01-4 0 U 0.00139 0.00300
Xylenes, Total 1330-20-7 6.98 0.120 0.00105 0.00780
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:0725_30 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:40
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 16:36
Dilution Factor:1.21 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.28 g
Total Solids (%):97.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 0 U 0.0465 0.0637
Acrylonitrile 107-13-1 3.67 U 0.00460 0.0159
Benzene 71-43-2 4.40 0.00413 0.000594 0.00127
Bromobenzene 108-86-1 0 U 0.00115 0.0159
Bromodichloromethane 75-27-4 5.11 U 0.000923 0.00319
Bromoform 75-25-2 0 U 0.00149 0.0319
Bromomethane 74-83-9 2.32 U 0.00250 0.0159
n-Butylbenzene 104-51-8 8.45 U 0.00668 0.0159
sec-Butylbenzene 135-98-8 8.01 U 0.00366 0.0159
tert-Butylbenzene 98-06-6 7.88 U 0.00248 0.00637
Carbon tetrachloride 56-23-5 4.16 0.00165 J 0.00115 0.00637
Chlorobenzene 108-90-7 6.57 U 0.000267 0.00319
Chlorodibromomethane 124-48-1 0 U 0.000780 0.00319
Chloroethane 75-00-3 2.43 U 0.00217 0.00637
Chloroform 67-66-3 4.06 U 0.00132 0.00319
Chloromethane 74-87-3 0 U 0.00553 0.0159
2-Chlorotoluene 95-49-8 0 U 0.00110 0.00319
4-Chlorotoluene 106-43-4 7.80 U 0.000572 0.00637
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00497 0.0319
1,2-Dibromoethane 106-93-4 0 U 0.000825 0.00319
Dibromomethane 74-95-3 0 U 0.000955 0.00637
1,2-Dichlorobenzene 95-50-1 0 U 0.000541 0.00637
1,3-Dichlorobenzene 541-73-1 8.27 U 0.000764 0.00637
1,4-Dichlorobenzene 106-46-7 8.27 U 0.000891 0.00637
Dichlorodifluoromethane 75-71-8 0 U 0.00205 0.00637
1,1-Dichloroethane 75-34-3 0 U 0.000625 0.00319
1,2-Dichloroethane 107-06-2 4.52 U 0.000826 0.00319
1,1-Dichloroethene 75-35-4 0 U 0.000771 0.00319
cis-1,2-Dichloroethene 156-59-2 3.99 U 0.000934 0.00319
trans-1,2-Dichloroethene 156-60-5 3.26 U 0.00133 0.00637
1,2-Dichloropropane 78-87-5 0 U 0.00181 0.00637
1,1-Dichloropropene 563-58-6 0 U 0.00103 0.00319
1,3-Dichloropropane 142-28-9 0 U 0.000638 0.00637
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000964 0.00319
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00145 0.00637
2,2-Dichloropropane 594-20-7 0 U 0.00176 0.00319
Di-isopropyl ether 108-20-3 3.44 U 0.000522 0.00127
Ethylbenzene 100-41-4 6.57 0.00649 0.000938 0.00319
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00764 0.0319
Isopropylbenzene 98-82-8 7.20 0.00299 J 0.000541 0.00319
p-Isopropyltoluene 99-87-6 8.11 0.0123 0.00325 0.00637
2-Butanone (MEK)78-93-3 4.24 U 0.0808 0.127
Methylene Chloride 75-09-2 3.21 0.0119 J 0.00845 0.0319
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:0725_30 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:40
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 16:36
Dilution Factor:1.21 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.28 g
Total Solids (%):97.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.76 U 0.00290 0.0319
Methyl tert-butyl ether 1634-04-4 0 U 0.000445 0.00127
Naphthalene 91-20-3 10.08 0.0459 0.00621 0.0159
n-Propylbenzene 103-65-1 7.50 0.00280 J 0.00121 0.00637
Styrene 100-42-5 7.02 0.0369 0.000291 0.0159
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00121 0.00319
1,1,2,2-Tetrachloroethane 79-34-5 7.53 U 0.000885 0.00319
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000960 0.00319
Tetrachloroethene 127-18-4 5.84 0.0122 0.00114 0.00319
Toluene 108-88-3 5.58 0.0240 0.00165 0.00637
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00933 0.0159
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00560 0.0159
1,1,1-Trichloroethane 71-55-6 4.19 U 0.00118 0.00319
1,1,2-Trichloroethane 79-00-5 5.94 U 0.000760 0.00319
Trichloroethene 79-01-6 4.72 0.00850 0.000744 0.00127
Trichlorofluoromethane 75-69-4 0 U 0.00105 0.00319
1,2,3-Trichloropropane 96-18-4 7.70 U 0.00206 0.0159
1,2,4-Trimethylbenzene 95-63-6 7.93 0.0312 0.00201 0.00637
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0214 0.00201 0.00637
1,3,5-Trimethylbenzene 108-67-8 7.63 0.0120 0.00255 0.00637
Vinyl chloride 75-01-4 0 U 0.00147 0.00319
Xylenes, Total 1330-20-7 6.98 0.0641 0.00112 0.00827
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:0725_24 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 13:55
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 14:34
Dilution Factor:1.06 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.44 g
Total Solids (%):95.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.18 U 0.0426 0.0583
Acrylonitrile 107-13-1 3.66 U 0.00421 0.0146
Benzene 71-43-2 4.40 0.0162 0.000544 0.00117
Bromobenzene 108-86-1 0 U 0.00105 0.0146
Bromodichloromethane 75-27-4 0 U 0.000846 0.00291
Bromoform 75-25-2 7.06 U 0.00136 0.0291
Bromomethane 74-83-9 0 U 0.00230 0.0146
n-Butylbenzene 104-51-8 8.41 U 0.00612 0.0146
sec-Butylbenzene 135-98-8 8.01 U 0.00335 0.0146
tert-Butylbenzene 98-06-6 7.93 U 0.00228 0.00583
Carbon tetrachloride 56-23-5 0 U 0.00105 0.00583
Chlorobenzene 108-90-7 0 U 0.000245 0.00291
Chlorodibromomethane 124-48-1 0 U 0.000714 0.00291
Chloroethane 75-00-3 2.48 U 0.00198 0.00583
Chloroform 67-66-3 4.06 U 0.00120 0.00291
Chloromethane 74-87-3 2.02 U 0.00507 0.0146
2-Chlorotoluene 95-49-8 0 U 0.00101 0.00291
4-Chlorotoluene 106-43-4 7.80 U 0.000525 0.00583
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00454 0.0291
1,2-Dibromoethane 106-93-4 0 U 0.000756 0.00291
Dibromomethane 74-95-3 0 U 0.000874 0.00583
1,2-Dichlorobenzene 95-50-1 0 U 0.000496 0.00583
1,3-Dichlorobenzene 541-73-1 0 U 0.000700 0.00583
1,4-Dichlorobenzene 106-46-7 0 U 0.000816 0.00583
Dichlorodifluoromethane 75-71-8 0 U 0.00188 0.00583
1,1-Dichloroethane 75-34-3 3.62 0.00685 0.000572 0.00291
1,2-Dichloroethane 107-06-2 4.51 U 0.000757 0.00291
1,1-Dichloroethene 75-35-4 0 U 0.000706 0.00291
cis-1,2-Dichloroethene 156-59-2 3.92 0.0285 0.000856 0.00291
trans-1,2-Dichloroethene 156-60-5 3.27 0.00338 J 0.00121 0.00583
1,2-Dichloropropane 78-87-5 0 U 0.00166 0.00583
1,1-Dichloropropene 563-58-6 4.28 U 0.000944 0.00291
1,3-Dichloropropane 142-28-9 0 U 0.000584 0.00583
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000882 0.00291
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00133 0.00583
2,2-Dichloropropane 594-20-7 3.95 U 0.00161 0.00291
Di-isopropyl ether 108-20-3 0 U 0.000478 0.00117
Ethylbenzene 100-41-4 6.57 0.0186 0.000859 0.00291
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00700 0.0291
Isopropylbenzene 98-82-8 7.20 0.00775 0.000496 0.00291
p-Isopropyltoluene 99-87-6 8.11 0.00871 0.00297 0.00583
2-Butanone (MEK)78-93-3 0 U 0.0740 0.117
Methylene Chloride 75-09-2 3.21 U 0.00774 0.0291
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:0725_24 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 13:55
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 14:34
Dilution Factor:1.06 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.44 g
Total Solids (%):95.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.76 U 0.00266 0.0291
Methyl tert-butyl ether 1634-04-4 3.33 U 0.000408 0.00117
Naphthalene 91-20-3 10.08 0.0382 0.00569 0.0146
n-Propylbenzene 103-65-1 7.50 0.00636 0.00111 0.00583
Styrene 100-42-5 6.97 U 0.000267 0.0146
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00110 0.00291
1,1,2,2-Tetrachloroethane 79-34-5 7.52 U 0.000811 0.00291
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000879 0.00291
Tetrachloroethene 127-18-4 5.83 0.0246 0.00104 0.00291
Toluene 108-88-3 5.58 0.0921 0.00152 0.00583
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00855 0.0146
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00513 0.0146
1,1,1-Trichloroethane 71-55-6 4.19 U 0.00108 0.00291
1,1,2-Trichloroethane 79-00-5 0 U 0.000696 0.00291
Trichloroethene 79-01-6 4.72 0.0477 0.000681 0.00117
Trichlorofluoromethane 75-69-4 0 U 0.000965 0.00291
1,2,3-Trichloropropane 96-18-4 0 U 0.00189 0.0146
1,2,4-Trimethylbenzene 95-63-6 7.93 0.0784 0.00184 0.00583
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0438 0.00184 0.00583
1,3,5-Trimethylbenzene 108-67-8 7.63 0.0430 0.00233 0.00583
Vinyl chloride 75-01-4 0 U 0.00135 0.00291
Xylenes, Total 1330-20-7 6.97 0.220 0.00103 0.00758
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:0724A_16 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:10
Analytical Batch:WG2329566 Analysis Date/Time:07/25/24 00:48
Dilution Factor:1.22 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.23 g
Total Solids (%):93.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.18 U 0.0505 0.0692
Acrylonitrile 107-13-1 3.67 U 0.00499 0.0174
Benzene 71-43-2 4.40 0.00713 0.000647 0.00138
Bromobenzene 108-86-1 0 U 0.00125 0.0174
Bromodichloromethane 75-27-4 0 U 0.00100 0.00346
Bromoform 75-25-2 0 U 0.00162 0.0346
Bromomethane 74-83-9 0 U 0.00272 0.0174
n-Butylbenzene 104-51-8 8.45 U 0.00726 0.0174
sec-Butylbenzene 135-98-8 8.02 U 0.00398 0.0174
tert-Butylbenzene 98-06-6 7.88 U 0.00270 0.00692
Carbon tetrachloride 56-23-5 0 U 0.00125 0.00692
Chlorobenzene 108-90-7 0 U 0.000291 0.00346
Chlorodibromomethane 124-48-1 0 U 0.000848 0.00346
Chloroethane 75-00-3 2.40 U J4 0.00235 0.00692
Chloroform 67-66-3 4.07 U 0.00143 0.00346
Chloromethane 74-87-3 0 U 0.00603 0.0174
2-Chlorotoluene 95-49-8 0 U 0.00120 0.00346
4-Chlorotoluene 106-43-4 7.80 U 0.000623 0.00692
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00540 0.0346
1,2-Dibromoethane 106-93-4 0 U 0.000898 0.00346
Dibromomethane 74-95-3 0 U 0.00104 0.00692
1,2-Dichlorobenzene 95-50-1 0 U 0.000589 0.00692
1,3-Dichlorobenzene 541-73-1 0 U 0.000831 0.00692
1,4-Dichlorobenzene 106-46-7 0 U 0.000969 0.00692
Dichlorodifluoromethane 75-71-8 0 U 0.00222 0.00692
1,1-Dichloroethane 75-34-3 3.62 U 0.000680 0.00346
1,2-Dichloroethane 107-06-2 4.52 U 0.000899 0.00346
1,1-Dichloroethene 75-35-4 0 U 0.000839 0.00346
cis-1,2-Dichloroethene 156-59-2 3.93 0.00198 J 0.00102 0.00346
trans-1,2-Dichloroethene 156-60-5 0 U 0.00144 0.00692
1,2-Dichloropropane 78-87-5 0 U 0.00196 0.00692
1,1-Dichloropropene 563-58-6 4.30 U 0.00112 0.00346
1,3-Dichloropropane 142-28-9 0 U 0.000694 0.00692
cis-1,3-Dichloropropene 10061-01-5 5.46 U 0.00105 0.00346
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00158 0.00692
2,2-Dichloropropane 594-20-7 4.04 U 0.00191 0.00346
Di-isopropyl ether 108-20-3 0 U 0.000568 0.00138
Ethylbenzene 100-41-4 6.58 0.00537 0.00102 0.00346
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00831 0.0346
Isopropylbenzene 98-82-8 7.20 0.00221 J 0.000589 0.00346
p-Isopropyltoluene 99-87-6 8.11 0.0131 0.00353 0.00692
2-Butanone (MEK)78-93-3 4.24 U 0.0880 0.138
Methylene Chloride 75-09-2 3.21 U 0.00919 0.0346
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:0724A_16 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:10
Analytical Batch:WG2329566 Analysis Date/Time:07/25/24 00:48
Dilution Factor:1.22 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.23 g
Total Solids (%):93.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.83 U 0.00316 0.0346
Methyl tert-butyl ether 1634-04-4 0 U 0.000485 0.00138
Naphthalene 91-20-3 10.08 0.0453 B 0.00675 0.0174
n-Propylbenzene 103-65-1 7.50 0.00294 J 0.00132 0.00692
Styrene 100-42-5 7.03 U 0.000317 0.0174
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00132 0.00346
1,1,2,2-Tetrachloroethane 79-34-5 7.52 U 0.000963 0.00346
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00104 0.00346
Tetrachloroethene 127-18-4 5.83 0.0157 0.00124 0.00346
Toluene 108-88-3 5.58 0.0403 0.00180 0.00692
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0101 0.0174
1,2,4-Trichlorobenzene 120-82-1 9.82 U 0.00610 0.0174
1,1,1-Trichloroethane 71-55-6 0 U 0.00128 0.00346
1,1,2-Trichloroethane 79-00-5 5.94 U 0.000826 0.00346
Trichloroethene 79-01-6 4.72 0.0150 0.000808 0.00138
Trichlorofluoromethane 75-69-4 2.52 U 0.00115 0.00346
1,2,3-Trichloropropane 96-18-4 0 U 0.00225 0.0174
1,2,4-Trimethylbenzene 95-63-6 7.93 0.0348 0.00219 0.00692
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0252 0.00219 0.00692
1,3,5-Trimethylbenzene 108-67-8 7.63 0.0107 0.00277 0.00692
Vinyl chloride 75-01-4 0 U 0.00161 0.00346
Xylenes, Total 1330-20-7 6.98 0.0721 0.00121 0.00900
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:0724A_17 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:25
Analytical Batch:WG2329566 Analysis Date/Time:07/25/24 01:07
Dilution Factor:1.19 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.38 g
Total Solids (%):91.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.18 U 0.0513 0.0704
Acrylonitrile 107-13-1 3.66 U 0.00508 0.0176
Benzene 71-43-2 4.40 0.0242 0.000657 0.00141
Bromobenzene 108-86-1 0 U 0.00127 0.0176
Bromodichloromethane 75-27-4 0 U 0.00102 0.00351
Bromoform 75-25-2 0 U 0.00164 0.0351
Bromomethane 74-83-9 2.37 U 0.00277 0.0176
n-Butylbenzene 104-51-8 8.46 U 0.00739 0.0176
sec-Butylbenzene 135-98-8 8.01 U 0.00406 0.0176
tert-Butylbenzene 98-06-6 7.93 U 0.00274 0.00704
Carbon tetrachloride 56-23-5 0 U 0.00127 0.00704
Chlorobenzene 108-90-7 0 U 0.000296 0.00351
Chlorodibromomethane 124-48-1 0 U 0.000861 0.00351
Chloroethane 75-00-3 2.42 U J4 0.00239 0.00704
Chloroform 67-66-3 4.07 U 0.00145 0.00351
Chloromethane 74-87-3 2.01 U 0.00612 0.0176
2-Chlorotoluene 95-49-8 0 U 0.00122 0.00351
4-Chlorotoluene 106-43-4 7.80 U 0.000633 0.00704
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00549 0.0351
1,2-Dibromoethane 106-93-4 0 U 0.000912 0.00351
Dibromomethane 74-95-3 0 U 0.00105 0.00704
1,2-Dichlorobenzene 95-50-1 0 U 0.000598 0.00704
1,3-Dichlorobenzene 541-73-1 0 U 0.000844 0.00704
1,4-Dichlorobenzene 106-46-7 0 U 0.000985 0.00704
Dichlorodifluoromethane 75-71-8 0 U 0.00227 0.00704
1,1-Dichloroethane 75-34-3 3.63 0.00479 0.000691 0.00351
1,2-Dichloroethane 107-06-2 4.52 U 0.000913 0.00351
1,1-Dichloroethene 75-35-4 0 U 0.000853 0.00351
cis-1,2-Dichloroethene 156-59-2 3.93 0.0294 0.00103 0.00351
trans-1,2-Dichloroethene 156-60-5 3.28 0.00246 J 0.00147 0.00704
1,2-Dichloropropane 78-87-5 0 U 0.00200 0.00704
1,1-Dichloropropene 563-58-6 0 U 0.00114 0.00351
1,3-Dichloropropane 142-28-9 0 U 0.000705 0.00704
cis-1,3-Dichloropropene 10061-01-5 5.45 U 0.00107 0.00351
trans-1,3-Dichloropropene 10061-02-6 5.80 U 0.00161 0.00704
2,2-Dichloropropane 594-20-7 3.94 U 0.00194 0.00351
Di-isopropyl ether 108-20-3 0 U 0.000577 0.00141
Ethylbenzene 100-41-4 6.58 0.0104 0.00104 0.00351
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00844 0.0351
Isopropylbenzene 98-82-8 7.20 0.00342 J 0.000598 0.00351
p-Isopropyltoluene 99-87-6 8.11 0.0114 0.00358 0.00704
2-Butanone (MEK)78-93-3 4.24 U 0.0894 0.141
Methylene Chloride 75-09-2 0 U 0.00934 0.0351
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:0724A_17 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:25
Analytical Batch:WG2329566 Analysis Date/Time:07/25/24 01:07
Dilution Factor:1.19 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.38 g
Total Solids (%):91.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.76 U 0.00320 0.0351
Methyl tert-butyl ether 1634-04-4 3.28 U 0.000493 0.00141
Naphthalene 91-20-3 10.08 0.0477 B 0.00687 0.0176
n-Propylbenzene 103-65-1 7.50 0.00355 J 0.00134 0.00704
Styrene 100-42-5 6.98 U 0.000323 0.0176
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00134 0.00351
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000978 0.00351
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00106 0.00351
Tetrachloroethene 127-18-4 5.84 0.0492 0.00127 0.00351
Toluene 108-88-3 5.58 0.0893 0.00183 0.00704
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0103 0.0176
1,2,4-Trichlorobenzene 120-82-1 9.81 U 0.00620 0.0176
1,1,1-Trichloroethane 71-55-6 4.19 U 0.00130 0.00351
1,1,2-Trichloroethane 79-00-5 5.94 U 0.000840 0.00351
Trichloroethene 79-01-6 4.72 0.101 0.000822 0.00141
Trichlorofluoromethane 75-69-4 0 U 0.00116 0.00351
1,2,3-Trichloropropane 96-18-4 0 U 0.00228 0.0176
1,2,4-Trimethylbenzene 95-63-6 7.93 0.0408 0.00222 0.00704
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0287 0.00222 0.00704
1,3,5-Trimethylbenzene 108-67-8 7.63 0.0110 0.00281 0.00704
Vinyl chloride 75-01-4 0 U 0.00163 0.00351
Xylenes, Total 1330-20-7 6.98 0.130 0.00124 0.00915
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:0724A_18 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:41
Analytical Batch:WG2329566 Analysis Date/Time:07/25/24 01:26
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.3 g
Total Solids (%):85.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.18 U 0.0490 0.0671
Acrylonitrile 107-13-1 3.67 U 0.00485 0.0168
Benzene 71-43-2 4.41 0.000911 J 0.000627 0.00134
Bromobenzene 108-86-1 0 U 0.00121 0.0168
Bromodichloromethane 75-27-4 0 U 0.000973 0.00336
Bromoform 75-25-2 0 U 0.00157 0.0336
Bromomethane 74-83-9 2.39 U 0.00264 0.0168
n-Butylbenzene 104-51-8 8.45 U 0.00705 0.0168
sec-Butylbenzene 135-98-8 0 U 0.00387 0.0168
tert-Butylbenzene 98-06-6 7.93 U 0.00262 0.00671
Carbon tetrachloride 56-23-5 4.20 U 0.00121 0.00671
Chlorobenzene 108-90-7 0 U 0.000282 0.00336
Chlorodibromomethane 124-48-1 0 U 0.000822 0.00336
Chloroethane 75-00-3 2.42 U J4 0.00228 0.00671
Chloroform 67-66-3 4.07 U 0.00138 0.00336
Chloromethane 74-87-3 0 U 0.00584 0.0168
2-Chlorotoluene 95-49-8 0 U 0.00116 0.00336
4-Chlorotoluene 106-43-4 7.80 U 0.000604 0.00671
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00524 0.0336
1,2-Dibromoethane 106-93-4 0 U 0.000870 0.00336
Dibromomethane 74-95-3 0 U 0.00101 0.00671
1,2-Dichlorobenzene 95-50-1 0 U 0.000571 0.00671
1,3-Dichlorobenzene 541-73-1 0 U 0.000805 0.00671
1,4-Dichlorobenzene 106-46-7 0 U 0.000940 0.00671
Dichlorodifluoromethane 75-71-8 0 U 0.00216 0.00671
1,1-Dichloroethane 75-34-3 3.62 0.00297 J 0.000659 0.00336
1,2-Dichloroethane 107-06-2 4.51 U 0.000871 0.00336
1,1-Dichloroethene 75-35-4 0 U 0.000813 0.00336
cis-1,2-Dichloroethene 156-59-2 3.93 0.0106 0.000985 0.00336
trans-1,2-Dichloroethene 156-60-5 3.28 0.00185 J 0.00140 0.00671
1,2-Dichloropropane 78-87-5 0 U 0.00191 0.00671
1,1-Dichloropropene 563-58-6 0 U 0.00109 0.00336
1,3-Dichloropropane 142-28-9 0 U 0.000673 0.00671
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00102 0.00336
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00153 0.00671
2,2-Dichloropropane 594-20-7 3.95 U 0.00185 0.00336
Di-isopropyl ether 108-20-3 0 U 0.000550 0.00134
Ethylbenzene 100-41-4 6.58 0.00277 J 0.000989 0.00336
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00805 0.0336
Isopropylbenzene 98-82-8 7.20 0.00215 J 0.000571 0.00336
p-Isopropyltoluene 99-87-6 8.11 0.00765 0.00342 0.00671
2-Butanone (MEK)78-93-3 4.24 U 0.0852 0.134
Methylene Chloride 75-09-2 3.21 U 0.00891 0.0336
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:0724A_18 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:07/16/24 14:41
Analytical Batch:WG2329566 Analysis Date/Time:07/25/24 01:26
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.3 g
Total Solids (%):85.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.76 U 0.00306 0.0336
Methyl tert-butyl ether 1634-04-4 3.34 U 0.000470 0.00134
Naphthalene 91-20-3 10.08 0.0315 B 0.00655 0.0168
n-Propylbenzene 103-65-1 7.50 0.00189 J 0.00128 0.00671
Styrene 100-42-5 6.98 U 0.000307 0.0168
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00127 0.00336
1,1,2,2-Tetrachloroethane 79-34-5 7.51 U 0.000933 0.00336
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00101 0.00336
Tetrachloroethene 127-18-4 5.83 0.209 0.00120 0.00336
Toluene 108-88-3 5.58 0.00976 0.00175 0.00671
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00984 0.0168
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00591 0.0168
1,1,1-Trichloroethane 71-55-6 4.20 0.0148 0.00124 0.00336
1,1,2-Trichloroethane 79-00-5 5.94 U 0.000801 0.00336
Trichloroethene 79-01-6 4.72 0.176 0.000784 0.00134
Trichlorofluoromethane 75-69-4 0 U 0.00111 0.00336
1,2,3-Trichloropropane 96-18-4 0 U 0.00217 0.0168
1,2,4-Trimethylbenzene 95-63-6 7.93 0.0273 0.00212 0.00671
1,2,3-Trimethylbenzene 526-73-8 8.28 0.0165 0.00212 0.00671
1,3,5-Trimethylbenzene 108-67-8 7.63 0.0104 0.00268 0.00671
Vinyl chloride 75-01-4 0 U 0.00156 0.00336
Xylenes, Total 1330-20-7 6.98 0.0456 0.00118 0.00873
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:0721_35 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS21 Preparation Date/Time:07/22/24 01:20
Analytical Batch:WG2327390 Analysis Date/Time:07/22/24 01:20
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 2.78 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U J4 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-1-071624
Lab Sample ID:L1757957-16 SDG:L1757957
Client Sample ID:EB-1-071624 Collected Date/Time:07/16/24 15:00
Lab File ID:0721_35 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS21 Preparation Date/Time:07/22/24 01:20
Analytical Batch:WG2327390 Analysis Date/Time:07/22/24 01:20
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1757957-17 SDG:L1757957
Client Sample ID:TRIP BLANK Collected Date/Time:07/16/24 00:00
Lab File ID:0721_33 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS21 Preparation Date/Time:07/22/24 00:33
Analytical Batch:WG2327390 Analysis Date/Time:07/22/24 00:33
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 2.78 U 0.0113 0.0500
Acrolein 107-02-8 2.61 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U J4 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 3.78 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1757957-17 SDG:L1757957
Client Sample ID:TRIP BLANK Collected Date/Time:07/16/24 00:00
Lab File ID:0721_33 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS21 Preparation Date/Time:07/22/24 00:33
Analytical Batch:WG2327390 Analysis Date/Time:07/22/24 00:33
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS21
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 07/10/24
11:59
07/10/24
12:23
07/10/24
12:46
07/10/24
13:10
07/10/24
13:33
07/10/24
13:57
07/10/24
14:20
07/10/24
14:44
DICHLORODIFLUOROMETHANE 0.2560 0.2360 0.2820 0.2370 0.2580 0.2750 0.2560 0.2740
CHLOROMETHANE 0.4150 0.3840 0.3840 0.3590 0.3570 0.3810 0.3870
VINYL CHLORIDE 0.2970 0.2690 0.2940 0.2520 0.2690 0.2910 0.2720 0.2770
BROMOMETHANE 0.0830 0.0930 0.0890 0.0850 0.0820 0.1030
CHLOROETHANE 0.1370 0.1390 0.1430 0.1250 0.1240 0.1230
TRICHLOROFLUOROMETHANE 0.3520 0.3370 0.3690 0.3270 0.3470 0.3810 0.3560 0.3270
ACROLEIN 0.1290 0.1240 0.1260 0.1180 0.1080 0.1160 0.1170 0.1030
1,1-DICHLOROETHENE 0.1310 0.1350 0.1440 0.1340 0.1410 0.1530 0.15 0.1530
1,1,2-TRICHLOROTRIFLUOROETHANE 0.1640 0.1510 0.1720 0.1490 0.16 0.1760 0.1670 0.1630
METHYLENE CHLORIDE 0.2190 0.2080 0.2060 0.2030 0.1910 0.2030 0.20 0.1940
ACRYLONITRILE 0.1580 0.1530 0.1540 0.1480 0.1450 0.1540 0.1460 0.1210
TRANS-1,2-DICHLOROETHENE 0.1690 0.1830 0.1790 0.1760 0.1770 0.1830 0.1770 0.1690
METHYL TERT-BUTYL ETHER 0.5960 0.5960 0.6020 0.5820 0.5630 0.5840 0.56 0.5070
1,1-DICHLOROETHANE 0.40 0.4020 0.3950 0.3740 0.3740 0.3970 0.3860 0.36
DI-ISOPROPYL ETHER 0.8440 0.8730 0.8720 0.8330 0.8280 0.8470 0.8030 0.6520
2,2-DICHLOROPROPANE 0.3560 0.3340 0.3420 0.31 0.3130 0.3320 0.3140 0.2960
CIS-1,2-DICHLOROETHENE 0.2240 0.2050 0.20 0.1990 0.1910 0.2030 0.1980 0.1920
2-BUTANONE (MEK)0.2390 0.2340 0.24 0.2290 0.23 0.2230 0.2020
CHLOROFORM 0.6620 0.5080 0.4550 0.3950 0.3710 0.3940 0.3780 0.3480
1,1,1-TRICHLOROETHANE 0.3180 0.3210 0.3360 0.3220 0.33 0.3570 0.3390 0.3220
CARBON TETRACHLORIDE 0.3210 0.3040 0.3210 0.2920 0.3040 0.3290 0.3130 0.3030
1,1-DICHLOROPROPENE 0.2580 0.2650 0.2540 0.2430 0.2570 0.2770 0.2630 0.2530
BENZENE 0.7910 0.7660 0.7460 0.7220 0.7210 0.7460 0.6990 0.5790
1,2-DICHLOROETHANE 0.3370 0.3450 0.3280 0.3070 0.3030 0.3170 0.3060 0.2870
TRICHLOROETHENE 0.1970 0.2050 0.2190 0.1940 0.2070 0.2180 0.2110 0.1970
1,2-DICHLOROPROPANE 0.1610 0.1620 0.1650 0.16 0.1580 0.1720 0.1680 0.1630
DIBROMOMETHANE 0.1240 0.1370 0.1430 0.1360 0.1320 0.1430 0.1410 0.1370
BROMODICHLOROMETHANE 0.2840 0.2920 0.2860 0.2790 0.2840 0.30 0.2940 0.2770
CIS-1,3-DICHLOROPROPENE 0.3320 0.3440 0.3420 0.3340 0.3310 0.3510 0.3410 0.3170
4-METHYL-2-PENTANONE (MIBK)0.8130 0.8020 0.8120 0.7770 0.7640 0.6320 0.5290
TOLUENE 1.8170 1.6210 1.5220 1.4570 1.4590 1.4750 1.3620 1.0720
TRANS-1,3-DICHLOROPROPENE 0.5840 0.5680 0.5780 0.5690 0.5750 0.6230 0.6010 0.5560
1,1,2-TRICHLOROETHANE 0.3360 0.3210 0.3430 0.3230 0.3170 0.3430 0.3330 0.3210
TETRACHLOROETHENE 0.3390 0.3330 0.3430 0.3250 0.3360 0.3620 0.3450 0.33
1,3-DICHLOROPROPANE 0.5710 0.5970 0.5680 0.5470 0.5530 0.5870 0.5710 0.5370
CHLORODIBROMOMETHANE 0.40 0.3970 0.4030 0.3940 0.4060 0.4470 0.4320 0.4120
1,2-DIBROMOETHANE 0.3420 0.3680 0.3660 0.3590 0.36 0.3880 0.3770 0.3610
CHLOROBENZENE 1.0360 0.9560 1.0040 0.9360 0.9350 0.9850 0.9170 0.78
1,1,1,2-TETRACHLOROETHANE 0.3190 0.3640 0.3570 0.3490 0.3540 0.3860 0.3720 0.3540
ETHYLBENZENE 0.5110 0.5290 0.50 0.4760 0.5040 0.5370 0.5090 0.4680
M&P-XYLENE 0.6090 0.6150 0.6220 0.5880 0.6030 0.6230 0.5780 0.4580
O-XYLENE 0.6010 0.5920 0.6090 0.5850 0.5860 0.6330 0.6090 0.5550
STYRENE 1.04 1.0430 1.0190 0.9660 1.0030 1.0760 1.0180 0.8510
BROMOFORM 0.3680 0.3640 0.3650 0.3680 0.3790 0.4230 0.4110 0.3930
ISOPROPYLBENZENE 1.4930 1.4890 1.4920 1.3910 1.4590 1.5270 1.4150 1.0850
BROMOBENZENE 0.7890 0.6520 0.6510 0.6080 0.6350 0.6590 0.6460 0.6060
1,1,2,2-TETRACHLOROETHANE 0.5150 0.5380 0.5410 0.51 0.5120 0.5410 0.5230 0.5050
1,2,3-TRICHLOROPROPANE 0.1480 0.1730 0.1710 0.1580 0.1620 0.1710 0.1670 0.1620
N-PROPYLBENZENE 1.6910 1.6510 1.6240 1.4930 1.5780 1.5580 1.4250 1.0890
2-CHLOROTOLUENE 1.04 1.0920 1.0910 1.05 1.0750 1.1060 1.0530 0.9030
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS21
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 07/10/24
11:59
07/10/24
12:23
07/10/24
12:46
07/10/24
13:10
07/10/24
13:33
07/10/24
13:57
07/10/24
14:20
07/10/24
14:44
4-CHLOROTOLUENE 1.1330 1.0750 1.0670 0.9850 1.0110 1.0580 1.0010 0.8530
1,3,5-TRIMETHYLBENZENE 1.0920 1.11 1.1140 1.0690 1.09 1.1140 1.0490 0.8730
TERT-BUTYLBENZENE 0.9050 0.8630 0.8850 0.8290 0.8760 0.9080 0.8560 0.7780
1,2,4-TRIMETHYLBENZENE 1.2060 1.1170 1.1320 1.0840 1.1220 1.1380 1.0780 0.8940
SEC-BUTYLBENZENE 1.2570 1.1990 1.2360 1.16 1.1970 1.2250 1.1470 0.9560
1,3-DICHLOROBENZENE 0.6570 0.6430 0.6340 0.62 0.6450 0.6760 0.6540 0.61
P-ISOPROPYLTOLUENE 1.1330 1.0670 1.1160 1.02 1.0650 1.0820 1.0130 0.8710
1,4-DICHLOROBENZENE 0.6940 0.6770 0.6640 0.6450 0.6580 0.6850 0.66 0.5980
1,2,3-TRIMETHYLBENZENE 1.1710 1.1660 1.14 1.0850 1.1010 1.12 1.06 0.8870
1,2-DICHLOROBENZENE 0.6210 0.6320 0.6330 0.6150 0.6240 0.6480 0.6310 0.5820
N-BUTYLBENZENE 1.0240 0.8870 0.9060 0.8450 0.85 0.89 0.8390 0.7550
1,2-DIBROMO-3-CHLOROPROPANE 0.15 0.1620 0.1820 0.1690 0.1720 0.1840 0.1770 0.1720
1,2,4-TRICHLOROBENZENE 0.3670 0.3610 0.3680 0.3470 0.35 0.3760 0.3620 0.3630
HEXACHLORO-1,3-BUTADIENE 0.2070 0.1850 0.1840 0.1790 0.1730 0.1810 0.17 0.18
NAPHTHALENE 0.9420 0.9350 0.9420 0.9460 1.0290 1.1030 1.0520 0.8960
1,2,3-TRICHLOROBENZENE 0.37 0.3460 0.3450 0.3320 0.3430 0.36 0.3440 0.3470
1,2-DICHLOROETHANE-D4 0.3740 0.36 0.3520 0.3540 0.3560 0.3310 0.3290 0.3120
TOLUENE-D8 2.0010 1.9240 1.9020 1.8420 1.82 1.8290 1.7760 1.7280
4-BROMOFLUOROBENZENE 0.9340 0.8960 0.8660 0.8440 0.8390 0.8580 0.8310 0.8020
ACETONE 0.1710 0.1610 0.1450 0.1420 0.1460 0.1390 0.1150
File ID:0710_04 0710_05 0710_06 0710_07 0710_08 0710_09 0710_10 0710_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS21
Analyte RRF. Avg %RSD COD
Analysis date/time
DICHLORODIFLUOROMETHANE 0.25918 6.64
CHLOROMETHANE 0.38116 5.14
VINYL CHLORIDE 0.277494 5.56
BROMOMETHANE 0.088827 9.03
CHLOROETHANE 0.13198 6.64
TRICHLOROFLUOROMETHANE 0.349485 5.51
ACROLEIN 0.117573 7.52
1,1-DICHLOROETHENE 0.142518 6.3
1,1,2-TRICHLOROTRIFLUOROETHANE 0.162675 5.81
METHYLENE CHLORIDE 0.202966 4.26
ACRYLONITRILE 0.14733 7.88
TRANS-1,2-DICHLOROETHENE 0.176484 3.07
METHYL TERT-BUTYL ETHER 0.573816 5.41
1,1-DICHLOROETHANE 0.385988 3.93
DI-ISOPROPYL ETHER 0.819005 8.69
2,2-DICHLOROPROPANE 0.32462 6.1
CIS-1,2-DICHLOROETHENE 0.201576 5.15
2-BUTANONE (MEK)0.228205 5.65
CHLOROFORM 0.43888 23.66 0.998
1,1,1-TRICHLOROETHANE 0.330522 3.9
CARBON TETRACHLORIDE 0.310829 3.88
1,1-DICHLOROPROPENE 0.258749 3.89
BENZENE 0.721318 8.88
1,2-DICHLOROETHANE 0.316045 6.15
TRICHLOROETHENE 0.206203 4.67
1,2-DICHLOROPROPANE 0.16361 2.72
DIBROMOMETHANE 0.136665 4.68
BROMODICHLOROMETHANE 0.286859 2.78
CIS-1,3-DICHLOROPROPENE 0.336416 3.12
4-METHYL-2-PENTANONE (MIBK)0.732693 14.98
TOLUENE 1.473141 14.43
TRANS-1,3-DICHLOROPROPENE 0.581837 3.63
1,1,2-TRICHLOROETHANE 0.329463 3.2
TETRACHLOROETHENE 0.338995 3.38
1,3-DICHLOROPROPANE 0.566327 3.55
CHLORODIBROMOMETHANE 0.411313 4.55
1,2-DIBROMOETHANE 0.365029 3.72
CHLOROBENZENE 0.943604 8.17
1,1,1,2-TETRACHLOROETHANE 0.356705 5.45
ETHYLBENZENE 0.504132 4.67
M&P-XYLENE 0.586996 9.3
O-XYLENE 0.596017 3.84
STYRENE 1.002074 6.87
BROMOFORM 0.383731 5.92
ISOPROPYLBENZENE 1.4189 10
BROMOBENZENE 0.655581 8.76
1,1,2,2-TETRACHLOROETHANE 0.522995 2.83
1,2,3-TRICHLOROPROPANE 0.163877 5.13
N-PROPYLBENZENE 1.513385 12.67
2-CHLOROTOLUENE 1.051243 6.1
4-CHLOROTOLUENE 1.0228 8.16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS21
Analyte RRF. Avg %RSD COD
Analysis date/time
1,3,5-TRIMETHYLBENZENE 1.063924 7.56
TERT-BUTYLBENZENE 0.862527 4.99
1,2,4-TRIMETHYLBENZENE 1.09648 8.26
SEC-BUTYLBENZENE 1.172023 8.09
1,3-DICHLOROBENZENE 0.642402 3.29
P-ISOPROPYLTOLUENE 1.045782 7.83
1,4-DICHLOROBENZENE 0.660108 4.49
1,2,3-TRIMETHYLBENZENE 1.091305 8.34
1,2-DICHLOROBENZENE 0.623121 3.11
N-BUTYLBENZENE 0.874508 8.74
1,2-DIBROMO-3-CHLOROPROPANE 0.171003 6.44
1,2,4-TRICHLOROBENZENE 0.361999 2.62
HEXACHLORO-1,3-BUTADIENE 0.182425 6.11
NAPHTHALENE 0.980662 7.29
1,2,3-TRICHLOROBENZENE 0.348558 3.25
1,2-DICHLOROETHANE-D4 0.345914 5.76
TOLUENE-D8 1.852796 4.68
4-BROMOFLUOROBENZENE 0.858684 4.77
ACETONE 0.14562 12.21
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 439 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 07/08/24
19:30
07/08/24
19:49
07/08/24
20:08
07/08/24
20:27
07/08/24
20:46
07/08/24
21:05
07/08/24
21:24
07/08/24
21:43
07/08/24
22:02
07/08/24
22:21
VINYL CHLORIDE 0.3820 0.4610 0.3520 0.3050 0.2940 0.3010 0.30 0.3370 0.34 0.3380
METHYL TERT-BUTYL ETHER 0.5310 0.6040 0.5780 0.7310 0.7030 0.7950 0.7120 0.7740 0.7030 0.6910
DI-ISOPROPYL ETHER 0.6340 0.8110 0.7970 0.8090 0.7970 0.8420 0.8090 0.8550 0.8270 0.8080
BENZENE 1.1970 1.4020 1.2640 1.0260 0.9950 1.0120 0.9940 1.0410 1.0110 0.98
TRICHLOROETHENE 0.1030 0.29 0.2750 0.2750 0.2590 0.2620 0.2630 0.2820 0.28 0.2740
TRANS-1,3-DICHLOROPROPENE 0.9140 0.9280 0.8820 0.9040 0.9180 0.9360 0.9040 0.9260 0.8450 0.9980
1,3-DICHLOROPROPANE 0.9740 1.0170 1.0340 0.96 1.0260 1.0140 0.9390 0.9460 0.8640 1.0250
CHLOROBENZENE 1.9980 1.8270 1.8220 1.7360 1.6640 1.6320 1.5790 1.5710 1.4010 1.6120
ETHYLBENZENE 0.8290 1.0430 1.0050 0.90 0.8950 0.8530 0.84 0.8630 0.7680 0.8790
M&P-XYLENE 1.0850 1.2470 1.1470 1.0810 1.0390 1.0390 1.0090 1.04 0.9030 1.02
O-XYLENE 1.1160 1.2150 1.2110 1.0810 1.0210 1.0060 0.9930 0.9990 0.8890 1.0310
BROMOBENZENE 0.9650 0.7560 0.8320 0.9040 0.8840 0.9060 0.8670 0.8650 0.8520 0.8810
1,1,2,2-TETRACHLOROETHANE 0.8350 1.0410 1.1560 1.12 1.1640 1.25 1.1330 1.13 1.1090 1.1590
4-CHLOROTOLUENE 2.17 1.9010 2.3090 2.2890 2.4260 2.4750 2.4110 2.4390 2.4030 2.3870
1,3,5-TRIMETHYLBENZENE 2.0610 2.6810 2.6990 2.6880 2.7520 2.6530 2.5360 2.5410 2.3110 2.2370
1,2,4-TRIMETHYLBENZENE 1.7450 2.6580 2.6060 2.4650 2.5370 2.5790 2.4410 2.4770 2.35 2.3590
1,3-DICHLOROBENZENE 1.2530 1.1950 1.2180 1.3010 1.2920 1.2760 1.2320 1.2930 1.2970 1.3240
1,4-DICHLOROBENZENE 1.5580 1.4160 1.3910 1.3260 1.3620 1.3890 1.3070 1.3260 1.3090 1.3350
1,2,3-TRIMETHYLBENZENE 2.9070 2.6750 2.6030 2.5830 2.4030 2.4510 2.33 2.3170 2.1610 2.2120
1,2-DICHLOROBENZENE 0.9580 1.1740 1.2030 1.1220 1.1940 1.2340 1.1370 1.1630 1.1820 1.2250
1,2-DICHLOROETHANE-D4 0.2620 0.3150 0.3070 0.3160 0.3010 0.31 0.31 0.3360 0.3670 0.3780
TOLUENE-D8 2.3620 2.3460 2.3430 2.3140 2.34 2.3360 2.2920 2.2070 2.0450 2.4320
4-BROMOFLUOROBENZENE 0.8550 0.8420 0.8340 0.8570 0.8270 0.84 0.8350 0.8150 0.7540 0.8740
DICHLORODIFLUOROMETHANE 0.2590 0.3630 0.2910 0.3150 0.3030 0.3220 0.3770 0.3790 0.3650
CHLOROETHANE 0.23 0.2230 0.1960 0.1750 0.1910 0.1830 0.1990 0.1880 0.1760
TRICHLOROFLUOROMETHANE 0.3010 0.3040 0.2820 0.2890 0.3170 0.3290 0.4150 0.4280 0.4070
1,1-DICHLOROETHENE 0.49 0.5050 0.4170 0.4170 0.3980 0.4040 0.4490 0.4490 0.4380
1,1,2-TRICHLOROTRIFLUOROETHANE 0.2550 0.2910 0.2390 0.2380 0.2310 0.2230 0.26 0.2610 0.2620
ACRYLONITRILE 0.0930 0.1020 0.1320 0.12 0.1120 0.1280 0.1380 0.1340 0.1330
TRANS-1,2-DICHLOROETHENE 0.2770 0.2290 0.2540 0.2390 0.2620 0.2520 0.2740 0.2690 0.2620
1,1-DICHLOROETHANE 0.5690 0.4870 0.5270 0.4710 0.4990 0.4680 0.5070 0.4870 0.4820
2,2-DICHLOROPROPANE 0.3730 0.2890 0.3140 0.2650 0.2930 0.2820 0.2810 0.2720 0.2570
CIS-1,2-DICHLOROETHENE 0.2580 0.3360 0.3060 0.2790 0.30 0.2880 0.3060 0.2990 0.2950
CHLOROFORM 0.7090 0.5680 0.5580 0.4930 0.5230 0.4870 0.5220 0.5020 0.4910
1,1,1-TRICHLOROETHANE 0.3740 0.3990 0.3770 0.3560 0.37 0.3750 0.3990 0.4060 0.3940
CARBON TETRACHLORIDE 0.5390 0.4530 0.3880 0.3630 0.3510 0.3580 0.3860 0.3890 0.3790
1,1-DICHLOROPROPENE 0.3480 0.3830 0.3220 0.3240 0.3010 0.3110 0.3480 0.3380 0.3430
1,2-DICHLOROETHANE 0.4970 0.4480 0.40 0.38 0.3970 0.3620 0.3790 0.3770 0.3670
1,2-DICHLOROPROPANE 0.3490 0.3320 0.3050 0.31 0.2970 0.2730 0.2940 0.2940 0.2910
DIBROMOMETHANE 0.1630 0.1480 0.1880 0.1780 0.1690 0.1590 0.1740 0.1730 0.1720
BROMODICHLOROMETHANE 0.2950 0.3130 0.34 0.3330 0.3420 0.3360 0.3730 0.3690 0.3660
CIS-1,3-DICHLOROPROPENE 0.3990 0.3770 0.39 0.3670 0.4090 0.3770 0.4370 0.4380 0.4360
4-METHYL-2-PENTANONE (MIBK)0.8520 0.7630 0.8830 0.8480 0.8540 0.8330 0.8460 0.6940 0.7850
TOLUENE 3.1010 2.7670 2.7210 2.5740 2.4810 2.4160 2.5150 2.2520 2.6060
1,1,2-TRICHLOROETHANE 0.6190 0.6080 0.5540 0.5660 0.5610 0.5120 0.5540 0.5040 0.6010
TETRACHLOROETHENE 0.5250 0.5070 0.4670 0.4950 0.4720 0.4830 0.4850 0.4510 0.5250
CHLORODIBROMOMETHANE 0.7820 0.6920 0.6170 0.6180 0.6080 0.5880 0.6170 0.5830 0.6930
1,2-DIBROMOETHANE 0.5440 0.7550 0.6760 0.6610 0.6450 0.5870 0.6180 0.5580 0.6650
1,1,1,2-TETRACHLOROETHANE 0.8310 0.6150 0.58 0.5470 0.5460 0.5390 0.5390 0.48
STYRENE 2.0030 1.9520 1.7910 1.6840 1.7570 1.6870 1.72 1.5630 1.7920
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 440 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 07/08/24
19:30
07/08/24
19:49
07/08/24
20:08
07/08/24
20:27
07/08/24
20:46
07/08/24
21:05
07/08/24
21:24
07/08/24
21:43
07/08/24
22:02
07/08/24
22:21
BROMOFORM 0.4090 0.3820 0.3750 0.3680 0.3990 0.3990 0.4340 0.4130 0.5020
ISOPROPYLBENZENE 2.7970 2.4050 2.5060 2.3950 2.3920 2.3630 2.4130 2.0760 2.3120
N-PROPYLBENZENE 3.2220 3.43 3.41 3.9890 3.79 3.7140 3.7240 3.4570 3.3790
2-CHLOROTOLUENE 1.0250 0.8160 0.7780 0.8610 0.8150 0.7740 0.7380 0.7770 0.7890
TERT-BUTYLBENZENE 2.5240 2.1060 1.9950 2.0510 2.1350 2.0360 2.0460 1.8630 1.85
SEC-BUTYLBENZENE 3.4840 2.9610 2.5790 2.7580 2.7830 2.7320 2.7190 2.4910 2.5050
P-ISOPROPYLTOLUENE 1.9870 2.5970 2.2070 2.2180 2.3180 2.2440 2.26 2.0460 2.1060
N-BUTYLBENZENE 1.2740 1.7270 1.72 1.7150 1.6980 1.6340 1.7470 1.6490 1.7260
1,2,4-TRICHLOROBENZENE 0.2740 0.3480 0.3310 0.3480 0.3540 0.3460 0.3730 0.4280 0.4640
HEXACHLORO-1,3-BUTADIENE 0.1140 0.1860 0.1950 0.1860 0.1850 0.1720 0.1810 0.18 0.1980
1,2,3-TRICHLOROBENZENE 0.2930 0.3480 0.3010 0.2940 0.31 0.2940 0.3140 0.3830
CHLOROMETHANE 0.5250 0.5550 0.4440 0.4920 0.4660 0.5060 0.4870 0.4880
ACETONE 0.0840 0.0650 0.0460 0.0480 0.0540 0.0560 0.0530 0.0510
2-BUTANONE (MEK)0.1450 0.1130 0.1070 0.1130 0.1140 0.1370 0.1480 0.1450
1,2,3-TRICHLOROPROPANE 0.46 0.4650 0.4050 0.3990 0.3610 0.35 0.3420 0.3570
NAPHTHALENE 1.2640 1.3010 1.3430 1.4710 1.3290 1.49 1.8090 1.9310
BROMOMETHANE 0.1550 0.1420 0.1650 0.1720 0.1940 0.1710 0.1840
METHYLENE CHLORIDE 0.3920 0.3020 0.3170 0.2750 0.28 0.27 0.2670
1,2-DIBROMO-3-CHLOROPROPANE 0.2240 0.19 0.2180 0.21 0.2370 0.2490 0.2640
File ID:0708_09 0708_10 0708_11 0708_12 0708_13 0708_14 0708_15 0708_16 0708_17 0708_18
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 441 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF. Avg %RSD COD
Analysis date/time
VINYL CHLORIDE 0.341 14.79
METHYL TERT-BUTYL ETHER 0.682 12.5
DI-ISOPROPYL ETHER 0.799 7.64
BENZENE 1.092 13.24
TRICHLOROETHENE 0.256 21.31 1
TRANS-1,3-DICHLOROPROPENE 0.915 4.3
1,3-DICHLOROPROPANE 0.98 5.5
CHLOROBENZENE 1.684 9.94
ETHYLBENZENE 0.888 9.2
M&P-XYLENE 1.061 8.53
O-XYLENE 1.056 9.62
BROMOBENZENE 0.871 6.24
1,1,2,2-TETRACHLOROETHANE 1.11 9.89
4-CHLOROTOLUENE 2.321 7.44
1,3,5-TRIMETHYLBENZENE 2.516 9.31
1,2,4-TRIMETHYLBENZENE 2.422 10.66
1,3-DICHLOROBENZENE 1.268 3.29
1,4-DICHLOROBENZENE 1.372 5.49
1,2,3-TRIMETHYLBENZENE 2.464 9.31
1,2-DICHLOROBENZENE 1.159 6.83
1,2-DICHLOROETHANE-D4 0.32 10.4
TOLUENE-D8 2.302 4.62
4-BROMOFLUOROBENZENE 0.833 3.89
DICHLORODIFLUOROMETHANE 0.33 12.9
CHLOROETHANE 0.196 9.79
TRICHLOROFLUOROMETHANE 0.341 17.11 0.998
1,1-DICHLOROETHENE 0.441 8.41
1,1,2-TRICHLOROTRIFLUOROETHANE 0.251 8.25
ACRYLONITRILE 0.121 13.04
TRANS-1,2-DICHLOROETHENE 0.257 6.21
1,1-DICHLOROETHANE 0.5 6.36
2,2-DICHLOROPROPANE 0.292 11.91
CIS-1,2-DICHLOROETHENE 0.296 7.25
CHLOROFORM 0.539 12.95
1,1,1-TRICHLOROETHANE 0.383 4.32
CARBON TETRACHLORIDE 0.401 14.87
1,1-DICHLOROPROPENE 0.335 7.25
1,2-DICHLOROETHANE 0.401 10.99
1,2-DICHLOROPROPANE 0.305 7.53
DIBROMOMETHANE 0.169 6.87
BROMODICHLOROMETHANE 0.341 7.63
CIS-1,3-DICHLOROPROPENE 0.403 6.97
4-METHYL-2-PENTANONE (MIBK)0.817 7.24
TOLUENE 2.604 9.31
1,1,2-TRICHLOROETHANE 0.564 7.1
TETRACHLOROETHENE 0.49 5.22
CHLORODIBROMOMETHANE 0.644 10.13
1,2-DIBROMOETHANE 0.634 10.36
1,1,1,2-TETRACHLOROETHANE 0.585 18.26 0.997
STYRENE 1.772 7.67
BROMOFORM 0.409 9.85
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 442 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF. Avg %RSD COD
Analysis date/time
ISOPROPYLBENZENE 2.407 7.81
N-PROPYLBENZENE 3.568 6.89
2-CHLOROTOLUENE 0.819 10.33
TERT-BUTYLBENZENE 2.067 9.53
SEC-BUTYLBENZENE 2.779 10.91
P-ISOPROPYLTOLUENE 2.22 7.99
N-BUTYLBENZENE 1.654 8.91
1,2,4-TRICHLOROBENZENE 0.363 15.17
HEXACHLORO-1,3-BUTADIENE 0.177 14.1
1,2,3-TRICHLOROBENZENE 0.317 10.18
CHLOROMETHANE 0.495 6.89
ACETONE 0.057 21.24 0.999
2-BUTANONE (MEK)0.128 13.67
1,2,3-TRICHLOROPROPANE 0.392 12.45
NAPHTHALENE 1.492 16.64 0.992
BROMOMETHANE 0.169 10.26
METHYLENE CHLORIDE 0.3 14.69
1,2-DIBROMO-3-CHLOROPROPANE 0.228 10.99
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 443 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS58
Analyte RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 07/19/24
04:01
07/19/24
04:20
07/19/24
04:39
07/19/24
04:58
07/19/24
05:17
07/19/24
05:36
07/19/24
05:55
07/19/24
06:14
07/19/24
06:33
07/19/24
06:52
DICHLORODIFLUOROMETHANE 0.3290 0.3270 0.3680 0.3520 0.3050 0.3110 0.3270 0.3440 0.3590 0.3260
CHLOROMETHANE 0.5830 0.4890 0.5630 0.6970 0.6470 0.5540 0.5570 0.5380 0.5710 0.54
VINYL CHLORIDE 0.3030 0.31 0.3330 0.4060 0.3610 0.3790 0.3740 0.3820 0.3980 0.3830
TRICHLOROFLUOROMETHANE 0.3710 0.42 0.5050 0.5030 0.4550 0.4770 0.4720 0.50 0.5080 0.4570
1,1-DICHLOROETHENE 0.4010 0.44 0.4710 0.5050 0.4440 0.4460 0.4490 0.4620 0.4930 0.46
ACRYLONITRILE 0.1240 0.1630 0.1610 0.1680 0.1730 0.1710 0.1620 0.1750 0.1680 0.1770
TRANS-1,2-DICHLOROETHENE 0.2360 0.2470 0.2540 0.2570 0.2630 0.2630 0.2650 0.2580 0.28 0.2660
METHYL TERT-BUTYL ETHER 0.6450 0.62 0.7210 0.77 0.7560 0.7260 0.7460 0.7630 0.81 0.7370
1,1-DICHLOROETHANE 0.4980 0.4890 0.5540 0.5620 0.5410 0.5360 0.54 0.5270 0.5690 0.5390
DI-ISOPROPYL ETHER 1.1420 1.1270 1.1530 1.2280 1.2030 1.1830 1.23 1.22 1.2960 1.1990
2,2-DICHLOROPROPANE 0.3310 0.3340 0.2870 0.3210 0.3250 0.3230 0.3220 0.3060 0.3150 0.2910
CIS-1,2-DICHLOROETHENE 0.2320 0.2690 0.26 0.30 0.2890 0.2850 0.2860 0.2820 0.3090 0.2950
2-BUTANONE (MEK)0.2560 0.2260 0.1980 0.2120 0.2510 0.2190 0.2310 0.2420 0.2480 0.2180
CHLOROFORM 0.4820 0.5020 0.5270 0.5340 0.5230 0.5240 0.5230 0.5040 0.5510 0.5160
1,1,1-TRICHLOROETHANE 0.3710 0.4240 0.4530 0.4490 0.4310 0.4490 0.4430 0.4450 0.4730 0.4380
CARBON TETRACHLORIDE 0.45 0.4640 0.4930 0.4870 0.4320 0.4540 0.4550 0.4670 0.5080 0.4650
BENZENE 1.05 1.0040 1.0290 1.0690 1.0670 1.0570 1.0410 1.0280 1.11 1.0390
TRICHLOROETHENE 0.2640 0.3270 0.32 0.3270 0.3010 0.2950 0.3120 0.3150 0.3390 0.3190
1,2-DICHLOROPROPANE 0.3610 0.2560 0.31 0.3210 0.3320 0.3320 0.3220 0.3260 0.3580 0.3370
4-METHYL-2-PENTANONE (MIBK)1.0990 0.9620 1.0030 1.0510 1.09 1.0870 1.1080 1.06 0.9250 1.0170
TOLUENE 2.8780 2.5180 2.6780 2.6740 2.5940 2.4590 2.4080 2.2680 2.1150 2.3760
TRANS-1,3-DICHLOROPROPENE 0.6860 0.7380 0.7460 0.8540 0.8730 0.8620 0.8740 0.8720 0.8350 0.9570
1,1,2-TRICHLOROETHANE 0.5290 0.4450 0.50 0.5190 0.5520 0.5370 0.5230 0.4840 0.4610 0.5410
TETRACHLOROETHENE 0.3860 0.4870 0.5090 0.5750 0.5240 0.5230 0.5180 0.4960 0.4670 0.5240
1,3-DICHLOROPROPANE 0.8530 0.9110 0.8570 0.9160 0.8980 0.9180 0.90 0.8380 0.8030 0.9220
1,2-DIBROMOETHANE 0.4830 0.5010 0.5730 0.5740 0.5710 0.5470 0.5660 0.5360 0.5150 0.5950
CHLOROBENZENE 1.7480 1.6530 1.6390 1.6790 1.70 1.65 1.6070 1.51 1.4080 1.59
1,1,1,2-TETRACHLOROETHANE 0.5260 0.5360 0.5170 0.5570 0.5560 0.5620 0.5460 0.5260 0.4960 0.5650
ETHYLBENZENE 0.7920 0.7710 0.9050 0.8940 0.8820 0.8640 0.8640 0.8170 0.7780 0.8620
M&P-XYLENE 0.9570 0.9010 0.9770 1.0650 1.0030 0.9980 1.0210 0.9790 0.9040 1.0010
O-XYLENE 0.7480 0.7960 0.8510 0.90 0.9550 0.9230 0.9380 0.9360 0.8870 0.9920
BROMOFORM 0.5790 0.4470 0.5120 0.4450 0.4670 0.4510 0.4630 0.4760 0.4690 0.5330
ISOPROPYLBENZENE 2.0230 2.0650 2.0720 2.2770 2.34 2.3880 2.3830 2.3360 2.1460 2.2990
BROMOBENZENE 0.7480 0.6310 0.76 0.7610 0.7680 0.7410 0.7350 0.7230 0.7380 0.7780
1,1,2,2-TETRACHLOROETHANE 0.6320 0.8110 0.76 0.7730 0.7920 0.79 0.7740 0.7740 0.8130 0.87
N-PROPYLBENZENE 3.0970 2.8680 2.9680 2.9810 2.9920 3.0280 3.0050 3.0170 3.0020 3.0120
2-CHLOROTOLUENE 0.55 0.5850 0.6570 0.6970 0.6930 0.6670 0.6890 0.6810 0.69 0.7110
4-CHLOROTOLUENE 1.4480 1.7060 1.8790 2.0170 1.9560 1.9690 1.9270 1.9320 1.9680 2.0680
1,3,5-TRIMETHYLBENZENE 1.5710 1.8050 1.9630 2 1.9320 1.9880 2.0360 2.0520 2.0070 1.9730
TERT-BUTYLBENZENE 1.32 1.7030 1.4640 1.6230 1.58 1.6010 1.62 1.6470 1.6210 1.8520
1,2,4-TRIMETHYLBENZENE 1.7870 1.8560 1.8380 1.9590 1.9910 1.9970 2.0430 2.0570 2.0710 2.0790
SEC-BUTYLBENZENE 1.7250 1.8560 1.9730 2.1230 2.0350 2.0510 2.1160 2.1420 2.0710 2.0720
1,3-DICHLOROBENZENE 0.9390 1.0450 1.2370 1.2440 1.2480 1.1840 1.1890 1.1750 1.2240 1.2410
P-ISOPROPYLTOLUENE 1.4220 1.5560 1.6440 1.7350 1.8080 1.8330 1.8890 1.96 1.8950 1.89
1,4-DICHLOROBENZENE 1.4720 1.2160 1.3020 1.24 1.2860 1.2180 1.2180 1.1880 1.2220 1.2370
1,2,3-TRIMETHYLBENZENE 2.2810 1.9320 2.0860 2.0170 2 1.9950 2.0070 1.9890 1.9970 1.98
1,2-DICHLOROBENZENE 1.0690 0.9520 1.1330 1.1030 1.1050 1.0910 1.0720 1.0840 1.1330 1.1440
N-BUTYLBENZENE 1.2720 1.3910 1.3230 1.37 1.4720 1.4620 1.4950 1.5540 1.52 1.5110
1,2,4-TRICHLOROBENZENE 0.3560 0.3250 0.4070 0.37 0.4450 0.4330 0.4340 0.4680 0.4730 0.4770
1,2-DICHLOROETHANE-D4 0.3590 0.3580 0.3590 0.3580 0.3610 0.3630 0.3630 0.3790 0.4250 0.41
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 444 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS58
Analyte RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 07/19/24
04:01
07/19/24
04:20
07/19/24
04:39
07/19/24
04:58
07/19/24
05:17
07/19/24
05:36
07/19/24
05:55
07/19/24
06:14
07/19/24
06:33
07/19/24
06:52
TOLUENE-D8 2.20 2.2210 2.1970 2.1980 2.21 2.1850 2.15 2.0090 1.8060 2.0770
4-BROMOFLUOROBENZENE 0.8760 0.8670 0.8690 0.8740 0.8740 0.8720 0.8560 0.82 0.7440 0.8290
CHLOROETHANE 0.21 0.23 0.2290 0.2510 0.2320 0.2330 0.2310 0.2280 0.20
1,1,2-TRICHLOROTRIFLUOROETHANE 0.2150 0.2390 0.27 0.2270 0.2260 0.2350 0.2490 0.2580 0.2390
1,1-DICHLOROPROPENE 0.2820 0.3190 0.3430 0.3160 0.3290 0.3390 0.3530 0.3830 0.3590
1,2-DICHLOROETHANE 0.66 0.5270 0.5010 0.4590 0.4410 0.4440 0.4240 0.4640 0.4330
DIBROMOMETHANE 0.1620 0.1690 0.1940 0.1970 0.1750 0.1820 0.1820 0.1980 0.1870
BROMODICHLOROMETHANE 0.3460 0.3510 0.37 0.3820 0.3680 0.3820 0.3870 0.4250 0.4040
CIS-1,3-DICHLOROPROPENE 0.3530 0.4140 0.4250 0.4380 0.4140 0.4360 0.4510 0.4960 0.4720
CHLORODIBROMOMETHANE 0.58 0.5870 0.62 0.6370 0.6190 0.6210 0.6180 0.60 0.6910
STYRENE 1.1550 1.3230 1.4230 1.51 1.5570 1.6010 1.5970 1.5530 1.7360
1,2,3-TRICHLOROPROPANE 0.2660 0.25 0.2920 0.2890 0.2650 0.2610 0.2620 0.2690 0.2880
HEXACHLORO-1,3-BUTADIENE 0.1890 0.2120 0.2290 0.2250 0.2360 0.2180 0.2140 0.1850 0.19
1,2,3-TRICHLOROBENZENE 0.2940 0.3810 0.3210 0.39 0.3650 0.3670 0.3880 0.3960 0.3970
BROMOMETHANE 0.2430 0.2470 0.2130 0.2110 0.21 0.1950 0.1920 0.1780
ACETONE 0.1480 0.1210 0.1220 0.1130 0.1170 0.1170 0.1080 0.0960
NAPHTHALENE 1.1820 1.0470 1.2380 1.2120 1.2560 1.4890 1.6620 1.6460
1,2-DIBROMO-3-CHLOROPROPANE 0.1490 0.1860 0.1570 0.1690 0.1790 0.2020 0.2130
METHYLENE CHLORIDE 0.34 0.3010 0.28 0.2620 0.2810 0.2640
File ID:0718_07 0718_08 0718_09 0718_10 0718_11 0718_12 0718_13 0718_14 0718_15 0718_16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 445 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS58
Analyte RRF. Avg %RSD COD
Analysis date/time
DICHLORODIFLUOROMETHANE 0.335 6.12
CHLOROMETHANE 0.574 10.22
VINYL CHLORIDE 0.363 9.87
TRICHLOROFLUOROMETHANE 0.467 9.39
1,1-DICHLOROETHENE 0.457 6.41
ACRYLONITRILE 0.164 9.16
TRANS-1,2-DICHLOROETHENE 0.259 4.57
METHYL TERT-BUTYL ETHER 0.73 7.82
1,1-DICHLOROETHANE 0.535 4.74
DI-ISOPROPYL ETHER 1.198 4.17
2,2-DICHLOROPROPANE 0.315 5.12
CIS-1,2-DICHLOROETHENE 0.281 7.89
2-BUTANONE (MEK)0.23 8.18
CHLOROFORM 0.519 3.67
1,1,1-TRICHLOROETHANE 0.438 6.14
CARBON TETRACHLORIDE 0.467 4.82
BENZENE 1.049 2.75
TRICHLOROETHENE 0.312 6.81
1,2-DICHLOROPROPANE 0.326 8.96
4-METHYL-2-PENTANONE (MIBK)1.04 5.95
TOLUENE 2.497 8.88
TRANS-1,3-DICHLOROPROPENE 0.83 9.81
1,1,2-TRICHLOROETHANE 0.509 7.02
TETRACHLOROETHENE 0.501 9.84
1,3-DICHLOROPROPANE 0.882 4.66
1,2-DIBROMOETHANE 0.546 6.66
CHLOROBENZENE 1.618 6.07
1,1,1,2-TETRACHLOROETHANE 0.539 4.19
ETHYLBENZENE 0.843 5.83
M&P-XYLENE 0.981 5.12
O-XYLENE 0.893 8.42
BROMOFORM 0.484 9.01
ISOPROPYLBENZENE 2.233 6.35
BROMOBENZENE 0.738 5.59
1,1,2,2-TETRACHLOROETHANE 0.779 7.72
N-PROPYLBENZENE 2.997 1.9
2-CHLOROTOLUENE 0.662 7.95
4-CHLOROTOLUENE 1.887 9.63
1,3,5-TRIMETHYLBENZENE 1.933 7.47
TERT-BUTYLBENZENE 1.603 8.69
1,2,4-TRIMETHYLBENZENE 1.968 5.37
SEC-BUTYLBENZENE 2.016 6.56
1,3-DICHLOROBENZENE 1.173 8.7
P-ISOPROPYLTOLUENE 1.763 9.81
1,4-DICHLOROBENZENE 1.26 6.51
1,2,3-TRIMETHYLBENZENE 2.028 4.76
1,2-DICHLOROBENZENE 1.089 5.01
N-BUTYLBENZENE 1.437 6.49
1,2,4-TRICHLOROBENZENE 0.419 12.56
1,2-DICHLOROETHANE-D4 0.373 6.49
TOLUENE-D8 2.125 6.16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 446 of 530
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS58
Analyte RRF. Avg %RSD COD
Analysis date/time
4-BROMOFLUOROBENZENE 0.848 4.92
CHLOROETHANE 0.227 6.41
1,1,2-TRICHLOROTRIFLUOROETHANE 0.24 7.05
1,1-DICHLOROPROPENE 0.336 8.68
1,2-DICHLOROETHANE 0.484 15.31
DIBROMOMETHANE 0.183 6.87
BROMODICHLOROMETHANE 0.379 6.56
CIS-1,3-DICHLOROPROPENE 0.433 9.34
CHLORODIBROMOMETHANE 0.619 5.23
STYRENE 1.495 11.52
1,2,3-TRICHLOROPROPANE 0.271 5.42
HEXACHLORO-1,3-BUTADIENE 0.211 8.9
1,2,3-TRICHLOROBENZENE 0.366 9.81
BROMOMETHANE 0.211 11.26
ACETONE 0.118 12.55
NAPHTHALENE 1.342 17 0.997
1,2-DIBROMO-3-CHLOROPROPANE 0.179 12.88
METHYLENE CHLORIDE 0.288 10.08
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 447 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/10/24 11:59
Instrument ID:VOCMS21 Calibration (end) date/time:07/10/24 19:49
Lab File ID:0710_15 Analysis date/time:07/10/24 16:17
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.356705 0.36273470 1.69 40 0.0050 0.005085 102
1,1,1-TRICHLOROETHANE 0.330522 0.35839810 8.43 40 0.0050 0.005422 108
1,1,2,2-TETRACHLOROETHANE 0.522995 0.51936160 0.30 0.6950 40 0.0050 0.004965 99.30
1,1,2-TRICHLOROETHANE 0.329463 0.32695170 0.7620 40 0.0050 0.004962 99.20
1,1,2-TRICHLOROTRIFLUOROETHANE 0.162675 0.18093170 11.20 40 0.0050 0.005561 111
1,1-DICHLOROETHANE 0.385988 0.43409010 0.10 12.50 40 0.0050 0.005623 112
1,1-DICHLOROETHENE 0.142518 0.148636 4.29 20.49 0.0050 0.005215 104
1,1-DICHLOROPROPENE 0.258749 0.32180440 24.40 40 0.0050 0.006218 124
1,2,3-TRICHLOROBENZENE 0.348558 0.362058 3.87 40 0.0050 0.005194 104
1,2,3-TRICHLOROPROPANE 0.163877 0.16719290 2.02 40 0.0050 0.005101 102
1,2,3-TRIMETHYLBENZENE 1.091305 1.211123 11 40 0.0050 0.005549 111
1,2,4-TRICHLOROBENZENE 0.361999 0.38139070 5.36 40 0.0050 0.005268 105
1,2,4-TRIMETHYLBENZENE 1.096480 1.200119 9.45 40 0.0050 0.005473 109
1,2-DIBROMO-3-CHLOROPROPANE 0.171003 0.17307970 1.21 40 0.0050 0.005061 101 58 - 134
1,2-DIBROMOETHANE 0.365029 0.36834570 0.9090 40 0.0050 0.005045 101
1,2-DICHLOROBENZENE 0.623121 0.64672970 3.79 40 0.0050 0.005189 104
1,2-DICHLOROETHANE 0.316045 0.31696840 0.2920 40 0.0050 0.005015 100
1,2-DICHLOROPROPANE 0.163610 0.172925 5.69 20.49 0.0050 0.005285 106
1,3,5-TRIMETHYLBENZENE 1.063924 1.204935 13.30 40 0.0050 0.005663 113
1,3-DICHLOROBENZENE 0.642402 0.67297480 4.76 40 0.0050 0.005238 105
1,3-DICHLOROPROPANE 0.566327 0.579276 2.29 40 0.0050 0.005114 102
1,4-DICHLOROBENZENE 0.660108 0.68684440 4.05 40 0.0050 0.005203 104
2,2-DICHLOROPROPANE 0.324620 0.32519920 0.1780 40 0.0050 0.005009 100
2-BUTANONE (MEK)0.228205 0.232195 1.75 40 0.0250 0.02544 102 44 - 160
2-CHLOROTOLUENE 1.051243 1.176382 11.90 40 0.0050 0.005595 112
4-CHLOROTOLUENE 1.0228 1.111661 8.69 40 0.0050 0.005434 109
4-METHYL-2-PENTANONE (MIBK)0.732693 0.78642330 7.33 40 0.0250 0.02683 107 68 - 142
ACETONE 0.145620 0.13957880 4.15 40 0.0250 0.02396 95.80 19 - 160
ACRYLONITRILE 0.147330 0.15390370 4.46 40 0.0250 0.02612 104
BENZENE 0.721318 0.81012850 12.30 40 0.0050 0.005616 112
BROMOBENZENE 0.655581 0.67170380 2.46 40 0.0050 0.005123 102
BROMODICHLOROMETHANE 0.286859 0.29086020 1.39 40 0.0050 0.005070 101
BROMOFORM 0.383731 0.36373620 0.10 5.21 40 0.0050 0.004739 94.80
BROMOMETHANE 0.088827 0.10524620 18.50 40 0.0050 0.005924 118 10 - 160
CARBON TETRACHLORIDE 0.310829 0.34184030 9.98 40 0.0050 0.005499 110
CHLOROBENZENE 0.943604 1.012712 0.30 7.32 40 0.0050 0.005366 107
CHLORODIBROMOMETHANE 0.411313 0.41348410 0.5280 40 0.0050 0.005026 101
CHLOROETHANE 0.131980 0.14444690 9.45 40 0.0050 0.005472 109 47 - 150
CHLOROFORM 0.438880 0.42503930 3.15 20.49 0.0050 0.005402 108
CHLOROMETHANE 0.381160 0.42937570 0.10 12.60 40 0.0050 0.005632 113
CIS-1,2-DICHLOROETHENE 0.201576 0.21133150 4.84 40 0.0050 0.005242 105
CIS-1,3-DICHLOROPROPENE 0.336416 0.35206960 4.65 40 0.0050 0.005233 105
DI-ISOPROPYL ETHER 0.819005 0.886256 8.21 40 0.0050 0.005411 108
DIBROMOMETHANE 0.136665 0.14162210 3.63 40 0.0050 0.005181 104
DICHLORODIFLUOROMETHANE 0.259180 0.301602 16.40 40 0.0050 0.005818 116 51 - 149
ETHYLBENZENE 0.504132 0.54926350 8.95 20.49 0.0050 0.005448 109
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 448 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/10/24 11:59
Instrument ID:VOCMS21 Calibration (end) date/time:07/10/24 19:49
Lab File ID:0710_15 Analysis date/time:07/10/24 16:17
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
HEXACHLORO-1,3-BUTADIENE 0.182425 0.19771930 8.38 40 0.0050 0.005419 108
ISOPROPYLBENZENE 1.4189 1.414803 0.2890 40 0.0050 0.004986 99.70
M&P-XYLENE 0.586996 0.65732930 12 40 0.01 0.01120 112
METHYL TERT-BUTYL ETHER 0.573816 0.58225850 1.47 40 0.0050 0.005074 101
METHYLENE CHLORIDE 0.202966 0.20956360 3.25 40 0.0050 0.005163 103
N-BUTYLBENZENE 0.874508 0.983022 12.40 40 0.0050 0.005620 112
N-PROPYLBENZENE 1.513385 1.793734 18.50 40 0.0050 0.005926 119
NAPHTHALENE 0.980662 1.027674 4.79 40 0.0050 0.005240 105 54 - 135
O-XYLENE 0.596017 0.63454380 6.46 40 0.0050 0.005323 106
P-ISOPROPYLTOLUENE 1.045782 1.156548 10.60 40 0.0050 0.005530 111
SEC-BUTYLBENZENE 1.172023 1.362952 16.30 40 0.0050 0.005815 116
STYRENE 1.002074 1.037341 3.52 40 0.0050 0.005176 104
TERT-BUTYLBENZENE 0.862527 0.98645590 14.40 40 0.0050 0.005718 114
TETRACHLOROETHENE 0.338995 0.37265920 9.93 40 0.0050 0.005497 110
TOLUENE 1.473141 1.632221 10.80 20.49 0.0050 0.005540 111
TRANS-1,2-DICHLOROETHENE 0.176484 0.19349260 9.64 40 0.0050 0.005482 110
TRANS-1,3-DICHLOROPROPENE 0.581837 0.58048250 0.2330 40 0.0050 0.004988 99.80
TRICHLOROETHENE 0.206203 0.22981730 11.50 40 0.0050 0.005573 111
TRICHLOROFLUOROMETHANE 0.349485 0.353703 1.21 40 0.0050 0.005060 101
VINYL CHLORIDE 0.277494 0.31323410 12.90 20.49 0.0050 0.005644 113
XYLENES, TOTAL 0 0.63647990 0 40 0.0150 0.016523 110
1,2-DICHLOROETHANE-D4 0.345914 0.36494240 5.50 40 0.0160 0.01688 105 70 - 130
4-BROMOFLUOROBENZENE 0.858684 0.91992520 7.13 40 0.0160 0.01714 107 67 - 138
TOLUENE-D8 1.852796 1.963782 5.99 40 0.0160 0.01696 106 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 449 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/10/24 11:59
Instrument ID:VOCMS21 Calibration (end) date/time:07/10/24 19:49
Lab File ID:0710_17 Analysis date/time:07/10/24 17:04
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ACROLEIN 0.117573 0.07667149 34.80 20 0.0250 0.01630 65.20 10 - 160
1,2-DICHLOROETHANE-D4 0.345914 0.36458860 5.40 40 0.0160 0.01686 105 70 - 130
4-BROMOFLUOROBENZENE 0.858684 0.923559 7.56 40 0.0160 0.01721 108 67 - 138
TOLUENE-D8 1.852796 2.002678 8.09 40 0.0160 0.01729 108 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 450 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/10/24 11:59
Instrument ID:VOCMS21 Calibration (end) date/time:07/10/24 19:49
Lab File ID:0721_28 Analysis date/time:07/21/24 21:51
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.356705 0.29205570 18.10 0.0050 0.004094 81.90
1,1,1-TRICHLOROETHANE 0.330522 0.31394560 5.02 0.0050 0.004749 95
1,1,2,2-TETRACHLOROETHANE 0.522995 0.497771 0.30 4.82 0.0050 0.004759 95.20
1,1,2-TRICHLOROETHANE 0.329463 0.28910940 12.20 0.0050 0.004388 87.80
1,1,2-TRICHLOROTRIFLUOROETHANE 0.162675 0.15892260 2.31 0.0050 0.004885 97.70
1,1-DICHLOROETHANE 0.385988 0.38884480 0.10 0.74 0.0050 0.005037 101
1,1-DICHLOROETHENE 0.142518 0.14194920 0.3990 20 0.0050 0.004980 99.60
1,1-DICHLOROPROPENE 0.258749 0.256251 0.9650 0.0050 0.004952 99
1,2,3-TRICHLOROBENZENE 0.348558 0.25470140 26.90 0.0050 0.003654 73.10
1,2,3-TRICHLOROPROPANE 0.163877 0.14897920 9.09 0.0050 0.004545 90.90
1,2,3-TRIMETHYLBENZENE 1.091305 1.093154 0.1690 0.0050 0.005008 100
1,2,4-TRICHLOROBENZENE 0.361999 0.259727 28.30 0.0050 0.003587 71.70
1,2,4-TRIMETHYLBENZENE 1.096480 1.110084 1.24 0.0050 0.005062 101
1,2-DIBROMO-3-CHLOROPROPANE 0.171003 0.12363330 27.70 0.0050 0.003615 72.30
1,2-DIBROMOETHANE 0.365029 0.31669090 13.20 0.0050 0.004338 86.80
1,2-DICHLOROBENZENE 0.623121 0.52982130 15 0.0050 0.004251 85
1,2-DICHLOROETHANE 0.316045 0.31903890 0.9470 0.0050 0.005047 101
1,2-DICHLOROPROPANE 0.163610 0.17169020 4.94 20 0.0050 0.005247 105
1,3,5-TRIMETHYLBENZENE 1.063924 1.066053 0.20 0.0050 0.005010 100
1,3-DICHLOROBENZENE 0.642402 0.567802 11.60 0.0050 0.004419 88.40
1,3-DICHLOROPROPANE 0.566327 0.53215310 6.03 0.0050 0.004698 94
1,4-DICHLOROBENZENE 0.660108 0.56958970 13.70 0.0050 0.004314 86.30
2,2-DICHLOROPROPANE 0.324620 0.31280820 3.64 0.0050 0.004818 96.40
2-BUTANONE (MEK)0.228205 0.21731090 4.77 0.0250 0.02381 95.20
2-CHLOROTOLUENE 1.051243 1.050867 0.0358 0.0050 0.004998 100
4-CHLOROTOLUENE 1.0228 0.97417530 4.75 0.0050 0.004762 95.20
4-METHYL-2-PENTANONE (MIBK)0.732693 0.72582520 0.9370 0.0250 0.02477 99.10
ACETONE 0.145620 0.13590850 6.67 0.0250 0.02333 93.30
ACROLEIN 0.117573 0.122696 4.36 0.0250 0.02609 104
ACRYLONITRILE 0.147330 0.144224 2.11 0.0250 0.02447 97.90
BENZENE 0.721318 0.76436590 5.97 0.0050 0.005298 106
BROMOBENZENE 0.655581 0.65236450 0.4910 0.0050 0.004975 99.50
BROMODICHLOROMETHANE 0.286859 0.27627410 3.69 0.0050 0.004816 96.30
BROMOFORM 0.383731 0.27636280 0.10 28 0.0050 0.003601 72
BROMOMETHANE 0.088827 0.03467175 61 0.0050 0.001952 39
CARBON TETRACHLORIDE 0.310829 0.28690440 7.70 0.0050 0.004615 92.30
CHLOROBENZENE 0.943604 0.82556310 0.30 12.50 0.0050 0.004375 87.50
CHLORODIBROMOMETHANE 0.411313 0.33931020 17.50 0.0050 0.004125 82.50
CHLOROETHANE 0.131980 0.29487240 123 0.0050 0.01117 223
CHLOROFORM 0.438880 0.39000720 11.10 20 0.0050 0.004921 98.40 80 - 120
CHLOROMETHANE 0.381160 0.34033690 0.10 10.70 0.0050 0.004464 89.30
CIS-1,2-DICHLOROETHENE 0.201576 0.19318190 4.16 0.0050 0.004792 95.80
CIS-1,3-DICHLOROPROPENE 0.336416 0.33545610 0.2850 0.0050 0.004986 99.70
DI-ISOPROPYL ETHER 0.819005 0.90272170 10.20 0.0050 0.005511 110
DIBROMOMETHANE 0.136665 0.13265010 2.94 0.0050 0.004853 97.10
DICHLORODIFLUOROMETHANE 0.259180 0.21984820 15.20 0.0050 0.004241 84.80
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 451 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/10/24 11:59
Instrument ID:VOCMS21 Calibration (end) date/time:07/10/24 19:49
Lab File ID:0721_28 Analysis date/time:07/21/24 21:51
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.504132 0.45515660 9.71 20 0.0050 0.004514 90.30
HEXACHLORO-1,3-BUTADIENE 0.182425 0.13200560 27.60 0.0050 0.003618 72.40
ISOPROPYLBENZENE 1.4189 1.274083 10.20 0.0050 0.004490 89.80
M&P-XYLENE 0.586996 0.53452050 8.94 0.01 0.009106 91.10
METHYL TERT-BUTYL ETHER 0.573816 0.59479430 3.66 0.0050 0.005183 104
METHYLENE CHLORIDE 0.202966 0.19881260 2.05 0.0050 0.004898 98
N-BUTYLBENZENE 0.874508 0.82250330 5.95 0.0050 0.004703 94.10
N-PROPYLBENZENE 1.513385 1.568064 3.61 0.0050 0.005181 104
NAPHTHALENE 0.980662 0.88352970 9.90 0.0050 0.004505 90.10
O-XYLENE 0.596017 0.52997180 11.10 0.0050 0.004446 88.90
P-ISOPROPYLTOLUENE 1.045782 0.98496770 5.82 0.0050 0.004709 94.20
SEC-BUTYLBENZENE 1.172023 1.132072 3.41 0.0050 0.004830 96.60
STYRENE 1.002074 0.82077660 18.10 0.0050 0.004095 81.90
TERT-BUTYLBENZENE 0.862527 0.83627190 3.04 0.0050 0.004848 97
TETRACHLOROETHENE 0.338995 0.257982 23.90 0.0050 0.003805 76.10
TOLUENE 1.473141 1.366783 7.22 20 0.0050 0.004639 92.80
TRANS-1,2-DICHLOROETHENE 0.176484 0.18075810 2.42 0.0050 0.005121 102
TRANS-1,3-DICHLOROPROPENE 0.581837 0.54133320 6.96 0.0050 0.004652 93
TRICHLOROETHENE 0.206203 0.19176950 7 0.0050 0.004650 93
TRICHLOROFLUOROMETHANE 0.349485 0.331219 5.23 0.0050 0.004739 94.80
VINYL CHLORIDE 0.277494 0.29397870 5.94 20 0.0050 0.005297 106
XYLENES, TOTAL 0 0.56206050 0 0.0150 0.013552 90.30
1,2-DICHLOROETHANE-D4 0.345914 0.37691780 8.96 0.0160 0.01743 109 70 - 130
4-BROMOFLUOROBENZENE 0.858684 0.94618480 10.20 0.0160 0.01763 110 70 - 130
TOLUENE-D8 1.852796 1.888483 1.93 0.0160 0.01631 102 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 452 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0708_22 Analysis date/time:07/08/24 23:37
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5850 0.53945150 7.79 40 0.0050 0.005356 107
1,1,1-TRICHLOROETHANE 0.3830 0.40841850 6.64 40 0.0050 0.005327 107
1,1,2,2-TETRACHLOROETHANE 1.11 1.103447 0.30 0.59 40 0.0050 0.004972 99.40
1,1,2-TRICHLOROETHANE 0.5640 0.53093760 5.86 40 0.0050 0.004704 94.10
1,1,2-TRICHLOROTRIFLUOROETHANE 0.2510 0.24654080 1.78 40 0.0050 0.004908 98.20
1,1-DICHLOROETHANE 0.50 0.50118290 0.10 0.2370 40 0.0050 0.005016 100
1,1-DICHLOROETHENE 0.4410 0.42874110 2.78 20.49 0.0050 0.004864 97.30
1,1-DICHLOROPROPENE 0.3350 0.38067450 13.60 40 0.0050 0.005674 113
1,2,3-TRICHLOROBENZENE 0.3170 0.28783090 9.20 40 0.0050 0.004540 90.80
1,2,3-TRICHLOROPROPANE 0.3920 0.366128 6.60 40 0.0050 0.004667 93.30
1,2,3-TRIMETHYLBENZENE 2.4640 2.345124 4.82 40 0.0050 0.004759 95.20
1,2,4-TRICHLOROBENZENE 0.3630 0.34294350 5.53 40 0.0050 0.004725 94.50
1,2,4-TRIMETHYLBENZENE 2.4220 2.488166 2.73 40 0.0050 0.005138 103
1,2-DIBROMO-3-CHLOROPROPANE 0.2280 0.21696330 4.84 40 0.0050 0.004767 95.30 58 - 134
1,2-DIBROMOETHANE 0.6340 0.60198870 5.05 40 0.0050 0.004745 94.90
1,2-DICHLOROBENZENE 1.1590 1.127929 2.68 40 0.0050 0.004865 97.30
1,2-DICHLOROETHANE 0.4010 0.36368670 9.31 40 0.0050 0.004536 90.70
1,2-DICHLOROPROPANE 0.3050 0.27713660 9.14 20.49 0.0050 0.004543 90.90
1,3,5-TRIMETHYLBENZENE 2.5160 2.562206 1.84 40 0.0050 0.005092 102
1,3-DICHLOROBENZENE 1.2680 1.264841 0.2490 40 0.0050 0.004987 99.70
1,3-DICHLOROPROPANE 0.98 0.91405110 6.73 40 0.0050 0.004665 93.30
1,4-DICHLOROBENZENE 1.3720 1.285638 6.29 40 0.0050 0.004686 93.70
2,2-DICHLOROPROPANE 0.2920 0.29832920 2.17 40 0.0050 0.005115 102
2-BUTANONE (MEK)0.1280 0.13650210 6.64 40 0.0250 0.02669 107 44 - 160
2-CHLOROTOLUENE 0.8190 0.78914980 3.64 40 0.0050 0.004816 96.30
4-CHLOROTOLUENE 2.3210 2.353380 1.40 40 0.0050 0.005070 101
4-METHYL-2-PENTANONE (MIBK)0.8170 0.81159540 0.6620 40 0.0250 0.02482 99.30 68 - 142
ACETONE 0.0570 0.04683598 17.80 40 0.0250 0.02200 88 19 - 160
ACRYLONITRILE 0.1210 0.12372630 2.25 40 0.0250 0.02552 102
BENZENE 1.0920 1.016872 6.88 40 0.0050 0.004655 93.10
BROMOBENZENE 0.8710 0.88160130 1.22 40 0.0050 0.005060 101
BROMODICHLOROMETHANE 0.3410 0.33566050 1.57 40 0.0050 0.004925 98.50
BROMOFORM 0.4090 0.37921640 0.10 7.28 40 0.0050 0.004636 92.70
BROMOMETHANE 0.1690 0.18881170 11.70 40 0.0050 0.005594 112 10 - 160
CARBON TETRACHLORIDE 0.4010 0.39403340 1.74 40 0.0050 0.004917 98.30
CHLOROBENZENE 1.6840 1.570503 0.30 6.74 40 0.0050 0.004663 93.30
CHLORODIBROMOMETHANE 0.6440 0.58856330 8.61 40 0.0050 0.004567 91.30
CHLOROETHANE 0.1960 0.19397950 1.03 40 0.0050 0.004954 99.10 47 - 150
CHLOROFORM 0.5390 0.50001390 7.23 20.49 0.0050 0.004638 92.80
CHLOROMETHANE 0.4950 0.45865050 0.10 7.34 40 0.0050 0.004629 92.60
CIS-1,2-DICHLOROETHENE 0.2960 0.30222410 2.10 40 0.0050 0.005101 102
CIS-1,3-DICHLOROPROPENE 0.4030 0.38989660 3.25 40 0.0050 0.004835 96.70
DI-ISOPROPYL ETHER 0.7990 0.802808 0.4770 40 0.0050 0.005024 100
DIBROMOMETHANE 0.1690 0.16581590 1.88 40 0.0050 0.004899 98
DICHLORODIFLUOROMETHANE 0.33 0.33987550 2.99 40 0.0050 0.005144 103 51 - 149
ETHYLBENZENE 0.8880 0.86589210 2.49 20.49 0.0050 0.004878 97.60
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 453 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0708_22 Analysis date/time:07/08/24 23:37
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
HEXACHLORO-1,3-BUTADIENE 0.1770 0.20979710 18.50 40 0.0050 0.005916 118
ISOPROPYLBENZENE 2.4070 2.197937 8.69 40 0.0050 0.004567 91.30
M&P-XYLENE 1.0610 1.043711 1.63 40 0.01 0.009837 98.40
METHYL TERT-BUTYL ETHER 0.6820 0.69397340 1.76 40 0.0050 0.005087 102
METHYLENE CHLORIDE 0.30 0.26592170 11.40 40 0.0050 0.004425 88.50
N-BUTYLBENZENE 1.6540 1.774770 7.30 40 0.0050 0.005364 107
N-PROPYLBENZENE 3.5680 3.894173 9.14 40 0.0050 0.005457 109
NAPHTHALENE 1.4920 1.289235 13.60 40 0.0050 0.003703 74.10 54 - 135
O-XYLENE 1.0560 0.99115590 6.14 40 0.0050 0.004692 93.80
P-ISOPROPYLTOLUENE 2.22 2.288885 3.10 40 0.0050 0.005154 103
SEC-BUTYLBENZENE 2.7790 2.899163 4.32 40 0.0050 0.005216 104
STYRENE 1.7720 1.644408 7.20 40 0.0050 0.004640 92.80
TERT-BUTYLBENZENE 2.0670 2.111833 2.17 40 0.0050 0.005108 102
TETRACHLOROETHENE 0.49 0.49382010 0.78 40 0.0050 0.005040 101
TOLUENE 2.6040 2.521890 3.15 20.49 0.0050 0.004843 96.90
TRANS-1,2-DICHLOROETHENE 0.2570 0.25979970 1.09 40 0.0050 0.005046 101
TRANS-1,3-DICHLOROPROPENE 0.9150 0.89071490 2.65 40 0.0050 0.004865 97.30
TRICHLOROETHENE 0.2560 0.27875190 8.89 40 0.0050 0.005055 101
TRICHLOROFLUOROMETHANE 0.3410 0.36653260 7.49 40 0.0050 0.004519 90.40
VINYL CHLORIDE 0.3410 0.32549140 4.55 20.49 0.0050 0.004771 95.40
1,2-DICHLOROETHANE-D4 0.32 0.32418020 1.31 40 0.0160 0.01619 101 70 - 130
4-BROMOFLUOROBENZENE 0.8330 0.860027 3.24 40 0.0160 0.01652 103 67 - 138
TOLUENE-D8 2.3020 2.307253 0.2280 40 0.0160 0.01604 100 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 454 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0708_23 Analysis date/time:07/08/24 23:56
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,2-DICHLOROETHANE 0.4010 0.004025985
0 99 20 0.0050 0.00005000 1
4-METHYL-2-PENTANONE (MIBK)0.8170 0.0028163190 99.70 20 0.0250 0.00008600 0.3440 68 - 142
ACROLEIN 0.0560 0.02440697 56.40 40 0.0250 0.008482 33.90 10 - 160
1,2-DICHLOROETHANE-D4 0.32 0.32404030 1.26 40 0.0160 0.01618 101 70 - 130
4-BROMOFLUOROBENZENE 0.8330 0.86035320 3.28 40 0.0160 0.01652 103 67 - 138
TOLUENE-D8 2.3020 2.328748 1.16 40 0.0160 0.01619 101 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 455 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0724A_03 Analysis date/time:07/24/24 20:32
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5850 0.57451080 1.79 0.0050 0.005709 114
1,1,1-TRICHLOROETHANE 0.3830 0.43295930 13 0.0050 0.005647 113
1,1,2,2-TETRACHLOROETHANE 1.11 1.1320 0.30 1.98 0.0050 0.005101 102
1,1,2-TRICHLOROETHANE 0.5640 0.576016 2.13 0.0050 0.005104 102
1,1,2-TRICHLOROTRIFLUOROETHANE 0.2510 0.21366540 14.90 0.0050 0.004254 85.10
1,1-DICHLOROETHANE 0.50 0.49752130 0.10 0.4960 0.0050 0.004979 99.60
1,1-DICHLOROETHENE 0.4410 0.39835680 9.67 20 0.0050 0.004520 90.40
1,1-DICHLOROPROPENE 0.3350 0.33219190 0.8380 0.0050 0.004952 99
1,2,3-TRICHLOROBENZENE 0.3170 0.40831380 28.80 0.0050 0.006440 129
1,2,3-TRICHLOROPROPANE 0.3920 0.36242410 7.54 0.0050 0.004619 92.40
1,2,3-TRIMETHYLBENZENE 2.4640 2.169902 11.90 0.0050 0.004403 88.10
1,2,4-TRICHLOROBENZENE 0.3630 0.39556770 8.97 0.0050 0.005451 109
1,2,4-TRIMETHYLBENZENE 2.4220 2.216932 8.47 0.0050 0.004577 91.50
1,2-DIBROMO-3-CHLOROPROPANE 0.2280 0.28290020 24.10 0.0050 0.006216 124
1,2-DIBROMOETHANE 0.6340 0.64211080 1.28 0.0050 0.005061 101
1,2-DICHLOROBENZENE 1.1590 1.204176 3.90 0.0050 0.005194 104
1,2-DICHLOROETHANE 0.4010 0.39833710 0.6640 0.0050 0.004969 99.40
1,2-DICHLOROPROPANE 0.3050 0.30826060 1.07 20 0.0050 0.005053 101
1,3,5-TRIMETHYLBENZENE 2.5160 2.327067 7.51 0.0050 0.004625 92.50
1,3-DICHLOROBENZENE 1.2680 1.223015 3.55 0.0050 0.004822 96.40
1,3-DICHLOROPROPANE 0.98 0.95488060 2.56 0.0050 0.004873 97.50
1,4-DICHLOROBENZENE 1.3720 1.286414 6.24 0.0050 0.004689 93.80
2,2-DICHLOROPROPANE 0.2920 0.25561520 12.50 0.0050 0.004382 87.60
2-BUTANONE (MEK)0.1280 0.13179260 2.96 0.0250 0.02577 103
2-CHLOROTOLUENE 0.8190 0.74840910 8.62 0.0050 0.004567 91.30
4-CHLOROTOLUENE 2.3210 2.193934 5.47 0.0050 0.004727 94.50
4-METHYL-2-PENTANONE (MIBK)0.8170 0.97153130 18.90 0.0250 0.02971 119
ACETONE 0.0570 0.04528520 20.60 0.0250 0.02125 85
ACROLEIN 0.0560 0.11496210 105 0.0250 0.03784 151
ACRYLONITRILE 0.1210 0.16610270 37.30 0.0250 0.03426 137
BENZENE 1.0920 1.012352 7.29 0.0050 0.004634 92.70
BROMOBENZENE 0.8710 0.86970120 0.1490 0.0050 0.004991 99.80
BROMODICHLOROMETHANE 0.3410 0.37832360 10.90 0.0050 0.005551 111
BROMOFORM 0.4090 0.52210960 0.10 27.70 0.0050 0.006382 128
BROMOMETHANE 0.1690 0.19018310 12.50 0.0050 0.005635 113
CARBON TETRACHLORIDE 0.4010 0.445509 11.10 0.0050 0.005560 111
CHLOROBENZENE 1.6840 1.608834 0.30 4.46 0.0050 0.004776 95.50
CHLORODIBROMOMETHANE 0.6440 0.67916590 5.46 0.0050 0.005270 105
CHLOROETHANE 0.1960 0.26598460 35.70 0.0050 0.006793 136
CHLOROFORM 0.5390 0.50486270 6.33 20 0.0050 0.004683 93.70
CHLOROMETHANE 0.4950 0.44556330 0.10 9.99 0.0050 0.004497 89.90
CIS-1,2-DICHLOROETHENE 0.2960 0.29249210 1.19 0.0050 0.004937 98.70
CIS-1,3-DICHLOROPROPENE 0.4030 0.43473780 7.88 0.0050 0.005391 108
DI-ISOPROPYL ETHER 0.7990 0.92351420 15.60 0.0050 0.005780 116
DIBROMOMETHANE 0.1690 0.17653820 4.46 0.0050 0.005216 104
DICHLORODIFLUOROMETHANE 0.33 0.33727310 2.20 0.0050 0.005105 102
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 456 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0724A_03 Analysis date/time:07/24/24 20:32
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.8880 0.84061120 5.34 20 0.0050 0.004736 94.70
HEXACHLORO-1,3-BUTADIENE 0.1770 0.18563740 4.88 0.0050 0.005235 105
ISOPROPYLBENZENE 2.4070 2.391207 0.6560 0.0050 0.004968 99.40
M&P-XYLENE 1.0610 1.019120 3.95 0.01 0.009605 96.10
METHYL TERT-BUTYL ETHER 0.6820 0.80817710 18.50 0.0050 0.005924 118
METHYLENE CHLORIDE 0.30 0.26662370 11.10 0.0050 0.004437 88.70
N-BUTYLBENZENE 1.6540 1.347021 18.60 0.0050 0.004071 81.40
N-PROPYLBENZENE 3.5680 3.233374 9.38 0.0050 0.004531 90.60
NAPHTHALENE 1.4920 1.812811 21.50 0.0050 0.005139 103
O-XYLENE 1.0560 0.985092 6.71 0.0050 0.004663 93.30
P-ISOPROPYLTOLUENE 2.22 1.941379 12.60 0.0050 0.004372 87.40
SEC-BUTYLBENZENE 2.7790 2.313658 16.70 0.0050 0.004163 83.30
STYRENE 1.7720 1.679753 5.21 0.0050 0.004739 94.80
TERT-BUTYLBENZENE 2.0670 1.859849 10 0.0050 0.004498 90
TETRACHLOROETHENE 0.49 0.509509 3.98 0.0050 0.005200 104
TOLUENE 2.6040 2.468082 5.22 20 0.0050 0.004739 94.80
TRANS-1,2-DICHLOROETHENE 0.2570 0.26118040 1.63 0.0050 0.005073 101
TRANS-1,3-DICHLOROPROPENE 0.9150 0.93530070 2.22 0.0050 0.005108 102
TRICHLOROETHENE 0.2560 0.28544190 11.50 0.0050 0.005176 104
TRICHLOROFLUOROMETHANE 0.3410 0.35269920 3.43 0.0050 0.004352 87
VINYL CHLORIDE 0.3410 0.279609 18 20 0.0050 0.004099 82
1,2-DICHLOROETHANE-D4 0.32 0.32318710 0.9960 0.0160 0.01614 101 70 - 130
4-BROMOFLUOROBENZENE 0.8330 0.86085240 3.34 0.0160 0.01653 103 70 - 130
TOLUENE-D8 2.3020 2.2523 2.16 0.0160 0.01566 97.90 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 457 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0725_03 Analysis date/time:07/25/24 07:27
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5850 0.54101530 7.52 0.0050 0.005371 107
1,1,1-TRICHLOROETHANE 0.3830 0.42326480 10.50 0.0050 0.005521 110
1,1,2,2-TETRACHLOROETHANE 1.11 1.111728 0.30 0.1560 0.0050 0.005009 100
1,1,2-TRICHLOROETHANE 0.5640 0.56649630 0.4430 0.0050 0.005019 100
1,1,2-TRICHLOROTRIFLUOROETHANE 0.2510 0.23455350 6.55 0.0050 0.004670 93.40
1,1-DICHLOROETHANE 0.50 0.48081910 0.10 3.84 0.0050 0.004812 96.20
1,1-DICHLOROETHENE 0.4410 0.403317 8.54 20 0.0050 0.004576 91.50
1,1-DICHLOROPROPENE 0.3350 0.31473570 6.05 0.0050 0.004692 93.80
1,2,3-TRICHLOROBENZENE 0.3170 0.30479150 3.85 0.0050 0.004808 96.20
1,2,3-TRICHLOROPROPANE 0.3920 0.34785230 11.30 0.0050 0.004434 88.70
1,2,3-TRIMETHYLBENZENE 2.4640 2.078373 15.70 0.0050 0.004217 84.30
1,2,4-TRICHLOROBENZENE 0.3630 0.33856080 6.73 0.0050 0.004665 93.30
1,2,4-TRIMETHYLBENZENE 2.4220 2.174794 10.20 0.0050 0.004490 89.80
1,2-DIBROMO-3-CHLOROPROPANE 0.2280 0.24368780 6.88 0.0050 0.005355 107
1,2-DIBROMOETHANE 0.6340 0.60682340 4.29 0.0050 0.004783 95.70
1,2-DICHLOROBENZENE 1.1590 1.044446 9.88 0.0050 0.004505 90.10
1,2-DICHLOROETHANE 0.4010 0.38528220 3.92 0.0050 0.004806 96.10
1,2-DICHLOROPROPANE 0.3050 0.30351620 0.4860 20 0.0050 0.004975 99.50
1,3,5-TRIMETHYLBENZENE 2.5160 2.256637 10.30 0.0050 0.004485 89.70
1,3-DICHLOROBENZENE 1.2680 1.161593 8.39 0.0050 0.004580 91.60
1,3-DICHLOROPROPANE 0.98 0.94112440 3.97 0.0050 0.004803 96.10
1,4-DICHLOROBENZENE 1.3720 1.247912 9.04 0.0050 0.004548 91
2,2-DICHLOROPROPANE 0.2920 0.27230660 6.74 0.0050 0.004669 93.40
2-BUTANONE (MEK)0.1280 0.17616210 37.60 0.0250 0.03444 138
2-CHLOROTOLUENE 0.8190 0.73146150 10.70 0.0050 0.004464 89.30
4-CHLOROTOLUENE 2.3210 2.008935 13.40 0.0050 0.004328 86.60
4-METHYL-2-PENTANONE (MIBK)0.8170 0.989564 21.10 0.0250 0.03026 121
ACETONE 0.0570 0.05046931 11.50 0.0250 0.02373 94.90
ACROLEIN 0.0560 0.11589750 107 0.0250 0.03814 153
ACRYLONITRILE 0.1210 0.16599660 37.20 0.0250 0.03423 137
BENZENE 1.0920 0.993064 9.06 0.0050 0.004546 90.90
BROMOBENZENE 0.8710 0.84592210 2.88 0.0050 0.004855 97.10
BROMODICHLOROMETHANE 0.3410 0.360425 5.70 0.0050 0.005289 106
BROMOFORM 0.4090 0.47612820 0.10 16.40 0.0050 0.005820 116
BROMOMETHANE 0.1690 0.16215470 4.05 0.0050 0.004805 96.10
CARBON TETRACHLORIDE 0.4010 0.41113180 2.53 0.0050 0.005131 103
CHLOROBENZENE 1.6840 1.544131 0.30 8.31 0.0050 0.004584 91.70
CHLORODIBROMOMETHANE 0.6440 0.62614380 2.77 0.0050 0.004859 97.20
CHLOROETHANE 0.1960 0.22668140 15.70 0.0050 0.005789 116
CHLOROFORM 0.5390 0.48251010 10.50 20 0.0050 0.004476 89.50
CHLOROMETHANE 0.4950 0.36411040 0.10 26.40 0.0050 0.003675 73.50
CIS-1,2-DICHLOROETHENE 0.2960 0.28370540 4.15 0.0050 0.004789 95.80
CIS-1,3-DICHLOROPROPENE 0.4030 0.41811210 3.75 0.0050 0.005185 104
DI-ISOPROPYL ETHER 0.7990 0.96686390 21 0.0050 0.006051 121
DIBROMOMETHANE 0.1690 0.17549060 3.84 0.0050 0.005185 104
DICHLORODIFLUOROMETHANE 0.33 0.26980290 18.20 0.0050 0.004084 81.70
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 458 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/08/24 19:30
Instrument ID:VOCMS56 Calibration (end) date/time:07/08/24 22:21
Lab File ID:0725_03 Analysis date/time:07/25/24 07:27
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.8880 0.81868410 7.81 20 0.0050 0.004612 92.20
HEXACHLORO-1,3-BUTADIENE 0.1770 0.15647640 11.60 0.0050 0.004412 88.20
ISOPROPYLBENZENE 2.4070 2.247827 6.61 0.0050 0.004670 93.40
M&P-XYLENE 1.0610 0.983908 7.27 0.01 0.009273 92.70
METHYL TERT-BUTYL ETHER 0.6820 0.74292730 8.93 0.0050 0.005445 109
METHYLENE CHLORIDE 0.30 0.25670190 14.40 0.0050 0.004272 85.40
N-BUTYLBENZENE 1.6540 1.289756 22 0.0050 0.003898 78
N-PROPYLBENZENE 3.5680 3.300198 7.51 0.0050 0.004624 92.50
NAPHTHALENE 1.4920 1.451304 2.73 0.0050 0.004147 82.90
O-XYLENE 1.0560 0.93599720 11.40 0.0050 0.004431 88.60
P-ISOPROPYLTOLUENE 2.22 1.885116 15.10 0.0050 0.004245 84.90
SEC-BUTYLBENZENE 2.7790 2.250580 19 0.0050 0.004049 81
STYRENE 1.7720 1.583426 10.60 0.0050 0.004468 89.40
TERT-BUTYLBENZENE 2.0670 1.780430 13.90 0.0050 0.004306 86.10
TETRACHLOROETHENE 0.49 0.49347040 0.7080 0.0050 0.005036 101
TOLUENE 2.6040 2.379417 8.62 20 0.0050 0.004569 91.40
TRANS-1,2-DICHLOROETHENE 0.2570 0.25268460 1.68 0.0050 0.004908 98.20
TRANS-1,3-DICHLOROPROPENE 0.9150 0.91269610 0.2520 0.0050 0.004985 99.70
TRICHLOROETHENE 0.2560 0.27827550 8.70 0.0050 0.005047 101
TRICHLOROFLUOROMETHANE 0.3410 0.37365940 9.58 0.0050 0.004605 92.10
VINYL CHLORIDE 0.3410 0.34207430 0.3150 20 0.0050 0.005014 100
1,2-DICHLOROETHANE-D4 0.32 0.31515190 1.52 0.0160 0.01574 98.40 70 - 130
4-BROMOFLUOROBENZENE 0.8330 0.84576950 1.53 0.0160 0.01624 102 70 - 130
TOLUENE-D8 2.3020 2.275784 1.14 0.0160 0.01582 98.90 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 459 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/19/24 04:01
Instrument ID:VOCMS58 Calibration (end) date/time:07/19/24 06:52
Lab File ID:0718_21 Analysis date/time:07/19/24 08:27
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5390 0.604007 12.10 40 0.0050 0.005608 112
1,1,1-TRICHLOROETHANE 0.4380 0.49543440 13.10 40 0.0050 0.005661 113
1,1,2,2-TETRACHLOROETHANE 0.7790 0.828221 0.30 6.32 40 0.0050 0.005317 106
1,1,2-TRICHLOROETHANE 0.5090 0.572159 12.40 40 0.0050 0.005619 112
1,1,2-TRICHLOROTRIFLUOROETHANE 0.24 0.27083560 12.80 40 0.0050 0.005649 113
1,1-DICHLOROETHANE 0.5350 0.59790010 0.10 11.80 40 0.0050 0.005584 112
1,1-DICHLOROETHENE 0.4570 0.49594860 8.52 20.49 0.0050 0.005424 108
1,1-DICHLOROPROPENE 0.3360 0.427134 27.10 40 0.0050 0.006358 127
1,2,3-TRICHLOROBENZENE 0.3660 0.38123880 4.16 40 0.0050 0.005204 104
1,2,3-TRICHLOROPROPANE 0.2710 0.28861130 6.50 40 0.0050 0.005320 106
1,2,3-TRIMETHYLBENZENE 2.0280 2.137198 5.38 40 0.0050 0.005268 105
1,2,4-TRICHLOROBENZENE 0.4190 0.47688130 13.80 40 0.0050 0.005695 114
1,2,4-TRIMETHYLBENZENE 1.9680 2.169996 10.30 40 0.0050 0.005514 110
1,2-DIBROMO-3-CHLOROPROPANE 0.1790 0.17601010 1.67 40 0.0050 0.004910 98.20 58 - 134
1,2-DIBROMOETHANE 0.5460 0.61417390 12.50 40 0.0050 0.005624 112
1,2-DICHLOROBENZENE 1.0890 1.159229 6.45 40 0.0050 0.005324 106
1,2-DICHLOROETHANE 0.4840 0.45113490 6.79 40 0.0050 0.004663 93.30
1,2-DICHLOROPROPANE 0.3260 0.34265060 5.11 20.49 0.0050 0.005262 105
1,3,5-TRIMETHYLBENZENE 1.9330 2.207284 14.20 40 0.0050 0.005710 114
1,3-DICHLOROBENZENE 1.1730 1.293150 10.20 40 0.0050 0.005514 110
1,3-DICHLOROPROPANE 0.8820 0.98264010 11.40 40 0.0050 0.005573 111
1,4-DICHLOROBENZENE 1.26 1.321468 4.88 40 0.0050 0.005245 105
2,2-DICHLOROPROPANE 0.3150 0.35262560 11.90 40 0.0050 0.005589 112
2-BUTANONE (MEK)0.23 0.24039890 4.52 40 0.0250 0.02613 105 44 - 160
2-CHLOROTOLUENE 0.6620 0.73784480 11.50 40 0.0050 0.005572 111
4-CHLOROTOLUENE 1.8870 2.123009 12.50 40 0.0050 0.005625 113
4-METHYL-2-PENTANONE (MIBK)1.04 1.146875 10.30 40 0.0250 0.02756 110 68 - 142
ACETONE 0.1180 0.12099730 2.54 40 0.0250 0.02567 103 19 - 160
ACRYLONITRILE 0.1640 0.18039080 9.99 40 0.0250 0.02747 110
BENZENE 1.0490 1.137675 8.45 40 0.0050 0.005420 108
BROMOBENZENE 0.7380 0.79515330 7.74 40 0.0050 0.005385 108
BROMODICHLOROMETHANE 0.3790 0.39658110 4.64 40 0.0050 0.005226 105
BROMOFORM 0.4840 0.50370610 0.10 4.07 40 0.0050 0.005199 104
BROMOMETHANE 0.2110 0.20280070 3.89 40 0.0050 0.004801 96 10 - 160
CARBON TETRACHLORIDE 0.4670 0.50868570 8.93 40 0.0050 0.005441 109
CHLOROBENZENE 1.6180 1.779320 0.30 9.97 40 0.0050 0.005497 110
CHLORODIBROMOMETHANE 0.6190 0.68340750 10.40 40 0.0050 0.005518 110
CHLOROETHANE 0.2270 0.24109950 6.21 40 0.0050 0.005308 106 47 - 150
CHLOROFORM 0.5190 0.55747620 7.41 20.49 0.0050 0.005373 107
CHLOROMETHANE 0.5740 0.52081080 0.10 9.27 40 0.0050 0.004537 90.70
CIS-1,2-DICHLOROETHENE 0.2810 0.30877540 9.88 40 0.0050 0.005496 110
CIS-1,3-DICHLOROPROPENE 0.4330 0.47058450 8.68 40 0.0050 0.005434 109
DI-ISOPROPYL ETHER 1.1980 1.274574 6.39 40 0.0050 0.005319 106
DIBROMOMETHANE 0.1830 0.18876160 3.15 40 0.0050 0.005161 103
DICHLORODIFLUOROMETHANE 0.3350 0.33189770 0.9260 40 0.0050 0.004955 99.10 51 - 149
ETHYLBENZENE 0.8430 0.95611830 13.40 20.49 0.0050 0.005671 113
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 460 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/19/24 04:01
Instrument ID:VOCMS58 Calibration (end) date/time:07/19/24 06:52
Lab File ID:0718_21 Analysis date/time:07/19/24 08:27
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
HEXACHLORO-1,3-BUTADIENE 0.2110 0.25112930 19 40 0.0050 0.005955 119
ISOPROPYLBENZENE 2.2330 2.354025 5.42 40 0.0050 0.005271 105
M&P-XYLENE 0.9810 1.137919 16 40 0.01 0.01160 116
METHYL TERT-BUTYL ETHER 0.73 0.78698590 7.81 40 0.0050 0.005394 108
METHYLENE CHLORIDE 0.2880 0.29303260 1.75 40 0.0050 0.005084 102
N-BUTYLBENZENE 1.4370 1.667489 16 40 0.0050 0.005801 116
N-PROPYLBENZENE 2.9970 3.333146 11.20 40 0.0050 0.005561 111
NAPHTHALENE 1.3420 1.348473 0.4820 40 0.0050 0.004307 86.10 54 - 135
O-XYLENE 0.8930 1.065113 19.30 40 0.0050 0.005966 119
P-ISOPROPYLTOLUENE 1.7630 2.033859 15.40 40 0.0050 0.005768 115
SEC-BUTYLBENZENE 2.0160 2.319975 15.10 40 0.0050 0.005753 115
STYRENE 1.4950 1.765101 18.10 40 0.0050 0.005903 118
TERT-BUTYLBENZENE 1.6030 1.822138 13.70 40 0.0050 0.005683 114
TETRACHLOROETHENE 0.5010 0.57999920 15.80 40 0.0050 0.005789 116
TOLUENE 2.4970 2.674930 7.13 20.49 0.0050 0.005357 107
TRANS-1,2-DICHLOROETHENE 0.2590 0.28435150 9.79 40 0.0050 0.005493 110
TRANS-1,3-DICHLOROPROPENE 0.83 0.96190550 15.90 40 0.0050 0.005798 116
TRICHLOROETHENE 0.3120 0.33361320 6.93 40 0.0050 0.005346 107
TRICHLOROFLUOROMETHANE 0.4670 0.49639780 6.30 40 0.0050 0.005316 106
VINYL CHLORIDE 0.3630 0.39198370 7.98 20.49 0.0050 0.005399 108
1,2-DICHLOROETHANE-D4 0.3730 0.36020540 3.43 40 0.0160 0.01543 96.40 70 - 130
4-BROMOFLUOROBENZENE 0.8480 0.87541120 3.23 40 0.0160 0.01652 103 67 - 138
TOLUENE-D8 2.1250 2.177665 2.48 40 0.0160 0.01639 102 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 461 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/19/24 04:01
Instrument ID:VOCMS58 Calibration (end) date/time:07/19/24 06:52
Lab File ID:0718_23 Analysis date/time:07/19/24 09:05
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ACROLEIN 0.0370 0.03572148 3.46 40 0.0250 0.02796 112 10 - 160
1,2-DICHLOROETHANE-D4 0.3730 0.35682570 4.34 40 0.0160 0.01529 95.60 70 - 130
4-BROMOFLUOROBENZENE 0.8480 0.87157920 2.78 40 0.0160 0.01644 103 67 - 138
TOLUENE-D8 2.1250 2.225692 4.74 40 0.0160 0.01675 105 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 462 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/19/24 04:01
Instrument ID:VOCMS58 Calibration (end) date/time:07/19/24 06:52
Lab File ID:0725_29 Analysis date/time:07/25/24 08:30
Analytical Method:8260B Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5390 0.53661870 0.4420 0.0050 0.004982 99.60
1,1,1-TRICHLOROETHANE 0.4380 0.42983090 1.87 0.0050 0.004912 98.20
1,1,2,2-TETRACHLOROETHANE 0.7790 0.76215740 0.30 2.16 0.0050 0.004893 97.90
1,1,2-TRICHLOROETHANE 0.5090 0.50719450 0.3550 0.0050 0.004981 99.60
1,1,2-TRICHLOROTRIFLUOROETHANE 0.24 0.22870870 4.70 0.0050 0.004770 95.40
1,1-DICHLOROETHANE 0.5350 0.51587740 0.10 3.57 0.0050 0.004818 96.40
1,1-DICHLOROETHENE 0.4570 0.43234950 5.39 20 0.0050 0.004728 94.60
1,1-DICHLOROPROPENE 0.3360 0.32581540 3.03 0.0050 0.004850 97
1,2,3-TRICHLOROBENZENE 0.3660 0.390292 6.64 0.0050 0.005328 107
1,2,3-TRICHLOROPROPANE 0.2710 0.26514880 2.16 0.0050 0.004888 97.80
1,2,3-TRIMETHYLBENZENE 2.0280 1.891029 6.75 0.0050 0.004661 93.20
1,2,4-TRICHLOROBENZENE 0.4190 0.43503530 3.83 0.0050 0.005195 104
1,2,4-TRIMETHYLBENZENE 1.9680 1.896214 3.65 0.0050 0.004818 96.40
1,2-DIBROMO-3-CHLOROPROPANE 0.1790 0.16131490 9.88 0.0050 0.004500 90
1,2-DIBROMOETHANE 0.5460 0.54315820 0.52 0.0050 0.004974 99.50
1,2-DICHLOROBENZENE 1.0890 1.033514 5.10 0.0050 0.004746 94.90
1,2-DICHLOROETHANE 0.4840 0.42236910 12.70 0.0050 0.004366 87.30
1,2-DICHLOROPROPANE 0.3260 0.31779790 2.52 20 0.0050 0.004880 97.60
1,3,5-TRIMETHYLBENZENE 1.9330 1.876332 2.93 0.0050 0.004854 97.10
1,3-DICHLOROBENZENE 1.1730 1.112140 5.19 0.0050 0.004742 94.80
1,3-DICHLOROPROPANE 0.8820 0.89202890 1.14 0.0050 0.005059 101
1,4-DICHLOROBENZENE 1.26 1.137952 9.69 0.0050 0.004516 90.30
2,2-DICHLOROPROPANE 0.3150 0.28711690 8.85 0.0050 0.004551 91
2-BUTANONE (MEK)0.23 0.23729650 3.17 0.0250 0.02579 103
2-CHLOROTOLUENE 0.6620 0.635995 3.93 0.0050 0.004803 96.10
4-CHLOROTOLUENE 1.8870 1.746121 7.47 0.0050 0.004627 92.50
4-METHYL-2-PENTANONE (MIBK)1.04 1.089189 4.73 0.0250 0.02617 105
ACETONE 0.1180 0.11875860 0.6430 0.0250 0.02520 101
ACROLEIN 0.0370 0.03773243 1.98 0.0250 0.02956 118
ACRYLONITRILE 0.1640 0.17714910 8.02 0.0250 0.02698 108
BENZENE 1.0490 1.013444 3.39 0.0050 0.004828 96.60
BROMOBENZENE 0.7380 0.68366720 7.36 0.0050 0.004630 92.60
BROMODICHLOROMETHANE 0.3790 0.36184020 4.53 0.0050 0.004768 95.40
BROMOFORM 0.4840 0.44165030 0.10 8.75 0.0050 0.004559 91.20
BROMOMETHANE 0.2110 0.17666710 16.30 0.0050 0.004182 83.60
CARBON TETRACHLORIDE 0.4670 0.43830420 6.14 0.0050 0.004688 93.80
CHLOROBENZENE 1.6180 1.548624 0.30 4.29 0.0050 0.004784 95.70
CHLORODIBROMOMETHANE 0.6190 0.59116490 4.50 0.0050 0.004773 95.50
CHLOROETHANE 0.2270 0.21046480 7.28 0.0050 0.004634 92.70
CHLOROFORM 0.5190 0.49634010 4.37 20 0.0050 0.004784 95.70
CHLOROMETHANE 0.5740 0.48255830 0.10 15.90 0.0050 0.004204 84.10
CIS-1,2-DICHLOROETHENE 0.2810 0.27671410 1.53 0.0050 0.004925 98.50
CIS-1,3-DICHLOROPROPENE 0.4330 0.41414130 4.36 0.0050 0.004782 95.60
DI-ISOPROPYL ETHER 1.1980 1.170130 2.33 0.0050 0.004883 97.70
DIBROMOMETHANE 0.1830 0.17550790 4.09 0.0050 0.004799 96
DICHLORODIFLUOROMETHANE 0.3350 0.26912250 19.70 0.0050 0.004018 80.40
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 463 of 530
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1757957 Calibration (begin) date/time:07/19/24 04:01
Instrument ID:VOCMS58 Calibration (end) date/time:07/19/24 06:52
Lab File ID:0725_29 Analysis date/time:07/25/24 08:30
Analytical Method:8260B Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.8430 0.81561770 3.25 20 0.0050 0.004838 96.80
HEXACHLORO-1,3-BUTADIENE 0.2110 0.19665490 6.80 0.0050 0.004663 93.30
ISOPROPYLBENZENE 2.2330 2.261747 1.29 0.0050 0.005064 101
M&P-XYLENE 0.9810 0.97744950 0.3620 0.01 0.009967 99.70
METHYL TERT-BUTYL ETHER 0.73 0.75711720 3.71 0.0050 0.005189 104
METHYLENE CHLORIDE 0.2880 0.26676740 7.37 0.0050 0.004628 92.60
N-BUTYLBENZENE 1.4370 1.367892 4.81 0.0050 0.004759 95.20
N-PROPYLBENZENE 2.9970 2.789785 6.91 0.0050 0.004654 93.10
NAPHTHALENE 1.3420 1.371051 2.16 0.0050 0.004377 87.50
O-XYLENE 0.8930 0.89672950 0.4180 0.0050 0.005023 100
P-ISOPROPYLTOLUENE 1.7630 1.748860 0.8020 0.0050 0.004959 99.20
SEC-BUTYLBENZENE 2.0160 1.915644 4.98 0.0050 0.004751 95
STYRENE 1.4950 1.542092 3.15 0.0050 0.005157 103
TERT-BUTYLBENZENE 1.6030 1.513684 5.57 0.0050 0.004721 94.40
TETRACHLOROETHENE 0.5010 0.49052830 2.09 0.0050 0.004896 97.90
TOLUENE 2.4970 2.332266 6.60 20 0.0050 0.004670 93.40
TRANS-1,2-DICHLOROETHENE 0.2590 0.25510190 1.51 0.0050 0.004928 98.60
TRANS-1,3-DICHLOROPROPENE 0.83 0.82797750 0.2440 0.0050 0.004991 99.80
TRICHLOROETHENE 0.3120 0.29854180 4.31 0.0050 0.004784 95.70
TRICHLOROFLUOROMETHANE 0.4670 0.42969480 7.99 0.0050 0.004602 92
VINYL CHLORIDE 0.3630 0.33790390 6.91 20 0.0050 0.004654 93.10
1,2-DICHLOROETHANE-D4 0.3730 0.36497310 2.15 0.0160 0.01564 97.80 70 - 130
4-BROMOFLUOROBENZENE 0.8480 0.88065570 3.85 0.0160 0.01662 104 70 - 130
TOLUENE-D8 2.1250 2.178587 2.52 0.0160 0.01640 103 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 464 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS21 Calibration Start Date:07/10/24 11:59
Calibration End Date:07/10/24 19:49
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS210710240710_01740563 0710_01 07/10/24 10:50
TUNE VOCMS21071024A0710_01A740563 0710_01A 07/10/24 10:50
CAL 0.5 0710_04 07/10/24 11:59
CAL 1 0710_05 07/10/24 12:23
CAL 2 0710_06 07/10/24 12:46
CAL 5.0 0710_07 07/10/24 13:10
CAL 25 0710_08 07/10/24 13:33
CAL 75 0710_09 07/10/24 13:57
CAL 100 0710_10 07/10/24 14:20
CAL 200 0710_11 07/10/24 14:44
SSCV VOCMS210710240710_15740563 0710_15 07/10/24 16:17
SSCV VOCMS210710240710_17740563 0710_17 07/10/24 17:04
CAL 1A 0710_20A 07/10/24 18:15
CAL 5A 0710_21A 07/10/24 18:38
CAL 10A 0710_22A 07/10/24 19:02
CAL 15A 0710_23A 07/10/24 19:25
CAL 20A 0710_24A 07/10/24 19:49
TUNE VOCMS210721240721_01T740563 0721_01T 07/21/24 09:19
TUNE VOCMS210721240721_27T740563 0721_27T 07/21/24 21:27
ICV VOCMS210721240721_28740563 0721_28 07/21/24 21:51
LCS R4097932-1 0721_28LCS 07/21/24 21:51 1 WG2327390
LCSD R4097932-2 0721_29 07/21/24 22:14 1 WG2327390
BLANK R4097932-3 0721_32 07/21/24 23:25 1 WG2327390
TRIP BLANK L1757957-17 0721_33 07/22/24 00:33 1 WG2327390
L1757975-10 L1757975-10 0721_34 07/22/24 00:57 1 WG2327390
EB-1-071624 L1757957-16 0721_35 07/22/24 01:20 1 WG2327390
L1757930-09 L1757930-09 0721_36 07/22/24 01:44 1 WG2327390
L1757930-10 L1757930-10 0721_37 07/22/24 02:07 1 WG2327390
L1757930-11 L1757930-11 0721_38 07/22/24 02:31 1 WG2327390
L1757930-12 L1757930-12 0721_39 07/22/24 02:54 1 WG2327390
L1757930-13 L1757930-13 0721_40 07/22/24 03:18 1 WG2327390
L1757930-14 L1757930-14 0721_41 07/22/24 03:41 1 WG2327390
L1757930-15 L1757930-15 0721_42 07/22/24 04:05 1 WG2327390
L1757930-16 L1757930-16 0721_43 07/22/24 04:28 1 WG2327390
L1757975-01 L1757975-01 0721_44 07/22/24 04:52 1 WG2327390
L1757975-02 L1757975-02 0721_45 07/22/24 05:15 1 WG2327390
L1757975-03 L1757975-03 0721_46 07/22/24 05:39 1 WG2327390
L1757975-04 L1757975-04 0721_47 07/22/24 06:03 1 WG2327390
L1757975-06 L1757975-06 0721_48 07/22/24 06:26 1 WG2327390
L1757975-09 L1757975-09 0721_49 07/22/24 06:49 1 WG2327390
L1757975-05 L1757975-05 0721_50 07/22/24 07:13 5 WG2327390
L1757975-07 L1757975-07 0721_51 07/22/24 07:36 5 WG2327390
L1757975-08 L1757975-08 0721_52 07/22/24 08:00 5 WG2327390
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 465 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56 Calibration Start Date:07/08/24 19:30
Calibration End Date:07/08/24 22:21
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS560708240708_08737277 0708_08 07/08/24 19:11
CAL 0.04 0708_09 07/08/24 19:30
CAL 0.1 0708_10 07/08/24 19:49
CAL 0.2 0708_11 07/08/24 20:08
CAL 0.5 0708_12 07/08/24 20:27
CAL 1 0708_13 07/08/24 20:46
CAL 2 0708_14 07/08/24 21:05
CAL 5.0 0708_15 07/08/24 21:24
CAL 25 0708_16 07/08/24 21:43
CAL 75 0708_17 07/08/24 22:02
CAL 100 0708_18 07/08/24 22:21
SSCV VOCMS560708240708_22737277 0708_22 07/08/24 23:37
SSCV VOCMS560708240708_23737277 0708_23 07/08/24 23:56
TUNE VOCMS56072424A0724A_01T737277 0724A_01T 07/24/24 19:54
ICV VOCMS56072424A0724A_03737277 0724A_03 07/24/24 20:32
LCS R4098226-1 0724A_03LCS 07/24/24 20:32 1 WG2329566
BLANK R4098226-2 0724A_07 07/24/24 21:48 1 WG2329566
L1758898-02 L1758898-02 0724A_15 07/25/24 00:29 1 WG2329566
S-1 (0-6)L1757957-13 0724A_16 07/25/24 00:48 1.22 WG2329566
S-1 (6-12)L1757957-14 0724A_17 07/25/24 01:07 1.19 WG2329566
SS-1 (6-12)L1757957-15 0724A_18 07/25/24 01:26 1 WG2329566
L1757983-01 L1757983-01 0724A_19 07/25/24 01:45 1 WG2329566
L1757983-02 L1757983-02 0724A_20 07/25/24 02:04 1 WG2329566
L1757983-03 L1757983-03 0724A_21 07/25/24 02:23 1 WG2329566
L1757983-04 L1757983-04 0724A_22 07/25/24 02:42 1 WG2329566
L1757983-05 L1757983-05 0724A_23 07/25/24 03:01 1 WG2329566
L1757983-06 L1757983-06 0724A_24 07/25/24 03:20 1 WG2329566
L1757983-07 L1757983-07 0724A_25 07/25/24 03:39 1 WG2329566
L1757983-08 L1757983-08 0724A_26 07/25/24 03:58 1 WG2329566
L1757983-09 L1757983-09 0724A_27 07/25/24 04:17 1 WG2329566
L1757983-10 L1757983-10 0724A_28 07/25/24 04:36 1 WG2329566
L1757983-11 L1757983-11 0724A_29 07/25/24 04:55 1 WG2329566
L1757983-12 L1757983-12 0724A_30 07/25/24 05:14 1 WG2329566
L1757983-13 L1757983-13 0724A_31 07/25/24 05:33 1 WG2329566
L1757987-01 L1757987-01 0724A_32 07/25/24 05:53 1.01 WG2329566
L1757987-02 L1757987-02 0724A_33 07/25/24 06:11 1 WG2329566
L1758028-01 L1758028-01 0724A_34 07/25/24 06:31 1.01 WG2329566
TUNE VOCMS560725240725_01T737277 0725_01T 07/25/24 06:49
ICV VOCMS560725240725_03737277 0725_03 07/25/24 07:27
LCS R4098753-1 0725_03LCS 07/25/24 07:27 1 WG2329510
BLANK R4098753-2 0725_07 07/25/24 08:44 1 WG2329510
L1757958-01 L1757958-01 0725_08 07/25/24 09:29 1 WG2329510
L1757958-02 L1757958-02 0725_09 07/25/24 09:48 1 WG2329510
L1757958-03 L1757958-03 0725_10 07/25/24 10:07 1 WG2329510
L1757958-04 L1757958-04 0725_11 07/25/24 10:26 1 WG2329510
L1757994-01 L1757994-01 0725_12 07/25/24 10:46 1 WG2329510
L1757994-02 L1757994-02 0725_13 07/25/24 11:04 1 WG2329510
L1757994-03 L1757994-03 0725_14 07/25/24 11:23 1 WG2329510
L1757994-04 L1757994-04 0725_15 07/25/24 11:42 1.01 WG2329510
L1757994-05 L1757994-05 0725_16 07/25/24 12:01 1.01 WG2329510
L1758030-01 L1758030-01 0725_17 07/25/24 12:21 1 WG2329510
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 466 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS56 Calibration Start Date:07/08/24 19:30
Calibration End Date:07/08/24 22:21
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
L1758079-02 L1758079-02 0725_18 07/25/24 12:40 1 WG2329510
L1758079-04 L1758079-04 0725_19 07/25/24 12:59 1 WG2329510
L1758079-06 L1758079-06 0725_20 07/25/24 13:18 1.01 WG2329510
L1757864-01 L1757864-01 0725_21 07/25/24 13:37 1 WG2329510
L1757864-02 L1757864-02 0725_22 07/25/24 13:56 1.65 WG2329510
L1757864-03 L1757864-03 0725_23 07/25/24 14:15 1.2 WG2329510
S-2 (0-6)L1757957-12 0725_24 07/25/24 14:34 1.06 WG2329510
S-5 (0-6)L1757957-09 0725_28 07/25/24 15:58 1 WG2329510
S-4 (0-6)L1757957-10 0725_29 07/25/24 16:17 1.14 WG2329510
S-31 (0-6)L1757957-11 0725_30 07/25/24 16:36 1.21 WG2329510
TUNE VOCMS560725240725_31T737277 0725_31T 07/25/24 16:55
TUNE VOCMS560725240725_32T737277 0725_32T 07/25/24 17:14
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 467 of 530
8B-OR ANALYTICAL SEQUENCE
SDG:L1757957 Analytical Method:8260B
Instrument ID:VOCMS58 Calibration Start Date:07/19/24 04:01
Calibration End Date:07/19/24 06:52
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS580718240718_05740383 0718_05 07/19/24 03:22
CAL 0.04 0718_07 07/19/24 04:01
CAL 0.1 0718_08 07/19/24 04:20
CAL 0.2 0718_09 07/19/24 04:39
CAL 0.5 0718_10 07/19/24 04:58
CAL 1 0718_11 07/19/24 05:17
CAL 2 0718_12 07/19/24 05:36
CAL 5.0 0718_13 07/19/24 05:55
CAL 25 0718_14 07/19/24 06:14
CAL 75 0718_15 07/19/24 06:33
CAL 100 0718_16 07/19/24 06:52
SSCV VOCMS580718240718_21740383 0718_21 07/19/24 08:27
SSCV VOCMS580718240718_23740383 0718_23 07/19/24 09:05
TUNE VOCMS580725240725_28T740383 0725_28T 07/25/24 08:11
CCV VOCMS580725240725_29740383 0725_29 07/25/24 08:30
LCS R4098455-1 0725_29LCS 07/25/24 08:30 1 WG2329486
LCSD R4098455-2 0725_30 07/25/24 08:49 1 WG2329486
BLANK R4098455-3 0725_34 07/25/24 10:05 1 WG2329486
L1755451-06 L1755451-06 0725_35 07/25/24 10:25 1 WG2329486
L1755451-10 L1755451-10 0725_36 07/25/24 10:46 1 WG2329486
L1755451-12 L1755451-12 0725_37 07/25/24 11:05 1 WG2329486
L1755451-14 L1755451-14 0725_38 07/25/24 11:24 1 WG2329486
L1758893-01 L1758893-01 0725_39 07/25/24 11:43 1 WG2329486
L1758893-02 L1758893-02 0725_40 07/25/24 12:02 1 WG2329486
S-3 (6-12)L1757957-02 0725_41 07/25/24 12:21 1.05 WG2329486
S-30 (6-12)L1757957-03 0725_42 07/25/24 12:40 1.1 WG2329486
S-8 (0-6)L1757957-05 0725_43 07/25/24 12:59 1 WG2329486
S-7 (6-12)L1757957-07 0725_44 07/25/24 13:18 1.21 WG2329486
L1758431-01 L1758431-01 0725_45 07/25/24 13:37 1 WG2329486
L1758431-02 L1758431-02 0725_46 07/25/24 13:56 1.38 WG2329486
L1758431-03 L1758431-03 0725_47 07/25/24 14:16 1 WG2329486
L1758431-04 L1758431-04 0725_48 07/25/24 14:35 1.22 WG2329486
L1758431-05 L1758431-05 0725_49 07/25/24 14:54 1 WG2329486
S-3 (0-6)L1757957-01 0725_53 07/25/24 15:51 1.1 WG2329486
S-9 (0-6)L1757957-04 0725_54 07/25/24 16:10 1.03 WG2329486
S-7 (0-6)L1757957-06 0725_55 07/25/24 16:29 1.37 WG2329486
S-6 (0-6)L1757957-08 0725_56 07/25/24 16:48 1 WG2329486
MS R4098455-4 0725_59 07/25/24 17:45 1.1 WG2329486
MSD R4098455-5 0725_60 07/25/24 18:04 1.1 WG2329486
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16,17 Analytical Method:8260B
Matrix:GW Prep Method:8260B
Analyte CAS MDL RDL
mg/l mg/l
n-Butylbenzene 104-51-8 0.000157 0.0010
sec-Butylbenzene 135-98-8 0.000125 0.0010
tert-Butylbenzene 98-06-6 0.000127 0.0010
Carbon tetrachloride 56-23-5 0.000128 0.0010
Chlorobenzene 108-90-7 0.000116 0.0010
Chlorodibromomethane 124-48-1 0.000140 0.0010
Chloroethane 75-00-3 0.000192 0.0050
Chloroform 67-66-3 0.000111 0.0050
Chloromethane 74-87-3 0.000960 0.0025
Acetone 67-64-1 0.0113 0.05
2-Chlorotoluene 95-49-8 0.000106 0.0010
4-Chlorotoluene 106-43-4 0.000114 0.0010
1,2-Dibromo-3-Chloropropane 96-12-8 0.000276 0.0050
1,2-Dibromoethane 106-93-4 0.000126 0.0010
Dibromomethane 74-95-3 0.000122 0.0010
1,2-Dichlorobenzene 95-50-1 0.000107 0.0010
1,3-Dichlorobenzene 541-73-1 0.000110 0.0010
1,4-Dichlorobenzene 106-46-7 0.000120 0.0010
Dichlorodifluoromethane 75-71-8 0.000374 0.0050
1,1-Dichloroethane 75-34-3 0.0001 0.0010
Acrolein 107-02-8 0.002540 0.05
1,2-Dichloroethane 107-06-2 0.00008190 0.0010
1,1-Dichloroethene 75-35-4 0.000188 0.0010
cis-1,2-Dichloroethene 156-59-2 0.000126 0.0010
trans-1,2-Dichloroethene 156-60-5 0.000149 0.0010
1,2-Dichloropropane 78-87-5 0.000149 0.0010
1,1-Dichloropropene 563-58-6 0.000142 0.0010
1,3-Dichloropropane 142-28-9 0.000110 0.0010
cis-1,3-Dichloropropene 10061-01-5 0.000111 0.0010
trans-1,3-Dichloropropene 10061-02-6 0.000118 0.0010
2,2-Dichloropropane 594-20-7 0.000161 0.0010
Acrylonitrile 107-13-1 0.000671 0.01
Di-isopropyl ether 108-20-3 0.000105 0.0010
Ethylbenzene 100-41-4 0.000137 0.0010
Hexachloro-1,3-butadiene 87-68-3 0.000337 0.0010
Isopropylbenzene 98-82-8 0.000105 0.0010
p-Isopropyltoluene 99-87-6 0.000120 0.0010
2-Butanone (MEK)78-93-3 0.001190 0.01
Methylene Chloride 75-09-2 0.000430 0.0050
4-Methyl-2-pentanone (MIBK)108-10-1 0.000478 0.01
Methyl tert-butyl ether 1634-04-4 0.000101 0.0010
Naphthalene 91-20-3 0.0010 0.0050
Benzene 71-43-2 0.00009410 0.0010
n-Propylbenzene 103-65-1 0.00009930 0.0010
Styrene 100-42-5 0.000118 0.0010
1,1,1,2-Tetrachloroethane 630-20-6 0.000147 0.0010
1,1,2,2-Tetrachloroethane 79-34-5 0.000133 0.0010
1,1,2-Trichlorotrifluoroethane 76-13-1 0.000180 0.0010
Tetrachloroethene 127-18-4 0.0003 0.0010
Toluene 108-88-3 0.000278 0.0010
1,2,3-Trichlorobenzene 87-61-6 0.000230 0.0010
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-16,17 Analytical Method:8260B
Matrix:GW Prep Method:8260B
Analyte CAS MDL RDL
mg/l mg/l
1,2,4-Trichlorobenzene 120-82-1 0.000481 0.0010
1,1,1-Trichloroethane 71-55-6 0.000149 0.0010
Bromobenzene 108-86-1 0.000118 0.0010
1,1,2-Trichloroethane 79-00-5 0.000158 0.0010
Trichloroethene 79-01-6 0.000190 0.0010
Trichlorofluoromethane 75-69-4 0.000160 0.0050
1,2,3-Trichloropropane 96-18-4 0.000237 0.0025
1,2,4-Trimethylbenzene 95-63-6 0.000322 0.0010
1,2,3-Trimethylbenzene 526-73-8 0.000104 0.0010
1,3,5-Trimethylbenzene 108-67-8 0.000104 0.0010
Vinyl chloride 75-01-4 0.000234 0.0010
Xylenes, Total 1330-20-7 0.000174 0.0030
Bromodichloromethane 75-27-4 0.000136 0.0010
Bromoform 75-25-2 0.000129 0.0010
Bromomethane 74-83-9 0.000605 0.0050
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:8260B
Matrix:Solid Prep Method:5035A
Analyte CAS MDL RDL
mg/kg mg/kg
sec-Butylbenzene 135-98-8 0.002880 0.0125
tert-Butylbenzene 98-06-6 0.001950 0.0050
Carbon tetrachloride 56-23-5 0.000898 0.0050
Chlorobenzene 108-90-7 0.000210 0.0025
Chlorodibromomethane 124-48-1 0.000612 0.0025
Chloroethane 75-00-3 0.0017 0.0050
Chloroform 67-66-3 0.001030 0.0025
Chloromethane 74-87-3 0.004350 0.0125
2-Chlorotoluene 95-49-8 0.000865 0.0025
Acetone 67-64-1 0.0365 0.05
4-Chlorotoluene 106-43-4 0.000450 0.0050
1,2-Dibromo-3-Chloropropane 96-12-8 0.0039 0.0250
1,2-Dibromoethane 106-93-4 0.000648 0.0025
Dibromomethane 74-95-3 0.000750 0.0050
1,2-Dichlorobenzene 95-50-1 0.000425 0.0050
1,3-Dichlorobenzene 541-73-1 0.0006 0.0050
1,4-Dichlorobenzene 106-46-7 0.0007 0.0050
Dichlorodifluoromethane 75-71-8 0.001610 0.0050
1,1-Dichloroethane 75-34-3 0.000491 0.0025
1,2-Dichloroethane 107-06-2 0.000649 0.0025
Acrylonitrile 107-13-1 0.003610 0.0125
1,1-Dichloroethene 75-35-4 0.000606 0.0025
cis-1,2-Dichloroethene 156-59-2 0.000734 0.0025
trans-1,2-Dichloroethene 156-60-5 0.001040 0.0050
1,2-Dichloropropane 78-87-5 0.001420 0.0050
1,1-Dichloropropene 563-58-6 0.000809 0.0025
1,3-Dichloropropane 142-28-9 0.000501 0.0050
cis-1,3-Dichloropropene 10061-01-5 0.000757 0.0025
trans-1,3-Dichloropropene 10061-02-6 0.001140 0.0050
2,2-Dichloropropane 594-20-7 0.001380 0.0025
Di-isopropyl ether 108-20-3 0.000410 0.0010
Benzene 71-43-2 0.000467 0.0010
Ethylbenzene 100-41-4 0.000737 0.0025
Hexachloro-1,3-butadiene 87-68-3 0.0060 0.0250
Isopropylbenzene 98-82-8 0.000425 0.0025
p-Isopropyltoluene 99-87-6 0.002550 0.0050
2-Butanone (MEK)78-93-3 0.0635 0.10
Methylene Chloride 75-09-2 0.006640 0.0250
4-Methyl-2-pentanone (MIBK)108-10-1 0.002280 0.0250
Methyl tert-butyl ether 1634-04-4 0.000350 0.0010
Naphthalene 91-20-3 0.004880 0.0125
n-Propylbenzene 103-65-1 0.000950 0.0050
Bromobenzene 108-86-1 0.0009 0.0125
Styrene 100-42-5 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0.000948 0.0025
1,1,2,2-Tetrachloroethane 79-34-5 0.000695 0.0025
1,1,2-Trichlorotrifluoroethane 76-13-1 0.000754 0.0025
Tetrachloroethene 127-18-4 0.000896 0.0025
Toluene 108-88-3 0.0013 0.0050
1,2,3-Trichlorobenzene 87-61-6 0.007330 0.0125
1,2,4-Trichlorobenzene 120-82-1 0.0044 0.0125
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:8260B
Matrix:Solid Prep Method:5035A
Analyte CAS MDL RDL
mg/kg mg/kg
1,1,1-Trichloroethane 71-55-6 0.000923 0.0025
1,1,2-Trichloroethane 79-00-5 0.000597 0.0025
Bromodichloromethane 75-27-4 0.000725 0.0025
Trichloroethene 79-01-6 0.000584 0.0010
Trichlorofluoromethane 75-69-4 0.000827 0.0025
1,2,3-Trichloropropane 96-18-4 0.001620 0.0125
1,2,4-Trimethylbenzene 95-63-6 0.001580 0.0050
1,2,3-Trimethylbenzene 526-73-8 0.001580 0.0050
1,3,5-Trimethylbenzene 108-67-8 0.0020 0.0050
Vinyl chloride 75-01-4 0.001160 0.0025
Xylenes, Total 1330-20-7 0.000880 0.0065
Bromoform 75-25-2 0.001170 0.0250
Bromomethane 74-83-9 0.001970 0.0125
n-Butylbenzene 104-51-8 0.005250 0.0125
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4097932-3
Lab Sample ID:R4097932-3 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0721_32 Received Date/Time:_______________
Instrument ID:VOCMS21 Preparation Date/Time:07/21/24 23:25
Analytical Batch:WG2327390 Analysis Date/Time:07/21/24 23:25
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 2.78 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4097932-3
Lab Sample ID:R4097932-3 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0721_32 Received Date/Time:_______________
Instrument ID:VOCMS21 Preparation Date/Time:07/21/24 23:25
Analytical Batch:WG2327390 Analysis Date/Time:07/21/24 23:25
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098226-2
Lab Sample ID:R4098226-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0724A_07 Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/24/24 21:48
Analytical Batch:WG2329566 Analysis Date/Time:07/24/24 21:48
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 0 U 0.0365 0.0500
Acrylonitrile 107-13-1 0 U 0.00361 0.0125
Benzene 71-43-2 0 U 0.000467 0.00100
Bromobenzene 108-86-1 0 U 0.000900 0.0125
Bromodichloromethane 75-27-4 0 U 0.000725 0.00250
Bromoform 75-25-2 0 U 0.00117 0.0250
Bromomethane 74-83-9 2.38 U 0.00197 0.0125
n-Butylbenzene 104-51-8 8.46 U 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.02 U 0.00288 0.0125
tert-Butylbenzene 98-06-6 0 U 0.00195 0.00500
Carbon tetrachloride 56-23-5 0 U 0.000898 0.00500
Chlorobenzene 108-90-7 0 U 0.000210 0.00250
Chlorodibromomethane 124-48-1 0 U 0.000612 0.00250
Chloroethane 75-00-3 2.48 U 0.00170 0.00500
Chloroform 67-66-3 0 U 0.00103 0.00250
Chloromethane 74-87-3 0 U 0.00435 0.0125
2-Chlorotoluene 95-49-8 0 U 0.000865 0.00250
4-Chlorotoluene 106-43-4 0 U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00390 0.0250
1,2-Dibromoethane 106-93-4 0 U 0.000648 0.00250
Dibromomethane 74-95-3 0 U 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 0 U 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 0 U 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 0 U 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 0 U 0.00161 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.52 U 0.000649 0.00250
1,1-Dichloroethene 75-35-4 0 U 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 0 U 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 0 U 0.00104 0.00500
1,2-Dichloropropane 78-87-5 0 U 0.00142 0.00500
1,1-Dichloropropene 563-58-6 0 U 0.000809 0.00250
1,3-Dichloropropane 142-28-9 0 U 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00114 0.00500
2,2-Dichloropropane 594-20-7 0 U 0.00138 0.00250
Di-isopropyl ether 108-20-3 0 U 0.000410 0.00100
Ethylbenzene 100-41-4 0 U 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00600 0.0250
Isopropylbenzene 98-82-8 0 U 0.000425 0.00250
p-Isopropyltoluene 99-87-6 0 U 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.24 U 0.0635 0.100
Methylene Chloride 75-09-2 3.22 U 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098226-2
Lab Sample ID:R4098226-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0724A_07 Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/24/24 21:48
Analytical Batch:WG2329566 Analysis Date/Time:07/24/24 21:48
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 U 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 0 U 0.000350 0.00100
Naphthalene 91-20-3 10.09 0.00772 J 0.00488 0.0125
n-Propylbenzene 103-65-1 0 U 0.000950 0.00500
Styrene 100-42-5 0 U 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000754 0.00250
Tetrachloroethene 127-18-4 0 U 0.000896 0.00250
Toluene 108-88-3 5.58 U 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 0 U 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 0 U 0.000597 0.00250
Trichloroethene 79-01-6 0 U 0.000584 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 0 U 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.95 U 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.28 U 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.58 U 0.00200 0.00500
Vinyl chloride 75-01-4 0 U 0.00116 0.00250
Xylenes, Total 1330-20-7 0 U 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-3
Lab Sample ID:R4098455-3 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_34 Received Date/Time:_______________
Instrument ID:VOCMS58 Preparation Date/Time:07/25/24 10:05
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 10:05
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 U 0.0365 0.0500
Acrylonitrile 107-13-1 0 U 0.00361 0.0125
Benzene 71-43-2 0 U 0.000467 0.00100
Bromobenzene 108-86-1 0 U 0.000900 0.0125
Bromodichloromethane 75-27-4 0 U 0.000725 0.00250
Bromoform 75-25-2 0 U 0.00117 0.0250
Bromomethane 74-83-9 2.30 U 0.00197 0.0125
n-Butylbenzene 104-51-8 0 U 0.00525 0.0125
sec-Butylbenzene 135-98-8 0 U 0.00288 0.0125
tert-Butylbenzene 98-06-6 0 U 0.00195 0.00500
Carbon tetrachloride 56-23-5 0 U 0.000898 0.00500
Chlorobenzene 108-90-7 0 U 0.000210 0.00250
Chlorodibromomethane 124-48-1 0 U 0.000612 0.00250
Chloroethane 75-00-3 2.38 U 0.00170 0.00500
Chloroform 67-66-3 0 U 0.00103 0.00250
Chloromethane 74-87-3 0 U 0.00435 0.0125
2-Chlorotoluene 95-49-8 0 U 0.000865 0.00250
4-Chlorotoluene 106-43-4 0 U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00390 0.0250
1,2-Dibromoethane 106-93-4 0 U 0.000648 0.00250
Dibromomethane 74-95-3 0 U 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 0 U 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 0 U 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 0 U 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 0 U 0.00161 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.50 U 0.000649 0.00250
1,1-Dichloroethene 75-35-4 0 U 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.98 U 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 0 U 0.00104 0.00500
1,2-Dichloropropane 78-87-5 0 U 0.00142 0.00500
1,1-Dichloropropene 563-58-6 0 U 0.000809 0.00250
1,3-Dichloropropane 142-28-9 0 U 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00114 0.00500
2,2-Dichloropropane 594-20-7 0 U 0.00138 0.00250
Di-isopropyl ether 108-20-3 0 U 0.000410 0.00100
Ethylbenzene 100-41-4 0 U 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00600 0.0250
Isopropylbenzene 98-82-8 0 U 0.000425 0.00250
p-Isopropyltoluene 99-87-6 0 U 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.20 U 0.0635 0.100
Methylene Chloride 75-09-2 3.16 U 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-3
Lab Sample ID:R4098455-3 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_34 Received Date/Time:_______________
Instrument ID:VOCMS58 Preparation Date/Time:07/25/24 10:05
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 10:05
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 0 U 0.000350 0.00100
Naphthalene 91-20-3 0 U 0.00488 0.0125
n-Propylbenzene 103-65-1 7.43 U 0.000950 0.00500
Styrene 100-42-5 0 U 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000754 0.00250
Tetrachloroethene 127-18-4 0 U 0.000896 0.00250
Toluene 108-88-3 5.58 U 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 0 U 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 0 U 0.000597 0.00250
Trichloroethene 79-01-6 0 U 0.000584 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 0 U 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 0 U 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.28 U 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 0 U 0.00200 0.00500
Vinyl chloride 75-01-4 0 U 0.00116 0.00250
Xylenes, Total 1330-20-7 0 U 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098753-2
Lab Sample ID:R4098753-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_07 Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/25/24 08:44
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 08:44
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 U 0.0365 0.0500
Acrylonitrile 107-13-1 0 U 0.00361 0.0125
Benzene 71-43-2 4.41 U 0.000467 0.00100
Bromobenzene 108-86-1 0 U 0.000900 0.0125
Bromodichloromethane 75-27-4 0 U 0.000725 0.00250
Bromoform 75-25-2 0 U 0.00117 0.0250
Bromomethane 74-83-9 2.35 U 0.00197 0.0125
n-Butylbenzene 104-51-8 0 U 0.00525 0.0125
sec-Butylbenzene 135-98-8 0 U 0.00288 0.0125
tert-Butylbenzene 98-06-6 0 U 0.00195 0.00500
Carbon tetrachloride 56-23-5 0 U 0.000898 0.00500
Chlorobenzene 108-90-7 0 U 0.000210 0.00250
Chlorodibromomethane 124-48-1 0 U 0.000612 0.00250
Chloroethane 75-00-3 2.44 U 0.00170 0.00500
Chloroform 67-66-3 0 U 0.00103 0.00250
Chloromethane 74-87-3 0 U 0.00435 0.0125
2-Chlorotoluene 95-49-8 0 U 0.000865 0.00250
4-Chlorotoluene 106-43-4 0 U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00390 0.0250
1,2-Dibromoethane 106-93-4 0 U 0.000648 0.00250
Dibromomethane 74-95-3 0 U 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 0 U 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 0 U 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 0 U 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 0 U 0.00161 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.52 U 0.000649 0.00250
1,1-Dichloroethene 75-35-4 0 U 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.99 U 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 0 U 0.00104 0.00500
1,2-Dichloropropane 78-87-5 0 U 0.00142 0.00500
1,1-Dichloropropene 563-58-6 0 U 0.000809 0.00250
1,3-Dichloropropane 142-28-9 0 U 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00114 0.00500
2,2-Dichloropropane 594-20-7 0 U 0.00138 0.00250
Di-isopropyl ether 108-20-3 0 U 0.000410 0.00100
Ethylbenzene 100-41-4 0 U 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00600 0.0250
Isopropylbenzene 98-82-8 0 U 0.000425 0.00250
p-Isopropyltoluene 99-87-6 0 U 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.24 U 0.0635 0.100
Methylene Chloride 75-09-2 3.21 U 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098753-2
Lab Sample ID:R4098753-2 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_07 Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/25/24 08:44
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 08:44
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.79 U 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 0 U 0.000350 0.00100
Naphthalene 91-20-3 10.10 U 0.00488 0.0125
n-Propylbenzene 103-65-1 0 U 0.000950 0.00500
Styrene 100-42-5 0 U 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000754 0.00250
Tetrachloroethene 127-18-4 0 U 0.000896 0.00250
Toluene 108-88-3 5.58 U 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 0 U 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 0 U 0.000597 0.00250
Trichloroethene 79-01-6 0 U 0.000584 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 0 U 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.95 U 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 0 U 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 0 U 0.00200 0.00500
Vinyl chloride 75-01-4 0 U 0.00116 0.00250
Xylenes, Total 1330-20-7 0 U 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4097932-1
Lab Sample ID:R4097932-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0721_28LCS Received Date/Time:_______________
Instrument ID:VOCMS21 Preparation Date/Time:07/21/24 21:51
Analytical Batch:WG2327390 Analysis Date/Time:07/21/24 21:51
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 2.78 0.0233 J 0.0113 0.0500
Acrolein 107-02-8 2.62 0.0261 J 0.000 0.0500
Acrylonitrile 107-13-1 3.21 0.0245 0.000671 0.0100
Benzene 71-43-2 3.95 0.00530 0.0000941 0.00100
Bromobenzene 108-86-1 7.05 0.00498 0.000118 0.00100
Bromodichloromethane 75-27-4 4.60 0.00482 0.000136 0.00100
Bromoform 75-25-2 6.60 0.00360 0.000129 0.00100
Bromomethane 74-83-9 1.93 0.00195 J 0.000605 0.00500
n-Butylbenzene 104-51-8 8.01 0.00470 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.57 0.00483 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.44 0.00485 0.000127 0.00100
Carbon tetrachloride 56-23-5 3.70 0.00462 0.000128 0.00100
Chlorobenzene 108-90-7 6.12 0.00438 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.60 0.00413 0.000140 0.00100
Chloroethane 75-00-3 2.01 0.0112 J4 0.000192 0.00500
Chloroform 67-66-3 3.62 0.00492 J 0.000111 0.00500
Chloromethane 74-87-3 1.66 0.00446 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.18 0.00500 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.30 0.00476 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 8.80 0.00362 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 5.78 0.00434 0.000126 0.00100
Dibromomethane 74-95-3 4.51 0.00485 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.15 0.00425 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 7.76 0.00442 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 7.82 0.00431 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.50 0.00424 J 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.18 0.00504 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.06 0.00505 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.42 0.00498 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.48 0.00479 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 2.84 0.00512 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.57 0.00525 0.000149 0.00100
1,1-Dichloropropene 563-58-6 3.81 0.00495 0.000142 0.00100
1,3-Dichloropropane 142-28-9 5.67 0.00470 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 4.98 0.00499 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.37 0.00465 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.54 0.00482 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.09 0.00551 0.000105 0.00100
Ethylbenzene 100-41-4 6.12 0.00451 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.32 0.00362 0.000337 0.00100
Isopropylbenzene 98-82-8 6.75 0.00449 0.000105 0.00100
p-Isopropyltoluene 99-87-6 7.68 0.00471 0.000120 0.00100
2-Butanone (MEK)78-93-3 3.78 0.0238 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4097932-1
Lab Sample ID:R4097932-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0721_28LCS Received Date/Time:_______________
Instrument ID:VOCMS21 Preparation Date/Time:07/21/24 21:51
Analytical Batch:WG2327390 Analysis Date/Time:07/21/24 21:51
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 2.75 0.00490 J 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.34 0.0248 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 2.89 0.00518 0.000101 0.00100
Naphthalene 91-20-3 9.63 0.00451 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.05 0.00518 0.0000993 0.00100
Styrene 100-42-5 6.56 0.00409 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.16 0.00409 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.10 0.00476 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.43 0.00489 0.000180 0.00100
Tetrachloroethene 127-18-4 5.37 0.00381 0.000300 0.00100
Toluene 108-88-3 5.12 0.00464 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 9.78 0.00365 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.35 0.00359 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 3.74 0.00475 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.48 0.00439 0.000158 0.00100
Trichloroethene 79-01-6 4.26 0.00465 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.11 0.00474 J 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.21 0.00455 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.49 0.00506 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 7.84 0.00501 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.20 0.00501 0.000104 0.00100
Vinyl chloride 75-01-4 1.70 0.00530 0.000234 0.00100
Xylenes, Total 1330-20-7 6.52 0.0136 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098226-1
Lab Sample ID:R4098226-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0724A_03LCS Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/24/24 20:32
Analytical Batch:WG2329566 Analysis Date/Time:07/24/24 20:32
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 0.531 0.0365 0.0500
Acrylonitrile 107-13-1 3.66 0.857 0.00361 0.0125
Benzene 71-43-2 4.41 0.116 0.000467 0.00100
Bromobenzene 108-86-1 7.51 0.125 0.000900 0.0125
Bromodichloromethane 75-27-4 5.06 0.139 0.000725 0.00250
Bromoform 75-25-2 7.05 0.160 0.00117 0.0250
Bromomethane 74-83-9 2.37 0.141 0.00197 0.0125
n-Butylbenzene 104-51-8 8.45 0.102 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.01 0.104 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.88 0.112 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.17 0.139 0.000898 0.00500
Chlorobenzene 108-90-7 6.58 0.119 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.07 0.132 0.000612 0.00250
Chloroethane 75-00-3 2.43 0.170 J4 0.00170 0.00500
Chloroform 67-66-3 4.07 0.117 0.00103 0.00250
Chloromethane 74-87-3 2.02 0.112 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.63 0.114 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.75 0.118 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.155 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.24 0.127 0.000648 0.00250
Dibromomethane 74-95-3 4.98 0.130 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.61 0.130 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.21 0.121 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.27 0.117 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.85 0.128 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.63 0.124 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.52 0.124 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.86 0.113 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.93 0.123 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.28 0.127 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.03 0.126 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.27 0.124 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.12 0.122 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.43 0.135 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.83 0.128 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.99 0.110 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.52 0.145 0.000410 0.00100
Ethylbenzene 100-41-4 6.57 0.118 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.76 0.131 0.00600 0.0250
Isopropylbenzene 98-82-8 7.19 0.124 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.11 0.109 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.23 0.644 0.0635 0.100
Methylene Chloride 75-09-2 3.19 0.111 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098226-1
Lab Sample ID:R4098226-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0724A_03LCS Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/24/24 20:32
Analytical Batch:WG2329566 Analysis Date/Time:07/24/24 20:32
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.79 0.743 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.33 0.148 0.000350 0.00100
Naphthalene 91-20-3 10.08 0.128 0.00488 0.0125
n-Propylbenzene 103-65-1 7.49 0.113 0.000950 0.00500
Styrene 100-42-5 7.01 0.118 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.143 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.55 0.128 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.88 0.106 0.000754 0.00250
Tetrachloroethene 127-18-4 5.83 0.130 0.000896 0.00250
Toluene 108-88-3 5.58 0.118 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.23 0.161 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.80 0.136 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.20 0.141 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.94 0.128 0.000597 0.00250
Trichloroethene 79-01-6 4.72 0.129 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.55 0.109 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.66 0.115 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.93 0.114 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.27 0.110 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.63 0.116 0.00200 0.00500
Vinyl chloride 75-01-4 2.10 0.102 0.00116 0.00250
Xylenes, Total 1330-20-7 6.97 0.357 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-1
Lab Sample ID:R4098455-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_29LCS Received Date/Time:_______________
Instrument ID:VOCMS58 Preparation Date/Time:07/25/24 08:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 08:30
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 0.630 0.0365 0.0500
Acrylonitrile 107-13-1 3.61 0.675 0.00361 0.0125
Benzene 71-43-2 4.39 0.121 0.000467 0.00100
Bromobenzene 108-86-1 7.52 0.116 0.000900 0.0125
Bromodichloromethane 75-27-4 5.05 0.119 0.000725 0.00250
Bromoform 75-25-2 7.06 0.114 0.00117 0.0250
Bromomethane 74-83-9 2.30 0.105 0.00197 0.0125
n-Butylbenzene 104-51-8 8.46 0.119 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.03 0.119 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.89 0.118 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.15 0.117 0.000898 0.00500
Chlorobenzene 108-90-7 6.58 0.120 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.06 0.119 0.000612 0.00250
Chloroethane 75-00-3 2.38 0.116 0.00170 0.00500
Chloroform 67-66-3 4.04 0.120 0.00103 0.00250
Chloromethane 74-87-3 1.95 0.105 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.64 0.120 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.76 0.116 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.113 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.24 0.124 0.000648 0.00250
Dibromomethane 74-95-3 4.97 0.120 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.62 0.119 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.22 0.119 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.28 0.113 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.77 0.100 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.60 0.120 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.50 0.109 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.80 0.118 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.90 0.123 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.25 0.123 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.03 0.122 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.25 0.121 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.12 0.126 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.43 0.120 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.82 0.125 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.97 0.114 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.50 0.122 0.000410 0.00100
Ethylbenzene 100-41-4 6.58 0.121 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.79 0.117 0.00600 0.0250
Isopropylbenzene 98-82-8 7.20 0.127 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.13 0.124 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.19 0.645 0.0635 0.100
Methylene Chloride 75-09-2 3.15 0.116 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 485 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-1
Lab Sample ID:R4098455-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_29LCS Received Date/Time:_______________
Instrument ID:VOCMS58 Preparation Date/Time:07/25/24 08:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 08:30
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.654 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.29 0.130 0.000350 0.00100
Naphthalene 91-20-3 10.09 0.109 0.00488 0.0125
n-Propylbenzene 103-65-1 7.50 0.116 0.000950 0.00500
Styrene 100-42-5 7.02 0.129 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.125 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.55 0.122 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.84 0.119 0.000754 0.00250
Tetrachloroethene 127-18-4 5.84 0.122 0.000896 0.00250
Toluene 108-88-3 5.58 0.117 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.25 0.133 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.82 0.130 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.19 0.123 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.94 0.125 0.000597 0.00250
Trichloroethene 79-01-6 4.72 0.120 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.48 0.115 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.66 0.122 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.94 0.120 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.28 0.117 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.64 0.121 0.00200 0.00500
Vinyl chloride 75-01-4 2.02 0.116 0.00116 0.00250
Xylenes, Total 1330-20-7 6.99 0.375 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 486 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098753-1
Lab Sample ID:R4098753-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_03LCS Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/25/24 07:27
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 07:27
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 0.593 0.0365 0.0500
Acrylonitrile 107-13-1 3.66 0.856 0.00361 0.0125
Benzene 71-43-2 4.41 0.114 0.000467 0.00100
Bromobenzene 108-86-1 7.51 0.121 0.000900 0.0125
Bromodichloromethane 75-27-4 5.06 0.132 0.000725 0.00250
Bromoform 75-25-2 7.06 0.145 0.00117 0.0250
Bromomethane 74-83-9 2.37 0.120 0.00197 0.0125
n-Butylbenzene 104-51-8 8.45 0.0975 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.01 0.101 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.88 0.108 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.17 0.128 0.000898 0.00500
Chlorobenzene 108-90-7 6.58 0.115 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.07 0.121 0.000612 0.00250
Chloroethane 75-00-3 2.43 0.145 0.00170 0.00500
Chloroform 67-66-3 4.07 0.112 0.00103 0.00250
Chloromethane 74-87-3 2.02 0.0919 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.63 0.112 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.75 0.108 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.134 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.24 0.120 0.000648 0.00250
Dibromomethane 74-95-3 4.98 0.130 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.61 0.113 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.21 0.115 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.28 0.114 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.85 0.102 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.64 0.120 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.52 0.120 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.85 0.114 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.93 0.120 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.28 0.123 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.04 0.124 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.27 0.117 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.13 0.120 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.43 0.130 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.83 0.125 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.99 0.117 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.52 0.151 0.000410 0.00100
Ethylbenzene 100-41-4 6.57 0.115 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.76 0.110 0.00600 0.0250
Isopropylbenzene 98-82-8 7.19 0.117 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.11 0.106 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.23 0.861 0.0635 0.100
Methylene Chloride 75-09-2 3.19 0.107 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098753-1
Lab Sample ID:R4098753-1 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_03LCS Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:07/25/24 07:27
Analytical Batch:WG2329510 Analysis Date/Time:07/25/24 07:27
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.79 0.756 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.33 0.136 0.000350 0.00100
Naphthalene 91-20-3 10.08 0.104 0.00488 0.0125
n-Propylbenzene 103-65-1 7.50 0.116 0.000950 0.00500
Styrene 100-42-5 7.02 0.112 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.134 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.55 0.125 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.88 0.117 0.000754 0.00250
Tetrachloroethene 127-18-4 5.83 0.126 0.000896 0.00250
Toluene 108-88-3 5.58 0.114 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.23 0.120 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.80 0.117 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.20 0.138 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.94 0.125 0.000597 0.00250
Trichloroethene 79-01-6 4.73 0.126 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.53 0.115 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.66 0.111 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.93 0.112 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.28 0.105 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.63 0.112 0.00200 0.00500
Vinyl chloride 75-01-4 2.10 0.125 0.00116 0.00250
Xylenes, Total 1330-20-7 6.98 0.343 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4097932-2
Lab Sample ID:R4097932-2 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0721_29 Received Date/Time:_______________
Instrument ID:VOCMS21 Preparation Date/Time:07/21/24 22:14
Analytical Batch:WG2327390 Analysis Date/Time:07/21/24 22:14
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 2.78 0.0234 J 0.0113 0.0500
Acrolein 107-02-8 2.62 0.0289 J 0.000 0.0500
Acrylonitrile 107-13-1 3.21 0.0266 0.000671 0.0100
Benzene 71-43-2 3.95 0.00570 0.0000941 0.00100
Bromobenzene 108-86-1 7.05 0.00527 0.000118 0.00100
Bromodichloromethane 75-27-4 4.60 0.00522 0.000136 0.00100
Bromoform 75-25-2 6.60 0.00382 0.000129 0.00100
Bromomethane 74-83-9 1.93 0.00236 J 0.000605 0.00500
n-Butylbenzene 104-51-8 8.01 0.00498 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.57 0.00512 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.44 0.00511 0.000127 0.00100
Carbon tetrachloride 56-23-5 3.71 0.00504 0.000128 0.00100
Chlorobenzene 108-90-7 6.12 0.00457 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.60 0.00433 0.000140 0.00100
Chloroethane 75-00-3 2.01 0.0104 J4 0.000192 0.00500
Chloroform 67-66-3 3.61 0.00499 J 0.000111 0.00500
Chloromethane 74-87-3 1.66 0.00498 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.18 0.00536 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.31 0.00514 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 8.80 0.00398 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 5.78 0.00450 0.000126 0.00100
Dibromomethane 74-95-3 4.51 0.00519 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.16 0.00460 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 7.76 0.00455 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 7.82 0.00464 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.49 0.00497 J 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.18 0.00553 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.06 0.00538 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.42 0.00561 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.48 0.00542 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 2.84 0.00517 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.57 0.00556 0.000149 0.00100
1,1-Dichloropropene 563-58-6 3.81 0.00545 0.000142 0.00100
1,3-Dichloropropane 142-28-9 5.67 0.00495 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 4.98 0.00526 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.37 0.00485 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.54 0.00512 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.09 0.00587 0.000105 0.00100
Ethylbenzene 100-41-4 6.12 0.00469 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.32 0.00373 0.000337 0.00100
Isopropylbenzene 98-82-8 6.75 0.00481 0.000105 0.00100
p-Isopropyltoluene 99-87-6 7.68 0.00511 0.000120 0.00100
2-Butanone (MEK)78-93-3 3.78 0.0258 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4097932-2
Lab Sample ID:R4097932-2 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0721_29 Received Date/Time:_______________
Instrument ID:VOCMS21 Preparation Date/Time:07/21/24 22:14
Analytical Batch:WG2327390 Analysis Date/Time:07/21/24 22:14
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 2.76 0.00572 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.34 0.0265 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 2.89 0.00555 0.000101 0.00100
Naphthalene 91-20-3 9.63 0.00445 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.06 0.00551 0.0000993 0.00100
Styrene 100-42-5 6.56 0.00430 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.16 0.00441 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.10 0.00525 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.43 0.00533 0.000180 0.00100
Tetrachloroethene 127-18-4 5.37 0.00407 0.000300 0.00100
Toluene 108-88-3 5.12 0.00484 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 9.78 0.00385 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.35 0.00383 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 3.74 0.00524 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.48 0.00467 0.000158 0.00100
Trichloroethene 79-01-6 4.27 0.00491 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.11 0.00532 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.21 0.00488 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.49 0.00523 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 7.84 0.00526 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.20 0.00523 0.000104 0.00100
Vinyl chloride 75-01-4 1.70 0.00590 0.000234 0.00100
Xylenes, Total 1330-20-7 6.53 0.0140 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1757957 11/22/24 14:29 490 of 530
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-2
Lab Sample ID:R4098455-2 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0725_30 Received Date/Time:_______________
Instrument ID:VOCMS58 Preparation Date/Time:07/25/24 08:49
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 08:49
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 0.610 0.0365 0.0500
Acrylonitrile 107-13-1 3.61 0.656 0.00361 0.0125
Benzene 71-43-2 4.39 0.122 0.000467 0.00100
Bromobenzene 108-86-1 7.52 0.117 0.000900 0.0125
Bromodichloromethane 75-27-4 5.05 0.119 0.000725 0.00250
Bromoform 75-25-2 7.06 0.114 0.00117 0.0250
Bromomethane 74-83-9 2.30 0.110 0.00197 0.0125
n-Butylbenzene 104-51-8 8.46 0.121 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.03 0.124 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.89 0.120 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.15 0.119 0.000898 0.00500
Chlorobenzene 108-90-7 6.58 0.119 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.06 0.121 0.000612 0.00250
Chloroethane 75-00-3 2.38 0.115 0.00170 0.00500
Chloroform 67-66-3 4.04 0.119 0.00103 0.00250
Chloromethane 74-87-3 1.95 0.133 J3 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.64 0.120 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.76 0.119 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.115 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.24 0.122 0.000648 0.00250
Dibromomethane 74-95-3 4.97 0.119 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.62 0.120 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.22 0.119 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.28 0.117 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.77 0.101 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.60 0.122 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.50 0.108 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.80 0.120 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.90 0.128 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.25 0.123 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.03 0.120 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.25 0.121 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.12 0.121 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.43 0.121 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.82 0.126 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.97 0.113 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.50 0.123 0.000410 0.00100
Ethylbenzene 100-41-4 6.58 0.123 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.79 0.121 0.00600 0.0250
Isopropylbenzene 98-82-8 7.20 0.129 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.13 0.127 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.19 0.627 0.0635 0.100
Methylene Chloride 75-09-2 3.15 0.116 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-2
Lab Sample ID:R4098455-2 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0725_30 Received Date/Time:_______________
Instrument ID:VOCMS58 Preparation Date/Time:07/25/24 08:49
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 08:49
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.646 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.29 0.126 0.000350 0.00100
Naphthalene 91-20-3 10.09 0.112 0.00488 0.0125
n-Propylbenzene 103-65-1 7.50 0.118 0.000950 0.00500
Styrene 100-42-5 7.02 0.129 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.124 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.55 0.121 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.84 0.122 0.000754 0.00250
Tetrachloroethene 127-18-4 5.84 0.124 0.000896 0.00250
Toluene 108-88-3 5.58 0.117 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.25 0.134 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.82 0.133 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.19 0.126 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.94 0.127 0.000597 0.00250
Trichloroethene 79-01-6 4.72 0.121 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.48 0.119 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.66 0.122 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.94 0.123 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.28 0.119 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.64 0.127 0.00200 0.00500
Vinyl chloride 75-01-4 2.03 0.117 0.00116 0.00250
Xylenes, Total 1330-20-7 6.99 0.377 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-4
Lab Sample ID:R4098455-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:0725_59 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 17:45
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 0.282 0.0413 0.0565
Acrylonitrile 107-13-1 3.61 0.485 0.00408 0.0142
Benzene 71-43-2 4.38 0.128 0.000528 0.00113
Bromobenzene 108-86-1 7.52 0.126 0.00102 0.0142
Bromodichloromethane 75-27-4 5.05 0.122 0.000820 0.00282
Bromoform 75-25-2 7.06 0.112 0.00132 0.0282
Bromomethane 74-83-9 2.26 0.0731 0.00223 0.0142
n-Butylbenzene 104-51-8 8.46 0.159 0.00594 0.0142
sec-Butylbenzene 135-98-8 8.03 0.151 0.00326 0.0142
tert-Butylbenzene 98-06-6 7.89 0.139 0.00221 0.00565
Carbon tetrachloride 56-23-5 4.14 0.130 0.00101 0.00565
Chlorobenzene 108-90-7 6.58 0.134 0.000237 0.00282
Chlorodibromomethane 124-48-1 6.06 0.123 0.000691 0.00282
Chloroethane 75-00-3 2.34 0.0558 0.00192 0.00565
Chloroform 67-66-3 4.04 0.132 0.00116 0.00282
Chloromethane 74-87-3 1.95 0.114 0.00492 0.0142
2-Chlorotoluene 95-49-8 7.64 0.134 0.000978 0.00282
4-Chlorotoluene 106-43-4 7.76 0.136 0.000508 0.00565
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.0863 0.00441 0.0282
1,2-Dibromoethane 106-93-4 6.24 0.127 0.000732 0.00282
Dibromomethane 74-95-3 4.97 0.115 0.000847 0.00565
1,2-Dichlorobenzene 95-50-1 8.62 0.131 0.000481 0.00565
1,3-Dichlorobenzene 541-73-1 8.22 0.134 0.000678 0.00565
1,4-Dichlorobenzene 106-46-7 8.28 0.131 0.000791 0.00565
Dichlorodifluoromethane 75-71-8 1.76 0.139 0.00182 0.00565
1,1-Dichloroethane 75-34-3 3.59 0.129 0.000555 0.00282
1,2-Dichloroethane 107-06-2 4.49 0.111 0.000733 0.00282
1,1-Dichloroethene 75-35-4 2.79 0.129 0.000685 0.00282
cis-1,2-Dichloroethene 156-59-2 3.89 0.132 0.000829 0.00282
trans-1,2-Dichloroethene 156-60-5 3.23 0.128 0.00117 0.00565
1,2-Dichloropropane 78-87-5 5.02 0.128 0.00160 0.00565
1,1-Dichloropropene 563-58-6 4.24 0.134 0.000914 0.00282
1,3-Dichloropropane 142-28-9 6.11 0.134 0.000566 0.00565
cis-1,3-Dichloropropene 10061-01-5 5.42 0.135 0.000856 0.00282
trans-1,3-Dichloropropene 10061-02-6 5.82 0.138 0.00128 0.00565
2,2-Dichloropropane 594-20-7 3.96 0.110 0.00156 0.00282
Di-isopropyl ether 108-20-3 3.49 0.134 0.000463 0.00113
Ethylbenzene 100-41-4 6.58 0.139 0.000833 0.00282
Hexachloro-1,3-butadiene 87-68-3 9.79 0.183 0.00678 0.0282
Isopropylbenzene 98-82-8 7.20 0.150 0.000481 0.00282
p-Isopropyltoluene 99-87-6 8.13 0.153 0.00289 0.00565
2-Butanone (MEK)78-93-3 4.19 0.420 0.0718 0.113
Methylene Chloride 75-09-2 3.16 0.130 0.00750 0.0282
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-4
Lab Sample ID:R4098455-4 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:0725_59 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 17:45
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.575 0.00258 0.0282
Methyl tert-butyl ether 1634-04-4 3.29 0.119 0.000395 0.00113
Naphthalene 91-20-3 10.09 0.108 0.00552 0.0142
n-Propylbenzene 103-65-1 7.50 0.132 0.00108 0.00565
Styrene 100-42-5 7.02 0.146 0.000259 0.0142
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.134 0.00107 0.00282
1,1,2,2-Tetrachloroethane 79-34-5 7.55 0.111 0.000786 0.00282
1,1,2-Trichlorotrifluoroethane 76-13-1 2.82 0.147 0.000851 0.00282
Tetrachloroethene 127-18-4 5.84 0.136 0.00101 0.00282
Toluene 108-88-3 5.58 0.131 0.00147 0.00565
1,2,3-Trichlorobenzene 87-61-6 10.25 0.163 0.00828 0.0142
1,2,4-Trichlorobenzene 120-82-1 9.82 0.164 0.00497 0.0142
1,1,1-Trichloroethane 71-55-6 4.18 0.136 0.00105 0.00282
1,1,2-Trichloroethane 79-00-5 5.93 0.137 0.000675 0.00282
Trichloroethene 79-01-6 4.72 0.131 0.000659 0.00113
Trichlorofluoromethane 75-69-4 2.43 0.0615 0.000935 0.00282
1,2,3-Trichloropropane 96-18-4 7.66 0.115 0.00183 0.0142
1,2,4-Trimethylbenzene 95-63-6 7.94 0.146 0.00179 0.00565
1,2,3-Trimethylbenzene 526-73-8 8.28 0.128 0.00179 0.00565
1,3,5-Trimethylbenzene 108-67-8 7.64 0.143 0.00226 0.00565
Vinyl chloride 75-01-4 2.01 0.129 0.00131 0.00282
Xylenes, Total 1330-20-7 6.98 0.425 0.000994 0.00734
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-5
Lab Sample ID:R4098455-5 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:0725_60 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 18:04
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.16 0.109 J3 0.0413 0.0565
Acrylonitrile 107-13-1 3.61 0.507 0.00408 0.0142
Benzene 71-43-2 4.38 0.127 0.000528 0.00113
Bromobenzene 108-86-1 7.51 0.127 0.00102 0.0142
Bromodichloromethane 75-27-4 5.04 0.128 0.000820 0.00282
Bromoform 75-25-2 7.06 0.112 0.00132 0.0282
Bromomethane 74-83-9 2.25 0.0704 0.00223 0.0142
n-Butylbenzene 104-51-8 8.46 0.162 0.00594 0.0142
sec-Butylbenzene 135-98-8 8.03 0.154 0.00326 0.0142
tert-Butylbenzene 98-06-6 7.89 0.146 0.00221 0.00565
Carbon tetrachloride 56-23-5 4.14 0.124 0.00101 0.00565
Chlorobenzene 108-90-7 6.58 0.131 0.000237 0.00282
Chlorodibromomethane 124-48-1 6.06 0.125 0.000691 0.00282
Chloroethane 75-00-3 2.34 0.0660 0.00192 0.00565
Chloroform 67-66-3 4.04 0.128 0.00116 0.00282
Chloromethane 74-87-3 1.94 0.109 0.00492 0.0142
2-Chlorotoluene 95-49-8 7.64 0.138 0.000978 0.00282
4-Chlorotoluene 106-43-4 7.76 0.136 0.000508 0.00565
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.0974 0.00441 0.0282
1,2-Dibromoethane 106-93-4 6.24 0.130 0.000732 0.00282
Dibromomethane 74-95-3 4.97 0.119 0.000847 0.00565
1,2-Dichlorobenzene 95-50-1 8.62 0.139 0.000481 0.00565
1,3-Dichlorobenzene 541-73-1 8.22 0.136 0.000678 0.00565
1,4-Dichlorobenzene 106-46-7 8.28 0.132 0.000791 0.00565
Dichlorodifluoromethane 75-71-8 1.75 0.126 0.00182 0.00565
1,1-Dichloroethane 75-34-3 3.59 0.127 0.000555 0.00282
1,2-Dichloroethane 107-06-2 4.49 0.112 0.000733 0.00282
1,1-Dichloroethene 75-35-4 2.80 0.123 0.000685 0.00282
cis-1,2-Dichloroethene 156-59-2 3.89 0.135 0.000829 0.00282
trans-1,2-Dichloroethene 156-60-5 3.23 0.123 0.00117 0.00565
1,2-Dichloropropane 78-87-5 5.02 0.131 0.00160 0.00565
1,1-Dichloropropene 563-58-6 4.24 0.126 0.000914 0.00282
1,3-Dichloropropane 142-28-9 6.11 0.132 0.000566 0.00565
cis-1,3-Dichloropropene 10061-01-5 5.42 0.135 0.000856 0.00282
trans-1,3-Dichloropropene 10061-02-6 5.82 0.139 0.00128 0.00565
2,2-Dichloropropane 594-20-7 3.96 0.108 0.00156 0.00282
Di-isopropyl ether 108-20-3 3.49 0.131 0.000463 0.00113
Ethylbenzene 100-41-4 6.58 0.136 0.000833 0.00282
Hexachloro-1,3-butadiene 87-68-3 9.79 0.197 0.00678 0.0282
Isopropylbenzene 98-82-8 7.20 0.149 0.000481 0.00282
p-Isopropyltoluene 99-87-6 8.13 0.158 0.00289 0.00565
2-Butanone (MEK)78-93-3 4.19 0.447 0.0718 0.113
Methylene Chloride 75-09-2 3.16 0.126 0.00750 0.0282
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098455-5
Lab Sample ID:R4098455-5 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:0725_60 Received Date/Time:07/18/24 09:00
Instrument ID:VOCMS58 Preparation Date/Time:07/16/24 09:30
Analytical Batch:WG2329486 Analysis Date/Time:07/25/24 18:04
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):98.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.592 0.00258 0.0282
Methyl tert-butyl ether 1634-04-4 3.28 0.125 0.000395 0.00113
Naphthalene 91-20-3 10.08 0.121 0.00552 0.0142
n-Propylbenzene 103-65-1 7.50 0.137 0.00108 0.00565
Styrene 100-42-5 7.02 0.142 0.000259 0.0142
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.130 0.00107 0.00282
1,1,2,2-Tetrachloroethane 79-34-5 7.55 0.110 0.000786 0.00282
1,1,2-Trichlorotrifluoroethane 76-13-1 2.82 0.140 0.000851 0.00282
Tetrachloroethene 127-18-4 5.84 0.134 0.00101 0.00282
Toluene 108-88-3 5.58 0.129 0.00147 0.00565
1,2,3-Trichlorobenzene 87-61-6 10.25 0.161 0.00828 0.0142
1,2,4-Trichlorobenzene 120-82-1 9.82 0.166 0.00497 0.0142
1,1,1-Trichloroethane 71-55-6 4.17 0.134 0.00105 0.00282
1,1,2-Trichloroethane 79-00-5 5.93 0.135 0.000675 0.00282
Trichloroethene 79-01-6 4.71 0.138 0.000659 0.00113
Trichlorofluoromethane 75-69-4 2.44 0.0719 0.000935 0.00282
1,2,3-Trichloropropane 96-18-4 7.66 0.121 0.00183 0.0142
1,2,4-Trimethylbenzene 95-63-6 7.94 0.148 0.00179 0.00565
1,2,3-Trimethylbenzene 526-73-8 8.28 0.136 0.00179 0.00565
1,3,5-Trimethylbenzene 108-67-8 7.64 0.145 0.00226 0.00565
Vinyl chloride 75-01-4 2.01 0.123 0.00131 0.00282
Xylenes, Total 1330-20-7 6.98 0.424 0.000994 0.00734
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9071B Wet Chemistry
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (0-6)
Lab Sample ID:L1757957-01 SDG:L1757957
Client Sample ID:S-3 (0-6)Collected Date/Time:07/16/24 09:30
Lab File ID:10 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.49 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):98.6 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)251 J3 J6 P1 33.5 101
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (6-12)
Lab Sample ID:L1757957-02 SDG:L1757957
Client Sample ID:S-3 (6-12)Collected Date/Time:07/16/24 10:00
Lab File ID:11 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.06 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):92.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)162 35.9 109
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-30 (6-12)
Lab Sample ID:L1757957-03 SDG:L1757957
Client Sample ID:S-30 (6-12)Collected Date/Time:07/16/24 13:30
Lab File ID:12 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.08 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):92.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)150 35.6 108
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-9 (0-6)
Lab Sample ID:L1757957-04 SDG:L1757957
Client Sample ID:S-9 (0-6)Collected Date/Time:07/16/24 10:34
Lab File ID:13 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.11 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):97.8 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)445 33.7 102
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-8 (0-6)
Lab Sample ID:L1757957-05 SDG:L1757957
Client Sample ID:S-8 (0-6)Collected Date/Time:07/16/24 10:58
Lab File ID:14 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.12 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):98.2 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)362 33.6 102
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (0-6)
Lab Sample ID:L1757957-06 SDG:L1757957
Client Sample ID:S-7 (0-6)Collected Date/Time:07/16/24 11:20
Lab File ID:15 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.22 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):94.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)5380 35.1 106
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (6-12)
Lab Sample ID:L1757957-07 SDG:L1757957
Client Sample ID:S-7 (6-12)Collected Date/Time:07/16/24 11:35
Lab File ID:16 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.06 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):93.8 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)646 35.2 107
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (0-6)
Lab Sample ID:L1757957-08 SDG:L1757957
Client Sample ID:S-6 (0-6)Collected Date/Time:07/16/24 11:55
Lab File ID:17 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.07 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):98.1 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)2070 33.6 102
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-5 (0-6)
Lab Sample ID:L1757957-09 SDG:L1757957
Client Sample ID:S-5 (0-6)Collected Date/Time:07/16/24 13:15
Lab File ID:18 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.25 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):98.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)1440 33.4 101
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (0-6)
Lab Sample ID:L1757957-10 SDG:L1757957
Client Sample ID:S-4 (0-6)Collected Date/Time:07/16/24 13:30
Lab File ID:19 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.25 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):97.3 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)8270 33.9 103
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-31 (0-6)
Lab Sample ID:L1757957-11 SDG:L1757957
Client Sample ID:S-31 (0-6)Collected Date/Time:07/16/24 14:40
Lab File ID:20 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.24 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):97.2 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)11500 33.9 103
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-2 (0-6)
Lab Sample ID:L1757957-12 SDG:L1757957
Client Sample ID:S-2 (0-6)Collected Date/Time:07/16/24 13:55
Lab File ID:21 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.47 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):95.1 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)512 34.7 105
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (0-6)
Lab Sample ID:L1757957-13 SDG:L1757957
Client Sample ID:S-1 (0-6)Collected Date/Time:07/16/24 14:10
Lab File ID:22 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.08 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):93.1 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)852 35.4 107
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (6-12)
Lab Sample ID:L1757957-14 SDG:L1757957
Client Sample ID:S-1 (6-12)Collected Date/Time:07/16/24 14:25
Lab File ID:23 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.08 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):91.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)785 36.3 110
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (6-12)
Lab Sample ID:L1757957-15 SDG:L1757957
Client Sample ID:SS-1 (6-12)Collected Date/Time:07/16/24 14:41
Lab File ID:24 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:10.12 g
Matrix:Solid Initial Wt/Vol:_______________
Total Solids (%):85.6 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)1220 38.6 117
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098647-1
Lab Sample ID:R4098647-1 SDG:L1757957
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:29
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)U 33.0 100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098647-2
Lab Sample ID:R4098647-2 SDG:L1757957
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:05 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:29
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)4000 33.0 100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098647-4
Lab Sample ID:R4098647-4 SDG:L1757957
Client Sample ID:DUP Collected Date/Time:07/16/24 09:30
Lab File ID:04 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.09 g
Total Solids (%):98.6 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)372 P1 33.5 101
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098647-3
Lab Sample ID:R4098647-3 SDG:L1757957
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:06 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:29
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3660 33.0 100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098647-5
Lab Sample ID:R4098647-5 SDG:L1757957
Client Sample ID:MS Collected Date/Time:07/16/24 09:30
Lab File ID:07 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):98.6 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)4210 33.5 101
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4098647-6
Lab Sample ID:R4098647-6 SDG:L1757957
Client Sample ID:MSD Collected Date/Time:07/16/24 09:30
Lab File ID:08 Received Date/Time:07/18/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:07/25/24 16:30
Analytical Batch:WG2330146 Analysis Date/Time:07/25/24 23:08
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):98.6 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)2840 J3 J6 33.5 101
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3-IN BLANKS
SDG:L1757957 Calibration (begin) date/time:_______________
Instrument ID:OGBAL1 Calibration (end) date/time:_______________
Analytical Method:9071B Analytical Run:WG2330146
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte mg/kg
OIL & GREASE
(HEXANE EXTR)U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4098647-5
L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 R4098647-6
MS Sample / File ID:R4098647-5 / 07 SDG:L1757957
MSD Sample / File ID:R4098647-6 / 08 Analytical Batch:WG2330146
OS Sample / File ID:L1757957-01 / 10 Matrix:Solid
Instrument ID:OGBAL1
Analytical Method:9071B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Oil & Grease (Hexane Extr)4060 251 4210 2840 97.6 63.8*1 80.0 - 120 38.8*20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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6-IN DUPLICATES SAMPLE NO.:
L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 R4098647-4
DUP Sample / File ID:R4098647-4 / 04 SDG:L1757957
OS Sample / File ID:L1757957-01 / 10 Analytical Batch:WG2330146
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:9071B Matrix:Solid
Analyte
OS
Result
(dry)
DUP
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)251 372 38.7*20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098647-2
RECOVERY R4098647-3
L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
LCS Sample / File ID:R4098647-2 / 05 SDG:L1757957
LCSD Sample / File ID:R4098647-3 / 06 Analytical Batch:WG2330146
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:9071B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg %%%%%
Oil & Grease (Hexane Extr)4000 4000 3660 100 91.5 80.0 - 120 8.88 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1757957-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15 Analytical Method:9071B
Matrix:Solid Prep Method:9071B
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Oil & Grease (Hexane Extr)33 100
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12-IN ANALYSIS LOG
SDG:L1757957 Analytical Method:9071B
Instrument ID:OGBAL1 Calibration Start Date:_______________
Analytical Run:WG2330146 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4098647-1 01 07/25/24 23:08 1 WG2330146
DUP R4098647-4 04 07/25/24 23:08 1 WG2330146
LCS R4098647-2 05 07/25/24 23:08 1 WG2330146
LCSD R4098647-3 06 07/25/24 23:08 1 WG2330146
MS R4098647-5 07 07/25/24 23:08 1 WG2330146
MSD R4098647-6 08 07/25/24 23:08 1 WG2330146
S-3 (0-6)L1757957-01 10 07/25/24 23:08 1 WG2330146
S-7 (0-6)L1757957-06 15 07/25/24 23:08 1 WG2330146
S-7 (6-12)L1757957-07 16 07/25/24 23:08 1 WG2330146
S-3 (6-12)L1757957-02 11 07/25/24 23:08 1 WG2330146
S-5 (0-6)L1757957-09 18 07/25/24 23:08 1 WG2330146
S-6 (0-6)L1757957-08 17 07/25/24 23:08 1 WG2330146
S-4 (0-6)L1757957-10 19 07/25/24 23:08 1 WG2330146
S-8 (0-6)L1757957-05 14 07/25/24 23:08 1 WG2330146
S-9 (0-6)L1757957-04 13 07/25/24 23:08 1 WG2330146
S-1 (6-12)L1757957-14 23 07/25/24 23:08 1 WG2330146
S-31 (0-6)L1757957-11 20 07/25/24 23:08 1 WG2330146
SS-1 (6-12)L1757957-15 24 07/25/24 23:08 1 WG2330146
S-1 (0-6)L1757957-13 22 07/25/24 23:08 1 WG2330146
S-30 (6-12)L1757957-03 12 07/25/24 23:08 1 WG2330146
S-2 (0-6)L1757957-12 21 07/25/24 23:08 1 WG2330146
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
COD Coefficient of Determination.
Corr.Correlation Coefficient.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
Incpt Intercept.
Mass Mass of parameter.
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
RRF Relative Response Factor.
RT Retention Time.
SDG Sample Delivery Group.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Slope Slope of calibration curve.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Wavelength Wavelength of parameter.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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GLOSSARY OF TERMS
Qualifier Description
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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ANALYTICAL REPORT
October 18, 2024
Geosyntec Consultants - UT
Sample Delivery Group:L1784578
Samples Received:10/02/2024
Project Number:SLC1091
Description:Paxton Ave.
Report To:Brian Smith
215 South State Street
Suite 500
Salt Lake City, UT 84111
Entire Report Reviewed By:
October 18, 2024
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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October 18, 2024
Chris Ward
Project Manager
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TABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 15
Cn: Case Narrative 19
Su: Summary Results 20
1664B Wet Chemistry 20
Sample Result Inorganic Analysis Data Sheet 21
L1784578-17 10/12/24 15:02 OGBAL1 21
BLANK(R4131931-1) WG2380187 10/12/24 15:02 OGBAL1 22
LCS(R4131931-2) WG2380187 10/12/24 15:02 OGBAL1 23
LCSD(R4131931-3) WG2380187 10/12/24 15:02 OGBAL1 24
MS(R4131931-4) WG2380187 10/12/24 15:02 OGBAL1 25
Blank 26
OGBAL1 WG2380187 26
Matrix Spike / Duplicate 27
WG2380187 MS(R4131931-4) 27
Laboratory Control Sample / Duplicate 28
WG2380187 LCS(R4131931-2) LCSD(R4131931-3) 28
Detection Limit Summary 29
1664B - GW 29
Analysis Log 30
OGBAL1 WG2380187 30
2540 G-2011 Total Solids 31
Sample Result Inorganic Analysis Data Sheet 32
L1784578-01 10/05/24 15:11 LOGBAL1 32
L1784578-02 10/05/24 15:11 LOGBAL1 33
L1784578-03 10/05/24 15:11 LOGBAL1 34
L1784578-04 10/05/24 15:11 LOGBAL1 35
L1784578-05 10/05/24 15:11 LOGBAL1 36
L1784578-06 10/05/24 15:11 LOGBAL1 37
L1784578-07 10/05/24 15:11 LOGBAL1 38
L1784578-08 10/05/24 15:11 LOGBAL1 39
L1784578-09 10/05/24 15:11 LOGBAL1 40
L1784578-10 10/05/24 15:11 LOGBAL1 41
L1784578-11 10/05/24 14:56 LOGBAL1 42
L1784578-12 10/05/24 14:56 LOGBAL1 43
L1784578-13 10/05/24 14:56 LOGBAL1 44
L1784578-14 10/05/24 14:56 LOGBAL1 45
L1784578-15 10/05/24 14:56 LOGBAL1 46
L1784578-16 10/05/24 16:52 LOGBAL1 47
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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BLANK(R4129340-1) WG2376182 10/05/24 14:56 LOGBAL1 48
BLANK(R4129341-1) WG2376181 10/05/24 15:11 LOGBAL1 49
BLANK(R4129364-1) WG2376477 10/05/24 16:52 LOGBAL1 50
DUP(R4129340-3) WG2376182 10/05/24 14:56 LOGBAL1 51
LCS(R4129340-2) WG2376182 10/05/24 14:56 LOGBAL1 52
LCS(R4129341-2) WG2376181 10/05/24 15:11 LOGBAL1 53
LCS(R4129364-2) WG2376477 10/05/24 16:52 LOGBAL1 54
DUP(R4129341-3) WG2376181 10/05/24 15:11 LOGBAL1 55
DUP(R4129364-3) WG2376477 10/05/24 16:52 LOGBAL1 56
Blank 57
LOGBAL1 WG2376182 57
LOGBAL1 WG2376181 58
LOGBAL1 WG2376477 59
Laboratory Duplicate 60
WG2376182 DUP(R4129340-3) 60
WG2376181 DUP(R4129341-3) 61
WG2376477 DUP(R4129364-3) 62
Laboratory Control Sample / Duplicate 63
WG2376182 LCS(R4129340-2) 63
WG2376181 LCS(R4129341-2) 64
WG2376477 LCS(R4129364-2) 65
Detection Limit Summary 66
2540 G-2011 - Solid 66
Analysis Log 67
LOGBAL1 WG2376182 67
LOGBAL1 WG2376181 68
LOGBAL1 WG2376477 69
3511/8015 Semi-Volatile Organic Compounds (GC) 70
Surrogate Recovery 71
GW Surrogate Summary 71
Laboratory Control Sample / Duplicate 72
WG2380823 LCS(R4132895-2) LCSD(R4132895-3) 72
Method Blank 73
WG2380823 R4132895-1 SVGC26 10/14/24 00:13 73
Sample Result Summary Organic Analysis Data Sheet 74
L1784578-17 10/14/24 02:54 SVGC26 74
Retention Time of Single Component Analytes 75
SVGC26 09/24/24 14:13 75
Calibration Factor of Single Component Analytes 76
SVGC26 09/24/24 14:13 76
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Calibration Verification Single Component Analytes 78
SVGC26 09/24/24 18:32 78
SVGC26 10/13/24 22:08 79
SVGC26 10/14/24 08:36 80
Analytical Sequence 81
SVGC26 09/24/24 14:13 81
Detection Limit Summary 82
3511/8015 - GW 82
QC Result Summary Organic Analysis Data Sheet 83
BLANK(R4132895-1) WG2380823 10/14/24 00:13 SVGC26 83
LCS(R4132895-2) WG2380823 10/14/24 00:33 SVGC26 84
LCSD(R4132895-3) WG2380823 10/14/24 00:53 SVGC26 85
6010B Metals (ICP) 86
Sample Result Inorganic Analysis Data Sheet 87
L1784578-01 10/11/24 11:36 ICP17 87
L1784578-02 10/11/24 11:41 ICP17 88
L1784578-03 10/11/24 11:43 ICP17 89
L1784578-04 10/11/24 11:45 ICP17 90
L1784578-05 10/11/24 11:46 ICP17 91
L1784578-06 10/11/24 11:25 ICP17 92
L1784578-07 10/11/24 11:48 ICP17 93
L1784578-09 10/11/24 11:50 ICP17 94
L1784578-10 10/11/24 11:51 ICP17 95
L1784578-11 10/11/24 11:53 ICP17 96
L1784578-12 10/11/24 11:55 ICP17 97
L1784578-13 10/11/24 11:56 ICP17 98
L1784578-14 10/11/24 12:01 ICP17 99
L1784578-15 10/11/24 12:03 ICP17 100
L1784578-16 10/07/24 14:05 ICP17 101
L1784578-17 10/16/24 15:19 ICP17 102
BLANK(R4129463-1) WG2376546 10/07/24 12:47 ICP17 103
BLANK(R4131568-1) WG2376598 10/11/24 11:21 ICP17 104
BLANK(R4133611-1) WG2378117 10/16/24 14:48 ICP17 105
LCS(R4129463-2) WG2376546 10/07/24 12:48 ICP17 106
LCS(R4131568-2) WG2376598 10/11/24 11:23 ICP17 107
LCS(R4133611-2) WG2378117 10/16/24 14:50 ICP17 108
MS(R4129463-5) WG2376546 10/07/24 12:55 ICP17 109
MS(R4131568-5) WG2376598 10/11/24 11:30 ICP17 110
MS(R4133611-4) WG2378117 10/16/24 14:55 ICP17 111
MSD(R4129463-6) WG2376546 10/07/24 12:57 ICP17 112
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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MSD(R4131568-6) WG2376598 10/11/24 11:31 ICP17 113
MSD(R4133611-5) WG2378117 10/16/24 14:57 ICP17 114
PS(R4129463-4) WG2376546 10/07/24 12:53 ICP17 115
PS(R4131568-4) WG2376598 10/11/24 11:28 ICP17 116
SD(R4129463-3) WG2376546 10/07/24 12:52 ICP17 117
SD(R4131568-3) WG2376598 10/11/24 11:26 ICP17 118
SD(R4133611-3) WG2378117 10/16/24 14:54 ICP17 119
Calibration Verification 120
ICP17 100724ICP17 120
ICP17 101124ICP17 122
ICP17 101624ICP17 125
Blank 127
ICP17 100724ICP17 127
ICP17 101124ICP17 129
ICP17 101624ICP17 131
ICP Interference Check Sample 133
ICP17 10/07/24 09:09 133
ICP17 10/07/24 13:27 134
ICP17 10/07/24 20:20 135
ICP17 10/11/24 08:44 136
ICP17 10/11/24 14:17 137
ICP17 10/16/24 07:02 138
ICP17 10/16/24 13:56 139
ICP17 10/16/24 16:55 140
Matrix Spike / Duplicate 141
WG2376546 MS(R4129463-5) MSD(R4129463-6) 141
WG2376598 MS(R4131568-5) MSD(R4131568-6) 142
WG2378117 MS(R4133611-4) MSD(R4133611-5) 143
Post Digestion Spike 144
WG2376546 PS(R4129463-4) 144
WG2376598 PS(R4131568-4) 145
Laboratory Control Sample / Duplicate 146
WG2376546 LCS(R4129463-2) 146
WG2376598 LCS(R4131568-2) 147
WG2378117 LCS(R4133611-2) 148
Serial Dilution 149
WG2376546 SD(R4129463-3) 149
WG2376598 SD(R4131568-3) 150
WG2378117 SD(R4133611-3) 151
Detection Limit Summary 152
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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6010B - GW 152
6010B - Solid 153
Linear Dynamic Range 154
ICP17 06/09/24 17:06 154
Analysis Log 155
ICP17 100724ICP17 10/07/24 08:46 155
ICP17 101124ICP17 10/11/24 08:18 156
ICP17 101624ICP17 10/16/24 06:39 157
Initial Calibration Recovery 158
ICP17 101624ICP17 10/16/24 06:39 158
ICP17 100724ICP17 10/07/24 08:46 161
ICP17 101124ICP17 10/11/24 08:18 164
Initial Calibration 167
ICP17 101624ICP17 10/16/24 06:39 167
ICP17 100724ICP17 10/07/24 08:46 168
ICP17 101124ICP17 10/11/24 08:18 169
7470A Mercury 170
Sample Result Inorganic Analysis Data Sheet 171
L1784578-17 10/05/24 14:51 CVAA9 171
BLANK(R4128943-1) WG2375204 10/05/24 14:06 CVAA9 172
LCS(R4128943-2) WG2375204 10/05/24 14:08 CVAA9 173
MS(R4128943-4) WG2375204 10/05/24 14:16 CVAA9 174
MSD(R4128943-5) WG2375204 10/05/24 14:18 CVAA9 175
PS(R4128943-6) WG2375204 10/05/24 16:47 CVAA9 176
SD(R4128943-3) WG2375204 10/05/24 14:13 CVAA9 177
Calibration Verification 178
CVAA9 100524CVAA9 WE 178
Blank 181
CVAA9 100524CVAA9 WE 181
Matrix Spike / Duplicate 183
WG2375204 MS(R4128943-4) MSD(R4128943-5) 183
Post Digestion Spike 184
WG2375204 PS(R4128943-6) 184
Laboratory Control Sample / Duplicate 185
WG2375204 LCS(R4128943-2) 185
Serial Dilution 186
WG2375204 SD(R4128943-3) 186
Detection Limit Summary 187
7470A - GW 187
Linear Dynamic Range 188
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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CVAA9 07/10/23 14:11 188
Analysis Log 189
CVAA9 100524CVAA9 WE 10/05/24 11:31 189
Initial Calibration Recovery 190
CVAA9 100524CVAA9 WE 10/05/24 11:31 190
Initial Calibration 193
CVAA9 100524CVAA9 WE 10/05/24 11:31 193
7471B Mercury 194
Sample Result Inorganic Analysis Data Sheet 195
L1784578-01 10/07/24 13:59 CVAA10 195
L1784578-02 10/07/24 14:02 CVAA10 196
L1784578-03 10/07/24 14:04 CVAA10 197
L1784578-04 10/07/24 14:07 CVAA10 198
L1784578-05 10/07/24 14:15 CVAA10 199
L1784578-06 10/07/24 13:15 CVAA10 200
L1784578-11 10/07/24 14:17 CVAA10 201
L1784578-12 10/07/24 14:20 CVAA10 202
L1784578-13 10/07/24 14:23 CVAA10 203
L1784578-15 10/07/24 14:25 CVAA10 204
BLANK(R4129510-1) WG2376309 10/07/24 13:09 CVAA10 205
LCS(R4129510-2) WG2376309 10/07/24 13:12 CVAA10 206
MS(R4129510-4) WG2376309 10/07/24 13:20 CVAA10 207
MSD(R4129510-5) WG2376309 10/07/24 13:23 CVAA10 208
SD(R4129510-3) WG2376309 10/07/24 13:17 CVAA10 209
Calibration Verification 210
CVAA10 100724CVAA10 S 210
Blank 213
CVAA10 100724CVAA10 S 213
Matrix Spike / Duplicate 215
WG2376309 MS(R4129510-4) MSD(R4129510-5) 215
Laboratory Control Sample / Duplicate 216
WG2376309 LCS(R4129510-2) 216
Serial Dilution 217
WG2376309 SD(R4129510-3) 217
Detection Limit Summary 218
7471B - Solid 218
Analysis Log 219
CVAA10 100724CVAA10 S 10/07/24 09:21 219
Initial Calibration Recovery 220
CVAA10 100724CVAA10 S 10/07/24 09:21 220
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Initial Calibration 222
CVAA10 100724CVAA10 S 10/07/24 09:21 222
8015 Semi-Volatile Organic Compounds (GC) 223
Surrogate Recovery 224
Solid Surrogate Summary 224
Matrix Spike / Duplicate 225
WG2380134 MS(R4131935-1) MSD(R4131935-2) 225
WG2380815 MS(R4133395-3) MSD(R4133395-4) 226
Laboratory Control Sample / Duplicate 227
WG2380134 LCS(R4131845-2) 227
WG2380815 LCS(R4133395-2) 228
Method Blank 229
WG2380134 R4131845-1 SVGC50 10/11/24 20:04 229
WG2380815 R4133395-1 SVGC50 10/15/24 16:52 230
Sample Result Summary Organic Analysis Data Sheet 231
L1784578-01 10/15/24 18:44 SVGC50 231
L1784578-02 10/11/24 23:35 SVGC50 232
L1784578-03 10/15/24 18:32 SVGC50 233
L1784578-04 10/12/24 11:11 SVGC7 234
L1784578-05 10/12/24 12:03 SVGC7 235
L1784578-06 10/12/24 11:24 SVGC7 236
L1784578-11 10/11/24 23:59 SVGC50 237
L1784578-12 10/15/24 18:56 SVGC50 238
L1784578-13 10/15/24 19:21 SVGC50 239
L1784578-15 10/15/24 17:54 SVGC50 240
Retention Time of Single Component Analytes 241
SVGC7 08/02/24 19:00 241
SVGC50 06/26/24 17:36 242
SVGC50 06/26/24 17:36 243
Calibration Factor of Single Component Analytes 244
SVGC7 08/02/24 19:00 244
SVGC50 06/26/24 17:36 246
SVGC50 06/26/24 17:36 248
Calibration Verification Single Component Analytes 250
SVGC7 08/03/24 00:00 250
SVGC7 10/12/24 09:56 251
SVGC7 10/12/24 13:34 252
SVGC50 06/26/24 22:32 253
SVGC50 10/11/24 09:09 254
SVGC50 10/11/24 19:27 255
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SVGC50 10/12/24 01:39 256
SVGC50 10/15/24 16:15 257
SVGC50 10/15/24 19:46 258
Analytical Sequence 259
SVGC7 08/02/24 19:00 259
SVGC50 06/26/24 17:36 260
SVGC50 06/26/24 17:36 261
Detection Limit Summary 262
8015 - Solid 262
QC Result Summary Organic Analysis Data Sheet 263
BLANK(R4131845-1) WG2380134 10/11/24 20:04 SVGC50 263
BLANK(R4133395-1) WG2380815 10/15/24 16:52 SVGC50 264
LCS(R4131845-2) WG2380134 10/11/24 20:16 SVGC50 265
LCS(R4133395-2) WG2380815 10/15/24 17:05 SVGC50 266
MS(R4131935-1) WG2380134 10/12/24 11:37 SVGC7 267
MS(R4133395-3) WG2380815 10/15/24 17:30 SVGC50 268
MSD(R4131935-2) WG2380134 10/12/24 11:50 SVGC7 269
MSD(R4133395-4) WG2380815 10/15/24 17:42 SVGC50 270
8015D/GRO Volatile Organic Compounds (GC) 271
Surrogate Recovery 272
GW Surrogate Summary 272
Solid Surrogate Summary 273
Matrix Spike / Duplicate 274
WG2378256 MS(R4130871-4) MSD(R4130871-5) 274
WG2378697 MS(R4131083-4) MSD(R4131083-5) 275
WG2377924 MS(R4132130-4) MSD(R4132130-5) 276
Laboratory Control Sample / Duplicate 277
WG2377829 LCS(R4130869-1) 277
WG2378256 LCS(R4130871-1) LCSD(R4130871-2) 278
WG2378697 LCS(R4131083-1) LCSD(R4131083-2) 279
WG2377924 LCS(R4132130-1) LCSD(R4132130-2) 280
Method Blank 281
WG2378697 R4131083-3 VOCGC12 10/09/24 10:15 281
WG2377924 R4132130-3 VOCGC15 10/08/24 13:22 282
WG2377829 R4130869-2 VOCGC17 10/08/24 10:10 283
WG2378256 R4130871-3 VOCGC17 10/08/24 22:07 284
Internal Standard & Retention Time 285
VOCGC12 10/09/24 09:09 285
VOCGC15 10/08/24 11:19 286
VOCGC15 10/08/24 17:22 287
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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VOCGC17 10/08/24 08:51 288
VOCGC17 10/08/24 20:14 289
Sample Result Summary Organic Analysis Data Sheet 290
L1784578-01 10/08/24 15:59 VOCGC17 290
L1784578-02 10/08/24 16:18 VOCGC17 291
L1784578-03 10/08/24 16:38 VOCGC17 292
L1784578-04 10/08/24 16:57 VOCGC17 293
L1784578-05 10/08/24 17:17 VOCGC17 294
L1784578-06 10/09/24 02:36 VOCGC17 295
L1784578-11 10/08/24 21:11 VOCGC15 296
L1784578-12 10/08/24 21:35 VOCGC15 297
L1784578-13 10/08/24 21:58 VOCGC15 298
L1784578-15 10/08/24 22:21 VOCGC15 299
L1784578-17 10/09/24 12:31 VOCGC12 300
Retention Time of Single Component Analytes 301
VOCGC12 05/23/24 00:27 301
VOCGC15 06/26/24 14:42 302
VOCGC17 08/28/24 16:05 303
Calibration Factor of Single Component Analytes 304
VOCGC12 05/23/24 00:27 304
VOCGC15 06/26/24 14:42 306
VOCGC17 08/28/24 16:05 308
Calibration Verification Single Component Analytes 310
VOCGC12 05/23/24 06:03 310
VOCGC12 10/09/24 09:09 311
VOCGC15 06/26/24 22:05 312
VOCGC15 10/08/24 11:19 313
VOCGC15 10/08/24 17:22 314
VOCGC17 08/28/24 19:00 315
VOCGC17 10/08/24 08:51 316
VOCGC17 10/08/24 20:14 317
Analytical Sequence 318
VOCGC12 05/23/24 00:27 318
VOCGC15 06/26/24 14:42 319
VOCGC17 08/28/24 16:05 320
Detection Limit Summary 322
8015D/GRO - GW 322
8015D/GRO - Solid 323
QC Result Summary Organic Analysis Data Sheet 324
BLANK(R4130869-2) WG2377829 10/08/24 10:10 VOCGC17 324
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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BLANK(R4130871-3) WG2378256 10/08/24 22:07 VOCGC17 325
BLANK(R4131083-3) WG2378697 10/09/24 10:15 VOCGC12 326
BLANK(R4132130-3) WG2377924 10/08/24 13:22 VOCGC15 327
LCS(R4130869-1) WG2377829 10/08/24 09:11 VOCGC17 328
LCS(R4130871-1) WG2378256 10/08/24 20:34 VOCGC17 329
LCS(R4131083-1) WG2378697 10/09/24 09:09 VOCGC12 330
LCS(R4132130-1) WG2377924 10/08/24 11:43 VOCGC15 331
LCSD(R4130871-2) WG2378256 10/08/24 21:09 VOCGC17 332
LCSD(R4131083-2) WG2378697 10/09/24 09:31 VOCGC12 333
LCSD(R4132130-2) WG2377924 10/08/24 12:06 VOCGC15 334
MS(R4130871-4) WG2378256 10/09/24 06:48 VOCGC17 335
MS(R4131083-4) WG2378697 10/09/24 19:28 VOCGC12 336
MS(R4132130-4) WG2377924 10/08/24 23:40 VOCGC15 337
MSD(R4130871-5) WG2378256 10/09/24 07:08 VOCGC17 338
MSD(R4131083-5) WG2378697 10/09/24 19:50 VOCGC12 339
MSD(R4132130-5) WG2377924 10/09/24 00:05 VOCGC15 340
8260B Volatile Organic Compounds (GC/MS) 341
Surrogate Recovery 342
GW Surrogate Summary 342
Solid Surrogate Summary 343
Matrix Spike / Duplicate 344
WG2379147 MS(R4131341-4) MSD(R4131341-5) 344
WG2380545 MS(R4132125-3) MSD(R4132125-4) 346
Laboratory Control Sample / Duplicate 348
WG2379147 LCS(R4131341-1) LCSD(R4131341-2) 348
WG2380092 LCS(R4131396-1) 350
WG2380545 LCS(R4132125-1) 352
WG2379334 LCS(R4132481-1) LCSD(R4132481-2) 354
WG2381936 LCS(R4133124-1) LCSD(R4133124-2) 356
Method Blank 357
WG2380092 R4131396-3 VOCMS16 10/10/24 22:33 357
WG2379334 R4132481-3 VOCMS36 10/10/24 05:50 358
WG2381936 R4133124-3 VOCMS42 10/15/24 09:42 359
WG2380545 R4132125-2 VOCMS56 10/12/24 04:44 360
WG2379147 R4131341-3 VOCMS59 10/11/24 02:15 361
GC/MS Performance Check 362
VOCMS16 092224 09/22/24 16:25 362
VOCMS16 101024 10/10/24 21:27 363
VOCMS36 091224 09/12/24 16:31 364
VOCMS36 091224 09/12/24 23:26 365
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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VOCMS36 091224 09/13/24 09:20 366
VOCMS36 101024 10/10/24 03:27 367
VOCMS42 100324a 10/03/24 14:22 368
VOCMS42 101524 10/15/24 08:43 369
VOCMS56 100824a 10/08/24 21:52 370
VOCMS56 101124a 10/12/24 03:09 371
VOCMS59 100724 10/07/24 17:05 372
VOCMS59 101124 10/11/24 00:19 373
Internal Standard & Retention Time 374
VOCMS16 10/10/24 21:27 374
VOCMS36 10/10/24 03:47 375
VOCMS42 10/15/24 08:43 376
VOCMS56 10/12/24 03:47 377
VOCMS59 10/11/24 00:38 378
Sample Result Summary Organic Analysis Data Sheet 379
L1784578-01 10/12/24 07:53 VOCMS56 379
L1784578-02 10/11/24 06:08 VOCMS59 381
L1784578-03 10/12/24 08:12 VOCMS56 383
L1784578-04 10/11/24 06:28 VOCMS59 385
L1784578-05 10/11/24 06:47 VOCMS59 387
L1784578-06 10/11/24 07:07 VOCMS59 389
L1784578-11 10/11/24 07:26 VOCMS59 391
L1784578-12 10/12/24 08:31 VOCMS56 393
L1784578-13 10/12/24 08:50 VOCMS56 395
L1784578-15 10/12/24 09:09 VOCMS56 397
L1784578-17 10/11/24 01:18 VOCMS16 399
L1784578-18 10/10/24 06:31 VOCMS36 401
L1784578-18 10/15/24 10:43 VOCMS42 403
GC/MS Initial Calibration 404
VOCMS16 09/22/24 17:10 404
VOCMS36 09/12/24 18:56 408
VOCMS42 10/03/24 15:22 412
VOCMS56 10/08/24 22:49 414
VOCMS59 10/07/24 18:03 418
GC/MS Calibration Verification 422
VOCMS16 09/22/24 21:13 422
VOCMS16 10/10/24 21:27 424
VOCMS36 09/12/24 22:44 426
VOCMS36 09/13/24 14:12 427
VOCMS36 10/10/24 03:47 429
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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VOCMS42 10/03/24 19:59 431
VOCMS42 10/15/24 08:43 433
VOCMS56 10/09/24 03:13 435
VOCMS56 10/12/24 03:47 437
VOCMS59 10/07/24 22:36 439
VOCMS59 10/11/24 00:38 441
Analytical Sequence 443
VOCMS16 09/22/24 17:10 443
VOCMS36 09/12/24 18:56 445
VOCMS42 10/03/24 15:22 446
VOCMS56 10/08/24 22:49 447
VOCMS59 10/07/24 18:03 448
Detection Limit Summary 449
8260B - GW 449
8260B - Solid 451
QC Result Summary Organic Analysis Data Sheet 453
BLANK(R4131341-3) WG2379147 10/11/24 02:15 VOCMS59 453
BLANK(R4131396-3) WG2380092 10/10/24 22:33 VOCMS16 455
BLANK(R4132125-2) WG2380545 10/12/24 04:44 VOCMS56 457
BLANK(R4132481-3) WG2379334 10/10/24 05:50 VOCMS36 459
BLANK(R4133124-3) WG2381936 10/15/24 09:42 VOCMS42 461
LCS(R4131341-1) WG2379147 10/11/24 00:38 VOCMS59 462
LCS(R4131396-1) WG2380092 10/10/24 21:27 VOCMS16 464
LCS(R4132125-1) WG2380545 10/12/24 03:47 VOCMS56 466
LCS(R4132481-1) WG2379334 10/10/24 03:47 VOCMS36 468
LCS(R4133124-1) WG2381936 10/15/24 08:43 VOCMS42 470
LCSD(R4131341-2) WG2379147 10/11/24 00:57 VOCMS59 471
LCSD(R4132481-2) WG2379334 10/10/24 04:07 VOCMS36 473
LCSD(R4133124-2) WG2381936 10/15/24 09:03 VOCMS42 475
MS(R4131341-4) WG2379147 10/11/24 09:04 VOCMS59 476
MS(R4132125-3) WG2380545 10/12/24 12:38 VOCMS56 478
MSD(R4131341-5) WG2379147 10/11/24 09:24 VOCMS59 480
MSD(R4132125-4) WG2380545 10/12/24 12:57 VOCMS56 482
9071B Wet Chemistry 484
Sample Result Inorganic Analysis Data Sheet 485
L1784578-01 10/08/24 21:31 OGBAL1 485
L1784578-02 10/08/24 21:31 OGBAL1 486
L1784578-03 10/08/24 21:31 OGBAL1 487
L1784578-04 10/10/24 14:22 OGBAL1 488
L1784578-05 10/10/24 14:22 OGBAL1 489
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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L1784578-06 10/10/24 14:22 OGBAL1 490
L1784578-07 10/10/24 14:22 OGBAL1 491
L1784578-08 10/10/24 14:22 OGBAL1 492
L1784578-11 10/10/24 14:22 OGBAL1 493
L1784578-12 10/10/24 14:22 OGBAL1 494
L1784578-13 10/10/24 14:22 OGBAL1 495
L1784578-14 10/10/24 14:22 OGBAL1 496
L1784578-15 10/10/24 14:22 OGBAL1 497
BLANK(R4130193-1) WG2378003 10/08/24 21:31 OGBAL1 498
BLANK(R4131067-1) WG2378468 10/10/24 14:22 OGBAL1 499
DUP(R4130193-4) WG2378003 10/08/24 21:31 OGBAL1 500
DUP(R4131067-4) WG2378468 10/10/24 14:22 OGBAL1 501
LCS(R4130193-2) WG2378003 10/08/24 21:31 OGBAL1 502
LCS(R4131067-2) WG2378468 10/10/24 14:22 OGBAL1 503
LCSD(R4130193-3) WG2378003 10/08/24 21:31 OGBAL1 504
LCSD(R4131067-3) WG2378468 10/10/24 14:22 OGBAL1 505
MS(R4130193-5) WG2378003 10/08/24 21:31 OGBAL1 506
MS(R4131067-5) WG2378468 10/10/24 14:22 OGBAL1 507
MSD(R4130193-6) WG2378003 10/08/24 21:31 OGBAL1 508
MSD(R4131067-6) WG2378468 10/10/24 14:22 OGBAL1 509
Blank 510
OGBAL1 WG2378003 510
OGBAL1 WG2378468 511
Matrix Spike / Duplicate 512
WG2378003 MS(R4130193-5) MSD(R4130193-6) 512
WG2378468 MS(R4131067-5) MSD(R4131067-6) 513
Laboratory Duplicate 514
WG2378003 DUP(R4130193-4) 514
WG2378468 DUP(R4131067-4) 515
Laboratory Control Sample / Duplicate 516
WG2378003 LCS(R4130193-2) LCSD(R4130193-3) 516
WG2378468 LCS(R4131067-2) LCSD(R4131067-3) 517
Detection Limit Summary 518
9071B - Solid 518
Analysis Log 519
OGBAL1 WG2378003 519
OGBAL1 WG2378468 520
Gl: Glossary of Terms 521
Al: Accreditations & Locations 523
Sc: Sample Chain of Custody 524
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-13 (0-6) L1784578-01 Solid Jessica Welch 09/30/24 10:00 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378003 1 10/08/24 15:16 10/08/24 21:31 DAL Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 13:59 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:36 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377829 25 09/30/24 10:00 10/08/24 15:59 CDD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2380545 1 09/30/24 10:00 10/12/24 07:53 AV Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380815 1 10/12/24 19:39 10/15/24 18:44 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-15 (0-6) L1784578-02 Solid Jessica Welch 09/27/24 14:25 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378003 1 10/08/24 15:16 10/08/24 21:31 DAL Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:02 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:41 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377829 27 09/27/24 14:25 10/08/24 16:18 CDD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2379147 1.08 09/27/24 14:25 10/11/24 06:08 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380134 5 10/11/24 08:02 10/11/24 23:35 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-32 (0-6) L1784578-03 Solid Jessica Welch 09/30/24 10:10 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378003 1 10/08/24 15:16 10/08/24 21:31 DAL Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:04 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:43 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377829 25 09/30/24 10:10 10/08/24 16:38 CDD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2380545 1 09/30/24 10:10 10/12/24 08:12 AV Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380815 1 10/12/24 19:39 10/15/24 18:32 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-12 (6-12) L1784578-04 Solid Jessica Welch 09/27/24 16:05 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:07 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:45 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377829 25 09/27/24 16:05 10/08/24 16:57 CDD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2379147 1 09/27/24 16:05 10/11/24 06:28 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380134 50 10/11/24 08:02 10/12/24 11:11 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-12 (0-6) L1784578-05 Solid Jessica Welch 09/27/24 15:50 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:15 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:46 JTM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-12 (0-6) L1784578-05 Solid Jessica Welch 09/27/24 15:50 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377829 25 09/27/24 15:50 10/08/24 17:17 CDD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2379147 1 09/27/24 15:50 10/11/24 06:47 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380134 10 10/11/24 08:02 10/12/24 12:03 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-10 (0-6) L1784578-06 Solid Jessica Welch 09/27/24 12:00 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 13:15 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:25 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2378256 34.5 09/27/24 12:00 10/09/24 02:36 CDD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2379147 1.13 09/27/24 12:00 10/11/24 07:07 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380134 20 10/11/24 08:02 10/12/24 11:24 JDG Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-4 (12-18) L1784578-07 Solid Jessica Welch 09/27/24 15:05 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:48 JTM Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-6 (12-18) L1784578-08 Solid Jessica Welch 09/27/24 15:20 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-1 (12-18) L1784578-09 Solid Jessica Welch 09/27/24 14:40 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:50 JTM Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-7 (12-18) L1784578-10 Solid Jessica Welch 09/27/24 15:30 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 CMB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:51 JTM Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-10 (6-12) L1784578-11 Solid Jessica Welch 09/27/24 12:30 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376182 1 10/05/24 14:43 10/05/24 14:56 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:17 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:53 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377924 28 09/27/24 12:30 10/08/24 21:11 NCD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2379147 1.12 09/27/24 12:30 10/11/24 07:26 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380134 10 10/11/24 08:02 10/11/24 23:59 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-14 (0-6) L1784578-12 Solid Jessica Welch 09/30/24 09:10 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376182 1 10/05/24 14:43 10/05/24 14:56 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:20 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:55 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377924 27.5 09/30/24 09:10 10/08/24 21:35 NCD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2380545 1.1 09/30/24 09:10 10/12/24 08:31 AV Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380815 2 10/12/24 19:39 10/15/24 18:56 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-11 (0-6) L1784578-13 Solid Jessica Welch 09/30/24 08:40 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376182 1 10/05/24 14:43 10/05/24 14:56 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:23 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 11:56 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377924 25 09/30/24 08:40 10/08/24 21:58 NCD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2380545 1 09/30/24 08:40 10/12/24 08:50 AV Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380815 20 10/12/24 19:39 10/15/24 19:21 KKS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-1 (12-18) L1784578-14 Solid Jessica Welch 09/30/24 10:25 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376182 1 10/05/24 14:43 10/05/24 14:56 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 12:01 JTM Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-14 (6-12) L1784578-15 Solid Jessica Welch 09/30/24 09:20 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376182 1 10/05/24 14:43 10/05/24 14:56 CMB Mt. Juliet, TN
Wet Chemistry by Method 9071B WG2378468 1 10/09/24 15:05 10/10/24 14:22 MAB Mt. Juliet, TN
Mercury by Method 7471B WG2376309 1 10/06/24 18:02 10/07/24 14:25 NDL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376598 1 10/10/24 23:50 10/11/24 12:03 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2377924 27.5 09/30/24 09:20 10/08/24 22:21 NCD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2380545 1.1 09/30/24 09:20 10/12/24 09:09 AV Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG2380815 1 10/12/24 19:39 10/15/24 17:54 KKS Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-3 (12-18) L1784578-16 Solid Jessica Welch 09/27/24 11:00 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376477 1 10/05/24 16:38 10/05/24 16:52 CMB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2376546 1 10/05/24 22:06 10/07/24 14:05 ZSA Mt. Juliet, TN
Collected by Collected date/time Received date/time
EB-93024 L1784578-17 GW Jessica Welch 09/30/24 10:35 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664B WG2380187 1 10/11/24 10:25 10/12/24 15:02 CLC Mt. Juliet, TN
Mercury by Method 7470A WG2375204 1 10/04/24 10:11 10/05/24 14:51 LAS Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2378117 1 10/16/24 09:44 10/16/24 15:19 MAP Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2378697 1 10/09/24 12:31 10/09/24 12:31 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2380092 1 10/11/24 01:18 10/11/24 01:18 WHS Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2380823 1 10/12/24 11:49 10/14/24 02:54 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
TRIP BLANK L1784578-18 GW Jessica Welch 09/27/24 00:00 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG2379334 1 10/10/24 06:31 10/10/24 06:31 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2381936 1 10/15/24 10:43 10/15/24 10:43 JHH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 10/17/24 13:33
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Chris Ward
Project Manager
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1664B Wet Chemistry
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:25 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/11/24 10:25
Analytical Batch:WG2380187 Analysis Date/Time:10/12/24 15:02
Dilution Factor:1 Prep Method:1664B
Analytical Method:1664B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:890 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.57 5.62
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131931-1
Lab Sample ID:R4131931-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/11/24 10:25
Analytical Batch:WG2380187 Analysis Date/Time:10/12/24 15:02
Dilution Factor:1 Prep Method:1664B
Analytical Method:1664B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.40 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131931-2
Lab Sample ID:R4131931-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:04 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/11/24 10:25
Analytical Batch:WG2380187 Analysis Date/Time:10/12/24 15:02
Dilution Factor:1 Prep Method:1664B
Analytical Method:1664B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)38.4 1.40 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131931-3
Lab Sample ID:R4131931-3 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:05 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/11/24 10:25
Analytical Batch:WG2380187 Analysis Date/Time:10/12/24 15:02
Dilution Factor:1 Prep Method:1664B
Analytical Method:1664B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)36.8 1.40 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131931-4
Lab Sample ID:R4131931-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:10/01/24 10:00
Lab File ID:06 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/11/24 10:25
Analytical Batch:WG2380187 Analysis Date/Time:10/12/24 15:02
Dilution Factor:1 Prep Method:1664B
Analytical Method:1664B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:690 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)47.7 J5 1.40 5.00
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:_______________
Instrument ID:OGBAL1 Calibration (end) date/time:_______________
Analytical Method:1664B Analytical Run:WG2380187
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte mg/l
OIL & GREASE
(HEXANE EXTR)U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131931-4
L1784578-17 _______________
MS Sample / File ID:R4131931-4 / 06 SDG:L1784578
MSD Sample / File ID:_______________Analytical Batch:WG2380187
OS Sample / File ID:L1784152-01 / 08 Matrix:GW
Instrument ID:OGBAL1
Analytical Method:1664B
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 U 47.7 119*1 78.0 - 114
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131931-2
RECOVERY R4131931-3
L1784578-17
LCS Sample / File ID:R4131931-2 / 04 SDG:L1784578
LCSD Sample / File ID:R4131931-3 / 05 Analytical Batch:WG2380187
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:1664B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 38.4 36.8 96.0 92.0 78.0 - 114 4.26 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17 Analytical Method:1664B
Matrix:GW Prep Method:1664B
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Oil & Grease (Hexane Extr)1.57 5.62
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:1664B
Instrument ID:OGBAL1 Calibration Start Date:_______________
Analytical Run:WG2380187 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4131931-1 01 10/12/24 15:02 1 WG2380187
LCS R4131931-2 04 10/12/24 15:02 1 WG2380187
LCSD R4131931-3 05 10/12/24 15:02 1 WG2380187
MS R4131931-4 06 10/12/24 15:02 1 WG2380187
OS L1784152-01 08 10/12/24 15:02
EB-93024 L1784578-17 25 10/12/24 15:02 1 WG2380187
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2540 G-2011 Total Solids
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:04 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.136 g
Total Solids (%):83.9 Final Wt/Vol:8.718 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 83.9
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:05 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.146 g
Total Solids (%):87.1 Final Wt/Vol:8.138 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 87.1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:06 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.599 g
Total Solids (%):83.0 Final Wt/Vol:9.016 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 83.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:07 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.09 g
Total Solids (%):85.5 Final Wt/Vol:8.817 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 85.5
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:08 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.442 g
Total Solids (%):90.4 Final Wt/Vol:9.567 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 90.4
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:09 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.291 g
Total Solids (%):93.7 Final Wt/Vol:8.784 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 93.7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (12-18)
Lab Sample ID:L1784578-07 SDG:L1784578
Client Sample ID:S-4 (12-18)Collected Date/Time:09/27/24 15:05
Lab File ID:10 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.938 g
Total Solids (%):91.1 Final Wt/Vol:8.255 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 91.1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (12-18)
Lab Sample ID:L1784578-08 SDG:L1784578
Client Sample ID:S-6 (12-18)Collected Date/Time:09/27/24 15:20
Lab File ID:11 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:6.689 g
Total Solids (%):90.7 Final Wt/Vol:6.188 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 90.7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (12-18)
Lab Sample ID:L1784578-09 SDG:L1784578
Client Sample ID:S-1 (12-18)Collected Date/Time:09/27/24 14:40
Lab File ID:12 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.24 g
Total Solids (%):90.5 Final Wt/Vol:7.58 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 90.5
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (12-18)
Lab Sample ID:L1784578-10 SDG:L1784578
Client Sample ID:S-7 (12-18)Collected Date/Time:09/27/24 15:30
Lab File ID:13 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.586 g
Total Solids (%):94.4 Final Wt/Vol:9.121 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 94.4
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:04 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:43
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.225 g
Total Solids (%):95.7 Final Wt/Vol:9.844 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 95.7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:05 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:43
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.919 g
Total Solids (%):84.6 Final Wt/Vol:7.745 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 84.6
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:06 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:43
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.132 g
Total Solids (%):97.4 Final Wt/Vol:10.872 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 97.4
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (12-18)
Lab Sample ID:L1784578-14 SDG:L1784578
Client Sample ID:SS-1 (12-18)Collected Date/Time:09/30/24 10:25
Lab File ID:07 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:43
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.149 g
Total Solids (%):88.3 Final Wt/Vol:8.23 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 88.3
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:08 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:43
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.974 g
Total Solids (%):86.3 Final Wt/Vol:7.919 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 86.3
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (12-18)
Lab Sample ID:L1784578-16 SDG:L1784578
Client Sample ID:S-3 (12-18)Collected Date/Time:09/27/24 11:00
Lab File ID:09 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 16:38
Analytical Batch:WG2376477 Analysis Date/Time:10/05/24 16:52
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.646 g
Total Solids (%):89.0 Final Wt/Vol:8.724 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 89.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129340-1
Lab Sample ID:R4129340-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:40
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.269 g
Total Solids (%):_______________Final Wt/Vol:1.268 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129341-1
Lab Sample ID:R4129341-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:56
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.302 g
Total Solids (%):_______________Final Wt/Vol:1.305 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129364-1
Lab Sample ID:R4129364-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 16:35
Analytical Batch:WG2376477 Analysis Date/Time:10/05/24 16:52
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.286 g
Total Solids (%):_______________Final Wt/Vol:1.291 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.00500 J
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129340-3
Lab Sample ID:R4129340-3 SDG:L1784578
Client Sample ID:DUP Collected Date/Time:10/01/24 10:21
Lab File ID:02 Received Date/Time:10/03/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:43
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.731 g
Total Solids (%):86.0 Final Wt/Vol:6.607 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 82.6
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129340-2
Lab Sample ID:R4129340-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:40
Analytical Batch:WG2376182 Analysis Date/Time:10/05/24 14:56
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.274 g
Total Solids (%):_______________Final Wt/Vol:6.274 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.0
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129341-2
Lab Sample ID:R4129341-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:56
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.304 g
Total Solids (%):_______________Final Wt/Vol:6.311 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129364-2
Lab Sample ID:R4129364-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 16:35
Analytical Batch:WG2376477 Analysis Date/Time:10/05/24 16:52
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.288 g
Total Solids (%):_______________Final Wt/Vol:6.294 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129341-3
Lab Sample ID:R4129341-3 SDG:L1784578
Client Sample ID:DUP Collected Date/Time:09/27/24 12:00
Lab File ID:02 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:56
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.281 g
Total Solids (%):93.7 Final Wt/Vol:8.74 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 93.2
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129364-3
Lab Sample ID:R4129364-3 SDG:L1784578
Client Sample ID:DUP Collected Date/Time:10/01/24 12:00
Lab File ID:02 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 16:35
Analytical Batch:WG2376477 Analysis Date/Time:10/05/24 16:52
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.922 g
Total Solids (%):79.6 Final Wt/Vol:8.247 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 80.6
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2376182
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2376181
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2376477
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.00500 J
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6-IN DUPLICATES SAMPLE NO.:
L1784578-11,12,13,14,15 R4129340-3
DUP Sample / File ID:R4129340-3 / 02 SDG:L1784578
OS Sample / File ID:L1784800-04 / 12 Analytical Batch:WG2376182
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 86.0 82.6 4.09 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6-IN DUPLICATES SAMPLE NO.:
L1784578-01,02,03,04,05,06,07,08,09,10 R4129341-3
DUP Sample / File ID:R4129341-3 / 02 SDG:L1784578
OS Sample / File ID:L1784578-06 / 09 Analytical Batch:WG2376181
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 93.7 93.2 0.463 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6-IN DUPLICATES SAMPLE NO.:
L1784578-16 R4129364-3
DUP Sample / File ID:R4129364-3 / 02 SDG:L1784578
OS Sample / File ID:L1784576-13 / 07 Analytical Batch:WG2376477
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 79.6 80.6 1.23 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129340-2
RECOVERY _______________
L1784578-11,12,13,14,15
LCS Sample / File ID:R4129340-2 / 03 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2376182
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.0 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129341-2
RECOVERY _______________
L1784578-01,02,03,04,05,06,07,08,09,10
LCS Sample / File ID:R4129341-2 / 03 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2376181
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.1 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129364-2
RECOVERY _______________
L1784578-16
LCS Sample / File ID:R4129364-2 / 03 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2376477
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.1 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,1
6 Analytical Method:2540 G-2011
Matrix:Solid Prep Method:SM 2540 G
Analyte CAS Wavelength Mass MDL RDL
%%
Total Solids TSOLIDS
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2376182 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4129340-1 01 10/05/24 14:56 1 WG2376182
DUP R4129340-3 02 10/05/24 14:56 1 WG2376182
LCS R4129340-2 03 10/05/24 14:56 1 WG2376182
OS L1784800-04 12 10/05/24 14:56
S-10 (6-12)L1784578-11 04 10/05/24 14:56 1 WG2376182
S-14 (0-6)L1784578-12 05 10/05/24 14:56 1 WG2376182
S-11 (0-6)L1784578-13 06 10/05/24 14:56 1 WG2376182
SS-1 (12-18)L1784578-14 07 10/05/24 14:56 1 WG2376182
S-14 (6-12)L1784578-15 08 10/05/24 14:56 1 WG2376182
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2376181 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4129341-1 01 10/05/24 15:11 1 WG2376181
DUP R4129341-3 02 10/05/24 15:11 1 WG2376181
LCS R4129341-2 03 10/05/24 15:11 1 WG2376181
S-32 (0-6)L1784578-03 06 10/05/24 15:11 1 WG2376181
S-10 (0-6)L1784578-06 09 10/05/24 15:11 1 WG2376181
S-13 (0-6)L1784578-01 04 10/05/24 15:11 1 WG2376181
S-15 (0-6)L1784578-02 05 10/05/24 15:11 1 WG2376181
S-12 (6-12)L1784578-04 07 10/05/24 15:11 1 WG2376181
S-12 (0-6)L1784578-05 08 10/05/24 15:11 1 WG2376181
S-4 (12-18)L1784578-07 10 10/05/24 15:11 1 WG2376181
S-7 (12-18)L1784578-10 13 10/05/24 15:11 1 WG2376181
S-1 (12-18)L1784578-09 12 10/05/24 15:11 1 WG2376181
S-6 (12-18)L1784578-08 11 10/05/24 15:11 1 WG2376181
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2376477 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4129364-1 01 10/05/24 16:52 1 WG2376477
DUP R4129364-3 02 10/05/24 16:52 1 WG2376477
LCS R4129364-2 03 10/05/24 16:52 1 WG2376477
OS L1784576-13 07 10/05/24 16:52
S-3 (12-18)L1784578-16 09 10/05/24 16:52 1 WG2376477
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3511/8015 Semi-Volatile Organic Compounds (GC)
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2A-OR SURROGATE RECOVERY
Analytical Method:3511/8015 SDG:L1784578
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
EB-93024 L1784578-17 SVGC26 1013_017 118 0
BLANK R4132895-1 SVGC26 1013_009 139 0
LCS R4132895-2 SVGC26 1013_010 133 0
LCSD R4132895-3 SVGC26 1013_011 128 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 o-Terphenyl 52.0 - 156
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4132895-2
RECOVERY R4132895-3
L1784578-17
LCS Sample / File ID:R4132895-2 / 1013_010 SDG:L1784578
LCSD Sample / File ID:R4132895-3 / 1013_011 Analytical Batch:WG2380823
Instrument ID:SVGC26 Dilution Factor:1
Analytical Method:3511/8015 Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.50 1.79 1.76 119 117 50.0 - 150 1.69 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4132895-1
Lab Sample ID:R4132895-1 SDG:L1784578
Lab File ID:1013_009 Preparation Date/Time:10/12/24 11:48
Instrument ID:SVGC26 Analysis Date/Time:10/14/24 00:13
Analytical Batch:WG2380823 Dilution Factor:1
Analytical Method:3511/8015 Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4132895-2 SVGC26 1013_010 10/14/24 00:33
LCSD R4132895-3 SVGC26 1013_011 10/14/24 00:53
EB-93024 L1784578-17 SVGC26 1013_017 10/14/24 02:54
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:1013_017 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC26 Preparation Date/Time:10/12/24 11:49
Analytical Batch:WG2380823 Analysis Date/Time:10/14/24 02:54
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 5.95 0.0480 J 0.0247 0.100
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:09/24/24 14:13
Instrument ID:SVGC26 Calibration (end) date/time:09/24/24 21:18
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200
TPH (GC/FID) HIGH FRACTION 5.98 5.98 5.98 5.98 5.98 5.98 5.98 5.98
O-TERPHENYL 8.24 8.22 8.22 8.21 8.22 8.22 8.22
File ID:0924_008 0924_009 0924_010 0924_011 0924_019 0924_013 0924_014 0924_015
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:09/24/24 14:13
Instrument ID:SVGC26 Calibration (end) date/time:09/24/24 21:18
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 28240000 21420000 17720000 15930000 16330000 15200000 15320000 15820000
O-TERPHENYL 16270000 10440000 12310000 15870000 15730000 16700000 17740000
File ID:0924_008 0924_009 0924_010 0924_011 0924_019 0924_013 0924_014 0924_015
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:09/24/24 14:13
Instrument ID:SVGC26 Calibration (end) date/time:09/24/24 21:18
Analytical Method:3511/8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 18247100 24.76 0.999
O-TERPHENYL 15007970 17.48
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:09/24/24 14:13
Instrument ID:SVGC26 Calibration (end) date/time:09/24/24 21:18
Lab File ID:0924_020 Analysis date/time:09/24/24 18:32
Analytical Method:3511/8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 18247100 16258270 10.90 60 61.85 103 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:09/24/24 14:13
Instrument ID:SVGC26 Calibration (end) date/time:09/24/24 21:18
Lab File ID:1013_003 Analysis date/time:10/13/24 22:08
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 18247100 16386050 10.20 60 62.35 104 85 - 115
O-TERPHENYL 15007970 26684500 77.80 0.40 0.7112 178 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:09/24/24 14:13
Instrument ID:SVGC26 Calibration (end) date/time:09/24/24 21:18
Lab File ID:1013_034 Analysis date/time:10/14/24 08:36
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 18247100 16092710 11.80 60 61.20 102 85 - 115
O-TERPHENYL 15007970 26066170 73.70 0.40 0.6947 174 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:3511/8015
Instrument ID:SVGC26 Calibration Start Date:09/24/24 14:13
Calibration End Date:09/24/24 21:18
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2 0924_008 09/24/24 14:13
CAL 4 0924_009 09/24/24 14:34
CAL 10 0924_010 09/24/24 14:55
CAL 20 0924_011 09/24/24 15:15
CAL 60 0924_013 09/24/24 15:57
CAL 100 0924_014 09/24/24 16:17
CAL 200 0924_015 09/24/24 16:38
CAL 40 0924_019 09/24/24 18:12
SSCV SVGC260924240924_020759199 0924_020 09/24/24 18:32
CAL 2M 0924_022 09/24/24 19:14
CAL 4M 0924_023 09/24/24 19:34
CAL 10M 0924_024 09/24/24 19:55
CAL 20M 0924_025 09/24/24 20:15
CAL 40M 0924_026 09/24/24 20:36
CAL 50M 0924_027 09/24/24 20:57
CAL 100M 0924_028 09/24/24 21:18
CCV SVGC261013241013_003759199 1013_003 10/13/24 22:08
CCV SVGC261013241013_004759199 1013_004 10/13/24 22:29
BLANK R4132896-1 1013_006 10/13/24 23:13 1 WG2380825
LCS R4132896-2 1013_007 10/13/24 23:33 1 WG2380825
LCSD R4132896-3 1013_008 10/13/24 23:53 1 WG2380825
BLANK R4132895-1 1013_009 10/14/24 00:13 1 WG2380823
LCS R4132895-2 1013_010 10/14/24 00:33 1 WG2380823
LCSD R4132895-3 1013_011 10/14/24 00:53 1 WG2380823
EB-93024 L1784578-17 1013_017 10/14/24 02:54 1 WG2380823
L1784571-01 L1784571-01 1013_022 10/14/24 04:35 5 WG2380823
L1784563-01 L1784563-01 1013_023 10/14/24 04:55 5 WG2380823
L1784563-02 L1784563-02 1013_024 10/14/24 05:15 5 WG2380823
L1784569-03 L1784569-03 1013_026 10/14/24 05:55 5 WG2380823
L1784569-04 L1784569-04 1013_029 10/14/24 06:56 5 WG2380823
L1784571-02 L1784571-02 1013_030 10/14/24 07:16 5 WG2380823
L1784571-03 L1784571-03 1013_031 10/14/24 07:36 5 WG2380823
CCV SVGC261013241013_034759199 1013_034 10/14/24 08:36
CCV SVGC261013241013_035759199 1013_035 10/14/24 08:57
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17 Analytical Method:3511/8015
Matrix:GW Prep Method:3511/8015
Analyte CAS MDL RDL
mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 0.0247 0.10
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132895-1
Lab Sample ID:R4132895-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1013_009 Received Date/Time:_______________
Instrument ID:SVGC26 Preparation Date/Time:10/12/24 11:48
Analytical Batch:WG2380823 Analysis Date/Time:10/14/24 00:13
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 5.95 U 0.0247 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132895-2
Lab Sample ID:R4132895-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1013_010 Received Date/Time:_______________
Instrument ID:SVGC26 Preparation Date/Time:10/12/24 11:48
Analytical Batch:WG2380823 Analysis Date/Time:10/14/24 00:33
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 5.95 1.79 0.0247 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132895-3
Lab Sample ID:R4132895-3 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1013_011 Received Date/Time:_______________
Instrument ID:SVGC26 Preparation Date/Time:10/12/24 11:48
Analytical Batch:WG2380823 Analysis Date/Time:10/14/24 00:53
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 5.95 1.76 0.0247 0.100
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6010B Metals (ICP)
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:20241011113653 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:36
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.50 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 4.40 0.617 2.38
Barium 7440-39-3 92.2 0.102 0.596
Cadmium 7440-43-9 0.249 J 0.0561 0.596
Chromium 7440-47-3 5.65 0.158 1.19
Lead 7439-92-1 26.2 0.248 0.596
Selenium 7782-49-2 U 0.910 2.38
Silver 7440-22-4 0.402 B J 0.151 1.19
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:20241011114152 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:41
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):87.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 26.5 0.594 2.30
Barium 7440-39-3 251 0.0978 0.574
Cadmium 7440-43-9 1.99 0.0541 0.574
Chromium 7440-47-3 10.6 0.153 1.15
Lead 7439-92-1 309 0.239 0.574
Selenium 7782-49-2 U 0.877 2.30
Silver 7440-22-4 1.05 B J 0.146 1.15
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:20241011114332 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:43
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):83.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 4.03 0.624 2.41
Barium 7440-39-3 81.2 0.103 0.603
Cadmium 7440-43-9 0.413 J 0.0568 0.603
Chromium 7440-47-3 4.50 0.160 1.21
Lead 7439-92-1 27.1 0.251 0.603
Selenium 7782-49-2 U 0.921 2.41
Silver 7440-22-4 0.373 B J 0.153 1.21
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:20241011114511 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:45
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):85.5 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 13.6 0.606 2.34
Barium 7440-39-3 144 0.0996 0.585
Cadmium 7440-43-9 1.38 0.0551 0.585
Chromium 7440-47-3 8.49 0.156 1.17
Lead 7439-92-1 190 0.243 0.585
Selenium 7782-49-2 U 0.893 2.34
Silver 7440-22-4 0.749 B J 0.149 1.17
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:20241011114651 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:46
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):90.4 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 12.1 0.573 2.21
Barium 7440-39-3 103 0.0942 0.553
Cadmium 7440-43-9 1.13 0.0521 0.553
Chromium 7440-47-3 6.69 0.147 1.11
Lead 7439-92-1 136 0.230 0.553
Selenium 7782-49-2 U 0.845 2.21
Silver 7440-22-4 0.669 B J 0.140 1.11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 91 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:20241011112517 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:25
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 15.5 0.553 2.14
Barium 7440-39-3 170 J3 J5 0.0910 0.534
Cadmium 7440-43-9 1.98 0.0503 0.534
Chromium 7440-47-3 8.16 0.142 1.07
Lead 7439-92-1 183 0.222 0.534
Selenium 7782-49-2 U 0.816 2.14
Silver 7440-22-4 0.689 B J O1 0.136 1.07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 92 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (12-18)
Lab Sample ID:L1784578-07 SDG:L1784578
Client Sample ID:S-4 (12-18)Collected Date/Time:09/27/24 15:05
Lab File ID:20241011114831 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:48
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):91.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 8.48 0.569 2.20
Cadmium 7440-43-9 1.65 0.0517 0.549
Lead 7439-92-1 186 0.228 0.549
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-1 (12-18)
Lab Sample ID:L1784578-09 SDG:L1784578
Client Sample ID:S-1 (12-18)Collected Date/Time:09/27/24 14:40
Lab File ID:20241011115011 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:50
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):90.5 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 6.92 0.572 2.21
Lead 7439-92-1 53.4 0.230 0.553
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-7 (12-18)
Lab Sample ID:L1784578-10 SDG:L1784578
Client Sample ID:S-7 (12-18)Collected Date/Time:09/27/24 15:30
Lab File ID:20241011115151 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:51
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):94.4 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 11.3 0.549 2.12
Lead 7439-92-1 96.7 0.220 0.530
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 95 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:20241011115331 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:53
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):95.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 9.25 0.541 2.09
Barium 7440-39-3 88.8 0.0890 0.522
Cadmium 7440-43-9 0.375 J 0.0492 0.522
Chromium 7440-47-3 3.49 0.139 1.04
Lead 7439-92-1 26.1 0.217 0.522
Selenium 7782-49-2 U 0.798 2.09
Silver 7440-22-4 0.358 B J 0.133 1.04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:20241011115511 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:55
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):84.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 10.9 0.612 2.36
Barium 7440-39-3 137 0.101 0.591
Cadmium 7440-43-9 0.613 0.0556 0.591
Chromium 7440-47-3 7.68 0.157 1.18
Lead 7439-92-1 121 0.246 0.591
Selenium 7782-49-2 U 0.903 2.36
Silver 7440-22-4 0.977 B J 0.150 1.18
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 97 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:20241011115651 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:56
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):97.4 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 9.30 0.532 2.05
Barium 7440-39-3 34.0 0.0875 0.514
Cadmium 7440-43-9 0.173 J 0.0484 0.514
Chromium 7440-47-3 67.0 0.137 1.03
Lead 7439-92-1 6.06 0.214 0.514
Selenium 7782-49-2 U 0.785 2.05
Silver 7440-22-4 0.350 B J 0.130 1.03
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 98 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (12-18)
Lab Sample ID:L1784578-14 SDG:L1784578
Client Sample ID:SS-1 (12-18)Collected Date/Time:09/30/24 10:25
Lab File ID:20241011120151 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 12:01
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):88.3 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 6.44 0.587 2.26
Lead 7439-92-1 19.1 0.236 0.566
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 99 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:20241011120331 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 12:03
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):86.3 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 3.13 0.600 2.32
Barium 7440-39-3 89.2 0.0987 0.579
Cadmium 7440-43-9 0.137 J 0.0546 0.579
Chromium 7440-47-3 5.20 0.154 1.16
Lead 7439-92-1 12.8 0.241 0.579
Selenium 7782-49-2 U 0.885 2.32
Silver 7440-22-4 0.265 B J 0.147 1.16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 100 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-3 (12-18)
Lab Sample ID:L1784578-16 SDG:L1784578
Client Sample ID:S-3 (12-18)Collected Date/Time:09/27/24 11:00
Lab File ID:20241007140535 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:06
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 14:05
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.49 g
Total Solids (%):89.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 14.3 0.582 2.25
Lead 7439-92-1 224 0.234 0.562
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 101 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:20241016151943 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/16/24 09:44
Analytical Batch:WG2378117 Analysis Date/Time:10/16/24 15:19
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 U 0.00440 0.0100
Barium 7440-39-3 U 0.000736 0.00500
Cadmium 7440-43-9 U 0.000479 0.00200
Chromium 7440-47-3 U 0.00140 0.0100
Lead 7439-92-1 U 0.00299 0.00600
Selenium 7782-49-2 U 0.00735 0.0100
Silver 7440-22-4 U 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 102 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129463-1
Lab Sample ID:R4129463-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20241007124713 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:05
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 12:47
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 0.761 J 0.518 2.00
Lead 7439-92-1 U 0.208 0.500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131568-1
Lab Sample ID:R4131568-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20241011112158 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:05
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:21
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 U 0.518 2.00
Barium 7440-39-3 U 0.0852 0.500
Cadmium 7440-43-9 U 0.0471 0.500
Chromium 7440-47-3 U 0.133 1.00
Lead 7439-92-1 U 0.208 0.500
Selenium 7782-49-2 U 0.764 2.00
Silver 7440-22-4 0.184 J 0.127 1.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 104 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4133611-1
Lab Sample ID:R4133611-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20241016144855 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:10/16/24 09:42
Analytical Batch:WG2378117 Analysis Date/Time:10/16/24 14:48
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 U 0.00440 0.0100
Barium 7440-39-3 U 0.000736 0.00500
Cadmium 7440-43-9 U 0.000479 0.00200
Chromium 7440-47-3 U 0.00140 0.0100
Lead 7439-92-1 U 0.00299 0.00600
Selenium 7782-49-2 U 0.00735 0.0100
Silver 7440-22-4 U 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 105 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129463-2
Lab Sample ID:R4129463-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20241007124853 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:05
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 12:48
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 93.7 0.518 2.00
Lead 7439-92-1 87.2 0.208 0.500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131568-2
Lab Sample ID:R4131568-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20241011112337 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:05
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:23
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 102 0.518 2.00
Barium 7440-39-3 99.6 0.0852 0.500
Cadmium 7440-43-9 97.9 0.0471 0.500
Chromium 7440-47-3 99.9 0.133 1.00
Lead 7439-92-1 97.6 0.208 0.500
Selenium 7782-49-2 99.9 0.764 2.00
Silver 7440-22-4 21.1 0.127 1.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 107 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4133611-2
Lab Sample ID:R4133611-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20241016145037 Received Date/Time:_______________
Instrument ID:ICP17 Preparation Date/Time:10/16/24 09:42
Analytical Batch:WG2378117 Analysis Date/Time:10/16/24 14:50
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 0.977 0.00440 0.0100
Barium 7440-39-3 1.02 0.000763 0.00500
Cadmium 7440-43-9 0.982 0.000479 0.00200
Chromium 7440-47-3 1.01 0.00140 0.0100
Lead 7439-92-1 0.965 0.00299 0.00600
Selenium 7782-49-2 0.956 0.00735 0.0100
Silver 7440-22-4 0.203 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129463-5
Lab Sample ID:R4129463-5 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/30/24 13:02
Lab File ID:20241007125534 Received Date/Time:10/01/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:06
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 12:55
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):81.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 108 0.635 2.45
Lead 7439-92-1 117 0.255 0.613
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131568-5
Lab Sample ID:R4131568-5 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:20241011113015 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:30
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.53 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 119 0.553 2.14
Barium 7440-39-3 268 0.0910 0.534
Cadmium 7440-43-9 102 0.0503 0.534
Chromium 7440-47-3 106 0.142 1.07
Lead 7439-92-1 286 0.222 0.534
Selenium 7782-49-2 102 0.816 2.14
Silver 7440-22-4 22.5 0.136 1.07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4133611-4
Lab Sample ID:R4133611-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/30/24 13:46
Lab File ID:20241016145545 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/16/24 09:44
Analytical Batch:WG2378117 Analysis Date/Time:10/16/24 14:55
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 1.04 0.00440 0.0100
Barium 7440-39-3 1.29 0.000736 0.00500
Cadmium 7440-43-9 1.03 0.000479 0.00200
Chromium 7440-47-3 1.05 0.00140 0.0100
Lead 7439-92-1 1.04 0.00299 0.00600
Selenium 7782-49-2 1.03 0.00735 0.0100
Silver 7440-22-4 0.212 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 111 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129463-6
Lab Sample ID:R4129463-6 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/30/24 13:02
Lab File ID:20241007125714 Received Date/Time:10/01/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:06
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 12:57
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):81.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 109 0.635 2.45
Lead 7439-92-1 122 0.255 0.613
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131568-6
Lab Sample ID:R4131568-6 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:20241011113155 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:31
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 125 0.553 2.14
Barium 7440-39-3 415 J3 J5 0.0910 0.534
Cadmium 7440-43-9 105 0.0503 0.534
Chromium 7440-47-3 109 0.142 1.07
Lead 7439-92-1 286 0.222 0.534
Selenium 7782-49-2 105 0.816 2.14
Silver 7440-22-4 23.1 0.136 1.07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 113 of 526
1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4133611-5
Lab Sample ID:R4133611-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/30/24 13:46
Lab File ID:20241016145728 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/16/24 09:44
Analytical Batch:WG2378117 Analysis Date/Time:10/16/24 14:57
Dilution Factor:1 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 1.05 0.00440 0.0100
Barium 7440-39-3 1.30 0.000736 0.00500
Cadmium 7440-43-9 1.03 0.000479 0.00200
Chromium 7440-47-3 1.06 0.00140 0.0100
Lead 7439-92-1 1.04 0.00299 0.00600
Selenium 7782-49-2 1.03 0.00735 0.0100
Silver 7440-22-4 0.213 0.00154 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129463-4
Lab Sample ID:R4129463-4 SDG:L1784578
Client Sample ID:PS Collected Date/Time:09/30/24 13:02
Lab File ID:20241007125354 Received Date/Time:10/01/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:06
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 12:53
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):81.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 117 0.635 2.45
Lead 7439-92-1 126 0.255 0.613
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131568-4
Lab Sample ID:R4131568-4 SDG:L1784578
Client Sample ID:PS Collected Date/Time:09/27/24 12:00
Lab File ID:20241011112836 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:28
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 121 0.553 2.14
Barium 7440-39-3 266 0.0910 0.534
Cadmium 7440-43-9 104 0.0503 0.534
Chromium 7440-47-3 107 0.142 1.07
Lead 7439-92-1 282 0.222 0.534
Selenium 7782-49-2 104 0.816 2.14
Silver 7440-22-4 9.16 O1 0.136 1.07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129463-3
Lab Sample ID:R4129463-3 SDG:L1784578
Client Sample ID:SD Collected Date/Time:09/30/24 13:02
Lab File ID:20241007125214 Received Date/Time:10/01/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/05/24 22:06
Analytical Batch:WG2376546 Analysis Date/Time:10/07/24 12:52
Dilution Factor:5 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):81.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 9.11 3.17 12.3
Lead 7439-92-1 18.1 1.27 3.06
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131568-3
Lab Sample ID:R4131568-3 SDG:L1784578
Client Sample ID:SD Collected Date/Time:09/27/24 12:00
Lab File ID:20241011112656 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/10/24 23:50
Analytical Batch:WG2376598 Analysis Date/Time:10/11/24 11:26
Dilution Factor:5 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Arsenic 7440-38-2 15.1 2.77 10.7
Barium 7440-39-3 167 0.455 2.67
Cadmium 7440-43-9 1.90 0.252 2.67
Chromium 7440-47-3 7.68 0.710 5.34
Lead 7439-92-1 169 1.11 2.67
Selenium 7782-49-2 U 4.08 10.7
Silver 7440-22-4 0.961 0.678 5.34
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4133611-3
Lab Sample ID:R4133611-3 SDG:L1784578
Client Sample ID:SD Collected Date/Time:09/30/24 13:46
Lab File ID:20241016145402 Received Date/Time:10/02/24 09:00
Instrument ID:ICP17 Preparation Date/Time:10/16/24 09:44
Analytical Batch:WG2378117 Analysis Date/Time:10/16/24 14:54
Dilution Factor:5 Prep Method:3015
Analytical Method:6010B Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:45 mL
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Arsenic 7440-38-2 U 0.0220 0.0500
Barium 7440-39-3 0.240 0.00368 0.0250
Cadmium 7440-43-9 U 0.00240 0.0100
Chromium 7440-47-3 U 0.00700 0.0500
Lead 7439-92-1 U 0.0150 0.0300
Selenium 7782-49-2 U 0.0368 0.0500
Silver 7440-22-4 U 0.00770 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Concentration Units:mg/l
ICV ICVLL CCV
Sample ID:ICP171007240858-2 ICP171007240907-2 ICP171007241243-2
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.9998432 100 0.581000 0.01 0.01024259 102 18.300000 1 0.9680012 96.8
0 1.080000
LEAD 1 0.9662432 96.6
0 0.934000 0.0050 0.004568765 91.40 53.900000 0.50 0.4634552 92.7
0 2.080000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Concentration Units:mg/l
CCV CCV CCV
Sample ID:ICP171007241304 ICP171007241324 ICP171007241407
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.981733 98.2
0 1.940000 1 0.9697328 97 2.070000 1 0.9818227 98.2
0 1.410000
LEAD 0.50 0.4663714 93.3
0 0.386000 0.50 0.4585451 91.70 3.740000 0.50 0.4638239 92.8
0 0.620000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Concentration Units:mg/l
ICV ICVLL CCV
Sample ID:ICP171011240829 ICP171011240840 ICP171011241102
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 1.017771 102 1.470000 0.01 0.008751987 87.5
0 34.400000 1 1.012402 101 1.630000
BARIUM 1 1.008689 101 1.560000 0.0050 0.00522055
8 104 5.710000 0.50 0.4943824 98.9
0 1.510000
CADMIUM 1 0.9908708 99.10 1.570000 0.0020 0.002312353 116 34.600000 0.50 0.4842617 96.9
0 3.810000
CHROMIUM 1 1.013281 101 1.200000 0.01 0.009081033 90.8
0 3.560000 1 0.9927026 99.3
0 2.040000
LEAD 1 0.9736793 97.4
0 1.210000 0.0050 0.005797131 116 45.300000 0.50 0.4895878 97.9
0 1.420000
SELENIUM 1 0.9901922 99 1.890000 0.01 0.01134757 113 32.700000 1 1.004723 100 1.660000
SILVER 1 1.02227 102 1.870000 0.0050 0.005428456 109 11.800000 0.50 0.5243209 105 0.171000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Concentration Units:mg/l
CCV CCV CCV
Sample ID:ICP171011241138 ICP171011241158 ICP171011241218
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 1.009618 101 0.729000 1 1.016031 102 0.484000 1 1.019266 102 0.988000
BARIUM 0.50 0.4895666 97.9
0 1.230000 0.50 0.4954248 99.10 0.371000 0.50 0.4933097 98.7
0 1.250000
CADMIUM 0.50 0.49062 98.10 2.450000 0.50 0.4901298 98 0.716000 0.50 0.4912999 98.3
0 2.080000
CHROMIUM 1 0.9824943 98.2
0 1.810000 1 0.9984537 99.8
0 0.236000 1 0.994643 99.5
0 1.290000
LEAD 0.50 0.4879988 97.6
0 1.420000 0.50 0.4933727 98.7
0 0.181000 0.50 0.4891534 97.8
0 0.440000
SELENIUM 1 1.007139 101 2.360000 1 1.019309 102 1.080000 1 1.007803 101 1.890000
SILVER 0.50 0.5172047 103 0.648000 0.50 0.5210118 104 1.500000 0.50 0.5225224 105 0.841000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Concentration Units:mg/l
CCVLL
Sample ID:ICP171011241415
Analyte True Found %R %RSD
ARSENIC 0.01 0.01424643 142 39.400000
BARIUM 0.0050 0.005344363 107 7.190000
CADMIUM 0.0020 0.002444745 122 22.700000
CHROMIUM 0.01 0.00902722
9
90.3
0 6.930000
LEAD 0.0050 0.002517985 50.4
0 41.800000
SELENIUM 0.01 0.008188148 81.90 63.300000
SILVER 0.0050 0.00749203 150 16.500000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Concentration Units:mg/l
ICV ICVLL CCV
Sample ID:ICP171016240651 ICP171016240700 ICP171016241351
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 1 0.9914635 99.10 0.903000 0.01 0.01186469 119 10.300000 1 0.9949954 99.5
0 0.813000
BARIUM 1 1.037158 104 0.710000 0.0050 0.00524296
3 105 3.570000 0.50 0.5129636 103 0.644000
CADMIUM 1 0.9920129 99.2
0 0.533000 0.0020 0.001920185 96 24.100000 0.50 0.489137 97.8
0 0.630000
CHROMIUM 1 1.035267 104 0.524000 0.01 0.01049821 105 6.400000 1 1.001848 100 0.342000
LEAD 1 0.9812483 98.10 0.589000 0.0050 0.004598974 92 45.300000 0.50 0.4918822 98.4
0 0.197000
SELENIUM 1 0.9723666 97.2
0 0.259000 0.01 0.01177595 118 42.200000 1 1.018824 102 0.655000
SILVER 1 0.9985485 99.9
0 0.679000 0.0050 0.005245871 105 13.500000 0.50 0.5185819 104 0.688000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 125 of 526
2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Concentration Units:mg/l
CCVLL CCV CCV
Sample ID:ICP171016241354 ICP171016241504 ICP171016241524-2
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
ARSENIC 0.01 0.011328 113 11.500000 1 0.9841781 98.4
0 0.458000 1 0.9949518 99.5
0 0.385000
BARIUM 0.0050 0.005323248 106 5.250000 0.50 0.5088091 102 1.160000 0.50 0.5166823 103 0.139000
CADMIUM 0.0020 0.002484195 124 25.600000 0.50 0.4938821 98.8
0 1.740000 0.50 0.4930377 98.6
0 0.699000
CHROMIUM 0.01 0.01049719 105 1.700000 1 1.01461 101 1.430000 1 1.01822 102 0.524000
LEAD 0.0050 0.003645734 72.9
0 51.100000 0.50 0.4971897 99.4
0 2.080000 0.50 0.4976778 99.5
0 0.509000
SELENIUM 0.01 0.00798022
6
79.8
0 85.900000 1 1.013188 101 1.170000 1 1.004968 100 2.660000
SILVER 0.0050 0.005352983 107 9.230000 0.50 0.5111137 102 1.330000 0.50 0.5219583 104 1.310000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20241007090230-2 20241007124529-2 20241007124713 20241007130543
Analyte mg/l mg/l mg/kg mg/l
ARSENIC 0.0003974852 U 0.003387943 U 0.761 J 0.008367432 U
LEAD 0.0001705198 U 0.0004522174 U U -0.0001548615 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Sample ID:CCB Result CCB Qual CCB Result CCB Qual
File ID:20241007132557 20241007140857
Analyte mg/l mg/l
ARSENIC 0.002964793 U 0.003374388 U
LEAD -0.0009758803 U 0.0006997347 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20241011083519 20241011110409 20241011112158 20241011114012
Analyte mg/l mg/l mg/kg mg/l
ARSENIC -0.002437994 U 0.004678281 U U 0.006266802 U
BARIUM 0.0003237292 U 0.0011569 U U 0.001714265 U
CADMIUM 0.0001395371 U 0.0007900507 U U 0.001458263 U
CHROMIUM -0.001157456 U 0.001355564 U U 0.001830484 U
LEAD -0.001148027 U -0.002004119 U U -0.002602868 U
SELENIUM 0.004340659 U 0.006539343 U U 0.003931328 U
SILVER 0.0005676304 U 0.002067275 U 0.184 J 0.002650839 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Sample ID:CCB Result CCB Qual CCB Result CCB Qual
File ID:20241011120011 20241011122016
Analyte mg/l mg/l
ARSENIC 0.006978736 U 0.005598658 U
BARIUM 0.00151677 U 0.001153781 U
CADMIUM 0.0009032841 U 0.000860468 U
CHROMIUM 0.001704017 U 0.0006429172 U
LEAD -0.001008639 U -0.003226938 U
SELENIUM 0.003671888 U 0.001191652 U
SILVER 0.00203765 U 0.001798562 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20241016065531 20241016135313 20241016144855 20241016150603
Analyte mg/l mg/l mg/l mg/l
ARSENIC 0.004795121 U 0.001791541 U U 0.003199197 U
BARIUM 0.00002342792 U 0.00051055 U U 0.0007075786 U
CADMIUM 0.0002348493 U 0.0008351174 U U 0.001041237 U
CHROMIUM 0.0004343504 U 0.001057603 U U 0.001214822 U
LEAD 0.0005078268 U -0.0001887006 U U 0.0000093902
96 U
SELENIUM 0.00071358 U 0.004960908 U U 0.009188297 U
SILVER 0.0005061944 U -0.0003683045 U U -0.0001867245 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Sample ID:CCB Result CCB Qual
File ID:20241016152633-2
Analyte mg/l
ARSENIC 0.001405284 U
BARIUM 0.0005411791 U
CADMIUM 0.0006151397 U
CHROMIUM 0.001671339 U
LEAD 0.001092689 U
SELENIUM 0.003551963 U
SILVER 0.0001591441 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/07/24 09:09
Instrument Run:100724ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 503.3276 101 500 500.3778 100
ANTIMONY 0 -0.00632197 0.50 0.4741903 94.80
ARSENIC 0 -0.006241994 0.50 0.4716343 94.30
BARIUM 0 -0.000528187 0.50 0.5043742 101
BERYLLIUM 0 0.000560998 0.50 0.4928782 98.60
BORON 0 -0.01290431 1 0.9657647 96.60
CADMIUM 0 -0.0006467297 1 0.9887898 98.90
CALCIUM 500 503.5141 101 500 499.0408 99.80
CERIUM 0 0.05590324 0 0.07517654
CHROMIUM 0 -0.00415546 0.50 0.4943461 98.90
COBALT 0 0.002322873 0.50 0.4722271 94.40
COPPER 0 0.00007255561 0.50 0.5339953 107
IRON 200 200.8432 100 200 199.7222 99.90
LANTHANUM 0 -0.001579787 0 -0.006460461
LEAD 0 -0.001380408 1 0.972516 97.30
LITHIUM 0 0.003865292 0 0.002749794
MAGNESIUM 500 503.7164 101 500 500.8356 100
MANGANESE 0 -0.005408137 0.50 0.5091157 102
MOLYBDENUM 0 -0.001964345 0.50 0.4935733 98.70
NICKEL 0 0.004470306 1 0.9351594 93.50
PHOSPHORUS 0 0.01164227 0 0.002213443
POTASSIUM 0 0.1043504 0 0.02930883
SELENIUM 0 0.01513163 0.50 0.5080212 102
SILICON 0 -0.008447662 1 0.9128161 91.30
SILVER 0 0.000004499867 1 0.9786146 97.90
SODIUM 0 0.1588335 0 0.08909632
STRONTIUM 0 0.003475109 0 0.003394208
SULFUR 0 0.02840737 0 0.03735356
THALLIUM 0 -0.01089722 0.50 0.4671591 93.40
TIN 0 0.01004945 0.50 0.4961508 99.20
TITANIUM 0 -0.007623369 0.50 0.4707766 94.20
VANADIUM 0 0.001839626 0.50 0.4690773 93.80
ZINC 0 0.0153815 1 0.9778012 97.80
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 133 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/07/24 13:27
Instrument Run:100724ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 497.6534 99.50 500 491.4681 98.30
ANTIMONY 0 -0.005056862 0.50 0.4728875 94.60
ARSENIC 0 -0.007093795 0.50 0.4742239 94.80
BARIUM 0 -0.0006176094 0.50 0.4834772 96.70
BERYLLIUM 0 0.000595638 0.50 0.482675 96.50
BORON 0 -0.01269696 1 0.9483495 94.80
CADMIUM 0 -0.0001339863 1 0.9702837 97
CALCIUM 500 492.3749 98.50 500 487.9746 97.60
CERIUM 0 0.08017964 0 0.05356533
CHROMIUM 0 -0.004763887 0.50 0.4744638 94.90
COBALT 0 0.002296819 0.50 0.4717466 94.30
COPPER 0 0.0005752085 0.50 0.5115344 102
IRON 200 195.3477 97.70 200 193.0978 96.50
LANTHANUM 0 -0.00114781 0 -0.005108755
LEAD 0 -0.002591164 1 0.944092 94.40
LITHIUM 0 0.003389228 0 0.003691856
MAGNESIUM 500 498.8453 99.80 500 491.4037 98.30
MANGANESE 0 -0.00539463 0.50 0.4878306 97.60
MOLYBDENUM 0 -0.001540376 0.50 0.4682229 93.60
NICKEL 0 0.004023637 1 0.9311353 93.10
PHOSPHORUS 0 0.006716293 0 0.007329467
POTASSIUM 0 0.1618639 0 0.08350349
SELENIUM 0 0.01806652 0.50 0.4904234 98.10
SILICON 0 -0.004289213 1 0.888234 88.80
SILVER 0 -0.0009779989 1 0.9007232 90.10
SODIUM 0 0.2236354 0 0.1378192
STRONTIUM 0 0.003628955 0 0.00339272
SULFUR 0 0.03724273 0 0.01517136
THALLIUM 0 -0.01143464 0.50 0.4572886 91.50
TIN 0 0.007634682 0.50 0.4819165 96.40
TITANIUM 0 -0.009047822 0.50 0.4589025 91.80
VANADIUM 0 0.002622414 0.50 0.4627878 92.60
ZINC 0 0.014568 1 0.9459128 94.60
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 134 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/07/24 20:20
Instrument Run:100724ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 491.5454 98.30 500 493.6846 98.70
ANTIMONY 0 -0.01152171 0.50 0.4592307 91.80
ARSENIC 0 -0.006625055 0.50 0.4666201 93.30
BARIUM 0 -0.0009049092 0.50 0.491495 98.30
BERYLLIUM 0 0.0006480182 0.50 0.4877221 97.50
BORON 0 -0.01488104 1 0.9524623 95.20
CADMIUM 0 -0.0003261186 1 0.96888 96.90
CALCIUM 500 496.4987 99.30 500 501.8014 100
CERIUM 0 0.06478001 0 0.07178059
CHROMIUM 0 -0.004652928 0.50 0.4849739 97
COBALT 0 0.002249965 0.50 0.4602313 92
COPPER 0 0.0004174836 0.50 0.5292213 106
IRON 200 197.1295 98.60 200 196.9831 98.50
LANTHANUM 0 -0.001922418 0 -0.00614088
LEAD 0 0.000718309 1 0.9478867 94.80
LITHIUM 0 0.004489656 0 0.004956215
MAGNESIUM 500 485.6894 97.10 500 489.3369 97.90
MANGANESE 0 -0.004880355 0.50 0.50092 100
MOLYBDENUM 0 -0.002239678 0.50 0.4841878 96.80
NICKEL 0 0.004520 1 0.9101874 91
PHOSPHORUS 0 0.006414189 0 0.001959053
POTASSIUM 0 0.08776966 0 0.07519719
SELENIUM 0 0.00756606 0.50 0.4964595 99.30
SILICON 0 0.0008796863 1 0.9076079 90.80
SILVER 0 -0.0001283429 1 0.9170961 91.70
SODIUM 0 0.07899967 0 0.07274289
STRONTIUM 0 0.003308976 0 0.00342386
SULFUR 0 0.02126691 0 0.00409792
THALLIUM 0 -0.006904629 0.50 0.467977 93.60
TIN 0 0.00641616 0.50 0.4804818 96.10
TITANIUM 0 -0.008101216 0.50 0.4690216 93.80
VANADIUM 0 0.002974586 0.50 0.4609611 92.20
ZINC 0 0.01012213 1 0.9480448 94.80
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 135 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/11/24 08:44
Instrument Run:101124ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 513.0997 103 500 517.6964 104
ANTIMONY 0 0.0001705535 0.50 0.5072162 101
ARSENIC 0 -0.006553748 0.50 0.5051409 101
BARIUM 0 -0.0006657294 0.50 0.5037929 101
BERYLLIUM 0 0.0006382786 0.50 0.5132261 103
BORON 0 -0.006241195 1 1.023715 102
CADMIUM 0 0.0005829711 1 1.099087 110
CALCIUM 500 516.0399 103 500 519.109 104
CERIUM 0 0.05281577 0 0.05585982
CHROMIUM 0 -0.005364375 0.50 0.4952071 99
COBALT 0 0.002503531 0.50 0.4901579 98
COPPER 0 0.0003933494 0.50 0.5209872 104
IRON 200 204.8141 102 200 206.3206 103
LANTHANUM 0 -0.002790383 0 -0.005613993
LEAD 0 -0.002351234 1 0.9724067 97.20
LITHIUM 0 0.001878086 0 0.0005619719
MAGNESIUM 500 513.1627 103 500 519.1274 104
MANGANESE 0 -0.004743632 0.50 0.4997483 99.90
MOLYBDENUM 0 -0.001427876 0.50 0.488398 97.70
NICKEL 0 0.003526462 1 0.9812841 98.10
PHOSPHORUS 0 0.009947946 0 0.00319479
POTASSIUM 0 0.2016693 0 -0.01872904
SELENIUM 0 -0.0009990988 0.50 0.4742458 94.80
SILICON 0 -0.004624665 1 1.055631 106
SILVER 0 -0.0003522647 1 0.8062534 80.60
SODIUM 0 0.2972825 0 0.0909511
STRONTIUM 0 0.00367544 0 0.003612616
SULFUR 0 -0.0105688 0 -0.02988578
THALLIUM 0 -0.003015798 0.50 0.477688 95.50
TIN 0 0.003368227 0.50 0.4904112 98.10
TITANIUM 0 -0.009163819 0.50 0.4897855 98
VANADIUM 0 0.002706999 0.50 0.4881914 97.60
ZINC 0 0.01241542 1 0.9743147 97.40
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 136 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/11/24 14:17
Instrument Run:101124ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 508.1301 102 500 505.5995 101
ANTIMONY 0 0.003012282 0.50 0.4997521 100
ARSENIC 0 0.001474939 0.50 0.517717 104
BARIUM 0 -0.0001767548 0.50 0.492282 98.50
BERYLLIUM 0 0.0005958013 0.50 0.4907845 98.20
BORON 0 -0.003672768 1 0.9587516 95.90
CADMIUM 0 0.000883382 1 1.043767 104
CALCIUM 500 495.7108 99.10 500 492.3014 98.50
CERIUM 0 0.04154502 0 0.03364894
CHROMIUM 0 -0.00514981 0.50 0.482829 96.60
COBALT 0 0.00232338 0.50 0.4925733 98.50
COPPER 0 0.0008449427 0.50 0.5158451 103
IRON 200 196.4562 98.20 200 194.7218 97.40
LANTHANUM 0 -0.001594553 0 -0.004297783
LEAD 0 -0.008239787 1 0.9600799 96
LITHIUM 0 0.001331004 0 0.002986402
MAGNESIUM 500 504.7791 101 500 502.402 100
MANGANESE 0 -0.004797885 0.50 0.4867325 97.30
MOLYBDENUM 0 -0.002137216 0.50 0.4836886 96.70
NICKEL 0 0.004925684 1 0.97232 97.20
PHOSPHORUS 0 0.01004314 0 0.001525489
POTASSIUM 0 0.1956077 0 -0.1099411
SELENIUM 0 -0.01355715 0.50 0.4730886 94.60
SILICON 0 0.008224061 1 0.9206868 92.10
SILVER 0 0.003820727 1 1.096532 110
SODIUM 0 0.303616 0 0.03088359
STRONTIUM 0 0.003665987 0 0.003597887
SULFUR 0 -0.01168233 0 -0.01825218
THALLIUM 0 0.001450908 0.50 0.4856875 97.10
TIN 0 0.004523738 0.50 0.4949377 99
TITANIUM 0 -0.00791184 0.50 0.4626189 92.50
VANADIUM 0 0.004145856 0.50 0.4712886 94.30
ZINC 0 0.01247999 1 0.9507124 95.10
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 137 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/16/24 07:02
Instrument Run:101624ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 508.01 102 500 496.7074 99.30
ANTIMONY 0 0.006406111 0.50 0.5148888 103
ARSENIC 0 0.004635356 0.50 0.5202256 104
BARIUM 0 -0.001106798 0.50 0.5168956 103
BERYLLIUM 0 0.000669899 0.50 0.5066582 101
BORON 0 -0.01383158 1 0.996518 99.70
CADMIUM 0 0.001037594 1 1.046457 105
CALCIUM 500 514.3935 103 500 505.1532 101
CERIUM 0 0.05764846 0 0.06480873
CHROMIUM 0 -0.004092436 0.50 0.5027921 101
COBALT 0 0.001864315 0.50 0.4861932 97.20
COPPER 0 0.00056482 0.50 0.5246085 105
IRON 200 202.7948 101 200 198.6079 99.30
LANTHANUM 0 -0.003395401 0 -0.00659757
LEAD 0 -0.003983416 1 0.9896265 99
LITHIUM 0 0.00315103 0 0.004904982
MAGNESIUM 500 508.4012 102 500 497.0807 99.40
MANGANESE 0 -0.006691258 0.50 0.5041332 101
MOLYBDENUM 0 0.001556253 0.50 0.492812 98.60
NICKEL 0 0.001763504 1 0.9874011 98.70
PHOSPHORUS 0 -0.002839968 0 0.004997586
POTASSIUM 0 -0.020924 0 -0.000487208
SELENIUM 0 0.0002505473 0.50 0.5022263 100
SILICON 0 -0.005749975 1 1.029856 103
SILVER 0 0.0008939568 1 0.8783252 87.80
SODIUM 0 0.04589498 0 0.07506762
STRONTIUM 0 0.003536327 0 0.003551656
SULFUR 0 0.02030066 0 0.02732018
THALLIUM 0 -0.004461246 0.50 0.4879667 97.60
TIN 0 0.007210528 0.50 0.4927741 98.60
TITANIUM 0 -0.009861 0.50 0.4837045 96.70
VANADIUM 0 0.003672045 0.50 0.4845231 96.90
ZINC 0 0.008065502 1 1.00056 100
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 138 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/16/24 13:56
Instrument Run:101624ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 497.2924 99.50 500 478.1846 95.60
ANTIMONY 0 0.006769747 0.50 0.4962083 99.20
ARSENIC 0 0.0009992919 0.50 0.4978067 99.60
BARIUM 0 -0.0008881434 0.50 0.492256 98.50
BERYLLIUM 0 0.0006422243 0.50 0.488009 97.60
BORON 0 -0.01519983 1 0.9651411 96.50
CADMIUM 0 0.0006228652 1 1.000373 100
CALCIUM 500 507.4435 101 500 483.5163 96.70
CERIUM 0 0.04193611 0 0.06464115
CHROMIUM 0 -0.003996483 0.50 0.4779806 95.60
COBALT 0 0.0007825106 0.50 0.4648387 93
COPPER 0 0.0001162389 0.50 0.5082644 102
IRON 200 198.2493 99.10 200 191.5122 95.80
LANTHANUM 0 -0.002938647 0 -0.006959216
LEAD 0 -0.001178393 1 0.9505545 95.10
LITHIUM 0 0.004717068 0 0.004351131
MAGNESIUM 500 498.2338 99.60 500 480.2442 96
MANGANESE 0 -0.006652477 0.50 0.4826579 96.50
MOLYBDENUM 0 0.0007507824 0.50 0.4671419 93.40
NICKEL 0 0.002427732 1 0.9454343 94.50
PHOSPHORUS 0 -0.003022779 0 0.006598518
POTASSIUM 0 0.0380122 0 0.008864783
SELENIUM 0 0.006414524 0.50 0.4859968 97.20
SILICON 0 -0.003126213 1 0.9877067 98.80
SILVER 0 0.0008034483 1 0.845543 84.60
SODIUM 0 0.1423302 0 0.1455077
STRONTIUM 0 0.003493805 0 0.003464335
SULFUR 0 0.02597316 0 0.02011293
THALLIUM 0 0.001325782 0.50 0.4744804 94.90
TIN 0 0.005511392 0.50 0.4714728 94.30
TITANIUM 0 -0.008982379 0.50 0.4682705 93.70
VANADIUM 0 0.004594626 0.50 0.4673695 93.50
ZINC 0 0.007627696 1 0.9515205 95.20
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 139 of 526
4-IN INTERFERENCE CHECK SAMPLE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:10/16/24 16:55
Instrument Run:101624ICP17
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 479.5747 95.90 500 476.9578 95.40
ANTIMONY 0 0.009810175 0.50 0.519875 104
ARSENIC 0 0.005394571 0.50 0.5214632 104
BARIUM 0 -0.001131164 0.50 0.515802 103
BERYLLIUM 0 0.0006757485 0.50 0.4903452 98.10
BORON 0 -0.01888106 1 0.9662198 96.60
CADMIUM 0 0.001345413 1 1.044793 104
CALCIUM 500 484.9682 97 500 483.1075 96.60
CERIUM 0 0.04031067 0 0.04986591
CHROMIUM 0 -0.003843878 0.50 0.5031171 101
COBALT 0 0.001357406 0.50 0.4849213 97
COPPER 0 0.001008286 0.50 0.5294727 106
IRON 200 191.3751 95.70 200 190.1634 95.10
LANTHANUM 0 -0.002958655 0 -0.007416052
LEAD 0 -0.005186991 1 0.9922304 99.20
LITHIUM 0 0.00160781 0 0.002444591
MAGNESIUM 500 479.2631 95.90 500 475.69 95.10
MANGANESE 0 -0.006983581 0.50 0.5070031 101
MOLYBDENUM 0 -0.00002845975 0.50 0.4911291 98.20
NICKEL 0 0.001712374 1 0.9898037 99
PHOSPHORUS 0 0.002129079 0 0.003705688
POTASSIUM 0 0.1183448 0 0.1157638
SELENIUM 0 0.009884913 0.50 0.5012654 100
SILICON 0 -0.005054595 1 1.065609 107
SILVER 0 0.00142626 1 0.8886708 88.90
SODIUM 0 0.05621257 0 0.07246973
STRONTIUM 0 0.003492145 0 0.003449735
SULFUR 0 0.03013607 0 0.04205152
THALLIUM 0 -0.005287901 0.50 0.4912554 98.30
TIN 0 0.004773083 0.50 0.4927982 98.60
TITANIUM 0 -0.008843115 0.50 0.4687259 93.70
VANADIUM 0 0.004125983 0.50 0.4661628 93.20
ZINC 0 0.007772657 1 1.000731 100
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 140 of 526
5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4129463-5
L1784578-16 R4129463-6
MS Sample / File ID:R4129463-5 / 20241007125534 SDG:L1784578
MSD Sample / File ID:R4129463-6 / 20241007125714 Analytical Batch:WG2376546
OS Sample / File ID:L1784006-12 / 20241007125033 Matrix:Solid
Instrument ID:ICP17
Analytical Method:6010B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 123 7.58 108 109 82.3 82.5 1 75.0 - 125 0.194 20
Lead 123 19.1 117 122 80.2 83.8 1 75.0 - 125 3.68 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 141 of 526
5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131568-5
L1784578-01,02,03,04,05,06,07,09,10,11,12,13,14,15 R4131568-6
MS Sample / File ID:R4131568-5 / 20241011113015 SDG:L1784578
MSD Sample / File ID:R4131568-6 / 20241011113155 Analytical Batch:WG2376598
OS Sample / File ID:L1784578-06 / 20241011112517 Matrix:Solid
Instrument ID:ICP17
Analytical Method:6010B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 107 15.5 119 125 97.4 103 1 75.0 - 125 4.60 20
Barium 107 170 268 415 92.0 230*1 75.0 - 125 43.1*20
Cadmium 107 1.98 102 105 93.8 96.9 1 75.0 - 125 3.20 20
Chromium 107 8.16 106 109 91.7 94.1 1 75.0 - 125 2.44 20
Lead 107 183 286 286 97.0 96.9 1 75.0 - 125 0.0110 20
Selenium 107 U 102 105 95.6 98.6 1 75.0 - 125 3.16 20
Silver 21.4 0.689 22.5 23.1 102 105 1 75.0 - 125 2.82 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 142 of 526
5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4133611-4
L1784578-17 R4133611-5
MS Sample / File ID:R4133611-4 / 20241016145545 SDG:L1784578
MSD Sample / File ID:R4133611-5 / 20241016145728 Analytical Batch:WG2378117
OS Sample / File ID:L1784574-04 / 20241016145220 Matrix:GW
Instrument ID:ICP17
Analytical Method:6010B
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 0.0102 1.04 1.05 103 104 1 75.0 - 125 1.11 20
Barium 1.00 0.250 1.29 1.30 104 105 1 75.0 - 125 0.499 20
Cadmium 1.00 0.00172 1.03 1.03 103 103 1 75.0 - 125 0.436 20
Chromium 1.00 0.00264 1.05 1.06 105 105 1 75.0 - 125 0.864 20
Lead 1.00 0.0217 1.04 1.04 102 102 1 75.0 - 125 0.589 20
Selenium 1.00 U 1.03 1.03 103 103 1 75.0 - 125 0.294 20
Silver 0.200 U 0.212 0.213 106 106 1 75.0 - 125 0.329 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 143 of 526
5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4129463-4
L1784578-16
PS Sample / File ID:R4129463-4 / 20241007125354 SDG:L1784578
OS Sample / File ID:L1784006-12 / 20241007125033 Analytical Batch:WG2376546
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
PD
Result
(dry)
DS
Result
(dry)
PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/kg mg/kg mg/kg %%%mg/kg mg/kg
Arsenic 123 7.58 117 89.2 1 80.0 -
120
Lead 123 19.1 126 86.9 1 80.0 -
120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4131568-4
L1784578-01,02,03,04,05,06,07,09,10,11,12,13,14,15
PS Sample / File ID:R4131568-4 / 20241011112836 SDG:L1784578
OS Sample / File ID:L1784578-06 / 20241011112517 Analytical Batch:WG2376598
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
PD
Result
(dry)
DS
Result
(dry)
PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/kg mg/kg mg/kg %%%mg/kg mg/kg
Arsenic 107 15.5 121 98.7 1 80.0 -
120
Barium 107 170 266 89.7 1 80.0 -
120
Cadmium 107 1.98 104 95.2 1 80.0 -
120
Chromium 107 8.16 107 92.5 1 80.0 -
120
Lead 107 183 282 93.2 1 80.0 -
120
Selenium 107 U 104 97.8 1 80.0 -
120
Silver 21.4 0.689 9.16 39.6*1 80.0 -
120 *
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129463-2
RECOVERY _______________
L1784578-16
LCS Sample / File ID:R4129463-2 / 20241007124853 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2376546
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Arsenic 100 93.7 93.7 80.0 - 120
Lead 100 87.2 87.2 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131568-2
RECOVERY _______________
L1784578-01,02,03,04,05,06,07,09,10,11,12,13,14,15
LCS Sample / File ID:R4131568-2 / 20241011112337 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2376598
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Arsenic 100 102 102 80.0 - 120
Barium 100 99.6 99.6 80.0 - 120
Cadmium 100 97.9 97.9 80.0 - 120
Chromium 100 99.9 99.9 80.0 - 120
Lead 100 97.6 97.6 80.0 - 120
Selenium 100 99.9 99.9 80.0 - 120
Silver 20.0 21.1 105 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4133611-2
RECOVERY _______________
L1784578-17
LCS Sample / File ID:R4133611-2 / 20241016145037 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2378117
Instrument ID:ICP17 Dilution Factor:1
Analytical Method:6010B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l %%%%%
Arsenic 1.00 0.977 97.7 80.0 - 120
Barium 1.00 1.02 102 80.0 - 120
Cadmium 1.00 0.982 98.2 80.0 - 120
Chromium 1.00 1.01 101 80.0 - 120
Lead 1.00 0.965 96.5 80.0 - 120
Selenium 1.00 0.956 95.6 80.0 - 120
Silver 0.200 0.203 101 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4129463-3
L1784578-16
SD Sample / File ID:R4129463-3 / 20241007125214 SDG:L1784578
OS Sample / File ID:L1784006-12 / 20241007125033 Analytical Batch:WG2376546
Lab File ID:20241007125214 Dilution Factor:5
Instrument ID:ICP17 Matrix:Solid
Analytical Method:6010B
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Arsenic 7.58 9.11 20.1 10
Lead 19.1 18.1 5.15 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4131568-3
L1784578-01,02,03,04,05,06,07,09,10,11,12,13,14,15
SD Sample / File ID:R4131568-3 / 20241011112656 SDG:L1784578
OS Sample / File ID:L1784578-06 / 20241011112517 Analytical Batch:WG2376598
Lab File ID:20241011112656 Dilution Factor:5
Instrument ID:ICP17 Matrix:Solid
Analytical Method:6010B
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Arsenic 15.5 15.1 1.97 10
Barium 170 167 1.54 10
Cadmium 1.98 1.90 3.87 10
Chromium 8.16 7.68 5.86 10
Lead 183 169 7.60 10
Selenium U U 0.000 10
Silver 0.689 0.961 39.4 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4133611-3
L1784578-17
SD Sample / File ID:R4133611-3 / 20241016145402 SDG:L1784578
OS Sample / File ID:L1784574-04 / 20241016145220 Analytical Batch:WG2378117
Lab File ID:20241016145402 Dilution Factor:5
Instrument ID:ICP17 Matrix:GW
Analytical Method:6010B
Analyte OS
Result
SD
Result RPD RPD
Limits
mg/l mg/l %%
Arsenic 0.0102 U 0.000 10
Barium 0.250 0.240 4.25 10
Cadmium 0.00172 U 0.000 10
Chromium 0.00264 U 0.000 10
Lead 0.0217 U 100 10
Selenium U U 0.000 10
Silver U U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17 Analytical Method:6010B
Matrix:GW Prep Method:3015
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Cadmium 7440-43-9 228.8020 0.000479 0.0020
Chromium 7440-47-3 267.7160 0.0014 0.01
Lead 7439-92-1 220.3530 0.002990 0.0060
Selenium 7782-49-2 196.09 0.007350 0.01
Silver 7440-22-4 328.0680 0.001540 0.0050
Arsenic 7440-38-2 189.0420 0.0044 0.01
Barium 7440-39-3 233.5270 0.000736 0.0050
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,07,09,10,11,12,13,14,15,16 Analytical Method:6010B
Matrix:Solid Prep Method:3051
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Lead 7439-92-1 220.3530 0.2080 0.50
Selenium 7782-49-2 196.09 0.7640 2
Silver 7440-22-4 328.0680 0.1270 1
Arsenic 7440-38-2 189.0420 0.5180 2
Barium 7440-39-3 233.5270 0.0852 0.50
Cadmium 7440-43-9 228.8020 0.0471 0.50
Chromium 7440-47-3 267.7160 0.1330 1
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10C-IN LINEAR DYNAMIC RANGE
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Date:06/09/24 17:06
Analyte LDR
ppm
ALUMINUM 500
ANTIMONY 10
ARSENIC 50
BARIUM 50
BERYLLIUM 10
BORON 50
CADMIUM 10
CALCIUM 1000
CHROMIUM 50
COBALT 50
COPPER 50
IRON 500
LEAD 100
LITHIUM 10
MAGNESIUM 1000
MANGANESE 20
MOLYBDENUM 20
NICKEL 50
PHOSPHORUS 200
POTASSIUM 500
SELENIUM 10
SILICON 100
SILVER 10
SODIUM 1000
STRONTIUM 20
SULFUR 200
THALLIUM 10
TIN 50
TITANIUM 50
VANADIUM 20
ZINC 20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 154 of 526
12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Calibration Start Date:10/07/24 08:46
Analytical Run:100724ICP17 Calibration End Date:10/07/24 08:56
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP171007240845 20241007084514 10/07/24 08:45
CAL STD1 20241007084654 10/07/24 08:46
CAL STD2 20241007084834 10/07/24 08:48
CAL STD3 20241007085013 10/07/24 08:50
CAL STD4 20241007085152 10/07/24 08:51
CAL STD5 20241007085330 10/07/24 08:53
CAL STD6 20241007085508 10/07/24 08:55
ICV ICP171007240858-2 20241007085836-2 10/07/24 08:58
ICB ICP171007240902-2 20241007090230-2 10/07/24 09:02
ICVLL ICP171007240907-2 20241007090726-2 10/07/24 09:07
ICSA ICP171007240909-2 20241007090905-2 10/07/24 09:09
ICSAB ICP171007240910-2 20241007091043-2 10/07/24 09:10
CCV ICP171007241243-2 20241007124349-2 10/07/24 12:43
CCB ICP171007241245-2 20241007124529-2 10/07/24 12:45
BLANK R4129463-1 20241007124713 10/07/24 12:47 1 WG2376546
LCS R4129463-2 20241007124853 10/07/24 12:48 1 WG2376546
OS L1784006-12 20241007125033 10/07/24 12:50
L1784006-12 L1784006-12 20241007125033 10/07/24 12:50 1 WG2376546
SD R4129463-3 20241007125214 10/07/24 12:52 5 WG2376546
PS R4129463-4 20241007125354 10/07/24 12:53 1 WG2376546
MS R4129463-5 20241007125534 10/07/24 12:55 1 WG2376546
MSD R4129463-6 20241007125714 10/07/24 12:57 1 WG2376546
L1784006-01 L1784006-01 20241007130040 10/07/24 13:00 1 WG2376546
L1784006-02 L1784006-02 20241007130220 10/07/24 13:02 1 WG2376546
CCV ICP171007241304 20241007130403 10/07/24 13:04
CCB ICP171007241305 20241007130543 10/07/24 13:05
CCV ICP171007241324 20241007132417 10/07/24 13:24
CCB ICP171007241325 20241007132557 10/07/24 13:25
ICSA ICP171007241327-2 20241007132741-2 10/07/24 13:27
ICSAB ICP171007241329-2 20241007132921-2 10/07/24 13:29
L1784006-03 L1784006-03 20241007135022 10/07/24 13:50 1 WG2376546
L1784006-04 L1784006-04 20241007135206 10/07/24 13:52 1 WG2376546
L1784006-05 L1784006-05 20241007135347 10/07/24 13:53 1 WG2376546
L1784006-06 L1784006-06 20241007135527 10/07/24 13:55 1 WG2376546
L1784006-07 L1784006-07 20241007135708 10/07/24 13:57 1 WG2376546
L1784006-08 L1784006-08 20241007135849 10/07/24 13:58 1 WG2376546
L1784006-09 L1784006-09 20241007140030 10/07/24 14:00 1 WG2376546
L1784006-10 L1784006-10 20241007140211 10/07/24 14:02 1 WG2376546
L1784006-11 L1784006-11 20241007140352 10/07/24 14:03 1 WG2376546
S-3 (12-18)L1784578-16 20241007140535 10/07/24 14:05 1 WG2376546
CCV ICP171007241407 20241007140716 10/07/24 14:07
CCB ICP171007241408 20241007140857 10/07/24 14:08
ICSA ICP171007242020 20241007202037 10/07/24 20:20
ICSAB ICP171007242022 20241007202223 10/07/24 20:22
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 155 of 526
12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Calibration Start Date:10/11/24 08:18
Analytical Run:101124ICP17 Calibration End Date:10/11/24 08:27
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP171011240816 20241011081623 10/11/24 08:16
CAL STD1 20241011081802 10/11/24 08:18
CAL STD2 20241011081943 10/11/24 08:19
CAL STD3 20241011082122 10/11/24 08:21
CAL STD4 20241011082300 10/11/24 08:23
CAL STD5 20241011082438 10/11/24 08:24
CAL STD6 20241011082616 10/11/24 08:26
ICV ICP171011240829 20241011082943 10/11/24 08:29
ICB ICP171011240835 20241011083519 10/11/24 08:35
ICVLL ICP171011240840 20241011084037 10/11/24 08:40
ICSA ICP171011240844 20241011084454 10/11/24 08:44
ICSAB ICP171011240846 20241011084633 10/11/24 08:46
CCV ICP171011241102 20241011110229 10/11/24 11:02
CCB ICP171011241104 20241011110409 10/11/24 11:04
BLANK R4131568-1 20241011112158 10/11/24 11:21 1 WG2376598
LCS R4131568-2 20241011112337 10/11/24 11:23 1 WG2376598
S-10 (0-6)L1784578-06 20241011112517 10/11/24 11:25 1 WG2376598
SD R4131568-3 20241011112656 10/11/24 11:26 5 WG2376598
PS R4131568-4 20241011112836 10/11/24 11:28 1 WG2376598
MS R4131568-5 20241011113015 10/11/24 11:30 1 WG2376598
MSD R4131568-6 20241011113155 10/11/24 11:31 1 WG2376598
S-13 (0-6)L1784578-01 20241011113653 10/11/24 11:36 1 WG2376598
CCV ICP171011241138 20241011113833 10/11/24 11:38
CCB ICP171011241140 20241011114012 10/11/24 11:40
S-15 (0-6)L1784578-02 20241011114152 10/11/24 11:41 1 WG2376598
S-32 (0-6)L1784578-03 20241011114332 10/11/24 11:43 1 WG2376598
S-12 (6-12)L1784578-04 20241011114511 10/11/24 11:45 1 WG2376598
S-12 (0-6)L1784578-05 20241011114651 10/11/24 11:46 1 WG2376598
S-4 (12-18)L1784578-07 20241011114831 10/11/24 11:48 1 WG2376598
S-1 (12-18)L1784578-09 20241011115011 10/11/24 11:50 1 WG2376598
S-7 (12-18)L1784578-10 20241011115151 10/11/24 11:51 1 WG2376598
S-10 (6-12)L1784578-11 20241011115331 10/11/24 11:53 1 WG2376598
S-14 (0-6)L1784578-12 20241011115511 10/11/24 11:55 1 WG2376598
S-11 (0-6)L1784578-13 20241011115651 10/11/24 11:56 1 WG2376598
CCV ICP171011241158 20241011115831 10/11/24 11:58
CCB ICP171011241200 20241011120011 10/11/24 12:00
SS-1 (12-18)L1784578-14 20241011120151 10/11/24 12:01 1 WG2376598
S-14 (6-12)L1784578-15 20241011120331 10/11/24 12:03 1 WG2376598
CCV ICP171011241218 20241011121837 10/11/24 12:18
CCB ICP171011241220 20241011122016 10/11/24 12:20
CCVLL ICP171011241415 20241011141525 10/11/24 14:15
ICSA ICP171011241417 20241011141706 10/11/24 14:17
ICSAB ICP171011241417 20241011141754 10/11/24 14:17
ICSAB ICP171011241420 20241011142050 10/11/24 14:20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 156 of 526
12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:6010B
Instrument ID:ICP17 Calibration Start Date:10/16/24 06:39
Analytical Run:101624ICP17 Calibration End Date:10/16/24 06:49
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP171016240638 20241016063800 10/16/24 06:38
CAL STD1 20241016063939 10/16/24 06:39
CAL STD2 20241016064119 10/16/24 06:41
CAL STD3 20241016064257 10/16/24 06:42
CAL STD4 20241016064435 10/16/24 06:44
CAL STD5 20241016064613 10/16/24 06:46
CAL STD6 20241016064750 10/16/24 06:47
CAL STD7 20241016064928 10/16/24 06:49
ICV ICP171016240651 20241016065119 10/16/24 06:51
ICB ICP171016240655 20241016065531 10/16/24 06:55
ICVLL ICP171016240700 20241016070028 10/16/24 07:00
ICSA ICP171016240702 20241016070208 10/16/24 07:02
ICSAB ICP171016240703 20241016070348 10/16/24 07:03
CCV ICP171016241351 20241016135130 10/16/24 13:51
CCB ICP171016241353 20241016135313 10/16/24 13:53
CCVLL ICP171016241354 20241016135459 10/16/24 13:54
ICSA ICP171016241356 20241016135641 10/16/24 13:56
ICSAB ICP171016241358 20241016135824 10/16/24 13:58
BLANK R4133611-1 20241016144855 10/16/24 14:48 1 WG2378117
LCS R4133611-2 20241016145037 10/16/24 14:50 1 WG2378117
OS L1784574-04 20241016145220 10/16/24 14:52
L1784574-04 L1784574-04 20241016145220 10/16/24 14:52 1 WG2378117
SD R4133611-3 20241016145402 10/16/24 14:54 5 WG2378117
MS R4133611-4 20241016145545 10/16/24 14:55 1 WG2378117
MSD R4133611-5 20241016145728 10/16/24 14:57 1 WG2378117
CCV ICP171016241504 20241016150421 10/16/24 15:04
CCB ICP171016241506 20241016150603 10/16/24 15:06
EB-93024 L1784578-17 20241016151943 10/16/24 15:19 1 WG2378117
CCV ICP171016241524-2 20241016152451-2 10/16/24 15:24
CCB ICP171016241526-2 20241016152633-2 10/16/24 15:26
ICSA ICP171016241655 20241016165547 10/16/24 16:55
ICSAB ICP171016241657 20241016165732 10/16/24 16:57
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.01 .00866112 86.60 0.20 .1950446 97.50
BARIUM 0.0050 .004973573 99.50 0.10 .1009531 101
CADMIUM 0.0020 .00235512 118 0.10 .09752225 97.50
CHROMIUM 0.01 .009838921 98.40 0.20 .1999386 100
LEAD 0.0050 .005477183 110 0.10 .09561032 95.60
SELENIUM 0.01 .008523004 85.20 0.20 .1905573 95.30
SILVER 0.0050 .004218438 84.40 0.10 .09977085 99.80
File ID: 20241016063939 20241016064119
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.40 .3869039 96.70 1 .9759946 97.60
BARIUM 0.20 .2011798 101 0.50 .5075443 102
CADMIUM 0.20 .193504 96.80 0.50 .4879136 97.60
CHROMIUM 0.40 .4004065 100 1 1.005596 101
LEAD 0.20 .1927643 96.40 0.50 .4865723 97.30
SELENIUM 0.40 .3837721 95.90 1 .9797416 98
SILVER 0.20 .1982973 99.10 0.50 .5035968 101
File ID: 20241016064257 20241016064435
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 159 of 526
15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 2 1.982642 99.10 4 4.016241 100
BARIUM 1 1.007305 101 2 1.994296 99.70
CADMIUM 1 .9909943 99.10 2 2.008298 100
CHROMIUM 2 2.006916 100 4 3.995106 99.90
LEAD 1 .9900814 99 2 2.009258 100
SELENIUM 2 1.969483 98.50 4 4.022422 101
SILVER 1 .9989175 99.90 2 1.999826 100
File ID: 20241016064613 20241016064750
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.01 .0102664 103 0.20 .1929333 96.50
LEAD 0.0050 .005250531 105 0.10 .09568333 95.70
File ID: 20241007084654 20241007084834
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.40 .3901232 97.50 1 1.007006 101
LEAD 0.20 .1871727 93.60 0.50 .4946746 98.90
File ID: 20241007085013 20241007085152
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 2 2.014869 101 4 3.992154 99.80
LEAD 1 .9788248 97.90 2 2.013417 101
File ID: 20241007085330 20241007085508
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.01 .008607893 86.10 0.20 .201515 101
BARIUM 0.0050 .005159259 103 0.10 .1017841 102
CADMIUM 0.0020 .001615685 80.80 0.10 .09923211 99.20
CHROMIUM 0.01 .009666611 96.70 0.20 .2038268 102
LEAD 0.0050 .005694489 114 0.10 .09936933 99.40
SELENIUM 0.01 .01190298 119 0.20 .2084917 104
SILVER 0.0050 .005180066 104 0.10 .1024167 102
File ID: 20241011081802 20241011081943
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 0.40 .3971859 99.30 1 1.007093 101
BARIUM 0.20 .1999022 100 0.50 .5014537 100
CADMIUM 0.20 .1983797 99.20 0.50 .4969327 99.40
CHROMIUM 0.40 .4005691 100 1 1.005174 101
LEAD 0.20 .1951643 97.60 0.50 .4947901 99
SELENIUM 0.40 .3981228 99.50 1 .9979691 99.80
SILVER 0.20 .2028401 101 0.50 .4708542 94.20
File ID: 20241011082122 20241011082300
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
ARSENIC 2 2.07535 104 4 3.960761 99
BARIUM 1 .9991603 99.90 2 1.999977 100
CADMIUM 1 1.001935 100
CHROMIUM 2 2.021456 101 4 3.987731 99.70
LEAD 1 1.011894 101 2 1.995869 99.80
SELENIUM 2 2.092579 105 4 3.953977 98.80
SILVER 1 1.04102 104 2 1.986371 99.30
File ID: 20241011082438 20241011082616
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16A-IN INITIAL
CALIBRATION
SDG:L1784578 Calibration (begin) date/time:10/16/24 06:39
Instrument ID:ICP17 Calibration (end) date/time:10/16/24 06:49
Analytical Method:6010B Analytical Run:101624ICP17
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
ARSENIC 189.042 8 5 0.999949 206.709 -0.773845
BARIUM 233.527 8 5 0.999978 6496.036 -2.609982
CADMIUM 228.802 8 5 0.999947 3627.564 -2.277703
CHROMIUM 267.716 8 5 0.999996 3062.219 6.567311
LEAD 220.353 8 5 0.999933 647.2402 1.545316
SELENIUM 196.09 8 5 0.999916 112.5094 -0.03032
SILVER 328.068 8 5 0.999997 4743.558 1.22215
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
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16A-IN INITIAL
CALIBRATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 08:46
Instrument ID:ICP17 Calibration (end) date/time:10/07/24 08:56
Analytical Method:6010B Analytical Run:100724ICP17
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
ARSENIC 189.042 8 5 0.999982 177.8877 -0.959484
LEAD 220.353 8 5 0.999871 680.695 0.960188
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
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16A-IN INITIAL
CALIBRATION
SDG:L1784578 Calibration (begin) date/time:10/11/24 08:18
Instrument ID:ICP17 Calibration (end) date/time:10/11/24 08:27
Analytical Method:6010B Analytical Run:101124ICP17
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
ARSENIC 189.042 8 5 0.999717 177.2555 -1.064292
BARIUM 233.527 8 5 0.999999 7087.324 -3.614712
CADMIUM 228.802 8 5 0.999989 2165.466 -3.953133
CHROMIUM 267.716 8 5 0.999975 3280.266 10.73711
LEAD 220.353 8 5 0.999968 697.6368 1.642025
SELENIUM 196.09 8 5 0.99958 100.6372 0.101968
SILVER 328.068 8 5 0.999577 4800.458 1.468256
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
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7470A Mercury
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:20241005145148 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:11
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 14:51
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 U 0.000100 0.000200
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4128943-1
Lab Sample ID:R4128943-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20241005140615 Received Date/Time:_______________
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:08
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 14:06
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 U 0.000100 0.000200
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4128943-2
Lab Sample ID:R4128943-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20241005140848 Received Date/Time:_______________
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:08
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 14:08
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00319 0.000100 0.000200
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4128943-4
Lab Sample ID:R4128943-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/30/24 13:00
Lab File ID:20241005141617 Received Date/Time:10/02/24 08:00
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:11
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 14:16
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00140 J6 0.000100 0.000200
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4128943-5
Lab Sample ID:R4128943-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/30/24 13:00
Lab File ID:20241005141851 Received Date/Time:10/02/24 08:00
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:11
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 14:18
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00135 J6 0.000100 0.000200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4128943-6
Lab Sample ID:R4128943-6 SDG:L1784578
Client Sample ID:PS Collected Date/Time:09/30/24 13:00
Lab File ID:20241005164748 Received Date/Time:10/02/24 08:00
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:11
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 16:47
Dilution Factor:1 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 0.00143 O1 0.000100 0.000200
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4128943-3
Lab Sample ID:R4128943-3 SDG:L1784578
Client Sample ID:SD Collected Date/Time:09/30/24 13:00
Lab File ID:20241005141355 Received Date/Time:10/02/24 08:00
Instrument ID:CVAA9 Preparation Date/Time:10/04/24 10:11
Analytical Batch:WG2375204 Analysis Date/Time:10/05/24 14:13
Dilution Factor:5 Prep Method:7470A
Analytical Method:7470A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:30 mL
Total Solids (%):_______________Final Wt/Vol:30.0 mL
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Mercury 7439-97-6 U 0.000500 0.00100
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Concentration Units:mg/L
ICV ICVLL CCV
Sample ID:CVAA91005241146-2 CVAA91005241206-2 CVAA91005241353
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.005015278 100 6.550000 0.0002 0.000186703
1
93.4
0 4.700000 0.0050 0.00496315 99.3
0 2.570000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Concentration Units:mg/L
CCV CCV CCV
Sample ID:CVAA91005241423 CVAA91005241454 CVAA91005241627
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.005096378 102 2.550000 0.0050 0.005078363 102 3.950000 0.0050 0.004865824 97.3
0 1.500000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Concentration Units:mg/L
CCV CCV
Sample ID:CVAA91005241708-2 CVAA91005241710-2
Analyte True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.00485859
2
97.2
0 2.960000 0.0050 0.00487057 97.4
0 4.690000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCV Limits:90 - 110
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20241005115126-2 20241005135612 20241005140615 20241005142631
Analyte mg/L mg/L mg/l mg/L
MERCURY -0.0000009473
426 U -0.0000157062
5 U U 0.00001281772 U
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Sample ID:CCB Result CCB Qual CCB Result CCB Qual CCB Result CCB Qual
File ID:20241005145654 20241005162934 20241005171253-2
Analyte mg/L mg/L mg/L
MERCURY 0.00001372346 U 0.00000271201
7 U 0.00001158809 U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4128943-4
L1784578-17 R4128943-5
MS Sample / File ID:R4128943-4 / 20241005141617 SDG:L1784578
MSD Sample / File ID:R4128943-5 / 20241005141851 Analytical Batch:WG2375204
OS Sample / File ID:L1784402-03 / 20241005141122 Matrix:GW
Instrument ID:CVAA9
Analytical Method:7470A
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 U 0.00140 0.00135 46.6*44.9*1 75.0 - 125 3.56 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4128943-6
L1784578-17
PS Sample / File ID:R4128943-6 / 20241005164748 SDG:L1784578
OS Sample / File ID:L1784402-03 / 20241005141122 Analytical Batch:WG2375204
Instrument ID:CVAA9 Dilution Factor:1
Analytical Method:7470A Matrix:GW
Analyte Spike
Amount
OS
Result
PD
Result
DS
Result PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/l mg/l mg/l %%%mg/l mg/l
Mercury 0.00300 U 0.00143 47.8*1 80.0 -
120 *
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4128943-2
RECOVERY _______________
L1784578-17
LCS Sample / File ID:R4128943-2 / 20241005140848 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2375204
Instrument ID:CVAA9 Dilution Factor:1
Analytical Method:7470A Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l %%%%%
Mercury 0.00300 0.00319 106 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4128943-3
L1784578-17
SD Sample / File ID:R4128943-3 / 20241005141355 SDG:L1784578
OS Sample / File ID:L1784402-03 / 20241005141122 Analytical Batch:WG2375204
Lab File ID:20241005141355 Dilution Factor:5
Instrument ID:CVAA9 Matrix:GW
Analytical Method:7470A
Analyte OS
Result
SD
Result RPD RPD
Limits
mg/l mg/l %%
Mercury U U 0.000 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17 Analytical Method:7470A
Matrix:GW Prep Method:7470A
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Mercury 7439-97-6 253.70 0.0001 0.0002
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10C-IN LINEAR DYNAMIC RANGE
SDG:L1784578 Analytical Method:7470A
Instrument ID:CVAA9 Date:07/10/23 14:11
Analyte LDR
ppm
MERCURY 0.01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:7470A
Instrument ID:CVAA9 Calibration Start Date:10/05/24 11:31
Analytical Run:100524CVAA9 WE Calibration End Date:10/05/24 11:43
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK CVAA91005241128 20241005112837 10/05/24 11:28
CAL STD 0.2 20241005113106 10/05/24 11:31
CAL STD 0.4 20241005113335 10/05/24 11:33
CAL STD 1.0 20241005113604 10/05/24 11:36
CAL STD 2.0 20241005113835 10/05/24 11:38
CAL STD 5.0 20241005114106 10/05/24 11:41
CAL STD 10.0 20241005114335 10/05/24 11:43
ICV CVAA91005241146-2 20241005114627-2 10/05/24 11:46
ICB CVAA91005241151-2 20241005115126-2 10/05/24 11:51
ICVLL CVAA91005241206-2 20241005120626-2 10/05/24 12:06
CCV CVAA91005241353 20241005135339 10/05/24 13:53
CCB CVAA91005241356 20241005135612 10/05/24 13:56
BLANK R4128943-1 20241005140615 10/05/24 14:06 1 WG2375204
LCS R4128943-2 20241005140848 10/05/24 14:08 1 WG2375204
OS L1784402-03 20241005141122 10/05/24 14:11
L1784402-03 L1784402-03 20241005141122 10/05/24 14:11 1 WG2375204
SD R4128943-3 20241005141355 10/05/24 14:13 5 WG2375204
MS R4128943-4 20241005141617 10/05/24 14:16 1 WG2375204
MSD R4128943-5 20241005141851 10/05/24 14:18 1 WG2375204
L1784063-01 L1784063-01 20241005142125 10/05/24 14:21 1 WG2375204
CCV CVAA91005241423 20241005142359 10/05/24 14:23
CCB CVAA91005241426 20241005142631 10/05/24 14:26
L1784063-03 L1784063-03 20241005142903 10/05/24 14:29 1 WG2375204
EB-93024 L1784578-17 20241005145148 10/05/24 14:51 1 WG2375204
CCV CVAA91005241454 20241005145422 10/05/24 14:54
CCB CVAA91005241456 20241005145654 10/05/24 14:56
CCV CVAA91005241627 20241005162702 10/05/24 16:27
CCB CVAA91005241629 20241005162934 10/05/24 16:29
PS R4128943-6 20241005164748 10/05/24 16:47 1 WG2375204
L1784208-01 L1784208-01 20241005165921 10/05/24 16:59 20 WG2374312
CCV CVAA91005241708-2 20241005170810-2 10/05/24 17:08
CCV CVAA91005241710-2 20241005171021-2 10/05/24 17:10
CCB CVAA91005241712-2 20241005171253-2 10/05/24 17:12
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/L mg/L %mg/L mg/L %
MERCURY 0.0002 .0001731868 86.60 0.0004 .0004458182 111
File ID: 20241005113106 20241005113335
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/L mg/L %mg/L mg/L %
MERCURY 0.0010 .0009502922 95 0.0020 .001992651 99.60
File ID: 20241005113604 20241005113835
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/L mg/L %mg/L mg/L %
MERCURY 0.0050 .004897523 98 0.01 .01005638 101
File ID: 20241005114106 20241005114335
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16A-IN INITIAL
CALIBRATION
SDG:L1784578 Calibration (begin) date/time:10/05/24 11:31
Instrument ID:CVAA9 Calibration (end) date/time:10/05/24 11:43
Analytical Method:7470A Analytical Run:100524CVAA9 WE
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
MERCURY 253.7 0 5 0.999599 11.53662 -0.000971
Calibration Type
0 = Linear Regression
Weightage
5 = None
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7471B Mercury
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:20241007135938 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:59
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):83.9 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.226 0.0245 0.0477
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:20241007140214 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:02
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.35 g
Total Solids (%):87.1 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.947 0.0236 0.0459
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:20241007140452 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:04
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.35 g
Total Solids (%):83.0 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.487 0.0248 0.0482
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:20241007140730 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:07
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):85.5 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.208 0.0241 0.0468
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:20241007141519 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:15
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):90.4 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.195 0.0228 0.0442
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:20241007131510 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:15
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.128 0.0220 0.0427
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:20241007141757 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:17
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):95.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0320 J 0.0215 0.0418
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:20241007142034 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:20
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.34 g
Total Solids (%):84.6 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.560 0.0243 0.0473
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:20241007142312 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:23
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):97.4 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 U 0.0212 0.0411
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:20241007142550 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 14:25
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.34 g
Total Solids (%):86.3 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.0243 J 0.0239 0.0463
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129510-1
Lab Sample ID:R4129510-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20241007130955 Received Date/Time:_______________
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 17:58
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:09
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 U 0.0206 0.0400
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129510-2
Lab Sample ID:R4129510-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20241007131232 Received Date/Time:_______________
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 17:58
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:12
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.30 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.512 0.0206 0.0400
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129510-4
Lab Sample ID:R4129510-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:20241007132024 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 17:58
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:20
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.585 0.0220 0.0427
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129510-5
Lab Sample ID:R4129510-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:20241007132300 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 17:58
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:23
Dilution Factor:1 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.32 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.597 0.0220 0.0427
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129510-3
Lab Sample ID:R4129510-3 SDG:L1784578
Client Sample ID:SD Collected Date/Time:09/27/24 12:00
Lab File ID:20241007131747 Received Date/Time:10/02/24 09:00
Instrument ID:CVAA10 Preparation Date/Time:10/06/24 18:02
Analytical Batch:WG2376309 Analysis Date/Time:10/07/24 13:17
Dilution Factor:5 Prep Method:7471A
Analytical Method:7471B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.31 g
Total Solids (%):93.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Mercury 7439-97-6 0.135 0.110 0.214
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Concentration Units:mg/kg
ICV ICVLL CCVLL
Sample ID:CVAA101007241017 CVAA101007241027 CVAA101007241204
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.00504930
6 101 1.150000 0.0002 0.000209041
5 105 0.980000 0.0002 0.00020762
58 104 1.080000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCVLL Limits:70 - 130 CCV Limits:90 - 110
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Concentration Units:mg/kg
CCV CCV CCVLL
Sample ID:CVAA101007241304 CVAA101007241336-2 CVAA101007241341
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.00489429 97.9
0 2.140000 0.0050 0.00485993
9
97.2
0 1.800000 0.0002 0.000203101
4 102 2.500000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCVLL Limits:70 - 130 CCV Limits:90 - 110
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2-IN CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Concentration Units:mg/kg
CCV CCV CCVLL
Sample ID:CVAA101007241410 CVAA101007241441 CVAA101007241518
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
MERCURY 0.0050 0.004849527 97 1.860000 0.0050 0.004783345 95.7
0 2.740000 0.0002 0.000201721
2 101 1.810000
ICV Limits:90 - 110 ICVLL Limits:70 - 130 CCVLL Limits:70 - 130 CCV Limits:90 - 110
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20241007101944 20241007130721 20241007130955 20241007133840-2
Analyte mg/kg mg/kg mg/kg mg/kg
MERCURY 0.00000778664
7 U 0.00000418810
6 U U 0.0000066638
68 U
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Sample ID:CCB Result CCB Qual CCB Result CCB Qual
File ID:20241007141244 20241007144414
Analyte mg/kg mg/kg
MERCURY 0.00000612316 U 0.00000810860
8 U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4129510-4
L1784578-01,02,03,04,05,06,11,12,13,15 R4129510-5
MS Sample / File ID:R4129510-4 / 20241007132024 SDG:L1784578
MSD Sample / File ID:R4129510-5 / 20241007132300 Analytical Batch:WG2376309
OS Sample / File ID:L1784578-06 / 20241007131510 Matrix:Solid
Instrument ID:CVAA10
Analytical Method:7471B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.534 0.128 0.585 0.597 85.7 87.9 1 75.0 - 125 1.94 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129510-2
RECOVERY _______________
L1784578-01,02,03,04,05,06,11,12,13,15
LCS Sample / File ID:R4129510-2 / 20241007131232 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2376309
Instrument ID:CVAA10 Dilution Factor:1
Analytical Method:7471B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Mercury 0.500 0.512 102 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4129510-3
L1784578-01,02,03,04,05,06,11,12,13,15
SD Sample / File ID:R4129510-3 / 20241007131747 SDG:L1784578
OS Sample / File ID:L1784578-06 / 20241007131510 Analytical Batch:WG2376309
Lab File ID:20241007131747 Dilution Factor:5
Instrument ID:CVAA10 Matrix:Solid
Analytical Method:7471B
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Mercury 0.128 0.135 5.97 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,11,12,13,15 Analytical Method:7471B
Matrix:Solid Prep Method:7471A
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Mercury 7439-97-6 253.70 0.0206 0.04
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:7471B
Instrument ID:CVAA10 Calibration Start Date:10/07/24 09:21
Analytical Run:100724CVAA10 S Calibration End Date:10/07/24 09:34
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK CVAA101007240918 20241007091854 10/07/24 09:18
CAL STD 0.2 20241007092128 10/07/24 09:21
CAL STD 0.4 20241007092403 10/07/24 09:24
CAL STD 2.0 20241007092914 10/07/24 09:29
CAL STD 10.0 20241007093425 10/07/24 09:34
ICV CVAA101007241017 20241007101709 10/07/24 10:17
ICB CVAA101007241019 20241007101944 10/07/24 10:19
ICVLL CVAA101007241027 20241007102728 10/07/24 10:27
CCVLL CVAA101007241204 20241007120443 10/07/24 12:04
CCV CVAA101007241304 20241007130445 10/07/24 13:04
CCB CVAA101007241307 20241007130721 10/07/24 13:07
BLANK R4129510-1 20241007130955 10/07/24 13:09 1 WG2376309
LCS R4129510-2 20241007131232 10/07/24 13:12 1 WG2376309
S-10 (0-6)L1784578-06 20241007131510 10/07/24 13:15 1 WG2376309
SD R4129510-3 20241007131747 10/07/24 13:17 5 WG2376309
MS R4129510-4 20241007132024 10/07/24 13:20 1 WG2376309
MSD R4129510-5 20241007132300 10/07/24 13:23 1 WG2376309
L1784409-10 L1784409-10 20241007132536 10/07/24 13:25 1 WG2376309
L1784409-11 L1784409-11 20241007132813 10/07/24 13:28 1 WG2376309
L1784409-12 L1784409-12 20241007133050 10/07/24 13:30 1 WG2376309
L1784409-13 L1784409-13 20241007133327 10/07/24 13:33 1 WG2376309
CCV CVAA101007241336-2 20241007133605-2 10/07/24 13:36
CCB CVAA101007241338-2 20241007133840-2 10/07/24 13:38
CCVLL CVAA101007241341 20241007134115 10/07/24 13:41
L1784482-05 L1784482-05 20241007134626 10/07/24 13:46 1 WG2376309
L1784482-06 L1784482-06 20241007134904 10/07/24 13:49 1 WG2376309
L1784525-01 L1784525-01 20241007135421 10/07/24 13:54 1 WG2376309
L1784539-02 L1784539-02 20241007135659 10/07/24 13:56 1 WG2376309
S-13 (0-6)L1784578-01 20241007135938 10/07/24 13:59 1 WG2376309
S-15 (0-6)L1784578-02 20241007140214 10/07/24 14:02 1 WG2376309
S-32 (0-6)L1784578-03 20241007140452 10/07/24 14:04 1 WG2376309
S-12 (6-12)L1784578-04 20241007140730 10/07/24 14:07 1 WG2376309
CCV CVAA101007241410 20241007141009 10/07/24 14:10
CCB CVAA101007241412 20241007141244 10/07/24 14:12
S-12 (0-6)L1784578-05 20241007141519 10/07/24 14:15 1 WG2376309
S-10 (6-12)L1784578-11 20241007141757 10/07/24 14:17 1 WG2376309
S-14 (0-6)L1784578-12 20241007142034 10/07/24 14:20 1 WG2376309
S-11 (0-6)L1784578-13 20241007142312 10/07/24 14:23 1 WG2376309
S-14 (6-12)L1784578-15 20241007142550 10/07/24 14:25 1 WG2376309
BLANK R4129553-1 20241007142828 10/07/24 14:28 1 WG2376742
LCS R4129553-2 20241007143106 10/07/24 14:31 1 WG2376742
OS L1785073-04 20241007143345 10/07/24 14:33
L1785073-04 L1785073-04 20241007143345 10/07/24 14:33 1 WG2376742
SD R4129553-3 20241007143623 10/07/24 14:36 5 WG2376742
MS R4129553-4 20241007143901 10/07/24 14:39 1 WG2376742
CCV CVAA101007241441 20241007144139 10/07/24 14:41
CCB CVAA101007241444 20241007144414 10/07/24 14:44
CCVLL CVAA101007241518 20241007151820 10/07/24 15:18
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0002 .0001797988 89.90 0.0004 .000383112 95.80
File ID: 20241007092128 20241007092403
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/kg mg/kg %mg/kg mg/kg %
MERCURY 0.0020 .002009024 100 0.01 .009950831 99.50
File ID: 20241007092914 20241007093425
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16A-IN INITIAL
CALIBRATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 09:21
Instrument ID:CVAA10 Calibration (end) date/time:10/07/24 09:34
Analytical Method:7471B Analytical Run:100724CVAA10 S
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
MERCURY 253.7 0 5 0.999887 17.06568 0.000477
Calibration Type
0 = Linear Regression
Weightage
5 = None
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8015 Semi-Volatile Organic Compounds (GC)
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2A-OR SURROGATE RECOVERY
Analytical Method:8015 SDG:L1784578
Matrix:Solid
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
S-13 (0-6)L1784578-01 SVGC50 1015_044 89.2 0
S-15 (0-6)L1784578-02 SVGC50 1011_027 93.0 0
S-32 (0-6)L1784578-03 SVGC50 1015_043 76.4 0
S-12 (6-12)L1784578-04 SVGC7 1012_009 81.0D 1
S-12 (0-6)L1784578-05 SVGC7 1012_013 80.5 0
S-10 (0-6)L1784578-06 SVGC7 1012_010 85.0D 1
S-10 (6-12)L1784578-11 SVGC50 1011_029 85.0 0
S-14 (0-6)L1784578-12 SVGC50 1015_045 97.7 0
S-11 (0-6)L1784578-13 SVGC50 1015_047 89.8D 1
S-14 (6-12)L1784578-15 SVGC50 1015_040 89.6 0
MS R4131935-1 SVGC7 1012_011 83.3D 1
MSD R4131935-2 SVGC7 1012_012 84.7D 1
MS R4133395-3 SVGC50 1015_038 88.0 0
MSD R4133395-4 SVGC50 1015_039 91.8 0
BLANK R4131845-1 SVGC50 1011_010 88.6 0
BLANK R4133395-1 SVGC50 1015_035 97.3 0
LCS R4131845-2 SVGC50 1011_011 100 0
LCS R4133395-2 SVGC50 1015_036 106 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 o-Terphenyl 18.0 - 148
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131935-1
L1784578-02,04,05,06,11 R4131935-2
MS Sample / File ID:R4131935-1 / 1012_011 SDG:L1784578
MSD Sample / File ID:R4131935-2 / 1012_012 Analytical Batch:WG2380134
OS Sample / File ID:L1784578-06 / 1012_010 Matrix:Solid
Instrument ID:SVGC7
Analytical Method:8015
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 52.2 49.8 57.4 65.9 14.7*30.9*20 50.0 - 150 13.7 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4133395-3
L1784578-01,03,12,13,15 R4133395-4
MS Sample / File ID:R4133395-3 / 1015_038 SDG:L1784578
MSD Sample / File ID:R4133395-4 / 1015_039 Analytical Batch:WG2380815
OS Sample / File ID:L1785084-03 / 1015_037 Matrix:Solid
Instrument ID:SVGC50
Analytical Method:8015
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 63.0 5.46 55.5 56.7 79.5 81.2 1 50.0 - 150 2.10 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131845-2
RECOVERY _______________
L1784578-02,04,05,06,11
LCS Sample / File ID:R4131845-2 / 1011_011 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2380134
Instrument ID:SVGC50 Dilution Factor:1
Analytical Method:8015 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 50.0 43.4 86.8 50.0 - 150
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4133395-2
RECOVERY _______________
L1784578-01,03,12,13,15
LCS Sample / File ID:R4133395-2 / 1015_036 SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2380815
Instrument ID:SVGC50 Dilution Factor:1
Analytical Method:8015 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 50.0 45.6 91.2 50.0 - 150
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4131845-1
Lab Sample ID:R4131845-1 SDG:L1784578
Lab File ID:1011_010 Preparation Date/Time:10/11/24 08:00
Instrument ID:SVGC50 Analysis Date/Time:10/11/24 20:04
Analytical Batch:WG2380134 Dilution Factor:1
Analytical Method:8015 Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4131845-2 SVGC50 1011_011 10/11/24 20:16
S-15 (0-6)L1784578-02 SVGC50 1011_027 10/11/24 23:35
S-10 (6-12)L1784578-11 SVGC50 1011_029 10/11/24 23:59
S-12 (6-12)L1784578-04 SVGC7 1012_009 10/12/24 11:11
S-10 (0-6)L1784578-06 SVGC7 1012_010 10/12/24 11:24
MS R4131935-1 SVGC7 1012_011 10/12/24 11:37
MSD R4131935-2 SVGC7 1012_012 10/12/24 11:50
S-12 (0-6)L1784578-05 SVGC7 1012_013 10/12/24 12:03

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
Dilution due to matrix impact during extract concentration procedure
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4A-OR METHOD BLANK SAMPLE NO.:
R4133395-1
Lab Sample ID:R4133395-1 SDG:L1784578
Lab File ID:1015_035 Preparation Date/Time:10/12/24 19:38
Instrument ID:SVGC50 Analysis Date/Time:10/15/24 16:52
Analytical Batch:WG2380815 Dilution Factor:1
Analytical Method:8015 Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4133395-2 SVGC50 1015_036 10/15/24 17:05
OS L1785084-03 SVGC50 1015_037 10/15/24 17:17
MS R4133395-3 SVGC50 1015_038 10/15/24 17:30
MSD R4133395-4 SVGC50 1015_039 10/15/24 17:42
S-14 (6-12)L1784578-15 SVGC50 1015_040 10/15/24 17:54
S-32 (0-6)L1784578-03 SVGC50 1015_043 10/15/24 18:32
S-13 (0-6)L1784578-01 SVGC50 1015_044 10/15/24 18:44
S-14 (0-6)L1784578-12 SVGC50 1015_045 10/15/24 18:56
S-11 (0-6)L1784578-13 SVGC50 1015_047 10/15/24 19:21

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
Dilution due to matrix impact during extract concentration procedure
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:1015_044 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:39
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 18:44
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.21 g
Total Solids (%):83.9 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 6.92 0.916 4.77
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:1011_027 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/11/24 23:35
Dilution Factor:5 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.28 g
Total Solids (%):87.1 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.59 72.1 4.42 23.0
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:1015_043 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:39
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 18:32
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.14 g
Total Solids (%):83.0 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 3.17 J 0.927 4.82
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:1012_009 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC7 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/12/24 11:11
Dilution Factor:50 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.31 g
Total Solids (%):85.5 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.88 126 J 45.0 234

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:1012_013 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC7 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/12/24 12:03
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.15 g
Total Solids (%):90.4 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.88 39.6 J 8.50 44.2

Sample Narrative:
Dilution due to matrix impact during extract concentration procedure
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:1012_010 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC7 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/12/24 11:24
Dilution Factor:20 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):93.7 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.88 49.8 J J6 16.4 85.4

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:1011_029 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/11/24 23:59
Dilution Factor:10 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.28 g
Total Solids (%):95.7 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.59 41.6 J 8.03 41.8

Sample Narrative:
Cannot run at lower dilution due to viscosity of extract
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:1015_045 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:39
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 18:56
Dilution Factor:2 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.52 g
Total Solids (%):84.6 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 29.7 1.82 9.45
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:1015_047 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:39
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 19:21
Dilution Factor:20 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.48 g
Total Solids (%):97.4 Final Wt/Vol:1 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 114 15.8 82.2
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:1015_040 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:39
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 17:54
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.32 g
Total Solids (%):86.3 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 2.26 J 0.891 4.63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 240 of 526
6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/02/24 19:00
Instrument ID:SVGC7 Calibration (end) date/time:09/24/24 11:25
Analytical Method:8015
Analyte CS: 100 CS: 200 CS: 500 CS: 1000 CS: 2000 CS: 3000 CS: 5000 CS: 10000
TPH (GC/FID) HIGH FRACTION 1.99 1.99 1.99 1.99 1.99 1.99 1.99 1.99
O-TERPHENYL 3.62 3.62 3.62 3.62 3.62 3.62 3.62 3.63
File ID:0802A_01
0
0802A_01
1
0802A_01
2
0802A_01
3
0802A_01
4
0802A_01
5
0802A_01
6
0802A_01
7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 241 of 526
6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Analytical Method:8015
Analyte CS: 100 CS: 200 CS: 500 CS: 1000 CS: 2000 CS: 3000 CS: 5000 CS: 10000
TPH (GC/FID) HIGH FRACTION 1.71 1.71 1.71 1.71 1.71 1.71 1.71 1.71
O-TERPHENYL 3.30 3.30 3.30 3.30 3.31 3.31 3.31 3.32
File ID:0626A_01
0
0626A_01
1
0626A_01
2
0626A_01
3
0626A_01
4
0626A_01
5
0626A_01
6
0626A_01
7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 242 of 526
6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Analytical Method:8015
Analyte CS: 100 CS: 200 CS: 500 CS: 1000 CS: 2000 CS: 3000 CS: 5000 CS: 10000
TPH (GC/FID) HIGH FRACTION 1.71 1.71 1.71 1.71 1.71 1.71 1.71 1.71
O-TERPHENYL 3.30 3.30 3.30 3.30 3.31 3.31 3.31 3.32
File ID:0626A_01
0
0626A_01
1
0626A_01
2
0626A_01
3
0626A_01
4
0626A_01
5
0626A_01
6
0626A_01
7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 243 of 526
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/02/24 19:00
Instrument ID:SVGC7 Calibration (end) date/time:09/24/24 11:25
Analytical Method:8015
Analyte RRF: 100 RRF: 200 RRF: 500 RRF: 1000 RRF: 2000 RRF: 3000 RRF: 5000 RRF: 10000
TPH (GC/FID) HIGH FRACTION 1097000 1047000 1011000 1093000 1051000 1031000 1035000 1021000
O-TERPHENYL 1228000 1148000 1106000 1157000 1042000 1009000 1024000 973000
File ID:0802A_010 0802A_011 0802A_012 0802A_013 0802A_014 0802A_015 0802A_016 0802A_017
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 244 of 526
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/02/24 19:00
Instrument ID:SVGC7 Calibration (end) date/time:09/24/24 11:25
Analytical Method:8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 1048240 2.99 1
O-TERPHENYL 1085903 8.09
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 245 of 526
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Analytical Method:8015
Analyte RRF: 100 RRF: 200 RRF: 500 RRF: 1000 RRF: 2000 RRF: 3000 RRF: 5000 RRF: 10000
TPH (GC/FID) HIGH FRACTION 2325000 2187000 2131000 2320000 2255000 2267000 2215000 2225000
O-TERPHENYL 2263000 2316000 2331000 2409000 2292000 2236000 2232000 2190000
File ID:0626A_010 0626A_011 0626A_012 0626A_013 0626A_014 0626A_015 0626A_016 0626A_017
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 246 of 526
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Analytical Method:8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 2240621 2.93 1
O-TERPHENYL 2283651 3.02
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 247 of 526
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Analytical Method:8015
Analyte RRF: 100 RRF: 200 RRF: 500 RRF: 1000 RRF: 2000 RRF: 3000 RRF: 5000 RRF: 10000
TPH (GC/FID) HIGH FRACTION 2325000 2187000 2131000 2320000 2255000 2267000 2215000 2225000
O-TERPHENYL 2263000 2316000 2331000 2409000 2292000 2236000 2232000 2190000
File ID:0626A_010 0626A_011 0626A_012 0626A_013 0626A_014 0626A_015 0626A_016 0626A_017
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 248 of 526
6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Analytical Method:8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 2240621 2.93 1
O-TERPHENYL 2283651 3.02
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 249 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/02/24 19:00
Instrument ID:SVGC7 Calibration (end) date/time:09/24/24 11:25
Lab File ID:0802A_027 Analysis date/time:08/03/24 00:00
Analytical Method:8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 1048240 930391.30 11.20 1500 1348 89.90 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 250 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/02/24 19:00
Instrument ID:SVGC7 Calibration (end) date/time:09/24/24 11:25
Lab File ID:1012_004 Analysis date/time:10/12/24 09:56
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 1048240 1090892 4.07 3000 3172 106 85 - 115
O-TERPHENYL 1085903 1757678 61.90 20 32.37 162 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 251 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/02/24 19:00
Instrument ID:SVGC7 Calibration (end) date/time:09/24/24 11:25
Lab File ID:1012_020 Analysis date/time:10/12/24 13:34
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 1048240 1140736 8.82 3000 3317 111 85 - 115
O-TERPHENYL 1085903 1591282 46.50 20 29.31 147 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 252 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Lab File ID:0626A_028 Analysis date/time:06/26/24 22:32
Analytical Method:8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2240621 2034139 9.22 1500 1365 91 80 - 120
TPH (GC/FID) HIGH FRACTION 2240621 2034139 9.22 1500 1365 91 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 253 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Lab File ID:1011_003 Analysis date/time:10/11/24 09:09
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2240621 2512824 12.10 3000 3376 113 85 - 115
O-TERPHENYL 2283651 2616849 14.60 20 22.92 115 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 254 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Lab File ID:1011_007 Analysis date/time:10/11/24 19:27
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2240621 2364233 5.52 3000 3176 106 85 - 115
O-TERPHENYL 2283651 2959144 29.60 20 25.92 130 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 255 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Lab File ID:1011_037 Analysis date/time:10/12/24 01:39
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2240621 2360416 5.35 3000 3171 106 85 - 115
O-TERPHENYL 2283651 2949861 29.20 20 25.83 129 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 256 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Lab File ID:1015_032 Analysis date/time:10/15/24 16:15
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2240621 2390414 6.69 3000 3211 107 85 - 115
O-TERPHENYL 2283651 3262471 42.90 20 28.57 143 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 257 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 17:36
Instrument ID:SVGC50 Calibration (end) date/time:06/26/24 21:55
Lab File ID:1015_049 Analysis date/time:10/15/24 19:46
Analytical Method:8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 2240621 2296889 2.51 3000 3085 103 85 - 115
O-TERPHENYL 2283651 3012156 31.90 20 26.38 132 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 258 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015
Instrument ID:SVGC7 Calibration Start Date:08/02/24 19:00
Calibration End Date:09/24/24 11:25
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 100A 0802A_004 08/02/24 19:00
CAL 400A 0802A_005 08/02/24 19:13
CAL 1KA 0802A_006 08/02/24 19:26
CAL 2500 0802A_007 08/02/24 19:39
CAL 5KA 0802A_008 08/02/24 19:52
CAL 100 0802A_010 08/02/24 20:18
CAL 200 0802A_011 08/02/24 20:31
CAL 500 0802A_012 08/02/24 20:44
CAL 1000 0802A_013 08/02/24 20:57
CAL 2000 0802A_014 08/02/24 21:10
CAL 3000 0802A_015 08/02/24 21:23
CAL 5000 0802A_016 08/02/24 21:36
CAL 10000 0802A_017 08/02/24 21:49
SSCV SVGC7080224A0802A_027759406 0802A_027 08/03/24 00:00
CAL 100M 0924_007 09/24/24 10:06
CAL 200M 0924_008 09/24/24 10:19
CAL 500M 0924_009 09/24/24 10:33
CAL 1KM 0924_010 09/24/24 10:45
CAL 2KM 0924_011 09/24/24 10:59
CAL 2.5000 0924_012 09/24/24 11:12
CAL 5KM 0924_013 09/24/24 11:25
CCV SVGC71012241012_003759406 1012_003 10/12/24 09:43
CCV SVGC71012241012_004759406 1012_004 10/12/24 09:56
S-12 (6-12)L1784578-04 1012_009 10/12/24 11:11 50 WG2380134
S-10 (0-6)L1784578-06 1012_010 10/12/24 11:24 20 WG2380134
MS R4131935-1 1012_011 10/12/24 11:37 20 WG2380134
MSD R4131935-2 1012_012 10/12/24 11:50 20 WG2380134
S-12 (0-6)L1784578-05 1012_013 10/12/24 12:03 10 WG2380134
L1784475-01 L1784475-01 1012_015 10/12/24 12:29 100 WG2380134
CCV SVGC71012241012_019759406 1012_019 10/12/24 13:21
CCV SVGC71012241012_020759406 1012_020 10/12/24 13:34
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 259 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015
Instrument ID:SVGC50 Calibration Start Date:06/26/24 17:36
Calibration End Date:06/26/24 21:55
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 100A 0626A_004 06/26/24 17:36
CAL 400A 0626A_005 06/26/24 17:49
CAL 1KA 0626A_006 06/26/24 18:01
CAL 2500 0626A_007 06/26/24 18:12
CAL 5KA 0626A_008 06/26/24 18:25
CAL 100 0626A_010 06/26/24 18:50
CAL 200 0626A_011 06/26/24 19:01
CAL 500 0626A_012 06/26/24 19:13
CAL 1000 0626A_013 06/26/24 19:26
CAL 2000 0626A_014 06/26/24 19:38
CAL 3000 0626A_015 06/26/24 19:51
CAL 5000 0626A_016 06/26/24 20:03
CAL 10000 0626A_017 06/26/24 20:15
CAL 100M 0626A_019 06/26/24 20:40
CAL 200M 0626A_020 06/26/24 20:53
CAL 500M 0626A_021 06/26/24 21:05
CAL 1KM 0626A_022 06/26/24 21:17
CAL 2KM 0626A_023 06/26/24 21:30
CAL 2.5000 0626A_024 06/26/24 21:42
CAL 5KM 0626A_025 06/26/24 21:55
SSCV SVGC50062624A0626A_028759404 0626A_028 06/26/24 22:32
CCV SVGC501011241011_003759404 1011_003 10/11/24 09:09
CCV SVGC501011241011_004759404 1011_004 10/11/24 09:22
CCV SVGC501011241011_007759404 1011_007 10/11/24 19:27
CCV SVGC501011241011_008759404 1011_008 10/11/24 19:39
BLANK R4131845-1 1011_010 10/11/24 20:04 1 WG2380134
LCS R4131845-2 1011_011 10/11/24 20:16 1 WG2380134
S-15 (0-6)L1784578-02 1011_027 10/11/24 23:35 5 WG2380134
S-10 (6-12)L1784578-11 1011_029 10/11/24 23:59 10 WG2380134
CCV SVGC501011241011_037759404 1011_037 10/12/24 01:39
CCV SVGC501011241011_038759404 1011_038 10/12/24 01:51
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 260 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015
Instrument ID:SVGC50 Calibration Start Date:06/26/24 17:36
Calibration End Date:06/26/24 21:55
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 100A 0626A_004 06/26/24 17:36
CAL 400A 0626A_005 06/26/24 17:49
CAL 1KA 0626A_006 06/26/24 18:01
CAL 2500 0626A_007 06/26/24 18:12
CAL 5KA 0626A_008 06/26/24 18:25
CAL 100 0626A_010 06/26/24 18:50
CAL 200 0626A_011 06/26/24 19:01
CAL 500 0626A_012 06/26/24 19:13
CAL 1000 0626A_013 06/26/24 19:26
CAL 2000 0626A_014 06/26/24 19:38
CAL 3000 0626A_015 06/26/24 19:51
CAL 5000 0626A_016 06/26/24 20:03
CAL 10000 0626A_017 06/26/24 20:15
CAL 100M 0626A_019 06/26/24 20:40
CAL 200M 0626A_020 06/26/24 20:53
CAL 500M 0626A_021 06/26/24 21:05
CAL 1KM 0626A_022 06/26/24 21:17
CAL 2KM 0626A_023 06/26/24 21:30
CAL 2.5000 0626A_024 06/26/24 21:42
CAL 5KM 0626A_025 06/26/24 21:55
SSCV SVGC50062624A0626A_028760321 0626A_028 06/26/24 22:32
CCV SVGC501015241015_032760321 1015_032 10/15/24 16:15
CCV SVGC501015241015_033760321 1015_033 10/15/24 16:27
BLANK R4133395-1 1015_035 10/15/24 16:52 1 WG2380815
LCS R4133395-2 1015_036 10/15/24 17:05 1 WG2380815
OS L1785084-03 1015_037 10/15/24 17:17
L1785084-03 L1785084-03 1015_037 10/15/24 17:17 1 WG2380815
MS R4133395-3 1015_038 10/15/24 17:30 1 WG2380815
MSD R4133395-4 1015_039 10/15/24 17:42 1 WG2380815
S-14 (6-12)L1784578-15 1015_040 10/15/24 17:54 1 WG2380815
L1785084-01 L1785084-01 1015_041 10/15/24 18:07 1 WG2380815
L1785084-02 L1785084-02 1015_042 10/15/24 18:19 1 WG2380815
S-32 (0-6)L1784578-03 1015_043 10/15/24 18:32 1 WG2380815
S-13 (0-6)L1784578-01 1015_044 10/15/24 18:44 1 WG2380815
S-14 (0-6)L1784578-12 1015_045 10/15/24 18:56 2 WG2380815
S-11 (0-6)L1784578-13 1015_047 10/15/24 19:21 20 WG2380815
CCV SVGC501015241015_049760321 1015_049 10/15/24 19:46
CCV SVGC501015241015_050760321 1015_050 10/15/24 19:58
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 261 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,11,12,13,15 Analytical Method:8015
Matrix:Solid Prep Method:3546
Analyte CAS MDL RDL
mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 0.7690 4
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 262 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131845-1
Lab Sample ID:R4131845-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1011_010 Received Date/Time:_______________
Instrument ID:SVGC50 Preparation Date/Time:10/11/24 08:00
Analytical Batch:WG2380134 Analysis Date/Time:10/11/24 20:04
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.59 U 0.769 4.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 263 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133395-1
Lab Sample ID:R4133395-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1015_035 Received Date/Time:_______________
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:38
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 16:52
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 U 0.769 4.00
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131845-2
Lab Sample ID:R4131845-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1011_011 Received Date/Time:_______________
Instrument ID:SVGC50 Preparation Date/Time:10/11/24 08:00
Analytical Batch:WG2380134 Analysis Date/Time:10/11/24 20:16
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.59 43.4 1.33 4.00
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133395-2
Lab Sample ID:R4133395-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1015_036 Received Date/Time:_______________
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:38
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 17:05
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15 g
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 45.6 1.33 4.00
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131935-1
Lab Sample ID:R4131935-1 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:1012_011 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC7 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/12/24 11:37
Dilution Factor:20 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.35 g
Total Solids (%):93.7 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.88 57.4 J6 16.4 85.4
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133395-3
Lab Sample ID:R4133395-3 SDG:L1784578
Client Sample ID:MS Collected Date/Time:10/01/24 10:48
Lab File ID:1015_038 Received Date/Time:10/03/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:38
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 17:30
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.57 g
Total Solids (%):76.6 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 55.5 1.00 5.22
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131935-2
Lab Sample ID:R4131935-2 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:1012_012 Received Date/Time:10/02/24 09:00
Instrument ID:SVGC7 Preparation Date/Time:10/11/24 08:02
Analytical Batch:WG2380134 Analysis Date/Time:10/12/24 11:50
Dilution Factor:20 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.35 g
Total Solids (%):93.7 Final Wt/Vol:5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.88 65.9 J6 16.4 85.4
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133395-4
Lab Sample ID:R4133395-4 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:10/01/24 10:48
Lab File ID:1015_039 Received Date/Time:10/03/24 09:00
Instrument ID:SVGC50 Preparation Date/Time:10/12/24 19:38
Analytical Batch:WG2380815 Analysis Date/Time:10/15/24 17:42
Dilution Factor:1 Prep Method:3546
Analytical Method:8015 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:15.53 g
Total Solids (%):76.6 Final Wt/Vol:0.5 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction 68334-30-5 1.57 56.7 1.00 5.22
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8015D/GRO Volatile Organic Compounds (GC)
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2A-OR SURROGATE RECOVERY
Analytical Method:8015D/GRO SDG:L1784578
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
EB-93024 L1784578-17 VOCGC12 1009_07 99.2 0
MS R4131083-4 VOCGC12 1009_26 103 0
MSD R4131083-5 VOCGC12 1009_27 105 0
BLANK R4131083-3 VOCGC12 1009_05 99.4 0
LCS R4131083-1 VOCGC12 1009_02U 105 0
LCSD R4131083-2 VOCGC12 1009_03 105 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 a,a,a-Trifluorotoluene(FID)78.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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2A-OR SURROGATE RECOVERY
Analytical Method:8015D/GRO SDG:L1784578
Matrix:Solid
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
S-13 (0-6)L1784578-01 VOCGC17 1008_21 96.7 0
S-15 (0-6)L1784578-02 VOCGC17 1008_22 94.0 0
S-32 (0-6)L1784578-03 VOCGC17 1008_23 93.6 0
S-12 (6-12)L1784578-04 VOCGC17 1008_24 95.6 0
S-12 (0-6)L1784578-05 VOCGC17 1008_25 92.7 0
S-10 (0-6)L1784578-06 VOCGC17 1008_50 95.5 0
S-10 (6-12)L1784578-11 VOCGC15 1008_26 99.6 0
S-14 (0-6)L1784578-12 VOCGC15 1008_27 99.0 0
S-11 (0-6)L1784578-13 VOCGC15 1008_28 100 0
S-14 (6-12)L1784578-15 VOCGC15 1008_29 99.0 0
MS R4130871-4 VOCGC17 1008_63 107 0
MSD R4130871-5 VOCGC17 1008_64 108 0
MS R4132130-4 VOCGC15 1008_32 108 0
MSD R4132130-5 VOCGC15 1008_33 107 0
BLANK R4132130-3 VOCGC15 1008_08 99.4 0
BLANK R4130869-2 VOCGC17 1008_06A 96.8 0
BLANK R4130871-3 VOCGC17 1008_37 96.3 0
LCS R4132130-1 VOCGC15 1008_04 108 0
LCS R4130869-1 VOCGC17 1008_03A 108 0
LCS R4130871-1 VOCGC17 1008_33 107 0
LCSD R4132130-2 VOCGC15 1008_05 108 0
LCSD R4130871-2 VOCGC17 1008_34 108 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 a,a,a-Trifluorotoluene(FID)77.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4130871-4
L1784578-06 R4130871-5
MS Sample / File ID:R4130871-4 / 1008_63 SDG:L1784578
MSD Sample / File ID:R4130871-5 / 1008_64 Analytical Batch:WG2378256
OS Sample / File ID:L1784578-06 / 1008_50 Matrix:Solid
Instrument ID:VOCGC17
Analytical Method:8015D/GRO
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 193 4.59 228 231 116 117 34.5 10.0 - 151 1.46 28
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131083-4
L1784578-17 R4131083-5
MS Sample / File ID:R4131083-4 / 1009_26 SDG:L1784578
MSD Sample / File ID:R4131083-5 / 1009_27 Analytical Batch:WG2378697
OS Sample / File ID:L1784965-03 / 1009_17 Matrix:GW
Instrument ID:VOCGC12
Analytical Method:8015D/GRO
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.00 0.0316 5.89 6.51 117 130 1 10.0 - 160 10.0 22
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4132130-4
L1784578-11,12,13,15 R4132130-5
MS Sample / File ID:R4132130-4 / 1008_32 SDG:L1784578
MSD Sample / File ID:R4132130-5 / 1008_33 Analytical Batch:WG2377924
OS Sample / File ID:L1784370-04 / 1008_21 Matrix:Solid
Instrument ID:VOCGC15
Analytical Method:8015D/GRO
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 140 1.35 131 131 92.6 92.6 28 10.0 - 151 0.000 28
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4130869-1
RECOVERY _______________
L1784578-01,02,03,04,05
LCS Sample / File ID:R4130869-1 / 1008_03A SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2377829
Instrument ID:VOCGC17 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 5.72 114 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4130871-1
RECOVERY R4130871-2
L1784578-06
LCS Sample / File ID:R4130871-1 / 1008_33 SDG:L1784578
LCSD Sample / File ID:R4130871-2 / 1008_34 Analytical Batch:WG2378256
Instrument ID:VOCGC17 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 5.58 5.87 112 117 72.0 - 127 5.07 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131083-1
RECOVERY R4131083-2
L1784578-17
LCS Sample / File ID:R4131083-1 / 1009_02U SDG:L1784578
LCSD Sample / File ID:R4131083-2 / 1009_03 Analytical Batch:WG2378697
Instrument ID:VOCGC12 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.00 5.55 5.36 111 107 72.0 - 127 3.48 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4132130-1
RECOVERY R4132130-2
L1784578-11,12,13,15
LCS Sample / File ID:R4132130-1 / 1008_04 SDG:L1784578
LCSD Sample / File ID:R4132130-2 / 1008_05 Analytical Batch:WG2377924
Instrument ID:VOCGC15 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.00 4.64 5.37 92.8 107 72.0 - 127 14.6 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4131083-3
Lab Sample ID:R4131083-3 SDG:L1784578
Lab File ID:1009_05 Preparation Date/Time:10/09/24 10:15
Instrument ID:VOCGC12 Analysis Date/Time:10/09/24 10:15
Analytical Batch:WG2378697 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4131083-1 VOCGC12 1009_02U 10/09/24 09:09
LCSD R4131083-2 VOCGC12 1009_03 10/09/24 09:31
EB-93024 L1784578-17 VOCGC12 1009_07 10/09/24 12:31
OS L1784965-03 VOCGC12 1009_17 10/09/24 16:11
MS R4131083-4 VOCGC12 1009_26 10/09/24 19:28
MSD R4131083-5 VOCGC12 1009_27 10/09/24 19:50
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4A-OR METHOD BLANK SAMPLE NO.:
R4132130-3
Lab Sample ID:R4132130-3 SDG:L1784578
Lab File ID:1008_08 Preparation Date/Time:10/08/24 13:22
Instrument ID:VOCGC15 Analysis Date/Time:10/08/24 13:22
Analytical Batch:WG2377924 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4132130-1 VOCGC15 1008_04 10/08/24 11:43
LCSD R4132130-2 VOCGC15 1008_05 10/08/24 12:06
OS L1784370-04 VOCGC15 1008_21 10/08/24 19:13
S-10 (6-12)L1784578-11 VOCGC15 1008_26 10/08/24 21:11
S-14 (0-6)L1784578-12 VOCGC15 1008_27 10/08/24 21:35
S-11 (0-6)L1784578-13 VOCGC15 1008_28 10/08/24 21:58
S-14 (6-12)L1784578-15 VOCGC15 1008_29 10/08/24 22:21
MS R4132130-4 VOCGC15 1008_32 10/08/24 23:40
MSD R4132130-5 VOCGC15 1008_33 10/09/24 00:05
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4A-OR METHOD BLANK SAMPLE NO.:
R4130869-2
Lab Sample ID:R4130869-2 SDG:L1784578
Lab File ID:1008_06A Preparation Date/Time:10/08/24 10:10
Instrument ID:VOCGC17 Analysis Date/Time:10/08/24 10:10
Analytical Batch:WG2377829 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4130869-1 VOCGC17 1008_03A 10/08/24 09:11
S-13 (0-6)L1784578-01 VOCGC17 1008_21 10/08/24 15:59
S-15 (0-6)L1784578-02 VOCGC17 1008_22 10/08/24 16:18
S-32 (0-6)L1784578-03 VOCGC17 1008_23 10/08/24 16:38
S-12 (6-12)L1784578-04 VOCGC17 1008_24 10/08/24 16:57
S-12 (0-6)L1784578-05 VOCGC17 1008_25 10/08/24 17:17
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4A-OR METHOD BLANK SAMPLE NO.:
R4130871-3
Lab Sample ID:R4130871-3 SDG:L1784578
Lab File ID:1008_37 Preparation Date/Time:10/08/24 22:07
Instrument ID:VOCGC17 Analysis Date/Time:10/08/24 22:07
Analytical Batch:WG2378256 Dilution Factor:25
Analytical Method:8015D/GRO Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4130871-1 VOCGC17 1008_33 10/08/24 20:34
LCSD R4130871-2 VOCGC17 1008_34 10/08/24 21:09
S-10 (0-6)L1784578-06 VOCGC17 1008_50 10/09/24 02:36
MS R4130871-4 VOCGC17 1008_63 10/09/24 06:48
MSD R4130871-5 VOCGC17 1008_64 10/09/24 07:08
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC12 Calibration Start Date:05/23/24 00:27
Std File: 1009_02 Calibration End Date:05/23/24 03:10
Std Analysis Date:10/09/24 09:09
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 765355700 6.59 778243400 6.59
UPPER LIMIT 1530711000 1556487000
LOWER LIMIT 382677900 389121700
LCS R4131083-1
WG2378697 1x 1009_02U 765355700 6.59 778243400 6.59
LCSD R4131083-2
WG2378697 1x 1009_03 784882700 6.59 811526000 6.59
BLANK R4131083-3
WG2378697 1x 1009_05 709174900 6.59 709195600 6.59
L1784578-17 WG2378697
1x 1009_07 689283400 6.59 689255400 6.59
OS L1784965-03
WG2378697 1x 1009_17 718074000 6.59 718067200 6.59
MS R4131083-4
WG2378697 1x 1009_26 795510300 6.59 812626800 6.59
MSD R4131083-5
WG2378697 1x 1009_27 788118000 6.59 801641000 6.59
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC15 Calibration Start Date:06/26/24 14:42
Std File: 1008_03 Calibration End Date:06/26/24 19:34
Std Analysis Date:10/08/24 11:19
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 373773100 7.40 0 0
UPPER LIMIT 747546200 0
LOWER LIMIT 186886500 0
LCS R4132130-1
WG2377924 1x 1008_04 381275600 7.40 0 0
LCSD R4132130-2
WG2377924 1x 1008_05 370129100 7.40 0 0
BLANK R4132130-3
WG2377924 25x 1008_08 373091300 7.40 0 0
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC15 Calibration Start Date:06/26/24 14:42
Std File: 1008_17 Calibration End Date:06/26/24 19:34
Std Analysis Date:10/08/24 17:22
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 391436600 7.40 0 0
UPPER LIMIT 747546200 0
LOWER LIMIT 186886500 0
OS L1784370-04
WG2377924 28x 1008_21 349326900 7.40 0 0
L1784578-11 WG2377924
28x 1008_26 367879200 7.40 0 0
L1784578-12 WG2377924
27.5x 1008_27 370666400 7.40 0 0
L1784578-13 WG2377924
25x 1008_28 338733900 7.40 0 0
L1784578-15 WG2377924
27.5x 1008_29 342554800 7.40 0 0
MS R4132130-4
WG2377924 28x 1008_32 371474400 7.40 0 0
MSD R4132130-5
WG2377924 28x 1008_33 372221100 7.40 0 0
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC17 Calibration Start Date:08/28/24 16:05
Std File: 1008_02 Calibration End Date:08/28/24 18:02
Std Analysis Date:10/08/24 08:51
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 275185200 5.03 275185200 5.03
UPPER LIMIT 550370400 550370400
LOWER LIMIT 137592600 137592600
LCS R4130869-1
WG2377829 1x 1008_03A 248219900 5.03 248219900 5.03
BLANK R4130869-2
WG2377829 25x 1008_06A 241022800 5.03 241022800 5.03
L1784578-01 WG2377829
25x 1008_21 255043600 5.03 255043600 5.03
L1784578-02 WG2377829
27x 1008_22 245931100 5.03 245931100 5.03
L1784578-03 WG2377829
25x 1008_23 231725400 5.03 231725400 5.03
L1784578-04 WG2377829
25x 1008_24 254040800 5.03 254040800 5.03
L1784578-05 WG2377829
25x 1008_25 220302500 5.03 220302500 5.03
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC17 Calibration Start Date:08/28/24 16:05
Std File: 1008_32 Calibration End Date:08/28/24 18:02
Std Analysis Date:10/08/24 20:14
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 251091200 5.03 251091200 5.03
UPPER LIMIT 502182400 502182400
LOWER LIMIT 125545600 125545600
LCS R4130871-1
WG2378256 1x 1008_33 268932800 5.03 268932800 5.03
LCSD R4130871-2
WG2378256 1x 1008_34 266376200 5.03 266376200 5.03
BLANK R4130871-3
WG2378256 25x 1008_37 240324200 5.03 240324200 5.03
OS L1784578-06
WG2378256 34.5x 1008_50 204332600 5.03 204332600 5.03
L1784578-06 WG2378256
34.5x 1008_50 204332600 5.03 204332600 5.03
MS R4130871-4
WG2378256 34.5x 1008_63 268258800 5.03 268258800 5.03
MSD R4130871-5
WG2378256 34.5x 1008_64 268215200 5.03 268215200 5.03
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:1008_21 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/30/24 10:00
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 15:59
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.04 g
Total Solids (%):83.9 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 1.25 B J 0.762 3.51
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:1008_22 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/27/24 14:25
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 16:18
Dilution Factor:27 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.26 g
Total Solids (%):87.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 4.76 B 0.753 3.47
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:1008_23 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/30/24 10:10
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 16:38
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.73 g
Total Solids (%):83.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 1.18 B J 0.774 3.56
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:1008_24 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/27/24 16:05
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 16:57
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.63 g
Total Solids (%):85.5 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 2.02 B J 0.733 3.37
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:1008_25 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/27/24 15:50
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 17:17
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.56 g
Total Solids (%):90.4 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 1.50 B J 0.661 3.04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:1008_50 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2378256 Analysis Date/Time:10/09/24 02:36
Dilution Factor:34.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.23 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 4.59 B 0.836 3.85
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:1008_26 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:09/27/24 12:30
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 21:11
Dilution Factor:28 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.95 g
Total Solids (%):95.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 0.954 B J 0.659 3.04
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:1008_27 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:09/30/24 09:10
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 21:35
Dilution Factor:27.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.13 g
Total Solids (%):84.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 1.37 B J 0.804 3.70
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:1008_28 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:09/30/24 08:40
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 21:58
Dilution Factor:25 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.79 g
Total Solids (%):97.4 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 0.834 B J 0.574 2.64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:1008_29 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:09/30/24 09:20
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 22:21
Dilution Factor:27.5 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):86.3 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 1.12 B J 0.778 3.58
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:1009_07 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC12 Preparation Date/Time:10/09/24 12:31
Analytical Batch:WG2378697 Analysis Date/Time:10/09/24 12:31
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 U 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:05/23/24 00:27
Instrument ID:VOCGC12 Calibration (end) date/time:05/23/24 03:10
Analytical Method:8015D/GRO
Analyte CS: .05G CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G
TPH (GC/FID) LOW FRACTION 8 8 8 8 8 8 8
A,A,A-TRIFLUOROTOLUENE(FID)7.07 7.07 7.07 7.07 7.07 7.07 7.07
File ID:0522A_13 0522A_14 0522A_15 0522A_16 0522A_17 0522A_18 0522A_19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Analytical Method:8015D/GRO
Analyte CS: .05G CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G
TPH (GC/FID) LOW FRACTION 8 8 8 8 8 8 8
A,A,A-TRIFLUOROTOLUENE(FID)7.85 7.85 7.85 7.85 7.85 7.85 7.85
File ID:0626_05 0626_06 0626_07 0626_08 0626_09 0626_10 0626_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/28/24 16:05
Instrument ID:VOCGC17 Calibration (end) date/time:08/28/24 18:02
Analytical Method:8015D/GRO
Analyte CS: .05G CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G
TPH (GC/FID) LOW FRACTION 6 6 6 6 6 6 6
A,A,A-TRIFLUOROTOLUENE(FID)5.33 5.33 5.33 5.33 5.33 5.33 5.35
File ID:0828A_06 0828A_07 0828A_08 0828A_09 0828A_10 0828A_11 0828A_12
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:05/23/24 00:27
Instrument ID:VOCGC12 Calibration (end) date/time:05/23/24 03:10
Analytical Method:8015D/GRO
Analyte RRF: .05G RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G
TPH (GC/FID) LOW FRACTION 635.10 687.90 761.40 609.40 659.90 572 721.90
A,A,A-TRIFLUOROTOLUENE(FID)0.7220 0.7140 0.6890 0.6660 0.7190 0.7330 0.8290
File ID:0522A_13 0522A_14 0522A_15 0522A_16 0522A_17 0522A_18 0522A_19
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:05/23/24 00:27
Instrument ID:VOCGC12 Calibration (end) date/time:05/23/24 03:10
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 663.9457 9.86
A,A,A-TRIFLUOROTOLUENE(FID)0.724634 7.11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Analytical Method:8015D/GRO
Analyte RRF: .05G RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G
TPH (GC/FID) LOW FRACTION 896.70 868.5001 829.90 748.60 774.80 699.10 709.80
A,A,A-TRIFLUOROTOLUENE(FID)0.7190 0.7140 0.7140 0.70 0.7470 0.7620 0.8380
File ID:0626_05 0626_06 0626_07 0626_08 0626_09 0626_10 0626_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 789.6191 9.78
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 6.39
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/28/24 16:05
Instrument ID:VOCGC17 Calibration (end) date/time:08/28/24 18:02
Analytical Method:8015D/GRO
Analyte RRF: .05G RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G
TPH (GC/FID) LOW FRACTION 540.30 674.10 653.50 720.60 648.40 679.10 666.80
A,A,A-TRIFLUOROTOLUENE(FID)0.6440 0.6530 0.6150 0.67 0.6860 0.7120 0.7880
File ID:0828A_06 0828A_07 0828A_08 0828A_09 0828A_10 0828A_11 0828A_12
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/28/24 16:05
Instrument ID:VOCGC17 Calibration (end) date/time:08/28/24 18:02
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 654.6799 8.5
A,A,A-TRIFLUOROTOLUENE(FID)0.680968 8.27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:05/23/24 00:27
Instrument ID:VOCGC12 Calibration (end) date/time:05/23/24 03:10
Lab File ID:0522A_22 Analysis date/time:05/23/24 06:03
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 663.9457 0.61496350 99.90 5 4.631 92.60 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.724634 0.72166810 0.4090 0.20 0.1992 99.60 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:05/23/24 00:27
Instrument ID:VOCGC12 Calibration (end) date/time:05/23/24 03:10
Lab File ID:1009_02 Analysis date/time:10/09/24 09:09
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 663.9457 0.73733610 99.90 5 5.553 111 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.724634 0.75784930 4.58 0.20 0.2092 105 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Lab File ID:0626_14 Analysis date/time:06/26/24 22:05
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 789.6191 0.63304530 99.90 5 4.009 80.20 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 0.73361710 1.14 0.20 0.1977 98.80 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Lab File ID:1008_03 Analysis date/time:10/08/24 11:19
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 789.6191 0.71848860 99.90 5 4.550 91 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 0.78440670 5.71 0.20 0.2114 106 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 313 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:06/26/24 14:42
Instrument ID:VOCGC15 Calibration (end) date/time:06/26/24 19:34
Lab File ID:1008_17 Analysis date/time:10/08/24 17:22
Analytical Method:8015D/GRO Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 789.6191 0.78531170 99.90 5 4.973 99.50 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.742071 0.78485360 5.77 0.20 0.2115 106 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 314 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/28/24 16:05
Instrument ID:VOCGC17 Calibration (end) date/time:08/28/24 18:02
Lab File ID:0828A_15 Analysis date/time:08/28/24 19:00
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 654.6799 0.54542510 99.90 5 4.166 83.30 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.680968 0.677486 0.5110 0.20 0.1990 99.50 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 315 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/28/24 16:05
Instrument ID:VOCGC17 Calibration (end) date/time:08/28/24 18:02
Lab File ID:1008_02 Analysis date/time:10/08/24 08:51
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 654.6799 0.752996 99.90 5 5.751 115 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.680968 0.72834940 6.96 0.20 0.2139 107 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 316 of 526
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1784578 Calibration (begin) date/time:08/28/24 16:05
Instrument ID:VOCGC17 Calibration (end) date/time:08/28/24 18:02
Lab File ID:1008_32 Analysis date/time:10/08/24 20:14
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 654.6799 0.74645260 99.90 5 5.701 114 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.680968 0.73066120 7.30 0.20 0.2146 107 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC12 Calibration Start Date:05/23/24 00:27
Calibration End Date:05/23/24 03:10
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL .05G 0522A_13 05/23/24 00:27
CAL .1G 0522A_14 05/23/24 00:50
CAL .5G 0522A_15 05/23/24 01:12
CAL 1G 0522A_16 05/23/24 01:34
CAL 2.5G 0522A_17 05/23/24 01:56
CAL 5G 0522A_18 05/23/24 02:18
CAL 10G 0522A_19 05/23/24 03:10
SSCV VOCGC12052224A0522A_22726248 0522A_22 05/23/24 06:03
ICV VOCGC121009241009_02726248 1009_02 10/09/24 09:09
LCS R4131083-1 1009_02U 10/09/24 09:09 1 WG2378697
LCSD R4131083-2 1009_03 10/09/24 09:31 1 WG2378697
BLANK R4131083-3 1009_05 10/09/24 10:15 1 WG2378697
L1784443-14 L1784443-14 1009_06 10/09/24 12:09 1 WG2378697
EB-93024 L1784578-17 1009_07 10/09/24 12:31 1 WG2378697
L1784443-05 L1784443-05 1009_08 10/09/24 12:53 1 WG2378697
L1784443-06 L1784443-06 1009_09 10/09/24 13:15 1 WG2378697
L1784443-07 L1784443-07 1009_10 10/09/24 13:37 1 WG2378697
L1784443-08 L1784443-08 1009_11 10/09/24 14:00 1 WG2378697
L1784443-09 L1784443-09 1009_12 10/09/24 14:22 1 WG2378697
L1784443-10 L1784443-10 1009_13 10/09/24 14:44 1 WG2378697
L1784443-13 L1784443-13 1009_14 10/09/24 15:06 1 WG2378697
L1784965-01 L1784965-01 1009_15 10/09/24 15:27 1 WG2378697
L1784965-02 L1784965-02 1009_16 10/09/24 15:49 1 WG2378697
OS L1784965-03 1009_17 10/09/24 16:11
L1784965-03 L1784965-03 1009_17 10/09/24 16:11 1 WG2378697
L1784965-04 L1784965-04 1009_18 10/09/24 16:33 1 WG2378697
L1784965-06 L1784965-06 1009_19 10/09/24 16:55 1 WG2378697
L1784569-01 L1784569-01 1009_20 10/09/24 17:17 50 WG2378697
L1784569-03 L1784569-03 1009_21 10/09/24 17:39 25 WG2378697
L1784569-04 L1784569-04 1009_22 10/09/24 18:01 20 WG2378697
L1784571-01 L1784571-01 1009_23 10/09/24 18:23 50 WG2378697
L1784571-02 L1784571-02 1009_24 10/09/24 18:45 50 WG2378697
L1784571-03 L1784571-03 1009_25 10/09/24 19:07 100 WG2378697
MS R4131083-4 1009_26 10/09/24 19:28 1 WG2378697
MSD R4131083-5 1009_27 10/09/24 19:50 1 WG2378697
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 318 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC15 Calibration Start Date:06/26/24 14:42
Calibration End Date:06/26/24 19:34
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL .05G 0626_05 06/26/24 14:42
CAL .1G 0626_06 06/26/24 15:29
CAL .5G 0626_07 06/26/24 15:57
CAL 1G 0626_08 06/26/24 17:00
CAL 2.5G 0626_09 06/26/24 18:19
CAL 5G 0626_10 06/26/24 19:11
CAL 10G 0626_11 06/26/24 19:34
SSCV VOCGC150626240626_14734485 0626_14 06/26/24 22:05
ICV VOCGC151008241008_03734485 1008_03 10/08/24 11:19
LCS R4132130-1 1008_04 10/08/24 11:43 1 WG2377924
LCSD R4132130-2 1008_05 10/08/24 12:06 1 WG2377924
BLANK R4132130-3 1008_08 10/08/24 13:22 25 WG2377924
L1784539-01 L1784539-01 1008_09 10/08/24 13:56 25 WG2377924
L1784539-02 L1784539-02 1008_10 10/08/24 14:25 25 WG2377924
L1784539-03 L1784539-03 1008_11 10/08/24 14:49 25 WG2377924
L1784539-04 L1784539-04 1008_12 10/08/24 15:12 25 WG2377924
L1784539-05 L1784539-05 1008_13 10/08/24 15:38 25 WG2377924
L1784539-06 L1784539-06 1008_14 10/08/24 16:05 25 WG2377924
L1784539-07 L1784539-07 1008_15 10/08/24 16:31 25 WG2377924
CCV VOCGC151008241008_17734485 1008_17 10/08/24 17:22
L1784539-08 L1784539-08 1008_19 10/08/24 18:20 25 WG2377924
L1784539-09 L1784539-09 1008_20 10/08/24 18:48 25 WG2377924
OS L1784370-04 1008_21 10/08/24 19:13
S-10 (6-12)L1784578-11 1008_26 10/08/24 21:11 28 WG2377924
S-14 (0-6)L1784578-12 1008_27 10/08/24 21:35 27.5 WG2377924
S-11 (0-6)L1784578-13 1008_28 10/08/24 21:58 25 WG2377924
S-14 (6-12)L1784578-15 1008_29 10/08/24 22:21 27.5 WG2377924
MS R4132130-4 1008_32 10/08/24 23:40 28 WG2377924
MSD R4132130-5 1008_33 10/09/24 00:05 28 WG2377924
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC17 Calibration Start Date:08/28/24 16:05
Calibration End Date:08/28/24 18:02
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL .05G 0828A_06 08/28/24 16:05
CAL .1G 0828A_07 08/28/24 16:25
CAL .5G 0828A_08 08/28/24 16:44
CAL 1G 0828A_09 08/28/24 17:03
CAL 2.5G 0828A_10 08/28/24 17:23
CAL 5G 0828A_11 08/28/24 17:42
CAL 10G 0828A_12 08/28/24 18:02
SSCV VOCGC17082824A0828A_15749168 0828A_15 08/28/24 19:00
ICV VOCGC171008241008_02749168 1008_02 10/08/24 08:51
LCS R4129909-1 1008_03 10/08/24 09:11 1 WG2377797
LCS R4130869-1 1008_03A 10/08/24 09:11 1 WG2377829
BLANK R4129909-2 1008_06 10/08/24 10:10 25 WG2377797
BLANK R4130869-2 1008_06A 10/08/24 10:10 25 WG2377829
L1784789-05 L1784789-05 1008_07 10/08/24 11:27 25 WG2377797
L1784789-06 L1784789-06 1008_08 10/08/24 11:47 25 WG2377797
L1784482-01 L1784482-01 1008_14 10/08/24 13:43 25 WG2377829
L1784482-02 L1784482-02 1008_15 10/08/24 14:03 25.8 WG2377829
L1784482-03 L1784482-03 1008_16 10/08/24 14:22 25 WG2377829
L1784482-04 L1784482-04 1008_17 10/08/24 14:42 25 WG2377829
L1784482-05 L1784482-05 1008_18 10/08/24 15:01 25 WG2377829
L1784482-06 L1784482-06 1008_19 10/08/24 15:20 28 WG2377829
L1784525-01 L1784525-01 1008_20 10/08/24 15:40 25 WG2377829
S-13 (0-6)L1784578-01 1008_21 10/08/24 15:59 25 WG2377829
S-15 (0-6)L1784578-02 1008_22 10/08/24 16:18 27 WG2377829
S-32 (0-6)L1784578-03 1008_23 10/08/24 16:38 25 WG2377829
S-12 (6-12)L1784578-04 1008_24 10/08/24 16:57 25 WG2377829
S-12 (0-6)L1784578-05 1008_25 10/08/24 17:17 25 WG2377829
L1784395-04 L1784395-04 1008_26 10/08/24 17:36 250 WG2377829
ICV VOCGC171008241008_32749168 1008_32 10/08/24 20:14
LCS R4130870-1 1008_33A 10/08/24 20:34 1 WG2378065
LCS R4130871-1 1008_33 10/08/24 20:34 1 WG2378256
LCSD R4130870-2 1008_34A 10/08/24 21:09 1 WG2378065
LCSD R4130871-2 1008_34 10/08/24 21:09 1 WG2378256
BLANK R4130870-3 1008_37A 10/08/24 22:07 25 WG2378065
BLANK R4130871-3 1008_37 10/08/24 22:07 25 WG2378256
L1781808-09 L1781808-09 1008_38 10/08/24 22:42 31 WG2378256
L1784113-05 L1784113-05 1008_39 10/08/24 23:02 25 WG2378256
L1784113-03 L1784113-03 1008_40 10/08/24 23:21 2040 WG2378065
L1784113-04 L1784113-04 1008_41 10/08/24 23:41 253 WG2378065
OS L1784367-01 1008_43 10/09/24 00:20
L1784374-01 L1784374-01 1008_44 10/09/24 00:39 25 WG2378065
L1784395-02 L1784395-02 1008_45 10/09/24 00:59 100 WG2378065
MS R4130870-4 1008_46 10/09/24 01:18 34 WG2378065
MSD R4130870-5 1008_47 10/09/24 01:38 34 WG2378065
S-10 (0-6)L1784578-06 1008_50 10/09/24 02:36 34.5 WG2378256
L1784968-01 L1784968-01 1008_51 10/09/24 02:55 25 WG2378256
L1784968-02 L1784968-02 1008_52 10/09/24 03:14 29.8 WG2378256
L1784968-03 L1784968-03 1008_53 10/09/24 03:34 25 WG2378256
L1784968-04 L1784968-04 1008_54 10/09/24 03:53 25 WG2378256
L1784968-05 L1784968-05 1008_55 10/09/24 04:13 25 WG2378256
L1784968-07 L1784968-07 1008_56 10/09/24 04:32 25 WG2378256
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 320 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8015D/GRO
Instrument ID:VOCGC17 Calibration Start Date:08/28/24 16:05
Calibration End Date:08/28/24 18:02
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
L1784968-08 L1784968-08 1008_57 10/09/24 04:51 25 WG2378256
L1784968-09 L1784968-09 1008_58 10/09/24 05:11 25 WG2378256
L1784968-10 L1784968-10 1008_59 10/09/24 05:30 26 WG2378256
L1784968-11 L1784968-11 1008_60 10/09/24 05:50 25.8 WG2378256
L1784968-12 L1784968-12 1008_61 10/09/24 06:09 25 WG2378256
L1784968-13 L1784968-13 1008_62 10/09/24 06:29 27.3 WG2378256
MS R4130871-4 1008_63 10/09/24 06:48 34.5 WG2378256
MSD R4130871-5 1008_64 10/09/24 07:08 34.5 WG2378256
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 321 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17 Analytical Method:8015D/GRO
Matrix:GW Prep Method:8015D/GRO
Analyte CAS MDL RDL
mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 0.0314 0.10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 322 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,11,12,13,15 Analytical Method:8015D/GRO
Matrix:Solid Prep Method:8015D/GRO
Analyte CAS MDL RDL
mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 0.0217 0.10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 323 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130869-2
Lab Sample ID:R4130869-2 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1008_06A Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:10/08/24 10:10
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 10:10
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 0.675 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 324 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130871-3
Lab Sample ID:R4130871-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1008_37 Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:10/08/24 22:07
Analytical Batch:WG2378256 Analysis Date/Time:10/08/24 22:07
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 0.800 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 325 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131083-3
Lab Sample ID:R4131083-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1009_05 Received Date/Time:_______________
Instrument ID:VOCGC12 Preparation Date/Time:10/09/24 10:15
Analytical Batch:WG2378697 Analysis Date/Time:10/09/24 10:15
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 U 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 326 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132130-3
Lab Sample ID:R4132130-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1008_08 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:10/08/24 13:22
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 13:22
Dilution Factor:25 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 0.846 J 0.543 2.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 327 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130869-1
Lab Sample ID:R4130869-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1008_03A Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:10/08/24 09:11
Analytical Batch:WG2377829 Analysis Date/Time:10/08/24 09:11
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 5.72 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 328 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130871-1
Lab Sample ID:R4130871-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1008_33 Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:10/08/24 20:34
Analytical Batch:WG2378256 Analysis Date/Time:10/08/24 20:34
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 5.58 0.0217 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 329 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131083-1
Lab Sample ID:R4131083-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1009_02U Received Date/Time:_______________
Instrument ID:VOCGC12 Preparation Date/Time:10/09/24 09:09
Analytical Batch:WG2378697 Analysis Date/Time:10/09/24 09:09
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 5.55 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 330 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132130-1
Lab Sample ID:R4132130-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1008_04 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:10/08/24 11:43
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 11:43
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 4.64 0.0217 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130871-2
Lab Sample ID:R4130871-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1008_34 Received Date/Time:_______________
Instrument ID:VOCGC17 Preparation Date/Time:10/08/24 21:09
Analytical Batch:WG2378256 Analysis Date/Time:10/08/24 21:09
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 5.87 0.0217 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131083-2
Lab Sample ID:R4131083-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1009_03 Received Date/Time:_______________
Instrument ID:VOCGC12 Preparation Date/Time:10/09/24 09:31
Analytical Batch:WG2378697 Analysis Date/Time:10/09/24 09:31
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 5.36 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132130-2
Lab Sample ID:R4132130-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1008_05 Received Date/Time:_______________
Instrument ID:VOCGC15 Preparation Date/Time:10/08/24 12:06
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 12:06
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 5.37 0.0217 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130871-4
Lab Sample ID:R4130871-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:1008_63 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2378256 Analysis Date/Time:10/09/24 06:48
Dilution Factor:34.5 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.23 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 228 0.836 3.85
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131083-4
Lab Sample ID:R4131083-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:10/01/24 16:28
Lab File ID:1009_26 Received Date/Time:10/03/24 09:00
Instrument ID:VOCGC12 Preparation Date/Time:10/09/24 19:28
Analytical Batch:WG2378697 Analysis Date/Time:10/09/24 19:28
Dilution Factor:1 Prep Method:8015/NWTPHGX
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 5.89 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132130-4
Lab Sample ID:R4132130-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:10/01/24 12:10
Lab File ID:1008_32 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:10/01/24 12:10
Analytical Batch:WG2377924 Analysis Date/Time:10/08/24 23:40
Dilution Factor:28 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.94 g
Total Solids (%):_______________Final Wt/Vol:10 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 131 0.608 2.80
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4130871-5
Lab Sample ID:R4130871-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:1008_64 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC17 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2378256 Analysis Date/Time:10/09/24 07:08
Dilution Factor:34.5 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:7.23 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 6 231 0.836 3.85
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131083-5
Lab Sample ID:R4131083-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:10/01/24 16:28
Lab File ID:1009_27 Received Date/Time:10/03/24 09:00
Instrument ID:VOCGC12 Preparation Date/Time:10/09/24 19:50
Analytical Batch:WG2378697 Analysis Date/Time:10/09/24 19:50
Dilution Factor:1 Prep Method:8015/NWTPHGX
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 8 6.51 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132130-5
Lab Sample ID:R4132130-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:10/01/24 12:10
Lab File ID:1008_33 Received Date/Time:10/02/24 09:00
Instrument ID:VOCGC15 Preparation Date/Time:10/01/24 12:10
Analytical Batch:WG2377924 Analysis Date/Time:10/09/24 00:05
Dilution Factor:28 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.94 g
Total Solids (%):_______________Final Wt/Vol:10 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 8006-61-9 8 131 0.608 2.80
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8260B Volatile Organic Compounds (GC/MS)
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2A-OR SURROGATE RECOVERY
Analytical Method:8260B SDG:L1784578
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 DMC-2 DMC-3 TOT Out
% Rec.% Rec.% Rec.
EB-93024 L1784578-17 VOCMS16 1010_38 96.3 98.3 104 0
TRIP BLANK L1784578-18 VOCMS36 1010_10 102 92.0 102 0
TRIP BLANK L1784578-18 VOCMS42 1015_06 96.0 101 111 0
BLANK R4131396-3 VOCMS16 1010_34A 95.1 98.1 99.7 0
BLANK R4132481-3 VOCMS36 1010_08A 105 95.1 107 0
BLANK R4133124-3 VOCMS42 1015_05A 98.6 99.4 110 0
LCS R4131396-1 VOCMS16 1010_31LCSA 96.6 107 105 0
LCS R4132481-1 VOCMS36 1010_02LCSA 101 92.7 108 0
LCS R4133124-1 VOCMS42 1015_02LCSA 102 107 106 0
LCSD R4132481-2 VOCMS36 1010_03A 100 93.3 105 0
LCSD R4133124-2 VOCMS42 1015_03A 102 110 105 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 Toluene-d8 80.0 - 120
DMC-2 4-Bromofluorobenzene 77.0 - 126
DMC-3 1,2-Dichloroethane-d4 70.0 - 130
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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2A-OR SURROGATE RECOVERY
Analytical Method:8260B SDG:L1784578
Matrix:Solid
Sample ID Lab Sample ID Instrument File ID DMC-1 DMC-2 DMC-3 TOT Out
% Rec.% Rec.% Rec.
S-13 (0-6)L1784578-01 VOCMS56 1011a_16 120 95.9 93.3 0
S-15 (0-6)L1784578-02 VOCMS59 1011_19 102 96.4 98.5 0
S-32 (0-6)L1784578-03 VOCMS56 1011a_17 121 91.9 91.4 0
S-12 (6-12)L1784578-04 VOCMS59 1011_20 97.6 96.5 100 0
S-12 (0-6)L1784578-05 VOCMS59 1011_21 99.3 99.2 101 0
S-10 (0-6)L1784578-06 VOCMS59 1011_22 99.5 92.6 96.3 0
S-10 (6-12)L1784578-11 VOCMS59 1011_23 99.5 98.5 103 0
S-14 (0-6)L1784578-12 VOCMS56 1011a_18 122 92.6 92.5 0
S-11 (0-6)L1784578-13 VOCMS56 1011a_19 122 90.3 92.8 0
S-14 (6-12)L1784578-15 VOCMS56 1011a_20 119 93.6 91.8 0
OS L1784968-27 VOCMS56 1011a_30 113 105 94.1 0
MS R4131341-4 VOCMS59 1011_28 99.9 92.0 100 0
MSD R4131341-5 VOCMS59 1011_29 101 95.8 95.1 0
MS R4132125-3 VOCMS56 1011a_31 114 102 96.8 0
MSD R4132125-4 VOCMS56 1011a_32 116 104 94.7 0
BLANK R4132125-2 VOCMS56 1011a_06 119 92.0 94.5 0
BLANK R4131341-3 VOCMS59 1011_07 102 98.0 98.9 0
LCS R4132125-1 VOCMS56 1011a_03LCS 113 96.1 97.4 0
LCS R4131341-1 VOCMS59 1011_02LCS 96.5 97.0 108 0
LCSD R4131341-2 VOCMS59 1011_03 97.9 98.1 110 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 Toluene-d8 75.0 - 131
DMC-2 4-Bromofluorobenzene 67.0 - 138
DMC-3 1,2-Dichloroethane-d4 70.0 - 130
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131341-4
L1784578-02,04,05,06,11 R4131341-5
MS Sample / File ID:R4131341-4 / 1011_28 SDG:L1784578
MSD Sample / File ID:R4131341-5 / 1011_29 Analytical Batch:WG2379147
OS Sample / File ID:L1784578-06 / 1011_22 Matrix:Solid
Instrument ID:VOCMS59
Analytical Method:8260B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.795 U 0.391 0.373 49.2 47.0 1.13 10.0 - 160 4.72 40
Acrylonitrile 0.795 U 0.615 0.607 77.3 76.3 1.13 10.0 - 160 1.29 40
Benzene 0.159 0.0350 0.144 0.176 68.8 88.7 1.13 10.0 - 149 19.7 37
Bromobenzene 0.159 U 0.145 0.170 91.5 107 1.13 10.0 - 156 15.7 38
Bromodichloromethane 0.159 U 0.141 0.160 88.7 101 1.13 10.0 - 143 12.7 37
Bromoform 0.159 U 0.139 0.144 87.2 90.8 1.13 10.0 - 146 3.98 36
Bromomethane 0.159 U 0.0747 0.0832 47.0 52.3 1.13 10.0 - 149 10.9 38
n-Butylbenzene 0.159 U 0.147 0.183 92.2 115 1.13 10.0 - 160 21.9 40
sec-Butylbenzene 0.159 U 0.157 0.196 98.6 123 1.13 10.0 - 159 22.4 39
tert-Butylbenzene 0.159 U 0.149 0.214 93.6 135 1.13 10.0 - 156 36.0 39
Carbon tetrachloride 0.159 U 0.143 0.184 90.1 116 1.13 10.0 - 145 24.8 37
Chlorobenzene 0.159 U 0.135 0.167 85.1 105 1.13 10.0 - 152 20.9 39
Chlorodibromomethane 0.159 U 0.139 0.156 87.2 97.9 1.13 10.0 - 146 11.5 37
Chloroethane 0.159 U 0.0394 0.0449 24.8 28.2 1.13 10.0 - 146 13.1 40
Chloroform 0.159 U 0.136 0.167 85.8 105 1.13 10.0 - 146 20.1 37
Chloromethane 0.159 U 0.110 0.143 69.0 90.1 1.13 10.0 - 159 26.5 37
2-Chlorotoluene 0.159 U 0.147 0.176 92.2 111 1.13 10.0 - 159 18.2 38
4-Chlorotoluene 0.159 U 0.151 0.178 95.0 112 1.13 10.0 - 155 16.4 39
1,2-Dibromo-3-Chloropropane 0.159 U 0.121 0.125 75.9 78.7 1.13 10.0 - 151 3.67 39
1,2-Dibromoethane 0.159 U 0.144 0.151 90.8 95.0 1.13 10.0 - 148 4.58 34
Dibromomethane 0.159 U 0.144 0.160 90.8 101 1.13 10.0 - 147 10.4 35
1,2-Dichlorobenzene 0.159 U 0.140 0.161 87.9 101 1.13 10.0 - 155 14.2 37
1,3-Dichlorobenzene 0.159 U 0.145 0.166 91.5 104 1.13 10.0 - 153 13.0 38
1,4-Dichlorobenzene 0.159 U 0.144 0.164 90.8 103 1.13 10.0 - 151 12.5 38
Dichlorodifluoromethane 0.159 U 0.114 0.156 71.6 97.9 1.13 10.0 - 160 31.0 35
1,1-Dichloroethane 0.159 0.0106 0.147 0.171 85.5 101 1.13 10.0 - 147 15.6 37
1,2-Dichloroethane 0.159 U 0.147 0.160 92.2 101 1.13 10.0 - 148 8.82 35
1,1-Dichloroethene 0.159 U 0.143 0.192 90.1 121 1.13 10.0 - 155 29.0 37
cis-1,2-Dichloroethene 0.159 0.165 0.307 0.324 89.4 100 1.13 10.0 - 149 5.37 37
trans-1,2-Dichloroethene 0.159 0.00733 0.126 0.162 74.8 97.5 1.13 10.0 - 150 25.0 37
1,2-Dichloropropane 0.159 U 0.144 0.165 90.8 104 1.13 10.0 - 148 13.1 37
1,1-Dichloropropene 0.159 U 0.141 0.184 88.7 116 1.13 10.0 - 153 26.4 35
1,3-Dichloropropane 0.159 U 0.157 0.171 98.6 108 1.13 10.0 - 154 8.93 35
cis-1,3-Dichloropropene 0.159 U 0.142 0.165 89.4 104 1.13 10.0 - 151 14.7 37
trans-1,3-Dichloropropene 0.159 U 0.149 0.170 93.6 107 1.13 10.0 - 148 13.4 37
2,2-Dichloropropane 0.159 U 0.107 0.142 67.5 89.4 1.13 10.0 - 138 27.8 36
Di-isopropyl ether 0.159 U 0.142 0.160 89.4 101 1.13 10.0 - 147 11.9 36
Ethylbenzene 0.159 0.00988 0.135 0.169 78.9 100 1.13 10.0 - 160 22.2 38
Hexachloro-1,3-butadiene 0.159 U 0.156 0.188 97.9 118 1.13 10.0 - 160 19.0 40
Isopropylbenzene 0.159 0.00277 0.132 0.170 81.2 105 1.13 10.0 - 155 25.4 38
p-Isopropyltoluene 0.159 0.0132 0.157 0.192 90.3 112 1.13 10.0 - 160 20.1 40
2-Butanone (MEK)0.795 U 0.710 0.697 89.4 87.7 1.13 10.0 - 160 1.92 40
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131341-4
L1784578-02,04,05,06,11 R4131341-5
MS Sample / File ID:R4131341-4 / 1011_28 SDG:L1784578
MSD Sample / File ID:R4131341-5 / 1011_29 Analytical Batch:WG2379147
OS Sample / File ID:L1784578-06 / 1011_22 Matrix:Solid
Instrument ID:VOCMS59
Analytical Method:8260B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
Methylene Chloride 0.159 0.0134 0.135 0.159 76.7 91.6 1.13 10.0 - 141 16.1 37
4-Methyl-2-pentanone (MIBK)0.795 0.0133 0.743 0.744 91.8 91.9 1.13 10.0 - 160 0.152 35
Methyl tert-butyl ether 0.159 U 0.142 0.147 89.4 92.2 1.13 11.0 - 147 3.12 35
Naphthalene 0.159 0.0451 0.156 0.167 69.5 76.6 1.13 10.0 - 160 6.99 36
n-Propylbenzene 0.159 0.00293 0.149 0.188 91.8 117 1.13 10.0 - 158 23.4 38
Styrene 0.159 U 0.127 0.157 80.1 98.6 1.13 10.0 - 160 20.6 40
1,1,1,2-Tetrachloroethane 0.159 U 0.126 0.148 79.4 92.9 1.13 10.0 - 149 15.6 39
1,1,2,2-Tetrachloroethane 0.159 U 0.0704 0.0743 44.3 46.7 1.13 10.0 - 160 5.46 35
1,1,2-Trichlorotrifluoroethane 0.159 U 0.160 0.224 101 141 1.13 10.0 - 160 33.4 36
Tetrachloroethene 0.159 0.0461 0.192 0.231 91.6 116 1.13 10.0 - 156 18.7 39
Toluene 0.159 0.169 0.171 0.209 1.42*24.8 1.13 10.0 - 156 19.6 38
1,2,3-Trichlorobenzene 0.159 U 0.131 0.151 82.3 95.0 1.13 10.0 - 160 14.4 40
1,2,4-Trichlorobenzene 0.159 U 0.131 0.151 82.3 95.0 1.13 10.0 - 160 14.4 40
1,1,1-Trichloroethane 0.159 0.00564 0.135 0.177 81.6 108 1.13 10.0 - 144 26.7 35
1,1,2-Trichloroethane 0.159 U 0.150 0.158 94.3 99.3 1.13 10.0 - 160 5.13 35
Trichloroethene 0.159 0.0625 0.267 0.309 129 155 1.13 10.0 - 156 14.5 38
Trichlorofluoromethane 0.159 U 0.0559 0.0803 35.2 50.5 1.13 10.0 - 160 35.8 40
1,2,3-Trichloropropane 0.159 U 0.154 0.157 97.2 98.6 1.13 10.0 - 156 1.45 35
1,2,4-Trimethylbenzene 0.159 0.0529 0.175 0.202 76.7 93.7 1.13 10.0 - 160 14.4 36
1,2,3-Trimethylbenzene 0.159 0.0379 0.166 0.189 80.4 95.3 1.13 10.0 - 160 13.3 36
1,3,5-Trimethylbenzene 0.159 0.0132 0.161 0.195 93.1 114 1.13 10.0 - 160 19.0 38
Vinyl chloride 0.159 U 0.108 0.145 68.2 91.5 1.13 10.0 - 160 29.2 37
Xylenes, Total 0.477 0.142 0.445 0.547 63.6 84.9 1.13 10.0 - 160 20.5 38
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4132125-3
L1784578-01,03,12,13,15 R4132125-4
MS Sample / File ID:R4132125-3 / 1011a_31 SDG:L1784578
MSD Sample / File ID:R4132125-4 / 1011a_32 Analytical Batch:WG2380545
OS Sample / File ID:L1784968-27 / 1011a_30 Matrix:Solid
Instrument ID:VOCMS56
Analytical Method:8260B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 14.8 U 13.9 11.5 94.2 77.9 20 10.0 - 160 18.9 40
Acrylonitrile 14.8 U 13.7 13.5 92.6 91.7 20 10.0 - 160 0.897 40
Benzene 2.97 0.0480 2.78 1.49 92.2 48.6 20 10.0 - 149 60.6*37
Bromobenzene 2.97 U 3.86 2.45 130 82.7 20 10.0 - 156 44.5*38
Bromodichloromethane 2.97 U 2.84 1.87 95.9 63.0 20 10.0 - 143 41.5*37
Bromoform 2.97 U 3.54 3.12 119 105 20 10.0 - 146 12.5 36
Bromomethane 2.97 U 2.20 1.16 74.1 39.3 20 10.0 - 149 61.4*38
n-Butylbenzene 2.97 U 6.66 2.72 225*91.8 20 10.0 - 160 84.0*40
sec-Butylbenzene 2.97 0.668 5.05 3.12 148 82.8 20 10.0 - 159 47.2*39
tert-Butylbenzene 2.97 U 4.16 7.95 140 268*20 10.0 - 156 62.5*39
Carbon tetrachloride 2.97 U 2.84 1.27 95.9 42.8 20 10.0 - 145 76.6*37
Chlorobenzene 2.97 U 3.47 2.10 117 70.8 20 10.0 - 152 49.1*39
Chlorodibromomethane 2.97 U 3.65 2.64 123 88.9 20 10.0 - 146 32.2 37
Chloroethane 2.97 U 2.50 1.21 84.4 40.8 20 10.0 - 146 69.6*40
Chloroform 2.97 U 2.71 1.55 91.4 52.3 20 10.0 - 146 54.4*37
Chloromethane 2.97 U 2.27 1.05 76.5 35.6 20 10.0 - 159 73.1*37
2-Chlorotoluene 2.97 U 3.91 1.70 132 57.2 20 10.0 - 159 78.9*38
4-Chlorotoluene 2.97 U U 2.27 0.000*76.5 20 10.0 - 155 200*39
1,2-Dibromo-3-Chloropropane 2.97 U 3.95 4.06 133 137 20 10.0 - 151 2.74 39
1,2-Dibromoethane 2.97 U 3.64 3.08 123 104 20 10.0 - 148 16.7 34
Dibromomethane 2.97 U 2.84 2.28 95.9 77.0 20 10.0 - 147 21.9 35
1,2-Dichlorobenzene 2.97 U 3.95 2.69 133 90.5 20 10.0 - 155 38.2*37
1,3-Dichlorobenzene 2.97 U 3.92 2.45 132 82.7 20 10.0 - 153 46.0*38
1,4-Dichlorobenzene 2.97 U 3.83 2.42 129 81.5 20 10.0 - 151 45.3*38
Dichlorodifluoromethane 2.97 U 3.04 1.28 102 43.2 20 10.0 - 160 81.4*35
1,1-Dichloroethane 2.97 U 2.87 1.50 96.7 50.6 20 10.0 - 147 62.6*37
1,2-Dichloroethane 2.97 U 2.72 1.94 91.8 65.4 20 10.0 - 148 33.5 35
1,1-Dichloroethene 2.97 U 2.82 1.21 95.1 40.8 20 10.0 - 155 79.9*37
cis-1,2-Dichloroethene 2.97 U 2.83 1.64 95.5 55.1 20 10.0 - 149 53.6*37
trans-1,2-Dichloroethene 2.97 U 2.75 1.34 92.6 45.3 20 10.0 - 150 68.7*37
1,2-Dichloropropane 2.97 U 2.86 1.71 96.3 57.6 20 10.0 - 148 50.3*37
1,1-Dichloropropene 2.97 U 2.65 1.21 89.3 40.8 20 10.0 - 153 74.6*35
1,3-Dichloropropane 2.97 U 3.52 2.82 119 95.1 20 10.0 - 154 22.0 35
cis-1,3-Dichloropropene 2.97 U 3.20 2.16 108 72.8 20 10.0 - 151 38.7*37
trans-1,3-Dichloropropene 2.97 U 3.73 2.86 126 96.3 20 10.0 - 148 26.7 37
2,2-Dichloropropane 2.97 U 2.80 1.39 94.2 46.9 20 10.0 - 138 67.1*36
Di-isopropyl ether 2.97 U 2.95 2.00 99.6 67.5 20 10.0 - 147 38.4*36
Ethylbenzene 2.97 2.84 6.22 4.69 114 62.1 20 10.0 - 160 28.2 38
Hexachloro-1,3-butadiene 2.97 U 4.60 2.90 155 97.9 20 10.0 - 160 45.2*40
Isopropylbenzene 2.97 0.508 4.37 2.53 130 68.1 20 10.0 - 155 53.5*38
p-Isopropyltoluene 2.97 1.73 5.74 3.86 135 71.6 20 10.0 - 160 39.2 40
2-Butanone (MEK)14.8 U 13.1 11.1 88.4 75.4 20 10.0 - 160 15.9 40
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4132125-3
L1784578-01,03,12,13,15 R4132125-4
MS Sample / File ID:R4132125-3 / 1011a_31 SDG:L1784578
MSD Sample / File ID:R4132125-4 / 1011a_32 Analytical Batch:WG2380545
OS Sample / File ID:L1784968-27 / 1011a_30 Matrix:Solid
Instrument ID:VOCMS56
Analytical Method:8260B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg mg/kg %%%%%
Methylene Chloride 2.97 U 2.80 1.84 94.2 62.1 20 10.0 - 141 41.1*37
4-Methyl-2-pentanone (MIBK)14.8 U 20.1 20.1 136 136 20 10.0 - 160 0.000 35
Methyl tert-butyl ether 2.97 U 3.03 2.43 102 81.9 20 11.0 - 147 21.9 35
Naphthalene 2.97 13.1 17.9 17.7 165*156 20 10.0 - 160 1.37 36
n-Propylbenzene 2.97 2.29 6.38 4.09 138 60.5 20 10.0 - 158 43.8*38
Styrene 2.97 U 3.65 2.33 123 78.6 20 10.0 - 160 44.1*40
1,1,1,2-Tetrachloroethane 2.97 U 3.42 2.22 115 74.9 20 10.0 - 149 42.4*39
1,1,2,2-Tetrachloroethane 2.97 U 3.86 3.43 130 116 20 10.0 - 160 11.7 35
1,1,2-Trichlorotrifluoroethane 2.97 U 2.86 1.12 96.3 37.7 20 10.0 - 160 87.6*36
Tetrachloroethene 2.97 U 3.41 1.65 115 55.6 20 10.0 - 156 69.6*39
Toluene 2.97 U 3.43 1.84 116 62.1 20 10.0 - 156 60.2*38
1,2,3-Trichlorobenzene 2.97 U 5.04 3.86 170*130 20 10.0 - 160 26.6 40
1,2,4-Trichlorobenzene 2.97 U 4.94 3.82 167*129 20 10.0 - 160 25.6 40
1,1,1-Trichloroethane 2.97 U 2.76 1.31 93.0 44.0 20 10.0 - 144 71.5*35
1,1,2-Trichloroethane 2.97 U 3.88 3.23 131 109 20 10.0 - 160 18.2 35
Trichloroethene 2.97 U 2.95 1.40 99.6 47.3 20 10.0 - 156 71.1*38
Trichlorofluoromethane 2.97 U 0.965 0.701 32.6 23.6 20 10.0 - 160 31.8 40
1,2,3-Trichloropropane 2.97 U 3.59 3.21 121 108 20 10.0 - 156 11.1 35
1,2,4-Trimethylbenzene 2.97 51.9 58.3 53.9 218*70.0 20 10.0 - 160 7.83 36
1,2,3-Trimethylbenzene 2.97 13.1 17.7 10.8 156 0.000*20 10.0 - 160 48.8*36
1,3,5-Trimethylbenzene 2.97 1.70 5.47 3.78 127 70.4 20 10.0 - 160 36.4 38
Vinyl chloride 2.97 U 2.53 1.16 85.2 39.1 20 10.0 - 160 74.3*37
Xylenes, Total 8.89 9.21 20.6 15.3 128 68.0 20 10.0 - 160 29.9 38
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131341-1
RECOVERY R4131341-2
L1784578-02,04,05,06,11
LCS Sample / File ID:R4131341-1 / 1011_02LCS SDG:L1784578
LCSD Sample / File ID:R4131341-2 / 1011_03 Analytical Batch:WG2379147
Instrument ID:VOCMS59 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.736 0.634 118 101 10.0 - 160 14.9 31
Acrylonitrile 0.625 0.710 0.665 114 106 45.0 - 153 6.55 22
Benzene 0.125 0.127 0.131 102 105 70.0 - 123 3.10 20
Bromobenzene 0.125 0.123 0.117 98.4 93.6 73.0 - 121 5.00 20
Bromodichloromethane 0.125 0.125 0.127 100 102 73.0 - 121 1.59 20
Bromoform 0.125 0.128 0.127 102 102 64.0 - 132 0.784 20
Bromomethane 0.125 0.157 0.160 126 128 56.0 - 147 1.89 20
n-Butylbenzene 0.125 0.136 0.128 109 102 68.0 - 135 6.06 20
sec-Butylbenzene 0.125 0.134 0.128 107 102 74.0 - 130 4.58 20
tert-Butylbenzene 0.125 0.120 0.119 96.0 95.2 75.0 - 127 0.837 20
Carbon tetrachloride 0.125 0.150 0.147 120 118 66.0 - 128 2.02 20
Chlorobenzene 0.125 0.118 0.118 94.4 94.4 76.0 - 128 0.000 20
Chlorodibromomethane 0.125 0.124 0.118 99.2 94.4 74.0 - 127 4.96 20
Chloroethane 0.125 0.167 0.171 134 137*61.0 - 134 2.37 20
Chloroform 0.125 0.145 0.142 116 114 72.0 - 123 2.09 20
Chloromethane 0.125 0.143 0.143 114 114 51.0 - 138 0.000 20
2-Chlorotoluene 0.125 0.127 0.121 102 96.8 75.0 - 124 4.84 20
4-Chlorotoluene 0.125 0.128 0.121 102 96.8 75.0 - 124 5.62 20
1,2-Dibromo-3-Chloropropane 0.125 0.124 0.119 99.2 95.2 59.0 - 130 4.12 20
1,2-Dibromoethane 0.125 0.117 0.116 93.6 92.8 74.0 - 128 0.858 20
Dibromomethane 0.125 0.136 0.131 109 105 75.0 - 122 3.75 20
1,2-Dichlorobenzene 0.125 0.125 0.121 100 96.8 76.0 - 124 3.25 20
1,3-Dichlorobenzene 0.125 0.130 0.124 104 99.2 76.0 - 125 4.72 20
1,4-Dichlorobenzene 0.125 0.125 0.119 100 95.2 77.0 - 121 4.92 20
Dichlorodifluoromethane 0.125 0.146 0.141 117 113 43.0 - 156 3.48 20
1,1-Dichloroethane 0.125 0.143 0.138 114 110 70.0 - 127 3.56 20
1,2-Dichloroethane 0.125 0.136 0.137 109 110 65.0 - 131 0.733 20
1,1-Dichloroethene 0.125 0.168 0.162 134*130 65.0 - 131 3.64 20
cis-1,2-Dichloroethene 0.125 0.143 0.139 114 111 73.0 - 125 2.84 20
trans-1,2-Dichloroethene 0.125 0.137 0.136 110 109 71.0 - 125 0.733 20
1,2-Dichloropropane 0.125 0.123 0.128 98.4 102 74.0 - 125 3.98 20
1,1-Dichloropropene 0.125 0.139 0.140 111 112 73.0 - 125 0.717 20
1,3-Dichloropropane 0.125 0.126 0.119 101 95.2 80.0 - 125 5.71 20
cis-1,3-Dichloropropene 0.125 0.127 0.125 102 100 76.0 - 127 1.59 20
trans-1,3-Dichloropropene 0.125 0.122 0.121 97.6 96.8 73.0 - 127 0.823 20
2,2-Dichloropropane 0.125 0.166 0.166 133 133 59.0 - 135 0.000 20
Di-isopropyl ether 0.125 0.142 0.135 114 108 60.0 - 136 5.05 20
Ethylbenzene 0.125 0.121 0.122 96.8 97.6 74.0 - 126 0.823 20
Hexachloro-1,3-butadiene 0.125 0.126 0.119 101 95.2 57.0 - 150 5.71 20
Isopropylbenzene 0.125 0.123 0.122 98.4 97.6 72.0 - 127 0.816 20
p-Isopropyltoluene 0.125 0.127 0.123 102 98.4 72.0 - 133 3.20 20
2-Butanone (MEK)0.625 0.750 0.772 120 124 30.0 - 160 2.89 24
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 348 of 526
3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131341-1
RECOVERY R4131341-2
L1784578-02,04,05,06,11
LCS Sample / File ID:R4131341-1 / 1011_02LCS SDG:L1784578
LCSD Sample / File ID:R4131341-2 / 1011_03 Analytical Batch:WG2379147
Instrument ID:VOCMS59 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg mg/kg %%%%%
Methylene Chloride 0.125 0.143 0.143 114 114 68.0 - 123 0.000 20
4-Methyl-2-pentanone (MIBK)0.625 0.663 0.655 106 105 56.0 - 143 1.21 20
Methyl tert-butyl ether 0.125 0.149 0.141 119 113 66.0 - 132 5.52 20
Naphthalene 0.125 0.113 0.111 90.4 88.8 59.0 - 130 1.79 20
n-Propylbenzene 0.125 0.129 0.124 103 99.2 74.0 - 126 3.95 20
Styrene 0.125 0.116 0.115 92.8 92.0 72.0 - 127 0.866 20
1,1,1,2-Tetrachloroethane 0.125 0.117 0.115 93.6 92.0 74.0 - 129 1.72 20
1,1,2,2-Tetrachloroethane 0.125 0.121 0.114 96.8 91.2 68.0 - 128 5.96 20
1,1,2-Trichlorotrifluoroethane 0.125 0.180 0.172 144*138 61.0 - 139 4.55 20
Tetrachloroethene 0.125 0.110 0.113 88.0 90.4 70.0 - 136 2.69 20
Toluene 0.125 0.121 0.124 96.8 99.2 75.0 - 121 2.45 20
1,2,3-Trichlorobenzene 0.125 0.118 0.111 94.4 88.8 59.0 - 139 6.11 20
1,2,4-Trichlorobenzene 0.125 0.118 0.113 94.4 90.4 62.0 - 137 4.33 20
1,1,1-Trichloroethane 0.125 0.142 0.139 114 111 69.0 - 126 2.14 20
1,1,2-Trichloroethane 0.125 0.118 0.116 94.4 92.8 78.0 - 123 1.71 20
Trichloroethene 0.125 0.130 0.125 104 100 76.0 - 126 3.92 20
Trichlorofluoromethane 0.125 0.163 0.165 130 132 61.0 - 142 1.22 20
1,2,3-Trichloropropane 0.125 0.137 0.131 110 105 67.0 - 129 4.48 20
1,2,4-Trimethylbenzene 0.125 0.126 0.120 101 96.0 70.0 - 126 4.88 20
1,2,3-Trimethylbenzene 0.125 0.125 0.119 100 95.2 74.0 - 124 4.92 20
1,3,5-Trimethylbenzene 0.125 0.130 0.124 104 99.2 73.0 - 127 4.72 20
Vinyl chloride 0.125 0.139 0.139 111 111 63.0 - 134 0.000 20
Xylenes, Total 0.375 0.358 0.357 95.5 95.2 72.0 - 127 0.280 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 349 of 526
3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131396-1
RECOVERY _______________
L1784578-17
LCS Sample / File ID:R4131396-1 / 1010_31LCSA SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2380092
Instrument ID:VOCMS16 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
Acetone 0.0250 0.0347 139 19.0 - 160
Acrolein 0.0250 0.0299 120 10.0 - 160
Acrylonitrile 0.0250 0.0305 122 55.0 - 149
Benzene 0.00500 0.00464 92.8 70.0 - 123
Bromobenzene 0.00500 0.00415 83.0 73.0 - 121
Bromodichloromethane 0.00500 0.00459 91.8 75.0 - 120
Bromoform 0.00500 0.00390 78.0 68.0 - 132
Bromomethane 0.00500 0.00641 128 10.0 - 160
n-Butylbenzene 0.00500 0.00459 91.8 73.0 - 125
sec-Butylbenzene 0.00500 0.00450 90.0 75.0 - 125
tert-Butylbenzene 0.00500 0.00410 82.0 76.0 - 124
Carbon tetrachloride 0.00500 0.00513 103 68.0 - 126
Chlorobenzene 0.00500 0.00441 88.2 80.0 - 121
Chlorodibromomethane 0.00500 0.00403 80.6 77.0 - 125
Chloroethane 0.00500 0.00658 132 47.0 - 150
Chloroform 0.00500 0.00516 103 73.0 - 120
Chloromethane 0.00500 0.00515 103 41.0 - 142
2-Chlorotoluene 0.00500 0.00456 91.2 76.0 - 123
4-Chlorotoluene 0.00500 0.00413 82.6 75.0 - 122
1,2-Dibromo-3-Chloropropane 0.00500 0.00509 102 58.0 - 134
1,2-Dibromoethane 0.00500 0.00436 87.2 80.0 - 122
Dibromomethane 0.00500 0.00549 110 80.0 - 120
1,2-Dichlorobenzene 0.00500 0.00476 95.2 79.0 - 121
1,3-Dichlorobenzene 0.00500 0.00451 90.2 79.0 - 120
1,4-Dichlorobenzene 0.00500 0.00458 91.6 79.0 - 120
Dichlorodifluoromethane 0.00500 0.00509 102 51.0 - 149
1,1-Dichloroethane 0.00500 0.00540 108 70.0 - 126
1,2-Dichloroethane 0.00500 0.00511 102 70.0 - 128
1,1-Dichloroethene 0.00500 0.00537 107 71.0 - 124
cis-1,2-Dichloroethene 0.00500 0.00534 107 73.0 - 120
trans-1,2-Dichloroethene 0.00500 0.00535 107 73.0 - 120
1,2-Dichloropropane 0.00500 0.00444 88.8 77.0 - 125
1,1-Dichloropropene 0.00500 0.00512 102 74.0 - 126
1,3-Dichloropropane 0.00500 0.00433 86.6 80.0 - 120
cis-1,3-Dichloropropene 0.00500 0.00375 75.0*80.0 - 123
trans-1,3-Dichloropropene 0.00500 0.00394 78.8 78.0 - 124
2,2-Dichloropropane 0.00500 0.0107 214*58.0 - 130
Di-isopropyl ether 0.00500 0.00521 104 58.0 - 138
Ethylbenzene 0.00500 0.00450 90.0 79.0 - 123
Hexachloro-1,3-butadiene 0.00500 0.00655 131 54.0 - 138
Isopropylbenzene 0.00500 0.00497 99.4 76.0 - 127
p-Isopropyltoluene 0.00500 0.00435 87.0 76.0 - 125
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 350 of 526
3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131396-1
RECOVERY _______________
L1784578-17
LCS Sample / File ID:R4131396-1 / 1010_31LCSA SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2380092
Instrument ID:VOCMS16 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
2-Butanone (MEK)0.0250 0.0248 99.2 44.0 - 160
Methylene Chloride 0.00500 0.00546 109 67.0 - 120
4-Methyl-2-pentanone (MIBK)0.0250 0.0251 100 68.0 - 142
Methyl tert-butyl ether 0.00500 0.00530 106 68.0 - 125
Naphthalene 0.00500 0.00558 112 54.0 - 135
n-Propylbenzene 0.00500 0.00420 84.0 77.0 - 124
Styrene 0.00500 0.00443 88.6 73.0 - 130
1,1,1,2-Tetrachloroethane 0.00500 0.00497 99.4 75.0 - 125
1,1,2,2-Tetrachloroethane 0.00500 0.00436 87.2 65.0 - 130
1,1,2-Trichlorotrifluoroethane 0.00500 0.00496 99.2 69.0 - 132
Tetrachloroethene 0.00500 0.00455 91.0 72.0 - 132
Toluene 0.00500 0.00432 86.4 79.0 - 120
1,2,3-Trichlorobenzene 0.00500 0.00672 134 50.0 - 138
1,2,4-Trichlorobenzene 0.00500 0.00599 120 57.0 - 137
1,1,1-Trichloroethane 0.00500 0.00532 106 73.0 - 124
1,1,2-Trichloroethane 0.00500 0.00461 92.2 80.0 - 120
Trichloroethene 0.00500 0.00461 92.2 78.0 - 124
Trichlorofluoromethane 0.00500 0.00594 119 59.0 - 147
1,2,3-Trichloropropane 0.00500 0.00461 92.2 73.0 - 130
1,2,4-Trimethylbenzene 0.00500 0.00454 90.8 76.0 - 121
1,2,3-Trimethylbenzene 0.00500 0.00471 94.2 77.0 - 120
1,3,5-Trimethylbenzene 0.00500 0.00450 90.0 76.0 - 122
Vinyl chloride 0.00500 0.00593 119 67.0 - 131
Xylenes, Total 0.0150 0.0140 93.3 79.0 - 123
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 351 of 526
3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4132125-1
RECOVERY _______________
L1784578-01,03,12,13,15
LCS Sample / File ID:R4132125-1 / 1011a_03LCS SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2380545
Instrument ID:VOCMS56 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
Acetone 0.625 0.531 85.0 10.0 - 160
Acrylonitrile 0.625 0.568 90.9 45.0 - 153
Benzene 0.125 0.105 84.0 70.0 - 123
Bromobenzene 0.125 0.143 114 73.0 - 121
Bromodichloromethane 0.125 0.109 87.2 73.0 - 121
Bromoform 0.125 0.125 100 64.0 - 132
Bromomethane 0.125 0.0982 78.6 56.0 - 147
n-Butylbenzene 0.125 0.143 114 68.0 - 135
sec-Butylbenzene 0.125 0.148 118 74.0 - 130
tert-Butylbenzene 0.125 0.149 119 75.0 - 127
Carbon tetrachloride 0.125 0.109 87.2 66.0 - 128
Chlorobenzene 0.125 0.124 99.2 76.0 - 128
Chlorodibromomethane 0.125 0.129 103 74.0 - 127
Chloroethane 0.125 0.0990 79.2 61.0 - 134
Chloroform 0.125 0.102 81.6 72.0 - 123
Chloromethane 0.125 0.0934 74.7 51.0 - 138
2-Chlorotoluene 0.125 0.139 111 75.0 - 124
4-Chlorotoluene 0.125 0.150 120 75.0 - 124
1,2-Dibromo-3-Chloropropane 0.125 0.130 104 59.0 - 130
1,2-Dibromoethane 0.125 0.131 105 74.0 - 128
Dibromomethane 0.125 0.106 84.8 75.0 - 122
1,2-Dichlorobenzene 0.125 0.132 106 76.0 - 124
1,3-Dichlorobenzene 0.125 0.136 109 76.0 - 125
1,4-Dichlorobenzene 0.125 0.135 108 77.0 - 121
Dichlorodifluoromethane 0.125 0.107 85.6 43.0 - 156
1,1-Dichloroethane 0.125 0.106 84.8 70.0 - 127
1,2-Dichloroethane 0.125 0.0996 79.7 65.0 - 131
1,1-Dichloroethene 0.125 0.109 87.2 65.0 - 131
cis-1,2-Dichloroethene 0.125 0.108 86.4 73.0 - 125
trans-1,2-Dichloroethene 0.125 0.106 84.8 71.0 - 125
1,2-Dichloropropane 0.125 0.108 86.4 74.0 - 125
1,1-Dichloropropene 0.125 0.104 83.2 73.0 - 125
1,3-Dichloropropane 0.125 0.129 103 80.0 - 125
cis-1,3-Dichloropropene 0.125 0.118 94.4 76.0 - 127
trans-1,3-Dichloropropene 0.125 0.135 108 73.0 - 127
2,2-Dichloropropane 0.125 0.107 85.6 59.0 - 135
Di-isopropyl ether 0.125 0.112 89.6 60.0 - 136
Ethylbenzene 0.125 0.123 98.4 74.0 - 126
Hexachloro-1,3-butadiene 0.125 0.134 107 57.0 - 150
Isopropylbenzene 0.125 0.129 103 72.0 - 127
p-Isopropyltoluene 0.125 0.131 105 72.0 - 133
2-Butanone (MEK)0.625 0.569 91.0 30.0 - 160
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 352 of 526
3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4132125-1
RECOVERY _______________
L1784578-01,03,12,13,15
LCS Sample / File ID:R4132125-1 / 1011a_03LCS SDG:L1784578
LCSD Sample / File ID:_______________Analytical Batch:WG2380545
Instrument ID:VOCMS56 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/kg mg/kg %%%%%
Methylene Chloride 0.125 0.103 82.4 68.0 - 123
4-Methyl-2-pentanone (MIBK)0.625 0.693 111 56.0 - 143
Methyl tert-butyl ether 0.125 0.114 91.2 66.0 - 132
Naphthalene 0.125 0.116 92.8 59.0 - 130
n-Propylbenzene 0.125 0.139 111 74.0 - 126
Styrene 0.125 0.127 102 72.0 - 127
1,1,1,2-Tetrachloroethane 0.125 0.124 99.2 74.0 - 129
1,1,2,2-Tetrachloroethane 0.125 0.144 115 68.0 - 128
1,1,2-Trichlorotrifluoroethane 0.125 0.102 81.6 61.0 - 139
Tetrachloroethene 0.125 0.124 99.2 70.0 - 136
Toluene 0.125 0.131 105 75.0 - 121
1,2,3-Trichlorobenzene 0.125 0.135 108 59.0 - 139
1,2,4-Trichlorobenzene 0.125 0.140 112 62.0 - 137
1,1,1-Trichloroethane 0.125 0.114 91.2 69.0 - 126
1,1,2-Trichloroethane 0.125 0.122 97.6 78.0 - 123
Trichloroethene 0.125 0.107 85.6 76.0 - 126
Trichlorofluoromethane 0.125 0.110 88.0 61.0 - 142
1,2,3-Trichloropropane 0.125 0.148 118 67.0 - 129
1,2,4-Trimethylbenzene 0.125 0.151 121 70.0 - 126
1,2,3-Trimethylbenzene 0.125 0.144 115 74.0 - 124
1,3,5-Trimethylbenzene 0.125 0.144 115 73.0 - 127
Vinyl chloride 0.125 0.103 82.4 63.0 - 134
Xylenes, Total 0.375 0.413 110 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4132481-1
RECOVERY R4132481-2
L1784578-18
LCS Sample / File ID:R4132481-1 / 1010_02LCSA SDG:L1784578
LCSD Sample / File ID:R4132481-2 / 1010_03A Analytical Batch:WG2379334
Instrument ID:VOCMS36 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0212 0.0195 84.8 78.0 19.0 - 160 8.35 27
Acrolein 0.0250 0.0229 0.0215 91.6 86.0 10.0 - 160 6.31 26
Acrylonitrile 0.0250 0.0230 0.0225 92.0 90.0 55.0 - 149 2.20 20
Benzene 0.00500 0.00538 0.00513 108 103 70.0 - 123 4.76 20
Bromobenzene 0.00500 0.00490 0.00464 98.0 92.8 73.0 - 121 5.45 20
Bromodichloromethane 0.00500 0.00553 0.00534 111 107 75.0 - 120 3.50 20
Bromoform 0.00500 0.00397 0.00420 79.4 84.0 68.0 - 132 5.63 20
Bromomethane 0.00500 0.00916 0.00926 183*185*10.0 - 160 1.09 25
n-Butylbenzene 0.00500 0.00441 0.00431 88.2 86.2 73.0 - 125 2.29 20
sec-Butylbenzene 0.00500 0.00508 0.00465 102 93.0 75.0 - 125 8.84 20
tert-Butylbenzene 0.00500 0.00472 0.00449 94.4 89.8 76.0 - 124 4.99 20
Carbon tetrachloride 0.00500 0.00581 0.00550 116 110 68.0 - 126 5.48 20
Chlorobenzene 0.00500 0.00529 0.00512 106 102 80.0 - 121 3.27 20
Chlorodibromomethane 0.00500 0.00466 0.00462 93.2 92.4 77.0 - 125 0.862 20
Chloroethane 0.00500 0.00717 0.00658 143 132 47.0 - 150 8.58 20
Chloroform 0.00500 0.00562 0.00548 112 110 73.0 - 120 2.52 20
Chloromethane 0.00500 0.00500 0.00515 100 103 41.0 - 142 2.96 20
2-Chlorotoluene 0.00500 0.00510 0.00483 102 96.6 76.0 - 123 5.44 20
4-Chlorotoluene 0.00500 0.00489 0.00465 97.8 93.0 75.0 - 122 5.03 20
1,2-Dibromo-3-Chloropropane 0.00500 0.00236 0.00251 47.2*50.2*58.0 - 134 6.16 20
1,2-Dibromoethane 0.00500 0.00436 0.00431 87.2 86.2 80.0 - 122 1.15 20
Dibromomethane 0.00500 0.00565 0.00521 113 104 80.0 - 120 8.10 20
1,2-Dichlorobenzene 0.00500 0.00492 0.00465 98.4 93.0 79.0 - 121 5.64 20
1,3-Dichlorobenzene 0.00500 0.00505 0.00486 101 97.2 79.0 - 120 3.83 20
1,4-Dichlorobenzene 0.00500 0.00522 0.00502 104 100 79.0 - 120 3.91 20
Dichlorodifluoromethane 0.00500 0.00475 0.00473 95.0 94.6 51.0 - 149 0.422 20
1,1-Dichloroethane 0.00500 0.00548 0.00539 110 108 70.0 - 126 1.66 20
1,2-Dichloroethane 0.00500 0.00561 0.00560 112 112 70.0 - 128 0.178 20
1,1-Dichloroethene 0.00500 0.00519 0.00486 104 97.2 71.0 - 124 6.57 20
cis-1,2-Dichloroethene 0.00500 0.00563 0.00540 113 108 73.0 - 120 4.17 20
trans-1,2-Dichloroethene 0.00500 0.00544 0.00499 109 99.8 73.0 - 120 8.63 20
1,2-Dichloropropane 0.00500 0.00549 0.00523 110 105 77.0 - 125 4.85 20
1,1-Dichloropropene 0.00500 0.00544 0.00498 109 99.6 74.0 - 126 8.83 20
1,3-Dichloropropane 0.00500 0.00482 0.00481 96.4 96.2 80.0 - 120 0.208 20
cis-1,3-Dichloropropene 0.00500 0.00495 0.00472 99.0 94.4 80.0 - 123 4.76 20
trans-1,3-Dichloropropene 0.00500 0.00477 0.00441 95.4 88.2 78.0 - 124 7.84 20
2,2-Dichloropropane 0.00500 0.00556 0.00518 111 104 58.0 - 130 7.08 20
Di-isopropyl ether 0.00500 0.00562 0.00525 112 105 58.0 - 138 6.81 20
Ethylbenzene 0.00500 0.00491 0.00456 98.2 91.2 79.0 - 123 7.39 20
Hexachloro-1,3-butadiene 0.00500 0.00479 0.00463 95.8 92.6 54.0 - 138 3.40 20
Isopropylbenzene 0.00500 0.00454 0.00453 90.8 90.6 76.0 - 127 0.221 20
p-Isopropyltoluene 0.00500 0.00473 0.00459 94.6 91.8 76.0 - 125 3.00 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4132481-1
RECOVERY R4132481-2
L1784578-18
LCS Sample / File ID:R4132481-1 / 1010_02LCSA SDG:L1784578
LCSD Sample / File ID:R4132481-2 / 1010_03A Analytical Batch:WG2379334
Instrument ID:VOCMS36 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
2-Butanone (MEK)0.0250 0.0189 0.0182 75.6 72.8 44.0 - 160 3.77 20
Methylene Chloride 0.00500 0.00595 0.00544 119 109 67.0 - 120 8.96 20
4-Methyl-2-pentanone (MIBK)0.0250 0.0205 0.0200 82.0 80.0 68.0 - 142 2.47 20
Methyl tert-butyl ether 0.00500 0.00480 0.00446 96.0 89.2 68.0 - 125 7.34 20
n-Propylbenzene 0.00500 0.00483 0.00473 96.6 94.6 77.0 - 124 2.09 20
Styrene 0.00500 0.00417 0.00404 83.4 80.8 73.0 - 130 3.17 20
1,1,1,2-Tetrachloroethane 0.00500 0.00494 0.00511 98.8 102 75.0 - 125 3.38 20
1,1,2,2-Tetrachloroethane 0.00500 0.00444 0.00434 88.8 86.8 65.0 - 130 2.28 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00534 0.00508 107 102 69.0 - 132 4.99 20
Tetrachloroethene 0.00500 0.00542 0.00502 108 100 72.0 - 132 7.66 20
Toluene 0.00500 0.00521 0.00511 104 102 79.0 - 120 1.94 20
1,2,3-Trichlorobenzene 0.00500 0.00288 0.00325 57.6 65.0 50.0 - 138 12.1 20
1,2,4-Trichlorobenzene 0.00500 0.00342 0.00362 68.4 72.4 57.0 - 137 5.68 20
1,1,1-Trichloroethane 0.00500 0.00532 0.00528 106 106 73.0 - 124 0.755 20
1,1,2-Trichloroethane 0.00500 0.00490 0.00458 98.0 91.6 80.0 - 120 6.75 20
Trichloroethene 0.00500 0.00548 0.00537 110 107 78.0 - 124 2.03 20
Trichlorofluoromethane 0.00500 0.00550 0.00539 110 108 59.0 - 147 2.02 20
1,2,3-Trichloropropane 0.00500 0.00486 0.00416 97.2 83.2 73.0 - 130 15.5 20
1,2,4-Trimethylbenzene 0.00500 0.00460 0.00441 92.0 88.2 76.0 - 121 4.22 20
1,2,3-Trimethylbenzene 0.00500 0.00491 0.00465 98.2 93.0 77.0 - 120 5.44 20
1,3,5-Trimethylbenzene 0.00500 0.00493 0.00462 98.6 92.4 76.0 - 122 6.49 20
Vinyl chloride 0.00500 0.00550 0.00515 110 103 67.0 - 131 6.57 20
Xylenes, Total 0.0150 0.0142 0.0140 94.7 93.3 79.0 - 123 1.42 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4133124-1
RECOVERY R4133124-2
L1784578-18
LCS Sample / File ID:R4133124-1 / 1015_02LCSA SDG:L1784578
LCSD Sample / File ID:R4133124-2 / 1015_03A Analytical Batch:WG2381936
Instrument ID:VOCMS42 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
Naphthalene 0.00500 0.00386 0.00428 77.2 85.6 54.0 - 135 10.3 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4131396-3
Lab Sample ID:R4131396-3 SDG:L1784578
Lab File ID:1010_34A Preparation Date/Time:10/10/24 22:33
Instrument ID:VOCMS16 Analysis Date/Time:10/10/24 22:33
Analytical Batch:WG2380092 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4131396-1 VOCMS16 1010_31LCSA 10/10/24 21:27
EB-93024 L1784578-17 VOCMS16 1010_38 10/11/24 01:18
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4132481-3
Lab Sample ID:R4132481-3 SDG:L1784578
Lab File ID:1010_08A Preparation Date/Time:10/10/24 05:50
Instrument ID:VOCMS36 Analysis Date/Time:10/10/24 05:50
Analytical Batch:WG2379334 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4132481-1 VOCMS36 1010_02LCSA 10/10/24 03:47
LCSD R4132481-2 VOCMS36 1010_03A 10/10/24 04:07
TRIP BLANK L1784578-18 VOCMS36 1010_10 10/10/24 06:31
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4133124-3
Lab Sample ID:R4133124-3 SDG:L1784578
Lab File ID:1015_05A Preparation Date/Time:10/15/24 09:42
Instrument ID:VOCMS42 Analysis Date/Time:10/15/24 09:42
Analytical Batch:WG2381936 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4133124-1 VOCMS42 1015_02LCSA 10/15/24 08:43
LCSD R4133124-2 VOCMS42 1015_03A 10/15/24 09:03
TRIP BLANK L1784578-18 VOCMS42 1015_06 10/15/24 10:43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4132125-2
Lab Sample ID:R4132125-2 SDG:L1784578
Lab File ID:1011a_06 Preparation Date/Time:10/12/24 04:44
Instrument ID:VOCMS56 Analysis Date/Time:10/12/24 04:44
Analytical Batch:WG2380545 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4132125-1 VOCMS56 1011a_03LCS 10/12/24 03:47
S-13 (0-6)L1784578-01 VOCMS56 1011a_16 10/12/24 07:53
S-32 (0-6)L1784578-03 VOCMS56 1011a_17 10/12/24 08:12
S-14 (0-6)L1784578-12 VOCMS56 1011a_18 10/12/24 08:31
S-11 (0-6)L1784578-13 VOCMS56 1011a_19 10/12/24 08:50
S-14 (6-12)L1784578-15 VOCMS56 1011a_20 10/12/24 09:09
OS L1784968-27 VOCMS56 1011a_30 10/12/24 12:19
MS R4132125-3 VOCMS56 1011a_31 10/12/24 12:38
MSD R4132125-4 VOCMS56 1011a_32 10/12/24 12:57
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4131341-3
Lab Sample ID:R4131341-3 SDG:L1784578
Lab File ID:1011_07 Preparation Date/Time:10/11/24 02:15
Instrument ID:VOCMS59 Analysis Date/Time:10/11/24 02:15
Analytical Batch:WG2379147 Dilution Factor:1
Analytical Method:8260B Matrix:Solid
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4131341-1 VOCMS59 1011_02LCS 10/11/24 00:38
LCSD R4131341-2 VOCMS59 1011_03 10/11/24 00:57
S-15 (0-6)L1784578-02 VOCMS59 1011_19 10/11/24 06:08
S-12 (6-12)L1784578-04 VOCMS59 1011_20 10/11/24 06:28
S-12 (0-6)L1784578-05 VOCMS59 1011_21 10/11/24 06:47
S-10 (0-6)L1784578-06 VOCMS59 1011_22 10/11/24 07:07
S-10 (6-12)L1784578-11 VOCMS59 1011_23 10/11/24 07:26
MS R4131341-4 VOCMS59 1011_28 10/11/24 09:04
MSD R4131341-5 VOCMS59 1011_29 10/11/24 09:24
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0922_07 SDG:L1784578
Instrument ID:VOCMS16 Analytical Method:8260B
Analysis Date/Time:09/22/24 16:25
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 124
96 95 5 9 6
173 174 0 2 0
174 95 50 200 81
175 174 5 9 8
176 174 95 105 99
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.5 0.5 0922_09 09/22/24 17:10
STD-1 1 0922_10 09/22/24 17:32
STD-2 2 0922_11 09/22/24 17:54
STD-5.0 5.0 0922_12 09/22/24 18:16
STD-25 25 0922_13 09/22/24 18:38
STD-75 75 0922_14 09/22/24 19:00
STD-100 100 0922_15 09/22/24 19:22
STD-200 200 0922_16 09/22/24 19:44
SSCV VOCMS160922240922_20755006 0922_20 09/22/24 21:13
STD-.05A .05A 0922_22 09/22/24 21:57
STD-0.1A 0.1A 0922_23 09/22/24 22:18
STD-0.2A 0.2A 0922_24 09/22/24 22:40
STD-0.5A 0.5A 0922_25 09/22/24 23:02
STD-1A 1A 0922_26 09/22/24 23:24
STD-5A 5A 0922_27 09/22/24 23:46
STD-10A 10A 0922_28 09/23/24 00:08
STD-15A 15A 0922_29 09/23/24 00:30
STD-20A 20A 0922_30 09/23/24 00:52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1010_31T SDG:L1784578
Instrument ID:VOCMS16 Analytical Method:8260B
Analysis Date/Time:10/10/24 21:27
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 133
96 95 5 9 6
173 174 0 2 0
174 95 50 200 75
175 174 5 9 8
176 174 95 105 100
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS161010241010_31755006 1010_31 10/10/24 21:27
LCS R4131396-1 1010_31LCSA 10/10/24 21:27
BLANK R4131396-3 1010_34A 10/10/24 22:33
EB-93024 L1784578-17 1010_38 10/11/24 01:18
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0912_01 SDG:L1784578
Instrument ID:VOCMS36 Analytical Method:8260B
Analysis Date/Time:09/12/24 16:31
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 119
96 95 5 9 7
173 174 0 2 1
174 95 50 200 84
175 174 5 9 7
176 174 95 105 96
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.5 0.5 0912_08 09/12/24 18:56
STD-1 1 0912_09 09/12/24 19:17
STD-2 2 0912_10 09/12/24 19:38
STD-5.0 5.0 0912_11 09/12/24 19:58
STD-25 25 0912_12 09/12/24 20:19
STD-75 75 0912_13 09/12/24 20:40
STD-100 100 0912_14 09/12/24 21:00
STD-200 200 0912_15 09/12/24 21:21
SSCV VOCMS360912240912_19752875 0912_19 09/12/24 22:44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0912_21 SDG:L1784578
Instrument ID:VOCMS36 Analytical Method:8260B
Analysis Date/Time:09/12/24 23:26
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 121
96 95 5 9 8
173 174 0 2 1
174 95 50 200 83
175 174 5 9 7
176 174 95 105 97
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-.05A .05A 0912_23 09/13/24 00:08
STD-0.1A 0.1A 0912_24 09/13/24 04:34
STD-0.2A 0.2A 0912_25 09/13/24 04:55
STD-0.5A 0.5A 0912_26 09/13/24 05:16
STD-1A 1A 0912_27 09/13/24 05:36
STD-5A 5A 0912_28 09/13/24 05:57
STD-10A 10A 0912_29 09/13/24 06:18
STD-15A 15A 0912_30 09/13/24 06:39
STD-20A 20A 0912_31 09/13/24 07:00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0912_36 SDG:L1784578
Instrument ID:VOCMS36 Analytical Method:8260B
Analysis Date/Time:09/13/24 09:20
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 119
96 95 5 9 6
173 174 0 2 1
174 95 50 200 84
175 174 5 9 7
176 174 95 105 96
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.5 0.5 0912_39 09/13/24 10:22
STD-1 1 0912_40 09/13/24 10:43
STD-2 2 0912_41 09/13/24 11:04
STD-5.0 5.0 0912_42 09/13/24 11:25
STD-25 25 0912_43 09/13/24 11:45
STD-75 75 0912_44 09/13/24 12:06
SSCV VOCMS360912240912_48752875 0912_48 09/13/24 14:12
STD-0.5 0.5 0912_53 09/13/24 15:56
STD-1 1 0912_54 09/13/24 16:16
STD-2 2 0912_55 09/13/24 16:37
STD-5.0 5.0 0912_56 09/13/24 16:58
STD-10 10 0912_57 09/13/24 17:19
STD-20 20 0912_58 09/13/24 17:40
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1010_01T SDG:L1784578
Instrument ID:VOCMS36 Analytical Method:8260B
Analysis Date/Time:10/10/24 03:27
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 114
96 95 5 9 7
173 174 0 2 2
174 95 50 200 88
175 174 5 9 8
176 174 95 105 95
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS361010241010_02752875 1010_02 10/10/24 03:47
LCS R4132481-1 1010_02LCSA 10/10/24 03:47
LCSD R4132481-2 1010_03A 10/10/24 04:07
BLANK R4132481-3 1010_08A 10/10/24 05:50
TRIP BLANK L1784578-18 1010_10 10/10/24 06:31
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1003a_01 SDG:L1784578
Instrument ID:VOCMS42 Analytical Method:8260B
Analysis Date/Time:10/03/24 14:22
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 114
96 95 5 9 6
173 174 0 2 1
174 95 50 200 87
175 174 5 9 7
176 174 95 105 97
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.02 0.02 1003A_04 10/03/24 15:22
STD-0.04 0.04 1003A_05 10/03/24 15:42
STD-0.1 0.1 1003A_06 10/03/24 16:02
STD-0.2 0.2 1003A_07 10/03/24 16:21
STD-0.5 0.5 1003A_08 10/03/24 16:41
STD-1 1 1003A_09 10/03/24 17:01
STD-2 2 1003A_10 10/03/24 17:21
STD-5.0 5.0 1003A_11 10/03/24 17:41
STD-25 25 1003A_12 10/03/24 18:01
STD-75 75 1003A_13 10/03/24 18:21
STD-100 100 1003A_14 10/03/24 18:40
SSCV VOCMS42100324a1003a_18757788 1003a_18 10/03/24 19:59
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1015_02T SDG:L1784578
Instrument ID:VOCMS42 Analytical Method:8260B
Analysis Date/Time:10/15/24 08:43
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 113
96 95 5 9 7
173 174 0 2 1
174 95 50 200 89
175 174 5 9 7
176 174 95 105 96
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS421015241015_02757788 1015_02 10/15/24 08:43
LCS R4133124-1 1015_02LCSA 10/15/24 08:43
LCSD R4133124-2 1015_03A 10/15/24 09:03
BLANK R4133124-3 1015_05A 10/15/24 09:42
TRIP BLANK L1784578-18 1015_06 10/15/24 10:43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1008a_11 SDG:L1784578
Instrument ID:VOCMS56 Analytical Method:8260B
Analysis Date/Time:10/08/24 21:52
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 110
96 95 5 9 7
173 174 0 2 2
174 95 50 200 91
175 174 5 9 8
176 174 95 105 95
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.02 0.02 1008A_14 10/08/24 22:49
STD-0.04 0.04 1008A_15 10/08/24 23:08
STD-0.1 0.1 1008A_16 10/08/24 23:27
STD-0.2 0.2 1008A_17 10/08/24 23:46
STD-0.5 0.5 1008A_18 10/09/24 00:04
STD-2 2 1008A_20 10/09/24 00:42
STD-5.0 5.0 1008A_21 10/09/24 01:01
STD-25 25 1008A_22 10/09/24 01:20
STD-75 75 1008A_23 10/09/24 01:39
STD-100 100 1008A_24 10/09/24 01:58
SSCV VOCMS56100824a1008a_28758896 1008a_28 10/09/24 03:13
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1011a_01T SDG:L1784578
Instrument ID:VOCMS56 Analytical Method:8260B
Analysis Date/Time:10/12/24 03:09
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 121
96 95 5 9 7
173 174 0 2 1
174 95 50 200 82
175 174 5 9 8
176 174 95 105 95
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS56101124a1011a_03758896 1011a_03 10/12/24 03:47
LCS R4132125-1 1011a_03LCS 10/12/24 03:47
BLANK R4132125-2 1011a_06 10/12/24 04:44
S-13 (0-6)L1784578-01 1011a_16 10/12/24 07:53
S-32 (0-6)L1784578-03 1011a_17 10/12/24 08:12
S-14 (0-6)L1784578-12 1011a_18 10/12/24 08:31
S-11 (0-6)L1784578-13 1011a_19 10/12/24 08:50
S-14 (6-12)L1784578-15 1011a_20 10/12/24 09:09
OS L1784968-27 1011a_30 10/12/24 12:19
MS R4132125-3 1011a_31 10/12/24 12:38
MSD R4132125-4 1011a_32 10/12/24 12:57
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1007_01 SDG:L1784578
Instrument ID:VOCMS59 Analytical Method:8260B
Analysis Date/Time:10/07/24 17:05
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 134
96 95 5 9 7
173 174 0 2 1
174 95 50 200 74
175 174 5 9 7
176 174 95 105 100
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.02 0.02 1007_04 10/07/24 18:03
STD-0.04 0.04 1007_05 10/07/24 18:23
STD-0.1 0.1 1007_06 10/07/24 18:43
STD-0.2 0.2 1007_07 10/07/24 19:02
STD-0.5 0.5 1007_08 10/07/24 19:22
STD-1 1 1007_09 10/07/24 19:42
STD-2 2 1007_10 10/07/24 20:01
STD-5.0 5.0 1007_11 10/07/24 20:21
STD-25 25 1007_12 10/07/24 20:40
STD-75 75 1007_13 10/07/24 20:59
STD-100 100 1007_14 10/07/24 21:19
SSCV VOCMS591007241007_18758651 1007_18 10/07/24 22:36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1011_01T SDG:L1784578
Instrument ID:VOCMS59 Analytical Method:8260B
Analysis Date/Time:10/11/24 00:19
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 134
96 95 5 9 7
173 174 0 2 1
174 95 50 200 74
175 174 5 9 7
176 174 95 105 98
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS591011241011_02758651 1011_02 10/11/24 00:38
LCS R4131341-1 1011_02LCS 10/11/24 00:38
LCSD R4131341-2 1011_03 10/11/24 00:57
BLANK R4131341-3 1011_07 10/11/24 02:15
S-15 (0-6)L1784578-02 1011_19 10/11/24 06:08
S-12 (6-12)L1784578-04 1011_20 10/11/24 06:28
S-12 (0-6)L1784578-05 1011_21 10/11/24 06:47
OS L1784578-06 1011_22 10/11/24 07:07
S-10 (0-6)L1784578-06 1011_22 10/11/24 07:07
S-10 (6-12)L1784578-11 1011_23 10/11/24 07:26
MS R4131341-4 1011_28 10/11/24 09:04
MSD R4131341-5 1011_29 10/11/24 09:24
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16 Calibration Start Date:09/22/24 17:10
Std File: 1010_31 Calibration End Date:09/23/24 00:52
Std Analysis Date:10/10/24 21:27
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 41622 8.19 46528 6.51 116763 4.58
UPPER LIMIT 83244 93056 233526
LOWER LIMIT 20811 23264 58382
LCS R4131396-1
WG2380092 1x
1010_31LCS
A 41622 8.19 46528 6.51 116763 4.58
BLANK R4131396-3
WG2380092 1x 1010_34A 42396 8.19 54292 6.51 128569 4.59
L1784578-17 WG2380092
1x 1010_38 43362 8.19 53452 6.51 128673 4.58
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS36 Calibration Start Date:09/12/24 18:56
Std File: 1010_02 Calibration End Date:09/13/24 17:40
Std Analysis Date:10/10/24 03:47
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 64968 8.09 75672 6.40 155845 4.47
UPPER LIMIT 129936 151344 311690
LOWER LIMIT 32484 37836 77923
LCS R4132481-1
WG2379334 1x
1010_02LCS
A 64968 8.09 75672 6.40 155845 4.47
LCSD R4132481-2
WG2379334 1x 1010_03A 68080 8.10 75594 6.40 161219 4.47
BLANK R4132481-3
WG2379334 1x 1010_08A 70536 8.10 81941 6.40 176004 4.47
L1784578-18 WG2379334
1x 1010_10 66297 8.10 79187 6.41 172774 4.47
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS42 Calibration Start Date:10/03/24 15:22
Std File: 1015_02 Calibration End Date:10/03/24 18:40
Std Analysis Date:10/15/24 08:43
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 180564.20 8.83 189013.40 7.07 436091 5
UPPER LIMIT 361128 378027 872182
LOWER LIMIT 90282 94507 218046
LCS R4133124-1
WG2381936 1x
1015_02LCS
A 180564.20 8.83 189013.40 7.07 436091 5
LCSD R4133124-2
WG2381936 1x 1015_03A 182047.40 8.82 190724.20 7.07 438337.10 5
BLANK R4133124-3
WG2381936 1x 1015_05A 170712.20 8.83 192902.80 7.08 424388.20 5
L1784578-18 WG2381936
1x 1015_06 211258.90 8.82 232601.10 7.07 496267.20 5
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS56 Calibration Start Date:10/08/24 22:49
Std File: 1011a_03 Calibration End Date:10/09/24 01:58
Std Analysis Date:10/12/24 03:47
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 516439.20 8.26 600561.20 6.57 1199064 4.62
UPPER LIMIT 1032878 1201122 2398128
LOWER LIMIT 258220 300281 599532
LCS R4132125-1
WG2380545 1x
1011a_03LC
S 516439.20 8.26 600561.20 6.57 1199064 4.62
BLANK R4132125-2
WG2380545 1x 1011a_06 409084.40 8.26 536712.10 6.57 1207301 4.62
L1784578-01 WG2380545
1x 1011a_16 517384.60 8.26 616867 6.57 1393999 4.62
L1784578-03 WG2380545
1x 1011a_17 416870.20 8.26 563155.30 6.57 1308421 4.62
L1784578-12 WG2380545
1.1x 1011a_18 493033.90 8.26 622684.50 6.57 1380266 4.62
L1784578-13 WG2380545
1x 1011a_19 495176.50 8.26 648918.60 6.57 1452058 4.62
L1784578-15 WG2380545
1.1x 1011a_20 521963.10 8.26 626108.90 6.57 1404197 4.62
OS L1784968-27
WG2380545 20x 1011a_30 639289.60 8.26 643563.50 6.57 1401316 4.62
MS R4132125-3
WG2380545 20x 1011a_31 597977.50 8.26 636860 6.57 1332179 4.62
MSD R4132125-4
WG2380545 20x 1011a_32 623657.40 8.26 624283.80 6.57 1354709 4.62
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS59 Calibration Start Date:10/07/24 18:03
Std File: 1011_02 Calibration End Date:10/07/24 21:19
Std Analysis Date:10/11/24 00:38
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 151903.10 8.36 181903.70 6.63 386782.30 4.63
UPPER LIMIT 303806 363807 773565
LOWER LIMIT 75952 90952 193391
LCS R4131341-1
WG2379147 1x 1011_02LCS 151903.10 8.36 181903.70 6.63 386782.30 4.63
LCSD R4131341-2
WG2379147 1x 1011_03 159961.40 8.36 182974 6.63 391754.60 4.63
BLANK R4131341-3
WG2379147 1x 1011_07 152674.90 8.36 188404.10 6.63 445651.60 4.63
L1784578-02 WG2379147
1.08x 1011_19 167717.90 8.36 219741 6.63 501924.40 4.63
L1784578-04 WG2379147
1x 1011_20 167163.70 8.36 208181.80 6.64 477932 4.63
L1784578-05 WG2379147
1x 1011_21 160889.30 8.36 201756.20 6.63 464034.60 4.63
L1784578-06 WG2379147
1.13x 1011_22 167301.50 8.36 221022.60 6.63 506902.90 4.63
OS L1784578-06
WG2379147 1.13x 1011_22 167301.50 8.36 221022.60 6.63 506902.90 4.63
L1784578-11 WG2379147
1.12x 1011_23 167881.80 8.36 206046.50 6.64 478265.50 4.63
MS R4131341-4
WG2379147 1.13x 1011_28 168948.30 8.36 226956.50 6.63 501846.30 4.63
MSD R4131341-5
WG2379147 1.13x 1011_29 169239.30 8.36 220594.70 6.63 500325.60 4.63
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:1011a_16 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 10:00
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 07:53
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.04 g
Total Solids (%):83.9 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.20 U 0.0512 0.0701
Acrylonitrile 107-13-1 0 U 0.00506 0.0175
Benzene 71-43-2 4.40 U 0.000655 0.00140
Bromobenzene 108-86-1 0 U 0.00126 0.0175
Bromodichloromethane 75-27-4 0 U 0.00102 0.00351
Bromoform 75-25-2 0 U 0.00164 0.0351
Bromomethane 74-83-9 0 U 0.00276 0.0175
n-Butylbenzene 104-51-8 0 U 0.00736 0.0175
sec-Butylbenzene 135-98-8 0 U 0.00404 0.0175
tert-Butylbenzene 98-06-6 0 U 0.00274 0.00701
Carbon tetrachloride 56-23-5 0 U 0.00126 0.00701
Chlorobenzene 108-90-7 0 U 0.000295 0.00351
Chlorodibromomethane 124-48-1 0 U 0.000858 0.00351
Chloroethane 75-00-3 2.38 U 0.00238 0.00701
Chloroform 67-66-3 4.07 U 0.00144 0.00351
Chloromethane 74-87-3 0 U 0.00610 0.0175
2-Chlorotoluene 95-49-8 0 U 0.00121 0.00351
4-Chlorotoluene 106-43-4 0 U 0.000631 0.00701
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00547 0.0351
1,2-Dibromoethane 106-93-4 0 U 0.000909 0.00351
Dibromomethane 74-95-3 0 U 0.00105 0.00701
1,2-Dichlorobenzene 95-50-1 0 U 0.000596 0.00701
1,3-Dichlorobenzene 541-73-1 0 U 0.000842 0.00701
1,4-Dichlorobenzene 106-46-7 8.27 U 0.000982 0.00701
Dichlorodifluoromethane 75-71-8 0 U 0.00226 0.00701
1,1-Dichloroethane 75-34-3 0 U 0.000689 0.00351
1,2-Dichloroethane 107-06-2 4.52 U 0.000910 0.00351
1,1-Dichloroethene 75-35-4 0 U 0.000850 0.00351
cis-1,2-Dichloroethene 156-59-2 3.98 U 0.00103 0.00351
trans-1,2-Dichloroethene 156-60-5 0 U 0.00146 0.00701
1,2-Dichloropropane 78-87-5 0 U 0.00199 0.00701
1,1-Dichloropropene 563-58-6 0 U 0.00113 0.00351
1,3-Dichloropropane 142-28-9 0 U 0.000703 0.00701
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00106 0.00351
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00160 0.00701
2,2-Dichloropropane 594-20-7 3.96 U 0.00194 0.00351
Di-isopropyl ether 108-20-3 3.37 U 0.000575 0.00140
Ethylbenzene 100-41-4 0 U 0.00103 0.00351
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00842 0.0351
Isopropylbenzene 98-82-8 0 U 0.000596 0.00351
p-Isopropyltoluene 99-87-6 0 U 0.00358 0.00701
2-Butanone (MEK)78-93-3 4.24 U 0.0891 0.140
Methylene Chloride 75-09-2 3.18 U 0.00931 0.0351
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:1011a_16 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 10:00
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 07:53
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.04 g
Total Solids (%):83.9 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.79 U 0.00320 0.0351
Methyl tert-butyl ether 1634-04-4 0 U 0.000491 0.00140
Naphthalene 91-20-3 0 U 0.00685 0.0175
n-Propylbenzene 103-65-1 0 U 0.00133 0.00701
Styrene 100-42-5 0 U 0.000321 0.0175
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00133 0.00351
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000975 0.00351
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00106 0.00351
Tetrachloroethene 127-18-4 5.84 0.00243 J 0.00126 0.00351
Toluene 108-88-3 5.58 U 0.00182 0.00701
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0103 0.0175
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00617 0.0175
1,1,1-Trichloroethane 71-55-6 0 U 0.00129 0.00351
1,1,2-Trichloroethane 79-00-5 0 U 0.000837 0.00351
Trichloroethene 79-01-6 4.72 U 0.000819 0.00140
Trichlorofluoromethane 75-69-4 0 U 0.00116 0.00351
1,2,3-Trichloropropane 96-18-4 0 U 0.00227 0.0175
1,2,4-Trimethylbenzene 95-63-6 0 U 0.00222 0.00701
1,2,3-Trimethylbenzene 526-73-8 8.26 U 0.00222 0.00701
1,3,5-Trimethylbenzene 108-67-8 0 U 0.00281 0.00701
Vinyl chloride 75-01-4 0 U 0.00163 0.00351
Xylenes, Total 1330-20-7 6.69 U 0.00123 0.00912
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:1011_19 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 14:25
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 06:08
Dilution Factor:1.08 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.26 g
Total Solids (%):87.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 U 0.0506 0.0693
Acrylonitrile 107-13-1 3.64 U 0.00501 0.0173
Benzene 71-43-2 4.40 0.0184 0.000647 0.00139
Bromobenzene 108-86-1 0 U 0.00125 0.0173
Bromodichloromethane 75-27-4 0 U 0.00101 0.00347
Bromoform 75-25-2 0 U 0.00162 0.0347
Bromomethane 74-83-9 0 U 0.00274 0.0173
n-Butylbenzene 104-51-8 8.52 U 0.00728 0.0173
sec-Butylbenzene 135-98-8 8.12 U 0.00399 0.0173
tert-Butylbenzene 98-06-6 8.03 U 0.00271 0.00693
Carbon tetrachloride 56-23-5 4.19 U 0.00125 0.00693
Chlorobenzene 108-90-7 0 U 0.000292 0.00347
Chlorodibromomethane 124-48-1 0 U 0.000849 0.00347
Chloroethane 75-00-3 2.30 U J4 0.00236 0.00693
Chloroform 67-66-3 4.04 U 0.00143 0.00347
Chloromethane 74-87-3 1.87 U 0.00604 0.0173
2-Chlorotoluene 95-49-8 0 U 0.00120 0.00347
4-Chlorotoluene 106-43-4 7.90 U 0.000624 0.00693
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00541 0.0347
1,2-Dibromoethane 106-93-4 6.30 U 0.000899 0.00347
Dibromomethane 74-95-3 0 U 0.00104 0.00693
1,2-Dichlorobenzene 95-50-1 0 U 0.000589 0.00693
1,3-Dichlorobenzene 541-73-1 8.36 U 0.000832 0.00693
1,4-Dichlorobenzene 106-46-7 8.36 U 0.000971 0.00693
Dichlorodifluoromethane 75-71-8 0 U 0.00223 0.00693
1,1-Dichloroethane 75-34-3 3.64 U 0.000681 0.00347
1,2-Dichloroethane 107-06-2 4.52 U 0.000900 0.00347
1,1-Dichloroethene 75-35-4 0 U J4 0.000840 0.00347
cis-1,2-Dichloroethene 156-59-2 0 U 0.00102 0.00347
trans-1,2-Dichloroethene 156-60-5 0 U 0.00144 0.00693
1,2-Dichloropropane 78-87-5 0 U 0.00196 0.00693
1,1-Dichloropropene 563-58-6 4.27 U 0.00112 0.00347
1,3-Dichloropropane 142-28-9 0 U 0.000695 0.00693
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00105 0.00347
trans-1,3-Dichloropropene 10061-02-6 5.84 U 0.00158 0.00693
2,2-Dichloropropane 594-20-7 3.94 U 0.00191 0.00347
Di-isopropyl ether 108-20-3 0 U 0.000569 0.00139
Ethylbenzene 100-41-4 6.65 0.0289 0.00102 0.00347
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00832 0.0347
Isopropylbenzene 98-82-8 7.28 0.00434 0.000589 0.00347
p-Isopropyltoluene 99-87-6 8.22 0.0203 0.00353 0.00693
2-Butanone (MEK)78-93-3 4.21 U 0.0881 0.139
Methylene Chloride 75-09-2 3.11 0.00985 B J 0.00921 0.0347
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:1011_19 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 14:25
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 06:08
Dilution Factor:1.08 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.26 g
Total Solids (%):87.1 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.00946 J 0.00316 0.0347
Methyl tert-butyl ether 1634-04-4 3.28 0.00125 J 0.000485 0.00139
Naphthalene 91-20-3 10.18 0.0203 0.00677 0.0173
n-Propylbenzene 103-65-1 7.59 0.00981 0.00132 0.00693
Styrene 100-42-5 7.06 U 0.000317 0.0173
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00131 0.00347
1,1,2,2-Tetrachloroethane 79-34-5 7.63 U 0.000964 0.00347
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U J4 0.00105 0.00347
Tetrachloroethene 127-18-4 5.89 1.71 0.00124 0.00347
Toluene 108-88-3 5.63 0.176 0.00180 0.00693
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0102 0.0173
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00610 0.0173
1,1,1-Trichloroethane 71-55-6 4.18 0.00604 0.00128 0.00347
1,1,2-Trichloroethane 79-00-5 6 U 0.000828 0.00347
Trichloroethene 79-01-6 4.74 0.0103 0.000810 0.00139
Trichlorofluoromethane 75-69-4 2.38 U 0.00115 0.00347
1,2,3-Trichloropropane 96-18-4 0 U 0.00225 0.0173
1,2,4-Trimethylbenzene 95-63-6 8.03 0.119 0.00220 0.00693
1,2,3-Trimethylbenzene 526-73-8 8.38 0.0462 0.00220 0.00693
1,3,5-Trimethylbenzene 108-67-8 7.73 0.0533 0.00277 0.00693
Vinyl chloride 75-01-4 0 U 0.00161 0.00347
Xylenes, Total 1330-20-7 7.06 0.326 0.00122 0.00902
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 382 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:1011a_17 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 10:10
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 08:12
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.73 g
Total Solids (%):83.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.19 U 0.0520 0.0713
Acrylonitrile 107-13-1 0 U 0.00515 0.0178
Benzene 71-43-2 4.40 U 0.000666 0.00143
Bromobenzene 108-86-1 0 U 0.00128 0.0178
Bromodichloromethane 75-27-4 0 U 0.00103 0.00356
Bromoform 75-25-2 0 U 0.00167 0.0356
Bromomethane 74-83-9 2.39 U 0.00281 0.0178
n-Butylbenzene 104-51-8 0 U 0.00748 0.0178
sec-Butylbenzene 135-98-8 7.96 U 0.00411 0.0178
tert-Butylbenzene 98-06-6 0 U 0.00278 0.00713
Carbon tetrachloride 56-23-5 0 U 0.00128 0.00713
Chlorobenzene 108-90-7 0 U 0.000299 0.00356
Chlorodibromomethane 124-48-1 0 U 0.000872 0.00356
Chloroethane 75-00-3 0 U 0.00242 0.00713
Chloroform 67-66-3 4.06 U 0.00147 0.00356
Chloromethane 74-87-3 0 U 0.00620 0.0178
2-Chlorotoluene 95-49-8 0 U 0.00123 0.00356
4-Chlorotoluene 106-43-4 0 U 0.000641 0.00713
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00556 0.0356
1,2-Dibromoethane 106-93-4 0 U 0.000924 0.00356
Dibromomethane 74-95-3 0 U 0.00107 0.00713
1,2-Dichlorobenzene 95-50-1 0 U 0.000606 0.00713
1,3-Dichlorobenzene 541-73-1 8.26 U 0.000855 0.00713
1,4-Dichlorobenzene 106-46-7 8.26 U 0.000998 0.00713
Dichlorodifluoromethane 75-71-8 0 U 0.00229 0.00713
1,1-Dichloroethane 75-34-3 0 U 0.000700 0.00356
1,2-Dichloroethane 107-06-2 4.51 U 0.000925 0.00356
1,1-Dichloroethene 75-35-4 0 U 0.000864 0.00356
cis-1,2-Dichloroethene 156-59-2 0 U 0.00105 0.00356
trans-1,2-Dichloroethene 156-60-5 0 U 0.00148 0.00713
1,2-Dichloropropane 78-87-5 0 U 0.00202 0.00713
1,1-Dichloropropene 563-58-6 0 U 0.00115 0.00356
1,3-Dichloropropane 142-28-9 0 U 0.000714 0.00713
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00108 0.00356
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00162 0.00713
2,2-Dichloropropane 594-20-7 4 U 0.00197 0.00356
Di-isopropyl ether 108-20-3 0 U 0.000584 0.00143
Ethylbenzene 100-41-4 6.58 0.00143 J 0.00105 0.00356
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00855 0.0356
Isopropylbenzene 98-82-8 0 U 0.000606 0.00356
p-Isopropyltoluene 99-87-6 8.12 0.00405 J 0.00363 0.00713
2-Butanone (MEK)78-93-3 4.22 U 0.0905 0.143
Methylene Chloride 75-09-2 3.18 0.0113 B J 0.00946 0.0356
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 383 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:1011a_17 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 10:10
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 08:12
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.73 g
Total Solids (%):83.0 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.00325 0.0356
Methyl tert-butyl ether 1634-04-4 0 U 0.000499 0.00143
Naphthalene 91-20-3 0 U 0.00696 0.0178
n-Propylbenzene 103-65-1 0 U 0.00135 0.00713
Styrene 100-42-5 0 U 0.000326 0.0178
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00135 0.00356
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000991 0.00356
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00107 0.00356
Tetrachloroethene 127-18-4 5.83 0.00170 J 0.00128 0.00356
Toluene 108-88-3 5.58 U 0.00185 0.00713
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0104 0.0178
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00627 0.0178
1,1,1-Trichloroethane 71-55-6 0 U 0.00132 0.00356
1,1,2-Trichloroethane 79-00-5 0 U 0.000851 0.00356
Trichloroethene 79-01-6 0 U 0.000832 0.00143
Trichlorofluoromethane 75-69-4 0 U 0.00118 0.00356
1,2,3-Trichloropropane 96-18-4 0 U 0.00231 0.0178
1,2,4-Trimethylbenzene 95-63-6 7.96 U 0.00225 0.00713
1,2,3-Trimethylbenzene 526-73-8 8.26 U 0.00225 0.00713
1,3,5-Trimethylbenzene 108-67-8 7.58 U 0.00285 0.00713
Vinyl chloride 75-01-4 0 U 0.00165 0.00356
Xylenes, Total 1330-20-7 6.99 0.00235 J 0.00125 0.00926
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:1011_20 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 16:05
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 06:28
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.63 g
Total Solids (%):85.5 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.14 U 0.0493 0.0675
Acrylonitrile 107-13-1 3.64 U 0.00487 0.0169
Benzene 71-43-2 4.40 0.0155 0.000630 0.00135
Bromobenzene 108-86-1 0 U 0.00121 0.0169
Bromodichloromethane 75-27-4 0 U 0.000978 0.00337
Bromoform 75-25-2 0 U 0.00158 0.0337
Bromomethane 74-83-9 0 U 0.00266 0.0169
n-Butylbenzene 104-51-8 8.56 U 0.00708 0.0169
sec-Butylbenzene 135-98-8 8.13 U 0.00389 0.0169
tert-Butylbenzene 98-06-6 8.03 U 0.00263 0.00675
Carbon tetrachloride 56-23-5 0 U 0.00121 0.00675
Chlorobenzene 108-90-7 0 U 0.000283 0.00337
Chlorodibromomethane 124-48-1 0 U 0.000826 0.00337
Chloroethane 75-00-3 0 U J4 0.00229 0.00675
Chloroform 67-66-3 4.04 U 0.00139 0.00337
Chloromethane 74-87-3 0 U 0.00587 0.0169
2-Chlorotoluene 95-49-8 0 U 0.00117 0.00337
4-Chlorotoluene 106-43-4 7.81 U 0.000607 0.00675
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00526 0.0337
1,2-Dibromoethane 106-93-4 0 U 0.000874 0.00337
Dibromomethane 74-95-3 0 U 0.00101 0.00675
1,2-Dichlorobenzene 95-50-1 0 U 0.000574 0.00675
1,3-Dichlorobenzene 541-73-1 8.36 U 0.000810 0.00675
1,4-Dichlorobenzene 106-46-7 8.36 U 0.000945 0.00675
Dichlorodifluoromethane 75-71-8 0 U 0.00217 0.00675
1,1-Dichloroethane 75-34-3 3.58 0.00951 0.000663 0.00337
1,2-Dichloroethane 107-06-2 4.51 U 0.000876 0.00337
1,1-Dichloroethene 75-35-4 0 U J4 0.000818 0.00337
cis-1,2-Dichloroethene 156-59-2 3.89 0.0606 0.000991 0.00337
trans-1,2-Dichloroethene 156-60-5 3.21 0.00660 J 0.00140 0.00675
1,2-Dichloropropane 78-87-5 0 U 0.00192 0.00675
1,1-Dichloropropene 563-58-6 0 U 0.00109 0.00337
1,3-Dichloropropane 142-28-9 0 U 0.000676 0.00675
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00102 0.00337
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00154 0.00675
2,2-Dichloropropane 594-20-7 3.99 U 0.00186 0.00337
Di-isopropyl ether 108-20-3 3.47 U 0.000553 0.00135
Ethylbenzene 100-41-4 6.65 0.00704 0.000995 0.00337
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00810 0.0337
Isopropylbenzene 98-82-8 7.28 0.00152 J 0.000574 0.00337
p-Isopropyltoluene 99-87-6 8.23 0.00761 0.00344 0.00675
2-Butanone (MEK)78-93-3 4.22 U 0.0857 0.135
Methylene Chloride 75-09-2 3.11 0.0103 B J 0.00896 0.0337
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 385 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:1011_20 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 16:05
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 06:28
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.63 g
Total Solids (%):85.5 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 U 0.00308 0.0337
Methyl tert-butyl ether 1634-04-4 0 U 0.000472 0.00135
Naphthalene 91-20-3 10.18 0.0225 0.00659 0.0169
n-Propylbenzene 103-65-1 7.59 0.00219 J 0.00128 0.00675
Styrene 100-42-5 7.07 U 0.000309 0.0169
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00128 0.00337
1,1,2,2-Tetrachloroethane 79-34-5 7.62 U 0.000938 0.00337
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U J4 0.00102 0.00337
Tetrachloroethene 127-18-4 5.89 0.0112 0.00121 0.00337
Toluene 108-88-3 5.63 0.0781 0.00175 0.00675
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00989 0.0169
1,2,4-Trichlorobenzene 120-82-1 9.91 U 0.00594 0.0169
1,1,1-Trichloroethane 71-55-6 4.19 U 0.00125 0.00337
1,1,2-Trichloroethane 79-00-5 0 U 0.000806 0.00337
Trichloroethene 79-01-6 4.74 0.0258 0.000788 0.00135
Trichlorofluoromethane 75-69-4 0 U 0.00112 0.00337
1,2,3-Trichloropropane 96-18-4 0 U 0.00219 0.0169
1,2,4-Trimethylbenzene 95-63-6 8.03 0.0200 0.00213 0.00675
1,2,3-Trimethylbenzene 526-73-8 8.38 0.00954 0.00213 0.00675
1,3,5-Trimethylbenzene 108-67-8 7.73 0.00609 J 0.00270 0.00675
Vinyl chloride 75-01-4 0 U 0.00157 0.00337
Xylenes, Total 1330-20-7 7.06 0.0793 0.00119 0.00877
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 386 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:1011_21 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 15:50
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 06:47
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.56 g
Total Solids (%):90.4 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 U 0.0444 0.0609
Acrylonitrile 107-13-1 3.66 U 0.00440 0.0152
Benzene 71-43-2 4.40 0.00153 0.000569 0.00122
Bromobenzene 108-86-1 0 U 0.00110 0.0152
Bromodichloromethane 75-27-4 0 U 0.000883 0.00304
Bromoform 75-25-2 0 U 0.00142 0.0304
Bromomethane 74-83-9 0 U 0.00240 0.0152
n-Butylbenzene 104-51-8 8.56 U 0.00639 0.0152
sec-Butylbenzene 135-98-8 8.13 U 0.00351 0.0152
tert-Butylbenzene 98-06-6 8.03 U 0.00237 0.00609
Carbon tetrachloride 56-23-5 0 U 0.00109 0.00609
Chlorobenzene 108-90-7 0 U 0.000256 0.00304
Chlorodibromomethane 124-48-1 0 U 0.000745 0.00304
Chloroethane 75-00-3 2.30 U J4 0.00207 0.00609
Chloroform 67-66-3 4.04 U 0.00125 0.00304
Chloromethane 74-87-3 1.87 U 0.00530 0.0152
2-Chlorotoluene 95-49-8 0 U 0.00105 0.00304
4-Chlorotoluene 106-43-4 7.90 U 0.000548 0.00609
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00475 0.0304
1,2-Dibromoethane 106-93-4 0 U 0.000789 0.00304
Dibromomethane 74-95-3 0 U 0.000913 0.00609
1,2-Dichlorobenzene 95-50-1 0 U 0.000518 0.00609
1,3-Dichlorobenzene 541-73-1 8.36 U 0.000731 0.00609
1,4-Dichlorobenzene 106-46-7 8.36 U 0.000852 0.00609
Dichlorodifluoromethane 75-71-8 0 U 0.00196 0.00609
1,1-Dichloroethane 75-34-3 3.58 0.00330 0.000598 0.00304
1,2-Dichloroethane 107-06-2 4.51 U 0.000790 0.00304
1,1-Dichloroethene 75-35-4 0 U J4 0.000738 0.00304
cis-1,2-Dichloroethene 156-59-2 3.89 0.0321 0.000894 0.00304
trans-1,2-Dichloroethene 156-60-5 3.21 0.00477 J 0.00127 0.00609
1,2-Dichloropropane 78-87-5 0 U 0.00173 0.00609
1,1-Dichloropropene 563-58-6 0 U 0.000985 0.00304
1,3-Dichloropropane 142-28-9 0 U 0.000610 0.00609
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000922 0.00304
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00139 0.00609
2,2-Dichloropropane 594-20-7 0 U 0.00168 0.00304
Di-isopropyl ether 108-20-3 3.46 U 0.000499 0.00122
Ethylbenzene 100-41-4 6.65 0.00196 J 0.000897 0.00304
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00731 0.0304
Isopropylbenzene 98-82-8 7.28 0.00122 J 0.000518 0.00304
p-Isopropyltoluene 99-87-6 8.22 0.00679 0.00311 0.00609
2-Butanone (MEK)78-93-3 4.21 U 0.0773 0.122
Methylene Chloride 75-09-2 3.11 0.00871 B J 0.00809 0.0304
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 387 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:1011_21 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 15:50
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 06:47
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.56 g
Total Solids (%):90.4 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.00309 J 0.00278 0.0304
Methyl tert-butyl ether 1634-04-4 0 U 0.000426 0.00122
Naphthalene 91-20-3 10.18 0.0192 0.00594 0.0152
n-Propylbenzene 103-65-1 7.59 0.00136 J 0.00116 0.00609
Styrene 100-42-5 7.07 U 0.000279 0.0152
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00115 0.00304
1,1,2,2-Tetrachloroethane 79-34-5 7.63 U 0.000846 0.00304
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U J4 0.000918 0.00304
Tetrachloroethene 127-18-4 5.89 0.00425 0.00109 0.00304
Toluene 108-88-3 5.63 0.0115 0.00158 0.00609
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00893 0.0152
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00536 0.0152
1,1,1-Trichloroethane 71-55-6 4.19 0.00145 J 0.00112 0.00304
1,1,2-Trichloroethane 79-00-5 0 U 0.000727 0.00304
Trichloroethene 79-01-6 4.74 0.0106 0.000711 0.00122
Trichlorofluoromethane 75-69-4 0 U 0.00101 0.00304
1,2,3-Trichloropropane 96-18-4 0 U 0.00197 0.0152
1,2,4-Trimethylbenzene 95-63-6 8.03 0.0190 0.00192 0.00609
1,2,3-Trimethylbenzene 526-73-8 8.38 0.0109 0.00192 0.00609
1,3,5-Trimethylbenzene 108-67-8 7.73 0.00772 0.00244 0.00609
Vinyl chloride 75-01-4 0 U 0.00141 0.00304
Xylenes, Total 1330-20-7 7.06 0.0311 0.00107 0.00792
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 388 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:1011_22 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 07:07
Dilution Factor:1.13 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.85 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 U 0.0465 0.0637
Acrylonitrile 107-13-1 3.64 U 0.00460 0.0159
Benzene 71-43-2 4.40 0.0350 0.000595 0.00127
Bromobenzene 108-86-1 0 U 0.00115 0.0159
Bromodichloromethane 75-27-4 0 U 0.000924 0.00319
Bromoform 75-25-2 0 U 0.00149 0.0319
Bromomethane 74-83-9 0 U 0.00251 0.0159
n-Butylbenzene 104-51-8 8.56 U 0.00669 0.0159
sec-Butylbenzene 135-98-8 8.12 U 0.00367 0.0159
tert-Butylbenzene 98-06-6 8.03 U 0.00248 0.00637
Carbon tetrachloride 56-23-5 4.17 U 0.00114 0.00637
Chlorobenzene 108-90-7 0 U 0.000267 0.00319
Chlorodibromomethane 124-48-1 0 U 0.000780 0.00319
Chloroethane 75-00-3 2.25 U J4 0.00217 0.00637
Chloroform 67-66-3 4.04 U 0.00131 0.00319
Chloromethane 74-87-3 0 U 0.00555 0.0159
2-Chlorotoluene 95-49-8 0 U 0.00110 0.00319
4-Chlorotoluene 106-43-4 7.90 U 0.000574 0.00637
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00497 0.0319
1,2-Dibromoethane 106-93-4 0 U 0.000825 0.00319
Dibromomethane 74-95-3 0 U 0.000956 0.00637
1,2-Dichlorobenzene 95-50-1 0 U 0.000541 0.00637
1,3-Dichlorobenzene 541-73-1 0 U 0.000765 0.00637
1,4-Dichlorobenzene 106-46-7 0 U 0.000892 0.00637
Dichlorodifluoromethane 75-71-8 0 U 0.00205 0.00637
1,1-Dichloroethane 75-34-3 3.58 0.0106 0.000626 0.00319
1,2-Dichloroethane 107-06-2 4.50 U 0.000827 0.00319
1,1-Dichloroethene 75-35-4 0 U J4 0.000772 0.00319
cis-1,2-Dichloroethene 156-59-2 3.89 0.165 0.000935 0.00319
trans-1,2-Dichloroethene 156-60-5 3.21 0.00733 0.00133 0.00637
1,2-Dichloropropane 78-87-5 0 U 0.00180 0.00637
1,1-Dichloropropene 563-58-6 0 U 0.00103 0.00319
1,3-Dichloropropane 142-28-9 0 U 0.000638 0.00637
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000964 0.00319
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00145 0.00637
2,2-Dichloropropane 594-20-7 3.93 U 0.00176 0.00319
Di-isopropyl ether 108-20-3 3.48 U 0.000522 0.00127
Ethylbenzene 100-41-4 6.65 0.00988 0.000939 0.00319
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00765 0.0319
Isopropylbenzene 98-82-8 7.28 0.00277 J 0.000541 0.00319
p-Isopropyltoluene 99-87-6 8.22 0.0132 0.00325 0.00637
2-Butanone (MEK)78-93-3 4.21 U 0.0810 0.127
Methylene Chloride 75-09-2 3.11 0.0134 B J 0.00846 0.0319
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:1011_22 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 07:07
Dilution Factor:1.13 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.85 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.0133 J 0.00291 0.0319
Methyl tert-butyl ether 1634-04-4 3.26 U 0.000447 0.00127
Naphthalene 91-20-3 10.18 0.0451 0.00621 0.0159
n-Propylbenzene 103-65-1 7.59 0.00293 J 0.00121 0.00637
Styrene 100-42-5 7.06 U 0.000292 0.0159
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00121 0.00319
1,1,2,2-Tetrachloroethane 79-34-5 7.63 U 0.000885 0.00319
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U J4 0.000961 0.00319
Tetrachloroethene 127-18-4 5.89 0.0461 0.00114 0.00319
Toluene 108-88-3 5.63 0.169 J6 0.00166 0.00637
1,2,3-Trichlorobenzene 87-61-6 10.36 U 0.00934 0.0159
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00560 0.0159
1,1,1-Trichloroethane 71-55-6 4.18 0.00564 0.00117 0.00319
1,1,2-Trichloroethane 79-00-5 6 U 0.000761 0.00319
Trichloroethene 79-01-6 4.74 0.0625 0.000744 0.00127
Trichlorofluoromethane 75-69-4 2.38 U 0.00105 0.00319
1,2,3-Trichloropropane 96-18-4 7.72 U 0.00206 0.0159
1,2,4-Trimethylbenzene 95-63-6 8.03 0.0529 0.00202 0.00637
1,2,3-Trimethylbenzene 526-73-8 8.38 0.0379 0.00202 0.00637
1,3,5-Trimethylbenzene 108-67-8 7.73 0.0132 0.00255 0.00637
Vinyl chloride 75-01-4 0 U 0.00148 0.00319
Xylenes, Total 1330-20-7 7.06 0.142 0.00112 0.00829
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:1011_23 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:30
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 07:26
Dilution Factor:1.12 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.95 g
Total Solids (%):95.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 U 0.0443 0.0607
Acrylonitrile 107-13-1 3.58 U 0.00438 0.0152
Benzene 71-43-2 4.40 0.000911 J 0.000567 0.00121
Bromobenzene 108-86-1 0 U 0.00110 0.0152
Bromodichloromethane 75-27-4 0 U 0.000880 0.00304
Bromoform 75-25-2 0 U 0.00142 0.0304
Bromomethane 74-83-9 0 U 0.00240 0.0152
n-Butylbenzene 104-51-8 8.58 U 0.00638 0.0152
sec-Butylbenzene 135-98-8 0 U 0.00350 0.0152
tert-Butylbenzene 98-06-6 8.03 U 0.00236 0.00607
Carbon tetrachloride 56-23-5 0 U 0.00110 0.00607
Chlorobenzene 108-90-7 0 U 0.000255 0.00304
Chlorodibromomethane 124-48-1 0 U 0.000743 0.00304
Chloroethane 75-00-3 2.35 U J4 0.00206 0.00607
Chloroform 67-66-3 4.04 U 0.00125 0.00304
Chloromethane 74-87-3 1.90 U 0.00528 0.0152
2-Chlorotoluene 95-49-8 0 U 0.00105 0.00304
4-Chlorotoluene 106-43-4 7.90 U 0.000546 0.00607
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00474 0.0304
1,2-Dibromoethane 106-93-4 0 U 0.000787 0.00304
Dibromomethane 74-95-3 0 U 0.000911 0.00607
1,2-Dichlorobenzene 95-50-1 0 U 0.000516 0.00607
1,3-Dichlorobenzene 541-73-1 8.36 U 0.000729 0.00607
1,4-Dichlorobenzene 106-46-7 8.36 U 0.000850 0.00607
Dichlorodifluoromethane 75-71-8 0 U 0.00195 0.00607
1,1-Dichloroethane 75-34-3 3.56 U 0.000596 0.00304
1,2-Dichloroethane 107-06-2 4.50 U 0.000788 0.00304
1,1-Dichloroethene 75-35-4 0 U J4 0.000736 0.00304
cis-1,2-Dichloroethene 156-59-2 3.89 0.0101 0.000891 0.00304
trans-1,2-Dichloroethene 156-60-5 3.20 U 0.00126 0.00607
1,2-Dichloropropane 78-87-5 0 U 0.00172 0.00607
1,1-Dichloropropene 563-58-6 0 U 0.000982 0.00304
1,3-Dichloropropane 142-28-9 0 U 0.000608 0.00607
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000919 0.00304
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00139 0.00607
2,2-Dichloropropane 594-20-7 3.97 U 0.00168 0.00304
Di-isopropyl ether 108-20-3 0 U 0.000498 0.00121
Ethylbenzene 100-41-4 6.64 U 0.000894 0.00304
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00729 0.0304
Isopropylbenzene 98-82-8 7.28 U 0.000516 0.00304
p-Isopropyltoluene 99-87-6 8.22 U 0.00310 0.00607
2-Butanone (MEK)78-93-3 4.22 U 0.0771 0.121
Methylene Chloride 75-09-2 3.11 0.00980 B J 0.00807 0.0304
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 391 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:1011_23 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:30
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 07:26
Dilution Factor:1.12 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.95 g
Total Solids (%):95.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 U 0.00276 0.0304
Methyl tert-butyl ether 1634-04-4 0 U 0.000425 0.00121
Naphthalene 91-20-3 10.18 U 0.00593 0.0152
n-Propylbenzene 103-65-1 7.59 U 0.00115 0.00607
Styrene 100-42-5 0 U 0.000278 0.0152
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00115 0.00304
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000844 0.00304
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U J4 0.000915 0.00304
Tetrachloroethene 127-18-4 5.89 0.00388 0.00108 0.00304
Toluene 108-88-3 5.63 0.00459 J 0.00158 0.00607
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00890 0.0152
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00535 0.0152
1,1,1-Trichloroethane 71-55-6 4.18 U 0.00112 0.00304
1,1,2-Trichloroethane 79-00-5 0 U 0.000725 0.00304
Trichloroethene 79-01-6 4.73 0.00310 0.000709 0.00121
Trichlorofluoromethane 75-69-4 0 U 0.00100 0.00304
1,2,3-Trichloropropane 96-18-4 0 U 0.00196 0.0152
1,2,4-Trimethylbenzene 95-63-6 8.03 0.00276 J 0.00192 0.00607
1,2,3-Trimethylbenzene 526-73-8 8.38 0.00236 J 0.00192 0.00607
1,3,5-Trimethylbenzene 108-67-8 7.73 U 0.00243 0.00607
Vinyl chloride 75-01-4 0 U 0.00141 0.00304
Xylenes, Total 1330-20-7 7.06 0.00571 J 0.00107 0.00789
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:1011a_18 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 09:10
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 08:31
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.13 g
Total Solids (%):84.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.26 U 0.0540 0.0741
Acrylonitrile 107-13-1 3.66 U 0.00535 0.0186
Benzene 71-43-2 4.40 0.00671 0.000692 0.00148
Bromobenzene 108-86-1 0 U 0.00133 0.0186
Bromodichloromethane 75-27-4 0 U 0.00107 0.00370
Bromoform 75-25-2 0 U 0.00174 0.0370
Bromomethane 74-83-9 2.39 U 0.00292 0.0186
n-Butylbenzene 104-51-8 0 U 0.00779 0.0186
sec-Butylbenzene 135-98-8 7.94 U 0.00427 0.0186
tert-Butylbenzene 98-06-6 0 U 0.00290 0.00741
Carbon tetrachloride 56-23-5 4.19 0.00174 J 0.00133 0.00741
Chlorobenzene 108-90-7 0 U 0.000311 0.00370
Chlorodibromomethane 124-48-1 0 U 0.000907 0.00370
Chloroethane 75-00-3 2.37 U 0.00252 0.00741
Chloroform 67-66-3 4.07 U 0.00152 0.00370
Chloromethane 74-87-3 0 U 0.00645 0.0186
2-Chlorotoluene 95-49-8 0 U 0.00128 0.00370
4-Chlorotoluene 106-43-4 7.81 U 0.000667 0.00741
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00578 0.0370
1,2-Dibromoethane 106-93-4 0 U 0.000960 0.00370
Dibromomethane 74-95-3 0 U 0.00111 0.00741
1,2-Dichlorobenzene 95-50-1 0 U 0.000630 0.00741
1,3-Dichlorobenzene 541-73-1 8.26 U 0.000889 0.00741
1,4-Dichlorobenzene 106-46-7 8.26 U 0.00104 0.00741
Dichlorodifluoromethane 75-71-8 0 U 0.00238 0.00741
1,1-Dichloroethane 75-34-3 3.62 0.00230 J 0.000727 0.00370
1,2-Dichloroethane 107-06-2 4.51 U 0.000962 0.00370
1,1-Dichloroethene 75-35-4 0 U 0.000898 0.00370
cis-1,2-Dichloroethene 156-59-2 3.92 0.0114 0.00109 0.00370
trans-1,2-Dichloroethene 156-60-5 3.26 0.00167 J 0.00154 0.00741
1,2-Dichloropropane 78-87-5 0 U 0.00210 0.00741
1,1-Dichloropropene 563-58-6 0 U 0.00120 0.00370
1,3-Dichloropropane 142-28-9 0 U 0.000742 0.00741
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00112 0.00370
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00168 0.00741
2,2-Dichloropropane 594-20-7 0 U 0.00205 0.00370
Di-isopropyl ether 108-20-3 0 U 0.000608 0.00148
Ethylbenzene 100-41-4 6.58 0.00341 J 0.00109 0.00370
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00889 0.0370
Isopropylbenzene 98-82-8 7.20 U 0.000630 0.00370
p-Isopropyltoluene 99-87-6 8.11 0.00508 J 0.00379 0.00741
2-Butanone (MEK)78-93-3 4.26 U 0.0942 0.148
Methylene Chloride 75-09-2 3.18 U 0.00983 0.0370
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 393 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:1011a_18 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 09:10
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 08:31
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.13 g
Total Solids (%):84.6 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 U 0.00338 0.0370
Methyl tert-butyl ether 1634-04-4 3.31 U 0.000519 0.00148
Naphthalene 91-20-3 10.10 0.0143 J 0.00723 0.0186
n-Propylbenzene 103-65-1 7.52 U 0.00141 0.00741
Styrene 100-42-5 0 U 0.000339 0.0186
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00140 0.00370
1,1,2,2-Tetrachloroethane 79-34-5 7.41 U 0.00103 0.00370
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00112 0.00370
Tetrachloroethene 127-18-4 5.83 0.119 0.00133 0.00370
Toluene 108-88-3 5.58 0.0264 0.00193 0.00741
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0109 0.0186
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00652 0.0186
1,1,1-Trichloroethane 71-55-6 4.19 0.0160 0.00137 0.00370
1,1,2-Trichloroethane 79-00-5 0 U 0.000885 0.00370
Trichloroethene 79-01-6 4.72 0.244 0.000865 0.00148
Trichlorofluoromethane 75-69-4 0 U 0.00123 0.00370
1,2,3-Trichloropropane 96-18-4 0 U 0.00240 0.0186
1,2,4-Trimethylbenzene 95-63-6 7.94 0.00455 J 0.00234 0.00741
1,2,3-Trimethylbenzene 526-73-8 8.28 0.00319 J 0.00234 0.00741
1,3,5-Trimethylbenzene 108-67-8 7.64 U 0.00296 0.00741
Vinyl chloride 75-01-4 0 U 0.00172 0.00370
Xylenes, Total 1330-20-7 6.98 0.0214 0.00130 0.00963
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:1011a_19 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 08:40
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 08:50
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.79 g
Total Solids (%):97.4 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.26 U 0.0386 0.0528
Acrylonitrile 107-13-1 0 U 0.00381 0.0132
Benzene 71-43-2 4.40 U 0.000493 0.00106
Bromobenzene 108-86-1 0 U 0.000951 0.0132
Bromodichloromethane 75-27-4 0 U 0.000766 0.00264
Bromoform 75-25-2 7.07 U 0.00124 0.0264
Bromomethane 74-83-9 2.38 U 0.00208 0.0132
n-Butylbenzene 104-51-8 0 U 0.00555 0.0132
sec-Butylbenzene 135-98-8 0 U 0.00304 0.0132
tert-Butylbenzene 98-06-6 0 U 0.00206 0.00528
Carbon tetrachloride 56-23-5 0 U 0.000949 0.00528
Chlorobenzene 108-90-7 0 U 0.000222 0.00264
Chlorodibromomethane 124-48-1 0 U 0.000646 0.00264
Chloroethane 75-00-3 2.40 U 0.00180 0.00528
Chloroform 67-66-3 0 U 0.00109 0.00264
Chloromethane 74-87-3 0 U 0.00459 0.0132
2-Chlorotoluene 95-49-8 0 U 0.000914 0.00264
4-Chlorotoluene 106-43-4 0 U 0.000475 0.00528
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00412 0.0264
1,2-Dibromoethane 106-93-4 0 U 0.000684 0.00264
Dibromomethane 74-95-3 0 U 0.000792 0.00528
1,2-Dichlorobenzene 95-50-1 0 U 0.000449 0.00528
1,3-Dichlorobenzene 541-73-1 8.26 U 0.000634 0.00528
1,4-Dichlorobenzene 106-46-7 8.26 U 0.000739 0.00528
Dichlorodifluoromethane 75-71-8 0 U 0.00170 0.00528
1,1-Dichloroethane 75-34-3 0 U 0.000519 0.00264
1,2-Dichloroethane 107-06-2 4.52 U 0.000686 0.00264
1,1-Dichloroethene 75-35-4 0 U 0.000640 0.00264
cis-1,2-Dichloroethene 156-59-2 3.97 U 0.000775 0.00264
trans-1,2-Dichloroethene 156-60-5 0 U 0.00110 0.00528
1,2-Dichloropropane 78-87-5 0 U 0.00150 0.00528
1,1-Dichloropropene 563-58-6 0 U 0.000855 0.00264
1,3-Dichloropropane 142-28-9 0 U 0.000529 0.00528
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000800 0.00264
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00120 0.00528
2,2-Dichloropropane 594-20-7 3.95 U 0.00146 0.00264
Di-isopropyl ether 108-20-3 0 U 0.000433 0.00106
Ethylbenzene 100-41-4 0 U 0.000778 0.00264
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00634 0.0264
Isopropylbenzene 98-82-8 0 U 0.000449 0.00264
p-Isopropyltoluene 99-87-6 8.11 U 0.00269 0.00528
2-Butanone (MEK)78-93-3 4.24 U 0.0671 0.106
Methylene Chloride 75-09-2 3.19 U 0.00701 0.0264
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:1011a_19 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 08:40
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 08:50
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.79 g
Total Solids (%):97.4 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.00241 0.0264
Methyl tert-butyl ether 1634-04-4 3.32 0.000860 J 0.000370 0.00106
Naphthalene 91-20-3 10.11 0.00879 J 0.00515 0.0132
n-Propylbenzene 103-65-1 7.50 U 0.00100 0.00528
Styrene 100-42-5 0 U 0.000242 0.0132
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00100 0.00264
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000734 0.00264
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000796 0.00264
Tetrachloroethene 127-18-4 0 U 0.000946 0.00264
Toluene 108-88-3 5.58 U 0.00137 0.00528
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00774 0.0132
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00465 0.0132
1,1,1-Trichloroethane 71-55-6 0 U 0.000975 0.00264
1,1,2-Trichloroethane 79-00-5 0 U 0.000631 0.00264
Trichloroethene 79-01-6 0 U 0.000617 0.00106
Trichlorofluoromethane 75-69-4 0 U 0.000874 0.00264
1,2,3-Trichloropropane 96-18-4 0 U 0.00171 0.0132
1,2,4-Trimethylbenzene 95-63-6 7.95 U 0.00167 0.00528
1,2,3-Trimethylbenzene 526-73-8 8.28 U 0.00167 0.00528
1,3,5-Trimethylbenzene 108-67-8 7.65 U 0.00211 0.00528
Vinyl chloride 75-01-4 0 U 0.00123 0.00264
Xylenes, Total 1330-20-7 6.69 U 0.000930 0.00687
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:1011a_20 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 09:20
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 09:09
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):86.3 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.26 U 0.0523 0.0717
Acrylonitrile 107-13-1 0 U 0.00517 0.0180
Benzene 71-43-2 4.40 U 0.000670 0.00143
Bromobenzene 108-86-1 0 U 0.00129 0.0180
Bromodichloromethane 75-27-4 0 U 0.00104 0.00358
Bromoform 75-25-2 7.07 U 0.00168 0.0358
Bromomethane 74-83-9 2.32 U 0.00283 0.0180
n-Butylbenzene 104-51-8 0 U 0.00753 0.0180
sec-Butylbenzene 135-98-8 0 U 0.00413 0.0180
tert-Butylbenzene 98-06-6 0 U 0.00280 0.00717
Carbon tetrachloride 56-23-5 0 U 0.00129 0.00717
Chlorobenzene 108-90-7 0 U 0.000301 0.00358
Chlorodibromomethane 124-48-1 0 U 0.000877 0.00358
Chloroethane 75-00-3 0 U 0.00244 0.00717
Chloroform 67-66-3 4.07 U 0.00147 0.00358
Chloromethane 74-87-3 0 U 0.00624 0.0180
2-Chlorotoluene 95-49-8 0 U 0.00124 0.00358
4-Chlorotoluene 106-43-4 0 U 0.000645 0.00717
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00559 0.0358
1,2-Dibromoethane 106-93-4 0 U 0.000929 0.00358
Dibromomethane 74-95-3 0 U 0.00108 0.00717
1,2-Dichlorobenzene 95-50-1 0 U 0.000610 0.00717
1,3-Dichlorobenzene 541-73-1 8.26 U 0.000860 0.00717
1,4-Dichlorobenzene 106-46-7 8.26 U 0.00100 0.00717
Dichlorodifluoromethane 75-71-8 0 U 0.00231 0.00717
1,1-Dichloroethane 75-34-3 0 U 0.000704 0.00358
1,2-Dichloroethane 107-06-2 4.51 U 0.000930 0.00358
1,1-Dichloroethene 75-35-4 0 U 0.000869 0.00358
cis-1,2-Dichloroethene 156-59-2 3.92 U 0.00105 0.00358
trans-1,2-Dichloroethene 156-60-5 0 U 0.00149 0.00717
1,2-Dichloropropane 78-87-5 0 U 0.00203 0.00717
1,1-Dichloropropene 563-58-6 0 U 0.00116 0.00358
1,3-Dichloropropane 142-28-9 0 U 0.000718 0.00717
cis-1,3-Dichloropropene 10061-01-5 0 U 0.00109 0.00358
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00163 0.00717
2,2-Dichloropropane 594-20-7 3.96 U 0.00198 0.00358
Di-isopropyl ether 108-20-3 0 U 0.000588 0.00143
Ethylbenzene 100-41-4 6.58 0.00172 J 0.00106 0.00358
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00860 0.0358
Isopropylbenzene 98-82-8 7.21 U 0.000610 0.00358
p-Isopropyltoluene 99-87-6 8.08 U 0.00366 0.00717
2-Butanone (MEK)78-93-3 4.23 U 0.0911 0.143
Methylene Chloride 75-09-2 3.19 U 0.00951 0.0358
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:1011a_20 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:09/30/24 09:20
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 09:09
Dilution Factor:1.1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.1 g
Total Solids (%):86.3 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.77 U 0.00327 0.0358
Methyl tert-butyl ether 1634-04-4 0 U 0.000502 0.00143
Naphthalene 91-20-3 10.13 U 0.00700 0.0180
n-Propylbenzene 103-65-1 0 U 0.00137 0.00717
Styrene 100-42-5 0 U 0.000328 0.0180
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.00136 0.00358
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000997 0.00358
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.00108 0.00358
Tetrachloroethene 127-18-4 5.83 0.0128 0.00128 0.00358
Toluene 108-88-3 5.58 U 0.00186 0.00717
1,2,3-Trichlorobenzene 87-61-6 0 U 0.0105 0.0180
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00631 0.0180
1,1,1-Trichloroethane 71-55-6 4.19 U 0.00133 0.00358
1,1,2-Trichloroethane 79-00-5 0 U 0.000856 0.00358
Trichloroethene 79-01-6 4.72 0.0159 0.000837 0.00143
Trichlorofluoromethane 75-69-4 0 U 0.00119 0.00358
1,2,3-Trichloropropane 96-18-4 0 U 0.00232 0.0180
1,2,4-Trimethylbenzene 95-63-6 7.95 U 0.00227 0.00717
1,2,3-Trimethylbenzene 526-73-8 8.27 U 0.00227 0.00717
1,3,5-Trimethylbenzene 108-67-8 7.59 U 0.00287 0.00717
Vinyl chloride 75-01-4 0 U 0.00167 0.00358
Xylenes, Total 1330-20-7 7 0.00244 J 0.00126 0.00932
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:1010_38 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS16 Preparation Date/Time:10/11/24 01:18
Analytical Batch:WG2380092 Analysis Date/Time:10/11/24 01:18
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.15 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 4.02 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U J4 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U J4 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 399 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET EB-93024
Lab Sample ID:L1784578-17 SDG:L1784578
Client Sample ID:EB-93024 Collected Date/Time:09/30/24 10:35
Lab File ID:1010_38 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS16 Preparation Date/Time:10/11/24 01:18
Analytical Batch:WG2380092 Analysis Date/Time:10/11/24 01:18
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1784578-18 SDG:L1784578
Client Sample ID:TRIP BLANK Collected Date/Time:09/27/24 00:00
Lab File ID:1010_10 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 06:31
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 06:31
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.06 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U J4 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U J4 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1784578-18 SDG:L1784578
Client Sample ID:TRIP BLANK Collected Date/Time:09/27/24 00:00
Lab File ID:1010_10 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 06:31
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 06:31
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1784578-18 SDG:L1784578
Client Sample ID:TRIP BLANK Collected Date/Time:09/27/24 00:00
Lab File ID:1015_06 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS42 Preparation Date/Time:10/15/24 10:43
Analytical Batch:WG2381936 Analysis Date/Time:10/15/24 10:43
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Naphthalene 91-20-3 10.60 U Q 0.00100 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 403 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 09/22/24
17:10
09/22/24
17:32
09/22/24
17:54
09/22/24
18:16
09/22/24
18:38
09/22/24
19:00
09/22/24
19:22
09/22/24
19:44
VINYL CHLORIDE 0.1680 0.2860 0.2870 0.3450 0.3950 0.39 0.3470 0.3920
BROMOMETHANE 0.1190 0.1710 0.1450 0.1780 0.1790 0.1760 0.1650 0.1740
CHLOROETHANE 0.1530 0.1710 0.2040 0.2060 0.2260 0.1960 0.1770 0.1830
ACROLEIN 0.0730 0.0760 0.0770 0.0820 0.0920 0.0980 0.0970 0.0810
1,1-DICHLOROETHENE 0.1980 0.2680 0.2150 0.2780 0.3140 0.2950 0.28 0.3020
1,1,2-TRICHLOROTRIFLUOROETHANE 0.1210 0.2030 0.2220 0.2840 0.2950 0.2890 0.2590 0.2820
METHYLENE CHLORIDE 0.3680 0.2730 0.3350 0.3340 0.3350 0.3110 0.2990 0.3140
ACRYLONITRILE 0.2940 0.2490 0.2820 0.2960 0.3030 0.2880 0.2880 0.2260
TRANS-1,2-DICHLOROETHENE 0.2720 0.28 0.2970 0.3250 0.3350 0.31 0.2920 0.3090
METHYL TERT-BUTYL ETHER 1.0090 0.9910 1.0190 1.0230 1.11 1.0220 1.05 0.9810
1,1-DICHLOROETHANE 0.6280 0.5880 0.6710 0.6960 0.6950 0.6530 0.6270 0.6510
DI-ISOPROPYL ETHER 1.4660 1.3670 1.4640 1.5050 1.5870 1.4950 1.4740 1.44
2,2-DICHLOROPROPANE 0.1430 0.20 0.1990 0.2450 0.2270 0.2080
CIS-1,2-DICHLOROETHENE 0.3260 0.3010 0.33 0.3580 0.3580 0.3430 0.3250 0.3390
2-BUTANONE (MEK)0.43 0.3820 0.3880 0.3990 0.4080 0.4050 0.4110 0.3210
CHLOROFORM 0.5770 0.5870 0.5740 0.6240 0.6290 0.5920 0.5730 0.5860
1,1,1-TRICHLOROETHANE 0.30 0.3940 0.46 0.4810 0.53 0.4990 0.46 0.4980
CARBON TETRACHLORIDE 0.3150 0.39 0.4820 0.4760 0.5090 0.4870 0.4620 0.4990
1,1-DICHLOROPROPENE 0.2790 0.3570 0.3620 0.4230 0.4530 0.4290 0.4060 0.4310
BENZENE 1.2970 1.2680 1.2930 1.3560 1.3820 1.3210 1.2840 1.3340
1,2-DICHLOROETHANE 0.6050 0.4940 0.5190 0.5450 0.5450 0.5130 0.5080 0.4880
TRICHLOROETHENE 0.2750 0.2830 0.2860 0.3420 0.3510 0.3320 0.3210 0.3310
1,2-DICHLOROPROPANE 0.26 0.2430 0.2950 0.2960 0.2980 0.2890 0.2810 0.2820
DIBROMOMETHANE 0.1840 0.1770 0.2080 0.20 0.2070 0.2030 0.2010 0.1930
BROMODICHLOROMETHANE 0.4380 0.4050 0.4260 0.46 0.47 0.4550 0.4470 0.4520
CIS-1,3-DICHLOROPROPENE 0.4840 0.4890 0.4910 0.5170 0.5650 0.5490 0.5520 0.5450
4-METHYL-2-PENTANONE (MIBK)1.5720 1.5990 1.6870 1.7120 1.7480 1.6840 1.7140 1.48
TOLUENE 3.16 2.9860 3.2660 3.3690 3.2730 3.2410 3.1890 3.2780
TRANS-1,3-DICHLOROPROPENE 1.1190 1.0630 1.1920 1.2550 1.2220 1.2230 1.2380 1.1970
1,1,2-TRICHLOROETHANE 0.71 0.7240 0.7410 0.7270 0.7150 0.7060 0.7150 0.6850
TETRACHLOROETHENE 0.3980 0.4940 0.51 0.5480 0.5810 0.56 0.5340 0.55
1,3-DICHLOROPROPANE 1.3190 1.1840 1.2970 1.3020 1.2720 1.2610 1.2880 1.2520
CHLORODIBROMOMETHANE 0.75 0.7390 0.7860 0.81 0.8010 0.8140 0.8230 0.7930
1,2-DIBROMOETHANE 0.6850 0.7770 0.7330 0.7560 0.7480 0.7550 0.7730 0.7360
CHLOROBENZENE 2.0990 1.7720 1.9360 2.0320 2.0280 2.0060 1.9780 1.9280
1,1,1,2-TETRACHLOROETHANE 0.7580 0.6050 0.7060 0.7190 0.6870 0.6930 0.6950 0.6460
ETHYLBENZENE 0.9120 0.8950 0.9560 1.0180 1.0780 1.0680 1.0530 1.0390
M&P-XYLENE 1.0650 1.0980 1.1560 1.2180 1.3090 1.30 1.2880 1.2630
O-XYLENE 1.0860 1.0440 1.1350 1.1860 1.2470 1.2640 1.2570 1.2150
STYRENE 1.6250 1.7690 1.7590 1.9680 2.1290 2.1640 2.1910 2.1270
BROMOFORM 0.4590 0.44 0.5070 0.52 0.5520 0.56 0.5740 0.5370
ISOPROPYLBENZENE 2.1230 2.3640 2.5640 2.8010 3.0110 3.0680 2.9740 2.8480
BROMOBENZENE 1.7650 1.7850 1.8380 1.8670 1.9660 1.8110 1.8040 1.82
1,1,2,2-TETRACHLOROETHANE 1.3840 1.2420 1.48 1.4020 1.4240 1.2910 1.3510 1.2770
1,2,3-TRICHLOROPROPANE 0.4630 0.3940 0.4940 0.4740 0.5040 0.4620 0.48 0.4480
N-PROPYLBENZENE 3.3730 3.6930 3.6180 4.1540 4.70 4.3430 4.3010 4.4440
2-CHLOROTOLUENE 2.6370 2.6440 2.8310 3.0330 3.2360 2.9080 2.8630 2.8640
4-CHLOROTOLUENE 2.5680 2.3310 2.6070 2.8260 3.0860 2.8650 2.8720 2.9610
1,3,5-TRIMETHYLBENZENE 2.3150 2.2070 2.53 2.9420 3.2840 3.0110 2.96 2.92
TERT-BUTYLBENZENE 1.7970 1.8570 1.9750 2.3230 2.6720 2.4830 2.3940 2.3760
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 404 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 09/22/24
17:10
09/22/24
17:32
09/22/24
17:54
09/22/24
18:16
09/22/24
18:38
09/22/24
19:00
09/22/24
19:22
09/22/24
19:44
1,2,4-TRIMETHYLBENZENE 2.6150 2.3390 2.6520 2.9730 3.4270 3.1910 3.1610 3.1670
SEC-BUTYLBENZENE 2.2380 2.5710 2.84 3.1940 3.5590 3.3530 3.2330 3.2930
1,3-DICHLOROBENZENE 1.5370 1.5420 1.5530 1.6490 1.7790 1.6280 1.6520 1.6710
P-ISOPROPYLTOLUENE 1.7970 2.1410 2.3880 2.8220 3.1790 2.9590 2.8680 2.92
1,4-DICHLOROBENZENE 1.6120 1.5370 1.5890 1.7030 1.7910 1.66 1.6590 1.6940
1,2,3-TRIMETHYLBENZENE 2.9730 2.6310 2.7650 2.9610 3.3140 3.0350 3.04 3.0250
1,2-DICHLOROBENZENE 1.5710 1.3350 1.5330 1.58 1.6770 1.5690 1.5890 1.6040
N-BUTYLBENZENE 1.5390 1.7820 1.8610 2.2290 2.4990 2.3630 2.2730 2.4210
1,2,4-TRICHLOROBENZENE 0.7480 0.5210 0.6950 0.6740 0.7590 0.7360 0.7490 0.8920
HEXACHLORO-1,3-BUTADIENE 0.2640 0.2270 0.2440 0.31 0.3130 0.2840 0.2630 0.3580
1,2,3-TRICHLOROBENZENE 0.61 0.5010 0.63 0.6280 0.6740 0.6250 0.6890 0.8420
1,2-DICHLOROETHANE-D4 0.3260 0.3370 0.3330 0.3460 0.3610 0.42 0.3540 0.3460
TOLUENE-D8 2.3390 2.3030 2.3550 2.3380 2.2480 2.3750 2.3480 2.3590
4-BROMOFLUOROBENZENE 0.77 0.7630 0.80 0.7630 0.7840 0.8290 0.8440 0.8160
DICHLORODIFLUOROMETHANE 0.3660 0.4170 0.4750 0.51 0.4730 0.4130 0.4190
CHLOROMETHANE 0.4430 0.5140 0.5790 0.6210 0.5580 0.5130 0.5340
ACETONE 0.2250 0.2280 0.2190 0.2090 0.2030 0.1920
1,2-DIBROMO-3-CHLOROPROPANE 0.2610 0.3270 0.3040 0.3520 0.3440 0.3640 0.3520
NAPHTHALENE 1.9710 2.3130 2.3120 2.9390 2.9480 3.1470
TRICHLOROFLUOROMETHANE 0.2870 0.4010 0.4490 0.4390 0.3970 0.4250
File ID:0922_09 0922_10 0922_11 0922_12 0922_13 0922_14 0922_15 0922_16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 405 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF. Avg %RSD COD
Analysis date/time
VINYL CHLORIDE 0.326285 23.8 0.997
BROMOMETHANE 0.163366 12.91
CHLOROETHANE 0.18953 12.13
ACROLEIN 0.084458 11.66
1,1-DICHLOROETHENE 0.268947 15.33
1,1,2-TRICHLOROTRIFLUOROETHANE 0.244519 24.5 0.998
METHYLENE CHLORIDE 0.321035 8.88
ACRYLONITRILE 0.278354 9.57
TRANS-1,2-DICHLOROETHENE 0.302556 7.11
METHYL TERT-BUTYL ETHER 1.025657 3.9
1,1-DICHLOROETHANE 0.651085 5.65
DI-ISOPROPYL ETHER 1.474766 4.19
2,2-DICHLOROPROPANE 0.203557 17.02 0.997
CIS-1,2-DICHLOROETHENE 0.334984 5.6
2-BUTANONE (MEK)0.392902 8.32
CHLOROFORM 0.592765 3.72
1,1,1-TRICHLOROETHANE 0.452589 16.26 0.998
CARBON TETRACHLORIDE 0.452522 14.71
1,1-DICHLOROPROPENE 0.392634 14.5
BENZENE 1.316981 2.94
1,2-DICHLOROETHANE 0.527112 7.16
TRICHLOROETHENE 0.31529 9.28
1,2-DICHLOROPROPANE 0.280321 7
DIBROMOMETHANE 0.196511 5.69
BROMODICHLOROMETHANE 0.444113 4.69
CIS-1,3-DICHLOROPROPENE 0.523849 6.29
4-METHYL-2-PENTANONE (MIBK)1.649593 5.49
TOLUENE 3.220154 3.52
TRANS-1,3-DICHLOROPROPENE 1.188654 5.49
1,1,2-TRICHLOROETHANE 0.715309 2.3
TETRACHLOROETHENE 0.521817 10.92
1,3-DICHLOROPROPANE 1.271896 3.29
CHLORODIBROMOMETHANE 0.789395 3.83
1,2-DIBROMOETHANE 0.745263 3.87
CHLOROBENZENE 1.972298 4.96
1,1,1,2-TETRACHLOROETHANE 0.688789 6.7
ETHYLBENZENE 1.002526 7.16
M&P-XYLENE 1.212176 7.84
O-XYLENE 1.179372 7.03
STYRENE 1.966524 11.23
BROMOFORM 0.51852 9.23
ISOPROPYLBENZENE 2.718978 12.44
BROMOBENZENE 1.831992 3.41
1,1,2,2-TETRACHLOROETHANE 1.356469 6.01
1,2,3-TRICHLOROPROPANE 0.464807 7.3
N-PROPYLBENZENE 4.078355 11.36
2-CHLOROTOLUENE 2.876765 6.81
4-CHLOROTOLUENE 2.764345 8.85
1,3,5-TRIMETHYLBENZENE 2.771371 13.58
TERT-BUTYLBENZENE 2.234499 14.22
1,2,4-TRIMETHYLBENZENE 2.940738 12.54
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 406 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF. Avg %RSD COD
Analysis date/time
SEC-BUTYLBENZENE 3.03506 14.7
1,3-DICHLOROBENZENE 1.626495 5.03
P-ISOPROPYLTOLUENE 2.634126 18.03 0.999
1,4-DICHLOROBENZENE 1.655608 4.72
1,2,3-TRIMETHYLBENZENE 2.968035 6.84
1,2-DICHLOROBENZENE 1.557143 6.34
N-BUTYLBENZENE 2.120771 16.41 0.999
1,2,4-TRICHLOROBENZENE 0.721617 14.38
HEXACHLORO-1,3-BUTADIENE 0.282892 14.98
1,2,3-TRICHLOROBENZENE 0.649952 14.71
1,2-DICHLOROETHANE-D4 0.35297 8.29
TOLUENE-D8 2.333081 1.72
4-BROMOFLUOROBENZENE 0.796137 3.9
DICHLORODIFLUOROMETHANE 0.439284 11.17
CHLOROMETHANE 0.537364 10.5
ACETONE 0.212553 6.45
1,2-DIBROMO-3-CHLOROPROPANE 0.329343 10.91
NAPHTHALENE 2.604989 17.97 0.998
TRICHLOROFLUOROMETHANE 0.399803 14.7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 407 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS36
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 09/12/24
18:56
09/12/24
19:17
09/12/24
19:38
09/12/24
19:58
09/12/24
20:19
09/12/24
20:40
09/12/24
21:00
09/12/24
21:21
DICHLORODIFLUOROMETHANE 0.2530 0.3440 0.3250 0.3120 0.3930 0.3960 0.3950 0.38
CHLOROMETHANE 0.7910 0.7580 0.7620 0.77 0.8170 0.7880 0.8210 0.7860
VINYL CHLORIDE 0.3380 0.40 0.3720 0.38 0.4220 0.42 0.4370 0.4320
CHLOROETHANE 0.1970 0.2130 0.2110 0.2080 0.2050 0.1940 0.1990 0.1610
ACROLEIN 0.0610 0.0520 0.0550 0.0540 0.0590 0.0590 0.0620 0.0610
1,1-DICHLOROETHENE 0.1790 0.2280 0.2020 0.2080 0.2240 0.2210 0.2320 0.2310
1,1,2-TRICHLOROTRIFLUOROETHANE 0.1360 0.2110 0.1840 0.1820 0.2210 0.2260 0.2270 0.2290
ACETONE 0.11 0.0950 0.0990 0.0950 0.0970 0.0970 0.0950 0.0960
METHYLENE CHLORIDE 0.3140 0.2540 0.2860 0.2640 0.2660 0.2550 0.2750 0.27
ACRYLONITRILE 0.1220 0.1260 0.1290 0.13 0.1360 0.1360 0.14 0.1390
TRANS-1,2-DICHLOROETHENE 0.2180 0.24 0.2420 0.2420 0.2420 0.2330 0.25 0.2430
METHYL TERT-BUTYL ETHER 0.7580 0.7470 0.7970 0.7710 0.7810 0.7660 0.7850 0.7850
1,1-DICHLOROETHANE 0.4830 0.5070 0.5190 0.5130 0.5450 0.52 0.5480 0.54
DI-ISOPROPYL ETHER 1.0090 1.0790 1.0810 1.0650 1.1080 1.0720 1.11 1.0790
2,2-DICHLOROPROPANE 0.3630 0.3710 0.3720 0.3720 0.3710 0.3710 0.3680 0.3610
CIS-1,2-DICHLOROETHENE 0.2330 0.2570 0.2680 0.25 0.2740 0.2720 0.2840 0.2690
2-BUTANONE (MEK)0.1260 0.1120 0.1340 0.1370 0.1510 0.1490 0.1540 0.1560
CHLOROFORM 0.4570 0.4960 0.4740 0.4760 0.4780 0.4760 0.4970 0.4870
1,1,1-TRICHLOROETHANE 0.3540 0.3880 0.3880 0.3790 0.4120 0.4110 0.4290 0.4220
CARBON TETRACHLORIDE 0.2690 0.3440 0.3310 0.3460 0.3920 0.3840 0.4030 0.3980
1,1-DICHLOROPROPENE 0.2650 0.3040 0.2890 0.3130 0.3440 0.33 0.3450 0.3420
BENZENE 0.98 0.9650 0.9870 0.99 1.0390 1.0170 1.0570 1.0510
1,2-DICHLOROETHANE 0.4320 0.4390 0.4240 0.42 0.4340 0.4170 0.4280 0.4330
TRICHLOROETHENE 0.2260 0.2460 0.2440 0.2480 0.2650 0.26 0.2710 0.2690
1,2-DICHLOROPROPANE 0.2090 0.2140 0.2240 0.2260 0.2320 0.2250 0.2410 0.2370
DIBROMOMETHANE 0.1640 0.1560 0.17 0.1650 0.1750 0.1730 0.1780 0.1780
BROMODICHLOROMETHANE 0.3450 0.3620 0.3520 0.3680 0.3770 0.3710 0.3910 0.3870
CIS-1,3-DICHLOROPROPENE 0.4060 0.4010 0.4320 0.4250 0.4520 0.4440 0.4620 0.4550
4-METHYL-2-PENTANONE (MIBK)0.68 0.7050 0.6990 0.7160 0.7360 0.7510 0.7260 0.6980
TOLUENE 2.2030 2.3390 2.2890 2.2820 2.2990 2.3480 2.3460 2.2890
TRANS-1,3-DICHLOROPROPENE 0.7460 0.8190 0.7650 0.86 0.89 0.9210 0.9190 0.8920
1,1,2-TRICHLOROETHANE 0.5480 0.48 0.5580 0.54 0.5160 0.5350 0.5270 0.5190
TETRACHLOROETHENE 0.4180 0.4620 0.4440 0.4550 0.4810 0.4840 0.4780 0.4690
1,3-DICHLOROPROPANE 0.8860 0.9510 0.9060 0.9180 0.9110 0.9380 0.9380 0.9110
CHLORODIBROMOMETHANE 0.6190 0.5640 0.5870 0.6060 0.6050 0.6470 0.64 0.65
1,2-DIBROMOETHANE 0.6070 0.5260 0.5530 0.5390 0.5530 0.5570 0.5630 0.5550
CHLOROBENZENE 1.4390 1.4740 1.4720 1.4620 1.4570 1.5020 1.5090 1.4510
1,1,1,2-TETRACHLOROETHANE 0.4980 0.5230 0.5040 0.5270 0.5310 0.55 0.5490 0.5370
ETHYLBENZENE 0.8130 0.7790 0.7650 0.7830 0.7990 0.8310 0.8230 0.8020
M&P-XYLENE 0.8940 0.9440 0.94 0.9240 0.9680 1 0.9870 0.9580
O-XYLENE 0.9490 0.9190 0.9240 0.9410 0.9480 0.9990 0.9980 0.9780
STYRENE 1.5980 1.3690 1.4810 1.5720 1.6350 1.7260 1.7140 1.6490
BROMOFORM 0.3930 0.4320 0.4260 0.4490 0.4640 0.49 0.4960 0.4910
ISOPROPYLBENZENE 2.3320 2.4280 2.3350 2.2990 2.3830 2.5370 2.5130 2.4350
BROMOBENZENE 1.3240 1.3020 1.2050 1.2490 1.2770 1.2380 1.2590 1.33
1,1,2,2-TETRACHLOROETHANE 0.8370 0.7750 0.7760 0.7570 0.7520 0.71 0.74 0.7550
1,2,3-TRICHLOROPROPANE 0.21 0.2360 0.2230 0.2260 0.2220 0.2140 0.2190 0.2250
N-PROPYLBENZENE 3.1030 3.0860 3.0220 3.0420 3.2180 3.1030 3.1610 3.32
2-CHLOROTOLUENE 2.0180 1.8960 2.0550 2.0840 2.1360 2.0980 2.1430 2.1940
4-CHLOROTOLUENE 1.8090 1.8420 1.8780 1.9040 2.0210 2.0010 2.0610 2.0770
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 408 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS36
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 09/12/24
18:56
09/12/24
19:17
09/12/24
19:38
09/12/24
19:58
09/12/24
20:19
09/12/24
20:40
09/12/24
21:00
09/12/24
21:21
1,3,5-TRIMETHYLBENZENE 2.22 2.0850 2.0710 2.1460 2.2330 2.1780 2.2190 2.2530
TERT-BUTYLBENZENE 1.6370 1.7990 1.7110 1.7010 1.8170 1.7540 1.7490 1.8320
1,2,4-TRIMETHYLBENZENE 2.2710 2.3170 2.2140 2.2140 2.3510 2.2710 2.2760 2.3610
SEC-BUTYLBENZENE 2.2340 2.33 2.2730 2.3730 2.5320 2.5050 2.5350 2.5850
1,3-DICHLOROBENZENE 1.1780 1.1750 1.1570 1.2110 1.2890 1.2610 1.2940 1.3140
P-ISOPROPYLTOLUENE 2.0150 2.1180 2.0620 2.0690 2.2320 2.1730 2.2150 2.2340
1,4-DICHLOROBENZENE 1.2250 1.3160 1.2840 1.2470 1.3060 1.2850 1.2840 1.3110
1,2,3-TRIMETHYLBENZENE 2.3610 2.29 2.3380 2.2850 2.3060 2.2390 2.2840 2.2960
1,2-DICHLOROBENZENE 1.16 1.1970 1.1830 1.1920 1.2470 1.2280 1.2470 1.2760
N-BUTYLBENZENE 1.6830 1.98 1.8070 1.7360 1.9050 1.8380 1.8730 1.9380
1,2,4-TRICHLOROBENZENE 0.5640 0.5180 0.5520 0.6120 0.6710 0.6770 0.6990 0.7130
HEXACHLORO-1,3-BUTADIENE 0.2540 0.2770 0.2850 0.3040 0.31 0.2990 0.2930 0.3020
1,2,3-TRICHLOROBENZENE 0.4480 0.3930 0.4540 0.4640 0.5070 0.5220 0.5380 0.5440
1,2-DICHLOROETHANE-D4 0.3520 0.3480 0.37 0.3530 0.3640 0.3360 0.3590 0.3410
TOLUENE-D8 2.2620 2.2440 2.1950 2.1520 2.0810 2.2240 2.1910 2.0820
4-BROMOFLUOROBENZENE 0.8930 0.8830 0.8540 0.8560 0.8340 0.9220 0.9120 0.8420
BROMOMETHANE 0.0850 0.0760 0.0640 0.0620 0.0660 0.0760 0.0780
TRICHLOROFLUOROMETHANE 0.3560 0.3470 0.3530 0.4460 0.43 0.4390 0.4290
1,2-DIBROMO-3-CHLOROPROPANE 0.1270 0.1230 0.1210 0.1460 0.1480 0.1520 0.1580
File ID:0912_08 0912_09 0912_10 0912_11 0912_12 0912_13 0912_14 0912_15
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 409 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS36
Analyte RRF. Avg %RSD COD
Analysis date/time
DICHLORODIFLUOROMETHANE 0.349605 14.67
CHLOROMETHANE 0.786618 2.98
VINYL CHLORIDE 0.400016 8.55
CHLOROETHANE 0.198396 8.43
ACROLEIN 0.057784 6.15
1,1-DICHLOROETHENE 0.215678 8.5
1,1,2-TRICHLOROTRIFLUOROETHANE 0.202287 16.16 1
ACETONE 0.097906 5.18
METHYLENE CHLORIDE 0.272985 7.15
ACRYLONITRILE 0.132139 4.99
TRANS-1,2-DICHLOROETHENE 0.238768 3.99
METHYL TERT-BUTYL ETHER 0.773773 2.13
1,1-DICHLOROETHANE 0.521612 4.19
DI-ISOPROPYL ETHER 1.075257 2.92
2,2-DICHLOROPROPANE 0.368685 1.17
CIS-1,2-DICHLOROETHENE 0.263482 6.16
2-BUTANONE (MEK)0.139779 11.07
CHLOROFORM 0.480073 2.71
1,1,1-TRICHLOROETHANE 0.397925 6.31
CARBON TETRACHLORIDE 0.358308 12.63
1,1-DICHLOROPROPENE 0.316672 9.2
BENZENE 1.010804 3.48
1,2-DICHLOROETHANE 0.428278 1.75
TRICHLOROETHENE 0.253669 5.99
1,2-DICHLOROPROPANE 0.225933 4.87
DIBROMOMETHANE 0.169932 4.56
BROMODICHLOROMETHANE 0.369064 4.33
CIS-1,3-DICHLOROPROPENE 0.434567 5.24
4-METHYL-2-PENTANONE (MIBK)0.71406 3.25
TOLUENE 2.299271 2.08
TRANS-1,3-DICHLOROPROPENE 0.851531 7.98
1,1,2-TRICHLOROETHANE 0.528049 4.5
TETRACHLOROETHENE 0.46159 4.82
1,3-DICHLOROPROPANE 0.919659 2.29
CHLORODIBROMOMETHANE 0.614624 4.95
1,2-DIBROMOETHANE 0.556511 4.17
CHLOROBENZENE 1.470714 1.64
1,1,1,2-TETRACHLOROETHANE 0.527456 3.57
ETHYLBENZENE 0.799111 2.85
M&P-XYLENE 0.951884 3.58
O-XYLENE 0.956971 3.28
STYRENE 1.593142 7.52
BROMOFORM 0.455168 8.12
ISOPROPYLBENZENE 2.407659 3.6
BROMOBENZENE 1.272924 3.41
1,1,2,2-TETRACHLOROETHANE 0.76275 4.8
1,2,3-TRICHLOROPROPANE 0.221729 3.63
N-PROPYLBENZENE 3.131754 3.14
2-CHLOROTOLUENE 2.077852 4.41
4-CHLOROTOLUENE 1.948999 5.3
1,3,5-TRIMETHYLBENZENE 2.175434 3.16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 410 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS36
Analyte RRF. Avg %RSD COD
Analysis date/time
TERT-BUTYLBENZENE 1.749995 3.76
1,2,4-TRIMETHYLBENZENE 2.284274 2.43
SEC-BUTYLBENZENE 2.421009 5.56
1,3-DICHLOROBENZENE 1.234858 5.03
P-ISOPROPYLTOLUENE 2.139802 4
1,4-DICHLOROBENZENE 1.282226 2.47
1,2,3-TRIMETHYLBENZENE 2.299797 1.6
1,2-DICHLOROBENZENE 1.216427 3.22
N-BUTYLBENZENE 1.844892 5.45
1,2,4-TRICHLOROBENZENE 0.625757 11.88
HEXACHLORO-1,3-BUTADIENE 0.290731 6.31
1,2,3-TRICHLOROBENZENE 0.483839 10.89
1,2-DICHLOROETHANE-D4 0.352716 3.19
TOLUENE-D8 2.178867 3.16
4-BROMOFLUOROBENZENE 0.874532 3.77
BROMOMETHANE 0.072201 11.87
TRICHLOROFLUOROMETHANE 0.39991 11.28
1,2-DIBROMO-3-CHLOROPROPANE 0.139259 10.99
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 411 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS42
Analyte RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 0.02 RRF: 0.04 RRF: 0.1 RRF: 0.2
Analysis date/time 10/03/24
17:01
10/03/24
17:21
10/03/24
17:41
10/03/24
18:01
10/03/24
18:21
10/03/24
18:40
10/03/24
15:22
10/03/24
15:42
10/03/24
16:02
10/03/24
16:21
NAPHTHALENE 1.3510 1.3930 1.9520 2.5310 2.0490 2.0380
1,2-DICHLOROETHANE-D4 0.3140 0.3060 0.3190 0.3220 0.2510 0.2590 0.3120 0.33 0.3220 0.3040
TOLUENE-D8 2.3180 2.3020 2.2510 2.1760 2.0010 1.9420 2.3020 2.2850 2.3630 2.3480
4-BROMOFLUOROBENZENE 0.8360 0.8580 0.8490 0.84 0.7610 0.7410 0.8270 0.8340 0.8340 0.8220
File ID:1003A_09 1003A_10 1003A_11 1003A_12 1003A_13 1003A_14 1003A_04 1003A_05 1003A_06 1003A_07
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 412 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS42
Analyte RRF: 0.5 RRF. Avg %RSD COD
Analysis date/time 10/03/24
16:41
NAPHTHALENE 1.886 23.72 0.993
1,2-DICHLOROETHANE-D4 0.3210 0.305 8.55
TOLUENE-D8 2.3680 2.241 6.45
4-BROMOFLUOROBENZENE 0.8480 0.823 4.54
File ID:1003A_08
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 413 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF: 0.02 RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 10/08/24
22:49
10/08/24
23:08
10/08/24
23:27
10/08/24
23:46
10/09/24
00:04
10/09/24
00:42
10/09/24
01:01
10/09/24
01:20
10/09/24
01:39
10/09/24
01:58
1,1-DICHLOROETHANE 0.4760 0.5680 0.5260 0.6160 0.5610 0.61 0.5970 0.63 0.5670 0.6060
CHLOROFORM 0.7120 0.8340 0.6870 0.6890 0.6640 0.7160 0.6910 0.7310 0.6930 0.7170
CHLOROBENZENE 1.5170 1.5820 1.6340 1.5090 1.6270 1.6150 1.5720 1.5180 1.5440 1.5610
1,2-DICHLOROETHANE-D4 0.3220 0.3280 0.3310 0.32 0.3270 0.3290 0.3330 0.37 0.4040 0.4290
TOLUENE-D8 1.9130 1.9170 1.9640 1.9750 1.94 1.9290 1.8470 1.6590 1.7190 1.6810
4-BROMOFLUOROBENZENE 0.9490 0.9470 0.9240 0.9020 0.9420 0.9310 0.9060 0.8520 0.8590 0.8460
CHLOROMETHANE 0.6550 0.70 0.6430 0.6380 0.6080 0.6080 0.6110 0.5190 0.5370
CHLOROETHANE 0.2720 0.25 0.2950 0.2770 0.2730 0.2820 0.3120 0.2730 0.2970
1,1-DICHLOROETHENE 0.5650 0.5360 0.4630 0.4570 0.4720 0.5420 0.5680 0.4970 0.5270
ACRYLONITRILE 0.1250 0.1170 0.1290 0.1430 0.1290 0.1440 0.1610 0.1480 0.15
METHYL TERT-BUTYL ETHER 0.6770 0.9190 0.8520 0.8780 0.9360 0.9350 1.0080 0.9120 0.9840
DI-ISOPROPYL ETHER 0.6430 0.7630 0.8380 0.8130 0.8870 0.85 0.97 0.8820 0.9540
2,2-DICHLOROPROPANE 0.5240 0.45 0.4430 0.5060 0.4370 0.4790 0.5080 0.4540 0.4810
CIS-1,2-DICHLOROETHENE 0.3230 0.28 0.4080 0.39 0.4110 0.3960 0.4310 0.3910 0.4120
CARBON TETRACHLORIDE 0.5310 0.6190 0.5570 0.5820 0.5580 0.6490 0.6910 0.6270 0.6380
1,1-DICHLOROPROPENE 0.5230 0.5410 0.4320 0.3990 0.4080 0.4540 0.4810 0.4470 0.4530
BENZENE 1.3510 1.1670 1.2790 1.3410 1.27 1.2620 1.3830 1.2750 1.29
TRICHLOROETHENE 0.2860 0.2660 0.3940 0.37 0.3660 0.3790 0.4090 0.3790 0.38
BROMODICHLOROMETHANE 0.4840 0.36 0.4630 0.4690 0.4790 0.4860 0.5290 0.5040 0.5180
CIS-1,3-DICHLOROPROPENE 0.4780 0.32 0.4670 0.4260 0.4620 0.4850 0.5420
TOLUENE 2.7030 2.1530 2.3480 2.2230 2.4040 2.3380 2.20 2.2550 2.1880
1,2-DIBROMOETHANE 0.5960 0.4610 0.4890 0.5160 0.5580 0.5610 0.5440 0.56 0.56
1,1,1,2-TETRACHLOROETHANE 0.4970 0.5330 0.6040 0.5730 0.5840 0.5690 0.5570 0.5430 0.55
M&P-XYLENE 0.5890 0.8090 0.8820 0.9430 0.9950 1.0220 1.0120 0.9980 0.9940
ISOPROPYLBENZENE 2.1720 2.09 2.2270 2.0090 2.3650 2.4490 2.5050 2.4210 2.3940
BROMOBENZENE 0.6070 0.60 0.6470 0.6560 0.7080 0.6840 0.6580 0.6460 0.6730
1,4-DICHLOROBENZENE 0.90 1.1560 1.2590 1.0540 1.14 1.0840 1.08 1.06 1.1040
1,2,3-TRIMETHYLBENZENE 1.6270 1.6010 1.8210 1.6780 1.8460 1.8640 1.9430 1.8750 1.9290
DICHLORODIFLUOROMETHANE 0.4440 0.3460 0.4690 0.4340 0.5480 0.5610 0.4620 0.47
VINYL CHLORIDE 0.40 0.4620 0.4970 0.4610 0.5180 0.5340 0.4850 0.5020
BROMOMETHANE 0.4760 0.4390 0.4090 0.4160 0.4330 0.5170 0.4430 0.4450
TRICHLOROFLUOROMETHANE 0.5530 0.6320 0.6310 0.6280 0.7150 0.7710 0.6950 0.7370
1,1,2-TRICHLOROTRIFLUOROETHANE 0.3020 0.25 0.3420 0.3210 0.37 0.3960 0.3430 0.3550
TRANS-1,2-DICHLOROETHENE 0.3570 0.3190 0.3260 0.3720 0.3720 0.3990 0.3490 0.3720
1,1,1-TRICHLOROETHANE 0.5080 0.5110 0.5870 0.5810 0.6380 0.6740 0.61 0.6270
1,2-DICHLOROETHANE 0.6390 0.5160 0.5160 0.4790 0.4620 0.5080 0.4850 0.4980
1,2-DICHLOROPROPANE 0.3020 0.3040 0.2840 0.3040 0.3320 0.3430 0.33 0.3320
DIBROMOMETHANE 0.1940 0.2410 0.2330 0.2490 0.2360 0.2590 0.2420 0.2540
4-METHYL-2-PENTANONE (MIBK)0.5580 0.5720 0.6020 0.6110 0.6750 0.6780 0.6850 0.6470
TRANS-1,3-DICHLOROPROPENE 0.6130 0.6950 0.7380 0.7990 0.7870 0.81 0.8920 0.8980
1,1,2-TRICHLOROETHANE 0.58 0.6430 0.51 0.5490 0.5230 0.4960 0.5070 0.5080
TETRACHLOROETHENE 0.4380 0.5670 0.4990 0.4740 0.51 0.4870 0.4930 0.4830
1,3-DICHLOROPROPANE 0.83 0.9140 0.8410 0.86 0.8450 0.7960 0.8240 0.8160
CHLORODIBROMOMETHANE 0.5650 0.4940 0.6330 0.6140 0.6110 0.6060 0.6280 0.6310
ETHYLBENZENE 0.4590 0.7480 0.8140 0.8330 0.8450 0.8290 0.8480 0.8440
O-XYLENE 0.6640 0.9080 0.8230 0.9610 0.9680 0.9780 0.9680 0.9890
BROMOFORM 0.3760 0.4590 0.4080 0.4560 0.4740 0.5150 0.5270 0.54
1,1,2,2-TETRACHLOROETHANE 0.8340 0.8720 0.8390 0.8530 0.8390 0.8240 0.8030 0.82
N-PROPYLBENZENE 2.5380 2.8740 2.4920 2.6780 2.7890 2.7840 2.63 2.6270
2-CHLOROTOLUENE 0.2830 0.58 0.4610 0.6010 0.6120 0.5990 0.5780 0.6190
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 414 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF: 0.02 RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 10/08/24
22:49
10/08/24
23:08
10/08/24
23:27
10/08/24
23:46
10/09/24
00:04
10/09/24
00:42
10/09/24
01:01
10/09/24
01:20
10/09/24
01:39
10/09/24
01:58
4-CHLOROTOLUENE 1.5420 1.27 1.40 1.6440 1.6840 1.7010 1.67 1.7340
1,3,5-TRIMETHYLBENZENE 2.0270 1.73 1.6510 1.8230 1.9470 1.9450 1.8920 1.9270
TERT-BUTYLBENZENE 1.32 1.2640 1.1940 1.3020 1.4570 1.4780 1.4250 1.4790
1,2,4-TRIMETHYLBENZENE 1.3220 1.57 1.4630 1.7350 1.86 1.8970 1.8570 1.8960
SEC-BUTYLBENZENE 1.7330 1.67 1.9460 1.8330 2.1040 2.1360 2.0260 2.0730
1,3-DICHLOROBENZENE 1.0670 0.9930 0.9450 0.9910 1.05 1.0690 1.01 1.0590
1,2-DICHLOROBENZENE 1.1970 0.9930 0.8220 0.9980 0.9790 0.9870 0.9440 0.9920
N-BUTYLBENZENE 1.0670 1.1830 1.1540 1.2630 1.3830 1.5090 1.4740 1.4950
ACETONE 0.0970 0.0870 0.0780 0.0980 0.0990
STYRENE 1.1680 1.2530 1.5360 1.5590 1.6490 1.6790 1.6860
1,2,3-TRICHLOROPROPANE 0.2470 0.2440 0.2470 0.2780 0.2620 0.2530 0.2620
P-ISOPROPYLTOLUENE 1.21 1.2840 1.5390 1.7720 1.8420 1.7730 1.8220
1,2,4-TRICHLOROBENZENE 0.3090 0.2510 0.3090 0.3080 0.38 0.3490 0.3520
METHYLENE CHLORIDE 0.3910 0.4160 0.39 0.3850 0.3390 0.3660
2-BUTANONE (MEK)0.1060 0.1380 0.1710 0.1840 0.1840 0.1760
1,2-DIBROMO-3-CHLOROPROPANE 0.1230 0.1470 0.1630 0.18 0.18 0.1840
HEXACHLORO-1,3-BUTADIENE 0.1960 0.1850 0.20 0.2020 0.1820 0.18
NAPHTHALENE 0.7440 0.8680 0.8970 1.2130 1.2130
1,2,3-TRICHLOROBENZENE 0.1920 0.2970 0.2630 0.3170 0.2940 0.2940
File ID:1008A_14 1008A_15 1008A_16 1008A_17 1008A_18 1008A_20 1008A_21 1008A_22 1008A_23 1008A_24
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 415 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF. Avg %RSD COD
Analysis date/time
1,1-DICHLOROETHANE 0.576 8.17
CHLOROFORM 0.713 6.53
CHLOROBENZENE 1.568 2.97
1,2-DICHLOROETHANE-D4 0.349 11
TOLUENE-D8 1.854 6.57
4-BROMOFLUOROBENZENE 0.906 4.42
CHLOROMETHANE 0.613 9.2
CHLOROETHANE 0.281 6.39
1,1-DICHLOROETHENE 0.514 8.4
ACRYLONITRILE 0.138 10.25
METHYL TERT-BUTYL ETHER 0.9 10.71
DI-ISOPROPYL ETHER 0.844 11.78
2,2-DICHLOROPROPANE 0.476 6.65
CIS-1,2-DICHLOROETHENE 0.382 12.78
CARBON TETRACHLORIDE 0.606 8.58
1,1-DICHLOROPROPENE 0.46 10.45
BENZENE 1.291 4.87
TRICHLOROETHENE 0.359 13.61
BROMODICHLOROMETHANE 0.477 10.23
CIS-1,3-DICHLOROPROPENE 0.454 15.07
TOLUENE 2.312 7.3
1,2-DIBROMOETHANE 0.538 7.8
1,1,1,2-TETRACHLOROETHANE 0.557 5.62
M&P-XYLENE 0.916 15.42
ISOPROPYLBENZENE 2.292 7.58
BROMOBENZENE 0.653 5.25
1,4-DICHLOROBENZENE 1.093 8.8
1,2,3-TRIMETHYLBENZENE 1.798 7.19
DICHLORODIFLUOROMETHANE 0.467 14.38
VINYL CHLORIDE 0.482 8.68
BROMOMETHANE 0.447 7.74
TRICHLOROFLUOROMETHANE 0.67 10.65
1,1,2-TRICHLOROTRIFLUOROETHANE 0.335 13.38
TRANS-1,2-DICHLOROETHENE 0.358 7.38
1,1,1-TRICHLOROETHANE 0.592 9.91
1,2-DICHLOROETHANE 0.513 10.57
1,2-DICHLOROPROPANE 0.316 6.52
DIBROMOMETHANE 0.238 8.43
4-METHYL-2-PENTANONE (MIBK)0.629 7.9
TRANS-1,3-DICHLOROPROPENE 0.779 12.31
1,1,2-TRICHLOROETHANE 0.54 9.29
TETRACHLOROETHENE 0.494 7.37
1,3-DICHLOROPROPANE 0.841 4.21
CHLORODIBROMOMETHANE 0.598 7.88
ETHYLBENZENE 0.778 17.09 1
O-XYLENE 0.907 12.38
BROMOFORM 0.469 12.26
1,1,2,2-TETRACHLOROETHANE 0.835 2.54
N-PROPYLBENZENE 2.677 4.9
2-CHLOROTOLUENE 0.542 21.39 0.999
4-CHLOROTOLUENE 1.58 10.47
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 416 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS56
Analyte RRF. Avg %RSD COD
Analysis date/time
1,3,5-TRIMETHYLBENZENE 1.868 6.7
TERT-BUTYLBENZENE 1.365 8
1,2,4-TRIMETHYLBENZENE 1.7 13.06
SEC-BUTYLBENZENE 1.94 9.08
1,3-DICHLOROBENZENE 1.023 4.43
1,2-DICHLOROBENZENE 0.989 10.35
N-BUTYLBENZENE 1.316 13.08
ACETONE 0.092 9.79
STYRENE 1.504 13.97
1,2,3-TRICHLOROPROPANE 0.256 4.64
P-ISOPROPYLTOLUENE 1.606 16.52 1
1,2,4-TRICHLOROBENZENE 0.322 13.02
METHYLENE CHLORIDE 0.381 6.83
2-BUTANONE (MEK)0.16 19.68 0.999
1,2-DIBROMO-3-CHLOROPROPANE 0.163 14.7
HEXACHLORO-1,3-BUTADIENE 0.191 5.1
NAPHTHALENE 0.987 21.68 0.997
1,2,3-TRICHLOROBENZENE 0.276 16.15 0.999
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 417 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS59
Analyte RRF: 0.02 RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75
Analysis date/time 10/07/24
18:03
10/07/24
18:23
10/07/24
18:43
10/07/24
19:02
10/07/24
19:22
10/07/24
19:42
10/07/24
20:01
10/07/24
20:21
10/07/24
20:40
10/07/24
20:59
1,1-DICHLOROETHENE 0.5620 0.6560 0.6240 0.4990 0.5240 0.5570 0.5890 0.65 0.6760 0.62
ACRYLONITRILE 0.2380 0.2550 0.2960 0.2970 0.29 0.2880 0.3280 0.2950 0.3150 0.2760
CIS-1,3-DICHLOROPROPENE 0.5630 0.7020 0.59 0.5870 0.52 0.5120 0.6120 0.5440 0.5740 0.5890
4-METHYL-2-PENTANONE (MIBK)1.5290 1.7080 1.8850 1.68 1.6310 1.5720 1.8880 1.6160 1.5970 1.5830
CHLOROBENZENE 2.24 2.3660 2.0770 1.9770 1.9250 2.0160 2.3010 2.0580 2.0190 2.0930
1,3-DICHLOROBENZENE 1.5580 1.6960 1.77 1.7350 1.61 1.56 1.9420 1.7060 1.7930 1.8170
1,2-DICHLOROETHANE-D4 0.3210 0.3310 0.3240 0.3190 0.3290 0.33 0.3340 0.3450 0.3560 0.3950
TOLUENE-D8 2.1820 2.1490 2.2120 2.1820 2.2010 2.1540 2.1820 2.13 2.0130 2.1320
4-BROMOFLUOROBENZENE 0.9020 0.9230 0.9560 0.9040 0.9660 0.9280 0.9210 0.9270 0.8830 0.9450
METHYL TERT-BUTYL ETHER 1.3680 0.9190 0.8770 0.9740 1.02 1.1240 1.0540 1.1010 0.9280
DI-ISOPROPYL ETHER 1.8450 1.7150 1.5060 1.5590 1.4410 1.7380 1.58 1.6380 1.5270
BENZENE 1.4780 1.7320 1.3770 1.3220 1.3230 1.4810 1.3190 1.3960 1.34
TRICHLOROETHENE 0.36 0.3540 0.3350 0.3150 0.3060 0.3680 0.3360 0.3570 0.3530
1,2-DIBROMOETHANE 0.7990 1.0390 0.9190 0.8410 0.7480 0.94 0.8170 0.8230 0.8680
M&P-XYLENE 1.5210 1.6140 1.4820 1.2280 1.2520 1.4770 1.3250 1.3010 1.3560
N-PROPYLBENZENE 4.6780 4.9260 4.4140 3.8140 3.90 4.9260 4.3010 4.5050 4.5920
4-CHLOROTOLUENE 3.4710 2.7210 3.0060 2.64 2.7960 3.3630 2.9290 3.0260 3.1030
1,3,5-TRIMETHYLBENZENE 3.2480 2.9660 2.9730 2.7050 2.8250 3.4910 3.0620 3.1870 3.2370
1,2,4-TRIMETHYLBENZENE 3.9270 3.52 3.1760 2.8610 3.2010 3.7060 3.15 3.3930 3.3680
SEC-BUTYLBENZENE 3.2770 2.8290 2.8480 3.0460 2.9640 3.5540 3.2550 3.48 3.5560
VINYL CHLORIDE 1.0040 0.7670 0.5790 0.4950 0.5370 0.5740 0.6020 0.5520
TRICHLOROFLUOROMETHANE 0.5240 0.3760 0.3560 0.4090 0.41 0.5120 0.5640 0.5160
1,1,2-TRICHLOROTRIFLUOROETHANE 0.2820 0.2430 0.2410 0.2440 0.24 0.3140 0.3230 0.30
ACETONE 0.4930 0.3410 0.2320 0.2150 0.2250 0.2070 0.1890 0.1510
1,1-DICHLOROETHANE 0.9550 0.6270 0.7660 0.7620 0.7990 0.77 0.7980 0.7220
2,2-DICHLOROPROPANE 0.6030 0.3530 0.4740 0.4230 0.4140 0.4130 0.46 0.4120
CIS-1,2-DICHLOROETHENE 0.3250 0.3550 0.4190 0.4340 0.4460 0.4060 0.4130 0.3830
2-BUTANONE (MEK)0.3660 0.3050 0.3270 0.3220 0.4160 0.3520 0.36 0.34
CHLOROFORM 0.7670 0.6870 0.6490 0.6770 0.7220 0.6930 0.7090 0.6550
1,1,1-TRICHLOROETHANE 0.9030 0.4520 0.5160 0.5330 0.5530 0.5360 0.5880 0.5460
1,1-DICHLOROPROPENE 0.5350 0.42 0.3730 0.3640 0.4410 0.43 0.4490 0.4430
1,2-DICHLOROETHANE 0.7550 0.6220 0.5870 0.5640 0.6350 0.57 0.5660 0.54
1,2-DICHLOROPROPANE 0.5120 0.5260 0.4310 0.4120 0.4710 0.4330 0.44 0.4350
BROMODICHLOROMETHANE 0.8040 0.5340 0.4260 0.4670 0.5120 0.4560 0.5070 0.4980
TRANS-1,3-DICHLOROPROPENE 1.3790 1.0840 1.1440 1.1060 1.2930 1.1690 1.1640 1.29
1,1,2-TRICHLOROETHANE 0.8910 0.8360 0.7350 0.6950 0.89 0.7140 0.7250 0.7770
TETRACHLOROETHENE 0.8090 0.4940 0.4990 0.5050 0.6180 0.5830 0.5820 0.6140
1,3-DICHLOROPROPANE 1.4570 1.3010 1.2580 1.2030 1.4320 1.2140 1.21 1.3090
CHLORODIBROMOMETHANE 0.99 0.7130 0.7810 0.7780 0.8690 0.7410 0.8030 0.8740
1,1,1,2-TETRACHLOROETHANE 0.8460 0.7860 0.8170 0.7050 0.7890 0.7310 0.7160 0.73
ETHYLBENZENE 1.1750 1.1910 1.0870 1.0270 1.2690 1.14 1.0810 1.1290
O-XYLENE 1.5420 1.3030 1.2980 1.3710 1.4920 1.40 1.3520 1.3750
STYRENE 3.0740 2.35 2.3190 2.2560 2.4580 2.32 2.2810 2.3880
BROMOFORM 0.7290 0.5350 0.5630 0.5140 0.5990 0.5570 0.6230 0.6740
ISOPROPYLBENZENE 3.4490 3.2430 3.1590 2.9870 3.4120 3.2840 3.2440 3.3080
BROMOBENZENE 1.3270 1.0080 1.0160 0.9410 1.1920 1.0160 1.0450 1.0610
1,1,2,2-TETRACHLOROETHANE 2.1440 1.6720 1.4370 1.3790 1.75 1.4930 1.5120 1.5120
1,2,3-TRICHLOROPROPANE 0.4710 0.4720 0.4420 0.41 0.4920 0.4480 0.4420 0.4410
2-CHLOROTOLUENE 0.8720 1.0170 0.8610 0.9160 1.0920 0.9410 0.9640 0.9850
TERT-BUTYLBENZENE 3.1730 2.2290 2.0490 2.1090 2.6240 2.2830 2.4560 2.5250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 418 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS59
Analyte RRF: 0.02 RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75
Analysis date/time 10/07/24
18:03
10/07/24
18:23
10/07/24
18:43
10/07/24
19:02
10/07/24
19:22
10/07/24
19:42
10/07/24
20:01
10/07/24
20:21
10/07/24
20:40
10/07/24
20:59
P-ISOPROPYLTOLUENE 3.2990 3.1190 2.5930 2.6720 3.2760 2.86 3.0560 3.0790
1,4-DICHLOROBENZENE 1.8910 1.9390 1.6650 1.6570 2.0320 1.7810 1.8250 1.8050
1,2,3-TRIMETHYLBENZENE 4.0670 3.7290 3.0780 3.1860 3.68 3.2720 3.3980 3.3620
1,2-DICHLOROBENZENE 1.8550 1.5420 1.6740 1.5930 1.89 1.6870 1.77 1.7530
N-BUTYLBENZENE 2.9030 2.3540 2.4970 2.2980 2.7960 2.5470 2.7190 2.7610
1,2,4-TRICHLOROBENZENE 1.0230 0.89 0.8710 0.8420 0.9550 0.8760 0.9450 0.9470
HEXACHLORO-1,3-BUTADIENE 0.4990 0.3710 0.37 0.3680 0.3950 0.4020 0.4340 0.4330
NAPHTHALENE 4.2510 3.0610 3.0220 2.9610 3.5740 3.2650 3.4660 3.3980
1,2,3-TRICHLOROBENZENE 0.8670 0.8640 0.80 0.8470 0.8970 0.82 0.8910 0.8790
DICHLORODIFLUOROMETHANE 0.3990 0.3420 0.3470 0.3940 0.54 0.5780 0.5330
BROMOMETHANE 0.26 0.29 0.2990 0.3080 0.3060 0.3160 0.2590
CHLOROETHANE 0.1760 0.2780 0.27 0.2730 0.2910 0.2970 0.2540
TRANS-1,2-DICHLOROETHENE 0.4730 0.3680 0.3730 0.3790 0.3860 0.3870 0.3480
CARBON TETRACHLORIDE 0.5140 0.4690 0.4210 0.4850 0.5290 0.5690 0.53
DIBROMOMETHANE 0.2870 0.2490 0.2550 0.2770 0.2540 0.2590 0.2470
TOLUENE 3.1760 3.13 3.1260 3.5330 3.1280 3.1240 3.2810
1,2-DIBROMO-3-CHLOROPROPANE 0.3320 0.3570 0.32 0.3580 0.3460 0.3960 0.3970
CHLOROMETHANE 0.66 0.6920 0.6670 0.6620 0.6840 0.6290
METHYLENE CHLORIDE 0.4620 0.43 0.43 0.3860 0.4010 0.3580
File ID:1007_04 1007_05 1007_06 1007_07 1007_08 1007_09 1007_10 1007_11 1007_12 1007_13
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 419 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS59
Analyte RRF: 100 RRF. Avg %RSD COD
Analysis date/time 10/07/24
21:19
1,1-DICHLOROETHENE 0.71 0.606 10.91
ACRYLONITRILE 0.3050 0.29 8.82
CIS-1,3-DICHLOROPROPENE 0.6390 0.585 9.21
4-METHYL-2-PENTANONE (MIBK)1.5670 1.66 7.42
CHLOROBENZENE 2.1320 2.109 6.58
1,3-DICHLOROBENZENE 1.8010 1.726 6.8
1,2-DICHLOROETHANE-D4 0.4530 0.349 11.72
TOLUENE-D8 2.1160 2.15 2.56
4-BROMOFLUOROBENZENE 0.9430 0.927 2.66
METHYL TERT-BUTYL ETHER 1.1580 1.052 13.79
DI-ISOPROPYL ETHER 1.7310 1.628 7.79
BENZENE 1.5020 1.427 9.01
TRICHLOROETHENE 0.3810 0.347 6.77
1,2-DIBROMOETHANE 0.8760 0.867 9.56
M&P-XYLENE 1.3750 1.393 9.02
N-PROPYLBENZENE 4.5070 4.456 8.4
4-CHLOROTOLUENE 3.1010 3.016 8.75
1,3,5-TRIMETHYLBENZENE 3.2150 3.091 7.48
1,2,4-TRIMETHYLBENZENE 3.4080 3.371 8.96
SEC-BUTYLBENZENE 3.5430 3.235 9.12
VINYL CHLORIDE 0.6330 0.638 24.64 0.996
TRICHLOROFLUOROMETHANE 0.458 17.27 0.997
1,1,2-TRICHLOROTRIFLUOROETHANE 0.3340 0.28 13.88
ACETONE 0.1850 0.249 42.48 0.99
1,1-DICHLOROETHANE 0.8360 0.782 11.23
2,2-DICHLOROPROPANE 0.4520 0.445 15.53 0.998
CIS-1,2-DICHLOROETHENE 0.4490 0.403 10.41
2-BUTANONE (MEK)0.3630 0.35 9.21
CHLOROFORM 0.7590 0.702 5.92
1,1,1-TRICHLOROETHANE 0.6230 0.583 22.07 0.996
1,1-DICHLOROPROPENE 0.4960 0.439 12.18
1,2-DICHLOROETHANE 0.6210 0.607 10.54
1,2-DICHLOROPROPANE 0.4850 0.461 8.66
BROMODICHLOROMETHANE 0.5610 0.529 20.9 0.996
TRANS-1,3-DICHLOROPROPENE 1.2790 1.212 8.31
1,1,2-TRICHLOROETHANE 0.7740 0.782 9.5
TETRACHLOROETHENE 0.61 0.59 16.35 0.999
1,3-DICHLOROPROPANE 1.3060 1.299 7.14
CHLORODIBROMOMETHANE 0.9010 0.828 10.58
1,1,1,2-TETRACHLOROETHANE 0.7690 0.765 6.31
ETHYLBENZENE 1.14 1.138 6.16
O-XYLENE 1.4290 1.396 5.82
STYRENE 2.4430 2.432 10.29
BROMOFORM 0.7150 0.612 12.82
ISOPROPYLBENZENE 3.4180 3.278 4.44
BROMOBENZENE 1.0620 1.074 10.81
1,1,2,2-TETRACHLOROETHANE 1.5510 1.605 14.42
1,2,3-TRICHLOROPROPANE 0.4390 0.451 5.32
2-CHLOROTOLUENE 0.9750 0.958 7.49
TERT-BUTYLBENZENE 2.5030 2.439 13.87
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 420 of 526
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS59
Analyte RRF: 100 RRF. Avg %RSD COD
Analysis date/time 10/07/24
21:19
P-ISOPROPYLTOLUENE 3.0750 3.003 8.22
1,4-DICHLOROBENZENE 1.8410 1.826 6.61
1,2,3-TRIMETHYLBENZENE 3.39 3.462 8.92
1,2-DICHLOROBENZENE 1.7890 1.728 6.66
N-BUTYLBENZENE 2.7460 2.624 7.98
1,2,4-TRICHLOROBENZENE 0.94 0.921 6.05
HEXACHLORO-1,3-BUTADIENE 0.4090 0.409 10.28
NAPHTHALENE 3.3950 3.377 11.57
1,2,3-TRICHLOROBENZENE 0.8680 0.859 3.75
DICHLORODIFLUOROMETHANE 0.5830 0.465 22.31 0.997
BROMOMETHANE 0.3060 0.293 7.56
CHLOROETHANE 0.29 0.266 14.66
TRANS-1,2-DICHLOROETHENE 0.4050 0.39 9.6
CARBON TETRACHLORIDE 0.6040 0.515 11.16
DIBROMOMETHANE 0.2820 0.264 6.05
TOLUENE 3.2920 3.224 4.43
1,2-DIBROMO-3-CHLOROPROPANE 0.4130 0.365 9.18
CHLOROMETHANE 0.7310 0.675 4.73
METHYLENE CHLORIDE 0.4180 0.412 8.25
File ID:1007_14
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 421 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/22/24 17:10
Instrument ID:VOCMS16 Calibration (end) date/time:09/23/24 00:52
Lab File ID:0922_20 Analysis date/time:09/22/24 21:13
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.688789 0.69260210 0.5540 40 0.0050 0.005028 101
1,1,1-TRICHLOROETHANE 0.452589 0.46109330 1.88 40 0.0050 0.004859 97.20
1,1,2,2-TETRACHLOROETHANE 1.356469 1.271235 0.30 6.28 40 0.0050 0.004686 93.70
1,1,2-TRICHLOROETHANE 0.715309 0.707139 1.14 40 0.0050 0.004943 98.90
1,1,2-TRICHLOROTRIFLUOROETHANE 0.244519 0.24135420 1.29 40 0.0050 0.004585 91.70
1,1-DICHLOROETHANE 0.651085 0.66087170 0.10 1.50 40 0.0050 0.005075 102
1,1-DICHLOROETHENE 0.268947 0.27210090 1.17 20.49 0.0050 0.005059 101
1,1-DICHLOROPROPENE 0.392634 0.44800820 14.10 40 0.0050 0.005705 114
1,2,3-TRICHLOROBENZENE 0.649952 0.58427740 10.10 40 0.0050 0.004495 89.90
1,2,3-TRICHLOROPROPANE 0.464807 0.46768750 0.62 40 0.0050 0.005031 101
1,2,3-TRIMETHYLBENZENE 2.968035 2.904402 2.14 40 0.0050 0.004893 97.90
1,2,4-TRICHLOROBENZENE 0.721617 0.63739990 11.70 40 0.0050 0.004416 88.30
1,2,4-TRIMETHYLBENZENE 2.940738 2.907617 1.13 40 0.0050 0.004944 98.90
1,2-DIBROMO-3-CHLOROPROPANE 0.329343 0.283017 14.10 40 0.0050 0.004297 85.90 58 - 134
1,2-DIBROMOETHANE 0.745263 0.74138140 0.5210 40 0.0050 0.004974 99.50
1,2-DICHLOROBENZENE 1.557143 1.527691 1.89 40 0.0050 0.004905 98.10
1,2-DICHLOROETHANE 0.527112 0.48397610 8.18 40 0.0050 0.004591 91.80
1,2-DICHLOROPROPANE 0.280321 0.27500150 1.90 20.49 0.0050 0.004905 98.10
1,3,5-TRIMETHYLBENZENE 2.771371 2.792914 0.7770 40 0.0050 0.005039 101
1,3-DICHLOROBENZENE 1.626495 1.605417 1.30 40 0.0050 0.004935 98.70
1,3-DICHLOROPROPANE 1.271896 1.212484 4.67 40 0.0050 0.004766 95.30
1,4-DICHLOROBENZENE 1.655608 1.671750 0.9750 40 0.0050 0.005049 101
2,2-DICHLOROPROPANE 0.203557 0.24528620 20.50 40 0.0050 0.005800 116
2-BUTANONE (MEK)0.392902 0.37506260 4.54 40 0.0250 0.02386 95.40 44 - 160
2-CHLOROTOLUENE 2.876765 2.908735 1.11 40 0.0050 0.005056 101
4-CHLOROTOLUENE 2.764345 2.772015 0.2770 40 0.0050 0.005014 100
4-METHYL-2-PENTANONE (MIBK)1.649593 1.675231 1.55 40 0.0250 0.02539 102 68 - 142
ACETONE 0.212553 0.20659810 2.80 40 0.0250 0.02430 97.20 19 - 160
ACROLEIN 0.084458 0.08081380 4.31 40 0.0250 0.02392 95.70 10 - 160
ACRYLONITRILE 0.278354 0.28777720 3.39 40 0.0250 0.02585 103
BENZENE 1.316981 1.294284 1.72 40 0.0050 0.004914 98.30
BROMOBENZENE 1.831992 1.825666 0.3450 40 0.0050 0.004983 99.70
BROMODICHLOROMETHANE 0.444113 0.388427 12.50 40 0.0050 0.004373 87.50
BROMOFORM 0.518520 0.49403890 0.10 4.72 40 0.0050 0.004764 95.30
BROMOMETHANE 0.163366 0.20325920 24.40 40 0.0050 0.006221 124 10 - 160
CARBON TETRACHLORIDE 0.452522 0.47211570 4.33 40 0.0050 0.005216 104
CHLOROBENZENE 1.972298 1.994838 0.30 1.14 40 0.0050 0.005057 101
CHLORODIBROMOMETHANE 0.789395 0.74929590 5.08 40 0.0050 0.004746 94.90
CHLOROETHANE 0.189530 0.18482410 2.48 40 0.0050 0.004876 97.50 47 - 150
CHLOROFORM 0.592765 0.54819820 7.52 20.49 0.0050 0.004624 92.50
CHLOROMETHANE 0.537364 0.42579150 0.10 20.80 40 0.0050 0.003962 79.20
CIS-1,2-DICHLOROETHENE 0.334984 0.31606160 5.65 40 0.0050 0.004718 94.40
CIS-1,3-DICHLOROPROPENE 0.523849 0.50054190 4.45 40 0.0050 0.004778 95.60
DI-ISOPROPYL ETHER 1.474766 1.417507 3.88 40 0.0050 0.004806 96.10
DIBROMOMETHANE 0.196511 0.19146330 2.57 40 0.0050 0.004872 97.40
DICHLORODIFLUOROMETHANE 0.439284 0.32742780 25.50 40 0.0050 0.003727 74.50 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 422 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/22/24 17:10
Instrument ID:VOCMS16 Calibration (end) date/time:09/23/24 00:52
Lab File ID:0922_20 Analysis date/time:09/22/24 21:13
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.002526 1.022643 2.01 20.49 0.0050 0.005100 102
HEXACHLORO-1,3-BUTADIENE 0.282892 0.314541 11.20 40 0.0050 0.005559 111
ISOPROPYLBENZENE 2.718978 2.556231 5.99 40 0.0050 0.004701 94
M&P-XYLENE 1.212176 1.217276 0.4210 40 0.01 0.01004 100
METHYL TERT-BUTYL ETHER 1.025657 0.98230490 4.23 40 0.0050 0.004789 95.80
METHYLENE CHLORIDE 0.321035 0.29354410 8.56 40 0.0050 0.004572 91.40
N-BUTYLBENZENE 2.120771 2.199061 3.69 40 0.0050 0.004849 97
N-PROPYLBENZENE 4.078355 4.082532 0.1020 40 0.0050 0.005005 100
NAPHTHALENE 2.604989 2.301042 11.70 40 0.0050 0.004265 85.30 54 - 135
O-XYLENE 1.179372 1.189979 0.8990 40 0.0050 0.005045 101
P-ISOPROPYLTOLUENE 2.634126 2.741469 4.08 40 0.0050 0.004887 97.70
SEC-BUTYLBENZENE 3.035060 3.256618 7.30 40 0.0050 0.005365 107
STYRENE 1.966524 1.897226 3.52 40 0.0050 0.004824 96.50
TERT-BUTYLBENZENE 2.234499 2.393587 7.12 40 0.0050 0.005356 107
TETRACHLOROETHENE 0.521817 0.57539170 10.30 40 0.0050 0.005513 110
TOLUENE 3.220154 3.164950 1.71 20.49 0.0050 0.004914 98.30
TRANS-1,2-DICHLOROETHENE 0.302556 0.29822810 1.43 40 0.0050 0.004928 98.60
TRANS-1,3-DICHLOROPROPENE 1.188654 1.147768 3.44 40 0.0050 0.004828 96.60
TRICHLOROETHENE 0.315290 0.33918070 7.58 40 0.0050 0.005379 108
TRICHLOROFLUOROMETHANE 0.399803 0.34328460 14.10 40 0.0050 0.004293 85.90
VINYL CHLORIDE 0.326285 0.31436420 3.65 20.49 0.0050 0.004426 88.50
XYLENES, TOTAL 0 1.568511 0 40 0.0150 0.015085 101
1,2-DICHLOROETHANE-D4 0.352970 0.32466950 8.02 40 0.0160 0.01472 92 70 - 130
4-BROMOFLUOROBENZENE 0.796137 0.80205270 0.7430 40 0.0160 0.01612 101 67 - 138
TOLUENE-D8 2.333081 2.348869 0.6770 40 0.0160 0.01611 101 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 423 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/22/24 17:10
Instrument ID:VOCMS16 Calibration (end) date/time:09/23/24 00:52
Lab File ID:1010_31 Analysis date/time:10/10/24 21:27
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.688789 0.68466310 0.5990 0.0050 0.004970 99.40
1,1,1-TRICHLOROETHANE 0.452589 0.50690040 12 0.0050 0.005325 106
1,1,2,2-TETRACHLOROETHANE 1.356469 1.183682 0.30 12.70 0.0050 0.004363 87.30
1,1,2-TRICHLOROETHANE 0.715309 0.65928480 7.83 0.0050 0.004608 92.20
1,1,2-TRICHLOROTRIFLUOROETHANE 0.244519 0.26246670 7.34 0.0050 0.004963 99.30
1,1-DICHLOROETHANE 0.651085 0.70364760 0.10 8.07 0.0050 0.005404 108
1,1-DICHLOROETHENE 0.268947 0.28869420 7.34 20 0.0050 0.005367 107
1,1-DICHLOROPROPENE 0.392634 0.40212740 2.42 0.0050 0.005121 102
1,2,3-TRICHLOROBENZENE 0.649952 0.87284620 34.30 0.0050 0.006715 134
1,2,3-TRICHLOROPROPANE 0.464807 0.42885020 7.74 0.0050 0.004613 92.30
1,2,3-TRIMETHYLBENZENE 2.968035 2.797598 5.74 0.0050 0.004713 94.30
1,2,4-TRICHLOROBENZENE 0.721617 0.86423540 19.80 0.0050 0.005988 120
1,2,4-TRIMETHYLBENZENE 2.940738 2.671049 9.17 0.0050 0.004541 90.80
1,2-DIBROMO-3-CHLOROPROPANE 0.329343 0.33505360 1.73 0.0050 0.005087 102
1,2-DIBROMOETHANE 0.745263 0.64965620 12.80 0.0050 0.004359 87.20
1,2-DICHLOROBENZENE 1.557143 1.482985 4.76 0.0050 0.004762 95.20
1,2-DICHLOROETHANE 0.527112 0.53915720 2.29 0.0050 0.005114 102
1,2-DICHLOROPROPANE 0.280321 0.24901040 11.20 20 0.0050 0.004442 88.80
1,3,5-TRIMETHYLBENZENE 2.771371 2.496526 9.92 0.0050 0.004504 90.10
1,3-DICHLOROBENZENE 1.626495 1.468531 9.71 0.0050 0.004514 90.30
1,3-DICHLOROPROPANE 1.271896 1.102476 13.30 0.0050 0.004334 86.70
1,4-DICHLOROBENZENE 1.655608 1.515045 8.49 0.0050 0.004575 91.50
2,2-DICHLOROPROPANE 0.203557 0.45395210 123 0.0050 0.01066 213
2-BUTANONE (MEK)0.392902 0.38974540 0.8030 0.0250 0.02480 99.20
2-CHLOROTOLUENE 2.876765 2.623997 8.79 0.0050 0.004561 91.20
4-CHLOROTOLUENE 2.764345 2.281486 17.50 0.0050 0.004127 82.50
4-METHYL-2-PENTANONE (MIBK)1.649593 1.657731 0.4930 0.0250 0.02512 100
ACETONE 0.212553 0.29460840 38.60 0.0250 0.03465 139
ACROLEIN 0.084458 0.10093060 19.50 0.0250 0.02988 120
ACRYLONITRILE 0.278354 0.33995430 22.10 0.0250 0.03053 122
BENZENE 1.316981 1.220907 7.30 0.0050 0.004635 92.70
BROMOBENZENE 1.831992 1.520042 17 0.0050 0.004149 83
BROMODICHLOROMETHANE 0.444113 0.40771820 8.19 0.0050 0.004590 91.80
BROMOFORM 0.518520 0.40481430 0.10 21.90 0.0050 0.003904 78.10
BROMOMETHANE 0.163366 0.20929920 28.10 0.0050 0.006406 128
CARBON TETRACHLORIDE 0.452522 0.46439370 2.62 0.0050 0.005131 103
CHLOROBENZENE 1.972298 1.738308 0.30 11.90 0.0050 0.004407 88.10
CHLORODIBROMOMETHANE 0.789395 0.635901 19.40 0.0050 0.004028 80.60
CHLOROETHANE 0.189530 0.24955850 31.70 0.0050 0.006584 132
CHLOROFORM 0.592765 0.61230360 3.30 20 0.0050 0.005165 103
CHLOROMETHANE 0.537364 0.554066 0.10 3.11 0.0050 0.005155 103
CIS-1,2-DICHLOROETHENE 0.334984 0.35792160 6.85 0.0050 0.005342 107
CIS-1,3-DICHLOROPROPENE 0.523849 0.39250790 25.10 0.0050 0.003746 74.90
DI-ISOPROPYL ETHER 1.474766 1.536240 4.17 0.0050 0.005208 104
DIBROMOMETHANE 0.196511 0.215904 9.87 0.0050 0.005493 110
DICHLORODIFLUOROMETHANE 0.439284 0.44701840 1.76 0.0050 0.005088 102
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 424 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/22/24 17:10
Instrument ID:VOCMS16 Calibration (end) date/time:09/23/24 00:52
Lab File ID:1010_31 Analysis date/time:10/10/24 21:27
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.002526 0.90254480 9.97 20 0.0050 0.004501 90
HEXACHLORO-1,3-BUTADIENE 0.282892 0.37041950 30.90 0.0050 0.006547 131
ISOPROPYLBENZENE 2.718978 2.700344 0.6850 0.0050 0.004966 99.30
M&P-XYLENE 1.212176 1.117194 7.84 0.01 0.009216 92.20
METHYL TERT-BUTYL ETHER 1.025657 1.086289 5.91 0.0050 0.005296 106
METHYLENE CHLORIDE 0.321035 0.35074130 9.25 0.0050 0.005463 109
N-BUTYLBENZENE 2.120771 2.074595 2.18 0.0050 0.004588 91.80
N-PROPYLBENZENE 4.078355 3.424574 16 0.0050 0.004198 84
NAPHTHALENE 2.604989 3.106819 19.30 0.0050 0.005582 112
O-XYLENE 1.179372 1.120014 5.03 0.0050 0.004748 95
P-ISOPROPYLTOLUENE 2.634126 2.426794 7.87 0.0050 0.004351 87
SEC-BUTYLBENZENE 3.035060 2.729326 10.10 0.0050 0.004496 89.90
STYRENE 1.966524 1.740234 11.50 0.0050 0.004425 88.50
TERT-BUTYLBENZENE 2.234499 1.833569 17.90 0.0050 0.004103 82.10
TETRACHLOROETHENE 0.521817 0.47469060 9.03 0.0050 0.004548 91
TOLUENE 3.220154 2.780124 13.70 20 0.0050 0.004317 86.30
TRANS-1,2-DICHLOROETHENE 0.302556 0.32396570 7.08 0.0050 0.005354 107
TRANS-1,3-DICHLOROPROPENE 1.188654 0.93631370 21.20 0.0050 0.003939 78.80
TRICHLOROETHENE 0.315290 0.29091410 7.73 0.0050 0.004613 92.30
TRICHLOROFLUOROMETHANE 0.399803 0.47497240 18.80 0.0050 0.005940 119
VINYL CHLORIDE 0.326285 0.42901270 31.50 20 0.0050 0.005928 119 80 - 120
XYLENES, TOTAL 0 1.249929 0 0.0150 0.013964 93.10
1,2-DICHLOROETHANE-D4 0.352970 0.37172730 5.31 0.0160 0.01685 105 70 - 130
4-BROMOFLUOROBENZENE 0.796137 0.84923060 6.67 0.0160 0.01707 107 70 - 130
TOLUENE-D8 2.333081 2.254406 3.37 0.0160 0.01546 96.60 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 425 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/12/24 18:56
Instrument ID:VOCMS36 Calibration (end) date/time:09/13/24 17:40
Lab File ID:0912_19 Analysis date/time:09/12/24 22:44
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ACROLEIN 0.057784 0.05397861 6.59 20 0.0250 0.02335 93.40 10 - 160
1,2-DICHLOROETHANE-D4 0.352716 0.35987730 2.03 40 0.0160 0.01632 102 70 - 130
4-BROMOFLUOROBENZENE 0.874532 0.87218140 0.2690 40 0.0160 0.01596 99.80 67 - 138
TOLUENE-D8 2.178867 2.241631 2.88 40 0.0160 0.01646 103 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 426 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/12/24 18:56
Instrument ID:VOCMS36 Calibration (end) date/time:09/13/24 17:40
Lab File ID:0912_48 Analysis date/time:09/13/24 14:12
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.527456 0.53633170 1.68 40 0.0050 0.005084 102
1,1,1-TRICHLOROETHANE 0.397925 0.42179410 6 40 0.0050 0.005300 106
1,1,2,2-TETRACHLOROETHANE 0.762750 0.78376990 0.30 2.76 40 0.0050 0.005138 103
1,1,2-TRICHLOROETHANE 0.528049 0.52610450 0.3680 40 0.0050 0.004982 99.60
1,1,2-TRICHLOROTRIFLUOROETHANE 0.202287 0.19682030 2.70 40 0.0050 0.004556 91.10
1,1-DICHLOROETHANE 0.521612 0.54681720 0.10 4.83 40 0.0050 0.005242 105
1,1-DICHLOROETHENE 0.215678 0.220728 2.34 20.49 0.0050 0.005117 102
1,1-DICHLOROPROPENE 0.316672 0.36471420 15.20 40 0.0050 0.005759 115
1,2,3-TRICHLOROBENZENE 0.483839 0.459886 4.95 40 0.0050 0.004752 95
1,2,3-TRICHLOROPROPANE 0.221729 0.21360370 3.66 40 0.0050 0.004817 96.30
1,2,3-TRIMETHYLBENZENE 2.299797 2.359755 2.61 40 0.0050 0.005130 103
1,2,4-TRICHLOROBENZENE 0.625757 0.63706340 1.81 40 0.0050 0.005090 102
1,2,4-TRIMETHYLBENZENE 2.284274 2.408504 5.44 40 0.0050 0.005272 105
1,2-DIBROMO-3-CHLOROPROPANE 0.139259 0.13348630 4.15 40 0.0050 0.004793 95.90 58 - 134
1,2-DIBROMOETHANE 0.556511 0.53895760 3.15 40 0.0050 0.004842 96.80
1,2-DICHLOROBENZENE 1.216427 1.231950 1.28 40 0.0050 0.005064 101
1,2-DICHLOROETHANE 0.428278 0.428401 0.0287 40 0.0050 0.005001 100
1,2-DICHLOROPROPANE 0.225933 0.22353380 1.06 20.49 0.0050 0.004947 98.90
1,3,5-TRIMETHYLBENZENE 2.175434 2.294296 5.46 40 0.0050 0.005273 105
1,3-DICHLOROBENZENE 1.234858 1.258237 1.89 40 0.0050 0.005095 102
1,3-DICHLOROPROPANE 0.919659 0.94689590 2.96 40 0.0050 0.005148 103
1,4-DICHLOROBENZENE 1.282226 1.3248 3.32 40 0.0050 0.005166 103
2,2-DICHLOROPROPANE 0.368685 0.42908920 16.40 40 0.0050 0.005819 116
2-BUTANONE (MEK)0.139779 0.12466940 10.80 40 0.0250 0.02230 89.20 44 - 160
2-CHLOROTOLUENE 2.077852 2.153673 3.65 40 0.0050 0.005182 104
4-CHLOROTOLUENE 1.948999 2.001242 2.68 40 0.0050 0.005134 103
4-METHYL-2-PENTANONE (MIBK)0.714060 0.69363780 2.86 40 0.0250 0.02428 97.10 68 - 142
ACETONE 0.097906 0.08487975 13.30 40 0.0250 0.02167 86.70 19 - 160
ACROLEIN 0.057784 0.05655262 2.13 40 0.0250 0.02447 97.90 10 - 160
ACRYLONITRILE 0.132139 0.12652020 4.25 40 0.0250 0.02394 95.80
BENZENE 1.010804 1.078853 6.73 40 0.0050 0.005337 107
BROMOBENZENE 1.272924 1.320051 3.70 40 0.0050 0.005185 104
BROMODICHLOROMETHANE 0.369064 0.37266580 0.9760 40 0.0050 0.005049 101
BROMOFORM 0.455168 0.44315780 0.10 2.64 40 0.0050 0.004868 97.40
BROMOMETHANE 0.072201 0.05476113 24.20 40 0.0050 0.003792 75.80 10 - 160
CARBON TETRACHLORIDE 0.358308 0.388209 8.35 40 0.0050 0.005417 108
CHLOROBENZENE 1.470714 1.547010 0.30 5.19 40 0.0050 0.005259 105
CHLORODIBROMOMETHANE 0.614624 0.61591540 0.21 40 0.0050 0.005011 100
CHLOROETHANE 0.198396 0.18373350 7.39 40 0.0050 0.004630 92.60 47 - 150
CHLOROFORM 0.480073 0.50734510 5.68 20.49 0.0050 0.005284 106
CHLOROMETHANE 0.786618 0.64997610 0.10 17.40 40 0.0050 0.004131 82.60
CIS-1,2-DICHLOROETHENE 0.263482 0.29292760 11.20 40 0.0050 0.005559 111
CIS-1,3-DICHLOROPROPENE 0.434567 0.44715240 2.90 40 0.0050 0.005145 103
DI-ISOPROPYL ETHER 1.075257 1.021911 4.96 40 0.0050 0.004752 95
DIBROMOMETHANE 0.169932 0.16968330 0.1460 40 0.0050 0.004993 99.90
DICHLORODIFLUOROMETHANE 0.349605 0.22686910 35.10 40 0.0050 0.003245 64.90 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 427 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/12/24 18:56
Instrument ID:VOCMS36 Calibration (end) date/time:09/13/24 17:40
Lab File ID:0912_48 Analysis date/time:09/13/24 14:12
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.799111 0.85351470 6.81 20.49 0.0050 0.005340 107
HEXACHLORO-1,3-BUTADIENE 0.290731 0.29282270 0.7190 40 0.0050 0.005036 101
ISOPROPYLBENZENE 2.407659 2.226938 7.51 40 0.0050 0.004625 92.50
M&P-XYLENE 0.951884 1.054754 10.80 40 0.01 0.01108 111
METHYL TERT-BUTYL ETHER 0.773773 0.78986470 2.08 40 0.0050 0.005104 102
METHYLENE CHLORIDE 0.272985 0.27952320 2.40 40 0.0050 0.005120 102
N-BUTYLBENZENE 1.844892 1.879179 1.86 40 0.0050 0.005093 102
N-PROPYLBENZENE 3.131754 3.274650 4.56 40 0.0050 0.005228 105
NAPHTHALENE 1.216609 1.553575 27.70 40 0.0050 0.006385 128 54 - 135
O-XYLENE 0.956971 1.010379 5.58 40 0.0050 0.005279 106
P-ISOPROPYLTOLUENE 2.139802 2.221135 3.80 40 0.0050 0.005190 104
SEC-BUTYLBENZENE 2.421009 2.593972 7.14 40 0.0050 0.005357 107
STYRENE 1.593142 1.605310 0.7640 40 0.0050 0.005038 101
TERT-BUTYLBENZENE 1.749995 1.786791 2.10 40 0.0050 0.005105 102
TETRACHLOROETHENE 0.461590 0.502978 8.97 40 0.0050 0.005448 109
TOLUENE 2.299271 2.434845 5.90 20.49 0.0050 0.005295 106
TRANS-1,2-DICHLOROETHENE 0.238768 0.24578980 2.94 40 0.0050 0.005147 103
TRANS-1,3-DICHLOROPROPENE 0.851531 0.84692670 0.5410 40 0.0050 0.004973 99.50
TRICHLOROETHENE 0.253669 0.26932690 6.17 40 0.0050 0.005309 106
TRICHLOROFLUOROMETHANE 0.399910 0.311986 22 40 0.0050 0.003901 78
VINYL CHLORIDE 0.400016 0.32020230 20 20.49 0.0050 0.004002 80
XYLENES, TOTAL 0 1.158978 0 40 0.0150 0.016359 109
1,2-DICHLOROETHANE-D4 0.352716 0.36480950 3.43 40 0.0160 0.01655 103 70 - 130
4-BROMOFLUOROBENZENE 0.874532 0.87556420 0.1180 40 0.0160 0.01602 100 67 - 138
TOLUENE-D8 2.178867 2.211981 1.52 40 0.0160 0.01624 102 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 428 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/12/24 18:56
Instrument ID:VOCMS36 Calibration (end) date/time:09/13/24 17:40
Lab File ID:1010_02 Analysis date/time:10/10/24 03:47
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.527456 0.520943 1.23 0.0050 0.004938 98.80
1,1,1-TRICHLOROETHANE 0.397925 0.42325130 6.36 0.0050 0.005318 106
1,1,2,2-TETRACHLOROETHANE 0.762750 0.67765060 0.30 11.20 0.0050 0.004442 88.80
1,1,2-TRICHLOROETHANE 0.528049 0.516968 2.10 0.0050 0.004895 97.90
1,1,2-TRICHLOROTRIFLUOROETHANE 0.202287 0.23255930 15 0.0050 0.005340 107
1,1-DICHLOROETHANE 0.521612 0.57121380 0.10 9.51 0.0050 0.005475 110
1,1-DICHLOROETHENE 0.215678 0.22405850 3.89 20 0.0050 0.005194 104
1,1-DICHLOROPROPENE 0.316672 0.34462960 8.83 0.0050 0.005441 109
1,2,3-TRICHLOROBENZENE 0.483839 0.27843860 42.50 0.0050 0.002877 57.50
1,2,3-TRICHLOROPROPANE 0.221729 0.21539220 2.86 0.0050 0.004857 97.10
1,2,3-TRIMETHYLBENZENE 2.299797 2.256520 1.88 0.0050 0.004906 98.10
1,2,4-TRICHLOROBENZENE 0.625757 0.42777990 31.60 0.0050 0.003418 68.40
1,2,4-TRIMETHYLBENZENE 2.284274 2.102943 7.94 0.0050 0.004603 92.10
1,2-DIBROMO-3-CHLOROPROPANE 0.139259 0.06585397 52.70 0.0050 0.002364 47.30
1,2-DIBROMOETHANE 0.556511 0.48550590 12.80 0.0050 0.004362 87.20
1,2-DICHLOROBENZENE 1.216427 1.198227 1.50 0.0050 0.004925 98.50
1,2-DICHLOROETHANE 0.428278 0.48041590 12.20 0.0050 0.005609 112
1,2-DICHLOROPROPANE 0.225933 0.24791810 9.73 20 0.0050 0.005487 110
1,3,5-TRIMETHYLBENZENE 2.175434 2.143086 1.49 0.0050 0.004926 98.50
1,3-DICHLOROBENZENE 1.234858 1.246792 0.9660 0.0050 0.005048 101
1,3-DICHLOROPROPANE 0.919659 0.88588650 3.67 0.0050 0.004816 96.30
1,4-DICHLOROBENZENE 1.282226 1.337372 4.30 0.0050 0.005215 104
2,2-DICHLOROPROPANE 0.368685 0.40974050 11.10 0.0050 0.005557 111
2-BUTANONE (MEK)0.139779 0.10563930 24.40 0.0250 0.01889 75.60
2-CHLOROTOLUENE 2.077852 2.121217 2.09 0.0050 0.005104 102
4-CHLOROTOLUENE 1.948999 1.905037 2.26 0.0050 0.004887 97.70
4-METHYL-2-PENTANONE (MIBK)0.714060 0.58555880 18 0.0250 0.02050 82
ACETONE 0.097906 0.08301993 15.20 0.0250 0.02120 84.80
ACROLEIN 0.057784 0.05290590 8.44 0.0250 0.02289 91.60
ACRYLONITRILE 0.132139 0.12162650 7.96 0.0250 0.02301 92
BENZENE 1.010804 1.087542 7.59 0.0050 0.005380 108
BROMOBENZENE 1.272924 1.246152 2.10 0.0050 0.004895 97.90
BROMODICHLOROMETHANE 0.369064 0.407913 10.50 0.0050 0.005526 111
BROMOFORM 0.455168 0.36096840 0.10 20.70 0.0050 0.003965 79.30
BROMOMETHANE 0.072201 0.13231610 83.30 0.0050 0.009163 183
CARBON TETRACHLORIDE 0.358308 0.41641380 16.20 0.0050 0.005811 116
CHLOROBENZENE 1.470714 1.555683 0.30 5.78 0.0050 0.005289 106
CHLORODIBROMOMETHANE 0.614624 0.57308390 6.76 0.0050 0.004662 93.20
CHLOROETHANE 0.198396 0.28432350 43.30 0.0050 0.007166 143
CHLOROFORM 0.480073 0.53930510 12.30 20 0.0050 0.005617 112
CHLOROMETHANE 0.786618 0.786094 0.10 0.0666 0.0050 0.004997 99.90
CIS-1,2-DICHLOROETHENE 0.263482 0.29647920 12.50 0.0050 0.005626 113
CIS-1,3-DICHLOROPROPENE 0.434567 0.42990410 1.07 0.0050 0.004946 98.90
DI-ISOPROPYL ETHER 1.075257 1.208319 12.40 0.0050 0.005619 112
DIBROMOMETHANE 0.169932 0.19196510 13 0.0050 0.005648 113
DICHLORODIFLUOROMETHANE 0.349605 0.33204280 5.02 0.0050 0.004749 95
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 429 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:09/12/24 18:56
Instrument ID:VOCMS36 Calibration (end) date/time:09/13/24 17:40
Lab File ID:1010_02 Analysis date/time:10/10/24 03:47
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.799111 0.78511480 1.75 20 0.0050 0.004912 98.20
HEXACHLORO-1,3-BUTADIENE 0.290731 0.27868490 4.14 0.0050 0.004793 95.90
ISOPROPYLBENZENE 2.407659 2.187758 9.13 0.0050 0.004543 90.90
M&P-XYLENE 0.951884 0.92584850 2.74 0.01 0.009726 97.30
METHYL TERT-BUTYL ETHER 0.773773 0.74293310 3.99 0.0050 0.004801 96
METHYLENE CHLORIDE 0.272985 0.32479450 19 0.0050 0.005949 119
N-BUTYLBENZENE 1.844892 1.628322 11.70 0.0050 0.004413 88.30
N-PROPYLBENZENE 3.131754 3.026376 3.36 0.0050 0.004832 96.60
NAPHTHALENE 1.216609 0.36493050 70 0.0050 0.001500 30
O-XYLENE 0.956971 0.86368550 9.75 0.0050 0.004513 90.30
P-ISOPROPYLTOLUENE 2.139802 2.025416 5.35 0.0050 0.004733 94.70
SEC-BUTYLBENZENE 2.421009 2.458318 1.54 0.0050 0.005077 102
STYRENE 1.593142 1.328724 16.60 0.0050 0.004170 83.40
TERT-BUTYLBENZENE 1.749995 1.651816 5.61 0.0050 0.004719 94.40
TETRACHLOROETHENE 0.461590 0.499926 8.31 0.0050 0.005415 108
TOLUENE 2.299271 2.394841 4.16 20 0.0050 0.005208 104
TRANS-1,2-DICHLOROETHENE 0.238768 0.25951940 8.69 0.0050 0.005435 109
TRANS-1,3-DICHLOROPROPENE 0.851531 0.81302470 4.52 0.0050 0.004774 95.50
TRICHLOROETHENE 0.253669 0.277794 9.51 0.0050 0.005476 110
TRICHLOROFLUOROMETHANE 0.399910 0.43996540 10 0.0050 0.005501 110
VINYL CHLORIDE 0.400016 0.44035550 10.10 20 0.0050 0.005504 110
XYLENES, TOTAL 0 1.054254 0 0.0150 0.014239 94.90
1,2-DICHLOROETHANE-D4 0.352716 0.379916 7.71 0.0160 0.01723 108 70 - 130
4-BROMOFLUOROBENZENE 0.874532 0.81055080 7.32 0.0160 0.01483 92.70 70 - 130
TOLUENE-D8 2.178867 2.197854 0.8710 0.0160 0.01614 101 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 430 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/03/24 15:22
Instrument ID:VOCMS42 Calibration (end) date/time:10/03/24 18:40
Lab File ID:1003a_18 Analysis date/time:10/03/24 19:59
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5110 0.43573620 14.70 40 0.0050 0.004264 85.30
1,1,1-TRICHLOROETHANE 0.38 0.335639 11.70 40 0.0050 0.004418 88.40
1,1,2,2-TETRACHLOROETHANE 0.8820 0.73559770 0.30 16.60 40 0.0050 0.004172 83.40
1,1,2-TRICHLOROETHANE 0.5410 0.49292250 8.89 40 0.0050 0.004559 91.20
1,1,2-TRICHLOROTRIFLUOROETHANE 0.24 0.24111920 0.4660 40 0.0050 0.005021 100
1,1-DICHLOROETHANE 0.5130 0.50260080 0.10 2.03 40 0.0050 0.004896 97.90
1,1-DICHLOROETHENE 0.4520 0.41693080 7.76 20.49 0.0050 0.004611 92.20
1,1-DICHLOROPROPENE 0.33 0.33964860 2.92 40 0.0050 0.005150 103
1,2,3-TRICHLOROBENZENE 0.4790 0.37943680 20.80 40 0.0050 0.003779 75.60
1,2,3-TRICHLOROPROPANE 0.2780 0.25633930 7.79 40 0.0050 0.004604 92.10
1,2,3-TRIMETHYLBENZENE 1.8940 1.784175 5.80 40 0.0050 0.004710 94.20
1,2,4-TRICHLOROBENZENE 0.4880 0.40506580 17 40 0.0050 0.004151 83
1,2,4-TRIMETHYLBENZENE 1.8760 1.787329 4.73 40 0.0050 0.004764 95.30
1,2-DIBROMO-3-CHLOROPROPANE 0.2040 0.15291970 25 40 0.0050 0.003161 63.20 58 - 134
1,2-DIBROMOETHANE 0.5840 0.53971470 7.58 40 0.0050 0.004618 92.40
1,2-DICHLOROBENZENE 1.1020 1.033603 6.21 40 0.0050 0.004691 93.80
1,2-DICHLOROETHANE 0.3930 0.32605720 17 40 0.0050 0.004150 83
1,2-DICHLOROPROPANE 0.32 0.28708040 10.30 20.49 0.0050 0.004491 89.80
1,3,5-TRIMETHYLBENZENE 1.9020 1.794720 5.64 40 0.0050 0.004719 94.40
1,3-DICHLOROBENZENE 1.2410 1.140939 8.06 40 0.0050 0.004597 91.90
1,3-DICHLOROPROPANE 0.9010 0.87703160 2.66 40 0.0050 0.004865 97.30
1,4-DICHLOROBENZENE 1.2740 1.177312 7.59 40 0.0050 0.004621 92.40
2,2-DICHLOROPROPANE 0.2360 0.21602890 8.46 40 0.0050 0.004568 91.40
2-BUTANONE (MEK)0.3090 0.26656170 13.70 40 0.0250 0.02157 86.30 44 - 160
2-CHLOROTOLUENE 0.6460 0.60019430 7.09 40 0.0050 0.004646 92.90
4-CHLOROTOLUENE 2.1860 2.128133 2.65 40 0.0050 0.004868 97.40
4-METHYL-2-PENTANONE (MIBK)0.9440 0.86806480 8.04 40 0.0250 0.02300 92 68 - 142
ACETONE 0.0980 0.08017438 18.20 40 0.0250 0.01652 66.10 19 - 160
ACROLEIN 0.0160 0.01412956 11.70 40 0.0250 0.02146 85.80 10 - 160
ACRYLONITRILE 0.1590 0.10464880 34.20 40 0.0250 0.01429 57.20
BENZENE 1.0370 0.92778070 10.50 40 0.0050 0.004472 89.40
BROMOBENZENE 0.74 0.71065690 3.97 40 0.0050 0.004805 96.10
BROMODICHLOROMETHANE 0.3270 0.30049570 8.11 40 0.0050 0.004590 91.80
BROMOFORM 0.4350 0.37028430 0.10 14.90 40 0.0050 0.004256 85.10
BROMOMETHANE 0.1820 0.18461940 1.44 40 0.0050 0.005064 101 10 - 160
CARBON TETRACHLORIDE 0.34 0.31233240 8.14 40 0.0050 0.004598 92
CHLOROBENZENE 1.6750 1.584339 0.30 5.41 40 0.0050 0.004729 94.60
CHLORODIBROMOMETHANE 0.5840 0.55274910 5.35 40 0.0050 0.004734 94.70
CHLOROETHANE 0.2240 0.19908070 11.10 40 0.0050 0.004446 88.90 47 - 150
CHLOROFORM 0.4670 0.40520610 13.20 20.49 0.0050 0.004338 86.80
CHLOROMETHANE 0.4670 0.435617 0.10 6.72 40 0.0050 0.004661 93.20
CIS-1,2-DICHLOROETHENE 0.28 0.25791850 7.89 40 0.0050 0.004604 92.10
CIS-1,3-DICHLOROPROPENE 0.3770 0.36366950 3.54 40 0.0050 0.004826 96.50
DI-ISOPROPYL ETHER 0.9670 0.88453780 8.53 40 0.0050 0.004572 91.40
DIBROMOMETHANE 0.1570 0.14551490 7.32 40 0.0050 0.004639 92.80
DICHLORODIFLUOROMETHANE 0.2430 0.25066030 3.15 40 0.0050 0.005151 103 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 431 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/03/24 15:22
Instrument ID:VOCMS42 Calibration (end) date/time:10/03/24 18:40
Lab File ID:1003a_18 Analysis date/time:10/03/24 19:59
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.8520 0.81810480 3.98 20.49 0.0050 0.004801 96
HEXACHLORO-1,3-BUTADIENE 0.22 0.22377790 1.72 40 0.0050 0.005089 102
ISOPROPYLBENZENE 2.2930 1.941777 15.30 40 0.0050 0.004233 84.70
M&P-XYLENE 1.0470 0.996803 4.79 40 0.01 0.009521 95.20
METHYL TERT-BUTYL ETHER 0.5850 0.46952190 19.70 40 0.0050 0.004011 80.20
METHYLENE CHLORIDE 0.2780 0.24338640 12.50 40 0.0050 0.004380 87.60
N-BUTYLBENZENE 1.4030 1.298527 7.45 40 0.0050 0.004629 92.60
N-PROPYLBENZENE 2.95 2.760267 6.43 40 0.0050 0.004679 93.60
NAPHTHALENE 1.8860 1.377827 26.90 40 0.0050 0.003627 72.50 54 - 135
O-XYLENE 0.94 0.89193190 5.11 40 0.0050 0.004743 94.90
P-ISOPROPYLTOLUENE 1.74 1.684605 3.18 40 0.0050 0.004840 96.80
SEC-BUTYLBENZENE 2.0680 1.980369 4.24 40 0.0050 0.004789 95.80
STYRENE 1.5610 1.424917 8.72 40 0.0050 0.004564 91.30
TERT-BUTYLBENZENE 1.5440 1.520130 1.55 40 0.0050 0.004922 98.40
TETRACHLOROETHENE 0.54 0.53267230 1.36 40 0.0050 0.004932 98.60
TOLUENE 2.6840 2.481733 7.54 20.49 0.0050 0.004624 92.50
TRANS-1,2-DICHLOROETHENE 0.2780 0.24593130 11.50 40 0.0050 0.004422 88.40
TRANS-1,3-DICHLOROPROPENE 0.8170 0.78068140 4.45 40 0.0050 0.004777 95.50
TRICHLOROETHENE 0.3120 0.28993540 7.07 40 0.0050 0.004646 92.90
TRICHLOROFLUOROMETHANE 0.3480 0.348573 0.1650 40 0.0050 0.005002 100
VINYL CHLORIDE 0.3630 0.32952650 9.22 20.49 0.0050 0.004542 90.80
1,2-DICHLOROETHANE-D4 0.3050 0.29831630 2.19 40 0.0160 0.01563 97.70 70 - 130
4-BROMOFLUOROBENZENE 0.8230 0.86791270 5.46 40 0.0160 0.01688 105 67 - 138
TOLUENE-D8 2.2410 2.353128 5 40 0.0160 0.01680 105 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 432 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/03/24 15:22
Instrument ID:VOCMS42 Calibration (end) date/time:10/03/24 18:40
Lab File ID:1015_02 Analysis date/time:10/15/24 08:43
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5110 0.54909630 7.46 0.0050 0.005373 107
1,1,1-TRICHLOROETHANE 0.38 0.42993310 13.10 0.0050 0.005659 113
1,1,2,2-TETRACHLOROETHANE 0.8820 0.91311840 0.30 3.53 0.0050 0.005178 104
1,1,2-TRICHLOROETHANE 0.5410 0.52001060 3.88 0.0050 0.004810 96.20
1,1,2-TRICHLOROTRIFLUOROETHANE 0.24 0.28066440 16.90 0.0050 0.005844 117
1,1-DICHLOROETHANE 0.5130 0.539759 0.10 5.22 0.0050 0.005258 105
1,1-DICHLOROETHENE 0.4520 0.48559260 7.43 20 0.0050 0.005370 107
1,1-DICHLOROPROPENE 0.33 0.333253 0.9860 0.0050 0.005053 101
1,2,3-TRICHLOROBENZENE 0.4790 0.39691060 17.10 0.0050 0.003945 78.90
1,2,3-TRICHLOROPROPANE 0.2780 0.28486530 2.47 0.0050 0.005116 102
1,2,3-TRIMETHYLBENZENE 1.8940 1.828737 3.45 0.0050 0.004828 96.60
1,2,4-TRICHLOROBENZENE 0.4880 0.41579540 14.80 0.0050 0.004261 85.20
1,2,4-TRIMETHYLBENZENE 1.8760 1.785960 4.80 0.0050 0.004760 95.20
1,2-DIBROMO-3-CHLOROPROPANE 0.2040 0.23029510 12.90 0.0050 0.004594 91.90
1,2-DIBROMOETHANE 0.5840 0.58757660 0.6120 0.0050 0.005027 101
1,2-DICHLOROBENZENE 1.1020 1.067849 3.10 0.0050 0.004847 96.90
1,2-DICHLOROETHANE 0.3930 0.37171250 5.42 0.0050 0.004731 94.60
1,2-DICHLOROPROPANE 0.32 0.31778990 0.6910 20 0.0050 0.004972 99.40
1,3,5-TRIMETHYLBENZENE 1.9020 1.794032 5.68 0.0050 0.004717 94.30
1,3-DICHLOROBENZENE 1.2410 1.157802 6.70 0.0050 0.004665 93.30
1,3-DICHLOROPROPANE 0.9010 0.87814650 2.54 0.0050 0.004871 97.40
1,4-DICHLOROBENZENE 1.2740 1.133666 11 0.0050 0.004450 89
2,2-DICHLOROPROPANE 0.2360 0.32034340 35.70 0.0050 0.006773 135
2-BUTANONE (MEK)0.3090 0.35889160 16.10 0.0250 0.02904 116
2-CHLOROTOLUENE 0.6460 0.60208430 6.80 0.0050 0.004660 93.20
4-CHLOROTOLUENE 2.1860 1.995144 8.73 0.0050 0.004564 91.30
4-METHYL-2-PENTANONE (MIBK)0.9440 1.085201 15 0.0250 0.02875 115
ACETONE 0.0980 0.09487547 3.19 0.0250 0.01920 76.80
ACROLEIN 0.0160 0.01203066 24.80 0.0250 0.01827 73.10
ACRYLONITRILE 0.1590 0.19342230 21.60 0.0250 0.02518 101
BENZENE 1.0370 1.024084 1.25 0.0050 0.004936 98.70
BROMOBENZENE 0.74 0.68899070 6.89 0.0050 0.004658 93.20
BROMODICHLOROMETHANE 0.3270 0.33921290 3.73 0.0050 0.005182 104
BROMOFORM 0.4350 0.47193780 0.10 8.49 0.0050 0.005425 109
BROMOMETHANE 0.1820 0.214301 17.70 0.0050 0.005878 118
CARBON TETRACHLORIDE 0.34 0.389755 14.60 0.0050 0.005737 115
CHLOROBENZENE 1.6750 1.630877 0.30 2.63 0.0050 0.004868 97.40
CHLORODIBROMOMETHANE 0.5840 0.63153710 8.14 0.0050 0.005409 108
CHLOROETHANE 0.2240 0.25984530 16 0.0050 0.005803 116
CHLOROFORM 0.4670 0.47732280 2.21 20 0.0050 0.005110 102
CHLOROMETHANE 0.4670 0.57682860 0.10 23.50 0.0050 0.006172 123
CIS-1,2-DICHLOROETHENE 0.28 0.27498330 1.79 0.0050 0.004909 98.20
CIS-1,3-DICHLOROPROPENE 0.3770 0.37413620 0.76 0.0050 0.004965 99.30
DI-ISOPROPYL ETHER 0.9670 1.013803 4.84 0.0050 0.005241 105
DIBROMOMETHANE 0.1570 0.16673220 6.20 0.0050 0.005316 106
DICHLORODIFLUOROMETHANE 0.2430 0.38476160 58.30 0.0050 0.007906 158
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 433 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/03/24 15:22
Instrument ID:VOCMS42 Calibration (end) date/time:10/03/24 18:40
Lab File ID:1015_02 Analysis date/time:10/15/24 08:43
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.8520 0.83760760 1.69 20 0.0050 0.004916 98.30
HEXACHLORO-1,3-BUTADIENE 0.22 0.19065220 13.30 0.0050 0.004336 86.70
ISOPROPYLBENZENE 2.2930 2.320853 1.21 0.0050 0.005060 101
M&P-XYLENE 1.0470 1.005220 3.99 0.01 0.009602 96
METHYL TERT-BUTYL ETHER 0.5850 0.64598480 10.40 0.0050 0.005519 110
METHYLENE CHLORIDE 0.2780 0.284552 2.36 0.0050 0.005121 102
N-BUTYLBENZENE 1.4030 1.352869 3.57 0.0050 0.004822 96.40
N-PROPYLBENZENE 2.95 2.663091 9.73 0.0050 0.004514 90.30
NAPHTHALENE 1.8860 1.477591 21.70 0.0050 0.003863 77.30
O-XYLENE 0.94 0.98686590 4.99 0.0050 0.005248 105
P-ISOPROPYLTOLUENE 1.74 1.689318 2.91 0.0050 0.004854 97.10
SEC-BUTYLBENZENE 2.0680 1.998947 3.34 0.0050 0.004834 96.70
STYRENE 1.5610 1.529463 2.02 0.0050 0.004899 98
TERT-BUTYLBENZENE 1.5440 1.451922 5.96 0.0050 0.004701 94
TETRACHLOROETHENE 0.54 0.552843 2.38 0.0050 0.005119 102
TOLUENE 2.6840 2.556048 4.77 20 0.0050 0.004762 95.20
TRANS-1,2-DICHLOROETHENE 0.2780 0.278678 0.2440 0.0050 0.005011 100
TRANS-1,3-DICHLOROPROPENE 0.8170 0.80629380 1.31 0.0050 0.004934 98.70
TRICHLOROETHENE 0.3120 0.31348180 0.4750 0.0050 0.005023 100
TRICHLOROFLUOROMETHANE 0.3480 0.43372530 24.60 0.0050 0.006224 124
VINYL CHLORIDE 0.3630 0.41355630 13.90 20 0.0050 0.005700 114
1,2-DICHLOROETHANE-D4 0.3050 0.32338110 6.03 0.0160 0.01694 106 70 - 130
4-BROMOFLUOROBENZENE 0.8230 0.880545 6.99 0.0160 0.01712 107 70 - 130
TOLUENE-D8 2.2410 2.282119 1.83 0.0160 0.01629 102 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 434 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/08/24 22:49
Instrument ID:VOCMS56 Calibration (end) date/time:10/09/24 01:58
Lab File ID:1008a_28 Analysis date/time:10/09/24 03:13
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5570 0.57081160 2.48 40 0.0050 0.005128 103
1,1,1-TRICHLOROETHANE 0.5920 0.60480850 2.16 40 0.0050 0.005109 102
1,1,2,2-TETRACHLOROETHANE 0.8350 0.84354340 0.30 1.02 40 0.0050 0.005049 101
1,1,2-TRICHLOROETHANE 0.54 0.50547760 6.39 40 0.0050 0.004685 93.70
1,1,2-TRICHLOROTRIFLUOROETHANE 0.3350 0.32876510 1.86 40 0.0050 0.004909 98.20
1,1-DICHLOROETHANE 0.5760 0.60273190 0.10 4.64 40 0.0050 0.005235 105
1,1-DICHLOROETHENE 0.5140 0.49311270 4.06 20.49 0.0050 0.004795 95.90
1,1-DICHLOROPROPENE 0.46 0.47375660 2.99 40 0.0050 0.005151 103
1,2,3-TRICHLOROBENZENE 0.2760 0.33305080 20.70 40 0.0050 0.005755 115
1,2,3-TRICHLOROPROPANE 0.2560 0.281645 10 40 0.0050 0.005496 110
1,2,3-TRIMETHYLBENZENE 1.7980 1.889721 5.10 40 0.0050 0.005254 105
1,2,4-TRICHLOROBENZENE 0.3220 0.39634140 23.10 40 0.0050 0.006145 123
1,2,4-TRIMETHYLBENZENE 1.70 1.845740 8.57 40 0.0050 0.005428 109
1,2-DIBROMO-3-CHLOROPROPANE 0.1630 0.19346020 18.70 40 0.0050 0.005930 119 58 - 134
1,2-DIBROMOETHANE 0.5380 0.57686580 7.22 40 0.0050 0.005358 107
1,2-DICHLOROBENZENE 0.9890 1.011966 2.32 40 0.0050 0.005116 102
1,2-DICHLOROETHANE 0.5130 0.48443480 5.57 40 0.0050 0.004722 94.40
1,2-DICHLOROPROPANE 0.3160 0.31966850 1.16 20.49 0.0050 0.005052 101
1,3,5-TRIMETHYLBENZENE 1.8680 1.914410 2.48 40 0.0050 0.005125 103
1,3-DICHLOROBENZENE 1.0230 1.050476 2.69 40 0.0050 0.005135 103
1,3-DICHLOROPROPANE 0.8410 0.84036290 0.0758 40 0.0050 0.004998 100
1,4-DICHLOROBENZENE 1.0930 1.106074 1.20 40 0.0050 0.005059 101
2,2-DICHLOROPROPANE 0.4760 0.47112250 1.02 40 0.0050 0.004951 99
2-BUTANONE (MEK)0.16 0.18609980 16.30 40 0.0250 0.02698 108 44 - 160
2-CHLOROTOLUENE 0.5420 0.58777840 8.45 40 0.0050 0.004928 98.60
4-CHLOROTOLUENE 1.58 1.699741 7.58 40 0.0050 0.005377 108
4-METHYL-2-PENTANONE (MIBK)0.6290 0.68816160 9.41 40 0.0250 0.02737 109 68 - 142
ACETONE 0.0920 0.10890860 18.40 40 0.0250 0.02971 119 19 - 160
ACROLEIN 0.01 0.01496783 49.70 40 0.0250 0.03788 152 10 - 160
ACRYLONITRILE 0.1380 0.15775710 14.30 40 0.0250 0.02849 114
BENZENE 1.2910 1.305218 1.10 40 0.0050 0.005055 101
BROMOBENZENE 0.6530 0.68051540 4.21 40 0.0050 0.005209 104
BROMODICHLOROMETHANE 0.4770 0.48408770 1.49 40 0.0050 0.005077 102
BROMOFORM 0.4690 0.50011620 0.10 6.63 40 0.0050 0.005327 107
BROMOMETHANE 0.4470 0.38992460 12.80 40 0.0050 0.004359 87.20 10 - 160
CARBON TETRACHLORIDE 0.6060 0.61573450 1.61 40 0.0050 0.005083 102
CHLOROBENZENE 1.5680 1.570169 0.30 0.1380 40 0.0050 0.005007 100
CHLORODIBROMOMETHANE 0.5980 0.62061290 3.78 40 0.0050 0.005189 104
CHLOROETHANE 0.2810 0.264982 5.70 40 0.0050 0.004712 94.20 47 - 150
CHLOROFORM 0.7130 0.721940 1.25 20.49 0.0050 0.005060 101
CHLOROMETHANE 0.6130 0.56029670 0.10 8.60 40 0.0050 0.004569 91.40
CIS-1,2-DICHLOROETHENE 0.3820 0.40181530 5.19 40 0.0050 0.005254 105
CIS-1,3-DICHLOROPROPENE 0.4540 0.50183640 10.50 40 0.0050 0.005525 111
DI-ISOPROPYL ETHER 0.8440 0.89119990 5.59 40 0.0050 0.005278 106
DIBROMOMETHANE 0.2380 0.25930270 8.95 40 0.0050 0.005439 109
DICHLORODIFLUOROMETHANE 0.4670 0.43189490 7.52 40 0.0050 0.004627 92.50 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 435 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/08/24 22:49
Instrument ID:VOCMS56 Calibration (end) date/time:10/09/24 01:58
Lab File ID:1008a_28 Analysis date/time:10/09/24 03:13
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.7780 0.83537150 7.37 20.49 0.0050 0.004982 99.60
HEXACHLORO-1,3-BUTADIENE 0.1910 0.22450410 17.50 40 0.0050 0.005887 118
ISOPROPYLBENZENE 2.2920 2.152225 6.10 40 0.0050 0.004694 93.90
M&P-XYLENE 0.9160 1.018515 11.20 40 0.01 0.01112 111
METHYL TERT-BUTYL ETHER 0.90 0.97613640 8.46 40 0.0050 0.005422 108
METHYLENE CHLORIDE 0.3810 0.38833030 1.92 40 0.0050 0.005095 102
N-BUTYLBENZENE 1.3160 1.355771 3.02 40 0.0050 0.005151 103
N-PROPYLBENZENE 2.6770 2.701893 0.93 40 0.0050 0.005047 101
NAPHTHALENE 0.9870 1.149899 16.50 40 0.0050 0.005090 102 54 - 135
O-XYLENE 0.9070 0.97709640 7.73 40 0.0050 0.005385 108
P-ISOPROPYLTOLUENE 1.6060 1.670755 4.03 40 0.0050 0.004724 94.50
SEC-BUTYLBENZENE 1.94 1.996977 2.94 40 0.0050 0.005147 103
STYRENE 1.5040 1.607909 6.91 40 0.0050 0.005345 107
TERT-BUTYLBENZENE 1.3650 1.428961 4.69 40 0.0050 0.005235 105
TETRACHLOROETHENE 0.4940 0.47456440 3.93 40 0.0050 0.004806 96.10
TOLUENE 2.3120 2.253228 2.54 20.49 0.0050 0.004872 97.40
TRANS-1,2-DICHLOROETHENE 0.3580 0.36800890 2.80 40 0.0050 0.005137 103
TRANS-1,3-DICHLOROPROPENE 0.7790 0.77802080 0.1260 40 0.0050 0.004992 99.80
TRICHLOROETHENE 0.3590 0.37935510 5.67 40 0.0050 0.005285 106
TRICHLOROFLUOROMETHANE 0.67 0.60935960 9.05 40 0.0050 0.004545 90.90
VINYL CHLORIDE 0.4820 0.42701790 11.40 20.49 0.0050 0.004427 88.50
1,2-DICHLOROETHANE-D4 0.3490 0.33614430 3.68 40 0.0160 0.01540 96.30 70 - 130
4-BROMOFLUOROBENZENE 0.9060 0.93792010 3.52 40 0.0160 0.01657 104 67 - 138
TOLUENE-D8 1.8540 1.868881 0.8030 40 0.0160 0.01613 101 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 436 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/08/24 22:49
Instrument ID:VOCMS56 Calibration (end) date/time:10/09/24 01:58
Lab File ID:1011a_03 Analysis date/time:10/12/24 03:47
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.5570 0.55391020 0.5550 0.0050 0.004976 99.50
1,1,1-TRICHLOROETHANE 0.5920 0.53768530 9.17 0.0050 0.004542 90.80
1,1,2,2-TETRACHLOROETHANE 0.8350 0.95964960 0.30 14.90 0.0050 0.005744 115
1,1,2-TRICHLOROETHANE 0.54 0.52627370 2.54 0.0050 0.004877 97.50
1,1,2-TRICHLOROTRIFLUOROETHANE 0.3350 0.27199270 18.80 0.0050 0.004061 81.20
1,1-DICHLOROETHANE 0.5760 0.48855770 0.10 15.20 0.0050 0.004243 84.90
1,1-DICHLOROETHENE 0.5140 0.44776210 12.90 20 0.0050 0.004354 87.10
1,1-DICHLOROPROPENE 0.46 0.38253840 16.80 0.0050 0.004160 83.20
1,2,3-TRICHLOROBENZENE 0.2760 0.31163490 12.90 0.0050 0.005395 108
1,2,3-TRICHLOROPROPANE 0.2560 0.30363860 18.60 0.0050 0.005926 119
1,2,3-TRIMETHYLBENZENE 1.7980 2.074275 15.40 0.0050 0.005768 115
1,2,4-TRICHLOROBENZENE 0.3220 0.36119520 12.20 0.0050 0.005600 112
1,2,4-TRIMETHYLBENZENE 1.70 2.048604 20.50 0.0050 0.006025 121
1,2-DIBROMO-3-CHLOROPROPANE 0.1630 0.16980460 4.17 0.0050 0.005205 104
1,2-DIBROMOETHANE 0.5380 0.56460950 4.95 0.0050 0.005244 105
1,2-DICHLOROBENZENE 0.9890 1.045883 5.75 0.0050 0.005288 106
1,2-DICHLOROETHANE 0.5130 0.40881710 20.30 0.0050 0.003985 79.70
1,2-DICHLOROPROPANE 0.3160 0.27298870 13.60 20 0.0050 0.004314 86.30
1,3,5-TRIMETHYLBENZENE 1.8680 2.149184 15.10 0.0050 0.005753 115
1,3-DICHLOROBENZENE 1.0230 1.115955 9.09 0.0050 0.005455 109
1,3-DICHLOROPROPANE 0.8410 0.86678410 3.07 0.0050 0.005155 103
1,4-DICHLOROBENZENE 1.0930 1.176752 7.66 0.0050 0.005383 108
2,2-DICHLOROPROPANE 0.4760 0.40810590 14.30 0.0050 0.004288 85.80
2-BUTANONE (MEK)0.16 0.15568350 2.70 0.0250 0.02277 91.10
2-CHLOROTOLUENE 0.5420 0.66246260 22.20 0.0050 0.005549 111
4-CHLOROTOLUENE 1.58 1.891617 19.70 0.0050 0.005984 120
4-METHYL-2-PENTANONE (MIBK)0.6290 0.69668270 10.80 0.0250 0.02771 111
ACETONE 0.0920 0.07778735 15.40 0.0250 0.02122 84.90
ACROLEIN 0.01 0.01113946 11.40 0.0250 0.02819 113
ACRYLONITRILE 0.1380 0.12580560 8.84 0.0250 0.02272 90.90
BENZENE 1.2910 1.083633 16.10 0.0050 0.004197 83.90
BROMOBENZENE 0.6530 0.74487120 14.10 0.0050 0.005701 114
BROMODICHLOROMETHANE 0.4770 0.41540990 12.90 0.0050 0.004356 87.10
BROMOFORM 0.4690 0.46905630 0.10 0.0120 0.0050 0.004996 99.90
BROMOMETHANE 0.4470 0.35136050 21.40 0.0050 0.003928 78.60
CARBON TETRACHLORIDE 0.6060 0.527626 12.90 0.0050 0.004355 87.10
CHLOROBENZENE 1.5680 1.553925 0.30 0.8980 0.0050 0.004955 99.10
CHLORODIBROMOMETHANE 0.5980 0.61544630 2.92 0.0050 0.005146 103
CHLOROETHANE 0.2810 0.22271560 20.70 0.0050 0.003960 79.20
CHLOROFORM 0.7130 0.58137270 18.50 20 0.0050 0.004075 81.50
CHLOROMETHANE 0.6130 0.45826570 0.10 25.20 0.0050 0.003737 74.70
CIS-1,2-DICHLOROETHENE 0.3820 0.32921010 13.80 0.0050 0.004304 86.10
CIS-1,3-DICHLOROPROPENE 0.4540 0.43009790 5.26 0.0050 0.004736 94.70
DI-ISOPROPYL ETHER 0.8440 0.75617040 10.40 0.0050 0.004478 89.60
DIBROMOMETHANE 0.2380 0.20247870 14.90 0.0050 0.004247 84.90
DICHLORODIFLUOROMETHANE 0.4670 0.39841270 14.70 0.0050 0.004268 85.40
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 437 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/08/24 22:49
Instrument ID:VOCMS56 Calibration (end) date/time:10/09/24 01:58
Lab File ID:1011a_03 Analysis date/time:10/12/24 03:47
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.7780 0.82702920 6.30 20 0.0050 0.004932 98.60 80 - 120
HEXACHLORO-1,3-BUTADIENE 0.1910 0.20398450 6.80 0.0050 0.005349 107
ISOPROPYLBENZENE 2.2920 2.367629 3.30 0.0050 0.005164 103
M&P-XYLENE 0.9160 1.024216 11.80 0.01 0.01118 112
METHYL TERT-BUTYL ETHER 0.90 0.82275870 8.58 0.0050 0.004570 91.40
METHYLENE CHLORIDE 0.3810 0.31454940 17.40 0.0050 0.004127 82.50
N-BUTYLBENZENE 1.3160 1.504406 14.30 0.0050 0.005716 114
N-PROPYLBENZENE 2.6770 2.981967 11.40 0.0050 0.005570 111
NAPHTHALENE 0.9870 1.039620 5.33 0.0050 0.004634 92.70
O-XYLENE 0.9070 0.96214230 6.08 0.0050 0.005302 106
P-ISOPROPYLTOLUENE 1.6060 1.862650 16 0.0050 0.005255 105
SEC-BUTYLBENZENE 1.94 2.297123 18.40 0.0050 0.005920 118
STYRENE 1.5040 1.530433 1.76 0.0050 0.005087 102
TERT-BUTYLBENZENE 1.3650 1.625445 19.10 0.0050 0.005954 119
TETRACHLOROETHENE 0.4940 0.48793140 1.23 0.0050 0.004941 98.80
TOLUENE 2.3120 2.418373 4.60 20 0.0050 0.005229 105
TRANS-1,2-DICHLOROETHENE 0.3580 0.30423810 15 0.0050 0.004247 84.90
TRANS-1,3-DICHLOROPROPENE 0.7790 0.84427980 8.38 0.0050 0.005418 108
TRICHLOROETHENE 0.3590 0.30681750 14.50 0.0050 0.004274 85.50
TRICHLOROFLUOROMETHANE 0.67 0.58774110 12.30 0.0050 0.004384 87.70
VINYL CHLORIDE 0.4820 0.396801 17.70 20 0.0050 0.004114 82.30
1,2-DICHLOROETHANE-D4 0.3490 0.34015770 2.53 0.0160 0.01558 97.40 70 - 130
4-BROMOFLUOROBENZENE 0.9060 0.87059390 3.91 0.0160 0.01538 96.10 70 - 130
TOLUENE-D8 1.8540 2.097493 13.10 0.0160 0.01810 113 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 438 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 18:03
Instrument ID:VOCMS59 Calibration (end) date/time:10/07/24 21:19
Lab File ID:1007_18 Analysis date/time:10/07/24 22:36
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.7650 0.71104490 7.05 40 0.0050 0.004645 92.90
1,1,1-TRICHLOROETHANE 0.5830 0.59158780 1.47 40 0.0050 0.005036 101
1,1,2,2-TETRACHLOROETHANE 1.6050 1.490691 0.30 7.12 40 0.0050 0.004642 92.80
1,1,2-TRICHLOROETHANE 0.7820 0.66091130 15.50 40 0.0050 0.004227 84.50
1,1,2-TRICHLOROTRIFLUOROETHANE 0.28 0.31275590 11.70 40 0.0050 0.005582 112
1,1-DICHLOROETHANE 0.7820 0.80689820 0.10 3.18 40 0.0050 0.005161 103
1,1-DICHLOROETHENE 0.6060 0.65758130 8.51 20.49 0.0050 0.005426 109
1,1-DICHLOROPROPENE 0.4390 0.47248580 7.63 40 0.0050 0.005383 108
1,2,3-TRICHLOROBENZENE 0.8590 0.83207960 3.13 40 0.0050 0.004842 96.80
1,2,3-TRICHLOROPROPANE 0.4510 0.47209350 4.68 40 0.0050 0.005236 105
1,2,3-TRIMETHYLBENZENE 3.4620 3.313421 4.29 40 0.0050 0.004785 95.70
1,2,4-TRICHLOROBENZENE 0.9210 0.89710410 2.59 40 0.0050 0.004870 97.40
1,2,4-TRIMETHYLBENZENE 3.3710 3.220965 4.45 40 0.0050 0.004777 95.50
1,2-DIBROMO-3-CHLOROPROPANE 0.3650 0.33988530 6.88 40 0.0050 0.004656 93.10 58 - 134
1,2-DIBROMOETHANE 0.8670 0.766337 11.60 40 0.0050 0.004420 88.40
1,2-DICHLOROBENZENE 1.7280 1.657583 4.08 40 0.0050 0.004796 95.90
1,2-DICHLOROETHANE 0.6070 0.561209 7.54 40 0.0050 0.004624 92.50
1,2-DICHLOROPROPANE 0.4610 0.42737030 7.29 20.49 0.0050 0.004639 92.80
1,3,5-TRIMETHYLBENZENE 3.0910 3.037977 1.72 40 0.0050 0.004914 98.30
1,3-DICHLOROBENZENE 1.7260 1.720852 0.2980 40 0.0050 0.004984 99.70
1,3-DICHLOROPROPANE 1.2990 1.189633 8.42 40 0.0050 0.004580 91.60
1,4-DICHLOROBENZENE 1.8260 1.738518 4.79 40 0.0050 0.004759 95.20
2,2-DICHLOROPROPANE 0.4450 0.465039 4.50 40 0.0050 0.005316 106
2-BUTANONE (MEK)0.35 0.35106260 0.3040 40 0.0250 0.02507 100 44 - 160
2-CHLOROTOLUENE 0.9580 0.93255750 2.66 40 0.0050 0.004866 97.30
4-CHLOROTOLUENE 3.0160 2.975558 1.34 40 0.0050 0.004933 98.70
4-METHYL-2-PENTANONE (MIBK)1.66 1.595417 3.89 40 0.0250 0.02403 96.10 68 - 142
ACETONE 0.2490 0.215253 13.60 40 0.0250 0.03004 120 19 - 160
ACROLEIN 0.0390 0.06263071 60.60 40 0.0250 0.05810 232 10 - 160
ACRYLONITRILE 0.29 0.30141610 3.94 40 0.0250 0.02603 104
BENZENE 1.4270 1.365777 4.29 40 0.0050 0.004785 95.70
BROMOBENZENE 1.0740 0.94701320 11.80 40 0.0050 0.004408 88.20
BROMODICHLOROMETHANE 0.5290 0.46065580 12.90 40 0.0050 0.004359 87.20
BROMOFORM 0.6120 0.54933760 0.10 10.20 40 0.0050 0.004487 89.70
BROMOMETHANE 0.2930 0.30899020 5.46 40 0.0050 0.005271 105 10 - 160
CARBON TETRACHLORIDE 0.5150 0.54933140 6.67 40 0.0050 0.005329 107
CHLOROBENZENE 2.1090 1.973591 0.30 6.42 40 0.0050 0.004678 93.60
CHLORODIBROMOMETHANE 0.8280 0.72984950 11.90 40 0.0050 0.004409 88.20
CHLOROETHANE 0.2660 0.278701 4.77 40 0.0050 0.005239 105 47 - 150
CHLOROFORM 0.7020 0.70196950 0.00435
0 20.49 0.0050 0.004999 100
CHLOROMETHANE 0.6750 0.66467660 0.10 1.53 40 0.0050 0.004924 98.50
CIS-1,2-DICHLOROETHENE 0.4030 0.42818450 6.25 40 0.0050 0.005306 106
CIS-1,3-DICHLOROPROPENE 0.5850 0.52406460 10.40 40 0.0050 0.004481 89.60
DI-ISOPROPYL ETHER 1.6280 1.632120 0.2530 40 0.0050 0.005013 100
DIBROMOMETHANE 0.2640 0.268703 1.78 40 0.0050 0.005093 102
DICHLORODIFLUOROMETHANE 0.4650 0.428774 7.79 40 0.0050 0.003967 79.30 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 439 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 18:03
Instrument ID:VOCMS59 Calibration (end) date/time:10/07/24 21:19
Lab File ID:1007_18 Analysis date/time:10/07/24 22:36
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.1380 1.101724 3.19 20.49 0.0050 0.004842 96.80
HEXACHLORO-1,3-BUTADIENE 0.4090 0.41103140 0.4970 40 0.0050 0.005025 101
ISOPROPYLBENZENE 3.2780 2.808397 14.30 40 0.0050 0.004284 85.70
M&P-XYLENE 1.3930 1.309884 5.97 40 0.01 0.009403 94
METHYL TERT-BUTYL ETHER 1.0520 1.073269 2.02 40 0.0050 0.005099 102
METHYLENE CHLORIDE 0.4120 0.41275530 0.1830 40 0.0050 0.005006 100
N-BUTYLBENZENE 2.6240 2.585474 1.47 40 0.0050 0.004926 98.50
N-PROPYLBENZENE 4.4560 4.257466 4.46 40 0.0050 0.004777 95.50
NAPHTHALENE 3.3770 3.250991 3.73 40 0.0050 0.004814 96.30 54 - 135
O-XYLENE 1.3960 1.348534 3.40 40 0.0050 0.004831 96.60
P-ISOPROPYLTOLUENE 3.0030 2.796339 6.88 40 0.0050 0.004656 93.10
SEC-BUTYLBENZENE 3.2350 3.289244 1.68 40 0.0050 0.005084 102
STYRENE 2.4320 2.282790 6.14 40 0.0050 0.004693 93.90
TERT-BUTYLBENZENE 2.4390 2.212862 9.27 40 0.0050 0.004536 90.70
TETRACHLOROETHENE 0.59 0.56598520 4.07 40 0.0050 0.004673 93.50
TOLUENE 3.2240 3.052085 5.33 20.49 0.0050 0.004734 94.70
TRANS-1,2-DICHLOROETHENE 0.39 0.40160370 2.98 40 0.0050 0.005152 103
TRANS-1,3-DICHLOROPROPENE 1.2120 1.102747 9.01 40 0.0050 0.004550 91
TRICHLOROETHENE 0.3470 0.33508090 3.43 40 0.0050 0.004834 96.70
TRICHLOROFLUOROMETHANE 0.4580 0.47826360 4.42 40 0.0050 0.004610 92.20
VINYL CHLORIDE 0.6380 0.51137270 19.80 20.49 0.0050 0.004254 85.10
1,2-DICHLOROETHANE-D4 0.3490 0.34892160 0.0225 40 0.0160 0.01600 100 70 - 130
4-BROMOFLUOROBENZENE 0.9270 0.92709670 0.0104 40 0.0160 0.01600 100 67 - 138
TOLUENE-D8 2.15 2.136450 0.63 40 0.0160 0.01590 99.40 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 440 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 18:03
Instrument ID:VOCMS59 Calibration (end) date/time:10/07/24 21:19
Lab File ID:1011_02 Analysis date/time:10/11/24 00:38
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.7650 0.71727450 6.24 20 0.0050 0.004685 93.70
1,1,1-TRICHLOROETHANE 0.5830 0.66873880 14.70 0.0050 0.005693 114 80 - 120
1,1,2,2-TETRACHLOROETHANE 1.6050 1.558097 0.30 2.92 20 0.0050 0.004852 97
1,1,2-TRICHLOROETHANE 0.7820 0.73828260 5.59 20 0.0050 0.004722 94.40
1,1,2-TRICHLOROTRIFLUOROETHANE 0.28 0.40277750 43.80 20 0.0050 0.007188 144
1,1-DICHLOROETHANE 0.7820 0.89129880 0.10 14 20 0.0050 0.005701 114
1,1-DICHLOROETHENE 0.6060 0.81473180 34.40 20 0.0050 0.006722 134
1,1-DICHLOROPROPENE 0.4390 0.487545 11.10 20 0.0050 0.005555 111
1,2,3-TRICHLOROBENZENE 0.8590 0.80914750 5.80 20 0.0050 0.004709 94.20
1,2,3-TRICHLOROPROPANE 0.4510 0.49393810 9.52 20 0.0050 0.005478 110
1,2,3-TRIMETHYLBENZENE 3.4620 3.464009 0.0580 20 0.0050 0.005002 100
1,2,4-TRICHLOROBENZENE 0.9210 0.86572250 6 20 0.0050 0.004700 94
1,2,4-TRIMETHYLBENZENE 3.3710 3.407950 1.10 20 0.0050 0.005055 101
1,2-DIBROMO-3-CHLOROPROPANE 0.3650 0.36107020 1.08 20 0.0050 0.004946 98.90
1,2-DIBROMOETHANE 0.8670 0.808354 6.76 20 0.0050 0.004662 93.20
1,2-DICHLOROBENZENE 1.7280 1.724868 0.1810 20 0.0050 0.004990 99.80
1,2-DICHLOROETHANE 0.6070 0.65957930 8.66 20 0.0050 0.005434 109
1,2-DICHLOROPROPANE 0.4610 0.453375 1.65 20 0.0050 0.004921 98.40
1,3,5-TRIMETHYLBENZENE 3.0910 3.224414 4.32 20 0.0050 0.005216 104
1,3-DICHLOROBENZENE 1.7260 1.789126 3.66 20 0.0050 0.005182 104
1,3-DICHLOROPROPANE 1.2990 1.306650 0.5890 20 0.0050 0.005030 101
1,4-DICHLOROBENZENE 1.8260 1.833361 0.4030 20 0.0050 0.005019 100
2,2-DICHLOROPROPANE 0.4450 0.579708 30.30 0.0050 0.006629 133 80 - 120
2-BUTANONE (MEK)0.35 0.42004410 20 20 0.0250 0.03000 120
2-CHLOROTOLUENE 0.9580 0.973564 1.62 20 0.0050 0.005080 102
4-CHLOROTOLUENE 3.0160 3.099262 2.76 20 0.0050 0.005139 103
4-METHYL-2-PENTANONE (MIBK)1.66 1.760605 6.06 20 0.0250 0.02652 106
ACETONE 0.2490 0.21114510 15.20 0.0250 0.02944 118 80 - 120
ACROLEIN 0.0390 0.05447712 39.70 0.0250 0.05059 202 80 - 120
ACRYLONITRILE 0.29 0.32876410 13.40 20 0.0250 0.02839 114
BENZENE 1.4270 1.451166 1.69 20 0.0050 0.005085 102
BROMOBENZENE 1.0740 1.055410 1.73 20 0.0050 0.004912 98.20
BROMODICHLOROMETHANE 0.5290 0.52774370 0.2370 0.0050 0.004994 99.90 80 - 120
BROMOFORM 0.6120 0.62824460 0.10 2.65 20 0.0050 0.005132 103
BROMOMETHANE 0.2930 0.36810460 25.60 20 0.0050 0.006279 126
CARBON TETRACHLORIDE 0.5150 0.61721550 19.80 20 0.0050 0.005988 120
CHLOROBENZENE 2.1090 1.998717 0.30 5.23 20 0.0050 0.004737 94.70
CHLORODIBROMOMETHANE 0.8280 0.819829 0.9870 20 0.0050 0.004952 99
CHLOROETHANE 0.2660 0.35488450 33.40 20 0.0050 0.006671 133
CHLOROFORM 0.7020 0.81626240 16.30 20 0.0050 0.005813 116
CHLOROMETHANE 0.6750 0.77349570 0.10 14.60 20 0.0050 0.005730 115
CIS-1,2-DICHLOROETHENE 0.4030 0.46102630 14.40 20 0.0050 0.005713 114
CIS-1,3-DICHLOROPROPENE 0.5850 0.59586180 1.86 20 0.0050 0.005094 102
DI-ISOPROPYL ETHER 1.6280 1.848674 13.60 20 0.0050 0.005678 114
DIBROMOMETHANE 0.2640 0.285963 8.32 20 0.0050 0.005420 108
DICHLORODIFLUOROMETHANE 0.4650 0.63778140 37.20 0.0050 0.005824 116 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 441 of 526
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784578 Calibration (begin) date/time:10/07/24 18:03
Instrument ID:VOCMS59 Calibration (end) date/time:10/07/24 21:19
Lab File ID:1011_02 Analysis date/time:10/11/24 00:38
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.1380 1.097453 3.56 20 0.0050 0.004824 96.50
HEXACHLORO-1,3-BUTADIENE 0.4090 0.41218280 0.7780 20 0.0050 0.005039 101
ISOPROPYLBENZENE 3.2780 3.235432 1.30 20 0.0050 0.004935 98.70
M&P-XYLENE 1.3930 1.326992 4.74 20 0.01 0.009526 95.30
METHYL TERT-BUTYL ETHER 1.0520 1.256719 19.50 20 0.0050 0.005971 119
METHYLENE CHLORIDE 0.4120 0.47191990 14.50 20 0.0050 0.005724 114
N-BUTYLBENZENE 2.6240 2.851633 8.68 20 0.0050 0.005433 109
N-PROPYLBENZENE 4.4560 4.596232 3.15 20 0.0050 0.005157 103
NAPHTHALENE 3.3770 3.063895 9.27 20 0.0050 0.004537 90.70
O-XYLENE 1.3960 1.337423 4.20 20 0.0050 0.004791 95.80
P-ISOPROPYLTOLUENE 3.0030 3.059045 1.87 20 0.0050 0.005093 102
SEC-BUTYLBENZENE 3.2350 3.454917 6.80 20 0.0050 0.005340 107
STYRENE 2.4320 2.259524 7.09 20 0.0050 0.004645 92.90
TERT-BUTYLBENZENE 2.4390 2.348620 3.71 20 0.0050 0.004815 96.30
TETRACHLOROETHENE 0.59 0.53260180 9.73 0.0050 0.004398 88 80 - 120
TOLUENE 3.2240 3.128296 2.97 20 0.0050 0.004852 97
TRANS-1,2-DICHLOROETHENE 0.39 0.42751910 9.62 20 0.0050 0.005484 110
TRANS-1,3-DICHLOROPROPENE 1.2120 1.183663 2.34 20 0.0050 0.004883 97.70
TRICHLOROETHENE 0.3470 0.36153130 4.19 20 0.0050 0.005216 104
TRICHLOROFLUOROMETHANE 0.4580 0.67798110 48 0.0050 0.006512 130 80 - 120
VINYL CHLORIDE 0.6380 0.66949580 4.94 20 0.0050 0.005580 112 80 - 120
1,2-DICHLOROETHANE-D4 0.3490 0.375959 7.72 0.0160 0.01724 108 70 - 130
4-BROMOFLUOROBENZENE 0.9270 0.89889820 3.03 0.0160 0.01552 97 70 - 130
TOLUENE-D8 2.15 2.075469 3.47 0.0160 0.01544 96.50 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 442 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16 Calibration Start Date:09/22/24 17:10
Calibration End Date:09/23/24 00:52
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS160922240922_07755006 0922_07 09/22/24 16:25
CAL 0.5 0922_09 09/22/24 17:10
CAL 1 0922_10 09/22/24 17:32
CAL 2 0922_11 09/22/24 17:54
CAL 5.0 0922_12 09/22/24 18:16
CAL 25 0922_13 09/22/24 18:38
CAL 75 0922_14 09/22/24 19:00
CAL 100 0922_15 09/22/24 19:22
CAL 200 0922_16 09/22/24 19:44
SSCV VOCMS160922240922_20755006 0922_20 09/22/24 21:13
CAL .05A 0922_22 09/22/24 21:57
CAL 0.1A 0922_23 09/22/24 22:18
CAL 0.2A 0922_24 09/22/24 22:40
CAL 0.5A 0922_25 09/22/24 23:02
CAL 1A 0922_26 09/22/24 23:24
CAL 5A 0922_27 09/22/24 23:46
CAL 10A 0922_28 09/23/24 00:08
CAL 15A 0922_29 09/23/24 00:30
CAL 20A 0922_30 09/23/24 00:52
TUNE VOCMS161010241010_29T755006 1010_29T 10/10/24 20:43
ICV VOCMS161010241010_31755006 1010_31 10/10/24 21:27
LCS R4131395-1 1010_31LCS 10/10/24 21:27 1 WG2379935
LCS R4131396-1 1010_31LCSA 10/10/24 21:27 1 WG2380092
TUNE VOCMS161010241010_31T755006 1010_31T 10/10/24 21:27
ICV VOCMS161010241010_32755006 1010_32 10/10/24 21:49
LCS R4131396-2 1010_32LCSA 10/10/24 21:49 1 WG2380092
BLANK R4131395-3 1010_34 10/10/24 22:33 1 WG2379935
BLANK R4131396-3 1010_34A 10/10/24 22:33 1 WG2380092
L1784178-04 L1784178-04 1010_35 10/11/24 00:12 1 WG2380092
L1784178-08 L1784178-08 1010_36 10/11/24 00:34 1 WG2380092
L1784693-03 L1784693-03 1010_37 10/11/24 00:56 1 WG2380092
EB-93024 L1784578-17 1010_38 10/11/24 01:18 1 WG2380092
L1782276-08 L1782276-08 1010_39 10/11/24 01:39 1 WG2379935
L1782276-09 L1782276-09 1010_40 10/11/24 02:01 1 WG2379935
L1782276-10 L1782276-10 1010_41 10/11/24 02:23 1 WG2379935
L1782276-11 L1782276-11 1010_42 10/11/24 02:44 1 WG2379935
L1782276-12 L1782276-12 1010_43 10/11/24 03:06 1 WG2379935
L1782276-07 L1782276-07 1010_44 10/11/24 03:28 25 WG2379935
L1782874-09 L1782874-09 1010_45 10/11/24 03:50 20 WG2379935
L1784693-01 L1784693-01 1010_47 10/11/24 04:34 1 WG2380092
L1784693-02 L1784693-02 1010_48 10/11/24 04:55 1 WG2380092
L1784790-01 L1784790-01 1010_50 10/11/24 05:39 1 WG2380092
L1784790-02 L1784790-02 1010_51 10/11/24 06:01 1 WG2380092
L1784790-03 L1784790-03 1010_52 10/11/24 06:23 1 WG2380092
L1784790-04 L1784790-04 1010_53 10/11/24 06:45 1 WG2380092
L1784563-01 L1784563-01 1010_54 10/11/24 07:07 5 WG2380092
L1784563-02 L1784563-02 1010_55 10/11/24 07:29 5 WG2380092
L1784569-01 L1784569-01 1010_56 10/11/24 07:51 500 WG2380092
L1784569-03 L1784569-03 1010_57 10/11/24 08:13 50 WG2380092
L1784569-04 L1784569-04 1010_58 10/11/24 08:34 200 WG2380092
L1784571-01 L1784571-01 1010_59 10/11/24 08:56 1000 WG2380092
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 443 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS16 Calibration Start Date:09/22/24 17:10
Calibration End Date:09/23/24 00:52
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
L1784571-02 L1784571-02 1010_60 10/11/24 09:18 1000 WG2380092
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 444 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS36 Calibration Start Date:09/12/24 18:56
Calibration End Date:09/13/24 17:40
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS360912240912_01752875 0912_01 09/12/24 16:31
CAL 0.5 0912_08 09/12/24 18:56
CAL 1 0912_09 09/12/24 19:17
CAL 2 0912_10 09/12/24 19:38
CAL 5.0 0912_11 09/12/24 19:58
CAL 25 0912_12 09/12/24 20:19
CAL 75 0912_13 09/12/24 20:40
CAL 100 0912_14 09/12/24 21:00
CAL 200 0912_15 09/12/24 21:21
SSCV VOCMS360912240912_19752875 0912_19 09/12/24 22:44
TUNE VOCMS360912240912_21752875 0912_21 09/12/24 23:26
CAL .05A 0912_23 09/13/24 00:08
CAL 0.1A 0912_24 09/13/24 04:34
CAL 0.2A 0912_25 09/13/24 04:55
CAL 0.5A 0912_26 09/13/24 05:16
CAL 1A 0912_27 09/13/24 05:36
CAL 5A 0912_28 09/13/24 05:57
CAL 10A 0912_29 09/13/24 06:18
CAL 15A 0912_30 09/13/24 06:39
CAL 20A 0912_31 09/13/24 07:00
TUNE VOCMS360912240912_36752875 0912_36 09/13/24 09:20
CAL 0.5 0912_39 09/13/24 10:22
CAL 1 0912_40 09/13/24 10:43
CAL 2 0912_41 09/13/24 11:04
CAL 5.0 0912_42 09/13/24 11:25
CAL 25 0912_43 09/13/24 11:45
CAL 75 0912_44 09/13/24 12:06
SSCV VOCMS360912240912_48752875 0912_48 09/13/24 14:12
CAL 0.5 0912_53 09/13/24 15:56
CAL 1 0912_54 09/13/24 16:16
CAL 2 0912_55 09/13/24 16:37
CAL 5.0 0912_56 09/13/24 16:58
CAL 10 0912_57 09/13/24 17:19
CAL 20 0912_58 09/13/24 17:40
TUNE VOCMS361010241010_01T752875 1010_01T 10/10/24 03:27
ICV VOCMS361010241010_02752875 1010_02 10/10/24 03:47
LCS R4132481-1 1010_02LCSA 10/10/24 03:47 1 WG2379334
LCSD R4132481-2 1010_03A 10/10/24 04:07 1 WG2379334
ICV VOCMS361010241010_04752875 1010_04 10/10/24 04:28
BLANK R4132481-3 1010_08A 10/10/24 05:50 1 WG2379334
TRIP BLANK L1784578-18 1010_10 10/10/24 06:31 1 WG2379334
L1784484-14 L1784484-14 1010_12 10/10/24 07:11 1 WG2379334
L1784556-01 L1784556-01 1010_21 10/10/24 07:52 50 WG2379334
L1784556-02 L1784556-02 1010_22 10/10/24 08:13 10 WG2379334
TUNE VOCMS361010241010_36T752875 1010_36T 10/10/24 14:59
TUNE VOCMS361010241010_37T752875 1010_37T 10/10/24 15:20
TUNE VOCMS361010241010_37UT752875 1010_37UT 10/10/24 15:20
TUNE VOCMS361010241011_01T752875 1011_01T 10/11/24 03:18
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 445 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS42 Calibration Start Date:10/03/24 15:22
Calibration End Date:10/03/24 18:40
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS42100324a1003a_01757788 1003a_01 10/03/24 14:22
CAL 0.02 1003A_04 10/03/24 15:22
CAL 0.04 1003A_05 10/03/24 15:42
CAL 0.1 1003A_06 10/03/24 16:02
CAL 0.2 1003A_07 10/03/24 16:21
CAL 0.5 1003A_08 10/03/24 16:41
CAL 1 1003A_09 10/03/24 17:01
CAL 2 1003A_10 10/03/24 17:21
CAL 5.0 1003A_11 10/03/24 17:41
CAL 25 1003A_12 10/03/24 18:01
CAL 75 1003A_13 10/03/24 18:21
CAL 100 1003A_14 10/03/24 18:40
SSCV VOCMS42100324a1003a_18757788 1003a_18 10/03/24 19:59
ICV VOCMS421015241015_02757788 1015_02 10/15/24 08:43
LCS R4133124-1 1015_02LCSA 10/15/24 08:43 1 WG2381936
TUNE VOCMS421015241015_02T757788 1015_02T 10/15/24 08:43
LCS R4133127-1 1015_02LCSB 10/15/24 08:43 1 WG2382244
LCSD R4133124-2 1015_03A 10/15/24 09:03 1 WG2381936
LCSD R4133127-2 1015_03B 10/15/24 09:03 1 WG2382244
BLANK R4133124-3 1015_05A 10/15/24 09:42 1 WG2381936
BLANK R4133127-3 1015_05B 10/15/24 09:42 1 WG2382244
TRIP BLANK L1784578-18 1015_06 10/15/24 10:43 1 WG2381936
L1784484-14 L1784484-14 1015_08 10/15/24 11:22 1 WG2381936
L1787382-01 L1787382-01 1015_10 10/15/24 12:02 1 WG2382244
L1787348-01 L1787348-01 1015_12 10/15/24 12:41 10 WG2382244
L1784556-01 L1784556-01 1015_13 10/15/24 13:00 1000 WG2381936
L1784556-02 L1784556-02 1015_14 10/15/24 13:19 500 WG2381936
TUNE VOCMS421015241015_28T757788 1015_28T 10/15/24 17:55
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 446 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS56 Calibration Start Date:10/08/24 22:49
Calibration End Date:10/09/24 01:58
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS56100824a1008a_11758896 1008a_11 10/08/24 21:52
CAL 0.02 1008A_14 10/08/24 22:49
CAL 0.04 1008A_15 10/08/24 23:08
CAL 0.1 1008A_16 10/08/24 23:27
CAL 0.2 1008A_17 10/08/24 23:46
CAL 0.5 1008A_18 10/09/24 00:04
CAL 2 1008A_20 10/09/24 00:42
CAL 5.0 1008A_21 10/09/24 01:01
CAL 25 1008A_22 10/09/24 01:20
CAL 75 1008A_23 10/09/24 01:39
CAL 100 1008A_24 10/09/24 01:58
SSCV VOCMS56100824a1008a_28758896 1008a_28 10/09/24 03:13
TUNE VOCMS56101124a1011a_01T758896 1011a_01T 10/12/24 03:09
ICV VOCMS56101124a1011a_03758896 1011a_03 10/12/24 03:47
LCS R4132124-1 1011a_03LCSA 10/12/24 03:47 1 WG2379121
LCS R4132125-1 1011a_03LCS 10/12/24 03:47 1 WG2380545
BLANK R4132124-2 1011a_06A 10/12/24 04:44 1 WG2379121
BLANK R4132125-2 1011a_06 10/12/24 04:44 1 WG2380545
L1784539-01 L1784539-01 1011a_07 10/12/24 05:03 1 WG2380545
L1784539-02 L1784539-02 1011a_08 10/12/24 05:22 1 WG2380545
L1784539-03 L1784539-03 1011a_09 10/12/24 05:40 1 WG2380545
L1784539-04 L1784539-04 1011a_10 10/12/24 05:59 1 WG2380545
L1784539-05 L1784539-05 1011a_11 10/12/24 06:18 1 WG2380545
L1784539-06 L1784539-06 1011a_12 10/12/24 06:37 1 WG2380545
L1784539-07 L1784539-07 1011a_13 10/12/24 06:56 1 WG2380545
L1784539-08 L1784539-08 1011a_14 10/12/24 07:15 1 WG2380545
L1784539-09 L1784539-09 1011a_15 10/12/24 07:34 1 WG2380545
S-13 (0-6)L1784578-01 1011a_16 10/12/24 07:53 1 WG2380545
S-32 (0-6)L1784578-03 1011a_17 10/12/24 08:12 1 WG2380545
S-14 (0-6)L1784578-12 1011a_18 10/12/24 08:31 1.1 WG2380545
S-11 (0-6)L1784578-13 1011a_19 10/12/24 08:50 1 WG2380545
S-14 (6-12)L1784578-15 1011a_20 10/12/24 09:09 1.1 WG2380545
L1784968-22 L1784968-22 1011a_21 10/12/24 09:28 1.02 WG2380545
L1784968-23 L1784968-23 1011a_22 10/12/24 09:47 1.09 WG2380545
L1784968-24 L1784968-24 1011a_23 10/12/24 10:06 1 WG2380545
L1784968-25 L1784968-25 1011a_24 10/12/24 10:25 1 WG2380545
L1784968-26 L1784968-26 1011a_25 10/12/24 10:44 1.01 WG2380545
OS L1784968-27 1011a_30 10/12/24 12:19
L1784968-27 L1784968-27 1011a_30 10/12/24 12:19 20 WG2380545
MS R4132125-3 1011a_31 10/12/24 12:38 20 WG2380545
MSD R4132125-4 1011a_32 10/12/24 12:57 20 WG2380545
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 447 of 526
8B-OR ANALYTICAL SEQUENCE
SDG:L1784578 Analytical Method:8260B
Instrument ID:VOCMS59 Calibration Start Date:10/07/24 18:03
Calibration End Date:10/07/24 21:19
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS591007241007_01758651 1007_01 10/07/24 17:05
CAL 0.02 1007_04 10/07/24 18:03
CAL 0.04 1007_05 10/07/24 18:23
CAL 0.1 1007_06 10/07/24 18:43
CAL 0.2 1007_07 10/07/24 19:02
CAL 0.5 1007_08 10/07/24 19:22
CAL 1 1007_09 10/07/24 19:42
CAL 2 1007_10 10/07/24 20:01
CAL 5.0 1007_11 10/07/24 20:21
CAL 25 1007_12 10/07/24 20:40
CAL 75 1007_13 10/07/24 20:59
CAL 100 1007_14 10/07/24 21:19
SSCV VOCMS591007241007_18758651 1007_18 10/07/24 22:36
TUNE VOCMS591011241011_01T758651 1011_01T 10/11/24 00:19
ICV VOCMS591011241011_02758651 1011_02 10/11/24 00:38
LCS R4131341-1 1011_02LCS 10/11/24 00:38 1 WG2379147
LCSD R4131341-2 1011_03 10/11/24 00:57 1 WG2379147
BLANK R4131341-3 1011_07 10/11/24 02:15 1 WG2379147
L1784484-06 L1784484-06 1011_08 10/11/24 02:34 1.08 WG2379147
L1784484-07 L1784484-07 1011_09 10/11/24 02:54 1 WG2379147
L1784484-08 L1784484-08 1011_10 10/11/24 03:14 1 WG2379147
L1784484-09 L1784484-09 1011_11 10/11/24 03:33 1 WG2379147
L1784484-10 L1784484-10 1011_12 10/11/24 03:52 1 WG2379147
L1784484-11 L1784484-11 1011_13 10/11/24 04:12 1 WG2379147
S-15 (0-6)L1784578-02 1011_19 10/11/24 06:08 1.08 WG2379147
S-12 (6-12)L1784578-04 1011_20 10/11/24 06:28 1 WG2379147
S-12 (0-6)L1784578-05 1011_21 10/11/24 06:47 1 WG2379147
S-10 (0-6)L1784578-06 1011_22 10/11/24 07:07 1.13 WG2379147
S-10 (6-12)L1784578-11 1011_23 10/11/24 07:26 1.12 WG2379147
L1784968-32 L1784968-32 1011_24 10/11/24 07:46 1 WG2379147
L1784968-33 L1784968-33 1011_25 10/11/24 08:05 1.01 WG2379147
L1784968-34 L1784968-34 1011_26 10/11/24 08:25 1 WG2379147
MS R4131341-4 1011_28 10/11/24 09:04 1.13 WG2379147
MSD R4131341-5 1011_29 10/11/24 09:24 1.13 WG2379147
TUNE VOCMS591011241011_30T758651 1011_30T 10/11/24 09:43
TUNE VOCMS591011241011_57T758651 1011_57T 10/11/24 20:08
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 448 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17,18 Analytical Method:8260B
Matrix:GW Prep Method:8260B
Analyte CAS MDL RDL
mg/l mg/l
n-Butylbenzene 104-51-8 0.000157 0.0010
sec-Butylbenzene 135-98-8 0.000125 0.0010
tert-Butylbenzene 98-06-6 0.000127 0.0010
Carbon tetrachloride 56-23-5 0.000128 0.0010
Chlorobenzene 108-90-7 0.000116 0.0010
Chlorodibromomethane 124-48-1 0.000140 0.0010
Chloroethane 75-00-3 0.000192 0.0050
Chloroform 67-66-3 0.000111 0.0050
Chloromethane 74-87-3 0.000960 0.0025
Acetone 67-64-1 0.0113 0.05
2-Chlorotoluene 95-49-8 0.000106 0.0010
4-Chlorotoluene 106-43-4 0.000114 0.0010
1,2-Dibromo-3-Chloropropane 96-12-8 0.000276 0.0050
1,2-Dibromoethane 106-93-4 0.000126 0.0010
Dibromomethane 74-95-3 0.000122 0.0010
1,2-Dichlorobenzene 95-50-1 0.000107 0.0010
1,3-Dichlorobenzene 541-73-1 0.000110 0.0010
1,4-Dichlorobenzene 106-46-7 0.000120 0.0010
Dichlorodifluoromethane 75-71-8 0.000374 0.0050
1,1-Dichloroethane 75-34-3 0.0001 0.0010
Acrolein 107-02-8 0.002540 0.05
1,2-Dichloroethane 107-06-2 0.00008190 0.0010
1,1-Dichloroethene 75-35-4 0.000188 0.0010
cis-1,2-Dichloroethene 156-59-2 0.000126 0.0010
trans-1,2-Dichloroethene 156-60-5 0.000149 0.0010
1,2-Dichloropropane 78-87-5 0.000149 0.0010
1,1-Dichloropropene 563-58-6 0.000142 0.0010
1,3-Dichloropropane 142-28-9 0.000110 0.0010
cis-1,3-Dichloropropene 10061-01-5 0.000111 0.0010
trans-1,3-Dichloropropene 10061-02-6 0.000118 0.0010
2,2-Dichloropropane 594-20-7 0.000161 0.0010
Acrylonitrile 107-13-1 0.000671 0.01
Di-isopropyl ether 108-20-3 0.000105 0.0010
Ethylbenzene 100-41-4 0.000137 0.0010
Hexachloro-1,3-butadiene 87-68-3 0.000337 0.0010
Isopropylbenzene 98-82-8 0.000105 0.0010
p-Isopropyltoluene 99-87-6 0.000120 0.0010
2-Butanone (MEK)78-93-3 0.001190 0.01
Methylene Chloride 75-09-2 0.000430 0.0050
4-Methyl-2-pentanone (MIBK)108-10-1 0.000478 0.01
Methyl tert-butyl ether 1634-04-4 0.000101 0.0010
Naphthalene 91-20-3 0.0010 0.0050
Benzene 71-43-2 0.00009410 0.0010
n-Propylbenzene 103-65-1 0.00009930 0.0010
Styrene 100-42-5 0.000118 0.0010
1,1,1,2-Tetrachloroethane 630-20-6 0.000147 0.0010
1,1,2,2-Tetrachloroethane 79-34-5 0.000133 0.0010
1,1,2-Trichlorotrifluoroethane 76-13-1 0.000180 0.0010
Tetrachloroethene 127-18-4 0.0003 0.0010
Toluene 108-88-3 0.000278 0.0010
1,2,3-Trichlorobenzene 87-61-6 0.000230 0.0010
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 449 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-17,18 Analytical Method:8260B
Matrix:GW Prep Method:8260B
Analyte CAS MDL RDL
mg/l mg/l
1,2,4-Trichlorobenzene 120-82-1 0.000481 0.0010
1,1,1-Trichloroethane 71-55-6 0.000149 0.0010
Bromobenzene 108-86-1 0.000118 0.0010
1,1,2-Trichloroethane 79-00-5 0.000158 0.0010
Trichloroethene 79-01-6 0.000190 0.0010
Trichlorofluoromethane 75-69-4 0.000160 0.0050
1,2,3-Trichloropropane 96-18-4 0.000237 0.0025
1,2,4-Trimethylbenzene 95-63-6 0.000322 0.0010
1,2,3-Trimethylbenzene 526-73-8 0.000104 0.0010
1,3,5-Trimethylbenzene 108-67-8 0.000104 0.0010
Vinyl chloride 75-01-4 0.000234 0.0010
Xylenes, Total 1330-20-7 0.000174 0.0030
Bromodichloromethane 75-27-4 0.000136 0.0010
Bromoform 75-25-2 0.000129 0.0010
Bromomethane 74-83-9 0.000605 0.0050
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 450 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,11,12,13,15 Analytical Method:8260B
Matrix:Solid Prep Method:5035A
Analyte CAS MDL RDL
mg/kg mg/kg
sec-Butylbenzene 135-98-8 0.002880 0.0125
tert-Butylbenzene 98-06-6 0.001950 0.0050
Carbon tetrachloride 56-23-5 0.000898 0.0050
Chlorobenzene 108-90-7 0.000210 0.0025
Chlorodibromomethane 124-48-1 0.000612 0.0025
Chloroethane 75-00-3 0.0017 0.0050
Chloroform 67-66-3 0.001030 0.0025
Chloromethane 74-87-3 0.004350 0.0125
2-Chlorotoluene 95-49-8 0.000865 0.0025
Acetone 67-64-1 0.0365 0.05
4-Chlorotoluene 106-43-4 0.000450 0.0050
1,2-Dibromo-3-Chloropropane 96-12-8 0.0039 0.0250
1,2-Dibromoethane 106-93-4 0.000648 0.0025
Dibromomethane 74-95-3 0.000750 0.0050
1,2-Dichlorobenzene 95-50-1 0.000425 0.0050
1,3-Dichlorobenzene 541-73-1 0.0006 0.0050
1,4-Dichlorobenzene 106-46-7 0.0007 0.0050
Dichlorodifluoromethane 75-71-8 0.001610 0.0050
1,1-Dichloroethane 75-34-3 0.000491 0.0025
1,2-Dichloroethane 107-06-2 0.000649 0.0025
Acrylonitrile 107-13-1 0.003610 0.0125
1,1-Dichloroethene 75-35-4 0.000606 0.0025
cis-1,2-Dichloroethene 156-59-2 0.000734 0.0025
trans-1,2-Dichloroethene 156-60-5 0.001040 0.0050
1,2-Dichloropropane 78-87-5 0.001420 0.0050
1,1-Dichloropropene 563-58-6 0.000809 0.0025
1,3-Dichloropropane 142-28-9 0.000501 0.0050
cis-1,3-Dichloropropene 10061-01-5 0.000757 0.0025
trans-1,3-Dichloropropene 10061-02-6 0.001140 0.0050
2,2-Dichloropropane 594-20-7 0.001380 0.0025
Di-isopropyl ether 108-20-3 0.000410 0.0010
Benzene 71-43-2 0.000467 0.0010
Ethylbenzene 100-41-4 0.000737 0.0025
Hexachloro-1,3-butadiene 87-68-3 0.0060 0.0250
Isopropylbenzene 98-82-8 0.000425 0.0025
p-Isopropyltoluene 99-87-6 0.002550 0.0050
2-Butanone (MEK)78-93-3 0.0635 0.10
Methylene Chloride 75-09-2 0.006640 0.0250
4-Methyl-2-pentanone (MIBK)108-10-1 0.002280 0.0250
Methyl tert-butyl ether 1634-04-4 0.000350 0.0010
Naphthalene 91-20-3 0.004880 0.0125
n-Propylbenzene 103-65-1 0.000950 0.0050
Bromobenzene 108-86-1 0.0009 0.0125
Styrene 100-42-5 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0.000948 0.0025
1,1,2,2-Tetrachloroethane 79-34-5 0.000695 0.0025
1,1,2-Trichlorotrifluoroethane 76-13-1 0.000754 0.0025
Tetrachloroethene 127-18-4 0.000896 0.0025
Toluene 108-88-3 0.0013 0.0050
1,2,3-Trichlorobenzene 87-61-6 0.007330 0.0125
1,2,4-Trichlorobenzene 120-82-1 0.0044 0.0125
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 451 of 526
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,11,12,13,15 Analytical Method:8260B
Matrix:Solid Prep Method:5035A
Analyte CAS MDL RDL
mg/kg mg/kg
1,1,1-Trichloroethane 71-55-6 0.000923 0.0025
1,1,2-Trichloroethane 79-00-5 0.000597 0.0025
Bromodichloromethane 75-27-4 0.000725 0.0025
Trichloroethene 79-01-6 0.000584 0.0010
Trichlorofluoromethane 75-69-4 0.000827 0.0025
1,2,3-Trichloropropane 96-18-4 0.001620 0.0125
1,2,4-Trimethylbenzene 95-63-6 0.001580 0.0050
1,2,3-Trimethylbenzene 526-73-8 0.001580 0.0050
1,3,5-Trimethylbenzene 108-67-8 0.0020 0.0050
Vinyl chloride 75-01-4 0.001160 0.0025
Xylenes, Total 1330-20-7 0.000880 0.0065
Bromoform 75-25-2 0.001170 0.0250
Bromomethane 74-83-9 0.001970 0.0125
n-Butylbenzene 104-51-8 0.005250 0.0125
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-3
Lab Sample ID:R4131341-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1011_07 Received Date/Time:_______________
Instrument ID:VOCMS59 Preparation Date/Time:10/11/24 02:15
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 02:15
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 U 0.0365 0.0500
Acrylonitrile 107-13-1 3.64 U 0.00361 0.0125
Benzene 71-43-2 4.40 U 0.000467 0.00100
Bromobenzene 108-86-1 0 U 0.000900 0.0125
Bromodichloromethane 75-27-4 0 U 0.000725 0.00250
Bromoform 75-25-2 0 U 0.00117 0.0250
Bromomethane 74-83-9 0 U 0.00197 0.0125
n-Butylbenzene 104-51-8 8.56 U 0.00525 0.0125
sec-Butylbenzene 135-98-8 0 U 0.00288 0.0125
tert-Butylbenzene 98-06-6 0 U 0.00195 0.00500
Carbon tetrachloride 56-23-5 0 U 0.000898 0.00500
Chlorobenzene 108-90-7 0 U 0.000210 0.00250
Chlorodibromomethane 124-48-1 0 U 0.000612 0.00250
Chloroethane 75-00-3 0 U 0.00170 0.00500
Chloroform 67-66-3 4.04 U 0.00103 0.00250
Chloromethane 74-87-3 1.86 U 0.00435 0.0125
2-Chlorotoluene 95-49-8 0 U 0.000865 0.00250
4-Chlorotoluene 106-43-4 0 U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00390 0.0250
1,2-Dibromoethane 106-93-4 0 U 0.000648 0.00250
Dibromomethane 74-95-3 0 U 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 0 U 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.36 U 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.36 U 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 0 U 0.00161 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.50 U 0.000649 0.00250
1,1-Dichloroethene 75-35-4 0 U 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.95 U 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 0 U 0.00104 0.00500
1,2-Dichloropropane 78-87-5 0 U 0.00142 0.00500
1,1-Dichloropropene 563-58-6 0 U 0.000809 0.00250
1,3-Dichloropropane 142-28-9 0 U 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.98 U 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.51 U 0.000410 0.00100
Ethylbenzene 100-41-4 0 U 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 0 U 0.00600 0.0250
Isopropylbenzene 98-82-8 0 U 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.22 U 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.22 U 0.0635 0.100
Methylene Chloride 75-09-2 3.11 0.00888 J 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 453 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-3
Lab Sample ID:R4131341-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1011_07 Received Date/Time:_______________
Instrument ID:VOCMS59 Preparation Date/Time:10/11/24 02:15
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 02:15
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 0 U 0.000350 0.00100
Naphthalene 91-20-3 10.19 U 0.00488 0.0125
n-Propylbenzene 103-65-1 0 U 0.000950 0.00500
Styrene 100-42-5 0 U 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000754 0.00250
Tetrachloroethene 127-18-4 0 U 0.000896 0.00250
Toluene 108-88-3 5.62 U 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 0 U 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 0 U 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 0 U 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 0 U 0.000597 0.00250
Trichloroethene 79-01-6 0 U 0.000584 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 0 U 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 0 U 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 0 U 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 0 U 0.00200 0.00500
Vinyl chloride 75-01-4 0 U 0.00116 0.00250
Xylenes, Total 1330-20-7 6.75 U 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 454 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131396-3
Lab Sample ID:R4131396-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1010_34A Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:10/10/24 22:33
Analytical Batch:WG2380092 Analysis Date/Time:10/10/24 22:33
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.15 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131396-3
Lab Sample ID:R4131396-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1010_34A Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:10/10/24 22:33
Analytical Batch:WG2380092 Analysis Date/Time:10/10/24 22:33
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-2
Lab Sample ID:R4132125-2 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1011a_06 Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:10/12/24 04:44
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 04:44
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 U 0.0365 0.0500
Acrylonitrile 107-13-1 0 U 0.00361 0.0125
Benzene 71-43-2 4.40 U 0.000467 0.00100
Bromobenzene 108-86-1 0 U 0.000900 0.0125
Bromodichloromethane 75-27-4 0 U 0.000725 0.00250
Bromoform 75-25-2 7.07 U 0.00117 0.0250
Bromomethane 74-83-9 2.35 U 0.00197 0.0125
n-Butylbenzene 104-51-8 8.50 U 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.03 U 0.00288 0.0125
tert-Butylbenzene 98-06-6 0 U 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.16 U 0.000898 0.00500
Chlorobenzene 108-90-7 0 U 0.000210 0.00250
Chlorodibromomethane 124-48-1 0 U 0.000612 0.00250
Chloroethane 75-00-3 0 U 0.00170 0.00500
Chloroform 67-66-3 0 U 0.00103 0.00250
Chloromethane 74-87-3 0 U 0.00435 0.0125
2-Chlorotoluene 95-49-8 0 U 0.000865 0.00250
4-Chlorotoluene 106-43-4 0 U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.00390 0.0250
1,2-Dibromoethane 106-93-4 0 U 0.000648 0.00250
Dibromomethane 74-95-3 0 U 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.62 U 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.21 U 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.26 0.000775 J 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 0 U 0.00161 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.51 U 0.000649 0.00250
1,1-Dichloroethene 75-35-4 0 U 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.97 U 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 0 U 0.00104 0.00500
1,2-Dichloropropane 78-87-5 0 U 0.00142 0.00500
1,1-Dichloropropene 563-58-6 0 U 0.000809 0.00250
1,3-Dichloropropane 142-28-9 0 U 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 0 U 0.00114 0.00500
2,2-Dichloropropane 594-20-7 0 U 0.00138 0.00250
Di-isopropyl ether 108-20-3 0 U 0.000410 0.00100
Ethylbenzene 100-41-4 0 U 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.77 U 0.00600 0.0250
Isopropylbenzene 98-82-8 0 U 0.000425 0.00250
p-Isopropyltoluene 99-87-6 0 U 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.26 U 0.0635 0.100
Methylene Chloride 75-09-2 3.18 0.0130 J 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-2
Lab Sample ID:R4132125-2 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1011a_06 Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:10/12/24 04:44
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 04:44
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 U 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.34 U 0.000350 0.00100
Naphthalene 91-20-3 10.11 U 0.00488 0.0125
n-Propylbenzene 103-65-1 7.50 U 0.000950 0.00500
Styrene 100-42-5 0 U 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000754 0.00250
Tetrachloroethene 127-18-4 0 U 0.000896 0.00250
Toluene 108-88-3 5.58 U 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.26 U 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.84 U 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 0 U 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 0 U 0.000597 0.00250
Trichloroethene 79-01-6 0 U 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.59 U 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 0 U 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 0 U 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.28 U 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.64 U 0.00200 0.00500
Vinyl chloride 75-01-4 0 U 0.00116 0.00250
Xylenes, Total 1330-20-7 6.99 U 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 458 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132481-3
Lab Sample ID:R4132481-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1010_08A Received Date/Time:_______________
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 05:50
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 05:50
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 0 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132481-3
Lab Sample ID:R4132481-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1010_08A Received Date/Time:_______________
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 05:50
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 05:50
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.03 0.000518 J 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.78 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 460 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133124-3
Lab Sample ID:R4133124-3 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1015_05A Received Date/Time:_______________
Instrument ID:VOCMS42 Preparation Date/Time:10/15/24 09:42
Analytical Batch:WG2381936 Analysis Date/Time:10/15/24 09:42
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Naphthalene 91-20-3 10.60 U 0.00100 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 461 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-1
Lab Sample ID:R4131341-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1011_02LCS Received Date/Time:_______________
Instrument ID:VOCMS59 Preparation Date/Time:10/11/24 00:38
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 00:38
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.12 0.736 0.0365 0.0500
Acrylonitrile 107-13-1 3.59 0.710 0.00361 0.0125
Benzene 71-43-2 4.40 0.127 0.000467 0.00100
Bromobenzene 108-86-1 7.60 0.123 0.000900 0.0125
Bromodichloromethane 75-27-4 5.08 0.125 0.000725 0.00250
Bromoform 75-25-2 7.13 0.128 0.00117 0.0250
Bromomethane 74-83-9 2.20 0.157 0.00197 0.0125
n-Butylbenzene 104-51-8 8.56 0.136 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.12 0.134 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.98 0.120 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.15 0.150 0.000898 0.00500
Chlorobenzene 108-90-7 6.64 0.118 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.12 0.124 0.000612 0.00250
Chloroethane 75-00-3 2.28 0.167 0.00170 0.00500
Chloroform 67-66-3 4.04 0.145 0.00103 0.00250
Chloromethane 74-87-3 1.87 0.143 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.73 0.127 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.85 0.128 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.35 0.124 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.29 0.117 0.000648 0.00250
Dibromomethane 74-95-3 5 0.136 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.71 0.125 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.31 0.130 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.37 0.125 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.67 0.146 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.58 0.143 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.51 0.136 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.74 0.168 J4 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.89 0.143 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.21 0.137 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.05 0.123 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.25 0.139 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.18 0.126 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.46 0.127 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.87 0.122 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.97 0.166 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.48 0.142 0.000410 0.00100
Ethylbenzene 100-41-4 6.65 0.121 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.88 0.126 0.00600 0.0250
Isopropylbenzene 98-82-8 7.28 0.123 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.22 0.127 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.20 0.750 0.0635 0.100
Methylene Chloride 75-09-2 3.11 0.143 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 462 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-1
Lab Sample ID:R4131341-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1011_02LCS Received Date/Time:_______________
Instrument ID:VOCMS59 Preparation Date/Time:10/11/24 00:38
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 00:38
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.663 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.26 0.149 0.000350 0.00100
Naphthalene 91-20-3 10.18 0.113 0.00488 0.0125
n-Propylbenzene 103-65-1 7.59 0.129 0.000950 0.00500
Styrene 100-42-5 7.10 0.116 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.68 0.117 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.63 0.121 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.78 0.180 J4 0.000754 0.00250
Tetrachloroethene 127-18-4 5.89 0.110 0.000896 0.00250
Toluene 108-88-3 5.63 0.121 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.34 0.118 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.91 0.118 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.19 0.142 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.99 0.118 0.000597 0.00250
Trichloroethene 79-01-6 4.74 0.130 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.38 0.163 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.75 0.137 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 8.03 0.126 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.38 0.125 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.73 0.130 0.00200 0.00500
Vinyl chloride 75-01-4 1.94 0.139 0.00116 0.00250
Xylenes, Total 1330-20-7 7.06 0.358 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131396-1
Lab Sample ID:R4131396-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1010_31LCSA Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:10/10/24 21:27
Analytical Batch:WG2380092 Analysis Date/Time:10/10/24 21:27
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.15 0.0347 J 0.0113 0.0500
Acrolein 107-02-8 2.98 0.0299 J 0.000 0.0500
Acrylonitrile 107-13-1 3.60 0.0305 0.000671 0.0100
Benzene 71-43-2 4.36 0.00464 0.0000941 0.00100
Bromobenzene 108-86-1 7.44 0.00415 0.000118 0.00100
Bromodichloromethane 75-27-4 5.01 0.00459 0.000136 0.00100
Bromoform 75-25-2 6.99 0.00390 0.000129 0.00100
Bromomethane 74-83-9 2.28 0.00641 0.000605 0.00500
n-Butylbenzene 104-51-8 8.38 0.00459 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.95 0.00450 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.82 0.00410 0.000127 0.00100
Carbon tetrachloride 56-23-5 4.12 0.00513 0.000128 0.00100
Chlorobenzene 108-90-7 6.52 0.00441 0.000116 0.00100
Chlorodibromomethane 124-48-1 6.01 0.00403 0.000140 0.00100
Chloroethane 75-00-3 2.34 0.00658 0.000192 0.00500
Chloroform 67-66-3 4.01 0.00516 0.000111 0.00500
Chloromethane 74-87-3 1.95 0.00515 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.57 0.00456 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.69 0.00413 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.16 0.00509 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.19 0.00436 0.000126 0.00100
Dibromomethane 74-95-3 4.93 0.00549 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.53 0.00476 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.13 0.00451 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.20 0.00458 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.77 0.00509 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.58 0.00540 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.47 0.00511 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.77 0.00537 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.88 0.00534 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.22 0.00535 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.99 0.00444 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.21 0.00512 0.000142 0.00100
1,3-Dichloropropane 142-28-9 6.07 0.00433 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.38 0.00375 J4 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.77 0.00394 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.95 0.0107 J4 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.48 0.00521 0.000105 0.00100
Ethylbenzene 100-41-4 6.52 0.00450 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.67 0.00655 0.000337 0.00100
Isopropylbenzene 98-82-8 7.13 0.00497 0.000105 0.00100
p-Isopropyltoluene 99-87-6 8.05 0.00435 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.18 0.0248 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 464 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131396-1
Lab Sample ID:R4131396-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1010_31LCSA Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:10/10/24 21:27
Analytical Batch:WG2380092 Analysis Date/Time:10/10/24 21:27
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.12 0.00546 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.74 0.0251 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.28 0.00530 0.000101 0.00100
Naphthalene 91-20-3 9.98 0.00558 0.00100 0.00500
n-Propylbenzene 103-65-1 7.43 0.00420 0.0000993 0.00100
Styrene 100-42-5 6.96 0.00443 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.56 0.00497 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.48 0.00436 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.80 0.00496 0.000180 0.00100
Tetrachloroethene 127-18-4 5.79 0.00455 0.000300 0.00100
Toluene 108-88-3 5.54 0.00432 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.13 0.00672 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.71 0.00599 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.15 0.00532 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.88 0.00461 0.000158 0.00100
Trichloroethene 79-01-6 4.68 0.00461 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.42 0.00594 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.59 0.00461 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.87 0.00454 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.20 0.00471 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.57 0.00450 0.000104 0.00100
Vinyl chloride 75-01-4 2.02 0.00593 0.000234 0.00100
Xylenes, Total 1330-20-7 6.92 0.0140 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 465 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-1
Lab Sample ID:R4132125-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1011a_03LCS Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:10/12/24 03:47
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 03:47
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 0.531 0.0365 0.0500
Acrylonitrile 107-13-1 3.65 0.568 0.00361 0.0125
Benzene 71-43-2 4.40 0.105 0.000467 0.00100
Bromobenzene 108-86-1 7.51 0.143 0.000900 0.0125
Bromodichloromethane 75-27-4 5.05 0.109 0.000725 0.00250
Bromoform 75-25-2 7.06 0.125 0.00117 0.0250
Bromomethane 74-83-9 2.37 0.0982 0.00197 0.0125
n-Butylbenzene 104-51-8 8.45 0.143 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.01 0.148 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.88 0.149 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.17 0.109 0.000898 0.00500
Chlorobenzene 108-90-7 6.58 0.124 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.07 0.129 0.000612 0.00250
Chloroethane 75-00-3 2.43 0.0990 0.00170 0.00500
Chloroform 67-66-3 4.07 0.102 0.00103 0.00250
Chloromethane 74-87-3 2.08 0.0934 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.63 0.139 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.75 0.150 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.25 0.130 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.24 0.131 0.000648 0.00250
Dibromomethane 74-95-3 4.98 0.106 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.61 0.132 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.21 0.136 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.28 0.135 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.87 0.107 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.63 0.106 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.52 0.0996 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.84 0.109 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.93 0.108 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.28 0.106 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.03 0.108 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.26 0.104 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.12 0.129 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.43 0.118 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.83 0.135 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.99 0.107 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.52 0.112 0.000410 0.00100
Ethylbenzene 100-41-4 6.57 0.123 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.76 0.134 0.00600 0.0250
Isopropylbenzene 98-82-8 7.19 0.129 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.11 0.131 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.22 0.569 0.0635 0.100
Methylene Chloride 75-09-2 3.18 0.103 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 466 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-1
Lab Sample ID:R4132125-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1011a_03LCS Received Date/Time:_______________
Instrument ID:VOCMS56 Preparation Date/Time:10/12/24 03:47
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 03:47
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 0.693 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.32 0.114 0.000350 0.00100
Naphthalene 91-20-3 10.08 0.116 0.00488 0.0125
n-Propylbenzene 103-65-1 7.50 0.139 0.000950 0.00500
Styrene 100-42-5 7.02 0.127 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.62 0.124 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.54 0.144 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.88 0.102 0.000754 0.00250
Tetrachloroethene 127-18-4 5.83 0.124 0.000896 0.00250
Toluene 108-88-3 5.58 0.131 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.23 0.135 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.80 0.140 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.20 0.114 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.94 0.122 0.000597 0.00250
Trichloroethene 79-01-6 4.72 0.107 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.50 0.110 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.66 0.148 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 7.93 0.151 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.27 0.144 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.63 0.144 0.00200 0.00500
Vinyl chloride 75-01-4 2.14 0.103 0.00116 0.00250
Xylenes, Total 1330-20-7 6.97 0.413 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 467 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132481-1
Lab Sample ID:R4132481-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1010_02LCSA Received Date/Time:_______________
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 03:47
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 03:47
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.05 0.0212 J 0.0113 0.0500
Acrolein 107-02-8 2.89 0.0229 J 0.000 0.0500
Acrylonitrile 107-13-1 3.50 0.0230 0.000671 0.0100
Benzene 71-43-2 4.25 0.00538 0.0000941 0.00100
Bromobenzene 108-86-1 7.35 0.00490 0.000118 0.00100
Bromodichloromethane 75-27-4 4.90 0.00553 0.000136 0.00100
Bromoform 75-25-2 6.89 0.00397 0.000129 0.00100
Bromomethane 74-83-9 2.15 0.00916 J4 0.000605 0.00500
n-Butylbenzene 104-51-8 8.28 0.00441 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.85 0.00508 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.71 0.00472 0.000127 0.00100
Carbon tetrachloride 56-23-5 4 0.00581 0.000128 0.00100
Chlorobenzene 108-90-7 6.42 0.00529 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.90 0.00466 0.000140 0.00100
Chloroethane 75-00-3 2.25 0.00717 0.000192 0.00500
Chloroform 67-66-3 3.91 0.00562 0.000111 0.00500
Chloromethane 74-87-3 1.83 0.00500 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.47 0.00510 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.59 0.00489 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.09 0.00236 J J4 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.08 0.00436 0.000126 0.00100
Dibromomethane 74-95-3 4.83 0.00565 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.44 0.00492 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.05 0.00505 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.11 0.00522 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.67 0.00475 J 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.47 0.00548 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.36 0.00561 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.68 0.00519 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.76 0.00563 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.12 0.00544 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.87 0.00549 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.10 0.00544 0.000142 0.00100
1,3-Dichloropropane 142-28-9 5.97 0.00482 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.27 0.00495 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.67 0.00477 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.83 0.00556 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.36 0.00562 0.000105 0.00100
Ethylbenzene 100-41-4 6.42 0.00491 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.58 0.00479 0.000337 0.00100
Isopropylbenzene 98-82-8 7.03 0.00454 0.000105 0.00100
p-Isopropyltoluene 99-87-6 7.95 0.00473 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.07 0.0189 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 468 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132481-1
Lab Sample ID:R4132481-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1010_02LCSA Received Date/Time:_______________
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 03:47
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 03:47
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.02 0.00595 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.63 0.0205 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.16 0.00480 0.000101 0.00100
n-Propylbenzene 103-65-1 7.33 0.00483 0.0000993 0.00100
Styrene 100-42-5 6.86 0.00417 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.45 0.00494 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.38 0.00444 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.69 0.00534 0.000180 0.00100
Tetrachloroethene 127-18-4 5.67 0.00542 0.000300 0.00100
Toluene 108-88-3 5.42 0.00521 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.06 0.00288 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.63 0.00342 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.04 0.00532 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.78 0.00490 0.000158 0.00100
Trichloroethene 79-01-6 4.57 0.00548 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.34 0.00550 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.50 0.00486 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.76 0.00460 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.10 0.00491 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.46 0.00493 0.000104 0.00100
Vinyl chloride 75-01-4 1.90 0.00550 0.000234 0.00100
Xylenes, Total 1330-20-7 6.82 0.0142 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 469 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133124-1
Lab Sample ID:R4133124-1 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1015_02LCSA Received Date/Time:_______________
Instrument ID:VOCMS42 Preparation Date/Time:10/15/24 08:43
Analytical Batch:WG2381936 Analysis Date/Time:10/15/24 08:43
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Naphthalene 91-20-3 10.60 0.00386 J 0.00100 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 470 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-2
Lab Sample ID:R4131341-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1011_03 Received Date/Time:_______________
Instrument ID:VOCMS59 Preparation Date/Time:10/11/24 00:57
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 00:57
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.12 0.634 0.0365 0.0500
Acrylonitrile 107-13-1 3.59 0.665 0.00361 0.0125
Benzene 71-43-2 4.40 0.131 0.000467 0.00100
Bromobenzene 108-86-1 7.60 0.117 0.000900 0.0125
Bromodichloromethane 75-27-4 5.08 0.127 0.000725 0.00250
Bromoform 75-25-2 7.13 0.127 0.00117 0.0250
Bromomethane 74-83-9 2.20 0.160 0.00197 0.0125
n-Butylbenzene 104-51-8 8.56 0.128 0.00525 0.0125
sec-Butylbenzene 135-98-8 8.12 0.128 0.00288 0.0125
tert-Butylbenzene 98-06-6 7.98 0.119 0.00195 0.00500
Carbon tetrachloride 56-23-5 4.15 0.147 0.000898 0.00500
Chlorobenzene 108-90-7 6.65 0.118 0.000210 0.00250
Chlorodibromomethane 124-48-1 6.12 0.118 0.000612 0.00250
Chloroethane 75-00-3 2.28 0.171 J4 0.00170 0.00500
Chloroform 67-66-3 4.04 0.142 0.00103 0.00250
Chloromethane 74-87-3 1.87 0.143 0.00435 0.0125
2-Chlorotoluene 95-49-8 7.73 0.121 0.000865 0.00250
4-Chlorotoluene 106-43-4 7.85 0.121 0.000450 0.00500
1,2-Dibromo-3-Chloropropane 96-12-8 9.35 0.119 0.00390 0.0250
1,2-Dibromoethane 106-93-4 6.29 0.116 0.000648 0.00250
Dibromomethane 74-95-3 5 0.131 0.000750 0.00500
1,2-Dichlorobenzene 95-50-1 8.71 0.121 0.000425 0.00500
1,3-Dichlorobenzene 541-73-1 8.31 0.124 0.000600 0.00500
1,4-Dichlorobenzene 106-46-7 8.37 0.119 0.000700 0.00500
Dichlorodifluoromethane 75-71-8 1.68 0.141 0.00161 0.00500
1,1-Dichloroethane 75-34-3 3.58 0.138 0.000491 0.00250
1,2-Dichloroethane 107-06-2 4.51 0.137 0.000649 0.00250
1,1-Dichloroethene 75-35-4 2.74 0.162 0.000606 0.00250
cis-1,2-Dichloroethene 156-59-2 3.89 0.139 0.000734 0.00250
trans-1,2-Dichloroethene 156-60-5 3.21 0.136 0.00104 0.00500
1,2-Dichloropropane 78-87-5 5.05 0.128 0.00142 0.00500
1,1-Dichloropropene 563-58-6 4.25 0.140 0.000809 0.00250
1,3-Dichloropropane 142-28-9 6.18 0.119 0.000501 0.00500
cis-1,3-Dichloropropene 10061-01-5 5.46 0.125 0.000757 0.00250
trans-1,3-Dichloropropene 10061-02-6 5.87 0.121 0.00114 0.00500
2,2-Dichloropropane 594-20-7 3.97 0.166 0.00138 0.00250
Di-isopropyl ether 108-20-3 3.48 0.135 0.000410 0.00100
Ethylbenzene 100-41-4 6.65 0.122 0.000737 0.00250
Hexachloro-1,3-butadiene 87-68-3 9.88 0.119 0.00600 0.0250
Isopropylbenzene 98-82-8 7.28 0.122 0.000425 0.00250
p-Isopropyltoluene 99-87-6 8.22 0.123 0.00255 0.00500
2-Butanone (MEK)78-93-3 4.20 0.772 0.0635 0.100
Methylene Chloride 75-09-2 3.11 0.143 0.00664 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 471 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-2
Lab Sample ID:R4131341-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1011_03 Received Date/Time:_______________
Instrument ID:VOCMS59 Preparation Date/Time:10/11/24 00:57
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 00:57
Dilution Factor:1 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:5 g
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.655 0.00228 0.0250
Methyl tert-butyl ether 1634-04-4 3.26 0.141 0.000350 0.00100
Naphthalene 91-20-3 10.18 0.111 0.00488 0.0125
n-Propylbenzene 103-65-1 7.59 0.124 0.000950 0.00500
Styrene 100-42-5 7.10 0.115 0.000229 0.0125
1,1,1,2-Tetrachloroethane 630-20-6 6.68 0.115 0.000948 0.00250
1,1,2,2-Tetrachloroethane 79-34-5 7.63 0.114 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane 76-13-1 2.78 0.172 0.000754 0.00250
Tetrachloroethene 127-18-4 5.89 0.113 0.000896 0.00250
Toluene 108-88-3 5.63 0.124 0.00130 0.00500
1,2,3-Trichlorobenzene 87-61-6 10.34 0.111 0.00733 0.0125
1,2,4-Trichlorobenzene 120-82-1 9.91 0.113 0.00440 0.0125
1,1,1-Trichloroethane 71-55-6 4.19 0.139 0.000923 0.00250
1,1,2-Trichloroethane 79-00-5 5.99 0.116 0.000597 0.00250
Trichloroethene 79-01-6 4.74 0.125 0.000584 0.00100
Trichlorofluoromethane 75-69-4 2.38 0.165 0.000827 0.00250
1,2,3-Trichloropropane 96-18-4 7.75 0.131 0.00162 0.0125
1,2,4-Trimethylbenzene 95-63-6 8.03 0.120 0.00158 0.00500
1,2,3-Trimethylbenzene 526-73-8 8.38 0.119 0.00158 0.00500
1,3,5-Trimethylbenzene 108-67-8 7.73 0.124 0.00200 0.00500
Vinyl chloride 75-01-4 1.94 0.139 0.00116 0.00250
Xylenes, Total 1330-20-7 7.06 0.357 0.000880 0.00650
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132481-2
Lab Sample ID:R4132481-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1010_03A Received Date/Time:_______________
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 04:07
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 04:07
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.05 0.0195 J 0.0113 0.0500
Acrolein 107-02-8 2.89 0.0215 J 0.000 0.0500
Acrylonitrile 107-13-1 3.50 0.0225 0.000671 0.0100
Benzene 71-43-2 4.25 0.00513 0.0000941 0.00100
Bromobenzene 108-86-1 7.35 0.00464 0.000118 0.00100
Bromodichloromethane 75-27-4 4.90 0.00534 0.000136 0.00100
Bromoform 75-25-2 6.89 0.00420 0.000129 0.00100
Bromomethane 74-83-9 2.16 0.00926 J4 0.000605 0.00500
n-Butylbenzene 104-51-8 8.28 0.00431 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.85 0.00465 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.71 0.00449 0.000127 0.00100
Carbon tetrachloride 56-23-5 4 0.00550 0.000128 0.00100
Chlorobenzene 108-90-7 6.42 0.00512 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.91 0.00462 0.000140 0.00100
Chloroethane 75-00-3 2.25 0.00658 0.000192 0.00500
Chloroform 67-66-3 3.91 0.00548 0.000111 0.00500
Chloromethane 74-87-3 1.84 0.00515 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.47 0.00483 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.59 0.00465 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.07 0.00251 J J4 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.09 0.00431 0.000126 0.00100
Dibromomethane 74-95-3 4.83 0.00521 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.44 0.00465 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.05 0.00486 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.11 0.00502 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.68 0.00473 J 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.47 0.00539 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.36 0.00560 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.68 0.00486 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.77 0.00540 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.13 0.00499 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.87 0.00523 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.10 0.00498 0.000142 0.00100
1,3-Dichloropropane 142-28-9 5.97 0.00481 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.27 0.00472 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.67 0.00441 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.83 0.00518 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.36 0.00525 0.000105 0.00100
Ethylbenzene 100-41-4 6.42 0.00456 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.58 0.00463 0.000337 0.00100
Isopropylbenzene 98-82-8 7.03 0.00453 0.000105 0.00100
p-Isopropyltoluene 99-87-6 7.95 0.00459 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.07 0.0182 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132481-2
Lab Sample ID:R4132481-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1010_03A Received Date/Time:_______________
Instrument ID:VOCMS36 Preparation Date/Time:10/10/24 04:07
Analytical Batch:WG2379334 Analysis Date/Time:10/10/24 04:07
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.03 0.00544 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.63 0.0200 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.16 0.00446 0.000101 0.00100
n-Propylbenzene 103-65-1 7.33 0.00473 0.0000993 0.00100
Styrene 100-42-5 6.85 0.00404 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.45 0.00511 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.38 0.00434 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.70 0.00508 0.000180 0.00100
Tetrachloroethene 127-18-4 5.68 0.00502 0.000300 0.00100
Toluene 108-88-3 5.42 0.00511 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.05 0.00325 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.63 0.00362 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.04 0.00528 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.78 0.00458 0.000158 0.00100
Trichloroethene 79-01-6 4.57 0.00537 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.35 0.00539 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.50 0.00416 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.76 0.00441 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.10 0.00465 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.46 0.00462 0.000104 0.00100
Vinyl chloride 75-01-4 1.91 0.00515 0.000234 0.00100
Xylenes, Total 1330-20-7 6.82 0.0140 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4133124-2
Lab Sample ID:R4133124-2 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1015_03A Received Date/Time:_______________
Instrument ID:VOCMS42 Preparation Date/Time:10/15/24 09:03
Analytical Batch:WG2381936 Analysis Date/Time:10/15/24 09:03
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Naphthalene 91-20-3 10.60 0.00428 J 0.00100 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-4
Lab Sample ID:R4131341-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:1011_28 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 09:04
Dilution Factor:1.13 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.85 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 0.391 0.0465 0.0637
Acrylonitrile 107-13-1 3.59 0.615 0.00460 0.0159
Benzene 71-43-2 4.40 0.144 0.000595 0.00127
Bromobenzene 108-86-1 7.59 0.145 0.00115 0.0159
Bromodichloromethane 75-27-4 5.08 0.141 0.000924 0.00319
Bromoform 75-25-2 7.13 0.139 0.00149 0.0319
Bromomethane 74-83-9 2.19 0.0747 0.00251 0.0159
n-Butylbenzene 104-51-8 8.56 0.147 0.00669 0.0159
sec-Butylbenzene 135-98-8 8.12 0.157 0.00367 0.0159
tert-Butylbenzene 98-06-6 7.98 0.149 0.00248 0.00637
Carbon tetrachloride 56-23-5 4.15 0.143 0.00114 0.00637
Chlorobenzene 108-90-7 6.65 0.135 0.000267 0.00319
Chlorodibromomethane 124-48-1 6.11 0.139 0.000780 0.00319
Chloroethane 75-00-3 2.26 0.0394 0.00217 0.00637
Chloroform 67-66-3 4.04 0.136 0.00131 0.00319
Chloromethane 74-87-3 1.87 0.110 0.00555 0.0159
2-Chlorotoluene 95-49-8 7.72 0.147 0.00110 0.00319
4-Chlorotoluene 106-43-4 7.84 0.151 0.000574 0.00637
1,2-Dibromo-3-Chloropropane 96-12-8 9.35 0.121 0.00497 0.0319
1,2-Dibromoethane 106-93-4 6.29 0.144 0.000825 0.00319
Dibromomethane 74-95-3 4.99 0.144 0.000956 0.00637
1,2-Dichlorobenzene 95-50-1 8.71 0.140 0.000541 0.00637
1,3-Dichlorobenzene 541-73-1 8.31 0.145 0.000765 0.00637
1,4-Dichlorobenzene 106-46-7 8.37 0.144 0.000892 0.00637
Dichlorodifluoromethane 75-71-8 1.68 0.114 0.00205 0.00637
1,1-Dichloroethane 75-34-3 3.57 0.147 0.000626 0.00319
1,2-Dichloroethane 107-06-2 4.50 0.147 0.000827 0.00319
1,1-Dichloroethene 75-35-4 2.73 0.143 0.000772 0.00319
cis-1,2-Dichloroethene 156-59-2 3.89 0.307 0.000935 0.00319
trans-1,2-Dichloroethene 156-60-5 3.20 0.126 0.00133 0.00637
1,2-Dichloropropane 78-87-5 5.05 0.144 0.00180 0.00637
1,1-Dichloropropene 563-58-6 4.25 0.141 0.00103 0.00319
1,3-Dichloropropane 142-28-9 6.17 0.157 0.000638 0.00637
cis-1,3-Dichloropropene 10061-01-5 5.46 0.142 0.000964 0.00319
trans-1,3-Dichloropropene 10061-02-6 5.87 0.149 0.00145 0.00637
2,2-Dichloropropane 594-20-7 3.96 0.107 0.00176 0.00319
Di-isopropyl ether 108-20-3 3.49 0.142 0.000522 0.00127
Ethylbenzene 100-41-4 6.65 0.135 0.000939 0.00319
Hexachloro-1,3-butadiene 87-68-3 9.88 0.156 0.00765 0.0319
Isopropylbenzene 98-82-8 7.28 0.132 0.000541 0.00319
p-Isopropyltoluene 99-87-6 8.22 0.157 0.00325 0.00637
2-Butanone (MEK)78-93-3 4.21 0.710 0.0810 0.127
Methylene Chloride 75-09-2 3.12 0.135 0.00846 0.0319
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-4
Lab Sample ID:R4131341-4 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:1011_28 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 09:04
Dilution Factor:1.13 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.85 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.743 0.00291 0.0319
Methyl tert-butyl ether 1634-04-4 3.27 0.142 0.000447 0.00127
Naphthalene 91-20-3 10.18 0.156 0.00621 0.0159
n-Propylbenzene 103-65-1 7.59 0.149 0.00121 0.00637
Styrene 100-42-5 7.09 0.127 0.000292 0.0159
1,1,1,2-Tetrachloroethane 630-20-6 6.68 0.126 0.00121 0.00319
1,1,2,2-Tetrachloroethane 79-34-5 7.63 0.0704 0.000885 0.00319
1,1,2-Trichlorotrifluoroethane 76-13-1 2.76 0.160 0.000961 0.00319
Tetrachloroethene 127-18-4 5.89 0.192 0.00114 0.00319
Toluene 108-88-3 5.62 0.171 J6 0.00166 0.00637
1,2,3-Trichlorobenzene 87-61-6 10.34 0.131 0.00934 0.0159
1,2,4-Trichlorobenzene 120-82-1 9.91 0.131 0.00560 0.0159
1,1,1-Trichloroethane 71-55-6 4.18 0.135 0.00117 0.00319
1,1,2-Trichloroethane 79-00-5 5.99 0.150 0.000761 0.00319
Trichloroethene 79-01-6 4.73 0.267 0.000744 0.00127
Trichlorofluoromethane 75-69-4 2.38 0.0559 0.00105 0.00319
1,2,3-Trichloropropane 96-18-4 7.75 0.154 0.00206 0.0159
1,2,4-Trimethylbenzene 95-63-6 8.03 0.175 0.00202 0.00637
1,2,3-Trimethylbenzene 526-73-8 8.38 0.166 0.00202 0.00637
1,3,5-Trimethylbenzene 108-67-8 7.73 0.161 0.00255 0.00637
Vinyl chloride 75-01-4 1.94 0.108 0.00148 0.00319
Xylenes, Total 1330-20-7 7.06 0.445 0.00112 0.00829
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 477 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-3
Lab Sample ID:R4132125-3 SDG:L1784578
Client Sample ID:MS Collected Date/Time:10/01/24 08:21
Lab File ID:1011a_31 Received Date/Time:10/03/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:10/01/24 08:21
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 12:38
Dilution Factor:20 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.28 g
Total Solids (%):90.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.21 13.9 0.891 1.22
Acrylonitrile 107-13-1 3.65 13.7 0.0881 0.305
Benzene 71-43-2 4.40 2.78 0.0114 0.0244
Bromobenzene 108-86-1 7.50 3.86 0.0220 0.305
Bromodichloromethane 75-27-4 5.05 2.84 0.0177 0.0610
Bromoform 75-25-2 7.05 3.54 0.0286 0.610
Bromomethane 74-83-9 2.38 2.20 0.0481 0.305
n-Butylbenzene 104-51-8 8.44 6.66 J5 0.128 0.305
sec-Butylbenzene 135-98-8 8.01 5.05 0.0703 0.305
tert-Butylbenzene 98-06-6 7.88 4.16 0.0476 0.122
Carbon tetrachloride 56-23-5 4.16 2.84 0.0220 0.122
Chlorobenzene 108-90-7 6.58 3.47 0.00513 0.0610
Chlorodibromomethane 124-48-1 6.06 3.65 0.0149 0.0610
Chloroethane 75-00-3 2.43 2.50 0.0415 0.122
Chloroform 67-66-3 4.07 2.71 0.0251 0.0610
Chloromethane 74-87-3 2.09 2.27 0.106 0.305
2-Chlorotoluene 95-49-8 7.63 3.91 0.0211 0.0610
4-Chlorotoluene 106-43-4 0 U J6 0.0110 0.122
1,2-Dibromo-3-Chloropropane 96-12-8 9.24 3.95 0.0952 0.610
1,2-Dibromoethane 106-93-4 6.24 3.64 0.0159 0.0610
Dibromomethane 74-95-3 4.98 2.84 0.0183 0.122
1,2-Dichlorobenzene 95-50-1 8.61 3.95 0.0104 0.122
1,3-Dichlorobenzene 541-73-1 8.21 3.92 0.0146 0.122
1,4-Dichlorobenzene 106-46-7 8.27 3.83 0.0171 0.122
Dichlorodifluoromethane 75-71-8 1.87 3.04 0.0393 0.122
1,1-Dichloroethane 75-34-3 3.63 2.87 0.0120 0.0610
1,2-Dichloroethane 107-06-2 4.52 2.72 0.0159 0.0610
1,1-Dichloroethene 75-35-4 2.83 2.82 0.0148 0.0610
cis-1,2-Dichloroethene 156-59-2 3.93 2.83 0.0179 0.0610
trans-1,2-Dichloroethene 156-60-5 3.28 2.75 0.0254 0.122
1,2-Dichloropropane 78-87-5 5.03 2.86 0.0347 0.122
1,1-Dichloropropene 563-58-6 4.26 2.65 0.0198 0.0610
1,3-Dichloropropane 142-28-9 6.12 3.52 0.0122 0.122
cis-1,3-Dichloropropene 10061-01-5 5.43 3.20 0.0184 0.0610
trans-1,3-Dichloropropene 10061-02-6 5.83 3.73 0.0278 0.122
2,2-Dichloropropane 594-20-7 3.99 2.80 0.0337 0.0610
Di-isopropyl ether 108-20-3 3.51 2.95 0.0100 0.0244
Ethylbenzene 100-41-4 6.57 6.22 0.0179 0.0610
Hexachloro-1,3-butadiene 87-68-3 9.76 4.60 0.146 0.610
Isopropylbenzene 98-82-8 7.19 4.37 0.0104 0.0610
p-Isopropyltoluene 99-87-6 8.11 5.74 0.0622 0.122
2-Butanone (MEK)78-93-3 4.22 13.1 1.55 2.44
Methylene Chloride 75-09-2 3.18 2.80 0.162 0.610
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 478 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-3
Lab Sample ID:R4132125-3 SDG:L1784578
Client Sample ID:MS Collected Date/Time:10/01/24 08:21
Lab File ID:1011a_31 Received Date/Time:10/03/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:10/01/24 08:21
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 12:38
Dilution Factor:20 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.28 g
Total Solids (%):90.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 20.1 0.0557 0.610
Methyl tert-butyl ether 1634-04-4 3.32 3.03 0.00854 0.0244
Naphthalene 91-20-3 10.08 17.9 V 0.119 0.305
n-Propylbenzene 103-65-1 7.49 6.38 0.0232 0.122
Styrene 100-42-5 7.01 3.65 0.00559 0.305
1,1,1,2-Tetrachloroethane 630-20-6 6.61 3.42 0.0232 0.0610
1,1,2,2-Tetrachloroethane 79-34-5 7.54 3.86 0.0170 0.0610
1,1,2-Trichlorotrifluoroethane 76-13-1 2.88 2.86 0.0184 0.0610
Tetrachloroethene 127-18-4 5.83 3.41 0.0218 0.0610
Toluene 108-88-3 5.58 3.43 0.0317 0.122
1,2,3-Trichlorobenzene 87-61-6 10.23 5.04 J5 0.179 0.305
1,2,4-Trichlorobenzene 120-82-1 9.80 4.94 J5 0.107 0.305
1,1,1-Trichloroethane 71-55-6 4.19 2.76 0.0226 0.0610
1,1,2-Trichloroethane 79-00-5 5.94 3.88 0.0145 0.0610
Trichloroethene 79-01-6 4.72 2.95 0.0143 0.0244
Trichlorofluoromethane 75-69-4 2.49 0.965 0.0201 0.0610
1,2,3-Trichloropropane 96-18-4 7.66 3.59 0.0395 0.305
1,2,4-Trimethylbenzene 95-63-6 7.93 58.3 V 0.0386 0.122
1,2,3-Trimethylbenzene 526-73-8 8.27 17.7 0.0386 0.122
1,3,5-Trimethylbenzene 108-67-8 7.63 5.47 0.0488 0.122
Vinyl chloride 75-01-4 2.14 2.53 0.0283 0.0610
Xylenes, Total 1330-20-7 6.97 20.6 0.0215 0.159
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784578 10/18/24 11:02 479 of 526
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-5
Lab Sample ID:R4131341-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:1011_29 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 09:24
Dilution Factor:1.13 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.85 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.13 0.373 0.0465 0.0637
Acrylonitrile 107-13-1 3.59 0.607 0.00460 0.0159
Benzene 71-43-2 4.40 0.176 0.000595 0.00127
Bromobenzene 108-86-1 7.59 0.170 0.00115 0.0159
Bromodichloromethane 75-27-4 5.08 0.160 0.000924 0.00319
Bromoform 75-25-2 7.13 0.144 0.00149 0.0319
Bromomethane 74-83-9 2.19 0.0832 0.00251 0.0159
n-Butylbenzene 104-51-8 8.56 0.183 0.00669 0.0159
sec-Butylbenzene 135-98-8 8.12 0.196 0.00367 0.0159
tert-Butylbenzene 98-06-6 7.98 0.214 0.00248 0.00637
Carbon tetrachloride 56-23-5 4.14 0.184 0.00114 0.00637
Chlorobenzene 108-90-7 6.64 0.167 0.000267 0.00319
Chlorodibromomethane 124-48-1 6.11 0.156 0.000780 0.00319
Chloroethane 75-00-3 2.26 0.0449 0.00217 0.00637
Chloroform 67-66-3 4.04 0.167 0.00131 0.00319
Chloromethane 74-87-3 1.87 0.143 0.00555 0.0159
2-Chlorotoluene 95-49-8 7.72 0.176 0.00110 0.00319
4-Chlorotoluene 106-43-4 7.85 0.178 0.000574 0.00637
1,2-Dibromo-3-Chloropropane 96-12-8 9.35 0.125 0.00497 0.0319
1,2-Dibromoethane 106-93-4 6.29 0.151 0.000825 0.00319
Dibromomethane 74-95-3 4.99 0.160 0.000956 0.00637
1,2-Dichlorobenzene 95-50-1 8.71 0.161 0.000541 0.00637
1,3-Dichlorobenzene 541-73-1 8.31 0.166 0.000765 0.00637
1,4-Dichlorobenzene 106-46-7 8.37 0.164 0.000892 0.00637
Dichlorodifluoromethane 75-71-8 1.68 0.156 0.00205 0.00637
1,1-Dichloroethane 75-34-3 3.57 0.171 0.000626 0.00319
1,2-Dichloroethane 107-06-2 4.51 0.160 0.000827 0.00319
1,1-Dichloroethene 75-35-4 2.73 0.192 0.000772 0.00319
cis-1,2-Dichloroethene 156-59-2 3.89 0.324 0.000935 0.00319
trans-1,2-Dichloroethene 156-60-5 3.21 0.162 0.00133 0.00637
1,2-Dichloropropane 78-87-5 5.05 0.165 0.00180 0.00637
1,1-Dichloropropene 563-58-6 4.25 0.184 0.00103 0.00319
1,3-Dichloropropane 142-28-9 6.17 0.171 0.000638 0.00637
cis-1,3-Dichloropropene 10061-01-5 5.46 0.165 0.000964 0.00319
trans-1,3-Dichloropropene 10061-02-6 5.87 0.170 0.00145 0.00637
2,2-Dichloropropane 594-20-7 3.96 0.142 0.00176 0.00319
Di-isopropyl ether 108-20-3 3.49 0.160 0.000522 0.00127
Ethylbenzene 100-41-4 6.65 0.169 0.000939 0.00319
Hexachloro-1,3-butadiene 87-68-3 9.88 0.188 0.00765 0.0319
Isopropylbenzene 98-82-8 7.28 0.170 0.000541 0.00319
p-Isopropyltoluene 99-87-6 8.22 0.192 0.00325 0.00637
2-Butanone (MEK)78-93-3 4.20 0.697 0.0810 0.127
Methylene Chloride 75-09-2 3.12 0.159 0.00846 0.0319
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4131341-5
Lab Sample ID:R4131341-5 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:1011_29 Received Date/Time:10/02/24 09:00
Instrument ID:VOCMS59 Preparation Date/Time:09/27/24 12:00
Analytical Batch:WG2379147 Analysis Date/Time:10/11/24 09:24
Dilution Factor:1.13 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:8.85 g
Total Solids (%):93.7 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.84 0.744 0.00291 0.0319
Methyl tert-butyl ether 1634-04-4 3.27 0.147 0.000447 0.00127
Naphthalene 91-20-3 10.18 0.167 0.00621 0.0159
n-Propylbenzene 103-65-1 7.59 0.188 0.00121 0.00637
Styrene 100-42-5 7.10 0.157 0.000292 0.0159
1,1,1,2-Tetrachloroethane 630-20-6 6.68 0.148 0.00121 0.00319
1,1,2,2-Tetrachloroethane 79-34-5 7.63 0.0743 0.000885 0.00319
1,1,2-Trichlorotrifluoroethane 76-13-1 2.76 0.224 0.000961 0.00319
Tetrachloroethene 127-18-4 5.89 0.231 0.00114 0.00319
Toluene 108-88-3 5.62 0.209 0.00166 0.00637
1,2,3-Trichlorobenzene 87-61-6 10.34 0.151 0.00934 0.0159
1,2,4-Trichlorobenzene 120-82-1 9.91 0.151 0.00560 0.0159
1,1,1-Trichloroethane 71-55-6 4.18 0.177 0.00117 0.00319
1,1,2-Trichloroethane 79-00-5 5.99 0.158 0.000761 0.00319
Trichloroethene 79-01-6 4.73 0.309 0.000744 0.00127
Trichlorofluoromethane 75-69-4 2.38 0.0803 0.00105 0.00319
1,2,3-Trichloropropane 96-18-4 7.75 0.157 0.00206 0.0159
1,2,4-Trimethylbenzene 95-63-6 8.03 0.202 0.00202 0.00637
1,2,3-Trimethylbenzene 526-73-8 8.38 0.189 0.00202 0.00637
1,3,5-Trimethylbenzene 108-67-8 7.73 0.195 0.00255 0.00637
Vinyl chloride 75-01-4 1.94 0.145 0.00148 0.00319
Xylenes, Total 1330-20-7 7.06 0.547 0.00112 0.00829
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-4
Lab Sample ID:R4132125-4 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:10/01/24 08:21
Lab File ID:1011a_32 Received Date/Time:10/03/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:10/01/24 08:21
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 12:57
Dilution Factor:20 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.28 g
Total Solids (%):90.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Acetone 67-64-1 3.20 11.5 0.891 1.22
Acrylonitrile 107-13-1 3.65 13.5 0.0881 0.305
Benzene 71-43-2 4.40 1.49 J3 0.0114 0.0244
Bromobenzene 108-86-1 7.50 2.45 J3 0.0220 0.305
Bromodichloromethane 75-27-4 5.05 1.87 J3 0.0177 0.0610
Bromoform 75-25-2 7.05 3.12 0.0286 0.610
Bromomethane 74-83-9 2.38 1.16 J3 0.0481 0.305
n-Butylbenzene 104-51-8 8.44 2.72 J3 0.128 0.305
sec-Butylbenzene 135-98-8 8.01 3.12 J3 0.0703 0.305
tert-Butylbenzene 98-06-6 7.93 7.95 J3 J5 0.0476 0.122
Carbon tetrachloride 56-23-5 4.16 1.27 J3 0.0220 0.122
Chlorobenzene 108-90-7 6.57 2.10 J3 0.00513 0.0610
Chlorodibromomethane 124-48-1 6.06 2.64 0.0149 0.0610
Chloroethane 75-00-3 2.41 1.21 J3 0.0415 0.122
Chloroform 67-66-3 4.06 1.55 J3 0.0251 0.0610
Chloromethane 74-87-3 2.08 1.05 J3 0.106 0.305
2-Chlorotoluene 95-49-8 7.63 1.70 J3 0.0211 0.0610
4-Chlorotoluene 106-43-4 7.75 2.27 J3 0.0110 0.122
1,2-Dibromo-3-Chloropropane 96-12-8 9.24 4.06 0.0952 0.610
1,2-Dibromoethane 106-93-4 6.24 3.08 0.0159 0.0610
Dibromomethane 74-95-3 4.98 2.28 0.0183 0.122
1,2-Dichlorobenzene 95-50-1 8.61 2.69 J3 0.0104 0.122
1,3-Dichlorobenzene 541-73-1 8.21 2.45 J3 0.0146 0.122
1,4-Dichlorobenzene 106-46-7 8.27 2.42 J3 0.0171 0.122
Dichlorodifluoromethane 75-71-8 1.86 1.28 J3 0.0393 0.122
1,1-Dichloroethane 75-34-3 3.62 1.50 J3 0.0120 0.0610
1,2-Dichloroethane 107-06-2 4.51 1.94 0.0159 0.0610
1,1-Dichloroethene 75-35-4 2.83 1.21 J3 0.0148 0.0610
cis-1,2-Dichloroethene 156-59-2 3.92 1.64 J3 0.0179 0.0610
trans-1,2-Dichloroethene 156-60-5 3.27 1.34 J3 0.0254 0.122
1,2-Dichloropropane 78-87-5 5.03 1.71 J3 0.0347 0.122
1,1-Dichloropropene 563-58-6 4.26 1.21 J3 0.0198 0.0610
1,3-Dichloropropane 142-28-9 6.12 2.82 0.0122 0.122
cis-1,3-Dichloropropene 10061-01-5 5.43 2.16 J3 0.0184 0.0610
trans-1,3-Dichloropropene 10061-02-6 5.83 2.86 0.0278 0.122
2,2-Dichloropropane 594-20-7 3.99 1.39 J3 0.0337 0.0610
Di-isopropyl ether 108-20-3 3.51 2.00 J3 0.0100 0.0244
Ethylbenzene 100-41-4 6.57 4.69 0.0179 0.0610
Hexachloro-1,3-butadiene 87-68-3 9.76 2.90 J3 0.146 0.610
Isopropylbenzene 98-82-8 7.19 2.53 J3 0.0104 0.0610
p-Isopropyltoluene 99-87-6 8.11 3.86 0.0622 0.122
2-Butanone (MEK)78-93-3 4.22 11.1 1.55 2.44
Methylene Chloride 75-09-2 3.18 1.84 J3 0.162 0.610
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4132125-4
Lab Sample ID:R4132125-4 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:10/01/24 08:21
Lab File ID:1011a_32 Received Date/Time:10/03/24 09:00
Instrument ID:VOCMS56 Preparation Date/Time:10/01/24 08:21
Analytical Batch:WG2380545 Analysis Date/Time:10/12/24 12:57
Dilution Factor:20 Prep Method:5035A
Analytical Method:8260B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.28 g
Total Solids (%):90.2 Final Wt/Vol:10 mL
Analyte CAS RT Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)108-10-1 5.78 20.1 0.0557 0.610
Methyl tert-butyl ether 1634-04-4 3.32 2.43 0.00854 0.0244
Naphthalene 91-20-3 10.08 17.7 0.119 0.305
n-Propylbenzene 103-65-1 7.49 4.09 J3 0.0232 0.122
Styrene 100-42-5 7.01 2.33 J3 0.00559 0.305
1,1,1,2-Tetrachloroethane 630-20-6 6.61 2.22 J3 0.0232 0.0610
1,1,2,2-Tetrachloroethane 79-34-5 7.54 3.43 0.0170 0.0610
1,1,2-Trichlorotrifluoroethane 76-13-1 2.88 1.12 J3 0.0184 0.0610
Tetrachloroethene 127-18-4 5.83 1.65 J3 0.0218 0.0610
Toluene 108-88-3 5.58 1.84 J3 0.0317 0.122
1,2,3-Trichlorobenzene 87-61-6 10.23 3.86 0.179 0.305
1,2,4-Trichlorobenzene 120-82-1 9.80 3.82 0.107 0.305
1,1,1-Trichloroethane 71-55-6 4.19 1.31 J3 0.0226 0.0610
1,1,2-Trichloroethane 79-00-5 5.94 3.23 0.0145 0.0610
Trichloroethene 79-01-6 4.72 1.40 J3 0.0143 0.0244
Trichlorofluoromethane 75-69-4 2.55 0.701 0.0201 0.0610
1,2,3-Trichloropropane 96-18-4 7.66 3.21 0.0395 0.305
1,2,4-Trimethylbenzene 95-63-6 7.93 53.9 0.0386 0.122
1,2,3-Trimethylbenzene 526-73-8 8.27 10.8 J3 V 0.0386 0.122
1,3,5-Trimethylbenzene 108-67-8 7.63 3.78 0.0488 0.122
Vinyl chloride 75-01-4 2.13 1.16 J3 0.0283 0.0610
Xylenes, Total 1330-20-7 6.97 15.3 0.0215 0.159
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9071B Wet Chemistry
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-13 (0-6)
Lab Sample ID:L1784578-01 SDG:L1784578
Client Sample ID:S-13 (0-6)Collected Date/Time:09/30/24 10:00
Lab File ID:24 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:16
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.29 g
Total Solids (%):83.9 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)116 J 39.3 119
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-15 (0-6)
Lab Sample ID:L1784578-02 SDG:L1784578
Client Sample ID:S-15 (0-6)Collected Date/Time:09/27/24 14:25
Lab File ID:25 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:16
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):87.1 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)184 37.9 115
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-32 (0-6)
Lab Sample ID:L1784578-03 SDG:L1784578
Client Sample ID:S-32 (0-6)Collected Date/Time:09/30/24 10:10
Lab File ID:26 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:16
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.02 g
Total Solids (%):83.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)120 J J6 P1 39.8 121
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (6-12)
Lab Sample ID:L1784578-04 SDG:L1784578
Client Sample ID:S-12 (6-12)Collected Date/Time:09/27/24 16:05
Lab File ID:09 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.15 g
Total Solids (%):85.5 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)979 38.6 117
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-12 (0-6)
Lab Sample ID:L1784578-05 SDG:L1784578
Client Sample ID:S-12 (0-6)Collected Date/Time:09/27/24 15:50
Lab File ID:10 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.41 g
Total Solids (%):90.4 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)1250 36.5 111
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (0-6)
Lab Sample ID:L1784578-06 SDG:L1784578
Client Sample ID:S-10 (0-6)Collected Date/Time:09/27/24 12:00
Lab File ID:11 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.2 g
Total Solids (%):93.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)785 J3 35.2 107
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-4 (12-18)
Lab Sample ID:L1784578-07 SDG:L1784578
Client Sample ID:S-4 (12-18)Collected Date/Time:09/27/24 15:05
Lab File ID:12 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.49 g
Total Solids (%):91.1 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)345 36.2 110
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (12-18)
Lab Sample ID:L1784578-08 SDG:L1784578
Client Sample ID:S-6 (12-18)Collected Date/Time:09/27/24 15:20
Lab File ID:13 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.25 g
Total Solids (%):90.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)495 36.4 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-10 (6-12)
Lab Sample ID:L1784578-11 SDG:L1784578
Client Sample ID:S-10 (6-12)Collected Date/Time:09/27/24 12:30
Lab File ID:14 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.84 g
Total Solids (%):95.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)646 34.5 104
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (0-6)
Lab Sample ID:L1784578-12 SDG:L1784578
Client Sample ID:S-14 (0-6)Collected Date/Time:09/30/24 09:10
Lab File ID:15 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.16 g
Total Solids (%):84.6 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)128 39.0 118
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-11 (0-6)
Lab Sample ID:L1784578-13 SDG:L1784578
Client Sample ID:S-11 (0-6)Collected Date/Time:09/30/24 08:40
Lab File ID:16 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.17 g
Total Solids (%):97.4 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)2280 33.9 103
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET SS-1 (12-18)
Lab Sample ID:L1784578-14 SDG:L1784578
Client Sample ID:SS-1 (12-18)Collected Date/Time:09/30/24 10:25
Lab File ID:17 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.49 g
Total Solids (%):88.3 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)151 37.4 113
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-14 (6-12)
Lab Sample ID:L1784578-15 SDG:L1784578
Client Sample ID:S-14 (6-12)Collected Date/Time:09/30/24 09:20
Lab File ID:18 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.33 g
Total Solids (%):86.3 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)U 38.2 116
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4130193-1
Lab Sample ID:R4130193-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:15
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)U 33.0 100
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131067-1
Lab Sample ID:R4131067-1 SDG:L1784578
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:01
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)U 33.0 100
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4130193-4
Lab Sample ID:R4130193-4 SDG:L1784578
Client Sample ID:DUP Collected Date/Time:09/30/24 10:10
Lab File ID:04 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:16
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.01 g
Total Solids (%):83.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)193 P1 39.8 121
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131067-4
Lab Sample ID:R4131067-4 SDG:L1784578
Client Sample ID:DUP Collected Date/Time:09/27/24 12:00
Lab File ID:04 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.44 g
Total Solids (%):93.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)1100 J3 35.2 107
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4130193-2
Lab Sample ID:R4130193-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:05 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:15
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3810 33.0 100
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131067-2
Lab Sample ID:R4131067-2 SDG:L1784578
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:05 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:01
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3510 33.0 100
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4130193-3
Lab Sample ID:R4130193-3 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:06 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:15
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3720 33.0 100
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131067-3
Lab Sample ID:R4131067-3 SDG:L1784578
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:06 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:01
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3630 33.0 100
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4130193-5
Lab Sample ID:R4130193-5 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/30/24 10:10
Lab File ID:07 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:16
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.02 g
Total Solids (%):83.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3950 J6 39.8 121
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131067-5
Lab Sample ID:R4131067-5 SDG:L1784578
Client Sample ID:MS Collected Date/Time:09/27/24 12:00
Lab File ID:07 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.43 g
Total Solids (%):93.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)4490 35.2 107
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4130193-6
Lab Sample ID:R4130193-6 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/30/24 10:10
Lab File ID:08 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/08/24 15:16
Analytical Batch:WG2378003 Analysis Date/Time:10/08/24 21:31
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10 g
Total Solids (%):83.0 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)3840 J6 39.8 121
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4131067-6
Lab Sample ID:R4131067-6 SDG:L1784578
Client Sample ID:MSD Collected Date/Time:09/27/24 12:00
Lab File ID:08 Received Date/Time:10/02/24 09:00
Instrument ID:OGBAL1 Preparation Date/Time:10/09/24 15:05
Analytical Batch:WG2378468 Analysis Date/Time:10/10/24 14:22
Dilution Factor:1 Prep Method:9071B
Analytical Method:9071B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:10.52 g
Total Solids (%):93.7 Final Wt/Vol:_______________
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)4350 35.2 107
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:_______________
Instrument ID:OGBAL1 Calibration (end) date/time:_______________
Analytical Method:9071B Analytical Run:WG2378003
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte mg/kg
OIL & GREASE
(HEXANE EXTR)U
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3-IN BLANKS
SDG:L1784578 Calibration (begin) date/time:_______________
Instrument ID:OGBAL1 Calibration (end) date/time:_______________
Analytical Method:9071B Analytical Run:WG2378468
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte mg/kg
OIL & GREASE
(HEXANE EXTR)U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4130193-5
L1784578-01,02,03 R4130193-6
MS Sample / File ID:R4130193-5 / 07 SDG:L1784578
MSD Sample / File ID:R4130193-6 / 08 Analytical Batch:WG2378003
OS Sample / File ID:L1784578-03 / 26 Matrix:Solid
Instrument ID:OGBAL1
Analytical Method:9071B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Oil & Grease (Hexane Extr)4820 120 3950 3840 79.3*77.3*1 80.0 - 120 2.58 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4131067-5
L1784578-04,05,06,07,08,11,12,13,14,15 R4131067-6
MS Sample / File ID:R4131067-5 / 07 SDG:L1784578
MSD Sample / File ID:R4131067-6 / 08 Analytical Batch:WG2378468
OS Sample / File ID:L1784578-06 / 11 Matrix:Solid
Instrument ID:OGBAL1
Analytical Method:9071B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Oil & Grease (Hexane Extr)4270 785 4490 4350 86.8 83.6 1 80.0 - 120 3.16 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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6-IN DUPLICATES SAMPLE NO.:
L1784578-01,02,03 R4130193-4
DUP Sample / File ID:R4130193-4 / 04 SDG:L1784578
OS Sample / File ID:L1784578-03 / 26 Analytical Batch:WG2378003
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:9071B Matrix:Solid
Analyte
OS
Result
(dry)
DUP
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)120 193 46.2*20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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6-IN DUPLICATES SAMPLE NO.:
L1784578-04,05,06,07,08,11,12,13,14,15 R4131067-4
DUP Sample / File ID:R4131067-4 / 04 SDG:L1784578
OS Sample / File ID:L1784578-06 / 11 Analytical Batch:WG2378468
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:9071B Matrix:Solid
Analyte
OS
Result
(dry)
DUP
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg mg/kg mg/kg
Oil & Grease (Hexane Extr)785 1100 33.8*20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4130193-2
RECOVERY R4130193-3
L1784578-01,02,03
LCS Sample / File ID:R4130193-2 / 05 SDG:L1784578
LCSD Sample / File ID:R4130193-3 / 06 Analytical Batch:WG2378003
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:9071B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg %%%%%
Oil & Grease (Hexane Extr)4000 3810 3720 95.3 93.0 80.0 - 120 2.39 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4131067-2
RECOVERY R4131067-3
L1784578-04,05,06,07,08,11,12,13,14,15
LCS Sample / File ID:R4131067-2 / 05 SDG:L1784578
LCSD Sample / File ID:R4131067-3 / 06 Analytical Batch:WG2378468
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:9071B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg %%%%%
Oil & Grease (Hexane Extr)4000 3510 3630 87.8 90.8 80.0 - 120 3.36 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784578-01,02,03,04,05,06,07,08,11,12,13,14,15 Analytical Method:9071B
Matrix:Solid Prep Method:9071B
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Oil & Grease (Hexane Extr)33 100
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:9071B
Instrument ID:OGBAL1 Calibration Start Date:_______________
Analytical Run:WG2378003 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4130193-1 01 10/08/24 21:31 1 WG2378003
DUP R4130193-4 04 10/08/24 21:31 1 WG2378003
LCS R4130193-2 05 10/08/24 21:31 1 WG2378003
LCSD R4130193-3 06 10/08/24 21:31 1 WG2378003
MS R4130193-5 07 10/08/24 21:31 1 WG2378003
MSD R4130193-6 08 10/08/24 21:31 1 WG2378003
S-13 (0-6)L1784578-01 24 10/08/24 21:31 1 WG2378003
S-15 (0-6)L1784578-02 25 10/08/24 21:31 1 WG2378003
S-32 (0-6)L1784578-03 26 10/08/24 21:31 1 WG2378003
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12-IN ANALYSIS LOG
SDG:L1784578 Analytical Method:9071B
Instrument ID:OGBAL1 Calibration Start Date:_______________
Analytical Run:WG2378468 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4131067-1 01 10/10/24 14:22 1 WG2378468
DUP R4131067-4 04 10/10/24 14:22 1 WG2378468
LCS R4131067-2 05 10/10/24 14:22 1 WG2378468
LCSD R4131067-3 06 10/10/24 14:22 1 WG2378468
MS R4131067-5 07 10/10/24 14:22 1 WG2378468
MSD R4131067-6 08 10/10/24 14:22 1 WG2378468
S-12 (6-12)L1784578-04 09 10/10/24 14:22 1 WG2378468
S-4 (12-18)L1784578-07 12 10/10/24 14:22 1 WG2378468
S-14 (0-6)L1784578-12 15 10/10/24 14:22 1 WG2378468
S-6 (12-18)L1784578-08 13 10/10/24 14:22 1 WG2378468
S-11 (0-6)L1784578-13 16 10/10/24 14:22 1 WG2378468
SS-1 (12-18)L1784578-14 17 10/10/24 14:22 1 WG2378468
S-14 (6-12)L1784578-15 18 10/10/24 14:22 1 WG2378468
S-12 (0-6)L1784578-05 10 10/10/24 14:22 1 WG2378468
S-10 (6-12)L1784578-11 14 10/10/24 14:22 1 WG2378468
S-10 (0-6)L1784578-06 11 10/10/24 14:22 1 WG2378468
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
COD Coefficient of Determination.
Corr.Correlation Coefficient.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
Incpt Intercept.
Mass Mass of parameter.
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
RRF Relative Response Factor.
RT Retention Time.
SDG Sample Delivery Group.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Slope Slope of calibration curve.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Wavelength Wavelength of parameter.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
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GLOSSARY OF TERMS
Qualifier Description
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
V The sample concentration is too high to evaluate accurate spike recoveries.
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
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ANALYTICAL REPORT
November 05, 2024
Geosyntec Consultants - UT
Sample Delivery Group:L1791693
Samples Received:10/02/2024
Project Number:SLC1091
Description:Paxton Ave.
Report To:Brian Smith
215 South State Street
Suite 500
Salt Lake City, UT 84111
Entire Report Reviewed By:
November 05, 2024
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com
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November 05, 2024
Chris Ward
Project Manager
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TABLE OF CONTENTSTABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 4
Cn: Case Narrative 5
Su: Summary Results 6
2540 G-2011 Total Solids 6
Sample Result Inorganic Analysis Data Sheet 7
L1791693-01 10/05/24 15:11 LOGBAL1 7
BLANK(R4129341-1) WG2376181 10/05/24 15:11 LOGBAL1 8
DUP(R4129341-3) WG2376181 10/05/24 15:11 LOGBAL1 9
LCS(R4129341-2) WG2376181 10/05/24 15:11 LOGBAL1 10
Blank 11
LOGBAL1 WG2376181 11
Laboratory Duplicate 12
WG2376181 DUP(R4129341-3) 12
Laboratory Control Sample / Duplicate 13
WG2376181 LCS(R4129341-2) 13
Detection Limit Summary 14
2540 G-2011 - Solid 14
Analysis Log 15
LOGBAL1 WG2376181 15
6010B Metals (ICP) 16
Sample Result Inorganic Analysis Data Sheet 17
L1791693-01 11/02/24 17:11 ICP13 17
BLANK(R4141311-1) WG2393511 11/02/24 17:05 ICP13 18
LCS(R4141311-2) WG2393511 11/02/24 17:08 ICP13 19
MS(R4141311-5) WG2393511 11/02/24 17:19 ICP13 20
MSD(R4141311-6) WG2393511 11/02/24 17:22 ICP13 21
PS(R4141311-4) WG2393511 11/02/24 17:16 ICP13 22
SD(R4141311-3) WG2393511 11/02/24 17:13 ICP13 23
Calibration Verification 24
ICP13 110224ICP13 24
Blank 26
ICP13 110224ICP13 26
ICP Interference Check Sample 27
ICP13 11/02/24 10:40 27
ICP13 11/02/24 16:25 28
ICP13 11/02/24 20:29 29
Matrix Spike / Duplicate 30
WG2393511 MS(R4141311-5) MSD(R4141311-6) 30
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Post Digestion Spike 31
WG2393511 PS(R4141311-4) 31
Laboratory Control Sample / Duplicate 32
WG2393511 LCS(R4141311-2) 32
Serial Dilution 33
WG2393511 SD(R4141311-3) 33
Detection Limit Summary 34
6010B - Solid 34
Interelement Correction Factor 35
ICP13 07/28/23 07:16 35
Linear Dynamic Range 38
ICP13 01/25/24 15:12 38
Analysis Log 39
ICP13 110224ICP13 11/02/24 09:56 39
Initial Calibration Recovery 40
ICP13 110224ICP13 11/02/24 09:56 40
Initial Calibration 43
ICP13 110224ICP13 11/02/24 09:56 43
Gl: Glossary of Terms 44
Al: Accreditations & Locations 45
Sc: Sample Chain of Custody 46
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-6 (12-18) L1791693-01 Solid Jessica Welch 09/27/24 15:20 10/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2376181 1 10/05/24 14:59 10/05/24 15:11 JAV Mt. Juliet, TN
Metals (ICP) by Method 6010B WG2393511 1 11/01/24 10:20 11/02/24 17:11 MAP Mt. Juliet, TN
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 11/05/24 10:52
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Chris Ward
Project Manager
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2540 G-2011 Total Solids
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (12-18)
Lab Sample ID:L1791693-01 SDG:L1791693
Client Sample ID:S-6 (12-18)Collected Date/Time:09/27/24 15:20
Lab File ID:14 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:59
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:6.689 g
Total Solids (%):90.7 Final Wt/Vol:6.188 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 90.7
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129341-1
Lab Sample ID:R4129341-1 SDG:L1791693
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:56
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:1.302 g
Total Solids (%):_______________Final Wt/Vol:1.305 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 0.00300
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129341-3
Lab Sample ID:R4129341-3 SDG:L1791693
Client Sample ID:DUP Collected Date/Time:09/27/24 12:00
Lab File ID:02 Received Date/Time:10/02/24 09:00
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:56
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:9.281 g
Total Solids (%):93.7 Final Wt/Vol:8.74 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 93.2
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4129341-2
Lab Sample ID:R4129341-2 SDG:L1791693
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:03 Received Date/Time:_______________
Instrument ID:LOGBAL1 Preparation Date/Time:10/05/24 14:56
Analytical Batch:WG2376181 Analysis Date/Time:10/05/24 15:11
Dilution Factor:1 Prep Method:SM 2540 G
Analytical Method:2540 G-2011 Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:11.304 g
Total Solids (%):_______________Final Wt/Vol:6.311 g
Analyte CAS Result Qualifier
%
Total Solids TSOLIDS 50.1
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3-IN BLANKS
SDG:L1791693 Calibration (begin) date/time:_______________
Instrument ID:LOGBAL1 Calibration (end) date/time:_______________
Analytical Method:2540 G-2011 Analytical Run:WG2376181
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte %
TOTAL SOLIDS 0.00300
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6-IN DUPLICATES SAMPLE NO.:
L1791693-01 R4129341-3
DUP Sample / File ID:R4129341-3 / 02 SDG:L1791693
OS Sample / File ID:L1784578-06 / 09 Analytical Batch:WG2376181
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte OS
Result
DUP
Result RPD RPD
Limits
%%%%
Total Solids 93.7 93.2 0.463 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129341-2
RECOVERY _______________
L1791693-01
LCS Sample / File ID:R4129341-2 / 03 SDG:L1791693
LCSD Sample / File ID:_______________Analytical Batch:WG2376181
Instrument ID:LOGBAL1 Dilution Factor:1
Analytical Method:2540 G-2011 Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
%%%%%%%
Total Solids 50.0 50.1 100 90.0 - 110
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1791693-01 Analytical Method:2540 G-2011
Matrix:Solid Prep Method:SM 2540 G
Analyte CAS Wavelength Mass MDL RDL
%%
Total Solids TSOLIDS
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12-IN ANALYSIS LOG
SDG:L1791693 Analytical Method:2540 G-2011
Instrument ID:LOGBAL1 Calibration Start Date:_______________
Analytical Run:WG2376181 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4129341-1 01 10/05/24 15:11 1 WG2376181
DUP R4129341-3 02 10/05/24 15:11 1 WG2376181
LCS R4129341-2 03 10/05/24 15:11 1 WG2376181
OS L1784578-06 09 10/05/24 15:11
S-6 (12-18)L1791693-01 14 10/05/24 15:11 1 WG2376181
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6010B Metals (ICP)
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET S-6 (12-18)
Lab Sample ID:L1791693-01 SDG:L1791693
Client Sample ID:S-6 (12-18)Collected Date/Time:09/27/24 15:20
Lab File ID:20241102171108 Received Date/Time:10/02/24 09:00
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:11
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):90.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Lead 7439-92-1 482 J3 V 0.229 0.551
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4141311-1
Lab Sample ID:R4141311-1 SDG:L1791693
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:20241102170528 Received Date/Time:_______________
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:05
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.52 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Lead 7439-92-1 U 0.208 0.500
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4141311-2
Lab Sample ID:R4141311-2 SDG:L1791693
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:20241102170807 Received Date/Time:_______________
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:08
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.49 g
Total Solids (%):_______________Final Wt/Vol:50 mL
Analyte CAS Result Qualifier MDL RDL
mg/kg mg/kg mg/kg
Lead 7439-92-1 99.6 0.208 0.500
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4141311-5
Lab Sample ID:R4141311-5 SDG:L1791693
Client Sample ID:MS Collected Date/Time:09/27/24 15:20
Lab File ID:20241102171952 Received Date/Time:10/02/24 09:00
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:19
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.51 g
Total Solids (%):90.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Lead 7439-92-1 2040 V 0.229 0.551
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4141311-6
Lab Sample ID:R4141311-6 SDG:L1791693
Client Sample ID:MSD Collected Date/Time:09/27/24 15:20
Lab File ID:20241102172253 Received Date/Time:10/02/24 09:00
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:22
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.54 g
Total Solids (%):90.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Lead 7439-92-1 527 J3 V 0.229 0.551
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4141311-4
Lab Sample ID:R4141311-4 SDG:L1791693
Client Sample ID:PS Collected Date/Time:09/27/24 15:20
Lab File ID:20241102171654 Received Date/Time:10/02/24 09:00
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:16
Dilution Factor:1 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):90.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Lead 7439-92-1 577 0.229 0.551
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4141311-3
Lab Sample ID:R4141311-3 SDG:L1791693
Client Sample ID:SD Collected Date/Time:09/27/24 15:20
Lab File ID:20241102171354 Received Date/Time:10/02/24 09:00
Instrument ID:ICP13 Preparation Date/Time:11/01/24 10:20
Analytical Batch:WG2393511 Analysis Date/Time:11/02/24 17:13
Dilution Factor:5 Prep Method:3051
Analytical Method:6010B Sample Vol Used:_______________
Matrix:Solid Initial Wt/Vol:0.55 g
Total Solids (%):90.7 Final Wt/Vol:50 mL
Analyte CAS Result (dry)Qualifier MDL (dry)RDL (dry)
mg/kg mg/kg mg/kg
Lead 7439-92-1 457 1.15 2.76
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2-IN CALIBRATION VERIFICATION
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Concentration Units:mg/l
ICV ICVLL CCV
Sample ID:ICP131102241015 ICP131102241037 ICP131102241615
Analyte True Found %R %RSD True Found %R %RSD True Found %R %RSD
LEAD 1 0.9481699 94.8
0 0.538000 0.0050 0.005250881 105 18.500000 0.50 0.5049635 101 0.337000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
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2-IN CALIBRATION VERIFICATION
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Concentration Units:mg/l
CCVLL CCV
Sample ID:ICP131102241622 ICP131102241731
Analyte True Found %R %RSD True Found %R %RSD
LEAD 0.0050 0.006312087 126 25.800000 0.50 0.5125307 103 0.075000
ICV Limits:90 - 110 ICVLL Limits:50 - 150 CCV Limits:90 - 110 CCVLL Limits:50 - 150
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3-IN BLANKS
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Sample ID:ICB Result ICB Qual CCB Result CCB Qual BLANK Result BLANK
Qual CCB Result CCB Qual
File ID:20241102102408 20241102161850 20241102170528 20241102173422
Analyte mg/l mg/l mg/kg mg/l
LEAD 0.0001507766 U 0.0001839608 U U 0.002028559 U
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4-IN INTERFERENCE CHECK SAMPLE
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:11/02/24 10:40
Instrument Run:110224ICP13
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 502.5472 101 500 503.2424 101
ANTIMONY 0 0.003012036 0.50 0.5016268 100
ARSENIC 0 -0.004047744 0.50 0.502607 101
BARIUM 0 0.002372679 0.50 0.4961711 99.20
BERYLLIUM 0 0.0006444008 0.50 0.4932577 98.70
BORON 0 -0.003273668 1 0.975883 97.60
CADMIUM 0 0.001665445 1 1.013752 101
CALCIUM 500 499.7896 100 500 500.5515 100
CERIUM 0 -0.04911886 0 -0.07344419
CHROMIUM 0 0.0008744604 0.50 0.4915725 98.30
COBALT 0 0.001993349 0.50 0.4921932 98.40
COPPER 0 0.005588594 0.50 0.5340551 107
IRON 200 200.1648 100 200 200.9077 100
LANTHANUM 0 -0.01667469 0 -0.01804495
LEAD 0 0.0001378526 1 0.9850439 98.50
LITHIUM 0 0.008406338 0 0.008418476
MAGNESIUM 500 497.0501 99.40 500 497.9751 99.60
MANGANESE 0 0.002628202 0.50 0.4942535 98.90
MOLYBDENUM 0 0.001176092 0.50 0.4826801 96.50
NICKEL 0 -0.004218652 1 0.963441 96.30
PHOSPHORUS 0 0.004860748 0 0.004531775
POTASSIUM 0 0.07871525 0 0.09349205
SELENIUM 0 0.000001484058 0.50 0.4945375 98.90
SILICON 0 0.01696691 1 1.007145 101
SILVER 0 -0.000009604364 1 0.8544639 85.40
SODIUM 0 0.03617114 0 0.06243972
STRONTIUM 0 0.003899261 0 0.003662726
SULFUR 0 -0.4377862 0 -0.4223515
THALLIUM 0 -0.001631569 0.50 0.492819 98.60
TIN 0 -0.001957575 0.50 0.4750316 95
TITANIUM 0 0.007133892 0.50 0.4878748 97.60
VANADIUM 0 0.0009833154 0.50 0.4675497 93.50
ZINC 0 0.0005107407 1 0.9399432 94
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4-IN INTERFERENCE CHECK SAMPLE
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:11/02/24 16:25
Instrument Run:110224ICP13
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 491.7576 98.40 500 492.8336 98.60
ANTIMONY 0 -0.001471063 0.50 0.5138184 103
ARSENIC 0 -0.01560031 0.50 0.4977434 99.50
BARIUM 0 0.002144886 0.50 0.4964715 99.30
BERYLLIUM 0 0.0006816499 0.50 0.4974741 99.50
BORON 0 0.002063603 1 0.9720705 97.20
CADMIUM 0 0.0009333664 1 1.02012 102
CALCIUM 500 479.0732 95.80 500 479.4894 95.90
CERIUM 0 -0.14565 0 -0.1328964
CHROMIUM 0 0.0005961675 0.50 0.4892386 97.80
COBALT 0 0.001686338 0.50 0.4908774 98.20
COPPER 0 0.004796086 0.50 0.5453611 109
IRON 200 198.6318 99.30 200 198.7151 99.40
LANTHANUM 0 -0.0160036 0 -0.01774344
LEAD 0 0.002823053 1 0.9973561 99.70
LITHIUM 0 0.009790258 0 0.00938933
MAGNESIUM 500 496.6359 99.30 500 496.6752 99.30
MANGANESE 0 0.002596092 0.50 0.4960364 99.20
MOLYBDENUM 0 -0.0001834128 0.50 0.4822552 96.50
NICKEL 0 -0.005519574 1 0.9443524 94.40
PHOSPHORUS 0 0.01612778 0 0.003726896
POTASSIUM 0 0.04953355 0 0.08671382
SELENIUM 0 -0.006234646 0.50 0.5014393 100
SILICON 0 0.02158924 1 1.006388 101
SILVER 0 -0.0006716511 1 0.9980714 99.80
SODIUM 0 0.04706037 0 0.0615227
STRONTIUM 0 0.003939264 0 0.003836154
SULFUR 0 -0.4243353 0 -0.413215
THALLIUM 0 -0.0006806794 0.50 0.5028364 101
TIN 0 -0.001749944 0.50 0.4792218 95.80
TITANIUM 0 0.006929341 0.50 0.4944575 98.90
VANADIUM 0 0.0000859174 0.50 0.4701498 94
ZINC 0 -0.0002929 1 0.9326228 93.30
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4-IN INTERFERENCE CHECK SAMPLE
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:11/02/24 20:29
Instrument Run:110224ICP13
Analyte True Found True Found
ICSA ICSA ICSA ICSAB ICSAB ICSAB
mg/l mg/l % Rec.mg/l mg/l % Rec.
ALUMINUM 500 490.4063 98.10 500 488.1402 97.60
ANTIMONY 0 0.004431065 0.50 0.5160712 103
ARSENIC 0 -0.004669839 0.50 0.4908545 98.20
BARIUM 0 0.001981965 0.50 0.4920731 98.40
BERYLLIUM 0 0.0006884228 0.50 0.4944702 98.90
BORON 0 -0.004092802 1 0.9416452 94.20
CADMIUM 0 0.001631375 1 1.012356 101
CALCIUM 500 477.7689 95.60 500 473.938 94.80
CERIUM 0 -0.1245297 0 -0.1488599
CHROMIUM 0 0.0008521775 0.50 0.488514 97.70
COBALT 0 0.001573751 0.50 0.4874467 97.50
COPPER 0 0.004356423 0.50 0.5430952 109
IRON 200 196.6657 98.30 200 195.5627 97.80
LANTHANUM 0 -0.01754133 0 -0.01979841
LEAD 0 0.004466975 1 0.9905223 99.10
LITHIUM 0 0.01108 0 0.01052802
MAGNESIUM 500 491.6842 98.30 500 487.9847 97.60
MANGANESE 0 0.002551143 0.50 0.489059 97.80
MOLYBDENUM 0 -0.00007508884 0.50 0.4768036 95.40
NICKEL 0 -0.005857996 1 0.9319159 93.20
PHOSPHORUS 0 0.008609374 0 0.02243596
POTASSIUM 0 0.05278199 0 0.06272512
SELENIUM 0 -0.005142691 0.50 0.5028976 101
SILICON 0 0.01756862 1 0.9776344 97.80
SILVER 0 -0.001156385 1 0.8112905 81.10
SODIUM 0 0.06430284 0 0.06499734
STRONTIUM 0 0.004152606 0 0.003895642
SULFUR 0 -0.4238207 0 -0.464742
THALLIUM 0 -0.006141939 0.50 0.4993759 99.90
TIN 0 -0.001444235 0.50 0.4814113 96.30
TITANIUM 0 0.006213727 0.50 0.4922301 98.40
VANADIUM 0 0.0006595684 0.50 0.4680823 93.60
ZINC 0 0.0003073071 1 0.9279282 92.80
ICSA Limits:80 - 120 ICSAB Limits:80 - 120
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4141311-5
L1791693-01 R4141311-6
MS Sample / File ID:R4141311-5 / 20241102171952 SDG:L1791693
MSD Sample / File ID:R4141311-6 / 20241102172253 Analytical Batch:WG2393511
OS Sample / File ID:L1791693-01 / 20241102171108 Matrix:Solid
Instrument ID:ICP13
Analytical Method:6010B
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
MS
Result
(dry)
MSD
Result
(dry)
MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/kg mg/kg mg/kg mg/kg %%%%%
Lead 110 482 2040 527 1410*40.7*1 75.0 - 125 118*20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5B-IN POST-DIGESTION / DISTILLATION SPIKE SAMPLE NO.:
SAMPLE RECOVERY R4141311-4
L1791693-01
PS Sample / File ID:R4141311-4 / 20241102171654 SDG:L1791693
OS Sample / File ID:L1791693-01 / 20241102171108 Analytical Batch:WG2393511
Instrument ID:ICP13 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte
Spike
Amount
(dry)
OS
Result
(dry)
PD
Result
(dry)
DS
Result
(dry)
PD Rec.DS Rec.Dilution Rec.
Limits RPD RPD
Limits
mg/kg mg/kg mg/kg %%%mg/kg mg/kg
Lead 110 482 577 86.2 1 80.0 -
120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4141311-2
RECOVERY _______________
L1791693-01
LCS Sample / File ID:R4141311-2 / 20241102170807 SDG:L1791693
LCSD Sample / File ID:_______________Analytical Batch:WG2393511
Instrument ID:ICP13 Dilution Factor:1
Analytical Method:6010B Matrix:Solid
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/kg mg/kg %%%%%
Lead 100 99.6 99.6 80.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8-IN ICP AND ICP/MS SAMPLE NO.:
SERIAL DILUTIONS R4141311-3
L1791693-01
SD Sample / File ID:R4141311-3 / 20241102171354 SDG:L1791693
OS Sample / File ID:L1791693-01 / 20241102171108 Analytical Batch:WG2393511
Lab File ID:20241102171354 Dilution Factor:5
Instrument ID:ICP13 Matrix:Solid
Analytical Method:6010B
Analyte
OS
Result
(dry)
SD
Result
(dry)
RPD RPD
Limits
mg/kg mg/kg %%
Lead 482 457 5.21 10
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1791693-01 Analytical Method:6010B
Matrix:Solid Prep Method:3051
Analyte CAS Wavelength Mass MDL RDL
mg/kg mg/kg
Lead 7439-92-1 177.4950 220.3530 0.2080 0.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10A-IN INTERELEMENT CORRECTION FACTORS
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:07/28/23 07:16
Analyte Wavelength ARSENIC CERIUM CHROMIUM COBALT COPPER IRON LANTHANUM
nm 189.0420 535.3530 267.7160 228.6160 324.7540 271.4410 333.7490
ALUMINUM 308.2150
ANTIMONY 206.8330 -0.00043260
ARSENIC 189.0420 -0.00532076
BERYLLIUM 313.0420
CADMIUM 228.8020 -0.15291673
COBALT 228.6160
LEAD 220.3530 -0.00035078 -0.00001401 -0.00041235 0.00000145
NICKEL 231.6040 -0.00098060
PHOSPHORU
S 177.4950
THALLIUM 190.8560 -0.00008407
TITANIUM 334.9410 -0.00012044
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10A-IN INTERELEMENT CORRECTION FACTORS
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:07/28/23 07:16
Analyte Wavelength MAGNESIUM MANGANESE MOLYBDENUM POTASSIUM SILICON SULFUR TITANIUM
nm 279.0790 257.61 202.03 766.49 251.6110 182.0340 334.9410
ALUMINUM 308.2150 -0.00393995
ANTIMONY 206.8330 -0.00013070 -0.00001138 -0.00557514
ARSENIC 189.0420 -0.00023896
BERYLLIUM 313.0420
CADMIUM 228.8020
COBALT 228.6160 -0.00163701
LEAD 220.3530 -0.00003453
NICKEL 231.6040
PHOSPHORU
S 177.4950 -0.00001698
THALLIUM 190.8560 -0.00000157 -0.00027950
TITANIUM 334.9410
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10A-IN INTERELEMENT CORRECTION FACTORS
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:07/28/23 07:16
Analyte Wavelength VANADIUM ZINC
nm 292.4020 206.20
ALUMINUM 308.2150
ANTIMONY 206.8330 -0.00016041
ARSENIC 189.0420
BERYLLIUM 313.0420 -0.01698239
CADMIUM 228.8020
COBALT 228.6160
LEAD 220.3530
NICKEL 231.6040
PHOSPHORU
S 177.4950 -0.00005985
THALLIUM 190.8560
TITANIUM 334.9410
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10C-IN LINEAR DYNAMIC RANGE
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Date:01/25/24 15:12
Analyte LDR
ppm
ALUMINUM 500
ANTIMONY 10
ARSENIC 50
BARIUM 50
BERYLLIUM 10
BORON 50
CADMIUM 10
CALCIUM 1000
CHROMIUM 50
COBALT 50
COPPER 50
IRON 500
LEAD 100
LITHIUM 10
MAGNESIUM 1000
MANGANESE 20
MOLYBDENUM 20
NICKEL 50
PHOSPHORUS 200
POTASSIUM 500
SELENIUM 10
SILICON 100
SILVER 10
SODIUM 1000
STRONTIUM 20
SULFUR 200
THALLIUM 10
TIN 50
TITANIUM 50
VANADIUM 20
ZINC 20
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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12-IN ANALYSIS LOG
SDG:L1791693 Analytical Method:6010B
Instrument ID:ICP13 Calibration Start Date:11/02/24 09:56
Analytical Run:110224ICP13 Calibration End Date:11/02/24 10:12
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CALBLK ICP131102240953 20241102095338 11/02/24 09:53
CAL STD1 20241102095623 11/02/24 09:56
CAL STD2 20241102095903 11/02/24 09:59
CAL STD3 20241102100137 11/02/24 10:01
CAL STD4 20241102100409 11/02/24 10:04
CAL STD5 20241102100640 11/02/24 10:06
CAL STD6 20241102100939 11/02/24 10:09
CAL STD7 20241102101246 11/02/24 10:12
ICV ICP131102241015 20241102101548 11/02/24 10:15
ICB ICP131102241024 20241102102408 11/02/24 10:24
ICVLL ICP131102241037 20241102103736 11/02/24 10:37
ICSA ICP131102241040 20241102104036 11/02/24 10:40
ICSAB ICP131102241043 20241102104325 11/02/24 10:43
CCV ICP131102241615 20241102161553 11/02/24 16:15
CCB ICP131102241618 20241102161850 11/02/24 16:18
CCVLL ICP131102241622 20241102162209 11/02/24 16:22
ICSA ICP131102241625 20241102162509 11/02/24 16:25
ICSAB ICP131102241627 20241102162759 11/02/24 16:27
ICSAB ICP131102241638 20241102163817 11/02/24 16:38
BLANK R4141311-1 20241102170528 11/02/24 17:05 1 WG2393511
LCS R4141311-2 20241102170807 11/02/24 17:08 1 WG2393511
S-6 (12-18)L1791693-01 20241102171108 11/02/24 17:11 1 WG2393511
SD R4141311-3 20241102171354 11/02/24 17:13 5 WG2393511
PS R4141311-4 20241102171654 11/02/24 17:16 1 WG2393511
MS R4141311-5 20241102171952 11/02/24 17:19 1 WG2393511
MSD R4141311-6 20241102172253 11/02/24 17:22 1 WG2393511
L1782974-10 L1782974-10 20241102172558 11/02/24 17:25 1 WG2393511
CCV ICP131102241731 20241102173125 11/02/24 17:31
CCB ICP131102241734 20241102173422 11/02/24 17:34
ICSA ICP131102242029 20241102202947 11/02/24 20:29
ICSAB ICP131102242032 20241102203237 11/02/24 20:32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
LEAD 0.0050 .005043117 101 0.10 .09931334 99.30
File ID: 20241102095623 20241102095903
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
LEAD 0.20 .1987223 99.40 0.50 .5037809 101
File ID: 20241102100137 20241102100409
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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15-IN INITIAL CALIBRATION RECOVERY
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Analyte Std Conc Result Rec.Std Conc Result Rec.
mg/l mg/l %mg/l mg/l %
LEAD 1 .9788762 97.90 2 2.009779 100
File ID: 20241102100640 20241102100939
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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16A-IN INITIAL
CALIBRATION
SDG:L1791693 Calibration (begin) date/time:11/02/24 09:56
Instrument ID:ICP13 Calibration (end) date/time:11/02/24 10:12
Analytical Method:6010B Analytical Run:110224ICP13
Analyte Wavelength Cal. Type Weightage Corr.Slope Incpt
LEAD 220.353 8 5 0.999914 708.1415 -0.13113
Calibration Type
8 = Linear Regression Forced through Blank
Weightage
5 = None
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
Corr.Correlation Coefficient.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
Incpt Intercept.
Mass Mass of parameter.
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Slope Slope of calibration curve.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Wavelength Wavelength of parameter.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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ANALYTICAL REPORT
August 05, 2024
Geosyntec Consultants - UT
Sample Delivery Group:L1758896
Samples Received:07/20/2024
Project Number:
Description:Paxton
Report To:Brian Smith
215 South State Street
Suite 500
Salt Lake City, UT 84111
Entire Report Reviewed By:
August 05, 2024
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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August 05, 2024
Chris Ward
Project Manager
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TABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTSTABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 8
Cn: Case Narrative 10
Su: Summary Results 11
1664A Wet Chemistry 11
Sample Result Inorganic Analysis Data Sheet 12
L1758896-01 07/28/24 17:36 OGBAL1 12
L1758896-02 07/28/24 17:36 OGBAL1 13
L1758896-03 07/28/24 17:36 OGBAL1 14
L1758896-04 07/28/24 17:36 OGBAL1 15
L1758896-05 07/28/24 17:36 OGBAL1 16
L1758896-06 07/28/24 17:36 OGBAL1 17
L1758896-07 07/28/24 17:36 OGBAL1 18
L1758896-08 07/28/24 17:36 OGBAL1 19
L1758896-09 07/28/24 17:36 OGBAL1 20
L1758896-10 07/28/24 17:36 OGBAL1 21
BLANK(R4099402-1) WG2331265 07/28/24 17:36 OGBAL1 22
LCS(R4099402-2) WG2331265 07/28/24 17:36 OGBAL1 23
LCSD(R4099402-3) WG2331265 07/28/24 17:36 OGBAL1 24
MS(R4099402-4) WG2331265 07/28/24 17:36 OGBAL1 25
MSD(R4099402-5) WG2331265 07/28/24 17:36 OGBAL1 26
Blank 27
OGBAL1 WG2331265 27
Matrix Spike / Duplicate 28
WG2331265 MS(R4099402-4) MSD(R4099402-5) 28
Laboratory Control Sample / Duplicate 29
WG2331265 LCS(R4099402-2) LCSD(R4099402-3) 29
Detection Limit Summary 30
1664A - GW 30
Analysis Log 31
OGBAL1 WG2331265 31
3511/8015 Semi-Volatile Organic Compounds (GC) 32
Surrogate Recovery 33
GW Surrogate Summary 33
Matrix Spike / Duplicate 34
WG2332252 MS(R4100686-1) MSD(R4100686-2) 34
Laboratory Control Sample / Duplicate 35
WG2332252 LCS(R4100691-1) 35
Method Blank 36
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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WG2332252 R4100691-2 SVGC31 07/31/24 04:42 36
Sample Result Summary Organic Analysis Data Sheet 37
L1758896-01 07/30/24 21:37 SVGC47 37
L1758896-02 07/30/24 21:59 SVGC47 38
L1758896-03 07/31/24 00:13 SVGC47 39
L1758896-04 07/30/24 22:22 SVGC47 40
L1758896-05 07/30/24 22:44 SVGC47 41
L1758896-06 08/01/24 13:23 SVGC26 42
L1758896-07 07/30/24 23:28 SVGC47 43
L1758896-08 07/30/24 23:50 SVGC47 44
L1758896-09 08/01/24 11:58 SVGC27 45
L1758896-10 07/31/24 14:09 SVGC21 46
Retention Time of Single Component Analytes 47
SVGC21 07/26/24 07:27 47
SVGC26 06/27/24 12:09 48
SVGC27 05/30/24 02:22 49
SVGC31 07/18/24 09:57 50
SVGC47 05/10/24 06:54 51
Calibration Factor of Single Component Analytes 52
SVGC21 07/26/24 07:27 52
SVGC26 06/27/24 12:09 54
SVGC27 05/30/24 02:22 56
SVGC31 07/18/24 09:57 58
SVGC47 05/10/24 06:54 60
Calibration Verification Single Component Analytes 62
SVGC21 07/26/24 11:53 62
SVGC21 07/31/24 08:42 63
SVGC21 07/31/24 20:55 64
SVGC26 08/01/24 12:22 65
SVGC26 08/01/24 20:53 66
SVGC27 05/30/24 05:28 67
SVGC27 07/31/24 22:26 68
SVGC27 08/01/24 13:00 69
SVGC31 07/18/24 13:00 70
SVGC31 07/30/24 20:02 71
SVGC31 07/31/24 00:03 72
SVGC31 07/31/24 09:01 73
SVGC47 07/03/24 14:47 74
SVGC47 07/30/24 20:53 75
SVGC47 07/31/24 06:08 76
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Analytical Sequence 77
SVGC21 07/26/24 07:27 77
SVGC26 06/27/24 12:09 78
SVGC27 05/30/24 02:22 79
SVGC31 07/18/24 09:57 80
SVGC47 05/10/24 06:54 81
Detection Limit Summary 82
3511/8015 - GW 82
QC Result Summary Organic Analysis Data Sheet 83
BLANK(R4100691-2) WG2332252 07/31/24 04:42 SVGC31 83
LCS(R4100691-1) WG2332252 07/30/24 22:23 SVGC31 84
MS(R4100686-1) WG2332252 07/31/24 00:35 SVGC47 85
MSD(R4100686-2) WG2332252 07/31/24 00:57 SVGC47 86
8015D/GRO Volatile Organic Compounds (GC) 87
Surrogate Recovery 88
GW Surrogate Summary 88
Matrix Spike / Duplicate 89
WG2329885 MS(R4099262-3) MSD(R4099262-4) 89
Laboratory Control Sample / Duplicate 90
WG2329885 LCS(R4099262-1) 90
Method Blank 91
WG2329885 R4099262-2 VOCGC6 07/25/24 10:52 91
Internal Standard & Retention Time 92
VOCGC6 07/25/24 10:08 92
Sample Result Summary Organic Analysis Data Sheet 93
L1758896-01 07/25/24 12:15 VOCGC6 93
L1758896-02 07/25/24 12:37 VOCGC6 94
L1758896-03 07/25/24 13:00 VOCGC6 95
L1758896-04 07/25/24 13:22 VOCGC6 96
L1758896-05 07/25/24 13:45 VOCGC6 97
L1758896-06 07/25/24 14:08 VOCGC6 98
L1758896-07 07/25/24 14:31 VOCGC6 99
L1758896-08 07/25/24 14:53 VOCGC6 100
L1758896-09 07/25/24 15:15 VOCGC6 101
L1758896-10 07/25/24 15:38 VOCGC6 102
Retention Time of Single Component Analytes 103
VOCGC6 07/18/24 16:32 103
Calibration Factor of Single Component Analytes 104
VOCGC6 07/18/24 16:32 104
Calibration Verification Single Component Analytes 106
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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VOCGC6 07/19/24 01:12 106
VOCGC6 07/25/24 10:08 107
Analytical Sequence 108
VOCGC6 07/18/24 16:32 108
Detection Limit Summary 109
8015D/GRO - GW 109
QC Result Summary Organic Analysis Data Sheet 110
BLANK(R4099262-2) WG2329885 07/25/24 10:52 VOCGC6 110
LCS(R4099262-1) WG2329885 07/25/24 10:08 VOCGC6 111
MS(R4099262-3) WG2329885 07/25/24 19:52 VOCGC6 112
MSD(R4099262-4) WG2329885 07/25/24 20:15 VOCGC6 113
8260B Volatile Organic Compounds (GC/MS) 114
Surrogate Recovery 115
GW Surrogate Summary 115
Matrix Spike / Duplicate 116
WG2330260 MS(R4099344-3) MSD(R4099344-4) 116
Laboratory Control Sample / Duplicate 118
WG2330346 LCS(R4098893-1) LCSD(R4098893-4) 118
WG2330260 LCS(R4099344-1) 120
WG2332276 LCS(R4100703-1) 122
Method Blank 123
WG2330260 R4099344-2 VOCMS13 07/26/24 09:41 123
WG2330346 R4098893-3 VOCMS16 07/25/24 22:50 124
WG2332276 R4100703-2 VOCMS26 07/29/24 19:59 125
GC/MS Performance Check 126
VOCMS13 062824 06/28/24 10:39 126
VOCMS13 072624 07/26/24 08:18 127
VOCMS16 071724A 07/17/24 19:17 128
VOCMS16 072524 07/25/24 21:23 129
VOCMS26 062124 06/21/24 17:15 130
VOCMS26 072924A 07/29/24 19:18 131
Internal Standard & Retention Time 132
VOCMS13 07/26/24 09:00 132
VOCMS16 07/25/24 21:45 133
VOCMS26 07/29/24 19:18 134
Sample Result Summary Organic Analysis Data Sheet 135
L1758896-01 07/26/24 12:11 VOCMS13 135
L1758896-02 07/26/24 12:32 VOCMS13 137
L1758896-03 07/26/24 12:53 VOCMS13 139
L1758896-04 07/26/24 13:13 VOCMS13 141
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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L1758896-04 07/29/24 22:55 VOCMS26 143
L1758896-05 07/26/24 13:34 VOCMS13 144
L1758896-05 07/29/24 23:16 VOCMS26 146
L1758896-06 07/26/24 13:55 VOCMS13 147
L1758896-07 07/26/24 14:16 VOCMS13 149
L1758896-07 07/29/24 23:36 VOCMS26 151
L1758896-08 07/26/24 14:37 VOCMS13 152
L1758896-08 07/29/24 23:56 VOCMS26 154
L1758896-09 07/26/24 14:58 VOCMS13 155
L1758896-09 07/29/24 20:32 VOCMS26 157
L1758896-10 07/26/24 07:35 VOCMS16 158
L1758896-11 07/26/24 00:18 VOCMS16 160
GC/MS Initial Calibration 162
VOCMS13 06/28/24 11:00 162
VOCMS16 07/17/24 19:39 166
VOCMS26 06/21/24 17:35 170
GC/MS Calibration Verification 172
VOCMS13 06/28/24 15:35 172
VOCMS13 07/26/24 09:00 174
VOCMS16 07/17/24 23:39 176
VOCMS16 07/18/24 00:23 178
VOCMS16 07/25/24 21:45 179
VOCMS26 06/21/24 22:23 181
VOCMS26 07/29/24 19:18 183
Analytical Sequence 185
VOCMS13 06/28/24 11:00 185
VOCMS16 07/17/24 19:39 186
VOCMS26 06/21/24 17:35 187
Detection Limit Summary 188
8260B - GW 188
QC Result Summary Organic Analysis Data Sheet 190
BLANK(R4098893-3) WG2330346 07/25/24 22:50 VOCMS16 190
BLANK(R4099344-2) WG2330260 07/26/24 09:41 VOCMS13 192
BLANK(R4100703-2) WG2332276 07/29/24 19:59 VOCMS26 194
LCS(R4098893-1) WG2330346 07/25/24 21:45 VOCMS16 195
LCS(R4099344-1) WG2330260 07/26/24 09:00 VOCMS13 197
LCS(R4100703-1) WG2332276 07/29/24 19:18 VOCMS26 199
LCSD(R4098893-4) WG2330346 07/26/24 08:41 VOCMS16 200
MS(R4099344-3) WG2330260 07/26/24 17:45 VOCMS13 202
MSD(R4099344-4) WG2330260 07/26/24 18:06 VOCMS13 204
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Gl: Glossary of Terms 206
Al: Accreditations & Locations 207
Sc: Sample Chain of Custody 208
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1758896-01 GW Jessica Welch 07/17/24 08:48 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 12:15 07/25/24 12:15 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 12:11 07/26/24 12:11 DYW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/30/24 21:37 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-25 L1758896-02 GW Jessica Welch 07/17/24 09:45 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 12:37 07/25/24 12:37 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 12:32 07/26/24 12:32 DYW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/30/24 21:59 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1758896-03 GW Jessica Welch 07/17/24 10:32 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 13:00 07/25/24 13:00 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 12:53 07/26/24 12:53 DYW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/31/24 00:13 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4 L1758896-04 GW Jessica Welch 07/17/24 12:40 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 13:22 07/25/24 13:22 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 13:13 07/26/24 13:13 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2332276 10 07/29/24 22:55 07/29/24 22:55 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/30/24 22:22 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-8 L1758896-05 GW Jessica Welch 07/17/24 14:05 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 13:45 07/25/24 13:45 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 13:34 07/26/24 13:34 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2332276 25 07/29/24 23:16 07/29/24 23:16 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/30/24 22:44 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1758896-06 GW Jessica Welch 07/17/24 15:35 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 14:08 07/25/24 14:08 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 13:55 07/26/24 13:55 DYW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 08/01/24 13:23 JDJ Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-7 L1758896-07 GW Jessica Welch 07/18/24 08:20 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 14:31 07/25/24 14:31 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 14:16 07/26/24 14:16 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2332276 200 07/29/24 23:36 07/29/24 23:36 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/30/24 23:28 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1758896-08 GW Jessica Welch 07/18/24 09:40 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 14:53 07/25/24 14:53 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 14:37 07/26/24 14:37 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2332276 25 07/29/24 23:56 07/29/24 23:56 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/30/24 23:50 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-10 L1758896-09 GW Jessica Welch 07/18/24 11:00 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 15:15 07/25/24 15:15 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330260 1 07/26/24 14:58 07/26/24 14:58 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2332276 1 07/29/24 20:32 07/29/24 20:32 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 08/01/24 11:58 TJD Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-9 L1758896-10 GW Jessica Welch 07/18/24 12:30 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1664A WG2331265 1 07/27/24 16:22 07/28/24 17:36 DAL Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2329885 1 07/25/24 15:38 07/25/24 15:38 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330346 1 07/26/24 07:35 07/26/24 07:35 DYW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2332252 1 07/30/24 07:59 07/31/24 14:09 DMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
TRIP BLANK L1758896-11 GW Jessica Welch 07/18/24 00:00 07/20/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG2330346 1 07/26/24 00:18 07/26/24 00:18 JHH Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 08/05/24 14:06
Sample Delivery Group (SDG) Narrative
pH outside of method requirement.
Lab Sample ID Project Sample ID Method
L1758896-03 MW-2 3511/8015
L1758896-09 MW-10 8260B, 3511/8015
L1758896-10 MW-9 3511/8015
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Chris Ward
Project Manager
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1664A Wet Chemistry
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-1
Lab Sample ID:L1758896-01 SDG:L1758896
Client Sample ID:MW-1 Collected Date/Time:07/17/24 08:48
Lab File ID:16 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:900 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.29 5.56
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-25
Lab Sample ID:L1758896-02 SDG:L1758896
Client Sample ID:MW-25 Collected Date/Time:07/17/24 09:45
Lab File ID:17 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:950 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)1.68 J 1.22 5.26
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-2
Lab Sample ID:L1758896-03 SDG:L1758896
Client Sample ID:MW-2 Collected Date/Time:07/17/24 10:32
Lab File ID:18 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:950 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U J5 1.22 5.26
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-4
Lab Sample ID:L1758896-04 SDG:L1758896
Client Sample ID:MW-4 Collected Date/Time:07/17/24 12:40
Lab File ID:19 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:850 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.36 5.88
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-8
Lab Sample ID:L1758896-05 SDG:L1758896
Client Sample ID:MW-8 Collected Date/Time:07/17/24 14:05
Lab File ID:20 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:840 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.38 5.95
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-3
Lab Sample ID:L1758896-06 SDG:L1758896
Client Sample ID:MW-3 Collected Date/Time:07/17/24 15:35
Lab File ID:21 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:840 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.38 5.95
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-7
Lab Sample ID:L1758896-07 SDG:L1758896
Client Sample ID:MW-7 Collected Date/Time:07/18/24 08:20
Lab File ID:22 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:950 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.22 5.26
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-5
Lab Sample ID:L1758896-08 SDG:L1758896
Client Sample ID:MW-5 Collected Date/Time:07/18/24 09:40
Lab File ID:23 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:850 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.36 5.88
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-10
Lab Sample ID:L1758896-09 SDG:L1758896
Client Sample ID:MW-10 Collected Date/Time:07/18/24 11:00
Lab File ID:24 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:850 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.36 5.88
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET MW-9
Lab Sample ID:L1758896-10 SDG:L1758896
Client Sample ID:MW-9 Collected Date/Time:07/18/24 12:30
Lab File ID:25 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:850 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.36 5.88
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099402-1
Lab Sample ID:R4099402-1 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:01 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099402-2
Lab Sample ID:R4099402-2 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:04 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)37.9 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099402-3
Lab Sample ID:R4099402-3 SDG:L1758896
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:05 Received Date/Time:_______________
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:1000 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)37.6 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099402-4
Lab Sample ID:R4099402-4 SDG:L1758896
Client Sample ID:MS Collected Date/Time:07/17/24 10:32
Lab File ID:06 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:850 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)47.9 J5 1.16 5.00
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1-IN SAMPLE RESULT SUMMARY SAMPLE NO.:
INORGANIC ANALYSIS DATA SHEET R4099402-5
Lab Sample ID:R4099402-5 SDG:L1758896
Client Sample ID:MSD Collected Date/Time:07/17/24 10:32
Lab File ID:07 Received Date/Time:07/20/24 08:00
Instrument ID:OGBAL1 Preparation Date/Time:07/27/24 16:22
Analytical Batch:WG2331265 Analysis Date/Time:07/28/24 17:36
Dilution Factor:1 Prep Method:1664A
Analytical Method:1664A Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:910 ml
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS Result Qualifier MDL RDL
mg/l mg/l mg/l
Oil & Grease (Hexane Extr)45.1 1.16 5.00
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3-IN BLANKS
SDG:L1758896 Calibration (begin) date/time:_______________
Instrument ID:OGBAL1 Calibration (end) date/time:_______________
Analytical Method:1664A Analytical Run:WG2331265
Sample ID:BLANK Result BLANK
Qual
File ID:01
Analyte mg/l
OIL & GREASE
(HEXANE EXTR)U
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5A-IN MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4099402-4
L1758896-01,02,03,04,05,06,07,08,09,10 R4099402-5
MS Sample / File ID:R4099402-4 / 06 SDG:L1758896
MSD Sample / File ID:R4099402-5 / 07 Analytical Batch:WG2331265
OS Sample / File ID:L1758896-03 / 18 Matrix:GW
Instrument ID:OGBAL1
Analytical Method:1664A
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD Limits
mg/l mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 U 47.9 45.1 120*113 1 78.0 - 114 6.09 18
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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7-IN LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4099402-2
RECOVERY R4099402-3
L1758896-01,02,03,04,05,06,07,08,09,10
LCS Sample / File ID:R4099402-2 / 04 SDG:L1758896
LCSD Sample / File ID:R4099402-3 / 05 Analytical Batch:WG2331265
Instrument ID:OGBAL1 Dilution Factor:1
Analytical Method:1664A Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD
Rec.Rec. Limits RPD RPD Limits
mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 37.9 37.6 94.8 94.0 78.0 - 114 0.795 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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9-IN DETECTION LIMIT SUMMARY
Lab Sample IDs:L1758896-01,02,03,04,05,06,07,08,09,10 Analytical Method:1664A
Matrix:GW Prep Method:1664A
Analyte CAS Wavelength Mass MDL RDL
mg/l mg/l
Oil & Grease (Hexane Extr)1.22 5.26
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12-IN ANALYSIS LOG
SDG:L1758896 Analytical Method:1664A
Instrument ID:OGBAL1 Calibration Start Date:_______________
Analytical Run:WG2331265 Calibration End Date:_______________
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
BLANK R4099402-1 01 07/28/24 17:36 1 WG2331265
LCS R4099402-2 04 07/28/24 17:36 1 WG2331265
LCSD R4099402-3 05 07/28/24 17:36 1 WG2331265
MS R4099402-4 06 07/28/24 17:36 1 WG2331265
MSD R4099402-5 07 07/28/24 17:36 1 WG2331265
MW-2 L1758896-03 18 07/28/24 17:36 1 WG2331265
MW-25 L1758896-02 17 07/28/24 17:36 1 WG2331265
MW-1 L1758896-01 16 07/28/24 17:36 1 WG2331265
MW-4 L1758896-04 19 07/28/24 17:36 1 WG2331265
MW-8 L1758896-05 20 07/28/24 17:36 1 WG2331265
MW-7 L1758896-07 22 07/28/24 17:36 1 WG2331265
MW-3 L1758896-06 21 07/28/24 17:36 1 WG2331265
MW-9 L1758896-10 25 07/28/24 17:36 1 WG2331265
MW-10 L1758896-09 24 07/28/24 17:36 1 WG2331265
MW-5 L1758896-08 23 07/28/24 17:36 1 WG2331265
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3511/8015 Semi-Volatile Organic Compounds (GC)
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2A-OR SURROGATE RECOVERY
Analytical Method:3511/8015 SDG:L1758896
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
MW-1 L1758896-01 SVGC47 0730_017 72.1 0
MW-25 L1758896-02 SVGC47 0730_018 68.9 0
MW-2 L1758896-03 SVGC47 0730_024 71.1 0
MW-4 L1758896-04 SVGC47 0730_019 71.6 0
MW-8 L1758896-05 SVGC47 0730_020 80.0 0
MW-3 L1758896-06 SVGC26 0801_006 55.3 0
MW-7 L1758896-07 SVGC47 0730_022 73.7 0
MW-5 L1758896-08 SVGC47 0730_023 67.9 0
MW-10 L1758896-09 SVGC27 0731_037 68.9 0
MW-9 L1758896-10 SVGC21 0731_018 34.6* 1
MS R4100686-1 SVGC47 0730_025 68.4 0
MSD R4100686-2 SVGC47 0730_026 68.9 0
BLANK R4100691-2 SVGC31 0730_030 67.5 0
LCS R4100691-1 SVGC31 0730_011 50.5* 1
Parm Abbreviation Parameter QC LIMITS
DMC-1 o-Terphenyl 52.0 - 156
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4100686-1
L1758896-01,02,03,04,05,06,07,08,09,10 R4100686-2
MS Sample / File ID:R4100686-1 / 0730_025 SDG:L1758896
MSD Sample / File ID:R4100686-2 / 0730_026 Analytical Batch:WG2332252
OS Sample / File ID:L1758896-03 / 0730_024 Matrix:GW
Instrument ID:SVGC47
Analytical Method:3511/8015
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.43 1.08 1.89 2.13 56.6 73.4 1 50.0 - 150 11.9 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4100691-1
RECOVERY _______________
L1758896-01,02,03,04,05,06,07,08,09,10
LCS Sample / File ID:R4100691-1 / 0730_011 SDG:L1758896
LCSD Sample / File ID:_______________Analytical Batch:WG2332252
Instrument ID:SVGC31 Dilution Factor:1
Analytical Method:3511/8015 Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
TPH (GC/FID) High Fraction 1.50 1.09 72.7 50.0 - 150
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4100691-2
Lab Sample ID:R4100691-2 SDG:L1758896
Lab File ID:0730_030 Preparation Date/Time:07/30/24 07:46
Instrument ID:SVGC31 Analysis Date/Time:07/31/24 04:42
Analytical Batch:WG2332252 Dilution Factor:1
Analytical Method:3511/8015 Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
MW-1 L1758896-01 SVGC47 0730_017 07/30/24 21:37
MW-25 L1758896-02 SVGC47 0730_018 07/30/24 21:59
MW-4 L1758896-04 SVGC47 0730_019 07/30/24 22:22
LCS R4100691-1 SVGC31 0730_011 07/30/24 22:23
MW-8 L1758896-05 SVGC47 0730_020 07/30/24 22:44
MW-7 L1758896-07 SVGC47 0730_022 07/30/24 23:28
MW-5 L1758896-08 SVGC47 0730_023 07/30/24 23:50
MW-2 L1758896-03 SVGC47 0730_024 07/31/24 00:13
MS R4100686-1 SVGC47 0730_025 07/31/24 00:35
MSD R4100686-2 SVGC47 0730_026 07/31/24 00:57
MW-9 L1758896-10 SVGC21 0731_018 07/31/24 14:09
MW-10 L1758896-09 SVGC27 0731_037 08/01/24 11:58
MW-3 L1758896-06 SVGC26 0801_006 08/01/24 13:23

Sample Narrative:
Surrogate failure due to matrix interference during extraction procedure..
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-1
Lab Sample ID:L1758896-01 SDG:L1758896
Client Sample ID:MW-1 Collected Date/Time:07/17/24 08:48
Lab File ID:0730_017 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 21:37
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 0.107 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-25
Lab Sample ID:L1758896-02 SDG:L1758896
Client Sample ID:MW-25 Collected Date/Time:07/17/24 09:45
Lab File ID:0730_018 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 21:59
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 0.0391 J 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-2
Lab Sample ID:L1758896-03 SDG:L1758896
Client Sample ID:MW-2 Collected Date/Time:07/17/24 10:32
Lab File ID:0730_024 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/31/24 00:13
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 1.08 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-4
Lab Sample ID:L1758896-04 SDG:L1758896
Client Sample ID:MW-4 Collected Date/Time:07/17/24 12:40
Lab File ID:0730_019 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 22:22
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 0.133 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-8
Lab Sample ID:L1758896-05 SDG:L1758896
Client Sample ID:MW-8 Collected Date/Time:07/17/24 14:05
Lab File ID:0730_020 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 22:44
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 0.189 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-3
Lab Sample ID:L1758896-06 SDG:L1758896
Client Sample ID:MW-3 Collected Date/Time:07/17/24 15:35
Lab File ID:0801_006 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC26 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:08/01/24 13:23
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6.09 0.134 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-7
Lab Sample ID:L1758896-07 SDG:L1758896
Client Sample ID:MW-7 Collected Date/Time:07/18/24 08:20
Lab File ID:0730_022 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 23:28
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 0.130 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-5
Lab Sample ID:L1758896-08 SDG:L1758896
Client Sample ID:MW-5 Collected Date/Time:07/18/24 09:40
Lab File ID:0730_023 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 23:50
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 0.145 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-10
Lab Sample ID:L1758896-09 SDG:L1758896
Client Sample ID:MW-10 Collected Date/Time:07/18/24 11:00
Lab File ID:0731_037 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC27 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:08/01/24 11:58
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6.12 0.216 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-9
Lab Sample ID:L1758896-10 SDG:L1758896
Client Sample ID:MW-9 Collected Date/Time:07/18/24 12:30
Lab File ID:0731_018 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC21 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/31/24 14:09
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 5.88 0.164 0.0247 0.100

Sample Narrative:
Surrogate failure due to matrix interference during extraction procedure..
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/26/24 07:27
Instrument ID:SVGC21 Calibration (end) date/time:07/26/24 14:36
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200
TPH (GC/FID) HIGH FRACTION 5.88 5.88 5.88 5.88 5.88 5.88 5.88 5.88
O-TERPHENYL 8.10 8.10 8.10 8.10 8.10 8.10 8.11
File ID:0726_005 0726_006 0726_007 0726_008 0726_009 0726_010 0726_011 0726_012
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:06/27/24 12:09
Instrument ID:SVGC26 Calibration (end) date/time:07/02/24 16:23
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200
TPH (GC/FID) HIGH FRACTION 6.09 6.09 6.09 6.09 6.09 6.09 6.09 6.09
O-TERPHENYL 8.33 8.33 8.33 8.33 8.33 8.33 8.33 8.33
File ID:0627_015 0627_016 0627_017 0627_018 0627_019 0627_020 0627_021 0627_022
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200 CS: 2M
TPH (GC/FID) HIGH FRACTION 5.79 5.79 5.79 5.79 5.79 5.79 5.79 5.79 0
O-TERPHENYL 7.71 7.73 7.72 7.71 7.71 7.71 7.71
File ID:0530_004 0530_005 0530_006 0530_007 0530_008 0530_009 0530_010 0530_011 0729_007
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200
TPH (GC/FID) HIGH FRACTION 6 6 6 6 6 6 6 6
O-TERPHENYL 7.93 7.90 7.87 7.86 7.84 7.84 7.84 7.85
File ID:0718_012 0718_013 0718_014 0718_015 0718_016 0718_017 0718_018 0718_019
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/10/24 06:54
Instrument ID:SVGC47 Calibration (end) date/time:07/03/24 14:02
Analytical Method:3511/8015
Analyte CS: 2 CS: 4 CS: 10 CS: 20 CS: 40 CS: 60 CS: 100 CS: 200
TPH (GC/FID) HIGH FRACTION 7.62 7.62 7.62 7.62 7.62 7.62 7.62 7.62
O-TERPHENYL 10.17 10.14 10.13 10.13 10.13
File ID:0703A_00
6
0703A_00
7
0703A_00
8
0703A_00
9
0703A_01
0 0703A_011 0703A_01
2
0703A_01
3
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/26/24 07:27
Instrument ID:SVGC21 Calibration (end) date/time:07/26/24 14:36
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 15170000 15850000 13300000 12520000 12890000 13010000 12490000 12720000
O-TERPHENYL 22540000 17850000 16470000 15720000 16010000 14630000 15260000
File ID:0726_005 0726_006 0726_007 0726_008 0726_009 0726_010 0726_011 0726_012
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/26/24 07:27
Instrument ID:SVGC21 Calibration (end) date/time:07/26/24 14:36
Analytical Method:3511/8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 13490920 9.52 1
O-TERPHENYL 16924960 15.8
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:06/27/24 12:09
Instrument ID:SVGC26 Calibration (end) date/time:07/02/24 16:23
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 28960000 23020000 17610000 16700000 15480000 15440000 15230000 15640000
O-TERPHENYL 14510000 17020000 15300000 16160000 15750000 16090000 15990000 16950000
File ID:0627_015 0627_016 0627_017 0627_018 0627_019 0627_020 0627_021 0627_022
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:06/27/24 12:09
Instrument ID:SVGC26 Calibration (end) date/time:07/02/24 16:23
Analytical Method:3511/8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 18508910 26.71 1
O-TERPHENYL 15970470 5.16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 20960000 17370000 14610000 13340000 13690000 14100000 14530000 14590000
O-TERPHENYL 15420000 9640000 13450000 15220000 13400000 13920000 14380000
File ID:0530_004 0530_005 0530_006 0530_007 0530_008 0530_009 0530_010 0530_011
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Analytical Method:3511/8015
Analyte RRF: 2M RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 14250000 15270560 15.84 0.998
O-TERPHENYL 13631050 14.17
File ID:0729_007
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 31090000 24550000 19730000 18160000 17240000 17470000 16480000 16180000
O-TERPHENYL 30550000 22650000 17850000 18500000 19850000 19300000 20040000 19040000
File ID:0718_012 0718_013 0718_014 0718_015 0718_016 0718_017 0718_018 0718_019
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Analytical Method:3511/8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 20110990 25.78 1
O-TERPHENYL 20973460 19.66
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/10/24 06:54
Instrument ID:SVGC47 Calibration (end) date/time:07/03/24 14:02
Analytical Method:3511/8015
Analyte RRF: 2 RRF: 4 RRF: 10 RRF: 20 RRF: 40 RRF: 60 RRF: 100 RRF: 200
TPH (GC/FID) HIGH FRACTION 125000000 86800000 52800000 47800000 42100000 40600000 40200000 41800000
O-TERPHENYL 31820000 24300000 28200000 34550000 38710000
File ID:0703A_006 0703A_007 0703A_008 0703A_009 0703A_010 0703A_011 0703A_012 0703A_013
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/10/24 06:54
Instrument ID:SVGC47 Calibration (end) date/time:07/03/24 14:02
Analytical Method:3511/8015
Analyte RRF. Avg %RSD COD
TPH (GC/FID) HIGH FRACTION 59630800 51.35 0.998
O-TERPHENYL 31514710 17.68
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/26/24 07:27
Instrument ID:SVGC21 Calibration (end) date/time:07/26/24 14:36
Lab File ID:0726_014 Analysis date/time:07/26/24 11:53
Analytical Method:3511/8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 13490920 11325510 16.10 60 53.22 88.70 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/26/24 07:27
Instrument ID:SVGC21 Calibration (end) date/time:07/26/24 14:36
Lab File ID:0731_003 Analysis date/time:07/31/24 08:42
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 13490920 12933760 4.13 60 60.86 101 85 - 115
O-TERPHENYL 16924960 13219310 21.90 0.40 0.3124 78.10 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/26/24 07:27
Instrument ID:SVGC21 Calibration (end) date/time:07/26/24 14:36
Lab File ID:0731_038 Analysis date/time:07/31/24 20:55
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 13490920 14210400 5.33 60 66.93 112 85 - 115
O-TERPHENYL 16924960 15032490 11.20 0.40 0.3553 88.80 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:06/27/24 12:09
Instrument ID:SVGC26 Calibration (end) date/time:07/02/24 16:23
Lab File ID:0801_003 Analysis date/time:08/01/24 12:22
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 18508910 14185460 23.40 60 54.10 90.20 85 - 115
O-TERPHENYL 15970470 16638050 4.18 0.40 0.4167 104 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:06/27/24 12:09
Instrument ID:SVGC26 Calibration (end) date/time:07/02/24 16:23
Lab File ID:0801_028 Analysis date/time:08/01/24 20:53
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 18508910 14267040 22.90 60 54.43 90.70 85 - 115
O-TERPHENYL 15970470 16346240 2.35 0.40 0.4094 102 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 66 of 210
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Lab File ID:0530_013-1 Analysis date/time:05/30/24 05:28
Analytical Method:3511/8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 15270560 13015600 14.80 60 54.13 90.20 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 67 of 210
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Lab File ID:0730_003-1 Analysis date/time:07/31/24 22:26
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 15270560 13827040 9.45 60 57.59 96 85 - 115
O-TERPHENYL 13631050 17967450 31.80 0.40 0.5273 132 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 68 of 210
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/30/24 02:22
Instrument ID:SVGC27 Calibration (end) date/time:07/29/24 11:16
Lab File ID:0731_040-1 Analysis date/time:08/01/24 13:00
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 15270560 14110290 7.60 60 58.78 98 85 - 115
O-TERPHENYL 13631050 17160130 25.90 0.40 0.5036 126 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Lab File ID:0718_021 Analysis date/time:07/18/24 13:00
Analytical Method:3511/8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 20110990 15522330 22.80 60 55.34 92.20 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 70 of 210
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Lab File ID:0730_004 Analysis date/time:07/30/24 20:02
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 20110990 19159300 4.73 60 68.78 115 85 - 115
O-TERPHENYL 20973460 20769900 0.9710 0.40 0.3961 99 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Lab File ID:0730_016 Analysis date/time:07/31/24 00:03
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 20110990 19184720 4.61 60 68.87 115 85 - 115
O-TERPHENYL 20973460 19478630 7.13 0.40 0.3715 92.90 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 72 of 210
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 09:57
Instrument ID:SVGC31 Calibration (end) date/time:07/18/24 15:43
Lab File ID:0730_043 Analysis date/time:07/31/24 09:01
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 20110990 20431170 1.59 60 73.47 122 85 - 115
O-TERPHENYL 20973460 24869610 18.60 0.40 0.4743 119 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/10/24 06:54
Instrument ID:SVGC47 Calibration (end) date/time:07/03/24 14:02
Lab File ID:0703A_015 Analysis date/time:07/03/24 14:47
Analytical Method:3511/8015 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 59630800 47345560 20.60 60 67.65 113 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 74 of 210
7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/10/24 06:54
Instrument ID:SVGC47 Calibration (end) date/time:07/03/24 14:02
Lab File ID:0730_015 Analysis date/time:07/30/24 20:53
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 59630800 40829520 31.50 60 57.75 96.30 85 - 115
O-TERPHENYL 31514710 41599200 32 0.40 0.5280 132 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:05/10/24 06:54
Instrument ID:SVGC47 Calibration (end) date/time:07/03/24 14:02
Lab File ID:0730_040 Analysis date/time:07/31/24 06:08
Analytical Method:3511/8015 Sample ID:CCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) HIGH FRACTION 59630800 42144040 29.30 60 59.75 99.60 85 - 115
O-TERPHENYL 31514710 37854620 20.10 0.40 0.4805 120 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:3511/8015
Instrument ID:SVGC21 Calibration Start Date:07/26/24 07:27
Calibration End Date:07/26/24 14:36
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2 0726_005 07/26/24 07:27
CAL 4 0726_006 07/26/24 09:10
CAL 10 0726_007 07/26/24 09:30
CAL 20 0726_008 07/26/24 09:51
CAL 40 0726_009 07/26/24 10:11
CAL 60 0726_010 07/26/24 10:31
CAL 100 0726_011 07/26/24 10:52
CAL 200 0726_012 07/26/24 11:12
SSCV SVGC210726240726_014742106 0726_014 07/26/24 11:53
CAL 2M 0726_016 07/26/24 12:33
CAL 4M 0726_017 07/26/24 12:54
CAL 10M 0726_018 07/26/24 13:14
CAL 20M 0726_019 07/26/24 13:35
CAL 40M 0726_020 07/26/24 13:55
CAL 50M 0726_021 07/26/24 14:15
CAL 100M 0726_022 07/26/24 14:36
CCV SVGC210731240731_003742106 0731_003 07/31/24 08:42
CCV SVGC210731240731_004742106 0731_004 07/31/24 09:03
MW-9 L1758896-10 0731_018 07/31/24 14:09 1 WG2332252
CCV SVGC210731240731_038742106 0731_038 07/31/24 20:55
CCV SVGC210731240731_039742106 0731_039 07/31/24 21:16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:3511/8015
Instrument ID:SVGC26 Calibration Start Date:06/27/24 12:09
Calibration End Date:07/02/24 16:23
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2 0627_015 06/27/24 12:09
CAL 4 0627_016 06/27/24 12:29
CAL 10 0627_017 06/27/24 12:49
CAL 20 0627_018 06/27/24 13:09
CAL 40 0627_019 06/27/24 13:29
CAL 60 0627_020 06/27/24 13:49
CAL 100 0627_021 06/27/24 14:09
CAL 200 0627_022 06/27/24 14:30
CAL 2M 0702_005 07/02/24 14:22
CAL 4M 0702_006 07/02/24 14:42
CAL 10M 0702_007 07/02/24 15:03
CAL 20M 0702_008 07/02/24 15:23
CAL 40M 0702_009 07/02/24 15:43
CAL 50M 0702_010 07/02/24 16:03
CAL 100M 0702_011 07/02/24 16:23
CCV SVGC260801240801_003735901 0801_003 08/01/24 12:22
CCV SVGC260801240801_004735901 0801_004 08/01/24 12:42
MW-3 L1758896-06 0801_006 08/01/24 13:23 1 WG2332252
CCV SVGC260801240801_028735901 0801_028 08/01/24 20:53
CCV SVGC260801240801_029735901 0801_029 08/01/24 21:13
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 78 of 210
8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:3511/8015
Instrument ID:SVGC27 Calibration Start Date:05/30/24 02:22
Calibration End Date:07/29/24 11:16
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2 0530_004 05/30/24 02:22
CAL 4 0530_005 05/30/24 02:43
CAL 10 0530_006 05/30/24 03:03
CAL 20 0530_007 05/30/24 03:24
CAL 40 0530_008 05/30/24 03:45
CAL 60 0530_009 05/30/24 04:06
CAL 100 0530_010 05/30/24 04:26
CAL 200 0530_011 05/30/24 04:47
SSCV SVGC270530240530_013-1742251 0530_013-1 05/30/24 05:28
CAL 2M 0729_007 07/29/24 09:13
CAL 4M 0729_008 07/29/24 09:33
CAL 10M 0729_009 07/29/24 09:54
CAL 20M 0729_010 07/29/24 10:14
CAL 40M 0729_011 07/29/24 10:35
CAL 50M 0729_012 07/29/24 10:55
CAL 100M 0729_013 07/29/24 11:16
CCV SVGC270731240730_003-1742251 0730_003-1 07/31/24 22:26
CCV SVGC270731240731_007-1742251 0731_007-1 08/01/24 01:40
BLANK R4101659-1 0731_012 08/01/24 03:23 1 WG2332724
BLANK R4101660-1 0731_012A 08/01/24 03:23 1 WG2332731
LCS R4101659-2 0731_013 08/01/24 03:43 1 WG2332724
LCS R4101660-2 0731_013A 08/01/24 03:43 1 WG2332731
LCSD R4101659-3 0731_014 08/01/24 04:04 1 WG2332724
LCSD R4101660-3 0731_014A 08/01/24 04:04 1 WG2332731
BLANK R4101663-1 0731_015 08/01/24 04:24 1 WG2334698
LCS R4101663-2 0731_016 08/01/24 04:45 1 WG2334698
LCSD R4101663-3 0731_017 08/01/24 05:05 1 WG2334698
L1760484-01 L1760484-01 0731_023 08/01/24 07:08 1 WG2332724
L1760484-02 L1760484-02 0731_024 08/01/24 07:28 1 WG2332724
L1760484-03 L1760484-03 0731_025 08/01/24 07:48 1 WG2332724
L1760484-04 L1760484-04 0731_026 08/01/24 08:09 1 WG2332724
L1760484-05 L1760484-05 0731_027 08/01/24 08:29 1 WG2332724
L1760484-06 L1760484-06 0731_028 08/01/24 08:50 1 WG2332724
L1760484-07 L1760484-07 0731_029 08/01/24 09:11 1 WG2332724
LCS R4101662-1 0731_030 08/01/24 09:32 1 WG2334069
LCSD R4101662-2 0731_031 08/01/24 09:53 1 WG2334069
BLANK R4101662-3 0731_032 08/01/24 10:13 1 WG2334069
MW-10 L1758896-09 0731_037 08/01/24 11:58 1 WG2332252
CCV SVGC270731240731_039-1742251 0731_039-1 08/01/24 12:40
CCV SVGC270731240731_040-1742251 0731_040-1 08/01/24 13:00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:3511/8015
Instrument ID:SVGC31 Calibration Start Date:07/18/24 09:57
Calibration End Date:07/18/24 15:43
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2 0718_012 07/18/24 09:57
CAL 4 0718_013 07/18/24 10:18
CAL 10 0718_014 07/18/24 10:38
CAL 20 0718_015 07/18/24 10:58
CAL 40 0718_016 07/18/24 11:19
CAL 60 0718_017 07/18/24 11:39
CAL 100 0718_018 07/18/24 11:59
CAL 200 0718_019 07/18/24 12:20
SSCV SVGC310718240718_021740543 0718_021 07/18/24 13:00
CAL 2M 0718_023 07/18/24 13:41
CAL 4M 0718_024 07/18/24 14:01
CAL 10M 0718_025 07/18/24 14:21
CAL 20M 0718_026 07/18/24 14:42
CAL 40M 0718_027 07/18/24 15:02
CAL 50M 0718_028 07/18/24 15:22
CAL 100M 0718_029 07/18/24 15:43
CCV SVGC310730240730_004740543 0730_004 07/30/24 20:02
CCV SVGC310730240730_005740543 0730_005 07/30/24 20:22
LCS R4100690-1 0730_008 07/30/24 21:23 1 WG2331725
LCSD R4100690-2 0730_009 07/30/24 21:43 1 WG2331725
LCS R4100691-1 0730_011 07/30/24 22:23 1 WG2332252
CCV SVGC310730240730_016740543 0730_016 07/31/24 00:03
CCV SVGC310730240730_017740543 0730_017 07/31/24 00:23
BLANK R4100690-3 0730_029 07/31/24 04:22 1 WG2331725
BLANK R4100691-2 0730_030 07/31/24 04:42 1 WG2332252
CCV SVGC310730240730_043740543 0730_043 07/31/24 09:01
CCV SVGC310730240730_044740543 0730_044 07/31/24 09:21
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 80 of 210
8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:3511/8015
Instrument ID:SVGC47 Calibration Start Date:05/10/24 06:54
Calibration End Date:07/03/24 14:02
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 2M 0509_032 05/10/24 06:54
CAL 4M 0509_033 05/10/24 07:16
CAL 10M 0509_034 05/10/24 07:38
CAL 20M 0509_035 05/10/24 08:00
CAL 40M 0509_036 05/10/24 08:23
CAL 50M 0509_037 05/10/24 08:45
CAL 100M 0509_038 05/10/24 09:07
CAL 2 0703A_006 07/03/24 11:27
CAL 4 0703A_007 07/03/24 11:49
CAL 10 0703A_008 07/03/24 12:11
CAL 20 0703A_009 07/03/24 12:34
CAL 40 0703A_010 07/03/24 12:56
CAL 60 0703A_011 07/03/24 13:18
CAL 100 0703A_012 07/03/24 13:40
CAL 200 0703A_013 07/03/24 14:02
SSCV SVGC47070324A0703A_015736149 0703A_015 07/03/24 14:47
CCV SVGC470730240730_015736149 0730_015 07/30/24 20:53
MW-1 L1758896-01 0730_017 07/30/24 21:37 1 WG2332252
MW-25 L1758896-02 0730_018 07/30/24 21:59 1 WG2332252
MW-4 L1758896-04 0730_019 07/30/24 22:22 1 WG2332252
MW-8 L1758896-05 0730_020 07/30/24 22:44 1 WG2332252
MW-7 L1758896-07 0730_022 07/30/24 23:28 1 WG2332252
MW-5 L1758896-08 0730_023 07/30/24 23:50 1 WG2332252
MW-2 L1758896-03 0730_024 07/31/24 00:13 1 WG2332252
MS R4100686-1 0730_025 07/31/24 00:35 1 WG2332252
MSD R4100686-2 0730_026 07/31/24 00:57 1 WG2332252
L1758630-08 L1758630-08 0730_035 07/31/24 04:17 1 WG2331725
L1758630-05 L1758630-05 0730_036 07/31/24 04:39 1 WG2331725
CCV SVGC470730240730_040736149 0730_040 07/31/24 06:08
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1758896-01,02,03,04,05,06,07,08,09,10 Analytical Method:3511/8015
Matrix:GW Prep Method:3511/8015
Analyte CAS MDL RDL
mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 0.0247 0.10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100691-2
Lab Sample ID:R4100691-2 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0730_030 Received Date/Time:_______________
Instrument ID:SVGC31 Preparation Date/Time:07/30/24 07:46
Analytical Batch:WG2332252 Analysis Date/Time:07/31/24 04:42
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6 U 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100691-1
Lab Sample ID:R4100691-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0730_011 Received Date/Time:_______________
Instrument ID:SVGC31 Preparation Date/Time:07/30/24 07:46
Analytical Batch:WG2332252 Analysis Date/Time:07/30/24 22:23
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:40 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 6 1.09 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100686-1
Lab Sample ID:R4100686-1 SDG:L1758896
Client Sample ID:MS Collected Date/Time:07/17/24 10:32
Lab File ID:0730_025 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/31/24 00:35
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 1.89 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100686-2
Lab Sample ID:R4100686-2 SDG:L1758896
Client Sample ID:MSD Collected Date/Time:07/17/24 10:32
Lab File ID:0730_026 Received Date/Time:07/20/24 08:00
Instrument ID:SVGC47 Preparation Date/Time:07/30/24 07:59
Analytical Batch:WG2332252 Analysis Date/Time:07/31/24 00:57
Dilution Factor:1 Prep Method:3511/8015
Analytical Method:3511/8015 Sample Vol Used:_______________
Matrix:GW Initial Wt/Vol:42 mL
Total Solids (%):_______________Final Wt/Vol:2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) High Fraction 68334-30-5 7.62 2.13 0.0247 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8015D/GRO Volatile Organic Compounds (GC)
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2A-OR SURROGATE RECOVERY
Analytical Method:8015D/GRO SDG:L1758896
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
MW-1 L1758896-01 VOCGC6 0725_07 97.5 0
MW-25 L1758896-02 VOCGC6 0725_08 98.1 0
MW-2 L1758896-03 VOCGC6 0725_09 96.4 0
MW-4 L1758896-04 VOCGC6 0725_10 96.9 0
MW-8 L1758896-05 VOCGC6 0725_11 96.1 0
MW-3 L1758896-06 VOCGC6 0725_12 96.9 0
MW-7 L1758896-07 VOCGC6 0725_13 97.1 0
MW-5 L1758896-08 VOCGC6 0725_14 96.7 0
MW-10 L1758896-09 VOCGC6 0725_15 97.5 0
MW-9 L1758896-10 VOCGC6 0725_16 96.9 0
MS R4099262-3 VOCGC6 0725_26 100 0
MSD R4099262-4 VOCGC6 0725_27 101 0
BLANK R4099262-2 VOCGC6 0725_05 97.5 0
LCS R4099262-1 VOCGC6 0725_03U 104 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 a,a,a-Trifluorotoluene(FID)78.0 - 120
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4099262-3
L1758896-01,02,03,04,05,06,07,08,09,10 R4099262-4
MS Sample / File ID:R4099262-3 / 0725_26 SDG:L1758896
MSD Sample / File ID:R4099262-4 / 0725_27 Analytical Batch:WG2329885
OS Sample / File ID:L1758896-03 / 0725_09 Matrix:GW
Instrument ID:VOCGC6
Analytical Method:8015D/GRO
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.00 0.139 4.55 6.53 88.2 128 1 10.0 - 160 35.7*22
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4099262-1
RECOVERY _______________
L1758896-01,02,03,04,05,06,07,08,09,10
LCS Sample / File ID:R4099262-1 / 0725_03U SDG:L1758896
LCSD Sample / File ID:_______________Analytical Batch:WG2329885
Instrument ID:VOCGC6 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
TPH (GC/FID) Low Fraction 5.00 5.61 112 72.0 - 127
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4099262-2
Lab Sample ID:R4099262-2 SDG:L1758896
Lab File ID:0725_05 Preparation Date/Time:07/25/24 10:52
Instrument ID:VOCGC6 Analysis Date/Time:07/25/24 10:52
Analytical Batch:WG2329885 Dilution Factor:1
Analytical Method:8015D/GRO Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4099262-1 VOCGC6 0725_03U 07/25/24 10:08
MW-1 L1758896-01 VOCGC6 0725_07 07/25/24 12:15
MW-25 L1758896-02 VOCGC6 0725_08 07/25/24 12:37
MW-2 L1758896-03 VOCGC6 0725_09 07/25/24 13:00
MW-4 L1758896-04 VOCGC6 0725_10 07/25/24 13:22
MW-8 L1758896-05 VOCGC6 0725_11 07/25/24 13:45
MW-3 L1758896-06 VOCGC6 0725_12 07/25/24 14:08
MW-7 L1758896-07 VOCGC6 0725_13 07/25/24 14:31
MW-5 L1758896-08 VOCGC6 0725_14 07/25/24 14:53
MW-10 L1758896-09 VOCGC6 0725_15 07/25/24 15:15
MW-9 L1758896-10 VOCGC6 0725_16 07/25/24 15:38
MS R4099262-3 VOCGC6 0725_26 07/25/24 19:52
MSD R4099262-4 VOCGC6 0725_27 07/25/24 20:15
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1758896 Analytical Method:8015D/GRO
Instrument ID:VOCGC6 Calibration Start Date:07/18/24 16:32
Std File: 0725_03 Calibration End Date:07/18/24 23:41
Std Analysis Date:07/25/24 10:08
Sample ID File ID FB (FID)FB (PID)
Response RT Response RT
STANDARD 46064580 7.61 133634400 7.61
UPPER LIMIT 92129160 267268800
LOWER LIMIT 23032290 66817200
LCS R4099262-1
WG2329885 1x 0725_03U 46064580 7.61 133634400 7.61
BLANK R4099262-2
WG2329885 1x 0725_05 42239810 7.61 135740400 7.61
L1758896-01 WG2329885
1x 0725_07 42863090 7.61 137984000 7.61
L1758896-02 WG2329885
1x 0725_08 40158020 7.61 129252200 7.61
L1758896-03 WG2329885
1x 0725_09 43247180 7.61 138536600 7.61
OS L1758896-03
WG2329885 1x 0725_09 43247180 7.61 138536600 7.61
L1758896-04 WG2329885
1x 0725_10 42547700 7.61 136412800 7.61
L1758896-05 WG2329885
1x 0725_11 43846260 7.61 140391100 7.61
L1758896-06 WG2329885
1x 0725_12 42761790 7.61 137059400 7.61
L1758896-07 WG2329885
1x 0725_13 44400280 7.61 141010700 7.61
L1758896-08 WG2329885
1x 0725_14 43244660 7.61 138766600 7.61
L1758896-09 WG2329885
1x 0725_15 40759040 7.61 130961700 7.61
L1758896-10 WG2329885
1x 0725_16 41314840 7.61 132642400 7.61
MS R4099262-3
WG2329885 1x 0725_26 45222330 7.61 134192700 7.61
MSD R4099262-4
WG2329885 1x 0725_27 47499700 7.61 138730800 7.61
FB (FID) - FLUOROBENZENE (FID) FB (PID) - FLUOROBENZENE (PID)
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-1
Lab Sample ID:L1758896-01 SDG:L1758896
Client Sample ID:MW-1 Collected Date/Time:07/17/24 08:48
Lab File ID:0725_07 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 12:15
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 12:15
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.0502 B J 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-25
Lab Sample ID:L1758896-02 SDG:L1758896
Client Sample ID:MW-25 Collected Date/Time:07/17/24 09:45
Lab File ID:0725_08 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 12:37
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 12:37
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.0556 B J 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-2
Lab Sample ID:L1758896-03 SDG:L1758896
Client Sample ID:MW-2 Collected Date/Time:07/17/24 10:32
Lab File ID:0725_09 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 13:00
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 13:00
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.139 B J3 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-4
Lab Sample ID:L1758896-04 SDG:L1758896
Client Sample ID:MW-4 Collected Date/Time:07/17/24 12:40
Lab File ID:0725_10 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 13:22
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 13:22
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.254 B 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-8
Lab Sample ID:L1758896-05 SDG:L1758896
Client Sample ID:MW-8 Collected Date/Time:07/17/24 14:05
Lab File ID:0725_11 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 13:45
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 13:45
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.583 B 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-3
Lab Sample ID:L1758896-06 SDG:L1758896
Client Sample ID:MW-3 Collected Date/Time:07/17/24 15:35
Lab File ID:0725_12 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 14:08
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 14:08
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.0890 B J 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-7
Lab Sample ID:L1758896-07 SDG:L1758896
Client Sample ID:MW-7 Collected Date/Time:07/18/24 08:20
Lab File ID:0725_13 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 14:31
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 14:31
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 3.28 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-5
Lab Sample ID:L1758896-08 SDG:L1758896
Client Sample ID:MW-5 Collected Date/Time:07/18/24 09:40
Lab File ID:0725_14 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 14:53
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 14:53
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.570 B 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-10
Lab Sample ID:L1758896-09 SDG:L1758896
Client Sample ID:MW-10 Collected Date/Time:07/18/24 11:00
Lab File ID:0725_15 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 15:15
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 15:15
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.0522 B J 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-9
Lab Sample ID:L1758896-10 SDG:L1758896
Client Sample ID:MW-9 Collected Date/Time:07/18/24 12:30
Lab File ID:0725_16 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 15:38
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 15:38
Dilution Factor:1 Prep Method:8015D/GRO
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.0508 B J 0.0314 0.100
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6B-OR RETENTION TIME
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 16:32
Instrument ID:VOCGC6 Calibration (end) date/time:07/18/24 23:41
Analytical Method:8015D/GRO
Analyte CS: .1G CS: .5G CS: 1G CS: 2.5G CS: 5G CS: 10G CS: .05G
TPH (GC/FID) LOW FRACTION 7 7 7 7 7 7
A,A,A-TRIFLUOROTOLUENE(FID)8.08 8.08 8.08 8.08 8.08 8.08 8.08
File ID:0718_19 0718_20 0718_21 0718_22 0718_23 0718_24 0718_18
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 16:32
Instrument ID:VOCGC6 Calibration (end) date/time:07/18/24 23:41
Analytical Method:8015D/GRO
Analyte RRF: .1G RRF: .5G RRF: 1G RRF: 2.5G RRF: 5G RRF: 10G RRF: .05G
TPH (GC/FID) LOW FRACTION 928 1085 997 950 971 1228
A,A,A-TRIFLUOROTOLUENE(FID)0.9060 0.8970 0.9350 0.9230 0.9660 1.0740 0.9170
File ID:0718_19 0718_20 0718_21 0718_22 0718_23 0718_24 0718_18
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6C-OR CALIBRATION FACTOR
INITIAL CALIBRATION OF
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 16:32
Instrument ID:VOCGC6 Calibration (end) date/time:07/18/24 23:41
Analytical Method:8015D/GRO
Analyte RRF. Avg %RSD COD
TPH (GC/FID) LOW FRACTION 1026.536 10.97
A,A,A-TRIFLUOROTOLUENE(FID)0.945325 6.45
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 16:32
Instrument ID:VOCGC6 Calibration (end) date/time:07/18/24 23:41
Lab File ID:0718_27 Analysis date/time:07/19/24 01:12
Analytical Method:8015D/GRO Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 1026.5360 1.126877 99.90 5 5.489 110 80 - 120
A,A,A-TRIFLUOROTOLUENE(FID)0.945325 0.91370280 3.35 0.20 0.1933 96.70 80 - 120
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7C-OR CONTINUING CALIBRATION VERIFICATION
SINGLE COMPONENT ANALYTES
SDG:L1758896 Calibration (begin) date/time:07/18/24 16:32
Instrument ID:VOCGC6 Calibration (end) date/time:07/18/24 23:41
Lab File ID:0725_03 Analysis date/time:07/25/24 10:08
Analytical Method:8015D/GRO Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
TPH (GC/FID) LOW FRACTION 1026.5360 1.151810 99.90 5 5.610 112 85 - 115
A,A,A-TRIFLUOROTOLUENE(FID)0.945325 0.98279980 3.96 0.20 0.2079 104 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:8015D/GRO
Instrument ID:VOCGC6 Calibration Start Date:07/18/24 16:32
Calibration End Date:07/18/24 23:41
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
CAL 0.5 0718_05 07/18/24 16:32
CAL 1 0718_06 07/18/24 16:55
CAL 5 0718_07 07/18/24 17:17
CAL 25 0718_08 07/18/24 17:40
CAL 50 0718_09 07/18/24 18:02
CAL 150 0718_10 07/18/24 18:25
CAL 250 0718_11 07/18/24 18:48
SSCV VOCGC60718240718_14740278 0718_14 07/18/24 19:56
CAL .05G 0718_18 07/18/24 21:26
CAL .1G 0718_19 07/18/24 21:48
CAL .5G 0718_20 07/18/24 22:10
CAL 1G 0718_21 07/18/24 22:33
CAL 2.5G 0718_22 07/18/24 22:56
CAL 5G 0718_23 07/18/24 23:18
CAL 10G 0718_24 07/18/24 23:41
SSCV VOCGC60718240718_27740278 0718_27 07/19/24 01:12
ICV VOCGC60725240725_03740278 0725_03 07/25/24 10:08
LCS R4099262-1 0725_03U 07/25/24 10:08 1 WG2329885
BLANK R4099262-2 0725_05 07/25/24 10:52 1 WG2329885
L1758639-06 L1758639-06 0725_06 07/25/24 11:52 1 WG2329885
MW-1 L1758896-01 0725_07 07/25/24 12:15 1 WG2329885
MW-25 L1758896-02 0725_08 07/25/24 12:37 1 WG2329885
MW-2 L1758896-03 0725_09 07/25/24 13:00 1 WG2329885
MW-4 L1758896-04 0725_10 07/25/24 13:22 1 WG2329885
MW-8 L1758896-05 0725_11 07/25/24 13:45 1 WG2329885
MW-3 L1758896-06 0725_12 07/25/24 14:08 1 WG2329885
MW-7 L1758896-07 0725_13 07/25/24 14:31 1 WG2329885
MW-5 L1758896-08 0725_14 07/25/24 14:53 1 WG2329885
MW-10 L1758896-09 0725_15 07/25/24 15:15 1 WG2329885
MW-9 L1758896-10 0725_16 07/25/24 15:38 1 WG2329885
L1758910-11 L1758910-11 0725_17 07/25/24 16:00 1 WG2329885
L1758910-12 L1758910-12 0725_18 07/25/24 16:50 1 WG2329885
L1758639-01 L1758639-01 0725_19 07/25/24 17:12 500 WG2329885
L1758639-03 L1758639-03 0725_21 07/25/24 17:58 10 WG2329885
L1758639-05 L1758639-05 0725_22 07/25/24 18:21 10 WG2329885
L1758739-01 L1758739-01 0725_25 07/25/24 19:28 10 WG2329885
MS R4099262-3 0725_26 07/25/24 19:52 1 WG2329885
MSD R4099262-4 0725_27 07/25/24 20:15 1 WG2329885
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1758896-01,02,03,04,05,06,07,08,09,10 Analytical Method:8015D/GRO
Matrix:GW Prep Method:8015D/GRO
Analyte CAS MDL RDL
mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 0.0314 0.10
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099262-2
Lab Sample ID:R4099262-2 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_05 Received Date/Time:_______________
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 10:52
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 10:52
Dilution Factor:1 Prep Method:8015/8021
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 0.0744 J 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099262-1
Lab Sample ID:R4099262-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_03U Received Date/Time:_______________
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 10:08
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 10:08
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 5.61 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099262-3
Lab Sample ID:R4099262-3 SDG:L1758896
Client Sample ID:MS Collected Date/Time:07/17/24 10:32
Lab File ID:0725_26 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 19:52
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 19:52
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 4.55 0.0314 0.100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099262-4
Lab Sample ID:R4099262-4 SDG:L1758896
Client Sample ID:MSD Collected Date/Time:07/17/24 10:32
Lab File ID:0725_27 Received Date/Time:07/20/24 08:00
Instrument ID:VOCGC6 Preparation Date/Time:07/25/24 20:15
Analytical Batch:WG2329885 Analysis Date/Time:07/25/24 20:15
Dilution Factor:1 Prep Method:8015
Analytical Method:8015D/GRO Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
TPH (GC/FID) Low Fraction 8006-61-9 7 6.53 J3 0.0314 0.100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8260B Volatile Organic Compounds (GC/MS)
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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2A-OR SURROGATE RECOVERY
Analytical Method:8260B SDG:L1758896
Matrix:GW
Sample ID Lab Sample ID Instrument File ID DMC-1 DMC-2 DMC-3 TOT Out
% Rec.% Rec.% Rec.
MW-1 L1758896-01 VOCMS13 0726_10 96.7 95.4 117 0
MW-25 L1758896-02 VOCMS13 0726_11 95.0 95.7 119 0
MW-2 L1758896-03 VOCMS13 0726_12 95.2 93.8 115 0
MW-4 L1758896-04 VOCMS13 0726_13 95.4 92.2 119 0
MW-4 L1758896-04 VOCMS26 0729A_11 99.1 105 98.9 0
MW-8 L1758896-05 VOCMS13 0726_14 96.9 94.4 116 0
MW-8 L1758896-05 VOCMS26 0729A_12 102 105 96.8 0
MW-3 L1758896-06 VOCMS13 0726_15 95.8 95.4 115 0
MW-7 L1758896-07 VOCMS13 0726_16 96.3 93.9 114 0
MW-7 L1758896-07 VOCMS26 0729A_13 99.9 103 98.3 0
MW-5 L1758896-08 VOCMS13 0726_17 95.6 92.3 117 0
MW-5 L1758896-08 VOCMS26 0729A_14 99.2 103 98.3 0
MW-10 L1758896-09 VOCMS13 0726_18 92.3 91.8 120 0
MW-10 L1758896-09 VOCMS26 0729A_04 100 105 97.1 0
MW-9 L1758896-10 VOCMS16 0725_69 101 95.4 99.9 0
TRIP BLANK L1758896-11 VOCMS16 0725_49 103 90.9 99.9 0
MS R4099344-3 VOCMS13 0726_26 90.8 97.9 114 0
MSD R4099344-4 VOCMS13 0726_27 90.1 96.9 113 0
BLANK R4099344-2 VOCMS13 0726_05 97.1 95.2 118 0
BLANK R4098893-3 VOCMS16 0725_48 101 92.6 103 0
BLANK R4100703-2 VOCMS26 0729A_03A 101 105 98.7 0
LCS R4099344-1 VOCMS13 0726_03LCS 97.4 100 112 0
LCS R4098893-1 VOCMS16 0725_45LCS 96.3 93.4 95.9 0
LCS R4100703-1 VOCMS26 0729A_01LCSA 99.4 108 97.1 0
LCSD R4098893-4 VOCMS16 0725_72 98.6 91.8 99.1 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 Toluene-d8 80.0 - 120
DMC-2 4-Bromofluorobenzene 77.0 - 126
DMC-3 1,2-Dichloroethane-d4 70.0 - 130
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4099344-3
L1758896-01,02,03,04,05,06,07,08,09 R4099344-4
MS Sample / File ID:R4099344-3 / 0726_26 SDG:L1758896
MSD Sample / File ID:R4099344-4 / 0726_27 Analytical Batch:WG2330260
OS Sample / File ID:L1758896-03 / 0726_12 Matrix:GW
Instrument ID:VOCMS13
Analytical Method:8260B
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l mg/l %%%%%
Acetone 0.0250 U 0.0217 0.0217 86.8 86.8 1 10.0 - 160 0.000 35
Acrolein 0.0250 U 0.0593 0.0606 237*242*1 10.0 - 160 2.17 39
Acrylonitrile 0.0250 U 0.0322 0.0320 129 128 1 21.0 - 160 0.623 32
Benzene 0.00500 0.00023
2 0.00750 0.00745 145 144 1 17.0 - 158 0.669 27
Bromobenzene 0.00500 U 0.00650 0.00678 130 136 1 30.0 - 149 4.22 28
Bromodichloromethane 0.00500 U 0.00701 0.00721 140 144 1 31.0 - 150 2.81 27
Bromoform 0.00500 U 0.00476 0.00452 95.2 90.4 1 29.0 - 150 5.17 29
Bromomethane 0.00500 U 0.00235 0.00282 47.0 56.4 1 10.0 - 160 18.2 38
n-Butylbenzene 0.00500 U 0.00599 0.00595 120 119 1 31.0 - 150 0.670 30
sec-Butylbenzene 0.00500 U 0.00635 0.00668 127 134 1 33.0 - 155 5.07 29
tert-Butylbenzene 0.00500 U 0.00595 0.00620 119 124 1 34.0 - 153 4.12 28
Carbon tetrachloride 0.00500 U 0.00834 0.00877 167*175*1 23.0 - 159 5.03 28
Chlorobenzene 0.00500 U 0.00579 0.00587 116 117 1 33.0 - 152 1.37 27
Chlorodibromomethane 0.00500 U 0.00562 0.00563 112 113 1 37.0 - 149 0.178 27
Chloroethane 0.00500 U 0.00877 0.00887 175*177*1 10.0 - 160 1.13 30
Chloroform 0.00500 U 0.00720 0.00753 144 151 1 29.0 - 154 4.48 28
Chloromethane 0.00500 U 0.00576 0.00598 115 120 1 10.0 - 160 3.75 29
2-Chlorotoluene 0.00500 U 0.00644 0.00666 129 133 1 32.0 - 153 3.36 28
4-Chlorotoluene 0.00500 U 0.00630 0.00653 126 131 1 32.0 - 150 3.59 28
1,2-Dibromo-3-Chloropropane 0.00500 U 0.00409 0.00417 81.8 83.4 1 22.0 - 151 1.94 34
1,2-Dibromoethane 0.00500 U 0.00535 0.00541 107 108 1 34.0 - 147 1.12 27
Dibromomethane 0.00500 U 0.00684 0.00691 137 138 1 30.0 - 151 1.02 27
1,2-Dichlorobenzene 0.00500 U 0.00556 0.00596 111 119 1 34.0 - 149 6.94 28
1,3-Dichlorobenzene 0.00500 U 0.00592 0.00619 118 124 1 36.0 - 146 4.46 27
1,4-Dichlorobenzene 0.00500 U 0.00601 0.00618 120 124 1 35.0 - 142 2.79 27
Dichlorodifluoromethane 0.00500 U 0.00716 0.00727 143 145 1 10.0 - 160 1.52 29
1,1-Dichloroethane 0.00500 0.00965 0.0174 0.0169 155 145 1 25.0 - 158 2.92 27
1,2-Dichloroethane 0.00500 U 0.00768 0.00758 154*152*1 29.0 - 151 1.31 27
1,1-Dichloroethene 0.00500 0.00284 0.0100 0.0101 143 145 1 11.0 - 160 0.995 29
cis-1,2-Dichloroethene 0.00500 0.146 0.146 0.144 0.000*0.000*1 10.0 - 160 1.38 27
trans-1,2-Dichloroethene 0.00500 0.00346 0.0110 0.0107 151 145 1 17.0 - 153 2.76 27
1,2-Dichloropropane 0.00500 U 0.00735 0.00774 147 155 1 30.0 - 156 5.17 27
1,1-Dichloropropene 0.00500 U 0.00757 0.00771 151 154 1 25.0 - 158 1.83 27
1,3-Dichloropropane 0.00500 U 0.00567 0.00579 113 116 1 38.0 - 147 2.09 27
cis-1,3-Dichloropropene 0.00500 U 0.00636 0.00652 127 130 1 34.0 - 149 2.48 28
trans-1,3-Dichloropropene 0.00500 U 0.00563 0.00567 113 113 1 32.0 - 149 0.708 28
2,2-Dichloropropane 0.00500 U 0.00622 0.00630 124 126 1 24.0 - 152 1.28 29
Di-isopropyl ether 0.00500 U 0.00727 0.00737 145 147 1 21.0 - 160 1.37 28
Ethylbenzene 0.00500 U 0.00565 0.00572 113 114 1 30.0 - 155 1.23 27
Hexachloro-1,3-butadiene 0.00500 U 0.00547 0.00556 109 111 1 20.0 - 154 1.63 34
Isopropylbenzene 0.00500 U 0.00541 0.00570 108 114 1 28.0 - 157 5.22 27
p-Isopropyltoluene 0.00500 U 0.00605 0.00644 121 129 1 30.0 - 154 6.24 29
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3A-OR MATRIX SPIKE /SAMPLE NO.:
MATRIX SPIKE DUPLICATE RECOVERY R4099344-3
L1758896-01,02,03,04,05,06,07,08,09 R4099344-4
MS Sample / File ID:R4099344-3 / 0726_26 SDG:L1758896
MSD Sample / File ID:R4099344-4 / 0726_27 Analytical Batch:WG2330260
OS Sample / File ID:L1758896-03 / 0726_12 Matrix:GW
Instrument ID:VOCMS13
Analytical Method:8260B
Analyte Spike
Amount
OS
Result
MS
Result
MSD
Result MS Rec.MSD
Rec.Dilution Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l mg/l %%%%%
2-Butanone (MEK)0.0250 U 0.0255 0.0250 102 100 1 10.0 - 160 1.98 32
Methylene Chloride 0.00500 U 0.00702 0.00723 140 145*1 23.0 - 144 2.95 28
4-Methyl-2-pentanone (MIBK)0.0250 U 0.0271 0.0267 108 107 1 29.0 - 160 1.49 29
Methyl tert-butyl ether 0.00500 U 0.00668 0.00671 134 134 1 28.0 - 150 0.448 29
Naphthalene 0.00500 U 0.00427 0.00463 85.4 92.6 1 12.0 - 156 8.09 35
n-Propylbenzene 0.00500 U 0.00629 0.00660 126 132 1 31.0 - 154 4.81 28
Styrene 0.00500 U 0.00550 0.00567 110 113 1 33.0 - 155 3.04 28
1,1,1,2-Tetrachloroethane 0.00500 U 0.00610 0.00591 122 118 1 36.0 - 151 3.16 29
1,1,2,2-Tetrachloroethane 0.00500 U 0.00612 0.00613 122 123 1 33.0 - 150 0.163 28
1,1,2-Trichlorotrifluoroethane 0.00500 U 0.00816 0.00840 163*168*1 23.0 - 160 2.90 30
Tetrachloroethene 0.00500 U 0.00547 0.00552 109 110 1 10.0 - 160 0.910 27
Toluene 0.00500 U 0.00582 0.00599 116 120 1 26.0 - 154 2.88 28
1,2,3-Trichlorobenzene 0.00500 U 0.00457 0.00490 91.4 98.0 1 17.0 - 150 6.97 36
1,2,4-Trichlorobenzene 0.00500 U 0.00438 0.00473 87.6 94.6 1 24.0 - 150 7.68 33
1,1,1-Trichloroethane 0.00500 U 0.00728 0.00750 146 150 1 23.0 - 160 2.98 28
1,1,2-Trichloroethane 0.00500 U 0.00556 0.00572 111 114 1 35.0 - 147 2.84 27
Trichloroethene 0.00500 0.00034
0 0.00734 0.00735 140 140 1 10.0 - 160 0.136 25
Trichlorofluoromethane 0.00500 U 0.00855 0.00893 171*179*1 17.0 - 160 4.35 31
1,2,3-Trichloropropane 0.00500 U 0.00608 0.00614 122 123 1 34.0 - 151 0.982 29
1,2,4-Trimethylbenzene 0.00500 U 0.00607 0.00635 121 127 1 26.0 - 154 4.51 27
1,2,3-Trimethylbenzene 0.00500 U 0.00611 0.00634 122 127 1 32.0 - 149 3.69 28
1,3,5-Trimethylbenzene 0.00500 U 0.00610 0.00643 122 129 1 28.0 - 153 5.27 27
Vinyl chloride 0.00500 0.00191 0.00965 0.00988 155 159 1 10.0 - 160 2.36 27
Xylenes, Total 0.0150 U 0.0164 0.0171 109 114 1 29.0 - 154 4.18 28
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098893-1
RECOVERY R4098893-4
L1758896-10,11
LCS Sample / File ID:R4098893-1 / 0725_45LCS SDG:L1758896
LCSD Sample / File ID:R4098893-4 / 0725_72 Analytical Batch:WG2330346
Instrument ID:VOCMS16 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0241 0.0225 96.4 90.0 19.0 - 160 6.87 27
Acrolein 0.0250 0.0215 0.0172 86.0 68.8 10.0 - 160 22.2 26
Acrylonitrile 0.0250 0.0243 0.0247 97.2 98.8 55.0 - 149 1.63 20
Benzene 0.00500 0.00460 0.00454 92.0 90.8 70.0 - 123 1.31 20
Bromobenzene 0.00500 0.00436 0.00434 87.2 86.8 73.0 - 121 0.460 20
Bromodichloromethane 0.00500 0.00464 0.00465 92.8 93.0 75.0 - 120 0.215 20
Bromoform 0.00500 0.00426 0.00454 85.2 90.8 68.0 - 132 6.36 20
Bromomethane 0.00500 0.00471 0.00513 94.2 103 10.0 - 160 8.54 25
n-Butylbenzene 0.00500 0.00408 0.00387 81.6 77.4 73.0 - 125 5.28 20
sec-Butylbenzene 0.00500 0.00412 0.00398 82.4 79.6 75.0 - 125 3.46 20
tert-Butylbenzene 0.00500 0.00426 0.00411 85.2 82.2 76.0 - 124 3.58 20
Carbon tetrachloride 0.00500 0.00532 0.00497 106 99.4 68.0 - 126 6.80 20
Chlorobenzene 0.00500 0.00456 0.00466 91.2 93.2 80.0 - 121 2.17 20
Chlorodibromomethane 0.00500 0.00466 0.00467 93.2 93.4 77.0 - 125 0.214 20
Chloroethane 0.00500 0.00479 0.00445 95.8 89.0 47.0 - 150 7.36 20
Chloroform 0.00500 0.00459 0.00466 91.8 93.2 73.0 - 120 1.51 20
Chloromethane 0.00500 0.00566 0.00578 113 116 41.0 - 142 2.10 20
2-Chlorotoluene 0.00500 0.00443 0.00431 88.6 86.2 76.0 - 123 2.75 20
4-Chlorotoluene 0.00500 0.00437 0.00437 87.4 87.4 75.0 - 122 0.000 20
1,2-Dibromo-3-Chloropropane 0.00500 0.00414 0.00428 82.8 85.6 58.0 - 134 3.33 20
1,2-Dibromoethane 0.00500 0.00445 0.00480 89.0 96.0 80.0 - 122 7.57 20
Dibromomethane 0.00500 0.00505 0.00454 101 90.8 80.0 - 120 10.6 20
1,2-Dichlorobenzene 0.00500 0.00440 0.00428 88.0 85.6 79.0 - 121 2.76 20
1,3-Dichlorobenzene 0.00500 0.00466 0.00440 93.2 88.0 79.0 - 120 5.74 20
1,4-Dichlorobenzene 0.00500 0.00446 0.00447 89.2 89.4 79.0 - 120 0.224 20
Dichlorodifluoromethane 0.00500 0.00569 0.00528 114 106 51.0 - 149 7.47 20
1,1-Dichloroethane 0.00500 0.00474 0.00463 94.8 92.6 70.0 - 126 2.35 20
1,2-Dichloroethane 0.00500 0.00476 0.00489 95.2 97.8 70.0 - 128 2.69 20
1,1-Dichloroethene 0.00500 0.00510 0.00490 102 98.0 71.0 - 124 4.00 20
cis-1,2-Dichloroethene 0.00500 0.00469 0.00443 93.8 88.6 73.0 - 120 5.70 20
trans-1,2-Dichloroethene 0.00500 0.00467 0.00479 93.4 95.8 73.0 - 120 2.54 20
1,2-Dichloropropane 0.00500 0.00481 0.00494 96.2 98.8 77.0 - 125 2.67 20
1,1-Dichloropropene 0.00500 0.00448 0.00444 89.6 88.8 74.0 - 126 0.897 20
1,3-Dichloropropane 0.00500 0.00449 0.00457 89.8 91.4 80.0 - 120 1.77 20
cis-1,3-Dichloropropene 0.00500 0.00446 0.00424 89.2 84.8 80.0 - 123 5.06 20
trans-1,3-Dichloropropene 0.00500 0.00471 0.00457 94.2 91.4 78.0 - 124 3.02 20
2,2-Dichloropropane 0.00500 0.00453 0.00452 90.6 90.4 58.0 - 130 0.221 20
Di-isopropyl ether 0.00500 0.00469 0.00455 93.8 91.0 58.0 - 138 3.03 20
Ethylbenzene 0.00500 0.00429 0.00462 85.8 92.4 79.0 - 123 7.41 20
Hexachloro-1,3-butadiene 0.00500 0.00409 0.00393 81.8 78.6 54.0 - 138 3.99 20
Isopropylbenzene 0.00500 0.00404 0.00397 80.8 79.4 76.0 - 127 1.75 20
p-Isopropyltoluene 0.00500 0.00408 0.00384 81.6 76.8 76.0 - 125 6.06 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4098893-1
RECOVERY R4098893-4
L1758896-10,11
LCS Sample / File ID:R4098893-1 / 0725_45LCS SDG:L1758896
LCSD Sample / File ID:R4098893-4 / 0725_72 Analytical Batch:WG2330346
Instrument ID:VOCMS16 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l mg/l %%%%%
2-Butanone (MEK)0.0250 0.0241 0.0242 96.4 96.8 44.0 - 160 0.414 20
Methylene Chloride 0.00500 0.00455 0.00458 91.0 91.6 67.0 - 120 0.657 20
4-Methyl-2-pentanone (MIBK)0.0250 0.0235 0.0244 94.0 97.6 68.0 - 142 3.76 20
Methyl tert-butyl ether 0.00500 0.00458 0.00443 91.6 88.6 68.0 - 125 3.33 20
Naphthalene 0.00500 0.00319 0.00289 63.8 57.8 54.0 - 135 9.87 20
n-Propylbenzene 0.00500 0.00437 0.00426 87.4 85.2 77.0 - 124 2.55 20
Styrene 0.00500 0.00430 0.00414 86.0 82.8 73.0 - 130 3.79 20
1,1,1,2-Tetrachloroethane 0.00500 0.00431 0.00454 86.2 90.8 75.0 - 125 5.20 20
1,1,2,2-Tetrachloroethane 0.00500 0.00461 0.00473 92.2 94.6 65.0 - 130 2.57 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00512 0.00435 102 87.0 69.0 - 132 16.3 20
Tetrachloroethene 0.00500 0.00498 0.00478 99.6 95.6 72.0 - 132 4.10 20
Toluene 0.00500 0.00443 0.00467 88.6 93.4 79.0 - 120 5.27 20
1,2,3-Trichlorobenzene 0.00500 0.00369 0.00348 73.8 69.6 50.0 - 138 5.86 20
1,2,4-Trichlorobenzene 0.00500 0.00370 0.00336 74.0 67.2 57.0 - 137 9.63 20
1,1,1-Trichloroethane 0.00500 0.00535 0.00525 107 105 73.0 - 124 1.89 20
1,1,2-Trichloroethane 0.00500 0.00458 0.00472 91.6 94.4 80.0 - 120 3.01 20
Trichloroethene 0.00500 0.00480 0.00468 96.0 93.6 78.0 - 124 2.53 20
Trichlorofluoromethane 0.00500 0.00517 0.00439 103 87.8 59.0 - 147 16.3 20
1,2,3-Trichloropropane 0.00500 0.00501 0.00526 100 105 73.0 - 130 4.87 20
1,2,4-Trimethylbenzene 0.00500 0.00420 0.00404 84.0 80.8 76.0 - 121 3.88 20
1,2,3-Trimethylbenzene 0.00500 0.00412 0.00414 82.4 82.8 77.0 - 120 0.484 20
1,3,5-Trimethylbenzene 0.00500 0.00446 0.00427 89.2 85.4 76.0 - 122 4.35 20
Vinyl chloride 0.00500 0.00483 0.00386 96.6 77.2 67.0 - 131 22.3*20
Xylenes, Total 0.0150 0.0130 0.0135 86.7 90.0 79.0 - 123 3.77 20
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4099344-1
RECOVERY _______________
L1758896-01,02,03,04,05,06,07,08,09
LCS Sample / File ID:R4099344-1 / 0726_03LCS SDG:L1758896
LCSD Sample / File ID:_______________Analytical Batch:WG2330260
Instrument ID:VOCMS13 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
Acetone 0.0250 0.0185 74.0 19.0 - 160
Acrolein 0.0250 0.0457 183*10.0 - 160
Acrylonitrile 0.0250 0.0257 103 55.0 - 149
Benzene 0.00500 0.00530 106 70.0 - 123
Bromobenzene 0.00500 0.00502 100 73.0 - 121
Bromodichloromethane 0.00500 0.00546 109 75.0 - 120
Bromoform 0.00500 0.00371 74.2 68.0 - 132
Bromomethane 0.00500 0.00180 36.0 10.0 - 160
n-Butylbenzene 0.00500 0.00475 95.0 73.0 - 125
sec-Butylbenzene 0.00500 0.00495 99.0 75.0 - 125
tert-Butylbenzene 0.00500 0.00464 92.8 76.0 - 124
Carbon tetrachloride 0.00500 0.00578 116 68.0 - 126
Chlorobenzene 0.00500 0.00453 90.6 80.0 - 121
Chlorodibromomethane 0.00500 0.00445 89.0 77.0 - 125
Chloroethane 0.00500 0.00639 128 47.0 - 150
Chloroform 0.00500 0.00533 107 73.0 - 120
Chloromethane 0.00500 0.00418 83.6 41.0 - 142
2-Chlorotoluene 0.00500 0.00504 101 76.0 - 123
4-Chlorotoluene 0.00500 0.00492 98.4 75.0 - 122
1,2-Dibromo-3-Chloropropane 0.00500 0.00321 64.2 58.0 - 134
1,2-Dibromoethane 0.00500 0.00448 89.6 80.0 - 122
Dibromomethane 0.00500 0.00539 108 80.0 - 120
1,2-Dichlorobenzene 0.00500 0.00460 92.0 79.0 - 121
1,3-Dichlorobenzene 0.00500 0.00471 94.2 79.0 - 120
1,4-Dichlorobenzene 0.00500 0.00469 93.8 79.0 - 120
Dichlorodifluoromethane 0.00500 0.00423 84.6 51.0 - 149
1,1-Dichloroethane 0.00500 0.00579 116 70.0 - 126
1,2-Dichloroethane 0.00500 0.00581 116 70.0 - 128
1,1-Dichloroethene 0.00500 0.00542 108 71.0 - 124
cis-1,2-Dichloroethene 0.00500 0.00556 111 73.0 - 120
trans-1,2-Dichloroethene 0.00500 0.00545 109 73.0 - 120
1,2-Dichloropropane 0.00500 0.00560 112 77.0 - 125
1,1-Dichloropropene 0.00500 0.00551 110 74.0 - 126
1,3-Dichloropropane 0.00500 0.00451 90.2 80.0 - 120
cis-1,3-Dichloropropene 0.00500 0.00540 108 80.0 - 123
trans-1,3-Dichloropropene 0.00500 0.00473 94.6 78.0 - 124
2,2-Dichloropropane 0.00500 0.00495 99.0 58.0 - 130
Di-isopropyl ether 0.00500 0.00540 108 58.0 - 138
Ethylbenzene 0.00500 0.00440 88.0 79.0 - 123
Hexachloro-1,3-butadiene 0.00500 0.00456 91.2 54.0 - 138
Isopropylbenzene 0.00500 0.00432 86.4 76.0 - 127
p-Isopropyltoluene 0.00500 0.00485 97.0 76.0 - 125
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4099344-1
RECOVERY _______________
L1758896-01,02,03,04,05,06,07,08,09
LCS Sample / File ID:R4099344-1 / 0726_03LCS SDG:L1758896
LCSD Sample / File ID:_______________Analytical Batch:WG2330260
Instrument ID:VOCMS13 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
2-Butanone (MEK)0.0250 0.0205 82.0 44.0 - 160
Methylene Chloride 0.00500 0.00560 112 67.0 - 120
4-Methyl-2-pentanone (MIBK)0.0250 0.0216 86.4 68.0 - 142
Methyl tert-butyl ether 0.00500 0.00505 101 68.0 - 125
Naphthalene 0.00500 0.00394 78.8 54.0 - 135
n-Propylbenzene 0.00500 0.00484 96.8 77.0 - 124
Styrene 0.00500 0.00433 86.6 73.0 - 130
1,1,1,2-Tetrachloroethane 0.00500 0.00456 91.2 75.0 - 125
1,1,2,2-Tetrachloroethane 0.00500 0.00477 95.4 65.0 - 130
1,1,2-Trichlorotrifluoroethane 0.00500 0.00495 99.0 69.0 - 132
Tetrachloroethene 0.00500 0.00409 81.8 72.0 - 132
Toluene 0.00500 0.00465 93.0 79.0 - 120
1,2,3-Trichlorobenzene 0.00500 0.00409 81.8 50.0 - 138
1,2,4-Trichlorobenzene 0.00500 0.00386 77.2 57.0 - 137
1,1,1-Trichloroethane 0.00500 0.00546 109 73.0 - 124
1,1,2-Trichloroethane 0.00500 0.00462 92.4 80.0 - 120
Trichloroethene 0.00500 0.00517 103 78.0 - 124
Trichlorofluoromethane 0.00500 0.00542 108 59.0 - 147
1,2,3-Trichloropropane 0.00500 0.00490 98.0 73.0 - 130
1,2,4-Trimethylbenzene 0.00500 0.00473 94.6 76.0 - 121
1,2,3-Trimethylbenzene 0.00500 0.00481 96.2 77.0 - 120
1,3,5-Trimethylbenzene 0.00500 0.00472 94.4 76.0 - 122
Vinyl chloride 0.00500 0.00519 104 67.0 - 131
Xylenes, Total 0.0150 0.0130 86.7 79.0 - 123
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4100703-1
RECOVERY _______________
L1758896-04,05,07,08,09
LCS Sample / File ID:R4100703-1 / 0729A_01LCSA SDG:L1758896
LCSD Sample / File ID:_______________Analytical Batch:WG2332276
Instrument ID:VOCMS26 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
mg/l mg/l %%%%%
1,1-Dichloroethane 0.00500 0.00486 97.2 70.0 - 126
cis-1,2-Dichloroethene 0.00500 0.00479 95.8 73.0 - 120
Vinyl chloride 0.00500 0.00447 89.4 67.0 - 131
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4099344-2
Lab Sample ID:R4099344-2 SDG:L1758896
Lab File ID:0726_05 Preparation Date/Time:07/26/24 09:41
Instrument ID:VOCMS13 Analysis Date/Time:07/26/24 09:41
Analytical Batch:WG2330260 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4099344-1 VOCMS13 0726_03LCS 07/26/24 09:00
MW-1 L1758896-01 VOCMS13 0726_10 07/26/24 12:11
MW-25 L1758896-02 VOCMS13 0726_11 07/26/24 12:32
MW-2 L1758896-03 VOCMS13 0726_12 07/26/24 12:53
MW-4 L1758896-04 VOCMS13 0726_13 07/26/24 13:13
MW-8 L1758896-05 VOCMS13 0726_14 07/26/24 13:34
MW-3 L1758896-06 VOCMS13 0726_15 07/26/24 13:55
MW-7 L1758896-07 VOCMS13 0726_16 07/26/24 14:16
MW-5 L1758896-08 VOCMS13 0726_17 07/26/24 14:37
MW-10 L1758896-09 VOCMS13 0726_18 07/26/24 14:58
MS R4099344-3 VOCMS13 0726_26 07/26/24 17:45
MSD R4099344-4 VOCMS13 0726_27 07/26/24 18:06
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4098893-3
Lab Sample ID:R4098893-3 SDG:L1758896
Lab File ID:0725_48 Preparation Date/Time:07/25/24 22:50
Instrument ID:VOCMS16 Analysis Date/Time:07/25/24 22:50
Analytical Batch:WG2330346 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4098893-1 VOCMS16 0725_45LCS 07/25/24 21:45
TRIP BLANK L1758896-11 VOCMS16 0725_49 07/26/24 00:18
MW-9 L1758896-10 VOCMS16 0725_69 07/26/24 07:35
LCSD R4098893-4 VOCMS16 0725_72 07/26/24 08:41
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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4A-OR METHOD BLANK SAMPLE NO.:
R4100703-2
Lab Sample ID:R4100703-2 SDG:L1758896
Lab File ID:0729A_03A Preparation Date/Time:07/29/24 19:59
Instrument ID:VOCMS26 Analysis Date/Time:07/29/24 19:59
Analytical Batch:WG2332276 Dilution Factor:1
Analytical Method:8260B Matrix:GW
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4100703-1 VOCMS26 0729A_01LCSA 07/29/24 19:18
MW-10 L1758896-09 VOCMS26 0729A_04 07/29/24 20:32
MW-4 L1758896-04 VOCMS26 0729A_11 07/29/24 22:55
MW-8 L1758896-05 VOCMS26 0729A_12 07/29/24 23:16
MW-7 L1758896-07 VOCMS26 0729A_13 07/29/24 23:36
MW-5 L1758896-08 VOCMS26 0729A_14 07/29/24 23:56
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0628_01 SDG:L1758896
Instrument ID:VOCMS13 Analytical Method:8260B
Analysis Date/Time:06/28/24 10:39
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 107
96 95 5 9 7
173 174 0 2 0
174 95 50 200 94
175 174 5 9 9
176 174 95 105 97
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-.05A .05A 0628_02 06/28/24 11:00
STD-0.1A 0.1A 0628_02 06/28/24 11:00
STD-0.2A 0.2A 0628_02 06/28/24 11:00
STD-0.5A 0.5A 0628_02 06/28/24 11:00
STD-10A 10A 0628_02 06/28/24 11:00
STD-15A 15A 0628_02 06/28/24 11:00
STD-1A 1A 0628_02 06/28/24 11:00
STD-20A 20A 0628_02 06/28/24 11:00
STD-5A 5A 0628_02 06/28/24 11:00
STD-0.5 0.5 0628_04 06/28/24 11:42
STD-1 1 0628_05 06/28/24 12:03
STD-2 2 0628_06 06/28/24 12:25
STD-5.0 5.0 0628_07 06/28/24 12:46
STD-25 25 0628_08 06/28/24 13:07
STD-75 75 0628_09 06/28/24 13:28
STD-100 100 0628_10 06/28/24 13:50
STD-200 200 0628_11 06/28/24 14:11
SSCV VOCMS130628240628_15735103 0628_15 06/28/24 15:35
SSCV VOCMS130628240628_16735103 0628_16 06/28/24 15:56
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0726_01T SDG:L1758896
Instrument ID:VOCMS13 Analytical Method:8260B
Analysis Date/Time:07/26/24 08:18
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 118
96 95 5 9 6
173 174 0 2 0
174 95 50 200 85
175 174 5 9 8
176 174 95 105 99
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS130726240726_03735103 0726_03 07/26/24 09:00
LCS R4099344-1 0726_03LCS 07/26/24 09:00
BLANK R4099344-2 0726_05 07/26/24 09:41
MW-1 L1758896-01 0726_10 07/26/24 12:11
MW-25 L1758896-02 0726_11 07/26/24 12:32
OS L1758896-03 0726_12 07/26/24 12:53
MW-2 L1758896-03 0726_12 07/26/24 12:53
MW-4 L1758896-04 0726_13 07/26/24 13:13
MW-8 L1758896-05 0726_14 07/26/24 13:34
MW-3 L1758896-06 0726_15 07/26/24 13:55
MW-7 L1758896-07 0726_16 07/26/24 14:16
MW-5 L1758896-08 0726_17 07/26/24 14:37
MW-10 L1758896-09 0726_18 07/26/24 14:58
MS R4099344-3 0726_26 07/26/24 17:45
MSD R4099344-4 0726_27 07/26/24 18:06
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0717A_03 SDG:L1758896
Instrument ID:VOCMS16 Analytical Method:8260B
Analysis Date/Time:07/17/24 19:17
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 106
96 95 5 9 7
173 174 0 2 0
174 95 50 200 94
175 174 5 9 8
176 174 95 105 97
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.5 0.5 0717A_04 07/17/24 19:39
STD-1 1 0717A_05 07/17/24 20:00
STD-2 2 0717A_06 07/17/24 20:23
STD-5.0 5.0 0717A_07 07/17/24 20:44
STD-25 25 0717A_08 07/17/24 21:06
STD-75 75 0717A_09 07/17/24 21:28
STD-100 100 0717A_10 07/17/24 21:50
STD-200 200 0717A_11 07/17/24 22:11
SSCV VOCMS16071724A0717A_15739536 0717A_15 07/17/24 23:39
SSCV VOCMS16071724A0717A_17739536 0717A_17 07/18/24 00:23
STD-.05A .05A 0717A_19 07/18/24 01:06
STD-0.1A 0.1A 0717A_20 07/18/24 01:28
STD-0.2A 0.2A 0717A_21 07/18/24 01:51
STD-0.5A 0.5A 0717A_22 07/18/24 02:12
STD-1A 1A 0717A_23 07/18/24 02:34
STD-5A 5A 0717A_24 07/18/24 02:56
STD-10A 10A 0717A_25 07/18/24 03:18
STD-15A 15A 0717A_26 07/18/24 03:40
STD-20A 20A 0717A_27 07/18/24 04:01
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0725_44T SDG:L1758896
Instrument ID:VOCMS16 Analytical Method:8260B
Analysis Date/Time:07/25/24 21:23
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 109
96 95 5 9 8
173 174 0 2 0
174 95 50 200 92
175 174 5 9 8
176 174 95 105 99
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS160725240725_45739536 0725_45 07/25/24 21:45
LCS R4098893-1 0725_45LCS 07/25/24 21:45
BLANK R4098893-3 0725_48 07/25/24 22:50
TRIP BLANK L1758896-11 0725_49 07/26/24 00:18
MW-9 L1758896-10 0725_69 07/26/24 07:35
LCSD R4098893-4 0725_72 07/26/24 08:41
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0621_07 SDG:L1758896
Instrument ID:VOCMS26 Analytical Method:8260B
Analysis Date/Time:06/21/24 17:15
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 116
96 95 5 9 6
173 174 0 2 1
174 95 50 200 86
175 174 5 9 7
176 174 95 105 97
177 176 5 10 7
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.04 0.04 0621_08 06/21/24 17:35
STD-0.1 0.1 0621_09 06/21/24 17:56
STD-0.2 0.2 0621_10 06/21/24 18:16
STD-0.5 0.5 0621_11 06/21/24 18:37
STD-1 1 0621_12 06/21/24 18:58
STD-2 2 0621_13 06/21/24 19:18
STD-5.0 5.0 0621_14 06/21/24 19:39
STD-25 25 0621_15 06/21/24 20:00
STD-75 75 0621_16 06/21/24 20:20
STD-100 100 0621_17 06/21/24 20:40
STD-200 200 0621_18 06/21/24 21:01
STD-.05A .05A 0621_20 06/21/24 21:42
STD-0.1A 0.1A 0621_20 06/21/24 21:42
STD-0.2A 0.2A 0621_20 06/21/24 21:42
STD-0.5A 0.5A 0621_20 06/21/24 21:42
STD-10A 10A 0621_20 06/21/24 21:42
STD-15A 15A 0621_20 06/21/24 21:42
STD-1A 1A 0621_20 06/21/24 21:42
STD-20A 20A 0621_20 06/21/24 21:42
STD-5A 5A 0621_20 06/21/24 21:42
SSCV VOCMS260621240621_22733345 0621_22 06/21/24 22:23
SSCV VOCMS260621240621_23733345 0621_23 06/21/24 22:43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0729A_01T SDG:L1758896
Instrument ID:VOCMS26 Analytical Method:8260B
Analysis Date/Time:07/29/24 19:18
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
95 174 50 200 105
96 95 5 9 7
173 174 0 2 1
174 95 50 200 95
175 174 5 9 7
176 174 95 105 98
177 176 5 10 6
Sample ID Lab Sample ID File ID Analysis date/time
ICV VOCMS26072924A0729A_01733345 0729A_01 07/29/24 19:18
LCS R4100703-1 0729A_01LCSA 07/29/24 19:18
BLANK R4100703-2 0729A_03A 07/29/24 19:59
MW-10 L1758896-09 0729A_04 07/29/24 20:32
MW-4 L1758896-04 0729A_11 07/29/24 22:55
MW-8 L1758896-05 0729A_12 07/29/24 23:16
MW-7 L1758896-07 0729A_13 07/29/24 23:36
MW-5 L1758896-08 0729A_14 07/29/24 23:56
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS13 Calibration Start Date:06/28/24 11:00
Std File: 0726_03 Calibration End Date:06/28/24 14:11
Std Analysis Date:07/26/24 09:00
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 94060 8.15 93690 6.46 204723 4.52
UPPER LIMIT 188120 187380 409446
LOWER LIMIT 47030 46845 102362
LCS R4099344-1
WG2330260 1x
0726_03LC
S 94060 8.15 93690 6.46 204723 4.52
BLANK R4099344-2
WG2330260 1x 0726_05 78858 8.15 85346 6.46 186102 4.52
L1758896-01 WG2330260
1x 0726_10 82026 8.15 88763 6.46 197214 4.52
L1758896-02 WG2330260
1x 0726_11 78734 8.15 84806 6.46 184804 4.52
L1758896-03 WG2330260
1x 0726_12 79460 8.16 85795 6.46 189971 4.52
OS L1758896-03
WG2330260 1x 0726_12 79460 8.16 85795 6.46 189971 4.52
L1758896-04 WG2330260
1x 0726_13 79957 8.15 88029 6.46 193664 4.52
L1758896-05 WG2330260
1x 0726_14 77899 8.15 86454 6.46 193867 4.52
L1758896-06 WG2330260
1x 0726_15 77880 8.15 83958 6.46 188705 4.52
L1758896-07 WG2330260
1x 0726_16 79534 8.15 88961 6.46 200748 4.52
L1758896-08 WG2330260
1x 0726_17 79437 8.15 88170 6.46 195965 4.52
L1758896-09 WG2330260
1x 0726_18 78579 8.15 88656 6.46 187452 4.52
MS R4099344-3
WG2330260 1x 0726_26 89722 8.16 92150 6.46 195040 4.51
MSD R4099344-4
WG2330260 1x 0726_27 92200 8.15 95296 6.46 200599 4.52
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS16 Calibration Start Date:07/17/24 19:39
Std File: 0725_45 Calibration End Date:07/18/24 04:01
Std Analysis Date:07/25/24 21:45
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 55802 8.20 58499 6.52 149578 4.59
UPPER LIMIT 111604 116998 299156
LOWER LIMIT 27901 29250 74789
LCS R4098893-1
WG2330346 1x
0725_45LC
S 55802 8.20 58499 6.52 149578 4.59
BLANK R4098893-3
WG2330346 1x 0725_48 46390 8.20 49903 6.52 136802 4.59
L1758896-11 WG2330346
1x 0725_49 46470 8.19 49972 6.51 142108 4.59
L1758896-10 WG2330346
1x 0725_69 43055 8.20 45849 6.52 132821 4.59
LCSD R4098893-4
WG2330346 1x 0725_72 56542 8.20 57522 6.52 151553 4.59
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS26 Calibration Start Date:06/21/24 17:35
Std File: 0729A_01 Calibration End Date:06/21/24 21:42
Std Analysis Date:07/29/24 19:18
Sample ID File ID 1,4-DCB 8260-CB 8260-FB
Response RT Response RT Response RT
STANDARD 261993 8.24 236128 6.54 483577 4.60
UPPER LIMIT 523986 472256 967154
LOWER LIMIT 130997 118064 241789
LCS R4100703-1
WG2332276 1x
0729A_01L
CSA 261993 8.24 236128 6.54 483577 4.60
BLANK R4100703-2
WG2332276 1x 0729A_03A 233206 8.24 226514 6.54 467325 4.60
L1758896-09 WG2332276
1x 0729A_04 240245 8.24 231696 6.54 477266 4.60
L1758896-04 WG2332276
10x 0729A_11 229650 8.24 221123 6.54 459496 4.60
L1758896-05 WG2332276
25x 0729A_12 229913 8.24 218093 6.54 458575 4.60
L1758896-07 WG2332276
200x 0729A_13 228917 8.24 222157 6.54 458147 4.60
L1758896-08 WG2332276
25x 0729A_14 229995 8.24 222795 6.54 458525 4.60
1,4-DCB - 8260-1,4-DICHLOROBENZENE-D4 8260-CB - 8260-CHLOROBENZENE-D5
8260-FB - 8260-FLUOROBENZENE
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-1
Lab Sample ID:L1758896-01 SDG:L1758896
Client Sample ID:MW-1 Collected Date/Time:07/17/24 08:48
Lab File ID:0726_10 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 12:11
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 12:11
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.09 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-1
Lab Sample ID:L1758896-01 SDG:L1758896
Client Sample ID:MW-1 Collected Date/Time:07/17/24 08:48
Lab File ID:0726_10 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 12:11
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 12:11
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-25
Lab Sample ID:L1758896-02 SDG:L1758896
Client Sample ID:MW-25 Collected Date/Time:07/17/24 09:45
Lab File ID:0726_11 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 12:32
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 12:32
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 2.22 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-25
Lab Sample ID:L1758896-02 SDG:L1758896
Client Sample ID:MW-25 Collected Date/Time:07/17/24 09:45
Lab File ID:0726_11 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 12:32
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 12:32
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-2
Lab Sample ID:L1758896-03 SDG:L1758896
Client Sample ID:MW-2 Collected Date/Time:07/17/24 10:32
Lab File ID:0726_12 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 12:53
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 12:53
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 J5 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 4.29 0.000232 J 0.0000941 0.00100
Bromobenzene 108-86-1 7.32 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U J5 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U J5 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.00965 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U J5 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.00284 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.81 0.146 V 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.00346 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-2
Lab Sample ID:L1758896-03 SDG:L1758896
Client Sample ID:MW-2 Collected Date/Time:07/17/24 10:32
Lab File ID:0726_12 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 12:53
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 12:53
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U J5 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U J5 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 5.47 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 4.62 0.000340 J 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U J5 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.00191 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-4
Lab Sample ID:L1758896-04 SDG:L1758896
Client Sample ID:MW-4 Collected Date/Time:07/17/24 12:40
Lab File ID:0726_13 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 13:13
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 13:13
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 4.29 0.000247 J 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.0437 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.00647 0.000188 0.00100
trans-1,2-Dichloroethene 156-60-5 3.16 0.00881 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-4
Lab Sample ID:L1758896-04 SDG:L1758896
Client Sample ID:MW-4 Collected Date/Time:07/17/24 12:40
Lab File ID:0726_13 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 13:13
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 13:13
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00112 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.0434 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-4
Lab Sample ID:L1758896-04 SDG:L1758896
Client Sample ID:MW-4 Collected Date/Time:07/17/24 12:40
Lab File ID:0729A_11 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 22:55
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 22:55
Dilution Factor:10 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:0.5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
cis-1,2-Dichloroethene 156-59-2 3.90 0.247 0.00126 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-8
Lab Sample ID:L1758896-05 SDG:L1758896
Client Sample ID:MW-8 Collected Date/Time:07/17/24 14:05
Lab File ID:0726_14 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 13:34
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 13:34
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 4.29 0.000292 J 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 2.27 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.138 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.0416 0.000188 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.0127 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-8
Lab Sample ID:L1758896-05 SDG:L1758896
Client Sample ID:MW-8 Collected Date/Time:07/17/24 14:05
Lab File ID:0726_14 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 13:34
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 13:34
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.21 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 4.62 0.000632 J 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.0105 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-8
Lab Sample ID:L1758896-05 SDG:L1758896
Client Sample ID:MW-8 Collected Date/Time:07/17/24 14:05
Lab File ID:0729A_12 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 23:16
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 23:16
Dilution Factor:25 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:0.2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
cis-1,2-Dichloroethene 156-59-2 3.89 0.726 0.00315 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-3
Lab Sample ID:L1758896-06 SDG:L1758896
Client Sample ID:MW-3 Collected Date/Time:07/17/24 15:35
Lab File ID:0726_15 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 13:55
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 13:55
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.09 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 4.29 0.00140 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.00405 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.000683 J 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.81 0.0527 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.00162 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 6.47 0.000175 J 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-3
Lab Sample ID:L1758896-06 SDG:L1758896
Client Sample ID:MW-3 Collected Date/Time:07/17/24 15:35
Lab File ID:0726_15 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 13:55
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 13:55
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 5.73 0.000401 J 0.000300 0.00100
Toluene 108-88-3 5.47 0.00123 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.09 0.000163 J 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00162 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.000865 J 0.000234 0.00100
Xylenes, Total 1330-20-7 6.87 0.000433 J 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-7
Lab Sample ID:L1758896-07 SDG:L1758896
Client Sample ID:MW-7 Collected Date/Time:07/18/24 08:20
Lab File ID:0726_16 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 14:16
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 14:16
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.05 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 3.49 U 0.000671 0.0100
Benzene 71-43-2 4.29 0.00141 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,2-Dichloroethane 107-06-2 4.40 0.00114 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.141 0.000188 0.00100
trans-1,2-Dichloroethene 156-60-5 3.16 0.0901 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.92 0.00695 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.13 U 0.00119 0.0100
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-7
Lab Sample ID:L1758896-07 SDG:L1758896
Client Sample ID:MW-7 Collected Date/Time:07/18/24 08:20
Lab File ID:0726_16 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 14:16
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 14:16
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00141 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-7
Lab Sample ID:L1758896-07 SDG:L1758896
Client Sample ID:MW-7 Collected Date/Time:07/18/24 08:20
Lab File ID:0729A_13 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 23:36
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 23:36
Dilution Factor:200 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:0.025 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
1,1-Dichloroethane 75-34-3 3.59 0.707 0.0200 0.200
cis-1,2-Dichloroethene 156-59-2 3.89 4.19 0.0252 0.200
Vinyl chloride 75-01-4 2.01 0.280 0.0468 0.200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-5
Lab Sample ID:L1758896-08 SDG:L1758896
Client Sample ID:MW-5 Collected Date/Time:07/18/24 09:40
Lab File ID:0726_17 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 14:37
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 14:37
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 4.29 0.000343 J 0.0000941 0.00100
Bromobenzene 108-86-1 7.30 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 2.26 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.0829 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.0233 0.000188 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.0195 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.93 0.000255 J 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-5
Lab Sample ID:L1758896-08 SDG:L1758896
Client Sample ID:MW-5 Collected Date/Time:07/18/24 09:40
Lab File ID:0726_17 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 14:37
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 14:37
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.20 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00115 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.00767 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-5
Lab Sample ID:L1758896-08 SDG:L1758896
Client Sample ID:MW-5 Collected Date/Time:07/18/24 09:40
Lab File ID:0729A_14 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 23:56
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 23:56
Dilution Factor:25 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:0.2 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
cis-1,2-Dichloroethene 156-59-2 3.89 0.672 0.00315 0.0250
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-10
Lab Sample ID:L1758896-09 SDG:L1758896
Client Sample ID:MW-10 Collected Date/Time:07/18/24 11:00
Lab File ID:0726_18 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 14:58
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 14:58
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U J4 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-10
Lab Sample ID:L1758896-09 SDG:L1758896
Client Sample ID:MW-10 Collected Date/Time:07/18/24 11:00
Lab File ID:0726_18 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 14:58
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 14:58
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-10
Lab Sample ID:L1758896-09 SDG:L1758896
Client Sample ID:MW-10 Collected Date/Time:07/18/24 11:00
Lab File ID:0729A_04 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 20:32
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 20:32
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
cis-1,2-Dichloroethene 156-59-2 3.89 0.000166 J 0.000126 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-9
Lab Sample ID:L1758896-10 SDG:L1758896
Client Sample ID:MW-9 Collected Date/Time:07/18/24 12:30
Lab File ID:0725_69 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS16 Preparation Date/Time:07/26/24 07:35
Analytical Batch:WG2330346 Analysis Date/Time:07/26/24 07:35
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.17 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.89 0.000309 J 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET MW-9
Lab Sample ID:L1758896-10 SDG:L1758896
Client Sample ID:MW-9 Collected Date/Time:07/18/24 12:30
Lab File ID:0725_69 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS16 Preparation Date/Time:07/26/24 07:35
Analytical Batch:WG2330346 Analysis Date/Time:07/26/24 07:35
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 5.54 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U J3 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1758896-11 SDG:L1758896
Client Sample ID:TRIP BLANK Collected Date/Time:07/18/24 00:00
Lab File ID:0725_49 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS16 Preparation Date/Time:07/26/24 00:18
Analytical Batch:WG2330346 Analysis Date/Time:07/26/24 00:18
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.16 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET TRIP BLANK
Lab Sample ID:L1758896-11 SDG:L1758896
Client Sample ID:TRIP BLANK Collected Date/Time:07/18/24 00:00
Lab File ID:0725_49 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS16 Preparation Date/Time:07/26/24 00:18
Analytical Batch:WG2330346 Analysis Date/Time:07/26/24 00:18
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.13 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 5.54 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U J3 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS13
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 06/28/24
11:42
06/28/24
12:03
06/28/24
12:25
06/28/24
12:46
06/28/24
13:07
06/28/24
13:28
06/28/24
13:50
06/28/24
14:11
VINYL CHLORIDE 0.4570 0.4190 0.4120 0.4160 0.4730 0.4250 0.41 0.42
CHLOROETHANE 0.2490 0.2260 0.2240 0.2230 0.2410 0.2110 0.20 0.1810
TRICHLOROFLUOROMETHANE 0.4110 0.4040 0.4040 0.3940 0.4630 0.4270 0.4290 0.4310
ACROLEIN 0.0560 0.0570 0.0580 0.0610 0.0670 0.0610 0.0580 0.0550
1,1-DICHLOROETHENE 0.2310 0.2090 0.2150 0.2090 0.2530 0.2250 0.2260 0.2340
1,1,2-TRICHLOROTRIFLUOROETHANE 0.23 0.23 0.2210 0.2080 0.2530 0.2310 0.2240 0.2370
ACRYLONITRILE 0.1360 0.13 0.13 0.1320 0.1480 0.1350 0.1280 0.1230
TRANS-1,2-DICHLOROETHENE 0.2650 0.2420 0.2490 0.2530 0.2830 0.2560 0.2550 0.2560
METHYL TERT-BUTYL ETHER 0.7760 0.73 0.7110 0.75 0.8350 0.7620 0.7530 0.7370
1,1-DICHLOROETHANE 0.5510 0.52 0.5210 0.5230 0.57 0.5220 0.5160 0.5090
DI-ISOPROPYL ETHER 1.2560 1.1790 1.1690 1.2150 1.3570 1.2540 1.2280 1.1930
2,2-DICHLOROPROPANE 0.4470 0.3930 0.3750 0.3790 0.4180 0.3790 0.3670 0.3710
CIS-1,2-DICHLOROETHENE 0.3050 0.2690 0.2730 0.28 0.3050 0.2790 0.2770 0.2730
2-BUTANONE (MEK)0.19 0.1860 0.1840 0.1890 0.2130 0.1940 0.1860 0.18
CHLOROFORM 0.5780 0.5060 0.4820 0.49 0.5340 0.4990 0.4820 0.4810
1,1,1-TRICHLOROETHANE 0.4570 0.4040 0.4210 0.4120 0.4780 0.44 0.4330 0.4380
CARBON TETRACHLORIDE 0.3190 0.3160 0.3370 0.3590 0.4410 0.4120 0.4060 0.4210
1,1-DICHLOROPROPENE 0.3350 0.2940 0.3050 0.3160 0.3640 0.3390 0.3330 0.3420
BENZENE 1.1530 1.1030 1.1050 1.0980 1.2140 1.11 1.0930 1.0860
1,2-DICHLOROETHANE 0.42 0.3870 0.3870 0.3930 0.4220 0.3810 0.3770 0.37
TRICHLOROETHENE 0.3160 0.2910 0.2890 0.2980 0.3290 0.3050 0.3030 0.3030
1,2-DICHLOROPROPANE 0.2420 0.2250 0.2240 0.2250 0.2560 0.2370 0.2350 0.2350
DIBROMOMETHANE 0.1740 0.1670 0.1580 0.1640 0.1790 0.1640 0.1620 0.1610
BROMODICHLOROMETHANE 0.3840 0.3640 0.3510 0.3630 0.4070 0.3760 0.3750 0.3760
CIS-1,3-DICHLOROPROPENE 0.42 0.3990 0.3870 0.4190 0.4820 0.4550 0.4560 0.4550
4-METHYL-2-PENTANONE (MIBK)0.8520 0.8330 0.8140 0.8730 0.9880 0.9060 0.8330 0.7690
TOLUENE 3.3460 3.2330 3.0030 3.0580 3.2810 3.0260 2.9150 2.8030
TRANS-1,3-DICHLOROPROPENE 1.0470 0.9330 0.95 0.9780 1.1130 1.0350 1.0050 0.9850
1,1,2-TRICHLOROETHANE 0.7190 0.6210 0.5930 0.6330 0.67 0.62 0.5960 0.5670
TETRACHLOROETHENE 0.6730 0.6250 0.6220 0.6420 0.7050 0.64 0.62 0.6110
1,3-DICHLOROPROPANE 1.0850 1.1210 1.0360 1.0750 1.1810 1.0880 1.0440 1.0030
CHLORODIBROMOMETHANE 0.7110 0.6790 0.7010 0.72 0.8060 0.76 0.7370 0.7190
1,2-DIBROMOETHANE 0.6110 0.6050 0.5840 0.6250 0.6860 0.64 0.6130 0.5890
CHLOROBENZENE 2.3290 2.16 1.9570 2.0560 2.2260 2.0630 1.9910 1.9130
1,1,1,2-TETRACHLOROETHANE 0.7280 0.6730 0.6590 0.6960 0.7660 0.7130 0.6950 0.6770
ETHYLBENZENE 1.1350 1.0170 1.0080 1.0870 1.2050 1.1340 1.0970 1.0690
M&P-XYLENE 1.3820 1.3080 1.2870 1.3410 1.5020 1.3990 1.35 1.2970
O-XYLENE 1.3340 1.2160 1.2070 1.2810 1.4530 1.3590 1.3150 1.28
STYRENE 1.9970 1.9560 1.8360 2.0760 2.4510 2.3390 2.28 2.2060
BROMOFORM 0.5040 0.5180 0.5170 0.5250 0.6040 0.5760 0.56 0.5440
ISOPROPYLBENZENE 3.1750 3.1480 3.0380 3.2860 3.7430 3.5020 3.3710 3.2980
BROMOBENZENE 1.4280 1.3180 1.3010 1.3030 1.37 1.2590 1.2510 1.2520
1,1,2,2-TETRACHLOROETHANE 0.87 0.7640 0.7510 0.7590 0.7680 0.6940 0.6690 0.6620
1,2,3-TRICHLOROPROPANE 0.22 0.2350 0.2240 0.2350 0.2530 0.2290 0.22 0.2180
N-PROPYLBENZENE 3.7680 3.3880 3.3950 3.5280 3.8520 3.4980 3.50 3.4550
2-CHLOROTOLUENE 2.5810 2.3750 2.3370 2.3680 2.5160 2.30 2.2810 2.2840
4-CHLOROTOLUENE 2.2290 2.1260 2.1370 2.1930 2.3470 2.1570 2.1550 2.1230
1,3,5-TRIMETHYLBENZENE 2.6080 2.4140 2.4290 2.5910 2.8460 2.5920 2.5640 2.5380
TERT-BUTYLBENZENE 2.2240 2.08 2.0910 2.2160 2.4460 2.2360 2.2090 2.20
1,2,4-TRIMETHYLBENZENE 2.5890 2.3830 2.5160 2.6650 2.9560 2.6710 2.6580 2.62
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS13
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 06/28/24
11:42
06/28/24
12:03
06/28/24
12:25
06/28/24
12:46
06/28/24
13:07
06/28/24
13:28
06/28/24
13:50
06/28/24
14:11
SEC-BUTYLBENZENE 3.0530 2.8570 2.9210 3.0390 3.3690 3.0830 3.0630 3.0570
1,3-DICHLOROBENZENE 1.64 1.5090 1.5560 1.5910 1.6920 1.5550 1.5410 1.5260
P-ISOPROPYLTOLUENE 2.6130 2.4740 2.58 2.7460 3.1590 2.8870 2.8590 2.82
1,4-DICHLOROBENZENE 1.7330 1.5780 1.5860 1.5950 1.7120 1.57 1.5630 1.5250
1,2,3-TRIMETHYLBENZENE 2.8360 2.57 2.6210 2.7180 2.9510 2.6990 2.6760 2.6030
1,2-DICHLOROBENZENE 1.6080 1.4750 1.4810 1.5070 1.6170 1.4950 1.4960 1.4470
N-BUTYLBENZENE 0.5710 0.5450 0.5490 0.5930 0.7020 0.66 0.65 0.6520
1,2,4-TRICHLOROBENZENE 0.5210 0.5710 0.6590 0.7440 0.9270 0.8980 0.9020 0.89
HEXACHLORO-1,3-BUTADIENE 0.3940 0.3470 0.3660 0.3710 0.4110 0.3720 0.3730 0.37
1,2,3-TRICHLOROBENZENE 0.3260 0.46 0.56 0.6530 0.8160 0.7740 0.7730 0.7430
1,2-DICHLOROETHANE-D4 0.2740 0.2730 0.2780 0.2760 0.29 0.2650 0.2650 0.1970
TOLUENE-D8 2.5150 2.5480 2.4430 2.45 2.4020 2.4120 2.30 1.6780
4-BROMOFLUOROBENZENE 0.8740 0.8780 0.8670 0.8710 0.8920 0.9010 0.87 0.6260
DICHLORODIFLUOROMETHANE 0.3380 0.3630 0.3410 0.4130 0.3730 0.3570 0.3560
CHLOROMETHANE 0.7310 0.6870 0.6760 0.6780 0.5880 0.5640
ACETONE 0.1560 0.1430 0.1430 0.1530 0.1360 0.1310 0.1260
NAPHTHALENE 0.55 0.8630 1.3190 1.8460 1.8670 1.8630 1.8180
BROMOMETHANE 0.2280 0.1960 0.1870 0.1710 0.1750 0.1770
METHYLENE CHLORIDE 0.3110 0.2920 0.3010 0.2720 0.2690 0.2680
1,2-DIBROMO-3-CHLOROPROPANE 0.1570 0.1540 0.1880 0.1780 0.1730 0.1660
File ID:0628_04 0628_05 0628_06 0628_07 0628_08 0628_09 0628_10 0628_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS13
Analyte RRF. Avg %RSD COD
Analysis date/time
VINYL CHLORIDE 0.428873 5.39
CHLOROETHANE 0.21943 9.97
TRICHLOROFLUOROMETHANE 0.420408 5.24
ACROLEIN 0.059056 6.61
1,1-DICHLOROETHENE 0.225304 6.45
1,1,2-TRICHLOROTRIFLUOROETHANE 0.229233 5.57
ACRYLONITRILE 0.132905 5.44
TRANS-1,2-DICHLOROETHENE 0.25725 4.84
METHYL TERT-BUTYL ETHER 0.756676 4.94
1,1-DICHLOROETHANE 0.529217 3.9
DI-ISOPROPYL ETHER 1.231409 4.88
2,2-DICHLOROPROPANE 0.391083 7.13
CIS-1,2-DICHLOROETHENE 0.282524 5.01
2-BUTANONE (MEK)0.19025 5.33
CHLOROFORM 0.50627 6.69
1,1,1-TRICHLOROETHANE 0.435282 5.53
CARBON TETRACHLORIDE 0.376477 13.12
1,1-DICHLOROPROPENE 0.328448 6.77
BENZENE 1.120314 3.84
1,2-DICHLOROETHANE 0.392202 4.84
TRICHLOROETHENE 0.304292 4.28
1,2-DICHLOROPROPANE 0.234841 4.53
DIBROMOMETHANE 0.16624 4.27
BROMODICHLOROMETHANE 0.374536 4.44
CIS-1,3-DICHLOROPROPENE 0.434157 7.55
4-METHYL-2-PENTANONE (MIBK)0.858553 7.7
TOLUENE 3.083207 6.1
TRANS-1,3-DICHLOROPROPENE 1.00575 5.77
1,1,2-TRICHLOROETHANE 0.627302 7.65
TETRACHLOROETHENE 0.642306 4.95
1,3-DICHLOROPROPANE 1.079068 5.08
CHLORODIBROMOMETHANE 0.729268 5.38
1,2-DIBROMOETHANE 0.619217 5.21
CHLOROBENZENE 2.086819 6.8
1,1,1,2-TETRACHLOROETHANE 0.700879 4.9
ETHYLBENZENE 1.093962 5.95
M&P-XYLENE 1.358244 5.16
O-XYLENE 1.305602 6.09
STYRENE 2.142575 9.83
BROMOFORM 0.543422 6.31
ISOPROPYLBENZENE 3.320195 6.7
BROMOBENZENE 1.310195 4.75
1,1,2,2-TETRACHLOROETHANE 0.742076 9.09
1,2,3-TRICHLOROPROPANE 0.229206 5.18
N-PROPYLBENZENE 3.548029 4.81
2-CHLOROTOLUENE 2.380237 4.67
4-CHLOROTOLUENE 2.183439 3.44
1,3,5-TRIMETHYLBENZENE 2.572716 5.17
TERT-BUTYLBENZENE 2.212822 5.05
1,2,4-TRIMETHYLBENZENE 2.632246 6.18
SEC-BUTYLBENZENE 3.055452 4.89
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS13
Analyte RRF. Avg %RSD COD
Analysis date/time
1,3-DICHLOROBENZENE 1.57613 3.93
P-ISOPROPYLTOLUENE 2.767262 7.78
1,4-DICHLOROBENZENE 1.607767 4.6
1,2,3-TRIMETHYLBENZENE 2.709197 4.72
1,2-DICHLOROBENZENE 1.515628 4.1
N-BUTYLBENZENE 0.615416 9.46
1,2,4-TRICHLOROBENZENE 0.764183 21.38 1
HEXACHLORO-1,3-BUTADIENE 0.375422 5.1
1,2,3-TRICHLOROBENZENE 0.63797 27.46 0.999
1,2-DICHLOROETHANE-D4 0.264575 10.71
TOLUENE-D8 2.343532 11.91
4-BROMOFLUOROBENZENE 0.847362 10.64
DICHLORODIFLUOROMETHANE 0.363016 6.92
CHLOROMETHANE 0.654161 9.78 0.996
ACETONE 0.141098 7.75
NAPHTHALENE 1.446623 37.96 0.999
BROMOMETHANE 0.189002 11.09
METHYLENE CHLORIDE 0.285518 6.48
1,2-DIBROMO-3-CHLOROPROPANE 0.169172 7.47
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 07/17/24
19:39
07/17/24
20:00
07/17/24
20:23
07/17/24
20:44
07/17/24
21:06
07/17/24
21:28
07/17/24
21:50
07/17/24
22:11
DICHLORODIFLUOROMETHANE 0.16 0.2250 0.2310 0.2680 0.3310 0.3110
VINYL CHLORIDE 0.1890 0.2440 0.20 0.2780 0.3190 0.3590 0.4010 0.3910
BROMOMETHANE 0.2080 0.1730 0.1650 0.1570 0.1570 0.1760 0.1610 0.1420
ACROLEIN 0.1610 0.1710 0.1750 0.1910 0.2090 0.2130 0.21 0.2110
1,1-DICHLOROETHENE 0.1820 0.2230 0.2130 0.2330 0.2870 0.2730 0.2760 0.2660
1,1,2-TRICHLOROTRIFLUOROETHANE 0.1020 0.1770 0.1980 0.2170 0.2780 0.26 0.2760 0.2650
ACETONE 0.23 0.2060 0.1890 0.2080 0.1940 0.1650 0.2430 0.2350
ACRYLONITRILE 0.2580 0.2460 0.2510 0.2850 0.2960 0.2860 0.2720 0.2670
TRANS-1,2-DICHLOROETHENE 0.2390 0.2950 0.2970 0.3080 0.3320 0.3130 0.3020 0.2970
METHYL TERT-BUTYL ETHER 0.8420 0.9290 0.8770 0.9510 1.02 0.9880 0.9360 0.9490
1,1-DICHLOROETHANE 0.59 0.61 0.5960 0.6370 0.6450 0.6280 0.6030 0.59
DI-ISOPROPYL ETHER 1.2730 1.3910 1.4090 1.4840 1.5660 1.5050 1.4350 1.3980
2,2-DICHLOROPROPANE 0.2330 0.2740 0.2640 0.2870 0.3090 0.2780 0.2490 0.22
CIS-1,2-DICHLOROETHENE 0.2940 0.3590 0.3320 0.3520 0.3630 0.3580 0.3410 0.3330
2-BUTANONE (MEK)0.39 0.3260 0.3680 0.3820 0.3870 0.3870 0.3920 0.3950
CHLOROFORM 0.5610 0.5980 0.5650 0.5840 0.5950 0.5840 0.5560 0.5410
1,1,1-TRICHLOROETHANE 0.3490 0.4010 0.4290 0.4380 0.50 0.4840 0.4650 0.4580
CARBON TETRACHLORIDE 0.3390 0.4010 0.4030 0.4410 0.5070 0.4770 0.4620 0.4630
1,1-DICHLOROPROPENE 0.22 0.3080 0.3330 0.36 0.4170 0.41 0.3950 0.3950
BENZENE 1.1840 1.2290 1.2650 1.3010 1.33 1.3070 1.26 1.2610
1,2-DICHLOROETHANE 0.4760 0.5020 0.48 0.5030 0.50 0.4870 0.4610 0.45
TRICHLOROETHENE 0.2730 0.3170 0.3210 0.3360 0.3770 0.3720 0.3560 0.3570
1,2-DICHLOROPROPANE 0.2180 0.2450 0.26 0.2630 0.2690 0.2680 0.2560 0.2580
DIBROMOMETHANE 0.1440 0.1940 0.2010 0.2040 0.21 0.2080 0.1960 0.1990
BROMODICHLOROMETHANE 0.4080 0.3930 0.41 0.4170 0.4330 0.4340 0.4170 0.42
CIS-1,3-DICHLOROPROPENE 0.4650 0.4560 0.4830 0.4970 0.5290 0.5340 0.5110 0.5250
4-METHYL-2-PENTANONE (MIBK)1.6460 1.7430 1.8950 1.9510 1.9510 1.9030 1.8280 1.7420
TOLUENE 3.1230 3.3660 3.5240 3.4690 3.4880 3.47 3.4020 3.4020
TRANS-1,3-DICHLOROPROPENE 1.1140 1.1350 1.24 1.2350 1.2270 1.23 1.2120 1.24
1,1,2-TRICHLOROETHANE 0.7350 0.8250 0.8390 0.7880 0.7610 0.7410 0.7410 0.7350
TETRACHLOROETHENE 0.4660 0.5950 0.6370 0.6480 0.6780 0.6620 0.6440 0.6510
1,3-DICHLOROPROPANE 1.2790 1.2670 1.37 1.3270 1.2780 1.2910 1.2710 1.2990
CHLORODIBROMOMETHANE 0.7820 0.9180 0.94 0.9080 0.8870 0.8910 0.8810 0.8920
1,2-DIBROMOETHANE 0.7990 0.7940 0.81 0.8390 0.8340 0.8180 0.8060 0.8160
CHLOROBENZENE 2.2050 2.2710 2.3830 2.2840 2.29 2.2920 2.2480 2.2540
1,1,1,2-TETRACHLOROETHANE 0.78 0.8960 0.8540 0.8810 0.8290 0.8360 0.8090 0.8070
ETHYLBENZENE 0.8980 1.1090 1.0880 1.2180 1.1880 1.1820 1.1610 1.1660
M&P-XYLENE 1.1330 1.2490 1.2790 1.40 1.4580 1.44 1.4140 1.4250
O-XYLENE 1.0730 1.1150 1.2770 1.3820 1.4440 1.4560 1.4140 1.4190
STYRENE 1.8460 1.9110 2.1570 2.2940 2.4440 2.46 2.4220 2.4590
BROMOFORM 0.6780 0.6690 0.6870 0.6810 0.69 0.6990 0.6790 0.6990
ISOPROPYLBENZENE 2.0610 2.6220 2.9140 3.1050 3.4470 3.4840 3.33 3.4190
BROMOBENZENE 1.5530 1.4820 1.7010 1.6230 1.5530 1.4930 1.4020 1.4210
1,1,2,2-TETRACHLOROETHANE 1.0840 1.18 1.3210 1.2920 1.2170 1.1690 1.0840 1.1030
1,2,3-TRICHLOROPROPANE 0.3770 0.4310 0.4950 0.4370 0.4250 0.4110 0.3830 0.3840
N-PROPYLBENZENE 2.7060 3.1990 3.5880 3.5660 3.9370 3.8240 3.5680 3.6170
2-CHLOROTOLUENE 2.2860 2.4530 2.6750 2.5850 2.6570 2.5930 2.4030 2.4050
4-CHLOROTOLUENE 1.9520 2.1160 2.4550 2.4210 2.50 2.4270 2.2890 2.3290
1,3,5-TRIMETHYLBENZENE 1.9710 2.1210 2.4770 2.5430 2.7940 2.7220 2.4870 2.5740
TERT-BUTYLBENZENE 1.5830 1.7060 2.0610 2.0330 2.3720 2.3620 2.1690 2.2460
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100 RRF: 200
Analysis date/time 07/17/24
19:39
07/17/24
20:00
07/17/24
20:23
07/17/24
20:44
07/17/24
21:06
07/17/24
21:28
07/17/24
21:50
07/17/24
22:11
1,2,4-TRIMETHYLBENZENE 2.1210 2.3310 2.5470 2.6090 2.9880 2.92 2.7060 2.7540
SEC-BUTYLBENZENE 1.8980 2.3940 2.5410 2.7730 3.1840 3.0910 2.8610 2.9720
1,3-DICHLOROBENZENE 1.48 1.64 1.8810 1.7390 1.75 1.7130 1.5950 1.6280
P-ISOPROPYLTOLUENE 1.7720 2.0850 2.4310 2.5990 2.9560 2.9030 2.6630 2.76
1,4-DICHLOROBENZENE 1.7240 1.6260 1.8680 1.7380 1.7990 1.74 1.65 1.6750
1,2,3-TRIMETHYLBENZENE 2.3370 2.4030 2.9060 2.7680 2.9140 2.9170 2.6850 2.7810
1,2-DICHLOROBENZENE 1.4590 1.5980 1.7880 1.6940 1.7340 1.7110 1.6210 1.6490
N-BUTYLBENZENE 1.5350 1.6680 1.9090 1.9390 2.2470 2.1880 2.09 2.1530
1,2-DIBROMO-3-CHLOROPROPANE 0.3210 0.3430 0.3690 0.3740 0.4030 0.4220 0.4040 0.4190
1,2,4-TRICHLOROBENZENE 0.6180 0.7130 0.79 0.7960 0.88 0.9230 0.9150 0.9680
HEXACHLORO-1,3-BUTADIENE 0.2850 0.3230 0.36 0.3390 0.3740 0.3710 0.3560 0.3690
NAPHTHALENE 2.4950 2.5240 2.62 2.9740 3.3810 3.8110 3.6930 3.9280
1,2,3-TRICHLOROBENZENE 0.74 0.7060 0.8040 0.7890 0.8540 0.9090 0.9050 0.9550
1,2-DICHLOROETHANE-D4 0.3140 0.3210 0.3070 0.3210 0.3250 0.3760 0.3990 0.32
TOLUENE-D8 2.5610 2.5740 2.5740 2.5230 2.3370 2.4670 2.5060 2.51
4-BROMOFLUOROBENZENE 0.81 0.8120 0.8290 0.8540 0.8110 0.8560 0.8650 0.87
CHLOROMETHANE 0.4720 0.5270 0.5350 0.5570 0.5340 0.6180
CHLOROETHANE 0.2170 0.2020 0.22 0.2090 0.2040 0.2150
TRICHLOROFLUOROMETHANE 0.2590 0.2930 0.3420 0.4560 0.4450 0.4690 0.42
METHYLENE CHLORIDE 0.4090 0.3440 0.3340 0.3190 0.3090 0.30 0.2880
File ID:0717A_04 0717A_05 0717A_06 0717A_07 0717A_08 0717A_09 0717A_10 0717A_11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF. Avg %RSD COD
Analysis date/time
DICHLORODIFLUOROMETHANE 0.254376 24.69 0.998
VINYL CHLORIDE 0.29769 27.83 0.996
BROMOMETHANE 0.167512 11.59
ACROLEIN 0.19265 10.95
1,1-DICHLOROETHENE 0.244208 15.15
1,1,2-TRICHLOROTRIFLUOROETHANE 0.221763 27.71 0.999
ACETONE 0.208496 12.71
ACRYLONITRILE 0.270116 6.63
TRANS-1,2-DICHLOROETHENE 0.297636 8.99
METHYL TERT-BUTYL ETHER 0.93626 6.06
1,1-DICHLOROETHANE 0.612377 3.51
DI-ISOPROPYL ETHER 1.432752 6.16
2,2-DICHLOROPROPANE 0.264226 11.06
CIS-1,2-DICHLOROETHENE 0.341391 6.6
2-BUTANONE (MEK)0.378345 6.02
CHLOROFORM 0.573031 3.51
1,1,1-TRICHLOROETHANE 0.440409 10.99
CARBON TETRACHLORIDE 0.436794 12.23
1,1-DICHLOROPROPENE 0.354768 18.78 1
BENZENE 1.267036 3.66
1,2-DICHLOROETHANE 0.482428 4.1
TRICHLOROETHENE 0.338581 10.16
1,2-DICHLOROPROPANE 0.254835 6.61
DIBROMOMETHANE 0.194301 10.94
BROMODICHLOROMETHANE 0.41641 3.23
CIS-1,3-DICHLOROPROPENE 0.49995 5.96
4-METHYL-2-PENTANONE (MIBK)1.832194 6.12
TOLUENE 3.405426 3.69
TRANS-1,3-DICHLOROPROPENE 1.204143 4.2
1,1,2-TRICHLOROETHANE 0.770831 5.46
TETRACHLOROETHENE 0.622672 10.83
1,3-DICHLOROPROPANE 1.297694 2.69
CHLORODIBROMOMETHANE 0.887393 5.27
1,2-DIBROMOETHANE 0.814653 1.93
CHLOROBENZENE 2.278444 2.24
1,1,1,2-TETRACHLOROETHANE 0.83652 4.68
ETHYLBENZENE 1.126467 9
M&P-XYLENE 1.349857 8.61
O-XYLENE 1.322473 11.47
STYRENE 2.24899 11.19
BROMOFORM 0.685293 1.53
ISOPROPYLBENZENE 3.047868 16.38 1
BROMOBENZENE 1.528381 6.57
1,1,2,2-TETRACHLOROETHANE 1.181404 7.73
1,2,3-TRICHLOROPROPANE 0.417852 9.33
N-PROPYLBENZENE 3.500733 11.05
2-CHLOROTOLUENE 2.507119 5.58
4-CHLOROTOLUENE 2.311288 8.17
1,3,5-TRIMETHYLBENZENE 2.460901 11.44
TERT-BUTYLBENZENE 2.06668 14.04
1,2,4-TRIMETHYLBENZENE 2.621917 11.06
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS16
Analyte RRF. Avg %RSD COD
Analysis date/time
SEC-BUTYLBENZENE 2.71428 15.59 0.999
1,3-DICHLOROBENZENE 1.678222 7.17
P-ISOPROPYLTOLUENE 2.52095 16.28 0.999
1,4-DICHLOROBENZENE 1.727261 4.61
1,2,3-TRIMETHYLBENZENE 2.713978 8.41
1,2-DICHLOROBENZENE 1.656652 6.1
N-BUTYLBENZENE 1.966112 12.99
1,2-DIBROMO-3-CHLOROPROPANE 0.38191 9.61
1,2,4-TRICHLOROBENZENE 0.825345 14.39
HEXACHLORO-1,3-BUTADIENE 0.347141 8.73
NAPHTHALENE 3.178219 18.87 0.998
1,2,3-TRICHLOROBENZENE 0.832627 10.55
1,2-DICHLOROETHANE-D4 0.335295 9.86
TOLUENE-D8 2.506546 3.11
4-BROMOFLUOROBENZENE 0.838191 3.08
CHLOROMETHANE 0.540532 8.77
CHLOROETHANE 0.211053 3.48
TRICHLOROFLUOROMETHANE 0.383533 22.1 0.997
METHYLENE CHLORIDE 0.328977 12.17
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS26
Analyte RRF: 0.04 RRF: 0.1 RRF: 0.2 RRF: 0.5 RRF: 1 RRF: 2 RRF: 5.0 RRF: 25 RRF: 75 RRF: 100
Analysis date/time 06/21/24
17:35
06/21/24
17:56
06/21/24
18:16
06/21/24
18:37
06/21/24
18:58
06/21/24
19:18
06/21/24
19:39
06/21/24
20:00
06/21/24
20:20
06/21/24
20:40
VINYL CHLORIDE 0.4060 0.4490 0.4150 0.37 0.3670 0.4070 0.4070 0.4170 0.3850 0.3850
1,1-DICHLOROETHANE 0.41 0.5330 0.5180 0.4660 0.4750 0.4840 0.5150 0.5350 0.5140 0.5140
1,2-DICHLOROETHANE-D4 0.3760 0.3740 0.3750 0.3730 0.37 0.3610 0.3580 0.3730 0.4010 0.4030
TOLUENE-D8 2.31 2.3430 2.3280 2.3410 2.2850 2.2230 2.20 2.0530 2.0090 2.0340
4-BROMOFLUOROBENZENE 0.8610 0.8830 0.8630 0.8610 0.8480 0.8290 0.8270 0.8140 0.8040 0.8110
CIS-1,2-DICHLOROETHENE 0.2660 0.2730 0.2530 0.2520 0.2780 0.2870 0.3010 0.2910 0.2930
File ID:0621_08 0621_09 0621_10 0621_11 0621_12 0621_13 0621_14 0621_15 0621_16 0621_17
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS26
Analyte RRF: 200 RRF. Avg %RSD COD
Analysis date/time 06/21/24
21:01
VINYL CHLORIDE 0.3370 0.394947 7.7
1,1-DICHLOROETHANE 0.4810 0.494917 7.44
1,2-DICHLOROETHANE-D4 0.3390 0.373112 4.81
TOLUENE-D8 1.9520 2.188859 6.8
4-BROMOFLUOROBENZENE 0.8070 0.837058 3.26
CIS-1,2-DICHLOROETHENE 0.2710 0.276581 6.02
File ID:0621_18
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/28/24 11:00
Instrument ID:VOCMS13 Calibration (end) date/time:06/28/24 14:11
Lab File ID:0628_15 Analysis date/time:06/28/24 15:35
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.700879 0.69140750 1.35 40 0.0050 0.004932 98.60
1,1,1-TRICHLOROETHANE 0.435282 0.39999170 8.11 40 0.0050 0.004595 91.90
1,1,2,2-TETRACHLOROETHANE 0.742076 0.66695340 0.30 10.10 40 0.0050 0.004494 89.90
1,1,2-TRICHLOROETHANE 0.627302 0.59398680 5.31 40 0.0050 0.004734 94.70
1,1,2-TRICHLOROTRIFLUOROETHANE 0.229233 0.212391 7.35 40 0.0050 0.004633 92.70
1,1-DICHLOROETHANE 0.529217 0.52277270 0.10 1.22 40 0.0050 0.004939 98.80
1,1-DICHLOROETHENE 0.225304 0.20748980 7.91 20.49 0.0050 0.004605 92.10
1,1-DICHLOROPROPENE 0.328448 0.350528 6.72 40 0.0050 0.005336 107
1,2,3-TRICHLOROBENZENE 0.637970 0.626591 1.78 40 0.0050 0.004457 89.10
1,2,3-TRICHLOROPROPANE 0.229206 0.223524 2.48 40 0.0050 0.004876 97.50
1,2,3-TRIMETHYLBENZENE 2.709197 2.697598 0.4280 40 0.0050 0.004979 99.60
1,2,4-TRICHLOROBENZENE 0.764183 0.77440080 1.34 40 0.0050 0.004627 92.50
1,2,4-TRIMETHYLBENZENE 2.632246 2.641568 0.3540 40 0.0050 0.005018 100
1,2-DIBROMO-3-CHLOROPROPANE 0.169172 0.15317820 9.45 40 0.0050 0.004527 90.50 58 - 134
1,2-DIBROMOETHANE 0.619217 0.61032780 1.44 40 0.0050 0.004928 98.60
1,2-DICHLOROBENZENE 1.515628 1.517228 0.1060 40 0.0050 0.005005 100
1,2-DICHLOROETHANE 0.392202 0.38221020 2.55 40 0.0050 0.004873 97.50
1,2-DICHLOROPROPANE 0.234841 0.22461890 4.35 20.49 0.0050 0.004782 95.60
1,3,5-TRIMETHYLBENZENE 2.572716 2.636637 2.48 40 0.0050 0.005124 102
1,3-DICHLOROBENZENE 1.576130 1.584631 0.5390 40 0.0050 0.005027 101
1,3-DICHLOROPROPANE 1.079068 1.051618 2.54 40 0.0050 0.004873 97.50
1,4-DICHLOROBENZENE 1.607767 1.608888 0.0697 40 0.0050 0.005003 100
2,2-DICHLOROPROPANE 0.391083 0.35561320 9.07 40 0.0050 0.004547 90.90
2-BUTANONE (MEK)0.190250 0.14339950 24.60 40 0.0250 0.01884 75.40 44 - 160
2-CHLOROTOLUENE 2.380237 2.375375 0.2040 40 0.0050 0.004990 99.80
4-CHLOROTOLUENE 2.183439 2.188635 0.2380 40 0.0050 0.005012 100
4-METHYL-2-PENTANONE (MIBK)0.858553 0.83147320 3.15 40 0.0250 0.02421 96.80 68 - 142
ACETONE 0.141098 0.09739844 31 40 0.0250 0.01726 69 19 - 160
ACROLEIN 0.059056 0.06268855 6.15 40 0.0250 0.02654 106 10 - 160
ACRYLONITRILE 0.132905 0.12181410 8.34 40 0.0250 0.02291 91.60
BENZENE 1.120314 1.110097 0.9120 40 0.0050 0.004954 99.10
BROMOBENZENE 1.310195 1.303883 0.4820 40 0.0050 0.004976 99.50
BROMODICHLOROMETHANE 0.374536 0.336644 10.10 40 0.0050 0.004494 89.90
BROMOFORM 0.543422 0.50427810 0.10 7.20 40 0.0050 0.004640 92.80
BROMOMETHANE 0.189002 0.11742810 37.90 40 0.0050 0.003107 62.10 10 - 160
CARBON TETRACHLORIDE 0.376477 0.38316370 1.78 40 0.0050 0.005089 102
CHLOROBENZENE 2.086819 2.012569 0.30 3.56 40 0.0050 0.004822 96.40
CHLORODIBROMOMETHANE 0.729268 0.71333440 2.18 40 0.0050 0.004891 97.80
CHLOROETHANE 0.219430 0.21414740 2.41 40 0.0050 0.004880 97.60 47 - 150
CHLOROFORM 0.506270 0.48110410 4.97 20.49 0.0050 0.004751 95
CHLOROMETHANE 0.654161 0.51511140 0.10 21.30 40 0.0050 0.004001 80
CIS-1,2-DICHLOROETHENE 0.282524 0.28503920 0.89 40 0.0050 0.005045 101
CIS-1,3-DICHLOROPROPENE 0.434157 0.42682280 1.69 40 0.0050 0.004916 98.30
DI-ISOPROPYL ETHER 1.231409 1.193418 3.09 40 0.0050 0.004846 96.90
DIBROMOMETHANE 0.166240 0.16705910 0.4930 40 0.0050 0.005025 101
DICHLORODIFLUOROMETHANE 0.363016 0.25355780 30.20 40 0.0050 0.003492 69.80 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/28/24 11:00
Instrument ID:VOCMS13 Calibration (end) date/time:06/28/24 14:11
Lab File ID:0628_15 Analysis date/time:06/28/24 15:35
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.093962 1.083591 0.9480 20.49 0.0050 0.004953 99.10
HEXACHLORO-1,3-BUTADIENE 0.375422 0.37256660 0.7610 40 0.0050 0.004962 99.20
ISOPROPYLBENZENE 3.320195 2.866969 13.70 40 0.0050 0.004317 86.30
M&P-XYLENE 1.358244 1.353718 0.3330 40 0.01 0.009967 99.70
METHYL TERT-BUTYL ETHER 0.756676 0.73280510 3.15 40 0.0050 0.004842 96.80
METHYLENE CHLORIDE 0.285518 0.27572190 3.43 40 0.0050 0.004828 96.60
N-BUTYLBENZENE 0.615416 0.62861910 2.15 40 0.0050 0.005107 102
N-PROPYLBENZENE 3.548029 3.604022 1.58 40 0.0050 0.005079 102
NAPHTHALENE 1.446623 1.219063 15.70 40 0.0050 0.004157 83.10 54 - 135
O-XYLENE 1.305602 1.290105 1.19 40 0.0050 0.004941 98.80
P-ISOPROPYLTOLUENE 2.767262 2.750328 0.6120 40 0.0050 0.004969 99.40
SEC-BUTYLBENZENE 3.055452 3.143414 2.88 40 0.0050 0.005144 103
STYRENE 2.142575 2.072972 3.25 40 0.0050 0.004838 96.80
TERT-BUTYLBENZENE 2.212822 2.264071 2.32 40 0.0050 0.005116 102
TETRACHLOROETHENE 0.642306 0.64030020 0.3120 40 0.0050 0.004984 99.70
TOLUENE 3.083207 3.009494 2.39 20.49 0.0050 0.004880 97.60
TRANS-1,2-DICHLOROETHENE 0.257250 0.25181810 2.11 40 0.0050 0.004894 97.90
TRANS-1,3-DICHLOROPROPENE 1.005750 0.97408170 3.15 40 0.0050 0.004843 96.90
TRICHLOROETHENE 0.304292 0.30558080 0.4240 40 0.0050 0.005021 100
TRICHLOROFLUOROMETHANE 0.420408 0.34286670 18.40 40 0.0050 0.004078 81.60
VINYL CHLORIDE 0.428873 0.37232410 13.20 20.49 0.0050 0.004341 86.80
XYLENES, TOTAL 0 1.271130 0 40 0.0150 0.014908 99.40
1,2-DICHLOROETHANE-D4 0.264575 0.27245160 2.98 40 0.0160 0.01648 103 70 - 130
4-BROMOFLUOROBENZENE 0.847362 0.87257050 2.97 40 0.0160 0.01648 103 67 - 138
TOLUENE-D8 2.343532 2.523305 7.67 40 0.0160 0.01723 108 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/28/24 11:00
Instrument ID:VOCMS13 Calibration (end) date/time:06/28/24 14:11
Lab File ID:0726_03 Analysis date/time:07/26/24 09:00
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.700879 0.63986340 8.71 0.0050 0.004565 91.30
1,1,1-TRICHLOROETHANE 0.435282 0.47566330 9.28 0.0050 0.005464 109
1,1,2,2-TETRACHLOROETHANE 0.742076 0.70763350 0.30 4.64 0.0050 0.004768 95.40
1,1,2-TRICHLOROETHANE 0.627302 0.57981860 7.57 0.0050 0.004622 92.40
1,1,2-TRICHLOROTRIFLUOROETHANE 0.229233 0.22708540 0.9370 0.0050 0.004953 99.10
1,1-DICHLOROETHANE 0.529217 0.61269920 0.10 15.80 0.0050 0.005789 116
1,1-DICHLOROETHENE 0.225304 0.24406050 8.32 20 0.0050 0.005416 108
1,1-DICHLOROPROPENE 0.328448 0.36201110 10.20 0.0050 0.005511 110
1,2,3-TRICHLOROBENZENE 0.637970 0.57049550 10.60 0.0050 0.004089 81.80
1,2,3-TRICHLOROPROPANE 0.229206 0.22480970 1.92 0.0050 0.004904 98.10
1,2,3-TRIMETHYLBENZENE 2.709197 2.6078 3.74 0.0050 0.004813 96.30
1,2,4-TRICHLOROBENZENE 0.764183 0.63734640 16.60 0.0050 0.003864 77.30
1,2,4-TRIMETHYLBENZENE 2.632246 2.487298 5.51 0.0050 0.004725 94.50
1,2-DIBROMO-3-CHLOROPROPANE 0.169172 0.10849250 35.90 0.0050 0.003207 64.10
1,2-DIBROMOETHANE 0.619217 0.55498780 10.40 0.0050 0.004481 89.60
1,2-DICHLOROBENZENE 1.515628 1.393187 8.08 0.0050 0.004596 91.90
1,2-DICHLOROETHANE 0.392202 0.45593710 16.30 0.0050 0.005813 116
1,2-DICHLOROPROPANE 0.234841 0.26298950 12 20 0.0050 0.005599 112
1,3,5-TRIMETHYLBENZENE 2.572716 2.430653 5.52 0.0050 0.004724 94.50
1,3-DICHLOROBENZENE 1.576130 1.484329 5.82 0.0050 0.004709 94.20
1,3-DICHLOROPROPANE 1.079068 0.97420870 9.72 0.0050 0.004514 90.30
1,4-DICHLOROBENZENE 1.607767 1.506851 6.28 0.0050 0.004686 93.70
2,2-DICHLOROPROPANE 0.391083 0.38734880 0.9550 0.0050 0.004952 99
2-BUTANONE (MEK)0.190250 0.15561480 18.20 0.0250 0.02045 81.80
2-CHLOROTOLUENE 2.380237 2.400647 0.8570 0.0050 0.005043 101
4-CHLOROTOLUENE 2.183439 2.146851 1.68 0.0050 0.004916 98.30
4-METHYL-2-PENTANONE (MIBK)0.858553 0.74283450 13.50 0.0250 0.02163 86.50
ACETONE 0.141098 0.10447990 26 0.0250 0.01851 74
ACROLEIN 0.059056 0.10783120 82.60 0.0250 0.04565 183
ACRYLONITRILE 0.132905 0.13684520 2.96 0.0250 0.02574 103
BENZENE 1.120314 1.186368 5.90 0.0050 0.005295 106
BROMOBENZENE 1.310195 1.316164 0.4560 0.0050 0.005023 100
BROMODICHLOROMETHANE 0.374536 0.40907570 9.22 0.0050 0.005461 109
BROMOFORM 0.543422 0.40275810 0.10 25.90 0.0050 0.003706 74.10
BROMOMETHANE 0.189002 0.06816626 63.90 0.0050 0.001803 36.10
CARBON TETRACHLORIDE 0.376477 0.43542940 15.70 0.0050 0.005783 116
CHLOROBENZENE 2.086819 1.890183 0.30 9.42 0.0050 0.004529 90.60
CHLORODIBROMOMETHANE 0.729268 0.64888040 11 0.0050 0.004449 89
CHLOROETHANE 0.219430 0.28019910 27.70 0.0050 0.006385 128
CHLOROFORM 0.506270 0.54006250 6.67 20 0.0050 0.005334 107
CHLOROMETHANE 0.654161 0.53615470 0.10 18 0.0050 0.004181 83.60
CIS-1,2-DICHLOROETHENE 0.282524 0.31421190 11.20 0.0050 0.005561 111
CIS-1,3-DICHLOROPROPENE 0.434157 0.46903580 8.03 0.0050 0.005402 108
DI-ISOPROPYL ETHER 1.231409 1.329625 7.98 0.0050 0.005399 108
DIBROMOMETHANE 0.166240 0.179208 7.80 0.0050 0.005390 108
DICHLORODIFLUOROMETHANE 0.363016 0.30731870 15.30 0.0050 0.004233 84.70
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 174 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/28/24 11:00
Instrument ID:VOCMS13 Calibration (end) date/time:06/28/24 14:11
Lab File ID:0726_03 Analysis date/time:07/26/24 09:00
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.093962 0.96153710 12.10 20 0.0050 0.004395 87.90
HEXACHLORO-1,3-BUTADIENE 0.375422 0.34228370 8.83 0.0050 0.004559 91.20
ISOPROPYLBENZENE 3.320195 2.866919 13.70 0.0050 0.004317 86.30
M&P-XYLENE 1.358244 1.205542 11.20 0.01 0.008876 88.80
METHYL TERT-BUTYL ETHER 0.756676 0.76416240 0.9890 0.0050 0.005049 101
METHYLENE CHLORIDE 0.285518 0.31958890 11.90 0.0050 0.005597 112
N-BUTYLBENZENE 0.615416 0.58458010 5.01 0.0050 0.004749 95
N-PROPYLBENZENE 3.548029 3.432193 3.26 0.0050 0.004837 96.70
NAPHTHALENE 1.446623 1.136738 21.40 0.0050 0.003935 78.70
O-XYLENE 1.305602 1.079885 17.30 0.0050 0.004136 82.70
P-ISOPROPYLTOLUENE 2.767262 2.683802 3.02 0.0050 0.004849 97
SEC-BUTYLBENZENE 3.055452 3.026766 0.9390 0.0050 0.004953 99.10
STYRENE 2.142575 1.854627 13.40 0.0050 0.004328 86.60
TERT-BUTYLBENZENE 2.212822 2.051661 7.28 0.0050 0.004636 92.70
TETRACHLOROETHENE 0.642306 0.52595590 18.10 0.0050 0.004094 81.90
TOLUENE 3.083207 2.867499 7 20 0.0050 0.004650 93
TRANS-1,2-DICHLOROETHENE 0.257250 0.28058990 9.07 0.0050 0.005454 109
TRANS-1,3-DICHLOROPROPENE 1.005750 0.95077820 5.47 0.0050 0.004727 94.50
TRICHLOROETHENE 0.304292 0.31452450 3.36 0.0050 0.005168 103
TRICHLOROFLUOROMETHANE 0.420408 0.455390 8.32 0.0050 0.005416 108
VINYL CHLORIDE 0.428873 0.44516740 3.80 20 0.0050 0.005190 104
XYLENES, TOTAL 0 1.159079 0 0.0150 0.013012 86.70
1,2-DICHLOROETHANE-D4 0.264575 0.29623440 12 0.0160 0.01791 112 70 - 130
4-BROMOFLUOROBENZENE 0.847362 0.84973850 0.28 0.0160 0.01604 100 70 - 130
TOLUENE-D8 2.343532 2.283147 2.58 0.0160 0.01559 97.40 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:07/17/24 19:39
Instrument ID:VOCMS16 Calibration (end) date/time:07/18/24 04:01
Lab File ID:0717A_15 Analysis date/time:07/17/24 23:39
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.836520 0.77258610 7.64 40 0.0050 0.004618 92.40 75 - 122
1,1,1-TRICHLOROETHANE 0.440409 0.40676680 7.64 40 0.0050 0.004618 92.40 70 - 130
1,1,2,2-TETRACHLOROETHANE 1.181404 1.184137 0.30 0.2310 40 0.0050 0.005012 100 60 - 140
1,1,2-TRICHLOROETHANE 0.770831 0.76195930 1.15 40 0.0050 0.004942 98.80 78 - 120
1,1,2-TRICHLOROTRIFLUOROETHANE 0.221763 0.22240650 0.29 40 0.0050 0.004511 90.20 61 - 136
1,1-DICHLOROETHANE 0.612377 0.60794670 0.10 0.7230 40 0.0050 0.004964 99.30 70 - 130
1,1-DICHLOROETHENE 0.244208 0.24192520 0.9350 20.49 0.0050 0.004953 99.10 50 - 150
1,1-DICHLOROPROPENE 0.354768 0.38098070 7.39 40 0.0050 0.005003 100 71 - 129
1,2,3-TRICHLOROBENZENE 0.832627 0.73257150 12 40 0.0050 0.004399 88 61 - 133
1,2,3-TRICHLOROPROPANE 0.417852 0.42185730 0.9590 40 0.0050 0.005048 101 72 - 124
1,2,3-TRIMETHYLBENZENE 2.713978 2.582133 4.86 40 0.0050 0.004757 95.10 75 - 120
1,2,4-TRICHLOROBENZENE 0.825345 0.77001010 6.70 40 0.0050 0.004665 93.30 69 - 129
1,2,4-TRIMETHYLBENZENE 2.621917 2.457874 6.26 40 0.0050 0.004687 93.70 75 - 120
1,2-DIBROMO-3-CHLOROPROPANE 0.381910 0.37386470 2.11 40 0.0050 0.004895 97.90 58 - 134
1,2-DIBROMOETHANE 0.814653 0.82411160 1.16 40 0.0050 0.005058 101 77 - 123
1,2-DICHLOROBENZENE 1.656652 1.561215 5.76 40 0.0050 0.004712 94.20 65 - 135
1,2-DICHLOROETHANE 0.482428 0.45652420 5.37 40 0.0050 0.004732 94.60 70 - 130
1,2-DICHLOROPROPANE 0.254835 0.25192850 1.14 20.49 0.0050 0.004943 98.90 35 - 165
1,3,5-TRIMETHYLBENZENE 2.460901 2.462521 0.0658 40 0.0050 0.005003 100 75 - 120
1,3-DICHLOROBENZENE 1.678222 1.593485 5.05 40 0.0050 0.004748 95 70 - 130
1,3-DICHLOROPROPANE 1.297694 1.315276 1.35 40 0.0050 0.005068 101 80 - 121
1,4-DICHLOROBENZENE 1.727261 1.639827 5.06 40 0.0050 0.004747 94.90 65 - 135
2,2-DICHLOROPROPANE 0.264226 0.27324660 3.41 40 0.0050 0.005171 103 60 - 125
2-BUTANONE (MEK)0.378345 0.342105 9.58 40 0.0250 0.02261 90.40 44 - 160
2-CHLOROTOLUENE 2.507119 2.431250 3.03 40 0.0050 0.004849 97 74 - 122
4-CHLOROTOLUENE 2.311288 2.287272 1.04 40 0.0050 0.004948 99 79 - 120
4-METHYL-2-PENTANONE (MIBK)1.832194 1.768455 3.48 40 0.0250 0.02413 96.50 68 - 142
ACETONE 0.208496 0.18963640 9.05 40 0.0250 0.02274 91 19 - 160
ACRYLONITRILE 0.270116 0.26446020 2.09 40 0.0250 0.02448 97.90 60 - 140
BENZENE 1.267036 1.238523 2.25 40 0.0050 0.004887 97.70 65 - 135
BROMOBENZENE 1.528381 1.486685 2.73 40 0.0050 0.004864 97.30 79 - 120
BROMODICHLOROMETHANE 0.416410 0.373829 10.20 40 0.0050 0.004489 89.80 65 - 135
BROMOFORM 0.685293 0.65319260 0.10 4.68 40 0.0050 0.004766 95.30 70 - 130
BROMOMETHANE 0.167512 0.19912130 18.90 40 0.0050 0.005943 119 10 - 160
CARBON TETRACHLORIDE 0.436794 0.40545540 7.17 40 0.0050 0.004641 92.80 70 - 130
CHLOROBENZENE 2.278444 2.230584 0.30 2.10 40 0.0050 0.004895 97.90 65 - 135
CHLORODIBROMOMETHANE 0.887393 0.84354480 4.94 40 0.0050 0.004753 95.10 70 - 135
CHLOROETHANE 0.211053 0.19280820 8.64 40 0.0050 0.004568 91.40 47 - 150
CHLOROFORM 0.573031 0.54263530 5.30 20.49 0.0050 0.004735 94.70 70 - 130
CHLOROMETHANE 0.540532 0.43438270 0.10 19.60 40 0.0050 0.004018 80.40 0.0010 -
205
CIS-1,2-DICHLOROETHENE 0.341391 0.34523710 1.13 40 0.0050 0.005056 101 73 - 120
CIS-1,3-DICHLOROPROPENE 0.499950 0.47799480 4.39 40 0.0050 0.004780 95.60 25 - 175
DI-ISOPROPYL ETHER 1.432752 1.370076 4.37 40 0.0050 0.004781 95.60 59 - 133
DIBROMOMETHANE 0.194301 0.18940770 2.52 40 0.0050 0.004874 97.50 78 - 120
DICHLORODIFLUOROMETHANE 0.254376 0.28111510 10.50 40 0.0050 0.004757 95.10 51 - 149
ETHYLBENZENE 1.126467 1.117176 0.8250 20.49 0.0050 0.004959 99.20 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 176 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:07/17/24 19:39
Instrument ID:VOCMS16 Calibration (end) date/time:07/18/24 04:01
Lab File ID:0717A_15 Analysis date/time:07/17/24 23:39
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
HEXACHLORO-1,3-BUTADIENE 0.347141 0.33368990 3.87 40 0.0050 0.004806 96.10 64 - 131
ISOPROPYLBENZENE 3.047868 2.608791 14.40 40 0.0050 0.004047 80.90 75 - 120
M&P-XYLENE 1.349857 1.339367 0.7770 40 0.01 0.009922 99.20 77 - 120
METHYL TERT-BUTYL ETHER 0.936260 0.95781950 2.30 40 0.0050 0.005115 102 64 - 123
METHYLENE CHLORIDE 0.328977 0.327411 0.4760 40 0.0050 0.004976 99.50 60 - 140
N-BUTYLBENZENE 1.966112 1.849301 5.94 40 0.0050 0.004703 94.10 72 - 126
N-PROPYLBENZENE 3.500733 3.404392 2.75 40 0.0050 0.004862 97.20 79 - 120
NAPHTHALENE 3.178219 2.653492 16.50 40 0.0050 0.003830 76.60 54 - 135
O-XYLENE 1.322473 1.352195 2.25 40 0.0050 0.005112 102 78 - 120
P-ISOPROPYLTOLUENE 2.520950 2.304601 8.58 40 0.0050 0.004344 86.90 74 - 126
SEC-BUTYLBENZENE 2.714280 2.653406 2.24 40 0.0050 0.004638 92.80 74 - 121
STYRENE 2.248990 2.154799 4.19 40 0.0050 0.004791 95.80 78 - 124
TERT-BUTYLBENZENE 2.066680 1.985374 3.93 40 0.0050 0.004803 96.10 75 - 122
TETRACHLOROETHENE 0.622672 0.62910220 1.03 40 0.0050 0.005052 101 70 - 130
TOLUENE 3.405426 3.342129 1.86 20.49 0.0050 0.004907 98.10 70 - 130
TRANS-1,2-DICHLOROETHENE 0.297636 0.29200290 1.89 40 0.0050 0.004905 98.10 70 - 130
TRANS-1,3-DICHLOROPROPENE 1.204143 1.199566 0.38 40 0.0050 0.004981 99.60 50 - 150
TRICHLOROETHENE 0.338581 0.32004580 5.47 40 0.0050 0.004726 94.50 65 - 135
TRICHLOROFLUOROMETHANE 0.383533 0.32600810 15 40 0.0050 0.004212 84.20 50 - 150
VINYL CHLORIDE 0.297690 0.29965790 0.6610 20.49 0.0050 0.004381 87.60 5 - 195
XYLENES, TOTAL 0 1.378365 0 40 0.0150 0.015034 100 77 - 120
1,2-DICHLOROETHANE-D4 0.335295 0.30307360 9.61 40 0.0160 0.01446 90.40 70 - 130
4-BROMOFLUOROBENZENE 0.838191 0.86250690 2.90 40 0.0160 0.01646 103 67 - 138
TOLUENE-D8 2.506546 2.577757 2.84 40 0.0160 0.01645 103 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 177 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:07/17/24 19:39
Instrument ID:VOCMS16 Calibration (end) date/time:07/18/24 04:01
Lab File ID:0717A_17 Analysis date/time:07/18/24 00:23
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ACROLEIN 0.192650 0.11521660 40.20 20 0.0250 0.01495 59.80 10 - 160
1,2-DICHLOROETHANE-D4 0.335295 0.30437530 9.22 40 0.0160 0.01452 90.80 70 - 130
4-BROMOFLUOROBENZENE 0.838191 0.82766520 1.26 40 0.0160 0.01580 98.70 67 - 138
TOLUENE-D8 2.506546 2.529262 0.9060 40 0.0160 0.01615 101 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 178 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:07/17/24 19:39
Instrument ID:VOCMS16 Calibration (end) date/time:07/18/24 04:01
Lab File ID:0725_45 Analysis date/time:07/25/24 21:45
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.836520 0.72124310 13.80 0.0050 0.004311 86.20
1,1,1-TRICHLOROETHANE 0.440409 0.47138490 7.03 0.0050 0.005352 107
1,1,2,2-TETRACHLOROETHANE 1.181404 1.088707 0.30 7.85 0.0050 0.004608 92.20
1,1,2-TRICHLOROETHANE 0.770831 0.70592670 8.42 0.0050 0.004579 91.60
1,1,2-TRICHLOROTRIFLUOROETHANE 0.221763 0.25528890 15.10 0.0050 0.005123 102
1,1-DICHLOROETHANE 0.612377 0.58059880 0.10 5.19 0.0050 0.004741 94.80
1,1-DICHLOROETHENE 0.244208 0.24891360 1.93 20 0.0050 0.005096 102
1,1-DICHLOROPROPENE 0.354768 0.33902310 4.44 0.0050 0.004479 89.60
1,2,3-TRICHLOROBENZENE 0.832627 0.61394220 26.30 0.0050 0.003687 73.70
1,2,3-TRICHLOROPROPANE 0.417852 0.41902450 0.2810 0.0050 0.005014 100
1,2,3-TRIMETHYLBENZENE 2.713978 2.234472 17.70 0.0050 0.004117 82.30
1,2,4-TRICHLOROBENZENE 0.825345 0.611247 25.90 0.0050 0.003703 74.10
1,2,4-TRIMETHYLBENZENE 2.621917 2.201728 16 0.0050 0.004199 84
1,2-DIBROMO-3-CHLOROPROPANE 0.381910 0.31626110 17.20 0.0050 0.004141 82.80
1,2-DIBROMOETHANE 0.814653 0.72490820 11 0.0050 0.004449 89
1,2-DICHLOROBENZENE 1.656652 1.458528 12 0.0050 0.004402 88
1,2-DICHLOROETHANE 0.482428 0.45891250 4.87 0.0050 0.004756 95.10
1,2-DICHLOROPROPANE 0.254835 0.24504140 3.84 20 0.0050 0.004808 96.20
1,3,5-TRIMETHYLBENZENE 2.460901 2.192782 10.90 0.0050 0.004455 89.10
1,3-DICHLOROBENZENE 1.678222 1.564044 6.80 0.0050 0.004660 93.20
1,3-DICHLOROPROPANE 1.297694 1.165531 10.20 0.0050 0.004491 89.80
1,4-DICHLOROBENZENE 1.727261 1.540877 10.80 0.0050 0.004460 89.20
2,2-DICHLOROPROPANE 0.264226 0.23960750 9.32 0.0050 0.004534 90.70
2-BUTANONE (MEK)0.378345 0.36521740 3.47 0.0250 0.02413 96.50
2-CHLOROTOLUENE 2.507119 2.220193 11.40 0.0050 0.004428 88.60
4-CHLOROTOLUENE 2.311288 2.020688 12.60 0.0050 0.004371 87.40
4-METHYL-2-PENTANONE (MIBK)1.832194 1.719540 6.15 0.0250 0.02346 93.80
ACETONE 0.208496 0.20096220 3.61 0.0250 0.02410 96.40
ACROLEIN 0.192650 0.165312 14.20 0.0250 0.02145 85.80
ACRYLONITRILE 0.270116 0.26252840 2.81 0.0250 0.02430 97.20
BENZENE 1.267036 1.166589 7.93 0.0050 0.004604 92.10
BROMOBENZENE 1.528381 1.333802 12.70 0.0050 0.004363 87.30
BROMODICHLOROMETHANE 0.416410 0.38643120 7.20 0.0050 0.004640 92.80
BROMOFORM 0.685293 0.58344930 0.10 14.90 0.0050 0.004257 85.10
BROMOMETHANE 0.167512 0.15788420 5.75 0.0050 0.004713 94.30
CARBON TETRACHLORIDE 0.436794 0.46466730 6.38 0.0050 0.005319 106
CHLOROBENZENE 2.278444 2.077137 0.30 8.84 0.0050 0.004558 91.20
CHLORODIBROMOMETHANE 0.887393 0.82627060 6.89 0.0050 0.004656 93.10
CHLOROETHANE 0.211053 0.20199760 4.29 0.0050 0.004785 95.70
CHLOROFORM 0.573031 0.52625930 8.16 20 0.0050 0.004592 91.80
CHLOROMETHANE 0.540532 0.61144820 0.10 13.10 0.0050 0.005656 113
CIS-1,2-DICHLOROETHENE 0.341391 0.32019680 6.21 0.0050 0.004690 93.80
CIS-1,3-DICHLOROPROPENE 0.499950 0.44586240 10.80 0.0050 0.004459 89.20
DI-ISOPROPYL ETHER 1.432752 1.342914 6.27 0.0050 0.004686 93.70
DIBROMOMETHANE 0.194301 0.19611440 0.9330 0.0050 0.005047 101
DICHLORODIFLUOROMETHANE 0.254376 0.34009280 33.70 0.0050 0.005689 114
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 179 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:07/17/24 19:39
Instrument ID:VOCMS16 Calibration (end) date/time:07/18/24 04:01
Lab File ID:0725_45 Analysis date/time:07/25/24 21:45
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 1.126467 0.96745590 14.10 20 0.0050 0.004294 85.90
HEXACHLORO-1,3-BUTADIENE 0.347141 0.28426220 18.10 0.0050 0.004094 81.90
ISOPROPYLBENZENE 3.047868 2.603641 14.60 0.0050 0.004039 80.80
M&P-XYLENE 1.349857 1.199638 11.10 0.01 0.008887 88.90
METHYL TERT-BUTYL ETHER 0.936260 0.85841510 8.31 0.0050 0.004584 91.70
METHYLENE CHLORIDE 0.328977 0.29929540 9.02 0.0050 0.004549 91
N-BUTYLBENZENE 1.966112 1.605620 18.30 0.0050 0.004083 81.70
N-PROPYLBENZENE 3.500733 3.060650 12.60 0.0050 0.004371 87.40
NAPHTHALENE 3.178219 2.161299 32 0.0050 0.003186 63.70
O-XYLENE 1.322473 1.095349 17.20 0.0050 0.004141 82.80
P-ISOPROPYLTOLUENE 2.520950 2.155851 14.50 0.0050 0.004076 81.50
SEC-BUTYLBENZENE 2.714280 2.342913 13.70 0.0050 0.004118 82.40
STYRENE 2.248990 1.931903 14.10 0.0050 0.004295 85.90
TERT-BUTYLBENZENE 2.066680 1.762231 14.70 0.0050 0.004263 85.30
TETRACHLOROETHENE 0.622672 0.62020890 0.3960 0.0050 0.004980 99.60
TOLUENE 3.405426 3.019649 11.30 20 0.0050 0.004434 88.70
TRANS-1,2-DICHLOROETHENE 0.297636 0.27815860 6.54 0.0050 0.004673 93.50
TRANS-1,3-DICHLOROPROPENE 1.204143 1.134187 5.81 0.0050 0.004710 94.20
TRICHLOROETHENE 0.338581 0.32492480 4.03 0.0050 0.004798 96
TRICHLOROFLUOROMETHANE 0.383533 0.41011380 6.93 0.0050 0.005166 103
VINYL CHLORIDE 0.297690 0.33386730 12.20 20 0.0050 0.004827 96.50 80 - 120
XYLENES, TOTAL 0 1.221175 0 0.0150 0.013028 86.90
1,2-DICHLOROETHANE-D4 0.335295 0.32149110 4.12 0.0160 0.01534 95.90 70 - 130
4-BROMOFLUOROBENZENE 0.838191 0.78331260 6.55 0.0160 0.01495 93.40 70 - 130
TOLUENE-D8 2.506546 2.414417 3.68 0.0160 0.01541 96.30 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 180 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/21/24 17:35
Instrument ID:VOCMS26 Calibration (end) date/time:06/21/24 21:42
Lab File ID:0621_22 Analysis date/time:06/21/24 22:23
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.558987 0.57332460 2.56 40 0.0050 0.005128 103
1,1,1-TRICHLOROETHANE 0.421560 0.397856 5.62 40 0.0050 0.004719 94.40
1,1,2,2-TETRACHLOROETHANE 0.819101 0.82393310 0.30 0.59 40 0.0050 0.005029 101
1,1,2-TRICHLOROETHANE 0.520686 0.52788680 1.38 40 0.0050 0.005069 101
1,1,2-TRICHLOROTRIFLUOROETHANE 0.257149 0.22887170 11 40 0.0050 0.004450 89
1,1-DICHLOROETHANE 0.494917 0.51654030 0.10 4.37 40 0.0050 0.005218 104
1,1-DICHLOROETHENE 0.221665 0.20161010 9.05 20.49 0.0050 0.004548 91
1,1-DICHLOROPROPENE 0.330872 0.35056490 5.95 40 0.0050 0.005298 106
1,2,3-TRICHLOROBENZENE 0.221629 0.21400810 3.44 40 0.0050 0.004505 90.10
1,2,3-TRICHLOROPROPANE 0.250142 0.27503990 9.95 40 0.0050 0.005498 110
1,2,3-TRIMETHYLBENZENE 2.190395 2.176890 0.6170 40 0.0050 0.004969 99.40
1,2,4-TRICHLOROBENZENE 0.368765 0.37107340 0.6260 40 0.0050 0.004555 91.10
1,2,4-TRIMETHYLBENZENE 2.184704 2.206051 0.9770 40 0.0050 0.005049 101
1,2-DIBROMO-3-CHLOROPROPANE 0.190730 0.18124250 4.97 40 0.0050 0.004751 95 58 - 134
1,2-DIBROMOETHANE 0.5731 0.58716550 2.45 40 0.0050 0.005123 102
1,2-DICHLOROBENZENE 1.051311 1.113175 5.88 40 0.0050 0.005294 106
1,2-DICHLOROETHANE 0.445499 0.41963360 5.81 40 0.0050 0.004710 94.20
1,2-DICHLOROPROPANE 0.203665 0.20479690 0.5560 20.49 0.0050 0.005028 101
1,3,5-TRIMETHYLBENZENE 2.209450 2.183881 1.16 40 0.0050 0.004942 98.80
1,3-DICHLOROBENZENE 1.176881 1.200611 2.02 40 0.0050 0.005101 102
1,3-DICHLOROPROPANE 0.887882 0.909673 2.45 40 0.0050 0.005123 102
1,4-DICHLOROBENZENE 1.250137 1.219458 2.45 40 0.0050 0.004877 97.50
2,2-DICHLOROPROPANE 0.389103 0.35391410 9.04 40 0.0050 0.004548 91
2-BUTANONE (MEK)0.238018 0.22911770 3.74 40 0.0250 0.02407 96.30 44 - 160
2-CHLOROTOLUENE 2.012824 1.972128 2.02 40 0.0050 0.004899 98
4-CHLOROTOLUENE 1.870712 1.891044 1.09 40 0.0050 0.005054 101
4-METHYL-2-PENTANONE (MIBK)0.985641 1.100489 11.70 40 0.0250 0.02791 112 68 - 142
ACETONE 0.147133 0.15015060 2.05 40 0.0250 0.02551 102 19 - 160
ACROLEIN 0.068268 0.07791361 14.10 40 0.0250 0.02853 114 10 - 160
ACRYLONITRILE 0.178896 0.17059080 4.64 40 0.0250 0.02384 95.40
BENZENE 1.018125 0.99030660 2.73 40 0.0050 0.004863 97.30
BROMOBENZENE 1.186369 1.093470 7.83 40 0.0050 0.004608 92.20
BROMODICHLOROMETHANE 0.363722 0.34196750 5.98 40 0.0050 0.004701 94
BROMOFORM 0.494288 0.47197740 0.10 4.51 40 0.0050 0.004774 95.50
BROMOMETHANE 0.188872 0.09257511 51 40 0.0050 0.002451 49 10 - 160
CARBON TETRACHLORIDE 0.417708 0.39165260 6.24 40 0.0050 0.004688 93.80
CHLOROBENZENE 1.605724 1.581798 0.30 1.49 40 0.0050 0.004925 98.50
CHLORODIBROMOMETHANE 0.616446 0.64521430 4.67 40 0.0050 0.005233 105
CHLOROETHANE 0.235642 0.20431340 13.30 40 0.0050 0.004335 86.70 47 - 150
CHLOROFORM 0.488843 0.47920780 1.97 20.49 0.0050 0.004901 98
CHLOROMETHANE 0.395221 0.33860670 0.10 14.30 40 0.0050 0.004284 85.70
CIS-1,2-DICHLOROETHENE 0.276581 0.27670430 0.0446 40 0.0050 0.005002 100
CIS-1,3-DICHLOROPROPENE 0.414653 0.42263870 1.93 40 0.0050 0.005096 102
DI-ISOPROPYL ETHER 0.982869 0.960856 2.24 40 0.0050 0.004888 97.80
DIBROMOMETHANE 0.183202 0.17809990 2.78 40 0.0050 0.004861 97.20
DICHLORODIFLUOROMETHANE 0.297929 0.27861870 6.48 40 0.0050 0.004676 93.50 51 - 149
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 181 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/21/24 17:35
Instrument ID:VOCMS26 Calibration (end) date/time:06/21/24 21:42
Lab File ID:0621_22 Analysis date/time:06/21/24 22:23
Analytical Method:8260B Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.858036 0.88844380 3.54 20.49 0.0050 0.005177 104
HEXACHLORO-1,3-BUTADIENE 0.217036 0.23285520 7.29 40 0.0050 0.005364 107
ISOPROPYLBENZENE 2.555342 2.382025 6.78 40 0.0050 0.004661 93.20
M&P-XYLENE 1.054936 1.071078 1.53 40 0.01 0.01015 102
METHYL TERT-BUTYL ETHER 0.773824 0.77008250 0.4840 40 0.0050 0.004976 99.50
METHYLENE CHLORIDE 0.278306 0.25806320 7.27 40 0.0050 0.004636 92.70
N-BUTYLBENZENE 0.468170 0.48019490 2.57 40 0.0050 0.005128 103
N-PROPYLBENZENE 3.164886 3.255492 2.86 40 0.0050 0.005143 103
NAPHTHALENE 0.822392 0.84078150 2.24 40 0.0050 0.004348 87 54 - 135
O-XYLENE 0.985199 0.998028 1.30 40 0.0050 0.005065 101
P-ISOPROPYLTOLUENE 2.183617 2.236124 2.40 40 0.0050 0.005120 102
SEC-BUTYLBENZENE 2.537728 2.641852 4.10 40 0.0050 0.005205 104
STYRENE 1.556508 1.624317 4.36 40 0.0050 0.005218 104
TERT-BUTYLBENZENE 1.838936 1.938486 5.41 40 0.0050 0.005271 105
TETRACHLOROETHENE 0.499348 0.58531190 17.20 40 0.0050 0.005861 117
TOLUENE 2.421440 2.382779 1.60 20.49 0.0050 0.004920 98.40
TRANS-1,2-DICHLOROETHENE 0.247841 0.23650220 4.58 40 0.0050 0.004771 95.40
TRANS-1,3-DICHLOROPROPENE 0.852610 0.88347230 3.62 40 0.0050 0.005181 104
TRICHLOROETHENE 0.277705 0.27970550 0.72 40 0.0050 0.005036 101
TRICHLOROFLUOROMETHANE 0.465155 0.39879190 14.30 40 0.0050 0.004287 85.70
VINYL CHLORIDE 0.394947 0.34909140 11.60 20.49 0.0050 0.004419 88.40
XYLENES, TOTAL 0 1.102986 0 40 0.0150 0.015215 101
1,2-DICHLOROETHANE-D4 0.373112 0.366790 1.69 40 0.0160 0.01573 98.30 70 - 130
4-BROMOFLUOROBENZENE 0.837058 0.857444 2.44 40 0.0160 0.01639 102 67 - 138
TOLUENE-D8 2.188859 2.318426 5.92 40 0.0160 0.01695 106 75 - 131
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 182 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/21/24 17:35
Instrument ID:VOCMS26 Calibration (end) date/time:06/21/24 21:42
Lab File ID:0729A_01 Analysis date/time:07/29/24 19:18
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
1,1,1,2-TETRACHLOROETHANE 0.558987 0.54619870 2.29 0.0050 0.004886 97.70
1,1,1-TRICHLOROETHANE 0.421560 0.41122220 2.45 0.0050 0.004877 97.50
1,1,2,2-TETRACHLOROETHANE 0.819101 0.59493510 0.30 27.40 0.0050 0.003632 72.60
1,1,2-TRICHLOROETHANE 0.520686 0.47701590 8.39 0.0050 0.004581 91.60
1,1,2-TRICHLOROTRIFLUOROETHANE 0.257149 0.23119710 10.10 0.0050 0.004495 89.90
1,1-DICHLOROETHANE 0.494917 0.48115440 0.10 2.78 0.0050 0.004861 97.20
1,1-DICHLOROETHENE 0.221665 0.21133180 4.66 20 0.0050 0.004767 95.30
1,1-DICHLOROPROPENE 0.330872 0.30535120 7.71 0.0050 0.004614 92.30
1,2,3-TRICHLOROBENZENE 0.221629 0.31148310 40.50 0.0050 0.006464 129
1,2,3-TRICHLOROPROPANE 0.250142 0.226461 9.47 0.0050 0.004527 90.50
1,2,3-TRIMETHYLBENZENE 2.190395 1.726117 21.20 0.0050 0.003940 78.80
1,2,4-TRICHLOROBENZENE 0.368765 0.37480090 1.64 0.0050 0.004598 92
1,2,4-TRIMETHYLBENZENE 2.184704 1.708406 21.80 0.0050 0.003910 78.20
1,2-DIBROMO-3-CHLOROPROPANE 0.190730 0.16535410 13.30 0.0050 0.004335 86.70
1,2-DIBROMOETHANE 0.5731 0.53116960 7.32 0.0050 0.004634 92.70
1,2-DICHLOROBENZENE 1.051311 0.93168910 11.40 0.0050 0.004431 88.60
1,2-DICHLOROETHANE 0.445499 0.39964850 10.30 0.0050 0.004485 89.70
1,2-DICHLOROPROPANE 0.203665 0.20242490 0.6090 20 0.0050 0.004970 99.40
1,3,5-TRIMETHYLBENZENE 2.209450 1.671129 24.40 0.0050 0.003782 75.60
1,3-DICHLOROBENZENE 1.176881 0.99548320 15.40 0.0050 0.004229 84.60
1,3-DICHLOROPROPANE 0.887882 0.78650230 11.40 0.0050 0.004429 88.60
1,4-DICHLOROBENZENE 1.250137 1.006158 19.50 0.0050 0.004024 80.50
2,2-DICHLOROPROPANE 0.389103 0.29159370 25.10 0.0050 0.003747 74.90
2-BUTANONE (MEK)0.238018 0.27728430 16.50 0.0250 0.02912 116
2-CHLOROTOLUENE 2.012824 1.522655 24.40 0.0050 0.003782 75.60
4-CHLOROTOLUENE 1.870712 1.412911 24.50 0.0050 0.003776 75.50
4-METHYL-2-PENTANONE (MIBK)0.985641 1.057203 7.26 0.0250 0.02682 107
ACETONE 0.147133 0.179734 22.20 0.0250 0.03054 122
ACROLEIN 0.068268 0.14051290 106 0.0250 0.05146 206
ACRYLONITRILE 0.178896 0.20598630 15.10 0.0250 0.02879 115
BENZENE 1.018125 0.93131980 8.53 0.0050 0.004574 91.50
BROMOBENZENE 1.186369 0.85880770 27.60 0.0050 0.003619 72.40
BROMODICHLOROMETHANE 0.363722 0.349661 3.87 0.0050 0.004807 96.10
BROMOFORM 0.494288 0.47354660 0.10 4.20 0.0050 0.004790 95.80
BROMOMETHANE 0.188872 0.14681260 22.30 0.0050 0.003887 77.70
CARBON TETRACHLORIDE 0.417708 0.41914320 0.3440 0.0050 0.005017 100
CHLOROBENZENE 1.605724 1.421927 0.30 11.40 0.0050 0.004428 88.60
CHLORODIBROMOMETHANE 0.616446 0.59653070 3.23 0.0050 0.004838 96.80
CHLOROETHANE 0.235642 0.18696670 20.70 0.0050 0.003967 79.30
CHLOROFORM 0.488843 0.47115560 3.62 20 0.0050 0.004819 96.40
CHLOROMETHANE 0.395221 0.43143820 0.10 9.16 0.0050 0.005458 109
CIS-1,2-DICHLOROETHENE 0.276581 0.26500520 4.19 0.0050 0.004791 95.80
CIS-1,3-DICHLOROPROPENE 0.414653 0.38452780 7.27 0.0050 0.004637 92.70
DI-ISOPROPYL ETHER 0.982869 0.97227460 1.08 0.0050 0.004946 98.90
DIBROMOMETHANE 0.183202 0.18028320 1.59 0.0050 0.004920 98.40
DICHLORODIFLUOROMETHANE 0.297929 0.34762950 16.70 0.0050 0.005834 117
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 183 of 210
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1758896 Calibration (begin) date/time:06/21/24 17:35
Instrument ID:VOCMS26 Calibration (end) date/time:06/21/24 21:42
Lab File ID:0729A_01 Analysis date/time:07/29/24 19:18
Analytical Method:8260B Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%mg/l mg/l % Rec.%
ETHYLBENZENE 0.858036 0.74946480 12.70 20 0.0050 0.004367 87.30
HEXACHLORO-1,3-BUTADIENE 0.217036 0.21634780 0.3170 0.0050 0.004984 99.70
ISOPROPYLBENZENE 2.555342 2.241279 12.30 0.0050 0.004385 87.70
M&P-XYLENE 1.054936 0.89909890 14.80 0.01 0.008523 85.20
METHYL TERT-BUTYL ETHER 0.773824 0.72889490 5.81 0.0050 0.004710 94.20
METHYLENE CHLORIDE 0.278306 0.25323950 9.01 0.0050 0.004550 91
N-BUTYLBENZENE 0.468170 0.36369830 22.30 0.0050 0.003884 77.70
N-PROPYLBENZENE 3.164886 2.365645 25.30 0.0050 0.003737 74.70
NAPHTHALENE 0.822392 0.89916310 9.34 0.0050 0.004619 92.40
O-XYLENE 0.985199 0.84474870 14.30 0.0050 0.004287 85.70
P-ISOPROPYLTOLUENE 2.183617 1.825392 16.40 0.0050 0.004180 83.60
SEC-BUTYLBENZENE 2.537728 2.000176 21.20 0.0050 0.003941 78.80
STYRENE 1.556508 1.421588 8.67 0.0050 0.004567 91.30
TERT-BUTYLBENZENE 1.838936 1.469682 20.10 0.0050 0.003996 79.90
TETRACHLOROETHENE 0.499348 0.46769210 6.34 0.0050 0.004683 93.70
TOLUENE 2.421440 2.070647 14.50 20 0.0050 0.004276 85.50
TRANS-1,2-DICHLOROETHENE 0.247841 0.23543880 5 0.0050 0.004750 95
TRANS-1,3-DICHLOROPROPENE 0.852610 0.74016810 13.20 0.0050 0.004341 86.80
TRICHLOROETHENE 0.277705 0.301480 8.56 0.0050 0.005428 109
TRICHLOROFLUOROMETHANE 0.465155 0.46250670 0.5690 0.0050 0.004972 99.40
VINYL CHLORIDE 0.394947 0.35342630 10.50 20 0.0050 0.004474 89.50
XYLENES, TOTAL 0 0.794008 0 0.0150 0.01281 85.40
1,2-DICHLOROETHANE-D4 0.373112 0.36237870 2.88 0.0160 0.01554 97.10 70 - 130
4-BROMOFLUOROBENZENE 0.837058 0.90071060 7.60 0.0160 0.01722 108 70 - 130
TOLUENE-D8 2.188859 2.175405 0.6150 0.0160 0.01590 99.40 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 184 of 210
8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS13 Calibration Start Date:06/28/24 11:00
Calibration End Date:06/28/24 14:11
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS130628240628_01735103 0628_01 06/28/24 10:39
CAL .05A 0628_02 06/28/24 11:00
CAL 0.1A 0628_02 06/28/24 11:00
CAL 0.2A 0628_02 06/28/24 11:00
CAL 0.5A 0628_02 06/28/24 11:00
CAL 1A 0628_02 06/28/24 11:00
CAL 5A 0628_02 06/28/24 11:00
CAL 10A 0628_02 06/28/24 11:00
CAL 15A 0628_02 06/28/24 11:00
CAL 20A 0628_02 06/28/24 11:00
CAL 0.5 0628_04 06/28/24 11:42
CAL 1 0628_05 06/28/24 12:03
CAL 2 0628_06 06/28/24 12:25
CAL 5.0 0628_07 06/28/24 12:46
CAL 25 0628_08 06/28/24 13:07
CAL 75 0628_09 06/28/24 13:28
CAL 100 0628_10 06/28/24 13:50
CAL 200 0628_11 06/28/24 14:11
SSCV VOCMS130628240628_15735103 0628_15 06/28/24 15:35
SSCV VOCMS130628240628_16735103 0628_16 06/28/24 15:56
TUNE VOCMS130726240726_01T735103 0726_01T 07/26/24 08:18
ICV VOCMS130726240726_03735103 0726_03 07/26/24 09:00
LCS R4099344-1 0726_03LCS 07/26/24 09:00 1 WG2330260
BLANK R4099344-2 0726_05 07/26/24 09:41 1 WG2330260
L1758894-14 L1758894-14 0726_09 07/26/24 11:50 1 WG2330260
MW-1 L1758896-01 0726_10 07/26/24 12:11 1 WG2330260
MW-25 L1758896-02 0726_11 07/26/24 12:32 1 WG2330260
MW-2 L1758896-03 0726_12 07/26/24 12:53 1 WG2330260
MW-4 L1758896-04 0726_13 07/26/24 13:13 1 WG2330260
MW-8 L1758896-05 0726_14 07/26/24 13:34 1 WG2330260
MW-3 L1758896-06 0726_15 07/26/24 13:55 1 WG2330260
MW-7 L1758896-07 0726_16 07/26/24 14:16 1 WG2330260
MW-5 L1758896-08 0726_17 07/26/24 14:37 1 WG2330260
MW-10 L1758896-09 0726_18 07/26/24 14:58 1 WG2330260
MS R4099344-3 0726_26 07/26/24 17:45 1 WG2330260
MSD R4099344-4 0726_27 07/26/24 18:06 1 WG2330260
TUNE VOCMS130726240726_28T735103 0726_28T 07/26/24 18:27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 185 of 210
8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS16 Calibration Start Date:07/17/24 19:39
Calibration End Date:07/18/24 04:01
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS16071724A0717A_01739536 0717A_01 07/17/24 18:33
TUNE VOCMS16071724A0717A_03739536 0717A_03 07/17/24 19:17
CAL 0.5 0717A_04 07/17/24 19:39
CAL 1 0717A_05 07/17/24 20:00
CAL 2 0717A_06 07/17/24 20:23
CAL 5.0 0717A_07 07/17/24 20:44
CAL 25 0717A_08 07/17/24 21:06
CAL 75 0717A_09 07/17/24 21:28
CAL 100 0717A_10 07/17/24 21:50
CAL 200 0717A_11 07/17/24 22:11
SSCV VOCMS16071724A0717A_15739536 0717A_15 07/17/24 23:39
SSCV VOCMS16071724A0717A_17739536 0717A_17 07/18/24 00:23
CAL .05A 0717A_19 07/18/24 01:06
CAL 0.1A 0717A_20 07/18/24 01:28
CAL 0.2A 0717A_21 07/18/24 01:51
CAL 0.5A 0717A_22 07/18/24 02:12
CAL 1A 0717A_23 07/18/24 02:34
CAL 5A 0717A_24 07/18/24 02:56
CAL 10A 0717A_25 07/18/24 03:18
CAL 15A 0717A_26 07/18/24 03:40
CAL 20A 0717A_27 07/18/24 04:01
TUNE VOCMS160725240725_01T739536 0725_01T 07/25/24 04:59
TUNE VOCMS160725240725_13T739536 0725_13T 07/25/24 09:28
TUNE VOCMS160725240725_43T739536 0725_43T 07/25/24 21:01
TUNE VOCMS160725240725_44T739536 0725_44T 07/25/24 21:23
ICV VOCMS160725240725_45739536 0725_45 07/25/24 21:45
LCS R4098892-1 0725_45LCSA 07/25/24 21:45 1 WG2329432
LCS R4098893-1 0725_45LCS 07/25/24 21:45 1 WG2330346
ICV VOCMS160725240725_46739536 0725_46 07/25/24 22:07
LCS R4098892-2 0725_46LCSA 07/25/24 22:07 1 WG2329432
BLANK R4098892-3 0725_48A 07/25/24 22:50 1 WG2329432
BLANK R4098893-3 0725_48 07/25/24 22:50 1 WG2330346
TRIP BLANK L1758896-11 0725_49 07/26/24 00:18 1 WG2330346
L1758900-19 L1758900-19 0725_50 07/26/24 00:40 1 WG2330346
L1757706-01 L1757706-01 0725_51 07/26/24 01:02 10 WG2329432
L1758607-07 L1758607-07 0725_55 07/26/24 02:29 1 WG2330346
MW-9 L1758896-10 0725_69 07/26/24 07:35 1 WG2330346
LCSD R4098892-4 0725_72A 07/26/24 08:41 1 WG2329432
LCSD R4098893-4 0725_72 07/26/24 08:41 1 WG2330346
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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8B-OR ANALYTICAL SEQUENCE
SDG:L1758896 Analytical Method:8260B
Instrument ID:VOCMS26 Calibration Start Date:06/21/24 17:35
Calibration End Date:06/21/24 21:42
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE VOCMS260621240621_07733345 0621_07 06/21/24 17:15
CAL 0.04 0621_08 06/21/24 17:35
CAL 0.1 0621_09 06/21/24 17:56
CAL 0.2 0621_10 06/21/24 18:16
CAL 0.5 0621_11 06/21/24 18:37
CAL 1 0621_12 06/21/24 18:58
CAL 2 0621_13 06/21/24 19:18
CAL 5.0 0621_14 06/21/24 19:39
CAL 25 0621_15 06/21/24 20:00
CAL 75 0621_16 06/21/24 20:20
CAL 100 0621_17 06/21/24 20:40
CAL 200 0621_18 06/21/24 21:01
CAL .05A 0621_20 06/21/24 21:42
CAL 0.1A 0621_20 06/21/24 21:42
CAL 0.2A 0621_20 06/21/24 21:42
CAL 0.5A 0621_20 06/21/24 21:42
CAL 1A 0621_20 06/21/24 21:42
CAL 5A 0621_20 06/21/24 21:42
CAL 10A 0621_20 06/21/24 21:42
CAL 15A 0621_20 06/21/24 21:42
CAL 20A 0621_20 06/21/24 21:42
SSCV VOCMS260621240621_22733345 0621_22 06/21/24 22:23
SSCV VOCMS260621240621_23733345 0621_23 06/21/24 22:43
ICV VOCMS26072924A0729A_01733345 0729A_01 07/29/24 19:18
LCS R4100702-1 0729A_01LCSB 07/29/24 19:18 1 WG2332144
LCS R4100703-1 0729A_01LCSA 07/29/24 19:18 1 WG2332276
TUNE VOCMS26072924A0729A_01T733345 0729A_01T 07/29/24 19:18
LCS R4100704-1 0729A_01LCS 07/29/24 19:18 1 WG2332303
BLANK R4100702-2 0729A_03B 07/29/24 19:59 1 WG2332144
BLANK R4100703-2 0729A_03A 07/29/24 19:59 1 WG2332276
BLANK R4100704-2 0729A_03 07/29/24 19:59 1 WG2332303
MW-10 L1758896-09 0729A_04 07/29/24 20:32 1 WG2332276
L1758917-04 L1758917-04 0729A_09 07/29/24 22:14 1 WG2332144
L1758917-10 L1758917-10 0729A_10 07/29/24 22:35 1 WG2332144
MW-4 L1758896-04 0729A_11 07/29/24 22:55 10 WG2332276
MW-8 L1758896-05 0729A_12 07/29/24 23:16 25 WG2332276
MW-7 L1758896-07 0729A_13 07/29/24 23:36 200 WG2332276
MW-5 L1758896-08 0729A_14 07/29/24 23:56 25 WG2332276
L1758917-13 L1758917-13 0729A_16 07/30/24 00:37 10 WG2332144
L1760493-12 L1760493-12 0729A_19 07/30/24 01:39 1 WG2332303
L1760525-01 L1760525-01 0729A_21 07/30/24 02:20 20 WG2332303
L1760525-03 L1760525-03 0729A_22 07/30/24 02:40 200 WG2332303
L1760525-04 L1760525-04 0729A_23 07/30/24 03:01 5 WG2332303
L1760525-05 L1760525-05 0729A_24 07/30/24 03:21 20 WG2332303
L1760525-07 L1760525-07 0729A_25 07/30/24 03:42 200 WG2332303
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1758896-01,02,03,04,05,06,07,08,09,10,11 Analytical Method:8260B
Matrix:GW Prep Method:8260B
Analyte CAS MDL RDL
mg/l mg/l
n-Butylbenzene 104-51-8 0.000157 0.0010
sec-Butylbenzene 135-98-8 0.000125 0.0010
tert-Butylbenzene 98-06-6 0.000127 0.0010
Carbon tetrachloride 56-23-5 0.000128 0.0010
Chlorobenzene 108-90-7 0.000116 0.0010
Chlorodibromomethane 124-48-1 0.000140 0.0010
Chloroethane 75-00-3 0.000192 0.0050
Chloroform 67-66-3 0.000111 0.0050
Chloromethane 74-87-3 0.000960 0.0025
Acetone 67-64-1 0.0113 0.05
2-Chlorotoluene 95-49-8 0.000106 0.0010
4-Chlorotoluene 106-43-4 0.000114 0.0010
1,2-Dibromo-3-Chloropropane 96-12-8 0.000276 0.0050
1,2-Dibromoethane 106-93-4 0.000126 0.0010
Dibromomethane 74-95-3 0.000122 0.0010
1,2-Dichlorobenzene 95-50-1 0.000107 0.0010
1,3-Dichlorobenzene 541-73-1 0.000110 0.0010
1,4-Dichlorobenzene 106-46-7 0.000120 0.0010
Dichlorodifluoromethane 75-71-8 0.000374 0.0050
1,1-Dichloroethane 75-34-3 0.0001 0.0010
Acrolein 107-02-8 0.002540 0.05
1,2-Dichloroethane 107-06-2 0.00008190 0.0010
1,1-Dichloroethene 75-35-4 0.000188 0.0010
cis-1,2-Dichloroethene 156-59-2 0.000126 0.0010
trans-1,2-Dichloroethene 156-60-5 0.000149 0.0010
1,2-Dichloropropane 78-87-5 0.000149 0.0010
1,1-Dichloropropene 563-58-6 0.000142 0.0010
1,3-Dichloropropane 142-28-9 0.000110 0.0010
cis-1,3-Dichloropropene 10061-01-5 0.000111 0.0010
trans-1,3-Dichloropropene 10061-02-6 0.000118 0.0010
2,2-Dichloropropane 594-20-7 0.000161 0.0010
Acrylonitrile 107-13-1 0.000671 0.01
Di-isopropyl ether 108-20-3 0.000105 0.0010
Ethylbenzene 100-41-4 0.000137 0.0010
Hexachloro-1,3-butadiene 87-68-3 0.000337 0.0010
Isopropylbenzene 98-82-8 0.000105 0.0010
p-Isopropyltoluene 99-87-6 0.000120 0.0010
2-Butanone (MEK)78-93-3 0.001190 0.01
Methylene Chloride 75-09-2 0.000430 0.0050
4-Methyl-2-pentanone (MIBK)108-10-1 0.000478 0.01
Methyl tert-butyl ether 1634-04-4 0.000101 0.0010
Naphthalene 91-20-3 0.0010 0.0050
Benzene 71-43-2 0.00009410 0.0010
n-Propylbenzene 103-65-1 0.00009930 0.0010
Styrene 100-42-5 0.000118 0.0010
1,1,1,2-Tetrachloroethane 630-20-6 0.000147 0.0010
1,1,2,2-Tetrachloroethane 79-34-5 0.000133 0.0010
1,1,2-Trichlorotrifluoroethane 76-13-1 0.000180 0.0010
Tetrachloroethene 127-18-4 0.0003 0.0010
Toluene 108-88-3 0.000278 0.0010
1,2,3-Trichlorobenzene 87-61-6 0.000230 0.0010
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1758896-01,02,03,04,05,06,07,08,09,10,11 Analytical Method:8260B
Matrix:GW Prep Method:8260B
Analyte CAS MDL RDL
mg/l mg/l
1,2,4-Trichlorobenzene 120-82-1 0.000481 0.0010
1,1,1-Trichloroethane 71-55-6 0.000149 0.0010
Bromobenzene 108-86-1 0.000118 0.0010
1,1,2-Trichloroethane 79-00-5 0.000158 0.0010
Trichloroethene 79-01-6 0.000190 0.0010
Trichlorofluoromethane 75-69-4 0.000160 0.0050
1,2,3-Trichloropropane 96-18-4 0.000237 0.0025
1,2,4-Trimethylbenzene 95-63-6 0.000322 0.0010
1,2,3-Trimethylbenzene 526-73-8 0.000104 0.0010
1,3,5-Trimethylbenzene 108-67-8 0.000104 0.0010
Vinyl chloride 75-01-4 0.000234 0.0010
Xylenes, Total 1330-20-7 0.000174 0.0030
Bromodichloromethane 75-27-4 0.000136 0.0010
Bromoform 75-25-2 0.000129 0.0010
Bromomethane 74-83-9 0.000605 0.0050
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098893-3
Lab Sample ID:R4098893-3 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_48 Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:07/25/24 22:50
Analytical Batch:WG2330346 Analysis Date/Time:07/25/24 22:50
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.17 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098893-3
Lab Sample ID:R4098893-3 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0725_48 Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:07/25/24 22:50
Analytical Batch:WG2330346 Analysis Date/Time:07/25/24 22:50
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 0 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-2
Lab Sample ID:R4099344-2 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0726_05 Received Date/Time:_______________
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 09:41
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 09:41
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 U 0.0113 0.0500
Acrolein 107-02-8 0 U 0.00254 0.0500
Acrylonitrile 107-13-1 0 U 0.000671 0.0100
Benzene 71-43-2 0 U 0.0000941 0.00100
Bromobenzene 108-86-1 0 U 0.000118 0.00100
Bromodichloromethane 75-27-4 0 U 0.000136 0.00100
Bromoform 75-25-2 0 U 0.000129 0.00100
Bromomethane 74-83-9 0 U 0.000605 0.00500
n-Butylbenzene 104-51-8 0 U 0.000157 0.00100
sec-Butylbenzene 135-98-8 0 U 0.000125 0.00100
tert-Butylbenzene 98-06-6 0 U 0.000127 0.00100
Carbon tetrachloride 56-23-5 0 U 0.000128 0.00100
Chlorobenzene 108-90-7 0 U 0.000116 0.00100
Chlorodibromomethane 124-48-1 0 U 0.000140 0.00100
Chloroethane 75-00-3 0 U 0.000192 0.00500
Chloroform 67-66-3 0 U 0.000111 0.00500
Chloromethane 74-87-3 0 U 0.000960 0.00250
2-Chlorotoluene 95-49-8 0 U 0.000106 0.00100
4-Chlorotoluene 106-43-4 0 U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 0 U 0.000276 0.00500
1,2-Dibromoethane 106-93-4 0 U 0.000126 0.00100
Dibromomethane 74-95-3 0 U 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 0 U 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 0 U 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 0 U 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 0 U 0.000374 0.00500
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
1,2-Dichloroethane 107-06-2 0 U 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 0 U 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 0 U 0.000149 0.00100
1,2-Dichloropropane 78-87-5 0 U 0.000149 0.00100
1,1-Dichloropropene 563-58-6 0 U 0.000142 0.00100
1,3-Dichloropropane 142-28-9 0 U 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 0 U 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 0 U 0.000118 0.00100
2,2-Dichloropropane 594-20-7 0 U 0.000161 0.00100
Di-isopropyl ether 108-20-3 0 U 0.000105 0.00100
Ethylbenzene 100-41-4 0 U 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 0 U 0.000337 0.00100
Isopropylbenzene 98-82-8 0 U 0.000105 0.00100
p-Isopropyltoluene 99-87-6 0 U 0.000120 0.00100
2-Butanone (MEK)78-93-3 0 U 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-2
Lab Sample ID:R4099344-2 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0726_05 Received Date/Time:_______________
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 09:41
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 09:41
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.07 U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 0 U 0.000101 0.00100
Naphthalene 91-20-3 0 U 0.00100 0.00500
n-Propylbenzene 103-65-1 0 U 0.0000993 0.00100
Styrene 100-42-5 0 U 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 0 U 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.000180 0.00100
Tetrachloroethene 127-18-4 0 U 0.000300 0.00100
Toluene 108-88-3 0 U 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 0 U 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 0 U 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 0 U 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 0 U 0.000158 0.00100
Trichloroethene 79-01-6 0 U 0.000190 0.00100
Trichlorofluoromethane 75-69-4 0 U 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 0 U 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 0 U 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 0 U 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 0 U 0.000104 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
Xylenes, Total 1330-20-7 0 U 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100703-2
Lab Sample ID:R4100703-2 SDG:L1758896
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:0729A_03A Received Date/Time:_______________
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 19:59
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 19:59
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
1,1-Dichloroethane 75-34-3 0 U 0.000100 0.00100
cis-1,2-Dichloroethene 156-59-2 0 U 0.000126 0.00100
Vinyl chloride 75-01-4 0 U 0.000234 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098893-1
Lab Sample ID:R4098893-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_45LCS Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:07/25/24 21:45
Analytical Batch:WG2330346 Analysis Date/Time:07/25/24 21:45
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.17 0.0241 J 0.0113 0.0500
Acrolein 107-02-8 3 0.0215 J 0.000 0.0500
Acrylonitrile 107-13-1 3.62 0.0243 0.000671 0.0100
Benzene 71-43-2 4.37 0.00460 0.0000941 0.00100
Bromobenzene 108-86-1 7.45 0.00436 0.000118 0.00100
Bromodichloromethane 75-27-4 5.02 0.00464 0.000136 0.00100
Bromoform 75-25-2 7 0.00426 0.000129 0.00100
Bromomethane 74-83-9 2.27 0.00471 J 0.000605 0.00500
n-Butylbenzene 104-51-8 8.38 0.00408 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.96 0.00412 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.82 0.00426 0.000127 0.00100
Carbon tetrachloride 56-23-5 4.13 0.00532 0.000128 0.00100
Chlorobenzene 108-90-7 6.53 0.00456 0.000116 0.00100
Chlorodibromomethane 124-48-1 6.02 0.00466 0.000140 0.00100
Chloroethane 75-00-3 2.35 0.00479 J 0.000192 0.00500
Chloroform 67-66-3 4.03 0.00459 J 0.000111 0.00500
Chloromethane 74-87-3 1.93 0.00566 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.57 0.00443 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.70 0.00437 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.16 0.00414 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.20 0.00445 0.000126 0.00100
Dibromomethane 74-95-3 4.94 0.00505 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.54 0.00440 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.14 0.00466 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.21 0.00446 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.76 0.00569 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.59 0.00474 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.48 0.00476 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.79 0.00510 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.89 0.00469 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.23 0.00467 0.000149 0.00100
1,2-Dichloropropane 78-87-5 5 0.00481 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.23 0.00448 0.000142 0.00100
1,3-Dichloropropane 142-28-9 6.08 0.00449 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.39 0.00446 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.79 0.00471 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.95 0.00453 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.49 0.00469 0.000105 0.00100
Ethylbenzene 100-41-4 6.53 0.00429 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.68 0.00409 0.000337 0.00100
Isopropylbenzene 98-82-8 7.14 0.00404 0.000105 0.00100
p-Isopropyltoluene 99-87-6 8.06 0.00408 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.19 0.0241 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098893-1
Lab Sample ID:R4098893-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0725_45LCS Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:07/25/24 21:45
Analytical Batch:WG2330346 Analysis Date/Time:07/25/24 21:45
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.14 0.00455 J 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.75 0.0235 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.29 0.00458 0.000101 0.00100
Naphthalene 91-20-3 9.98 0.00319 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.44 0.00437 0.0000993 0.00100
Styrene 100-42-5 6.96 0.00430 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.56 0.00431 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.48 0.00461 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.81 0.00512 0.000180 0.00100
Tetrachloroethene 127-18-4 5.79 0.00498 0.000300 0.00100
Toluene 108-88-3 5.54 0.00443 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.13 0.00369 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.71 0.00370 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.17 0.00535 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.90 0.00458 0.000158 0.00100
Trichloroethene 79-01-6 4.69 0.00480 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.45 0.00517 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.60 0.00501 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.87 0.00420 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.21 0.00412 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.57 0.00446 0.000104 0.00100
Vinyl chloride 75-01-4 2 0.00483 0.000234 0.00100
Xylenes, Total 1330-20-7 6.93 0.0130 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 196 of 210
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-1
Lab Sample ID:R4099344-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0726_03LCS Received Date/Time:_______________
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 09:00
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 09:00
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 0.0185 J 0.0113 0.0500
Acrolein 107-02-8 2.91 0.0457 J J4 0.000 0.0500
Acrylonitrile 107-13-1 3.53 0.0257 0.000671 0.0100
Benzene 71-43-2 4.29 0.00530 0.0000941 0.00100
Bromobenzene 108-86-1 7.39 0.00502 0.000118 0.00100
Bromodichloromethane 75-27-4 4.95 0.00546 0.000136 0.00100
Bromoform 75-25-2 6.94 0.00371 0.000129 0.00100
Bromomethane 74-83-9 2.18 0.00180 J 0.000605 0.00500
n-Butylbenzene 104-51-8 8.34 0.00475 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.91 0.00495 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.77 0.00464 0.000127 0.00100
Carbon tetrachloride 56-23-5 4.05 0.00578 0.000128 0.00100
Chlorobenzene 108-90-7 6.47 0.00453 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.96 0.00445 0.000140 0.00100
Chloroethane 75-00-3 2.27 0.00639 0.000192 0.00500
Chloroform 67-66-3 3.95 0.00533 0.000111 0.00500
Chloromethane 74-87-3 1.86 0.00418 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.52 0.00504 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.64 0.00492 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.13 0.00321 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.14 0.00448 0.000126 0.00100
Dibromomethane 74-95-3 4.87 0.00539 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.50 0.00460 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.10 0.00471 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.16 0.00469 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.69 0.00423 J 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.00579 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.40 0.00581 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.00542 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.81 0.00556 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.00545 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.92 0.00560 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.15 0.00551 0.000142 0.00100
1,3-Dichloropropane 142-28-9 6.01 0.00451 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.32 0.00540 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.72 0.00473 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.87 0.00495 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.40 0.00540 0.000105 0.00100
Ethylbenzene 100-41-4 6.47 0.00440 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.65 0.00456 0.000337 0.00100
Isopropylbenzene 98-82-8 7.08 0.00432 0.000105 0.00100
p-Isopropyltoluene 99-87-6 8.01 0.00485 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.11 0.0205 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-1
Lab Sample ID:R4099344-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0726_03LCS Received Date/Time:_______________
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 09:00
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 09:00
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.06 0.00560 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.68 0.0216 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.20 0.00505 0.000101 0.00100
Naphthalene 91-20-3 9.96 0.00394 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.39 0.00484 0.0000993 0.00100
Styrene 100-42-5 6.91 0.00433 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.51 0.00456 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.44 0.00477 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.73 0.00495 0.000180 0.00100
Tetrachloroethene 127-18-4 5.73 0.00409 0.000300 0.00100
Toluene 108-88-3 5.47 0.00465 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.11 0.00409 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.68 0.00386 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.09 0.00546 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.83 0.00462 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00517 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.37 0.00542 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.55 0.00490 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.82 0.00473 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.17 0.00481 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.52 0.00472 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.00519 0.000234 0.00100
Xylenes, Total 1330-20-7 6.87 0.0130 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4100703-1
Lab Sample ID:R4100703-1 SDG:L1758896
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:0729A_01LCSA Received Date/Time:_______________
Instrument ID:VOCMS26 Preparation Date/Time:07/29/24 19:18
Analytical Batch:WG2332276 Analysis Date/Time:07/29/24 19:18
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
1,1-Dichloroethane 75-34-3 3.59 0.00486 0.000100 0.00100
cis-1,2-Dichloroethene 156-59-2 3.89 0.00479 0.000126 0.00100
Vinyl chloride 75-01-4 2.01 0.00447 0.000234 0.00100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT L1758896 08/05/24 14:07 199 of 210
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098893-4
Lab Sample ID:R4098893-4 SDG:L1758896
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0725_72 Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:07/26/24 08:41
Analytical Batch:WG2330346 Analysis Date/Time:07/26/24 08:41
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.17 0.0225 J 0.0113 0.0500
Acrolein 107-02-8 2.99 0.0172 J 0.000 0.0500
Acrylonitrile 107-13-1 3.62 0.0247 0.000671 0.0100
Benzene 71-43-2 4.37 0.00454 0.0000941 0.00100
Bromobenzene 108-86-1 7.45 0.00434 0.000118 0.00100
Bromodichloromethane 75-27-4 5.01 0.00465 0.000136 0.00100
Bromoform 75-25-2 7 0.00454 0.000129 0.00100
Bromomethane 74-83-9 2.27 0.00513 0.000605 0.00500
n-Butylbenzene 104-51-8 8.38 0.00387 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.96 0.00398 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.82 0.00411 0.000127 0.00100
Carbon tetrachloride 56-23-5 4.12 0.00497 0.000128 0.00100
Chlorobenzene 108-90-7 6.53 0.00466 0.000116 0.00100
Chlorodibromomethane 124-48-1 6.02 0.00467 0.000140 0.00100
Chloroethane 75-00-3 2.36 0.00445 J 0.000192 0.00500
Chloroform 67-66-3 4.03 0.00466 J 0.000111 0.00500
Chloromethane 74-87-3 1.94 0.00578 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.57 0.00431 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.70 0.00437 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.16 0.00428 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.20 0.00480 0.000126 0.00100
Dibromomethane 74-95-3 4.94 0.00454 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.54 0.00428 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.14 0.00440 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.21 0.00447 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.76 0.00528 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.59 0.00463 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.48 0.00489 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.78 0.00490 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.89 0.00443 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.23 0.00479 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.99 0.00494 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.22 0.00444 0.000142 0.00100
1,3-Dichloropropane 142-28-9 6.08 0.00457 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.39 0.00424 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.79 0.00457 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.95 0.00452 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.49 0.00455 0.000105 0.00100
Ethylbenzene 100-41-4 6.53 0.00462 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.68 0.00393 0.000337 0.00100
Isopropylbenzene 98-82-8 7.14 0.00397 0.000105 0.00100
p-Isopropyltoluene 99-87-6 8.06 0.00384 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.19 0.0242 0.00119 0.0100
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4098893-4
Lab Sample ID:R4098893-4 SDG:L1758896
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:0725_72 Received Date/Time:_______________
Instrument ID:VOCMS16 Preparation Date/Time:07/26/24 08:41
Analytical Batch:WG2330346 Analysis Date/Time:07/26/24 08:41
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.14 0.00458 J 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.75 0.0244 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.29 0.00443 0.000101 0.00100
Naphthalene 91-20-3 9.98 0.00289 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.44 0.00426 0.0000993 0.00100
Styrene 100-42-5 6.96 0.00414 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.56 0.00454 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.48 0.00473 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.81 0.00435 0.000180 0.00100
Tetrachloroethene 127-18-4 5.79 0.00478 0.000300 0.00100
Toluene 108-88-3 5.54 0.00467 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.13 0.00348 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.71 0.00336 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.16 0.00525 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.90 0.00472 0.000158 0.00100
Trichloroethene 79-01-6 4.68 0.00468 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.45 0.00439 J 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.60 0.00526 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.87 0.00404 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.21 0.00414 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.57 0.00427 0.000104 0.00100
Vinyl chloride 75-01-4 2 0.00386 J3 0.000234 0.00100
Xylenes, Total 1330-20-7 6.93 0.0135 0.000174 0.00300
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-3
Lab Sample ID:R4099344-3 SDG:L1758896
Client Sample ID:MS Collected Date/Time:07/17/24 10:32
Lab File ID:0726_26 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 17:45
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 17:45
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 0.0217 0.0113 0.0500
Acrolein 107-02-8 2.91 0.0593 J5 0.00254 0.0500
Acrylonitrile 107-13-1 3.53 0.0322 0.000671 0.0100
Benzene 71-43-2 4.29 0.00750 0.0000941 0.00100
Bromobenzene 108-86-1 7.39 0.00650 0.000118 0.00100
Bromodichloromethane 75-27-4 4.94 0.00701 0.000136 0.00100
Bromoform 75-25-2 6.94 0.00476 0.000129 0.00100
Bromomethane 74-83-9 2.17 0.00235 0.000605 0.00500
n-Butylbenzene 104-51-8 8.34 0.00599 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.91 0.00635 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.77 0.00595 0.000127 0.00100
Carbon tetrachloride 56-23-5 4.05 0.00834 J5 0.000128 0.00100
Chlorobenzene 108-90-7 6.47 0.00579 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.96 0.00562 0.000140 0.00100
Chloroethane 75-00-3 2.27 0.00877 J5 0.000192 0.00500
Chloroform 67-66-3 3.95 0.00720 0.000111 0.00500
Chloromethane 74-87-3 1.86 0.00576 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.52 0.00644 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.64 0.00630 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.13 0.00409 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.14 0.00535 0.000126 0.00100
Dibromomethane 74-95-3 4.87 0.00684 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.50 0.00556 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.10 0.00592 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.16 0.00601 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.69 0.00716 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.0174 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.40 0.00768 J5 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.0100 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.81 0.146 V 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.0110 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.92 0.00735 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.15 0.00757 0.000142 0.00100
1,3-Dichloropropane 142-28-9 6.01 0.00567 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.32 0.00636 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.72 0.00563 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.87 0.00622 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.40 0.00727 0.000105 0.00100
Ethylbenzene 100-41-4 6.47 0.00565 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.65 0.00547 0.000337 0.00100
Isopropylbenzene 98-82-8 7.08 0.00541 0.000105 0.00100
p-Isopropyltoluene 99-87-6 8.01 0.00605 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.11 0.0255 0.00119 0.0100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-3
Lab Sample ID:R4099344-3 SDG:L1758896
Client Sample ID:MS Collected Date/Time:07/17/24 10:32
Lab File ID:0726_26 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 17:45
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 17:45
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.06 0.00702 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.68 0.0271 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.20 0.00668 0.000101 0.00100
Naphthalene 91-20-3 9.96 0.00427 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.39 0.00629 0.0000993 0.00100
Styrene 100-42-5 6.90 0.00550 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.51 0.00610 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.44 0.00612 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.72 0.00816 J5 0.000180 0.00100
Tetrachloroethene 127-18-4 5.73 0.00547 0.000300 0.00100
Toluene 108-88-3 5.47 0.00582 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.11 0.00457 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.69 0.00438 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.09 0.00728 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.83 0.00556 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00734 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.36 0.00855 J5 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.55 0.00608 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.82 0.00607 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.17 0.00611 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.52 0.00610 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.00965 0.000234 0.00100
Xylenes, Total 1330-20-7 6.87 0.0164 0.000174 0.00300
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-4
Lab Sample ID:R4099344-4 SDG:L1758896
Client Sample ID:MSD Collected Date/Time:07/17/24 10:32
Lab File ID:0726_27 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 18:06
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 18:06
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Acetone 67-64-1 3.08 0.0217 0.0113 0.0500
Acrolein 107-02-8 2.91 0.0606 J5 0.00254 0.0500
Acrylonitrile 107-13-1 3.53 0.0320 0.000671 0.0100
Benzene 71-43-2 4.29 0.00745 0.0000941 0.00100
Bromobenzene 108-86-1 7.39 0.00678 0.000118 0.00100
Bromodichloromethane 75-27-4 4.95 0.00721 0.000136 0.00100
Bromoform 75-25-2 6.94 0.00452 0.000129 0.00100
Bromomethane 74-83-9 2.17 0.00282 0.000605 0.00500
n-Butylbenzene 104-51-8 8.34 0.00595 0.000157 0.00100
sec-Butylbenzene 135-98-8 7.91 0.00668 0.000125 0.00100
tert-Butylbenzene 98-06-6 7.77 0.00620 0.000127 0.00100
Carbon tetrachloride 56-23-5 4.05 0.00877 J5 0.000128 0.00100
Chlorobenzene 108-90-7 6.47 0.00587 0.000116 0.00100
Chlorodibromomethane 124-48-1 5.96 0.00563 0.000140 0.00100
Chloroethane 75-00-3 2.27 0.00887 J5 0.000192 0.00500
Chloroform 67-66-3 3.95 0.00753 0.000111 0.00500
Chloromethane 74-87-3 1.85 0.00598 0.000960 0.00250
2-Chlorotoluene 95-49-8 7.52 0.00666 0.000106 0.00100
4-Chlorotoluene 106-43-4 7.64 0.00653 0.000114 0.00100
1,2-Dibromo-3-Chloropropane 96-12-8 9.13 0.00417 J 0.000276 0.00500
1,2-Dibromoethane 106-93-4 6.13 0.00541 0.000126 0.00100
Dibromomethane 74-95-3 4.87 0.00691 0.000122 0.00100
1,2-Dichlorobenzene 95-50-1 8.50 0.00596 0.000107 0.00100
1,3-Dichlorobenzene 541-73-1 8.10 0.00619 0.000110 0.00100
1,4-Dichlorobenzene 106-46-7 8.16 0.00618 0.000120 0.00100
Dichlorodifluoromethane 75-71-8 1.68 0.00727 0.000374 0.00500
1,1-Dichloroethane 75-34-3 3.51 0.0169 0.000100 0.00100
1,2-Dichloroethane 107-06-2 4.40 0.00758 J5 0.0000819 0.00100
1,1-Dichloroethene 75-35-4 2.71 0.0101 0.000188 0.00100
cis-1,2-Dichloroethene 156-59-2 3.81 0.144 V 0.000126 0.00100
trans-1,2-Dichloroethene 156-60-5 3.15 0.0107 0.000149 0.00100
1,2-Dichloropropane 78-87-5 4.92 0.00774 0.000149 0.00100
1,1-Dichloropropene 563-58-6 4.15 0.00771 0.000142 0.00100
1,3-Dichloropropane 142-28-9 6.01 0.00579 0.000110 0.00100
cis-1,3-Dichloropropene 10061-01-5 5.32 0.00652 0.000111 0.00100
trans-1,3-Dichloropropene 10061-02-6 5.72 0.00567 0.000118 0.00100
2,2-Dichloropropane 594-20-7 3.87 0.00630 0.000161 0.00100
Di-isopropyl ether 108-20-3 3.40 0.00737 0.000105 0.00100
Ethylbenzene 100-41-4 6.47 0.00572 0.000137 0.00100
Hexachloro-1,3-butadiene 87-68-3 9.65 0.00556 0.000337 0.00100
Isopropylbenzene 98-82-8 7.08 0.00570 0.000105 0.00100
p-Isopropyltoluene 99-87-6 8.01 0.00644 0.000120 0.00100
2-Butanone (MEK)78-93-3 4.11 0.0250 0.00119 0.0100
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4099344-4
Lab Sample ID:R4099344-4 SDG:L1758896
Client Sample ID:MSD Collected Date/Time:07/17/24 10:32
Lab File ID:0726_27 Received Date/Time:07/20/24 08:00
Instrument ID:VOCMS13 Preparation Date/Time:07/26/24 18:06
Analytical Batch:WG2330260 Analysis Date/Time:07/26/24 18:06
Dilution Factor:1 Prep Method:8260B
Analytical Method:8260B Sample Vol Used:5 mL
Matrix:GW Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:5 mL
Analyte CAS RT Result Qualifier MDL RDL
mg/l mg/l mg/l
Methylene Chloride 75-09-2 3.06 0.00723 J5 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)108-10-1 5.68 0.0267 0.000478 0.0100
Methyl tert-butyl ether 1634-04-4 3.20 0.00671 0.000101 0.00100
Naphthalene 91-20-3 9.96 0.00463 J 0.00100 0.00500
n-Propylbenzene 103-65-1 7.39 0.00660 0.0000993 0.00100
Styrene 100-42-5 6.90 0.00567 0.000118 0.00100
1,1,1,2-Tetrachloroethane 630-20-6 6.51 0.00591 0.000147 0.00100
1,1,2,2-Tetrachloroethane 79-34-5 7.44 0.00613 0.000133 0.00100
1,1,2-Trichlorotrifluoroethane 76-13-1 2.73 0.00840 J5 0.000180 0.00100
Tetrachloroethene 127-18-4 5.73 0.00552 0.000300 0.00100
Toluene 108-88-3 5.47 0.00599 0.000278 0.00100
1,2,3-Trichlorobenzene 87-61-6 10.11 0.00490 0.000230 0.00100
1,2,4-Trichlorobenzene 120-82-1 9.69 0.00473 0.000481 0.00100
1,1,1-Trichloroethane 71-55-6 4.09 0.00750 0.000149 0.00100
1,1,2-Trichloroethane 79-00-5 5.83 0.00572 0.000158 0.00100
Trichloroethene 79-01-6 4.61 0.00735 0.000190 0.00100
Trichlorofluoromethane 75-69-4 2.37 0.00893 J5 0.000160 0.00500
1,2,3-Trichloropropane 96-18-4 7.55 0.00614 0.000237 0.00250
1,2,4-Trimethylbenzene 95-63-6 7.82 0.00635 0.000322 0.00100
1,2,3-Trimethylbenzene 526-73-8 8.17 0.00634 0.000104 0.00100
1,3,5-Trimethylbenzene 108-67-8 7.52 0.00643 0.000104 0.00100
Vinyl chloride 75-01-4 1.92 0.00988 0.000234 0.00100
Xylenes, Total 1330-20-7 6.87 0.0171 0.000174 0.00300
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
COD Coefficient of Determination.
Mass Mass of parameter.
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
RRF Relative Response Factor.
RT Retention Time.
SDG Sample Delivery Group.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Wavelength Wavelength of parameter.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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ANALYTICAL REPORT
October 31, 2024
Geosyntec Consultants - UT
Sample Delivery Group:L1784259
Samples Received:10/02/2024
Project Number:SLC1091
Description:Paxton Ave
Report To:Brian Smith
215 South State Street
Suite 500
Salt Lake City, UT 84111
Entire Report Reviewed By:
October 31, 2024
[Preliminary Report]
Chris Ward
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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October 31, 2024
Chris Ward
Project Manager
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TABLE OF CONTENTSTABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 4
Cn: Case Narrative 5
Su: Summary Results 6
TO-15 Volatile Organic Compounds (MS) 6
Surrogate Recovery 7
Air Surrogate Summary 7
Laboratory Control Sample / Duplicate 8
WG2374030 LCS(R4127354-1) LCSD(R4127354-2) 8
WG2376939 LCS(R4129260-1) LCSD(R4129260-2) 10
Method Blank 11
WG2376939 R4129260-3 AIRMS14 10/06/24 10:56 11
WG2374030 R4127354-3 AIRMS17 10/02/24 10:00 12
GC/MS Performance Check 13
AIRMS14 093024A 09/30/24 20:20 13
AIRMS14 100624 10/06/24 08:30 14
AIRMS17 092724A 09/27/24 16:33 15
AIRMS17 100224 10/02/24 08:36 16
Internal Standard & Retention Time 17
AIRMS14 10/06/24 08:30 17
AIRMS17 10/02/24 08:36 18
Sample Result Summary Organic Analysis Data Sheet 19
L1784259-01 10/06/24 19:57 AIRMS14 19
L1784259-01 10/02/24 23:03 AIRMS17 20
L1784259-02 10/06/24 20:42 AIRMS14 22
L1784259-02 10/02/24 23:32 AIRMS17 23
L1784259-03 10/06/24 21:27 AIRMS14 25
L1784259-03 10/03/24 00:00 AIRMS17 26
GC/MS Initial Calibration 28
AIRMS14 09/30/24 21:51 28
AIRMS17 09/27/24 17:25 30
GC/MS Calibration Verification 34
AIRMS14 10/01/24 06:43 34
AIRMS14 10/06/24 08:30 36
AIRMS17 09/27/24 22:27 38
AIRMS17 10/02/24 08:36 40
Analytical Sequence 42
AIRMS14 09/30/24 21:51 42
AIRMS17 09/27/24 17:25 43
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Detection Limit Summary 44
TO-15 - Air 44
QC Result Summary Organic Analysis Data Sheet 46
BLANK(R4127354-3) WG2374030 10/02/24 10:00 AIRMS17 46
BLANK(R4129260-3) WG2376939 10/06/24 10:56 AIRMS14 48
LCS(R4127354-1) WG2374030 10/02/24 09:05 AIRMS17 49
LCS(R4129260-1) WG2376939 10/06/24 09:20 AIRMS14 51
LCSD(R4127354-2) WG2374030 10/02/24 09:34 AIRMS17 52
LCSD(R4129260-2) WG2376939 10/06/24 10:09 AIRMS14 54
Gl: Glossary of Terms 55
Al: Accreditations & Locations 56
Sc: Sample Chain of Custody 57
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SV-1 L1784259-01 Air Jessica Welch 09/30/24 17:03 10/02/24 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2374030 1 10/02/24 23:03 10/02/24 23:03 MNP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2376939 20 10/06/24 19:57 10/06/24 19:57 MNP Mt. Juliet, TN
Collected by Collected date/time Received date/time
SV-2 L1784259-02 Air Jessica Welch 09/30/24 16:13 10/02/24 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2374030 1 10/02/24 23:32 10/02/24 23:32 MNP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2376939 20 10/06/24 20:42 10/06/24 20:42 MNP Mt. Juliet, TN
Collected by Collected date/time Received date/time
SV-20 L1784259-03 Air Jessica Welch 09/30/24 16:13 10/02/24 12:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2374030 1 10/03/24 00:00 10/03/24 00:00 MNP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2376939 20 10/06/24 21:27 10/06/24 21:27 MNP Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris Ward
Project Manager
Report Revision History
Level II Report - Version 1: 10/07/24 16:53
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Chris Ward
Project Manager
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TO-15 Volatile Organic Compounds (MS)
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2A-OR SURROGATE RECOVERY
Analytical Method:TO-15 SDG:L1784259
Matrix:Air
Sample ID Lab Sample ID Instrument File ID DMC-1 TOT Out
% Rec.
SV-1 L1784259-01 AIRMS17 1002_19 101 0
SV-1 L1784259-01 AIRMS14 1006_13 92.5 0
SV-2 L1784259-02 AIRMS17 1002_20 96.2 0
SV-2 L1784259-02 AIRMS14 1006_14 91.0 0
SV-20 L1784259-03 AIRMS17 1002_21 100 0
SV-20 L1784259-03 AIRMS14 1006_15 92.5 0
BLANK R4129260-3 AIRMS14 1006_04 95.4 0
BLANK R4127354-3 AIRMS17 1002_04 96.7 0
LCS R4129260-1 AIRMS14 1006_02 94.9 0
LCS R4127354-1 AIRMS17 1002_02 103 0
LCSD R4129260-2 AIRMS14 1006_03 93.4 0
LCSD R4127354-2 AIRMS17 1002_03 102 0
Parm Abbreviation Parameter QC LIMITS
DMC-1 1,4-Bromofluorobenzene 60.0 - 140
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4127354-1
RECOVERY R4127354-2
L1784259-01,02,03
LCS Sample / File ID:R4127354-1 / 1002_02 SDG:L1784259
LCSD Sample / File ID:R4127354-2 / 1002_03 Analytical Batch:WG2374030
Instrument ID:AIRMS17 Dilution Factor:1
Analytical Method:TO-15 Matrix:Air
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
ppbv ppbv ppbv %%%%%
Acetone 3.75 3.81 3.74 102 99.7 70.0 - 130 1.85 25
Allyl chloride 3.75 3.96 3.88 106 103 70.0 - 130 2.04 25
Benzene 3.75 4.02 3.96 107 106 70.0 - 130 1.50 25
Benzyl Chloride 3.75 3.67 3.58 97.9 95.5 70.0 - 152 2.48 25
Bromodichloromethane 3.75 4.35 4.33 116 115 70.0 - 130 0.461 25
Bromoform 3.75 4.16 4.20 111 112 70.0 - 130 0.957 25
Bromomethane 3.75 3.92 3.89 105 104 70.0 - 130 0.768 25
1,3-Butadiene 3.75 3.80 3.78 101 101 70.0 - 130 0.528 25
Carbon disulfide 7.50 8.13 8.25 108 110 70.0 - 130 1.47 25
Carbon tetrachloride 3.75 4.22 4.30 113 115 70.0 - 130 1.88 25
Chlorobenzene 3.75 4.05 3.98 108 106 70.0 - 130 1.74 25
Chloroethane 3.75 3.80 3.76 101 100 70.0 - 130 1.06 25
Chloroform 3.75 4.09 4.11 109 110 70.0 - 130 0.488 25
Chloromethane 3.75 3.73 3.86 99.5 103 70.0 - 130 3.43 25
2-Chlorotoluene 3.75 4.01 4.01 107 107 70.0 - 130 0.000 25
Cyclohexane 3.75 3.72 3.85 99.2 103 70.0 - 130 3.43 25
Dibromochloromethane 3.75 4.34 4.25 116 113 70.0 - 130 2.10 25
1,2-Dibromoethane 3.75 4.16 4.05 111 108 70.0 - 130 2.68 25
1,2-Dichlorobenzene 3.75 4.10 4.19 109 112 70.0 - 130 2.17 25
1,3-Dichlorobenzene 3.75 4.09 4.28 109 114 70.0 - 130 4.54 25
1,4-Dichlorobenzene 3.75 4.09 4.26 109 114 70.0 - 130 4.07 25
1,2-Dichloroethane 3.75 4.23 4.28 113 114 70.0 - 130 1.18 25
1,1-Dichloroethene 3.75 3.96 3.99 106 106 70.0 - 130 0.755 25
trans-1,2-Dichloroethene 3.75 4.21 3.95 112 105 70.0 - 130 6.37 25
1,2-Dichloropropane 3.75 3.87 3.89 103 104 70.0 - 130 0.515 25
cis-1,3-Dichloropropene 3.75 4.02 4.04 107 108 70.0 - 130 0.496 25
trans-1,3-Dichloropropene 3.75 3.91 4.08 104 109 70.0 - 130 4.26 25
1,4-Dioxane 3.75 3.94 4.06 105 108 70.0 - 140 3.00 25
Ethanol 3.75 3.56 3.80 94.9 101 55.0 - 148 6.52 25
Ethylbenzene 3.75 3.93 3.94 105 105 70.0 - 130 0.254 25
4-Ethyltoluene 3.75 4.19 4.26 112 114 70.0 - 130 1.66 25
Trichlorofluoromethane 3.75 4.18 4.18 111 111 70.0 - 130 0.000 25
Dichlorodifluoromethane 3.75 4.12 4.19 110 112 64.0 - 139 1.68 25
1,1,2-Trichlorotrifluoroethane 3.75 4.02 4.12 107 110 70.0 - 130 2.46 25
1,2-Dichlorotetrafluoroethane 3.75 3.94 4.05 105 108 70.0 - 130 2.75 25
Heptane 3.75 3.88 3.96 103 106 70.0 - 130 2.04 25
Hexachloro-1,3-butadiene 3.75 4.24 4.27 113 114 70.0 - 151 0.705 25
n-Hexane 3.75 3.80 3.82 101 102 70.0 - 130 0.525 25
Isopropylbenzene 3.75 4.06 4.12 108 110 70.0 - 130 1.47 25
Methylene Chloride 3.75 3.73 3.83 99.5 102 70.0 - 130 2.65 25
Methyl Butyl Ketone 3.75 3.81 3.88 102 103 70.0 - 149 1.82 25
2-Butanone (MEK)3.75 3.85 3.66 103 97.6 70.0 - 130 5.06 25
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4127354-1
RECOVERY R4127354-2
L1784259-01,02,03
LCS Sample / File ID:R4127354-1 / 1002_02 SDG:L1784259
LCSD Sample / File ID:R4127354-2 / 1002_03 Analytical Batch:WG2374030
Instrument ID:AIRMS17 Dilution Factor:1
Analytical Method:TO-15 Matrix:Air
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
ppbv ppbv ppbv %%%%%
4-Methyl-2-pentanone (MIBK)3.75 4.14 3.97 110 106 70.0 - 139 4.19 25
Methyl methacrylate 3.75 3.96 4.08 106 109 70.0 - 130 2.99 25
MTBE 3.75 3.82 3.92 102 105 70.0 - 130 2.58 25
Naphthalene 3.75 4.09 4.22 109 113 70.0 - 159 3.13 25
2-Propanol 3.75 3.60 3.71 96.0 98.9 70.0 - 139 3.01 25
Propene 3.75 3.52 3.43 93.9 91.5 64.0 - 144 2.59 25
Styrene 7.50 8.43 8.78 112 117 70.0 - 130 4.07 25
1,1,2,2-Tetrachloroethane 3.75 3.97 4.15 106 111 70.0 - 130 4.43 25
Tetrahydrofuran 3.75 3.84 3.87 102 103 70.0 - 137 0.778 25
Toluene 3.75 3.91 3.98 104 106 70.0 - 130 1.77 25
1,2,4-Trichlorobenzene 3.75 4.02 4.17 107 111 70.0 - 160 3.66 25
1,1,1-Trichloroethane 3.75 4.30 4.21 115 112 70.0 - 130 2.12 25
1,1,2-Trichloroethane 3.75 3.99 4.09 106 109 70.0 - 130 2.48 25
1,2,4-Trimethylbenzene 3.75 4.21 4.32 112 115 70.0 - 130 2.58 25
1,3,5-Trimethylbenzene 3.75 4.18 4.30 111 115 70.0 - 130 2.83 25
2,2,4-Trimethylpentane 3.75 3.79 3.86 101 103 70.0 - 130 1.83 25
Vinyl chloride 3.75 3.88 4.15 103 111 70.0 - 130 6.72 25
Vinyl Bromide 3.75 4.06 4.08 108 109 70.0 - 130 0.491 25
Vinyl acetate 3.75 3.53 3.62 94.1 96.5 70.0 - 130 2.52 25
m&p-Xylene 7.50 8.05 8.26 107 110 70.0 - 130 2.58 25
o-Xylene 3.75 4.15 4.32 111 115 70.0 - 130 4.01 25
TPH (GC/MS) Low Fraction 188 189 190 101 101 70.0 - 130 0.528 25
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:
LABORATORY CONTROL SAMPLE DUPLICATE R4129260-1
RECOVERY R4129260-2
L1784259-01,02,03
LCS Sample / File ID:R4129260-1 / 1006_02 SDG:L1784259
LCSD Sample / File ID:R4129260-2 / 1006_03 Analytical Batch:WG2376939
Instrument ID:AIRMS14 Dilution Factor:1
Analytical Method:TO-15 Matrix:Air
Analyte Spike
Amount
LCS
Result
LCSD
Result LCS Rec.LCSD Rec.Rec. Limits RPD RPD
Limit
ppbv ppbv ppbv %%%%%
1,1-Dichloroethane 3.75 4.12 4.10 110 109 70.0 - 130 0.487 25
cis-1,2-Dichloroethene 3.75 3.95 4.02 105 107 70.0 - 130 1.76 25
trans-1,2-Dichloroethene 3.75 4.01 3.93 107 105 70.0 - 130 2.02 25
Tetrachloroethylene 3.75 4.15 4.15 111 111 70.0 - 130 0.000 25
Trichloroethylene 3.75 4.30 4.28 115 114 70.0 - 130 0.466 25
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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4A-OR METHOD BLANK SAMPLE NO.:
R4129260-3
Lab Sample ID:R4129260-3 SDG:L1784259
Lab File ID:1006_04 Preparation Date/Time:10/06/24 10:56
Instrument ID:AIRMS14 Analysis Date/Time:10/06/24 10:56
Analytical Batch:WG2376939 Dilution Factor:1
Analytical Method:TO-15 Matrix:Air
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4129260-1 AIRMS14 1006_02 10/06/24 09:20
LCSD R4129260-2 AIRMS14 1006_03 10/06/24 10:09
SV-1 L1784259-01 AIRMS14 1006_13 10/06/24 19:57
SV-2 L1784259-02 AIRMS14 1006_14 10/06/24 20:42
SV-20 L1784259-03 AIRMS14 1006_15 10/06/24 21:27
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4A-OR METHOD BLANK SAMPLE NO.:
R4127354-3
Lab Sample ID:R4127354-3 SDG:L1784259
Lab File ID:1002_04 Preparation Date/Time:10/02/24 10:00
Instrument ID:AIRMS17 Analysis Date/Time:10/02/24 10:00
Analytical Batch:WG2374030 Dilution Factor:1
Analytical Method:TO-15 Matrix:Air
Sample ID Lab Sample ID Instrument File ID Analysis
date/time
LCS R4127354-1 AIRMS17 1002_02 10/02/24 09:05
LCSD R4127354-2 AIRMS17 1002_03 10/02/24 09:34
SV-1 L1784259-01 AIRMS17 1002_19 10/02/24 23:03
SV-2 L1784259-02 AIRMS17 1002_20 10/02/24 23:32
SV-20 L1784259-03 AIRMS17 1002_21 10/03/24 00:00
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0930A_01 SDG:L1784259
Instrument ID:AIRMS14 Analytical Method:TO-15
Analysis Date/Time:09/30/24 20:20
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
50 95 8 40 17
75 95 30 66 49
95 95 100 100 100
96 95 5 9 7
173 174 0 2 0
174 95 50 120 84
175 174 4 9 8
176 174 93 101 97
177 176 5 9 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-.19 .19 0930A_03 09/30/24 21:51
STD-.31 .31 0930A_04 09/30/24 22:35
STD-.63 .63 0930A_05 09/30/24 23:19
STD-1.25 1.25 0930A_06 10/01/24 00:05
STD-2.5 2.5 0930A_07 10/01/24 00:52
STD-3.75 3.75 0930A_08 10/01/24 01:41
STD-10 10 0930A_09 10/01/24 02:26
STD-25 25 0930A_10 10/01/24 03:14
STD-50 50 0930A_11 10/01/24 04:05
STD-100 100 0930A_12 10/01/24 05:04
SSCV AIRMS14093024A0930A_14756826 0930A_14 10/01/24 06:43
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1006_01T SDG:L1784259
Instrument ID:AIRMS14 Analytical Method:TO-15
Analysis Date/Time:10/06/24 08:30
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
50 95 8 40 16
75 95 30 66 48
95 95 100 100 100
96 95 5 9 6
173 174 0 2 0
174 95 50 120 87
175 174 4 9 8
176 174 93 101 97
177 176 5 9 7
Sample ID Lab Sample ID File ID Analysis date/time
ICV AIRMS141006241006_01756826 1006_01 10/06/24 08:30
LCS R4129260-1 1006_02 10/06/24 09:20
LCSD R4129260-2 1006_03 10/06/24 10:09
BLANK R4129260-3 1006_04 10/06/24 10:56
SV-1 L1784259-01 1006_13 10/06/24 19:57
SV-2 L1784259-02 1006_14 10/06/24 20:42
SV-20 L1784259-03 1006_15 10/06/24 21:27
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 0927A_01 SDG:L1784259
Instrument ID:AIRMS17 Analytical Method:TO-15
Analysis Date/Time:09/27/24 16:33
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
50 95 8 40 17
75 95 30 66 47
95 95 100 100 100
96 95 5 9 7
173 174 0 2 1
174 95 50 120 86
175 174 4 9 7
176 174 93 101 97
177 176 5 9 6
Sample ID Lab Sample ID File ID Analysis date/time
STD-0.19 0.19 0927A_03 09/27/24 17:25
STD-0.31 0.31 0927A_04 09/27/24 17:50
STD-0.63 0.63 0927A_05 09/27/24 18:15
STD-1.25 1.25 0927A_06 09/27/24 18:40
STD-2.5 2.5 0927A_07 09/27/24 19:06
STD-3.75 3.75 0927A_08 09/27/24 19:34
STD-10.0 10.0 0927A_09 09/27/24 19:59
STD-25 25 0927A_10 09/27/24 20:25
STD-50 50 0927A_11 09/27/24 20:55
STD-100 100 0927A_12 09/27/24 21:32
SSCV AIRMS17092724A0927A_14756221 0927A_14 09/27/24 22:27
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5A-OR GC/MS INSTRUMENT
PERFORMANCE CHECK
Lab File ID: 1002_01T SDG:L1784259
Instrument ID:AIRMS17 Analytical Method:TO-15
Analysis Date/Time:10/02/24 08:36
Target Mass (m/e)Relative Mass Low Limit High Limit % Relative Abundance
50 95 8 40 17
75 95 30 66 49
95 95 100 100 100
96 95 5 9 6
173 174 0 2 1
174 95 50 120 87
175 174 4 9 7
176 174 93 101 100
177 176 5 9 6
Sample ID Lab Sample ID File ID Analysis date/time
ICV AIRMS171002241002_01756221 1002_01 10/02/24 08:36
LCS R4127354-1 1002_02 10/02/24 09:05
LCSD R4127354-2 1002_03 10/02/24 09:34
BLANK R4127354-3 1002_04 10/02/24 10:00
SV-1 L1784259-01 1002_19 10/02/24 23:03
SV-2 L1784259-02 1002_20 10/02/24 23:32
SV-20 L1784259-03 1002_21 10/03/24 00:00
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS14 Calibration Start Date:09/30/24 21:51
Std File: 1006_01 Calibration End Date:10/01/24 05:04
Std Analysis Date:10/06/24 08:30
Sample ID File ID DFB BCM CB
Response RT Response RT Response RT
STANDARD 323672 8.62 84059 7.78 307467 11.72
UPPER LIMIT 519172 129870 485982
LOWER LIMIT 222502 55658 208278
LCS R4129260-1
WG2376939 1x 1006_02 328438 8.61 84291 7.78 299592 11.72
LCSD R4129260-2
WG2376939 1x 1006_03 326696 8.61 84606 7.78 307689 11.72
BLANK R4129260-3
WG2376939 1x 1006_04 325631 8.61 83360 7.78 303885 11.72
L1784259-01 WG2376939
20x 1006_13 306714 8.61 78743 7.78 285653 11.72
L1784259-02 WG2376939
20x 1006_14 306367 8.61 77826 7.78 289863 11.72
L1784259-03 WG2376939
20x 1006_15 297405 8.61 77781 7.78 282327 11.72
DFB - 1,4-DIFLUOROBENZENE BCM - BROMOCHLOROMETHANE
CB - CHLOROBENZENE-D5
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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8A-OR INTERNAL STANDARD
AND RETENTION TIME
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS17 Calibration Start Date:09/27/24 17:25
Std File: 1002_01 Calibration End Date:09/27/24 21:32
Std Analysis Date:10/02/24 08:36
Sample ID File ID DFB BCM CB
Response RT Response RT Response RT
STANDARD 74530 4.12 18529 3.15 65517 6.34
UPPER LIMIT 138355 33666 122013
LOWER LIMIT 59295 14428 52291
LCS R4127354-1
WG2374030 1x 1002_02 78249 4.12 19554 3.15 69790 6.34
LCSD R4127354-2
WG2374030 1x 1002_03 76925 4.12 19251 3.15 67686 6.34
BLANK R4127354-3
WG2374030 1x 1002_04 75540 4.12 18796 3.15 66512 6.34
L1784259-01 WG2374030
1x 1002_19 84172 4.12 19863 3.15 73760 6.34
L1784259-02 WG2374030
1x 1002_20 86258 4.12 20750 3.16 79369 6.34
L1784259-03 WG2374030
1x 1002_21 87180 4.12 20605 3.16 77257 6.34
DFB - 1,4-DIFLUOROBENZENE BCM - BROMOCHLOROMETHANE
CB - CHLOROBENZENE-D5
*: Value outside the established quality control limits.
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-1
Lab Sample ID:L1784259-01 SDG:L1784259
Client Sample ID:SV-1 Collected Date/Time:09/30/24 17:03
Lab File ID:1006_13 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS14 Preparation Date/Time:10/06/24 19:57
Analytical Batch:WG2376939 Analysis Date/Time:10/06/24 19:57
Dilution Factor:20 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:10 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
1,1-Dichloroethane 75-34-3 7.03 393 1.45 4.00
cis-1,2-Dichloroethene 156-59-2 7.54 319 1.57 4.00
Tetrachloroethylene 127-18-4 10.74 162 1.63 4.00
Trichloroethylene 79-01-6 8.89 301 1.36 4.00
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-1
Lab Sample ID:L1784259-01 SDG:L1784259
Client Sample ID:SV-1 Collected Date/Time:09/30/24 17:03
Lab File ID:1002_19 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 23:03
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 23:03
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Acetone 67-64-1 2.07 3.99 0.584 1.25
Allyl chloride 107-05-1 0 ND 0.114 0.200
Benzene 71-43-2 3.91 6.29 0.0715 0.200
Benzyl Chloride 100-44-7 0 ND 0.0598 0.200
Bromodichloromethane 75-27-4 0 ND 0.0702 0.200
Bromoform 75-25-2 0 ND 0.0732 0.600
Bromomethane 74-83-9 0 ND 0.0982 0.200
1,3-Butadiene 106-99-0 0 ND 0.104 2.00
Carbon disulfide 75-15-0 2.44 0.627 0.102 0.400
Carbon tetrachloride 56-23-5 0 ND 0.0732 0.200
Chlorobenzene 108-90-7 0 ND 0.0832 0.200
Chloroethane 75-00-3 0 ND 0.0996 0.200
Chloroform 67-66-3 3.22 1.10 0.0717 0.200
Chloromethane 74-87-3 1.70 ND 0.103 0.200
2-Chlorotoluene 95-49-8 0 ND 0.0828 0.200
Cyclohexane 110-82-7 0 ND 0.0753 0.200
Dibromochloromethane 124-48-1 0 ND 0.0727 0.200
1,2-Dibromoethane 106-93-4 0 ND 0.0721 0.200
1,2-Dichlorobenzene 95-50-1 0 ND 0.128 0.200
1,3-Dichlorobenzene 541-73-1 0 ND 0.182 0.200
1,4-Dichlorobenzene 106-46-7 0 ND 0.0557 0.200
1,2-Dichloroethane 107-06-2 0 ND 0.0700 0.200
1,1-Dichloroethene 75-35-4 2.32 14.4 0.0762 0.200
trans-1,2-Dichloroethene 156-60-5 2.66 17.3 0.0673 0.200
1,2-Dichloropropane 78-87-5 4.33 0.811 0.0760 0.200
cis-1,3-Dichloropropene 10061-01-5 0 ND 0.0689 0.200
trans-1,3-Dichloropropene 10061-02-6 0 ND 0.0728 0.200
1,4-Dioxane 123-91-1 0 ND 0.0833 0.630
Ethanol 64-17-5 1.94 5.90 0.265 2.50
Ethylbenzene 100-41-4 6.58 3.30 0.0835 0.200
4-Ethyltoluene 622-96-8 7.56 1.34 0.0783 0.200
Trichlorofluoromethane 75-69-4 2.13 ND 0.0819 0.200
Dichlorodifluoromethane 75-71-8 1.66 0.251 0.137 0.200
1,1,2-Trichlorotrifluoroethane 76-13-1 0 ND 0.0793 0.200
1,2-Dichlorotetrafluoroethane 76-14-2 0 ND 0.0890 0.200
Heptane 142-82-5 4.67 1.32 0.104 0.200
Hexachloro-1,3-butadiene 87-68-3 0 ND 0.105 0.630
n-Hexane 110-54-3 3.20 1.05 0.206 0.630
Isopropylbenzene 98-82-8 7.21 0.425 0.0777 0.200
Methylene Chloride 75-09-2 2.35 0.651 0.0979 0.200
Methyl Butyl Ketone 591-78-6 0 ND 0.133 1.25
2-Butanone (MEK)78-93-3 2.90 ND 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 0 ND 0.0765 1.25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 20 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-1
Lab Sample ID:L1784259-01 SDG:L1784259
Client Sample ID:SV-1 Collected Date/Time:09/30/24 17:03
Lab File ID:1002_19 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 23:03
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 23:03
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Methyl methacrylate 80-62-6 0 ND 0.0876 0.200
MTBE 1634-04-4 2.77 1.36 0.0647 0.200
Naphthalene 91-20-3 9.16 ND 0.350 0.630
2-Propanol 67-63-0 2.14 ND 0.264 1.25
Propene 115-07-1 0 ND 0.0932 1.25
Styrene 100-42-5 6.84 ND 0.0788 0.400
1,1,2,2-Tetrachloroethane 79-34-5 0 ND 0.0743 0.200
Tetrahydrofuran 109-99-9 3.41 0.749 0.0734 0.200
Toluene 108-88-3 5.44 17.9 0.0870 0.500
1,2,4-Trichlorobenzene 120-82-1 0 ND 0.148 0.630
1,1,1-Trichloroethane 71-55-6 3.69 11.1 0.0736 0.200
1,1,2-Trichloroethane 79-00-5 0 ND 0.0775 0.200
1,2,4-Trimethylbenzene 95-63-6 7.82 6.89 0.0764 0.200
1,3,5-Trimethylbenzene 108-67-8 7.60 2.11 0.0779 0.200
2,2,4-Trimethylpentane 540-84-1 4.51 1.27 0.133 0.200
Vinyl chloride 75-01-4 1.76 1.57 0.0949 0.200
Vinyl Bromide 593-60-2 0 ND 0.0852 0.200
Vinyl acetate 108-05-4 0 ND 0.116 0.630
m&p-Xylene 179601-23-1 6.66 10.8 0.135 0.400
o-Xylene 95-47-6 6.90 4.23 0.0828 0.200
TPH (GC/MS) Low Fraction 8006-61-9 5.43 705 39.7 200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 21 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-2
Lab Sample ID:L1784259-02 SDG:L1784259
Client Sample ID:SV-2 Collected Date/Time:09/30/24 16:13
Lab File ID:1006_14 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS14 Preparation Date/Time:10/06/24 20:42
Analytical Batch:WG2376939 Analysis Date/Time:10/06/24 20:42
Dilution Factor:20 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:10 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
1,1-Dichloroethane 75-34-3 7.02 260 1.45 4.00
cis-1,2-Dichloroethene 156-59-2 7.54 990 1.57 4.00
trans-1,2-Dichloroethene 156-60-5 6.61 57.2 1.35 4.00
Tetrachloroethylene 127-18-4 10.74 108 1.63 4.00
Trichloroethylene 79-01-6 8.89 156 1.36 4.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 22 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-2
Lab Sample ID:L1784259-02 SDG:L1784259
Client Sample ID:SV-2 Collected Date/Time:09/30/24 16:13
Lab File ID:1002_20 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 23:32
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 23:32
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Acetone 67-64-1 2.07 5.69 0.584 1.25
Allyl chloride 107-05-1 0 ND 0.114 0.200
Benzene 71-43-2 3.91 1.54 0.0715 0.200
Benzyl Chloride 100-44-7 0 ND 0.0598 0.200
Bromodichloromethane 75-27-4 0 ND 0.0702 0.200
Bromoform 75-25-2 0 ND 0.0732 0.600
Bromomethane 74-83-9 0 ND 0.0982 0.200
1,3-Butadiene 106-99-0 0 ND 0.104 2.00
Carbon disulfide 75-15-0 2.45 0.445 0.102 0.400
Carbon tetrachloride 56-23-5 0 ND 0.0732 0.200
Chlorobenzene 108-90-7 0 ND 0.0832 0.200
Chloroethane 75-00-3 0 ND 0.0996 0.200
Chloroform 67-66-3 3.22 3.26 0.0717 0.200
Chloromethane 74-87-3 1.70 ND 0.103 0.200
2-Chlorotoluene 95-49-8 0 ND 0.0828 0.200
Cyclohexane 110-82-7 4.06 ND 0.0753 0.200
Dibromochloromethane 124-48-1 0 ND 0.0727 0.200
1,2-Dibromoethane 106-93-4 0 ND 0.0721 0.200
1,2-Dichlorobenzene 95-50-1 0 ND 0.128 0.200
1,3-Dichlorobenzene 541-73-1 0 ND 0.182 0.200
1,4-Dichlorobenzene 106-46-7 0 ND 0.0557 0.200
1,2-Dichloroethane 107-06-2 0 ND 0.0700 0.200
1,1-Dichloroethene 75-35-4 2.32 20.4 0.0762 0.200
1,2-Dichloropropane 78-87-5 4.33 0.550 0.0760 0.200
cis-1,3-Dichloropropene 10061-01-5 0 ND 0.0689 0.200
trans-1,3-Dichloropropene 10061-02-6 0 ND 0.0728 0.200
1,4-Dioxane 123-91-1 0 ND 0.0833 0.630
Ethanol 64-17-5 1.94 4.85 0.265 2.50
Ethylbenzene 100-41-4 6.58 0.965 0.0835 0.200
4-Ethyltoluene 622-96-8 7.56 ND 0.0783 0.200
Trichlorofluoromethane 75-69-4 2.13 0.253 0.0819 0.200
Dichlorodifluoromethane 75-71-8 1.66 0.444 0.137 0.200
1,1,2-Trichlorotrifluoroethane 76-13-1 0 ND 0.0793 0.200
1,2-Dichlorotetrafluoroethane 76-14-2 0 ND 0.0890 0.200
Heptane 142-82-5 4.67 0.883 0.104 0.200
Hexachloro-1,3-butadiene 87-68-3 0 ND 0.105 0.630
n-Hexane 110-54-3 3.20 0.671 0.206 0.630
Isopropylbenzene 98-82-8 7.21 ND 0.0777 0.200
Methylene Chloride 75-09-2 2.35 0.777 0.0979 0.200
Methyl Butyl Ketone 591-78-6 0 ND 0.133 1.25
2-Butanone (MEK)78-93-3 2.90 ND 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 0 ND 0.0765 1.25
Methyl methacrylate 80-62-6 0 ND 0.0876 0.200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 23 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-2
Lab Sample ID:L1784259-02 SDG:L1784259
Client Sample ID:SV-2 Collected Date/Time:09/30/24 16:13
Lab File ID:1002_20 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 23:32
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 23:32
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
MTBE 1634-04-4 0 ND 0.0647 0.200
Naphthalene 91-20-3 9.16 ND 0.350 0.630
2-Propanol 67-63-0 2.14 ND 0.264 1.25
Propene 115-07-1 0 ND 0.0932 1.25
Styrene 100-42-5 6.84 ND 0.0788 0.400
1,1,2,2-Tetrachloroethane 79-34-5 0 ND 0.0743 0.200
Tetrahydrofuran 109-99-9 3.41 0.656 0.0734 0.200
Toluene 108-88-3 5.44 6.62 0.0870 0.500
1,2,4-Trichlorobenzene 120-82-1 0 ND 0.148 0.630
1,1,1-Trichloroethane 71-55-6 3.69 10.1 0.0736 0.200
1,1,2-Trichloroethane 79-00-5 0 ND 0.0775 0.200
1,2,4-Trimethylbenzene 95-63-6 7.82 0.501 0.0764 0.200
1,3,5-Trimethylbenzene 108-67-8 7.61 ND 0.0779 0.200
2,2,4-Trimethylpentane 540-84-1 4.51 1.07 0.133 0.200
Vinyl chloride 75-01-4 1.76 ND 0.0949 0.200
Vinyl Bromide 593-60-2 0 ND 0.0852 0.200
Vinyl acetate 108-05-4 0 ND 0.116 0.630
m&p-Xylene 179601-23-1 6.67 2.44 0.135 0.400
o-Xylene 95-47-6 6.90 0.907 0.0828 0.200
TPH (GC/MS) Low Fraction 8006-61-9 5.43 716 39.7 200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 24 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-20
Lab Sample ID:L1784259-03 SDG:L1784259
Client Sample ID:SV-20 Collected Date/Time:09/30/24 16:13
Lab File ID:1006_15 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS14 Preparation Date/Time:10/06/24 21:27
Analytical Batch:WG2376939 Analysis Date/Time:10/06/24 21:27
Dilution Factor:20 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:10 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
1,1-Dichloroethane 75-34-3 7.02 368 1.45 4.00
cis-1,2-Dichloroethene 156-59-2 7.54 1420 1.57 4.00
trans-1,2-Dichloroethene 156-60-5 6.61 82.0 1.35 4.00
Tetrachloroethylene 127-18-4 10.74 158 1.63 4.00
Trichloroethylene 79-01-6 8.89 233 1.36 4.00
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 25 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-20
Lab Sample ID:L1784259-03 SDG:L1784259
Client Sample ID:SV-20 Collected Date/Time:09/30/24 16:13
Lab File ID:1002_21 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS17 Preparation Date/Time:10/03/24 00:00
Analytical Batch:WG2374030 Analysis Date/Time:10/03/24 00:00
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Acetone 67-64-1 2.08 2.92 0.584 1.25
Allyl chloride 107-05-1 0 ND 0.114 0.200
Benzene 71-43-2 3.92 1.55 0.0715 0.200
Benzyl Chloride 100-44-7 0 ND 0.0598 0.200
Bromodichloromethane 75-27-4 0 ND 0.0702 0.200
Bromoform 75-25-2 0 ND 0.0732 0.600
Bromomethane 74-83-9 0 ND 0.0982 0.200
1,3-Butadiene 106-99-0 0 ND 0.104 2.00
Carbon disulfide 75-15-0 2.44 ND 0.102 0.400
Carbon tetrachloride 56-23-5 0 ND 0.0732 0.200
Chlorobenzene 108-90-7 0 ND 0.0832 0.200
Chloroethane 75-00-3 0 ND 0.0996 0.200
Chloroform 67-66-3 3.22 3.36 0.0717 0.200
Chloromethane 74-87-3 0 ND 0.103 0.200
2-Chlorotoluene 95-49-8 0 ND 0.0828 0.200
Cyclohexane 110-82-7 4.05 ND 0.0753 0.200
Dibromochloromethane 124-48-1 0 ND 0.0727 0.200
1,2-Dibromoethane 106-93-4 0 ND 0.0721 0.200
1,2-Dichlorobenzene 95-50-1 0 ND 0.128 0.200
1,3-Dichlorobenzene 541-73-1 0 ND 0.182 0.200
1,4-Dichlorobenzene 106-46-7 0 ND 0.0557 0.200
1,2-Dichloroethane 107-06-2 0 ND 0.0700 0.200
1,1-Dichloroethene 75-35-4 2.32 21.3 0.0762 0.200
1,2-Dichloropropane 78-87-5 4.33 0.518 0.0760 0.200
cis-1,3-Dichloropropene 10061-01-5 0 ND 0.0689 0.200
trans-1,3-Dichloropropene 10061-02-6 0 ND 0.0728 0.200
1,4-Dioxane 123-91-1 0 ND 0.0833 0.630
Ethanol 64-17-5 1.94 2.89 0.265 2.50
Ethylbenzene 100-41-4 6.58 0.967 0.0835 0.200
4-Ethyltoluene 622-96-8 7.56 ND 0.0783 0.200
Trichlorofluoromethane 75-69-4 2.13 0.250 0.0819 0.200
Dichlorodifluoromethane 75-71-8 1.66 0.574 0.137 0.200
1,1,2-Trichlorotrifluoroethane 76-13-1 0 ND 0.0793 0.200
1,2-Dichlorotetrafluoroethane 76-14-2 0 ND 0.0890 0.200
Heptane 142-82-5 4.67 0.782 0.104 0.200
Hexachloro-1,3-butadiene 87-68-3 0 ND 0.105 0.630
n-Hexane 110-54-3 3.20 ND 0.206 0.630
Isopropylbenzene 98-82-8 7.21 ND 0.0777 0.200
Methylene Chloride 75-09-2 2.35 0.354 0.0979 0.200
Methyl Butyl Ketone 591-78-6 0 ND 0.133 1.25
2-Butanone (MEK)78-93-3 2.90 ND 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 0 ND 0.0765 1.25
Methyl methacrylate 80-62-6 0 ND 0.0876 0.200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 26 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET SV-20
Lab Sample ID:L1784259-03 SDG:L1784259
Client Sample ID:SV-20 Collected Date/Time:09/30/24 16:13
Lab File ID:1002_21 Received Date/Time:10/02/24 12:00
Instrument ID:AIRMS17 Preparation Date/Time:10/03/24 00:00
Analytical Batch:WG2374030 Analysis Date/Time:10/03/24 00:00
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
MTBE 1634-04-4 0 ND 0.0647 0.200
Naphthalene 91-20-3 0 ND 0.350 0.630
2-Propanol 67-63-0 2.14 ND 0.264 1.25
Propene 115-07-1 0 ND 0.0932 1.25
Styrene 100-42-5 0 ND 0.0788 0.400
1,1,2,2-Tetrachloroethane 79-34-5 0 ND 0.0743 0.200
Tetrahydrofuran 109-99-9 3.41 0.633 0.0734 0.200
Toluene 108-88-3 5.44 6.99 0.0870 0.500
1,2,4-Trichlorobenzene 120-82-1 0 ND 0.148 0.630
1,1,1-Trichloroethane 71-55-6 3.69 10.5 0.0736 0.200
1,1,2-Trichloroethane 79-00-5 0 ND 0.0775 0.200
1,2,4-Trimethylbenzene 95-63-6 7.82 0.369 0.0764 0.200
1,3,5-Trimethylbenzene 108-67-8 7.61 ND 0.0779 0.200
2,2,4-Trimethylpentane 540-84-1 4.51 1.10 0.133 0.200
Vinyl chloride 75-01-4 1.76 ND 0.0949 0.200
Vinyl Bromide 593-60-2 0 ND 0.0852 0.200
Vinyl acetate 108-05-4 0 ND 0.116 0.630
m&p-Xylene 179601-23-1 6.66 2.62 0.135 0.400
o-Xylene 95-47-6 6.90 1.01 0.0828 0.200
TPH (GC/MS) Low Fraction 8006-61-9 5.43 536 39.7 200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 27 of 57
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS14
Analyte RRF: .19 RRF: .31 RRF: .63 RRF: 1.25 RRF: 2.5 RRF: 3.75 RRF: 10 RRF: 25 RRF: 50 RRF: 100
Analysis date/time 09/30/24
21:51
09/30/24
22:35
09/30/24
23:19
10/01/24
00:05
10/01/24
00:52
10/01/24
01:41
10/01/24
02:26
10/01/24
03:14
10/01/24
04:05
10/01/24
05:04
TRANS-1,2-DICHLOROETHENE 0.3450 0.2940 0.3120 0.3040 0.3060 0.31 0.3090 0.3250 0.3320 0.3440
1,1-DICHLOROETHANE 0.4220 0.3810 0.4030 0.3960 0.4010 0.4080 0.40 0.42 0.4270 0.44
CIS-1,2-DICHLOROETHENE 0.3470 0.2850 0.2990 0.3110 0.31 0.3080 0.2980 0.3130 0.3190 0.33
TRICHLOROETHENE 0.0950 0.08 0.0860 0.0880 0.0850 0.0870 0.0860 0.0880 0.0880 0.0880
TETRACHLOROETHENE 0.1490 0.1190 0.1250 0.1290 0.1270 0.1280 0.1260 0.1260 0.1250 0.1210
1,4-BROMOFLUOROBENZENE 0.6460 0.6430 0.6480 0.6420 0.6430 0.6450 0.6550 0.6540 0.6630 0.6830
File ID:0930A_03 0930A_04 0930A_05 0930A_06 0930A_07 0930A_08 0930A_09 0930A_10 0930A_11 0930A_12
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 28 of 57
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS14
Analyte RRF. Avg %RSD COD
Analysis date/time
TRANS-1,2-DICHLOROETHENE 0.31824 5.45
1,1-DICHLOROETHANE 0.409832 4.26
CIS-1,2-DICHLOROETHENE 0.311944 5.52
TRICHLOROETHENE 0.087101 4.43
TETRACHLOROETHENE 0.127397 6.43
1,4-BROMOFLUOROBENZENE 0.652337 1.96
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 29 of 57
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS17
Analyte RRF: 0.19 RRF: 0.31 RRF: 0.63 RRF: 1.25 RRF: 2.5 RRF: 3.75 RRF: 10.0 RRF: 25 RRF: 50 RRF: 100
Analysis date/time 09/27/24
17:25
09/27/24
17:50
09/27/24
18:15
09/27/24
18:40
09/27/24
19:06
09/27/24
19:34
09/27/24
19:59
09/27/24
20:25
09/27/24
20:55
09/27/24
21:32
DICHLORODIFLUOROMETHANE 0.7860 0.71 0.7920 0.7710 0.7630 0.7440 0.7340 0.74 0.7510 0.7160
1,2-DICHLOROTETRAFLUOROETHANE 0.7580 0.7130 0.8120 0.7420 0.7370 0.7340 0.72 0.7170 0.73 0.6850
CHLOROMETHANE 0.2510 0.2120 0.23 0.2120 0.2140 0.2090 0.2030 0.2040 0.21 0.2040
VINYL CHLORIDE 0.2490 0.2520 0.2850 0.2720 0.2550 0.2520 0.2540 0.2570 0.2610 0.2520
1,3-BUTADIENE 0.2160 0.2260 0.2240 0.2120 0.1990 0.20 0.2020 0.20 0.2070 0.1970
BROMOMETHANE 0.2710 0.2410 0.2680 0.2470 0.2520 0.2560 0.2460 0.2470 0.2550 0.2420
CHLOROETHANE 0.1730 0.15 0.1740 0.1480 0.1490 0.14 0.1410 0.14 0.1440 0.14
VINYL BROMIDE 0.25 0.2670 0.2790 0.2490 0.2650 0.2530 0.2480 0.2550 0.2590 0.2470
TRICHLOROFLUOROMETHANE 0.8250 0.8120 0.8280 0.8130 0.7970 0.82 0.7940 0.7960 0.7980 0.7460
1,1,2-TRICHLOROTRIFLUOROETHANE 0.6150 0.6310 0.6170 0.6050 0.60 0.5930 0.5840 0.5730 0.5790 0.5330
1,1-DICHLOROETHENE 0.5250 0.5250 0.53 0.49 0.4740 0.4880 0.4840 0.4780 0.4860 0.4580
ACETONE 0.1470 0.1550 0.1630 0.1530 0.1390 0.1420 0.14 0.1370 0.1390 0.1340
2-PROPANOL 0.5570 0.5270 0.5550 0.5180 0.4920 0.4810 0.4830 0.4770 0.48 0.46
CARBON DISULFIDE 0.6330 0.6310 0.6590 0.6430 0.6520 0.6550 0.6690 0.6820 0.6970 0.6470
ALLYL CHLORIDE 0.3650 0.3450 0.3710 0.3380 0.3420 0.3270 0.3290 0.3340 0.3460 0.3330
METHYLENE CHLORIDE 0.3520 0.3050 0.3260 0.3240 0.3030 0.2920 0.2870 0.2830 0.2850 0.2690
METHYL TERT-BUTYL ETHER 0.8680 0.8440 0.8960 0.8490 0.8570 0.8510 0.8390 0.8540 0.8760 0.8420
TRANS-1,2-DICHLOROETHENE 0.37 0.3650 0.4010 0.3650 0.3670 0.3680 0.3660 0.3930 0.3680 0.3560
N-HEXANE 0.4520 0.4710 0.4480 0.42 0.4210 0.42 0.4250 0.4250 0.43 0.4070
VINYL ACETATE 0.6390 0.5820 0.6340 0.5860 0.5440 0.5690 0.6050 0.6490 0.6920 0.6860
2-BUTANONE (MEK)0.1590 0.1260 0.15 0.1540 0.1480 0.1520 0.15 0.1530 0.1550 0.15
TETRAHYDROFURAN 0.2550 0.25 0.2790 0.2830 0.2780 0.2850 0.2840 0.2890 0.2960 0.2910
CHLOROFORM 0.6060 0.62 0.67 0.6250 0.6270 0.6210 0.6140 0.6130 0.6190 0.5820
CYCLOHEXANE 0.3770 0.3720 0.3890 0.3770 0.3810 0.3890 0.3890 0.3950 0.4050 0.3910
1,1,1-TRICHLOROETHANE 0.6310 0.6320 0.6470 0.6470 0.6420 0.6370 0.6430 0.6670 0.6790 0.6550
CARBON TETRACHLORIDE 0.6640 0.6150 0.6560 0.6330 0.6550 0.6650 0.67 0.6950 0.7060 0.6810
2,2,4-TRIMETHYLPENTANE 1.5510 1.43 1.4880 1.4610 1.4250 1.4290 1.4270 1.4230 1.4380 1.3730
BENZENE 0.2330 0.2320 0.2370 0.2270 0.2290 0.2290 0.2260 0.2280 0.2270 0.2210
1,2-DICHLOROETHANE 0.0980 0.1040 0.1090 0.1010 0.1010 0.1020 0.10 0.1010 0.1010 0.0970
HEPTANE 0.1230 0.1120 0.13 0.1170 0.1220 0.12 0.12 0.1210 0.1210 0.1170
1,2-DICHLOROPROPANE 0.0950 0.0780 0.0840 0.0810 0.08 0.0790 0.0780 0.0780 0.0770 0.0750
METHYL METHACRYLATE 0.0640 0.0690 0.0820 0.0810 0.0790 0.0820 0.0840 0.0860 0.0880 0.0870
1,4-DIOXANE 0.0420 0.0420 0.0510 0.05 0.05 0.05 0.0530 0.0540 0.0530 0.0510
BROMODICHLOROMETHANE 0.1370 0.1260 0.1340 0.1360 0.1410 0.1460 0.1490 0.1570 0.1590 0.1550
CIS-1,3-DICHLOROPROPENE 0.1090 0.1140 0.1260 0.1170 0.1230 0.1240 0.1330 0.1410 0.1460 0.1460
4-METHYL-2-PENTANONE (MIBK)0.2590 0.2360 0.2530 0.2430 0.2320 0.2370 0.2410 0.2310 0.23 0.2260
TOLUENE 0.2870 0.2810 0.2810 0.2750 0.2790 0.2720 0.2810 0.2850 0.2890 0.2810
TRANS-1,3-DICHLOROPROPENE 0.0750 0.08 0.0950 0.09 0.0920 0.0970 0.1020 0.1120 0.1180 0.1190
1,1,2-TRICHLOROETHANE 0.1040 0.1020 0.1010 0.0980 0.0940 0.0980 0.0960 0.0960 0.0960 0.0940
METHYL BUTYL KETONE 0.1340 0.14 0.1530 0.1340 0.1450 0.1470 0.1560 0.1570 0.1580 0.1570
CHLORODIBROMOMETHANE 0.1140 0.1190 0.1340 0.1310 0.1340 0.1380 0.1490 0.16 0.1650 0.1620
1,2-DIBROMOETHANE 0.1370 0.1370 0.1480 0.1390 0.1470 0.1540 0.1490 0.1530 0.1540 0.1510
CHLOROBENZENE 0.2310 0.2280 0.2490 0.2250 0.23 0.2220 0.2260 0.2290 0.23 0.2230
ETHYLBENZENE 0.4110 0.3810 0.4030 0.3940 0.4050 0.3980 0.4150 0.4290 0.4220 0.4170
M&P-XYLENE 0.3220 0.3120 0.3240 0.3150 0.3330 0.3320 0.3490 0.3580 0.3450 0.33
O-XYLENE 0.3070 0.2960 0.3340 0.3330 0.3410 0.3340 0.3440 0.3480 0.3320 0.3190
STYRENE 0.2280 0.2130 0.2350 0.2380 0.2550 0.26 0.27 0.2760 0.2660 0.2520
BROMOFORM 0.13 0.1270 0.1380 0.1270 0.1410 0.1460 0.1710 0.1880 0.19 0.1870
ISOPROPYLBENZENE 0.4670 0.4380 0.4910 0.4610 0.4690 0.4680 0.4790 0.4940 0.4860 0.47
1,1,2,2-TETRACHLOROETHANE 0.2540 0.2330 0.2510 0.2420 0.2440 0.2410 0.2390 0.2410 0.23 0.22
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS17
Analyte RRF: 0.19 RRF: 0.31 RRF: 0.63 RRF: 1.25 RRF: 2.5 RRF: 3.75 RRF: 10.0 RRF: 25 RRF: 50 RRF: 100
Analysis date/time 09/27/24
17:25
09/27/24
17:50
09/27/24
18:15
09/27/24
18:40
09/27/24
19:06
09/27/24
19:34
09/27/24
19:59
09/27/24
20:25
09/27/24
20:55
09/27/24
21:32
4-ETHYLTOLUENE 0.4630 0.4340 0.4770 0.49 0.5130 0.5090 0.5270 0.5430 0.5270 0.5130
2-CHLOROTOLUENE 0.3730 0.3420 0.3760 0.37 0.3690 0.3610 0.3710 0.3830 0.3740 0.3660
1,3,5-TRIMETHYLBENZENE 0.4060 0.3760 0.3990 0.4190 0.4320 0.4410 0.4450 0.4530 0.4450 0.4310
1,2,4-TRIMETHYLBENZENE 0.3680 0.41 0.4140 0.4120 0.4390 0.4390 0.4520 0.4650 0.45 0.4310
1,3-DICHLOROBENZENE 0.31 0.3180 0.3260 0.3230 0.3310 0.3170 0.3160 0.3230 0.3120 0.2970
1,4-DICHLOROBENZENE 0.3220 0.2990 0.3390 0.3220 0.3170 0.3190 0.3240 0.3280 0.3140 0.3020
BENZYL CHLORIDE 0.2140 0.1930 0.2230 0.2120 0.2250 0.24 0.2920 0.3540 0.3660 0.3810
1,2-DICHLOROBENZENE 0.2980 0.2740 0.3040 0.2880 0.2920 0.2880 0.29 0.2970 0.2860 0.2830
1,2,4-TRICHLOROBENZENE 0.29 0.25 0.2990 0.3050 0.2950 0.3110 0.3150 0.3430 0.3450 0.3550
HEXACHLORO-1,3-BUTADIENE 0.2910 0.2770 0.2860 0.2890 0.2950 0.3010 0.2980 0.3170 0.3110 0.3050
NAPHTHALENE 0.4680 0.4750 0.5220 0.5740 0.5850 0.6290 0.6570 0.7140 0.7370 0.7530
1,4-BROMOFLUOROBENZENE 0.7480 0.74 0.7540 0.7650 0.7610 0.7650 0.7630 0.7650 0.7540 0.7630
PROPENE 0.3710 0.2870 0.24 0.2450 0.2360 0.23 0.2280 0.2350 0.2280
ETHANOL 0.1140 0.1120 0.1040 0.1070 0.1070 0.1010 0.1020 0.1050 0.1030
TPH (GC/MS) LOW FRACTION 5.8020 4.4850 4.0710 3.5420 3.39 3.3840 3.2060
File ID:0927A_03 0927A_04 0927A_05 0927A_06 0927A_07 0927A_08 0927A_09 0927A_10 0927A_11 0927A_12
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS17
Analyte RRF. Avg %RSD COD
Analysis date/time
DICHLORODIFLUOROMETHANE 0.750639 3.66
1,2-DICHLOROTETRAFLUOROETHANE 0.734668 4.55
CHLOROMETHANE 0.21492 6.83
VINYL CHLORIDE 0.258782 4.39
1,3-BUTADIENE 0.208322 5.15
BROMOMETHANE 0.252515 4.07
CHLOROETHANE 0.149828 8.54
VINYL BROMIDE 0.257153 4.08
TRICHLOROFLUOROMETHANE 0.802932 2.93
1,1,2-TRICHLOROTRIFLUOROETHANE 0.592946 4.69
1,1-DICHLOROETHENE 0.493813 4.96
ACETONE 0.144952 6.49
2-PROPANOL 0.503072 6.79
CARBON DISULFIDE 0.656881 3.16
ALLYL CHLORIDE 0.343121 4.32
METHYLENE CHLORIDE 0.302533 8.22
METHYL TERT-BUTYL ETHER 0.857628 2.06
TRANS-1,2-DICHLOROETHENE 0.371982 3.74
N-HEXANE 0.43199 4.47
VINYL ACETATE 0.618707 8.01
2-BUTANONE (MEK)0.149659 6.07
TETRAHYDROFURAN 0.27895 5.4
CHLOROFORM 0.619681 3.56
CYCLOHEXANE 0.386461 2.55
1,1,1-TRICHLOROETHANE 0.648112 2.38
CARBON TETRACHLORIDE 0.663959 4.05
2,2,4-TRIMETHYLPENTANE 1.444457 3.29
BENZENE 0.228792 1.97
1,2-DICHLOROETHANE 0.101509 3.2
HEPTANE 0.120159 3.75
1,2-DICHLOROPROPANE 0.080571 6.95
METHYL METHACRYLATE 0.080036 9.87
1,4-DIOXANE 0.049438 8.47
BROMODICHLOROMETHANE 0.143883 7.76
CIS-1,3-DICHLOROPROPENE 0.127951 10.38
4-METHYL-2-PENTANONE (MIBK)0.238717 4.38
TOLUENE 0.281212 1.82
TRANS-1,3-DICHLOROPROPENE 0.098028 15.27
1,1,2-TRICHLOROETHANE 0.097998 3.34
METHYL BUTYL KETONE 0.148072 6.25
CHLORODIBROMOMETHANE 0.140622 12.61
1,2-DIBROMOETHANE 0.146834 4.67
CHLOROBENZENE 0.229233 3.31
ETHYLBENZENE 0.407528 3.52
M&P-XYLENE 0.331978 4.45
O-XYLENE 0.328739 5.02
STYRENE 0.249369 8
BROMOFORM 0.154423 17.22
ISOPROPYLBENZENE 0.472383 3.46
1,1,2,2-TETRACHLOROETHANE 0.23945 4.15
4-ETHYLTOLUENE 0.499794 6.7
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 32 of 57
6A-OR GC/MS INITIAL CALIBRATION DATA
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS17
Analyte RRF. Avg %RSD COD
Analysis date/time
2-CHLOROTOLUENE 0.368387 2.96
1,3,5-TRIMETHYLBENZENE 0.424726 5.75
1,2,4-TRIMETHYLBENZENE 0.427778 6.56
1,3-DICHLOROBENZENE 0.317444 3.06
1,4-DICHLOROBENZENE 0.318559 3.71
BENZYL CHLORIDE 0.269896 26.68
1,2-DICHLOROBENZENE 0.290095 2.92
1,2,4-TRICHLOROBENZENE 0.310827 10
HEXACHLORO-1,3-BUTADIENE 0.297008 4.08
NAPHTHALENE 0.611294 17.08
1,4-BROMOFLUOROBENZENE 0.757842 1.13
PROPENE 0.255611 18.34
ETHANOL 0.10612 4.21
TPH (GC/MS) LOW FRACTION 3.982962 23.09
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 33 of 57
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/30/24 21:51
Instrument ID:AIRMS14 Calibration (end) date/time:10/01/24 05:04
Lab File ID:0930A_14 Analysis date/time:10/01/24 06:43
Analytical Method:TO-15 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
1,1,1-TRICHLOROETHANE 0.567519 0.57848730 1.93 10 10.19 102 60 - 140
1,1,2,2-TETRACHLOROETHANE 0.186860 0.18891640 1.10 10 10.11 101 60 - 140
1,1,2-TRICHLOROETHANE 0.083789 0.08719360 4.06 10 10.41 104 60 - 140
1,1,2-TRICHLOROTRIFLUOROETHANE 0.510029 0.53754610 5.40 10 10.54 105 60 - 140
1,1-DICHLOROETHANE 0.409832 0.42720910 4.24 10 10.42 104 60 - 140
1,1-DICHLOROETHENE 0.370472 0.37499590 1.22 10 10.12 101 60 - 140
1,2,4-TRICHLOROBENZENE 0.178632 0.20117930 12.60 10 11.26 113 60 - 140
1,2,4-TRIMETHYLBENZENE 0.313902 0.317537 1.16 10 10.12 101 60 - 140
1,2-DIBROMOETHANE 0.140932 0.14391410 2.12 10 10.21 102 60 - 140
1,2-DICHLOROBENZENE 0.202329 0.20623890 1.93 10 10.19 102 60 - 140
1,2-DICHLOROETHANE 0.0817 0.08449854 3.43 10 10.34 103 60 - 140
1,2-DICHLOROPROPANE 0.064969 0.06518160 0.3270 10 10.03 100 60 - 140
1,2-DICHLOROTETRAFLUOROETHANE 0.562985 0.49156770 12.70 10 8.731 87.30 60 - 140
1,3,5-TRIMETHYLBENZENE 0.303524 0.312993 3.12 10 10.31 103 60 - 140
1,3-BUTADIENE 0.104694 0.11359270 8.50 10 10.85 109 60 - 140
1,3-DICHLOROBENZENE 0.218547 0.22417440 2.57 10 10.26 103 60 - 140
1,4-DICHLOROBENZENE 0.217867 0.21959090 0.7910 10 10.08 101 60 - 140
1,4-DIOXANE 0.042611 0.04176643 1.98 10 9.802 98 60 - 140
2,2,4-TRIMETHYLPENTANE 1.120895 1.130738 0.8780 10 10.09 101 60 - 140
2-BUTANONE (MEK)0.103776 0.10959320 5.61 10 10.56 106 60 - 140
2-CHLOROTOLUENE 0.297659 0.30387130 2.09 10 10.21 102 60 - 140
2-PROPANOL 0.384595 0.44301230 15.20 10 11.52 115 60 - 140
4-ETHYLTOLUENE 0.377283 0.38204350 1.26 10 10.13 101 60 - 140
4-METHYL-2-PENTANONE (MIBK)0.137720 0.13517320 1.85 10 9.815 98.10 60 - 140
ACETONE 0.096641 0.09299017 3.78 10 9.622 96.20 60 - 140
ALLYL CHLORIDE 0.287733 0.29332960 1.95 10 10.19 102 60 - 140
BENZENE 0.183367 0.185471 1.15 10 10.11 101 60 - 140
BENZYL CHLORIDE 0.268953 0.24724860 8.07 10 9.193 91.90 60 - 140
BROMODICHLOROMETHANE 0.138405 0.13939030 0.7120 10 10.07 101 60 - 140
BROMOFORM 0.162487 0.15251110 6.14 10 9.386 93.90 60 - 140
BROMOMETHANE 0.141962 0.14618920 2.98 10 10.30 103 60 - 140
CARBON DISULFIDE 0.703674 0.73979660 5.13 10 10.51 105 60 - 140
CARBON TETRACHLORIDE 0.625043 0.64767550 3.62 10 10.36 104 60 - 140
CHLOROBENZENE 0.202863 0.20469180 0.9010 10 10.09 101 60 - 140
CHLORODIBROMOMETHANE 0.157261 0.15607050 0.7570 10 9.924 99.20 60 - 140
CHLOROETHANE 0.078937 0.07161372 9.28 10 9.072 90.70 60 - 140
CHLOROFORM 0.513634 0.51984480 1.21 10 10.12 101 60 - 140
CHLOROMETHANE 0.147767 0.14267830 3.44 10 9.656 96.60 60 - 140
CIS-1,2-DICHLOROETHENE 0.311944 0.31511250 1.02 10 10.10 101 60 - 140
CIS-1,3-DICHLOROPROPENE 0.127077 0.128933 1.46 10 10.15 102 60 - 140
CYCLOHEXANE 0.307280 0.31490060 2.48 10 10.25 103 60 - 140
DICHLORODIFLUOROMETHANE 0.512501 0.43198690 15.70 10 8.429 84.30 60 - 140
ETHANOL 0.086227 0.08657810 0.4070 10 10.04 100 60 - 140
ETHYLBENZENE 0.348659 0.35008230 0.4080 10 10.04 100 60 - 140
HEPTANE 0.053971 0.05502030 1.94 10 10.19 102 60 - 140
HEXACHLORO-1,3-BUTADIENE 0.163871 0.17282260 5.46 10 10.55 106 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/30/24 21:51
Instrument ID:AIRMS14 Calibration (end) date/time:10/01/24 05:04
Lab File ID:0930A_14 Analysis date/time:10/01/24 06:43
Analytical Method:TO-15 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
ISOPROPYLBENZENE 0.371371 0.37603520 1.26 10 10.13 101 60 - 140
M&P-XYLENE 0.276423 0.27893340 0.9080 20 20.18 101 60 - 140
METHYL BUTYL KETONE 0.132085 0.13454780 1.86 10 10.19 102 60 - 140
METHYL METHACRYLATE 0.065763 0.06727283 2.30 10 10.23 102 60 - 140
METHYL TERT-BUTYL ETHER 0.643996 0.65100040 1.09 10 10.11 101 60 - 140
METHYLENE CHLORIDE 0.287106 0.25024380 12.80 10 8.716 87.20 60 - 140
N-HEXANE 0.323134 0.32405390 0.2850 10 10.03 100 60 - 140
NAPHTHALENE 0.392871 0.461363 17.40 10 11.74 117 60 - 140
O-XYLENE 0.276078 0.28417410 2.93 10 10.29 103 60 - 140
PROPENE 0.159586 0.15511330 2.80 10 9.720 97.20 60 - 140
STYRENE 0.215048 0.22182170 3.15 10 10.31 103 60 - 140
TETRACHLOROETHENE 0.127397 0.12709460 0.2370 10 9.976 99.80 60 - 140
TETRAHYDROFURAN 0.238683 0.23824980 0.1810 10 9.982 99.80 60 - 140
TOLUENE 0.260142 0.24730720 4.93 10 9.507 95.10 60 - 140
TPH (GC/MS) LOW FRACTION 2.120709 1.987289 6.29 470 440.4 93.70 60 - 140
TRANS-1,2-DICHLOROETHENE 0.318240 0.32890510 3.35 10 10.34 103 60 - 140
TRANS-1,3-DICHLOROPROPENE 0.103310 0.10405420 0.72 10 10.07 101 60 - 140
TRICHLOROETHENE 0.087101 0.09002261 3.35 10 10.34 103 60 - 140
TRICHLOROFLUOROMETHANE 0.606307 0.61973570 2.21 10 10.22 102 60 - 140
VINYL ACETATE 0.524864 0.53339530 1.63 10 10.16 102 60 - 140
VINYL BROMIDE 0.193213 0.19293290 0.1450 10 9.985 99.80 60 - 140
VINYL CHLORIDE 0.137770 0.14926770 8.35 10 10.83 108 60 - 140
1,4-BROMOFLUOROBENZENE 0.652337 0.66324480 1.67 4 4.067 102 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/30/24 21:51
Instrument ID:AIRMS14 Calibration (end) date/time:10/01/24 05:04
Lab File ID:1006_01 Analysis date/time:10/06/24 08:30
Analytical Method:TO-15 Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
1,1,1-TRICHLOROETHANE 0.567519 0.60598710 6.78 3.75 4.004 107 70 - 130
1,1,2,2-TETRACHLOROETHANE 0.186860 0.202678 8.47 3.75 4.067 108 70 - 130
1,1,2-TRICHLOROETHANE 0.083789 0.09812733 17.10 3.75 4.392 117 70 - 130
1,1,2-TRICHLOROTRIFLUOROETHANE 0.510029 0.57406030 12.60 3.75 4.221 113 70 - 130
1,1-DICHLOROETHANE 0.409832 0.45064220 9.96 3.75 4.123 110 70 - 130
1,1-DICHLOROETHENE 0.370472 0.39208020 5.83 3.75 3.969 106 70 - 130
1,2,4-TRICHLOROBENZENE 0.178632 0.20967190 17.40 3.75 4.402 117 70 - 130
1,2,4-TRIMETHYLBENZENE 0.313902 0.34336830 9.39 3.75 4.102 109 70 - 130
1,2-DIBROMOETHANE 0.140932 0.16409040 16.40 3.75 4.366 116 70 - 130
1,2-DICHLOROBENZENE 0.202329 0.22240050 9.92 3.75 4.122 110 70 - 130
1,2-DICHLOROETHANE 0.0817 0.08593062 5.18 3.75 3.944 105 70 - 130
1,2-DICHLOROPROPANE 0.064969 0.07292321 12.20 3.75 4.209 112 70 - 130
1,2-DICHLOROTETRAFLUOROETHANE 0.562985 0.52737560 6.33 3.75 3.513 93.70 70 - 130
1,3,5-TRIMETHYLBENZENE 0.303524 0.33590950 10.70 3.75 4.150 111 70 - 130
1,3-BUTADIENE 0.104694 0.13595530 29.90 3.75 4.870 130 70 - 130
1,3-DICHLOROBENZENE 0.218547 0.24240040 10.90 3.75 4.159 111 70 - 130
1,4-DICHLOROBENZENE 0.217867 0.24349670 11.80 3.75 4.191 112 70 - 130
1,4-DIOXANE 0.042611 0.04826945 13.30 3.75 4.248 113 70 - 130
2,2,4-TRIMETHYLPENTANE 1.120895 1.142601 1.94 3.75 3.823 102 70 - 130
2-BUTANONE (MEK)0.103776 0.14902550 43.60 3.75 5.385 144 70 - 130
2-CHLOROTOLUENE 0.297659 0.32248010 8.34 3.75 4.063 108 70 - 130
2-PROPANOL 0.384595 0.398095 3.51 3.75 3.882 104 70 - 130
4-ETHYLTOLUENE 0.377283 0.40386430 7.05 3.75 4.014 107 70 - 130
4-METHYL-2-PENTANONE (MIBK)0.137720 0.14769520 7.24 3.75 4.022 107 70 - 130
ACETONE 0.096641 0.10308950 6.67 3.75 4.000 107 70 - 130
ALLYL CHLORIDE 0.287733 0.28711260 0.2160 3.75 3.742 99.80 70 - 130
BENZENE 0.183367 0.19626780 7.04 3.75 4.014 107 70 - 130
BENZYL CHLORIDE 0.268953 0.29259990 8.79 3.75 4.080 109 70 - 130
BROMODICHLOROMETHANE 0.138405 0.15346240 10.90 3.75 4.158 111 70 - 130
BROMOFORM 0.162487 0.17939270 10.40 3.75 4.140 110 70 - 130
BROMOMETHANE 0.141962 0.18501290 30.30 3.75 4.887 130 70 - 130
CARBON DISULFIDE 0.703674 0.77817090 10.60 7.50 8.294 111 70 - 130
CARBON TETRACHLORIDE 0.625043 0.674485 7.91 3.75 4.047 108 70 - 130
CHLOROBENZENE 0.202863 0.22761480 12.20 3.75 4.208 112 70 - 130
CHLORODIBROMOMETHANE 0.157261 0.18054490 14.80 3.75 4.305 115 70 - 130
CHLOROETHANE 0.078937 0.08453745 7.09 3.75 4.016 107 70 - 130
CHLOROFORM 0.513634 0.548694 6.83 3.75 4.006 107 70 - 130
CHLOROMETHANE 0.147767 0.18017820 21.90 3.75 4.573 122 70 - 130
CIS-1,2-DICHLOROETHENE 0.311944 0.33358160 6.94 3.75 4.010 107 70 - 130
CIS-1,3-DICHLOROPROPENE 0.127077 0.14066590 10.70 3.75 4.151 111 70 - 130
CYCLOHEXANE 0.307280 0.32681810 6.36 3.75 3.988 106 70 - 130
DICHLORODIFLUOROMETHANE 0.512501 0.43974190 14.20 3.75 3.218 85.80 70 - 130
ETHANOL 0.086227 0.09352162 8.46 3.75 4.067 108 70 - 130
ETHYLBENZENE 0.348659 0.38231350 9.65 3.75 4.112 110 70 - 130
HEPTANE 0.053971 0.05886453 9.07 3.75 4.090 109 70 - 130
HEXACHLORO-1,3-BUTADIENE 0.163871 0.18596680 13.50 3.75 4.256 113 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 36 of 57
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/30/24 21:51
Instrument ID:AIRMS14 Calibration (end) date/time:10/01/24 05:04
Lab File ID:1006_01 Analysis date/time:10/06/24 08:30
Analytical Method:TO-15 Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
ISOPROPYLBENZENE 0.371371 0.39887560 7.41 3.75 4.028 107 70 - 130
M&P-XYLENE 0.276423 0.30008120 8.56 7.50 8.142 109 70 - 130
METHYL BUTYL KETONE 0.132085 0.14174350 7.31 3.75 4.024 107 70 - 130
METHYL METHACRYLATE 0.065763 0.07331208 11.50 3.75 4.180 111 70 - 130
METHYL TERT-BUTYL ETHER 0.643996 0.68977590 7.11 3.75 4.017 107 70 - 130
METHYLENE CHLORIDE 0.287106 0.26820530 6.58 3.75 3.503 93.40 70 - 130
N-HEXANE 0.323134 0.33962180 5.10 3.75 3.941 105 70 - 130
NAPHTHALENE 0.392871 0.45681130 16.30 3.75 4.360 116 70 - 130
O-XYLENE 0.276078 0.29809510 7.97 3.75 4.049 108 70 - 130
PROPENE 0.159586 0.192119 20.40 3.75 4.514 120 70 - 130
STYRENE 0.215048 0.24087220 12 7.50 8.401 112 70 - 130
TETRACHLOROETHENE 0.127397 0.14290680 12.20 3.75 4.207 112 70 - 130
TETRAHYDROFURAN 0.238683 0.25175970 5.48 3.75 3.955 105 70 - 130
TOLUENE 0.260142 0.27393990 5.30 3.75 3.949 105 70 - 130
TPH (GC/MS) LOW FRACTION 2.120709 2.323415 9.56 176.25 193.1 110 70 - 130
TRANS-1,2-DICHLOROETHENE 0.318240 0.33558650 5.45 3.75 3.954 105 70 - 130
TRANS-1,3-DICHLOROPROPENE 0.103310 0.11480260 11.10 3.75 4.167 111 70 - 130
TRICHLOROETHENE 0.087101 0.10392410 19.30 3.75 4.474 119 70 - 130
TRICHLOROFLUOROMETHANE 0.606307 0.69811280 15.10 3.75 4.318 115 70 - 130
VINYL ACETATE 0.524864 0.51870870 1.17 3.75 3.706 98.80 70 - 130
VINYL BROMIDE 0.193213 0.23856260 23.50 3.75 4.630 123 70 - 130
VINYL CHLORIDE 0.137770 0.19190330 39.30 3.75 5.223 139 70 - 130
1,4-BROMOFLUOROBENZENE 0.652337 0.61435540 5.82 4 3.767 94.20 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 37 of 57
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/27/24 17:25
Instrument ID:AIRMS17 Calibration (end) date/time:09/27/24 21:32
Lab File ID:0927A_14 Analysis date/time:09/27/24 22:27
Analytical Method:TO-15 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
1,1,1-TRICHLOROETHANE 0.648112 0.65465830 1.01 10 10.10 101 60 - 140
1,1,2,2-TETRACHLOROETHANE 0.239450 0.23839070 0.4420 10 9.956 99.60 60 - 140
1,1,2-TRICHLOROETHANE 0.097998 0.09698846 1.03 10 9.897 99 60 - 140
1,1,2-TRICHLOROTRIFLUOROETHANE 0.592946 0.600183 1.22 10 10.12 101 60 - 140
1,1-DICHLOROETHANE 0.553609 0.552340 0.2290 10 9.977 99.80 60 - 140
1,1-DICHLOROETHENE 0.493813 0.488083 1.16 10 9.884 98.80 60 - 140
1,2,4-TRICHLOROBENZENE 0.310827 0.296880 4.49 10 9.551 95.50 60 - 140
1,2,4-TRIMETHYLBENZENE 0.427778 0.44096190 3.08 10 10.31 103 60 - 140
1,2-DIBROMOETHANE 0.146834 0.14564890 0.8070 10 9.919 99.20 60 - 140
1,2-DICHLOROBENZENE 0.290095 0.27573570 4.95 10 9.505 95.10 60 - 140
1,2-DICHLOROETHANE 0.101509 0.09717350 4.27 10 9.573 95.70 60 - 140
1,2-DICHLOROPROPANE 0.080571 0.07693296 4.52 10 9.548 95.50 60 - 140
1,2-DICHLOROTETRAFLUOROETHANE 0.734668 0.72884010 0.7930 10 9.921 99.20 60 - 140
1,3,5-TRIMETHYLBENZENE 0.424726 0.42972210 1.18 10 10.12 101 60 - 140
1,3-BUTADIENE 0.208322 0.20761060 0.3410 10 9.966 99.70 60 - 140
1,3-DICHLOROBENZENE 0.317444 0.30385030 4.28 10 9.572 95.70 60 - 140
1,4-DICHLOROBENZENE 0.318559 0.30692280 3.65 10 9.635 96.40 60 - 140
1,4-DIOXANE 0.049438 0.05224024 5.67 10 10.57 106 60 - 140
2,2,4-TRIMETHYLPENTANE 1.444457 1.464854 1.41 10 10.14 101 60 - 140
2-BUTANONE (MEK)0.149659 0.15407370 2.95 10 10.29 103 60 - 140
2-CHLOROTOLUENE 0.368387 0.36579670 0.7030 10 9.930 99.30 60 - 140
2-PROPANOL 0.503072 0.50712160 0.8050 10 10.08 101 60 - 140
4-ETHYLTOLUENE 0.499794 0.50687090 1.42 10 10.14 101 60 - 140
4-METHYL-2-PENTANONE (MIBK)0.238717 0.236584 0.8940 10 9.911 99.10 60 - 140
ACETONE 0.144952 0.14147680 2.40 10 9.760 97.60 60 - 140
ALLYL CHLORIDE 0.343121 0.36098450 5.21 10 10.52 105 60 - 140
BENZENE 0.228792 0.22580670 1.30 10 9.870 98.70 60 - 140
BENZYL CHLORIDE 0.269896 0.28213990 4.54 10 10.45 104 60 - 140
BROMODICHLOROMETHANE 0.143883 0.14662690 1.91 10 10.19 102 60 - 140
BROMOFORM 0.154423 0.15275050 1.08 10 9.892 98.90 60 - 140
BROMOMETHANE 0.252515 0.25941390 2.73 10 10.27 103 60 - 140
CARBON DISULFIDE 0.656881 0.63776690 2.91 10 9.709 97.10 60 - 140
CARBON TETRACHLORIDE 0.663959 0.66922740 0.7930 10 10.08 101 60 - 140
CHLOROBENZENE 0.229233 0.22106380 3.56 10 9.644 96.40 60 - 140
CHLORODIBROMOMETHANE 0.140622 0.14428560 2.61 10 10.26 103 60 - 140
CHLOROETHANE 0.149828 0.14725040 1.72 10 9.828 98.30 60 - 140
CHLOROFORM 0.619681 0.61182550 1.27 10 9.873 98.70 60 - 140
CHLOROMETHANE 0.214920 0.21104620 1.80 10 9.820 98.20 60 - 140
CIS-1,2-DICHLOROETHENE 0.390936 0.39880710 2.01 10 10.20 102 60 - 140
CIS-1,3-DICHLOROPROPENE 0.127951 0.13395390 4.69 10 10.47 105 60 - 140
CYCLOHEXANE 0.386461 0.40384910 4.50 10 10.45 104 60 - 140
DICHLORODIFLUOROMETHANE 0.750639 0.74460210 0.8040 10 9.920 99.20 60 - 140
ETHANOL 0.106120 0.11507420 8.44 10 10.84 108 60 - 140
ETHYLBENZENE 0.407528 0.41184040 1.06 10 10.11 101 60 - 140
HEPTANE 0.120159 0.12200970 1.54 10 10.15 102 60 - 140
HEXACHLORO-1,3-BUTADIENE 0.297008 0.28439130 4.25 10 9.575 95.80 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 38 of 57
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/27/24 17:25
Instrument ID:AIRMS17 Calibration (end) date/time:09/27/24 21:32
Lab File ID:0927A_14 Analysis date/time:09/27/24 22:27
Analytical Method:TO-15 Sample ID:SSCV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
ISOPROPYLBENZENE 0.472383 0.47379980 0.30 10 10.03 100 60 - 140
M&P-XYLENE 0.331978 0.34181110 2.96 20 20.59 103 60 - 140
METHYL BUTYL KETONE 0.148072 0.15613160 5.44 10 10.54 105 60 - 140
METHYL METHACRYLATE 0.080036 0.08423239 5.24 10 10.52 105 60 - 140
METHYL TERT-BUTYL ETHER 0.857628 0.864925 0.8510 10 10.09 101 60 - 140
METHYLENE CHLORIDE 0.302533 0.29108120 3.79 10 9.621 96.20 60 - 140
N-HEXANE 0.431990 0.43697960 1.16 10 10.12 101 60 - 140
NAPHTHALENE 0.611294 0.65011020 6.35 10 10.63 106 60 - 140
O-XYLENE 0.328739 0.33425090 1.68 10 10.17 102 60 - 140
PROPENE 0.255611 0.24039130 5.95 10 9.405 94 60 - 140
STYRENE 0.249369 0.25460010 2.10 10 10.21 102 60 - 140
TETRACHLOROETHENE 0.148092 0.142760 3.60 10 9.640 96.40 60 - 140
TETRAHYDROFURAN 0.278950 0.29430990 5.51 10 10.55 106 60 - 140
TOLUENE 0.281212 0.27622680 1.77 10 9.823 98.20 60 - 140
TPH (GC/MS) LOW FRACTION 3.982962 3.465775 13 470 409.0 87 60 - 140
TRANS-1,2-DICHLOROETHENE 0.371982 0.36379980 2.20 10 9.780 97.80 60 - 140
TRANS-1,3-DICHLOROPROPENE 0.098028 0.10483550 6.94 10 10.69 107 60 - 140
TRICHLOROETHENE 0.101684 0.09793252 3.69 10 9.631 96.30 60 - 140
TRICHLOROFLUOROMETHANE 0.802932 0.78867550 1.78 10 9.822 98.20 60 - 140
VINYL ACETATE 0.618707 0.66059090 6.77 10 10.68 107 60 - 140
VINYL BROMIDE 0.257153 0.25634420 0.3150 10 9.969 99.70 60 - 140
VINYL CHLORIDE 0.258782 0.26354930 1.84 10 10.18 102 60 - 140
1,4-BROMOFLUOROBENZENE 0.757842 0.74653210 1.49 4 3.940 98.50 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 39 of 57
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/27/24 17:25
Instrument ID:AIRMS17 Calibration (end) date/time:09/27/24 21:32
Lab File ID:1002_01 Analysis date/time:10/02/24 08:36
Analytical Method:TO-15 Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
1,1,1-TRICHLOROETHANE 0.648112 0.78142020 20.60 3.75 4.521 121 70 - 130
1,1,2,2-TETRACHLOROETHANE 0.239450 0.27674040 15.60 3.75 4.334 116 70 - 130
1,1,2-TRICHLOROETHANE 0.097998 0.11306410 15.40 3.75 4.327 115 70 - 130
1,1,2-TRICHLOROTRIFLUOROETHANE 0.592946 0.68585820 15.70 3.75 4.338 116 70 - 130
1,1-DICHLOROETHANE 0.553609 0.59720440 7.87 3.75 4.045 108 70 - 130
1,1-DICHLOROETHENE 0.493813 0.55696480 12.80 3.75 4.230 113 70 - 130
1,2,4-TRICHLOROBENZENE 0.310827 0.35203890 13.30 3.75 4.247 113 70 - 130
1,2,4-TRIMETHYLBENZENE 0.427778 0.50602240 18.30 3.75 4.436 118 70 - 130
1,2-DIBROMOETHANE 0.146834 0.16424350 11.90 3.75 4.195 112 70 - 130
1,2-DICHLOROBENZENE 0.290095 0.334993 15.50 3.75 4.330 115 70 - 130
1,2-DICHLOROETHANE 0.101509 0.12385530 22 3.75 4.576 122 70 - 130
1,2-DICHLOROPROPANE 0.080571 0.08866229 10 3.75 4.127 110 70 - 130
1,2-DICHLOROTETRAFLUOROETHANE 0.734668 0.83818160 14.10 3.75 4.278 114 70 - 130
1,3,5-TRIMETHYLBENZENE 0.424726 0.50030790 17.80 3.75 4.417 118 70 - 130
1,3-BUTADIENE 0.208322 0.22416750 7.61 3.75 4.035 108 70 - 130
1,3-DICHLOROBENZENE 0.317444 0.37055020 16.70 3.75 4.377 117 70 - 130
1,4-DICHLOROBENZENE 0.318559 0.377730 18.60 3.75 4.447 119 70 - 130
1,4-DIOXANE 0.049438 0.05590232 13.10 3.75 4.240 113 70 - 130
2,2,4-TRIMETHYLPENTANE 1.444457 1.523004 5.44 3.75 3.954 105 70 - 130
2-BUTANONE (MEK)0.149659 0.16550630 10.60 3.75 4.147 111 70 - 130
2-CHLOROTOLUENE 0.368387 0.41118690 11.60 3.75 4.186 112 70 - 130
2-PROPANOL 0.503072 0.54297590 7.93 3.75 4.047 108 70 - 130
4-ETHYLTOLUENE 0.499794 0.58389330 16.80 3.75 4.381 117 70 - 130
4-METHYL-2-PENTANONE (MIBK)0.238717 0.25993290 8.89 3.75 4.083 109 70 - 130
ACETONE 0.144952 0.16688790 15.10 3.75 4.318 115 70 - 130
ALLYL CHLORIDE 0.343121 0.38403230 11.90 3.75 4.197 112 70 - 130
BENZENE 0.228792 0.25595420 11.90 3.75 4.195 112 70 - 130
BENZYL CHLORIDE 0.269896 0.28989530 7.41 3.75 4.028 107 70 - 130
BROMODICHLOROMETHANE 0.143883 0.17967170 24.90 3.75 4.683 125 70 - 130
BROMOFORM 0.154423 0.19006160 23.10 3.75 4.615 123 70 - 130
BROMOMETHANE 0.252515 0.28467090 12.70 3.75 4.228 113 70 - 130
CARBON DISULFIDE 0.656881 0.78167920 19 7.50 8.925 119 70 - 130
CARBON TETRACHLORIDE 0.663959 0.797021 20 3.75 4.502 120 70 - 130
CHLOROBENZENE 0.229233 0.25611170 11.70 3.75 4.190 112 70 - 130
CHLORODIBROMOMETHANE 0.140622 0.17058370 21.30 3.75 4.549 121 70 - 130
CHLOROETHANE 0.149828 0.16631230 11 3.75 4.163 111 70 - 130
CHLOROFORM 0.619681 0.72275890 16.60 3.75 4.374 117 70 - 130
CHLOROMETHANE 0.214920 0.22698830 5.62 3.75 3.961 106 70 - 130
CIS-1,2-DICHLOROETHENE 0.390936 0.44211780 13.10 3.75 4.241 113 70 - 130
CIS-1,3-DICHLOROPROPENE 0.127951 0.14681160 14.70 3.75 4.303 115 70 - 130
CYCLOHEXANE 0.386461 0.41943620 8.53 3.75 4.070 109 70 - 130
DICHLORODIFLUOROMETHANE 0.750639 0.88400520 17.80 3.75 4.416 118 70 - 130
ETHANOL 0.106120 0.12008560 13.20 3.75 4.244 113 70 - 130
ETHYLBENZENE 0.407528 0.44334140 8.79 3.75 4.080 109 70 - 130
HEPTANE 0.120159 0.13020980 8.36 3.75 4.064 108 70 - 130
HEXACHLORO-1,3-BUTADIENE 0.297008 0.35490440 19.50 3.75 4.481 119 70 - 130
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 40 of 57
7A-OR GC/MS CONTINUING
CALIBRATION VERIFICATION
SDG:L1784259 Calibration (begin) date/time:09/27/24 17:25
Instrument ID:AIRMS17 Calibration (end) date/time:09/27/24 21:32
Lab File ID:1002_01 Analysis date/time:10/02/24 08:36
Analytical Method:TO-15 Sample ID:ICV
Analyte Avg. RRF RRF Min. RRF Diff.Max Diff.True Value Result Result Limits
%%ppbv ppbv % Rec.%
ISOPROPYLBENZENE 0.472383 0.53975610 14.30 3.75 4.285 114 70 - 130
M&P-XYLENE 0.331978 0.38180020 15 7.50 8.626 115 70 - 130
METHYL BUTYL KETONE 0.148072 0.15838990 6.97 3.75 4.011 107 70 - 130
METHYL METHACRYLATE 0.080036 0.09285568 16 3.75 4.351 116 70 - 130
METHYL TERT-BUTYL ETHER 0.857628 0.92948360 8.38 3.75 4.064 108 70 - 130
METHYLENE CHLORIDE 0.302533 0.32824950 8.50 3.75 4.069 109 70 - 130
N-HEXANE 0.431990 0.46738990 8.19 3.75 4.057 108 70 - 130
NAPHTHALENE 0.611294 0.70474540 15.30 3.75 4.323 115 70 - 130
O-XYLENE 0.328739 0.38033490 15.70 3.75 4.339 116 70 - 130
PROPENE 0.255611 0.26832180 4.97 3.75 3.936 105 70 - 130
STYRENE 0.249369 0.290286 16.40 7.50 8.731 116 70 - 130
TETRACHLOROETHENE 0.148092 0.16659060 12.50 3.75 4.218 112 70 - 130
TETRAHYDROFURAN 0.278950 0.300099 7.58 3.75 4.034 108 70 - 130
TOLUENE 0.281212 0.30379890 8.03 3.75 4.051 108 70 - 130
TPH (GC/MS) LOW FRACTION 3.982962 4.459149 12 176.25 197.3 112 70 - 130
TRANS-1,2-DICHLOROETHENE 0.371982 0.42824410 15.10 3.75 4.317 115 70 - 130
TRANS-1,3-DICHLOROPROPENE 0.098028 0.11502480 17.30 3.75 4.400 117 70 - 130
TRICHLOROETHENE 0.101684 0.11398010 12.10 3.75 4.203 112 70 - 130
TRICHLOROFLUOROMETHANE 0.802932 0.94859590 18.10 3.75 4.430 118 70 - 130
VINYL ACETATE 0.618707 0.682174 10.30 3.75 4.135 110 70 - 130
VINYL BROMIDE 0.257153 0.28916110 12.40 3.75 4.217 112 70 - 130
VINYL CHLORIDE 0.258782 0.28789470 11.20 3.75 4.172 111 70 - 130
1,4-BROMOFLUOROBENZENE 0.757842 0.78814660 4 4 4.160 104 60 - 140
D: Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 41 of 57
8B-OR ANALYTICAL SEQUENCE
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS14 Calibration Start Date:09/30/24 21:51
Calibration End Date:10/01/24 05:04
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE AIRMS14093024A0930A_01756826 0930A_01 09/30/24 20:20
CAL .19 0930A_03 09/30/24 21:51
CAL .31 0930A_04 09/30/24 22:35
CAL .63 0930A_05 09/30/24 23:19
CAL 1.25 0930A_06 10/01/24 00:05
CAL 2.5 0930A_07 10/01/24 00:52
CAL 3.75 0930A_08 10/01/24 01:41
CAL 10 0930A_09 10/01/24 02:26
CAL 25 0930A_10 10/01/24 03:14
CAL 50 0930A_11 10/01/24 04:05
CAL 100 0930A_12 10/01/24 05:04
SSCV AIRMS14093024A0930A_14756826 0930A_14 10/01/24 06:43
ICV AIRMS141006241006_01756826 1006_01 10/06/24 08:30
TUNE AIRMS141006241006_01T756826 1006_01T 10/06/24 08:30
LCS R4129260-1 1006_02 10/06/24 09:20 1 WG2376939
LCSD R4129260-2 1006_03 10/06/24 10:09 1 WG2376939
BLANK R4129260-3 1006_04 10/06/24 10:56 1 WG2376939
L1782196-04 L1782196-04 1006_05 10/06/24 12:49 500 WG2376939
L1784350-01 L1784350-01 1006_07 10/06/24 14:25 1 WG2376939
L1784715-02 L1784715-02 1006_08 10/06/24 15:12 1 WG2376939
L1784210-02 L1784210-02 1006_09 10/06/24 15:57 36.1 WG2376939
L1784350-02 L1784350-02 1006_10 10/06/24 16:42 10 WG2376939
L1784677-02 L1784677-02 1006_11 10/06/24 17:28 10 WG2376939
SV-1 L1784259-01 1006_13 10/06/24 19:57 20 WG2376939
SV-2 L1784259-02 1006_14 10/06/24 20:42 20 WG2376939
SV-20 L1784259-03 1006_15 10/06/24 21:27 20 WG2376939
L1784677-01 L1784677-01 1006_18 10/06/24 23:40 20 WG2376939
L1784715-01 L1784715-01 1006_19 10/07/24 00:25 20 WG2376939
L1784337-01 L1784337-01 1006_20 10/07/24 01:13 100 WG2376939
L1784337-02 L1784337-02 1006_21 10/07/24 01:57 500 WG2376939
L1784337-03 L1784337-03 1006_22 10/07/24 02:42 500 WG2376939
L1784347-01 L1784347-01 1006_23 10/07/24 03:26 500 WG2376939
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 42 of 57
8B-OR ANALYTICAL SEQUENCE
SDG:L1784259 Analytical Method:TO-15
Instrument ID:AIRMS17 Calibration Start Date:09/27/24 17:25
Calibration End Date:09/27/24 21:32
Client Sample ID Lab Sample ID File ID Analysis Date Time Dilution Batch
TUNE AIRMS17092724A0927A_01756221 0927A_01 09/27/24 16:33
CAL 0.19 0927A_03 09/27/24 17:25
CAL 0.31 0927A_04 09/27/24 17:50
CAL 0.63 0927A_05 09/27/24 18:15
CAL 1.25 0927A_06 09/27/24 18:40
CAL 2.5 0927A_07 09/27/24 19:06
CAL 3.75 0927A_08 09/27/24 19:34
CAL 10.0 0927A_09 09/27/24 19:59
CAL 25 0927A_10 09/27/24 20:25
CAL 50 0927A_11 09/27/24 20:55
CAL 100 0927A_12 09/27/24 21:32
SSCV AIRMS17092724A0927A_14756221 0927A_14 09/27/24 22:27
ICV AIRMS171002241002_01756221 1002_01 10/02/24 08:36
TUNE AIRMS171002241002_01T756221 1002_01T 10/02/24 08:36
LCS R4127354-1 1002_02 10/02/24 09:05 1 WG2374030
LCSD R4127354-2 1002_03 10/02/24 09:34 1 WG2374030
BLANK R4127354-3 1002_04 10/02/24 10:00 1 WG2374030
L1783907-01 L1783907-01 1002_05 10/02/24 10:58 1 WG2374030
L1783907-02 L1783907-02 1002_06 10/02/24 11:26 1 WG2374030
L1783907-03 L1783907-03 1002_07 10/02/24 11:54 1 WG2374030
L1783907-04 L1783907-04 1002_08 10/02/24 12:21 1 WG2374030
L1783907-05 L1783907-05 1002_09 10/02/24 12:49 1 WG2374030
L1783907-06 L1783907-06 1002_10 10/02/24 13:16 1 WG2374030
L1783907-07 L1783907-07 1002_11 10/02/24 13:43 1 WG2374030
L1783907-08 L1783907-08 1002_12 10/02/24 14:11 1 WG2374030
L1783907-11 L1783907-11 1002_13 10/02/24 18:26 1 WG2374030
L1783907-12 L1783907-12 1002_14 10/02/24 18:54 1 WG2374030
L1784069-01 L1784069-01 1002_16 10/02/24 20:27 1 WG2374030
L1784069-02 L1784069-02 1002_17 10/02/24 20:54 1 WG2374030
L1784069-03 L1784069-03 1002_18 10/02/24 21:22 1 WG2374030
SV-1 L1784259-01 1002_19 10/02/24 23:03 1 WG2374030
SV-2 L1784259-02 1002_20 10/02/24 23:32 1 WG2374030
SV-20 L1784259-03 1002_21 10/03/24 00:00 1 WG2374030
L1784294-01 L1784294-01 1002_22 10/03/24 00:28 1 WG2374030
L1781954-15 L1781954-15 1002_23 10/03/24 00:55 100 WG2374030
L1781954-22 L1781954-22 1002_24 10/03/24 01:20 20000 WG2374030
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 43 of 57
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784259-01,02,03 Analytical Method:TO-15
Matrix:Air Prep Method:TO-15
Analyte CAS MDL RDL
ppbv ppbv
Carbon tetrachloride 56-23-5 0.0732 0.20
Chlorobenzene 108-90-7 0.0832 0.20
Chloroethane 75-00-3 0.0996 0.20
Chloroform 67-66-3 0.0717 0.20
Chloromethane 74-87-3 0.1030 0.20
2-Chlorotoluene 95-49-8 0.0828 0.20
Cyclohexane 110-82-7 0.0753 0.20
Dibromochloromethane 124-48-1 0.0727 0.20
1,2-Dibromoethane 106-93-4 0.0721 0.20
1,2-Dichlorobenzene 95-50-1 0.1280 0.20
1,3-Dichlorobenzene 541-73-1 0.1820 0.20
Acetone 67-64-1 0.5840 1.25
1,4-Dichlorobenzene 106-46-7 0.0557 0.20
1,2-Dichloroethane 107-06-2 0.07 0.20
1,1-Dichloroethane 75-34-3 0.0723 0.20
1,1-Dichloroethene 75-35-4 0.0762 0.20
cis-1,2-Dichloroethene 156-59-2 0.0784 0.20
Allyl chloride 107-05-1 0.1140 0.20
trans-1,2-Dichloroethene 156-60-5 0.0673 0.20
1,2-Dichloropropane 78-87-5 0.0760 0.20
cis-1,3-Dichloropropene 10061-01-5 0.0689 0.20
trans-1,3-Dichloropropene 10061-02-6 0.0728 0.20
1,4-Dioxane 123-91-1 0.0833 0.63
Benzene 71-43-2 0.0715 0.20
Ethanol 64-17-5 0.2650 2.50
Ethylbenzene 100-41-4 0.0835 0.20
4-Ethyltoluene 622-96-8 0.0783 0.20
Trichlorofluoromethane 75-69-4 0.0819 0.20
Dichlorodifluoromethane 75-71-8 0.1370 0.20
1,1,2-Trichlorotrifluoroethane 76-13-1 0.0793 0.20
1,2-Dichlorotetrafluoroethane 76-14-2 0.0890 0.20
Heptane 142-82-5 0.1040 0.20
Hexachloro-1,3-butadiene 87-68-3 0.1050 0.63
n-Hexane 110-54-3 0.2060 0.63
Isopropylbenzene 98-82-8 0.0777 0.20
Benzyl Chloride 100-44-7 0.0598 0.20
Methylene Chloride 75-09-2 0.0979 0.20
Methyl Butyl Ketone 591-78-6 0.1330 1.25
2-Butanone (MEK)78-93-3 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 0.0765 1.25
Methyl methacrylate 80-62-6 0.0876 0.20
MTBE 1634-04-4 0.0647 0.20
Naphthalene 91-20-3 0.35 0.63
2-Propanol 67-63-0 0.2640 1.25
Propene 115-07-1 0.0932 1.25
Styrene 100-42-5 0.0788 0.40
1,1,2,2-Tetrachloroethane 79-34-5 0.0743 0.20
Bromodichloromethane 75-27-4 0.0702 0.20
Tetrachloroethylene 127-18-4 0.0814 0.20
Tetrahydrofuran 109-99-9 0.0734 0.20
Toluene 108-88-3 0.0870 0.50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 44 of 57
11-OR DETECTION LIMIT SUMMARY
Lab Sample IDs:L1784259-01,02,03 Analytical Method:TO-15
Matrix:Air Prep Method:TO-15
Analyte CAS MDL RDL
ppbv ppbv
1,2,4-Trichlorobenzene 120-82-1 0.1480 0.63
1,1,1-Trichloroethane 71-55-6 0.0736 0.20
1,1,2-Trichloroethane 79-00-5 0.0775 0.20
Trichloroethylene 79-01-6 0.0680 0.20
1,2,4-Trimethylbenzene 95-63-6 0.0764 0.20
1,3,5-Trimethylbenzene 108-67-8 0.0779 0.20
2,2,4-Trimethylpentane 540-84-1 0.1330 0.20
Vinyl chloride 75-01-4 0.0949 0.20
Vinyl Bromide 593-60-2 0.0852 0.20
Vinyl acetate 108-05-4 0.1160 0.63
Bromoform 75-25-2 0.0732 0.60
m&p-Xylene 179601-23-1 0.1350 0.40
o-Xylene 95-47-6 0.0828 0.20
TPH (GC/MS) Low Fraction 8006-61-9 39.70 200
Bromomethane 74-83-9 0.0982 0.20
1,3-Butadiene 106-99-0 0.1040 2
Carbon disulfide 75-15-0 0.1020 0.40
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 45 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4127354-3
Lab Sample ID:R4127354-3 SDG:L1784259
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1002_04 Received Date/Time:_______________
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 10:00
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 10:00
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Acetone 67-64-1 0 U 0.584 1.25
Allyl chloride 107-05-1 0 U 0.114 0.200
Benzene 71-43-2 0 U 0.0715 0.200
Benzyl Chloride 100-44-7 0 U 0.0598 0.200
Bromodichloromethane 75-27-4 0 U 0.0702 0.200
Bromoform 75-25-2 0 U 0.0732 0.600
Bromomethane 74-83-9 0 U 0.0982 0.200
1,3-Butadiene 106-99-0 0 U 0.104 2.00
Carbon disulfide 75-15-0 0 U 0.102 0.400
Carbon tetrachloride 56-23-5 0 U 0.0732 0.200
Chlorobenzene 108-90-7 0 U 0.0832 0.200
Chloroethane 75-00-3 0 U 0.0996 0.200
Chloroform 67-66-3 0 U 0.0717 0.200
Chloromethane 74-87-3 0 U 0.103 0.200
2-Chlorotoluene 95-49-8 0 U 0.0828 0.200
Cyclohexane 110-82-7 0 U 0.0753 0.200
Dibromochloromethane 124-48-1 0 U 0.0727 0.200
1,2-Dibromoethane 106-93-4 0 U 0.0721 0.200
1,2-Dichlorobenzene 95-50-1 0 U 0.128 0.200
1,3-Dichlorobenzene 541-73-1 0 U 0.182 0.200
1,4-Dichlorobenzene 106-46-7 0 U 0.0557 0.200
1,2-Dichloroethane 107-06-2 0 U 0.0700 0.200
1,1-Dichloroethene 75-35-4 0 U 0.0762 0.200
trans-1,2-Dichloroethene 156-60-5 0 U 0.0673 0.200
1,2-Dichloropropane 78-87-5 0 U 0.0760 0.200
cis-1,3-Dichloropropene 10061-01-5 0 U 0.0689 0.200
trans-1,3-Dichloropropene 10061-02-6 0 U 0.0728 0.200
1,4-Dioxane 123-91-1 0 U 0.0833 0.630
Ethanol 64-17-5 0 U 0.265 2.50
Ethylbenzene 100-41-4 0 U 0.0835 0.200
4-Ethyltoluene 622-96-8 0 U 0.0783 0.200
Trichlorofluoromethane 75-69-4 0 U 0.0819 0.200
Dichlorodifluoromethane 75-71-8 0 U 0.137 0.200
1,1,2-Trichlorotrifluoroethane 76-13-1 0 U 0.0793 0.200
1,2-Dichlorotetrafluoroethane 76-14-2 0 U 0.0890 0.200
Heptane 142-82-5 0 U 0.104 0.200
Hexachloro-1,3-butadiene 87-68-3 0 U 0.105 0.630
n-Hexane 110-54-3 0 U 0.206 0.630
Isopropylbenzene 98-82-8 0 U 0.0777 0.200
Methylene Chloride 75-09-2 0 U 0.0979 0.200
Methyl Butyl Ketone 591-78-6 0 U 0.133 1.25
2-Butanone (MEK)78-93-3 0 U 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 0 U 0.0765 1.25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 46 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4127354-3
Lab Sample ID:R4127354-3 SDG:L1784259
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1002_04 Received Date/Time:_______________
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 10:00
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 10:00
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Methyl methacrylate 80-62-6 0 U 0.0876 0.200
MTBE 1634-04-4 0 U 0.0647 0.200
Naphthalene 91-20-3 0 U 0.350 0.630
2-Propanol 67-63-0 0 U 0.264 1.25
Propene 115-07-1 1.65 0.110 J 0.0932 1.25
Styrene 100-42-5 0 U 0.0788 0.400
1,1,2,2-Tetrachloroethane 79-34-5 0 U 0.0743 0.200
Tetrahydrofuran 109-99-9 0 U 0.0734 0.200
Toluene 108-88-3 0 U 0.0870 0.500
1,2,4-Trichlorobenzene 120-82-1 0 U 0.148 0.630
1,1,1-Trichloroethane 71-55-6 0 U 0.0736 0.200
1,1,2-Trichloroethane 79-00-5 0 U 0.0775 0.200
1,2,4-Trimethylbenzene 95-63-6 0 U 0.0764 0.200
1,3,5-Trimethylbenzene 108-67-8 0 U 0.0779 0.200
2,2,4-Trimethylpentane 540-84-1 0 U 0.133 0.200
Vinyl chloride 75-01-4 0 U 0.0949 0.200
Vinyl Bromide 593-60-2 0 U 0.0852 0.200
Vinyl acetate 108-05-4 0 U 0.116 0.630
m&p-Xylene 179601-23-1 0 U 0.135 0.400
o-Xylene 95-47-6 0 U 0.0828 0.200
TPH (GC/MS) Low Fraction 8006-61-9 5.43 40.7 J 39.7 200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 47 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4129260-3
Lab Sample ID:R4129260-3 SDG:L1784259
Client Sample ID:BLANK Collected Date/Time:_______________
Lab File ID:1006_04 Received Date/Time:_______________
Instrument ID:AIRMS14 Preparation Date/Time:10/06/24 10:56
Analytical Batch:WG2376939 Analysis Date/Time:10/06/24 10:56
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:200 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
1,1-Dichloroethane 75-34-3 0 U 0.0723 0.200
cis-1,2-Dichloroethene 156-59-2 0 U 0.0784 0.200
trans-1,2-Dichloroethene 156-60-5 0 U 0.0673 0.200
Tetrachloroethylene 127-18-4 0 U 0.0814 0.200
Trichloroethylene 79-01-6 0 U 0.0680 0.200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 48 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4127354-1
Lab Sample ID:R4127354-1 SDG:L1784259
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1002_02 Received Date/Time:_______________
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 09:05
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 09:05
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:300 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Acetone 67-64-1 2.07 3.81 0.584 1.25
Allyl chloride 107-05-1 2.39 3.96 0.114 0.200
Benzene 71-43-2 3.91 4.02 0.0715 0.200
Benzyl Chloride 100-44-7 7.87 3.67 0.0598 0.200
Bromodichloromethane 75-27-4 4.44 4.35 0.0702 0.200
Bromoform 75-25-2 6.67 4.16 0.0732 0.600
Bromomethane 74-83-9 1.87 3.92 0.0982 0.200
1,3-Butadiene 106-99-0 1.80 3.80 0.104 2.00
Carbon disulfide 75-15-0 2.44 8.13 0.102 0.400
Carbon tetrachloride 56-23-5 3.99 4.22 0.0732 0.200
Chlorobenzene 108-90-7 6.37 4.05 0.0832 0.200
Chloroethane 75-00-3 1.91 3.80 0.0996 0.200
Chloroform 67-66-3 3.22 4.09 0.0717 0.200
Chloromethane 74-87-3 1.71 3.73 0.103 0.200
2-Chlorotoluene 95-49-8 7.44 4.01 0.0828 0.200
Cyclohexane 110-82-7 4.05 3.72 0.0753 0.200
Dibromochloromethane 124-48-1 5.64 4.34 0.0727 0.200
1,2-Dibromoethane 106-93-4 5.76 4.16 0.0721 0.200
1,2-Dichlorobenzene 95-50-1 8.10 4.10 0.128 0.200
1,3-Dichlorobenzene 541-73-1 7.88 4.09 0.182 0.200
1,4-Dichlorobenzene 106-46-7 7.92 4.09 0.0557 0.200
1,2-Dichloroethane 107-06-2 3.56 4.23 0.0700 0.200
1,1-Dichloroethene 75-35-4 2.32 3.96 0.0762 0.200
trans-1,2-Dichloroethene 156-60-5 2.66 4.21 0.0673 0.200
1,2-Dichloropropane 78-87-5 4.33 3.87 0.0760 0.200
cis-1,3-Dichloropropene 10061-01-5 4.93 4.02 0.0689 0.200
trans-1,3-Dichloropropene 10061-02-6 5.22 3.91 0.0728 0.200
1,4-Dioxane 123-91-1 4.47 3.94 0.0833 0.630
Ethanol 64-17-5 1.94 3.56 0.265 2.50
Ethylbenzene 100-41-4 6.58 3.93 0.0835 0.200
4-Ethyltoluene 622-96-8 7.56 4.19 0.0783 0.200
Trichlorofluoromethane 75-69-4 2.13 4.18 0.0819 0.200
Dichlorodifluoromethane 75-71-8 1.67 4.12 0.137 0.200
1,1,2-Trichlorotrifluoroethane 76-13-1 2.44 4.02 0.0793 0.200
1,2-Dichlorotetrafluoroethane 76-14-2 1.74 3.94 0.0891 0.200
Heptane 142-82-5 4.67 3.88 0.104 0.200
Hexachloro-1,3-butadiene 87-68-3 9.39 4.24 0.105 0.630
n-Hexane 110-54-3 3.20 3.80 0.206 0.630
Isopropylbenzene 98-82-8 7.21 4.06 0.0777 0.200
Methylene Chloride 75-09-2 2.35 3.73 0.0979 0.200
Methyl Butyl Ketone 591-78-6 5.62 3.81 0.133 1.25
2-Butanone (MEK)78-93-3 2.90 3.85 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 4.97 4.14 0.0765 1.25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 49 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4127354-1
Lab Sample ID:R4127354-1 SDG:L1784259
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1002_02 Received Date/Time:_______________
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 09:05
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 09:05
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:300 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Methyl methacrylate 80-62-6 4.61 3.96 0.0876 0.200
MTBE 1634-04-4 2.77 3.82 0.0647 0.200
Naphthalene 91-20-3 9.16 4.09 0.350 0.630
2-Propanol 67-63-0 2.14 3.60 0.264 1.25
Propene 115-07-1 1.65 3.52 0.0932 1.25
Styrene 100-42-5 6.85 8.43 0.0788 0.400
1,1,2,2-Tetrachloroethane 79-34-5 6.89 3.97 0.0743 0.200
Tetrahydrofuran 109-99-9 3.40 3.84 0.0734 0.200
Toluene 108-88-3 5.44 3.91 0.0870 0.500
1,2,4-Trichlorobenzene 120-82-1 9.11 4.02 0.148 0.630
1,1,1-Trichloroethane 71-55-6 3.69 4.30 0.0736 0.200
1,1,2-Trichloroethane 79-00-5 5.29 3.99 0.0775 0.200
1,2,4-Trimethylbenzene 95-63-6 7.82 4.21 0.0764 0.200
1,3,5-Trimethylbenzene 108-67-8 7.61 4.18 0.0779 0.200
2,2,4-Trimethylpentane 540-84-1 4.51 3.79 0.133 0.200
Vinyl chloride 75-01-4 1.77 3.88 0.0949 0.200
Vinyl Bromide 593-60-2 2.01 4.06 0.0852 0.200
Vinyl acetate 108-05-4 2.80 3.53 0.116 0.630
m&p-Xylene 179601-23-1 6.67 8.05 0.135 0.400
o-Xylene 95-47-6 6.90 4.15 0.0828 0.200
TPH (GC/MS) Low Fraction 8006-61-9 5.43 189 39.7 200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 50 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4129260-1
Lab Sample ID:R4129260-1 SDG:L1784259
Client Sample ID:LCS Collected Date/Time:_______________
Lab File ID:1006_02 Received Date/Time:_______________
Instrument ID:AIRMS14 Preparation Date/Time:10/06/24 09:20
Analytical Batch:WG2376939 Analysis Date/Time:10/06/24 09:20
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:300 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
1,1-Dichloroethane 75-34-3 7.03 4.12 0.0723 0.200
cis-1,2-Dichloroethene 156-59-2 7.54 3.95 0.0784 0.200
trans-1,2-Dichloroethene 156-60-5 6.61 4.01 0.0673 0.200
Tetrachloroethylene 127-18-4 10.74 4.15 0.0814 0.200
Trichloroethylene 79-01-6 8.89 4.30 0.0680 0.200
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geosyntec Consultants - UT SLC1091 L1784259 10/31/24 16:28 51 of 57
1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4127354-2
Lab Sample ID:R4127354-2 SDG:L1784259
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1002_03 Received Date/Time:_______________
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 09:34
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 09:34
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:300 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Acetone 67-64-1 2.07 3.74 0.584 1.25
Allyl chloride 107-05-1 2.39 3.88 0.114 0.200
Benzene 71-43-2 3.91 3.96 0.0715 0.200
Benzyl Chloride 100-44-7 7.87 3.58 0.0598 0.200
Bromodichloromethane 75-27-4 4.44 4.33 0.0702 0.200
Bromoform 75-25-2 6.66 4.20 0.0732 0.600
Bromomethane 74-83-9 1.86 3.89 0.0982 0.200
1,3-Butadiene 106-99-0 1.80 3.78 0.104 2.00
Carbon disulfide 75-15-0 2.44 8.25 0.102 0.400
Carbon tetrachloride 56-23-5 3.99 4.30 0.0732 0.200
Chlorobenzene 108-90-7 6.37 3.98 0.0832 0.200
Chloroethane 75-00-3 1.91 3.76 0.0996 0.200
Chloroform 67-66-3 3.22 4.11 0.0717 0.200
Chloromethane 74-87-3 1.70 3.86 0.103 0.200
2-Chlorotoluene 95-49-8 7.44 4.01 0.0828 0.200
Cyclohexane 110-82-7 4.05 3.85 0.0753 0.200
Dibromochloromethane 124-48-1 5.64 4.25 0.0727 0.200
1,2-Dibromoethane 106-93-4 5.76 4.05 0.0721 0.200
1,2-Dichlorobenzene 95-50-1 8.10 4.19 0.128 0.200
1,3-Dichlorobenzene 541-73-1 7.88 4.28 0.182 0.200
1,4-Dichlorobenzene 106-46-7 7.92 4.26 0.0557 0.200
1,2-Dichloroethane 107-06-2 3.56 4.28 0.0700 0.200
1,1-Dichloroethene 75-35-4 2.32 3.99 0.0762 0.200
trans-1,2-Dichloroethene 156-60-5 2.66 3.95 0.0673 0.200
1,2-Dichloropropane 78-87-5 4.33 3.89 0.0760 0.200
cis-1,3-Dichloropropene 10061-01-5 4.93 4.04 0.0689 0.200
trans-1,3-Dichloropropene 10061-02-6 5.22 4.08 0.0728 0.200
1,4-Dioxane 123-91-1 4.47 4.06 0.0833 0.630
Ethanol 64-17-5 1.94 3.80 0.265 2.50
Ethylbenzene 100-41-4 6.58 3.94 0.0835 0.200
4-Ethyltoluene 622-96-8 7.56 4.26 0.0783 0.200
Trichlorofluoromethane 75-69-4 2.12 4.18 0.0819 0.200
Dichlorodifluoromethane 75-71-8 1.66 4.19 0.137 0.200
1,1,2-Trichlorotrifluoroethane 76-13-1 2.44 4.12 0.0793 0.200
1,2-Dichlorotetrafluoroethane 76-14-2 1.73 4.05 0.0891 0.200
Heptane 142-82-5 4.67 3.96 0.104 0.200
Hexachloro-1,3-butadiene 87-68-3 9.39 4.27 0.105 0.630
n-Hexane 110-54-3 3.20 3.82 0.206 0.630
Isopropylbenzene 98-82-8 7.21 4.12 0.0777 0.200
Methylene Chloride 75-09-2 2.35 3.83 0.0979 0.200
Methyl Butyl Ketone 591-78-6 5.62 3.88 0.133 1.25
2-Butanone (MEK)78-93-3 2.89 3.66 0.0814 1.25
4-Methyl-2-pentanone (MIBK)108-10-1 4.97 3.97 0.0765 1.25
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4127354-2
Lab Sample ID:R4127354-2 SDG:L1784259
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1002_03 Received Date/Time:_______________
Instrument ID:AIRMS17 Preparation Date/Time:10/02/24 09:34
Analytical Batch:WG2374030 Analysis Date/Time:10/02/24 09:34
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:300 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
Methyl methacrylate 80-62-6 4.61 4.08 0.0876 0.200
MTBE 1634-04-4 2.77 3.92 0.0647 0.200
Naphthalene 91-20-3 9.16 4.22 0.350 0.630
2-Propanol 67-63-0 2.14 3.71 0.264 1.25
Propene 115-07-1 1.65 3.43 0.0932 1.25
Styrene 100-42-5 6.85 8.78 0.0788 0.400
1,1,2,2-Tetrachloroethane 79-34-5 6.89 4.15 0.0743 0.200
Tetrahydrofuran 109-99-9 3.40 3.87 0.0734 0.200
Toluene 108-88-3 5.44 3.98 0.0870 0.500
1,2,4-Trichlorobenzene 120-82-1 9.11 4.17 0.148 0.630
1,1,1-Trichloroethane 71-55-6 3.69 4.21 0.0736 0.200
1,1,2-Trichloroethane 79-00-5 5.29 4.09 0.0775 0.200
1,2,4-Trimethylbenzene 95-63-6 7.82 4.32 0.0764 0.200
1,3,5-Trimethylbenzene 108-67-8 7.61 4.30 0.0779 0.200
2,2,4-Trimethylpentane 540-84-1 4.51 3.86 0.133 0.200
Vinyl chloride 75-01-4 1.76 4.15 0.0949 0.200
Vinyl Bromide 593-60-2 2 4.08 0.0852 0.200
Vinyl acetate 108-05-4 2.80 3.62 0.116 0.630
m&p-Xylene 179601-23-1 6.67 8.26 0.135 0.400
o-Xylene 95-47-6 6.90 4.32 0.0828 0.200
TPH (GC/MS) Low Fraction 8006-61-9 5.43 190 39.7 200
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1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:
ORGANIC ANALYSIS DATA SHEET R4129260-2
Lab Sample ID:R4129260-2 SDG:L1784259
Client Sample ID:LCSD Collected Date/Time:_______________
Lab File ID:1006_03 Received Date/Time:_______________
Instrument ID:AIRMS14 Preparation Date/Time:10/06/24 10:09
Analytical Batch:WG2376939 Analysis Date/Time:10/06/24 10:09
Dilution Factor:1 Prep Method:TO-15
Analytical Method:TO-15 Sample Vol Used:300 mL
Matrix:Air Initial Wt/Vol:_______________
Total Solids (%):_______________Final Wt/Vol:_______________
Analyte CAS RT Result Qualifier MDL RDL
ppbv ppbv ppbv
1,1-Dichloroethane 75-34-3 7.03 4.10 0.0723 0.200
cis-1,2-Dichloroethene 156-59-2 7.54 4.02 0.0784 0.200
trans-1,2-Dichloroethene 156-60-5 6.61 3.93 0.0673 0.200
Tetrachloroethylene 127-18-4 10.75 4.15 0.0814 0.200
Trichloroethylene 79-01-6 8.89 4.28 0.0680 0.200
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
COD Coefficient of Determination.
Mass Mass of parameter.
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
RRF Relative Response Factor.
RT Retention Time.
SDG Sample Delivery Group.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Su
6 Gl
7 Al
8 Sc
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Paxton SCR

APPENDIX D
Data Validation Reports
180A Market Place Boulevard
Knoxville, TN 37922
PH 865.330.0037
www.geosyntec.com

DVR L1757957, L1784578, L1791693 R1.docx Final Review: K Henderson 11/25/2024
Memorandum
Date: 26 November 2024
To: Brian Smith
From: Chase Harris
CC: Kristoffer Henderson
Subject: Stage 2A Data Validation - Level II Data Deliverable – Pace
Analytical National Job IDs L1757957, L1784578, L1791693
SITE: Paxton
INTRODUCTION
This report summarizes the findings of the Stage 2A data validation of twenty-nine soil samples,
two trip blanks and three field duplicates, collected on 16 July 2024 and 27-30 September 2024 as
part of the Paxton Voluntary Cleanup Program (VCP), site characterization activities (VCP Site
#C-129).
Pace Analytical National Mount Juliet, Tennessee analyzed the samples for the following
analytical tests:
• Total Solids by Standard Method (SM) 2540 G-2011
• Oil and Grease by United States (US) Environmental Protection Agency (EPA) methods
9071B and 1664A and 1664B
• Mercury by US EPA methods 7471A/7471B
• Metals by US EPA method 6010B
• Total Petroleum Hydrocarbons (TPH) Low Fraction by US EPA methods 8015D/GRO
• Volatile Organic Compounds (VOCs) by US EPA Method 8260B
• Total Petroleum Hydrocarbons (TPH) High Fraction by US EPA Method 8015
EXECUTIVE SUMMARY
Overall, based on this Stage 2A data validation covering the quality control (QC) parameters listed
below and based on the information provided, the data as qualified are usable for supporting project
objectives. The qualified data should be used within the limitations of the qualifications. If there
are results with two or more different qualifications due to multiple QC failures, the final
qualification is reconciled in the electronic data deliverable (EDD) with qualifications.
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The data were reviewed based on professional and technical judgment and the following
documents:
• Quality Assurance Project Plan, Paxton Development, 203 to 225 West Paxton Avenue,
Salt Lake City, Utah, Voluntary Cleanup Site #C-129, June 19, 2024 (herein referred to as
the QAPP);
• US EPA Contract Laboratory Program National Functional Guidelines for Organic
Superfund Methods Data Review, November 2020 (EPA 540-R-20-005);
• US EPA Contract Laboratory Program National Functional Guidelines for Superfund
Inorganic Superfund Data Review, November 2020 (EPA 540-R-20-006); and,
• The pertinent methods referenced by the data package.
The following samples were analyzed in the data set:

Laboratory ID Client ID
L1757957-01 S-3 (0-6)
L1757957-02 S-3 (6-12)
L1757957-03 S-30 (6-12)
L1757957-04 S-9 (0-6)
L1757957-05 S-8 (0-6)
L1757957-06 S-7 (0-6)
L1757957-07 S-7 (6-12)
L1757957-08 S-6 (0-6)
L1757957-09 S-5 (0-6)
L1757957-10 S-4 (0-6)
L1757957-11 S-31 (0-6)
L1757957-12 S-2 (0-6)
L1757957-13 S-1 (0-6)
L1757957-14 S-1 (6-12)
L1757957-15 SS-1 (6-12)
L1757957-16 EB-1-071624
L1757957-17 TRIP BLANK
L1784578-01 S-13 (0-6)
Laboratory ID Client ID
L1784578-02 S-15 (0-6)
L1784578-03 S-32 (0-6)
L1784578-04 S-12 (6-12)
L1784578-05 S-12 (0-6)
L1784578-06 S-10 (0-6)
L1784578-07 S-4 (12-18)
L1784578-08 S-6 (12-18)
L1784578-09 S-1 (12-18)
L1784578-10 S-7 (12-18)
L1784578-11 S-10 (6-12)
L1784578-12 S-14 (0-6)
L1784578-13 S-11 (0-6)
L1784578-14 SS-1 (12-18)
L1784578-15 S-14 (6-12)
L1784578-16 S-3 (12-18)
L1784578-17 EB-93024
L1784578-18 TRIP BLANK
L1791693-01 S-6 (12-18)
The solids data, used to report the samples on a dry weight basis, were not validated.
The QAPP requires the samples to be cooled to 4 (±2) degrees Celsius (°C). Since the samples
were received within 0-6°C, the sample receipt temperature was considered acceptable. No
preservation issues were noted by the laboratory.
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The laboratory reported results for the analytical method(s) requested for each sample on the chain
of custody (COC).
Incorrect error corrections were observed on the COC, instead of the proper procedure of a single
strike through, correction, and initials and date of person making the corrections.
Laboratory report L1757957 was revised on November 22, 2024, to correct a sample ID. The
revised report was identified as L1757957 Revised Report.
The data validation report was revised on November 26, 2024, to make edits.
1.0 Oil and Grease
The samples were analyzed for oil and grease by US EPA methods 9071B, 1664A and 1664B.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
⊗ Overall Assessment
 Holding Times
 Method Blank
⊗ Matrix Spike/Matrix Spike Duplicate
⊗ Laboratory Duplicate
 Laboratory Control Sample
 Equipment Blank
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review
1.1 Overall Assessment
The oil and grease data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
1.2 Holding Time
The QAPP specified holding times for the oil and grease analysis of soil and water samples are 28
days from sample collection to analysis. The holding times were met for the sample analyses.
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1.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Five method blanks were reported for oil and grease
(batches WG2330367, WG2330146, WG2380187, WG2378003, and WG2378468). Oil and
grease were not detected in the method blanks at or above the MDLs.
1.4 Matrix Spike (MS)/Matrix Spike Duplicate (MSD)
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). Three sample specific MS/MSD pairs and sample specific MS were
reported using samples S-3 (0-6), S-32 (0-6) and S-10 (0-6) and on MS was reported using sample
EB-1-071624. The recovery and RPD results were within the laboratory specified acceptance
criteria, with the following exceptions.
L1757957: The recovery of oil and grease in the MSD of sample S-3 (0-6) was low and outside of
the laboratory specified acceptance criteria. The RPD of oil and grease between the MS and MSD
of sample S-3 (0-6) was high and outside of the laboratory specified acceptance criteria. Therefore,
the oil and grease data of sample S-3 (0-6) was J qualified as estimated.
L1784578: The recoveries of oil and grease in the MS/MSD of sample S-32 (0-6) were low and
outside of the laboratory specified acceptance criteria. Therefore, the oil and grease data of sample
S-32 (0-6) was J- qualified as estimated with low bias.
A batch MS was analyzed with batch WG2380187. Since this was batch QC, the results were not
qualified.
Sample
ID
Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier*
Reason
Code**
S-3 (0-6) Oil & Grease 251 J3 J6 P1 251 J 4
S-32 (0-6) Oil & Grease 120 J J6 P1 120 J- 4
mg/Kg-milligram per kilogram
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the reporting
detection limit (RDL)
J3-Laboratory flag denoting the associated batch QC was outside of the quality control range for precision
J6-Laboratory flag denoting matrix spike interference with low spike recovery
P1-Laboratory flag denoting the RPD value is not applicable for sample concentrations less than 5 times the RDL
* Validation qualifiers are defined in Attachment 1 at the end of this report
** Reason codes are defined in Attachment 2 at the end of the report
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1.5 Laboratory Duplicate
Three sample specific laboratory duplicates were reported using samples S-3 (0-6), S-32 (0-6) and
S-10 (0-6). The RPD results were within the laboratory specified acceptance criteria, with the
following exceptions.
L1757957: The RPD of oil and grease in the laboratory duplicate pair of sample S-3 (0-6) was
outside of the laboratory specified acceptance criteria. Since the oil and grease concentration for
sample S-3 (0-6) was less than five times the RDL and the difference between the laboratory
duplicate and original sample results was less than the RL, no qualifications were applied to the
data.
L1784578: The RPD of oil and grease in the laboratory duplicate pair of sample S-32 (0-6) was
outside of the laboratory specified acceptance criteria. Since the oil and grease concentration for
sample S-32 (0-6) was less than five times the RDL and the difference between the laboratory
duplicate and original sample results was less than the RDL, no qualifications were applied to the
data.
L1784578: The RPD of oil and grease in the laboratory duplicate pair of sample S-10 (0-6) was
outside of the laboratory specified acceptance criteria. Therefore, the oil and grease data of sample
S-10 (0-6) was J qualified as estimated.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier*
Reason
Code**
S-10 (0-6) Oil & Grease 785 J3 785 J 12
mg/Kg-milligram per kilogram
J3-Laboratory flag denoting the associated batch QC was outside of the quality control range for precision
* Validation qualifiers are defined in Attachment 1 at the end of this report
** Reason codes are defined in Attachment 2 at the end of the report
1.6 Laboratory Control Sample (LCS)
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). LCS/LCS duplicate (LCSD) pairs were reported. The recovery and RPD
results were within the laboratory specified acceptance criteria.
1.7 Equipment Blank
Two equipment blanks were collected with the sample set: EB-1-071624 and EB-93024. Oil and
grease were not detected in the equipment blanks at or above the MDLs.
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1.8 Field Duplicate
Three field duplicates were collected with the sample set: S-30 (6-12), S-31 (0-6), and S-32 (0-6).
Acceptable precision (RPD<30%) were demonstrated between the field duplicates and the original
samples S-3 (6-12), S-4 (0-6), and S-13 (0-6) respectively, with the following exceptions.
L1757957: The RPD of oil and grease between the field duplicate S-31 (0-6) and original sample
S-4 (0-6) was high and outside of the laboratory specified acceptance criteria. Therefore, based on
technical and professional judgement, the oil and grease data were J qualified as estimated.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-4 (0-6) Oil & Grease 8270 NA 33 8270 J 7
S-31 (0-6) Oil & Grease 11500 NA 11500 J 7
mg/Kg-milligram per kilogram
NA-not applicable
1.9 Sensitivity
The samples were reported to the MDLs. Elevated non-detect results were not reported.
1.10 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD.
2.0 Mercury
The samples were analyzed for mercury by US EPA methods 7471A and 7471B.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Equipment Blank
⊗ Field Duplicate
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 Sensitivity
 Electronic Data Deliverable Review
2.1 Overall Assessment
The mercury data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
2.2 Holding Time
The holding times for the mercury analysis of water and soil samples are 28 days from sample
collection to analysis. The holding times were met for the sample analyses.
2.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Five method blanks were reported for mercury (batches
WG2325902, WG2326412, WG2326415, WG2375204, and WG2376309). Mercury was not
detected in the method blanks at or above the MDLs.
2.4 Matrix Spike (MS)/Matrix Spike Duplicate (MSD)
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). Two sample specific MS/MSD pairs were reported using samples
S-3 (0-6) and S-10 (0-6). The recovery and RPD results were within the laboratory specified
acceptance criteria. Batch MS/MSDs were analyzed with batches WG2375204, WG2325902, and
WG2326415. Since these were batch QC, the results were not qualified.
2.5 Laboratory Control Sample (LCS)
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). LCS/LCSD pairs and LCSs were reported. The recovery and RPD results
were within the laboratory specified acceptance criteria.
2.6 Equipment Blank
Two equipment blanks were collected with the sample set: EB-1-071624 and EB-93024. Mercury
was not detected in the equipment blanks at or above the MDLs.
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2.7 Field Duplicate
Three field duplicates were collected with the sample set: S-30 (6-12), S-31 (0-6), and S-32 (0-6).
Acceptable precision (RPD<30%) were demonstrated between the field duplicates and the original
samples S-3 (6-12), S-4 (0-6), and S-13 (0-6) respectively, with the following exception.
The RPD of mercury between the field duplicate S-32 (0-6) and original sample S-13 (0-6) was
high and outside of the laboratory specified acceptance criteria. Therefore, the mercury
concentrations in the field duplicate pair were J qualified as estimated.
Sample
ID
Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-32 (0-6) Mercury 0.487 NA 73 0.487 J 7
S-13 (0-6) Mercury 0.226 NA 0.226 J 7
mg/Kg-milligram per kilogram
NA-not applicable
2.8 Sensitivity
The samples were reported to the MDLs. Elevated non-detect results were not reported.
2.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD.
3.0 Metals
The samples were analyzed for metals by US EPA method 6010B.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
 Overall Assessment
 Holding Times
⊗ Method Blank
⊗ Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
⊗ Equipment Blank
⊗ Field Duplicate
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 Sensitivity
 Electronic Data Deliverable Review

3.1 Overall Assessment
The metals data reported in this sample set are considered usable for supporting project objectives.
The results are considered valid; the analytical completeness defined as the ratio of the number of
valid analytical results (valid analytical results include values qualified as estimated) to the total
number of analytical results requested on samples submitted for analysis, for the sample set is
100%.
3.2 Holding Times
The holding times for the metals analysis of water and soil samples are 180 days from sample
collection to analysis. The holding times were met for the sample analyses.
3.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Seven method blanks were reported (batches WG2326410,
WG2326543, WG2327640, WG2376546, WG2376598, WG2378117 and WG2393511). Metals
were not detected in the method blanks at or above the MDLs, with the following exceptions.
L1757957: Silver (0.766 mg/kg) was detected at an estimated concentration greater than or equal
to the MDL and less than the RDL in the method blank of batch WG2326410. Therefore, the
estimated silver data in the associated samples were qualified U as non-detect and reported at the
RDL.
L1784578: Silver (0.184 mg/kg) was detected at an estimated concentration greater than or equal
to the MDL and less than the RDL in the method blank of batch WG2376598. Therefore, the
estimated silver data were qualified U as non-detect and reported at the RDL.
L1757957: Chromium (0.00143 mg/L) was detected at an estimated concentration greater than or
equal to the MDL and less than the RDL in the method blank of batch WG2327640. Therefore,
the estimated chromium data of the associated sample was U qualified as non-detect and reported
at the RDL.
L1784578: Arsenic (0.761 mg/kg) was detected at an estimated concentration greater than or equal
to the MDL and less than the RDL in the method blank of batch WG2376546. Since arsenic was
detected at a concentration greater than ten times the method blank concentration in the associated
sample, no qualifications were applied to the arsenic data.
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Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-13 (0-6) Silver 0.402 BJ 1.19 U 3
S-15 (0-6) Silver 1.05 BJ 1.15 U 3
S-32 (0-6) Silver 0.373 BJ 1.21 U 3
S-12 (6-12) Silver 0.749 BJ 1.17 U 3
S-12 (0-6) Silver 0.669 BJ 1.11 U 3
S-10 (0-6) Silver 0.689 BJO1 1.07 U 3
S-10 (6-12) Silver 0.358 BJ 1.04 U 3
S-14 (0-6) Silver 0.977 BJ 1.18 U 3
S-11 (0-6) Silver 0.35 BJ 1.03 U 3
S-14 (6-12) Silver 0.265 BJ 1.16 U 3
S-7 (0-6) Silver 0.242 BJ 1.06 U 3
S-7 (6-12) Silver 0.229 BJ 1.07 U 3
mg/Kg-milligram per kilogram
B-Laboratory flag denoting that the analyte was detected at or above the MDL in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
O1-Laboratory flag denoting the analyte failed the method required serial dilution test and/or subsequent post spike
criteria indicating matrix interference
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
EB-1-071624 Chromium 0.00159 BJ 0.0100 U 3
mg/Kg-milligram per kilogram
B-Laboratory flag denoting that the analyte was detected at or above the MDL in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
O1-Laboratory flag denoting the analyte failed the method required serial dilution test and/or subsequent post spike
criteria indicating matrix interference
3.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). Three sample specific MS/MSD pairs were reported using samples
S-3 (0-6), S-10 (0-6), and S-6 (12-18). The recovery and RPD results were within the laboratory
specified acceptance criteria, with the following exceptions.
Batch MS/MSD pairs were reported for batches WG2326410, WG2327640, WG2376546, and
WG2378117. Since these were batch QC the results were not qualified.
The recovery of lead in the MS/MSD of sample S-6 (12-18) was flagged ‘V’ indicating the sample
concentration of lead was greater than five times the spike concentration. Therefore, based on
technical and professional judgement, no qualifications were applied to the lead data of sample S-
6 (12-18).
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L1784578: The recovery of barium in the MSD of sample S-10 (0-6) was high and outside of the
laboratory specified acceptance criteria. The RPD of barium between the MS and MSD of sample
S-10 (0-6) was high and outside of the laboratory specified acceptance criteria. Therefore, based
on technical and professional judgement, the barium data of sample S-10 (0-6) was J qualified as
estimated.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-10 (0-6) Barium 170 J3 J5 170 J 4
mg/Kg-milligram per kilogram
J3-Laboratory flag denoting the associated batch QC was outside of the established quality control range for precision
J5-Laboratorty flag denoting matrix interference with high spike recoveries
3.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). LCSs were reported. The recovery results were within the laboratory
specified acceptance criteria.
3.6 Equipment Blank
Two equipment blanks, EB-1-071624 and EB-93024, were collected with the sample set. Metals
were not detected in the equipment blanks at or above the MDLs, with the following exceptions.
L1757957: Cadmium (soil equivalent concentration 0.106 mg/kg) and chromium (soil equivalent
concentration 0.159 mg/kg) were detected in the equipment blank EB-1-071624 at estimated
concentrations greater than or equal to the MDL and less than the RDL. Since the chromium
concentration in EB-1-071624 was U qualified due to method blank contamination, no
qualifications were applied to the chromium data. However, the cadmium concentrations in the
associated samples greater than the RDL and less than ten times the soil equivalent equipment
blank concentration were J+ qualified as estimated with high bias.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-8 (0-6) Cadmium 0.909 NA 0.909 J+ 3
S-6 (0-6) Cadmium 0.681 NA 0.681 J+ 3
S-5 (0-6) Cadmium 0.609 NA 0.609 J+ 3
S-2 (0-6) Cadmium 0.891 NA 0.891 J+ 3
mg/Kg-milligram per kilogram
NA-not applicable
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3.7 Field Duplicate
Three field duplicates were collected with the sample set: S-30 (6-12), S-31 (0-6), and S-32 (0-6).
Acceptable precision (RPD<50%) were demonstrated between the field duplicates and the original
samples S-3 (6-12), S-4 (0-6), and S-13 (0-6) respectively, with the following exceptions.
The RPDs of arsenic, barium, cadmium and lead between the field duplicate S-30 (6-12) and
original sample S-3 (6-12) were high and outside of the laboratory specified acceptance criteria.
Therefore, the arsenic, barium, cadmium and lead data were J qualified as estimated.
The RPD of selenium between the field duplicate sample S-31 (0-6) and original sample S-4 (0-6)
was high and outside of the laboratory specified acceptance criteria. Therefore, the selenium data
were J qualified as estimated.
Sample ID Compound Laborator
y Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-3 (6-12) Arsenic 10.7 NA 83 10.7 J 7
S-30 (6-12) Arsenic 25.9 NA 25.9 J 7
S-3 (6-12) Barium 118 NA 57 118 J 7
S-30 (6-12) Barium 213 NA 213 J 7
S-3 (6-12) Cadmium 1.28 NA 60 1.28 J 7
S-30 (6-12) Cadmium 2.37 NA 2.37 J 7
S-3 (6-12) Lead 125 NA 87 125 J 7
S-30 (6-12) Lead 316 NA 316 J 7
S-4 (0-6) Selenium 6.34 NA 70 6.34 J 7
S-31 (0-6) Selenium 13.2 NA 13.2 J 7
mg/Kg-milligram per kilogram
NA-Not applicable
3.8 Sensitivity
The samples were reported to the MDL. Elevated non-detect results were not reported.
3.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD
4.0 Total Petroleum Hydrocarbons
The samples were analyzed for TPH low fraction by US EPA methods 8015D/GRO. The areas of
data review are listed below. A leading check mark () indicates an area of review in which the
data were acceptable. A preceding crossed circle (⊗) signifies areas where issues were raised
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during the course of the validation review and should be considered to determine any impact on
data quality and usability.
 Overall Assessment
 Holding Times
⊗ Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Equipment Blank
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

4.1 Overall Assessment
The TPH low fraction data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
4.2 Holding Times
The holding times for the TPH low fraction analysis of water and soil samples are 14 days from
collection to analysis. The holding times were met for the sample analyses.
4.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Eleven method blanks were reported (batches
WG2327971, WG2328825, WG2329459, WG2329829, WG2329941, WG2330767,
WG2330774, WG2377829, WG2377924, WG2378256, and WG2378697). TPH low fraction was
not detected in the method blanks at or above the MDLs, with the following exceptions.
L1757957, l1791693 and L1784578: TPH low fraction was detected at estimated concentrations
greater than or equal to the MDLs and less than the RDLs in the method blanks of batches:
WG2328825 (0.657 mg/kg), WG2329459 (1.06 mg/kg), WG2329829 (0.738 mg/kg),
WG2330767 (2.01 mg/kg), WG2330774 (2.01 mg/kg), WG2377829 (0.675 mg/kg), WG2377924
(0.846 mg/kg), and WG2378256 (0.800 mg/kg). Therefore, based on technical and professional
judgement, the TPH low fraction data of the associated samples with estimated concentrations
greater than or equal to the MDL and less than the RDL were U qualified as non-detect and
reported at the RDL. The TPH low fraction data in the associated samples with concentrations
greater than the RDL, or less than the MDL were not qualified.
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Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-3 (0-6) TPH (GC/FID) Low Fraction 2.32 B J 2.82 U 3
S-3 (6-12) TPH (GC/FID) Low Fraction 2.91 B J 3.08 U 3
S-30 (6-12) TPH (GC/FID) Low Fraction 3.36 B 3.36 J+ 3
S-8 (0-6) TPH (GC/FID) Low Fraction 1.4 B J 2.59 U 3
S-7 (6-12) TPH (GC/FID) Low Fraction 3.67 B 3.67 J+ 3
S-1 (0-6) TPH (GC/FID) Low Fraction 6.95 B 6.95 J+ 3
S-1 (6-12) TPH (GC/FID) Low Fraction 2.93 B J 3.38 U 3
SS-1 (6-12) TPH (GC/FID) Low Fraction 3.14 B J 3.36 U 3
S-13 (0-6) TPH (GC/FID) Low Fraction 1.25 B J 3.51 U 3
S-15 (0-6) TPH (GC/FID) Low Fraction 4.76 B 4.76 J+ 3
S-32 (0-6) TPH (GC/FID) Low Fraction 1.18 B J 3.56 U 3
S-12 (6-12) TPH (GC/FID) Low Fraction 2.02 B J 3.37 U 3
S-12 (0-6) TPH (GC/FID) Low Fraction 1.5 B J 3.04 U 3
S-10 (0-6) TPH (GC/FID) Low Fraction 4.59 B 4.59 J+ 3
S-10 (6-12) TPH (GC/FID) Low Fraction 0.954 B J 3.04 U 3
S-14 (0-6) TPH (GC/FID) Low Fraction 1.37 B J 3.7 U 3
S-11 (0-6) TPH (GC/FID) Low Fraction 0.834 B J 2.64 U 3
S-14 (6-12) TPH (GC/FID) Low Fraction 1.12 B J 3.58 U 3
mg/Kg-milligram per kilogram
B-Laboratory flag denoting the target analyte was detected in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
4.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). Two sample specific MS/MSD pairs were reported using samples
S-3 (0-6) and S-10 (0-6). The recovery and RPD results were within the laboratory specified
acceptance criteria.
Batch MS/MSD pairs were reported for batches WG2327971, WG2377924 and WG2378697.
Since these were batch QC the results were not qualified.
MS/MSDs were not reported for batches WG2328825, WG2329459, WG2329829, WG2329941,
WG2330767, and WG2377829. Accuracy was assessed using an LCS for batches WG2328825,
WG2329459, WG2330767, and WG2377829. Accuracy and precision were assessed using an
LCS/LCSD pair for batches WG2329829 and WG2329941.
4.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). LCS/LCSD pairs and LCSs were reported. The recovery and RPD results
were within the laboratory specified acceptance criteria.
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4.6 Equipment Blank
Two equipment blanks, EB-1-071624 and EB-93024, were collected with the sample set. TPH low
fraction was not detected in the equipment blanks at or above the MDLs.
4.7 Field Duplicate
Three field duplicates were collected with the sample set: S-30 (6-12), S-31 (0-6), and S-32 (0-6).
Acceptable precision (RPD<50%) were demonstrated between the field duplicates and the original
samples S-3 (6-12), S-4 (0-6), and S-13 (0-6) respectively, with the following exceptions.
TPH low fraction was detected at an estimated concentration greater than or equal to the MDL and
less than the RDL in sample S-3 (6-12), but TPH low fraction was detected at a concentration
greater than the RDL in field duplicate sample S-30 (6-12), resulting in a non-calculable RPD.
Therefore, the TPH low fraction data of sample S-3 (6-12) and field duplicate S-30 (6-12) were J
qualified as estimated. Since the TPH low fraction result for S-3 (6-12) was also U qualified due
to method blank contamination, the final qualification is UJ as estimated not detected at the RDL.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-3 (6-12) TPH (GC/FID) Low
Fraction
2.91 B J NC 2.91 UJ 7
S-30 (6-12) TPH (GC/FID) Low
Fraction
3.36 B 3.36 J 7
mg/Kg-milligram per kilogram
B-Laboratory flag denoting the analyte was detected in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
NC-Not calculable
4.8 Sensitivity
The samples were reported to the MDL. Elevated non-detect results were not reported.
4.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD
5.0 Volatile Organic Compounds
The samples were analyzed for VOCs by US EPA Method 8260B. The areas of data review are
listed below. A leading check mark () indicates an area of review in which the data were
acceptable. A preceding crossed circle (⊗) signifies areas where issues were raised during the
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course of the validation review and should be considered to determine any impact on data quality
and usability.
 Overall Assessment
 Holding Times
⊗ Method Blank
⊗ Matrix Spike/Matrix Spike Duplicate
⊗ Laboratory Control Sample
 Surrogates
 Equipment Blank
 Trip Blank
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

5.1 Overall Assessment
The VOCs data reported in this sample set are considered usable for supporting project objectives.
The results are considered valid; the analytical completeness defined as the ratio of the number of
valid analytical results (valid analytical results include values qualified as estimated) to the total
number of analytical results requested on samples submitted for analysis, for the sample set is
100%.
5.2 Holding Times
The holding times for the VOCs analysis of water and soil samples are 14 days from collection to
analysis. The holding times were met for the sample analyses.
5.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Nine method blanks were reported (batches WG2327390,
WG2329486, WG2329510, WG2329566, WG2379147, WG2380545, WG2379334,
WG2380092, and WG2381936). VOCs were not detected in the method blanks at or above the
MDLs, with the following exceptions.
L1757957: Naphthalene (0.00772 mg/kg) was detected at an estimated concentration greater than
or equal to the MDL and less than the RDL in the method blank of batch WG2329566. Therefore,
the naphthalene concentrations greater than the RDL and less than ten times the method blank
concentration were J+ qualified as estimated with high bias.
L1784578: 1,4-Dichlorobenzene (0.000775 mg/kg) was detected at an estimated concentration
greater than or equal to the MDL and less than the RDL in the method blank of batch WG2380545.
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However, since 1,4-dichlorobenzene was not detected in the associated samples at concentration
greater than or equal to the MDLs, no qualifications were applied to the 1,4-dichlorobenzene data.
L1784578: Methylene chloride (0.000518 mg/kg) was detected at an estimated concentration
greater than or equal to the MDL and less than the RDL in the method blank of batch WG2379334.
However, since methylene chloride was not detected in the associated samples at concentrations
greater than or equal to the MDLs, no qualifications were applied to the methylene chloride data.
L1784578: Methylene chloride was detected at estimated concentrations greater than or equal to
the MDLs and less than the RDLs in the method blanks of batches WG2379147 (0.00888 mg/kg)
and WG2380545 (0.0130 mg/kg). Methylene chloride was detected at estimated concentrations
greater than or equal to the MDLs and less than the RDLs in samples: S-15 (0-6), S-12 (6-12), S-
12 (0-6), S-10 (0-6), S-10 (6-12), and S-32 (0-6). Therefore, based on technical and professional
judgement, the estimated methylene chloride data of the associated samples were U qualified as
non-detect and reported at the RDLs.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-1 (0-6) Naphthalene 0.0453 B 0.0453 J+ 3
S-1 (6-12) Naphthalene 0.0477 B 0.0477 J+ 3
SS-1 (6-12) Naphthalene 0.0315 B 0.0315 J+ 3
S-15 (0-6) Methylene Chloride 0.00985 B J 0.0347 U 3
S-32 (0-6) Methylene Chloride 0.0113 B J 0.0356 U 3
S-12 (6-12) Methylene Chloride 0.0103 B J 0.0337 U 3
S-12 (0-6) Methylene Chloride 0.00871 B J 0.0304 U 3
S-10 (0-6) Methylene Chloride 0.0134 B J 0.0319 U 3
S-10 (6-12) Methylene Chloride 0.0098 B J 0.0304 U 3
mg/Kg-milligram per kilogram
B-Laboratory flag denoting the associated analyte was detected in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
5.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). Two sample specific MS/MSD pairs were reported using samples
S-3 (0-6) and S-10 (0-6). The recovery and RPD results were within the laboratory specified
acceptance criteria, with the following exceptions.
A batch MS/MSD pair was reported for batch WG2380545. Since these were batch QC the results
were not qualified.
L1757957: The RPD of acetone between the MS and MSD of sample S-3 (0-6) was high and
outside of the laboratory specified acceptance criteria. Since acetone was not detected in sample
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S-3 (0-6) at concentrations greater than or equal to the MDL, no qualifications were applied to the
acetone data.
L1784578: The recovery of toluene in the MS of sample S-10 (0-6) was low and outside of the
laboratory specified acceptance criteria. Therefore, the detected toluene data of sample S-10 (0-6)
was J qualified as estimated.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-10 (0-6) Toluene 0.169 J6 0.169 J 4
mg/Kg-milligram per kilogram
J6-Laboratory flag denoting matrix interference and low spike recovery
MS/MSDs were not reported for batches WG2327390, WG2329510, WG2329566, WG2379334,
WG2380092, and WG2381936. Accuracy was assessed using an LCS for batches WG2329510,
WG2329566, and WG2380092. Accuracy and precision were assessed using an LCS/LCSD pair
for batches WG2327390, WG2379334, and WG2381936.
5.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). LCS/LCSD pairs and LCSs were reported. The recovery and RPD results
were within the laboratory specified acceptance criteria, with the following exceptions.
L1757957: The recoveries of chloroethane in the LCS/LCSD of batch WG2327390 were high and
outside of the laboratory specified acceptance criteria. Since chloroethane was not detected in the
associated samples at or above the MDLs, no qualifications were applied to the chloroethane data.
L1757957: The RPD of chloromethane between the LCS and LCSD of batch WG2329486 was
high and outside of the laboratory specified acceptance criteria. Since chloromethane was not
detected in associated samples at concentrations greater than or equal to the MDLs, no
qualifications were applied to the chloromethane data.
L1757957: The recovery of chloroethane in the LCS of batch WG2329566 was high and outside
of the laboratory specified acceptance criteria. Since chloroethane was not detected in the
associated samples at concentrations greater than or equal to the MDLs, no qualifications were
applied to the chloroethane data.
L1784578: The recoveries chloroethane, 1,1-dichloroethene, and 1,1,2-trichlorotrifluoroethane in
one or both the LCS/LCSD of batch WG2379147 were high and outside of the laboratory specified
acceptance criteria. Since these analytes were not detected in the associated samples at
concentrations greater than or equal to the MDLs, no qualifications were applied to the data.
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L1784578: The recoveries of bromomethane in the LCS/LCSD of batch WG2379334 were high
and outside of the laboratory specified acceptance criteria. Since bromomethane was not detected
in the associated samples at concentrations greater than or equal to the MDLs, no qualifications
were applied to the data.
L1784578: The recoveries of 1,2-dibromo-3-chloropropane in the LCS/LCSD of batch
WG2379334 were low and outside of the laboratory specified acceptance criteria. Therefore, the
non-detect 1,2-dibromo-3-chloropropane data of the associated samples were UJ qualified as
estimated non-detect.
L1784578: The recovery of cis-1,3-dichloropropene in the LCS of batch WG2380092 was low
and outside of the laboratory specified acceptance criteria. Therefore, the non-detect cis-1,3-
dichloropropene data of the associated samples were UJ qualified as estimated non-detect.
L1784578: The recovery of 2,2-dichloropropane in the LCS of batch WG2380092 was high and
outside of the laboratory specified acceptance criteria. Since 2,2-dichloropropane was not detected
in the associated samples at concentrations greater than or equal to the MDLs no qualifications
were applied to the 2,2-dichloroprpane data.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
EB-93024 Cis-1,3-Dichloropropene 0.000111 U J4 0.000111 UJ 5
TRIP
BLANK
1,2-Dibromo-3-Chloropropane 0.000276 U J4 0.000276 UJ 5
mg/Kg-milligram per kilogram
U-Laboratory flag denoting a non-detect concentration less than the MDL
J4-Laboratory flag denoting the associated batch QC was outside of the quality control range for accuracy
5.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
5.7 Equipment Blank
Two equipment blanks, EB-1-071624 and EB-93024, were collected with the sample set. VOCs
were not detected in the equipment blanks at or above the MDLs.
5.8 Trip Blank
Two trip blanks, both identified as TRIP BLANK, were collected with the sample set. VOCs were
not detected in the trip blanks at or above the MDLs.
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5.9 Field Duplicate
Three field duplicates were collected with the sample set: S-30 (6-12), S-31 (0-6), and S-32 (0-6).
Acceptable precision (RPD<50%) were demonstrated between the field duplicates and the original
samples S-3 (6-12), S-4 (0-6), and S-13 (0-6) respectively, with the following exceptions.
The RPDs of ethylbenzene, p-isopropyltoluene, toluene, 1,2,4-trimethylbenzene, 1,2,3-
trimethylbenzene, 1,3,5-trimethylbenzene, and total xylenes between the field duplicate S-30 (6-
12) and original sample S-3 (6-12) were high and outside of the laboratory specified acceptance
criteria. Therefore, the ethylbenzene, P-isopropyltoluene, toluene, 1,2,4-trimethylbenzene, 1,2,3-
trimethylbenzene, 1,3,5-trimethylbenzene, and total xylenes data of the field duplicate S-30 (6-12)
and original sample S-3 (6-12) were J qualified as estimated.
Isopropylbenzene was detected at an estimated concentration greater than or equal to the MDL
and less than the RDL in the field duplicate sample S-30 (6-12), but isopropylbenzene was detected
above the RDL in sample S-3 (6-12), resulting in a non-calculable RPD. Therefore, the
isopropylbenzene data of field duplicate S-30 (6-12) and original sample S-3 (6-12) were J
qualified as estimated.
The RPDs of benzene, ethylbenzene, toluene, and total xylenes between the field duplicate S-31
(0-6) and original sample S-4 (0-6) were high and outside of the laboratory specified acceptance
criteria. Therefore, the benzene, ethylbenzene, toluene, and total xylenes data of field duplicate S-
31 (0-6) and original sample S-4 (0-6) were J qualified as estimated.
Isopropylbenzene and methylene chloride were detected at estimated concentrations greater than
or equal to the MDLs and less than the RDLs in the field duplicate sample S-31 (0-6), but were
not detected at or above the MDLs in the original sample S-4 (0-6); resulting in a non-calculable
RPD. Therefore, the non-detect isopropylbenzene and methylene chloride data were UJ qualified
as estimated non detect, and the detected isopropyl and methylene chloride data were J qualified
as estimated.
Ethylbenzene, p-isopropyltoluene, methylene chloride, and total xylenes were detected at
estimated concentrations greater than or equal to the MDLs and less than the RDLs in the field
duplicate sample S-32 (0-6), but were not detected at or above the MDLs in the original sample S-
13 (0-6); resulting in a non-calculable RPD. Since the non-detect results were reported to the RDL
and based on professional and technical judgment, no qualifications were applied to the data.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-3 (6-12) Ethylbenzene 0.00786 NA 81 0.00786 J 7
S-30 (6-12) Ethylbenzene 0.00332 NA 0.00332 J 7
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Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-3 (6-12) Isopropylbenzene 0.00427 NA NC 0.00427 J 7
S-30 (6-12) Isopropylbenzene 0.00186 J 0.00186 J 7
S-3 (6-12) P-Isopropyltoluene 0.0367 NA 107 0.0367 J 7
S-30 (6-12) P-Isopropyltoluene 0.0111 NA 0.0111 J 7
S-3 (6-12) Toluene 0.039 NA 87 0.039 J 7
S-30 (6-12) Toluene 0.0153 NA 0.0153 J 7
S-3 (6-12) 1,2,4-
Trimethylbenzene
0.0536 NA 86 0.0536 J 7
S-30 (6-12) 1,2,4-
Trimethylbenzene
0.0213 NA 0.0213 J 7
S-3 (6-12) 1,2,3-
Trimethylbenzene
0.0344 NA 66 0.0344 J 7
S-30 (6-12) 1,2,3-
Trimethylbenzene
0.0173 NA 0.0173 J 7
S-3 (6-12) 1,3,5-
Trimethylbenzene
0.0233 NA 77 0.0233 J 7
S-30 (6-12) 1,3,5-
Trimethylbenzene
0.0104 NA 0.0104 J 7
S-3 (6-12) Xylenes, Total 0.0836 NA 58 0.0836 J 7
S-30 (6-12) Xylenes, Total 0.046 NA 0.046 J 7
S-4 (0-6) Benzene 0.0163 NA 119 0.0163 J 7
S-31 (0-6) Benzene 0.00413 NA 0.00413 J 7
S-4 (0-6) Ethylbenzene 0.0112 NA 53 0.0112 J 7
S-31 (0-6) Ethylbenzene 0.00649 NA 0.00649 J 7
S-4 (0-6) Toluene 0.0718 NA 100 0.0718 J 7
S-31 (0-6) Toluene 0.024 NA 0.024 J 7
S-4 (0-6) Xylenes, Total 0.12 NA 61 0.12 J 7
S-31 (0-6) Xylenes, Total 0.0641 NA 0.0641 J 7
mg/Kg-milligram per kilogram
NC-non calculable
NA-not applicable
J-laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
5.10 Sensitivity
The samples were reported to the MDL. Elevated non-detect results were not reported.
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5.11 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD
6.0 TPH High Fraction
The samples were analyzed for TPH high fraction by US EPA Method 8015/3511. The areas of
data review are listed below. A leading check mark () indicates an area of review in which the
data were acceptable. A preceding crossed circle (⊗) signifies areas where issues were raised
during the course of the validation review and should be considered to determine any impact on
data quality and usability.
 Overall Assessment
 Holding Times
⊗ Method Blank
⊗ Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Surrogates
 Equipment Blank
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

6.1 Overall Assessment
The TPH high fraction data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
6.2 Holding Times
The holding times for the TPH high fraction analysis of a soil sample are 14 days from collection
to extraction, and 40 days from extraction to analysis. The holding times for the TPH high fraction
analysis of a water sample are 7 days from collection to extraction, and 40 days from extraction to
analysis. It was noted the holding time was document as 14 days in the QAPP. The holding times
were met for the sample analyses.
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6.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Five method blanks were reported (batches WG2330427,
WG2331405, WG2380823, WG2380134 and WG2380815). TPH high fraction was not detected
in the method blanks at or above the MDL, with the following exceptions.
TPH high fraction (0.0252 mg/L) was detected at an estimated concentration greater than or equal
to the MDL and less than the RDL in the method blank of batch WG2330427. Therefore, based
on technical and professional judgement, the TPH high fraction data of sample EB-1-071624 was
qualified U as non-detect and reported at the RDL.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
EB-1-
071624
TPH (GC/FID) High Fraction 0.0688 B J 0.1 U 3
mg/Kg-milligram per kilogram
B-Laboratory flag denoting the analyte was detected in the associated method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
6.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). Two sample specific MS/MSD pairs were reported using samples
S-3 (0-6) and S-10 (0-6). The recovery and RPD results were within the laboratory specified
acceptance criteria, with the following exceptions.
L1784578: The recoveries of TPH high fraction in the MS and MSD of sample S-10 (0-6) were
low and outside of the laboratory specified acceptance criteria. Therefore, the TPH high fraction
data of sample S-10 (0-6) was J qualified as estimated.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-10 (0-6) TPH (GC/FID) High Fraction 49.8 J J6 49.8 J 4
mg/Kg-milligram per kilogram
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
J6-Laboratory flag denoting matrix interference with low spike recovery
A batch MS/MSD was reported for batch WG2380815. Since this was batch QC the results were
not qualified.
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Sample specific MS/MSD pairs were not reported for batches: WG2330427 and WG2380823.
Accuracy and precision were assessed using an LCS/LCSD pair for batches WG2330427 and
WG2380823.
6.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). LCS/LCSD pairs and LCSs were reported. The recovery and RPD results
were within the laboratory specified acceptance criteria.
6.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria, with the
following exception.
The recovery of the surrogate o-Terphenyl in the MS and MSD of sample S-10 (0-6) were flagged
‘J7’ by the laboratory indicating that the surrogate recoveries could not be used for control limit
evaluation due to dilution. Due to technical and professional judgement, no qualifications were
applied to the surrogate data of the MS/MSD of sample S-10 (0-6).
6.7 Equipment Blank
Two equipment blanks, EB-1-071624 and EB-93024, were collected with the sample set; however,
they were not analyzed for TPH high fraction, with the following exception.
L1757957: TPH high fraction (0.0688 mg/L) was detected in EB-1-071624 at an estimated
concentration greater than the MDL and less than the RDL.
6.8 Field Duplicate
Three field duplicates were collected with the sample set: S-30 (6-12), S-31 (0-6), and S-32 (0-6).
Acceptable precision (RPD<50%) were demonstrated between the field duplicates and the original
samples S-3 (6-12), S-4 (0-6), and S-13 (0-6) respectively, with the following exceptions.
TPH high fraction was detected at an estimated concentration greater than or equal to the MDL
and less than the RDL in the field duplicate sample S-32 (0-6), but was detected above the RDL
in sample S-13 (0-6); resulting in a non-calculable RPD. Therefore, the TPH high fraction data of
field duplicate S-32 (0-6) and sample S-13 (0-6) were J qualified as estimated.
Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-13 (0-6) TPH (GC/FID) High
Fraction
6.92 NA NC 6.92 J 7
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Sample ID Compound Laboratory
Result
(mg/Kg)
Laboratory
Flag
RPD Validation
Result
(mg/Kg)
Validation
Qualifier
Reason
Code
S-32 (0-6) TPH (GC/FID) High
Fraction
3.17 J 3.17 J 7
mg/Kg-milligram per kilogram
NA-not applicable
NC-non calculable
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
6.9 Sensitivity
The samples were reported to the MDL. Elevated non-detect results were not reported.
6.10 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD

* * * * *
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ATTACHMENT 1
DATA VALIDATION QUALIFIER DEFINITIONS
AND INTERPRETATION KEY
Assigned by Geosyntec’s Data Validation Team

DATA QUALIFIER DEFINITIONS
U The analyte was analyzed for, but was not detected above the reported sample quantitation
limit.
J The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
J+ The analyte was positively identified; however, the associated numerical value is likely to be
higher than the concentration of the analyte in the sample due to positive bias of associated
QC or calibration data or attributable to matrix interference.
J- The analyte was positively identified; however, the associated numerical value is likely to be
lower than the concentration of the analyte in the sample due to negative bias of associated
QC or calibration data or attributable to matrix interference.
UJ The analyte was not detected above the reported sample quantitation limit. However, the
reported quantitation limit is approximate and may or may not represent the actual limit of
quantitation necessary to accurately and precisely measure the analyte in the sample.
R The sample results are rejected due to serious deficiencies in the ability to analyze the sample
and meet quality control criteria. The presence or absence of the analyte cannot be verified.

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ATTACHMENT 2
DATA VALIDATION REASON CODES
Assigned by Geosyntec’s Data Validation Team

Valid Value Description
1 Preservation requirement not met
2 Extraction or analysis holding time exceeded
3 Blank contamination (i.e., method, trip, equipment, etc.)
4 Matrix spike/matrix spike duplicate recovery or RPD outside limits
5 LCS recovery outside limits or RPD outside limits (LCS/LCSD)
6 Surrogate recovery outside limits
7 Field Duplicate RPD exceeded
8 Serial dilution percent difference exceeded
9 Calibration criteria not met
10 Calibration range exceeded
11 Internal standard or isotope dilution standard criteria not met
12 Lab duplicates RPD exceeded
13 Other
14 Lab flag removed
LCS - Laboratory Control Sample
LCSD - Laboratory Control Sample duplicate
RPD - Relative percent difference

180A Market Place Boulevard
Knoxville, TN 37922
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DVR L1758896 R3.docx Final Review: K Henderson 11/26/2024
Memorandum
Date: 26 November 2024
To: Brian Smith
From: Chase Harris
CC: Kristoffer Henderson
Subject: Stage 2A Data Validation - Level II Data Deliverable – Pace
Analytical National Job ID L1758896
SITE: Paxton
INTRODUCTION
This report summarizes the findings of the Stage 2A data validation of nine groundwater samples
including one sample designated for matrix spike/matrix spike duplicate (MS/MSD) pair analysis,
one trip blank and one field duplicate, collected on 17 July 2024, as part of the Paxton Voluntary
Cleanup Program (VCP), site characterization activities (VCP Site #C-129).
Pace Analytical National Mount Juliet, Tennessee analyzed the samples for the following
analytical tests:
• Oil and Grease by United States (US) Environmental Protection Agency (EPA) Method
1664A
• Total Petroleum Hydrocarbons (TPH) Low Fraction by US EPA Methods 8015D/GRO
• Volatile Organic Compounds (VOCs) by US EPA Method 8260B
• TPH High Fraction by US EPA Methods 3511/8015
EXECUTIVE SUMMARY
Overall, based on this Stage 2A data validation covering the quality control (QC) parameters listed
below and based on the information provided, the data as qualified are usable for supporting project
objectives, with the following exceptions.
The non-detect VOC result for sample MW-10 were R qualified as rejected due to holding time
exceedance.
The qualified data that was not rejected should be used within the limitations of the qualifications.
If there are results with two or more different qualifications due to multiple QC failures, the final
qualification is reconciled in the electronic data deliverable (EDD) with qualifications.
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The data were reviewed based on professional and technical judgment and the following
documents:
• Quality Assurance Project Plan, Paxton Development, 203 to 225 West Paxton Avenue,
Salt Lake City, Utah, Voluntary Cleanup Site #C-129, June 19, 2024 (herein referred to as
the QAPP);
• US EPA Contract Laboratory Program National Functional Guidelines for Organic
Superfund Methods Data Review, November 2020 (EPA 540-R-20-005);
• US EPA Contract Laboratory Program National Functional Guidelines for Superfund
Inorganic Superfund Data Review, November 2020 (EPA 540-R-20-006); and,
• The pertinent methods referenced by the data package.
The following samples were analyzed in the data set:

Laboratory ID Client ID
L1758896-01 MW-1
L1758896-02 MW-25
L1758896-03 MW-2
L1758896-03 MS MW-2 MS
L1758896-03 MSD MW-2 MSD
L1758896-04 MW-4
L1758896-05 MW-8
Laboratory ID Client ID
L1758896-06 MW-3
L1758896-07 MW-7
L1758896-08 MW-5
L1758896-09 MW-10
L1758896-10 MW-9
L1758896-11 TRIP BLANK
The samples were received within 0-6°C. No preservation issues were noted by the laboratory.
The laboratory reported results for the analytical method(s) requested for each sample on the chain
of custody (COC).
The data validation report was revised on November 25, 2024, to use the method detection limits
(MDLs) for the non-detect results and to correct a qualification.
The data validation report was revised on November 26, 2024, to correct the completeness
percentage for the VOC data.
The data validation report was revised on November 26, 2024, to correct make edits.
1.0 Oil and Grease
The samples were analyzed for oil and grease by US EPA method 1664A.
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The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the validation review and should be considered to determine any impact on data
quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

1.1 Overall Assessment
The oil and grease data reported in this data set are considered usable for supporting project
objectives. The analytical completeness, defined as the ratio of the number of valid analytical
results (valid analytical results include values qualified as estimated) to the total number of
analytical results requested on samples submitted for this analysis, for the data set is 100%.
1.2 Holding Times
The holding time for oil and grease analysis of a preserved water sample is 28 days from sample
collection to analysis. The holding times were met for the sample analyses.
1.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). One method blank was reported for oil and grease by US
EPA method 1664A (batch WG2331265). Oil and grease were not detected in the method blank
at or above the MDL.
1.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). One sample specific MS/MSD pair was reported using sample MW-
2. The recovery and relative percent difference (RPD) results were within the laboratory specified
acceptance criteria, with the following exceptions.
The recovery of oil and grease in the MS of sample MW-2 was high and outside of the laboratory
specified acceptance criteria. Since oil and grease was not detected in sample MW-2 at a
concentration greater than the MDL, no qualifications were applied to the data.
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1.5 Laboratory Control Sample (LCS)
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS/LCS duplicate (LCSD) pair was reported for batch
WG2331265. The recovery and RPD results were within the laboratory specified acceptance
criteria.
1.6 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was not demonstrated between the field duplicate and the original sample MW-1.
Oil and grease were not detected in the original sample MW-1 at or above the MDL. Oil and grease
were detected at an estimated concentration greater than or equal to the MDL and less than the
reporting detection limit (RDL) in the field duplicate sample MW-25, resulting in a non-calculable
RPD between MW-1 and MW-25. Therefore, based on technical and professional judgement the
oil and grease data were J or UJ qualified as estimated or estimated non-detect.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
RPD Validation
Result (mg/L)
Validation
Qualifier*
Reason
Code**
MW-1 Oil & Grease
(Hexane Extr)
1.29 U NC 1.29 UJ 7
MW-25 Oil & Grease
(Hexane Extr)
1.68 J 1.68 J 7
mg/L-milligram per liter
U-Laboratory flag denoting a non-detect concentration less than the MDL
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
NC-Not calculable
* Validation qualifiers are defined in Attachment 1 at the end of this report
**Reason codes are defined in Attachment 2 at the end of this report
1.7 Sensitivity
The samples were evaluated to the MDLs. Elevated non-detect results were not reported.
1.8 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDLs and RDLs, however, only the RDLs were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.
2.0 Total Petroleum Hydrocarbons Low Fraction
The samples were analyzed for TPH low fraction by US EPA method 8015D/GRO.
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The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
 Overall Assessment
⊗ Holding Times
⊗ Method Blank
⊗ Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Surrogates
 Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review
2.1 Overall Assessment
2.1.1 Completeness
The TPH low fraction data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
2.1.2 Analysis Anomaly
The pH’s of samples MW-2, MW-10, and MW-9 did not meet the method criteria of pHs ≤ 2.
Therefore, the samples were considered unpreserved.
2.2 Holding Time
The holding time for TPH low fraction analysis of a preserved water sample is 14 days from sample
collection to analysis. The holding time for TPH low fraction analysis of an unpreserved water
sample is 7 days from sample collection to analysis. The holding times were met for the sample
analyses, with the following exception.
Sample MW-2 was analyzed outside the holding time of an unpreserved sample. Therefore, the
TPH low fraction concentration for sample MW-2 was J qualified as estimated.
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Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-2 TPH (GC/FID)
Low Fraction
0.139 B J3 0.139 J 2
mg/L-milligram per liter
B-Laboratory flag denoting the target analyte was detected in the method blank
J3-Laboratory flag denoting the associated batch QC was outside of the established quality control range for precision
2.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). One method blank was reported for TPH low fraction by
US EPA method 8015D/GRO (batch WG2329885).
TPH low fraction (0.0744 mg/L) was detected in the method blank at an estimated concentration
greater than or equal to the MDL and less than the RDL.
Therefore, based on technical and professional judgement, the TPH low fraction data with
estimated recoveries greater than or equal to the MDL and less than the RDL were U qualified as
non-detect and reported at the RDL. In addition, the TPH low fraction concentrations greater the
RDL and less than five times the method blank concentration were J+ qualified as estimated with
high bias. The TPH low fraction data with concentrations greater than five times the method blank
concentration were not qualified. Since the TPH low fraction concentration for sample MW-2 was
also qualified for holding time exceedance and MS/MSD RPD outside criteria, the final
qualification was J qualified as estimated.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-1 TPH (GC/FID)
Low Fraction
0.0502 B J 0.1 U 3
MW-25 TPH (GC/FID)
Low Fraction
0.0556 B J 0.1 U 3
MW-2 TPH (GC/FID)
Low Fraction
0.139 B J3 0.139 J 3
MW-4 TPH (GC/FID)
Low Fraction
0.254 B 0.254 J+ 3
MW-3 TPH (GC/FID)
Low Fraction
0.089 B J 0.1 U 3
MW-10 TPH (GC/FID)
Low Fraction
0.0522 B J 0.1 U 3
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Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-9 TPH (GC/FID)
Low Fraction
0.0508 B J 0.1 U 3
mg/L-milligram per liter
B-Laboratory flag denoting the target analyte was detected in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
2.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). One sample specific MS/MSD pair was reported using sample MW-
2. The recovery and RPD results were within the laboratory specified acceptance criteria, with the
following exceptions.
The RPD of TPH low fraction between the MS and MSD of sample MW-2 was high and outside
of the laboratory specified acceptance criteria. Therefore, the detected TPH low fraction data of
sample MW-2 was J qualified as estimated.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-2 TPH (GC/FID)
Low Fraction
0.139 B J3 0.139 J 4
mg/L-milligram per liter
B-Laboratory flag denoting the target analyte was detected in the method blank
J3-Laboratory flag denoting the associated batch QC was outside of the established quality control range for precision
2.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS was reported. The recovery result was within the laboratory
specified acceptance criteria.
2.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
2.7 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample MW-1.
2.8 Sensitivity
The samples were evaluated to the MDLs. Elevated non-detect results were not reported.
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2.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDLs and RDLs, however, only the RDLs were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.
3.0 VOLATILE ORGANIC COMPOUNDS
The samples were analyzed for VOCs by US EPA method 8260B.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
⊗ Overall Assessment
⊗ Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Surrogates
 Trip Blank
 Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review
3.1 Overall Assessment
3.1.1 Completeness
The VOCs data reported in this sample set are considered usable for supporting project objectives,
with the following exceptions.
The non-detect VOC result for sample MW-10 were R qualified as rejected due to holding time
exceedance.
Therefore, the analytical completeness defined as the ratio of the number of valid analytical results
(valid analytical results include values qualified as estimated) to the total number of analytical
results requested on samples submitted for analysis, for the sample set is 91.0%.
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3.1.2 Analysis Anomaly
The pH of sample MW-10 did not meet the method criteria of pHs ≤ 2. Therefore, the sample was
considered unpreserved.
3.2 Holding Times
The holding times for the VOCs analysis of preserved water samples is 14 days from sample
collection to analysis. The holding times for the VOCs analysis of unpreserved water samples is 7
days from sample collection to analysis. The holding times were met for the sample analyses, with
the following exception.
Sample MW-10 was analyzed outside the holding time of an unpreserved sample. Therefore, the
non-detect VOC results were R qualified as rejected and the cis-1,2-Dichloroethene concentration
was J qualified as estimated for sample MW-10.
Sample Analyte Laboratory
Result
(mg/L)
Laboratory
Flag
Validation
Result
(mg/L)
Validation
Qualifier
Reason
Code
MW-10 Acetone 0.0113 U 0.0113 R 2
MW-10 Acrolein 0.00254 U J4 0.00254 R 2
MW-10 Acrylonitrile 0.000671 U 0.000671 R 2
MW-10 Benzene 0.0000941 U 0.0000941 R 2
MW-10 Bromobenzene 0.000118 U 0.000118 R 2
MW-10 Bromodichloromethane 0.000136 U 0.000136 R 2
MW-10 Bromoform 0.000129 U 0.000129 R 2
MW-10 Bromomethane 0.000605 U 0.000605 R 2
MW-10 N-Butylbenzene 0.000157 U 0.000157 R 2
MW-10 Sec-Butylbenzene 0.000125 U 0.000125 R 2
MW-10 Tert-Butylbenzene 0.000127 U 0.000127 R 2
MW-10 Carbon Tetrachloride 0.000128 U 0.000128 R 2
MW-10 Chlorobenzene 0.000116 U 0.000116 R 2
MW-10 Chlorodibromomethane 0.00014 U 0.00014 R 2
MW-10 Chloroethane 0.000192 U 0.000192 R 2
MW-10 Chloroform 0.000111 U 0.000111 R 2
MW-10 Chloromethane 0.00096 U 0.00096 R 2
MW-10 2-Chlorotoluene 0.000106 U 0.000106 R 2
MW-10 4-Chlorotoluene 0.000114 U 0.000114 R 2
MW-10 1,2-Dibromo-3-Chloropropane 0.000276 U 0.000276 R 2
MW-10 1,2-Dibromoethane 0.000126 U 0.000126 R 2
MW-10 Dibromomethane 0.000122 U 0.000122 R 2
MW-10 1,2-Dichlorobenzene 0.000107 U 0.000107 R 2
MW-10 1,3-Dichlorobenzene 0.00011 U 0.00011 R 2
MW-10 1,4-Dichlorobenzene 0.00012 U 0.00012 R 2
MW-10 Dichlorodifluoromethane 0.000374 U 0.000374 R 2
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Sample Analyte Laboratory
Result
(mg/L)
Laboratory
Flag
Validation
Result
(mg/L)
Validation
Qualifier
Reason
Code
MW-10 1,1-Dichloroethane 0.0001 U 0.0001 R 2
MW-10 1,2-Dichloroethane 0.0000819 U 0.0000819 R 2
MW-10 1,1-Dichloroethene 0.000188 U 0.000188 R 2
MW-10 Cis-1,2-Dichloroethene 0.000166 J 0.000166 J 2
MW-10 Trans-1,2-Dichloroethene 0.000149 U 0.000149 R 2
MW-10 1,2-Dichloropropane 0.000149 U 0.000149 R 2
MW-10 1,1-Dichloropropene 0.000142 U 0.000142 R 2
MW-10 1,3-Dichloropropane 0.00011 U 0.00011 R 2
MW-10 Cis-1,3-Dichloropropene 0.000111 U 0.000111 R 2
MW-10 Trans-1,3-Dichloropropene 0.000118 U 0.000118 R 2
MW-10 2,2-Dichloropropane 0.000161 U 0.000161 R 2
MW-10 Di-Isopropyl Ether 0.000105 U 0.000105 R 2
MW-10 Ethylbenzene 0.000137 U 0.000137 R 2
MW-10 Hexachloro-1,3-Butadiene 0.000337 U 0.000337 R 2
MW-10 Isopropylbenzene 0.000105 U 0.000105 R 2
MW-10 P-Isopropyltoluene 0.00012 U 0.00012 R 2
MW-10 2-Butanone (MEK) 0.00119 U 0.00119 R 2
MW-10 Methylene Chloride 0.00043 U 0.00043 R 2
MW-10 4-Methyl-2-Pentanone (MIBK) 0.000478 U 0.000478 R 2
MW-10 Methyl Tert-Butyl Ether 0.000101 U 0.000101 R 2
MW-10 Naphthalene 0.001 U 0.001 R 2
MW-10 N-Propylbenzene 0.0000993 U 0.0000993 R 2
MW-10 Styrene 0.000118 U 0.000118 R 2
MW-10 1,1,1,2-Tetrachloroethane 0.000147 U 0.000147 R 2
MW-10 1,1,2,2-Tetrachloroethane 0.000133 U 0.000133 R 2
MW-10 1,1,2-Trichlorotrifluoroethane 0.00018 U 0.00018 R 2
MW-10 Tetrachloroethene 0.0003 U 0.0003 R 2
MW-10 Toluene 0.000278 U 0.000278 R 2
MW-10 1,2,3-Trichlorobenzene 0.00023 U 0.00023 R 2
MW-10 1,2,4-Trichlorobenzene 0.000481 U 0.000481 R 2
MW-10 1,1,1-Trichloroethane 0.000149 U 0.000149 R 2
MW-10 1,1,2-Trichloroethane 0.000158 U 0.000158 R 2
MW-10 Trichloroethene 0.00019 U 0.00019 R 2
MW-10 Trichlorofluoromethane 0.00016 U 0.00016 R 2
MW-10 1,2,3-Trichloropropane 0.000237 U 0.000237 R 2
MW-10 1,2,4-Trimethylbenzene 0.000322 U 0.000322 R 2
MW-10 1,2,3-Trimethylbenzene 0.000104 U 0.000104 R 2
MW-10 1,3,5-Trimethylbenzene 0.000104 U 0.000104 R 2
MW-10 Vinyl Chloride 0.000234 U 0.000234 R 2
MW-10 Xylenes, Total 0.000174 U 0.000174 R 2
mg/L-milligrams per liter
J-estimated concentration greater than the MDL and less than the RDL
U-not detected at or above the RDL
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3.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Three method blanks were reported (batches WG2330260,
WG2330346 and WG2332276). VOCs were not detected in the method blanks at or above the
MDL.
3.4 Matrix Spike/Matrix Spike Duplicate
One sample specific MS/MSD pair was reported using sample MW-2. The recovery and RPD
results were within the laboratory specified acceptance criteria, with the following exceptions.
Cis-1,2-dichloroethene was flagged ‘V’ by the laboratory indicating the concentration of cis-1,2-
dichloroethene in the original sample, MW-2, was greater than the spike concentration. Therefore,
based on technical and professional judgement, no qualifications were applied to the data.
The recoveries of acrolein, carbon tetrachloride, chloroethane, 1,2-dichloroethane, 1,1,2-
trichlorotrifluoroethane, and trichlorofluoromethane in the MS/MSD of sample MW-2 were high
and outside of the laboratory specified acceptance criteria. Since these analytes were not detected
in sample MW-2 at concentrations greater than or equal to the MDLs, no qualifications were
applied to the data.
The recovery of methylene chloride in the MSD of sample MW-2 was high and outside of the
laboratory specified acceptance criteria. Since methylene chloride was not detected in sample
MW-2 at concentrations greater than or equal to the MDL, no qualifications were applied to the
data.
Sample specific MS/MSDs were not reported for batches WG2330346 and WG2332276.
Accuracy and precision were assessed using an LCS/LCSD pair for batch WG2330346. Precision
was assessed using an LCS for batch WG2332276.
3.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS/LCSD pair and two LCSs were reported. The recovery and
RPD results were within the laboratory specified acceptance criteria, with the following
exceptions.
The recovery of acrolein in the LCS of batch WG2330260 was high and outside of the laboratory
specified acceptance criteria. Since acrolein was not detected in the associated samples at
concentrations greater than or equal to the MDL, no qualifications were applied to the data.
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The RPD of vinyl chloride between the LCS and LCSD of batch WG2330346 was high and outside
of the laboratory specified acceptance criteria. Since vinyl chloride was not detected in the
associated samples at concentrations greater than or equal to the MDL, no qualifications were
applied to the data.
3.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
3.7 Trip Blank
One trip blank, TRIP BLANK, accompanied the sample shipment. VOCs were not detected in the
trip blank at or above the MDLs.
3.8 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample MW-1.
3.9 Sensitivity
The samples were evaluated to the MDL. Elevated non-detect results were not reported.
3.10 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDLs and RDLs, however, only the RDLs were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.
4.0 Total Petroleum Hydrocarbons High Fraction
The samples were analyzed for TPH high fraction by US EPA methods 3511/8015 3510C.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
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⊗ Surrogates
 Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

4.1 Overall Assessment
The TPH high fraction data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
4.2 Holding Times
The holding times for the TPH high fraction analysis of a water sample are 7 days from sample
collection to sample extraction and 40 days from sample extraction to analysis. The holding times
were met for the sample analyses.
4.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). One method blank was reported (batch WG2332252).
TPH high fraction were not detected in the method blank at or above the MDL.
4.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). One sample specific MS/MSD pair was reported using sample MW-
2. The recovery and RPD results were within the laboratory specified acceptance criteria.
4.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS was reported. The recovery results were within the laboratory
specified acceptance criteria.
4.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria, with the
following exceptions.
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O-Terphenyl recovered low and outside of the laboratory specified acceptance criteria in the LCS
of batch WG2332252. However, since the spike recovery was within the laboratory specified
acceptance criteria, and due to technical and professional judgement, no qualifications were
applied to the data.
O-Terphenyl recovered low and outside of the laboratory specified acceptance criteria in sample
MW-9. Therefore, based on technical and professional judgement, the detected TPH high fraction
data of sample MW-9 was J- qualified as estimated with low bias.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-9 TPH (GC/FID)
High Fraction
0.164 NA 0.164 J- 6
mg/L-milligram per liter
NA-Not applicable
4.7 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample MW-1.
4.8 Sensitivity
The samples were evaluated to the MDL. Elevated non-detect results were not reported.
4.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDL and RDL, however, only the RDL were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.

* * * * *
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ATTACHMENT 1
DATA VALIDATION QUALIFIER DEFINITIONS
AND INTERPRETATION KEY
Assigned by Geosyntec’s Data Validation Team

DATA QUALIFIER DEFINITIONS
U The analyte was analyzed for, but was not detected above the reported sample quantitation
limit.
J The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
J+ The analyte was positively identified; however, the associated numerical value is likely to be
higher than the concentration of the analyte in the sample due to positive bias of associated
QC or calibration data or attributable to matrix interference.
J- The analyte was positively identified; however, the associated numerical value is likely to be
lower than the concentration of the analyte in the sample due to negative bias of associated
QC or calibration data or attributable to matrix interference.
UJ The analyte was not detected above the reported sample quantitation limit. However, the
reported quantitation limit is approximate and may or may not represent the actual limit of
quantitation necessary to accurately and precisely measure the analyte in the sample.
R The sample results are rejected due to serious deficiencies in the ability to analyze the sample
and meet quality control criteria. The presence or absence of the analyte cannot be verified.

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ATTACHMENT 2
DATA VALIDATION REASON CODES
Assigned by Geosyntec’s Data Validation Team

Valid Value Description
1 Preservation requirement not met
2 Extraction or analysis holding time exceeded
3 Blank contamination (i.e., method, trip, equipment, etc.)
4 Matrix spike/matrix spike duplicate recovery or RPD outside limits
5 LCS recovery outside limits or RPD outside limits (LCS/LCSD)
6 Surrogate recovery outside limits
7 Field Duplicate RPD exceeded
8 Serial dilution percent difference exceeded
9 Calibration criteria not met
10 Calibration range exceeded
11 Internal standard or isotope dilution standard criteria not met
12 Lab duplicates RPD exceeded
13 Other
14 Lab flag removed
LCS - Laboratory Control Sample
LCSD - Laboratory Control Sample duplicate
RPD - Relative percent difference

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DVR L1784259 R1.docx Final Review: K Henderson 11/26/2024
Memorandum
Date: 26 November 2024
To: Brian Smith
From: Chase Harris
CC: Kristoffer Henderson
Subject: Stage 2A Data Validation - Level II Data Deliverable – Pace
Analytical National Job ID L1784259
SITE: Paxton
INTRODUCTION
This report summarizes the findings of the Stage 2A data validation of two soil vapor samples and
one field duplicate, collected on 30 September 2024, as part of the Paxton Voluntary Cleanup
Program (VCP), site characterization activities (VCP Site #C-129).
Pace Analytical National Mount Juliet, Tennessee analyzed the samples for the following
analytical test:
• Volatile Organic Compounds (VOCs) by United States (US) Environmental Protection
Agency (EPA) Method TO-15.
EXECUTIVE SUMMARY
Overall, based on this Stage 2A data validation covering the quality control (QC) parameters listed
below and based on the information provided, the data as qualified are usable for supporting project
objectives. The qualified data should be used within the limitations of the qualifications. If there
are results with two or more different qualifications due to multiple QC failures, the final
qualification is reconciled in the electronic data deliverable (EDD) with qualifications.
The data were reviewed based on professional and technical judgment and the following
documents:
• Quality Assurance Project Plan, Paxton Development, 203 to 225 West Paxton Avenue,
Salt Lake City, Utah, Voluntary Cleanup Site #C-129, June 19, 2024 (herein referred to as
the QAPP);
• US EPA Contract Laboratory Program National Functional Guidelines for Organic
Superfund Methods Data Review, November 2020 (EPA 540-R-20-005);
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• The pertinent methods referenced by the data package.
The following samples were analyzed in the data set:
Laboratory ID Client ID
L1784259-01 SV-1
L1784259-02 SV-2
Laboratory ID Client ID
L1784259-03 SV-20
The samples were received within 0-6°C. No preservation issues were noted by the laboratory.
The laboratory reported results for the analytical method(s) requested for each sample on the COC.
The data validation report was revised on November 26, 2024, to make edits.
1.0 Volatile Organic Compounds
The samples were analyzed for VOCs by US EPA method TO-15.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the validation review and should be considered to determine any impact on data
quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Laboratory Control Sample
 Surrogates
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

1.1 Overall Assessment
The VOC data reported in this data set are considered usable for supporting project objectives. The
analytical completeness, defined as the ratio of the number of valid analytical results (valid
analytical results include values qualified as estimated) to the total number of analytical results
requested on samples submitted for this analysis, for the data set is 100%.
1.2 Holding Times
The holding time for the VOCs analysis of a soil vapor sample is 30 days from sample collection
to analysis. The holding times were met for the sample analyses.
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1.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Two method blanks were reported (batches WG2374030
and WG2376939). VOCs were not detected in the method blanks at or above the method detection
limits (MDLs), with the following exceptions.
Propene and TPH were detected in the method blank of batch WG2374030 at estimated
concentrations greater than or equal to the MDLs and less than the reported detection limits
(RDLs). However, since propene was not detected in the associated samples at concentrations
greater than or equal to the MDL, no qualifications were applied to the propene data. Since the
associated samples had detected concentrations of TPH greater than ten times the concentration of
TPH in the method blank, no qualifications were applied to the TPH data.
1.4 Laboratory Control Sample (LCS)
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). Two LCS/LCS duplicate (LCSD) pairs were reported for batches
WG2374030 and WG2376939. The recovery and relative percent difference (RPD) results were
within the laboratory specified acceptance criteria.
1.5 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
1.6 Field Duplicate
One field duplicate was collected with the sample set, SV-20. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample SV-2, with the following
exceptions.
The RPDs of acetone, 1,1-dichloroethane, cis-1,2-dichloroethene, trans-1,2-dichloroethene,
ethanol, methylene chloride, tetrachloroethene, trichloroethene, and 1,2,4-trimethylbenzene
between the field duplicate sample SV-20 and original sample SV-2 were high and outside of the
laboratory specified acceptance criteria. Therefore, the data of these analytes were J qualified as
estimated in the field duplicate sample SV-20 and original sample SV-2.
Carbon disulfide was not detected at or above the RDL in the field duplicate sample SV-20 but
was detected at a concentration greater than the RDL in the original sample SV-2, resulting in a
non-calculable RPD. Therefore, the carbon disulfide data of the field duplicate sample SV-20 and
original sample SV-2 were UJ or J qualified as estimated non-detect or estimated.
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N-Hexane was not detected at or above the RDL in the field duplicate sample SV-20 but was
detected at a concentration greater than the RDL in the original sample SV-2, resulting in a non-
calculable RPD. Therefore, the n-hexane data of the field duplicate sample SV-20 and original
sample SV-2 were UJ or J qualified as estimated non-detect or estimated.
Sample
ID
Compound Laboratory
Result
(µg/m3)
Laboratory
Flag
RPD Validation
Result
(µg/m3)
Validation
Qualifier
Reason
Code
SV-2 Acetone 13.5 NA 64 13.5 J 7
SV-20 Acetone 6.94 NA 6.94 J 7
SV-2 Carbon Disulfide 1.39 NA NC 1.39 J 7
SV-20 Carbon Disulfide <1.24 U <1.24 UJ 7
SV-2 1,1-Dichloroethane 1040 NA 35 1040 J 7
SV-20 1,1-Dichloroethane 1480 NA 1480 J 7
SV-2 Cis-1,2-Dichloroethene 3920 NA 36 3920 J 7
SV-20 Cis-1,2-Dichloroethene 5630 NA 5630 J 7
SV-2 Trans-1,2-Dichloroethene 227 NA 36 227 J 7
SV-20 Trans-1,2-Dichloroethene 325 NA 325 J 7
SV-2 Ethanol 9.14 NA 51 9.14 J 7
SV-20 Ethanol 5.45 NA 5.45 J 7
SV-2 N-Hexane 2.37 NA NC 2.37 J 7
SV-20 N-Hexane <2.22 U <2.22 UJ 7
SV-2 Methylene Chloride 2.7 NA 75 2.7 J 7
SV-20 Methylene Chloride 1.23 NA 1.23 J 7
SV-2 Tetrachloroethene 733 NA 37 733 J 7
SV-20 Tetrachloroethene 1070 NA 1070 J 7
SV-2 Trichloroethene 836 NA 40 836 J 7
SV-20 Trichloroethene 1250 NA 1250 J 7
SV-2 1,2,4-Trimethylbenzene 2.46 NA 30 2.46 J 7
SV-20 1,2,4-Trimethylbenzene 1.81 NA 1.81 J 7
µg/m3-microgram per cubic meter
NA-not applicable
NC-not calculable
U-Laboratory flag denoting a non-detect concentration less than the RDL
* Validation qualifiers are defined in Attachment 1 at the end of this report
**Reason codes are defined in Attachment 2 at the end of this report
1.7 Sensitivity
The samples were reported to the RDLs. Elevated non-detect results were not reported.
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1.8 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD.

* * * * *
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ATTACHMENT 1
DATA VALIDATION QUALIFIER DEFINITIONS
AND INTERPRETATION KEY
Assigned by Geosyntec’s Data Validation Team

DATA QUALIFIER DEFINITIONS
U The analyte was analyzed for, but was not detected above the reported sample quantitation
limit.
J The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
J+ The analyte was positively identified; however, the associated numerical value is likely to be
higher than the concentration of the analyte in the sample due to positive bias of associated
QC or calibration data or attributable to matrix interference.
J- The analyte was positively identified; however, the associated numerical value is likely to be
lower than the concentration of the analyte in the sample due to negative bias of associated
QC or calibration data or attributable to matrix interference.
UJ The analyte was not detected above the reported sample quantitation limit. However, the
reported quantitation limit is approximate and may or may not represent the actual limit of
quantitation necessary to accurately and precisely measure the analyte in the sample.
R The sample results are rejected due to serious deficiencies in the ability to analyze the sample
and meet quality control criteria. The presence or absence of the analyte cannot be verified.

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ATTACHMENT 2
DATA VALIDATION REASON CODES
Assigned by Geosyntec’s Data Validation Team

Valid Value Description
1 Preservation requirement not met
2 Extraction or analysis holding time exceeded
3 Blank contamination (i.e., method, trip, equipment, etc.)
4 Matrix spike/matrix spike duplicate recovery or RPD outside limits
5 LCS recovery outside limits or RPD outside limits (LCS/LCSD)
6 Surrogate recovery outside limits
7 Field Duplicate RPD exceeded
8 Serial dilution percent difference exceeded
9 Calibration criteria not met
10 Calibration range exceeded
11 Internal standard or isotope dilution standard criteria not met
12 Lab duplicates RPD exceeded
13 Other
14 Lab flag removed
LCS - Laboratory Control Sample
LCSD - Laboratory Control Sample duplicate
RPD - Relative percent difference

180A Market Place Boulevard
Knoxville, TN 37922
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DVR L1758896 R3.docx Final Review: K Henderson 11/26/2024
Memorandum
Date: 26 November 2024
To: Brian Smith
From: Chase Harris
CC: Kristoffer Henderson
Subject: Stage 2A Data Validation - Level II Data Deliverable – Pace
Analytical National Job ID L1758896
SITE: Paxton
INTRODUCTION
This report summarizes the findings of the Stage 2A data validation of nine groundwater samples
including one sample designated for matrix spike/matrix spike duplicate (MS/MSD) pair analysis,
one trip blank and one field duplicate, collected on 17 July 2024, as part of the Paxton Voluntary
Cleanup Program (VCP), site characterization activities (VCP Site #C-129).
Pace Analytical National Mount Juliet, Tennessee analyzed the samples for the following
analytical tests:
• Oil and Grease by United States (US) Environmental Protection Agency (EPA) Method
1664A
• Total Petroleum Hydrocarbons (TPH) Low Fraction by US EPA Methods 8015D/GRO
• Volatile Organic Compounds (VOCs) by US EPA Method 8260B
• TPH High Fraction by US EPA Methods 3511/8015
EXECUTIVE SUMMARY
Overall, based on this Stage 2A data validation covering the quality control (QC) parameters listed
below and based on the information provided, the data as qualified are usable for supporting project
objectives, with the following exceptions.
The non-detect VOC result for sample MW-10 were R qualified as rejected due to holding time
exceedance.
The qualified data that was not rejected should be used within the limitations of the qualifications.
If there are results with two or more different qualifications due to multiple QC failures, the final
qualification is reconciled in the electronic data deliverable (EDD) with qualifications.
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The data were reviewed based on professional and technical judgment and the following
documents:
• Quality Assurance Project Plan, Paxton Development, 203 to 225 West Paxton Avenue,
Salt Lake City, Utah, Voluntary Cleanup Site #C-129, June 19, 2024 (herein referred to as
the QAPP);
• US EPA Contract Laboratory Program National Functional Guidelines for Organic
Superfund Methods Data Review, November 2020 (EPA 540-R-20-005);
• US EPA Contract Laboratory Program National Functional Guidelines for Superfund
Inorganic Superfund Data Review, November 2020 (EPA 540-R-20-006); and,
• The pertinent methods referenced by the data package.
The following samples were analyzed in the data set:

Laboratory ID Client ID
L1758896-01 MW-1
L1758896-02 MW-25
L1758896-03 MW-2
L1758896-03 MS MW-2 MS
L1758896-03 MSD MW-2 MSD
L1758896-04 MW-4
L1758896-05 MW-8
Laboratory ID Client ID
L1758896-06 MW-3
L1758896-07 MW-7
L1758896-08 MW-5
L1758896-09 MW-10
L1758896-10 MW-9
L1758896-11 TRIP BLANK
The samples were received within 0-6°C. No preservation issues were noted by the laboratory.
The laboratory reported results for the analytical method(s) requested for each sample on the chain
of custody (COC).
The data validation report was revised on November 25, 2024, to use the method detection limits
(MDLs) for the non-detect results and to correct a qualification.
The data validation report was revised on November 26, 2024, to correct the completeness
percentage for the VOC data.
The data validation report was revised on November 26, 2024, to correct make edits.
1.0 Oil and Grease
The samples were analyzed for oil and grease by US EPA method 1664A.
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The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the validation review and should be considered to determine any impact on data
quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

1.1 Overall Assessment
The oil and grease data reported in this data set are considered usable for supporting project
objectives. The analytical completeness, defined as the ratio of the number of valid analytical
results (valid analytical results include values qualified as estimated) to the total number of
analytical results requested on samples submitted for this analysis, for the data set is 100%.
1.2 Holding Times
The holding time for oil and grease analysis of a preserved water sample is 28 days from sample
collection to analysis. The holding times were met for the sample analyses.
1.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). One method blank was reported for oil and grease by US
EPA method 1664A (batch WG2331265). Oil and grease were not detected in the method blank
at or above the MDL.
1.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). One sample specific MS/MSD pair was reported using sample MW-
2. The recovery and relative percent difference (RPD) results were within the laboratory specified
acceptance criteria, with the following exceptions.
The recovery of oil and grease in the MS of sample MW-2 was high and outside of the laboratory
specified acceptance criteria. Since oil and grease was not detected in sample MW-2 at a
concentration greater than the MDL, no qualifications were applied to the data.
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1.5 Laboratory Control Sample (LCS)
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS/LCS duplicate (LCSD) pair was reported for batch
WG2331265. The recovery and RPD results were within the laboratory specified acceptance
criteria.
1.6 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was not demonstrated between the field duplicate and the original sample MW-1.
Oil and grease were not detected in the original sample MW-1 at or above the MDL. Oil and grease
were detected at an estimated concentration greater than or equal to the MDL and less than the
reporting detection limit (RDL) in the field duplicate sample MW-25, resulting in a non-calculable
RPD between MW-1 and MW-25. Therefore, based on technical and professional judgement the
oil and grease data were J or UJ qualified as estimated or estimated non-detect.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
RPD Validation
Result (mg/L)
Validation
Qualifier*
Reason
Code**
MW-1 Oil & Grease
(Hexane Extr)
1.29 U NC 1.29 UJ 7
MW-25 Oil & Grease
(Hexane Extr)
1.68 J 1.68 J 7
mg/L-milligram per liter
U-Laboratory flag denoting a non-detect concentration less than the MDL
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
NC-Not calculable
* Validation qualifiers are defined in Attachment 1 at the end of this report
**Reason codes are defined in Attachment 2 at the end of this report
1.7 Sensitivity
The samples were evaluated to the MDLs. Elevated non-detect results were not reported.
1.8 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDLs and RDLs, however, only the RDLs were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.
2.0 Total Petroleum Hydrocarbons Low Fraction
The samples were analyzed for TPH low fraction by US EPA method 8015D/GRO.
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The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
 Overall Assessment
⊗ Holding Times
⊗ Method Blank
⊗ Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Surrogates
 Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review
2.1 Overall Assessment
2.1.1 Completeness
The TPH low fraction data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
2.1.2 Analysis Anomaly
The pH’s of samples MW-2, MW-10, and MW-9 did not meet the method criteria of pHs ≤ 2.
Therefore, the samples were considered unpreserved.
2.2 Holding Time
The holding time for TPH low fraction analysis of a preserved water sample is 14 days from sample
collection to analysis. The holding time for TPH low fraction analysis of an unpreserved water
sample is 7 days from sample collection to analysis. The holding times were met for the sample
analyses, with the following exception.
Sample MW-2 was analyzed outside the holding time of an unpreserved sample. Therefore, the
TPH low fraction concentration for sample MW-2 was J qualified as estimated.
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Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-2 TPH (GC/FID)
Low Fraction
0.139 B J3 0.139 J 2
mg/L-milligram per liter
B-Laboratory flag denoting the target analyte was detected in the method blank
J3-Laboratory flag denoting the associated batch QC was outside of the established quality control range for precision
2.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). One method blank was reported for TPH low fraction by
US EPA method 8015D/GRO (batch WG2329885).
TPH low fraction (0.0744 mg/L) was detected in the method blank at an estimated concentration
greater than or equal to the MDL and less than the RDL.
Therefore, based on technical and professional judgement, the TPH low fraction data with
estimated recoveries greater than or equal to the MDL and less than the RDL were U qualified as
non-detect and reported at the RDL. In addition, the TPH low fraction concentrations greater the
RDL and less than five times the method blank concentration were J+ qualified as estimated with
high bias. The TPH low fraction data with concentrations greater than five times the method blank
concentration were not qualified. Since the TPH low fraction concentration for sample MW-2 was
also qualified for holding time exceedance and MS/MSD RPD outside criteria, the final
qualification was J qualified as estimated.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-1 TPH (GC/FID)
Low Fraction
0.0502 B J 0.1 U 3
MW-25 TPH (GC/FID)
Low Fraction
0.0556 B J 0.1 U 3
MW-2 TPH (GC/FID)
Low Fraction
0.139 B J3 0.139 J 3
MW-4 TPH (GC/FID)
Low Fraction
0.254 B 0.254 J+ 3
MW-3 TPH (GC/FID)
Low Fraction
0.089 B J 0.1 U 3
MW-10 TPH (GC/FID)
Low Fraction
0.0522 B J 0.1 U 3
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Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-9 TPH (GC/FID)
Low Fraction
0.0508 B J 0.1 U 3
mg/L-milligram per liter
B-Laboratory flag denoting the target analyte was detected in the method blank
J-Laboratory flag denoting an estimated concentration greater than or equal to the MDL and less than the RDL
2.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). One sample specific MS/MSD pair was reported using sample MW-
2. The recovery and RPD results were within the laboratory specified acceptance criteria, with the
following exceptions.
The RPD of TPH low fraction between the MS and MSD of sample MW-2 was high and outside
of the laboratory specified acceptance criteria. Therefore, the detected TPH low fraction data of
sample MW-2 was J qualified as estimated.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-2 TPH (GC/FID)
Low Fraction
0.139 B J3 0.139 J 4
mg/L-milligram per liter
B-Laboratory flag denoting the target analyte was detected in the method blank
J3-Laboratory flag denoting the associated batch QC was outside of the established quality control range for precision
2.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS was reported. The recovery result was within the laboratory
specified acceptance criteria.
2.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
2.7 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample MW-1.
2.8 Sensitivity
The samples were evaluated to the MDLs. Elevated non-detect results were not reported.
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2.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDLs and RDLs, however, only the RDLs were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.
3.0 VOLATILE ORGANIC COMPOUNDS
The samples were analyzed for VOCs by US EPA method 8260B.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
⊗ Overall Assessment
⊗ Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
 Surrogates
 Trip Blank
 Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review
3.1 Overall Assessment
3.1.1 Completeness
The VOCs data reported in this sample set are considered usable for supporting project objectives,
with the following exceptions.
The non-detect VOC result for sample MW-10 were R qualified as rejected due to holding time
exceedance.
Therefore, the analytical completeness defined as the ratio of the number of valid analytical results
(valid analytical results include values qualified as estimated) to the total number of analytical
results requested on samples submitted for analysis, for the sample set is 91.0%.
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3.1.2 Analysis Anomaly
The pH of sample MW-10 did not meet the method criteria of pHs ≤ 2. Therefore, the sample was
considered unpreserved.
3.2 Holding Times
The holding times for the VOCs analysis of preserved water samples is 14 days from sample
collection to analysis. The holding times for the VOCs analysis of unpreserved water samples is 7
days from sample collection to analysis. The holding times were met for the sample analyses, with
the following exception.
Sample MW-10 was analyzed outside the holding time of an unpreserved sample. Therefore, the
non-detect VOC results were R qualified as rejected and the cis-1,2-Dichloroethene concentration
was J qualified as estimated for sample MW-10.
Sample Analyte Laboratory
Result
(mg/L)
Laboratory
Flag
Validation
Result
(mg/L)
Validation
Qualifier
Reason
Code
MW-10 Acetone 0.0113 U 0.0113 R 2
MW-10 Acrolein 0.00254 U J4 0.00254 R 2
MW-10 Acrylonitrile 0.000671 U 0.000671 R 2
MW-10 Benzene 0.0000941 U 0.0000941 R 2
MW-10 Bromobenzene 0.000118 U 0.000118 R 2
MW-10 Bromodichloromethane 0.000136 U 0.000136 R 2
MW-10 Bromoform 0.000129 U 0.000129 R 2
MW-10 Bromomethane 0.000605 U 0.000605 R 2
MW-10 N-Butylbenzene 0.000157 U 0.000157 R 2
MW-10 Sec-Butylbenzene 0.000125 U 0.000125 R 2
MW-10 Tert-Butylbenzene 0.000127 U 0.000127 R 2
MW-10 Carbon Tetrachloride 0.000128 U 0.000128 R 2
MW-10 Chlorobenzene 0.000116 U 0.000116 R 2
MW-10 Chlorodibromomethane 0.00014 U 0.00014 R 2
MW-10 Chloroethane 0.000192 U 0.000192 R 2
MW-10 Chloroform 0.000111 U 0.000111 R 2
MW-10 Chloromethane 0.00096 U 0.00096 R 2
MW-10 2-Chlorotoluene 0.000106 U 0.000106 R 2
MW-10 4-Chlorotoluene 0.000114 U 0.000114 R 2
MW-10 1,2-Dibromo-3-Chloropropane 0.000276 U 0.000276 R 2
MW-10 1,2-Dibromoethane 0.000126 U 0.000126 R 2
MW-10 Dibromomethane 0.000122 U 0.000122 R 2
MW-10 1,2-Dichlorobenzene 0.000107 U 0.000107 R 2
MW-10 1,3-Dichlorobenzene 0.00011 U 0.00011 R 2
MW-10 1,4-Dichlorobenzene 0.00012 U 0.00012 R 2
MW-10 Dichlorodifluoromethane 0.000374 U 0.000374 R 2
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Sample Analyte Laboratory
Result
(mg/L)
Laboratory
Flag
Validation
Result
(mg/L)
Validation
Qualifier
Reason
Code
MW-10 1,1-Dichloroethane 0.0001 U 0.0001 R 2
MW-10 1,2-Dichloroethane 0.0000819 U 0.0000819 R 2
MW-10 1,1-Dichloroethene 0.000188 U 0.000188 R 2
MW-10 Cis-1,2-Dichloroethene 0.000166 J 0.000166 J 2
MW-10 Trans-1,2-Dichloroethene 0.000149 U 0.000149 R 2
MW-10 1,2-Dichloropropane 0.000149 U 0.000149 R 2
MW-10 1,1-Dichloropropene 0.000142 U 0.000142 R 2
MW-10 1,3-Dichloropropane 0.00011 U 0.00011 R 2
MW-10 Cis-1,3-Dichloropropene 0.000111 U 0.000111 R 2
MW-10 Trans-1,3-Dichloropropene 0.000118 U 0.000118 R 2
MW-10 2,2-Dichloropropane 0.000161 U 0.000161 R 2
MW-10 Di-Isopropyl Ether 0.000105 U 0.000105 R 2
MW-10 Ethylbenzene 0.000137 U 0.000137 R 2
MW-10 Hexachloro-1,3-Butadiene 0.000337 U 0.000337 R 2
MW-10 Isopropylbenzene 0.000105 U 0.000105 R 2
MW-10 P-Isopropyltoluene 0.00012 U 0.00012 R 2
MW-10 2-Butanone (MEK) 0.00119 U 0.00119 R 2
MW-10 Methylene Chloride 0.00043 U 0.00043 R 2
MW-10 4-Methyl-2-Pentanone (MIBK) 0.000478 U 0.000478 R 2
MW-10 Methyl Tert-Butyl Ether 0.000101 U 0.000101 R 2
MW-10 Naphthalene 0.001 U 0.001 R 2
MW-10 N-Propylbenzene 0.0000993 U 0.0000993 R 2
MW-10 Styrene 0.000118 U 0.000118 R 2
MW-10 1,1,1,2-Tetrachloroethane 0.000147 U 0.000147 R 2
MW-10 1,1,2,2-Tetrachloroethane 0.000133 U 0.000133 R 2
MW-10 1,1,2-Trichlorotrifluoroethane 0.00018 U 0.00018 R 2
MW-10 Tetrachloroethene 0.0003 U 0.0003 R 2
MW-10 Toluene 0.000278 U 0.000278 R 2
MW-10 1,2,3-Trichlorobenzene 0.00023 U 0.00023 R 2
MW-10 1,2,4-Trichlorobenzene 0.000481 U 0.000481 R 2
MW-10 1,1,1-Trichloroethane 0.000149 U 0.000149 R 2
MW-10 1,1,2-Trichloroethane 0.000158 U 0.000158 R 2
MW-10 Trichloroethene 0.00019 U 0.00019 R 2
MW-10 Trichlorofluoromethane 0.00016 U 0.00016 R 2
MW-10 1,2,3-Trichloropropane 0.000237 U 0.000237 R 2
MW-10 1,2,4-Trimethylbenzene 0.000322 U 0.000322 R 2
MW-10 1,2,3-Trimethylbenzene 0.000104 U 0.000104 R 2
MW-10 1,3,5-Trimethylbenzene 0.000104 U 0.000104 R 2
MW-10 Vinyl Chloride 0.000234 U 0.000234 R 2
MW-10 Xylenes, Total 0.000174 U 0.000174 R 2
mg/L-milligrams per liter
J-estimated concentration greater than the MDL and less than the RDL
U-not detected at or above the RDL
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3.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Three method blanks were reported (batches WG2330260,
WG2330346 and WG2332276). VOCs were not detected in the method blanks at or above the
MDL.
3.4 Matrix Spike/Matrix Spike Duplicate
One sample specific MS/MSD pair was reported using sample MW-2. The recovery and RPD
results were within the laboratory specified acceptance criteria, with the following exceptions.
Cis-1,2-dichloroethene was flagged ‘V’ by the laboratory indicating the concentration of cis-1,2-
dichloroethene in the original sample, MW-2, was greater than the spike concentration. Therefore,
based on technical and professional judgement, no qualifications were applied to the data.
The recoveries of acrolein, carbon tetrachloride, chloroethane, 1,2-dichloroethane, 1,1,2-
trichlorotrifluoroethane, and trichlorofluoromethane in the MS/MSD of sample MW-2 were high
and outside of the laboratory specified acceptance criteria. Since these analytes were not detected
in sample MW-2 at concentrations greater than or equal to the MDLs, no qualifications were
applied to the data.
The recovery of methylene chloride in the MSD of sample MW-2 was high and outside of the
laboratory specified acceptance criteria. Since methylene chloride was not detected in sample
MW-2 at concentrations greater than or equal to the MDL, no qualifications were applied to the
data.
Sample specific MS/MSDs were not reported for batches WG2330346 and WG2332276.
Accuracy and precision were assessed using an LCS/LCSD pair for batch WG2330346. Precision
was assessed using an LCS for batch WG2332276.
3.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS/LCSD pair and two LCSs were reported. The recovery and
RPD results were within the laboratory specified acceptance criteria, with the following
exceptions.
The recovery of acrolein in the LCS of batch WG2330260 was high and outside of the laboratory
specified acceptance criteria. Since acrolein was not detected in the associated samples at
concentrations greater than or equal to the MDL, no qualifications were applied to the data.
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The RPD of vinyl chloride between the LCS and LCSD of batch WG2330346 was high and outside
of the laboratory specified acceptance criteria. Since vinyl chloride was not detected in the
associated samples at concentrations greater than or equal to the MDL, no qualifications were
applied to the data.
3.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
3.7 Trip Blank
One trip blank, TRIP BLANK, accompanied the sample shipment. VOCs were not detected in the
trip blank at or above the MDLs.
3.8 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample MW-1.
3.9 Sensitivity
The samples were evaluated to the MDL. Elevated non-detect results were not reported.
3.10 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDLs and RDLs, however, only the RDLs were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.
4.0 Total Petroleum Hydrocarbons High Fraction
The samples were analyzed for TPH high fraction by US EPA methods 3511/8015 3510C.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the course of the validation review and should be considered to determine any
impact on data quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Matrix Spike/Matrix Spike Duplicate
 Laboratory Control Sample
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⊗ Surrogates
 Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

4.1 Overall Assessment
The TPH high fraction data reported in this sample set are considered usable for supporting project
objectives. The results are considered valid; the analytical completeness defined as the ratio of the
number of valid analytical results (valid analytical results include values qualified as estimated) to
the total number of analytical results requested on samples submitted for analysis, for the sample
set is 100%.
4.2 Holding Times
The holding times for the TPH high fraction analysis of a water sample are 7 days from sample
collection to sample extraction and 40 days from sample extraction to analysis. The holding times
were met for the sample analyses.
4.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). One method blank was reported (batch WG2332252).
TPH high fraction were not detected in the method blank at or above the MDL.
4.4 Matrix Spike/Matrix Spike Duplicate
MS/MSDs were analyzed at the proper frequency for the number and types of samples analyzed
(one per batch of 20 samples). One sample specific MS/MSD pair was reported using sample MW-
2. The recovery and RPD results were within the laboratory specified acceptance criteria.
4.5 Laboratory Control Sample
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). One LCS was reported. The recovery results were within the laboratory
specified acceptance criteria.
4.6 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria, with the
following exceptions.
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O-Terphenyl recovered low and outside of the laboratory specified acceptance criteria in the LCS
of batch WG2332252. However, since the spike recovery was within the laboratory specified
acceptance criteria, and due to technical and professional judgement, no qualifications were
applied to the data.
O-Terphenyl recovered low and outside of the laboratory specified acceptance criteria in sample
MW-9. Therefore, based on technical and professional judgement, the detected TPH high fraction
data of sample MW-9 was J- qualified as estimated with low bias.
Sample
ID
Compound Laboratory
Result (mg/L)
Laboratory
Flag
Validation
Result (mg/L)
Validation
Qualifier
Reason
Code
MW-9 TPH (GC/FID)
High Fraction
0.164 NA 0.164 J- 6
mg/L-milligram per liter
NA-Not applicable
4.7 Field Duplicate
One field duplicate was collected with the sample set, MW-25. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample MW-1.
4.8 Sensitivity
The samples were evaluated to the MDL. Elevated non-detect results were not reported.
4.9 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. It was noted
the laboratory reported included both the MDL and RDL, however, only the RDL were included
in the EDD. No other discrepancies were identified between the level II report and the EDD.

* * * * *
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ATTACHMENT 1
DATA VALIDATION QUALIFIER DEFINITIONS
AND INTERPRETATION KEY
Assigned by Geosyntec’s Data Validation Team

DATA QUALIFIER DEFINITIONS
U The analyte was analyzed for, but was not detected above the reported sample quantitation
limit.
J The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
J+ The analyte was positively identified; however, the associated numerical value is likely to be
higher than the concentration of the analyte in the sample due to positive bias of associated
QC or calibration data or attributable to matrix interference.
J- The analyte was positively identified; however, the associated numerical value is likely to be
lower than the concentration of the analyte in the sample due to negative bias of associated
QC or calibration data or attributable to matrix interference.
UJ The analyte was not detected above the reported sample quantitation limit. However, the
reported quantitation limit is approximate and may or may not represent the actual limit of
quantitation necessary to accurately and precisely measure the analyte in the sample.
R The sample results are rejected due to serious deficiencies in the ability to analyze the sample
and meet quality control criteria. The presence or absence of the analyte cannot be verified.

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ATTACHMENT 2
DATA VALIDATION REASON CODES
Assigned by Geosyntec’s Data Validation Team

Valid Value Description
1 Preservation requirement not met
2 Extraction or analysis holding time exceeded
3 Blank contamination (i.e., method, trip, equipment, etc.)
4 Matrix spike/matrix spike duplicate recovery or RPD outside limits
5 LCS recovery outside limits or RPD outside limits (LCS/LCSD)
6 Surrogate recovery outside limits
7 Field Duplicate RPD exceeded
8 Serial dilution percent difference exceeded
9 Calibration criteria not met
10 Calibration range exceeded
11 Internal standard or isotope dilution standard criteria not met
12 Lab duplicates RPD exceeded
13 Other
14 Lab flag removed
LCS - Laboratory Control Sample
LCSD - Laboratory Control Sample duplicate
RPD - Relative percent difference

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DVR L1784259 R1.docx Final Review: K Henderson 11/26/2024
Memorandum
Date: 26 November 2024
To: Brian Smith
From: Chase Harris
CC: Kristoffer Henderson
Subject: Stage 2A Data Validation - Level II Data Deliverable – Pace
Analytical National Job ID L1784259
SITE: Paxton
INTRODUCTION
This report summarizes the findings of the Stage 2A data validation of two soil vapor samples and
one field duplicate, collected on 30 September 2024, as part of the Paxton Voluntary Cleanup
Program (VCP), site characterization activities (VCP Site #C-129).
Pace Analytical National Mount Juliet, Tennessee analyzed the samples for the following
analytical test:
• Volatile Organic Compounds (VOCs) by United States (US) Environmental Protection
Agency (EPA) Method TO-15.
EXECUTIVE SUMMARY
Overall, based on this Stage 2A data validation covering the quality control (QC) parameters listed
below and based on the information provided, the data as qualified are usable for supporting project
objectives. The qualified data should be used within the limitations of the qualifications. If there
are results with two or more different qualifications due to multiple QC failures, the final
qualification is reconciled in the electronic data deliverable (EDD) with qualifications.
The data were reviewed based on professional and technical judgment and the following
documents:
• Quality Assurance Project Plan, Paxton Development, 203 to 225 West Paxton Avenue,
Salt Lake City, Utah, Voluntary Cleanup Site #C-129, June 19, 2024 (herein referred to as
the QAPP);
• US EPA Contract Laboratory Program National Functional Guidelines for Organic
Superfund Methods Data Review, November 2020 (EPA 540-R-20-005);
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• The pertinent methods referenced by the data package.
The following samples were analyzed in the data set:
Laboratory ID Client ID
L1784259-01 SV-1
L1784259-02 SV-2
Laboratory ID Client ID
L1784259-03 SV-20
The samples were received within 0-6°C. No preservation issues were noted by the laboratory.
The laboratory reported results for the analytical method(s) requested for each sample on the COC.
The data validation report was revised on November 26, 2024, to make edits.
1.0 Volatile Organic Compounds
The samples were analyzed for VOCs by US EPA method TO-15.
The areas of data review are listed below. A leading check mark () indicates an area of review
in which the data were acceptable. A preceding crossed circle (⊗) signifies areas where issues
were raised during the validation review and should be considered to determine any impact on data
quality and usability.
 Overall Assessment
 Holding Times
 Method Blank
 Laboratory Control Sample
 Surrogates
⊗ Field Duplicate
 Sensitivity
 Electronic Data Deliverable Review

1.1 Overall Assessment
The VOC data reported in this data set are considered usable for supporting project objectives. The
analytical completeness, defined as the ratio of the number of valid analytical results (valid
analytical results include values qualified as estimated) to the total number of analytical results
requested on samples submitted for this analysis, for the data set is 100%.
1.2 Holding Times
The holding time for the VOCs analysis of a soil vapor sample is 30 days from sample collection
to analysis. The holding times were met for the sample analyses.
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1.3 Method Blank
Method blanks were analyzed at the proper frequency for the number and types of samples
analyzed (one per batch of 20 samples). Two method blanks were reported (batches WG2374030
and WG2376939). VOCs were not detected in the method blanks at or above the method detection
limits (MDLs), with the following exceptions.
Propene and TPH were detected in the method blank of batch WG2374030 at estimated
concentrations greater than or equal to the MDLs and less than the reported detection limits
(RDLs). However, since propene was not detected in the associated samples at concentrations
greater than or equal to the MDL, no qualifications were applied to the propene data. Since the
associated samples had detected concentrations of TPH greater than ten times the concentration of
TPH in the method blank, no qualifications were applied to the TPH data.
1.4 Laboratory Control Sample (LCS)
LCSs were analyzed at the proper frequency for the number and types of samples analyzed (one
per batch of 20 samples). Two LCS/LCS duplicate (LCSD) pairs were reported for batches
WG2374030 and WG2376939. The recovery and relative percent difference (RPD) results were
within the laboratory specified acceptance criteria.
1.5 Surrogates
The surrogate recoveries were within the laboratory specified acceptance criteria.
1.6 Field Duplicate
One field duplicate was collected with the sample set, SV-20. Acceptable precision (RPD<30%)
was demonstrated between the field duplicate and the original sample SV-2, with the following
exceptions.
The RPDs of acetone, 1,1-dichloroethane, cis-1,2-dichloroethene, trans-1,2-dichloroethene,
ethanol, methylene chloride, tetrachloroethene, trichloroethene, and 1,2,4-trimethylbenzene
between the field duplicate sample SV-20 and original sample SV-2 were high and outside of the
laboratory specified acceptance criteria. Therefore, the data of these analytes were J qualified as
estimated in the field duplicate sample SV-20 and original sample SV-2.
Carbon disulfide was not detected at or above the RDL in the field duplicate sample SV-20 but
was detected at a concentration greater than the RDL in the original sample SV-2, resulting in a
non-calculable RPD. Therefore, the carbon disulfide data of the field duplicate sample SV-20 and
original sample SV-2 were UJ or J qualified as estimated non-detect or estimated.
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N-Hexane was not detected at or above the RDL in the field duplicate sample SV-20 but was
detected at a concentration greater than the RDL in the original sample SV-2, resulting in a non-
calculable RPD. Therefore, the n-hexane data of the field duplicate sample SV-20 and original
sample SV-2 were UJ or J qualified as estimated non-detect or estimated.
Sample
ID
Compound Laboratory
Result
(µg/m3)
Laboratory
Flag
RPD Validation
Result
(µg/m3)
Validation
Qualifier
Reason
Code
SV-2 Acetone 13.5 NA 64 13.5 J 7
SV-20 Acetone 6.94 NA 6.94 J 7
SV-2 Carbon Disulfide 1.39 NA NC 1.39 J 7
SV-20 Carbon Disulfide <1.24 U <1.24 UJ 7
SV-2 1,1-Dichloroethane 1040 NA 35 1040 J 7
SV-20 1,1-Dichloroethane 1480 NA 1480 J 7
SV-2 Cis-1,2-Dichloroethene 3920 NA 36 3920 J 7
SV-20 Cis-1,2-Dichloroethene 5630 NA 5630 J 7
SV-2 Trans-1,2-Dichloroethene 227 NA 36 227 J 7
SV-20 Trans-1,2-Dichloroethene 325 NA 325 J 7
SV-2 Ethanol 9.14 NA 51 9.14 J 7
SV-20 Ethanol 5.45 NA 5.45 J 7
SV-2 N-Hexane 2.37 NA NC 2.37 J 7
SV-20 N-Hexane <2.22 U <2.22 UJ 7
SV-2 Methylene Chloride 2.7 NA 75 2.7 J 7
SV-20 Methylene Chloride 1.23 NA 1.23 J 7
SV-2 Tetrachloroethene 733 NA 37 733 J 7
SV-20 Tetrachloroethene 1070 NA 1070 J 7
SV-2 Trichloroethene 836 NA 40 836 J 7
SV-20 Trichloroethene 1250 NA 1250 J 7
SV-2 1,2,4-Trimethylbenzene 2.46 NA 30 2.46 J 7
SV-20 1,2,4-Trimethylbenzene 1.81 NA 1.81 J 7
µg/m3-microgram per cubic meter
NA-not applicable
NC-not calculable
U-Laboratory flag denoting a non-detect concentration less than the RDL
* Validation qualifiers are defined in Attachment 1 at the end of this report
**Reason codes are defined in Attachment 2 at the end of this report
1.7 Sensitivity
The samples were reported to the RDLs. Elevated non-detect results were not reported.
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1.8 Electronic Data Deliverable Review
The results and sample IDs in the EDD were reviewed against the information provided by the
associated level II report at a minimum of 20% as part of the data validation process. No
discrepancies were identified between the level II report and the EDD.

* * * * *
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ATTACHMENT 1
DATA VALIDATION QUALIFIER DEFINITIONS
AND INTERPRETATION KEY
Assigned by Geosyntec’s Data Validation Team

DATA QUALIFIER DEFINITIONS
U The analyte was analyzed for, but was not detected above the reported sample quantitation
limit.
J The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
J+ The analyte was positively identified; however, the associated numerical value is likely to be
higher than the concentration of the analyte in the sample due to positive bias of associated
QC or calibration data or attributable to matrix interference.
J- The analyte was positively identified; however, the associated numerical value is likely to be
lower than the concentration of the analyte in the sample due to negative bias of associated
QC or calibration data or attributable to matrix interference.
UJ The analyte was not detected above the reported sample quantitation limit. However, the
reported quantitation limit is approximate and may or may not represent the actual limit of
quantitation necessary to accurately and precisely measure the analyte in the sample.
R The sample results are rejected due to serious deficiencies in the ability to analyze the sample
and meet quality control criteria. The presence or absence of the analyte cannot be verified.

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ATTACHMENT 2
DATA VALIDATION REASON CODES
Assigned by Geosyntec’s Data Validation Team

Valid Value Description
1 Preservation requirement not met
2 Extraction or analysis holding time exceeded
3 Blank contamination (i.e., method, trip, equipment, etc.)
4 Matrix spike/matrix spike duplicate recovery or RPD outside limits
5 LCS recovery outside limits or RPD outside limits (LCS/LCSD)
6 Surrogate recovery outside limits
7 Field Duplicate RPD exceeded
8 Serial dilution percent difference exceeded
9 Calibration criteria not met
10 Calibration range exceeded
11 Internal standard or isotope dilution standard criteria not met
12 Lab duplicates RPD exceeded
13 Other
14 Lab flag removed
LCS - Laboratory Control Sample
LCSD - Laboratory Control Sample duplicate
RPD - Relative percent difference

Paxton SCR