DAQ-2025-000535

1

DAQC-082-25
Site ID 16168 (B4)

MEMORANDUM

TO: STACK TEST FILE – CRUSOE ENERGY SYSTEMS, INC. – Residue Booster
Facility – Duchesne County

THROUGH: Rik Ombach, Minor Source Oil and Gas Compliance Section Manager

FROM: Kyle Greenberg, Environmental Scientist

DATE: January 23, 2025

SUBJECT: Sources: Four (4) Waukesha 9394 GSI generator engines; SN’s: 1673772,
1673777, 1673786, 1673793
Contact: Phil Solomon: [phone]
Location: Duchesne County, UT
Test Contractor: Great Plains Analytical Services, Inc.
Permit/AO#: DAQE-AN161680001-23, dated November 7, 2023
Action Code: TR
Subject: Review of Stack Test Report dated December 19, 2024

On December 19, 2024, DAQ received a test report for the above listed units. Testing was performed
December 3-5, 2024, to demonstrate compliance with the emission limits found in Condition II.B.2 of
Approval Order DAQE-AN161680001-23 and 40 CFR Part 60 Subpart JJJJ. The calculated test results
are:

Source Test
Date
Test
Method Pollutant Tester Results DAQ Results Limits
Unit #:
1524;
SN:
1673772
Dec. 3,
2024
ASTM
D6348-03
NOx 0.121 g/hp-hr 0.120 g/hp-hr 0.15 g/hp-hr
CO 0.003 g/hp-hr 0.003 g/hp-hr 0.30 g/hp-hr
VOC 0.004 g/hp-hr 0.004 g/hp-hr 0.03 g/hp-hr
Unit #:
1525;
SN:
1673777
Dec. 5,
2024
ASTM
D6348-03
NOx 0.011 g/hp-hr 0.011 g/hp-hr 0.15 g/hp-hr
CO 0.029 g/hp-hr 0.028 g/hp-hr 0.30 g/hp-hr
VOC 0.006 g/hp-hr 0.006 g/hp-hr 0.03 g/hp-hr
Unit #:
1526;
SN:
1673786
Dec. 4,
2024
ASTM
D6348-03
NOx 0.038 g/hp-hr 0.038 g/hp-hr 0.15 g/hp-hr
CO 0.003 g/hp-hr 0.003 g/hp-hr 0.30 g/hp-hr
VOC 0.002 g/hp-hr 0.002 g/hp-hr 0.03 g/hp-hr
4 ' - ) - "
2

Source Test
Date
Test
Method Pollutant Tester Results DAQ Results Limits
Unit #:
1527;
SN:
1673793
Dec. 4,
2024
ASTM
D6348-03
NOx 0.038 g/hp-hr 0.038 g/hp-hr 0.15 g/hp-hr
CO 0.041 g/hp-hr 0.041 g/hp-hr 0.30 g/hp-hr
VOC 0.006 g/hp-hr 0.007 g/hp-hr 0.03 g/hp-hr

DEVIATIONS: None.

CONCLUSION: The stack test report appears to be acceptable.

RECOMMENDATION: The emissions from the four (4) Waukesha 9394 GSI generator
engines should be considered to be in compliance with the
emission limits found in Condition II.B.2 of Approval Order
DAQE-AN161680001-23 and 40 CFR Part 60 Subpart JJJJ
during the time of testing.

ATTACHMENTS: DAQ stack test review Excel Spreadsheets; Crusoe Energy
System stack test report
Emissions
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1524; SN: 1673772
Test Date: 12/3/2024
Run # 1 2 3 Average
Start Time 11:12 12:59 14:21
Stop Time 12:12 13:59 15:21
Sample Duration (minutes) 60 60 60
BHP Engine Load - Actual (bhp) 2125 2200 2225 2183
DS Stack Diameter (inches) 20.0 20.0 20.0 20.0
PAVG Average (Delta P)½ (" H2O)½0.7245 0.7189 0.7215 0.7216
CP Pitot Tube Constant (unitless) 0.99 0.99 0.99 0.99
TS Stack Temperature (°F) 917 922 930 923
Pbar Barometric Pressure (mbar) 846 845 844 845
Pbar Barometric Pressure (" Hg) 24.98 24.95 24.92 24.95
Ps Stack Pressure ('' H2O)0.53 0.52 0.52 0.52
O2%vd O2 (%vd)0.8 0.3 1.0 0.7
CO2%vd CO2 (%vd)9.4 9.4 9.4 9.4
N2%vd N2 (%vd)89.8 90.3 89.6 89.9
dry NOX (ppmvd)23.9 30.5 27.6 27.3
dry CO (ppmvd) 2.6 0.3 0.9 1.3
wet NMEOC (ppmvw as C3H8)0.7 1.1 0.8 0.8
Run # 1 2 3 Average
Bws Measured Moisture Content (%/100) 0.180 0.179 0.179 0.179
Bws Saturated Moisture Content (%/100) 701.582 717.406 741.370 720.119
Bws Actual Moisture Content (%/100) 0.180 0.179 0.179 0.179
MD Molecular Weight Dry (lb/lb-mole) 29.53 29.52 29.55 29.53
MA Molecular Weight Wet (lb/lb-mole) 27.46 27.47 27.48 27.47
VS Gas Velocity (ft/sec) 86.8 86.3 86.9 86.7
FACFM Gas Flow (acfm) 11364 11302 11378 11348
FDSCFM Gas Flow (dscfm) 2986 2960 2958 2968
FWSCFM Gas Flow (wscfm) 3643 3606 3605 3618
FKWSCFH Gas Flow (kwscfh) 219 216 216 217
FKWSCFM Gas Flow (kwscfm) 4 4 4 4
lb/hr Gas Flow (lb/hr) 15579 15422 15430 15477
Fo Fo (unitless)2.144 2.183 2.110 2.146
wet O2 (%vw)0.627 0.241 0.820 0.563
wet CO2 (%vw)7.700 7.754 7.741 7.732
wet NOX (ppmvw)19.577 25.052 22.653 22.427
15 NOX (ppmvd @ 15% O2)6.995 8.733 8.181 7.970
lb/hr NOX (lb/hr)0.510 0.646 0.584 0.580
g/bhp-hr NOX (g/bhp-hr)0.109 0.133 0.119 0.120 0.15
wet CO (ppmvw) 2.148 0.210 0.774 1.044
15 CO (ppmvd @ 15% O2)0.767 0.073 0.280 0.373
lb/hr CO (lb/hr) 0.034 0.003 0.012 0.017
g/bhp-hr CO (g/bhp-hr) 0.007 0.001 0.002 0.003 0.30
dry NMEOC (ppmvd as C3H8)0.794 1.334 0.916 1.015
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.233 0.382 0.272 0.295
lb/hr NMEOC (lb/hr as C3H8)0.016 0.027 0.019 0.021
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.003 0.006 0.004 0.004 0.03
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1524; SN: 1673772
Test Date: 12/3/2024
O2
21.1
10.62
0.0
10.7
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.7
%
0.00
10.62
21.05
0.0
10.7
20.9
0.0
0.1
0.1
0.0
0.00%
0.19%
0.57%
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
4
Difference
1
4
Response
1
2
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
Page 2 of 5
Run 1
Crusoe Energy System Inc. Run 1
Residue Booster Facility
Duchesne County, Utah Start Time 11:12
Waukesha 9394 GSI; Unit #: 1524; SN: 1673772 Run Length 60
Test Date: 12/3/2024 Stop Time 12:12
O2
21.1
10.62
0.0
10.7
0.0
11.0
0.0%
1.4%
0.0%
1.6%
Corrected O2 %
0.76
Run Length
(Minutes) Uncorrected O2 %
60 0.78
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Page 3 of 5
Run 2
Crusoe Energy System Inc. Run 2
Residue Booster Facility
Duchesne County, Utah Start Time 12:59
Waukesha 9394 GSI; Unit #: 1524; SN: 1673772 Run Length 60
Test Date: 12/3/2024 Stop Time 13:59
O2
21.1
10.62
0.0
10.7
0.0
11.0
0.0%
1.4%
0.0%
1.6%
Corrected O2 %
0.29
Run Length
(Minutes) Uncorrected O2 %
60 0.30
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Page 4 of 5
Run 3
Crusoe Energy System Inc. Run 3
Residue Booster Facility
Duchesne County, Utah Start Time 14:21
Waukesha 9394 GSI; Unit #: 1524; SN: 1673772 Run Length 60
Test Date: 12/3/2024 Stop Time 15:21
O2
21.1
10.62
0.0
10.7
0.0
11.0
0.0%
1.4%
0.0%
1.6%
Corrected O2 %
1.00
Run Length
(Minutes) Uncorrected O2 %
60 1.02
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Page 5 of 5
Emissions
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1525; SN: 1673777
Test Date: 12/5/2024
Run # 1 2 3 Average
Start Time 7:45 9:03 10:17
Stop Time 8:45 10:03 11:17
Sample Duration (minutes) 60 60 60
BHP Engine Load - Actual (bhp) 2275 2275 2275 2275
DS Stack Diameter (inches) 20.0 20.0 20.0 20.0
PAVG Average (Delta P)½ (" H2O)½0.7569 0.7646 0.7594 0.7603
CP Pitot Tube Constant (unitless) 0.99 0.99 0.99 0.99
TS Stack Temperature (°F) 928 934 938 934
Pbar Barometric Pressure (mbar) 844 845 845 845
Pbar Barometric Pressure (" Hg) 24.93 24.95 24.95 24.94
Ps Stack Pressure ('' H2O)0.57 0.59 0.58 0.58
O2%vd O2 (%vd)0.3 0.5 0.5 0.4
CO2%vd CO2 (%vd)9.6 9.6 9.5 9.6
N2%vd N2 (%vd)90.2 89.9 90.0 90.0
dry NOX (ppmvd)1.5 2.7 3.2 2.5
dry CO (ppmvd) 11.6 10.8 9.3 10.6
wet NMEOC (ppmvw as C3H8)1.0 1.2 1.0 1.1
Run # 1 2 3 Average
Bws Measured Moisture Content (%/100) 0.182 0.183 0.182 0.183
Bws Saturated Moisture Content (%/100) 735.743 752.933 764.519 751.065
Bws Actual Moisture Content (%/100) 0.182 0.183 0.182 0.183
MD Molecular Weight Dry (lb/lb-mole) 29.54 29.55 29.54 29.55
MA Molecular Weight Wet (lb/lb-mole) 27.44 27.44 27.44 27.44
VS Gas Velocity (ft/sec) 91.2 92.3 91.8 91.7
FACFM Gas Flow (acfm) 11936 12077 12012 12009
FDSCFM Gas Flow (dscfm) 3097 3119 3097 3104
FWSCFM Gas Flow (wscfm) 3788 3820 3789 3799
FKWSCFH Gas Flow (kwscfh) 227 229 227 228
FKWSCFM Gas Flow (kwscfm) 4 4 4 4
lb/hr Gas Flow (lb/hr) 16188 16325 16194 16236
Fo Fo (unitless)2.162 2.125 2.141 2.143
wet O2 (%vw)0.206 0.443 0.420 0.357
wet CO2 (%vw)7.812 7.825 7.785 7.807
wet NOX (ppmvw)1.260 2.245 2.639 2.048
15 NOX (ppmvd @ 15% O2)0.440 0.796 0.934 0.723
lb/hr NOX (lb/hr)0.034 0.061 0.072 0.056
g/bhp-hr NOX (g/bhp-hr)0.007 0.012 0.014 0.011 0.15
wet CO (ppmvw) 9.468 8.803 7.636 8.635
15 CO (ppmvd @ 15% O2)3.307 3.123 2.703 3.044
lb/hr CO (lb/hr) 0.156 0.146 0.126 0.143
g/bhp-hr CO (g/bhp-hr) 0.031 0.029 0.025 0.028 0.30
dry NMEOC (ppmvd as C3H8)1.204 1.512 1.236 1.318
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.344 0.438 0.358 0.380
lb/hr NMEOC (lb/hr as C3H8)0.026 0.032 0.026 0.028
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.005 0.006 0.005 0.006 0.03
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1525; SN: 1673777
Test Date: 12/5/2024
O2
21.1
10.62
0.0
10.8
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.62
21.05
0.0
10.8
21.0
0.0
0.1
0.0
0.0
0.00%
0.33%
0.67%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy System Inc. Run 1
Residue Booster Facility
Duchesne County, Utah Start Time 7:45
Waukesha 9394 GSI; Unit #: 1525; SN: 1673777 Run Length 60
Test Date: 12/5/2024 Stop Time 8:45
O2
21.1
10.62
0.0
10.8
0.0
11.1
0.0%
1.5%
0.0%
1.2%
Corrected O2 %
0.25
Run Length
(Minutes) Uncorrected O2 %
60 0.26
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy System Inc. Run 2
Residue Booster Facility
Duchesne County, Utah Start Time 9:03
Waukesha 9394 GSI; Unit #: 1525; SN: 1673777 Run Length 60
Test Date: 12/5/2024 Stop Time 10:03
O2
21.1
10.62
0.0
10.8
0.0
11.1
0.0%
1.5%
0.0%
1.2%
Corrected O2 %
0.54
Run Length
(Minutes) Uncorrected O2 %
60 0.56
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy System Inc. Run 3
Residue Booster Facility
Duchesne County, Utah Start Time 10:17
Waukesha 9394 GSI; Unit #: 1525; SN: 1673777 Run Length 60
Test Date: 12/5/2024 Stop Time 11:17
O2
21.1
10.62
0.0
10.8
0.0
11.1
0.0%
1.5%
0.0%
1.2%
Corrected O2 %
0.51
Run Length
(Minutes) Uncorrected O2 %
60 0.53
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1526; SN: 1673786
Test Date: 12/4/2024
Run # 1 2 3 Average
Start Time 13:18 14:28 15:41
Stop Time 14:18 15:28 16:41
Sample Duration (minutes) 60 60 60
BHP Engine Load - Actual (bhp) 2400 2400 2400 2400
DS Stack Diameter (inches) 20.0 20.0 20.0 20.0
PAVG Average (Delta P)½ (" H2O)½0.7532 0.7557 0.7508 0.7532
CP Pitot Tube Constant (unitless) 0.99 0.99 0.99 0.99
TS Stack Temperature (°F) 935 936 930 934
Pbar Barometric Pressure (mbar) 844 843 844 844
Pbar Barometric Pressure (" Hg) 24.92 24.90 24.91 24.91
Ps Stack Pressure ('' H2O)0.57 0.57 0.56 0.57
O2%vd O2 (%vd)0.6 0.6 0.3 0.5
CO2%vd CO2 (%vd)9.4 9.2 9.2 9.3
N2%vd N2 (%vd)90.0 90.1 90.4 90.2
dry NOX (ppmvd)9.3 9.4 8.9 9.2
dry CO (ppmvd) 1.3 2.3 0.1 1.2
wet NMEOC (ppmvw as C3H8)0.3 0.5 0.3 0.3
Run # 1 2 3 Average
Bws Measured Moisture Content (%/100) 0.182 0.180 0.180 0.181
Bws Saturated Moisture Content (%/100) 756.546 759.588 741.875 752.670
Bws Actual Moisture Content (%/100) 0.182 0.180 0.180 0.181
MD Molecular Weight Dry (lb/lb-mole) 29.52 29.50 29.49 29.50
MA Molecular Weight Wet (lb/lb-mole) 27.43 27.44 27.43 27.43
VS Gas Velocity (ft/sec) 91.0 91.3 90.6 91.0
FACFM Gas Flow (acfm) 11911 11957 11855 11908
FDSCFM Gas Flow (dscfm) 3074 3091 3077 3081
FWSCFM Gas Flow (wscfm) 3761 3770 3755 3762
FKWSCFH Gas Flow (kwscfh) 226 226 225 226
FKWSCFM Gas Flow (kwscfm) 4 4 4 4
lb/hr Gas Flow (lb/hr) 16063 16109 16035 16069
Fo Fo (unitless)2.166 2.197 2.227 2.197
wet O2 (%vw)0.510 0.528 0.264 0.434
wet CO2 (%vw)7.656 7.565 7.577 7.599
wet NOX (ppmvw)7.641 7.719 7.298 7.553
15 NOX (ppmvd @ 15% O2)2.718 2.740 2.552 2.670
lb/hr NOX (lb/hr)0.206 0.208 0.196 0.203
g/bhp-hr NOX (g/bhp-hr)0.039 0.039 0.037 0.038 0.15
wet CO (ppmvw) 1.077 1.926 0.065 1.023
15 CO (ppmvd @ 15% O2)0.383 0.684 0.023 0.363
lb/hr CO (lb/hr) 0.018 0.032 0.001 0.017
g/bhp-hr CO (g/bhp-hr) 0.003 0.006 0.000 0.003 0.30
dry NMEOC (ppmvd as C3H8)0.329 0.568 0.350 0.416
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.096 0.165 0.100 0.120
lb/hr NMEOC (lb/hr as C3H8)0.007 0.012 0.007 0.009
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.001 0.002 0.001 0.002 0.03
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1526; SN: 1673786
Test Date: 12/4/2024
O2
21.1
10.62
0.0
10.9
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.62
21.05
0.0
10.8
21.0
0.0
0.2
0.0
0.0
0.00%
0.29%
0.90%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy System Inc. Run 1
Residue Booster Facility
Duchesne County, Utah Start Time 13:18
Waukesha 9394 GSI; Unit #: 1526; SN: 1673786 Run Length 60
Test Date: 12/4/2024 Stop Time 14:18
O2
21.1
10.62
0.0
10.9
0.0
10.9
0.0%
0.5%
0.0%
0.2%
Corrected O2 %
0.62
Run Length
(Minutes) Uncorrected O2 %
60 0.64
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy System Inc. Run 2
Residue Booster Facility
Duchesne County, Utah Start Time 14:28
Waukesha 9394 GSI; Unit #: 1526; SN: 1673786 Run Length 60
Test Date: 12/4/2024 Stop Time 15:28
O2
21.1
10.62
0.0
10.9
0.0
10.9
0.0%
0.5%
0.0%
0.2%
Corrected O2 %
0.64
Run Length
(Minutes) Uncorrected O2 %
60 0.66
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy System Inc. Run 3
Residue Booster Facility
Duchesne County, Utah Start Time 15:41
Waukesha 9394 GSI; Unit #: 1526; SN: 1673786 Run Length 60
Test Date: 12/4/2024 Stop Time 16:41
O2
21.1
10.62
0.0
10.9
0.0
10.9
0.0%
0.5%
0.0%
0.2%
Corrected O2 %
0.32
Run Length
(Minutes) Uncorrected O2 %
60 0.33
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
Emissions
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1527; SN: 1673793
Test Date: 12/4/2024
Run # 1 2 3 Average
Start Time 8:46 10:02 f11:12
Stop Time 9:46 11:02 #VALUE!
Sample Duration (minutes) 60 60 60
BHP Engine Load - Actual (bhp) 2125 2150 2125 2133
DS Stack Diameter (inches) 20.0 20.0 20.0 20.0
PAVG Average (Delta P)½ (" H2O)½0.7245 0.7253 0.7245 0.7248
CP Pitot Tube Constant (unitless) 0.99 0.99 0.99 0.99
TS Stack Temperature (°F) 924 919 927 924
Pbar Barometric Pressure (mbar) 845 846 845 845
Pbar Barometric Pressure (" Hg) 24.95 24.97 24.95 24.96
Ps Stack Pressure ('' H2O)0.53 0.53 0.53 0.53
O2%vd O2 (%vd)0.5 0.7 0.7 0.6
CO2%vd CO2 (%vd)8.6 8.6 8.6 8.6
N2%vd N2 (%vd)90.9 90.7 90.7 90.8
dry NOX (ppmvd)10.4 7.6 7.0 8.3
dry CO (ppmvd) 12.5 17.2 14.2 14.6
wet NMEOC (ppmvw as C3H8)1.7 1.4 0.9 1.3
Run # 1 2 3 Average
Bws Measured Moisture Content (%/100) 0.167 0.168 0.168 0.168
Bws Saturated Moisture Content (%/100) 722.286 707.943 731.875 720.701
Bws Actual Moisture Content (%/100) 0.167 0.168 0.168 0.168
MD Molecular Weight Dry (lb/lb-mole) 29.39 29.40 29.41 29.40
MA Molecular Weight Wet (lb/lb-mole) 27.49 27.50 27.49 27.49
VS Gas Velocity (ft/sec) 87.0 86.9 87.1 87.0
FACFM Gas Flow (acfm) 11393 11382 11405 11393
FDSCFM Gas Flow (dscfm) 3021 3030 3015 3022
FWSCFM Gas Flow (wscfm) 3630 3641 3626 3632
FKWSCFH Gas Flow (kwscfh) 218 218 218 218
FKWSCFM Gas Flow (kwscfm) 4 4 4 4
lb/hr Gas Flow (lb/hr) 15539 15591 15523 15551
Fo Fo (unitless)2.381 2.354 2.344 2.360
wet O2 (%vw)0.394 0.549 0.557 0.500
wet CO2 (%vw)7.144 7.160 7.180 7.161
wet NOX (ppmvw)8.645 6.347 5.792 6.928
15 NOX (ppmvd @ 15% O2)2.999 2.222 2.030 2.417
lb/hr NOX (lb/hr)0.225 0.165 0.150 0.180
g/bhp-hr NOX (g/bhp-hr)0.048 0.035 0.032 0.038 0.15
wet CO (ppmvw) 10.394 14.317 11.846 12.186
15 CO (ppmvd @ 15% O2)3.606 5.013 4.152 4.257
lb/hr CO (lb/hr) 0.164 0.227 0.187 0.193
g/bhp-hr CO (g/bhp-hr) 0.035 0.048 0.040 0.041 0.30
dry NMEOC (ppmvd as C3H8)2.072 1.667 1.124 1.621
15 NMEOC (ppmvd as C3H8 @ 15% O2)0.598 0.486 0.328 0.471
lb/hr NMEOC (lb/hr as C3H8)0.043 0.035 0.023 0.034
g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.009 0.007 0.005 0.007 0.03
Permit Limits
Field Reference Method Data
Reference Method Calculations
Page 1 of 5
Linearity
Crusoe Energy System Inc.
Residue Booster Facility
Duchesne County, Utah
Waukesha 9394 GSI; Unit #: 1527; SN: 1673793
Test Date: 12/4/2024
O2
21.1
10.62
0.0
10.9
Linearity Bias (Zero) 0.0
Linearity Bias (Span) 10.8
%
0.00
10.62
21.05
0.0
10.8
21.0
0.0
0.2
0.0
0.0
0.00%
0.29%
0.90%
Gas Concentration
1
2
3
Linearity Information
Gas
Span Gas Value/Range
Bias Gas Value
4
Difference
1
4
Response
1
2
Span Bias
Max Calibration Error
Bias Check (Zero)
Bias Check (Span)
2
3
4
Results
3
Zero Bias
Page 2 of 5
Run 1
Crusoe Energy System Inc. Run 1
Residue Booster Facility
Duchesne County, Utah Start Time 8:46
Waukesha 9394 GSI; Unit #: 1527; SN: 1673793 Run Length 60
Test Date: 12/4/2024 Stop Time 9:46
O2
21.1
10.62
0.0
10.9
0.0
10.7
0.0%
0.5%
0.0%
0.8%
Corrected O2 %
0.47
Run Length
(Minutes) Uncorrected O2 %
60 0.48
Zero%
Span%
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Results
Post Test Calibration
Calibration Information
Instrument Range
Span Gas Value
Gas
Calibration
Pretest Calibration
Zero%
Span%
Page 3 of 5
Run 2
Crusoe Energy System Inc. Run 2
Residue Booster Facility
Duchesne County, Utah Start Time 10:02
Waukesha 9394 GSI; Unit #: 1527; SN: 1673793 Run Length 60
Test Date: 12/4/2024 Stop Time 11:02
O2
21.1
10.62
0.0
10.9
0.0
10.7
0.0%
0.5%
0.0%
0.8%
Corrected O2 %
0.66
Run Length
(Minutes) Uncorrected O2 %
60 0.67
Gas
Instrument Range
Post Test Calibration
Zero%
Span Gas Value
Calibration
Pretest Calibration
Zero%
Calibration Information
Results
Absolute Bias (Zero)
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Span%
Span%
Page 4 of 5
Run 3
Crusoe Energy System Inc. Run 3
Residue Booster Facility
Duchesne County, Utah Start Time f11:12
Waukesha 9394 GSI; Unit #: 1527; SN: 1673793 Run Length 60
Test Date: 12/4/2024 Stop Time #VALUE!
O2
21.1
10.62
0.0
10.9
0.0
10.7
0.0%
0.5%
0.0%
0.8%
Corrected O2 %
0.67
Run Length
(Minutes) Uncorrected O2 %
60 0.68
Post Test Calibration
Instrument Range
Zero%
Results
Absolute Bias (Zero)
Span%
Span%
Zero%
Absolute Bias (Span)
Absolute Drift (Zero)
Absolute Drift (Span)
Calibration Information
Span Gas Value
Calibration
Pretest Calibration
Gas
Page 5 of 5
303 West 3rd Street ● Elk City, Oklahoma 73644 ● 580-225-0403

GAS Inc.
www.gasinc.us
December 19, 2024

Utah Department of Environmental Quality
State Office Building – Air Quality Division
195 North 1950 West
Salt Lake City, Utah 84116

RE: Crusoe Energy Systems, Inc.
40 CFR Part 60 Subpart JJJJ – Test Report SubmiVal

To Whom It May Concern,

Please find the enclosed test reports for 40 CFR Part 60, Subpart JJJJ on behalf of Crusoe Energy
Systems, Inc. Please see below for the informaYon perYnent to the tesYng. The tesYng took
place the week of December 2, 2024.

Facility Unit # Serial # Loca1on
Residue Booster Sta9on 1524 1673772 Duchesne County, Utah
Residue Booster Sta9on 1525 1673777 Duchesne County, Utah
Residue Booster Sta9on 1526 1673786 Duchesne County, Utah
Residue Booster Sta9on 1527 1673793 Duchesne County, Utah

Our tesYng protocol is included, for informaYon regarding our protocol or the performance test,
you can contact me by email at [e-mail] or by phone at 580-225-0403. For
informaYon regarding engine or locaYon informaYon, please contact Kaitlin Meszaros by email
at [e-mail] or by phone at (631)-245-0308.

Regards,

Macie Holsapple
Client Services Supervisor
GAS Inc.
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:11:12 AM 04:03 PM
Source:
Unit Number: 1524
Serial Number: 1673772
Engine Hours:4158
Permit #: #DAQE-AN161680001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Residue Booster Station
CO NOx NMNEHC
1.273 27.323 1.015
2.000 0.300 1.000 0.150 0.700 0.030
0.003 0.121 0.004
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results ppmvd
Results g/hp-hr
Permit g/hp-hr
PASS ALL
40 CFR Part 60 Subpart JJJJ
Performance Test Report
Test Type: Initial
Test Date: 12/3/2024
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS, Inc.
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Jason Wooly
3
Hunter Newton
Gas, Inc.
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
Gas, Inc.
Unit 1524 with a serial number of 1673772 which is a Waukesha 9394 GSI engine located at Residue
Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 12/3/2024 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2183 BHP and 1200 RPM which is 87.33% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1524 is authorized to
operate under permit #DAQE-AN161680001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Residue Booster StationLocation 1524Unit ID
Make Waukesha Site Elevation ft.5406
Model 9394 GSI Atmospheric Pressure psi.11.91
Serial Number 1673772 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2125 2200 2225 2183
1200 1200 1199 1200
Percent Load %
Intake Manifold Pressure (hg)
85.00%88.00%89.00%87.33%
60.00 60.00 58.00 59.33
Intake Manifold Temperature (F)116.00 116.00 115.00 115.67
Ambient Conditions
Ambient Temperature Dry (F)29.00 34.00 41.00 34.67
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
179341.43 177771.20 177670.80 178261.14
5078.34 5033.87 5031.03 5047.75
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %18.00%17.86%17.91%17.92%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.76%0.29%1.00%0.68%
Permitted Standards Results
5
Catalyst
0.0020.001
Run 1 Run 2 Run 3 3 Run Average Pass Permits
11:12 AM 12:59 PM 02:21 PM 12/3/2024
CO (g/hp-hr)0.007 0.0032.000 0.300 Pass
StateFederal
CO (ppmvw)2.148 0.211 0.774 1.044
CO (ppmvd)2.619 0.256 0.943 1.273
CO (mol wt) 28.01
CO (ppmvd) @15% O2 0.767 0.073 0.280 0.373 Fail
CO (ppbvd) @15% O2 767.152 73.360 279.511 373.341 Fail
NOx (g/hp-hr)0.109 0.133 0.119 0.1211.000 0.150 Pass
NOx (ppmvw)19.578 25.052 22.654 22.428
NOx (ppmvd)23.874 30.499 27.595 27.323
NOx (mol wt) 46.01
0.651 1.096 0.752 0.833NMNEHC (ppmvw)
0.794 1.334 0.916 1.015NMNEHC (ppmvd)
NOx (ppbvd) @15% O2 6993.856 8730.685 8180.921 7968.487 Fail
NOx (ppmvd) @15% O2 6.994 8.731 8.181 7.968 Fail
NMNEHC (mol wt) 44.10
232.557 381.959 271.566 295.361 FailNMNEHC (ppbvd) @15% O2
0.003 0.006 0.004 0.0040.700 0.030 PassNMNEHC (g/hp-hr)
0.233 0.382 0.272 0.295 FailNMNEHC (ppmvd) @15% O2
Gas, Inc.
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
0.00Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
2.15
0.00
19.49
0.06
0.09
0.06
19.58
0.41
0.65
0.15%
0.63%
0.00%
18.00%
NMNEHC
1.52 18.31 0.06 18.37 0.52 0.58%18.02%
43.68 30.05 0.40 30.45 22.48 0.17%16.48%
2.78 20.67 0.12 20.79 0.78 0.69%17.97%
0.00 0.00 0.00 0.00 0.66 0.25%0.01%
Avg. Wet
NO2NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.00 0.00 0.66 0.25%0.01%
0.20 24.09 0.00 24.09 0.90 0.11%17.93%
50.50 48.04 0.00 48.04 28.57 1.76%15.93%
0.22 26.02 0.00 26.02 1.29 0.37%17.79%
0.00 0.00 0.00 0.00 0.64 0.00%0.00%
Avg. Wet 0.21 25.05 0.00 25.05 1.10 0.24%17.86%
NO2NO
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 23.34 0.00 23.34 0.96 0.68%17.86%
50.23 36.03 0.00 36.03 27.10 0.14%16.06%
1.55 21.71 0.26 21.97 0.54 0.98%17.95%
0.00 0.00 0.00 0.00 0.81 0.15%0.03%
0.00 0.00 0.00 0.00 0.64 0.00%0.00%
Avg. Wet 0.77 22.53 0.13 22.65 0.75 0.83%17.91%
NO2NO
Gas, Inc.
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Stack diameter =
Table 6.1. Data used for volumetric flow rate (Method 2)
20 inches or:1.67 feet. or:2.18 Square Feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.51
Yes
20.00
10.00
16.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
ppmd
%d
%d
%d 18.00
29.53
0.53
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
9.39
0.64
2.15
846.00
0.04
24.99
25.03
917.25
1376.92
491.81
27.45
86.81
189.40
218695.72
179341.43
Run 2
17.86
29.52
0.52
9.44
0.24
0.21
844.98
0.04
24.96
25.00
922.38
1382.05
494.65
27.46
86.34
188.36
216425.96
177771.20
Run 3
17.91
29.54
0.52
9.43
0.84
0.77
844.00
0.04
24.93
24.97
930.19
1389.86
498.99
27.48
86.93
189.64
216420.97
177670.80
17.92
29.53
0.52
9.42
0.57
1.04
844.99
0.04
24.96
25.00
923.27
1382.94
495.15
27.46
86.69
189.14
217179.69
178260.73
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.55
Exhaust Temp F
917.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.53
0.54
0.54
919.00
918.00
916.00
0.53
0.52
0.50
915.00
919.00
917.00
0.51
0.52
0.53
916.00
917.00
918.00
0.55 915.00
0.54
0.51
0.52
916.00
917.00
919.00
0.50
0.51
0.53
918.00
919.00
917.25
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.50
Exhaust Temp F
930.00
0.50
0.53
0.52
933.00
927.00
928.00
0.52
0.54
0.55
932.00
931.00
930.00
0.53
0.52
0.50
927.00
933.00
928.00
0.51 933.00
0.53
0.52
0.53
931.00
932.00
933.00
0.52
0.51
927.00
928.00
930.190.52
Run 2
Δpstd (in) H2O
0.53
Exhaust Temp F
922.00
0.50
0.52
0.51
921.00
920.00
926.00
0.53
0.53
0.52
923.00
922.00
926.00
0.51
0.50
0.52
924.00
920.00
921.00
0.50 920.00
0.51
0.55
0.51
919.00
925.00
924.00
0.52
0.51
923.00
922.00
0.52 922.38
Pass
Strat Check
31.373Check 1
31.353Check 2
31.333Check 3
MethaneGas Used
Pass/Fail
7
Gas, Inc.
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(.094)+.32(.008)+.28(.898+0) = 29.527 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.527(1 -.17995)+.18.0(.17995) = 27.453 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.53*√(1376.92/(25.03*27.453)) = 86.82 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.18)86.815*2.182((528*25.03)/ (1376.92*29.92)) = 179341.43 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 179341.428/35.315 = 5078.336 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 2.619*(20.9-15)/(20.9-.8%)) = .769 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(2.619*(1.164*10^-3)*5078.336*(Run Time/60))/2125 = .007 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .007*1/453.6*2125 = .034 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .034*4.38 = .149 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
2.62 = 2.1475*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
Gas, Inc.
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.71%
20.93%
10.67%
11.01%
10.62%
10.62%
11.01%10.67%
10.71%
20.93%
10.62%
21.05%
10.62%
21.05%
10.62%21.05%
0.00%
10.62%
21.05%
0.09%
0.12%
0.43%
0.57%
10.62%
Span
Zero Offset 0.00%
21.05
0.00%
10.71%0.18%1.41%0.02%
0.78%
0.30%
1.02%
0.76%
0.29%
1.00%
9
Gas, Inc.
0.0 0.0 0.0
0.0 0.0 0.0
1053.0 1062.0 1056.0
1018.0 1027.0 1021.0
4.8 4.8 4.8
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Residue Booster Station
12/3/2024
5406
1524
Waukesha
Model
Serial Number
9394 GSI
1673772
Technician Hunter Newton
Run Start Times 11:12 AM 12:59 PM 02:21 PM 04:03 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1200.0 1199.0 1199.7
Engine Hours 4155 4156 4157 4158
Intake Manifold Pressure (psi)60.0 60.0 58.0 59.3
Intake Manifold Temp °F 116.0 116.0 115.0 115.7
Engine Load (BHP)2125.0 2200.0 2225.0 2183.3
Ambient Temp °F 29.0 34.0 41.0 34.7
Humidity %67.0 67.0 39.0 57.7
Dew Point °F 19.0 19.0 18.0 18.7
Waukesha
YesCatalyst (Yes or No)
AFR Manufacturer/Type Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1053.0
1018.0
4.8Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
Gas, Inc.
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.06
Average:NOx 0.06
Average:VOC 0.30
Average:Oxygen 0.09
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 98.09
Tolerance 2.00%
Difference between measured and expected 0.19%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.29
Average:Oxygen 0.04
Pre-test System Zero Time:
Mechanical Response Time 52 seconds
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 97.50
Tolerance 5.00%
Difference between measured and expected 0.79%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 251.92
Value:Spike Expected 252.40
System (Equilibration) Response Time Target (Spike)
54 secondsSystem Zero Response Time
45 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC506322 9/17/2027 99.95 10.62%
EB0020295 6/20/2032 98.28
EB0090574 11/27/2031 21.05%
Cylinder # ALM-063647 Expiration: 5-03-2032
Propane CO NO SF6
Bottle Value 252.40 501.70 237.50 10.20
Analyzer System Response 251.92 504.15 238.23 10.18
Percent Difference 0.19%0.49%0.31%0.17%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.089 4.990
Spike Direct
Propane 252.270
Mechanical
Response Time
SF6 10.189
CO 501.091
NO 238.064
Ethylene 97.502 52 seconds
Analyzer
Response
Propane 251.920
SF6 10.183
CO 504.146
NO 238.225
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.640
CO 502.416
NO 240.888
110 seconds
54 seconds
7.91%
9.98%
9.67%
105.08%
104.76%
104.04%
10.269
12
Gas, Inc.
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
Gas, Inc.
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
10
16
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
178260.73
H2O%d @ Sampling Point:17.92
CO2%d @ Sampling Point:9.42
Pressure @ Sampling Point (Pg "H2O):0.52
Temperature @ Sampling Point (Deg F):923.27
Gas, Inc.
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 98.28 98.09 4.99 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 98.089 4.990
Spike Direct
Propane 252.270
Mechanical
Response Time
SF6 10.189
CO 501.091
NO 238.064
Ethylene 97.502 52 seconds
Analyzer
Response
Propane 251.920
SF6 10.183
CO 504.146
NO 238.225
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.640
CO 502.416
NO 240.888
110 seconds
54 seconds
7.91%
9.98%
9.67%
105.08%
104.76%
104.04%
10.269
Gas, Inc.
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
252.400
10.200
501.700
237.500
252.270
10.189
501.091
238.064
0.05%
0.11%
0.12%
0.24%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
20.980
0.806
Dilution Factor
7.910%
Expected
19.965
% Recovery
105.080%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
1.017
Dilution Factor
9.981%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.985
Dilution Factor
9.667%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 25.392 24.407 104.040%
0.000165
0.000480
0.000430
0.000 26.389 25.190 104.760%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass3.63%
16
Gas, Inc.
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-15.1359889 Pass
Line Position Difference:Resolution Difference to Reference 3.63%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
98.28
95.94
2.44%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
Gas, Inc.
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Residue Booster Station; 1524; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
12/3/2024
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
12/3/2024
Hunter Newton
Gas, Inc.
Appendices
Gas, Inc.
Gas, Inc.
Spike (5 Gas)
Gas, Inc.
9% O2/NO2
Gas, Inc.
Ethylene Only
Gas, Inc.
BIP
Gas, Inc.
21% O2
Tri Probe Certification
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3/3/2022
Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS, Inc.
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
Gas, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Residue Booster Station
Unit Number:1524
Make:Waukesha
Location:9394 GSIModel:
1673772Serial Number:
RAW Result Data
Stability
12/3/2024 06:59 18.0180.0000.068 0.000 0.00030.582 1.286 3.436 0.0000.117167.959 19.690 0.0000.230 1.351 859.024.2712.666 0.438 18.02 0.01 180.0
Pre Test Baseline Direct
12/3/2024 07:07 0.0000.0000.011 0.000 0.0000.000 0.000 0.925 0.0000.0000.000 0.000 0.0000.000 0.023 859.00.050.000 0.000 0.00 0.18 181.0
12/3/2024 07:07 0.1770.000-0.007 0.000 0.4780.000 0.000 0.845 0.0000.0000.072 0.000 0.0000.000 0.000 859.00.400.594 0.000 0.18 0.00 180.0
12/3/2024 07:08 0.0000.000-0.010 0.000 0.3070.000 0.000 0.852 0.0000.0000.000 0.000 0.0000.019 0.000 859.00.440.664 0.000 0.00 0.10 180.0
CTS Direct
12/3/2024 07:11 0.0000.658-0.001 0.000 0.0000.000 0.000 0.261 0.0000.0000.000 98.020 0.0000.000 0.000 859.065.730.565 0.000 0.66 0.20 180.0
12/3/2024 07:12 0.0000.8670.001 0.000 0.0000.000 0.000 0.231 0.0000.0000.000 98.454 0.0000.000 0.000 859.066.020.577 0.000 0.87 0.06 180.0
12/3/2024 07:12 0.00013.978-0.000 0.000 0.0000.000 0.000 0.193 0.0000.0380.000 97.793 0.0000.000 0.000 860.065.610.623 0.000 13.98 0.20 180.0
High O2 Direct
12/3/2024 07:19 0.0000.000-0.011 0.000 0.0000.000 0.000 0.790 0.0000.0000.000 0.000 0.0000.051 0.000 854.00.390.583 0.000 0.00 21.00 180.0
12/3/2024 07:19 0.0000.000-0.013 0.000 0.0000.000 0.000 0.894 0.0000.0000.000 0.000 0.0000.000 0.000 854.00.380.575 0.000 0.00 20.87 180.0
12/3/2024 07:20 0.0000.000-0.012 0.000 0.0570.000 0.000 0.948 0.0000.3060.000 0.000 0.0000.000 0.000 853.00.510.766 0.000 0.00 20.92 180.0
NO2/Mid O2 Direct
12/3/2024 07:29 99.8820.000-0.014 0.000 0.0000.000 0.834 0.253 0.3490.0000.000 0.000 0.0000.000 0.000 846.00.000.000 0.000 99.88 10.73 180.0
12/3/2024 07:29 100.5710.000-0.013 0.000 0.0000.000 0.834 0.182 0.3350.0000.000 0.000 0.0000.000 0.000 846.00.000.000 0.000 100.57 10.73 180.0
12/3/2024 07:29 101.4710.000-0.013 0.000 0.0000.000 0.843 0.174 0.4250.0610.388 0.000 0.0000.000 0.000 846.00.000.000 0.000 101.47 10.67 180.0
Spike Direct
12/3/2024 07:36 3.688238.556-0.017 4.797 0.000502.084 2.210 1.430 1.5440.3490.000 1.507 253.0590.000 0.000 846.0254.490.646 10.196 242.24 3.08 181.0
12/3/2024 07:37 2.518237.853-0.017 4.790 0.000500.949 2.288 1.726 1.7150.3380.000 1.501 251.9860.000 0.000 846.0253.100.168 10.189 240.37 2.00 180.0
12/3/2024 07:37 2.654237.783-0.018 4.789 0.000500.241 2.339 1.516 1.3860.3460.000 1.463 251.7650.000 0.000 846.0253.040.444 10.182 240.44 1.87 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
12/3/2024 07:39 0.0000.0000.009 0.000 0.1810.000 0.000 1.495 0.0000.0050.000 0.000 0.0000.000 0.061 846.00.300.271 0.000 0.00 0.00 180.0
12/3/2024 07:40 0.0000.0000.005 0.000 0.2570.000 0.000 1.409 0.0000.0150.000 0.000 0.0000.000 0.037 846.00.310.352 0.000 0.00 0.13 180.0
12/3/2024 07:40 0.0000.0000.002 0.000 0.0250.000 0.000 1.347 0.0000.0000.000 0.000 0.0000.000 0.011 846.00.270.376 0.000 0.00 0.00 180.0
CTS System with Response Time
12/3/2024 07:43 0.0002.1370.010 0.000 0.0000.000 0.000 0.724 0.0000.0000.000 97.471 0.0000.000 0.011 846.065.330.482 0.000 2.14 0.18 180.0
12/3/2024 07:43 0.0002.0490.009 0.000 0.0000.000 0.000 0.670 0.0000.0030.000 97.522 0.0000.000 0.000 846.065.340.489 0.000 2.05 0.24 180.0
12/3/2024 07:44 0.0002.3160.007 0.000 0.1210.000 0.000 0.756 0.0000.0030.000 97.513 0.0000.000 0.000 846.065.290.420 0.000 2.32 0.18 180.0
NO2/Mid O2 System with Response Time
12/3/2024 07:47 97.0121.886-0.000 0.000 0.0000.000 0.902 1.170 0.0000.0020.000 0.000 0.0000.004 0.109 846.00.630.619 0.000 98.90 10.73 180.0
12/3/2024 07:47 97.8671.628-0.000 0.000 0.0000.000 0.883 1.188 0.0000.0000.000 0.000 0.0000.000 0.082 846.00.570.602 0.000 99.50 10.69 180.0
12/3/2024 07:48 98.2150.000-0.000 0.000 0.0000.000 0.882 1.191 0.0000.0020.000 0.000 0.0000.000 0.071 846.00.490.520 0.000 98.21 10.60 180.0
Spike System with Response Time
12/3/2024 07:51 0.887238.464-0.000 4.796 0.000504.903 2.317 1.590 6.0620.1021.203 1.442 252.3760.000 0.000 846.0253.350.022 10.193 239.35 0.02 180.0
12/3/2024 07:51 0.000238.170-0.000 4.782 0.000504.612 2.333 1.644 6.7170.1480.620 1.431 251.9060.005 0.000 846.0253.190.492 10.174 238.17 0.15 180.0
12/3/2024 07:51 0.000238.206-0.000 4.781 0.000503.474 2.369 1.754 6.9880.0591.040 1.412 251.6070.000 0.000 846.0252.810.396 10.183 238.21 0.02 180.0
12/3/2024 07:52 0.000238.061-0.000 4.775 0.000503.596 2.338 1.707 6.7220.0921.200 1.383 251.7900.088 0.000 846.0253.120.610 10.182 238.06 0.02 180.0
Baseline System with Response Time
12/3/2024 08:02 0.0000.000-0.000 0.000 0.0470.000 0.000 0.981 0.0000.0070.000 0.000 0.0000.000 0.000 846.00.370.561 0.000 0.00 0.19 180.0
12/3/2024 08:02 0.1350.000-0.000 0.000 0.2960.000 0.000 1.003 0.0000.0040.000 0.000 0.0000.000 0.000 846.00.400.601 0.000 0.14 0.14 180.0
12/3/2024 08:03 0.0530.000-0.000 0.000 0.2990.000 0.000 1.029 0.0000.0010.000 0.000 0.0000.000 0.000 846.00.470.698 0.000 0.05 0.14 180.0
Run 1 - A 30minute/60min
12/3/2024 11:13 0.73915.06718.036 9.367 30.6590.891 0.755 9.653 0.0000.0002.931 0.000 0.0000.538 0.044 846.00.710.929 0.000 15.81 0.02 180.0
12/3/2024 11:14 0.00015.36718.058 9.362 32.9374.299 0.576 11.217 0.0000.0002.981 0.000 0.0000.518 0.033 846.00.700.947 0.000 15.37 5.08 180.0
12/3/2024 11:15 0.00022.82318.034 9.375 37.75313.586 1.283 19.760 0.2020.0003.091 0.000 0.0000.583 0.028 846.00.620.841 0.000 22.82 6.82 180.0
12/3/2024 11:16 0.00025.65918.030 9.376 31.2976.995 1.125 16.701 0.0000.0002.963 0.000 0.0000.650 0.024 846.00.550.756 0.000 25.66 0.17 180.0
12/3/2024 11:17 0.00013.81118.017 9.347 27.5830.000 0.008 5.862 0.0000.0002.679 0.000 0.0000.631 0.000 846.00.360.542 0.000 13.81 0.13 180.0
12/3/2024 11:18 0.00023.45018.022 9.403 19.7930.000 0.000 4.256 0.0000.0001.987 0.000 0.0000.585 0.008 846.00.390.563 0.000 23.45 0.13 180.0
12/3/2024 11:19 1.06418.30918.035 9.364 14.3050.000 0.000 3.324 0.0000.0002.548 0.000 0.0000.567 0.000 846.00.390.582 0.000 19.37 1.30 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/3/2024 11:20 0.00012.97218.012 9.360 24.1498.205 0.000 4.538 0.0000.0002.898 0.000 0.0000.549 0.000 846.00.520.783 0.000 12.97 0.19 180.0
12/3/2024 11:21 0.00023.32418.004 9.380 11.6820.000 0.000 2.841 0.0000.0001.918 0.000 0.0000.674 0.001 846.00.410.617 0.000 23.32 0.17 180.0
12/3/2024 11:22 0.00016.75917.997 9.369 19.6480.562 0.000 3.513 0.0000.0002.265 0.000 0.0000.560 0.000 846.00.510.761 0.000 16.76 0.01 180.0
12/3/2024 11:23 0.00018.06717.984 9.379 26.5572.839 0.873 6.787 0.0000.0002.659 0.000 0.0000.582 0.024 846.00.530.722 0.000 18.07 0.16 180.0
12/3/2024 11:24 0.00017.25917.983 9.388 25.4510.000 0.576 4.641 0.0000.0002.529 0.000 0.0000.503 0.029 846.00.560.758 0.000 17.26 0.18 180.0
12/3/2024 11:25 0.00019.96418.034 9.370 13.7290.000 0.000 2.683 0.0000.0002.241 0.000 0.0000.495 0.000 846.00.450.680 0.000 19.96 0.14 180.0
12/3/2024 11:26 0.00013.63418.040 9.343 27.5200.000 0.443 4.593 0.0000.0004.174 0.000 0.0000.521 0.000 846.00.560.835 0.000 13.63 0.01 180.0
12/3/2024 11:27 0.00016.51718.013 9.383 28.4320.000 0.947 5.657 0.0000.0002.756 0.000 0.0000.455 0.007 846.00.520.760 0.000 16.52 0.16 180.0
12/3/2024 11:28 0.00019.14717.978 9.412 38.6624.209 1.708 16.118 0.0260.0002.864 0.000 0.0000.542 0.075 846.00.740.882 0.000 19.15 0.17 180.0
12/3/2024 11:29 0.00020.21017.982 9.346 33.5000.648 1.673 13.623 0.0000.0003.314 0.000 0.0000.556 0.028 846.00.580.782 0.000 20.21 0.17 180.0
12/3/2024 11:30 0.00015.40218.008 9.366 19.5980.000 0.589 5.338 0.0000.0002.959 0.000 0.0000.495 0.000 846.00.440.667 0.000 15.40 0.13 180.0
12/3/2024 11:31 0.00013.86618.046 9.376 18.4120.000 0.000 2.978 0.0000.0002.146 0.000 0.0000.504 0.000 846.00.510.765 0.000 13.87 0.14 180.0
12/3/2024 11:32 0.00020.09318.043 9.357 30.1600.116 1.424 9.129 0.0000.0003.210 0.000 0.0000.522 0.016 846.00.530.749 0.000 20.09 0.16 180.0
12/3/2024 11:33 0.00018.02318.034 9.365 30.3480.000 1.054 6.931 0.0000.0003.109 0.000 0.0000.526 0.020 846.00.500.698 0.000 18.02 0.14 180.0
12/3/2024 11:34 0.00017.63118.026 9.375 35.5100.000 1.453 7.521 0.0000.0003.100 0.000 0.0000.629 0.022 846.00.470.644 0.000 17.63 0.15 180.0
12/3/2024 11:35 0.00019.16218.002 9.354 33.3280.000 1.387 10.045 0.0000.0003.296 0.000 0.0000.572 0.031 846.00.550.734 0.000 19.16 0.02 180.0
12/3/2024 11:36 0.00015.87118.047 9.373 29.6040.000 0.412 4.788 0.0000.0002.755 0.000 0.0000.473 0.011 846.00.570.822 0.000 15.87 1.14 180.0
12/3/2024 11:37 0.00017.86018.029 9.349 37.0791.247 0.865 7.820 0.0920.0002.938 0.000 0.0000.524 0.053 846.00.720.921 0.000 17.86 0.02 180.0
12/3/2024 11:38 0.00028.02618.038 9.353 23.7181.918 0.866 6.802 0.0000.0002.798 0.000 0.0000.542 0.000 846.00.450.669 0.000 28.03 0.16 180.0
12/3/2024 11:39 0.00021.86818.028 9.352 27.3320.000 0.559 5.015 0.0000.0002.839 0.000 0.0000.649 0.006 846.00.470.692 0.000 21.87 0.02 180.0
12/3/2024 11:40 0.00017.74518.046 9.353 18.3980.000 0.000 3.312 0.0000.0002.506 0.000 0.0000.492 0.000 846.00.470.701 0.000 17.75 0.14 180.0
12/3/2024 11:41 0.00014.98818.022 9.333 30.6930.000 0.550 4.935 0.0000.0002.992 0.000 0.0000.577 0.009 846.00.480.687 0.000 14.99 0.17 180.0
12/3/2024 11:42 0.00016.36318.021 9.343 19.9490.000 0.584 6.107 0.0000.0002.861 0.000 0.0000.611 0.000 846.00.450.669 0.000 16.36 0.02 180.0
0.06018.30818.022 9.366 26.5931.517 0.657 7.216 0.0110.0002.810 0.000 0.0000.554 0.016 846.000.5240.739 0.000 18.368 0.581 180.0Avg.
Spike 1
12/3/2024 11:47 0.39530.05416.476 9.058 33.70343.677 1.772 4.182 0.7790.0002.511 0.000 20.9800.508 0.322 846.022.481.281 0.806 30.45 0.17 180.0
Run 1 - B 30minute/60min
12/3/2024 11:50 0.24625.34218.043 9.384 49.72711.554 3.345 27.322 0.6640.0002.219 0.000 0.0000.620 0.118 846.00.870.954 0.000 25.59 0.14 180.0
12/3/2024 11:51 0.70727.08618.066 9.383 36.3137.243 1.838 18.382 0.0000.0003.521 0.000 0.0000.656 0.081 846.00.730.855 0.000 27.79 0.18 180.0
12/3/2024 11:52 0.60917.35918.001 9.342 33.8904.191 1.211 12.901 0.0000.0003.316 0.000 0.0000.561 0.054 846.00.740.942 0.000 17.97 0.17 179.0
12/3/2024 11:53 0.73118.03818.054 9.396 21.6350.000 0.750 6.399 0.0000.0003.218 0.000 0.0000.574 0.038 846.00.580.756 0.000 18.77 0.13 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/3/2024 11:54 0.00016.79918.072 9.344 35.7790.356 0.534 7.254 0.0000.0003.372 0.000 0.0000.650 0.079 846.00.790.951 0.000 16.80 0.01 180.0
12/3/2024 11:56 0.74521.04518.036 9.366 30.8420.000 1.220 7.455 0.0000.0003.459 0.000 0.0000.628 0.055 846.00.720.912 0.000 21.79 0.02 180.0
12/3/2024 11:57 0.45720.53218.059 9.380 43.7027.481 1.766 18.557 0.1380.0003.467 0.000 0.0000.614 0.123 846.00.890.966 0.000 20.99 0.20 180.0
12/3/2024 11:58 0.00024.79918.033 9.371 40.56512.987 2.044 20.769 0.0160.0003.297 0.000 0.0000.684 0.110 846.00.870.981 0.000 24.80 5.53 180.0
12/3/2024 11:59 0.00022.21518.018 9.405 42.60913.556 2.130 21.799 0.0890.0003.230 0.000 0.0000.539 0.117 846.00.880.976 0.000 22.21 1.62 180.0
12/3/2024 12:00 0.00028.83317.993 9.407 25.2641.671 1.267 11.833 0.0000.0003.154 0.000 0.0000.553 0.033 846.00.610.810 0.000 28.83 0.20 180.0
12/3/2024 12:01 0.00016.05817.980 9.402 26.8180.707 0.524 5.858 0.0000.0003.207 0.000 0.0000.664 0.039 846.00.670.892 0.000 16.06 0.14 180.0
12/3/2024 12:02 0.00014.73117.948 9.426 22.9691.032 0.562 4.308 0.0000.0002.802 0.000 0.0000.600 0.012 846.00.520.744 0.000 14.73 0.02 180.0
12/3/2024 12:03 0.00023.45617.939 9.371 28.6170.000 1.659 8.148 0.0000.0003.210 0.000 0.0000.626 0.047 846.00.781.035 0.000 23.46 0.18 180.0
12/3/2024 12:04 0.00029.00517.961 9.390 19.2270.000 0.131 3.459 0.0000.0002.833 0.000 0.0000.567 0.016 846.00.630.896 0.000 29.00 0.02 180.0
12/3/2024 12:05 0.00018.61817.964 9.410 24.4160.000 0.189 3.819 0.0000.0003.267 0.000 0.0000.582 0.017 846.00.680.973 0.000 18.62 5.77 180.0
12/3/2024 12:06 0.00020.24317.988 9.423 23.6730.000 0.279 3.590 0.0000.0003.213 0.000 0.0000.568 0.024 846.00.650.904 0.000 20.24 0.02 180.0
12/3/2024 12:07 0.00013.87718.030 9.411 25.7790.000 0.084 3.342 0.0000.0003.174 0.000 0.0000.632 0.047 846.00.761.000 0.000 13.88 0.17 180.0
12/3/2024 12:08 0.00014.64117.971 9.384 31.7600.000 0.000 3.584 0.0000.0003.376 0.000 0.0000.606 0.048 846.00.851.129 0.000 14.64 0.17 180.0
12/3/2024 12:09 0.00022.36517.982 9.395 39.9230.000 1.576 11.706 0.0000.0003.580 0.000 0.0000.746 0.104 846.00.981.153 0.000 22.36 0.02 180.0
12/3/2024 12:10 0.00025.49817.971 9.401 40.9589.354 1.985 20.717 0.0000.0003.501 0.000 0.0000.711 0.116 846.00.961.098 0.000 25.50 0.03 180.0
12/3/2024 12:11 0.00025.18517.909 9.440 45.15110.556 1.713 22.221 0.0820.0003.440 0.000 0.0000.629 0.167 846.01.071.105 0.000 25.18 0.18 180.0
12/3/2024 12:12 0.00027.90917.872 9.422 25.0840.000 1.401 9.051 0.0000.0003.642 0.000 0.0000.594 0.051 846.00.831.098 0.000 27.91 0.18 180.0
12/3/2024 12:13 0.00030.92517.894 9.410 11.6430.000 0.000 2.959 0.0000.0003.038 0.000 0.0000.609 0.005 846.00.420.612 0.000 30.93 0.14 180.0
12/3/2024 12:14 0.00015.07817.926 9.477 25.5550.000 0.000 3.161 0.0000.0003.260 0.000 0.0000.532 0.036 846.00.771.044 0.000 15.08 0.16 180.0
12/3/2024 12:15 0.00015.62217.887 9.417 14.5960.000 0.000 2.380 0.0000.0002.883 0.000 0.0000.535 0.036 846.00.751.021 0.000 15.62 0.02 180.0
12/3/2024 12:16 0.00013.43517.875 9.388 16.0890.000 0.000 1.961 0.0000.0003.367 0.000 0.0000.485 0.002 846.00.640.950 0.000 13.43 0.13 179.0
12/3/2024 12:17 0.00014.16917.868 9.452 28.5550.000 0.000 3.252 0.0000.0002.889 0.000 0.0000.676 0.058 846.00.871.136 0.000 14.17 0.16 180.0
12/3/2024 12:21 0.00023.03617.899 9.446 48.2852.652 1.724 18.246 0.1800.0003.550 0.000 0.0000.704 0.135 846.01.091.235 0.000 23.04 4.78 180.0
12/3/2024 12:23 0.00019.67517.838 9.470 24.3560.000 0.093 5.520 0.0000.0003.354 0.000 0.0000.581 0.059 846.00.861.117 0.000 19.68 0.22 180.0
12/3/2024 12:29 0.00014.57517.976 9.426 27.4770.000 0.284 5.056 0.0000.0003.517 0.000 0.0000.739 0.077 846.00.871.072 0.000 14.58 0.02 180.0
0.11720.67217.968 9.405 30.3752.778 0.944 9.834 0.0390.0003.245 0.000 0.0000.616 0.063 846.000.7780.977 0.000 20.788 0.691 179.9Avg.
0.08819.49017.995 9.385 28.4842.148 0.800 8.525 0.0250.0003.028 0.000 0.0000.585 0.040 846.000.6510.858 0.000 19.578 0.636 180.0Run 1 Avg:
Baseline 1
12/3/2024 12:32 0.0000.0000.005 0.000 0.0000.000 0.000 1.549 0.0000.0080.000 0.000 0.0000.025 0.000 845.00.660.990 0.000 0.00 0.25 180.0
Run 2 - A 30minute/60min
12/3/2024 13:00 0.00042.69017.813 9.421 14.3230.000 0.974 4.453 0.0000.0003.204 0.000 0.0000.609 0.013 845.00.690.994 0.000 42.69 0.02 179.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/3/2024 13:01 0.00030.50417.883 9.481 10.4020.000 0.000 2.186 0.0000.0002.734 0.000 0.0000.585 0.002 845.00.580.867 0.000 30.50 0.17 180.0
12/3/2024 13:02 0.00017.37817.876 9.430 29.7420.000 0.520 6.614 0.0000.0003.743 0.000 0.0000.688 0.054 845.00.891.181 0.000 17.38 0.01 180.0
12/3/2024 13:03 0.00017.98617.918 9.467 28.8970.000 0.564 6.472 0.0000.0003.473 0.000 0.0000.667 0.055 845.00.871.139 0.000 17.99 0.02 180.0
12/3/2024 13:04 0.00026.40917.926 9.472 20.5590.000 0.000 2.832 0.0000.0002.985 0.000 0.0000.725 0.029 845.00.771.062 0.000 26.41 0.02 180.0
12/3/2024 13:05 0.00013.82117.909 9.456 20.1750.000 0.000 2.154 0.0000.0003.309 0.000 0.0000.571 0.035 845.00.771.043 0.000 13.82 0.01 180.0
12/3/2024 13:06 0.00031.82917.950 9.460 14.2410.000 0.255 2.011 0.0000.0003.372 0.000 0.0000.655 0.023 845.00.731.028 0.000 31.83 0.23 180.0
12/3/2024 13:07 0.00019.10117.932 9.426 28.6020.000 0.402 3.522 0.0000.0003.711 0.000 0.0000.712 0.033 845.00.710.972 0.000 19.10 0.13 180.0
12/3/2024 13:08 0.00016.77517.926 9.372 25.8040.000 0.000 2.442 0.0000.0003.809 0.000 0.0000.486 0.015 845.00.861.250 0.000 16.78 0.17 179.0
12/3/2024 13:09 0.00032.80417.976 9.421 15.3690.000 0.347 2.061 0.0000.0003.563 0.000 0.0000.642 0.026 845.00.640.885 0.000 32.80 0.16 180.0
12/3/2024 13:10 0.00027.76818.014 9.445 13.9420.000 0.000 1.800 0.0000.0002.752 0.000 0.0000.641 0.004 845.00.741.091 0.000 27.77 0.16 180.0
12/3/2024 13:11 0.00019.30618.015 9.394 37.7440.000 1.422 7.531 0.0000.0003.822 0.000 0.0000.743 0.089 845.01.031.282 0.000 19.31 0.14 180.0
12/3/2024 13:12 0.00020.46717.965 9.401 38.9790.000 1.382 9.963 0.0000.0003.664 0.000 0.0000.722 0.087 845.01.021.272 0.000 20.47 0.17 180.0
12/3/2024 13:13 0.00021.55317.958 9.405 35.3410.000 1.397 9.149 0.0000.0003.728 0.000 0.0000.641 0.080 845.01.041.318 0.000 21.55 0.03 180.0
12/3/2024 13:14 0.00018.13717.967 9.420 31.6170.000 0.662 6.910 0.0000.0003.394 0.000 0.0000.732 0.058 845.00.841.078 0.000 18.14 0.14 180.0
12/3/2024 13:15 0.00014.39117.976 9.390 27.9290.000 0.326 4.572 0.0000.0004.170 0.000 0.0000.660 0.056 845.00.931.220 0.000 14.39 0.15 180.0
12/3/2024 13:16 0.00014.80017.988 9.431 29.8320.000 0.194 3.912 0.0000.0003.532 0.000 0.0000.595 0.088 845.01.001.240 0.000 14.80 0.02 180.0
12/3/2024 13:17 0.00018.44817.959 9.438 39.2600.000 1.556 10.913 0.0000.0003.627 0.000 0.0000.711 0.120 845.01.111.297 0.000 18.45 0.16 180.0
12/3/2024 13:18 0.00016.99017.963 9.410 30.2360.000 0.845 6.593 0.0000.0003.724 0.000 0.0000.624 0.073 845.00.881.101 0.000 16.99 0.03 180.0
12/3/2024 13:20 0.00017.57517.925 9.444 24.3700.000 0.000 3.816 0.0000.0003.572 0.000 0.0000.597 0.075 845.00.981.249 0.000 17.58 0.15 180.0
12/3/2024 13:21 0.00016.39017.929 9.429 21.6120.000 0.000 2.939 0.0000.0003.217 0.000 0.0000.636 0.060 845.00.931.221 0.000 16.39 0.02 180.0
12/3/2024 13:22 0.00017.10917.947 9.395 30.3670.000 0.383 4.784 0.0000.0003.978 0.000 0.0000.699 0.069 845.00.921.165 0.000 17.11 0.15 180.0
12/3/2024 13:23 0.00018.06517.986 9.399 22.9730.000 0.000 3.173 0.0000.0003.751 0.000 0.0000.669 0.051 845.00.931.248 0.000 18.06 0.19 180.0
12/3/2024 13:24 0.00020.90417.960 9.416 41.3570.000 1.055 12.724 0.0000.0003.605 0.000 0.0000.765 0.145 845.01.041.118 0.000 20.90 0.16 180.0
12/3/2024 13:25 0.00018.57317.948 9.443 37.3390.000 1.195 10.155 0.0000.0003.615 0.000 0.0000.679 0.127 845.01.061.213 0.000 18.57 0.03 180.0
12/3/2024 13:26 0.00023.93117.890 9.421 36.9821.125 1.311 11.848 0.0000.0003.491 0.000 0.0000.571 0.112 845.01.161.403 0.000 23.93 0.15 180.0
12/3/2024 13:27 0.00033.24317.832 9.444 23.3230.000 0.538 6.031 0.0000.0003.211 0.000 0.0000.611 0.042 845.00.881.193 0.000 33.24 0.16 180.0
12/3/2024 13:28 0.00018.14617.841 9.485 29.3024.835 0.000 5.628 0.0000.0003.448 0.000 0.0000.612 0.079 845.01.051.337 0.000 18.15 0.13 180.0
12/3/2024 13:29 0.00078.57417.814 9.432 17.8620.000 1.763 5.807 0.0000.0003.331 0.000 0.0000.532 0.058 845.00.981.300 0.000 78.57 0.14 180.0
12/3/2024 13:30 0.00038.99817.836 9.447 20.9500.000 0.172 3.648 0.0000.0003.513 0.000 0.0000.604 0.052 845.00.961.277 0.000 39.00 0.15 180.0
0.00024.08917.927 9.430 26.6480.199 0.575 5.555 0.0000.0003.502 0.000 0.0000.646 0.060 845.000.9001.168 0.000 24.089 0.112 179.9Avg.
Spike 2
12/3/2024 13:38 0.00048.04315.928 9.061 28.72950.499 2.141 8.988 0.5810.0002.848 0.000 26.3890.436 0.340 845.028.572.256 1.017 48.04 1.76 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
12/3/2024 13:44 0.00016.42917.839 9.467 25.1090.000 0.253 3.958 0.0000.0003.722 0.000 0.0000.656 0.116 845.01.091.290 0.000 16.43 0.02 180.0
12/3/2024 13:45 0.00019.59317.866 9.426 17.9870.000 0.000 2.328 0.0000.0003.567 0.000 0.0000.591 0.070 845.01.031.340 0.000 19.59 0.14 180.0
12/3/2024 13:46 0.00026.44417.865 9.447 24.6360.000 0.000 2.762 0.0000.0003.551 0.000 0.0000.564 0.111 845.01.211.482 0.000 26.44 0.01 180.0
12/3/2024 13:47 0.00017.30617.856 9.443 28.4470.000 0.000 3.422 0.0000.0003.755 0.000 0.0000.510 0.103 845.01.171.446 0.000 17.31 0.17 180.0
12/3/2024 13:48 0.00024.47317.878 9.447 31.3730.000 0.000 4.791 0.0000.0003.849 0.000 0.0000.566 0.128 845.01.111.283 0.000 24.47 0.15 180.0
12/3/2024 13:49 0.00018.01917.862 9.478 18.8890.000 0.000 3.255 0.0000.0003.391 0.000 0.0000.509 0.077 845.01.151.489 0.000 18.02 0.14 180.0
12/3/2024 13:50 0.00025.64817.838 9.473 23.6930.000 0.000 2.710 0.0000.0003.539 0.000 0.0000.671 0.099 845.01.031.242 0.000 25.65 0.01 180.0
12/3/2024 13:51 0.00019.16617.866 9.431 21.2020.000 0.000 2.268 0.0000.0003.569 0.000 0.0000.612 0.077 845.01.091.408 0.000 19.17 0.15 180.0
12/3/2024 13:52 0.00019.11217.858 9.434 24.7320.000 0.000 3.616 0.0000.0003.918 0.000 0.0000.612 0.114 845.01.091.290 0.000 19.11 0.13 180.0
12/3/2024 13:53 0.00015.15317.855 9.475 26.1870.000 0.000 2.151 0.0000.0003.579 0.000 0.0000.615 0.102 845.01.081.319 0.000 15.15 0.14 180.0
12/3/2024 13:54 0.00036.67717.857 9.457 11.0170.000 0.000 1.917 0.0000.0003.471 0.000 0.0000.488 0.066 845.00.931.194 0.000 36.68 0.02 180.0
12/3/2024 13:55 0.00053.14217.867 9.428 9.5500.000 0.000 1.625 0.0000.0003.221 0.000 0.0000.610 0.085 845.00.941.151 0.000 53.14 0.15 180.0
12/3/2024 13:56 0.00017.76417.903 9.429 24.6760.000 0.000 2.656 0.0000.0003.832 0.000 0.0000.583 0.091 845.01.031.273 0.000 17.76 0.12 180.0
12/3/2024 13:57 0.00032.95817.922 9.419 45.0343.102 2.609 19.457 0.0000.0004.238 0.000 0.0000.640 0.209 845.01.301.325 0.000 32.96 5.48 181.0
12/3/2024 13:58 0.00019.08917.884 9.414 34.2640.000 1.376 9.293 0.0000.0004.272 0.000 0.0000.582 0.144 845.01.271.470 0.000 19.09 0.03 180.0
12/3/2024 13:59 0.00016.85417.912 9.446 22.9150.000 0.000 3.275 0.0000.0003.577 0.000 0.0000.514 0.085 845.00.971.204 0.000 16.85 0.15 180.0
12/3/2024 14:00 0.00018.93317.907 9.432 38.2490.000 1.308 9.964 0.0000.0004.039 0.000 0.0000.729 0.170 845.01.271.397 0.000 18.93 0.16 180.0
12/3/2024 14:02 0.00018.35017.879 9.458 39.8220.000 1.939 11.918 0.0000.0003.711 0.000 0.0000.751 0.159 845.01.321.508 0.000 18.35 0.20 180.0
12/3/2024 14:03 0.00020.73617.862 9.457 37.6310.000 1.308 12.099 0.0000.0003.779 0.000 0.0000.710 0.136 845.01.261.487 0.000 20.74 0.03 180.0
12/3/2024 14:04 0.00016.71417.822 9.475 43.8720.000 1.604 12.217 0.0000.0003.753 0.000 0.0000.731 0.166 845.01.251.372 0.000 16.71 0.75 180.0
12/3/2024 14:05 0.00036.57717.789 9.461 35.8770.000 1.851 14.911 0.0000.0003.491 0.000 0.0000.571 0.165 845.01.271.404 0.000 36.58 0.03 180.0
12/3/2024 14:07 0.00026.57117.788 9.488 18.6560.000 0.000 3.499 0.0000.0003.463 0.000 0.0000.595 0.099 845.01.041.267 0.000 26.57 0.17 180.0
12/3/2024 14:08 0.00032.78517.769 9.505 16.7130.000 0.494 3.234 0.0000.0003.019 0.000 0.0000.566 0.097 845.01.061.292 0.000 32.79 1.27 180.0
12/3/2024 14:09 0.00020.47117.754 9.486 31.3533.543 0.429 9.121 0.0000.0003.709 0.000 0.0000.653 0.151 845.01.231.393 0.000 20.47 0.15 180.0
12/3/2024 14:10 0.00050.95617.742 9.459 23.4720.000 2.675 7.918 0.0000.0003.454 0.000 0.0000.576 0.122 845.01.171.388 0.000 50.96 0.23 180.0
12/3/2024 14:11 0.00036.61617.754 9.480 15.1060.000 0.000 2.556 0.0000.0003.494 0.000 0.0000.558 0.078 845.01.051.346 0.000 36.62 0.54 180.0
12/3/2024 14:12 0.00037.85517.761 9.502 16.1870.000 0.000 2.171 0.0000.0003.168 0.000 0.0000.558 0.094 845.01.041.276 0.000 37.85 0.13 180.0
12/3/2024 14:13 0.00029.18917.791 9.467 25.7040.000 0.000 2.545 0.0000.0003.891 0.000 0.0000.696 0.125 845.01.121.309 0.000 29.19 0.13 180.0
12/3/2024 14:14 0.00019.05417.814 9.464 29.2550.000 0.064 3.604 0.0000.0004.187 0.000 0.0000.613 0.141 845.01.101.229 0.000 19.05 0.21 180.0
12/3/2024 14:15 0.00037.82516.462 8.953 14.1050.000 0.259 2.361 0.0000.0001.348 0.000 4.3830.586 0.467 844.06.101.172 0.110 37.83 0.18 180.0
0.00026.01517.794 9.440 25.8570.222 0.539 5.587 0.0000.0003.585 0.000 0.1460.607 0.128 844.971.2921.335 0.004 26.015 0.373 180.0Avg.
0.00025.05217.861 9.435 26.2520.210 0.557 5.571 0.0000.0003.543 0.000 0.0730.627 0.094 844.981.0961.252 0.002 25.052 0.243 180.0Run 2 Avg:
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
12/3/2024 14:18 0.0000.000-0.000 0.000 0.0000.000 0.000 1.296 0.0000.0010.000 0.000 0.0000.015 0.000 844.00.640.958 0.000 0.00 0.00 180.0
Run 3 - A 30minute/60min
12/3/2024 14:21 0.00014.81517.855 9.414 21.9340.000 0.000 2.471 0.0000.0003.700 0.000 0.0000.674 0.085 844.01.071.348 0.000 14.82 0.16 180.0
12/3/2024 14:22 0.00018.35117.887 9.425 23.7290.000 0.000 2.408 0.0000.0003.399 0.000 0.0000.558 0.121 844.01.161.378 0.000 18.35 0.18 180.0
12/3/2024 14:23 0.00019.38117.904 9.397 36.9810.000 0.669 6.194 0.0000.0003.911 0.000 0.0000.593 0.138 844.01.201.378 0.000 19.38 0.02 179.0
12/3/2024 14:24 0.00022.61017.903 9.481 45.6450.000 1.823 13.204 0.0000.0003.459 0.000 0.0000.565 0.184 844.01.341.458 0.000 22.61 2.26 180.0
12/3/2024 14:25 0.00021.17817.915 9.395 46.5970.000 1.981 15.499 0.0000.0004.254 0.000 0.0000.636 0.181 844.01.441.613 0.000 21.18 0.03 180.0
12/3/2024 14:26 0.00018.49817.855 9.382 40.3730.000 1.822 12.104 0.0000.0002.257 0.000 0.0000.701 0.121 844.01.181.415 0.000 18.50 2.11 179.0
12/3/2024 14:27 0.00020.50817.867 9.473 40.9550.000 1.471 11.833 0.0000.0003.560 0.000 0.0000.642 0.146 844.01.271.470 0.000 20.51 0.17 180.0
12/3/2024 14:28 0.00019.63217.845 9.424 45.3450.000 0.626 8.995 0.0000.0003.611 0.000 0.0000.748 0.179 844.01.151.188 0.000 19.63 0.03 180.0
12/3/2024 14:29 0.00017.40417.856 9.423 45.1430.000 1.345 14.889 0.0000.0003.955 0.000 0.0000.678 0.187 844.01.411.552 0.000 17.40 1.90 180.0
12/3/2024 14:30 0.00033.80117.781 9.469 31.8960.000 0.912 13.013 0.0000.0003.467 0.000 0.0000.689 0.122 844.01.101.282 0.000 33.80 0.21 180.0
12/3/2024 14:31 0.00019.19217.806 9.436 38.7070.000 0.301 11.559 0.0000.0003.715 0.000 0.0000.614 0.127 844.01.131.309 0.000 19.19 3.44 180.0
12/3/2024 14:32 0.00021.07117.745 9.430 32.3870.000 1.126 12.051 0.0000.0003.624 0.000 0.0000.666 0.081 844.01.121.442 0.000 21.07 0.18 179.0
12/3/2024 14:33 0.00036.39917.804 9.504 10.4770.000 0.000 3.005 0.0000.0002.711 0.000 0.0000.526 0.000 844.00.761.134 0.000 36.40 0.14 180.0
12/3/2024 14:34 0.00014.61217.798 9.464 16.6280.000 0.000 2.229 0.0000.0002.318 0.000 0.0000.571 0.015 844.00.931.346 0.000 14.61 0.14 180.0
12/3/2024 14:35 0.00024.31117.857 9.451 11.9890.000 0.000 1.926 0.0000.0002.946 0.000 0.0000.493 0.007 844.00.841.237 0.000 24.31 0.01 180.0
12/3/2024 14:36 0.00015.93817.914 9.425 31.5790.000 0.000 6.268 0.0000.0003.298 0.000 0.0000.585 0.052 844.01.031.388 0.000 15.94 2.13 181.0
12/3/2024 14:37 0.00021.14117.876 9.413 27.9980.000 0.569 7.732 0.0000.0003.668 0.000 0.0000.618 0.029 844.00.710.984 0.000 21.14 0.17 180.0
12/3/2024 14:38 0.00023.39817.872 9.436 15.9330.000 0.000 2.712 0.0000.0002.925 0.000 0.0000.533 0.000 844.00.941.413 0.000 23.40 0.18 180.0
12/3/2024 14:39 0.00016.10917.881 9.418 32.6360.000 0.060 5.276 0.0000.0003.435 0.000 0.0000.532 0.020 844.00.961.380 0.000 16.11 5.72 180.0
12/3/2024 14:40 0.00019.35217.876 9.446 37.7660.000 0.979 8.134 0.0000.0003.326 0.000 0.0000.660 0.045 844.00.961.310 0.000 19.35 0.15 180.0
12/3/2024 14:41 0.00016.70517.928 9.460 26.4140.000 0.181 5.481 0.0000.0003.300 0.000 0.0000.515 0.006 844.00.801.176 0.000 16.71 0.18 181.0
12/3/2024 14:42 0.00015.57817.880 9.413 17.8270.000 0.000 2.411 0.0000.0002.800 0.000 0.0000.505 0.000 844.00.771.150 0.000 15.58 0.16 180.0
12/3/2024 14:43 0.00017.28417.832 9.428 33.8490.000 0.516 5.628 0.0000.0003.254 0.000 0.0000.525 0.002 844.00.821.219 0.000 17.28 0.14 180.0
12/3/2024 14:44 0.00017.17617.910 9.420 28.6980.000 0.080 4.816 0.0000.0003.471 0.000 0.0000.440 0.010 844.00.721.057 0.000 17.18 0.02 180.0
12/3/2024 14:45 0.00015.06317.899 9.427 28.7220.000 0.185 4.062 0.0000.0003.405 0.000 0.0000.558 0.000 844.00.701.050 0.000 15.06 0.02 180.0
12/3/2024 14:46 0.00031.78117.893 9.408 25.5640.000 1.338 4.630 0.0000.0003.399 0.000 0.0000.617 0.000 844.00.671.007 0.000 31.78 0.18 180.0
12/3/2024 14:48 0.00025.49217.849 9.440 23.1050.000 0.000 3.497 0.0000.0002.703 0.000 0.0000.442 0.000 844.00.691.042 0.000 25.49 0.16 180.0
12/3/2024 14:49 0.00056.34617.834 9.465 17.2430.000 0.852 2.719 0.0000.0002.757 0.000 0.0000.440 0.000 844.00.721.083 0.000 56.35 0.14 180.0
12/3/2024 14:50 0.00055.39817.893 9.420 14.0590.000 0.684 2.011 0.0000.0002.841 0.000 0.0000.391 0.000 844.00.610.920 0.000 55.40 0.12 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/3/2024 14:51 0.00031.75917.880 9.487 12.7910.000 0.000 1.686 0.0000.0001.960 0.000 0.0000.445 0.000 844.00.600.893 0.000 31.76 0.13 180.0
0.00023.34317.863 9.436 28.7660.000 0.584 6.615 0.0000.0003.248 0.000 0.0000.572 0.062 844.000.9601.254 0.000 23.343 0.686 180.0Avg.
Spike 3
12/3/2024 14:56 0.00036.03016.056 9.057 17.20150.234 1.126 2.345 0.3670.0002.161 0.060 25.3920.276 0.273 844.027.101.677 0.985 36.03 0.14 180.0
Run 3 - B 30minute/60min
12/3/2024 14:59 0.00015.42617.963 9.394 28.3730.000 0.734 3.806 0.0000.0003.305 0.000 0.0000.502 0.000 844.00.630.946 0.000 15.43 0.14 180.0
12/3/2024 15:00 0.00015.44417.963 9.401 29.3910.000 0.545 3.713 0.0000.0003.010 0.000 0.0000.605 0.000 844.00.480.724 0.000 15.44 0.15 180.0
12/3/2024 15:01 0.87520.78317.947 9.389 18.6080.000 0.264 2.525 0.0000.0002.397 0.000 0.0000.517 0.000 844.00.540.817 0.000 21.66 0.16 180.0
12/3/2024 15:02 1.00116.42417.966 9.372 17.9130.000 0.075 1.936 0.0000.0002.459 0.000 0.0000.493 0.000 844.00.540.813 0.000 17.43 0.12 180.0
12/3/2024 15:03 1.17318.65017.978 9.396 20.8560.000 0.161 2.143 0.0000.0002.335 0.000 0.0000.557 0.000 844.00.470.703 0.000 19.82 0.01 180.0
12/3/2024 15:04 0.00015.25718.032 9.366 29.0820.000 0.364 2.756 0.0000.0002.647 0.000 0.0000.486 0.000 844.00.510.760 0.000 15.26 0.12 180.0
12/3/2024 15:05 0.00017.86618.101 9.361 38.4210.000 1.815 8.747 0.0000.0003.396 0.000 0.0000.495 0.003 844.00.530.791 0.000 17.87 0.18 181.0
12/3/2024 15:06 0.00018.02718.053 9.344 39.9084.136 1.910 13.315 0.0000.0003.202 0.000 0.0000.551 0.024 844.00.540.736 0.000 18.03 2.41 180.0
12/3/2024 15:07 0.00021.75317.984 9.414 36.2314.933 2.095 15.595 0.0000.0002.843 0.000 0.0000.412 0.008 844.00.470.681 0.000 21.75 0.03 180.0
12/3/2024 15:08 1.15215.21818.005 9.364 20.3750.000 0.000 3.318 0.0000.0002.625 0.000 0.0000.501 0.000 844.00.520.774 0.000 16.37 4.03 180.0
12/3/2024 15:09 0.00017.80317.990 9.359 37.0830.000 1.143 7.691 0.0000.0003.206 0.000 0.0000.498 0.000 844.00.570.855 0.000 17.80 0.01 180.0
12/3/2024 15:10 0.00019.06217.981 9.366 37.3970.000 1.597 8.421 0.0000.0003.113 0.000 0.0000.434 0.011 844.00.600.869 0.000 19.06 0.02 180.0
12/3/2024 15:11 0.00015.93217.984 9.377 34.8047.492 0.810 10.416 0.0000.0002.850 0.000 0.0000.515 0.000 844.00.530.793 0.000 15.93 0.16 180.0
12/3/2024 15:12 0.00021.00217.926 9.422 38.6296.704 1.788 12.920 0.0240.0003.065 0.000 0.0000.513 0.051 844.00.720.928 0.000 21.00 5.41 180.0
12/3/2024 15:13 0.00023.65217.934 9.397 32.2470.000 0.971 10.717 0.0000.0003.020 0.000 0.0000.470 0.000 844.00.530.789 0.000 23.65 0.80 180.0
12/3/2024 15:14 0.03615.24917.950 9.407 24.0450.000 0.742 6.199 0.0000.0002.913 0.000 0.0000.425 0.000 844.00.500.753 0.000 15.29 0.13 180.0
12/3/2024 15:15 0.00019.37717.986 9.469 33.0540.233 1.469 9.301 0.0000.0003.207 0.000 0.0000.600 0.022 844.00.530.727 0.000 19.38 0.02 181.0
12/3/2024 15:16 0.00017.07617.935 9.467 39.4538.346 1.617 13.548 0.1690.0003.214 0.000 0.0000.370 0.003 844.00.550.814 0.000 17.08 0.16 180.0
12/3/2024 15:17 0.00027.81217.857 9.468 34.4299.780 2.063 18.566 0.0000.0003.074 0.000 0.0000.490 0.026 844.00.600.820 0.000 27.81 0.15 180.0
12/3/2024 15:18 0.00015.14517.814 9.474 34.3414.724 1.236 11.321 0.0000.0002.970 0.000 0.0000.533 0.012 844.00.580.836 0.000 15.14 0.98 180.0
12/3/2024 15:19 0.00029.75117.814 9.501 28.2400.000 1.276 8.674 0.0000.0003.266 0.000 0.0000.462 0.025 844.00.550.750 0.000 29.75 0.02 180.0
12/3/2024 15:20 0.01929.44717.828 9.482 17.5730.000 0.294 2.853 0.0000.0002.448 0.000 0.0000.429 0.000 844.00.530.791 0.000 29.47 0.02 180.0
12/3/2024 15:21 0.00071.45117.842 9.461 11.9870.000 1.112 2.341 0.0000.0002.986 0.000 0.0000.351 0.000 844.00.520.772 0.000 71.45 0.01 180.0
12/3/2024 15:22 1.14021.64017.858 9.511 15.0010.000 0.109 1.992 0.0000.0002.192 0.000 0.0000.365 0.000 844.00.530.799 0.000 22.78 0.21 180.0
12/3/2024 15:23 1.16725.73417.936 9.444 20.7840.000 0.000 2.464 0.0000.0002.515 0.000 0.0000.454 0.000 844.00.490.737 0.000 26.90 2.26 180.0
12/3/2024 15:24 0.00021.10717.938 9.417 30.7820.100 1.257 7.051 0.0000.0003.231 0.000 0.0000.449 0.006 844.00.580.855 0.000 21.11 5.98 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/3/2024 15:25 0.00020.98917.981 9.460 25.0860.000 1.050 6.430 0.0000.0003.173 0.000 0.0000.447 0.000 844.00.530.799 0.000 20.99 0.16 181.0
12/3/2024 15:26 1.14118.47017.948 9.430 18.0520.000 0.000 2.587 0.0000.0002.620 0.000 0.0000.463 0.000 844.00.540.803 0.000 19.61 0.15 180.0
12/3/2024 15:28 0.00020.87517.979 9.422 24.1200.000 0.288 3.058 0.0000.0002.743 0.000 0.0000.542 0.000 844.00.520.779 0.000 20.88 0.01 180.0
12/3/2024 15:29 0.00024.79817.941 9.398 17.6570.000 0.000 2.620 0.0000.0002.047 0.000 0.0000.466 0.000 844.00.580.863 0.000 24.80 5.64 180.0
0.25721.70717.947 9.418 27.7971.548 0.893 6.901 0.0060.0002.869 0.000 0.0000.480 0.006 844.000.5440.796 0.000 21.965 0.988 180.1Avg.
0.12822.52517.905 9.427 28.2820.774 0.738 6.758 0.0030.0003.058 0.000 0.0000.526 0.034 844.000.7521.025 0.000 22.654 0.837 180.0Run 3 Avg:
Baseline 3
12/3/2024 15:31 0.0000.0000.026 0.000 0.0000.000 0.000 1.302 0.0000.0010.000 0.000 0.0000.000 0.000 844.00.811.213 0.000 0.00 0.15 180.0
Post CTS
12/3/2024 15:54 0.0002.3020.035 0.000 0.0000.000 0.000 1.269 0.0000.0370.000 95.596 0.0000.000 0.123 844.064.630.969 0.000 2.30 0.18 180.0
12/3/2024 15:54 0.0002.9270.025 0.000 0.0000.000 0.000 1.150 0.0000.0000.000 95.872 0.0000.000 0.072 844.064.751.033 0.000 2.93 0.20 180.0
12/3/2024 15:54 0.0003.6110.015 0.000 0.0000.000 0.000 0.802 0.0000.0090.000 96.344 0.0000.000 0.000 844.064.810.869 0.000 3.61 0.19 180.0
Post NO2/Mid O2
12/3/2024 15:59 96.3104.353-0.000 0.000 0.0000.000 0.827 1.142 0.0000.0620.000 0.000 0.0000.288 0.095 847.01.001.209 0.000 100.66 11.02 180.0
12/3/2024 15:59 95.5850.914-0.000 0.000 0.0000.000 0.871 1.020 0.0000.0160.000 0.000 0.0000.043 0.092 847.01.061.318 0.000 96.50 11.07 180.0
12/3/2024 15:59 97.1080.838-0.000 0.000 0.0000.000 0.878 1.070 0.0000.0000.000 0.000 0.0000.000 0.011 847.00.440.626 0.000 97.95 10.93 180.0
Post 5-Gas
12/3/2024 16:02 0.000240.475-0.000 4.785 0.380499.463 1.969 1.710 7.4410.0980.000 1.134 252.5700.000 0.000 851.0255.433.148 10.280 240.47 0.02 180.0
12/3/2024 16:02 0.000240.299-0.000 4.749 0.000504.851 1.743 1.258 7.7240.0820.000 1.149 251.8960.000 0.000 852.0255.013.518 10.282 240.30 0.02 180.0
12/3/2024 16:02 0.000240.741-0.000 4.750 3.679501.915 2.087 1.260 10.0380.0700.317 1.320 253.0410.000 0.000 852.0255.852.893 10.239 240.74 0.02 180.0
12/3/2024 16:02 0.000241.378-0.000 4.750 3.231502.954 2.145 1.476 9.4660.1880.168 1.375 253.0510.000 0.000 852.0255.782.726 10.226 241.38 0.20 180.0
12/3/2024 16:02 0.000240.984-0.000 4.740 0.000503.459 1.842 1.340 8.6260.1080.000 1.281 251.4370.185 0.000 852.0254.583.427 10.273 240.98 0.17 180.0
12/3/2024 16:02 0.000240.275-0.000 4.715 0.000503.684 1.801 1.594 6.9510.0570.348 1.080 252.9060.314 0.000 852.0255.813.282 10.294 240.28 0.02 180.0
12/3/2024 16:02 0.000241.301-0.000 4.737 0.000499.607 1.752 1.296 8.9140.0880.000 1.244 251.8500.000 0.000 852.0255.273.881 10.283 241.30 0.02 180.0
12/3/2024 16:03 0.000241.653-0.000 4.730 0.305503.395 1.958 1.742 9.4300.1650.000 1.249 254.3660.000 0.000 852.0257.383.268 10.271 241.65 0.17 180.0
End of Test Purge
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 0.802 0.0000.0010.000 0.000 0.0000.000 0.146 854.00.640.519 0.000 0.00 0.00 180.0
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 0.862 0.0000.0000.000 0.000 0.0000.200 0.056 854.00.580.697 0.000 0.00 0.18 179.0
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 1.050 0.0000.0000.000 0.000 0.0000.000 0.010 854.00.450.651 0.000 0.00 0.12 180.0
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 1.050 0.0000.0000.000 0.000 0.0000.000 0.060 854.00.640.788 0.000 0.00 0.00 179.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 0.947 0.0000.0000.000 0.000 0.0000.000 0.015 854.00.630.901 0.000 0.00 0.00 180.0
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 1.207 0.0000.0020.000 0.000 0.0000.000 0.001 855.00.450.678 0.000 0.00 0.18 180.0
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 1.001 0.0000.0000.000 0.000 0.0000.000 0.000 854.00.500.750 0.000 0.00 0.17 180.0
12/3/2024 16:05 0.0000.000-0.000 0.000 0.0000.000 0.000 1.031 0.0000.0090.000 0.000 0.0000.000 0.000 855.00.540.813 0.000 0.00 0.00 180.0
12/3/2024 16:05 0.1040.000-0.000 0.000 0.0000.000 0.000 1.005 0.0000.0000.000 0.000 0.0000.000 0.000 855.00.630.951 0.000 0.10 0.00 180.0
GAS, Inc.
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:07:45 AM 11:46 AM
Source:
Unit Number: 1525
Serial Number: 1673777
Engine Hours:3791
Permit #: #DAQE-AN161680001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Residue Booster Station
CO NOx NMNEHC
10.563 2.505 1.318
2.000 0.300 1.000 0.150 0.700 0.030
0.029 0.011 0.006
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results ppmvd
Results g/hp-hr
Permit g/hp-hr
PASS ALL
40 CFR Part 60 Subpart JJJJ
Performance Test Report
Test Type: Initial
Test Date: 12/5/2024
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS, Inc.
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Jason Wooly
3
Hunter Newton
Gas, Inc.
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
Gas, Inc.
Unit 1525 with a serial number of 1673777 which is a Waukesha 9394 GSI engine located at Residue
Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 12/5/2024 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2275 BHP and 1200 RPM which is 91.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1525 is authorized to
operate under permit #DAQE-AN161680001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Residue Booster StationLocation 1525Unit ID
Make Waukesha Site Elevation ft.5406
Model 9394 GSI Atmospheric Pressure psi.11.86
Serial Number 1673777 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2275 2275 2275 2275
1200 1199 1200 1200
Percent Load %
Intake Manifold Pressure (hg)
91.00%91.00%91.00%91.00%
60.00 60.00 62.00 60.67
Intake Manifold Temperature (F)115.00 115.00 116.00 115.33
Ambient Conditions
Ambient Temperature Dry (F)21.00 21.00 32.00 24.67
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
186030.07 187368.48 185998.28 186465.61
5267.74 5305.63 5266.84 5280.07
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %18.20%18.32%18.23%18.25%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.26%0.54%0.51%0.44%
Permitted Standards Results
5
Catalyst
0.0250.029
Run 1 Run 2 Run 3 3 Run Average Pass Permits
07:45 AM 09:03 AM 10:17 AM 12/5/2024
CO (g/hp-hr)0.031 0.0292.000 0.300 Pass
StateFederal
CO (ppmvw)9.468 8.803 7.636 8.635
CO (ppmvd)11.574 10.777 9.338 10.563
CO (mol wt) 28.01
CO (ppmvd) @15% O2 3.308 3.123 2.702 3.044 Fail
CO (ppbvd) @15% O2 3307.745 3122.898 2702.018 3044.220 Fail
NOx (g/hp-hr)0.007 0.012 0.014 0.0111.000 0.150 Pass
NOx (ppmvw)1.260 2.245 2.639 2.048
NOx (ppmvd)1.540 2.748 3.227 2.505
NOx (mol wt) 46.01
0.985 1.235 1.011 1.077NMNEHC (ppmvw)
1.204 1.512 1.236 1.318NMNEHC (ppmvd)
NOx (ppbvd) @15% O2 440.194 796.290 933.878 723.454 Fail
NOx (ppmvd) @15% O2 0.440 0.796 0.934 0.723 Fail
NMNEHC (mol wt) 44.10
344.120 438.146 357.768 380.011 FailNMNEHC (ppbvd) @15% O2
0.005 0.006 0.005 0.0060.700 0.030 PassNMNEHC (g/hp-hr)
0.344 0.438 0.358 0.380 FailNMNEHC (ppmvd) @15% O2
Gas, Inc.
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
0.00Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
9.47
0.00
1.26
0.00
0.00
0.00
1.26
0.17
0.99
0.15%
0.21%
0.00%
18.20%
NMNEHC
8.50 1.50 0.00 1.50 1.00 0.28%18.07%
60.33 31.46 0.00 31.46 27.12 0.14%16.35%
10.44 1.02 0.00 1.02 0.97 0.15%18.32%
0.00 0.00 0.00 0.00 0.49 0.12%0.02%
Avg. Wet
NO2NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.00 0.00 0.49 0.12%0.02%
9.27 1.80 0.00 1.79 1.02 0.25%18.28%
56.09 29.58 0.00 29.58 24.98 0.14%16.64%
8.33 2.70 0.00 2.70 1.45 0.65%18.36%
0.00 0.00 0.00 0.00 0.49 0.18%0.02%
Avg. Wet 8.80 2.25 0.00 2.24 1.24 0.45%18.32%
NO2NO
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
8.30 3.03 0.00 3.03 1.01 0.29%18.10%
59.77 28.59 0.00 28.59 23.76 0.20%16.64%
6.97 2.20 0.05 2.25 1.01 0.56%18.37%
0.00 0.00 0.00 0.00 0.46 0.13%0.04%
0.00 0.00 0.00 0.00 0.49 0.18%0.02%
Avg. Wet 7.64 2.62 0.03 2.64 1.01 0.43%18.23%
NO2NO
Gas, Inc.
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Stack diameter =
Table 6.1. Data used for volumetric flow rate (Method 2)
20 inches or:1.67 feet. or:2.18 Square Feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.55
Yes
20.00
10.00
16.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
ppmd
%d
%d
%d 18.20
29.54
0.57
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
9.55
0.22
9.47
844.13
0.04
24.93
24.97
928.38
1388.05
497.99
27.44
91.19
198.95
227410.90
186030.07
Run 2
18.32
29.55
0.59
9.58
0.46
8.80
845.00
0.04
24.96
25.00
934.38
1394.05
501.32
27.44
92.28
201.33
229389.13
187368.48
Run 3
18.23
29.54
0.58
9.52
0.43
7.64
845.00
0.04
24.96
25.00
938.19
1397.86
503.44
27.44
91.77
200.20
227472.14
185998.28
18.25
29.54
0.58
9.55
0.37
8.64
844.71
0.04
24.95
24.99
933.65
1393.32
500.92
27.44
91.75
200.16
228092.58
186467.58
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.58
Exhaust Temp F
928.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.57
0.59
0.60
927.00
931.00
929.00
0.54
0.52
0.56
927.00
928.00
930.00
0.55
0.59
0.58
931.00
927.00
926.00
0.61 928.00
0.60
0.59
0.56
926.00
928.00
929.00
0.55
0.58
0.57
930.00
929.00
928.38
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.57
Exhaust Temp F
938.00
0.59
0.61
0.61
937.00
940.00
941.00
0.57
0.57
0.56
939.00
938.00
937.00
0.58
0.58
0.55
940.00
941.00
938.00
0.59 936.00
0.59
0.57
0.56
937.00
938.00
937.00
0.58
0.55
938.00
936.00
938.190.58
Run 2
Δpstd (in) H2O
0.59
Exhaust Temp F
934.00
0.57
0.60
0.61
931.00
932.00
931.00
0.60
0.69
0.55
936.00
934.00
935.00
0.57
0.58
0.59
937.00
930.00
934.00
0.54 938.00
0.56
0.58
0.59
936.00
934.00
936.00
0.56
0.58
937.00
935.00
0.59 934.38
Pass
Strat Check
26.567Check 1
26.598Check 2
26.712Check 3
MethaneGas Used
Pass/Fail
7
Gas, Inc.
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(.096)+.32(.003)+.28(.901+.001) = 29.537 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.537(1 -.18197)+.18.0(.18197) = 27.438 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.57*√(1388.045/(24.97*27.438)) = 91.19 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.182)91.192*2.182((528*24.97)/ (1388.045*29.92)) = 186030.07 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 186030.074/35.315 = 5267.735 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 11.574*(20.9-15)/(20.9-.3%)) = 3.315 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(11.574*(1.164*10^-3)*5267.735*(Run Time/60))/2275 = .031 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .031*1/453.6*2275 = .156 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .156*4.38 = .683 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
11.57 = 9.468*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
Gas, Inc.
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.76%
21.02%
10.83%
11.08%
10.62%
10.62%
11.08%10.83%
10.76%
21.02%
10.62%
21.05%
10.62%
21.05%
10.62%21.05%
0.00%
10.62%
21.05%
0.14%
0.03%
0.68%
0.14%
10.62%
Span
Zero Offset 0.00%
21.05
0.00%
10.76%0.33%1.48%0.01%
0.26%
0.56%
0.53%
0.26%
0.54%
0.51%
9
Gas, Inc.
0.0 0.0 0.0
0.0 0.0 0.0
1096.0 1094.0 1097.0
1060.0 1058.0 1061.0
7.2 7.2 7.2
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Residue Booster Station
12/5/2024
5406
1525
Waukesha
Model
Serial Number
9394 GSI
1673777
Technician Hunter Newton
Run Start Times 07:45 AM 09:03 AM 10:17 AM 11:46 AM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1199.0 1200.0 1199.7
Engine Hours 3788 3789 3790 3791
Intake Manifold Pressure (psi)60.0 60.0 62.0 60.7
Intake Manifold Temp °F 115.0 115.0 116.0 115.3
Engine Load (BHP)2275.0 2275.0 2275.0 2275.0
Ambient Temp °F 21.0 21.0 32.0 24.7
Humidity %81.0 81.0 62.0 74.7
Dew Point °F 16.0 16.0 20.0 17.3
Waukesha
YesCatalyst (Yes or No)
AFR Manufacturer/Type Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1101.0
1065.0
7.2Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
Gas, Inc.
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.34
Average:Oxygen 0.04
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 99.05
Tolerance 2.00%
Difference between measured and expected 0.78%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.32
Average:Oxygen 0.09
Pre-test System Zero Time:
Mechanical Response Time 45 seconds
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 97.82
Tolerance 5.00%
Difference between measured and expected 0.47%
Pre-test System CTS & Mechanical Response Time
49 secondsEquilibration Response Time
Value:Spike Reported 252.84
Value:Spike Expected 252.40
System (Equilibration) Response Time Target (Spike)
45 secondsSystem Zero Response Time
49 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC506322 9/17/2027 99.95 10.62%
EB0020295 6/20/2032 98.28
EB0090574 11/27/2031 21.05%
Cylinder # ALM-063647 Expiration: 5-03-2032
Propane CO NO SF6
Bottle Value 252.40 501.70 237.50 10.20
Analyzer System Response 252.84 499.33 239.00 10.24
Percent Difference 0.18%0.47%0.63%0.39%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.049 5.039
Spike Direct
Propane 254.884
Mechanical
Response Time
SF6 10.298
CO 501.208
NO 240.974
Ethylene 97.818 38 seconds
Analyzer
Response
Propane 252.842
SF6 10.240
CO 499.327
NO 239.000
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 253.492
CO 509.549
NO 241.035
49 seconds
39 seconds
9.49%
8.71%
8.43%
104.88%
104.63%
103.21%
10.258
12
Gas, Inc.
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
Gas, Inc.
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
10
16
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
186467.58
H2O%d @ Sampling Point:18.25
CO2%d @ Sampling Point:9.55
Pressure @ Sampling Point (Pg "H2O):0.58
Temperature @ Sampling Point (Deg F):933.65
Gas, Inc.
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 98.28 99.05 5.039 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 99.049 5.039
Spike Direct
Propane 254.884
Mechanical
Response Time
SF6 10.298
CO 501.208
NO 240.974
Ethylene 97.818 38 seconds
Analyzer
Response
Propane 252.842
SF6 10.240
CO 499.327
NO 239.000
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 253.492
CO 509.549
NO 241.035
49 seconds
39 seconds
9.49%
8.71%
8.43%
104.88%
104.63%
103.21%
10.258
Gas, Inc.
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
252.400
10.200
501.700
237.500
254.884
10.298
501.208
240.974
0.98%
0.96%
0.10%
1.46%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.038
0.000
Spike Average
25.158
0.977
Dilution Factor
9.487%
Expected
23.987
% Recovery
104.880%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.897
Dilution Factor
8.710%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.868
Dilution Factor
8.429%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.003 21.963 21.280 103.210%
0.000683
0.001017
0.000708
0.000 23.002 21.984 104.630%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass4.82%
16
Gas, Inc.
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-18.6062841 Pass
Line Position Difference:Resolution Difference to Reference 4.82%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
98.28
97.97
0.32%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
Gas, Inc.
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Residue Booster Station; 1525; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
12/5/2024
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
12/5/2024
Hunter Newton
Gas, Inc.
Appendices
Gas, Inc.
Gas, Inc.
Spike (5 Gas)
Gas, Inc.
9% O2/NO2
Gas, Inc.
Ethylene Only
Gas, Inc.
BIP
Gas, Inc.
21% O2
Tri Probe Certification
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3/3/2022
Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS, Inc.
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
Gas, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Residue Booster Station
Unit Number:1525
Make:Waukesha
Location:9394 GSIModel:
1673777Serial Number:
RAW Result Data
Stability
12/5/2024 06:17 2.3080.0000.002 0.003 0.2560.642 0.000 0.000 0.0000.0380.000 0.642 0.6900.000 0.000 857.01.120.000 0.000 2.31 0.01 180.0
Pre Test Baseline Direct
12/5/2024 06:25 0.0000.000-0.001 0.000 0.0000.000 0.000 0.458 0.0000.0220.062 0.000 0.0000.017 0.000 854.00.300.449 0.000 0.00 0.00 180.0
12/5/2024 06:26 0.0000.000-0.003 0.000 0.0000.000 0.000 0.571 0.0000.0000.002 0.000 0.0000.000 0.000 854.00.340.503 0.000 0.00 0.00 180.0
12/5/2024 06:27 0.0000.000-0.002 0.000 0.0000.000 0.000 0.651 0.0000.0820.091 0.000 0.0000.000 0.000 852.00.390.578 0.000 0.00 0.13 180.0
CTS Direct
12/5/2024 06:32 0.0000.0000.008 0.000 0.0780.000 0.000 0.192 0.0000.0000.000 98.642 0.0000.000 0.000 845.066.100.506 0.000 0.00 0.06 180.0
12/5/2024 06:33 0.0000.0000.006 0.000 0.0000.000 0.000 0.237 0.0000.0230.000 99.022 0.0000.061 0.000 844.066.370.523 0.000 0.00 0.19 180.0
12/5/2024 06:34 0.0000.0000.007 0.000 0.0000.000 0.000 0.256 0.0000.0060.000 99.482 0.0000.000 0.000 844.066.680.537 0.000 0.00 0.06 182.0
High O2 Direct
12/5/2024 06:39 0.0000.0000.002 0.000 0.0000.000 0.000 0.429 0.0000.0000.000 0.000 0.0000.000 0.000 844.00.480.714 0.000 0.00 21.04 180.0
12/5/2024 06:39 0.3080.000-0.010 0.000 0.0000.000 0.000 0.564 0.0000.0300.000 0.000 0.0000.007 0.000 844.00.340.511 0.000 0.31 20.95 180.0
12/5/2024 06:40 0.0000.000-0.003 0.000 0.0000.000 0.000 0.622 0.0000.0590.000 0.000 0.0000.000 0.000 844.00.410.614 0.000 0.00 21.07 180.0
NO2/Mid O2 Direct
12/5/2024 06:49 100.4650.000-0.004 0.000 0.0000.000 0.857 0.410 0.3730.0000.000 0.000 0.0000.000 0.000 844.00.150.232 0.000 100.47 10.65 180.0
12/5/2024 06:49 100.3770.000-0.003 0.000 0.0000.000 0.858 0.563 0.3720.0000.000 0.000 0.0000.000 0.000 844.00.160.234 0.000 100.38 10.84 180.0
12/5/2024 06:50 100.7080.000-0.002 0.000 0.0000.000 0.811 0.378 0.4340.0000.000 0.000 0.0000.000 0.000 844.00.220.336 0.000 100.71 10.80 180.0
Spike Direct
12/5/2024 06:53 0.000240.3450.001 4.768 1.427499.552 1.840 1.464 11.6220.3540.000 1.356 254.3160.000 0.000 844.0257.813.888 10.296 240.34 0.23 180.0
12/5/2024 06:54 0.000241.2350.002 4.778 1.108502.217 1.800 1.606 10.9350.3150.000 1.406 255.1590.112 0.000 844.0258.583.727 10.297 241.24 0.27 180.0
12/5/2024 06:54 0.000241.3420.002 4.776 1.297501.854 1.809 1.609 10.9880.1950.000 1.408 255.1780.000 0.000 844.0258.593.703 10.300 241.34 0.31 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
12/5/2024 06:56 0.0000.0000.027 0.000 0.0000.000 0.000 1.069 0.0000.0010.341 0.000 0.0000.000 0.058 844.00.440.483 0.000 0.00 0.12 179.0
12/5/2024 06:56 0.0000.0000.018 0.000 0.0000.000 0.000 1.067 0.0000.0040.000 0.000 0.0000.106 0.000 844.00.320.482 0.000 0.00 0.00 180.0
12/5/2024 06:57 0.0000.0000.014 0.000 0.0000.000 0.000 1.026 0.0000.0010.000 0.000 0.0000.000 0.000 844.00.210.314 0.000 0.00 0.15 180.0
CTS System with Response Time
12/5/2024 06:58 0.0000.0000.021 0.000 0.0000.000 0.000 0.345 0.0000.0050.000 97.622 0.0000.000 0.000 844.065.440.534 0.000 0.00 0.20 179.0
12/5/2024 06:59 0.0000.0000.020 0.000 0.0000.000 0.000 0.424 0.0000.0000.000 97.852 0.0000.111 0.000 844.065.650.616 0.000 0.00 0.19 179.0
12/5/2024 06:59 0.0000.0000.020 0.000 0.0000.000 0.000 0.507 0.0000.0050.000 97.980 0.0000.000 0.000 844.065.700.572 0.000 0.00 0.06 180.0
NO2/Mid O2 System with Response Time
12/5/2024 07:07 98.7600.0000.006 0.000 0.0000.000 0.894 0.726 0.0000.0000.000 0.000 0.0000.000 0.000 844.00.040.065 0.000 98.76 10.84 179.0
12/5/2024 07:07 99.2200.0000.006 0.000 0.0000.000 0.894 0.876 0.0000.0010.000 0.000 0.0000.000 0.005 844.00.100.140 0.000 99.22 10.84 180.0
12/5/2024 07:07 99.4990.0000.007 0.000 0.2130.000 0.905 0.691 0.0650.0020.000 0.000 0.0000.127 0.000 844.00.060.090 0.000 99.50 10.82 181.0
Spike System with Response Time
12/5/2024 07:09 0.000238.9280.011 4.801 1.080499.486 2.017 1.453 11.0470.1160.262 1.448 252.7970.000 0.000 844.0256.093.498 10.233 238.93 0.26 180.0
12/5/2024 07:10 0.000238.9990.012 4.822 0.808499.326 2.014 1.431 10.8240.1120.437 1.395 252.9300.063 0.000 844.0256.183.476 10.243 239.00 0.26 180.0
12/5/2024 07:10 0.000239.0730.014 4.801 1.167499.169 2.046 1.569 10.9840.0940.000 1.392 252.8000.000 0.000 844.0256.093.540 10.243 239.07 0.19 180.0
Baseline System with Response Time
12/5/2024 07:12 0.0000.0000.003 0.000 0.0000.000 0.000 0.618 0.0170.0000.000 0.000 0.0000.000 0.000 844.00.100.151 0.000 0.00 0.17 180.0
12/5/2024 07:13 0.0000.0000.005 0.000 0.0320.000 0.000 0.793 0.0000.0050.000 0.000 0.0000.000 0.000 844.00.180.263 0.000 0.00 0.17 180.0
12/5/2024 07:13 0.0000.0000.004 0.000 0.0000.000 0.000 0.658 0.0000.0010.000 0.000 0.0000.000 0.000 844.00.220.324 0.000 0.00 0.11 180.0
Run 1 - A 30minute/60min
12/5/2024 07:45 0.00011.58210.225 7.873 29.3177.049 1.623 2.917 0.0000.0442.357 0.000 1.1510.650 0.527 844.02.941.106 0.000 11.58 0.14 179.0
12/5/2024 07:46 0.0001.63016.019 9.815 38.8545.914 1.399 5.373 0.0580.0002.395 0.000 0.0000.639 0.272 844.01.150.904 0.000 1.63 0.13 180.0
12/5/2024 07:47 0.0004.73417.937 9.480 36.2390.028 1.004 4.965 0.0000.0001.149 0.000 0.0000.525 0.213 844.01.080.977 0.000 4.73 0.14 180.0
12/5/2024 07:48 0.0005.00918.773 9.411 32.4280.144 1.164 5.982 0.0000.0001.258 0.000 0.0000.614 0.210 844.01.020.897 0.000 5.01 0.16 179.0
12/5/2024 07:49 0.0001.23118.401 9.532 24.3660.499 0.857 5.282 0.0000.0001.027 0.000 0.0000.527 0.170 844.00.930.891 0.000 1.23 0.02 180.0
12/5/2024 07:50 0.0002.84819.340 9.387 32.1632.972 1.678 7.841 0.0000.0000.920 0.000 0.0000.619 0.206 844.00.970.833 0.000 2.85 0.02 180.0
12/5/2024 07:51 0.0001.10218.967 9.420 28.5947.278 1.183 10.291 0.0000.0001.029 0.000 0.0000.538 0.184 844.00.950.868 0.000 1.10 0.19 180.0
12/5/2024 07:53 0.0001.87918.596 9.556 43.3207.036 1.176 9.753 0.2460.0001.757 0.000 0.0000.654 0.237 844.01.070.887 0.000 1.88 0.15 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/5/2024 07:54 0.0000.00018.323 9.515 33.25310.233 0.616 8.748 0.0000.0000.597 0.000 0.0000.636 0.180 844.00.930.861 0.000 0.00 0.19 180.0
12/5/2024 07:55 0.0000.47118.425 9.496 36.18018.315 0.829 11.186 0.0000.0000.438 0.000 0.0000.549 0.206 844.00.950.808 0.000 0.47 0.02 179.0
12/5/2024 07:56 0.0001.96418.546 9.549 33.21415.257 1.292 12.877 0.0000.0000.049 0.000 0.0000.564 0.194 844.01.000.914 0.000 1.96 0.21 180.0
12/5/2024 07:57 0.0001.33818.668 9.509 27.5095.148 0.896 8.929 0.0000.0000.307 0.000 0.0000.436 0.139 844.00.870.883 0.000 1.34 0.02 180.0
12/5/2024 07:58 0.0000.37618.747 9.512 29.51015.966 0.757 10.663 0.0000.0000.000 0.000 0.0000.485 0.157 844.00.930.916 0.000 0.38 0.15 180.0
12/5/2024 07:59 0.0000.27518.720 9.490 26.57520.482 0.777 12.541 0.0000.0000.443 0.000 0.0000.518 0.133 844.00.820.827 0.000 0.27 0.24 179.0
12/5/2024 08:00 0.0001.19218.615 9.578 28.24119.145 0.843 12.308 0.0000.0000.824 0.000 0.0000.561 0.169 844.00.920.874 0.000 1.19 0.15 180.0
12/5/2024 08:01 0.0000.03418.246 9.615 35.43025.749 0.656 11.848 0.0000.0000.103 0.000 0.0000.543 0.204 844.00.930.789 0.000 0.03 0.14 180.0
12/5/2024 08:02 0.0002.21618.189 9.610 27.43117.884 1.536 16.057 0.0000.0000.000 0.000 0.0000.556 0.166 844.00.900.858 0.000 2.22 0.19 179.0
12/5/2024 08:03 0.0001.73418.233 9.663 26.0846.870 0.624 6.944 0.0000.0000.000 0.000 0.0000.486 0.155 844.00.900.891 0.000 1.73 0.02 180.0
12/5/2024 08:04 0.0000.52718.243 9.568 14.3040.000 0.000 3.519 0.0000.0000.958 0.000 0.0000.468 0.102 844.00.750.825 0.000 0.53 4.43 179.0
12/5/2024 08:05 0.0002.00318.289 9.629 21.5400.000 0.000 3.885 0.0000.0000.233 0.000 0.0000.576 0.128 844.00.840.869 0.000 2.00 0.15 180.0
12/5/2024 08:06 0.0000.00018.302 9.597 27.24510.509 0.588 8.520 0.0000.0000.000 0.000 0.0000.523 0.144 844.00.880.889 0.000 0.00 0.15 180.0
12/5/2024 08:07 0.0000.00018.278 9.604 39.80210.357 0.900 9.947 0.0440.0000.000 0.000 0.0000.543 0.215 844.01.030.896 0.000 0.00 0.13 180.0
12/5/2024 08:08 0.0000.00018.254 9.580 37.9359.964 0.690 9.115 0.0000.0000.000 0.000 0.0000.538 0.177 844.00.930.870 0.000 0.00 0.18 180.0
12/5/2024 08:09 0.0000.55718.210 9.587 28.9166.783 1.360 10.010 0.0000.0000.000 0.000 0.0000.541 0.161 844.00.930.907 0.000 0.56 0.03 179.0
12/5/2024 08:10 0.0001.70418.236 9.635 25.2403.575 1.139 8.703 0.0000.0000.000 0.000 0.0000.524 0.151 844.00.920.928 0.000 1.70 0.25 180.0
12/5/2024 08:11 0.0000.00018.278 9.606 30.6195.532 0.754 8.002 0.0000.0000.001 0.000 0.0000.574 0.156 844.00.830.776 0.000 0.00 0.24 180.0
12/5/2024 08:12 0.0000.07218.216 9.596 33.9305.200 0.852 6.947 0.0000.0000.000 0.000 0.0000.494 0.165 844.00.970.968 0.000 0.07 0.19 180.0
12/5/2024 08:13 0.0000.57818.253 9.620 27.1516.054 0.867 7.540 0.0000.0000.000 0.000 0.0000.504 0.153 844.00.920.918 0.000 0.58 0.17 180.0
12/5/2024 08:14 0.0000.00018.289 9.601 25.0614.628 0.928 8.573 0.0000.0000.000 0.000 0.0000.448 0.121 844.00.780.813 0.000 0.00 0.02 180.0
12/5/2024 08:15 0.0000.00018.299 9.574 33.4896.279 0.308 6.645 0.0000.0001.065 0.000 0.0000.555 0.161 844.00.940.930 0.000 0.00 0.18 180.0
0.0001.50218.071 9.507 30.4658.495 0.910 8.530 0.0120.0010.564 0.000 0.0380.546 0.185 844.000.9990.886 0.000 1.501 0.280 179.8Avg.
Spike 1
12/5/2024 08:20 0.00031.46216.351 9.174 24.65760.325 1.888 8.496 0.2590.0000.000 0.797 25.1580.382 0.267 844.027.121.350 0.977 31.46 0.14 180.0
Run 1 - B 30minute/60min
12/5/2024 08:29 0.0001.49418.386 9.566 25.5590.000 0.000 2.349 0.0000.0000.000 0.000 0.0000.550 0.155 844.00.860.819 0.000 1.49 0.01 180.0
12/5/2024 08:30 0.0000.00018.387 9.543 31.4936.798 0.505 8.054 0.0000.0000.000 0.000 0.0000.535 0.172 844.00.940.895 0.000 0.00 0.17 180.0
12/5/2024 08:31 0.0000.26918.330 9.517 26.9226.604 1.070 10.370 0.0000.0000.000 0.000 0.0000.556 0.154 844.00.830.779 0.000 0.27 0.23 179.0
12/5/2024 08:32 0.0001.70318.375 9.591 31.65611.623 0.998 11.601 0.0000.0000.000 0.000 0.0000.701 0.182 844.00.900.801 0.000 1.70 0.14 180.0
12/5/2024 08:33 0.0000.00018.403 9.562 32.97129.911 0.910 14.887 0.0000.0000.000 0.000 0.0000.626 0.203 844.01.010.903 0.000 0.00 0.15 181.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/5/2024 08:34 0.0001.29618.332 9.579 36.92118.650 1.385 13.927 0.0000.0000.000 0.000 0.0000.613 0.240 844.01.040.835 0.000 1.30 0.20 180.0
12/5/2024 08:35 0.0002.12418.328 9.609 31.56719.085 1.356 13.398 0.0000.0000.000 0.000 0.0000.558 0.202 844.00.990.880 0.000 2.12 0.02 180.0
12/5/2024 08:36 0.0001.21818.293 9.566 36.39823.480 1.396 16.244 0.0000.0000.000 0.000 0.0000.599 0.233 844.01.070.900 0.000 1.22 0.02 179.0
12/5/2024 08:37 0.0000.94418.335 9.616 39.75417.585 1.428 14.300 0.0000.0000.000 0.000 0.0000.660 0.241 844.01.080.903 0.000 0.94 0.17 180.0
12/5/2024 08:38 0.0001.36418.330 9.631 36.44913.261 1.389 13.137 0.0000.0000.000 0.000 0.0000.620 0.223 844.01.010.851 0.000 1.36 0.03 180.0
12/5/2024 08:39 0.0000.06418.312 9.598 28.16811.117 1.181 11.190 0.0000.0000.000 0.000 0.0000.550 0.171 844.00.880.805 0.000 0.06 0.17 180.0
12/5/2024 08:40 0.0001.25018.279 9.622 29.87214.406 1.227 11.958 0.0000.0000.000 0.000 0.0000.559 0.202 844.00.940.796 0.000 1.25 0.15 180.0
12/5/2024 08:41 0.0000.94318.298 9.620 26.0225.431 1.485 9.438 0.0000.0000.000 0.000 0.0000.530 0.216 844.01.050.920 0.000 0.94 0.16 180.0
12/5/2024 08:42 0.0000.00018.337 9.588 26.5670.472 0.852 6.431 0.0000.0000.000 0.000 0.0000.576 0.181 844.00.910.827 0.000 0.00 0.14 180.0
12/5/2024 08:43 0.0000.18218.299 9.563 28.2546.914 0.421 7.579 0.0000.0000.370 0.000 0.0000.568 0.194 844.00.910.779 0.000 0.18 0.14 179.0
12/5/2024 08:44 0.0002.08618.314 9.634 31.41120.069 1.184 13.403 0.0000.0000.000 0.000 0.0000.691 0.215 844.01.010.869 0.000 2.09 0.02 180.0
12/5/2024 08:45 0.0000.00018.250 9.551 35.74416.971 1.139 12.608 0.0000.0000.000 0.000 0.0000.628 0.220 844.01.070.948 0.000 0.00 0.17 179.0
12/5/2024 08:46 0.0001.40118.287 9.594 26.59812.380 1.674 13.098 0.0000.0000.000 0.000 0.0000.602 0.190 844.00.940.843 0.000 1.40 0.16 179.0
12/5/2024 08:47 0.0001.77118.303 9.625 25.7129.693 1.403 10.981 0.0000.0000.000 0.000 0.0000.599 0.192 844.00.950.854 0.000 1.77 0.16 180.0
12/5/2024 08:48 0.0001.79718.307 9.642 31.8919.144 1.028 8.847 0.0000.0000.000 0.000 0.0000.673 0.219 844.01.020.872 0.000 1.80 0.15 180.0
12/5/2024 08:49 0.0000.03018.346 9.602 32.8298.667 1.172 9.347 0.0000.0000.000 0.000 0.0000.618 0.202 844.00.990.875 0.000 0.03 0.13 180.0
12/5/2024 08:50 0.0000.67518.258 9.573 26.4601.243 1.018 6.742 0.0000.0000.000 0.000 0.0000.685 0.172 845.00.870.787 0.000 0.68 1.07 179.0
12/5/2024 08:51 0.0001.60418.337 9.635 26.7043.209 0.568 5.794 0.0000.0000.000 0.000 0.0000.672 0.195 844.00.940.827 0.000 1.60 0.15 180.0
12/5/2024 08:52 0.0001.48018.326 9.618 32.1385.223 0.743 7.671 0.0000.0000.000 0.000 0.0000.656 0.219 845.01.020.866 0.000 1.48 0.15 180.0
12/5/2024 08:53 0.0000.35118.322 9.589 27.5785.615 1.039 8.526 0.0000.0000.000 0.000 0.0000.568 0.184 845.00.960.882 0.000 0.35 0.02 180.0
12/5/2024 08:54 0.0002.31218.312 9.596 26.8212.147 0.861 7.082 0.0000.0000.000 0.000 0.0000.625 0.193 845.00.950.848 0.000 2.31 0.02 180.0
12/5/2024 08:55 0.0001.55518.338 9.603 26.1012.790 0.779 6.408 0.0000.0000.000 0.000 0.0000.590 0.194 845.00.970.874 0.000 1.56 0.22 180.0
12/5/2024 08:56 0.0001.05818.312 9.586 30.6799.897 1.460 11.068 0.0000.0000.000 0.000 0.0000.683 0.214 845.01.010.878 0.000 1.06 0.02 180.0
12/5/2024 08:57 0.0001.06518.300 9.582 27.48110.542 1.626 12.180 0.0000.0000.000 0.000 0.0000.676 0.209 845.01.010.889 0.000 1.06 0.02 180.0
12/5/2024 08:58 0.0000.55818.310 9.568 32.71910.305 0.924 9.229 0.0000.0000.000 0.000 0.0000.601 0.230 845.01.010.824 0.000 0.56 0.16 180.0
0.0001.02018.322 9.592 30.31510.441 1.074 10.262 0.0000.0000.012 0.000 0.0000.612 0.201 844.270.9710.854 0.000 1.019 0.151 179.8Avg.
0.0001.26118.196 9.550 30.3909.468 0.992 9.396 0.0060.0010.288 0.000 0.0190.579 0.193 844.130.9850.870 0.000 1.260 0.215 179.8Run 1 Avg:
Baseline 1
12/5/2024 09:01 0.0000.0000.022 0.000 0.0790.000 0.000 1.127 0.0000.0010.526 0.000 0.0000.075 0.000 845.00.490.734 0.000 0.00 0.12 180.0
Run 2 - A 30minute/60min
12/5/2024 09:03 0.0004.44317.410 9.190 28.01718.580 1.668 10.663 0.0000.0000.000 0.000 0.0000.684 0.237 845.01.060.883 0.000 4.44 0.16 180.0
12/5/2024 09:04 0.0002.32718.216 9.571 32.44022.028 1.776 14.476 0.0000.0000.000 0.000 0.0000.697 0.254 845.01.060.827 0.000 2.33 0.15 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/5/2024 09:05 0.0000.58018.274 9.553 27.7048.994 1.602 10.817 0.0000.0000.000 0.000 0.0000.609 0.221 845.01.000.840 0.000 0.58 0.02 180.0
12/5/2024 09:07 0.0001.31318.263 9.570 26.2805.631 1.215 8.397 0.0000.0000.000 0.000 0.0000.512 0.201 845.01.040.952 0.000 1.31 0.16 179.0
12/5/2024 09:08 0.0002.30118.338 9.636 26.5066.409 1.112 7.447 0.0000.0000.000 0.000 0.0000.640 0.202 845.01.000.898 0.000 2.30 0.02 180.0
12/5/2024 09:09 0.0000.00018.421 9.583 31.27312.244 1.015 9.730 0.0000.0000.000 0.000 0.0000.641 0.214 845.01.020.891 0.000 0.00 0.18 180.0
12/5/2024 09:10 0.0001.92018.348 9.597 27.52212.589 1.157 9.659 0.0000.0000.000 0.000 0.0000.653 0.203 845.01.020.926 0.000 1.92 0.02 180.0
12/5/2024 09:11 0.0001.67318.363 9.614 30.0447.079 0.990 7.433 0.0000.0000.000 0.000 0.0000.632 0.215 845.00.950.774 0.000 1.67 0.21 180.0
12/5/2024 09:12 0.0000.00018.340 9.554 34.85917.251 1.227 12.165 0.0000.0000.000 0.000 0.0000.549 0.233 845.01.070.901 0.000 0.00 0.15 180.0
12/5/2024 09:13 0.0000.24718.317 9.525 31.68213.799 1.830 14.264 0.0000.0000.592 0.000 0.0000.627 0.203 845.01.010.906 0.000 0.25 0.02 180.0
12/5/2024 09:14 0.0001.72418.266 9.572 23.0922.359 0.700 5.896 0.0000.0000.000 0.000 0.0000.603 0.166 845.00.880.818 0.000 1.72 0.19 179.0
12/5/2024 09:15 0.0002.93518.295 9.677 35.0477.422 1.412 8.329 0.0000.0010.000 0.000 0.0000.675 0.252 845.01.090.874 0.000 2.94 0.02 180.0
12/5/2024 09:16 0.0000.70418.345 9.588 29.12410.627 1.432 10.122 0.0000.0000.000 0.000 0.0000.661 0.226 845.01.060.909 0.000 0.70 0.25 180.0
12/5/2024 09:17 0.0000.99918.264 9.569 36.68615.593 1.329 11.586 0.0000.0000.000 0.000 0.0000.620 0.252 845.01.160.983 0.000 1.00 0.02 179.0
12/5/2024 09:18 0.0002.63018.271 9.650 34.72316.411 2.150 15.190 0.0000.0000.000 0.000 0.0000.670 0.263 845.01.100.859 0.000 2.63 0.21 180.0
12/5/2024 09:19 0.0002.17218.314 9.606 30.9813.551 1.297 7.658 0.0000.0000.051 0.000 0.0000.663 0.217 845.01.000.857 0.000 2.17 0.17 180.0
12/5/2024 09:20 0.0000.74718.295 9.595 32.40610.388 0.915 8.448 0.0000.0000.000 0.000 0.0000.676 0.215 845.01.040.918 0.000 0.75 0.02 180.0
12/5/2024 09:21 0.0002.29318.298 9.633 26.0446.317 1.240 6.793 0.0000.0000.000 0.000 0.0000.677 0.200 845.01.030.945 0.000 2.29 0.14 180.0
12/5/2024 09:22 0.0001.93418.330 9.633 26.9956.037 0.704 6.051 0.0000.0000.000 0.000 0.0000.696 0.201 845.01.000.897 0.000 1.93 0.02 180.0
12/5/2024 09:23 0.0002.16918.289 9.611 35.04718.230 1.424 12.673 0.0000.0000.000 0.000 0.0000.713 0.231 845.01.090.940 0.000 2.17 0.02 180.0
12/5/2024 09:24 0.0002.41618.313 9.628 26.23310.405 1.474 10.554 0.0000.0000.000 0.000 0.0000.733 0.205 845.01.040.948 0.000 2.42 0.14 180.0
12/5/2024 09:25 0.0001.98518.309 9.626 21.9977.392 1.450 9.243 0.0000.0000.000 0.000 0.0000.682 0.176 845.00.940.887 0.000 1.98 0.02 180.0
12/5/2024 09:26 0.0001.82918.309 9.637 21.4854.209 1.296 7.504 0.0000.0000.000 0.000 0.0000.682 0.182 845.00.970.903 0.000 1.83 0.36 180.0
12/5/2024 09:27 0.0001.51818.326 9.619 27.0962.333 0.619 5.730 0.0000.0000.000 0.000 0.0000.712 0.186 845.00.980.913 0.000 1.52 0.18 180.0
12/5/2024 09:28 0.0002.57318.294 9.647 26.7877.696 1.374 9.546 0.0000.0000.000 0.000 0.0000.685 0.200 845.01.040.961 0.000 2.57 0.15 180.0
12/5/2024 09:29 0.0002.02518.277 9.629 21.4902.076 0.569 4.549 0.0000.0000.000 0.000 0.0000.614 0.181 845.00.950.885 0.000 2.02 0.14 180.0
12/5/2024 09:30 0.0000.39918.309 9.588 32.59011.333 0.538 7.158 0.0000.0000.000 0.000 0.0000.739 0.231 845.01.060.903 0.000 0.40 0.15 180.0
12/5/2024 09:31 0.0002.06718.313 9.646 28.6167.337 1.571 8.895 0.0000.0000.000 0.000 0.0000.712 0.211 845.01.010.884 0.000 2.07 0.14 180.0
12/5/2024 09:32 0.0001.75718.329 9.623 30.3803.516 1.509 7.644 0.0000.0000.000 0.000 0.0000.645 0.202 845.00.990.884 0.000 1.76 0.14 180.0
12/5/2024 09:33 0.0004.16518.310 9.576 25.4280.292 1.199 5.495 0.0000.0000.000 0.000 0.0000.724 0.182 845.00.980.921 0.000 4.16 4.08 180.0
0.0001.79518.278 9.592 28.9529.271 1.260 9.137 0.0000.0000.021 0.000 0.0000.661 0.212 845.001.0210.896 0.000 1.794 0.255 179.9Avg.
Spike 2
12/5/2024 09:40 0.00029.58116.635 9.186 28.42556.091 2.336 6.505 0.2730.0000.000 0.509 23.0020.481 0.378 845.024.981.328 0.897 29.58 0.14 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
12/5/2024 09:42 0.00018.06317.423 9.378 20.01622.986 1.458 2.416 0.2270.0000.000 0.000 11.8080.409 0.341 845.013.161.004 0.439 18.06 4.46 180.0
12/5/2024 09:43 0.0002.03118.399 9.537 23.8460.000 0.577 3.615 0.0000.0000.000 0.000 0.0000.533 0.206 845.01.010.889 0.000 2.03 0.17 180.0
12/5/2024 09:44 0.0002.54518.431 9.548 26.3230.000 0.939 4.096 0.0000.0000.000 0.000 0.0000.650 0.215 845.00.980.821 0.000 2.54 0.14 180.0
12/5/2024 09:45 0.0001.80118.441 9.571 32.5304.402 1.001 6.129 0.0000.0000.000 0.000 0.0000.589 0.250 845.01.120.933 0.000 1.80 0.19 180.0
12/5/2024 09:46 0.0002.10318.422 9.540 35.2455.875 1.167 7.343 0.0000.0000.000 0.000 0.0000.610 0.247 845.01.060.855 0.000 2.10 0.18 180.0
12/5/2024 09:47 0.0001.98318.436 9.559 35.55912.289 1.310 10.260 0.0120.0000.000 0.000 0.0000.629 0.269 845.01.190.976 0.000 1.98 0.22 180.0
12/5/2024 09:48 0.0002.75418.417 9.561 34.22615.055 1.763 13.301 0.0000.0000.000 0.000 0.0000.641 0.258 845.01.090.854 0.000 2.75 0.21 180.0
12/5/2024 09:50 0.0002.97518.405 9.565 32.51524.198 1.535 14.959 0.0000.0000.000 0.000 0.0000.631 0.256 845.01.140.940 0.000 2.97 0.02 180.0
12/5/2024 09:51 0.0001.79118.413 9.586 27.63016.009 2.187 15.401 0.0000.0000.000 0.000 0.0000.584 0.210 845.01.000.866 0.000 1.79 0.02 181.0
12/5/2024 09:52 0.0001.74418.380 9.599 28.1716.063 1.613 9.331 0.0000.0000.000 0.000 0.0000.489 0.207 845.01.010.891 0.000 1.74 0.02 180.0
12/5/2024 09:53 0.0002.16818.354 9.599 36.32110.212 1.162 8.049 0.0000.0000.000 0.000 0.0000.488 0.272 845.01.221.008 0.000 2.17 0.14 180.0
12/5/2024 09:54 0.0002.16918.373 9.594 37.0225.524 1.337 8.353 0.0000.0000.000 0.000 0.0000.533 0.266 845.01.150.926 0.000 2.17 0.02 180.0
12/5/2024 09:55 0.0002.01618.376 9.600 30.25610.180 1.611 11.268 0.0000.0000.000 0.000 0.0000.593 0.242 845.01.070.872 0.000 2.02 0.02 180.0
12/5/2024 09:56 0.0002.38718.322 9.600 37.46616.247 1.502 12.858 0.2110.0000.000 0.000 0.0000.547 0.270 845.01.160.930 0.000 2.39 0.02 180.0
12/5/2024 09:57 0.0002.48618.333 9.598 32.94114.837 1.494 12.987 0.1910.0000.000 0.000 0.0000.441 0.259 845.01.191.008 0.000 2.49 0.16 180.0
12/5/2024 09:58 0.0002.98718.335 9.619 31.64520.288 1.765 14.555 0.0260.0000.000 0.000 0.0000.617 0.253 845.01.100.890 0.000 2.99 0.15 180.0
12/5/2024 09:59 0.0002.20718.303 9.575 26.8027.328 1.529 9.729 0.0000.0000.000 0.000 0.0000.553 0.192 845.01.010.943 0.000 2.21 0.17 179.0
12/5/2024 10:00 0.0001.68818.369 9.612 21.7661.181 0.589 5.380 0.0000.0000.000 0.000 0.0000.380 0.187 845.01.010.960 0.000 1.69 0.13 180.0
12/5/2024 10:01 0.0001.56318.335 9.592 20.4311.729 0.725 4.458 0.0000.0000.000 0.000 0.0000.568 0.175 845.00.880.789 0.000 1.56 1.13 180.0
12/5/2024 10:02 0.0002.59118.383 9.584 23.2000.000 0.351 2.762 0.0000.0000.411 0.000 0.0000.466 0.182 845.00.940.870 0.000 2.59 1.03 180.0
12/5/2024 10:03 0.0002.17018.395 9.593 16.5410.000 0.000 1.926 0.0000.0000.000 0.000 0.0000.493 0.161 845.00.900.867 0.000 2.17 0.24 180.0
12/5/2024 10:04 0.0001.85818.415 9.594 27.2516.494 0.275 3.905 0.0000.0000.000 0.000 0.0000.587 0.197 845.00.940.826 0.000 1.86 0.13 180.0
12/5/2024 10:05 0.0002.22618.422 9.584 26.6179.067 1.143 8.425 0.0000.0000.000 0.000 0.0000.578 0.235 845.01.050.870 0.000 2.23 0.19 180.0
12/5/2024 10:06 0.0002.04718.439 9.614 27.70313.626 1.233 10.063 0.0000.0000.000 0.000 0.0000.518 0.224 845.01.040.888 0.000 2.05 0.14 180.0
12/5/2024 10:07 0.0002.25818.402 9.580 29.61111.261 1.339 10.001 0.0000.0000.000 0.000 0.0000.530 0.229 845.01.110.982 0.000 2.26 0.14 180.0
12/5/2024 10:08 0.0002.00518.386 9.576 24.7311.353 0.881 4.389 0.0000.0000.107 0.000 0.0000.461 0.195 845.01.000.920 0.000 2.01 1.45 180.0
12/5/2024 10:09 0.0002.24818.371 9.600 18.3070.000 0.283 2.161 0.0000.0000.251 0.000 0.0000.495 0.194 845.00.950.844 0.000 2.25 2.67 180.0
12/5/2024 10:10 0.0001.07318.424 9.562 14.5410.000 0.000 1.654 0.0000.0000.070 0.000 0.0000.500 0.164 845.00.920.880 0.000 1.07 5.92 180.0
12/5/2024 10:11 0.0003.17418.422 9.566 24.7580.000 0.341 2.865 0.0000.0000.103 0.000 0.0000.582 0.210 845.00.990.858 0.000 3.17 0.14 180.0
12/5/2024 10:12 0.0001.75118.441 9.541 31.05313.825 1.368 12.103 0.0000.0000.000 0.000 0.0000.591 0.216 845.01.080.965 0.000 1.75 0.02 180.0
0.0002.69518.359 9.574 27.8348.334 1.083 7.825 0.0220.0000.031 0.000 0.3940.543 0.226 845.001.4490.904 0.015 2.695 0.655 180.0Avg.
0.0002.24518.319 9.583 28.3938.803 1.171 8.481 0.0110.0000.026 0.000 0.1970.602 0.219 845.001.2350.900 0.007 2.245 0.455 180.0Run 2 Avg:
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
12/5/2024 10:15 0.0000.0000.019 0.000 0.1700.000 0.000 1.056 0.0000.0000.720 0.000 0.0000.016 0.000 845.00.490.735 0.000 0.00 0.18 180.0
Run 3 - A 30minute/60min
12/5/2024 10:17 0.00030.4098.924 5.627 24.5040.000 0.850 4.331 0.3800.4180.000 0.000 0.0810.491 0.457 845.01.500.755 0.000 30.41 0.00 180.0
12/5/2024 10:18 0.0002.10818.318 9.539 23.82810.006 1.465 8.876 0.0000.0000.000 0.000 0.0000.563 0.200 845.00.980.869 0.000 2.11 0.02 180.0
12/5/2024 10:19 0.0003.62418.380 9.557 23.8200.371 0.687 4.273 0.0000.0000.178 0.000 0.0000.494 0.198 845.00.980.873 0.000 3.62 0.28 180.0
12/5/2024 10:20 0.0003.03718.423 9.552 19.4080.000 0.862 3.912 0.0000.0000.000 0.000 0.0000.577 0.187 845.00.870.750 0.000 3.04 0.43 180.0
12/5/2024 10:21 0.0001.82918.512 9.602 29.8202.712 0.207 3.907 0.0000.0000.242 0.000 0.0000.553 0.215 845.01.010.875 0.000 1.83 0.14 181.0
12/5/2024 10:22 0.0001.99818.491 9.596 28.3558.181 1.400 8.288 0.0000.0000.000 0.000 0.0000.633 0.226 845.01.020.854 0.000 2.00 0.22 180.0
12/5/2024 10:23 0.0002.46018.491 9.615 29.3049.922 1.477 8.907 0.0000.0000.000 0.000 0.0000.567 0.229 845.01.070.923 0.000 2.46 0.17 180.0
12/5/2024 10:24 0.0001.83118.449 9.579 30.1409.762 1.709 9.407 0.0000.0000.000 0.000 0.0000.592 0.229 845.01.090.944 0.000 1.83 0.02 180.0
12/5/2024 10:25 0.0001.15618.429 9.613 27.6437.192 1.983 10.029 0.0000.0000.000 0.000 0.0000.653 0.221 845.01.030.889 0.000 1.16 0.18 180.0
12/5/2024 10:26 0.0001.36818.472 9.540 27.0436.940 1.517 8.748 0.0000.0000.178 0.000 0.0000.641 0.191 845.00.980.898 0.000 1.37 0.02 180.0
12/5/2024 10:27 0.0001.73318.474 9.596 28.8261.545 0.779 5.455 0.0000.0000.000 0.000 0.0000.529 0.206 845.01.050.955 0.000 1.73 0.02 180.0
12/5/2024 10:28 0.0001.87618.463 9.565 32.0928.616 1.750 10.825 0.0000.0000.107 0.000 0.0000.695 0.218 845.00.990.826 0.000 1.88 0.16 180.0
12/5/2024 10:29 0.0000.65818.444 9.581 29.1837.951 1.991 10.540 0.0000.0000.180 0.000 0.0000.544 0.203 845.01.000.883 0.000 0.66 0.13 180.0
12/5/2024 10:30 0.0002.22618.398 9.613 33.8783.511 1.039 6.195 0.0000.0000.000 0.000 0.0000.590 0.226 845.00.950.745 0.000 2.23 0.17 180.0
12/5/2024 10:31 0.0003.03818.404 9.612 29.9405.775 1.910 8.937 0.0000.0000.000 0.000 0.0000.646 0.223 845.01.020.857 0.000 3.04 0.02 180.0
12/5/2024 10:33 0.0002.65618.372 9.561 31.02921.741 1.707 14.305 0.0570.0000.000 0.000 0.0000.515 0.222 845.01.090.971 0.000 2.66 0.17 180.0
12/5/2024 10:34 0.0001.68818.351 9.562 30.29424.540 2.388 18.522 0.0000.0000.197 0.000 0.0000.653 0.236 845.01.070.904 0.000 1.69 0.17 180.0
12/5/2024 10:35 0.0002.22218.318 9.632 26.14912.972 2.433 13.338 0.0000.0000.000 0.000 0.0000.691 0.208 845.00.950.806 0.000 2.22 0.15 180.0
12/5/2024 10:36 0.0001.84918.372 9.607 24.7922.416 0.650 5.064 0.0000.0000.117 0.000 0.0000.545 0.199 845.00.930.805 0.000 1.85 0.02 180.0
12/5/2024 10:37 0.0001.70318.355 9.573 25.1606.231 1.375 7.248 0.0000.0000.000 0.000 0.0000.682 0.192 845.00.960.860 0.000 1.70 0.16 179.0
12/5/2024 10:38 0.0002.15618.363 9.603 25.4845.059 1.146 5.681 0.0000.0000.018 0.000 0.0000.585 0.210 845.01.040.924 0.000 2.16 0.02 180.0
12/5/2024 10:39 0.0002.08318.411 9.562 15.3160.000 0.666 3.538 0.0000.0000.256 0.000 0.0000.528 0.164 845.00.900.861 0.000 2.08 5.07 180.0
12/5/2024 10:40 0.0002.73818.387 9.558 19.3380.258 0.000 2.732 0.0000.0000.087 0.000 0.0000.457 0.165 845.00.910.862 0.000 2.74 0.15 179.0
12/5/2024 10:41 0.0001.67318.420 9.596 25.1806.167 0.938 6.568 0.0000.0000.000 0.000 0.0000.544 0.197 845.00.930.810 0.000 1.67 0.17 180.0
12/5/2024 10:42 0.0001.60718.417 9.560 27.39216.105 1.069 9.604 0.0000.0000.000 0.000 0.0000.547 0.212 845.01.030.906 0.000 1.61 0.24 180.0
12/5/2024 10:43 0.0002.42818.415 9.594 27.95715.353 1.454 11.687 0.0000.0000.000 0.000 0.0000.562 0.222 845.01.010.848 0.000 2.43 0.02 180.0
12/5/2024 10:44 0.0002.38018.423 9.586 26.00716.631 1.446 12.460 0.0000.0000.000 0.000 0.0000.531 0.200 845.01.010.910 0.000 2.38 0.14 180.0
12/5/2024 10:45 0.0001.62918.418 9.557 26.50313.161 1.351 10.042 0.0000.0000.095 0.000 0.0000.584 0.204 845.00.970.838 0.000 1.63 0.18 180.0
12/5/2024 10:46 0.0002.44918.381 9.587 27.09416.506 1.510 10.372 0.0000.0000.000 0.000 0.0000.556 0.207 845.00.950.805 0.000 2.45 0.02 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/5/2024 10:47 0.0002.12718.377 9.574 26.8979.441 0.988 7.960 0.0000.0000.281 0.000 0.0000.474 0.208 845.00.990.863 0.000 2.13 0.23 180.0
0.0003.02518.095 9.450 26.7468.302 1.292 8.392 0.0150.0140.065 0.000 0.0030.574 0.216 845.001.0090.862 0.000 3.026 0.296 180.0Avg.
Spike 3
12/5/2024 10:49 0.00028.59216.644 9.192 27.49159.769 2.129 7.593 0.6060.0000.000 0.402 21.9630.440 0.382 845.023.761.144 0.868 28.59 0.20 180.0
Run 3 - B 30minute/60min
12/5/2024 10:51 0.0009.86217.898 9.521 27.12316.998 1.404 6.663 0.4720.0000.463 0.000 5.3590.603 0.411 845.06.820.952 0.190 9.86 0.16 180.0
12/5/2024 10:52 0.0001.94218.408 9.608 25.0000.854 1.189 5.650 0.0000.0000.515 0.000 0.0000.541 0.192 845.00.930.819 0.000 1.94 0.24 181.0
12/5/2024 10:53 0.0001.43218.310 9.580 32.5724.692 1.071 7.264 0.0000.0000.113 0.000 0.0000.571 0.198 845.00.970.867 0.000 1.43 0.02 179.0
12/5/2024 10:54 0.0002.37218.353 9.629 34.5199.481 1.935 11.028 0.0630.0000.085 0.000 0.0000.583 0.254 845.01.110.907 0.000 2.37 0.19 180.0
12/5/2024 10:55 0.0001.89118.392 9.608 30.1843.212 1.699 7.208 0.0000.0000.352 0.000 0.0000.621 0.196 845.01.000.916 0.000 1.89 0.19 180.0
12/5/2024 10:56 0.0001.13018.417 9.614 20.5470.000 0.635 3.288 0.0000.0000.592 0.000 0.0000.513 0.161 845.00.890.854 0.000 1.13 5.22 180.0
12/5/2024 10:57 0.0001.73018.392 9.623 26.3850.000 0.945 3.662 0.0000.0000.238 0.000 0.0000.563 0.192 845.00.870.727 0.000 1.73 0.18 180.0
12/5/2024 10:58 0.0002.74218.371 9.588 24.4550.000 1.121 4.275 0.0000.0000.534 0.000 0.0000.547 0.181 845.00.930.849 0.000 2.74 0.83 180.0
12/5/2024 10:59 0.0001.97318.376 9.572 22.0160.000 0.990 3.536 0.0000.0000.229 0.000 0.0000.555 0.159 845.00.790.709 0.000 1.97 5.69 180.0
12/5/2024 11:00 0.0001.63618.386 9.561 26.6360.876 0.071 2.864 0.0000.0000.880 0.000 0.0000.590 0.168 845.00.860.788 0.000 1.64 0.16 180.0
12/5/2024 11:01 0.0002.38918.392 9.614 27.6848.190 1.377 8.012 0.0000.0000.112 0.000 0.0000.557 0.187 845.00.930.834 0.000 2.39 0.15 180.0
12/5/2024 11:02 0.0002.14418.345 9.603 25.23812.012 1.581 10.095 0.0000.0000.000 0.000 0.0000.554 0.177 845.00.860.757 0.000 2.14 0.02 180.0
12/5/2024 11:03 0.0001.52118.409 9.575 22.3184.543 1.433 8.246 0.0000.0000.387 0.000 0.0000.525 0.147 845.00.900.903 0.000 1.52 0.14 180.0
12/5/2024 11:04 0.0001.79218.405 9.607 24.1376.628 1.271 7.546 0.0000.0000.233 0.000 0.0000.557 0.152 845.00.870.854 0.000 1.79 0.16 180.0
12/5/2024 11:05 0.0002.27818.386 9.593 25.81021.658 1.783 13.773 0.0000.0000.287 0.000 0.0000.628 0.162 845.00.900.858 0.000 2.28 0.18 180.0
12/5/2024 11:06 0.0001.67018.338 9.542 22.5277.334 0.883 7.414 0.0000.0000.719 0.000 0.0000.638 0.147 845.00.710.618 0.000 1.67 0.13 179.0
12/5/2024 11:07 0.4112.17418.367 9.617 22.4886.894 1.308 6.387 0.0000.0000.596 0.000 0.0000.566 0.145 845.00.850.838 0.000 2.58 0.01 180.0
12/5/2024 11:08 0.0001.65218.378 9.579 25.9292.781 0.529 4.402 0.0000.0000.736 0.000 0.0000.619 0.143 845.00.830.820 0.000 1.65 0.01 180.0
12/5/2024 11:09 0.0002.09518.380 9.598 30.73011.016 1.505 10.460 0.0880.0000.625 0.000 0.0000.632 0.170 845.00.890.829 0.000 2.10 0.13 180.0
12/5/2024 11:10 0.0002.10618.396 9.591 26.61714.938 1.445 10.798 0.0000.0000.664 0.000 0.0000.570 0.139 845.00.850.855 0.000 2.11 0.02 180.0
12/5/2024 11:11 0.0001.98718.350 9.592 36.49418.809 1.331 11.274 0.3200.0000.843 0.000 0.0000.631 0.140 845.00.870.887 0.000 1.99 0.02 180.0
12/5/2024 11:13 0.0001.04818.331 9.640 23.26713.335 2.426 14.584 0.0000.0000.440 0.000 0.0000.654 0.119 845.00.770.791 0.000 1.05 0.16 180.0
12/5/2024 11:14 0.0002.66618.401 9.599 12.0190.000 1.387 5.161 0.0000.0001.053 0.000 0.0000.655 0.060 845.00.610.728 0.000 2.67 2.09 181.0
12/5/2024 11:15 0.6180.00218.427 9.604 9.3710.000 0.000 1.985 0.0000.0000.944 0.000 0.0000.588 0.099 845.00.570.561 0.000 0.62 0.01 180.0
12/5/2024 11:16 0.4682.41018.434 9.647 15.8700.000 0.000 1.934 0.0000.0000.598 0.000 0.0000.681 0.120 845.00.660.627 0.000 2.88 0.01 180.0
12/5/2024 11:17 0.0001.55518.400 9.562 26.53514.440 0.724 5.857 0.0000.0000.546 0.000 0.0000.613 0.109 845.00.630.622 0.000 1.55 0.15 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/5/2024 11:18 0.0002.41418.412 9.589 24.3074.858 0.645 4.944 0.0000.0000.759 0.000 0.0000.676 0.108 845.00.620.612 0.000 2.41 0.15 180.0
12/5/2024 11:19 0.1192.90218.425 9.631 20.4197.933 1.476 8.601 0.0000.0000.938 0.000 0.0000.685 0.103 845.00.610.604 0.000 3.02 0.18 181.0
12/5/2024 11:20 0.0001.75318.436 9.593 23.9877.694 0.803 7.156 0.0000.0000.764 0.000 0.0000.763 0.125 845.00.670.626 0.000 1.75 0.19 180.0
12/5/2024 11:21 0.0002.69818.383 9.583 23.1979.881 1.890 11.375 0.0000.0000.880 0.000 0.0000.707 0.110 845.00.620.606 0.000 2.70 0.14 180.0
0.0542.19918.370 9.595 24.6136.969 1.162 7.181 0.0310.0000.538 0.000 0.1790.606 0.159 845.001.0130.774 0.006 2.252 0.564 180.0Avg.
0.0272.61218.233 9.523 25.6797.635 1.227 7.787 0.0230.0070.301 0.000 0.0910.590 0.187 845.001.0110.818 0.003 2.639 0.430 180.0Run 3 Avg:
Baseline 3
12/5/2024 11:23 0.0000.0000.043 0.000 0.3150.000 0.000 1.047 0.0000.0000.000 0.000 0.0000.180 0.000 845.00.460.695 0.000 0.00 0.13 180.0
Post CTS
12/5/2024 11:39 0.0000.0000.036 0.000 0.0000.000 0.000 0.764 0.0000.0000.000 97.573 0.0000.000 0.060 845.065.510.503 0.000 0.00 0.06 180.0
12/5/2024 11:39 0.0000.0000.033 0.000 0.0000.000 0.000 0.632 0.0000.0000.000 98.019 0.0000.000 0.027 845.065.880.710 0.000 0.00 0.06 180.0
12/5/2024 11:39 0.0000.0000.026 0.000 0.0000.000 0.000 0.610 0.0000.0000.000 98.319 0.0000.033 0.010 845.066.150.877 0.000 0.00 0.06 180.0
Post NO2/Mid O2
12/5/2024 11:42 95.6573.0850.010 0.000 0.3560.000 0.894 1.013 0.2010.0000.000 0.000 0.0000.233 0.007 846.00.010.000 0.000 98.74 11.15 180.0
12/5/2024 11:42 95.3542.7490.009 0.000 0.0000.000 0.911 0.892 0.0040.0000.000 0.000 0.0000.000 0.013 846.00.080.085 0.000 98.10 11.04 180.0
12/5/2024 11:42 95.6732.1790.010 0.000 0.0060.000 0.921 0.680 0.2390.0000.000 0.000 0.0000.013 0.026 847.00.050.000 0.000 97.85 11.09 180.0
12/5/2024 11:42 95.7822.3600.011 0.000 0.0000.000 0.898 0.733 0.0000.0000.000 0.000 0.0000.000 0.000 847.00.000.000 0.000 98.14 11.02 180.0
Post 5-Gas
12/5/2024 11:45 0.000240.5990.013 4.807 0.000509.307 2.006 1.237 9.9800.0681.236 1.430 253.9820.069 0.000 852.0256.872.900 10.263 240.60 0.02 180.0
12/5/2024 11:45 0.000239.9420.014 4.769 0.479510.034 2.065 1.592 3.8380.1511.258 1.117 254.8480.228 0.000 852.0257.853.385 10.319 239.94 0.36 180.0
12/5/2024 11:45 0.000242.8830.014 4.854 0.000510.660 1.851 1.000 16.6160.1401.185 2.042 252.2820.000 0.000 852.0256.544.339 10.217 242.88 0.02 180.0
12/5/2024 11:46 0.000240.7740.011 4.800 0.000509.542 2.014 1.536 11.9610.1130.992 1.502 253.5350.108 0.000 852.0256.763.337 10.265 240.77 0.23 180.0
12/5/2024 11:46 0.000239.7410.016 4.787 1.157509.155 2.131 1.466 4.2160.0791.402 1.334 254.0360.090 0.000 853.0257.393.697 10.274 239.74 0.02 180.0
12/5/2024 11:46 0.000241.7990.013 4.822 0.000508.273 2.027 1.496 13.5040.2060.506 1.916 252.4120.000 0.000 853.0255.793.148 10.193 241.80 0.16 180.0
12/5/2024 11:46 0.000241.3180.013 4.827 2.833510.826 2.100 1.499 11.4570.0650.523 1.538 253.1420.000 0.000 853.0256.283.166 10.253 241.32 0.21 180.0
12/5/2024 11:46 0.000241.2230.014 4.765 0.000508.593 1.751 1.305 4.4640.0531.566 1.371 253.6950.000 0.000 853.0257.364.134 10.276 241.22 0.15 180.0
End of Test Purge
12/5/2024 11:48 0.0000.0000.009 0.000 0.0000.000 0.000 0.586 0.2410.0040.000 0.000 0.0490.004 0.000 855.00.210.236 0.000 0.00 0.20 180.0
12/5/2024 11:49 0.0000.0000.006 0.000 0.0000.000 0.000 0.779 0.1510.0000.000 0.000 0.0000.008 0.000 855.00.210.318 0.000 0.00 0.00 180.0
12/5/2024 11:49 0.0000.0000.004 0.000 0.0000.000 0.000 0.795 0.2020.0010.000 0.000 0.0350.048 0.000 855.00.280.365 0.000 0.00 0.00 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/5/2024 11:49 0.0000.0000.006 0.000 0.0000.000 0.000 1.027 0.0540.0210.000 0.000 0.0000.037 0.000 855.00.190.280 0.000 0.00 0.00 180.0
12/5/2024 11:49 0.0000.0000.008 0.000 0.0000.000 0.000 0.504 0.2880.0020.182 0.000 0.0910.457 0.000 855.00.350.393 0.000 0.00 0.00 180.0
12/5/2024 11:49 0.0000.0000.008 0.000 0.4240.000 0.000 0.637 0.1510.0000.000 0.000 0.0000.000 0.000 855.00.230.344 0.000 0.00 0.14 180.0
12/5/2024 11:49 0.0000.0000.007 0.000 0.0000.000 0.000 0.976 0.1930.0110.000 0.000 0.0000.000 0.000 855.00.190.284 0.000 0.00 0.00 180.0
12/5/2024 11:49 0.0000.0000.011 0.000 0.0000.000 0.000 0.868 0.2140.0060.000 0.000 0.0040.000 0.000 856.00.210.311 0.000 0.00 0.17 180.0
12/5/2024 11:49 0.0000.0000.007 0.000 0.0000.000 0.000 0.734 0.3860.0000.000 0.000 0.0390.000 0.000 856.00.280.358 0.000 0.00 0.00 180.0
GAS, Inc.
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:01:18 PM 05:12 PM
Source:
Unit Number: 1526
Serial Number: 1673786
Engine Hours:3754
Permit #: #DAQE-AN161680001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Residue Booster Station
CO NOx NMNEHC
1.247 9.217 0.416
2.000 0.300 1.000 0.150 0.700 0.030
0.003 0.038 0.002
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results ppmvd
Results g/hp-hr
Permit g/hp-hr
PASS ALL
40 CFR Part 60 Subpart JJJJ
Performance Test Report
Test Type: Initial
Test Date: 12/4/2024
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS, Inc.
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Jason Wooly
3
Hunter Newton
Gas, Inc.
4.0 Test Summary
T
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Site Verification Photos
Gas, Inc.
Unit 1526 with a serial number of 1673786 which is a Waukesha 9394 GSI engine located at Residue
Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 12/4/2024 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2400 BHP and 1200 RPM which is 96.00% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1526 is authorized to
operate under permit #DAQE-AN161680001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Residue Booster StationLocation 1526Unit ID
Make Waukesha Site Elevation ft.5406
Model 9394 GSI Atmospheric Pressure psi.11.94
Serial Number 1673786 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2400 2400 2400 2400
1200 1199 1200 1200
Percent Load %
Intake Manifold Pressure (hg)
96.00%96.00%96.00%96.00%
65.00 66.00 67.00 66.00
Intake Manifold Temperature (F)120.00 119.00 120.00 119.67
Ambient Conditions
Ambient Temperature Dry (F)34.00 41.00 41.00 38.67
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
184661.96 185687.48 184801.21 185050.22
5229.00 5258.03 5232.94 5239.99
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.18 0.18 0.18 0.18
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %18.21%17.95%18.00%18.06%
T
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mfg. rated rpm
Test RPM
0.62%0.64%0.32%0.53%
Permitted Standards Results
5
Catalyst
0.0000.006
Run 1 Run 2 Run 3 3 Run Average Pass Permits
01:18 PM 02:28 PM 03:41 PM 12/4/2024
CO (g/hp-hr)0.003 0.0032.000 0.300 Pass
StateFederal
CO (ppmvw)1.077 1.926 0.065 1.022
CO (ppmvd)1.317 2.347 0.079 1.247
CO (mol wt) 28.01
CO (ppmvd) @15% O2 0.383 0.684 0.023 0.363 Fail
CO (ppbvd) @15% O2 383.087 683.573 22.551 363.070 Fail
NOx (g/hp-hr)0.039 0.039 0.037 0.0381.000 0.150 Pass
NOx (ppmvw)7.641 7.719 7.298 7.553
NOx (ppmvd)9.342 9.408 8.900 9.217
NOx (mol wt) 46.01
0.269 0.466 0.287 0.341NMNEHC (ppmvw)
0.329 0.568 0.350 0.416NMNEHC (ppmvd)
NOx (ppbvd) @15% O2 2717.894 2740.326 2551.617 2669.945 Fail
NOx (ppmvd) @15% O2 2.718 2.740 2.552 2.670 Fail
NMNEHC (mol wt) 44.10
95.683 165.435 100.344 120.487 FailNMNEHC (ppbvd) @15% O2
0.001 0.002 0.001 0.0020.700 0.030 PassNMNEHC (g/hp-hr)
0.096 0.165 0.100 0.120 FailNMNEHC (ppmvd) @15% O2
Gas, Inc.
5.0 Run Summaries
Summary Source Run 1
R
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Table 5.1 Run Summaries
S
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0.00Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
1.08
0.00
7.64
0.00
0.01
0.00
7.64
0.28
0.27
0.13%
0.52%
0.00%
18.21%
NMNEHC
0.46 7.33 0.01 7.34 0.30 0.47%18.24%
47.56 25.29 0.97 26.26 22.64 0.18%16.71%
1.69 7.94 0.00 7.94 0.24 0.56%18.18%
0.00 0.00 0.00 0.00 0.42 0.18%0.05%
Avg. Wet
NO2NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.00 0.00 0.42 0.18%0.05%
1.19 7.25 0.00 7.25 0.41 0.63%17.90%
38.44 28.48 0.61 29.09 23.35 0.01%16.34%
2.66 8.04 0.15 8.19 0.53 0.45%18.01%
0.00 0.00 0.00 0.00 0.44 0.13%0.03%
Avg. Wet 1.93 7.64 0.08 7.72 0.47 0.54%17.95%
NO2NO
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.09 6.19 0.07 6.26 0.39 0.42%18.01%
58.37 29.40 0.00 29.40 22.08 0.01%16.29%
0.04 8.34 0.00 8.34 0.19 0.11%18.00%
0.00 0.00 0.00 0.00 0.41 0.01%0.05%
0.00 0.00 0.00 0.00 0.44 0.13%0.03%
Avg. Wet 0.06 7.27 0.04 7.30 0.29 0.26%18.00%
NO2NO
Gas, Inc.
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Stack diameter =
Table 6.1. Data used for volumetric flow rate (Method 2)
20 inches or:1.67 feet. or:2.18 Square Feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.58
Yes
20.00
10.00
16.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
ppmd
%d
%d
%d 18.21
29.52
0.57
Inches
3.34
10
16.66
Vo
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F
l
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Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
9.36
0.52
1.08
843.95
0.04
24.93
24.97
935.25
1394.92
501.81
27.42
91.01
198.54
225775.72
184661.96
Run 2
17.95
29.50
0.57
9.22
0.54
1.93
843.30
0.04
24.91
24.95
936.06
1395.73
502.26
27.43
91.35
199.29
226319.81
185687.48
Run 3
18.00
29.49
0.56
9.24
0.27
0.06
843.53
0.04
24.91
24.96
930.25
1389.92
499.03
27.42
90.57
197.58
225378.32
184801.21
18.06
29.50
0.57
9.27
0.44
1.02
843.59
0.04
24.92
24.96
933.85
1393.52
501.03
27.42
90.97
198.47
225825.69
185050.98
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.55
Exhaust Temp F
935.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.57
0.56
0.54
934.00
932.00
933.00
0.58
0.59
0.57
937.00
938.00
937.00
0.53
0.54
0.55
938.00
939.00
933.00
0.56 934.00
0.59
0.59
0.60
932.00
935.00
936.00
0.61
0.55
0.57
937.00
934.00
935.25
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.57
Exhaust Temp F
930.00
0.57
0.56
0.57
933.00
928.00
927.00
0.55
0.58
0.59
929.00
931.00
930.00
0.55
0.53
0.56
928.00
929.00
933.00
0.59 934.00
0.57
0.54
0.56
932.00
930.00
931.00
0.55
0.58
928.00
931.00
930.250.56
Run 2
Δpstd (in) H2O
0.57
Exhaust Temp F
936.00
0.55
0.54
0.57
937.00
938.00
939.00
0.56
0.58
0.55
933.00
934.00
936.00
0.59
0.60
0.57
935.00
937.00
936.00
0.55 938.00
0.58
0.59
0.61
937.00
935.00
936.00
0.58
0.55
933.00
937.00
0.57 936.06
Pass
Strat Check
33.150Check 1
33.984Check 2
33.830Check 3
MethaneGas Used
Pass/Fail
7
Gas, Inc.
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(.094)+.32(.006)+.28(.9+0) = 29.518 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.518(1 -.1821)+.18.0(.1821) = 27.421 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.57*√(1394.92/(24.97*27.421)) = 91.01 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.182)91.006*2.182((528*24.97)/ (1394.92*29.92)) = 184661.96 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 184661.96/35.315 = 5228.995 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 1.317*(20.9-15)/(20.9-.6%)) = .383 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(1.317*(1.164*10^-3)*5228.995*(Run Time/60))/2400 = .003 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .003*1/453.6*2400 = .018 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .018*4.38 = .079 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
1.32 = 1.077*(1/(1-.18))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
Gas, Inc.
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.81%
21.01%
10.87%
10.91%
10.62%
10.62%
10.91%10.87%
10.81%
21.01%
10.62%
21.05%
10.62%
21.05%
10.62%21.05%
0.00%
10.62%
21.05%
0.19%
0.04%
0.92%
0.18%
10.62%
Span
Zero Offset 0.00%
21.05
0.00%
10.81%0.29%0.46%0.00%
0.64%
0.66%
0.33%
0.62%
0.64%
0.32%
9
Gas, Inc.
0.0 0.0 0.0
0.0 0.0 0.0
1090.0 1090.0 1090.0
1071.0 1069.0 1069.7
8.0 8.0 8
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Residue Booster Station
12/4/2024
5406
1526
Waukesha
Model
Serial Number
9394 GSI
1673786
Technician Hunter Newton
Run Start Times 01:18 PM 02:28 PM 03:41 PM 05:12 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1199.0 1200.0 1199.7
Engine Hours 3751 3752 3753 3754
Intake Manifold Pressure (psi)65.0 66.0 67.0 66.0
Intake Manifold Temp °F 120.0 119.0 120.0 119.7
Engine Load (BHP)2400.0 2400.0 2400.0 2400.0
Ambient Temp °F 34.0 41.0 41.0 38.7
Humidity %60.0 41.0 41.0 47.3
Dew Point °F 21.0 19.0 19.0 19.7
Waukesha
YesCatalyst (Yes or No)
AFR Manufacturer/Type Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1090.0
1069.0
8.0Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
Gas, Inc.
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
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Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.43
Average:Oxygen 0.11
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 97.23
Tolerance 2.00%
Difference between measured and expected 1.07%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.26
Average:Oxygen 0.09
Pre-test System Zero Time:
Mechanical Response Time 58 seconds
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 96.73
Tolerance 5.00%
Difference between measured and expected 1.58%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 252.50
Value:Spike Expected 252.40
System (Equilibration) Response Time Target (Spike)
53 secondsSystem Zero Response Time
58 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC506322 9/17/2027 99.95 10.62%
EB0020295 6/20/2032 98.28
EB0090574 11/27/2031 21.05%
Cylinder # ALM-063647 Expiration: 5-03-2032
Propane CO NO SF6
Bottle Value 252.40 501.70 237.50 10.20
Analyzer System Response 252.50 500.85 236.64 10.15
Percent Difference 0.04%0.17%0.36%0.47%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 97.233 4.947
Spike Direct
Propane 254.684
Mechanical
Response Time
SF6 10.210
CO 508.291
NO 239.111
Ethylene 96.728 58 seconds
Analyzer
Response
Propane 252.495
SF6 10.152
CO 500.850
NO 236.640
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.633
CO 502.273
NO 236.905
44 seconds
53 seconds
7.52%
7.69%
7.38%
114.43%
115.15%
113.85%
10.144
12
Gas, Inc.
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
Gas, Inc.
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
10
16
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
185050.98
H2O%d @ Sampling Point:18.06
CO2%d @ Sampling Point:9.27
Pressure @ Sampling Point (Pg "H2O):0.57
Temperature @ Sampling Point (Deg F):933.85
Gas, Inc.
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 98.28 97.23 4.947 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 97.233 4.947
Spike Direct
Propane 254.684
Mechanical
Response Time
SF6 10.210
CO 508.291
NO 239.111
Ethylene 96.728 58 seconds
Analyzer
Response
Propane 252.495
SF6 10.152
CO 500.850
NO 236.640
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 252.633
CO 502.273
NO 236.905
44 seconds
53 seconds
7.52%
7.69%
7.38%
114.43%
115.15%
113.85%
10.144
Gas, Inc.
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
252.400
10.200
501.700
237.500
254.684
10.210
508.291
239.111
0.90%
0.10%
1.31%
0.68%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.000
0.000
Spike Average
21.720
0.768
Dilution Factor
7.522%
Expected
18.980
% Recovery
114.430%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.785
Dilution Factor
7.689%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.753
Dilution Factor
7.375%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 21.207 18.627 113.850%
0.001120
0.001825
0.001394
0.000 22.350 19.410 115.150%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass4.63%
16
Gas, Inc.
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-17.6417408 Pass
Line Position Difference:Resolution Difference to Reference 4.63%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
98.28
97.07
1.24%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
Gas, Inc.
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Residue Booster Station; 1526; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
12/4/2024
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
12/4/2024
Hunter Newton
Gas, Inc.
Appendices
Gas, Inc.
Gas, Inc.
Spike (5 Gas)
Gas, Inc.
9% O2/NO2
Gas, Inc.
Ethylene Only
Gas, Inc.
BIP
Gas, Inc.
21% O2
Tri Probe Certification
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3/3/2022
Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS, Inc.
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
Gas, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Residue Booster Station
Unit Number:1526
Make:Waukesha
Location:9394 GSIModel:
1673786Serial Number:
RAW Result Data
Stability
12/4/2024 06:50 5.1575.243-0.027 0.079 0.00034.157 0.000 0.000 0.0000.0070.000 12.176 1.5250.008 0.000 858.09.850.305 0.301 10.40 0.16 180.0
Pre Test Baseline Direct
12/4/2024 06:59 0.0000.000-0.000 0.000 0.2710.000 0.000 1.205 0.0000.0000.459 0.000 0.0000.011 0.000 856.00.450.672 0.000 0.00 0.17 180.0
12/4/2024 07:00 0.0000.000-0.001 0.000 0.2050.000 0.000 1.274 0.0000.0820.256 0.000 0.0000.047 0.000 855.00.420.636 0.000 0.00 0.17 180.0
12/4/2024 07:00 0.0000.000-0.002 0.000 0.6050.000 0.000 1.369 0.0000.0290.122 0.000 0.0000.000 0.000 855.00.430.645 0.000 0.00 0.00 180.0
CTS Direct
12/4/2024 07:05 0.0000.0000.006 0.000 0.2080.000 0.000 0.215 0.0000.0000.000 96.788 0.0000.000 0.000 849.064.920.583 0.000 0.00 0.06 180.0
12/4/2024 07:06 0.0000.0000.006 0.000 0.1040.000 0.000 0.213 0.0000.0000.000 97.497 0.0000.000 0.000 848.065.390.577 0.000 0.00 0.06 181.0
12/4/2024 07:06 0.0000.0000.006 0.000 0.2030.000 0.000 0.179 0.0000.0000.000 97.413 0.0000.000 0.000 847.065.340.597 0.000 0.00 0.06 180.0
High O2 Direct
12/4/2024 07:09 0.0000.0000.000 0.000 0.0000.000 0.000 1.319 0.0000.0090.000 0.000 0.0000.069 0.000 845.00.440.653 0.000 0.00 21.16 180.0
12/4/2024 07:10 0.0000.000-0.004 0.000 0.0000.000 0.000 1.581 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.520.785 0.000 0.00 20.94 180.0
12/4/2024 07:10 0.0000.000-0.007 0.000 0.0000.000 0.000 1.528 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.470.697 0.000 0.00 20.94 180.0
NO2/Mid O2 Direct
12/4/2024 07:18 99.3530.000-0.004 0.000 0.0450.000 0.577 1.150 0.4980.0000.627 0.000 0.0000.000 0.000 845.00.000.000 0.000 99.35 10.80 180.0
12/4/2024 07:18 99.7100.000-0.002 0.000 0.0000.000 0.462 1.073 0.4950.0000.062 0.000 0.0000.000 0.000 845.00.000.000 0.000 99.71 10.78 180.0
12/4/2024 07:18 100.0870.000-0.004 0.000 0.0000.000 0.571 1.216 0.4650.0000.358 0.000 0.0000.000 0.000 845.00.000.000 0.000 100.09 10.86 180.0
Spike Direct
12/4/2024 07:28 0.000239.121-0.003 4.777 5.487508.704 2.271 1.524 8.9780.3080.000 1.366 254.9140.000 0.000 844.0257.652.734 10.221 239.12 0.19 180.0
12/4/2024 07:28 0.000239.2070.003 4.769 5.276508.864 2.291 1.535 8.9140.2070.060 1.396 254.8560.014 0.000 844.0257.572.676 10.210 239.21 0.02 180.0
12/4/2024 07:29 0.000239.0040.000 4.757 5.353507.305 2.301 1.446 9.3050.2420.000 1.394 254.2810.000 0.000 845.0257.122.859 10.198 239.00 0.02 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
12/4/2024 07:31 0.0000.0000.026 0.000 0.0000.000 0.000 2.041 0.0000.0000.963 0.000 0.0000.000 0.058 845.00.270.227 0.000 0.00 0.13 180.0
12/4/2024 07:31 0.0000.0000.017 0.000 0.3220.000 0.000 1.905 0.0000.0050.477 0.000 0.0000.000 0.000 845.00.260.385 0.000 0.00 0.13 180.0
12/4/2024 07:31 0.0000.0000.013 0.000 0.5700.000 0.000 1.953 0.0000.0000.573 0.000 0.0000.025 0.000 845.00.250.378 0.000 0.00 0.00 180.0
CTS System with Response Time
12/4/2024 07:33 0.0000.0000.020 0.000 0.0110.000 0.000 0.588 0.0000.0000.000 96.566 0.0000.000 0.000 845.064.670.429 0.000 0.00 0.18 180.0
12/4/2024 07:34 0.0000.0000.021 0.000 0.0590.000 0.000 0.494 0.0000.0000.000 96.602 0.0000.000 0.000 845.064.700.447 0.000 0.00 0.06 180.0
12/4/2024 07:34 0.0000.0000.020 0.000 0.0420.000 0.000 0.588 0.0000.0000.000 97.015 0.0000.000 0.000 845.064.980.455 0.000 0.00 0.19 180.0
NO2/Mid O2 System with Response Time
12/4/2024 07:40 97.9010.0000.008 0.000 0.0000.000 0.643 1.744 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.120.180 0.000 97.90 10.89 180.0
12/4/2024 07:41 99.8180.0000.008 0.000 0.0000.000 0.652 1.809 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.170.251 0.000 99.82 10.82 180.0
12/4/2024 07:41 99.4920.0000.006 0.000 0.0000.000 0.650 1.700 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.180.268 0.000 99.49 10.91 180.0
Spike System with Response Time
12/4/2024 07:43 0.000236.4840.012 4.774 4.130499.794 2.327 1.499 10.0990.1381.014 1.389 252.1450.033 0.000 845.0254.912.763 10.139 236.48 0.38 180.0
12/4/2024 07:43 0.000236.7340.011 4.762 3.840501.112 2.293 1.573 9.9790.1120.741 1.391 252.5850.000 0.000 845.0255.372.792 10.156 236.73 0.20 180.0
12/4/2024 07:44 0.000236.7020.011 4.773 3.919501.644 2.283 1.532 9.9430.0850.897 1.362 252.7560.000 0.000 845.0255.532.799 10.160 236.70 0.02 180.0
Baseline System with Response Time
12/4/2024 07:46 0.0000.0000.005 0.000 0.0000.000 0.000 1.461 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.240.355 0.000 0.00 0.13 180.0
12/4/2024 07:47 0.0000.0000.005 0.000 0.3200.000 0.000 1.505 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.270.403 0.000 0.00 0.12 180.0
12/4/2024 07:47 0.0000.0000.004 0.000 0.2990.000 0.000 1.600 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.320.487 0.000 0.00 0.14 180.0
Run 1 - A 30minute/60min
12/4/2024 13:19 0.00018.75818.179 9.383 19.6970.000 0.743 2.838 0.3280.0001.763 0.000 0.0000.133 0.046 844.00.340.376 0.000 18.76 0.20 180.0
12/4/2024 13:20 0.0003.15518.308 9.338 23.1110.000 1.166 2.878 0.2750.0002.650 0.000 0.0000.307 0.041 844.00.400.481 0.000 3.15 0.16 180.0
12/4/2024 13:21 0.0002.59518.320 9.212 28.2620.000 0.551 2.972 0.4950.0002.761 0.000 0.0000.213 0.000 844.00.160.245 0.000 2.60 1.64 181.0
12/4/2024 13:22 0.0004.36518.201 9.394 54.7270.000 1.934 4.879 1.4400.0003.408 0.000 0.0000.331 0.000 844.00.320.485 0.000 4.36 0.02 180.0
12/4/2024 13:23 0.00021.82718.209 9.391 22.7610.000 2.835 4.781 0.5050.0002.198 0.000 0.0000.277 0.000 844.00.190.278 0.000 21.83 0.18 180.0
12/4/2024 13:24 0.0005.37018.248 9.348 19.6110.000 0.456 2.786 0.3030.0002.166 0.000 0.0000.197 0.025 844.00.190.216 0.000 5.37 0.02 180.0
12/4/2024 13:25 0.0002.51418.210 9.362 26.3920.000 0.837 2.748 0.4480.0002.210 0.000 0.0000.270 0.046 844.00.410.478 0.000 2.51 0.20 180.0
12/4/2024 13:26 0.0004.27618.199 9.380 55.2277.387 2.445 5.844 1.5680.0002.425 0.000 0.0000.339 0.000 844.00.340.515 0.000 4.28 0.02 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 13:27 0.0006.04318.216 9.350 52.6473.694 2.455 7.034 1.3990.0003.055 0.000 0.0000.256 0.000 844.00.270.405 0.000 6.04 0.15 180.0
12/4/2024 13:28 0.00022.94718.206 9.389 31.8940.000 3.349 6.808 0.9280.0002.691 0.000 0.0000.235 0.012 844.00.210.286 0.000 22.95 0.04 180.0
12/4/2024 13:29 0.0006.37118.173 9.423 30.0030.000 0.925 3.745 0.5910.0001.595 0.000 0.0000.189 0.088 844.00.510.498 0.000 6.37 0.02 180.0
12/4/2024 13:30 0.0000.00018.196 9.368 37.7720.000 2.016 4.405 0.7750.0002.535 0.000 0.0000.162 0.000 844.00.200.297 0.000 0.00 0.02 180.0
12/4/2024 13:31 0.00027.03118.235 9.400 15.1350.000 2.029 3.210 0.1820.0001.960 0.000 0.0000.113 0.029 844.00.190.201 0.000 27.03 0.03 180.0
12/4/2024 13:32 0.00017.79318.208 9.373 28.0650.000 1.344 3.060 0.6640.0002.066 0.000 0.0000.180 0.096 844.00.520.497 0.000 17.79 2.90 179.0
12/4/2024 13:33 0.4144.28918.246 9.403 33.7650.000 2.453 4.475 0.6700.0002.592 0.000 0.0000.169 0.039 844.00.290.321 0.000 4.70 0.17 180.0
12/4/2024 13:34 0.0002.99618.235 9.398 39.7590.000 1.258 3.479 0.8240.0002.446 0.000 0.0000.184 0.036 844.00.310.350 0.000 3.00 0.02 180.0
12/4/2024 13:35 0.0006.89418.255 9.351 32.8650.000 2.206 4.670 0.8590.0002.717 0.000 0.0000.230 0.010 844.00.230.312 0.000 6.89 0.15 180.0
12/4/2024 13:36 0.0001.20718.192 9.359 30.1760.000 0.414 3.119 0.6720.0001.579 0.000 0.0000.141 0.004 844.00.220.325 0.000 1.21 5.54 179.0
12/4/2024 13:37 0.0000.00018.264 9.415 28.3150.000 1.309 3.050 0.5870.0001.846 0.000 0.0000.286 0.088 844.00.470.437 0.000 0.00 0.15 180.0
12/4/2024 13:38 0.00023.17418.248 9.320 20.7980.000 1.850 2.731 0.3510.0002.106 0.000 0.0000.168 0.031 844.00.190.198 0.000 23.17 0.16 179.0
12/4/2024 13:39 0.00010.83318.261 9.358 6.9090.000 0.241 2.264 0.0420.0000.904 0.000 0.0000.177 0.008 844.00.090.108 0.000 10.83 0.01 180.0
12/4/2024 13:40 0.0000.01518.267 9.356 19.7500.000 0.474 2.283 0.2270.0001.428 0.000 0.0000.193 0.043 844.00.310.339 0.000 0.02 0.46 180.0
12/4/2024 13:41 0.0000.00018.278 9.332 34.1760.000 0.977 2.940 0.6030.0002.104 0.000 0.0000.180 0.075 844.00.440.439 0.000 0.00 0.81 180.0
12/4/2024 13:42 0.0000.00018.277 9.351 23.2530.000 0.507 2.729 0.3800.0001.706 0.000 0.0000.309 0.047 844.00.400.455 0.000 0.00 0.02 180.0
12/4/2024 13:43 0.0003.84618.253 9.321 41.3460.000 1.207 3.295 0.8410.0001.960 0.000 0.0000.278 0.016 844.00.280.368 0.000 3.85 0.16 180.0
12/4/2024 13:44 0.0000.74518.261 9.339 41.7190.000 2.068 4.377 0.8880.0002.195 0.000 0.0000.198 0.017 844.00.270.348 0.000 0.75 0.15 180.0
12/4/2024 13:45 0.0004.43118.254 9.350 33.1500.000 1.082 3.457 0.5980.0001.609 0.000 0.0000.213 0.085 844.00.520.533 0.000 4.43 0.19 180.0
12/4/2024 13:46 0.0004.94118.224 9.307 61.8762.844 1.632 5.251 1.9270.0002.646 0.000 0.0000.345 0.019 844.00.310.402 0.000 4.94 0.13 179.0
12/4/2024 13:47 0.0008.67418.278 9.352 26.9560.000 1.923 4.333 0.6120.0002.040 0.000 0.0000.199 0.003 844.00.190.273 0.000 8.67 0.22 180.0
12/4/2024 13:49 0.0004.71418.296 9.390 35.4350.000 1.210 3.856 0.8660.0001.846 0.000 0.0000.209 0.028 844.00.280.334 0.000 4.71 0.26 180.0
0.0147.32718.240 9.360 31.8520.464 1.463 3.810 0.6950.0002.174 0.000 0.0000.223 0.031 844.000.3020.360 0.000 7.340 0.473 179.9Avg.
Spike 1
12/4/2024 13:53 0.97025.28816.706 9.102 47.90647.556 2.729 3.043 1.5150.0001.606 0.000 21.7200.161 0.288 844.022.640.517 0.768 26.26 0.18 180.0
Run 1 - B 30minute/60min
12/4/2024 13:55 0.0004.30218.198 9.340 50.9432.823 2.385 6.855 1.3170.0002.525 0.000 0.0000.261 0.025 844.00.250.306 0.000 4.30 0.20 180.0
12/4/2024 13:56 0.0003.25018.161 9.333 52.4481.864 2.082 5.810 1.3790.0002.414 0.000 0.0000.292 0.016 844.00.280.366 0.000 3.25 0.14 180.0
12/4/2024 13:57 0.0003.36518.201 9.312 57.8451.735 2.101 7.147 1.6180.0003.065 0.000 0.0000.220 0.014 844.00.260.354 0.000 3.36 0.54 180.0
12/4/2024 13:58 0.0004.28718.170 9.364 44.5970.000 1.812 5.533 0.9990.0002.318 0.000 0.0000.194 0.000 844.00.250.378 0.000 4.29 0.19 180.0
12/4/2024 13:59 0.0003.49018.141 9.419 43.7543.334 2.161 5.514 0.9910.0001.822 0.000 0.0000.293 0.037 844.00.250.268 0.000 3.49 0.03 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 14:00 0.0000.82318.178 9.374 40.2520.000 1.482 4.284 0.8610.0002.490 0.000 0.0000.216 0.009 844.00.250.346 0.000 0.82 0.03 180.0
12/4/2024 14:01 0.0001.19518.128 9.327 32.5210.000 1.201 3.636 0.5620.0002.285 0.000 0.0000.200 0.000 844.00.220.333 0.000 1.19 0.17 179.0
12/4/2024 14:02 0.0003.60018.180 9.410 57.4180.000 1.905 4.814 1.7020.0002.125 0.000 0.0000.348 0.024 844.00.270.332 0.000 3.60 4.62 180.0
12/4/2024 14:03 0.0004.58218.139 9.349 33.9840.000 1.915 4.421 0.5950.0002.149 0.000 0.0000.237 0.000 844.00.210.313 0.000 4.58 0.04 180.0
12/4/2024 14:04 0.0005.23918.166 9.363 25.9290.000 1.650 3.883 0.4080.0002.278 0.000 0.0000.172 0.038 844.00.290.323 0.000 5.24 0.18 180.0
12/4/2024 14:05 0.00011.45218.152 9.339 9.2840.000 0.554 2.539 0.0570.0001.387 0.000 0.0000.174 0.001 844.00.040.050 0.000 11.45 0.16 179.0
12/4/2024 14:06 0.0002.86218.140 9.379 40.7620.000 1.465 3.505 0.8510.0002.003 0.000 0.0000.269 0.006 844.00.230.326 0.000 2.86 0.14 180.0
12/4/2024 14:07 0.0003.92918.188 9.343 45.5131.743 2.549 4.771 1.0200.0002.759 0.000 0.0000.235 0.000 844.00.300.446 0.000 3.93 0.03 180.0
12/4/2024 14:08 0.000129.95818.196 9.314 7.8180.000 5.852 2.892 0.0000.0001.529 0.000 0.0000.291 0.000 844.00.120.180 0.000 129.96 0.03 180.0
12/4/2024 14:09 0.00016.39818.201 9.370 9.1430.000 0.986 2.213 0.0440.0001.247 0.000 0.0000.207 0.005 844.00.090.118 0.000 16.40 0.15 180.0
12/4/2024 14:10 0.0004.49018.246 9.347 44.7362.642 1.861 4.198 1.2040.0002.554 0.000 0.0000.327 0.007 844.00.270.388 0.000 4.49 2.45 180.0
12/4/2024 14:11 0.0004.76118.230 9.354 64.09117.115 2.361 8.013 2.0430.0003.100 0.000 0.0000.239 0.000 844.00.300.451 0.000 4.76 0.16 180.0
12/4/2024 14:12 0.0006.56018.129 9.376 61.78319.435 2.706 9.865 1.8190.0002.898 0.000 0.0000.356 0.002 844.00.190.279 0.000 6.56 0.26 180.0
12/4/2024 14:13 0.0001.72518.190 9.373 40.8530.000 2.664 6.525 0.7210.0002.933 0.000 0.0000.275 0.000 844.00.210.313 0.000 1.73 0.16 180.0
12/4/2024 14:14 0.0002.67418.138 9.353 35.7080.000 1.626 4.858 0.7020.0002.308 0.000 0.0000.230 0.000 844.00.250.375 0.000 2.67 0.03 180.0
12/4/2024 14:15 0.0000.00018.178 9.359 17.7640.000 0.527 3.015 0.1890.0001.941 0.000 0.0000.139 0.000 844.00.150.223 0.000 0.00 0.19 181.0
12/4/2024 14:16 0.0000.00018.160 9.357 29.9770.000 1.410 2.899 0.3380.0002.657 0.000 0.0000.218 0.032 844.00.270.312 0.000 0.00 0.80 180.0
12/4/2024 14:17 0.0000.01018.173 9.405 33.0280.000 1.329 3.070 0.4970.0002.246 0.000 0.0000.280 0.000 844.00.230.349 0.000 0.01 5.42 180.0
12/4/2024 14:18 0.00010.47118.196 9.347 16.5710.000 1.659 2.914 0.0120.0002.303 0.000 0.0000.237 0.000 844.00.090.139 0.000 10.47 0.19 180.0
12/4/2024 14:19 0.0000.00018.195 9.354 28.5880.000 1.033 2.614 0.3940.0002.373 0.000 0.0000.197 0.052 844.00.340.346 0.000 0.00 0.13 180.0
12/4/2024 14:20 0.0007.43918.180 9.365 43.8480.000 2.653 5.121 1.0180.0002.817 0.000 0.0000.357 0.000 844.00.240.356 0.000 7.44 0.02 180.0
12/4/2024 14:21 0.0000.00018.195 9.343 28.5820.000 0.948 3.116 0.3560.0002.538 0.000 0.0000.264 0.044 844.00.350.385 0.000 0.00 0.16 180.0
12/4/2024 14:22 0.0001.08218.223 9.381 47.1540.000 1.963 4.298 1.0730.0002.922 0.000 0.0000.331 0.000 843.00.240.366 0.000 1.08 0.14 180.0
12/4/2024 14:23 0.0000.00018.206 9.354 28.4510.000 1.219 3.472 0.3650.0002.877 0.000 0.0000.237 0.063 843.00.430.458 0.000 0.00 0.23 180.0
12/4/2024 14:24 0.0000.33818.218 9.391 36.1750.000 2.159 3.657 0.6410.0002.486 0.000 0.0000.288 0.000 843.00.210.313 0.000 0.34 0.02 180.0
0.0007.94318.180 9.360 36.9841.690 1.874 4.515 0.7930.0002.378 0.000 0.0000.253 0.013 843.900.2360.316 0.000 7.942 0.567 180.0Avg.
0.0077.63518.210 9.360 34.4181.077 1.669 4.162 0.7440.0002.276 0.000 0.0000.238 0.022 843.950.2690.338 0.000 7.641 0.520 179.9Run 1 Avg:
Baseline 1
12/4/2024 14:26 0.0000.0000.048 0.000 0.5690.000 0.000 1.855 0.0000.0000.000 0.000 0.0000.000 0.000 843.00.420.628 0.000 0.00 0.18 180.0
Run 2 - A 30minute/60min
12/4/2024 14:29 0.0005.32518.098 9.323 43.9751.741 1.750 5.259 0.8030.0002.813 0.000 0.0000.231 0.007 843.00.270.378 0.000 5.32 0.02 181.0
12/4/2024 14:30 0.0002.46618.134 9.295 37.9020.000 1.980 5.097 0.6000.0003.011 0.000 0.0000.210 0.000 843.00.170.248 0.000 2.47 0.03 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 14:31 0.0001.04218.203 9.362 33.4780.000 1.015 3.687 0.5090.0002.382 0.000 0.0000.146 0.020 843.00.150.168 0.000 1.04 0.48 180.0
12/4/2024 14:32 0.0000.00018.219 9.345 31.5130.000 1.022 3.567 0.4900.0002.308 0.000 0.0000.259 0.075 843.00.430.422 0.000 0.00 0.02 180.0
12/4/2024 14:33 0.00014.63318.114 9.279 17.9270.000 1.570 3.220 0.1940.0002.231 0.000 0.0000.232 0.036 843.00.230.235 0.000 14.63 0.16 180.0
12/4/2024 14:34 0.0000.00018.177 9.318 18.9840.000 0.290 2.557 0.1330.0001.900 0.000 0.0000.207 0.043 843.00.330.369 0.000 0.00 0.25 180.0
12/4/2024 14:35 0.0005.85417.719 9.126 37.4120.000 2.154 3.762 0.3750.0000.728 0.000 0.0000.225 0.079 843.00.540.565 0.000 5.85 2.00 180.0
12/4/2024 14:36 0.0005.74117.747 9.093 24.8100.000 1.818 3.769 0.0610.0001.235 0.000 0.0000.164 0.077 843.00.450.439 0.000 5.74 0.15 180.0
12/4/2024 14:37 0.00020.60817.778 9.100 10.8040.000 1.835 2.634 0.0080.0000.751 0.000 0.0000.268 0.037 843.00.220.222 0.000 20.61 0.25 180.0
12/4/2024 14:38 0.0000.40417.754 9.104 23.8450.000 0.722 2.355 0.3260.0000.745 0.000 0.0000.310 0.068 844.00.420.433 0.000 0.40 0.01 180.0
12/4/2024 14:39 0.0003.12617.772 9.108 49.1290.000 2.054 4.362 0.9350.0001.947 0.000 0.0000.296 0.063 844.00.480.530 0.000 3.13 3.22 180.0
12/4/2024 14:41 0.00046.61117.763 9.108 6.4230.000 2.630 2.927 0.0000.0000.719 0.000 0.0000.173 0.001 844.00.100.140 0.000 46.61 0.28 180.0
12/4/2024 14:42 0.0001.60217.804 9.129 22.9320.000 1.370 2.480 0.1830.0001.256 0.000 0.0000.147 0.043 844.00.330.370 0.000 1.60 0.31 181.0
12/4/2024 14:43 0.0002.60017.735 9.070 20.3670.000 1.452 2.544 0.1500.0001.106 0.000 0.0000.203 0.030 844.00.240.271 0.000 2.60 0.27 179.0
12/4/2024 14:44 0.0004.43717.772 9.140 46.8670.000 2.265 3.905 0.8030.0001.415 0.000 0.0000.246 0.080 844.00.560.592 0.000 4.44 6.12 180.0
12/4/2024 14:45 0.0006.09917.766 9.107 65.3462.338 3.029 7.244 1.7260.0002.382 0.000 0.0000.377 0.071 844.00.540.593 0.000 6.10 0.03 180.0
12/4/2024 14:46 0.0007.40717.760 9.134 65.23612.403 3.119 9.407 1.8080.0002.152 0.000 0.0000.280 0.106 844.00.630.626 0.000 7.41 0.15 180.0
12/4/2024 14:47 0.00011.98117.828 9.209 47.75410.442 3.779 10.137 1.1650.0001.789 0.000 0.0000.235 0.074 844.00.550.600 0.000 11.98 0.23 180.0
12/4/2024 14:48 0.0007.59917.879 9.216 55.6870.000 2.745 6.690 1.2400.0001.933 0.000 0.0000.298 0.077 844.00.650.739 0.000 7.60 3.29 180.0
12/4/2024 14:49 0.0009.74017.847 9.243 55.5268.676 3.652 8.872 1.2760.0001.882 0.000 0.0000.247 0.096 844.00.600.619 0.000 9.74 0.04 180.0
12/4/2024 14:50 0.0007.44217.879 9.228 36.7570.000 2.430 5.378 0.7510.0001.858 0.000 0.0000.204 0.046 844.00.480.581 0.000 7.44 0.19 180.0
12/4/2024 14:51 0.0005.15817.888 9.248 28.9910.000 1.402 3.489 0.5370.0001.211 0.000 0.0000.240 0.045 844.00.420.500 0.000 5.16 0.02 180.0
12/4/2024 14:52 0.0002.72117.871 9.274 42.2640.000 2.099 4.256 0.7430.0001.519 0.000 0.0000.296 0.061 843.00.540.627 0.000 2.72 0.14 180.0
12/4/2024 14:53 0.0002.98717.868 9.197 26.0050.000 1.282 3.203 0.3220.0001.543 0.000 0.0000.250 0.056 843.00.460.521 0.000 2.99 0.19 179.0
12/4/2024 14:54 0.0004.31217.904 9.263 40.3640.000 2.077 3.856 0.7640.0001.150 0.000 0.0000.228 0.057 844.00.510.595 0.000 4.31 0.02 180.0
12/4/2024 14:55 0.0003.83417.946 9.256 37.9680.000 1.859 3.549 0.6600.0001.613 0.000 0.0000.198 0.025 843.00.300.378 0.000 3.83 0.03 180.0
12/4/2024 14:56 0.0003.47817.933 9.255 29.9350.000 1.409 3.175 0.4240.0001.200 0.000 0.0000.225 0.071 844.00.480.508 0.000 3.48 0.15 180.0
12/4/2024 14:57 0.0004.81217.917 9.236 37.0030.000 2.152 3.523 0.6450.0001.722 0.000 0.0000.221 0.039 844.00.310.356 0.000 4.81 0.15 180.0
12/4/2024 14:58 0.00020.67317.931 9.225 24.3300.000 1.471 2.883 0.3500.0001.275 0.000 0.0000.246 0.052 844.00.430.490 0.000 20.67 0.55 180.0
12/4/2024 14:59 0.0004.74717.946 9.250 40.6510.000 2.248 3.970 0.6940.0001.982 0.000 0.0000.254 0.035 844.00.330.382 0.000 4.75 0.20 180.0
0.0007.24817.898 9.208 35.3401.187 1.956 4.392 0.6230.0001.659 0.000 0.0000.237 0.052 843.600.4050.450 0.000 7.248 0.632 180.0Avg.
Spike 2
12/4/2024 15:03 0.60528.48216.338 8.923 19.81538.440 1.967 1.451 0.5330.0001.940 0.000 22.3500.092 0.262 843.023.350.720 0.785 29.09 0.01 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
12/4/2024 15:05 0.00010.52117.815 9.280 29.7660.000 1.871 2.065 1.2540.0001.089 0.000 0.7660.068 0.292 843.01.750.596 0.000 10.52 0.54 180.0
12/4/2024 15:06 0.3474.45517.998 9.204 35.0400.000 1.877 3.014 0.2960.0001.693 0.000 0.0000.270 0.050 843.00.460.543 0.000 4.80 0.14 180.0
12/4/2024 15:08 0.1896.21918.006 9.212 50.4280.000 2.355 4.737 0.8180.0001.755 0.000 0.0000.316 0.059 843.00.540.638 0.000 6.41 0.14 180.0
12/4/2024 15:09 0.1895.22718.006 9.253 35.8320.000 2.061 3.789 0.3710.0001.584 0.000 0.0000.313 0.067 843.00.500.546 0.000 5.42 0.14 180.0
12/4/2024 15:10 0.0004.15218.031 9.250 39.1600.000 1.468 3.396 0.7570.0001.236 0.000 0.0000.226 0.049 843.00.460.549 0.000 4.15 0.02 180.0
12/4/2024 15:11 0.0003.59218.027 9.257 47.8890.000 2.218 4.467 0.7390.0001.938 0.000 0.0000.354 0.088 843.00.580.600 0.000 3.59 0.03 180.0
12/4/2024 15:12 0.0764.60817.985 9.215 41.3110.000 2.264 4.550 0.6790.0001.544 0.000 0.0000.278 0.062 843.00.480.528 0.000 4.68 0.03 179.0
12/4/2024 15:13 0.3582.93618.046 9.232 31.7030.000 1.224 3.071 0.3000.0000.957 0.000 0.0000.200 0.059 843.00.440.481 0.000 3.29 0.17 180.0
12/4/2024 15:14 0.38121.78218.033 9.249 25.1020.000 2.761 3.438 0.3570.0001.375 0.000 0.0000.334 0.047 843.00.320.344 0.000 22.16 0.02 180.0
12/4/2024 15:15 0.0009.85818.034 9.214 18.5780.000 1.092 2.289 0.0230.0000.629 0.000 0.0000.189 0.076 843.00.410.385 0.000 9.86 0.17 180.0
12/4/2024 15:16 0.3596.75218.013 9.214 34.2720.000 1.767 2.573 0.2660.0001.583 0.000 0.0000.273 0.073 843.00.520.560 0.000 7.11 0.14 180.0
12/4/2024 15:17 0.2705.68718.010 9.245 41.0120.000 1.937 3.015 0.5210.0001.413 0.000 0.0000.281 0.076 843.00.520.547 0.000 5.96 3.41 180.0
12/4/2024 15:18 0.2985.65318.040 9.214 34.4090.000 2.409 3.868 0.3290.0001.466 0.000 0.0000.264 0.064 843.00.510.566 0.000 5.95 0.23 180.0
12/4/2024 15:19 0.3814.30618.037 9.218 30.6700.000 1.286 2.548 0.2230.0001.060 0.000 0.0000.278 0.043 843.00.420.495 0.000 4.69 0.17 180.0
12/4/2024 15:20 0.00012.29518.020 9.217 24.1920.000 2.357 3.152 0.1240.0001.194 0.000 0.0000.287 0.091 843.00.510.491 0.000 12.30 0.20 180.0
12/4/2024 15:21 0.00023.36618.028 9.202 12.8160.000 1.253 2.173 0.0000.0000.567 0.000 0.0000.184 0.059 843.00.360.363 0.000 23.37 0.02 180.0
12/4/2024 15:22 0.1987.40218.033 9.211 39.0710.000 1.844 3.044 0.5760.0000.782 0.000 0.0000.255 0.059 843.00.510.591 0.000 7.60 0.93 180.0
12/4/2024 15:23 0.0418.77018.048 9.211 61.42617.042 2.957 7.291 1.6180.0001.870 0.000 0.0000.401 0.082 843.00.590.640 0.000 8.81 0.03 180.0
12/4/2024 15:24 0.2394.23318.064 9.228 33.3090.000 2.025 3.719 0.3190.0001.297 0.000 0.0000.269 0.065 843.00.450.481 0.000 4.47 0.25 180.0
12/4/2024 15:25 0.2676.91918.043 9.223 32.2870.000 1.140 2.886 0.5200.0000.458 0.000 0.0000.232 0.052 843.00.390.433 0.000 7.19 0.83 180.0
12/4/2024 15:26 0.5477.50518.063 9.232 30.8760.000 2.451 3.670 0.3310.0001.101 0.000 0.0000.242 0.056 843.00.420.468 0.000 8.05 0.16 180.0
12/4/2024 15:27 0.0004.80118.030 9.204 26.1170.000 1.438 2.901 0.4920.0000.805 0.000 0.0000.199 0.076 843.00.480.492 0.000 4.80 0.02 180.0
12/4/2024 15:28 0.0006.35518.006 9.192 66.06129.471 1.995 8.268 1.9280.0001.091 0.000 0.0000.216 0.108 843.00.620.615 0.000 6.35 1.69 180.0
12/4/2024 15:29 0.0009.78817.989 9.234 57.93716.566 3.189 9.873 1.4270.0001.191 0.000 0.0000.293 0.105 843.00.560.522 0.000 9.79 0.04 180.0
12/4/2024 15:30 0.00010.08217.978 9.250 54.98810.225 3.428 9.828 1.4580.0001.396 0.000 0.0000.241 0.097 843.00.550.540 0.000 10.08 0.04 180.0
12/4/2024 15:31 0.0006.71518.019 9.230 33.3610.000 1.877 4.531 0.6880.0001.076 0.000 0.0000.174 0.054 843.00.460.528 0.000 6.71 0.04 180.0
12/4/2024 15:32 0.0006.08417.973 9.257 49.3992.084 2.501 5.884 1.0010.0000.528 0.000 0.0000.288 0.088 843.00.600.630 0.000 6.08 3.10 180.0
12/4/2024 15:33 0.0396.63317.956 9.275 45.2664.538 2.301 5.688 0.7180.0000.831 0.000 0.0000.223 0.081 843.00.510.520 0.000 6.67 0.65 180.0
12/4/2024 15:34 0.3724.24817.953 9.253 33.8300.000 1.818 4.535 0.4840.0000.827 0.000 0.0000.210 0.047 843.00.500.613 0.000 4.62 0.03 180.0
12/4/2024 15:35 0.00020.20717.976 9.264 11.9380.000 1.829 2.723 0.0000.0000.316 0.000 0.0000.234 0.060 843.00.380.391 0.000 20.21 0.17 180.0
0.1528.03818.009 9.231 36.9352.664 2.033 4.233 0.6210.0001.155 0.000 0.0260.253 0.076 843.000.5270.523 0.000 8.190 0.452 180.0Avg.
0.0767.64317.954 9.220 36.1371.925 1.995 4.312 0.6220.0001.407 0.000 0.0130.245 0.064 843.300.4660.487 0.000 7.719 0.542 180.0Run 2 Avg:
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
12/4/2024 15:38 0.0000.0000.029 0.000 0.6210.000 0.000 1.818 0.0000.0000.000 0.000 0.0000.000 0.000 843.00.440.656 0.000 0.00 0.13 180.0
Run 3 - A 30minute/60min
12/4/2024 15:41 0.43913.93617.783 9.142 23.9930.000 2.182 3.657 0.1380.0000.947 0.000 0.0000.181 0.092 843.00.490.458 0.000 14.37 0.16 179.0
12/4/2024 15:42 0.00018.16617.882 9.221 13.5660.000 1.807 2.618 0.1730.0000.193 0.000 0.0000.179 0.049 843.00.340.368 0.000 18.17 0.02 180.0
12/4/2024 15:43 0.0002.21917.934 9.201 20.4930.000 1.430 2.313 0.0920.0000.523 0.000 0.0000.159 0.049 843.00.360.400 0.000 2.22 0.13 180.0
12/4/2024 15:44 0.0003.66617.978 9.240 19.5030.000 1.441 2.224 0.1700.0000.493 0.000 0.0000.221 0.037 843.00.240.241 0.000 3.67 0.01 180.0
12/4/2024 15:45 0.0934.52118.008 9.247 35.4730.000 2.161 2.965 0.3980.0000.948 0.000 0.0000.336 0.049 843.00.490.588 0.000 4.61 0.16 180.0
12/4/2024 15:46 0.0002.44518.097 9.218 36.9240.000 2.017 3.539 0.5590.0001.251 0.000 0.0000.130 0.032 843.00.250.282 0.000 2.44 0.02 181.0
12/4/2024 15:48 0.0005.98118.064 9.249 43.4300.000 2.745 5.203 0.9900.0001.400 0.000 0.0000.285 0.034 843.00.260.290 0.000 5.98 0.17 180.0
12/4/2024 15:49 0.3171.80718.090 9.265 32.1120.000 1.774 3.368 0.1620.0000.898 0.000 0.0000.254 0.075 843.00.480.500 0.000 2.12 0.03 181.0
12/4/2024 15:50 0.0006.83618.058 9.234 18.7620.000 1.521 2.724 0.2550.0001.002 0.000 0.0000.103 0.031 843.00.250.289 0.000 6.84 0.16 180.0
12/4/2024 15:51 0.0006.71818.059 9.257 20.1960.000 1.439 2.375 0.1170.0000.395 0.000 0.0000.195 0.029 843.00.140.129 0.000 6.72 0.01 180.0
12/4/2024 15:52 0.2236.86318.039 9.218 36.0050.000 2.007 3.865 0.4480.0001.316 0.000 0.0000.252 0.049 843.00.470.560 0.000 7.09 0.17 180.0
12/4/2024 15:53 0.1194.75118.006 9.256 37.8190.000 2.489 4.231 0.4620.0000.984 0.000 0.0000.150 0.059 843.00.450.493 0.000 4.87 0.18 180.0
12/4/2024 15:54 0.2835.33618.013 9.246 34.0560.000 1.582 3.393 0.3660.0000.598 0.000 0.0000.297 0.039 843.00.230.230 0.000 5.62 0.03 180.0
12/4/2024 15:55 0.0006.76318.006 9.238 40.0330.000 2.914 5.169 0.6740.0001.452 0.000 0.0000.281 0.039 843.00.310.355 0.000 6.76 0.17 180.0
12/4/2024 15:56 0.0000.48018.022 9.250 22.2590.000 1.234 2.816 0.0830.0000.521 0.000 0.0000.270 0.052 843.00.390.423 0.000 0.48 0.15 180.0
12/4/2024 15:57 0.00015.77618.047 9.243 20.3990.000 2.029 2.844 0.2460.0000.733 0.000 0.0000.188 0.050 843.00.410.467 0.000 15.78 0.01 180.0
12/4/2024 15:58 0.0003.28318.036 9.211 25.4400.000 1.547 2.439 0.1930.0000.883 0.000 0.0000.250 0.046 843.00.320.345 0.000 3.28 0.12 179.0
12/4/2024 15:59 0.0004.69718.060 9.259 23.3950.000 1.847 2.584 0.1130.0000.795 0.000 0.0000.250 0.063 843.00.390.394 0.000 4.70 0.17 180.0
12/4/2024 16:00 0.00017.92018.059 9.220 9.1000.000 1.588 2.176 0.0000.0000.227 0.000 0.0000.275 0.007 843.00.110.147 0.000 17.92 0.13 180.0
12/4/2024 16:01 0.0003.13118.036 9.204 28.4160.000 1.404 2.314 0.3530.0000.786 0.000 0.0000.220 0.061 843.00.360.355 0.000 3.13 0.01 180.0
12/4/2024 16:02 0.0560.54818.016 9.218 32.4420.000 1.436 2.374 0.2370.0001.018 0.000 0.0000.352 0.047 843.00.430.500 0.000 0.60 0.13 180.0
12/4/2024 16:03 0.1817.42218.001 9.241 51.8130.000 3.028 4.981 0.8930.0001.170 0.000 0.0000.361 0.079 844.00.550.591 0.000 7.60 2.19 180.0
12/4/2024 16:04 0.0927.02318.042 9.222 39.9510.000 3.171 5.474 0.7500.0001.355 0.000 0.0000.329 0.048 843.00.400.456 0.000 7.12 0.03 180.0
12/4/2024 16:05 0.0002.01417.999 9.194 32.8040.000 1.741 3.155 0.4980.0000.857 0.000 0.0000.293 0.076 843.00.480.485 0.000 2.01 0.15 179.0
12/4/2024 16:06 0.0573.22118.067 9.241 58.8180.000 2.515 5.018 1.4060.0001.649 0.000 0.0000.264 0.048 843.00.470.562 0.000 3.28 0.02 180.0
12/4/2024 16:07 0.0007.12618.009 9.228 56.8041.195 3.436 7.069 1.2410.0001.493 0.000 0.0000.321 0.083 843.00.520.535 0.000 7.13 1.96 180.0
12/4/2024 16:08 0.0007.99317.949 9.259 53.2460.000 2.980 5.919 1.1100.0001.306 0.000 0.0000.294 0.082 843.00.550.578 0.000 7.99 5.62 180.0
12/4/2024 16:09 0.0006.67218.013 9.274 52.4541.400 3.404 7.238 1.2680.0001.498 0.000 0.0000.425 0.079 843.00.560.608 0.000 6.67 0.17 180.0
12/4/2024 16:10 0.1176.77817.995 9.278 42.3020.000 2.893 5.806 0.5610.0001.026 0.000 0.0000.249 0.061 843.00.490.557 0.000 6.90 0.17 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 16:11 0.2371.51017.989 9.255 31.7600.000 2.137 3.814 0.2790.0001.204 0.000 0.0000.200 0.067 844.00.430.439 0.000 1.75 0.19 180.0
0.0746.18718.012 9.234 33.1260.087 2.130 3.789 0.4750.0000.964 0.000 0.0000.252 0.054 843.070.3870.421 0.000 6.261 0.421 180.0Avg.
Spike 3
12/4/2024 16:13 0.00029.40216.293 8.949 48.80058.369 2.312 4.472 1.5940.0001.765 0.000 21.2070.171 0.367 844.022.080.207 0.753 29.40 0.01 180.0
Run 3 - B 30minute/60min
12/4/2024 16:16 0.0009.87417.933 9.262 10.4110.000 1.378 3.393 0.1280.0000.718 0.000 0.0000.174 0.029 844.00.180.180 0.000 9.87 0.03 180.0
12/4/2024 16:17 0.0003.08117.945 9.277 36.6770.000 1.478 3.126 0.6760.0000.434 0.000 0.0000.230 0.023 844.00.200.231 0.000 3.08 0.01 180.0
12/4/2024 16:18 0.00021.61317.948 9.287 12.2790.000 2.143 2.568 0.0290.0000.374 0.000 0.0000.155 0.009 844.00.120.159 0.000 21.61 0.15 180.0
12/4/2024 16:19 0.00039.20817.972 9.191 6.2830.000 1.943 2.110 0.0000.0000.549 0.000 0.0000.250 0.000 844.00.140.214 0.000 39.21 0.01 180.0
12/4/2024 16:20 0.0004.68417.971 9.255 32.1460.000 1.237 2.639 0.5240.0000.475 0.000 0.0000.293 0.011 844.00.250.340 0.000 4.68 0.00 180.0
12/4/2024 16:21 0.0003.84417.913 9.259 33.3680.000 2.157 3.637 0.5670.0000.893 0.000 0.0000.214 0.012 844.00.270.365 0.000 3.84 0.02 180.0
12/4/2024 16:22 0.0003.42617.973 9.236 31.0290.000 2.122 3.336 0.3330.0001.227 0.000 0.0000.182 0.035 844.00.180.159 0.000 3.43 0.02 180.0
12/4/2024 16:23 0.0002.16517.926 9.200 15.8430.000 1.122 2.284 0.0660.0000.528 0.000 0.0000.151 0.012 844.00.200.266 0.000 2.17 0.21 179.0
12/4/2024 16:24 0.0009.00917.996 9.240 15.5780.000 1.403 2.077 0.0000.0000.719 0.000 0.0000.202 0.000 844.00.120.177 0.000 9.01 0.01 180.0
12/4/2024 16:25 0.0004.61718.003 9.257 41.6370.000 1.986 2.792 0.8000.0000.889 0.000 0.0000.225 0.006 844.00.180.258 0.000 4.62 0.23 180.0
12/4/2024 16:27 0.0005.80417.991 9.249 47.7191.250 2.847 4.554 1.0060.0001.773 0.000 0.0000.287 0.021 844.00.250.312 0.000 5.80 0.15 180.0
12/4/2024 16:28 0.0003.72518.002 9.213 29.6020.000 1.909 3.330 0.2280.0001.363 0.000 0.0000.179 0.022 844.00.190.213 0.000 3.72 0.20 180.0
12/4/2024 16:29 0.0001.17918.008 9.251 37.4250.000 1.617 2.937 0.5230.0001.741 0.000 0.0000.315 0.000 844.00.230.346 0.000 1.18 0.21 179.0
12/4/2024 16:30 0.0006.35218.028 9.289 20.6020.000 2.012 2.972 0.0720.0001.041 0.000 0.0000.331 0.005 844.00.120.168 0.000 6.35 0.19 180.0
12/4/2024 16:31 0.0009.86818.045 9.248 19.3120.000 1.329 2.218 0.0530.0001.295 0.000 0.0000.137 0.000 844.00.120.183 0.000 9.87 0.18 180.0
12/4/2024 16:32 0.0003.43718.015 9.251 39.4310.000 1.735 2.825 0.5890.0001.503 0.000 0.0000.289 0.000 844.00.220.326 0.000 3.44 0.01 180.0
12/4/2024 16:33 0.0001.53117.986 9.244 25.6560.000 1.712 2.662 0.2660.0001.427 0.000 0.0000.232 0.041 844.00.360.423 0.000 1.53 0.16 180.0
12/4/2024 16:34 0.0002.82217.984 9.261 44.7870.000 2.173 3.669 0.8770.0001.869 0.000 0.0000.271 0.008 844.00.210.295 0.000 2.82 0.19 180.0
12/4/2024 16:35 0.0002.13217.962 9.248 34.4030.000 2.403 3.596 0.4730.0001.726 0.000 0.0000.278 0.000 844.00.180.277 0.000 2.13 0.14 180.0
12/4/2024 16:36 0.00017.42918.029 9.235 8.6730.000 1.479 2.358 0.0000.0001.252 0.000 0.0000.200 0.000 844.00.120.178 0.000 17.43 0.02 180.0
12/4/2024 16:37 0.00033.96117.964 9.183 6.2130.000 1.715 1.921 0.0000.0001.008 0.000 0.0000.218 0.000 844.00.070.108 0.000 33.96 0.01 179.0
12/4/2024 16:38 0.0002.37917.967 9.213 25.2950.000 1.285 1.956 0.4780.0001.374 0.000 0.0000.365 0.000 844.00.200.299 0.000 2.38 0.15 180.0
12/4/2024 16:39 0.0005.51618.002 9.234 42.4550.000 2.334 3.504 0.7390.0001.695 0.000 0.0000.307 0.012 844.00.180.238 0.000 5.52 0.16 180.0
12/4/2024 16:40 0.0001.11518.014 9.223 37.7970.000 2.094 3.509 0.4260.0001.962 0.000 0.0000.343 0.000 844.00.230.352 0.000 1.11 0.19 180.0
12/4/2024 16:41 0.0004.58718.059 9.227 17.1950.000 1.247 2.396 0.0350.0001.458 0.000 0.0000.141 0.000 844.00.130.198 0.000 4.59 0.17 180.0
12/4/2024 16:42 0.00029.74318.086 9.247 6.0400.000 1.676 2.012 0.0000.0001.094 0.000 0.0000.190 0.000 844.00.110.164 0.000 29.74 0.01 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 16:43 0.0002.61018.052 9.222 20.0360.000 0.961 1.899 0.0860.0001.471 0.000 0.0000.242 0.007 844.00.060.065 0.000 2.61 0.18 180.0
12/4/2024 16:44 0.0002.75218.025 9.198 41.7710.000 1.811 3.036 0.6900.0002.097 0.000 0.0000.273 0.000 844.00.280.420 0.000 2.75 0.01 179.0
12/4/2024 16:45 0.0004.61318.051 9.269 42.1630.000 1.770 3.315 0.7000.0001.644 0.000 0.0000.320 0.012 844.00.200.261 0.000 4.61 0.45 180.0
12/4/2024 16:46 0.0006.98618.042 9.281 50.4060.000 2.572 5.270 1.1080.0001.878 0.000 0.0000.398 0.027 844.00.320.396 0.000 6.99 0.03 180.0
0.0008.33517.996 9.242 27.7410.042 1.788 2.930 0.3820.0001.249 0.000 0.0000.246 0.010 844.000.1870.252 0.000 8.335 0.117 179.9Avg.
0.0377.26118.004 9.238 30.4330.064 1.959 3.359 0.4280.0001.107 0.000 0.0000.249 0.032 843.530.2870.337 0.000 7.298 0.269 179.9Run 3 Avg:
Baseline 3
12/4/2024 16:48 0.0000.0000.045 0.000 0.5530.000 0.000 1.801 0.0000.0000.000 0.000 0.0000.000 0.000 844.00.410.619 0.000 0.00 0.01 180.0
Post CTS
12/4/2024 17:07 0.0000.0000.121 0.000 0.0480.000 0.000 0.833 0.0000.0000.000 96.698 0.0000.000 0.055 844.064.940.546 0.000 0.00 0.20 180.0
12/4/2024 17:07 0.0000.0000.088 0.000 0.0000.000 0.000 1.081 0.0000.0000.000 97.303 0.0000.000 0.000 844.065.130.381 0.000 0.00 0.18 180.0
12/4/2024 17:07 0.0000.0000.076 0.000 0.0000.000 0.000 0.772 0.0000.0000.000 97.215 0.0000.000 0.000 844.065.110.443 0.000 0.00 0.06 180.0
Post NO2/Mid O2
12/4/2024 17:09 96.5520.0000.027 0.000 0.0000.000 0.637 1.829 0.0000.0000.000 0.000 0.0000.000 0.055 845.00.580.713 0.000 96.55 10.80 180.0
12/4/2024 17:09 94.7580.0000.022 0.000 0.0000.000 0.608 2.096 0.0000.0030.000 0.000 0.0000.000 0.146 845.01.191.343 0.000 94.76 10.94 180.0
12/4/2024 17:10 98.3600.0000.020 0.000 0.0000.000 0.634 1.919 0.0000.0000.000 0.000 0.0000.106 0.000 845.00.370.557 0.000 98.36 10.92 180.0
12/4/2024 17:10 98.0210.0000.024 0.000 0.0000.000 0.618 1.964 0.0000.0000.000 0.000 0.0000.055 0.000 845.00.270.399 0.000 98.02 10.98 180.0
Post 5-Gas
12/4/2024 17:11 0.000236.9240.025 4.707 0.000505.766 2.269 1.623 3.7720.1171.542 1.414 252.2850.000 0.000 849.0255.142.863 10.124 236.92 0.29 180.0
12/4/2024 17:12 0.000237.0580.021 4.723 0.000501.802 2.006 1.576 4.9020.1481.365 1.435 251.5620.000 0.000 849.0255.454.403 10.153 237.06 0.22 180.0
12/4/2024 17:12 0.000236.3660.021 4.734 1.621499.384 2.188 1.402 5.5750.0750.968 1.373 252.8900.000 0.000 849.0256.323.771 10.148 236.37 0.26 180.0
12/4/2024 17:12 0.000236.8960.024 4.737 0.706498.159 2.224 1.610 4.6330.1020.923 1.449 253.3460.000 0.000 849.0256.483.246 10.140 236.90 0.14 180.0
12/4/2024 17:12 0.000237.9230.024 4.751 1.698506.741 2.430 1.492 4.5750.1090.884 1.556 252.1230.000 0.000 849.0254.992.747 10.117 237.92 0.19 180.0
12/4/2024 17:12 0.000237.0580.020 4.726 0.633502.733 2.130 1.659 4.9620.0801.064 1.238 253.7300.000 0.000 849.0257.143.883 10.183 237.06 0.17 180.0
12/4/2024 17:12 0.000235.5960.017 4.738 5.542499.928 2.421 1.630 5.5210.0751.656 1.181 252.9860.000 0.000 850.0255.702.897 10.161 235.60 0.18 180.0
12/4/2024 17:12 0.000237.4150.020 4.743 2.510503.673 2.347 1.533 5.0470.1121.510 1.557 252.1400.000 0.000 850.0255.453.402 10.128 237.42 0.02 180.0
End of Test Purge
12/4/2024 17:15 0.0000.0000.017 0.000 0.0120.000 0.000 1.586 0.1080.0000.127 0.000 0.2800.000 0.001 853.00.580.447 0.000 0.00 0.12 180.0
12/4/2024 17:15 0.0000.0000.013 0.000 0.0000.000 0.000 1.669 0.4990.0000.000 0.000 0.1120.000 0.000 853.00.320.306 0.000 0.00 0.18 180.0
12/4/2024 17:15 0.0000.0000.018 0.000 0.0000.000 0.000 1.634 0.0000.0000.000 0.000 0.0000.000 0.000 853.00.100.143 0.000 0.00 0.12 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 17:15 0.0000.0000.010 0.000 0.0000.000 0.000 1.601 0.0620.0050.000 0.000 0.0000.000 0.000 853.00.190.280 0.000 0.00 0.17 180.0
12/4/2024 17:15 0.0000.0000.015 0.000 0.0000.000 0.000 1.847 0.1520.0000.000 0.000 0.0000.152 0.000 853.00.360.545 0.000 0.00 0.00 180.0
12/4/2024 17:15 0.0000.0000.017 0.000 0.0000.000 0.000 1.754 0.1270.0000.332 0.000 0.0000.015 0.000 853.00.240.362 0.000 0.00 0.00 180.0
12/4/2024 17:15 0.0000.0000.011 0.000 0.0000.000 0.000 1.996 0.5830.0000.000 0.000 0.0820.000 0.000 854.00.240.230 0.000 0.00 0.12 180.0
12/4/2024 17:15 0.0000.0000.011 0.000 0.0550.000 0.000 1.993 0.2200.0190.000 0.000 0.0000.000 0.000 854.00.080.118 0.000 0.00 0.15 180.0
GAS, Inc.
Waukesha 9394 GSI
Rich Burn (4 Cycle)
303 W. 3rd St Elk City , OK 73644(580) 225-0403
Test Started:Test Completed:08:46 AM 12:26 PM
Source:
Unit Number: 1527
Serial Number: 1673793
Engine Hours:3731
Permit #: #DAQE-AN161680001-23
Location:
Duchesne County, Utah
Prepared on Behalf of:
Crusoe Energy Systems, Inc.
Residue Booster Station
CO NOx NMNEHC
14.640 8.323 1.349
2.000 0.300 1.000 0.150 0.700 0.030
0.041 0.038 0.006
Pass Pass Pass Pass Pass Pass
Federal State Federal State Federal State
Results ppmvd
Results g/hp-hr
Permit g/hp-hr
PASS ALL
40 CFR Part 60 Subpart JJJJ
Performance Test Report
Test Type: Initial
Test Date: 12/4/2024
Index
Tables
Figures
Appendices
Table 5.1 (Run Summaries)................................................................
Table 6.1 (Volumetric Flow Rate Data)...............................................
Table 6.2 (Stack Gas Measurements).................................................
Table 8.1 (Oxygen Calibration)...........................................................
Annex Table 1.2.1 (Certified Calibration Bottle Concentrations).........
Annex Table 1.2.2 (Measurement System Capabilities).....................
Annex Table 1.3.1 (Test Specific Target Analytes).............................
Annex Table 4.1 (Measure System Capabilities)................................
Figure 6.1 (Location of Traverse Points per Method 1).......................
Annex Figure 1.4.1 (Sampling Train)..................................................
Annex Figure 1.4.2 (Sampling Points).................................................
Annex Figure 1.4.3 (Sampling Port Locations)....................................
Certified Calibration Bottle Certificates................................................
Tri Probe Certification via GD-031......................................................
GAS ALT 141_FTIR EPA....................................................................
Tester Qualifications (resume)............................................................
Raw Data............................................................................................
27
Key Personnel.............................................................................1.0 3
Sampling System........................................................................2.0 3
Methods Used.............................................................................3.0 3
Test Summaries..........................................................................4.0 5
Run Summaries..........................................................................5.0 6
6
Volumetric Flow Rate Data.........................................................6.0 7
7
7
7
Calculations................................................................................7.0 8
9
12
12
13
15
13
14
14
20
25
28
29
Oxygen Calibration.....................................................................9
Engine Parameter Data Sheet....................................................10
QA/QC Results............................................................................11
Signature Page...........................................................................12.0
Appendices.................................................................................13.0
Bottle Certs.................................................................................2014.0
Tri Probe Certification via GD-031..............................................2515.0
GAS ALT 141_FTIR EPA............................................................16.0
Tester Qualifications (resume)....................................................2817.0
D6348 Annexes..........................................................................1211.0
18
19
26
8.0
9.0
10.0
Raw Data....................................................................................2918.0
1.0 Key Personnel
GAS, Inc.
Crusoe Energy Systems, Inc.
2.0 Sampling System
The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning
system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet
Personal Sampling System with a Zirconium Oxide oxygen sensor.
3.0 Methods Used
This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target
analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is
potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific.
The analytes, detection levels, and data quality objectives are expected to change for any particular testing
situation. It is the responsibility of the tester to define the target analytes, the associated detection limits for
those analytes in the particular source effluent, and the required data quality objectives for each specific
test program. Provisions are included in this test method that require the tester to determine critical
sampling system and instrument operational parameters, and for the conduct of QA/QC procedures.
Testers following this test method will generate data that will allow an independent observer to verify the
valid collection, identification, and quantification of the subject target analytes.
EPA Method 1 & 1A
EPA Method 2 & 2C
EPA Method 3A
The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at
which sampling for air pollutants will be performed pursuant to regulations set forth in this part.
This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas
stream. The average gas velocity in a stack is determined from the gas density and from measurement of
the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16
separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated
utilizing the formulas seen in section 7.0 of this report.
This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions
using a continuous instrumental analyzer. Quality assurance and quality control requirements are included
to assure that the tester collects data of known quality. Documentation to these specific requirements for
equipment, supplies, sample collection and analysis, calculations, and data analysis will be included.
ASTM D6348-03
Jason Wooly
3
Hunter Newton
Gas, Inc.
4.0 Test Summary
T
e
s
t
S
u
m
m
a
r
y
Site Verification Photos
Gas, Inc.
Unit 1527 with a serial number of 1673793 which is a Waukesha 9394 GSI engine located at Residue
Booster Station and operated by Crusoe Energy Systems, Inc. was tested for emissions of: Carbon
Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 12/4/2024 by
Hunter Newton with Great Plains Analytical Services, Inc. All quality assurance and quality control tests
were within acceptable tolerances.
The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at
1200 RPM. The engine was operating at 2133 BHP and 866 RPM which is 85.33% of maximum engine
load during the test. The test HP calculation can be found on page 8. The engine was running at the
maximum load available at the test site.
This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Unit 1527 is authorized to
operate under permit #DAQE-AN161680001-23.
4
4.0 Test Summary
Engine/Compressor Specs
Residue Booster StationLocation 1527Unit ID
Make Waukesha Site Elevation ft.5406
Model 9394 GSI Atmospheric Pressure psi.11.91
Serial Number 1673793 Stack Diameter in.20
mfg. rated hp 2500 Yes
1200 Date of Manufacture
Engine/Compressor Operation Run 2 Run 3 3 Run AveragesRun 1
Test Horsepower 2125 2150 2125 2133
1200 1200 199 866
Percent Load %
Intake Manifold Pressure (hg)
85.00%86.00%85.00%85.33%
60.00 60.00 58.00 59.33
Intake Manifold Temperature (F)113.00 115.00 115.00 114.33
Ambient Conditions
Ambient Temperature Dry (F)41.00 24.00 34.00 33.00
Exhaust Flow Data
Q Stack (dscfh)
Q Stack (dscm/hr)
181441.21 181978.10 181072.29 181497.20
5137.80 5153.00 5127.35 5139.38
Moisture Fraction Bws
Fuel Consumption (Btu/h[-hr)
0.17 0.17 0.17 0.17
0 0 0 0
Fuel Flow (dscfh)
Fuel (btu/scf)1020 1020 1020 1020
O2 F factor 8710.0 8710 8710 8710
Results
Method 3A Corrected O2% Dry
Moisture %16.74%16.75%16.80%16.76%
T
e
s
t
S
u
m
m
a
r
y
mfg. rated rpm
Test RPM
0.47%0.66%0.67%0.60%
Permitted Standards Results
5
Catalyst
0.0400.048
Run 1 Run 2 Run 3 3 Run Average Pass Permits
08:46 AM 10:02 AM 11:12 AM 12/4/2024
CO (g/hp-hr)0.035 0.0412.000 0.300 Pass
StateFederal
CO (ppmvw)10.395 14.317 11.846 12.186
CO (ppmvd)12.484 17.197 14.238 14.640
CO (mol wt) 28.01
CO (ppmvd) @15% O2 3.605 5.013 4.152 4.257 Fail
CO (ppbvd) @15% O2 3605.383 5012.582 4151.677 4256.547 Fail
NOx (g/hp-hr)0.048 0.035 0.032 0.0381.000 0.150 Pass
NOx (ppmvw)8.645 6.347 5.793 6.928
NOx (ppmvd)10.383 7.624 6.962 8.323
NOx (mol wt) 46.01
1.437 1.156 0.778 1.123NMNEHC (ppmvw)
1.725 1.388 0.935 1.349NMNEHC (ppmvd)
NOx (ppbvd) @15% O2 2998.417 2222.174 2030.188 2416.926 Fail
NOx (ppmvd) @15% O2 2.998 2.222 2.030 2.417 Fail
NMNEHC (mol wt) 44.10
498.233 404.557 272.503 391.764 FailNMNEHC (ppbvd) @15% O2
0.008 0.006 0.004 0.0060.700 0.030 PassNMNEHC (g/hp-hr)
0.498 0.405 0.273 0.392 FailNMNEHC (ppmvd) @15% O2
Gas, Inc.
5.0 Run Summaries
Summary Source Run 1
R
u
n
Table 5.1 Run Summaries
S
u
m
m
a
r
i
e
s
6
0.00Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %
10.40
0.00
8.64
0.00
0.00
0.00
8.65
0.28
1.44
0.13%
0.39%
0.00%
16.74%
NMNEHC
11.60 9.54 0.00 9.54 1.35 0.41%16.67%
78.69 31.20 0.00 31.20 26.37 0.20%14.97%
9.19 7.75 0.00 7.75 1.53 0.38%16.81%
0.00 0.00 0.33 0.33 0.17 0.14%0.04%
Avg. Wet
NO2NO
Summary Source Run 2
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
0.00 0.00 0.33 0.33 0.17 0.14%0.04%
13.72 6.46 0.00 6.46 1.24 0.69%16.71%
60.46 32.47 0.00 32.47 24.73 0.16%15.35%
14.92 6.24 0.00 6.24 1.07 0.42%16.79%
0.00 0.00 0.00 0.00 0.31 0.13%0.04%
Avg. Wet 14.32 6.35 0.00 6.35 1.16 0.55%16.75%
NO2NO
Summary Source Run 3
Baseline
Source
Spike
Source
Baseline
PPM Wet CO NOx Oxygen %Moisture %NMNEHC
12.11 6.22 0.00 6.22 0.84 0.70%16.73%
79.93 29.33 0.00 29.32 23.31 0.21%15.37%
11.59 5.37 0.00 5.37 0.71 0.42%16.87%
0.00 0.00 0.00 0.00 0.47 0.19%0.04%
0.00 0.00 0.00 0.00 0.31 0.13%0.04%
Avg. Wet 11.85 5.80 0.00 5.79 0.78 0.56%16.80%
NO2NO
Gas, Inc.
6.0 Volumetric Flow Rate Data
Volumetric Flow Rate Data
.99
Stack diameter =
Table 6.1. Data used for volumetric flow rate (Method 2)
20 inches or:1.67 feet. or:2.18 Square Feet
Run 1 Average
Pitot Tube Coefficient Cp(std)=
H2O
CO2
O2
CO
Molecular Weight Stack Gas dry basis (Md)
Molecular Weight Stack Gas wet basis (Ms)
Stack Static Pressure (Pg)
Stack Static Pressure (Pg)
Atmospheric Pressure at Location (Pbar)
Atmospheric Pressure at Location (Pbar)
Absolute Stack Pressure (Ps)
Stack Temperature
Stack Temperature
Stack Temperature
Stack Gas Velocity
Stack Flow Rate Q
Stack Gas Wet Volmetric Flow Rate
Stack Gas Dry Volumetric Flow Rate
Sample after Back Purge:
Within 5% of Last Δpstd reading:
Stack Diameter (inches)
Inches upstream from disturbance
Inches downstream from disturbance
scf/hr
0.54
Yes
20.00
10.00
16.00
scf/hr
cfs
ft/sec
Deg R
Deg F
Deg C
"Hg
"Hg
MBAR
"Hg
"H20
g/g mole
g/g mole
ppmd
%d
%d
%d 16.74
29.39
0.53
Inches
3.34
10
16.66
Vo
l
u
m
e
t
r
i
c
F
l
o
w
Ra
tes
Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1
Figure 6.1
16 Traverse Points Were Used
Emissions Sampling Points - 3 point long line sampling probe
First Sampling Point Taken @ 16.7% of Stack Diameter
Second Sampling Point Taken @ 50% of Stack Diameter
Third Sampling Point Taken @ 83.3% of Stack Diameter
8.58
0.40
10.40
845.00
0.04
24.96
25.00
924.06
1383.73
495.59
27.48
87.03
189.88
217910.76
181441.21
Run 2
16.75
29.40
0.53
8.60
0.56
14.32
845.53
0.04
24.97
25.01
919.31
1378.98
492.95
27.49
86.95
189.69
218588.37
181978.10
Run 3
16.80
29.40
0.53
8.63
0.56
11.85
845.02
0.04
24.96
25.00
927.31
1386.98
497.40
27.49
87.13
190.08
217637.58
181072.29
16.76
29.40
0.53
8.60
0.51
12.19
845.18
0.04
24.96
25.00
923.56
1383.23
495.31
27.49
87.04
189.89
218044.96
181496.63
*The exhaust stack did not present cyclonic flow conditions at the sampling location due to the
absence of cyclones, inertial demisters, venturi scrubbers, or tangential inlets.
* Cyclonic Flow Check (Pass/Fail): PASS
Δpstd (in) H2O
0.53
Exhaust Temp F
924.00
Pitot Tube Sampling Points (Velocity)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Δpstd Average=
Run 1
Table 6.2. Stack gas pressure readings measured with a standard pitot tube use for Volumetric Flow Rate
0.55
0.51
0.52
922.00
927.00
925.00
0.52
0.51
0.50
926.00
920.00
922.00
0.54
0.53
0.50
921.00
920.00
923.00
0.52 920.00
0.55
0.54
0.54
926.00
925.00
928.00
0.53
0.51
0.53
927.00
929.00
924.06
Δpstd = Velocity head measured by the
standard pitot tube, (in.) H2O.Run 3
Δpstd (in) H2O
0.52
Exhaust Temp F
927.00
0.51
0.53
0.54
925.00
926.00
922.00
0.54
0.53
0.52
923.00
928.00
930.00
0.50
0.55
0.53
929.00
928.00
931.00
0.54 932.00
0.51
0.51
0.50
926.00
927.00
926.00
0.53
0.54
928.00
929.00
927.310.53
Run 2
Δpstd (in) H2O
0.55
Exhaust Temp F
919.00
0.55
0.52
0.50
918.00
917.00
921.00
0.51
0.51
0.54
922.00
923.00
917.00
0.53
0.52
0.51
916.00
919.00
918.00
0.55 919.00
0.53
0.52
0.51
921.00
922.00
920.00
0.53
0.54
918.00
919.00
0.53 919.31
Pass
Strat Check
77.344Check 1
76.390Check 2
76.660Check 3
MethaneGas Used
Pass/Fail
7
Gas, Inc.
7.0 Calculations
Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate
*Note- Use of this method negates the need for any fuel related numbers for emissions calculations
Nomenclature
Δp(avg) = Velocity head of stack gas, mm H2O (in. H2O).Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg)
3600 = Conversion Factor, sec/hr.
A = Cross-sectional area of stack, m2 (ft2).
Bws = Water vapor in the gas stream (from ASTM D6348)
Kp = Velocity equation constant.
Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole).
Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole).
Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg).
Qsd = Dry volumetric stack gas flow rate corrected to
standard conditions, dscm/hr. (dscf/hr.).
Ts(abs) = Absolute stack temperature, °K (°R). = 460 + Ts for
English units.
Tstd = Standard absolute temperature, 293°K (528 °R).
Vs = Average stack gas velocity, m/sec (ft./sec).
*(Observed from Method 3 12.3) Dry Molecular Weight. Equation 3-1
Md = .44(.086)+.32(.005)+.28(.908+.001) = 29.388 LB/LB-MOLEMd = .44(%CO2)+.32(%O2)+.28(%N2+%CO)
12.5 Molecular Weight of Stack Gas. Equation 2-6
Ms = 29.388(1 -.16736)+.18.0(.16736) = 27.482 LB/LB-MOLEMs = Md(1-Bws)+18.0(Bws)
12.6 Average Stack Gas Velocity. Equation 2-7
Vs = 85.49*.99*√.53*√(1383.7325/(25*27.482)) = 87.03 FT/SECVs = Kp*Cp(std)*√Δpavg*√(Ts(abs)/(Ps*Ms))
12.7 Average Stack Gas Volumetric Flow Rate. Equation 2-8
Qsd = 3600(1-.167)87.034*2.182((528*25)/ (1383.7325*29.92)) = 181441.21 DSCF/HRQsd = 3600(1-Bws)Vs*A((Tstd*Ps)/(Ts(abs)*Pstd))
*Standard conversion from feet to meters
Q = 181441.214/35.315 = 5137.795 DSCM/HRQ = Qsd/35.315
Emission Rates (Examples use CO Run 1)
Nomenclature
CO corrected @ 15% O2
453.6= Conversion factor lb. to gram HP= Engines rated Horsepower
A = Cross-sectional area of stack, m2 (ft2).
BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.).
BTU/HP-HR. = Brake Specific Fuel Consumption (HHV)
ER = Emission rate of (CO) in g/HP-hr.
F(d )= Volumes of combustion components per unit of heat
content, scm/J (scf/million Btu).
Q = Stack gas volumetric flow rate, in standard cubic meters
per hour, dry basis
LB/HR.= Emission rate of (CO) in LB/HR.
Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min)
O2 = Concentration of oxygen on a dry basis, percent.
ppm= Parts Per Million (CO)
ppm@15% O2= PPM corrected to 15% O2
Qsd = Dry volumetric stack gas flow rate corrected
to standard conditions, dscm/hr. (DSCF/HR.).
Run Time = Run Time in Minutes
TPY= Tons per Year
Mol wt.= Mol Weight of CO (28.01)
Vs = Average stack gas velocity, m/sec (ft./sec).
ppm @ 15% O2 = 12.484*(20.9-15)/(20.9-.5%)) = 3.611 PPM @ 15% O2ppm @ 15% O2 = PPM*((20.9-15%O2)/(20.9-O2))
G/HP HR from 40 CFR Part 60 Subpart JJJJ
(12.484*(1.164*10^-3)*5137.795*(Run Time/60))/2125 = .035 G/HP-HRg/hp-hr = (PPM*(1.164*10^-3)*Q*(Run Time/60))/BHP/HR
LB/HR from Grams
LB/HR = .035*1/453.6*2125 = .165 LB/HRlb/hr = ER*1/453.6*BHP-HR
TPY
TPY = .165*4.38 = .723 TPYTPY = LB/HR. *4.38
Horsepower
HP Provided On Site
Wet to Dry PPM
12.48 = 10.395*(1/(1-.17))ppm wet * (1/(1-H2O) = ppm dry
8
Cp(std) = Standard pitot tube coefficient; use 0.99
Gas, Inc.
8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the
sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or
failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level
(low, mid, and high) the calibration error must be within ± 2.0 percent of the calibration span.
8.0 Oxygen Calibration
8.2 Initial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level
calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample-
conditioning components in system calibration mode.
8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple
runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed
final test in this case will invalidate all runs subsequent to the last passed test.
(1) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration.
(2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be
operated at the normal sampling rate during all system bias checks.
(3) If the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA
Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre-
and post-run system bias must be within ± 5.0 percent of the calibration span for the low-level and upscale calibration gases.
(1) If the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration
error test and system bias is passed before repeating the run.
(2) After each run, the low-level and upscale drift is calculated, using Equation 7E–4 in Section 12.5 from EPA Method 7E. If the post-run low-
and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point
calibration error test and a system bias check must be performed and passed prior to additional testing.
Table 8.1 Oxygen Calibration
EPA Method 3A QA Worksheet
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Certified Gas Concentraion
Low-Level (%)
0.00%
Certified Gas Concentraion
Mid-Level (%)
Certified Gas Concentraion
High-Level (%)
(DIRECT) Analyzer Calibration Error (≤ 2%)
Certified
Concentration
Value (%)
Direct
Calibration
Response (%)
Absolute
Difference (%)
Analyzer
Calibration
Error (%)Analyzer Direct
Calibration
Response
Certified bottle
value %
0.00%
0.00%
0.00%
Zero Gas %
Mid-Level Gas %
High-Level Gas %
Bias Pre Initial Value Bias Post Inital Values
System
Calibrations
Response Pre
(%)
0.00%
System Bias (%
of Span) Pre
System
Calibration
Response Post
(%)
System Bias (%
of Span) Post
Drift (% of
Span)
0.00%0.00%0.00%0.00%
(SYSTEM) Calibration Bias Checks (≤ 5%) and Drift Checks (≤ 3%)
Avg. Gas Concentration (Run 1)
Avg. Gas Concentration (Run 2)
Avg. Gas Concentration (Run 3)
Effluent Gas (Cgas) Run 1
Effluent Gas (Cgas) Run 2
Effluent Gas (Cgas) Run 3
Linearity Check
0.00%0.00%0.00%
Method 7E 3.4 To the extent practicable, the measured emissions should be between
20 to 100 percent of the selected calibration span. This may not be practicable in some
cases of low concentration measurements or testing for compliance with an emission
limit when emissions are substantially less than the limit.
7E 8.5: Note: that you may
risk sampling for multiple
runs before performing the
post-run bias provided you
pass this test at the
conclusion of the group of
runs
Upscale Gas
Analyzer
Calibration
Response (%)
Zero Gas
Upscale Gas
EPA Method 3A QA Worksheet
Zero Gas
Mid-Level Gas
High-Level Gas
100% Nitrogen
O2 QA/QC
Zero Gas %0.00%
Mid-Level Gas %
High-Level Gas %
System
Calibration
Response Pre
(%)
System
Calibration
Response Post
(%)
Zero Gas %
Upscale Cal
Zero Gas %
Upscale Cal
Upscale Used
Upscale Used
10.81%
21.01%
10.87%
10.70%
10.62%
10.62%
10.70%10.87%
10.81%
21.01%
10.62%
21.05%
10.62%
21.05%
10.62%21.05%
0.00%
10.62%
21.05%
0.19%
0.04%
0.92%
0.18%
10.62%
Span
Zero Offset 0.00%
21.05
0.00%
10.81%0.29%0.54%0.01%
0.48%
0.67%
0.68%
0.47%
0.66%
0.67%
9
Gas, Inc.
0.0 0.0 0.0
0.0 0.0 0.0
1044.0 1036.0 1039.3
1015.0 1011.0 1013.7
4.4 4.4 4.5
9.0 Engine Parameter Data Sheet
Company
Site Elevation (ft)
Facility
Unit ID
Date
Make
Crusoe Energy Systems, Inc.
Residue Booster Station
12/4/2024
5406
1527
Waukesha
Model
Serial Number
9394 GSI
1673793
Technician Hunter Newton
Run Start Times 08:46 AM 10:02 AM 11:12 AM 12:26 PM
Run 1 Run 2 Run 3 Completed
Engine Parameter Data
Run 1
Engine Speed (RPM)1200.0 1200.0 199.0 866.3
Engine Hours 3728 3729 3730 3731
Intake Manifold Pressure (psi)60.0 60.0 58.0 59.3
Intake Manifold Temp °F 113.0 115.0 115.0 114.3
Engine Load (BHP)2125.0 2150.0 2125.0 2133.3
Ambient Temp °F 41.0 24.0 34.0 33.0
Humidity %39.0 77.0 60.0 58.7
Dew Point °F 18.0 18.0 21.0 19.0
Waukesha
YesCatalyst (Yes or No)
AFR Manufacturer/Type Waukesha Waukesha Waukesha
10
Run 3 AverageRun 2
0.0
0.0Discharge Pressure (psi)
Suction Pressure (psi)
1038.0
1015.0
4.8Catalyst Pressure Drop H2O
Catalyst Outlet Temp °F
Catalyst Inlet Temp °F
Gas, Inc.
10.0 QA/QC Results
Average:Carbon monoxide CO
Gas, Inc.
0.00
R
e
s
u
l
t
s
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.43
Average:Oxygen 0.11
Pre-test Baseline Results Time:
Q
A
/
Q
C
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 97.23
Tolerance 2.00%
Difference between measured and expected 1.07%
CTS Direct to Analyzer Time:
Average:Carbon monoxide CO 0.00
Average:Nitrogen monoxide NO 0.00
Average:Nitrogen dioxide NO2 0.00
Average:NOx 0.00
Average:VOC 0.26
Average:Oxygen 0.09
Pre-test System Zero Time:
Mechanical Response Time 58 seconds
Value:CTS Bottle Concentration 98.28
Value:CTS Compound Concentration Avg 96.73
Tolerance 5.00%
Difference between measured and expected 1.58%
Pre-test System CTS & Mechanical Response Time
45 secondsEquilibration Response Time
Value:Spike Reported 252.50
Value:Spike Expected 252.40
System (Equilibration) Response Time Target (Spike)
53 secondsSystem Zero Response Time
58 secondsSystem Response Time
System (Zero) Response Time
11
11.0 D6348 Annexes 1-8
D6348 Annexes 1. Test Plan Requirements
Annex 1.2
The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1, 2, 3,
4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures
were within acceptable limits. Data generated during the pre-test and post-test procedures are
summarized below in order of the distinctive Annex.
Three 60 minute test runs were performed. The final analyte concentrations are the average of each test
run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans.
Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the
VOC that is most commonly found in the combustion process of natural gas.  Additionally, the molecular
weight of Propane coincides with with molecular weight of VOC's per the EPA.
Annex Table 1.2.1 Certified Calibration Bottle Concentrations
Bottle Expiration NO2 Ethylene SF6 O2 (%)
CC506322 9/17/2027 99.95 10.62%
EB0020295 6/20/2032 98.28
EB0090574 11/27/2031 21.05%
Cylinder # ALM-063647 Expiration: 5-03-2032
Propane CO NO SF6
Bottle Value 252.40 501.70 237.50 10.20
Analyzer System Response 252.50 500.85 236.64 10.15
Percent Difference 0.04%0.17%0.36%0.47%
Annex Table 1.2.2 Measurement System Capabilities
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 97.233 4.947
Spike Direct
Propane 254.684
Mechanical
Response Time
SF6 10.210
CO 508.291
NO 239.111
Ethylene 96.728 58 seconds
Analyzer
Response
Propane 252.495
SF6 10.152
CO 500.850
NO 236.640
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 250.815
CO 507.871
NO 236.442
44 seconds
53 seconds
8.32%
7.84%
7.59%
117.86%
117.92%
116.14%
10.065
12
Gas, Inc.
Annex 1.3
Compounds
Infrared
Analysis Region
(cm-1)
Expected
Concentration
Range
Measurement
System
Achievable
Minimum
Detectable
Concentrations
Required
Measurement
System
Accuracy and
Precision for
Test Application
CO 2000-2200 0-1200 ppm
NO 1875-2138
NO2 2700-2950
VOC
2600-3200
910-1150
2550-2950
CH2O 2550-2850
Interfering
Compounds * CO is analyzed in a separate analysis region than CO2 and H2O
CO2
Water Vapor
926-1150
3200-3401
Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives
0.16267 ppm 4 ppm
0-1000 ppm 0.4007 ppm 2 ppm
0-100 ppm 0.4899 ppm 2 ppm
0-100 ppm 1.8520 ppm Total
VOC's 1 ppm per VOC
0-100 ppm 0.7878 ppm 1 ppm
0-10%
0-22%
0%
0.20%
n/a
n/a
* VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane.
Annex 1.4
Figure Annex 1.4.1 Sampling Train
The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A
heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges
through the FTIR outlet.
13
Gas, Inc.
Sampling Point Locations
in Inches
16.7%3.340
50%10.000
83.3%16.660
Figure Annex 1.4.3 Sample Port Location
Figure Annex 1.4.2 Sampling Points
Interior Stack Diameter (inches):
Inches
Upstream:
Inches
Downstream:
20
10
16
14
Stack Gas Dry Volumetric Flow Rate
(scf/hr):
181496.63
H2O%d @ Sampling Point:16.76
CO2%d @ Sampling Point:8.6
Pressure @ Sampling Point (Pg "H2O):0.53
Temperature @ Sampling Point (Deg F):923.56
Gas, Inc.
D6348 Annex 2. Determination of FTIR Measurement System Minimum Detectable Concentrations (MDC#1)
Target Analyte Results (ppm)
CO 0.1627
NO 0.4007
NO2 0.4899
Ethylene 0.3782
Propane 0.4351
Hexane 0.2233
Acetaldehyde 0.8152
Formaldehyde 0.7878
D6348 Annex 3. FTIR Reference Spectra
Calibration Transfer Standard Expected Measured Path Length Validated
Ethylene 98.28 97.23 4.947 Passed
D6348 Annex 4. Required Pre-Test Procedures
Annex Table 1.2.2 Measurement System Capabilities
15
SF6
Parameter
Measured Gas Concentration
(ppm)Path Length Equilibration
Time Dilution Factor % Recovery
Path Length Ethylene 97.233 4.947
Spike Direct
Propane 254.684
Mechanical
Response Time
SF6 10.210
CO 508.291
NO 239.111
Ethylene 96.728 58 seconds
Analyzer
Response
Propane 252.495
SF6 10.152
CO 500.850
NO 236.640
Analyte Spike
Recovery Propane & SF6
System Zero Nitrogen
Post Spike
System
Propane 250.815
CO 507.871
NO 236.442
44 seconds
53 seconds
8.32%
7.84%
7.59%
117.86%
117.92%
116.14%
10.065
Gas, Inc.
D6348 Annex 5. Analyte Spiking Technique
Propane
Spike Direct
SF6
CO
NO
252.400
10.200
501.700
237.500
254.684
10.210
508.291
239.111
0.90%
0.10%
1.31%
0.68%
+/- 2%
+/- 2%
+/- 2%
+/- 2%
Pass
Pass
Pass
Pass
Parameter Gas Concentration Measured % Difference Specification Validated
0.103
0.000
Spike Average
24.862
0.849
Dilution Factor
8.315%
Expected
21.094
% Recovery
117.860%
Specification
70-130%
<10%
Spike Run 1 via the System
Source Output
Propane
SF6
D6348 Annex 6. Determination of System Performance Parameters
Noise Equivalent Absorbance (NEA)
RMS High
RMS Mid
RMS Low
Line Position: Demonstrating the peak positions align correctly (Manual Comparison +/- 20%)
0.000
Spike Average
0.800
Dilution Factor
7.835%
Expected % Recovery Specification
70-130%
<10%
Spike Run 2 via the System
Source Output
Propane
SF6
0.000
Spike Average
0.775
Dilution Factor
7.591%
Expected % Recovery Specification
70-130%
<10%
Spike Run 3 via the System
Source Output
Propane
SF6
0.000 22.249 19.157 116.140%
0.001120
0.001825
0.001394
0.001 23.336 19.789 117.920%
Line Position Difference:Resolution Difference to Reference0.00%Pass Pass4.63%
16
Gas, Inc.
Resolution
The Gasmet GICCOR (Genzel Interferometer with Cube Corner Retroreflectors) interferometer is specially
designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining
stable with any vibration and temperature changes.
Detector Linerarity
The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle
setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS
gas was performed and validated.
D6348 Annex 7. Preparation of Analytical Quantification Algorithm
The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex
7.6
Regression Slope:-17.6417408 Pass
Line Position Difference:Resolution Difference to Reference 4.63%
D6348 Annex 8. Post Test Quality Assurance/Quality Control Procedures
CTS Bottle Concentration:
CTS Sample Concentration Average:
Difference between measured and expected:
Tolerance:
98.28
96.09
2.27%
5.00%
POST CTS System Check:
Run 1 Points 1 & 2 on CO/NO/Propane
Run 2 Points 1 & 2 on CO/NO/Propane
Run 3 Points 1 & 2 on CO/NO/Propane
Run Data Validation - Automated vs Manual Reading Validated Comments
All within 20%
All within 20%
All within 20%
Passed
Passed
Passed
Demonstrates no interferences observed.
Demonstrates no interferences observed.
Demonstrates no interferences observed.
17
Gas, Inc.
12.0 Signature Page
Job/File Name:
We certify that based on review of test data, knowledge of those individuals directly responsible for
conducting this test, we believe the submitted information to be accurate and complete.
Crusoe Energy Systems, Inc.; Residue Booster Station; 1527; JJJJ
18
Company:
Print Name:
Signature:
Title:
Phone Number:
Date:
Company:G.A.S. Inc.Date:
Print Name:
Title:
12/4/2024
Emissions Specialist
Company:G.A.S. Inc.Date:
Print Name:
Title:
Signature:
Phone Number:
Travis Hartley
Director of Stack Testing
580-225-0403
12/4/2024
Hunter Newton
Gas, Inc.
Appendices
Gas, Inc.
Gas, Inc.
Spike (5 Gas)
Gas, Inc.
9% O2/NO2
Gas, Inc.
Ethylene Only
Gas, Inc.
BIP
Gas, Inc.
21% O2
Tri Probe Certification
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3/3/2022
Probe size: 20S
Mr. Jordan Williamson
CEO
GAS Inc.
303 W. 3rd Street
Elk City, OK 73644
Dear Mr. Williamson:
We are writing in response to your letter received on September 17, 2020, in which you request the approval
of alternative testing procedures. The EPA’s Office of Air Quality Planning and Standards (OAQPS) is the
delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40
CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of
the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under
40 CFR part 60, Subpart JJJJ – Standards of Performance for Stationary Spark Ignition Internal Combustion
Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ – National Emissions Standards for Hazardous
Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ).
The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR)
instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section
8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts
JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 when conducting testing using ASTM
D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ.
In your request, you state that this alternative linearity check procedure will produce consistent results when
utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow
for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct
the entirety of the ASTM D6348-03 method in its current form using such an instrument.
Based on our understanding of FTIR instrument principles and recognition that the requested alternative
determination of detector linearity is both technically sound and contained within Method 320, we are
approving the requested change. We believe that this alternative is acceptable for use for use in testing all
engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this
letter as ALT-141 on EPA’s website (at www.epa.gov/emc/broadly-applicable-approved-alternative-
testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for
the purposes of meeting Subparts JJJJ and ZZZZ.
March 15, 2021
Sincerely,
Steffan M. Johnson, Group Leader
Measurement Technology Group
If you should have any questions or require further information regarding this approval, please contact David
Nash of my staff at 919-541-9425 or email at [e-mail].
cc:
Sara Ayers, EPA/OECA/OC/MAMPD, ([e-mail])
Melanie King, EPA/OAR/OAQPS/SPPD, ([e-mail])
James Leather, EPA Region 6, ([e-mail])
David Nash, EPA/OAR/OAQPS/AQAD, ([e-mail])
Heather Sessing, Oklahoma DEQ, ([e-mail])
Hunter Newton
GAS, Inc.
Type of Sources Tested:
[e-mail]
Stationary Internal Combustion Engines
• 4 Stroke Rich Burn Engines
• 2 Stroke & 4 Stroke Lean Burn Engines
Stationary Natural Gas Fired Generators
Stationary Propane Fired Generators
Gas Fired Boilers
Qualifications:
Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the
following Reference Methods:
• EPA Method 1 & 1A – Sampling & Traverse Points
• EPA Method 2 & 2C – Velocity & Volumetric Flow Rate of a Gas Stream
• EPA Method 3A – Oxygen
• EPA Method 7E – NOX
• EPA Method 10 – Carbon Monoxide
• EPA Method 25A – Volatile Organic Compounds
• ASTM D6348 – Extractive Fourier Transform Infrared Spectroscopy
Conducts emissions testing on a weekly basis including, but not limited to, the following test types: Initial
Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. All tests performed
are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117,
PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico,
Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York,
Kentucky, & Mississippi.
• Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State
Compliance guidelines, & site-specific safety certifications.
Types of Analyzers:
• Gasmet DX4000 FTIR
• Gasmet Portable Sampling Unit with Zirconium Oxide O2 Sensory
• Testo 350
• Flame Ionization Detector
580-225-0403
Gas, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
1 Minute Average Data Sheet
Crusoe Energy Systems, Inc.Client:
Residue Booster Station
Unit Number:1527
Make:Waukesha
Location:9394 GSIModel:
1673793Serial Number:
RAW Result Data
Stability
12/4/2024 06:50 5.1575.243-0.027 0.079 0.00034.157 0.000 0.000 0.0000.0070.000 12.176 1.5250.008 0.000 858.09.850.305 0.301 10.40 0.16 180.0
Pre Test Baseline Direct
12/4/2024 06:59 0.0000.000-0.000 0.000 0.2710.000 0.000 1.205 0.0000.0000.459 0.000 0.0000.011 0.000 856.00.450.672 0.000 0.00 0.17 180.0
12/4/2024 07:00 0.0000.000-0.001 0.000 0.2050.000 0.000 1.274 0.0000.0820.256 0.000 0.0000.047 0.000 855.00.420.636 0.000 0.00 0.17 180.0
12/4/2024 07:00 0.0000.000-0.002 0.000 0.6050.000 0.000 1.369 0.0000.0290.122 0.000 0.0000.000 0.000 855.00.430.645 0.000 0.00 0.00 180.0
CTS Direct
12/4/2024 07:05 0.0000.0000.006 0.000 0.2080.000 0.000 0.215 0.0000.0000.000 96.788 0.0000.000 0.000 849.064.920.583 0.000 0.00 0.06 180.0
12/4/2024 07:06 0.0000.0000.006 0.000 0.1040.000 0.000 0.213 0.0000.0000.000 97.497 0.0000.000 0.000 848.065.390.577 0.000 0.00 0.06 181.0
12/4/2024 07:06 0.0000.0000.006 0.000 0.2030.000 0.000 0.179 0.0000.0000.000 97.413 0.0000.000 0.000 847.065.340.597 0.000 0.00 0.06 180.0
High O2 Direct
12/4/2024 07:09 0.0000.0000.000 0.000 0.0000.000 0.000 1.319 0.0000.0090.000 0.000 0.0000.069 0.000 845.00.440.653 0.000 0.00 21.16 180.0
12/4/2024 07:10 0.0000.000-0.004 0.000 0.0000.000 0.000 1.581 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.520.785 0.000 0.00 20.94 180.0
12/4/2024 07:10 0.0000.000-0.007 0.000 0.0000.000 0.000 1.528 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.470.697 0.000 0.00 20.94 180.0
NO2/Mid O2 Direct
12/4/2024 07:18 99.3530.000-0.004 0.000 0.0450.000 0.577 1.150 0.4980.0000.627 0.000 0.0000.000 0.000 845.00.000.000 0.000 99.35 10.80 180.0
12/4/2024 07:18 99.7100.000-0.002 0.000 0.0000.000 0.462 1.073 0.4950.0000.062 0.000 0.0000.000 0.000 845.00.000.000 0.000 99.71 10.78 180.0
12/4/2024 07:18 100.0870.000-0.004 0.000 0.0000.000 0.571 1.216 0.4650.0000.358 0.000 0.0000.000 0.000 845.00.000.000 0.000 100.09 10.86 180.0
Spike Direct
12/4/2024 07:28 0.000239.121-0.003 4.777 5.487508.704 2.271 1.524 8.9780.3080.000 1.366 254.9140.000 0.000 844.0257.652.734 10.221 239.12 0.19 180.0
12/4/2024 07:28 0.000239.2070.003 4.769 5.276508.864 2.291 1.535 8.9140.2070.060 1.396 254.8560.014 0.000 844.0257.572.676 10.210 239.21 0.02 180.0
12/4/2024 07:29 0.000239.0040.000 4.757 5.353507.305 2.301 1.446 9.3050.2420.000 1.394 254.2810.000 0.000 845.0257.122.859 10.198 239.00 0.02 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline System
12/4/2024 07:31 0.0000.0000.026 0.000 0.0000.000 0.000 2.041 0.0000.0000.963 0.000 0.0000.000 0.058 845.00.270.227 0.000 0.00 0.13 180.0
12/4/2024 07:31 0.0000.0000.017 0.000 0.3220.000 0.000 1.905 0.0000.0050.477 0.000 0.0000.000 0.000 845.00.260.385 0.000 0.00 0.13 180.0
12/4/2024 07:31 0.0000.0000.013 0.000 0.5700.000 0.000 1.953 0.0000.0000.573 0.000 0.0000.025 0.000 845.00.250.378 0.000 0.00 0.00 180.0
CTS System with Response Time
12/4/2024 07:33 0.0000.0000.020 0.000 0.0110.000 0.000 0.588 0.0000.0000.000 96.566 0.0000.000 0.000 845.064.670.429 0.000 0.00 0.18 180.0
12/4/2024 07:34 0.0000.0000.021 0.000 0.0590.000 0.000 0.494 0.0000.0000.000 96.602 0.0000.000 0.000 845.064.700.447 0.000 0.00 0.06 180.0
12/4/2024 07:34 0.0000.0000.020 0.000 0.0420.000 0.000 0.588 0.0000.0000.000 97.015 0.0000.000 0.000 845.064.980.455 0.000 0.00 0.19 180.0
NO2/Mid O2 System with Response Time
12/4/2024 07:40 97.9010.0000.008 0.000 0.0000.000 0.643 1.744 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.120.180 0.000 97.90 10.89 180.0
12/4/2024 07:41 99.8180.0000.008 0.000 0.0000.000 0.652 1.809 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.170.251 0.000 99.82 10.82 180.0
12/4/2024 07:41 99.4920.0000.006 0.000 0.0000.000 0.650 1.700 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.180.268 0.000 99.49 10.91 180.0
Spike System with Response Time
12/4/2024 07:43 0.000236.4840.012 4.774 4.130499.794 2.327 1.499 10.0990.1381.014 1.389 252.1450.033 0.000 845.0254.912.763 10.139 236.48 0.38 180.0
12/4/2024 07:43 0.000236.7340.011 4.762 3.840501.112 2.293 1.573 9.9790.1120.741 1.391 252.5850.000 0.000 845.0255.372.792 10.156 236.73 0.20 180.0
12/4/2024 07:44 0.000236.7020.011 4.773 3.919501.644 2.283 1.532 9.9430.0850.897 1.362 252.7560.000 0.000 845.0255.532.799 10.160 236.70 0.02 180.0
Baseline System with Response Time
12/4/2024 07:46 0.0000.0000.005 0.000 0.0000.000 0.000 1.461 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.240.355 0.000 0.00 0.13 180.0
12/4/2024 07:47 0.0000.0000.005 0.000 0.3200.000 0.000 1.505 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.270.403 0.000 0.00 0.12 180.0
12/4/2024 07:47 0.0000.0000.004 0.000 0.2990.000 0.000 1.600 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.320.487 0.000 0.00 0.14 180.0
Run 1 - A 30minute/60min
12/4/2024 08:47 0.0006.66613.743 8.725 80.6704.887 3.925 9.835 2.1370.0002.590 0.000 0.1500.510 0.219 845.01.030.671 0.000 6.67 0.49 180.0
12/4/2024 08:48 0.0009.00516.405 8.435 84.45620.208 3.474 14.360 1.4520.0003.699 0.000 0.3550.346 0.234 845.01.430.906 0.000 9.01 0.42 179.0
12/4/2024 08:49 0.0009.62416.117 8.500 87.66523.536 3.524 15.505 1.9010.0002.406 0.000 0.3330.433 0.197 845.01.390.995 0.000 9.62 0.21 180.0
12/4/2024 08:50 0.00013.10416.118 8.501 87.25729.060 4.417 18.565 2.0650.0001.915 0.000 0.3740.391 0.289 845.01.641.030 0.000 13.10 0.57 180.0
12/4/2024 08:51 0.00010.03416.696 8.479 86.36616.171 3.651 16.587 1.8730.0002.070 0.000 0.2240.401 0.368 845.01.651.031 0.000 10.03 0.40 180.0
12/4/2024 08:52 0.00011.25816.982 8.416 70.5462.779 4.527 17.646 1.8500.0002.047 0.000 0.0000.506 0.296 845.01.200.914 0.000 11.26 0.22 181.0
12/4/2024 08:53 0.00010.88216.709 8.412 75.1910.000 4.851 15.377 2.2330.0002.340 0.000 0.0000.587 0.274 845.01.060.767 0.000 10.88 0.85 179.0
12/4/2024 08:54 0.0004.79316.782 8.545 72.7300.000 2.795 10.453 1.8860.0001.585 0.000 0.0000.472 0.299 845.01.200.902 0.000 4.79 0.40 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 08:55 0.0007.76716.928 8.440 83.4870.000 3.989 13.809 1.6680.0002.082 0.000 0.1440.433 0.368 845.01.490.912 0.000 7.77 0.83 180.0
12/4/2024 08:56 0.0004.71916.900 8.478 85.8990.000 2.984 10.735 1.7730.0002.080 0.000 0.1690.385 0.356 845.01.551.003 0.000 4.72 0.76 180.0
12/4/2024 08:57 0.0007.46816.865 8.516 84.9530.000 3.666 11.808 1.6790.0001.741 0.000 0.1320.455 0.398 845.01.480.831 0.000 7.47 0.52 180.0
12/4/2024 08:58 0.0009.94216.865 8.466 96.2427.850 4.026 17.092 2.5270.0001.609 0.000 0.2760.446 0.364 845.01.620.922 0.000 9.94 0.37 180.0
12/4/2024 08:59 0.00013.23716.852 8.424 73.9912.942 6.013 20.400 2.1760.0001.568 0.000 0.0000.585 0.345 845.01.210.784 0.000 13.24 0.86 179.0
12/4/2024 09:00 0.0001.94916.963 8.532 64.1760.000 2.537 9.024 1.3270.0001.233 0.000 0.0000.466 0.274 845.01.110.837 0.000 1.95 0.74 180.0
12/4/2024 09:01 0.0746.60717.045 8.520 71.5000.000 3.163 10.319 1.6660.0000.936 0.000 0.0000.411 0.283 845.01.120.829 0.000 6.68 0.27 180.0
12/4/2024 09:02 0.0005.31717.031 8.481 91.04213.127 2.855 14.184 2.0960.0001.572 0.000 0.1270.333 0.346 845.01.430.911 0.000 5.32 0.33 180.0
12/4/2024 09:03 0.00012.95516.931 8.466 83.8718.755 4.979 19.332 1.7230.0001.289 0.000 0.0080.404 0.339 845.01.320.954 0.000 12.96 0.74 180.0
12/4/2024 09:04 0.0007.22716.882 8.499 74.1220.000 3.295 11.457 1.8460.0001.123 0.000 0.0000.489 0.276 845.01.160.905 0.000 7.23 0.31 180.0
12/4/2024 09:05 0.0008.08416.868 8.495 92.88721.970 3.244 17.978 2.2120.0001.021 0.000 0.1130.341 0.375 845.01.460.888 0.000 8.08 0.05 180.0
12/4/2024 09:06 0.00013.94116.870 8.478 92.99039.144 3.774 23.109 2.3220.0001.268 0.000 0.1420.469 0.369 845.01.480.896 0.000 13.94 0.52 180.0
12/4/2024 09:07 0.00013.01516.846 8.470 87.68813.160 3.936 19.448 2.0300.0001.184 0.000 0.1130.425 0.341 845.01.390.900 0.000 13.01 0.35 180.0
12/4/2024 09:08 0.0008.97116.866 8.507 84.4530.474 3.370 13.531 1.5850.0001.476 0.000 0.0000.515 0.324 845.01.331.022 0.000 8.97 0.19 180.0
12/4/2024 09:09 0.0008.08116.867 8.524 89.29113.791 3.300 15.860 1.9980.0001.178 0.000 0.0240.370 0.337 845.01.340.955 0.000 8.08 0.40 180.0
12/4/2024 09:10 0.00011.80316.843 8.555 90.23417.838 3.612 18.426 2.0980.0001.243 0.000 0.0890.429 0.343 845.01.390.922 0.000 11.80 0.20 180.0
12/4/2024 09:11 0.00012.18916.861 8.533 84.28114.008 3.860 18.442 1.6980.0001.776 0.000 0.0280.400 0.350 845.01.380.971 0.000 12.19 0.06 180.0
12/4/2024 09:12 0.00011.25216.762 8.549 75.58919.753 3.399 17.178 2.0940.0001.610 0.000 0.0000.521 0.298 845.01.180.882 0.000 11.25 0.29 180.0
12/4/2024 09:13 0.0009.86316.658 8.540 88.16427.835 2.777 17.149 1.9590.0002.073 0.000 0.1270.411 0.376 845.01.530.980 0.000 9.86 0.17 180.0
12/4/2024 09:15 0.00013.44516.577 8.561 91.37939.648 3.300 21.589 2.3360.0001.259 0.000 0.1670.398 0.366 845.01.520.932 0.000 13.44 0.20 180.0
12/4/2024 09:16 0.00012.85916.545 8.522 75.0927.470 4.516 19.270 2.2320.0001.259 0.000 0.0000.501 0.275 845.01.140.879 0.000 12.86 0.22 180.0
12/4/2024 09:17 0.00010.05916.591 8.556 71.4123.490 4.245 16.437 1.9120.0000.871 0.000 0.0000.524 0.269 845.01.140.904 0.000 10.06 0.51 180.0
0.0029.53716.666 8.504 82.58711.597 3.733 15.830 1.9450.0001.670 0.000 0.1030.445 0.318 845.001.3460.908 0.000 9.539 0.415 179.9Avg.
Spike 1
12/4/2024 09:24 0.00031.20214.967 8.256 83.43978.690 3.663 18.729 1.8160.0001.290 0.000 24.8620.175 0.278 845.026.371.425 0.849 31.20 0.20 179.0
Run 1 - B 30minute/60min
12/4/2024 09:29 0.0007.09316.771 8.646 85.9542.318 3.518 13.630 1.6720.0001.015 0.000 0.0440.380 0.356 845.01.390.945 0.000 7.09 0.42 180.0
12/4/2024 09:30 0.0006.97816.777 8.653 82.6957.256 3.614 15.626 1.3870.0000.948 0.000 0.0000.498 0.363 845.01.390.996 0.000 6.98 0.06 180.0
12/4/2024 09:31 0.0007.30016.817 8.655 92.8890.000 3.558 13.590 2.2330.0001.221 0.000 0.0680.423 0.387 845.01.551.054 0.000 7.30 0.47 180.0
12/4/2024 09:32 0.0006.53616.777 8.665 84.2620.000 3.169 11.697 1.4980.0001.079 0.000 0.0000.431 0.398 845.01.450.979 0.000 6.54 0.43 180.0
12/4/2024 09:33 0.0005.98216.775 8.644 90.3288.520 3.242 14.723 1.7460.0000.820 0.000 0.0000.496 0.433 845.01.611.119 0.000 5.98 0.22 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 09:34 0.0005.89216.843 8.638 77.6440.823 3.719 14.092 2.0110.0001.115 0.000 0.0000.566 0.335 845.01.270.901 0.000 5.89 0.32 180.0
12/4/2024 09:35 0.0006.57616.793 8.635 83.7960.000 3.223 11.983 1.2250.0000.739 0.000 0.0000.492 0.405 845.01.551.108 0.000 6.58 0.42 180.0
12/4/2024 09:36 0.0007.32316.808 8.644 83.5710.000 3.540 12.469 1.2890.0000.599 0.000 0.0000.413 0.380 845.01.471.064 0.000 7.32 0.36 180.0
12/4/2024 09:37 0.0003.63716.822 8.614 89.92812.012 2.562 13.310 1.8140.0000.851 0.000 0.0000.416 0.387 845.01.511.100 0.000 3.64 2.39 180.0
12/4/2024 09:38 0.0008.21616.852 8.642 98.27126.171 3.081 18.457 2.7910.0001.105 0.000 0.1280.469 0.414 845.01.701.119 0.000 8.22 0.20 180.0
12/4/2024 09:39 0.00014.18616.784 8.627 91.18815.702 4.240 21.631 2.0110.0000.628 0.000 0.0000.472 0.435 845.01.581.070 0.000 14.19 0.07 180.0
12/4/2024 09:40 0.00010.38416.784 8.571 75.2676.676 4.648 19.140 1.9120.0000.518 0.000 0.0000.680 0.346 845.01.250.841 0.000 10.38 0.20 180.0
12/4/2024 09:41 0.0008.61316.823 8.615 84.4026.952 4.088 17.045 1.5720.0000.629 0.000 0.0000.461 0.399 845.01.501.058 0.000 8.61 0.22 180.0
12/4/2024 09:42 0.00012.69316.798 8.623 88.04418.434 4.476 20.728 1.7870.0000.540 0.000 0.0000.523 0.443 845.01.540.981 0.000 12.69 0.19 180.0
12/4/2024 09:43 0.0005.59016.859 8.642 93.7685.068 3.131 14.095 2.2240.0000.764 0.000 0.0000.508 0.452 845.01.701.188 0.000 5.59 0.17 180.0
12/4/2024 09:44 0.0006.50316.964 8.681 91.43316.366 3.230 17.266 1.9730.0000.884 0.000 0.0000.492 0.457 845.01.641.090 0.000 6.50 0.06 180.0
12/4/2024 09:45 0.00010.90916.874 8.664 84.83311.085 4.254 19.381 1.6150.0000.686 0.000 0.0000.571 0.482 845.01.610.972 0.000 10.91 2.37 180.0
12/4/2024 09:46 0.00012.38216.808 8.661 92.77529.756 3.940 22.529 2.2750.0000.222 0.000 0.0000.570 0.519 845.01.771.099 0.000 12.38 0.06 180.0
12/4/2024 09:47 0.0009.36916.823 8.632 77.72617.418 3.977 19.823 2.0850.0000.583 0.000 0.0000.575 0.410 845.01.480.997 0.000 9.37 0.21 180.0
12/4/2024 09:48 0.0007.04316.858 8.684 82.2233.849 3.852 15.341 1.2750.0000.631 0.000 0.0000.485 0.453 845.01.631.086 0.000 7.04 0.23 180.0
12/4/2024 09:49 0.0007.60116.866 8.736 90.36117.988 3.084 17.050 1.8510.0000.434 0.000 0.0000.521 0.507 845.01.741.083 0.000 7.60 0.06 180.0
12/4/2024 09:50 0.00011.70116.816 8.660 84.90617.673 4.888 22.033 1.6630.0000.530 0.000 0.0000.583 0.498 845.01.630.951 0.000 11.70 0.23 180.0
12/4/2024 09:51 0.0008.70216.746 8.633 78.13910.222 3.672 17.323 2.1870.0000.413 0.000 0.0000.591 0.420 845.01.500.990 0.000 8.70 0.06 179.0
12/4/2024 09:52 0.0009.89816.712 8.646 85.3660.000 3.999 14.578 1.5550.0000.315 0.000 0.0000.503 0.460 845.01.661.109 0.000 9.90 0.55 180.0
12/4/2024 09:53 0.0006.80716.650 8.610 83.21512.592 3.504 18.248 1.4830.0000.106 0.000 0.0000.454 0.432 845.01.591.090 0.000 6.81 0.18 180.0
12/4/2024 09:54 0.0006.97416.713 8.642 81.7515.772 3.833 15.044 1.2160.0000.362 0.000 0.0000.509 0.423 845.01.531.027 0.000 6.97 0.40 180.0
12/4/2024 09:55 0.0004.62816.738 8.622 65.4250.000 3.565 12.611 1.2410.0000.015 0.000 0.0000.564 0.328 845.01.250.897 0.000 4.63 0.44 179.0
12/4/2024 09:56 0.0004.18516.876 8.709 72.7360.000 2.308 9.313 1.6630.0000.223 0.000 0.0000.606 0.340 845.01.280.899 0.000 4.18 0.16 180.0
12/4/2024 09:57 0.0003.36116.824 8.672 85.41410.217 2.935 13.267 1.2690.0000.136 0.000 0.0000.516 0.410 845.01.521.054 0.000 3.36 0.05 180.0
12/4/2024 09:58 0.0005.48316.830 8.662 81.76412.905 3.276 14.522 1.2050.0000.066 0.000 0.0000.487 0.396 845.01.511.077 0.000 5.48 0.19 180.0
0.0007.75216.806 8.648 84.6699.193 3.604 16.018 1.7240.0000.606 0.000 0.0080.509 0.416 845.001.5271.031 0.000 7.751 0.380 179.9Avg.
0.0018.64416.736 8.576 83.62810.395 3.669 15.924 1.8350.0001.138 0.000 0.0560.477 0.367 845.001.4360.970 0.000 8.645 0.397 179.9Run 1 Avg:
Baseline 1
12/4/2024 10:00 0.3280.0000.041 0.000 0.1720.000 0.000 2.205 0.0000.0000.496 0.000 0.0000.000 0.000 845.00.170.248 0.000 0.33 0.14 180.0
Run 2 - A 30minute/60min
12/4/2024 10:02 0.00018.77712.810 6.927 67.5710.000 3.611 12.837 1.6810.0090.000 0.000 0.0000.423 0.408 845.01.240.638 0.000 18.78 0.23 180.0
12/4/2024 10:04 0.0003.45216.783 8.605 75.3070.000 3.609 11.520 1.6580.0000.469 0.000 0.0000.580 0.324 845.01.200.834 0.000 3.45 0.47 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 10:05 0.0005.06716.838 8.658 38.55215.241 2.733 8.369 0.0000.0000.000 0.000 0.0000.543 0.250 845.00.940.659 0.000 5.07 0.41 180.0
12/4/2024 10:06 0.0002.25716.903 8.665 54.4820.000 2.157 7.517 0.7820.0000.000 0.000 0.0000.446 0.236 845.01.050.864 0.000 2.26 0.70 180.0
12/4/2024 10:07 0.0003.34316.850 8.644 74.0920.000 2.636 8.630 1.4230.0000.000 0.000 0.0000.586 0.315 845.01.160.796 0.000 3.34 0.59 179.0
12/4/2024 10:08 0.0003.76616.959 8.707 82.9894.210 3.378 12.935 1.0510.0000.072 0.000 0.0000.529 0.358 845.01.350.945 0.000 3.77 0.21 180.0
12/4/2024 10:09 0.0006.70216.950 8.675 94.74215.524 3.740 17.930 2.1740.0000.191 0.000 0.0250.363 0.408 845.01.470.937 0.000 6.70 0.20 180.0
12/4/2024 10:10 0.00013.44916.880 8.634 87.67344.898 4.347 26.290 1.9260.0000.000 0.000 0.0000.380 0.393 845.01.440.979 0.000 13.45 1.49 180.0
12/4/2024 10:11 0.00012.81116.891 8.664 89.67323.084 4.016 21.399 2.0740.0000.299 0.000 0.0000.468 0.410 845.01.511.037 0.000 12.81 0.06 180.0
12/4/2024 10:12 0.0007.77616.910 8.650 82.6419.246 4.159 18.211 1.4170.0000.429 0.000 0.0000.310 0.359 845.01.360.966 0.000 7.78 0.23 180.0
12/4/2024 10:13 0.0009.36716.883 8.674 87.54524.007 3.839 19.841 1.7630.0000.056 0.000 0.0000.520 0.418 845.01.561.087 0.000 9.37 0.28 180.0
12/4/2024 10:14 0.0005.82716.845 8.643 72.00511.028 3.779 15.247 1.8460.0000.195 0.000 0.0000.499 0.311 845.01.230.919 0.000 5.83 0.17 179.0
12/4/2024 10:15 0.00013.82816.769 8.637 49.39627.929 3.238 14.920 1.3900.0000.000 0.000 0.0000.544 0.267 845.01.140.907 0.000 13.83 0.21 180.0
12/4/2024 10:16 0.0001.98716.798 8.643 64.17824.721 0.940 8.921 1.0270.0000.000 0.000 0.0000.447 0.259 845.01.170.976 0.000 1.99 0.17 180.0
12/4/2024 10:17 0.0005.77116.789 8.652 51.1123.207 3.485 11.458 0.8510.0000.000 0.000 0.0000.446 0.262 845.01.060.808 0.000 5.77 1.19 180.0
12/4/2024 10:18 0.0001.06016.856 8.646 70.72230.454 1.030 9.281 1.3650.0000.000 0.000 0.0000.509 0.272 845.01.160.926 0.000 1.06 0.03 180.0
12/4/2024 10:19 0.0003.33316.860 8.625 70.1140.000 3.122 9.430 1.5300.0000.000 0.000 0.0000.447 0.282 845.01.150.886 0.000 3.33 0.43 180.0
12/4/2024 10:20 0.0004.29516.855 8.656 54.5386.794 3.397 10.320 0.6420.0000.000 0.000 0.0000.482 0.346 845.01.230.813 0.000 4.29 0.37 180.0
12/4/2024 10:21 0.0001.95016.744 8.649 83.13937.512 1.211 12.542 1.4020.0000.000 0.000 0.0000.181 0.355 845.01.350.953 0.000 1.95 0.04 180.0
12/4/2024 10:22 0.0009.70316.763 8.595 74.40915.586 4.991 23.021 2.0930.0000.000 0.000 0.0000.518 0.316 845.01.220.883 0.000 9.70 0.39 180.0
12/4/2024 10:23 0.0003.39316.834 8.647 57.9730.000 2.747 8.887 0.7520.0000.008 0.000 0.0000.438 0.247 845.01.090.890 0.000 3.39 2.76 180.0
12/4/2024 10:24 0.0002.75716.871 8.646 61.5810.521 2.781 8.980 0.9500.0000.000 0.000 0.0000.472 0.271 845.01.120.860 0.000 2.76 0.16 180.0
12/4/2024 10:25 0.0004.40816.845 8.636 81.5830.633 3.332 10.470 1.1860.0000.094 0.000 0.0000.490 0.362 845.01.330.912 0.000 4.41 4.66 180.0
12/4/2024 10:26 0.0005.67316.857 8.582 64.4661.984 4.610 13.733 1.2340.0000.086 0.000 0.0000.545 0.275 845.01.070.781 0.000 5.67 0.19 180.0
12/4/2024 10:27 0.0004.67716.826 8.628 73.38815.663 3.166 14.833 1.8690.0000.000 0.000 0.0000.454 0.289 845.01.150.852 0.000 4.68 0.15 180.0
12/4/2024 10:28 0.0006.98416.844 8.623 91.57529.707 3.228 18.601 2.2790.0000.264 0.000 0.0000.359 0.374 845.01.451.046 0.000 6.98 0.05 180.0
12/4/2024 10:29 0.0006.18616.787 8.546 81.2534.182 3.903 15.264 1.3450.0000.555 0.000 0.0000.245 0.331 845.01.320.993 0.000 6.19 0.30 179.0
12/4/2024 10:30 0.0006.14616.750 8.616 85.23622.936 2.944 14.993 1.6890.0000.077 0.000 0.0000.250 0.352 846.01.310.911 0.000 6.15 4.20 180.0
12/4/2024 10:31 0.0007.81816.845 8.634 85.45215.741 3.378 16.234 1.8290.0000.339 0.000 0.0000.298 0.347 846.01.381.031 0.000 7.82 0.21 181.0
12/4/2024 10:32 0.00011.13916.781 8.607 73.05726.710 3.758 19.302 1.7900.0000.000 0.000 0.0000.541 0.293 846.01.050.693 0.000 11.14 0.21 180.0
0.0006.45716.706 8.580 72.68113.717 3.242 14.064 1.4340.0000.104 0.000 0.0010.444 0.323 845.101.2420.893 0.000 6.457 0.692 179.9Avg.
Spike 2
12/4/2024 10:36 0.00032.46815.346 8.436 71.33960.458 3.800 13.996 2.2430.0000.919 0.000 23.3360.243 0.318 846.024.731.128 0.800 32.47 0.16 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Run 2 - B 30minute/60min
12/4/2024 10:38 0.0005.81516.822 8.652 74.1279.639 3.818 13.463 2.0660.0000.272 0.000 0.0000.511 0.262 846.01.070.815 0.000 5.82 0.21 180.0
12/4/2024 10:39 0.0006.13716.807 8.663 70.52318.226 3.681 14.674 2.0360.0000.110 0.000 0.0000.397 0.253 846.01.110.913 0.000 6.14 0.20 180.0
12/4/2024 10:40 0.0005.99016.764 8.633 89.08739.996 2.789 17.518 2.2980.0000.547 0.000 0.0000.178 0.346 846.01.350.985 0.000 5.99 0.17 180.0
12/4/2024 10:41 0.0009.85016.815 8.630 67.57918.448 4.454 16.465 1.9320.0000.516 0.000 0.0000.427 0.241 846.01.070.885 0.000 9.85 0.49 180.0
12/4/2024 10:42 0.0005.83816.752 8.670 60.9550.000 2.712 8.545 1.3310.0000.137 0.000 0.0000.393 0.217 846.00.990.834 0.000 5.84 0.38 180.0
12/4/2024 10:44 0.0004.07716.692 8.635 68.3846.971 3.427 10.080 1.8220.0000.343 0.000 0.0000.456 0.230 846.01.080.928 0.000 4.08 0.49 180.0
12/4/2024 10:45 0.0003.48516.697 8.589 40.5777.210 1.519 6.757 0.5250.0000.084 0.000 0.0000.315 0.152 846.00.840.810 0.000 3.48 0.23 180.0
12/4/2024 10:46 0.0002.55116.739 8.636 86.10921.464 1.738 12.290 1.9340.0000.624 0.000 0.0000.254 0.304 846.01.260.983 0.000 2.55 0.15 180.0
12/4/2024 10:47 0.0007.48316.699 8.588 64.4859.605 4.398 15.904 2.6380.0000.463 0.000 0.0000.422 0.268 846.01.070.802 0.000 7.48 0.29 180.0
12/4/2024 10:48 0.0002.28816.718 8.616 38.8618.918 1.764 7.760 0.2210.0000.000 0.000 0.0000.308 0.201 846.00.880.715 0.000 2.29 0.62 180.0
12/4/2024 10:49 0.0001.43216.768 8.609 58.2050.000 2.599 6.464 1.0310.0000.083 0.000 0.0000.329 0.173 846.00.930.876 0.000 1.43 0.53 180.0
12/4/2024 10:50 0.0002.07316.822 8.617 72.30913.071 2.375 9.163 1.9850.0000.331 0.000 0.0000.358 0.180 846.00.990.949 0.000 2.07 0.16 180.0
12/4/2024 10:51 0.0004.57516.733 8.598 88.57321.597 3.262 15.264 2.3540.0000.733 0.000 0.0000.255 0.296 846.01.220.937 0.000 4.58 5.56 180.0
12/4/2024 10:52 0.00010.93216.713 8.537 81.33116.355 5.342 21.532 1.8700.0000.612 0.000 0.0000.329 0.278 846.01.190.948 0.000 10.93 0.06 180.0
12/4/2024 10:53 0.0008.12116.744 8.519 63.1360.000 4.212 12.705 1.4800.0000.951 0.000 0.0000.430 0.173 846.00.950.899 0.000 8.12 0.21 180.0
12/4/2024 10:54 0.0006.34916.785 8.578 85.85522.058 3.978 18.946 2.1140.0000.559 0.000 0.0000.256 0.267 846.01.170.947 0.000 6.35 0.04 180.0
12/4/2024 10:55 0.0005.65616.856 8.640 62.0040.000 4.098 10.533 1.5180.0000.740 0.000 0.0000.422 0.187 846.00.910.811 0.000 5.66 0.50 180.0
12/4/2024 10:56 0.0005.39016.820 8.593 76.4550.000 2.719 8.037 2.1940.0001.328 0.000 0.0000.404 0.199 846.00.970.857 0.000 5.39 0.29 179.0
12/4/2024 10:57 0.0006.19116.857 8.602 72.5783.206 4.400 12.559 2.0770.0000.569 0.000 0.0000.399 0.221 846.01.040.902 0.000 6.19 0.05 180.0
12/4/2024 10:58 0.0006.18316.914 8.623 80.55116.971 4.071 16.781 1.5260.0000.915 0.000 0.0000.295 0.248 846.01.120.941 0.000 6.18 0.20 181.0
12/4/2024 10:59 0.0005.87016.921 8.625 71.18310.763 3.581 12.959 2.0550.0000.857 0.000 0.0000.395 0.163 846.00.910.872 0.000 5.87 0.16 180.0
12/4/2024 11:00 0.0004.84616.777 8.597 71.48111.249 3.638 12.369 2.0300.0000.521 0.000 0.0000.401 0.147 846.00.900.914 0.000 4.85 0.05 180.0
12/4/2024 11:01 0.0007.23716.805 8.605 88.01423.107 3.644 17.442 2.3080.0000.846 0.000 0.0000.274 0.235 846.01.110.959 0.000 7.24 0.19 180.0
12/4/2024 11:02 0.0008.46216.797 8.585 93.01228.784 3.601 19.651 2.7370.0001.113 0.000 0.0000.188 0.292 846.01.220.950 0.000 8.46 0.18 180.0
12/4/2024 11:03 0.0009.77516.802 8.580 89.15322.006 4.134 19.606 2.6220.0001.384 0.000 0.0000.262 0.274 846.01.180.946 0.000 9.78 0.39 180.0
12/4/2024 11:04 0.0005.15916.879 8.682 77.55216.139 3.291 13.759 2.7970.0000.783 0.000 0.0000.458 0.204 846.01.020.916 0.000 5.16 0.18 180.0
12/4/2024 11:05 0.0008.82516.841 8.614 85.59620.359 4.397 18.947 2.3830.0001.217 0.000 0.0000.327 0.268 846.01.170.946 0.000 8.83 0.21 180.0
12/4/2024 11:06 0.0007.35916.815 8.579 83.28913.735 4.054 18.805 2.1960.0001.221 0.000 0.0000.334 0.240 846.01.150.999 0.000 7.36 0.19 180.0
12/4/2024 11:07 0.0009.59916.753 8.575 83.39640.634 3.639 21.282 2.0960.0001.264 0.000 0.0000.237 0.252 846.01.100.895 0.000 9.60 0.19 179.0
12/4/2024 11:08 0.0009.52916.821 8.700 82.76527.013 3.765 18.213 2.2570.0001.137 0.000 0.0000.304 0.242 845.01.090.902 0.000 9.53 0.06 180.0
0.0006.23616.791 8.612 74.23814.917 3.503 14.282 1.9480.0000.675 0.000 0.0000.344 0.234 845.971.0690.901 0.000 6.237 0.421 180.0Avg.
0.0006.34616.748 8.596 73.45914.317 3.373 14.173 1.6910.0000.390 0.000 0.0000.394 0.278 845.531.1550.897 0.000 6.347 0.557 180.0Run 2 Avg:
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
Baseline 2
12/4/2024 11:10 0.0000.0000.042 0.000 0.5270.000 0.000 2.091 0.0000.0000.246 0.000 0.0000.000 0.000 845.00.310.471 0.000 0.00 0.13 180.0
Run 3 - A 30minute/60min
12/4/2024 11:12 0.0007.20813.810 7.320 64.29611.764 2.935 12.192 2.0680.0000.286 0.000 0.0000.259 0.220 845.00.880.653 0.000 7.21 0.13 180.0
12/4/2024 11:13 0.0005.65216.687 8.579 67.1086.326 3.235 10.884 2.0870.0001.106 0.000 0.0000.385 0.137 845.00.820.815 0.000 5.65 1.07 179.0
12/4/2024 11:14 0.0006.11016.745 8.642 73.2588.547 3.445 11.560 2.4150.0001.069 0.000 0.0000.271 0.160 846.00.870.818 0.000 6.11 0.19 180.0
12/4/2024 11:15 0.0005.56116.796 8.676 67.1564.979 3.498 10.959 1.9250.0000.982 0.000 0.0000.305 0.110 845.00.690.701 0.000 5.56 0.19 180.0
12/4/2024 11:16 0.0004.36416.830 8.677 70.98512.421 3.626 13.320 2.1980.0000.803 0.000 0.0000.375 0.142 845.00.780.751 0.000 4.36 5.50 180.0
12/4/2024 11:17 0.0006.34516.905 8.657 69.7199.416 4.028 13.696 2.2020.0000.878 0.000 0.0000.367 0.119 845.00.840.900 0.000 6.34 0.05 181.0
12/4/2024 11:18 0.0006.60716.752 8.599 76.27512.657 3.668 13.632 2.7070.0001.150 0.000 0.0000.386 0.116 845.00.750.784 0.000 6.61 0.20 179.0
12/4/2024 11:19 0.0005.85616.787 8.663 73.68711.344 3.435 14.194 2.5440.0000.844 0.000 0.0000.393 0.135 845.00.760.734 0.000 5.86 0.05 180.0
12/4/2024 11:20 0.0006.95716.832 8.669 77.34419.966 3.752 15.958 2.8590.0001.094 0.000 0.0000.348 0.150 845.00.850.832 0.000 6.96 0.05 180.0
12/4/2024 11:21 0.0005.85516.804 8.619 90.70512.523 3.955 15.481 3.0260.0001.669 0.000 0.0000.222 0.256 845.01.130.928 0.000 5.85 0.20 180.0
12/4/2024 11:22 0.0004.59916.756 8.634 80.9092.148 3.657 12.782 1.8190.0001.286 0.000 0.0000.281 0.209 845.01.020.909 0.000 4.60 0.45 180.0
12/4/2024 11:24 0.0005.35816.804 8.638 81.1972.886 4.112 14.247 1.9250.0001.284 0.000 0.0000.336 0.181 845.00.970.918 0.000 5.36 0.26 180.0
12/4/2024 11:25 0.0004.91116.900 8.703 76.6608.549 3.482 13.747 2.6370.0001.299 0.000 0.0000.284 0.133 845.00.790.784 0.000 4.91 0.65 180.0
12/4/2024 11:26 0.0005.78116.814 8.630 86.0995.968 3.821 14.173 2.2720.0001.561 0.000 0.0000.314 0.190 845.01.020.965 0.000 5.78 0.26 180.0
12/4/2024 11:27 0.0005.16616.835 8.677 73.1915.814 3.315 10.851 2.5010.0001.506 0.000 0.0000.363 0.115 845.00.710.716 0.000 5.17 0.40 180.0
12/4/2024 11:28 0.0004.85716.849 8.692 76.3502.987 3.161 9.751 2.7090.0001.198 0.000 0.0000.394 0.111 845.00.780.833 0.000 4.86 0.45 180.0
12/4/2024 11:29 0.0004.21816.898 8.699 82.5403.342 2.771 10.157 1.9200.0001.485 0.000 0.0000.227 0.172 845.00.950.903 0.000 4.22 0.18 180.0
12/4/2024 11:30 0.0004.93916.939 8.688 77.44113.378 4.031 14.949 2.8770.0001.188 0.000 0.0000.429 0.126 845.00.800.819 0.000 4.94 0.06 180.0
12/4/2024 11:31 0.0005.31716.914 8.637 74.7701.491 3.928 12.566 2.4630.0001.827 0.000 0.0000.339 0.119 845.00.770.791 0.000 5.32 0.05 181.0
12/4/2024 11:32 0.0004.92416.838 8.665 75.05410.931 3.175 11.288 2.6820.0001.332 0.000 0.0000.389 0.106 845.00.750.805 0.000 4.92 6.11 179.0
12/4/2024 11:33 0.0005.20916.860 8.688 78.2411.497 4.209 12.541 2.8690.0001.525 0.000 0.0000.364 0.126 845.00.760.754 0.000 5.21 0.19 180.0
12/4/2024 11:34 0.0008.52816.844 8.619 69.6330.000 4.934 14.581 2.4110.0001.700 0.000 0.0000.364 0.102 845.00.700.749 0.000 8.53 0.49 180.0
12/4/2024 11:35 0.0001.92216.816 8.607 62.6580.000 2.827 8.228 1.6530.0001.408 0.000 0.0000.321 0.066 845.00.660.794 0.000 1.92 0.17 180.0
12/4/2024 11:36 0.0003.57316.843 8.579 77.0983.891 3.997 12.982 2.6560.0001.604 0.000 0.0000.347 0.116 845.00.730.747 0.000 3.57 2.79 180.0
12/4/2024 11:37 0.0008.59716.902 8.620 89.46525.036 4.635 19.968 2.7750.0001.669 0.000 0.0000.190 0.177 845.00.920.855 0.000 8.60 0.44 180.0
12/4/2024 11:38 0.0003.43316.890 8.643 73.1780.754 3.865 12.629 2.4300.0001.570 0.000 0.0000.335 0.107 845.00.740.793 0.000 3.43 0.19 180.0
12/4/2024 11:39 0.0006.21916.866 8.623 93.41054.379 3.130 22.012 3.1500.0001.549 0.000 0.0000.211 0.183 845.00.970.905 0.000 6.22 0.20 180.0
12/4/2024 11:40 0.00014.22416.806 8.631 87.50039.980 4.520 24.243 2.7450.0001.230 0.000 0.0000.254 0.205 845.00.980.861 0.000 14.22 0.06 180.0
12/4/2024 11:41 0.00014.83816.777 8.649 80.97142.204 4.436 24.265 2.1700.0001.318 0.000 0.0000.264 0.182 845.00.910.819 0.000 14.84 0.06 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 11:42 0.0009.37816.736 8.641 81.48928.002 3.700 18.530 2.2990.0001.654 0.000 0.0000.264 0.180 845.00.920.846 0.000 9.38 0.05 180.0
0.0006.21716.728 8.602 76.94612.106 3.709 14.212 2.4330.0001.302 0.000 0.0000.319 0.148 845.030.8410.816 0.000 6.217 0.705 180.0Avg.
Spike 3
12/4/2024 11:44 0.00029.32515.374 8.526 67.34679.934 4.415 17.290 2.8140.0002.149 0.000 22.2490.248 0.262 845.023.310.807 0.775 29.32 0.21 181.0
Run 3 - B 30minute/60min
12/4/2024 11:47 0.0005.38516.734 8.653 72.4445.682 4.022 14.632 2.6930.0001.581 0.000 0.0000.293 0.104 845.00.680.709 0.000 5.39 0.05 180.0
12/4/2024 11:48 0.0004.53916.728 8.690 72.2906.539 3.569 11.750 2.7550.0001.619 0.000 0.0000.350 0.089 845.00.700.781 0.000 4.54 0.19 180.0
12/4/2024 11:49 0.0004.05616.810 8.694 72.0552.388 3.724 12.416 2.5780.0001.807 0.000 0.0000.415 0.085 845.00.720.826 0.000 4.06 0.17 180.0
12/4/2024 11:50 0.0006.73016.798 8.718 72.58112.985 3.771 14.919 2.7670.0001.446 0.000 0.0000.303 0.094 845.00.650.695 0.000 6.73 0.17 180.0
12/4/2024 11:51 0.0006.22416.756 8.649 68.3277.795 3.921 13.869 2.3860.0001.768 0.000 0.0000.343 0.066 845.00.650.778 0.000 6.22 0.47 180.0
12/4/2024 11:52 0.0001.43416.804 8.666 59.1050.000 3.214 8.367 1.8520.0001.568 0.000 0.0000.414 0.051 845.00.620.782 0.000 1.43 0.42 180.0
12/4/2024 11:53 0.0001.79316.803 8.663 40.7040.000 2.591 6.494 0.9740.0001.619 0.000 0.0000.278 0.022 845.00.310.404 0.000 1.79 0.15 180.0
12/4/2024 11:54 0.0003.45716.894 8.677 63.2713.092 1.776 6.194 1.8700.0001.344 0.000 0.0000.275 0.016 845.00.370.505 0.000 3.46 0.15 180.0
12/4/2024 11:55 0.0005.64516.920 8.674 74.9040.000 2.867 8.941 2.6270.0001.633 0.000 0.0000.264 0.062 845.00.730.913 0.000 5.64 0.21 180.0
12/4/2024 11:56 0.0004.80316.948 8.707 77.82620.387 3.470 15.218 2.9360.0001.575 0.000 0.0000.404 0.088 845.00.710.800 0.000 4.80 0.72 180.0
12/4/2024 11:57 0.0004.95616.943 8.672 77.6459.391 3.707 13.378 3.0250.0001.845 0.000 0.0000.300 0.072 845.00.720.865 0.000 4.96 0.19 180.0
12/4/2024 11:58 0.0003.58816.856 8.619 79.9529.322 3.062 12.142 2.0760.0001.764 0.000 0.0000.153 0.084 845.00.780.925 0.000 3.59 0.19 179.0
12/4/2024 11:59 0.0006.33916.896 8.627 74.0458.547 4.315 15.304 2.8810.0001.746 0.000 0.0000.411 0.065 845.00.640.767 0.000 6.34 0.05 180.0
12/4/2024 12:00 0.0004.82916.892 8.673 81.3299.426 3.563 13.535 2.1570.0001.602 0.000 0.0000.271 0.135 845.00.890.928 0.000 4.83 0.16 180.0
12/4/2024 12:01 0.0006.88616.908 8.625 84.17311.264 4.020 17.201 2.4870.0002.063 0.000 0.0000.246 0.125 845.00.860.916 0.000 6.89 0.18 180.0
12/4/2024 12:03 0.0008.66316.860 8.601 84.32018.550 4.180 18.714 2.4220.0001.898 0.000 0.0000.200 0.155 845.00.930.932 0.000 8.66 0.44 180.0
12/4/2024 12:04 0.0005.57616.879 8.676 74.64111.574 3.784 15.541 2.7590.0001.810 0.000 0.0000.361 0.082 845.00.730.846 0.000 5.58 0.21 180.0
12/4/2024 12:05 0.0005.81716.938 8.699 84.52322.687 3.583 16.154 2.3270.0001.846 0.000 0.0000.236 0.140 845.00.820.814 0.000 5.82 0.30 180.0
12/4/2024 12:06 0.0008.02616.966 8.657 67.4211.430 4.963 14.849 2.2530.0002.208 0.000 0.0000.339 0.068 845.00.670.805 0.000 8.03 0.61 180.0
12/4/2024 12:07 0.0001.82316.943 8.674 67.0790.000 1.981 6.576 1.9400.0001.953 0.000 0.0000.398 0.064 845.00.670.819 0.000 1.82 0.18 180.0
12/4/2024 12:08 0.0004.22916.950 8.639 76.54617.649 4.029 15.407 2.8980.0002.011 0.000 0.0000.460 0.072 845.00.690.813 0.000 4.23 0.40 180.0
12/4/2024 12:09 0.0002.81716.995 8.680 71.6477.734 2.456 10.901 2.4670.0002.054 0.000 0.0000.332 0.087 845.00.730.830 0.000 2.82 3.67 180.0
12/4/2024 12:10 0.0004.23016.981 8.651 70.20820.960 3.474 17.266 2.3600.0002.218 0.000 0.0000.310 0.093 845.00.700.768 0.000 4.23 0.20 180.0
12/4/2024 12:11 0.0004.03916.974 8.632 65.8592.648 4.487 12.701 2.3390.0002.236 0.000 0.0000.373 0.062 845.00.670.824 0.000 4.04 0.50 180.0
12/4/2024 12:12 0.0003.78816.944 8.671 83.79921.975 2.851 13.407 1.9700.0002.156 0.000 0.0000.258 0.161 845.00.920.900 0.000 3.79 0.18 180.0
12/4/2024 12:13 0.00010.98616.837 8.593 88.50838.416 4.125 22.920 2.8070.0002.130 0.000 0.0000.292 0.176 845.00.980.936 0.000 10.99 0.19 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 12:14 0.00013.13816.887 8.566 76.12220.502 4.639 21.573 2.8930.0002.261 0.000 0.0000.423 0.081 845.00.750.886 0.000 13.14 0.19 181.0
12/4/2024 12:15 0.0004.07816.787 8.607 64.11912.145 3.617 12.435 2.2260.0001.911 0.000 0.0000.280 0.042 845.00.640.831 0.000 4.08 0.05 180.0
12/4/2024 12:16 0.0005.24316.771 8.614 74.41222.936 3.650 16.954 2.6900.0001.919 0.000 0.0000.415 0.087 845.00.680.752 0.000 5.24 1.50 180.0
12/4/2024 12:17 0.0007.89316.829 8.630 80.35821.525 3.853 16.819 2.1800.0002.451 0.000 0.0000.283 0.071 845.00.811.004 0.000 7.89 0.58 180.0
0.0005.36716.874 8.653 73.34011.585 3.575 13.886 2.4200.0001.868 0.000 0.0000.323 0.087 845.000.7140.812 0.000 5.368 0.422 180.0Avg.
0.0005.79216.801 8.628 75.14311.845 3.642 14.049 2.4260.0001.585 0.000 0.0000.321 0.118 845.020.7770.814 0.000 5.792 0.564 180.0Run 3 Avg:
Baseline 3
12/4/2024 12:19 0.0000.0000.042 0.000 0.5740.000 0.000 2.008 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.470.699 0.000 0.00 0.19 180.0
Post CTS
12/4/2024 12:21 0.0000.0000.028 0.000 0.0000.000 0.000 0.706 0.0000.0100.000 95.483 0.0000.000 0.000 845.064.010.528 0.000 0.00 0.21 180.0
12/4/2024 12:21 0.0000.0000.024 0.000 0.0000.000 0.000 0.987 0.0000.0000.000 96.235 0.0000.000 0.000 845.064.580.626 0.000 0.00 0.06 180.0
12/4/2024 12:21 0.0000.0000.025 0.000 0.0000.000 0.000 0.598 0.0000.0020.000 96.566 0.0000.000 0.000 845.064.840.695 0.000 0.00 0.22 180.0
Post NO2/Mid O2
12/4/2024 12:23 94.2910.0000.013 0.000 0.0000.000 0.697 1.802 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.090.136 0.000 94.29 10.63 180.0
12/4/2024 12:23 94.8970.0000.010 0.000 0.0000.000 0.669 1.810 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.070.099 0.000 94.90 10.63 180.0
12/4/2024 12:24 96.3790.0000.015 0.000 0.0000.000 0.675 1.813 0.0000.0000.000 0.000 0.0000.001 0.015 845.00.480.675 0.000 96.38 10.84 180.0
Post 5-Gas
12/4/2024 12:25 1.761232.1000.012 4.635 0.000496.612 2.427 1.579 7.4480.0190.592 2.015 245.3430.000 0.000 845.0247.130.660 9.851 233.86 6.30 180.0
12/4/2024 12:25 0.071235.7120.015 4.681 0.000504.155 2.477 1.421 1.8500.1720.632 1.694 249.4120.000 0.000 845.0251.000.683 9.999 235.78 2.71 180.0
12/4/2024 12:25 0.813236.6750.017 4.731 0.000509.011 2.507 1.583 1.4450.2281.359 1.571 251.3900.000 0.000 845.0253.040.904 10.068 237.49 1.19 180.0
12/4/2024 12:25 0.000237.4030.014 4.720 0.000511.341 2.430 1.900 7.6620.0901.610 1.541 251.8750.000 0.000 845.0253.881.472 10.091 237.40 0.63 180.0
12/4/2024 12:25 0.000237.5840.012 4.764 0.000511.374 2.376 1.538 8.5530.0441.126 1.390 251.9430.000 0.000 845.0254.252.064 10.138 237.58 0.46 180.0
12/4/2024 12:25 0.000236.7970.010 4.732 0.000509.258 2.556 1.912 7.4170.0920.689 1.446 252.0470.000 0.000 845.0253.811.196 10.118 236.80 0.29 180.0
12/4/2024 12:26 0.000237.0820.014 4.752 0.000509.271 2.539 1.502 7.4870.0381.123 1.383 252.3490.000 0.000 845.0254.001.093 10.134 237.08 0.23 180.0
12/4/2024 12:26 0.000238.1840.011 4.754 0.000511.947 2.548 1.720 7.4590.1480.889 1.487 252.1580.000 0.000 845.0253.800.975 10.118 238.18 0.29 180.0
End of Test Purge
12/4/2024 12:45 0.0000.0000.006 0.000 0.7910.000 0.000 2.052 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.370.557 0.000 0.00 0.00 180.0
12/4/2024 12:45 0.0000.0000.009 0.000 0.7200.000 0.000 2.029 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.390.592 0.000 0.00 0.13 180.0
12/4/2024 12:45 0.0000.0000.011 0.000 0.2980.000 0.000 1.964 0.0280.0000.000 0.000 0.0000.000 0.000 845.00.350.523 0.000 0.00 0.00 180.0
12/4/2024 12:45 0.0000.0000.010 0.000 0.5490.000 0.000 1.962 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.390.578 0.000 0.00 0.17 180.0
GAS, Inc.
Date Time
H2O
(%)
CO2
(%)
CO
(ppmvw)
NO
(ppmvw)
NO2
(ppmvw)
CH4
(ppmvw)
N2O
(ppmvw)
NH3
(ppmvw)
SO2
(ppmvw)
C2H4
(ppmvw)
HCL
(ppmvw)
HF
(ppmvw)
C2H6
(ppmvw)
C3H8
(ppmvw)
C6H14
(ppmvw)
C2H4O
(ppmvw)
SF6
(ppmvw)
Nox
(ppmvw)
VOC
(ppmvw)
Oxygen
(%)
Cell
Temp
(C).
Ambient
Press.
(mbar)
12/4/2024 12:45 0.0000.0000.005 0.000 0.3070.000 0.000 2.079 0.0260.0000.000 0.000 0.0000.000 0.000 845.00.410.621 0.000 0.00 0.00 180.0
12/4/2024 12:45 0.0000.0000.007 0.000 0.3870.000 0.000 1.894 0.0000.0000.000 0.000 0.0000.000 0.000 845.00.470.698 0.000 0.00 0.00 180.0
12/4/2024 12:45 0.0000.0000.009 0.000 1.0100.000 0.000 1.940 0.0000.0020.000 0.000 0.0000.000 0.000 845.00.350.520 0.000 0.00 0.14 180.0
12/4/2024 12:45 0.0000.0000.006 0.000 0.7670.000 0.000 1.795 0.0000.0000.000 0.000 0.0000.033 0.000 845.00.400.595 0.000 0.00 0.21 180.0
12/4/2024 12:46 0.0000.0000.010 0.000 0.0000.000 0.000 2.049 0.3600.0000.000 0.000 0.0000.000 0.000 845.00.440.653 0.000 0.00 0.00 180.0
12/4/2024 12:46 0.0000.0000.012 0.000 0.0000.000 0.000 2.012 0.1730.0090.000 0.000 0.0000.000 0.000 845.00.330.491 0.000 0.00 0.00 180.0
GAS, Inc.